RA-7781_39876_CA_IAR_20160412

INITIAL ABATEMENT ACTION REPORT

APRIL 12, 2016

FRIENDLY MART
3055 Stantonsburg Road
Wilson, Wilson County, NC 27893
Facility ID #: 0-024589; UST Incident #: 39876
LATITUDE: N 35.69099167o; LONGITUDE: W 77.88775o (From GPS) UST OWNER:
Rose Oil Company, Inc., P.O. Box 706
Henderson, NC 27536; Phone Number: [phone]
PROPERTY OWNER & OCCUPANT:
Owner: SMW, Inc. – Occupant: Rose Oil Company, Inc., P.O. Box 706
Henderson, NC 27536; Phone Number: [phone]
CONSULTANT: Henry Nemargut Engineering Services, 2211 Chestnut Street, Wilmington, NC 28405 Phone Number: [phone]
LABORATORY: Pace Analytical Services, Inc., 9800 Kincey Ave, Suite 100, Huntersville, NC 28078 Phone Number: [phone]; State Certification #12
RELEASE INFORMATION: Date Discovered: 12/17/15 Estimated Quantity of Release: Unknown; Cause of Release: Corrosion Source of Release: UST; Size and Contents: (1) 4,000 Gallon Diesel UST The 20 Day Report for this site has been prepared by Henry Nemargut Engineering Services (sole proprietorship) under the direct supervision of a licensed engineer. I certify that the information contained in this report is correct and accurate to the best of my knowledge:
Henry Nemargut, P.E. North Carolina License #17669

April 12, 2016

Raymond Bartholomew
Rose Oil Company, Inc.
P.O. Box 706
Raleigh, NC 27536

Reference: Initial Abatement Action Report
Friendly Mart
3055 Stantonsburg Road
Wilson, Wilson County, North Carolina 27893
Facility ID#: 0-024589; Incident #39876

Dear Mr. Bartholomew:

In accordance with the requirements of March 1, 2007 Guidelines of the North Carolina Department of Environment and Natural Resources (NCDEQ), contained herein is a Initial Abatement Action Report for the release which occurred at the above referenced facility. These activities have been conducted following the release of petroleum which occurred in the vicinity of (1) underground storage tank (UST). All activities were conducted in accordance with NCDEQ guidelines and the requirements of 15A NCAC 2N.
Mr. Bartholomew, if you have questions regarding this report please contact my office..
Sincerely,

Henry Nemargut, P.E.
Henry Nemargut Engineering Services

TABLE OF CONTENTS

Page

1.0 SITE HISTORY AND CHARACTERIZATION 1

2.0 UST CLOSURE REPORT 1

3.0 INITIAL REPONSE AND ABATEMENT ACTIVITIES 4

4.0 SOURCE INVESTIGATION 5

5.0 GROUNDWATER INVESTIGATION 6

6.0 CONCLUSION AND RECOMMENDATIONS 7

LIST OF FIGURES

Figure 1: Project Location/U.S.G.S. Topographic Map
Figure 2: Site Layout and Former UST Locations
Figure 3: Site Layout, Soil Sample Locations and Soil TPH/VPH/EPH Map
Figure 4: Monitor Well Location Map

LIST OF TABLES
Table 1: Site History Table 2: Summary of TPH Soil Laboratory Analytical Results Table 3: Summary of Risk-Based Soil Laboratory Analytical Results Table 4: Summary of Groundwater Laboratory Analytical Results
APPENDICES

Appendix A: Form GW/UST-2
Appendix B: Form GW/UST-3 Appendix C: Geologic Log of Excavation Appendix D: Certificate of Soil Disposal Appendix E: Laboratory Analytical Results
Appendix F: Tank Disposal Manifest
Appendix G: Well Construction Record
Page - 1
Initial Abatement Action Report Friendly Mart 3055 Stantonsburg Road Wilson, North Carolina

1.0 - SITE HISTORY AND CHARACTERIZATION
Rose Oil Company, Inc. owns USTs which are operated at the Friendly Mart facility located at 3055 Stantonsburg Road in Wilson, North Carolina. Figure 1 illustrates the location of this facility on the Wilson Quadrangle U.S.G.S. Topo Map. This facility contains one permanent structure which is used as a gasoline convenience store. The site formerly contained (2) 6,000 gallon gasoline, (1) 4,000 gallon gasoline, & (1) 4,000 gallon diesel USTs. All of the gasoline USTs are still in use at this facility. The 4,000 gallon diesel UST, which was last used at this facility in November, 2015, was removed on December 17, 2015. Figure 2 illustrates the overall layout of this site and the UST locations. Table 1 summarizes the UST history for the Friendly Mart site. A release from the UST system was suspected on 12/17/15 based on elevated PID readings observed in soil samples collected from around the UST and the presence of a floating layer of diesel in the UST excavation. Groundwater was observed at a depth of approximately 4’ to 5’ below surface in the UST pit during soil abatement activities. The site and adjacent properties are used for commercial, residential and industrial purposes. Municipal water supplies are available to properties within 1,500’; however, adjacent properties are served by a local water supply well.
2.0 – UST CLOSURE REPORT
I. General Information

A. Ownership

Name: Rose Oil Company, Inc.
P.O. Box 706, Henderson, NC 27536
[phone]

B. Facility Information

Facility: Friendly Mart
3055 Stantonsburg Road, Wilson, NC 27893
Facility ID#: 0-024589

C. Contacts

1. Primary Contact: Rose Oil Company, Inc.
P.O. Box 706, Henderson, NC 27536
[phone]

Page - 2
2. Closure Contractor: Ready Contractors
3041 Stantonsburg Rd, Wilson, NC 27893
[phone]

3. Consultant: Henry Nemargut Engineering Services
2211 Chestnut Street, Wilmington, NC 28405
Contact: Henry Nemargut
[phone]

4. Laboratory: Pace Analytical Services, Inc.
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Lab. Cert.: NCDEM #12

D. UST Information

Tank Installation Size Tank Last Previous
No Date (Gal) Dimensions Contents Contents
4 8/19/81 4,000 64” x 24’ Diesel N/A

E. Site Characteristics

1. Past Releases: None reported.

2. Facility/UST Status: The UST removed from this facility was last in use in
November, 2015. The facility in still in operation for commercial petroleum sales.

3. Surrounding Property Use: Industrial/Residential/Commercial

4. Site Geology: Native soils consist of silt with varying amounts of clay and sand.
Bedrock was not encountered. Groundwater was observed in the remedial excavation at
a depth of approximately 4’ to 5’ below surface, and in remedial excavation monitoring
well MW-1 at a level of 4.57’ below top of casing. A geologic log is contained in
Appendix C.

Other pertinent site information is contained on the GW/UST-2 Site Investigation Form
which is included in Appendix A.

II. Closure Procedures

A. Notification and Tank Preparation

Page - 3
NCDEQ: Henry Nemargut Engineering Services notified the UST Section of the
NCDEQ Raleigh Regional Office of the intent to permanently close by submitting a
Notice of Intent: A copy of UST-3 is included in Appendix B.

B. Residuals

Petroleum liquids were removed from the UST by Rose Oil Company, Inc. and
transferred to other vessels owned by Rose Oil Company, Inc. Liquids disposal
manifests have not been made available to Henry Nemargut Engineering Services.

C. Excavation

The UST closure project at the Friendly Mart facility was conducted on December 17,
2015. Ready Contractors excavated the product and vent pipes, drained and vacuumed
them to avoid release of product into the surrounding soils, then removed the lines from
the tank. The UST was then exhumed from the ground on December 17, 2015. Figure 2
illustrates the layout of the project site and the locations of the tanks removed during this
closure project.

Henry Nemargut Engineering’s staff inspected the tank for structural integrity upon
removal. Documentation concerning the conditions the tanks is contained in Section 3.0
of this report.

Following removal of the UST, the excavation was visually inspected for the presence of
free product and groundwater. Water was observed in the tank pit at a depth of
approximately 4’ to 5’ below surface. Free product was evident on the pit groundwater
during the removal project. Petroleum odors were noted around the UST and in
overburden soils. The dimensions of the excavation created by the removal of the UST
were approximately 36' long by 17' wide by 13’-14’ deep.

D. Contaminated Soil

Contaminated soils were noted during abatement activities conducted in December, 2015.
Approximately 409.86 tons of contaminated soil generated during UST closure
operations and remedial excavation activities were transported and disposed of at
Soilworks, Inc. in Selma, NC. Composite samples obtained from these soils indicated
TPH-GRO/DRO contaminant levels in excess of NCDEQ Action Levels Appendix D
contains a soil disposal certificate for the soils disposed of from this site during Initial
Abatement Action activities.

III. Site Investigation

Site investigation activities are described in Section 3.0 through Section 5.0 of this
report.
Page - 4
3.0 - INITIAL RESPONSE AND ABATEMENT ACTIVITIES
Initial abatement activities were conducted at the Friendly Mart on December 17-21, 2015 by removal and disposal of approximately 409.86 tons of contaminated soil removed from the remedial excavation. Ready Contractors excavated the fill, product and vent pipes, cut and drained them to avoid release of product into the surrounding soils, then removed them from the tank. The UST was then exhumed from the ground. The tank was inspected for structural integrity upon removal. The UST was in poor condition, with at least 2 holes noted in its shell. After removal, the UST was transported to Foss Recycling in Wilson, NC for recycling. A scrap metal receipt for the UST removed during abatement is contained in Appendix F. Appendix C contains a soil disposal certificate for the soils disposed of from this site during Initial Abatement Action activities. Figure 4 illustrates the approximate limits of excavation for soils removed from the project site. Following removal of the UST, the excavation was visually inspected for the presence of odors, free product and groundwater. Water was observed in the tank pit at the time of removal. Free product was evident floating on the pit groundwater during the removal project. Petroleum odors were noted around the UST. Based on the observed free product and elevated PID readings noted around the USTs, a decision was made to excavate, transport and dispose of off-site suspected contaminated soils encountered during UST closure. Following removal of the UST, additional excavation was conducted at the site on December 17, 2015 in areas of the site that exhibited elevated PID readings and free product. Excavation was ceased after all suspected contaminated soils were removed from the UST area. Appendix D contains soil disposal manifests for the soils disposed of from this site during Initial Abatement Action activities. 4.0 - SOURCE INVESTIGATION
On December 17, 2015, following the excavation of the UST and soils in the tank area, soil samples were collected in accordance with NCDEQ guidelines. Soil samples were obtained from the excavation walls since the UST pit contained water. The soil samples were collected from a depth of approximately 3’-4’ from the perimeter of the UST excavation based on the observed depth to water in the UST pit. Soil Samples were analyzed via TPH-GRO/DRO and/or EPA 8260/8270/MADEP EPH/VPH in areas were over-excavation was conducted. (2) Stockpile soil samples were obtained from stockpiled soils for TPH analyses from soils excavated during UST closure and remedial operations. TPH laboratory analytical results are summarized in Table 2. Risk-based results are tabulated in Table 3, with TPH/VPH/EPH results depicted on Figure 3. A geologic log of excavation for these activities is contained as Appendix C. The soil samples collected at 3055 Stantonsburg Road were labeled with sample location, depth, and date collected. All soil samples were submitted to Pace Analytical, Inc for analyses. The soil samples were obtained as specified in the collection, preservation, and handling section of the specific method. Each container was labeled with sample location, analyses to be performed, time, date, and the sampler's name. They were then placed in a cooler and chilled with ice to approximately 4oC in preparation for transportation to the analytical laboratory utilizing EPA approved chain of custody procedures.
Page - 5
Results from the release confirmation soil samples were above current NCDEQ action levels for TPH-DRO/GRO compounds for stockpile soil samples. Laboratory TPH analytical results confirm that contamination was present in the soils disposed of from the project site, with TPH-DRO compounds noted at levels of 179 mg/kg to 1,480 mg/kg and TPH-GRO levels noted at levels of 14.6 mg/kg to 86.5 mg/kg in composite stockpile soil samples X-1 & X-2 collected during abatement activities.
Soil samples were collected from the perimeter of the UST excavation where over-excavation was conducted to obtain risk-based analytical data for the site. Results from the risk-based and TPH soil samples were below NCDEQ lowest MSCCs or Action Levels for all 8260/8270/VPH/EPH/TPH compounds for pit wall samples. Appendix F contains copies of the laboratory analytical reports and the chain of custody records for the soil samples collected at the project site. 5.0 – GROUNDWATER INVESTIGATION

5.1 Monitoring Well Installation

A total of one North Carolina Type II groundwater monitoring well was installed on-site
during initial abatement action activities per discussions with Brenda Hafshejani of the
UST section. Figure 4 illustrates the location of this monitoring well, denoted as MW-1.
MW-1 was placed in the diesel UST pit which was excavated to below the water table
during remedial excavation activities. The monitoring well was constructed of 2-inch
Schedule 40 PVC pipe with 3.75’ of casing and 10 feet of 0.010 inch slotted screen.
Based on the assumption that the contaminants being addressed were primarily
hydrocarbon constituents with specific gravities of less than 1.0, the Type II monitoring
well was installed so that the screened interval intersected the shallow groundwater table
at the time of installation.

5.2 Monitor Well Sampling and Analyses

On June 5, 2015, monitor well MW-1 was sampled for analyses utilizing EPA Methods
6200B plus MTBE, IPE, & EDB, 625 + 10 peaks, Pb, and MADEP Methods for
VPH/EPH as appropriate based on UST contents. Before sampling, the monitor well was
purged with a submersible pump by removing 3 well volumes to ensure that the samples
were representative of the actual groundwater conditions. The monitor wells were then
sampled using the submersible pump at a reduced pumping rate. Groundwater was
detected in monitor well MW-1 at a depth of approximately 4.57’ below top of casing
prior to purging and sampling.

All samples were placed in laboratory supplied glassware, labeled with sample location,
analysis to be performed, time, date and sampler's name. The sample jars were then
immediately placed in a cooler, chilled with ice to approximately 4oC in preparation of
transportation to an analytical laboratory utilizing EPA approved chain-of-custody
procedures.
Page - 6

Laboratory analytical results from MW-1 indicate the presence of 4
compounds/compound groups above 15 NCAC 2L Standards. Benzene was noted at a
concentration of 37.9 ug/l in MW-1, above its 2L Standard of 1 ug/l. Naphthalene was
noted at a concentration of 21.8 ug/l in MW-1, above its 2L Standard of 6 ug/l. No
compounds were detected in MW-1 at levels above GCLs. Table 4 summarizes the
laboratory analytical results for the groundwater samples. Appendix D contains a copy
of the laboratory analytical report and chain of custody record for the groundwater
samples.

6.0 - CONCLUSIONS AND RECOMMENDATIONS
6.1 General Summary
The activities conducted for this Initial Abatement Action Report at the Friendly Mart have been completed. From a review of all information gathered during this project, Henry Nemargut Engineering Services makes the following conclusions:

o (1) 4,000 gallon diesel UST was removed from 3055 Stantonsburg Road on December 17, 2015.

o A release was confirmed from the UST in the form of contaminated soil and free product floating on UST pit water. Corrosion holes were noted in the shell of the UST.

o Approximately 409.86 tons of contaminated soil generated during UST closure operations and remedial excavation activities were transported and disposed of at Soilworks, Inc. in Selma, NC. Composite samples obtained from these soils indicated TPH-DRO compounds noted at levels of 179 mg/kg to 1,480 mg/kg and TPH-GRO levels noted at levels of 14.6 mg/kg to 86.5 mg/kg.

o Laboratory analytical results for the risk-based and TPH soil samples obtained on December 17, 2015 following completion of remedial excavation indicate that soil contamination in the vicinity of the diesel UST has been remediated to below NCDEQ lowest Maximum Soil Contaminant Concentrations (MSCCs) for all 8260/8270/VPH/EPH/TPH compounds.

o One groundwater monitoring well, MW-1, was installed in the UST remedial excavation since groundwater was encountered during remediation in this pit. MW-1 was placed in the portion of this excavated pit which exhibited free product. Groundwater was observed at a depth of approximately 4.57’ below top of casing in this well. Free product was not observed this monitoring well during sampling on January 28, 2016.

o Laboratory analytical results from MW-1 indicate the presence of 4 compounds/compound groups above 15 NCAC 2L Standards. Benzene was noted at a concentration of 37.9 ug/l in MW-1, above its 2L Standard of 1 ug/l. Naphthalene was noted at a concentration of 21.8 ug/l in MW-1, above its 2L Standard of 6 ug/l. No compounds were detected in MW-1 at levels above GCLs.
Page - 7
6.2 Recommendations
Based upon a review of all information gathered during this project, Henry Nemargut Engineering Services makes the following recommendations:

o A copy of this report has been forwarded to the following address:
Mr. John Maloy NCDEQ – UST Section 3800 Barrett Drive Raleigh, NC 27609 6.3 Limitations
This report has been prepared for the exclusive use of the Rose Oil Company, Inc. for the specific application to the referenced site located in Wilson County, North Carolina. The evaluation was conducted based on the scope of work and level of effort desired by the client and with resources adequate only for the scope of work. Our findings have been developed in accordance with generally accepted standards for Initial Abatement Action Reports in the State of North Carolina, available information and our professional judgment. No other warranty is expressed or implied. The data presented in this report are indicative of conditions at the precise locations sampled and the time the sample was collected. Additionally, the data obtained from the samples would be interpreted as meaningful with respect to the parameters in the laboratory reports. No additional information can be logically inferred from this data.

FIGURES

TABLES
TABLE 1: SITE HISTORY
Plainview Grocery
3055 Stantonsburg Road, Wilson, NC 27565

Property Ownership:

S.M.W., Inc.
P.O. Box 706
Henderson, NC 27536-0706
9/4/1985 to present

Previous Property Owners:

Lawrence & Annie Jones
1/31/1974 to 9/4/1985

UST Information:

Tank Inst. Size Closure UST Tank
No Date (Gal) Date Status Contents
1 8/19/81 6,000 N/A In-use Gasoline
2 8/19/81 6,000 N/A In-use Gasoline
3 8/19/81 4,000 1/6/99 Closed Gasoline
3A 7/14/99 4,000 N/A In-use Gasoline
4 1/1/64 4,000 12/17/15 Closed Diesel

Tank owner:

Rose Oil Company, Inc.
P.O. Box 706
Henderson, NC 27536-0706
9/4/1985 to present
Sample Sample Sample Sample TPH GRO TPH DRO Field PID
ID Location Depth Date Result (ppm) Result (ppm) Result (ppm)
E East Pit Wall 3' 12/17/2015 N/A N/A BDL
N1 North Pit Wall 3' 12/17/2015 BDL BDL 3
N2 North Pit Wall 3' 12/17/2015 BDL BDL 2
N3 North Pit Wall 3' 12/17/2015 BDL BDL 3
W West Pit Wall 3' 12/17/2015 N/A N/A BDL
X-1 Soil Stockpile n/a 12/17/2015 86.5 179 320
X-2 Soil Stockpile n/a 12/17/2015 14.6 1,480 160
NR = Analyses not requested N/A = not analyzed <10 = below NCDENR action level
TABLE 2: SUMMARY OF TPH SOIL ANALYTICAL AND FIELD SCREENING RESULTS
Friendly Mart, 3055 Stantonsburg Road, Wilson, NC
Sample Location E W Lowest MSCC Ind/Comm MSCC Residential MSCCDate12/17/2015 12/17/2015 (note units) (note units) (note units)Sample depth3' 3' Method 8260 (ug/kg)Benzene BDL BDL 5.6 164,000.0 18,000Methylene Chloride BDL 18.6 20 763,000 85,000n-Butylbenzene BDL BDL 4,300 16,350,000 626,000sec-Butylbenzene BDL BDL 3,300 16,350,000 626,000Ethylbenzene BDL BDL 4,900 40,000,000 1,560,000Isopropylbenzene BDL BDL 2,000 40,880,000 1,564,000p-Isopropyltoluene BDL BDL NSE NSE NSENaphthalene BDL BDL 160 8176000 313,000Acetone BDL BDL 24,000 360,000,000 14,000,000n-Propylbenzene BDL BDL 2,000 16,350,000 626,000Toluene BDL BDL 4,300 32,000,000 1,200,0001,2,4-Trimethylbenzene BDL BDL 8,500 20,440,000 782,0001,3,5-Trimethylbenzene BDL BDL 8,300 20,440,000 782,000MTBE BDL BDL 91 3,100,000 350,000sec-butylbenzene BDL BDL 3,400 16,350,000 626,000Xylenes (total) BDL BDL 4,600 81,760,000 3,129,000Method 8270 (ug/kg)FluoreneBDLBDL47,00016,400,000620,000Fluoranthene BDL BDL 290,000 16,400,000 620,000Phenanthrene BDL BDL 56,000 12,264,000 469,0001-Methylnaphthalene BDL BDL 4 100,000 20,0002-Methylnaphthalene BDL BDL 3,600 1,635,000 63,000Naphthalene BDL BDL 160 8176000 313,000Aliphatic Fraction Classes (mg/kg) C5 - C8 Volatile Aliphatics BDL BDL 68 24,528 939C9 - C12 Volatile Aliphatics BDL BDL NSE NSE NSEC9-C18 Extractable Aliphatics BDL BDL NSE NSE NSEC9-C18 Aliphatics (total) BDL BDL 540 40,000 1,500C19-C36 Extractable AliphaticsBDLBDLNSE810,00031,000Aromatic Fraction Classes (mg/kg) C9 - C10 Volatile AromaticsBDLBDLNSENSENSEC11 - C22 Extractable Aromatics BDL BDL NSE NSE NSEC9 - C22 Aromatics (total)BDLBDL3112264469BDL = below detection limits NR = analyses not requestedNSE = no standard establishedTABLE 3Laboratory Analytical Results - Risk Based Soil SamplesFriendly Mart, 3055 Stantonsburg Road, Wilson, NC
TABLE 4
SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
Friendly Mart
3055 Stantonsburg Rd, Wilson, NC 27893
Constituent MW-1 GCL 2L Standard

Date 1/28/2016
Standard Method 6200B (ug/L)
Benzene 37.9 5,000 1
Toluene 4.1 260,000 600
Ethylbenzene 64.5 84,500 600
Xylenes (total) 38.6 85,500 500
BTEX (total) 145.1 NSE NSE
p-Isopropyltoluene BDL NSE NSE
Isopropylbenzene 124 25,000 70
Diisopropyl Ether (DIPE) BDL 70,000 70
Naphthalene 21.8 6,000 6
n-propylbenzene BDL 30,000 70
n-butylbenzene BDL 6,900 70
sec-butylbenzene BDL 8,500 70
Methyl-tert-butyl-ether (MTBE) 6.4 20,000 20
1,2,4-Trimethylbenzene BDL 28,500 400
1,3,5-Trimethylbenzene BDL 25,000 400
Methyl Ethyl Ketone (MEK) BDL 4,000,000 4000
Methyl Isobutyl Ketone (MIBK) BDL NSE NSE
Styrene BDL 70,000 70
Acetone BDL 6,000,000 6000
Lead (EPA 6010) BDL 15,000 15
Method 625 (ug/L)
Acenaphthene BDL 2,120 80
Naphthalene 8 6,000 6
1-Methylnaphthalene BDL 1,000 1
2-Methylnaphthalene BDL 125,000 30
TOTAL TICs 292.1 NSE NSE
MADEP Aliphatic Fraction Classes (ug/L)
C5-C8 Volatile Aliphatics 330 NSE 400
C9-C12 Volatile Aliphatics 584 NSE NSE
C9-C18 Extractable Aliphatics 106 NSE 700
C9-C18 Aliphatics (total) 690 NSE 700
C19-C36 Extractable Aliphatics BDL NSE 10,000
MADEP Aromatic Fraction Classes (ug/L)
C9-C10 Volatile Aromatics 508 NSE NSE
C11-C22 Extractable Aromatics BDL NSE NSE
C9-C22 Aromatics (total)508 NSE 200
N/A = Not Analyzed
BDL = Below Detection Limits
NSE = No Standard Established

APPENDIX A

FORM GW/UST-2
,
UST-2 Site Investigation Report for Permanent Closure or Change-in-Service of UST
STATE USE ONLY: Return completed form to:
The DWM Regional Office located in the area where the facility is located. Send a copy to the Central Office in Raleigh so that 1.0. #
the status of the tank may be changed to "PERMANENTLY CLOSED" and your tank fee account can be closed out.
Dale Received SEE MAP ON THE BACK OF THIS FORM FOR THE CENTRAL AND REGIONAL OFFICE ADDRESSES
INSTRUCTIONS (READ THIS FIRST)
For more than five UST systems you may attach additional forms as needed.

Permanent closure -For permanent closure, complete all sections of this form.

Change-in-service -For change-in-service where UST systems will be converted from containing a regulated substance to storing a non-regulated

substance, complete sections I, II, III, IV, and VIII

Effective February 1, 1995, all UST closure/change-in-service reports must be submitted in the format provided in the UST-12 form. UST closure and

change-in-services must be completed in accordance with the latest version of the Guidelines for Tank Closure. A copy of the UST-12 form and the

Guidelines for Tank Closure can be obtained at www.wastenotnc.org.

You must make sure that USTs removed from your property are disposed of properly. When choosing a closure contractor, ask where the tank(s) will be

taken for disposal. Usually, USTs are cleaned and cut up for scrap metal. This is dangerous work and must be performed by a qualified company. Tanks

disposed of illegally in fields or other dumpsites can leak petroleum products and sludge into the environment. If your tanks are disposed of improperly, you

could be held responsible for the cleanup of any environmental damage that occurs.

NOTE: If a release from the tank(s) has occurred, the site assessment portion of the tank closure must be conducted under the supervision of a P.E. or

L.G., with all closure site assessment reports bearing the signature and seal of the P.E. or L.G.

I. OWNERSHIP OF TANKS II. LOCATION OF TANKS
Owner Name (Corporation, Individual, Public Agency, or Other Entity) Facility Name or Company
ROSE OIL COMPANY INC FRIENDLY MART
Street Address Facility 10 # (If known)
PO BOX 706 0-024589
City County Street Address
HENDERSON VANCE 3055 STANTONSBURG ROAD
State Zip Code City County Zip Code
NC 27536 WILSON WILSON 27893
Phone Number Phone Number
[phone]
til. CONTACT PERSONNEL
Contact for Facility:
RAYMOND BARTHOLOMEW
Closure Contractor Name:
GARRY JONES
Primary Consultant Name:
HENRY NEMARGUT
Phone. No:Job Title:
[phone]DIRECTOR OF OPERATIONS
Closure Contractor Company: Phone. No:Address:
[phone]READY CONTRACTORS 3041 STANTONSBURG ROAD, WILSON
Phone. No:Primary Consultant Company: Address:
HENRY NEMARGUT ENGINEERING 2211 CHESTNUT ST, WILMINGTON 28405 [phone]
IV. UST INFORMATION FOR REGISTERED UST SYSTEMS
Tank
10 No.
4
Size in
Gallons
4000
Tank
Dimensions
5'4" X 24'
-
Last
Contents
Last Use
Date
Permanent
Close Date
Change-in-
Service
Date
Dielsel, Dieisl 11/2015 12/17/2015
VI. UST IN'FORMATION FOR UNREGISTERED UST SYSTEMS
Tank Size in Tank Last Last Use Permanent Tank Owner
10 No. Gallons Dimensions Contents Name *Date Close Date
V. EXCAVATION CONDITION
Water in
excavation
Yes No
~
D
D
D
D
D
D
D
D
D
Free
product
Yes No
Notable odor or visible
soil contamination
Yes No
~
D
D
D
0
D
~
D
D
D
D
D
D
D
D
D
D
D I
D
D
VII. EXCAVATION CONDITION
Water in
excavation
Yes No
D D
D D
D D
D D
D D
Notable odor or visible Free
product soil contamination
Yes No Yes No
DD D D
D D D D
D D D D
DD D D
D D DD
* If the tank owner address is different from the one listed in Section I., then enter the street address, city, state, zip code and telephone no. below
VIII. CERTIFICATION
I certify under penalty of law that I have personally examined and am familiar with the information submitted in this and all attached documents and that
based on my inquiry of those individuals immediately responsible for obtaining the information, I believe that the submitted information is true accurate and
complete.
Print name and official title of owner or owner's authorized representative I Date Signed Si9)7. -1/4/2016HENRY NEMARGUT/CO SULTING ENGINEER
) ......~ ~~
UST-2 Rev 11/2006 /' /

APPENDIX B

FORM GW/UST-3
UST-3 Notice of Intent: UST Permanent Closure.or Change-in-Service
Return completed form to: STATE USE ONLY
The DWM Regional Office located in the area where the facility is located. Send a copy to the Central Office in Raleigh so that LD. # the status of the tank may be changed to "PERMANENTLY CLOSED" and your tank fee account can be closed out.
SEE MAP ON THE BACK OF THIS FORM FOR THE CENTRAL AND REGIONAL OFFICE ADDRESSES. Date Received
INSTRUCTIONS (READ THIS FIRST)
Complete and return at least thirty (30) days prior to closure or change-in-service activities. If a Professional Engineer (P.E.) or a Licensed Geologist (L.G.)
provides supervision for closure or change-in-service site assessment activities and signs and seals all closure reports then at least a five (5) working
days notice is acceptable.
Completed UST closure or change-In-service site assessment reports, along with a copy of the UST-2 form, should be submitted to the appropriate Division
of Waste Management (DWM) Regional Office within thirty (30) days following closure activities. The UST-2 form should also be submitted to the Central
Office in Raleigh so that the status of the tanks may be changed to permanently closed and your tank fee account can be closed out.
UST closure and change-in-service site assessments must be completed in accordance with the latest version of the Guidelines for Tank Closure. The
Guidelines for Tank Closure can be obtained at www.wastenotnc.org.
You must make sure that USTs removed from your property are disposed of properly. When choosing a closure contractor, ask where the tank(s) will be
taken for disposal. Usually, USTs are cleaned and cut up for scrap metal. This is dangerous work and must be performed by a qualified company. Tanks
disposed of illegally in fields or other dumpsites can leak petroleum products and sludge into the environment. If your tanks are disposed of improperly, you
could be held responsible for the cleanup of any environmental damage that occurs.
I. OWNERSHIP OF TANKS II. LOCATION
Owner Name (Corporation, Individual, Public Agency, or Other Entity) Facility Name or Company
ROSE OIL COMPANY INC FRIENDLY MART
Street Address Facility ID # (If known)
PO BOX 706 0-024589
City County Street Address
HENDERSON VANCE 3055 STANTONBURG ROAD
State Zip Code City County Zip Code
NC 27536 WILSON WILSON 27893
Phone Number Phone Number
[phone] NIA
I III. CONTACT PERSONNEL
Name: I Company Name: I Job Title: Phone Number:
RAYMOND BARTHOLOMEW ROSE OIL COMPANY INC DIRECTOR OF OPERATIONS 438-7141
IV. TANK REMOVAL, CLOSURE IN PLACE, CHANGE-IN SERViCe'
1. Contact local fire marshal. 5. Provide a sketch locating piping, tanks and a P.E. or L.G, with all closure site
2 Plan entire closure event. soil samplipg locations. assessment reports bearing the signature
6. Submit a closure report in the format of and seal of the P.E. or L.G. If a release has
3. Conduct Site Soil Assessment. UST-12 (including the form UST-2) within not occurred, the supervision, signature or
4. If removing tanks or closing in place, refer to thirty (30) days following the site seal of a P.E. or L.G. is not required.
API Publication 2015 Cleaning Petroleum investigation. 8. Keep closure records for three (3) years.
Storage Tanks and 1604 Removal and 7. If a release from the tanks has occurred, the Disposal of Used Underground Petroleum
Storage Tanks. site assessment portion of the tank closure
must be conducted under the supervision of
V. WORK TO BE PERFORMED BY
Contractor Name: Contractor Company Name:
GARRY JONES READY CONTRACTORS
Address: State: I Zip Code: Phone No:
3041 STANTONSBURG ROAD, WILSON NC 27893 [phone]
Primary Consultant Name: I Primary Consultant Company Name: Consultant Phone No:
HENRY NEMARGUT HENRY NEMARGUT ENGINEERING SERVICES [phone]
VI. TANKS SCHEDULED FOR CLOSURE OR CHANGE-IN-SERVICE
Proposed Activity
Closure ChanQe-ln-Service
Tank ID No. Size in Gallons Last Contents Removal Abandonment in Place' New Contents Stored
4 4000 Dielsel, Dielsel Mix ~ 0
0 0
D D
D D
D D
• Prior written approval to abandon a tank in place must be received from a DWM Reqional Office.
VII. OWNER OR OWNER'S AUTHORIZED REPRESENTATIVE
I understand that I can be held responsible for environmental damage resulting from the improper disposal of my USTs.
Print name and official HENRY NEMARGUT/CONSULTING ENGINEER
title:
~ru· t{l;~i;d~ SCHEDULED REMOVAL DATE Notify your DWM Regional Office
12/16/2015 48 hours before this date if
1 scheduled removal date changes
(UST-3 ~ev 1012006 (

APPENDIX C

GEOLOGIC LOG OF EXCAVATION
GEOLOGIC LOG OF EXCAVATION
Henry Nemargut Engineering Services
Job Name: Friendly Mart
Address: 3055 Old Stantonsburg Rd, Wilson, NC
Job No.:
Start Date: 12/17/2016
Contractor: Ready Contractors
Sample ID: UST Closure Samples
Comments:

Sample Depth OVA
Number (FT.)Soil Decription (color, soil type, moisture) (ppm)
E 3' tan-gray, Clay w/silt and little sand BDL
N1 3' gray-red, Silt w/clay 3
N2 3' gray-red, Silt w/clay 2
N3 3' gray-orange-brown, Silt w/clay 3
W 3' orange-brown-red, Silt w/clay and trace sand BDL

APPENDIX D

CERTIFICATE OF SOIL DISPOSAL

APPENDIX E

LABORATORY ANALYTICAL RESULTS
#=CL#
December 28, 2015
LIMS USE: FR - HENRY NEMARGUT
LIMS OBJECT ID: 92280538
92280538
Project:
Pace Project No.:
RE:
Henry Nemargut
Henry Nemargut Engineering
2211 Chestnut Street
Wilmington, NC 28405
FRIENDLY MRT 3055 STANTONSBURG
Dear Henry Nemargut:
Enclosed are the analytical results for sample(s) received by the laboratory on December 17, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 43
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
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[phone]
Page 2 of 43
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Lab ID Sample ID Matrix Date Collected Date Received
92280538001 X-1 Solid 12/17/15 10:20 12/17/15 17:26
92280538002 X-2 Solid 12/17/15 14:40 12/17/15 17:26
92280538003 E Solid 12/17/15 15:00 12/17/15 17:26
92280538004 N1 Solid 12/17/15 15:10 12/17/15 17:26
92280538005 N2 Solid 12/17/15 15:15 12/17/15 17:26
92280538006 N3 Solid 12/17/15 15:20 12/17/15 17:26
92280538007 W Solid 12/17/15 15:40 12/17/15 17:26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 43
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92280538001 X-1 EPA 8015 Modified 2 PASI-CBJL
EPA 8015 Modified 2 PASI-CZDO
ASTM D2974-87 1 PASI-CKDF
92280538002 X-2 EPA 8015 Modified 2 PASI-CSWB
EPA 8015 Modified 2 PASI-CZDO
ASTM D2974-87 1 PASI-CKDF
92280538003 E MADEP EPH 7 PASI-CBJL
MADEP VPH 5 PASI-CZDO
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92280538004 N1 EPA 8015 Modified 2 PASI-CBJL
EPA 8015 Modified 2 PASI-CZDO
ASTM D2974-87 1 PASI-CKDF
92280538005 N2 EPA 8015 Modified 2 PASI-CBJL
EPA 8015 Modified 2 PASI-CZDO
ASTM D2974-87 1 PASI-CKDF
92280538006 N3 EPA 8015 Modified 2 PASI-CBJL
EPA 8015 Modified 2 PASI-CZDO
ASTM D2974-87 1 PASI-CKDF
92280538007 W MADEP EPH 7 PASI-CBJL
MADEP VPH 5 PASI-CZDO
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 43
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92280538001 X-1
Diesel Range Organics(C10-C28) 179 mg/kg 12/22/15 00:185.5EPA 8015 Modified
Gas Range Organics (C6-C10) 86.5 mg/kg 12/23/15 06:115.2EPA 8015 Modified
Percent Moisture 9.5 % 12/21/15 06:550.10ASTM D2974-87
92280538002 X-2
Diesel Range Organics(C10-C28) 1480 mg/kg 12/24/15 11:4028.7EPA 8015 Modified
Gas Range Organics (C6-C10) 14.6 mg/kg 12/23/15 15:225.9EPA 8015 Modified
Percent Moisture 13.0 % 12/21/15 06:560.10ASTM D2974-87
92280538003 E
Percent Moisture 14.5 % 12/21/15 06:560.10ASTM D2974-87
92280538004 N1
Percent Moisture 18.5 % 12/21/15 06:560.10ASTM D2974-87
92280538005 N2
Percent Moisture 16.9 % 12/21/15 06:560.10ASTM D2974-87
92280538006 N3
Percent Moisture 15.2 % 12/21/15 06:560.10ASTM D2974-87
92280538007 W
Methylene Chloride 18.6 ug/kg 12/22/15 16:32 C918.2EPA 8260
Percent Moisture 18.7 % 12/21/15 06:560.10ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Sample: X-1 Lab ID: 92280538001 Collected: 12/17/15 10:20 Received: 12/17/15 17:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-C28)179 mg/kg 12/22/15 00:1812/20/15 11:005.5 1
Surrogates
n-Pentacosane (S) 80 % 12/22/15 00:18 629-99-212/20/15 11:0041-119 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)86.5 mg/kg 12/23/15 06:1112/21/15 09:585.2 1
Surrogates
4-Bromofluorobenzene (S) 101 % 12/23/15 06:11 460-00-412/21/15 09:5870-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 9.5 % 12/21/15 06:550.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/28/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Sample: X-2 Lab ID: 92280538002 Collected: 12/17/15 14:40 Received: 12/17/15 17:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-C28)1480 mg/kg 12/24/15 11:4012/23/15 06:5028.7 5
Surrogates
n-Pentacosane (S) 0 % 12/24/15 11:40 629-99-2 S012/23/15 06:5041-119 5
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)14.6 mg/kg 12/23/15 15:2212/23/15 10:345.9 1
Surrogates
4-Bromofluorobenzene (S) 95 % 12/23/15 15:22 460-00-412/23/15 10:3470-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 13.0 % 12/21/15 06:560.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/28/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Sample: E Lab ID: 92280538003 Collected: 12/17/15 15:00 Received: 12/17/15 17:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18) ND mg/kg 12/23/15 20:38 N212/21/15 14:3011.7 1
Aliphatic (C19-C36) ND mg/kg 12/23/15 20:38 N212/21/15 14:3011.7 1
Aromatic (C11-C22) ND mg/kg 12/23/15 20:38 N212/21/15 14:3011.7 1
Surrogates
Nonatriacontane (S) 84 % 12/23/15 20:38 7194-86-712/21/15 14:3040-140 1
o-Terphenyl (S) 83 % 12/23/15 20:38 84-15-112/21/15 14:3040-140 1
2-Fluorobiphenyl (S) 92 % 12/23/15 20:38 321-60-812/21/15 14:3040-140 1
2-Bromonaphthalene (S) 82 % 12/23/15 20:38 580-13-212/21/15 14:3040-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08) ND mg/kg 12/21/15 20:28 N212/21/15 09:442.4 1
Aliphatic (C09-C12) ND mg/kg 12/21/15 20:28 N212/21/15 09:442.4 1
Aromatic (C09-C10) ND mg/kg 12/21/15 20:28 N212/21/15 09:442.4 1
Surrogates
4-Bromofluorobenzene (FID) (S) 92 % 12/21/15 20:28 460-00-412/21/15 09:4470-130 1
4-Bromofluorobenzene (PID) (S) 93 % 12/21/15 20:28 460-00-412/21/15 09:4470-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 12/19/15 22:50 83-32-912/19/15 11:04386 1
Acenaphthylene ND ug/kg 12/19/15 22:50 208-96-812/19/15 11:04386 1
Aniline ND ug/kg 12/19/15 22:50 62-53-312/19/15 11:04386 1
Anthracene ND ug/kg 12/19/15 22:50 120-12-712/19/15 11:04386 1
Benzo(a)anthracene ND ug/kg 12/19/15 22:50 56-55-312/19/15 11:04386 1
Benzo(a)pyrene ND ug/kg 12/19/15 22:50 50-32-812/19/15 11:04386 1
Benzo(b)fluoranthene ND ug/kg 12/19/15 22:50 205-99-212/19/15 11:04386 1
Benzo(g,h,i)perylene ND ug/kg 12/19/15 22:50 191-24-212/19/15 11:04386 1
Benzo(k)fluoranthene ND ug/kg 12/19/15 22:50 207-08-912/19/15 11:04386 1
Benzoic Acid ND ug/kg 12/19/15 22:50 65-85-012/19/15 11:041930 1
Benzyl alcohol ND ug/kg 12/19/15 22:50 100-51-612/19/15 11:04772 1
4-Bromophenylphenyl ether ND ug/kg 12/19/15 22:50 101-55-312/19/15 11:04386 1
Butylbenzylphthalate ND ug/kg 12/19/15 22:50 85-68-712/19/15 11:04386 1
4-Chloro-3-methylphenol ND ug/kg 12/19/15 22:50 59-50-712/19/15 11:04772 1
4-Chloroaniline ND ug/kg 12/19/15 22:50 106-47-812/19/15 11:041930 1
bis(2-Chloroethoxy)methane ND ug/kg 12/19/15 22:50 111-91-112/19/15 11:04386 1
bis(2-Chloroethyl) ether ND ug/kg 12/19/15 22:50 111-44-412/19/15 11:04386 1
bis(2-Chloroisopropyl) ether ND ug/kg 12/19/15 22:50 108-60-112/19/15 11:04386 1
2-Chloronaphthalene ND ug/kg 12/19/15 22:50 91-58-712/19/15 11:04386 1
2-Chlorophenol ND ug/kg 12/19/15 22:50 95-57-812/19/15 11:04386 1
4-Chlorophenylphenyl ether ND ug/kg 12/19/15 22:50 7005-72-312/19/15 11:04386 1
Chrysene ND ug/kg 12/19/15 22:50 218-01-912/19/15 11:04386 1
Dibenz(a,h)anthracene ND ug/kg 12/19/15 22:50 53-70-312/19/15 11:04386 1
Dibenzofuran ND ug/kg 12/19/15 22:50 132-64-912/19/15 11:04386 1
1,2-Dichlorobenzene ND ug/kg 12/19/15 22:50 95-50-112/19/15 11:04386 1
1,3-Dichlorobenzene ND ug/kg 12/19/15 22:50 541-73-112/19/15 11:04386 1
1,4-Dichlorobenzene ND ug/kg 12/19/15 22:50 106-46-712/19/15 11:04386 1
3,3'-Dichlorobenzidine ND ug/kg 12/19/15 22:50 91-94-112/19/15 11:041930 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/28/2015 04:56 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Sample: E Lab ID: 92280538003 Collected: 12/17/15 15:00 Received: 12/17/15 17:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
2,4-Dichlorophenol ND ug/kg 12/19/15 22:50 120-83-212/19/15 11:04386 1
Diethylphthalate ND ug/kg 12/19/15 22:50 84-66-212/19/15 11:04386 1
2,4-Dimethylphenol ND ug/kg 12/19/15 22:50 105-67-912/19/15 11:04386 1
Dimethylphthalate ND ug/kg 12/19/15 22:50 131-11-312/19/15 11:04386 1
Di-n-butylphthalate ND ug/kg 12/19/15 22:50 84-74-212/19/15 11:04386 1
4,6-Dinitro-2-methylphenol ND ug/kg 12/19/15 22:50 534-52-112/19/15 11:04772 1
2,4-Dinitrophenol ND ug/kg 12/19/15 22:50 51-28-512/19/15 11:041930 1
2,4-Dinitrotoluene ND ug/kg 12/19/15 22:50 121-14-212/19/15 11:04386 1
2,6-Dinitrotoluene ND ug/kg 12/19/15 22:50 606-20-2 L312/19/15 11:04386 1
Di-n-octylphthalate ND ug/kg 12/19/15 22:50 117-84-012/19/15 11:04386 1
bis(2-Ethylhexyl)phthalate ND ug/kg 12/19/15 22:50 117-81-712/19/15 11:04386 1
Fluoranthene ND ug/kg 12/19/15 22:50 206-44-012/19/15 11:04386 1
Fluorene ND ug/kg 12/19/15 22:50 86-73-712/19/15 11:04386 1
Hexachloro-1,3-butadiene ND ug/kg 12/19/15 22:50 87-68-312/19/15 11:04386 1
Hexachlorobenzene ND ug/kg 12/19/15 22:50 118-74-112/19/15 11:04386 1
Hexachlorocyclopentadiene ND ug/kg 12/19/15 22:50 77-47-412/19/15 11:04386 1
Hexachloroethane ND ug/kg 12/19/15 22:50 67-72-112/19/15 11:04386 1
Indeno(1,2,3-cd)pyrene ND ug/kg 12/19/15 22:50 193-39-512/19/15 11:04386 1
Isophorone ND ug/kg 12/19/15 22:50 78-59-112/19/15 11:04386 1
1-Methylnaphthalene ND ug/kg 12/19/15 22:50 90-12-012/19/15 11:04386 1
2-Methylnaphthalene ND ug/kg 12/19/15 22:50 91-57-612/19/15 11:04386 1
2-Methylphenol(o-Cresol) ND ug/kg 12/19/15 22:50 95-48-712/19/15 11:04386 1
3&4-Methylphenol(m&p Cresol) ND ug/kg 12/19/15 22:5012/19/15 11:04386 1
Naphthalene ND ug/kg 12/19/15 22:50 91-20-312/19/15 11:04386 1
2-Nitroaniline ND ug/kg 12/19/15 22:50 88-74-412/19/15 11:041930 1
3-Nitroaniline ND ug/kg 12/19/15 22:50 99-09-212/19/15 11:041930 1
4-Nitroaniline ND ug/kg 12/19/15 22:50 100-01-612/19/15 11:04772 1
Nitrobenzene ND ug/kg 12/19/15 22:50 98-95-312/19/15 11:04386 1
2-Nitrophenol ND ug/kg 12/19/15 22:50 88-75-512/19/15 11:04386 1
4-Nitrophenol ND ug/kg 12/19/15 22:50 100-02-712/19/15 11:041930 1
N-Nitrosodimethylamine ND ug/kg 12/19/15 22:50 62-75-912/19/15 11:04386 1
N-Nitroso-di-n-propylamine ND ug/kg 12/19/15 22:50 621-64-712/19/15 11:04386 1
N-Nitrosodiphenylamine ND ug/kg 12/19/15 22:50 86-30-612/19/15 11:04386 1
Pentachlorophenol ND ug/kg 12/19/15 22:50 87-86-512/19/15 11:041930 1
Phenanthrene ND ug/kg 12/19/15 22:50 85-01-812/19/15 11:04386 1
Phenol ND ug/kg 12/19/15 22:50 108-95-212/19/15 11:04386 1
Pyrene ND ug/kg 12/19/15 22:50 129-00-012/19/15 11:04386 1
1,2,4-Trichlorobenzene ND ug/kg 12/19/15 22:50 120-82-112/19/15 11:04386 1
2,4,5-Trichlorophenol ND ug/kg 12/19/15 22:50 95-95-412/19/15 11:04386 1
2,4,6-Trichlorophenol ND ug/kg 12/19/15 22:50 88-06-212/19/15 11:04386 1
Surrogates
Nitrobenzene-d5 (S) 53 % 12/19/15 22:50 4165-60-012/19/15 11:0423-110 1
2-Fluorobiphenyl (S) 80 % 12/19/15 22:50 321-60-812/19/15 11:0430-110 1
Terphenyl-d14 (S) 65 % 12/19/15 22:50 1718-51-012/19/15 11:0428-110 1
Phenol-d6 (S) 49 % 12/19/15 22:50 13127-88-312/19/15 11:0422-110 1
2-Fluorophenol (S) 52 % 12/19/15 22:50 367-12-412/19/15 11:0413-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/28/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Sample: E Lab ID: 92280538003 Collected: 12/17/15 15:00 Received: 12/17/15 17:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S) 75 % 12/19/15 22:50 118-79-612/19/15 11:0427-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 12/22/15 15:52 67-64-183.9 1
Benzene ND ug/kg 12/22/15 15:52 71-43-24.2 1
Bromobenzene ND ug/kg 12/22/15 15:52 108-86-14.2 1
Bromochloromethane ND ug/kg 12/22/15 15:52 74-97-54.2 1
Bromodichloromethane ND ug/kg 12/22/15 15:52 75-27-44.2 1
Bromoform ND ug/kg 12/22/15 15:52 75-25-24.2 1
Bromomethane ND ug/kg 12/22/15 15:52 74-83-98.4 1
2-Butanone (MEK) ND ug/kg 12/22/15 15:52 78-93-383.9 1
n-Butylbenzene ND ug/kg 12/22/15 15:52 104-51-84.2 1
sec-Butylbenzene ND ug/kg 12/22/15 15:52 135-98-84.2 1
tert-Butylbenzene ND ug/kg 12/22/15 15:52 98-06-64.2 1
Carbon tetrachloride ND ug/kg 12/22/15 15:52 56-23-54.2 1
Chlorobenzene ND ug/kg 12/22/15 15:52 108-90-74.2 1
Chloroethane ND ug/kg 12/22/15 15:52 75-00-38.4 1
Chloroform ND ug/kg 12/22/15 15:52 67-66-34.2 1
Chloromethane ND ug/kg 12/22/15 15:52 74-87-38.4 1
2-Chlorotoluene ND ug/kg 12/22/15 15:52 95-49-84.2 1
4-Chlorotoluene ND ug/kg 12/22/15 15:52 106-43-44.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 12/22/15 15:52 96-12-84.2 1
Dibromochloromethane ND ug/kg 12/22/15 15:52 124-48-14.2 1
1,2-Dibromoethane (EDB) ND ug/kg 12/22/15 15:52 106-93-44.2 1
Dibromomethane ND ug/kg 12/22/15 15:52 74-95-34.2 1
1,2-Dichlorobenzene ND ug/kg 12/22/15 15:52 95-50-14.2 1
1,3-Dichlorobenzene ND ug/kg 12/22/15 15:52 541-73-14.2 1
1,4-Dichlorobenzene ND ug/kg 12/22/15 15:52 106-46-74.2 1
Dichlorodifluoromethane ND ug/kg 12/22/15 15:52 75-71-88.4 1
1,1-Dichloroethane ND ug/kg 12/22/15 15:52 75-34-34.2 1
1,2-Dichloroethane ND ug/kg 12/22/15 15:52 107-06-24.2 1
1,1-Dichloroethene ND ug/kg 12/22/15 15:52 75-35-44.2 1
cis-1,2-Dichloroethene ND ug/kg 12/22/15 15:52 156-59-24.2 1
trans-1,2-Dichloroethene ND ug/kg 12/22/15 15:52 156-60-54.2 1
1,2-Dichloropropane ND ug/kg 12/22/15 15:52 78-87-54.2 1
1,3-Dichloropropane ND ug/kg 12/22/15 15:52 142-28-94.2 1
2,2-Dichloropropane ND ug/kg 12/22/15 15:52 594-20-74.2 1
1,1-Dichloropropene ND ug/kg 12/22/15 15:52 563-58-64.2 1
cis-1,3-Dichloropropene ND ug/kg 12/22/15 15:52 10061-01-54.2 1
trans-1,3-Dichloropropene ND ug/kg 12/22/15 15:52 10061-02-64.2 1
Diisopropyl ether ND ug/kg 12/22/15 15:52 108-20-34.2 1
Ethylbenzene ND ug/kg 12/22/15 15:52 100-41-44.2 1
Hexachloro-1,3-butadiene ND ug/kg 12/22/15 15:52 87-68-34.2 1
2-Hexanone ND ug/kg 12/22/15 15:52 591-78-641.9 1
Isopropylbenzene (Cumene) ND ug/kg 12/22/15 15:52 98-82-84.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/28/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Sample: E Lab ID: 92280538003 Collected: 12/17/15 15:00 Received: 12/17/15 17:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene ND ug/kg 12/22/15 15:52 99-87-64.2 1
Methylene Chloride ND ug/kg 12/22/15 15:52 75-09-216.8 1
4-Methyl-2-pentanone (MIBK) ND ug/kg 12/22/15 15:52 108-10-141.9 1
Methyl-tert-butyl ether ND ug/kg 12/22/15 15:52 1634-04-44.2 1
Naphthalene ND ug/kg 12/22/15 15:52 91-20-34.2 1
n-Propylbenzene ND ug/kg 12/22/15 15:52 103-65-14.2 1
Styrene ND ug/kg 12/22/15 15:52 100-42-54.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 12/22/15 15:52 630-20-64.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 12/22/15 15:52 79-34-54.2 1
Tetrachloroethene ND ug/kg 12/22/15 15:52 127-18-44.2 1
Toluene ND ug/kg 12/22/15 15:52 108-88-34.2 1
1,2,3-Trichlorobenzene ND ug/kg 12/22/15 15:52 87-61-64.2 1
1,2,4-Trichlorobenzene ND ug/kg 12/22/15 15:52 120-82-14.2 1
1,1,1-Trichloroethane ND ug/kg 12/22/15 15:52 71-55-64.2 1
1,1,2-Trichloroethane ND ug/kg 12/22/15 15:52 79-00-54.2 1
Trichloroethene ND ug/kg 12/22/15 15:52 79-01-64.2 1
Trichlorofluoromethane ND ug/kg 12/22/15 15:52 75-69-44.2 1
1,2,3-Trichloropropane ND ug/kg 12/22/15 15:52 96-18-44.2 1
1,2,4-Trimethylbenzene ND ug/kg 12/22/15 15:52 95-63-64.2 1
1,3,5-Trimethylbenzene ND ug/kg 12/22/15 15:52 108-67-84.2 1
Vinyl acetate ND ug/kg 12/22/15 15:52 108-05-441.9 1
Vinyl chloride ND ug/kg 12/22/15 15:52 75-01-48.4 1
Xylene (Total) ND ug/kg 12/22/15 15:52 1330-20-78.4 1
m&p-Xylene ND ug/kg 12/22/15 15:52 179601-23-18.4 1
o-Xylene ND ug/kg 12/22/15 15:52 95-47-64.2 1
Surrogates
Toluene-d8 (S) 101 % 12/22/15 15:52 2037-26-570-130 1
4-Bromofluorobenzene (S) 100 % 12/22/15 15:52 460-00-470-130 1
1,2-Dichloroethane-d4 (S) 122 % 12/22/15 15:52 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 14.5 % 12/21/15 06:560.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/28/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Sample: N1 Lab ID: 92280538004 Collected: 12/17/15 15:10 Received: 12/17/15 17:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-C28) ND mg/kg 12/22/15 00:1812/20/15 11:006.1 1
Surrogates
n-Pentacosane (S) 86 % 12/22/15 00:18 629-99-212/20/15 11:0041-119 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10) ND mg/kg 12/23/15 06:4112/21/15 09:586.2 1
Surrogates
4-Bromofluorobenzene (S) 99 % 12/23/15 06:41 460-00-412/21/15 09:5870-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 18.5 % 12/21/15 06:560.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/28/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Sample: N2 Lab ID: 92280538005 Collected: 12/17/15 15:15 Received: 12/17/15 17:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-C28) ND mg/kg 12/22/15 00:4112/20/15 11:006.0 1
Surrogates
n-Pentacosane (S) 82 % 12/22/15 00:41 629-99-212/20/15 11:0041-119 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10) ND mg/kg 12/23/15 07:1112/21/15 09:587.4 1
Surrogates
4-Bromofluorobenzene (S) 105 % 12/23/15 07:11 460-00-412/21/15 09:5870-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 16.9 % 12/21/15 06:560.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/28/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Sample: N3 Lab ID: 92280538006 Collected: 12/17/15 15:20 Received: 12/17/15 17:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 35468015 GCS THC-Diesel
Diesel Range Organics(C10-C28) ND mg/kg 12/22/15 00:4112/20/15 11:005.9 1
Surrogates
n-Pentacosane (S) 79 % 12/22/15 00:41 629-99-212/20/15 11:0041-119 1
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10) ND mg/kg 12/23/15 07:4212/21/15 09:586.1 1
Surrogates
4-Bromofluorobenzene (S) 98 % 12/23/15 07:42 460-00-412/21/15 09:5870-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 15.2 % 12/21/15 06:560.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/28/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Sample: W Lab ID: 92280538007 Collected: 12/17/15 15:40 Received: 12/17/15 17:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18) ND mg/kg 12/23/15 21:06 N212/21/15 14:3012.3 1
Aliphatic (C19-C36) ND mg/kg 12/23/15 21:06 N212/21/15 14:3012.3 1
Aromatic (C11-C22) ND mg/kg 12/23/15 21:06 N212/21/15 14:3012.3 1
Surrogates
Nonatriacontane (S) 78 % 12/23/15 21:06 7194-86-712/21/15 14:3040-140 1
o-Terphenyl (S) 76 % 12/23/15 21:06 84-15-112/21/15 14:3040-140 1
2-Fluorobiphenyl (S) 92 % 12/23/15 21:06 321-60-812/21/15 14:3040-140 1
2-Bromonaphthalene (S) 89 % 12/23/15 21:06 580-13-212/21/15 14:3040-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08) ND mg/kg 12/21/15 20:58 N212/21/15 09:442.4 1
Aliphatic (C09-C12) ND mg/kg 12/21/15 20:58 N212/21/15 09:442.4 1
Aromatic (C09-C10) ND mg/kg 12/21/15 20:58 N212/21/15 09:442.4 1
Surrogates
4-Bromofluorobenzene (FID) (S) 93 % 12/21/15 20:58 460-00-412/21/15 09:4470-130 1
4-Bromofluorobenzene (PID) (S) 94 % 12/21/15 20:58 460-00-412/21/15 09:4470-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 12/19/15 23:17 83-32-912/19/15 11:04406 1
Acenaphthylene ND ug/kg 12/19/15 23:17 208-96-812/19/15 11:04406 1
Aniline ND ug/kg 12/19/15 23:17 62-53-312/19/15 11:04406 1
Anthracene ND ug/kg 12/19/15 23:17 120-12-712/19/15 11:04406 1
Benzo(a)anthracene ND ug/kg 12/19/15 23:17 56-55-312/19/15 11:04406 1
Benzo(a)pyrene ND ug/kg 12/19/15 23:17 50-32-812/19/15 11:04406 1
Benzo(b)fluoranthene ND ug/kg 12/19/15 23:17 205-99-212/19/15 11:04406 1
Benzo(g,h,i)perylene ND ug/kg 12/19/15 23:17 191-24-212/19/15 11:04406 1
Benzo(k)fluoranthene ND ug/kg 12/19/15 23:17 207-08-912/19/15 11:04406 1
Benzoic Acid ND ug/kg 12/19/15 23:17 65-85-012/19/15 11:042030 1
Benzyl alcohol ND ug/kg 12/19/15 23:17 100-51-612/19/15 11:04812 1
4-Bromophenylphenyl ether ND ug/kg 12/19/15 23:17 101-55-312/19/15 11:04406 1
Butylbenzylphthalate ND ug/kg 12/19/15 23:17 85-68-712/19/15 11:04406 1
4-Chloro-3-methylphenol ND ug/kg 12/19/15 23:17 59-50-712/19/15 11:04812 1
4-Chloroaniline ND ug/kg 12/19/15 23:17 106-47-812/19/15 11:042030 1
bis(2-Chloroethoxy)methane ND ug/kg 12/19/15 23:17 111-91-112/19/15 11:04406 1
bis(2-Chloroethyl) ether ND ug/kg 12/19/15 23:17 111-44-412/19/15 11:04406 1
bis(2-Chloroisopropyl) ether ND ug/kg 12/19/15 23:17 108-60-112/19/15 11:04406 1
2-Chloronaphthalene ND ug/kg 12/19/15 23:17 91-58-712/19/15 11:04406 1
2-Chlorophenol ND ug/kg 12/19/15 23:17 95-57-812/19/15 11:04406 1
4-Chlorophenylphenyl ether ND ug/kg 12/19/15 23:17 7005-72-312/19/15 11:04406 1
Chrysene ND ug/kg 12/19/15 23:17 218-01-912/19/15 11:04406 1
Dibenz(a,h)anthracene ND ug/kg 12/19/15 23:17 53-70-312/19/15 11:04406 1
Dibenzofuran ND ug/kg 12/19/15 23:17 132-64-912/19/15 11:04406 1
1,2-Dichlorobenzene ND ug/kg 12/19/15 23:17 95-50-112/19/15 11:04406 1
1,3-Dichlorobenzene ND ug/kg 12/19/15 23:17 541-73-112/19/15 11:04406 1
1,4-Dichlorobenzene ND ug/kg 12/19/15 23:17 106-46-712/19/15 11:04406 1
3,3'-Dichlorobenzidine ND ug/kg 12/19/15 23:17 91-94-112/19/15 11:042030 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/28/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Sample: W Lab ID: 92280538007 Collected: 12/17/15 15:40 Received: 12/17/15 17:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
2,4-Dichlorophenol ND ug/kg 12/19/15 23:17 120-83-212/19/15 11:04406 1
Diethylphthalate ND ug/kg 12/19/15 23:17 84-66-212/19/15 11:04406 1
2,4-Dimethylphenol ND ug/kg 12/19/15 23:17 105-67-912/19/15 11:04406 1
Dimethylphthalate ND ug/kg 12/19/15 23:17 131-11-312/19/15 11:04406 1
Di-n-butylphthalate ND ug/kg 12/19/15 23:17 84-74-212/19/15 11:04406 1
4,6-Dinitro-2-methylphenol ND ug/kg 12/19/15 23:17 534-52-112/19/15 11:04812 1
2,4-Dinitrophenol ND ug/kg 12/19/15 23:17 51-28-512/19/15 11:042030 1
2,4-Dinitrotoluene ND ug/kg 12/19/15 23:17 121-14-212/19/15 11:04406 1
2,6-Dinitrotoluene ND ug/kg 12/19/15 23:17 606-20-2 L312/19/15 11:04406 1
Di-n-octylphthalate ND ug/kg 12/19/15 23:17 117-84-012/19/15 11:04406 1
bis(2-Ethylhexyl)phthalate ND ug/kg 12/19/15 23:17 117-81-712/19/15 11:04406 1
Fluoranthene ND ug/kg 12/19/15 23:17 206-44-012/19/15 11:04406 1
Fluorene ND ug/kg 12/19/15 23:17 86-73-712/19/15 11:04406 1
Hexachloro-1,3-butadiene ND ug/kg 12/19/15 23:17 87-68-312/19/15 11:04406 1
Hexachlorobenzene ND ug/kg 12/19/15 23:17 118-74-112/19/15 11:04406 1
Hexachlorocyclopentadiene ND ug/kg 12/19/15 23:17 77-47-412/19/15 11:04406 1
Hexachloroethane ND ug/kg 12/19/15 23:17 67-72-112/19/15 11:04406 1
Indeno(1,2,3-cd)pyrene ND ug/kg 12/19/15 23:17 193-39-512/19/15 11:04406 1
Isophorone ND ug/kg 12/19/15 23:17 78-59-112/19/15 11:04406 1
1-Methylnaphthalene ND ug/kg 12/19/15 23:17 90-12-012/19/15 11:04406 1
2-Methylnaphthalene ND ug/kg 12/19/15 23:17 91-57-612/19/15 11:04406 1
2-Methylphenol(o-Cresol) ND ug/kg 12/19/15 23:17 95-48-712/19/15 11:04406 1
3&4-Methylphenol(m&p Cresol) ND ug/kg 12/19/15 23:1712/19/15 11:04406 1
Naphthalene ND ug/kg 12/19/15 23:17 91-20-312/19/15 11:04406 1
2-Nitroaniline ND ug/kg 12/19/15 23:17 88-74-412/19/15 11:042030 1
3-Nitroaniline ND ug/kg 12/19/15 23:17 99-09-212/19/15 11:042030 1
4-Nitroaniline ND ug/kg 12/19/15 23:17 100-01-612/19/15 11:04812 1
Nitrobenzene ND ug/kg 12/19/15 23:17 98-95-312/19/15 11:04406 1
2-Nitrophenol ND ug/kg 12/19/15 23:17 88-75-512/19/15 11:04406 1
4-Nitrophenol ND ug/kg 12/19/15 23:17 100-02-712/19/15 11:042030 1
N-Nitrosodimethylamine ND ug/kg 12/19/15 23:17 62-75-912/19/15 11:04406 1
N-Nitroso-di-n-propylamine ND ug/kg 12/19/15 23:17 621-64-712/19/15 11:04406 1
N-Nitrosodiphenylamine ND ug/kg 12/19/15 23:17 86-30-612/19/15 11:04406 1
Pentachlorophenol ND ug/kg 12/19/15 23:17 87-86-512/19/15 11:042030 1
Phenanthrene ND ug/kg 12/19/15 23:17 85-01-812/19/15 11:04406 1
Phenol ND ug/kg 12/19/15 23:17 108-95-212/19/15 11:04406 1
Pyrene ND ug/kg 12/19/15 23:17 129-00-012/19/15 11:04406 1
1,2,4-Trichlorobenzene ND ug/kg 12/19/15 23:17 120-82-112/19/15 11:04406 1
2,4,5-Trichlorophenol ND ug/kg 12/19/15 23:17 95-95-412/19/15 11:04406 1
2,4,6-Trichlorophenol ND ug/kg 12/19/15 23:17 88-06-212/19/15 11:04406 1
Surrogates
Nitrobenzene-d5 (S) 58 % 12/19/15 23:17 4165-60-012/19/15 11:0423-110 1
2-Fluorobiphenyl (S) 67 % 12/19/15 23:17 321-60-812/19/15 11:0430-110 1
Terphenyl-d14 (S) 68 % 12/19/15 23:17 1718-51-012/19/15 11:0428-110 1
Phenol-d6 (S) 54 % 12/19/15 23:17 13127-88-312/19/15 11:0422-110 1
2-Fluorophenol (S) 60 % 12/19/15 23:17 367-12-412/19/15 11:0413-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/28/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Sample: W Lab ID: 92280538007 Collected: 12/17/15 15:40 Received: 12/17/15 17:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S) 75 % 12/19/15 23:17 118-79-612/19/15 11:0427-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 12/22/15 16:32 67-64-190.9 1
Benzene ND ug/kg 12/22/15 16:32 71-43-24.5 1
Bromobenzene ND ug/kg 12/22/15 16:32 108-86-14.5 1
Bromochloromethane ND ug/kg 12/22/15 16:32 74-97-54.5 1
Bromodichloromethane ND ug/kg 12/22/15 16:32 75-27-44.5 1
Bromoform ND ug/kg 12/22/15 16:32 75-25-24.5 1
Bromomethane ND ug/kg 12/22/15 16:32 74-83-99.1 1
2-Butanone (MEK) ND ug/kg 12/22/15 16:32 78-93-390.9 1
n-Butylbenzene ND ug/kg 12/22/15 16:32 104-51-84.5 1
sec-Butylbenzene ND ug/kg 12/22/15 16:32 135-98-84.5 1
tert-Butylbenzene ND ug/kg 12/22/15 16:32 98-06-64.5 1
Carbon tetrachloride ND ug/kg 12/22/15 16:32 56-23-54.5 1
Chlorobenzene ND ug/kg 12/22/15 16:32 108-90-74.5 1
Chloroethane ND ug/kg 12/22/15 16:32 75-00-39.1 1
Chloroform ND ug/kg 12/22/15 16:32 67-66-34.5 1
Chloromethane ND ug/kg 12/22/15 16:32 74-87-39.1 1
2-Chlorotoluene ND ug/kg 12/22/15 16:32 95-49-84.5 1
4-Chlorotoluene ND ug/kg 12/22/15 16:32 106-43-44.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 12/22/15 16:32 96-12-84.5 1
Dibromochloromethane ND ug/kg 12/22/15 16:32 124-48-14.5 1
1,2-Dibromoethane (EDB) ND ug/kg 12/22/15 16:32 106-93-44.5 1
Dibromomethane ND ug/kg 12/22/15 16:32 74-95-34.5 1
1,2-Dichlorobenzene ND ug/kg 12/22/15 16:32 95-50-14.5 1
1,3-Dichlorobenzene ND ug/kg 12/22/15 16:32 541-73-14.5 1
1,4-Dichlorobenzene ND ug/kg 12/22/15 16:32 106-46-74.5 1
Dichlorodifluoromethane ND ug/kg 12/22/15 16:32 75-71-89.1 1
1,1-Dichloroethane ND ug/kg 12/22/15 16:32 75-34-34.5 1
1,2-Dichloroethane ND ug/kg 12/22/15 16:32 107-06-24.5 1
1,1-Dichloroethene ND ug/kg 12/22/15 16:32 75-35-44.5 1
cis-1,2-Dichloroethene ND ug/kg 12/22/15 16:32 156-59-24.5 1
trans-1,2-Dichloroethene ND ug/kg 12/22/15 16:32 156-60-54.5 1
1,2-Dichloropropane ND ug/kg 12/22/15 16:32 78-87-54.5 1
1,3-Dichloropropane ND ug/kg 12/22/15 16:32 142-28-94.5 1
2,2-Dichloropropane ND ug/kg 12/22/15 16:32 594-20-74.5 1
1,1-Dichloropropene ND ug/kg 12/22/15 16:32 563-58-64.5 1
cis-1,3-Dichloropropene ND ug/kg 12/22/15 16:32 10061-01-54.5 1
trans-1,3-Dichloropropene ND ug/kg 12/22/15 16:32 10061-02-64.5 1
Diisopropyl ether ND ug/kg 12/22/15 16:32 108-20-34.5 1
Ethylbenzene ND ug/kg 12/22/15 16:32 100-41-44.5 1
Hexachloro-1,3-butadiene ND ug/kg 12/22/15 16:32 87-68-34.5 1
2-Hexanone ND ug/kg 12/22/15 16:32 591-78-645.4 1
Isopropylbenzene (Cumene) ND ug/kg 12/22/15 16:32 98-82-84.5 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/28/2015 04:56 PM
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Page 17 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Sample: W Lab ID: 92280538007 Collected: 12/17/15 15:40 Received: 12/17/15 17:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene ND ug/kg 12/22/15 16:32 99-87-64.5 1
Methylene Chloride 18.6 ug/kg 12/22/15 16:32 75-09-2 C918.2 1
4-Methyl-2-pentanone (MIBK) ND ug/kg 12/22/15 16:32 108-10-145.4 1
Methyl-tert-butyl ether ND ug/kg 12/22/15 16:32 1634-04-44.5 1
Naphthalene ND ug/kg 12/22/15 16:32 91-20-34.5 1
n-Propylbenzene ND ug/kg 12/22/15 16:32 103-65-14.5 1
Styrene ND ug/kg 12/22/15 16:32 100-42-54.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 12/22/15 16:32 630-20-64.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 12/22/15 16:32 79-34-54.5 1
Tetrachloroethene ND ug/kg 12/22/15 16:32 127-18-44.5 1
Toluene ND ug/kg 12/22/15 16:32 108-88-34.5 1
1,2,3-Trichlorobenzene ND ug/kg 12/22/15 16:32 87-61-64.5 1
1,2,4-Trichlorobenzene ND ug/kg 12/22/15 16:32 120-82-14.5 1
1,1,1-Trichloroethane ND ug/kg 12/22/15 16:32 71-55-64.5 1
1,1,2-Trichloroethane ND ug/kg 12/22/15 16:32 79-00-54.5 1
Trichloroethene ND ug/kg 12/22/15 16:32 79-01-64.5 1
Trichlorofluoromethane ND ug/kg 12/22/15 16:32 75-69-44.5 1
1,2,3-Trichloropropane ND ug/kg 12/22/15 16:32 96-18-44.5 1
1,2,4-Trimethylbenzene ND ug/kg 12/22/15 16:32 95-63-64.5 1
1,3,5-Trimethylbenzene ND ug/kg 12/22/15 16:32 108-67-84.5 1
Vinyl acetate ND ug/kg 12/22/15 16:32 108-05-445.4 1
Vinyl chloride ND ug/kg 12/22/15 16:32 75-01-49.1 1
Xylene (Total) ND ug/kg 12/22/15 16:32 1330-20-79.1 1
m&p-Xylene ND ug/kg 12/22/15 16:32 179601-23-19.1 1
o-Xylene ND ug/kg 12/22/15 16:32 95-47-64.5 1
Surrogates
Toluene-d8 (S) 103 % 12/22/15 16:32 2037-26-570-130 1
4-Bromofluorobenzene (S) 97 % 12/22/15 16:32 460-00-470-130 1
1,2-Dichloroethane-d4 (S) 111 % 12/22/15 16:32 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 18.7 % 12/21/15 06:560.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/28/2015 04:56 PM
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Page 18 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/10207
EPA 5035A/5030B
EPA 8015 Modified
Gasoline Range Organics
Associated Lab Samples: 92280538001, 92280538004, 92280538005, 92280538006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1634191
Associated Lab Samples:92280538001, 92280538004, 92280538005, 92280538006
Matrix: Solid
Analyzed
Gas Range Organics (C6-C10) mg/kg ND 6.0 12/23/15 00:39
4-Bromofluorobenzene (S) % 102 70-167 12/23/15 00:39
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1634192LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10) mg/kg 50.250 100 70-165
4-Bromofluorobenzene (S) % 103 70-167
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1634193MATRIX SPIKE SAMPLE:
MSSpike
Result
92280342001
Gas Range Organics (C6-C10) mg/kg 59.753.6 111 47-187<6.4
4-Bromofluorobenzene (S) % 97 70-167
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92280342002
1634194SAMPLE DUPLICATE:
Gas Range Organics (C6-C10) mg/kg ND 30<6.1
4-Bromofluorobenzene (S) % 97 5103
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/28/2015 04:56 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/10216
EPA 5035A/5030B
EPA 8015 Modified
Gasoline Range Organics
Associated Lab Samples: 92280538002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1636307
Associated Lab Samples:92280538002
Matrix: Solid
Analyzed
Gas Range Organics (C6-C10) mg/kg ND 6.0 12/23/15 14:37
4-Bromofluorobenzene (S) % 92 70-167 12/23/15 14:37
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1636308LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10) mg/kg 49.350 99 70-165
4-Bromofluorobenzene (S) % 90 70-167
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1636309MATRIX SPIKE SAMPLE:
MSSpike
Result
92280575006
Gas Range Organics (C6-C10) mg/kg 49.849.6 99 47-187ND
4-Bromofluorobenzene (S) % 78 70-167
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92280575007
1636310SAMPLE DUPLICATE:
Gas Range Organics (C6-C10) mg/kg 58.7 14 3051.2
4-Bromofluorobenzene (S) % 85 978
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/28/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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[phone]
Page 20 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/10205
MADEP VPH
MADEP VPH
VPH NC Soil
Associated Lab Samples: 92280538003, 92280538007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1634168
Associated Lab Samples:92280538003, 92280538007
Matrix: Solid
Analyzed
Aliphatic (C05-C08) mg/kg ND 2.5 N212/21/15 13:26
Aliphatic (C09-C12) mg/kg ND 2.5 N212/21/15 13:26
Aromatic (C09-C10) mg/kg ND 2.5 N212/21/15 13:26
4-Bromofluorobenzene (FID) (S) % 97 70-130 12/21/15 13:26
4-Bromofluorobenzene (PID) (S) % 99 70-130 12/21/15 13:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1634169LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1634170
Aliphatic (C05-C08) mg/kg 14.6 N215 97 70-1309514.3 2 25
Aliphatic (C09-C12) mg/kg 13.1 N215 88 30-1309113.7 4 25
Aromatic (C09-C10) mg/kg 5.0 N25 101 70-130984.9 2 25
4-Bromofluorobenzene (FID) (S) % 102 70-130101
4-Bromofluorobenzene (PID) (S) % 105 70-130103
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/28/2015 04:56 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/34861
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples: 92280538003, 92280538007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1635236
Associated Lab Samples:92280538003, 92280538007
Matrix: Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.3 12/22/15 10:35
1,1,1-Trichloroethane ug/kg ND 5.3 12/22/15 10:35
1,1,2,2-Tetrachloroethane ug/kg ND 5.3 12/22/15 10:35
1,1,2-Trichloroethane ug/kg ND 5.3 12/22/15 10:35
1,1-Dichloroethane ug/kg ND 5.3 12/22/15 10:35
1,1-Dichloroethene ug/kg ND 5.3 12/22/15 10:35
1,1-Dichloropropene ug/kg ND 5.3 12/22/15 10:35
1,2,3-Trichlorobenzene ug/kg ND 5.3 12/22/15 10:35
1,2,3-Trichloropropane ug/kg ND 5.3 12/22/15 10:35
1,2,4-Trichlorobenzene ug/kg ND 5.3 12/22/15 10:35
1,2,4-Trimethylbenzene ug/kg ND 5.3 12/22/15 10:35
1,2-Dibromo-3-chloropropane ug/kg ND 5.3 12/22/15 10:35
1,2-Dibromoethane (EDB) ug/kg ND 5.3 12/22/15 10:35
1,2-Dichlorobenzene ug/kg ND 5.3 12/22/15 10:35
1,2-Dichloroethane ug/kg ND 5.3 12/22/15 10:35
1,2-Dichloropropane ug/kg ND 5.3 12/22/15 10:35
1,3,5-Trimethylbenzene ug/kg ND 5.3 12/22/15 10:35
1,3-Dichlorobenzene ug/kg ND 5.3 12/22/15 10:35
1,3-Dichloropropane ug/kg ND 5.3 12/22/15 10:35
1,4-Dichlorobenzene ug/kg ND 5.3 12/22/15 10:35
2,2-Dichloropropane ug/kg ND 5.3 12/22/15 10:35
2-Butanone (MEK) ug/kg ND 107 12/22/15 10:35
2-Chlorotoluene ug/kg ND 5.3 12/22/15 10:35
2-Hexanone ug/kg ND 53.3 12/22/15 10:35
4-Chlorotoluene ug/kg ND 5.3 12/22/15 10:35
4-Methyl-2-pentanone (MIBK) ug/kg ND 53.3 12/22/15 10:35
Acetone ug/kg ND 107 12/22/15 10:35
Benzene ug/kg ND 5.3 12/22/15 10:35
Bromobenzene ug/kg ND 5.3 12/22/15 10:35
Bromochloromethane ug/kg ND 5.3 12/22/15 10:35
Bromodichloromethane ug/kg ND 5.3 12/22/15 10:35
Bromoform ug/kg ND 5.3 12/22/15 10:35
Bromomethane ug/kg ND 10.7 12/22/15 10:35
Carbon tetrachloride ug/kg ND 5.3 12/22/15 10:35
Chlorobenzene ug/kg ND 5.3 12/22/15 10:35
Chloroethane ug/kg ND 10.7 12/22/15 10:35
Chloroform ug/kg ND 5.3 12/22/15 10:35
Chloromethane ug/kg ND 10.7 12/22/15 10:35
cis-1,2-Dichloroethene ug/kg ND 5.3 12/22/15 10:35
cis-1,3-Dichloropropene ug/kg ND 5.3 12/22/15 10:35
Dibromochloromethane ug/kg ND 5.3 12/22/15 10:35
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/28/2015 04:56 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1635236
Associated Lab Samples:92280538003, 92280538007
Matrix: Solid
Analyzed
Dibromomethane ug/kg ND 5.3 12/22/15 10:35
Dichlorodifluoromethane ug/kg ND 10.7 12/22/15 10:35
Diisopropyl ether ug/kg ND 5.3 12/22/15 10:35
Ethylbenzene ug/kg ND 5.3 12/22/15 10:35
Hexachloro-1,3-butadiene ug/kg ND 5.3 12/22/15 10:35
Isopropylbenzene (Cumene) ug/kg ND 5.3 12/22/15 10:35
m&p-Xylene ug/kg ND 10.7 12/22/15 10:35
Methyl-tert-butyl ether ug/kg ND 5.3 12/22/15 10:35
Methylene Chloride ug/kg ND 21.3 12/22/15 10:35
n-Butylbenzene ug/kg ND 5.3 12/22/15 10:35
n-Propylbenzene ug/kg ND 5.3 12/22/15 10:35
Naphthalene ug/kg ND 5.3 12/22/15 10:35
o-Xylene ug/kg ND 5.3 12/22/15 10:35
p-Isopropyltoluene ug/kg ND 5.3 12/22/15 10:35
sec-Butylbenzene ug/kg ND 5.3 12/22/15 10:35
Styrene ug/kg ND 5.3 12/22/15 10:35
tert-Butylbenzene ug/kg ND 5.3 12/22/15 10:35
Tetrachloroethene ug/kg ND 5.3 12/22/15 10:35
Toluene ug/kg ND 5.3 12/22/15 10:35
trans-1,2-Dichloroethene ug/kg ND 5.3 12/22/15 10:35
trans-1,3-Dichloropropene ug/kg ND 5.3 12/22/15 10:35
Trichloroethene ug/kg ND 5.3 12/22/15 10:35
Trichlorofluoromethane ug/kg ND 5.3 12/22/15 10:35
Vinyl acetate ug/kg ND 53.3 12/22/15 10:35
Vinyl chloride ug/kg ND 10.7 12/22/15 10:35
Xylene (Total) ug/kg ND 10.7 12/22/15 10:35
1,2-Dichloroethane-d4 (S) % 103 70-132 12/22/15 10:35
4-Bromofluorobenzene (S) % 97 70-130 12/22/15 10:35
Toluene-d8 (S) % 101 70-130 12/22/15 10:35
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1635237LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 51.655.9 92 74-137
1,1,1-Trichloroethane ug/kg 53.555.9 96 67-140
1,1,2,2-Tetrachloroethane ug/kg 52.555.9 94 72-141
1,1,2-Trichloroethane ug/kg 53.855.9 96 78-138
1,1-Dichloroethane ug/kg 52.755.9 94 69-134
1,1-Dichloroethene ug/kg 58.755.9 105 67-138
1,1-Dichloropropene ug/kg 58.255.9 104 69-139
1,2,3-Trichlorobenzene ug/kg 55.355.9 99 70-146
1,2,3-Trichloropropane ug/kg 51.255.9 91 69-144
1,2,4-Trichlorobenzene ug/kg 53.455.9 96 68-148
1,2,4-Trimethylbenzene ug/kg 55.755.9 100 74-137
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/28/2015 04:56 PM
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Page 23 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1635237LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 58.855.9 105 65-140
1,2-Dibromoethane (EDB) ug/kg 53.355.9 95 77-135
1,2-Dichlorobenzene ug/kg 55.455.9 99 77-141
1,2-Dichloroethane ug/kg 53.655.9 96 65-137
1,2-Dichloropropane ug/kg 54.255.9 97 72-136
1,3,5-Trimethylbenzene ug/kg 54.655.9 98 76-133
1,3-Dichlorobenzene ug/kg 56.655.9 101 74-138
1,3-Dichloropropane ug/kg 53.255.9 95 71-139
1,4-Dichlorobenzene ug/kg 54.755.9 98 76-138
2,2-Dichloropropane ug/kg 54.055.9 97 68-137
2-Butanone (MEK) ug/kg 110J112 98 58-147
2-Chlorotoluene ug/kg 56.155.9 100 73-139
2-Hexanone ug/kg 110112 98 62-145
4-Chlorotoluene ug/kg 55.455.9 99 76-141
4-Methyl-2-pentanone (MIBK) ug/kg 118112 105 64-149
Acetone ug/kg 108J112 97 53-153
Benzene ug/kg 56.055.9 100 73-135
Bromobenzene ug/kg 54.955.9 98 75-133
Bromochloromethane ug/kg 55.455.9 99 73-134
Bromodichloromethane ug/kg 53.055.9 95 71-135
Bromoform ug/kg 49.555.9 88 66-141
Bromomethane ug/kg 58.755.9 105 53-160
Carbon tetrachloride ug/kg 52.455.9 94 60-145
Chlorobenzene ug/kg 53.155.9 95 78-130
Chloroethane ug/kg 60.055.9 107 64-149
Chloroform ug/kg 56.555.9 101 70-134
Chloromethane ug/kg 57.855.9 103 52-150
cis-1,2-Dichloroethene ug/kg 57.655.9 103 70-133
cis-1,3-Dichloropropene ug/kg 53.055.9 95 68-134
Dibromochloromethane ug/kg 53.055.9 95 71-138
Dibromomethane ug/kg 54.555.9 97 74-130
Dichlorodifluoromethane ug/kg 53.455.9 95 40-160
Diisopropyl ether ug/kg 59.255.9 106 69-141
Ethylbenzene ug/kg 52.955.9 95 75-133
Hexachloro-1,3-butadiene ug/kg 52.755.9 94 68-143
Isopropylbenzene (Cumene) ug/kg 56.655.9 101 76-143
m&p-Xylene ug/kg 105112 94 75-136
Methyl-tert-butyl ether ug/kg 56.155.9 100 68-144
Methylene Chloride ug/kg 60.655.9 108 45-154
n-Butylbenzene ug/kg 57.355.9 102 72-137
n-Propylbenzene ug/kg 54.055.9 97 76-136
Naphthalene ug/kg 58.655.9 105 68-151
o-Xylene ug/kg 52.455.9 94 76-141
p-Isopropyltoluene ug/kg 54.755.9 98 76-140
sec-Butylbenzene ug/kg 57.655.9 103 79-139
Styrene ug/kg 54.455.9 97 79-137
tert-Butylbenzene ug/kg 49.955.9 89 74-143
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/28/2015 04:56 PM
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9800 Kincey Ave. Suite 100
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Page 24 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1635237LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 43.755.9 78 71-138
Toluene ug/kg 53.755.9 96 74-131
trans-1,2-Dichloroethene ug/kg 59.055.9 105 67-135
trans-1,3-Dichloropropene ug/kg 52.655.9 94 65-146
Trichloroethene ug/kg 54.055.9 97 67-135
Trichlorofluoromethane ug/kg 56.855.9 102 59-144
Vinyl acetate ug/kg 118112 106 40-160
Vinyl chloride ug/kg 63.455.9 113 56-141
Xylene (Total) ug/kg 158168 94 76-137
1,2-Dichloroethane-d4 (S) % 101 70-132
4-Bromofluorobenzene (S) % 92 70-130
Toluene-d8 (S) % 100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1636222MATRIX SPIKE SAMPLE:
MSSpike
Result
92280058002
1,1,1,2-Tetrachloroethane ug/kg 19.720.4 97 70-130ND
1,1,1-Trichloroethane ug/kg 23.920.4 117 70-130ND
1,1,2,2-Tetrachloroethane ug/kg 20.920.4 103 70-130ND
1,1,2-Trichloroethane ug/kg 21.320.4 104 70-130ND
1,1-Dichloroethane ug/kg 23.620.4 116 70-130ND
1,1-Dichloroethene ug/kg 25.620.4 126 49-180ND
1,1-Dichloropropene ug/kg 24.420.4 120 70-130ND
1,2,3-Trichlorobenzene ug/kg 9.3 M120.4 45 70-130ND
1,2,3-Trichloropropane ug/kg 18.620.4 91 70-130ND
1,2,4-Trichlorobenzene ug/kg 9.6 M120.4 47 70-130ND
1,2,4-Trimethylbenzene ug/kg 20.220.4 99 70-130ND
1,2-Dibromo-3-chloropropane ug/kg 23.220.4 114 70-130ND
1,2-Dibromoethane (EDB) ug/kg 22.020.4 108 70-130ND
1,2-Dichlorobenzene ug/kg 17.820.4 87 70-130ND
1,2-Dichloroethane ug/kg 25.020.4 122 70-130ND
1,2-Dichloropropane ug/kg 22.520.4 110 70-130ND
1,3,5-Trimethylbenzene ug/kg 20.320.4 100 70-130ND
1,3-Dichlorobenzene ug/kg 17.420.4 85 70-130ND
1,3-Dichloropropane ug/kg 21.220.4 104 70-130ND
1,4-Dichlorobenzene ug/kg 17.320.4 85 70-130ND
2,2-Dichloropropane ug/kg 22.920.4 112 70-130ND
2-Butanone (MEK) ug/kg 56.6J M140.8 139 70-130ND
2-Chlorotoluene ug/kg 20.720.4 102 70-130ND
2-Hexanone ug/kg 44.2J40.8 108 70-130ND
4-Chlorotoluene ug/kg 20.320.4 100 70-130ND
4-Methyl-2-pentanone (MIBK) ug/kg 52.640.8 129 70-130ND
Acetone ug/kg 68.2J40.8 104 70-13025.9J
Benzene ug/kg 22.420.4 110 50-166ND
Bromobenzene ug/kg 20.820.4 102 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/28/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1636222MATRIX SPIKE SAMPLE:
MSSpike
Result
92280058002
Bromochloromethane ug/kg 21.620.4 106 70-130ND
Bromodichloromethane ug/kg 21.420.4 105 70-130ND
Bromoform ug/kg 18.020.4 88 70-130ND
Bromomethane ug/kg 24.620.4 120 70-130ND
Carbon tetrachloride ug/kg 23.420.4 115 70-130ND
Chlorobenzene ug/kg 19.620.4 96 43-169ND
Chloroethane ug/kg 24.020.4 118 70-130ND
Chloroform ug/kg 24.820.4 122 70-130ND
Chloromethane ug/kg 25.220.4 123 70-130ND
cis-1,2-Dichloroethene ug/kg 25.220.4 124 70-130ND
cis-1,3-Dichloropropene ug/kg 21.620.4 106 70-130ND
Dibromochloromethane ug/kg 20.420.4 100 70-130ND
Dibromomethane ug/kg 22.720.4 111 70-130ND
Dichlorodifluoromethane ug/kg 20.020.4 98 70-130ND
Diisopropyl ether ug/kg 26.8 M120.4 132 70-130ND
Ethylbenzene ug/kg 20.520.4 101 70-130ND
Hexachloro-1,3-butadiene ug/kg 10.2 M120.4 50 70-130ND
Isopropylbenzene (Cumene) ug/kg 21.620.4 106 70-130ND
m&p-Xylene ug/kg 41.040.8 101 70-130ND
Methyl-tert-butyl ether ug/kg 23.520.4 115 70-130ND
Methylene Chloride ug/kg 60.6 M120.4 212 70-13017.4J
n-Butylbenzene ug/kg 17.820.4 87 70-130ND
n-Propylbenzene ug/kg 21.220.4 104 70-130ND
Naphthalene ug/kg 13.5 M120.4 66 70-130ND
o-Xylene ug/kg 19.620.4 96 70-130ND
p-Isopropyltoluene ug/kg 19.320.4 94 70-130ND
sec-Butylbenzene ug/kg 20.920.4 102 70-130ND
Styrene ug/kg 18.520.4 91 70-130ND
tert-Butylbenzene ug/kg 19.220.4 94 70-130ND
Tetrachloroethene ug/kg 16.820.4 82 70-130ND
Toluene ug/kg 21.520.4 105 52-163ND
trans-1,2-Dichloroethene ug/kg 25.520.4 125 70-130ND
trans-1,3-Dichloropropene ug/kg 20.720.4 101 70-130ND
Trichloroethene ug/kg 21.420.4 105 49-167ND
Trichlorofluoromethane ug/kg 19.020.4 93 70-130ND
Vinyl acetate ug/kg 11.6J M140.8 28 70-130ND
Vinyl chloride ug/kg 26.120.4 128 70-130ND
1,2-Dichloroethane-d4 (S) % 122 70-132
4-Bromofluorobenzene (S) % 90 70-130
Toluene-d8 (S) % 99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92280058001
1636221SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/28/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92280058001
1636221SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB) ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK) ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK) ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene) ug/kg ND 30ND
m&p-Xylene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/28/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92280058001
1636221SAMPLE DUPLICATE:
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg 18.5J 3012.6J
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total) ug/kg ND 30ND
1,2-Dichloroethane-d4 (S) % 127 32103
4-Bromofluorobenzene (S) % 89 1288
Toluene-d8 (S) % 102 1g1499
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/28/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/39871
EPA 3546
EPA 8015 Modified
8015 Solid GCSV
Associated Lab Samples: 92280538001, 92280538004, 92280538005, 92280538006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1633990
Associated Lab Samples:92280538001, 92280538004, 92280538005, 92280538006
Matrix: Solid
Analyzed
Diesel Range Organics(C10-C28) mg/kg ND 5.0 12/21/15 23:54
n-Pentacosane (S) % 77 41-119 12/21/15 23:54
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1633991LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28) mg/kg 62.066.7 93 49-113
n-Pentacosane (S) % 87 41-119
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1633992MATRIX SPIKE SAMPLE:
MSSpike
Result
92280575005
Diesel Range Organics(C10-C28) mg/kg 99.081.1 101 10-14617.3
n-Pentacosane (S) % 88 41-119
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92280575006
1633993SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28) mg/kg ND 30ND
n-Pentacosane (S) % 86 781
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/28/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/39945
EPA 3546
EPA 8015 Modified
8015 Solid GCSV
Associated Lab Samples: 92280538002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1636128
Associated Lab Samples:92280538002
Matrix: Solid
Analyzed
Diesel Range Organics(C10-C28) mg/kg ND 5.0 12/23/15 18:41
n-Pentacosane (S) % 78 41-119 12/23/15 18:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1636129LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1636130
Diesel Range Organics(C10-C28) mg/kg 54.166.7 81 49-1139060.1 11 30
n-Pentacosane (S) % 81 41-11983
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/28/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/39866
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples: 92280538003, 92280538007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1633907
Associated Lab Samples:92280538003, 92280538007
Matrix: Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 330 12/19/15 18:47
1,2-Dichlorobenzene ug/kg ND 330 12/19/15 18:47
1,3-Dichlorobenzene ug/kg ND 330 12/19/15 18:47
1,4-Dichlorobenzene ug/kg ND 330 12/19/15 18:47
1-Methylnaphthalene ug/kg ND 330 12/19/15 18:47
2,4,5-Trichlorophenol ug/kg ND 330 12/19/15 18:47
2,4,6-Trichlorophenol ug/kg ND 330 12/19/15 18:47
2,4-Dichlorophenol ug/kg ND 330 12/19/15 18:47
2,4-Dimethylphenol ug/kg ND 330 12/19/15 18:47
2,4-Dinitrophenol ug/kg ND 1650 12/19/15 18:47
2,4-Dinitrotoluene ug/kg ND 330 12/19/15 18:47
2,6-Dinitrotoluene ug/kg ND 330 12/19/15 18:47
2-Chloronaphthalene ug/kg ND 330 12/19/15 18:47
2-Chlorophenol ug/kg ND 330 12/19/15 18:47
2-Methylnaphthalene ug/kg ND 330 12/19/15 18:47
2-Methylphenol(o-Cresol) ug/kg ND 330 12/19/15 18:47
2-Nitroaniline ug/kg ND 1650 12/19/15 18:47
2-Nitrophenol ug/kg ND 330 12/19/15 18:47
3&4-Methylphenol(m&p Cresol) ug/kg ND 330 12/19/15 18:47
3,3'-Dichlorobenzidine ug/kg ND 1650 12/19/15 18:47
3-Nitroaniline ug/kg ND 1650 12/19/15 18:47
4,6-Dinitro-2-methylphenol ug/kg ND 660 12/19/15 18:47
4-Bromophenylphenyl ether ug/kg ND 330 12/19/15 18:47
4-Chloro-3-methylphenol ug/kg ND 660 12/19/15 18:47
4-Chloroaniline ug/kg ND 1650 12/19/15 18:47
4-Chlorophenylphenyl ether ug/kg ND 330 12/19/15 18:47
4-Nitroaniline ug/kg ND 660 12/19/15 18:47
4-Nitrophenol ug/kg ND 1650 12/19/15 18:47
Acenaphthene ug/kg ND 330 12/19/15 18:47
Acenaphthylene ug/kg ND 330 12/19/15 18:47
Aniline ug/kg ND 330 12/19/15 18:47
Anthracene ug/kg ND 330 12/19/15 18:47
Benzo(a)anthracene ug/kg ND 330 12/19/15 18:47
Benzo(a)pyrene ug/kg ND 330 12/19/15 18:47
Benzo(b)fluoranthene ug/kg ND 330 12/19/15 18:47
Benzo(g,h,i)perylene ug/kg ND 330 12/19/15 18:47
Benzo(k)fluoranthene ug/kg ND 330 12/19/15 18:47
Benzoic Acid ug/kg ND 1650 12/19/15 18:47
Benzyl alcohol ug/kg ND 660 12/19/15 18:47
bis(2-Chloroethoxy)methane ug/kg ND 330 12/19/15 18:47
bis(2-Chloroethyl) ether ug/kg ND 330 12/19/15 18:47
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/28/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1633907
Associated Lab Samples:92280538003, 92280538007
Matrix: Solid
Analyzed
bis(2-Chloroisopropyl) ether ug/kg ND 330 12/19/15 18:47
bis(2-Ethylhexyl)phthalate ug/kg ND 330 12/19/15 18:47
Butylbenzylphthalate ug/kg ND 330 12/19/15 18:47
Chrysene ug/kg ND 330 12/19/15 18:47
Di-n-butylphthalate ug/kg ND 330 12/19/15 18:47
Di-n-octylphthalate ug/kg ND 330 12/19/15 18:47
Dibenz(a,h)anthracene ug/kg ND 330 12/19/15 18:47
Dibenzofuran ug/kg ND 330 12/19/15 18:47
Diethylphthalate ug/kg ND 330 12/19/15 18:47
Dimethylphthalate ug/kg ND 330 12/19/15 18:47
Fluoranthene ug/kg ND 330 12/19/15 18:47
Fluorene ug/kg ND 330 12/19/15 18:47
Hexachloro-1,3-butadiene ug/kg ND 330 12/19/15 18:47
Hexachlorobenzene ug/kg ND 330 12/19/15 18:47
Hexachlorocyclopentadiene ug/kg ND 330 12/19/15 18:47
Hexachloroethane ug/kg ND 330 12/19/15 18:47
Indeno(1,2,3-cd)pyrene ug/kg ND 330 12/19/15 18:47
Isophorone ug/kg ND 330 12/19/15 18:47
N-Nitroso-di-n-propylamine ug/kg ND 330 12/19/15 18:47
N-Nitrosodimethylamine ug/kg ND 330 12/19/15 18:47
N-Nitrosodiphenylamine ug/kg ND 330 12/19/15 18:47
Naphthalene ug/kg ND 330 12/19/15 18:47
Nitrobenzene ug/kg ND 330 12/19/15 18:47
Pentachlorophenol ug/kg ND 1650 12/19/15 18:47
Phenanthrene ug/kg ND 330 12/19/15 18:47
Phenol ug/kg ND 330 12/19/15 18:47
Pyrene ug/kg ND 330 12/19/15 18:47
2,4,6-Tribromophenol (S) % 91 27-110 12/19/15 18:47
2-Fluorobiphenyl (S) % 75 30-110 12/19/15 18:47
2-Fluorophenol (S) % 52 13-110 12/19/15 18:47
Nitrobenzene-d5 (S) % 61 23-110 12/19/15 18:47
Phenol-d6 (S) % 59 22-110 12/19/15 18:47
Terphenyl-d14 (S) % 82 28-110 12/19/15 18:47
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1633908LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 12701670 76 36-120
1,2-Dichlorobenzene ug/kg 14001670 84 41-120
1,3-Dichlorobenzene ug/kg 12101670 72 66-120
1,4-Dichlorobenzene ug/kg 12001670 72 42-120
1-Methylnaphthalene ug/kg 16001670 96 40-120
2,4,5-Trichlorophenol ug/kg 15301670 92 37-120
2,4,6-Trichlorophenol ug/kg 15401670 92 40-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/28/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1633908LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dichlorophenol ug/kg 14201670 85 33-120
2,4-Dimethylphenol ug/kg 13401670 80 36-120
2,4-Dinitrophenol ug/kg 74808330 90 22-121
2,4-Dinitrotoluene ug/kg 15401670 92 60-120
2,6-Dinitrotoluene ug/kg 2030 L01670 122 54-120
2-Chloronaphthalene ug/kg 14201670 85 41-120
2-Chlorophenol ug/kg 13501670 81 39-120
2-Methylnaphthalene ug/kg 15601670 94 26-120
2-Methylphenol(o-Cresol) ug/kg 13301670 80 41-120
2-Nitroaniline ug/kg 22203330 66 45-120
2-Nitrophenol ug/kg 14501670 87 35-120
3&4-Methylphenol(m&p Cresol) ug/kg 11701670 70 35-120
3,3'-Dichlorobenzidine ug/kg 25903330 78 16-125
3-Nitroaniline ug/kg 25303330 76 45-120
4,6-Dinitro-2-methylphenol ug/kg 27703330 83 46-120
4-Bromophenylphenyl ether ug/kg 12801670 77 36-120
4-Chloro-3-methylphenol ug/kg 27903330 84 37-120
4-Chloroaniline ug/kg 21703330 65 35-120
4-Chlorophenylphenyl ether ug/kg 12701670 76 30-120
4-Nitroaniline ug/kg 26103330 78 48-120
4-Nitrophenol ug/kg 62908330 76 43-120
Acenaphthene ug/kg 13601670 82 46-120
Acenaphthylene ug/kg 19001670 114 46-120
Aniline ug/kg 10901670 66 33-120
Anthracene ug/kg 14301670 86 63-120
Benzo(a)anthracene ug/kg 14001670 84 61-120
Benzo(a)pyrene ug/kg 12001670 72 59-120
Benzo(b)fluoranthene ug/kg 12101670 73 55-120
Benzo(g,h,i)perylene ug/kg 9621670 58 57-120
Benzo(k)fluoranthene ug/kg 14401670 86 56-120
Benzoic Acid ug/kg 53808330 65 13-120
Benzyl alcohol ug/kg 29803330 89 34-120
bis(2-Chloroethoxy)methane ug/kg 10201670 61 21-120
bis(2-Chloroethyl) ether ug/kg 10301670 62 25-120
bis(2-Chloroisopropyl) ether ug/kg 5871670 35 13-120
bis(2-Ethylhexyl)phthalate ug/kg 16101670 97 56-123
Butylbenzylphthalate ug/kg 17101670 103 57-120
Chrysene ug/kg 12901670 78 64-120
Di-n-butylphthalate ug/kg 17201670 103 58-120
Di-n-octylphthalate ug/kg 14501670 87 47-121
Dibenz(a,h)anthracene ug/kg 12001670 72 56-120
Dibenzofuran ug/kg 13901670 83 43-120
Diethylphthalate ug/kg 13801670 83 55-120
Dimethylphthalate ug/kg 16601670 99 54-120
Fluoranthene ug/kg 14601670 87 61-120
Fluorene ug/kg 13901670 83 51-120
Hexachloro-1,3-butadiene ug/kg 15501670 93 22-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 12/28/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1633908LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/kg 14201670 85 53-120
Hexachlorocyclopentadiene ug/kg 9661670 58 18-150
Hexachloroethane ug/kg 11401670 68 39-120
Indeno(1,2,3-cd)pyrene ug/kg 11801670 71 58-120
Isophorone ug/kg 9921670 60 38-120
N-Nitroso-di-n-propylamine ug/kg 10401670 62 30-120
N-Nitrosodimethylamine ug/kg 9531670 57 32-120
N-Nitrosodiphenylamine ug/kg 13201670 79 50-120
Naphthalene ug/kg 12201670 73 38-120
Nitrobenzene ug/kg 9671670 58 37-120
Pentachlorophenol ug/kg 27003330 81 10-120
Phenanthrene ug/kg 13201670 79 62-120
Phenol ug/kg 12901670 77 37-120
Pyrene ug/kg 15001670 90 63-120
2,4,6-Tribromophenol (S) % 88 27-110
2-Fluorobiphenyl (S) % 94 30-110
2-Fluorophenol (S) % 68 13-110
Nitrobenzene-d5 (S) % 61 23-110
Phenol-d6 (S) % 77 22-110
Terphenyl-d14 (S) % 80 28-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1633909MATRIX SPIKE SAMPLE:
MSSpike
Result
92280612003
1,2,4-Trichlorobenzene ug/kg 12501960 64 18-119ND
1,2-Dichlorobenzene ug/kg 12301960 63 50-110ND
1,3-Dichlorobenzene ug/kg 12001960 61 27-110ND
1,4-Dichlorobenzene ug/kg 12001960 61 28-110ND
1-Methylnaphthalene ug/kg 12501960 64 24-116ND
2,4,5-Trichlorophenol ug/kg 12001960 61 28-110ND
2,4,6-Trichlorophenol ug/kg 13001960 66 17-117ND
2,4-Dichlorophenol ug/kg 12601960 64 21-128ND
2,4-Dimethylphenol ug/kg 11401960 58 10-120ND
2,4-Dinitrophenol ug/kg 405J M19800 4 10-107ND
2,4-Dinitrotoluene ug/kg 13601960 69 36-109ND
2,6-Dinitrotoluene ug/kg 13901960 71 32-110ND
2-Chloronaphthalene ug/kg 12801960 65 30-107ND
2-Chlorophenol ug/kg 11901960 61 14-106ND
2-Methylnaphthalene ug/kg 12901960 66 10-135ND
2-Methylphenol(o-Cresol) ug/kg 10901960 55 10-124ND
2-Nitroaniline ug/kg 1890J3920 48 26-116ND
2-Nitrophenol ug/kg 11801960 60 28-103ND
3&4-Methylphenol(m&p Cresol) ug/kg 9481960 48 10-109ND
3,3'-Dichlorobenzidine ug/kg 25803920 66 10-150ND
3-Nitroaniline ug/kg 24103920 62 22-110ND
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1633909MATRIX SPIKE SAMPLE:
MSSpike
Result
92280612003
4,6-Dinitro-2-methylphenol ug/kg 8143920 21 13-121ND
4-Bromophenylphenyl ether ug/kg 13001960 66 31-109ND
4-Chloro-3-methylphenol ug/kg 28103920 72 13-128ND
4-Chloroaniline ug/kg 21103920 54 18-102ND
4-Chlorophenylphenyl ether ug/kg 13501960 69 29-112ND
4-Nitroaniline ug/kg 24503920 62 16-111ND
4-Nitrophenol ug/kg 34009800 35 14-135ND
Acenaphthene ug/kg 12301960 63 26-114ND
Acenaphthylene ug/kg 13501960 69 32-108ND
Aniline ug/kg 8561960 44 10-107ND
Anthracene ug/kg 12901960 66 32-111ND
Benzo(a)anthracene ug/kg 13301960 68 25-117ND
Benzo(a)pyrene ug/kg 11201960 57 25-106ND
Benzo(b)fluoranthene ug/kg 11801960 60 24-110ND
Benzo(g,h,i)perylene ug/kg 10601960 54 19-112ND
Benzo(k)fluoranthene ug/kg 13301960 68 24-114ND
Benzoic Acid ug/kg ND M19800 0 10-110ND
Benzyl alcohol ug/kg 21803920 56 24-106ND
bis(2-Chloroethoxy)methane ug/kg 9751960 50 13-119ND
bis(2-Chloroethyl) ether ug/kg 9741960 50 10-134ND
bis(2-Chloroisopropyl) ether ug/kg 5691960 29 10-113ND
bis(2-Ethylhexyl)phthalate ug/kg 14501960 74 10-125ND
Butylbenzylphthalate ug/kg 15101960 77 18-110ND
Chrysene ug/kg 13001960 66 30-110ND
Di-n-butylphthalate ug/kg 13901960 71 19-112ND
Di-n-octylphthalate ug/kg 17001960 87 17-105ND
Dibenz(a,h)anthracene ug/kg 10901960 56 23-111ND
Dibenzofuran ug/kg 13301960 68 35-103ND
Diethylphthalate ug/kg 13601960 70 27-113ND
Dimethylphthalate ug/kg 13901960 71 26-111ND
Fluoranthene ug/kg 12901960 66 33-109ND
Fluorene ug/kg 13301960 68 32-113ND
Hexachloro-1,3-butadiene ug/kg 11701960 60 16-116ND
Hexachlorobenzene ug/kg 14301960 73 27-120ND
Hexachlorocyclopentadiene ug/kg 6071960 31 10-108ND
Hexachloroethane ug/kg 12001960 61 10-117ND
Indeno(1,2,3-cd)pyrene ug/kg 11001960 56 10-122ND
Isophorone ug/kg 9531960 49 28-114ND
N-Nitroso-di-n-propylamine ug/kg 9771960 50 27-113ND
N-Nitrosodimethylamine ug/kg 9051960 46 10-109ND
N-Nitrosodiphenylamine ug/kg 12001960 61 10-128ND
Naphthalene ug/kg 11701960 60 25-110ND
Nitrobenzene ug/kg 9281960 47 18-114ND
Pentachlorophenol ug/kg 1430J3920 37 10-122ND
Phenanthrene ug/kg 12401960 63 30-114ND
Phenol ug/kg 11101960 57 11-102ND
Pyrene ug/kg 12901960 66 25-116ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/28/2015 04:56 PM
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Page 35 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1633909MATRIX SPIKE SAMPLE:
MSSpike
Result
92280612003
2,4,6-Tribromophenol (S) % 63 27-110
2-Fluorobiphenyl (S) % 67 30-110
2-Fluorophenol (S) % 54 13-110
Nitrobenzene-d5 (S) % 51 23-110
Phenol-d6 (S) % 59 22-110
Terphenyl-d14 (S) % 65 28-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92280612004
1633910SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND 30ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol) ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol) ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND 30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND 30ND
4-Nitrophenol ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
Aniline ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
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Page 36 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92280612004
1633910SAMPLE DUPLICATE:
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Benzoic Acid ug/kg ND 30ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Chloroisopropyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND 30ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND 30ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Phenol ug/kg ND 30ND
Pyrene ug/kg ND 30ND
2,4,6-Tribromophenol (S) % 60 362
2-Fluorobiphenyl (S) % 55 1061
2-Fluorophenol (S) % 50 2141
Nitrobenzene-d5 (S) % 49 1456
Phenol-d6 (S) % 47 1341
Terphenyl-d14 (S) % 56 459
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 12/28/2015 04:56 PM
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[phone]
Page 37 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/39886
MADEP EPH
MADEP EPH
MADEP EPH NC Soil
Associated Lab Samples: 92280538003, 92280538007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1634245
Associated Lab Samples:92280538003, 92280538007
Matrix: Solid
Analyzed
Aliphatic (C09-C18) mg/kg ND 10.0 N212/22/15 18:07
Aliphatic (C19-C36) mg/kg ND 10.0 N212/22/15 18:07
Aromatic (C11-C22) mg/kg ND 10.0 N212/22/15 18:07
2-Bromonaphthalene (S) % 87 40-140 12/22/15 18:07
2-Fluorobiphenyl (S) % 93 40-140 12/22/15 18:07
Nonatriacontane (S) % 73 40-140 12/22/15 18:07
o-Terphenyl (S) % 79 40-140 12/22/15 18:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1634246LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1634247
Aliphatic (C09-C18) mg/kg ND N210 52 40-14053ND 50
Aliphatic (C19-C36) mg/kg ND N213.3 64 40-14062ND 50
Aromatic (C11-C22) mg/kg 21.9 N228.3 77 40-1407420.9 5 50
2-Bromonaphthalene (S) % 85 40-14081
2-Fluorobiphenyl (S) % 83 40-14083
Nonatriacontane (S) % 68 40-14067
o-Terphenyl (S) % 75 40-14073
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 38 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/8675
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples: 92280538001, 92280538002, 92280538003, 92280538004, 92280538005, 92280538006, 92280538007
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92280538001
1633710SAMPLE DUPLICATE:
Percent Moisture % 9.9 5 259.5
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92280575009
1633711SAMPLE DUPLICATE:
Percent Moisture % 21.6 0 2521.5
REPORT OF LABORATORY ANALYSIS
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Page 39 of 43
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The internal standard response is below criteria. No hits associated with this internal standard. Results unaffected by
high bias.
1g
Common Laboratory Contaminant.C9
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.
L3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold TNI accreditation for this parameter.N2
Surrogate recovery outside laboratory control limits.S0
REPORT OF LABORATORY ANALYSIS
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Page 40 of 43
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92280538
FRIENDLY MRT 3055 STANTONSBURG
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92280538001 OEXT/39871 GCSV/23614X-1 EPA 3546 EPA 8015 Modified
92280538002 OEXT/39945 GCSV/23649X-2 EPA 3546 EPA 8015 Modified
92280538004 OEXT/39871 GCSV/23614N1EPA 3546 EPA 8015 Modified
92280538005 OEXT/39871 GCSV/23614N2EPA 3546 EPA 8015 Modified
92280538006 OEXT/39871 GCSV/23614N3EPA 3546 EPA 8015 Modified
92280538003 OEXT/39886 GCSV/23642EMADEP EPH MADEP EPH
92280538007 OEXT/39886 GCSV/23642WMADEP EPH MADEP EPH
92280538001 GCV/10207 GCV/10214X-1 EPA 5035A/5030B EPA 8015 Modified
92280538002 GCV/10216 GCV/10218X-2 EPA 5035A/5030B EPA 8015 Modified
92280538004 GCV/10207 GCV/10214N1EPA 5035A/5030B EPA 8015 Modified
92280538005 GCV/10207 GCV/10214N2EPA 5035A/5030B EPA 8015 Modified
92280538006 GCV/10207 GCV/10214N3EPA 5035A/5030B EPA 8015 Modified
92280538003 GCV/10205 GCV/10208EMADEP VPH MADEP VPH
92280538007 GCV/10205 GCV/10208WMADEP VPH MADEP VPH
92280538003 OEXT/39866 MSSV/11680EEPA 3546 EPA 8270
92280538007 OEXT/39866 MSSV/11680WEPA 3546 EPA 8270
92280538003 MSV/34861EEPA 8260
92280538007 MSV/34861WEPA 8260
92280538001 PMST/8675X-1 ASTM D2974-87
92280538002 PMST/8675X-2 ASTM D2974-87
92280538003 PMST/8675EASTM D2974-87
92280538004 PMST/8675N1ASTM D2974-87
92280538005 PMST/8675N2ASTM D2974-87
92280538006 PMST/8675N3ASTM D2974-87
92280538007 PMST/8675WASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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Page 41 of 43
Page 42 of 43
Page 43 of 43
#=CL#
February 17, 2016
LIMS USE: FR - HENRY NEMARGUT
LIMS OBJECT ID: 92284631
92284631
Project:
Pace Project No.:
RE:
Henry Nemargut
Henry Nemargut Engineering
2211 Chestnut Street
Wilmington, NC 28405
FRIENDLY MART 3055 STANSBURG
Dear Henry Nemargut:
Enclosed are the analytical results for sample(s) received by the laboratory on January 29, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Report revised 2/17/16 to update a diltuon error for 602 by 6200B.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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Page 1 of 21
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92284631
FRIENDLY MART 3055 STANSBURG
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 2 of 21
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92284631
FRIENDLY MART 3055 STANSBURG
Lab ID Sample ID Matrix Date Collected Date Received
92284631001 MW-1 Water 01/28/16 16:20 01/29/16 09:45
REPORT OF LABORATORY ANALYSIS
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Page 3 of 21
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92284631
FRIENDLY MART 3055 STANSBURG
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92284631001 MW-1 MADEP EPH 7 PASI-CBJL
MADEP VPH 5 PASI-CZDO
EPA 625 67 PASI-CBPJ
SM 6200B 16 PASI-CCAH
REPORT OF LABORATORY ANALYSIS
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Page 4 of 21
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92284631
FRIENDLY MART 3055 STANSBURG
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92284631001 MW-1
Aliphatic (C09-C18) 106 ug/L 02/03/16 22:08 N2100MADEP EPH
Aliphatic (C05-C08) 330 ug/L 02/03/16 01:52 N250.0MADEP VPH
Aliphatic (C09-C12) 584 ug/L 02/03/16 01:52 N250.0MADEP VPH
Aromatic (C09-C10) 508 ug/L 02/03/16 01:52 N250.0MADEP VPH
Naphthalene 8.0 ug/L 02/03/16 02:075.0EPA 625
4.094:2-Butanol, 2,3-dimethyl- 43.4 ug/L 02/03/16 02:07 NEPA 625
5.965:o-Xylene 25.5 ug/L 02/03/16 02:07 NEPA 625
6.263:Benzene, (1-methylethyl) 39.9 ug/L 02/03/16 02:07 NEPA 625
6.757:Benzene, 1-ethyl-3-methy 25.8 ug/L 02/03/16 02:07 NEPA 625
6.891:1,2,4-Trimethylbenzene 64.8 ug/L 02/03/16 02:07 NEPA 625
7.205:Unknown 32.3 ug/L 02/03/16 02:07 NEPA 625
8.066:Benzene, 2-ethenyl-1,4-d 12.3 ug/L 02/03/16 02:07 NEPA 625
10.387:Unknown 13.7 ug/L 02/03/16 02:07 NEPA 625
12.063:n-Hexadecanoic acid 34.4 ug/L 02/03/16 02:07 NEPA 625
Benzene 37.9 ug/L 02/09/16 14:181.0SM 6200B
Ethylbenzene 64.5 ug/L 02/09/16 14:181.0SM 6200B
Isopropylbenzene (Cumene) 124 ug/L 02/09/16 14:181.0SM 6200B
Methyl-tert-butyl ether 6.4 ug/L 02/09/16 14:181.0SM 6200B
Naphthalene 21.8 ug/L 02/09/16 14:182.0SM 6200B
Toluene 4.1 ug/L 02/09/16 14:181.0SM 6200B
m&p-Xylene 5.2 ug/L 02/09/16 14:182.0SM 6200B
o-Xylene 33.4 ug/L 02/09/16 14:181.0SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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Huntersville, NC 28078
[phone]
Page 5 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284631
FRIENDLY MART 3055 STANSBURG
Sample: MW-1 Lab ID: 92284631001 Collected: 01/28/16 16:20 Received: 01/29/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Water
Aliphatic (C09-C18)106 ug/L 02/03/16 22:08 N201/29/16 13:30100 1
Aliphatic (C19-C36) ND ug/L 02/03/16 22:08 N201/29/16 13:30100 1
Aromatic (C11-C22) ND ug/L 02/03/16 22:08 N201/29/16 13:30100 1
Surrogates
Nonatriacontane (S) 66 % 02/03/16 22:08 7194-86-701/29/16 13:3040-140 1
o-Terphenyl (S) 69 % 02/03/16 22:08 84-15-101/29/16 13:3040-140 1
2-Fluorobiphenyl (S) 85 % 02/03/16 22:08 321-60-801/29/16 13:3040-140 1
2-Bromonaphthalene (S) 84 % 02/03/16 22:08 580-13-201/29/16 13:3040-140 1
Analytical Method: MADEP VPHVPH NC Water
Aliphatic (C05-C08)330 ug/L 02/03/16 01:52 N250.0 1
Aliphatic (C09-C12)584 ug/L 02/03/16 01:52 N250.0 1
Aromatic (C09-C10)508 ug/L 02/03/16 01:52 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S) 94 % 02/03/16 01:52 460-00-470-130 1
4-Bromofluorobenzene (PID) (S) 95 % 02/03/16 01:52 460-00-470-130 1
Analytical Method: EPA 625 Preparation Method: EPA 625625 MSSV
Acenaphthene ND ug/L 02/03/16 02:07 83-32-902/02/16 09:055.0 1
Acenaphthylene ND ug/L 02/03/16 02:07 208-96-802/02/16 09:055.0 1
Anthracene ND ug/L 02/03/16 02:07 120-12-702/02/16 09:055.0 1
Benzo(a)anthracene ND ug/L 02/03/16 02:07 56-55-302/02/16 09:055.0 1
Benzo(a)pyrene ND ug/L 02/03/16 02:07 50-32-802/02/16 09:055.0 1
Benzo(b)fluoranthene ND ug/L 02/03/16 02:07 205-99-202/02/16 09:055.0 1
Benzo(g,h,i)perylene ND ug/L 02/03/16 02:07 191-24-202/02/16 09:055.0 1
Benzo(k)fluoranthene ND ug/L 02/03/16 02:07 207-08-902/02/16 09:055.0 1
4-Bromophenylphenyl ether ND ug/L 02/03/16 02:07 101-55-302/02/16 09:055.0 1
Butylbenzylphthalate ND ug/L 02/03/16 02:07 85-68-702/02/16 09:055.0 1
4-Chloro-3-methylphenol ND ug/L 02/03/16 02:07 59-50-702/02/16 09:055.0 1
bis(2-Chloroethoxy)methane ND ug/L 02/03/16 02:07 111-91-102/02/16 09:0510.0 1
bis(2-Chloroethyl) ether ND ug/L 02/03/16 02:07 111-44-402/02/16 09:055.0 1
bis(2-Chloroisopropyl) ether ND ug/L 02/03/16 02:07 108-60-102/02/16 09:055.0 1
2-Chloronaphthalene ND ug/L 02/03/16 02:07 91-58-702/02/16 09:055.0 1
2-Chlorophenol ND ug/L 02/03/16 02:07 95-57-802/02/16 09:055.0 1
4-Chlorophenylphenyl ether ND ug/L 02/03/16 02:07 7005-72-302/02/16 09:055.0 1
Chrysene ND ug/L 02/03/16 02:07 218-01-902/02/16 09:055.0 1
Dibenz(a,h)anthracene ND ug/L 02/03/16 02:07 53-70-302/02/16 09:055.0 1
3,3'-Dichlorobenzidine ND ug/L 02/03/16 02:07 91-94-102/02/16 09:0525.0 1
2,4-Dichlorophenol ND ug/L 02/03/16 02:07 120-83-202/02/16 09:055.0 1
Diethylphthalate ND ug/L 02/03/16 02:07 84-66-202/02/16 09:055.0 1
2,4-Dimethylphenol ND ug/L 02/03/16 02:07 105-67-902/02/16 09:0510.0 1
Dimethylphthalate ND ug/L 02/03/16 02:07 131-11-302/02/16 09:055.0 1
Di-n-butylphthalate ND ug/L 02/03/16 02:07 84-74-202/02/16 09:055.0 1
4,6-Dinitro-2-methylphenol ND ug/L 02/03/16 02:07 534-52-102/02/16 09:0520.0 1
2,4-Dinitrophenol ND ug/L 02/03/16 02:07 51-28-502/02/16 09:0550.0 1
2,4-Dinitrotoluene ND ug/L 02/03/16 02:07 121-14-202/02/16 09:055.0 1
2,6-Dinitrotoluene ND ug/L 02/03/16 02:07 606-20-202/02/16 09:055.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/17/2016 10:55 AM
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Page 6 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284631
FRIENDLY MART 3055 STANSBURG
Sample: MW-1 Lab ID: 92284631001 Collected: 01/28/16 16:20 Received: 01/29/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 625 Preparation Method: EPA 625625 MSSV
Di-n-octylphthalate ND ug/L 02/03/16 02:07 117-84-002/02/16 09:055.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 02/03/16 02:07 117-81-702/02/16 09:055.0 1
Fluoranthene ND ug/L 02/03/16 02:07 206-44-002/02/16 09:055.0 1
Fluorene ND ug/L 02/03/16 02:07 86-73-702/02/16 09:055.0 1
Hexachloro-1,3-butadiene ND ug/L 02/03/16 02:07 87-68-302/02/16 09:055.0 1
Hexachlorobenzene ND ug/L 02/03/16 02:07 118-74-102/02/16 09:055.0 1
Hexachlorocyclopentadiene ND ug/L 02/03/16 02:07 77-47-402/02/16 09:0510.0 1
Hexachloroethane ND ug/L 02/03/16 02:07 67-72-102/02/16 09:055.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 02/03/16 02:07 193-39-502/02/16 09:055.0 1
Isophorone ND ug/L 02/03/16 02:07 78-59-102/02/16 09:0510.0 1
Naphthalene 8.0 ug/L 02/03/16 02:07 91-20-302/02/16 09:055.0 1
Nitrobenzene ND ug/L 02/03/16 02:07 98-95-302/02/16 09:055.0 1
2-Nitrophenol ND ug/L 02/03/16 02:07 88-75-502/02/16 09:055.0 1
4-Nitrophenol ND ug/L 02/03/16 02:07 100-02-702/02/16 09:0550.0 1
N-Nitrosodimethylamine ND ug/L 02/03/16 02:07 62-75-902/02/16 09:055.0 1
N-Nitroso-di-n-propylamine ND ug/L 02/03/16 02:07 621-64-702/02/16 09:055.0 1
N-Nitrosodiphenylamine ND ug/L 02/03/16 02:07 86-30-602/02/16 09:0510.0 1
Pentachlorophenol ND ug/L 02/03/16 02:07 87-86-502/02/16 09:0510.0 1
Phenanthrene ND ug/L 02/03/16 02:07 85-01-802/02/16 09:055.0 1
Phenol ND ug/L 02/03/16 02:07 108-95-202/02/16 09:055.0 1
Pyrene ND ug/L 02/03/16 02:07 129-00-002/02/16 09:055.0 1
1,2,4-Trichlorobenzene ND ug/L 02/03/16 02:07 120-82-102/02/16 09:055.0 1
2,4,6-Trichlorophenol ND ug/L 02/03/16 02:07 88-06-202/02/16 09:0510.0 1
Surrogates
Nitrobenzene-d5 (S) 78 % 02/03/16 02:07 4165-60-002/02/16 09:0510-120 1
2-Fluorobiphenyl (S) 75 % 02/03/16 02:07 321-60-802/02/16 09:0515-120 1
Terphenyl-d14 (S) 81 % 02/03/16 02:07 1718-51-002/02/16 09:0511-131 1
Phenol-d6 (S) 36 % 02/03/16 02:07 13127-88-302/02/16 09:0510-120 1
2-Fluorophenol (S) 45 % 02/03/16 02:07 367-12-402/02/16 09:0510-120 1
2,4,6-Tribromophenol (S) 93 % 02/03/16 02:07 118-79-602/02/16 09:0510-137 1
Tentatively Identified Compounds
2-Butanol, 2,3-dimethyl-43.4 ug/L 02/03/16 02:07 594-60-5 N02/02/16 09:051
o-Xylene 25.5 ug/L 02/03/16 02:07 95-47-6 N02/02/16 09:051
Benzene, (1-methylethyl)39.9 ug/L 02/03/16 02:07 98-82-8 N02/02/16 09:051
Benzene, 1-ethyl-3-methy 25.8 ug/L 02/03/16 02:07 620-14-4 N02/02/16 09:051
1,2,4-Trimethylbenzene 64.8 ug/L 02/03/16 02:07 95-36-3 N02/02/16 09:051
Unknown 32.3 ug/L 02/03/16 02:07 N02/02/16 09:051
Benzene, 2-ethenyl-1,4-d 12.3 ug/L 02/03/16 02:07 2039-89-6 N02/02/16 09:051
Unknown 13.7 ug/L 02/03/16 02:07 N02/02/16 09:051
n-Hexadecanoic acid 34.4 ug/L 02/03/16 02:07 57-10-3 N02/02/16 09:051
Analytical Method: SM 6200B602 Volatiles by Method 6200
Benzene 37.9 ug/L 02/09/16 14:18 71-43-21.0 1
Chlorobenzene ND ug/L 02/09/16 14:18 108-90-71.0 1
1,2-Dichlorobenzene ND ug/L 02/09/16 14:18 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 02/09/16 14:18 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 02/09/16 14:18 106-46-71.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/17/2016 10:55 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284631
FRIENDLY MART 3055 STANSBURG
Sample: MW-1 Lab ID: 92284631001 Collected: 01/28/16 16:20 Received: 01/29/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B602 Volatiles by Method 6200
Diisopropyl ether ND ug/L 02/09/16 14:18 108-20-31.0 1
Ethylbenzene 64.5 ug/L 02/09/16 14:18 100-41-41.0 1
Isopropylbenzene (Cumene)124 ug/L 02/09/16 14:18 98-82-81.0 1
Methyl-tert-butyl ether 6.4 ug/L 02/09/16 14:18 1634-04-41.0 1
Naphthalene 21.8 ug/L 02/09/16 14:18 91-20-32.0 1
Toluene 4.1 ug/L 02/09/16 14:18 108-88-31.0 1
m&p-Xylene 5.2 ug/L 02/09/16 14:18 179601-23-12.0 1
o-Xylene 33.4 ug/L 02/09/16 14:18 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S) 99 % 02/09/16 14:18 460-00-470-130 1
1,2-Dichloroethane-d4 (S) 114 % 02/09/16 14:18 17060-07-070-130 1
Toluene-d8 (S) 105 % 02/09/16 14:18 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/17/2016 10:55 AM
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9800 Kincey Ave. Suite 100
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[phone]
Page 8 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92284631
FRIENDLY MART 3055 STANSBURG
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/10302
MADEP VPH
MADEP VPH
VPH NC Water
Associated Lab Samples: 92284631001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1658191
Associated Lab Samples:92284631001
Matrix: Water
Analyzed
Aliphatic (C05-C08) ug/L ND 50.0 N202/02/16 17:50
Aliphatic (C09-C12) ug/L ND 50.0 N202/02/16 17:50
Aromatic (C09-C10) ug/L ND 50.0 N202/02/16 17:50
4-Bromofluorobenzene (FID) (S) % 95 70-130 02/02/16 17:50
4-Bromofluorobenzene (PID) (S) % 95 70-130 02/02/16 17:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1658192LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1658193
Aliphatic (C05-C08) ug/L 271 N2300 90 70-13089267 1 25
Aliphatic (C09-C12) ug/L 305 N2300 102 30-130107321 5 25
Aromatic (C09-C10) ug/L 106 N2100 106 70-130104104 1 25
4-Bromofluorobenzene (FID) (S) % 100 70-130105
4-Bromofluorobenzene (PID) (S) % 101 70-130107
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/17/2016 10:55 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92284631
FRIENDLY MART 3055 STANSBURG
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/35452
SM 6200B
SM 6200B
602 by 6200B
Associated Lab Samples: 92284631001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1660482
Associated Lab Samples:92284631001
Matrix: Water
Analyzed
1,2-Dichloroethane-d4 (S) % 107 70-130 02/09/16 13:27
4-Bromofluorobenzene (S) % 99 70-130 02/09/16 13:27
Toluene-d8 (S) % 103 70-130 02/09/16 13:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1660483LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloroethane-d4 (S) % 101 70-130
4-Bromofluorobenzene (S) % 98 70-130
Toluene-d8 (S) % 102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/17/2016 10:55 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92284631
FRIENDLY MART 3055 STANSBURG
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/40542
EPA 625
EPA 625
625 MSS
Associated Lab Samples: 92284631001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1657919
Associated Lab Samples:92284631001
Matrix: Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 5.0 02/03/16 08:16
2,4,6-Trichlorophenol ug/L ND 10.0 02/03/16 08:16
2,4-Dichlorophenol ug/L ND 5.0 02/03/16 08:16
2,4-Dimethylphenol ug/L ND 10.0 02/03/16 08:16
2,4-Dinitrophenol ug/L ND 50.0 02/03/16 08:16
2,4-Dinitrotoluene ug/L ND 5.0 02/03/16 08:16
2,6-Dinitrotoluene ug/L ND 5.0 02/03/16 08:16
2-Chloronaphthalene ug/L ND 5.0 02/03/16 08:16
2-Chlorophenol ug/L ND 5.0 02/03/16 08:16
2-Nitrophenol ug/L ND 5.0 02/03/16 08:16
3,3'-Dichlorobenzidine ug/L ND 25.0 02/03/16 08:16
4,6-Dinitro-2-methylphenol ug/L ND 20.0 02/03/16 08:16
4-Bromophenylphenyl ether ug/L ND 5.0 02/03/16 08:16
4-Chloro-3-methylphenol ug/L ND 5.0 02/03/16 08:16
4-Chlorophenylphenyl ether ug/L ND 5.0 02/03/16 08:16
4-Nitrophenol ug/L ND 50.0 02/03/16 08:16
Acenaphthene ug/L ND 5.0 02/03/16 08:16
Acenaphthylene ug/L ND 5.0 02/03/16 08:16
Anthracene ug/L ND 5.0 02/03/16 08:16
Benzo(a)anthracene ug/L ND 5.0 02/03/16 08:16
Benzo(a)pyrene ug/L ND 5.0 02/03/16 08:16
Benzo(b)fluoranthene ug/L ND 5.0 02/03/16 08:16
Benzo(g,h,i)perylene ug/L ND 5.0 02/03/16 08:16
Benzo(k)fluoranthene ug/L ND 5.0 02/03/16 08:16
bis(2-Chloroethoxy)methane ug/L ND 10.0 02/03/16 08:16
bis(2-Chloroethyl) ether ug/L ND 5.0 02/03/16 08:16
bis(2-Chloroisopropyl) ether ug/L ND 5.0 02/03/16 08:16
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 02/03/16 08:16
Butylbenzylphthalate ug/L ND 5.0 02/03/16 08:16
Chrysene ug/L ND 5.0 02/03/16 08:16
Di-n-butylphthalate ug/L ND 5.0 02/03/16 08:16
Di-n-octylphthalate ug/L ND 5.0 02/03/16 08:16
Dibenz(a,h)anthracene ug/L ND 5.0 02/03/16 08:16
Diethylphthalate ug/L ND 5.0 02/03/16 08:16
Dimethylphthalate ug/L ND 5.0 02/03/16 08:16
Fluoranthene ug/L ND 5.0 02/03/16 08:16
Fluorene ug/L ND 5.0 02/03/16 08:16
Hexachloro-1,3-butadiene ug/L ND 5.0 02/03/16 08:16
Hexachlorobenzene ug/L ND 5.0 02/03/16 08:16
Hexachlorocyclopentadiene ug/L ND 10.0 02/03/16 08:16
Hexachloroethane ug/L ND 5.0 02/03/16 08:16
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/17/2016 10:55 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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[phone]
Page 11 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92284631
FRIENDLY MART 3055 STANSBURG
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1657919
Associated Lab Samples:92284631001
Matrix: Water
Analyzed
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 02/03/16 08:16
Isophorone ug/L ND 10.0 02/03/16 08:16
N-Nitroso-di-n-propylamine ug/L ND 5.0 02/03/16 08:16
N-Nitrosodimethylamine ug/L ND 5.0 02/03/16 08:16
N-Nitrosodiphenylamine ug/L ND 10.0 02/03/16 08:16
Naphthalene ug/L ND 5.0 02/03/16 08:16
Nitrobenzene ug/L ND 5.0 02/03/16 08:16
Pentachlorophenol ug/L ND 10.0 02/03/16 08:16
Phenanthrene ug/L ND 5.0 02/03/16 08:16
Phenol ug/L ND 5.0 02/03/16 08:16
Pyrene ug/L ND 5.0 02/03/16 08:16
2,4,6-Tribromophenol (S) % 87 10-137 02/03/16 08:16
2-Fluorobiphenyl (S) % 75 15-120 02/03/16 08:16
2-Fluorophenol (S) % 43 10-120 02/03/16 08:16
Nitrobenzene-d5 (S) % 76 10-120 02/03/16 08:16
Phenol-d6 (S) % 31 10-120 02/03/16 08:16
Terphenyl-d14 (S) % 101 11-131 02/03/16 08:16
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1657920LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 36.350 73 44-142
2,4,6-Trichlorophenol ug/L 49.850 100 37-144
2,4-Dichlorophenol ug/L 46.650 93 1-191
2,4-Dimethylphenol ug/L 43.950 88 32-119
2,4-Dinitrophenol ug/L 267250 107 1-181
2,4-Dinitrotoluene ug/L 51.250 102 39-139
2,6-Dinitrotoluene ug/L 51.150 102 50-158
2-Chloronaphthalene ug/L 42.350 85 60-118
2-Chlorophenol ug/L 46.350 93 23-134
2-Nitrophenol ug/L 44.050 88 29-182
3,3'-Dichlorobenzidine ug/L 101100 101 1-262
4,6-Dinitro-2-methylphenol ug/L 104100 104 1-181
4-Bromophenylphenyl ether ug/L 48.950 98 53-127
4-Chloro-3-methylphenol ug/L 98.7100 99 22-147
4-Chlorophenylphenyl ether ug/L 47.950 96 25-158
4-Nitrophenol ug/L 94.0250 38 1-132
Acenaphthene ug/L 44.450 89 47-145
Acenaphthylene ug/L 44.550 89 33-145
Anthracene ug/L 50.550 101 1-166
Benzo(a)anthracene ug/L 53.150 106 33-143
Benzo(a)pyrene ug/L 53.650 107 17-163
Benzo(b)fluoranthene ug/L 52.050 104 24-159
Benzo(g,h,i)perylene ug/L 50.750 101 1-219
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/17/2016 10:55 AM
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Page 12 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92284631
FRIENDLY MART 3055 STANSBURG
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1657920LABORATORY CONTROL SAMPLE:
LCSSpike
Benzo(k)fluoranthene ug/L 50.350 101 11-162
bis(2-Chloroethoxy)methane ug/L 40.450 81 33-184
bis(2-Chloroethyl) ether ug/L 43.850 88 12-158
bis(2-Chloroisopropyl) ether ug/L 30.350 61 36-166
bis(2-Ethylhexyl)phthalate ug/L 54.950 110 8-158
Butylbenzylphthalate ug/L 53.950 108 1-152
Chrysene ug/L 52.450 105 17-168
Di-n-butylphthalate ug/L 51.150 102 1-118
Di-n-octylphthalate ug/L 56.250 112 4-146
Dibenz(a,h)anthracene ug/L 54.250 108 1-227
Diethylphthalate ug/L 47.950 96 1-114
Dimethylphthalate ug/L 47.150 94 1-112
Fluoranthene ug/L 50.450 101 26-137
Fluorene ug/L 49.950 100 59-121
Hexachloro-1,3-butadiene ug/L 33.550 67 24-116
Hexachlorobenzene ug/L 49.350 99 1-152
Hexachlorocyclopentadiene ug/L 31.650 63 25-150
Hexachloroethane ug/L 33.350 67 40-113
Indeno(1,2,3-cd)pyrene ug/L 56.250 112 1-171
Isophorone ug/L 41.550 83 21-196
N-Nitroso-di-n-propylamine ug/L 46.550 93 1-230
N-Nitrosodimethylamine ug/L 25.450 51 25-150
N-Nitrosodiphenylamine ug/L 43.950 88 25-150
Naphthalene ug/L 37.750 75 21-133
Nitrobenzene ug/L 38.450 77 35-180
Pentachlorophenol ug/L 109100 109 14-176
Phenanthrene ug/L 47.450 95 54-120
Phenol ug/L 20.350 41 5-112
Pyrene ug/L 49.550 99 52-115
2,4,6-Tribromophenol (S) % 103 10-137
2-Fluorobiphenyl (S) % 80 15-120
2-Fluorophenol (S) % 48 10-120
Nitrobenzene-d5 (S) % 78 10-120
Phenol-d6 (S) % 38 10-120
Terphenyl-d14 (S) % 101 11-131
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1657921MATRIX SPIKE SAMPLE:
MSSpike
Result
92284602001
1,2,4-Trichlorobenzene ug/L 36.550 73 44-142ND
2,4,6-Trichlorophenol ug/L 47.450 95 37-144ND
2,4-Dichlorophenol ug/L 39.750 79 1-191ND
2,4-Dimethylphenol ug/L 37.050 74 32-119ND
2,4-Dinitrophenol ug/L 260250 104 1-181ND
2,4-Dinitrotoluene ug/L 51.950 104 39-139ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/17/2016 10:55 AM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
[phone]
Page 13 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92284631
FRIENDLY MART 3055 STANSBURG
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1657921MATRIX SPIKE SAMPLE:
MSSpike
Result
92284602001
2,6-Dinitrotoluene ug/L 47.050 94 50-158ND
2-Chloronaphthalene ug/L 40.250 80 60-118ND
2-Chlorophenol ug/L 36.050 72 23-134ND
2-Nitrophenol ug/L 40.150 80 29-182ND
3,3'-Dichlorobenzidine ug/L 98.8100 99 1-262ND
4,6-Dinitro-2-methylphenol ug/L 93.7100 94 1-181ND
4-Bromophenylphenyl ether ug/L 43.550 87 53-127ND
4-Chloro-3-methylphenol ug/L 84.7100 85 22-147ND
4-Chlorophenylphenyl ether ug/L 45.750 91 25-158ND
4-Nitrophenol ug/L 116250 47 1-132ND
Acenaphthene ug/L 41.650 83 47-145ND
Acenaphthylene ug/L 41.650 83 33-145ND
Anthracene ug/L 48.750 97 1-166ND
Benzo(a)anthracene ug/L 50.150 100 33-143ND
Benzo(a)pyrene ug/L 51.250 102 17-163ND
Benzo(b)fluoranthene ug/L 48.450 97 24-159ND
Benzo(g,h,i)perylene ug/L 52.850 106 1-219ND
Benzo(k)fluoranthene ug/L 46.950 94 11-162ND
bis(2-Chloroethoxy)methane ug/L 36.250 72 33-184ND
bis(2-Chloroethyl) ether ug/L 38.150 76 12-158ND
bis(2-Chloroisopropyl) ether ug/L 24.850 50 36-166ND
bis(2-Ethylhexyl)phthalate ug/L 50.950 102 8-158ND
Butylbenzylphthalate ug/L 50.150 100 1-152ND
Chrysene ug/L 50.050 100 17-168ND
Di-n-butylphthalate ug/L 51.050 102 1-118ND
Di-n-octylphthalate ug/L 57.250 114 4-146ND
Dibenz(a,h)anthracene ug/L 57.450 115 1-227ND
Diethylphthalate ug/L 47.650 95 1-114ND
Dimethylphthalate ug/L 44.750 89 1-112ND
Fluoranthene ug/L 55.250 110 26-137ND
Fluorene ug/L 48.350 97 59-121ND
Hexachloro-1,3-butadiene ug/L 36.050 72 24-116ND
Hexachlorobenzene ug/L 42.050 84 1-152ND
Hexachlorocyclopentadiene ug/L 33.150 66 25-150ND
Hexachloroethane ug/L 31.050 62 40-113ND
Indeno(1,2,3-cd)pyrene ug/L 57.850 116 1-171ND
Isophorone ug/L 36.050 72 21-196ND
N-Nitroso-di-n-propylamine ug/L 34.150 68 1-230ND
N-Nitrosodimethylamine ug/L 22.850 46 25-150ND
N-Nitrosodiphenylamine ug/L 38.750 77 25-150ND
Naphthalene ug/L 35.850 72 21-133ND
Nitrobenzene ug/L 36.250 72 35-180ND
Pentachlorophenol ug/L 108100 108 14-176ND
Phenanthrene ug/L 45.850 92 54-120ND
Phenol ug/L 14.350 29 5-112ND
Pyrene ug/L 41.350 83 52-115ND
2,4,6-Tribromophenol (S) % 97 10-137
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/17/2016 10:55 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92284631
FRIENDLY MART 3055 STANSBURG
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1657921MATRIX SPIKE SAMPLE:
MSSpike
Result
92284602001
2-Fluorobiphenyl (S) % 77 15-120
2-Fluorophenol (S) % 40 10-120
Nitrobenzene-d5 (S) % 73 10-120
Phenol-d6 (S) % 26 10-120
Terphenyl-d14 (S) % 65 11-131
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92284622001
1657922SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/L ND 30ND
2,4,6-Trichlorophenol ug/L ND 30ND
2,4-Dichlorophenol ug/L ND 30ND
2,4-Dimethylphenol ug/L ND 30ND
2,4-Dinitrophenol ug/L ND 30ND
2,4-Dinitrotoluene ug/L ND 30ND
2,6-Dinitrotoluene ug/L ND 30ND
2-Chloronaphthalene ug/L ND 30ND
2-Chlorophenol ug/L ND 30ND
2-Nitrophenol ug/L ND 30ND
3,3'-Dichlorobenzidine ug/L ND 30ND
4,6-Dinitro-2-methylphenol ug/L ND 30ND
4-Bromophenylphenyl ether ug/L ND 30ND
4-Chloro-3-methylphenol ug/L ND 30ND
4-Chlorophenylphenyl ether ug/L ND 30ND
4-Nitrophenol ug/L ND 30ND
Acenaphthene ug/L ND 30ND
Acenaphthylene ug/L ND 30ND
Anthracene ug/L ND 30ND
Benzo(a)anthracene ug/L ND 30ND
Benzo(a)pyrene ug/L ND 30ND
Benzo(b)fluoranthene ug/L ND 30ND
Benzo(g,h,i)perylene ug/L ND 30ND
Benzo(k)fluoranthene ug/L ND 30ND
bis(2-Chloroethoxy)methane ug/L ND 30ND
bis(2-Chloroethyl) ether ug/L ND 30ND
bis(2-Chloroisopropyl) ether ug/L ND 30ND
bis(2-Ethylhexyl)phthalate ug/L 2J 30ND
Butylbenzylphthalate ug/L ND 30ND
Chrysene ug/L ND 30ND
Di-n-butylphthalate ug/L ND 30ND
Di-n-octylphthalate ug/L ND 30ND
Dibenz(a,h)anthracene ug/L ND 30ND
Diethylphthalate ug/L ND 30ND
Dimethylphthalate ug/L ND 30ND
Fluoranthene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/17/2016 10:55 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92284631
FRIENDLY MART 3055 STANSBURG
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92284622001
1657922SAMPLE DUPLICATE:
Fluorene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
Hexachlorobenzene ug/L ND 30ND
Hexachlorocyclopentadiene ug/L ND 30ND
Hexachloroethane ug/L ND 30ND
Indeno(1,2,3-cd)pyrene ug/L ND 30ND
Isophorone ug/L ND 30ND
N-Nitroso-di-n-propylamine ug/L ND 30ND
N-Nitrosodimethylamine ug/L ND 30ND
N-Nitrosodiphenylamine ug/L ND 30ND
Naphthalene ug/L ND 30ND
Nitrobenzene ug/L ND 30ND
Pentachlorophenol ug/L ND 30ND
Phenanthrene ug/L ND 30ND
Phenol ug/L ND 30ND
Pyrene ug/L ND 30ND
2,4,6-Tribromophenol (S) % 21 520
2-Fluorobiphenyl (S) % 38 339
2-Fluorophenol (S) % 0 S00
Nitrobenzene-d5 (S) % 38 339
Phenol-d6 (S) % 0 S00
Terphenyl-d14 (S) % 78 1170
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/17/2016 10:55 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92284631
FRIENDLY MART 3055 STANSBURG
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/40495
MADEP EPH
MADEP EPH
MADEP EPH NC Water
Associated Lab Samples: 92284631001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1656750
Associated Lab Samples:92284631001
Matrix: Water
Analyzed
Aliphatic (C09-C18) ug/L ND 100 N202/04/16 16:25
Aliphatic (C19-C36) ug/L ND 100 N202/04/16 16:25
Aromatic (C11-C22) ug/L ND 100 N202/03/16 14:54
2-Bromonaphthalene (S) % 85 40-140 02/03/16 14:54
2-Fluorobiphenyl (S) % 86 40-140 02/03/16 14:54
Nonatriacontane (S) % 83 40-140 02/04/16 16:25
o-Terphenyl (S) % 82 40-140 02/03/16 14:54
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1656751LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1656752
Aliphatic (C09-C18) ug/L 156 N2300 52 40-14062186 17 50
Aliphatic (C19-C36) ug/L 235 N2400 59 40-14068273 15 50
Aromatic (C11-C22) ug/L 689 N2850 81 40-14077651 6 50
2-Bromonaphthalene (S) % 88 40-14085
2-Fluorobiphenyl (S) % 87 40-14087
Nonatriacontane (S) % 67 40-14077
o-Terphenyl (S) % 83 40-14078
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/17/2016 10:55 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 21
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92284631
FRIENDLY MART 3055 STANSBURG
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Tentatively identified compound (TIC) based on mass spectral library search. Result is estimated.N
The lab does not hold TNI accreditation for this parameter.N2
Surrogate recovery outside laboratory control limits.S0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/17/2016 10:55 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 21
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92284631
FRIENDLY MART 3055 STANSBURG
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92284631001 OEXT/40495 GCSV/23992MW-1 MADEP EPH MADEP EPH
92284631001 GCV/10302MW-1 MADEP VPH
92284631001 OEXT/40542 MSSV/11830MW-1 EPA 625 EPA 625
92284631001 MSV/35452MW-1 SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/17/2016 10:55 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 21
Page 20 of 21
Page 21 of 21

APPENDIX F

TANK DISPOSAL MANIFEST

APPENDIX G

WELL CONSTRUCTION RECORD

3426
Henry Nemargut
Henry Nemargut Engineering Services
2211 Chestnut Street
Wilmington NC 28405
910 762-5475
MW-1
X
1/22/2016
5:30 X
Wilson Wilson
3055 Stantonsburg Rd, Wilson, NC 27893
X
35.69099167
77.88775
XX
0-024589
Friendly Mart
3055 Stantonsburg Road
Wilson NC 27893
Raymond Bartholomew
P.O. Box 706
Henderson NC 27536
252 438-7141
13.75'
X
4.57'
0'
0'3.75'2"Sch 40 PVC
0' 3'Portland Pour
3.75'13.75'2 0.01 PVC
3'14'#2 Filter Sand
0' 1'gray, Gravel (ABC)
1' 13'orange-tan brown, Silt w/clay and sand (backfill)
13' 14'gray-tan, Silt w/sand and clay
4/12/2016