3901_Granville_Oxford_Unit1_MSWLF_CDLF_GW_FID1261328_2018810

ENR USE ONLY ❑Paper Report_ ❑Electronic Data - Email CD (data loaded: Yes / No) Doc/Event #.
"NC DENR Environmental Monitoring
Division of Waste Management - Solid Waste Reporting Form
Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6),
Instructions:
Prepare one form for each individually monitored unit.
Please type or print legibly.
Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646.
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Joyce Engineering, Inc.
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: G. Van Ness Burbach, Ph.D., P.G.
E-mail: [e-mail]
Phone: [phone]
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006)
6584 Landfill Rd. 3901- August 14-16, 2018
Oxford Landfill Unit 1 Oxford, NC 27565 CDLF-1997 .1600 November 02, 2018
Environmental Status: (Check all that apply)
Initial/Background Monitoring Detection Monitoring
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells 71
Groundwater monitoring data from private water supply wells X
Leachate monitoring data ❑
Surface water monitoring data
Q Assessment Monitoring
Methane gas monitoring data
Corrective action data (specify)
Other(specify)
0 Corrective Action
MNA Parameters
Notification attached?
No. No groundwater or surface water standards were exceeded.
X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard. NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
G. VanNess Burbach, Ph.D., PG Technical Consultant [phone]
2211 W. Meadowview Rd., Ste 101 Greensboro, NC 27407
Facility Representative Address
C-0782
NC PE Firm License Number (if applicable effective May 1, 2009)
Revised 6/2009
!a Code) Telephone Number
Affix NC Uuam"
CA yi
SEAL
1349
G G'F�COG` Qvz
#•,!bFSS ev..•�
Geologist Seal

PREPARED FOR:
GRANVILLE COUNTY
SOLID WASTE DEPARTMENT
P.O. Box 906
OXFORD, NORTH CAROLINA 27565
O F
w r
CAYL
OXFORD UNIT 1 LANDFILL
PERMIT No. 3901-CDLF-1997
AUGUST 2018 SEMIANNUAL WATER QUALITY
MONITORING REPORT
DECEMBER 2018
PREPARED BY:
r�L11 i�
EIVGfNEE14fNG
2211 WEST MEADOWVIEW ROAD, SUITE 101
GREENSBORO, NORTH CAROLINA 27407
NC LICENSE NUMBER C-0782
PHONE: [phone]
FAx: [phone]
JOYCE PROJECT No. 2182022.01.05

AUGUST 2018 SEMIANNUAL WATER QUALITY MONITORING REPORT
Oxford Unit 1 Landfill - Granville County - Permit No. 3901-CDLF-1997
TABLE OF CONTENTS
1.0 INTRODUCTION.................................................................................................................1
1.1 Site Background..................................................................................................................1
1.2 Site Conceptual Model........................................................................................................2
1.2.1 Site Geology............................................................................................................2
1.2.2 Site Hydrogeology...................................................................................................2
1.3 Monitoring History and Regulatory Status......................................................................... 3
1.3.1 Monitoring History.................................................................................................. 3
1.3.2 Regulatory Status.................................................................................................... 3
1.4 Hydrogeology......................................................................................................................5
2.0
FACILITY MONITORING PROGRAM...........................................................................6
2.1
Groundwater Monitoring Program......................................................................................
6
2.2
Surface Water Monitoring Program....................................................................................
7
3.0
FIRST SEMIANNUAL SAMPLING EVENT OF 2018....................................................
7
3.1
Field Work...........................................................................................................................
7
3.2
Laboratory Analysis and Quality Control...........................................................................
8
3.3
Data Analyses......................................................................................................................
9
3.3.1 Analytical Results for Groundwater........................................................................
9
3.3.1.1 Inorganic Analyses............................................................................................................................................
9
3.3.1.2 Organic Analyses............................................................................................................................................
10
3.3.1.3 Performance and Sentinel Wells......................................................................................................................
10
3.3.2 Analytical Results for Surface Water....................................................................10
3.3.3 Statistical Analyses...............................................................................................11
3.3.3.1 Statistical Methods............................................................................................................................................
11
3.3.3.2 Results of Statistical Analyses.............................................................................................................................
11
4.0
EVALUATION OF MONITORED NATURAL ATTENUATION (MNA)..................11
4.1
MNA Parameters and Biodegradation Screening Matrix..................................................11
4.2
Biochlor Modeling and Mass -Balance Assessment..........................................................13
4.3
Trend Analysis and Plume Stability..................................................................................13
5.0
CONCLUSIONS..................................................................................................................13
6.0
REFERENCES....................................................................................................................14
7.0
ACRONYMS.......................................................................................................................15
August 2018 Semiannual Water Quality Monitoring Report Joyce Engineering
Oxford Unit 1 Landfill, Permit No. 3 901 -CDLF- 1997 December 2018
I

AUGUST 2018 SEMIANNUAL WATER QUALITY MONITORING REPORT
Oxford Unit 1 Landfill - Granville County - Permit No. 3901-CDLF-1997
TABLE OF CONTENTS
TABLES:
Table 1 Monitoring Well Construction Data
Table 2 Groundwater Elevation Data
Table 3 Groundwater Gradients and Calculated Flow Rates
Table 4 Detections of Groundwater and Surface Water Constituents
Table 5 Exceedances of Groundwater and Surface Water Standards
Table 6 Field Parameters
Table 7 Biodegradation Screening Matrix
CHARTS:
Chart 1 Vinyl Chloride in MW-5 & MW-5R vs. Time
Chart 2 1, 1 -Dichloroethane in MW-5 & MW-5R vs. Time
FIGURE:
Figure 1 Site Location Map (USGS Topographic Map)
DRAWING:
Drawing 1 Groundwater Potentiometric Surface Map
APPENDICES:
Appendix A Field Sampling Logs
Appendix B Laboratory Reports with Chains of Custody
Appendix C Historical Tables
Table C-01 Historical Groundwater Elevation Data
Table C-02 Historical Detected Inorganic Constituents in Compliance Wells
Table C-03 Historical Detected Organic Constituents in Compliance Wells
Table C-04 Historical Detected COCs in Performance and Sentinel Wells
Table C-05 Historical Detected Constituents in Surface Water
Table C-06 Historical MNA Parameter Data
August 2018 Semiannual Water Quality Monitoring Report
Oxford Unit 1 Landfill, Permit No. 3 901 -CDLF- 1997
Joyce Engineering
December 2018
ii

1.0 INTRODUCTION
On behalf of Granville County, Joyce Engineering, (JOYCE) has prepared this Water Quality
Monitoring Report for the Oxford Unit 1 Landfill, Solid Waste Permit Number
3901-CDLF-1997 (facility), in accordance with 15A NCAC 13B.1632 of the North Carolina
Solid Waste Management Rules (NCSWMR).
1.1 Site Background
The Oxford Landfill is located at 6584 Landfill Road, Oxford, Granville County, North Carolina,
near the town of Kinton Fork (Figure 1). The facility is owned and operated by Granville
County under Permit Number 3901-CDLF-1997, issued by the North Carolina Department of
Environment and Natural Resources (NCDENR), now the Department of Environmental Quality
(NCDEQ), Solid Waste Section (SWS). The Oxford Landfill consists of two separate waste
disposal units. Unit 1 is a former unlined municipal solid waste (MSW) landfill originally
permitted for disposal of domestic, institutional, industrial, agricultural, and demolition wastes.
Between 1997 and 2017, the facility disposed of construction and demolition (C&D) waste in
Unit 1 on top of the closed MSW landfill in accordance with the Transition Plan dated 1994.
The C&D portion of the Unit 1 Landfill is slated for closure in 2018. The permitted facility
consists of approximately 283 acres, of which approximately 29 acres constitutes the Unit 1
Landfill waste unit. Unit 2 is a Subtitle-D MSW landfill which was permitted to operate in
February 2013 and began receiving waste in May 2013.
The groundwater monitoring network at the Unit 1 landfill consists of one upgradient well
(MW-7) and five downgradient wells (MW-2, MW-3R, MW-4R, MW-5R and MW-6R) as
shown on Drawing 1. Monitoring wells MW-3R, MW-4R, MW-5R, and MW-6R replaced
MW-3, MW-4, MW-5, and MW-6, respectively, in 1999, due to the close proximity to waste of
the original wells. Wells NES-1S&D and NES-2S&D were installed down -gradient of MW-4R
and MW-5R, respectively in May 2004 as part of the Nature and Extent Study (NES). The
Corrective Action Plan (CAP) dated April 23, 2009, designated NES-lS and NES-2S as
performance wells and NES-11) and NES-21) as sentinel wells; however, NES-11) and NES-IS
were removed from the monitoring network in June 2014. NES-1 D was abandoned in July 2016.
MW-7 replaced MW-lA as the facility background well beginning with the first semiannual
monitoring event of 2011. The monitoring wells are screened within the uppermost aquifer
underlying the facility. Well construction details are summarized in Table 1.
In addition, there are two surface water sampling points, SW-1 and SW-2 associated with Unit 1.
Sampling point SW-1 is a sedimentation pond located near the southeast corner of the waste unit,
and is up -stream of waste. Sampling point SW-2 is a small creek located northeast of the waste
unit and is downstream of the waste unit. The locations of SW-1 and SW-2 are shown on
Drawing 1.
August 2018 Semiannual Water Quality Monitoring Report Joyce Engineering
Oxford Unit 1 Landfill, Permit No. 3901-CDLF-1997 December 2018
1

1.2 Site Conceptual Model
1.2.1 Site Geology
The Oxford Unit 1 Landfill is located in the Carolina Slate Belt of the Piedmont Physiographic
Province of North Carolina. The geologic province is characterized by a rolling topography with
a thick mantle of saprolite overlying Late Proterozoic and Paleozoic igneous and metamorphic
bedrock. The Carolina Slate Belt is comprised of 550 to 650 million year old, metamorphosed
sedimentary and volcanic rocks, intruded by granitic rocks.
The Oxford Unit 1 Landfill is underlain by the Flat River Complex, which is a shallow intrusive
complex of granitic composition, which comprises a large portion of the northern Carolina Slate
Belt (Butler, 1991). The landfill is approximately 18 miles east of the Virgilina Synclinorium,
approximately 10 miles west of the Nutbush Creek Fault Zone, and approximately 4 miles
northwest of the Durham Basin (Butler, 1991).
Previous investigations discovered limited exposures in the borrow area of a competent, massive,
gray to greenish gray meta -volcanic rock that is moderately fractured with prominent fractures
with near vertical dips and striking approximately N25° to 30°W (Woodward -Clyde, 1994).
Boring logs indicate that the depth to bedrock at Oxford Unit 1 Landfill ranges from 5 to 30 feet
below ground surface. The overlying saprolite consists of brownish sandy to clayey silt
(Woodward -Clyde, 1994).
1.2.2 Site Hydroeg ology
Groundwater in the Piedmont can occur in substantial volumes where soils and regolith are thick,
but groundwater is typically found in minimal volumes in bedrock, primarily restricted to
fractures. The water table under the area of investigation was encountered in the unconfined
aquifer that is mostly in the transition zone that consists of saprolite and highly fractured
bedrock. This unconfined aquifer is pervasive across the site and generally mimics the surface
topography. The saturated portion of the uppermost aquifer beneath the study area is vertically
continuous to bedrock, and no confining layers have been encountered during site investigations.
There is a high degree of connectivity between the saprolite and underlying fractured bedrock
such that they behave as a single continuous aquifer. Depth to water ranged from 5 to 10 feet
below grade in wells MW-4R, MW-6R, NES-2S, and NES-21); and 10 to 25 feet below grade in
MW-lA, MW-2, MW-3R, MW-5R, MW-7, NES-IS, and NES-11) (Table 2). In general, the
water table is near the saprolite/bedrock interface.
Groundwater in the saprolite feeds the fractures in the bedrock and is discharged into creeks
north of the landfill. Groundwater flow at deeper levels within the fractured bedrock is
controlled by fractures. A groundwater potentiometric surface map, based on static water level
data obtained on August 14, 2018, is presented as Drawing 1. The groundwater map depicts
groundwater flow to the north.
August 2018 Semiannual Water Quality Monitoring Report Joyce Engineering
Oxford Unit 1 Landfill, Permit No. 3901-CDLF-1997 December 2018
2

1.3 Monitoring History and Regulatory Status
1.3.1 Monitoring HrX
• 1995: Oxford Unit 1 entered Assessment
constituents in several monitoring wells.
• 1998: Monitoring wells MW-3R, MW-4R,
MW-4, MW-5, and MW-6, respectively.
Monitoring due to detections of organic
MW-5R, and MW-6R replaced MW-3,
• 2003: Assessment of Corrective Measures (ACM) and Nature and Extent Study (NES)
initiated due to 15A NCAC 2L.0202(NC2L) Groundwater Standard exceedances of
benzene in MW-4R and vinyl chloride in MW-5R.
• May 2004: Nature and Extent wells NES-1 S&D and NES-2S&D installed.
• May 2005: NES, ACM, & Risk Assessment submitted to the SWS.
• August 21, 2006: ACM Public Meeting held in Oxford, NC.
• June 2008: Corrective Action Plan (CAP) submitted to the SWS.
• December 2008: First Baseline sampling event for MNA
• March 2009: Final Revision of CAP submitted to the SWS.
• April 23, 2009: CAP Approved by the SWS.
• June 2010: Final Baseline sampling event for MNA.
• December 23, 2010: Request for Background Well Replacement approved by the SWS
makes MW-7 (formerly P-2) the new site background monitoring well.
• January 27, 2011: Corrective Action Evaluation Report (CAER) reviewed and approved
by the SWS with an updated list of constituents of concern (COCs), along with the
Alternate Source Demonstration (ASD) for Chromium, Thallium and TDS in MW-IA.
The SWS denied the request to remove selected MNA parameters but allowed a modified
monitoring frequency (beginning June 2011).
• June 9, 2011: The ASD for Iron and Manganese approved by the SWS.
• February 24, 2012: Beta-BHC added to COC list due to confirmed exceedance during
the December 2011 sampling event.
• June 3, 2014: The SWS approved the following: Monitoring wells MW-2, MW-3R,
MW-4R, and MW-6R reverted back to detection monitoring (Appendix I) from assessment
monitoring (Appendix II). NES-1S and NES-ID were removed from the groundwater
corrective action monitoring network. Sampling for Monitored Natural Attenuation
parameters in monitoring wells MW-3R and MW-4R was discontinued.
• July 30, 2015: Corrective Action Evaluation Report (CAER) reviewed and approved by
the SWS with an updated list of COCs, removing 1, 1 -dichloroethane and beta-BHC from
the COC list.
• July 8, 2016: Well NES-ID abandoned.
1.3.2 Re u�ry Status
The Oxford Unit 1 Landfill has remained in Assessment Monitoring since 1995 due to detections
of organic constituents. There were NC2L Standard exceedances of benzene in MW-4R in 2003,
which have not been detected since, and there have been persistent NC2L exceedances of vinyl
August 2018 Semiannual Water Quality Monitoring Report Joyce Engineering
Oxford Unit 1 Landfill, Permit No. 3901-CDLF-1997 December 2018

chloride in MW-5R from 2003 to present. The County received a letter from the SWS dated
August 20, 2003, that requested the County to proceed with assessment activities at Oxford Unit
1 Landfill. A meeting between JOYCE and the SWS was held on February 11, 2004, to discuss
the SWS's requirements for a Nature and Extent Study (NES) and an Assessment of Corrective
Measures (ACM). In May 2005, Granville County submitted a NES (JOYCE, 2005a), and an
ACM (JOYCE, 2005b) and a Quantitative Risk Assessment (QRA) (JOYCE, 2005c) to the SWS
in accordance with 15A NCAC 13B.1634. Granville County held a public meeting for the ACM
on August 21, 2006. A CAP was submitted in June 2008, with revisions in October 2008 and
March 2009 (JOYCE, 2009). The CAP proposed Monitored Natural Attenuation (MNA) as the
primary remedy, supplemented with Control of Decomposition Gasses as a secondary remedy.
The CAP was approved in a letter from the SWS dated April 23, 2009. The gas interception
trench proposed in the Control of Decomposition Gasses was installed July 2009. The last
sampling event for the Baseline MNA was completed in December 2010.
A Request for Background Well Replacement was submitted to the SWS October 25, 2010
because the background monitoring well, MW-1 A, was dry or affected by low water levels and
excessive sediment as well as possible bore seal damage. The request proposed piezometer P-2
to be upgraded and re -named MW-7 to become the facility background monitoring well. The
SWS approved the request on December 23, 2010. MW-7 became the background monitoring
well for the first semiannual sampling event of 2011.
An Alternate Source Demonstration for Iron and Manganese was submitted to the SWS October
26, 2010, after the requirements for additional constituent monitoring for C&D facilities showed
elevated concentrations of iron and manganese across multiple site wells in June 2010. The ASD
showed that the concentrations of iron and manganese were a result of natural occurrence in site
soil and not a release from the landfill. The ASD for Iron and Manganese was approved as
described by the SWS on June 9, 2011.
The first CAER was submitted to the SWS on November 29, 2010, and in a letter dated January
27, 2011, the SWS reviewed and approved the CAER. The SWS denied a request to remove
some of the MNA parameters made on behalf of the county, but did approve a reduced alternate
monitoring frequency as follows; carbon dioxide, ferrous iron, volatile fatty acids, total organic
carbon (TOC), sulfide, and dissolved ethane and ethane for every third year on a semiannual
basis. The SWS also approved removing benzene and cis-1,2-dichloroethylene from the COC
list and adding 1,1-dichloroethane. As a result, the current COC list includes vinyl chloride and
1, 1 -dichloroethane. The ASD for chromium, thallium, and total dissolved solids in MW-1A was
also approved. The Oxford Unit 1 landfill continues in Assessment Monitoring, with additional
C&D indicator parameters and selected MNA parameters and COC monitored at designated
wells at frequencies presented in the January 27, 2011, SWS review of the CAER and ASD and
summarized in the next section.
Beta-BHC was added to the COC list due to confirmed exceedance during the December 2011
sampling event.
August 2018 Semiannual Water Quality Monitoring Report Joyce Engineering
Oxford Unit 1 Landfill, Permit No. 3901-CDLF-1997 December 2018
4

In a letter dated May 22, 2014, Joyce Engineering requested the following changes:
• Revert groundwater monitoring wells MW-2, MW-3R, MW-4R, and MW-6R from
assessment monitoring (Appendix II) to detection monitoring (Appendix I).
• Remove groundwater monitoring wells NES-IS and NES-ID from the groundwater
corrective action monitoring network.
• Discontinue sampling for Monitored Natural Attenuation parameters in groundwater
monitoring wells MW-3R and MW-4R.
The SWS granted approval of the changes in a letter dated June 3, 2014.
The second CAER was submitted to the SWS on July 10, 2015, and in a letter dated July 30,
2015, the SWS reviewed and approved the CAER. The SWS approval included removal of
1,1-dichloroethane and beta-BHC from the COC list due to the lack of recent exceedances. This
left vinyl chloride as the only COC for the facility.
1.4 Hydrogeology
Groundwater in the region generally occurs in the unconfined aquifer that includes both the
saprolite (soil and regolith derived from in -situ weathering of igneous or metamorphic bedrock)
and the underlying fractured bedrock. The transition zone between saprolite and fractured
bedrock is often gradational and can range in thickness from a few inches to several feet.
Typically, the uppermost portion of the fractured bedrock is hydraulically connected to the
overlying saprolite such that they act as a single aquifer. The frequency and connectivity of
fractures normally decreases with depth. The unconfined aquifer is pervasive across the site.
Depth to groundwater is measured in all compliance monitoring wells at the site prior to each
sampling event. The groundwater elevations calculated relative to the surveyed measuring point
(top of casing) for each monitoring well are summarized in Table 2. Historical groundwater
elevation data is found in Appendix C, Table C-01. The groundwater elevation contours shown
in Drawing I are based on data from the August 2018 sampling event. Groundwater flow
beneath the Unit 1 Landfill is primarily to the northeast. Horizontal groundwater gradients were
estimated from the August 2018 groundwater levels and are summarized in Table 3. Horizontal
gradients (i) across the site ranged from 0.0225 to 0.0261. These values are consistent with
previous estimates.
Linear groundwater flow velocities for wells screened in saprolite were computed using the
following modified Darcy equation:
where
V=Ki/ne,
V = average linear velocity (feet/year),
K = hydraulic conductivity (feet/day),
i = horizontal hydraulic gradient, and
ne = effective porosity.
August 2018 Semiannual Water Quality Monitoring Report Joyce Engineering
Oxford Unit 1 Landfill, Permit No. 3901-CDLF-1997 December 2018
5

Under Unit 1, the water table is mostly above top of bedrock so flow is primarily in saprolite;
therefore, the hydraulic conductivity (K = .0731 ft/day) was based on the geometric mean of
values from slug tests conducted on saprolite wells at the facility in 2009 and the effective
porosity (ne) value was estimated at 85% of the laboratory -determined porosity for soil samples
from the facility. Under Unit 2, the water table is mostly below top of bedrock so flow is
primarily in fractured bedrock; therefore, the hydraulic conductivity (K = 4.43 ft/day) was based
on the geometric mean of values from slug tests conducted on bedrock wells at the facility in
2009 and the effective porosity (ne) value for fractured bedrock was estimated at 15%.
Calculations for both Units are presented in Table 3.
The estimated linear groundwater flow velocity under Unit 1 was calculated at about 1.9
feet/year. The modified Darcy equation for linear flow velocity makes the simplifying
assumptions of a homogeneous and isotropic aquifer.
2.0 FACILITY MONITORING PROGRAM
2.1 Groundwater Monitoring Program
Six groundwater monitoring wells comprise the compliance monitoring network at the Oxford
Unit 1 Landfill. The compliance network includes monitoring wells MW-7 (the current facility
background well), MW-2, MW-3R, MW-4R, MW-5R, and MW-6R. In addition, there is one
performance well (NES-2S) that is sampled under the Corrective Action Plan (CAP) for the
facility. The following table summarizes the monitoring network and required analytical
parameters for the two semiannual sampling events:
Groundwater Monitoring Network
Monitoring
Date
Classification
Monitoring
TD
Lithology of Screened
1" SA Event
2"" SA Event
Well
Installed
Program
Interval
Analyses
Analyses
MW-1A
unknown
Observation
Water
Level
28.77
Saprolite
NS
NS
MW-2
unknown
Compliance
Detection
29.34
Saprolite/Bedrock
App. I, C&D
App. I, C&D
MW-3R
8/25/99
Compliance
Detection
27.12
Partially Weathered
App. I, C&D
App. I, C&D
Rock
MW-4R
8/26/99
Compliance
Detection
63.22
Bedrock
App. I, C&D
App. I, C&D
MW-5R
8/25/99
Compliance
Assessment
40.25
Bedrock
App. II, C&D,
App. I + Det.,
MNA
C&D, MNA
MW-6R
8/25/99
Compliance
Detection
42.90
Bedrock
App. I, C&D
App. I, C&D
MW-7
7/28/08
Background
Assessment
34.50
Partially Weathered
App. II, C&D,
App. I + Det.,
Rock
MNA
C&D, MNA
NES-2S
5/11/04
Performance
CAMP
21.5
Saprolite
COC, MNA
COC, MNA
NES-2D
5/11/04
Sentinel
CAMP
66.5
Bedrock
COC, MNA
NS
App. I = NCSWMR Appendix I list of constituents. COC = Constituents of concern.
App. II = NCSWMR Appendix II list of constituents. MNA = Monitoring Natural Attenuation parameters.
App. I + Det. = App. I list plus detected App. II constituents. C&D = C&D indicator parameters.
NS = Not Sampled (After baseline period, sentinel wells are sampled annually).
CAMP = Corrective Action Monitoring Plan.
August 2018 Semiannual Water Quality Monitoring Report Joyce Engineering
Oxford Unit 1 Landfill, Permit No. 3901-CDLF-1997 December 2018
6

C&D indicator parameters: mercury, manganese, iron, sulfate, chloride, alkalinity, total
dissolved solids (TDS), temperature, pH, and specific conductance.
Current Appendix II detected constituents: mercury, sulfide, endosulfan I, and beta-
BHC.
Constituents of Concern: 1, 1 -dichloroethane, vinyl chloride, and beta-BHC.
NINA Field Parameters:
Temperature, pH, specific conductance, oxidation reduction
potential, turbidity, dissolved oxygen on a semiannual basis. Dissolved carbon dioxide,
and ferrous iron are sampled for both sampling events every third year.
MNA Laboratory Parameters: Dissolved hydrogen, dissolved methane, nitrate, sulfate,
chloride, alkalinity on a semiannual basis. Sulfide, TOC, ethane, ethene, and volatile
fatty acids are sampled for both sampling events every third year.
Note that beginning in July 2018, the NCDEQ now requires all landfills to include analysis for
1,4-dioxane for all compliance groundwater and surface water samples (see NCDEQ Memo
dated May 29, 2018).
Monitoring wells MW-3R, MW-4R, MW-5R, and MW-6R replaced MW-3, MW-4, MW-5, and
MW-6, respectively, in August 1999, due to the close proximity to waste of the original wells.
The former background well, MW-1, was abandoned in 2001 after being damaged by a vehicle.
MW-lA was replaced as the background monitoring well by MW-7 in 2011, as described in
Section 1.4.2, above. MW-lA is still monitored for static water level. Monitoring wells NES-
2S, and NES-2D were installed as part of the NES in May 2004.
2.2 Surface Water Monitoring Program
There are two surface water sampling points, SW-1 and SW-2 associated with the Unit 1 landfill.
Sampling point SW-1 is located in a sedimentation basin near the southeast corner of the waste
unit, upgradient of the waste. Sampling point SW-2 is located northeast of the waste unit along a
tributary of Little Grassy Creek, down -gradient of the waste. The surface water samples are
analyzed for the NCSWMR Appendix I list of constituents during both semiannual events.
3.0 FIRST SEMIANNUAL SAMPLING EVENT OF 2018
3.1 Field Work
On August 14-16, 2018, JOYCE personnel visited Oxford Unit 1 Landfill to purge and sample
monitoring wells MW-7, MW-2, MW-3R, MW-4R, MW-5R, MW-6R, and NES-2S, collect
water samples from surface points SW-1 and SW-2, and obtain water levels for MW-lA and
NES-2D.
Monitoring wells were purged and sampled using a 12 volt submersible pump or disposable
bailers. Field measurements of temperature, pH, specific conductivity, and turbidity were
August 2018 Semiannual Water Quality Monitoring Report Joyce Engineering
Oxford Unit 1 Landfill, Permit No. 3901-CDLF-1997 December 2018
7

recorded in a field log for all wells and surface water points. For selected wells, additional MNA
field parameters were also measured and recorded, including dissolved hydrogen which was
sampled with a QED bladder pump. Prior to sampling, laboratory -supplied containers were
prepared with the following information:
• Monitoring well ID (completed by laboratory or field personnel);
• Date and time of sample collection (completed by field personnel);
• Initials of sampling personnel (completed by field personnel);
• Project name and number (completed by the laboratory or field personnel);
• Chemical preservative (completed by the laboratory or field personnel); and
• Requested chemical analyses (completed by the laboratory or field personnel).
Groundwater samples from each monitoring well were collected either immediately after purging
or within 24 hours of the final purge volume and were dispensed directly from the pump flow or
bailers into the provided laboratory containers. Immediately after collection, the samples were
placed in a laboratory provided cooler and chilled on ice. Field sampling logs are provided in
Appendix A.
Surface water samples from SW-1 and SW-2 were collected directly from stream by lowering a
clean, unpreserved sample container into the stream flow and dispensing the water into
laboratory -prepared sample containers. Care was taken to avoid sample -induced turbidity. At the
time of sampling, surface water was also measured for temperature, pH, specific conductivity,
dissolved oxygen, oxidation reduction potential, and turbidity. After sample collection, the
samples were placed in a laboratory provided cooler and chilled on ice. Field sampling logs are
provided in Appendix A.
Due to exceedances for cobalt, chromium, and vanadium, MW-2 was resampled on November 2,
2018, in accordance with the above -described sampling methods and protocols. The field
sampling log for this resample event in included in Appendix A.
3.2 Laboratory Analysis and Quality Control
Pace Analytical Services Inc. of Huntersville, North Carolina analyzed the August 2018
groundwater and surface water samples under chain -of -custody control. Groundwater samples
from the compliance wells were analyzed for the parameters summarized in Section 2.1 plus
1,4-dioxane. The surface water samples were analyzed for NC Appendix I constituents plus
1,4-dioxane. The samples were received by the laboratory August 17, 2018, in good condition,
properly preserved, at proper temperatures, and within analysis hold times.
In addition to samples collected for compliance monitoring at the Oxford Unit 1 Landfill,
JOYCE personnel collected a Field Blank as part of the August 2018 sampling event. The Field
Blank was analyzed for the NC Appendix I plus previously detected Appendix II constituents,
plus iron, manganese and tetrahydrofuran. Also, a Trip Blank that was prepared by the
laboratory accompanied the volatile sampling containers to and from the laboratory. The Trip
August 2018 Semiannual Water Quality Monitoring Report Joyce Engineering
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8

Blank was analyzed for the NC Appendix I1 list of volatile organic compounds and
tetrahydrofuran.
Upon receipt of the laboratory data package, JOYCE personnel reviewed the following data:
• General typographical errors;
• Correct analyses performed and within method specified hold times;
• Biased data results based on Matrix Spike, Matrix Spike Duplicate, and Laboratory
Control Samples;
• Blank qualified data (B-flags);
• Detections above the 15A NCAC 2L (NC2L) Groundwater Standards or NCDEQ Solid
Waste Section Groundwater Water Protection Standards (GWPS), or 15A NCAC 2B
(NC2B) Surface Water Standards; and
• Detections above historical levels.
The complete laboratory analytical packages and chains of custody for the August 2018
sampling event and the November 2018 resampling event are included in Appendix B.
Historical data tables are included in Appendix C. Constituents detected during the August
2018 sampling event are summarized in Table 4. Constituents with exceedances of groundwater
or surface water standards during the August 2018 sampling event are summarized in Table 5.
Field parameters for the August 2018 event are summarized in Table 6.
3.3 Data Analyses
3.3.1 Analtical Results for Groundwater
3.3.1.1 Inorganic Analyses
Inorganic constituents detected at quantified concentrations above the NCDEQ Solid Waste
Section (SWS) report limits (SWSL) in one or monitoring wells during the August 2018 event
include: barium, copper, iron, manganese, alkalinity, chloride, and Total Dissolved Solids (TDS).
A summary of all constituents with detections for the August 2018 event is presented as Table 4.
The laboratory analytical reports, the laboratory quality assurance/quality control information,
and the chains of custody, are included in the Appendix B. Complete historical analytical results
for inorganic constituents are presented in Appendix C, Table C-02.
Iron and manganese were detected at quantified concentrations above their NC2L or GWPS in
several of the monitoring well samples. Iron and manganese were shown to be naturally
occurring in an ASD approved by the NCDEQ-SWS on June 9, 2011.
Cobalt, chromium, and vanadium were detected at quantified concentrations above their
respective NC2L or GWPS in MW-2 during the August 2018 sampling event. The results of a
verification resampling event conducted on November 2, 2018, found significantly lower
concentrations of all three metals, all below the laboratory quantitation limit (QL). Since
estimated detections below the QL are not considered exceedances, the initial exceedances were
refuted.
August 2018 Semiannual Water Quality Monitoring Report Joyce Engineering
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3.3.1.2 Organic Analyses
The only organic constituents detected at quantified concentrations during the August 2018
sampling event were vinyl chloride in MW-5R and 1,4-dioxane in MW-3R, MW-4R, and
MW-5R. These quantified detections were also above the NC2L Standards, and therefore are in
exceedance of the Groundwater Protection Standards (GPS) as defined in 15A NCAC
13B.1634.9. There were no other quantified detections or exceedances for organic constituents.
A summary of all constituents with detections for the August 2018 event is presented as Table 4,
and a summary of groundwater and surface water exceedances for the August 2018 event is
presented as Table 5. The laboratory analytical reports, the laboratory quality assurance/quality
control information, and the chains of custody are included in the Appendix B. Complete
historical analytical results for organic constituents are presented in Appendix C, Table C-03.
3.3.1.3 Performance and Sentinel Wells
Corrective action performance well, NES-2S was sampled for the contaminants of concern
(COCs) list approved by the SWS and for MNA parameters. No COCs were detected above the
SWSL, and therefore there were no GPS exceedances in the sample from the performance well.
Sentinel Well NES-21) was not sampled, but will be sampled during the next semiannual
sampling event. A summary of historical detections of COCs in performance and sentinel wells
for the facility is provided in Appendix C, Table C-04.
3.3.2 Analytical Results for Surface Water
Sampling point SW-1 is located in a sedimentation basin near the southeast corner of the waste
unit, upstream of the waste. Sampling point SW-2 is located northeast of the waste unit along a
tributary of Little Grassy Creek, downstream of the waste.
Surface water analytical results from the site were compared to the 15A-NCAC-2B (NC2B)
surface water standards for protection of freshwater aquatic life or human health, whichever is
lower (more protective) for a given constituent. No organic or inorganic constituents were
detected above their NC2B in SW-1 during the August 2018 event. The detected constituents in
the August 2018 surface water samples are summarized in Table 4.
The analytical results from the August 2018 surface water sampling event at the Oxford Unit 1
Landfill are presented along with historical data in Appendix C, Table C-05. The laboratory
analytical reports, the laboratory quality assurance/quality control information, and the chain of
custody, are included in Appendix B.
August 2018 Semiannual Water Quality Monitoring Report Joyce Engineering
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3.3.3 Statistical Anal
3.3.3.1 Statistical Methods
Monitoring well MW-lA was designated as the background well for the facility until the first
semiannual sampling of 2011. Prior to the spring 2001 sampling event, the site had two
background wells, MW-1 and MW-IA. MW-1 was damaged by a vehicle and, with the approval
of NCDEQ, was abandoned in early 2001. MW-lA was affected by low water levels and impact
from high turbidity levels during more recent events, and was therefore approved to be replaced
by MW-7 as the background for the first semiannual sampling event of 2011. Data from MW-1
between September 1994 and October 2000, data from MW-lA from September 1994 to June
2010 and data from MW-7 from June 2011 to present have been used to determine statistical
background concentrations for inorganic constituents detected at the facility in exceedance of
their respective NC2L or GWPS. Alternatively, intrawell statistics may be used for a
downgradient well by excluding the most recent 6-8 samples and using the earlier results from
that well as the background data.
The background data for inorganic constituents are evaluated in accordance with the procedures
outlined in 15A NCAC 1313.1632 (g) and (h) to determine if the reported concentrations
exceeded the facility background concentrations using the Shapiro -Wilk Test, Parametric
Prediction Limits, Parametric Tolerance Intervals, Aitchison's Adjustment, Non -Parametric
Prediction Limits, and Poisson Prediction Limits as appropriate. Background data, tests for
normality, outliers, Aitchison's adjustment, tolerance interval, or prediction limits are used, as
appropriate based on the background data. The statistical test by which downgradient data are
compared to facility background data is based upon the nature of the data and the number of data
values that are less than the laboratory limit of detection. All statistical tests are evaluated at the
0.05 level of significance, 95% confidence level, and are conducted as one -tailed tests.
3.3.3.2 Results of Statistical Analyses
Iron and manganese were detected in several wells at concentrations above the NC2L standard in
the August 2018 samples. Iron and manganese were shown to be naturally occurring in an ASD
approved by the NCDEQ-SWS on June 9, 2011.
Barium and copper were detected at quantified concentrations in MW-2 and MW-6R,
respectively; however, neither was in exceedance of applicable standards so there was no need
for statistical analyses.
4.0 EVALUATION OF MONITORED NATURAL ATTENUATION (MNA)
4.1 MNA Parameters and Biodegradation Screening Matrix
In accordance with the CAP for the facility, MNA baseline sampling was initiated with the
December 2008 sampling event. The June 2010 sampling event was the fourth and final baseline
sampling event for MNA. MNA sampling was continued in accordance with the modified
sampling frequency approved by NCDEQ-SWS on January 27, 2011.
August 2018 Semiannual Water Quality Monitoring Report Joyce Engineering
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During the August 2018 sampling event, MNA parameters were obtained for the: background
well MW-7, downgradient compliance well MW-5R; and performance well NES-2S. MNA
parameters included field parameters temperature, pH, specific conductance, oxidation reduction
potential, turbidity, dissolved oxygen, as well as laboratory parameters dissolved hydrogen,
nitrate, sulfate, chloride, alkalinity, and methane. In addition, the performance well (NES-2S)
was sampled and analyzed for the COC vinyl chloride. Field parameter data for the August 2018
event are summarized in Table 6. Field data logs and laboratory reports are included in
Appendices A and B, respectively. The MNA parameter data from the August 2018 event, as
well as historical MNA data, are presented in Appendix C, Table C-06.
The MNA parameter data were evaluated in general accordance with the United States
Environmental Protection Agency's (EPA's) Technical Protocol Manual (EPA, 1998) to
determine whether the conditions are conducive to, or whether there is evidence for anaerobic
degradation of the chlorinated hydrocarbons. Specifically, the results were evaluated according
to the weighted system presented in Table 2.3 of the Technical Protocol Manual, referred to
hereafter as the Biodegradation Screening Matrix. According to this manual, a score less than 5
indicates that there is inadequate evidence for anaerobic natural attenuation, a score of 6 to 14
indicates that there is limited evidence for anaerobic natural attenuation, a score of 15 to 19
indicates that there is adequate evidence for anaerobic natural attenuation, and a score of 20 or
more indicates that there is strong evidence that anaerobic natural attenuation is occurring.
The evaluation was performed for data from MW-5R based on the results from the August 2018
sampling event. The Biodegradation Screening Matrix is presented in Table 7 of this report.
One aspect of the scoring process is ambiguous with respect to how it should be applied to a
landfill site such as this facility, and that is the issue of daughter products. Methane, carbon
dioxide (CO2), cis-1,2-dichloroethylene, vinyl chloride, and 1,1-dichlroethane can all be
daughter products produced by the biodegradation of higher -order chlorinated ethanes and
ethenes, and as such, their presence can be strong indicators that biodegradation is occurring, and
are therefore included in the EPA scoring matrix. On the other hand, methane and CO2 are gases
produced by the natural metabolization of biomass by microorganisms in a landfill, and cis-1,2-
dichloroethylene, vinyl chloride, and 1,1-dichloroethane can be primary contaminants leached
from waste in landfills. Some of these compounds are present in the groundwater plume;
however, it is unclear whether or not they are daughter products indicating natural attenuation.
For this reason, the score for MW-5R has been calculated both with and without the points for
daughter products. The following table summarizes the scoring results from Table 7 for both
options for interpreting the data. The scores ranged from 12 to 17 (limited to adequate evidence
of natural attenuation). In reality, the best score is probably in the middle of this range.
Points Awarded
including DP's
Points Awarded
excluding DP's
17
12
DP's = Points for possible daughter products.
August 2018 Semiannual Water Quality Monitoring Report Joyce Engineering
Oxford Unit 1 Landfill, Permit No. 3901-CDLF-1997 December 2018
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Note that the Biodegradation Screening Matrix only evaluates anaerobic degradation of
chlorinated hydrocarbons, especially the dehalogenation of higher -order chlorinated
hydrocarbons such as tetrachloroethene and trichloroethene to the lower -order forms such as
vinyl chloride. Vinyl chloride, which is the only COC at this site, can also degrade aerobically,
and the decrease in the matrix score may indicate that aerobic degradation is the more active
mechanism for natural attenuation of the vinyl chloride at this site. This is supported by some of
the MNA parameters that indicate a more aerobic environment, such as the relatively high
dissolved oxygen concentration and the high oxidation—reduction potential in the area of the
plume. This transition from anaerobic to aerobic degradation, coupled with the fact that the only
remaining COC is vinyl chloride, indicates that the site is in the final stages of natural
attenuation.
4.2 Biochlor Modeling and Mass -Balance Assessment
Anaerobic degradation of organic constituents at this site, specifically chlorinated ethylenes, has
previously been modeled using the EPA Biochlor System; however, Biochlor models the
degradation of higher -order chlorinated hydrocarbons such as tetrachloroethene and
trichloroethene to the lower -order forms such as vinyl chloride. Since the only remaining COC
is vinyl chloride and there have been no quantified detections of any higher -order chlorinated
hydrocarbons in recent sampling events, Biochlor modeling is no longer applicable to this site.
Also, there is evidence that the primary degradation process has shifted from anaerobic to
aerobic, further decreasing the applicability of Biochlor modeling.
4.3 Trend Analysis and Plume Stability
Chart 1 shows the concentration of vinyl chloride (VC) versus time for MW-5 and MW-5R from
June 1994 through August 2018. Similarly, Chart 2 shows the 1, 1 -dichloroethane (1,1-DCA)
concentration versus time for the same time period and the same wells. Both charts include best -
fit trend lines through the MW-5R data and both display decreasing trends. 1,1-dichloroethane
has not been detected in exceedance of the NC2L standard since June 2011. These data show
that the plume is decreasing, and that natural attenuation is adequately controlling and
remediating the plume.
5.0 CONCLUSIONS
Iron and manganese were again detected in several wells at concentrations above the NC2L
standard in the August 2018 samples; however, an ASD showing that iron and manganese are
naturally occurring was approved by NCDEQ-SWS.
Vinyl chloride was detected in MW-5R in exceedance of its NC2L Standard during the August
2018 sampling, which is consistent with historical data. There were no other exceedances for
organic constituents. Overall, the organic detections are consistent with historical data from the
site and indicate decreasing trends. MNA data continues to indicate evidence that natural
attenuation is occurring in the vicinity of MW-5R; however, it appears that aerobic degradation
August 2018 Semiannual Water Quality Monitoring Report Joyce Engineering
Oxford Unit 1 Landfill, Permit No. 3901-CDLF-1997 December 2018
13

of vinyl chloride, rather that anaerobic degradation, is now the dominant mechanism for natural
attenuation at this site. There have been downward trends for all VOCs, included the only
remaining COC, vinyl chloride, indicating that natural attenuation is adequately controlling and
remediating the plume.
The newly required parameter 1,4-dioxane was detected in monitoring well samples MW-3R,
MW-4R, and MW-5R in exceedance of its NC2L standard. It was also detected in surface water
sample SW-2, but it was not in exceedance of the NC2B standard. We recommend that
1,4-dioxane be added to the list of constituents of concern for the Unit 1 landfill. We will
continue to monitor for 1,4-dioxane semiannually, including in the performance well, NES-2S,
and we will look for trends and possible seasonal variations.
The groundwater flow regime is consistent with previous data and the groundwater monitoring
system remains adequate for monitoring the site. The next semiannual sampling event is
tentatively scheduled for August 2018.
6.0 REFERENCES
The references cited herein were used to prepare this document and may or may not be cited in
the text of this report.
Butler, J. Robert, and Secor, Jr., Donald T., 1991, The Central Piedmont, in Horton, J. W., Jr.,
and Zullo, V. A., eds., The Geology of the Carolinas: The University of Tennessee Press,
p. 59-78.
Cowie, S. (2004). Emission of Non -methane Organic Compounds (NMOCs) and hazardous air
Pollutants (HAPs) from Decomposing Refuse and Individual Waste Components and
Under Different Conditions. Master's Thesis, North Carolina State University.
Deisper, A. and Stegmann, R. (1994). The Origin and Fate of Volatile Trace Components in
Municipal Solid Waste Landfills. Waste Management & Research. v. 12, p. 129-139.
Joyce Engineering, (JOYCE), 2005a. Nature and Extent Study, Granville County Oxford
Landfill. May 2005.
JOYCE, 2005b. Assessment of Corrective Measures, Granville County Oxford Landfill. May
2005.
JOYCE, 2005c. Quantitative Risk Assessment, Granville County Oxford Landfill. May 2005.
JOYCE, 2009. Corrective Action Plan, Granville County Oxford Landfill. March 2009.
JOYCE, 2010a. Request for Background Well Replacement, Granville County Oxford Landfill,
Permit # 39-01. October 25, 2010.
August 2018 Semiannual Water Quality Monitoring Report Joyce Engineering
Oxford Unit 1 Landfill, Permit No. 3901-CDLF-1997 December 2018
14

JOYCE, 2010b. Alternate Source Demonstration for Iron and Manganese, Granville County
Oxford C&D Over MSW Landfall, Permit # 39-01. October 26, 2010.
JOYCE, 2010c. Corrective Action Evaluation Report and Alternate Source
Demonstrations, Granville County Oxford C&D Over MSW Landfall, Permit # 39-01.
November 29, 2010.
JOYCE, 2011. Second Semiannual Water Quality Report of 2010, Oxford Landfall, Granville
County, Permit Number 39-01. May 2011.
North Carolina Department of Environment, Health, and Natural Resources, 1997. North
Carolina Solid Waste Management Rules. 15 NCAC 13B.1600. January 1, 1997.
North Carolina Geological Survey, 1985, Geologic map of North Carolina: North Carolina
Department of Natural Resources and Community Development, scale 1:500000.
NRC, 2000. Natural Attenuation for Groundwater Remediation. National Academy Press,
Washington, D.C. pp. 108-111.
USEPA, 1998. Technical Protocol for Evaluating Natural Attenuation of Chlorinated Solvents
in Groundwater. ORD, EPA/600/R-98/128. September 1998.
USEAP, 1992. Statistical Analysis of Groundwater Monitoring Data at RCRA Facilities,
Addendum to Interim Final Guidance. July 1992.
Woodward -Clyde Consultants, 1994. Transition Plan, Oxford Landfall Granville County, North
Carolina. April 1994.
7.0 ACRONYMS
ACM
Assessment of Corrective Measures (report)
AOC
Area of Concern
ASD
Alternate Source Demonstration (report)
C&D
Construction and Demolition Waste
CAP
Corrective Action Plan (report)
CAER
Corrective Action Evaluation Report (report)
CPVC
Chlorinated Poly Vinyl Chloride
COz
Carbon Dioxide
COC
Contaminant of Concern
DCA
Dichloroethane
DCE
Dichloroethylene
DENR
See NCDEQ
DEQ
See NCDENR
August 2018 Semiannual Water Quality Monitoring Report Joyce Engineering
Oxford Unit 1 Landfill, Permit No. 3901-CDLF-1997 December 2018
15

DH Dissolved Hydrogen
DL Detection Limit (for laboratory data)
DO Dissolved Oxygen
EPA United States Environmental Protection Agency
Fee+ Ferrous Iron
GEU Gas Extraction Unit
GPS Groundwater Protection Standards per NCSWMR rule .1634.g.5.
GWPS Groundwater Protection Standards set by the NCDEQ-SWS for constituents with
no NC2L standard.
HASP Site -specific Health and Safety Plan
HDPE High -density Polyethylene
JE Joyce Engineering
JOYCE Joyce Engineering
LFG Landfill Gas
LEL Lower Explosive Limit
MNA Monitored Natural Attenuation
MSW Municipal Solid Waste
MW Monitoring Well
NC 2B North Carolina Surface Water Standards found in 15A NCAC 2B.0101
NC 2L North Carolina Groundwater Standards found in 15A NCAC 2L.0202
NCAC North Carolina Administrative Code
NCDENR North Carolina Department of Environment and Natural Resources
(now NCDEQ)
NCDEQ North Carolina Department of Environmental Quality
(formerly NCDENR)
NCSWMR North Carolina Solid Waste Management Regulations (15A NCAC 13B.1600)
ND Not Detected (for laboratory data)
NES Nature and Extent Study (report)
O&M Operations and Maintenance
ORP Oxidation -Reduction Potential
OSHA Occupational Health and Safety Association
PCE Perchloroethylene (aka — tetrachloroethylene)
PVC Poly Vinyl Chloride
QL Quantitation Limit (for laboratory data)
QRA Quantitative Risk Assessment (report)
RL Reporting Limit (for laboratory data)
SC Specific Conductance
SSI Statistically Significant Increase (over background concentration)
SWQS Surface Water Quality Standards
SWS NCDEQ (or NCDENR) Division of Waste Management, Solid Waste Section
SWSL North Carolina Solid Waste Section Reporting Limits (for laboratory data)
TCE Trichloroethylene
TDS Total Dissolved Solids
TOC Total Organic Carbon
August 2018 Semiannual Water Quality Monitoring Report Joyce Engineering
Oxford Unit 1 Landfill, Permit No. 3901-CDLF-1997 December 2018
16

TSS Total Suspended Solids
VC Vinyl Chloride
VFA Volatile Fatty Acid
VOC Volatile Organic Compound
WQMP Water Quality Monitoring Plan (report)
August 2018 Semiannual Water Quality Monitoring Report
Oxford Unit 1 Landfill, Permit No. 3901-CDLF-1997
Joyce Engineering
December 2018
17

TABLES
Table 1
Monitoring Well Construction Data
Table 2
Groundwater Elevation Data
Table 3
Groundwater Gradients and Calculated Flow Rates
Table 4
Detections of Groundwater and Surface Water Constituents
Table 5
Exceedances of Groundwater and Surface Water Standards
Table 6
Field Parameters
Table 7
Biodegradation Screening Matrix

TABLE 1: Monitoring Well Construction Details
Well ID
Date
Installed
Northing
Easting
GS Elev.
(Ft-AMSL)
TOC Elev.
(Ft-AMSL)
AR
(Bedrock)
(Ft-BGS)
TD (Boring)
(Ft-BGS)
TD
(Fell)
(Ft-BTOC)
TOC
Stick-up
(Ft-AGS)
Top Screen
(Ft-BGS)
Top Screen
(Ft-BTOC)
Bottom
Screen (Ft
BGS)
BottomScreened
Screen (Ft
BTOC)
Lithology
DTW
(Ft-BTOC)
Comments
MW-lA
---
952141.6930
2110755.3908
535.18
538.18
> 22
22.00
25.00
3*
7.00
10.00
22.00
25.00
Saprolite
20.02
Fortner Unit I BackgroundWell, No longer
MW-2
---
953940.0174
2110351.7384
517.00
518.62
21.00
27.50
29.12
1.62
12.50
14.12
27.50
29.12
Sap/BR
10.66
Unit 1 Compliance
MW-3R
08/25/99
954025.5824
2111681.3905
501.3*
503.82
25.00
25.00
32.97
2.5*
14.00
21.97
24.00
31.97
Saprolite
20.24
Unit 1 Compliance
MW-4
---
---
---
---
---
---
---
22.00
---
7.00
---
22.00
---
Bedrock
---
Not Sampled
MW-4R
08/26/99
954975.1334
2110797.9991
504.90
507.34
17.50
60.00
62.44
2.44
50.00
52.44
60.00
62.44
Bedrock
10.28
Unit 1 Compliance
MW-5
---
---
---
---
---
---
---
27.50
---
12.50
---
27.50
---
Sap/BR
---
Not Sampled
MW-5R
08/25/99
954947.2480
2111685.6720
487.24
489.95
22.00
37.00
39.71
2.71
27.00
29.71
37.00
39.71
Bedrock
21.96
Unit 1 Compliance
MW-6R
08/25/99
954725.8325
2110287.6108
504.42
506.81
13.00
40.00
42.39
2.39
30.00
32.39
40.00
42.39
Bedrock
9.25
Unit 1 Compliance
NES-1S
05/01/04
955167.9708
2111057.1915
514.35
516.93
27.00
34.00
36.58
2.58
18.50
21.08
33.50
36.08
Sap/BR
29.90
Unit 1 Perfomance
NES-11)
05/01/04
955177.3548
2111054.7005
514.38
516.62
27.00
79.00
81.24
2.24
63.50
65.74
78.50
80.74
Bedrock
30.03
Unit 1 Sentinel
NES-2S
05/01/04
955091.2902
2111945.3411
474.53
477.20
9.00
21.50
24.17
2.67
11.00
13.67
21.00
23.67
Saprolite
9.14
Unit 1 Perfomance
NES-2D
05/01/04
955081.7805
2111946.7398
474.72
477.43
21.50
66.50
69.21
2.71
51.00
53.71
66.00
68.71
Bedrock
5.00
Unit 1 Sentinel
MW-7
07/28/08
1 953292.1160
2112043.4480
531.24
534.24
34.50
34.50
37.50
3.00
19.50
22.50
34.50
37.50
Saprolite
23.91
Units 1 & 2 Background Well
NOTES: AR = Auger Refusal (Estimate of depth to bedrock).
TD = Total Depth (of boring or well/piezometer).
TOC = Top of Casing
GS = Ground Surface.
DTW = Depth to Water (as measured on 11/20/08).
Ft-BGS = Feet below ground surface.
Ft-AGS = Feet above ground surface.
Ft-AMSL = Feet above mean sea level.
Ft-BTOC = Feet below TOC.
--- = data not available.
* = estimated TOC Stickup, or estimated GS Elev.
MW-3R survey data are after MW-3R was raised and resurveyed in 2012.
MW-3R depths relative to TOC have been adjusted to the new TOC,
but depths BGS have not been adjusted.
Granville County - Oxford Landfill, Unit 1,
Permit 3 90 1 -CDLF- 1997
Joyce Engineering

TABLE 2: Groundwater Elevation Data
Well ID:
Well TOC
Elevation
(Ft-AMSL)
Well Total
Depth
(Feet-BTOC)
Depth to
Groundwater
(Ft-BTOC)
Groundwater
Elevation
(Ft-AMSL)
MW-IA
538.18
28.77
23.46
514.72
MW-7
534.24
34.50
24.02
510.22
MW-2
518.62
29.34
14.18
504.44
MW-3R
503.82
31.63
19.67
484.15
MW-4R
507.34
63.22
8.98
498.36
MW-5R
489.95
40.25
22.47
467.48
MW-6R
506.81
42.90
8.15
498.66
NES-lS
516.93
36.10
-
-
NES-2S
477.20
24.20
6.39
470.81
NES-2D
477.43
69.20
2.97
474.46
Notes:
TOC = top of casing.
Ft-BTOC= Feet below TOC.
Ft-AMSL = Feet above mean sea level.
- = data not available.
Granville Co. - Oxford Landfill, Unit 1
Permit 3901-CDLF-1997 Joyce Engineering

TABLE 3: Groundwater Gradients and Calculated Flow Rates
Date of Water Table Measurements:
August 14, 2018
SEGMENT
HORIZ.
HYDRAULIC
EFFECTIVE
LINEAR
FLOW LINE
SEGMENT
FLOW
BEGIN & END
GRADIENT
CONDUCTIVITY
POROSITY
VELOCITY
LENGTH
SEGMENT
DIRECTION
GW ELEVATION
i
K
n e
V
(feet)
(feet-AMSL)
(ft/da)
(ft/ ear)
500 500
Z 1
1110
NE
0.0225
7.31E-02
0.31
1.94
475
505
Z 2
1341
NNW
0.0261
4.43E+00
0.15
281
470
Average:
0.0243
Average:
141
Notes: Linear flow velocity: V = Kiln ,, (modified Darcy equation).
Along Flow Path i I under Unit 1, the water table is mostly above top of bedrock, so flow is primarily in saprolite.
l 1 Hydraulic conductivity (K) is based on the geometic mean of values from slug tests conducted on saprolite wells at the facility in 2009.
Effective porosity (n,,) value is estimated at 85% of the laboratory -determined porosity for soil samples from the facility.
Along Flow Path i 2 under Unit 2, the water table is mostly below top of bedrock, so flow is primarily in fractured bedrock.
l 2 Hydraulic conductivity (K) is based on the geometic mean of values from slug tests conducted on bedrock wells at the facility in 2009.
Effective porosity (n,,) value for fractured bedrock is estimated at 15%.
Refer to Drawing 1 for flow line segments.
Granville Co. - Oxford Landfill
Permit # 3901-CDLF-1997 Joyce Engineering

TABLE 4: Detections of Groundwater and Surface Water Constituents
SAMPLE
NC2L/
COLLECT
PARAMETER
RESULT
UNITS
MDL
MRL
ID
GWPS*/NC2B**
DATE
3901-MW2
Alkalinity, Total as CaCO3
22,100
µg/l
1000
5000
NE
8/16/2018
3901-MW2
Arsenic
5.3 J
µg/l
5.0
10.0
10
8/16/2018
3901-MW2
Barium
21.7 J
µg/l
2.5
100
700
8/16/2018
3901-MW2
Chromium
12.5
µg/I
2.5
10.0
10
8/16/2018
3901-MW2*
Chromium
4.1J
µg/1
2.5
10.0
10
11/2/2018
3901-MW2
Cobalt
11.6
µg/I
2.5
10.0
1 *
8/16/2018
3901-MW2*
Cobalt
8.3J
µg/l
2.5
10.0
1*
11/2/2018
3901-MW2
Copper
7.4 J
µg/l
2.5
10.0
1000
8/16/2018
3901-MW2
Iron
14,000
µg/I
25.0
300
300
8/16/2018
3901-MW2
Manganese
284
µg/I
2.5
50.0
50
8/16/2018
3901-MW2
Nickel
5.5 J
µg/l
2.5
50.0
100
8/16/2018
3901-MW2
Sulfate
7690 J
µg/l
500
250000
250,000
8/16/2018
3901-MW2
Total Dissolved Solids, Dissolved
238,000
µg/l
25000
25000
500,000
8/16/2018
3901-MW2
Vanadium
34.5
µg/I
2.5
25.0
0.3*
8/16/2018
3901-MW2*
Vanadium
13.OJ
µg/l
2.5
25.0
0.3*
11/2/2018
3901-MW2
Zinc
15.3
µg/l
5.0
10.0
1000
8/16/2018
3901-MW3R
1,4-Dioxane (p-Dioxane)
16.5
µg/I
1.9
2.0
3
8/16/2018
3901-MW3R
Alkalinity, Total as CaCO3
93,200
µg/l
1000
5000
NE
8/16/2018
3901-MW3R
Barium
16.6 J
µg/l
2.5
100
700
8/16/2018
3901-MW3R
Chromium
3.2 J
µg/l
2.5
10
10
8/16/2018
3901-MW3R
Copper
2.8 J
µg/l
2.5
10
1000
8/16/2018
3901-MW3R
Iron
1,200
µg/I
25.0
300
300
8/16/2018
3901-MW3R
Manganese
63.6
µg/I
2.5
50.0
50
8/16/2018
3901-MW3R
Nickel
3.4 J
µg/l
2.5
50
100
8/16/2018
3901-MW3R
Sulfate
7,130
µg/l
0.5
250
250,000
8/16/2018
3901-MW3R
Total Dissolved Solids, Dissolved
164,000
µg/l
25000
25000
500000
8/16/2018
3901-MW3R
Vanadium
2.6 J
µg/l
2.5
25
0.3*
8/16/2018
3901-MW3R
Zinc
6.6 J
µg/l
5.0
10.0
1000
8/16/2018
3901-MW4R
1,4-Dioxane (p-Dioxane)
21.2
µg/I
1.9
2.0
3
8/16/2018
3901-MW4R
Alkalinity, Total as CaCO3
302,000
µg/l
1000
5000
NE
8/16/2018
3901-MW4R
Barium
39.9 J
µg/l
2.5
100
700
8/16/2018
3901-MW4R
Iron
75.5 J
µg/l
25.0
300
300
8/16/2018
3901-MW4R
Manganese
937.0
µg/I
2.5
50.0
50
8/16/2018
3901-MW4R
Sulfate
6,470 J
µg/l
500
250000
250,000
8/16/2018
3901-MW4R
Total Dissolved Solids, Dissolved
458,000
µg/l
25000
25000
500000
8/16/2018
Oxford Unit 1, Granville Co. Joyce Engineering
Permit No. 39-01 Page 1 of 3

TABLE 4: Detections of Groundwater and Surface Water Constituents
SAMPLE
NC2L/
COLLECT
PARAMETER
RESULT
UNITS
MDL
MRL
ID
GWPS*/NC2B**
DATE
3901-MW5R
1,1-Dichloroethane
2.4 J
µg/l
0.32
5.0
6
8/16/2018
3901-MW5R
1,2-Dichlorobenzene
1.2 J
µg/l
0.30
5.0
20
8/16/2018
3901-MW5R
1,4-Dichlorobenzene
1.1
µg/l
0.33
1.0
6
8/16/2018
3901-MW5R
1,4-Dioxane (p-Dioxane)
41.6
µg/I
1.9
2.0
3
8/16/2018
3901-MW5R
Alkalinity, Total as CaCO3
192,000
µg/l
1000
5000
NE
8/16/2018
3901-MW5R
Barium
41.6 J
µg/1
2.5
100
700
8/16/2018
3901-MW5R
Benzene
0.35 J
µg/l
0.25
1.0
1 *
8/16/2018
3901-MW5R
Chlorobenzene
1.11
µg/l
0.23
3.00
50
8/16/2018
3901-MW5R
cis-1,2-Dichloroethene
1.2 J
µg/l
0.19
5.0
70
8/16/2018
3901-MW5R
Manganese
105
µg/I
2.5
50.0
50
8/16/2018
3901-MW5R
Sulfate
4,200 J
µg/1
500
250000
250,000
8/16/2018
3901-MW5R
Total Dissolved Solids, Dissolved
303,000
µg/l
25000
25000
500000
8/16/2018
3901-MW5R
Vinyl chloride
3.5
µg/I
0.62
1.0
0.03
8/16/2018
3901-MW6R
1, 1 -Dichloroethane
0.93 J
µg/l
0.32
5.0
6
8/16/2018
3901-MW6R
Alkalinity, Total as CaCO3
203,000
µg/l
1000
5000
NE
8/16/2018
3901-MW6R
Barium
108
µg/l
2.5
100
700
8/16/2018
3901-MW6R
cis-1,2-Dichloroethene
0.62 J
µg/l
0.19
5.0
70
8/16/2018
3901-MW6R
Iron
1,180
µg/I
25.0
300
300
8/16/2018
3901-MW6R
Manganese
1,870
µg/I
2.5
50.0
50
8/16/2018
3901-MW6R
Sulfate
2,650 J
µg/l
500
250000
250,000
8/16/2018
3901-MW6R
Total Dissolved Solids, Dissolved
509,000
µg/I
25000
25000
500000
8/16/2018
3901-MW-7
Alkalinity, Total as CaCO3
124,000
µg/1
1000
5000
NE
8/16/2018
3901-MW-7
Barium
3.8 J
µg/l
2.5
100
700
8/16/2018
3901-MW-7
Chloride
9,720
µg/l
500
1000
250,000
8/16/2018
3901-MW-7
Iron
340
µg/I
25.0
300
300
8/16/2018
3901-MW-7
Manganese
6.7 J
µg/l
2.5
50.0
50
8/16/2018
3901-MW-7
Sulfate
51,400 J
µg/l
500
250000
250,000
8/16/2018
3901-MW-7
Total Dissolved Solids, Dissolved
249,000
µg/l
25000
25000
500000
8/16/2018
3901-NES-2S
Barium
25.8 J
µg/l
2.5
100
700
8/16/2018
3901-NES-2S
Vanadium
2.5 J
µg/l
2.5
25
0.3*
8/16/2018
3901-SW1
Barium
19.11
µg/l
2.5
100
NE
8/16/2018
3901-SW1
Copper
3.9 J
µg/l
2.5
10
7
8/16/2018
3901-SW1
Iron
3,320
µg/l
25.0
300
NE
8/16/2018
3901-SW1
Manganese
176
µg/l
2.5
50.0
NE
8/16/2018
3901-SW1
Vanadium
7.6 J
µg/l
2.5
25
NE
8/16/2018
3901-SW1
Zinc
6.2 J
µg/l
5.0
10.0
36
8/16/2018
Oxford Unit 1, Granville Co. Joyce Engineering
Permit No. 39-01 Page 2 of 3

TABLE 4: Detections of Groundwater and Surface Water Constituents
SAMPLE
ID
PARAMETER
RESULT
UNITS
MDL
MRL
NC2L/
GWPS*/NC2B**
COLLECT
DATE
3901-SW2
1,4-Dioxane (p-Dioxane)
4.5
µg/1
1.9
2.0
80
8/16/2018
3901-SW2
Barium
28.3 J
µg/l
2.5
100
NE
8/16/2018
3901-SW2
Chromium
3.2 J
µg/l
2.5
10
7
8/16/2018
3901-SW2
Copper
3.0 J
µg/l
2.5
10
11
8/16/2018
3901-SW2
Iron
2,750
µg/1
25.0
300
NE
8/16/2018
3901-SW2
Manganese
45.2 J
µg/1
2.5
50.0
NE
8/16/2018
3901-SW2
Vanadium
5.8 J
µg/1
2.5
25
NE
8/16/2018
NOTES: All results in micrograms ner liter (us/1'
MDL = Method Detection Limit
MRL = Method Reuortin¢ Limit
NC21, = NC Groundwater Standard from 15A NCAC 2L.0202
NC2B = NC Surface Water Standard for fresh -water aquatic life from 15A-NCAC-2B
GWPS = NC Solid Waste Section Groundwater Protection Standard (for constituents with no NC2L1
NE = Not Established
J = Estimated concentration below the MRL
Bold values= Detections above the NC2L. GWPS. or NC2B stardards (see Table 51
*RESAMPLE 11/2/2018
Oxford Unit 1, Granville Co. Joyce Engineering
Permit No. 39-01 Page 3 of 3

TABLE 5: Exceedances of Groundwater and Surface Water Standards
SAMPLE
NC2L/
COLLECT
PARAMETER
RESULT
UNITS
MDL
MRL
ID
GWPS*/NC2B**
DATE
3901-MW2
Chromium
12.5
µg/l
2.5
10.0
10
8/16/2018
3901-MW2*
Chromium
4.1J
µg/l
2.5
10.0
10
11/2/2018
3901-MW2
Cobalt
11.6
µg/l
2.5
10.0
1 *
8/16/2018
3901-MW2*
Cobalt
8.3J
µg/l
2.5
10.0
1 *
11/2/2018
3901-MW2
Iron
14,000
µg/l
25.0
300
300
8/16/2018
3901-MW2
Manganese
284
µg/1
2.5
50.0
50
8/16/2018
3901-MW2
Vanadium
34.5
µg/1
2.5
25.0
0.3*
8/16/2018
3901-MW2*
Vanadium
13.OJ
µg/l
2.5
25.0
0.3*
11/2/2018
3901-MW3R
1,4-Dioxane (p-Dioxane)
16.5
µg/l
1.9
2.0
3
8/16/2018
3901-MW3R
Iron
1,200
µg/l
25.0
300
300
8/16/2018
3901-MW3R
Manganese
63.6
µg/1
2.5
50.0
50
8/16/2018
3901-MW4R
1,4-Dioxane (p-Dioxane)
21.2
µg/1
1.9
2.0
3
8/16/2018
3901-MW4R
Manganese
937
µg/1
2.5
50.0
50
8/16/2018
3901-MW5R
1,4-Dioxane (p-Dioxane)
41.6
µg/l
1.9
2.0
3
8/16/2018
3901-MW5R
Manganese
105
µg/1
2.5
50.0
50
8/16/2018
3901-MW5R
Vinyl chloride
3.5
µg/1
0.62
1.0
0.03
8/16/2018
3901-MW6R
Iron
1,180
µg/1
25.0
300
300
8/16/2018
3901-MW6R
Manganese
1,870
µg/l
2.5
50.0
50
8/16/2018
3901-MW6R
Total Dissolved Solids, Dissolved
509,000
µg/l
25000
25000
500,000
8/16/2018
3901-MW-7
Iron
340
µg/l
25.0
300
300
8/16/2018
NOTES: All results in micrograms per liter (up-4)
MDL =
Method Detection Limit
MRL =
Method Reporting Limit
NC2L
= NC Groundwater Standard from 15A NCAC 2L.0202
NC213
= NC Surface Water Standard for fresh -water aquatic life from 15A-NCAC-2B
GWPS
= NC Solid Waste Section Groundwater Protection Standard (for constituents with no NC2L)
Oxford Unit 1 Landfill, Granville Co. Joyce Engineering
Permit No. 39-01

TABLE 6: Field Parameters
WELL ID
PARAMETER
RESULT
UNITS
DATE
3901-MW2
pH
5.99
S.U.
8/16/2018
3901-MW2
Temperature
19.6
°C
8/16/2018
3901-MW2
Conductivity
90.1
µS/cm
8/16/2018
3901-MW2
Turbidity
113.5
NTU
8/16/2018
3901-MW2
Dissolved Oxygen
1.91
mg/1
8/16/2018
3901-MW2
Oxidation Reduction Potential
26.0
mV
8/16/2018
3901-MW2
Static Water Level
14.18
ft
8/16/2018
3901-MW2
Well Depth
29.34
ft
8/16/2018
3901-MW2*
pH
5.99
S.U.
11/2/2018
3 901-MW2 *
Temperature
19.6
°C
11/2/2018
3901-MW2*
Conductivity
90.1
µS/cm
11/2/2018
3901-MW2*
Turbidity
113.5
NTU
11/2/2018
3901-MW2*
Dissolved Oxygen
1.91
mg/l
11/2/2018
3901-MW2*
Oxidation Reduction Potential
26.0
my
11/2/2018
3901-MW2*
Static Water Level
14.18
ft
11/2/2018
3901-MW2*
Well Depth
29.34
ft
11/2/2018
3901-MW3R
pH
6.01
S.U.
8/15/2018
3901-MW3R
Temperature
19.9
°C
8/15/2018
3901-MW3R
Conductivity
265.4
µS/cm
8/15/2018
3901-MW3R
Turbidity
26.02
NTU
8/15/2018
3901-MW3R
Dissolved Oxygen
3.08
mg/l
8/15/2018
3901-MW3R
Oxidation Reduction Potential
44.2
my
8/15/2018
3901-MW3R
Static Water Level
19.67
ft
8/15/2018
3901-MW3R
Well Depth
31.63
ft
8/15/2018
3901-MW4R
pH
7.32
S.U.
8/16/2018
3901-MW4R
Temperature
16.4
°C
8/16/2018
3901-MW4R
Conductivity
656.0
µS/cm
8/16/2018
3901-MW4R
Turbidity
4.37
NTU
8/16/2018
3901-MW4R
Dissolved Oxygen
6.04
mg/l
8/16/2018
3901-MW4R
Oxidation Reduction Potential
36.6
my
8/16/2018
3901-MW4R
Static Water Level
8.98
ft
8/16/2018
3901-MW4R
Well Depth
63.22
ft
8/16/2018
3901-MW5R
pH
6.46
S.U.
8/16/2018
3901-MW5R
Temperature
16.1
°C
8/16/2018
3901-MW5R
Conductivity
469.0
µS/cm
8/16/2018
3901-MW5R
Turbidity
2.79
NTU
8/16/2018
3901-MW5R
Dissolved Oxygen
2.87
mg/l
8/16/2018
3901-MW5R
Oxidation Reduction Potential
31.2
my
8/16/2018
3901-MW5R
Static Water Level
22.47
ft
8/16/2018
3901-MW5R
Well Depth
40.25
ft
8/16/2018
Oxford Unit 1 Landfill, Granville Co. Joyce Engineering
Permit No. 39-01 1 of 2

TABLE 6: Field Parameters
WELL ID
PARAMETER
RESULT
UNITS
DATE
3901-MW6R
pH
6.96
S.U.
8/15/2018
3901-MW6R
Temperature
19.8
°C
8/15/2018
3901-MW6R
Conductivity
794
µS/cm
8/15/2018
3901-MW6R
Turbidity
2.73
NTU
8/15/2018
3901-MW6R
Dissolved Oxygen
4.0
mg/1
8/15/2018
3901-MW6R
Oxidation Reduction Potential
61.9
mV
8/15/2018
3901-MW6R
Static Water Level
8.15
ft
8/15/2018
3901-MW6R
Well Depth
42.90
ft
8/15/2018
3901-MW7
pH
6.61
S.U.
8/15/2018
3901-MW7
Temperature
17.9
°C
8/15/2018
3901-MW7
Conductivity
364.1
µS/cm
8/15/2018
3901-MW7
Turbidity
4.64
NTU
8/15/2018
3901-MW7
Dissolved Oxygen
5.4
mg/l
8/15/2018
3901-MW7
Oxidation Reduction Potential
50.9
mV
8/15/2018
3901-MW7
Static Water Level
24.02
ft
8/15/2018
3901-MW7
Well Depth
37.32
ft
8/15/2018
3901-NES2S
pH
6.02
S.U.
8/16/2018
3901-NES2S
Temperature
28.1
°C
8/16/2018
3901-NES2S
Conductivity
246.8
µS/cm
8/16/2018
3901-NES2S
Turbidity
17.35
NTU
8/16/2018
3901-NES2S
Dissolved Oxygen
1.09
mg/l
8/16/2018
3901-NES2S
Oxidation Reduction Potential
49.5
my
8/16/2018
3901-NES2S
Static Water Level
6.39
ft
8/16/2018
3901-NES2S
Well Depth
24.20
ft
8/16/2018
3901-SW 1
pH
7.19
S.U.
8/16/2018
3901-SW 1
Temperature
29.4
°C
8/16/2018
3901-SW1
Conductivity
137.2
µS/cm
8/16/2018
3901-SW1
Turbidity
72.94
NTU
8/16/2018
3901-SW2
pH
7.92
S.U.
8/16/2018
3901-SW2
Temperature
22.5
°C
8/16/2018
3901-SW2
Conductivity
175.6
µS/cm
8/16/2018
3901-SW2
Turbidity
38.24
NTU
8/16/2018
Notes: mg/l = milligrams per liter
°C= degrees Centigrade.
S.U.= Standard Units.
ft = feet.
µg/l = micrograms per liter.
µS/cm = microSemens per centimeter.
NTU = Nephelometric Turbidity Units.
Oxford Unit 1 Landfill, Granville Co. Joyce Engineering
Permit No. 39-01 2 of 2

TABLE 7: BIODEGRADATION SCREENING MATRIX (MW-5R)
Parameter
Concentration
in Plume
Interpretation
Possible
Points
Points Awarded
with DP points
Points Awarded
without DP points
Oxygen
< 0.5 mg/1
Tolerated, suppresses the reductive pathway at higher
3
0
0
concentrations
> 5 mg/l
Not tolerated; however, vinyl chloride may be oxidized
-3
0
0
aerobically
Nitrate
< 1 mg/l
At higher concentrations may compete with reductive
2
2
2
pathway
Iron II (Ferrous Iron)
> 1 mg/l
Reductive pathway possible; vinyl chloride may be
3
0
0
oxidized under Fe (111) - reducing conditions
Sulfate
< 20 mg/l
At higher concentrations may compete with reductive
2
2
2
pathway
Sulfide
> 1 mg/1
Reductive pathway possible
3
0
0
Methane
< 0.5 mg/1
Vinyl chloride oxidizes
0
> 0.5 mg/l
Ultimate reductive daughter product, vinyl chloride
3
0
0
accumulates
Oxidation Reduction
< 50 mV
Reductive pathway possible
1
1
1
Potential
< -100 mV
Reductive pathway likely
2
pH
5 < pH < 9
Optimal range for reductive pathway
0
0
0
5 > pH > 9
Outside optimal range for reductive pathway
-2
TOC
> 20 mg/l
Carbon and energy source; drives dechlorination; can
2
0
0
be natural or anthropogenic
Temperature
>200 C
At T > 200C biochemical process is accelerated
1
0
0
Carbon Dioxide
> 2x background
Ultimate oxidative daughter product
1
1
0
Alkalinity
> 2x background
Results from interaction between CO2 and
1
0
0
aquifer minerals
Chloride
> 2x background
Daughter product of organic chlorine
2
2
2
Hydrogen
> 1 nM
Reductive pathway possible
3
3
3
< 1 nM
Vinyl chloride oxidizes
0
0
0
Volatile Fatty Acids
> 0.1 mg/1
Intermediates resulting from biodegradation of more
2
2
2
complex compounds; carbon and energy source
BTEX
> 0.1 mg/l
Carbon and energy source; drives dechlorination
2
0
0
Tetrachloroethene (PCE)
---
Material released
0
0
0
Trichloroethene (TCE)
---
Material released
0
0
0
---
Daughter product of PCE
2
0
0
Dichloroethenes (DCE)
---
Material released
0
0
Daughter product of TCE
2
2
Dichloroethene, cis-1,2,
---
Material released
0
0
0
---
Daughter product of trichlorethene
2
Vinyl Chloride (VC)
---
Material released
0
0
---
Daughter product of DCE
2
2
1,1,1-Trichloroethane (TCA)
---
Material released
0
0
0
1, 1 -Dichloroethane (DCA)
---
Material released
0
0
0
Daughter product of TCA
2
Chloroethane
---
Daughter product of dichloroethane or vinyl chloride
under reducing conditions
2
0
0
Ethene/Ethane
> 0.01 mg/1
Daughter products of vinyl chloride/ethene
2
> 0.1 mg/l
3
0
0
Chloroform
---
Material released
0
0
0
---
Daughter product of carbon tetrachloride
2
0
0
Dichloromethane (MC)
---
Material released
0
0
0
(Methylene Chloride)
---
Daughter product of chloroform
2
0
0
Based on data collected in August 2018. Total Points Awarded:
17
12
mg/L = miligrams per liter
mV = millivolts
nM = Nanometer
C = Celcius
NOTE: Chloroethane, Methane, TCE, DCE, cis-1,2-DCE, MC, VC, DCA, and CQ are all present in the plume; however,
it is uncertain whether these are primary leachate constituents or daughter products (DPs); therefore, we
have two calculation columns. The first column assumes all of these are daughter products, and the
NA = Not Analyzed second column assumes none of them are. The true score is probably between the two.
BTEX = Sum of Benzene, Toluene, Ethylbenzene, and Total Xylenes
This screening matrix is prepared in general accordance with the United Stated Environmental Protection Agency's
(EPA's) Table 2.3 Analytical Parameters and Weighted for Preliminary Screeningfor Anaerobic Biodegradation
Process presented in the EPA's Technical Protocol for Evaluating Natural Attenuation of Chlorinated Solvents
in Groundwater, September 1988.
SCORE:
Evid. of Nat. Allen.
< 5
inadequate
6-14
limited
15-19
adequate
> 20
strong
Granville County - Oxford Landfill Permit 3901-CDLF-1997 Joyce Engineering

CHARTS
Chart 1 Vinyl Chloride in MW-5 & MW-5R vs. Time
Chart2 1,1-Dichloroethane in MW-5 & MW-5R vs. Time

J
bA
35.00
F-
30.00
25.00
10.00
L 11
1 11
CHART 1: Vinyl Chloride vs. Time in MW-5 & MW-SR
I-4-MW-5
LIl M lD lD I� n x W M M O O -1 r-I fV N M M'T IzT M M lD lD I- n W x M M O O -1 .-I cV N M M�IzT M M lD lD I, TI- x x
Ql Ql Ol T T T Ol T T T Ol O O O O O O O O O O O O O O O O O O O O-� -�- -� -� -� -� r� -� -� -� r� -� -� r� r� -�
qA -0 hA -0 bA -0 hA -0 qA -0 hA -0 on -0 hA -0 on -0 hA -0 hA -0 hA -0 bA -0 hA -0 hA -0 M -0 hA -0 M -0 hA -0 M -0 hA -0 M -0 t7A -0 on -0 hA
QL.L Q U- Q U- QL.L Q U- QL.L Q U- QL.L Q U- QL.L Q U- QL.L Q U- QL.L QL.L QL.L Q U- QL.L QL.L Q U- QL.L Q U- QL.L Q U- Q

12
10
14
CHART 2: 1,1-Dichloroethane vs. Time in MW-5 & MW-5R

FIGURE
Figure 1 Site Location Map (USGS Topographic Map)

• _..N6y9Yg0k.
P
a
T2
9
NUADRANGLES
TEU.S. .S. 5 MI T TOPO RAPHIC ti'� �`��FOR SATTERWHITE, STOVALL,�a
�BEREA AND OXFORD, NORTH CAROLINA. ; S�
OXFORD LANDFILL Vr� DESIGNED RWH PROJECT NO.
GRANVILLE COUNTY, NORTH CAROLINA AJLI i `L DRACHECKED ce SCALE 660
EM31"EERIIV1:3 APPROVED GVB
SITE LOCATION MAP DATE 10/15/15 1" = 2000' DRAWING NO.
2211 W. MEADOWVIEW ROAD
GREENSBORO, NC 27407 0 2018 Joyce Engineering, Inc. 1
PHONE: [phone] All dgh. reserved. NC CORP LIC: C-0782
L\GranAI.\dwg\0zfa d\, 2014 site Location Mw.dwg

DRAWING
Drawing 1 Groundwater Potentiometric Surface Map

9 4"—
SW-4 —
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- MW-7 GROUNDWATER CONTOURS MAY NOT REFLECT
510.22 a 1 ACTUAL GROUNDWATER CONDITIONS.
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APPENDICES
Appendix A Field Sampling Logs
Appendix B Laboratory Reports with Chains of Custody
Appendix C Historical Tables

Appendix A
Field Sampling Logs

__ DATE: 8/16/2018
.iJ it EE
EN�IIVEEFtIfv�� GROUND WATER SAMPLING LOG
Project Name: OXFORD, Granville Co. Project No. /Task No.: 2180175.02
Well ID: MW-2 Sampler(s): S.Slebodnik / R. Mesubed
Well Location: Behind SED. Basin at corner of landfill
Well Diameter:
2
inches
Initial Depth to Water (DTW):
14.18
feet
Depth to Bottom (DTB):
29.34
feet
Water Column Thickness (WCT):
15.16
feet [DTB-DTW]
Calculation for One Well Volume (WV):
For 2" Well: WCT X 0.163 =
2.47
gallons
For 4" Well: WCT X 0.653 =
gallons
For THREE Well Volumes: WV X 3 =
7.41
gallons
Actual Amount Purged/Bailed:
7.41
gallons
Purged with: Disposable Bailer
Sampled with: Disposable Bailer
Depth to Water before Sampling: --
feet
Gallons
Time
Temp.
°C
pH
Cond.
(µS/cm)
Turb.
NTU
Initials
0
1400
18.0
6.15
87.9
64.75
RM
2.47
1404
16.9
5.88
79.5
78.20
RM
4.94
1407
16.2
5.87
78.5
131.0
RM
7.41
1412
16.0
5.97
80.0
117.1
RM
Before
Sampling
1424
19.6
5.99
90.1
113.5
RM
Comments (weather conditions, odor, color, silt, etc.): The weather was sunny with
Signatures Date: P9114 / 13
QA/QC Sign Off: Date: I f-Z1 fj� r %

EJlIGIN'EERII'�'C
DATE: 08/ 14-15/18
GROUND WATER SAMPLING LOG
Project Name: OXFORD, Granville Co. Project No./Task No.: 2180175/02
Well ID: MW-3R Sampler(s): S. Slebodnik/ R. Mesubed
Well Location: Backside of landfill, turn right at tire pile, down trail
Well Diameter:
Initial Depth to Water (DTW):
Depth to Bottom (DTB):
Water Column Thickness (WCT):
Calculation for One Well Volume (WV):
For 2" Well:
For 4" Well:
WCT X 0.163
WCT X 0.653
For THREE Well Volumes: WV X 3
Actual Amount Purged/Bailed:
Purged with: Disposable Bailer
Sampled with: Disposable Bailer
2
inches
19.67
feet
31.63
feet
11.96
feet [DTB-DTW]
1.94 gallons
= eallons
= 5.82 gallons
4.54 gallons
Depth to Water before Sampling: 19.59 feet
Gallons
Time
Temp.
°C
pH
Cond.
(AS/cm)
Turb.
NTU
Initials
0
1446
19.1
8.16
278.4
125.4
SS
1.94
1450
17.5
8.05
261.9
294.5
SS
3.88
1453
16.9
6.13
243.4
337.3
SS
Dry @ 4.54 gal
08/15/18
Before
Sampling
1250
19.9
6.01
265.4
26.02
SS
Comments weather conditions, odor, color, silt, etc.):_.): The weather was sunny with
temperatures in the 60's on 08/14/18 and 08/15/18. The well was purged on 08/14/18 and
sampled on 08/15/18. Turbidity was 57.81 NTU on the 2°d bailer.
Signature: � i7� Date: D lls-I $
QA/QC Sign Off: �� � Date: /2ZZI-Al

_ DATE: 08/15-16/18
IrI
r iw add
E"C31fU'EEF?1f\A'G GROUND WATER SAMPLING LOG
Project Name: OXFORD, Granville Co. Project No./Task No.: 2180175/02
Well ID: MW-4R Sampler(s): R. Mesubed/S. Slebodnik
Well Location: Backside of landfill, near road
Well Diameter:
2
inches
Initial Depth to Water (DTW):
8.98
feet
Depth to Bottom (DTB):
63.22
feet
Water Column Thickness (WCT):
54.24
feet [DTB-DTW]
Calculation for One Well Volume (WV):
For 2" Well: WCT X 0.163 =
8.84
gallons
For 4" Well: WCT X 0.653 =
gallons
For THREE Well Volumes: WV X 3 =
26.5
gallons
Actual Amount Purged/Bailed:
12.82
gallons
Purged with: Disposable Bailer
Sampled with: Disposable Bailer
Depth to Water before Sampling: 16.40
feet
Gallons
Time
Temp.
°C
pH
Cond.
(PS/cm)
Turb.
NTU
Initials
0
0825
19.4
7.32
573
13.12
SS
8.84
0850
16.3
7.34
678
179.0
SS
Dry @ 12.82
08/16/18
Before
Sampling
0824
16.4
7.32
656
4.37
SS
Comments (weather conditions, odor, color, silt, etc.): The weather was sunny with
temperatures in the 60's on 08/15/18 and sunny with temperatures in the 80's on 08/16/18. The
well was purged on 08/15/18 and sampled on 08/16/18. Turbidity was 8.10 NTU on the 2"a
bailer; 10 bottles were sampled
Signature: A ,,t, Date: 09116148
QA/QC Sign Off: JVg160 // Date: 2

DATE: 08/15-16/18
EJlIGIIVEERII`1AG GROUND WATER SAMPLING LOG
Project Name: OXFORD, Granville Co. Project No. /Task No.: 2180175.02
Well ID: MW-5R Sampler(s): S. Slebodnik/R. Mesubed
Well Location: Far end of road
Well Diameter:
2
inches
Initial Depth to Water (DTW):
22.47
feet
Depth to Bottom (DTB):
40.25
feet
Water Column Thickness (WCT):
17.78
feet [DTB-DTW]
Calculation for One Well Volume (WV):
For 2" Well: WCT X 0.163 =
2.89
gallons
For 4" Well: WCT X 0.653 =
gallons
For THREE Well Volumes: WV X 3 =
8.69
gallons
Actual Amount Purged/Bailed:
8.69
gallons
Purged with: Disposable Bailer
Sampled with: Disposable Bailer
Depth to Water before Sampling: 22.51 feet
Gallons
Time
Temp.
°C
Dis.02
mg/L
Cond.
(µS/cm)
pH
ORP
mV
Turb.
NTU
Initials
0
0949
16.0
4.44
466
6.84
34.8
5.11
SS
2.89
0954
15.6
5.83
466.8
6.59
46.7
3.67
SS
5.78
0959
15.4
5.75
461.4
6.45
50.6
1.69
SS
8.69
1002
15.3
5.22
456.6
6.38
54.1
2.98
SS
08/16/18
Before
Sampling
0810
16.10
2.87
469.0
6.46
31.2
12.79
SS
Comments (weather conditions, odor, color, silt, etc.): The weather was sunny with
temperatures in the 60's on 08/15/18 and sunny with temperatures in the 80's on 08/16/18. The
well was purged on 08/15/18 and sampled on 08/16/18. 1 bottle of dis. H+ was sampled with a
bladder pump; 10 sec discharge time and 10 sec fill time; 8 bottles were sampledp
Signature: AdWle- 97Yji4'r,l Date: Of 116 US
QA/QC Sign Off: , Date: 1 ZMA f

DATE: 08/ 14-15/18
EE
ENGiNEEIGr1N� GROUND WATER SAMPLING LOG
Project Name: OXFORD, Granville Co. Project No. /Task No.: 2180175/02
Well ID: MW-6R Sampler(s): R. Mesubed/S. Slebodnik
Well Location: Back corner beyond MW-6
Well Diameter:
2
inches
Initial Depth to Water (DTW):
8.15
feet
Depth to Bottom (DTB):
42.90
feet
Water Column Thickness (WCT):
34.75
feet [DTB-DTW]
Calculation for One Well Volume (WV):
For 2" Well: WCT X 0.163 =
5.66
gallons
For 4" Well: WCT X 0.653 =
gallons
For THREE Well Volumes: WV X 3 =
16.99
gallons
Actual Amount Purged/Bailed:
16.99
gallons
Purged with: Disposable Bailer
Sampled with: Disposable Bailer
Depth to Water before Sampling: 8.19
feet
Gallons
Time
Temp.
°C
pH
Cond.
(PS/CM)
Turb.
NTU
Initials
0
1545
21.2
6.97
753
3.01
SS
5.66
1553
16.1
7.04
727
30.58
SS
11.33
1606
16.1
6.95
734
125.3
SS
16.99
1617
15.9
7.07
725
555.5
SS
08/15/18
Before Sampling
1020
19.8
6.96
794
2.73
SS
Comments (weather conditions, odor, color, silt, etc.): The weather was sunny with
temperatures in the 60's on 08/14/18 and 08/15/18. The well was purged on 08/14/18 and
sampled on 08/15/18. Turbidity was 9.43 NTU on the 2°d bailer, 10 bottles sampled.
Signature: U Date: 0911rIlk
QA/QC Sign Off: A40 Date:—. 12- ?r/l I

__ DATE: 08/ 14-15/ 18
i�LJ I
ENGIl�IEE►�ll'vt� GROUND WATER SAMPLING LOG
Project Name: OXFORD, Granville Co. Project No. /Task No.: 2180175/02
Well ID: MW-7 Sampler(s): R. Mesubed/S. Slebodnik
Well Location: _ Unit 2 area, near power lines
Well Diameter:
2
inches
Initial Depth to Water (DTW):
24.02
feet
Depth to Bottom (DTB):
37.32
feet
Water Column Thickness (WCT):
13.30
feet [DTB-DTW]
Calculation for One Well Volume (WV):
For 2" Well: WCT X 0.163 =
2.16
gallons
For 4" Well: WCT X 0.653 =
gallons
For THREE Well Volumes: WV X 3 =
6.5
gallons
Actual Amount Purged/Bailed:
6.5
gallons
Purged with: Disposable Bailer
Sampled with: Disposable Bailer
Depth to Water before Sampling: 24.13
feet
Gallons
Time
Temp.
°C
DO
mg/L
Cond.
(AS/cm)
pH
ORP
Turb.
NTU
Initials
0
1419
19.8
5.63
413.8
6.50
49.8
7.57
RM
2.16
1424
19.9
4.49
388.8
6.32
41.9
134.0
RM
4.32
1428
16.7
5.19
366.4
6.34
37.0
437.8
RM
6.5
1433
16.9
5.99
362.5
6.32
33.8
818.2
RM
08/15/18
Before
Sampling
1051
17.9
5.40
364.1
6.61
50.9
4.64
RM
Comments (weather conditions, odor, color, silt, etc.): The weather was sunny with
temperatures in the 60's on 08/14/18 and 08/15/18. The well was purged on 08/14/18 and
sampled on 08/15/18. 1 bottle of dis. H+ was sampled with a bladder pump,• 5 sec discharge time
and 5 sec fill time
Signature: &tWA4 Date: 0 0IS-119
QA/QC Sign Off: Date: 12/0l / F,

DATE: 08/ 14-15/ 18
�.
AJ
il�+►!(V� LRlNC GROUND WATER SAMPLING LOG
Project Name: OXFORD, Granville Co. Project No./Task No.: 2180175.02
Well ID: NES-2S Sampler(s):
S. Slebodnik / R. Mesubed
Well Location: Near MW-4R
Well Diameter:
2
inches
Initial Depth to Water (DTW):
6.39
feet
Depth to Bottom (DTB):
24.20
feet
Water Column Thickness (WCT):
17.81
feet [DTB-DTW]
Calculation for One Well Volume (WV):
For 2" Well: WCT X 0.163 =
2.90
gallons
For 4" Well: WCT X 0.653 =
gallons
For THREE Well Volumes: WV X 3 =
8.70
gallons
Actual Amount Purged/Bailed:
8.70
gallons
Purged with: Disposable Bailer
Sampled with: Disposable Bailer
Depth to Water before Sampling: 6.44
feet
Gallons
Time
Temp.
(°C)
pH
S.U.
Cond.
(µS/cm)
DO
(mg/L)
ORP
(mV)
Turb.
(NTU)
Initials
0
1508
22.6
6.39
135.7
4.43
54.8
143.7
SS
2.90
1514
17.8
6.13
135.4
6.01
60.7
63.35
SS
5.80
1519
17.1
6.16
141.9
6.05
61.7
135.1
SS
8.70
1527
17.4
6.31
144.4
5.51
63.7
64.78
SS
08/15/18
Before
Sampling
1416
28.1
6.02
246.8
1.09
49.5
17.35
SS
Comments (weather conditions, odor, color, silt, etc.): .): The weather was sunny with
temperatures in the 60's on 08/14/18 and 08/15/18. The well was purged on 08/14/18 and
sampled on 08/15/18. 1 bottle of dis. H+ was sampled with a bladder pump; 5 sec discharge and
5 sec fill time. Turbidity was 13.86 NTU on the 2"d bailer
Signature:
QA/QC Sign Off.
Date: bIl«-l!g
Date:

DATE: 08/16/18
E1VCRI"EEI?IP4'C9 SURFACE WATER MONITORING LOG
Project Name: OXFORD, Granville Co. Project/Task No.: 2180175.02
Surface Point ID: -SW- 1 Sampler(s): S. Slebodnik/R. Mesubed
Location: Sediment pond near rip -rap
Field Parameters:
Time of Sampling:
1335
pH:
7.19
Temperature:
29.4 (°C)
Conductivity:
137.2 (µS/cm)
Turbidity:
72.94 (NTU)
Comments/Sample Description (weather conditions, odor, color, silt, etc.): The
weather was sunny with temperatures in the 80s on 08/16/18.
Sketch of Sample Location (include flow direction, drainage pathways, etc.):
'I;rZ
r,11a'
QA/QC Sign Off:
Date:_ QiLnc LIE
Dater 4/-if

DATE: 08/16/18
E"C31MEEFUM3 SURFACE WATER MONITORING LOG
Project Name: OXFORD, Granville Co. Project/Task No.: 2180175/02
Surface Point ID: SW-2 Sampler(s): S. Slebodnik/R. Mesubed
Location: Back corner, near property line
Field Parameters:
Time of Sampling:
0930
pH:
7.92
Temperature:
22.5 (° C)
Conductivity:
175.6 (PS/cm)
Turbidity:
38.24 (NTU)
Comments/Sample Description (weather conditions, odor, color, silt, etc.): The
weather was sunny with temperatures in the 80s on 08/16/18,
A
QA/QC Sign Off: A�
Date: U 1 l G / /8
Date: I Z�/ I// __

LaBella
Project Name: ____
Gravw,ue' —-
Location:
KeetIr. G Q=J_
2211W. Meadowview Rd Suite 101
Project No.:
2022-.0 1-raSK:01 "Y -
Greensboro, NC 27407
Sampled By:
Nn.Ls" 6e-4
Telephone: [phone]
Facsimile: [phone]
Dale:
pZ
WELL I.D.: W _a
Weather:
WELL SAMPLING INFORMATION
Well Diameter: /t
`-
Static Water Level:
-•�
Depth of Woll: �
Length of Wcll Screen: --• - - - -- -
Measuring Point:
- —
De hlh to Tor of Pulp: - --- - - - -- - -- - -- - -
ump Type:
-- iG �t
o fit �V inji&c_
_
E'n�h►ru'Tx,1 ruhing Tyne:-
FIEL•`DPARAIETER MF.ASiiRFMT.NT
Time
Pump hate
Gallons
Purged
pFl Temp Conductivity Turbidity Dissolved 02 Redox Alkalinity Iron (II) Comments
- +/- 0. I - - +/- 3 i, (NTU) (m./L) (rn _
+ I Q9r +/ 10 mV
(l
[o�rnL s-sc.�
1 •
S•�1
•�
2
.2
y
I
•� , �
Q-13 1 110
I$3
I t�,� zoc
.3
i�•S
o.+
4.13 Q. 1 3
I
oov„� Zasa
5.3i
I,I
.g
� t S t
zo3
20$
oorv�� ioscc
too.n�/2osu
S,3y-�
5-38
2i3
toornr.30w-
-'42
90.
i Z$
toornL/3oscc
S tF
I-0
0 .t
-101. I ts55
' II►t.
23
jin
-.C1
1.2
}
-I12,i 2v
233
pow.L 3pt.0
0
T-41
I� K
I.4
oz.
.S3 -Its•} SK
00,,,,E �s
• `Fo
i •3
238
Icolml, i„
xj.S
Ii�i
$•
�1•
�I�
ti•�o -II.
12 3
S 43
�}
0.
l
0 �-I�•3.3 I 15:
tas3
[00w'1- wL'k 1
•o
S 4-L-
543
11.1
1if. 0
S
13.9
o s3
o•'W1
'Ibtal
riwCG
t;nllonc hr.
.... •,I
-►3�•I I5•$3
Purge Time Purge Time End: 1
Start:
OBSERNLAX-1OINS -
Notes::rP�,v,sfgJ}la Qum( I�ctd w. rO' 'I s 't a'war %6L,- •i-n S+u V - 6.4- V D+ aA
1P Mfls''� -+n� q
f` -vM WL • 10•3N- 14 -112'� -R&tA nth Wets g•I61 LZi rJe %{ovy ht4e_ � AAUg'I.1.1o1 tt �h.,�f
V 1NeA1 4f"r' amvAng down qnA qmw i"v,6'I4
Final Static Water- Level:
n In
Pw�� wtia �ag�- &,hd Tqjk 1%,Lhgj • vz"e' ca"ta iw CL") tnC&--'ed CtjU1Ce.; 4w,+Cj i•-' 9wh-av Ca 13tS \'M' . 1,t►�,d�+� s�a6,[;us•

L LaBeRa
Project Name: �('')MnVAV- - 0x&Aj
Location: N e v
Proiect No.: 1 p22,� �LiSk:b1 a
2211W. Meadowview Rd Suite 101
Greensboro, NC 27407 Sampled By: -
Telephone: [phone]
Facsimile: [phone] Date: (,l 02-
WELL I.D.: Weather:
WELL SAMPLING INFORMATION
Well Diameter:
Depth of Well: -_ army _.
Measuring Point:
Pump Type: —Pftd. �I_ c-�— L
.u6 J
Static Water Level: e1u„�
Length of Well Screen:
Depth to Top of PuiVp:
uhtng Type:
Time
I $
Pump Rale
--
Gallons--
Purged
--
--pll
Temp
°C
Conductivity
(mS/cm)
Turhidily DISSOIVCd 02 Redox Alkalinity Iron (II) Comments
(NTIJ) (m,/L) —(mV)
+ 1017, +/- 10 mV
43.1 '+.1 3
I
+/- 0.1
.13
1'+.
+/- 3`%
a• 4
I
"Total
Gallons Pnra*rrl
Purge Time Purge Time End: Final Static Water Level:
Start:
OWERVAIrIONS
Notcs:vk-►=,vd L 1�00 '�r .93,wtft'- vNu1 A bakfW .set / mf� T►14i'xI
� Qh un-6
E�a P+mccrt 6la nt� }uKivt @ 1 3S' ©ut±»c�- o� CJct a a,e- IV s;,te r lost
^jc i 9 btrft. su ,�-ple�

Appendix B
Laboratory Reports with
Chains of Custody

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
August 30, 2018
Mr. Van Burbach
Joyce Engineering -NC
2211 West Meadowview Rd
Boone Bldg, Suite 101
Greensboro, NC 27407
RE: Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
Dear Mr. Burbach:
Enclosed are the analytical results for sample(s) received by the laboratory on August 17, 2018. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
��i Flo _ _.1I , .�:
Nicole Gasiorowski
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Daniel Girdner, LaBella Associates, D.P.C.
Miguel Vazquez, Joyce Engineering
Rochelle mesubed, Joyce Engineering
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 45

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 45

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92396265001
3901-MW2
Water
08/16/18 14:24
08/17/18 09:37
92396265002
3901-MW3R
Water
08/15/18 12:50
08/17/18 09:37
92396265003
3901-MW4R
Water
08/16/18 08:24
08/17/18 09:37
92396265004
3901-MW5R
Water
08/16/18 08:10
08/17/18 09:37
92396265005
3901-MW6R
Water
08/15/18 10:20
08/17/18 09:37
92396265006
3901-SW1
Water
08/16/18 13:35
08/17/18 09:37
92396265007
3901-SW2
Water
08/16/18 09:30
08/17/18 09:37
92396265008
Trip Blank
Water
08/15/18 05:30
08/17/18 09:37
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 45

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Oxford Compliance Unit 1
92396265
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92396265001
3901-MW2
EPA 601 OD
DS
16
PASI-A
EPA6020B
JMW1
1
PASI-A
EPA 7470A
RDT
1
PASI-A
EPA 8260E
CAH
51
PASI-C
EPA 8260B Mod.
DLK
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
SM 2540C-2011
CEH
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
92396265002
3901-MW3R
EPA 601 OD
DS
16
PASI-A
EPA6020B
JMW1
1
PASI-A
EPA 7470A
RDT
1
PASI-A
EPA 8260E
CAH
51
PASI-C
EPA 8260B Mod.
DLK
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
SM 2540C-2011
CEH
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
92396265003
3901-MW4R
EPA 601 OD
DS
16
PASI-A
EPA6020B
JMW1
1
PASI-A
EPA 7470A
RDT
1
PASI-A
EPA 8260E
CAH
51
PASI-C
EPA 8260B Mod.
DLK
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
SM 2540C-2011
CEH
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
92396265004
3901-MW5R
EPA 601 OD
DS
16
PASI-A
EPA6020B
JMW1
1
PASI-A
EPA 7470A
JMW1
1
PASI-A
EPA 8260E
CAH
51
PASI-C
EPA 8260B Mod.
DLK
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
SM 2540C-2011
CEH
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
92396265005
3901-MW6R
EPA 601 OD
DS
16
PASI-A
EPA6020B
JMW1
1
PASI-A
EPA 7470A
RDT
1
PASI-A
EPA 8260E
CAH
51
PASI-C
EPA 8260B Mod.
DLK
3
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 45

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Oxford Compliance Unit 1
Pace Project No.:
92396265
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
SM 2320B-2011
ECH
1
PASI-A
SM 2540C-2011
CEH
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
92396265006
3901-SW1
EPA 601 OD
DS
16
PASI-A
EPA6020B
JMW1
1
PASI-A
EPA 8260E
CAH
51
PASI-C
EPA 8260B Mod.
DLK
3
PASI-C
92396265007
3901-SW2
EPA 601 OD
DS
16
PASI-A
EPA6020B
JMW1
1
PASI-A
EPA 8260E
CAH
51
PASI-C
EPA 8260B Mod.
DLK
3
PASI-C
92396265008
Trip Blank
EPA 8260E
CAH
51
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 5 of 45

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
Lab Sample ID
Method
92396265001
EPA 601 OD
EPA 601 OD
EPA 601 OD
EPA 601 OD
EPA 601 OD
EPA 601 OD
EPA 601 OD
EPA 601 OD
EPA 601 OD
EPA 601 OD
SM 2320B-2011
SM 2540C-2011
EPA 300.0 Rev 2.1 1993
92396265002
EPA 601 OD
EPA 601 OD
EPA 601 OD
EPA 601 OD
EPA 601 OD
EPA 601 OD
EPA 601 OD
EPA 601 OD
EPA 8260B Mod.
SM 2320B-2011
SM 2540C-2011
EPA 300.0 Rev 2.1 1993
92396265003
EPA 601 OD
EPA 601 OD
EPA 601 OD
EPA 8260B Mod.
SM 2320B-2011
SM 2540C-2011
EPA 300.0 Rev 2.1 1993
SUMMARY OF DETECTION
Client Sample ID
Parameters
Result
Units
Report Limit
Analyzed
3901-MW2
Arsenic
5.3J
ug/L
10.0
08/25/18 22:21
Barium
21.7J
ug/L
100
08/25/18 22:21
Chromium
12.5
ug/L
10.0
08/25/18 22:21
Cobalt
11.6
ug/L
10.0
08/25/18 22:21
Copper
7AJ
ug/L
10.0
08/25/18 22:21
Iron
14000
ug/L
300
08/25/18 22:21
Manganese
284
ug/L
50.0
08/25/18 22:21
Nickel
5.5J
ug/L
50.0
08/25/18 22:21
Vanadium
34.5
ug/L
25.0
08/25/18 22:21
Zinc
15.3
ug/L
10.0
08/25/18 22:21
Alkalinity, Total as CaCO3
22100
ug/L
5000
08/27/18 23:22
Total Dissolved Solids
238000
ug/L
25000
08/18/18 00:55
Sulfate
7690J
ug/L
250000
08/24/1810:22
3901-MW3R
Barium
16.6J
ug/L
100
08/25/18 22:25
Chromium
3.2J
ug/L
10.0
08/25/18 22:25
Copper
2.8J
ug/L
10.0
08/25/18 22:25
Iron
1200
ug/L
300
08/25/18 22:25
Manganese
63.6
ug/L
50.0
08/25/18 22:25
Nickel
3AJ
ug/L
50.0
08/25/18 22:25
Vanadium
2.6J
ug/L
25.0
08/25/18 22:25
Zinc
6.6J
ug/L
10.0
08/25/18 22:25
1,4-Dioxane (p-Dioxane)
16.5
ug/L
2.0
08/23/18 18:23
Alkalinity, Total as CaCO3
93200
ug/L
5000
08/24/18 21:10
Total Dissolved Solids
164000
ug/L
25000
08/17/18 22:52
Sulfate
7130J
ug/L
250000
08/25/18 08:06
3901-MW4R
Barium
39.9J
ug/L
100
08/25/18 22:28
Iron
75.5J
ug/L
300
08/25/18 22:28
Manganese
937
ug/L
50.0
08/25/18 22:28
1,4-Dioxane (p-Dioxane)
21.2
ug/L
2.0
08/23/18 20:59
Alkalinity, Total as CaCO3
302000
ug/L
5000
08/28/18 10:10
Total Dissolved Solids
458000
ug/L
25000
08/18/18 00:55
Sulfate
6470J
ug/L
250000
08/25/18 08:23
92396265004
3901-MW5R
EPA 601 OD
Barium
41.6J
ug/L
100
08/25/18 22:31
EPA 601 OD
Manganese
105
ug/L
50.0
08/25/18 22:31
EPA 8260B
Benzene
0.35J
ug/L
1.0
08/28/18 19:26
EPA 8260B
Chlorobenzene
1.1 J
ug/L
3.0
08/28/18 19:26
EPA 8260B
1,2-Dichlorobenzene
1.2J
ug/L
5.0
08/28/18 19:26
EPA 8260B
1,4-Dichlorobenzene
1.1
ug/L
1.0
08/28/18 19:26
EPA 8260B
1,1-Dichloroethane
2AJ
ug/L
5.0
08/28/18 19:26
EPA 8260B
cis-1,2-Dichloroethene
1.2J
ug/L
5.0
08/28/18 19:26
EPA 8260B
Vinyl chloride
3.5
ug/L
1.0
08/28/18 19:26
EPA 8260B Mod.
1,4-Dioxane (p-Dioxane)
41.6
ug/L
2.0
08/23/18 21:19
SM 2320B-2011
Alkalinity, Total as CaCO3
192000
ug/L
5000
08/27/18 23:42
REPORT OF LABORATORY ANALYSIS
Qualifiers
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 6 of 45

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
Lab Sample ID
Method
92396265004
SM 2540C-2011
EPA 300.0 Rev 2.1 1993
92396265005
EPA 6010D
EPA 6010D
EPA 6010D
EPA 8260B
EPA 8260B
SM 2320B-2011
SM 2540C-2011
EPA 300.0 Rev 2.1 1993
92396265006
EPA 6010D
EPA 6010D
EPA 6010D
EPA 6010D
EPA 6010D
EPA 6010D
92396265007
EPA 6010D
EPA 6010D
EPA 6010D
EPA 6010D
EPA 6010D
EPA 6010D
EPA 8260B Mod.
Client Sample ID
Parameters
3901-MWSR
Total Dissolved Solids
Sulfate
3901-MW6R
Barium
Iron
Manganese
1,1-Dichloroethane
cis-1,2-Dichloroethene
Alkalinity, Total as CaCO3
Total Dissolved Solids
Sulfate
3901-SW1
Barium
Copper
Iron
Manganese
Vanadium
Zinc
3901-SW2
Barium
Chromium
Copper
Iron
Manganese
Vanadium
1,4-Dioxane (p-Dioxane)
SUMMARY OF DETECTION
Result Units Report Limit Analyzed
303000
ug/L
25000
08/18/18 00:55
4200J
ug/L
250000
08/25/18 09:14
108
ug/L
100
08/25/18 22:34
1180
ug/L
300
08/25/18 22:34
1870
ug/L
50.0
08/25/18 22:34
0.93J
ug/L
5.0
08/28/1819:43
0.62J
ug/L
5.0
08/28/1819:43
203000
ug/L
5000
08/24/18 21:24
509000
ug/L
25000
08/17/18 22:52
2650J
ug/L
250000
08/25/18 09:31
19.1 J
ug/L
100
08/25/18 22:37
3.9J
ug/L
10.0
08/25/18 22:37
3320
ug/L
300
08/25/18 22:37
176
ug/L
50.0
08/25/18 22:37
7.6J
ug/L
25.0
08/25/18 22:37
6.2J
ug/L
10.0
08/25/18 22:37
28.3J
ug/L
100
08/25/18 22:40
3.2J
ug/L
10.0
08/25/18 22:40
3.OJ
ug/L
10.0
08/25/18 22:40
2750
ug/L
300
08/25/18 22:40
45.2J
ug/L
50.0
08/25/18 22:40
5.8J
ug/L
25.0
08/25/18 22:40
4.5
ug/L
2.0
08/23/18 21:57
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Qualifiers
Page 7 of 45

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
Sample: 3901-MW2 Lab ID: 92396265001 Collected: 08/16/18 14:24 Received: 08/17/18 09:37 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
7470 Mercury
Mercury
8260 MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
Date: 08/30/2018 12:04 PM
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
ND
ug/L
6.0
3.9
1
08/25/18 07:40
08/25/18 22:21
7440-36-0
5.3J
ug/L
10.0
5.0
1
08/25/18 07:40
08/25/18 22:21
7440-38-2
21.7J
ug/L
100
2.5
1
08/25/18 07:40
08/25/18 22:21
7440-39-3
ND
ug/L
1.0
0.50
1
08/25/18 07:40
08/25/18 22:21
7440-41-7
ND
ug/L
1.0
0.50
1
08/25/18 07:40
08/25/18 22:21
7440-43-9
12.5
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:21
7440-47-3
11.6
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:21
7440-48-4
7.4J
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:21
7440-50-8
14000
ug/L
300
25.0
1
08/25/18 07:40
08/25/18 22:21
7439-89-6
ND
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:21
7439-92-1
284
ug/L
50.0
2.5
1
08/25/18 07:40
08/25/18 22:21
7439-96-5
5.5J
ug/L
50.0
2.5
1
08/25/18 07:40
08/25/18 22:21
7440-02-0
ND
ug/L
10.0
5.0
1
08/25/18 07:40
08/25/18 22:21
7782-49-2
ND
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:21
7440-22-4
34.5
ug/L
25.0
2.5
1
08/25/18 07:40
08/25/18 22:21
7440-62-2
15.3
ug/L
10.0
5.0
1
08/25/18 07:40
08/25/18 22:21
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
ND ug/L 5.5 0.020 1 08/18/18 06:19 08/29/18 17:12 7440-28-0
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
ND ug/L 0.20 0.10 1 08/22/1814:24 08/24/1812:23 7439-97-6
Analytical Method: EPA 8260E
ND
ug/L
100
ND
ug/L
200
ND
ug/L
1.0
ND
ug/L
3.0
ND
ug/L
1.0
ND
ug/L
3.0
ND
ug/L
10.0
ND
ug/L
100
ND
ug/L
100
ND
ug/L
1.0
ND
ug/L
3.0
ND
ug/L
10.0
ND
ug/L
5.0
ND
ug/L
1.0
ND
ug/L
13.0
ND
ug/L
3.0
ND
ug/L
1.0
ND
ug/L
10.0
ND
ug/L
5.0
ND
ug/L
1.0
ND
ug/L
100
ND
ug/L
5.0
10.0
1
08/28/18 18:38
67-64-1
1.9
1
08/28/18 18:38
107-13-1
0.25
1
08/28/18 18:38
71-43-2
0.17
1
08/28/18 18:38
74-97-5
0.18
1
08/28/18 18:38
75-27-4
0.26
1
08/28/18 18:38
75-25-2
0.29
1
08/28/18 18:38
74-83-9
0.96
1
08/28/18 18:38
78-93-3
1.2
1
08/28/18 18:38
75-15-0
0.25
1
08/28/18 18:38
56-23-5
0.23
1
08/28/18 18:38
108-90-7
0.54
1
08/28/18 18:38
75-00-3
0.14
1
08/28/18 18:38
67-66-3
0.11
1
08/28/18 18:38
74-87-3
2.0
1
08/28/18 18:38
96-12-8
0.21
1
08/28/18 18:38
124-48-1
0.27
1
08/28/18 18:38
106-93-4
0.21
1
08/28/18 18:38
74-95-3
0.30
1
08/28/18 18:38
95-50-1
0.33
1
08/28/18 18:38
106-46-7
1.0
1
08/28/18 18:38
110-57-6
0.32
1
08/28/18 18:38
75-34-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 45

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
Sample: 3901-MW2 Lab ID: 92396265001 Collected: 08/16/18 14:24 Received: 08/17/18 09:37 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill Analytical Method: EPA 8260E
1,2-Dichloroethane
ND
ug/L
1.0
0.24
1
08/28/18 18:38
107-06-2
1,1-Dichloroethene
ND
ug/L
5.0
0.56
1
08/28/18 18:38
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
5.0
0.19
1
08/28/18 18:38
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
5.0
0.49
1
08/28/18 18:38
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.27
1
08/28/18 18:38
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.13
1
08/28/18 18:38
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.26
1
08/28/18 18:38
10061-02-6
Ethylbenzene
ND
ug/L
1.0
0.30
1
08/28/18 18:38
100-41-4
2-Hexanone
ND
ug/L
50.0
0.46
1
08/28/18 18:38
591-78-6
lodomethane
ND
ug/L
10.0
0.32
1
08/28/18 18:38
74-88-4
Methylene Chloride
ND
ug/L
1.0
0.97
1
08/28/18 18:38
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
100
0.33
1
08/28/18 18:38
108-10-1
Styrene
ND
ug/L
1.0
0.26
1
08/28/18 18:38
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
5.0
0.33
1
08/28/18 18:38
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
3.0
0.40
1
08/28/18 18:38
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.46
1
08/28/18 18:38
127-18-4
Tetrahydrofuran
ND
ug/L
10.0
3.1
1
08/28/18 18:38
109-99-9
Toluene
ND
ug/L
1.0
0.26
1
08/28/18 18:38
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.48
1
08/28/18 18:38
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.29
1
08/28/18 18:38
79-00-5
Trichloroethene
ND
ug/L
1.0
0.47
1
08/28/18 18:38
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.20
1
08/28/18 18:38
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.41
1
08/28/18 18:38
96-18-4
Vinyl acetate
ND
ug/L
50.0
0.35
1
08/28/18 18:38
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.62
1
08/28/18 18:38
75-01-4
Xylene (Total)
ND
ug/L
5.0
0.66
1
08/28/18 18:38
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
97
%
70-130
1
08/28/18 18:38
460-00-4
1,2-Dichloroethane-d4 (S)
98
%
70-130
1
08/28/18 18:38
17060-07-0
Toluene-d8 (S)
97
%
70-130
1
08/28/18 18:38
2037-26-5
8260 MSV SIM
Analytical Method: EPA 8260E Mod.
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1.9
1
08/23/18 20:40
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
96
%
50-150
1
08/23/18 20:40
17060-07-0
Toluene-d8 (S)
113
%
50-150
1
08/23/18 20:40
2037-26-5
2320B Alkalinity
Analytical Method: SM
2320B-2011
Alkalinity, Total as CaCO3
22100
ug/L
5000
1000
1
08/27/18 23:22
2540C Total Dissolved Solids
Analytical Method: SM
2540C-2011
Total Dissolved Solids
238000
ug/L
25000
25000
1
08/18/18 00:55
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1
1993
Sulfate
7690J
ug/L
250000
500
1
08/24/1810:22
14808-79-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/30/2018 12:04 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 45

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
Sample: 3901-MW3R Lab ID: 92396265002 Collected: 08/15/18 12:50 Received: 08/17/18 09:37 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
7470 Mercury
Mercury
8260 MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
Date: 08/30/2018 12:04 PM
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
ND
ug/L
6.0
3.9
1
08/25/18 07:40
08/25/18 22:25
7440-36-0
ND
ug/L
10.0
5.0
1
08/25/18 07:40
08/25/18 22:25
7440-38-2
16.6J
ug/L
100
2.5
1
08/25/18 07:40
08/25/18 22:25
7440-39-3
ND
ug/L
1.0
0.50
1
08/25/18 07:40
08/25/18 22:25
7440-41-7
ND
ug/L
1.0
0.50
1
08/25/18 07:40
08/25/18 22:25
7440-43-9
3.2J
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:25
7440-47-3
ND
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:25
7440-48-4
2.8J
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:25
7440-50-8
1200
ug/L
300
25.0
1
08/25/18 07:40
08/25/18 22:25
7439-89-6
ND
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:25
7439-92-1
63.6
ug/L
50.0
2.5
1
08/25/18 07:40
08/25/18 22:25
7439-96-5
3.4J
ug/L
50.0
2.5
1
08/25/18 07:40
08/25/18 22:25
7440-02-0
ND
ug/L
10.0
5.0
1
08/25/18 07:40
08/25/18 22:25
7782-49-2
ND
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:25
7440-22-4
2.6J
ug/L
25.0
2.5
1
08/25/18 07:40
08/25/18 22:25
7440-62-2
6.6J
ug/L
10.0
5.0
1
08/25/18 07:40
08/25/18 22:25
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
ND ug/L 5.5 0.020 1 08/18/18 06:19 08/29/18 17:15 7440-28-0
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
ND ug/L 0.20 0.10 1 08/22/1814:24 08/24/1812:30 7439-97-6
Analytical Method: EPA 8260E
ND
ug/L
100
ND
ug/L
200
ND
ug/L
1.0
ND
ug/L
3.0
ND
ug/L
1.0
ND
ug/L
3.0
ND
ug/L
10.0
ND
ug/L
100
ND
ug/L
100
ND
ug/L
1.0
ND
ug/L
3.0
ND
ug/L
10.0
ND
ug/L
5.0
ND
ug/L
1.0
ND
ug/L
13.0
ND
ug/L
3.0
ND
ug/L
1.0
ND
ug/L
10.0
ND
ug/L
5.0
ND
ug/L
1.0
ND
ug/L
100
ND
ug/L
5.0
10.0
1
08/28/18 18:54
67-64-1
1.9
1
08/28/18 18:54
107-13-1
0.25
1
08/28/18 18:54
71-43-2
0.17
1
08/28/18 18:54
74-97-5
0.18
1
08/28/18 18:54
75-27-4
0.26
1
08/28/18 18:54
75-25-2
0.29
1
08/28/18 18:54
74-83-9
0.96
1
08/28/18 18:54
78-93-3
1.2
1
08/28/18 18:54
75-15-0
0.25
1
08/28/18 18:54
56-23-5
0.23
1
08/28/18 18:54
108-90-7
0.54
1
08/28/18 18:54
75-00-3
0.14
1
08/28/18 18:54
67-66-3
0.11
1
08/28/18 18:54
74-87-3
2.0
1
08/28/18 18:54
96-12-8
0.21
1
08/28/18 18:54
124-48-1
0.27
1
08/28/18 18:54
106-93-4
0.21
1
08/28/18 18:54
74-95-3
0.30
1
08/28/18 18:54
95-50-1
0.33
1
08/28/18 18:54
106-46-7
1.0
1
08/28/18 18:54
110-57-6
0.32
1
08/28/18 18:54
75-34-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 45

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
Sample: 3901-MW3R Lab ID: 92396265002 Collected: 08/15/18 12:50 Received: 08/17/18 09:37 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill Analytical Method: EPA 8260E
1,2-Dichloroethane
ND
ug/L
1.0
0.24
1
08/28/18 18:54
107-06-2
1,1-Dichloroethene
ND
ug/L
5.0
0.56
1
08/28/18 18:54
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
5.0
0.19
1
08/28/18 18:54
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
5.0
0.49
1
08/28/18 18:54
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.27
1
08/28/18 18:54
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.13
1
08/28/18 18:54
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.26
1
08/28/18 18:54
10061-02-6
Ethylbenzene
ND
ug/L
1.0
0.30
1
08/28/18 18:54
100-41-4
2-Hexanone
ND
ug/L
50.0
0.46
1
08/28/18 18:54
591-78-6
lodomethane
ND
ug/L
10.0
0.32
1
08/28/18 18:54
74-88-4
Methylene Chloride
ND
ug/L
1.0
0.97
1
08/28/18 18:54
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
100
0.33
1
08/28/18 18:54
108-10-1
Styrene
ND
ug/L
1.0
0.26
1
08/28/18 18:54
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
5.0
0.33
1
08/28/18 18:54
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
3.0
0.40
1
08/28/18 18:54
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.46
1
08/28/18 18:54
127-18-4
Tetrahydrofuran
ND
ug/L
10.0
3.1
1
08/28/18 18:54
109-99-9
Toluene
ND
ug/L
1.0
0.26
1
08/28/18 18:54
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.48
1
08/28/18 18:54
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.29
1
08/28/18 18:54
79-00-5
Trichloroethene
ND
ug/L
1.0
0.47
1
08/28/18 18:54
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.20
1
08/28/18 18:54
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.41
1
08/28/18 18:54
96-18-4
Vinyl acetate
ND
ug/L
50.0
0.35
1
08/28/18 18:54
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.62
1
08/28/18 18:54
75-01-4
Xylene (Total)
ND
ug/L
5.0
0.66
1
08/28/18 18:54
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
94
%
70-130
1
08/28/18 18:54
460-00-4
1,2-Dichloroethane-d4 (S)
100
%
70-130
1
08/28/18 18:54
17060-07-0
Toluene-d8 (S)
97
%
70-130
1
08/28/18 18:54
2037-26-5
8260 MSV SIM
Analytical Method: EPA 8260E Mod.
1,4-Dioxane (p-Dioxane)
16.5
ug/L
2.0
1.9
1
08/23/18 18:23
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
97
%
50-150
1
08/23/18 18:23
17060-07-0
Toluene-d8 (S)
114
%
50-150
1
08/23/18 18:23
2037-26-5
2320B Alkalinity
Analytical Method: SM
2320B-2011
Alkalinity, Total as CaCO3
93200
ug/L
5000
1000
1
08/24/18 21:10
2540C Total Dissolved Solids
Analytical Method: SM
2540C-2011
Total Dissolved Solids
164000
ug/L
25000
25000
1
08/17/18 22:52
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1
1993
Sulfate
7130J
ug/L
250000
500
1
08/25/18 08:06
14808-79-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/30/2018 12:04 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 45

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
Sample: 3901-MW4R Lab ID: 92396265003 Collected: 08/16/18 08:24 Received: 08/17/18 09:37 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
7470 Mercury
Mercury
8260 MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
Date: 08/30/2018 12:04 PM
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
ND
ug/L
6.0
3.9
1
08/25/18 07:40
08/25/18 22:28
7440-36-0
ND
ug/L
10.0
5.0
1
08/25/18 07:40
08/25/18 22:28
7440-38-2
39.9J
ug/L
100
2.5
1
08/25/18 07:40
08/25/18 22:28
7440-39-3
ND
ug/L
1.0
0.50
1
08/25/18 07:40
08/25/18 22:28
7440-41-7
ND
ug/L
1.0
0.50
1
08/25/18 07:40
08/25/18 22:28
7440-43-9
ND
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:28
7440-47-3
ND
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:28
7440-48-4
ND
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:28
7440-50-8
75.5J
ug/L
300
25.0
1
08/25/18 07:40
08/25/18 22:28
7439-89-6
ND
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:28
7439-92-1
937
ug/L
50.0
2.5
1
08/25/18 07:40
08/25/18 22:28
7439-96-5
ND
ug/L
50.0
2.5
1
08/25/18 07:40
08/25/18 22:28
7440-02-0
ND
ug/L
10.0
5.0
1
08/25/18 07:40
08/25/18 22:28
7782-49-2
ND
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:28
7440-22-4
ND
ug/L
25.0
2.5
1
08/25/18 07:40
08/25/18 22:28
7440-62-2
ND
ug/L
10.0
5.0
1
08/25/18 07:40
08/25/18 22:28
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
ND ug/L 5.5 0.020 1 08/18/18 06:19 08/29/18 17:17 7440-28-0
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
ND ug/L 0.20 0.10 1 08/22/1814:24 08/24/1812:32 7439-97-6
Analytical Method: EPA 8260E
ND
ug/L
100
ND
ug/L
200
ND
ug/L
1.0
ND
ug/L
3.0
ND
ug/L
1.0
ND
ug/L
3.0
ND
ug/L
10.0
ND
ug/L
100
ND
ug/L
100
ND
ug/L
1.0
ND
ug/L
3.0
ND
ug/L
10.0
ND
ug/L
5.0
ND
ug/L
1.0
ND
ug/L
13.0
ND
ug/L
3.0
ND
ug/L
1.0
ND
ug/L
10.0
ND
ug/L
5.0
ND
ug/L
1.0
ND
ug/L
100
ND
ug/L
5.0
10.0
1
08/28/18 19:10
67-64-1
1.9
1
08/28/18 19:10
107-13-1
0.25
1
08/28/18 19:10
71-43-2
0.17
1
08/28/18 19:10
74-97-5
0.18
1
08/28/18 19:10
75-27-4
0.26
1
08/28/18 19:10
75-25-2
0.29
1
08/28/18 19:10
74-83-9
0.96
1
08/28/18 19:10
78-93-3
1.2
1
08/28/18 19:10
75-15-0
0.25
1
08/28/18 19:10
56-23-5
0.23
1
08/28/18 19:10
108-90-7
0.54
1
08/28/18 19:10
75-00-3
0.14
1
08/28/18 19:10
67-66-3
0.11
1
08/28/18 19:10
74-87-3
2.0
1
08/28/18 19:10
96-12-8
0.21
1
08/28/18 19:10
124-48-1
0.27
1
08/28/18 19:10
106-93-4
0.21
1
08/28/18 19:10
74-95-3
0.30
1
08/28/18 19:10
95-50-1
0.33
1
08/28/18 19:10
106-46-7
1.0
1
08/28/18 19:10
110-57-6
0.32
1
08/28/18 19:10
75-34-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 12 of 45

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
Sample: 3901-MW4R Lab ID: 92396265003 Collected: 08/16/18 08:24 Received: 08/17/18 09:37 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill Analytical Method: EPA 8260E
1,2-Dichloroethane
ND
ug/L
1.0
0.24
1
08/28/18 19:10
107-06-2
1,1-Dichloroethene
ND
ug/L
5.0
0.56
1
08/28/18 19:10
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
5.0
0.19
1
08/28/18 19:10
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
5.0
0.49
1
08/28/18 19:10
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.27
1
08/28/18 19:10
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.13
1
08/28/18 19:10
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.26
1
08/28/18 19:10
10061-02-6
Ethylbenzene
ND
ug/L
1.0
0.30
1
08/28/18 19:10
100-41-4
2-Hexanone
ND
ug/L
50.0
0.46
1
08/28/18 19:10
591-78-6
lodomethane
ND
ug/L
10.0
0.32
1
08/28/18 19:10
74-88-4
Methylene Chloride
ND
ug/L
1.0
0.97
1
08/28/18 19:10
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
100
0.33
1
08/28/18 19:10
108-10-1
Styrene
ND
ug/L
1.0
0.26
1
08/28/18 19:10
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
5.0
0.33
1
08/28/18 19:10
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
3.0
0.40
1
08/28/18 19:10
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.46
1
08/28/18 19:10
127-18-4
Tetrahydrofuran
ND
ug/L
10.0
3.1
1
08/28/18 19:10
109-99-9
Toluene
ND
ug/L
1.0
0.26
1
08/28/18 19:10
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.48
1
08/28/18 19:10
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.29
1
08/28/18 19:10
79-00-5
Trichloroethene
ND
ug/L
1.0
0.47
1
08/28/18 19:10
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.20
1
08/28/18 19:10
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.41
1
08/28/18 19:10
96-18-4
Vinyl acetate
ND
ug/L
50.0
0.35
1
08/28/18 19:10
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.62
1
08/28/18 19:10
75-01-4
Xylene (Total)
ND
ug/L
5.0
0.66
1
08/28/18 19:10
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
91
%
70-130
1
08/28/18 19:10
460-00-4
1,2-Dichloroethane-d4 (S)
99
%
70-130
1
08/28/18 19:10
17060-07-0
Toluene-d8 (S)
98
%
70-130
1
08/28/18 19:10
2037-26-5
8260 MSV SIM
Analytical Method: EPA 8260E Mod.
1,4-Dioxane (p-Dioxane)
21.2
ug/L
2.0
1.9
1
08/23/18 20:59
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
99
%
50-150
1
08/23/18 20:59
17060-07-0
Toluene-d8 (S)
113
%
50-150
1
08/23/18 20:59
2037-26-5
2320B Alkalinity
Analytical Method: SM
2320B-2011
Alkalinity, Total as CaCO3
302000
ug/L
5000
1000
1
08/28/18 10:10
2540C Total Dissolved Solids
Analytical Method: SM
2540C-2011
Total Dissolved Solids
458000
ug/L
25000
25000
1
08/18/18 00:55
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1
1993
Sulfate
6470J
ug/L
250000
500
1
08/25/18 08:23
14808-79-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/30/2018 12:04 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 45

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
Sample: 3901-MW5R Lab ID: 92396265004 Collected: 08/16/18 08:10 Received: 08/17/18 09:37 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
7470 Mercury
Mercury
8260 MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
Date: 08/30/2018 12:04 PM
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
ND
ug/L
6.0
3.9
1
08/25/18 07:40
08/25/18 22:31
7440-36-0
ND
ug/L
10.0
5.0
1
08/25/18 07:40
08/25/18 22:31
7440-38-2
41.6J
ug/L
100
2.5
1
08/25/18 07:40
08/25/18 22:31
7440-39-3
ND
ug/L
1.0
0.50
1
08/25/18 07:40
08/25/18 22:31
7440-41-7
ND
ug/L
1.0
0.50
1
08/25/18 07:40
08/25/18 22:31
7440-43-9
ND
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:31
7440-47-3
ND
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:31
7440-48-4
ND
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:31
7440-50-8
ND
ug/L
300
25.0
1
08/25/18 07:40
08/25/18 22:31
7439-89-6
ND
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:31
7439-92-1
105
ug/L
50.0
2.5
1
08/25/18 07:40
08/25/18 22:31
7439-96-5
ND
ug/L
50.0
2.5
1
08/25/18 07:40
08/25/18 22:31
7440-02-0
ND
ug/L
10.0
5.0
1
08/25/18 07:40
08/25/18 22:31
7782-49-2
ND
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:31
7440-22-4
ND
ug/L
25.0
2.5
1
08/25/18 07:40
08/25/18 22:31
7440-62-2
ND
ug/L
10.0
5.0
1
08/25/18 07:40
08/25/18 22:31
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
ND ug/L 5.5 0.020 1 08/18/18 06:19 08/29/18 17:20 7440-28-0
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
ND ug/L 0.20 0.10 1 08/20/1819:25 08/21/1813:25 7439-97-6
Analytical Method: EPA 8260E
ND
ug/L
100
ND
ug/L
200
0.35J
ug/L
1.0
ND
ug/L
3.0
ND
ug/L
1.0
ND
ug/L
3.0
ND
ug/L
10.0
ND
ug/L
100
ND
ug/L
100
ND
ug/L
1.0
1.1J
ug/L
3.0
ND
ug/L
10.0
ND
ug/L
5.0
ND
ug/L
1.0
ND
ug/L
13.0
ND
ug/L
3.0
ND
ug/L
1.0
ND
ug/L
10.0
1.2J
ug/L
5.0
1.1
ug/L
1.0
ND
ug/L
100
2.4J
ug/L
5.0
10.0
1
08/28/18 19:26
67-64-1
1.9
1
08/28/18 19:26
107-13-1
0.25
1
08/28/18 19:26
71-43-2
0.17
1
08/28/18 19:26
74-97-5
0.18
1
08/28/18 19:26
75-27-4
0.26
1
08/28/18 19:26
75-25-2
0.29
1
08/28/18 19:26
74-83-9
0.96
1
08/28/18 19:26
78-93-3
1.2
1
08/28/18 19:26
75-15-0
0.25
1
08/28/18 19:26
56-23-5
0.23
1
08/28/18 19:26
108-90-7
0.54
1
08/28/18 19:26
75-00-3
0.14
1
08/28/18 19:26
67-66-3
0.11
1
08/28/18 19:26
74-87-3
2.0
1
08/28/18 19:26
96-12-8
0.21
1
08/28/18 19:26
124-48-1
0.27
1
08/28/18 19:26
106-93-4
0.21
1
08/28/18 19:26
74-95-3
0.30
1
08/28/18 19:26
95-50-1
0.33
1
08/28/18 19:26
106-46-7
1.0
1
08/28/18 19:26
110-57-6
0.32
1
08/28/18 19:26
75-34-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 14 of 45

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
Sample: 3901-MW5R Lab ID: 92396265004 Collected: 08/16/18 08:10 Received: 08/17/18 09:37 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill Analytical Method: EPA 8260E
1,2-Dichloroethane
ND
ug/L
1.0
0.24
1
08/28/18 19:26
107-06-2
1,1-Dichloroethene
ND
ug/L
5.0
0.56
1
08/28/18 19:26
75-35-4
cis-1,2-Dichloroethene
1.2J
ug/L
5.0
0.19
1
08/28/18 19:26
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
5.0
0.49
1
08/28/18 19:26
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.27
1
08/28/18 19:26
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.13
1
08/28/18 19:26
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.26
1
08/28/18 19:26
10061-02-6
Ethylbenzene
ND
ug/L
1.0
0.30
1
08/28/18 19:26
100-41-4
2-Hexanone
ND
ug/L
50.0
0.46
1
08/28/18 19:26
591-78-6
lodomethane
ND
ug/L
10.0
0.32
1
08/28/18 19:26
74-88-4
Methylene Chloride
ND
ug/L
1.0
0.97
1
08/28/18 19:26
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
100
0.33
1
08/28/18 19:26
108-10-1
Styrene
ND
ug/L
1.0
0.26
1
08/28/18 19:26
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
5.0
0.33
1
08/28/18 19:26
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
3.0
0.40
1
08/28/18 19:26
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.46
1
08/28/18 19:26
127-18-4
Tetrahydrofuran
ND
ug/L
10.0
3.1
1
08/28/18 19:26
109-99-9
Toluene
ND
ug/L
1.0
0.26
1
08/28/18 19:26
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.48
1
08/28/18 19:26
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.29
1
08/28/18 19:26
79-00-5
Trichloroethene
ND
ug/L
1.0
0.47
1
08/28/18 19:26
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.20
1
08/28/18 19:26
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.41
1
08/28/18 19:26
96-18-4
Vinyl acetate
ND
ug/L
50.0
0.35
1
08/28/18 19:26
108-05-4
Vinyl chloride
3.5
ug/L
1.0
0.62
1
08/28/18 19:26
75-01-4
Xylene (Total)
ND
ug/L
5.0
0.66
1
08/28/18 19:26
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
93
%
70-130
1
08/28/18 19:26
460-00-4
1,2-Dichloroethane-d4 (S)
101
%
70-130
1
08/28/18 19:26
17060-07-0
Toluene-d8 (S)
99
%
70-130
1
08/28/18 19:26
2037-26-5
8260 MSV SIM
Analytical Method: EPA 8260E Mod.
1,4-Dioxane (p-Dioxane)
41.6
ug/L
2.0
1.9
1
08/23/18 21:19
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
98
%
50-150
1
08/23/18 21:19
17060-07-0
Toluene-d8 (S)
114
%
50-150
1
08/23/18 21:19
2037-26-5
2320B Alkalinity
Analytical Method: SM
2320B-2011
Alkalinity, Total as CaCO3
192000
ug/L
5000
1000
1
08/27/18 23:42
2540C Total Dissolved Solids
Analytical Method: SM
2540C-2011
Total Dissolved Solids
303000
ug/L
25000
25000
1
08/18/18 00:55
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1
1993
Sulfate
4200J
ug/L
250000
500
1
08/25/18 09:14
14808-79-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/30/2018 12:04 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 45

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
Sample: 3901-MW6R Lab ID: 92396265005 Collected: 08/15/18 10:20 Received: 08/17/18 09:37 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
7470 Mercury
Mercury
8260 MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
Date: 08/30/2018 12:04 PM
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
ND
ug/L
6.0
3.9
1
08/25/18 07:40
08/25/18 22:34
7440-36-0
ND
ug/L
10.0
5.0
1
08/25/18 07:40
08/25/18 22:34
7440-38-2
108
ug/L
100
2.5
1
08/25/18 07:40
08/25/18 22:34
7440-39-3
ND
ug/L
1.0
0.50
1
08/25/18 07:40
08/25/18 22:34
7440-41-7
ND
ug/L
1.0
0.50
1
08/25/18 07:40
08/25/18 22:34
7440-43-9
ND
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:34
7440-47-3
ND
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:34
7440-48-4
ND
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:34
7440-50-8
1180
ug/L
300
25.0
1
08/25/18 07:40
08/25/18 22:34
7439-89-6
ND
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:34
7439-92-1
1870
ug/L
50.0
2.5
1
08/25/18 07:40
08/25/18 22:34
7439-96-5
ND
ug/L
50.0
2.5
1
08/25/18 07:40
08/25/18 22:34
7440-02-0
ND
ug/L
10.0
5.0
1
08/25/18 07:40
08/25/18 22:34
7782-49-2
ND
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:34
7440-22-4
ND
ug/L
25.0
2.5
1
08/25/18 07:40
08/25/18 22:34
7440-62-2
ND
ug/L
10.0
5.0
1
08/25/18 07:40
08/25/18 22:34
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
ND ug/L 5.5 0.020 1 08/18/18 06:19 08/29/18 17:22 7440-28-0
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
ND ug/L 0.20 0.10 1 08/22/1814:24 08/24/1812:39 7439-97-6
Analytical Method: EPA 8260E
ND
ug/L
100
ND
ug/L
200
ND
ug/L
1.0
ND
ug/L
3.0
ND
ug/L
1.0
ND
ug/L
3.0
ND
ug/L
10.0
ND
ug/L
100
ND
ug/L
100
ND
ug/L
1.0
ND
ug/L
3.0
ND
ug/L
10.0
ND
ug/L
5.0
ND
ug/L
1.0
ND
ug/L
13.0
ND
ug/L
3.0
ND
ug/L
1.0
ND
ug/L
10.0
ND
ug/L
5.0
ND
ug/L
1.0
ND
ug/L
100
0.93J
ug/L
5.0
10.0
1
08/28/18 19:43
67-64-1
1.9
1
08/28/18 19:43
107-13-1
0.25
1
08/28/18 19:43
71-43-2
0.17
1
08/28/18 19:43
74-97-5
0.18
1
08/28/18 19:43
75-27-4
0.26
1
08/28/18 19:43
75-25-2
0.29
1
08/28/18 19:43
74-83-9
0.96
1
08/28/18 19:43
78-93-3
1.2
1
08/28/18 19:43
75-15-0
0.25
1
08/28/18 19:43
56-23-5
0.23
1
08/28/18 19:43
108-90-7
0.54
1
08/28/18 19:43
75-00-3
0.14
1
08/28/18 19:43
67-66-3
0.11
1
08/28/18 19:43
74-87-3
2.0
1
08/28/18 19:43
96-12-8
0.21
1
08/28/18 19:43
124-48-1
0.27
1
08/28/18 19:43
106-93-4
0.21
1
08/28/18 19:43
74-95-3
0.30
1
08/28/18 19:43
95-50-1
0.33
1
08/28/18 19:43
106-46-7
1.0
1
08/28/18 19:43
110-57-6
0.32
1
08/28/18 19:43
75-34-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 16 of 45

aceAnalytical
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ANALYTICAL RESULTS
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
Sample: 3901-MW6R Lab ID: 92396265005 Collected: 08/15/18 10:20 Received: 08/17/18 09:37 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill Analytical Method: EPA 8260E
1,2-Dichloroethane
ND
ug/L
1.0
0.24
1
08/28/18 19:43
107-06-2
1,1-Dichloroethene
ND
ug/L
5.0
0.56
1
08/28/18 19:43
75-35-4
cis-1,2-Dichloroethene
0.62J
ug/L
5.0
0.19
1
08/28/18 19:43
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
5.0
0.49
1
08/28/18 19:43
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.27
1
08/28/18 19:43
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.13
1
08/28/18 19:43
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.26
1
08/28/18 19:43
10061-02-6
Ethylbenzene
ND
ug/L
1.0
0.30
1
08/28/18 19:43
100-41-4
2-Hexanone
ND
ug/L
50.0
0.46
1
08/28/18 19:43
591-78-6
lodomethane
ND
ug/L
10.0
0.32
1
08/28/18 19:43
74-88-4
Methylene Chloride
ND
ug/L
1.0
0.97
1
08/28/18 19:43
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
100
0.33
1
08/28/18 19:43
108-10-1
Styrene
ND
ug/L
1.0
0.26
1
08/28/18 19:43
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
5.0
0.33
1
08/28/18 19:43
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
3.0
0.40
1
08/28/18 19:43
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.46
1
08/28/18 19:43
127-18-4
Tetrahydrofuran
ND
ug/L
10.0
3.1
1
08/28/18 19:43
109-99-9
Toluene
ND
ug/L
1.0
0.26
1
08/28/18 19:43
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.48
1
08/28/18 19:43
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.29
1
08/28/18 19:43
79-00-5
Trichloroethene
ND
ug/L
1.0
0.47
1
08/28/18 19:43
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.20
1
08/28/18 19:43
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.41
1
08/28/18 19:43
96-18-4
Vinyl acetate
ND
ug/L
50.0
0.35
1
08/28/18 19:43
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.62
1
08/28/18 19:43
75-01-4
Xylene (Total)
ND
ug/L
5.0
0.66
1
08/28/18 19:43
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
95
%
70-130
1
08/28/18 19:43
460-00-4
1,2-Dichloroethane-d4 (S)
101
%
70-130
1
08/28/18 19:43
17060-07-0
Toluene-d8 (S)
99
%
70-130
1
08/28/18 19:43
2037-26-5
8260 MSV SIM
Analytical Method: EPA 8260E Mod.
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1.9
1
08/23/18 18:43
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
101
%
50-150
1
08/23/18 18:43
17060-07-0
Toluene-d8 (S)
117
%
50-150
1
08/23/18 18:43
2037-26-5
2320B Alkalinity
Analytical Method: SM
2320B-2011
Alkalinity, Total as CaCO3
203000
ug/L
5000
1000
1
08/24/18 21:24
2540C Total Dissolved Solids
Analytical Method: SM
2540C-2011
Total Dissolved Solids
509000
ug/L
25000
25000
1
08/17/18 22:52
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1
1993
Sulfate
2650J
ug/L
250000
500
1
08/25/18 09:31
14808-79-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/30/2018 12:04 PM without the written consent of Pace Analytical Services, LLC.
Page 17 of 45

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
Sample: 3901-SW1 Lab ID: 92396265006 Collected: 08/16/18 13:35 Received: 08/17/18 09:37 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Antimony
ND
ug/L
6.0
3.9
1
08/25/18 07:40
08/25/18 22:37
7440-36-0
Arsenic
ND
ug/L
10.0
5.0
1
08/25/18 07:40
08/25/18 22:37
7440-38-2
Barium
19.11
ug/L
100
2.5
1
08/25/18 07:40
08/25/18 22:37
7440-39-3
Beryllium
ND
ug/L
1.0
0.50
1
08/25/18 07:40
08/25/18 22:37
7440-41-7
Cadmium
ND
ug/L
1.0
0.50
1
08/25/18 07:40
08/25/18 22:37
7440-43-9
Chromium
ND
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:37
7440-47-3
Cobalt
ND
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:37
7440-48-4
Copper
3.9J
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:37
7440-50-8
Iron
3320
ug/L
300
25.0
1
08/25/18 07:40
08/25/18 22:37
7439-89-6
Lead
ND
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:37
7439-92-1
Manganese
176
ug/L
50.0
2.5
1
08/25/18 07:40
08/25/18 22:37
7439-96-5
Nickel
ND
ug/L
50.0
2.5
1
08/25/18 07:40
08/25/18 22:37
7440-02-0
Selenium
ND
ug/L
10.0
5.0
1
08/25/18 07:40
08/25/18 22:37
7782-49-2
Silver
ND
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:37
7440-22-4
Vanadium
7.6J
ug/L
25.0
2.5
1
08/25/18 07:40
08/25/18 22:37
7440-62-2
Zinc
6.2J
ug/L
10.0
5.0
1
08/25/18 07:40
08/25/18 22:37
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Thallium
ND
ug/L
5.5
0.020
1
08/18/18 06:19
08/29/18 17:25
7440-28-0
8260 MSV Low Level Landfill
Analytical Method: EPA 8260E
Acetone
ND
ug/L
100
10.0
1
08/28/18 19:59
67-64-1
Acrylonitrile
ND
ug/L
200
1.9
1
08/28/18 19:59
107-13-1
Benzene
ND
ug/L
1.0
0.25
1
08/28/18 19:59
71-43-2
Bromochloromethane
ND
ug/L
3.0
0.17
1
08/28/18 19:59
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.18
1
08/28/18 19:59
75-27-4
Bromoform
ND
ug/L
3.0
0.26
1
08/28/18 19:59
75-25-2
Bromomethane
ND
ug/L
10.0
0.29
1
08/28/18 19:59
74-83-9
2-Butanone (MEK)
ND
ug/L
100
0.96
1
08/28/18 19:59
78-93-3
Carbon disulfide
ND
ug/L
100
1.2
1
08/28/18 19:59
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.25
1
08/28/18 19:59
56-23-5
Chlorobenzene
ND
ug/L
3.0
0.23
1
08/28/18 19:59
108-90-7
Chloroethane
ND
ug/L
10.0
0.54
1
08/28/18 19:59
75-00-3
Chloroform
ND
ug/L
5.0
0.14
1
08/28/18 19:59
67-66-3
Chloromethane
ND
ug/L
1.0
0.11
1
08/28/18 19:59
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
13.0
2.0
1
08/28/18 19:59
96-12-8
Dibromochloromethane
ND
ug/L
3.0
0.21
1
08/28/18 19:59
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
08/28/18 19:59
106-93-4
Dibromomethane
ND
ug/L
10.0
0.21
1
08/28/18 19:59
74-95-3
1,2-Dichlorobenzene
ND
ug/L
5.0
0.30
1
08/28/18 19:59
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
08/28/18 19:59
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
100
1.0
1
08/28/18 19:59
110-57-6
1,1-Dichloroethane
ND
ug/L
5.0
0.32
1
08/28/18 19:59
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.24
1
08/28/18 19:59
107-06-2
1,1-Dichloroethene
ND
ug/L
5.0
0.56
1
08/28/18 19:59
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
5.0
0.19
1
08/28/18 19:59
156-59-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/30/2018 12:04 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 45

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
Sample: 3901-SW1 Lab ID: 92396265006 Collected: 08/16/18 13:35 Received: 08/17/18 09:37 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260 MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 08/30/2018 12:04 PM
Analytical Method: EPA 8260E
ND
ug/L
5.0
0.49
1
08/28/1819:59
156-60-5
ND
ug/L
1.0
0.27
1
08/28/1819:59
78-87-5
ND
ug/L
1.0
0.13
1
08/28/1819:59
10061-01-5
ND
ug/L
1.0
0.26
1
08/28/1819:59
10061-02-6
ND
ug/L
1.0
0.30
1
08/28/1819:59
100-41-4
ND
ug/L
50.0
0.46
1
08/28/1819:59
591-78-6
ND
ug/L
10.0
0.32
1
08/28/1819:59
74-88-4
ND
ug/L
1.0
0.97
1
08/28/1819:59
75-09-2
ND
ug/L
100
0.33
1
08/28/1819:59
108-10-1
ND
ug/L
1.0
0.26
1
08/28/1819:59
100-42-5
ND
ug/L
5.0
0.33
1
08/28/1819:59
630-20-6
ND
ug/L
3.0
0.40
1
08/28/1819:59
79-34-5
ND
ug/L
1.0
0.46
1
08/28/1819:59
127-18-4
ND
ug/L
10.0
3.1
1
08/28/1819:59
109-99-9
ND
ug/L
1.0
0.26
1
08/28/1819:59
108-88-3
ND
ug/L
1.0
0.48
1
08/28/1819:59
71-55-6
ND
ug/L
1.0
0.29
1
08/28/1819:59
79-00-5
ND
ug/L
1.0
0.47
1
08/28/1819:59
79-01-6
ND
ug/L
1.0
0.20
1
08/28/1819:59
75-69-4
ND
ug/L
1.0
0.41
1
08/28/1819:59
96-18-4
ND
ug/L
50.0
0.35
1
08/28/1819:59
108-05-4
ND
ug/L
1.0
0.62
1
08/28/1819:59
75-01-4
ND
ug/L
5.0
0.66
1
08/28/1819:59
1330-20-7
93
%
70-130
1
08/28/1819:59
460-00-4
103
%
70-130
1
08/28/1819:59
17060-07-0
98
%
70-130
1
08/28/1819:59
2037-26-5
Analytical Method: EPA 8260E Mod.
ND
ug/L
2.0
1.9
1
08/23/18 21:38
123-91-1
98
%
50-150
1
08/23/18 21:38
17060-07-0
115
%
50-150
1
08/23/18 21:38
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 19 of 45

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
Sample: 3901-SW2 Lab ID: 92396265007 Collected: 08/16/18 09:30 Received: 08/17/18 09:37 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 301 OA
Antimony
ND
ug/L
6.0
3.9
1
08/25/18 07:40
08/25/18 22:40
7440-36-0
Arsenic
ND
ug/L
10.0
5.0
1
08/25/18 07:40
08/25/18 22:40
7440-38-2
Barium
28.3J
ug/L
100
2.5
1
08/25/18 07:40
08/25/18 22:40
7440-39-3
Beryllium
ND
ug/L
1.0
0.50
1
08/25/18 07:40
08/25/18 22:40
7440-41-7
Cadmium
ND
ug/L
1.0
0.50
1
08/25/18 07:40
08/25/18 22:40
7440-43-9
Chromium
3.2J
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:40
7440-47-3
Cobalt
ND
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:40
7440-48-4
Copper
3.OJ
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:40
7440-50-8
Iron
2750
ug/L
300
25.0
1
08/25/18 07:40
08/25/18 22:40
7439-89-6
Lead
ND
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:40
7439-92-1
Manganese
45.2J
ug/L
50.0
2.5
1
08/25/18 07:40
08/25/18 22:40
7439-96-5
Nickel
ND
ug/L
50.0
2.5
1
08/25/18 07:40
08/25/18 22:40
7440-02-0
Selenium
ND
ug/L
10.0
5.0
1
08/25/18 07:40
08/25/18 22:40
7782-49-2
Silver
ND
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:40
7440-22-4
Vanadium
5.8J
ug/L
25.0
2.5
1
08/25/18 07:40
08/25/18 22:40
7440-62-2
Zinc
ND
ug/L
10.0
5.0
1
08/25/18 07:40
08/25/18 22:40
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Thallium
ND
ug/L
5.5
0.020
1
08/18/18 06:19
08/29/18 17:27
7440-28-0
8260 MSV Low Level Landfill
Analytical Method: EPA 8260E
Acetone
ND
ug/L
100
10.0
1
08/28/18 20:15
67-64-1
Acrylonitrile
ND
ug/L
200
1.9
1
08/28/18 20:15
107-13-1
Benzene
ND
ug/L
1.0
0.25
1
08/28/18 20:15
71-43-2
Bromochloromethane
ND
ug/L
3.0
0.17
1
08/28/18 20:15
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.18
1
08/28/18 20:15
75-27-4
Bromoform
ND
ug/L
3.0
0.26
1
08/28/18 20:15
75-25-2
Bromomethane
ND
ug/L
10.0
0.29
1
08/28/18 20:15
74-83-9
2-Butanone (MEK)
ND
ug/L
100
0.96
1
08/28/18 20:15
78-93-3
Carbon disulfide
ND
ug/L
100
1.2
1
08/28/18 20:15
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.25
1
08/28/18 20:15
56-23-5
Chlorobenzene
ND
ug/L
3.0
0.23
1
08/28/18 20:15
108-90-7
Chloroethane
ND
ug/L
10.0
0.54
1
08/28/18 20:15
75-00-3
Chloroform
ND
ug/L
5.0
0.14
1
08/28/18 20:15
67-66-3
Chloromethane
ND
ug/L
1.0
0.11
1
08/28/18 20:15
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
13.0
2.0
1
08/28/18 20:15
96-12-8
Dibromochloromethane
ND
ug/L
3.0
0.21
1
08/28/18 20:15
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
08/28/18 20:15
106-93-4
Dibromomethane
ND
ug/L
10.0
0.21
1
08/28/18 20:15
74-95-3
1,2-Dichlorobenzene
ND
ug/L
5.0
0.30
1
08/28/18 20:15
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
08/28/18 20:15
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
100
1.0
1
08/28/18 20:15
110-57-6
1,1-Dichloroethane
ND
ug/L
5.0
0.32
1
08/28/18 20:15
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.24
1
08/28/18 20:15
107-06-2
1,1-Dichloroethene
ND
ug/L
5.0
0.56
1
08/28/18 20:15
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
5.0
0.19
1
08/28/18 20:15
156-59-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/30/2018 12:04 PM without the written consent of Pace Analytical Services, LLC.
Page 20 of 45

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ANALYTICAL RESULTS
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
Sample: 3901-SW2 Lab ID: 92396265007 Collected: 08/16/18 09:30 Received: 08/17/18 09:37 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260 MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 08/30/2018 12:04 PM
Analytical Method: EPA 8260E
ND
ug/L
5.0
0.49
1
08/28/18 20:15
156-60-5
ND
ug/L
1.0
0.27
1
08/28/18 20:15
78-87-5
ND
ug/L
1.0
0.13
1
08/28/18 20:15
10061-01-5
ND
ug/L
1.0
0.26
1
08/28/18 20:15
10061-02-6
ND
ug/L
1.0
0.30
1
08/28/18 20:15
100-41-4
ND
ug/L
50.0
0.46
1
08/28/18 20:15
591-78-6
ND
ug/L
10.0
0.32
1
08/28/18 20:15
74-88-4
ND
ug/L
1.0
0.97
1
08/28/18 20:15
75-09-2
ND
ug/L
100
0.33
1
08/28/18 20:15
108-10-1
ND
ug/L
1.0
0.26
1
08/28/18 20:15
100-42-5
ND
ug/L
5.0
0.33
1
08/28/18 20:15
630-20-6
ND
ug/L
3.0
0.40
1
08/28/18 20:15
79-34-5
ND
ug/L
1.0
0.46
1
08/28/18 20:15
127-18-4
ND
ug/L
10.0
3.1
1
08/28/18 20:15
109-99-9
ND
ug/L
1.0
0.26
1
08/28/18 20:15
108-88-3
ND
ug/L
1.0
0.48
1
08/28/18 20:15
71-55-6
ND
ug/L
1.0
0.29
1
08/28/18 20:15
79-00-5
ND
ug/L
1.0
0.47
1
08/28/18 20:15
79-01-6
ND
ug/L
1.0
0.20
1
08/28/18 20:15
75-69-4
ND
ug/L
1.0
0.41
1
08/28/18 20:15
96-18-4
ND
ug/L
50.0
0.35
1
08/28/18 20:15
108-05-4
ND
ug/L
1.0
0.62
1
08/28/18 20:15
75-01-4
ND
ug/L
5.0
0.66
1
08/28/18 20:15
1330-20-7
95
%
70-130
1
08/28/18 20:15
460-00-4
100
%
70-130
1
08/28/18 20:15
17060-07-0
99
%
70-130
1
08/28/18 20:15
2037-26-5
Analytical Method: EPA 8260E Mod.
4.5
ug/L
2.0
1.9
1
08/23/18 21:57
123-91-1
95
%
50-150
1
08/23/18 21:57
17060-07-0
113
%
50-150
1
08/23/18 21:57
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 21 of 45

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ANALYTICAL RESULTS
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
Sample: Trip Blank Lab ID: 92396265008 Collected: 08/15/18 05:30 Received: 08/17/18 09:37 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill Analytical Method: EPA 8260E
Acetone
ND
ug/L
100
10.0
1
08/28/18 20:31
67-64-1
Acrylonitrile
ND
ug/L
200
1.9
1
08/28/18 20:31
107-13-1
Benzene
ND
ug/L
1.0
0.25
1
08/28/18 20:31
71-43-2
Bromochloromethane
ND
ug/L
3.0
0.17
1
08/28/18 20:31
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.18
1
08/28/18 20:31
75-27-4
Bromoform
ND
ug/L
3.0
0.26
1
08/28/18 20:31
75-25-2
Bromomethane
ND
ug/L
10.0
0.29
1
08/28/18 20:31
74-83-9
2-Butanone (MEK)
ND
ug/L
100
0.96
1
08/28/18 20:31
78-93-3
Carbon disulfide
ND
ug/L
100
1.2
1
08/28/18 20:31
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.25
1
08/28/18 20:31
56-23-5
Chlorobenzene
ND
ug/L
3.0
0.23
1
08/28/18 20:31
108-90-7
Chloroethane
ND
ug/L
10.0
0.54
1
08/28/18 20:31
75-00-3
Chloroform
ND
ug/L
5.0
0.14
1
08/28/18 20:31
67-66-3
Chloromethane
ND
ug/L
1.0
0.11
1
08/28/18 20:31
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
13.0
2.0
1
08/28/18 20:31
96-12-8
Dibromochloromethane
ND
ug/L
3.0
0.21
1
08/28/18 20:31
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
08/28/18 20:31
106-93-4
Dibromomethane
ND
ug/L
10.0
0.21
1
08/28/18 20:31
74-95-3
1,2-Dichlorobenzene
ND
ug/L
5.0
0.30
1
08/28/18 20:31
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
08/28/18 20:31
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
100
1.0
1
08/28/18 20:31
110-57-6
1,1-Dichloroethane
ND
ug/L
5.0
0.32
1
08/28/18 20:31
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.24
1
08/28/18 20:31
107-06-2
1,1-Dichloroethene
ND
ug/L
5.0
0.56
1
08/28/18 20:31
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
5.0
0.19
1
08/28/18 20:31
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
5.0
0.49
1
08/28/18 20:31
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.27
1
08/28/18 20:31
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.13
1
08/28/18 20:31
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.26
1
08/28/18 20:31
10061-02-6
Ethylbenzene
ND
ug/L
1.0
0.30
1
08/28/18 20:31
100-41-4
2-Hexanone
ND
ug/L
50.0
0.46
1
08/28/18 20:31
591-78-6
lodomethane
ND
ug/L
10.0
0.32
1
08/28/18 20:31
74-88-4
Methylene Chloride
ND
ug/L
1.0
0.97
1
08/28/18 20:31
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
100
0.33
1
08/28/18 20:31
108-10-1
Styrene
ND
ug/L
1.0
0.26
1
08/28/18 20:31
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
5.0
0.33
1
08/28/18 20:31
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
3.0
0.40
1
08/28/18 20:31
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.46
1
08/28/18 20:31
127-18-4
Tetrahydrofuran
ND
ug/L
10.0
3.1
1
08/28/18 20:31
109-99-9
Toluene
ND
ug/L
1.0
0.26
1
08/28/18 20:31
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.48
1
08/28/18 20:31
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.29
1
08/28/18 20:31
79-00-5
Trichloroethene
ND
ug/L
1.0
0.47
1
08/28/18 20:31
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.20
1
08/28/18 20:31
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.41
1
08/28/18 20:31
96-18-4
Vinyl acetate
ND
ug/L
50.0
0.35
1
08/28/18 20:31
108-05-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/30/2018 12:04 PM without the written consent of Pace Analytical Services, LLC.
Page 22 of 45

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ANALYTICAL RESULTS
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
Sample: Trip Blank
Lab ID:
92396265008
Collected:
08/15/18 05:30
Received: 08/17/18 09:37 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL DF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level Landfill
Analytical
Method: EPA 8260E
Vinyl chloride
ND
ug/L
1.0
0.62 1
08/28/18 20:31
75-01-4
Xylene (Total)
ND
ug/L
5.0
0.66 1
08/28/18 20:31
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
94
%
70-130
1
08/28/18 20:31
460-00-4
1,2-Dichloroethane-d4 (S)
99
%
70-130
1
08/28/18 20:31
17060-07-0
Toluene-d8 (S)
99
%
70-130
1
08/28/18 20:31
2037-26-5
Date: 08/30/2018 12:04 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 23 of 45

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QUALITY CONTROL DATA
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
QC Batch: 425829
Analysis Method: EPA 7470A
QC Batch Method: EPA 7470A
Analysis Description: 7470 Mercury
Associated Lab Samples: 92396265004
METHOD BLANK: 2354113
Matrix: Water
Associated Lab Samples: 92396265004
Blank Reporting
Parameter Units
Result Limit MDL
Analyzed
Qualifiers
Mercury ug/L
ND 0.20 0.10 08/21/1811:38
LABORATORY CONTROL SAMPLE: 2354114
Spike LCS LCS
% Rec
Parameter Units
Conc. Result % Rec
Limits Qualifiers
Mercury ug/L
2.5 2.4 98
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2354115 2354116
MS MSD
92395555001
Spike Spike MS MSD
MS MSD
% Rec Max
Parameter Units Result
Conc. Conc. Result Result
% Rec % Rec
Limits RPD RPD Qual
Mercury ug/L ND
2.5 2.5 2.4 2.4
96 96
75-125 1 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/30/2018 12:04 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 45

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QUALITY CONTROL DATA
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
QC Batch: 426302
Analysis Method: EPA 7470A
QC Batch Method: EPA 7470A
Analysis Description: 7470 Mercury
Associated Lab Samples: 92396265001, 92396265002,
92396265003, 92396265005
METHOD BLANK: 2356266
Matrix: Water
Associated Lab Samples: 92396265001, 92396265002,
92396265003, 92396265005
Blank Reporting
Parameter Units
Result Limit MDL
Analyzed Qualifiers
Mercury ug/L
ND 0.20 0.10 08/24/1812:00
LABORATORY CONTROL SAMPLE: 2356267
Spike LCS LCS
% Rec
Parameter Units
Conc. Result % Rec
Limits Qualifiers
Mercury ug/L
2.5 2.8 112
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2356268 2356269
MS MSD
92396406001
Spike Spike MS MSD
MS MSD % Rec Max
Parameter Units Result
Conc. Conc. Result Result
% Rec % Rec Limits RPD RPD Qual
Mercury ug/L ND
2.5 2.5 2.6 2.6
104 106 75-125 2 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/30/2018 12:04 PM without the written consent of Pace Analytical Services, LLC.
Page 25 of 45

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Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
QC Batch: 427103 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Associated Lab Samples: 92396265001, 92396265002, 92396265003, 92396265004, 92396265005, 92396265006, 92396265007
METHOD BLANK: 2359969 Matrix: Water
Associated Lab Samples: 92396265001, 92396265002, 92396265003, 92396265004, 92396265005, 92396265006, 92396265007
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Antimony
ug/L
ND
6.0
3.9
08/25/18 21:44
Arsenic
ug/L
ND
10.0
5.0
08/25/18 21:44
Barium
ug/L
ND
100
2.5
08/25/18 21:44
Beryllium
ug/L
ND
1.0
0.50
08/25/18 21:44
Cadmium
ug/L
ND
1.0
0.50
08/25/18 21:44
Chromium
ug/L
ND
10.0
2.5
08/25/18 21:44
Cobalt
ug/L
ND
10.0
2.5
08/25/18 21:44
Copper
ug/L
ND
10.0
2.5
08/25/18 21:44
Iron
ug/L
ND
300
25.0
08/25/18 21:44
Lead
ug/L
ND
10.0
2.5
08/25/18 21:44
Manganese
ug/L
ND
50.0
2.5
08/25/18 21:44
Nickel
ug/L
ND
50.0
2.5
08/25/18 21:44
Selenium
ug/L
ND
10.0
5.0
08/25/18 21:44
Silver
ug/L
ND
10.0
2.5
08/25/18 21:44
Vanadium
ug/L
ND
25.0
2.5
08/25/18 21:44
Zinc
ug/L
ND
10.0
5.0
08/25/18 21:44
LABORATORY CONTROL SAMPLE:
Parameter
2359970
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Antimony
ug/L
500
453
91
80-120
Arsenic
ug/L
500
438
88
80-120
Barium
ug/L
500
473
95
80-120
Beryllium
ug/L
500
464
93
80-120
Cadmium
ug/L
500
452
90
80-120
Chromium
ug/L
500
462
92
80-120
Cobalt
ug/L
500
449
90
80-120
Copper
ug/L
500
469
94
80-120
Iron
ug/L
5000
4630
93
80-120
Lead
ug/L
500
444
89
80-120
Manganese
ug/L
500
449
90
80-120
Nickel
ug/L
500
450
90
80-120
Selenium
ug/L
500
435
87
80-120
Silver
ug/L
250
232
93
80-120
Vanadium
ug/L
500
458
92
80-120
Zinc
ug/L
500
439
88
80-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/30/2018 12:04 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 45

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QUALITY CONTROL DATA
Project:
Pace Project No.:
Oxford Compliance Unit 1
92396265
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
2359971
2359972
MS
MSD
92396257001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Antimony
ug/L
ND
500
500
467
460
93
92
75-125
1
20
Arsenic
ug/L
ND
500
500
462
455
92
91
75-125
1
20
Barium
ug/L
40.3J
500
500
526
517
97
95
75-125
2
20
Beryllium
ug/L
ND
500
500
479
474
96
95
75-125
1
20
Cadmium
ug/L
ND
500
500
471
466
94
93
75-125
1
20
Chromium
ug/L
ND
500
500
476
470
95
94
75-125
1
20
Cobalt
ug/L
ND
500
500
456
451
91
90
75-125
1
20
Copper
ug/L
24.7
500
500
508
500
97
95
75-125
2
20
Iron
ug/L
410
5000
5000
5320
5230
98
96
75-125
2
20
Lead
ug/L
ND
500
500
453
448
91
89
75-125
1
20
Manganese
ug/L
270
500
500
746
734
95
93
75-125
2
20
Nickel
ug/L
ND
500
500
458
454
92
91
75-125
1
20
Selenium
ug/L
ND
500
500
461
458
92
92
75-125
1
20
Silver
ug/L
ND
250
250
242
238
97
95
75-125
2
20
Vanadium
ug/L
ND
500
500
475
470
95
94
75-125
1
20
Zinc
ug/L
ND
500
500
457
454
91
90
75-125
1
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/30/2018 12:04 PM without the written consent of Pace Analytical Services, LLC.
Page 27 of 45

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
QC Batch: 425734 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Associated Lab Samples: 92396265001, 92396265002, 92396265003, 92396265004, 92396265005, 92396265006, 92396265007
METHOD BLANK: 2353880 Matrix: Water
Associated Lab Samples: 92396265001, 92396265002, 92396265003, 92396265004, 92396265005, 92396265006, 92396265007
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Thallium ug/L ND 5.5 0.020 08/29/1816:42
LABORATORY CONTROL SAMPLE: 2353881
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Thallium ug/L 10 9.9 99 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2353882 2353883
MS MSD
92396257001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Thallium ug/L ND 10 10 10.9 10 109 100 75-125 9 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/30/2018 12:04 PM without the written consent of Pace Analytical Services, LLC.
Page 28 of 45

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
QC Batch: 427539 Analysis Method: EPA 8260B
QC Batch Method: EPA 8260E Analysis Description: 8260 MSV Low Level Landfill
Associated Lab Samples: 92396265001, 92396265002, 92396265003, 92396265004, 92396265005, 92396265006, 92396265007,
92396265008
METHOD BLANK: 2361841 Matrix: Water
Associated Lab Samples: 92396265001, 92396265002, 92396265003, 92396265004, 92396265005, 92396265006, 92396265007,
92396265008
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
5.0
0.33
08/28/18 15:24
1,1,1-Trichloroethane
ug/L
ND
1.0
0.48
08/28/18 15:24
1,1,2,2-Tetrachloroethane
ug/L
ND
3.0
0.40
08/28/18 15:24
1,1,2-Trichloroethane
ug/L
ND
1.0
0.29
08/28/18 15:24
1,1-Dichloroethane
ug/L
ND
5.0
0.32
08/28/18 15:24
1,1-Dichloroethene
ug/L
ND
5.0
0.56
08/28/18 15:24
1,2,3-Trichloropropane
ug/L
ND
1.0
0.41
08/28/18 15:24
1,2-Dibromo-3-chloropropane
ug/L
ND
13.0
2.0
08/28/18 15:24
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.27
08/28/18 15:24
1,2-Dichlorobenzene
ug/L
ND
5.0
0.30
08/28/18 15:24
1,2-Dichloroethane
ug/L
ND
1.0
0.24
08/28/18 15:24
1,2-Dichloropropane
ug/L
ND
1.0
0.27
08/28/18 15:24
1,4-Dichlorobenzene
ug/L
ND
1.0
0.33
08/28/18 15:24
2-Butanone (MEK)
ug/L
ND
100
0.96
08/28/18 15:24
2-Hexanone
ug/L
ND
50.0
0.46
08/28/18 15:24
4-Methyl-2-pentanone (MIBK)
ug/L
ND
100
0.33
08/28/18 15:24
Acetone
ug/L
ND
100
10.0
08/28/18 15:24
Acrylonitrile
ug/L
ND
200
1.9
08/28/18 15:24
Benzene
ug/L
ND
1.0
0.25
08/28/18 15:24
Bromochloromethane
ug/L
ND
3.0
0.17
08/28/18 15:24
Bromodichloromethane
ug/L
ND
1.0
0.18
08/28/18 15:24
Bromoform
ug/L
ND
3.0
0.26
08/28/18 15:24
Bromomethane
ug/L
ND
10.0
0.29
08/28/18 15:24
Carbon disulfide
ug/L
ND
100
1.2
08/28/18 15:24
Carbon tetrachloride
ug/L
ND
1.0
0.25
08/28/18 15:24
Chlorobenzene
ug/L
ND
3.0
0.23
08/28/18 15:24
Chloroethane
ug/L
ND
10.0
0.54
08/28/18 15:24
Chloroform
ug/L
ND
5.0
0.14
08/28/18 15:24
Chloromethane
ug/L
ND
1.0
0.11
08/28/18 15:24
cis-1,2-Dichloroethene
ug/L
ND
5.0
0.19
08/28/18 15:24
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.13
08/28/18 15:24
Dibromochloromethane
ug/L
ND
3.0
0.21
08/28/18 15:24
Dibromomethane
ug/L
ND
10.0
0.21
08/28/18 15:24
Ethylbenzene
ug/L
ND
1.0
0.30
08/28/18 15:24
lodomethane
ug/L
ND
10.0
0.32
08/28/18 15:24
Methylene Chloride
ug/L
ND
1.0
0.97
08/28/18 15:24
Styrene
ug/L
ND
1.0
0.26
08/28/18 15:24
Tetrachloroethene
ug/L
ND
1.0
0.46
08/28/18 15:24
Tetrahydrofuran
ug/L
ND
10.0
3.1
08/28/18 15:24
Toluene
ug/L
ND
1.0
0.26
08/28/18 15:24
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/30/2018 12:04 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 45

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
METHOD BLANK: 2361841 Matrix: Water
Associated Lab Samples: 92396265001, 92396265002, 92396265003, 92396265004, 92396265005, 92396265006, 92396265007,
92396265008
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
trans-1,2-Dichloroethene
ug/L
ND
5.0
0.49
08/28/18 15:24
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.26
08/28/18 15:24
trans-1,4-Dichloro-2-butene
ug/L
ND
100
1.0
08/28/18 15:24
Trichloroethene
ug/L
ND
1.0
0.47
08/28/18 15:24
Trichlorofluoromethane
ug/L
ND
1.0
0.20
08/28/18 15:24
Vinyl acetate
ug/L
ND
50.0
0.35
08/28/18 15:24
Vinyl chloride
ug/L
ND
1.0
0.62
08/28/18 15:24
Xylene (Total)
ug/L
ND
5.0
0.66
08/28/18 15:24
1,2-Dichloroethane-d4 (S)
%
98
70-130
08/28/18 15:24
4-Bromofluorobenzene (S)
%
96
70-130
08/28/18 15:24
Toluene-d8 (S)
%
99
70-130
08/28/18 15:24
LABORATORY CONTROL SAMPLE:
2361842
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
53.1
106
80-125
1,1,1-Trichloroethane
ug/L
50
51.1
102
71-129
1,1,2,2-Tetrachloroethane
ug/L
50
49.6
99
79-124
1,1,2-Trichloroethane
ug/L
50
51.4
103
85-125
1,1-Dichloroethane
ug/L
50
46.9
94
73-126
1,1-Dichloroethene
ug/L
50
53.0
106
66-135
1,2,3-Trichloropropane
ug/L
50
50.1
100
75-130
1,2-Dibromo-3-chloropropane
ug/L
50
52.7
105
71-133
1,2-Dibromoethane (EDB)
ug/L
50
54.5
109
83-124
1,2-Dichlorobenzene
ug/L
50
50.4
101
80-133
1,2-Dichloroethane
ug/L
50
49.6
99
67-128
1,2-Dichloropropane
ug/L
50
48.8
98
75-132
1,4-Dichlorobenzene
ug/L
50
48.1
96
78-130
2-Butanone (MEK)
ug/L
100
90.5J
90
61-144
2-Hexanone
ug/L
100
100
100
68-143
4-Methyl-2-pentanone (MIBK)
ug/L
100
98.2J
98
72-135
Acetone
ug/L
100
103
103
48-146
Acrylonitrile
ug/L
250
240
96
40-160
Benzene
ug/L
50
50.2
100
80-125
Bromochloromethane
ug/L
50
52.3
105
71-125
Bromodichloromethane
ug/L
50
55.1
110
78-124
Bromoform
ug/L
50
53.9
108
71-128
Bromomethane
ug/L
50
42.6
85
40-160
Carbon disulfide
ug/L
50
52AJ
105
50-160
Carbon tetrachloride
ug/L
50
54.9
110
69-131
Chlorobenzene
ug/L
50
50.8
102
81-122
Chloroethane
ug/L
50
45.8
92
39-148
Chloroform
ug/L
50
51.5
103
73-127
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/30/2018 12:04 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 45

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
LABORATORY CONTROL SAMPLE:
2361842
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Chloromethane
ug/L
50
45.9
92
44-146
cis-1,2-Dichloroethene
ug/L
50
48.6
97
74-124
cis-1,3-Dichloropropene
ug/L
50
51.5
103
72-132
Dibromochloromethane
ug/L
50
54.5
109
78-125
Dibromomethane
ug/L
50
57.3
115
82-120
Ethylbenzene
ug/L
50
49.9
100
79-121
lodomethane
ug/L
100
124
124
39-154
Methylene Chloride
ug/L
50
53.4
107
64-133
Styrene
ug/L
50
50.8
102
84-126
Tetrachloroethene
ug/L
50
51.0
102
78-122
Tetrahydrofuran
ug/L
500
456
91
69-148
Toluene
ug/L
50
49.1
98
80-121
trans-1,2-Dichloroethene
ug/L
50
49.9
100
71-127
trans- 1,3-Dichloropropene
ug/L
50
52.2
104
69-141
trans-1,4-Dichloro-2-butene
ug/L
50
48.8J
98
40-160
Trichloroethene
ug/L
50
54.1
108
78-122
Trichlorofluoromethane
ug/L
50
54.5
109
53-137
Vinyl acetate
ug/L
100
99.2
99
40-160
Vinyl chloride
ug/L
50
56.7
113
58-137
Xylene (Total)
ug/L
150
153
102
81-126
1,2-Dichloroethane-d4 (S)
%
99
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene-d8 (S)
%
96
70-130
MATRIX SPIKE SAMPLE:
2361843
92396257003
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
20
21.4
107
70-130
1,1,1-Trichloroethane
ug/L
ND
20
21.9
110
70-130
1,1,2,2-Tetrachloroethane
ug/L
ND
20
19.5
97
70-130
1,1,2-Trichloroethane
ug/L
ND
20
20.4
102
70-130
1,1-Dichloroethane
ug/L
ND
20
20.1
100
70-130
1,1-Dichloroethene
ug/L
ND
20
23.6
118
70-166
1,2,3-Trichloropropane
ug/L
ND
20
19.9
99
70-130
1,2-Dibromo-3-chloropropane
ug/L
ND
20
19.0
95
70-130
1,2-Dibromoethane (EDB)
ug/L
ND
20
20.8
104
70-130
1,2-Dichlorobenzene
ug/L
ND
20
19.4
97
70-130
1,2-Dichloroethane
ug/L
ND
20
21.2
106
70-130
1,2-Dichloropropene
ug/L
ND
20
20.2
101
70-130
1,4-Dichlorobenzene
ug/L
ND
20
19.1
96
70-130
2-Butanone (MEK)
ug/L
ND
40
37.5J
94
70-130
2-Hexanone
ug/L
ND
40
39.7J
99
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
39.6J
99
70-130
Acetone
ug/L
ND
40
42.5J
106
70-130
Acrylonitrile
ug/L
ND
100
97.OJ
97
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/30/2018 12:04 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 45

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
MATRIX SPIKE SAMPLE:
Parameter
2361843
Units
92396257003
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Benzene
ug/L
ND
20
20.3
102
70-148
Bromochloromethane
ug/L
ND
20
20.9
105
70-130
Bromodichloromethane
ug/L
ND
20
22.1
110
70-130
Bromoform
ug/L
ND
20
19.5
98
70-130
Bromomethane
ug/L
ND
20
13.8
69
70-130 M1
Carbon disulfide
ug/L
ND
20
22.1J
111
70-130
Carbon tetrachloride
ug/L
ND
20
23.3
116
70-130
Chlorobenzene
ug/L
ND
20
20.5
102
70-146
Chloroethane
ug/L
ND
20
19.4
97
70-130
Chloroform
ug/L
ND
20
21.0
105
70-130
Chloromethane
ug/L
ND
20
21.0
105
70-130
cis-1,2-Dichloroethene
ug/L
ND
20
20.2
101
70-130
cis-1,3-Dichloropropene
ug/L
ND
20
19.3
97
70-130
Dibromochloromethane
ug/L
ND
20
20.8
104
70-130
Dibromomethane
ug/L
ND
20
22.8
114
70-130
Ethylbenzene
ug/L
ND
20
20.3
101
70-130
lodomethane
ug/L
ND
40
55.4
139
70-130 M1
Methylene Chloride
ug/L
ND
20
21.7
109
70-130
Styrene
ug/L
ND
20
19.8
99
70-130
Tetrachloroethene
ug/L
ND
20
20.6
103
70-130
Tetrahydrofuran
ug/L
ND
200
185
92
70-130
Toluene
ug/L
ND
20
19.9
99
70-155
trans-1,2-Dichloroethene
ug/L
ND
20
21.7
108
70-130
trans- 1,3-Dichloropropene
ug/L
ND
20
19.7
99
70-130
trans-1,4-Dichloro-2-butene
ug/L
ND
20
14.6J
73
70-130
Trichloroethene
ug/L
ND
20
21.8
109
69-151
Trichlorofluoromethane
ug/L
ND
20
25.4
127
70-130
Vinyl acetate
ug/L
ND
40
27.3J
68
70-130 M1
Vinyl chloride
ug/L
ND
20
24.4
122
70-130
Xylene (Total)
ug/L
ND
60
61.6
103
70-130
1,2-Dichloroethane-d4 (S)
%
101
70-130
4-Bromofluorobenzene (S)
%
97
70-130
Toluene-d8 (S)
%
97
70-130
SAMPLE DUPLICATE: 2361844
92396257004
Dup
Max
Parameter
Units
Result
Result RPD
RPD Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,1-Trichloroethane
ug/L
ND
ND
30
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,2-Trichloroethane
ug/L
ND
ND
30
1,1-Dichloroethane
ug/L
ND
ND
30
1,1-Dichloroethene
ug/L
ND
ND
30
1,2,3-Trichloropropane
ug/L
ND
ND
30
1,2-Dibromo-3-chloropropane
ug/L
ND
ND
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
SAMPLE DUPLICATE: 2361844
Parameter
Units
92396257004
Result
Dup
Result
1,2-Dibromoethane (EDB)
ug/L
ND
ND
1,2-Dichlorobenzene
ug/L
ND
ND
1,2-Dichloroethane
ug/L
ND
ND
1,2-Dichloropropane
ug/L
ND
ND
1,4-Dichlorobenzene
ug/L
ND
ND
2-Butanone (MEK)
ug/L
ND
ND
2-Hexanone
ug/L
ND
ND
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
Acetone
ug/L
ND
ND
Acrylonitrile
ug/L
ND
ND
Benzene
ug/L
ND
ND
Bromochloromethane
ug/L
ND
ND
Bromodichloromethane
ug/L
ND
ND
Bromoform
ug/L
ND
ND
Bromomethane
ug/L
ND
ND
Carbon disulfide
ug/L
ND
ND
Carbon tetrachloride
ug/L
ND
ND
Chlorobenzene
ug/L
ND
ND
Chloroethane
ug/L
ND
ND
Chloroform
ug/L
ND
ND
Chloromethane
ug/L
ND
ND
cis-1,2-Dichloroethene
ug/L
ND
ND
cis-1,3-Dichloropropene
ug/L
ND
ND
Dibromochloromethane
ug/L
ND
ND
Dibromomethane
ug/L
ND
ND
Ethylbenzene
ug/L
ND
ND
lodomethane
ug/L
ND
ND
Methylene Chloride
ug/L
ND
ND
Styrene
ug/L
ND
ND
Tetrachloroethene
ug/L
ND
ND
Tetrahydrofuran
ug/L
ND
ND
Toluene
ug/L
ND
ND
trans-1,2-Dichloroethene
ug/L
ND
ND
trans- 1,3-Dichloropropene
ug/L
ND
ND
trans-1,4-Dichloro-2-butene
ug/L
ND
ND
Trichloroethene
ug/L
ND
ND
Trichlorofluoromethane
ug/L
ND
ND
Vinyl acetate
ug/L
ND
ND
Vinyl chloride
ug/L
ND
ND
Xylene (Total)
ug/L
ND
ND
1,2-Dichloroethane-d4 (S)
%
103
102
4-Bromofluorobenzene (S)
%
95
93
Toluene-d8 (S)
%
99
99
Max
RPD RPD Qualifiers
0
2
0
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/30/2018 12:04 PM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
QC Batch: 426318 Analysis Method: EPA 8260B Mod.
QC Batch Method: EPA 8260E Mod. Analysis Description: 8260 MSV SIM
Associated Lab Samples: 92396265001, 92396265002, 92396265003, 92396265004, 92396265005, 92396265006, 92396265007
METHOD BLANK: 2356318
Matrix:
Water
Associated Lab Samples:
92396265001, 92396265002, 92396265003, 92396265004, 92396265005, 92396265006, 92396265007
Blank
Reporting
Parameter
Units
Result
Limit
MDL Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
1.9 08/23/18 14:49
1,2-Dichloroethane-d4 (S)
%
95
50-150
08/23/18 14:49
Toluene-d8 (S)
%
114
50-150
08/23/18 14:49
LABORATORY CONTROL SAMPLE: 2356319
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 16.6 83 71-125
1,2-Dichloroethane-d4 (S) % 95 50-150
Toluene-d8(S) % 113 50-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2356320
2356321
MS
MSD
92396277008 Spike
Spike MS
MSD MS
MSD
% Rec
Max
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits
RPD RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 16.4
16.4 79
79
50-150
0 30
1,2-Dichloroethane-d4 (S)
%
99
98
50-150
30
Toluene-d8 (S)
%
114
115
50-150
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/30/2018 12:04 PM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
QC Batch: 426910
Analysis Method: SM 2320B-2011
QC Batch Method: SM 2320B-2011
Analysis Description: 2320E Alkalinity
Associated Lab Samples: 92396265002, 92396265005
METHOD BLANK: 2358896
Matrix: Water
Associated Lab Samples: 92396265002, 92396265005
Blank Reporting
Parameter Units
Result Limit MDL Analyzed
Qualifiers
Alkalinity, Total as CaCO3 ug/L
ND 5000 1000 08/24/18 19:05
LABORATORY CONTROL SAMPLE: 2358897
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Alkalinity, Total as CaCO3 ug/L
50000 50000 100 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2358898 2358899
MS MSD
92396797013
Spike Spike MS MSD MS MSD
% Rec Max
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD RPD Qual
Alkalinity, Total as CaCO3 ug/L 88.0 mg/L
50000 50000 136000 136000 96 96
80-120 0 25
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2358900 2358901
MS MSD
92396834004 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Alkalinity, Total as CaCO3 ug/L 12.7 mg/L 50000 50000 61800 64600 98 104 80-120 4 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/30/2018 12:04 PM without the written consent of Pace Analytical Services, LLC.
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Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
QC Batch: 427280
Analysis Method: SM 2320B-2011
QC Batch Method: SM 2320B-2011
Analysis Description: 2320E Alkalinity
Associated Lab Samples: 92396265001, 92396265003,
92396265004
METHOD BLANK: 2360642
Matrix: Water
Associated Lab Samples: 92396265001, 92396265003,
92396265004
Blank Reporting
Parameter Units
Result Limit MDL Analyzed
Qualifiers
Alkalinity, Total as CaCO3 ug/L
ND 5000 1000 08/27/18 22:09
LABORATORY CONTROL SAMPLE: 2360643
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Alkalinity, Total as CaCO3 ug/L
50000 50200 100 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2360644 2360645
MS MSD
92397010023
Spike Spike MS MSD MS MSD
% Rec Max
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD RPD Qual
Alkalinity, Total as CaCO3 ug/L 29.9 mg/L
50000 50000 78800 78900 98 98
80-120 0 25
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2360659 2360660
MS MSD
92396725004 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Alkalinity, Total as CaCO3 ug/L 46.0 mg/L 50000 50000 96500 95400 101 99 80-120 1 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/30/2018 12:04 PM without the written consent of Pace Analytical Services, LLC.
Page 36 of 45

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Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
QC Batch: 425717
Analysis Method: SM 2540C-2011
QC Batch Method: SM 2540C-2011
Analysis Description: 2540C Total Dissolved Solids
Associated Lab Samples: 92396265001, 92396265002, 92396265003, 92396265004, 92396265005
METHOD BLANK: 2353818
Matrix: Water
Associated Lab Samples: 92396265001, 92396265002, 92396265003, 92396265004, 92396265005
Blank Reporting
Parameter
Units
Result Limit MDL
Analyzed Qualifiers
Total Dissolved Solids
ug/L
ND 25000 25000
08/17/18 22:45
LABORATORY CONTROL SAMPLE:
2353819
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
Total Dissolved Solids
ug/L
250000 234000 93
90-110
SAMPLE DUPLICATE: 2353820
92396265002 Dup
Max
Parameter
Units
Result Result RPD
RPD Qualifiers
Total Dissolved Solids
ug/L
164000 169000 3
5
SAMPLE DUPLICATE: 2353821
92396149007 Dup
Max
Parameter
Units
Result Result RPD
RPD Qualifiers
Total Dissolved Solids
ug/L
119 mg/L 121000 2
5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
QC Batch: 426573
Analysis Method: EPA 300.0 Rev 2.1 1993
QC Batch Method: EPA 300.0 Rev 2.1 1993
Analysis Description: 300.0 IC Anions
Associated Lab Samples: 92396265001
METHOD BLANK: 2357505
Matrix: Water
Associated Lab Samples: 92396265001
Blank Reporting
Parameter Units
Result Limit
MDL
Analyzed
Qualifiers
Sulfate ug/L
ND 250000
500 08/24/18 01:34
LABORATORY CONTROL SAMPLE: 2357506
Spike LCS
LCS
% Rec
Parameter Units
Conc. Result
% Rec
Limits Qualifiers
Sulfate ug/L
50000 49000J
98
90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2357507 2357508
MS MSD
92396726011
Spike Spike MS
MSD
MS MSD
% Rec Max
Parameter Units Result
Conc. Conc. Result
Result
% Rec % Rec
Limits RPD RPD Qual
Sulfate ug/L 2.9 mg/L
50000 50000 56700J
55800J
108 106
90-110 2 10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2357509 2357510
MS MSD
92396726021 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Sulfate ug/L 3.4 mg/L 50000 50000 54700J 56000J 103 105 90-110 2 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/30/2018 12:04 PM without the written consent of Pace Analytical Services, LLC.
Page 38 of 45

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
QC Batch: 426945
Analysis Method: EPA 300.0 Rev 2.1 1993
QC Batch Method: EPA 300.0 Rev 2.1 1993
Analysis Description: 300.0 IC Anions
Associated Lab Samples: 92396265002, 92396265003,
92396265004, 92396265005
METHOD BLANK: 2359118
Matrix: Water
Associated Lab Samples: 92396265002, 92396265003,
92396265004, 92396265005
Blank Reporting
Parameter Units
Result Limit
MDL
Analyzed
Qualifiers
Sulfate ug/L
ND 250000
500 08/25/18 00:43
LABORATORY CONTROL SAMPLE: 2359119
Spike LCS
LCS
% Rec
Parameter Units
Conc. Result
% Rec
Limits Qualifiers
Sulfate ug/L
50000 49400J
99
90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2359120 2359121
MS MSD
92396834001
Spike Spike MS
MSD
MS MSD
% Rec Max
Parameter Units Result
Conc. Conc. Result
Result
% Rec % Rec
Limits RPD RPD Qual
Sulfate ug/L 2.8 mg/L
50000 50000 54500J
55700J
103 106
90-110 2 10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2359122 2359123
MS MSD
92396834011 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Sulfate ug/L 3.4 mg/L 50000 50000 54100J 55400J 101 104 90-110 2 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/30/2018 12:04 PM without the written consent of Pace Analytical Services, LLC.
Page 39 of 45

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[phone]
QUALIFIERS
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Oxford Compliance Unit 1
92396265
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92396265001
3901-MW2
EPA 3010A
427103
EPA 6010D
427125
92396265002
3901-MW3R
EPA 3010A
427103
EPA 6010D
427125
92396265003
3901-MW4R
EPA 3010A
427103
EPA 6010D
427125
92396265004
3901-MW5R
EPA 3010A
427103
EPA 6010D
427125
92396265005
3901-MW6R
EPA 3010A
427103
EPA 6010D
427125
92396265006
3901-SW1
EPA 3010A
427103
EPA6010D
427125
92396265007
3901-SW2
EPA 3010A
427103
EPA 6010D
427125
92396265001
3901-MW2
EPA 3010A
425734
EPA 6020B
425756
92396265002
3901-MW3R
EPA 3010A
425734
EPA 6020B
425756
92396265003
3901-MW4R
EPA 3010A
425734
EPA 6020B
425756
92396265004
3901-MW5R
EPA 3010A
425734
EPA 6020B
425756
92396265005
3901-MW6R
EPA 3010A
425734
EPA 6020B
425756
92396265006
3901-SW1
EPA 3010A
425734
EPA 6020B
425756
92396265007
3901-SW2
EPA 3010A
425734
EPA 6020B
425756
92396265001
3901-MW2
EPA 7470A
426302
EPA 7470A
426432
92396265002
3901-MW3R
EPA 7470A
426302
EPA 7470A
426432
92396265003
3901-MW4R
EPA 7470A
426302
EPA 7470A
426432
92396265004
3901-MW5R
EPA 7470A
425829
EPA 7470A
426024
92396265005
3901-MW6R
EPA 7470A
426302
EPA 7470A
426432
92396265001
3901-MW2
EPA 8260B
427539
92396265002
3901-MW3R
EPA 8260B
427539
92396265003
3901-MW4R
EPA 8260B
427539
92396265004
3901-MW5R
EPA 8260B
427539
92396265005
3901-MW6R
EPA 8260B
427539
92396265006
3901-SW1
EPA 8260B
427539
92396265007
3901-SW2
EPA 8260B
427539
92396265008
Trip Blank
EPA 8260B
427539
92396265001
3901-MW2
EPA 8260B Mod.
426318
92396265002
3901-MW3R
EPA 8260B Mod.
426318
92396265003
3901-MW4R
EPA 8260B Mod.
426318
92396265004
3901-MW5R
EPA 8260B Mod.
426318
92396265005
3901-MW6R
EPA 8260B Mod.
426318
92396265006
3901-SW1
EPA 8260B Mod.
426318
92396265007
3901-SW2
EPA 8260B Mod.
426318
92396265001
3901-MW2
SM 2320B-2011
427280
92396265002
3901-MW3R
SM 2320B-2011
426910
92396265003
3901-MW4R
SM 2320B-2011
427280
92396265004
3901-MW5R
SM 2320B-2011
427280
92396265005
3901-MW6R
SM 2320B-2011
426910
92396265001
3901-MW2
SM 254OC-2011
425717
92396265002
3901-MW3R
SM 2540C-2011
425717
92396265003
3901-MW4R
SM 2540C-2011
425717
92396265004
3901-MW5R
SM 2540C-2011
425717
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 08/30/2018 12:04 PM
without the written consent of Pace Analytical Services, LLC.
Page 41 of 45

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Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Oxford Compliance Unit 1
Pace Project No.: 92396265
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
92396265005
3901-MW6R
SM 2540C-2011
425717
92396265001
3901-MW2
EPA 300.0
Rev 2.1 1993
426573
92396265002
3901-MW3R
EPA 300.0
Rev 2.1 1993
426945
92396265003
3901-MW4R
EPA 300.0
Rev 2.1 1993
426945
92396265004
3901-MW5R
EPA 300.0
Rev 2.1 1993
426945
92396265005
3901-MW6R
EPA 300.0
Rev 2.1 1993
426945
Date: 08/30/2018 12:04 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Batch
Page 42 of 45

Document Name:
Document Revised: February 7, 2018
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
c?C�f�I?a��flL�
F-CAR•CS-033-Rev.06
Pace Caroiinas Quality Office
-_
Ca oiratoryrecet`vving5artlpe_s:-:..:_-_.:-._----' —r� ---- ...-•----- ---
Asheville ❑ Eden❑ Greenwood ❑ Huntersville DI
Sample Condition Client Name:
Upon Receipt Project #:
Courier: ❑Fpd Ex EUPS ❑USPs ❑Client
❑ Commercial ❑Face []Other:
-
Custody Seal Present? ❑Yes ONo seals Intact? ❑Yes �]No
Raleigh[]
Mechanicsville❑
WO#:92396265
1111111111111111111111
92396265
Date/Initials Person Examining Contents: ' I) i f rl f 1' y
Packing Material: ❑Bubble Wrap ❑Bubble Bags ❑None ❑ Other Biological Tissue Frozen?
[]Yes [:]No '❑N/A
Thermometer: PIR Gun ID: 92T043 Type of Ice: ZWet [:]Blue ❑W.ie
Cooler Temp (°C): L l Correction Factor: Add/Subtract ('Q _0 2
Tempshould be above freezing to 6°C
Cooler Temp Corrected (°C): - ] ❑Samples cut of temp criteria. Samples on ice, cooling process
i hasbegun
USDA Regulated Soil (❑ N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did sanplesoriginate from a foreign source {internationally,
nyps FINn Includ!og Hawaii and Puerto Rico)? []Yes ❑No
Comments/Discrepancy:
Chain of Custody Present?
Elyes
❑ in
❑N/A
1.
Samples Arrived within Hold Time?
Yes
[]No
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
[]Yes
\31Nc
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
❑No
❑N/A
4.
Sufficient volume?
i Yes
❑No
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
❑Yes
❑Yes
❑No
❑No
❑N/A
❑N/A
5.
Containers Intact?
Yes
❑No
❑N/A
7.
Dissolved analysis: Samples Field Filtered? []yes
❑No
❑N/A
8.
Sample Labels Match CDC?
-Includes Datel-Fime/ID/Analysis
}Yes ❑No
y
Matrix: Li,
❑N/A
9.
Headspace in VOA Vials (>5-6mm)?
❑Yes-
❑No
❑N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
�;]4es
❑,Yes
❑No
[-]No
[]NIA
❑N/A
11.
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Date/Time:
4YL
Field Data Required? Dyes ❑No
Lot ID of sDlit containers:
Dat(a: L� �7-C1)
Date: 2�
Page 43 of 45

Document Name:
Document Revised: February 7, 2018
a
Sample Condition Upon Receipt(sCUR)
Page 1 of 2
Document No.:
Issuing Authority:
aceAnalytrcal
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
-_ -- - .62.65
*Check mark top half of box if pH and/or dechlorination is Project # ' WO# :9239
verified and within the acceptance range for preservation t'hi ; NMG T
Due Date: 08/31/18
samples, Exceptions; VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg CLIENT: 92-Joyce Eno
"Bottom half of box is to list number of bottle
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot 9
Nate: wneneverthere is a discrepancy arresting Norm Laraina compuance samples, a LUYY V1 Ll 113 1-1 Ue 5cnk w L
Out of hold, incorrect preserlative, out of temp, incorrect containers.
Page 44 of 45

CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Section B Section C
Required Client Information: Required Project Information: Invoice Information; Pa(le : 1 Of 1
Company: Joyce Engineering Report TO: Van Burbach Attention: Jason Falls
Address: 2211 West Meadowview Rd Copy To: Miguel Vazquez Company Name: Granville County, Solid Waste
Greensboro, NC 27407
Address, P.O. Box 906, Oxford NC 27565
Regulatory Agency
Email To: vburbach io teen ineerin .Com
Purchase Order No.
Phone, 336 323-0092 1FaK
Client Project ID: Oxford Cam lianee Unit 1
Pace PM: Nicole Gasioi
State I Location
Requested Due DaterTAT: 10 Da Default
Container Order Number:
Profile: 35664
North Carolina
Re
uested
Analysis
Filtered
YIN
_
E
2
MATRIX CODE
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Preservatives
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ADDITIONAL COMMENTS
RELINQUISHED BY I AFFILIATION
DATE
TIME
ACCEPTED BY I AFFILIATION
DATE
TIME
SAMPLE CONDITIONS
C&D Parameters = Iron. Manganese, Mercury,
q WK
Dg 17AV
093
'
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Alkalinity, Chloride, Sulfate, TDS, and
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SIGNATURE of SA R' BATE Signed:
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0-

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
September 13, 2018
Mr. Van Burbach
Joyce Engineering -NC
2211 West Meadowview Rd
Boone Bldg, Suite 101
Greensboro, NC 27407
RE: Project: OXFORD UNITS 1&2 BLANKS JOINT
Pace Project No.: 92396142
Dear Mr. Burbach:
Enclosed are the analytical results for sample(s) received by the laboratory between August 16,
2018 and August 17, 2018. The results relate only to the samples included in this report. Results
reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's
Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report.
This revision was issued on 9/13/18 to include the chloride data for sample 3901-MW-7. This data
did not show up on the original report due to an IT issue.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Gasiorowski
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Daniel Girdner, LaBella Associates, D.P.C.
Miguel Vazquez, Joyce Engineering
Rochelle mesubed, Joyce Engineering
�pQ ACrfFO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
9e0 without the written consent of Pace Analytical Services, LLC.
Page 1 of 41

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: OXFORD UNITS 1&2 BLANKS JOINT
Pace Project No.: 92396142
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 41

aceAnalytical
—pacelabsxom
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: OXFORD UNITS 1&2 BLANKS JOINT
Pace Project No.: 92396142
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92396142001
3901-MW-7
Water
08/15/1810:51
08/16/1810:00
92396142003
3901-NES-2S
Water
08/15/1814:16
08/16/1810:00
92396142005
3901- Trip Blank
Water
08/14/18 05:30
08/17/18 09:37
92396142006
3901- Field Blank
Water
08/16/18 16:30
08/17/18 09:37
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 41

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
OXFORD UNITS 1&2 BLANKS JOINT
92396142
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92396142001
3901-MW-7
EPA 601 OD
DS
16
PASI-A
EPA6020B
JMW1
1
PASI-A
EPA7470A
JMW1
1
PASI-A
EPA 8260E
CAH
51
PASI-C
EPA 8260B Mod.
DLK
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
SM 2540C-2011
CRV
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
2
PASI-A
92396142003
3901-NES-2S
EPA 601 OD
DS
14
PASI-A
EPA6020B
JMW1
1
PASI-A
EPA 8260E
CAH
50
PASI-C
EPA 8260B Mod.
DLK
3
PASI-C
92396142005
3901- Trip Blank
EPA 8260E
CAH
51
PASI-C
92396142006
3901- Field Blank
EPA 601 OD
DS
16
PASI-A
EPA6020B
JMW1
1
PASI-A
EPA7470A
JMW1
1
PASI-A
EPA 8260E
CAH
51
PASI-C
EPA 8260B Mod.
DLK
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
SM 2540C-2011
NAL
1
PASI-A
EPA 300.0 Rev 2.1 1993
KDF1
2
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 41

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SUMMARY OF DETECTION
Project: OXFORD UNITS 1&2 BLANKS JOINT
Pace Project No.: 92396142
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed Qualifiers
92396142001
3901-MW-7
EPA 601 OD
Barium
3.8J
ug/L
100
08/21/18 22:37
EPA 601 OD
Iron
340
ug/L
300
08/21/18 22:37
EPA 601 OD
Manganese
6.7J
ug/L
50.0
08/21/18 22:37
SM 2320B-2011
Alkalinity, Total as CaCO3
124000
ug/L
5000
08/24/18 20:54
SM 2540C-2011
Total Dissolved Solids
249000
ug/L
25000
08/17/18 16:50
EPA 300.0 Rev 2.1 1993
Chloride
9720
ug/L
1000
08/24/18 09:14
EPA 300.0 Rev 2.1 1993
Sulfate
51400J
ug/L
250000
08/24/18 09:14
92396142003
3901-NES-2S
EPA 601 OD
Barium
25.8J
ug/L
100
08/21/18 22:46
EPA 601 OD
Vanadium
2.5J
ug/L
25.0
08/21/18 22:46
92396142006
3901-Field Blank
EPA 601 OD
Iron
27.8J
ug/L
300
08/25/18 22:56
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 5 of 41

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD UNITS 1&2 BLANKS JOINT
Pace Project No.: 92396142
Sample: 3901-MW-7 Lab ID: 92396142001 Collected: 08/15/18 10:51 Received: 08/16/18 10:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
7470 Mercury
Mercury
8260 MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
Date: 09/13/2018 12:26 PM
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
ND
ug/L
6.0
3.9
1
08/17/18 07:28
08/21/18 22:37
7440-36-0
ND
ug/L
10.0
5.0
1
08/17/18 07:28
08/21/18 22:37
7440-38-2
3.8J
ug/L
100
2.5
1
08/17/18 07:28
08/21/18 22:37
7440-39-3
ND
ug/L
1.0
0.50
1
08/17/18 07:28
08/21/18 22:37
7440-41-7
ND
ug/L
1.0
0.50
1
08/17/18 07:28
08/21/18 22:37
7440-43-9
ND
ug/L
10.0
2.5
1
08/17/18 07:28
08/21/18 22:37
7440-47-3
ND
ug/L
10.0
2.5
1
08/17/18 07:28
08/21/18 22:37
7440-48-4
ND
ug/L
10.0
2.5
1
08/17/18 07:28
08/21/18 22:37
7440-50-8
340
ug/L
300
25.0
1
08/17/18 07:28
08/21/18 22:37
7439-89-6
ND
ug/L
10.0
2.5
1
08/17/18 07:28
08/21/18 22:37
7439-92-1
6.7J
ug/L
50.0
2.5
1
08/17/18 07:28
08/21/18 22:37
7439-96-5
ND
ug/L
50.0
2.5
1
08/17/18 07:28
08/21/18 22:37
7440-02-0
ND
ug/L
10.0
5.0
1
08/17/18 07:28
08/21/18 22:37
7782-49-2
ND
ug/L
10.0
2.5
1
08/17/18 07:28
08/21/18 22:37
7440-22-4
ND
ug/L
25.0
2.5
1
08/17/18 07:28
08/21/18 22:37
7440-62-2
ND
ug/L
10.0
5.0
1
08/17/18 07:28
08/21/18 22:37
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
ND ug/L 5.5 0.020 1 08/17/18 07:17 08/23/18 22:33 7440-28-0
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
ND ug/L 0.20 0.10 1 08/20/1819:25 08/21/1813:23 7439-97-6
Analytical Method: EPA 8260E
ND
ug/L
100
ND
ug/L
200
ND
ug/L
1.0
ND
ug/L
3.0
ND
ug/L
1.0
ND
ug/L
3.0
ND
ug/L
10.0
ND
ug/L
100
ND
ug/L
100
ND
ug/L
1.0
ND
ug/L
3.0
ND
ug/L
10.0
ND
ug/L
5.0
ND
ug/L
1.0
ND
ug/L
13.0
ND
ug/L
3.0
ND
ug/L
1.0
ND
ug/L
10.0
ND
ug/L
5.0
ND
ug/L
1.0
ND
ug/L
100
ND
ug/L
5.0
10.0
1
08/19/18 16:20
67-64-1
1.9
1
08/19/18 16:20
107-13-1
0.25
1
08/19/18 16:20
71-43-2
0.17
1
08/19/18 16:20
74-97-5
0.18
1
08/19/18 16:20
75-27-4
0.26
1
08/19/18 16:20
75-25-2
0.29
1
08/19/18 16:20
74-83-9
0.96
1
08/19/18 16:20
78-93-3
1.2
1
08/19/18 16:20
75-15-0
0.25
1
08/19/18 16:20
56-23-5
0.23
1
08/19/18 16:20
108-90-7
0.54
1
08/19/18 16:20
75-00-3
0.14
1
08/19/18 16:20
67-66-3
0.11
1
08/19/18 16:20
74-87-3
2.0
1
08/19/18 16:20
96-12-8
0.21
1
08/19/18 16:20
124-48-1
0.27
1
08/19/18 16:20
106-93-4
0.21
1
08/19/18 16:20
74-95-3
0.30
1
08/19/18 16:20
95-50-1
0.33
1
08/19/18 16:20
106-46-7
1.0
1
08/19/18 16:20
110-57-6
0.32
1
08/19/18 16:20
75-34-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 41

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD UNITS 1&2 BLANKS JOINT
Pace Project No.: 92396142
Sample: 3901-MW-7 Lab ID: 92396142001 Collected: 08/15/18 10:51 Received: 08/16/18 10:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill Analytical Method: EPA 8260E
1,2-Dichloroethane
ND
ug/L
1.0
0.24
1
08/19/18 16:20
107-06-2
1,1-Dichloroethene
ND
ug/L
5.0
0.56
1
08/19/18 16:20
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
5.0
0.19
1
08/19/18 16:20
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
5.0
0.49
1
08/19/18 16:20
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.27
1
08/19/18 16:20
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.13
1
08/19/18 16:20
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.26
1
08/19/18 16:20
10061-02-6
Ethylbenzene
ND
ug/L
1.0
0.30
1
08/19/18 16:20
100-41-4
2-Hexanone
ND
ug/L
50.0
0.46
1
08/19/18 16:20
591-78-6
lodomethane
ND
ug/L
10.0
0.32
1
08/19/18 16:20
74-88-4
Methylene Chloride
ND
ug/L
1.0
0.97
1
08/19/18 16:20
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
100
0.33
1
08/19/18 16:20
108-10-1
Styrene
ND
ug/L
1.0
0.26
1
08/19/18 16:20
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
5.0
0.33
1
08/19/18 16:20
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
3.0
0.40
1
08/19/18 16:20
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.46
1
08/19/18 16:20
127-18-4
Tetrahydrofuran
ND
ug/L
10.0
3.1
1
08/19/18 16:20
109-99-9
Toluene
ND
ug/L
1.0
0.26
1
08/19/18 16:20
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.48
1
08/19/18 16:20
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.29
1
08/19/18 16:20
79-00-5
Trichloroethene
ND
ug/L
1.0
0.47
1
08/19/18 16:20
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.20
1
08/19/18 16:20
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.41
1
08/19/18 16:20
96-18-4
Vinyl acetate
ND
ug/L
50.0
0.35
1
08/19/18 16:20
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.62
1
08/19/18 16:20
75-01-4
Xylene (Total)
ND
ug/L
5.0
0.66
1
08/19/18 16:20
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
94
%
70-130
1
08/19/18 16:20
460-00-4
1,2-Dichloroethane-d4 (S)
101
%
70-130
1
08/19/18 16:20
17060-07-0
Toluene-d8 (S)
99
%
70-130
1
08/19/18 16:20
2037-26-5
8260 MSV SIM
Analytical Method: EPA 8260E Mod.
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1.9
1
08/23/18 18:04
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
99
%
50-150
1
08/23/18 18:04
17060-07-0
Toluene-d8 (S)
118
%
50-150
1
08/23/18 18:04
2037-26-5
2320B Alkalinity
Analytical Method: SM
2320B-2011
Alkalinity, Total as CaCO3
124000
ug/L
5000
1000
1
08/24/18 20:54
2540C Total Dissolved Solids
Analytical Method: SM
2540C-2011
Total Dissolved Solids
249000
ug/L
25000
25000
1
08/17/18 16:50
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1
1993
Chloride
9720
ug/L
1000
500
1
08/24/18 09:14
16887-00-6
Sulfate
51400J
ug/L
250000
500
1
08/24/18 09:14
14808-79-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2018 12:26 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 41

aceAnalytical
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ANALYTICAL RESULTS
Project: OXFORD UNITS 1&2 BLANKS JOINT
Pace Project No.: 92396142
Sample: 3901-NES-2S Lab ID: 92396142003 Collected: 08/15/18 14:16 Received: 08/16/18 10:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
8260 MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
Date: 09/13/2018 12:26 PM
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
ND
ug/L
6.0
3.9
1
08/17/18 07:28
08/21/18 22:46
7440-36-0
ND
ug/L
10.0
5.0
1
08/17/18 07:28
08/21/18 22:46
7440-38-2
25.8J
ug/L
100
2.5
1
08/17/18 07:28
08/21/18 22:46
7440-39-3
ND
ug/L
1.0
0.50
1
08/17/18 07:28
08/21/18 22:46
7440-41-7
ND
ug/L
1.0
0.50
1
08/17/18 07:28
08/21/18 22:46
7440-43-9
ND
ug/L
10.0
2.5
1
08/17/18 07:28
08/21/18 22:46
7440-47-3
ND
ug/L
10.0
2.5
1
08/17/18 07:28
08/21/18 22:46
7440-48-4
ND
ug/L
10.0
2.5
1
08/17/18 07:28
08/21/18 22:46
7440-50-8
ND
ug/L
10.0
2.5
1
08/17/18 07:28
08/21/18 22:46
7439-92-1
ND
ug/L
50.0
2.5
1
08/17/18 07:28
08/21/18 22:46
7440-02-0
ND
ug/L
10.0
5.0
1
08/17/18 07:28
08/21/18 22:46
7782-49-2
ND
ug/L
10.0
2.5
1
08/17/18 07:28
08/21/18 22:46
7440-22-4
2.5J
ug/L
25.0
2.5
1
08/17/18 07:28
08/21/18 22:46
7440-62-2
ND
ug/L
10.0
5.0
1
08/17/18 07:28
08/21/18 22:46
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
ND ug/L 5.5 0.020 1 08/17/18 07:17 08/23/18 22:41 7440-28-0
Analytical Method: EPA 8260E
ND
ug/L
100
10.0
1
08/19/1816:36
67-64-1
ND
ug/L
200
1.9
1
08/19/1816:36
107-13-1
ND
ug/L
1.0
0.25
1
08/19/1816:36
71-43-2
ND
ug/L
3.0
0.17
1
08/19/1816:36
74-97-5
ND
ug/L
1.0
0.18
1
08/19/1816:36
75-27-4
ND
ug/L
3.0
0.26
1
08/19/1816:36
75-25-2
ND
ug/L
10.0
0.29
1
08/19/1816:36
74-83-9
ND
ug/L
100
0.96
1
08/19/1816:36
78-93-3
ND
ug/L
100
1.2
1
08/19/1816:36
75-15-0
ND
ug/L
1.0
0.25
1
08/19/1816:36
56-23-5
ND
ug/L
3.0
0.23
1
08/19/1816:36
108-90-7
ND
ug/L
10.0
0.54
1
08/19/1816:36
75-00-3
ND
ug/L
5.0
0.14
1
08/19/1816:36
67-66-3
ND
ug/L
1.0
0.11
1
08/19/1816:36
74-87-3
ND
ug/L
13.0
2.0
1
08/19/1816:36
96-12-8
ND
ug/L
3.0
0.21
1
08/19/1816:36
124-48-1
ND
ug/L
1.0
0.27
1
08/19/1816:36
106-93-4
ND
ug/L
10.0
0.21
1
08/19/1816:36
74-95-3
ND
ug/L
5.0
0.30
1
08/19/1816:36
95-50-1
ND
ug/L
1.0
0.33
1
08/19/1816:36
106-46-7
ND
ug/L
100
1.0
1
08/19/1816:36
110-57-6
ND
ug/L
5.0
0.32
1
08/19/1816:36
75-34-3
ND
ug/L
1.0
0.24
1
08/19/1816:36
107-06-2
ND
ug/L
5.0
0.56
1
08/19/1816:36
75-35-4
ND
ug/L
5.0
0.19
1
08/19/1816:36
156-59-2
ND
ug/L
5.0
0.49
1
08/19/1816:36
156-60-5
ND
ug/L
1.0
0.27
1
08/19/1816:36
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 41

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[phone]
ANALYTICAL RESULTS
Project: OXFORD UNITS 1&2 BLANKS JOINT
Pace Project No.: 92396142
Sample: 3901-NES-2S Lab ID: 92396142003 Collected: 08/15/18 14:16 Received: 08/16/18 10:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260 MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 09/13/2018 12:26 PM
Analytical Method: EPA 8260E
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
50.0
ND
ug/L
10.0
ND
ug/L
1.0
ND
ug/L
100
ND
ug/L
1.0
ND
ug/L
5.0
ND
ug/L
3.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
50.0
ND
ug/L
1.0
ND
ug/L
5.0
95
%
70-130
100
%
70-130
98
%
70-130
Analytical Method: EPA 8260E Mod.
ND
ug/L
2.0
98
%
50-150
113
%
50-150
0.13
1
08/19/18 16:36
10061-01-5
0.26
1
08/19/18 16:36
10061-02-6
0.30
1
08/19/18 16:36
100-41-4
0.46
1
08/19/18 16:36
591-78-6
0.32
1
08/19/18 16:36
74-88-4
0.97
1
08/19/18 16:36
75-09-2
0.33
1
08/19/18 16:36
108-10-1
0.26
1
08/19/18 16:36
100-42-5
0.33
1
08/19/18 16:36
630-20-6
0.40
1
08/19/18 16:36
79-34-5
0.46
1
08/19/18 16:36
127-18-4
0.26
1
08/19/18 16:36
108-88-3
0.48
1
08/19/18 16:36
71-55-6
0.29
1
08/19/18 16:36
79-00-5
0.47
1
08/19/18 16:36
79-01-6
0.20
1
08/19/18 16:36
75-69-4
0.41
1
08/19/18 16:36
96-18-4
0.35
1
08/19/18 16:36
108-05-4
0.62
1
08/19/18 16:36
75-01-4
0.66
1
08/19/18 16:36
1330-20-7
1
08/19/18 16:36
460-00-4
1
08/19/18 16:36
17060-07-0
1
08/19/18 16:36
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
08/21 /18 18:53 123-91-1
08/21 /18 18:53 17060-07-0
08/21 /18 18:53 2037-26-5
Page 9 of 41

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD UNITS 1&2 BLANKS JOINT
Pace Project No.: 92396142
Sample: 3901- Trip Blank Lab ID: 92396142005 Collected: 08/14/18 05:30 Received: 08/17/18 09:37 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill Analytical Method: EPA 8260E
Acetone
ND
ug/L
100
10.0
1
08/19/18 16:52
67-64-1
Acrylonitrile
ND
ug/L
200
1.9
1
08/19/18 16:52
107-13-1
Benzene
ND
ug/L
1.0
0.25
1
08/19/18 16:52
71-43-2
Bromochloromethane
ND
ug/L
3.0
0.17
1
08/19/18 16:52
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.18
1
08/19/18 16:52
75-27-4
Bromoform
ND
ug/L
3.0
0.26
1
08/19/18 16:52
75-25-2
Bromomethane
ND
ug/L
10.0
0.29
1
08/19/18 16:52
74-83-9
2-Butanone (MEK)
ND
ug/L
100
0.96
1
08/19/18 16:52
78-93-3
Carbon disulfide
ND
ug/L
100
1.2
1
08/19/18 16:52
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.25
1
08/19/18 16:52
56-23-5
Chlorobenzene
ND
ug/L
3.0
0.23
1
08/19/18 16:52
108-90-7
Chloroethane
ND
ug/L
10.0
0.54
1
08/19/18 16:52
75-00-3
Chloroform
ND
ug/L
5.0
0.14
1
08/19/18 16:52
67-66-3
Chloromethane
ND
ug/L
1.0
0.11
1
08/19/18 16:52
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
13.0
2.0
1
08/19/18 16:52
96-12-8
Dibromochloromethane
ND
ug/L
3.0
0.21
1
08/19/18 16:52
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
08/19/18 16:52
106-93-4
Dibromomethane
ND
ug/L
10.0
0.21
1
08/19/18 16:52
74-95-3
1,2-Dichlorobenzene
ND
ug/L
5.0
0.30
1
08/19/18 16:52
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
08/19/18 16:52
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
100
1.0
1
08/19/18 16:52
110-57-6
1,1-Dichloroethane
ND
ug/L
5.0
0.32
1
08/19/18 16:52
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.24
1
08/19/18 16:52
107-06-2
1,1-Dichloroethene
ND
ug/L
5.0
0.56
1
08/19/18 16:52
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
5.0
0.19
1
08/19/18 16:52
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
5.0
0.49
1
08/19/18 16:52
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.27
1
08/19/18 16:52
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.13
1
08/19/18 16:52
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.26
1
08/19/18 16:52
10061-02-6
Ethylbenzene
ND
ug/L
1.0
0.30
1
08/19/18 16:52
100-41-4
2-Hexanone
ND
ug/L
50.0
0.46
1
08/19/18 16:52
591-78-6
lodomethane
ND
ug/L
10.0
0.32
1
08/19/18 16:52
74-88-4
Methylene Chloride
ND
ug/L
1.0
0.97
1
08/19/18 16:52
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
100
0.33
1
08/19/18 16:52
108-10-1
Styrene
ND
ug/L
1.0
0.26
1
08/19/18 16:52
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
5.0
0.33
1
08/19/18 16:52
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
3.0
0.40
1
08/19/18 16:52
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.46
1
08/19/18 16:52
127-18-4
Tetrahydrofuran
ND
ug/L
10.0
3.1
1
08/19/18 16:52
109-99-9
Toluene
ND
ug/L
1.0
0.26
1
08/19/18 16:52
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.48
1
08/19/18 16:52
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.29
1
08/19/18 16:52
79-00-5
Trichloroethene
ND
ug/L
1.0
0.47
1
08/19/18 16:52
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.20
1
08/19/18 16:52
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.41
1
08/19/18 16:52
96-18-4
Vinyl acetate
ND
ug/L
50.0
0.35
1
08/19/18 16:52
108-05-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2018 12:26 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 41

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD UNITS 1&2 BLANKS JOINT
Pace Project No.: 92396142
Sample: 3901- Trip Blank
Lab ID:
92396142005
Collected:
08/14/18 05:30
Received: 08/17/18 09:37 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL DF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level Landfill
Analytical
Method: EPA 8260E
Vinyl chloride
ND
ug/L
1.0
0.62 1
08/19/18 16:52
75-01-4
Xylene (Total)
ND
ug/L
5.0
0.66 1
08/19/18 16:52
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
93
%
70-130
1
08/19/18 16:52
460-00-4
1,2-Dichloroethane-d4 (S)
98
%
70-130
1
08/19/18 16:52
17060-07-0
Toluene-d8 (S)
101
%
70-130
1
08/19/18 16:52
2037-26-5
Date: 09/13/2018 12:26 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 41

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ANALYTICAL RESULTS
Project: OXFORD UNITS 1&2 BLANKS JOINT
Pace Project No.: 92396142
Sample: 3901- Field Blank Lab ID: 92396142006 Collected: 08/16/18 16:30 Received: 08/17/18 09:37 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
7470 Mercury
Mercury
8260 MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
Date: 09/13/2018 12:26 PM
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
ND
ug/L
6.0
3.9
1
08/25/18 07:40
08/25/18 22:56
7440-36-0
ND
ug/L
10.0
5.0
1
08/25/18 07:40
08/25/18 22:56
7440-38-2
ND
ug/L
100
2.5
1
08/25/18 07:40
08/25/18 22:56
7440-39-3
ND
ug/L
1.0
0.50
1
08/25/18 07:40
08/25/18 22:56
7440-41-7
ND
ug/L
1.0
0.50
1
08/25/18 07:40
08/25/18 22:56
7440-43-9
ND
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:56
7440-47-3
ND
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:56
7440-48-4
ND
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:56
7440-50-8
27.8J
ug/L
300
25.0
1
08/25/18 07:40
08/25/18 22:56
7439-89-6
ND
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:56
7439-92-1
ND
ug/L
50.0
2.5
1
08/25/18 07:40
08/25/18 22:56
7439-96-5
ND
ug/L
50.0
2.5
1
08/25/18 07:40
08/25/18 22:56
7440-02-0
ND
ug/L
10.0
5.0
1
08/25/18 07:40
08/25/18 22:56
7782-49-2
ND
ug/L
10.0
2.5
1
08/25/18 07:40
08/25/18 22:56
7440-22-4
ND
ug/L
25.0
2.5
1
08/25/18 07:40
08/25/18 22:56
7440-62-2
ND
ug/L
10.0
5.0
1
08/25/18 07:40
08/25/18 22:56
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
ND ug/L 5.5 0.020 1 08/18/18 06:19 08/29/18 17:30 7440-28-0
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
ND ug/L 0.20 0.10 1 08/20/1819:25 08/21/1813:28 7439-97-6
Analytical Method: EPA 8260E
ND
ug/L
100
ND
ug/L
200
ND
ug/L
1.0
ND
ug/L
3.0
ND
ug/L
1.0
ND
ug/L
3.0
ND
ug/L
10.0
ND
ug/L
100
ND
ug/L
100
ND
ug/L
1.0
ND
ug/L
3.0
ND
ug/L
10.0
ND
ug/L
5.0
ND
ug/L
1.0
ND
ug/L
13.0
ND
ug/L
3.0
ND
ug/L
1.0
ND
ug/L
10.0
ND
ug/L
5.0
ND
ug/L
1.0
ND
ug/L
100
ND
ug/L
5.0
10.0
1
08/19/18 17:08
67-64-1
1.9
1
08/19/18 17:08
107-13-1
0.25
1
08/19/18 17:08
71-43-2
0.17
1
08/19/18 17:08
74-97-5
0.18
1
08/19/18 17:08
75-27-4
0.26
1
08/19/18 17:08
75-25-2
0.29
1
08/19/18 17:08
74-83-9
0.96
1
08/19/18 17:08
78-93-3
1.2
1
08/19/18 17:08
75-15-0
0.25
1
08/19/18 17:08
56-23-5
0.23
1
08/19/18 17:08
108-90-7
0.54
1
08/19/18 17:08
75-00-3
0.14
1
08/19/18 17:08
67-66-3
0.11
1
08/19/18 17:08
74-87-3
2.0
1
08/19/18 17:08
96-12-8
0.21
1
08/19/18 17:08
124-48-1
0.27
1
08/19/18 17:08
106-93-4
0.21
1
08/19/18 17:08
74-95-3
0.30
1
08/19/18 17:08
95-50-1
0.33
1
08/19/18 17:08
106-46-7
1.0
1
08/19/18 17:08
110-57-6
0.32
1
08/19/18 17:08
75-34-3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 12 of 41

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ANALYTICAL RESULTS
Project: OXFORD UNITS 1&2 BLANKS JOINT
Pace Project No.: 92396142
Sample: 3901- Field Blank Lab ID: 92396142006 Collected: 08/16/18 16:30 Received: 08/17/18 09:37 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill Analytical Method: EPA 8260E
1,2-Dichloroethane
ND
ug/L
1.0
0.24
1
08/19/18 17:08
107-06-2
1,1-Dichloroethene
ND
ug/L
5.0
0.56
1
08/19/18 17:08
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
5.0
0.19
1
08/19/18 17:08
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
5.0
0.49
1
08/19/18 17:08
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.27
1
08/19/18 17:08
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.13
1
08/19/18 17:08
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.26
1
08/19/18 17:08
10061-02-6
Ethylbenzene
ND
ug/L
1.0
0.30
1
08/19/18 17:08
100-41-4
2-Hexanone
ND
ug/L
50.0
0.46
1
08/19/18 17:08
591-78-6
lodomethane
ND
ug/L
10.0
0.32
1
08/19/18 17:08
74-88-4
Methylene Chloride
ND
ug/L
1.0
0.97
1
08/19/18 17:08
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
100
0.33
1
08/19/18 17:08
108-10-1
Styrene
ND
ug/L
1.0
0.26
1
08/19/18 17:08
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
5.0
0.33
1
08/19/18 17:08
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
3.0
0.40
1
08/19/18 17:08
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.46
1
08/19/18 17:08
127-18-4
Tetrahydrofuran
ND
ug/L
10.0
3.1
1
08/19/18 17:08
109-99-9
Toluene
ND
ug/L
1.0
0.26
1
08/19/18 17:08
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.48
1
08/19/18 17:08
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.29
1
08/19/18 17:08
79-00-5
Trichloroethene
ND
ug/L
1.0
0.47
1
08/19/18 17:08
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.20
1
08/19/18 17:08
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.41
1
08/19/18 17:08
96-18-4
Vinyl acetate
ND
ug/L
50.0
0.35
1
08/19/18 17:08
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.62
1
08/19/18 17:08
75-01-4
Xylene (Total)
ND
ug/L
5.0
0.66
1
08/19/18 17:08
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
94
%
70-130
1
08/19/18 17:08
460-00-4
1,2-Dichloroethane-d4 (S)
97
%
70-130
1
08/19/18 17:08
17060-07-0
Toluene-d8 (S)
101
%
70-130
1
08/19/18 17:08
2037-26-5
8260 MSV SIM
Analytical
Method: EPA 8260E Mod.
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1.9
1
08/21/18 18:14
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
102
%
50-150
1
08/21/18 18:14
17060-07-0
Toluene-d8 (S)
114
%
50-150
1
08/21/18 18:14
2037-26-5
2320B Alkalinity
Analytical
Method: SM
2320B-2011
Alkalinity, Total as CaCO3
ND
ug/L
5000
1000
1
08/28/18 00:17
2540C Total Dissolved Solids
Analytical
Method: SM
2540C-2011
Total Dissolved Solids
ND
ug/L
25000
25000
1
08/19/18 12:21
300.0 IC anions 48hr
Analytical
Method: EPA 300.0 Rev 2.1
1993
Chloride
ND
ug/L
1000
500
1
08/18/18 00:15
16887-00-6
Sulfate
ND
mg/L
250
0.50
1
08/18/18 00:15
14808-79-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2018 12:26 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 41

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD UNITS 1&2 BLANKS JOINT
Pace Project No.: 92396142
QC Batch: 425829
Analysis Method: EPA 7470A
QC Batch Method: EPA 7470A
Analysis Description: 7470 Mercury
Associated Lab Samples: 92396142001, 92396142006
METHOD BLANK: 2354113
Matrix: Water
Associated Lab Samples: 92396142001, 92396142006
Blank Reporting
Parameter Units
Result Limit MDL
Analyzed
Qualifiers
Mercury ug/L
ND 0.20 0.10 08/21/1811:38
LABORATORY CONTROL SAMPLE: 2354114
Spike LCS LCS
% Rec
Parameter Units
Conc. Result % Rec
Limits Qualifiers
Mercury ug/L
2.5 2.4 98
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2354115 2354116
MS MSD
92395555001
Spike Spike MS MSD
MS MSD
% Rec Max
Parameter Units Result
Conc. Conc. Result Result
% Rec % Rec
Limits RPD RPD Qual
Mercury ug/L ND
2.5 2.5 2.4 2.4
96 96
75-125 1 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2018 12:26 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 41

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD UNITS 1&2 BLANKS JOINT
Pace Project No.: 92396142
QC Batch: 425491 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Associated Lab Samples: 92396142001, 92396142003
METHOD BLANK: 2352643
Associated Lab Samples: 92396142001, 92396142003
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
Antimony
ug/L
ND
6.0
3.9
08/21/18 22:05
Arsenic
ug/L
ND
10.0
5.0
08/21/18 22:05
Barium
ug/L
ND
100
2.5
08/21/18 22:05
Beryllium
ug/L
ND
1.0
0.50
08/21/18 22:05
Cadmium
ug/L
ND
1.0
0.50
08/21/18 22:05
Chromium
ug/L
ND
10.0
2.5
08/21/18 22:05
Cobalt
ug/L
ND
10.0
2.5
08/21/18 22:05
Copper
ug/L
ND
10.0
2.5
08/21/18 22:05
Iron
ug/L
ND
300
25.0
08/21/18 22:05
Lead
ug/L
ND
10.0
2.5
08/21/18 22:05
Manganese
ug/L
ND
50.0
2.5
08/21/18 22:05
Nickel
ug/L
ND
50.0
2.5
08/21/18 22:05
Selenium
ug/L
ND
10.0
5.0
08/21/18 22:05
Silver
ug/L
ND
10.0
2.5
08/21/18 22:05
Vanadium
ug/L
ND
25.0
2.5
08/21/18 22:05
Zinc
ug/L
ND
10.0
5.0
08/21/18 22:05
LABORATORY CONTROL SAMPLE:
2352644
Parameter
Units
Antimony
ug/L
Arsenic
ug/L
Barium
ug/L
Beryllium
ug/L
Cadmium
ug/L
Chromium
ug/L
Cobalt
ug/L
Copper
ug/L
Iron
ug/L
Lead
ug/L
Manganese
ug/L
Nickel
ug/L
Selenium
ug/L
Silver
ug/L
Vanadium
ug/L
Zinc
ug/L
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
500
487
97
80-120
500
464
93
80-120
500
483
97
80-120
500
479
96
80-120
500
458
92
80-120
500
476
95
80-120
500
466
93
80-120
500
496
99
80-120
5000
4880
98
80-120
500
464
93
80-120
500
474
95
80-120
500
480
96
80-120
500
455
91
80-120
250
246
99
80-120
500
482
96
80-120
500
452
90
80-120
Qualifiers
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 09/13/2018 12:26 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 41

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Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
OXFORD UNITS 1&2
92396142
BLANKS JOINT
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE: 2352645
2352646
MS
MSD
92396141001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Antimony
ug/L
ND
500
500
504
496
101
99
75-125
2
20
Arsenic
ug/L
ND
500
500
487
478
97
96
75-125
2
20
Barium
ug/L
ND
500
500
475
472
95
94
75-125
1
20
Beryllium
ug/L
ND
500
500
500
495
100
99
75-125
1
20
Cadmium
ug/L
ND
500
500
456
449
91
90
75-125
2
20
Chromium
ug/L
ND
500
500
472
465
94
93
75-125
1
20
Cobalt
ug/L
ND
500
500
453
447
91
89
75-125
1
20
Copper
ug/L
ND
500
500
502
492
100
98
75-125
2
20
Iron
ug/L
83.9J
5000
5000
4940
4900
97
96
75-125
1
20
Lead
ug/L
ND
500
500
457
450
91
90
75-125
2
20
Manganese
ug/L
9.81
500
500
482
474
94
93
75-125
2
20
Nickel
ug/L
ND
500
500
464
456
93
91
75-125
2
20
Selenium
ug/L
ND
500
500
503
493
100
98
75-125
2
20
Silver
ug/L
ND
250
250
251
246
100
99
75-125
2
20
Vanadium
ug/L
ND
500
500
494
487
98
97
75-125
1
20
Zinc
ug/L
ND
500
500
454
444
90
88
75-125
2
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2018 12:26 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 41

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD UNITS 1&2 BLANKS JOINT
Pace Project No.: 92396142
QC Batch: 427103 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Associated Lab Samples: 92396142006
METHOD BLANK: 2359969
Associated Lab Samples: 92396142006
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
Antimony
ug/L
ND
6.0
3.9
08/25/18 21:44
Arsenic
ug/L
ND
10.0
5.0
08/25/18 21:44
Barium
ug/L
ND
100
2.5
08/25/18 21:44
Beryllium
ug/L
ND
1.0
0.50
08/25/18 21:44
Cadmium
ug/L
ND
1.0
0.50
08/25/18 21:44
Chromium
ug/L
ND
10.0
2.5
08/25/18 21:44
Cobalt
ug/L
ND
10.0
2.5
08/25/18 21:44
Copper
ug/L
ND
10.0
2.5
08/25/18 21:44
Iron
ug/L
ND
300
25.0
08/25/18 21:44
Lead
ug/L
ND
10.0
2.5
08/25/18 21:44
Manganese
ug/L
ND
50.0
2.5
08/25/18 21:44
Nickel
ug/L
ND
50.0
2.5
08/25/18 21:44
Selenium
ug/L
ND
10.0
5.0
08/25/18 21:44
Silver
ug/L
ND
10.0
2.5
08/25/18 21:44
Vanadium
ug/L
ND
25.0
2.5
08/25/18 21:44
Zinc
ug/L
ND
10.0
5.0
08/25/18 21:44
LABORATORY CONTROL SAMPLE:
2359970
Parameter
Units
Antimony
ug/L
Arsenic
ug/L
Barium
ug/L
Beryllium
ug/L
Cadmium
ug/L
Chromium
ug/L
Cobalt
ug/L
Copper
ug/L
Iron
ug/L
Lead
ug/L
Manganese
ug/L
Nickel
ug/L
Selenium
ug/L
Silver
ug/L
Vanadium
ug/L
Zinc
ug/L
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
500
453
91
80-120
500
438
88
80-120
500
473
95
80-120
500
464
93
80-120
500
452
90
80-120
500
462
92
80-120
500
449
90
80-120
500
469
94
80-120
5000
4630
93
80-120
500
444
89
80-120
500
449
90
80-120
500
450
90
80-120
500
435
87
80-120
250
232
93
80-120
500
458
92
80-120
500
439
88
80-120
Qualifiers
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2018 12:26 PM without the written consent of Pace Analytical Services, LLC.
Page 17 of 41

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
OXFORD UNITS 1&2
92396142
BLANKS JOINT
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE: 2359971
2359972
MS
MSD
92396257001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Antimony
ug/L
ND
500
500
467
460
93
92
75-125
1
20
Arsenic
ug/L
ND
500
500
462
455
92
91
75-125
1
20
Barium
ug/L
40.3J
500
500
526
517
97
95
75-125
2
20
Beryllium
ug/L
ND
500
500
479
474
96
95
75-125
1
20
Cadmium
ug/L
ND
500
500
471
466
94
93
75-125
1
20
Chromium
ug/L
ND
500
500
476
470
95
94
75-125
1
20
Cobalt
ug/L
ND
500
500
456
451
91
90
75-125
1
20
Copper
ug/L
24.7
500
500
508
500
97
95
75-125
2
20
Iron
ug/L
410
5000
5000
5320
5230
98
96
75-125
2
20
Lead
ug/L
ND
500
500
453
448
91
89
75-125
1
20
Manganese
ug/L
270
500
500
746
734
95
93
75-125
2
20
Nickel
ug/L
ND
500
500
458
454
92
91
75-125
1
20
Selenium
ug/L
ND
500
500
461
458
92
92
75-125
1
20
Silver
ug/L
ND
250
250
242
238
97
95
75-125
2
20
Vanadium
ug/L
ND
500
500
475
470
95
94
75-125
1
20
Zinc
ug/L
ND
500
500
457
454
91
90
75-125
1
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2018 12:26 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 41

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD UNITS 1&2 BLANKS JOINT
Pace Project No.: 92396142
QC Batch: 425510
Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A
Analysis Description: 6020 MET
Associated Lab Samples: 92396142001, 92396142003
METHOD BLANK: 2352702
Matrix: Water
Associated Lab Samples: 92396142001, 92396142003
Blank Reporting
Parameter Units
Result Limit MDL
Analyzed
Qualifiers
Thallium ug/L
ND 5.5 0.020
08/23/18 22:09
LABORATORY CONTROL SAMPLE: 2352703
Spike LCS LCS
% Rec
Parameter Units
Conc. Result % Rec
Limits Qualifiers
Thallium ug/L
10 10.1 101
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2352704 2352705
MS MSD
92396141001
Spike Spike MS MSD
MS MSD
% Rec Max
Parameter Units Result
Conc. Conc. Result Result
% Rec % Rec
Limits RPD RPD Qual
Thallium ug/L ND
10 10 10.3 10.3
103 103
75-125 1 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2018 12:26 PM without the written consent of Pace Analytical Services, LLC.
Page 19 of 41

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD UNITS 1&2 BLANKS JOINT
Pace Project No.: 92396142
QC Batch: 425734
Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A
Analysis Description: 6020 MET
Associated Lab Samples: 92396142006
METHOD BLANK: 2353880
Matrix: Water
Associated Lab Samples: 92396142006
Blank Reporting
Parameter Units
Result Limit MDL
Analyzed
Qualifiers
Thallium ug/L
ND 5.5 0.020
08/29/1816:42
LABORATORY CONTROL SAMPLE: 2353881
Spike LCS LCS
% Rec
Parameter Units
Conc. Result % Rec
Limits Qualifiers
Thallium ug/L
10 9.9 99
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2353882 2353883
MS MSD
92396257001
Spike Spike MS MSD
MS MSD
% Rec Max
Parameter Units Result
Conc. Conc. Result Result
% Rec % Rec
Limits RPD RPD Qual
Thallium ug/L ND
10 10 10.9 10
109 100
75-125 9 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2018 12:26 PM without the written consent of Pace Analytical Services, LLC.
Page 20 of 41

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD UNITS 1&2 BLANKS JOINT
Pace Project No.: 92396142
QC Batch: 425801 Analysis Method: EPA 8260B
QC Batch Method: EPA 8260E Analysis Description: 8260 MSV Low Level Landfill
Associated Lab Samples: 92396142001, 92396142003, 92396142005, 92396142006
METHOD BLANK: 2354038 Matrix: Water
Associated Lab Samples: 92396142001, 92396142003, 92396142005, 92396142006
Blank Reporting
Parameter Units Result Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
5.0
0.33
08/19/18 12:01
1,1,1-Trichloroethane
ug/L
ND
1.0
0.48
08/19/18 12:01
1,1,2,2-Tetrachloroethane
ug/L
ND
3.0
0.40
08/19/18 12:01
1,1,2-Trichloroethane
ug/L
ND
1.0
0.29
08/19/18 12:01
1,1-Dichloroethane
ug/L
ND
5.0
0.32
08/19/18 12:01
1,1-Dichloroethene
ug/L
ND
5.0
0.56
08/19/18 12:01
1,2,3-Trichloropropane
ug/L
ND
1.0
0.41
08/19/18 12:01
1,2-Dibromo-3-chloropropane
ug/L
ND
13.0
2.0
08/19/18 12:01
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.27
08/19/18 12:01
1,2-Dichlorobenzene
ug/L
ND
5.0
0.30
08/19/18 12:01
1,2-Dichloroethane
ug/L
ND
1.0
0.24
08/19/18 12:01
1,2-Dichloropropane
ug/L
ND
1.0
0.27
08/19/18 12:01
1,4-Dichlorobenzene
ug/L
ND
1.0
0.33
08/19/18 12:01
2-Butanone (MEK)
ug/L
ND
100
0.96
08/19/18 12:01
2-Hexanone
ug/L
ND
50.0
0.46
08/19/18 12:01
4-Methyl-2-pentanone (MIBK)
ug/L
ND
100
0.33
08/19/18 12:01
Acetone
ug/L
ND
100
10.0
08/19/18 12:01
Acrylonitrile
ug/L
ND
200
1.9
08/19/18 12:01
Benzene
ug/L
ND
1.0
0.25
08/19/18 12:01
Bromochloromethane
ug/L
ND
3.0
0.17
08/19/18 12:01
Bromodichloromethane
ug/L
ND
1.0
0.18
08/19/18 12:01
Bromoform
ug/L
ND
3.0
0.26
08/19/18 12:01
Bromomethane
ug/L
ND
10.0
0.29
08/19/18 12:01
Carbon disulfide
ug/L
ND
100
1.2
08/19/18 12:01
Carbon tetrachloride
ug/L
ND
1.0
0.25
08/19/18 12:01
Chlorobenzene
ug/L
ND
3.0
0.23
08/19/18 12:01
Chloroethane
ug/L
ND
10.0
0.54
08/19/18 12:01
Chloroform
ug/L
ND
5.0
0.14
08/19/18 12:01
Chloromethane
ug/L
ND
1.0
0.11
08/19/18 12:01
cis-1,2-Dichloroethene
ug/L
ND
5.0
0.19
08/19/18 12:01
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.13
08/19/18 12:01
Dibromochloromethane
ug/L
ND
3.0
0.21
08/19/18 12:01
Dibromomethane
ug/L
ND
10.0
0.21
08/19/18 12:01
Ethylbenzene
ug/L
ND
1.0
0.30
08/19/18 12:01
lodomethane
ug/L
ND
10.0
0.32
08/19/18 12:01
Methylene Chloride
ug/L
ND
1.0
0.97
08/19/18 12:01
Styrene
ug/L
ND
1.0
0.26
08/19/18 12:01
Tetrachloroethene
ug/L
ND
1.0
0.46
08/19/18 12:01
Tetrahydrofuran
ug/L
ND
10.0
3.1
08/19/18 12:01
Toluene
ug/L
ND
1.0
0.26
08/19/18 12:01
trans-1,2-Dichloroethene
ug/L
ND
5.0
0.49
08/19/18 12:01
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2018 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 41

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD UNITS 1&2 BLANKS JOINT
Pace Project No.: 92396142
METHOD BLANK: 2354038 Matrix: Water
Associated Lab Samples: 92396142001, 92396142003, 92396142005, 92396142006
Blank Reporting
Parameter Units Result Limit
MDL
Analyzed
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.26
08/19/18 12:01
trans-1,4-Dichloro-2-butene
ug/L
ND
100
1.0
08/19/18 12:01
Trichloroethene
ug/L
ND
1.0
0.47
08/19/18 12:01
Trichlorofluoromethane
ug/L
ND
1.0
0.20
08/19/18 12:01
Vinyl acetate
ug/L
ND
50.0
0.35
08/19/18 12:01
Vinyl chloride
ug/L
ND
1.0
0.62
08/19/18 12:01
Xylene (Total)
ug/L
ND
5.0
0.66
08/19/18 12:01
1,2-Dichloroethane-d4 (S)
%
98
70-130
08/19/18 12:01
4-Bromofluorobenzene (S)
%
96
70-130
08/19/18 12:01
Toluene-d8 (S)
%
100
70-130
08/19/18 12:01
LABORATORY CONTROL SAMPLE:
Parameter
2354039
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
51.6
103
80-125
1,1,1-Trichloroethane
ug/L
50
51.1
102
71-129
1,1,2,2-Tetrachloroethane
ug/L
50
49.3
99
79-124
1,1,2-Trichloroethane
ug/L
50
50.4
101
85-125
1,1-Dichloroethane
ug/L
50
46.8
94
73-126
1,1-Dichloroethene
ug/L
50
52.2
104
66-135
1,2,3-Trichloropropane
ug/L
50
48.5
97
75-130
1,2-Dibromo-3-chloropropane
ug/L
50
51.2
102
71-133
1,2-Dibromoethane (EDB)
ug/L
50
53.0
106
83-124
1,2-Dichlorobenzene
ug/L
50
49.2
98
80-133
1,2-Dichloroethane
ug/L
50
50.1
100
67-128
1,2-Dichloropropane
ug/L
50
50.1
100
75-132
1,4-Dichlorobenzene
ug/L
50
47.7
95
78-130
2-Butanone (MEK)
ug/L
100
96.2J
96
61-144
2-Hexanone
ug/L
100
100
100
68-143
4-Methyl-2-pentanone (MIBK)
ug/L
100
98AJ
98
72-135
Acetone
ug/L
100
112
112
48-146
Acrylonitrile
ug/L
250
248
99
40-160
Benzene
ug/L
50
49.1
98
80-125
Bromochloromethane
ug/L
50
52.0
104
71-125
Bromodichloromethane
ug/L
50
53.3
107
78-124
Bromoform
ug/L
50
51.1
102
71-128
Bromomethane
ug/L
50
37.9
76
40-160
Carbon disulfide
ug/L
50
51.3J
103
50-160
Carbon tetrachloride
ug/L
50
52.9
106
69-131
Chlorobenzene
ug/L
50
49.4
99
81-122
Chloroethane
ug/L
50
43.1
86
39-148
Chloroform
ug/L
50
51.7
103
73-127
Chloromethane
ug/L
50
44.4
89
44-146
cis-1,2-Dichloroethene
ug/L
50
49.2
98
74-124
Qualifiers
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2018 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 41

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD UNITS 1&2 BLANKS JOINT
Pace Project No.: 92396142
LABORATORY CONTROL SAMPLE:
2354039
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
cis-1,3-Dichloropropene
ug/L
50
50.2
100
72-132
Dibromochloromethane
ug/L
50
51.3
103
78-125
Dibromomethane
ug/L
50
54.0
108
82-120
Ethylbenzene
ug/L
50
48.9
98
79-121
lodomethane
ug/L
100
98.6
99
39-154
Methylene Chloride
ug/L
50
51.6
103
64-133
Styrene
ug/L
50
49.4
99
84-126
Tetrachloroethene
ug/L
50
48.4
97
78-122
Tetrahydrofuran
ug/L
500
477
95
69-148
Toluene
ug/L
50
47.9
96
80-121
trans-1,2-Dichloroethene
ug/L
50
50.8
102
71-127
trans- 1,3-Dichloropropene
ug/L
50
50.8
102
69-141
trans-1,4-Dichloro-2-butene
ug/L
50
52.6J
105
40-160
Trichloroethene
ug/L
50
52.8
106
78-122
Trichlorofluoromethane
ug/L
50
51.2
102
53-137
Vinyl acetate
ug/L
100
98.1
98
40-160
Vinyl chloride
ug/L
50
51.5
103
58-137
Xylene (Total)
ug/L
150
149
99
81-126
1,2-Dichloroethane-d4 (S)
%
100
70-130
4-Bromofluorobenzene (S)
%
97
70-130
Toluene-d8 (S)
%
97
70-130
MATRIX SPIKE SAMPLE:
2354041
92395744002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
20
19.3
96
70-130
1,1,1-Trichloroethane
ug/L
ND
20
20.7
103
70-130
1,1,2,2-Tetrachloroethane
ug/L
ND
20
18.9
94
70-130
1,1,2-Trichloroethane
ug/L
ND
20
19.4
97
70-130
1,1-Dichloroethane
ug/L
ND
20
19.3
97
70-130
1,1-Dichloroethene
ug/L
ND
20
21.8
109
70-166
1,2,3-Trichloropropane
ug/L
ND
20
18.8
94
70-130
1,2-Dibromo-3-chloropropane
ug/L
ND
20
18.0
90
70-130
1,2-Dibromoethane (EDB)
ug/L
ND
20
20.0
100
70-130
1,2-Dichlorobenzene
ug/L
1.2J
20
20.7
97
70-130
1,2-Dichloroethane
ug/L
ND
20
19.9
99
70-130
1,2-Dichloropropane
ug/L
ND
20
19.5
98
70-130
1,4-Dichlorobenzene
ug/L
1.9
20
20.2
92
70-130
2-Butanone (MEK)
ug/L
ND
40
39.OJ
97
70-130
2-Hexanone
ug/L
ND
40
37.2J
93
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
37.9J
95
70-130
Acetone
ug/L
ND
40
53.5J
134
70-130 M1
Acrylonitrile
ug/L
ND
100
97.3J
97
70-130
Benzene
ug/L
1.3
20
21.2
100
70-148
Bromochloromethane
ug/L
ND
20
20.5
103
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2018 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 41

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD UNITS 1&2 BLANKS JOINT
Pace Project No.: 92396142
MATRIX SPIKE SAMPLE:
2354041
92395744002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Bromodichloromethane
ug/L
ND
20
20.1
101
70-130
Bromoform
ug/L
ND
20
18.1
90
70-130
Bromomethane
ug/L
ND
20
9.6J
48
70-130 M1
Carbon disulfide
ug/L
ND
20
20.OJ
100
70-130
Carbon tetrachloride
ug/L
ND
20
20.6
103
70-130
Chlorobenzene
ug/L
14.5
20
33.9
97
70-146
Chloroethane
ug/L
1.2J
20
19.4
91
70-130
Chloroform
ug/L
ND
20
20.0
100
70-130
Chloromethane
ug/L
ND
20
17.7
89
70-130
cis-1,2-Dichloroethene
ug/L
ND
20
19.9
100
70-130
cis-1,3-Dichloropropene
ug/L
ND
20
18.6
93
70-130
Dibromochloromethane
ug/L
ND
20
19.0
95
70-130
Dibromomethane
ug/L
ND
20
21.3
107
70-130
Ethylbenzene
ug/L
ND
20
19.3
97
70-130
lodomethane
ug/L
ND
40
36.3
91
70-130
Methylene Chloride
ug/L
ND
20
19.9
100
70-130
Styrene
ug/L
ND
20
18.8
94
70-130
Tetrachloroethene
ug/L
ND
20
19.5
97
70-130
Tetrahydrofuran
ug/L
12.1
200
198
93
70-130
Toluene
ug/L
ND
20
19.2
96
70-155
trans-1,2-Dichloroethene
ug/L
ND
20
20.7
103
70-130
trans- 1,3-Dichloropropene
ug/L
ND
20
18.9
94
70-130
trans-1,4-Dichloro-2-butene
ug/L
ND
20
15.OJ
75
70-130
Trichloroethene
ug/L
ND
20
21.0
105
69-151
Trichlorofluoromethane
ug/L
ND
20
22.4
112
70-130
Vinyl acetate
ug/L
ND
40
35.9J
90
70-130
Vinyl chloride
ug/L
ND
20
21.2
106
70-130
Xylene (Total)
ug/L
ND
60
58.3
97
70-130
1,2-Dichloroethane-d4 (S)
%
100
70-130
4-Bromofluorobenzene (S)
%
97
70-130
Toluene-d8 (S)
%
96
70-130
SAMPLE DUPLICATE: 2354040
Parameter
Units
92395744001
Result
Dup
Result RPD
Max
RPD Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,1-Trichloroethane
ug/L
ND
ND
30
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,2-Trichloroethane
ug/L
ND
ND
30
1,1-Dichloroethane
ug/L
ND
ND
30
1,1-Dichloroethene
ug/L
ND
ND
30
1,2,3-Trichloropropane
ug/L
ND
ND
30
1,2-Dibromo-3-chloropropane
ug/L
ND
ND
30
1,2-Dibromoethane (EDB)
ug/L
ND
ND
30
1,2-Dichlorobenzene
ug/L
ND
ND
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2018 12:26 PM without the written consent of Pace Analytical Services, LLC.
Page 24 of 41

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD UNITS 1&2 BLANKS JOINT
Pace Project No.: 92396142
SAMPLE DUPLICATE: 2354040
Parameter
Units
92395744001
Result
Dup
Result
1,2-Dichloroethane
ug/L
ND
ND
1,2-Dichloropropane
ug/L
ND
ND
1,4-Dichlorobenzene
ug/L
ND
ND
2-Butanone (MEK)
ug/L
ND
ND
2-Hexanone
ug/L
ND
ND
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
Acetone
ug/L
ND
ND
Acrylonitrile
ug/L
ND
ND
Benzene
ug/L
ND
ND
Bromochloromethane
ug/L
ND
ND
Bromodichloromethane
ug/L
ND
ND
Bromoform
ug/L
ND
ND
Bromomethane
ug/L
ND
ND
Carbon disulfide
ug/L
ND
ND
Carbon tetrachloride
ug/L
ND
ND
Chlorobenzene
ug/L
ND
ND
Chloroethane
ug/L
ND
ND
Chloroform
ug/L
ND
ND
Chloromethane
ug/L
ND
ND
cis-1,2-Dichloroethene
ug/L
ND
ND
cis-1,3-Dichloropropene
ug/L
ND
ND
Dibromochloromethane
ug/L
ND
ND
Dibromomethane
ug/L
ND
ND
Ethylbenzene
ug/L
ND
ND
lodomethane
ug/L
ND
ND
Methylene Chloride
ug/L
ND
ND
Styrene
ug/L
ND
ND
Tetrachloroethene
ug/L
ND
ND
Tetrahydrofuran
ug/L
ND
ND
Toluene
ug/L
ND
ND
trans-1,2-Dichloroethene
ug/L
ND
ND
trans- 1,3-Dichloropropene
ug/L
ND
ND
trans-1,4-Dichloro-2-butene
ug/L
ND
ND
Trichloroethene
ug/L
ND
ND
Trichlorofluoromethane
ug/L
ND
ND
Vinyl acetate
ug/L
ND
ND
Vinyl chloride
ug/L
ND
ND
Xylene (Total)
ug/L
ND
ND
1,2-Dichloroethane-d4 (S)
%
98
102
4-Bromofluorobenzene (S)
%
97
95
Toluene-d8 (S)
%
98
99
Max
RPD RPD Qualifiers
3
2
0
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2018 12:26 PM without the written consent of Pace Analytical Services, LLC.
Page 25 of 41

Pace Analytical Services, LLC
ceAnalX cal ® 9800 Kiney Ave. Suite 100
Huntersville, NC 28078078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: OXFORD UNITS 1&2 BLANKS JOINT
Pace Project No.: 92396142
QC Batch: 426080 Analysis Method: EPA 8260B Mod.
QC Batch Method: EPA 8260E Mod. Analysis Description: 8260 MSV SIM
Associated Lab Samples: 92396142003, 92396142006
METHOD BLANK: 2355220
Matrix:
Water
Associated Lab Samples:
92396142003, 92396142006
Blank
Reporting
Parameter
Units
Result
Limit
MDL Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
1.9 08/21/18 15:18
1,2-Dichloroethane-d4 (S)
%
97
50-150
08/21/18 15:18
Toluene-d8 (S)
%
107
50-150
08/21/18 15:18
LABORATORY CONTROL SAMPLE: 2355221
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 17.7 88 71-125
1,2-Dichloroethane-d4 (S) % 97 50-150
Toluene-d8(S) % 107 50-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2355222
2355223
MS
MSD
92395199068 Spike
Spike MS
MSD MS
MSD
% Rec
Max
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits
RPD RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 18.5
17.9 91
88
50-150
3 30
1,2-Dichloroethane-d4 (S)
%
105
104
50-150
30
Toluene-d8 (S)
%
114
113
50-150
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2018 12:26 PM without the written consent of Pace Analytical Services, LLC.
Page 26 of 41

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD UNITS 1&2 BLANKS JOINT
Pace Project No.: 92396142
QC Batch: 426318 Analysis Method: EPA 8260B Mod.
QC Batch Method: EPA 8260E Mod. Analysis Description: 8260 MSV SIM
Associated Lab Samples: 92396142001
METHOD BLANK: 2356318
Associated Lab Samples: 92396142001
Parameter
Units
1,4-Dioxane (p-Dioxane)
ug/L
1,2-Dichloroethane-d4 (S)
%
Toluene-d8 (S)
%
Matrix: Water
Blank Reporting
Result Limit
ND 2.0
95 50-150
114 50-150
MDL Analyzed
1.9 08/23/18 14:49
08/23/18 14:49
08/23/18 14:49
Qualifiers
LABORATORY CONTROL SAMPLE: 2356319
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 16.6 83 71-125
1,2-Dichloroethane-d4 (S) % 95 50-150
Toluene-d8(S) % 113 50-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2356320
2356321
MS
MSD
92396277008 Spike
Spike MS
MSD MS
MSD
% Rec
Max
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits
RPD RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 16.4
16.4 79
79
50-150
0 30
1,2-Dichloroethane-d4 (S)
%
99
98
50-150
30
Toluene-d8 (S)
%
114
115
50-150
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2018 12:26 PM without the written consent of Pace Analytical Services, LLC.
Page 27 of 41

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD UNITS 1&2 BLANKS JOINT
Pace Project No.: 92396142
QC Batch: 426910
Analysis Method: SM 2320B-2011
QC Batch Method: SM 2320B-2011
Analysis Description: 2320E Alkalinity
Associated Lab Samples: 92396142001
METHOD BLANK: 2358896
Matrix: Water
Associated Lab Samples: 92396142001
Blank Reporting
Parameter Units
Result Limit MDL Analyzed
Qualifiers
Alkalinity, Total as CaCO3 ug/L
ND 5000 1000 08/24/18 19:05
LABORATORY CONTROL SAMPLE: 2358897
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Alkalinity, Total as CaCO3 ug/L
50000 50000 100 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2358898 2358899
MS MSD
92396797013
Spike Spike MS MSD MS MSD
% Rec Max
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD RPD Qual
Alkalinity, Total as CaCO3 ug/L 88.0 mg/L
50000 50000 136000 136000 96 96
80-120 0 25
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2358900 2358901
MS MSD
92396834004 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Alkalinity, Total as CaCO3 ug/L 12.7 mg/L 50000 50000 61800 64600 98 104 80-120 4 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2018 12:26 PM without the written consent of Pace Analytical Services, LLC.
Page 28 of 41

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD UNITS 1&2 BLANKS JOINT
Pace Project No.: 92396142
QC Batch: 427280
Analysis Method: SM 2320B-2011
QC Batch Method: SM 2320B-2011
Analysis Description: 2320E Alkalinity
Associated Lab Samples: 92396142006
METHOD BLANK: 2360642
Matrix: Water
Associated Lab Samples: 92396142006
Blank Reporting
Parameter Units
Result Limit MDL Analyzed
Qualifiers
Alkalinity, Total as CaCO3 ug/L
ND 5000 1000 08/27/18 22:09
LABORATORY CONTROL SAMPLE: 2360643
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Alkalinity, Total as CaCO3 ug/L
50000 50200 100 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2360644 2360645
MS MSD
92397010023
Spike Spike MS MSD MS MSD
% Rec Max
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD RPD Qual
Alkalinity, Total as CaCO3 ug/L 29.9 mg/L
50000 50000 78800 78900 98 98
80-120 0 25
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2360659 2360660
MS MSD
92396725004 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Alkalinity, Total as CaCO3 ug/L 46.0 mg/L 50000 50000 96500 95400 101 99 80-120 1 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2018 12:26 PM without the written consent of Pace Analytical Services, LLC.
Page 29 of 41

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD UNITS 1&2 BLANKS JOINT
Pace Project No.: 92396142
QC Batch: 425684
Analysis Method: SM 2540C-2011
QC Batch Method: SM 2540C-2011
Analysis Description:
2540C Total Dissolved Solids
Associated Lab Samples: 92396142001
METHOD BLANK: 2353674
Matrix:
Water
Associated Lab Samples: 92396142001
Blank
Reporting
Parameter
Units
Result
Limit MDL
Analyzed Qualifiers
Total Dissolved Solids
ug/L
ND
25000 25000
08/17/18 16:50
LABORATORY CONTROL SAMPLE: 2353675
Spike
LCS LCS
% Rec
Parameter
Units
Conc.
Result % Rec
Limits Qualifiers
Total Dissolved Solids
ug/L
251000
250000 100
90-110
SAMPLE DUPLICATE: 2353676
92395975002
Dup
Max
Parameter
Units
Result
Result RPD
RPD Qualifiers
Total Dissolved Solids
ug/L
890 mg/L
892000 0
5
SAMPLE DUPLICATE: 2353677
92395975012
Dup
Max
Parameter
Units
Result
Result RPD
RPD Qualifiers
Total Dissolved Solids
ug/L
162 mg/L
168000 4
5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 09/13/2018 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 41

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD UNITS 1&2 BLANKS JOINT
Pace Project No.: 92396142
QC Batch: 425804
Analysis Method: SM 2540C-2011
QC Batch Method: SM 2540C-2011
Analysis Description:
2540C Total Dissolved Solids
Associated Lab Samples: 92396142006
METHOD BLANK: 2354053
Matrix:
Water
Associated Lab Samples: 92396142006
Blank
Reporting
Parameter
Units
Result
Limit MDL
Analyzed Qualifiers
Total Dissolved Solids
ug/L
ND
25000 25000
08/19/18 12:18
LABORATORY CONTROL SAMPLE: 2354054
Spike
LCS LCS
% Rec
Parameter
Units
Conc.
Result % Rec
Limits Qualifiers
Total Dissolved Solids
ug/L
250000
262000 105
90-110
SAMPLE DUPLICATE: 2354055
92396221001
Dup
Max
Parameter
Units
Result
Result RPD
RPD Qualifiers
Total Dissolved Solids
ug/L
ND
ND
5
SAMPLE DUPLICATE: 2354056
92396251003
Dup
Max
Parameter
Units
Result
Result RPD
RPD Qualifiers
Total Dissolved Solids
ug/L
504 mg/L
504000 0
5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 09/13/2018 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 41

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD UNITS 1&2 BLANKS JOINT
Pace Project No.: 92396142
QC Batch: 426573 Analysis Method: EPA 300.0 Rev 2.1 1993
QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions
Associated Lab Samples: 92396142001
METHOD BLANK: 2357505 Matrix: Water
Associated Lab Samples: 92396142001
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Chloride ug/L ND 1000 500 08/24/18 01:34
Sulfate ug/L ND 250000 500 08/24/18 01:34
LABORATORY CONTROL SAMPLE: 2357506
Spike
LCS
LCS % Rec
Parameter Units
Conc.
Result
% Rec Limits Qualifiers
Chloride ug/L
50000
51800
104 90-110
Sulfate ug/L
50000
49000J
98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2357507
2357508
MS
MSD
92396726011
Spike
Spike
MS
MSD MS
MSD
% Rec
Max
Parameter Units
Result
Conc.
Conc.
Result
Result % Rec
% Rec
Limits
RPD RPD Qual
Chloride ug/L
4.5 mg/L
50000
50000
61100
60100 113
111
90-110
2 10 M1
Sulfate ug/L
2.9 mg/L
50000
50000
56700J
55800J 108
106
90-110
2 10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2357509
2357510
MS
MSD
92396726021
Spike
Spike
MS
MSD MS
MSD
% Rec
Max
Parameter Units
Result
Conc.
Conc.
Result
Result % Rec
% Rec
Limits
RPD RPD Qual
Chloride ug/L
4.9 mg/L
50000
50000
59300
60200 109
110
90-110
1 10
Sulfate ug/L
3.4 mg/L
50000
50000
54700J
56000J 103
105
90-110
2 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2018 12:26 PM without the written consent of Pace Analytical Services, LLC.
Page 32 of 41

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD UNITS 1&2 BLANKS JOINT
Pace Project No.: 92396142
QC Batch: 425712 Analysis Method: EPA 300.0 Rev 2.1 1993
QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions
Associated Lab Samples: 92396142006
METHOD BLANK: 2353804 Matrix: Water
Associated Lab Samples: 92396142006
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Chloride ug/L ND 1000 500 08/17/18 22:44
Sulfate mg/L ND 250 0.50 08/17/18 22:44
LABORATORY CONTROL SAMPLE: 2353805
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chloride ug/L 50000 50200 100 90-110
Sulfate mg/L 50 51.6J 103 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2353806
2353807
MS
MSD
92396275001 Spike
Spike
MS
MSD MS
MSD % Rec
Max
Parameter Units
Result Conc.
Conc.
Result
Result % Rec
% Rec Limits
RPD RPD Qual
Chloride ug/L
50600 50000
50000
96200
94200 91
87 90-110
2 10 M1
Sulfate mg/L
4AJ 50
50
56.3J
56.1J 104
104 90-110
0 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 09/13/2018 12:26 PM without the written consent of Pace Analytical Services, LLC.
Page 33 of 41

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: OXFORD UNITS 1&2 BLANKS JOINT
Pace Project No.: 92396142
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
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Date: 09/13/2018 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 41

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
OXFORD UNITS 1&2 BLANKS JOINT
92396142
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92396142001
3901-MW-7
EPA 3010A
425491
EPA 6010D
425539
92396142003
3901-NES-2S
EPA 3010A
425491
EPA6010D
425539
92396142006
3901- Field Blank
EPA 3010A
427103
EPA 6010D
427125
92396142001
3901-MW-7
EPA 3010A
425510
EPA 6020B
425544
92396142003
3901-NES-2S
EPA 3010A
425510
EPA 6020B
425544
92396142006
3901- Field Blank
EPA 3010A
425734
EPA 6020B
425756
92396142001
3901-MW-7
EPA 7470A
425829
EPA 7470A
426024
92396142006
3901- Field Blank
EPA 7470A
425829
EPA 7470A
426024
92396142001
3901-MW-7
EPA 8260B
425801
92396142003
3901-NES-2S
EPA 8260B
425801
92396142005
3901- Trip Blank
EPA 8260B
425801
92396142006
3901- Field Blank
EPA 8260B
425801
92396142001
3901-MW-7
EPA 8260B Mod.
426318
92396142003
3901-NES-2S
EPA 8260B Mod.
426080
92396142006
3901- Field Blank
EPA 8260B Mod.
426080
92396142001
3901-MW-7
SM 2320B-2011
426910
92396142006
3901-Field Blank
SM 2320B-2011
427280
92396142001
3901-MW-7
SM 2540C-2011
425684
92396142006
3901- Field Blank
SM 2540C-2011
425804
92396142001
3901-MW-7
EPA 300.0 Rev 2.1 1993
426573
92396142006
3901- Field Blank
EPA 300.0 Rev 2.1 1993
425712
Date: 09/13/2018 12:26 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 35 of 41

Document Name:
Document Revised: February 7, 2018
9
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issu€ng Authority:
aC2A,�alyfiCal
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples: /
Asheville ❑ Eden❑ Greenwood ❑ Huntersville K] " Raleigh[] Mechanicsville❑
' ; Client Name:
L
Project #;
Courier: ❑Fed Ex t []UPS OUSPS ❑Client
❑ Commercial ce ❑Other:
Custody Seal Present? ❑Yes ETNK, Seals Intact? Oyes 31O
WOit : 92396142
1111111111111111111111
1142
Date/initials Person Examining Contents..
Packing Material: ❑Bubble Wrap Hfulble Bags ❑None ❑ Other Biological Tissue Fr en?
Thermomete Dyes ❑No /A
ER Gun Ib;
92TO43 Type of Ice: Ovet ❑Blue ❑None
Cooler Temp ('C): —S ` Correction Factor: Add/Subtract (°C) _0.2
Temp should be above freezing to 6'C
Cooler Temp Corrected (°C): ❑<amples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Soil ( /MIA, water sample) -
Did samples originate in a quarantine zone within the United States: CA, NY, or 5C (check maps)? Did samples originate from a foreign source (internat ally,
Dyes o in,i uiinv Hawaii and P,,Prrn Ritn17 I—lYat FZ11Cn
Comments/Discrepancy:
Chain of Custody Present?
Yes
❑ryo
❑N/A
1.
Samples Arrived within Hold Time?
Yes
❑,
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
❑Yes
[No
L3 Na/
❑N/A
3,
Rush Turn Around Time Requested?
❑yes
090--
❑N/A
4.
Sufficient Volume?
�es
❑No
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
es
OKI'
[--]No
[]No
❑N/A
❑N/A
6.
Containers Intact?
4f Yes
[-]No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
❑No
N/A
a.
Sample Labels Match COC?
-Includes Date/TimeAD/Analysis Matrix:
3<s
I�
❑No
❑N/A
9.
Headspace in VOA Vials (>5-6mm)?
❑Yes
ONo
❑N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
afes
2 es
❑No
[]No
[]NIA
❑N/A
11.
COMMENTS/SAMPLE DISCREPANCY Field Data Required? ❑Yes ❑No
Lu n Gl i'7I�UA' i .�i ,11(C002 an� fi/ (VI ►c
� -
/
T7 RI�i}� �i�i�� t' ��i� co-J. 11 �(01^C Lb �t►l� illF'} ., `JU
,d,C-4)IV)
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: d tC. Datenme:
Project Manager SCURF Review: , Date: OR1,6} /
Project Manager SRF Review: _ Date: !� V
Page 36 of 41

Document Name:
Document Revised: February 7, 2018
a
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
acmnalytical
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples,
Exceptions: VOA, Cotiform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
Project It WO# » 2396142
li'i'I: NMG Due Date: 08/30/18
CLIENT: 92•-Joyce Eng
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot if
Note: whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (Le.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 37 of 41

1
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Page 38 of 41

Document Name:
Document Revised: February 7, 2018
Sample Condition Upon Receipt(SCUR)
Page I of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
ora orVreceivmampes:_
Asheville ❑ Eden[] Greenwood ❑ Huntersvill Raleigh[] Mechanicsville❑
SampleClient Name:
Upon Receipt
Project #:
Courier: LJFeJ Ex ❑UPS ❑LISPS []Client
❑ Commercial QWce ❑Other:
Custody Seal Present? ❑Yes Uo Seals Intact? ❑Peso
Packing Material: gpubble Wrap
Thermotnav;
1-J IR Gun ID: 92TO43
/Bubble Bags ❑None ❑ Other
W®# 92396142
PSI: NMG Due Date: 08/30/18
CLIENT: 92—Joyce Eng
Date/Initials Person Examining Contents:
Type of Ice: Wet ❑Blue ❑Mane
Cooler Temp ('C): Correction Factor: Add/Subtract ('C) -0.2
Cooler Temp Corrected ('C): S'
USDA Regulated Soil ([fl/A, water sample)
Did samples originate in a quarantine zone within the United States; CA, NY, or SC (check maps)?
❑Yes ❑No
Biological Tissue Fr zen?
[]Yes❑No Tissue
Temp should be above freezing to 6°C
❑samples cut of temp criteria. Samples on Ice, cooling process
hasbegun
Did samples originate from a foreign source (internationally,
includingHawail and Puerto Rico)? ❑Yes ❑No
Comments/Discrepancy:
Chain of Custody Present?
i,' yes
❑tio
[I N/A
1.
Samples Arrived w thin Hold Time?
es
[]No
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
❑Yes o
❑N/A
3.
Rush Turn Around Time Requested?
[]Yes
o
❑N/A
4.
Sufficient Volume?
Yes
❑Na
❑N/A
5.
Correct Containers Used?
Pace Containers Used?
i
Yes
❑No
❑No
❑N/A
❑N/A
6.
Containerslntact?
b,dYes
ON
[I N/A
7.
Dissolved analysis: Samples R, ..;erect?
9.
Sample Labels Match COC? rr es ❑No ❑NIA
-includes Date/Time/ID/Analysis Matrix:
Headspace in VOA Vials (>S-6mm)?
LEIYes
❑No
[]N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
Y s
tdves
❑No
❑No
[]N/A
❑N/A
11.
COMMENTS/SAMPLE DISCREPANCY
Field Data Required? ❑Yes [:]No
i l i Y; Ift'v— 09JU l Fik f l fio 0 i1 U1i64 q �z. ChS 'i' r
CA ltn d va. 0' it
Lot ID ofmlit containers:
CLIENT NOTIFICATION/RESOLUTION
h
Person contacted; Qk Date/Time: � 1 i n� b �a " w
Project Manager SCURF Review: j� +
Project Manager SRF Review:
Date: II Tf LJ
Date: rill �(7
Page 39 of 41

Document Name:
Document Revised: February 7, 2018
Sample Condition Upon Receipt(SCUR)
Page I of 2
Document No.:
Issuing Authority:
aeeAnalyWal'
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples,
Exceptions: VOA, Wiform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottarn half of box is to list number of bottle
Project Wo# . 9G396142
pM: NMG� Due Date; 08/30/18
CLIENT: 92—Joyce Emg
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot 4
Note: wnenever tnere is a discrepancy affecting North Carolina compliance samples, a copy at tnis term will he sent to the +larth Carolina oEHNR Certification Office (i.e.
Out of ho{d, incorrect preservative, out of temp, incorrect containers.
Page 40 of 41

j
1
HAIN-OF-CUSTODY /2%nalytical Request Document
!
The
Chain -of -Custody is a LEGAL DC!, -UMENT. All relevant fields must be completed accurately.
Section A
Section B
Section C
Required Client Information:
Required Project Information:
Invoice Information: Page : 1 Of 1
Attention: Jason Falls
Company Name: Granville County, Solid Waste
Company: Joyce Engineering
Report To: Van Burbach
Address: 2211 West Meadowview Rd
Copy To: Miguel Vazquez
Greensboro, NC 27407
Address: P.O. Box 906, Oxford NC 27565
Regulatory Agency
Email To: vburbach (a)loyceengineerim, Cbm
Purchase Order No.
Phone: [phone] Fax:
Client Project ID: Oxford Unit 1 MNA (f
ll list)
State! Location
Requested Due Date/TAT: 10 Day {DI=faUll}
i
Container Order Number:
North Carolina
Requested
Analysis
Filtered
(Y/N)
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SAMPLE CONDITIONS
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IN,

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
August 31, 2018
Mr. Van Burbach
Joyce Engineering -NC
2211 West Meadowview Rd
Boone Bldg, Suite 101
Greensboro, NC 27407
RE: Project: Oxford Unit 1 MNA (full list)
Pace Project No.: 92396107
Dear Mr. Burbach:
Enclosed are the analytical results for sample(s) received by the laboratory on August 16, 2018. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
��i Flo _ _.1I , .�:
Nicole Gasiorowski
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Daniel Girdner, LaBella Associates, D.P.C.
Miguel Vazquez, Joyce Engineering
Rochelle mesubed, Joyce Engineering
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 16

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Oxford Unit 1 MNA (full list)
Pace Project No.: 92396107
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 16

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: Oxford Unit 1 MNA (full list)
Pace Project No.: 92396107
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92396107001
92396107002
3901-MW7
3901-NES2S
Water
Water
08/15/1810:51
08/15/1814:16
08/16/1812:36
08/16/1810:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 16

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Oxford Unit 1 MNA (full list)
92396107
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92396107001
3901-MW7
RSK 175 Modified
CL
1
PASI-C
EPA 8260E
CAH
4
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 300.0 Rev 2.1 1993
KDF1
3
PASI-A
92396107002
3901-NES2S
RSK 175 Modified
CL
1
PASI-C
EPA 8260E
CAH
4
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 300.0 Rev 2.1 1993
KDF1
3
PASI-A
REPORT OF LABORATORY ANALYSIS
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SUMMARY OF DETECTION
Project: Oxford Unit 1 MNA (full list)
Pace Project No.: 92396107
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed Qualifiers
92396107001
3901-MW7
SM 2320B-2011
Alkalinity, Total as CaCO3
123000
ug/L
5000
08/24/18 20:27
EPA 300.0 Rev 2.1 1993
Chloride
9620
ug/L
1000
08/17/18 15:38
EPA 300.0 Rev 2.1 1993
Nitrate as N
198
ug/L
100
08/17/18 15:38 H1
EPA 300.0 Rev 2.1 1993
Sulfate
55.2J
mg/L
250
08/17/18 15:38
92396107002
3901-NES2S
RSK 175 Modified
Methane
57.6
ug/L
10.0
08/17/18 14:06
SM 2320B-2011
Alkalinity, Total as CaCO3
58300
ug/L
5000
08/24/18 20:42
EPA 300.0 Rev 2.1 1993
Chloride
7190
ug/L
1000
08/17/18 14:06
EPA 300.0 Rev 2.1 1993
Sulfate
7.3J
mg/L
250
08/17/18 14:06 M 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 5 of 16

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ANALYTICAL RESULTS
Project: Oxford Unit 1 MNA (full list)
Pace Project No.: 92396107
Sample: 3901-MW7
Lab ID: 92396107001 Collected:
08/15/18 10:51
Received: 08/16/18 12:36 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
RSK 175 Headspace
Analytical Method: RSK 175 Modified
Methane
ND ug/L 10.0
10.0
1
08/17/1814:21
74-82-8
8260 MSV Low Level Landfill
Analytical Method: EPA 8260E
Vinyl chloride
ND ug/L 1.0
0.62
1
08/19/18 14:42
75-01-4
Surrogates
4-Bromofluorobenzene (S)
97 % 70-130
1
08/19/18 14:42
460-00-4
1,2-Dichloroethane-d4 (S)
99 % 70-130
1
08/19/18 14:42
17060-07-0
Toluene-d8 (S)
98 % 70-130
1
08/19/18 14:42
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Alkalinity, Total as CaCO3
123000 ug/L 5000
1000
1
08/24/18 20:27
300.0 IC anions 48hr
Analytical Method: EPA 300.0 Rev 2.1
1993
Chloride
9620 ug/L 1000
500
1
08/17/1815:38
16887-00-6
Nitrate as N
198 ug/L 100
50.0
1
08/17/18 15:38
14797-55-8 H1
Sulfate
55.2J mg/L 250
0.50
1
08/17/1815:38
14808-79-8
Date: 08/31 /2018 09:30 AM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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ANALYTICAL RESULTS
Project: Oxford Unit 1 MNA (full list)
Pace Project No.: 92396107
Sample: 3901-NES2S
Lab ID: 92396107002 Collected:
08/15/18 14:16
Received: 08/16/18 10:00 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
RSK 175 Headspace
Analytical Method: RSK 175 Modified
Methane
57.6 ug/L 10.0
10.0
1
08/17/1814:06
74-82-8
8260 MSV Low Level Landfill
Analytical Method: EPA 8260E
Vinyl chloride
ND ug/L 1.0
0.62
1
08/19/18 14:59
75-01-4
Surrogates
4-Bromofluorobenzene (S)
97 % 70-130
1
08/19/18 14:59
460-00-4
1,2-Dichloroethane-d4 (S)
101 % 70-130
1
08/19/18 14:59
17060-07-0
Toluene-d8 (S)
100 % 70-130
1
08/19/18 14:59
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Alkalinity, Total as CaCO3
58300 ug/L 5000
1000
1
08/24/18 20:42
300.0 IC anions 48hr
Analytical Method: EPA 300.0 Rev 2.1
1993
Chloride
7190 ug/L 1000
500
1
08/17/1814:06
16887-00-6
Nitrate as N
ND ug/L 100
50.0
1
08/17/18 14:06
14797-55-8
Sulfate
7.3J mg/L 250
0.50
1
08/17/1814:06
14808-79-8 M1
Date: 08/31 /2018 09:30 AM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
QUALITY CONTROL DATA
Project: Oxford Unit 1 MNA (full list)
Pace Project No.: 92396107
QC Batch: 425562
Analysis Method: RSK 175 Modified
QC Batch Method: RSK 175 Modified
Analysis Description: RSK
175 HEADSPACE
Associated Lab Samples: 92396107001, 92396107002
METHOD BLANK: 2352828
Matrix: Water
Associated Lab Samples: 92396107001, 92396107002
Blank Reporting
Parameter Units
Result Limit
MDL
Analyzed
Qualifiers
Methane ug/L
ND 10.0
10.0
08/17/1812:04
LABORATORY CONTROL SAMPLE: 2352829
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec
Limits Qualifiers
Methane ug/L
396 424
107
70-130
MATRIX SPIKE SAMPLE: 2352831
92395967006 Spike
MS
MS
% Rec
Parameter Units
Result Conc.
Result
% Rec
Limits Qualifiers
Methane ug/L
31.4 396
499
118
70-130
SAMPLE DUPLICATE: 2352830
92395967001 Dup
Max
Parameter Units
Result Result
RPD
RPD
Qualifiers
Methane ug/L
ND ND
20
SAMPLE DUPLICATE: 2352832
92396053004 Dup
Max
Parameter Units
Result Result
RPD
RPD
Qualifiers
Methane ug/L
1010 964
4
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/31 /2018 09:30 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 16

aceAnalytical
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Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Oxford Unit 1 MNA (full list)
Pace Project No.: 92396107
QC Batch: 425801 Analysis Method: EPA 8260B
QC Batch Method: EPA 8260E Analysis Description: 8260 MSV Low Level Landfill
Associated Lab Samples: 92396107001, 92396107002
METHOD BLANK: 2354038
Matrix:
Water
Associated Lab Samples:
92396107001, 92396107002
Blank
Reporting
Parameter
Units
Result
Limit
MDL Analyzed Qualifiers
Vinyl chloride
ug/L
ND
1.0
0.62 08/19/18 12:01
1,2-Dichloroethane-d4 (S)
%
98
70-130
08/19/18 12:01
4-Bromofluorobenzene (S)
%
96
70-130
08/19/18 12:01
Toluene-d8 (S)
%
100
70-130
08/19/18 12:01
LABORATORY CONTROL SAMPLE:
2354039
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits Qualifiers
Vinyl chloride
ug/L
50 51.5
103
58-137
1,2-Dichloroethane-d4 (S)
%
100
70-130
4-Bromofluorobenzene (S)
%
97
70-130
Toluene-d8 (S)
%
97
70-130
MATRIX SPIKE SAMPLE:
2354041
92395744002 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Vinyl chloride
ug/L
ND 20
21.2
106
70-130
1,2-Dichloroethane-d4 (S)
%
100
70-130
4-Bromofluorobenzene (S)
%
97
70-130
Toluene-d8 (S)
%
96
70-130
SAMPLE DUPLICATE: 2354040
92395744001 Dup
Max
Parameter
Units
Result Result
RPD
RPD
Qualifiers
Vinyl chloride
ug/L
ND ND
30
1,2-Dichloroethane-d4 (S)
%
98 102
3
4-Bromofluorobenzene (S)
%
97 95
2
Toluene-d8 (S)
%
98 99
0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Oxford Unit 1 MNA (full list)
Pace Project No.: 92396107
QC Batch: 426910
Analysis Method: SM 2320B-2011
QC Batch Method: SM 2320B-2011
Analysis Description: 2320E Alkalinity
Associated Lab Samples: 92396107001, 92396107002
METHOD BLANK: 2358896
Matrix: Water
Associated Lab Samples: 92396107001, 92396107002
Blank Reporting
Parameter Units
Result Limit MDL Analyzed
Qualifiers
Alkalinity, Total as CaCO3 ug/L
ND 5000 1000 08/24/18 19:05
LABORATORY CONTROL SAMPLE: 2358897
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Alkalinity, Total as CaCO3 ug/L
50000 50000 100 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2358898 2358899
MS MSD
92396797013
Spike Spike MS MSD MS MSD
% Rec Max
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD RPD Qual
Alkalinity, Total as CaCO3 ug/L 88.0 mg/L
50000 50000 136000 136000 96 96
80-120 0 25
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2358900 2358901
MS MSD
92396834004 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Alkalinity, Total as CaCO3 ug/L 12.7 mg/L 50000 50000 61800 64600 98 104 80-120 4 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/31 /2018 09:30 AM without the written consent of Pace Analytical Services, LLC.
Page 10 of 16

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Oxford Unit 1 MNA (full list)
Pace Project No.: 92396107
QC Batch: 425599 Analysis Method: EPA 300.0 Rev 2.1 1993
QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions
Associated Lab Samples: 92396107001, 92396107002
METHOD BLANK: 2352977
Matrix:
Water
Associated Lab Samples:
92396107001, 92396107002
Blank
Reporting
Parameter
Units
Result
Limit
MDL Analyzed Qualifiers
Chloride
ug/L
ND
1000
500 08/17/1815:01
Nitrate as N
ug/L
ND
100
50.0 08/17/18 15:01
Sulfate
mg/L
ND
250
0.50 08/17/1815:01
LABORATORY CONTROL SAMPLE:
2352978
Spike
LCS LCS
% Rec
Parameter
Units
Conc.
Result % Rec
Limits Qualifiers
Chloride
ug/L
50000
50600 101
90-110
Nitrate as N
ug/L
2500
2440 98
90-110
Sulfate
mg/L
50
52.OJ 104
90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2352979
2352980
MS
MSD
92396107002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD RPD Qual
Chloride ug/L
7190
50000
50000
59900
61000
105
108
90-110
2 10 H1
Nitrate as N ug/L
ND
2500
2500
2550
2610
101
104
90-110
2 10 H1
Sulfate mg/L
7.3J
50
50
61.5J
62.7J
108
111
90-110
2 10 H1,M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/31 /2018 09:30 AM without the written consent of Pace Analytical Services, LLC.
Page 11 of 16

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[phone]
QUALIFIERS
Project: Oxford Unit 1 MNA (full list)
Pace Project No.: 92396107
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H1 Analysis conducted outside the EPA method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
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Date: 08/31 /2018 09:30 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 16

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[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Oxford Unit 1 MNA (full list)
Pace Project No.: 92396107
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
92396107001
3901-MW7
RSK 175 Modified
425562
92396107002
3901-NES2S
RSK 175 Modified
425562
92396107001
3901-MW7
EPA 8260B
425801
92396107002
3901-NES2S
EPA 8260B
425801
92396107001
3901-MW7
SM 2320B-2011
426910
92396107002
3901-NES2S
SM 2320B-2011
426910
92396107001
3901-MW7
EPA 300.0 Rev 2.1 1993
425599
92396107002
3901-NES2S
EPA 300.0 Rev 2.1 1993
425599
Date: 08/31 /2018 09:30 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Batch
Page 13 of 16

Document Name:
Document Revised: February 7, 2018
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
aceAnalF�tlCc��a
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville Raleigh❑ Mechanicsville❑
SampleCondition Client Name:
Upon Receipt Project #:
Courier: ❑Fed Ex I ❑UPS Musps ❑Client
❑ Commercial Qp-ace ❑Other:
Custody Seal Present? ❑Yes fo Seals Intact? ❑Yes to
WO#:92396107
92396107
IIIIII II I II III I I III III
Date/Wtials Person Examining Contents:. ► V `f c r lJ
Packing Material: ❑Bubble Wrap ubble Bags ❑None ❑ Other Biological Tissue F zen?
Thermometer Dyes [-]No1/A
IR Gun ID: 9�T�43 Type of Ice: Jet ❑Blue ❑None
Cooler Temp (°C): Correction Factor- Add/Subtract (°C) _0.2
Temp should be above freezing to 6°C
Cooler Temp Corrected (°C): 5, F.., ❑Samples out of temp criteria. Samples on ice, cooling process
hasbegun
USDA Regulated Soil (' N/A, water sample)
Did samples oflPatein a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internati ly,
nYes No includiae Hawaii and Puerto Rico)? F1Yes
Comments/Discrepancy:
Chain of Custody Present?
oy<
❑No
El NIA
1.
Samples Arrived within Hold Time?
[.}?res
❑No
❑NJA
2.
Short Hold Time Analysis (<72 hr.)?
❑Yes
(Jlo
❑N/A
3.
Rush Turn Around Time Requested?
[]Yes
EK.
❑N/A
4.
Sufficient Volume?
byes
❑No
❑N/A
S.
Correct Containers Used?
I�
[]No❑N/A
6.
-Pace Containers Used?
es
ON.
❑N/A
Containers Intact?
es
[]No
❑N/A
7.
Dissolved analysis: Samples Field Filtered? ❑Yes
❑No
/A
8.
Sample Labels Match C00
es
[:]No
❑N/A
9.
-Includes Date/Time/ID/Analysis
•-r^
Matrix: 1%i
Headspace in VOA Vials (>5-6mm)?
[]Yes
No
❑N/A
10.
Trip Blank Present?
❑Yes
o
❑N/A
11.
Trip Blank Custody Seals Present?
❑Yes
lO
❑N/A
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Date/Time:
Field Data Required? []Yes ❑No
Lot ID of split containers:
Date: --
Date: Zf
Page 14 of 16

Document Name:
a Sample Condition Upon Recell
aceARalytleal Document No.:
F-CAR-CS-033-Rev.06
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
Document Revised: February 7, 2018
t(SCUR) Page 1 of 2
Issuing Authority:
Pace Carolinas Quality Office
Project # WO# : 92J96107
PM: NMG Due Date:: 08/30/18
CLIENT: 92—Joyce Eng
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-•-i�'
�s'
\N\\
N\-\
I
6
8
9
16
it
12
pH Adjustment Log for Preserved Samples
Sample ID
Type of preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot #
�� r ... �:.., ncuni0 rerrlFireNnn
r)fflra li a
Note: Whenever there is a mscrepancy aaecung Norm Ldrouna cvnipridii�<
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 15 of 16

CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
1L
Section A Section B Section C
Required Client Information: Required Project Information: Invoice Information: 1--Page: 1 Of 1
Company: Joyce Engineering Report To: Van Burbach Attention: Jason Falls
Address: 2211 West Meadowview Rd Copy To- Miguel Vazquez Company Name: Granville County, Solid Waste
Greensboro, NC 27407
Address: P.O. Box 906, Oxford NC 27565
Regulatory Agency
Email To: vburbach(aDioviceen iejneeri0_q.com
Purchase Order No.
Phone: [phone] Fax
Client Project ID: Oxford Unit 1 MNA (full list)
Pace PM: Nicole Gasiorow<
State I Location
Requested Due Dale[TAT; 10 Dav (Default)
Container Order Number:
Profile: 3566-1
North Carolina
Requested
Analysis
Filtered
(YIN)
a
Z
°
o
COLLECTED
Presetvatives
>
MATRIX CODE
=
O
Drmhin0 WaIef DW
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F.
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In
U
W.M, Water WW
9
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ID Saivs.hd SL
to
START
END
F
=
One Character per box. DIiI Ot
a
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(A-Z, 0-9 !, -j Air AR
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w
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Sample Ids must be unique Othcr OT
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DATE
TIME
DATE
TIME
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=
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=
z
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3901-MW7
wr
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X
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6
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9
10
11
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ADDITIONAL COMMENTS
RELINQUISHED BY I AFFILIATION
DATE
TIME
ACCEPTED BY I AFFILIATION
TIME
SAMPLE CONDITIONS
COCs= Vinyl Chloride
C �u'
iL
( d2=
( S,
t
SAMPLER (NAME AND SIGNATURE
-
a
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PRINT Name of SAMPLER:
2
@ z
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SIGNATURE of SAMPLER:
DATE Signed:

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
August 29, 2018
Mr. Van Burbach
Joyce Engineering -NC
2211 West Meadowview Rd
Boone Bldg, Suite 101
Greensboro, NC 27407
RE: Project: Oxford Unit 1 MNA (full list)
Pace Project No.: 92396275
Dear Mr. Burbach:
Enclosed are the analytical results for sample(s) received by the laboratory on August 17, 2018. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
��i Flo _ _.1I , .�:
Nicole Gasiorowski
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Daniel Girdner, LaBella Associates, D.P.C.
Miguel Vazquez, Joyce Engineering
Rochelle mesubed, Joyce Engineering
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 15

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Oxford Unit 1 MNA (full list)
Pace Project No.: 92396275
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 15

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Oxford Unit 1 MNA (full list)
Pace Project No.: 92396275
Lab ID Sample ID
SAMPLE SUMMARY
Matrix Date Collected Date Received
92396275001 3901-MW5R Water 08/16/18 08:10 08/17/18 09:37
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 15

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Oxford Unit 1 MNA (full list)
92396275
Analytes
Lab lD
Sample ID
Method
Analysts
Reported
Laboratory
92396275001
3901-MW5R
RSK 175 Modified
CL
1
PASI-C
EPA 8260E
CAH
4
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 300.0 Rev 2.1 1993
KDF1
3
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 15

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SUMMARY OF DETECTION
Project: Oxford Unit 1 MNA (full list)
Pace Project No.: 92396275
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed Qualifiers
92396275001
3901-MW5R
RSK 175 Modified
Methane
94.5
ug/L
10.0
08/22/18 13:36
EPA 8260B
Vinyl chloride
3.5
ug/L
1.0
08/28/18 20:47
SM 2320B-2011
Alkalinity, Total as CaCO3
186000
ug/L
5000
08/28/18 00:00
EPA 300.0 Rev 2.1 1993
Chloride
50600
ug/L
1000
08/17/18 23:20 M1
EPA 300.0 Rev 2.1 1993
Sulfate
4AJ
mg/L
250
08/17/18 23:20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 15

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Oxford Unit 1 MNA (full list)
Pace Project No.: 92396275
Sample: 3901-MW5R
Lab ID: 92396275001 Collected:
08/16/18 08:10
Received: 08/17/18 09:37 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
RSK 175 Headspace
Analytical Method: RSK 175 Modified
Methane
94.5 ug/L 10.0
10.0
1
08/22/1813:36
74-82-8
8260 MSV Low Level Landfill
Analytical Method: EPA 8260E
Vinyl chloride
3.5 ug/L 1.0
0.62
1
08/28/18 20:47
75-01-4
Surrogates
4-Bromofluorobenzene (S)
93 % 70-130
1
08/28/18 20:47
460-00-4
1,2-Dichloroethane-d4 (S)
100 % 70-130
1
08/28/18 20:47
17060-07-0
Toluene-d8 (S)
95 % 70-130
1
08/28/18 20:47
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Alkalinity, Total as CaCO3
186000 ug/L 5000
1000
1
08/28/18 00:00
300.0 IC anions 48hr
Analytical Method: EPA 300.0 Rev 2.1
1993
Chloride
50600 ug/L 1000
500
1
08/17/18 23:20
16887-00-6 M1
Nitrate as N
ND ug/L 100
50.0
1
08/17/18 23:20
14797-55-8
Sulfate
4AJ mg/L 250
0.50
1
08/17/18 23:20
14808-79-8
Date: 08/29/2018 05:04 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 15

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Oxford Unit 1 MNA (full list)
Pace Project No.: 92396275
QC Batch: 426332
Analysis Method: RSK 175 Modified
QC Batch Method: RSK 175 Modified
Analysis Description: RSK
175 HEADSPACE
Associated Lab Samples: 92396275001
METHOD BLANK: 2356396
Matrix: Water
Associated Lab Samples: 92396275001
Blank Reporting
Parameter
Units
Result Limit
MDL
Analyzed
Qualifiers
Methane
ug/L
ND 10.0
10.0
08/22/1813:05
LABORATORY CONTROL SAMPLE: 2356397
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec
Limits Qualifiers
Methane
ug/L
396 352
89
70-130
MATRIX SPIKE SAMPLE: 2356562
92396430013 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Methane
ug/L
19.6 396
387
93
70-130
SAMPLE DUPLICATE: 2356398
92396430001 Dup
Max
Parameter
Units
Result Result
RPD
RPD
Qualifiers
Methane
ug/L
36.5 33.3
9
20
SAMPLE DUPLICATE: 2356399
92396430011 Dup
Max
Parameter
Units
Result Result
RPD
RPD
Qualifiers
Methane
ug/L
22.8 22.0
4
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/29/2018 05:04 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 15

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Oxford Unit 1 MNA (full list)
Pace Project No.: 92396275
QC Batch: 427539 Analysis Method: EPA 8260B
QC Batch Method: EPA 8260E Analysis Description: 8260 MSV Low Level Landfill
Associated Lab Samples: 92396275001
METHOD BLANK: 2361841
Matrix:
Water
Associated Lab Samples: 92396275001
Blank
Reporting
Parameter
Units
Result
Limit
MDL Analyzed Qualifiers
Vinyl chloride
ug/L
ND
1.0
0.62 08/28/18 15:24
1,2-Dichloroethane-d4 (S)
%
98
70-130
08/28/18 15:24
4-Bromofluorobenzene (S)
%
96
70-130
08/28/18 15:24
Toluene-d8 (S)
%
99
70-130
08/28/18 15:24
LABORATORY CONTROL SAMPLE:
2361842
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits Qualifiers
Vinyl chloride
ug/L
50 56.7
113
58-137
1,2-Dichloroethane-d4 (S)
%
99
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene-d8 (S)
%
96
70-130
MATRIX SPIKE SAMPLE:
2361843
92396257003 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Vinyl chloride
ug/L
ND 20
24.4
122
70-130
1,2-Dichloroethane-d4 (S)
%
101
70-130
4-Bromofluorobenzene (S)
%
97
70-130
Toluene-d8 (S)
%
97
70-130
SAMPLE DUPLICATE: 2361844
92396257004 Dup
Max
Parameter
Units
Result Result
RPD
RPD
Qualifiers
Vinyl chloride
ug/L
ND ND
30
1,2-Dichloroethane-d4 (S)
%
103 102
0
4-Bromofluorobenzene (S)
%
95 93
2
Toluene-d8 (S)
%
99 99
0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/29/2018 05:04 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 15

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Oxford Unit 1 MNA (full list)
Pace Project No.: 92396275
QC Batch: 427280
Analysis Method: SM 2320B-2011
QC Batch Method: SM 2320B-2011
Analysis Description: 2320E Alkalinity
Associated Lab Samples: 92396275001
METHOD BLANK: 2360642
Matrix: Water
Associated Lab Samples: 92396275001
Blank Reporting
Parameter Units
Result Limit MDL Analyzed
Qualifiers
Alkalinity, Total as CaCO3 ug/L
ND 5000 1000 08/27/18 22:09
LABORATORY CONTROL SAMPLE: 2360643
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Alkalinity, Total as CaCO3 ug/L
50000 50200 100 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2360644 2360645
MS MSD
92397010023
Spike Spike MS MSD MS MSD
% Rec Max
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD RPD Qual
Alkalinity, Total as CaCO3 ug/L 29.9 mg/L
50000 50000 78800 78900 98 98
80-120 0 25
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2360659 2360660
MS MSD
92396725004 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Alkalinity, Total as CaCO3 ug/L 46.0 mg/L 50000 50000 96500 95400 101 99 80-120 1 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/29/2018 05:04 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 15

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Oxford Unit 1 MNA (full list)
Pace Project No.: 92396275
QC Batch: 425712 Analysis Method: EPA 300.0 Rev 2.1 1993
QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions
Associated Lab Samples: 92396275001
METHOD BLANK: 2353804
Matrix:
Water
Associated Lab Samples: 92396275001
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
Chloride
ug/L
ND
1000
500 08/17/18 22:44
Nitrate as N
ug/L
ND
100
50.0 08/17/18 22:44
Sulfate
mg/L
ND
250
0.50 08/17/18 22:44
LABORATORY CONTROL SAMPLE:
2353805
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Chloride
ug/L
50000
50200
100
90-110
Nitrate as N
ug/L
2500
2430
97
90-110
Sulfate
mg/L
50
51.6J
103
90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2353806
2353807
MS
MSD
92396275001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD RPD Qual
Chloride ug/L
50600
50000
50000
96200
94200
91
87
90-110
2 10 M1
Nitrate as N ug/L
ND
2500
2500
2430
2420
97
96
90-110
0 10
Sulfate mg/L
4AJ
50
50
56.3J
56.1J
104
104
90-110
0 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/29/2018 05:04 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 15

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: Oxford Unit 1 MNA (full list)
Pace Project No.: 92396275
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/29/2018 05:04 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 15

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Oxford Unit 1 MNA (full list)
Pace Project No.: 92396275
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
92396275001
3901-MW5R
RSK 175 Modified
426332
92396275001
3901-MW5R
EPA 8260B
427539
92396275001
3901-MW5R
SM 2320B-2011
427280
92396275001
3901-MW5R
EPA 300.0 Rev 2.1 1993
425712
Date: 08/29/2018 05:04 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Batch
Page 12 of 15

Document Name:
Document Revised: February 7, 2018
9
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
_ 3CBAafL�
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
_l:a -ora ory-receiving sasamp�----- -- -
Asheville ❑ Eden[:] Greenwood ❑ Huntersvilleq� Raleigh[:] Mechanicsville[]
• , Client Nam
on eReceiptl Project #,, WO# : 92396275
Courier: ❑Fe Ex []UPS❑[]Client
Client
❑ Commercial gwce ❑Other: I II1 11 I!k !
92396275
Custody Seal Present? ❑Yes to Seals Intact? Dyes
Date/fniEials Person Examining Contents;
Packing Material: Pubble Wrap Bubble Bags ❑None ❑ Other
Thermomet r Type of Ice: Wet ❑Blue
VIR sun ID: 92TO43
Cooler Temp (°C): S , q Correction Factor: Add/Subtract ('C) _0.2
Cooler Temp Corrected (°C): �i
USDA Regulated Sail (Ei/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)?
r-IYes nNo
Biological Tissue Fr Zen?
[]Yes❑No A
❑f4oe
Temp<.hould be above freezing to 6°C
❑Samples out cf temp criteria. Samples on ice, cooling process
basbegun
Did samples originate from a foreign source (internationally,
inclu61ng Hawaii and Puerto €ilco)? ❑Yes []No
Comments/Discrepancy:
Chain of Custody Present?
i]Yes
[:]No
❑N/A
1.
Samples Arrived within Hold Time?
es
❑Na
El N/A
2.
Short Hold Time Analysis (<72 hr.)?
❑Yes
qNo
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
CK,
❑N/A
4.
Sufficient Volume?
Yes
❑Na
El N/A
S.
Correct Containers Used?
❑Na
[I N/A
6.
-Pace Containers Used?
Yes
❑No
❑N/A
Containers Intact?
L�s
❑No
❑N/A
7.
Dissolved anaiysis: Samples field Filtered? ❑Yes
❑No
/A
a.
Sample Labels Match CCC?
es
❑Na
❑N/A
9.
rr
lti I
-Includes Date/time/ID/Analysis
Matrix:
Headspace in VOA Vials (>5-6mm)?
J Yes
❑No
[I N/A
10.
Trip Blank Present?
Y
❑No
❑N/A
11.
Trip B1ankCustody Seals Present?
Yes
❑No
I[] NIA
COMMENTS/SAMPLE DISCREPANCY Field Data Required? ❑Yes [:]No
013AI� —,VIP oblul • F1'.l M I ir'} i} \40 'Za 1 -'er
Lot ID of split containers:
CLIENT NOTiFICATION/RESOLUTION
Person contacted: Q-fo �.1 l V L -Y S'i Datenme: 1 ��
Project Manager SCURF Review: Date:
Project Manager SRF Review: Date: 81Z 16
i
Page 13 of 15

Document Name:
Document Revised: February 7, 2018
a
Sample Condition Upon Receipt(SOUR)
Page 1 of 2
Document No.:
Issuing Authority:
aceArtaf�tiea!
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is Project # Wl►#� �iy
verified and within the acceptance range for preservation---�1,�/'�t_._.. 923 9 6 2 7 5
samples. PM: NMG Due Date: 08/31/18
Exceptions: VOA, Conform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg GI_ TENT : 92-J.yce Eng
**Bottom half of box is to list number of bottle
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Note: Wheneverthere is a discrepancy affecting North Carolina Compliance samples, a copy or tnis rorm win ne sent to the norm L-arouna ueniln 4ei ui �euun �= t •_•
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 14 of 15

CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
IL
Section A Section B Section C
Required Client Information: Required Project Information: Invoice Information: Page : 1 Of i
Company: Joyce Engineering Report To: Van Burbach Attention: Jason Falls
Address: 2211 West Meadowview Rd Copy To: Miguel Vazquez Company Name- Granville County, Solid Waste
Greensboro, NC 27407
Address: P.O. Box 906, Oxford NC 27565
Regulatory Agency
Email To: vburbach(d'jo ceencineerin�.corn
Purchase Order No.
Phone: [phone] JFnx
Client Project ID: OxfOTd Unit 1 MNA (full list)
State/Location
Requested Due DatelTAT: 10 Day (Default)
Container Order Number:
North Carolina
Requested
Analysis
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SAMPLER NAME AND SIGNATURE
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En

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
August 27, 2018
Mr. Van Burbach
Joyce Engineering -NC
2211 West Meadowview Rd
Boone Bldg, Suite 101
Greensboro, NC 27407
RE: Project: Oxford Diss. Hydrogen
Pace Project No.: 92396288
Dear Mr. Burbach:
Enclosed are the analytical results for sample(s) received by the laboratory on August 17, 2018. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Gasiorowski
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Daniel Girdner, LaBella Associates, D.P.C.
Miguel Vazquez, Joyce Engineering
Rochelle mesubed, Joyce Engineering
�pQ ACrfFO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
9e0 without the written consent of Pace Analytical Services, LLC.
Page 1 of 16

aceAnalytical
—pacelabsxom
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: Oxford Diss. Hydrogen
Pace Project No.: 92396288
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92396288001
3901-MW7
Water
08/15/18 12:15
08/17/18 09:37
92396288002
3901-MW5R
Water
08/16/18 09:36
08/17/18 09:37
92396288003
3901-NES2S
Water
08/15/18 15:58
08/17/18 09:37
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 2 of 16

Document Name:
Document Revised: February 7, 2018
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
aCr?f(13i1L`3�
F-CAR-CS-033•Rev.06
Pace Carolinas Quality Office
_TtailioraVory recei`vmg samples�=
Asheville ❑ Eden❑ Greenwood ❑ Huntersvilleo Raleigh❑ Mechanicsville[]
Sample Condition Client Name:
Upon Receipt A
Project ft:
Courier: []Fed Ex OUPS ❑USPS ❑Client
❑ Commercial Pace ❑Other:
Custody Seal Present? Dyes KNo Seals Intact? ❑Yes �No
WO# : 9239f 288
1111111111111111111111
92396288
� ��(Jy I
Date/Initiars Person Examining Contents:!
Packing Material ❑Bubble Wrap y 18ubble Bags ❑None ❑ Other Biological T1ssue rozen?
Thermome,� % ❑Yes ❑No VN/A
LrJ IR Gun o: 92TO43 Type of Ice: ❑Wet ❑slue �Ne�e
Cooler Temp (°C): Correction Factor: Add/Subtract (°C) -Q.2
TempshoLA be above freezing to VC
Cooler Temp Corrected (°C): ❑Samples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated soil 0 N/A, water sample)
Did samples orig ate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samplesofiginate from a foreign source (internationally,
I IYes o i—I—F—Hawaii anri Pnprtn Rirn)� F—iYas IJrNn
Comments/Discrepancy:
Samples Arrived within Hold Time?
VIYes
❑No
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
Des
ZN0
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
ZNo
❑N/A
4,
Sufficient Volume?
Zes
[:]Na
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
ZYes
es
❑No
[I No
❑N/A
❑N/A
6.
Containers Intact?
Yes
❑No
❑N/A
7,
Dissolved analysis: Samples Field Filtered?
[]Yes
❑No
N/A
S.
Sample Labels Match CDC?
-includes Date/`rme/ID/Analysis tvtatrix:
Yes
❑No
(—]N/A
9.
Headspace in VOAVials (>5-6mmi?
❑Yes
❑No
N/A
10.
Trip Blank Present?
Trip Wank Custody Seals Present?
Dyes
❑Yes
❑No
❑No
N/A
N/A
11,
COMMENTS/SAMPLE DISCREPANCY
Lot ID of spiit containers:
CLIENT NOTIFICATION/RESOLUTION
Field Data Required? []Yes ❑No
Person contacted: Datefrime:
Project Manager SCURF Review: 111�] Date: g
Project Manager SRF Review: Date: tom" � �J
V
Page 3 of 16

Document Name:
Document Revised: February7, 2018
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
issuing Authority:
aceAnalytrcala
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples,
Exceptions: VOA, Coliform, TOC, oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
Project # WO# : 92396288
PM: NMG Due Date: 08/31/18
CLIENT: 92- Joyce Eng
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added
Lot if
Note: Wheneverthete is a discrepancy affecting North Carolina comp(lante samples, a Copy of this Corm will oe sent to the North Carolina DEHNR Certification Ocoee {t.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 4 of 16

��nflar�;r�t
CHAIN
-OF -CUSTODY / Analytical Request Document
-
The Chi
in -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A
Se
tion a
Section C
Required Client Information:
Required
Project Information:
Invoice Information: Pa e : 1 Of 1
Attention',
Company Name',
Company; LaBellaAssociates, D.P.C.-NC
I lReiTO:
Van Burbach
Address. 2211 West Meadowview Rd
lCopy
To,
Greensboro, NC 27407
1
Address:
Regulatory Agency
EmaiP, vburbach label3apacom
Purchase Order #.
Pace Quote_
Phone, (336}707-3674 Fax i1
Project Name- Oxford Diss. Hydrogen
Pace Project Manager. nicole,gasiorowski pacelabs.com.
State 1 Location
Requested Due Date: -
Project #',
Pace Profile 9. 3566-1
NC
Requested
Anal
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lacmnalyficalo
August 27, 2018
Nicole Gasiorowski
Pace Analytical Services, Inc.
9800 Kincey Avenue
Suite 100
Huntersville, NC 28078
RE: OXFORD DISS. HYDROGEN
Pace Workorder. 27788
Dear Nicole Gasiorowski:
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Enclosed are the analytical results for sample(s) received by the laboratory on Tuesday, August 21, 2018.
Results reported herein conform to the most current NELAC standards, where applicable, unless otherwise
narrated in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Ruth Welsh 08/27/2018
[e-mail]
Customer Service Representative
Enclosures
As a valued client we would appreciate your comments on our service.
Please email [e-mail].
Report ID: 27788 - 1086021
F` CERTIFICATE OF ANALYSIS
ne"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.
Total Number of Pages
Page 1 of 10
Page 6 of 16

Pace Analytical Energy Services LLC
220 William Pitt Way
.,-- A__1.X__1 o Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
LABORATORY ACCREDITATIONS & CERTIFICATIONS
Accreditor: Pennsylvania Department of Environmental Protection, Bureau of Laboratories
Accreditation ID: 02-00538
Scope: NELAP Non -Potable Water
Accreditor:
West Virginia Department of Environmental Protection, Division of Water and Waste
Management
Accreditation ID:
395
Scope:
Non -Potable Water
Accreditor:
South Carolina Department of Health and Environmental Control, Office of Environmental
Laboratory Certification
Accreditation ID:
89009003
Scope:
Clean Water Act (CWA); Resource Conservation and Recovery Act (RCRA)
Accreditor:
State of Virginia
Accreditation ID:
460201
Scope:
Non -Potable Water
Accreditor:
NELAP: New Jersey, Department of Environmental Protection
Accreditation ID:
PA026
Scope:
Non -Potable Water
Accreditor:
NELAP: New York, Department of Health Wadsworth Center
Accreditation ID:
11815
Scope:
Non -Potable Water
Accreditor:
State of Connecticut, Department of Public Health, Division of Environmental Health
Accreditation ID:
PH-0263
Scope:
Clean Water Act (CWA) Resource Conservation and Recovery Act (RCRA)
Accreditor:
NELAP: Texas, Commission on Environmental Quality
Accreditation ID:
T104704453-09-TX
Scope:
Non -Potable Water
Accreditor:
State of New Hampshire
Accreditation ID:
299409
Scope:
Non -potable water
Accreditor:
State of Georgia
Accreditation ID:
Chapter 391-3-26
Scope:
As per the Georgia EPD Rules and Regulations for Commercial Laboratories, PAES is
accredited by the Pennsylvania Department of Environmental Protection Bureau of
Laboratories under the National Environmental Laboratory Approval Program (NELAC).
Report ID: 27788 - 1086021
F` CERTIFICATE OF ANALYSIS
nei"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.
Page 2 of 10
Page 7 of 16

lacmnalyficalo
SAMPLE SUMMARY
Workorder: 27788 OXFORD DISS. HYDROGEN
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID
Sample ID
Matrix
Date Collected
Date Received
277880001
3901-MW7
Bubble Strip
8/15/2018 12:15
8/21/2018 11:00
277880002
3901-MW5R
Bubble Strip
8/16/2018 09:36
8/21/2018 11:00
277880003
3901-NES2S
Bubble Strip
8/15/2018 15:58
8/21/2018 11:00
Report ID: 27788 - 1086021
4nela(f
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.
Page 3 of 10
Page 8 of 16

lacmnalyficalo
Workorder: 27788 OXFORD DISS. HYDROGEN
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 277880001 Date Received: 8/21/2018 11:00 Matrix: Bubble Strip
Sample ID: 3901-MW7 Date Collected: 8/15/2018 12:15
Parameters Results Units PQL MDL DF Analyzed By Qualifiers
RISK - PAES
Analysis Desc: AM20GAX Analytical Method: AM20GAX
Hydrogen 6.4 nM 1.0 0.65 1 8/24/201813:02 MM n
Report ID: 27788 - 1086021 Page 4 of 10
F` CERTIFICATE OF ANALYSIS
nei"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.
Page 9 of 16

lacmnalyficalo
Workorder: 27788 OXFORD DISS. HYDROGEN
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 277880002 Date Received: 8/21/2018 11:00 Matrix: Bubble Strip
Sample ID: 3901-MW5R Date Collected: 8/16/2018 09:36
Parameters Results Units PQL MDL DF Analyzed By Qualifiers
RISK - PAES
Analysis Desc: AM20GAX Analytical Method: AM20GAX
Hydrogen 4.3 nM 1.0 0.65 1 8/24/201813:14 MM n
Report ID: 27788 - 1086021 Page 5 of 10
F` CERTIFICATE OF ANALYSIS
nei"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.
Page 10 of 16

lacmnalyficalo
Workorder: 27788 OXFORD DISS. HYDROGEN
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 277880003 Date Received: 8/21/2018 11:00 Matrix: Bubble Strip
Sample ID: 3901-NES2S Date Collected: 8/15/2018 15:58
Parameters Results Units PQL MDL DF Analyzed By Qualifiers
RISK - PAES
Analysis Desc: AM20GAX Analytical Method: AM20GAX
Hydrogen 4.8 nM 1.0 0.65 1 8/24/201813:27 MM n
Report ID: 27788 - 1086021 Page 6 of 10
F` CERTIFICATE OF ANALYSIS
nei"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.
Page 11 of 16

lacmnalyficalo
ANALYTICAL RESULTS QUALIFIERS
Workorder: 27788 OXFORD DISS. HYDROGEN
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
DEFINITIONS/QUALIFIERS
MDL Method Detection Limit. Can be used synonymously with LOD; Limit Of Detection.
PQL Practical Quanitation Limit. Can be used synonymously with LOQ; Limit Of Quantitation.
ND Not detected at or above reporting limit.
DF Dilution Factor.
S Surrogate.
RPD Relative Percent Difference.
% Rec Percent Recovery.
U Indicates the compound was analyzed for, but not detected at or above the noted concentration.
J Estimated concentration greater than the set method detection limit (MDL) and less than the set reporting limit (PQL).
n The laboratory does not hold NELAP/TNI accreditation for this method or analyte.
Report ID: 27788 - 1086021
4r-tiela(f
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.
Page 7 of 10
Page 12 of 16

lacmnalyficalo
QUALITY CONTROL DATA
Workorder: 27788 OXFORD DISS. HYDROGEN
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
QC Batch: DISG/7027
Analysis Method:
AM20GAX
QC Batch Method: AM20GAX
Associated Lab Samples: 277880001, 277880002, 277880003
METHOD BLANK: 57143
Blank
Reporting
Parameter Units
Result
Limit Qualifiers
RISK
Hydrogen nM
0.65U
0.65 n
LABORATORY CONTROL SAMPLE & LCSD:
57144
57145
Spike LCS
LCSD LCS
LCSD % Rec Max
Parameter Units
Conc. Result
Result % Rec
% Rec Limit RPD RPD Qualifiers
RISK
Hydrogen nM
24 24
24 97
99 80-120 1.8 20 n
Report ID: 27788 - 1086021
.4r-tielac�,
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.
Page 8 of 10
Page 13 of 16

lacmnalyficalo
QUALITY CONTROL DATA QUALIFIERS
Workorder: 27788 OXFORD DISS. HYDROGEN
QUALITY CONTROL PARAMETER QUALIFIERS
The laboratory does not hold NELAP/TNI accreditation for this method or analyte.
Report ID: 27788 - 1086021
4r-tiela(f
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Page 9 of 10
Page 14 of 16

lacmnalyficalo
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Workorder: 27788 OXFORD DISS. HYDROGEN
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Analysis
Lab ID
Sample ID
Prep Method Prep Batch Analysis Method
Batch
277880001
3901-MW7
AM20GAX
DISG/7027
277880002
3901-MW5R
AM20GAX
DISG/7027
277880003
3901-NES2S
AM20GAX
DISG/7027
Report ID: 27788 - 1086021
4r-tiela(f
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.
Page 10 of 10
Page 15 of 16

Chain of Custody
Workorder: 92396288 Workorder Name: Oxford Diss. Hydrogen
Results Requested By:
1�;aceAnaljftal
www.pacWabs.com
8/31/2018
..... . ....
Requeste Analysis M
'M�
Nicole Gasiorowski
Pace Analytical Charlotte P.O. tK>1
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
Phone [phone]
Email: [e-mail]
>
State of Sample Origin: NC
>
tn
. ...... . .. ... . ...... . ........... . ...... . ........
.. . .......
..... . ... . .....
.. ........ ...... ...... .
... . . . . . . . .
E- . .... . ...
1m
...
................ .
.mgg
.......
... . .. . ...
LAB USE ONLY
----------
1
3901- MW7 8/15/2018 12:15
92396288001
Water
X
2
3901-MW5R 8/16/2018 09:36
92396288002
Water
X
3
3901-NES2S 8/15/2018 15:58
92396288003
Water
X
4
5
. . . . . . . . . .
---m— . .......
...... . ..... . .. . .
.
. .........
............
111- -1-
... .. .... .....
....... . .
-`3
......... ..
H.
. ....
Comments
Transfers
Ikelea4ed By
DaterTime
Received By
Date/Time
2
13
I Cooler Temperature on Receipt C
Custody Seal Y or N
Received on Ice Y or N
Samples lnta4 Y )or N
T
w
CC CD
c�
Fiday, August 17, 2018 5:29:29 PM FMT-ALL-C-002rev.00 24March2009 Page 1 of 1

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
November 11, 2018
Mr. Van Burbach
Joyce Engineering -NC
2211 West Meadowview Rd
Boone Bldg, Suite 101
Greensboro, NC 27407
RE: Project: Oxford Compliance Unit 1
Pace Project No.: 92405949
Dear Mr. Burbach:
Enclosed are the analytical results for sample(s) received by the laboratory on November 05, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
��i Flo _ _.1I , .�:
Nicole Gasiorowski
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Daniel Girdner, LaBella Associates, D.P.C.
Miguel Vazquez, Joyce Engineering
Rochelle mesubed, Joyce Engineering
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 14

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Oxford Compliance Unit 1
Pace Project No.: 92405949
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 14

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: Oxford Compliance Unit 1
Pace Project No.: 92405949
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92405949001
92405949002
3901-MW2
3901-MW2 (Filtered)
Water
Water
11/02/1816:18
11/02/18 16:18
11/05/1810:16
11/05/18 10:16
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 14

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: Oxford Compliance Unit 1
Pace Project No.: 92405949
Analytes
Lab lD Sample ID Method Analysts Reported Laboratory
92405949001 3901-MW2 EPA 601OD SH1 3 PASI-A
92405949002 3901-MW2 (Filtered) EPA 601OD SH1 3 PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 14

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SUMMARY OF DETECTION
Project:
Pace Project No.:
Oxford Compliance Unit 1
92405949
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed Qualifiers
92405949001
3901-MW2
EPA 6010D
Chromium
4.1J
ug/L
10.0
11/09/18 02:53
EPA 6010D
Cobalt
8.3J
ug/L
10.0
11/09/18 02:53
EPA 6010D
Vanadium
13.OJ
ug/L
25.0
11/09/18 02:53
92405949002
3901-MW2 (Filtered)
EPA 6010D
Cobalt, Dissolved
7.1
ug/L
5.0
11/08/18 23:09
EPA 6010D
Vanadium, Dissolved
2.7J
ug/L
5.0
11/08/18 23:09
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 5 of 14

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Oxford Compliance Unit 1
Pace Project No.: 92405949
Sample: 3901-MW2
Lab ID:
92405949001
Collected:
11/02/18 16:18
Received: 11/05/18 10:16 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical
Method: EPA 6010D
Preparation Method: EPA 3010A
Chromium
4.1J
ug/L
10.0
2.5 1
11/06/18 06:30
11/09/18 02:53
7440-47-3
Cobalt
8.3J
ug/L
10.0
2.5 1
11/06/18 06:30
11/09/18 02:53
7440-48-4
Vanadium
13.OJ
ug/L
25.0
2.5 1
11/06/18 06:30
11/09/18 02:53
7440-62-2
Date: 11 /11 /2018 10:25 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 14

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Oxford Compliance Unit 1
Pace Project No.: 92405949
Sample: 3901-MW2 (Filtered)
Lab ID:
92405949002
Collected:
11/02/18 16:18
Received: 11/05/18 10:16 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP, Dissolved
Analytical
Method: EPA 601
OD Preparation Method: EPA 3010A
Chromium, Dissolved
ND
ug/L
5.0
2.5 1
11/06/18 14:50
11/08/18 23:09
7440-47-3
Cobalt, Dissolved
7.1
ug/L
5.0
2.5 1
11/06/18 14:50
11/08/18 23:09
7440-48-4
Vanadium, Dissolved
2.7J
ug/L
5.0
2.5 1
11/06/18 14:50
11/08/18 23:09
7440-62-2
Date: 11 /11 /2018 10:25 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 14

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Oxford Compliance Unit 1
Pace Project No.: 92405949
QC Batch: 440466 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Associated Lab Samples: 92405949001
METHOD BLANK: 2419390
Matrix:
Water
Associated Lab Samples: 92405949001
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
Chromium
ug/L
ND
10.0
2.5 11/09/18 02:28
Cobalt
ug/L
ND
10.0
2.5 11/09/18 02:28
Vanadium
ug/L
ND
25.0
2.5 11/09/18 02:28
LABORATORY CONTROL SAMPLE:
2419391
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Chromium
ug/L
500
490
98
80-120
Cobalt
ug/L
500
487
97
80-120
Vanadium
ug/L
500
495
99
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2419392
2419393
MS
MSD
92405943001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD RPD Qual
Chromium ug/L
ND
500
500
494
487
99
97
75-125
2 20
Cobalt ug/L
10.0
500
500
481
475
94
93
75-125
1 20
Vanadium ug/L
4.1J
500
500
511
503
101
100
75-125
1 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2018 10:25 AM without the written consent of Pace Analytical Services, LLC.
Page 8 of 14

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Oxford Compliance Unit 1
Pace Project No.: 92405949
QC Batch: 440518 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET Filtered Diss.
Associated Lab Samples: 92405949002
METHOD BLANK: 2419525
Associated Lab Samples: 92405949002
Parameter
Units
Chromium, Dissolved
ug/L
Cobalt, Dissolved
ug/L
Vanadium, Dissolved
ug/L
Matrix: Water
Blank Reporting
Result Limit
ND 5.0
ND 5.0
ND 5.0
MDL Analyzed
2.5 11/08/18 22:50
2.5 11/08/18 22:50
2.5 11/08/18 22:50
Qualifiers
LABORATORY CONTROL SAMPLE:
2419526
Spike
LCS LCS % Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
Chromium, Dissolved
ug/L
500
494 99 80-120
Cobalt, Dissolved
ug/L
500
487 97 80-120
Vanadium, Dissolved
ug/L
500
493 99 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2419527
2419528
MS
MSD
92405943002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD RPD Qual
Chromium, Dissolved
ug/L
ND
500
500
444
445
89
89
75-125
0 20
Cobalt, Dissolved
ug/L
9.3
500
500
434
435
85
85
75-125
0 20
Vanadium, Dissolved
ug/L
3AJ
500
500
458
458
91
91
75-125
0 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2018 10:25 AM without the written consent of Pace Analytical Services, LLC.
Page 9 of 14

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: Oxford Compliance Unit 1
Pace Project No.: 92405949
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2018 10:25 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 14

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Oxford Compliance Unit 1
Pace Project No.: 92405949
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92405949001 3901-MW2 EPA 3010A 440466 EPA 6010D 440500
92405949002 3901-MW2 (Filtered) EPA 3010A 440518 EPA 6010D 440673
Date: 11 /11 /2018 10:25 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 14

Document Name: Document Revised: February 7, 2018
aceAnalXldal h Sample Condition Upon Recei t(SCUR) Page 1 of 2
Document No.: Issuing Authority:
F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑
Sample Condition Client Name.
Upon Receipt ffo yce,
—Courier. F dEx ❑UPS ❑U5P5
❑ Commercial Pace ❑Other:
Custody Seal Present? ❑Yes l3No Seals Intact? Des
Huntersville [` Raleigh❑ Mechanlesville❑
Project # WO# : 92405949
Client 11 U1111111WRI
924059�49
❑� 3
Date/Initials Person Examining Contents: eW
Packing Material; ❑Bubble Wrap ❑Bubble Bags ❑None ❑ Other Biological Tissue �Frf en?
Thermometer: / ❑Yes ❑No [Qi`I/A
IR Gun ID: 92TO 5 Type of rco: ®Wet [-]Blue ❑None
Cooler Temp ('C): 3.( Correction Factor: Add/Subtract ('Cj _() j
Cooler Temp Corrected {'C}: _�] C� Temp should be above freezing to 6'C
❑Samples out of temp criteria. Samples on ice, cooling process
USDA Regulated Soll { N/A, water sample] has begun
Did samples o�r-i-g�in to in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (intern nally,
❑Yes Ea including Hawaii and Puerto Rica)? []Yes FINo
Chain of Custody Present?
Samples Arrived within Hold Time?
Short Hold Time Analysis 1<72 hr.)?
Rush Turn Around Time Requested?
Sufficient Volume?
Correct Containers Used?
-Pace Containers Used?
Containers Intact?
Dissolved analysis: Samples Field Filtered?
Sample Labels Match COC?
Includes Date/Time/ID/Analysis
Headspace in VOA Vials (>5-6mm)?
Trip Blank Present?
Trip Blank Custody Seals Present?
COMMENTS/SAMPLE DISCREPANCY
M'es El No ❑N/A 16.
t A ! .l
UNo ❑N//A 7
[IN. [%A B.
❑No ❑N/A 1 9.
UNo LJN 10.
❑No �/A 11.
17No IaiA
CLIENT NDTIFI[A7IDN/RfSDi.UT10N Lot ID of split containers:
Person contacted: Date/Time:
Project Manager SCURF Review: 6
L
^
Project Manager SRF Review: 1VM 6
Field Data Required? ❑Yes ❑Na
Date: G� 5
Date:
Page 12 of 14

__ � aeeAraalytrea!"
Document Name:
Sample Condition Upon RecelptiSCUR)
Document Revised: February 7, 2018
Page 1 of 2
Document No.:
F-CAR-CS-033-Rev,06
Issuing Authority,
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination Is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
** Bottom half of box is to [istnumber of bottle
Project W0# ; 92405949
PM: NMG Due Date: 11/12/18
CLIENT: 92—Joyce Eng
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
pate preservation adjusted
Time preservation
adJuated
Amount of Preservative
added
Lot+r
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a Copy of this form will be sent to the North Carolina OEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out o{temp, incorrect containers.
Page 13 of 14

Section A
Required Client Information:
Company: JO ce En it
Address: 2211 West I
Greensboro, NC 27407
0
CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. a
Section B
Section C
Required Project Information:
Invoice Information:
Ripon ro: Van Burbach AilenEion: Pe e = t Of r
copy To: Rochelle Mesubed Jason Falls
company Name: Granville County, Solid Waste
Address: P.O. Box 906, Oxford NC 27565
purchase Order No. Regulartmy Agency
.Iienr Project lD: Oxford Compliance Unit 1
ne nested Anal sis Filtered YIN
MATRIX
WIDE
a
o o
COLLECTED
Preservatives
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ow
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WT
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SAMPLE 1D
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One Character per box.
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START END
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(A-Z. 0-91 , -)
A"
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Sample Ids must be unique
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ADDITIONAL COMMENTS
RELINQUISHED
BY / AFFILIATiON
DATE
TIME
ACCEPTED
BY AFFIUATION DATE TIME
'
SAMPLE CONDITIONS
SAMPLER NAME AND SIGNATURE
PRINT Name of SAMPLER:
°1
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:;
W,

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
November 11, 2018
Mr. Van Burbach
Joyce Engineering -NC
2211 West Meadowview Rd
Boone Bldg, Suite 101
Greensboro, NC 27407
RE: Project: Oxford Comp Unit 1 & Butner LF
Pace Project No.: 92405939
Dear Mr. Burbach:
Enclosed are the analytical results for sample(s) received by the laboratory on November 05, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
��i Flo _ _.1I , .�:
Nicole Gasiorowski
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Daniel Girdner, LaBella Associates, D.P.C.
Miguel Vazquez, Joyce Engineering
Rochelle mesubed, Joyce Engineering
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 11

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Oxford Comp Unit 1 & Butner LF
Pace Project No.: 92405939
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 11

aceAnalytical
—pacelabsxom
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: Oxford Comp Unit 1 & Butner LF
Pace Project No.: 92405939
Lab ID Sample ID Matrix Date Collected Date Received
92405939001 Equipment Blank Water 11/02/18 16:35 11/05/18 10:16
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 11

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: Oxford Comp Unit 1 & Butner LF
Pace Project No.: 92405939
Lab ID Sample ID Method
92405939001 Equipment Blank EPA 601 OD
REPORT OF LABORATORY ANALYSIS
Analytes
Analysts Reported
SH1
Laboratory
PAS I -A
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 11

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Oxford Comp Unit 1 & Butner LF
Pace Project No.: 92405939
Sample: Equipment Blank
Lab ID:
92405939001
Collected:
11/02/18 16:35
Received: 11/05/18 10:16 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical
Method: EPA 6010D
Preparation Method: EPA 3010A
Chromium
ND
ug/L
10.0
2.5 1
11/06/18 06:30
11/09/18 03:06
7440-47-3
Cobalt
ND
ug/L
10.0
2.5 1
11/06/18 06:30
11/09/18 03:06
7440-48-4
Vanadium
ND
ug/L
25.0
2.5 1
11/06/18 06:30
11/09/18 03:06
7440-62-2
Date: 11 /11 /2018 10:06 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 11

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Oxford Comp Unit 1 & Butner LF
Pace Project No.: 92405939
QC Batch: 440466 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Associated Lab Samples: 92405939001
METHOD BLANK: 2419390
Matrix:
Water
Associated Lab Samples: 92405939001
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
Chromium
ug/L
ND
10.0
2.5 11/09/18 02:28
Cobalt
ug/L
ND
10.0
2.5 11/09/18 02:28
Vanadium
ug/L
ND
25.0
2.5 11/09/18 02:28
LABORATORY CONTROL SAMPLE:
2419391
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Chromium
ug/L
500
490
98
80-120
Cobalt
ug/L
500
487
97
80-120
Vanadium
ug/L
500
495
99
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2419392
2419393
MS
MSD
92405943001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD RPD Qual
Chromium ug/L
ND
500
500
494
487
99
97
75-125
2 20
Cobalt ug/L
10.0
500
500
481
475
94
93
75-125
1 20
Vanadium ug/L
4.1J
500
500
511
503
101
100
75-125
1 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2018 10:06 AM without the written consent of Pace Analytical Services, LLC.
Page 6 of 11

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: Oxford Comp Unit 1 & Butner LF
Pace Project No.: 92405939
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /11 /2018 10:06 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 11

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Oxford Comp Unit 1 & Butner LF
Pace Project No.: 92405939
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92405939001 Equipment Blank EPA 3010A 440466 EPA 6010D 440500
Date: 11 /11 /2018 10:06 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 8 of 11

Document Name;
Document Revised: February 7, 2018
aeeAnalAicai
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-GAR-CS-033•Rev,06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑
Client Name:
Courier:
❑ Commercial
Greenwood ❑ Huntersville Er Raleigh❑ Mechanicsville❑
Project!: W0# : 92405939
-cN �irnmt�� t eft 6P5 ❑U5P5 ❑Client
❑other: 924OS939
Custody Seal Present? ❑Yes ❑No seals intact? ❑Yes ErNo
natahnitieis Person Examinlniz Contents: 0
Packing Material: ❑Bubble Wrap []Bubble Bags None ❑ Other Biological Tissue Fro en?
Thermometer []Yes [:]NOFIR Gun 10: 92T045 Type of Ice: [3Wet []Yes
❑None
Cooler Temp (°C): 31 r/ Correction Factor: Add/Subtract (°C] _{) j
�*-, Temp should be above freezing to b°C
Cooler Temp Corrected rcl: r lam' ❑samples out of temp criteria. Samples an ice, cooling process
hashegun
USDA Regulated Soil (E]---N//A, water sample)
Did samples origin a in a quarantine zone within the United States: CA, NY, or 5C (check maps►? Did samples originate from a foreign source linterna onally,
1-1— inrhirlinp Hawaii and Puerto Rical? FlYes 0
Comments/Discrepancy:
/
Chain of Custody Present?
2,Y-
❑No
❑N/A
1,
Samples Arrived within Hold Time?
❑Ves
❑N/a
N/A
2.
Short Hold Time Analysis (02 hr.)?
❑Yes
01v//o
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
ONo
❑N/A
4.
Sufficient Volume?
[DYes
ONO
❑N/A
S.
Correct Containers Used?
L7Yes
❑No
❑NIA
6.
-Pace Containers Used?
[ [YCs
❑No
❑N/A
Containers Intact?
['Yes
ONO
❑N/A
7.
Dissolved analysis; Samples Field Filtered?
❑Yes
❑No
0N/A
B.
Sample Labels Match COC?
(3�es
❑No
❑NIA
9.
-includes Date/Time/ID/Analysis Matrix:
CAJ
Headspace in VOA Vials (>5-6mm)?
Dyes
❑No
��
C❑N/A
10.
Trip Blank Present?
❑yes
❑No
CgZ;/AA
11.
Trip Blank Custody seals Present?
❑Yes
[]No
Ml /A
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Date/Time:
Lot ID of split containers;
Project Manager SCURF Review:
Project Manager SRF Review:
Field Data Required? ❑Yes []NO
Date:
Date: L;
Page 9 of 11

_, ace Analytical'
Document Name:
Sample Condition upon Recell
Document No.:
F-CAR-CS-033-Rev.06
*Check mark top half of box if pH and/or dechlorination Is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, coliform, TOC, Oil and Grease, DRO/8015 {water} DOC, LLHg
**Bottom half of box is to list number of bottle
Document Revised: February 7, 2018
Page 1 of 2
Issuing Authority:
Pace Carolinas Quality Office -
Project WO# : 92405939
RM: NMf Due Date: 11/19/18
CLIENT: 92-Joyce Eng
ayEr
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Note: Whenever there is a discrepancy affecting North Carolina compuance samples, a copy ui « +�, ++ �,,, �_•_ • •� ^ - -- -
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 10 of 11

CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. i
Section A
Section B Section C
Required Client Information:
Required Project Information: Invoice Information: Page: 1 Of 1
Report To: Van Burbach Attention: Jason Falls
Rd Copy To: Rochelle Mesubed company Name: Granville County, Solid Waste
Company: Joyce Engineering
Address: 2211 West Meadowvie1N
Greensboro, INC 27407
Address: P.O. Box 906, Oxford NC 27565
Regulatory Agency
Email To� vUi11! r!c:l r: yc:.'vc:�:I Ir111
CMI .Colic
Purchase Order No.
Phone: [phone] Fax
Client project ID: Oxford Compliance Unit 1 & Butner LF
State/ Location
Requested Due Date/TAT: 10 Da DdfauIt
Container Order Number:
North Carolina
_
Requested
An
lysis
Filtered
Y1N
o
COLLECTED
Preservatives
MnTFlx cooE
o
Drinking Wamr Dw
Water WT
o
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tJ
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=
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was<a Warnr WW
Product P
SAMPLE ID 01=hd oL
—
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START
END
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One Character per box. w,Pn wP
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Sample Ids must 6e unique �ssu`n Ts
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2
3
4
5
6
7
8
9
10
11
12
ADDITIONAL COMMENTS
RELINQUISHED BY 1 AFFILIATION
DATE
TIME
ACCEPTED BY! AFFILIATION
DATE
TIME
SAMPLE CONDITIONS
MIS
J4
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SAMPLER NAME AND SIGNATURE
°
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PRINT Name of SAMPLER: n--
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SIGNATURE of SAMPLER:
DATE Signed:
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UU
U)}

Appendix C
Historical Data Tables
Table C-01
Historical Groundwater Elevation Data
Table C-02
Historical Detected Inorganic Constituents in Compliance Wells
Table C-03
Historical Detected Organic Constituents in Compliance Wells
Table C-04
Historical Detected COCs in Performance and Sentinel Wells
Table C-05
Historical Detected Constituents in Surface Water
Table C-06
Historical MNA Parameter Data

TABLE C-01: Historical Groundwater Elevation Data
Background
Downgradient
Performance/Sentinel
Well ID:
MW-1
MW-lA
MW-7
MW-2
MW-3R
MW-4R
MW-5R
MW-6R
NES-1S
NES-ID
NES-2S
NES-2D
Well TOC Elev.:
121.46
538.18
534.24
518.62
503.82
507.34
489.95
506.81
516.93
516.62
477.20
477.43
Well Total Depth:
28.77
34.50
29.34
31.63
63.22
40.25
42.90
36.10
57.75
24.20
69.20
10-Sep-99
101.71
517.91
-
507.76
481.40
493.62
467.65
496.53
-
-
-
-
16-Nov-99
105.76
522.86
-
506.32
483.55
494.83
468.75
498.24
-
-
-
-
10-May-00
109.47
527.66
-
507.89
487.20
499.63
470.65
500.59
-
-
-
-
26-Oct-00
103.54
518.89
-
504.12
480.86
495.21
467.39
496.95
-
-
-
-
18-Apr-01
107.87
526.23
-
508.01
486.62
498.50
470.79
500.21
-
-
-
-
27-Oct-01
-
514.65
-
501.42
478.79
494.79
466.70
494.92
-
-
-
-
10-Jun-02
-
515.06
-
502.91
480.10
495.19
467.06
496.26
-
-
-
-
19-Nov-02
-
518.61
-
512.08
489.84
498.82
471.80
498.70
-
-
-
-
27-Jun-03
-
529.42
-
508.76
488.69
500.79
471.72
501.38
-
-
-
-
29-Dec-03
-
528.91
-
509.06
488.06
499.94
471.10
501.21
-
-
-
-
29-Jun-04
-
520.03
-
505.24
481.10
497.84
467.72
499.21
-
-
-
-
28-Dec-04
-
526.73
-
509.09
485.27
499.14
469.51
500.76
-
-
-
-
29-Jun-05
-
520.37
-
504.64
481.10
497.60
467.63
499.15
-
-
-
-
29-Dec-05
-
519.54
-
509.66
482.69
498.33
468.57
499.25
-
-
-
-
27-Jun-06
-
517.93
-
507.85
481.85
497.64
468.00
498.63
-
-
-
-
27-Dec-06
-
523.00
-
511.07
489.81
499.43
471.76
500.83
493.70
-
469.82
-
12-Jul-07
-
516.94
-
502.49
479.84
497.17
467.18
497.59
-
-
-
-
18-Dec-07
-
510.35
-
501.46
477.54
495.40
464.09
493.14
-
-
-
-
7-Jul-08
-
515.96
-
501.99
479.52
497.04
466.79
496.71
-
-
-
-
16-Dec-08
-
532.53
-
509.80
487.98
498.08
470.11
499.29
489.19
488.63
469.47
472.71
7-Jul-09
-
518.28
-
505.37
481.57
497.43
467.88
499.36
490.38
490.07
467.73
470.91
14-Dec-09
-
533.10
-
511.89
491.93
500.61
473.65
501.48
494.70
493.21
470.98
467.14
22-Jun-10
-
518.45
-
506.72
485.92
499.94
469.67
499.68
493.47
493.07
468.97
471.53
13-Dec-10
-
509.41
-
507.89
482.82
498.20
467.87
496.65
488.89
-
468.03
-
20-Jun-11
-
515.17
513.91
504.60
482.72
499.96
467.76
498.63
492.11
491.51
468.03
474.35
5-Dec-11
-
513.35
507.92
507.44
484.94
498.29
468.45
497.17
488.15
487.45
468.25
464.93
13-Jun-12
-
514.08
513.48
507.48
485.36
499.29
468.04
498.85
487.08
490.33
468.81
467.64
12-Dec-12
-
511.34
506.86
503.10
481.55
497.24
466.90
494.83
486.84
486.26
467.26
461.41
29-Apr-13
-
515.88
513.26
509.38
485.47
500.82
469.60
501.15
492.31
491.64
470.45
455.26
5-Aug-13
-
517.21
514.33
505.98
484.47
500.29
468.65
500.83
494.12
-
469.29
-
25-Feb-14
-
514.06
511.75
509.82
486.32
501.50
473.05
501.99
491.83
491.54
470.28
461.18
12-Aug-14
-
519.34
511.98
507.52
485.44
499.25
468.90
499.30
491.92
491.41
470.29
460.31
11-Mar-15
-
524.32
516.39
510.37
487.12
502.94
474.18
504.41
500.98
500.12
470.63
473.63
18-Aug-15
-
516.53
512.39
503.47
482.97
500.94
466.45
498.81
492.38
-
469.25
449.71
16-Feb-16
-
526.03
515.79
510.07
486.93
501.84
475.45
503.66
500.23
-
471.15
469.18
10-Aug-16
-
520.07
514.29
507.08
484.07
500.34
468.20
500.89
491.95
-
470.40
453.23
14-Feb-17
-
524.14
510.89
507.72
484.44
500.34
468.86
501.06
491.73
-
468.85
453.13
23-Aug-17
-
523.08
508.84
506.59
482.82
497.02
467.19
498.16
491.68
-
469.80
452.94
6-Feb-18
-
522.73
505.74
507.91
485.62
498.54
468.25
500.31
491.78
-
471.40
470.93
14-Aug-18
514.72
510.22
504.44
484.15
498.36
467.48
498.66
-
-
470.81
474.46
Notes: TOC = top of casing.
Water levels are measured from TOC.
All elevations are in feet above mean sea level (ft-amsl).
- = data not available.
MW-7 added to monitoring network in early 2011.
Prior to December 2012, the TOC elevation for MW-3R was 498.35 ft-amsl.
Granville Co. - Oxford Landfill, Unit 1
Permit 3901-CDLF-1997 Joyce Engineering

TABLE C-02: Historical Detected Inorganic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-1A
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Inorganic Compounds
Antimony
14-Sep-94
---
30
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
2-Dec-94
---
30
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
8-Feb-95
---
30.0
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
2-Mar-95
---
30.0
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
17-Nov-95
---
30.0
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
23-May-96
---
30.0
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
14-Nov-96
---
30.0
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
18-Jun-97
---
30.0
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
2-Dec-97
---
30.0
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
27-May-98
---
30.0
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
16-Nov-98
---
30.0
6
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
10-Sep-99
---
30.0
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
16-Nov-99
---
30.0
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
---
30.0
32
ND
---
ND
---
ND
---
ND
---
68
---
ND
---
26-Oct-00
---
30.0
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
---
30
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Oct-01
---
30
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
13-Jun-02
---
30
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
19-Nov-02
---
30.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Jun-03
---
30.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
30-Dec-03
---
30.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
30-Jun-04
---
30.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
---
30.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Jun-05
---
30.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
---
30.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Jun-06
---
30.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Dec-06
---
6.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
2-Jul-07
---
6.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
GWPS = 1.4 µg/L (10/23/07)
19-Dec-07
---
6.0
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
8-Jul-08
---
6.0
---
ND#
---
ND
---
ND
---
ND
---
ND
---
ND
ND
16-Dec-08
2.6
6.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
8-Jul-09
2.6
6.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Dec-09
2.6
6.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
23-Jun-10
2.6
6.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
GWPS = 1 µg/L (08/01/10)
14-Dec-10
2.6
6.0
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
21-Jun-11
5.0
6.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Dec-11
5.0
6.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Jun-12
5.0
6.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
11-Dec-12
5.0
6.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Apr-13
5.0
6.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug-13
5.0
6.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
25-Feb-14
5.0
6.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
5.0
6.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Mar-15
3.8
6.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
19-Aug-15
3.8
6.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
18-Feb-16
3.8
6.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
11-Aug-16
3.8
6.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Feb-17
3.9
6.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
24-Aug-17
3.9
6.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
7-Feb-18
3.9
6.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Aug-18
3.9
6.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit3901-CDLF-1997 Page 1 of22

TABLE C-02: Historical Detected Inorganic Constituents in Compliance Wells
Analyte
Sample Collection Date
DI, RL
MW-1
MW-1A
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Arsenic
14-Sep-94
---
10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
2-Dec-94
---
10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
8-Feb-95
---
10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
2-Mar-95
---
10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
17-Nov-95
---
10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
23-May-96
---
10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
14-Nov-96
---
10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
18-Jun-97
---
10
ND
7.0
---
14.0
14.0
---
ND
---
ND
---
5.0
---
---
2-Dec-97
---
10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
27-May-98
---
10
ND
ND
---
ND
5.0
---
ND
---
ND
---
ND
---
---
16-Nov-98
---
10
ND
ND
---
12.0
8.0
---
ND
---
ND
---
6.0
---
---
10-Sep-99
---
10
ND
ND
---
ND
---
ND
---
ND
---
11.0
---
ND
---
16-Nov-99
---
10
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
---
10
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
26-Oct-00
---
10
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Oct-01
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
13-Jun-02
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
19-Nov-02
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Jun-03
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
30-Dec-03
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
30-Jun-04
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Jun-05
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Jun-06
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Dec-06
---
10
---
4.4 J
---
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Jul-07
---
10
---
ND
---
4.9 J
---
ND
---
ND
---
ND
---
ND
ND
NC 2L = 50 µ L 10 23 07
19-Dec-07
---
10
---
---
---
2.9 J
---
ND
---
ND
---
ND
---
ND
ND
8-Jul-08
---
10.0
---
182#
---
3.7 J
---
ND
---
ND
---
ND
---
ND
ND
16-Dec-08
2.7
11.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
8-Jul-09
2.7
10.0
---
9.7 J
---
ND
---
ND
---
4.9 J
---
ND
---
2.9 J
ND
15-Dec-09
2.7
10.0
---
ND
---
3.2 1
---
ND
---
ND
---
ND
---
ND
ND
NC 2L=10 µ 5/10)
23-Jun-10
2.7
1.
---
5.9 J
---
2.7 J
---
ND
---
5.2 J
---
ND
---
4.4 J
ND
14-Dec-10
2.7
10.0
---
---
---
ND
---
ND
---
4.4 J
---
ND
---
ND
ND
21-Jun-11
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Dec-11
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Jun-12
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
11-Dec-12
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Apr-13
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug-13
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
25-Feb-14
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Mar-15
2.5
10.0
---
---
ND
5.5 J
---
2.9 J
---
3.8 J
---
ND
---
ND
ND
19-Aug-15
2.5
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
18-Feb-16
2.5
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
11-Aug-16
2.5
10.0
---
---
ND
3.5 J
---
ND
---
3.2 J
---
ND
---
3.7 J
ND
15-Feb-17
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
24-Aug-17
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
7-Feb-18
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Aug-18
5.0
10.0
---
---
ND
5.3 J
---
ND
---
ND
---
ND
---
ND
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 Page 2 of 22

TABLE C-02: Historical Detected Inorganic Constituents in Compliance Wells
Analyte
Sample Collection Date
DI, RL
MW-1
MW-1A
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Barium
14-Sep-94
---
500
680
680
---
260
580
---
30,300
---
ND
---
1,740
---
---
2-Dec-94
---
500
ND
ND
---
ND
ND
---
540
---
ND
---
ND
---
---
8-Feb-95
---
500
ND
ND
---
ND
ND
---
621
---
ND
---
ND
---
---
2-Mar-95
---
500
ND
ND
---
ND
541
---
2,710
---
ND
---
ND
---
---
17-Nov-95
---
500
ND
ND
---
ND
ND
---
2,440
---
ND
---
ND
---
---
23-May-96
---
500
ND
ND
---
ND
ND
---
0
---
ND
---
ND
---
---
14-Nov-96
---
500
2,500
510
---
600
480
---
1,700
---
39
---
21
---
---
18-Jun-97
---
500
960
1,200
---
280
720
---
3,400
---
93
---
700
---
---
---
68
---
260
---
---
27-May-98
---
500
2,100
310
---
95
660
---
2,800
---
69
---
350
---
---
>
---
100
---
5,900
---
---
10-Sep-99
---
500
ND
ND
---
ND
--
ND
---
ND
---
ND
---
ND
---
16-Nov-99
---
500
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
---
500
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
26-Oct-00
---
500
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
---
500
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Oct-01
---
500
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
13-Jun-02
---
500
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
19-Nov-02
---
500
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Jun-03
---
500
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
30-Dec-03
---
500
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
30-Jun-04
---
500
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
---
500
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Jun-05
---
500
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
---
500
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Jun-06
---
500
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Dec-06
---
100
---
15.4
---
30.8
---
24.8
---
78.5
---
33.4
---
77.4
0.20 J
NC 2L=2,000 µ 7
1 -Ju - 7
--
100
---
19.4 J
---
13.8 J
---
24.5 J
---
82.5 J
---
27.3 J
---
76.2 J
ND
19-Dec-07
---
100
---
---
---
14.7 B
---
20.1 B
---
28.7 B
---
27.2 B
---
64.9
10.5
8-Jul-08
---
100
---
5360#
---
21.7 J
---
19.6 J
---
54.1 J
---
35.3 J
---
78.2 J
0.29 J
16-Dec-08
0.20
100
---
19.4 B
---
11.2 B
---
16.5 B
---
27.0 B
---
38.8 B
---
66.7 J
10.7 J
8-Jul-09
0.20
100
---
213
---
11.9 B
---
26.6 B
---
74.6 B
---
34.2 B
---
78.4 B
17.6 J
15-Dec-09
0.20
100
---
12.6 B
---
16.4 B
---
18.8 B
---
38.2 B
---
39.8 B
---
89.3 J
17.1 J
NC 2L = 700 µg/L (2/5/10)
23-Jun-10
0.20
100
---
61.2 B
---
12.0 B
---
17.7 B
---
107 B
---
36.7 B
---
74.2 B
27.3 J
14-Dec-10
0.20
100
---
---
---
11.7 B
---
26.8 B
---
37.6 B
---
46.1 B
---
79.0 J
12.1 J
21-Jun-11
5.0
100
---
---
6.8 J
14.6 J
---
18.6 J
---
37.2 J
---
41.7 J
---
78.7 J
ND
---
43.3 J
---
83.7 J
ND
13-Jun-12
5.0
100
---
---
9.2 J
16.5 J
---
20.4 J
---
52.2 J
---
39.0 J
---
82.2 J
ND
11-Dec-12
5.0
100
---
---
5.2 J
12.6 J
---
17.2 J
---
32.1 J
---
47.3 J
---
81.9 J
ND
29-Apr-13
5.0
100
---
---
ND
14.7 J
---
19.6 J
---
37.6 J
---
42.2 J
---
81.8 J
ND
6-Aug-13
5.0
100
---
---
ND
19.7 J
---
18.7 J
---
39.8 J
---
43.1 J
---
84.7 J
ND
25-Feb-14
5.0
100
---
---
5.6 J
15.3 J
---
52.7 J
---
38.0 J
---
48.0 J
---
77.0 J
ND
13-Aug-14
5.0
100
---
---
ND
19.0 J
---
28.4 J
---
37.7 J
---
49.6 J
---
92.6 J
ND
12-Mar-15
2.5
100
---
---
12.4 J
13.3 J
---
28.0 J
---
38.6 J
---
38.9 J
---
93.1 J
ND
19-Aug-15
2.5
100
---
---
4.9 J
17.5 J
---
25.3 J
---
36.2 J
---
42.2 J
---
90.5 J
ND
18-Feb-16
2.5
100
---
---
4.4 J
12.1 J
---
15.7 J
---
36.4 J
---
36.7 J
---
98.2 J
ND
11-Aug-16
2.5
100
---
---
3.9 J
22.4 J
---
16.1 J
---
42.1 J
---
38.6 J
---
102
ND
15-Feb-17
2.5
100
---
---
6.1 J
18.2 J
---
18.6 J
---
37.2 J
---
38.9 J
---
102
ND
24-Aug-17
2.5
100
---
---
11.1 J
18.0 J
---
17.1 J
---
30.9 J
---
43.1 J
---
96.2 J
ND
7-Feb-18
2.5
100
---
---
3.9 J
15.4 J
---
18.0 J
---
44.6 J
---
48.7 J
---
122
ND
15-Aug-18
2.5
100
---
---
3.8 J
21.7 J
---
16.6 J
---
39.9 J
---
41.6 J
---
108
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 Page 3 of 22

TABLE C-02: Historical Detected Inorganic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-1A
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Beryllium
14-Sep-94
---
2
ND
ND
---
ND
ND
---
200
---
ND
---
ND
---
---
2-Dec-94
---
2
2.0
ND
---
ND
4.0
---
2.0
---
ND
---
ND
---
---
8-Feb-95
---
2
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
2-Mar-95
---
2
ND
ND
---
ND
6.0
---
7.0
---
ND
---
ND
---
---
17-Nov-95
---
2
ND
ND
---
ND
2.0
---
7.0
---
ND
---
ND
---
---
23-May-96
---
2
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
14-Nov-96
---
2
1.0
2.0
---
ND
2.0
---
2.0
---
ND
---
ND
---
---
18-Jun-97
---
2
5.0
14.0
---
3.0
7.0
---
13.0
---
ND
---
3.0
---
---
2-Dec-97
---
2
1.0
2.0
---
ND
2.0
---
5.0
---
ND
---
1.0
---
---
27-May-98
---
2
7.0
4.0
---
2.0
8.0
---
10.0
---
ND
---
3.0
---
---
16-Nov-98
---
2
9.0
5.0
---
2.0
5.0
---
4.0
---
ND
---
4.0
---
---
10-Sep-99
---
2
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
16-Nov-99
---
2
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
---
2
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
26-Oct-00
---
2
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
---
2
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Oct-01
---
2
---
ND
---
ND
---
ND
---
ND
---
ND
---
4.0
---
10-Jun-02
---
2
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
13-Jun-02
---
2
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
19-Nov-02
---
2
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Jun-03
---
2
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
30-Dec-03
---
2
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
30-Jun-04
---
2
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
---
2
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Jun-05
---
2
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
---
2
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Jun-06
---
2
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Dec-06
---
1
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Jul-07
---
1
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
GWPS = 4 µg/L (10/23/07)
19-Dec-07
---
1
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
8-Jul-08
---
1.0
---
65.2
---
0.14 J
---
0.10 J
---
ND
---
ND
---
ND
ND
16-Dec-08
0.10
1.0
---
0.21 J
---
ND
---
ND
---
ND
---
0.18 J
---
ND
ND
8-Jul-09
0.10
1.0
---
4.9
---
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Dec-09
0.10
1.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
23-Jun-10
0.10
1.0
---
1.3
---
ND
---
ND
---
ND
---
ND
---
ND
ND
GWPS = 4 µg/L (10/01/10)
14-Dec-10
0.10
1.0
---
---
---
ND
---
{ND)
---
{ND)
---
{ND)
---
ND
ND {0.15) J
21-Jun-11
1.0
1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Dec-11
1.0
1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Jun-12
1.0
1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
11-Dec-12
1.0
1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Apr-13
1.0
1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug-13
1.0
1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
25-Feb-14
1.0
1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
1.0
1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Mar-15
0.50
1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
19-Aug-15
0.50
1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
18-Feb-16
0.50
1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
11-Aug-16
0.50
1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Feb-17
0.50
1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
24-Aug-17
0.50
1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
7-Feb-18
0.50
1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Aug-18
0.50
1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 Page 4 of 22

TABLE C-02: Historical Detected Inorganic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-1A
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Cadmium
14-Sep-94
---
1
ND
ND
---
ND
2.0
---
4.0
---
ND
---
1.0
---
---
2-Dec-94
---
1
ND
ND
---
ND
1.0
---
ND
---
ND
---
ND
---
---
8-Feb-95
---
1
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
2-Mar-95
---
1
ND
ND
---
ND
1.0
---
1.0
---
ND
---
ND
---
---
17-Nov-95
---
1
ND
ND
---
ND
1.0
---
ND
---
ND
---
ND
---
---
23-May-96
---
1
ND
ND
---
ND
1.0
---
ND
---
ND
---
ND
---
---
14-Nov-96
---
1
ND
ND
---
ND
1.0
---
ND
---
ND
---
ND
---
---
18-Jun-97
---
1
ND
ND
---
ND
2.0
---
1.0
---
ND
---
3.0
---
---
2-Dec-97
---
1
ND
ND
---
ND
ND
---
2.0
---
ND
---
ND
---
---
27-May-98
---
1
ND
ND
---
ND
1.0
---
ND
---
ND
---
1.0
---
---
16-Nov-98
---
1
2.0
ND
---
ND
2.0
---
1.0
---
ND
---
4.0
---
---
10-Sep-99
---
1
ND
ND
---
ND
---
1.0
---
ND
---
ND
---
ND
---
16-Nov-99
---
1
2.0
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
---
1
ND
ND
---
ND
---
ND
---
ND
---
ND
---
1.0
---
26-Oct-00
---
1
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
---
1
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Oct-01
---
1
---
ND
---
2.0
---
2.0
---
ND
---
ND
---
2.0
---
10-Jun-02
---
1
---
ND
---
ND
---
3.0
---
ND
---
ND
---
3.0
---
13-Jun-02
---
1
---
ND
---
ND
---
3.0
---
ND
---
ND
---
3.0
---
19-Nov-02
---
1
---
4.0
---
3.0
---
2.0
---
ND
---
1.0
---
ND
---
27-Jun-03
---
1
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
30-Dec-03
---
1
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
30-Jun-04
---
1
---
ND
---
ND
---
1.0
---
ND
---
ND
---
ND
ND
29-Dec-04
---
1
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Jun-05
---
1
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
---
1
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Jun-06
---
1
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Dec-06
---
1
---
0.90 J
---
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Jul-07
---
1
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
NC 2L = 1.75 µg/L (10/23/07)
19-Dec-07
---
1
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
8-Jul-08
---
1.0
---
213#
---
ND
---
ND
---
ND
---
ND
---
ND
ND
16-Dec-08
0.50
1.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
8-Jul-09
0.50
1.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Dec-09
0.50
1.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
23-Jun-10
0.50
1.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
14-Dec-10
0.50
1.0
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
21-Jun-11
1.0
1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Dec-11
1.0
1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Jun-12
1.0
1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
11-Dec-12
1.0
1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Apr-13
1.0
1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug-13
1.0
1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
25-Feb-14
1.0
1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
1.0
1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Mar-15
0.50
1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
19-Aug-15
0.50
1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
18-Feb-16
0.50
1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
11-Aug-16
0.50
1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Feb-17
0.50
1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
24-Aug-17
0.50
1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
7-Feb-18
0.50
1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Aug-18
0.50
1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 Page 5 of 22

TABLE C-02: Historical Detected Inorganic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-1A
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Chromium
14-Sep-94
---
10
74.0
74.0
---
91.0
340
---
457
---
ND
---
177
---
---
2-Dec-94
---
10
93.0
ND
---
88.0
106
---
18.0
---
ND
---
24.0
---
---
8-Feb-95
---
10
ND
48.0
---
56.0
87.0
---
15.0
---
ND
---
19.0
---
---
2-Mar-95
---
10
ND
41.0
---
66.0
313
---
79.0
---
ND
---
10
---
---
17-Nov-95
---
10
130.0
11.0
---
53.0
92.0
---
79.0
---
ND
---
ND
---
---
23-May-96
---
10
71.0
ND
---
34.0
51.0
---
11.0
---
ND
---
ND
---
---
14-Nov-96
---
10
3.0
6.0
---
8.0
11.0
---
4.0
---
ND
---
8.0
---
---
18-Jun-97
---
10
470
340
---
100
270
---
100
---
10.0
---
83.0
---
---
2-Dec-97
---
10
17.0
8.0
---
14.0
ND
---
18.0
---
5.0
---
26.0
---
---
27-May-98
---
10
470
150
---
31.0
190
---
69.0
---
6.0
---
40.0
---
---
16-Nov-98
---
10
1000
220
---
130
190
---
44.0
---
4.0
---
260
---
---
10-Sep-99
---
10
23.0
ND
---
ND
---
40.0
---
ND
---
ND
---
23.0
---
16-Nov-99
---
10
28.0
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
---
10
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
26-Oct-00
---
10
16.0
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
---
10
---
ND
---
ND
---
13.0
---
ND
---
ND
---
ND
---
27-Oct-01
---
10
---
ND
---
16.0
---
56.0
---
10
---
ND
---
ND
---
10-Jun-02
---
10
---
ND
---
ND
---
13.0
---
ND
---
ND
---
ND
---
13-Jun-02
---
10
---
ND
---
ND
---
17.0
---
ND
---
ND
---
ND
---
19-Nov-02
---
10
---
12.0
---
12.0
---
ND
---
ND
---
ND
---
ND
---
27-Jun-03
---
10
---
ND
---
13.0
---
ND
---
ND
---
37.0
---
ND
---
30-Dec-03
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
30-Jun-04
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Jun-05
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Jun-06
---
10
---
ND
---
ND
---
67.0
---
ND
---
ND
---
ND
ND
28-Dec-06
---
10
---
2.8 J
---
8.9 J
---
ND
---
ND
---
ND
---
ND
ND
12-Jul-07
---
10
---
3.3 J
---
ND
---
ND
---
ND
---
ND
---
ND
ND
NC 2L = 50 µ 7
1 -Dec- 7
---
1
---
---
---
2.4 1
---
2.5 J
---
ND
---
2.4 J
---
ND
ND
8-Jul-08
---
10.0
---
488#
---
8.0 1
---
2.8 1
---
ND
---
1.8 J
---
ND
ND
6-Dec-08
0.40
10.0
---
1.5 J
---
2.0 J
---
3.2 J
---
ND
---
1.9 J
---
ND
ND
8-Jul-09
0.40
10.0
---
22.1
---
3.3 1
---
7.2 J
---
ND
---
0.86 J
---
ND
ND
15-Dec-09
0.40
10.0
---
0.60 J
---
4.6 J
---
3.6 J
---
ND
---
0.64 J
---
ND
ND
NC 2L = 10 µ L 2 5 10
23-Jun-10
0.40
10.0
---
12.0
---
4.1 J
---
2.6 B
---
0.90 B
---
1.3 B
---
1.1 B
0.71 J
Resample >
12-Aug-10
0.40
10.0
---
87.8# J
---
---
---
---
---
---
---
---
---
---
ND
14-Dec-10
0.40
10.0
---
---
---
2.8 1
---
9.1 J
---
1.0 1
---
1.2 J
---
0.43 1
ND
21-Jun-11
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Dec-11
5.0
10.0
---
---
ND
ND
---
11.6
---
ND
---
ND
---
ND
ND
Resample >
25-Jan-12
5.0
10.0
---
---
---
---
---
6.1 J
---
---
---
---
---
---
ND
13-Jun-12
5.0
10.0
---
---
ND
5.1 J
---
7.5 J
---
ND
---
ND
---
ND
ND
11-Dec-12
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Apr-13
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug-13
5.0
10.0
---
---
ND
7.4 J
---
ND
---
ND
---
ND
---
ND
ND
25-Feb-14
5.0
10.0
---
---
ND
ND
---
19.6
---
ND
---
ND
---
ND
ND
13-Aug-14
5.0
10.0
---
---
ND
6.1 J
---
6.6 J
---
ND
---
ND
---
ND
ND
12-Mar-15
2.5
10.0
---
---
ND
3.3 1
---
10.6
---
ND
---
ND
---
ND
ND
19-Aug-15
2.5
10.0
---
---
ND
5.9 J
---
7.5 J
---
ND
---
ND
---
ND
ND
18-Feb-16
2.5
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
11-Aug-16
2.5
10.0
---
---
3.4 J
11.0
---
3.1 J
---
2.7 J
---
ND
---
ND
ND
15-Feb-17
2.5
10.0
---
---
ND
6.8 1
---
2.9 J
---
ND
---
3.1 1
---
ND
ND
24-Aug-17
2.5
10.0
---
---
ND
7.6 J
---
ND
---
ND
---
ND
---
ND
ND
7-Feb-18
2.5
10.0
---
---
ND
5.1 1
---
ND
---
ND
---
ND
---
ND
ND
15-Aug-18
2.5
10.0
---
---
ND
12.5
---
3.2 J
---
ND
---
ND
---
ND
ND
Resample >
2-Nov-18
2.5
10.0
---
---
---
4.1 1
---
---
---
---
---
---
---
---
---
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 Page 6 of 22

TABLE C-02: Historical Detected Inorganic Constituents in Compliance Wells
Analyte
Sample Collection Date
DI, RL
MW-1
MW-1A
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Cobalt
14-Sep-94
---
10
160
160
---
ND
250
---
2810
---
ND
---
ND
---
---
2-Dec-94
---
10
47.0
ND
---
53.0
133
---
31.0
---
ND
---
ND
---
---
8-Feb-95
---
10
ND
45.0
---
ND
158
---
42.0
---
ND
---
23.0
---
---
2-Mar-95
---
10
ND
35.0
---
22.0
258
---
89.0
---
ND
---
24.0
---
---
17-Nov-95
---
10
58.0
13.0
---
31.0
86.0
---
76.0
---
ND
---
15.0
---
---
23-May-96
---
10
29.0
ND
---
19.0
88.0
---
34.0
---
ND
---
16.0
---
---
14-Nov-96
---
10
12.0
93.0
---
55.0
120
---
90.0
---
2.0
---
16.0
---
---
18-Jun-97
---
10
200
430
---
52.0
520
---
550
---
4.0
---
28.0
---
---
---
6.0
---
14.0
---
---
27-May-98
---
10
150
73.0
---
13.0
180
---
350
---
4.0
---
18.0
---
---
---
12.0
---
45.0
---
---
10-Sep-99
---
10
11.0
ND
---
ND
---
32.0
---
ND
---
ND
---
ND
---
16-Nov-99
---
10
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
---
10
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
26-Oct-00
---
10
10.0
ND
---
15.0
---
11.0
---
ND
---
ND
---
ND
---
18-Apr-01
---
10
---
17.0
---
ND
---
21.0
---
ND
---
ND
---
ND
---
27-Oct-01
---
10
---
ND
---
ND
---
28.0
---
ND
---
ND
---
ND
---
10-Jun-02
---
10
---
ND
---
11.0
---
15.0
---
ND
---
ND
---
ND
---
13-Jun-02
---
10
---
ND
---
11.0
---
15.0
---
ND
---
ND
---
ND
---
19-Nov-02
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Jun-03
---
10
---
ND
---
12.0
---
ND
---
ND
---
ND
---
ND
---
30-Dec-03
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
30-Jun-04
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
---
10
---
ND
---
12.0
---
ND
---
ND
---
ND
---
ND
ND
29-Jun-05
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
---
10
---
ND
---
11.0
---
ND
---
ND
---
ND
---
ND
ND
28-Jun-06
---
10
---
ND
---
ND
---
21.3
---
ND
---
ND
---
ND
ND
28-Dec-06
---
10
---
2.1 J
---
16.4
---
ND
---
ND
---
ND
---
ND
ND
12-Jul-07
---
10
---
ND
---
11.2
---
ND
---
ND
---
ND
---
ND
ND
WP = 70 µ 7
1 -Dec- 7
---
1
---
---
---
17.0
---
4.6 B
---
1.1 B
---
1.4 B
---
ND
1.6 J
8-Jul-08
---
10.0
---
436#
---
15.0 B
---
4.2 B
---
3.1 B
---
5.0 B
---
6.1 B
6.2 J
16-Dec-08
0.60
10.0
---
2.5 B
---
11.0
---
3.2 B
---
1.4 B
---
3.1 B
---
2.5 B
2.4 J
8-Jul-09
0.60
10.0
---
8.1 J
---
10.6
---
ND
---
ND
---
ND
---
ND
ND
15-Dec-09
0.60
10.0
---
ND
---
8.8 J
---
ND
---
ND
---
ND
---
ND
ND
23-Jun-10
0.60
10.0
---
3.9 J
---
11.8
---
ND
---
ND
---
ND
---
ND
ND
Resample >
12-Aug-10
0.60
10.0
---
---
---
---
---
---
---
---
---
---
---
---
ND
GWPS = 1 µg/L (10/01/10)
14-Dec-10
0.60
10.0
---
---
---
10.9
---
3.7 B
---
ND
---
3.1 B
---
0.71 B
1.6 J
21-Jun-11
5.0
10.0
---
---
ND
11.6
---
ND
---
ND
---
ND
---
ND
ND
6-Dec-11
5.0
10.0
---
---
5.0 J
9.3 J
---
ND
---
ND
---
ND
---
ND
ND
13-Jun-12
5.0
10.0
---
---
ND
10.7
---
ND
---
ND
---
ND
---
ND
ND
11-Dec-12
5.0
10.0
---
---
ND
10.1
---
ND
---
ND
---
ND
---
ND
ND
29-Apr-13
5.0
10.0
---
---
ND
13.0
---
ND
---
ND
---
ND
---
5.1 J
ND
6-Aug-13
5.0
10.0
---
---
ND
20.5
---
ND
---
ND
---
ND
---
ND
ND
25-Feb-14
5.0
10.0
---
---
ND
13.9
---
11.4
---
ND
---
ND
---
ND
ND
13-Aug-14
5.0
10.0
---
---
ND
9.5 J
---
ND
---
ND
---
ND
---
ND
ND
12-Mar-15
2.5
10.0
---
---
ND
8.0 J
---
ND
---
ND
---
ND
---
ND
ND
19-Aug-15
2.5
10.0
---
---
ND
11.8
---
ND
---
ND
---
ND
---
ND
ND
18-Feb-16
2.5
10.0
---
---
ND
7.5 J
---
ND
---
ND
---
ND
---
ND
ND
11-Aug-16
2.5
10.0
---
---
ND
12.7
---
ND
---
ND
---
ND
---
ND
ND
15-Feb-17
2.5
10.0
---
---
ND
11.3
---
ND
---
ND
---
ND
---
ND
ND
24-Aug-17
2.5
10.0
---
---
ND
14.1
---
ND
---
ND
---
ND
---
ND
ND
7-Feb-18
2.5
10.0
---
---
ND
6.5 J
---
ND
---
ND
---
ND
---
ND
ND
15-Aug-18
2.5
10.0
---
---
ND
11.6
---
ND
---
ND
---
ND
---
ND
ND
2-Nov-18
2.5
10.0
---
---
---
8.3 J
---
---
---
---
---
---
---
---
---
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 Page 7 of 22

TABLE C-02: Historical Detected Inorganic Constituents in Compliance Wells
Analyte
Sample Collection Date
DI, RL
MW-1
MW-1A
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Copper
14-Sep-94
---
200
260
260
---
130
340
---
4780
---
ND
---
ND
---
---
2-Dec-94
---
200
ND
ND
---
ND
237
---
ND
---
ND
---
ND
---
---
8-Feb-95
---
200
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
2-Mar-95
---
200
ND
ND
---
ND
270
---
545
---
ND
---
ND
---
---
17-Nov-95
---
200
ND
ND
---
ND
ND
---
456
---
ND
---
ND
---
---
23-May-96
---
200
ND
ND
---
ND
ND
---
ND
---
200
---
ND
---
---
14-Nov-96
---
200
10.0
31.0
---
54.0
17.0
---
60.0
---
12.0
---
15.0
---
---
18-Jun-97
---
200
96.0
340
---
97.0
310
---
660
---
170
---
45.0
---
---
2-Dec-97
---
200
10.0
13.0
---
24.0
26
---
210
---
130
---
17.0
---
---
27-May-98
---
200
84.0
100
---
26.0
300
---
400
---
91.0
---
28.0
---
---
16-Nov-98
---
200
280
320
---
150
290
---
400
---
320
---
80.0
---
---
10-Sep-99
---
200
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
16-Nov-99
---
200
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
---
200
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
26-Oct-00
---
200
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
---
200
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Oct-01
---
200
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
13-Jun-02
---
200
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
19-Nov-02
---
200
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Jun-03
---
200
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
30-Dec-03
---
200
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
30-Jun-04
---
200
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
---
200
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Jun-05
---
200
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
---
200
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Jun-06
---
200
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Dec-06
---
10
---
1.7 B
---
3.5 1
---
1.7 B
---
2.5 B
---
0.90 B
---
ND
0.60 J
12-Jul-07
---
10
---
ND
---
ND
---
2.0 J
---
ND
---
ND
---
ND
ND
NC 2L = 1,000 µ L (10 23 07)
19-Dec-07
---
10
---
---
---
4.6 B
---
3.8 B
---
0.56 B
---
1.9 B
---
0.58 B
10.5 B
8-Jul-08
---
10.0
---
828#
---
9.3 J
---
1.6 J
---
ND
---
ND
---
0.75 J
ND
16-Dec-08
0.30
10.0
---
2.0 J
---
2.1 1
---
2.3 1
---
ND
---
6.9 J
---
ND
ND
8-Jul-09
0.30
10.0
---
32.7
---
1.6 J
---
3.3 J
---
ND
---
ND
---
ND
ND
15-Dec-09
0.30
10.0
---
0.79 J
---
2.9 1
---
2.7 J
---
ND
---
2.1 J
---
ND
ND
23-Jun-10
0.30
10.0
---
23.2
---
2.0 J
---
1.1 J
---
ND
---
0.86 J
---
ND
ND
Resample >
12-Aug-10
0.30
10.0
---
---
---
---
---
---
---
---
---
---
---
---
ND
14-Dec-10
0.30
10.0
---
---
---
1.8 B
---
8.1 J
---
0.39 B
---
5.9 J
---
ND
0.49 J
21-Jun-11
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Dec-11
5.0
10.0
---
---
15.5
ND
---
10.0
---
ND
---
ND
---
ND
ND
13-Jun-12
5.0
10.0
---
---
ND
ND
---
5.6 J
---
ND
---
ND
---
ND
ND
11-Dec-12
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Apr-13
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug-13
5.0
10.0
---
---
ND
6.6 J
---
ND
---
ND
---
ND
---
ND
ND
25-Feb-14
5.0
10.0
---
---
ND
ND
---
14.7
---
ND
---
6.4 J
---
ND
ND
13-Aug-14
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Mar-15
2.5
10.0
---
---
ND
ND
---
7.6 J
---
ND
---
ND
---
ND
ND
19-Aug-15
2.5
10.0
---
---
ND
5.0 J
---
6.8 J
---
ND
---
ND
---
ND
ND
18-Feb-16
2.5
10.0
---
---
ND
ND
---
3.6 J
---
ND
---
ND
---
ND
ND
11-Aug-16
2.5
10.0
---
---
ND
7.8 J
---
ND
---
ND
---
ND
---
ND
ND
15-Feb-17
2.5
10.0
---
---
ND
6.3 J
---
ND
---
ND
---
ND
---
ND
ND
24-Aug-17
2.5
10.0
---
---
5.1 J
3.7 J
---
ND
---
ND
---
ND
---
ND
ND
7-Feb-18
2.5
10.0
---
---
ND
10.0
---
3.4 1
---
ND
---
ND
---
ND
ND
15-Aug-18
2.5
10.0
---
---
ND
7.4 J
---
2.8 J
---
ND
---
ND
---
ND
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 Page 8 of 22

TABLE C-02: Historical Detected Inorganic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-1A
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Iron
23-Jun-10
14.0
300
---
11800
---
4150
---
1040
---
102 J
---
413
---
776
ND
NC 2L = 300 µg/L (2/5/10) Resample >
12-Aug-10
140
3000
---
123,000
---
---
---
---
---
---
---
---
---
---
ND
14-Dec-10
14
300
---
---
---
3210
---
3880
---
141 J
---
877
---
1100
ND
21-Jun-11
50.0
300
---
---
2190
6030
---
667
---
114 J
---
981
---
1020
ND
6-Dec-11
50.0
300
---
---
8610
2680
---
5420
---
86.1 J
---
287 J
---
1040
ND
13-Jun-12
50.0
300
---
---
1770
5610
---
3280
---
63.4 J
---
698
---
1680
ND
11-Dec-12
50.0
300
---
---
1680
4020
---
1260
---
ND
---
545
---
981
ND
29-Apr-13
50.0
300
---
---
414
3500
---
1130
---
112 J
---
635
---
1750
ND
6-Aug-13
50.0
300
---
---
397
8970
---
307
---
ND
---
378
---
2130
ND
25-Feb-14
50.0
300
---
---
1040
7060
---
9750
---
102 J
---
2030
---
1710
ND
13-Aug-14
50.0
300
---
---
209 J
5380
---
3030
---
107 J
---
904
---
2140
ND
12-Mar-15
25.0
300
---
---
269 J
3680
---
6040
---
40.8 J
---
262 J
---
2650
ND
19-Aug-15
25.0
300
---
---
156 J
7250
---
3780
---
34.9 J
---
58.0 J
---
1460
ND
18-Feb-16
25.0
300
---
---
243 J
792
---
270 J
---
43.0 J
---
86.3 J
---
1500
ND
11-Aug-16
25.0
300
---
---
292 J
10400
---
839
---
104.0 J
---
ND
---
2090
ND
15-Feb-17
25.0
300
---
---
633
6250
---
1400
---
104.0 J
---
30.4 J
---
944
ND
24-Aug-17
25.0
300
---
---
3680
9740
---
792
---
46.8 J
---
38.5 J
---
1990
ND
7-Feb-18
25.0
300
---
---
323
6740
---
849
---
126 J
---
61.2 J
---
1060
ND
15-Aug-18
25.0
300
---
---
340
14000
---
1200
---
75.5 J
---
ND
---
1180
27.8 J
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 Page 9 of 22

TABLE C-02: Historical Detected Inorganic Constituents in Compliance Wells
Analyte
Sample Collection Date
DI, RL
MW-1
MW-1A
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Lead
14-Sep-94
---
10
31.0
31.0
---
230
23.0
---
355
---
ND
---
190
---
---
2-Dec-94
---
10
17.0
ND
---
26.0
30.0
---
11.0
---
ND
---
31.0
---
---
8-Feb-95
---
10
ND
13.0
---
23.0
10.0
---
19.0
---
ND
---
15.0
---
---
2-Mar-95
---
10
ND
11.0
---
14.0
27.0
---
47.0
---
ND
---
ND
---
---
17-Nov-95
---
10
ND
ND
---
ND
13.0
---
51.0
---
ND
---
ND
---
---
23-May-96
---
10
ND
ND
---
10.0
ND
---
ND
---
ND
---
ND
---
---
14-Nov-96
---
10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
18-Jun-97
---
10
33.0
69.0
---
21.0
40.0
---
78.0
---
8
---
70.0
---
---
2-Dec-97
---
10
8.0
8.0
---
20.0
14.0
---
21.0
---
11
---
24.0
---
---
27-May-98
---
10
27.0
18.0
---
23.0
31.0
---
32.0
---
ND
---
32.0
---
---
16-Nov-98
---
10
43.0
36.0
---
33.0
34.0
---
32.0
---
ND
---
110
---
---
10-Sep-99
---
10
ND
18.0
---
ND
---
14.0
---
ND
---
ND
---
ND
---
16-Nov-99
---
10
11.0
ND
---
ND
---
ND
---
ND
---
11.0
---
ND
---
10-May-00
---
10
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
26-Oct-00
---
10
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Oct-01
---
10
---
ND
---
28.0
---
15.0
---
ND
---
18.0
---
29.0
---
10-Jun-02
---
10
---
ND
---
13.0
---
ND
---
ND
---
ND
---
ND
---
13-Jun-02
---
10
---
ND
---
13.0
---
ND
---
ND
---
ND
---
ND
---
19-Nov-02
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Jun-03
---
10
---
ND
---
ND
---
ND
---
ND
---
10.0
---
ND
---
30-Dec-03
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
30-Jun-04
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Jun-05
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Jun-06
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Dec-06
---
10
---
ND
---
2.0 J
---
ND
---
ND
---
ND
---
ND
ND
12-Jul-07
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
NC 2L = 5 µ 7
1 -Dec- 7
---
1
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
8-Jul-08
---
10.0
---
78#
---
ND
---
ND
---
ND
---
ND
---
ND
ND
16-Dec-08
4.0
10.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
8-Jul-09
4.0
10.0
---
22.5
---
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Dec-09
4.0
10.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
23-Jun-10
4.0
10.0
---
6.7 J
---
ND
---
ND
---
ND
---
ND
---
ND
ND
14-Dec-10
4.0
10.0
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
21-Jun-11
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Dec-11
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Jun-12
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
11-Dec-12
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Apr-13
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug-13
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
25-Feb-14
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Mar-15
2.5
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
19-Aug-15
2.5
10.0
---
---
ND
2.9 J
---
ND
---
ND
---
ND
---
ND
ND
18-Feb-16
2.5
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
11-Aug-16
2.5
10.0
---
---
ND
2.7 J
---
ND
---
ND
---
ND
---
ND
ND
15-Feb-17
2.5
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
24-Aug-17
2.5
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
7-Feb-18
2.5
10.0
---
---
ND
2.8 J
---
ND
---
ND
---
ND
---
ND
ND
15-Aug-18
2.5
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 Page 10 of 22

TABLE C-02: Historical Detected Inorganic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-1A
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Mercury
17-Nov-95
---
0.5
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
2-Dec-97
---
0.5
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
23-Mar-98
---
0.5
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
27-May-98
---
0.5
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
16-Nov-98
---
0.5
ND
ND
---
ND
1.0
---
ND
---
ND
---
ND
---
---
10-Sep-99
---
0.5
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
16-Nov-99
---
0.5
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
---
0.5
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
26-Oct-00
---
0.5
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
---
0.5
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Oct-01
---
---
---
---
---
---
---
---
---
---
---
---
---
---
---
10-Jun-02
---
0.5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
13-Jun-02
---
0.5
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
19-Nov-02
---
---
---
---
---
---
---
---
---
---
---
---
---
---
---
27-Jun-03
---
1.5
---
ND
---
ND
---
ND
---
ND
---
0.78
---
ND
---
30-Dec-03
---
0.5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
30-Jun-04
---
0.5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
---
0.5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Jun-05
---
0.5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
---
0.5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Jun-06
---
2
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Dec-06
---
0.2
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Jul-07
---
0.2
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
NC 2L = 1.05 µg/L (10/23/07)
19-Dec-07
---
0.2
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
8-Jul-08
---
0.20
---
0.34#
---
ND
---
ND
---
ND
---
ND
---
ND
ND
16-Dec-08
0.090
0.20
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
8-Jul-09
0.070
0.20
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Dec-09
0.070
0.20
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
NC 2L = 1 µg/L (2/5/10)
23-Jun-10
0.070
0.20
---
ND
---
ND
---
ND
---
0.094 J
---
ND
---
ND
ND
14-Dec-10
0.070
0.20
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
21-Jun-11
0.10
0.20
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Dec-11
0.10
0.20
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Jun-12
0.10
0.20
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
11-Dec-12
0.10
0.20
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Apr-13
0.10
0.20
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug-13
0.10
0.20
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
25-Feb-14
0.10
0.20
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
0.10
0.20
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Mar-15
0.10
0.20
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
19-Aug-15
0.10
0.20
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
18-Feb-16
0.10
0.20
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
11-Aug-16
0.10
0.20
---
---
ND
0.11 J
---
ND
---
ND
---
ND
---
ND
ND
15-Feb-17
0.10
0.20
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
24-Aug-17
0.10
0.20
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
7-Feb-18
0.10
0.20
---
---
ND
0.11 J
---
ND
---
ND
---
ND
---
ND
ND
15-Aug-18
0.10
0.20
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 Page 11 of 22

TABLE C-02: Historical Detected Inorganic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-1A
MW-7
MW-2
MW-3
MW-311
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Manganese
23-Jun-10
0.30
50.0
---
88.3
---
217
---
44.0 B
---
513
---
127
---
1470
9.0 J
NC 2L = 50 µg/L (2/5/l0) Resample>
12-Aug-10
3.00
500
---
972
---
---
---
---
---
---
---
---
---
---
0.35 J
14-Dec-10
0.30
50.0
---
---
---
208
---
139
---
730
---
194
---
1260
1.1 J
21-Jun-11
5.0
50.0
---
---
38.2 J
245
---
36.9 J
---
833
---
130
---
1400
ND
6-Dec-11
5.0
50.0
---
---
198
216
---
170
---
808
---
187
---
1350
ND
13-Jun-12
5.0
50.0
---
---
41.7 J
226
---
95.8
---
760
---
125
---
1360
ND
11-Dec-12
5.0
50.0
---
---
33.8 J
230
---
28.9 J
---
770
---
279
---
1340
ND
29-Apr-13
5.0
50.0
---
---
14.2 J
193
---
47.3 J
---
724
---
139
---
1220
ND
6-Aug-13
5.0
50.0
---
---
10.3 J
273
---
38.5 J
---
749
---
135
---
1220
ND
25-Feb-14
5.0
50.0
---
---
29.8 J
222
---
340
---
897
---
154
---
862
ND
13-Aug-14
5.0
50.0
---
---
5.8 J
209
---
108
---
1230
---
125
---
1450
ND
12-Mar-15
2.5
50.0
---
---
6.0 J
210
---
200
---
676
---
104
---
1370
ND
19-Aug-15
2.5
50.0
---
---
4.3 J
288
---
199
---
802
---
103
---
1490
ND
18-Feb-16
2.5
50.0
---
---
5.4 J
201
---
72.7
---
981
---
82.4
---
1620
ND
11-Aug-16
2.5
50.0
---
---
5.9 J
336
---
122
---
1550
---
100.0
---
1770
ND
15-Feb-17
2.5
50.0
---
---
15.5 J
234
---
246
---
1390
---
91.4
---
2210
ND
24-Aug-17
2.5
50.0
---
---
94.7
344
---
116
---
999
---
98.3
---
1730
ND
7-Feb-18
2.5
50.0
---
---
7.6 J
168
---
196
---
1160
---
158
---
2660
ND
15-Aug-18
2.5
50.0
---
---
6.7 J
284
---
63.6
---
937
---
105
---
1870
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 Page 12 of 22

TABLE C-02: Historical Detected Inorganic Constituents in Compliance Wells
Analyte
Sample Collection Date
DI, RL
MW-1
MW-1A
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Nickel
14-Sep-94
---
50
180
18.0
---
ND
250
---
680
---
ND
---
ND
---
---
2-Dec-94
---
50
118
ND
---
119
164
---
ND
---
ND
---
ND
---
---
8-Feb-95
---
50
ND
ND
---
ND
84.0
---
ND
---
ND
---
ND
---
---
2-Mar-95
---
50
ND
ND
---
ND
204
---
75.0
---
ND
---
ND
---
---
17-Nov-95
---
50
71.0
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
23-May-96
---
50
69.0
ND
---
ND
51
---
ND
---
ND
---
ND
---
---
14-Nov-96
---
50
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
18-Jun-97
---
50
330
280
---
65.0
200
---
ND
---
ND
---
ND
---
---
2-Dec-97
---
50
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
27-May-98
---
50
310
88.0
---
ND
170
---
61
---
ND
---
ND
---
---
16-Nov-98
---
50
840
270
---
ND
ND
---
ND
---
ND
---
150
---
---
10-Sep-99
---
50
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
16-Nov-99
---
50
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
---
50
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
26-Oct-00
---
50
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
---
50
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Oct-01
---
50
---
ND
---
ND
---
59
---
ND
---
ND
---
ND
---
10-Jun-02
---
50
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
13-Jun-02
---
50
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
19-Nov-02
---
50
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Jun-03
---
50
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
30-Dec-03
---
50
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
30-Jun-04
---
50
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
---
50
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Jun-05
---
50
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
---
50
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Jun-06
---
50
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Dec-06
---
50
---
4.7 J
---
7.0 J
---
7.2 J
---
2.4 J
---
ND
---
ND
ND
12-Jul-07
---
50
---
4.6 J
---
3.2 1
---
2.5 J
---
ND
---
ND
---
ND
ND
NC 2L = 100 µg/L (10/23/07)
19-Dec-07
---
50
---
---
---
3.2 J
---
5.0
---
ND
---
2.3 J
---
ND
ND
8-Jul-08
---
50.0
---
122 J
---
5.3 1
---
2.3 J
---
ND
---
1.7 J
---
ND
ND
16-Dec-08
1.7
50.0
---
ND
---
2.3 B
---
2.5 B
---
ND
---
2.7 B
---
ND
2.4 J
8-Jul-09
1.7
50.0
---
38.6 J
---
3.2 J
---
6.0 J
---
ND
---
1.8 J
---
ND
ND
15-Dec-09
1.7
50.0
---
ND
---
3.6 B
---
4.4 B
---
2.1 B
---
2.6 B
---
2.0 B
3.0 J
23-Jun-10
1.7
50.0
---
10 J
---
2.3 J
---
ND
---
ND
---
ND
---
ND
ND
14-Dec-10
1.7
50.0
---
---
---
1.8 B
---
2.6 B
---
ND
---
ND
---
ND
2.7 J
21-Jun-11
5.0
50.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Dec-11
5.0
50.0
---
---
ND
ND
---
6.4 J
---
ND
---
ND
---
ND
ND
13-Jun-12
5.0
50.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
11-Dec-12
5.0
50.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Apr-13
5.0
50.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug-13
5.0
50.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
25-Feb-14
5.0
50.0
---
---
ND
ND
---
11.3 J
---
ND
---
ND
---
ND
ND
13-Aug-14
5.0
50.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Mar-15
2.5
50.0
---
---
ND
ND
---
11.7 J
---
ND
---
ND
---
ND
ND
19-Aug-15
2.5
50.0
---
---
ND
3.7 J
---
8.9 J
---
ND
---
ND
---
ND
ND
18-Feb-16
2.5
50.0
---
---
ND
ND
---
3.2 J
---
ND
---
ND
---
ND
ND
11-Aug-16
2.5
50.0
---
---
ND
6.4 J
---
6.7 J
---
ND
---
ND
---
22.8 J
ND
15-Feb-17
2.5
50.0
---
---
ND
4.9 J
---
8.8 J
---
ND
---
ND
---
ND
ND
24-Aug-17
2.5
50.0
---
---
3.3 J
5.6 J
---
4.6 J
---
ND
---
ND
---
ND
ND
7-Feb-18
2.5
50.0
---
---
ND
ND
---
4.8 J
---
ND
---
ND
---
ND
ND
15-Aug-18
2.5
50.0
---
---
ND
5.5 J
---
3.4 J
---
ND
---
ND
---
ND
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 Page 13 of 22

TABLE C-02: Historical Detected Inorganic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-1A
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Selenium
14-Sep-94
---
20
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
2-Dec-94
---
20
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
8-Feb-95
---
20
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
2-Mar-95
---
20
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
17-Nov-95
---
20
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
23-May-96
---
20
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
14-Nov-96
---
20
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
18-Jun-97
---
20
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
2-Dec-97
---
20
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
27-May-98
---
20
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
16-Nov-98
---
20
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
10-Sep-99
---
20
ND
24.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
16-Nov-99
---
20
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
---
20
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
26-Oct-00
---
20
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
---
20
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Oct-01
---
20
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
13-Jun-02
---
20
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
19-Nov-02
---
20
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Jun-03
---
20
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
30-Dec-03
---
20
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
30-Jun-04
---
20
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
---
20
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Jun-05
---
20
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
---
20
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Jun-06
---
20
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Dec-06
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Jul-07
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
NC 2L = 50 µ L 10 23 07
19-Dec-07
---
10
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
8-Jul-08
---
10.0
---
ND#
---
ND
---
ND
---
ND
---
ND
---
ND
ND
16-Dec-08
3.8
10.0
---
4.2 B
---
ND
---
ND
---
ND
---
ND
---
ND
4.9 J
8-Jul-09
3.8
10.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Dec-09
3.8
10.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
NC 2L=20 µ 5
-Jun-1
1.
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
14-Dec-10
3.8
10.0
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
21-Jun-11
10.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Dec-11
10.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Jun-12
10.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
11-Dec-12
10.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Apr-13
10.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug-13
10.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
25-Feb-14
10.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
10.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Mar-15
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
19-Aug-15
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
18-Feb-16
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
11-Aug-16
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
6.0 J
ND
15-Feb-17
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
24-Aug-17
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
7-Feb-18
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Aug-18
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 Page 14 of 22

TABLE C-02: Historical Detected Inorganic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-1A
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Silver
14-Sep-94
---
10
ND
ND
---
ND
ND
---
50.0
---
ND
---
ND
---
---
2-Dec-94
---
10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
8-Feb-95
---
10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
2-Mar-95
---
10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
17-Nov-95
---
10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
23-May-96
---
10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
14-Nov-96
---
10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
18-Jun-97
---
10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
2-Dec-97
---
10
ND
ND
---
ND
ND
---
ND
---
ND
---
4.0
---
---
27-May-98
---
10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
16-Nov-98
---
10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
10-Sep-99
---
10
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
16-Nov-99
---
10
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
---
10
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
26-Oct-00
---
10
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Oct-01
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
13-Jun-02
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
19-Nov-02
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Jun-03
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
30-Dec-03
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
30-Jun-04
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Jun-05
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Jun-06
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Dec-06
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Jul-07
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
NC 2L = 17.5 µg/L (10/23/07)
19-Dec-07
---
10
---
---
---
ND
---
ND
---
0.26 J
---
ND
---
ND
ND
8-Jul-08
---
10.0
---
14.6# J
---
0.27 J
---
0.41 J
---
0.83 J
---
0.39 J
---
0.56 J
ND
16-Dec-08
0.10
10.0
---
ND
---
ND
---
0.25 J
---
0.53 J
---
0.40 J
---
0.46 J
ND
8-Jul-09
0.10
10.0
---
0.16 J
---
ND
---
ND
---
0.17 J
---
ND
---
ND
ND
15-Dec-09
0.10
10.0
---
ND
---
ND
---
0.32 J
---
0.64 J
---
0.53 J
---
0.53 J
ND
NC 2L=20 µ 5/10)
23-Jun-10
0.10
1.
---
ND
---
ND
---
ND
---
0.13 J
---
0.13 J
---
ND
ND
{0.25 J}
14-Dec-10
0.10
10.0
---
---
---
ND
---
{0.24} B
---
{0.58} B
---
{0.34} B
---
0.17 B
J
0.19
21-Jun-11
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Dec-11
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Jun-12
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
11-Dec-12
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Apr-13
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug-13
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
25-Feb-14
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Mar-15
2.5
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
19-Aug-15
2.5
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
18-Feb-16
2.5
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
11-Aug-16
2.5
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Feb-17
2.5
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
24-Aug-17
2.5
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
7-Feb-18
2.5
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Aug-18
2.5
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 Page 15 of 22

TABLE C-02: Historical Detected Inorganic Constituents in Compliance Wells
Analyte
Sample Collection Date
DI, RL
MW-1
MW-1A
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Thallium
14-Sep-94
---
10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
2-Dec-94
---
10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
8-Feb-95
---
10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
2-Mar-95
---
10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
17-Nov-95
---
10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
23-May-96
---
10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
14-Nov-96
---
10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
18-Jun-97
---
10
ND
ND
---
ND
ND
---
5.0
---
ND
---
ND
---
---
2-Dec-97
---
10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
27-May-98
---
10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
16-Nov-98
---
10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
10-Sep-99
---
10
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
16-Nov-99
---
10
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
---
10
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
26-Oct-00
---
10
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Oct-01
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
13-Jun-02
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
19-Nov-02
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Jun-03
---
0.01
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
30-Dec-03
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
30-Jun-04
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Jun-05
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Jun-06
---
10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Dec-06
---
6
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Jul-07
---
5.5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
GWPS = 0.28 µg/L (10/23/07)
19-Dec-07
---
5.5
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
8-Jul-08
---
5.5
---
31.7#
---
4.5 J
---
ND
---
ND
---
ND
---
ND
ND
16-Dec-08
3.0
5.5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
8-Jul-09
3.0
5.5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Dec-09
3.0
5.5
---
ND
---
ND
---
ND
---
ND
---
3.8 J
---
ND
ND
23-Jun-10
3.0
5.5
---
6.6
---
ND
---
ND
---
ND
---
ND
---
ND
ND
Resample >
12-Aug-10
30.0
55.0
---
ND#
---
---
---
---
---
---
---
---
---
---
ND
GWPS = 0.2 µg/L (10/01/10)
14-Dec-10
3.0
5.5
---
---
---
ND
---
ND
---
8.1
---
ND
---
ND
ND
21-Jun-11
5.4
5.5
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Dec-11
5.4
5.5
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Jun-12
5.4
5.5
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
11-Dec-12
5.4
5.5
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Apr-13
5.4
5.5
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug-13
5.4
5.5
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
25-Feb-14
5.4
5.5
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
5.4
5.5
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Mar-15
5.0
5.5
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
19-Aug-15
5.0
5.5
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
18-Feb-16
5.0
5.5
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
11-Aug-16
5.0
5.5
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Feb-17
0.02
5.5
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
24-Aug-17
0.02
5.5
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
7-Feb-18
0.028
0.10
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Aug-18
0.020
5.50
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 Page 16 of 22

TABLE C-02: Historical Detected Inorganic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-1A
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Tin
8-Jul-08
---
100
---
232# J
---
1.9 J
---
3.0 J
---
3.0 J
---
3.6 J
---
3.6 J
ND
16-Dec-08
1.8
100
---
---
---
---
---
---
---
---
---
---
---
---
ND
8-Jul-09
1.8
100
---
7.4 J
---
ND
---
ND
---
1.8 J
---
ND
---
ND
ND
15-Dec-09
---
---
---
---
---
---
---
---
---
---
---
---
---
---
---
GWPS = 2100 µ 2 5 10
23-Jun-10
1.8
100
---
2.9 J
---
ND
---
ND
---
1.9 J
---
2.5 J
---
3.3 J
ND
GWPS = 2000 µg/L (10/01/10)
14-Dec-10
---
---
---
---
---
---
---
---
---
---
---
---
---
---
---
21-Jun-11
5.0
100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
N D
6-Dec-11
5.0
100
---
---
---
---
---
---
---
---
---
---
---
---
---
13-Jun-12
5.0
100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
11-Dec-12
---
---
---
---
---
---
---
---
---
---
---
---
---
---
---
29-Apr-13
5.0
100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug-13
---
---
---
---
---
---
---
---
---
---
---
---
---
---
---
25-Feb-14
5.0
100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
---
---
---
---
---
---
---
---
---
---
---
---
---
---
---
12-Mar-15
2.5
100
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
18-Feb-16
2.5
100
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
15-Feb-17
2.5
100
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
24-Aug-17
2.5
100
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
7-Feb-18
2.5
100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 Page 17 of 22

TABLE C-02: Historical Detected Inorganic Constituents in Compliance Wells
Gr;
Analyte
Sample Collection Date
DI, RL
MW-1
MW-1A
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Vanadium
14-Sep-94
---
40
580
580
---
390
540
---
12800
---
ND
---
340
---
---
2-Dec-94
---
40
107
ND
---
233
316
---
201
---
ND
---
ND
---
---
8-Feb-95
---
40
ND
81.0
---
132
162
---
190
---
ND
---
ND
---
---
2-Mar-95
---
40
ND
62.0
---
173
468
---
1260
---
ND
---
ND
---
---
17-Nov-95
---
40
100
ND
---
84.0
120
---
984
---
ND
---
ND
---
---
23-May-96
---
40
92.0
ND
---
103
139
---
196
---
ND
---
ND
---
---
14-Nov-96
---
40
16.0
10.0
---
140
280
---
320
---
10.0
---
22.0
---
---
18-Jun-97
---
40
470
1600
---
310
600
---
1700
---
57.0
---
82.0
---
---
2-Dec-97
---
40
32.0
15.0
---
52.0
120
---
970
---
22.0
---
27.0
---
---
27-May-98
---
40
330
120
---
71.0
460
---
1000
---
34.0
---
41.0
---
---
16-Nov-98
---
40
900
280
---
340
470
---
730
---
49.0
---
97.0
---
---
10-Sep-99
---
40
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
16-Nov-99
---
40
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
---
40
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
26-Oct-00
---
40
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
---
40
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Oct-01
---
40
---
ND
---
67.0
---
53.0
---
ND
---
63.0
---
ND
---
10-Jun-02
---
40
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
13-Jun-02
---
40
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
19-Nov-02
---
40
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Jun-03
---
40
---
ND
---
ND
---
ND
---
ND
---
94.0
---
ND
---
30-Dec-03
---
40
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
30-Jun-04
---
40
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
---
40
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Jun-05
---
40
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
---
40
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Jun-06
---
40
---
ND
---
ND
---
71.1
---
ND
---
ND
---
ND
ND
28-Dec-06
---
25
---
2.2 J
---
28.4
---
ND
---
ND
---
1.8 J
---
ND
ND
12-Jul-07
---
25
---
3.7 J
---
3.4 J
---
2.2 J
---
ND
---
ND
---
ND
ND
GWPS = 3.5 µg/L (10/23/07)
19-Dec-07
---
25
---
---
---
7.6
---
3.2 J
---
1.1 B
---
0.82 B
---
0.93 B
0.51 J
Resample >
14-Feb-08
---
25
---
---
---
7.2
---
---
---
---
---
---
---
---
0.24 J
Filtered >
14-Feb-08
---
25
---
---
---
3.2 J
---
---
---
---
---
---
---
---
ND
8-Jul-08
---
25.0
---
772#
---
21.9 J
---
2.2 J
---
0.94 B
---
0.78 B
---
2.3 J
0.20 J
16-Dec-08
0.20
25.0
---
3.4 J
---
4.9 J
---
3.4 J
---
0.84 B
---
6.1 J
---
0.47 B
0.76 J
8-Ju -09
0.20
25.0
---
39.6
---
10.6 J
---
8.3 J
---
1.7 B
---
1.9 B
---
1.4 B
1.3 J
15-Dec-09
0.20
25.0
---
1.2 B
---
12.1 J
---
3.8 J
---
1.3 B
---
2.3 B
---
ND
0.53 J
23-Jun-10
0.20
25.0
---
18.7 J
---
10.7 J
---
2.0 J
---
0.51 J
---
1.2 J
---
0.54 J
ND
Resample >
12-Aug-10
0.20
25.0
---
---
---
---
---
---
---
---
---
---
---
---
0.33 J
GWPS = 0.3 µg/L (10/01/10)
14-Dec-10
0.20
25.0
---
---
---
7.3 J
---
18.01 J
---
(1.21 B
---
14.01 J
---
ND
40.57 J) 0.36 J
21-Jun-11
5.0
25.0
---
---
5.9 J
14.6 J
---
ND
---
ND
---
ND
---
ND
ND
6-Dec-11
5.0
25.0
---
---
19.8 J
5.3 J
---
10 J
---
ND
---
ND
---
ND
ND
13-Jun-12
5.0
25.0
---
---
5.2 J
13.0 J
---
6.5 J
---
ND
---
ND
---
ND
ND
11-Dec-12
5.0
25.0
---
---
ND
7.4 J
---
ND
---
ND
---
ND
---
ND
ND
29-Apr-13
5.0
25.0
---
---
ND
8.4 J
---
ND
---
ND
---
ND
---
ND
ND
6-Aug-13
5.0
25.0
---
---
ND
27.6
---
ND
---
ND
---
ND
---
ND
ND
25-Feb-14
5.0
25.0
---
---
ND
18.6 J
---
19.0 J
---
ND
---
7.0 J
---
ND
ND
13-Aug-14
5.0
25.0
---
---
ND
15.0 J
---
7.2 J
---
ND
---
ND
---
ND
ND
12-Mar-15
2.5
25.0
---
---
ND
9.5 J
---
14.8 J
---
ND
---
3.3 J
---
ND
ND
19-Aug-15
2.5
25.0
---
---
ND
19.2 J
---
8.3 J
---
ND
---
ND
---
ND
ND
18-Feb-16
2.5
25.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
11-Aug-16
2.5
25.0
---
---
ND
25.2
---
ND
---
ND
---
ND
---
ND
ND
15-Feb-17
2.5
25.0
---
---
ND
13.9 J
---
ND
---
ND
---
ND
---
ND
ND
24-Aug-17
2.5
25.0
---
---
10.3 J
23.7 J
---
ND
---
ND
---
ND
---
ND
ND
WP =0.3 µ 1 1
7-Feb-18
2.5
25.0
---
---
ND
18.1 J
---
2.6 J
---
ND
---
ND
---
ND
ND
15-Aug-18
2.5
25.0
---
---
ND
34.5
---
2.6 J
---
ND
---
ND
---
ND
ND
Resample >
2-Nov-18
2.5
25.0
---
---
---
13.0 J
---
---
---
---
---
---
---
---
---
ing
Permit 3901-CDLF-1997
Page 18 of 22

TABLE C-02: Historical Detected Inorganic Constituents in Compliance Wells
Analyte
Sample Collection Date
DI, RL
MW-1
MW-1A
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Zinc
14-Sep-94
---
50
680
680
---
400
910
---
17,400
---
ND
---
640
---
---
2-Dec-94
---
50
299
ND
---
380
553
---
279
---
ND
---
98.0
---
---
8-Feb-95
---
50
ND
185
---
236
255
---
320
---
156
---
108
---
---
2-Mar-95
---
50
ND
114
---
102
601
---
1,530
---
191
---
ND
---
---
17-Nov-95
---
50
309
67.0
---
154
199
---
1,300
---
59.0
---
ND
---
---
23-May-96
---
50
237
94.0
---
116
237
---
314
---
149
---
ND
---
---
14-Nov-96
---
50
240
180
---
140
120
---
140
---
15.0
---
48.0
---
---
18-Jun-97
---
50
930
800
---
250
650
---
1,800
---
160
---
190
---
---
2-Dec-97
---
50
140
150
---
110
120
---
510
---
150
---
130
---
---
27-May-98
---
50
1,000
280
---
90.0
560
---
1,300
---
100
---
110
---
---
16-Nov-98
---
50
4,300
2,500
---
3,600
5,600
---
7,000
---
230
---
3,900
---
---
10-Sep-99
---
50
153
ND
---
ND
---
96.0
---
ND
---
ND
---
ND
---
16-Nov-99
---
50
140
119
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
---
50
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
26-Oct-00
---
50
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
---
50
---
ND
---
ND
---
64.0
---
ND
---
ND
---
ND
---
27-Oct-01
---
50
---
23.0
---
55.0
---
136.0
---
ND
---
32.0
---
ND
---
10-Jun-02
---
50
---
ND
---
ND
---
72.0
---
ND
---
ND
---
370
---
13-Jun-02
---
50
---
ND
---
ND
---
72.0
---
ND
---
ND
---
370
---
19-Nov-02
---
50
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Jun-03
---
50
---
ND
---
ND
---
ND
---
ND
---
52.0
---
ND
---
30-Dec-03
---
50
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
30-Jun-04
---
50
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
---
50
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Jun-05
---
50
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
---
50
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Jun-06
---
50
---
ND
---
ND
---
126
---
ND
---
ND
---
ND
ND
28-Dec-06
---
10
---
7.7 J
---
14.0
---
7.8 J
---
ND
---
ND
---
1.5 J
ND
12-Jul-07
---
10
---
48.1
---
3.6 J
---
6.5 J
---
ND
---
ND
---
ND
ND
NC 2L = 1,050 µg/L (10/23/07)
19-Dec-07
---
10
---
---
---
0.4 B
---
ND
---
4.5 B
---
ND
---
ND
87.9
8-Jul-08
---
10.0
---
4,540#
---
12.6
---
ND
---
ND
---
ND
---
ND
1.2 J
16-Dec-08
0.40
10.0
---
9.6 J
---
0.45 J
---
3.8 J
---
ND
---
12.3
---
ND
ND
8-Jul-09
0.40
10.0
---
169
---
0.67 J
---
7.0 J
---
ND
---
ND
---
ND
1.6 J
15-Dec-09
0.40
10.0
---
6.6 B
---
5.5 B
---
6.9 B
---
ND
---
1.9 B
---
ND
7.7 J
NC 2L = 1,000 µ L (2 5 10)
23-Jun-10
0.40
10.0
---
55.2
---
2.2 J
---
1.0 J
---
ND
---
ND
---
ND
ND
14-Dec-10
0.40
10.0
---
---
---
16.3 B
---
12.6 B
---
ND
---
ND
---
2.6 B
6.7 J
21-Jun-11
10.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Dec-11
10.0
10.0
---
---
21.8 B
ND
---
21.0 B
---
ND
---
ND
---
ND
12.4
13-Jun-12
10.0
10.0
---
---
ND
ND
---
14.0
---
ND
---
ND
---
ND
ND
11-Dec-12
10.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Apr-13
10.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug-13
10.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
25-Feb-14
10.0
10.0
---
---
ND
ND
---
31.9
---
ND
---
ND
---
ND
ND
13-Aug-14
10.0
10.0
---
---
ND
ND
---
24.1
---
ND
---
ND
---
ND
ND
12-Mar-15
5.0
10.0
---
---
9.2 B
11.5 B
---
24.3 B
---
6.8 B
---
7.5 B
---
7.1 B
6.1 J
19-Aug-15
5.0
10.0
---
---
ND
7.2 B
---
16.3 B
---
ND
---
ND
---
ND
11.5
18-Feb-16
5.0
10.0
---
---
14.8
ND
---
ND
---
6.6 J
---
ND
---
ND
ND
11-Aug-16
5.0
10.0
---
---
ND
18.2
---
8.6 J
---
ND
---
ND
---
ND
ND
15-Feb-17
5.0
10.0
---
---
ND
14.7
---
8.0 J
---
ND
---
ND
---
ND
ND
24-Aug-17
5.0
10.0
---
---
9.2 J
8.1 J
---
10.7
---
ND
---
ND
---
ND
ND
7-Feb-18
5.0
10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Aug-18
5.0
10.0
---
---
ND
15.3
---
6.6 J
---
ND
---
ND
---
ND
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 Page 19 of 22

TABLE C-02: Historical Detected Inorganic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-1A
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Alkalinity, Total as CaCO3
23-Jun-10
5,000
5,000
---
7,290
---
20,400
---
82,100
---
253,000
---
135,000
---
---
ND
NC 2L = NE µg/L (2/5/10)
14-Dec-10
5,000
5,000
---
---
---
17,600
---
99,800
---
291,000
---
169,000
---
178,000
ND
21-Jun-11
5,000
5,000
---
---
100,000
20,800
---
77,000
---
269,000
---
194,000
---
156,000
ND
6-Dec-11
5,000
5,000
---
---
98,700
10,500
---
81,900
---
274,000
---
164,000
---
151,000
ND
13-Jun-12
1,000
1,000
---
---
101,000
13,700
---
87,500
---
271,000
---
152,000
---
149,000
ND
11-Dec-12
1,000
5,000
---
---
100,000
16,500
---
98,300
---
284,000
---
147,000
---
152,000
ND
29-Apr-13
1,000
5,000
---
---
99,300
13,800
---
97,300
---
293,000
---
156,000
---
122,000
ND
6-Aug-13
1,000
5,000
---
---
102,000
14,300
---
99,100
---
148,000
---
86,800
---
159,000
ND
25-Feb-14
1,000
5,000
---
---
107,000
15,800
---
123,000
---
298,000
---
178,000
---
153,000
ND
13-Aug-14
1000
5000
---
---
103000
14300
---
93800
---
301000
---
187000
---
164000
ND
12-Mar-15
1000
5000
---
---
99700
14700
---
88300
---
306000
---
151000
---
164000
ND
19-Aug-15
1000
5000
---
---
102000
19600
---
88200
---
294000
---
180000
---
164000
ND
18-Feb-16
1000
5000
---
---
108000
4350 J
---
89800
---
308000
---
141000
---
168000
ND
11-Aug-16
1000
5000
---
---
108000
24400
---
91800
---
304000
---
176000
---
173000
ND
15-Feb-17
1000
5000
---
---
115000
16000
---
92800
---
300000
---
175000
---
183000
ND
24-Aug-17
1000
5000
---
---
121000
26800
---
98500
---
329000
---
194000
---
195000
ND
7-Feb-18
1000
5000
---
---
125000
6900
---
101000
---
330000
---
199000
---
207000
ND
15-Aug-18
1000
5000
---
---
123000
22100
---
93200
---
302000
---
192000
---
203000
ND
Chloride
23-Jun-10
5,000
5,000
---
7,950
---
ND
---
37,400
---
40,000
---
39,700
---
97,900
ND
NC 2L = 250000 µg/L (2/5/10)
14-Dec-10
5,000
5,000
---
---
---
5,100
---
38,400
---
44,500
---
39,600
---
108,000
ND
21-Jun-11
5,000
5,000
---
---
8,600
ND
---
35,800
---
45,300
---
41,400
---
106,000
ND
6-Dec-11
5,000
5,000
---
---
9,340
ND
---
28,600
---
49,200
---
39,200
---
110,000
ND
13-Jun-12
1,000
1,000
---
---
9,410
4,540
---
29,400
---
49,300
---
46,400
---
109,000
ND
11-Dec-12
1,000
1,000
---
---
8,570
5,220
---
30,800
---
50,600
---
46,600
---
107,000
ND
29-Apr-13
1,000
1,000
---
---
9,550
4,120
---
30,000
---
49,800
---
22,300
---
122,000
ND
6-Aug-13
1,000
1,000
---
---
7,590
5,180
---
25,700
---
50,100
---
48,700
---
107,000
ND
25-Feb-14
1,000
1,000
---
---
9,140
5,510
---
33,200
---
60,300
---
57,400
---
120,000
ND
13-Aug-14
500
1,000
---
---
8,030
4,070
---
21,300
---
97,600
---
43,400
---
106,000
ND
12-Mar-15
500
1,000
---
---
8,840
4,350
---
20,700
---
51,700
---
42,600
---
121,000
ND
19-Aug-15
500
1,000
---
---
9,440
5,160
---
23,200
---
51,500
---
48,500
---
111,000
ND
18-Feb-16
500
1,000
---
---
17,200
4,600
---
20,600
---
69,500
---
49,700
---
153,000
ND
11-Aug-16
500
1,000
---
---
9,410
4,430
---
23,200
---
57,300
---
51,300
---
147,000
ND
15-Feb-17
2,500
5,000
---
---
10,900
4,970
---
29,300
---
59,100
---
49,200 11,
---
142,000
ND
---
21,700
---
59,300
---
50,300
---
136,000
ND
7-Feb-18
500
1,000
---
---
10,000
4,790
---
23,000
---
60,200
---
58,600
---
149,000
ND
15-Aug-18
500
1,000
---
---
9,620
---
---
---
---
---
---
---
---
---
ND
Total Cyanide
8-Jul-08
---
10.0
---
---
---
ND
---
ND
---
6.2 J
---
ND
---
ND
ND
NC 2L = 70 µg/L (10/23/07)
16-Dec-08
---
---
---
---
---
---
---
---
---
---
---
---
---
---
---
8-Ju -09
5.0
10.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Dec-09
---
---
---
ND
---
---
---
---
---
---
---
---
---
---
---
- un-
5.0
10.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
14-Dec-10
---
---
---
---
---
---
---
---
---
---
---
---
---
---
---
21 -Jun- 11
5.
---
---
ND
ND
---
---
ND
ND
6-Dec-11
---
---
---
---
---
---
---
---
---
---
---
---
---
---
---
13-Jun-12
5.0
10
---
---
---
5.8 J
---
6.2 J
---
5.2 J
---
---
---
---
---
11-Dec-12
---
---
---
---
---
---
---
---
---
---
---
---
---
---
---
29-Apr-13
5.0
10
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug-13
---
---
---
---
---
---
---
---
---
---
---
---
---
---
---
25-Feb-14
5.0
10
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
---
---
---
---
---
---
---
---
---
---
---
---
---
---
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 Page 20 of 22

TABLE C-02: Historical Detected Inorganic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-1A
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Sulfide
17-Nov-95
---
1,000
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
2-Dec-97
---
1,000
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
23-Mar-98
---
1,000
ND
ND
---
1,000
ND
---
ND
---
1,200
---
1400
---
---
27-May-98
---
1,000
ND
ND
---
1,000
ND
---
ND
---
ND
---
ND
---
---
16-Nov-98
---
1,000
12,000
1,200
---
13,000
2,200
---
ND
---
13,000
---
ND
---
---
10-Sep-99
---
1,000
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
16-Nov-99
---
1,000
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
---
1,000
---
---
---
17,000
---
5,000
---
47,000
---
33,000
---
36,000
---
26-Oct-00
---
1,000
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
---
1,000
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
13-Jun-02
---
1,000
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Jun-03
---
1,000
---
---
---
---
---
---
---
---
---
---
---
ND
---
30-Dec-03
---
1,000
---
---
---
---
---
---
---
---
---
---
---
30-Jun-04
---
1,000
---
ND
---
ND
---
7
---
ND
---
ND
---
ND
---
29-Dec-04
---
1,000
---
---
---
---
---
---
---
---
---
---
---
---
---
29-Jun-05
---
1,000
---
ND
---
ND
---
ND
---
ND
---
ND
---
1,200
ND
29-Dec-05
---
1,000
---
1,200 B
---
ND
---
ND
---
1,700 B
---
ND
---
ND
1,200
28-Jun-06
---
1,000
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Dec-06
---
1,000
---
700 J
---
ND
---
500 J
---
ND
---
ND
---
ND
ND
12-Jul-07
---
1,000
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
NC 2L = NE µg/L (10/23/07)
19-Dec-07
---
1,000
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
8-Jul-08
---
1,000
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
16-Dec-08
100
1,000
---
259 J
---
ND
---
150 J
---
ND
---
141 J
---
ND
ND
8-Jul-09
100
1,000
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Dec-09
100
1,000
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
23-Jun-10
100
1,000
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
14-Dec-10
100
1,000
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
21-Jun-11
100
1,000
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Dec-11
100
1,000
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Jun-12
100
1,000
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
11-Dec-12
100
1,000
---
---
ND
ND
---
ND
---
ND
---
117 J
---
ND
ND
29-Apr-13
100
1,000
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug-13
100
1,000
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
25-Feb-14
100
1,000
---
---
ND
ND
---
141 J
---
189 J
---
ND
---
ND
ND
13-Aug-14
50
1,000
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
12-Mar-15
100
1,000
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
19-Aug-15
100
1,000
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
18-Feb-16
100
1,000
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
11-Aug-16
100
1,000
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
15-Feb-17
100
1,000
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
24-Aug-17
100
1,000
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
7-Feb-18
100
1,000
---
---
ND
---
---
---
ND
---
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 Page 21 of 22

TABLE C-02: Historical Detected Inorganic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-1A
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Sulfate
23-Jun-10
---
5,000
---
5,160
---
14,800
---
7,180
---
9,140
---
ND
---
---
ND
N L= 5 µ 5
-Dec-
--
5,000
---
---
---
14,500
---
9,210
---
9,700
---
ND
---
ND
ND
21-Jun-11
---
5,000
---
---
24,400
11,400
---
7,490
---
7,740
---
ND
---
ND
ND
6-Dec-11
5,000
5,000
---
---
39,800
13,800
---
8,000
---
7,730
---
ND
---
ND
ND
13-Jun-12
2,000
250,000
---
---
25,400 J
13,700 J
---
8,140 J
---
8,400 J
---
2,790 J
---
3,040 J
ND
11-Dec-12
2,000
250,000
---
---
28,000 J
14,800 J
---
9,120 J
---
10,100 J
---
4,420 J
---
2,900 J
ND
29-Apr-13
2,000
250,000
---
---
26,100 J
12,300 J
---
9,150 J
---
17,100 J
---
2,730 J
---
3,200 J
ND
6-Aug-13
2,000
250,000
---
---
25,300 J
7,370 J
---
7,830 J
---
11,700 J
---
2,760 J
---
3,320 J
ND
25-Feb-14
2,000
250,000
---
---
28,900 J
11,200 J
---
8,130 J
---
9,550 J
---
2,590 J
---
4,620 J
ND
13-Aug-14
1,000
250,000
---
---
31,900 J
9,370 J
---
7,910 J
---
11,600 J
---
2,450 J
---
2,780 J
ND
12-Mar-15
1,000
250,000
---
---
32,600 J
12,100 J
---
8,040 J
---
8,340 J
---
3,400 J
---
3,330 J
ND
19-Aug-15
10,000
250,000
---
---
42,900 J
10,200 J
---
8,110 J
---
10,400 J
---
2,890 J
---
3,210 J
ND
18-Feb-16
2,000
500,000
---
---
39,300 J
11,200 J
---
7,960 J
---
10,300 J
---
3,830 J
---
3,310 J
ND
11-Aug-16
5,000
1,250,000
---
---
112,000 J
8,500 J
---
7,700 J
---
10,300 J
---
3,100 J
---
3,140 J
ND
15-Feb-17
1,000
250,000
---
---
47,100 J
11,200 J
---
7,860 J
---
7,940 J
---
3,510 J
---
3,260 J
ND
24-Aug-17
500
250,000
---
---
49,700 J
9,940 J
---
8,310 J
---
9,260 J
---
6,680 J
---
2,620 J
ND
7-Feb-18
500
250,000
---
---
42,800 J
7,990 J
---
6,650 J
---
6,110 J
---
4,000 J
---
2,060 J
ND
15-Aug-18
500
250,000
---
---
55,200 J
7,690 J
---
7,130 J
---
6,470 J
---
4,200 J
---
2,650 J
ND
Total Dissolved Solids, Dissolved
23-Jun-10
250,000
250,000
---
710,000
---
96,200
---
184,000
---
364,000
---
237,000
---
360,000
ND
NC 2L = 500,000 µg/L (2/5/10)
14-Dec-10
25,000
25,000
---
---
---
100,000
---
218,000
---
372,000
---
260,000
---
347,000
ND
21-Jun-11
5,000
5,000
---
---
170,000
89,000
---
194,000
---
374,000
---
238,000
---
378,000
ND
6-Dec-11
25,000
25,000
---
---
174,000
92,000
---
168,000
---
378,000
---
242,000
---
408,000
ND
13-Jun-12
25,000
25,000
---
---
189,000
98,000
---
184,000
---
390,000
---
253,000
---
402,000
ND
11-Dec-12
25,000
25,000
---
---
199,000
141,000
---
199,000
---
427,000
---
274,000
---
419,000
ND
29-Apr-13
25,000
25,000
---
---
170,000
114,000
---
183,000
---
416,000
---
276,000
---
466,000
ND
6-Aug-13
25,000
25,000
---
---
179,000
142,000
---
175,000
---
421,000
---
291,000
---
423,000
ND
25-Feb-14
25,000
25,000
---
---
173,000
109,000
---
206,000
---
405,000
---
281,000
---
421,000
ND
13-Aug-14
25,000
25,000
---
---
172,000
184,000
---
187,000
---
446,000
---
319,000
---
504,000
ND
12-Mar-15
25,000
25,000
---
---
229,000
113,000
---
184,000
---
430,000
---
256,000
---
470,000
ND
19-Aug-15
25,000
25,000
---
---
217,000
149,000
---
172,000
---
431,000
---
303,000
---
487,000
ND
18-Feb-16
25,000
25,000
---
---
162,000
84,000
---
140,000
---
412,000
---
237,000
---
475,000
ND
- ug-
---
---
213,000
122,000 11,E
--
171,000
---
437,000
---
301,000
---
516,000
ND
15-Feb-17
25,000
25,000
---
---
233,000
62,000 D6
---
154,000
---
438,000
---
277,000
---
481,000
ND
24-Aug-17
25,000
25,000
---
226,000 D6
114,000
---
160,000
---
418,000
---
270,000
---
467,000
ND
7-Feb-18
25,000
25,000
---
---
235,000
124,000
---
170,000
---
444,000
---
308,000
---
520,000
ND
15-Aug-18
25,000
25,000
---
249,000
238,000
---
164,000
---
458,000
---
303,000
---
509,000
ND
Notes:
All concentrations are in micrograms per liter (µg/L).
RL = Reporting Limit (Lab. Reporting Limit for September 1994 - May 1999; NC PQL for October 1999 - December 2006; and SWSL for December 2006 - present).
DL = Laboratory detection limit.
J = Estimated value between the DL and the RL.
B = Blank -qualified data; result is expected to be biased high based on concentrations in the blanks.
ND = Not detected above laboratory reporting limit.
NC 2L = North Carolina Groundwater Standards from 15A NCAC 2L.0202.
GWPS = Groundwater Protection Standards established by the DENR Solid Waste Section (SWS).
When the NC 2L has not been established, the GWPS will be used.
Bold values for groundwater are above the NC 2L Standards or GWPS.
--- = Well was not monitored and/or not reported.
# = Data for MW-lA during the July 2008 event was not used in background calculations because samples were composed of too much sediment due to basically dry conditions, leading to skewed values of inorganic constituents.
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 Page 22 of 22

TABLE C-03: Historical Detected Organic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-IA
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Organic Compounds
Acetone
15-Dec-09
2.2 100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
2.8 J
23-Jun-10
2.2 100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
7.7 J
NC 2L = 700 µ 10 23 07
14-Dec-10
2.2 100
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
21-Jun-11
2.2 100
---
---
ND
3.8 B
---
2.8 B
---
ND
---
ND
---
ND
3.9 J
NC 2B =NEµ OS O1 07
6-Dec-11
2.2 100
---
--
ND
ND
---
ND
---
ND
---
ND
---
ND
8.8 J
NC 2L = 6,000 µ 2 5 10
13-Jun-12
2.2 100
---
--
ND
ND
---
ND
---
ND
---
ND
---
ND
4.7 J
12-Dec-12
10.0 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Apr-13
10.0 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
14.6 J
6-Aug-13
10.0 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
25-Feb-14
10.0 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
19.3 J
13-Aug-14
10.0 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Mar-15
10.0 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
19-Aug-15
10.0 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
18-Feb-16
10.0 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
11-Aug-16
10.0 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Feb-17
10.0 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
24-Aug-17
10.0 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
7-Feb-18
10.0 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
16-Aug-18
10.0 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 Page 1 of 28

TABLE C-03: Historical Detected Organic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-IA
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Benzene
14-Sep-94
--- 5
ND
ND
ND
12.0
---
ND
---
ND
---
ND
---
---
-Dec- 94
--- 5
ND
ND
---
ND
14.0
---
ND
---
ND
---
ND
---
---
8-Feb-95
--- 5
ND
ND
---
ND
15.0
---
ND
---
ND
---
ND
---
---
2-Mar-95
--- 5
ND
ND
---
ND
13.0
---
ND
---
ND
---
ND
---
---
17-Nov-95
--- 5
ND
ND
---
ND
16.0
---
ND
---
ND
---
ND
---
---
23-May-96
--- 5
ND
ND
---
ND
15.0
---
ND
---
ND
---
ND
---
---
14-Nov-96
--- 5
ND
ND
---
ND
9.0
---
ND
---
ND
---
ND
---
---
18-Jun-97
--- 5
ND
ND
---
ND
13.0
---
ND
---
ND
---
ND
---
---
2-Dec-97
--- 5
ND
ND
---
ND
13.0
---
ND
---
ND
---
ND
---
---
27-May-98
--- 5
ND
ND
---
ND
12.0
---
ND
---
ND
---
ND
---
---
16-Nov-98
--- 5
ND
ND
---
ND
12.4
---
ND
---
ND
---
ND
---
---
10-Sep-99
--- 5
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
16-Nov-99
--- 5
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
--- 5
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
26-Oct-00
--- 5
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Oct-0 I
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
I O-Jun-02
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
13-Jun-02
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
19-Nov-02
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Jun-03
--- 5
---
ND
---
ND
---
ND
---
7.0
---
ND
---
ND
ND
30-Dec-03
--- 5
---
ND
---
ND
---
ND
---
12.0
---
ND
---
ND
ND
30-Jun-04
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Jun-05
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Jun-06
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Dec-06
--- 3
---
ND
---
ND
---
ND
1.3
ND
ND
ND
---
ND
ND
C 213 = NE gg/L (05/01/07)
12-Jul-07
--- I
---
ND
---
ND
---
ND
---
ND
---
0.40 J
---
ND
ND
NC 2L = I gg/L (10/23/07)
19-Dec-07
--- I
---
---
---
ND
---
ND
---
ND
---
0.53 J
---
ND
ND
8-Jul-08
--- 1.0
---
---
---
ND
---
ND
---
ND
---
0.59 J
---
ND
ND
16-Dec-08
0.25 1.0
---
ND
---
ND
---
ND
---
ND
---
0.40 J
---
ND
ND
8-Jul-09
0.25 1.0
---
ND
---
ND
---
ND
---
ND
---
0.54 J
---
ND
ND
15-Dec-09
0.25 1.0
---
ND
---
ND
---
ND
---
ND
---
0.37 J
---
ND
ND
23-Jun-10
0.25 1.0
---
ND
---
ND
---
ND
---
ND
---
0.42 J
---
ND
ND
14-Dec-10
0.25 1.0
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
21-Jun-11
0.25 1.0
---
---
ND
ND
---
ND
---
ND
---
0.39 J
---
ND
ND
6-Dec- 11
0.25 1.0
---
---
ND
ND
---
ND
---
ND
---
0.40 J
---
ND
ND
13-Jun- 12
0.25 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Dec- 12
0.25 1.0
---
---
ND
ND
---
ND
---
ND
---
0.41 1
---
ND
ND
29-Apr- 13
0.25 1.0
---
---
ND
ND
---
ND
---
ND
---
0.33 J
---
ND
ND
6-Aug- 13
0.25 1.0
---
---
ND
ND
---
ND
---
ND
---
0.40 J
---
ND
ND
25-Feb-14
0.25 1.0
---
---
ND
ND
---
ND
---
ND
---
0.40 J
---
ND
ND
13-Aug-14
0.25 1.0
---
---
ND
ND
---
ND
---
ND
---
0.41 1
---
ND
ND
12-Mar- 15
0.25 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
19-Aug- 15
0.25 1.0
---
---
ND
ND
---
ND
---
ND
---
0.35 J
---
ND
ND
18-Feb-16
0.25 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
11 -Aug- 16
0.25 1.0
---
---
ND
ND
---
ND
---
ND
---
0.34 J
---
ND
ND
15-Feb-17
0.25 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
24-Aug- 17
0.25 1.0
---
---
ND
ND
---
ND
---
ND
---
0.30 J
---
ND
ND
7-Feb-18
0.25 1.0
---
---
ND
ND
---
ND
---
ND
---
0.31 1
---
ND
ND
16-Aug- 18
0.25 1.0
---
---
ND
ND
---
ND
---
ND
---
0.35 J
---
ND
ND
Granville County - Oxford Landfill, Unit I Joyce Engineering
Permit 3901-CDLF-1997 Page 2 of 28

TABLE C-03: Historical Detected Organic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-IA
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Carbon Disulfide
18-Jun-97
--- 100
ND
ND
ND
ND
---
ND
---
ND
---
16.0
---
---
-Dec- 7
-- 100
ND
ND
---
ND
12.0
---
ND
---
ND
---
23.0
---
---
27-May-98
100
ND
ND
---
ND
ND
---
ND
---
ND
---
46.0
---
---
16-Nov-98
100
ND
ND
---
ND
3.3
---
ND
---
ND
---
33.5
---
---
10-Sep-99
--- 100
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
16-Nov-99
100
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
--- 100
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
26-Oct-00
--- 100
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
--- 100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Oct-01
--- 100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
13-Jun-02
--- 100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
19-Nov-02
100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Jun-03
--- 100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
30-Dec-03
--- 100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
30-Jun-04
--- 100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
--- 100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Jun-05
--- 100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
--- 100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Jun-06
--- 100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Dec-06
--- 100
---
ND
---
ND
---
ND
ND
ND
ND
ND
---
ND
ND
NC 213 = NE µg/L (05/01/07)
12-Jul-07
--- 100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
NC 2L = 700 µ (10 23 07)
19-Dec-07
-- 100
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
8-Jul-08
--- 100
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
16-Dec-08
1.2 100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
8-Jul-09
1.2 100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Dec-09
1.2 100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
23-Jun-10
1.2 100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
14-Dec-10
1.2 100
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
21-Jun-11
1.2 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Dec-11
1.2 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Jun-12
1.2 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Dec-12
1.2 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Apr-13
1.2 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug- 13
1.2 100
---
---
ND
ND
---
ND
---
ND
--
ND
---
ND
ND
25-Feb-14
1.2 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
1.2 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Mar-15
1.2 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
19-Aug-15
1.2 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
18-Feb-16
1.2 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
11-Aug-16
1.2 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Feb-17
1.2 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
24-Aug-17
1.2 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
7-Feb-18
1.2 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
16-Aug-18
1.2 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 Page 3 of 28

TABLE C-03: Historical Detected Organic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-IA
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Chlorobenzene
16-Nov-98
--- 5
ND
ND
ND
ND
---
2.7
---
ND
---
ND
---
---
10-Sep-99
--- 5
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
16-Nov-99
--- 5
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
--- 5
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
26-Oct-00
--- 5
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Oct-0 I
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
13-Jun-02
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
19-Nov-02
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Jun-03
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
30-Dec-03
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
30-Jun-04
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Jun-05
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Jun-06
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Dec-06
--- 3
---
ND
---
ND
---
ND
---
ND
ND
ND
---
ND
ND
NC 213 = NE gg/L (05/01/07)
12-Jul-07
--- 3
---
ND
---
ND
---
ND
---
ND
---
0.34 J
---
ND
ND
C 2L = 50 gg/L (10/23/07)
19-Dec-07
--- 3
---
---
---
ND
---
0.64 J
---
ND
---
0.44 J
---
ND
ND
8-Jul-08
--- 3.0
---
---
---
ND
---
ND
---
ND
---
0.97 J
---
ND
ND
16-Dec-08
0.23 3.0
---
ND
---
ND
---
ND
---
ND
---
0.42 J
---
ND
ND
8-Jul-09
0.23 3.0
---
ND
---
ND
---
0.25 J
---
ND
---
0.57 J
---
ND
ND
15-Dec-09
0.23 3.0
---
ND
---
ND
---
0.25 J
---
ND
---
0.49 J
---
ND
ND
23-Jun-10
0.23 3.0
---
ND
---
ND
---
0.26 J
---
ND
---
0.53 J
---
ND
ND
14-Dec- 10
0.23 3.0
---
---
---
ND
---
ND
---
ND
---
0.93 B
---
ND
0.43 1
21-Jun-11
0.23 3.0
---
---
ND
ND
---
0.27 J
---
ND
---
0.65 J
---
ND
ND
6-Dec- 11
0.23 3.0
---
---
ND
ND
---
ND
---
ND
---
0.63 J
---
ND
ND
13-Jun-12
0.23 3.0
---
---
ND
ND
---
ND
---
ND
---
0.55 J
---
ND
ND
12-Dec- 12
0.23 3.0
---
---
ND
ND
---
ND
---
ND
---
1.0 1
---
ND
ND
29-Apr- 13
0.23 3.0
---
---
ND
ND
---
ND
---
ND
---
0.70 J
---
ND
ND
6-Aug- 13
0.23 3.0
---
---
ND
ND
---
ND
---
ND
---
0.83 J
---
ND
ND
25-Feb-14
0.23 3.0
---
---
ND
ND
---
ND
---
ND
---
0.78 J
---
ND
ND
13-Aug-14
0.23 3.0
---
---
ND
ND
---
ND
---
ND
---
0.87 J
---
ND
ND
12-Mar-15
0.23 3.0
---
---
ND
ND
---
ND
---
ND
---
0.64 J
---
ND
ND
19-Aug- 15
0.23 3.0
---
---
ND
ND
---
ND
---
ND
---
0.89 J
---
ND
ND
18-Feb-16
0.23 3.0
---
---
ND
ND
---
ND
---
ND
---
0.79 J
---
ND
ND
11 -Aug- 16
0.23 3.0
---
---
ND
ND
---
ND
---
ND
---
0.96 J
---
ND
ND
15-Feb-17
0.23 3.0
---
---
ND
ND
---
ND
---
ND
---
0.90 1
---
ND
ND
24-Aug- 17
0.23 3.0
---
---
ND
ND
---
ND
---
ND
---
0.78 J
---
ND
ND
7-Feb-18
0.23 3.0
---
---
ND
ND
---
ND
---
ND
---
0.91 1
---
ND
ND
16-Aug- 18
0.23 3.0
---
---
ND
ND
---
ND
---
ND
---
1.10 1
---
ND
ND
Granville County - Oxford Landfill, Unit I Joyce Engineering
Permit 3901-CDLF-1997 Page 4 of 28

TABLE C-03: Historical Detected Organic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL PIL
MW-1
MW-IA
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Chloroethane
14-Sep-94
--- 10
ND
ND
ND
30.0
---
ND
---
ND
---
ND
---
---
2-Dec-94
--- 10
ND
ND
---
ND
26.0
---
ND
---
ND
---
ND
---
---
8-Feb-95
--- 10
ND
ND
---
ND
33.0
---
ND
---
ND
---
35.0
---
---
2-Mar-95
--- 10
ND
ND
---
ND
26.0
---
ND
---
ND
---
24.0
---
---
17-Nov-95
--- 10
ND
ND
---
ND
25.0
---
ND
---
ND
---
27.0
---
---
23-May-96
--- to
ND
ND
---
ND
26.0
---
ND
---
ND
---
56.0
---
---
-Nov-
-- to
ND
ND
---
ND
16.0
---
ND
---
ND
---
ND
---
---
18-Jun-97
--- 10
ND
ND
---
ND
21.0
---
ND
---
ND
---
63.0
---
---
2-Dec-97
--- 10
ND
ND
---
ND
22.0
---
2.0
---
ND
---
64.0
---
---
27-May-98
--- to
ND
ND
---
ND
16.0
---
ND
---
ND
---
78.0
---
---
-Nov-
-- 10
ND
ND
---
ND
15.8
---
ND
---
ND
---
36.2
---
---
10-Sep-99
--- 10
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
-Nov-
-- 10
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
--- 10
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
26-Oct-00
--- to
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
--- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Oct-01
--- to
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
13-Jun-02
--- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
-Nov-
-- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Jun-03
--- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
30-Dec-03
--- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
30-Jun-04
--- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
--- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Jun-05
--- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
--- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Jun-06
--- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Dec-06
--- 10
---
ND
---
ND
---
ND
ND
ND
ND
ND
---
ND
ND
NC 213 = NE gg/L (05/01/07)
12-Jul-07
--- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
C 2L = 2,800 µg/L (10/23/07)
19-Dec-07
--- 10
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
8-Jul-08
--- 10.0
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
16-Dec-08
0.54 10.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
8-Jul-09
0.54 10.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Dec-09
0.54 10.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
C 2L = 3,000 gg/L (2/5/10)
23-Jun-10
0.54 10.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
14-Dec-10
0.54 10.0
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
21-Jun-11
0.54 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Dec- 11
0.54 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Jun-12
0.54 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Dec- 12
0.54 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Apr- 13
0.54 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug- 13
0.54 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
25-Feb-14
0.54 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
0.54 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Mar- 15
0.54 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
19-Aug-15
0.54 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
18-Feb-16
0.54 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
11-Aug-16
0.54 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Feb-17
0.54 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
24-Aug-17
0.54 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
7-Feb-18
0.54 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
16-Aug- 18
0.54 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
Granville County - Oxford Landfill, Unit I Joyce Engineering
Permit 3901-CDLF-1997 Page 5 of 28

TABLE C-03: Historical Detected Organic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-IA
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Chloromethane
23-Jun-10
0.11 1.0
---
0.14 J
---
ND
---
0.12 J
---
ND
---
ND
---
0.16 J
ND
NC 2L = 3 µ (2 5 10)
14-Dec-10
0.11 1.0
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
NC 2B =NEµ (OS O1 07)
21-Jun-11
0.11 1.0
---
--
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Dec-11
0.11 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Jun-12
0.11 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Dec-12
0.11 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Apr-13
0.11 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug-13
0.11 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
25-Feb-14
0.11 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
0.11 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Mar-15
0.11 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
19-Aug-15
0.11 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
18-Feb-16
0.11 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
11-Aug-16
0.11 1.0
---
---
ND
ND
---
ND
---
ND
---
0.12 J
---
ND
ND
15-Feb-17
0.11 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
24-Aug-17
0.11 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
7-Feb-18
0.11 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
16-Aug-18
0.11 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
1,2-Dichlorobenzene
12-Jul-07
--- 5
---
ND
---
ND
---
ND
---
ND
---
0.6 J
---
ND
ND
NC 2B = NE µg/L (05/01/07)
19-Dec-07
--- 5
---
---
ND
---
0.32 J
---
ND
---
0.99 J
---
ND
ND
NC 2L = 24 µ (10/23 07)
8-Jul-08
-- 5.0
---
---
---
ND
---
ND
---
ND
---
1.3 J
---
ND
ND
16-Dec-08
0.30 5.0
---
ND
---
ND
---
ND
---
ND
---
0.73 J
---
ND
ND
8-Jul-09
0.30 5.0
---
ND
---
ND
---
ND
---
ND
---
1.1 J
---
ND
ND
15-Dec-09
0.30 5.0
---
ND
---
ND
---
ND
---
ND
---
0.99 J
---
ND
ND
NC 2L = 20 µ (2 5 10)
23-Jun-10
0.30 5.0
--
ND
---
ND
---
ND
---
ND
---
1.0 J
---
ND
ND
14-Dec-10
0.30 5.0
---
---
---
ND
---
ND
---
ND
---
0.78 J
---
ND
ND
-Jun-
5.
---
---
ND
ND
---
ND
---
ND
--
1.1 J
---
ND
ND
6-Dec-11
0.30 5.0
---
---
ND
ND
---
ND
---
ND
---
0.74 J
---
ND
ND
-Jun-
5.
---
---
ND
ND
---
ND
---
ND
--
1.1 J
---
ND
ND
-Dec- 12
0.30 5.
---
---
ND
ND
---
ND
---
ND
--
1.1 J
---
ND
ND
- pr- 13
0.30 5.
---
---
ND
ND
---
ND
---
ND
--
1.2 J
---
ND
ND
6-Aug- 13
0.30 5.
---
---
ND
ND
---
ND
---
ND
--
1.2 J
---
ND
ND
5-Fe -
5.
---
---
ND
ND
---
ND
---
ND
--
1.1 J
---
ND
ND
- ug-
5.
---
---
ND
ND
--
ND
---
ND
---
1.1 J
---
ND
ND
12-Mar-15
0.30 5.0
---
---
ND
ND
---
ND
---
ND
---
0.89 J
---
ND
ND
- ug- 5
0.30 5.
---
---
ND
ND
---
ND
---
ND
---
1.2 J
---
ND
ND
-Fe -
5.
---
---
ND
ND
---
ND
---
ND
---
1.0 J
---
ND
ND
- ug-
5.
---
---
ND
ND
---
ND
---
ND
---
1.2 J
---
ND
ND
5-Fe - 7
0.30 5.
---
---
ND
ND
---
ND
---
ND
--
1.1 J
---
ND
ND
- ug- 17
0.30 5.
---
---
ND
ND
---
ND
---
ND
--
1.0 J
---
ND
ND
7-Fe -18
0.30 5.0
---
---
ND
ND
--
ND
---
ND
---
1.1 J
---
ND
ND
- ug-
5.
---
---
ND
ND
---
ND
---
ND
--
1.2 J
---
ND
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 Page 6 of 28

TABLE C-03: Historical Detected Organic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-IA
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
1,3-Dichlorobenzene
8-Jul-08
--- 5.0
---
---
ND
---
ND
---
ND
---
0.29 J
---
ND
ND
NC 2L = 170 gg/L (10/23/07)
16-Dec-08
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
NC 2B = NE gg/L (05/01/07)
8-Jul-09
0.24 5.0
---
ND
---
ND
---
ND
---
ND
---
0.38 J
---
ND
ND
15-Dec-09
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
NC 2L = 200 pg/L (2/5/10)
23-Jun-10
0.24 5.0
---
---
---
ND
---
---
---
ND
---
0.35 J
---
ND
ND
14-Dec-10
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
21-Jun-11
0.24 5.0
---
---
ND
ND
---
---
---
ND
---
0.32 J
---
ND
ND
6-Dec- 11
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
13-Jun-12
0.24 5.0
---
---
ND
ND
---
ND
---
ND
---
0.29 J
---
ND
ND
12-Dec-12
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
29-Apr- 13
0.24 5.0
---
---
ND
ND
---
ND
---
ND
---
0.36 J
---
ND
ND
6-Aug- 13
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
25-Feb-14
0.24 5.0
---
---
ND
ND
---
ND
---
ND
---
0.29 J
---
ND
ND
13-Aug-14
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
12-Mar- 15
0.24 5.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
18-Feb-16
0.24 5.0
---
---
ND
---
---
---
---
---
---
0.31 1
---
---
ND
11-Aug-16
0.24 5.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
15-Feb-17
0.24 5.0
---
---
ND
---
---
---
---
---
---
0.38 J
---
---
ND
24-Aug-17
0.24 5.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
7-Feb-18
0.24 5.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
Granville County - Oxford Landfill, Unit I Joyce Engineering
Permit 3901-CDLF-1997 Page 7 of 28

TABLE C-03: Historical Detected Organic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-IA
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
1,4-Dichlorobenzene
14-Sep-94
--- 5
ND
ND
ND
5.0
---
ND
---
ND
---
ND
---
NA
2-Dec-94
--- 5
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
NA
8-Feb-95
--- 5
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
NA
2-Mar-95
--- 5
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
NA
7-Nov- 5
--- 5
ND
ND
---
ND
ND
---
ND
--
ND
---
ND
---
---
23-May-96
--- 5
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
-Nov-
--- 5
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
18-Jun-97
--- 5
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
2-Dec-97
--- 5
ND
ND
---
ND
2.0
---
2.0
---
ND
---
ND
---
---
27-May-98
--- 5
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
-Nov-
--- 5
ND
ND
--
ND
2.1
---
3.2
---
ND
---
2.2
---
---
10-Sep-99
--- 5
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
16-Nov-99
--- 5
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
--- 5
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
26-Oct-00
--- 5
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Oct-01
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
13-Jun-02
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
19-Nov-02
--- 10.5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Jun-03
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
30-Dec-03
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
30-Jun-04
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Jun-05
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Jun-06
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Dec-06
--- 3
---
ND
---
ND
---
ND
3.7
ND
ND
ND
---
ND
ND
NC 2B = NE µg/L (05/01/07)
12-Jul-07
--- 1
---
ND
---
ND
---
0.32 J
---
ND
---
ND
---
ND
ND
Resample >
21-Aug-07
--- 1
---
---
---
---
---
0.30 J
---
---
---
---
---
---
---
NC 2L = 1.4 µ (10 23 07)
19-Dec-07
--- 1
---
---
--
ND
---
0.52 J
---
ND
---
0.71 J
---
ND
ND
8-Jul-08
--- 1.0
---
---
---
ND
---
ND
---
ND
---
0.96 J
---
ND
ND
16-Dec-08
0.33 1.0
---
ND
---
ND
---
ND
---
ND
---
0.64 J
---
ND
ND
8-Jul-09
0.33 1.0
---
ND
---
ND
---
ND
---
ND
---
0.84 J
---
ND
ND
15-Dec-09
0.33 1.0
---
ND
---
ND
---
ND
---
ND
---
0.76 J
---
ND
ND
NC 2L = 6 µ L (2 5 10)
23-Jun-10
0.33 1.0
--
ND
---
ND
---
ND
---
ND
---
0.79 J
---
ND
ND
-Dec-
---
---
--
ND
---
ND
---
ND
---
0.96 B
---
ND
0.35 J
-Jun-
---
---
ND
ND
---
ND
---
ND
--
1.0
---
ND
ND
6-Dec-11
0.33 1.0
---
---
ND
ND
---
ND
---
ND
---
0.81 J
---
ND
ND
13-Jun-12
0.33 1.0
---
---
ND
ND
---
ND
---
ND
---
0.77 J
---
ND
ND
12-Dec-12
0.33 1.0
---
---
ND
ND
---
ND
---
ND
---
0.83 J
---
ND
ND
- pr- 13
0.33 1.0
---
---
ND
ND
---
ND
---
ND
--
1.0
---
ND
ND
6-Aug- 13
0.33 1.0
---
---
ND
ND
---
ND
---
ND
--
1.0
---
ND
ND
25-Feb-14
0.33 1.0
---
---
ND
ND
---
ND
---
ND
---
0.82 J
---
ND
ND
13-Aug-14
0.33 1.0
---
---
ND
ND
---
ND
---
ND
---
0.97 J
---
ND
ND
12-Mar-15
0.33 1.0
---
---
ND
ND
---
ND
---
ND
---
0.86 J
---
ND
ND
- ug- 15
0.33 1.0
---
---
ND
ND
---
ND
---
ND
---
1.00
---
ND
ND
18-Feb-16
0.33 1.0
---
---
ND
ND
---
ND
---
ND
---
0.92 J
---
ND
ND
11-Aug-16
0.33 1.0
---
---
ND
ND
---
ND
---
ND
---
0.93 J
---
ND
ND
5-Fe - 7
0.33 1.0
---
---
ND
ND
---
ND
---
ND
---
1.10
---
ND
ND
24-Aug-17
0.33 1.0
---
---
ND
ND
---
ND
---
ND
---
0.81 J
---
ND
ND
7-Feb-18
0.33 1.0
---
---
ND
ND
---
ND
---
ND
---
0.81 J
---
ND
ND
- ug- 18
0.33 1.0
---
---
ND
ND
---
ND
---
ND
---
1.10
---
ND
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 Page 8 of 28

TABLE C-03: Historical Detected Organic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-IA
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Trans-1,4-Dichloro-2-Butene
27-May-98
--- 100
ND
ND
ND
ND
---
ND
---
ND
---
6.9
---
---
16-Nov-98
--- 100
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
10-Sep-99
--- 100
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
16-Nov-99
--- 100
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
--- 100
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
26-Oct-00
-- 100
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
--- 100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Oct-01
--- 100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
13-Jun-02
--- 100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
19-Nov-02
--- 100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Jun-03
--- 100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
30-Dec-03
--- 100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
30-Jun-04
--- 100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
--- 100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Jun-05
--- 100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
--- 100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Jun-06
--- 100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Dec-06
--- 100
---
ND
---
ND
---
ND
ND
ND
ND
ND
---
ND
ND
NC 213 = NE µg/L (05/01/07)
12-Jul-07
--- 100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
NC 2L =NEµ (10 23 07)
19-Dec-07
-- 100
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
8-Jul-08
--- 100
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
16-Dec-08
1.0 100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
8-Jul-09
1.0 100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Dec-09
1.0 100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
23-Jun-10
1.0 100
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
14-Dec-10
1.0 100
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
21-Jun-11
1.0 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Dec-11
1.0 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Jun-12
1.0 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Dec-12
1.0 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Apr-13
1.0 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug-13
1.0 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
25-Feb-14
1.0 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
1.0 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Mar-15
1.0 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
19-Aug-15
1.0 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
18-Feb-16
1.0 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
11-Aug-16
1.0 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Feb-17
1.0 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
24-Aug-17
1.0 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
7-Feb-18
1.0 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
16-Aug-18
1.0 100
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 Page 9 of 28

TABLE C-03: Historical Detected Organic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-IA
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Dichlorodifluorornethane
17-Nov-95
--- 5
ND
ND
ND
ND
---
ND
---
ND
---
ND
---
---
2-Dec-97
--- 5
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
23-Mar-98
--- 5
ND
ND
---
ND
ND
---
6.1
---
ND
---
6.0
---
---
27-May-98
--- 5
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
16-Nov-98
--- 5
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
10-Sep-99
--- 5
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
16-Nov-99
--- 5
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
--- 5
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
26-Oct-00
--- 5
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
--- 5
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
13-Jun-02
--- 5
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Jun-03
--- 5
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
30-Dec-03
--- 5
---
---
---
---
---
---
---
---
---
---
---
---
---
30-Jun-04
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
29-Jun-05
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
--- 5
---
---
---
---
---
---
---
---
---
---
---
---
---
28-Jun-06
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Dec-06
--- ---
---
---
---
---
---
---
ND
---
ND
---
---
---
---
NC 213 = NE gg/L (05/01/07)
12-Jul-07
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
NC 2L = 1,400 Rg/L (10/23/07)
19-Dec-07
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
8-Jul-08
--- 5.0
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
16-Dec-08
--- ---
---
---
---
ND
---
---
---
---
---
---
---
---
---
8-Jul-09
0.21 5.0
---
ND
---
ND
---
ND
---
ND
---
0.37 J
---
ND
ND
15-Dec-09
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
NC 2L = 1000 Rg/L (2/5/10)
23-Jun-10
0.21 5.0
---
---
---
ND
---
ND
---
ND
---
0.29 J
---
ND
ND
14-Dec- 10
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
21-Jun-11
0.21 5.0
---
---
ND
ND
---
ND
---
ND
---
0.36 J
---
ND
ND
6-Dec- 11
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
13-Jun-12
0.21 5.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Dec-12
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
29-Apr-13
0.21 5.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug- 13
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
25-Feb-14
0.21 5.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
12-Mar- 15
0.21 5.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
---
ND
---
---
ND
11-Aug-16
0.21 5.0
---
---
---
---
---
---
---
---
---
---
---
---
---
15-Feb-17
0.21 5.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
24-Aug-17
0.21 5.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
7-Feb-18
0.21 5.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
Granville County - Oxford Landfill, Unit I Joyce Engineering
Permit 3901-CDLF-1997 Page 10 of 28

TABLE C-03: Historical Detected Organic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-IA
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
1, 1 -Dichloroethane
14-Sep-94
--- 5
ND
ND
ND
ND
---
ND
---
ND
---
ND
---
---
2-Dec-94
--- 5
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
8-Feb-95
--- 5
ND
ND
---
ND
ND
---
ND
---
7.0
---
ND
---
---
2-Mar-95
--- 5
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
1, 1 -Dichloroethane
17-Nov-95
--- 5
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
23-May-96
--- 5
ND
ND
---
ND
ND
---
ND
---
5.0
---
7.0
---
---
14-Nov-96
--- 5
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
18-Jun-97
--- 5
ND
ND
---
ND
ND
---
ND
---
ND
---
9.7
---
---
2-Dec-97
--- 5
ND
ND
---
ND
ND
---
2.0
---
10.0
---
ND
---
---
27-May-98
--- 5
ND
ND
---
ND
ND
---
ND
---
6.0
---
12.0
---
---
16-Nov-98
--- 5
ND
ND
---
ND
ND
---
ND
---
9.0
---
5.2
---
---
10-Sep-99
--- 5
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
16-Nov-99
--- 5
ND
ND
---
ND
---
ND
---
ND
---
6.0
---
ND
---
16-Dec-99
--- 5
---
---
---
---
---
---
---
---
---
5.0
---
---
---
10-May-00
--- 5
ND
ND
---
ND
---
ND
---
ND
---
6.0
---
ND
---
26-Oct-00
--- 5
ND
ND
---
ND
---
ND
---
ND
---
7.0
---
ND
---
18-Apr-01
--- 5
---
ND
---
ND
---
ND
---
ND
---
6.0
---
ND
---
27-Oct-01
--- 5
---
ND
---
ND
---
ND
---
ND
---
7.0
---
ND
---
I O-Jun-02
--- 5
---
ND
---
ND
---
ND
---
ND
---
6.0
---
ND
---
13-Jun-02
--- 5
---
ND
---
ND
---
ND
---
ND
---
6.0
---
ND
---
19-Nov-02
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Jun-03
--- 5
---
ND
---
ND
---
ND
---
ND
---
7.2
---
ND
ND
30-Dec-03
--- 5
---
ND
---
ND
---
ND
---
ND
---
6.3
---
ND
ND
30-Jun-04
--- 5
---
ND
---
ND
---
ND
---
ND
---
6.5
---
ND
ND
29-Dec-04
--- 5
---
ND
---
ND
---
ND
---
ND
---
6.9
---
ND
ND
29-Jun-05
--- 5
---
ND
---
ND
---
ND
---
ND
---
7.0
---
ND
ND
29-Dec-05
--- 5
---
ND
---
ND
---
ND
---
ND
---
6.0
---
ND
ND
28-Jun-06
--- 5
---
ND
---
ND
---
ND
---
ND
---
6.6
---
ND
ND
28-Dec-06
--- 5
---
ND
---
ND
---
ND
ND
ND
1.7
5.3
---
ND
ND
NC 213 = NE pg/L (05/01/07)
12-Jul-07
--- 5
---
ND
---
ND
---
0.33 J
---
ND
---
5.4
---
ND
ND
Resample >
21-Aug-07
--- 5
---
---
---
---
---
0.40 J
---
---
---
---
---
---
---
NC 2L = 70 µg/L (10/23/07)
19-Dec-07
--- 5
---
---
---
ND
---
ND
---
ND
---
6.2
---
ND
ND
8-Jul-08
--- 5.0
---
---
---
ND
---
ND
---
ND
---
5.1
---
ND
ND
16-Dec-08
0.32 5.0
---
ND
---
ND
---
ND
---
ND
---
3.4 1
---
ND
ND
8-Jul-09
0.32 5.0
---
ND
---
ND
---
ND
---
ND
---
9.3
---
ND
ND
15-Dec-09
0.32 5.0
---
ND
---
ND
---
ND
---
ND
---
6.4
---
ND
ND
NC 2L = 6 µg/l, (2/5/10)
23-Jun-10
0.32 5.0
---
ND
---
ND
---
ND
---
ND
---
6.5
---
ND
ND
14-Dec- 10
0.32 5.0
---
---
---
ND
---
ND
---
ND
---
3.9 1
---
ND
ND
21-Jun-11
0.32 5.0
---
---
ND
ND
---
ND
---
ND
---
6.7
---
ND
ND
6-Dec- 11
0.32 5.0
---
---
ND
ND
---
ND
---
ND
---
3.0 1
---
ND
ND
13-Jun-12
0.32 5.0
---
---
ND
ND
---
ND
---
ND
---
3.7 1
---
ND
ND
12-Dec- 12
0.32 5.0
---
---
ND
ND
---
ND
---
ND
---
2.5 1
---
ND
ND
29-Apr- 13
0.32 5.0
---
---
ND
ND
---
ND
---
ND
---
5.8
---
ND
ND
6-Aug- 13
0.32 5.0
---
---
ND
ND
---
ND
---
ND
---
5.0
---
ND
ND
25-Feb-14
0.32 5.0
---
---
ND
ND
---
ND
---
ND
---
4.5 1
---
0.35 1
ND
13-Aug-14
0.32 5.0
---
---
ND
ND
---
ND
---
ND
---
3.4 1
---
0.39 1
ND
12-Mar-15
0.32 5.0
---
---
ND
ND
---
ND
---
ND
---
4.2 1
---
ND
ND
19-Aug- 15
0.32 5.0
---
---
ND
ND
---
ND
---
ND
---
3.7 1
---
0.54 1
ND
18-Feb-16
0.32 5.0
---
---
ND
ND
---
ND
---
ND
---
3.4 1
---
0.59 1
ND
11 -Aug- 16
0.32 5.0
---
---
ND
ND
---
ND
---
ND
---
3.4 1
---
0.77 1
ND
15-Feb-17
0.32 5.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
24-Aug- 17
0.32 5.0
---
---
ND
ND
---
ND
---
ND
---
2.2 1
---
0.99 1
ND
7-Feb-18
0.32 5.0
---
---
ND
ND
---
ND
---
ND
---
1.7 1
---
0.93 1
ND
16-Aug- 18
0.32 5.0
---
---
ND
ND
---
ND
---
ND
---
2.4 1
---
0.93 1
ND
Granville County - Oxford Landfill, Unit I Joyce Engineering
Permit 3901-CDLF-1997 Page 11 of 28

TABLE C-03: Historical Detected Organic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-IA
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
1,2-Dichloroethane
6-Aug-13
0.12 1.0
---
---
ND
ND
---
0.62 J
---
ND
---
ND
---
ND
ND
NC 2L = 0.4 µ (2 5 10)
25-Fe -14
0.12 1.0
---
--
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
0.12 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Mar-15
0.12 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
19-Aug-15
0.24 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
18-Feb-16
0.24 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
11-Aug-16
0.24 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Feb-17
0.24 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
24-Aug-17
0.24 1.0
---
---
0.24 J
ND
---
ND
---
ND
---
0.25 J
---
0.25 J
ND
7-Feb-18
0.24 1.0
---
---
ND U
ND
---
ND
---
ND
---
ND
---
ND
ND
16-Aug-18
0.24 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 Page 12 of28

TABLE C-03: Historical Detected Organic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-IA
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
cis- 1,2-Dichloroethene
14-Sep-94
--- 5
ND
ND
ND
ND
---
ND
---
ND
---
ND
---
---
2-Dec-94
--- 5
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
8-Feb-95
--- 5
ND
ND
---
ND
ND
---
ND
---
23.0
---
ND
---
---
2-Mar-95
--- 5
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
17-Nov-95
--- 5
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
23-May-96
--- 5
ND
ND
---
ND
ND
---
ND
---
14.0
---
ND
---
---
14-Nov-96
--- 5
ND
ND
---
ND
ND
---
ND
---
19.0
---
ND
---
---
18-Jun-97
--- 5
ND
ND
---
ND
ND
---
ND
---
12.0
---
ND
---
---
2-Dec-97
--- 5
ND
ND
---
ND
ND
---
ND
---
23.0
---
ND
---
---
27-May-98
--- 5
ND
ND
---
ND
ND
---
ND
---
12.0
---
5.8
---
---
16-Nov-98
--- 5
ND
ND
---
ND
ND
---
ND
---
24.8
---
3.7
---
---
10-Sep-99
--- 5
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
16-Nov-99
--- 5
ND
ND
---
ND
---
ND
---
ND
---
7.0
---
ND
---
16-Dec-99
--- 5
---
---
---
---
---
---
---
---
---
7.0
---
---
---
10-May-00
--- 5
ND
ND
---
ND
---
ND
---
ND
---
8.0
---
ND
---
26-Oct-00
--- 5
ND
ND
---
ND
---
ND
---
ND
---
9.0
---
ND
---
18-Apr-01
--- 5
---
ND
---
ND
---
ND
---
ND
---
7.0
---
ND
---
27-Oct-01
--- 5
---
ND
---
ND
---
ND
---
ND
---
13.0
---
ND
---
I 0-Jun-02
--- 5
---
ND
---
ND
---
ND
---
ND
---
8.0
---
ND
---
13-Jun-02
--- 5
---
ND
---
ND
---
ND
---
ND
---
8.0
---
ND
---
19-Nov-02
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Jun-03
--- 5
---
ND
---
ND
---
ND
---
ND
---
12.0
---
ND
ND
30-Dec-03
--- 5
---
ND
---
ND
---
ND
---
ND
---
10.0
---
ND
ND
30-Jun-04
--- 5
---
ND
---
ND
---
ND
---
ND
---
9.3
---
ND
ND
29-Dec-04
--- 5
---
ND
---
ND
---
ND
---
ND
---
9.4
---
ND
ND
29-Jun-05
--- 5
---
ND
---
ND
---
ND
---
ND
---
8.0
---
ND
ND
29-Dec-05
--- 5
---
ND
---
ND
---
ND
---
ND
---
8.0
---
ND
ND
28-Jun-06
--- 5
---
ND
---
ND
---
ND
ND
ND
---
8.8
---
ND
ND
28-Dec-06
--- 5
---
ND
---
ND
---
ND
---
ND
5.3
6.0
---
ND
ND
NC 213 = NE gg/L (05/01/07)
12-Jul-07
--- 5
---
ND
---
ND
---
ND
---
ND
---
6.2
---
ND
ND
NC 2L = 70 gg/L (10/23/07)
19-Dec-07
--- 5
---
---
---
ND
---
ND
---
ND
---
7.2
---
ND
ND
8-Jul-08
--- 5.0
---
---
---
ND
---
ND
---
ND
---
9.8
---
ND
ND
16-Dec- 08
1.9 5.0
---
ND
---
ND
---
ND
---
0.91 B
---
4.2 1
---
ND
0.31 1
8-Jul-09
0.19 5.0
---
ND
---
ND
---
ND
---
ND
---
7.7
---
ND
ND
15-Dec-09
0.19 5.0
---
ND
---
ND
---
ND
---
ND
---
7.4
---
ND
ND
23-Jun-10
0.19 5.0
---
ND
---
ND
---
ND
---
ND
---
7.1
---
ND
ND
14-Dec-10
0.19 5.0
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
21-Jun-11
0.19 5.0
---
---
ND
ND
---
ND
---
ND
---
6.4
---
ND
ND
6-Dec- 11
0.19 5.0
---
---
ND
ND
---
ND
---
ND
---
3.0 1
---
ND
ND
13-Jun- 12
0.19 5.0
---
---
ND
ND
---
ND
---
ND
---
4.3 1
---
ND
ND
12-Dec- 12
0.19 5.0
---
---
ND
ND
---
ND
---
ND
---
3.3 1
---
ND
ND
29-Apr- 13
0.19 5.0
---
---
ND
ND
---
ND
---
ND
---
4.8 1
---
ND
ND
6-Aug- 13
0.19 5.0
---
---
ND
ND
---
ND
---
ND
---
3.6 1
---
ND
ND
25-Feb-14
0.19 5.0
---
---
ND
ND
---
ND
---
ND
---
3.7 1
---
ND
ND
13-Aug-14
0.19 5.0
---
---
ND
ND
---
ND
---
ND
---
2.8 1
---
ND
ND
12-Mar- 15
0.19 5.0
---
---
ND
ND
---
ND
---
ND
---
2.6 1
---
ND
ND
19-Aug- 15
0.19 5.0
---
---
ND
ND
---
ND
---
ND
---
3.1 1
---
0.35 1
ND
18-Feb-16
0.19 5.0
---
---
ND
ND
---
ND
---
ND
---
2.5 1
---
0.32 1
ND
11 -Aug- 16
0.19 5.0
---
---
ND
ND
---
ND
---
ND
---
2.7 1
---
0.5 1
ND
15-Feb-17
0.19 5.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
24-Aug- 17
0.19 5.0
---
---
ND
ND
---
ND
---
ND
---
1.4 1
---
0.68 1
ND
7-Feb-18
0.19 5.0
---
---
ND
ND
---
ND
---
ND
---
0.79 J
---
0.68 1
ND
16-Aug- 18
0.19 5.0
---
---
ND
ND
---
ND
---
ND
---
1.2 1
---
0.62 1
ND
Granville County - Oxford Landfill, Unit I Joyce Engineering
Permit 3901-CDLF-1997 Page 13 of 28

TABLE C-03: Historical Detected Organic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-IA
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
2-Hexanone
27-May-98
--- 50
ND
ND
ND
ND
---
ND
---
ND
---
61.0
---
---
16-Nov-98
--- 50
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
10-Sep-99
--- 50
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
16-Nov-99
--- 50
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
--- 50
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
26-Oct-00
--- 50
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
--- 50
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Oct-01
--- 50
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
13-Jun-02
--- 50
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
19-Nov-02
--- 50
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Jun-03
--- 50
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
30-Dec-03
--- 50
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
30-Jun-04
--- 50
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
--- 50
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Jun-05
--- 50
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
--- 50
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Jun-06
--- 50
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Dec-06
--- 50
---
ND
---
ND
---
ND
ND
ND
ND
ND
---
ND
ND
NC 213 = NE gg/L (05/01/07)
12-Jul-07
--- 50
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
GWPS = 280 gg/L (10/23/07)
19-Dec-07
--- 50
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
8-Jul-08
--- 50.0
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
16-Dec-08
0.46 50.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
8-Jul-09
0.46 50.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Dec-09
0.46 50.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
23-Jun-10
0.46 50.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
14-Dec-10
0.46 50.0
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
21-Jun-11
0.46 50.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Dec- 11
0.46 50.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Jun-12
0.46 50.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Dec- 12
0.46 50.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Apr- 13
0.46 50.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug- 13
0.46 50.0
---
---
ND
ND
---
0.55 J
---
ND
---
ND
---
ND
ND
25-Feb-14
0.46 50.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
0.46 50.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Mar- 15
0.46 50.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
19-Aug- 15
0.46 50.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
18-Feb-16
0.46 50.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
I I -Aug- 16
0.46 50.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Feb-17
0.46 50.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
24-Aug-17
0.46 50.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
7-Feb-18
0.46 50.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
16-Aug- 18
0.46 50.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
Granville County - Oxford Landfill, Unit I Joyce Engineering
Permit 3901-CDLF-1997 Page 14 of 28

TABLE C-03: Historical Detected Organic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-IA
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Methylene Chloride
14-Sep-94
--- to
ND
ND
ND
ND
---
ND
---
ND
---
ND
---
NA
2-Dec-94
--- to
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
8-Feb-95
--- to
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
2-Mar-95
--- 10
ND
ND
---
ND
ND
---
ND
---
ND
---
6.0
---
---
17-Nov-95
--- to
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
23-May-96
--- to
ND
ND
---
ND
ND
---
ND
---
ND
---
17.0
---
---
14-Nov-96
--- to
ND
ND
---
ND
ND
---
ND
---
ND
---
8.2
---
---
18-Jun-97
--- to
ND
ND
---
ND
ND
---
ND
---
ND
---
12.0
---
---
2-Dec-97
--- to
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
27-May-98
--- to
ND
ND
---
ND
ND
---
ND
---
ND
---
15.0
---
---
16-Nov-98
--- to
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
10-Sep-99
--- 10
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
-Nov-
-- 10
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
--- 10
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
26-Oct-00
--- to
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
--- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Oct-01
--- to
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
13-Jun-02
--- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
-Nov-
-- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Jun-03
--- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
30-Dec-03
--- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
30-Jun-04
--- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
--- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Jun-05
--- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
--- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Jun-06
--- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Dec-06
--- 6
---
ND
---
ND
---
ND
ND
ND
ND
ND
---
ND
ND
NC 213 = NE gg/L (05/01/07)
12-Jul-07
--- I
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
C 2L = 4.6 gg/L (10/23/07)
19-Dec-07
--- I
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
8-Jul-08
--- 2.0
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
16-Dec-08
0.97 2.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
8-Jul-09
0.97 2.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
9.6
15-Dec-09
0.97 2.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
C 2L = 5 gg/l, (2/5/10)
23-Jun-10
0.97 1.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
14-Dec-10
0.97 1.0
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
21-Jun-11
0.97 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Dec- 11
0.97 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Jun-12
0.97 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Dec- 12
0.97 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Apr- 13
0.97 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug- 13
0.97 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
25-Feb-14
0.97 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
1.9 1
13-Aug-14
0.97 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Mar- 15
0.97 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
19-Aug- 15
0.97 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
1.1
18-Feb-16
0.97 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
11-Aug-16
0.97 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Feb-17
0.97 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
1.6
24-Aug- 17
0.97 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
1.4 'C9
7-Feb-18
0.97 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
16-Aug- 18
0.97 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
Granville County - Oxford Landfill, Unit I Joyce Engineering
Permit 3901-CDLF-1997 Page 15 of 28

TABLE C-03: Historical Detected Organic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-IA
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Naphthalene
8-Jul-08
--- 10.0
---
---
ND
---
ND
---
ND
---
ND
---
2.9 1
ND
NC 2L = 21 gg/L (10/23/07)
16-Dec-08
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
NC 2B = NE gg/L (OS /01/07)
8-Jul-09
0.24 10.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Dec-09
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
NC 2L = 6 ttg/L (2/5/10)
23-Jun-10
0.24 10.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
14-Dec-10
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
21-Jun-11
0.24 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Dec- 11
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
13-Jun-12
0.24 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Dec-12
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
29-Apr- 13
0.24 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug- 13
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
25-Feb-14
0.24 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
12-Mar- 15
0.24 10.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
18-Feb-16
0.24 10.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
11-Aug-16
0.24 10.0
---
---
---
---
---
---
---
---
---
---
---
---
---
15-Feb-17
0.24 10.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
24-Aug-17
0.24 10.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
7-Feb-18
0.24 10.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
Granville County - Oxford Landfill, Unit I Joyce Engineering
Permit 3901-CDLF-1997 Page 16 of 28

TABLE C-03: Historical Detected Organic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-IA
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Toluene
18-Jun-97
--- 5
ND
ND
ND
13
---
ND
---
ND
---
ND
---
---
2-Dec-97
--- 5
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
27-May-98
--- 5
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
16-Nov-98
--- 5
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
10-Sep-99
--- 5
ND
ND
---
7
---
ND
---
ND
---
ND
---
ND
---
19-Oct-99
--- 5
---
---
---
ND
---
---
---
---
---
---
---
---
---
16-Nov-99
--- 5
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
--- 5
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
26-Oct-00
--- 5
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Oct-0 I
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
13-Jun-02
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
19-Nov-02
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Jun-03
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
30-Dec-03
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
30-Jun-04
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Jun-05
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Jun-06
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Dec-06
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
NC 213 = NE gg/L (05/01/07)
12-Jul-07
--- I
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
0.34 1
NC 2L = 1,000 µg/L (10/23/07)
19-Dec-07
--- I
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
8-Jul-08
--- 1.0
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
16-Dec-08
0.26 1.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
8-Jul-09
0.26 1.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Dec-09
0.26 1.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
NC 2L = 600 [tg/1- (2/5/10)
23-Jun-10
0.26 1.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
14-Dec-10
0.26 1.0
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
21-Jun-11
0.26 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Dec- 11
0.26 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Jun-12
0.26 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Dec- 12
0.26 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Apr- 13
0.26 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug- 13
0.26 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
25-Feb-14
0.26 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
0.26 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Mar-15
0.26 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
19-Aug-15
0.26 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
18-Feb-16
0.26 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
I1-Aug-16
0.26 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Feb-17
0.26 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
24-Aug-17
0.26 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
7-Feb-18
0.26 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
16-Aug- 18
0.26 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
Granville County - Oxford Landfill, Unit I Joyce Engineering
Permit 3901-CDLF-1997 Page 17 of 28

TABLE C-03: Historical Detected Organic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-IA
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Trichloroethene
2-Dec-97
--- 5
ND
ND
ND
ND
---
ND
---
2.0
---
ND
---
---
27-May-98
--- 5
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
16-Nov-98
--- 5
ND
ND
---
ND
ND
---
ND
---
2.7
---
2.9
---
---
10-Sep-99
--- 5
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
16-Nov-99
--- 5
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
--- 5
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
26-Oct-00
--- 5
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Oct-0 1
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
13-Jun-02
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
19-Nov-02
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Jun-03
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
30-Dec-03
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
30-Jun-04
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Jun-05
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Jun-06
--- 5
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Dec-06
--- 3
---
ND
---
ND
---
ND
ND
ND
ND
ND
---
ND
ND
NC 213 = NE gg/L (05/01/07)
12-Jul-07
--- I
---
ND
---
ND
---
ND
---
ND
---
0.68 J
---
ND
ND
NC 2L = 2.8 gg/L (10/23/07)
19-Dec-07
--- I
---
---
---
ND
---
ND
---
ND
---
0.64 J
---
ND
ND
8-Jul-08
--- 1.0
---
---
---
ND
---
ND
---
ND
---
0.51 1
---
ND
ND
16-Dec-08
0.47 1.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
8-Jul-09
0.47 1.0
---
ND
---
ND
---
ND
---
ND
---
0.53 J
---
ND
ND
15-Dec-09
0.47 1.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
NC 2L = 3 gg/L (2/5/10)
23-Jun-10
0.47 1.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
14-Dec-10
0.47 1.0
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
21-Jun-11
0.47 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Dec- 11
0.47 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Jun-12
0.47 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Dec- 12
0.47 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Apr- 13
0.47 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug- 13
0.47 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
25-Feb-14
0.47 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
0.47 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Mar- 15
0.47 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
19-Aug- 15
0.47 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
18-Feb-16
0.47 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
11 -Aug- 16
0.47 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Feb-17
0.47 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
24-Aug- 17
0.47 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
7-Feb-18
0.47 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
16-Aug-18
0.47 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
Granville County - Oxford Landfill, Unit I Joyce Engineering
Permit 3901-CDLF-1997 Page 18 of 28

TABLE C-03: Historical Detected Organic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-IA
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Vinyl chloride
14-Sep-94
--- 10
ND
ND
ND
ND
---
ND
---
ND
---
ND
---
---
2-Dec-94
--- to
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
8-Feb-95
--- 10
ND
ND
---
ND
ND
---
ND
---
26.0
---
ND
---
---
2-Mar-95
--- 10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
17-Nov-95
--- 10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
23-May-96
--- to
ND
ND
---
ND
ND
---
ND
---
13.0
---
ND
---
---
-Nov-
-- to
ND
ND
---
ND
ND
---
ND
---
17.0
---
ND
---
---
18-Jun-97
--- 10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
2-Dec-97
--- 10
ND
ND
---
ND
2.0
---
ND
---
33.0
---
ND
---
---
27-May-98
--- to
ND
ND
---
ND
ND
---
ND
---
13.0
---
ND
---
---
-Nov-
-- to
ND
ND
---
ND
ND
---
ND
---
25.8
---
ND
---
---
10-Sep-99
--- 10
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
-Nov-
-- 10
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
--- 10
ND
ND
---
ND
---
ND
---
ND
---
12.0
---
ND
---
26-Oct-00
--- 10
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
--- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Oct-01
--- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
I O-Jun-02
--- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
13-Jun-02
--- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
-Nov-
-- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Jun-03
--- 10
---
ND
---
ND
---
ND
---
ND
---
26.9
---
ND
ND
30-Dec-03
--- 10
---
ND
---
ND
---
ND
---
ND
---
10.0
---
ND
ND
30-Jun-04
--- 10
---
ND
---
ND
---
ND
---
ND
---
11.0
---
ND
ND
29-Dec-04
--- 10
---
ND
---
ND
---
ND
---
ND
---
12.0
---
ND
ND
29-Jun-05
--- 10
---
ND
---
ND
---
ND
---
ND
---
14.0
---
ND
ND
29-Dec-05
--- 10
---
ND
---
ND
---
ND
---
ND
---
15.0
---
ND
ND
28-Jun-06
--- 10
---
ND
---
ND
---
ND
---
ND
---
12.5
---
ND
ND
28-Dec-06
--- 6
---
ND
---
ND
---
ND
ND
ND
8.1
8.9
---
ND
ND
C 213 = NE gg/L (05/01/07)
12-Jul-07
--- I
---
ND
---
ND
---
ND
---
ND
---
8.3
---
ND
ND
NC 2L = 0.015 µg/L (10/23/07)
19-Dec-07
--- 1
---
---
---
ND
---
ND
---
ND
---
8.4
---
ND
ND
8-Jul-08
--- 1.0
---
---
---
ND
---
ND
---
ND
---
10.6
---
ND
ND
16-Dec-08
0.62 1.0
---
ND
---
ND
---
ND
---
ND
---
5.0
---
ND
ND
8-Jul-09
0.62 1.0
---
ND
---
ND
---
ND
---
ND
---
13.3
---
ND
ND
15-Dec-09
0.62 1.0
---
ND
---
ND
---
ND
---
ND
---
9.9
---
ND
ND
NC 2L = 0.03 [tg/L (2/5/10)
23-Jun-10
0.62 1.0
---
ND
---
ND
---
ND
---
ND
---
11.2
---
ND
ND
14-Dec-10
0.62 1.0
---
---
---
ND
---
ND
---
ND
---
8.4
---
ND
ND
21-Jun-11
0.62 1.0
---
---
ND
ND
---
ND
---
ND
---
10.5
---
ND
ND
6-Dec- 11
0.62 1.0
---
---
ND
ND
---
ND
---
ND
---
4.1
---
ND
ND
13-Jun-12
0.62 1.0
---
---
ND
ND
---
ND
---
ND
---
6.6
---
ND
ND
12-Dec- 12
0.62 1.0
---
---
ND
ND
---
ND
---
ND
---
3.3
---
ND
ND
29-Apr- 13
0.62 1.0
---
---
ND
ND
---
ND
---
ND
---
7.6
---
ND
ND
6-Aug- 13
0.62 1.0
---
---
ND
ND
---
ND
---
ND
---
9.1
---
ND
ND
25-Feb-14
0.62 1.0
---
---
ND
ND
---
ND
---
ND
---
6.8
---
ND
ND
13-Aug-14
0.62 1.0
---
---
ND
ND
---
ND
---
ND
---
5.4
---
ND
ND
12-Mar-15
0.62 1.0
---
---
ND
ND
---
ND
---
ND
---
5.1
---
ND
ND
19-Aug-15
0.62 1.0
---
---
ND
ND
---
ND
---
ND
---
5.0
---
ND
ND
18-Feb-16
0.62 1.0
---
---
ND
ND
---
ND
---
ND
---
5.4
---
ND
ND
11-Aug-16
0.62 1.0
---
---
ND
ND
---
ND
---
ND
---
5.6
---
ND
ND
15-Feb-17
0.62 1.0
---
---
ND
ND
---
ND
---
ND
---
1.4
---
ND
ND
24-Aug-17
0.62 1.0
---
---
ND
ND
---
ND
---
ND
---
2.1
---
ND
ND
7-Feb-18
0.62 1.0
---
---
ND
ND
---
ND
---
ND
---
1.8
---
ND
ND
16-Aug-18
0.62 1.0
---
---
ND
ND
---
ND
---
ND
---
3.5
---
ND
ND
Granville County - Oxford Landfill, Unit I Joyce Engineering
Permit 3901-CDLF-1997 Page 19 of 28

TABLE C-03: Historical Detected Organic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-IA
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Bis(2-ethylhexyl)phthalate
21-Jun-11
0.79 15.0
---
---
ND
2.5 1
---
ND
---
4.5 1
---
ND
---
ND
ND
NC 2L = 3 gg/L (2/5/10)
6-Dec-11
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
13-Jun-12
0.79 15.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Dec-12
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
29-Apr- 13
0.79 15.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug- 13
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
25-Feb-14
0.79 15.0
---
---
ND
ND
---
40.4
---
5.0 1
---
ND
---
ND
ND
Resample >
15-Apr-14
0.79 15.0
---
---
---
---
---
ND
---
---
---
---
---
---
ND
13-Aug-14
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
12-Mar- 15
0.49 15.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
18-Feb-16
0.85 15.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
11-Aug-16
0.85 15.0
---
---
---
---
---
---
---
---
---
---
---
---
---
15-Feb-17
0.85 15.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
24-Aug- 17
2.3 15.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
7-Feb-18
2.3 15.3
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
Diethylphthalate
17-Nov-95
--- 10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
2-Dec-97
--- 10
ND
ND
---
ND
ND
---
24.0
---
ND
---
ND
---
---
23-Mar-98
--- 10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
27-May-98
--- 10
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
-Nov-
-- 10
ND
ND
---
ND
ND
---
10
---
ND
---
ND
---
---
10-Sep-99
--- 10
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
-Nov-
-- 10
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
--- 10
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
26-Oct-00
--- to
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
--- 10
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
-Jun-
-- 10.5
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Jun-03
--- 10
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
30-Dec-03
--- 10
---
---
---
---
---
---
---
---
---
---
---
---
---
30-Jun-04
--- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
29-Jun-05
--- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Jun-06
--- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Dec-06
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
NC 2B = NE gg/L (05/01/07)
12-Jul-07
--- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
NC 2L = 5,000 µg/L (10/23/07)
19-Dec-07
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
8-Jul-08
--- 20.0
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
16-Dec-08
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
8-Jul-09
2.7 11.1
---
ND
---
---
---
ND
---
ND
---
ND
---
ND
ND
15-Dec-09
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
NC 2L = 6,000 µg/L (2/5/10)
23-Jun-10
3.9 14.3
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
14-Dec-10
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
21-Jun-11
0.58 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Dec- 11
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
13-Jun-12
0.58 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Dec-12
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
29-Apr- 13
0.58 6000
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug- 13
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
25-Feb-14
0.58 6000
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
12-Mar- 15
0.91 6000
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
18-Feb-16
1.3 6000
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
11-Aug-16
1.3 6000
---
---
---
---
---
---
---
---
15-Feb-17
1.3 6000
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
24-Aug- 17
1.6 6000
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
7-Feb-18
1.7 6120
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
Granville County - Oxford Landfill, Unit I Joyce Engineering
Permit 3901-CDLF-1997 Page 20 of 28

TABLE C-03: Historical Detected Organic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL PIL
MW-1
MW-1A
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Benzo(g,h,i)perylene
21-Jun-11
0.79 15.0
---
---
ND
ND
---
ND
---
ND
---
1.1 1
---
ND
ND
NC 2L = 200 gg/L (2/5/10)
6-Dec- I I
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
13-Jun-12
0.38 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Dec-12
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
29-Apr- 13
0.38 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug- 13
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
25-Feb-14
0.38 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
12-Mar-15
0.45 10.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
18-Feb-16
0.38 10.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
11-Aug-16
0.38 10.0
---
---
---
---
---
---
---
---
---
---
---
---
---
15-Feb-17
0.38 10.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
24-Aug- 17
2.1 10.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
7-Feb-18
2.1 10.2
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
Dibenz(a,h)anthracene
21-Jun-11
0.79 15.0
---
---
ND
ND
---
ND
---
ND
---
1.2 1
---
ND
ND
NC 2L = 0.005 µg/L (2/5/10)
6-Dec- 11
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
13-Jun-12
0.55 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Dec-12
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
29-Apr- 13
0.55 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug- 13
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
25-Feb-14
0.55 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
12-Mar- 15
0.49 10.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
18-Feb-16
0.55 10.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
11-Aug-16
0.55 10.0
---
---
---
---
---
---
---
---
---
---
---
---
---
15-Feb-17
0.55 10.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
24-Aug- 17
2.0 10.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
7-Feb-18
2.1 10.2
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
Indeno(1,2,3-cd)pyrene
21-Jun-11
0.79 15.0
---
---
ND
ND
---
ND
---
ND
---
1.2 1
---
ND
ND
NC 2L = 0.05 gg/L (2/5/10)
6-Dec-1 I
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
13-Jun-12
0.29 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Dec-12
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
29-Apr- 13
0.29 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug- 13
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
25-Feb-14
0.29 10.0
---
---
ND
---
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
12-Mar- 15
0.53 10.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
18-Feb-16
0.29 10.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
11-Aug-16
0.29 10.0
---
---
---
---
---
---
---
---
---
---
---
---
---
15-Feb-17
0.29 10.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
24-Aug-17
2.0 10.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
7-Feb-18
2.1 10.2
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
Granville County - Oxford Landfill, Unit I Joyce Engineering
Permit 3901-CDLF-1997 Page 21 of 28

TABLE C-03: Historical Detected Organic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-IA
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Phorate
17-Nov-95
--- to
ND
ND
ND
ND
---
ND
---
ND
---
ND
---
---
2-Dec-97
--- to
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
-Nov-
-- to
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
10-Sep-99
--- to
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
--- to
---
---
---
ND
---
1.0
---
ND
---
0.8
---
ND
---
26-Oct-00
--- 1.5
---
---
---
ND
---
5.2
---
ND
---
ND
---
ND
---
18-Apr-01
--- 10
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
13-Jun-02
--- 0.5
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Jun-03
--- 10
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
30-Dec-03
--- 10
---
---
---
---
---
---
---
---
---
---
---
---
---
30-Jun-04
--- to
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
29-Jun-05
--- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
--- 10
---
---
---
---
---
---
---
---
---
---
---
---
---
28-Jun-06
--- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Dec-06
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
NC 213 = NE gg/L (05/01/07)
12-Jul-07
--- 10
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
NC 2L = 1.4 gg/L (10/23/07)
19-Dec-07
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
8-JUI-08
--- 40.0
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
16-Dec-08
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
8-JUI-09
6.6 22.2
---
ND
---
---
---
ND
---
ND
---
ND
---
ND
ND
15-Dec-09
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
NC 2L = I gg/L (2/5/10)
23-Jun-10
7.7 28.6
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
14-Dec-10
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
21-Jun-11
5.4 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Dec- 11
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
13-Jun-12
5.4 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Dec-12
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
29-Apr- 13
5.4 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug- 13
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
25-Feb-14
5.4 10.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
12-Mar-15
0.83 10.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
18-Feb-16
1.1 10.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
11-Aug-16
1.1 10.0
---
---
---
---
---
---
---
---
---
---
---
---
---
15-Feb-17
1.1 10.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
24-Aug-17
1.7 10.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
7-Feb-18
1.8 10.2
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
Granville County - Oxford Landfill, Unit I Joyce Engineering
Permit 3901-CDLF-1997 Page 22 of 28

TABLE C-03: Historical Detected Organic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-IA
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Aldrin
17-Nov-95
--- 0.05
ND
ND
ND
ND
---
ND
---
ND
---
ND
---
---
2-Dec-97
--- 0.05
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
23-Mar-98
--- 0.05
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
27-May-98
--- 0.05
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
16-Nov-98
--- 0.05
ND
ND
---
ND
ND
---
0.073
---
ND
---
ND
---
---
10-Sep-99
--- 0.05
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
16-Nov-99
--- 0.05
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
-May-
--- 0.05
---
---
---
ND
---
ND
---
ND
--
ND
---
ND
---
26-Oct-00
--- 0.05
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
--- 0.05
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
-Jun-
--- 0.05
---
---
---
ND
---
ND
---
ND
--
ND
---
ND
---
7-Jun-
--- 0.05
---
---
---
ND
---
ND
--
ND
---
ND
---
ND
---
30-Dec-03
--- 0.05
---
---
---
---
---
---
---
---
---
---
---
---
---
30-Jun-04
--- 0.05
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
29-Jun-05
--- 0.05
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
--- 0.05
---
---
---
---
---
---
---
---
---
28-Jun-06
--- 0.05
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Dec-06
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
NC 213 = NE µg/L (05/01/07)
12-Jul-07
--- 0.05
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
NC 2L = NE µg/L (10/23/07)
19-Dec-07
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
8-Jul-08
--- 0.050
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
16-Dec-08
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
8-Jul-09
0.050 0.050
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Dec-09
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
23-Jun-10
0.00053 0.011
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
14-Dec-10
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
21-Jun-11
0.00050 0.050
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Dec-11
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
13-Jun-12
0.05 0.05
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Dec-12
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
29-Apr-13
0.050 0.050
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug-13
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
25-Feb-14
0.050 0.050
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
-Mar- 5
0.050 0.050---
--
ND
---
---
---
---
---
---
ND
---
---
ND
--
ND
---
ND
---
---
ND
11-Aug-16
0.050 0.050
---
---
---
---
---
---
---
---
---
5-Fe - 7
0.050 0.050---
--
ND
---
---
---
---
---
---
ND
---
---
ND
7-Feb-18
0.053 0.053
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 Page 23 of28

TABLE C-03: Historical Detected Organic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-IA
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Alpha-BHC
17-Nov-95
--- 0.05
ND
ND
ND
ND
---
ND
---
ND
---
ND
---
---
2-Dec-97
--- 0.05
ND
ND
---
ND
ND
---
0.20
---
ND
---
ND
---
---
23-Mar-98
--- 0.05
ND
ND
---
ND
0.073
---
0.16
---
ND
---
ND
---
---
27-May-98
--- 0.05
ND
ND
---
ND
ND
---
ND
---
0.095
---
0.053
---
---
16-Nov-98
--- 0.05
ND
ND
---
ND
ND
---
0.23
---
ND
---
ND
---
---
10-Sep-99
--- 0.05
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
16-Nov-99
--- 0.05
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
-May-
--- 0.05
---
---
---
ND
---
ND
---
ND
--
ND
---
ND
---
26-Oct-00
--- 0.05
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
--- 0.05
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
-Jun-
--- 0.05
---
---
---
ND
---
ND
---
ND
--
ND
---
ND
---
7-Jun-
--- 0.05
---
---
---
ND
---
ND
--
ND
---
ND
---
ND
---
30-Dec-03
--- 0.05
---
---
---
---
---
---
---
---
---
---
---
---
---
30-Jun-04
--- 0.05
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
29-Jun-05
--- 0.05
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
--- 0.05
---
---
---
---
---
---
---
---
---
28-Jun-06
--- 0.05
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Dec-06
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
NC 213 = NE µg/L (05/01/07)
12-Jul-07
--- 0.05
---
ND
---
ND
---
ND
---
ND
---
ND
GWPS = 0.006 µg/L (10/23/07)
19-Dec-07
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
8-Jul-08
--- 0.050
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
16-Dec-08
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
8-Ju -09
0.050 0.050
---
ND
---
ND
---
ND
---
ND
--
ND
---
ND
ND
15-Dec-09
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
23-Jun-10
0.00032 0.011
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
14-Dec-10
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
21-Jun-11
0.00030 0.050
---
ND
ND
---
0.054
---
ND
---
ND
---
ND
ND
Resample>
28-Jul-11
0.00030 0.050
---
---
---
---
---
ND
---
---
---
---
---
---
ND
6-Dec-11
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
13-Jun-12
0.05 0.05
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Dec-12
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
29-Apr-13
0.050 0.050
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug-13
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
25-Feb-14
0.050 0.050
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
12-Mar-15
0.050 0.050
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
18-Feb-16
0.050 0.050
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
11-Aug-16
0.050 0.050
---
---
---
---
---
---
---
---
---
15-Feb-17
0.050 0.050
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
7-Feb-18
0.053 0.053
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 Page 24 of28

TABLE C-03: Historical Detected Organic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-IA
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Beta-BHC
27-Jun-03
--- 1.05
---
ND
ND
---
0.068
---
ND
---
ND
---
ND
---
30-Dec-03
--- 0.05
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
30-Jun-04
--- 0.05
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
--- 0.05
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Jun-05
--- 0.05
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
--- 0.05
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Jun-06
--- 0.05
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Dec-06
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
C 213 = NE gg/L (05/01/07)
12-Jul-07
--- 0.05
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
GWPS = 0.019 gg/L (10/23/07)
19-Dec-07
--- 0.05
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
8-Jul-08
--- 0.050
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
16-Dec-08
0.050 0.050
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
8-Jul-09
0.050 0.050
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Dec- 09
0.010 0.100
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
23-Jun-10
0.00053 0.011
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
14-Dec-10
0.00050 0.050
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
21-Jun-11
0.00050 0.050
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Dec- 11
0.050 0.050
---
---
ND
ND
---
ND
---
ND
---
0.059
---
ND
ND
Resample >
25-Jan-12
0.050 0.050
---
---
ND
---
---
---
---
---
---
0.082
---
---
ND
13-Jun-12
0.050 0.050
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Dec-12
0.050 0.050
---
---
ND
ND
---
ND
---
ND
---
0.078
---
ND
ND
29-Apr- 13
0.050 0.050
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug- 13
0.050 0.050
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
25-Feb-14
0.050 0.050
---
---
ND
ND
---
ND
---
ND
---
0.056
---
ND
ND
13-Aug-14
0.050 0.050
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
12-Mar-15
0.050 0.050
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
19-Aug-15
0.050 0.050
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
18-Feb-16
0.050 0.050
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
11-Aug-16
0.050 0.050
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
15-Feb-17
0.050 0.050
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
7-Feb-18
0.053 0.053
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
4,4'-DDT
23-Jun-10
0.0037 0.010
---
ND
---
ND
---
ND
---
ND
---
0.016 J
---
ND
ND
C 2L = 0.1 µg/L (2/5/10)
14-Dec-10
--- ---
---
---
---
---
---
---
---
---
---
ND
---
---
---
NC 213 = 0.001 µg/L (05/01/07)
21-Jun-11
0.0036 0.10
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Dec- I I
--- ---
---
---
---
---
---
---
---
---
---
ND
---
---
---
13-Jun-12
0.05 0.10
---
---
ND
ND
---
ND
---
ND
---
0.090 1
---
ND
ND
12-Dec-12
--- ---
---
---
---
---
---
---
---
---
---
ND
---
---
---
29-Apr- 13
0.050 0.10
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug- 13
--- ---
---
---
---
---
---
---
---
---
---
ND
---
---
---
25-Feb-14
0.050 0.10
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
12-Mar-15
0.050 0.10
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
---
---
ND
11-Aug-16
0.050 0.10
---
---
---
---
---
---
---
---
---
---
---
---
---
15-Feb-17
0.050 0.10
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
7-Feb-18
0.053 0.11
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
Granville County - Oxford Landfill, Unit I Joyce Engineering
Permit 3901-CDLF-1997 Page 25 of 28

TABLE C-03: Historical Detected Organic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-IA
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Dieldrin
17-Nov-95
--- 0.1
ND
ND
ND
ND
---
ND
---
ND
---
ND
---
---
2-Dec-97
--- 0.1
ND
ND
---
ND
ND
---
0.10
---
ND
---
ND
---
---
23-Mar-98
--- 0.05
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
27-May-98
--- 0.05
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
16-Nov-98
--- 0.1
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
10-Sep-99
--- 0.1
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
16-Nov-99
--- 0.05
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
--- 0.1
---
ND
---
ND
---
ND
---
ND
---
ND
---
26-Oct-00
--- 0.1
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
--- 0.1
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
13-Jun-02
--- 0.1
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
7-Jun-
--- 0.1
---
---
---
ND
---
ND
--
ND
---
ND
---
ND
---
30-Dec-03
--- 0.1
---
---
---
---
---
---
---
---
---
30-Jun-04
--- 0.1
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
29-Jun-05
--- 0.1
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
--- 0.1
---
---
---
---
---
---
---
---
---
---
---
---
---
28-Jun-06
--- 0.1
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Dec-06
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
NC 213 = 0.002 µg/L (05/01/07)
12-Jul-07
--- 0.075
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
NC 2L = 0.0022 µg/L (10/23/07)
19-Dec-07
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
8-Jul-08
--- 0.075
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
16-Dec-08
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
8-Jul-09
0.050 0.075
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Dec-09
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
NC 2L = 0.002 µ (2 5 10)
23-Jun-10
0.00053 0.011
--
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
14-Dec-10
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
21-Jun-11
0.00050 0.075
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Dec-11
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
-Jun-
5 0.05
---
---
ND
ND
---
ND
--
ND
---
ND
---
ND
ND
12-Dec-12
--- ---
---
---
---
---
---
---
---
---
---
ND
---
---
---
- pr- 13
0.05075
---
---
ND
ND
---
ND
---
ND
---
ND
--
ND
ND
6-Aug-13
--- ---
---
---
---
---
---
---
---
---
---
ND
---
---
---
5-Fe -0.05075
---
---
ND
ND
---
ND
--
ND
---
ND
---
ND
ND
13-Aug-14
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
-Mar- 5
5 75
---
--
ND
---
---
---
---
---
---
ND
---
---
ND
--
ND
---
ND
---
---
ND
11-Aug-16
0.050 0.075
---
---
---
---
---
---
---
---
---
15-Feb-17
0.050 0.075
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
7-Feb-18
0.053 0.080
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
Endosulfan I
21-Jun-11
0.00070 0.10
---
---
ND
ND
---
0.52
---
ND
---
ND
---
ND
ND
NC 2L = 40 µg/L (2/5/10) Resample >
28-Jul-11
0.00070 0.10
---
---
---
---
---
ND
---
---
---
---
---
---
ND
6-Dec-II
--- ---
---
---
---
---
---
ND
---
---
---
---
---
---
ND
13-Jun-12
0.050 0.10
---
---
ND
ND
---
0.33
---
ND
---
ND
---
ND
ND
12-Dec-12
0.050---
---
ND
ND
--
1.33
---
ND
---
ND
---
ND
ND
29-Apr-13
0.050 0.10
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug-13
0.050 0.10
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
25-Feb-14
0.050 0.10
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
0.050 0.10
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
12-Mar-15
0.050 0.10
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
19-Aug-15
0.050 0.10
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
18-Feb-16
0.050 0.10
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
11-Aug-16
0.050 0.10
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
15-Feb-17
0.050 0.10
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
7-Feb-18
0.053 0.11
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 Page 26 of 28

TABLE C-03: Historical Detected Organic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-IA
MW-7
MW-2
MW-3
MW-3R
MW-4
MW-4R
MW-5
MW-5R
MW-6
MW-6R
Blanks
Endosulfan Sulfate
13-Jun-12
0.050 0.10
---
---
ND
ND
---
0.090 1
---
ND
---
ND
---
ND
ND
12-Dec-12
--- ---
---
---
---
---
---
ND
---
---
---
---
---
---
---
29-Apr- 13
0.050 0.10
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug- 13
--- ---
---
---
---
---
---
---
---
---
---
ND
---
---
---
25-Feb-14
0.050 0.10
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
12-Mar- 15
0.05 0.10
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
18-Feb-16
0.05 0.10
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
11-Aug-16
0.05 0.10
---
---
---
---
---
---
---
---
---
---
---
---
---
15-Feb-17
0.05 0.10
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
7-Feb-18
0.05 0.11
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
Heptachlor
17-Nov-95
--- 0.05
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
2-Dec-97
--- 0.05
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
23-Mar-98
--- 0.05
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
27-May-98
--- 0.05
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
16-Nov-98
--- 0.05
ND
ND
---
ND
ND
---
0.068
---
ND
---
ND
---
---
10-Sep-99
--- 0.05
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
16-Nov-99
--- 0.05
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
--- 0.05
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
26-Oct-00
--- 0.05
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
--- 0.05
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
13-Jun-02
--- 0.05
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
27-Jun-03
--- 0.05
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
30-Dec-03
--- 0.05
---
---
---
---
---
---
---
---
---
---
---
---
ND
30-Jun-04
--- 0.05
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
--- 0.05
---
---
---
---
---
---
---
---
---
---
---
---
ND
29-Jun-05
--- 0.05
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
--- 0.05
---
---
---
---
---
---
---
---
---
---
---
---
ND
28-Jun- 06
--- 0.05
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Dec-06
--- 0.05
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
NC 213 = 0.004 µg/L (05/01/07)
12-Jul-07
--- 0.05
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
NC 2L = 0.0078 gg/L (10/23/07)
19-Dec-07
--- 0.05
---
---
---
---
---
---
---
---
---
---
---
---
ND
8-Jul-08
--- 0.050
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
16-Dec-08
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
8-Jul-09
0.050 0.050
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Dec-09
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
NC 2L = 0.008 gg/L (2/5/10)
23-Jun-10
0.0016 0.011
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
14-Dec- 10
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
21-Jun-11
0.0015 0.050
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Dec- 11
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
13-Jun-12
0.05 0.05
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
12-Dec-12
--- ---
---
---
---
---
---
ND
---
---
---
---
---
---
---
29-Apr- 13
0.050 0.050
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug- 13
--- ---
---
---
---
---
---
---
---
---
---
ND
---
---
---
25-Feb-14
0.050 0.050
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
12-Mar-15
0.050 0.050
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
18-Feb-16
0.050 0.050
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
11-Aug-16
0.050 0.050
---
---
---
---
---
---
---
---
---
---
---
---
15-Feb-17
0.050 0.050
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
7-Feb-18
0.053 0.053
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
Granville County - Oxford Landfill, Unit I Joyce Engineering
Permit 3901-CDLF-1997 Page 27 of 28

TABLE C-03: Historical Detected Organic Constituents in Compliance Wells
Analyte
Sample Collection Date
DL RL
MW-1
MW-IA
MW-7
MW-2
MW-3
MW-311
MW-4
MW-4R
MW-5
MW-511
MW-6
MW-6R
Blanks
Methoxychlor
17-Nov-95
--- 1
ND
ND
ND
ND
---
ND
---
ND
---
ND
---
---
2-Dec-97
--- 1
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
23-Mar-98
--- 2
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
27-May-98
--- 2
ND
ND
---
ND
ND
---
ND
---
ND
---
ND
---
---
16-Nov-98
1
ND
ND
---
ND
ND
---
0.51
---
ND
---
ND
---
---
10-Sep-99
--- 1
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
16-Nov-99
--- 2
ND
ND
---
ND
---
ND
---
ND
---
ND
---
ND
---
10-May-00
--- 1
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
26-Oct-00
--- 1
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
18-Apr-01
--- 1
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
13-Jun-02
--- 1
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
---
30-Dec-03
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
30-Jun-04
--- 1
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-04
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
-Jun- 5
-- 1
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
29-Dec-05
--- 1
---
---
---
---
---
---
---
---
---
---
---
---
---
28-Jun-06
--- 1
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
28-Dec-06
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
NC 2B = 0.03 µ (OS O1 07)
12-Jul-07
--- 1
--
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
NC 2L = 35 µg/L (10/23/07)
19-Dec-07
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
8-Jul-08
--- 1.0
---
---
---
ND
---
ND
---
ND
---
ND
---
ND
ND
16-Dec-08
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
8-Jul-09
0.50 1.0
---
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
15-Dec-09
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
NC 2L = 40 µ (2 5 10)
23-Jun-10
0.0074 1.1
--
ND
---
ND
---
ND
---
ND
---
ND
---
ND
ND
14-Dec-10
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
21-Jun-11
0.0070 1.0
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Dec-11
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
-Jun-
5 0.15
---
---
ND
ND
---
ND
---
ND
---
ND
--
ND
ND
12-Dec-12
--- ---
---
---
---
---
---
ND
---
---
---
---
---
---
---
29-Apr-13
0.15 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
6-Aug-13
--- ---
---
---
---
---
---
---
---
---
---
ND
---
---
---
25-Feb-14
0.15 1.0
---
---
ND
ND
---
ND
---
ND
---
ND
---
ND
ND
13-Aug-14
--- ---
---
---
---
---
---
---
---
---
---
---
---
---
---
12-Mar-15
0.15 1.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
18-Feb-16
0.15 1.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
11-Aug-16
0.15 1.0
---
---
---
---
---
---
---
---
---
15-Feb-17
0.15 1.0
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
7-Feb-18
0.16 1.1
---
---
ND
---
---
---
---
---
---
ND
---
---
ND
1,4-Dioxane (p-Dioxane)
16-Aug-18
1.90 2.0
--
---
ND
ND
--
16.5
21.2
--
41.6
ND
ND
NC 2L = 3.0 2018
Notes:
All concentrations are in micrograms per liter (µg/L).
RL = Reporting Limit (Lab. Reporting Limit for September 1994 - May 1999; NC PQL for October 1999 - December 2006; and SWSL for December 2006 - present).
DL = Laboratory detection limit.
J = Estimated value between the DL and the RL.
B = Blank -qualified data; result is expected to be biased high based on concentrations in the blanks.
ND = Not detected above laboratory reporting limit.
NC 2L = North Carolina Groundwater Standards from 15A NCAC 2L.0202.
GWPS = Groundwater Protection Standards established by the DENR Solid Waste Section (SWS).
When the NC 2L has not been established, the GWPS will be used.
Bold values for groundwater are above the NC 2L Standards or GWPS.
--- = Well was not monitored and/or not reported.
# = Constituent is included on the NC Appendix U list but not on the NC Appendix I list.
There was a resamplinging event on August 2, 2007 for MW-16D because the prevoius samples from the May 2007 were analyzed out of hold time. There were no detects in the resample.
Volatile organics (8260) for MW-9 for November 10, 2004 sampling event were unable to be analyzed and were resampled on December 1, 2004.
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 Page 28 of28

TABLE C-04: Historical Detected COCs in Performance and Sentinel Wells
Sample
Anal to
Collection Date
RL
NES-IS
NES-113
NES-2S
NES-213
Blanks
ORGANICS
Vinyl Chloride
18-May-04
10
ND
ND
ND
ND
ND
30-Jun-04
10
ND
ND
ND
ND
ND
28-Dec-06
6
ND
NS
ND
NS
ND
C 2L = 0.015 µg/L (10/23/07)
16-Dec-08
1
ND
ND
ND
ND
ND
8-Jul-09
1
ND
ND
ND
ND
ND
15-Dec-09
2
ND
ND
ND
ND
ND
C 2L = 0.03 µg/L (01/01/10)
23-Jun-10
1.0
ND
ND
ND
ND
ND
14-Dec-10
1.0
ND
NS
ND
NS
ND
21-Jun-11
1.0
ND
ND
ND
ND
ND
5-Dec-11
1.0
ND
ND
ND
ND
ND
13-Jun-12
1.0
ND
ND
ND
ND
ND
10-Dec-12
1.0
ND
ND
ND
ND
ND
30-Apr-13
1.0
ND
ND
ND
ND
ND
7-Aug-13
1.0
ND
NS
ND
NS
ND
25-Feb-14
1.0
ND
ND
ND
ND
ND
13-Aug-14
1.0
NS
NS
ND
NS
ND
12-Mar-15
1.0
NS
NS
ND
NS
ND
19-Aug-15
LO
NS
NS
ND
NS
ND
18-Feb-16
1.0
NS
NS
ND
NS
ND
11-Aug-16
LO
NS
NS
ND
NS
ND
15-Feb-17
1.0
NS
NS
ND
NS
ND
24-Aug-17
1.0
NS
NS
ND
NS
ND
7-Feb-18
1.0
NS
NS
ND
NS
ND
15-Aug-18
1.0
NS
NS
ND
NS
ND
1,1-Dichloroethane *
18-May-04
5
ND
ND
ND
ND
ND
30-Jun-04
5
ND
ND
ND
ND
ND
28-Dec-06
5
ND
NS
ND
NS
ND
C 2L = 70 µg/L (10/23/07)
16-Dec-08
5
NS
NS
NS
NS
NS
8-Jul-09
5
NS
NS
NS
NS
NS
15-Dec-09
5
NS
NS
NS
NS
NS
C 2L = 6 µg/L (01/01/10)
23-Jun-10
5.0
NS
NS
ND*
ND*
ND
14-Dec-10
5.0
0.32 J
NS
ND
NS
ND
21-Jun-11
5.0
ND
0.33 J
ND
ND
ND
5-Dec-11
5.0
ND
ND
ND
ND
ND
13-Jun-12
5.0
ND
ND
ND
ND
ND
10-Dec-12
5.0
ND
0.38 J
ND
ND
ND
30-Apr-13
5.0
ND
0.38 J
ND
ND
ND
7-Aug-13
5.0
ND
NS
ND
NS
ND
25-Feb-14
5.0
ND
0.33 J
ND
ND
ND
13-Aug-14
5.0
NS
NS
ND
NS
ND
12-Mar-15
5.0
NS
NS
ND
NS
ND
18-Feb-16
5.0
NS
NS
ND
NS
ND
11-Aug-16
5.0
NS
NS
NS
NS
NS
15-Feb-17
5.0
NS
NS
NS
NS
NS
24-Aug-17
5.0
NS
NS
NS
NS
NS
15-Aug-18
5.0
NS
NS
ND
NS
ND
beta-BHC *
13-Jun-12
5.0
ND
ND
ND
ND
ND
10-Dec-12
5.0
ND
ND
ND
ND
ND
GWPS = 0.019 µg/L (10/23/07)
30-Apr-13
5.0
ND
ND
ND
ND
ND
7-Aug-13
5.0
ND
ND
ND
ND
ND
25-Feb-14
5.0
ND
ND
ND
ND
ND
13-Aug-14
5.0
NS
NS
ND
NS
ND
12-Mar-15
5.0
NS
NS
ND
NS
ND
18-Feb-16
5.0
NS
NS
ND
NS
ND
11-Aug-16
5.0
NS
NS
NS
NS
NS
15-Feb-17
5.0
NS
NS
NS
NS
NS
24-Aug-17
5.0
NS
NS
NS
NS
NS
15-Aug-18
5.0
NS
NS
NS
NS
NS
Notes:
COC = Constituents of Concern. µg/L = micrograms per liter = parts per billion.
RL = Reporting Limit. J = Estimated concentraion below the RL.
B = Blank -qualified detection.
* 1,1-DCA was added to the COC list and Benzene and cis-1,2-dichloroethylene ND = Not detected above the laboratory detection limit.
were dropped following DENR SWS approval dataed January 27, 2011. NS = Not sampled for this parameter during this event.
1,1-DCA and beta-BHC were dropped from the COC list following DENR-SWS
approval dated July 30, 2015.
Granville County - Oxford Landfill, Unit 1
Permit 3901-CDLF-1997 Joyce Engineering

TABLE C-05: Historical Detected Constituents in Surface Water
Sample
Analyte
Collection Date
DL
RL
SW-1
SW-2
Blanks
INORGANICS
Antimony
23-Jun-10
2.6
6.0
2.8 J
ND
ND
NC 2B = NE (05/01/07)
14-Dec-10
2.6
6.0
ND
Dry
ND
21-Jun-11
5.0
6.0
ND
Dry
ND
6-Dec-11
5.0
6.0
ND
ND
ND
13-Jun-12
5.0
6.0
ND
ND
ND
11-Dec-12
5.0
6.0
ND
Dry
ND
29-Apr-13
5.0
6.0
ND
ND
ND
6-Aug-13
5.0
6.0
ND
ND
ND
25-Feb-14
5.0
6.0
ND
ND
ND
13-Aug-14
5.0
6.0
ND
ND
ND
11-Mar-15
3.8
6.0
ND
ND
ND
19-Aug-15
3.8
6.0
ND
Dry
ND
18-Feb-16
3.8
6.0
ND
ND
ND
11-Aug-16
3.8
6.0
ND
ND
ND
15-Feb-17
3.9
6.0
ND
ND
ND
24-Aug-17
3.9
6.0
ND
---
ND
6-Feb-18
3.9
6.0
ND
ND
ND
16-Aug-18
3.9
6.0
ND
ND
ND
Arsenic
19-Dec-07
NR
10
5.3
Dry
ND
NC 2B = 50 µg/L (05/01 /07)
8-Jul-08
NR
10.0
ND
Dry
ND
16-Dec-08
2.7
11.0
ND
ND
ND
8-Jul-09
2.7
10.0
ND
Dry
ND
15-Dec-09
2.7
10.0
ND
2.7 J
ND
23-Jun-10
2.7
10.0
9.2 J
ND
ND
14-Dec-10
2.7
10.0
3.1 J
Dry
ND
21-Jun-11
5.0
10.0
ND
Dry
ND
6-Dec-11
5.0
10.0
ND
ND
ND
13-Jun-12
5.0
10.0
6.5 J
ND
ND
11-Dec-12
5.0
10.0
ND
Dry
ND
29-Apr-13
5.0
10.0
ND
ND
ND
6-Aug-13
5.0
10.0
5.5 J
ND
ND
25-Feb-14
5.0
10.0
ND
ND
ND
13-Aug-14
5.0
10.0
ND
ND
ND
11-Mar-15
2.5
10.0
4.9 J
2.7 J
ND
19-Aug-15
2.5
10.0
ND
Dry
ND
18-Feb-16
2.5
10.0
ND
ND
ND
11-Aug-16
2.5
10.0
6.8 J
7.3 J
ND
15-Feb-17
5.0
10.0
ND
ND
ND
24-Aug-17
5.0
10.0
ND
---
ND
6-Feb-18
5.0
10.0
ND
ND
ND
16-Aug-18
5.0
10.0
ND
ND
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 1 of 14

TABLE C-05: Historical Detected Constituents in Surface Water
Analyte
Sample
Collection Date
DL
RL
SW-1
SW-2
Blanks
Barium
14-Sep-94
NR
500
160
ND
NS
2-Dec-94
NR
500
ND
ND
NS
8-Feb-95
NR
500
ND
ND
NS
2-Mar-95
NR
500
ND
ND
NS
17-Nov-95
NR
500
ND
ND
NS
23-May-96
NR
500
ND
ND
NS
14-Nov-96
NR
500
69
29
NS
18-Jun-97
NR
500
64
25
NS
2-Dec-97
NR
500
61
41
NS
27-May-98
NR
500
130
50
NS
16-Nov-98
NR
500
93
100
NS
10-Sep-99
NR
500
ND
ND
NS
16-Nov-99
NR
500
ND
ND
NS
10-May-00
NR
500
ND
ND
NS
26-Oct-00
NR
500
ND
ND
NS
18-Apr-01
NR
500
ND
ND
NS
19-Nov-02
NR
500
NS
ND
NS
27-Jun-03
NR
500
ND
ND
NS
30-Dec-03
NR
500
ND
ND
ND
30-Jun-04
NR
500
ND
ND
ND
29-Dec-04
NR
500
ND
ND
ND
29-Jun-05
NR
500
ND
ND
ND
29-Dec-05
NR
500
ND
ND
ND
28-Jun-06
NR
500
ND
ND
ND
NC 2B = NE (05/01/07)
28-Dec-06
NR
100
40.0
47.2
0.20 J
12-Jul-07
NR
100
66.2 J
Dry
ND
19-Dec-07
NR
100
112
Dry
10.5
8-Jul-08
NR
100
89.0 J
Dry
0.29 J
16-Dec-08
0.20
100
42.1 B
54.8 J
10.7 J
8-Jul-09
0.20
100
101
Dry
17.6 J
15-Dec-09
0.20
100
36.3 B
48.4 B
17.1 J
23-Jun-10
0.20
100
115 B
39.1 B
27.3 J
14-Dec-10
0.20
100
97.4 J
Dry
12.1 J
21-Jun-11
5.0
100
66.3 J
Dry
ND
6-Dec-11
5.0
100
59.7 J
55.3 J
ND
13-Jun-12
5.0
100
161
85.4 J
ND
11-Dec-12
5.0
100
71.1 J
Dry
ND
29-Apr-13
5.0
100
43.5 J
43.5 J
ND
6-Aug-13
5.0
100
80.3 J
23.8 J
ND
25-Feb-14
5.0
100
63.9 J
61.8 J
ND
13-Aug-14
5.0
100
47.4 J
43.9 J
ND
11-Mar-15
2.5
100
28.5 J
42.0 J
ND
19-Aug-15
2.5
100
37.0 J
Dry
ND
18-Feb-16
2.5
100
58.2 J
55.0 J
ND
11-Aug-16
2.5
100
175
152
ND
15-Feb-17
2.5
100
285
38.2 J
ND
24-Aug-17
2.5
100
31.6 J
---
ND
6-Feb-18
2.5
100
22.4 J
33.5 J
ND
16-Aug-18
2.5
100
19.1 J
28.3 J
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 2 of 14

TABLE C-05: Historical Detected Constituents in Surface Water
Analyte
Sample
Collection Date
DL
RL
SW-1
SW-2
Blanks
Beryllium
16-Nov-98
NR
2
1.0
1.0
NS
NC 2B = 6.5 µg/L (05/01/07)
10-Sep-99
NR
2
ND
ND
NS
16-Nov-99
NR
2
ND
ND
NS
10-May-00
NR
2
ND
ND
NS
26-Oct-00
NR
2
ND
ND
NS
18-Apr-01
NR
2
ND
ND
NS
19-Nov-02
NR
2
ND
ND
NS
27-Jun-03
NR
2
ND
ND
NS
30-Dec-03
NR
2
ND
ND
ND
30-Jun-04
NR
2
ND
ND
ND
29-Dec-04
NR
2
ND
ND
ND
29-Jun-05
NR
2
ND
ND
ND
29-Dec-05
NR
2
ND
ND
ND
28-Jun-06
NR
2
ND
ND
ND
28-Dec-06
NR
1
ND
ND
ND
NC 2B = 6.5 µg/L (05/01/07)
12-Jul-07
NR
1
ND
Dry
ND
19-Dec-07
NR
1
0.93 J
Dry
ND
8-Jul-08
NR
1.0
0.47 J
Dry
ND
16-Dec-08
0.10
1.0
0.21 J
0.27 J
ND
8-Jul-09
0.10
1.0
0.29 J
Dry
ND
15-Dec-09
0.10
1.0
0.27 J
0.22 J
ND
23-Jun-10
0.10
1.0
1.2
ND
ND
14-Dec-10
0.10
1.0
0.78 J
Dry
ND {0.15} J
21-Jun-11
1.0
1.0
ND
Dry
ND
6-Dec-11
1.0
1.0
ND
ND
ND
13-Jun-12
1.0
1.0
1.5
ND
ND
11-Dec-12
1.0
1.0
ND
Dry
ND
29-Apr-13
1.0
1.0
ND
ND
ND
6-Aug-13
1.0
1.0
ND
ND
ND
25-Feb-14
1.0
1.0
ND
ND
ND
13-Aug-14
1.0
1.0
ND
ND
ND
11-Mar-15
0.50
1.0
ND
ND
ND
19-Aug-15
0.50
1.0
ND
Dry
ND
18-Feb-16
0.50
1.0
ND
ND
ND
11-Aug-16
0.50
1.0
1.9
1.7
ND
15-Feb-17
0.50
1.0
ND
ND
ND
24-Aug-17
0.50
1.0
ND
---
ND
6-Feb-18
0.50
1.0
ND
ND
ND
16-Aug-18
0.50
1.0
ND
ND
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 3 of 14

TABLE C-05: Historical Detected Constituents in Surface Water
Analyte
Sample
Collection Date
DL
RL
SW-1
SW-2
Blanks
Cadmium
19-Nov-02
NR
1
ND
1.0
NS
27-Jun-03
NR
1
ND
ND
NS
30-Dec-03
NR
1
ND
ND
ND
30-Jun-04
NR
1
ND
ND
ND
29-Dec-04
NR
1
ND
ND
ND
29-Jun-05
NR
1
ND
ND
ND
29-Dec-05
NR
1
ND
ND
ND
28-Jun-06
NR
1
ND
ND
ND
28-Dec-06
NR
1
ND
ND
ND
NC 2B = 2 µg/L (05/01/07)
12-Jul-07
NR
1
ND
Dry
ND
NC 2L = 1.75 µg/L (10/23/07)
19-Dec-07
NR
1
ND
Dry
ND
8-Jul-08
NR
1.0
ND
Dry
ND
16-Dec-08
0.50
1.0
ND
ND
ND
8-Jul-09
0.50
1.0
ND
Dry
ND
15-Dec-09
0.50
1.0
ND
ND
ND
23-Jun-10
0.50
1.0
ND
ND
ND
14-Dec-10
0.50
1.0
ND
Dry
ND
21-Jun-11
1.0
1.0
ND
Dry
ND
6-Dec-11
1.0
1.0
ND
ND
ND
13-Jun-12
1.0
1.0
ND
ND
ND
11-Dec-12
1.0
1.0
ND
Dry
ND
29-Apr-13
1.0
1.0
ND
ND
ND
6-Aug-13
1.0
1.0
ND
ND
ND
25-Feb-14
1.0
1.0
ND
ND
ND
13-Aug-14
1.0
1.0
ND
ND
ND
11-Mar-15
0.50
1.0
ND
ND
ND
19-Aug-15
0.50
1.0
ND
ND
ND
18-Feb-16
0.50
1.0
ND
ND
ND
11-Aug-16
0.50
1.0
ND
ND
ND
15-Feb-17
0.50
1.0
ND
ND
ND
24-Aug-17
0.50
1.0
ND
---
ND
6-Feb-18
0.50
1.0
ND
ND
ND
16-Aug-18
0.50
1.0
ND
ND
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 4 of 14

TABLE C-05: Historical Detected Constituents in Surface Water
Analyte
Sample
Collection Date
DL
RL
SW-1
SW-2
Blanks
Chromium
18-Jun-97
NR
10
12.0
ND
NS
2-Dec-97
NR
10
8.0
ND
NS
27-May-98
NR
10
15.0
ND
NS
16-Nov-98
NR
10
30.0
31.0
NS
10-Sep-99
NR
10
24.0
ND
NS
16-Nov-99
NR
10
ND
ND
NS
10-May-00
NR
10
ND
ND
NS
26-Oct-00
NR
10
ND
ND
NS
18-Apr-01
NR
10
ND
ND
NS
19-Nov-02
NR
10
ND
ND
NS
27-Jun-03
NR
10
ND
ND
NS
30-Dec-03
NR
10
ND
ND
ND
30-Jun-04
NR
10
ND
ND
ND
29-Dec-04
NR
10
ND
ND
ND
29-Jun-05
NR
10
ND
ND
ND
29-Dec-05
NR
10
ND
ND
ND
28-Jun-06
NR
10
12.6
ND
ND
28-Dec-06
NR
10
4.8 J
6.1 J
ND
NC 2B = 50 µg/L (05/01/07)
12-Jul-07
NR
10
ND
Dry
ND
19-Dec-07
NR
10
27.9
Dry
ND
8-Jul-08
NR
10.0
19.3
Dry
ND
6-Dec-08
0.40
10.0
6.4 J
8.4 J
ND
8-Jul-09
0.40
10.0
12.9
Dry
ND
15-Dec-09
0.40
10.0
6.0 J
5.0 J
ND
23-Jun-10
0.40
10.0
41.8
4.8 J
0.71 J
Resample >
12-Aug-10
0.40
10.0
44.4
NS
ND
14-Dec-10
0.40
10.0
32.4
Dry
ND
21-Jun-11
5.0
10.0
12.1
Dry
ND
6-Dec-11
5.0
10.0
11.8
7.5 J
ND
13-Jun-12
5.0
10.0
46.1
20.7
ND
11-Dec-12
5.0
10.0
19.1
Dry
ND
29-Apr-13
5.0
10.0
5.8 J
5.8 J
ND
6-Aug-13
5.0
10.0
ND
ND
ND
25-Feb-14
5.0
10.0
13.5
13.2
ND
13-Aug-14
5.0
10.0
10.8
10 J
ND
NC 2B =11 µg/L 03/01/16)
11-Mar-15
2.5
10.0
4.0 1
3.1 1
ND
19-Aug-15
2.5
10.0
ND
Dry
ND
18-Feb-16
2.5
10.0
ND
ND
ND
11-Aug-16
2.5
10.0
63.0
55.1
ND
Resample >
13-Sep-16
2.5
10.0
13.8 (ND)
DRY
ND
15-Feb-17
2.5
10.0
6.1 J
7.2 J
ND
24-Aug-17
2.5
10.0
7.0 J
---
ND
6-Feb-18
2.5
10.0
2.8 J
5.4 J
ND
16-Aug-18
2.5
10.0
ND
3.2 J
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 5 of 14

TABLE C-05: Historical Detected Constituents in Surface Water
Analyte
Sample
Collection Date
DL
RL
SW-1
SW-2
Blanks
Cobalt
14-Nov-96
NR
10
3.0
ND
NS
18-Jun-97
NR
10
3.0
ND
NS
2-Dec-97
NR
10
ND
ND
NS
27-May-98
NR
10
8.0
5.0
NS
16-Nov-98
NR
10
4.9
5.9
NS
10-Sep-99
NR
10
ND
ND
NS
16-Nov-99
NR
10
ND
ND
NS
10-May-00
NR
10
ND
ND
NS
26-Oct-00
NR
10
ND
ND
NS
18-Apr-01
NR
10
ND
ND
NS
19-Nov-02
NR
10
ND
ND
NS
27-Jun-03
NR
10
ND
ND
NS
30-Dec-03
NR
10
ND
ND
ND
30-Jun-04
NR
10
ND
ND
ND
29-Dec-04
NR
10
ND
ND
ND
29-Jun-05
NR
10
ND
ND
ND
29-Dec-05
NR
10
ND
ND
ND
28-Jun-06
NR
10
ND
ND
ND
28-Dec-06
NR
10
ND
2.8 J
ND
NC 213 = NE (05/01/07)
12-Jul-07
NR
10
ND
Dry
ND
19-Dec-07
NR
10
34.3
Dry
1.6 J
8-Jul-08
NR
10.0
10.0 B
Dry
6.2 J
16-Dec-08
0.60
10.0
4.8 B
5.1 B
2.4 J
8-Jul-09
0.60
10.0
7.2 J
Dry
ND
15-Dec-09
0.60
10.0
1.6 J
1.3 J
ND
23-Jun-10
0.60
10.0
23.0
2.7 J
ND
Resample >
12-Aug-10
0.60
10.0
30.5
NS
ND
14-Dec-10
0.60
10.0
27.0
Dry
1.6 J
21-Jun-11
5.0
10.0
5.4 J
Dry
ND
6-Dec-11
5.0
10.0
ND
ND
ND
13-Jun-12
5.0
10.0
12.5
6.5 J
ND
11-Dec-12
5.0
10.0
ND
Dry
ND
29-Apr-13
5.0
10.0
10.2
10.8
ND
6-Aug-13
5.0
10.0
9.0 J
ND
ND
25-Feb-14
5.0
10.0
10.1
10.6
ND
13-Aug-14
5.0
10.0
ND
ND
ND
11-Mar-15
2.5
10.0
ND
ND
ND
19-Aug-15
2.5
10.0
ND
Dry
ND
18-Feb-16
2.5
10.0
ND
ND
ND
11-Aug-16
2.5
10.0
16.7
12.7
ND
15-Feb-17
2.5
10.0
4.0 J
ND
ND
24-Aug-17
2.5
10.0
ND
---
ND
6-Feb-18
2.5
10.0
ND
ND
ND
16-Aug-18
2.5
10.0
ND
ND
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 6 of 14

TABLE C-05: Historical Detected Constituents in Surface Water
Analyte
Sample
Collection Date
DL
RL
SW-1
SW-2
Blanks
Copper
18-Jun-97
NR
200
11.0
ND
NS
2-Dec-97
NR
200
11.0
ND
NS
27-May-98
NR
200
21.0
ND
NS
16-Nov-98
NR
200
14.0
16.0
NS
10-Sep-99
NR
200
ND
ND
NS
16-Nov-99
NR
200
ND
ND
NS
10-May-00
NR
200
ND
ND
NS
26-Oct-00
NR
200
ND
ND
NS
18-Apr-01
NR
200
ND
ND
NS
19-Nov-02
NR
200
NS
ND
NS
27-Jun-03
NR
200
ND
ND
NS
30-Dec-03
NR
200
ND
ND
ND
30-Jun-04
NR
200
ND
ND
ND
29-Dec-04
NR
200
ND
ND
ND
29-Jun-05
NR
200
ND
ND
ND
29-Dec-05
NR
200
ND
ND
ND
28-Jun-06
NR
200
ND
ND
ND
28-Dec-06
NR
10
3.0 B
3.9
0.60 J
NC 213 = 7 µg/L (05/01/07)
12-Jul-07
NR
10
ND
Dry
ND
19-Dec-07
NR
10
23.7 B
Dry
10.5 B
8-Jul-08
NR
10.0
14.7
Dry
ND
16-Dec-08
0.30
10.0
6.4 J
8.0 J
ND
8-Jul-09
0.30
10.0
7.0 J
Dry
ND
15-Dec-09
0.30
10.0
5.2 J
4.4 J
ND
23-Jun-10
0.30
10.0
23.9
2.7 J
ND
Resample >
12-Aug-10
0.30
10.0
25.9
ND
ND
14-Dec-10
0.30
10.0
21.1
Dry
0.49 J
21-Jun-11
5.0
10.0
7.7 J
Dry
ND
6-Dec-11
5.0
10.0
12.5
7.7 J
ND
13-Jun-12
5.0
10.0
34.5
14.8
ND
11-Dec-12
5.0
10.0
16.4
Dry
ND
29-Apr-13
5.0
10.0
7.7 J
7.4 J
ND
6-Aug-13
5.0
10.0
5.5 J
ND
ND
25-Feb-14
5.0
10.0
11.2
10.3
ND
13-Aug-14
5.0
10.0
9.6 J
7.7 J
ND
II-Mar-15
2.5
10.0
3.1 J
2.6 J
ND
NC 213 = 2.7 µg/L 03/01/16)
19-Aug-15
2.5
10.0
ND
Dry
ND
18-Feb-16
2.5
10.0
6.3 J
5.7 J
ND
11-Aug-16
2.5
10.0
39.9
34.5
ND
Resample >
13-Sep-16
2.5
10.0
9.3 (2.5 B) B
DRY
3.5 B
15-Feb-17
2.5
10.0
5.8 J
5.2 J
ND
24-Aug-17
2.5
10.0
4.5 J
---
ND
6-Feb-18
2.5
10.0
6.8 J
8.0 J
ND
16-Aug-18
2.5
10.0
3.9 J
3.0 J
ND
Iron 24-Aug-17
25.0
300
9760
---
---
16-Aug-18
11
25.0
300
3320
2750
27.8 J
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 7 of 14

TABLE C-05: Historical Detected Constituents in Surface Water
Analyte
Sample
Collection Date
DL
RL
SW-1
SW-2
Blanks
Lead
2-Dec-97
NR
10
ND
6.0
NS
27-May-98
NR
10
8.0
ND
NS
16-Nov-98
NR
10
7.3
8.9
NS
10-Sep-99
NR
10
ND
ND
NS
16-Nov-99
NR
10
ND
ND
NS
10-May-00
NR
10
ND
ND
NS
26-Oct-00
NR
10
ND
ND
NS
18-Apr-01
NR
10
ND
ND
NS
19-Nov-02
NR
10
ND
ND
NS
27-Jun-03
NR
10
ND
ND
NS
30-Dec-03
NR
10
ND
ND
ND
30-Jun-04
NR
10
ND
ND
ND
29-Dec-04
NR
10
ND
ND
ND
29-Jun-05
NR
10
ND
ND
ND
29-Dec-05
NR
10
ND
ND
ND
28-Jun-06
NR
10
ND
ND
ND
28-Dec-06
NR
10
ND
4.8 J
ND
NC 2B = 25 µg/L (05/01/07)
12-Jul-07
NR
10
3.2 J
Dry
ND
19-Dec-07
NR
10
ND
Dry
ND
8-Jul-08
NR
10.0
ND
Dry
ND
16-Dec-08
4.0
10.0
ND
ND
ND
8-Jul-09
4.0
10.0
ND
Dry
ND
15-Dec-09
4.0
10.0
ND
ND
ND
23-Jun-10
4.0
10.0
9.2 J
ND
ND
14-Dec-10
4.0
10.0
5.1 J
Dry
ND
21-Jun-11
5.0
10.0
ND
Dry
ND
6-Dec-11
5.0
10.0
ND
ND
ND
13-Jun-12
5.0
10.0
14.3
5.5 J
ND
11-Dec-12
5.0
10.0
ND
Dry
ND
29-Apr-13
5.0
10.0
ND
ND
ND
6-Aug-13
5.0
10.0
ND
ND
ND
25-Feb-14
5.0
10.0
ND
ND
ND
13-Aug-14
5.0
10.0
ND
ND
ND
11-Mar-15
2.5
10.0
ND
ND
ND
19-Aug-15
2.5
10.0
ND
Dry
ND
NC 2B = 14 µg/L 03/01/16)
18-Feb-16
2.5
10.0
4.0 J
2.6 J
ND
11-Aug-16
2.5
10.0
16.6
13.6
ND
Resample >
13-Sep-16
2.5
10.0
4.1 (2.6 J) J
DRY
ND
15-Feb-17
2.5
10.0
2.5 J
2.5 J
ND
24-Aug-17
2.5
10.0
2.5 J
---
ND
6-Feb-18
2.5
10.0
ND
ND
ND
16-Aug-18
2.5
10.0
ND
ND
ND
Manganese 24-Aug-17
2.5
50
244
---
---
16-Aug-18
2.5
50
176
45.2 J
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 8 of 14

TABLE C-05: Historical Detected Constituents in Surface Water
Analyte
Sample
Collection Date
DL
RL
SW-1
SW-2
Blanks
Nickel
28-Dec-06
NR
50
4.6 J
6.2 J
ND
NC 2B = 88 µg/L (05/01/07)
12-Jul-07
NR
50
4.0 J
Dry
ND
19-Dec-07
NR
50
21.9
Dry
ND
8-Jul-08
NR
50.0
12.1 J
Dry
ND
16-Dec-08
1.7
50.0
5.2 B
6.8 B
2.4 J
8-Jul-09
1.7
50.0
10.0 J
Dry
ND
15-Dec-09
1.7
50.0
4.8 B
4.7 B
3.0 J
23-Jun-10
1.7
50.0
21.5 J
ND
ND
14-Dec-10
1.7
50.0
14.4 J
Dry
2.7 J
21-Jun-11
5.0
50.0
5.8 J
Dry
ND
6-Dec-11
5.0
50.0
7.2 J
ND
ND
13-Jun-12
5.0
50.0
17.1 J
7.5 J
ND
11-Dec-12
5.0
50.0
7.6 J
Dry
ND
29-Apr-13
5.0
50.0
ND
ND
ND
6-Aug-13
5.0
50.0
ND
ND
ND
25-Feb-14
5.0
50.0
7.3 J
6.6 J
ND
13-Aug-14
5.0
50.0
7.5 J
5.4 J
ND
11-Mar-15
2.5
50.0
3.0 J
2.8 J
ND
19-Aug-15
2.5
50.0
ND
Dry
ND
18-Feb-16
2.5
50.0
3.3 J
3.0 J
ND
11-Aug-16
2.5
50.0
22.8 J
19.4 J
ND
15-Feb-17
2.5
50.0
4.2 J
4.1 J
ND
24-Aug-17
2.5
50.0
3.7 J
---
ND
6-Feb-18
2.5
50.0
ND
3.2 J
ND
16-Aug-18
2.5
50.0
ND
ND
ND
Selenium
19-Dec-07
NR
10
15.6
Dry
ND
NC 2B = 5 µg/L (05/01/07)
8-Jul-08
NR
10.0
ND
Dry
ND
16-Dec-08
3.8
10.0
3.9 B
ND
4.9 J
8-Jul-09
3.8
10.0
ND
Dry
ND
15-Dec-09
3.8
10.0
ND
ND
ND
NC 2L = 20 µg/L (2/5/10)
23-Jun-10
3.8
10.0
ND
ND
ND
14-Dec-10
3.8
10.0
5.9 J
Dry
ND
21-Jun-11
10.0
10.0
ND
Dry
ND
6-Dec-11
10.0
10.0
ND
ND
ND
13-Jun-12
10.0
10.0
ND
ND
ND
11-Dec-12
10.0
10.0
ND
Dry
ND
29-Apr-13
10.0
10.0
ND
ND
ND
6-Aug-13
10.0
10.0
ND
ND
ND
25-Feb-14
10.0
10.0
ND
ND
ND
13-Aug-14
10.0
10.0
ND
ND
ND
11-Mar-15
5.0
10.0
ND
ND
ND
19-Aug-15
5.0
10.0
ND
Dry
ND
18-Feb-16
5.0
10.0
ND
ND
ND
11-Aug-16
5.0
10.0
ND
6.0 J
ND
15-Feb-17
5.0
10.0
ND
ND
ND
24-Aug-17
5.0
10.0
ND
---
ND
6-Feb-18
5.0
10.0
ND
ND
ND
16-Aug-18
5.0
10.0
ND
ND
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 9 of 14

TABLE C-05: Historical Detected Constituents in Surface Water
Analyte
Sample
Collection Date
DL
RL
SW-1
SW-2
Blanks
Silver
8-Jul-08
NR
10.0
0.22 J
Dry
ND
NC 213 = 0.06 µg/L (05/01/07)
16-Dec-08
0.10
10.0
ND
0.11 J
ND
8-Jul-09
0.10
10.0
ND
Dry
ND
15-Dec-09
0.10
10.0
ND
0.19 J
ND
NC 2L = 20 µg/L (2/5/10)
23-Jun-10
0.10
10.0
ND
ND
ND
{0.25 J)
14-Dec-10
0.10
10.0
0.21 B
Dry
J
0.19
21-Jun-11
5.0
10.0
ND
Dry
ND
6-Dec-11
5.0
10.0
ND
ND
ND
13-Jun-12
5.0
10.0
ND
ND
ND
11-Dec-12
5.0
10.0
ND
Dry
ND
29-Apr-13
5.0
10.0
ND
ND
ND
6-Aug-13
5.0
10.0
ND
ND
ND
25-Feb-14
5.0
10.0
ND
ND
ND
13-Aug-14
5.0
10.0
ND
ND
ND
11-Mar-15
2.5
10.0
ND
ND
ND
19-Aug-15
2.5
10.0
ND
Dry
ND
18-Feb-16
2.5
10.0
ND
ND
ND
11-Aug-16
2.5
10.0
ND
ND
ND
15-Feb-17
2.5
10.0
ND
ND
ND
24-Aug-17
2.5
10.0
ND
---
ND
6-Feb-18
2.5
10.0
ND
ND
ND
16-Aug-18
2.5
10.0
ND
ND
ND
Thallium
19-Dec-07
NR
5.5
5.1 J
Dry
ND
NC 213 = NE (05/01/07)
8-Jul-08
NR
5.5
5.2 J
Dry
ND
16-Dec-08
3.0
5.5
ND
ND
ND
8-Jul-09
3.0
5.5
ND
Dry
ND
15-Dec-09
3.0
5.5
ND
ND
ND
23-Jun-10
3.0
5.5
ND
ND
ND
Resample >
12-Aug-10
30.0
55.0
NS
NS
ND
GWPS = 0.2 µg/L (10/01/10)
14-Dec-10
3.0
5.5
6.5
Dry
ND
21-Jun-11
5.4
5.5
8.2
Dry
ND
6-Dec-11
5.4
5.5
ND
ND
ND
13-Jun-12
5.4
5.5
ND
ND
ND
11-Dec-12
5.4
5.5
ND
Dry
ND
29-Apr-13
5.4
5.5
ND
ND
ND
6-Aug-13
5.4
5.5
ND
ND
ND
25-Feb-14
5.4
5.5
ND
ND
ND
13-Aug-14
5.4
5.5
ND
ND
ND
11-Mar-15
5.0
5.5
ND
ND
ND
19-Aug-15
5.0
5.5
ND
Dry
ND
18-Feb-16
5.0
5.5
ND
ND
ND
11-Aug-16
5.0
5.5
ND
ND
ND
15-Feb-17
0.02
5.5
ND
ND
ND
24-Aug-17
0.02
5.5
ND
---
ND
6-Feb-18
0.028
0.10
ND
ND
ND
16-Aug-18
0.020
5.50
ND
ND
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 10 of 14

TABLE C-05: Historical Detected Constituents in Surface Water
Analyte
Sample
Collection Date
DL
RL
SW-1
SW-2
Blanks
Vanadium
14-Nov-96
NR
40
11.0
5.0
NS
18-Jun-97
NR
40
20.0
ND
NS
2-Dec-97
NR
40
16.0
ND
NS
27-May-98
NR
40
44.0
ND
NS
16-Nov-98
NR
40
44.0
47.0
NS
10-Sep-99
NR
40
ND
ND
NS
16-Nov-99
NR
40
ND
ND
NS
10-May-00
NR
40
ND
ND
NS
26-Oct-00
NR
40
ND
ND
NS
18-Apr-01
NR
40
ND
ND
NS
19-Nov-02
NR
40
ND
ND
NS
27-Jun-03
NR
40
ND
ND
NS
30-Dec-03
NR
40
ND
ND
ND
30-Jun-04
NR
40
ND
ND
ND
29-Dec-04
NR
40
ND
ND
ND
29-Jun-05
NR
40
ND
ND
ND
29-Dec-05
NR
40
ND
ND
ND
28-Jun-06
NR
40
ND
ND
ND
28-Dec-06
NR
25
8.6 J
10.7
ND
NC 2B = NE (05/01/07)
12-Jul-07
NR
25
5.3 J
ND
ND
19-Dec-07
NR
25
41.2
ND
0.51 J
Resample >
14-Feb-08
NR
25
12.4
Dry
0.24 J
Filtered >
14-Feb-08
NR
25
1.6 J
Dry
ND
8-Jul-08
NR
25.0
38.2
Dry
0.20 J
16-Dec-08
0.20
25.0
11.5 J
14.1 J
0.76 J
8-Jul-09
0.20
25.0
24.3 J
Dry
1.3 J
15-Dec-09
0.20
25.0
10 J
7.0 J
0.53 J
23-Jun-10
0.20
25.0
63.4
8.3 J
ND
Resample >
12-Aug-10
0.20
25.0
67.9
NS
0.33 J
14-Dec-10
0.20
25.0
52.3
Dry
{0.57 J) 0.36 J
21-Jun-11
5.0
25.0
25.3
Dry
ND
6-Dec-11
5.0
25.0
19.7 J
13.0 J
ND
13-Jun-12
5.0
25.0
130
61.5
ND
11-Dec-12
5.0
25.0
50.7
Dry
ND
29-Apr-13
5.0
25.0
16.9 J
18.4 J
ND
6-Aug-13
5.0
25.0
15.4 J
ND
ND
25-Feb-14
5.0
25.0
29.2
29.4
ND
13-Aug-14
5.0
25.0
18.0 J
18.2 J
ND
11-Mar-15
2.5
25.0
7.8 J
8.3 J
ND
19-Aug-15
2.5
25.0
2.8 J
Dry
ND
18-Feb-16
2.5
25.0
6.4 J
6.1 J
ND
11-Aug-16
2.5
25.0
160
144
ND
15-Feb-17
2.5
25.0
18.2 J
20.8 J
ND
24-Aug-17
2.5
25.0
20.5 J
---
ND
6-Feb-18
2.5
25.0
6.9 J
14.4 J
ND
16-Aug-18
2.5
25.0
7.6 J
5.8 J
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 11 of 14

TABLE C-05: Historical Detected Constituents in Surface Water
Analyte
Sample
Collection Date
DL
RL
SW-1
SW-2
Blanks
Zinc
14-Sep-94
NR
50
ND
ND
NS
2-Dec-94
NR
50
61.0
ND
NS
8-Feb-95
NR
50
ND
ND
NS
2-Mar-95
NR
50
64.0
ND
NS
17-Nov-95
NR
50
ND
ND
NS
23-May-96
NR
50
ND
ND
NS
14-Nov-96
NR
50
ND
ND
NS
18-Jun-97
NR
50
26.0
ND
NS
2-Dec-97
NR
50
32.0
40.0
NS
27-May-98
NR
50
57.0
28.0
NS
16-Nov-98
NR
50
28.0
31.0
NS
10-Sep-99
NR
50
ND
ND
NS
16-Nov-99
NR
50
ND
ND
NS
10-May-00
NR
50
ND
ND
NS
26-Oct-00
NR
50
ND
ND
NS
18-Apr-01
NR
50
ND
ND
NS
19-Nov-02
NR
50
NS
ND
NS
27-Jun-03
NR
50
ND
ND
NS
30-Dec-03
NR
50
ND
ND
ND
30-Jun-04
NR
50
ND
ND
ND
29-Dec-04
NR
50
ND
ND
ND
29-Jun-05
NR
50
ND
ND
ND
29-Dec-05
NR
50
ND
ND
ND
28-Jun-06
NR
50
ND
ND
ND
28-Dec-06
NR
10
7.4 J
8.5 J
ND
NC 2B = 50 µg/L (05/01 /07)
12-Jul-07
NR
10
10.2
Dry
ND
19-Dec-07
NR
10
24.1 B
Dry
87.9
8-Jul-08
NR
10.0
17.2
Dry
1.2 J
16-Dec-08
0.40
10.0
8.9 J
11.9
ND
8-Jul-09
0.40
10.0
9.4 J
Dry
1.6 J
15-Dec-09
0.40
10.0
8.3 B
8.5 B
7.7 J
23-Jun-10
0.40
10.0
29.3
4.0 J
ND
14-Dec-10
0.40
10.0
25.1 B
Dry
6.7 J
21-Jun-11
10.0
10.0
10.9
Dry
ND
6-Dec-11
10.0
10.0
15.0 B
10.3 B
12.4
13-Jun-12
10.0
10.0
46.3
19.8
ND
11-Dec-12
10.0
10.0
25.4
Dry
ND
29-Apr-13
10.0
10.0
13.8
12.5
ND
6-Aug-13
10.0
10.0
11.3
ND
ND
25-Feb-14
10.0
10.0
15.0
14.8
ND
13-Aug-14
10.0
10.0
14.3
ND
ND
11-Mar-15
5.0
10.0
62.3
11.6 B
6.1 J
NC 2B = 36 µg/L (03/01/16)
19-Aug-15
5.0
10.0
ND
Dry
11.5
18-Feb-16
5.0
10.0
13.0
11.0
ND
11-Aug-16
5.0
10.0
66.4
54.1
ND
Resample >
13-Sep-16
5.0
10.0
14.5 (5.9 J) B
DRY
ND
15-Feb-17
5.0
10.0
11.0
9.6 J
ND
24-Aug-17
5.0
10.0
7.6 J
---
ND
6-Feb-18
5.0
10.0
9.4 J
6.8 J
ND
16-Aug-18
5.0
10.0
6.2 J
ND
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 12 of 14

TABLE C-05: Historical Detected Constituents in Surface Water
Sample
Analyte
Collection Date
DL
RL
SW-1
SW-2
Blanks
Organic Compounds
Acetone
15-Dec-09
2.2
100
3.9 B
3.2 B
2.8 J
NC 2B = NE (05/01/07)
23-Jun-10
2.2
100
5.4 B
2.2 B
7.7 J
14-Dec-10
2.2
100
ND
Dry
ND
21-Jun-11
2.2
100
3.4 B
Dry
3.9 J
6-Dec-11
2.2
100
ND
ND
8.8 J
13-Jun-12
2.2
100
2.2 B
ND
4.7 J
12-Dec-12
10.0
100
ND
Dry
ND
29-Apr-13
10.0
100
ND
ND
14.6 J
6-Aug-13
10.0
100
ND
ND
ND
25-Feb-14
10.0
100
ND
ND
ND
13-Aug-14
10.0
100
ND
ND
19.3 J
11-Mar-15
10.0
100
ND
ND
ND
19-Aug-15
10.0
100
ND
Dry
ND
18-Feb-16
10.0
100
ND
ND
ND
11-Aug-16
10.0
100
ND
ND
ND
15-Feb-17
10.0
100
ND
ND
ND
24-Aug-17
10.0
100
ND
---
ND
6-Feb-18
10.0
100
ND
ND
ND
16-Aug-18
10.0
100
ND
ND
ND
2-Hexanone
23-Jun-10
0.46
50.0
1.5 J
ND
ND
NC 2B = NE (05/01/07)
14-Dec-10
0.46
50.0
ND
Dry
ND
21-Jun-11
0.46
50.0
ND
Dry
ND
6-Dec-11
0.46
50.0
ND
ND
ND
13-Jun-12
0.46
50.0
ND
ND
ND
12-Dec-12
0.46
50.0
0.47 J
Dry
ND
29-Apr-13
0.46
50.0
ND
ND
ND
6-Aug-13
0.46
50.0
ND
ND
ND
25-Feb-14
0.46
50.0
ND
ND
ND
13-Aug-14
0.46
50.0
ND
ND
ND
11-Mar-15
0.46
50.0
ND
ND
ND
19-Aug-15
0.46
50.0
ND
Dry
ND
18-Feb-16
0.46
50.0
ND
ND
ND
11-Aug-16
0.46
50.0
1.2 J
ND
ND
15-Feb-17
0.46
50.0
ND
ND
ND
24-Aug-17
0.46
50.0
ND
---
ND
6-Feb-18
0.46
50.0
ND
ND
ND
16-Aug-18
0.46
50.0
ND
ND
ND
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 13 of 14

TABLE C-05: Historical Detected Constituents in Surface Water
Analyte
Sample
Collection Date
DL
RL
SW-1
SW-2
Blanks
Methylene Chloride
29-Apr-13
0.97
1.0
0.98 J
ND
ND
NC 2B = NE (05/01/07)
6-Aug-13
0.97
1.0
ND
ND
ND
25-Feb-14
0.97
1.0
ND
ND
ND
13-Aug-14
0.97
1.0
ND
ND
ND
11-Mar-15
0.97
1.0
ND
ND
ND
19-Aug-15
0.97
1.0
ND
Dry
ND
18-Feb-16
0.97
1.0
ND
ND
ND
11-Aug-16
0.97
1.0
ND
ND
ND
15-Feb-17
0.97
1.0
ND
ND
1.6
24-Aug-17
0.97
1.0
ND
---
1.4
6-Feb-18
0.97
1.0
ND
ND
ND
16-Aug-18
0.97
1.0
ND
ND
ND
1,4-Dioxane (p-Dioxane)
16-Aug-18
1.90
10.0
ND
4.5
ND
NC 2B = 80 /L 2018
Notes:
All concentrations are in micrograms per liter (µg/L).
RL = Reporting Limit (SWSL for December 2006 - present).
DL = Laboratory detection limit.
J = Estimated value between the DL and the RL.
B = Blank -qualified data; result is expected to be biased high based on concentrations in the blanks.
ND = Not detected above laboratory reporting limit.
NS = Not sampled.
NR = Not Reported.
Dry =Surface water point considered to be dry (12/14/10 SW-2 sample attempted, but stream was frozen solid).
NC 2B = North Carolina Surface Water Standards from 15A NCAC 2B.
NE = Not established.
Shaded values for surface water are above the NC 2B.
Surface waters are classified as fresh -water aquatic life.
Please see the report for information regarding NC 2B exceedences of surface water samples.
9/13/16 RESAMPLE= Parenthesis indicate Dissolved concentrations.
Granville County - Oxford Landfill, Unit 1 Joyce Engineering
Permit 3901-CDLF-1997 14 of 14

Table C-06: Historical MNA Parameter Data
Sample
Anal [e
Date
RL
Units
MW-IA
NM-7
MW-2
MW-3R
MW-4R
NM-5R
NM-6R
NES-1S
NES-ID
NES-2S
NES-2D
Temperature
30-Dec-03
°C
15.40
NI
NA
NS
12.51
13.58
NA
NS
NS
NS
NS
18-May-04
°C
14.05
NI
NA
NS
18.11
14.53
NA
15.04
17.15
12.86
16.41
30-Jun-04
°C
13.88
NI
NA
NS
14.33
14.18
NA
14.37
1 7. 98
15.67
15.66
29-Dec-04
°C
14.30
NI
NA
NS
14.80
14.40
NA
NS
NS
NS
NS
28-Dec-06
°C
11.60
NI
15.10
NS
14.60
13.40
14.50
14.30
NS
11.20
NS
11-Jul-07
°C
15.90
NI
15.70
NS
17.30
15.90
19.00
NS
NS
NS
NS
19-Dec-08
°C
14.50
NM
13.50
12.30
12.80
15.70
12.40
13.90
14.30
12.50
13.20
8-Jul-09
°C
14.80
NM
15.20
16.00
16.10
17.00
16.90
15.40
14.80
16.00
17.50
14-Dec-09
°C
9.20
NM
12.50
12.80
12.70
12.50
11.30
13.70
14.60
13.20
13.40
23-Jun-10
°C
18.50
NM
16.69
18.93
18.43
15.76
19.05
18.10
20.28
19.65
20.22
14-Dec-I0
°C
Dry
NM
11.80
11.31
10.63
12.20
13.20
12.12
NS
10.80
NS
21-Jun-11
°C
WL
15.26
15.90
15.85
17.20
15.66
18.20
15.56
18.40
18.33
16.53
6-Dec-lI
°C
WL
16.75
16.70
15.99
16.18
14.97
15.70
15.10
15.01
15.37
14.77
13-Jun-12
°C
WL
18.18
15.60
16.60
15.88
14.90
17.50
15.50
15.60
19.20
17.07
11-Dec-12
°C
WL
16.70
15.00
16.60
16.10
14.90
15.10
15.80
15.20
16.30
15.10
29-Apr-13
°C
WL
16.40
15.90
17.20
16.70
14.90
17.00
15.20
15.20
14.60
16.20
6-Aug-13
°C
WL
18.2
15.9
18.1
18.3
16.1
16.7
15.4
NS
19.4
NS
25-176-14
°C
WL
14.9
14.1
15.7
13.4
14.6
13.0
12.6
12.5
12.5
12.5
13-Aug-14
°C
WL
22.4
19.7
19.8
17.3
16.1
15.9
NS
NS
21.0
NS
12-Mar-15
°C
WL
13.9
11.6
17.0
11.6
12.5
15.2
NS
NS
15.9
20.7
19-Aug-15
°C
WL
17.26
17.80
18.69
16.36
15.75
19.2
NS
NS
19.04
NS
I8-Feb-16
°C
WL
12.80
13.90
14.20
13.40
12.50
8.5
NS
NS
11.3
14.1
11-Aug-16
°C
WL
16.7
15.8
17.3
18.9
18.8
18.4
NS
NS
18.3
NS
15-Feb-17
°C
WL
12.0
15.2
15.4
13.5
14.0
13.1
NS
NS
11.6
NS
24-Aug-17
°C
WL
16.8
16.0
16.5
16.5
16.4
17.8
NS
NS
18.4
NS
7-Feb-18
°C
WL
14.9
13.5
15.1
10.7
13.2
10.5
NS
NS
11.3
NS
16-Aug-18
°C
WL
17.9
19.6
19.9
16.4
16.1
19.8
NS
NS
28.1
NS
pH
30-Dec-03
SU
7.31
NI
NA
NS
6.90
7.24
NA
NS
NS
NS
NS
[Field Test]
18-May-04
SU
6.31
NI
NA
NS
7.27
6.39
NA
7.29
7.46
7.43
7.73
30-Jun-04
SU
8.03
NI
NA
NS
7.74
7.11
NA
6.70
6.79
6.93
Z64
29-Dec-04
SU
6.31
NI
NA
NS
7.47
6.67
NA
NS
NS
NS
NS
28-Dec-06
SU
7.50
NI
6.51
NS
7.38
6.46
8.02
6.06
NS
6.52
NS
11-Jul-07
SU
6.730
NI
6.58
NS
7.65
6.72
7.42
NS
NS
NS
NS
19-Dec-08
SU
6.26
NM
5.92
7.81
7.10
6.63
7.03
7.61
5.81
8.12
7.35
8-Jul-09
SU
6.75
NM
7.90
6.13
8.43
7.86
7.46
8.12
8.43
5.93
8.64
14-Dec-09
SU
6.82
NM
6.76
6.20
7.65
6.70
7.23
6.38
7.50
7.43
6.86
23-Jun-10
SU
5.28
NM
5.45
5.90
6.98
6.11
6.69
5.52
7.35
5.71
6.92
14-Dec-10
SU
Dry
NM
7.09
5.92
7.61
6.12
7.20
5.67
NS
6.36
NS
21-Jun-11
SU
WL
6.20
5.98
6.13
7.07
6.58
7.15
6.07
7.14
6.04
7.12
6-Dec-lI
SU
WL
6.79
6.10
6.61
7.54
6.73
6.92
6.28
7.05
6.46
7.17
13-Jun-12
SU
WL
7.49
6.15
6.43
6.95
6.43
6.88
6.46
7.02
7.15
7.31
11-Dec-12
SU
WL
6.48
6.15
7.47
7.38
6.25
6.92
5.79
6.99
5.99
7.60
29-Apr-13
SU
WL
6.11
5.68
5.96
7.15
6.23
6.91
5.85
6.54
6.69
7.01
6-Aug-13
SU
WL
6.29
7.56
5.96
7.00
6.48
6.96
7.23
NS
5.82
NS
25-176-14
SU
WL
6.73
5.77
5.98
6.61
6.81
6.41
5.89
6.60
6.70
7.61
13-Aug-14
SU
WL
6.16
6.86
6.16
7.11
6.69
6.79
NS
NS
5.89
NS
12-Mar-15
SU
WL
6.53
6.77
6.61
6.26
6.33
6.77
NS
NS
6.50
7.49
19-Aug-15
SU
WL
6.27
6.67
5.88
7.21
6.46
6.79
NS
NS
5.88
NS
I8-Feb-16
SU
WL
6.89
6.56
6.55
6.36
6.23
5.69
NS
NS
6.13
6.52
11-Aug-16
SU
WL
4.55
6.17
4.83
4.67
4.66
4.84
NS
NS
4.58
NS
15-176-17
SU
WL
6.52
5.73
6.23
7.08
6.44
7.30
NS
NS
6.42
NS
24-Aug-17
SU
WL
6.63
5.97
7.63
6.97
6.74
7.32
NS
NS
6.65
NS
7-Feb-18
SU
WL
6.51
6.88
6.84
7.15
6.50
7.75
NS
NS
6.05
NS
16-Aug-18
SU
WL
6.61
5.99
6.01
7.32
6.46
6.96
NS
NS
6.02
NS
Oxidation -Reduction Potential
30-Dec-03
mV
257.2
NI
NS
NS
212.7
187.3
NS
NS
NS
NS
NS
(ORP) (Redox Potential)
18-May-04
mV
352.8
NI
NS
NS
158.6
173.2
NS
150.5
105.7
129.1
55.1
[Field Test]
30-Jun-04
mV
275.0
NI
NS
NS
154.1
174.7
NS
182.8
223.0
179.4
199.7
28-Dec-06
mV
70.2
NI
NS
NS
72.6
75.8
NS
84.7
NS
69.3
NS
11-Jul-07
mV
281.0
NI
NS
NS
269.0
296.0
NS
NS
NS
NS
NS
19-Dec-08
mV
186.0
NM
NS
210.0
181.0
149.0
NS
218.0
240.0
".0
207.0
8-Jul-09
mV
104.0
NM
NS
219.0
115.0
1 24 .0
NS
144.0
146.0
160.0
159.0
14-Dec-09
mV
195.0
NM
NS
138.0
175.0
92.0
NS
96.0
126.0
147.0
119.0
23-Jun-I0
mV
139.6
NM
NS
32.0
-15.0
52.8
NS
33.8
22.8
61.7
1.3
14-Dec-10
mV
Dry
NM
NS
50.0
48.0
40.2
NS
42.5
NS
46.2
NS
21-Jun-I1
mV
WL
89.90
NS
52.8
38.1
50.8
NS
19.9
9.6
44.8
46.4
6-Dec-I1
mV
WL
119.6
NS
68.8
38.9
38.4
NS
28.1
25.0
75.1
87.0
13-Jun-12
mV
WL
-32.2
NS
-14.3
136.0
67.5
NS
-4.1
105.6
-18.1
21.8
11-Dec-12
mV
WL
114.9
NS
158.8
105.5
98.9
NS
123.7
164.8
157.8
121.9
29-Apr-13
mV
WL
78.4
NS
146.9
65.5
117.7
NS
61.3
90.0
142.3
74.3
6-Aug-13
mV
WL
89.0
NS
110.6
62.3
83.7
NS
112.7
NS
101.0
NS
25-Feb-14
mV
WL
102.3
NS
140.0
-44.2
137.8
NS
60.6
88.0
74.3
102.1
13-Aug-14
mV
WL
76.0
NS
NS
NS
49.2
NS
NS
NS
90.4
NS
12-Mar-15
mV
WL
71.8
NS
NS
NS
68.1
NS
NS
NS
72.2
49.6
19-Aug-15
mV
WL
61.9
NS
NS
NS
22.5
NS
NS
NS
57.9
NS
18-Feb-16
mV
WL
104.2
NS
NS
NS
123.5
NS
NS
NS
105.7
52.9
11-Aug-16
mV
WL
58.5
NS
NS
NS
48.7
NS
NS
NS
61.9
NS
15-Feb-17
mV
WL
72.6
NS
NS
NS
53.7
NS
NS
NS
39.6
NS
24-Aug-17
mV
WL
143.7
NS
NS
NS
144.2
NS
NS
NS
126.4
NS
7-Feb-18
mV
WL
42.3
NS
NS
NS
26.0
NS
NS
NS
62.5
NS
16-Aug-18
mV
WL
50.9
-3.20
44.20
36.60
31.2
61.90
NS
NS
49.5
NS
Granville Co. - Oxford Landfill, Unit 1
Permit 3901-CDLF-1997 Page 1 of 8 Joyce Engineering

Table C-06: Historical MNA Parameter Data
Sample
Anal [e
Date
RL
Units
MW-IA
NM-7
MW-2
NM-3R
MW-4R
NM-5R
NM-6R
NES-1S
NES-ID
NES-2S
NES-2D
Conductivity
28-Dec-06
pS/cm
65.3
NI
104.8
NS
588.0
355.0
642.0
173.4
NS
172.2
NS
[Field Test]
11-Jul-07
pS/cm
62.5
NI
122.4
NS
631.0
373.0
604.0
NS
NS
NS
NS
19-Dec-08
pS/cm
61.0
NM
100.4
291.0
562.0
384.0
530.0
155.0
1137.0
165.0
376.0
8-Jul-09
pS/cm
17.7
NM
111.8
377.0
625.0
421.0
578.0
321.0
792.0
159.0
369.0
14-Dec-09
pS/cm
60.2
NM
83.6
304.0
564.0
373.0
540.0
374.0
527.0
109.7
382.0
23-Jun-10
pS/cm
38.0
NM
68.0
269.0
540.0
347.0
528.0
282.0
466.0
111.0
427.0
14-Dec-I0
pS/cm
Dry
NM
114.3
229.0
355.0
294.0
589.0
236.0
NS
104.0
NS
21-Jun-11
pS/cm
WL
230.0
123.5
279.0
568.0
368.0
633.0
297.0
640.0
103.0
401.0
6-Dec-I1
pS/cm
WL
237.0
104.3
251.0
548.0
360.0
607.0
348.0
518.0
129.0
331.0
13-Jun-12
pS/cm
WL
259.0
82.7
246.0
553.0
416.0
586.0
405.0
641.0
122.0
392.0
11-Dec-12
pS/cm
WL
222.2
101.6
246.5
548.0
432.0
624.0
204.6
575.0
165.6
354.5
29-Apr-13
pS/cm
WL
215.7
75.7
242.3
562.0
328.9
537.0
389.1
609.0
98.8
356.7
6-Aug-13
pS/cm
WL
286.8
81.9
292.7
636.0
414.8
590
272.4
NS
151.2
NS
25-170-14
pS/cm
WL
231.3
61.5
289.2
470.2
399.2
502
341.1
450.8
95.3
288.3
13-Aug-14
pS/cm
WL
307.3
95.4
283.0
634.0
452.4
591
NS
NS
135.2
NS
12-Mar-15
pS/cm
WL
123.4
36.9
222.8
482.9
323.5
553
NS
NS
114.2
447.9
19-Aug-15
pS/cm
WL
28.4
13.4
215.0
565.0
386.0
556
NS
NS
112.0
NS
I8-170-16
pS/cm
WL
250.0
88.7
220.8
547.0
311.6
380
NS
NS
95.7
293.9
11-Aug-16
pS/cm
WL
287.1
79.9
232.0
670.0
434.4
704
NS
NS
123.7
NS
15-170-17
pS/cm
WL
239.0
63.6
196.7
498.6
344.6
540
NS
NS
112.4
NS
24-Aug-17
pS/cm
WL
297.2
81.7
236.9
605.0
407.7
678
NS
NS
133.3
NS
7-Feb-18
pS/cm
WL
285
44.6
215
500
388
600
NS
NS
107
NS
16-Aug-18
pS/cm
WL
364
90.1
265
656
469
794
NS
NS
247
NS
Ferrous Iron (Fe)
30-Dec-03
0.1
mgA
ND
NI
NS
NS
ND
ND
NS
NS
NS
NS
NS
[Field Test]
I8-May-04
0.1
mgp
ND
NI
NS
NS
ND
0.5
NS
ND
ND
ND
ND
30-Jun-04
0.1
mgA
ND
NI
NS
NS
ND
ND
NS
ND
ND
ND
NS
28-Dec-06
0.1
mgA
0.0
NI
NS
NS
0.0
0.0
NS
0.0
NS
0.0
NS
11-Jul-07
0.1
mg/1
0.2
NI
NS
NS
0.1
0.0
NS
NS
NS
NS
NS
19-Dec-08
0.1
mg/I
0.0
NM
NS
0.0
0.0
0.0
NS
0.0
0.0
0.0
0.0
8-Jul-09
0.1
mg/1
0.0
NM
NS
0.0
0.0
0.0
NS
1.8
0.0
0.0
0.0
14-Dec-09
0.1
tog,
0.0
NM
NS
0.0
0.0
0.0
NS
2.0
0.0
0.0
0.0
23-Jun-10
0.1
mgp
0.0
NM
NS
0.0
0.0
0.0
NS
4.1
0.0
0.0
0.0
14-Dec-10
0.1
mgA
Dry
NM
NS
0.0
0.0
0.0
NS
1.1
NS
0.0
NS
21-Jun-11
NR
NS
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
6-Dec-I1
NR
NS
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
13-Jun-12
0.1
mgp
WL
0.0
NS
NS
NS
NS
NS
NS
NS
NS
NS
11-Dec-12
NR
NS
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
29-Apr-13
NR
mgp
WL
0.0
NS
0.0
0.0
0.0
NS
3.5
0.0
0.0
0.0
6-Aug-13
NR
mgA
WL
0.0
NS
0.0
0.0
0.0
NS
1.0
NS
0.75
NS
25-Feb-14
NR
mgp
WL
0.0
NS
0.0
0.0
0.0
NS
2.0
0.0
1.0
0.0
13-Aug-14
NR
mgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
12-Mar-15
0.1
mgp
WL
0.0
NS
NS
NS
0.0
NS
NS
NS
0.5
0.0
19-Aug-15
1.1
mgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
I8-Feb-16
1.1
mgA
WL
0.0
NS
NS
NS
0.0
NS
NS
NS
1.0
0.0
II-Aug-16
1.1
mg/I
WL
0.0
NS
NS
NS
0.0
NS
NS
NS
0.5
NS
15-176-17
1.1
mgp
WL
0.0
NS
NS
NS
0.0
NS
NS
NS
0.0
NS
24-Aug-17
1.1
mgA
WL
0.0
NS
NS
NS
0.0
NS
NS
NS
0.0
NS
7-Feb-18
1.1
mgp
WL
0.0
NS
NS
NS
0.0
NS
NS
NS
0.0
NS
16-Aug-18
2.1
mgA
WL
0.0
NS
NS
NS
0.0
NS
NS
NS
NS
NS
Dissolved Carbon Dioxide
11-Jul-07
mg/I
60
NI
NS
NS
50
100
NS
NS
NS
NS
NS
[Field Test]
19-Dec-08
mg/1
30
NM
NS
60
25
102
NS
40
35
35
30
8-Jul-09
mg/I
28
NM
NS
120
50
170
NS
175
40
116
40
14-Dec-09
mg/1
40
NM
NS
130
50
50
NS
235
30
70
60
234un-10
mgA
40
NM
NS
160
65
140
NS
300
60
90
30
14-Dec-10
mgp
Dry
NM
NS
135
60
136
NS
435
NS
50
NS
21-Jun-I1
NS
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
6-Dec-I1
NS
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
13-Jun-12
mg/I
WL
60
NS
NS
NS
NS
NS
NS
NS
NS
NS
11-Dec-12
NS
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
29-Apr-13
mg/I
WL
65
NS
55
35
70
NS
85
65
15
55
6-Aug-13
mgp
WL
50
NS
120
55
115
NS
155
NS
45
NS
25-Feb-14
mg/I
WL
55
NS
95
60
85
NS
95
50
30
55
13-Aug-14
mgp
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
12-Mar-15
mg/I
WL
45
NS
NS
NS
50
NS
NS
NS
35
20
19-Aug-15
mgp
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
18-Feb-16
mg/I
WL
55
NS
NS
NS
45
NS
NS
NS
105
85
,I-Aug-16
mgp
WL
70
NS
NS
NS
75
NS
NS
NS
90
NS
15-Feb-17
mg/I
WL
35
NS
NS
NS
105
NS
NS
NS
20
NS
24-Aug-17
mgp
WL
50
NS
NS
NS
90
NS
NS
NS
35
NS
7-Feb-18
mg/I
WL
50
NS
NS
NS
125
NS
NS
NS
180
NS
16-Aug-18
mgp
WL
50
NS
NS
NS
125
NS
NS
NS
NS
NS
Dissolved Oxygen (DO)
30-Dec-03
0.01
mgA
9.49
NI
NS
NS
24.19
15.31
NS
NS
NS
NS
NS
[Field Test]
18-May-04
0.01
mgp
7.15
NI
NS
NS
11.77
1.15
NS
3.48
19.25
2.24
10.70
30-Jun-04
0.01
mgA
-
NI
NS
NS
-
-
NS
12.71
9.20
3.59
4.37
28-D-06
0.01
mgA
10.30
NI
NS
NS
3.18
7.99
NS
1.62
NS
5.11
NS
11-Jul-07
0.01
mgp
8.20
NI
NS
NS
3.70
3.60
NS
NS
NS
NS
NS
19-Dec-08
0.01
mg/I
2.86
NM
NS
4.38
3.56
1.55
NS
1.22
NS
NS
8.10
8-Jul-09
0
mgp
2.78
NM
NS
1.98
088
0.48
NS
0.54
4.51
0.91
7.76
0.0
mg/I
1.34
NM
NS
50
.
3.46
2.96
NS
0.57
NS
1. 89
NS14-Dec-09
23-Jun-10
0.01mgp
4.09
NM
NS
3.
49
2.89
NS
4.76
7.98
1.56
6.06
14-Dec-10
0.01
mgA
Dry
NM
NS
8.18
4.55
2.97
NS
1.60
NS
5.85
NS
21-Jun-11
0.01
mgp
WL
7.57
NS
3.94
2.68
3.49
NS
1.55
9.12
2.63
6.20
6-De11
0.01
mgA
WL
3.82
NS
6.24
3.13
2.01
NS
1.50
8.50
1.79
8.08
13-Jun-12
0.01
mgp
WL
13.78
NS
16.46
12.22
11.31
NS
12.57
12.69
13.09
16.32
11-D-12
0.01
mgA
WL
3.51
NS
3.38
3.17
6.21
NS
0.86
8.72
1.53
7.93
29-Apr-13
0.01
mgp
WL
3.51
NS
1.27
2.75
1.87
NS
0.98
9.04
2.01
6.68
6-Aug-13
0.01
mgA
WL
2.56
NS
1.26
2.08
1.33
NS
2.43
NS
1.38
NS
25-Feb-14
0.01
mgp
WL
3.90
NS
2.11
1.42
1.42
NS
1.69
8.33
1.88
7.12
13-Aug-14
0.01
mgA
WL
3.96
NS
NS
NS
4.14
NS
NS
NS
2.22
NS
12-Mar-15
0.01
mgp
WL
3.62
NS
NS
NS
1.24
NS
NS
NS
0.74
6.17
19-Aug-15
0.01
mgA
WL
5.29
NS
NS
NS
2.46
NS
NS
NS
2.74
NS
I8-Feb46
0.01
mgp
WL
3.51
NS
NS
NS
2.59
NS
NS
NS
2.54
7.07
11-Aug-16
0.01
mgA
WL
3.60
NS
NS
NS
1.45
NS
NS
NS
1.75
NS
15-Feb47
0.01
mgp
WL
5.19
NS
NS
NS
3.80
NS
NS
NS
5.15
NS
24-Aug-17
0.01
mgA
WL
7.81
NS
NS
NS
6.74
NS
NS
NS
4.34
NS
7-Feb-18
0.01
mgp
WL
12.2
NS
NS
NS
1.91
NS
NS
NS
5.86
NS
16-Aug-18
1.01
mgA
WL
6.0
3.23
3.1
6.0
2.87
4.02
NS
NS
1.09
NS
Granville Co. - Oxford Landfill, Unit 1
Permit 3901-CDLF-1997 Page 2 of 8 Joyce Engineering

Table C-06: Historical MNA Parameter Data
Sample
Anal [e
Date
RL
Units
MW-IA
NM-7
MW-2
NM-3R
MW-4R
MW-5R
M W-6R
NES-is
NES-ID
NES-2S
NES-2D
Dissolved Hydrogen
19- De'-08
0.600
nM
0.920
NM
NS
1.300
2.500
1.300
NS
1.100
NS
1.1
NS
8-Jul-09
1.600
nM
NS(dry)
NM
NS
LI00
2.100
1.400
NS
1.900
4.200
4.900
NS(dry)
14-Dec-09
0.600
nM
1.000
NM
NS
1.100
3.000
1.000
NS
0.880
2.500
0.750
NS(dry)
23-Jun-10
0.600
nM
4.400
NM
NS
4.500
5.600
3.700
NS
4.000
9.100
4.000
NS(dry)
14-Dec-10
0.600
nM
Dry
NM
NS
0.800
1.500
1.000
NS
1.000
NS
0.620
NS(dry)
21-Jun-l1
0.600
nM
WL
1.30
NS
1.400
2.900
1.400
NS
1.100
3.800
1.100
NS(dry)
6-Dec-11
0.60
nM
WL
2.4
NS
3.6
5.4
5.6
NS
5.3
5.2
3.4
NS(dry)
13-Jun-12
0.60
nM
WL
0.81
NS
2.7
4.7
3.8
NS
2.8
3.5
0.83
NS(dry)
11-Dec-12
0.60
nM
WL
0.53 J
NS
0.46 J
3.0
0.6
NS
0.056 J
0.53 J
0.22 J
NS
29-Apr-13
0.60
nM
WL
0.38 J
NS
0.41 J
1.9
NS
NS
0.37 J
1.3
0.39 J
0.42 J
6-Aug-13
0.60
nM
WL
0.84
NS
0.98
0.83
0.79
NS
1.0
NS
0.84
NS
25-Feb-l4
0.60
nM
WL
0.65
NS
0.92
0.77
0.86
NS
1.1
0.81
0.70
0.81
13-Aug-14
0.60
nM
WL
1.3
NS
NS
NS
1.2
NS
NS
NS
1.1
NS
12-Mar-15
0.60
nM
WL
1.5
NS
NS
NS
-
NS
NS
NS
1.2
1.5
30-Apr-15
0.60
nM
WL
NS
NS
NS
NS
1.5
NS
NS
NS
NS
NS
19-Aug-15
0.60
nM
WL
1.6
NS
NS
NS
2.0
NS
NS
NS
1.7
NS
18-Feb-16
0.60
nM
WL
2.9
NS
NS
NS
10.0
NS
NS
NS
2.2
NS
11-Aug-16
0.60
nM
WL
0.85
NS
NS
NS
1.6
NS
NS
NS
1.3
NS
15-Feb-17
0.60
nM
WL
2.2
NS
NS
NS
2.1
NS
NS
NS
2.2
NS
24-Aug-17
0.60
nM
WL
2.6
NS
NS
NS
3.3
NS
NS
NS
2.5
NS
7-Feb-18
0.60
nM
WL
12
NS
NS
NS
2.9
NS
NS
NS
2.1
NS
16-Aug-18
1.0
nM
WL
6.4
NS
NS
NS
4.3
NS
NS
NS
4.8
NS
Chloride
30-Dec-03
1
mgA
3
NI
NS
NS
17
24
NS
NS
NS
NS
NS
18-May-04
1
mgp
3.2
NI
NS
NS
26
26
NS
6.3
16
6.2
9.1
30-Jun-04
1
mgA
2.5
NI
NS
NS
28
26
NS
8.1
15
7.8
4.3
28-Dec-06
5
mgA
1.8
NI
NS
NS
22
18
NS
4.7
NS
6.6
NS
11-Jul-07
5
mgp
0.66 (2.6)
NI
NS
NS
17 (34)
15 (29)
NS
NS
NS
NS
NS
19-Dec-08
5
mgA
5.7
NM
NS
37.0
39.4
36.4
NS
16.0
10.8
12.6
6.2
8-Jul-09
5
mgp
6.8
NM
NS
46.8
39.1
38.6
NS
23.1
11.3
7.7
28.4
14-Dec-09
5.0
mgA
ND
NM
NS
36.4
38.8
37.6
NS
33.0
1 L5
5.5
6.2
23-Jun-10
5.0
mgp
7.91
NM
ND
37.4
40.0
39.7
97.9
17.6
13.4
5.97
6.5
14-Dec-I0
5.0
mgA
Dry
NM
5.1
38.4
44.5
39.6
108.0
29.1
NS
16.40
NS
NC-2L 250,000 ug/L
21-Jun-11
5.0
mgp
WL
8.6
ND
35.8
45.3
41.4
106.0
23.3
13.5
6.60
6.07
6-Dec-11
5.0
nM
WL
9.34
ND
28.6
49.2
39.2
110.0
47.8
22.5
13.9
6.2
13-Jun-12
5.0
mgp
WL
9.41
4.54
29.4
49.3
46.4
109.0
44.4
26.7
7.77
6.36
11-Dec-12
1.0
mgA
WL
8.57
5.22
30.8
50.6
46.6
107.0
40.1
25.7
15.6
6.26
29-Apr-13
1.0
mgp
WL
9.55
4.12
30.0
49.8
22.3
122.0
44.9
31.1
5.94
6.08
6-Aug-13
1.0
mgA
WL
7.59
5.18
25.7
50.1
48.7
107.0
24.8
NS
7.05
NS
25-170-14
1.0
mgp
WL
9.22
5.51
33.2
60.3
57.4
120.0
26.9
29.2
5.39
6.53
13-Aug-14
1.0
mgA
WL
8.03
4.07
21.3
97.6
43.4
106.0
NS
NS
5.61
NS
12-Mar-15
1.0
mgp
WL
8.84
43.5
20.7
51.7
42.6
121.0
NS
NS
5.81
5.58
19-Aug-15
1.0
mgA
WL
9.44
5.16
23.2
51.5
48.5
111.0
NS
NS
6.35
NS
I8-170-16
1.0
mgp
WL
17.2
4.60
20.6
69.5
49.7
153.0
NS
NS
6.28
5.65
11-Aug-16
1.0
mgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
7.08
NS
15-Feb-l7
1.0
mgp
WL
10.9
4.97
29.3
59.1
49.2
142.0
NS
NS
6.83
NS
24-Aug-17
1.0
mgA
WL
10.2
4.12
21.7
59.3
46.6
136.0
NS
NS
8.49
ND
7-Feb-18
2.0
mgp
WL
10.0
4.79
23.0
60.2
58.6
149.0
NS
NS
7.43
NS
16-Aug-18
1.0
mgA
WL
9.62
NS
NS
NS
50.6
NS
NS
NS
7.19
NS
Nitrate
30-Dec-03
0.10
mgp
0.23
NI
NS
NS
ND
ND
NS
NS
NS
NS
NS
18-May-04
0.10
mgA
0.21
NI
NS
NS
ND
ND
NS
ND
1.10
0.14
ND
30-Jun-04
0.10
mgp
0.15
NI
NS
NS
ND
ND
NS
ND
0.95
0.20
ND
28-Dec-06
100.0
mgp
0.15
NI
NS
NS
0.51
0.33
NS
0.36
NS
0.43
NS
11-Jul-07
100.0
mgA
0.14
NI
NS
NS
0.111
0.031
NS
NS
NS
NS
NS
19-Dec-08
100.0
mgA
ND
NM
NS
ND
ND
ND
NS
ND
ND
ND
ND
8-Jul-09
200.0
mgA
ND
NM
NS
ND
ND
ND
NS
ND
ND
ND
0.30
14-Dec-09
0.10
mgp
ND
NM
NS
ND
ND
ND
NS
ND
ND
ND
ND
23-Jun-10
0.10
mgA
ND
NM
NS
ND
ND
ND
NS
ND
ND
183
107
14-Dec-10
0.10
mgp
Dry
NM
NS
ND
ND
ND
NS
ND
NS
ND
NS
21-Jun-ll
0.10
mgA
WL
ND
NS
ND
ND
ND
NS
ND
ND
0.146
ND
6-13ec-11
0.10
mgp
WL
ND
NS
ND
ND
ND
NS
ND
ND
ND
ND
13-Jun-12
0.10
mgA
WL
0.181
NS
0.0743
ND
ND
NS
ND
0.0798
0.162
0.251
11-Dec-12
10.00
mgp
WL
0.115 J
NS
0.0655 J
ND
0.0326 J
NS
0.0557 J
0.022
ND
0.192 J
29-Apr-13
0.02
mgA
WL
0.0938
NS
0.0280
ND
ND
NS
ND
0.0298
0.0851
0.141
6-Aug-13
10.00
mgp
WL
0.0999 J
NS
ND
ND
ND
NS
ND
NS
ND
NS
25-Feb-14
10.00
mgA
WL
NS
NS
ND
ND
ND
ND
ND
ND
ND
0.417 J
13-Aug-14
10.00
mgA
WL
0.144 J
NS
NS
NS
ND
NS
NS
NS
ND
NS
12-Mar-15
10.00
mgA
WL
0.134 J
NS
NS
NS
0.0224 J
NS
NS
NS
ND
0.229 J
19-Aug-15
10.00
mgp
WL
0.186 J
NS
NS
NS
ND
NS
NS
NS
ND
NS
18-Feb-16
10.00
mgA
WL
0.179 J
NS
NS
NS
0.0373 J
NS
NS
NS
ND
0.122 J
11-Aug-16
10.00
mgp
WL
0.196 J
NS
NS
NS
0,0211 J
NS
NS
NS
0.0126 J
NS
15-Feb-17
10.00
mgA
WL
0.22 J
NS
NS
NS
0.0875 J
NS
NS
NS
0.0116 J
NS
24-Aug-17
10.00
mgp
WL
0.205 J
NS
NS
NS
0.0339 J
NS
NS
NS
0.0399 J
NS
7-Feb-18
10.00
mgA
WL
0.205 J
NS
NS
NS
ND
NS
NS
NS
0.0338 J
NS
16-Aug-18
0.10
mgp
WL
0.198
NS
NS
NS
ND
NS
NS
NS
ND
NS
Nitrite
28-Dec-06
mgp
<0.100
NI
NS
NS
<0.100
<0.100
NS
<0.100
NS
<0.100
NS
11-Jul-07
mgA
<0.1
NI
NS
NS
<0.1
<0.1
NS
NS
NS
NS
NS
14-Dec-10
mgp
Dry
NM
NS
NS
NS
NS
NS
NS
NS
NS
NS
21-Jun-ll
mgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
6-Dec-11
mgp
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
13-Jun-12
mgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
11-Dec-12
mgp
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
29-Apr-13
mgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
6-Aug-13
mgp
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
25-Feb-14
mgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
13-Aug-14
mgp
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
12-Mar-15
mgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
19-Aug-15
mgp
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
18-Feb-16
mgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
,I-Aug-16
mgp
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
15-Feb-17
mgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
24-Aug-17
mgp
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
7-Feb-18
mgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
16-Aug-18
mgp
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Granville Co. - Oxford Landfill, Unit 1
Permit 3901-CDLF-1997 Page 3 of 8 Joyce Engineering

Table C-06: Historical MNA Parameter Data
Sample
Anal [e
Date
RL
Units
MW-IA
MW-7
MW-2
MW-3R
MW-4R
MR
W-5W-6R
M
NES-IS
NES-1D
NES-2S
NES-2D
Sulfate
30-Dec-03
2.0
mgp
4.0
NI
NS
NS
17
2.7
NS
NS
NS
NS
NS
18-May-04
2.0
mgA
3.3
NI
NS
NS
40
2.8
NS
21
120
5.6
13
30-Jun-04
2.0
mgp
ND
NI
NS
NS
29
ND
NS
5.5
180
4.7
12
28-Dec-06
5
mgp
0.03
NI
NS
NS
10
4.6
NS
5.2
NS
12
NS
11-Jul-07
5
mgA
1.6
NI
NS
NS
13
2.2
NS
NS
NS
NS
NS
19-Dec-08
5
mgp
11.2
NM
NS
9.6
9
ND
NS
5.3
191
16.1
18.3
8-Jul-09
5
mgA
1140
NM
NS
8.4
9.3
ND
NS
5.2
161
8.4
39.2
14-Dec-09
5
mgp
ND
NM
NS
6.9
7.3
ND
NS
ND
79.5
6.5
49.7
23-Jun-10
5
mg/I
5.16
NM
14.8
7.18
9.14
ND
ND
ND
ND
25.1
ND
14-Dec-10
5
mgp
Dry
NM
14.5
9.21
9.7
ND
ND
5.38
NS
10.80
NS
21-Jun-11
5
mgA
WL
24.4
11.4
7.49
7.74
ND
ND
ND
91.9
ND
ND
NC-21,250,000 ug/L
6-Dec-I 1
5
mgp
WL
ND
NS
ND
ND
ND
NS
ND
31.4
11.80
52.9
13-Jun-12
5
mg/I
WL
25.4
13.7
8.14
8.4
2.79
3.04
4.70
24.5
5.38
83.1
11-Dec-12
2
mgp
WL
28.0 J
14.8 J
9.12 J
10.1 J
4.42 J
2.90 J
3.16 J
36.0
7.91 J
78.8
29-Apr-13
250
mgA
WL
26.1 J
12.3 J
9.15 J
17.1 J
2.73 J
3.20 J
5.23 J
57.0 J
4.61 J
73.8 J
6-Aug-13
250
mgp
WL
25.3 J
7.37 J
7.83 J
11.7 J
2.76 J
3.32 J
4.29 J
NS
5.07 J
NS
25-Feb-14
250
mgA
WL
28.9 J
11.2 J
8.13 J
9.55 J
2.59 J
4.62 J
3.59 J
10.4 J
33.8 J
4.56 J
13-Aug-14
250
mgp
WL
31.9 J
9.37 J
7.91 J
11.6 J
2.45 J
2.78 J
NS
NS
4.46 J
NS
12-Mar-15
250
mg/I
WL
32.6 J
12.1 J
8.04 J
8.34 J
3.34 J
3.33 J
NS
NS
4.81 J
83.4 J
19-Aug-15
250
mgp
WL
42.9 J
102 J
8.11 J
10.4 J
2.89 J
3.21 J
NS
NS
4.93 J
NS
18-Feb-16
250
mgA
WL
39.9 J
112 J
7.96 J
10.3 J
3.83 J
3.31
NS
NS
4.84 J
54.7 J
II-Aug-16
250
mgp
WL
NS
NS
NS
NS
NS
NS
NS
NS
5.33 J
NS
15-Feb-17
250
mgA
WL
47.1 J
11.2 J
7.86 J
7.94 J
3.55 J
3.26
NS
NS
5.31 J
NS
24-Aug-17
250
mgp
WL
50.3 J
NS
NS
NS
7.14 J
NS
NS
NS
6.29 J
NS
7-Feb-18
250
mgA
WL
42.8 J
7.99 J
6.65 J
6.11 J
4.00 J
2.06 J
NS
NS
5.56 J
NS
16-Aug-18
250
mgp
WL
55.2 J
7.69 J
7.13 J
6.47 J
4.40 J
2.65 J
NS
NS
7.30 J
ND
Sulfide
30-Dec-03
1.0
mgA
ND
NI
NS
NS
5.0
ND
NS
NS
NS
NS
NS
I8-May-04
1.0
mgA
ND
NI
NS
NS
ND
ND
NS
ND
ND
ND
ND
30-Jun-04
1.0
mgA
ND
NI
NS
NS
ND
ND
NS
ND
ND
ND
ND
19-Dec-08
1000
µg/I
259 J
NM
ND
150 J
ND
141 J
ND
ND
ND
ND
ND
8-Jul-09
1000
41
ND
NM
ND
ND
ND
ND
ND
ND
ND
ND
ND
14-Dec-09
1000
µg/I
ND
NM
ND
ND
ND
ND
ND
ND
ND
ND
ND
23-Jun-10
1000
µgA
ND
NM
ND
ND
ND
ND
ND
ND
ND
ND
ND
14-Dec-10
1000
µ9/1
Dry
NM
ND
ND
ND
ND
ND
ND
NS
ND
NS
21-Jun-11
1000
µgp
WL
ND
ND
ND
ND
ND
ND
NS
NS
NS
NS
6-Dec-11
1000
µg/I
WL
ND
ND
ND
ND
ND
ND
NS
NS
NS
NS
13-Jun-12
1000
µgA
WL
ND
ND
ND
ND
ND
ND
NS
NS
NS
NS
11-Dec-12
1000
µg/I
WL
ND
ND
ND
ND
117 J
NS
NS
NS
NS
NS
29-Apr-13
1000
µgA
WL
ND
ND
ND
ND
ND
ND
NS
NS
NS
NS
6-Aug-13
1000
µgA
WL
ND
ND
ND
ND
ND
ND
ND
NS
ND
NS
25-Feb-14
1000
41
WL
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
13-Aug-14
1000
µgA
WL
ND
NS
NS
NS
ND
NS
NS
NS
ND
NS
12-Mar-15
1000
µg/1
WL
ND
NS
NS
NS
ND
NS
NS
NS
ND
NS
19-Aug-15
1000
µgA
WL
ND
NS
NS
NS
ND
NS
NS
NS
ND
NS
I8-Feb-16
1000
41
WL
ND
NS
NS
NS
ND
NS
NS
NS
ND
NS
11-Aug-16
1000
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
15-17eb47
1000
41
WL
ND
NS
NS
NS
ND
NS
NS
NS
ND
NS
24-Aug-17
1000
µgA
WL
ND
NS
NS
NS
ND
NS
NS
NS
ND
NS
7-Feb-18
1000
41
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
16-Aug-18
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Hydrogen Sulfide
30-Dec-03
1.0
mgp
ND
NI
NS
NS
21
ND
NS
NS
NS
NS
NS
18-May-04
1.0
mgA
ND
NI
NS
NS
ND
ND
NS
ND
ND
ND
ND
30-Jun-04
1.0
mgA
ND
NI
NS
NS
ND
ND
NS
ND
ND
ND
ND
28-Dec-06
1.0
mgA
ND
NI
NS
NS
ND
ND
NS
ND
NS
ND
NS
11-Jul-07
1.0
mgA
ND
NI
NS
NS
ND
ND
NS
ND
NS
ND
NS
14-Dec-10
NR
mgp
Dry
NM
NS
NS
NS
NS
NS
NS
NS
NS
NS
21-Jun-11
NR
mgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
6-Dec-11
NR
mgp
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
13-Jun-12
1.0
mgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
11-Dec-12
NR
mgp
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
29-Apr-13
NR
mgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
6-Aug-13
NR
mgp
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
25-Feb-14
NR
mg/I
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
13-Aug-14
NR
mgp
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
12-Mar-15
NR
mg/I
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
19-Aug-15
NR
mgp
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
18-Feb-16
NR
mgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
,I-Aug-16
NR
mgp
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
15-Feb-17
NR
mgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
24-Aug-17
NR
mgp
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
7-Feb-18
NR
mgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Total Organic Carbon (TOC)
11-Jul-07
1
mgA
0.48
NI
NS
NS
3.2
1.9
NS
NS
NS
NS
NS
19-1)ec-08
1
mgp
6.3
NM
NS
48
24.7
21.1
NS
21.2
22.8
11.4
19.1
8-Jul-09
1
mgA
28.1
NM
NS
6.6
5.9
6.2
NS
3.4
5.7
4.2
4.4
14-Dec-09
1
mgp
3.0
NM
NS
32.4
48.2
ND
NS
11.5
5.0
2.9
3.8
23-Jun-10
1
mgA
3.7
NM
NS
3.16
5.8
6.07
NS
2.91
5.96
2.82
3.61
14-Dec-10
1
mgp
Dry
NM
NS
23.7
7.52
7.77
NS
23
NS
5.01
NS
21-Jun-I1
NR
mgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
6-Dec-II
NR
mgp
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
13-Jun-12
1
mgA
WL
3.71
NS
NS
NS
NS
NS
NS
NS
NS
NS
11-Dec-12
NR
mgp
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
29-Apr-13
NR
mgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
6-Aug-13
1
mgp
WL
4.68
NS
7.42
8.93
9.63
NS
12.4
NS
4.08
NS
25-Feb-14
1
mgA
WL
NS
NS
8.62
20.4
19.9
NS
33.7
26.2
9.50
8.03
13-Aug-14
1
mgp
WL
4.55
NS
NS
NS
8.34
NS
NS
NS
4.33
NS
12-Mar-15
1
mgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
19-Aug-15
1
mgp
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
18-Feb-16
1
mgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
,I-Aug-16
1
mgp
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
15-Feb-17
1
mgA
WL
ND
NS
NS
NS
1.7
NS
NS
NS
0,87 J
NS
24-Aug-17
1.0
mgp
WL
0.91 J
NS
NS
NS
2.3
NS
NS
NS
0.87 J
NS
7-Feb-18
NR
mgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
16-Aug-18
NR
mgp
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Granville Co. - Oxford Landfill, Unit 1
Permit 3901-CDLF-1997 Page 4 of 8 Joyce Engineering

Table C-06: Historical MNA Parameter Data
Sample
Anal to
Date
RL
Units
MW-IA
MW-7
MW-2
MW-3R
MW-4R
MW-5R
MW-6R
NES-1S
NES-ID
NES-2S
NES-2D
AlkaliniTy
30-Dec-03
10
mgp
14
NI
NS
NS
90
130
NS
NS
NS
NS
NS
(total as CaCO3)
18-May-04
10
mgA
ND
NI
NS
NS
210
140
NS
56
260
63
81
30-Jun-04
10
mgp
11
NI
NS
NS
240
160
NS
120
280
46
130
28-Dec-06
5
mgp
10
NI
NS
NS
255
133
NS
57
NS
42
NS
11-Jul-07
5
mgA
20
NI
NS
NS
220
150
NS
NS
NS
NS
NS
19-Dec-08
5
mgp
18.9
NM
NS
88.2
296
163
NS
76.7
202
44.2
222
8-Jul-09
6
mgA
16.5
NM
NS
110
301
176
NS
137
278
44.0
155
14-Dec-09
5
mgp
6.7
NM
NS
82.1
253
135
NS
134
210
29.6
137
23-Jun-10
5
mgA
7.29
NM
20.4
99.8
291
169
178.0
134
262
39.7
170
14-Dec-10
5
mgp
Dry
NM
17.6
99.6
292
168
156
168
NS
39.4
NS
21-Jun-11
5
mgA
WL
100
20.8
77
269
194
156
128
288.0
42.2
153.0
6-Dec-l1
5
mgp
WL
98.7
10.5
81.9
274
164
151
146
297
35.7
144
13-Jun-12
5
mgA
WL
101
13.7
87.5
271
152
149
152
309
46.2
147
11-Dec-12
5
mgp
WL
100
16.5
98.3
284
147
152
130
339
44.6
148
29-Apr-13
5
mgA
WL
99.3
13.8
97.3
293
156
153
180
339
46.2
143
6-Aug-13
5
mgp
WL
102
14.3
99.1
148
86.8
159
123
NS
43.3
NS
25-Feb-14
5
mgA
WL
98
15.8
123
298
178
153
145
303
164
3.87
13-Aug-14
5
mgp
WL
103
14.3
93.8
301
187
164
NS
NS
49.8
NS
12-Mar-15
5
mgA
WL
99.7
14.7
88.3
306
151
164
NS
NS
39.5
139
19-Aug-15
5
mgp
WL
102
19.6
88.2
294
180
164
NS
NS
46.9
NS
18-Feb-16
5
mgA
WL
108
4.35 J
89.8
308
141
168
NS
NS
49.6
150
11-Aug-16
5
mgp
WL
NS
NS
NS
NS
NS
NS
NS
NS
51.6
NS
15-Feb-17
5
mgA
WL
115
16.0
92.8
300
168
183
NS
NS
48.2
NS
24-Aug-17
5
mgp
WL
129
26.8
98.5
329
177
195
NS
NS
56.7
ND
7-Feb-18
5
mgA
WL
125
6.9
101
330
199
207
NS
NS
55.6
NS
16-Aug-18
5
mgp
WL
123
22.1
93.2
302
186
203
NS
NS
58.3
NS
Ethane
30-Dec-03
0.001
mgA
ND
NI
NS
NS
ND
ND
NS
NS
NS
NS
NS
I8-May-04
0.001
mgA
ND
NI
NS
NS
ND
ND
NS
ND
ND
ND
ND
30-Jun-04
0.001
mgA
ND
NI
NS
NS
ND
ND
NS
ND
ND
ND
ND
28-Dec-06
20.0
mgA
ND
NI
NS
NS
ND
ND
NS
ND
NS
ND
NS
11-Jul-07
20.0
mgp
ND
NI
NS
NS
ND
ND
NS
NS
NS
NS
NS
19-Dec-08
20.0
µg/I
ND
NM
NS
ND
ND
ND
NS
ND
ND
ND
ND
8-Jul-09
10.0
µg/1
ND
NM
NS
ND
ND
ND
NS
ND
ND
ND
ND
14-Dec-09
10.0
µ9/1
ND
NM
NS
ND
ND
ND
NS
ND
ND
ND
ND
23-Jun40
10.0
µgA
ND
NM
NS
ND
ND
ND
NS
ND
ND
ND
ND
14-Dec-10
10.0
µg/l
Dry
NM
NS
ND
ND
ND
NS
ND
NS
ND
NS
21-Jun41
NR
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
6-Dec-11
NR
µ9/1
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
13-Jun-12
10.0
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
11-Dec-12
NR
µg/l
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
29-Apr-13
NR
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
6-Aug-13
6.2
µgA
WL
NS
NS
ND
ND
ND
NS
ND
NS
ND
NS
25-Feb-14
6.2
µg/l
WL
NS
NS
ND
ND
ND
NS
ND
ND
ND
ND
13-Aug-14
6.2
µgA
WL
ND
NS
NS
NS
ND
NS
NS
NS
ND
NS
12-Mar-15
6.2
µg/l
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
19-Aug-15
6.2
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
I8-Feb-16
6.2
µg/l
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
11-Aug-16
6.2
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
15-Feb-17
6.2
µg/l
WL
ND
NS
NS
NS
ND
NS
NS
NS
ND
NS
24-Aug-17
6.2
µgA
WL
ND
NS
NS
NS
ND
NS
NS
NS
ND
NS
7-Feb-18
NR
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
16-Aug-18
NR
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Ethylene (Ethene)
30-Dec-03
0.001
mgp
ND
NI
NS
NS
ND
ND
NS
NS
NS
NS
NS
18-May-04
0.001
mgA
ND
NI
NS
NS
ND
ND
NS
ND
ND
ND
ND
30-Jun-04
0.001
mgp
ND
NI
NS
NS
ND
ND
NS
ND
ND
ND
ND
28-Dec-06
20.0
mgp
ND
NI
NS
NS
ND
ND
NS
ND
NS
ND
NS
11-Jul-07
20.0
mgA
ND
NI
NS
NS
ND
ND
NS
NS
NS
NS
NS
19-Dec-08
20.0
µg/1
ND
NM
NS
ND
ND
ND
NS
ND
ND
ND
ND
8-Jul-09
10.0
µgA
ND
NM
NS
ND
ND
ND
NS
ND
ND
ND
ND
14-Dec-09
10.0
µg/1
ND
NM
NS
ND
ND
ND
NS
ND
ND
ND
ND
23-Jun-10
11.0
µgA
ND
NM
NS
ND
ND
ND
NS
ND
ND
ND
ND
14-Dec-10
10.0
µg/1
Dry
NM
NS
ND
ND
ND
NS
ND
NS
ND
NS
21-Jun-11
NR
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
6-Dec-11
NR
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
13-Jun-12
10.0
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
11-Dec-12
NR
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
29-Apr-13
NR
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
6-Aug-13
6.2
µgA
WL
NS
NS
ND
ND
ND
NS
ND
NS
ND
NS
25-Feb-14
6.2
µgA
WL
NS
NS
ND
ND
ND
NS
ND
ND
ND
ND
13-Aug-14
6.2
µgA
WL
ND
NS
NS
NS
ND
NS
NS
NS
ND
NS
12-Mar-15
6.2
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
19-Aug-15
6.2
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
18-Feb-16
6.2
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
11-Aug-16
6.2
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
15-Feb-17
6.2
µgA
WL
ND
NS
NS
NS
ND
NS
NS
NS
ND
NS
24-Aug-17
6.2
µgA
WL
ND
NS
NS
NS
ND
NS
NS
NS
ND
NS
7-Feb-18
NR
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
16-Aug-18
NR
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Granville Co. - Oxford Landfill, Unit 1
Permit 3901-CDLF-1997 Page 5 of 8 Joyce Engineering

Table C-06: Historical MNA Parameter Data
Sample
Anal to
Date
RL
Units
MW-IA
MW-7
MW-2
MW-3R
MW-4R
MW-5R
MW-6R
NES-1S
NES-ID
NES-2S
NES-2D
Methane
30-Dec-03
0.001
mgp
ND
NI
NS
NS
1.8
0.1
NS
NS
NS
NS
NS
18-May-04
0.001
mgA
ND
NI
NS
NS
1.50
0.12
NS
0.09
0.46
0.004
ND
30-Jun-04
0.001
mgp
ND
NI
NS
NS
0.66
0.06
NS
0.26
ND
ND
ND
28-Dec-06
10.0
mgp
0.01
NI
NS
NS
0.173
0.044
NS
0.021
NS
0.001
NS
11-Jul-07
10.0
mgA
0.001
NI
NS
NS
0.189
0.008
NS
NS
NS
NS
NS
19-Dec-08
10.0
mgp
ND
NM
NS
0.0054 J
0.162
0.102
NS
0.0164
ND
ND
ND
8-Jul-09
10.0
mg/I
ND
NM
NS
0.0202
0.088
0.128
NS
0.226
ND
ND
ND
14-Dec-09
10.0
mgp
ND
NM
NS
0.0083 J
0.0205
0.0648
NS
1.130
ND
ND
ND
23-Jun-10
0.010
mg/I
0.0018 B
NM
NS
0.0117 B
0.064
0.101
NS
0.415
0.002 B
0.0012 B
0.0013 B
14-Dec-10
0.010
mgA
Dry
NM
NS
0.0025 J
0.155
0.102
NS
0.510
NS
ND
NS
21-Jun-11
0.010
mg/I
WL
0.0016 J
NS
0.099 J
0.103
0.108
NS
0.770
0.0017 J
0.0014 J
0.0017 J
6-Dec-11
0.010
mgp
WL
ND
NS
0.009 J
0.032
0.086
NS
0.376
ND
ND
ND
13-Jun-12
0.010
mg/I
WL
0.0011 J
NS
0.0062 J
0.0524
0.0698
NS
0.157
0.0017 J
0.0015 J
0.0013 J
11-Dec-12
0.01
mgp
WL
ND
NS
0.0036
0.0825
0.0506
NS
0.183
ND
ND
ND
29-Apr-13
0.01
mg/I
WL
ND
NS
0.0180
0.0737
0.0923
NS
1.290
ND
ND
ND
6-Aug-13
0.0066
mgp
WL
ND
NS
0.0229
0.0590
0.113
NS
0.284
NS
0.060
NS
25-Feb-14
0.0066
mgA
WL
ND
NS
0.0170
0.0703
0.0263
NS
0.498
ND
ND
ND
13-Aug-14
0.0066
mgp
WL
ND
NS
NS
NS
0.108
NS
NS
NS
0.339
NS
12-Mar-15
0.0066
mg/I
WL
ND
NS
NS
NS
0.0188
NS
NS
NS
0.330
0.0119
19-Aug-15
0.0066
mgp
WL
0.89 J
NS
NS
NS
0.0398
NS
NS
NS
0.340
NS
18-Feb-16
0.0066
mg/I
WL
0.0018 J
NS
NS
NS
0.0218
NS
NS
NS
0.512
0.0019 J
11-Aug-16
0.0066
mgp
WL
0.0025 J
NS
NS
NS
0.0676
NS
NS
NS
0.409
NS
15-Feb-17
0.0100
mg/I
WL
ND
NS
NS
NS
0.0949
NS
NS
NS
0.336
NS
24-Aug-17
0.0100
mgp
WL
ND
NS
NS
NS
0.0541
NS
NS
NS
0.263
NS
7-Feb-18
0.0100
mg/I
WL
0.0054 J
NS
NS
NS
0.0528
NS
NS
NS
0.0050 J
NS
16-Aug-18
0.0100
mgp
WL
ND
NS
NS
NS
0.0945
NS
NS
NS
0.0570
NS
Pyru,c Acid
28-Dec-06
100
µg/1
ND
NI
NS
ND
ND
ND
NS
ND
ND
ND
NS
19-Dec-08
100
µg/I
ND
NM
NS
ND
ND
ND
NS
ND
ND
ND
ND
8-Jul-09
10000
µg/1
ND
NM
NS
ND
ND
ND
NS
ND
ND
ND
ND
14-Dec-09
10000
µg/I
ND
NM
NS
ND
ND
ND
NS
ND
ND
ND
ND
23-Jun-10
10000
µgA
ND
NM
NS
ND
ND
ND
NS
ND
ND
ND
2800 J
14-Dec-10
10000
µ9/1
Dry
NM
NS
ND
ND
ND
NS
ND
NS
ND
NS
21-Jun-11
NR
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
6-Dec-11
NR
µg/I
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
13-Jun-12
10000
µgA
WL
ND
NS
NS
NS
NS
NS
NS
NS
NS
NS
11-Dec-12
NR
µg/I
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
29-Apr-13
NR
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
6-Aug-13
10000
µg/I
WL
NS
NS
ND
ND
ND
NS
ND
NS
ND
NS
25-Feb-14
10000
µg/1
WL
NS
NS
ND
ND
ND
NS
ND
ND
ND
ND
13-Aug-14
10000
µg/I
WL
ND
NS
NS
NS
ND
NS
NS
NS
ND
NS
12-Mar-15
10000
µg/1
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
19-Aug-15
10000
µg/I
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
I8-Feb-16
10000
µg/1
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
11-Aug-16
10000
µg/I
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
15-Feb-17
10000
µg/1
WL
ND
NS
NS
NS
ND
NS
NS
NS
ND
NS
24-Aug-17
10000
µg/I
WL
ND
NS
NS
NS
1600 J
NS
NS
NS
ND
NS
7-Feb-18
NR
41
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
16-Aug-18
NR
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Lactic Acid
28-Dec-06
1000
µg/I
ND
NI
NS
ND
ND
NS
NS
ND
ND
ND
NS
19-Dec-08
1000
µg/1
ND
NM
NS
ND
ND
4300
NS
ND
ND
ND
ND
8-Jul-09
25000
µg/I
ND
NM
NS
ND
ND
ND
NS
ND
ND
ND
ND
14-Dec-09
25000
µg/1
ND
NM
NS
ND
ND
ND
NS
ND
ND
ND
ND
23-Jun-10
25000
µg/I
ND
NM
NS
ND
ND
ND
NS
ND
ND
1900 J
ND
14-Dec-10
25000
µg/1
Dry
NM
NS
ND
ND
ND
NS
ND
NS
ND
NS
21-Jun-11
NR
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
6-Dec-11
NR
µg/1
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
13-Jun-12
25000
µg/I
WL
ND
NS
NS
NS
NS
NS
NS
NS
NS
NS
11-Dec-12
NR
µg/1
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
29-Apr-13
NR
µg/I
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
6-Aug-13
25000
µg/1
WL
NS
NS
ND
ND
ND
NS
ND
NS
ND
NS
25-F6-14
25000
µg/I
WL
NS
NS
ND
ND
ND
NS
ND
ND
ND
ND
13-Aug-14
25000
µg/1
WL
ND
NS
NS
NS
ND
NS
NS
NS
ND
NS
12-Mar-15
25000
µg/I
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
19-Aug-15
25000
µg/1
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
18-Feb-16
25000
µg/I
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
11-Aug-16
25000
µg/1
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
15-Feb-17
25000
µg/I
WL
ND
NS
NS
NS
ND
NS
NS
NS
ND
NS
24-Aug-17
25000
µg/1
WL
ND
NS
NS
NS
ND
NS
NS
NS
ND
NS
7-Feb-18
NR
µg/I
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
16-Aug-18
NR
µg/1
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Acetic Acid
28-Dec-06
1000
µg/1
ND
NI
NS
NS
ND
ND
NS
ND
NS
ND
NS
19-Dec-08
1000
µg/I
ND
NM
NS
1200
ND
ND
NS
ND
1000
ND
1600
8-Jul-09
1000
µg/1
ND
NM
NS
700 J
ND
ND
NS
ND
ND
700 J
ND
14-Dec-09
1000
µg/I
ND
NM
NS
ND
ND
ND
NS
ND
ND
ND
ND
23-Jun-10
1000
µg/1
ND
NM
NS
ND
ND
ND
NS
ND
ND
ND
ND
14-Dec-10
1000
µg/I
Dry
NM
NS
ND
600 J
2400
NS
ND
NS
ND
NS
21-Jun-11
NR
µg/1
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
6-Dec-11
NR
µg/I
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
13-Jun-12
1000
µg/1
WL
ND
NS
NS
NS
NS
NS
NS
NS
NS
NS
11-Dec-12
NR
µg/I
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
29-Apr-13
NR
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
6-Aug-13
5000
µgA
WL
NS
NS
ND
ND
ND
NS
ND
NS
ND
NS
25-Feb-14
5000
µgA
WL
NS
NS
ND
ND
ND
NS
ND
ND
ND
ND
13-Aug-14
5000
µgA
WL
ND
NS
NS
NS
ND
NS
NS
NS
ND
NS
12-Mar-15
5000
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
19-Aug-15
5000
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
I8-Feb-16
5000
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
11-Aug-16
5000
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
15-Feb-17
5000
µgA
WL
ND
NS
NS
NS
710 J
NS
NS
NS
950 J
NS
24-Aug-17
5000
µgA
WL
380 J
NS
NS
NS
7400
NS
NS
NS
4100 J
NS
7-Feb-18
NR
µgp
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
16-Aug-18
NR
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Granville Co. - Oxford Landfill, Unit 1
Permit 3901-CDLF-1997 Page 6 of 8 Joyce Engineering

Table C-06: Historical MNA Parameter Data
Sample
Anal to
Date
RL
Units
MW-IA
NM-7
MW-2
NM-3R
MW-4R
MW-5R
MW-6R
NES-1S
NES-1D
NES-2S
NES-2D
Propionic Acid
28-Dec-06
1000
µg/I
ND
NI
NS
NS
ND
NS
NS
NS
ND
ND
NS
19-Dec-08
1000
41
ND
NM
NS
9900
ND
64200
NS
1300
ND
ND
ND
8-Jul-09
1000
µgA
ND
NM
NS
ND
ND
ND
NS
ND
ND
ND
ND
14-Dec-09
1000
41
ND
NM
NS
ND
ND
ND
NS
ND
ND
ND
ND
23-Jun-10
1000
µgA
ND
NM
NS
800 J
ND
ND
NS
ND
3800
ND
ND
14-Dec-10
1000
µ9/1
Dry
NM
NS
ND
ND
ND
NS
ND
NS
ND
NS
21-Jun-11
NR
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
6-Dec-11
NR
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
13-Jun-12
1000
µg/I
WL
ND
NS
NS
NS
NS
NS
NS
NS
NS
NS
11-Dec-12
NR
µg/1
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
29-Apr-13
NR
µg/I
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
6-Aug-13
5000
µg/1
WL
NS
NS
ND
ND
ND
NS
ND
NS
ND
NS
25-Feb-14
5000
µg/I
WL
NS
NS
ND
ND
ND
NS
ND
ND
ND
ND
13-Aug-14
5000
µg/1
WL
ND
NS
NS
NS
ND
NS
NS
NS
ND
NS
12-Mar-15
5000
µg/I
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
19-Aug-15
5000
µ9/1
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
18-Feb-16
5000
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
11-Aug-16
5000
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
15-Feb-17
5000
µgA
WL
ND
NS
NS
NS
ND
NS
NS
NS
ND
NS
24-Aug-17
5000
µgA
WL
ND
NS
NS
NS
ND
NS
NS
NS
ND
NS
7-Feb-18
NR
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
16-Aug-18
NR
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Butyric Acid
28-Dec-06
1000
µg/1
ND
NI
NS
NS
ND
ND
NS
ND
ND
ND
NS
19-Dec-08
1000
µg/I
ND
NM
NS
1500
ND
ND
NS
ND
ND
ND
ND
8-Jul-09
1000
µg/1
ND
NM
NS
ND
ND
ND
NS
ND
ND
ND
ND
14-Dec-09
1000
µg/I
ND
NM
NS
ND
ND
ND
NS
ND
ND
ND
ND
23-Jun-10
1000
"A
ND
NM
NS
ND
600 J
ND
NS
1000 J
ND
ND
ND
14-Dec-10
1000
µ9/1
Dry
NM
NS
ND
ND
ND
NS
ND
NS
ND
NS
21-Jun-ll
NR
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
6-Dec-11
NR
µg/I
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
13-Jun-12
1000
µgA
WL
ND
NS
NS
NS
NS
NS
NS
NS
NS
NS
11-Dec-12
NR
µg/I
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
29-Apr-13
NR
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
6-Aug-13
5000
µgA
WL
NS
NS
ND
ND
ND
NS
ND
NS
ND
NS
25-Feb-14
5000
µg/1
WL
NS
NS
ND
ND
ND
NS
ND
ND
ND
ND
13-Aug-14
5000
µgA
WL
ND
NS
NS
NS
ND
NS
NS
NS
ND
NS
12-Mar-15
5000
µg/l
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
19-Aug-15
5000
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
I8-Feb-16
5000
µg/1
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
11-Aug-16
5000
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
15-Feb-17
5000
µ9/1
WL
ND
NS
NS
NS
ND
NS
NS
NS
ND
NS
24-Aug-17
5000
µgA
WL
ND
NS
NS
NS
ND
NS
NS
NS
430 J
NS
7-Feb-18
NR
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
16-Aug-18
NR
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Total Volatile Fatty Acids
19-Dec-08
µg/I
ND
NM
NS
12600
ND
68500
NS
1300
1000
ND
ND
(sum of above 5 parameters)
8-Jul-09
µg/1
ND
NM
NS
700 J
ND
ND
NS
ND
ND
700 J
ND
14-Dec-09
µg/I
ND
NM
NS
ND
ND
ND
NS
ND
ND
ND
ND
23-Jun-l0
µgA
ND
NM
NS
800 J
600 J
ND
NS
1000 J
3800
1900 J
2800 J
14-Dec-10
µg/I
Dry
NM
NS
ND
600 J
2400
NS
ND
NS
ND
NS
21-Jun-l1
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
6-Dec-11
µg/I
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
13-Jun-12
µgA
WL
ND
NS
NS
NS
NS
NS
NS
NS
NS
NS
11-Dec-12
µg/I
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
29-Apr-13
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
6-Aug-13
µgA
WL
NS
NS
ND
ND
ND
NS
ND
NS
ND
NS
25-Feb-14
µg/l
WL
NS
NS
ND
ND
ND
NS
ND
ND
ND
ND
13-Aug-14
µg/I
WL
ND
NS
NS
NS
ND
NS
NS
NS
ND
NS
12-Mar-15
µg/l
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
19-Aug-15
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
I8-Feb-16
µg/l
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
11-Aug-16
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
15-Feb-17
µg/l
WL
ND
NS
NS
NS
710 J
NS
NS
NS
950 J
NS
24-Aug-17
µgA
WL
380 J
NS
NS
NS
9000 J
NS
NS
NS
4530 J
NS
7-Feb-18
µg/l
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
16-Aug-18
µgA
WL
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
BTEX
28-Dec-06
µg/I
ND
NI
ND
ND
ND
NS
ND
ND
ND
ND
NS
(sum of benzene, toluene
19-Dec-08
µgA
ND
NM
ND
ND
ND
0.40 J
ND
ND
ND
ND
ND
etlrylbenzene, & xylenes:
8-Jul-09
µgA
ND
NM
ND
ND
ND
0.54 J
ND
0.60 J
ND
ND
ND
14-Dec-09
µg/l
ND
NM
ND
ND
ND
0.37 J
ND
NS J
NS
NS
NS
23-Jun-10
µgA
ND
NM
ND
ND
ND
0.42 J
ND
ND
ND
ND
ND
14-Dec-10
µg/l
Dry
NM
ND
ND
ND
ND
ND
0.53 J
NS
ND
NS
21-Jun-11
µgA
WL
ND
ND
ND
ND
ND
ND
NS
NS
NS
NS
6-Dec-11
9g/1
WL
ND
ND
ND
ND
0.40 J
ND
NS
NS
NS
NS
13-Jun-12
µgA
WL
ND
ND
ND
ND
ND
ND
NS
NS
NS
NS
II-Dec-12
µg/l
WL
ND
ND
ND
ND
0.41 J
ND
NS
NS
NS
NS
29-Apr-13
µgA
WL
ND
ND
ND
ND
0.33 J
ND
NS
NS
NS
NS
6-Aug-13
µgA
WL
ND
ND
ND
ND
0.40 J
ND
NS
NS
NS
NS
25-Feb-14
µgA
WL
ND
ND
ND
ND
0.40 J
ND
NS
ND
ND
ND
13-Aug-14
9g/1
WL
ND
ND
ND
ND
0.41 J
ND
NS
NS
ND
NS
12-Mar-15
µg/I
WL
ND
ND
ND
ND
ND
ND
NS
NS
ND
ND
19-Aug-15
µg/1
WL
ND
ND
ND
ND
0.35 J
ND
NS
NS
ND
ND
18-Feb-16
µgA
WL
ND
ND
ND
ND
ND
ND
NS
NS
ND
ND
11-Aug-16
µgA
WL
ND
ND
ND
ND
ND
ND
NS
NS
ND
ND
15-Feb-17
µgA
WL
ND
ND
ND
ND
ND
ND
NS
NS
ND
ND
24-Aug-17
µgA
WL
ND
ND
ND
ND
ND
ND
NS
NS
ND
ND
7-Feb-18
µgA
WL
ND
ND
ND
ND
ND
ND
NS
NS
NS
NS
7-Feb-18
µgA
WL
ND
ND
ND
ND
0.35 J
ND
NS
NS
NS
NS
Granville Co. - Oxford Landfill, Unit 1
Permit 3901-CDLF-1997 Page 7 of 8 Joyce Engineering

Table C-06: Historical MNA Parameter Data
Anal to
Sample
Date
RL
Units
MW-IA
NM-7
MW-2
NM-3R
MW-4R
MW-5R
MW-6R
NES-IS
NES-ID
NES-2S
NES-2D
DCE
28-Dec-06
µg/I
ND
NI
ND
NS
ND
6
ND
0.84 J
NS
ND
NS
(sum of dichloroethylenes)
11-Ju1-07
µg/l
ND
NI
ND
NS
ND
6.2
ND
NS
NS
NS
NS
19-Dec-08
µg/I
ND
NM
ND
ND
ND
ND
ND
ND
ND
ND
ND
8-Jul-09
µg/1
ND
NM
ND
ND
ND
7.7
ND
4.1 J
0.30 J
ND
ND
14-Dec-09
µg/I
ND
NM
ND
ND
ND
7.4
ND
NS
NS
NS
NS
23-Jun-10
µgA
ND
NM
ND
ND
ND
13.6
ND
5.6
0.55 J
ND
ND
14-Dec-10
µg/I
Dry
NM
ND
ND
ND
ND
ND
5.9
NS
ND
NS
21-Jun-11
µgA
WL
ND
ND
ND
ND
6.4
ND
NS
NS
NS
NS
6-Dec-ll
µg/I
WL
ND
ND
ND
ND
3.0 J
ND
NS
NS
NS
NS
13-Jun-12
µgA
WL
ND
ND
ND
ND
4.3 J
ND
NS
NS
NS
NS
11-Dec-12
µg/I
WL
ND
ND
ND
ND
3.3 J
ND
NS
NS
NS
NS
29-Apr-13
µgA
WL
ND
ND
ND
ND
4.8 J
ND
NS
NS
NS
NS
6-Aug-13
µgA
WL
ND
ND
ND
ND
3.6 J
ND
NS
NS
NS
NS
25-Feb-14
µg/1
WL
ND
ND
ND
ND
3.7 J
ND
NS
ND
ND
ND
13-Aug-14
µgA
WL
ND
ND
ND
ND
2.8 J
0.39 J
NS
NS
ND
NS
12-Mar-15
µg/1
WL
ND
ND
ND
ND
2.6 J
ND
NS
NS
ND
ND
19-Aug-15
µgA
WL
ND
ND
ND
ND
3.1 J
0.89 J
NS
NS
NS
NS
I8-Feb-16
µg/1
WL
ND
ND
ND
ND
2.5 J
0.32 J
NS
NS
NS
NS
11-Aug-16
µgA
WL
ND
ND
ND
ND
2.7 J
0.5 J
NS
NS
NS
NS
15-176-17
µg/1
WL
ND
ND
ND
ND
ND
ND
NS
NS
ND
ND
24-Aug-17
µgA
WL
ND
ND
ND
ND
ND
0.99 J
NS
NS
ND
ND
7-Feb-18
µg/1
WL
ND
ND
ND
ND
0.79 J
0.68 J
NS
NS
NS
NS
16-Aug-18
µgA
WL
ND
ND
ND
I ND
1 1.25 J
0.62 J
NS
I NS
I NS
I NS
Notes: ND=Not detected above the laboratory detection limit
NS = Not sampled for this parameter during this event.
mg/L = milligrams per liter = parts per million.
pg/L = micrograms per liter = parts per billion.
my = millivolts NA- Data not avaliable
mS/cm = milliseimens/centimeter.
SU - standard units.
°C = degrees centigrade
Granville Co. - Oxford Landfill, Unit 1
Permit 3901-CDLF-1997 Page 8 of 8 Joyce Engineering