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HomeMy WebLinkAboutMO-88513_91340_CA_MRP_20181001_2nd 2018 Semiannual Reporti` APEX October 1, 2018 Ms. Trudy Beverly Hydrogeologist UST Section — Corrective Action Branch Division of Waste Management — Mooresville Regional Office North Carolina Department of Environmental Quality 610 East Center Avenue, Suite 301 Mooresville, North Carolina 28115 RE: Semiannual Monitoring Report for the Kannapolis Booster Station Colonial Pipeline Company, Concord, North Carolina Incident Number: 14414 & 91340 Dear Ms. Beverly: Apex Companies, LLC (dba Apex Engineering, P.C.) is pleased to submit the March 2018 — August 2018 Semiannual Monitoring Report for the Colonial Pipeline Company Kannapolis Booster Station. This report also includes a summary of analytical results for private water supply well sampling performed in August 2018. Should you have any questions concerning this report, please do not hesitate to contact the undersigned at 704-799-6390. Sincerely, Apex Companies, LLC Andrew Street, CHMM Senior Project Manager Enclosure cc: John Culbreath, Colonial Pipeline Company Jeff Morrison, Colonial Pipeline Company Kathleen Roush, P.G. Program Manager NC Geology License No. 1353 Prepared for: Colonial Pipeline Company a 1185 Sanctuary Parkway Suite 100 Alpharetta, Georgia 30009 Semiannual Groundwater Monitoring Report Kannapolis Booster Station Incident Number 14414 & 91340 March 2018 — August 2018 A APEX 10610 Metromont Parkway, Suite 206 Charlotte NC 28269 Prepared by: Reviewed by: CA �z .�� .tq Andrew Street, CHMM Kathleen Roush, P.G. - Senior Project Manager Program Manager x x? 13 1n�i r NC GeologyLicense No. 135i T� N!G, = .FpL OG\�•••�J,, A.`,., October 2018 Apex Companies, LLC • 10610 Metromonl Parkway, Suite 206 - Charlotte, NC 28269 T 704.799.6390 - F 704.799.6395 • apexcos.com Semiannual Monitoring Report, March 2018-August 2018 Colonial Pipeline Company, Kannapolis Booster Station TABLE OF CONTENTS October 1, 2018 Page 1.0 INTRODUCTION....................................................................................................................................1 2.0 PROJECT BACKGROUND..................................................................................................................1 2.1 Historic Site Impacts................................................................................................................. 1 2.2 Recent Site Impacts.................................................................................................................. 2 3.0 GROUNDWATER SAMPLING FIELD ACTIVITIES............................................................................ 3 3.1 Groundwater Gauging.............................................................................................................. 3 3.2 Groundwater Sampling and Analysis....................................................................................... 3 4.0 GROUNDWATER FINDINGS............................................................................................................... 4 4.1 Well Gauging Results and Groundwater Flow........................................................................ 4 4.2 Groundwater Analytical Results............................................................................................... 5 5.1 Air Sparge Trench Remediation System................................................................................. 6 5.2 Bio-Sparge and Bio-Venting Systems..................................................................................... 6 6.0 WATER SUPPLY WELL SAMPLING.................................................................................................. 6 6.1 Water Supply Well Sampling and Analysis.............................................................................. 6 6.2 Water Supply Well Analytical Results...................................................................................... 7 7.0 CONCLUSIONS AND RECOMMENDATIONS.................................................................................... 7 Tables Table 1 Well Sampling and Analysis Program Table 2 Groundwater Elevation Summary Table 3 Recovery Well Gauging Data Table 4 Groundwater Analytical Data Table 5 Summary of Water Quality Data for Residential Wells Figures Figure 1 Site Location Map Figure 2 Site Plan Figure 3 Recovery Well Locations Figure 4 Groundwater Potentiometric Surface Map - Surficial Saprolite Unit - August 16, 2018 Figure 5 Benzene Isoconcentration Map - August 2018 Figure 6 Water Supply Well Location Map Appendices Appendix A Groundwater Sampling Field Logs Appendix B Laboratory Analytical Reports APEX Semiannual Monitoring Report, March 2018-August 2018 October 1, 2018 Colonial Pipeline Company, Kannapolis Booster Station Page 1 1.0 INTRODUCTION This report summarizes the semiannual groundwater monitoring activities and remediation system operations performed at the Colonial Pipeline Company (CPC) Kannapolis Booster Station located at 9301 Mooresville Road in Concord, North Carolina (the site) from March 2018 through August 2018. A site location map is provided as Figure 1. This report also includes a summary of analytical results for the annual private water supply well sampling performed in August 2018. Apex Companies, LLC (Apex; dba Apex Engineering, P.C.) prepared this Semiannual Groundwater Monitoring Report on behalf of CPC for submittal to the North Carolina Department of Environmental Quality (NCDEQ), Underground Storage Tank Section. 2.0 PROJECT BACKGROUND The facility consists of a control building, a switch gear building, eight large electric booster pumps, a 40-inch diameter pipeline for transporting gasoline products (Line 1), a 36-inch diameter pipeline for transporting kerosene, diesel fuel and other fuel oil products (Line 2), two 21,000-gallon above ground storage tanks and associated above -ground and below -ground piping and valves. The facility has been in operation since the 1970s. 2.1 Historic Site Impacts Formal assessment and remediation activities were initiated at the facility in 1995. Three areas of concern were identified at the facility including (1) the Line 2 Manifold Area; (2) the Line 1 Manifold Area; and, (3) the Line 1 Pig Signal Area. Impacts identified during the 1995 assessment are included in Incident Number 14414. Historic petroleum impacts in the Line 2 Manifold Area are the result of a kerosene release. Excavation of impacted soils was limited due to the presence of pumps, footings, and associated underground piping and valves. A light non -aqueous phase liquid (LNAPL) recovery system and a soil vapor extraction (SVE) system were installed in this area. A dissolved phase plume consisting of gasoline -related compounds was identified in the Line 1 Manifold Area. A limited amount of impacted soil was excavated in this area and an SVE system was installed. APEX Semiannual Monitoring Report, March 2018-August 2018 October 1, 2018 Colonial Pipeline Company, Kannapolis Booster Station Page 2 Gasoline impacted soil was also identified in the Line 1 Pig Signal Area as a result of a release from a leaking pipe fitting. Approximately 1,000 tons of soil was excavated and thermally treated in this area. The excavation extended to bedrock, removing the source material; however, the release resulted in dissolved phase groundwater impacts. An air sparge trench located near the downgradient property boundary and a non -discharge pump and treatment system were installed in the late-1990s to prevent off -site migration of petroleum hydrocarbons. The air sparge trench is currently in operation. The groundwater pump and treatment system was taken off-line in April 2010, following approval from NCDEQ on April 12, 2010. The LNAPL recovery and SVE systems were taken off-line in October 2010, following approval from NCDEQ on September 29, 2010. 2.2 Recent Site Impacts A 920-gallon petroleum release occurred at the site on March 13, 2015 when a valve gasket failed near the Line 2, Unit 4 booster pump. Emergency response and abatement activities were performed from March 13, 2015 through August 11, 2015. On August 13, 2015, a three -quarter -inch nipple on Line 2 was struck by a piece of equipment during backfilling operations resulting in a 5,000- gallon petroleum release over the recently remediated area. Approximately 4,750 gallons of diesel fuel were recovered during initial response activities and subsequent recovery well evacuation efforts. Residual soil impacts were detected at areas where additional excavation was not feasible due to the presence of booster pumps, footings, and associated underground piping and valves. Approximately 750 tons of petroleum -impacted soil was removed from the release area during the initial response activities associated with both 2015 releases. Impacts identified during the 2015 assessment are included in Incident Number 91340. A Corrective Action Plan (CAP) and CAP Addendum were submitted to NCDEQ on April 15, 2016 and July 12, 2016, respectively. The CAP documents specified installation and operation of a bio- venting and bio-sparge system to address residual soil impacts and dissolved phase groundwater impacts. The CAP was approved on May 6, 2016 and the CAP Addendum was approved on July 28, 2016. The semiannual groundwater monitoring program for the site incorporates the groundwater monitoring programs associated with Incident Numbers 14414 and 91340. A summary of the Groundwater Monitoring Program for the site is provided as Table 1. APEX Semiannual Monitoring Report, March 2018-August 2018 October 1, 2018 Colonial Pipeline Company, Kannapolis Booster Station Page 3 3.0 GROUNDWATER SAMPLING FIELD ACTIVITIES The following tasks were performed at the site from March 2018 through August 2018 summarized in this report: • Performed semiannual groundwater monitoring event on August 16, 2018; • Performed private water supply well sampling on August 23, 2018; • Operated air sparge trench remediation system near downgradient property boundary; and, • Operated biosparge and bioventing remediation system in the distillate manifold. 3.1 Groundwater Gauging Prior to sampling, groundwater monitoring wells were gauged to measure the depth to groundwater and LNAPL, if present. Upon arriving at the site, wells were opened and allowed to equilibrate. Wells were gauged in accordance with the United States Environmental Protection Agency (USEPA) Region IV Science and Ecosystem Support Division Field Branches Quality System and Technical Procedures. The wells were gauged in order of potential impact, moving from upgradient wells, to downgradient wells and finally source area wells. Depths to groundwater and LNAPL were measured using an electronic oil/water interface probe capable of measuring to an accuracy of 0.01 feet. The interface probe was thoroughly decontaminated before collecting measurements at each subsequent monitoring well. A total of ten monitoring wells (MW-1, MW-4, MW-5, MW-6, MW-8, MW-13, MW-23, MW-24, MW-25, and MW-25D) and 12 recovery wells (SB- 4, SB-6, SB-8, S13-9, S13-10, S13-11, S13-12, S13-14, S13-15, S13-16, S13-18, and RW-1 were gauged during the August 2018 monitoring event. Recovery well RW-2 was not located during the gauging event. The monitoring well and recovery well locations are shown on Figure 2 and Figure 3, respectively. 3.2 Groundwater Sampling and Analysis Groundwater samples were collected from seven monitoring wells (MW-4, MW-6, MW-8, MW-13, MW-24, MW-25, and MW-25D) during the August 2018 monitoring event. At each monitoring well, a baseline set of water quality stabilization data was measured (temperature, specific conductance, pH, oxidation reduction potential, dissolved oxygen, and turbidity), and recorded. The total volume of water in each well was calculated and approximately three well volumes were purged from each well. APEX Semiannual Monitoring Report, March 2018-August 2018 October 1, 2018 Colonial Pipeline Company, Kannapolis Booster Station Page 4 A complete set of parameter readings were recorded in -situ each time one well volume was purged. Monitoring wells were purged and sampled with disposable bailers. Groundwater sampling logs documenting the groundwater monitoring well purging and sampling are provided as Appendix A. After purging an adequate volume of water from each well, a sample was retrieved and transferred to laboratory supplied bottleware and immediately placed on ice and maintained at a temperature of approximately 4°C. Groundwater samples were transported under standard chain -of -custody procedures to Shealy Environmental Services, Inc. of West Columbia, South Carolina. Groundwater samples were analyzed for benzene, ethylbenzene, toluene, xylenes (BTEX), by EPA Method 602. Monitoring wells MW-4, MW-6, MW-8, and MW-13 ware also analyzed for methyl tertiary -butyl ether (MTBE) by EPA method 602. Groundwater samples from three monitoring wells associated with the diesel fuel releases that occurred on March 13, 2015 and August 13, 2015 (MW-24, MW-25, and MW-25D) were also analyzed for semi -volatile organic compounds by EPA Method 625; and Massachusetts Department of Environmental Protection extractable petroleum hydrocarbons and volatile petroleum hydrocarbons. 4.0 GROUNDWATER FINDINGS 4.1 Well Gauging Results and Groundwater Flow Depth to water and top of well casing elevation data from the monitoring wells were used to calculate groundwater elevations relative to an on -site benchmark referenced to mean sea level datum. LNAPL was not detected in any of the groundwater monitoring wells or recovery wells gauged in August 2018. A summary of groundwater level measurements is provided in Table 2. A groundwater potentiometric map for the surficial unit using water level elevation data from the August 2018 sampling event is provided as Figure 4. The potentiometric map depicts the direction of groundwater flow to the southeast. A hydraulic gradient of approximately 0.03 feet per foot was measured between the 720 feet potentiometric contour line near MW-23 and the 705 feet potentiometric contour line near MW-8. Groundwater flow patterns observed in August 2018 are consistent with historic sampling events. LNAPL was not detected in any of the 12 recovery wells gauged during the August 16, 2018 sampling event. A summary of historic recovery well gauging data is provided as Table 3. APEX Semiannual Monitoring Report, March 2018-August 2018 October 1, 2018 Colonial Pipeline Company, Kannapolis Booster Station Page 5 4.2 Groundwater Analytical Results Groundwater sampling activities performed at the site focused on collecting analytical data from the upgradient, downgradient, and central plume areas to evaluate Constituents of Concern trends over time. The analytical results for groundwater samples collected during this monitoring period were compared to the 15A NCAC 2L .0202 Groundwater Quality Standards (21- Standards) and to the 15A NCAC 2B .0215 Surface Water Standards (2B Standards) for a Water Supply II, High Quality Waters surface water classification following the Risk Based Corrective Action Rules for non -UST releases of petroleum under North Carolina House Bill 765. A groundwater concentration map showing the concentration of benzene in the groundwater from the August 2018 event is provided as Figure S. Laboratory analytical reports and chain -of -custody records for the groundwater samples are presented in Appendix B. The August 2018 results indicate that the hydrocarbon plume is stable compared to the historic monitoring results. A summary of groundwater analytical results is provided in Table 4. Notable results from the August 2018 sampling event are summarized below: • Benzene was detected in MW-13 (5.2 micrograms per liter [pg/L]) and MW-24 (2.0 pg/L during the August 2018 sampling event. These concentrations exceeded both the 2L and 2B Standards of 1.0 pg/L and 1.19 pg/L, respectively. • MTBE was detected in MW-8 (6.6 pg/L) and MW-13 (2.5 pg/L) during the August 2018 sampling event. Concentrations were below the 2L and 2B Standards of 20 pg/L and 19 pg/L, respectively. • Ethylbenzene, toluene, total xylenes, acenaphthene, anthracene, fluoranthene, phenanthrene, and pyrene were detected in MW-24 and pyrene was detected in MW-25 during the August 2018 sampling event at concentrations below the 2L and 2B Standards. • Aliphatic and aromatic petroleum compounds were detected in MW-24 during the August 2018 sampling event. The detected concentrations observed included C9-C12 Aliphatics at 410 pg/L, C5-C8 Aliphatics at 740 pg/L, C9-C10 Aromatics at 330 pg/L, and C11-C22 Aromatics at 130 pg/L. C5-C8 Aliphatics and C9-C22 Aromatics exceeded NCAC 2L groundwater standards (400 pg/L and 200 pg/L respectively). C5-C8 Aliphatics and C9- I PEP Semiannual Monitoring Report, March 2018-August 2018 October 1, 2018 Colonial Pipeline Company, Kannapolis Booster Station Page 6 C12 Aromatics also exceeded protective values for surface waters at 125 pg/L and 180 pg/L respectively. 5.1 Air Sparge Trench Remediation System The air sparge trench remediation system was brought on-line in June 1998 to treat shallow groundwater prior to migration off -site. The air sparge system continues to operate to aid in the removal of benzene and MTBE from groundwater in the vicinity of well MW-8 and MW-13. It was shut down approximately two weeks prior to the August monitoring event to allow for collection of representative groundwater samples. 5.2 Bio-Sparge and Bio-Venting Systems The bio-sparge and bioventing systems were brought on-line on March 7, 2017 to address soil and groundwater impacts associated with the 2015 diesel fuel releases. The systems were shut down approximately two weeks prior to the August monitoring event to allow for collection of representative groundwater samples. 6.0 WATER SUPPLY WELL SAMPLING 6.1 Water Supply Well Sampling and Analysis Annual water supply well sampling was performed by CPC personnel in the site vicinity on August 23, 2018. Colonial voluntarily provides point -of -entry (POE) treatment systems (i.e., activated carbon vessels) at several water supply wells identified in Figure 6. Seven water supply wells were sampled during the August 22, 2017 sampling event. Samples were collected in laboratory supplied glassware, placed in an ice -filled cooler, and transferred to Prism Laboratories, Inc. of Charlotte, North Carolina under chain -of -custody procedures for analysis of BTEX, MTBE, and naphthalene. APEX Semiannual Monitoring Report, March 2018-August 2018 October 1, 2018 Colonial Pipeline Company, Kannapolis Booster Station Page 7 6.2 Water Supply Well Analytical Results Laboratory analytical results indicate that BTEX and naphthalene were not detected in the seven water supply wells at the influent of the POE systems. MTBE was detected in DW-Maurer-Influent at a concentration of 1.9 pg/L and in the DW-Tucker-Influent at a concentration of 1.3 pg/L which are below the 2L Standard of 20 pg/L. MTBE has historically been present in both of these wells. No other petroleum hydrocarbon constituents were detected in the water supply wells. A summary of historic and recent water supply well sampling analytical results is provided as Table 5. A copy of the laboratory analytical report and chain -of -custody records are included in Appendix B. 7.0 CONCLUSIONS AND RECOMMENDATIONS During the August 2018 monitoring event, residual LNAPL was not detected in recovery wells installed in response to the 2015 diesel fuel releases. Benzene, C5-C12 Aliphatics and C9-C22 Aromatics exhibited concentrations above the applicable 2B and/or 2L Standards in MW-24. This well is located approximately 360 feet from the surface water body. These detections are attributed to the 2015 diesel fuel releases. The recently installed bio-sparge and bioventing system will aid in the removal of these remaining hydrocarbon constituents from the subsurface. Monitoring wells MW-25 and MW-25D, located nearly 250 feet from the surface water body, continue to delineate the downgradient boundary of the plume in this area. Both monitoring wells were free of any detections during the August 2018 sampling event with the exception of a detection in MW-25 of pyrene at an estimated concentration of 0.51 pg/L, below the applicable 2L and 2B Standards. Benzene was detected in MW-13 during the August 2018 sampling event at concentrations greater than the 2L and 2B Standards. Detections of benzene at MW-13 are associated with the 1995 release as historic groundwater analytical data indicates the presence of benzene in this well since February 1998. Benzene concentrations in MW-13 have been decreasing over time, with seasonal fluctuations. Although the concentration during this monitoring event is greater than the three previous sampling events, the long-term trend is still downward. Although 2B Surface Water Standards were exceeded, any discharge of the groundwater plume to surface water would not likely contravene the surface water standards within the surface water body itself. APEX Semiannual Monitoring Report, March 2018-August 2018 October 1, 2018 Colonial Pipeline Company, Kannapolis Booster Station Page 8 During the August 2018 sampling event, MTBE was detected in MW-8 (6.6 pg/L) and MW-13 (2.5 pg/L). Concentrations were below the 2L and 2B Standards of 20 pg/L and 19 pg/L, respectively. The historic concentration trends of MTBE show a continual decrease in both MW-8 and MW-13. The air sparge system in the vicinity of wells MW-8 and MW-13 continues to operate and aid in the removal of benzene and MTBE from groundwater. Results of the water supply well sampling indicated an absence of petroleum hydrocarbon constituents in the water supply wells with the exception of MTBE which was detected in the Maurer well (DW-Maurer-Influent) and the Tucker Well (DW-Tucker-Influent) at concentrations below the 2L Standard of 20 pg/L. MTBE has been historically detected in both of these wells and both properties are served by POE systems. Colonial will continue to maintain the off -site POE water treatment systems and continue annual sampling of select water supply wells. Apex proposes that based on the absence of LNAPL detections during the reporting period, and the stable and/or decreasing dissolved phase petroleum concentration trends observed at the site since the historic and recent 2015 release incidents, the reporting schedule for the site be modified from semiannual to annual. Following NCDEQ approval, one annual report will be submitted on or before October 1st of each year detailing the semiannual monitoring well sampling and annual water supply well sampling results. The next semiannual groundwater sampling event is scheduled to occur in February 2019. APEX TABLES �1 APEX Table 1 Well Sampling and Analysis Program Colonial Pipeline Company Kannapolis Booster Station Concord, NC Top of Casing Total Depth Screen Sampling/Gauging Well ID Elevation (ft. BGS) Interval Analysis Frequency (ft. MSL) (ft. BGS) MW-1 717.24 23.5 3.5 - 23.5 Gauge Only Semiannual MW-4 729.9 28 8 - 28 BTEX and MTBE by EPA Method 602 Semiannual MW-5 726.87 19 4 -19 Gauge Only Semiannual MW-6 724.61 13 3 -13 BTEX and MTBE by EPA Method 602 Semiannual MW-8 710.26 20 10 - 20 BTEX and MTBE by EPA Method 602 Semiannual MW-13 707.35 22 2 - 22 BTEX and MTBE by EPA Method 602 Semiannual MW-23 726.70 15 5 - 15 Gauge Only Semiannual BTEX by EPA Method 602; MW-24 724.61 10 10 - 20 SVOCs by EPA Method 625; MADEP Semiannual VPH and EPH BTEX by EPA Method 602; MW-25 724.32 17 7 - 17 SVOCs by EPA Method 625; MADEP Semiannual VPH and EPH BTEX by EPA Method 602; MW-25D 724.00 74 69 - 74 SVOCs by EPA Method 625; MADEP Semiannual VPH and EPH Notes: -- - unknown ft. MSL - Feet above mean sea level ft. BGS - Below ground surface BTEX - Benzene, toluene, ethylbenzene, and xylenes MTBE - Methyl tert-butyl ether EPA - United States Environmental Protection Agency SVOCs - Semi -volatile Organic Compounds MADEP - Massachusetts Department of Environmental Protection VPH - Volatile Petroleum Hydrocarbons EPH - Extricable Petroleum Hydrocarbons Page 1 of 1 Table 2 Groundwater Elevation Summary Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well Number Date Depth to Water (ft.) Elevation of TOC (ft. MSL) Groundwater Elevation ft. MSL M W-1 717.24 1 /31 /2001 6.70 710.54 2/7/2001 6.84 710.40 2/8/2001 6.80 710.44 2/9/2001 6.74 710.50 2/14/2001 6.22 711.02 2/21 /2001 6.54 710.70 8/16/2001 6.75 710.49 2/27/2002 6.32 710.92 8/28/2002 7.43 709.81 2/18/2003 5.15 712.09 8/18/2003 5.63 711.61 2/19/2004 5.45 711.79 8/17/2004 6.34 710.90 2/23/2005 5.64 711.60 8/16/2005 6.50 710.74 2/22/2006 5.85 711.39 8/16/2006 4.05 713.19 2/20/2007 5.78 711.46 8/15/2007 7.08 710.16 2/25/2008 6.20 711.04 8/27/2008 4.85 712.39 8/12/2010 6.18 711.06 9/8/2011 7.15 710.09 2/13/2012 6.14 711.1 8/3/2012 NM NM 2/4/2013 6.3 710.94 2/19/2014 5.06 712.18 8/25/2014 6.67 710.57 2/23/2015 5.96 711.28 8/18/2015 7.57 709.67 12/3/2015 5.10 712.14 2/16/2016 4.29 712.95 8/19/2016 6.71 710.53 2/7/2017 6.46 710.78 8/15/2017 7.00 710.24 2/1/2018 6.29 710.95 8/16/2018 6.32 710.92 M W-2 708.52 (MW-2D) 1/31/2001 3.40 705.12 2/7/2001 13.80 694.72 2/8/2001 13.50 695.02 2/9/2001 12.97 695.55 2/14/2001 13.25 695.27 2/21 /2001 13.72 694.80 7/23/2001 14.15 694.37 8/16/2001 14.30 694.22 8/20/2001 5.83 702.69 8/22/2001 9.20 699.32 2/27/2002 10.50 698.02 8/28/2002 10.60 697.92 2/18/2003 9.63 698.89 8/18/2003 6.68 701.84 2/19/2004 11.35 697.17 8/17/2004 4.70 703.82 2/23/2005 12.49 696.03 12/3/2015 3.58 704.94 Page 1 of 8 Table 2 Groundwater Elevation Summary Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well Number Date Depth to Water (ft.) Elevation of TOC (ft. MSL) Groundwater Elevation ft. MSL M W-3 716.64 1 /31 /2001 11.48 705.16 2/7/2001 11.86 704.78 2/8/2001 12.15 704.49 2/9/2001 12.48 704.16 2/14/2001 13.04 703.60 2/21 /2001 13.40 703.24 8/16/2001 13.30 703.34 2/27/2002 11.15 705.49 8/28/2002 13.95 702.69 2/18/2003 10.28 706.36 8/18/2003 9.17 707.47 2/19/2004 9.28 707.36 8/17/2004 10.61 706.03 2/23/2005 10.77 705.87 12/3/2015 9.33 707.31 M W-4 729.9 1 /31 /2001 15.57 714.33 2/7/2001 15.58 714.32 2/8/2001 15.51 714.39 2/9/2001 14.90 715.00 2/12/2001 14.07 715.83 2/14/2001 13.45 716.45 2/16/2001 12.80 717.10 2/21 /2001 7.00 722.90 2/27/2001 6.70 723.20 3/2/2001 6.85 723.05 3/9/2001 4.97 724.93 3/19/2001 5.02 724.88 3/26/2001 5.65 724.25 4/2/2001 5.00 724.90 4/9/2001 3.80 726.10 4/16/2001 5.00 724.90 4/23/2001 4.04 725.86 4/27/2001 3.65 726.25 5/1 /2001 4.35 725.55 5/21 /2001 5.33 724.57 6/13/2001 4.75 725.15 7/3/2001 3.64 726.26 7/19/2001 4.10 725.80 7/23/2001 3.58 726.32 7/30/2001 4.30 725.60 8/14/2001 3.55 726.35 8/16/2001 3.30 726.60 9/5/2001 4.62 725.28 9/11/2001 4.50 725.40 10/11/2001 5.20 724.70 11 /7/2001 5.62 724.28 11 /21 /2001 5.26 724.64 12/18/2001 3.35 726.55 12/27/2001 4.65 725.25 1/17/2002 6.16 723.74 2/26/2002 4.50 725.40 2/27/2002 4.75 725.15 3/14/2002 5.40 724.50 4/26/2002 6.75 723.15 5/10/2002 5.70 724.20 5/28/2002 3.80 726.10 6/19/2002 1 4.90 1 1 725.00 Page 2 of 8 Table 2 Groundwater Elevation Summary Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well Number Date Depth to Water (ft.) Elevation of TOC (ft. MSL) Groundwater Elevation ft. MSL MW-4 7/3/2002 5.85 724.05 continued 8/20/2002 5.80 724.10 8/28/2002 5.80 724.10 2/18/2003 4.38 725.52 3/17/2003 3.55 726.35 4/28/2003 3.80 726.10 5/19/2003 3.30 726.60 6/5/2003 3.75 726.15 7/7/2003 4.38 725.52 8/18/2003 4.73 725.17 9/5/2003 5.10 724.80 10/6/2003 4.70 725.20 11/21/2003 4.90 725.00 12/8/2003 4.30 725.60 1/29/2004 4.48 725.42 2/19/2004 4.50 725.40 3/9/2004 4.90 725.00 4/6/2004 4.00 725.90 5/7/2004 4.64 725.26 6/8/2004 4.66 725.24 7/22/2004 7.62 722.28 8/10/2004 7.15 722.75 8/17/2004 7.73 722.17 9/9/2004 6.40 723.50 2/23/2005 3.51 726.39 3/23/2005 6.95 722.95 4/11/2005 4.35 725.55 5/5/2005 3.94 725.96 6/23/2005 3.80 726.10 7/7/2005 3.90 726.00 8/16/2005 5.50 724.40 9/9/2005 5.40 724.50 10/18/2005 5.82 724.08 11/9/2005 6.70 723.20 12/20/2005 3.55 726.35 1/18/2006 4.33 725.57 2/22/2006 5.32 724.58 2/20/2007 5.54 724.36 8/15/2007 8.45 721.45 2/25/2008 4.46 725.44 8/27/2008 4.90 725.00 2/11/2009 8.66 721.24 8/20/2009 9.08 720.82 2/4/2010 6.06 723.84 8/12/2010 9.87 720.03 2/15/2011 11.73 718.17 9/8/2011 13.82 716.08 2/13/2012 10.76 719.14 8/3/2012 12.87 717.03 2/4/2013 13.12 716.78 2/19/2014 10.12 719.78 8/25/2014 11.03 718.87 2/23/2015 11.39 718.51 8/18/2015 13.96 715.94 12/3/2015 10.26 719.64 2/16/2016 8.46 721.44 8/19/2016 11.34 718.56 2/7/2017 12.01 717.89 8/15/2017 11.74 718.16 2/1 /2018 13.56 716.34 8/16/2018 12.2 717.7 Page 3 of 8 Table 2 Groundwater Elevation Summary Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well Number Date Depth to Water (ft.) Elevation of TOC (ft. MSL) Groundwater Elevation ft. MSL M W-5 726.87 2/23/2001 13.27 713.60 2/27/2002 10.35 716.52 2/18/2003 9.50 717.37 8/17/2004 9.85 717.02 2/23/2005 9.24 717.63 8/12/2010 10.32 716.55 9/8/2011 12.34 714.53 2/13/2012 10.97 715.9 8/3/2012 NM NM 2/4/2013 12.39 714.48 2/19/2014 10.76 716.11 8/25/2014 11.68 715.19 2/23/2015 11.41 715.46 8/18/2015 13.14 713.73 12/3/2015 10.02 716.85 2/16/2016 9.65 717.22 8/19/2016 11.22 715.65 2/7/2017 12.02 714.85 8/15/2017 11.94 714.93 2/1 /2018 12.76 714.11 8/16/2018 11.02 715.85 M W-6 724.61 1 /31 /2001 15.10 709.51 2/7/2001 15.18 709.43 2/8/2001 15.17 709.44 2/9/2001 15.18 709.43 2/14/2001 15.18 709.43 2/21 /2001 15.18 709.43 8/16/2001 15.52 709.09 2/27/2002 14.00 710.61 8/28/2002 30.45 694.16 2/18/2003 13.17 711.44 8/18/2003 11.62 712.99 2/19/2004 12.17 712.44 8/17/2004 12.98 711.63 2/23/2005 13.28 711.33 8/16/2005 12.97 711.64 2/22/2006 11.98 712.63 8/16/2006 12.55 712.06 2/20/2007 11.90 712.71 8/15/2007 14.23 710.38 2/25/2008 13.10 711.51 8/27/2008 12.78 711.83 2/11/2009 13.27 711.34 8/20/2009 13.86 710.75 2/4/2010 13.75 710.86 8/12/2010 12.15 712.46 2/15/2011 13.09 711.52 9/8/2011 DRY DRY 2/13/2012 12.42 712.19 8/3/2012 13.66 710.95 2/4/2013 13.61 711 2/19/2014 12.02 712.59 8/25/2014 13.31 711.3 2/23/2015 13.01 711.60 8/18/2015 14.50 710.11 12/3/2015 11.63 712.98 2/16/2016 11.24 713.37 8/19/2016 13.05 711.56 2/7/2017 13.35 711.26 8/15/2017 13.36 711.25 2/1 /2018 14.28 710.33 8/16/2018 12.93 711.68 Page 4 of 8 Table 2 Groundwater Elevation Summary Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well Number Date Depth to Water (ft.) Elevation of TOC (ft. MSL) Groundwater Elevation ft. MSL MW-7 725.52 (MW-6D) 1/31/2001 21.40 704.12 2/7/2001 30.48 695.04 2/8/2001 30.40 695.12 2/9/2001 29.23 696.29 2/14/2001 30.12 695.40 2/21 /2001 30.60 694.92 7/23/2001 31.02 694.50 8/16/2001 31.15 694.37 8/20/2001 22.75 702.77 8/22/2001 26.12 699.40 2/27/2002 27.40 698.12 8/28/2002 14.62 710.90 2/18/2003 26.50 699.02 8/18/2003 23.60 701.92 2/19/2004 28.17 697.35 8/17/2004 21.69 703.83 2/23/2005 29.37 696.15 8/16/2005 28.75 696.77 2/22/2006 25.10 700.42 8/16/2006 28.75 696.77 2/20/2007 26.68 698.84 8/15/2007 28.68 696.84 2/25/2008 13.10 712.42 8/27/2008 28.60 696.92 9/8/2011 23.76 701.76 2/13/2012 21.12 704.4 8/3/2012 NM NM 2/4/2013 21.69 703.83 8/18/2015 NM NM 12/3/2015 20.38 705.14 M W-8 710.26 1 /31 /2001 6.72 703.54 2/7/2001 6.80 703.46 2/8/2001 6.97 703.29 2/9/2001 7.08 703.18 2/14/2001 7.20 703.06 2/21 /2001 7.37 702.89 8/16/2001 7.75 702.51 2/27/2002 6.65 703.61 8/28/2002 8.60 701.66 2/18/2003 6.25 704.01 8/18/2003 6.13 704.13 2/19/2004 6.00 704.26 8/17/2004 6.36 703.90 2/23/2005 6.28 703.98 8/16/2005 6.55 703.71 2/22/2006 5.75 704.51 8/16/2006 7.08 703.18 2/20/2007 6.70 703.56 8/15/2007 15.80 694.46 2/25/2008 7.50 702.76 8/27/2008 10.30 699.96 2/11/2009 6.13 704.13 8/20/2009 7.90 702.36 2/4/2010 1 6.00 1 1 704.26 Page 5 of 8 Table 2 Groundwater Elevation Summary Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well Number Date Depth to Water (ft.) Elevation of TOC (ft. MSL) Groundwater Elevation ft. MSL MW-8 8/12/2010 6.52 703.74 continued 2/15/2011 6.69 703.57 9/8/2011 8.82 701.44 2/13/2012 6.23 704.03 8/3/2012 7.12 703.14 2/4/2013 6.72 703.54 2/19/2014 6.08 704.18 8/25/2014 4.67 705.59 2/23/2015 6.62 703.64 8/18/2015 7.87 702.39 12/3/2015 6.22 704.04 2/16/2016 5.82 704.44 8/19/2016 7.25 703.01 2/7/2017 6.48 703.78 8/15/2017 7.14 703.12 2/1/2018 6.44 703.82 8/16/2018 7.14 703.12 M W-13 707.35 1 /31 /2001 4.00 703.35 2/7/2001 4.63 702.72 2/8/2001 4.75 702.60 2/9/2001 4.75 702.60 2/14/2001 4.69 702.66 2/21 /2001 4.67 702.68 2/27/2002 4.85 702.50 8/28/2002 6.50 700.85 2/18/2003 4.66 702.69 8/18/2003 4.95 702.40 2/19/2004 4.15 703.20 8/17/2004 5.06 702.29 2/23/2005 4.25 703.10 8/16/2005 4.65 702.70 2/22/2006 4.02 703.33 8/16/2006 3.80 703.55 2/20/2007 4.30 703.05 8/15/2007 5.80 701.55 2/25/2008 3.90 703.45 8/27/2008 3.68 703.67 2/11/2009 4.30 703.05 8/20/2009 5.36 701.99 2/4/2010 3.87 703.48 8/12/2010 4.91 702.44 2/15/2011 3.98 703.37 9/8/2011 5.10 702.25 2/13/2012 4.12 703.23 8/3/2012 NM NM 2/4/2013 3.88 703.47 2/19/2014 3.86 703.49 8/25/2014 4.85 702.5 2/23/2015 4.65 702.70 8/18/2015 5.63 701.72 12/3/2015 3.55 703.80 2/16/2016 3.55 703.80 8/19/2016 4.99 702.36 2/7/2017 4.32 703.03 8/15/2017 4.71 702.64 2/1/2018 3.69 703.66 8/16/2018 4.6 702.75 Page 6 of 8 Table 2 Groundwater Elevation Summary Colonial Pipeline Company Kannapolis Booster Station Concord, NC Groundwater Depth to Water Elevation of TOC Well Number Date Elevation (ft.) (ft. MSL) ft. MSL MW-14 707.15 (MW-17) 1/31/2001 4.02 703.13 2/7/2001 4.20 702.95 2/8/2001 4.25 702.90 2/9/2001 4.18 702.97 2/14/2001 4.05 703.10 2/21 /2001 4.15 703.00 8/16/2001 4.80 702.35 2/27/2002 4.35 702.80 8/28/2002 6.10 701.05 2/18/2003 4.00 703.15 8/18/2003 4.25 702.90 2/19/2004 4.50 702.65 8/17/2004 4.55 702.60 2/23/2005 3.53 703.62 12/3/2015 3.51 703.64 M W-17 707.45 (MW-TR1U) 2/23/2001 4.45 703.00 8/16/2001 5.10 702.35 2/27/2002 4.15 703.30 8/28/2002 6.35 701.10 2/18/2003 4.35 703.10 2/19/2004 4.00 703.45 8/17/2004 4.71 702.74 2/23/2005 3.68 703.77 12/3/2015 3.51 703.94 MW-18 706.79 (MW-TR1D) 2/23/2001 3.88 702.91 8/16/2001 4.52 702.27 2/27/2002 4.10 702.69 8/28/2002 5.75 701.04 2/18/2003 3.75 703.04 2/19/2004 3.50 703.29 8/17/2004 4.12 702.67 2/23/2005 3.19 703.60 12/3/2015 3.32 703.47 MW-23 726.70 12/3/2015 7.72 718.98 2/16/2016 6.48 720.22 8/19/2016 8.82 717.88 2/7/2017 9.67 717.03 8/15/2017 9.49 717.21 2/1 /2018 11.11 715.59 8/16/2018 9.07 717.63 Page 7 of 8 Table 2 Groundwater Elevation Summary Colonial Pipeline Company Kannapolis Booster Station Concord, NC Groundwater Depth to Water Elevation of TOC Well Number Date Elevation (ft.) (ft. MSL) ft. MSL M W-24 724.61 12/3/2015 6.54 718.07 2/16/2016 6.16 718.45 8/19/2016 7.46 717.15 2/7/2017 8.49 716.12 8/15/2017 7.92 716.69 2/1/2018 9.07 715.54 8/16/2018 7.23 717.38 MW-25 724.32 12/3/2015 8.34 715.98 2/16/2016 8.11 716.21 8/19/2016 9.28 715.04 2/7/2017 10.60 713.72 8/15/2017 10.28 714.04 2/1/2018 10.61 713.71 8/16/2018 8.91 715.41 MW-25D 724.00 12/3/2015 19.70 704.30 2/16/2016 19.13 704.87 8/19/2016 22.77 701.23 2/7/2017 20.57 703.43 8/15/2017 22.04 701.96 2/1/2018 11.80 712.20 8/16/2018 21.63 702.37 Notes: TOC elevations obtained from ESP Associates survey (4/2001) and TWT survey (12/2015), with the exception of MW-15. Monitor well numbers modified January 2001. Former well designations in parenthesis. TOC - Top of casing ft. - Feet ft. MSL - Feet above mean sea level Page 8 of 8 Table 3 Recovery Well Gauging Data Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well Top of Casing Elevation (ft. MSL) Well Depth (ft. BLS) Date Depth to LNAPL (ft. TOC) Depth to Water (ft. TOC) LNAPL Thickness (ft.) Groundwater Elevation (ft. MSL) SB-1 NM 5.0 8/14/2015 2.67 4.03 1.36 8/15/2015 3.79 4.05 0.26 8/17/2015 3.60 4.10 0.50 8/18/2015 DRY SB-2 NM 5.0 8/14/2015 2.16 3.78 1.62 8/15/2015 3.22 4.00 0.78 8/17/2015 3.65 3.85 0.20 8/18/2015 DRY S113-3 NM 5.0 8/14/2015 0.99 4.03 3.04 8/15/2015 2.64 4.20 1.56 8/17/2015 3.99 4.20 0.21 8/18/2015 3.95 4.20 0.25 8/19/2015 DRY S113-4 722.57 13.55 8/15/2015 7.13 13.27 6.14 713.72 8/17/2015 7.51 13.26 5.75 713.45 8/18/2015 8.48 9.42 0.94 713.83 8/19/2015 8.70 9.40 0.70 713.67 8/20/2015 8.59 9.40 0.81 713.75 8/21 /2015 8.80 9.10 0.30 713.69 8/24/2015 8.50 8.58 0.08 714.05 8/27/2015 8.84 9.01 0.17 713.68 12/16/2015 7.03 7.05 0.02 715.53 2/16/2016 ND 3.45 NA 719.12 8/19/2016 ND 4.42 NA 718.15 2/7/2017 ND 5.91 NA 716.66 8/15/2017 ND 5.64 NA 716.93 2/1/2018 ND 5.33 NA 717.24 8/16/2018 ND 4.21 NA 718.36 SB-5 (converted to RW-oi) NM 11.43 8/15/2015 7.11 9.57 2.46 - 8/17/2015 7.49 9.65 2.16 8/18/2015 8.61 9.66 1.05 8/19/2015 8.92 10.92 2.00 - 8/20/2015 2.50 3.90 1.40 8/21 /2015 1.45 1.95 0.50 - SB-6 723.17 14.7 8/15/2015 8.68 10.05 1.37 714.11 8/17/2015 8.44 11.92 3.48 713.76 8/18/2015 8.88 10.04 1.16 713.97 8/19/2015 9.31 9.55 0.24 713.79 8/20/2015 5.64 8.50 2.86 716.73 8/21 /2015 9.04 10.06 1.02 713.84 8/24/2015 8.92 10.47 1.55 713.82 8/27/2015 9.34 9.60 0.26 713.76 12/16/2015 7.03 7.05 0.02 716.13 2/16/2016 ND 5.73 NA 717.44 8/19/2016 6.76 6.77 0.01 716.41 2/7/2017 ND 8.10 NA 715.07 8/15/2017 8.45 8.56 0.11 714.69 2/1/2018 8.01 8.02 0.01 715.16 8/16/2018 ND 6.32 NA 716.85 Page 1 of 5 Table 3 Recovery Well Gauging Data Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well Top of Casing Elevation (ft. MSL) Well Depth (ft. BLS) Date Depth to LNAPL (ft. TOC) Depth to Water (ft. TOC) LNAPL Thickness (ft.) Groundwater Elevation (ft. MSL) SB-7 723.33 9.35 8/15/2015 ND 7.50 NA 715.83 8/17/2015 7.68 7.72 0.04 715.64 8/18/2015 7.67 8.09 0.42 715.54 8/19/2015 8.23 8.24 0.01 715.10 8/20/2015 8.29 8.30 0.01 715.04 8/21/2015 ND 8.35 NA 714.98 8/24/2015 8.32 8.33 0.01 715.01 8/27/2015 ND 8.12 NA 715.21 12/16/2015 ND 6.05 NA 717.28 2/16/2016 ND 2.88 NA 720.45 8/19/2016 ND 3.32 NA 720.01 2/7/2017 ND 5.55 NA 717.78 Well Destroyed SB-8 722.60 12.76 8/17/2015 ND 8.41 NA 714.19 8/18/2015 ND 8.49 NA 714.11 8/19/2015 ND 8.70 NA 713.90 8/20/2015 ND 8.60 NA 714.00 8/21/2015 ND 8.62 NA 713.98 8/24/2015 ND 8.56 NA 714.04 8/27/2015 ND 8.75 NA 713.85 12/16/2015 ND 6.22 NA 716.38 2/16/2016 ND 4.70 NA 717.90 8/19/2016 ND 6.13 NA 716.47 2/7/2017 ND 6.89 NA 715.71 8/15/2017 ND 2.51 NA 720.09 2/1/2018 ND 3.60 NA 719.00 8/16/2018 ND 2.61 NA 719.99 SB-9 722.62 9.75 8/17/2015 7.45 9.75 2.30 714.53 8/18/2015 7.91 9.48 1.57 714.27 8/19/2015 8.41 9.48 1.07 713.91 8/20/2015 8.33 9.75 1.42 713.89 8/21/2015 8.43 9.47 1.04 713.90 8/24/2015 8.37 9.54 1.17 713.92 8/27/2015 8.46 9.45 0.99 713.88 12/16/2015 ND 5.96 NA 716.66 2/16/2016 ND 3.60 NA 719.02 8/19/2016 ND 4.28 NA 718.34 2/7/2017 ND 5.64 NA 716.98 8/15/2017 ND 5.34 NA 717.28 2/1/2018 ND 6.37 NA 716.25 8/16/2018 ND 3.94 NA 718.68 SB-10 724.35 15.35 8/17/2015 ND 10.53 NA 713.82 8/18/2015 ND 10.30 NA 714.05 8/19/2015 ND 10.45 NA 713.90 8/20/2015 ND 10.38 NA 713.97 8/21/2015 ND 10.40 NA 713.95 8/24/2015 ND 10.32 NA 714.03 8/27/2015 ND 10.50 NA 713.85 12/16/2015 ND 7.99 NA 716.36 2/16/2016 ND 6.49 NA 717.86 8/19/2016 ND 7.75 NA 716.60 2/7/2017 ND 8.73 NA 715.62 8/18/2017 ND 9.49 NA 714.86 2/1/2018 ND 9.13 NA 715.22 8/16/2018 ND 7.34 NA 717.01 Page 2 of 5 Table 3 Recovery Well Gauging Data Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well Top of Casing Elevation (ft. MSL) Well Depth (ft. BLS) Date Depth to LNAPL (ft. TOC) Depth to Water (ft. TOC) LNAPL Thickness (ft.) Groundwater Elevation (ft. MSL) SB-11 725.36 15.19 8/18/2015 ND 11.18 NA 714.18 8/19/2015 ND 11.30 NA 714.06 8/20/2015 ND 12.27 NA 713.09 8/21/2015 ND 11.35 NA 714.01 8/24/2015 ND 11.40 NA 713.96 8/27/2015 ND 11.55 NA 713.81 12/16/2015 ND 8.58 NA 716.78 2/16/2016 ND 6.29 NA 719.07 8/19/2016 ND 8.40 NA 716.96 2/7/2017 ND 8.90 NA 716.46 8/15/2017 ND 9.21 NA 716.15 2/1/2018 ND 9.58 NA 715.78 8/16/2018 ND 8.94 NA 716.42 SB-12 722.03 15.8 8/18/2015 ND 7.75 NA 714.28 8/19/2015 ND 7.88 NA 714.15 8/20/2015 ND 7.36 NA 714.67 8/21/2015 ND 7.86 NA 714.17 8/24/2015 ND 7.89 NA 714.14 8/27/2015 ND 9.13 NA 712.90 12/16/2015 ND 5.96 NA 716.07 2/16/2016 ND 4.83 NA 717.20 8/19/2016 ND 6.46 NA 715.57 2/7/2017 ND 6.77 NA 715.26 8/15/2017 ND 7.14 NA 714.89 2/1/2018 ND 7.08 NA 714.95 8/16/2018 ND 6.13 NA 715.9 SB-13 721.26 9 8/19/2015 7.29 8.53 1.24 713.62 8/20/2015 7.33 8.45 1.12 713.62 8/21/2015 7.58 8.65 1.07 713.38 8/24/2015 7.33 8.00 0.67 713.74 8/27/2015 7.45 8.55 1.10 713.50 12/16/2015 ND 5.30 NA 715.96 2/16/2016 ND 1.86 NA 719.40 8/19/2016 ND 3.10 NA 718.16 2/7/2017 ND 4.72 NA 716.54 Well Destroyed SB-14 721.69 18 8/19/2015 7.81 8.10 0.29 713.80 8/20/2015 7.65 8.90 1.25 713.69 8/21/2015 7.75 7.80 0.05 713.93 8/24/2015 7.86 8.28 0.42 713.71 8/27/2015 7.80 8.33 0.53 713.74 12/16/2015 ND 5.80 NA 715.89 2/16/2016 ND 3.23 NA 718.46 8/19/2016 4.48 4.65 0.17 717.16 2/7/2017 5.50 6.10 0.60 716.02 8/15/2017 ND 5.83 NA 715.86 2/1/2018 ND 5.41 NA 716.28 8/16/2018 ND 3.87 NA 717.82 Page 3 of 5 Table 3 Recovery Well Gauging Data Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well Top of Casing Elevation (ft. MSL) Well Depth (ft. BLS) Date Depth to LNAPL (ft. TOC) Depth to Water (ft. TOC) LNAPL Thickness (ft.) Groundwater Elevation (ft. MSL) SB-15 722.76 17.2 8/19/2015 8.64 10.28 1.64 713.66 8/20/2015 8.68 9.33 0.65 713.90 8/21/2015 8.78 8.90 0.12 713.95 8/24/2015 8.79 8.84 0.05 713.96 8/27/2015 ND 8.95 NA 713.81 12/16/2015 ND 6.46 NA 716.30 2/16/2016 ND 5.00 NA 717.76 8/19/2016 ND 6.41 NA 716.35 2/7/2017 ND 7.47 NA 715.29 8/15/2017 ND 7.88 NA 714.88 2/1/2018 ND 7.60 NA 715.16 8/16/2018 ND 5.85 NA 716.91 SB-16 722.88 12.5 8/20/2015 ND 8.90 NA 713.98 8/21/2015 ND 8.85 NA 714.03 8/24/2015 ND 8.80 NA 714.08 8/27/2015 ND 9.00 NA 713.88 12/16/2015 ND 6.47 NA 716.41 2/16/2016 ND 3.24 NA 719.64 8/19/2016 ND 5.21 NA 717.67 2/7/2017 ND 7.21 NA 715.67 8/15/2017 ND 7.76 NA 715.12 2/1/2018 ND 7.53 NA 715.35 8/16/2018 ND 5.48 NA 717.4 SB-17 722.88 13.8 8/20/2015 ND 8.95 NA 713.93 8/21/2015 ND 8.95 NA 713.93 8/24/2015 ND 8.88 NA 714.00 8/27/2015 ND 9.09 NA 713.79 12/16/2015 ND 6.90 NA 715.98 2/16/2016 ND 5.79 NA 717.09 8/19/2016 ND 6.80 NA 716.08 2/7/2017 7.57 7.58 0.01 715.31 Well Destroyed SB-18 721.87 15.8 8/21/2015 ND 8.45 NA 713.42 8/24/2015 ND 8.38 NA 713.49 8/27/2015 ND 8.68 NA 713.19 12/16/2015 5.50 8.83 3.33 715.44 2/16/2016 4.20 4.21 0.01 717.67 8/19/2016 6.10 6.35 0.25 715.70 2/7/2017 6.06 6.89 0.83 715.58 8/15/2017 ND 3.20 NA 718.67 2/1/2018 ND 3.12 NA 718.75 8/16/2018 ND 2.32 NA 719.55 Page 4 of 5 Table 3 Recovery Well Gauging Data Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well Top of Casing Elevation (ft. MSL) Well Depth (ft. BLS) Date Depth to LNAPL (ft. TOC) Depth to Water (ft. TOC) LNAPL Thickness (ft.) Groundwater Elevation (ft. MSL) SB-19 723.66 13.33 8/21 /2015 9.65 10.45 0.80 713.79 8/24/2015 9.67 10.06 0.39 713.88 8/27/2015 9.80 10.00 0.20 713.80 12/16/2015 7.52 7.57 0.05 716.13 2/16/2016 ND 4.42 NA 719.24 8/19/2016 5.80 5.95 0.15 717.82 2/7/2017 ND 7.43 NA 716.23 Well Destroyed RW-1 722.98 14.3 8/24/2015 9.03 9.91 0.88 713.70 8/27/2015 9.20 10.20 1.00 713.50 12/16/2015 ND 6.86 NA 716.12 2/16/2016 ND 4.11 NA 718.87 8/19/2016 ND 5.10 NA 717.88 2/7/2017 ND 7.50 NA 715.48 8/15/2017 ND 6.90 NA 716.08 2/1/2018 ND 8.22 NA 714.76 8/16/2018 ND 4.96 NA 718.02 RW-2 723.14 15 8/24/2015 ND 9.25 NA 713.89 8/27/2015 ND 9.45 NA 713.69 12/16/2015 ND 7.05 NA 716.09 2/16/2016 ND 5.25 NA 717.89 8/19/2016 ND 6.63 NA 716.51 2/7/2017 ND 7.97 NA 715.17 8/15/817 ND 8.06 NA 715.08 2/1/2018 ND 8.53 NA 714.61 8/16/2018 Well not located Notes: ft. - Feet ft. TOC - Feet below top of casing ft. BLS - Feet below ground surface ft. MSL - Feet above mean sea level LNAPL - Light non -aqueous phase liquid ND - None detected NA - Not applicable Corrected groundwater elevations calculated for wells with LNAPL detections (Corrected Groundwater Elevation = TOC - DTW + (Product Thickness x 0.72)) Page 5 of 5 Table 4 Groundwater Analytical Data Colonial Pipeline Company Kannapolis Booster Station Concord, NC Volatile Organic Compounds Method 6200B Semi Volatile Organic Compounds Method 625 MADEP-EPH/VPH L 4% t S Sample ID Sample Data � i X N •f0 •lC � lE i6 y � N O s s f0 £ O E O N ~ y Q Q Q Q 4) y y .. _ s y V lC N C L t d L t0 M 00 N Q O N N C CD N a7 T LU {0 O N LY R 2 ' U U 00 U U N U L _ y _ s M C t N v N O 3 C 7 r y mI W O HI T X N ._. L.1 Q C Q N m L 1 U M I LL LL L I d a. 1 U 01 U 01 U N 1 U 01 U U NCAC 2L Standard (ug/L) 1 600 600 500 20 80 2,000 0.05 1 5 3 300 300 200 200 10,000* 700* 400* 200* Surface Water Standard (ug/L) (WS-II, HQW) 1.19 68 (') 11 670 (Z) 19 (Z) 70_LL 300 (') 0.0028 0.32 (') 20 (') 50 (') NE 20 (') S 180 (S) (Z) 180 (S) (Z) 125 (S) (Z) NE NE MW-1 2/25/1998 ND ND ND ND 85 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/18/1998 ND ND ND ND 97 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/17/1999 ND ND ND ND 14 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/19/1999 ND ND ND ND 110 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/17/2000 ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2000 <1.0 <1.0 <1.0 <3.0 160 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2001 <1.0 <1.0 <1.0 <3.0 9.2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2001 <1.0 <1.0 <1.0 <3.0 58 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/27/2002 <1.0 <1.0 <1.0 <3.0 58 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/28/2002 <1.0 <1.0 <1.0 <1.0 17.8 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/18/2003 <1.0 <1.0 <1.0 <1.0 1.7 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/18/2003 <1.0 <1.0 <1.0 <3.0 40 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/19/2004 <1.0 <1.0 <1.0 <3.0 19 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/17/2004 <1.0 <1.0 <1.0 <3.0 <5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2005 <1.0 <1.0 <1.0 <3.0 6 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2005 <1.0 <1.0 <1.0 <3.0 16 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/22/2006 <1.0 <1.0 <1.0 <3.0 8.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2006 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/20/2007 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/15/2007 <1.0 <1.0 <1.0 <3.0 6.3 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/25/2008 <0.5 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/28/2008 <0.5 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 12/3/2015 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <2.0 <2.0 <2.0 <10 <2.0 <2.0 <2.0 <2.0 <100 <100 <75 <75 <25 <100 Page 1 of 9 Table 4 Groundwater Analytical Data Colonial Pipeline Company Kannapolis Booster Station Concord. NC Volatile Organic Compounds Method 6200B Semi Volatile Organic Compounds Method 625 MADEP-EPH/VPH L 4% t Sample ID Sample Data S d L - N •� U •M Q L % M •� V y m O a) a s s m E O E 0 O N O ~ O L � O O L_ � Q Q Q Q L Q L Q N O O O y y .O s Q V ce N C L C d C L C l0 M c0 N Q O N C d R L N N W a) U U U 00 U U N U N T L 3 d L m C V r N N N N O 7 O 7 O t y N m W O H T X N~ 2 Q C Q m t U s I LL LL d >, d 1 C) C) L0 U C) U U NCAC 2L Standard (ug/L) 1 600 600 500 20 80 2,000 0.05 5 3 300 300 200 200 10,000" 700' 400" 200' Surface Water Standard (ug/L) (WS-II, HQW) 1.19 68 (') 11 670 (2) 19 (2) 70 ' 300 (') 0.0028 0.32 (') 20 (') 50 (') NE 20 (') S 180 (S) (2) 180 (S) (2) 125 (S) (2) NE NE MW-2 10/20/1997 ND ND ND ND 2,100 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA (MW-2D) 2/25/1998 ND ND ND ND 3,500 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/18-19/98 ND ND ND ND 2,700 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/17/1999 ND ND ND ND 4,200 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/19/1999 ND ND ND ND 3,800 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 11/23/1999 ND ND ND ND 5,900 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/17/2000 ND ND ND ND 6,300 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2000 <1.0 1.1 <1.0 6.5 4,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 1/31/2001 <1.0 <1.0 <1.0 <3.0 1,400 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2001 <1.0 <1.0 <1.0 <3.0 430 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2001 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/27/2002 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/28/2002 <1.0 <1.0 <1.0 <1.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/18/2003 <1.0 <1.0 <1.0 <1.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/18/2003 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/19/2004 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/17/2004 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 12/3/2015 <1.0 <1.0 <1.0 <1.0 5.2 <2.0 <2.0 <2.0 <2.0 <10 <2.0 <2.0 <2.0 <2.0 <100 <100 <75 <75 <75 <100 MW-3 2/25/1998 ND ND ND ND 21 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/17/1999 ND ND ND ND 590 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/20/1999 ND ND ND ND 170 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/17/2000 ND ND ND ND 1,400 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2000 <1.0 <1.0 <1.0 <3.0 52 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2001 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2001 <1.0 <1.0 <1.0 <3.0 22 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/27/2002 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/28/2002 <1.0 <1.0 <1.0 <1.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/18/2003 <1.0 <1.0 <1.0 <1.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/18/2003 <1 <1 <1 <3 <5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/19/2004 <1 <1 <1 <3 <5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/17/2004 <1 <1 <1 <3 <5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2005 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 12/4/2015 <1.0 <1.0 <1.0 <1.0 0.83J <2.0 <2.0 <2.0 <2.0 <10 <2.0 <2.0 <2.0 <2.0 <100 <100 <75 <75 <25 <100 Page 2 of 9 Table 4 Groundwater Analytical Data Colonial Pipeline Company Kannapolis Booster Station Concord. NC Volatile Organic Compounds Method 6200B Semi Volatile Organic Compounds Method 625 MADEP-EPH/VPH L 4% t Sample ID Sample Data S d L - N •� U •M Q L % M •� V y m O a) a s s m E O E 0 O N O ~ O L � O O L_ � Q Q Q Q L Q L Q N O O O y y .O s Q V ce N C L C d C L C l0 M c0 N Q O N C d R L N N W a) U U U 00 U U N U N T L 3 d L m C V r N N N N O 7 O 7 O t y N m W O H T X N~ 2 Q C Q m t U s I LL LL d >, d 1 C) C) L0 U C) U U NCAC 2L Standard (ug/L) 1 600 600 500 20 80 2,000 0.05 5 3 300 300 200 200 10,000" 700' 400" 200' Surface Water Standard (ug/L) (WS-II, HQW) 1.19 68 (') 11 670 (2) 19 (2) 70 ' 300 (') 0.0028 0.32 (') 20 (') 50 (') NE 20 (') S 180 (S) (2) 180 (S) (2) 125 (S) (2) NE NE MW-4 1/31/2001 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2001 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2001 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/27/2002 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/28/2002 <1.0 <1.0 <1.0 <1.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/18/2003 <1.0 <1.0 <1.0 <1.0 15.7 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/18/2003 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/19/2004 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/17/2004 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2005 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2005 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/22/2006 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2006 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/20/2007 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/15/2007 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/25/2008 <0.5 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/27/2008 <0.5 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/11/2009 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/20/2009 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/4/2010 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/12/2010 <1.0 <1.0 <1.0 <3.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/15/2011 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 9/8/2011 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/13/2012 <1.0 <1.0 <1.0 <3.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/3/2012 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/4/2013 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/29/2013 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/19/2014 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/25/2014 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2015 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/18/2015 <0.5 <0.5 <0.5 <1.5 <0.5 <4.9 <4.9 <4.9 <4.9 <4.9 <4.9 <4.9 <4.9 <4.9 <200 <200 <100 <100 <100 <200 12/3/2015 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <2.0 <2.0 <2.0 <10 <2.0 <2.0 <2.0 <2.0 <100 <100 15J <75 <25 <100 2/16/2016 <0.5 <0.5 <0.5 <0.5 <0.5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/19/2016 <1.0 <1.0 <1.0 <3.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/7/2017 <1.0 <1.0 <1.0 <3.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/15/2017 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/1/2018 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2018 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA Page 3 of 9 Table 4 Groundwater Analytical Data Colonial Pipeline Company Kannapolis Booster Station Concord. NC Volatile Organic Compounds Method 6200B Semi Volatile Organic Compounds Method 625 MADEP-EPH/VPH L 4% t Sample ID Sample Data S d L - N •� U •M Q L % M •� V y m O a) a s s m E O E 0 O N O ~ O L � O O L_ � Q Q Q Q L Q L Q N O O O y y .O s Q V ce N C L C d C L C l0 M c0 N Q O N C d R L N N W a) U U U 00 U U N U N T L 3 d L m C V r N N N N O 7 O 7 O t y N m W O H T I X N~ 2 Q C Q m t U s I LL LL d >, d 1 C) C) L0 U C) U U NCAC 2L Standard (ug/L) 1 600 600 500 20 80 2,000 0.05 5 3 300 300 200 200 10,000" 700' 400" 200' Surface Water Standard (ug/L) (WS-II, HQW) 1.19 68 (') 11 670 (2) 19 (2) 70 ' 300 (') 0.0028 0.32 (') 20 (') 50 (') NE 20 (') S 180 (S) (2) 180 (S) (2) 125 (S) (2) NE NE MW-5 2/23/2005 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 12/3/2015 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <2.0 <2.0 <2.0 <10 <2.0 <2.0 <2.0 <2.0 <100 <100 <75 <75 <25 <100 MW-6 2/17/2000 2,000 1500 7,300 14,000 30,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2000 2,000 700 3,200 12,000 29,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2001 9 37 27 240 8,100 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/27/2002 160 27 32 570 2,600 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/28/2002 <20.0 <20.0 <20.0 <20.0 3,500 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/18/2003 354 <1.0 24.9 209 1,560 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/18/2003 22 <1.0 <1.0 <3.0 400 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/19/2004 260 13 4.6 4.4 410 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/17/2004 260 46 10 31 340 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2005 160 52 <10 <30 76 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2005 370 110 19 30 84 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/22/2006 110 47 <10 <30 120 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2006 240 33 9.8 J 17 58 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/20/2007 150 32 <10 <30 <50 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/15/2007 310 63 17 31 68 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/25/2008 130 37 4.5 14.9 95 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/28/2008 170 28 3.3 8.9 230 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/11/2009 13.2 <1.0 <1.0 <2.0 23 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/20/2009 73.7 5 1.4 <2.0 33.1 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/4/2010 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/12/2010 <1.0 <1.0 <1.0 <3.0 10.4 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/15/2011 6.5 <1.0 <1.0 <2.0 4.9 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 9/8/2011 NS NS NS NS NS NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/13/2012 3.6 <1.0 <1.0 <3.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/3/2012 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/4/2013 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/29/2013 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/19/2014 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/25/2014 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2015 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 12/3/2015 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <2.0 <2.0 <2.0 7.3,11 <2.0 <2.0 <2.0 <2.0 <100 <100 <75 10J <25 <100 2/16/2016 <0.5 <0.5 <0.5 <0.5 <0.5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/19/2016 <1.0 <1.0 <1.0 <3.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/7/2017 <1.0 <1.0 <1.0 <3.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/15/2017 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/1/2018 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2018 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA Page 4 of 9 Table 4 Groundwater Analytical Data Colonial Pipeline Company Kannapolis Booster Station Concord. NC Volatile Organic Compounds Method 6200B Semi Volatile Organic Compounds Method 625 MADEP-EPH/VPH L 4% t Sample ID Sample Data S d L - N •� U •M Q L % M •� V y m O a) a s s m E O E 0 O N O ~ O L � O O L_ � Q Q Q Q L Q L Q N O O O y y .O s Q V ce N C L C d C L C l0 M c0 N Q O N C d R L N N W a) U U U 00 U U N U N T L 3 d L m C V r N N N N O 7 O 7 O t y N m W O H T X N~ 2 Q C Q m t U s I LL LL d >, d 1 C) C) L0 U C) U U NCAC 2L Standard (ug/L) 1 600 600 500 20 80 2,000 0.05 5 3 300 300 200 200 10,000" 700' 400" 200' Surface Water Standard (ug/L) (WS-II, HQW) 1.19 68 (') 11 670 (2) 19 (2) 70 ' 300 (') 0.0028 0.32 (') 20 (') 50 (') NE 20 (') S 180 (S) (2) 180 (S) (2) 125 (S) (2) NE NE MW-7 10/25/1995 ND ND ND ND 57,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA (MW-6D) 12/12/95 ND ND ND ND 80,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 04/15/97 ND ND ND ND 40,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 07/16/97 ND ND ND ND 42,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 10/20/97 ND ND ND ND 43,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 11/9/1999 ND ND ND ND 25,900 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA (AFVR 11/9/99) 11/23/1999 ND ND ND ND 10,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 1/31/2001 <1.0 <1.0 <1.0 <3.0 17,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2001 <1.0 <1.0 <1.0 <3.0 22,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2001 4 <1.0 <1.0 <3.0 12,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/27/2002 7.1 <1.0 <1.0 <3.0 15,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/28/2002 <50.0 <50.0 <50.0 <50.0 4,120 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/18/2003 5.1 <1.0 <1.0 <1.0 2,890 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/18/2003 <1.0 <1.0 <1.0 <3.0 38 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/19/2004 6.5 <1.0 <1.0 <3.0 1,800 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/17/2004 <1 <1.0 <1.0 <3.0 2.7 J NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2005 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2005 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/22/2006 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2006 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/20/2007 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/15/2007 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/25/2008 <0.5 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/28/2008 <0.5 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 12/4/2015 <1.0 <1.0 <1.0 <1.0 2.8 <2.0 <2.0 <2.0 <2.0 <10 <2.0 <2.0 <2.0 <2.0 <100 <100 <75 12J <25 <100 Page 5 of 9 Table 4 Groundwater Analytical Data Colonial Pipeline Company Kannapolis Booster Station Concord. NC Volatile Organic Compounds Method 6200B Semi Volatile Organic Compounds Method 625 MADEP-EPH/VPH L 4% t Sample ID Sample Data S d L - N •� U •M Q L % M •� V y m O a) a s s m E O E 0 O N O ~ O L � O O L_ � Q Q Q Q L Q L Q N O O O y y .O s Q V ce N C L C d C L C l0 M c0 N Q O N C d R L N N W a) U U U 00 U U N U N T L 3 d L m C V r N N N N O 7 O 7 O t y N m W O H T X N~ 2 Q C Q m t U s I LL LL d >, d 1 C) C) L0 U C) U U NCAC 2L Standard (ug/L) 1 600 600 500 20 80 2,000 0.05 5 3 300 300 200 200 10,000" 700' 400" 200' Surface Water Standard (ug/L) (WS-II, HQW) 1.19 68 (') 11 670 (2) 19 (2) 70 ' 300 (') 0.0028 0.32 (') 20 (') 50 (') NE 20 (') S 180 (S) (2) 180 (S) (2) 125 (S) (2) NE NE MW-8 2/17/2000 ND ND ND ND 13,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2000 <1.0 <1.0 <1.0 <3.0 26,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2001 <1.0 <1.0 <1.0 <3.0 500 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2001 <1.0 <1.0 <1.0 <3.0 69 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/27/2002 <1.0 <1.0 <1.0 <3.0 680 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/28/2002 <1.0 <1.0 <1.0 <1.0 68.7 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/18/2003 <1.0 <1.0 <1.0 <1.0 2,200 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/18/2003 <1.0 <1.0 <1.0 <3.0 13,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/19/2004 <1.0 <1.0 <1.0 <3.0 80 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/17/2004 <1.0 <1.0 <1.0 <3.0 340 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2005 <10 <10 <10 <30 130 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2005 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/22/2006 <1.0 <1.0 <1.0 <3.0 9,600 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2006 <1.0 <1.0 <1.0 <3.0 860 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/20/2007 <1.0 <1.0 <1.0 <3.0 2,800 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/15/2007 <1.0 <1.0 <1.0 <3.0 1,600 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/25/2008 <0.5 <1.0 <1.0 <3.0 580 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/28/2008 <0.5 <1.0 <1.0 <3.0 640 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/11/2009 <1.0 <1.0 <1.0 <2.0 722 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/20/2009 <1.0 <1.0 <1.0 <2.0 475 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/4/2010 <1.0 <1.0 <1.0 <2.0 231 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/12/2010 <2.0 <2.0 <2.0 <6.0 215 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/15/2011 <1.0 <1.0 <1.0 <2.0 404 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 9/8/2011 <1.0 <1.0 <1.0 <2.0 37.9 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/13/2012 <1.0 <1.0 <1.0 <3.0 28.5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/3/2012 <1.0 <1.0 <1.0 <2.0 43.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/4/2013 <1.0 <1.0 <1.0 <2.0 27.1 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/29/2013 <1.0 <1.0 <1.0 <2.0 22.5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/19/2014 <1.0 <1.0 <1.0 <2.0 3.3 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/25/2014 <1.0 <1.0 <1.0 <2.0 27.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2015 <1.0 <1.0 <1.0 <2.0 24.4 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/18/2015 <0.5 <0.5 <0.5 <1.5 <0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <200 <200 <100 <100 <100 <200 12/4/2015 <1.0 <1.0 <1.0 <1.0 18 <2.0 <2.0 <2.0 <2.0 <10 <2.0 <2.0 <2.0 <2.0 <100 <100 <75 191 <25 <100 2/16/2016 <0.5 <0.5 <0.5 <0.5 16 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/19/2016 <1.0 <1.0 <1.0 <3.0 7.9 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/7/2017 <1.0 <1.0 <1.0 <3.0 9.7 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/15/2017 <0.50 <0.50 <0.50 <0.50 7.2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/1/2018 <0.50 <0.50 <0.50 <0.50 11 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2018 <0.50 <0.50 <0.50 <0.50 6.6 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA Page 6 of 9 Table 4 Groundwater Analytical Data Colonial Pipeline Company Kannapolis Booster Station Concord, NC Volatile Organic Compounds Method 6200B Semi Volatile Organic Compounds Method 625 MADEP-EPH/VPH L 4% t S Sample ID Sample Data X N •f0 •lC � lE i6 y N O s s f0 £ O E O N ~ y Q Q Q Q 4) y y .. _ s y V lC N C L t d L t0 M 00 N Q 00 O N N N C CD N a7 T LU M {0 C O N N LY R 2 r ' U U U U U L _ y _ s N t v N O 3 C 7 y mI W O H T I X L.1 C N m L U 1 M LL I LL L d I a. U 01 U 01 U N U 01 U U NCAC 2L Standard (ug/L) 1 600 600 500 20 80 2,000 0.05 5 3 300 300 200 200 10,000* 700* 400* 200* Surface Water Standard (ug/L) (WS-II, HQW) 1.19 68 (') 11 670 (Z) 19 (Z) 70 ' 300 (') 0.0028 0.32 (') 20 (') 50 (') NE 20 (') S 180 (S) (Z) 180 (S) (Z) 125 (S) (Z) NE NE MW-13 10/20/1997 ND ND ND ND 23,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/25/1998 190 ND ND ND 31,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/18-19/98 3 ND ND ND 4,300 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/17/1999 9 ND ND ND 10,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/19/1999 ND ND ND ND 530 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/17/2000 ND ND ND ND 1,200 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2000 1.8 <1.0 <1.0 <3.0 510 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2001 2.9 <1.0 <1.0 <3.0 410 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2001 5.2 <1.0 <1.0 <3.0 290 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/27/2002 1.2 <1.0 <1.0 <3.0 160 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/28/2002 3.3 <1.0 <1.0 <1.0 134 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/18/2003 <1.0 <1.0 <1.0 <1.0 1.1 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/18/2003 8.3 <1.0 <1.0 <3.0 45 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/19/2004 1.0 <1.0 <1.0 <3.0 3.8 J NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/17/2004 <1.0 <1.0 <1.0 <3.0 18 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2005 1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/17/2005 2.6 <1.0 <1.0 <3.0 5.4 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/22/2006 86 3.5 2.4 1.2 14.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2006 <1.0 <1.0 <1.0 <3.0 2.6 J NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/20/2007 3.5 <1.0 <1.0 <3.0 6.1 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/15/2007 31 <1.0 <1.0 <3.0 6.2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/25/2008 10 <1.0 <1.0 <3.0 2.9J NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/28/2008 7.6 <1.0 <1.0 <3.0 3.8J NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/11/2009 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/20/2009 5.7 <1.0 <1.0 <2.0 1.8 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/4/2010 2.1 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/12/2010 8.3 <1.0 <1.0 <3.0 3.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/15/2011 7.8 <1.0 <1.0 <2.0 6.8 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 9/8/2011 25.4 <1.0 <1.0 <2.0 1.4 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/13/2012 27.5 <1.0 <1.0 <3.0 3.1 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/3/2012 NS NS NS NS NS NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/4/2013 17.6 <1.0 <1.0 <2.0 2.4 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/29/2013 1.4 <1.0 <1.0 <2.0 1.4 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/19/2014 6.6 <1.0 <1.0 <2.0 3.8 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/25/2014 14.0 <1.0 <1.0 <2.0 4.5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2015 4.6 <1.0 <1.0 <2.0 5.1 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/18/2015 6.4 <0.5 <0.5 <1.5 1.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <200 <200 <100 53.9J <100 <200 12/4/2015 7.1 <1.0 <1.0 <1.0 9.0 <2.0 <2.0 <2.0 <2.0 <10 <2.0 <2.0 <2.0 <2.0 <100 <100 191 130 <25 <100 2/16/2016 32 1.3 0.85 1.00 5.3 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/19/2016 6.6 <1.0 <1.0 <3.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/7/2017 1.3 <1.0 <1.0 <3.0 3.5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/15/2017 0.69 <0.50 <0.50 <0.50 8.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/1/2018 1.9 <0.50 <0.50 <0.50 0.87 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2018 5.2 <0.50 <0.50 <0.50 2.5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA Page 7 of 9 Table 4 Groundwater Analytical Data Colonial Pipeline Company Kannapolis Booster Station Concord, NC Volatile Organic Compounds Method 6200B Semi Volatile Organic Compounds Method 625 MADEP-EPH/VPH L 4% t S Sample ID Sample Data X N •f0 •lC � lE 16 y N O s s f0 £ O E O N ~ y Q Q Q Q 4) y y .. _ s y V lC N C L t d L t0 M 00 N Q O N N C CD N a7 T LU {0 O N LY R 2 ' U U 00 U U N U L _ y _ s M C t N v N O 3 C 7 r y mI W O F- T I X N L.1 C N m L U 1 M LL I LL L d I a. U 01 U 01 U N U 01 U U NCAC 2L Standard (ug/L) 1 600 600 500 20 80 2,000 0.05 5 3 300 300 200 200 10,000* 700* 400* 200* Surface Water Standard (ug/L) (WS-II, HQW) 1.19 68 (') 11 670 (Z) 19 (Z) 70 ' 300 (') 0.0028 0.32 (') 20 (') 50 (') NE 20 (') S 180 (S) (Z) 180 (S) (Z) 125 (S) (Z) NE NE MW-17 8/18/1998 38 ND ND ND 3,500 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA (MW-TR1U) 2/17/1999 57 ND ND ND 2,400 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/19/1999 23 ND ND ND 370 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/17/2000 86 18 6 ND 170 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2000 50 7.9 2.2 <3.0 100 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2001 21 1.9 1.6 <3.0 21 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2001 16 1.4 <1.0 <3.0 20 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/27/2002 11 <1.0 <1.0 <3.0 12 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 12/4/2015 <1.0 <1.0 <1.0 <1.0 0.55J <2.0 <2.0 <2.0 <2.0 <10 <2.0 <2.0 <2.0 <2.0 <100 110 <75 71 J <25 <100 MW-18 8/18-19/98 ND ND ND ND 240 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA (MW-TR1D) 2/17/1999 ND ND ND ND 70 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/19/1999 ND ND ND ND 20 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/17/2000 ND ND ND ND 5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2000 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2001 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2001 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/27/2002 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 12/4/2015 <1.0 <1.0 <1.0 <1.0 0.43J <2.0 <2.0 <2.0 <2.0 <10 <2.0 <2.0 <2.0 <2.0 <100 <100 <75 <75 <25 <100 MW-23 12/3/2015 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <2.0 <2.0 <2.0 <10 <2.0 <2.0 <2.0 <2.0 <100 140 <75 <75 <25 <100 MW-24 12/4/2015 1.01 14 <5.0 <5.0 <5.0 14 4.3J 1.9J 1.2J <50 9.3J 2.8J 7.4J 7.3J <100 160 640 1,100 750 410 2/16/2016 8.7 8.7 2.0 J 3.9 <2.5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/19/2016 4.2 4.1 1.4 <3.0 NA 10.2 4.9J <0.33 <0.21 <0.79 11.5 2.1J 8.7 6.3 <100 <100 393 2,050 730 276 2/7/2017 4.7 4.8 1.3 <3.0 NA 9.2 4.8J 1.OJ <0.21 <0.79 10.6 1.5J 7.3 6.6 <100 101 564 1,520 783 244 8/15/2017 1.4 3.9 0.53 0.88 NA 4.8J 1.9J 0.77J 0.29J <8.0 6.8J <8.0 1.5J 5.5J <120 <120 340 660 280 180 2/1/2018 t 1.7 1.8 0.63 0.75 NA 8.6J 2.4J <16 <16 <16 8.9J <16 <16 7.1J <100 <100 280 620 280 160 8/16/2018 2.0 1.8 0.64 1.2 NA 5.7J 2.2J <16 <16 <16 4.1 J <16 2.1 J 3.1 J <100 <100 410 740 330 130 MW-25 12/4/2015 <1.0 <1.0 <1.0 <1.0 1.1 <2.0 <2.0 <2.0 <2.0 <10 <2.0 <2.0 <2.0 <2.0 <100 <100 <75 <75 <25 <100 2/16/2016 <0.5 <0.5 <0.5 <0.5 1.1 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/19/2016 <1.0 <1.0 <1.0 <3.0 NA <0.25 <0.14 <0.33 <0.21 <0.79 <0.21 <0.21 <0.22 <0.19 <100 <100 <50.0 <50.0 <50.0 <100 2/7/2017 <1.0 <1.0 <1.0 <3.0 NA <0.25 <0.14 <0.33 <0.21 <0.79 <0.21 <0.21 <0.22 <0.19 <100 <100 <50.0 <50.0 <50.0 <100 8/15/2017 0.61 <0.50 <0.50 <0.50 NA <1.6 <1.6 <1.6 <1.6 <1.6 <1.6 <1.6 <1.6 0.62J <110 <110 <75 <75 <25 <110 2/1/2018 <0.50 <0.50 <0.50 <0.50 NA <8.0 <8.0 <8.0 <8.0 <8.0 <8.0 <8.0 <8.0 0.68J <100 <100 <75 <75 <25 <100 8/16/2018 <0.50 <0.50 <0.50 <0.50 NA <8.0 <8.0 <8.0 <8.0 <8.0 <8.0 <8.0 <8.0 0.51 J <100 <100 <75 <75 <25 <100 MW-25D 12/4/2015 <1.0 <1.0 <1.0 <1.0 1.2 <2.0 <2.0 <2.0 <2.0 <10 <2.0 <2.0 <2.0 <2.0 <100 100 <75 <75 <25 <100 2/16/2016 <0.5 <0.5 <0.5 <0.5 1.3 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/19/2016 <1.0 <1.0 <1.0 <3.0 NA <0.25 <0.14 <0.33 <0.21 <0.79 <0.21 <0.21 <0.22 <0.19 <100 <100 <50.0 <50.0 <50.0 <100 2/7/2017 <1.0 <1.0 <1.0 <3.0 NA <0.25 <0.14 <0.33 <0.21 <0.79 <0.21 <0.21 <0.22 <0.19 <100 <100 <50.0 <50.0 <50.0 <100 8/15/2017 <0.50 <0.50 <0.50 <0.50 <0.50 <1.6 <1.6 <1.6 <1.6 <1.6 <1.6 <1.6 <1.6 <1.6 <100 <100 <75 <75 <25 <100 2/1/2018 t <0.50 <0.50 <0.50 <0.50 <0.50 <1.6 <1.6 <1.6 <1.6 0.75J <1.6 <1.6 <1.6 <1.6 <100 <100 <75 <75 <25 <100 8/16/2018 <0.50 <0.50 <0.50 <0.50 NA <1.6 <1.6 <1.6 <1.6 <8.0 <1.6 <1.6 <1.6 <1.6 <100 <100 <75 <75 <25 <100 Page 8 of 9 Table 4 Groundwater Analytical Data Colonial Pipeline Company Kannapolis Booster Station Concord, NC Volatile Organic Compounds Method 6200B Semi Volatile Organic Compounds Method 625 MADEP-EPH/VPH L 4% t S Sample ID Sample Data y X N N O •f0 s •lC s � f0 lE £ i6 E C O 16 C � � r � N t N � � _ Q �- �- L O. O L O L N 4) ~ y L y N L t d L t0 Q Q Q Q Q N y C y N .. _ T W {0 V lC O C N W R 2 M 00 N 00 O N N CD a7 y s m C t N v O C r ' U U U U U y L _ O _ T N <.1 C N L 23 7 L 01 01 N 01 m W HI X m U LL LL d a- U U U U U U NCAC 2L Standard (ug/L) 1 600 600 500 20 80 2,000 0.05 5 3 300 300 200 200 10,000* 700* 400* 200* Surface Water Standard (ug/L) (WS-II, HQW) 1.19 68 (') 11 1 670 (Z) 19 (Z) 1 70 ') 1300(1)1 0.0028 10.32(1)1 20 (') 1 50 (') 1 NE 1 20 (') 1 S I 180 (S) (Z) I 180 (S) (Z) 125 (S) (Z) NE I NE Quality Assurance / Qualit Control Samples Dup-1 (MW-4) 8/18/2015 <0.5 <0.5 <0.5 <1.5 <0.5 <4.8 <4.8 <4.8 <4.8 <4.8 <4.8 <4.8 <4.8 <4.8 <190 <190 <100 <100 <100 <190 Dup120415 (MW-25D) 12/4/2015 <1.0 <1.0 <1.0 <1.0 1.1 <2.0 <2.0 <2.0 <2.0 <10 <2.0 <2.0 <2.0 <2.0 <100 <100 <75 <75 <25 <100 Dup12032015 (MW-2) 12/3/2015 <1.0 <1.0 <1.0 <1.0 5.2 <2.0 <2.0 <2.0 <2.0 <10 <2.0 <2.0 <2.0 <2.0 <100 100 <75 <75 <25 <100 KSDUP (MW-24) 2/16/2016 7.7 12 2.1 J 3.8 <2.5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA DUP081916 (MW-8) 8/19/2016 <1.0 <1.0 <1.0 <3.0 7.2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA DUP020717 (MW-8) 2/7/2017 <1.0 <1.0 <1.0 <3.0 9.5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA DUP08152017(MW-13) 8/15/2017 0.75 <0.50 <0.50 <0.50 7.9 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA DUP-1 (MW-8) 2/1/2018 <0.50 <0.50 <0.50 <0.50 9.7 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA DUP-1(MW-24) 8/16/2018 1.8 1.9 0.61 1.1 <0.50 5.9J 2.1J <16 <16 <80 3.7J <16 1.9J 28J <100 <100 340 700 360 110 Notes: All concentrations reported in micrograms per liter (pg/L) MADEP = Massachusetts Department of Environmental Protection EPH = Extractable Petroleum Hydrocarbons VPH = Volatile Petroleum Hydrocarbons WS-II = Water Supply Class II HQW = High Quality Waters NE = No standard established NA = Not analyzed ND = Not detected Bold = Detection exceeds North Carolina Administrative Code (NCAC) 2L Groundwater Standard Gray fill indicates detection above the applicable Surface Water Standards (Indicated with superscript numerals 1 and 2) No superscript numeral indicates the NCAC 213 Surface Water Standard for Water Supply (WS) II, High Quality Waters (HQW) classification (') = Environmental Protection Agency Nationally Recommended Water Quality Criteria for Aquatic Life and Human Health. (2) = North Carolina Protective Values for Surface Waters = Analyte was not detected at or above the reporting limit shown. Final and interim groundwater quality standards "J" = Estimated concentration between the method detection limit and the reporting limit. "S" = Solubility exceeds toxicity; therefore, standard is met if no sheen is present on water surface or shoreline t = Additional analytes were detected in these wells during the sampling event flagged: MW-24: Benzo(a)pyrene at an estimated concentration of 1.0 pg/L which is above the 2L Standard of 0.005 pg/L and 2B Standard of 0.0028 pg/L for Total PAHs combined. MW-25D: Di-n-butyl phthalate at an estimated concentration of 0.44 pg/L which is below the 2L Standard of 700 pg/L and the 2B Standard of 20 pg/L. Monitor Well naming convention was modified January 2001. Former well designation in parentheses. Page 9 of 9 Table 5 Summary of Water Quality Data for Residential Wells Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well ID Date Benzene pg/I Ethylbenzene pg/I Toluene pg/I Xylenes pg/I MTBE pg/I Naphthalene pg/I 2L Groundwater Quality Standard 1 600 600 500 20 6 DW-Allen 12/20/1999 <1.0 <1.0 <1.0 <3.0 <5.0 - 4/10/2000 <1.0 <1.0 <1.0 <3.0 <5.0 6/15/2000 <1.0 I <1.0 <1.0 <3.0 <5.0 9/28/2000 <1.0 <1.0 <1.0 <3.0 <5.0 12/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 3/30/2001 <1.0 <1.0 <1.0 <3.0 <5.0 6/22/2001 <1.0 <1.0 <1.0 <3.0 <5.0 7/10/2002 <1.0 <1.0 <1.0 <1.0 <5.0 DW-6/15/2000 Church Bethpage- Chu 11/23/1999 <1.0 <1.0 <1.0 <3.0 <5.0 2/16/2000 <1.0 <1.0 <1.0 <3.0 <5.0 4/26/2000 <1.0 <1.0 <1.0 <3.0 <5.0 5/25/2000 <1.0 <1.0 <1.0 <3.0 <5.0 <1.0 <1.0 <1.0 <3.0 <5.0 8/16/2000 <1.0 <1.0 <1.0 <3.0 <5.0 12/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 3/30/2001 <1.0 <1.0 <1.0 <3.0 <5.0 6/21/2001 <1.0 <1.0 <1.0 <3.0 <5.0 7/10/2002 <1.0 <1.0 <1.0 <1.0 <5.0 8/29/2005 <1.0 <1.0 <1.0 <1.0 <5.0 DW-Boan 5/8/2000 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Brasington 3/27/2000 <1.0 <1.0 <1.0 <3.0 <5.0 9/28/2000 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Brooks 6/27/2000 <2.0 <2.0 <2.0 <4.0 <2.0 DW-Buchanan 9/11/2014 <0.5 <0.5 8.6 <3.0 <5.0 - 8/27/2015 <0.5 <0.5 <0.5 <3.0 <5.0 <1.0 8/29/2016 <0.5 <0.5 <0.5 <3.0 <5.0 <1.0 DW-Cain 2/16/2000 <1.0 <1.0 <1.0 <3.0 <5.0 - 6/15/2000 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Cain-Influent 7/18/2000 <1.0 <1.0 <1.0 <3.0 <5.0 8/16/2000 <1.0 <1.0 <1.0 <3.0 <5.0 9/28/2000 <1.0 <1.0 <1.0 <3.0 <5.0 11/14/2000 <1.0 <1.0 <1.0 <3.0 <5.0 12/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 1/18/2001 <1.0 <1.0 <1.0 <3.0 <5.0 2/23/2001 <1.0 <1.0 <1.0 <3.0 <5.0 3/30/2001 <1.0 <1.0 <1.0 <3.0 <5.0 5/1/2001 <1.0 <1.0 <1.0 <3.0 <5.0 6/21/2001 <1.0 <1.0 <1.0 <3.0 <5.0 8/16/2001 <1.0 <1.0 <1.0 <3.0 <5.0 10/24/2001 <1.0 <1.0 <1.0 <3.0 <5.0 3/1/2002 <1.0 <1.0 <1.0 <3.0 <5.0 5/14/2002 <1.0 <1.0 <1.0 <1.0 <5.0 7/10/2002 <1.0 <1.0 <1.0 <1.0 <5.0 11/6/2002 <1.0 <1.0 <1.0 <1.0 <5.0 3/11/2003 <1.0 <1.0 <1.0 <3.0 <5.0 3/9/2005 <1.0 <1.0 <1.0 <3.0 <5.0 9/28/2006 <1.0 <1.0 <1.0 <3.0 <5.0 8/25/2014 <0.5 <0.5 <0.5 <3.0 <5.0 8/27/2015 <0.5 <0.5 <0.5 <3.0 <5.0 - 8/27/2015 <0.5 <0.5 <0.5 <3.0 <5.0 <1.0 8/29/2016 <0.5 <0.5 <0.5 <3.0 <5.0 <1.0 Page 1 of 14 Table 5 Summary of Water Quality Data for Residential Wells Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well ID Date Benzene pg/I Ethylbenzene pg/I Toluene pg/I Xylenes pg/I MTBE pg/I Naphthalene pg/I 2L Groundwater Quality Standard 1 600 600 500 20 6 DW-Cain-Effluent 8/27/2015 <0.5 <0.5 <0.5 <3.0 <5.0 <1.0 DW-Cheeseman 6/27/2000 <2.0 <2.0 <2.0 <4.0 <2.0 - 9/28/2000 <1.0 I <1.0 <1.0 <3.0 1 <5.0 DW-Childers 2/16/2000 <1.0 <1.0 <1.0 <3.0 <5.0 7/31/2000 <1.0 <1.0 <1.0 <3.0 <5.0 9/28/2000 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Childers- Influent 11/14/2000 <1.0 <1.0 <1.0 <3.0 <5.0 12/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 1/18/2001 <1.0 <1.0 <1.0 <3.0 <5.0 2/23/2001 <1.0 <1.0 <1.0 <3.0 <5.0 3/30/2001 <1.0 <1.0 <1.0 <3.0 <5.0 5/1/2001 <1.0 <1.0 <1.0 <3.0 <5.0 6/21/2001 <1.0 <1.0 <1.0 <3.0 <5.0 8/16/2001 <1.0 <1.0 <1.0 <3.0 <5.0 10/24/2001 <1.0 <1.0 <1.0 <3.0 <5.0 3/1/2002 <1.0 <1.0 <1.0 <3.0 <5.0 5/14/2002 <1.0 <1.0 <1.0 <1.0 <5.0 7/10/2002 <1.0 <1.0 <1.0 <1.0 <5.0 11/6/2002 <1.0 <1.0 <1.0 <1.0 <5.0 3/11/2003 <1.0 <1.0 <1.0 <3.0 <5.0 3/9/2005 <1.0 <1.0 <1.0 <3.0 <5.0 9/28/2006 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Clark 11/23/1999 <1.0 <1.0 <1.0 <3.0 <5.0 3/27/2000 <1.0 <1.0 <1.0 <3.0 <5.0 6/15/2000 <1.0 <1.0 <1.0 <3.0 <5.0 9/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 12/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 3/30/2001 <1.0 <1.0 <1.0 <3.0 <5.0 6/21/2001 <1.0 <1.0 <1.0 <3.0 <5.0 3/14/2002 <1.0 <1.0 <1.0 <3.0 <5.0 8/22/2017 Not Sampled - Could not contact owner DW-Cook 11/23/1999 <1.0 <1.0 <1.0 <3.0 <5.0 3/27/2000 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Cook-Effluent 6/15/2000 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Cook- Influent 6/15/2000 <1.0 <1.0 <1.0 <3.0 <5.0 9/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 12/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 3/30/2001 <1.0 <1.0 <1.0 <3.0 <5.0 6/21/2001 <1.0 <1.0 <1.0 <3.0 <5.0 10/24/2001 <1.0 <1.0 <1.0 <3.0 <5.0 7/10/2002 <1.0 <1.0 <1.0 <1.0 <5.0 3/11/2003 <1.0 <1.0 <1.0 <3.0 <5.0 8/29/2005 <1.0 <1.0 <1.0 <3.0 <5.0 9/28/2006 <1.0 <1.0 <1.0 <3.0 <5.0 5/21/2009 <1.0 <1.0 <1.0 <3.0 <5.0 5/24/2011 <0.5 <1.0 <1.0 <3.0 <5.0 5/17/2012 <1.0 <1.0 <1.0 <3.0 <5.0 8/22/2017 <0.50 <0.50 <0.50 <3.0 <5.0 <1.0 8/23/2018 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 DW-Coren 11/23/1999 <1.0 <1.0 <1.0 <3.0 <5.0 - 3/27/2000 <1.0 <1.0 <1.0 <3.0 <5.0 6/15/2000 <1.0 <1.0 <1.0 <3.0 <5.0 Page 2 of 14 Table 5 Summary of Water Quality Data for Residential Wells Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well ID Date Benzene pg/I Ethylbenzene pg/I Toluene pg/I Xylenes pg/I MTBE pg/I Naphthalene pg/I 2L Groundwater Quality Standard 1 600 600 500 20 6 DW-Coren- Influent 9/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 - 12/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 3/30/2001 <1.0 I <1.0 <1.0 <3.0 1 <5.0 6/21/2001 <1.0 <1.0 <1.0 <3.0 <5.0 10/24/2001 <1.0 <1.0 <1.0 <3.0 <5.0 7/10/2002 <1.0 <1.0 <1.0 <1.0 <5.0 3/11/2003 <1.0 <1.0 <1.0 <3.0 <5.0 3/9/2005 <1.0 <1.0 <1.0 <3.0 <5.0 5/21/2009 <1.0 <1.0 <1.0 <3.0 <5.0 5/17/2012 <1.0 <1.0 <1.0 <3.0 <5.0 - 8/22/2017 <0.50 <0.50 1.3 <3.0 <5.0 <1.0 8/23/2018 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 DW-Crainshaw 12/7/1999 <1.0 <1.0 <1.0 <3.0 <5.0 - 3/27/2000 <1.0 <1.0 <1.0 <3.0 <5.0 6/15/2000 <1.0 <1.0 <1.0 <3.0 <5.0 9/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 12/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 3/30/2001 <1.0 <1.0 <1.0 <3.0 <5.0 6/22/2001 <1.0 <1.0 <1.0 <3.0 <5.0 7/10/2002 <1.0 <1.0 <1.0 <1.0 <5.0 DW-Crowe (MW-16)(1) 11/9/1999 <1.0 <1.0 <1.0 <3.0 116 11/19/1999 <1.0 <1.0 <1.0 <3.0 990 1/6/2000 <1.0 <1.0 <1.0 <3.0 600 8/16/2000 <1.0 <1.0 <1.0 <3.0 200 2/6/2001 <1.0 <1.0 <1.0 <3.0 69 3/1/2001 <1.0 <1.0 <1.0 <3.0 42 8/16/2001 <1.0 <1.0 <1.0 <3.0 19 2/27/2002 <1.0 <1.0 <1.0 <3.0 5 8/28/2002 <1.0 <1.0 <1.0 <1.0 <1.0 2/18/2003 <1.0 <1.0 <1.0 <1.0 <1.0 8/18/2003 <1.0 <1.0 <1.0 <3.0 1 <5.0 2/19/2004 <1.0 <1.0 <1.0 <3.0 <5.0 8/17/2004 <1.0 <1.0 <1.0 <3.0 <5.0 2/23/2005 <1.0 <1.0 <1.0 <3.0 <5.0 8/17/2005 <1.0 <1.0 <1.0 <3.0 <5.0 2/22/2006 <1.0 <1.0 <1.0 <3.0 <5.0 5/21/2009 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Daughtery 12/20/1999 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Deaton 12/20/1999 <1.0 <1.0 <1.0 <3.0 <5.0 3/27/2000 <1.0 <1.0 <1.0 <3.0 <5.0 6/15/2000 <1.0 <1.0 <1.0 <3.0 <5.0 9/28/2000 <1.0 <1.0 <1.0 <3.0 <5.0 12/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 3/30/2001 <1.0 <1.0 <1.0 <3.0 <5.0 6/22/2001 <1.0 <1.0 <1.0 <3.0 <5.0 7/10/2002 <1.0 <1.0 <1.0 <1.0 <5.0 - DW-Ellis 8/27/2015 <0.5 <0.5 2.0 <3.0 <5.0 <1.0 DW-Elwood 1/18/2000 <1.0 <1.0 <1.0 <3.0 <5.0 - 9/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 12/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 3/30/2001 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Elwood-D 5/7/2001 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Elwood 6/21/2001 <1.0 <1.0 <1.0 <3.0 <5.0 7/10/2002 <1.0 <1.0 <1.0 <1.0 <5.0 9/28/2006 <1.0 <1.0 <1.0 <3.0 <5.0 Page 3 of 14 Table 5 Summary of Water Quality Data for Residential Wells Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well ID Date Benzene pg/I Ethylbenzene pg/I Toluene pg/I Xylenes pg/I MTBE pg/I Naphthalene pg/I 2L Groundwater Quality Standard 1 600 600 500 20 6 DW-Emerson 11/23/1999 <1.0 <1.0 <1.0 <3.0 <5.0 - 12/27/1999 <1.0 <1.0 <1.0 <3.0 <5.0 3/27/2000 <1.0 <1.0 <1.0 <3.0 <5.0 4/26/2000 <1.0 <1.0 <1.0 <3.0 <5.0 5/25/2000 <1.0 <1.0 <1.0 <3.0 <5.0 6/15/2000 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Emerson- Effluent 7/18/2000 <1.0 <1.0 <1.0 <3.0 <5.0 3/14/2002 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Emerson- Influent 7/18/2000 <1.0 <1.0 <1.0 <3.0 <5.0 8/16/2000 <1.0 <1.0 <1.0 <3.0 <5.0 9/28/2000 <1.0 <1.0 <1.0 <3.0 <5.0 11/14/2000 <1.0 <1.0 <1.0 <3.0 <5.0 12/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 1/18/2001 <1.0 <1.0 <1.0 <3.0 <5.0 2/23/2001 <1.0 <1.0 <1.0 <3.0 <5.0 3/30/2001 <1.0 <1.0 <1.0 <3.0 <5.0 5/1/2001 <1.0 <1.0 <1.0 <3.0 <5.0 6/21/2001 <1.0 <1.0 <1.0 <3.0 <5.0 8/16/2001 <1.0 <1.0 <1.0 <3.0 <5.0 10/24/2001 <1.0 <1.0 <1.0 <3.0 <5.0 2/27/2002 <1.0 <1.0 <1.0 <3.0 <5.0 3/14/2002 <1.0 <1.0 <1.0 <3.0 <5.0 5/14/2002 <1.0 <1.0 <1.0 <1.0 <5.0 7/10/2002 <1.0 <1.0 <1.0 <1.0 <5.0 11/6/2002 <1.0 <1.0 <1.0 <1.0 <5.0 3/11/2003 <1.0 <1.0 <1.0 <3.0 <5.0 7/17/2003 <1.0 <1.0 <1.0 <3.0 <5.0 3/9/2005 <1.0 <1.0 <1.0 <3.0 <5.0 8/29/2005 <1.0 <1.0 <1.0 <3.0 <5.0 9/28/2006 <1.0 <1.0 <1.0 <3.0 <5.0 9/11/2014 <0.5 <0.5 <0.5 <3.0 <5.0 - 8/22/2017 <0.50 <0.50 <0.50 <3.0 <5.0 <1.0 DW-Gaultney 7/18/2000 <1.0 <1.0 <1.0 <3.0 <5.0 - DW-3/29/2000 New New <1.0 <1.0 <1.0 <3.0 72.4 4/17/2000 <1.0 <1.0 <1.0 <3.0 32 7/6/2000 <1.0 <1.0 2.2 <3.0 <5.0 DW-Goodnight- New-CV-1 7/18/2000 <1.0 <1.0 <1.0 <3.0 <5.0 8/16/2000 <1.0 <1.0 <1.0 <3.0 <5.0 9/28/2000 <1.0 <1.0 <1.0 <3.0 1 <5.0 11/14/2000 <1.0 <1.0 <1.0 <3.0 <5.0 1/18/2001 <1.0 <1.0 <1.0 <3.0 <5.0 6/21/2001 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Goodnight- New-CV-2 7/18/2000 <1.0 <1.0 <1.0 <3.0 <5.0 8/16/2000 <1.0 <1.0 <1.0 <3.0 <5.0 9/28/2000 <1.0 <1.0 <1.0 <3.0 <5.0 11/14/2000 <1.0 <1.0 <1.0 <3.0 <5.0 1/18/2001 <1.0 <1.0 <1.0 <3.0 <5.0 6/21/2001 <1.0 <1.0 <1.0 <3.0 <5.0 - 8/27/2015 <1.0 <1.0 <1.0 <3.0 <5.0 <1.0 8/29/2015 <1.0 <1.0 <1.0 <3.0 <5.0 <1.0 8/29/2016 1 <0.50 <0.50 <0.50 <3.0 <5.0 <1.0 Page 4 of 14 Table 5 Summary of Water Quality Data for Residential Wells Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well ID Date Benzene pg/I Ethylbenzene pg/I Toluene pg/I Xylenes pg/I MTBE pg/I Naphthalene pg/I 2L Groundwater Quality Standard 1 600 600 500 20 6 DW-Goodnight- New -Influent 7/18/2000 <1.0 <1.0 18 <3.0 6.2 - 8/16/2000 <1.0 <1.0 3 <3.0 <5.0 9/28/2000 <1.0 I <1.0 4.7 <3.0 1 <5.0 11/14/2000 <1.0 <1.0 <1.0 <3.0 <5.0 12/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 1/18/2001 <1.0 <1.0 <1.0 <3.0 <5.0 2/23/2001 <1.0 <1.0 <1.0 <3.0 <5.0 3/30/2001 <1.0 <1.0 <1.0 <3.0 <5.0 5/1/2001 <1.0 <1.0 <1.0 <3.0 <5.0 6/21/2001 <1.0 <1.0 <1.0 <3.0 <5.0 8/16/2001 <1.0 <1.0 <1.0 <3.0 <5.0 10/24/2001 <1.0 <1.0 <1.0 <3.0 <5.0 2/27/2002 <1.0 <1.0 <1.0 <3.0 <5.0 5/14/2002 <1.0 <1.0 <1.0 <1.0 <5.0 7/10/2002 <1.0 <1.0 <1.0 <1.0 <5.0 11/6/2002 <1.0 <1.0 <1.0 <1.0 <5.0 3/11/2003 <1.0 <1.0 <1.0 <3.0 <5.0 7/17/2003 <1.0 <1.0 <1.0 <3.0 <5.0 3/11/2004 <1.0 <1.0 <1.0 <3.0 <5.0 9/2/2004 <1.0 <1.0 <1.0 <2.0 <1.0 3/9/2005 <1.0 <1.0 <1.0 <3.0 <5.0 11/22/2005 <1.0 <1.0 <1.0 <3.0 <5.0 9/28/2006 <1.0 <1.0 <1.0 <3.0 <5.0 5/21/2009 <1.0 <1.0 <1.0 <3.0 <5.0 5/24/2011 <0.5 <1.0 <1.0 <3.0 <5.0 5/17/2012 <1.0 <1.0 <1.0 <3.0 <5.0 8/29/2013 <0.5 <0.5 <0.5 <3.0 <5.0 8/25/2014 <0.5 <0.5 <0.5 <3.0 <5.0 - 8/27/2015 <0.5 <0.5 <0.5 <3.0 <5.0 <1.0 8/29/2016 <0.5 <0.5 <0.5 <3.0 0.991 <1.0 8/22/2017 <0.50 <0.50 <0.50 <3.0 <5.0 <1.0 8/23/2018 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 Old Goodnight- Old 11/19/1999 <1.0 <1.0 <1.0 <3.0 <5.0 - 12/22/1999 <1.0 <1.0 <1.0 <3.0 <5.0 2/16/2000 <1.0 <1.0 <1.0 <3.0 <5.0 3/27/2000 <1.0 <1.0 <1.0 <3.0 <5.0 4/26/2000 <1.0 <1.0 <1.0 <3.0 <5.0 5/25/2000 <1.0 <1.0 <1.0 <3.0 <5.0 8/16/2000 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Goodnight- Old-CV-1 6/15/2000 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Goodnight- Old-CV-2 6/15/2000 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Goodnight- Old -Influent 6/15/2000 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Harwood 6/27/2000 <2.0 <2.0 <2.0 <4.0 <2.0 DW-Johnson 12/20/1999 <1.0 <1.0 <1.0 <3.0 <5.0 6/6/2007 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Kann-Station(2) 6/15/2000 <1.0 <1.0 <1.0 <3.0 <5.0 9/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 5/24/2011 <1.0 <1.0 <1.0 <3.0 <5.0 5/17/2012 <1.0 <1.0 <1.0 <3.0 <5.0 8/29/2013 <0.5 <0.5 <0.5 <3.0 <5.0 - 8/29/2016 <0.5 <0.5 <0.5 <3.0 <5.0 <1.0 8/22/2017 <0.50 <0.50 <0.50 <3.0 <5.0 <1.0 8/23/2018 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 DW-Keasler 10/2/2000 <1.0 <1.0 <1.0 <3.0 <5.0 - Page 5 of 14 Table 5 Summary of Water Quality Data for Residential Wells Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well ID Date Benzene pg/I Ethylbenzene pg/I Toluene pg/I Xylenes pg/I MTBE pg/I Naphthalene pg/I 2L Groundwater Quality Standard 1 600 600 500 20 6 DW-Keenan 11/23/1999 <1.0 <1.0 <1.0 <3.0 <5.0 - 2/16/2000 <1.0 <1.0 <1.0 <3.0 <5.0 3/27/2000 <1.0 <1.0 <1.0 <3.0 <5.0 4/26/2000 <1.0 <1.0 <1.0 <3.0 <5.0 5/25/2000 <1.0 <1.0 <1.0 <3.0 <5.0 6/15/2000 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Keenan- Influent 7/18/2000 <1.0 <1.0 <1.0 <3.0 <5.0 8/16/2000 <1.0 <1.0 <1.0 <3.0 <5.0 9/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 11/14/2000 <1.0 <1.0 <1.0 <3.0 <5.0 12/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 1/18/2001 <1.0 <1.0 <1.0 <3.0 <5.0 2/23/2001 <1.0 <1.0 <1.0 <3.0 <5.0 3/30/2001 <1.0 <1.0 <1.0 <3.0 <5.0 5/1/2001 <1.0 <1.0 <1.0 <3.0 <5.0 6/21/2001 <1.0 <1.0 <1.0 <3.0 <5.0 8/16/2001 <1.0 <1.0 <1.0 <3.0 <5.0 10/24/2001 <1.0 <1.0 <1.0 <3.0 <5.0 3/14/2002 <1.0 <1.0 <1.0 <3.0 <5.0 5/14/2002 <1.0 <1.0 <1.0 <1.0 <5.0 11/6/2002 <1.0 <1.0 <1.0 <1.0 <5.0 11/6/2002 <1.0 <1.0 <1.0 <1.0 <5.0 3/11/2003 <1.0 <1.0 <1.0 <3.0 <5.0 7/17/2003 <1.0 <1.0 <1.0 <3.0 <5.0 3/9/2005 <1.0 <1.0 <1.0 <3.0 <5.0 9/28/2006 <1.0 <1.0 <1.0 <3.0 <5.0 5/21/2009 <1.0 <1.0 <1.0 <3.0 <5.0 5/24/2011 <0.5 <1.0 <1.0 <3.0 <5.0 5/17/2012 <1.0 <1.0 <1.0 <3.0 <5.0 - 8/22/2017 <0.50 <0.50 <0.50 <3.0 <5.0 <1.0 DW-Kissiah 4/19/2000 <1.0 <1.0 <1.0 <3.0 <5.0 - DW-Laws 1/5/2000 <1.0 <1.0 <1.0 <3.0 <5.0 5/22/2000 <1.0 <1.0 <1.0 <3.0 <5.0 6/15/2000 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Laws Influent 7/31/2000 <1.0 <1.0 <1.0 <3.0 <5.0 9/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 11/14/2000 <1.0 <1.0 <1.0 <3.0 <5.0 12/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 1/18/2001 <1.0 <1.0 <1.0 <3.0 1 <5.0 2/23/2001 <1.0 <1.0 <1.0 <3.0 <5.0 3/30/2001 <1.0 <1.0 <1.0 <3.0 <5.0 5/1/2001 <1.0 <1.0 <1.0 <3.0 <5.0 7/6/2001 <1.0 <1.0 <1.0 <3.0 <5.0 8/16/2001 <1.0 <1.0 <1.0 <3.0 <5.0 10/24/2001 <1.0 <1.0 <1.0 <3.0 <5.0 3/1/2002 <1.0 <1.0 <1.0 <3.0 <5.0 7/10/2002 <1.0 <1.0 <1.0 <1.0 <5.0 11/6/2002 <1.0 <1.0 <1.0 <1.0 <5.0 3/11/2003 <1.0 <1.0 <1.0 <3.0 <5.0 7/17/2003 <1.0 <1.0 <1.0 <3.0 <5.0 12/28/2004 <1.0 <1.0 <1.0 <3.0 <5.0 8/29/2005 <1.0 <1.0 <1.0 <3.0 <5.0 9/28/2006 <1.0 <1.0 <1.0 <3.0 <5.0 9/28/2011 <1.0 <1.0 <1.0 <3.0 <5.0 9/11/2014 <0.5 <0.5 <0.5 <3.0 <5.0 Page 6 of 14 Table 5 Summary of Water Quality Data for Residential Wells Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well ID Date Benzene pg/I Ethylbenzene pg/I Toluene pg/I Xylenes pg/I MTBE pg/I Naphthalene pg/I 2L Groundwater Quality Standard 1 600 600 500 20 6 DW-Lunsford-D 6/28/2000 <2.0 <2.0 <2.0 <4.0 <2.0 - DW-Luther 11/23/1999 <1.0 <1.0 <1.0 <3.0 <5.0 3/27/2000 <1.0 I <1.0 <1.0 <3.0 1 <5.0 4/26/2000 <1.0 <1.0 <1.0 <3.0 <5.0 5/25/2000 <1.0 <1.0 <1.0 <3.0 <5.0 - 8/22/2017 <0.50 <0.50 <0.50 <3.0 <5.0 <1.0 DW-Luther- Effluent 6/15/2000 <1.0 <1.0 <1.0 <3.0 <5.0 - 8/11/2000 <5.0 <5.0 <5.0 <1.0 <5.0 6/15/2000 <1.0 <1.0 <1.0 <3.0 <5.0 8/11/2000 <5.0 <5.0 <5.0 <1.0 <5.0 9/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 11/14/2000 <1.0 <1.0 <1.0 <3.0 <5.0 1/18/2001 <1.0 <1.0 <1.0 <3.0 <5.0 2/23/2001 <1.0 <1.0 <1.0 <3.0 <5.0 6/22/2001 <1.0 <1.0 <1.0 <3.0 <5.0 3/1/2002 <1.0 <1.0 <1.0 <3.0 <5.0 7/10/2002 <1.0 <1.0 <1.0 <1.0 <5.0 11/22/2004 <1.0 <1.0 <1.0 <3.0 <5.0 9/28/2006 <1.0 <1.0 <1.0 <3.0 <5.0 5/21/2009 <1.0 <1.0 <1.0 <3.0 <5.0 5/24/2011 <0.5 <1.0 <1.0 <3.0 <5.0 5/17/2012 <1.0 <1.0 <1.0 <3.0 <5.0 D nutty- Inffluentluent 7/18/2000 <1.0 <1.0 <1.0 <3.0 <5.0 8/16/2000 <1.0 <1.0 <1.0 <3.0 <5.0 9/28/2000 <1.0 <1.0 <1.0 <3.0 <5.0 11/14/2000 <1.0 <1.0 <1.0 <3.0 <5.0 12/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 1/18/2001 <1.0 <1.0 <1.0 <3.0 <5.0 2/23/2001 <1.0 <1.0 <1.0 <3.0 <5.0 3/30/2001 <1.0 <1.0 <1.0 <3.0 <5.0 5/1/2001 <1.0 <1.0 <1.0 <3.0 <5.0 6/21/2001 <1.0 <1.0 <1.0 <3.0 <5.0 8/16/2001 <1.0 <1.0 <1.0 <3.0 <5.0 3/14/2002 <1.0 <1.0 <1.0 <3.0 <5.0 7/10/2002 <1.0 <1.0 <1.0 <1.0 <5.0 11/6/2002 <1.0 <1.0 <1.0 <1.0 <5.0 3/9/2005 <1.0 <1.0 <1.0 <3.0 <5.0 9/28/2006 <1.0 <1.0 <1.0 <3.0 <5.0 9/11/2014 <0.5 <0.5 <0.5 <3.0 <5.0 Page 7 of 14 Table 5 Summary of Water Quality Data for Residential Wells Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well ID Date Benzene pg/I Ethylbenzene pg/I Toluene pg/I Xylenes pg/I MTBE pg/I Naphthalene pg/I 2L Groundwater Quality Standard 1 600 600 500 20 6 DW-Maurer- CV-1 3/27/2000 <1.0 <1.0 <1.0 <3.0 <5.0 - 5/4/2000 <1.0 <1.0 <1.0 <3.0 <5.0 6/15/2000 <1.0 I <1.0 <1.0 <3.0 1 <5.0 7/18/2000 <1.0 <1.0 <1.0 <3.0 <5.0 8/16/2000 <1.0 <1.0 <1.0 <3.0 <5.0 9/28/2000 <1.0 <1.0 <1.0 <3.0 <5.0 11/14/2000 <1.0 <1.0 <1.0 <3.0 <5.0 2/23/2001 <1.0 <1.0 <1.0 <3.0 <5.0 3/30/2001 <1.0 <1.0 <1.0 <3.0 6.3 5/1/2001 <1.0 <1.0 <1.0 <3.0 5.4 6/21/2001 <1.0 <1.0 <1.0 <3.0 31 7/6/2001 <1.0 <1.0 <1.0 <3.0 <5.0 8/20/2001 <1.0 <1.0 <1.0 <3.0 <5.0 10/24/2001 <1.0 <1.0 <1.0 <3.0 6.1 3/1/2002 <1.0 <1.0 <1.0 <3.0 <5.0 5/14/2002 <1.0 <1.0 <1.0 <1.0 <5.0 7/10/2002 <1.0 <1.0 <1.0 <1.0 5.8 3/11/2003 <1.0 <1.0 <1.0 <3.0 <5.0 7/17/2003 <1.0 <1.0 <1.0 <3.0 <5.0 3/11/2004 <1.0 <1.0 <1.0 <3.0 <5.0 3/9/2005 <1.0 <1.0 <1.0 <3.0 <5.0 8/29/2005 <1.0 <1.0 <1.0 <3.0 <5.0 9/28/2006 <1.0 <1.0 <1.0 <3.0 <5.0 9/5/2007 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Maurer- CV-2 2/16/2000 <1.0 <1.0 <1.0 <3.0 <5.0 3/27/2000 <1.0 <1.0 <1.0 <3.0 <5.0 5/4/2000 <1.0 <1.0 <1.0 <3.0 <5.0 5/25/2000 <1.0 <1.0 <1.0 <3.0 <5.0 6/15/2000 <1.0 <1.0 <1.0 <3.0 <5.0 7/18/2000 <1.0 <1.0 <1.0 <3.0 <5.0 8/16/2000 <1.0 <1.0 <1.0 <3.0 <5.0 9/28/2000 <1.0 <1.0 <1.0 <3.0 <5.0 11/14/2000 <1.0 <1.0 <1.0 <3.0 <5.0 12/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 1/18/2001 <1.0 <1.0 <1.0 <3.0 <5.0 2/23/2001 <1.0 <1.0 <1.0 <3.0 <5.0 3/30/2001 <1.0 <1.0 <1.0 <3.0 <5.0 5/1/2001 <1.0 <1.0 <1.0 <3.0 <5.0 6/21/2001 <1.0 <1.0 <1.0 <3.0 <5.0 8/20/2001 <1.0 <1.0 <1.0 <3.0 <5.0 10/24/2001 <1.0 <1.0 <1.0 <3.0 <5.0 3/1/2002 <1.0 <1.0 <1.0 <3.0 <5.0 5/14/2002 <1.0 <1.0 <1.0 <1.0 <5.0 7/10/2002 <1.0 <1.0 <1.0 <1.0 <5.0 11/6/2002 <1.0 <1.0 <1.0 <1.0 <5.0 3/11/2003 <1.0 <1.0 <1.0 <3.0 <5.0 7/17/2003 <1.0 <1.0 <1.0 <3.0 <5.0 3/11/2004 <1.0 <1.0 <1.0 <3.0 <5.0 9/2/2004 <1.0 <1.0 <1.0 <2.0 <1.0 3/9/2005 <1.0 <1.0 <1.0 <3.0 <5.0 8/29/2005 <1.0 <1.0 <1.0 <3.0 <5.0 9/28/2006 <1.0 <1.0 <1.0 <3.0 <5.0 9/5/2007 <1.0 <1.0 <1.0 <3.0 <5.0 5/24/2011 <0.5 <1.0 <1.0 <3.0 <5.0 8/27/2015 <0.5 <0.5 <0.5 <3.0 <5.0 <1.0 8/29/2016 <0.5 <0.5 <0.5 <3.0 <5.0 <1.0 Page 8 of 14 Table 5 Summary of Water Quality Data for Residential Wells Colonial Pipeline Company Kannapolis Booster Station Concord, INC Well ID Date Benzene pg/I Ethylbenzene pg/I Toluene pg/I Xylenes pg/I MTBE pg/I Naphthalene pg/I 2L Groundwater Quality Standard 1 600 600 500 20 6 DW-Maurer 12/27/1999 <1.0 <1.0 <1.0 <3.0 <5.0 - 1/5/2000 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Maurer- Influent 2/16/2000 <1.0 I <1.0 <1.0 <3.0 <5.0 3/27/2000 <1.0 <1.0 <1.0 <3.0 10 5/4/2000 <1.0 <1.0 <1.0 <3.0 28 5/25/2000 <1.0 <1.0 <1.0 <3.0 31 6/15/2000 <1.0 <1.0 <1.0 <3.0 32 7/18/2000 <1.0 <1.0 <1.0 <3.0 12 8/16/2000 <1.0 <1.0 <1.0 <3.0 40 9/28/2000 <1.0 <1.0 <1.0 <3.0 40 11/14/2000 <1.0 <1.0 <1.0 <3.0 33 12/13/2000 <1.0 <1.0 <1.0 <3.0 40 1/18/2001 <1.0 <1.0 <1.0 <3.0 34 2/23/2001 <1.0 <1.0 <1.0 <3.0 38 3/30/2001 <1.0 <1.0 <1.0 <3.0 39 5/1/2001 <1.0 <1.0 <1.0 <3.0 23 6/21/2001 <1.0 <1.0 <1.0 <3.0 31 8/20/2001 <1.0 <1.0 <1.0 <3.0 19 10/24/2001 <1.0 <1.0 <1.0 <3.0 28 3/1/2002 <1.0 <1.0 <1.0 <3.0 18 5/14/2002 <1.0 <1.0 <1.0 <1.0 21 7/10/2002 <1.0 <1.0 <1.0 <1.0 28 11/6/2002 <1.0 <1.0 <1.0 <1.0 24 3/11/2003 <1.0 <1.0 <1.0 <3.0 12 7/17/2003 <1.0 <1.0 <1.0 <3.0 <5.0 3/11/2004 <1.0 <1.0 <1.0 <3.0 16 9/2/2004 <1.0 <1.0 <1.0 <2.0 8.7 3/9/2005 <1.0 <1.0 <1.0 <3.0 6.9 8/29/2005 <1.0 <1.0 <1.0 <3.0 7.4 9/28/2006 <1.0 <1.0 <1.0 <3.0 5.2 9/5/2007 <1.0 <1.0 <1.0 <3.0 <5.0 5/21/2009 <1.0 <1.0 <1.0 <3.0 <5.0 5/24/2011 <0.5 <1.0 <1.0 <3.0 <5.0 5/17/2012 <1.0 <1.0 <1.0 <3.0 <5.0 8/29/2013 <0.5 <0.5 <0.5 <3.0 <5.0 8/25/2014 <0.5 <0.5 <0.5 <3.0 <5.0 - 8/27/2015 <0.5 <0.5 <0.5 <3.0 <5.0 <1.0 8/29/2016 <0.5 <0.5 <0.5 <3.0 2.OJ <1.0 8/22/2017 <0.50 <0.50 <0.50 <3.0 <5.0 <1.0 8/23/2018 <1.0 <1.0 <1.0 <3.0 1.9 <1.0 DW-Mesimer-D 6/27/2000 <2.0 <2.0 <2.0 <4.0 <2.0 - DW-Mesimer-H 6/27/2000 <2.0 <2.0 <2.0 <4.0 <2.0 DW-Mesimer-K 6/27/2000 <2.0 <2.0 <2.0 <4.0 <2.0 DW-Michael 7/31/2000 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Murphy 6/15/2000 <1.0 <1.0 <1.0 <3.0 <5.0 9/28/2000 <1.0 <1.0 <1.0 <3.0 <5.0 6/21/2001 <1.0 <1.0 <1.0 <3.0 <5.0 12/6/2001 <1.0 <1.0 <1.0 <3.0 <5.0 7/10/2002 <1.0 <1.0 <1.0 <1.0 <5.0 6/5/2007 <1.0 <1.0 <1.0 <1.0 <5.0 DW-Myers 12/20/1999 <1.0 <1.0 <1.0 <3.0 48 12/22/1999 <1.0 <1.0 <1.0 <3.0 81 1/5/2000 <1.0 <1.0 <1.0 <3.0 51 5/21/2009 <1.0 <1.0 <1.0 <3.0 <5.0 Page 9 of 14 Table 5 Summary of Water Quality Data for Residential Wells Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well ID Date Benzene pg/I Ethylbenzene pg/I Toluene pg/I Xylenes pg/I MTBE pg/I Naphthalene pg/I 2L Groundwater Quality Standard 1 600 600 500 20 6 6W-Myers-CV-1 2/16/2000 <1.0 <1.0 <1.0 <3.0 <5.0 - DW-Myers CV-2 1/18/2000 <1.0 <1.0 <1.0 <3.0 <5.0 2/16/2000 <1.0 I <1.0 <1.0 <3.0 1 <5.0 DW-Myers-Influent 1/18/2000 <1.0 <1.0 <1.0 <3.0 66 2/16/2000 <1.0 <1.0 <1.0 <3.0 62 8/16/2001 <1.0 <1.0 <1.0 <3.0 <5.0 2/27/2002 <1.0 <1.0 <1.0 <3.0 <5.0 2/19/2004 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Owens 12/27/1999 <1.0 <1.0 <1.0 <3.0 <5.0 3/27/2000 <1.0 <1.0 <1.0 <3.0 <5.0 6/15/2000 <1.0 <1.0 <1.0 <3.0 <5.0 10/2/2000 <1.0 <1.0 <1.0 <3.0 <5.0 12/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 3/30/2001 <1.0 <1.0 <1.0 <3.0 <5.0 6/21/2001 <1.0 <1.0 <1.0 <3.0 <5.0 7/10/2002 <1.0 <1.0 <1.0 <1.0 <5.0 8/29/2005 <1.0 <1.0 <1.0 <1.0 <5.0 DW-Parker 12/20/1999 <1.0 <1.0 <1.0 <3.0 <5.0 4/10/2000 <1.0 <1.0 <1.0 <3.0 <5.0 6/15/2000 <1.0 <1.0 <1.0 <3.0 <5.0 9/28/2000 <1.0 <1.0 <1.0 <3.0 <5.0 12/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 3/30/2001 <1.0 <1.0 <1.0 <3.0 <5.0 6/22/2001 <1.0 <1.0 <1.0 <3.0 <5.0 7/10/2002 <1.0 <1.0 <1.0 <1.0 <5.0 DW-Porter 6/28/2000 <2.0 <2.0 <2.0 <4.0 <2.0 DW-Poteat 2/16/2000 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Preslar 5/22/2000 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Reynolds 4/10/2000 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Rhodes 6/28/2000 <2.0 <2.0 <2.0 <4.0 <2.0 8/16/2000 <1.0 <1.0 <1.0 <3.0 <5.0 11/14/2000 <1.0 <1.0 <1.0 <3.0 <5.0 12/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 1/18/2001 <1.0 <1.0 <1.0 <3.0 <5.0 2/23/2001 <1.0 <1.0 <1.0 <3.0 <5.0 3/30/2001 <1.0 <1.0 <1.0 <3.0 <5.0 5/1/2001 <1.0 <1.0 <1.0 <3.0 <5.0 8/16/2001 <1.0 <1.0 <1.0 <3.0 <5.0 3/14/2002 <1.0 <1.0 <1.0 <3.0 <5.0 7/10/2002 <1.0 <1.0 <1.0 <1.0 <5.0 11/6/2002 <1.0 <1.0 <1.0 <1.0 <5.0 3/9/2005 <1.0 <1.0 <1.0 <3.0 <5.0 9/11/2014 <0.5 <0.5 <0.5 <3.0 <5.0 DW-Schaffner- Influent 9/28/2000 <1.0 <1.0 <1.0 <3.0 <5.0 11/14/2000 <1.0 <1.0 <1.0 <3.0 <5.0 12/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 1/18/2001 <1.0 <1.0 <1.0 <3.0 <5.0 2/23/2001 <1.0 <1.0 <1.0 <3.0 <5.0 5/1/2001 <1.0 <1.0 <1.0 <3.0 <5.0 6/21/2001 <1.0 <1.0 <1.0 <3.0 <5.0 8/16/2001 <1.0 <1.0 <1.0 <3.0 <5.0 10/24/2001 <1.0 <1.0 <1.0 <3.0 <5.0 3/1/2002 <1.0 <1.0 <1.0 <3.0 <5.0 5/14/2002 <1.0 <1.0 <1.0 <1.0 <5.0 7/10/2002 <1.0 <1.0 <1.0 <1.0 <5.0 11/6/2002 <1.0 <1.0 <1.0 <1.0 <5.0 3/11/2003 <1.0 <1.0 <1.0 <3.0 <5.0 3/9/2005 <1.0 <1.0 <1.0 <3.0 <5.0 9/28/2006 1 <1.0 <1.0 <1.0 <3.0 <5.0 Page 10 of 14 Table 5 Summary of Water Quality Data for Residential Wells Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well ID Date Benzene pg/I Ethylbenzene pg/I Toluene pg/I Xylenes pg/I MTBE pg/I Naphthalene pg/I 2L Groundwater Quality Standard 1 600 600 500 20 6 DW-Schroeder 6/27/2000 <2.0 <2.0 <2.0 <4.0 <2.0 - DW-Shinn 8/11/2000 <5.0 <5.0 <5.0 <1.0 <5.0 DW-Smith 11/23/1999 <1.0 I <1.0 <1.0 <3.0 1 <5.0 3/27/2000 <1.0 <1.0 <1.0 <3.0 <5.0 6/15/2000 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Smith-David 5/22/2000 <1.0 <1.0 <1.0 <3.0 <5.0 3/30/2001 <1.0 <1.0 <1.0 <3.0 <5.0 9/11/2014 <0.5 <0.5 <0.5 <3.0 <5.0 DW-Smith-Influent 9/28/2000 <1.0 <1.0 <1.0 <3.0 <5.0 12/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 3/30/2001 <1.0 <1.0 <1.0 <3.0 <5.0 6/21/2001 <1.0 <1.0 <1.0 <3.0 <5.0 10/24/2001 <1.0 <1.0 <1.0 <3.0 <5.0 7/10/2002 <1.0 <1.0 <1.0 <1.0 <5.0 8/29/2005 <1.0 <1.0 <1.0 <1.0 <5.0 5/21/2009 <1.0 <1.0 <1.0 <3.0 <5.0 - 8/22/2017 <0.50 <0.50 <0.50 <3.0 <5.0 <1.0 DW-Snyder 7/6/2000 <1.0 <1.0 <1.0 <1.0 <1.0 - 9/17/2001 <1.0 <1.0 <1.0 <3.0 <5.0 6/18/2007 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Teal 8/25/2014 <0.5 <0.5 <0.5 <3.0 15 8/25/2014(4) <0.5 <0.5 <0.5 <3.0 7.4 - DW-Teal-Effluent 8/27/2015 <0.5 <0.5 <0.5 <3.0 <5.0 <1.0 8/29/2016 <0.5 <0.5 <0.5 <3.0 <5.0 <1.0 DW-Teal-Influent 8/27/2015 <0.5 <0.5 <0.5 <3.0 <5.0 <1.0 8/29/2016 <0.5 <0.5 <0.5 <3.0 <5.0 <1.0 DW-Tucker 12/27/1999 <1.0 <1.0 <1.0 <3.0 <5.0 - 3/27/2000 <1.0 <1.0 <1.0 <3.0 <5.0 4/26/2000 <1.0 <1.0 <1.0 <3.0 <5.0 5/25/2000 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Tucker-CV-1 6/15/2000 <1.0 <1.0 <1.0 <3.0 <5.0 7/18/2000 <1.0 <1.0 <1.0 <3.0 <5.0 8/16/2000 <1.0 <1.0 <1.0 <3.0 <5.0 9/28/2000 <1.0 <1.0 <1.0 <3.0 <5.0 11/14/2000 <1.0 <1.0 <1.0 <3.0 <5.0 12/13/2000 <1.0 <1.0 <1.0 <3.0 19 1/18/2001 <1.0 <1.0 <1.0 <3.0 <5.0 2/23/2001 <1.0 <1.0 <1.0 <3.0 <5.0 3/30/2001 <1.0 <1.0 <1.0 <3.0 <5.0 5/1/2001 <1.0 <1.0 <1.0 <3.0 <5.0 6/21/2001 <1.0 <1.0 <1.0 <3.0 27 7/6/2001 <1.0 <1.0 <1.0 <3.0 <5.0 8/16/2001 <1.0 <1.0 <1.0 <3.0 <5.0 10/24/2001 <1.0 <1.0 <1.0 <3.0 <5.0 3/1/2002 <1.0 <1.0 <1.0 <3.0 <5.0 5/14/2002 <1.0 <1.0 <1.0 <1.0 <5.0 7/10/2002 <1.0 <1.0 <1.0 <1.0 <5.0 11/6/2002 <1.0 <1.0 <1.0 <1.0 14 3/11/2003 <1.0 <1.0 <1.0 <3.0 <5.0 7/17/2003 <1.0 <1.0 <1.0 <3.0 <5.0 3/11/2004 <1.0 <1.0 <1.0 <3.0 7.5 9/2/2004 <1.0 <1.0 <1.0 <2.0 <1.0 3/9/2005 <1.0 <1.0 <1.0 <3.0 <1.0 8/29/2005 <1.0 <1.0 <1.0 <3.0 <1.0 9/5/2007 <1.0 <1.0 <1.0 <3.0 <1.0 9/5/2007 <1.0 <1.0 <1.0 <3.0 <1.0 Page 11 of 14 Table 5 Summary of Water Quality Data for Residential Wells Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well ID Date Benzene pg/I Ethylbenzene pg/I Toluene pg/I Xylenes pg/I MTBE pg/I Naphthalene pg/I 2L Groundwater Quality Standard 1 600 600 500 20 6 DW-Tucker-CV-2 6/15/2000 <1.0 <1.0 <1.0 <3.0 <5.0 - 7/18/2000 <1.0 <1.0 <1.0 <3.0 <5.0 8/16/2000 <1.0 I <1.0 <1.0 <3.0 1 <5.0 9/28/2000 <1.0 <1.0 <1.0 <3.0 <5.0 11/14/2000 <1.0 <1.0 <1.0 <3.0 <5.0 12/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 1/18/2001 <1.0 <1.0 <1.0 <3.0 <5.0 2/23/2001 <1.0 <1.0 <1.0 <3.0 <5.0 3/30/2001 <1.0 <1.0 <1.0 <3.0 <5.0 5/1/2001 <1.0 <1.0 <1.0 <3.0 <5.0 6/21/2001 <1.0 <1.0 <1.0 <3.0 <5.0 7/6/2001 <1.0 <1.0 <1.0 <3.0 <5.0 8/16/2001 <1.0 <1.0 <1.0 <3.0 <5.0 10/24/2001 <1.0 <1.0 <1.0 <3.0 <5.0 3/1/2002 <1.0 <1.0 <1.0 <3.0 <5.0 5/14/2002 <1.0 <1.0 <1.0 <1.0 <5.0 7/10/2002 <1.0 <1.0 <1.0 <1.0 <5.0 11/6/2002 <1.0 <1.0 <1.0 <1.0 <5.0 3/11/2003 <1.0 <1.0 <1.0 <3.0 <5.0 7/17/2003 <1.0 <1.0 <1.0 <3.0 <5.0 3/11/2004 <1.0 <1.0 <1.0 <3.0 5.5 9/2/2004 <1.0 <1.0 <1.0 <2.0 <1.0 3/9/2005 <1.0 <1.0 <1.0 <3.0 <5.0 8/29/2005 <1.0 <1.0 <1.0 <3.0 <5.0 9/28/2006 <1.0 <1.0 <1.0 <3.0 <5.0 9/5/2007 <1.0 <1.0 <1.0 <3.0 <5.0 5/24/2011 <0.5 <1.0 <1.0 <3.0 <5.0 - 8/27/2015 <0.5 <1.0 <1.0 <3.0 <5.0 <1.0 8/29/2016 <0.5 <1.0 <1.0 <3.0 <5.0 <1.0 DW-Tucker- Influent(3) 6/15/2000 <1.0 <1.0 <1.0 <3.0 <5.0 - 7/18/2000 <1.0 <1.0 <1.0 <3.0 <5.0 8/16/2000 <1.0 <1.0 <1.0 <3.0 <5.0 9/28/2000 <1.0 <1.0 <1.0 <3.0 8.4 11/14/2000 <1.0 <1.0 <1.0 <3.0 16 12/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 1/18/2001 <1.0 <1.0 <1.0 <3.0 23 2/23/2001 <1.0 <1.0 <1.0 <3.0 23 3/30/2001 <1.0 <1.0 <1.0 <3.0 24 5/1/2001 <1.0 <1.0 <1.0 <3.0 24 6/21/2001 <1.0 <1.0 <1.0 <3.0 <5.0 7/6/2001 <1.0 <1.0 <1.0 <3.0 36 8/16/2001 <1.0 <1.0 <1.0 <3.0 24 10/24/2001 <1.0 <1.0 <1.0 <3.0 20 3/1/2002 <1.0 <1.0 <1.0 <3.0 13 5/14/2002 <1.0 <1.0 <1.0 <1.0 11 7/10/2002 <1.0 <1.0 <1.0 <1.0 14 11/6/2002 <1.0 <1.0 <1.0 <1.0 15 3/11/2003 <1.0 <1.0 <1.0 <3.0 <5.0 7/17/2003 <1.0 <1.0 <1.0 <3.0 <5.0 3/11/2004 <1.0 <1.0 <1.0 <3.0 7.1 9/2/2004 <1.0 <1.0 <1.0 <2.0 3.9 3/9/2005 <1.0 <1.0 <1.0 <3.0 <5.0 8/29/2005 <1.0 <1.0 <1.0 <3.0 <5.0 9/28/2006 <1.0 <1.0 <1.0 <3.0 2.8 J 9/5/2007 <1.0 <1.0 <1.0 <3.0 <5.0 5/21/2009 <1.0 <1.0 <1.0 <3.0 <5.0 5/24/2011 <0.5 <1.0 <1.0 <3.0 <5.0 5/17/2012 <1.0 <1.0 <1.0 <3.0 <5.0 8/25/2014 <1.0 <1.0 <1.0 <3.0 <5.0 8/27/2015 <0.5 <0.5 <0.5 <3.0 <5.0 <1.0 8/29/2016 <0.5 <0.5 <0.5 <3.0 1.91 <1.0 8/24/2017 <0.50 <0.50 <0.50 <3.0 <5.0 <1.0 8/23/2018 <1.0 <1.0 <1.0 <3.0 1.3 <1.0 Page 12 of 14 Table 5 Summary of Water Quality Data for Residential Wells Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well ID Date Benzene pg/I Ethylbenzene pg/I Toluene pg/I Xylenes pg/I MTBE pg/I Naphthalene pg/I 2L Groundwater Quality Standard 1 600 600 500 20 6 DW-Wally 6/28/2000 <2.0 <2.0 <2.0 <4.0 <2.0 - DW-Ware 2/28/2001 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Watts 12/22/1999 <1.0 I <1.0 <1.0 <3.0 1 26 12/27/1999 <1.0 <1.0 <1.0 <3.0 <5.0 1/5/2000 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Watts-CV-1 3/27/2000 <1.0 <1.0 <1.0 <3.0 <5.0 5/4/2000 <1.0 <1.0 <1.0 <3.0 <5.0 6/15/2000 <1.0 <1.0 <1.0 <3.0 11 8/16/2000 <1.0 <1.0 <1.0 <3.0 <5.0 10/2/2000 <1.0 <1.0 <1.0 <3.0 <5.0 11/14/2000 <1.0 <1.0 <1.0 <3.0 <5.0 1/18/2001 <1.0 <1.0 <1.0 <3.0 <5.0 5/7/2001 <1.0 <1.0 <1.0 <3.0 <5.0 6/21/2001 <1.0 <1.0 <1.0 <3.0 <5.0 8/16/2001 <1.0 <1.0 <1.0 <3.0 <5.0 10/24/2001 <1.0 <1.0 <1.0 <3.0 <5.0 3/1/2002 <1.0 <1.0 <1.0 <3.0 <5.0 5/14/2002 <1.0 <1.0 <1.0 <1.0 <5.0 7/10/2002 <1.0 <1.0 <1.0 <1.0 <5.0 11/6/2002 <1.0 <1.0 <1.0 <1.0 <5.0 3/11/2003 <1.0 <1.0 <1.0 <3.0 <5.0 7/17/2003 <1.0 <1.0 <1.0 <3.0 <5.0 3/11/2004 <1.0 <1.0 <1.0 <3.0 19 9/2/2004 <1.0 <1.0 <1.0 <2.0 <1.0 3/9/2005 <1.0 <1.0 <1.0 <3.0 <5.0 8/29/2005 <1.0 <1.0 <1.0 <3.0 <5.0 9/28/2006 <1.0 <1.0 <1.0 <3.0 <5.0 9/5/2007 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Watts CV-2 2/2/2000 <1.0 <1.0 <1.0 <3.0 <5.0 3/27/2000 <1.0 <1.0 <1.0 <3.0 <5.0 5/4/2000 <1.0 <1.0 <1.0 <3.0 <5.0 5/25/2000 <1.0 <1.0 <1.0 <3.0 <5.0 6/15/2000 <1.0 <1.0 <1.0 <3.0 <5.0 7/18/2000 <1.0 <1.0 <1.0 <3.0 <5.0 8/16/2000 <1.0 <1.0 <1.0 <3.0 <5.0 9/28/2000 <1.0 <1.0 <1.0 <3.0 <5.0 11/14/2000 <1.0 <1.0 <1.0 <3.0 <5.0 12/13/2000 <1.0 <1.0 <1.0 <3.0 <5.0 1/18/2001 <1.0 <1.0 <1.0 <3.0 <5.0 2/23/2001 <1.0 <1.0 <1.0 <3.0 <5.0 3/30/2001 <1.0 <1.0 <1.0 <3.0 <5.0 5/1/2001 <1.0 <1.0 <1.0 <3.0 <5.0 6/21/2001 <1.0 <1.0 <1.0 <3.0 <5.0 8/16/2001 <1.0 <1.0 <1.0 <3.0 <5.0 10/24/2001 <1.0 <1.0 <1.0 <3.0 <5.0 3/1/2002 <1.0 <1.0 <1.0 <3.0 <5.0 5/14/2002 <1.0 <1.0 <1.0 <1.0 <5.0 7/10/2002 <1.0 <1.0 <1.0 <1.0 <5.0 11/6/2002 <1.0 <1.0 <1.0 <1.0 <5.0 3/11/2003 <1.0 <1.0 <1.0 <3.0 <5.0 7/17/2003 <1.0 <1.0 <1.0 <3.0 6.3 7/30/2003 <1.0 <1.0 <1.0 <3.0 <5.0 3/11/2004 <1.0 <1.0 <1.0 <3.0 <5.0 9/2/2004 <1.0 <1.0 <1.0 <2.0 <1.0 3/9/2005 <1.0 <1.0 <1.0 <3.0 <5.0 8/29/2005 <1.0 <1.0 <1.0 <3.0 <5.0 9/28/2006 <1.0 <1.0 <1.0 <3.0 <5.0 9/5/2007 <1.0 <1.0 <1.0 1 <3.0 <5.0 Page 13 of 14 Table 5 Summary of Water Quality Data for Residential Wells Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well ID Date Benzene pg/I Ethylbenzene pg/I Toluene pg/I Xylenes pg/I MTBE pg/I Naphthalene pg/I 2L Groundwater Quality Standard 1 600 600 500 20 6 DW-Watts New-CV2 8/27/2015 <0.5 <0.5 <0.5 <3.0 <5.0 <1.0 8/29/2016 <0.5 <0.5 <0.5 <3.0 <5.0 <1.0 DW-Watts Influent 2/2/2000 <1.0 I <1.0 <1.0 <3.0 15 1 - 3/27/2000 <1.0 <1.0 <1.0 <3.0 <5.0 5/4/2000 <1.0 <1.0 <1.0 <3.0 19 5/25/2000 <1.0 <1.0 <1.0 <3.0 21 6/15/2000 <1.0 <1.0 1.5 <3.0 17 7/18/2000 <1.0 <1.0 <1.0 <3.0 30 8/16/2000 <1.0 <1.0 <1.0 <3.0 30 9/28/2000 <1.0 <1.0 <1.0 <3.0 51 11/14/2000 <1.0 <1.0 <1.0 <3.0 46 12/13/2000 <1.0 <1.0 <1.0 <3.0 49 1/18/2001 <1.0 <1.0 <1.0 <3.0 65 2/23/2001 <1.0 <1.0 <1.0 <3.0 73 3/30/2001 <1.0 <1.0 <1.0 <3.0 81 5/1/2001 <1.0 <1.0 <1.0 <3.0 75 6/21/2001 <1.0 <1.0 <1.0 <3.0 <5.0 8/16/2001 <1.0 <1.0 <1.0 <3.0 <5.0 10/24/2001 <1.0 <1.0 <1.0 <3.0 61 3/1/2002 <1.0 <1.0 <1.0 <3.0 24 5/14/2002 <1.0 <1.0 <1.0 <1.0 13 7/10/2002 <1.0 <1.0 <1.0 <1.0 69 11/6/2002 <1.0 <1.0 <1.0 <1.0 35 3/11/2003 <1.0 <1.0 <1.0 <3.0 30 7/17/2003 <1.0 <1.0 <1.0 <3.0 13 3/11/2004 <1.0 <1.0 <1.0 <3.0 23 9/2/2004 <1.0 <1.0 <1.0 <2.0 6.2 3/9/2005 <1.0 <1.0 <1.0 <3.0 <5.0 8/29/2005 <1.0 <1.0 <1.0 <3.0 10 9/28/2006 <1.0 <1.0 <1.0 <3.0 4.4 J 9/5/2007 <1.0 <1.0 <1.0 <3.0 8.6 5/21/2009 <1.0 <1.0 <1.0 <3.0 <5.0 DW-Watts-New- Influent 2/25/2008 <0.5 <1.0 <1.0 <3.0 <5.0 5/21/2009 <1.0 <1.0 <1.0 <3.0 <5.0 5/24/2011 <0.5 <1.0 <1.0 <3.0 <5.0 5/17/2012 <1.0 <1.0 <1.0 <3.0 <5.0 8/29/2013 <0.5 <0.5 <0.5 <3.0 <5.0 8/25/2014 <0.5 <0.5 <0.5 <3.0 <5.0 8/27/2015 <0.5 <0.5 <0.5 <3.0 <5.0 <1.0 8/29/2016 <0.5 <0.5 <0.5 <3.0 1.3J <1.0 8/22/2017 <0.50 <0.50 <0.50 <3.0 <5.0 <1.0 8/23/2018 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 DW-Wilkinson 2/2/2000 <1.0 <1.0 <1.0 <3.0 <5.0 - 10/2/2000 <1.0 <1.0 <1.0 <3.0 <5.0 6/21/2001 <1.0 <1.0 <1.0 <3.0 <5.0 7/10/2002 <1.0 <1.0 <1.0 <1.0 <5.0 DW-Wright 6/28/2000 1 <2.0 <2.0 <2.0 <4.0 <2.0 Notes: pg/I = micrograms per liter 2L Groundwater Quality Standard = NCAC 15A 2L .0202 Groundwater Quality Standard MTBE = Methyl-tert-butyl ether < = Not detected above reporting limit. J = Estimated value below reporting limit. Bold values indicate constituent detection. CV-1 = 1 st carbon vessel effluent. CV-2 = 2nd carbon vessel effluent. Influent = for point -of -entry system. Effluent = for point -of -entry system. (1) DW-Crowe (MW-16) used as monitoring well only. (2) New well installed in 2010. (3) Tucker sold to Stief 3/2014. (4) Sample re -run. Page 14 of 14 FIGURES �1 APEX [ %BARRLIti , �. ---- a ti N USGS The National Map: National Boundaries Dataset, National Elevation Dataset, Geographic Names Information System, National Hydrography 0 1,000 2,000 Dataset; National Land Cover Database, National Structures Dataset, and National Transportation Dataset; U.S. Census Bureau - TIGER/Line; HERE Feet Road Data. Data Refreshed July, 2017. CHECK BY: AS FIGURE DRAWN BY: SP SITE LOCATION MAP � DATE: 9/6/18 SCALE: AS SHOWN COLONIAL PIPELINE COMPANY CAD NO.: CPC18012.001 KANNAPOLIS BOOSTER STATION APEX „ PRJ NO.: CPC18012.001 CONCORD, NORTH CAROLINA L X --- \ w f X x - . MW-4 �MW-23 r„1 • �, t�lkEl'POWER COMPA Y A * J t�4 r ; ..�.. • , .,x t SUB STATION-- / .1 •� 1 _. ��, . ' ,� �' ; . +� d MW-5 ., 24" CMP ASPHALT PAVED MW-24 * LINE 2 I �� MAN FOLDI I ` M W-25 1 4� [ Y ®BMW-25D LINE 1 MANIFOLD •, i .ter'.",@ ' ���"""� sr• �� MW-3' A. � I PZ-4 �•� MW-6 x I ' 4�• - AIRSPARGE V TRENCH �p PZ-3 1 3 _ y MW-1 SP SYSTEMTEM MW-21 PAD - I •t, ;, � , e MW-22I1 k TREATMENT _ � `'� ' _� SYSTEM PAD MW-8 � I I UNE 1 Y 1 PIG SIGNAL MW-2 i x POTABLE WATER MW_190 PZ-2 10 . SUPPLY WELL ' MW-17 O PZ41 1 a �_ x LiT''� .. il•' CHECK BY AS DRAWN BY SP ' r� DATE 9/6/18 SCALE AS SHOWN CAD NO. CPC18012.001 � PRJ N0. CPC18012.001 IA LEGEND :- - - PROPERTY LINE x FENCE LINE G COLONIAL PIPELINEI ANCILLARY PIPINGI MW-1 SHALLOW MONITORING WELL ,.4 t MW-2 DEEP MONITORING WELL 1�y• ; MW-11 ABANDONED MONITORING WELL r I9 RW-15 RECOVERY WELL 0 PZ-1 PIEZOMETER 0 PIG -SIGNAL NZ19MISfe Y SCALE IN FEET 0 40 80 160 WELL DESIGNATION UPDATE FORMER WELL NAME NEW WELL NAME MW-1 MW-1 MW-2 ABANDONED - MW-2D MW-2 MW-3 MW-3 MW-4 MW-4 MW-5 MW-5 MW-6 MW-6 MW-6D MW-7 MW-7 ABANDONED - MW-8 MW-8 MW-9D MW-9 MW-1 OD MW-10 MW-11 ABANDONED MW-11 MW-12D MW-12 MW-13 MW-13 MW-14 ABANDONED - MW-15 ABANDONED - MW-16 ABANDONED - MW-17 MW-14 MW-17D RECOVERY WELL MW-15 CROWE WELL MW-16 TR-lU MW-17 TR-lD MW-18 TR-2U MW-19 TR-2D MW-20 TR-3U 1MW-21 TR-3D MW-22 NOTES: 1. ANCILLARY PIPING AND COLONIAL PIPELINE LOCATIONS ARE APPROXIMATE AND ARE FOR FIGURE PURPOSES ONLY. 2. MAP BASED OFF DRAWING ENTITLED "FACILITY MAP" DATED APRIL 1, 2014 COMPLETED BY PROGRESSIVE ENGINEERING AND CONSTRUCTION, INC. FIGURE SITE PLAN COLONIAL PIPELINE COMPANY 2 KANNAPOLIS BOOSTER STATION r CONCORD, NORTH CAROLINA APEX LEGEND — — PROPERTY LINE X FENCE LINE c COLONIAL PIPELINE' ANCILLARY PIPING' ASPHALT PAVED SB-1 RECOVERY WELL 1W SB-7 RECOVERY WELL ABANDONED �..w� FREE PRODUCT EXTENT (NOT DETECTED AUGUST 2018) SB-11 BV-1 BIO—VENTING WELL BS-1 BIO—SPARGE WELL ®BV-1 BS-1 ® BV-3 (SVE-5) BV-2 SB-14 SB-6� SB— Ig SB-10 19 RW-02 BV-4 SSB/ SB-15 BS-3 SB-1 c CD • — SB-5 RW-01 "SB-1 SB-13 BS-2 0 SB-12 B-19 1w SB-7 B-17 CHECK BY AS DRAWN BY SP DATE 9/6/18 SCALE AS SHOWN CAD NO. CPC18012.001 PRJ NO. CPC18012.001 RECOVERY WELL LOCATIONS AUGUST 16, 2018 COLONIAL PIPELINE COMPANY KANNAPOLIS BOOSTER STATION CONCORD, NORTH CAROLINA SCALE IN FEET 0 10 20 40 NOTES: 1. ANCILLARY PIPING AND COLONIAL PIPELINE LOCATIONS ARE APPROXIMATE AND ARE FOR FIGURE PURPOSES ONLY. 2. MAP BASED OFF DRAWING ENTITLED "FACILITY MAP" DATED APRIL 1, 2014 COMPLETED BY PROGRESSIVE ENGINEERING AND CONSTRUCTION, INC. APEX FIGURE 3 i i 1 1 I 1 1 1 1 DUKE POWER COMPANY I 1 I 1 I 1 24" I 1 I 1 1 I 1 } 1 3 I 1 O I K I i a ' W 1 � IO 1 1 I 1 1 L_-- �x-x- I x x �x__j x / I 100, MW-4 / 717.70 Q5 W-18 MW-� MW-15 �f x (RW-15) PRJ NO. CPC18012.001 ' LEGEND - - PROPERTY LINE X FENCE LINE G COLONIAL PIPELINE' ANCILLARY PIPING' ' 0 MW-1 SHALLOW MONITORING WELL I MW-2 DEEP MONITORING WELL MW-11 ABANDONED MONITORING WELL 19 RW-15 RECOVERY WELL 0 PZ-1 PIEZOMETER ® PIG -SIGNAL GROUNDWATER POTENTIOMETRIC CONTOUR (FT. MSL) (DASHED WHERE INFERRED) x 710.92 GROUNDWATER ELEVATION (FT. MSL) y ESTIMATED GROUNDWATER FLOW DIRECTION POND SCALE IN FEET 0 40 80 160 WELL DESIGNATION UPDATE FORMER WELL NAME NEW WELL NAME MW-1 MW-1 MW-2 ABANDONED MW-2D MW-2 MW-3 MW-3 MW-4 MW-4 MW-5 MW-5 MW-6 MW-6 MW-6D MW-7 MW-7 ABANDONED - MW-8 MW-8 MW-9D MW-9 MW-10D MW-10 MW-11 ABANDONED MW-11 MW-12D MW-12 MW-13 MW-13 MW-14 ABANDONED MW-15 ABANDONED MW-16 ABANDONED MW-17 MW-14 MW-17D RECOVERY WELL MW-15 CROWE WELL MW-16 TR-1U MW-17 TR-11) MW-18 TR-2U MW-19 TR-2D MW-20 THE MW-21 TR-31) MW-22 NOTES: 1. ANCILLARY PIPING AND COLONIAL PIPELINE LOCATIONS ARE APPROXIMATE AND ARE FOR FIGURE PURPOSES ONLY. 2. MAP BASED OFF DRAWING ENTITLED "FACILITY MAP" DATED APRIL 1, 2014 COMPLETED BY PROGRESSIVE ENGINEERING AND CONSTRUCTION, INC. GROUNDWATER POTENTIOMETRIC SURFACE MAP SURFICIAL SAPROLITE UNIT - AUGUST 16, 2018 COLONIAL PIPELINE COMPANY KANNAPOLIS BOOSTER STATION CONCORD, NORTH CAROLINA APEX FIGURE 4 DUKE POWER COMPANY IIII ' I I 1 �x x-x-x� I I1 1 1 I MW-4 1 1qv x Q MW-230.50 � 1 x 1 Ix ASPHALT PAYED I 1 m -' 1 By-1 1 SUB STATION o B 1 " � MW-24 I zLINE v 2.0 MANIFOLD 1 3 B\ 1 n I BS-3 E? - x m BV-3 (SVE- NW 1 G7 I MW-5 1 24" CMP o I _ LINE 1 - - - - - MANIFOLD x 1 1 Mw-, I M W-6<0.50 x 1 1 I 1 1 x I MW-1 I 1 Ix MW-12 1 LINE 1 RETENTION POND Pic SIGNAL x POTABLE WATER Q, 1 SUPPLY WELL MW IPZ- D.Zf� i -14 iMW-14 Mw-15 �� X (RW-15) _ 1 PRJ NO. CPC18012.001 ISOCONCENTRATION MAP AUGUST 2018 I COLONIAL PIPELINE COMPANY KANNAPOLIS BOOSTER STATION CONCORD, NORTH CAROLINA LEGEND - - PROPERTY LINE x FENCE LINE G COLONIAL PIPELINE' ANCILLARY PIPING' 0 MW-1 SHALLOW MONITORING WELL MW-2 DEEP MONITORING WELL MW-11 ABANDONED MONITORING WELL * RW-1 RECOVERY WELL O PZ-1 PIEZOMETER 0 PIG -SIGNAL ® BV-1 BIO-VENTING WELL BS-1 BIO-SPARGE WELL !'1 — BENZENE ISOCONTOUR (DASHED WHERE INFERRED) 2.0 BENZENE CONCENTRATION (ug/L) 2B STANDARD FOR BENZENE IS 1.19 MICROGRAM PER LITER (ug/L) 2L STANDARD FOR BENZENE IS 1 ug/L <0.50 BENZENE NOT DETECTED AT OR ABOVE REPORTING LIMIT 111 SCALE IN FEET 0 40 80 160 WELL DESIGNATION UPDATE FORMER WELL NAME NEW WELL NAME MW-1 MW-1 MW-2 ABANDONED MW-2D MW-2 MW-3 MW-3 MW-4 MW-4 MW-5 MW-5 MW-6 MW-6 MW-6D MW-7 MW-7 ABANDONED MW-8 MW-8 MW-9D MW-9 MW-10D MW-10 MW-11 ABANDONED MW-11 MW-12D MW-12 MW-13 MW-13 MW-14 ABANDONED - MW-15 ABANDONED - MW-16 ABANDONED MW-17 MW-14 MW-17D RECOVERY WELL MW-15 CROWE WELL MW-16 TR-1U MW-17 TR-1D MW-18 TR-2U MW-19 TR-2D MW-20 TR-3U MW-21 TR-3D MW-22 NOTES: 1. ANCILLARY PIPING AND COLONIAL PIPELINE LOCATIONS ARE APPROXIMATE AND ARE FOR FIGURE PURPOSES ONLY. 2. MAP BASED OFF DRAWING ENTITLED "FACILITY MAP" DATED APRIL 1, 2014 COMPLETED BY PROGRESSIVE ENGINEERING AND CONSTRUCTION, INC. FIGURE 5 APEX 1 r - ;y i t F'�• � w Well Wilkinson Well • *McNaulty Wel . *Rhodes Well � (, 1,000 FT SITE � � �' • a��'� � ' BUFFERS"�i�,;• ,l• T a Ik V,7�- �• "d I SITE BOUNDARY I v ��� •Y �1 _J►...% O� i lui. T-Watts .. Well .� •. .. / I / - .. .... r �I K�. �1 a��aYe.jrr r A A. •,"r - �' NC OneMap, NC Center for Geographic Information and Analysis, NC 911 Board DATA SOURCE: CABARRUS COUNTY GIS AND MAPPING; AERIAL PHOTOGRAPHY DATED 2015. CHECK BY: AS FIGURE N DRAWN BY: SP SITE BOUNDARY PRIVATE SUPPLY WELLS DATE: 9/6/18 WATER SUPPLY WELL LOCATION MAP 1,000 FT BUFFER :i WELLS WITH POINT OF ENTRY (POE) SYSTEMS 0 250 500 SCALE: AS SHOWN PARCELS SURFACE WATER Feet CAD NO.: CPC18012.001 COLONIAL PIPELINE COMPANY KANNAPOLIS BOOSTER STATION APEX 6 PRJ NO.: CPC18012.001 CONCORD, NORTH CAROLINA GROUNDWATER SAMPLING FIELD LOGS �1 APEX ' N 9 2 Fo- 1 E Is 7 a O • � a a m E N a o z5t ' R v Z c v _ na E E v U ° 2 E s N 3 m a p U a `o ° J v E O o 3 a' a' ~O z o FF E u E w a OO �-E m � � �_ Y z K z z +` Cc P! Ii6 �- U$ ma n r er" e d E_ s E l E u O,E 0 ov o nCj�n N \E N 6(( O V)Y�i > Ci E g n E c_ 16 v x m ❑ Q w £�❑ gi �2 ❑ ❑ �i � 2i °� J U Fb- :i; 6 j ti x c° c N 5 3 Z N Tvi Y a U d � d y E h n m n � m N 3 a 0 O U0 J z a. J J u W LL N 0 w oa v3 wo C z O N 0 c 0 ° 1/ �. N c S\ ° ° O - N v > ° m - N m m m > a J d E O o E ui c � m m 10 N m U ~ m 6 C W U E m = E E ° U z Osi- } N U y C U Lzz} ° ° N O n 0 U U E > 3 � m J E E U d m r= a O � d N �p U D (� U f r.; S^ E E o o - m o o o>a J Ot c N m D 0 �1 N iV N D d 0 O J a J J wIL Z y OLU U IL O 2 o � c 2 O o r D 0 0 0 U 0 N 0 C N � (n N C N E E N w N N 6 N p. z c y ¢ 0 3 0 m ¢ 3 E L6 c u E O fn c0i n a�i Oy t � U � ry t m � N C `p •• T N o J E O o O J y N U N ry N (n N '2) w — — x E m F \ J c o z ¢ cc a z {� a c� 1n o Niu J O v_ o o `y a J N > a ¢ U U U= m o m— d d m EL 3 o. 0. M 0 cf7 c�J 0 N U d A O E u v ti F a , �) 3 d p p � tUC D IL O OI R Q C N ' O0ci .. N00`. I Al a iE D Co �v Id W o o o d E iE a° L N U�1 N i6 c O z 0 O J J Z J J wa Q N Ow U a 'zz Q� O. x u O c U, � o a ^ -La w > .°° N y N o O ri n o a N a g iL aci w t = w o m m a m m c o a ot o c s E O o a E 3 a a O z N 3 U " c nr 'J a � E m O o � 5 s lnvl Z K� Z Z &� ;" v �? N O N N N ON©� O C( to V C N O O O J d E o ° m c M LL 'S m 's a o m OU m 4 J F ° � go d m n n '9 ci 0: a N X 40 c o a m C sA a a � N U N 'o ro N a N a1 Z m c N O. ja N O V 0 \U � a m (j C O j an d Cn = 6 W V E o a a � Z j 1 o F- a a °- m •.¢\; � z Z Z \� aj E a ° N(?�: l °' c 0 0 0 0 -6 �Ej 9 3 a �r E u v r t J o ° ° -0t A.LL? ° a an 0 d O ✓ N �..y, T J N r� .� ro ° N O E r c UU m m R Q N. z G7- a cC N y[Rf a _ x y IL C j 2i « O N � cG IL IO 0 °= a° o m ° E m c '� 8 p m c d -'C m a o o o c o o N U m .N p ° v r r `m ¢ a" w d a°i o a m m E F .z W r O v � N V � D 0 .0 tll c 00 U o N N E d E L a c ¢ W t m m m Y Z c E 3 m m a m 3 $ L6 o v E C N U a m NLi❑ U L T E c m E O o C7 y U d 3 3 a a O z U w ` o ~ <i i J E U ❑ U� m � � E d -+ z z° N > \ E o U E �J a �kI ow L o s = O 3 o a m d a nn, '4 a U U U - E Od N m c a U M ELm d a o �.- 3 E vu 2 d 3 a �+ J m 0 `o A a° m t E m o ❑ E c « d E N w e a o o a m U m a .N L L❑ c m ❑ ¢ 0 d a d d r, S U ❑ ❑ 1- �i �i 2i 0 w a -9• .11 El i�p *a� w m S. N N s a` U a L9 T L N _ a 0 U z L 3 Ul Y FS d U � � � N o m E N m m v- d Fa 3 a a U 2 O FNN p C c 0 U O E S9 � U w d a a m iL N E. J D 6 a O c y E O ' a' n zl b IIII c c� E ❑ m = E, t4i In n r� — L F TL N Q p C h. Q 6- y 3 m t 2 , U C 9 J m Y o g d u C c c ."J c� a° ° m p E '� c ❑ : m n a e a`vi m m o m m d F E c U ❑ Q J (J C ❑ ❑ I- �i _S 2i $I N m m APPENDIX B LABORATORY ANALYTICAL REPORTS �1 APEX SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis Apex Companies, LLC 10610 Metromont Parkway Suite 206 Charlotte, NC 28269 Attention: Andrew Street Project Name: CPC Kannapolis Project Number: CPC18012 Lot Number:TH17080 Date Completed:08/31/2018 Revision Date: 08/31 /2018 08/31/2018 4:42 PM Approved and released by: Project Manager: Lucas Odom PCCRFp d / AM AC CF ED I T E D 11900 eLAa The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 1 of 49 SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative Apex Companies, LLC Lot Number: TH17080 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below. If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page. EPH The method blank associated with prep batch 81720 failed OTP low. The following samples were affected: TH17080-005, TH17080-006, TH17080-007, TH17080-008. The samples were re -extracted with a passing Method blank. TH17080-005, TH17080-006, TH17080-008 all failed 1-Chloro-octadecane in both Run 1 and Run 2 due to matrix interference. Due to the need for fractionation of the samples Run 2 has been reported SVOCs by GC/MS The following samples were diluted due to the nature of the sample matrix: TH17080-005, TH17080-006, TH17080-008. The LOQ has been elevated to reflect the dilution. Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 2 of 49 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary Apex Companies, LLC Lot Number: TH17080 Sample Number Sample ID Matrix Date Sampled Date Received 001 MW-4 Aqueous 08/16/20181010 08/17/2018 002 MW-6 Aqueous 08/16/20181235 08/17/2018 003 MW-8 Aqueous 08/16/20181300 08/17/2018 004 MW-13 Aqueous 08/16/20181320 08/17/2018 005 MW-24 Aqueous 08/16/20181220 08/17/2018 006 MW-25 Aqueous 08/16/20181040 08/17/2018 007 MW-25D Aqueous 08/16/20181110 08/17/2018 008 DUP-1 Aqueous 08/16/2018 08/17/2018 009 EB-1 Aqueous 08/16/20181155 08/17/2018 010 TB Aqueous 08/16/20181010 08/17/2018 (10 samples) Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 3 of 49 SHEALY ENVIRONMENTAL SERVICES, INC. Detection Summary Apex Companies, LLC Lot Number: TH17080 Sample Sample ID Matrix Parameter Method Result Q Units Page 003 MW-8 Aqueous Methyl tertiary butyl ether SM 6200B- 6.6 ug/L 9 004 MW-13 Aqueous Benzene SM 6200B- 5.2 ug/L 10 004 MW-13 Aqueous Methyl tertiary butyl ether SM 6200B- 2.5 ug/L 10 005 MW-24 Aqueous Benzene SM 6200B- 2.0 ug/L 11 005 MW-24 Aqueous Ethylbenzene SM 6200B- 1.8 ug/L 11 005 MW-24 Aqueous Toluene SM 6200B- 0.64 ug/L 11 005 MW-24 Aqueous Xylenes (total) SM 6200B- 1.2 ug/L 11 005 MW-24 Aqueous Acenaphthene 625.1 5.7 J ug/L 11 005 MW-24 Aqueous Anthracene 625.1 2.2 J ug/L 11 005 MW-24 Aqueous Fluoranthene 625.1 4.1 J ug/L 12 005 MW-24 Aqueous Phenanthrene 625.1 2.1 J ug/L 12 005 MW-24 Aqueous Pyrene 625.1 3.1 J ug/L 12 005 MW-24 Aqueous C11 - C22 Aromatics MADEP-EPH- 130 ug/L 13 005 MW-24 Aqueous C5 - C8 Aliphatics MADEP-VPH- 740 ug/L 13 005 MW-24 Aqueous C9 - C12 Aliphatics MADEP-VPH- 410 ug/L 13 005 MW-24 Aqueous C9 - C10 Aromatics MADEP-VPH- 330 ug/L 14 006 MW-25 Aqueous Pyrene 625.1 0.51 J ug/L 16 008 DUP-1 Aqueous Benzene SM 6200B- 1.8 ug/L 23 008 DUP-1 Aqueous Ethylbenzene SM 6200B- 1.9 ug/L 23 008 DUP-1 Aqueous Toluene SM 6200B- 0.61 ug/L 23 008 DUP-1 Aqueous Xylenes (total) SM 6200B- 1.1 ug/L 23 008 DUP-1 Aqueous Acenaphthene 625.1 5.9 J ug/L 23 008 DUP-1 Aqueous Anthracene 625.1 2.1 J ug/L 23 008 DUP-1 Aqueous Fluoranthene 625.1 3.7 J ug/L 24 008 DUP-1 Aqueous Phenanthrene 625.1 1.9 J ug/L 24 008 DUP-1 Aqueous Pyrene 625.1 2.8 J ug/L 24 008 DUP-1 Aqueous C11 - C22 Aromatics MADEP-EPH- 110 ug/L 25 008 DUP-1 Aqueous C5 - C8 Aliphatics MADEP-VPH- 700 ug/L 25 008 DUP-1 Aqueous C9 - C12 Aliphatics MADEP-VPH- 340 ug/L 25 008 DUP-1 Aqueous C9 - C10 Aromatics MADEP-VPH- 360 ug/L 26 (30 detections) Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 4 of 49 Client:Apex Companies, LLC Laboratory ID:TH17080-001 Description: MW-4 Matrix: Aqueous Date Sampled:08/16/2018 1010 Date Received:08/17/2018 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 SM 620013- SM 620OB-2011 1 08/29/2018 1238 JM1 82272 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Benzene 71-43-2 SM 6200B- ND 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 SM 6200B- ND 0.50 0.40 ug/L 1 Methyl tertiary butyl ether (MTBE) 1634-04-4 SM 6200B- ND 0.50 0.40 ug/L 1 Toluene 108-88-3 SM 6200B- ND 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 SM 6200B- ND 0.50 0.40 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 102 70-130 1,2-Dichloroethane-d4 100 70-130 Toluene-d8 106 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 5 of 49 Client:Apex Companies, LLC Laboratory ID:TH17080-002 Description: MW-6 Matrix: Aqueous Date Sampled:08/16/2018 1235 Date Received:08/17/2018 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 SM 620013- SM 620OB-2011 1 08/29/2018 1300 JM1 82272 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Benzene 71-43-2 SM 6200B- ND 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 SM 6200B- ND 0.50 0.40 ug/L 1 Methyl tertiary butyl ether (MTBE) 1634-04-4 SM 6200B- ND 0.50 0.40 ug/L 1 Toluene 108-88-3 SM 6200B- ND 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 SM 6200B- ND 0.50 0.40 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 103 70-130 1,2-Dichloroethane-d4 101 70-130 Toluene-d8 107 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 6 of 49 Client:Apex Companies, LLC Laboratory ID:TH17080-003 Description: MW-8 Matrix: Aqueous Date Sampled:08/16/2018 1300 Date Received:08/17/2018 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 SM 620013- SM 620OB-2011 1 08/29/2018 1322 JM1 82272 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Benzene 71-43-2 SM 6200B- ND 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 SM 6200B- ND 0.50 0.40 ug/L 1 Methyl tertiary butyl ether (MTBE) 1634-04-4 SM 6200B- 6.6 0.50 0.40 ug/L 1 Toluene 108-88-3 SM 6200B- ND 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 SM 6200B- ND 0.50 0.40 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 105 70-130 1,2-Dichloroethane-d4 103 70-130 Toluene-d8 108 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 7 of 49 Client:Apex Companies, LLC Laboratory ID:TH17080-004 Description: MW-13 Matrix: Aqueous Date Sampled:08/16/2018 1320 Date Received:08/17/2018 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 SM 620013- SM 620OB-2011 1 08/29/2018 1640 JM1 82272 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Benzene 71-43-2 SM 6200B- 5.2 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 SM 620013- ND 0.50 0.40 ug/L 1 Methyl tertiary butyl ether (MTBE) 1634-04-4 SM 6200113- 2.5 0.50 0.40 ug/L 1 Toluene 108-88-3 SM 620013- ND 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 SM 620013- ND 0.50 0.40 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 103 70-130 1,2-Dichloroethane-d4 103 70-130 Toluene-d8 107 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 8 of 49 Client:Apex Companies, LLC Laboratory ID:TH17080-005 Description: MW-24 Matrix: Aqueous Date Sampled:08/16/2018 1220 Date Received:08/17/2018 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 SM 620013- SM 620OB-2011 1 08/29/2018 1702 JM1 82272 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Benzene 71-43-2 SM 6200B- 2.0 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 SM 620013- 1.8 0.50 0.40 ug/L 1 Toluene 108-88-3 SM 6200113- 0.64 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 SM 6200113- 1.2 0.50 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 105 70-130 1,2-Dichloroethane-d4 105 70-130 Toluene-d8 106 70-130 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 10 08/29/20181853 CMP2 08/20/20181841 81238 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acenaphthene 83-32-9 625.1 5.7 J 16 1.1 ug/L 1 Acenaphthylene 208-96-8 625.1 ND 16 0.60 ug/L 1 Anthracene 120-12-7 625.1 2.2 J 16 0.60 ug/L 1 Benzo(a)anthracene 56-55-3 625.1 ND 16 0.70 ug/L 1 Benzo(a)pyrene 50-32-8 625.1 ND 16 0.40 ug/L 1 Benzo(b)fluoranthene 205-99-2 625.1 ND 16 0.50 ug/L 1 Benzo(g,h,i)perylene 191-24-2 625.1 ND 16 1.2 ug/L 1 Benzo(k)fluoranthene 207-08-9 625.1 ND 16 0.70 ug/L 1 Benzyl alcohol 100-51-6 625.1 ND 32 20 ug/L 1 4-Bromophenyl phenyl ether 101-55-3 625.1 ND 16 1.6 ug/L 1 Butyl benzyl phthalate 85-68-7 625.1 ND 16 1.5 ug/L 1 bis (2-Chloro-1-methylethyl) ether 108-60-1 625.1 ND 16 4.9 ug/L 1 4-Chloro-3-methyl phenol 59-50-7 625.1 ND 16 4.0 ug/L 1 bis(2-Chloroethoxy)methane 111-91-1 625.1 ND 16 4.8 ug/L 1 bis(2-Chloroethyl)ether 111-44-4 625.1 ND 16 5.0 ug/L 1 2-Chloronaphthalene 91-58-7 625.1 ND 16 4.0 ug/L 1 2-Chlorophenol 95-57-8 625.1 ND 16 3.4 ug/L 1 4-Chlorophenyl phenyl ether 7005-72-3 625.1 ND 16 2.1 ug/L 1 Chrysene 218-01-9 625.1 ND 16 0.50 ug/L 1 Dibenzo(a,h)anthracene 53-70-3 625.1 ND 16 1.1 ug/L 1 Dibenzofuran 132-64-9 625.1 ND 16 10 ug/L 1 1,2-Dichlorobenzene 95-50-1 625.1 ND 16 4.6 ug/L 1 1,3-Dichlorobenzene 541-73-1 625.1 ND 16 4.0 ug/L 1 1,4-Dichlorobenzene 106-46-7 625.1 ND 16 4.1 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 9 of 49 Client:Apex Companies, LLC Laboratory ID:TH17080-005 Description: MW-24 Matrix: Aqueous Date Sampled:08/16/2018 1220 Date Received:08/17/2018 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 10 08/29/20181853 CMP2 08/20/20181841 81238 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 3,3'-Dichlorobenzidine 91-94-1 625.1 ND 80 16 ug/L 2,4-Dichlorophenol 120-83-2 625.1 ND 16 7.0 ug/L Diethylphthalate 84-66-2 625.1 ND 16 1.9 ug/L Dimethyl phthalate 131-11-3 625.1 ND 16 2.1 ug/L 2,4-Dimethylphenol 105-67-9 625.1 ND 16 6.2 ug/L Di-n-butyl phthalate 84-74-2 625.1 ND 16 2.6 ug/L 4,6-Dinitro-2-methylphenol 534-52-1 625.1 ND 80 6.9 ug/L 2,4-Dinitrophenol 51-28-5 625.1 ND 80 6.5 ug/L Di-n-octylphthalate 117-84-0 625.1 ND 16 0.70 ug/L 1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625.1 ND 16 1.2 ug/L bis(2-Ethylhexyl)phthalate 117-81-7 625.1 ND 80 1.9 ug/L Fluoranthene 206-44-0 625.1 4.1 J 16 0.50 ug/L Fluorene 86-73-7 625.1 ND 16 0.60 ug/L Hexachlorobenzene 118-74-1 625.1 ND 16 3.9 ug/L Hexachlorobutadiene 87-68-3 625.1 ND 16 4.7 ug/L Hexachlorocyclopentadiene 77-47-4 625.1 ND 80 1.4 ug/L Hexachloroethane 67-72-1 625.1 ND 16 5.3 ug/L Indeno(1,2,3-c,d)pyrene 193-39-5 625.1 ND 16 1.1 ug/L Isophorone 78-59-1 625.1 ND 16 4.4 ug/L 1-Methylnaphthalene 90-12-0 625.1 ND 16 4.0 ug/L 2-Methylnaphthalene 91-57-6 625.1 ND 16 4.0 ug/L 2-Methylphenol 95-48-7 625.1 ND 16 6.7 ug/L 3+4-Methylphenol 106-44-5 625.1 ND 16 15 ug/L Naphthalene 91-20-3 625.1 ND 16 1.3 ug/L Nitrobenzene 98-95-3 625.1 ND 16 11 ug/L 2-Nitrophenol 88-75-5 625.1 ND 32 8.8 ug/L 4-Nitrophenol 100-02-7 625.1 ND 80 12 ug/L N-Nitrosodi-n-propylamine 621-64-7 625.1 ND 16 1.5 ug/L N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 625.1 ND 16 2.5 ug/L Pentachlorophenol 87-86-5 625.1 ND 80 14 ug/L Phenanthrene 85-01-8 625.1 2.1 J 16 1.2 ug/L Phenol 108-95-2 625.1 ND 16 2.2 ug/L Pyrene 129-00-0 625.1 3.1 J 16 0.60 ug/L 1,2,4-Trichlorobenzene 120-82-1 625.1 ND 16 5.7 ug/L 2,4,6-Trichlorophenol 88-06-2 625.1 ND 16 4.4 ug/L LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 10 of 49 Client:Apex Companies, LLC Laboratory ID:TH17080-005 Description: MW-24 Matrix: Aqueous Date Sampled:08/16/2018 1220 Date Received:08/17/2018 Run 1 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 60 37-129 2-Fluorophenol 57 24-127 Nitrobenzene-d5 76 38-127 Phenol-d5 54 28-128 Terphenyl-d14 98 10-148 2,4,6-Tribromophenol 72 41-144 MADEP EPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 MADEP-EPH- MADEP-EPH-04 1 08/28/2018 2151 CHG 08/23/2018 1850 81720 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C9 - C18 Aliphatics MADEP-EPH-04 ND 100 100 ug/L 2 C19 - C36 Aliphatics MADEP-EPH-04 ND 100 100 ug/L 2 Run 2 Acceptance Surrogate Q % Recovery Limits 1-Chloro-octadecane (aliphatic) N 18 40-140 MADEP EPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 MADEP-EPH- MADEP-EPH-04 1 08/28/2018 2221 CHG 08/23/2018 1850 81721 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C11 - C22 Aromatics MADEP-EPH- 130 100 100 ug/L 2 Run 2 Acceptance Surrogate Q % Recovery Limits o - Terphenyl (aromatic) 45 40-140 2-Fluorobiphenyl (fractionation 1) 76 40-140 2-Bromonaphthalene (fractionation 2) 51 40-140 MADEP VPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 08/22/20181848 JJG 81530 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C5 - C8 Aliphatics MADEP-VPH- 740 75 15 ug/L 1 C9 - C12 Aliphatics MADEP-VPH- 410 75 15 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 11 of 49 Client:Apex Companies, LLC Laboratory ID:TH17080-005 Description: MW-24 Matrix: Aqueous Date Sampled:08/16/2018 1220 Date Received:08/17/2018 Run 1 Acceptance Surrogate Q % Recovery Limits 2,5-Dibromotoluene (FID) 74 70-130 MADEP VPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 08/22/20181848 JJG 81529 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C9 - C10 Aromatics MADEP-VPH- 330 25 5.0 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2,5-Dibromotoluene (PID) 84 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 12 of 49 Client:Apex Companies, LLC Laboratory ID:TH17080-006 Description: MW-25 Matrix: Aqueous Date Sampled:08/16/2018 1040 Date Received:08/17/2018 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 SM 620013- SM 620OB-2011 1 08/29/2018 1344 JM1 82272 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Benzene 71-43-2 SM 6200B- ND 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 SM 6200B- ND 0.50 0.40 ug/L 1 Toluene 108-88-3 SM 6200B- ND 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 SM 6200B- ND 0.50 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 104 70-130 1,2-Dichloroethane-d4 104 70-130 Toluene-d8 108 70-130 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 5 08/29/20181918 CMP2 08/20/20181841 81238 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acenaphthene 83-32-9 625.1 ND 8.0 0.55 ug/L 1 Acenaphthylene 208-96-8 625.1 ND 8.0 0.30 ug/L 1 Anthracene 120-12-7 625.1 ND 8.0 0.30 ug/L 1 Benzo(a)anthracene 56-55-3 625.1 ND 8.0 0.35 ug/L 1 Benzo(a)pyrene 50-32-8 625.1 ND 8.0 0.20 ug/L 1 Benzo(b)fluoranthene 205-99-2 625.1 ND 8.0 0.25 ug/L 1 Benzo(g,h,i)perylene 191-24-2 625.1 ND 8.0 0.60 ug/L 1 Benzo(k)fluoranthene 207-08-9 625.1 ND 8.0 0.35 ug/L 1 Benzyl alcohol 100-51-6 625.1 ND 16 10 ug/L 1 4-Bromophenyl phenyl ether 101-55-3 625.1 ND 8.0 0.80 ug/L 1 Butyl benzyl phthalate 85-68-7 625.1 ND 8.0 0.75 ug/L 1 bis (2-Chloro-1-methylethyl) ether 108-60-1 625.1 ND 8.0 2.5 ug/L 1 4-Chloro-3-methyl phenol 59-50-7 625.1 ND 8.0 2.0 ug/L 1 bis(2-Chloroethoxy)methane 111-91-1 625.1 ND 8.0 2.4 ug/L 1 bis(2-Chloroethyl)ether 111-44-4 625.1 ND 8.0 2.5 ug/L 1 2-Chloronaphthalene 91-58-7 625.1 ND 8.0 2.0 ug/L 1 2-Chlorophenol 95-57-8 625.1 ND 8.0 1.7 ug/L 1 4-Chlorophenyl phenyl ether 7005-72-3 625.1 ND 8.0 1.1 ug/L 1 Chrysene 218-01-9 625.1 ND 8.0 0.25 ug/L 1 Dibenzo(a,h)anthracene 53-70-3 625.1 ND 8.0 0.55 ug/L 1 Dibenzofuran 132-64-9 625.1 ND 8.0 5.0 ug/L 1 1,2-Dichlorobenzene 95-50-1 625.1 ND 8.0 2.3 ug/L 1 1,3-Dichlorobenzene 541-73-1 625.1 ND 8.0 2.0 ug/L 1 1,4-Dichlorobenzene 106-46-7 625.1 ND 8.0 2.1 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 13 of 49 Client:Apex Companies, LLC Laboratory ID:TH17080-006 Description: MW-25 Matrix: Aqueous Date Sampled:08/16/2018 1040 Date Received:08/17/2018 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 5 08/29/20181918 CMP2 08/20/20181841 81238 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 3,3'-Dichlorobenzidine 91-94-1 625.1 ND 40 8.0 ug/L 2,4-Dichlorophenol 120-83-2 625.1 ND 8.0 3.5 ug/L Diethylphthalate 84-66-2 625.1 ND 8.0 0.95 ug/L Dimethyl phthalate 131-11-3 625.1 ND 8.0 1.1 ug/L 2,4-Dimethylphenol 105-67-9 625.1 ND 8.0 3.1 ug/L Di-n-butyl phthalate 84-74-2 625.1 ND 8.0 1.3 ug/L 4,6-Dinitro-2-methylphenol 534-52-1 625.1 ND 40 3.5 ug/L 2,4-Dinitrophenol 51-28-5 625.1 ND 40 3.3 ug/L Di-n-octylphthalate 117-84-0 625.1 ND 8.0 0.35 ug/L 1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625.1 ND 8.0 0.60 ug/L bis(2-Ethylhexyl)phthalate 117-81-7 625.1 ND 40 0.95 ug/L Fluoranthene 206-44-0 625.1 ND 8.0 0.25 ug/L Fluorene 86-73-7 625.1 ND 8.0 0.30 ug/L Hexachlorobenzene 118-74-1 625.1 ND 8.0 2.0 ug/L Hexachlorobutadiene 87-68-3 625.1 ND 8.0 2.3 ug/L Hexachlorocyclopentadiene 77-47-4 625.1 ND 40 0.70 ug/L Hexachloroethane 67-72-1 625.1 ND 8.0 2.7 ug/L Indeno(1,2,3-c,d)pyrene 193-39-5 625.1 ND 8.0 0.55 ug/L Isophorone 78-59-1 625.1 ND 8.0 2.2 ug/L 1-Methylnaphthalene 90-12-0 625.1 ND 8.0 2.0 ug/L 2-Methylnaphthalene 91-57-6 625.1 ND 8.0 2.0 ug/L 2-Methylphenol 95-48-7 625.1 ND 8.0 3.4 ug/L 3+4-Methylphenol 106-44-5 625.1 ND 8.0 7.5 ug/L Naphthalene 91-20-3 625.1 ND 8.0 0.65 ug/L Nitrobenzene 98-95-3 625.1 ND 8.0 5.5 ug/L 2-Nitrophenol 88-75-5 625.1 ND 16 4.4 ug/L 4-Nitrophenol 100-02-7 625.1 ND 40 6.0 ug/L N-Nitrosodi-n-propylamine 621-64-7 625.1 ND 8.0 0.75 ug/L N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 625.1 ND 8.0 1.3 ug/L Pentachlorophenol 87-86-5 625.1 ND 40 7.0 ug/L Phenanthrene 85-01-8 625.1 ND 8.0 0.60 ug/L Phenol 108-95-2 625.1 ND 8.0 1.1 ug/L Pyrene 129-00-0 625.1 0.51 J 8.0 0.30 ug/L 1,2,4-Trichlorobenzene 120-82-1 625.1 ND 8.0 2.8 ug/L 2,4,6-Trichlorophenol 88-06-2 625.1 ND 8.0 2.2 ug/L LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 14 of 49 Client:Apex Companies, LLC Laboratory ID:TH17080-006 Description: MW-25 Matrix: Aqueous Date Sampled:08/16/2018 1040 Date Received:08/17/2018 Run 1 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 47 37-129 2-Fluorophenol 49 24-127 Nitrobenzene-d5 60 38-127 Phenol-d5 48 28-128 Terphenyl-d14 86 10-148 2,4,6-Tribromophenol 54 41-144 MADEP EPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 MADEP-EPH- MADEP-EPH-04 1 08/25/2018 0312 CHG 08/23/2018 1850 81720 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C9 - C18 Aliphatics MADEP-EPH-04 ND 100 100 ug/L 2 C19 - C36 Aliphatics MADEP-EPH-04 ND 100 100 ug/L 2 Run 2 Acceptance Surrogate Q % Recovery Limits 1-Chloro-octadecane (aliphatic) N 21 40-140 MADEP EPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 MADEP-EPH- MADEP-EPH-04 1 08/25/2018 0635 CHG 08/23/2018 1850 81721 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C11 - C22 Aromatics MADEP-EPH-04 ND 100 100 ug/L 2 Run 2 Acceptance Surrogate Q % Recovery Limits o - Terphenyl (aromatic) 64 40-140 2-Fluorobiphenyl (fractionation 1) 94 40-140 2-Bromonaphthalene (fractionation 2) 63 40-140 MADEP VPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 08/22/20181916 JJG 81530 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C5 - C8 Aliphatics MADEP-VPH- ND 75 15 ug/L 1 C9 - C12 Aliphatics MADEP-VPH- ND 75 15 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 15 of 49 Client:Apex Companies, LLC Laboratory ID:TH17080-006 Description: MW-25 Matrix: Aqueous Date Sampled:08/16/2018 1040 Date Received:08/17/2018 Run 1 Acceptance Surrogate Q % Recovery Limits 2,5-Dibromotoluene (FID) 110 70-130 MADEP VPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 08/22/20181916 JJG 81529 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C9 - C10 Aromatics MADEP-VPH- ND 25 5.0 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2,5-Dibromotoluene (PID) 110 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 16 of 49 Client:Apex Companies, LLC Laboratory ID:TH17080-007 Description: MW-25D Matrix: Aqueous Date Sampled:08/16/2018 1110 Date Received:08/17/2018 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 SM 620013- SM 620OB-2011 1 08/29/2018 1406 JM1 82272 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Benzene 71-43-2 SM 6200B- ND 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 SM 6200B- ND 0.50 0.40 ug/L 1 Toluene 108-88-3 SM 6200B- ND 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 SM 6200B- ND 0.50 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 105 70-130 1,2-Dichloroethane-d4 105 70-130 Toluene-d8 110 70-130 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 1 08/29/20181943 CMP2 08/20/20181841 81238 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acenaphthene 83-32-9 625.1 ND 1.6 0.11 ug/L 1 Acenaphthylene 208-96-8 625.1 ND 1.6 0.060 ug/L 1 Anthracene 120-12-7 625.1 ND 1.6 0.060 ug/L 1 Benzo(a)anthracene 56-55-3 625.1 ND 1.6 0.070 ug/L 1 Benzo(a)pyrene 50-32-8 625.1 ND 1.6 0.040 ug/L 1 Benzo(b)fluoranthene 205-99-2 625.1 ND 1.6 0.050 ug/L 1 Benzo(g,h,i)perylene 191-24-2 625.1 ND 1.6 0.12 ug/L 1 Benzo(k)fluoranthene 207-08-9 625.1 ND 1.6 0.070 ug/L 1 Benzyl alcohol 100-51-6 625.1 ND 3.2 2.0 ug/L 1 4-Bromophenyl phenyl ether 101-55-3 625.1 ND 1.6 0.16 ug/L 1 Butyl benzyl phthalate 85-68-7 625.1 ND 1.6 0.15 ug/L 1 bis (2-Chloro-1-methylethyl) ether 108-60-1 625.1 ND 1.6 0.49 ug/L 1 4-Chloro-3-methyl phenol 59-50-7 625.1 ND 1.6 0.40 ug/L 1 bis(2-Chloroethoxy)methane 111-91-1 625.1 ND 1.6 0.48 ug/L 1 bis(2-Chloroethyl)ether 111-44-4 625.1 ND 1.6 0.50 ug/L 1 2-Chloronaphthalene 91-58-7 625.1 ND 1.6 0.40 ug/L 1 2-Chlorophenol 95-57-8 625.1 ND 1.6 0.34 ug/L 1 4-Chlorophenyl phenyl ether 7005-72-3 625.1 ND 1.6 0.21 ug/L 1 Chrysene 218-01-9 625.1 ND 1.6 0.050 ug/L 1 Dibenzo(a,h)anthracene 53-70-3 625.1 ND 1.6 0.11 ug/L 1 Dibenzofuran 132-64-9 625.1 ND 1.6 1.0 ug/L 1 1,2-Dichlorobenzene 95-50-1 625.1 ND 1.6 0.46 ug/L 1 1,3-Dichlorobenzene 541-73-1 625.1 ND 1.6 0.40 ug/L 1 1,4-Dichlorobenzene 106-46-7 625.1 ND 1.6 0.41 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 17 of 49 Client:Apex Companies, LLC Laboratory ID:TH17080-007 Description: MW-25D Matrix: Aqueous Date Sampled:08/16/2018 1110 Date Received:08/17/2018 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 1 08/29/20181943 CMP2 08/20/20181841 81238 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 3,3'-Dichlorobenzidine 91-94-1 625.1 ND 8.0 1.6 ug/L 2,4-Dichlorophenol 120-83-2 625.1 ND 1.6 0.70 ug/L Diethylphthalate 84-66-2 625.1 ND 1.6 0.19 ug/L Dimethyl phthalate 131-11-3 625.1 ND 1.6 0.21 ug/L 2,4-Dimethylphenol 105-67-9 625.1 ND 1.6 0.62 ug/L Di-n-butyl phthalate 84-74-2 625.1 ND 1.6 0.26 ug/L 4,6-Dinitro-2-methylphenol 534-52-1 625.1 ND 8.0 0.69 ug/L 2,4-Dinitrophenol 51-28-5 625.1 ND 8.0 0.65 ug/L Di-n-octylphthalate 117-84-0 625.1 ND 1.6 0.070 ug/L 1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625.1 ND 1.6 0.12 ug/L bis(2-Ethylhexyl)phthalate 117-81-7 625.1 ND 8.0 0.19 ug/L Fluoranthene 206-44-0 625.1 ND 1.6 0.050 ug/L Fluorene 86-73-7 625.1 ND 1.6 0.060 ug/L Hexachlorobenzene 118-74-1 625.1 ND 1.6 0.39 ug/L Hexachlorobutadiene 87-68-3 625.1 ND 1.6 0.47 ug/L Hexachlorocyclopentadiene 77-47-4 625.1 ND 8.0 0.14 ug/L Hexachloroethane 67-72-1 625.1 ND 1.6 0.53 ug/L Indeno(1,2,3-c,d)pyrene 193-39-5 625.1 ND 1.6 0.11 ug/L Isophorone 78-59-1 625.1 ND 1.6 0.44 ug/L 1-Methylnaphthalene 90-12-0 625.1 ND 1.6 0.40 ug/L 2-Methylnaphthalene 91-57-6 625.1 ND 1.6 0.40 ug/L 2-Methylphenol 95-48-7 625.1 ND 1.6 0.67 ug/L 3+4-Methylphenol 106-44-5 625.1 ND 1.6 1.5 ug/L Naphthalene 91-20-3 625.1 ND 1.6 0.13 ug/L Nitrobenzene 98-95-3 625.1 ND 1.6 1.1 ug/L 2-Nitrophenol 88-75-5 625.1 ND 3.2 0.88 ug/L 4-Nitrophenol 100-02-7 625.1 ND 8.0 1.2 ug/L N-Nitrosodi-n-propylamine 621-64-7 625.1 ND 1.6 0.15 ug/L N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 625.1 ND 1.6 0.25 ug/L Pentachlorophenol 87-86-5 625.1 ND 8.0 1.4 ug/L Phenanthrene 85-01-8 625.1 ND 1.6 0.12 ug/L Phenol 108-95-2 625.1 ND 1.6 0.22 ug/L Pyrene 129-00-0 625.1 ND 1.6 0.060 ug/L 1,2,4-Trichlorobenzene 120-82-1 625.1 ND 1.6 0.57 ug/L 2,4,6-Trichlorophenol 88-06-2 625.1 ND 1.6 0.44 ug/L LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 18 of 49 Client:Apex Companies, LLC Laboratory ID:TH17080-007 Description: MW-25D Matrix: Aqueous Date Sampled:08/16/2018 1110 Date Received:08/17/2018 Run 1 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 55 37-129 2-Fluorophenol 57 24-127 Nitrobenzene-d5 72 38-127 Phenol-d5 59 28-128 Terphenyl-d14 98 10-148 2,4,6-Tribromophenol 71 41-144 MADEP EPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 MADEP-EPH- MADEP-EPH-04 1 08/25/2018 0341 CHG 08/23/2018 1850 81720 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C9 - C18 Aliphatics MADEP-EPH-04 ND 100 100 ug/L 2 C19 - C36 Aliphatics MADEP-EPH-04 ND 100 100 ug/L 2 Run 2 Acceptance Surrogate Q % Recovery Limits 1-Chloro-octadecane (aliphatic) 58 40-140 MADEP EPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 MADEP-EPH- MADEP-EPH-04 1 08/25/2018 0704 CHG 08/23/2018 1850 81721 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C11 - C22 Aromatics MADEP-EPH-04 ND 100 100 ug/L 2 Run 2 Acceptance Surrogate Q % Recovery Limits o - Terphenyl (aromatic) 58 40-140 2-Fluorobiphenyl (fractionation 1) 80 40-140 2-Bromonaphthalene (fractionation 2) 50 40-140 MADEP VPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 08/22/2018 2012 JJG 81530 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C5 - C8 Aliphatics MADEP-VPH- ND 75 15 ug/L 1 C9 - C12 Aliphatics MADEP-VPH- ND 75 15 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 19 of 49 Client:Apex Companies, LLC Laboratory ID:TH17080-007 Description: MW-25D Matrix: Aqueous Date Sampled:08/16/2018 1110 Date Received:08/17/2018 Run 1 Acceptance Surrogate Q % Recovery Limits 2,5-Dibromotoluene (FID) 109 70-130 MADEP VPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 08/22/2018 2012 JJG 81529 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C9 - C10 Aromatics MADEP-VPH- ND 25 5.0 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2,5-Dibromotoluene (PID) 109 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 20 of 49 Client:Apex Companies, LLC Laboratory ID:TH17080-008 Description: DUP-1 Matrix: Aqueous Date Sampled:08/16/2018 Date Received:08/17/2018 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 SM 620013- SM 620OB-2011 1 08/29/2018 1724 JM1 82272 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Benzene 71-43-2 SM 6200113- 1.8 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 SM 6200113- 1.9 0.50 0.40 ug/L 1 Methyl tertiary butyl ether (MTBE) 1634-04-4 SM 620013- ND 0.50 0.40 ug/L 1 Toluene 108-88-3 SM 6200113- 0.61 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 SM 6200113- 1.1 0.50 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 107 70-130 1,2-Dichloroethane-d4 106 70-130 Toluene-d8 109 70-130 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 10 08/29/2018 2008 CMP2 08/20/2018 1841 81238 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acenaphthene 83-32-9 625.1 5.9 J 16 1.1 ug/L 1 Acenaphthylene 208-96-8 625.1 ND 16 0.60 ug/L 1 Anthracene 120-12-7 625.1 2.1 J 16 0.60 ug/L 1 Benzo(a)anthracene 56-55-3 625.1 ND 16 0.70 ug/L 1 Benzo(a)pyrene 50-32-8 625.1 ND 16 0.40 ug/L 1 Benzo(b)fluoranthene 205-99-2 625.1 ND 16 0.50 ug/L 1 Benzo(g,h,i)perylene 191-24-2 625.1 ND 16 1.2 ug/L 1 Benzo(k)fluoranthene 207-08-9 625.1 ND 16 0.70 ug/L 1 Benzyl alcohol 100-51-6 625.1 ND 32 20 ug/L 1 4-Bromophenyl phenyl ether 101-55-3 625.1 ND 16 1.6 ug/L 1 Butyl benzyl phthalate 85-68-7 625.1 ND 16 1.5 ug/L 1 bis (2-Chloro-1-methylethyl) ether 108-60-1 625.1 ND 16 4.9 ug/L 1 4-Chloro-3-methyl phenol 59-50-7 625.1 ND 16 4.0 ug/L 1 bis(2-Chloroethoxy)methane 111-91-1 625.1 ND 16 4.8 ug/L 1 bis(2-Chloroethyl)ether 111-44-4 625.1 ND 16 5.0 ug/L 1 2-Chloronaphthalene 91-58-7 625.1 ND 16 4.0 ug/L 1 2-Chlorophenol 95-57-8 625.1 ND 16 3.4 ug/L 1 4-Chlorophenyl phenyl ether 7005-72-3 625.1 ND 16 2.1 ug/L 1 Chrysene 218-01-9 625.1 ND 16 0.50 ug/L 1 Dibenzo(a,h)anthracene 53-70-3 625.1 ND 16 1.1 ug/L 1 Dibenzofuran 132-64-9 625.1 ND 16 10 ug/L 1 1,2-Dichlorobenzene 95-50-1 625.1 ND 16 4.6 ug/L 1 1,3-Dichlorobenzene 541-73-1 625.1 ND 16 4.0 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 21 of 49 Client:Apex Companies, LLC Laboratory ID:TH17080-008 Description: DUP-1 Matrix: Aqueous Date Sampled:08/16/2018 Date Received:08/17/2018 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 10 08/29/2018 2008 CMP2 08/20/2018 1841 81238 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dichlorobenzene 106-46-7 625.1 ND 16 4.1 ug/L 3,3'-Dichlorobenzidine 91-94-1 625.1 ND 80 16 ug/L 2,4-Dichlorophenol 120-83-2 625.1 ND 16 7.0 ug/L Diethylphthalate 84-66-2 625.1 ND 16 1.9 ug/L Dimethyl phthalate 131-11-3 625.1 ND 16 2.1 ug/L 2,4-Dimethylphenol 105-67-9 625.1 ND 16 6.2 ug/L Di-n-butyl phthalate 84-74-2 625.1 ND 16 2.6 ug/L 4,6-Dinitro-2-methylphenol 534-52-1 625.1 ND 80 6.9 ug/L 2,4-Dinitrophenol 51-28-5 625.1 ND 80 6.5 ug/L Di-n-octylphthalate 117-84-0 625.1 ND 16 0.70 ug/L 1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625.1 ND 16 1.2 ug/L bis(2-Ethylhexyl)phthalate 117-81-7 625.1 ND 80 1.9 ug/L Fluoranthene 206-44-0 625.1 3.7 J 16 0.50 ug/L Fluorene 86-73-7 625.1 ND 16 0.60 ug/L Hexachlorobenzene 118-74-1 625.1 ND 16 3.9 ug/L Hexachlorobutadiene 87-68-3 625.1 ND 16 4.7 ug/L Hexachlorocyclopentadiene 77-47-4 625.1 ND 80 1.4 ug/L Hexachloroethane 67-72-1 625.1 ND 16 5.3 ug/L Indeno(1,2,3-c,d)pyrene 193-39-5 625.1 ND 16 1.1 ug/L Isophorone 78-59-1 625.1 ND 16 4.4 ug/L 1-Methylnaphthalene 90-12-0 625.1 ND 16 4.0 ug/L 2-Methylnaphthalene 91-57-6 625.1 ND 16 4.0 ug/L 2-Methylphenol 95-48-7 625.1 ND 16 6.7 ug/L 3+4-Methylphenol 106-44-5 625.1 ND 16 15 ug/L Naphthalene 91-20-3 625.1 ND 16 1.3 ug/L Nitrobenzene 98-95-3 625.1 ND 16 11 ug/L 2-Nitrophenol 88-75-5 625.1 ND 32 8.8 ug/L 4-Nitrophenol 100-02-7 625.1 ND 80 12 ug/L N-Nitrosodi-n-propylamine 621-64-7 625.1 ND 16 1.5 ug/L N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 625.1 ND 16 2.5 ug/L Pentachlorophenol 87-86-5 625.1 ND 80 14 ug/L Phenanthrene 85-01-8 625.1 1.9 J 16 1.2 ug/L Phenol 108-95-2 625.1 ND 16 2.2 ug/L Pyrene 129-00-0 625.1 2.8 J 16 0.60 ug/L 1,2,4-Trichlorobenzene 120-82-1 625.1 ND 16 5.7 ug/L 2,4,6-Trichlorophenol 88-06-2 625.1 ND 16 4.4 ug/L LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 22 of 49 Client:Apex Companies, LLC Laboratory ID:TH17080-008 Description: DUP-1 Matrix: Aqueous Date Sampled:08/16/2018 Date Received:08/17/2018 Run 1 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 60 37-129 2-Fluorophenol 63 24-127 Nitrobenzene-d5 77 38-127 Phenol-d5 59 28-128 Terphenyl-d14 92 10-148 2,4,6-Tribromophenol 66 41-144 MADEP EPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 MADEP-EPH- MADEP-EPH-04 1 08/25/2018 0410 CHG 08/23/2018 1850 81720 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C9 - C18 Aliphatics MADEP-EPH-04 ND 100 100 ug/L 2 C19 - C36 Aliphatics MADEP-EPH-04 ND 100 100 ug/L 2 Run 2 Acceptance Surrogate Q % Recovery Limits 1-Chloro-octadecane (aliphatic) N 20 40-140 MADEP EPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 MADEP-EPH- MADEP-EPH-04 1 08/25/2018 0733 CHG 08/23/2018 1850 81721 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C11 - C22 Aromatics MADEP-EPH- 110 100 100 ug/L 2 Run 2 Acceptance Surrogate Q % Recovery Limits o - Terphenyl (aromatic) 45 40-140 2-Fluorobiphenyl (fractionation 1) 75 40-140 2-Bromonaphthalene (fractionation 2) 45 40-140 MADEP VPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 08/22/20181944 JJG 81530 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C5 - C8 Aliphatics MADEP-VPH- 700 75 15 ug/L 1 C9 - C12 Aliphatics MADEP-VPH- 340 75 15 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 23 of 49 Client:Apex Companies, LLC Laboratory ID:TH17080-008 Description: DUP-1 Matrix: Aqueous Date Sampled:08/16/2018 Date Received:08/17/2018 Run 1 Acceptance Surrogate Q % Recovery Limits 2,5-Dibromotoluene (FID) 70 70-130 MADEP VPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 08/22/20181944 JJG 81529 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C9 - C10 Aromatics MADEP-VPH- 360 25 5.0 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2,5-Dibromotoluene (PID) 82 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 24 of 49 Client:Apex Companies, LLC Laboratory ID:TH17080-009 Description: EB-1 Matrix: Aqueous Date Sampled:08/16/2018 1155 Date Received:08/17/2018 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 SM 620013- SM 620OB-2011 1 08/29/2018 1027 JM1 82272 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Benzene 71-43-2 SM 6200B- ND 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 SM 6200B- ND 0.50 0.40 ug/L 1 Methyl tertiary butyl ether (MTBE) 1634-04-4 SM 6200B- ND 0.50 0.40 ug/L 1 Toluene 108-88-3 SM 6200B- ND 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 SM 6200B- ND 0.50 0.40 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 105 70-130 1,2-Dichloroethane-d4 101 70-130 Toluene-d8 109 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 25 of 49 Client:Apex Companies, LLC Laboratory ID:TH17080-010 Description: TB Matrix: Aqueous Date Sampled:08/16/2018 1010 Date Received:08/17/2018 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 SM 620013- SM 620OB-2011 1 08/29/2018 1049 JM1 82272 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Benzene 71-43-2 SM 6200B- ND 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 SM 6200B- ND 0.50 0.40 ug/L 1 Methyl tertiary butyl ether (MTBE) 1634-04-4 SM 6200B- ND 0.50 0.40 ug/L 1 Toluene 108-88-3 SM 6200B- ND 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 SM 6200B- ND 0.50 0.40 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 101 70-130 1,2-Dichloroethane-d4 100 70-130 Toluene-d8 107 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 26 of 49 QC Summary Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 27 of 49 Volatile Organic Compounds by GC/MS - MB Sample ID: TQ82272-001 Matrix: Aqueous Batch: 82272 Prep Method: SM 620OB-2011 Analytical Method: SM 620OB-2011 Parameter Result Q Dil LOQ DL Units Analysis Date Benzene ND 1 0.50 0.40 ug/L 08/29/2018 0938 Ethylbenzene ND 1 0.50 0.40 ug/L 08/29/2018 0938 Methyl tertiary butyl ether (MTBE) ND 1 0.50 0.40 ug/L 08/29/2018 0938 Toluene ND 1 0.50 0.40 ug/L 08/29/2018 0938 Xylenes (total) ND 1 0.50 0.40 ug/L 08/29/2018 0938 Acceptance Surrogate Q % Rec Limit Bromofluorobenzene 103 70-130 1,2-Dichloroethane-d4 98 70-130 Toluene-d8 106 70-130 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 28 of 49 Volatile Organic Compounds by GC/MS - LCS Sample ID: TQ82272-002 Matrix: Aqueous Batch: 82272 Prep Method: SM 620OB-2011 Analytical Method: SM 620OB-2011 Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date Benzene 50 48 1 97 70-130 08/29/2018 0804 Ethylbenzene 50 50 1 100 70-130 08/29/2018 0804 Methyl tertiary butyl ether (MTBE) 50 46 1 92 70-130 08/29/2018 0804 Toluene 50 50 1 100 70-130 08/29/2018 0804 Xylenes (total) 100 99 1 99 70-130 08/29/2018 0804 Surrogate Q % Rec Acceptance Limit Bromofluorobenzene 92 70-130 1,2-Dichloroethane-d4 91 70-130 Toluene-d8 95 70-130 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 29 of 49 Volatile Organic Compounds by GC/MS - LCSD Sample ID: TQ82272-003 Matrix: Aqueous Batch: 82272 Prep Method: SM 620OB-2011 Analytical Method: SM 620OB-2011 Spike Amount Result % Rec % RPD Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date Benzene 50 45 1 90 7.5 70-130 20 08/29/2018 1746 Ethylbenzene 50 47 1 93 6.9 70-130 20 08/29/2018 1746 Methyl tertiary butyl ether (MTBE) 50 45 1 89 2.8 70-130 20 08/29/2018 1746 Toluene 50 47 1 94 5.5 70-130 20 08/29/2018 1746 Xylenes (total) 100 93 1 93 6.0 70-130 20 08/29/2018 1746 Acceptance Surrogate Q % Rec Limit Bromofluorobenzene 91 70-130 1,2-Dichloroethane-d4 93 70-130 Toluene-d8 93 70-130 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 30 of 49 Semivolatile Organic Compounds by GC/MS - MB Sample ID: TQ81238-001 Matrix: Aqueous Batch: 81238 Prep Method: 625.1 Analytical Method: 625.1 Prep Date: 08/20/2018 1841 Parameter Result Q Dil LOQ DL Units Analysis Date Acenaphthene ND 1 1.6 0.11 ug/L 08/28/2018 1042 Acenaphthylene ND 1 1.6 0.060 ug/L 08/28/2018 1042 Anthracene ND 1 1.6 0.060 ug/L 08/28/2018 1042 Benzo(a)anthracene ND 1 1.6 0.070 ug/L 08/28/2018 1042 Benzo(a)pyrene ND 1 1.6 0.040 ug/L 08/28/2018 1042 Benzo(b)fluoranthene ND 1 1.6 0.050 ug/L 08/28/2018 1042 Benzo(g,h,i)perylene ND 1 1.6 0.12 ug/L 08/28/2018 1042 Benzo(k)fluoranthene ND 1 1.6 0.070 ug/L 08/28/2018 1042 Benzyl alcohol ND 1 3.2 2.0 ug/L 08/28/2018 1042 4-Bromophenyl phenyl ether ND 1 1.6 0.16 ug/L 08/28/2018 1042 Butyl benzyl phthalate ND 1 1.6 0.15 ug/L 08/28/2018 1042 bis (2-Chloro-1-methylethyl) ether ND 1 1.6 0.49 ug/L 08/28/2018 1042 4-Chloro-3-methyl phenol ND 1 1.6 0.40 ug/L 08/28/2018 1042 bis(2-Chloroethoxy)methane ND 1 1.6 0.48 ug/L 08/28/2018 1042 bis(2-Chloroethyl)ether ND 1 1.6 0.50 ug/L 08/28/2018 1042 2-Chloronaphthalene ND 1 1.6 0.40 ug/L 08/28/2018 1042 2-Chlorophenol ND 1 1.6 0.34 ug/L 08/28/2018 1042 4-Chlorophenyl phenyl ether ND 1 1.6 0.21 ug/L 08/28/2018 1042 Chrysene ND 1 1.6 0.050 ug/L 08/28/2018 1042 Dibenzo(a,h)anth race ne ND 1 1.6 0.11 ug/L 08/28/2018 1042 Dibenzofuran ND 1 1.6 1.0 ug/L 08/28/2018 1042 1,2-Dichlorobenzene ND 1 1.6 0.46 ug/L 08/28/2018 1042 1,3-Dichlorobenzene ND 1 1.6 0.40 ug/L 08/28/2018 1042 1,4-Dichlorobenzene ND 1 1.6 0.41 ug/L 08/28/2018 1042 3,3'-Dichlorobenzidine ND 1 8.0 1.6 ug/L 08/28/2018 1042 2,4-Dichlorophenol ND 1 1.6 0.70 ug/L 08/28/2018 1042 Diethylphthalate ND 1 1.6 0.19 ug/L 08/28/2018 1042 Dimethyl phthalate ND 1 1.6 0.21 ug/L 08/28/2018 1042 2,4-Dimethylphenol ND 1 1.6 0.62 ug/L 08/28/2018 1042 Di-n-butyl phthalate ND 1 1.6 0.26 ug/L 08/28/2018 1042 4,6-Dinitro-2-methyl phenol ND 1 8.0 0.69 ug/L 08/28/2018 1042 2,4-Dinitrophenol ND 1 8.0 0.65 ug/L 08/28/2018 1042 Di-n-octylphthalate ND 1 1.6 0.070 ug/L 08/28/2018 1042 1,2-Diphenylhydrazine(as azobenzene) ND 1 1.6 0.12 ug/L 08/28/2018 1042 bis(2-Ethylhexyl)phthalate ND 1 8.0 0.19 ug/L 08/28/2018 1042 Fluoranthene ND 1 1.6 0.050 ug/L 08/28/2018 1042 Fluorene ND 1 1.6 0.060 ug/L 08/28/2018 1042 Hexachlorobenzene ND 1 1.6 0.39 ug/L 08/28/2018 1042 Hexachlorobutadiene ND 1 1.6 0.47 ug/L 08/28/2018 1042 Hexachlorocyclopentadiene ND 1 8.0 0.14 ug/L 08/28/2018 1042 Hexachloroethane ND 1 1.6 0.53 ug/L 08/28/2018 1042 Indeno(1,2,3-c,d)pyrene ND 1 1.6 0.11 ug/L 08/28/2018 1042 Isophorone ND 1 1.6 0.44 ug/L 08/28/2018 1042 1-Methyl naphthalene ND 1 1.6 0.40 ug/L 08/28/2018 1042 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 31 of 49 Semivolatile Organic Compounds by GC/MS - MB Sample ID: TQ81238-001 Matrix: Aqueous Batch: 81238 Prep Method: 625.1 Analytical Method: 625.1 Prep Date: 08/20/2018 1841 Parameter Result Q Dil LOQ DL Units Analysis Date 2-Methyl naphthalene ND 1 1.6 0.40 ug/L 08/28/20181042 2-Methylphenol ND 1 1.6 0.67 ug/L 08/28/20181042 3+4-Methylphenol ND 1 1.6 1.5 ug/L 08/28/20181042 Naphthalene ND 1 1.6 0.13 ug/L 08/28/20181042 Nitrobenzene ND 1 1.6 1.1 ug/L 08/28/20181042 2-Nitrophenol ND 1 3.2 0.88 ug/L 08/28/20181042 4-Nitrophenol ND 1 8.0 1.2 ug/L 08/28/20181042 N-Nitrosodi-n-propylamine ND 1 1.6 0.15 ug/L 08/28/20181042 N-Nitrosodiphenylamine (Diphenylamine) ND 1 1.6 0.25 ug/L 08/28/2018 1042 Pentachlorophenol ND 1 8.0 1.4 ug/L 08/28/20181042 Phenanthrene ND 1 1.6 0.12 ug/L 08/28/20181042 Phenol ND 1 1.6 0.22 ug/L 08/28/20181042 Pyrene ND 1 1.6 0.060 ug/L 08/28/20181042 1,2,4-Trichlorobenzene ND 1 1.6 0.57 ug/L 08/28/20181042 2,4,6-Trichlorophenol ND 1 1.6 0.44 ug/L 08/28/20181042 Surrogate Q % Rec Acceptance Limit 2-Fluorobiphenyl 68 37-129 2-Fluorophenol 34 24-127 Nitrobenzene-d5 66 38-127 Phenol-d5 51 28-128 Terphenyl-d 14 110 10-148 2,4,6-Tribromophenol 59 41-144 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 32 of 49 Semivolatile Organic Compounds by GC/MS - LCS Sample ID: TQ81238-002 Matrix: Aqueous Batch: 81238 Prep Method: 625.1 Analytical Method: 625.1 Prep Date: 08/20/2018 1841 Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date Acenaphthene 20 15 1 76 47-145 08/29/2018 1220 Acenaphthylene 20 15 1 77 33-145 08/29/2018 1220 Anthracene 20 17 1 86 27-133 08/29/2018 1220 Benzo(a)anthracene 20 18 1 92 33-143 08/29/2018 1220 Benzo(a)pyrene 20 16 1 78 17-163 08/29/2018 1220 Benzo(b)fluoranthene 20 19 1 95 24-159 08/29/2018 1220 Benzo(g,h,i)perylene 20 18 1 89 1-219 08/29/2018 1220 Benzo(k)fluoranthene 20 19 1 93 11-162 08/29/2018 1220 Benzyl alcohol 20 8.2 1 41 30-130 08/29/2018 1220 4-Bromophenyl phenyl ether 20 16 1 78 53-127 08/29/2018 1220 Butyl benzyl phthalate 20 23 1 114 1-152 08/29/2018 1220 bis (2-Chloro-1-methylethyl) ether 20 17 1 86 36-166 08/29/2018 1220 4-Chloro-3-methyl phenol 20 17 1 84 22-147 08/29/2018 1220 bis(2-Chloroethoxy)methane 20 17 1 87 33-184 08/29/2018 1220 bis(2-Chloroethyl)ether 20 17 1 83 12-158 08/29/2018 1220 2-Chloronaphthalene 20 14 1 70 60-120 08/29/2018 1220 2-Chlorophenol 20 13 1 66 23-134 08/29/2018 1220 4-Chlorophenyl phenyl ether 20 15 1 73 25-158 08/29/2018 1220 Chrysene 20 19 1 93 17-168 08/29/2018 1220 Dibenzo(a,h)anth race ne 20 19 1 93 1-227 08/29/2018 1220 Dibenzofuran 20 15 1 74 48-118 08/29/2018 1220 1,2-Dichlorobenzene 20 15 1 75 32-129 08/29/2018 1220 1,3-Dichlorobenzene 20 15 1 74 1-172 08/29/2018 1220 1,4-Dichlorobenzene 20 15 1 73 20-124 08/29/2018 1220 3,3'-Dichlorobenzidine 20 1.5 1 7.4 1-262 08/29/2018 1220 2,4-Dichlorophenol 20 12 1 59 39-135 08/29/2018 1220 Diethylphthalate 20 17 1 84 1-120 08/29/2018 1220 Dimethyl phthalate 20 16 1 81 1-120 08/29/2018 1220 2,4-Dimethylphenol 20 19 1 93 32-120 08/29/2018 1220 Di-n-butyl phthalate 20 20 1 101 1-120 08/29/2018 1220 4,6-Dinitro-2-methyl phenol 20 12 1 59 1-181 08/29/2018 1220 2,4-Dinitrophenol 40 19 1 46 1-191 08/29/2018 1220 Di-n-octylphthalate 20 19 1 93 4-146 08/29/2018 1220 1,2-Diphenylhydrazine(as azobenzene) 20 16 1 78 1-150 08/29/2018 1220 bis(2-Ethylhexyl)phthalate 20 23 1 114 8-158 08/29/2018 1220 Fluoranthene 20 17 1 87 26-137 08/29/2018 1220 Fluorene 20 16 1 78 59-121 08/29/2018 1220 Hexachlorobenzene 20 16 1 78 1-152 08/29/2018 1220 Hexachlorobutadiene 20 13 1 64 24-120 08/29/2018 1220 Hexachlorocyclopentadiene 100 24 1 24 1-150 08/29/2018 1220 Hexachloroethane 20 15 1 76 40-120 08/29/2018 1220 Indeno(1,2,3-c,d)pyrene 20 18 1 91 1-171 08/29/2018 1220 Isophorone 20 19 1 96 21-196 08/29/2018 1220 1-Methyl naphthalene 20 16 1 80 42-126 08/29/2018 1220 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 33 of 49 Semivolatile Organic Compounds by GC/MS - LCS Sample ID: TQ81238-002 Matrix: Aqueous Batch: 81238 Prep Method: 625.1 Analytical Method: 625.1 Prep Date: 08/20/2018 1841 Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date 2-Methyl naphthalene 20 16 1 80 40-132 08/29/20181220 2-Methylphenol 20 16 1 82 30-130 08/29/20181220 3+4-Methylphenol 20 16 1 78 30-130 08/29/20181220 Naphthalene 20 15 1 77 21-133 08/29/20181220 Nitrobenzene 20 17 1 83 35-180 08/29/20181220 2-Nitrophenol 20 13 1 65 29-182 08/29/20181220 4-Nitrophenol 40 20 1 50 1-132 08/29/20181220 N-Nitrosodi-n-propylamine 20 18 1 92 1-230 08/29/20181220 N-Nitrosodiphenylamine (Diphenylamine) 20 7.7 1 38 1-150 08/29/2018 1220 Pentachlorophenol 40 22 1 54 14-176 08/29/20181220 Phenanthrene 20 17 1 84 54-120 08/29/20181220 Phenol 20 13 1 66 5-120 08/29/20181220 Pyrene 20 19 1 95 52-120 08/29/20181220 1,2,4-Trichlorobenzene 20 13 1 66 44-142 08/29/20181220 2,4,6-Trichlorophenol 20 11 1 54 37-144 08/29/20181220 Surrogate Q % Rec Acceptance Limit 2-Fluorobiphenyl 71 37-129 2-Fluorophenol 51 24-127 Nitrobenzene-d5 81 38-127 Phenol-d5 66 28-128 Terphenyl-d 14 101 10-148 2,4,6-Tribromophenol 67 41-144 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 34 of 49 MADEP EPH (aliphatics) - MB Sample ID: TQ81720-001 Matrix: Aqueous Batch: 81720 Prep Method: MADEP-EPH-04 Analytical Method: MADEP-EPH-04 Prep Date: 08/23/2018 1850 Parameter Result Q Dil LOQ DL Units Analysis Date C9 - C18 Aliphatics ND 1 100 100 ug/L 08/25/2018 0116 C19 - C36 Aliphatics ND 1 100 100 ug/L 08/25/2018 0116 Surrogate Acceptance Q % Rec Limit 1-Chloro-octadecane (aliphatic) 69 40-140 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 35 of 49 MADEP EPH (aliphatics) - LCS Sample ID: TQ81720-002 Matrix: Aqueous Batch: 81720 Prep Method: MADEP-EPH-04 Analytical Method: MADEP-EPH-04 Prep Date: 08/23/2018 1850 Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date C9 - C18 Aliphatics 300 150 1 50 40-140 08/25/2018 0145 C19 - C36 Aliphatics 400 310 1 76 40-140 08/25/2018 0145 Surrogate Acceptance Q % Rec Limit 1-Chloro-octadecane (aliphatic) 72 40-140 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 36 of 49 MADEP EPH (aliphatics) - LCSD Sample ID: TQ81720-003 Matrix: Aqueous Batch: 81720 Prep Method: MADEP-EPH-04 Analytical Method: MADEP-EPH-04 Prep Date: 08/23/2018 1850 Spike Amount Result % Rec % RPD Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date C9 - C18 Aliphatics 300 150 1 49 2.3 40-140 25 08/25/2018 0214 C19 - C36 Aliphatics 400 300 1 75 1.2 40-140 25 08/25/2018 0214 Surrogate Acceptance Q % Rec Limit 1-Chloro-octadecane (aliphatic) 70 40-140 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 37 of 49 MADEP EPH (aromatics) - MB Sample ID: TQ81721-001 Matrix: Aqueous Batch: 81721 Prep Method: MADEP-EPH-04 Analytical Method: MADEP-EPH-04 Prep Date: 08/23/2018 1850 Parameter Result Q Dil LOQ DL Units Analysis Date C11 - C22 Aromatics ND 1 100 100 ug/L 08/25/2018 0439 Acceptance Surrogate Q % Rec Limit o - Terphenyl (aromatic) 62 40-140 2-Fluorobiphenyl (fractionation 1) 79 40-140 2-Bromonaphthalene (fractionation 2) 58 40-140 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 38 of 49 MADEP EPH (aromatics) - LCS Sample ID: TQ81721-002 Matrix: Aqueous Batch: 81721 Prep Method: MADEP-EPH-04 Analytical Method: MADEP-EPH-04 Prep Date: 08/23/2018 1850 Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date C11 - C22 Aromatics 850 590 1 69 40-140 08/25/2018 0508 Surrogate Q % Rec Acceptance Limit o - Terphenyl (aromatic) 67 40-140 2-Fluorobiphenyl (fractionation 1) 83 40-140 2-Bromonaphthalene (fractionation 2) 58 40-140 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 39 of 49 MADEP EPH (aromatics) - LCSD Sample ID: TQ81721-003 Matrix: Aqueous Batch: 81721 Prep Method: MADEP-EPH-04 Analytical Method: MADEP-EPH-04 Prep Date: 08/23/2018 1850 Spike Amount Result % Rec % RPD Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date C11 - C22 Aromatics 850 640 1 75 8.1 40-140 25 08/25/2018 0537 Acceptance Surrogate Q % Rec Limit o - Terphenyl (aromatic) 72 40-140 2-Fluorobiphenyl (fractionation 1) 87 40-140 2-Bromonaphthalene (fractionation 2) 72 40-140 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 40 of 49 MADEP VPH (aromatics) - MB Sample ID: TQ81529-001 Matrix: Aqueous Batch: 81529 Prep Method: VPH Analytical Method: MADEP-VPH-18-2.1 Parameter Result Q Dil LOQ DL Units Analysis Date C9 - C10 Aromatics ND 1 25 5.0 ug/L 08/22/2018 1515 Acceptance Surrogate Q % Rec Limit 2,5-Dibromotoluene (PID) 116 70-130 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 41 of 49 MADEP VPH (aromatics) - LCS Sample ID: TQ81529-002 Matrix: Aqueous Batch: 81529 Prep Method: VPH Analytical Method: MADEP-VPH-18-2.1 Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date C9 - C10 Aromatics 25 29 1 114 70-130 08/22/2018 1415 Acceptance Surrogate Q % Rec Limit 2,5-Dibromotoluene (PID) 98 70-130 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 42 of 49 MADEP VPH (aromatics) - LCSD Sample ID: TQ81529-003 Matrix: Aqueous Batch: 81529 Prep Method: VPH Analytical Method: MADEP-VPH-18-2.1 Spike Amount Result % Rec % RPD Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date C9 - C10 Aromatics 25 29 1 117 2.4 70-130 25 08/22/2018 1443 Acceptance Surrogate Q % Rec Limit 2,5-Dibromotoluene (PID) 106 70-130 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 43 of 49 MADEP VPH (aliphatics) - MB Sample ID: TQ81530-001 Matrix: Aqueous Batch: 81530 Prep Method: VPH Analytical Method: MADEP-VPH-18-2.1 Parameter Result Q Dil LOQ DL Units Analysis Date C5 - C8 Aliphatics ND 1 75 15 ug/L 08/22/2018 1515 C9 - C12 Aliphatics ND 1 75 15 ug/L 08/22/2018 1515 Acceptance Surrogate Q % Rec Limit 2,5-Dibromotoluene (FID) 114 70-130 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 44 of 49 MADEP VPH (aliphatics) - LCS Sample ID: TQ81530-002 Matrix: Aqueous Batch: 81530 Prep Method: VPH Analytical Method: MADEP-VPH-18-2.1 Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date C5 - C8 Aliphatics 150 150 1 99 70-130 08/22/2018 1415 C9 - C12 Aliphatics 180 170 1 97 70-130 08/22/2018 1415 Surrogate Q % Rec Acceptance Limit 2,5-Dibromotoluene (FID) 96 70-130 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 45 of 49 MADEP VPH (aliphatics) - LCSD Sample ID: TQ81530-003 Matrix: Aqueous Batch: 81530 Prep Method: VPH Analytical Method: MADEP-VPH-18-2.1 Spike Amount Result % Rec % RPD Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date C5 - C8 Aliphatics 150 150 1 103 4.0 70-130 25 08/22/2018 1443 C9 - C12 Aliphatics 180 180 1 102 4.2 70-130 25 08/22/2018 1443 Acceptance Surrogate Q % Rec Limit 2,5-Dibromotoluene (FID) 106 70-130 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 46 of 49 Chain of Custody and Miscellaneous Documents Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 47 of 49 SHEALY ENVIRONMENTAL SERVICES, INC. 9 .2 CD p 6 ¢ F E F_ - I� L 7 rt � I — [1 n rr RRR Lo Oy7 13 m a = � in " G{+ —1 X a � 4 }�f� In 'p S•7_w5 � 4 SlstAjeuV— J 71�1p � O L Q F E F 1- � Ln m }! _ -a)''�mm ` l ✓� P '�..5 dr�yy I O q' � � � 1j ❑ C do ��_Y='J � � � � � }C v� O 2ID IL �" C C6 n Co 1 J JQL ' R E ra Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 48 of 49 SHEALY ENVIRONMENTAL SERVICES, INC. Shu lr Rnvirurm I.-J R�r iarr� Ina rake 1 a i DncomcmMimhr.hid IR{'-I•I I.XwlivuUUW: Sumple Receipt Checklist ( R Client_ V. (fi4'1{1+1. i �A C'Llulrr InKpm-ted hy/&I.e= � V 1 IL rf' � j [.i)t CuicansaErc cipt; t<51 LJ l:licnt UPS~CI Fad�x J Olhcr _ ❑ Yes L c -_ Wr.rr rusttxty gals Trrsent mi i11e cnn]cf.• Yea I''I No t_ III L-LLSLudy scids %verC preiL-,lt, wcTu LIey iutur.t andunbnc kLn? H -Strip ID; ._-. - . _ ".� C'1110r:Fla Stri}r ID; .. _ Tested W: '^ L hi nsg11 ftppmturL }U[r}n rC Opk + lD6rivt:d (Corrt�CLL-[l) 1eJrt1pmlU� 4LpVA r"Cl.pt- °oi0(i Srwp-'Up 1D: 1 L:-1g � i � f 9C Aethod: I y v6perawrc Blank C, Against Do lw. IR Gun lD; ��_ , _ 1 R {`run Corregdon Factor; _vfeLhod of cx)olanv. Ice C1 Ice Packs Ej p Ise Nate Yes D Nio A[4. If 1er11lxraluxe of any cooler exceeded 6.l1°C', vt4x Project Manager Notified? - PAl was ldntif3eCl by.phone I tmaiE I I'hr&-m-&niC, (6rnle Nit). �I 1„ I yqi Wu , IS the COn1 I11=i a l C4ttriar's pac-&-ing slip attFLzhed to 6 is tbrni? es No 5_ Were proper 92wzLodyprocedwr%(relinyuirhedheceiVrd) Inllnwad`_- L N-D 5_ Were sample Ox li ac4l tin Lhc COQ9 L_ es L . No cm sample Dr listed on all saiuplL cuntai mm? er Mo $, War, co]luction date & t:mo listed an the COC"' No 9. Wa€. call action date & tune Eisued tut all sample crmtaineni? I 1---Yt 5 No :0. CJId a]I c.nn1aincr lakI infnitnatinn (IIJ, rLat,c, time) n rrac }with the f'0C:7 ex L NU .1. V4rcrc tests to bcP'rformcd listcd On di': COO es C No 12. Did all samples arrive in the proper containers for each test andlor in good candition (unbroken, lids cm, eic.)': ' c� � NU II Was adequate saJfiple %oluim avili We'? 'es U No 14. Werr, 911 isamplm rrwivcd within'/% tho holding time or 4$ hours, whiahover conies first? ' Yes L o t5_ Were arty 6amply tclrltakmm rniv:irkfiVeL teS {Circle Cale) stlrnplcs Not listcd on Ck)C? E. Yes �� t} ,. 16, For V'0A Land R -1?5 samples, iycrc babbles prcmcnt �"pca-size" (Y."or6mnl in diameter) in #Ina of iE.t! '4r0A4 vials? F Yes J -No 4AAA 17_ WcL- all DR01ri>Ictals+nutricm samples rc-,eivW at a pH of = 2? L_ Yel: C] No . Werc all cyanide samples rccziivcd at a pIt > 12 and sulfide. sanlp°es rEceived at a pi I > 97 Yas ' Nn I A 19_ Were all applicab a NlHyTKN!o}gaide} >oV625 (- 0_5n)VL) samples Lee aCresidual chlorins'? 'CS rrII U No. were elientremark0requesrs (,-S'l��ai Le. requested d illudoas, ryIS!MrgnatiOny, ete---Ek � Corr alv a itmezribcd ffom LkC ram_ ilk'-O L11L; C011LaLi]tt ?.UlkMJ 1[L MIS? G Yes ( 0 2l. Was the qucAe number listed on the con Diner Iahc lr? Tf }sex, Quote, # Saro[rIC PreNervatiou (Muhl he cnnVleLed rcrrarLv NEuiipl0H) inc "rrru ily prus rvLA <ir wish hcndslin a.] aLri(]lu[S) _ ;very rece k'ed utc meetly pmsoeeved and tiwert: a+]juz&ca :1 wrainstl} in crumple Leeeivirlg with mL ofcif ale ari& H2SO4-_ HNO3, HCI, NEL01-1 UL.ing SR !i Time ofpresea:vaLjan Ifrnord &3111Ogle lnesenal.iveisneedul, pleal;elrate in thr I:Lwra,LC33I�bc10w_ Samplca(s) inure :-mpivod with huhhlc ;-6 mm in riinmcter. $atrLples(s) were ueceiWd vrri tiL TR.0 = 0-$ a XiL {�l` +19 is nVa ) auu.l WnV aasteLl iJCL4 td:11.1y ift .Alilple receivida widi sodium ilkiosulfate (Na7%01) wi ffi Sl lculy 1FJ_ SR cnde liihcLL applie' d hy_ mate} � har16 Conulsents� Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 49 of 49 LP R I S M Full -Service Analytical & Environmental Solutions LABORATORIES, INC. Colonial Pipeline Company John Culbreath PO Box 87 Charlotte, NC 28130 NC Certification No. 402 NC Drinking Water Cert No. 37735 SC Certification No. 99012 Project: Kannapolis NPDES Lab Submittal Date: 08/24/2018 Prism Work Order: 8080423 Case Narrative 09/10/2018 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. Terri W. Cole Project Manager Data Qualifiers Key Reference: Reviewed By Terri W. Cole Project Manager CCV CCV result is above the control limits. Analyte not detected in the sample. No further action taken. L1 LCS recovery outside of the QC limits. LCSD recovery within the limits. No further action taken. SR Surrogate recovery outside the QC limits. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 1 of 12 �P R I S M Full -Service Analytical s Environmental Solutions LABORATORIES, INC. Sample Receipt Summary 09/10/2018 Prism Work Order: 8080423 Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received DW-Goodnight-New-Influent_08 8080423-01 Water 08/23/18 13:30 08/24/18 16:00 DW-Cook-Influent 08/23/18 Lab 8080423-02 Water 08/23/18 14:25 08/24/18 16:00 DW-Watts-New-Influent 08/23/18 8080423-03 Water 08/23/18 13:40 08/24/18 16:00 DW-Maurer-Influent 08/23/18 8080423-04 Water 08/23/18 14:05 08/24/18 16:00 DW-Kann-Station 08/23/18 Lab 8080423-05 Water 08/23/18 13:00 08/24/18 16:00 DW-Coren-Influent 08/23/18 Lab 8080423-06 Water 08/23/18 14:20 08/24/18 16:00 DW-Tucker-Influent 08/23/18 Lab 8080423-07 Water 08/23/18 13:50 08/24/18 16:00 Samples were received in good condition at 4.7 degrees C unless otherwise noted This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 2 of 12 /P R I IS M Full -Service Analytical Environmental Solutions LABORATORIES, INC. Laboratory Report 09/10/2018 Colonial Pipeline Company Attn: John Culbreath PO Box 87 Charlotte, NC 28130 Project: Kannapolis NPDES Sample Matrix: Water Client Sample ID: DW-Goodnight-New-Influent_08 Prism Sample ID: 8080423-01 Prism Work Order: 8080423 Time Collected: 08/23/18 13:30 Time Submitted: 08/24/18 16:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Volatile Organic Compounds by GUMS Benzene BRL ug/L 1.0 0.048 1 *8260B 9/6/18 0:53 KDM P810051 Ethylbenzene BRL ug/L 1.0 0.061 1 *8260B 9/6/18 0:53 KDM P810051 m,p-Xylenes BRL ug/L 2.0 0.12 1 *8260B 9/6/18 0:53 KDM P810051 Methyl-tert-Butyl Ether BRL ug/L 1.0 0.042 1 *8260B 9/6/18 0:53 KDM P810051 Naphthalene BRLCCV ug/L 1.0 0.19 1 *8260B 9/6/18 0:53 KDM P810051 o-Xylene BRL ug/L 1.0 0.044 1 *8260B 9/6/18 0:53 KDM P810051 Toluene BRL ug/L 1.0 0.044 1 *8260B 9/6/18 0:53 KDM P810051 Xylenes, total BRL ug/L 3.0 0.15 1 *8260B 9/6/18 0:53 KDM P810051 Surrogate Recovery Control Limits 4-Bromofluorobenzene 101 % 80-124 Dibromofluoromethane 104 % 75-129 Toluene-d8 102 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 3 of 12 �Full-Service Analytical P R I S M Environmental Solutions LABORATORIES INC. Colonial Pipeline Company Attn: John Culbreath PO Box 87 Charlotte, NC 28130 Project: Kannapolis NPDES Sample Matrix: Water Laboratory Report 09/10/2018 Client Sample ID: DW-cook-Influent_08/23/18_Lab Prism Sample ID: 8080423-02 Prism Work Order: 8080423 Time Collected: 08/23/18 14:25 Time Submitted: 08/24/18 16:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Volatile Organic Compounds by GC/MS Benzene BRL ug/L 1.0 0.048 1 *8260B 9/6/18 1:19 KDM P810051 Ethylbenzene BRL ug/L 1.0 0.061 1 *8260B 9/6/18 1:19 KDM P810051 m,p-Xylenes BRL ug/L 2.0 0.12 1 *8260B 9/6/18 1:19 KDM P810051 Methyl-tert-Butyl Ether BRL ug/L 1.0 0.042 1 *8260B 9/6/18 1:19 KDM P810051 Naphthalene BRLCCV ug/L 1.0 0.19 1 *8260B 9/6/18 1:19 KDM P810051 o-Xylene BRL ug/L 1.0 0.044 1 *8260B 9/6/18 1:19 KDM P810051 Toluene BRL ug/L 1.0 0.044 1 *8260B 9/6/18 1:19 KDM P810051 Xylenes, total BRL ug/L 3.0 0.15 1 *8260B 9/6/18 1:19 KDM P810051 Surrogate Recovery Control Limits 4-Bromofluorobenzene 104 % 80-124 Dibromofluoromethane 96 % 75-129 Toluene-d8 93 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 4 of 12 �Full-Service Analytical P R I S M Environmental Solutions LABORATORIES INC. Colonial Pipeline Company Attn: John Culbreath PO Box 87 Charlotte, NC 28130 Project: Kannapolis NPDES Sample Matrix: Water Laboratory Report 09/10/2018 Client Sample ID: DW-watts-New-Influent_08/23/18 Prism Sample ID: 8080423-03 Prism Work Order: 8080423 Time Collected: 08/23/18 13:40 Time Submitted: 08/24/18 16:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Volatile Organic Compounds by GC/MS Benzene BRL ug/L 1.0 0.048 1 *8260B 9/6/18 1:45 KDM P810051 Ethylbenzene BRL ug/L 1.0 0.061 1 *8260B 9/6/18 1:45 KDM P810051 m,p-Xylenes BRL ug/L 2.0 0.12 1 *8260B 9/6/18 1:45 KDM P810051 Methyl-tert-Butyl Ether BRL ug/L 1.0 0.042 1 *8260B 9/6/18 1:45 KDM P810051 Naphthalene BRLCCV ug/L 1.0 0.19 1 *8260B 9/6/18 1:45 KDM P810051 o-Xylene BRL ug/L 1.0 0.044 1 *8260B 9/6/18 1:45 KDM P810051 Toluene BRL ug/L 1.0 0.044 1 *8260B 9/6/18 1:45 KDM P810051 Xylenes, total BRL ug/L 3.0 0.15 1 *8260B 9/6/18 1:45 KDM P810051 Surrogate Recovery Control Limits 4-Bromofluorobenzene 130 % 80-124 SR Dibromofluoromethane 75 % 75-129 Toluene-d8 105 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 5 of 12 �Full-Service Analytical P R I S M Environmental Solutions LABORATORIES INC. Colonial Pipeline Company Attn: John Culbreath PO Box 87 Charlotte, NC 28130 Project: Kannapolis NPDES Sample Matrix: Water Laboratory Report 09/10/2018 Client Sample ID: DW-Maurer-Influent_08/23/18 Prism Sample ID: 8080423-04 Prism Work Order: 8080423 Time Collected: 08/23/18 14:05 Time Submitted: 08/24/18 16:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Volatile Organic Compounds by GC/MS Benzene BRL ug/L 1.0 0.048 1 *8260B 9/6/18 2:11 KDM P810051 Ethylbenzene BRL ug/L 1.0 0.061 1 *8260B 9/6/18 2:11 KDM P810051 m,p-Xylenes BRL ug/L 2.0 0.12 1 *8260B 9/6/18 2:11 KDM P810051 Methyl-tert-Butyl Ether 1.9 ug/L 1.0 0.042 1 *8260B 9/6/18 2:11 KDM P810051 Naphthalene BRLCCV ug/L 1.0 0.19 1 *8260B 9/6/18 2:11 KDM P810051 o-Xylene BRL ug/L 1.0 0.044 1 *8260B 9/6/18 2:11 KDM P810051 Toluene BRL ug/L 1.0 0.044 1 *8260B 9/6/18 2:11 KDM P810051 Xylenes, total BRL ug/L 3.0 0.15 1 *8260B 9/6/18 2:11 KDM P810051 Surrogate Recovery Control Limits 4-Bromofluorobenzene 76 % 80-124 SR Dibromofluoromethane 104 % 75-129 Toluene-d8 107 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 6 of 12 �Full-Service Analytical P R I S M Environmental Solutions LABORATORIES INC. Colonial Pipeline Company Attn: John Culbreath PO Box 87 Charlotte, NC 28130 Project: Kannapolis NPDES Sample Matrix: Water Laboratory Report 09/10/2018 Client Sample ID: DW-Kann-Station_08/23/18_Lab Prism Sample ID: 8080423-05 Prism Work Order: 8080423 Time Collected: 08/23/18 13:00 Time Submitted: 08/24/18 16:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Volatile Organic Compounds by GC/MS Benzene BRL ug/L 1.0 0.048 1 *8260B 9/6/18 2:37 KDM P810051 Ethylbenzene BRL ug/L 1.0 0.061 1 *8260B 9/6/18 2:37 KDM P810051 m,p-Xylenes BRL ug/L 2.0 0.12 1 *8260B 9/6/18 2:37 KDM P810051 Methyl-tert-Butyl Ether BRL ug/L 1.0 0.042 1 *8260B 9/6/18 2:37 KDM P810051 Naphthalene BRLCCV ug/L 1.0 0.19 1 *8260B 9/6/18 2:37 KDM P810051 o-Xylene BRL ug/L 1.0 0.044 1 *8260B 9/6/18 2:37 KDM P810051 Toluene BRL ug/L 1.0 0.044 1 *8260B 9/6/18 2:37 KDM P810051 Xylenes, total BRL ug/L 3.0 0.15 1 *8260B 9/6/18 2:37 KDM P810051 Surrogate Recovery Control Limits 4-Bromofluorobenzene 76 % 80-124 SR Dibromofluoromethane 123 % 75-129 Toluene-d8 119 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 7 of 12 �Full-Service Analytical P R I S M Environmental Solutions LABORATORIES INC. Colonial Pipeline Company Attn: John Culbreath PO Box 87 Charlotte, NC 28130 Project: Kannapolis NPDES Sample Matrix: Water Laboratory Report 09/10/2018 Client Sample ID: DW-Coren-Influent_08/23/18_Lab Prism Sample ID: 8080423-06 Prism Work Order: 8080423 Time Collected: 08/23/18 14:20 Time Submitted: 08/24/18 16:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Volatile Organic Compounds by GC/MS Benzene BRL ug/L 1.0 0.048 1 *8260B 9/6/18 3:03 KDM P810051 Ethylbenzene BRL ug/L 1.0 0.061 1 *8260B 9/6/18 3:03 KDM P810051 m,p-Xylenes BRL ug/L 2.0 0.12 1 *8260B 9/6/18 3:03 KDM P810051 Methyl-tert-Butyl Ether BRL ug/L 1.0 0.042 1 *8260B 9/6/18 3:03 KDM P810051 Naphthalene BRLCCV ug/L 1.0 0.19 1 *8260B 9/6/18 3:03 KDM P810051 o-Xylene BRL ug/L 1.0 0.044 1 *8260B 9/6/18 3:03 KDM P810051 Toluene BRL ug/L 1.0 0.044 1 *8260B 9/6/18 3:03 KDM P810051 Xylenes, total BRL ug/L 3.0 0.15 1 *8260B 9/6/18 3:03 KDM P810051 Surrogate Recovery Control Limits 4-Bromofluorobenzene 104 % 80-124 Dibromofluoromethane 100 % 75-129 Toluene-d8 124 % 77-123 SR This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 8 of 12 �Full-Service Analytical P R I S M Environmental Solutions LABORATORIES INC. Colonial Pipeline Company Attn: John Culbreath PO Box 87 Charlotte, NC 28130 Project: Kannapolis NPDES Sample Matrix: Water Laboratory Report 09/10/2018 Client Sample ID: DW-Tucker-Influent_08/23/18_La Prism Sample ID: 8080423-07 Prism Work Order: 8080423 Time Collected: 08/23/18 13:50 Time Submitted: 08/24/18 16:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Volatile Organic Compounds by GC/MS Benzene BRL ug/L 1.0 0.048 1 *8260B 9/6/18 3:29 KDM P810051 Ethylbenzene BRL ug/L 1.0 0.061 1 *8260B 9/6/18 3:29 KDM P810051 m,p-Xylenes BRL ug/L 2.0 0.12 1 *8260B 9/6/18 3:29 KDM P810051 Methyl-tert-Butyl Ether 1.3 ug/L 1.0 0.042 1 *8260B 9/6/18 3:29 KDM P810051 Naphthalene BRLCCV ug/L 1.0 0.19 1 *8260B 9/6/18 3:29 KDM P810051 o-Xylene BRL ug/L 1.0 0.044 1 *8260B 9/6/18 3:29 KDM P810051 Toluene BRL ug/L 1.0 0.044 1 *8260B 9/6/18 3:29 KDM P810051 Xylenes, total BRL ug/L 3.0 0.15 1 *8260B 9/6/18 3:29 KDM P810051 Surrogate Recovery Control Limits 4-Bromofluorobenzene 99 % 80-124 Dibromofluoromethane 100 % 75-129 Toluene-d8 104 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 9 of 12 P R I IS M EService Analytical Environmental Solutions LABORATORIES, INC. Level II QC Report 9/10/18 Colonial Pipeline Company Attn: John Culbreath PO Box 87 Charlotte, NC 28130 Project: Kannapolis NPDES Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P810051 - 5030B Reporting Result Limit Units Prism Work Order: 8080423 Time Submitted: 8/24/2018 4:00:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (P810051-BLKI) Prepared & Analyzed: 09/05/18 Benzene BRL 1.0 ug/L Ethylbenzene BRL 1.0 ug/L m,p-Xylenes BRL 2.0 ug/L Methyl-tert-Butyl Ether BRL 1.0 ug/L Naphthalene BRL 1.0 ug/L o-Xylene BRL 1.0 ug/L Toluene BRL 1.0 ug/L Xylenes, total BRL 3.0 ug/L Surrogate:4-Bromofluorobenzene 50.9 ug/L 50.00 102 80-124 Surrogate: Dibromofluoromethane 49.0 ug/L 50.00 98 75-129 Surrogate: Toluene-d8 50.7 ug/L 50.00 101 77-123 LCS (P810051-BSI) Prepared & Analyzed: 09/05/18 Benzene 20.9 1.0 ug/L 20.00 104 77-128 Ethylbenzene 23.1 1.0 ug/L 20.00 116 80-127 m,p-Xylenes 46.6 2.0 ug/L 40.00 116 77-133 Methyl-tert-Butyl Ether 19.7 1.0 ug/L 20.00 98 68-135 Naphthalene 30.3 1.0 ug/L 20.00 151 64-136 L1 o-Xylene 20.5 1.0 ug/L 20.00 103 78-128 Toluene 21.9 1.0 ug/L 20.00 110 76-131 Xylenes, total 67.1 3.0 ug/L 60.00 112 77-133 Surrogate:4-Bromofluorobenzene 51.5 ug/L 50.00 103 80-124 Surrogate: Dibromofluoromethane 47.6 ug/L 50.00 95 75-129 Surrogate: Toluene-d8 51.5 ug/L 50.00 103 77-123 LCS Dup (P810051-BSD1) Prepared & Analyzed: 09/05/18 Benzene 20.8 1.0 ug/L 20.00 104 77-128 0.2 20 Ethylbenzene 23.3 1.0 ug/L 20.00 116 80-127 0.8 20 m,p-Xylenes 47.0 2.0 ug/L 40.00 117 77-133 0.9 20 Methyl-tert-Butyl Ether 19.2 1.0 ug/L 20.00 96 68-135 2 20 Naphthalene 24.7 1.0 ug/L 20.00 124 64-136 20 20 o-Xylene 20.5 1.0 ug/L 20.00 103 78-128 0.05 20 Toluene 21.6 1.0 ug/L 20.00 108 76-131 2 20 Xylenes, total 67.5 3.0 ug/L 60.00 112 77-133 0.6 20 Surrogate:4-Bromofluorobenzene 50.9 ug/L 50.00 102 80-124 Surrogate: Dibromofluoromethane 48.4 ug/L 50.00 97 75-129 Surrogate: Toluene-d8 51.0 ug/L 50.00 102 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 10 of 12 Sample Extraction Data Prep Method: 5030E Lab Number Batch Initial Final Date/Time 8080423-01 P810051 10 mL 10 mL 09/05/18 9:57 8080423-02 P810051 10 mL 10 mL 09/05/18 9:57 8080423-03 P810051 10 mL 10 mL 09/05/18 9:57 8080423-04 P810051 10 mL 10 mL 09/05/18 9:57 8080423-05 P810051 10 mL 10 mL 09/05/18 9:57 8080423-06 P810051 10 mL 10 mL 09/05/18 9:57 8080423-07 P810051 10 mL 10 mL 09/05/18 9:57 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. 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