RA-7781_39876_CA_CSA_20161231

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COMPREHENSIVE SITE ASSESSMENT

DECEMBER 31, 2016

FRIENDLY MART
3055 Stantonsburg Road
Wilson, Wilson County, NC 27603
Facility ID #: 0-024589; UST Incident #: 39876
LATITUDE: N 35.69099167o; LONGITUDE: W 77.88775o (From GPS)
UST OWNER:
Rose Oil Company, Inc., 613 US 158 Bypass, Henderson, NC 27537-6825
Phone Number: [phone]
PROPERTY OWNER & OCCUPANT:
Owner: SMW, Inc. – Occupant: Rose Oil Company, Inc., 613 US 158 Bypass
Henderson, NC 27537; Phone Number: [phone]

CONSULTANT:
Henry Nemargut Engineering Services, 2211 Chestnut Street, Wilmington, NC 28405
Phone Number: [phone]
LABORATORY: Pace Analytical Services, Inc., 9800 Kincey Ave, Suite 100, Huntersville, NC 28078 Phone Number: [phone]; State Certification #12
RELEASE INFORMATION: Date Discovered: 12/17/15 Estimated Quantity of Release: Unknown; Cause of Release: Corrosion + Unknown Source of Release: UST System; Size and Contents: (1) 4,000 Gallon Diesel UST (2) 6,000 Gallon & (1) 4,000 Gallon Gasoline USTs

The Comprehensive Site Assessment Report for this site has been prepared by Henry Nemargut
Engineering Services under the direct supervision of licensed engineers or geologists. Technical
review of this document has been provided by Henry Nemargut, P.E. All engineering work
performed on this project was conducted under my direct supervision:
Henry Nemargut, P.E.
North Carolina License #17669
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B. EXECUTIVE SUMMARY

1. Source Information

Type: Low boiling point hydrocarbons in the form of gasoline
Containers: (2) 6000 & (1) 4,000 gallon gas; (1) 4,000 diesel USTs
Amount: Unknown; Source: Leaking UST system

2. Initial Abatement Information

Soil Removal: Approximately 1190 tons of petroleum contaminated soils were excavated
and disposed of from around the (5) USTs during IAA excavation activities.

Free Product/Vapor Removal: Free product was observed floating on pit groundwater
during abatement activities for the 4,000 gallon diesel fuel UST. These liquids were mixed
with overburden soils and removed via excavation. Free product has not been observed in
MW-1 which was placed in the former diesel fuel UST pit. On December 15, 2016, free
product was observed at a thickness of 0.01’ in MW-9 installed down-gradient of the active
gasoline UST pit which contains (2) 6,000 gallon USTs. No recovery has been performed
from this well to date.

3. Extent of Release and Potentially Affected Receptors

Water Supply Wells: (2) water supply wells were identified within 1,500’ of the release
source, one located within 900’ from the release source site. Public water is available.

Potential Receptors: Surface waters in the vicinity of the release area generally drain
towards the north/northeast towards an unnamed intermittent stream. This intermittent stream
empties into the Contentnea Creek which lies within the Neuse River Basin.

Subsurface Structures: Subsurface lines/structures are not present within the petroleum
affected area at this site. Subsurface utilities are present in the form of water, sewer &
communication lines, but are above the impacted area.

Population: The population of Wilson, NC is 49,628 according to a 2013 census
estimate. Surrounding areas are undeveloped or used for industrial/residential purposes.

4. Maximum Contaminant Concentrations-Soil:

Contaminated soils in the former 4,000 gallon diesel UST area were remediated to below lowest
MSCCs during initial abatement action activities. All samples obtained from the limits of
excavation were below laboratory detection limits for risk-base soil parameters.

5. Maximum Contaminant Concentrations-Groundwater:
Benzene 14,000 ug/l (MW-9)*
Toluene 43,100 ug/l (MW-9)
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Ethylbenzene 4,130 ug/l (MW-9)
Xylenes 19,950 ug/l (MW-9)
Naphthalene 844 ug/L (MW-4)
MTBE 6240 ug/l (MW-9)
Isopropylbenzene 175 ug/l (MW-9)
n-Propylbenzene 490 ug/l (MW-4)
Diisopropylether 778 ug/l (MW-9)
1,2,4 Trimethylbenzene 3,240 ug/l (MW-4)
1,3,5 Trimethylbenzene 892 ug/l (MW-4)
C5-C8 Aliphatics 140,000 ug/l (MW-9)
C9-C18 Aliphatics 26,100 ug/l (MW-9)
C9-C22 Aromatics 15,100 ug/l (MW-4)

* GCL violations for this compound

Groundwater Flow: General Flow Direction – Northeast
Flow Rate: Hydraulic Gradient = 0.00692; Estimated flow rate = 15.1 ft/year

6. Risk Classification Considerations

The site is currently classified as High risk, based on the presence of (1) water supply well
within 1,000’ of the site. The site contains GCL violations which constitute an Intermediate risk
ranking for the site. Lowering of the risk classification is possible with connection of the local user
to publically available water supply and remediation of GCL violations at the site.

7. Conclusions/Recommendations for Corrective Action

The extent of petroleum impacted soil and groundwater have been mostly delineated at this
site. Contaminated soils in the former 4,000 gallon diesel UST area of this site were completely
remediated via IAA soil excavation. The groundwater plume has been predominantly defined with
the exception of the MTBE plume which has migrated beyond the monitoring well network which
is currently in place. The latest groundwater analytical data indicates a benzene GCL violation and
some free product within the groundwater plume which will require remediation in order for the
site to be granted No Further Action status.

A CAP should be developed for remediation of contaminated groundwater at this site.
Natural Attenuation should be utilized to the maximum extent possible. Aggressive Fluid Vapor
Recovery (AFVR) and/or Mobile Multi-Phase Extraction (MMPE) events should be conducted at
the site to recover free product and reduce benzene contaminant levels to below Gross Contaminant
Levels (GCLs). Additional monitoring wells should be installed down gradient of monitoring wells
MW-5, 6 & 7 prior to the next groundwater sampling event.
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C. TABLE OF CONTENTS

Page

A. TITLE PAGE i

B. EXECUTIVE SUMMARY ii

C. TABLE OF CONTENTS iv

D. SITE HISTORY AND SOURCE CHARACTERIZATION 1

E. RECEPTOR INFORMATION 1

F. REGIONAL GEOLOGY AND HYDROGEOLOGY 3

G. SITE GEOLOGY AND HYDROGEOLOGY 3

H. SOIL SAMPLING RESULTS 3

I. GROUNDWATER SAMPLING RESULTS 4

J. FREE PRODUCT INVESTIGATION 5

K. HYDROGEOLOGIC INVESTIGATION 5

L. GROUNDWATER MODELING RESULTS 6

M. DISCUSSION 6

N. CONCLUSIONS AND RECOMMENDATIONS 6

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C. TABLE OF CONTENTS (CON'T)

O. FIGURES

Figure 1: Project Location/U.S.G.S. Topographic Map
Figure 2: Site Layout and UST Locations
Figure 3: Subsurface Utilities Map
Figure 4: Adjacent Properties Map
Figure 5: Receptor Map
Figure 6: Site Layout, Soil Sample Locations, and Soil VPH Map
Figure 7: Site Layout, Monitor Well & Geologic Cross-Section Locations
Figure 8: Geologic Cross-Section A to A'
Figure 9: Geologic Cross-Section B to B'
Figure 10 Benzene Isoconcentration Map
Figure 10A: Benzene Isoconcentration Cross-Section A to A'
Figure 10B: Benzene Isoconcentration Cross-Section B to B'
Figure 11 Naphthalene Isoconcentration Map
Figure 11A: Naphthalene Isoconcentration Cross-Section A to A'
Figure 11B: Naphthalene Isoconcentration Cross-Section B to B'
Figure 12: C5-C8 Total Aliphatics Isoconcentration Map
Figure 12A: C5-C8 Total Aliphatics Isoconcentration Cross-Section A to A'
Figure 12B: C5-C8 Total Aliphatics Isoconcentration Cross-Section B to B'
Figure 13 MTBE Isoconcentration Map
Figure 13A: MTBE Isoconcentration Cross-Section A to A'
Figure 13B: MTBE Isoconcentration Cross-Section B to B'
Figure 14: Potentiometric Surface Map (12/9/16)

P. TABLES

Table 1: Site History
Table 2: Adjacent Property Owners
Table 3: Supply Well Information
Table 4: Risk-Based Soil Laboratory Analytical Results
Table 5: Summary of Groundwater Laboratory Analytical Results
Table 6: Monitoring Well Information and Groundwater Elevations

Q. APPENDICES

Appendix A: Soil Boring Logs
Appendix B: Well Construction Records
Appendix C: Laboratory Analytical Results
Appendix D: Slug Test Data and Analyses

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COMPREHENSIVE SITE ASSESSMENT
FRIENDLY MART, 3055 STANTONSBURG ROAD
WILSON, WILSON COUNTY, NORTH CAROLINA
GW INCIDENT #39876

D. - SITE HISTORY AND SOURCE CHARACTERIZATION

1. Background

Rose Oil Company, Inc. owns USTs which are operated at the Friendly Mart facility located at
3055 Stantonsburg Road in Wilson, North Carolina. Figure 1 illustrates the location of this facility
on the Wilson Quadrangle U.S.G.S. Topo Map. This facility contains one permanent structure
which is used as a gasoline convenience store. The site contains (2) 6,000 gallon gasoline & (1)
4,000 gallon gasoline USTs which are currently in use. The site formerly contained a 4,000 gallon
diesel UST which was removed from the site on December 17, 2015. Figure 2 illustrates the
overall layout of this site and the UST locations. Table 1 summarizes the UST history for the
Friendly Mart site.

A release from the UST system was suspected on 12/17/15 based on elevated PID readings
observed in soil samples collected from around the UST and the presence of a floating layer of
diesel in the UST excavation. Groundwater was observed at a depth of approximately 4’ to 5’
below surface in the UST pit during soil abatement activities. The site and adjacent properties are
used for commercial, residential and industrial purposes. Municipal water supplies are available to
properties within 1,500’ and serve the Friendly Mart facility; however, 2 adjacent properties are
served by a local water supply well. Groundwater impact is above current 15 NCAC 2B Standards;
however, no surface water bodies are located within 500’ of the release source.

2. Previous Reports:

a) 20 Day Report, Henry Nemargut Engineering Services, January 7, 2016;

b) Initial Abatement Action, Henry Nemargut Engineering Services, April 12, 2016;

c) Phase II Limited Site Assessment Report, Henry Nemargut Engineering Services, June 10,
2016

E. - RECEPTOR INFORMATION

1. Water Supply Wells

A supply well survey has been conducted within a 1,500' radius of the release area. This survey
was conducted by interviews conducted with owners and occupants of properties located within
1,500’ of the release sources. During this reconnaissance (2) water supply wells (1 in-use potable
and 1 out of service potable) were found to be located within a 1,000’ radius. The in-use supply
well is located 140’ from the UST release source and is used to supply water for the adjacent
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private residence at 3043 Stantonsburg Road and also the Ready Contractors office building at
3041 Stantonsburg Road. Table 3 lists information for the wells identified during this
investigation. Figure 5 depicts the approximate locations of these wells on a Wilson County parcel
map.

2. Public Water Supplies

Public water supplies are available to properties within 1,500’ of the release site; however, water
lines have not yet been routed to all properties within the specified search radius.

3. Surface Water

The partial Wilson Quadrangle U.S.G.S. Topographic Map included as Figure 1 indicates that the
release site is located on a slight ridge at an approximate elevation of 122’ amsl. Surface waters in
the vicinity of the release area generally drain towards the north/northeast towards an unnamed
intermittent stream. This intermittent stream empties into the Contentnea Creek which lies within
the Neuse River Basin.

4. Wellhead Protection Areas

No wellhead protection areas are known to exist within the area of this release.

5. Deep Aquifers in the Coastal Plain Physiographic Region

This release is located in the coastal plain. It is unknown if the shallow groundwater in the release
area feeds deep aquifers.

6. Subsurface Structures

Subsurface lines/structures are not present within the petroleum affected area at this site.
Subsurface utilities are present in the form of natural gas, communications, water & sewer.
Underground water and sewer lines enter the store building on the south side from Stantonsburg
Rd, outside of the impacted areas within the property boundaries. Natural gas and communications
lines traverse the groundwater plume but are situated above the contamination which is at a depth
of >4’ below surface. Figure 3 illustrates the locations of subsurface utilities near the subject
property.

7. Land Use

The possibility of human exposure to soil contamination at 3055 Stantonsburg Road site is
minimal. Petroleum impacted soils were remediated in the diesel UST area. Contamination at this
facility lies within a commercial site.

8. Property Owners and Occupants

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Figure 4 illustrates the locations of properties adjacent to the release site. Table 2 lists property
ownership information for adjacent property owners. This information was obtained from Wilson
County Tax records.

F. - REGIONAL GEOLOGY AND HYDROGEOLOGY

The site is situated in the Coastal Plain. According to the Geological Map of North Carolina local
geology of the region is classified as the Yorktown Formation, underlain by fossiliferous clay with
varying amounts of fine-grained sand. Dense clay with weathered rock was observed at a depth of
approximately 71’ below grade and competent bedrock was encountered at a depth of 74 feet below
surface during installation of the vertical extent well for this facility.

G. - SITE GEOLOGY AND HYDROGEOLOGY

The soils at the project site consist of silts, sands and clays of varying proportions. During
installation of the vertical extent well, weathered rock was noted at a depth of 71’ below grade,
followed by competent rock at a depth of 74’ below grade. Soil logs for soil samples collected at
the site during IAA activities are contained as Appendix A, and soil boring logs are listed on well
construction records included as Appendix B. Field observations showed the soils at the site
consist of a variety of textural assemblages as noted on the soil boring logs. Geological Cross
Sections A to A' and B to B' included as Figures 7, 8, and 9 illustrate the plan view and cross-
section views of the subsurface geology as interpreted from borings advanced at the site.

H. – SOILS INVESTIGATION

Following IAA excavation activities, soil samples were collected from the perimeter of the UST
excavation where over-excavation was conducted to obtain risk-based analytical data for the site
during IAA activities. Results from the risk-based and TPH soil samples were below NCDEQ
lowest MSCCs or Action Levels for all 8260/8270/VPH/EPH/TPH compounds for pit wall
samples. The soil samples were obtained as specified in the collection, preservation, and handling
section of the specific method. Each container was labeled with sample location, analyses to be
performed, time, date, and the sampler's name. They were then placed in a cooler and chilled with
ice to approximately 4oC in preparation for transportation to the analytical laboratory utilizing EPA
approved chain of custody procedures. Additional samples from each pit wall were containerized
for possible analyses via risk-based methods. Figure 6 depicts soil analytical results on a site map
of the over-excavation area for the diesel UST. Copies of the soil analytical report and the chain of
custody records for the risk-based soil samples collected at 3055 Stantonsburg Road are contained
in the previously submitted IAA report.

Due to the high seasonal water table observed at the site, no additional soil samples were collected
for laboratory analyses during CSA activities.

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I. - GROUNDWATER INVESTIGATION

A total of nine North Carolina Type II groundwater monitoring wells and one Type III vertical
extent well have been installed at the project site in conjunction with CSA activities. The
monitoring wells were constructed of 2-inch Schedule 40 PVC pipe with 0.010 inch slotted screen.
Based on the assumption that the contaminants being addressed were primarily hydrocarbon
constituents with specific gravities of less than 1.0, the Type II monitoring wells were installed so
that the screened interval intersected the shallow groundwater table at the time of installation.
Figure 7 illustrates the locations of the monitor wells installed at the project site. Well construction
records for the monitor wells installed during CSA activities are included in Appendix B.

Following installation, monitoring wells MW-1 through MW-9 and VEW-1 were developed and
sampled in accordance with the July 15, 2008 NCDEQ Guidelines. The groundwater samples were
submitted to a certified laboratory for analyses according to Methods 6200B including adders,
3030C (lead), and MADEP Methods for VPH. The closest in-use water supply well (SW-1)
located on the property owned by Lawrence Jones was sampled for analyses via Method 6200B
only.

Fourteen petroleum related compounds/compound groups were found present in groundwater
samples collected at the project site above current 15 NCAC 2L groundwater standards. Benzene
was noted above its GCL. The maximum contaminant levels detected at the site are listed below:

Benzene 14,000 ug/l (MW-9)*
Toluene 43,100 ug/l (MW-9)
Ethylbenzene 4,130 ug/l (MW-9)
Xylenes 19,950 ug/l (MW-9)
Naphthalene 844 ug/L (MW-4)
MTBE 6240 ug/l (MW-9)
Isopropylbenzene 175 ug/l (MW-9)
n-Propylbenzene 490 ug/l (MW-4)
Diisopropylether 778 ug/l (MW-9)
1,2,4 Trimethylbenzene 3,240 ug/l (MW-4)
1,3,5 Trimethylbenzene 892 ug/l (MW-4)
C5-C8 Aliphatics 140,000 ug/l (MW-9)
C9-C18 Aliphatics 26,100 ug/l (MW-9)
C9-C22 Aromatics 15,100 ug/l (MW-4)

* GCL violation for this compound

Table 5 summarizes the groundwater analytical results, and Appendix C contains copies of the
laboratory analytical results for the most recent sampling event conducted during CSA activities.

The monitoring well network at this facility generally defines the vertical and horizontal extent of
the contaminant plume at the site. Concentrations of contaminants appear to originate from the
UST sources area and migrate east/northeast with the shallow groundwater flow. There is an
apparent skewed migration of contaminants towards the in-use water supply well on the Lawrence
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Jones property. Potentiometric data from the shallow wells and vertical extent well VEW-1
installed downgradient of the release source indicate that there is a strong downward vertical
groundwater flow from the upper aquifer to the lower aquifer.

Figures 10 through 13B illustrate the extent of petroleum constituents in the groundwater as
determined from the analytical results from CSA activities. These figures contain isoconcentration
maps and isoconcentration cross-sections for Benzene, Naphthalene, C5-C18 Aliphatics and
MTBE. All of these plumes are relatively confined to the source area and down-gradient areas just
beyond MW-5, MW-6 and MW-7.

J. - FREE PRODUCT INVESTIGATION

Free product observed in the diesel UST pit was remediated during initial abatement by soil
excavation and has not been observed in MW-1 installed in the former diesel UST excavation. On
December 15, 2016, free product was observed in monitoring well MW-9 at a thickness of 0.01’.
No recovery activities have been conducted in this well awaiting adoption of the new 2017
NCDEQ UST guidelines.

K. - HYDROGEOLOGIC INVESTIGATION

Figure 14 illustrates the shallow groundwater potentiometric surface as measured during CSA
activities. Groundwater is noted to be flowing towards the northeast according to the estimated
potentiometric surface maps. The average potentiometric surface gradient has been calculated at
approximately 0.00692 ft/ft. Table 6 summarizes monitoring well information and groundwater
elevations as measured on December 9, 2016.

Three single well rising head tests or "slug tests" were performed on MW-2, MW-6 and MW-8 to
determine the saturated hydraulic conductivity of the water table aquifer. The method of Bouwer
and Rice (Bouwer and Rice, 1989, 1976) was chosen to reduce the slug test data. A computer
program developed by the Geraghty & Miller Modeling Group named AQTESOLV was used to
estimate the aquifer parameters. Results of the slug tests indicated a hydraulic conductivity of 2.42
x10-3 feet/minute for MW-2, 3.696 x 10-4 feet/minute for MW-6, and 3.327 x 10-4 feet/minute for
MW-8. The results from MW-2, MW-6 and MW-8 are consistent with published values for silt,
loess and silty sand (Freeze & Cherry, 1979). Slug test data plots with AQTESOLV results are
included in Appendix D.

Groundwater flow velocity was determined using Darcy’s Law by using the geometric mean of the
hydraulic conductivity values and assuming an estimated effective porosity of 25% for soils at the
site. The following equation yields an estimate of average groundwater flow velocity:

v = k/n x dh/dl

Where v=average groundwater flow velocity
K=average hydraulic conductivity=1.041x10-3ft/min.
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n=effective porosity=0.25
dh/dl=groundwater head gradient=0.00692 ft/ft

Average groundwater flow velocity at the site is calculated to be 2.882 x 10-5 feet/minute (15.1
feet/year).

L. - GROUNDWATER MODELING RESULTS

No groundwater modeling other than the reduction of the slug test data using Aqtesolv has been
performed at the project site. The site is classified as high risk based on the potential impact to
nearby receptors. The monitor well network installed at the site will be utilized to insure that
contaminants are not migrating towards the nearby receptors. Groundwater modeling may be
utilized in generation of a corrective action plan for the site.

M. - DISCUSSION

Contaminated soils and free product in the former diesel UST area at this site were remediated via
IAA soil excavation. Some contaminated soils located above the seasonal high water table may be
located in the operational UST basin containing (2) 6,000 gallon gasoline USTs. Due to the close
proximity of these soils to operational USTs, excavation of these soils is not practical. The latest
groundwater analytical data indicates GCL violations and some free product emanating from this
area which will require remediation in order for the site to be granted No Further Action status.

The site is currently classified as High risk, based on the presence of (1) water supply well within
1,000’ of the site. The site contains GCL violations which constitute an Intermediate risk ranking
for the site. Lowering of the risk classification is possible with connection of the local user to
publically available water supply and remediation of GCL violations and free product at the site

N. - CONCLUSIONS AND RECOMMENDATIONS

Based on the information presented in this report, Henry Nemargut Engineering Services makes the
following conclusions and recommendations:

1) The extent of petroleum impacted soil and groundwater have been mostly delineated.
Additional monitoring wells should be installed down gradient of monitoring wells MW-5, 6 & 7
prior to the next groundwater sampling event.

2) Aggressive Fluid Vapor Recovery (AFVR) and/or Mobile Multi-Phase Extraction (MMPE)
events should be conducted at the site to remediate free product and reduce benzene contaminant
levels to below Gross Contaminant Levels (GCLs).

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3) A CAP should be prepared to determine a cost effective method of remediation for this site
following evaluation of AFVR/MMPE results.

This report has been prepared for the exclusive use of the Rose Oil Company, Inc. for the specific
application to the referenced site located in Wilson County, North Carolina. The evaluation was
conducted based on the scope of work and level of effort desired by the client and with resources
adequate only for the scope of work approved by the NCDEQ. Our findings have been developed
in accordance with generally accepted standards for Comprehensive Site Assessments in the State
of North Carolina, available information and our professional judgment. No other warranty is
expressed or implied.

The data presented in this report are indicative of conditions at the precise locations sampled and
the time the sample was collected. Additionally, the data obtained from the samples would be
interpreted as meaningful with respect to the parameters in the laboratory reports. No additional
information can be logically inferred from this data.

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O. FIGURES
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P. TABLES
TABLE 1: SITE HISTORY
Plainview Grocery
3055 Stantonsburg Road, Wilson, NC 27565

Property Ownership:

S.M.W., Inc.
P.O. Box 706
Henderson, NC 27536-0706
9/4/1985 to present

Previous Property Owners:

Lawrence & Annie Jones
1/31/1974 to 9/4/1985

UST Information:

Tank Inst. Size Closure UST Tank
No Date (Gal) Date Status Contents
1 8/19/81 6,000 N/A In-use Gasoline
2 8/19/81 6,000 N/A In-use Gasoline
3 8/19/81 4,000 1/6/99 Closed Gasoline
3A 7/14/99 4,000 N/A In-use Gasoline
4 1/1/64 4,000 12/17/15 Closed Diesel

Tank owner:

Rose Oil Company, Inc.
P.O. Box 706
Henderson, NC 27536-0706
9/4/1985 to present
TABLE 2: ADJACENT PROPERTY OWNERS
FRIENDLY MART
3055 STANTONSBURG ROAD
WISLON, NORTH CAROLINA 27893

MAP ID PARCEL ID OWNER INFORMATION

Project 3730-08-2189.000 S.W.M., Inc.
Site 613 US 158 Bypass
Henderson, NC 27537-6825

1 3730-18-6502.000 City of Wilson
P.O. Box 10
Wilson, NC 27894-0010

2 3730-08-5691.000 Lawrence Thomas Jones
4570 Aaron Court
Elm City, NC 27822-8600

3 3730-17-5223.000 McCall Farms, Inc.
6615 Irby Street South
Effingham, SC 29541

4 3730-98-0830.000 Alliance One International, Inc.
P.O. Box 650
Farmville, NC 27828-0650

5 3730-08-1453.000 Larene Bass Radford
3043 Stantonsburg Rd SE
Wilson, NC 27893-7865

WellIdentification IW-1 SW-1Owner Name Larene Bass Radford Lawrence Thomas JonesProperty Address3043 Stantonsburg Rd 3041 Stantonsburg RdWilson, NC 27893 Wilson, NC 27893Occupant Larene Bass Radford Ready Contractors, Inc.PARID # 3730-08-1453.000 3730-08-5691.000Use Out of Service Potable Potable for 3041 & 3043 Distance 120' 140'City Water? NO NODepth of Well Unknown UnknownWell Diameter 6" 6"Well Yield Unknown UnknownDepth to Pump Unknown UnknownDepth of Casing Unknown UnknownStatic Water Unknown UnknownFriendly Mart3055 STANTONSBURG RD, WILSON, NC 27893TABLE 3SUPPLY WELL INFORMATION1,500' RADIUSFRIENDLY MART
Sample Location E W Lowest MSCC Ind/Comm MSCC Residential MSCCDate12/17/2015 12/17/2015 (note units) (note units) (note units)Sample depth3' 3' Method 8260 (ug/kg)Benzene BDL BDL 5.6 164,000.0 18,000Methylene Chloride BDL 18.6 20 763,000 85,000n-Butylbenzene BDL BDL 4,300 16,350,000 626,000sec-Butylbenzene BDL BDL 3,300 16,350,000 626,000Ethylbenzene BDL BDL 4,900 40,000,000 1,560,000Isopropylbenzene BDL BDL 2,000 40,880,000 1,564,000p-Isopropyltoluene BDL BDL NSE NSE NSENaphthalene BDL BDL 160 8176000 313,000Acetone BDL BDL 24,000 360,000,000 14,000,000n-Propylbenzene BDL BDL 2,000 16,350,000 626,000Toluene BDL BDL 4,300 32,000,000 1,200,0001,2,4-Trimethylbenzene BDL BDL 8,500 20,440,000 782,0001,3,5-Trimethylbenzene BDL BDL 8,300 20,440,000 782,000MTBE BDL BDL 91 3,100,000 350,000sec-butylbenzene BDL BDL 3,400 16,350,000 626,000Xylenes (total) BDL BDL 4,600 81,760,000 3,129,000Method 8270 (ug/kg)FluoreneBDLBDL47,00016,400,000620,000Fluoranthene BDL BDL 290,000 16,400,000 620,000Phenanthrene BDL BDL 56,000 12,264,000 469,0001-Methylnaphthalene BDL BDL 4 100,000 20,0002-Methylnaphthalene BDL BDL 3,600 1,635,000 63,000Naphthalene BDL BDL 160 8176000 313,000Aliphatic Fraction Classes (mg/kg) C5 - C8 Volatile Aliphatics BDL BDL 68 24,528 939C9 - C12 Volatile Aliphatics BDL BDL NSE NSE NSEC9-C18 Extractable Aliphatics BDL BDL NSE NSE NSEC9-C18 Aliphatics (total) BDL BDL 540 40,000 1,500C19-C36 Extractable AliphaticsBDLBDLNSE810,00031,000Aromatic Fraction Classes (mg/kg) C9 - C10 Volatile AromaticsBDLBDLNSENSENSEC11 - C22 Extractable Aromatics BDL BDL NSE NSE NSEC9 - C22 Aromatics (total)BDLBDL3112264469BDL = below detection limits NR = analyses not requestedNSE = no standard establishedTABLE 4Laboratory Analytical Results - Risk Based Soil SamplesFriendly Mart, 3055 Stantonsburg Road, Wilson, NC
TABLE 5Monitoring Well Information and Groundwater ElevationsFriendly Mart, 3055 Stantonsburg, NC 27893Well Number Top of Casing Elevation Top of Screen Elevation Bottom of Screen Elevation Depth to Water Groundwater ElevationMW-1 99.79 95.79 85.79 7.10 92.69MW-2 100.00 96.00 86.00 8.59 91.41MW-3 99.19 95.19 85.19 8.68 90.51MW-4 99.88 95.88 85.88 9.16 90.72MW-5 99.42 94.42 84.42 9.54 89.88MW-6 99.78 94.78 84.78 10.87 88.91MW-7 100.06 95.06 85.06 10.76 89.30MW-8 100.52 95.52 85.52 10.18 90.34MW-9 100.01 95.01 85.01 9.07 90.94VEW-1 100.16 25.16 20.16 21.83 78.33All measurements taken in feet and based on an arbitrary benchmark of 100 ft. established at MW-1Groundwater levels measured on 12/9/2016Friendly Mart
TABLE 6
SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
FRIENDLY MART
3055 STANTONSBURG RD, WILSON, NC
Constituent MW-1 MW-2 MW-3 MW-4 GCL 2L Standard

Date 12/8/2016 12/8/2016 12/15/2016 12/8/2016
Method 6200B (ug/L)
Benzene BDL BDL 417 1540 5,000 1
Toluene BDL BDL BDL 1970 260,000 600
Ethylbenzene BDL 0.69 BDL 3040 84,500 600
Xylenes (total) BDL 0.64 18.9 8170 85,500 500
BTEX (total) 0 1.33 435.9 14720 NSE NSE
p-Isopropyltoluene BDL BDL BDL BDL NSE NSE
Isopropylbenzene 15.7 BDL 5.3 174 25,000 70
Diisopropyl Ether (DIPE) BDL BDL 19.8 135 70,000 70
Naphthalene BDL BDL 50.6 844 6,000 6
sec-Butylbenzene 0.8 BDL BDL BDL 8,500 70
n-propylbenzene 1.1 0.6 BDL 490 30,000 70
Bromodichloromethene BDL BDL 4 BDL NSE NSE
Chloroform BDL BDL 115 BDL 70,000 70.0
n-butylbenzene 0.55 BDL BDL BDL 6,900 70
Styrene BDL BDL BDL BDL 70,000 70
Methyl-tert-butyl-ether (MTBE) 2.9 BDL 915 848 20,000 20
1,2,4-Trimethylbenzene BDL 3.7 23 3240 28,500 400
1,3,5-Trimethylbenzene BDL 3.9 2.9 892 25,000 400
1,2-Dibromoethane (EDB) BDL BDL BDL BDL 50 0.02
Lead (3010) BDL BDL BDL BDL 15,000 15
Method 625 (ug/L)
Acenaphthene N/A N/A N/A N/A 2,120 80
Phenol N/A N/A N/A N/A 30,000 30
Naphthalene N/A N/A N/A N/A 6,000 6
Total TICs N/A N/A N/A N/A NSE NSE
Aliphatic Fraction Classes (ug/L)
C5-C8 Volatile Aliphatics 65 BDL 2670 11900 NSE 400
C9-C12 Volatile Aliphatics BDL BDL BDL 23400 NSE NSE
C9-C18 Extractable Aliphatics N/A N/A N/A N/A NSE 700
C9-C18 Aliphatics (total) 0 BDL BDL 23400 NSE 700
C19-C36 Extractable Aliphatics N/A N/A N/A N/A NSE 10,000
Aromatic Fraction Classes (ug/L)
C9-C10 Volatile Aromatics 89.6 118 BDL 15100 NSE NSE
C11-C22 Extractable Aromatics N/A N/A N/A N/A NSE NSE
C9-C22 Aromatics (total) 89.6 118 BDL 15100 NSE 200
N/A = Not Analyzed
BDL = Below Detection Limits
NSE = No Standard Established
TABLE 6 (continued)
SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
FRIENDLY MART
3055 STANTONSBURG RD, WILSON, NC
Constituent MW-5 MW-6 MW-7 MW-8 GCL 2L Standard

Date 12/8/2016 12/8/2016 12/8/2016 12/8/2016
Method 6200B (ug/L)
Benzene 6.5 BDL 0.97 0.96 5,000 1
Toluene BDL BDL BDL BDL 260,000 600
Ethylbenzene BDL BDL BDL BDL 84,500 600
Xylenes (total) 0.61 BDL BDL BDL 85,500 500
BTEX (total) 7.11 0 0.97 0.96 NSE NSE
p-Isopropyltoluene BDL BDL BDL BDL NSE NSE
Isopropylbenzene BDL BDL BDL BDL 25,000 70
Diisopropyl Ether (DIPE) BDL 25.4 33.1 2 70,000 70
Naphthalene 5.5 BDL BDL BDL 6,000 6
sec-Butylbenzene BDL BDL BDL BDL 8,500 70
n-propylbenzene BDL BDL BDL BDL 30,000 70
Chloroform BDL BDL BDL BDL 70,000 70.0
n-butylbenzene BDL BDL BDL BDL 6,900 70
1,2-Dichloroethane BDL BDL BDL BDL 400 0.4
Methyl-tert-butyl-ether (MTBE)176 364 191 8.2 20,000 20
1,2,4-Trimethylbenzene BDL BDL BDL BDL 28,500 400
1,3,5-Trimethylbenzene BDL BDL BDL BDL 25,000 400
1,2-Dibromoethane (EDB) BDL BDL BDL BDL 50 0.02
Methylene Chloride BDL 5.4 BDL BDL 5,000 5
Lead (3010) BDL BDL BDL BDL 15,000 15
Method 625 (ug/L)
Acenaphthene N/A N/A N/A N/A 2,120 80
Phenol N/A N/A N/A N/A 30,000 30
Naphthalene N/A N/A N/A N/A 6,000 6
Total TICs N/A N/A N/A N/A NSE NSE
Aliphatic Fraction Classes (ug/L)
C5-C8 Volatile Aliphatics 289 578 387 BDL NSE 400
C9-C12 Volatile Aliphatics BDL BDL BDL BDL NSE NSE
C9-C18 Extractable Aliphatics N/A N/A N/A N/A NSE 700
C9-C18 Aliphatics (total) BDL BDL BDL BDL NSE 700
C19-C36 Extractable Aliphatics N/A N/A N/A N/A NSE 10,000
Aromatic Fraction Classes (ug/L)
C9-C10 Volatile Aromatics BDL BDL BDL BDL NSE NSE
C11-C22 Extractable Aromatics N/A N/A N/A N/A NSE NSE
C9-C22 Aromatics (total) BDL BDL BDL BDL NSE 200
N/A = Not Analyzed
BDL = Below Detection Limits
NSE = No Standard Established
TABLE 6 (continued)
SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
FRIENDLY MART
3055 STANTONSBURG RD, WILSON, NC
Constituent VEW-1 MW-9 SW-1 GCL 2L Standard

Date 12/8/2016 12/8/2016 12/8/2016
Method 6200B (ug/L)
Benzene 0.61 14000 BDL 5,000 1
Toluene 0.7 43100 BDL 260,000 600
Ethylbenzene 0.51 4130 BDL 84,500 600
Xylenes (total) 2.69 19950 BDL 85,500 500
BTEX (total) 4.51 81180 0 NSE NSE
p-Isopropyltoluene BDL BDL BDL NSE NSE
Isopropylbenzene BDL 175 BDL 25,000 70
Diisopropyl Ether (DIPE) BDL 778 BDL 70,000 70
Naphthalene BDL 571 BDL 6,000 6
sec-Butylbenzene BDL BDL BDL 8,500 70
n-propylbenzene BDL 471 BDL 30,000 70
Chloroform 7 BDL BDL 70,000 70.0
n-butylbenzene BDL BDL BDL 6,900 70
1,2-Dichloroethane BDL BDL BDL 400 0.4
Methyl-tert-butyl-ether (MTBE) 0.76 6240 1.3 20,000 20
1,2,4-Trimethylbenzene 1 2860 BDL 28,500 400
1,3,5-Trimethylbenzene BDL 736 BDL 25,000 400
1,2-Dibromoethane (EDB) BDL BDL BDL 50 0.02
Lead (3010) BDL BDL BDL 15,000 15
Method 625 (ug/L)
Acenaphthene N/A N/A N/A 2,120 80
Phenol N/A N/A N/A 30,000 30
Naphthalene N/A N/A N/A 6,000 6
Total TICs N/A N/A N/A NSE NSE
Aliphatic Fraction Classes (ug/L)
C5-C8 Volatile Aliphatics 66.3 140000 BDL NSE 400
C9-C12 Volatile Aliphatics BDL 26100 BDL NSE NSE
C9-C18 Extractable Aliphatics N/A N/A N/A NSE 700
C9-C18 Aliphatics (total) BDL 26100 BDL NSE 700
C19-C36 Extractable Aliphatics N/A N/A N/A NSE 10,000
Aromatic Fraction Classes (ug/L)
C9-C10 Volatile Aromatics BDL BDL BDL NSE NSE
C11-C22 Extractable Aromatics N/A N/A N/A NSE NSE
C9-C22 Aromatics (total) BDL BDL BDL NSE 200
N/A = Not Analyzed
BDL = Below Detection Limits
NSE = No Standard Established
Page - 10

Q. APPENDICES
Page - 11

APPENDIX A

SOIL BORING LOGS

GEOLOGIC LOG OF EXCAVATION
Henry Nemargut Engineering Services
Job Name: Friendly Mart
Address: 3055 Old Stantonsburg Rd, Wilson, NC
Job No.:
Start Date: 12/17/2016
Contractor: Ready Contractors
Sample ID: UST Closure Samples
Comments:

Sample Depth OVA
Number (FT.)Soil Decription (color, soil type, moisture) (ppm)
E 3' tan-gray, Clay w/silt and little sand BDL
N1 3' gray-red, Silt w/clay 3
N2 3' gray-red, Silt w/clay 2
N3 3' gray-orange-brown, Silt w/clay 3
W 3' orange-brown-red, Silt w/clay and trace sand BDL
Page - 12

APPENDIX B

WELL CONSTRUCTION RECORDS

WELL CONTRACTOR CERTIFICATION # ...;:3:..,:.42::,:6::......--_
1. WELL CONTRACTOR: d. TOP OF CASING IS 0' FT. Above Land Surface'
'Top of casing terminated at/or below land surface may requireHenry Nemargut a variance in accordance with 15A NCAC 2C .0118.
Well Contractor (Individual) Name

e. YIELD (gpm): METHOD OF TEST ­Henry Nemargut Engineering Services
f. DISINFECTION: Type Amount _Well Contractor Company Name
g. WATER ZONES (depth): STREET ADDRESS 2211 Chestnut Street

From To___ From To _

Wilmington NC 28405
From To___ From To _ City or Town State Zip Code From To___ From To _
~_ 762-5475

6. CASING: Thickness/Area code- Phone number
Depth 2Qiameter Weight ~~ial2. WELL INFORMATION: ScH 40From_0_'__ To_5_'__ Ft. _SITE WELL 10 #(il applicable)_M_W_-5 _ From To Ft. _STATE WELL PERMIT#(il applicable), _ From To Ft. _

DWQ or OTHER PERMIT #(if applicable) _

7. GROUT: Depth Material Method WELL USE (Check Applicable Box) Monitoring IKJ Municipal/Public 0

From_O_'__ To_4_'__ Ft. Portland Pour
Industrial/CommercialO Agricultural 0 Recovery 0 Injection 0

From To Ft. _
Irrigationo Other 0 (list use) _ From To Ft. _

DATE DRILLED_12_/8_/_20_1_6 _

8. SCREEN: Depth Diameter Slot Size Material
TIME COMPLETED._1_0_:0.....:0 AM ~ PM 0 From_5_'__ To_1_5_'_ Ft._2__in. 0.01 in. PVC
3. WELL LOCATION: From To Ft __in. in. _
CITY: -'-W.....:il..:.so:...n COUNTY-.:W~ils:..:o.:.:n _ From To Ft.__in. in. _
3055 Stantonsburg Rd, Wilson, NC 27893 9. SAND/GRAVEL PACK: (Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code) Depth Size Material

TOPOGRAPHIC / LAND SETTING:
From 4' To_1_5'__ Ft. #2 Filter Sand
DSlope DValley KJFlat ORidge OOther _
From To Ft.. _ (check appropriate box) From To Ft .. ----'-_
LATITUDE -l-_ 3569099167 May be in degrees.

minutes, seconds or
10, DRILLING LOG LONGITUDE 77.88775 in a decimal format From To Formation Description
Latitude/longitude source: €IGPS oTopographic map 0' 3' tan, Silt w/little sand

(location of well must be shown on a USGS tapa map and
3' 6' tan-red, Silt wlsome clay
attached to this form if not using GPS) 6' 12' tan, Silt w/c1ay & sand
12' 15' tan, Slay w/sand &some clay

FACILITY ID #(if applicable)_0:...,..:.02:...4:..:5..:.8::...9 _

NAME OF FACILlTY_F::;r.:..:ie::;n:.::d:.:,ly...:,M::;a::.rt-=----_

STREET ADDRESS 3055 Stantonsburg Road

Wilson NC 27893

City or Town State Zip Code

CONTACT PERSON Raymond Bartholomew

MAILING ADDRESS,...:P....:...:.O.:....B=-0::.x:...:7--=O..:.6 _

Henderson NC 27536­
4. FACILlTY-is the name of the business where the well is located.
11. REMARKS:

City or Town State Zip Code

(252 ),_4_3_8_-7_1_4_1 _

Area code -Phone number

5. WELL DETAILS:
a. TOTALDEPTH:._15_' ___
b. DOES WELL REPLACE EXISTING WELL? YES 0 NO IZJ
c. WATER LEVEL Below Top of Casing: 9.54' FT.

(Use "+" if Above Top of Casing)

12/28/2016
DATE
Submit the original to the Division of Water Quality within 30 days. Attn: Information Mgt., Form GW-1b1617 Mail Service Center-Raleigh, NC 27699-1617 Phone No. (919) 733·7015 ext 568. Rev. 7/05
--------
-----
NON RESIDENTIAL WELL CONSTRUCTION RECORD
North Carolina Departm~nt of Environment and Natural Resources-Division of Water QuaLity
WELL CONTRACTOR CERTIFICATJON #...;::3...:.:42::.:;6:- _
1. WELL CONTRACTOR:
Henry Nemargut
Well Contractor (Individual) Name
Henry Nemargut Engineering Services
Well Contractor Company Name
STREET ADDRESS 2211 Chestnut Street
Wilmington NC 28405
City or Town State Zip Code
~_ 762-5475
Area code- Phone number
2. WELL INFORMATION:
SITE WELL 10 #(if applicable),_M_W_-_6 _
STATE WELL PERMIT#(if applicable), _
DWQ or OTHER PERMIT #(if applicable) _
WELL USE (Check Applicable Box) Monitoring (gJ Municipal/Public 0
Industrial/CommercialO AgriculturalO Recovery 0 Injection [j
Irrigationo Other 0 (list use) _
DATE DRILLED._12_1_8/_2_01_6 _
TIME COMPLETED_1_2_:0_0 AM 0 PM ~
3. WELL LOCATION:
CITY: Wilson COUNTy_W~i1s:.:o.:..n _
3055 Stantonsburg Rd, Wilson, NC 27893
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code)
TOPOGRAPHIC I LAND SETTING
OSlope oValley g]Flat, ORidge OOther _
(check appropriate box)
~ _ 35.69099167 May be in degrees,LATITUDE minutes, seconds or
LONGITUDE 77.88775 in a decimal format
Latitude/longitude source: >0GPS oTopographic map
(location of well must be shown on a USGS tapa map and
attached to this form if not using GPS)
4. FACILlTY-is the name Of the business where the well is located,
FACILITY ID #(if applicable),_0-=---=-0=-24.:..,:5:.:8-=-9 _
NAME OF FACILlTY~Fr.:...:ie:.:.n:.:d:..:.ly...:M.:..:.a::.:rt..:.-_
STREET ADDRESS 3055 Stantonsburg Road
Wilson NC 27893
City or Town State Zip Code
CONTACT PERSON Raymond Bartholomew
MAILING ADDRESS,..:.P.:..,-=-O.:.....B::.:o:.:.x:..:7:.:0-=-6 _
Henderson NC 27536­
City or Town State Zip Code

(252 )__4_3_8_-7_1_4_1 _

Area code -Phone number

5. WELL DETAILS:
a. TOTALDEPTH:,__15_,5_' __
b. DOES WELL REPLACE EXISTING WELL? YES 0 NO IKJ
c. WATER LEVEL Below Top of Casing: 10.87' FT.

(Use "+" if Above Top of Casing)

d. TOP OF CASING IS 0' FT. Above Land Surface'
'Top of casing terminated at/or below land surface may require
a variance in accordance with 15A NCAC 2C .0118.
e. YIELD (gpm): METHOD OF TEST _
f. DISINFECTION: Type Amount _
g. WATER ZONES (depth)

From To___ From To _

From To___ From To _
From To___ From To _
6. CASING: Thicknessl

Depth Qiameter Weight
~-eJ~ialSch 40 From_O_'__ To_5_'__ Ft. 2 '

From To Ft. _

From To Ft. _

7. GROUT: Depth Material Method
From_O_'__ To_4_'__ Ft. Portland Pour

From To Ft. _

From To Ft. _

8. SCREEN: Depth Diameter Slot Size Material
From_5_'--To~Ft._2 __in. 0.01 in. PVC

From To Ft.in. in.

From To___ Ft in. in.

9, SAND/GRAVEL PACK:
Depth Size Material
From 4' To~ Ft. #2 Filter Sand
From Ft.To___
To___From Ft.
10. DRILLING LOG
From To Formation Description
0' 2' gray Silt w/sand & some clay
2' 6' orange-tan-red, Silt w/clay
6' 11' tan-orange, Silt w/clay
11' 16' orange-tan, Silt w/sand &clay
11. REMARKS:
12/28/2016
DATE
Submit the original to the Division of Water Quality within 30 days. Attn: Information Mgt., Form GW-1b 1617 Mail Service Center -Raleigh, NC 27699-1617 Phone No. [phone] ext 568. Rev. 7/05
---
---
---
---
-----
-----
---
NON RESIDENTIAL WELL CONSTRUCTION RECORD
North Carolina D~partment o'f Environ~lenl and Natural Resources-Division of Water Quality
WELL CONTRACTOR CERTIFICATION # ....:3~4:;.:26~ _
1. WELL CONTRACTOR:
Henry Nemargut
Well Contractor (Individual) Name
Henry Nemargut Engineering Services
Well Contractor Company Name
STREET ADDRESS 2211 Chestnut Street
Wilmington NC 28405
City or Town State Zip Code
~_ 762-5475
Area code-Phone number
20 WELL INFORMATION:
SITE WELL ID #(If appliCable),_M_W_-_7 _
STATE WELL PERMIT#(if appllcable), _
DWQ or OTHER PERMIT #(if applicable), _
WELL USE (Check Applicable Box) Monitoring IX] MunicipallPublic 0
Industrial/CommercialO AgriculturalO Recovery 0 Injection 0
Irrigationo Other 0 (list use) _
DATE DRILLED--.:..:12::..:/8::..:/2::..:0~1..:.6 _
TIME COMPLETED 3:00 AM 0 PM ~
30 WELL LOCATION:
CITY: Wilson COUNTy~W...:..::.:ils:..:o.:..:n _
3055 Stantonsburg Rd, Wilson, NC 27893
(Street Name, Numbers. Community, Subdivision, Lot No., Parcel, Zip Code)
TOPOGRAPHIC / LAND SETTING:
o Slope 0 Valley [] Flat 0 Ridge 0 Other _
(check appropriate box)
LATITUDE -L _ 35.69099167 May be in degrees,
minutes, seconds or
LONGITUDE 77.88775 in a decimal format
Latitude/longitude source: 0GPS oTopographic map

(location of well must be shown on a USG S tapa map and

attached to this form if not using GPS)

4. FACILITY· is the name of Ihe business where Ihe well is localed.
FACILITY 10 #(if applicable)_0=----=.02:.:4:..:5:..:.8..:.9 _
NAME OF FACI L1TY_F~r..::ie::..:n:.::d:.e.ly...:.M::..:a::rt.:.- _
STREET ADDRESS 3055 Stantonsburg Road
Wilson NC 27893
City or Town State Zip Code
CONTACT PERSON Raymond Bartholomew
MAILING ADDRESS,~P....:..:::.O..:..::..:Bo:.:x::..:7:....:0:..:6 _
Henderson NC 2753&
City or Town
(252 )_._4_3_8_-7_1_41
Area code -Phone number
State
_
Zip Code
5. WELL DETAILS:
ao TOTAL DEPTH:_1....:5~' _
bo DOES WELL REPLACE EXISTING WELL? YES 0 NO IZJ
c. WATER LEVEL Below Top of Casing: 10.76'
(Use "+" if Above Top of Casing)
FT.
d. TOP OF CASING IS 0' FT. Above Land Surface*
*Top of casing terminated aUor below land surface may require
a variance in accordance with 15A NCAC 2C .0118.
e. YIELD (gpm) METHOD OF TEST
f. DISINFECTION: Type Amount
g. WATER ZONES (depth):

From---From--­To___ To___
From To From---------To--­
From From--­To___ To___
6. CASING: Thickness/
Depth Riameter ~eigh6 ~ei~ial From_O_'__ To_5_'__ Ft. 2' cM 4

From To___ Ft.

From---To Ft.

7. GROUT: Depth Material Method
0' 4' Portland PourFrom___ To___ Ft.

From---Ft.
To___

From To___ Ft.

80 SCREEN: Depth Diameter Slot Size Material
From_5_'__ To_1_5_'_ Ft._2__in. 0.01 in. PVC

From To___ Ft in. in.

From To___ Ft. in. in.

90 SAND/GRAVEL PACK:
Depth Size Material
From 4' To_1_5'__ Ft. #2 Filter Sand
From To Ft.
From To___ Ft.
100 DRILLING LOG
From To Formation Description
0' 2' It. brown, Sand w/silt
2' 4" It. brown. Clay lsi 11
4' 6' gray, Clay w/silt
6' 9' red-brown, Silt w/clay
9' 12' tan, Silt w/clay
12' 15' beige-brawn-tan, Silt w/sand & clay
110 REMARKS:
12/28/2016
DATE
Submit the original to the Division of Water Quality within 30 days. Attn: Information Mgt., Form GW-1b1617 Mail Service Center -Raleigh, NC 27699-1617 Phone No. (919) 733·7015 ext 568. Rev. 7/05
------
--
NONRESIDENTIAL WELL CO TSTRUCTION RECORD ..
North Carolina Department of Environment and Natural Resourees-Division of Water Quality
WELL CONTRACTOR CERTIFICATION # ....::3:....:.4::;26::.-....~ _
1. WELL CONTRACTOR:
Henry Nemargut
Well Contractor (Individual) Name
Henry Nemargut Engineering Services
Well Contractor Company Name
STREET ADDRESS 2211 Chestnut Street
Wilmington NC 28405
City or Town State Zip Code
~. 762-5475

Area code· Phone number

2. WELL INFORMATION:
SITE WELL ID #(if applicable)_M_W_-8

STATE WELL PERMIT#(ifapplicable),

DWQ or OTHER PERMIT #(if applicable)
WELL USE (Check Applicable Box) Monitoring I&J Municipal/Public 0
Industrial/CommercialD AgriculturalD Recovery 0 Injection 0
IrrigationD Other 0 (list use)
DATE DRILLED_12_/8_/_20_1_6
TIME COMPLETED_6_:0_0
3. WELL LOCATION:
CITY: Wilson
3055 Stantonsburg Rd, Wilson, NC
(Street Name. Numbers. Community. Subdivision. Lot No.. Parcel. Zip Code)
TOPOGRAPHIC / LAND SETTING:
DSlope DValley KJFlat DRidge DOther _
(check appropriate box)
-L _ 3569099167LATITUDE Mav be in degrees,
minutes, seconds or
LONGITUDE 77.88775 in a decimal format
Latitude/longitude source: €lGPS o Topographic map
(location of well must be shown on a USGS tapa map and
attached to this form if not using GPS)
4. FACILITY-is the name of the business where the well is located.
FACILITY ID #(if applicable)_0=-.~02=-4:...:5..:.8~9 _
NAME OF FACILlTY...:F...:r.:..:ie::..:n:.::d~ly...:.M::..:a:.:.rt..:....... _
STREET ADDRESS 3055 Stantonsburg Road
Wilson NC 27893
City or Town State Zip Code
CONTACT PERSON Raymond Bartholomew
MAILING ADDRESS,...:P:...:...:.O.:....B=-0:.:.x:.:7-=0..:.6 _
Henderson NC 27536­
City or Town State
(252 )__4_3_8_.7_1_4_1 _
Area code -Phone number
5. WELL DETAILS:
a. TOTALDEPTH:.__14_._5' __
b. DOES WELL REPLACE EXISTING WELL?
c. WATER LEVEL Below Top of Casing: 10.18'
(Use "+" if Above Top of Casing)
_
_
AM 0 PM ~
COUNTY,..:W...:..;;.:ils:...:o,..:n _
27893
Zip Code
YES 0 NO I6J
FT.
_
_
_
d. TOP OF CASING IS 0' FT. Above Land Surface*
*Top of casing terminated aVor below land surface may require
a variance in accordance with 15A NCAC 2C .0118.
e. YIELD (gpm): METHOD OF TEST _
f. DISINFECTION: Type
g. WATER ZONES (depth):
From To___ From
From To___ From
From To___ From
6. CASING:
Depth Qiameter
From_O_'__ To~Ft. 2'
From To Ft.
From---Ft.To___
7. GROUT: Depth Material
0' PortlandFrom___ To_3_'__ Ft.
From---Ft.To--­
From--­
8. SCREEN:
From_4_'__
From--­
From--­
9. SAND/GRAVEL PACK:
Depth Size
From,_3:::..'__To~Ft. #2
From, To

From To

10. DRILLING LOG
From To
0' l'
l' 3'
3' 7'
7' 10'
10' 14'
14' 15'
11. REMARKS:
I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
15A NCAC 2C. WELL CONSTRUCnO STANDARDS, AND THAT A COpy OF THIS
RECOR HAS BEEN PROVIDED TO THE ELL OWNER.
12/28/2016
DATE
STRUCTING THE WELL
To___ Ft.
Depth Diameter
To~Ft._2__in.
To___ Ft in.
To___ Ft.--in.
Ft..

Ft..

Formation Description
brown Sand w/silt
gray. Silt wlclay
red-brown, Clay wlsilt
red-tan, Clay wlsand
beige-tan, Sand w/cray
tan, Silt w/sand
Slot Size Material
0.01 in. PVC
in.
in.
Material
Filter Sand
_
---''-­
Amount _
To _

To _

To _

Thickness/
~eigh6 ~(}crialen 4
Method
Pour
Submit the original to the Division of Water Quality within 30 days. Attn: Information Mgt., Form GW-1b1617 Mail Service Center-Raleigh, NC 27699-1617 Phone No. [phone] ext 568. Rev. 7/05
---
---
-----
---
NON RESIDENTIAL WELL CONSTRUCTION RECORD. .
North Carolina Department of Environment and Natural Resources-Division of Water Quality
WELL CONTRACTOR CERTIFICAnON # ..::3:..:,4::::26=----- _
1. WELL CONTRACTOR:
Henry Nemargut

Well Contractor (Individual) Name

Henry Nemargut Engineering Services

Well Contractor Company Name

STREET ADDRESS 2211 Chestnut Street
Wilmington NC 28405

City or Town State Zip Code

~_ 762-5475

Area code-Phone number

2. WELL INFORMATION:
SITE WELL 10 #(if applicable),_M_W_,_9 _
STATE WELL PERMIT#(if applicable), _
DWQ or OTHER PERMIT #(if applicable) _
WELL USE (Check Applicable Box) Monitoring (gJ Municipal/Public 0
Industrial/CommercialD AgriculturalD Recovery 0 Injection 0

IrrigationD Other 0 (list use) _

DATE DRILLED._1_2/_8/_2_01_6 _
TIME COMPLETED 12:00 -12/9/16 AM 0 PM ~
3. WELL LOCATION:
CITY: Wilson COUNTY..,:W.-:--.:ils:..;,o_n _
3055 Stantonsburg Rd, Wilson, NC 27893
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code)
TOPOGRAPHIC / LAND SETTING:
DSlope oValley OFlat DRidge DOther _
(check appropriate box)
LATITUDE ...l-_ 35.69099167 May be in degrees,
minutes, seconds or
LONGITUDE 77.88775 in a decimal fonmat
Latitude/longitude source: J0 GPS 0 Topographic map
(/ocation of well must be shown on a USGS topo map and
attached to this form if not using GPS)
4. FACILITY, is the name of the business where the well is located.
FACILITY ID #(if applicable)_0:..,...:02_4_5.:.8...:9 _
NAME OF FACI L1TY_F...:r.:.:ie:.:.n~d~ly...:M:.:.a:..rt.:.- _
STREET ADDRESS 3055 Stantonsburg Road
Wilson NC 27893

City or Town State Zip Code

CONTACT PERSON Raymond Bartholomew
MAILING ADDRESS,_P_.~O...:.B=..0:.:.x:.:.7..:0.:.6 _

Henderson NC 2753&

City or Town State Zip Code

(252 )__4_3_8_-7_1_4_1 _

Area code -Phone number

5. WELL DETAILS:
a. TOTAL DEPTH:_1_5_' _
b. DOES WELL REPLACE EXISTING WELL? YES 0 NO IZJ
c. WATER LEVEL Below Top of Casing: 9.07' FT.

(Use "+" if Above Top of Casing)

d. TOP OF CASING IS 0' FT. Above Land Suliace*
*Top of casing terminated at/or below land suliace may require
a variance in accordance with 15A NCAC 2C .0118.
e. YIELD (gpm): METHOD OF TEST _
f. DISINFECTION: Type Amount _
g. WATER ZONES (depth):
From To___ From To _
From To___ From To _
From To___ From To _
6. CASING: Thickness/

Depth Riameter ~eigh6 ~~Eial
cH 4From_O_'__ To_5_'__ Ft. 2'

From To___ Ft.

From---Ft.
To___
7. GROUT: Depth Material Method
0' 4' Portland PourFrom___ To___ Ft.

From---To___ Ft.

From To___ Ft.

8. SCREEN: Depth Diameter Slot Size Material
From_5_'__ To_1_5_'_ Ft._2__in. 0.01 in. PVC
From Ft.in. in.To___

From Ft.---in. in.
To___
9. SAND/GRAVEL PACK:
Depth Size Material
From 4' To_1_5'__ Ft. #2 Filter Sand

From To Ft. _

From To Ft.. -C:._
10. DRILLING LOG
From To Fonmation Description
0' l' gray Gravel (ABC)
l' 4' gray'brown, Clay w/silt
4' 7' red-brown, Silt w/clay & little sand
7' 9' beige-gray, Silt w/clay & little sand
9' 13' beige-tan, Silt w/clay & little sand
13' 15' beige, Silt w/clay & little sand
11. REMARKS:
12/28/2016
DATE
Submit the original to the Division of Water Quality within 30 days. Attn: Information Mgt., Form GW-1b1617 Mail Service Center -Raleigh, NC 27699-1617 Phone No. [phone] ext 568. Rev. 7/05
List all applicable well permits (i.e. County, State, Variance, etc.)
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
For multiple injection or non-water supply wells ONLY with the same construction, you can
submit one form.
For multiple wells list all depths if different (example- 3@200’ and 2@100
If water level is above casing, use “+”
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner. _______________
80 rock
Bryan Vest
3580
Ransier Environmental Drilling, Inc.

9/9/16 VEW-1
Friendly Mart
3055 Old Stantonburg Rd Wilson
Wilson
35 39.50 77 52.34
1
80
39
8"/5
air hammer
0 69 5 sch 40 PVC
0 75 2 sch 40
75 80 2 .010 sch 40
0 69 neat cement tremmie
0 71 neat cement tremmie
73 80 medium quartz pour
0 10 silty sl sandy clay
10 16 silty clay
16 20 clayey silt
20 30 silty clay
30 71 clayey silt
71 74 clay weathered rock
74
Page - 13

APPENDIX C

GROUNDWATER

ANALYTICAL RESULTS

#=CL#
December 16, 2016
LIMS USE: FR - HENRY NEMARGUT
LIMS OBJECT ID: 92322865
92322865
Project:
Pace Project No.:
RE:
Henry Nemargut
Henry Nemargut Engineering
2211 Chestnut Street
Wilmington, NC 28405
Fiendly Mart
Dear Henry Nemargut:
Enclosed are the analytical results for sample(s) received by the laboratory on December 09, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 48
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92322865
Fiendly Mart
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 48
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92322865
Fiendly Mart
Lab ID Sample ID Matrix Date Collected Date Received
92322865001 SW1 Water 12/08/16 16:00 12/09/16 08:00
92322865002 MW1 Water 12/08/16 18:00 12/09/16 08:00
92322865003 MW2 Water 12/08/16 18:15 12/09/16 08:00
92322865004 MW4 Water 12/08/16 18:30 12/09/16 08:00
92322865005 MW5 Water 12/08/16 18:45 12/09/16 08:00
92322865006 MW6 Water 12/08/16 19:00 12/09/16 08:00
92322865007 MW7 Water 12/08/16 19:20 12/09/16 08:00
92322865008 MW8 Water 12/08/16 19:35 12/09/16 08:00
92322865009 MW9 Water 12/08/16 19:50 12/09/16 08:00
92322865010 VEW1 Water 12/08/16 20:30 12/09/16 08:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 48
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92322865
Fiendly Mart
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92322865001 SW1 SM 6200B 63 PASI-CCAH
92322865002 MW1 MADEP VPH 5 PASI-CWDV
EPA 6010 1 PASI-ASH1
SM 6200B 63 PASI-CCAH
92322865003 MW2 MADEP VPH 5 PASI-CWDV
EPA 6010 1 PASI-ASH1
SM 6200B 63 PASI-CCAH
92322865004 MW4 MADEP VPH 5 PASI-CWDV
EPA 6010 1 PASI-ASH1
SM 6200B 63 PASI-CCAH
92322865005 MW5 MADEP VPH 5 PASI-CWDV
EPA 6010 1 PASI-ASH1
SM 6200B 63 PASI-CCAH
92322865006 MW6 MADEP VPH 5 PASI-CWDV
EPA 6010 1 PASI-ASH1
SM 6200B 63 PASI-CCAH
92322865007 MW7 MADEP VPH 5 PASI-CWDV
EPA 6010 1 PASI-ASH1
SM 6200B 63 PASI-CCAH
92322865008 MW8 MADEP VPH 5 PASI-CWDV
EPA 6010 1 PASI-ASH1
SM 6200B 63 PASI-CCAH
92322865009 MW9 MADEP VPH 5 PASI-CWDV
EPA 6010 1 PASI-ASH1
SM 6200B 63 PASI-CCAH
92322865010 VEW1 MADEP VPH 5 PASI-CWDV
EPA 6010 1 PASI-ASH1
SM 6200B 63 PASI-CCAH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 48
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92322865
Fiendly Mart
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92322865001 SW1
Methyl-tert-butyl ether 1.3 ug/L 12/11/16 21:020.50SM 6200B
92322865002 MW1
Aliphatic (C05-C08) 65.0 ug/L 12/12/16 01:18 N250.0MADEP VPH
Aromatic (C09-C10) 89.6 ug/L 12/12/16 01:18 N250.0MADEP VPH
n-Butylbenzene 0.55 ug/L 12/12/16 00:270.50SM 6200B
sec-Butylbenzene 0.80 ug/L 12/12/16 00:270.50SM 6200B
Isopropylbenzene (Cumene) 15.7 ug/L 12/12/16 00:270.50SM 6200B
Methyl-tert-butyl ether 2.9 ug/L 12/12/16 00:270.50SM 6200B
n-Propylbenzene 1.1 ug/L 12/12/16 00:270.50SM 6200B
92322865003 MW2
Aromatic (C09-C10) 118 ug/L 12/12/16 01:45 N250.0MADEP VPH
Ethylbenzene 0.69 ug/L 12/12/16 00:440.50SM 6200B
n-Propylbenzene 0.60 ug/L 12/12/16 00:440.50SM 6200B
1,2,4-Trimethylbenzene 3.7 ug/L 12/12/16 00:440.50SM 6200B
1,3,5-Trimethylbenzene 3.9 ug/L 12/12/16 00:440.50SM 6200B
o-Xylene 0.64 ug/L 12/12/16 00:440.50SM 6200B
92322865004 MW4
Aliphatic (C05-C08) 11900 ug/L 12/12/16 17:31 N210000MADEP VPH
Aliphatic (C09-C12) 23400 ug/L 12/12/16 17:31 N210000MADEP VPH
Aromatic (C09-C10) 15100 ug/L 12/12/16 17:31 N210000MADEP VPH
Benzene 1540 ug/L 12/11/16 22:1012.5SM 6200B
Diisopropyl ether 135 ug/L 12/11/16 22:1012.5SM 6200B
Ethylbenzene 3040 ug/L 12/11/16 22:1012.5SM 6200B
Isopropylbenzene (Cumene) 174 ug/L 12/11/16 22:1012.5SM 6200B
Methyl-tert-butyl ether 848 ug/L 12/11/16 22:1012.5SM 6200B
Naphthalene 844 ug/L 12/11/16 22:1050.0SM 6200B
n-Propylbenzene 490 ug/L 12/11/16 22:1012.5SM 6200B
Toluene 1970 ug/L 12/11/16 22:1012.5SM 6200B
1,2,4-Trimethylbenzene 3240 ug/L 12/11/16 22:1012.5SM 6200B
1,3,5-Trimethylbenzene 892 ug/L 12/11/16 22:1012.5SM 6200B
m&p-Xylene 6770 ug/L 12/11/16 22:1025.0SM 6200B
o-Xylene 1400 ug/L 12/11/16 22:1012.5SM 6200B
92322865005 MW5
Aliphatic (C05-C08) 289 ug/L 12/12/16 18:54 N250.0MADEP VPH
Benzene 6.5 ug/L 12/12/16 07:500.50SM 6200B
Methyl-tert-butyl ether 176 ug/L 12/12/16 07:500.50SM 6200B
Naphthalene 5.5 ug/L 12/12/16 07:502.0SM 6200B
o-Xylene 0.61 ug/L 12/12/16 07:500.50SM 6200B
92322865006 MW6
Aliphatic (C05-C08) 578 ug/L 12/12/16 03:07 N250.0MADEP VPH
Diisopropyl ether 25.4 ug/L 12/12/16 19:481.2SM 6200B
Methylene Chloride 5.4 ug/L 12/12/16 19:48 C95.0SM 6200B
Methyl-tert-butyl ether 364 ug/L 12/12/16 19:481.2SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 48
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92322865
Fiendly Mart
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92322865007 MW7
Aliphatic (C05-C08) 387 ug/L 12/12/16 03:35 N250.0MADEP VPH
Benzene 0.97 ug/L 12/12/16 14:250.50SM 6200B
Diisopropyl ether 33.1 ug/L 12/12/16 14:250.50SM 6200B
Methyl-tert-butyl ether 191 ug/L 12/12/16 14:250.50SM 6200B
92322865008 MW8
Benzene 0.96 ug/L 12/12/16 19:310.50SM 6200B
Diisopropyl ether 2.0 ug/L 12/12/16 19:310.50SM 6200B
Methyl-tert-butyl ether 8.2 ug/L 12/12/16 19:310.50SM 6200B
92322865009 MW9
Aliphatic (C05-C08) 140000 ug/L 12/12/16 17:01 N225000MADEP VPH
Aliphatic (C09-C12) 26100 ug/L 12/12/16 17:01 N225000MADEP VPH
Benzene 14000 ug/L 12/12/16 17:32125SM 6200B
Diisopropyl ether 778 ug/L 12/12/16 17:32125SM 6200B
Ethylbenzene 4130 ug/L 12/12/16 17:32125SM 6200B
Isopropylbenzene (Cumene) 175 ug/L 12/12/16 17:32125SM 6200B
Methyl-tert-butyl ether 6240 ug/L 12/12/16 17:32125SM 6200B
Naphthalene 571 ug/L 12/12/16 17:32500SM 6200B
n-Propylbenzene 471 ug/L 12/12/16 17:32125SM 6200B
Toluene 43100 ug/L 12/12/16 17:32125SM 6200B
1,2,4-Trimethylbenzene 2860 ug/L 12/12/16 17:32125SM 6200B
1,3,5-Trimethylbenzene 736 ug/L 12/12/16 17:32125SM 6200B
m&p-Xylene 13600 ug/L 12/12/16 17:32250SM 6200B
o-Xylene 6350 ug/L 12/12/16 17:32125SM 6200B
92322865010 VEW1
Aliphatic (C05-C08) 66.3 ug/L 12/13/16 20:42 N250.0MADEP VPH
Benzene 0.61 ug/L 12/12/16 19:140.50SM 6200B
Chloroform 7.0 ug/L 12/12/16 19:140.50SM 6200B
Ethylbenzene 0.51 ug/L 12/12/16 19:140.50SM 6200B
Methyl-tert-butyl ether 0.76 ug/L 12/12/16 19:140.50SM 6200B
Toluene 0.70 ug/L 12/12/16 19:140.50SM 6200B
1,2,4-Trimethylbenzene 1.0 ug/L 12/12/16 19:140.50SM 6200B
m&p-Xylene 1.7 ug/L 12/12/16 19:141.0SM 6200B
o-Xylene 0.99 ug/L 12/12/16 19:140.50SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92322865
Fiendly Mart
Sample: SW1 Lab ID: 92322865001 Collected: 12/08/16 16:00 Received: 12/09/16 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 12/11/16 21:02 71-43-20.50 1
Bromobenzene ND ug/L 12/11/16 21:02 108-86-10.50 1
Bromochloromethane ND ug/L 12/11/16 21:02 74-97-50.50 1
Bromodichloromethane ND ug/L 12/11/16 21:02 75-27-40.50 1
Bromoform ND ug/L 12/11/16 21:02 75-25-20.50 1
Bromomethane ND ug/L 12/11/16 21:02 74-83-95.0 1
n-Butylbenzene ND ug/L 12/11/16 21:02 104-51-80.50 1
sec-Butylbenzene ND ug/L 12/11/16 21:02 135-98-80.50 1
tert-Butylbenzene ND ug/L 12/11/16 21:02 98-06-60.50 1
Carbon tetrachloride ND ug/L 12/11/16 21:02 56-23-50.50 1
Chlorobenzene ND ug/L 12/11/16 21:02 108-90-70.50 1
Chloroethane ND ug/L 12/11/16 21:02 75-00-31.0 1
Chloroform ND ug/L 12/11/16 21:02 67-66-30.50 1
Chloromethane ND ug/L 12/11/16 21:02 74-87-31.0 1
2-Chlorotoluene ND ug/L 12/11/16 21:02 95-49-80.50 1
4-Chlorotoluene ND ug/L 12/11/16 21:02 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 12/11/16 21:02 96-12-81.0 1
Dibromochloromethane ND ug/L 12/11/16 21:02 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 12/11/16 21:02 106-93-40.50 1
Dibromomethane ND ug/L 12/11/16 21:02 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 12/11/16 21:02 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 12/11/16 21:02 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 12/11/16 21:02 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 12/11/16 21:02 75-71-80.50 1
1,1-Dichloroethane ND ug/L 12/11/16 21:02 75-34-30.50 1
1,2-Dichloroethane ND ug/L 12/11/16 21:02 107-06-20.50 1
1,1-Dichloroethene ND ug/L 12/11/16 21:02 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 12/11/16 21:02 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 12/11/16 21:02 156-60-50.50 1
1,2-Dichloropropane ND ug/L 12/11/16 21:02 78-87-50.50 1
1,3-Dichloropropane ND ug/L 12/11/16 21:02 142-28-90.50 1
2,2-Dichloropropane ND ug/L 12/11/16 21:02 594-20-70.50 1
1,1-Dichloropropene ND ug/L 12/11/16 21:02 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 12/11/16 21:02 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 12/11/16 21:02 10061-02-60.50 1
Diisopropyl ether ND ug/L 12/11/16 21:02 108-20-30.50 1
Ethylbenzene ND ug/L 12/11/16 21:02 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 12/11/16 21:02 87-68-32.0 1
Isopropylbenzene (Cumene) ND ug/L 12/11/16 21:02 98-82-80.50 1
Methylene Chloride ND ug/L 12/11/16 21:02 75-09-22.0 1
Methyl-tert-butyl ether 1.3 ug/L 12/11/16 21:02 1634-04-40.50 1
Naphthalene ND ug/L 12/11/16 21:02 91-20-32.0 1
n-Propylbenzene ND ug/L 12/11/16 21:02 103-65-10.50 1
Styrene ND ug/L 12/11/16 21:02 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 12/11/16 21:02 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 12/11/16 21:02 79-34-50.50 1
Tetrachloroethene ND ug/L 12/11/16 21:02 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92322865
Fiendly Mart
Sample: SW1 Lab ID: 92322865001 Collected: 12/08/16 16:00 Received: 12/09/16 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 12/11/16 21:02 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 12/11/16 21:02 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 12/11/16 21:02 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 12/11/16 21:02 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 12/11/16 21:02 79-00-50.50 1
Trichloroethene ND ug/L 12/11/16 21:02 79-01-60.50 1
Trichlorofluoromethane ND ug/L 12/11/16 21:02 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/11/16 21:02 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 12/11/16 21:02 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 12/11/16 21:02 108-67-80.50 1
Vinyl chloride ND ug/L 12/11/16 21:02 75-01-41.0 1
m&p-Xylene ND ug/L 12/11/16 21:02 179601-23-11.0 1
o-Xylene ND ug/L 12/11/16 21:02 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 98 % 12/11/16 21:02 17060-07-070-130 1
4-Bromofluorobenzene (S) 95 % 12/11/16 21:02 460-00-470-130 1
Toluene-d8 (S) 101 % 12/11/16 21:02 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92322865
Fiendly Mart
Sample: MW1 Lab ID: 92322865002 Collected: 12/08/16 18:00 Received: 12/09/16 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: MADEP VPHVPH NC Water
Aliphatic (C05-C08)65.0 ug/L 12/12/16 01:18 N250.0 1
Aliphatic (C09-C12) ND ug/L 12/12/16 01:18 N250.0 1
Aromatic (C09-C10)89.6 ug/L 12/12/16 01:18 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S) 95 % 12/12/16 01:18 460-00-470-130 1
4-Bromofluorobenzene (PID) (S) 101 % 12/12/16 01:18 460-00-470-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Lead ND ug/L 12/15/16 15:32 7439-92-112/11/16 11:205.0 1
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 12/12/16 00:27 71-43-20.50 1
Bromobenzene ND ug/L 12/12/16 00:27 108-86-10.50 1
Bromochloromethane ND ug/L 12/12/16 00:27 74-97-50.50 1
Bromodichloromethane ND ug/L 12/12/16 00:27 75-27-40.50 1
Bromoform ND ug/L 12/12/16 00:27 75-25-20.50 1
Bromomethane ND ug/L 12/12/16 00:27 74-83-95.0 1
n-Butylbenzene 0.55 ug/L 12/12/16 00:27 104-51-80.50 1
sec-Butylbenzene 0.80 ug/L 12/12/16 00:27 135-98-80.50 1
tert-Butylbenzene ND ug/L 12/12/16 00:27 98-06-60.50 1
Carbon tetrachloride ND ug/L 12/12/16 00:27 56-23-50.50 1
Chlorobenzene ND ug/L 12/12/16 00:27 108-90-70.50 1
Chloroethane ND ug/L 12/12/16 00:27 75-00-31.0 1
Chloroform ND ug/L 12/12/16 00:27 67-66-30.50 1
Chloromethane ND ug/L 12/12/16 00:27 74-87-31.0 1
2-Chlorotoluene ND ug/L 12/12/16 00:27 95-49-80.50 1
4-Chlorotoluene ND ug/L 12/12/16 00:27 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 12/12/16 00:27 96-12-81.0 1
Dibromochloromethane ND ug/L 12/12/16 00:27 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 12/12/16 00:27 106-93-40.50 1
Dibromomethane ND ug/L 12/12/16 00:27 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 12/12/16 00:27 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 12/12/16 00:27 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 12/12/16 00:27 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 12/12/16 00:27 75-71-80.50 1
1,1-Dichloroethane ND ug/L 12/12/16 00:27 75-34-30.50 1
1,2-Dichloroethane ND ug/L 12/12/16 00:27 107-06-20.50 1
1,1-Dichloroethene ND ug/L 12/12/16 00:27 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 12/12/16 00:27 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 12/12/16 00:27 156-60-50.50 1
1,2-Dichloropropane ND ug/L 12/12/16 00:27 78-87-50.50 1
1,3-Dichloropropane ND ug/L 12/12/16 00:27 142-28-90.50 1
2,2-Dichloropropane ND ug/L 12/12/16 00:27 594-20-70.50 1
1,1-Dichloropropene ND ug/L 12/12/16 00:27 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 12/12/16 00:27 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 12/12/16 00:27 10061-02-60.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92322865
Fiendly Mart
Sample: MW1 Lab ID: 92322865002 Collected: 12/08/16 18:00 Received: 12/09/16 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Diisopropyl ether ND ug/L 12/12/16 00:27 108-20-30.50 1
Ethylbenzene ND ug/L 12/12/16 00:27 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 12/12/16 00:27 87-68-32.0 1
Isopropylbenzene (Cumene)15.7 ug/L 12/12/16 00:27 98-82-80.50 1
Methylene Chloride ND ug/L 12/12/16 00:27 75-09-22.0 1
Methyl-tert-butyl ether 2.9 ug/L 12/12/16 00:27 1634-04-40.50 1
Naphthalene ND ug/L 12/12/16 00:27 91-20-32.0 1
n-Propylbenzene 1.1 ug/L 12/12/16 00:27 103-65-10.50 1
Styrene ND ug/L 12/12/16 00:27 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 12/12/16 00:27 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 12/12/16 00:27 79-34-50.50 1
Tetrachloroethene ND ug/L 12/12/16 00:27 127-18-40.50 1
Toluene ND ug/L 12/12/16 00:27 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 12/12/16 00:27 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 12/12/16 00:27 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 12/12/16 00:27 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 12/12/16 00:27 79-00-50.50 1
Trichloroethene ND ug/L 12/12/16 00:27 79-01-60.50 1
Trichlorofluoromethane ND ug/L 12/12/16 00:27 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/12/16 00:27 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 12/12/16 00:27 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 12/12/16 00:27 108-67-80.50 1
Vinyl chloride ND ug/L 12/12/16 00:27 75-01-41.0 1
m&p-Xylene ND ug/L 12/12/16 00:27 179601-23-11.0 1
o-Xylene ND ug/L 12/12/16 00:27 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 103 % 12/12/16 00:27 17060-07-070-130 1
4-Bromofluorobenzene (S) 98 % 12/12/16 00:27 460-00-470-130 1
Toluene-d8 (S) 100 % 12/12/16 00:27 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92322865
Fiendly Mart
Sample: MW2 Lab ID: 92322865003 Collected: 12/08/16 18:15 Received: 12/09/16 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: MADEP VPHVPH NC Water
Aliphatic (C05-C08) ND ug/L 12/12/16 01:45 N250.0 1
Aliphatic (C09-C12) ND ug/L 12/12/16 01:45 N250.0 1
Aromatic (C09-C10)118 ug/L 12/12/16 01:45 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S) 93 % 12/12/16 01:45 460-00-470-130 1
4-Bromofluorobenzene (PID) (S) 99 % 12/12/16 01:45 460-00-470-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Lead ND ug/L 12/15/16 15:35 7439-92-112/11/16 11:205.0 1
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 12/12/16 00:44 71-43-20.50 1
Bromobenzene ND ug/L 12/12/16 00:44 108-86-10.50 1
Bromochloromethane ND ug/L 12/12/16 00:44 74-97-50.50 1
Bromodichloromethane ND ug/L 12/12/16 00:44 75-27-40.50 1
Bromoform ND ug/L 12/12/16 00:44 75-25-20.50 1
Bromomethane ND ug/L 12/12/16 00:44 74-83-95.0 1
n-Butylbenzene ND ug/L 12/12/16 00:44 104-51-80.50 1
sec-Butylbenzene ND ug/L 12/12/16 00:44 135-98-80.50 1
tert-Butylbenzene ND ug/L 12/12/16 00:44 98-06-60.50 1
Carbon tetrachloride ND ug/L 12/12/16 00:44 56-23-50.50 1
Chlorobenzene ND ug/L 12/12/16 00:44 108-90-70.50 1
Chloroethane ND ug/L 12/12/16 00:44 75-00-31.0 1
Chloroform ND ug/L 12/12/16 00:44 67-66-30.50 1
Chloromethane ND ug/L 12/12/16 00:44 74-87-31.0 1
2-Chlorotoluene ND ug/L 12/12/16 00:44 95-49-80.50 1
4-Chlorotoluene ND ug/L 12/12/16 00:44 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 12/12/16 00:44 96-12-81.0 1
Dibromochloromethane ND ug/L 12/12/16 00:44 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 12/12/16 00:44 106-93-40.50 1
Dibromomethane ND ug/L 12/12/16 00:44 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 12/12/16 00:44 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 12/12/16 00:44 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 12/12/16 00:44 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 12/12/16 00:44 75-71-80.50 1
1,1-Dichloroethane ND ug/L 12/12/16 00:44 75-34-30.50 1
1,2-Dichloroethane ND ug/L 12/12/16 00:44 107-06-20.50 1
1,1-Dichloroethene ND ug/L 12/12/16 00:44 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 12/12/16 00:44 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 12/12/16 00:44 156-60-50.50 1
1,2-Dichloropropane ND ug/L 12/12/16 00:44 78-87-50.50 1
1,3-Dichloropropane ND ug/L 12/12/16 00:44 142-28-90.50 1
2,2-Dichloropropane ND ug/L 12/12/16 00:44 594-20-70.50 1
1,1-Dichloropropene ND ug/L 12/12/16 00:44 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 12/12/16 00:44 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 12/12/16 00:44 10061-02-60.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92322865
Fiendly Mart
Sample: MW2 Lab ID: 92322865003 Collected: 12/08/16 18:15 Received: 12/09/16 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Diisopropyl ether ND ug/L 12/12/16 00:44 108-20-30.50 1
Ethylbenzene 0.69 ug/L 12/12/16 00:44 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 12/12/16 00:44 87-68-32.0 1
Isopropylbenzene (Cumene) ND ug/L 12/12/16 00:44 98-82-80.50 1
Methylene Chloride ND ug/L 12/12/16 00:44 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 12/12/16 00:44 1634-04-40.50 1
Naphthalene ND ug/L 12/12/16 00:44 91-20-32.0 1
n-Propylbenzene 0.60 ug/L 12/12/16 00:44 103-65-10.50 1
Styrene ND ug/L 12/12/16 00:44 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 12/12/16 00:44 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 12/12/16 00:44 79-34-50.50 1
Tetrachloroethene ND ug/L 12/12/16 00:44 127-18-40.50 1
Toluene ND ug/L 12/12/16 00:44 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 12/12/16 00:44 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 12/12/16 00:44 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 12/12/16 00:44 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 12/12/16 00:44 79-00-50.50 1
Trichloroethene ND ug/L 12/12/16 00:44 79-01-60.50 1
Trichlorofluoromethane ND ug/L 12/12/16 00:44 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/12/16 00:44 96-18-40.50 1
1,2,4-Trimethylbenzene 3.7 ug/L 12/12/16 00:44 95-63-60.50 1
1,3,5-Trimethylbenzene 3.9 ug/L 12/12/16 00:44 108-67-80.50 1
Vinyl chloride ND ug/L 12/12/16 00:44 75-01-41.0 1
m&p-Xylene ND ug/L 12/12/16 00:44 179601-23-11.0 1
o-Xylene 0.64 ug/L 12/12/16 00:44 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 105 % 12/12/16 00:44 17060-07-070-130 1
4-Bromofluorobenzene (S) 97 % 12/12/16 00:44 460-00-470-130 1
Toluene-d8 (S) 101 % 12/12/16 00:44 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92322865
Fiendly Mart
Sample: MW4 Lab ID: 92322865004 Collected: 12/08/16 18:30 Received: 12/09/16 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: MADEP VPHVPH NC Water
Aliphatic (C05-C08)11900 ug/L 12/12/16 17:31 N210000 200
Aliphatic (C09-C12)23400 ug/L 12/12/16 17:31 N210000 200
Aromatic (C09-C10)15100 ug/L 12/12/16 17:31 N210000 200
Surrogates
4-Bromofluorobenzene (FID) (S) 104 % 12/12/16 17:31 460-00-470-130 200
4-Bromofluorobenzene (PID) (S) 110 % 12/12/16 17:31 460-00-470-130 200
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Lead ND ug/L 12/15/16 15:38 7439-92-112/11/16 11:205.0 1
Analytical Method: SM 6200B6200B MSV
Benzene 1540 ug/L 12/11/16 22:10 71-43-212.5 25
Bromobenzene ND ug/L 12/11/16 22:10 108-86-112.5 25
Bromochloromethane ND ug/L 12/11/16 22:10 74-97-512.5 25
Bromodichloromethane ND ug/L 12/11/16 22:10 75-27-412.5 25
Bromoform ND ug/L 12/11/16 22:10 75-25-212.5 25
Bromomethane ND ug/L 12/11/16 22:10 74-83-9125 25
n-Butylbenzene ND ug/L 12/11/16 22:10 104-51-812.5 25
sec-Butylbenzene ND ug/L 12/11/16 22:10 135-98-812.5 25
tert-Butylbenzene ND ug/L 12/11/16 22:10 98-06-612.5 25
Carbon tetrachloride ND ug/L 12/11/16 22:10 56-23-512.5 25
Chlorobenzene ND ug/L 12/11/16 22:10 108-90-712.5 25
Chloroethane ND ug/L 12/11/16 22:10 75-00-325.0 25
Chloroform ND ug/L 12/11/16 22:10 67-66-312.5 25
Chloromethane ND ug/L 12/11/16 22:10 74-87-325.0 25
2-Chlorotoluene ND ug/L 12/11/16 22:10 95-49-812.5 25
4-Chlorotoluene ND ug/L 12/11/16 22:10 106-43-412.5 25
1,2-Dibromo-3-chloropropane ND ug/L 12/11/16 22:10 96-12-825.0 25
Dibromochloromethane ND ug/L 12/11/16 22:10 124-48-112.5 25
1,2-Dibromoethane (EDB) ND ug/L 12/11/16 22:10 106-93-412.5 25
Dibromomethane ND ug/L 12/11/16 22:10 74-95-312.5 25
1,2-Dichlorobenzene ND ug/L 12/11/16 22:10 95-50-112.5 25
1,3-Dichlorobenzene ND ug/L 12/11/16 22:10 541-73-112.5 25
1,4-Dichlorobenzene ND ug/L 12/11/16 22:10 106-46-712.5 25
Dichlorodifluoromethane ND ug/L 12/11/16 22:10 75-71-812.5 25
1,1-Dichloroethane ND ug/L 12/11/16 22:10 75-34-312.5 25
1,2-Dichloroethane ND ug/L 12/11/16 22:10 107-06-212.5 25
1,1-Dichloroethene ND ug/L 12/11/16 22:10 75-35-412.5 25
cis-1,2-Dichloroethene ND ug/L 12/11/16 22:10 156-59-212.5 25
trans-1,2-Dichloroethene ND ug/L 12/11/16 22:10 156-60-512.5 25
1,2-Dichloropropane ND ug/L 12/11/16 22:10 78-87-512.5 25
1,3-Dichloropropane ND ug/L 12/11/16 22:10 142-28-912.5 25
2,2-Dichloropropane ND ug/L 12/11/16 22:10 594-20-712.5 25
1,1-Dichloropropene ND ug/L 12/11/16 22:10 563-58-612.5 25
cis-1,3-Dichloropropene ND ug/L 12/11/16 22:10 10061-01-512.5 25
trans-1,3-Dichloropropene ND ug/L 12/11/16 22:10 10061-02-612.5 25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92322865
Fiendly Mart
Sample: MW4 Lab ID: 92322865004 Collected: 12/08/16 18:30 Received: 12/09/16 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Diisopropyl ether 135 ug/L 12/11/16 22:10 108-20-312.5 25
Ethylbenzene 3040 ug/L 12/11/16 22:10 100-41-412.5 25
Hexachloro-1,3-butadiene ND ug/L 12/11/16 22:10 87-68-350.0 25
Isopropylbenzene (Cumene)174 ug/L 12/11/16 22:10 98-82-812.5 25
Methylene Chloride ND ug/L 12/11/16 22:10 75-09-250.0 25
Methyl-tert-butyl ether 848 ug/L 12/11/16 22:10 1634-04-412.5 25
Naphthalene 844 ug/L 12/11/16 22:10 91-20-350.0 25
n-Propylbenzene 490 ug/L 12/11/16 22:10 103-65-112.5 25
Styrene ND ug/L 12/11/16 22:10 100-42-512.5 25
1,1,1,2-Tetrachloroethane ND ug/L 12/11/16 22:10 630-20-612.5 25
1,1,2,2-Tetrachloroethane ND ug/L 12/11/16 22:10 79-34-512.5 25
Tetrachloroethene ND ug/L 12/11/16 22:10 127-18-412.5 25
Toluene 1970 ug/L 12/11/16 22:10 108-88-312.5 25
1,2,3-Trichlorobenzene ND ug/L 12/11/16 22:10 87-61-650.0 25
1,2,4-Trichlorobenzene ND ug/L 12/11/16 22:10 120-82-150.0 25
1,1,1-Trichloroethane ND ug/L 12/11/16 22:10 71-55-612.5 25
1,1,2-Trichloroethane ND ug/L 12/11/16 22:10 79-00-512.5 25
Trichloroethene ND ug/L 12/11/16 22:10 79-01-612.5 25
Trichlorofluoromethane ND ug/L 12/11/16 22:10 75-69-425.0 25
1,2,3-Trichloropropane ND ug/L 12/11/16 22:10 96-18-412.5 25
1,2,4-Trimethylbenzene 3240 ug/L 12/11/16 22:10 95-63-612.5 25
1,3,5-Trimethylbenzene 892 ug/L 12/11/16 22:10 108-67-812.5 25
Vinyl chloride ND ug/L 12/11/16 22:10 75-01-425.0 25
m&p-Xylene 6770 ug/L 12/11/16 22:10 179601-23-125.0 25
o-Xylene 1400 ug/L 12/11/16 22:10 95-47-612.5 25
Surrogates
1,2-Dichloroethane-d4 (S) 104 % 12/11/16 22:10 17060-07-070-130 25
4-Bromofluorobenzene (S) 96 % 12/11/16 22:10 460-00-470-130 25
Toluene-d8 (S) 102 % 12/11/16 22:10 2037-26-570-130 25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92322865
Fiendly Mart
Sample: MW5 Lab ID: 92322865005 Collected: 12/08/16 18:45 Received: 12/09/16 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: MADEP VPHVPH NC Water
Aliphatic (C05-C08)289 ug/L 12/12/16 18:54 N250.0 1
Aliphatic (C09-C12) ND ug/L 12/12/16 18:54 N250.0 1
Aromatic (C09-C10) ND ug/L 12/12/16 18:54 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S) 103 % 12/12/16 18:54 460-00-470-130 1
4-Bromofluorobenzene (PID) (S) 110 % 12/12/16 18:54 460-00-470-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Lead ND ug/L 12/15/16 15:41 7439-92-112/11/16 11:205.0 1
Analytical Method: SM 6200B6200B MSV
Benzene 6.5 ug/L 12/12/16 07:50 71-43-20.50 1
Bromobenzene ND ug/L 12/12/16 07:50 108-86-10.50 1
Bromochloromethane ND ug/L 12/12/16 07:50 74-97-50.50 1
Bromodichloromethane ND ug/L 12/12/16 07:50 75-27-40.50 1
Bromoform ND ug/L 12/12/16 07:50 75-25-20.50 1
Bromomethane ND ug/L 12/12/16 07:50 74-83-95.0 1
n-Butylbenzene ND ug/L 12/12/16 07:50 104-51-80.50 1
sec-Butylbenzene ND ug/L 12/12/16 07:50 135-98-80.50 1
tert-Butylbenzene ND ug/L 12/12/16 07:50 98-06-60.50 1
Carbon tetrachloride ND ug/L 12/12/16 07:50 56-23-50.50 1
Chlorobenzene ND ug/L 12/12/16 07:50 108-90-70.50 1
Chloroethane ND ug/L 12/12/16 07:50 75-00-31.0 1
Chloroform ND ug/L 12/12/16 07:50 67-66-30.50 1
Chloromethane ND ug/L 12/12/16 07:50 74-87-31.0 1
2-Chlorotoluene ND ug/L 12/12/16 07:50 95-49-80.50 1
4-Chlorotoluene ND ug/L 12/12/16 07:50 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 12/12/16 07:50 96-12-81.0 1
Dibromochloromethane ND ug/L 12/12/16 07:50 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 12/12/16 07:50 106-93-40.50 1
Dibromomethane ND ug/L 12/12/16 07:50 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 12/12/16 07:50 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 12/12/16 07:50 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 12/12/16 07:50 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 12/12/16 07:50 75-71-80.50 1
1,1-Dichloroethane ND ug/L 12/12/16 07:50 75-34-30.50 1
1,2-Dichloroethane ND ug/L 12/12/16 07:50 107-06-20.50 1
1,1-Dichloroethene ND ug/L 12/12/16 07:50 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 12/12/16 07:50 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 12/12/16 07:50 156-60-50.50 1
1,2-Dichloropropane ND ug/L 12/12/16 07:50 78-87-50.50 1
1,3-Dichloropropane ND ug/L 12/12/16 07:50 142-28-90.50 1
2,2-Dichloropropane ND ug/L 12/12/16 07:50 594-20-70.50 1
1,1-Dichloropropene ND ug/L 12/12/16 07:50 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 12/12/16 07:50 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 12/12/16 07:50 10061-02-60.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92322865
Fiendly Mart
Sample: MW5 Lab ID: 92322865005 Collected: 12/08/16 18:45 Received: 12/09/16 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Diisopropyl ether ND ug/L 12/12/16 07:50 108-20-30.50 1
Ethylbenzene ND ug/L 12/12/16 07:50 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 12/12/16 07:50 87-68-32.0 1
Isopropylbenzene (Cumene) ND ug/L 12/12/16 07:50 98-82-80.50 1
Methylene Chloride ND ug/L 12/12/16 07:50 75-09-22.0 1
Methyl-tert-butyl ether 176 ug/L 12/12/16 07:50 1634-04-40.50 1
Naphthalene 5.5 ug/L 12/12/16 07:50 91-20-32.0 1
n-Propylbenzene ND ug/L 12/12/16 07:50 103-65-10.50 1
Styrene ND ug/L 12/12/16 07:50 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 12/12/16 07:50 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 12/12/16 07:50 79-34-50.50 1
Tetrachloroethene ND ug/L 12/12/16 07:50 127-18-40.50 1
Toluene ND ug/L 12/12/16 07:50 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 12/12/16 07:50 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 12/12/16 07:50 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 12/12/16 07:50 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 12/12/16 07:50 79-00-50.50 1
Trichloroethene ND ug/L 12/12/16 07:50 79-01-60.50 1
Trichlorofluoromethane ND ug/L 12/12/16 07:50 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/12/16 07:50 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 12/12/16 07:50 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 12/12/16 07:50 108-67-80.50 1
Vinyl chloride ND ug/L 12/12/16 07:50 75-01-41.0 1
m&p-Xylene ND ug/L 12/12/16 07:50 179601-23-11.0 1
o-Xylene 0.61 ug/L 12/12/16 07:50 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 101 % 12/12/16 07:50 17060-07-070-130 1
4-Bromofluorobenzene (S) 96 % 12/12/16 07:50 460-00-470-130 1
Toluene-d8 (S) 100 % 12/12/16 07:50 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92322865
Fiendly Mart
Sample: MW6 Lab ID: 92322865006 Collected: 12/08/16 19:00 Received: 12/09/16 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: MADEP VPHVPH NC Water
Aliphatic (C05-C08)578 ug/L 12/12/16 03:07 N250.0 1
Aliphatic (C09-C12) ND ug/L 12/12/16 03:07 N250.0 1
Aromatic (C09-C10) ND ug/L 12/12/16 03:07 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S) 97 % 12/12/16 03:07 460-00-470-130 1
4-Bromofluorobenzene (PID) (S) 103 % 12/12/16 03:07 460-00-470-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Lead ND ug/L 12/15/16 15:44 7439-92-112/11/16 11:205.0 1
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 12/12/16 19:48 71-43-21.2 2.5
Bromobenzene ND ug/L 12/12/16 19:48 108-86-11.2 2.5
Bromochloromethane ND ug/L 12/12/16 19:48 74-97-51.2 2.5
Bromodichloromethane ND ug/L 12/12/16 19:48 75-27-41.2 2.5
Bromoform ND ug/L 12/12/16 19:48 75-25-21.2 2.5
Bromomethane ND ug/L 12/12/16 19:48 74-83-912.5 2.5
n-Butylbenzene ND ug/L 12/12/16 19:48 104-51-81.2 2.5
sec-Butylbenzene ND ug/L 12/12/16 19:48 135-98-81.2 2.5
tert-Butylbenzene ND ug/L 12/12/16 19:48 98-06-61.2 2.5
Carbon tetrachloride ND ug/L 12/12/16 19:48 56-23-51.2 2.5
Chlorobenzene ND ug/L 12/12/16 19:48 108-90-71.2 2.5
Chloroethane ND ug/L 12/12/16 19:48 75-00-32.5 2.5
Chloroform ND ug/L 12/12/16 19:48 67-66-31.2 2.5
Chloromethane ND ug/L 12/12/16 19:48 74-87-32.5 2.5
2-Chlorotoluene ND ug/L 12/12/16 19:48 95-49-81.2 2.5
4-Chlorotoluene ND ug/L 12/12/16 19:48 106-43-41.2 2.5
1,2-Dibromo-3-chloropropane ND ug/L 12/12/16 19:48 96-12-82.5 2.5
Dibromochloromethane ND ug/L 12/12/16 19:48 124-48-11.2 2.5
1,2-Dibromoethane (EDB) ND ug/L 12/12/16 19:48 106-93-41.2 2.5
Dibromomethane ND ug/L 12/12/16 19:48 74-95-31.2 2.5
1,2-Dichlorobenzene ND ug/L 12/12/16 19:48 95-50-11.2 2.5
1,3-Dichlorobenzene ND ug/L 12/12/16 19:48 541-73-11.2 2.5
1,4-Dichlorobenzene ND ug/L 12/12/16 19:48 106-46-71.2 2.5
Dichlorodifluoromethane ND ug/L 12/12/16 19:48 75-71-81.2 2.5
1,1-Dichloroethane ND ug/L 12/12/16 19:48 75-34-31.2 2.5
1,2-Dichloroethane ND ug/L 12/12/16 19:48 107-06-21.2 2.5
1,1-Dichloroethene ND ug/L 12/12/16 19:48 75-35-41.2 2.5
cis-1,2-Dichloroethene ND ug/L 12/12/16 19:48 156-59-21.2 2.5
trans-1,2-Dichloroethene ND ug/L 12/12/16 19:48 156-60-51.2 2.5
1,2-Dichloropropane ND ug/L 12/12/16 19:48 78-87-51.2 2.5
1,3-Dichloropropane ND ug/L 12/12/16 19:48 142-28-91.2 2.5
2,2-Dichloropropane ND ug/L 12/12/16 19:48 594-20-71.2 2.5
1,1-Dichloropropene ND ug/L 12/12/16 19:48 563-58-61.2 2.5
cis-1,3-Dichloropropene ND ug/L 12/12/16 19:48 10061-01-51.2 2.5
trans-1,3-Dichloropropene ND ug/L 12/12/16 19:48 10061-02-61.2 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92322865
Fiendly Mart
Sample: MW6 Lab ID: 92322865006 Collected: 12/08/16 19:00 Received: 12/09/16 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Diisopropyl ether 25.4 ug/L 12/12/16 19:48 108-20-31.2 2.5
Ethylbenzene ND ug/L 12/12/16 19:48 100-41-41.2 2.5
Hexachloro-1,3-butadiene ND ug/L 12/12/16 19:48 87-68-35.0 2.5
Isopropylbenzene (Cumene) ND ug/L 12/12/16 19:48 98-82-81.2 2.5
Methylene Chloride 5.4 ug/L 12/12/16 19:48 75-09-2 C95.0 2.5
Methyl-tert-butyl ether 364 ug/L 12/12/16 19:48 1634-04-41.2 2.5
Naphthalene ND ug/L 12/12/16 19:48 91-20-35.0 2.5
n-Propylbenzene ND ug/L 12/12/16 19:48 103-65-11.2 2.5
Styrene ND ug/L 12/12/16 19:48 100-42-51.2 2.5
1,1,1,2-Tetrachloroethane ND ug/L 12/12/16 19:48 630-20-61.2 2.5
1,1,2,2-Tetrachloroethane ND ug/L 12/12/16 19:48 79-34-51.2 2.5
Tetrachloroethene ND ug/L 12/12/16 19:48 127-18-41.2 2.5
Toluene ND ug/L 12/12/16 19:48 108-88-31.2 2.5
1,2,3-Trichlorobenzene ND ug/L 12/12/16 19:48 87-61-65.0 2.5
1,2,4-Trichlorobenzene ND ug/L 12/12/16 19:48 120-82-15.0 2.5
1,1,1-Trichloroethane ND ug/L 12/12/16 19:48 71-55-61.2 2.5
1,1,2-Trichloroethane ND ug/L 12/12/16 19:48 79-00-51.2 2.5
Trichloroethene ND ug/L 12/12/16 19:48 79-01-61.2 2.5
Trichlorofluoromethane ND ug/L 12/12/16 19:48 75-69-42.5 2.5
1,2,3-Trichloropropane ND ug/L 12/12/16 19:48 96-18-41.2 2.5
1,2,4-Trimethylbenzene ND ug/L 12/12/16 19:48 95-63-61.2 2.5
1,3,5-Trimethylbenzene ND ug/L 12/12/16 19:48 108-67-81.2 2.5
Vinyl chloride ND ug/L 12/12/16 19:48 75-01-42.5 2.5
m&p-Xylene ND ug/L 12/12/16 19:48 179601-23-12.5 2.5
o-Xylene ND ug/L 12/12/16 19:48 95-47-61.2 2.5
Surrogates
1,2-Dichloroethane-d4 (S) 100 % 12/12/16 19:48 17060-07-070-130 2.5
4-Bromofluorobenzene (S) 94 % 12/12/16 19:48 460-00-470-130 2.5
Toluene-d8 (S) 101 % 12/12/16 19:48 2037-26-570-130 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92322865
Fiendly Mart
Sample: MW7 Lab ID: 92322865007 Collected: 12/08/16 19:20 Received: 12/09/16 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: MADEP VPHVPH NC Water
Aliphatic (C05-C08)387 ug/L 12/12/16 03:35 N250.0 1
Aliphatic (C09-C12) ND ug/L 12/12/16 03:35 N250.0 1
Aromatic (C09-C10) ND ug/L 12/12/16 03:35 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S) 94 % 12/12/16 03:35 460-00-470-130 1
4-Bromofluorobenzene (PID) (S) 101 % 12/12/16 03:35 460-00-470-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Lead ND ug/L 12/15/16 15:47 7439-92-112/11/16 11:205.0 1
Analytical Method: SM 6200B6200B MSV
Benzene 0.97 ug/L 12/12/16 14:25 71-43-20.50 1
Bromobenzene ND ug/L 12/12/16 14:25 108-86-10.50 1
Bromochloromethane ND ug/L 12/12/16 14:25 74-97-50.50 1
Bromodichloromethane ND ug/L 12/12/16 14:25 75-27-40.50 1
Bromoform ND ug/L 12/12/16 14:25 75-25-20.50 1
Bromomethane ND ug/L 12/12/16 14:25 74-83-95.0 1
n-Butylbenzene ND ug/L 12/12/16 14:25 104-51-80.50 1
sec-Butylbenzene ND ug/L 12/12/16 14:25 135-98-80.50 1
tert-Butylbenzene ND ug/L 12/12/16 14:25 98-06-60.50 1
Carbon tetrachloride ND ug/L 12/12/16 14:25 56-23-50.50 1
Chlorobenzene ND ug/L 12/12/16 14:25 108-90-70.50 1
Chloroethane ND ug/L 12/12/16 14:25 75-00-31.0 1
Chloroform ND ug/L 12/12/16 14:25 67-66-30.50 1
Chloromethane ND ug/L 12/12/16 14:25 74-87-31.0 1
2-Chlorotoluene ND ug/L 12/12/16 14:25 95-49-80.50 1
4-Chlorotoluene ND ug/L 12/12/16 14:25 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 12/12/16 14:25 96-12-81.0 1
Dibromochloromethane ND ug/L 12/12/16 14:25 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 12/12/16 14:25 106-93-40.50 1
Dibromomethane ND ug/L 12/12/16 14:25 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 12/12/16 14:25 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 12/12/16 14:25 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 12/12/16 14:25 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 12/12/16 14:25 75-71-80.50 1
1,1-Dichloroethane ND ug/L 12/12/16 14:25 75-34-30.50 1
1,2-Dichloroethane ND ug/L 12/12/16 14:25 107-06-20.50 1
1,1-Dichloroethene ND ug/L 12/12/16 14:25 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 12/12/16 14:25 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 12/12/16 14:25 156-60-50.50 1
1,2-Dichloropropane ND ug/L 12/12/16 14:25 78-87-50.50 1
1,3-Dichloropropane ND ug/L 12/12/16 14:25 142-28-90.50 1
2,2-Dichloropropane ND ug/L 12/12/16 14:25 594-20-70.50 1
1,1-Dichloropropene ND ug/L 12/12/16 14:25 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 12/12/16 14:25 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 12/12/16 14:25 10061-02-60.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92322865
Fiendly Mart
Sample: MW7 Lab ID: 92322865007 Collected: 12/08/16 19:20 Received: 12/09/16 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Diisopropyl ether 33.1 ug/L 12/12/16 14:25 108-20-30.50 1
Ethylbenzene ND ug/L 12/12/16 14:25 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 12/12/16 14:25 87-68-32.0 1
Isopropylbenzene (Cumene) ND ug/L 12/12/16 14:25 98-82-80.50 1
Methylene Chloride ND ug/L 12/12/16 14:25 75-09-22.0 1
Methyl-tert-butyl ether 191 ug/L 12/12/16 14:25 1634-04-40.50 1
Naphthalene ND ug/L 12/12/16 14:25 91-20-32.0 1
n-Propylbenzene ND ug/L 12/12/16 14:25 103-65-10.50 1
Styrene ND ug/L 12/12/16 14:25 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 12/12/16 14:25 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 12/12/16 14:25 79-34-50.50 1
Tetrachloroethene ND ug/L 12/12/16 14:25 127-18-40.50 1
Toluene ND ug/L 12/12/16 14:25 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 12/12/16 14:25 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 12/12/16 14:25 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 12/12/16 14:25 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 12/12/16 14:25 79-00-50.50 1
Trichloroethene ND ug/L 12/12/16 14:25 79-01-60.50 1
Trichlorofluoromethane ND ug/L 12/12/16 14:25 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/12/16 14:25 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 12/12/16 14:25 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 12/12/16 14:25 108-67-80.50 1
Vinyl chloride ND ug/L 12/12/16 14:25 75-01-41.0 1
m&p-Xylene ND ug/L 12/12/16 14:25 179601-23-11.0 1
o-Xylene ND ug/L 12/12/16 14:25 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 102 % 12/12/16 14:25 17060-07-070-130 1
4-Bromofluorobenzene (S) 97 % 12/12/16 14:25 460-00-470-130 1
Toluene-d8 (S) 102 % 12/12/16 14:25 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92322865
Fiendly Mart
Sample: MW8 Lab ID: 92322865008 Collected: 12/08/16 19:35 Received: 12/09/16 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: MADEP VPHVPH NC Water
Aliphatic (C05-C08) ND ug/L 12/12/16 04:02 N250.0 1
Aliphatic (C09-C12) ND ug/L 12/12/16 04:02 N250.0 1
Aromatic (C09-C10) ND ug/L 12/12/16 04:02 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S) 93 % 12/12/16 04:02 460-00-470-130 1
4-Bromofluorobenzene (PID) (S) 100 % 12/12/16 04:02 460-00-470-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Lead ND ug/L 12/15/16 15:50 7439-92-112/11/16 11:205.0 1
Analytical Method: SM 6200B6200B MSV
Benzene 0.96 ug/L 12/12/16 19:31 71-43-20.50 1
Bromobenzene ND ug/L 12/12/16 19:31 108-86-10.50 1
Bromochloromethane ND ug/L 12/12/16 19:31 74-97-50.50 1
Bromodichloromethane ND ug/L 12/12/16 19:31 75-27-40.50 1
Bromoform ND ug/L 12/12/16 19:31 75-25-20.50 1
Bromomethane ND ug/L 12/12/16 19:31 74-83-95.0 1
n-Butylbenzene ND ug/L 12/12/16 19:31 104-51-80.50 1
sec-Butylbenzene ND ug/L 12/12/16 19:31 135-98-80.50 1
tert-Butylbenzene ND ug/L 12/12/16 19:31 98-06-60.50 1
Carbon tetrachloride ND ug/L 12/12/16 19:31 56-23-50.50 1
Chlorobenzene ND ug/L 12/12/16 19:31 108-90-70.50 1
Chloroethane ND ug/L 12/12/16 19:31 75-00-31.0 1
Chloroform ND ug/L 12/12/16 19:31 67-66-30.50 1
Chloromethane ND ug/L 12/12/16 19:31 74-87-31.0 1
2-Chlorotoluene ND ug/L 12/12/16 19:31 95-49-80.50 1
4-Chlorotoluene ND ug/L 12/12/16 19:31 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 12/12/16 19:31 96-12-81.0 1
Dibromochloromethane ND ug/L 12/12/16 19:31 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 12/12/16 19:31 106-93-40.50 1
Dibromomethane ND ug/L 12/12/16 19:31 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 12/12/16 19:31 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 12/12/16 19:31 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 12/12/16 19:31 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 12/12/16 19:31 75-71-80.50 1
1,1-Dichloroethane ND ug/L 12/12/16 19:31 75-34-30.50 1
1,2-Dichloroethane ND ug/L 12/12/16 19:31 107-06-20.50 1
1,1-Dichloroethene ND ug/L 12/12/16 19:31 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 12/12/16 19:31 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 12/12/16 19:31 156-60-50.50 1
1,2-Dichloropropane ND ug/L 12/12/16 19:31 78-87-50.50 1
1,3-Dichloropropane ND ug/L 12/12/16 19:31 142-28-90.50 1
2,2-Dichloropropane ND ug/L 12/12/16 19:31 594-20-70.50 1
1,1-Dichloropropene ND ug/L 12/12/16 19:31 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 12/12/16 19:31 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 12/12/16 19:31 10061-02-60.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92322865
Fiendly Mart
Sample: MW8 Lab ID: 92322865008 Collected: 12/08/16 19:35 Received: 12/09/16 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Diisopropyl ether 2.0 ug/L 12/12/16 19:31 108-20-30.50 1
Ethylbenzene ND ug/L 12/12/16 19:31 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 12/12/16 19:31 87-68-32.0 1
Isopropylbenzene (Cumene) ND ug/L 12/12/16 19:31 98-82-80.50 1
Methylene Chloride ND ug/L 12/12/16 19:31 75-09-22.0 1
Methyl-tert-butyl ether 8.2 ug/L 12/12/16 19:31 1634-04-40.50 1
Naphthalene ND ug/L 12/12/16 19:31 91-20-32.0 1
n-Propylbenzene ND ug/L 12/12/16 19:31 103-65-10.50 1
Styrene ND ug/L 12/12/16 19:31 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 12/12/16 19:31 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 12/12/16 19:31 79-34-50.50 1
Tetrachloroethene ND ug/L 12/12/16 19:31 127-18-40.50 1
Toluene ND ug/L 12/12/16 19:31 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 12/12/16 19:31 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 12/12/16 19:31 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 12/12/16 19:31 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 12/12/16 19:31 79-00-50.50 1
Trichloroethene ND ug/L 12/12/16 19:31 79-01-60.50 1
Trichlorofluoromethane ND ug/L 12/12/16 19:31 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/12/16 19:31 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 12/12/16 19:31 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 12/12/16 19:31 108-67-80.50 1
Vinyl chloride ND ug/L 12/12/16 19:31 75-01-41.0 1
m&p-Xylene ND ug/L 12/12/16 19:31 179601-23-11.0 1
o-Xylene ND ug/L 12/12/16 19:31 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 100 % 12/12/16 19:31 17060-07-070-130 1
4-Bromofluorobenzene (S) 95 % 12/12/16 19:31 460-00-470-130 1
Toluene-d8 (S) 102 % 12/12/16 19:31 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92322865
Fiendly Mart
Sample: MW9 Lab ID: 92322865009 Collected: 12/08/16 19:50 Received: 12/09/16 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: MADEP VPHVPH NC Water
Aliphatic (C05-C08)140000 ug/L 12/12/16 17:01 N225000 500
Aliphatic (C09-C12)26100 ug/L 12/12/16 17:01 N225000 500
Aromatic (C09-C10) ND ug/L 12/12/16 17:01 N225000 500
Surrogates
4-Bromofluorobenzene (FID) (S) 102 % 12/12/16 17:01 460-00-470-130 500
4-Bromofluorobenzene (PID) (S) 108 % 12/12/16 17:01 460-00-470-130 500
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Lead ND ug/L 12/15/16 15:53 7439-92-112/11/16 11:205.0 1
Analytical Method: SM 6200B6200B MSV
Benzene 14000 ug/L 12/12/16 17:32 71-43-2125 250
Bromobenzene ND ug/L 12/12/16 17:32 108-86-1125 250
Bromochloromethane ND ug/L 12/12/16 17:32 74-97-5125 250
Bromodichloromethane ND ug/L 12/12/16 17:32 75-27-4125 250
Bromoform ND ug/L 12/12/16 17:32 75-25-2125 250
Bromomethane ND ug/L 12/12/16 17:32 74-83-91250 250
n-Butylbenzene ND ug/L 12/12/16 17:32 104-51-8125 250
sec-Butylbenzene ND ug/L 12/12/16 17:32 135-98-8125 250
tert-Butylbenzene ND ug/L 12/12/16 17:32 98-06-6125 250
Carbon tetrachloride ND ug/L 12/12/16 17:32 56-23-5125 250
Chlorobenzene ND ug/L 12/12/16 17:32 108-90-7125 250
Chloroethane ND ug/L 12/12/16 17:32 75-00-3250 250
Chloroform ND ug/L 12/12/16 17:32 67-66-3125 250
Chloromethane ND ug/L 12/12/16 17:32 74-87-3250 250
2-Chlorotoluene ND ug/L 12/12/16 17:32 95-49-8125 250
4-Chlorotoluene ND ug/L 12/12/16 17:32 106-43-4125 250
1,2-Dibromo-3-chloropropane ND ug/L 12/12/16 17:32 96-12-8250 250
Dibromochloromethane ND ug/L 12/12/16 17:32 124-48-1125 250
1,2-Dibromoethane (EDB) ND ug/L 12/12/16 17:32 106-93-4125 250
Dibromomethane ND ug/L 12/12/16 17:32 74-95-3125 250
1,2-Dichlorobenzene ND ug/L 12/12/16 17:32 95-50-1125 250
1,3-Dichlorobenzene ND ug/L 12/12/16 17:32 541-73-1125 250
1,4-Dichlorobenzene ND ug/L 12/12/16 17:32 106-46-7125 250
Dichlorodifluoromethane ND ug/L 12/12/16 17:32 75-71-8125 250
1,1-Dichloroethane ND ug/L 12/12/16 17:32 75-34-3125 250
1,2-Dichloroethane ND ug/L 12/12/16 17:32 107-06-2125 250
1,1-Dichloroethene ND ug/L 12/12/16 17:32 75-35-4125 250
cis-1,2-Dichloroethene ND ug/L 12/12/16 17:32 156-59-2125 250
trans-1,2-Dichloroethene ND ug/L 12/12/16 17:32 156-60-5125 250
1,2-Dichloropropane ND ug/L 12/12/16 17:32 78-87-5125 250
1,3-Dichloropropane ND ug/L 12/12/16 17:32 142-28-9125 250
2,2-Dichloropropane ND ug/L 12/12/16 17:32 594-20-7125 250
1,1-Dichloropropene ND ug/L 12/12/16 17:32 563-58-6125 250
cis-1,3-Dichloropropene ND ug/L 12/12/16 17:32 10061-01-5125 250
trans-1,3-Dichloropropene ND ug/L 12/12/16 17:32 10061-02-6125 250
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92322865
Fiendly Mart
Sample: MW9 Lab ID: 92322865009 Collected: 12/08/16 19:50 Received: 12/09/16 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Diisopropyl ether 778 ug/L 12/12/16 17:32 108-20-3125 250
Ethylbenzene 4130 ug/L 12/12/16 17:32 100-41-4125 250
Hexachloro-1,3-butadiene ND ug/L 12/12/16 17:32 87-68-3500 250
Isopropylbenzene (Cumene)175 ug/L 12/12/16 17:32 98-82-8125 250
Methylene Chloride ND ug/L 12/12/16 17:32 75-09-2500 250
Methyl-tert-butyl ether 6240 ug/L 12/12/16 17:32 1634-04-4125 250
Naphthalene 571 ug/L 12/12/16 17:32 91-20-3500 250
n-Propylbenzene 471 ug/L 12/12/16 17:32 103-65-1125 250
Styrene ND ug/L 12/12/16 17:32 100-42-5125 250
1,1,1,2-Tetrachloroethane ND ug/L 12/12/16 17:32 630-20-6125 250
1,1,2,2-Tetrachloroethane ND ug/L 12/12/16 17:32 79-34-5125 250
Tetrachloroethene ND ug/L 12/12/16 17:32 127-18-4125 250
Toluene 43100 ug/L 12/12/16 17:32 108-88-3125 250
1,2,3-Trichlorobenzene ND ug/L 12/12/16 17:32 87-61-6500 250
1,2,4-Trichlorobenzene ND ug/L 12/12/16 17:32 120-82-1500 250
1,1,1-Trichloroethane ND ug/L 12/12/16 17:32 71-55-6125 250
1,1,2-Trichloroethane ND ug/L 12/12/16 17:32 79-00-5125 250
Trichloroethene ND ug/L 12/12/16 17:32 79-01-6125 250
Trichlorofluoromethane ND ug/L 12/12/16 17:32 75-69-4250 250
1,2,3-Trichloropropane ND ug/L 12/12/16 17:32 96-18-4125 250
1,2,4-Trimethylbenzene 2860 ug/L 12/12/16 17:32 95-63-6125 250
1,3,5-Trimethylbenzene 736 ug/L 12/12/16 17:32 108-67-8125 250
Vinyl chloride ND ug/L 12/12/16 17:32 75-01-4250 250
m&p-Xylene 13600 ug/L 12/12/16 17:32 179601-23-1250 250
o-Xylene 6350 ug/L 12/12/16 17:32 95-47-6125 250
Surrogates
1,2-Dichloroethane-d4 (S) 100 % 12/12/16 17:32 17060-07-070-130 250
4-Bromofluorobenzene (S) 95 % 12/12/16 17:32 460-00-470-130 250
Toluene-d8 (S) 100 % 12/12/16 17:32 2037-26-570-130 250
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92322865
Fiendly Mart
Sample: VEW1 Lab ID: 92322865010 Collected: 12/08/16 20:30 Received: 12/09/16 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: MADEP VPHVPH NC Water
Aliphatic (C05-C08)66.3 ug/L 12/13/16 20:42 N250.0 1
Aliphatic (C09-C12) ND ug/L 12/13/16 20:42 N250.0 1
Aromatic (C09-C10) ND ug/L 12/13/16 20:42 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S) 95 % 12/13/16 20:42 460-00-470-130 1
4-Bromofluorobenzene (PID) (S) 101 % 12/13/16 20:42 460-00-470-130 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Lead ND ug/L 12/15/16 15:56 7439-92-112/11/16 11:205.0 1
Analytical Method: SM 6200B6200B MSV
Benzene 0.61 ug/L 12/12/16 19:14 71-43-20.50 1
Bromobenzene ND ug/L 12/12/16 19:14 108-86-10.50 1
Bromochloromethane ND ug/L 12/12/16 19:14 74-97-50.50 1
Bromodichloromethane ND ug/L 12/12/16 19:14 75-27-40.50 1
Bromoform ND ug/L 12/12/16 19:14 75-25-20.50 1
Bromomethane ND ug/L 12/12/16 19:14 74-83-95.0 1
n-Butylbenzene ND ug/L 12/12/16 19:14 104-51-80.50 1
sec-Butylbenzene ND ug/L 12/12/16 19:14 135-98-80.50 1
tert-Butylbenzene ND ug/L 12/12/16 19:14 98-06-60.50 1
Carbon tetrachloride ND ug/L 12/12/16 19:14 56-23-50.50 1
Chlorobenzene ND ug/L 12/12/16 19:14 108-90-70.50 1
Chloroethane ND ug/L 12/12/16 19:14 75-00-31.0 1
Chloroform 7.0 ug/L 12/12/16 19:14 67-66-30.50 1
Chloromethane ND ug/L 12/12/16 19:14 74-87-31.0 1
2-Chlorotoluene ND ug/L 12/12/16 19:14 95-49-80.50 1
4-Chlorotoluene ND ug/L 12/12/16 19:14 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 12/12/16 19:14 96-12-81.0 1
Dibromochloromethane ND ug/L 12/12/16 19:14 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 12/12/16 19:14 106-93-40.50 1
Dibromomethane ND ug/L 12/12/16 19:14 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 12/12/16 19:14 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 12/12/16 19:14 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 12/12/16 19:14 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 12/12/16 19:14 75-71-80.50 1
1,1-Dichloroethane ND ug/L 12/12/16 19:14 75-34-30.50 1
1,2-Dichloroethane ND ug/L 12/12/16 19:14 107-06-20.50 1
1,1-Dichloroethene ND ug/L 12/12/16 19:14 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 12/12/16 19:14 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 12/12/16 19:14 156-60-50.50 1
1,2-Dichloropropane ND ug/L 12/12/16 19:14 78-87-50.50 1
1,3-Dichloropropane ND ug/L 12/12/16 19:14 142-28-90.50 1
2,2-Dichloropropane ND ug/L 12/12/16 19:14 594-20-70.50 1
1,1-Dichloropropene ND ug/L 12/12/16 19:14 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 12/12/16 19:14 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 12/12/16 19:14 10061-02-60.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92322865
Fiendly Mart
Sample: VEW1 Lab ID: 92322865010 Collected: 12/08/16 20:30 Received: 12/09/16 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Diisopropyl ether ND ug/L 12/12/16 19:14 108-20-30.50 1
Ethylbenzene 0.51 ug/L 12/12/16 19:14 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 12/12/16 19:14 87-68-32.0 1
Isopropylbenzene (Cumene) ND ug/L 12/12/16 19:14 98-82-80.50 1
Methylene Chloride ND ug/L 12/12/16 19:14 75-09-22.0 1
Methyl-tert-butyl ether 0.76 ug/L 12/12/16 19:14 1634-04-40.50 1
Naphthalene ND ug/L 12/12/16 19:14 91-20-32.0 1
n-Propylbenzene ND ug/L 12/12/16 19:14 103-65-10.50 1
Styrene ND ug/L 12/12/16 19:14 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 12/12/16 19:14 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 12/12/16 19:14 79-34-50.50 1
Tetrachloroethene ND ug/L 12/12/16 19:14 127-18-40.50 1
Toluene 0.70 ug/L 12/12/16 19:14 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 12/12/16 19:14 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 12/12/16 19:14 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 12/12/16 19:14 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 12/12/16 19:14 79-00-50.50 1
Trichloroethene ND ug/L 12/12/16 19:14 79-01-60.50 1
Trichlorofluoromethane ND ug/L 12/12/16 19:14 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 12/12/16 19:14 96-18-40.50 1
1,2,4-Trimethylbenzene 1.0 ug/L 12/12/16 19:14 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 12/12/16 19:14 108-67-80.50 1
Vinyl chloride ND ug/L 12/12/16 19:14 75-01-41.0 1
m&p-Xylene 1.7 ug/L 12/12/16 19:14 179601-23-11.0 1
o-Xylene 0.99 ug/L 12/12/16 19:14 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 102 % 12/12/16 19:14 17060-07-070-130 1
4-Bromofluorobenzene (S) 95 % 12/12/16 19:14 460-00-470-130 1
Toluene-d8 (S) 100 % 12/12/16 19:14 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92322865
Fiendly Mart
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
340339
MADEP VPH
MADEP VPH
VPH NC Water
Associated Lab Samples:92322865002, 92322865003, 92322865004, 92322865005, 92322865006, 92322865007, 92322865008,
92322865009, 92322865010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1887758
Associated Lab Samples: 92322865002, 92322865003, 92322865004, 92322865005, 92322865006, 92322865007, 92322865008,
92322865009, 92322865010
Matrix: Water
Analyzed
Aliphatic (C05-C08) ug/L ND 50.0 N212/11/16 15:40
Aliphatic (C09-C12) ug/L ND 50.0 N212/11/16 15:40
Aromatic (C09-C10) ug/L ND 50.0 N212/11/16 15:40
4-Bromofluorobenzene (FID) (S) % 98 70-130 12/11/16 15:40
4-Bromofluorobenzene (PID) (S) % 105 70-130 12/11/16 15:40
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1887759LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1887760
Aliphatic (C05-C08) ug/L 332 N2300 111 70-13099298 11 25
Aliphatic (C09-C12) ug/L 310 N2300 103 30-130109327 5 25
Aromatic (C09-C10) ug/L 109 N2100 109 70-130105105 4 25
4-Bromofluorobenzene (FID) (S) % 104 70-13098
4-Bromofluorobenzene (PID) (S) % 113 70-130106
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92322865
Fiendly Mart
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
340273
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92322865002, 92322865003, 92322865004, 92322865005, 92322865006, 92322865007, 92322865008,
92322865009, 92322865010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1887512
Associated Lab Samples: 92322865002, 92322865003, 92322865004, 92322865005, 92322865006, 92322865007, 92322865008,
92322865009, 92322865010
Matrix: Water
Analyzed
Lead ug/L ND 5.0 12/15/16 15:04
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1887513LABORATORY CONTROL SAMPLE:
LCSSpike
Lead ug/L 497500 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1887514MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92322684001
1887515
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Lead ug/L 500 91 75-12591 1 20500ND 456 453
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92322865
Fiendly Mart
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
340356
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples: 92322865001, 92322865002, 92322865003, 92322865004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1887828
Associated Lab Samples:92322865001, 92322865002, 92322865003, 92322865004
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 12/11/16 18:12
1,1,1-Trichloroethane ug/L ND 0.50 12/11/16 18:12
1,1,2,2-Tetrachloroethane ug/L ND 0.50 12/11/16 18:12
1,1,2-Trichloroethane ug/L ND 0.50 12/11/16 18:12
1,1-Dichloroethane ug/L ND 0.50 12/11/16 18:12
1,1-Dichloroethene ug/L ND 0.50 12/11/16 18:12
1,1-Dichloropropene ug/L ND 0.50 12/11/16 18:12
1,2,3-Trichlorobenzene ug/L ND 2.0 12/11/16 18:12
1,2,3-Trichloropropane ug/L ND 0.50 12/11/16 18:12
1,2,4-Trichlorobenzene ug/L ND 2.0 12/11/16 18:12
1,2,4-Trimethylbenzene ug/L ND 0.50 12/11/16 18:12
1,2-Dibromo-3-chloropropane ug/L ND 1.0 12/11/16 18:12
1,2-Dibromoethane (EDB) ug/L ND 0.50 12/11/16 18:12
1,2-Dichlorobenzene ug/L ND 0.50 12/11/16 18:12
1,2-Dichloroethane ug/L ND 0.50 12/11/16 18:12
1,2-Dichloropropane ug/L ND 0.50 12/11/16 18:12
1,3,5-Trimethylbenzene ug/L ND 0.50 12/11/16 18:12
1,3-Dichlorobenzene ug/L ND 0.50 12/11/16 18:12
1,3-Dichloropropane ug/L ND 0.50 12/11/16 18:12
1,4-Dichlorobenzene ug/L ND 0.50 12/11/16 18:12
2,2-Dichloropropane ug/L ND 0.50 12/11/16 18:12
2-Chlorotoluene ug/L ND 0.50 12/11/16 18:12
4-Chlorotoluene ug/L ND 0.50 12/11/16 18:12
Benzene ug/L ND 0.50 12/11/16 18:12
Bromobenzene ug/L ND 0.50 12/11/16 18:12
Bromochloromethane ug/L ND 0.50 12/11/16 18:12
Bromodichloromethane ug/L ND 0.50 12/11/16 18:12
Bromoform ug/L ND 0.50 12/11/16 18:12
Bromomethane ug/L ND 5.0 12/11/16 18:12
Carbon tetrachloride ug/L ND 0.50 12/11/16 18:12
Chlorobenzene ug/L ND 0.50 12/11/16 18:12
Chloroethane ug/L ND 1.0 12/11/16 18:12
Chloroform ug/L ND 0.50 12/11/16 18:12
Chloromethane ug/L ND 1.0 12/11/16 18:12
cis-1,2-Dichloroethene ug/L ND 0.50 12/11/16 18:12
cis-1,3-Dichloropropene ug/L ND 0.50 12/11/16 18:12
Dibromochloromethane ug/L ND 0.50 12/11/16 18:12
Dibromomethane ug/L ND 0.50 12/11/16 18:12
Dichlorodifluoromethane ug/L ND 0.50 12/11/16 18:12
Diisopropyl ether ug/L ND 0.50 12/11/16 18:12
Ethylbenzene ug/L ND 0.50 12/11/16 18:12
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92322865
Fiendly Mart
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1887828
Associated Lab Samples:92322865001, 92322865002, 92322865003, 92322865004
Matrix: Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 12/11/16 18:12
Isopropylbenzene (Cumene) ug/L ND 0.50 12/11/16 18:12
m&p-Xylene ug/L ND 1.0 12/11/16 18:12
Methyl-tert-butyl ether ug/L ND 0.50 12/11/16 18:12
Methylene Chloride ug/L ND 2.0 12/11/16 18:12
n-Butylbenzene ug/L ND 0.50 12/11/16 18:12
n-Propylbenzene ug/L ND 0.50 12/11/16 18:12
Naphthalene ug/L ND 2.0 12/11/16 18:12
o-Xylene ug/L ND 0.50 12/11/16 18:12
sec-Butylbenzene ug/L ND 0.50 12/11/16 18:12
Styrene ug/L ND 0.50 12/11/16 18:12
tert-Butylbenzene ug/L ND 0.50 12/11/16 18:12
Tetrachloroethene ug/L ND 0.50 12/11/16 18:12
Toluene ug/L ND 0.50 12/11/16 18:12
trans-1,2-Dichloroethene ug/L ND 0.50 12/11/16 18:12
trans-1,3-Dichloropropene ug/L ND 0.50 12/11/16 18:12
Trichloroethene ug/L ND 0.50 12/11/16 18:12
Trichlorofluoromethane ug/L ND 1.0 12/11/16 18:12
Vinyl chloride ug/L ND 1.0 12/11/16 18:12
1,2-Dichloroethane-d4 (S) % 103 70-130 12/11/16 18:12
4-Bromofluorobenzene (S) % 95 70-130 12/11/16 18:12
Toluene-d8 (S) % 102 70-130 12/11/16 18:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1887829LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.050 102 60-140
1,1,1-Trichloroethane ug/L 48.550 97 60-140
1,1,2,2-Tetrachloroethane ug/L 49.750 99 60-140
1,1,2-Trichloroethane ug/L 51.150 102 60-140
1,1-Dichloroethane ug/L 46.750 93 60-140
1,1-Dichloroethene ug/L 46.450 93 60-140
1,1-Dichloropropene ug/L 49.850 100 60-140
1,2,3-Trichlorobenzene ug/L 48.050 96 60-140
1,2,3-Trichloropropane ug/L 48.350 97 60-140
1,2,4-Trichlorobenzene ug/L 48.850 98 60-140
1,2,4-Trimethylbenzene ug/L 49.350 99 60-140
1,2-Dibromo-3-chloropropane ug/L 48.450 97 60-140
1,2-Dibromoethane (EDB) ug/L 47.850 96 60-140
1,2-Dichlorobenzene ug/L 47.550 95 60-140
1,2-Dichloroethane ug/L 44.650 89 60-140
1,2-Dichloropropane ug/L 49.550 99 60-140
1,3,5-Trimethylbenzene ug/L 48.550 97 60-140
1,3-Dichlorobenzene ug/L 47.350 95 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92322865
Fiendly Mart
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1887829LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 49.350 99 60-140
1,4-Dichlorobenzene ug/L 47.450 95 60-140
2,2-Dichloropropane ug/L 48.250 96 60-140
2-Chlorotoluene ug/L 47.850 96 60-140
4-Chlorotoluene ug/L 47.850 96 60-140
Benzene ug/L 50.350 101 60-140
Bromobenzene ug/L 48.850 98 60-140
Bromochloromethane ug/L 48.950 98 60-140
Bromodichloromethane ug/L 52.650 105 60-140
Bromoform ug/L 53.750 107 60-140
Bromomethane ug/L 51.450 103 60-140
Carbon tetrachloride ug/L 49.250 98 60-140
Chlorobenzene ug/L 49.450 99 60-140
Chloroethane ug/L 56.250 112 60-140
Chloroform ug/L 47.050 94 60-140
Chloromethane ug/L 42.750 85 60-140
cis-1,2-Dichloroethene ug/L 46.850 94 60-140
cis-1,3-Dichloropropene ug/L 53.250 106 60-140
Dibromochloromethane ug/L 53.050 106 60-140
Dibromomethane ug/L 46.850 94 60-140
Dichlorodifluoromethane ug/L 48.250 96 60-140
Diisopropyl ether ug/L 49.950 100 60-140
Ethylbenzene ug/L 48.750 97 60-140
Hexachloro-1,3-butadiene ug/L 50.150 100 60-140
Isopropylbenzene (Cumene) ug/L 48.650 97 60-140
m&p-Xylene ug/L 97.3100 97 60-140
Methyl-tert-butyl ether ug/L 50.450 101 60-140
Methylene Chloride ug/L 46.950 94 60-140
n-Butylbenzene ug/L 49.050 98 60-140
n-Propylbenzene ug/L 48.350 97 60-140
Naphthalene ug/L 51.050 102 60-140
o-Xylene ug/L 49.050 98 60-140
sec-Butylbenzene ug/L 49.050 98 60-140
Styrene ug/L 52.250 104 60-140
tert-Butylbenzene ug/L 40.550 81 60-140
Tetrachloroethene ug/L 45.850 92 60-140
Toluene ug/L 48.950 98 60-140
trans-1,2-Dichloroethene ug/L 48.050 96 60-140
trans-1,3-Dichloropropene ug/L 54.550 109 60-140
Trichloroethene ug/L 46.050 92 60-140
Trichlorofluoromethane ug/L 48.250 96 60-140
Vinyl chloride ug/L 39.750 79 60-140
1,2-Dichloroethane-d4 (S) % 101 70-130
4-Bromofluorobenzene (S) % 100 70-130
Toluene-d8 (S) % 100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92322865
Fiendly Mart
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1887830MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92322865001
1887831
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 107 60-140109 1 3020ND 21.5 21.7
1,1,1-Trichloroethane ug/L 20 113 60-140119 6 3020ND 22.5 23.9
1,1,2,2-Tetrachloroethane ug/L 20 105 60-140105 1 3020ND 21.1 21.0
1,1,2-Trichloroethane ug/L 20 113 60-140113 1 3020ND 22.5 22.6
1,1-Dichloroethane ug/L 20 109 60-140120 10 3020ND 21.7 23.9
1,1-Dichloroethene ug/L 20 106 60-140104 2 3020ND 21.2 20.7
1,1-Dichloropropene ug/L 20 116 60-140122 5 3020ND 23.2 24.3
1,2,3-Trichlorobenzene ug/L 20 103 60-140110 6 3020ND 20.7 22.0
1,2,3-Trichloropropane ug/L 20 102 60-140104 2 3020ND 20.4 20.8
1,2,4-Trichlorobenzene ug/L 20 105 60-140109 3 3020ND 21.0 21.8
1,2,4-Trimethylbenzene ug/L 20 108 60-140108 0 3020ND 21.6 21.7
1,2-Dibromo-3-
chloropropane
ug/L 20 101 60-140106 5 3020ND 20.2 21.3
1,2-Dibromoethane (EDB) ug/L 20 102 60-140103 1 3020ND 20.3 20.6
1,2-Dichlorobenzene ug/L 20 105 60-140106 1 3020ND 20.9 21.1
1,2-Dichloroethane ug/L 20 102 60-14099 3 3020ND 20.7 20.0
1,2-Dichloropropane ug/L 20 108 60-140109 1 3020ND 21.7 21.8
1,3,5-Trimethylbenzene ug/L 20 107 60-140109 2 3020ND 21.4 21.7
1,3-Dichlorobenzene ug/L 20 103 60-140104 1 3020ND 20.6 20.8
1,3-Dichloropropane ug/L 20 109 60-140110 1 3020ND 21.8 22.0
1,4-Dichlorobenzene ug/L 20 102 60-140105 2 3020ND 20.5 21.0
2,2-Dichloropropane ug/L 20 106 60-140112 6 3020ND 21.2 22.4
2-Chlorotoluene ug/L 20 106 60-140108 2 3020ND 21.3 21.6
4-Chlorotoluene ug/L 20 106 60-140107 1 3020ND 21.2 21.5
Benzene ug/L 20 112 60-140111 1 3020ND 22.4 22.2
Bromobenzene ug/L 20 106 60-140109 3 3020ND 21.3 21.9
Bromochloromethane ug/L 20 110 60-140122 10 3020ND 22.1 24.3
Bromodichloromethane ug/L 20 114 60-140113 1 3020ND 22.9 22.6
Bromoform ug/L 20 107 60-140109 3 3020ND 21.3 21.9
Bromomethane ug/L 20 113 60-140119 5 3020ND 22.6 23.8
Carbon tetrachloride ug/L 20 109 60-140117 7 3020ND 21.9 23.4
Chlorobenzene ug/L 20 108 60-140108 0 3020ND 21.6 21.6
Chloroethane ug/L 20 113 60-140112 1 3020ND 22.6 22.3
Chloroform ug/L 20 108 60-140116 7 3020ND 21.7 23.2
Chloromethane ug/L 20 97 60-140103 6 3020ND 19.6 20.9
cis-1,2-Dichloroethene ug/L 20 110 60-140120 9 3020ND 21.9 23.9
cis-1,3-Dichloropropene ug/L 20 110 60-140109 1 3020ND 22.0 21.8
Dibromochloromethane ug/L 20 110 60-140109 1 3020ND 22.1 21.8
Dibromomethane ug/L 20 103 60-140101 2 3020ND 20.7 20.2
Dichlorodifluoromethane ug/L 20 116 60-140113 3 3020ND 23.3 22.6
Diisopropyl ether ug/L 20 115 60-140132 14 3020ND 23.0 26.5
Ethylbenzene ug/L 20 108 60-140108 0 3020ND 21.6 21.5
Hexachloro-1,3-butadiene ug/L 20 106 60-140112 6 3020ND 21.2 22.4
Isopropylbenzene (Cumene) ug/L 20 108 60-140108 0 3020ND 21.5 21.5
m&p-Xylene ug/L 40 107 60-140107 0 3040ND 43.0 43.0
Methyl-tert-butyl ether ug/L 20 112 60-140123 9 30201.3 23.8 26.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92322865
Fiendly Mart
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1887830MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92322865001
1887831
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methylene Chloride ug/L 20 105 60-140114 8 3020ND 20.9 22.8
n-Butylbenzene ug/L 20 107 60-140109 1 3020ND 21.4 21.7
n-Propylbenzene ug/L 20 109 60-140110 1 3020ND 21.7 22.0
Naphthalene ug/L 20 109 60-140113 4 3020ND 21.8 22.6
o-Xylene ug/L 20 107 60-140108 0 3020ND 21.5 21.6
sec-Butylbenzene ug/L 20 110 60-140110 0 3020ND 22.0 22.0
Styrene ug/L 20 111 60-140112 1 3020ND 22.3 22.4
tert-Butylbenzene ug/L 20 92 60-14092 0 3020ND 18.5 18.4
Tetrachloroethene ug/L 20 102 60-140100 2 3020ND 20.5 20.1
Toluene ug/L 20 110 60-140109 1 3020ND 22.0 21.8
trans-1,2-Dichloroethene ug/L 20 114 60-140125 9 3020ND 22.8 24.9
trans-1,3-Dichloropropene ug/L 20 112 60-140111 1 3020ND 22.4 22.3
Trichloroethene ug/L 20 104 60-140104 0 3020ND 20.9 20.8
Trichlorofluoromethane ug/L 20 113 60-140109 3 3020ND 22.6 21.9
Vinyl chloride ug/L 20 93 60-14093 1 3020ND 18.7 18.6
1,2-Dichloroethane-d4 (S) % 102 70-130100
4-Bromofluorobenzene (S) % 97 70-13097
Toluene-d8 (S) % 101 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92322865
Fiendly Mart
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
340357
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples: 92322865005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1887832
Associated Lab Samples:92322865005
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 12/12/16 04:25
1,1,1-Trichloroethane ug/L ND 0.50 12/12/16 04:25
1,1,2,2-Tetrachloroethane ug/L ND 0.50 12/12/16 04:25
1,1,2-Trichloroethane ug/L ND 0.50 12/12/16 04:25
1,1-Dichloroethane ug/L ND 0.50 12/12/16 04:25
1,1-Dichloroethene ug/L ND 0.50 12/12/16 04:25
1,1-Dichloropropene ug/L ND 0.50 12/12/16 04:25
1,2,3-Trichlorobenzene ug/L ND 2.0 12/12/16 04:25
1,2,3-Trichloropropane ug/L ND 0.50 12/12/16 04:25
1,2,4-Trichlorobenzene ug/L ND 2.0 12/12/16 04:25
1,2,4-Trimethylbenzene ug/L ND 0.50 12/12/16 04:25
1,2-Dibromo-3-chloropropane ug/L ND 1.0 12/12/16 04:25
1,2-Dibromoethane (EDB) ug/L ND 0.50 12/12/16 04:25
1,2-Dichlorobenzene ug/L ND 0.50 12/12/16 04:25
1,2-Dichloroethane ug/L ND 0.50 12/12/16 04:25
1,2-Dichloropropane ug/L ND 0.50 12/12/16 04:25
1,3,5-Trimethylbenzene ug/L ND 0.50 12/12/16 04:25
1,3-Dichlorobenzene ug/L ND 0.50 12/12/16 04:25
1,3-Dichloropropane ug/L ND 0.50 12/12/16 04:25
1,4-Dichlorobenzene ug/L ND 0.50 12/12/16 04:25
2,2-Dichloropropane ug/L ND 0.50 12/12/16 04:25
2-Chlorotoluene ug/L ND 0.50 12/12/16 04:25
4-Chlorotoluene ug/L ND 0.50 12/12/16 04:25
Benzene ug/L ND 0.50 12/12/16 04:25
Bromobenzene ug/L ND 0.50 12/12/16 04:25
Bromochloromethane ug/L ND 0.50 12/12/16 04:25
Bromodichloromethane ug/L ND 0.50 12/12/16 04:25
Bromoform ug/L ND 0.50 12/12/16 04:25
Bromomethane ug/L ND 5.0 12/12/16 04:25
Carbon tetrachloride ug/L ND 0.50 12/12/16 04:25
Chlorobenzene ug/L ND 0.50 12/12/16 04:25
Chloroethane ug/L ND 1.0 12/12/16 04:25
Chloroform ug/L ND 0.50 12/12/16 04:25
Chloromethane ug/L ND 1.0 12/12/16 04:25
cis-1,2-Dichloroethene ug/L ND 0.50 12/12/16 04:25
cis-1,3-Dichloropropene ug/L ND 0.50 12/12/16 04:25
Dibromochloromethane ug/L ND 0.50 12/12/16 04:25
Dibromomethane ug/L ND 0.50 12/12/16 04:25
Dichlorodifluoromethane ug/L ND 0.50 12/12/16 04:25
Diisopropyl ether ug/L ND 0.50 12/12/16 04:25
Ethylbenzene ug/L ND 0.50 12/12/16 04:25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92322865
Fiendly Mart
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1887832
Associated Lab Samples:92322865005
Matrix: Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 12/12/16 04:25
Isopropylbenzene (Cumene) ug/L ND 0.50 12/12/16 04:25
m&p-Xylene ug/L ND 1.0 12/12/16 04:25
Methyl-tert-butyl ether ug/L ND 0.50 12/12/16 04:25
Methylene Chloride ug/L ND 2.0 12/12/16 04:25
n-Butylbenzene ug/L ND 0.50 12/12/16 04:25
n-Propylbenzene ug/L ND 0.50 12/12/16 04:25
Naphthalene ug/L ND 2.0 12/12/16 04:25
o-Xylene ug/L ND 0.50 12/12/16 04:25
sec-Butylbenzene ug/L ND 0.50 12/12/16 04:25
Styrene ug/L ND 0.50 12/12/16 04:25
tert-Butylbenzene ug/L ND 0.50 12/12/16 04:25
Tetrachloroethene ug/L ND 0.50 12/12/16 04:25
Toluene ug/L ND 0.50 12/12/16 04:25
trans-1,2-Dichloroethene ug/L ND 0.50 12/12/16 04:25
trans-1,3-Dichloropropene ug/L ND 0.50 12/12/16 04:25
Trichloroethene ug/L ND 0.50 12/12/16 04:25
Trichlorofluoromethane ug/L ND 1.0 12/12/16 04:25
Vinyl chloride ug/L ND 1.0 12/12/16 04:25
1,2-Dichloroethane-d4 (S) % 99 70-130 12/12/16 04:25
4-Bromofluorobenzene (S) % 94 70-130 12/12/16 04:25
Toluene-d8 (S) % 100 70-130 12/12/16 04:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1887833LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.150 100 60-140
1,1,1-Trichloroethane ug/L 48.750 97 60-140
1,1,2,2-Tetrachloroethane ug/L 49.350 99 60-140
1,1,2-Trichloroethane ug/L 50.050 100 60-140
1,1-Dichloroethane ug/L 46.950 94 60-140
1,1-Dichloroethene ug/L 43.850 88 60-140
1,1-Dichloropropene ug/L 49.950 100 60-140
1,2,3-Trichlorobenzene ug/L 50.850 102 60-140
1,2,3-Trichloropropane ug/L 48.850 98 60-140
1,2,4-Trichlorobenzene ug/L 48.950 98 60-140
1,2,4-Trimethylbenzene ug/L 48.050 96 60-140
1,2-Dibromo-3-chloropropane ug/L 48.750 97 60-140
1,2-Dibromoethane (EDB) ug/L 47.350 95 60-140
1,2-Dichlorobenzene ug/L 47.550 95 60-140
1,2-Dichloroethane ug/L 43.950 88 60-140
1,2-Dichloropropane ug/L 48.250 96 60-140
1,3,5-Trimethylbenzene ug/L 47.450 95 60-140
1,3-Dichlorobenzene ug/L 47.850 96 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92322865
Fiendly Mart
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1887833LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 49.250 98 60-140
1,4-Dichlorobenzene ug/L 46.650 93 60-140
2,2-Dichloropropane ug/L 44.450 89 60-140
2-Chlorotoluene ug/L 47.550 95 60-140
4-Chlorotoluene ug/L 47.250 94 60-140
Benzene ug/L 49.050 98 60-140
Bromobenzene ug/L 48.450 97 60-140
Bromochloromethane ug/L 48.750 97 60-140
Bromodichloromethane ug/L 51.050 102 60-140
Bromoform ug/L 53.950 108 60-140
Bromomethane ug/L 55.150 110 60-140
Carbon tetrachloride ug/L 47.650 95 60-140
Chlorobenzene ug/L 48.450 97 60-140
Chloroethane ug/L 50.850 102 60-140
Chloroform ug/L 46.750 93 60-140
Chloromethane ug/L 51.850 104 60-140
cis-1,2-Dichloroethene ug/L 47.050 94 60-140
cis-1,3-Dichloropropene ug/L 51.650 103 60-140
Dibromochloromethane ug/L 51.050 102 60-140
Dibromomethane ug/L 46.250 92 60-140
Dichlorodifluoromethane ug/L 48.150 96 60-140
Diisopropyl ether ug/L 51.350 103 60-140
Ethylbenzene ug/L 47.650 95 60-140
Hexachloro-1,3-butadiene ug/L 48.450 97 60-140
Isopropylbenzene (Cumene) ug/L 48.350 97 60-140
m&p-Xylene ug/L 95.9100 96 60-140
Methyl-tert-butyl ether ug/L 51.050 102 60-140
Methylene Chloride ug/L 46.250 92 60-140
n-Butylbenzene ug/L 47.250 94 60-140
n-Propylbenzene ug/L 47.550 95 60-140
Naphthalene ug/L 53.150 106 60-140
o-Xylene ug/L 48.950 98 60-140
sec-Butylbenzene ug/L 47.950 96 60-140
Styrene ug/L 51.350 103 60-140
tert-Butylbenzene ug/L 40.450 81 60-140
Tetrachloroethene ug/L 44.250 88 60-140
Toluene ug/L 48.550 97 60-140
trans-1,2-Dichloroethene ug/L 48.450 97 60-140
trans-1,3-Dichloropropene ug/L 52.050 104 60-140
Trichloroethene ug/L 45.350 91 60-140
Trichlorofluoromethane ug/L 46.150 92 60-140
Vinyl chloride ug/L 39.150 78 60-140
1,2-Dichloroethane-d4 (S) % 100 70-130
4-Bromofluorobenzene (S) % 100 70-130
Toluene-d8 (S) % 99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92322865
Fiendly Mart
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1887834MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92322815001
1887835
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 110 60-140112 2 3020ND 22.0 22.3
1,1,1-Trichloroethane ug/L 20 112 60-140115 3 3020ND 22.4 23.0
1,1,2,2-Tetrachloroethane ug/L 20 106 60-140113 6 3020ND 21.2 22.5
1,1,2-Trichloroethane ug/L 20 113 60-140116 2 3020ND 22.6 23.2
1,1-Dichloroethane ug/L 20 108 60-140111 2 3020ND 21.6 22.2
1,1-Dichloroethene ug/L 20 102 60-140103 2 3020ND 20.3 20.7
1,1-Dichloropropene ug/L 20 116 60-140119 3 3020ND 23.3 23.9
1,2,3-Trichlorobenzene ug/L 20 111 60-140114 3 3020ND 22.1 22.7
1,2,3-Trichloropropane ug/L 20 102 60-140106 4 3020ND 20.4 21.1
1,2,4-Trichlorobenzene ug/L 20 108 60-140114 6 3020ND 21.5 22.8
1,2,4-Trimethylbenzene ug/L 20 109 60-140116 6 30200.78 22.6 24.0
1,2-Dibromo-3-
chloropropane
ug/L 20 109 60-140109 1 3020ND 21.7 21.9
1,2-Dibromoethane (EDB) ug/L 20 102 60-140109 7 3020ND 20.4 21.8
1,2-Dichlorobenzene ug/L 20 104 60-140108 4 3020ND 20.7 21.6
1,2-Dichloroethane ug/L 20 99 60-140101 2 3020ND 20.1 20.4
1,2-Dichloropropane ug/L 20 110 60-140111 1 3020ND 22.0 22.2
1,3,5-Trimethylbenzene ug/L 20 107 60-140112 5 3020ND 21.6 22.7
1,3-Dichlorobenzene ug/L 20 104 60-140108 3 3020ND 20.9 21.5
1,3-Dichloropropane ug/L 20 109 60-140113 3 3020ND 21.8 22.5
1,4-Dichlorobenzene ug/L 20 102 60-140107 4 3020ND 20.4 21.3
2,2-Dichloropropane ug/L 20 104 60-140107 3 3020ND 20.8 21.5
2-Chlorotoluene ug/L 20 106 60-140110 3 3020ND 21.3 22.0
4-Chlorotoluene ug/L 20 107 60-140111 4 3020ND 21.3 22.3
Benzene ug/L 20 110 60-140117 6 30200.79 22.8 24.3
Bromobenzene ug/L 20 109 60-140111 2 3020ND 21.7 22.2
Bromochloromethane ug/L 20 112 60-140112 0 3020ND 22.5 22.5
Bromodichloromethane ug/L 20 112 60-140118 5 3020ND 22.4 23.5
Bromoform ug/L 20 106 60-140116 8 3020ND 21.3 23.2
Bromomethane ug/L 20 133 60-140140 5 3020ND 26.6 28.0
Carbon tetrachloride ug/L 20 109 60-140113 3 3020ND 21.8 22.6
Chlorobenzene ug/L 20 108 60-140112 3 3020ND 21.6 22.3
Chloroethane ug/L 20 109 60-140111 2 3020ND 21.7 22.2
Chloroform ug/L 20 109 60-140111 3 3020ND 21.7 22.3
Chloromethane ug/L 20 105 60-140119 12 3020ND 21.0 23.7
cis-1,2-Dichloroethene ug/L 20 109 60-140110 1 3020ND 21.8 22.1
cis-1,3-Dichloropropene ug/L 20 109 60-140115 5 3020ND 21.8 22.9
Dibromochloromethane ug/L 20 108 60-140116 7 3020ND 21.6 23.3
Dibromomethane ug/L 20 102 60-140106 4 3020ND 20.4 21.2
Dichlorodifluoromethane ug/L 20 111 60-140115 3 3020ND 22.2 23.0
Diisopropyl ether ug/L 20 112 60-140118 5 30203.8 26.2 27.5
Ethylbenzene ug/L 20 107 60-140113 6 3020ND 21.7 23.0
Hexachloro-1,3-butadiene ug/L 20 115 60-140120 5 3020ND 23.0 24.1
Isopropylbenzene (Cumene) ug/L 20 107 60-140113 6 3020ND 21.4 22.6
m&p-Xylene ug/L 40 105 60-140116 9 30402.2 44.3 48.4
Methyl-tert-butyl ether ug/L 20 115 60-140118 2 3020ND 23.0 23.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92322865
Fiendly Mart
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1887834MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92322815001
1887835
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methylene Chloride ug/L 20 103 60-140104 2 3020ND 20.7 21.0
n-Butylbenzene ug/L 20 106 60-140110 4 3020ND 21.1 22.1
n-Propylbenzene ug/L 20 108 60-140113 4 3020ND 21.6 22.5
Naphthalene ug/L 20 110 60-140140 21 30204.1 26.1 32.1
o-Xylene ug/L 20 104 60-140121 14 30202.7 23.5 26.9
sec-Butylbenzene ug/L 20 109 60-140114 4 3020ND 21.8 22.7
Styrene ug/L 20 111 60-140115 4 3020ND 22.1 23.0
tert-Butylbenzene ug/L 20 92 60-14094 3 3020ND 18.3 18.9
Tetrachloroethene ug/L 20 98 60-140106 8 3020ND 19.5 21.3
Toluene ug/L 20 104 60-140127 17 30204.1 24.8 29.5
trans-1,2-Dichloroethene ug/L 20 114 60-140117 2 3020ND 22.8 23.4
trans-1,3-Dichloropropene ug/L 20 113 60-140116 3 3020ND 22.7 23.3
Trichloroethene ug/L 20 104 60-140108 3 3020ND 20.8 21.5
Trichlorofluoromethane ug/L 20 109 60-140109 0 3020ND 21.8 21.9
Vinyl chloride ug/L 20 96 60-14094 2 3020ND 19.2 18.8
1,2-Dichloroethane-d4 (S) % 102 70-130101
4-Bromofluorobenzene (S) % 99 70-13098
Toluene-d8 (S) % 101 70-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92322865
Fiendly Mart
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
340411
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples: 92322865006, 92322865007, 92322865008, 92322865009, 92322865010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1888095
Associated Lab Samples:92322865006, 92322865007, 92322865008, 92322865009, 92322865010
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 12/12/16 13:00
1,1,1-Trichloroethane ug/L ND 0.50 12/12/16 13:00
1,1,2,2-Tetrachloroethane ug/L ND 0.50 12/12/16 13:00
1,1,2-Trichloroethane ug/L ND 0.50 12/12/16 13:00
1,1-Dichloroethane ug/L ND 0.50 12/12/16 13:00
1,1-Dichloroethene ug/L ND 0.50 12/12/16 13:00
1,1-Dichloropropene ug/L ND 0.50 12/12/16 13:00
1,2,3-Trichlorobenzene ug/L ND 2.0 12/12/16 13:00
1,2,3-Trichloropropane ug/L ND 0.50 12/12/16 13:00
1,2,4-Trichlorobenzene ug/L ND 2.0 12/12/16 13:00
1,2,4-Trimethylbenzene ug/L ND 0.50 12/12/16 13:00
1,2-Dibromo-3-chloropropane ug/L ND 1.0 12/12/16 13:00
1,2-Dibromoethane (EDB) ug/L ND 0.50 12/12/16 13:00
1,2-Dichlorobenzene ug/L ND 0.50 12/12/16 13:00
1,2-Dichloroethane ug/L ND 0.50 12/12/16 13:00
1,2-Dichloropropane ug/L ND 0.50 12/12/16 13:00
1,3,5-Trimethylbenzene ug/L ND 0.50 12/12/16 13:00
1,3-Dichlorobenzene ug/L ND 0.50 12/12/16 13:00
1,3-Dichloropropane ug/L ND 0.50 12/12/16 13:00
1,4-Dichlorobenzene ug/L ND 0.50 12/12/16 13:00
2,2-Dichloropropane ug/L ND 0.50 12/12/16 13:00
2-Chlorotoluene ug/L ND 0.50 12/12/16 13:00
4-Chlorotoluene ug/L ND 0.50 12/12/16 13:00
Benzene ug/L ND 0.50 12/12/16 13:00
Bromobenzene ug/L ND 0.50 12/12/16 13:00
Bromochloromethane ug/L ND 0.50 12/12/16 13:00
Bromodichloromethane ug/L ND 0.50 12/12/16 13:00
Bromoform ug/L ND 0.50 12/12/16 13:00
Bromomethane ug/L ND 5.0 12/12/16 13:00
Carbon tetrachloride ug/L ND 0.50 12/12/16 13:00
Chlorobenzene ug/L ND 0.50 12/12/16 13:00
Chloroethane ug/L ND 1.0 12/12/16 13:00
Chloroform ug/L ND 0.50 12/12/16 13:00
Chloromethane ug/L ND 1.0 12/12/16 13:00
cis-1,2-Dichloroethene ug/L ND 0.50 12/12/16 13:00
cis-1,3-Dichloropropene ug/L ND 0.50 12/12/16 13:00
Dibromochloromethane ug/L ND 0.50 12/12/16 13:00
Dibromomethane ug/L ND 0.50 12/12/16 13:00
Dichlorodifluoromethane ug/L ND 0.50 12/12/16 13:00
Diisopropyl ether ug/L ND 0.50 12/12/16 13:00
Ethylbenzene ug/L ND 0.50 12/12/16 13:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92322865
Fiendly Mart
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1888095
Associated Lab Samples:92322865006, 92322865007, 92322865008, 92322865009, 92322865010
Matrix: Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 12/12/16 13:00
Isopropylbenzene (Cumene) ug/L ND 0.50 12/12/16 13:00
m&p-Xylene ug/L ND 1.0 12/12/16 13:00
Methyl-tert-butyl ether ug/L ND 0.50 12/12/16 13:00
Methylene Chloride ug/L ND 2.0 12/12/16 13:00
n-Butylbenzene ug/L ND 0.50 12/12/16 13:00
n-Propylbenzene ug/L ND 0.50 12/12/16 13:00
Naphthalene ug/L ND 2.0 12/12/16 13:00
o-Xylene ug/L ND 0.50 12/12/16 13:00
sec-Butylbenzene ug/L ND 0.50 12/12/16 13:00
Styrene ug/L ND 0.50 12/12/16 13:00
tert-Butylbenzene ug/L ND 0.50 12/12/16 13:00
Tetrachloroethene ug/L ND 0.50 12/12/16 13:00
Toluene ug/L ND 0.50 12/12/16 13:00
trans-1,2-Dichloroethene ug/L ND 0.50 12/12/16 13:00
trans-1,3-Dichloropropene ug/L ND 0.50 12/12/16 13:00
Trichloroethene ug/L ND 0.50 12/12/16 13:00
Trichlorofluoromethane ug/L ND 1.0 12/12/16 13:00
Vinyl chloride ug/L ND 1.0 12/12/16 13:00
1,2-Dichloroethane-d4 (S) % 99 70-130 12/12/16 13:00
4-Bromofluorobenzene (S) % 97 70-130 12/12/16 13:00
Toluene-d8 (S) % 101 70-130 12/12/16 13:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1888096LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.850 102 60-140
1,1,1-Trichloroethane ug/L 49.850 100 60-140
1,1,2,2-Tetrachloroethane ug/L 48.250 96 60-140
1,1,2-Trichloroethane ug/L 49.750 99 60-140
1,1-Dichloroethane ug/L 48.150 96 60-140
1,1-Dichloroethene ug/L 43.850 88 60-140
1,1-Dichloropropene ug/L 51.150 102 60-140
1,2,3-Trichlorobenzene ug/L 48.850 98 60-140
1,2,3-Trichloropropane ug/L 46.250 92 60-140
1,2,4-Trichlorobenzene ug/L 49.850 100 60-140
1,2,4-Trimethylbenzene ug/L 49.450 99 60-140
1,2-Dibromo-3-chloropropane ug/L 47.150 94 60-140
1,2-Dibromoethane (EDB) ug/L 47.950 96 60-140
1,2-Dichlorobenzene ug/L 47.350 95 60-140
1,2-Dichloroethane ug/L 43.950 88 60-140
1,2-Dichloropropane ug/L 49.150 98 60-140
1,3,5-Trimethylbenzene ug/L 49.250 98 60-140
1,3-Dichlorobenzene ug/L 47.250 94 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92322865
Fiendly Mart
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1888096LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 49.450 99 60-140
1,4-Dichlorobenzene ug/L 46.750 93 60-140
2,2-Dichloropropane ug/L 49.150 98 60-140
2-Chlorotoluene ug/L 49.150 98 60-140
4-Chlorotoluene ug/L 48.550 97 60-140
Benzene ug/L 50.850 102 60-140
Bromobenzene ug/L 49.350 99 60-140
Bromochloromethane ug/L 49.350 99 60-140
Bromodichloromethane ug/L 52.050 104 60-140
Bromoform ug/L 52.350 105 60-140
Bromomethane ug/L 49.150 98 60-140
Carbon tetrachloride ug/L 49.750 99 60-140
Chlorobenzene ug/L 48.850 98 60-140
Chloroethane ug/L 49.250 98 60-140
Chloroform ug/L 47.850 96 60-140
Chloromethane ug/L 52.350 105 60-140
cis-1,2-Dichloroethene ug/L 48.050 96 60-140
cis-1,3-Dichloropropene ug/L 53.650 107 60-140
Dibromochloromethane ug/L 52.150 104 60-140
Dibromomethane ug/L 46.650 93 60-140
Dichlorodifluoromethane ug/L 46.850 94 60-140
Diisopropyl ether ug/L 51.950 104 60-140
Ethylbenzene ug/L 48.750 97 60-140
Hexachloro-1,3-butadiene ug/L 52.450 105 60-140
Isopropylbenzene (Cumene) ug/L 49.350 99 60-140
m&p-Xylene ug/L 97.2100 97 60-140
Methyl-tert-butyl ether ug/L 50.250 100 60-140
Methylene Chloride ug/L 46.550 93 60-140
n-Butylbenzene ug/L 49.650 99 60-140
n-Propylbenzene ug/L 49.450 99 60-140
Naphthalene ug/L 51.250 102 60-140
o-Xylene ug/L 49.250 98 60-140
sec-Butylbenzene ug/L 49.650 99 60-140
Styrene ug/L 52.550 105 60-140
tert-Butylbenzene ug/L 41.450 83 60-140
Tetrachloroethene ug/L 45.550 91 60-140
Toluene ug/L 48.950 98 60-140
trans-1,2-Dichloroethene ug/L 49.850 100 60-140
trans-1,3-Dichloropropene ug/L 54.250 108 60-140
Trichloroethene ug/L 47.050 94 60-140
Trichlorofluoromethane ug/L 45.750 91 60-140
Vinyl chloride ug/L 39.850 80 60-140
1,2-Dichloroethane-d4 (S) % 97 70-130
4-Bromofluorobenzene (S) % 98 70-130
Toluene-d8 (S) % 100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92322865
Fiendly Mart
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1888097MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92322863004
1888098
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 110 60-140103 7 3020ND 21.9 20.5
1,1,1-Trichloroethane ug/L 20 110 60-140109 1 3020ND 22.0 21.7
1,1,2,2-Tetrachloroethane ug/L 20 108 60-140105 3 3020ND 21.6 21.0
1,1,2-Trichloroethane ug/L 20 109 60-140106 3 3020ND 21.8 21.2
1,1-Dichloroethane ug/L 20 108 60-140106 2 3020ND 21.7 21.2
1,1-Dichloroethene ug/L 20 99 60-14095 4 3020ND 19.8 19.0
1,1-Dichloropropene ug/L 20 111 60-140109 3 3020ND 22.3 21.7
1,2,3-Trichlorobenzene ug/L 20 108 60-140104 4 3020ND 21.7 20.9
1,2,3-Trichloropropane ug/L 20 104 60-140100 4 3020ND 20.8 20.0
1,2,4-Trichlorobenzene ug/L 20 109 60-140106 3 3020ND 21.8 21.1
1,2,4-Trimethylbenzene ug/L 20 112 60-140108 3 3020ND 22.6 21.8
1,2-Dibromo-3-
chloropropane
ug/L 20 112 60-140111 0 3020ND 22.3 22.3
1,2-Dibromoethane (EDB) ug/L 20 109 60-140106 3 3020ND 21.7 21.1
1,2-Dichlorobenzene ug/L 20 108 60-140103 5 3020ND 21.6 20.6
1,2-Dichloroethane ug/L 20 98 60-14095 4 3020ND 19.8 19.1
1,2-Dichloropropane ug/L 20 106 60-140104 2 3020ND 21.3 20.9
1,3,5-Trimethylbenzene ug/L 20 112 60-140108 3 3020ND 22.5 21.7
1,3-Dichlorobenzene ug/L 20 105 60-140103 2 3020ND 21.0 20.7
1,3-Dichloropropane ug/L 20 108 60-140102 5 3020ND 21.5 20.4
1,4-Dichlorobenzene ug/L 20 104 60-140100 3 3020ND 20.7 20.0
2,2-Dichloropropane ug/L 20 108 60-140104 4 3020ND 21.6 20.8
2-Chlorotoluene ug/L 20 109 60-140105 4 3020ND 21.9 20.9
4-Chlorotoluene ug/L 20 108 60-140104 4 3020ND 21.6 20.9
Benzene ug/L 20 116 60-140111 5 3020ND 23.2 22.1
Bromobenzene ug/L 20 107 60-140107 1 3020ND 21.5 21.3
Bromochloromethane ug/L 20 111 60-140111 0 3020ND 22.2 22.2
Bromodichloromethane ug/L 20 112 60-140111 1 3020ND 22.3 22.2
Bromoform ug/L 20 107 60-140103 4 3020ND 21.5 20.6
Bromomethane ug/L 20 110 60-140120 8 3020ND 22.0 24.0
Carbon tetrachloride ug/L 20 109 60-140108 1 3020ND 21.9 21.6
Chlorobenzene ug/L 20 108 60-140102 6 3020ND 21.7 20.4
Chloroethane ug/L 20 96 60-14099 3 3020ND 19.3 19.8
Chloroform ug/L 20 107 60-140106 2 3020ND 21.4 21.1
Chloromethane ug/L 20 118 60-14093 24 3020ND 23.7 18.6
cis-1,2-Dichloroethene ug/L 20 107 60-140105 1 3020ND 21.4 21.2
cis-1,3-Dichloropropene ug/L 20 106 60-140103 2 3020ND 21.1 20.6
Dibromochloromethane ug/L 20 114 60-140107 7 3020ND 22.9 21.3
Dibromomethane ug/L 20 103 60-140103 0 3020ND 20.7 20.7
Dichlorodifluoromethane ug/L 20 105 60-140101 4 3020ND 21.0 20.1
Diisopropyl ether ug/L 20 115 60-140113 2 3020ND 22.9 22.5
Ethylbenzene ug/L 20 110 60-140105 5 3020ND 22.1 21.1
Hexachloro-1,3-butadiene ug/L 20 106 60-140106 0 3020ND 21.2 21.3
Isopropylbenzene (Cumene) ug/L 20 108 60-140104 4 3020ND 21.7 20.9
m&p-Xylene ug/L 40 109 60-140104 5 3040ND 44.3 42.2
Methyl-tert-butyl ether ug/L 20 112 60-140110 2 3020ND 22.3 21.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92322865
Fiendly Mart
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1888097MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92322863004
1888098
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methylene Chloride ug/L 20 105 60-140103 2 3020ND 21.1 20.6
n-Butylbenzene ug/L 20 111 60-140107 4 3020ND 22.2 21.3
n-Propylbenzene ug/L 20 113 60-140109 4 3020ND 22.7 21.8
Naphthalene ug/L 20 116 60-140111 3 30209.7 33.0 32.0
o-Xylene ug/L 20 109 60-140104 5 3020ND 22.0 21.0
sec-Butylbenzene ug/L 20 110 60-140107 3 3020ND 22.0 21.4
Styrene ug/L 20 112 60-140107 4 3020ND 22.4 21.4
tert-Butylbenzene ug/L 20 92 60-14089 3 3020ND 18.4 17.8
Tetrachloroethene ug/L 20 98 60-14094 4 3020ND 19.5 18.7
Toluene ug/L 20 110 60-140107 3 3020ND 21.9 21.4
trans-1,2-Dichloroethene ug/L 20 113 60-140109 3 3020ND 22.5 21.9
trans-1,3-Dichloropropene ug/L 20 107 60-140104 3 3020ND 21.5 20.8
Trichloroethene ug/L 20 104 60-140104 1 3020ND 20.9 20.8
Trichlorofluoromethane ug/L 20 105 60-140103 2 3020ND 21.0 20.6
Vinyl chloride ug/L 20 93 60-14088 5 3020ND 18.5 17.7
1,2-Dichloroethane-d4 (S) % 99 70-130100
4-Bromofluorobenzene (S) % 97 70-13097
Toluene-d8 (S) % 101 70-130101
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
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Page 43 of 48
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92322865
Fiendly Mart
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Common Laboratory Contaminant.C9
The lab does not hold NELAC/TNI accreditation for this parameter.N2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
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Page 44 of 48
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92322865
Fiendly Mart
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92322865002 340339MW1MADEP VPH
92322865003 340339MW2MADEP VPH
92322865004 340339MW4MADEP VPH
92322865005 340339MW5MADEP VPH
92322865006 340339MW6MADEP VPH
92322865007 340339MW7MADEP VPH
92322865008 340339MW8MADEP VPH
92322865009 340339MW9MADEP VPH
92322865010 340339VEW1MADEP VPH
92322865002 340273 340360MW1EPA 3010A EPA 6010
92322865003 340273 340360MW2EPA 3010A EPA 6010
92322865004 340273 340360MW4EPA 3010A EPA 6010
92322865005 340273 340360MW5EPA 3010A EPA 6010
92322865006 340273 340360MW6EPA 3010A EPA 6010
92322865007 340273 340360MW7EPA 3010A EPA 6010
92322865008 340273 340360MW8EPA 3010A EPA 6010
92322865009 340273 340360MW9EPA 3010A EPA 6010
92322865010 340273 340360VEW1EPA 3010A EPA 6010
92322865001 340356SW1SM 6200B
92322865002 340356MW1SM 6200B
92322865003 340356MW2SM 6200B
92322865004 340356MW4SM 6200B
92322865005 340357MW5SM 6200B
92322865006 340411MW6SM 6200B
92322865007 340411MW7SM 6200B
92322865008 340411MW8SM 6200B
92322865009 340411MW9SM 6200B
92322865010 340411VEW1SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 05:00 PM
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[phone]
Page 45 of 48
Page 46 of 48
Page 47 of 48
Page 48 of 48
#=CL#
December 22, 2016
LIMS USE: FR - HENRY NEMARGUT
LIMS OBJECT ID: 92323886
92323886
Project:
Pace Project No.:
RE:
Henry Nemargut
Henry Nemargut Engineering
2211 Chestnut Street
Wilmington, NC 28405
Friendly Mart
Dear Henry Nemargut:
Enclosed are the analytical results for sample(s) received by the laboratory on December 16, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
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[phone]
Page 1 of 19
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92323886
Friendly Mart
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 2 of 19
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92323886
Friendly Mart
Lab ID Sample ID Matrix Date Collected Date Received
92323886001 MW 3 Water 12/15/16 17:30 12/16/16 17:10
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 3 of 19
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92323886
Friendly Mart
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92323886001 MW 3 MADEP VPH 5 PASI-CWDV
EPA 6010 1 PASI-ASH1
SM 6200B 63 PASI-CCAH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 4 of 19
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92323886
Friendly Mart
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92323886001 MW 3
Aliphatic (C05-C08) 2670 ug/L 12/22/16 01:03 N2625MADEP VPH
Benzene 417 ug/L 12/21/16 02:202.5SM 6200B
Bromodichloromethane 4.0 ug/L 12/21/16 02:202.5SM 6200B
Chloroform 115 ug/L 12/21/16 02:202.5SM 6200B
Diisopropyl ether 19.8 ug/L 12/21/16 02:202.5SM 6200B
Isopropylbenzene (Cumene) 5.3 ug/L 12/21/16 02:202.5SM 6200B
Methyl-tert-butyl ether 915 ug/L 12/21/16 02:202.5SM 6200B
Naphthalene 50.6 ug/L 12/21/16 02:2010.0SM 6200B
1,2,4-Trimethylbenzene 23.0 ug/L 12/21/16 02:202.5SM 6200B
1,3,5-Trimethylbenzene 2.9 ug/L 12/21/16 02:202.5SM 6200B
m&p-Xylene 5.3 ug/L 12/21/16 02:205.0SM 6200B
o-Xylene 13.6 ug/L 12/21/16 02:202.5SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 5 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92323886
Friendly Mart
Sample: MW 3 Lab ID: 92323886001 Collected: 12/15/16 17:30 Received: 12/16/16 17:10 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: MADEP VPHVPH NC Water
Aliphatic (C05-C08)2670 ug/L 12/22/16 01:03 N2625 12.5
Aliphatic (C09-C12) ND ug/L 12/22/16 01:03 N2625 12.5
Aromatic (C09-C10) ND ug/L 12/22/16 01:03 N2625 12.5
Surrogates
4-Bromofluorobenzene (FID) (S) 88 % 12/22/16 01:03 460-00-470-130 12.5
4-Bromofluorobenzene (PID) (S) 93 % 12/22/16 01:03 460-00-470-130 12.5
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Lead ND ug/L 12/22/16 11:10 7439-92-112/21/16 21:005.0 1
Analytical Method: SM 6200B6200B MSV
Benzene 417 ug/L 12/21/16 02:20 71-43-22.5 5
Bromobenzene ND ug/L 12/21/16 02:20 108-86-12.5 5
Bromochloromethane ND ug/L 12/21/16 02:20 74-97-52.5 5
Bromodichloromethane 4.0 ug/L 12/21/16 02:20 75-27-42.5 5
Bromoform ND ug/L 12/21/16 02:20 75-25-22.5 5
Bromomethane ND ug/L 12/21/16 02:20 74-83-925.0 5
n-Butylbenzene ND ug/L 12/21/16 02:20 104-51-82.5 5
sec-Butylbenzene ND ug/L 12/21/16 02:20 135-98-82.5 5
tert-Butylbenzene ND ug/L 12/21/16 02:20 98-06-62.5 5
Carbon tetrachloride ND ug/L 12/21/16 02:20 56-23-52.5 5
Chlorobenzene ND ug/L 12/21/16 02:20 108-90-72.5 5
Chloroethane ND ug/L 12/21/16 02:20 75-00-35.0 5
Chloroform 115 ug/L 12/21/16 02:20 67-66-32.5 5
Chloromethane ND ug/L 12/21/16 02:20 74-87-35.0 5
2-Chlorotoluene ND ug/L 12/21/16 02:20 95-49-82.5 5
4-Chlorotoluene ND ug/L 12/21/16 02:20 106-43-42.5 5
1,2-Dibromo-3-chloropropane ND ug/L 12/21/16 02:20 96-12-85.0 5
Dibromochloromethane ND ug/L 12/21/16 02:20 124-48-12.5 5
1,2-Dibromoethane (EDB) ND ug/L 12/21/16 02:20 106-93-42.5 5
Dibromomethane ND ug/L 12/21/16 02:20 74-95-32.5 5
1,2-Dichlorobenzene ND ug/L 12/21/16 02:20 95-50-12.5 5
1,3-Dichlorobenzene ND ug/L 12/21/16 02:20 541-73-12.5 5
1,4-Dichlorobenzene ND ug/L 12/21/16 02:20 106-46-72.5 5
Dichlorodifluoromethane ND ug/L 12/21/16 02:20 75-71-82.5 5
1,1-Dichloroethane ND ug/L 12/21/16 02:20 75-34-32.5 5
1,2-Dichloroethane ND ug/L 12/21/16 02:20 107-06-22.5 5
1,1-Dichloroethene ND ug/L 12/21/16 02:20 75-35-42.5 5
cis-1,2-Dichloroethene ND ug/L 12/21/16 02:20 156-59-22.5 5
trans-1,2-Dichloroethene ND ug/L 12/21/16 02:20 156-60-52.5 5
1,2-Dichloropropane ND ug/L 12/21/16 02:20 78-87-52.5 5
1,3-Dichloropropane ND ug/L 12/21/16 02:20 142-28-92.5 5
2,2-Dichloropropane ND ug/L 12/21/16 02:20 594-20-72.5 5
1,1-Dichloropropene ND ug/L 12/21/16 02:20 563-58-62.5 5
cis-1,3-Dichloropropene ND ug/L 12/21/16 02:20 10061-01-52.5 5
trans-1,3-Dichloropropene ND ug/L 12/21/16 02:20 10061-02-62.5 5
REPORT OF LABORATORY ANALYSIS
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Page 6 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92323886
Friendly Mart
Sample: MW 3 Lab ID: 92323886001 Collected: 12/15/16 17:30 Received: 12/16/16 17:10 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Diisopropyl ether 19.8 ug/L 12/21/16 02:20 108-20-32.5 5
Ethylbenzene ND ug/L 12/21/16 02:20 100-41-42.5 5
Hexachloro-1,3-butadiene ND ug/L 12/21/16 02:20 87-68-310.0 5
Isopropylbenzene (Cumene)5.3 ug/L 12/21/16 02:20 98-82-82.5 5
Methylene Chloride ND ug/L 12/21/16 02:20 75-09-210.0 5
Methyl-tert-butyl ether 915 ug/L 12/21/16 02:20 1634-04-42.5 5
Naphthalene 50.6 ug/L 12/21/16 02:20 91-20-310.0 5
n-Propylbenzene ND ug/L 12/21/16 02:20 103-65-12.5 5
Styrene ND ug/L 12/21/16 02:20 100-42-52.5 5
1,1,1,2-Tetrachloroethane ND ug/L 12/21/16 02:20 630-20-62.5 5
1,1,2,2-Tetrachloroethane ND ug/L 12/21/16 02:20 79-34-52.5 5
Tetrachloroethene ND ug/L 12/21/16 02:20 127-18-42.5 5
Toluene ND ug/L 12/21/16 02:20 108-88-32.5 5
1,2,3-Trichlorobenzene ND ug/L 12/21/16 02:20 87-61-610.0 5
1,2,4-Trichlorobenzene ND ug/L 12/21/16 02:20 120-82-110.0 5
1,1,1-Trichloroethane ND ug/L 12/21/16 02:20 71-55-62.5 5
1,1,2-Trichloroethane ND ug/L 12/21/16 02:20 79-00-52.5 5
Trichloroethene ND ug/L 12/21/16 02:20 79-01-62.5 5
Trichlorofluoromethane ND ug/L 12/21/16 02:20 75-69-45.0 5
1,2,3-Trichloropropane ND ug/L 12/21/16 02:20 96-18-42.5 5
1,2,4-Trimethylbenzene 23.0 ug/L 12/21/16 02:20 95-63-62.5 5
1,3,5-Trimethylbenzene 2.9 ug/L 12/21/16 02:20 108-67-82.5 5
Vinyl chloride ND ug/L 12/21/16 02:20 75-01-45.0 5
m&p-Xylene 5.3 ug/L 12/21/16 02:20 179601-23-15.0 5
o-Xylene 13.6 ug/L 12/21/16 02:20 95-47-62.5 5
Surrogates
1,2-Dichloroethane-d4 (S) 96 % 12/21/16 02:20 17060-07-070-130 5
4-Bromofluorobenzene (S) 99 % 12/21/16 02:20 460-00-470-130 5
Toluene-d8 (S) 102 % 12/21/16 02:20 2037-26-570-130 5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 04:38 PM
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Page 7 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92323886
Friendly Mart
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
341690
MADEP VPH
MADEP VPH
VPH NC Water
Associated Lab Samples: 92323886001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1895721
Associated Lab Samples:92323886001
Matrix: Water
Analyzed
Aliphatic (C05-C08) ug/L ND 50.0 N212/20/16 11:43
Aliphatic (C09-C12) ug/L ND 50.0 N212/20/16 11:43
Aromatic (C09-C10) ug/L ND 50.0 N212/20/16 11:43
4-Bromofluorobenzene (FID) (S) % 101 70-130 12/20/16 11:43
4-Bromofluorobenzene (PID) (S) % 107 70-130 12/20/16 11:43
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1895722LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1895723
Aliphatic (C05-C08) ug/L 308 N2300 103 70-13096289 6 25
Aliphatic (C09-C12) ug/L 303 N2300 101 30-130107321 5 25
Aromatic (C09-C10) ug/L 111 N2100 111 70-130108108 3 25
4-Bromofluorobenzene (FID) (S) % 97 70-13090
4-Bromofluorobenzene (PID) (S) % 103 70-13096
REPORT OF LABORATORY ANALYSIS
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Page 8 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92323886
Friendly Mart
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
341612
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples: 92323886001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1895425
Associated Lab Samples:92323886001
Matrix: Water
Analyzed
Lead ug/L ND 5.0 12/22/16 10:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1895426LABORATORY CONTROL SAMPLE:
LCSSpike
Lead ug/L 488500 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1895427MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92323758005
1895428
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Lead ug/L 500 99 75-12595 3 20500ND 496 479
REPORT OF LABORATORY ANALYSIS
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Page 9 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92323886
Friendly Mart
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
341708
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples: 92323886001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1895795
Associated Lab Samples:92323886001
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 12/20/16 22:56
1,1,1-Trichloroethane ug/L ND 0.50 12/20/16 22:56
1,1,2,2-Tetrachloroethane ug/L ND 0.50 12/20/16 22:56
1,1,2-Trichloroethane ug/L ND 0.50 12/20/16 22:56
1,1-Dichloroethane ug/L ND 0.50 12/20/16 22:56
1,1-Dichloroethene ug/L ND 0.50 12/20/16 22:56
1,1-Dichloropropene ug/L ND 0.50 12/20/16 22:56
1,2,3-Trichlorobenzene ug/L ND 2.0 12/20/16 22:56
1,2,3-Trichloropropane ug/L ND 0.50 12/20/16 22:56
1,2,4-Trichlorobenzene ug/L ND 2.0 12/20/16 22:56
1,2,4-Trimethylbenzene ug/L ND 0.50 12/20/16 22:56
1,2-Dibromo-3-chloropropane ug/L ND 1.0 12/20/16 22:56
1,2-Dibromoethane (EDB) ug/L ND 0.50 12/20/16 22:56
1,2-Dichlorobenzene ug/L ND 0.50 12/20/16 22:56
1,2-Dichloroethane ug/L ND 0.50 12/20/16 22:56
1,2-Dichloropropane ug/L ND 0.50 12/20/16 22:56
1,3,5-Trimethylbenzene ug/L ND 0.50 12/20/16 22:56
1,3-Dichlorobenzene ug/L ND 0.50 12/20/16 22:56
1,3-Dichloropropane ug/L ND 0.50 12/20/16 22:56
1,4-Dichlorobenzene ug/L ND 0.50 12/20/16 22:56
2,2-Dichloropropane ug/L ND 0.50 12/20/16 22:56
2-Chlorotoluene ug/L ND 0.50 12/20/16 22:56
4-Chlorotoluene ug/L ND 0.50 12/20/16 22:56
Benzene ug/L ND 0.50 12/20/16 22:56
Bromobenzene ug/L ND 0.50 12/20/16 22:56
Bromochloromethane ug/L ND 0.50 12/20/16 22:56
Bromodichloromethane ug/L ND 0.50 12/20/16 22:56
Bromoform ug/L ND 0.50 12/20/16 22:56
Bromomethane ug/L ND 5.0 12/20/16 22:56
Carbon tetrachloride ug/L ND 0.50 12/20/16 22:56
Chlorobenzene ug/L ND 0.50 12/20/16 22:56
Chloroethane ug/L ND 1.0 12/20/16 22:56
Chloroform ug/L ND 0.50 12/20/16 22:56
Chloromethane ug/L ND 1.0 12/20/16 22:56
cis-1,2-Dichloroethene ug/L ND 0.50 12/20/16 22:56
cis-1,3-Dichloropropene ug/L ND 0.50 12/20/16 22:56
Dibromochloromethane ug/L ND 0.50 12/20/16 22:56
Dibromomethane ug/L ND 0.50 12/20/16 22:56
Dichlorodifluoromethane ug/L ND 0.50 12/20/16 22:56
Diisopropyl ether ug/L ND 0.50 12/20/16 22:56
Ethylbenzene ug/L ND 0.50 12/20/16 22:56
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 04:38 PM
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Page 10 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92323886
Friendly Mart
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1895795
Associated Lab Samples:92323886001
Matrix: Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 12/20/16 22:56
Isopropylbenzene (Cumene) ug/L ND 0.50 12/20/16 22:56
m&p-Xylene ug/L ND 1.0 12/20/16 22:56
Methyl-tert-butyl ether ug/L ND 0.50 12/20/16 22:56
Methylene Chloride ug/L ND 2.0 12/20/16 22:56
n-Butylbenzene ug/L ND 0.50 12/20/16 22:56
n-Propylbenzene ug/L ND 0.50 12/20/16 22:56
Naphthalene ug/L ND 2.0 12/20/16 22:56
o-Xylene ug/L ND 0.50 12/20/16 22:56
sec-Butylbenzene ug/L ND 0.50 12/20/16 22:56
Styrene ug/L ND 0.50 12/20/16 22:56
tert-Butylbenzene ug/L ND 0.50 12/20/16 22:56
Tetrachloroethene ug/L ND 0.50 12/20/16 22:56
Toluene ug/L ND 0.50 12/20/16 22:56
trans-1,2-Dichloroethene ug/L ND 0.50 12/20/16 22:56
trans-1,3-Dichloropropene ug/L ND 0.50 12/20/16 22:56
Trichloroethene ug/L ND 0.50 12/20/16 22:56
Trichlorofluoromethane ug/L ND 1.0 12/20/16 22:56
Vinyl chloride ug/L ND 1.0 12/20/16 22:56
1,2-Dichloroethane-d4 (S) % 98 70-130 12/20/16 22:56
4-Bromofluorobenzene (S) % 97 70-130 12/20/16 22:56
Toluene-d8 (S) % 102 70-130 12/20/16 22:56
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1895796LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 48.850 98 60-140
1,1,1-Trichloroethane ug/L 54.350 109 60-140
1,1,2,2-Tetrachloroethane ug/L 46.750 93 60-140
1,1,2-Trichloroethane ug/L 48.050 96 60-140
1,1-Dichloroethane ug/L 56.650 113 60-140
1,1-Dichloroethene ug/L 51.150 102 60-140
1,1-Dichloropropene ug/L 54.150 108 60-140
1,2,3-Trichlorobenzene ug/L 45.550 91 60-140
1,2,3-Trichloropropane ug/L 47.450 95 60-140
1,2,4-Trichlorobenzene ug/L 47.550 95 60-140
1,2,4-Trimethylbenzene ug/L 46.550 93 60-140
1,2-Dibromo-3-chloropropane ug/L 46.950 94 60-140
1,2-Dibromoethane (EDB) ug/L 47.750 95 60-140
1,2-Dichlorobenzene ug/L 46.550 93 60-140
1,2-Dichloroethane ug/L 42.350 85 60-140
1,2-Dichloropropane ug/L 45.450 91 60-140
1,3,5-Trimethylbenzene ug/L 45.150 90 60-140
1,3-Dichlorobenzene ug/L 43.650 87 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 04:38 PM
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Huntersville, NC 28078
[phone]
Page 11 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92323886
Friendly Mart
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1895796LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 48.250 96 60-140
1,4-Dichlorobenzene ug/L 44.450 89 60-140
2,2-Dichloropropane ug/L 52.550 105 60-140
2-Chlorotoluene ug/L 44.350 89 60-140
4-Chlorotoluene ug/L 45.050 90 60-140
Benzene ug/L 54.450 109 60-140
Bromobenzene ug/L 44.050 88 60-140
Bromochloromethane ug/L 56.050 112 60-140
Bromodichloromethane ug/L 49.050 98 60-140
Bromoform ug/L 49.350 99 60-140
Bromomethane ug/L 48.150 96 60-140
Carbon tetrachloride ug/L 57.750 115 60-140
Chlorobenzene ug/L 46.150 92 60-140
Chloroethane ug/L 50.850 102 60-140
Chloroform ug/L 54.550 109 60-140
Chloromethane ug/L 51.450 103 60-140
cis-1,2-Dichloroethene ug/L 55.250 110 60-140
cis-1,3-Dichloropropene ug/L 49.950 100 60-140
Dibromochloromethane ug/L 49.950 100 60-140
Dibromomethane ug/L 47.550 95 60-140
Dichlorodifluoromethane ug/L 47.650 95 60-140
Diisopropyl ether ug/L 58.550 117 60-140
Ethylbenzene ug/L 48.150 96 60-140
Hexachloro-1,3-butadiene ug/L 49.850 100 60-140
Isopropylbenzene (Cumene) ug/L 47.650 95 60-140
m&p-Xylene ug/L 94.4100 94 60-140
Methyl-tert-butyl ether ug/L 60.150 120 60-140
Methylene Chloride ug/L 60.250 120 60-140
n-Butylbenzene ug/L 44.050 88 60-140
n-Propylbenzene ug/L 44.150 88 60-140
Naphthalene ug/L 50.750 101 60-140
o-Xylene ug/L 47.550 95 60-140
sec-Butylbenzene ug/L 46.050 92 60-140
Styrene ug/L 48.950 98 60-140
tert-Butylbenzene ug/L 39.650 79 60-140
Tetrachloroethene ug/L 44.650 89 60-140
Toluene ug/L 48.750 97 60-140
trans-1,2-Dichloroethene ug/L 55.750 111 60-140
trans-1,3-Dichloropropene ug/L 49.950 100 60-140
Trichloroethene ug/L 45.150 90 60-140
Trichlorofluoromethane ug/L 52.350 105 60-140
Vinyl chloride ug/L 39.950 80 60-140
1,2-Dichloroethane-d4 (S) % 97 70-130
4-Bromofluorobenzene (S) % 107 70-130
Toluene-d8 (S) % 105 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 04:38 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 12 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92323886
Friendly Mart
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1895797MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92323907001
1895798
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 108 60-140101 7 3020ND 21.5 20.2
1,1,1-Trichloroethane ug/L 20 106 60-140101 5 3020ND 21.1 20.1
1,1,2,2-Tetrachloroethane ug/L 20 100 60-140100 0 3020ND 20.0 20.0
1,1,2-Trichloroethane ug/L R120 77 60-140109 35 3020ND 15.4 21.8
1,1-Dichloroethane ug/L 20 108 60-14099 9 3020ND 21.6 19.8
1,1-Dichloroethene ug/L 20 113 60-14098 15 3020ND 22.6 19.5
1,1-Dichloropropene ug/L 20 111 60-140105 5 3020ND 22.2 21.1
1,2,3-Trichlorobenzene ug/L 20 108 60-140101 6 3020ND 21.5 20.2
1,2,3-Trichloropropane ug/L 20 101 60-140101 0 3020ND 20.2 20.3
1,2,4-Trichlorobenzene ug/L 20 106 60-140101 5 3020ND 21.2 20.2
1,2,4-Trimethylbenzene ug/L 20 104 60-140100 4 3020ND 20.8 20.1
1,2-Dibromo-3-
chloropropane
ug/L 20 94 60-140100 5 3020ND 18.9 19.9
1,2-Dibromoethane (EDB) ug/L 20 103 60-14098 5 3020ND 20.6 19.7
1,2-Dichlorobenzene ug/L 20 104 60-140103 1 3020ND 20.7 20.5
1,2-Dichloroethane ug/L 20 95 60-14090 5 3020ND 19.2 18.2
1,2-Dichloropropane ug/L 20 103 60-140102 1 3020ND 20.7 20.4
1,3,5-Trimethylbenzene ug/L 20 103 60-140101 2 3020ND 20.7 20.2
1,3-Dichlorobenzene ug/L 20 101 60-140101 0 3020ND 20.2 20.3
1,3-Dichloropropane ug/L 20 105 60-140103 2 3020ND 20.9 20.5
1,4-Dichlorobenzene ug/L 20 101 60-14098 3 3020ND 20.2 19.5
2,2-Dichloropropane ug/L 20 109 60-140105 4 3020ND 21.9 20.9
2-Chlorotoluene ug/L 20 103 60-140100 3 3020ND 20.6 20.0
4-Chlorotoluene ug/L 20 103 60-140100 4 3020ND 20.6 19.9
Benzene ug/L 20 113 60-140108 4 3020ND 22.6 21.6
Bromobenzene ug/L 20 100 60-14097 3 3020ND 20.1 19.4
Bromochloromethane ug/L 20 103 60-140102 1 3020ND 20.5 20.3
Bromodichloromethane ug/L 20 107 60-140105 2 3020ND 21.5 21.0
Bromoform ug/L 20 106 60-14097 9 3020ND 21.2 19.4
Bromomethane ug/L M120 59 60-14060 2 3020ND 11.8 12.1
Carbon tetrachloride ug/L 20 116 60-140117 1 3020ND 23.2 23.4
Chlorobenzene ug/L 20 105 60-140101 4 3020ND 21.0 20.1
Chloroethane ug/L 20 111 60-14095 16 3020ND 22.2 19.0
Chloroform ug/L 20 103 60-14098 6 3020ND 21.0 19.8
Chloromethane ug/L 20 101 60-14087 16 3020ND 20.3 17.3
cis-1,2-Dichloroethene ug/L 20 103 60-14099 4 3020ND 20.7 19.9
cis-1,3-Dichloropropene ug/L 20 87 60-140100 15 3020ND 17.3 20.0
Dibromochloromethane ug/L 20 107 60-140101 5 3020ND 21.3 20.2
Dibromomethane ug/L 20 102 60-140103 1 3020ND 20.4 20.7
Dichlorodifluoromethane ug/L 20 111 60-14096 14 3020ND 22.1 19.2
Diisopropyl ether ug/L 20 106 60-14097 9 3020ND 21.3 19.4
Ethylbenzene ug/L 20 108 60-140104 4 3020ND 21.6 20.8
Hexachloro-1,3-butadiene ug/L 20 123 60-140117 5 3020ND 24.7 23.4
Isopropylbenzene (Cumene) ug/L 20 109 60-14096 13 3020ND 21.8 19.2
m&p-Xylene ug/L 40 107 60-140102 6 3040ND 42.9 40.6
Methyl-tert-butyl ether ug/L 20 110 60-14096 14 3020ND 22.0 19.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 04:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92323886
Friendly Mart
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1895797MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92323907001
1895798
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methylene Chloride ug/L 20 105 60-14083 24 3020ND 21.1 16.5
n-Butylbenzene ug/L 20 106 60-140104 2 3020ND 21.2 20.8
n-Propylbenzene ug/L 20 104 60-140100 3 3020ND 20.8 20.1
Naphthalene ug/L 20 105 60-140105 0 3020ND 21.0 21.0
o-Xylene ug/L 20 108 60-14095 13 3020ND 21.5 19.0
sec-Butylbenzene ug/L 20 108 60-140104 4 3020ND 21.6 20.8
Styrene ug/L 20 107 60-14099 8 3020ND 21.5 19.8
tert-Butylbenzene ug/L 20 91 60-14089 1 3020ND 18.1 17.9
Tetrachloroethene ug/L 20 103 60-14097 5 3020ND 20.5 19.5
Toluene ug/L 20 83 60-140103 22 3020ND 16.6 20.6
trans-1,2-Dichloroethene ug/L 20 110 60-14095 15 3020ND 22.0 18.9
trans-1,3-Dichloropropene ug/L 20 81 60-140106 27 3020ND 16.2 21.2
Trichloroethene ug/L 20 106 60-140106 0 3020ND 21.2 21.1
Trichlorofluoromethane ug/L 20 115 60-140108 7 3020ND 23.1 21.6
Vinyl chloride ug/L 20 88 60-14075 16 3020ND 17.6 15.0
1,2-Dichloroethane-d4 (S) % 99 70-13094
4-Bromofluorobenzene (S) % 105 70-13099
Toluene-d8 (S) % 78 70-130100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 04:38 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 19
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92323886
Friendly Mart
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter.N2
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 04:38 PM
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Huntersville, NC 28078
[phone]
Page 15 of 19
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92323886
Friendly Mart
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92323886001 341690MW 3 MADEP VPH
92323886001 341612 342086MW 3 EPA 3010A EPA 6010
92323886001 341708MW 3 SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 04:38 PM
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Huntersville, NC 28078
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Page 16 of 19
Page 17 of 19
Page 18 of 19
Page 19 of 19
Page - 14

APPENDIX D

SLUG TEST DATA

AND ANALYSES

0.01
O. 2. 4. 6. 8.10.
Time (min)
AQTESOLV
,.-..
....,;
~
'--'
....,;
~
s 0,)
0,)
C,)
ro
~
~ rn
• .-4 o
10.
1.
0.1
O. 6. 12. 18. 24. 30.
Time (min)
DATA SET:
FM-MW6.DAT
12/27/16
AQUIFER MODEL:
Unconfined
SOLUTION METHOD:
Bouwer-Rice
PROJECT DA T A:
test date: 12/9/2016
test we 11: MW-6
obs. we 11: MW-6
TEST DATA:
HO = 3.47B ft
rc = 0.08333 ft
rw = 0.2 ft
L = 4.66 ft
b = 60. f t
H = 4.66 ft
PARAMETER ESTIMATES:
K = 0.0003696 ft/min
yO = 3.397 ft
AQTESOLV
..-...
.....,>
C+-4
'-'"
.....,>
l::
Q) a

Q)
C,)
Cd
~
~ rn 0l"""l
Q
10.
1.
0.1 o. 6. 12. lB. 24. 30.
Time (min)
DATA SET:
FM-MWB.DAT
12/27/16
AQU I FER MODEL:
Unconfined
SOL UT I ON ME THOD:
Bouwer-Rice
PROJECT DA T A:
test date: 12/9/2016
test well: MW-8
obs. we 11: MW-8
TEST DATA:
HO = 338<1 ft
rc = 0.08333 ft
rw = 0.2 ft
L = 4.78 ft
b = 60. f t
H = 4.78 ft
PARAMETER ESTIMATES:
K = 0.0003327 ft/min
yO = 3.234 ft
AQTESOLV

<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>

A Q T E S O L V R E S U L T S
Version 2.0

Developed by Glenn M. Duffield
(c) 1993, 1994 Geraghty & Miller, Inc.

12/27/16 15:18:34

================================================================================
TEST DESCRIPTION

Data set........... FM-MW2.DAT
Output file........ FM-MW2.OUT
Data set title..... FRIENDLY MART SLUG TEST - MW-2
Company............ HENRY NEMARGUT ENGINEERING
Project............ FRIENDLY MART
Client............. ROSE OIL COMPANY, INC.
Location........... 3055 STANTONSBURG RD, WILSON
Test date.......... 12/9/2016
Test well.......... MW-2
Obs. well.......... MW-2

Units of Measurement
Length.......... ft
Time............ min

Test Well Data
Initial displacement in well..... 3.067
Radius of well casing............ 0.08333
Radius of wellbore............... 0.2
Aquifer saturated thickness...... 60
Well screen length............... 5.07
Static height of water in well... 5.07
Gravel pack porosity............. 0.25
Effective well casing radius..... 0.1233
Effective wellbore radius........ 0.2
Log(Re/Rw)....................... 1.948
Constants A, B and C............. 2.303 , 0.371, 0.000
No. of observations.............. 115

================================================================================
ANALYTICAL METHOD

Bouwer-Rice (Unconfined Aquifer Slug Test)

================================================================================
RESULTS FROM STATISTICAL CURVE MATCHING

STATISTICAL MATCH PARAMETER ESTIMATES

Estimate Std. Error
K = 2.4207E-003 2.3122E-005 ft/min
y0 = 3.0263E 퍍 7.0165E-003 ft

ANALYSIS OF MODEL RESIDUALS

residual = observed - calculated
weighted residual = residual * weight

Weighted Residual Statistics:
Number of residuals............... 115
Number of estimated parameters.... 2
Degrees of freedom................ 113
Residual mean..................... 0.01257
Residual standard deviation....... 0.04191
Residual variance................. 0.001756

Model Residuals:

Time Observed Calculated Residual Weight
------------- ------------- ------------- ------------- -------------
0.006 3.051 3.0113 0.039705 1
0.01 3.036 3.0013 0.034667 1
0.015 3.017 2.9889 0.028074 1
0.019 3.003 2.979 0.023962 1
0.023 2.998 2.9692 0.028818 1
0.027 2.981 2.9594 0.02164 1
0.031 2.962 2.9496 0.012431 1
0.035 2.95 2.9398 0.010189 1
0.04 2.931 2.9277 0.003341 1
0.044 2.926 2.918 0.0080266 1
0.048 2.909 2.9083 0.00068008 1
0.052 2.902 2.8987 0.0033016 1
0.056 2.887 2.8891 -0.0021086 1
0.06 2.878 2.8796 -0.0015506 1
0.065 2.861 2.8676 -0.0066476 1
0.069 2.854 2.8582 -0.0041606 1
0.073 2.842 2.8487 -0.006705 1
0.077 2.832 2.8393 -0.0072806 1
0.081 2.825 2.8299 -0.0048875 1
0.085 2.808 2.8205 -0.012525 1
0.09 2.798 2.8089 -0.010866 1
0.094 2.793 2.7996 -0.0065738 1
0.098 2.776 2.7903 -0.014312 1
0.102 2.774 2.7811 -0.0070809 1
0.106 2.767 2.7719 -0.0048803 1
0.11 2.75 2.7627 -0.01271 1
0.115 2.738 2.7513 -0.01329 1
0.119 2.733 2.7422 -0.009188 1
0.123 2.723 2.7331 -0.010116 1
0.127 2.711 2.7241 -0.013074 1
0.131 2.704 2.7151 -0.011062 1
0.135 2.706 2.7061 -7.9869E-005 1
0.14 2.694 2.6949 -0.00089389 1
0.144 2.684 2.686 -0.0019784 1
0.148 2.677 2.6771 -9.2422E-005 1
0.152 2.665 2.6682 -0.0032358 1
0.156 2.655 2.6594 -0.0044085 1
0.16 2.652 2.6506 0.0013895 1
0.165 2.638 2.6397 -0.0016538 1
0.169 2.631 2.6309 7.8962E-005 1
0.173 2.631 2.6222 0.0087828 1
0.177 2.621 2.6135 0.0074578 1
0.181 2.614 2.6049 0.0091042 1
0.185 2.6 2.5963 0.0037219 1
0.19 2.595 2.5855 0.009454 1
0.194 2.585 2.577 0.0080078 1
0.198 2.573 2.5685 0.0045332 1
0.202 2.568 2.56 0.0080304 1
0.206 2.558 2.5515 0.0064995 1
0.21 2.549 2.5431 0.0059406 1
0.215 2.541 2.5325 0.0084527 1
0.219 2.539 2.5242 0.014831 1
0.223 2.525 2.5158 0.0091818 1
0.227 2.519 2.5075 0.011505 1
0.231 2.505 2.4992 0.0058004 1
0.235 2.5 2.4909 0.0090684 1
0.24 2.49 2.4806 0.0093651 1
0.244 2.486 2.4724 0.013572 1
0.248 2.467 2.4642 0.0027512 1
0.252 2.462 2.4561 0.0059037 1
0.256 2.452 2.448 0.0040291 1
0.26 2.447 2.4399 0.0071277 1
0.265 2.437 2.4298 0.0072133 1
0.269 2.427 2.4217 0.0052517 1
0.273 2.418 2.4137 0.0042636 1
0.277 2.408 2.4058 0.0022489 1
0.281 2.399 2.3978 0.0012078 1
0.285 2.386 2.3899 -0.0038596 1
0.29 2.375 2.38 -0.0049808 1
0.294 2.37 2.3721 -0.0021071 1
0.298 2.355 2.3643 -0.0092595 1
0.302 2.35 2.3564 -0.0064379 1
0.306 2.341 2.3486 -0.0076421 1
0.31 2.329 2.3409 -0.011872 1
0.315 2.324 2.3312 -0.0071958 1
0.319 2.314 2.3235 -0.0094835 1
0.323 2.304 2.3158 -0.011797 1
0.327 2.297 2.3081 -0.011135 1
0.331 2.29 2.3005 -0.010499 1
0.419 2.111 2.1388 -0.027754 1
0.502 1.964 1.9966 -0.032634 1
0.585 1.828 1.864 -0.035957 1
0.669 1.705 1.7387 -0.033656 1
0.752 1.591 1.6231 -0.032123 1
0.835 1.485 1.5153 -0.030266 1
0.919 1.384 1.4134 -0.029405 1
1.002 1.29 1.3195 -0.029485 1
1.085 1.2 1.2318 -0.031805 1
1.169 1.121 1.149 -0.027999 1
1.252 1.044 1.0726 -0.028648 1
1.335 0.973 1.0014 -0.028371 1
1.419 0.915 0.93406 -0.019055 1
1.502 0.86 0.87199 -0.011987 1
1.585 0.814 0.81404 -4.387E-005 1
1.669 0.764 0.75932 0.0046787 1
1.752 0.722 0.70886 0.013136 1
1.835 0.674 0.66176 0.01224 1
1.919 0.637 0.61727 0.019725 1
2.002 0.601 0.57626 0.024743 1
2.502 0.446 0.38082 0.065178 1
3.002 0.347 0.25167 0.095332 1
3.502 0.286 0.16632 0.11968 1
4.002 0.238 0.10991 0.12809 1
4.502 0.211 0.072635 0.13837 1
5.002 0.18 0.048001 0.132 1
5.502 0.158 0.031722 0.12628 1
6.002 0.145 0.020963 0.12404 1
6.502 0.128 0.013854 0.11415 1
7 0.113 0.0091705 0.10383 1
7.5 0.106 0.0060604 0.09994 1
8 0.091 0.004005 0.086995 1
8.5 0.086 0.0026467 0.083353 1
9 0.077 0.0017491 0.075251 1
9.5 0.074 0.0011559 0.072844 1
10 0.064 0.00076389 0.063236 1

================================================================================
RESULTS FROM VISUAL CURVE MATCHING

VISUAL MATCH PARAMETER ESTIMATES

Estimate
K = 2.4207E-003 ft/min
y0 = 3.0263E 퍍 ft

<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>

A Q T E S O L V R E S U L T S
Version 2.0

Developed by Glenn M. Duffield
(c) 1993, 1994 Geraghty & Miller, Inc.

12/27/16 15:23:56

================================================================================
TEST DESCRIPTION

Data set........... FM-MW6.DAT
Output file........ FM-MW6.OUT
Data set title..... FRIENDLY MART SLUG TEST - MW-6
Company............ HENRY NEMARGUT ENGINEERING
Project............ FRIENDLY MART
Client............. ROSE OIL COMPANY, INC.
Location........... 3055 STANTONSBURG RD, WILSON
Test date.......... 12/9/2016
Test well.......... MW-6
Obs. well.......... MW-6

Units of Measurement
Length.......... ft
Time............ min

Test Well Data
Initial displacement in well..... 3.478
Radius of well casing............ 0.08333
Radius of wellbore............... 0.2
Aquifer saturated thickness...... 60
Well screen length............... 4.66
Static height of water in well... 4.66
Gravel pack porosity............. 0.25
Effective well casing radius..... 0.1233
Effective wellbore radius........ 0.2
Log(Re/Rw)....................... 1.879
Constants A, B and C............. 2.243 , 0.359, 0.000
No. of observations.............. 123

================================================================================
ANALYTICAL METHOD

Bouwer-Rice (Unconfined Aquifer Slug Test)

================================================================================
RESULTS FROM STATISTICAL CURVE MATCHING

STATISTICAL MATCH PARAMETER ESTIMATES

Estimate Std. Error
K = 3.6965E-004 5.9534E-006 ft/min
y0 = 3.3973E 퍍 9.0905E-003 ft

ANALYSIS OF MODEL RESIDUALS

residual = observed - calculated
weighted residual = residual * weight

Weighted Residual Statistics:
Number of residuals............... 123
Number of estimated parameters.... 2
Degrees of freedom................ 121
Residual mean..................... 0.008871
Residual standard deviation....... 0.08126
Residual variance................. 0.006604

Model Residuals:

Time Observed Calculated Residual Weight
------------- ------------- ------------- ------------- -------------
0.004 3.478 3.3956 0.082356 1
0.008 3.478 3.394 0.083993 1
0.012 3.471 3.3924 0.078629 1
0.017 3.466 3.3903 0.075673 1
0.021 3.464 3.3887 0.075308 1
0.025 3.461 3.3871 0.073941 1
0.029 3.454 3.3854 0.068574 1
0.033 3.452 3.3838 0.068206 1
0.037 3.449 3.3822 0.066837 1
0.042 3.449 3.3801 0.068875 1
0.046 3.445 3.3785 0.066505 1
0.05 3.445 3.3769 0.068134 1
0.054 3.433 3.3752 0.057762 1
0.058 3.43 3.3736 0.056389 1
0.062 3.43 3.372 0.058015 1
0.067 3.43 3.37 0.060047 1
0.071 3.423 3.3683 0.054672 1
0.075 3.418 3.3667 0.051295 1
0.079 3.418 3.3651 0.052918 1
0.083 3.413 3.3635 0.049541 1
0.088 3.409 3.3614 0.047567 1
0.092 3.406 3.3598 0.046188 1
0.096 3.404 3.3582 0.045808 1
0.1 3.399 3.3566 0.042427 1
0.104 3.397 3.355 0.042045 1
0.108 3.389 3.3533 0.035662 1
0.113 3.387 3.3513 0.035683 1
0.117 3.387 3.3497 0.037298 1
0.121 3.387 3.3481 0.038913 1
0.125 3.387 3.3465 0.040527 1
0.129 3.384 3.3449 0.039141 1
0.133 3.377 3.3432 0.033753 1
0.138 3.377 3.3412 0.035768 1
0.142 3.37 3.3396 0.030378 1
0.146 3.367 3.338 0.028988 1
0.15 3.365 3.3364 0.028598 1
0.154 3.362 3.3348 0.027206 1
0.158 3.355 3.3332 0.021814 1
0.163 3.353 3.3312 0.021822 1
0.167 3.352 3.3296 0.022428 1
0.171 3.345 3.328 0.017033 1
0.175 3.343 3.3264 0.016638 1
0.179 3.343 3.3248 0.018241 1
0.183 3.338 3.3232 0.014844 1
0.187 3.338 3.3216 0.016446 1
0.192 3.335 3.3196 0.015448 1
0.196 3.335 3.318 0.017048 1
0.2 3.328 3.3164 0.011647 1
0.204 3.326 3.3148 0.011246 1
0.208 3.323 3.3132 0.0098441 1
0.212 3.323 3.3116 0.011441 1
0.217 3.316 3.3096 0.0064368 1
0.221 3.311 3.308 0.0030323 1
0.225 3.311 3.3064 0.004627 1
0.229 3.309 3.3048 0.004221 1
0.233 3.309 3.3032 0.0058142 1
0.237 3.304 3.3016 0.0024066 1
0.242 3.301 3.2996 0.001396 1
0.246 3.301 3.298 0.0029867 1
0.25 3.294 3.2964 -0.0024233 1
0.254 3.291 3.2948 -0.0038342 1
0.258 3.289 3.2932 -0.0042458 1
0.262 3.282 3.2917 -0.0096582 1
0.267 3.282 3.2897 -0.0076747 1
0.271 3.279 3.2881 -0.0090888 1
0.275 3.279 3.2865 -0.0075036 1
0.279 3.277 3.2849 -0.0079193 1
0.283 3.279 3.2833 -0.0043356 1
0.287 3.274 3.2818 -0.0077528 1
0.292 3.272 3.2798 -0.0077753 1
0.296 3.262 3.2782 -0.016194 1
0.3 3.265 3.2766 -0.011614 1
0.304 3.26 3.275 -0.015034 1
0.308 3.26 3.2735 -0.013455 1
0.312 3.257 3.2719 -0.014877 1
0.317 3.255 3.2699 -0.014906 1
0.321 3.255 3.2683 -0.013329 1
0.325 3.25 3.2668 -0.016754 1
0.329 3.25 3.2652 -0.015179 1
0.417 3.198 3.2307 -0.032723 1
0.5 3.147 3.1986 -0.051559 1
0.583 3.103 3.1667 -0.063715 1
0.667 3.064 3.1348 -0.07081 1
0.75 3.025 3.1036 -0.0786 1
0.833 2.992 3.0727 -0.080701 1
0.917 2.953 3.0417 -0.088743 1
1 2.909 3.0115 -0.10246 1
1.083 2.871 2.9815 -0.11048 1
1.167 2.837 2.9514 -0.11444 1
1.25 2.798 2.9221 -0.12406 1
1.333 2.76 2.893 -0.13296 1
1.417 2.726 2.8638 -0.13782 1
1.5 2.697 2.8353 -0.13831 1
1.583 2.666 2.8071 -0.14108 1
1.667 2.64 2.7788 -0.1388 1
1.75 2.62 2.7511 -0.13113 1
1.833 2.584 2.7237 -0.13974 1
1.917 2.563 2.6963 -0.1333 1
2 2.534 2.6695 -0.13546 1
2.5 2.385 2.5133 -0.12831 1
3 2.248 2.3663 -0.11829 1
3.5 2.125 2.2279 -0.10288 1
4 2.003 2.0976 -0.094556 1
4.5 1.89 1.9749 -0.08486 1
5 1.794 1.8593 -0.065341 1
5.5 1.698 1.7506 -0.05258 1
6 1.612 1.6482 -0.03618 1
6.5 1.535 1.5518 -0.01677 1
7 1.458 1.461 -0.0029998 1
7.5 1.391 1.3755 0.015461 1
8 1.323 1.2951 0.027923 1
8.5 1.263 1.2193 0.043678 1
9 1.206 1.148 0.058002 1
9.5 1.155 1.0808 0.074154 1
10 1.103 1.0176 0.085378 1
12 0.93 0.79961 0.13039 1
14 0.795 0.6283 0.1667 1
16 0.687 0.4937 0.1933 1
18 0.602 0.38793 0.21407 1
20 0.526 0.30482 0.22118 1
22 0.468 0.23952 0.22848 1
24 0.429 0.1882 0.2408 1
24.57 0.41 0.1757 0.2343 1

================================================================================
RESULTS FROM VISUAL CURVE MATCHING

VISUAL MATCH PARAMETER ESTIMATES

Estimate
K = 3.6965E-004 ft/min
y0 = 3.3973E 퍍 ft

<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>
<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>

A Q T E S O L V R E S U L T S
Version 2.0

Developed by Glenn M. Duffield
(c) 1993, 1994 Geraghty & Miller, Inc.

12/27/16 15:41:36

================================================================================
TEST DESCRIPTION

Data set........... FM-MW8.DAT
Output file........ FM-MW8.OUT
Data set title..... FRIENDLY MART SLUG TEST - MW-8
Company............ HENRY NEMARGUT ENGINEERING
Project............ FRIENDLY MART
Client............. ROSE OIL COMPANY, INC.
Location........... 3055 STANTONSBURG RD, WILSON
Test date.......... 12/9/2016
Test well.......... MW-8
Obs. well.......... MW-8

Units of Measurement
Length.......... ft
Time............ min

Test Well Data
Initial displacement in well..... 3.384
Radius of well casing............ 0.08333
Radius of wellbore............... 0.2
Aquifer saturated thickness...... 60
Well screen length............... 4.78
Static height of water in well... 4.78
Gravel pack porosity............. 0.25
Effective well casing radius..... 0.1233
Effective wellbore radius........ 0.2
Log(Re/Rw)....................... 1.9
Constants A, B and C............. 2.260 , 0.362, 0.000
No. of observations.............. 122

================================================================================
ANALYTICAL METHOD

Bouwer-Rice (Unconfined Aquifer Slug Test)

================================================================================
RESULTS FROM STATISTICAL CURVE MATCHING

STATISTICAL MATCH PARAMETER ESTIMATES

Estimate Std. Error
K = 3.3269E-004 8.2380E-006 ft/min
y0 = 3.2337E퍍 1.3083E-002 ft

ANALYSIS OF MODEL RESIDUALS

residual = observed - calculated
weighted residual = residual * weight

Weighted Residual Statistics:
Number of residuals............... 122
Number of estimated parameters.... 2
Degrees of freedom................ 120
Residual mean..................... 0.009097
Residual standard deviation....... 0.1178
Residual variance................. 0.01388

Model Residuals:

Time Observed Calculated Residual Weight
------------- ------------- ------------- ------------- -------------
0.006 3.377 3.2316 0.14542 1
0.01 3.377 3.2302 0.14684 1
0.015 3.365 3.2284 0.13662 1
0.019 3.363 3.227 0.13604 1
0.023 3.356 3.2255 0.13046 1
0.027 3.353 3.2241 0.12888 1
0.031 3.348 3.2227 0.1253 1
0.035 3.339 3.2213 0.11771 1
0.04 3.339 3.2195 0.11949 1
0.044 3.336 3.2181 0.1179 1
0.048 3.329 3.2167 0.11232 1
0.052 3.324 3.2153 0.10874 1
0.056 3.32 3.2138 0.10615 1
0.06 3.317 3.2124 0.10457 1
0.065 3.305 3.2107 0.094334 1
0.069 3.303 3.2093 0.093748 1
0.073 3.3 3.2078 0.09216 1
0.077 3.296 3.2064 0.089573 1
0.081 3.296 3.205 0.090984 1
0.085 3.286 3.2036 0.082395 1
0.09 3.284 3.2018 0.082158 1
0.094 3.279 3.2004 0.078567 1
0.098 3.272 3.199 0.072976 1
0.102 3.267 3.1976 0.069384 1
0.106 3.267 3.1962 0.070792 1
0.11 3.259 3.1948 0.064198 1
0.115 3.257 3.193 0.063956 1
0.119 3.25 3.1916 0.058362 1
0.123 3.247 3.1902 0.056767 1
0.127 3.236 3.1888 0.047171 1
0.131 3.236 3.1874 0.048575 1
0.135 3.233 3.186 0.046978 1
0.14 3.233 3.1843 0.048731 1
0.144 3.221 3.1829 0.038133 1
0.148 3.223 3.1815 0.041534 1
0.152 3.216 3.1801 0.035934 1
0.156 3.214 3.1787 0.035334 1
0.16 3.214 3.1773 0.036733 1
0.165 3.211 3.1755 0.035481 1
0.169 3.209 3.1741 0.034879 1
0.173 3.204 3.1727 0.031277 1
0.177 3.199 3.1713 0.027673 1
0.181 3.192 3.1699 0.022069 1
0.185 3.192 3.1685 0.023465 1
0.19 3.19 3.1668 0.023208 1
0.194 3.189 3.1654 0.023602 1
0.198 3.182 3.164 0.017995 1
0.202 3.18 3.1626 0.017388 1
0.206 3.175 3.1612 0.01378 1
0.21 3.175 3.1598 0.015172 1
0.215 3.168 3.1581 0.0099104 1
0.219 3.168 3.1567 0.011301 1
0.223 3.165 3.1553 0.0096901 1
0.227 3.156 3.1539 0.0020791 1
0.231 3.158 3.1525 0.0054674 1
0.235 3.151 3.1511 -0.00014487 1
0.24 3.151 3.1494 0.0015889 1
0.244 3.148 3.148 -2.4709E-005 1
0.248 3.151 3.1466 0.004361 1
0.252 3.143 3.1453 -0.0022538 1
0.256 3.139 3.1439 -0.0048693 1
0.26 3.134 3.1425 -0.0084854 1
0.265 3.131 3.1408 -0.0097563 1
0.269 3.127 3.1394 -0.012374 1
0.273 3.124 3.138 -0.013992 1
0.277 3.119 3.1366 -0.017611 1
0.281 3.117 3.1352 -0.01823 1
0.285 3.117 3.1338 -0.01685 1
0.29 3.117 3.1321 -0.015125 1
0.294 3.114 3.1307 -0.016747 1
0.298 3.105 3.1294 -0.024369 1
0.302 3.105 3.128 -0.022991 1
0.306 3.097 3.1266 -0.029614 1
0.31 3.097 3.1252 -0.028238 1
0.315 3.095 3.1235 -0.028518 1
0.319 3.095 3.1221 -0.027143 1
0.323 3.09 3.1208 -0.030769 1
0.327 3.085 3.1194 -0.034395 1
0.331 3.083 3.118 -0.035022 1
0.419 3.027 3.088 -0.060965 1
0.502 2.974 3.0599 -0.085882 1
0.585 2.93 3.0321 -0.10205 1
0.669 2.877 3.0041 -0.12715 1
0.752 2.832 2.9768 -0.14483 1
0.835 2.788 2.9498 -0.16175 1
0.919 2.757 2.9226 -0.16561 1
1.002 2.721 2.896 -0.17503 1
1.085 2.682 2.8697 -0.18769 1
1.169 2.653 2.8433 -0.19028 1
1.252 2.624 2.8174 -0.19342 1
1.335 2.59 2.7918 -0.2018 1
1.419 2.566 2.7661 -0.2001 1
1.502 2.542 2.7409 -0.19895 1
1.585 2.514 2.716 -0.20202 1
1.669 2.485 2.691 -0.20602 1
1.752 2.463 2.6665 -0.20355 1
1.835 2.437 2.6423 -0.2053 1
1.919 2.417 2.618 -0.20098 1
2.002 2.391 2.5942 -0.20317 1
2.502 2.252 2.4553 -0.20325 1
3.002 2.141 2.3238 -0.18278 1
3.502 2.033 2.1993 -0.16634 1
4.002 1.932 2.0816 -0.14957 1
4.502 1.853 1.9701 -0.1171 1
5.002 1.772 1.8646 -0.092602 1
5.502 1.692 1.7648 -0.072754 1
6.002 1.624 1.6703 -0.046252 1
6.502 1.56 1.5808 -0.020811 1
7 1.504 1.4965 0.0075106 1
7.5 1.454 1.4164 0.037647 1
8 1.396 1.3405 0.055492 1
8.5 1.341 1.2687 0.072275 1
9 1.298 1.2008 0.097214 1
9.5 1.252 1.1365 0.11552 1
10 1.209 1.0756 0.13337 1
12 1.06 0.86308 0.19692 1
14 0.935 0.69254 0.24246 1
16 0.825 0.5557 0.2693 1
18 0.728 0.44589 0.28211 1
20 0.644 0.35778 0.28622 1
22 0.572 0.28709 0.28491 1
22.73 0.553 0.26492 0.28808 1

================================================================================
RESULTS FROM VISUAL CURVE MATCHING

VISUAL MATCH PARAMETER ESTIMATES

Estimate
K = 3.3269E-004 ft/min
y0 = 3.2337E퍍 ft

<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>