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HomeMy WebLinkAbout9203_Feltonsville_MSWLF_GWMR_20170601Closed Feltonsville Landfill
Facility Permit No. 9203-
MSWLF-1980
Semi-Annual Sampling Report
(April 2017 Sampling Event)
Wake County
Report
Prepared June 2017
5400 Glenwood Ave, Suite 400
Raleigh, North Carolina 27612
tel: 919 325-3500
fax: 919 781-5730
June 1, 2017
Ms. Jaclynne Drummond
North Carolina Department of Environmental Quality
Division of Waste Management
Solid Waste Section
2090 U.S. 70 Highway
Swannanoa, North Carolina 28778
Subject: April 2017 Semi-Annual Groundwater Sampling Report
Closed Feltonsville Landfill - Wake County
Facility Permit No. 9203-MSWLF-1980
Dear Ms. Drummond:
CDM Smith Inc., on behalf of Wake County, is submitting an electronic copy of the April 2017
semi-annual sampling event report. This letter report presents the results of the semi-annual sampling
event that was recently completed at the Closed Feltonsville Landfill and constitutes the first semi-
annual sampling event for 2017. The current groundwater monitoring network consists of the following
wells: MW-2, -4, -6, -8, -9, -10, -11, -12, -13, -14, -15, -16, -17, -18, -19, -20, -21, -22, -23, -24, -25, -26,
-27, -28, and -29 as well as surface water sampling locations SW-1, -2, and -3. Monitoring wells MW-2,
-6, -8, -9, -10, -11, -12, -13, -14, -15, -16, -17, -18, -19, -20, -28, and -29 monitor the closed Feltonsville
Landfill. The remaining wells (i.e. MW-4, -21, -22, -23, -24, -25, -26, and -27) monitor the old cells
located in the back of the property. Field activities, sampling results for all wells and surface water
locations, an evaluation of the groundwater corrective action effectiveness, and recommendations are
discussed below.
Field Activities
Groundwater and surface water samples from the Closed Feltonsville Landfill were collected on April 27-
28, 2017. Monitoring well and surface water sample locations are shown on Figure 1. Construction
details for each monitoring well are summarized in Table 1.
Samples were collected from the monitoring wells by use of a peristaltic pump or disposable, laboratory
decontaminated bailers. Groundwater elevations were measured at each well on April 26, 2017, using
an electronic water level indicator with an accuracy of 0.01 feet and are presented in Table 1. These
groundwater elevations were used to construct potentiometric contours for this sampling event and are
shown on Figure 1. The groundwater elevations and potentiometric contours were also used to estimate
groundwater velocities at each well as presented in Table 2.
Ms. Jaclynne Drummond
June 1, 2017
Page 2
After depth to groundwater was determined, three well volumes of water were removed from each well
prior to sampling to provide fresh formation water within the well water column. Each well volume and
surface water sample was measured in the field for pH, conductivity, temperature, turbidity, dissolved
oxygen, and oxidation-reduction potential using a YSI-556 multi-parameter water quality meter and a
HANNA HI 98703 turbidity meter. Wells that had elevated turbidity were allowed to stabilize prior to
sample collection. The water quality parameters at the time of sampling are provided in Table 3.
Sampling Results
Groundwater and surface water samples were analyzed by Shealy Environmental Services, Inc. located
in West Columbia, South Carolina, for the North Carolina Appendix I volatile organic compounds (VOCs)
plus dichlorodifluoromethane and Appendix I metals plus mercury. Additional samples were collected
from select monitoring wells to evaluate natural attenuation and the effectiveness of the corrective
action. Results of the additional sampling and an evaluation of natural attenuation are discussed in the
next section of this report.
In accordance with North Carolina Department of Environmental Quality - Solid Waste Section (SWS)
guidelines the analytical results were reported to the laboratory specific method detection limit (MDL)
and are quantifiable at or below SWS Limits (SWSLs). All monitoring wells and surface water locations
for the closed Feltonsville Landfill had detections of analytes above the MDL with a majority of the
detections below SWSLs. These detections were qualified as estimated or “J” flags. “B” flags, which
indicate an analyte was detected in the method blank, were also reported.
The following list indicates the analytes detected above the MDL at each sampling location. No “J” flag
detections are provided. Underlined analytes exceeded the 15A NCAC 02L .0202 (NC 2L) Groundwater
Quality Standard, Groundwater Protection Standard, or the 15A NCAC 02B Surface Water Quality
Standard for Class C Waters. A complete summary of all detected and estimated concentrations for the
March 2011 through the April 2017 sampling events, as well as historical detections of herbicides,
pesticides, and polychlorinated biphenyls, is provided in Table 4. Laboratory data reports are provided in
Appendix A.
MW-2 (Background)
Metals: Barium
Volatile Organic Compounds: None Detected
MW-4
Metals: None Detected
Volatile Organic Compounds: None Detected
Ms. Jaclynne Drummond
June 1, 2017
Page 3
MW-6
Metals: Barium, Cobalt, Zinc
Volatile Organic Compounds: 1,1-Dichloroethane
MW-8
Inorganics: Barium, Sodium, Total Dissolved Solids
Volatile Organic Compounds: None Detected
MW-9
Inorganics: Barium, Cobalt, Copper, Sodium, Total Dissolved Solids
Volatile Organic Compounds: Benzene, Chloroethane, 1,1-Dichloroethane
MW-10
Inorganics: Arsenic, Barium, Cobalt, Sodium, Total Dissolved Solids
Volatile Organic Compounds: Benzene, 1,4-Dichlorobenzene, 1,1-Dichloroethane, Vinyl Chloride
MW-11
Metals: None Detected
Volatile Organic Compounds: None Detected
MW-12
Metals: Barium
Volatile Organic Compounds: None Detected
MW-13
Metals: Barium, Mercury, Zinc
Volatile Organic Compounds: Benzene, Chlorobenzene, 1,4-Dichlorobenzene
MW-14
Metals: Barium, Mercury
Volatile Organic Compounds: None Detected
MW-15
Metals: Barium
Volatile Organic Compounds: Chlorobenzene
MW-16
Metals: Arsenic, Barium
Volatile Organic Compounds: Chloroethane, 1,1-Dichloroethane, Trichloroethene
Ms. Jaclynne Drummond
June 1, 2017
Page 4
MW-17
Metals: Barium
Volatile Organic Compounds: 1,1-Dichloroethane
MW-18
Metals: Barium, Zinc
Volatile Organic Compounds: None Detected
MW-19
Inorganics: Barium, Sodium, Total Dissolved Solids
Volatile Organic Compounds: None Detected
MW-20
Metals: Barium
Volatile Organic Compounds: None Detected
MW-21
Metals: None Detected
Volatile Organic Compounds: None Detected
MW-22
Metals: Barium
Volatile Organic Compounds: None Detected
MW-23
Metals: Barium, Zinc
Volatile Organic Compounds: None Detected
MW-24
Metals: Arsenic, Barium
Volatile Organic Compounds: None Detected
MW-25
Metals: Barium
Volatile Organic Compounds: None Detected
MW-26
Metals: Cobalt, Zinc
Volatile Organic Compounds: Benzene, Chlorobenzene, 1,4-Dichlorobenzene
Ms. Jaclynne Drummond
June 1, 2017
Page 5
MW-27
Metals: Barium
Volatile Organic Compounds: 1,1-Dichloroethane
MW-28
Metals: Barium, Chromium, Copper, Zinc
Volatile Organic Compounds: None Detected
MW-29
Inorganics: Sodium, Zinc, Total Dissolved Solids
Volatile Organic Compounds: None Detected
SW-1
Metals: None Detected
Volatile Organic Compounds: None Detected
SW-2
Metals: None Detected
Volatile Organic Compounds: None Detected
SW-3
Metals: None Detected
Volatile Organic Compounds: None Detected
Equipment Blank
Metals: None Detected
Volatile Organic Compounds: None Detected
Trip Blank
Metals: Not analyzed
Volatile Organic Compounds: None Detected
“J” flags were not included in the previous list, but several sampling locations had “J” flag detections
that exceeded the standards. The “J” flag constituents above the standards along with their location are
listed below:
Antimony: MW-14
Cadmium: SW-3
Cobalt: MW-8, -11, -13, -16, -18, -19, -22, -23, -24, -28, and -29
Lead: SW-2 and -3
Ms. Jaclynne Drummond
June 1, 2017
Page 6
Vanadium: MW-2, -4, -6, -8, -9, -10, -11, -13, -14, -15, -17, -18, -19, -20, -21, -22, -23, -24,
-25, -26, -27, -28, and -29
Equipment and trip blanks were analyzed for quality control. A duplicate sample was also collected for
quality control. The duplicate sample, labeled DUP, was collected from MW-12 and had similar
concentrations to the MW-12 sample, with the exception of estimated detections of copper and
mercury in the parent sample. Additionally, an estimated concentration of dichlorofluoromethane was
detected in the duplicate sample, but not the parent sample. The equipment blank had “J” flag
detections of acetone and 2-butatone below their respective NC 2L Standard. Vanadium was detected
as an estimated concentration in the equipment blank above its Groundwater Protection Standard. No
VOCs were detected in the trip blank above the MDLs. Table 5 presents a summary of all parameters
detected during the April 2017 sampling event that exceeded the NC 2L or Groundwater Protection
Standards.
Monitored Natural Attenuation Sampling
Additional groundwater samples were collected from the background well, MW-2, and downgradient
monitoring wells MW-8, -9, -10, -12, -13, and -14. The samples were analyzed for alkalinity, biochemical
oxygen demand, chemical oxygen demand, carbon dioxide, chloride, dissolved hydrogen, methane,
ethane, ethene, volatile fatty acids (i.e. acetic, butyric, lactic, propionic, and pyruvic), nitrate, sulfate,
sulfide, and total organic carbon. Ferrous iron was also analyzed using a HACH test field kit due to the
short hold time (i.e. 15 minutes). These additional samples were collected to monitor for natural
attenuation as part of the approved corrective action program as required by SWS guidelines. Additional
samples were also collected from wells MW-19 and -29, which are located downgradient of the injection
area, in order to monitor the effectiveness of the injection. Sampling results are provided in Table 6 and
trend figures of total detected VOCs for select wells are presented on Figures 2-10.
Corrective Action via In situ Bioremediation Injection
In accordance with the Corrective Action Plan that was approved by the SWS in a letter dated December
1, 2011, two in situ bioremediation injections have been completed. Phase I consisted of injecting
sodium lactate into 5 injection wells upgradient of monitoring wells MW-8, -9, and -10 on June 18-21,
2012. A total of 1,268 gallons of a 10% sodium lactate solution were injected resulting in each well
receiving approximately 254 gallons of the sodium lactate solution.
Phase I post-injection samples were collected 1, 2, and 5 months after injection. During each sampling
event, samples from MW-8, -9, -10, -19, and -29 were analyzed for the following field measurements:
pH, temperature, oxidation-reduction potential, dissolved oxygen, conductivity, turbidity, nitrate,
sulfate, ferrous iron, carbon dioxide, and alkalinity along with laboratory analyses of chlorides, chemical
oxygen demand, VOCs, dissolved gases (i.e. methane, ethane, and ethene), sodium, and total dissolved
solids. Volatile fatty acids were also collected during the 1 month post-injection sampling event.
Ms. Jaclynne Drummond
June 1, 2017
Page 7
Additionally, samples were collected from MW-8, -9, and -10 and analyzed for bacterial population size
and functional gene presence during the baseline and 5 month post-injection sampling events.
Analytical results for each sampling event are summarized in Tables 4 and 6.
Analytical results post-sodium lactate injection for MW-8, -9, and -10 indicated that bioremediation was
occurring with no VOCs detected above NC 2L standards in MW-8 or -10, with the exception of 1,1-
dichloroethane detected in samples collected from MW-10 in July 2012. MW-9 had detections of 1,1-
dichloroethane, tetrachloroethene, trichloroethene, and vinyl chloride above NC 2L standards, but
contaminant concentrations were decreasing. DNA analyses revealed healthy populations of bacteria
(Dehalococcoides sp) in MW-9 and -10 that continued to reduce contaminant concentrations. Bacterial
populations in MW-8 decreased as a result of little to no VOCs being detected during the post-injection
sampling.
The Phase I injection of sodium lactate successfully caused degradation of trichloroethene and
tetrachloroethene to daughter products using enhanced anaerobic bioremediation in the injection area.
Although the Phase I injection reduced contaminant concentrations, a second injection was needed to
supply a longer lasting source of electron donors. Biodegradation can be sustained for as long as
sufficient concentrations of substrate remain in the groundwater. For this reason, emulsified vegetable
oil was utilized in the Phase 2 injection as it is a slow-release compound, and therefore should release
organic carbon into the groundwater for three to five years, depending on site conditions.
During the Phase 2 injection, a 10% emulsified vegetable oil solution was injected into the injection wells
on March 25-27, 2013. Injection at each well consisted of approximately 220 gallons of water containing
approximately 22 gallons of the emulsified vegetable oil product. The emulsified vegetable oil product
consisted of 60% emulsified vegetable oil and 4% sodium lactate by weight, which resulted in a total
injection volume of 1,100 gallons of water and 110 gallons of emulsified vegetable oil product.
Post-injection samples were collected 1, 4, 7, 10, and 12 months after injection. The April 2014
monitoring event concluded the post-injection monitoring. Analyses for each sampling event were
similar to the Phase I events except that a DNA analyses to determine bacterial population size and
functional gene presence was only done during the April 2014 sampling event.
No VOCs have been detected above the standards in MW-8 since the November 2011 semi-annual
sampling event. Benzene and 1,1-dichloroethane were detected above their respective NC 2L Standards
in MW-9 during the April 2017 sampling event. The concentration of 1,1,-dichloroethane in MW-9 shows
a decreasing trend. Benzene was detected slightly above the standard (1 part per billion (ppb)) at 1.1
ppb. Historically, benzene has been detected as a “J” flag detection below the standards with the
exception of the May 2015 sampling event were it was detected at 1.1 ppb.
Ms. Jaclynne Drummond
June 1, 2017
Page 8
MW-10 samples had concentrations of benzene, 1,1-dichloroethane, and an estimated concentration of
vinyl chloride above their respective NC 2L Standards. 1,1-Dichloroethane and vinyl chloride show a
decreasing trend. Concentrations of benzene have historically fluctuated at MW-10.
No VOCs were detected in samples collected from bedrock monitoring well MW-19 during the April
2017 sampling event with the exception of an estimated concentration of trans-1,2-dichloroethene
below the NC 2L Standard. Historically, VOCs have never been detected above the standards in
monitoring well MW-19.
MW-29, located at the compliance boundary, has not had any chlorinated ethenes detected above NC
2L Standards since November 2012. No VOCs were detected in samples collected from MW-29 during
the April 2017 sampling event with the exception of an estimated concentration of acetone below its NC
2L Standard. Concentrations of 1,1-dichloroethane have decreased following the injection events. 1,1-
Dichloroethane has been detected below the NC 2L Standard since the January 2014 post-injection
sampling event with the exception of the October 2014 semi-annual sampling event (7.2 ppb) when it
was detected slightly above the NC 2L Standard (6 ppb).
Dechlorination of chlorinated ethenes from tetrachloroethene to ethene is ongoing. Chlorinated ethene
concentrations in MW-9 and -10 remain below the NC 2L Standards. The geochemical data indicates
favorable conditions for reductive dechlorination based on samples collected from MW-9 and -10 during
the April 2017 monitoring event. Subsequent monitoring events will be evaluated to identify any trends.
Recommendations
Wake County will continue with the semi-annual assessment monitoring program. All wells will continue
to be sampled for Appendix I VOCs plus dichlorodifluoromethane and Appendix I metals plus mercury.
Samples collected from MW-2, -8, -9, -10, -12, -13, and -14 will also be analyzed for natural attenuation
parameters. The next semi-annual sampling event will be completed in the fall of 2017.
Ms. Jaclynne Drummond
June 1, 2017
Page 9
If you have any questions or require further explanation, do not hesitate to call me at 919-325-3500.
Very truly yours,
Mathew F. Colone, P.G.
CDM Smith Inc.
cc: John Roberson, WCSWM
Elliott Cornell, WCSWM
Facility Permit
Number
Monitoring
Well Code
Installation
Date Latitude Longitude
Geology of
Screened
Interval
Total Depth
(feet BTOC)
Screened
Interval
(feet BTOC)
Seal
Interval
(feet BTOC)
Top of Casing
Elevation
(feet AMSL)
Depth to
Groundwater
(feet BTOC)
Groundwater
Elevation
(feet AMSL)
Monitoring
Well
Diameter
(inches)
9203-MSWLF-1980 MW-2 1994 35.68420 78.84301 Bedrock 60.0 50.0 - 60.0 48.0 - 50.0 366.03 27.02 339.01 2.0
9203-MSWLF-1980 MW-4 1994 35.68161 78.86000 Regolith 36.0 26.0 - 36.0 24.0 - 26.0 310.80 20.60 290.20 2.0
9203-MSWLF-1980 MW-6 1994 35.68380 78.84769 Bedrock 33.5 23.5 - 33.5 21.5 - 23.5 319.71 16.24 303.47 2.0
9203-MSWLF-1980 MW-8 1994 35.68394 78.85367 Regolith 45.7 35.7 - 45.7 33.7 - 35.7 287.72 9.08 278.64 2.0
9203-MSWLF-1980 MW-9 1994 35.68402 78.85362 Bedrock 37.2 27.2 - 37.2 25.2 - 27.2 285.83 6.35 279.48 2.0
9203-MSWLF-1980 MW-10 1994 35.68406 78.85358 Regolith 22.5 12.5 - 22.5 10.5 - 12.5 287.10 6.49 280.61 2.0
9203-MSWLF-1980 MW-11 1994 35.68314 78.85380 Regolith 23.8 13.8 - 23.8 10.8 - 13.8 282.80 4.41 278.39 2.0
9203-MSWLF-1980 MW-12 1994 35.68018 78.84787 Regolith 21.8 11.8 - 21.8 9.8 - 11.8 306.52 7.61 298.91 2.0
9203-MSWLF-1980 MW-13 1994 35.68013 78.84987 Regolith 23.3 13.3 - 23.3 11.3 - 13.3 305.93 12.45 293.48 2.0
9203-MSWLF-1980 MW-14 1994 35.68010 78.84994 Bedrock 39.8 29.8 - 39.8 27.8 - 29.8 305.29 11.84 293.45 2.0
9203-MSWLF-1980 MW-15 1994 35.68012 78.84990 Saprolite 41.0 31.0 - 41.0 29.0 - 31.0 305.64 12.15 293.49 2.0
9203-MSWLF-1980 MW-16 1994 35.68070 78.85300 Regolith 45.0 35.0 - 45.0 33.0 - 35.0 315.30 28.57 286.73 2.0
9203-MSWLF-1980 MW-17 1994 35.68141 78.85434 Regolith 28.5 18.5 - 28.5 16.5 - 18.5 291.58 14.81 276.77 2.0
9203-MSWLF-1980 MW-18 1994 35.68389 78.85087 Regolith 26.5 16.5 - 26.5 14.5 - 16.5 300.82 12.24 288.58 2.0
9203-MSWLF-1980 MW-19 6/10/1999 35.68405 78.85366 Bedrock 68.0 58.0 - 68.0 56.0 - 58.0 286.17 7.52 278.65 2.0
9203-MSWLF-1980 MW-20 6/10/1999 35.68456 78.85302 Regolith 28.5 13.5 - 28.5 11.5 - 13.5 285.80 7.31 278.49 2.0
9203-MSWLF-1980 MW-21 6/10/1999 35.68229 78.86262 Regolith 31.0 16.0 - 31.0 14.0 - 16.0 339.25 5.11 334.14 2.0
9203-MSWLF-1980 MW-22 6/10/1999 35.67984 78.86062 Regolith 28.5 13.5 - 28.5 11.5 - 13.5 299.39 13.92 285.47 2.0
9203-MSWLF-1980 MW-23 6/10/1999 35.68029 78.85884 Regolith 27.7 12.7 - 27.7 10.7 - 12.7 286.83 13.85 272.98 2.0
9203-MSWLF-1980 MW-24 6/10/1999 35.68179 78.85827 Regolith 31.0 16.0 - 31.0 14.0 - 16.0 295.04 9.61 285.43 2.0
9203-MSWLF-1980 MW-25 6/10/1999 35.68267 78.85769 Regolith 30.6 15.6 - 30.6 13.6 - 15.6 295.87 13.02 282.85 2.0
9203-MSWLF-1980 MW-26 6/9/1999 35.67795 78.85668 Regolith 20.0 7.0 - 20.0 5.0 - 7.0 282.95 5.20 277.75 2.0
9203-MSWLF-1980 MW-27 6/9/1999 35.67585 78.85661 Regolith 31.5 16.5 - 31.5 14.5 - 16.5 297.31 17.64 279.67 2.0
9203-MSWLF-1980 MW-28 6/10/1999 35.68378 78.84759 Bedrock 71.0 61.0 - 71.0 59.0 - 61.0 319.70 46.65 273.05 2.0
9203-MSWLF-1980 MW-29 2/21/2011 35.68420 78.85379 Regolith 25.3 15.3 - 25.3 13.3 - 15.3 284.76 5.80 278.96 2.0
Notes:
1. Groundwater elevations were measured on April 26, 2017.
2. AMSL - Above Mean Sea Level
3. BTOC - Below Top of Casing
4. Latitude and longitude are in decimal degrees (World Geodetic System 1983).
Feltonsville Landfill - Wake County
Monitoring Well Construction Summary
Table 1
Permit Number 9203-MSWLF-1980
April 2017 Semi-Annual Sampling Event
Page 1 of 1 June 2017
Table 2
Summary of Calculated Groundwater Flow Velocities
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
Permit Number 9203-MSWLF-1980
MW-2 0.42 0.019 0.13 6.03E-02
MW-6 0.42 0.025 0.05 2.09E-01
MW-8 2.63 0.019 0.13 3.79E-01
MW-9 0.33 0.018 0.05 1.22E-01
MW-10 0.52 0.018 0.13 7.35E-02
MW-11 0.42 0.019 0.13 6.01E-02
MW-12 0.42 0.019 0.25 3.27E-02
MW-13 1.24 0.015 0.05 3.63E-01
MW-14 0.26 0.018 0.05 9.29E-02
MW-15 2.00 0.018 0.18 1.99E-01
MW-16 0.42 0.016 0.05 1.35E-01
MW-17 0.42 0.018 0.13 5.66E-02
MW-18 6.43 0.021 0.08 1.70E+00
MW-19 1.84 0.019 0.13 2.65E-01
Notes:
1. Hydraulic conductivity and effective porosity values are estimated from previously performed slug tests and
grain size analyses.
2. The gradient and linear velocity values shown for MW-2 are based on the average of all the listed wells.
Monitoring Well Code
Hydraulic
Conductivity
(feet/day)
Gradient Effective Porosity Average Linear Velocity
(feet/day)
Page 1 of 1 June 2017
pH Conductivity Temperature Turbidity DO ORP
(S.U.)(mS/cm)(degrees Celsius)(NTUs)(mg/L)(mV)
9203-MSWLF-1980 MW-2 6.91 3,068 16.9 16 6.72 154.9
9203-MSWLF-1980 MW-4 6.81 195 16.7 26 7.81 104.7
9203-MSWLF-1980 MW-6 6.45 1,395 17.1 11 2.66 39.8
9203-MSWLF-1980 MW-8 6.42 335 16.6 3 1.38 -6.7
9203-MSWLF-1980 MW-9 6.62 563 21.4 54 1.38 -17.9
9203-MSWLF-1980 MW-10 5.73 428 15.5 2 1.73 -14.5
9203-MSWLF-1980 MW-11 5.70 263 14.9 24 1.95 50.4
9203-MSWLF-1980 MW-12 6.45 1,307 16.5 8 1.43 1.2
9203-MSWLF-1980 MW-13 5.43 317 15.9 14 1.61 115.4
9203-MSWLF-1980 MW-14 5.95 368 17.3 3 1.55 53.7
9203-MSWLF-1980 MW-15 5.84 562 16.6 59 1.80 70.8
9203-MSWLF-1980 MW-16 5.95 312 19.3 24 1.91 21.1
9203-MSWLF-1980 MW-17 5.44 418 15.7 42 1.84 124.3
9203-MSWLF-1980 MW-18 6.97 1,127 16.9 12 2.08 35.6
9203-MSWLF-1980 MW-19 7.25 245 16.8 3 1.47 1.4
9203-MSWLF-1980 MW-20 7.96 279 16.1 5 2.76 43.8
9203-MSWLF-1980 MW-21 6.23 113 17.2 60 6.67 127.6
9203-MSWLF-1980 MW-22 6.03 501 15.7 71 5.40 41.9
9203-MSWLF-1980 MW-23 6.49 1,749 16.0 19 4.53 -11.6
9203-MSWLF-1980 MW-24 6.30 2,014 16.6 12 7.15 35.2
9203-MSWLF-1980 MW-25 6.40 1,338 15.6 10 3.65 95.1
9203-MSWLF-1980 MW-26 4.71 702 14.7 67 5.80 126.1
9203-MSWLF-1980 MW-27 6.45 763 17.8 71 1.15 -25.8
9203-MSWLF-1980 MW-28 7.05 871 17.5 158 1.46 121.6
9203-MSWLF-1980 MW-29 5.59 74 15.2 170 2.13 5.0
9203-MSWLF-1980 SW-1 7.17 103 21.4 25 6.38 53.9
9203-MSWLF-1980 SW-2 6.41 206 22.2 55 4.37 104.0
9203-MSWLF-1980 SW-3 7.25 109 23.9 52 6.55 75.9
Notes:
1. Water quality measurements were collected from April 26-28, 2017.
2. SW - Surface Water
3. ORP - Oxidation Reduction Potential (mV - millivolt)
4. DO - Dissolved Oxygen (mg/L - milligrams per liter)
5. S.U. - Standard Units
6. NTUs - Nephelometric Turbidity Units
7. mS/cm - Microsiemens per centimeter
8. Turbidity measurements recorded at the time of sample collection.
Surface Water Sample Location
Table 3
Water Quality Parameters
Feltonsville Landfill - Wake County
April 2017 Semi-Annual Sampling Event
Facility Permit
Number
Monitoring
Well Code
Water Quality Measurements
Permit Number 9203-MSWLF-1980
Page 1 of 1 June 2017
Table 4a
Detected Groundwater Constituents - Inorganics
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
Permit Number 9203-MSWLF-1980
Monitoring Well CodeSample DateAntimonyArsenicBariumBerylliumCadmiumChromiumCobaltCopperLeadMercuryNickelSeleniumSilverSodiumThalliumVanadiumZincTotal Dissolved Solids1*10 700 4*2 10 1*1,000 15 1 100 20 20 20,000*0.2*0.3*1,000 500,000
6 10 100 1 1 10 10 10 10 0.2 50 10 10 NE 5.5 25 10 NE
MW-2 31-Mar-11 0.315J 169 10.7 4.55J 6.56JB 25.2 6.35J 9.35J 20.3J 34.9
MW-2 8-Nov-11 522 24.4 6.29J 16.9B 0.215 12.7J 16.0J 36.9
MW-2 4-Apr-12 159 18.3 7.27J
MW-2 6-Nov-12 0.563J 401 2.39J 2.24J 1.97J 2.43J 8.83J
MW-2 15-May-13 80J 0.2J 0.07J 0.5J 4J 34
MW-2 6-Nov-13 210 1.0J 0.2J 2J 0.4J 1J 5JB
MW-2 9-Apr-14 150 0.3J 0.10J 2J 0.2J 0.04J 0.7J 2J 14J 5JB
MW-2 28-Oct-14 2J 360 0.1J 0.2J 2J 0.02J 2J 2J 0.07J 4JB
MW-2 5-May-15 0.7J 190 0.1J 1J 0.04J 1J 3JB
MW-2 19-Nov-15 0.5J 650 2J 1J 4J 6J 0.06J 3J 2J 10
MW-2 26-Apr-16 250 20
MW-2 17-Nov-16 0.40J 370 0.16J 1.5JB 1.8J 1.0J 0.36J 6.4JB 4.2J
MW-2 27-Apr-17 2.1J 160 0.97J 0.28J 2.8J 9.4J 9.6J
MW-4 31-Mar-11 44.8J 1.98J 3.36JB 2.33J 2.10J 6.02J 20.9
MW-4 8-Nov-11 45.6J 2.27J 4.15JB 6.85J 17.8
MW-4 4-Apr-12 0.91J 38.8J 3.84J
MW-4 6-Nov-12 1.10J 57.4J 2.85J 1.62J 2.58J 2.87J 3.48J 7.65J 11.1
MW-4 15-May-13 2J 50J 0.05J 2J 1.0J 2J 2J 2J 5JB
MW-4 6-Nov-13 4J 90J 0.1J 6J 4J 11 4J 9J 12J 27
MW-4 9-Apr-14 2J 40J 1J 0.3J 1.0J 0.5J 0.02J 1.0J 6J 7JB
MW-4 28-Oct-14 2J 70J 0.08J 4JB 2J 4J 3J 5J 0.09J 5J 16B
MW-4 5-May-15 4J 80J 0.1J 0.1J 5J 2J 8J 4J 4J 5J 13B
MW-4 19-Nov-15 2J 40J 0.1J 2J 0.6J 1J 1J 0.11J 2J 6J
MW-4 26-Apr-16 50J 1J 0.4J 1J
MW-4 16-Nov-16 1.7J 48J 0.12J 0.090J 2.8J 0.79J 2.7J 2.0J 2.5J 7.1J 7.6J
MW-4 28-Apr-17 33J 5.6J 3.6J
MW-6 1-Apr-11 277 10.3 4.70J 6.89JB 1.95J 6.29J 1.45J 22.3J 30.6
MW-6 9-Nov-11 225 5.93J 2.17J 14.9J 6.69J
MW-6 4-Apr-12 0.254J 248 6.79J 1.49J 2.52J 2.18J 15.8J 7.07J
MW-6 6-Nov-12 509 6.42J 1.16J 1.91J 2.60J 16.2J 18.4
MW-6 15-May-13 0.6J 280 0.8J 7J 1J 27J 2J 9JB
MW-6 6-Nov-13 450 0.3J 0.2J 2J 1J 0.02J 19J 2J 6JB
MW-6 9-Apr-14 1J 470 0.8J 0.3J 10 2J 0.04J 31J 3J 10J 27B
MW-6 28-Oct-14 0.9J 530 0.4J 6J 2J 0.03J 26J 2J 9JB
MW-6 5-May-15 1J 570 0.5J 0.4J 5J 3J 0.06J 25J 2J 13JB
MW-6 18-Nov-15 0.5J 660 0.2J 2J 3J 4J 0.7J 20J 1J 11
MW-6 dup 18-Nov-15 1J 620 0.06J 0.2J 3J 3J 4J 0.8J 0.03J 20J 1J 12
MW-6 27-Apr-16 0.3J 1J 610 0.07J 0.3J 2JB 3JB 4J 0.8J 21J 1J 13
MW-6 16-Nov-16 0.25J 0.91J 570 0.62J 0.86J 3.9J 25J 1.2J 0.33J 2.7J 5.9J
MW-6 27-Apr-17 620D 0.67J 13 4.3J 19J 1.8J 3.6J 25
MW-8 30-Mar-11 0.749J 68.1J 0.497J 47.4 2.24J 9.89J 3.48J 11.2J 14.3J 14.1
MW-8 7-Nov-11 4.28J 41.3J 32.9 1.49J 2.83JB 1.99J 11.9J
MW-8 4-Apr-12 0.574J 40.4J 31.4 2.35J 3.20J 10.0J
MW-8 4-Jun-12 --------------------------8,290 ------200,000
MW-8 19-Jul-12 --------------------------10,100 ------240,000
MW-8 16-Aug-12 --------------------------8,600 ------170,000
MW-8 6-Nov-12 104 18.7 5.60J 13.2 52.3 10,000 5.13J 5.20J 110,000
MW-8 15-May-13 0.9J 3J 110 0.2J 0.4J 23 6J 115 0.5J 24J 9,520 12B 212,000
MW-8 31-Jul-13 --------------------------9,150 ------248,000
MW-8 6-Nov-13 0.3J 150 6J 2J 6J 24J 7,900 2JB 189,000
MW-8 16-Jan-14 --------------------------8,280 ------212,000
MW-8 10-Apr-14 0.6J 0.5J 130 0.3J 7J 3J 8J 0.2J 0.05J 34J 8,830 8J 14B 212,000
MW-8 29-Oct-14 0.5J 160 0.2J 11 4J 5J 0.3J 53 7,800 10B 181,000
MW-8 7-May-15 3.1J 0.6J 140 0.2J 9J 2J 9J 0.3J 0.02J 29J 7,900 5J 196,000
MW-8 19-Nov-15 1.3J 0.7J 190 0.6J 6J 7J 6J 0.3J 102 1J 15J 4J 178,000
MW-8 26-Apr-16 1J 200 20 10 9J 0.7J 0.03J 67 9,150 5J 196,000
MW-8 16-Nov-16 0.52J 160 6.9J 0.68J 73 6,000 5.8J 180,000
MW-8 28-Apr-17 0.67J 120 3.2J 3.9J 4.6J 0.27J 30J 6,400 14J 3.9J 210,000
North Carolina 2L or
Groundwater Protection
Standard
Solid Waste Section Limit
Page 1 of 24 June 2017
Table 4a
Detected Groundwater Constituents - Inorganics
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
Permit Number 9203-MSWLF-1980
Monitoring Well CodeSample DateAntimonyArsenicBariumBerylliumCadmiumChromiumCobaltCopperLeadMercuryNickelSeleniumSilverSodiumThalliumVanadiumZincTotal Dissolved Solids1*10 700 4*2 10 1*1,000 15 1 100 20 20 20,000*0.2*0.3*1,000 500,000
6 10 100 1 1 10 10 10 10 0.2 50 10 10 NE 5.5 25 10 NE
North Carolina 2L or
Groundwater Protection
Standard
Solid Waste Section Limit
MW-9 30-Mar-11 176 0.204J 8.41J 3.19J 9.17JB 3.09J 10.3J 5.39J 14.4
MW-9 7-Nov-11 147 0.136J 3.18J 1.28J 2.82JB 3.16J 35.9
MW-9 4-Apr-12 191 0.355J 10.1 3.92J 12 2.58J 11.6J 7.48J 20.2
MW-9 dup 4-Apr-12 180 0.293J 8.31J 3.38J 9.98J 10.2J 6.06J 31.1
MW-9 4-Jun-12 --------------------------11,400 ------280,000
MW-9 19-Jul-12 --------------------------38,600 ------1,100,000
MW-9 16-Aug-12 --------------------------28,500 ------650,000
MW-9 6-Nov-12 0.446J 2,110 0.546J 16.2 23.8 125 8.16J 144 4.15J 45,100 17.4J 36 970,000
MW-9 15-May-13 6J 1,320 0.2J 5J 25 57 4J 0.08J 65 2J 30,100 4J 15B 473,000
MW-9 dup 15-May-13 0.2J 7J 1,260 0.2J 3J 24 57 4J 0.07J 63 2J --2J 12B --
MW-9 31-Jul-13 --------------------------30,800 ------463,000
MW-9 6-Nov-13 8J 1,200 0.4J 0.1J 7J 21 65 7J 0.08J 47J 3J 23,600 0.1J 19J 27 431,000
MW-9 16-Jan-14 --------------------------21,800 ------427,000
MW-9 10-Apr-14 8J 1,060 0.1J 0.1J 1J 19 39 4J 0.07J 31J 2J 21,300 10J 11B 417,000
MW-9 dup 10-Apr-14 0.3J 10 1,050 0.1J 0.3J 1J 19 50 4J 0.06J 32J 2J --12J 17B --
MW-9 29-Oct-14 6J 820 0.1J 0.2J 2JB 14 29 5J 0.1J 32J 21,300 13B 375,000
MW-9 dup 29-Oct-14 6J 820 0.1J 0.2J 1JB 14 30 5J 0.04J 32J --10B --
MW-9 7-May-15 7J 1,000 0.3J 4J 16 29 8J 0.04J 33J 19,800 4J 15 389,000
MW-9 20-Nov-15 6J 810 0.06J 0.8J 12 18 7J 0.10J 25J 2J 3J 383,000
MW-9 27-Apr-16 6J 930 0.1J 0.4JB 13 11 6J 24J 1J 21,200 4J 403,000
MW-9 16-Nov-16 6.8J 1,100 0.061J 0.93J 14 10 7.4J 0.036J 28J 19,000 2.8J 4.0J 370,000
MW-9 27-Apr-17 5.1J 950D 0.18J 1.4J 12 14 8.3J 0.041J 32J 21,000 3.3J 5.5J 420,000
MW-10 30-Mar-11 14.4 534 6.73J 51.6 2.63JB 2.93J 41.6J 2.01J
MW-10 7-Nov-11 8.75J 476 0.141J 4.52J 11.4 1.64J 3.72JB 18.7J 3.30J 9.39J
MW-10 4-Apr-12 10.2 596 4.97J 58.8 47.4J
MW-10 4-Jun-12 --------------------------58,100 ------630,000
MW-10 19-Jul-12 --------------------------1,680,000 ------11,000,000
MW-10 16-Aug-12 --------------------------1,900,000 ------11,000,000
MW-10 6-Nov-12 34.2 2,050 2.94 67.6 42.5 152 34.7 0.349 107 7.64J 595,000 111 195 2,800,000
MW-10 dup 6-Nov-12 28.5 2,060 3.31 76.1 46.1 190 42.8 0.306 113 8.23J --127 231 --
MW-10 15-May-13 32 1,140 2.9 41 46 154 28 0.19J 77 2J 253,000 0.3J 84 269 1,100,000
MW-10 31-Jul-13 --------------------------121,000 ------680,000
MW-10 6-Nov-13 21 880 0.8J 0.1J 10 31 45 8J 0.06J 39J 3J 128,000 0.08J 31 55 794,000
MW-10 dup 6-Nov-13 22 1,040 1.6 0.4J 20 37 75 16 0.10J 50J 4J --0.1J 57 114 --
MW-10 16-Jan-14 --------------------------69,600 ------460,000
MW-10 10-Apr-14 16 310 0.08J 1J 14 2J 0.4J 0.07J 14J 50,400 7J 7JB 393,000
MW-10 26-Oct-14 13 720 0.2J 3J 21 12 3J 0.1J 23J 2J 86,300 24 670,000
MW-10 7-May-15 23 700 0.1J 2J 29 3J 0.6J 0.02J 36J 3J 77,800 6J 756,000
MW-10 20-Nov-15 25 730 0.1J 3J 21 7J 0.9J 0.05J 32J 3J 6J 680,000
MW-10 27-Apr-16 0.3J 34 850 0.1J 0.5JB 24 2J 0.2J 30J 2J 93,400 2J 832,000
MW-10 16-Nov-16 20 830 1.2J 17 1.2J 25J 65,000 1.6J 1.9J 760,000
MW-10 27-Apr-17 23 350 0.14J 11 3.5J 0.40J 13J 40,000 2.1J 2.8J 350,000
MW-11 31-Mar-11 75.5J 9.29J
MW-11 8-Nov-11 83.8J 1.08J 1.64J 14.7
MW-11 4-Apr-12 84.3J
MW-11 6-Nov-12 93.2J 2.52J 1.55J 13.2
MW-11 15-May-13 0.6J 70J 0.5J 2J 0.8J 2J 3JB
MW-11 6-Nov-13 0.8J 70J 1J 0.9J 2J 4JB
MW-11 10-Apr-14 1J 70J 0.7J 0.5J 1J 0.3J 0.04J 2J 6J 8JB
MW-11 29-Oct-14 0.6J 70J 0.4JB 0.9J 1J 0.2J 2J 5J
MW-11 6-May-15 2J 110 0.05J 1J 8J 2J 0.5J 0.02J 4J 7JB
MW-11 20-Nov-15 1J 70J 0.05J 0.2J 0.5J 5J 2J 0.2J 3J 1J 13
MW-11 27-Apr-16 1J 110 9J 0.8J 3J 4J
MW-11 16-Nov-16 0.60J 91J 2.4J 0.77J 2.6J 1.4J 3.5J
MW-11 28-Apr-17 96J 3.9J 1.5J 2.3J 9.8J
Page 2 of 24 June 2017
Table 4a
Detected Groundwater Constituents - Inorganics
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
Permit Number 9203-MSWLF-1980
Monitoring Well CodeSample DateAntimonyArsenicBariumBerylliumCadmiumChromiumCobaltCopperLeadMercuryNickelSeleniumSilverSodiumThalliumVanadiumZincTotal Dissolved Solids1*10 700 4*2 10 1*1,000 15 1 100 20 20 20,000*0.2*0.3*1,000 500,000
6 10 100 1 1 10 10 10 10 0.2 50 10 10 NE 5.5 25 10 NE
North Carolina 2L or
Groundwater Protection
Standard
Solid Waste Section Limit
MW-12 31-Mar-11 276 1.66JB 2.46J 9.68J 1.42J 10.1
MW-12 8-Nov-11 3.93J 115 3.02JB 6.15J
MW-12 3-Apr-12 182 1.28J
MW-12 5-Nov-12 123
MW-12 15-May-13 2J 170 0.9J 0.1J 0.3J 2J
MW-12 6-Nov-13 4J 140 0.5J 0.2J 2J 1J
MW-12 10-Apr-14 2J 230 0.9J 0.2J 0.6J 0.04J 2J 5J 4JB
MW-12 28-Oct-14 2J 130 0.9JB 0.1J 0.5J 1J 2JB
MW-12 6-May-15 2J 290 0.4J 0.1J 0.5J 0.05J 3J 3JB
MW-12 20-Nov-15 6J 200 0.3J 0.6J 1J 2J
MW-12 27-Apr-16 5J 330 0.08J 3J 1J 4J 1J 5J 1J 6J
MW-12 17-Nov-16 5.1J 140 0.67JB 1.4J
MW-12 27-Apr-17 3.9J 260 0.82J 0.049J 4.2J 5.9J
MW-12 (dup)27-Apr-17 3.9J 250 3.9J 3.9J
MW-13 31-Mar-11 576 2.30J 11.3 3.33JB 0.273 44.9J 3.48J 60.9
MW-13 8-Nov-11 4.70J 906 0.130J 1.21 3.08J 16.8 5.29J 53.2 7.77J 243
MW-13 3-Apr-12 4.41J 960 2.48J 17.0 4.64J 0.384 53.4 88.1
MW-13 5-Nov-12 757 0.633J 1.13J 10.4 8.36J 0.487 46.2J 4.12J 234
MW-13 16-May-13 2J 550 0.1J 0.6J 0.5J 9J 13 0.4J 0.35 36J 103
MW-13 7-Nov-13 0.9J 480 0.08J 0.2J 7J 4JB 0.15J 33J 36
MW-13 10-Apr-14 2J 590 0.1J 0.6J 0.3J 10.0 18 0.79 35J 6J 144
MW-13 28-Oct-14 2J 460 0.1J 1.7 6J 13 0.2J 0.21 30J 0.06J 265
MW-13 6-May-15 2J 610 0.1J 0.8J 0.2J 10 17 0.39 39J 98
MW-13 20-Nov-15 1J 500 0.1J 0.3J 0.3J 8J 13 0.50 32J 3J 48
MW-13 27-Apr-16 3J 620 0.1J 0.2J 0.3JB 9J 13 0.6J 0.51 35J 58
MW-13 17-Nov-16 1.2J 500 0.18J 6.4J 4.7JB 0.20J 0.36 31J 0.17J 2.0J 41
MW-13 28-Apr-17 2.6J 380 0.16J 5.7J 5.5J 0.36 24J 4.8J 3.2J 38
MW-14 30-Mar-11 0.982J 36.3J 0.504J 2.89J 3.31JB 7.52J 13.0
MW-14 7-Nov-11 0.528J 5.60J 26.6J 2.00 1.91J 5.77J 5.42J
MW-14 3-Apr-12 0.446J 178 2.38J 3.65J 8.28J 3.09J
MW-14 5-Nov-12 0.299J 60.0J 3.59J 2.09J
MW-14 16-May-13 1.5J 0.7J 70J 1.8 1J 1J 5J 0.02J 5J 5J
MW-14 7-Nov-13 1.0J 0.6J 100J 2J 0.6J 0.9JB 5J 8J 7JB
MW-14 10-Apr-14 1.9J 0.9J 90J 0.8J 1J 2J 5J 0.2J 0.09J 9J 15J 56.0
MW-14 28-Oct-14 0.3J 140 0.1J 0.4JB 0.5J 1J 5J 2JB
MW-14 6-May-15 0.7J 0.8J 140 0.1J 1J 1J 7J 0.18J 10J 6JB
MW-14 dup 6-May-15 1.4J 90 0.2J 1JB 1J 12 0.08J 6J 6J
MW-14 20-Nov-15 0.9J 150 0.7J 0.7J 4J 0.08J 5J 1J 4J
MW-14 27-Apr-16 0.4J 0.5J 240 3JB 2J 1J 0.12J 18J
MW-14 17-Nov-16 0.72J 0.93J 210 0.17J 2.7J 0.76J 2.6JB 0.17J 0.80 16J 0.20J 4.1J 3.6J
MW-14 28-Apr-17 1.1J 120 5.5J 0.43 4.6J 1.6J 5.5J 5.0J
MW-15 31-Mar-11 0.444J 118 1.11 2.91J 1.21J 8.29JB 2.42J 0.190J 23.9J 0.848J 4.56J 5.65J
MW-15 8-Nov-11 118 0.700J 1.09J 16.5J 2.31J
MW-15 5-Apr-12 1.01J 117 5.95J 18.7J
MW-15 7-Nov-12 1.20J 133 18.3J 5.03J
MW-15 16-May-13 1.3J 140 0.5J 1J 1J 14 0.3J 0.07J 21J
MW-15 7-Nov-13 220 0.05J 0.1J 2J 4J 5JB 0.11J 34J
MW-15 8-Apr-14 0.8J 160 1 0.5J 1J 4J 0.3J 0.08J 23J 2J 6J 7JB
MW-15 27-Oct-14 1.6J 180 0.4J 0.2JB 2J 2J 0.2J 25J 4JB
MW-15 5-May-15 1.0J 0.8J 210 0.4J 0.8J 4J 17 0.2J 0.08J 28J 5JB
MW-15 18-Nov-15 0.4J 180 0.7J 0.3J 2J 2J 0.3J 0.03J 27J 1J 5J
MW-15 27-Apr-16 280 0.07J 0.2J 5J 4J 7J 0.8J 0.21 32J 6J
MW-15 17-Nov-16 0.80J 0.36J 190 0.49J 2.0J 0.71J 3.9JB 0.21J 0.11J 30J 0.33J 1.8J 7.0J
MW-15 28-Apr-17 190 0.27J 5.5J 0.12J 23J 3.9J 2.7J 5.6J
Page 3 of 24 June 2017
Table 4a
Detected Groundwater Constituents - Inorganics
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
Permit Number 9203-MSWLF-1980
Monitoring Well CodeSample DateAntimonyArsenicBariumBerylliumCadmiumChromiumCobaltCopperLeadMercuryNickelSeleniumSilverSodiumThalliumVanadiumZincTotal Dissolved Solids1*10 700 4*2 10 1*1,000 15 1 100 20 20 20,000*0.2*0.3*1,000 500,000
6 10 100 1 1 10 10 10 10 0.2 50 10 10 NE 5.5 25 10 NE
North Carolina 2L or
Groundwater Protection
Standard
Solid Waste Section Limit
MW-16 1-Apr-11 10.8 451 4.40J 5.91J 2.72JB 10.3J 1.72J 6.35J
MW-16 9-Nov-11 18.9 348 0.123J 6.12J 5.69J 4.97J 5.31J 7.05J 13.8
MW-16 5-Apr-12 0.267J 14.6 433 4.11J 5.20J 9.34J 2.68J
MW-16 7-Nov-12 1.71J 11.1 436 2.64J 6.13J 3.98J 7.56J 5.46J
MW-16 14-May-13 14 350 1J 6J 3J 0.8J 9J 3JB
MW-16 5-Nov-13 16 260 1J 5J 1J 0.3J 4J 2J 7JB
MW-16 8-Apr-14 13 300 0.3J 5J 1J 0.3J 0.02J 7J 2J 5J 6JB
MW-16 27-Oct-14 10J 330 0.1J 0.2JB 5J 1J 0.4J 7J 5JB
MW-16 5-May-15 13 280 1J 5J 3J 0.7J 0.03J 7J 2J 5JB
MW-16 3-Nov-15 12 300 0.4J 5J 1JB 0.4J 7J 4J
MW-16 27-Apr-16 12 330 0.7J 4J 0.5J 8J 1J 4J
MW-16 16-Nov-16 14 280 0.34J 0.73J 4.4J 1.5J 0.73J 6.5J 0.20J 1.8J 6.5J
MW-16 27-Apr-17 13 230 2.0J 1.0J 0.28J 3.9J 3.1J
MW-17 1-Apr-11 12.0 111 2.02J 2.72J 4.04JB 5.52J 2.44J 3.16J 8.97J
MW-17 9-Nov-11 13.3 190 0.183J 8.34J 5.52J 6.55J 7.49J 8.80J 10.6J 27.5
MW-17 5-Apr-12 5.59J 105 1.70J 2.00J 3.22J 5.18J 2.42J
MW-17 7-Nov-12 0.226J 3.57J 156 1.93J 2.15J 1.78J 3.23J 4.98J 3.12J 7.49J
MW-17 14-May-13 10J 120 0.08J 0.1J 2J 2J 3J 2J 5J 6JB
MW-17 6-Nov-13 12 120 0.9J 1J 2J 0.6J 3J 5J 22
MW-17 10-Apr-14 8J 70J 0.3J 1J 1J 2J 0.7J 0.04J 3J 5J 9JB
MW-17 28-Oct-14 8J 140 0.04J 2JB 3J 3J 2J 0.02J 6J 11
MW-17 5-May-15 11 140 0.2J 0.1J 5J 6J 7J 3J 9J 3J 24
MW-17 19-Nov-15 14 150 0.09J 0.1J 2J 7J 3J 2J 10J 1J 10J
MW-17 26-Apr-16 11 110 0.2J 2J 4J 3J 1J 7J 9J
MW-17 17-Nov-16 0.22J 12 120 0.21J 2.3J 1.8JB 0.30J 6.3J 0.20J 3.7J 3.5J
MW-17 28-Apr-17 8.9J 100 1.5J 0.50J 2.9J 2.1J 2.8J 5.7J
MW-18 31-Mar-11 89.9J 1.90J 1.44J 2.78JB 9.44J 4.60J 2.44J 8.98J
MW-18 8-Nov-11 104 1.33J 1.30J 2.53JB 8.05J 2.09J 8.83J
MW-18 4-Apr-12 89.5J 1.44J 9.94J
MW-18 6-Nov-12 104 12.1J 5.80J
MW-18 15-May-13 2J 90J 0.3J 1J 1J 0.3J 13J
MW-18 6-Nov-13 4J 120 0.2J 4J 4J 6J 2J 0.02J 18J 2J 6J 24
MW-18 10-Apr-14 2J 80J 0.5J 1J 2J 0.03J 15J 7J 6JB
MW-18 28-Oct-14 2J 80J 1J 1J 14J 3J
MW-18 5-May-15 2J 90J 0.3J 1J 2J 15J 4JB
MW-18 19-Nov-15 2J 90J 0.4J 1J 1J 16J 1J 4J
MW-18 26-Apr-16 1J 90J 0.4J 1J 2J 15J 4J
MW-18 16-Nov-16 2.3J 100 0.11J 0.93J 2.2J 0.47J 16J 1.2J 2.3J 7.1J
MW-18 27-Apr-17 3.2J 110 0.14J 3.2J 2.3J 5.6J 1.9J 0.034J 23J 3.7J 6.9J 16
MW-19 1-Apr-11 0.816J 127 0.492J 2.60J 5.65JB 3.62J 1.45J 4.26J 7.49J
MW-19 9-Nov-11 0.701J 4.52J 169 0.431J 1.95J 2.11J 0.166J 6.52J 5.22J
MW-19 5-Apr-12 2.30J 125 2.08J 6.00J 3.03J 2.78J 6.08J
MW-19 4-Jun-12 --------------------------44,700 ------230,000
MW-19 19-Jul-12 --------------------------40,300 ------240,000
MW-19 16-Aug-12 --------------------------42,500 ------110,000
MW-19 7-Nov-12 1.88J 181 0.749J 4.97J 3.09J 6.14J 34,800 8.19J 21.2 130,000
MW-19 16-May-13 1.5J 1J 180 1 2J 2J 21 0.4J 5J 37,100 2J 5J 220,000
MW-19 31-Jul-13 --------------------------40,500 ------242,000
MW-19 7-Nov-13 2J 170 0.5J 0.1J 1JB 1J 36,800 4J 4JB 222,000
MW-19 16-Jan-14 --------------------------40,900 ------232,000
MW-19 9-Apr-14 1.0J 3J 150 0.4J 2J 10J 7J 0.4J 0.04J 12J 10,200 6J 10B 154,000
MW-19 29-Oct-14 4.1J 2J 150 0.9J 2JB 8J 4J 0.3J 10J 14,900 9JB 170,000
MW-19 7-May-15 3.2J 2J 220 0.09J 0.2J 3J 18 14 0.3J 0.03J 25J 7,900 2J 27 150,000
MW-19 20-Nov-15 1.3J 2J 150 0.08J 0.3J 3J 5J 5J 0.4J 10J 1J 3J 8J 134,000
MW-19 26-Apr-16 0.3J 1J 160 0.06J 2J 5J 19 0.2J 15J 7,900 8J 120,000
MW-19 (dup)26-Apr-16 0.4J 1J 160 0.07J 0.1J 2J 5J 20 0.2J 15J 8J
MW-19 16-Nov-16 0.58J 2.1J 180 0.13J 3.0J 11 6.0J 0.47J 16J 7,600 4.8J 7.2J 160,000
MW-19 27-Apr-17 170 1.6J 2.5J 6.0J 0.34J 0.048J 9.5J 18,000 4.7J 6.2J 170,000
Page 4 of 24 June 2017
Table 4a
Detected Groundwater Constituents - Inorganics
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
Permit Number 9203-MSWLF-1980
Monitoring Well CodeSample DateAntimonyArsenicBariumBerylliumCadmiumChromiumCobaltCopperLeadMercuryNickelSeleniumSilverSodiumThalliumVanadiumZincTotal Dissolved Solids1*10 700 4*2 10 1*1,000 15 1 100 20 20 20,000*0.2*0.3*1,000 500,000
6 10 100 1 1 10 10 10 10 0.2 50 10 10 NE 5.5 25 10 NE
North Carolina 2L or
Groundwater Protection
Standard
Solid Waste Section Limit
MW-20 1-Apr-11 4.27J 270 0.244J 19.8 11.1 18.6B 12.9 21.4J 1.53J 25.5 60.3
MW-20 9-Nov-11 6.55J 290 0.371J 24.2 14.1 16.6 14.4 23.1J 29.5 78.5
MW-20 5-Apr-12 0.722J 4.37J 162 4.66J 1.57J 4.30J 2.52J 4.25J 6.28J 9.31J
MW-20 7-Nov-12 218 12.6 3.41J 5.42J 5.18J 9.29J 11.5J 24.7
MW-20 14-May-13 0.3J 3J 190 0.1J 11 3J 14 3J 9J 5J 19B
MW-20 5-Nov-13 0.3J 4J 240 0.2J 0.1J 10 7J 11 5J 13J 0.08J 18J 47
MW-20 9-Apr-14 0.5J 2J 160 0.3J 3J 2J 568 2J 0.03J 5J 14J 51
MW-20 28-Oct-14 6J 450 0.3J 0.2J 7J 6J 46 3J 0.09J 10J 45 137
MW-20 5-May-15 0.6J 4J 220 0.2J 7J 5J 14 3J 9J 11J 38
MW-20 19-Nov-15 0.4J 3J 210 0.1J 6J 4J 9J 3J 8J 8J 26
MW-20 27-Apr-16 0.2J 4J 240 0.2J 7J 5J 8J 4J 9J 1J 28
MW-20 17-Nov-16 0.25J 3.7J 290 0.52J 0.18J 12 8.4J 19B 7.5J 18J 0.20J 21J 56
MW-20 27-Apr-17 2.0J 110 0.82J 1.6J 3.9J
MW-21 31-Mar-11 5.64J 68.2J 3.98J 2.59J 7.16JB 3.89J 5.66J 8.91J 21.6
MW-21 8-Nov-11 16.1 135 0.295J 12.7 7.88J 13.1 11.8B 13.2J 22.4J 48.7
MW-21 4-Apr-12 6.23J 58.1J 1.85J 2.48J 4.35J 3.08J 3.78J 6.78J 11.7
MW-21 6-Nov-12 3.19J 76.4J 3.52J 2.14J 4.73J 4.37J 3.13J 9.45J 18.3
MW-21 15-May-13 4J 70J 0.08J 2J 2J 4J 2J 3J 5J 9JB
MW-21 6-Nov-13 2J 60J 0.06J 2J 1J 3JB 1J 2J 6J 7JB
MW-21 9-Apr-14 6J 220 0.2J 7J 5J 11 5J 0.04J 10J 37 89
MW-21 28-Oct-14 3J 60J 0.04J 2JB 1J 3J 2J 2J 4J 7J
MW-21 5-May-15 5J 100 0.2J 6J 3J 8J 4J 7J 13J 25
MW-21 19-Nov-15 2J 40J 0.05J 0.2J 1J 1J 3J 1J 2J 3J 7J
MW-21 26-Apr-16 2J 60J 0.05J 1J 1J 2J 1J 2J 6J
MW-21 16-Nov-16 2.3J 56J 0.073J 2.7J 2.1J 5.0J 2.4J 4.3J 6.3J 13
MW-21 28-Apr-17 8.3J 0.81J 3.2J
MW-22 31-Mar-11 192 4.64J 3.08J 7.81J 4.27J 6.41J 3.75J 7.30J 21.7
MW-22 8-Nov-11 4.30J 173 1.44J 2.21JB 1.82J 14.6
MW-22 4-Apr-12 4.66J 159 2.17J 3.18J 2.41J 2.38J 2.79J 3.14J 8.59J
MW-22 6-Nov-12 4.70J 184 2.41J 1.47J 7.72J
MW-22 15-May-13 3J 200 0.1J 0.7J 4J 4J 7J 2J 0.04J 7J 19B
MW-22 6-Nov-13 3J 160 0.2J 0.9J 3J 3JB 0.3J 0.06J 3J 4JB
MW-22 9-Apr-14 2J 240 0.2J 1J 2J 3J 0.6J 0.05J 4J 8J 9JB
MW-22 28-Oct-14 3J 250 0.1J 0.5J 4JB 7J 7J 2J 0.11J 7J 3J 36
MW-22 5-May-15 4J 240 0.05J 1J 6J 3J 0.6J 0.06J 5J 7JB
MW-22 19-Nov-15 4J 240 0.09J 2J 7J 5J 1J 0.03J 6J 1J 11
MW-22 26-Apr-16 5J 240 0.8J 5J 2J 0.8J 0.03J 5J 9J
MW-22 16-Nov-16 6.3J 250 0.084J 4.6J 1.1J 0.24J 3.4J 1.5J 5.2J
MW-22 (dup)16-Nov-16 6.3J 250 0.058J 4.6J 1.2J 0.26J 3.5J 1.8J 4.8J
MW-22 28-Apr-17 5.6J 240 4.3J 1.9J 0.54J 1.6J 5.1J 4.1J 4.9J
MW-23 31-Mar-11 159 1.06J 1.82J 2.33J 41.7
MW-23 8-Nov-11 4.39J 203 1.68J 3.78JB 3.38J
MW-23 4-Apr-12 201 1.03J 2.76J 7.63J
MW-23 5-Nov-12
MW-23 15-May-13
MW-23 5-Nov-13
MW-23 8-Apr-14
MW-23 27-Oct-14
MW-23 5-May-15 2J 270 0.3J 0.3J 0.9J 0.02J 2J 4JB
MW-23 19-Nov-15 10 830 0.06J 3J 7J 5J 2J 9J 1J 20
MW-23 26-Apr-16 260 1J 0.05J 12
MW-23 16-Nov-16 0.43J 3.2J 310 0.27J 6.7J 0.98J 6.0J 0.21J 3.5J 4.2J
MW-23 28-Apr-17 2.3J 210 2.4J 0.78J 0.041J 7.8J 6.3J 15
No Samples Collected - Well was Dry
Page 5 of 24 June 2017
Table 4a
Detected Groundwater Constituents - Inorganics
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
Permit Number 9203-MSWLF-1980
Monitoring Well CodeSample DateAntimonyArsenicBariumBerylliumCadmiumChromiumCobaltCopperLeadMercuryNickelSeleniumSilverSodiumThalliumVanadiumZincTotal Dissolved Solids1*10 700 4*2 10 1*1,000 15 1 100 20 20 20,000*0.2*0.3*1,000 500,000
6 10 100 1 1 10 10 10 10 0.2 50 10 10 NE 5.5 25 10 NE
North Carolina 2L or
Groundwater Protection
Standard
Solid Waste Section Limit
MW-24 1-Apr-11 35.1 653 0.918J 43.6 35.3 56B 38.8 0.916 66.1 9.82J 70.9 175
MW-24 dup 1-Apr-11 49.8 743 1.29 60.9 46.9 77.8B 54.9 0.649 86.7 10.1 99.0 251
MW-24 9-Nov-11 20.1 402 0.101J 8.94J 12.6 1.67J 7.00J 0.237 24.4J 8.52J 23.8
MW-24 5-Apr-12 0.297J 27.2 599 0.439J 16.8 19.5 19.9 11.2 0.708 34.3J 2.77J 31.7 64.3
MW-24 7-Nov-12 15.2 415 7.43J 11.7 3.44J 3.75J 0.192J 24.7J 2.24J 9.92J 26.2
MW-24 16-May-13 15 570 0.6J 0.3J 21 24 41 15 0.17J 45J 0.10J 43 132
MW-24 6-Nov-13 15 360 0.1J 3J 12 4JB 2J 0.04J 26J 2J 14B
MW-24 8-Apr-14 9J 550 0.6J 0.4J 25 23 31 18 0.26 46J 0.05J 86 219
MW-24 27-Oct-14 11 410 0.2J 8J 14 9J 5J 0.12J 30J 49
MW-24 5-May-15 4J 160 0.7J 4J 1J 0.2J 11J 11JB
MW-24 19-Nov-15 6J 200 0.05J 0.4J 1J 5J 3J 0.9J 0.02J 15J 1J 9J
MW-24 25-Apr-16 7J 140 3J 2J 4J 1J 10J 18
MW-24 15-Nov-16 0.37J 7.8JD 370 0.81J 0.54JD 20D 19D 36 21 0.20 0.40J 0.084J 34 96
MW-24 27-Apr-17 17 330 6.5J 0.84J 0.26J 25J 7.3J 2.0J 3.7J
MW-25 31-Mar-11 0.857J 836 1.17J 4.62J 8.85J 2.51J 9.05J
MW-25 8-Nov-11 3.59J 903 3.49J 1.33J 2.62JB 6.03J 8.20J 18.3
MW-25 4-Apr-12 894 1.20J 4.53J 1.92J
MW-25 6-Nov-12 963 4.55J 5.23J 5.51J
MW-25 15-May-13 2J 900 0.2J 0.4J 0.8J 1J 0.3J 8J
MW-25 6-Nov-13 2J 820 0.4J 0.7J 1JB 8J 2J
MW-25 9-Apr-14 2J 830 0.4J 0.7J 1J 2J 0.3J 8J 3J 11J 9JB
MW-25 28-Oct-14 2J 780 0.4J 0.6J 0.7J 8J 2J 3J
MW-25 5-May-15 2J 820 0.3J 0.7J 1J 0.04J 8J 3JB
MW-25 19-Nov-15 1J 890 0.4J 0.8J 2J 9J 1J 4J
MW-25 26-Apr-16 830 0.7J 8J
MW-25 16-Nov-16 1.6J 860 0.39J 1.2J 7.8J 1.2J 0.32J 2.0J 3.9J
MW-25 27-Apr-17 2.0J 890D 1.3J 13J 4.8J 1.7J 5.5J
MW-26 31-Mar-11 161 1.31 0.522J 6.42J 31.1 9.24JB 6.33J 19.9J 4.19J 9.00J 70.1
MW-26 8-Nov-11 3.21J 230 1.66 1.75J 34.0 3.04JB 16.3J 2.58J 52.5
MW-26 4-Apr-12 364 2.12 1.78 60.2 4.53J 23.5J 30.4
MW-26 6-Nov-12 357 1.98 47.9 1.85J 21.2J 46.9
MW-26 15-May-13 0.5J 340 1.9 0.4J 0.4J 55 2J 0.3J 21J 25
MW-26 6-Nov-13 5J 400 1.8 0.4J 16 40 17 10J 0.04J 31J 0.07J 29 72
MW-26 9-Apr-14 330 1.6 0.4J 0.6J 56 2J 0.3J 0.03J 20J 5J 30B
MW-26 28-Oct-14 1J 350 1.8 0.3J 0.4JB 50 2J 0.3J 0.04J 19J 25
MW-26 5-May-15 1J 300 1.6 0.3J 2J 47 3J 0.5J 0.05J 18J 2J 26
MW-26 19-Nov-15 0.6J 180 1.4 0.3J 1J 32 4J 0.7J 0.04J 13J 1J 27
MW-26 26-Apr-16 180 1.1 2J 29 2J 0.9J 0.03J 10J 36
MW-26 16-Nov-16 0.57J 170 1.2 0.21J 1.3J 25 2.9J 0.81J 0.046J 9.7J 0.96J 2.0J 16
MW-26 28-Apr-17 1.5J 81J 0.66J 0.13J 14 2.3J 1.4J 0.028J 6.9J 5.0J 3.3J 17
MW-27 31-Mar-11 97.1J 0.63J 1.76J 1.15J 4.12JB 1.92J 0.33 1.97J 0.938J 3.51J 14.6
MW-27 8-Nov-11 9.70J 128 0.159J 6.51J 4.23J 5.94J 7.64JB 0.286 7.06J 9.22J 27.7
MW-27 4-Apr-12 4.27J 110 2.36J 1.46J 5.25J
MW-27 6-Nov-12 139 1.21J 1.47J 1.71J 1.98J 2.02J 13.3J 8.97J
MW-27 15-May-13 2J 110 1J 0.4J 1J
MW-27 6-Nov-13 4J 150 0.1J 4J 4J 8J 3J 0.09J 8J 19J 25
MW-27 9-Apr-14 3J 120 0.2J 2J 2J 0.6J 0.12J 2J 7J 8JB
MW-27 28-Oct-14 2J 140 0.7J 0.3J 1J 2J 2J
MW-27 5-May-15 8J 150 3J 0.4J 0.05J 2J 3JB
MW-27 19-Nov-15 3J 130 1J 0.4J 1J 1J 4J
MW-27 26-Apr-16 18 160 11 0.02J 4J 10
MW-27 16-Nov-16 0.23J 2.4J 120 0.049J 0.38J 1.8J 0.48J 0.040J 1.6J 15J 4.1J
MW-27 28-Apr-17 0.53J 2.1J 120 1.9J 0.78J 0.054J 1.5J 21J 5.5J
Page 6 of 24 June 2017
Table 4a
Detected Groundwater Constituents - Inorganics
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
Permit Number 9203-MSWLF-1980
Monitoring Well CodeSample DateAntimonyArsenicBariumBerylliumCadmiumChromiumCobaltCopperLeadMercuryNickelSeleniumSilverSodiumThalliumVanadiumZincTotal Dissolved Solids1*10 700 4*2 10 1*1,000 15 1 100 20 20 20,000*0.2*0.3*1,000 500,000
6 10 100 1 1 10 10 10 10 0.2 50 10 10 NE 5.5 25 10 NE
North Carolina 2L or
Groundwater Protection
Standard
Solid Waste Section Limit
MW-28 1-Apr-11 189 10.1 6.31J 11.2B 4.68J 9.03J 1.64J 25.8 47.0
MW-28 9-Nov-11 18.8 464 0.791J 47.1 25.5 30.3 14.2 34.0J 85.6 180
MW-28 5-Apr-12 2.96J 233 14.0 7.61J 12.6 5.46J 11.2J 30.2 51.4
MW-28 6-Nov-12 24.4 620 0.359J 21.7 11.0 19.7 9.09J 17.0J 2.19J 62.3 90.4
MW-28 15-May-13 13 1040 1.7 0.5J 67 52 65 32 0.04J 67 0.3J 291 683
MW-28 6-Nov-13 5J 300 0.4J 0.2J 15 12 16 6J 15J 2J 53 94
MW-28 9-Apr-14 1J 160 0.3J 2J 1J 144 0.6J 0.04J 3J 14J 31
MW-28 28-Oct-14 0.8J 150 3JB 1J 9J 0.5J 3J 6J 10
MW-28 5-May-15 1J 270 0.8J 0.5J 1J 2J 3JB
MW-28 19-Nov-15 2J 190 0.1J 6J 3J 12 1J 5J 1J 13J 21
MW-28 26-Apr-16 5J 300 0.4J
MW-28 16-Nov-16 0.38J 0.58J 180 0.081J 0.97J 1.7J 1.6J 5.3J 2.8J
MW-28 27-Apr-17 2.4J 230 0.36J 12 5.9J 11 3.6J 11J 24J 43
MW-29 1-Apr-11 193 4.92J 8.59J 7.77JB 2.27J 10.5J 1.16J 1.92J 13.1
MW-29 9-Nov-11 142 0.173J 2.53J 2.63J 2.50J 3.42J 2.96J 8.54J
MW-29 dup 9-Nov-11 154 0.233J 4.47J 3.01J 3.09J 3.35J 4.95J 3.95J 16.5
MW-29 5-Apr-12 827 4.23 42.2 28.1 116 27.5 57.2 0.245J 28.7 186
MW-29 4-Jun-12 --------------------------9,800 ------190,000
MW-29 19-Jul-12 --------------------------12,900 ------260,000
MW-29 16-Aug-12 --------------------------13,500 ------160,000
MW-29 7-Nov-12 375 2.17 31.2 16.9 72.2 21.1 31.1J 13,400 0.136J 23.9J 132 220,000
MW-29 16-May-13 10J 2300 28.6 2.3 140 100 1610 193 0.29 200J 25,600 0.8J 575 1270 316,000
MW-29 31-Jul-13 --------------------------20,000 ------309,000
MW-29 7-Nov-13 7J 2330 25 2.4 150 100 360 176 0.29 190J 2J 22,700 0.8J 707 847 312,000
MW-29 16-Jan-14 --------------------------13,600 ------129,000
MW-29 9-Apr-14 7J 630 4.2 0.8J 68 32 71 33 0.16J 55 12,100 0.3J 124 168 268,000
MW-29 29-Oct-14 4J 330 1.5 0.5J 20 11 31 18 0.09J 21J 13,900 0.1J 47 74 228,000
MW-29 6-May-15 7J 470 2.3 0.3J 35 19 50 20 0.06J 37J 12,100 0.2J 53 104 202,000
MW-29 20-Nov-15 2J 250 1.1 1.4 14 7J 20 17 0.07J 15J 0.1J 41 87 160,000
MW-29 27-Apr-16 350 1.5 0.2J 19 11 25 21 20J 11,000 0.1J 46 70 176,000
MW-29 17-Nov-16 0.38J 3.8J 450 2.9 0.37J 26 17 58B 27 0.083J 34J 0.39J 10,000 0.12J 28 110 130,000
MW-29 27-Apr-17 83J 0.40J 5.5J 2.5J 8.2J 5.8J 0.032J 7.4J 9,100 11J 19 180,000
Notes:
1. All units are in micrograms per liter (parts per billion).
2. * - Groundwater Protection Standard
3. J - Indicates the analytical result is an estimated concentration between the laboratory method detection limit and the Solid Waste Section reporting limit.
4. B - Amount in prep blank > method detection limit
5. dup - Duplicate Sample
6. -- Not analyzed for
7. NE - Standard Not Established
- Concentration exceeds the 15A NCAC 02L .0202 or Groundwater Protection Standard
- Indicates the result is below the detection limit
- A sodium lactate injection was performed near MW-8, -9, and -10 on June 18-21, 2012.
- An emulsified vegetable oil injection was performed near MW-8, -9, and -10 on March 25-27, 2013.
Page 7 of 24 June 2017
Table 4b
Detected Groundwater Constituents - Volatile Organic Compounds
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
Permit Number 9203-MSWLF-1980
Monitoring Well CodeSample DateAcetoneBenzeneMEK (2-Butanone)ChlorobenzeneChloroethaneChloroformChloromethane1,4-DichlorobenzeneDichlorodifluoromethane1,1-Dichloroethane1,1-Dichloroethene1,2-Dichloroethanecis-1,2-Dichloroethenetrans-1,2-Dichloroethene1,2-DichloropropaneEthylbenzeneMethylene Chloride4-Methyl-2-PentanoneNaphthaleneTetrachloroethene1,1,1-TrichloroethaneTrichloroetheneTrichlorofluoromethanem,p-Xyleneso-XyleneTotal XylenesTolueneVinyl Chloride6,000 1 4,000 50 3,000 70 3 6 1,000 6 7 0.4 70 100 0.6 600 5 560*6 0.7 200 3 2,000 500 500 500 600 0.03
100 1 100 3 10 5 1 1 5 5 5 1 5 5 1 1 1 100 10 1 1 1 1 5 5 5 1 1
MW-2 31-Mar-11 1.5J
MW-2 8-Nov-11 7.6
MW-2 4-Apr-12 0.65J
MW-2 6-Nov-12 3.1J
MW-2 15-May-13
MW-2 6-Nov-13 1.7J
MW-2 9-Apr-14 8.1J 1.3J
MW-2 28-Oct-14 1.9J
MW-2 5-May-15 10J 2.7J 0.39J
MW-2 19-Nov-15 9.1
MW-2 26-Apr-16 2.3J
MW-2 17-Nov-16 3.1J
MW-2 27-Apr-17 1.2J
MW-4 31-Mar-11 1.3J
MW-4 8-Nov-11 2.0J
MW-4 4-Apr-12 0.51J 0.45J 1.9J
MW-4 6-Nov-12 2.2J
MW-4 15-May-13 0.52J 1.2J 1.9J 0.32J
MW-4 6-Nov-13 2.7J
MW-4 9-Apr-14 0.63J 0.65J 2.2J 0.26J
MW-4 28-Oct-14 0.43J 2.4J 0.43J
MW-4 5-May-15 0.64J 0.51J 3.5J
MW-4 19-Nov-15 0.56J 0.32J 3.1J 0.24J 0.44J
MW-4 26-Apr-16 0.50J 3.8J
MW-4 16-Nov-16 0.52J 0.68J 3.7J 0.64J 0.46J
MW-4 28-Apr-17 0.74J 0.73J 4.2J 0.57J 0.54J
MW-6 1-Apr-11 1.0J
MW-6 9-Nov-11 1.1J
MW-6 4-Apr-12 1.4J
MW-6 6-Nov-12 1.8J
MW-6 15-May-13 0.93J 0.97J 2.7J 0.77J 5.6 5.4 0.24J
MW-6 6-Nov-13 3.0J
MW-6 9-Apr-14 7.1J 0.60J 0.74J 4.7J 0.31J 5.4 4.1J 0.52J
MW-6 28-Oct-14 0.28J 0.94J 3.2J 0.42J 3.6J 2.0J
MW-6 5-May-15 0.77J 1.2J 2.6J 7.4 4.5J 1.5J 0.70J
MW-6 18-Nov-15 0.74J 0.36J 0.35J 5.0J 1.1J
MW-6 dup 18-Nov-15 0.68J 0.37J 0.32J 4.8J 1.1J
MW-6 27-Apr-16 0.40J 0.70J 6.2 0.94J
MW-6 16-Nov-16 0.42J 1.5J 1.2J 0.50J 5.4 1.8J 0.71J
MW-6 27-Apr-17 1.7J 0.91J 0.58J 5.4 0.77J
North Carolina 2L or
Groundwater Protection
Standard
Solid Waste Section Limit
Page 8 of 24 June 2017
Table 4b
Detected Groundwater Constituents - Volatile Organic Compounds
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
Permit Number 9203-MSWLF-1980
Monitoring Well CodeSample DateAcetoneBenzeneMEK (2-Butanone)ChlorobenzeneChloroethaneChloroformChloromethane1,4-DichlorobenzeneDichlorodifluoromethane1,1-Dichloroethane1,1-Dichloroethene1,2-Dichloroethanecis-1,2-Dichloroethenetrans-1,2-Dichloroethene1,2-DichloropropaneEthylbenzeneMethylene Chloride4-Methyl-2-PentanoneNaphthaleneTetrachloroethene1,1,1-TrichloroethaneTrichloroetheneTrichlorofluoromethanem,p-Xyleneso-XyleneTotal XylenesTolueneVinyl Chloride6,000 1 4,000 50 3,000 70 3 6 1,000 6 7 0.4 70 100 0.6 600 5 560*6 0.7 200 3 2,000 500 500 500 600 0.03
100 1 100 3 10 5 1 1 5 5 5 1 5 5 1 1 1 100 10 1 1 1 1 5 5 5 1 1
North Carolina 2L or
Groundwater Protection
Standard
Solid Waste Section Limit
MW-8 30-Mar-11 4.3J 7.8 3.8J 0.73J 1.2 1.5 4.4
MW-8 7-Nov-11 0.52J
MW-8 4-Apr-12 3.3J 4.1J 2.7J 0.38J 0.33J 0.55J 0.80J 3.6
MW-8 19-Jul-12 7.6J 0.72J 0.46J
MW-8 16-Aug-12
MW-8 6-Nov-12 0.41J 0.60J
MW-8 15-May-13 0.81J 0.47J
MW-8 31-Jul-13 0.89J 0.72J 0.26J
MW-8 6-Nov-13
MW-8 16-Jan-14 0.57J 0.38J
MW-8 10-Apr-14 7.4J 0.28J 0.97J
MW-8 29-Oct-14 0.59J 0.52J 0.31J 0.20J
MW-8 7-May-15 11J 0.72J 0.40J 0.96J 0.30J
MW-8 19-Nov-15 0.39J 0.75J 0.67J 0.34J 0.22J
MW-8 26-Apr-16 1.5J 0.59J
MW-8 16-Nov-16 2.7J 2.7J 1.4J 0.48J 0.68J
MW-8 28-Apr-17 1.2J 0.60J 1.2J
MW-9 30-Mar-11 1.8J 6.60 34 3.8J 4.0J 6.5 0.67J 5.0 5.9
MW-9 7-Nov-11 2.7J 4.3J 36 3.4J 3.8J 0.70J 4.6 3.8 4.2 0.66J
MW-9 4-Apr-12 0.43J 1.2J 3.5J 42 3.1J 4.9J 0.66J 4.5 0.35J 4.0 3.9 0.82J
MW-9 dup 4-Apr-12 0.42J 3.6J 6.10 46 3.3J 4.1J 0.74J 4.9 0.47J 4.0 6.4 0.94J
MW-9 19-Jul-12 140 0.54J 15 2.8J 0.44J 37 1.6J 4.2J 0.49J 3.3 3.2 0.46 0.81J
MW-9 16-Aug-12 120 16 6.0J 41 1.2J 3.9J 0.86J 2.4 1.3
MW-9 6-Nov-12 250 0.50J 37J 6.1J 2.1J 32 1.4J 3.6J 0.87J 2.7 2.5 0.6J 0.82J
MW-9 15-May-13 0.96J 28J 21 0.46J 21 0.42J 2.8J 2.2J 0.63J 0.76J
MW-9 dup 15-May-13 0.98J 28J 16 1.4J 20 2.5J 2.2J 0.54J 0.71J
MW-9 31-Jul-13 0.75J 22 3.1J 1.9J 0.85J
MW-9 6-Nov-13 32J 0.73J 4.2J 19 1.5J 12 1.7J 0.47J 1.5
MW-9 16-Jan-14 24J 0.57J 19 0.74J 4.9J 1.6J 0.55J 4.1 0.56J
MW-9 10-Apr-14 13J 0.71J 20 0.66J 17 0.17J 2.3J 1.2J 0.51J 2.6 1.4
MW-9 dup 10-Apr-14 23J 0.60J 21 0.59J 18 2.4J 1.2J 2.2 1.4
MW-9 29-Oct-14 6.4J 0.66J 15 0.47J 11 1.4J 0.63J 0.41J 0.98J
MW-9 dup 29-Oct-14 8.9J 0.61J 16 0.47J 0.43J 10 1.3J 0.66J 0.04J 1.09J 1.7
MW-9 7-May-15 1.1 16 1 19 1.6J 2.0J 1.3 0.91J
MW-9 20-Nov-15 0.86J 15 0.74J 0.61J 11 1.0J 0.52J 0.43J 1.5J 0.31J 0.89J 0.47J
MW-9 27-Apr-16 0.96J 14 0.74J 14 0.60J 0.51JB 0.41J 0.78J 0.53J
MW-9 16-Nov-16 1.3 12 0.77J 0.44J 7.4 2.2J 0.73J
MW-9 27-Apr-17 1.1 13 0.87J 12 0.67J 2.0J 0.40J
Page 9 of 24 June 2017
Table 4b
Detected Groundwater Constituents - Volatile Organic Compounds
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
Permit Number 9203-MSWLF-1980
Monitoring Well CodeSample DateAcetoneBenzeneMEK (2-Butanone)ChlorobenzeneChloroethaneChloroformChloromethane1,4-DichlorobenzeneDichlorodifluoromethane1,1-Dichloroethane1,1-Dichloroethene1,2-Dichloroethanecis-1,2-Dichloroethenetrans-1,2-Dichloroethene1,2-DichloropropaneEthylbenzeneMethylene Chloride4-Methyl-2-PentanoneNaphthaleneTetrachloroethene1,1,1-TrichloroethaneTrichloroetheneTrichlorofluoromethanem,p-Xyleneso-XyleneTotal XylenesTolueneVinyl Chloride6,000 1 4,000 50 3,000 70 3 6 1,000 6 7 0.4 70 100 0.6 600 5 560*6 0.7 200 3 2,000 500 500 500 600 0.03
100 1 100 3 10 5 1 1 5 5 5 1 5 5 1 1 1 100 10 1 1 1 1 5 5 5 1 1
North Carolina 2L or
Groundwater Protection
Standard
Solid Waste Section Limit
MW-10 30-Mar-11 0.79J 11 2.5 43 0.56J 3.3J 1.1 1.2J 0.73J 3.2
MW-10 7-Nov-11 3.9J 3 15 1.5 53 3.1J 0.43J 0.80J 2.2
MW-10 4-Apr-12 6.4J 4.9 0.35J 2.5 0.55J 54 2.8J 0.38J 1.6 0.81J 1.4J 0.53J 0.51J 1.1J 4.3
MW-10 19-Jul-12 840 220 8.5J 30
MW-10 16-Aug-12 5800 1,100
MW-10 6-Nov-12 780D 330D 21D 4.2JD
MW-10 dup 6-Nov-12 700D 310D 21D 3.9JD
MW-10 15-May-13 530.0 1.9 87J 24 1.9J 0.58J 0.33J 1.3J 1.7J 0.16J 4.6
MW-10 31-Jul-13 2.4 18 0.63J 0.40J 0.78J 0.48J 0.25J 20
MW-10 6-Nov-13 2.1 21 1.2 3.0J 2.5
MW-10 dup 6-Nov-13 1.6 18 0.93J 2.4J 2.6
MW-10 16-Jan-14 6.6J 2.6 17 1.5 12 1.1J 1.1 0.69J 0.76J 1.4 2.2
MW-10 10-Apr-14 8.0J 2.8 0.31J 16 1.7 20 0.22J 1.1J 1.4 1.3J 0.92J 2.5 4.2
MW-10 29-Oct-14 2.4 0.25J 18 1.6 9.0 0.43J 0.27J 0.48J 0.66J 0.39J
MW-10 7-May-15 6.6 0.82J 23 3.6 68.0 0.48J 1.9J 0.36J 2 2.6J 2.9J 2.33J 0.27J 4.5
MW-10 20-Nov-15 17J 4.1 1.4J 17 0.65J 4.0 46 0.42J 0.94J 0.22J 1.5 1.1 2.0J 0.86J 1.1J 0.34J 2.9
MW-10 27-Apr-16 17J 5.6 0.77J 27 4.3 44 0.48J 0.95J 0.94JB 2.9
MW-10 16-Nov-16 2.3J 4.7 0.71J 16 3.7 0.42J 31 0.63J 0.70J 0.43J 0.67J 0.49J 0.50J
MW-10 27-Apr-17 7.1J 2.4 0.40J 9.6J 2.8 23 0.40J 2.2
MW-11 31-Mar-11
MW-11 8-Nov-11
MW-11 4-Apr-12
MW-11 6-Nov-12
MW-11 15-May-13
MW-11 6-Nov-13
MW-11 10-Apr-14
MW-11 29-Oct-14
MW-11 6-May-15 0.55J 0.40J
MW-11 20-Nov-15 0.57J
MW-11 27-Apr-16 7.3J
MW-11 16-Nov-16
MW-11 28-Apr-17
Page 10 of 24 June 2017
Table 4b
Detected Groundwater Constituents - Volatile Organic Compounds
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
Permit Number 9203-MSWLF-1980
Monitoring Well CodeSample DateAcetoneBenzeneMEK (2-Butanone)ChlorobenzeneChloroethaneChloroformChloromethane1,4-DichlorobenzeneDichlorodifluoromethane1,1-Dichloroethane1,1-Dichloroethene1,2-Dichloroethanecis-1,2-Dichloroethenetrans-1,2-Dichloroethene1,2-DichloropropaneEthylbenzeneMethylene Chloride4-Methyl-2-PentanoneNaphthaleneTetrachloroethene1,1,1-TrichloroethaneTrichloroetheneTrichlorofluoromethanem,p-Xyleneso-XyleneTotal XylenesTolueneVinyl Chloride6,000 1 4,000 50 3,000 70 3 6 1,000 6 7 0.4 70 100 0.6 600 5 560*6 0.7 200 3 2,000 500 500 500 600 0.03
100 1 100 3 10 5 1 1 5 5 5 1 5 5 1 1 1 100 10 1 1 1 1 5 5 5 1 1
North Carolina 2L or
Groundwater Protection
Standard
Solid Waste Section Limit
MW-12 31-Mar-11
MW-12 8-Nov-11
MW-12 3-Apr-12
MW-12 5-Nov-12
MW-12 15-May-13
MW-12 6-Nov-13
MW-12 10-Apr-14
MW-12 28-Oct-14
MW-12 6-May-15 0.33J
MW-12 20-Nov-15 7.8J 0.82J
MW-12 27-Apr-16
MW-12 17-Nov-16
MW-12 27-Apr-17
MW-12 (dup)27-Apr-17 0.43J
MW-13 31-Mar-11 12.0 2.2 0.42J 1.4J
MW-13 8-Nov-11 2.1 15.0 2.0 1.9J
MW-13 3-Apr-12 2.4 17.0 3.0 2.3J
MW-13 5-Nov-12 1.6 13.0 2.5 0.52J 1.4J
MW-13 16-May-13 2.5 18 0.52J 3.2 2.4J
MW-13 7-Nov-13 1.4 12 0.73J 1.7J
MW-13 10-Apr-14 1.9 12 2.4 2.1J
MW-13 28-Oct-14 1.4 13 2.1 1.3J
MW-13 6-May-15 2 13 2.7 2.3J 0.28J 0.28J
MW-13 20-Nov-15 1.2 9.0 0.63J 1.9 1.4J 0.32J
MW-13 27-Apr-16 1.4 12 2.6 1.4J
MW-13 17-Nov-16 0.94J 8.3 2.0 0.46J 0.96J
MW-13 28-Apr-17 1.3 11 2.2 1.0J
MW-14 30-Mar-11
MW-14 7-Nov-11 25J
MW-14 3-Apr-12 0.38J 0.63J 1.2J
MW-14 5-Nov-12 0.47J
MW-14 16-May-13 0.46J
MW-14 7-Nov-13
MW-14 10-Apr-14 0.23J
MW-14 28-Oct-14 0.47J 0.41J 0.59J 0.19J
MW-14 6-May-15 0.40J 0.28J 0.61J
MW-14 dup 6-May-15 11J 0.37J 0.67J
MW-14 20-Nov-15 8.2J 0.44J 0.95J 1.2 0.71J 1.1J 0.53J 0.22J
MW-14 27-Apr-16 0.75J 3.3 1.2 1.4J 0.61J
MW-14 17-Nov-16 0.65J 3.1 0.97J 0.45J 0.98J
MW-14 28-Apr-17 0.80J 0.43J 0.62J
Page 11 of 24 June 2017
Table 4b
Detected Groundwater Constituents - Volatile Organic Compounds
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
Permit Number 9203-MSWLF-1980
Monitoring Well CodeSample DateAcetoneBenzeneMEK (2-Butanone)ChlorobenzeneChloroethaneChloroformChloromethane1,4-DichlorobenzeneDichlorodifluoromethane1,1-Dichloroethane1,1-Dichloroethene1,2-Dichloroethanecis-1,2-Dichloroethenetrans-1,2-Dichloroethene1,2-DichloropropaneEthylbenzeneMethylene Chloride4-Methyl-2-PentanoneNaphthaleneTetrachloroethene1,1,1-TrichloroethaneTrichloroetheneTrichlorofluoromethanem,p-Xyleneso-XyleneTotal XylenesTolueneVinyl Chloride6,000 1 4,000 50 3,000 70 3 6 1,000 6 7 0.4 70 100 0.6 600 5 560*6 0.7 200 3 2,000 500 500 500 600 0.03
100 1 100 3 10 5 1 1 5 5 5 1 5 5 1 1 1 100 10 1 1 1 1 5 5 5 1 1
North Carolina 2L or
Groundwater Protection
Standard
Solid Waste Section Limit
MW-15 31-Mar-11
MW-15 8-Nov-11 0.85J
MW-15 5-Apr-12 0.59J
MW-15 7-Nov-12 0.45J 0.48J 0.97J
MW-15 16-May-13 0.35J 0.69J
MW-15 7-Nov-13 1.0J
MW-15 8-Apr-14 0.85J 0.58J 0.65J
MW-15 27-Oct-14 1.1J 0.68J 0.96J
MW-15 5-May-15 0.42J 3.1 0.58J 1 0.66J 0.47J
MW-15 18-Nov-15 0.22J 1.7J 0.87J 1.3J 0.54J 0.22J
MW-15 27-Apr-16 0.34J 5.3 1.5 1.2J 0.50J
MW-15 17-Nov-16 1.7J 0.74J 0.74J
MW-15 28-Apr-17 3.2 0.92J 0.56J 0.61J
MW-16 1-Apr-11 6.2J 1.7 2.3J 6.6 5.1 1.8
MW-16 9-Nov-11 1.3 2.3J 5.1 4.3J 0.93J
MW-16 5-Apr-12 21J 1.4 0.53J 1.9J 1.7J 5.6 2.9J 2.0
MW-16 7-Nov-12 34J 1.5 0.56J 3.7J 3.6J 6.8 3.3J 0.74J 5.5
MW-16 14-May-13 1.3 0.61J 2.4J 5.2J 7.1 3.3J 0.35J 5.8
MW-16 5-Nov-13 1.2 2.5J 6.5 3.5J 2.9
MW-16 8-Apr-14 1.2 0.40J 3.5J 3.3J 8.3 0.19J 3.6J 0.92J 4.4
MW-16 27-Oct-14 0.99J 0.35J 2.7J 2.5J 6.2 0.81J 2.7J 3.7
MW-16 5-May-15 1.2 0.36J 0.48J 2.5J 7.3 3.5J 1.5J 3.5 0.36J
MW-16 3-Nov-15 1.0 1.0J 1.9J 6.5 0.17J 2.8J 3.9 0.38J
MW-16 27-Apr-16 1.0 0.39J 1.3J 0.26J 7.0 3.3J 2.0 0.49J
MW-16 16-Nov-16 1.2 0.99J 2.9J 6.1 2.8J 0.45J 3.4 0.43J
MW-16 27-Apr-17 0.91J 1.3 1.6J 6.2 3.8J 1.7
MW-17 1-Apr-11 2.6J 21 3.5J
MW-17 9-Nov-11 5.6J 17 2.8J
MW-17 5-Apr-12 2.9J 19 2.3J 0.49J
MW-17 7-Nov-12 3.6J 18 2.7J 0.43J
MW-17 14-May-13 2.1J 14 2.1J
MW-17 6-Nov-13 10 1.3J
MW-17 10-Apr-14 6.7J 1.5J 10 1.3J
MW-17 28-Oct-14 5.3J 12 2.1J 0.45J
MW-17 5-May-15 19J 1.0J 0.85J 14 2.0J 0.41J
MW-17 19-Nov-15 7.9J 0.84J 0.88J 16 0.31J 2.7J 0.24J 0.44J 1.0
MW-17 26-Apr-16 0.33J 10 1.4J
MW-17 17-Nov-16 2.7J 2.4J 9.8 1.4J
MW-17 28-Apr-17 1.8J 12 1.4J
Page 12 of 24 June 2017
Table 4b
Detected Groundwater Constituents - Volatile Organic Compounds
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
Permit Number 9203-MSWLF-1980
Monitoring Well CodeSample DateAcetoneBenzeneMEK (2-Butanone)ChlorobenzeneChloroethaneChloroformChloromethane1,4-DichlorobenzeneDichlorodifluoromethane1,1-Dichloroethane1,1-Dichloroethene1,2-Dichloroethanecis-1,2-Dichloroethenetrans-1,2-Dichloroethene1,2-DichloropropaneEthylbenzeneMethylene Chloride4-Methyl-2-PentanoneNaphthaleneTetrachloroethene1,1,1-TrichloroethaneTrichloroetheneTrichlorofluoromethanem,p-Xyleneso-XyleneTotal XylenesTolueneVinyl Chloride6,000 1 4,000 50 3,000 70 3 6 1,000 6 7 0.4 70 100 0.6 600 5 560*6 0.7 200 3 2,000 500 500 500 600 0.03
100 1 100 3 10 5 1 1 5 5 5 1 5 5 1 1 1 100 10 1 1 1 1 5 5 5 1 1
North Carolina 2L or
Groundwater Protection
Standard
Solid Waste Section Limit
MW-18 31-Mar-11
MW-18 8-Nov-11
MW-18 4-Apr-12
MW-18 6-Nov-12
MW-18 15-May-13
MW-18 6-Nov-13
MW-18 10-Apr-14
MW-18 28-Oct-14
MW-18 5-May-15 7.1J 0.52J
MW-18 19-Nov-15 7.3J 0.29J
MW-18 26-Apr-16
MW-18 16-Nov-16
MW-18 27-Apr-17
MW-19 1-Apr-11 0.64J
MW-19 9-Nov-11
MW-19 5-Apr-12 1.0J
MW-19 19-Jul-12 4.0J
MW-19 16-Aug-12
MW-19 7-Nov-12
MW-19 16-May-13 230
MW-19 31-Jul-13
MW-19 7-Nov-13
MW-19 16-Jan-14
MW-19 9-Apr-14
MW-19 29-Oct-14
MW-19 7-May-15 12J
MW-19 20-Nov-15
MW-19 26-Apr-16 0.33J
MW-19 (dup)26-Apr-16
MW-19 16-Nov-16 0.44J 0.69J
MW-19 27-Apr-17 0.54J
Page 13 of 24 June 2017
Table 4b
Detected Groundwater Constituents - Volatile Organic Compounds
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
Permit Number 9203-MSWLF-1980
Monitoring Well CodeSample DateAcetoneBenzeneMEK (2-Butanone)ChlorobenzeneChloroethaneChloroformChloromethane1,4-DichlorobenzeneDichlorodifluoromethane1,1-Dichloroethane1,1-Dichloroethene1,2-Dichloroethanecis-1,2-Dichloroethenetrans-1,2-Dichloroethene1,2-DichloropropaneEthylbenzeneMethylene Chloride4-Methyl-2-PentanoneNaphthaleneTetrachloroethene1,1,1-TrichloroethaneTrichloroetheneTrichlorofluoromethanem,p-Xyleneso-XyleneTotal XylenesTolueneVinyl Chloride6,000 1 4,000 50 3,000 70 3 6 1,000 6 7 0.4 70 100 0.6 600 5 560*6 0.7 200 3 2,000 500 500 500 600 0.03
100 1 100 3 10 5 1 1 5 5 5 1 5 5 1 1 1 100 10 1 1 1 1 5 5 5 1 1
North Carolina 2L or
Groundwater Protection
Standard
Solid Waste Section Limit
MW-20 1-Apr-11
MW-20 9-Nov-11
MW-20 5-Apr-12
MW-20 7-Nov-12
MW-20 14-May-13
MW-20 5-Nov-13
MW-20 9-Apr-14 9.3J 0.53J
MW-20 28-Oct-14
MW-20 5-May-15 8.7J 0.50J
MW-20 19-Nov-15 0.25J
MW-20 27-Apr-16
MW-20 17-Nov-16
MW-20 27-Apr-17 2.4J
MW-21 31-Mar-11
MW-21 8-Nov-11
MW-21 4-Apr-12
MW-21 6-Nov-12
MW-21 15-May-13
MW-21 6-Nov-13
MW-21 9-Apr-14
MW-21 28-Oct-14
MW-21 5-May-15 0.64J
MW-21 19-Nov-15
MW-21 26-Apr-16
MW-21 16-Nov-16
MW-21 28-Apr-17
MW-22 31-Mar-11
MW-22 8-Nov-11
MW-22 4-Apr-12
MW-22 6-Nov-12
MW-22 15-May-13
MW-22 6-Nov-13
MW-22 9-Apr-14
MW-22 28-Oct-14
MW-22 5-May-15 0.97J
MW-22 19-Nov-15
MW-22 26-Apr-16
MW-22 16-Nov-16
MW-22 (dup)16-Nov-16
MW-22 28-Apr-17
Page 14 of 24 June 2017
Table 4b
Detected Groundwater Constituents - Volatile Organic Compounds
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
Permit Number 9203-MSWLF-1980
Monitoring Well CodeSample DateAcetoneBenzeneMEK (2-Butanone)ChlorobenzeneChloroethaneChloroformChloromethane1,4-DichlorobenzeneDichlorodifluoromethane1,1-Dichloroethane1,1-Dichloroethene1,2-Dichloroethanecis-1,2-Dichloroethenetrans-1,2-Dichloroethene1,2-DichloropropaneEthylbenzeneMethylene Chloride4-Methyl-2-PentanoneNaphthaleneTetrachloroethene1,1,1-TrichloroethaneTrichloroetheneTrichlorofluoromethanem,p-Xyleneso-XyleneTotal XylenesTolueneVinyl Chloride6,000 1 4,000 50 3,000 70 3 6 1,000 6 7 0.4 70 100 0.6 600 5 560*6 0.7 200 3 2,000 500 500 500 600 0.03
100 1 100 3 10 5 1 1 5 5 5 1 5 5 1 1 1 100 10 1 1 1 1 5 5 5 1 1
North Carolina 2L or
Groundwater Protection
Standard
Solid Waste Section Limit
MW-23 31-Mar-11
MW-23 8-Nov-11
MW-23 4-Apr-12
MW-23 5-Nov-12
MW-23 15-May-13
MW-23 5-Nov-13
MW-23 10-Apr-14
MW-23 27-Oct-14
MW-23 5-May-15 0.71J
MW-23 19-Nov-15 23J 0.81J
MW-23 26-Apr-16 6.0J
MW-23 16-Nov-16 15J 0.40J
MW-23 28-Apr-17 11J
MW-24 1-Apr-11 2.6 7.6 2.1J 3.0 7.8 1.2J
MW-24 (dup)1-Apr-11 7.5 1.7J 3.3 7.6 1.2J
MW-24 9-Nov-11 3.3 10 3.4J 3.5 9.9 1.3J
MW-24 5-Apr-12 3.0 8.5 3.0J 3.5 8.6 1.0J 0.48J 0.42J
MW-24 7-Nov-12 3.2 9.5 3.2J 3.2 9.0
MW-24 16-May-13 2.9 7.9 2.5J 3.2 7.8 0.31J 1.1J 0.62J 0.42J
MW-24 6-Nov-13 2.5 6.4 3.2J 2.6 8.8 1.1J
MW-24 8-Apr-14 1.4 3.6 2.2J 1.7 5.3 0.64J 0.20J
MW-24 27-Oct-14 2.6 6.6 2.9J 2.3 9.0 1.2J 0.43J 0.33J
MW-24 5-May-15 1.1 2.1J 0.48J 1.1 4.6J 0.61J 1.6J 0.25J
MW-24 19-Nov-15 12J 1.4 3.6 1.3 5.0 0.70J 0.27J 0.21J
MW-24 25-Apr-16 7.6J 0.25J 2.0J 0.54J
MW-24 15-Nov-16 1.0 2.0J 0.86J 0.84J 3.0J
MW-24 27-Apr-17 1.3J
MW-25 31-Mar-11 1.9J 3.4J
MW-25 8-Nov-11 1.4J 3.2J
MW-25 4-Apr-12 0.65J 2.9J 4.4J
MW-25 6-Nov-12 0.78J 2.3J 3.9J
MW-25 15-May-13 0.83J 2.3J 1.2J 4.0J
MW-25 6-Nov-13 0.87J 3.2J
MW-25 9-Apr-14 0.80J 2.7J 3.1J
MW-25 28-Oct-14 0.87J 4.3J 2.6J
MW-25 5-May-15 1.4 2.1J 0.77J 3.7J 1.6J
MW-25 19-Nov-15 17J 1.2 2.7J 0.37J
MW-25 26-Apr-16 12J 1.2 2.9J
MW-25 16-Nov-16 0.80J 1.7J 0.47J 2.6J
MW-25 27-Apr-17 1.4J 2.6J
No Sample Collected - Well was Dry
No Sample Collected - Well was Dry
No Sample Collected - Well was Dry
No Sample Collected - Well was Dry
No Sample Collected - Well was Dry
Page 15 of 24 June 2017
Table 4b
Detected Groundwater Constituents - Volatile Organic Compounds
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
Permit Number 9203-MSWLF-1980
Monitoring Well CodeSample DateAcetoneBenzeneMEK (2-Butanone)ChlorobenzeneChloroethaneChloroformChloromethane1,4-DichlorobenzeneDichlorodifluoromethane1,1-Dichloroethane1,1-Dichloroethene1,2-Dichloroethanecis-1,2-Dichloroethenetrans-1,2-Dichloroethene1,2-DichloropropaneEthylbenzeneMethylene Chloride4-Methyl-2-PentanoneNaphthaleneTetrachloroethene1,1,1-TrichloroethaneTrichloroetheneTrichlorofluoromethanem,p-Xyleneso-XyleneTotal XylenesTolueneVinyl Chloride6,000 1 4,000 50 3,000 70 3 6 1,000 6 7 0.4 70 100 0.6 600 5 560*6 0.7 200 3 2,000 500 500 500 600 0.03
100 1 100 3 10 5 1 1 5 5 5 1 5 5 1 1 1 100 10 1 1 1 1 5 5 5 1 1
North Carolina 2L or
Groundwater Protection
Standard
Solid Waste Section Limit
MW-26 31-Mar-11 0.62J
MW-26 8-Nov-11 1.4 0.91J
MW-26 4-Apr-12 1.6 0.66J 1.1J 1.4J 0.49J
MW-26 6-Nov-12 1.4 0.47J 0.83J 1.1J 0.60J
MW-26 15-May-13 0.88J 0.54J 0.32J 0.57J
MW-26 6-Nov-13 0.82J
MW-26 9-Apr-14 1.5 0.69J 0.33J 1.4J 0.66J 0.87J
MW-26 28-Oct-14 1.5 0.87J 1.9J 0.37J 0.97J 0.50J
MW-26 5-May-15 16J 1.4 0.77J 0.84J 1.0J 0.50J 1.6J 0.21J
MW-26 19-Nov-15 14J 1.3 1.1J 0.42J 0.71J 0.39J 0.32J
MW-26 26-Apr-16 9.6J 1.4 1.5J 0.62J 0.70J
MW-26 16-Nov-16 3.7J 2.4 3.3 2.0J 1.9 0.84J 0.41J 1.3J
MW-26 28-Apr-17 2.1 3.3 2.6J 1.9 0.95J 0.67J
MW-27 31-Mar-11 4.1J 4.7J 1.4
MW-27 8-Nov-11 1.7J 4.4J 1.2J 0.98J
MW-27 4-Apr-12 0.45J 3.0J 5.8 1.1J 1.3
MW-27 6-Nov-12 0.46J 1.4J 5.4 1.3J 1.1
MW-27 15-May-13 0.5J 2.9J 5.5 2.5J 0.32J 1.4J
MW-27 6-Nov-13 5.0J 6.1
MW-27 9-Apr-14 0.42J 2.3J 5.7 0.67J 0.31J
MW-27 28-Oct-14 0.43J 2.0J 6.1 1.4J 0.26J 1.2J
MW-27 5-May-15 9.1J 0.54J 0.50J 2.8J 8.6 1.2J 0.38J 1.6J
MW-27 19-Nov-15 0.51J 3.3J 7.8 1.2J 0.40J 0.27J 0.65J 0.37J 1.0
MW-27 26-Apr-16 0.44J 7.6 1.3J 0.37J 0.67J 0.88J
MW-27 16-Nov-16 7.8 1.5J 0.74J 0.48J 0.66J
MW-27 28-Apr-17 4.2J 9.4 1.8J 0.40J 0.51J 0.60J
MW-28 1-Apr-11
MW-28 9-Nov-11
MW-28 5-Apr-12
MW-28 6-Nov-12
MW-28 15-May-13
MW-28 6-Nov-13
MW-28 9-Apr-14 4.1J
MW-28 28-Oct-14 1.2J
MW-28 5-May-15 6.9J 8.2 0.44J
MW-28 19-Nov-15 1.8J
MW-28 26-Apr-16 1.8J 0.43J
MW-28 16-Nov-16 0.78J
MW-28 27-Apr-17 0.53J
Page 16 of 24 June 2017
Table 4b
Detected Groundwater Constituents - Volatile Organic Compounds
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
Permit Number 9203-MSWLF-1980
Monitoring Well CodeSample DateAcetoneBenzeneMEK (2-Butanone)ChlorobenzeneChloroethaneChloroformChloromethane1,4-DichlorobenzeneDichlorodifluoromethane1,1-Dichloroethane1,1-Dichloroethene1,2-Dichloroethanecis-1,2-Dichloroethenetrans-1,2-Dichloroethene1,2-DichloropropaneEthylbenzeneMethylene Chloride4-Methyl-2-PentanoneNaphthaleneTetrachloroethene1,1,1-TrichloroethaneTrichloroetheneTrichlorofluoromethanem,p-Xyleneso-XyleneTotal XylenesTolueneVinyl Chloride6,000 1 4,000 50 3,000 70 3 6 1,000 6 7 0.4 70 100 0.6 600 5 560*6 0.7 200 3 2,000 500 500 500 600 0.03
100 1 100 3 10 5 1 1 5 5 5 1 5 5 1 1 1 100 10 1 1 1 1 5 5 5 1 1
North Carolina 2L or
Groundwater Protection
Standard
Solid Waste Section Limit
MW-29 4-Mar-11 2.1J 1.6J 0.95J 19 1.8J 0.98J
MW-29 1-Apr-11 1.3J 1.8J 19 1.1J 2.5J 1.5 1.2 0.76J 0.61J
MW-29 9-Nov-11 2.1J 0.89J 23 2.9J 1.0
MW-29 dup 9-Nov-11 2.0J 0.96J 23 3.0J 0.93J
MW-29 5-Apr-12 1.5J 1.1J 12 0.54J 1.2J 0.80J 0.68J 0.58J
MW-29 19-Jul-12 4.6J 0.45J 1.7J 21 2.6J 0.81J 0.66J
MW-29 16-Aug-12 2.1J 20 2.4J 0.83J 0.49J
MW-29 7-Nov-12 1.4J 0.68J 18 0.45J 2.6J 0.76J 1.3 0.49J
MW-29 16-May-13 12J 0.27J 1.4J 12 0.49J 1.8J 0.5J 0.76J
MW-29 31-Jul-13 0.26J 8.8J 7 0.78J 2.5J 1.5
MW-29 7-Nov-13 0.28J 3.4J 13 3.0J 0.68J
MW-29 16-Jan-14 6.3J 0.27J
MW-29 9-Apr-14 5.9J 0.89J
MW-29 29-Oct-14 7.2 1.2J 0.36J 0.33J
MW-29 6-May-15 9.4J 0.54J 1.7J 1.5J
MW-29 20-Nov-15
MW-29 27-Apr-16 1.0J
MW-29 17-Nov-16 0.78J 2.1J
MW-29 27-Apr-17 5.5J
Notes:
1. All units are in micrograms per liter (parts per billion).
2. * - Groundwater Protection Standard
3. J - Indicates the analytical result is an estimated concentration between the laboratory method detection limit and the Solid Waste Section reporting limit
4. dup - Duplicate Sample
- Concentration exceeds the 15A NCAC 02L .0202 or Groundwater Protection Standard
- Indicates the result is below the detection limit
- A sodium lactate injection was performed near MW-8, -9, and -10 on June 18-21, 2012.
- An emulsified vegetable oil injection was performed near MW-8, -9, and -10 on March 25-27, 2013.
Page 17 of 24 June 2017
Table 4c
Detected Groundwater Constituents - Pesticides, Herbicides, and PCBs
Historical Results
Feltonsville Landfill - Wake County
Permit Number 9203-MSWLF-1980
Monitoring Well CodeSample Date2,4-D2,4,5-TP(Silvex)Alpha-BHCBeta-BHCDelta-BHCGamma-BHC (Lindane)DDD4,4-DDTDieldrinDinosebEndosulfan IEndosulfan IIEndrinHeptachlor EpoxideHeptachlorMethoxychlor70 50 0.006*0.019*0.019*0.03 0.1 0.1 0.002 7*40 42*2 0.004 0.008 40
2 2 0.05 0.05 0.05 0.05 0.1 0.1 0.075 1 0.1 0.1 0.1 0.075 0.05 1
MW-2 16-Nov-04
MW-2 19-Apr-05
MW-2 8-Nov-05
MW-2 11-Apr-06
MW-2 7-Nov-06
MW-2 17-Apr-07
MW-2 6-Nov-07
MW-2 22-May-08
MW-2 2-Apr-09 0.418J
MW-2 20-May-10
MW-2 31-Mar-11
MW-4 16-Nov-04
MW-4 19-Apr-05
MW-4 8-Nov-05
MW-4 11-Apr-06
MW-4 7-Nov-06
MW-4 17-Apr-07
MW-4 6-Nov-07
MW-4 21-May-08 0.125
MW-4 3-Apr-09
MW-4 20-May-10
MW-4 31-Mar-11
MW-6 16-Nov-04
MW-6 19-Apr-05
MW-6 8-Nov-05
MW-6 11-Apr-06
MW-6 7-Nov-06
MW-6 17-Apr-07
MW-6 6-Nov-07
MW-6 22-May-08 0.0163J 0.0272J**
MW-6 3-Apr-09
MW-6 21-May-10
MW-6 1-Apr-11
MW-8 16-Nov-04
MW-8 19-Apr-05
MW-8 8-Nov-05
MW-8 11-Apr-06
MW-8 7-Nov-06
MW-8 17-Apr-07
MW-8 6-Nov-07
MW-8 22-May-08 0.0531J**
MW-9 16-Nov-04
MW-9 19-Apr-05
MW-9 8-Nov-05
MW-9 11-Apr-06
MW-9 7-Nov-06
MW-9 17-Apr-07
MW-9 6-Nov-07
MW-9 23-May-08 0.0241J
MW-9 2-Apr-09
MW-9 20-May-10
MW-9 30-Mar-11
Solid Waste Section Limit
North Carolina 2L or Groundwater
Protection Standard
Page 18 of 24 June 2017
Table 4c
Detected Groundwater Constituents - Pesticides, Herbicides, and PCBs
Historical Results
Feltonsville Landfill - Wake County
Permit Number 9203-MSWLF-1980
Monitoring Well CodeSample Date2,4-D2,4,5-TP(Silvex)Alpha-BHCBeta-BHCDelta-BHCGamma-BHC (Lindane)DDD4,4-DDTDieldrinDinosebEndosulfan IEndosulfan IIEndrinHeptachlor EpoxideHeptachlorMethoxychlor70 50 0.006*0.019*0.019*0.03 0.1 0.1 0.002 7*40 42*2 0.004 0.008 40
2 2 0.05 0.05 0.05 0.05 0.1 0.1 0.075 1 0.1 0.1 0.1 0.075 0.05 1Solid Waste Section Limit
North Carolina 2L or Groundwater
Protection Standard
MW-10 16-Nov-04
MW-10 19-Apr-05
MW-10 8-Nov-05
MW-10 11-Apr-06
MW-10 7-Nov-06 0.56J
MW-10 17-Apr-07
MW-10 6-Nov-07
MW-10 23-May-08 0.0632 0.0253J
MW-10 2-Apr-09 0.325J 0.066J 0.0399J
MW-10 20-May-10
MW-10 30-Mar-11
MW-11 16-Nov-04
MW-11 19-Apr-05
MW-11 8-Nov-05
MW-11 11-Apr-06
MW-11 7-Nov-06
MW-11 17-Apr-07
MW-11 6-Nov-07
MW-11 23-May-08 0.0227J**
MW-12 16-Nov-04 2.6
MW-12 19-Apr-05
MW-12 8-Nov-05
MW-12 11-Apr-06
MW-12 7-Nov-06
MW-12 17-Apr-07
MW-12 6-Nov-07
MW-12 22-May-08 0.0942 0.0539J 0.064J**
MW-12 2-Apr-09 0.363J 0.0484J 0.0324J
MW-12 20-May-10 0.19J
MW-12 31-Mar-11
MW-13 16-Nov-04
MW-13 19-Apr-05
MW-13 8-Nov-05
MW-13 11-Apr-06
MW-13 7-Nov-06
MW-13 17-Apr-07
MW-13 6-Nov-07
MW-13 23-May-08 0.042J 0.0647J
MW-13 2-Apr-09 0.0151J 0.0677J 0.032J 0.0125J
MW-13 20-May-10
MW-13 31-Mar-11
MW-14 16-Nov-04
MW-14 19-Apr-05
MW-14 8-Nov-05
MW-14 11-Apr-06
MW-14 7-Nov-06
MW-14 17-Apr-07
MW-14 6-Nov-07
MW-14 23-May-08 0.0866J**
Page 19 of 24 June 2017
Table 4c
Detected Groundwater Constituents - Pesticides, Herbicides, and PCBs
Historical Results
Feltonsville Landfill - Wake County
Permit Number 9203-MSWLF-1980
Monitoring Well CodeSample Date2,4-D2,4,5-TP(Silvex)Alpha-BHCBeta-BHCDelta-BHCGamma-BHC (Lindane)DDD4,4-DDTDieldrinDinosebEndosulfan IEndosulfan IIEndrinHeptachlor EpoxideHeptachlorMethoxychlor70 50 0.006*0.019*0.019*0.03 0.1 0.1 0.002 7*40 42*2 0.004 0.008 40
2 2 0.05 0.05 0.05 0.05 0.1 0.1 0.075 1 0.1 0.1 0.1 0.075 0.05 1Solid Waste Section Limit
North Carolina 2L or Groundwater
Protection Standard
MW-15 16-Nov-04
MW-15 19-Apr-05
MW-15 8-Nov-05
MW-15 11-Apr-06
MW-15 7-Nov-06
MW-15 17-Apr-07
MW-15 6-Nov-07 0.077 0.059
MW-15 23-May-08 0.088J 0.0318J 0.092J**
MW-15 (dup)23-May-08 0.0370J 0.069J**
MW-15 3-Apr-09 0.0199J
MW-15 (dup)3-Apr-09 0.504J 0.0236J
MW-15 21-May-10
MW-15 31-Mar-11
MW-16 16-Nov-04
MW-16 19-Apr-05
MW-16 8-Nov-05
MW-16 11-Apr-06
MW-16 7-Nov-06
MW-16 17-Apr-07
MW-16 6-Nov-07
MW-16 21-May-08 0.152J 0.167
MW-16 3-Apr-09 0.293J
MW-16 21-May-10
MW-16 1-Apr-11
MW-17 16-Nov-04
MW-17 19-Apr-05
MW-17 8-Nov-05
MW-17 11-Apr-06
MW-17 7-Nov-06
MW-17 17-Apr-07
MW-17 6-Nov-07
MW-17 23-May-08 0.0222J
MW-17 1-Apr-09
MW-17 21-May-10
MW-17 1-Apr-11
MW-18 16-Nov-04
MW-18 19-Apr-05
MW-18 8-Nov-05
MW-18 11-Apr-06
MW-18 7-Nov-06
MW-18 17-Apr-07
MW-18 6-Nov-07
MW-18 22-May-08 0.17 0.0322J 0.128
MW-18 3-Apr-09
MW-18 20-May-10
MW-18 31-Mar-11
MW-19 16-Nov-04
MW-19 19-Apr-05
MW-19 8-Nov-05
MW-19 11-Apr-06
MW-19 7-Nov-06
MW-19 17-Apr-07
MW-19 6-Nov-07
MW-19 23-May-08 0.0149J**
Page 20 of 24 June 2017
Table 4c
Detected Groundwater Constituents - Pesticides, Herbicides, and PCBs
Historical Results
Feltonsville Landfill - Wake County
Permit Number 9203-MSWLF-1980
Monitoring Well CodeSample Date2,4-D2,4,5-TP(Silvex)Alpha-BHCBeta-BHCDelta-BHCGamma-BHC (Lindane)DDD4,4-DDTDieldrinDinosebEndosulfan IEndosulfan IIEndrinHeptachlor EpoxideHeptachlorMethoxychlor70 50 0.006*0.019*0.019*0.03 0.1 0.1 0.002 7*40 42*2 0.004 0.008 40
2 2 0.05 0.05 0.05 0.05 0.1 0.1 0.075 1 0.1 0.1 0.1 0.075 0.05 1Solid Waste Section Limit
North Carolina 2L or Groundwater
Protection Standard
MW-20 16-Nov-04
MW-20 19-Apr-05
MW-20 8-Nov-05
MW-20 11-Apr-06
MW-20 7-Nov-06
MW-20 17-Apr-07
MW-20 6-Nov-07
MW-20 22-May-08 0.0391J 0.061J**
MW-20 3-Apr-09
MW-20 21-May-10
MW-20 1-Apr-11
MW-21 16-Nov-04
MW-21 19-Apr-05
MW-21 8-Nov-05
MW-21 11-Apr-06
MW-21 7-Nov-06
MW-21 17-Apr-07
MW-21 6-Nov-07 0.86J
MW-21 22-May-08 0.0481J 0.201
MW-21 3-Apr-09 0.53J
MW-21 20-May-10
MW-21 31-Mar-11
MW-22 16-Nov-04
MW-22 19-Apr-05 9.64
MW-22 8-Nov-05
MW-22 11-Apr-06 18.9
MW-22 7-Nov-06
MW-22 17-Apr-07
MW-22 6-Nov-07
MW-22 21-May-08 0.0415J 0.118J 0.0105J**0.0379J
MW-22 3-Apr-09
MW-22 20-May-10
MW-22 31-Mar-11
MW-23 16-Nov-04
MW-23 19-Apr-05
MW-23 8-Nov-05
MW-23 11-Apr-06
MW-23 7-Nov-06
MW-23 17-Apr-07
MW-23 6-Nov-07
MW-23 21-May-08 0.0230J 0.0557J**
MW-23 1-Apr-09
MW-23 20-May-10
MW-23 31-Mar-11
MW-24 16-Nov-04
MW-24 19-Apr-05
MW-24 8-Nov-05
MW-24 11-Apr-06 20.8
MW-24 7-Nov-06
MW-24 17-Apr-07
MW-24 6-Nov-07 0.073
MW-24 22-May-08 0.0693 0.1 0.0303J 0.0284J 0.114
MW-24 3-Apr-09 1.75 0.150J 0.0586J 0.0589J
MW-24 21-May-10
MW-24 (dup)21-May-10
MW-24 1-Apr-11
MW-24 (dup)1-Apr-11
Page 21 of 24 June 2017
Table 4c
Detected Groundwater Constituents - Pesticides, Herbicides, and PCBs
Historical Results
Feltonsville Landfill - Wake County
Permit Number 9203-MSWLF-1980
Monitoring Well CodeSample Date2,4-D2,4,5-TP(Silvex)Alpha-BHCBeta-BHCDelta-BHCGamma-BHC (Lindane)DDD4,4-DDTDieldrinDinosebEndosulfan IEndosulfan IIEndrinHeptachlor EpoxideHeptachlorMethoxychlor70 50 0.006*0.019*0.019*0.03 0.1 0.1 0.002 7*40 42*2 0.004 0.008 40
2 2 0.05 0.05 0.05 0.05 0.1 0.1 0.075 1 0.1 0.1 0.1 0.075 0.05 1Solid Waste Section Limit
North Carolina 2L or Groundwater
Protection Standard
MW-25 16-Nov-04
MW-25 19-Apr-05
MW-25 8-Nov-05
MW-25 11-Apr-06
MW-25 7-Nov-06
MW-25 17-Apr-07
MW-25 6-Nov-07
MW-25 22-May-08 0.234 0.0466J 0.101 0.0452J 0.116 0.0141J
MW-25 3-Apr-09 0.0113J 0.0202J
MW-25 20-May-10
MW-25 31-Mar-11
MW-26 16-Nov-04
MW-26 19-Apr-05
MW-26 8-Nov-05
MW-26 11-Apr-06
MW-26 7-Nov-06 0.052
MW-26 17-Apr-07
MW-26 6-Nov-07 0.058
MW-26 21-May-08 0.0282J
MW-26 3-Apr-09 0.176J 0.177J 0.438J
MW-26 20-May-10
MW-26 31-Mar-11
MW-27 16-Nov-04
MW-27 19-Apr-05
MW-27 8-Nov-05
MW-27 11-Apr-06
MW-27 7-Nov-06
MW-27 17-Apr-07
MW-27 6-Nov-07
MW-27 21-May-08 0.0436J**
MW-28 19-Apr-05
MW-28 8-Nov-05
MW-28 11-Apr-06
MW-28 7-Nov-06
MW-28 17-Apr-07
MW-28 6-Nov-07
MW-28 22-May-08 0.0484J**
Notes:
1. All units are in micrograms per liter (parts per billion).
2. * - Groundwater Protection Standard
3. J - Indicates the analytical result is an estimated concentration between the laboratory method detection limit and the Solid Waste Section reporting Limit.
4. B - Amount in prep blank > method detection limit
5. ** - Endosulfan I was also detected in the Method Blank and Equipment Blank at similar concentrations.
6. NS - Not Sampled; dup - Duplicate Sample
- Concentration exceeds the 15A NCAC 02L .0202 or Groundwater Protection Standard
- Indicates the result is below the detection limit
Page 22 of 24 June 2017
Table 4d
Detected Surface Water Constituents -
Metals and Volatile Organic Compounds
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
Permit Number 9203-MSWLF-1980
AntimonyArsenicBariumBerylliumCadmiumChromiumCobaltCopperLeadNickelSeleniumSilverVanadiumZincAcetoneChloromethaneToluene640**10**200,000**6.5*0.15*24*4**2.7*0.54*16*5*0.06*NS 36*2,000*96**11*
6 10 100 1 1 10 10 10 10 50 10 10 25 10 100 1 1
SW-1 31-Mar-11 48.6J 1.11J 3.55J 3.02J 5.99J
SW-1 8-Nov-11 43.3J 0.111J 2.90J 5.10J 4.98J
SW-1 4-Apr-12 57.1J 3.18JB 1.84J
SW-1 6-Nov-12 39.4J
SW-1 14-May-13 60J 0.06J 0.4J 0.9J 1J 0.7J 0.8J 5JB
SW-1 5-Nov-13 0.9J 50J 0.6J 3JB 0.7J 4JB
SW-1 9-Apr-14 40J 0.9J 0.4J 2J 0.6J 0.8J 5J 7JB 8.1J
SW-1 28-Oct-14 40J 0.4JB 0.4J 0.6J 0.6J
SW-1 5-May-15 40J 0.4J 1J 0.2J 0.7J 3JB 0.73J
SW-1 19-Nov-15 2J 70J 0.2J 0.5J 3J 2J 4J 3J 2J 1J 13J 16
SW-1 26-Apr-16 0.7J 40J 0.3J 1J 0.3J 0.6J 3J
SW-1 16-Nov-16 0.24J 0.73J 56J 0.28J 1.2J 1.1J 1.9J
SW-1 28-Apr-17 40J 1.6J 0.45J 3.3J 3.3J
SW-2 30-Mar-11 86.1J 3.16J 1.24J 2.18J 16
SW-2 8-Nov-11 3.63J 55.8J 0.165J 3.42J 6.80J 12.3
SW-2 4-Apr-12 69.4J 2.66JB 2.04J 5.75J
SW-2 6-Nov-12 3.37J 76.9J 2.30J 9.18J
SW-2 14-May-13 1J 80J 0.1J 1J 2J 2J 2J 2J 3J 10B 0.21J
SW-2 5-Nov-13 60J 0.1J 1J 0.6J 3JB 0.8J 1J 7J 11B
SW-2 8-Apr-14 0.6J 50J 1J 0.6J 2J 1J 0.8J 6J 11B
SW-2 27-Oct-14 30J 0.3JB 0.2J 1J 0.3J 5J
SW-2 5-May-15 60J 0.2J 1J 0.8J 0.3J 0.7J 25 0.6J
SW-2 18-Nov-15 0.2J 70J 0.04J 0.8J 0.5J 1J 0.3J 0.7J 1J 13
SW-2 25-Apr-16
SW-2 17-Nov-16 0.34J 1.5J 130 0.20J 0.052J 3.5J 1.8J 5.4JB 4.2J 2.8J 8.9J 23 2.8J
SW-2 28-Apr-17 66J 1.5J 1.0J 1.5J 4.0J 6.8J
DRY
Volatile Organic Compounds
North Carolina 2B Freshwater
Aquatic Life or Human Health
Standard
Solid Waste Section LimitSample DateSurface Water Sample CodeMetals
Page 23 of 24 June 2017
Table 4d
Detected Surface Water Constituents -
Metals and Volatile Organic Compounds
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
Permit Number 9203-MSWLF-1980
AntimonyArsenicBariumBerylliumCadmiumChromiumCobaltCopperLeadNickelSeleniumSilverVanadiumZincAcetoneChloromethaneToluene640**10**200,000**6.5*0.15*24*4**2.7*0.54*16*5*0.06*NS 36*2,000*96**11*
6 10 100 1 1 10 10 10 10 50 10 10 25 10 100 1 1
Volatile Organic Compounds
North Carolina 2B Freshwater
Aquatic Life or Human Health
Standard
Solid Waste Section LimitSample DateSurface Water Sample CodeMetals
SW-3 31-Mar-11 48.3J 1.10J 3.66J 2.05J 1.42J 3.42J 6.05J
SW-3 8-Nov-11 3.99J 52.2J 0.141J 2.36J 3.50JB 8.01J 7.55J
SW-3 4-Apr-12 46.7J 2.88JB
SW-3 6-Nov-12 41.5J 1.62J
SW-3 15-May-13 0.6J 40J 0.3J 0.8J 0.2J 0.5J 2JB
SW-3 5-Nov-13 0.6J 40J 0.6J 0.4J 2JB 0.4J 1J 3J 6JB
SW-3 8-Apr-14 50J 0.05J 1J 0.7J 2J 1J 1J 6J 10B
SW-3 27-Oct-14 40J 0.4JB 0.5J 0.7J 0.2J 0.7J 2JB
SW-3 5-May-15 0.8J 40J 0.3J 0.5J 1J 0.3J 0.7J 4JB 0.94J
SW-3 18-Nov-15 50J 0.4J 0.6J 1J 0.2J 0.8J 3J
SW-3 26-Apr-16 40J 0.3J 0.4J 1J 0.4J 0.7J 4JB
SW-3 16-Nov-16 0.45J 38J 0.93J 0.19J 0.77J 2.0J
SW-3 28-Apr-17 41J 0.16J 1.6J 0.68J 3.6J 4.6J 2.4J
Notes:
1. All units are in micrograms per liter (parts per billion).
2. * - Freshwater Aquatic Life Standard
3. ** - Human Health Standard
4. J - Indicates the analytical result is an estimated concentration between the laboratory method detection limit and the Solid Waste Section reporting limit
5. B - Amount in prep blank > method detection limit
- Concentration exceeds the North Carolina 15A NCAC 02B Freshwater Aquatic Life or Human Health Standard for Class C Waters
- Indicates the result is below the detection limit
Page 24 of 24 June 2017
Table 5
Constituents Detected Above Standards
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
Permit Number 9203-MSWLF-1980
MW-2 Vanadium*
MW-4 Vanadium*
MW-6 Cobalt*, Vanadium*
MW-8 Cobalt*, Vanadium*
MW-9 Barium, Cobalt*, Sodium*, Vanadium*, Benzene, 1,1-Dichloroethane
MW-10 Arsenic, Cobalt*, Sodium*, Vanadium*, Benzene, 1,1-Dichloroethane, Vinyl Chloride
MW-11 Cobalt*, Vanadium*
MW-12 None
MW-13 Cobalt*, Vanadium*, Benzene
MW-14 Antimony*, Vanadium*
MW-15 Vanadium*
MW-16 Arsenic, Cobalt*, 1,1-Dichloroethane
MW-17 Vanadium*, 1,1-Dichloroethane
MW-18 Cobalt*, Vanadium*
MW-19 Cobalt*, Vanadium*
MW-20 Vanadium*
MW-21 Vanadium*
MW-22 Cobalt*, Vanadium*
MW-23 Cobalt*, Vanadium*
MW-24 Arsenic, Cobalt*, Vanadium*
MW-25 Barium, Vanadium*
MW-26 Cobalt*, Vanadium*, Benzene
MW-27 Vanadium*, 1,1-Dichloroethane
MW-28 Chromium, Cobalt*, Vanadium*
MW-29 Cobalt*, Vanadium*
Notes:
1. Bold - "J" flag
2. (*) - Groundwater Protection Standard
APRIL 2017 PARAMETERS EXCEEDING THE NORTH CAROLINA 2L OR
GROUNDWATER PROTECTION STANDARDMONITORING WELL CODE
Page 1 of 1 June 2017
Table 6
Geochemical Data
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
Permit Number 9203-MSWLF-1980
Monitoring Well CodeSample DateOxidation Reduction Potential (mV)pHDissolved Oxygen Biochemical Oxygen DemandChemical Oxygen DemandMethane (ug/l)Ethane (ug/l)Ethene (ug/l)ChlorideNitrateSulfateSulfideTotal Organic CarbonAlkalinity (CaCO3)Carbon DioxideFerrous IronAcetic AcidButyric AcidLactic AcidPropionic AcidPyruvic AcidDissolved Hydrogen (nM)NS NS NS NS NS NS NS NS NS 10,000 250,000 1,000 NS NS NS NS NS NS NS NS NS NS
MW-2 31-Mar-11 154.5 6.82 3.52 <2 77 <0.49 <1.5 <1.6 560 0.084J 30J <0.01 4.4 160 5.1 0.095 <0.083 <0.16 <0.44 <0.18 <0.14 --
MW-2 8-Nov-11 298.0 9.11 6.63 <2 100 0.969 <1 <2.3 1,200BD 0.87J 19J <0.01 7.4 260D 27.3 0.040 0.98 <0.024 <0.062 <0.057 <0.061 --
MW-2 4-Apr-12 211.8 6.73 8.20 <2 67 <0.72 <1 <2.3 450BD 0.47J 33JB <0.01 2.1 150D 8.7 0.052 <0.04 <0.024 <0.062 <0.057 <0.061 --
MW-2 6-Nov-12 41.4 6.85 6.12 <2 180 <0.43 <0.2 <0.54 1,200BD 0.85J 23J <0.01 6.4 230D 29.3 <0.046 <0.031 <0.031 <0.095 <0.063 <0.010 --
MW-2 15-May-13 109.7 7.02 6.94 <4 22 <0.3 <0.061 <0.069 462 0.14J 35.2 <0.4 2.6 152 5.2 0.0*<0.50 <1.0 <0.50 <0.50 <0.25 --
MW-2 6-Nov-13 21.2 7.46 8.19 <4 46 0.34 <0.061 <0.069 834 0.54 32.5 <0.4 2.7 215 12 1.1*<0.50 <1.0 <0.50 <0.50 <0.25 --
MW-2 9-Apr-14 124.1 6.76 7.71 <2 52 <0.3 <0.061 <0.069 589 0.22 32.5 <0.4 5.1 162 8 0.0*1.40 <1.0 <0.50 <0.50 <0.25 --
MW-2 28-Oct-14 59.3 6.63 6.08 <4 430 <0.3 <0.061 <0.069 1,040 0.47 26.4 <0.4 5.7 232 13.0 0.0*<0.50 <1.0 <0.50 <0.50 <0.25 --
MW-2 5-May-15 69.1 6.75 6.01 <2 25 <0.3 <0.061 <0.069 785 0.9J 30.9 <0.4 4.3 175 6.0 0.0*<0.50 <1.0 <0.50 <0.50 <0.25 --
MW-2 19-Nov-15 130.2 6.89 6.60 <2.0 169 <0.30 <0.061 <0.069 1,480 0.8J 17.7 <0.4 12.5 274 19 0.0*<0.50 <1.0 <0.50 <0.50 <0.020 --
MW-2 26-Apr-16 93.0 7.31 7.50 <2.0 42 <0.30 <0.061 <0.069 756 0.24 26.1 <0.4 7.1 180 8.3 0.0*<0.50 <1.0 <0.50 <0.50 <0.020 --
MW-2 17-Nov-16 82.6 7.32 7.65 <12 29 <10 <10 <10 1,100D 0.45 24 --6.4 200 190 0.0*<1.0 <1.0 <2.0 <1.0 <1.0 --
MW-2 27-Apr-17 154.9 6.91 6.72 <2.0 20 2.8B <10 <10 730D 0.20D 14D <1.0 4.7 170 160 0.0*<1.0 <1.0 <2.0 <1.0 <1.0 --
MW-8 30-Mar-11 129.6 6.27 1.16 <2 <10 49.1 <1.5 <1.6 4.9 0.08J 2.8J <0.01 1.1 180 507D <0.037 <0.083 <0.16 <0.44 <0.18 <0.14 2.1
MW-8 7-Nov-11 161.7 6.08 2.09 <2 <10 4.5 <1 <2.3 4.1B 0.33J 2.4J <0.01 <0.28 120 62.2 0.033 1.1 <0.024 0.19 0.28 <0.061 1.0
MW-8 4-Apr-12 167.8 6.59 1.65 <2 <10 1,430D <1 <2.3 4.7B 0.27J 2.2JB <0.01 0.54 120 90.5 0.056 <0.04 <0.024 0.082 <0.057 <0.061 7.5
MW-8 19-Jul-12 -43.5 6.36 0.21 <2 21 7.32 <0.2 <0.54 4.1 0.2*7*----144*182*2.4*3.4 <0.31 0.330 2.50 <0.01 --
MW-8 16-Aug-12 -56.1 5.85 0.59 <2 17 26.7 <0.2 <0.54 4.1 0.3*1*----190*186*1.6*------------
MW-8 6-Nov-12 -63.4 6.31 0.93 <2 17 96.5D <0.2 <0.54 5.3B 0.7*2.40J <0.01 1.6 150 40.6 1.0*0.56 <0.031 <0.095 0.37 <0.010 4.5
MW-8 15-May-13 -59.4 5.12 1.43 34.7 20 110.0 0.17 0.35 5.55 <0.03 0.63 <0.4 3.8 155 22 3.5*3.0 <1.0 <0.50 0.96J <0.25 64
MW-8 31-Jul-13 -33.8 7.12 0.96 --30 3,000 1.6 1.4 4.85 <0.03 0.52 ----191 15 2.8*23.0 <1.0 <0.50 <0.50 <0.25 --
MW-8 6-Nov-13 -81.4 7.27 0.81 <2 <16 600 <0.061 0.17 4.15 <0.03 0.51 <0.4 0.5 152 17 1.2*<0.50 <1.0 <0.50 <0.50 <0.25 1.6
MW-8 16-Jan-14 -94.8 7.09 0.49 --<16 1,400 0.14 0.10 4.37 <0.03 0.48J ----168 18 0.8*<0.50 <1.0 <0.50 <0.50 <0.25 --
MW-8 10-Apr-14 -77.7 7.08 1.53 47.2 <16 200 <0.061 <0.069 4.9 0.15J 0.7J <0.4 1.9 154 12 0.0*1.9 <1.0 <0.50 <0.50 <0.25 1.6
MW-8 29-Oct-14 -76.4 5.90 0.78 <4 <5 110 <0.061 0.10 5.10 <0.03 1.1 <0.4 0.4 138 23 0.5*<0.50 <1.0 <0.50 <0.50 <0.25 1.6
MW-8 7-May-15 -78.3 6.57 0.89 16.5 <16 210 <0.061 <0.069 5.70 <0.03 4.2B <0.4 1.0 165 9.6 3.0*<0.50 <1.0 <0.50 <0.50 <0.25 18.0
MW-8 19-Nov-15 -7.9 6.18 2.79 3.1 <16 32 0.23 <0.069 5.3 0.09J 1.4 <0.4 0.5 120 19 0.5*<0.50 <1.0 <0.50 <0.50 <0.020 12
MW-8 26-Apr-16 -40.8 7.13 1.45 <2.0 14J 890 0.31 <0.069 5.2 0.06J 1.3 <0.4 0.6 141 12 3.0*<0.50 <1.0 <0.50 <0.50 <0.020 2.8
MW-8 16-Nov-16 -1.7 7.18 1.69 <2.0 <10 270B <10 <10 9.0 0.0072J 0.23J 1.6 0.71 130 150 0.5*<0.10 <0.10 <0.20 <0.10 <0.10 7.3
MW-8 28-Apr-17 -6.7 6.42 1.38 <2.0 <10 64B <10 <10 7.3 0.042J <1.0 <1.0 120 0.74J 110 1.5*<0.10 <0.10 <0.20 <0.10 <0.10 13
MW-9 30-Mar-11 51.8 6.08 0.90 <2 <10 29.1 <1.5 <1.6 9.9 7.0J 2.9J <0.01 1.0 210 219 0.078 <0.083 <0.16 <0.44 <0.18 <0.14 2.0
MW-9 7-Nov-11 1.1 6.11 1.21 <2 <10 174D <1 <2.3 9.9B 0.12J 2.9J <0.01 0.43 200D 315D 0.10 1.4 <0.024 0.34 0.27 <0.061 1.6
MW-9 4-Apr-12 148.8 6.41 2.71 <2 29 310D <1 <2.3 12B 0.061J 2.8JB <0.01 0.80 210D 342D 0.21 <0.04 <0.024 <0.062 0.12 <0.061 8.2
MW-9 19-Jul-12 -99.8 6.40 0.18 <2 690 602D <0.2 <0.54 17 0*6*----506*440*9.8*230 110 22 76 <0.01 --
MW-9 16-Aug-12 -112.9 6.31 0.58 <2 440 5,330D 1.24 2.34 15 1.5*9*----408*368*10.0*------------
MW-9 6-Nov-12 -109.6 6.36 1.06 >73 930 6,190D 1.04 2.26 23B 2.1*2.30J <0.01 310D 650D 88.1 3.8*230 180 <0.095 120 <0.01 39
MW-9 15-May-13 -71.4 5.72 1.27 198 961 4,400 2.2 1.7 36.8 <0.03 0.58 <1.6 163 312 71 7.8*71 8 <0.50 17 <0.25 11
MW-9 31-Jul-13 -55.2 6.49 1.21 --156 6,200 0.58 0.16 32.1 <0.03 0.57 ----367 220 11.3*30 2.9 <0.50 9.3 <0.25 --
MW-9 6-Nov-13 -52.2 6.49 0.89 58.7 125 8,600 0.96 0.40 27.7 <0.03 0.53 <0.4 32.3 348 120 9.5*54 <1.0 <0.50 3.6 <0.25 9.8
MW-9 16-Jan-14 -128.5 6.40 0.28 --63 5,100 0.27 <0.069 24.2 <0.03 0.53 ----388 210 3.0*6.8 <1.0 <0.50 <0.50 <0.25 --
MW-9 10-Apr-14 -29.1 6.63 0.93 51.7 88 12,000 1.10 0.31 25.4 <0.03 0.5J <0.4 16.8 325 110 3.5*32.0 <1.0 <0.50 <0.50 <0.25 4.0
MW-9 29-Oct-14 -90.3 5.40 1.39 25.3 72 9,700 1.1 0.21 25.9 0.09J 0.8J <0.4 15.1 308 79 2.0*21 <1.0 <0.50 <0.50 <0.25 --
MW-9 7-May-15 -81.7 6.34 1.13 18.1 29 11,000 2.2 0.60 28.9 <0.03 0.8BJ <0.4 8.7 374 62 1.0*10 <1.0 <0.50 <0.50 <0.25 7.8
MW-9 20-Nov-15 -51.4 6.18 1.97 9.5 24 6,400 0.93 <0.069 27.9 <0.03 0.6J <1.6 7.2 349 62 4.0*7.0 <1.0 <0.50 <0.50 <0.020 16
MW-9 27-Apr-16 -47.4 6.86 0.96 14.0 32 6,000 1.1 0.2 31.1 <0.04 0.5J <0.8 7.1 325 72 3.0*8.4 <1.0 <0.50 <0.50 <0.020 5.1
MW-9 16-Nov-16 -48.3 7.08 1.91 23 33 11,000BD <10 <10 36 0.0064J <1.0 1.0 7.4 310 400 3.0*7.1DB <0.10 <0.20 0.14 <0.10 9.7
MW-9 27-Apr-17 -17.9 6.62 1.38 17 21 11,000BD <100 <100 42D 0.025 <1.0 <1.0 6.1 320 360 2.0*2.7 <0.10 <0.20 <0.10 <0.10 2.6
MW-10 30-Mar-11 -33.1 5.81 1.29 <2 60 1,950 <1.5 <1.6 100 0.063J 12J <0.01 16 250 478 5.7 6.0 <0.16 <0.44 0.52 <0.14 2.0
MW-10 7-Nov-11 -76.5 5.82 1.29 <2 38 2,540D <1 <2.3 77B 0.052J 5.9J <0.01 8.9 250D 509D 1.1 <0.40 <0.024 <0.062 5.3 <0.061 0.92
MW-10 4-Apr-12 84.8 6.05 1.18 4.5 80 6,540D <1 <2.3 130BD 0.069J 11JB 0.17J 13 270D 653D 5.3 <0.04 <0.024 <0.062 8.8 <0.061 3.5
MW-10 19-Jul-12 -96.7 5.93 0.63 <2 13,000 1,590D <0.2 4.89 150 5*90*----1,650*2,080*30*1500 2000 220 1800 4.2 --
MW-10 16-Aug-12 -54.6 5.85 0.36 <2 13,000 1,470D <0.2 1.76 140 4*30*----1,860*2,140*36*------------
MW-10 6-Nov-12 -48.6 5.74 1.15 >220 2,100 16,200D <0.2 <0.54 67B 4.6*61*<0.01 660D 1,800 442 12*210 45 <0.095 630D 0.43 4.2
MW-10 15-May-13 -54.9 5.65 1.28 195 1,250 4,200 0.22 0.13 63.1 0.03J 0.56 1.0J 597 729 340 17.2*120 33 1.1 86 <0.25 11
MW-10 31-Jul-13 -84.7 6.39 2.08 --265 5,300 0.098 0.11 108 <0.03 0.77 ----487 350 48.2*3.4 4.0 <0.50 <0.50 0.26 --
MW-10 6-Nov-13 -59.4 6.69 1.94 19.1 118 6,500 0.25 <0.069 77.6 0.15J 0.54 <0.4 30.6 662 300 8.2*4.4 <1.0 <0.50 <0.50 <0.25 3.4
MW-10 16-Jan-14 -114.4 6.16 0.31 --116 6,800 <0.061 0.08 81.4 <0.03 1.95 ----308 400 1.75*<0.50 <1.0 <0.50 <0.50 0.41 --
MW-10 10-Apr-14 -38.5 6.15 2.19 12.7 59 7,600 0.13 0.260 78.9 <0.03 3.6 0.4J 14.7 226 400 2.5*<0.50 <1.0 <0.50 <0.50 <0.25 1.0
MW-10 29-Oct-14 -90.0 5.35 0.92 12.8 104 5,400 0.43 <0.069 93.7 0.08J 1.6 <0.4 16.8 505 240 2.5*1.0 <1.0 1.0 <0.50 0.29 1.40
MW-10 7-May-15 -67.7 5.79 1.19 5.9 78 2,300 0.27 0.32 180.0 <0.03 7.3B <0.4 22.6 421 290 3.0*<0.50 <1.0 <0.50 <0.50 0.61 1.90
MW-10 20-Nov-15 -29.5 6.01 3.61 4.4 105 840 <0.061 <0.069 144 <0.3 9J <0.4 24.2 457 210 3.0*1.1 <1.0 <0.50 <0.50 <0.020 13
MW-10 27-Apr-16 -36.5 6.20 2.07 6.8 97 710 <0.061 <0.069 207 <0.04 13.2 <0.4 23.5 444 240 5.5*0.5 <1.0 <0.50 <0.50 1.0 2.8
MW-10 16-Nov-16 -30.6 6.54 1.16 12 93 4,000BD <10 <10 190D <0.10 3.6JD 0.72J 21 390 1,000 6.5*<1.0 <1.0 <2.0 <1.0 <1.0 5.8
MW-10 27-Apr-17 -14.5 5.73 1.73 4.3 39 2,900B <10 <10 64D 0.0071J 5.0 <1.0 10 200 440 4.5*<0.10 <0.10 <0.20 <0.10 <0.10 3.5
Solid Waste Section Limit
Page 1 of 3 June 2017
Table 6
Geochemical Data
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
Permit Number 9203-MSWLF-1980
Monitoring Well CodeSample DateOxidation Reduction Potential (mV)pHDissolved Oxygen Biochemical Oxygen DemandChemical Oxygen DemandMethane (ug/l)Ethane (ug/l)Ethene (ug/l)ChlorideNitrateSulfateSulfideTotal Organic CarbonAlkalinity (CaCO3)Carbon DioxideFerrous IronAcetic AcidButyric AcidLactic AcidPropionic AcidPyruvic AcidDissolved Hydrogen (nM)NS NS NS NS NS NS NS NS NS 10,000 250,000 1,000 NS NS NS NS NS NS NS NS NS NSSolid Waste Section Limit
MW-12 31-Mar-11 130.6 6.62 1.49 <2 28 14.4 <1.5 <1.6 290 <0.025 14J <0.01 7.1 700 196 <0.037 11.0 1.10 <0.44 <0.18 <0.14 2.3
MW-12 8-Nov-11 -42.9 6.98 1.94 <2 23 45.1 <1 <2.3 160BD <0.025 12J <0.01 2.4 280D 69.9 <0.030 0.67 <0.024 <0.062 0.56 <0.061 0.88
MW-12 3-Apr-12 148.5 6.86 2.23 <2 34 20.2 <1 <2.3 240BD 0.045J 12JB <0.01 3.4 540D 177D 0.049 <0.04 <0.024 <0.062 0.87 <0.061 6.9
MW-12 5-Nov-12 -65.4 7.09 1.14 <2 17 26.7 <0.2 <0.54 150BD <0.025 11J <0.01 2.2 240D 66.7 <0.031 <0.031 <0.031 <0.095 0.24 <0.010 5.1
MW-12 15-May-13 1.7 6.25 1.75 <4 <16 6.9 <0.061 <0.069 223 0.18J 10.7 <0.4 4.6 523 110 0.0*<0.50 1.5J <0.50 <0.50 <0.25 0.74
MW-12 6-Nov-13 -19.7 7.09 1.25 <2 <16 13 <0.061 <0.069 179 <0.03 11.4 <0.4 2.8 351 60 1.0*<0.50 <1.0 <0.50 <0.50 <0.25 0.99
MW-12 10-Apr-14 14.9 6.99 3.33 <2 19 3.8 <0.061 <0.069 258 0.17J 14.7 <0.4 5 651 140 0.0*<0.50 <1.0 <0.50 <0.50 <0.25 0.89
MW-12 28-Oct-14 -42.4 5.81 0.91 <4 21 10.0 <0.061 <0.069 184 <0.03 13.3 <0.4 2.0 401 42 0.0*<0.50 <1.0 <0.50 <0.50 <0.25 0.74
MW-12 6-May-15 4.1 6.73 1.18 <2 19 22.0 <0.061 <0.069 245 <0.03 18.6 <0.4 5.5 736 120 0.0*<0.50 <1.0 <0.50 <0.50 <0.25 2.60
MW-12 20-Nov-15 -23.2 6.68 6.11 <2.0 <16 3.6 <0.061 <0.069 169 <0.2 7.6 <1.6 3.3 288 24 0.5*2.4 <1.0 <0.50 <0.50 <0.020 29
MW-12 27-Apr-16 -44.0 7.02 6.36 <2.0 32 7.3 <0.061 <0.069 238 <0.08 21.0 0.8J 6.4 699 96 1.0*<0.50 <1.0 0.56J <0.50 <0.020 2.5
MW-12 17-Nov-16 -39.5 7.29 1.36 <12 9.6 17B <10 <10 180D <0.10 13D --2.5 330 340 1.0*<0.10 <0.10 <0.20 <0.10 <0.10 4.7
MW-12 27-Apr-17 1.2 6.45 1.43 <2.0 15 21B <10 <10 220D <0.040 16D <1.0 5.2 610 600 0.5*<1.0 <1.0 <2.0 <1.0 <1.0 3.3
MW-13 20-May-10 74.4 6.14 1.69 <2 5 597 <0.4 <0.4 58 <0.025 4J <0.031 3.8 200 348 0.509 <0.083 <0.16 2.4 0.56 <0.14 1.2
MW-13 2-Nov-10 89.8 6.02 0.98 <2 20 418 <1.5 <1.6 63 <0.025 4.9J <0.01 4.8 220 365 0.13 <0.083 <0.16 <0.44 <0.18 <0.14 5.6
MW-13 31-Mar-11 99.9 5.70 1.58 <2 19 1,300 <1.5 <1.6 61 <0.025 5.5J <0.01 5.9 210 498 0.44 <0.083 <0.16 <0.44 <0.18 <0.14 2.2
MW-13 8-Nov-11 -20.4 5.76 3.81 <2 38 3,150D <1 <2.3 49B 0.170J 7.2J <0.01 8.6 250D 737D 0.16 0.72 <0.024 <0.062 <0.057 <0.061 0.96
MW-13 3-Apr-12 200.9 5.93 1.28 <2 48 2,260D <1 <2.3 45B 0.050J 8.7JB <0.01 6.0 250D 559D 0.47 <0.04 <0.024 <0.062 <0.057 <0.061 7.0
MW-13 5-Nov-12 50.7 5.84 1.07 <2 28 1,050D <0.2 <0.54 61B <0.025 6.80J <0.01 4.9 230D 993D <0.046 <0.031 <0.031 2.70 0.23 <0.010 5.7
MW-13 16-May-13 48.3 5.73 1.41 <4 27 410 <0.061 <0.069 48.4 0.14J 7.25 <0.4 5.8 237 450 0.7*<0.5 <1.0 <0.50 <0.50 <0.25 0.61
MW-13 7-Nov-13 35.2 5.92 1.24 <2 <16 190 <0.061 <0.069 66.0 0.18J 5.12 <0.4 3.3 253 550 0.2*<0.5 <1.0 <0.50 <0.50 <0.25 1.0
MW-13 10-Apr-14 90.4 5.94 2.64 <2 30 430 <0.061 <0.069 35.6 0.29 7 <0.4 7.1 178 --0.5*<0.5 <1.0 <0.50 <0.50 <0.25 2.0
MW-13 28-Oct-14 70.5 5.17 0.74 <4 33 150 <0.061 <0.069 47.9 0.14J 8.5 <0.4 5.3 263 350 0.0*<0.5 <1.0 <0.50 <0.50 <0.25 1
MW-13 6-May-15 42.5 5.10 1.09 <2 <16 270 <0.061 <0.069 39.3 0.12J 9.2B <0.4 6.7 197 300 0.0*<0.5 <1.0 <0.50 <0.50 <0.25 6
MW-13 20-Nov-15 119.4 5.49 6.40 <2.0 <16 100 <0.061 <0.069 32.7 0.37 6.3 <0.4 7.5 162 190 0.5*<0.50 <1.0 <0.50 <0.50 <0.020 22
MW-13 27-Apr-16 107.5 5.76 4.24 <2.0 20 68 <0.061 <0.069 44.0 <0.04 8.8 <0.4 5.7 200 240 0.5*<0.50 <1.0 <0.50 <0.50 <0.020 2.8
MW-13 17-Nov-16 92.7 6.20 1.72 <2.0 16 190B <10 <10 49D 0.12 8.1 --4.5 190 410 1.0*<0.10 <0.10 <0.20 <0.10 <0.10 40
MW-13 28-Apr-17 115.4 5.43 1.61 <2.0 16 170B <10 <10 29 0.091 9.1 <1.0 5.5 190 420 0.5*<0.10 <0.10 <0.20 <0.10 <0.10 2.3
MW-14 30-Mar-11 108.1 6.69 2.25 <2 <10 0.57 <1.5 <1.6 6.7 0.76J 4.1J <0.01 0.6 83 20.6 <0.037 <0.083 <0.16 <0.44 <0.18 <0.14 4.5
MW-14 7-Nov-11 18.2 6.78 1.06 6.7 25 299D <1 <2.3 11B 0.036J 4.8J 0.065J 5.5 70 <1.3 0.040 1.5 <0.024 0.069J <0.057 <0.061 0.95
MW-14 3-Apr-12 174.2 6.57 1.04 <2 19 282D <1 <2.3 62B <0.025 3.9JB <0.01 1.8 220D 170D 0.042 <0.04 <0.024 <0.062 0.19 <0.061 9.1
MW-14 5-Nov-12 -78.2 6.40 1.78 4 39 838D <0.2 1.19 55B <0.025 4.6J 0.20J 8.1 120D 13.8 <0.046 <0.031 <0.031 2.30 1.30 <0.010 6.1
MW-14 16-May-13 30.6 6.18 1.11 2.9 <16 7.6 <0.061 <0.069 38.5 <0.03 4.22 <0.4 3.3 140 52 0.8*<0.50 <1.0 <0.50 <0.50 <0.25 5.1
MW-14 7-Nov-13 12.2 6.64 1.55 <4 <16 8.3 <0.061 <0.069 23.4 <0.03 3.09 <0.4 0.7 173 93 0.0*<0.5 <1.0 <0.50 <0.50 <0.25 1.4
MW-14 10-Apr-14 36.8 6.47 2.25 <2 <16 23.0 <0.061 <0.069 25.7 0.16J 3.9 <0.4 1.6 158 --0.0*<0.5 <1.0 <0.50 <0.50 <0.25 2.8
MW-14 28-Oct-14 -7.1 5.64 0.77 5.2 <16 790 0.23 1.0 65.1 <0.03 1.8 0.6JB 4.8 225 56 0.5*<0.5 <1.0 <0.50 <0.50 <0.25 1.1
MW-14 6-May-15 -27.6 6.22 0.91 <2 <16 17 <0.061 <0.069 68.3 0.08J 3.6B <0.4 3.1 214 23 0.5*<0.5 <1.0 <0.50 <0.50 <0.25 4.6
MW-14 20-Nov-15 86.5 5.28 4.49 9.6 <16 730 0.14 0.52 77.7 <0.03 2.6 0.7J 7.2 212 53 0.5*1.0 <1.0 <0.50 <0.50 <0.020 31
MW-14 27-Apr-16 43.6 6.27 1.61 <2.0 <12 130 <0.061 <0.069 87.7 <0.04 4.5 0.4J 2.4 245 49 0.5*<0.50 <1.0 <0.50 <0.50 <0.020 23
MW-14 17-Nov-16 52.0 6.55 1.16 <2.0 8.3 390B <10 <10 76D <0.020 5.6 --1.6 230 310 0.0*<0.10 <0.10 <0.20 <0.10 <0.10 7.5
MW-14 28-Apr-17 53.7 5.95 1.55 3.4 8.4 30B <10 <10 45 0.019J 3.4 <1.0 2.8 180 180 0.0*<0.10 <0.10 <0.20 <0.10 <0.10 3.7
MW-19 5-Apr-12 203.3 7.12 1.15 --<1 ----------------------------------
MW-19 19-Jul-12 -64.2 7.19 0.28 --<1 <0.43 <0.2 <0.54 15 0.2*2*----154*108*0.4*<0.031 <0.031 0.098J <0.063 0.022J --
MW-19 16-Aug-12 -18.4 6.80 0.27 --<10 <0.43 <0.2 <0.54 15 3.7*2*----140*120*0.2*------------
MW-19 6-Nov-12 -21.5 6.71 1.41 --17 7.27 <0.2 1.96 13 4.1*11*----170*140*0.4*------------
MW-19 16-May-13 2.4 6.60 1.08 189 320 33 0.58 0.41 17 <0.03 0.79 1.7J 17.6 148 45 0.4*15 2.4 <0.50 4.9 <0.25 --
MW-19 31-Jul-13 -107.8 6.81 1.21 --29 1,200 0.30 0.69 21.4 <0.03 1.83 ----161 23 1.3*17 <1.0 <0.50 1.1 <0.25 --
MW-19 7-Nov-13 -32.8 7.65 1.19 <2 <16 1,200 1.1 0.084 19.7 0.17J 2.99 <0.4 0.2 157 110 0.5*<0.5 <1.0 <0.50 <0.50 <0.25 --
MW-19 16-Jan-14 -141.9 7.54 0.36 --<16 64 <0.061 <0.069 21.2 <0.03 3.18 ----162 6.9 0.0*<0.50 <1.0 <0.50 <0.50 <0.25 --
MW-19 9-Apr-14 -74.8 7.19 1.24 <2 29 1,800 0.14 0.093 4.6 <0.03 4.9 ----128 76 0.0*1.1 <1.0 <0.50 <0.50 <0.25 --
MW-19 29-Oct-14 -31.2 6.63 1.31 <4 19 730 0.55 1.60 8.9 <0.03 4.3 0.4JB 1.5 124 54 0.0*<0.50 <1.0 <0.50 <0.50 <0.25 --
MW-19 7-May-15 -22.4 7.21 1.38 3.9 <16 95 <0.061 <0.069 4.1 0.08J 7.0B <0.4 1.6 106 46 0.0*<0.50 <1.0 <0.50 <0.50 <0.25 18.0
MW-19 20-Nov-15 194.9 7.51 1.50 <2.0 <16 24 <0.061 <0.069 5.8 <0.03 5.0 <0.4 1.8 87.5 55 1.5*<0.50 <1.0 <0.50 <0.50 <0.020 12
MW-19 26-Apr-16 21.1 7.69 1.94 <2.0 15 12 <0.061 <0.069 8.5 0.05J 6.7 <0.4 1.5 83.5 62 1.5*<0.50 <1.0 <0.50 <0.50 <0.020 260
MW-19 16-Nov-16 -34.7 7.68 1.43 <2.0 13 460B <10 <10 9.6 0.0083J 5.4 <1.0 2.2 95 140 3.5*<0.10 <0.10 <0.20 <0.10 <0.10 7.3
MW-19 27-Apr-17 1.4 7.25 1.47 <2.0 <10 7.6B <10 <10 11 0.015J 4.4 <1.0 1.6 120 140 2.0*<0.10 <0.10 <0.20 <0.10 <0.10 38
Page 2 of 3 June 2017
Table 6
Geochemical Data
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
Permit Number 9203-MSWLF-1980
Monitoring Well CodeSample DateOxidation Reduction Potential (mV)pHDissolved Oxygen Biochemical Oxygen DemandChemical Oxygen DemandMethane (ug/l)Ethane (ug/l)Ethene (ug/l)ChlorideNitrateSulfateSulfideTotal Organic CarbonAlkalinity (CaCO3)Carbon DioxideFerrous IronAcetic AcidButyric AcidLactic AcidPropionic AcidPyruvic AcidDissolved Hydrogen (nM)NS NS NS NS NS NS NS NS NS 10,000 250,000 1,000 NS NS NS NS NS NS NS NS NS NSSolid Waste Section Limit
MW-29 5-Apr-12 113.4 6.54 0.83 --360 221D <1 <2.3 10B 1.9*6.0*----84*268*5.8*------------
MW-29 19-Jul-12 -102.8 6.46 0.18 --27 464D <0.2 <0.54 15 0.8*8*----220*292*4.2*4.5 <0.031 <0.095 1.80 <0.010 --
MW-29 16-Aug-12 -6.4 6.57 0.48 --17 219D <0.2 <0.54 14 2.6*4*----162*204*2.2*------------
MW-29 6-Nov-12 1.6 6.42 1.47 --37 59.8 <0.2 <0.54 13 9.2*14*----208*288*2.4*------------
MW-29 16-May-13 -1.4 5.49 0.98 154 620 300 <0.061 0.41 11.1 <0.03 1.45 8.0 33.8 220 110 10.2*48 1.8J <0.50 21 <0.25 --
MW-29 31-Jul-13 -54.2 6.40 1.85 --81 3,000 0.41 0.34 14.0 <0.03 0.73 ----242 140 11.7*26 <1.0 <0.50 9.1 <0.25 --
MW-29 7-Nov-13 -42.4 6.74 1.21 5.7 55 4,300 0.064 0.071 17.6 <0.03 1.18 0.9J 15 301 6.6 9.8*3 <1.0 <0.50 <0.50 <0.25 --
MW-29 16-Jan-14 -119.2 5.65 0.47 --99 2,400 <0.061 <0.069 5.23 <0.03 7.67 ----49.1 50 1.0*<0.50 <1.0 <0.50 <0.50 <0.25 --
MW-29 9-Apr-14 -23.7 5.63 0.89 13.4 86 4,500 0.098 0.098J 6.30 <0.03 4.4 ----107 79 1.0*<0.50 <1.0 <0.50 <0.50 <0.25 --
MW-29 29-Oct-14 -95.6 6.38 0.41 <70 54 2,700 <0.061 <0.069 11.80 <0.03 2.5 0.8JB 18.6 173 57 1.0*<0.50 <1.0 <0.50 <0.50 <0.25 1.0
MW-29 7-May-15 -39.1 5.72 1.88 5.6 48 120 <0.061 <0.069 8.1 <0.03 4.0B <0.4 8 94 56 0.5*<0.50 <1.0 <0.50 <0.50 <0.25 1.8
MW-29 20-Nov-15 76.7 5.49 2.71 2.1 74 2 <0.061 <0.069 7.0 <0.03 5.0 1.6J 14.4 34.3 32 3.0*<0.50 <1.0 <0.50 <0.50 <0.020 13
MW-29 27-Apr-16 -45.9 6.07 1.94 2.5 54 58 <0.061 <0.069 8.3 <0.04 2.3 <0.8 11.7 58.6 65 2.5*<0.50 <1.0 <0.50 <0.50 <0.020 2.6
MW-29 17-Nov-16 -21.6 6.70 2.02 <2.0 16 260B <10 <10 9.3 0.12JD 1.9 <1.0 4.0 81 140 2.0*<0.10 <0.10 <0.20 <0.10 <0.10 7.5
MW-29 27-Apr-17 5.0 5.59 2.13 2.7 72 7.6B <10 <10 6.5 0.011J 2.0 0.80J 18 36 73 2.5*<0.10 <0.10 <0.20 <0.10 <0.10 2.2
Notes:
1. All units are in milligrams per liter (parts per million), unless otherwise noted.
2. ug/L - micrograms per liter
3. -- Not analyzed for
4. J - The analytical result is an estimated concentration between the laboratory method detection limit and the Solid Waste Section reporting limit.
5. D - The sample was analyzed at dilution.
6. B - The analyte was detected in the associated method blank.
7. mV - millivolt
8. nM - nanomoles per liter
9. * - Field analysis performed using a HACH kit.
- A sodium lactate injection was performed near MW-8, -9, and -10 on June 18-21, 2012.
- An emulsified vegetable oil injection was performed near MW-8, -9, and -10 on March 25-27, 2013.
Page 3 of 3 June 2017
Figure 2
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
0
20
40
60
80
100
120
140
160
Total detected VOC (ppb)Date
MW-8 Total Detected VOCs
MSW Closed 1998C&D Closed 2005LFG RecoverySystem on-line 2011Insitu bioremediation implementation June 2012Insitu bioremediation implementation March2013Note:Acetone was omitted as it is a common laboratory contaminant.
Figure 3
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
0
20
40
60
80
100
120
140
160
180
Total detected VOC (ppb)Date
MW-9 Total Detected VOCs
MSW Closed 1998C&D Closed 2005LFG RecoverySystem on-line 2011Insitu bioremediation implementation June 2012Insitu bioremediation implementation March2013Note:Acetone was omitted as it is a common laboratory contaminant.
Figure 4
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
0
100
200
300
400
500
600
Total detected VOC (ppb)Date
MW-10 Total Detected VOCs
MSW Closed 1998C&D Closed 2005LFG RecoverySystem on-line 2011Insitu bioremediation implementation June 2012Insitu bioremediation implementation March2013Note:Acetone was omitted as it is a common laboratory contaminant.
Figure 5
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
0
1
2
3
4
5
6
7
8
Total detected VOC (ppb)Date
MW-12 Total Detected VOCs
MSW Closed 1998C&D Closed 2005LFG RecoverySystem on-line 2011Note:Acetone was omitted as it is a common laboratory contaminant.
Figure 6
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
0
5
10
15
20
25
30
Total detected VOC (ppb)Date
MW-13 Total Detected VOCs
MSW Closed 1998C&D Closed 2005LFG RecoverySystem on-line 2011Note:Acetone was omitted as it is a common laboratory contaminant.
Figure 7
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
0
2
4
6
8
10
12
Total detected VOC (ppb)Date
MW-14 Total Detected VOCs
MSW Closed 1998C&D Closed 2005LFG RecoverySystem on-line 2011Note:Acetone was omitted as it is a common laboratory contaminant.
Figure 8
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
0
2
4
6
8
10
12
14
16
18
Total detected VOC (ppb)Date
MW-15 Total Detected VOCs
MSW Closed 1998C&D Closed 2005LFG RecoverySystem on-line 2011Note:Acetone was omitted as it is a common laboratory contaminant.
Figure 9
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
0
5
10
15
20
25
30
35
Total detected VOC (ppb)Date
MW-16 Total Detected VOCs
MSW Closed 1998C&D Closed 2005LFG RecoverySystem on-line 2011Note:Acetone was omitted as it is a common laboratory contaminant.
Figure 10
April 2017 Semi-Annual Sampling Event
Feltonsville Landfill - Wake County
0
5
10
15
20
25
30
35
Total detected VOC (ppb)Date
MW-29 Total Detected VOCs
LFG RecoverySystem on-line 2011Insitu bioremediation implementation June 2012Insitu bioremediation implementation March2013Note:Acetone was omitted as it is a common laboratory contaminant.
Appendix A
Analytical Data
SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
CDM Smith
5400 Glenwood Avenue
Suite 400
Raleigh, NC 27612
Attention: Mathew Colone
SD28007Lot Number:
Feltonsville LandfillProject Name:
05/11/2017Date Completed:
Catherine S. Dover
Project Manager
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
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SHEALY ENVIRONMENTAL SERVICES, INC.
Case Narrative
CDM Smith
Lot Number: SD28007
SC DHEC No: 32010 NC Field Parameters No: 5639 NELAC No: E87653 NC DENR No: 329
Project Name: Feltonsville Landfill
Project Number:
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
VOC 8260B
The continuing calibration verification (CCV) associated with samples SD28007-009 (MW-20), SD28007-010 (MW-24), SD28007-011 (MW-25),
SD28007-012 (MW-28), SD28007-013 (MW-29), SD28007-014 (DUP),for analytes: DCDFM, Acetone and Acrylonitrile recovered above the upper
control limit. The samples associated with this CCV were non-detect for the affected analytes; therefore, the data has been reported except for
sample SD28010-003 (MW-9) for Acetone and SD28020-006 (MW-16) for DCDFM. Both of these samples were re-analyzed for affected target
analytes and reported.
Nitrate
Sample SD28007-005 (MW-12) was diluted due to the nature of the sample matrix (high chloride). The LOQ has been elevated to reflect the dilution.
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SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
CDM Smith
Lot Number: SD28007
Project Name: Feltonsville Landfill
Project Number:
Sample Number Sample ID Matrix Date Sampled Date Received
001 04/27/2017 1020MW-2 Aqueous 04/28/2017
002 04/27/2017 1700MW-6 Aqueous 04/28/2017
003 04/27/2017 1300MW-9 Aqueous 04/28/2017
004 04/27/2017 1405MW-10 Aqueous 04/28/2017
005 04/27/2017 1615MW-12 Aqueous 04/28/2017
006 04/27/2017 1505MW-16 Aqueous 04/28/2017
007 04/27/2017 1710MW-18 Aqueous 04/28/2017
008 04/27/2017 1320MW-19 Aqueous 04/28/2017
009 04/27/2017 1715MW-20 Aqueous 04/28/2017
010 04/27/2017 1630MW-24 Aqueous 04/28/2017
011 04/27/2017 1645MW-25 Aqueous 04/28/2017
012 04/27/2017 1650MW-28 Aqueous 04/28/2017
013 04/27/2017 1100MW-29 Aqueous 04/28/2017
014 04/27/2017 0800DUPAqueous 04/28/2017
(14 samples)
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Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-2
SD28007-001
04/27/2017 1020
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 05/02/2017 1650 BWS 40944
1 (BOD, 5 day) SM 5210B-2011 1 05/03/2017 0948 AMM1 04/28/2017 1312 11310
1 (Chloride) 300.0 10 04/28/2017 1541 TAF 40901
1 (CO2 (calcula) SM 4500-CO2 D 1 05/02/2017 1650 BWS
1 (COD) SM 5220D-2011 1 05/06/2017 1117 TAF 05/04/2017 1037
1 (Nitrate - N) 300.0 10 04/28/2017 1541 TAF 40795
1 (Sulfate) 300.0 10 04/28/2017 1541 TAF 41004
1 (Sulfide) SM 4500-S2 F-2011 1 05/01/2017 1623 BWS 40932
1 (TOC) SM 5310C-2011 1 05/01/2017 1935 BWS 40876
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Alkalinity SM 2320B-20 170 1mg/L2.010
BOD, 5 day SM 5210B-20 2.0 U 1mg/L0.182.0
Chloride 300.0 730 D 1mg/L2.010
CO2 (calculation)124-38-9 SM 4500-CO2 160 1mg/L27
COD SM 5220D-20 20 1mg/L8.010
Nitrate - N 300.0 0.20 D 1mg/L0.0500.20
Sulfate 300.0 14 D 1mg/L2.010
Sulfide 18496-25-8 SM 4500-S2 1.0 U 1mg/L0.621.0
TOC SM 5310C-20 4.7 1mg/L0.601.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
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Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-2
SD28007-001
04/27/2017 1020
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/28/2017 2232 ECP 40810
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 1.2 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
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Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-2
SD28007-001
04/27/2017 1020
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/28/2017 2232 ECP 40810
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 101 70-130
1,2-Dichloroethane-d4 105 70-130
Toluene-d8 103 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
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Dissolved Gases
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-2
SD28007-001
04/27/2017 1020
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 05/03/2017 1426 TML 41108
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Ethane 74-84-0 RSK - 175 10 U 1ug/L2.510
Ethene 74-85-1 RSK - 175 10 U 1ug/L2.510
Methane 74-82-8 RSK - 175 2.8 BJ 1ug/L2.510
Propane 74-98-6 RSK - 175 15 U 1ug/L3.515
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
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ICP-MS Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-2
SD28007-001
04/27/2017 1020
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 05/02/2017 2347 BNW 04/28/2017 1749 40785
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020B 6.0 U 1ug/L0.506.0
Arsenic 7440-38-2 6020B 2.1 J 1ug/L1.310
Barium 7440-39-3 6020B 160 1ug/L0.63100
Beryllium 7440-41-7 6020B 1.0 U 1ug/L0.131.0
Cadmium 7440-43-9 6020B 1.0 U 1ug/L0.131.0
Chromium 7440-47-3 6020B 10 U 1ug/L1.310
Cobalt 7440-48-4 6020B 10 U 1ug/L0.6310
Copper 7440-50-8 6020B 0.97 J 1ug/L0.6310
Lead 7439-92-1 6020B 0.28 J 1ug/L0.2510
Nickel 7440-02-0 6020B 2.8 J 1ug/L1.350
Selenium 7782-49-2 6020B 9.4 J 1ug/L1.310
Silver 7440-22-4 6020B 10 U 1ug/L0.2510
Thallium 7440-28-0 6020B 5.5 U 1ug/L0.135.5
Vanadium 7440-62-2 6020B 9.6 J 1ug/L1.525
Zinc 7440-66-6 6020B 10 U 1ug/L2.510
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 8 of 130
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Shealy Environmental Services, Inc.
CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-2
SD28007-001
04/27/2017 1020
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 05/01/2017 1857 COH 05/01/2017 1334 40848
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Mercury 7439-97-6 7470A 0.00010 U 1mg/L0.0000280.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 9 of 130
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-6
SD28007-002
04/27/2017 1700
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/28/2017 2254 ECP 40810
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 1.7 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.91 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.58 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 5.4 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.77 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 10 of 130
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-6
SD28007-002
04/27/2017 1700
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/28/2017 2254 ECP 40810
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 104 70-130
1,2-Dichloroethane-d4 105 70-130
Toluene-d8 102 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 11 of 130
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Shealy Environmental Services, Inc.
ICP-MS Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-6
SD28007-002
04/27/2017 1700
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 05/03/2017 0014 BNW 04/28/2017 1749 40785
2 3005A 6020B 2 05/04/2017 0939 BNW 04/28/2017 1749 40785
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020B 6.0 U 1ug/L0.506.0
Arsenic 7440-38-2 6020B 10 U 1ug/L1.310
Barium 7440-39-3 6020B 620 D 2ug/L1.3200
Beryllium 7440-41-7 6020B 1.0 U 1ug/L0.131.0
Cadmium 7440-43-9 6020B 0.67 J 1ug/L0.131.0
Chromium 7440-47-3 6020B 10 U 1ug/L1.310
Cobalt 7440-48-4 6020B 13 1ug/L0.6310
Copper 7440-50-8 6020B 4.3 J 1ug/L0.6310
Lead 7439-92-1 6020B 10 U 1ug/L0.2510
Nickel 7440-02-0 6020B 19 J 1ug/L1.350
Selenium 7782-49-2 6020B 1.8 J 1ug/L1.310
Silver 7440-22-4 6020B 10 U 1ug/L0.2510
Thallium 7440-28-0 6020B 5.5 U 1ug/L0.135.5
Vanadium 7440-62-2 6020B 3.6 J 1ug/L1.525
Zinc 7440-66-6 6020B 25 1ug/L2.510
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 12 of 130
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Shealy Environmental Services, Inc.
CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-6
SD28007-002
04/27/2017 1700
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 05/01/2017 1859 COH 05/01/2017 1334 40848
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Mercury 7439-97-6 7470A 0.00010 U 1mg/L0.0000280.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 13 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-9
SD28007-003
04/27/2017 1300
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 05/02/2017 1703 BWS 40944
1 (BOD, 5 day) SM 5210B-2011 1 05/03/2017 0948 AMM1 04/28/2017 1312 11310
1 (Chloride) 300.0 5 04/28/2017 1553 TAF 40901
1 (CO2 (calcula) SM 4500-CO2 D 1 05/02/2017 1703 BWS
1 (COD) SM 5220D-2011 1 05/06/2017 1117 TAF 05/04/2017 1037
2 (Nitrate - N) 300.0 1 04/29/2017 1125 TAF 40902
2 (Sulfate) 300.0 1 04/29/2017 1125 TAF 41010
1 (Sulfide) SM 4500-S2 F-2011 1 05/01/2017 1623 BWS 40932
1 (TDS) SM 2540C-2011 1 05/01/2017 1544 MGM 40849
1 (TOC) SM 5310C-2011 1 05/01/2017 2025 BWS 40876
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Alkalinity SM 2320B-20 320 1mg/L2.010
BOD, 5 day SM 5210B-20 17 1mg/L0.182.0
Chloride 300.0 42 D 1mg/L1.05.0
CO2 (calculation)124-38-9 SM 4500-CO2 360 1mg/L27
COD SM 5220D-20 21 1mg/L8.010
Nitrate - N 300.0 0.025 2mg/L0.00500.020
Sulfate 300.0 1.0 U 2mg/L0.201.0
Sulfide 18496-25-8 SM 4500-S2 1.0 U 1mg/L0.621.0
TDS SM 2540C-20 420 1mg/L3.410
TOC SM 5310C-20 6.1 1mg/L0.601.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 14 of 130
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-9
SD28007-003
04/27/2017 1300
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/28/2017 2316 ECP 40810
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 1.1 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 13 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.87 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 12 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.67 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.40 J 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 15 of 130
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-9
SD28007-003
04/27/2017 1300
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/28/2017 2316 ECP 40810
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 2.0 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 103 70-130
1,2-Dichloroethane-d4 104 70-130
Toluene-d8 102 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 16 of 130
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Shealy Environmental Services, Inc.
Dissolved Gases
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-9
SD28007-003
04/27/2017 1300
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 10 05/03/2017 1400 TML 41108
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Ethane 74-84-0 RSK - 175 100 U 1ug/L25100
Ethene 74-85-1 RSK - 175 100 U 1ug/L25100
Methane 74-82-8 RSK - 175 11000 BD 1ug/L25100
Propane 74-98-6 RSK - 175 150 U 1ug/L35150
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 17 of 130
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Shealy Environmental Services, Inc.
ICP-MS Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-9
SD28007-003
04/27/2017 1300
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 05/03/2017 0019 BNW 04/28/2017 1749 40785
2 3005A 6020B 5 05/04/2017 0944 BNW 04/28/2017 1749 40785
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020B 6.0 U 1ug/L0.506.0
Arsenic 7440-38-2 6020B 5.1 J 1ug/L1.310
Barium 7440-39-3 6020B 950 D 2ug/L3.1500
Beryllium 7440-41-7 6020B 0.18 J 1ug/L0.131.0
Cadmium 7440-43-9 6020B 1.0 U 1ug/L0.131.0
Chromium 7440-47-3 6020B 1.4 J 1ug/L1.310
Cobalt 7440-48-4 6020B 12 1ug/L0.6310
Copper 7440-50-8 6020B 14 1ug/L0.6310
Lead 7439-92-1 6020B 8.3 J 1ug/L0.2510
Nickel 7440-02-0 6020B 32 J 1ug/L1.350
Selenium 7782-49-2 6020B 10 U 1ug/L1.310
Silver 7440-22-4 6020B 10 U 1ug/L0.2510
Sodium 7440-23-5 6020B 21000 1ug/L50400
Thallium 7440-28-0 6020B 5.5 U 1ug/L0.135.5
Vanadium 7440-62-2 6020B 3.3 J 1ug/L1.525
Zinc 7440-66-6 6020B 5.5 J 1ug/L2.510
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 18 of 130
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Shealy Environmental Services, Inc.
CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-9
SD28007-003
04/27/2017 1300
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 05/01/2017 1902 COH 05/01/2017 1334 40848
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Mercury 7439-97-6 7470A 0.000041 J 1mg/L0.0000280.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 19 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-10
SD28007-004
04/27/2017 1405
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 05/02/2017 1710 BWS 40944
1 (BOD, 5 day) SM 5210B-2011 1 05/03/2017 0948 AMM1 04/28/2017 1312 11310
1 (Chloride) 300.0 5 04/28/2017 1605 TAF 40901
1 (CO2 (calcula) SM 4500-CO2 D 1 05/02/2017 1710 BWS
1 (COD) SM 5220D-2011 1 05/06/2017 1117 TAF 05/04/2017 1037
2 (Nitrate - N) 300.0 1 04/29/2017 1137 TAF 40902
2 (Sulfate) 300.0 1 04/29/2017 1137 TAF 41010
1 (Sulfide) SM 4500-S2 F-2011 1 05/01/2017 1623 BWS 40932
1 (TDS) SM 2540C-2011 1 05/01/2017 1544 MGM 40849
1 (TOC) SM 5310C-2011 1 05/01/2017 2041 BWS 40876
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Alkalinity SM 2320B-20 200 1mg/L2.010
BOD, 5 day SM 5210B-20 4.3 1mg/L0.182.0
Chloride 300.0 64 D 1mg/L1.05.0
CO2 (calculation)124-38-9 SM 4500-CO2 440 1mg/L27
COD SM 5220D-20 39 1mg/L8.010
Nitrate - N 300.0 0.0071 J 2mg/L0.00500.020
Sulfate 300.0 5.0 2mg/L0.201.0
Sulfide 18496-25-8 SM 4500-S2 1.0 U 1mg/L0.621.0
TDS SM 2540C-20 350 1mg/L3.410
TOC SM 5310C-20 10 1mg/L0.601.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 20 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-10
SD28007-004
04/27/2017 1405
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/28/2017 2337 ECP 40810
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 7.1 J 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 2.4 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.40 J 1ug/L0.400.50
Chloroethane 75-00-3 8260B 9.6 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 2.8 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 23 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.40 J 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 21 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-10
SD28007-004
04/27/2017 1405
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/28/2017 2337 ECP 40810
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 2.2 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 105 70-130
1,2-Dichloroethane-d4 104 70-130
Toluene-d8 104 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 22 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Dissolved Gases
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-10
SD28007-004
04/27/2017 1405
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 RSK - 175 1 05/05/2017 1510 TML 41344
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Ethane 74-84-0 RSK - 175 10 U 2ug/L2.510
Ethene 74-85-1 RSK - 175 10 U 2ug/L2.510
Methane 74-82-8 RSK - 175 2900 B 2ug/L2.510
Propane 74-98-6 RSK - 175 15 U 2ug/L3.515
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 23 of 130
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Shealy Environmental Services, Inc.
ICP-MS Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-10
SD28007-004
04/27/2017 1405
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 05/03/2017 0035 BNW 04/28/2017 1749 40785
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020B 6.0 U 1ug/L0.506.0
Arsenic 7440-38-2 6020B 23 1ug/L1.310
Barium 7440-39-3 6020B 350 1ug/L0.63100
Beryllium 7440-41-7 6020B 0.14 J 1ug/L0.131.0
Cadmium 7440-43-9 6020B 1.0 U 1ug/L0.131.0
Chromium 7440-47-3 6020B 10 U 1ug/L1.310
Cobalt 7440-48-4 6020B 11 1ug/L0.6310
Copper 7440-50-8 6020B 3.5 J 1ug/L0.6310
Lead 7439-92-1 6020B 0.40 J 1ug/L0.2510
Nickel 7440-02-0 6020B 13 J 1ug/L1.350
Selenium 7782-49-2 6020B 10 U 1ug/L1.310
Silver 7440-22-4 6020B 10 U 1ug/L0.2510
Sodium 7440-23-5 6020B 40000 1ug/L50400
Thallium 7440-28-0 6020B 5.5 U 1ug/L0.135.5
Vanadium 7440-62-2 6020B 2.1 J 1ug/L1.525
Zinc 7440-66-6 6020B 2.8 J 1ug/L2.510
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 24 of 130
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Shealy Environmental Services, Inc.
CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-10
SD28007-004
04/27/2017 1405
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 05/01/2017 1904 COH 05/01/2017 1334 40848
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Mercury 7439-97-6 7470A 0.00010 U 1mg/L0.0000280.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 25 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-12
SD28007-005
04/27/2017 1615
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 05/02/2017 1721 BWS 40944
1 (BOD, 5 day) SM 5210B-2011 1 05/03/2017 0948 AMM1 04/28/2017 1312 11310
1 (Chloride) 300.0 5 04/28/2017 1617 TAF 40901
1 (CO2 (calcula) SM 4500-CO2 D 1 05/02/2017 1721 BWS
1 (COD) SM 5220D-2011 1 05/06/2017 1117 TAF 05/04/2017 1037
2 (Nitrate - N) 300.0 2 04/29/2017 1238 TAF 40902
2 (Sulfate) 300.0 2 04/29/2017 1238 TAF 41010
1 (Sulfide) SM 4500-S2 F-2011 1 05/01/2017 1623 BWS 40932
1 (TOC) SM 5310C-2011 1 05/01/2017 2058 BWS 40876
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Alkalinity SM 2320B-20 610 1mg/L2.010
BOD, 5 day SM 5210B-20 2.0 U 1mg/L0.182.0
Chloride 300.0 220 D 1mg/L1.05.0
CO2 (calculation)124-38-9 SM 4500-CO2 600 1mg/L27
COD SM 5220D-20 15 1mg/L8.010
Nitrate - N 300.0 0.040 U 2mg/L0.0100.040
Sulfate 300.0 16 D 2mg/L0.402.0
Sulfide 18496-25-8 SM 4500-S2 1.0 U 1mg/L0.621.0
TOC SM 5310C-20 5.2 1mg/L0.601.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 26 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-12
SD28007-005
04/27/2017 1615
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/28/2017 2359 ECP 40810
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 27 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-12
SD28007-005
04/27/2017 1615
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/28/2017 2359 ECP 40810
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 104 70-130
1,2-Dichloroethane-d4 105 70-130
Toluene-d8 105 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 28 of 130
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Shealy Environmental Services, Inc.
Dissolved Gases
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-12
SD28007-005
04/27/2017 1615
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 05/03/2017 1439 TML 41108
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Ethane 74-84-0 RSK - 175 10 U 1ug/L2.510
Ethene 74-85-1 RSK - 175 10 U 1ug/L2.510
Methane 74-82-8 RSK - 175 21 B 1ug/L2.510
Propane 74-98-6 RSK - 175 15 U 1ug/L3.515
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 29 of 130
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Shealy Environmental Services, Inc.
ICP-MS Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-12
SD28007-005
04/27/2017 1615
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 05/03/2017 0041 BNW 04/28/2017 1749 40785
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020B 6.0 U 1ug/L0.506.0
Arsenic 7440-38-2 6020B 3.9 J 1ug/L1.310
Barium 7440-39-3 6020B 260 1ug/L0.63100
Beryllium 7440-41-7 6020B 1.0 U 1ug/L0.131.0
Cadmium 7440-43-9 6020B 1.0 U 1ug/L0.131.0
Chromium 7440-47-3 6020B 10 U 1ug/L1.310
Cobalt 7440-48-4 6020B 10 U 1ug/L0.6310
Copper 7440-50-8 6020B 0.82 J 1ug/L0.6310
Lead 7439-92-1 6020B 10 U 1ug/L0.2510
Nickel 7440-02-0 6020B 4.2 J 1ug/L1.350
Selenium 7782-49-2 6020B 5.9 J 1ug/L1.310
Silver 7440-22-4 6020B 10 U 1ug/L0.2510
Thallium 7440-28-0 6020B 5.5 U 1ug/L0.135.5
Vanadium 7440-62-2 6020B 25 U 1ug/L1.525
Zinc 7440-66-6 6020B 10 U 1ug/L2.510
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 30 of 130
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Shealy Environmental Services, Inc.
CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-12
SD28007-005
04/27/2017 1615
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 05/01/2017 1906 COH 05/01/2017 1334 40848
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Mercury 7439-97-6 7470A 0.000049 J 1mg/L0.0000280.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 31 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-16
SD28007-006
04/27/2017 1505
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/29/2017 0021 ECP 40810
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.91 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 1.3 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 1.6 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 6.2 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 3.8 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 1.7 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 32 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-16
SD28007-006
04/27/2017 1505
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/29/2017 0021 ECP 40810
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 107 70-130
1,2-Dichloroethane-d4 110 70-130
Toluene-d8 105 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 33 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
ICP-MS Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-16
SD28007-006
04/27/2017 1505
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 05/03/2017 0046 BNW 04/28/2017 1749 40785
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020B 6.0 U 1ug/L0.506.0
Arsenic 7440-38-2 6020B 13 1ug/L1.310
Barium 7440-39-3 6020B 230 1ug/L0.63100
Beryllium 7440-41-7 6020B 1.0 U 1ug/L0.131.0
Cadmium 7440-43-9 6020B 1.0 U 1ug/L0.131.0
Chromium 7440-47-3 6020B 10 U 1ug/L1.310
Cobalt 7440-48-4 6020B 2.0 J 1ug/L0.6310
Copper 7440-50-8 6020B 1.0 J 1ug/L0.6310
Lead 7439-92-1 6020B 0.28 J 1ug/L0.2510
Nickel 7440-02-0 6020B 3.9 J 1ug/L1.350
Selenium 7782-49-2 6020B 10 U 1ug/L1.310
Silver 7440-22-4 6020B 10 U 1ug/L0.2510
Thallium 7440-28-0 6020B 5.5 U 1ug/L0.135.5
Vanadium 7440-62-2 6020B 25 U 1ug/L1.525
Zinc 7440-66-6 6020B 3.1 J 1ug/L2.510
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 34 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-16
SD28007-006
04/27/2017 1505
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 05/02/2017 0941 COH 05/01/2017 1334 40848
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Mercury 7439-97-6 7470A 0.00010 U 1mg/L0.0000280.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 35 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-18
SD28007-007
04/27/2017 1710
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/29/2017 0042 ECP 40810
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 36 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-18
SD28007-007
04/27/2017 1710
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/29/2017 0042 ECP 40810
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 103 70-130
1,2-Dichloroethane-d4 106 70-130
Toluene-d8 104 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 37 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
ICP-MS Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-18
SD28007-007
04/27/2017 1710
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 05/03/2017 0051 BNW 04/28/2017 1749 40785
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020B 6.0 U 1ug/L0.506.0
Arsenic 7440-38-2 6020B 3.2 J 1ug/L1.310
Barium 7440-39-3 6020B 110 1ug/L0.63100
Beryllium 7440-41-7 6020B 0.14 J 1ug/L0.131.0
Cadmium 7440-43-9 6020B 1.0 U 1ug/L0.131.0
Chromium 7440-47-3 6020B 3.2 J 1ug/L1.310
Cobalt 7440-48-4 6020B 2.3 J 1ug/L0.6310
Copper 7440-50-8 6020B 5.6 J 1ug/L0.6310
Lead 7439-92-1 6020B 1.9 J 1ug/L0.2510
Nickel 7440-02-0 6020B 23 J 1ug/L1.350
Selenium 7782-49-2 6020B 3.7 J 1ug/L1.310
Silver 7440-22-4 6020B 10 U 1ug/L0.2510
Thallium 7440-28-0 6020B 5.5 U 1ug/L0.135.5
Vanadium 7440-62-2 6020B 6.9 J 1ug/L1.525
Zinc 7440-66-6 6020B 16 1ug/L2.510
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 38 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-18
SD28007-007
04/27/2017 1710
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 05/02/2017 1000 COH 05/01/2017 1334 40848
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Mercury 7439-97-6 7470A 0.000034 J 1mg/L0.0000280.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 39 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-19
SD28007-008
04/27/2017 1320
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 05/02/2017 1726 BWS 40944
1 (BOD, 5 day) SM 5210B-2011 1 05/03/2017 0948 AMM1 04/28/2017 1312 11310
1 (Chloride) 300.0 1 04/28/2017 1630 TAF 40901
1 (CO2 (calcula) SM 4500-CO2 D 1 05/02/2017 1726 BWS
1 (COD) SM 5220D-2011 1 05/06/2017 1117 TAF 05/04/2017 1037
1 (Nitrate - N) 300.0 1 04/28/2017 1630 TAF 40795
1 (Sulfate) 300.0 1 04/28/2017 1630 TAF 41004
1 (Sulfide) SM 4500-S2 F-2011 1 05/01/2017 1623 BWS 40932
1 (TDS) SM 2540C-2011 1 05/01/2017 1544 MGM 40849
1 (TOC) SM 5310C-2011 1 05/01/2017 2114 BWS 40876
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Alkalinity SM 2320B-20 120 1mg/L2.010
BOD, 5 day SM 5210B-20 2.0 U 1mg/L0.182.0
Chloride 300.0 11 1mg/L0.201.0
CO2 (calculation)124-38-9 SM 4500-CO2 140 1mg/L27
COD SM 5220D-20 10 U 1mg/L8.010
Nitrate - N 300.0 0.015 J 1mg/L0.00500.020
Sulfate 300.0 4.4 1mg/L0.201.0
Sulfide 18496-25-8 SM 4500-S2 1.0 U 1mg/L0.621.0
TDS SM 2540C-20 170 1mg/L3.410
TOC SM 5310C-20 1.6 1mg/L0.601.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 40 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-19
SD28007-008
04/27/2017 1320
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/29/2017 0104 ECP 40810
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.54 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 41 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-19
SD28007-008
04/27/2017 1320
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/29/2017 0104 ECP 40810
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 103 70-130
1,2-Dichloroethane-d4 107 70-130
Toluene-d8 102 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 42 of 130
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Shealy Environmental Services, Inc.
Dissolved Gases
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-19
SD28007-008
04/27/2017 1320
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 05/03/2017 1452 TML 41108
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Ethane 74-84-0 RSK - 175 10 U 1ug/L2.510
Ethene 74-85-1 RSK - 175 10 U 1ug/L2.510
Methane 74-82-8 RSK - 175 7.6 BJ 1ug/L2.510
Propane 74-98-6 RSK - 175 15 U 1ug/L3.515
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 43 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
ICP-MS Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-19
SD28007-008
04/27/2017 1320
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 05/03/2017 0057 BNW 04/28/2017 1749 40785
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020B 6.0 U 1ug/L0.506.0
Arsenic 7440-38-2 6020B 10 U 1ug/L1.310
Barium 7440-39-3 6020B 170 1ug/L0.63100
Beryllium 7440-41-7 6020B 1.0 U 1ug/L0.131.0
Cadmium 7440-43-9 6020B 1.0 U 1ug/L0.131.0
Chromium 7440-47-3 6020B 1.6 J 1ug/L1.310
Cobalt 7440-48-4 6020B 2.5 J 1ug/L0.6310
Copper 7440-50-8 6020B 6.0 J 1ug/L0.6310
Lead 7439-92-1 6020B 0.34 J 1ug/L0.2510
Nickel 7440-02-0 6020B 9.5 J 1ug/L1.350
Selenium 7782-49-2 6020B 10 U 1ug/L1.310
Silver 7440-22-4 6020B 10 U 1ug/L0.2510
Sodium 7440-23-5 6020B 18000 1ug/L50400
Thallium 7440-28-0 6020B 5.5 U 1ug/L0.135.5
Vanadium 7440-62-2 6020B 4.7 J 1ug/L1.525
Zinc 7440-66-6 6020B 6.2 J 1ug/L2.510
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 44 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-19
SD28007-008
04/27/2017 1320
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 05/02/2017 1002 COH 05/01/2017 1334 40848
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Mercury 7439-97-6 7470A 0.000048 J 1mg/L0.0000280.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 45 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-20
SD28007-009
04/27/2017 1715
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/01/2017 1112 ALL 40863
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 2.4 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 46 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-20
SD28007-009
04/27/2017 1715
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/01/2017 1112 ALL 40863
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 104 70-130
1,2-Dichloroethane-d4 106 70-130
Toluene-d8 104 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 47 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
ICP-MS Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-20
SD28007-009
04/27/2017 1715
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 05/03/2017 0102 BNW 04/28/2017 1749 40785
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020B 6.0 U 1ug/L0.506.0
Arsenic 7440-38-2 6020B 2.0 J 1ug/L1.310
Barium 7440-39-3 6020B 110 1ug/L0.63100
Beryllium 7440-41-7 6020B 1.0 U 1ug/L0.131.0
Cadmium 7440-43-9 6020B 1.0 U 1ug/L0.131.0
Chromium 7440-47-3 6020B 10 U 1ug/L1.310
Cobalt 7440-48-4 6020B 10 U 1ug/L0.6310
Copper 7440-50-8 6020B 0.82 J 1ug/L0.6310
Lead 7439-92-1 6020B 10 U 1ug/L0.2510
Nickel 7440-02-0 6020B 1.6 J 1ug/L1.350
Selenium 7782-49-2 6020B 10 U 1ug/L1.310
Silver 7440-22-4 6020B 10 U 1ug/L0.2510
Thallium 7440-28-0 6020B 5.5 U 1ug/L0.135.5
Vanadium 7440-62-2 6020B 3.9 J 1ug/L1.525
Zinc 7440-66-6 6020B 10 U 1ug/L2.510
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 48 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-20
SD28007-009
04/27/2017 1715
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 05/02/2017 1004 COH 05/01/2017 1334 40848
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Mercury 7439-97-6 7470A 0.00010 U 1mg/L0.0000280.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 49 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-24
SD28007-010
04/27/2017 1630
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/01/2017 1134 ALL 40863
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 1.3 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 50 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-24
SD28007-010
04/27/2017 1630
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/01/2017 1134 ALL 40863
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 99 70-130
1,2-Dichloroethane-d4 104 70-130
Toluene-d8 102 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 51 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
ICP-MS Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-24
SD28007-010
04/27/2017 1630
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 05/03/2017 0108 BNW 04/28/2017 1749 40785
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020B 6.0 U 1ug/L0.506.0
Arsenic 7440-38-2 6020B 17 1ug/L1.310
Barium 7440-39-3 6020B 330 1ug/L0.63100
Beryllium 7440-41-7 6020B 1.0 U 1ug/L0.131.0
Cadmium 7440-43-9 6020B 1.0 U 1ug/L0.131.0
Chromium 7440-47-3 6020B 10 U 1ug/L1.310
Cobalt 7440-48-4 6020B 6.5 J 1ug/L0.6310
Copper 7440-50-8 6020B 0.84 J 1ug/L0.6310
Lead 7439-92-1 6020B 0.26 J 1ug/L0.2510
Nickel 7440-02-0 6020B 25 J 1ug/L1.350
Selenium 7782-49-2 6020B 7.3 J 1ug/L1.310
Silver 7440-22-4 6020B 10 U 1ug/L0.2510
Thallium 7440-28-0 6020B 5.5 U 1ug/L0.135.5
Vanadium 7440-62-2 6020B 2.0 J 1ug/L1.525
Zinc 7440-66-6 6020B 3.7 J 1ug/L2.510
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 52 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-24
SD28007-010
04/27/2017 1630
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 05/02/2017 1007 COH 05/01/2017 1334 40848
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Mercury 7439-97-6 7470A 0.00010 U 1mg/L0.0000280.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 53 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-25
SD28007-011
04/27/2017 1645
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/01/2017 1155 ALL 40863
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 1.4 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 2.6 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 54 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-25
SD28007-011
04/27/2017 1645
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/01/2017 1155 ALL 40863
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 108 70-130
1,2-Dichloroethane-d4 110 70-130
Toluene-d8 107 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 55 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
ICP-MS Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-25
SD28007-011
04/27/2017 1645
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 05/03/2017 0113 BNW 04/28/2017 1749 40785
2 3005A 6020B 5 05/04/2017 0949 BNW 04/28/2017 1749 40785
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020B 6.0 U 1ug/L0.506.0
Arsenic 7440-38-2 6020B 2.0 J 1ug/L1.310
Barium 7440-39-3 6020B 890 D 2ug/L3.1500
Beryllium 7440-41-7 6020B 1.0 U 1ug/L0.131.0
Cadmium 7440-43-9 6020B 1.0 U 1ug/L0.131.0
Chromium 7440-47-3 6020B 10 U 1ug/L1.310
Cobalt 7440-48-4 6020B 10 U 1ug/L0.6310
Copper 7440-50-8 6020B 1.3 J 1ug/L0.6310
Lead 7439-92-1 6020B 10 U 1ug/L0.2510
Nickel 7440-02-0 6020B 13 J 1ug/L1.350
Selenium 7782-49-2 6020B 4.8 J 1ug/L1.310
Silver 7440-22-4 6020B 10 U 1ug/L0.2510
Thallium 7440-28-0 6020B 5.5 U 1ug/L0.135.5
Vanadium 7440-62-2 6020B 1.7 J 1ug/L1.525
Zinc 7440-66-6 6020B 5.5 J 1ug/L2.510
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 56 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-25
SD28007-011
04/27/2017 1645
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 05/02/2017 1009 COH 05/01/2017 1334 40848
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Mercury 7439-97-6 7470A 0.00010 U 1mg/L0.0000280.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 57 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-28
SD28007-012
04/27/2017 1650
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/01/2017 1217 ALL 40863
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.55 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.53 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 58 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-28
SD28007-012
04/27/2017 1650
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/01/2017 1217 ALL 40863
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 106 70-130
1,2-Dichloroethane-d4 109 70-130
Toluene-d8 106 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 59 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
ICP-MS Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-28
SD28007-012
04/27/2017 1650
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 05/03/2017 0118 BNW 04/28/2017 1749 40785
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020B 6.0 U 1ug/L0.506.0
Arsenic 7440-38-2 6020B 2.4 J 1ug/L1.310
Barium 7440-39-3 6020B 230 1ug/L0.63100
Beryllium 7440-41-7 6020B 0.36 J 1ug/L0.131.0
Cadmium 7440-43-9 6020B 1.0 U 1ug/L0.131.0
Chromium 7440-47-3 6020B 12 1ug/L1.310
Cobalt 7440-48-4 6020B 5.9 J 1ug/L0.6310
Copper 7440-50-8 6020B 11 1ug/L0.6310
Lead 7439-92-1 6020B 3.6 J 1ug/L0.2510
Nickel 7440-02-0 6020B 11 J 1ug/L1.350
Selenium 7782-49-2 6020B 10 U 1ug/L1.310
Silver 7440-22-4 6020B 10 U 1ug/L0.2510
Thallium 7440-28-0 6020B 5.5 U 1ug/L0.135.5
Vanadium 7440-62-2 6020B 24 J 1ug/L1.525
Zinc 7440-66-6 6020B 43 1ug/L2.510
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 60 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-28
SD28007-012
04/27/2017 1650
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 05/02/2017 1011 COH 05/01/2017 1334 40848
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Mercury 7439-97-6 7470A 0.00010 U 1mg/L0.0000280.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 61 of 130
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-29
SD28007-013
04/27/2017 1100
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 05/02/2017 1731 BWS 40944
1 (BOD, 5 day) SM 5210B-2011 1 05/03/2017 0948 AMM1 04/28/2017 1312 11310
1 (Chloride) 300.0 1 04/28/2017 1706 TAF 40901
1 (CO2 (calcula) SM 4500-CO2 D 1 05/02/2017 1731 BWS
1 (COD) SM 5220D-2011 1 05/06/2017 1117 TAF 05/04/2017 1037
1 (Nitrate - N) 300.0 1 04/28/2017 1706 TAF 40795
1 (Sulfate) 300.0 1 04/28/2017 1706 TAF 41004
1 (Sulfide) SM 4500-S2 F-2011 1 05/01/2017 1623 BWS 40932
1 (TDS) SM 2540C-2011 1 05/01/2017 1544 MGM 40849
1 (TOC) SM 5310C-2011 1 05/01/2017 2130 BWS 40876
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Alkalinity SM 2320B-20 36 1mg/L2.010
BOD, 5 day SM 5210B-20 2.7 1mg/L0.182.0
Chloride 300.0 6.5 1mg/L0.201.0
CO2 (calculation)124-38-9 SM 4500-CO2 73 1mg/L27
COD SM 5220D-20 72 1mg/L8.010
Nitrate - N 300.0 0.011 J 1mg/L0.00500.020
Sulfate 300.0 2.0 1mg/L0.201.0
Sulfide 18496-25-8 SM 4500-S2 0.80 J 1mg/L0.621.0
TDS SM 2540C-20 180 1mg/L3.410
TOC SM 5310C-20 18 1mg/L0.601.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 62 of 130
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-29
SD28007-013
04/27/2017 1100
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/01/2017 1239 ALL 40863
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 5.5 J 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 63 of 130
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-29
SD28007-013
04/27/2017 1100
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/01/2017 1239 ALL 40863
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 104 70-130
1,2-Dichloroethane-d4 108 70-130
Toluene-d8 104 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 64 of 130
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Shealy Environmental Services, Inc.
Dissolved Gases
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-29
SD28007-013
04/27/2017 1100
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 05/03/2017 1504 TML 41108
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Ethane 74-84-0 RSK - 175 10 U 1ug/L2.510
Ethene 74-85-1 RSK - 175 10 U 1ug/L2.510
Methane 74-82-8 RSK - 175 7.6 BJ 1ug/L2.510
Propane 74-98-6 RSK - 175 15 U 1ug/L3.515
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 65 of 130
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ICP-MS Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-29
SD28007-013
04/27/2017 1100
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 05/03/2017 0124 BNW 04/28/2017 1749 40785
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020B 6.0 U 1ug/L0.506.0
Arsenic 7440-38-2 6020B 10 U 1ug/L1.310
Barium 7440-39-3 6020B 83 J 1ug/L0.63100
Beryllium 7440-41-7 6020B 0.40 J 1ug/L0.131.0
Cadmium 7440-43-9 6020B 1.0 U 1ug/L0.131.0
Chromium 7440-47-3 6020B 5.5 J 1ug/L1.310
Cobalt 7440-48-4 6020B 2.5 J 1ug/L0.6310
Copper 7440-50-8 6020B 8.2 J 1ug/L0.6310
Lead 7439-92-1 6020B 5.8 J 1ug/L0.2510
Nickel 7440-02-0 6020B 7.4 J 1ug/L1.350
Selenium 7782-49-2 6020B 10 U 1ug/L1.310
Silver 7440-22-4 6020B 10 U 1ug/L0.2510
Sodium 7440-23-5 6020B 9100 1ug/L50400
Thallium 7440-28-0 6020B 5.5 U 1ug/L0.135.5
Vanadium 7440-62-2 6020B 11 J 1ug/L1.525
Zinc 7440-66-6 6020B 19 1ug/L2.510
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 66 of 130
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CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-29
SD28007-013
04/27/2017 1100
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 05/02/2017 1013 COH 05/01/2017 1334 40848
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Mercury 7439-97-6 7470A 0.000032 J 1mg/L0.0000280.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 67 of 130
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
DUP
SD28007-014
04/27/2017 0800
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/01/2017 1300 ALL 40863
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 0.43 J 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 68 of 130
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
DUP
SD28007-014
04/27/2017 0800
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/01/2017 1300 ALL 40863
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 104 70-130
1,2-Dichloroethane-d4 104 70-130
Toluene-d8 103 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 69 of 130
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Shealy Environmental Services, Inc.
ICP-MS Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
DUP
SD28007-014
04/27/2017 0800
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 05/03/2017 0140 BNW 04/28/2017 1749 40785
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020B 6.0 U 1ug/L0.506.0
Arsenic 7440-38-2 6020B 3.9 J 1ug/L1.310
Barium 7440-39-3 6020B 250 1ug/L0.63100
Beryllium 7440-41-7 6020B 1.0 U 1ug/L0.131.0
Cadmium 7440-43-9 6020B 1.0 U 1ug/L0.131.0
Chromium 7440-47-3 6020B 10 U 1ug/L1.310
Cobalt 7440-48-4 6020B 10 U 1ug/L0.6310
Copper 7440-50-8 6020B 10 U 1ug/L0.6310
Lead 7439-92-1 6020B 10 U 1ug/L0.2510
Nickel 7440-02-0 6020B 3.9 J 1ug/L1.350
Selenium 7782-49-2 6020B 3.9 J 1ug/L1.310
Silver 7440-22-4 6020B 10 U 1ug/L0.2510
Thallium 7440-28-0 6020B 5.5 U 1ug/L0.135.5
Vanadium 7440-62-2 6020B 25 U 1ug/L1.525
Zinc 7440-66-6 6020B 10 U 1ug/L2.510
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 70 of 130
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Shealy Environmental Services, Inc.
CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
DUP
SD28007-014
04/27/2017 0800
04/28/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 05/02/2017 1015 COH 05/01/2017 1334 40848
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Mercury 7439-97-6 7470A 0.00010 U 1mg/L0.0000280.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
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Shealy Environmental Services, Inc.
QC Summary
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Shealy Environmental Services, Inc.
Inorganic non-metals - MB
Batch:
Sample ID:SQ40795-001
40795
Analytical Method:300.0
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Nitrate - N 0.020 04/28/2017 1517U0.020 0.0050 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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Shealy Environmental Services, Inc.
Inorganic non-metals - LCS
Batch:
Sample ID:SQ40795-002
40795
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Nitrate - N 0.84 04/28/2017 15291040.80 90-1101
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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Shealy Environmental Services, Inc.
Inorganic non-metals - MS
Batch:
Sample ID:SD28007-008MS
40795
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Nitrate - N 0.79 04/28/2017 1642970.80 90-1100.015 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 75 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals - MSD
Batch:
Sample ID:SD28007-008MD
40795
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Nitrate - N 0.81 04/28/2017 1654990.80 90-1101.8 200.015 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 76 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals - MB
Batch:
Sample ID:SQ40849-001
40849
Analytical Method:SM 2540C-2011
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
TDS 10 05/01/2017 1544U103.4 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 77 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals - LCS
Batch:
Sample ID:SQ40849-002
40849
Analytical Method:SM 2540C-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
TDS 1500 05/01/2017 154498150090-1101
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 78 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals - Duplicate
Batch:
Sample ID:SD28007-003DU
40849
Analytical Method:SM 2540C-2011
Matrix:Aqueous
Parameter
Result
Q Analysis Date% RPD
% RPD
Limit
Sample
Amount
Dil(mg/L)(mg/L)
TDS 390 05/01/2017 15446.2 204201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 79 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals - MB
Batch:
Sample ID:SQ40876-001
40876
Analytical Method:SM 5310C-2011
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
TOC 1.0 05/01/2017 1549U1.0 0.60 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 80 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals - LCS
Batch:
Sample ID:SQ40876-002
40876
Analytical Method:SM 5310C-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
TOC 19 05/01/2017 1605952090-1101
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 81 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals - MS
Batch:
Sample ID:SD28007-001MS
40876
Analytical Method:SM 5310C-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
TOC 22 05/01/2017 1952882070-1304.7 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 82 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals - MSD
Batch:
Sample ID:SD28007-001MD
40876
Analytical Method:SM 5310C-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
TOC 22 05/01/2017 2008882070-1300.013 204.7 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 83 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals - MB
Batch:
Sample ID:SQ40901-001
40901
Analytical Method:300.0
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Chloride 1.0 04/28/2017 1517U1.0 0.20 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 84 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals - LCS
Batch:
Sample ID:SQ40901-002
40901
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Chloride 20 04/28/2017 15291002090-1101
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 85 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals - MS
Batch:
Sample ID:SD28007-008MS
40901
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Chloride 30 04/28/2017 1642932090-110111
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 86 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals - MSD
Batch:
Sample ID:SD28007-008MD
40901
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Chloride 30 04/28/2017 1654952090-1101.2 20111
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 87 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals - MB
Batch:
Sample ID:SQ40902-001
40902
Analytical Method:300.0
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Nitrate - N 0.020 04/29/2017 0949U0.020 0.0050 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 88 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals - LCS
Batch:
Sample ID:SQ40902-002
40902
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Nitrate - N 0.84 04/29/2017 10011050.80 90-1101
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 89 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals - MS
Batch:
Sample ID:SD28007-004MS
40902
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Nitrate - N 0.81 04/29/2017 11491010.80 90-1100.0071 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 90 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals - MSD
Batch:
Sample ID:SD28007-004MD
40902
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Nitrate - N 0.83 04/29/2017 12261030.80 90-1101.9 200.0071 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 91 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals - MB
Batch:
Sample ID:SQ40932-001
40932
Analytical Method:SM 4500-S2 F-2011
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Sulfide 1.0 05/01/2017 1623U1.0 0.62 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 92 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals - LCS
Batch:
Sample ID:SQ40932-002
40932
Analytical Method:SM 4500-S2 F-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Sulfide 9.4 05/01/2017 1623941080-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 93 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals - MS
Batch:
Sample ID:SD28007-003MS
40932
Analytical Method:SM 4500-S2 F-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Sulfide 5.1 05/01/2017 1623N511070-1300.0 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 94 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals - MSD
Batch:
Sample ID:SD28007-003MD
40932
Analytical Method:SM 4500-S2 F-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Sulfide 5.4 05/01/2017 1623N541070-1306.5 200.0 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 95 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals - MB
Batch:
Sample ID:SQ40944-001
40944
Analytical Method:SM 2320B-2011
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Alkalinity 10 05/02/2017 1544U102.0 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 96 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals - LCS
Batch:
Sample ID:SQ40944-002
40944
Analytical Method:SM 2320B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Alkalinity 96 05/02/2017 15509610090-1101
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 97 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals - Duplicate
Batch:
Sample ID:SD28007-001DU
40944
Analytical Method:SM 2320B-2011
Matrix:Aqueous
Parameter
Result
Q Analysis Date% RPD
% RPD
Limit
Sample
Amount
Dil(mg/L)(mg/L)
Alkalinity 170 05/02/2017 16550.080 201701
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 98 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals - MB
Batch:
Sample ID:SQ41004-001
41004
Analytical Method:300.0
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Sulfate 1.0 04/28/2017 1517U1.0 0.20 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 99 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals - LCS
Batch:
Sample ID:SQ41004-002
41004
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Sulfate 22 04/28/2017 15291102090-1101
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 100 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals - MS
Batch:
Sample ID:SD28007-008MS
41004
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Sulfate 23 04/28/2017 1642962090-1104.4 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 101 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals - MSD
Batch:
Sample ID:SD28007-008MD
41004
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Sulfate 24 04/28/2017 1654972090-1101.1 204.4 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 102 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals - MB
Batch:
Sample ID:SQ41010-001
41010
Analytical Method:300.0
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Sulfate 1.0 04/29/2017 0949U1.0 0.20 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 103 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals - LCS
Batch:
Sample ID:SQ41010-002
41010
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Sulfate 22 04/29/2017 10011082090-1101
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 104 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals - MS
Batch:
Sample ID:SD28007-004MS
41010
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Sulfate 25 04/29/2017 1149992090-1105.0 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 105 of 130
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Shealy Environmental Services, Inc.
Inorganic non-metals - MSD
Batch:
Sample ID:SD28007-004MD
41010
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Sulfate 25 04/29/2017 12261012090-1101.3 205.0 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 106 of 130
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:SQ40810-001
40810 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Acetone 10 04/28/2017 2045U102.0 ug/L1
Acrylonitrile 5.0 04/28/2017 2045U5.0 0.80 ug/L1
Benzene 0.50 04/28/2017 2045U0.50 0.40 ug/L1
Bromochloromethane 0.50 04/28/2017 2045U0.50 0.40 ug/L1
Bromodichloromethane 0.50 04/28/2017 2045U0.50 0.40 ug/L1
Bromoform 0.50 04/28/2017 2045U0.50 0.40 ug/L1
Bromomethane (Methyl bromide)0.50 04/28/2017 2045U0.50 0.40 ug/L1
2-Butanone (MEK)10 04/28/2017 2045U102.0 ug/L1
Carbon disulfide 0.50 04/28/2017 2045U0.50 0.40 ug/L1
Carbon tetrachloride 0.50 04/28/2017 2045U0.50 0.40 ug/L1
Chlorobenzene 0.50 04/28/2017 2045U0.50 0.40 ug/L1
Chloroethane 0.50 04/28/2017 2045U0.50 0.40 ug/L1
Chloroform 0.50 04/28/2017 2045U0.50 0.40 ug/L1
Chloromethane (Methyl chloride)0.50 04/28/2017 2045U0.50 0.40 ug/L1
1,2-Dibromo-3-chloropropane (DBCP)0.50 04/28/2017 2045U0.50 0.40 ug/L1
Dibromochloromethane 0.50 04/28/2017 2045U0.50 0.40 ug/L1
1,2-Dibromoethane (EDB)0.50 04/28/2017 2045U0.50 0.40 ug/L1
Dibromomethane (Methylene bromide)0.50 04/28/2017 2045U0.50 0.40 ug/L1
trans-1,4-Dichloro-2-butene 2.0 04/28/2017 2045U2.0 0.40 ug/L1
1,4-Dichlorobenzene 0.50 04/28/2017 2045U0.50 0.40 ug/L1
1,2-Dichlorobenzene 0.50 04/28/2017 2045U0.50 0.40 ug/L1
Dichlorodifluoromethane 0.50 04/28/2017 2045U0.50 0.40 ug/L1
1,2-Dichloroethane 0.50 04/28/2017 2045U0.50 0.40 ug/L1
1,1-Dichloroethane 0.50 04/28/2017 2045U0.50 0.40 ug/L1
trans-1,2-Dichloroethene 0.50 04/28/2017 2045U0.50 0.40 ug/L1
cis-1,2-Dichloroethene 0.50 04/28/2017 2045U0.50 0.40 ug/L1
1,1-Dichloroethene 0.50 04/28/2017 2045U0.50 0.40 ug/L1
1,2-Dichloropropane 0.50 04/28/2017 2045U0.50 0.40 ug/L1
trans-1,3-Dichloropropene 0.50 04/28/2017 2045U0.50 0.40 ug/L1
cis-1,3-Dichloropropene 0.50 04/28/2017 2045U0.50 0.40 ug/L1
Ethylbenzene 0.50 04/28/2017 2045U0.50 0.40 ug/L1
2-Hexanone 10 04/28/2017 2045U102.0 ug/L1
Methyl iodide (Iodomethane)5.0 04/28/2017 2045U5.0 0.40 ug/L1
4-Methyl-2-pentanone 10 04/28/2017 2045U102.0 ug/L1
Methylene chloride 0.50 04/28/2017 2045U0.50 0.40 ug/L1
Styrene 0.50 04/28/2017 2045U0.50 0.40 ug/L1
1,1,2,2-Tetrachloroethane 0.50 04/28/2017 2045U0.50 0.40 ug/L1
1,1,1,2-Tetrachloroethane 0.50 04/28/2017 2045U0.50 0.40 ug/L1
Tetrachloroethene 0.50 04/28/2017 2045U0.50 0.40 ug/L1
Toluene 0.50 04/28/2017 2045U0.50 0.40 ug/L1
1,1,2-Trichloroethane 0.50 04/28/2017 2045U0.50 0.40 ug/L1
1,1,1-Trichloroethane 0.50 04/28/2017 2045U0.50 0.40 ug/L1
Trichloroethene 0.50 04/28/2017 2045U0.50 0.40 ug/L1
Trichlorofluoromethane 0.50 04/28/2017 2045U0.50 0.40 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 107 of 130
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:SQ40810-001
40810 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
1,2,3-Trichloropropane 0.50 04/28/2017 2045U0.50 0.40 ug/L1
Vinyl acetate 5.0 04/28/2017 2045U5.0 1.2 ug/L1
Vinyl chloride 0.50 04/28/2017 2045U0.50 0.40 ug/L1
Xylenes (total)1.0 04/28/2017 2045U1.0 0.40 ug/L1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 106 70-130
1,2-Dichloroethane-d4 106 70-130
Toluene-d8 104 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 108 of 130
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:SQ40810-002
40810 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Acetone 120 04/28/2017 194612210060-1401
Acrylonitrile 120 04/28/2017 194611910060-1401
Benzene 51 04/28/2017 19461025070-1301
Bromochloromethane 54 04/28/2017 19461085070-1301
Bromodichloromethane 53 04/28/2017 19461065070-1301
Bromoform 51 04/28/2017 19461035070-1301
Bromomethane (Methyl bromide)61 04/28/2017 19461225060-1401
2-Butanone (MEK)110 04/28/2017 194610610060-1401
Carbon disulfide 48 04/28/2017 1946975060-1401
Carbon tetrachloride 48 04/28/2017 1946955070-1301
Chlorobenzene 54 04/28/2017 19461075070-1301
Chloroethane 54 04/28/2017 19461075060-1401
Chloroform 56 04/28/2017 19461115070-1301
Chloromethane (Methyl chloride)53 04/28/2017 19461075060-1401
1,2-Dibromo-3-chloropropane (DBCP)50 04/28/2017 19461005070-1301
Dibromochloromethane 54 04/28/2017 19461075070-1301
1,2-Dibromoethane (EDB)50 04/28/2017 19461005070-1301
Dibromomethane (Methylene bromide)51 04/28/2017 19461035070-1301
trans-1,4-Dichloro-2-butene 46 04/28/2017 1946925034-1421
1,4-Dichlorobenzene 53 04/28/2017 19461075070-1301
1,2-Dichlorobenzene 54 04/28/2017 19461085070-1301
Dichlorodifluoromethane 57 04/28/2017 19461145060-1401
1,2-Dichloroethane 53 04/28/2017 19461065070-1301
1,1-Dichloroethane 55 04/28/2017 19461105070-1301
trans-1,2-Dichloroethene 55 04/28/2017 19461105070-1301
cis-1,2-Dichloroethene 54 04/28/2017 19461095070-1301
1,1-Dichloroethene 49 04/28/2017 1946995070-1301
1,2-Dichloropropane 53 04/28/2017 19461055070-1301
trans-1,3-Dichloropropene 53 04/28/2017 19461055070-1301
cis-1,3-Dichloropropene 53 04/28/2017 19461055070-1301
Ethylbenzene 53 04/28/2017 19461055070-1301
2-Hexanone 91 04/28/2017 19469110060-1401
Methyl iodide (Iodomethane)51 04/28/2017 19461025070-1301
4-Methyl-2-pentanone 98 04/28/2017 19469810060-1401
Methylene chloride 51 04/28/2017 19461015070-1301
Styrene 53 04/28/2017 19461075070-1301
1,1,2,2-Tetrachloroethane 52 04/28/2017 19461045070-1301
1,1,1,2-Tetrachloroethane 52 04/28/2017 19461035070-1301
Tetrachloroethene 54 04/28/2017 19461085070-1301
Toluene 55 04/28/2017 19461095070-1301
1,1,2-Trichloroethane 50 04/28/2017 19461005070-1301
1,1,1-Trichloroethane 49 04/28/2017 1946985070-1301
Trichloroethene 49 04/28/2017 1946985070-1301
Trichlorofluoromethane 52 04/28/2017 19461035060-1401
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 109 of 130
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:SQ40810-002
40810 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
1,2,3-Trichloropropane 52 04/28/2017 19461035070-1301
Vinyl acetate 56 04/28/2017 19461115060-1401
Vinyl chloride 54 04/28/2017 19461085060-1401
Xylenes (total)100 04/28/2017 194610410070-1301
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 100 70-130
1,2-Dichloroethane-d4 102 70-130
Toluene-d8 103 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 110 of 130
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:SQ40863-001
40863 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Acetone 10 05/01/2017 0934U102.0 ug/L1
Acrylonitrile 5.0 05/01/2017 0934U5.0 0.80 ug/L1
Benzene 0.50 05/01/2017 0934U0.50 0.40 ug/L1
Bromochloromethane 0.50 05/01/2017 0934U0.50 0.40 ug/L1
Bromodichloromethane 0.50 05/01/2017 0934U0.50 0.40 ug/L1
Bromoform 0.50 05/01/2017 0934U0.50 0.40 ug/L1
Bromomethane (Methyl bromide)0.50 05/01/2017 0934U0.50 0.40 ug/L1
2-Butanone (MEK)10 05/01/2017 0934U102.0 ug/L1
Carbon disulfide 0.50 05/01/2017 0934U0.50 0.40 ug/L1
Carbon tetrachloride 0.50 05/01/2017 0934U0.50 0.40 ug/L1
Chlorobenzene 0.50 05/01/2017 0934U0.50 0.40 ug/L1
Chloroethane 0.50 05/01/2017 0934U0.50 0.40 ug/L1
Chloroform 0.50 05/01/2017 0934U0.50 0.40 ug/L1
Chloromethane (Methyl chloride)0.50 05/01/2017 0934U0.50 0.40 ug/L1
1,2-Dibromo-3-chloropropane (DBCP)0.50 05/01/2017 0934U0.50 0.40 ug/L1
Dibromochloromethane 0.50 05/01/2017 0934U0.50 0.40 ug/L1
1,2-Dibromoethane (EDB)0.50 05/01/2017 0934U0.50 0.40 ug/L1
Dibromomethane (Methylene bromide)0.50 05/01/2017 0934U0.50 0.40 ug/L1
trans-1,4-Dichloro-2-butene 2.0 05/01/2017 0934U2.0 0.40 ug/L1
1,4-Dichlorobenzene 0.50 05/01/2017 0934U0.50 0.40 ug/L1
1,2-Dichlorobenzene 0.50 05/01/2017 0934U0.50 0.40 ug/L1
Dichlorodifluoromethane 0.50 05/01/2017 0934U0.50 0.40 ug/L1
1,2-Dichloroethane 0.50 05/01/2017 0934U0.50 0.40 ug/L1
1,1-Dichloroethane 0.50 05/01/2017 0934U0.50 0.40 ug/L1
trans-1,2-Dichloroethene 0.50 05/01/2017 0934U0.50 0.40 ug/L1
cis-1,2-Dichloroethene 0.50 05/01/2017 0934U0.50 0.40 ug/L1
1,1-Dichloroethene 0.50 05/01/2017 0934U0.50 0.40 ug/L1
1,2-Dichloropropane 0.50 05/01/2017 0934U0.50 0.40 ug/L1
trans-1,3-Dichloropropene 0.50 05/01/2017 0934U0.50 0.40 ug/L1
cis-1,3-Dichloropropene 0.50 05/01/2017 0934U0.50 0.40 ug/L1
Ethylbenzene 0.50 05/01/2017 0934U0.50 0.40 ug/L1
2-Hexanone 10 05/01/2017 0934U102.0 ug/L1
Methyl iodide (Iodomethane)5.0 05/01/2017 0934U5.0 0.40 ug/L1
4-Methyl-2-pentanone 10 05/01/2017 0934U102.0 ug/L1
Methylene chloride 0.50 05/01/2017 0934U0.50 0.40 ug/L1
Styrene 0.50 05/01/2017 0934U0.50 0.40 ug/L1
1,1,2,2-Tetrachloroethane 0.50 05/01/2017 0934U0.50 0.40 ug/L1
1,1,1,2-Tetrachloroethane 0.50 05/01/2017 0934U0.50 0.40 ug/L1
Tetrachloroethene 0.50 05/01/2017 0934U0.50 0.40 ug/L1
Toluene 0.50 05/01/2017 0934U0.50 0.40 ug/L1
1,1,2-Trichloroethane 0.50 05/01/2017 0934U0.50 0.40 ug/L1
1,1,1-Trichloroethane 0.50 05/01/2017 0934U0.50 0.40 ug/L1
Trichloroethene 0.50 05/01/2017 0934U0.50 0.40 ug/L1
Trichlorofluoromethane 0.50 05/01/2017 0934U0.50 0.40 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 111 of 130
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:SQ40863-001
40863 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
1,2,3-Trichloropropane 0.50 05/01/2017 0934U0.50 0.40 ug/L1
Vinyl acetate 5.0 05/01/2017 0934U5.0 1.2 ug/L1
Vinyl chloride 0.50 05/01/2017 0934U0.50 0.40 ug/L1
Xylenes (total)1.0 05/01/2017 0934U1.0 0.40 ug/L1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 103 70-130
1,2-Dichloroethane-d4 108 70-130
Toluene-d8 103 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 112 of 130
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:SQ40863-002
40863 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Acetone 130 05/01/2017 083612710060-1401
Acrylonitrile 110 05/01/2017 083611310060-1401
Benzene 52 05/01/2017 08361045070-1301
Bromochloromethane 55 05/01/2017 08361105070-1301
Bromodichloromethane 54 05/01/2017 08361085070-1301
Bromoform 52 05/01/2017 08361035070-1301
Bromomethane (Methyl bromide)61 05/01/2017 08361235060-1401
2-Butanone (MEK)110 05/01/2017 083611310060-1401
Carbon disulfide 57 05/01/2017 08361145060-1401
Carbon tetrachloride 50 05/01/2017 08361015070-1301
Chlorobenzene 54 05/01/2017 08361075070-1301
Chloroethane 58 05/01/2017 08361155060-1401
Chloroform 58 05/01/2017 08361155070-1301
Chloromethane (Methyl chloride)59 05/01/2017 08361185060-1401
1,2-Dibromo-3-chloropropane (DBCP)48 05/01/2017 0836965070-1301
Dibromochloromethane 54 05/01/2017 08361085070-1301
1,2-Dibromoethane (EDB)51 05/01/2017 08361025070-1301
Dibromomethane (Methylene bromide)52 05/01/2017 08361035070-1301
trans-1,4-Dichloro-2-butene 46 05/01/2017 0836925034-1421
1,4-Dichlorobenzene 53 05/01/2017 08361075070-1301
1,2-Dichlorobenzene 54 05/01/2017 08361095070-1301
Dichlorodifluoromethane 69 05/01/2017 08361385060-1401
1,2-Dichloroethane 54 05/01/2017 08361085070-1301
1,1-Dichloroethane 58 05/01/2017 08361165070-1301
trans-1,2-Dichloroethene 59 05/01/2017 08361185070-1301
cis-1,2-Dichloroethene 57 05/01/2017 08361145070-1301
1,1-Dichloroethene 54 05/01/2017 08361085070-1301
1,2-Dichloropropane 53 05/01/2017 08361055070-1301
trans-1,3-Dichloropropene 53 05/01/2017 08361075070-1301
cis-1,3-Dichloropropene 53 05/01/2017 08361075070-1301
Ethylbenzene 54 05/01/2017 08361085070-1301
2-Hexanone 93 05/01/2017 08369310060-1401
Methyl iodide (Iodomethane)58 05/01/2017 08361165070-1301
4-Methyl-2-pentanone 97 05/01/2017 08369710060-1401
Methylene chloride 55 05/01/2017 08361095070-1301
Styrene 54 05/01/2017 08361075070-1301
1,1,2,2-Tetrachloroethane 52 05/01/2017 08361055070-1301
1,1,1,2-Tetrachloroethane 53 05/01/2017 08361055070-1301
Tetrachloroethene 56 05/01/2017 08361125070-1301
Toluene 57 05/01/2017 08361135070-1301
1,1,2-Trichloroethane 51 05/01/2017 08361015070-1301
1,1,1-Trichloroethane 52 05/01/2017 08361035070-1301
Trichloroethene 51 05/01/2017 08361015070-1301
Trichlorofluoromethane 60 05/01/2017 08361215060-1401
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 113 of 130
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:SQ40863-002
40863 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
1,2,3-Trichloropropane 53 05/01/2017 08361065070-1301
Vinyl acetate 57 05/01/2017 08361145060-1401
Vinyl chloride 61 05/01/2017 08361235060-1401
Xylenes (total)110 05/01/2017 083610610070-1301
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 102 70-130
1,2-Dichloroethane-d4 102 70-130
Toluene-d8 105 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 114 of 130
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS - Duplicate
Batch:Prep Method:
Sample ID:SD28007-009DU
40863 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q Analysis Date% RPD
% RPD
Limit
Sample
Amount
Dil(ug/L)(ug/L)
Acetone 1.0 05/01/2017 1720U0.00 20ND1
Acrylonitrile 1.0 05/01/2017 1720U0.00 20ND1
Benzene 1.0 05/01/2017 1720U0.00 20ND1
Bromochloromethane 1.0 05/01/2017 1720U0.00 20ND1
Bromodichloromethane 1.0 05/01/2017 1720U0.00 20ND1
Bromoform 1.0 05/01/2017 1720U0.00 20ND1
Bromomethane (Methyl bromide)1.0 05/01/2017 1720U0.00 20ND1
2-Butanone (MEK)1.0 05/01/2017 1720U0.00 20ND1
Carbon disulfide 1.0 05/01/2017 1720U0.00 20ND1
Carbon tetrachloride 1.0 05/01/2017 1720U0.00 20ND1
Chlorobenzene 1.0 05/01/2017 1720U0.00 20ND1
Chloroethane 1.0 05/01/2017 1720U0.00 20ND1
Chloroform 1.0 05/01/2017 1720U0.00 20ND1
Chloromethane (Methyl chloride)1.0 05/01/2017 1720U0.00 20ND1
1,2-Dibromo-3-chloropropane (DBCP)1.0 05/01/2017 1720U0.00 20ND1
Dibromochloromethane 1.0 05/01/2017 1720U0.00 20ND1
1,2-Dibromoethane (EDB)1.0 05/01/2017 1720U0.00 20ND1
Dibromomethane (Methylene bromide)1.0 05/01/2017 1720U0.00 20ND1
trans-1,4-Dichloro-2-butene 1.0 05/01/2017 1720U0.00 20ND1
1,2-Dichlorobenzene 1.0 05/01/2017 1720U0.00 20ND1
1,4-Dichlorobenzene 1.0 05/01/2017 1720U0.00 20ND1
Dichlorodifluoromethane 1.0 05/01/2017 1720U0.00 20ND1
1,1-Dichloroethane 1.0 05/01/2017 1720U0.00 20ND1
1,2-Dichloroethane 1.0 05/01/2017 1720U0.00 20ND1
1,1-Dichloroethene 1.0 05/01/2017 1720U0.00 20ND1
cis-1,2-Dichloroethene 1.0 05/01/2017 1720U0.00 20ND1
trans-1,2-Dichloroethene 1.9 05/01/2017 172020202.4 1
1,2-Dichloropropane 1.0 05/01/2017 1720U0.00 20ND1
cis-1,3-Dichloropropene 1.0 05/01/2017 1720U0.00 20ND1
trans-1,3-Dichloropropene 1.0 05/01/2017 1720U0.00 20ND1
Ethylbenzene 1.0 05/01/2017 1720U0.00 20ND1
2-Hexanone 1.0 05/01/2017 1720U0.00 20ND1
Methyl iodide (Iodomethane)1.0 05/01/2017 1720U0.00 20ND1
4-Methyl-2-pentanone 1.0 05/01/2017 1720U0.00 20ND1
Methylene chloride 1.0 05/01/2017 1720U0.00 20ND1
Styrene 1.0 05/01/2017 1720U0.00 20ND1
1,1,1,2-Tetrachloroethane 1.0 05/01/2017 1720U0.00 20ND1
1,1,2,2-Tetrachloroethane 1.0 05/01/2017 1720U0.00 20ND1
Tetrachloroethene 1.0 05/01/2017 1720U0.00 20ND1
Toluene 1.0 05/01/2017 1720U0.00 20ND1
1,1,1-Trichloroethane 1.0 05/01/2017 1720U0.00 20ND1
1,1,2-Trichloroethane 1.0 05/01/2017 1720U0.00 20ND1
Trichloroethene 1.0 05/01/2017 1720U0.00 20ND1
Trichlorofluoromethane 1.0 05/01/2017 1720U0.00 20ND1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 115 of 130
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS - Duplicate
Batch:Prep Method:
Sample ID:SD28007-009DU
40863 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q Analysis Date% RPD
% RPD
Limit
Sample
Amount
Dil(ug/L)(ug/L)
1,2,3-Trichloropropane 1.0 05/01/2017 1720U0.00 20ND1
Vinyl acetate 1.0 05/01/2017 1720U0.00 20ND1
Vinyl chloride 1.0 05/01/2017 1720U0.00 20ND1
Xylenes (total)1.0 05/01/2017 1720U0.00 20ND1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 104 70-130
1,2-Dichloroethane-d4 107 70-130
Toluene-d8 103 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 116 of 130
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Sample ID:SD28007-010MS
40863 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
Acetone 110 05/01/2017 174111310060-1400.0 1
Acrylonitrile 120 05/01/2017 174111610060-1400.0 1
Benzene 54 05/01/2017 17411095070-1300.0 1
Bromochloromethane 54 05/01/2017 17411095070-1300.0 1
Bromodichloromethane 56 05/01/2017 17411115070-1300.0 1
Bromoform 53 05/01/2017 17411065070-1300.0 1
Bromomethane (Methyl bromide)59 05/01/2017 17411185060-1400.0 1
2-Butanone (MEK)100 05/01/2017 174110310060-1400.0 1
Carbon disulfide 54 05/01/2017 17411095060-1400.0 1
Carbon tetrachloride 53 05/01/2017 17411075070-1300.0 1
Chlorobenzene 55 05/01/2017 17411115070-1300.0 1
Chloroethane 62 05/01/2017 17411245060-1400.0 1
Chloroform 59 05/01/2017 17411175070-1300.0 1
Chloromethane (Methyl chloride)64 05/01/2017 17411295020-1580.0 1
1,2-Dibromo-3-chloropropane (DBCP)46 05/01/2017 1741915070-1300.0 1
Dibromochloromethane 56 05/01/2017 17411125070-1300.0 1
1,2-Dibromoethane (EDB)51 05/01/2017 17411035070-1300.0 1
Dibromomethane (Methylene bromide)52 05/01/2017 17411045070-1300.0 1
trans-1,4-Dichloro-2-butene 48 05/01/2017 1741965034-1420.0 1
1,2-Dichlorobenzene 52 05/01/2017 17411045070-1300.0 1
1,4-Dichlorobenzene 52 05/01/2017 17411045070-1300.0 1
Dichlorodifluoromethane 81 05/01/2017 1741N1635060-1400.0 1
1,1-Dichloroethane 60 05/01/2017 17411175070-1301.3 1
1,2-Dichloroethane 54 05/01/2017 17411085070-1300.0 1
1,1-Dichloroethene 54 05/01/2017 17411085070-1300.0 1
cis-1,2-Dichloroethene 57 05/01/2017 17411145070-1300.0 1
trans-1,2-Dichloroethene 60 05/01/2017 17411195070-1300.0 1
1,2-Dichloropropane 55 05/01/2017 17411105070-1300.0 1
cis-1,3-Dichloropropene 54 05/01/2017 17411085070-1300.0 1
trans-1,3-Dichloropropene 52 05/01/2017 17411045070-1300.0 1
Ethylbenzene 55 05/01/2017 17411115070-1300.0 1
2-Hexanone 100 05/01/2017 174110210060-1400.0 1
Methyl iodide (Iodomethane)56 05/01/2017 17411125070-1300.0 1
4-Methyl-2-pentanone 100 05/01/2017 174110310060-1400.0 1
Methylene chloride 53 05/01/2017 17411055070-1300.0 1
Styrene 56 05/01/2017 17411115070-1300.0 1
1,1,1,2-Tetrachloroethane 51 05/01/2017 17411025070-1300.0 1
1,1,2,2-Tetrachloroethane 50 05/01/2017 1741995070-1300.0 1
Tetrachloroethene 58 05/01/2017 17411165070-1300.0 1
Toluene 58 05/01/2017 17411175070-1300.0 1
1,1,1-Trichloroethane 55 05/01/2017 17411095070-1300.0 1
1,1,2-Trichloroethane 51 05/01/2017 17411025070-1300.0 1
Trichloroethene 52 05/01/2017 17411045070-1300.0 1
Trichlorofluoromethane 63 05/01/2017 17411255060-1400.0 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 117 of 130
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Sample ID:SD28007-010MS
40863 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
1,2,3-Trichloropropane 52 05/01/2017 17411045070-1300.0 1
Vinyl acetate 47 05/01/2017 1741945029-1970.0 1
Vinyl chloride 67 05/01/2017 17411355060-1400.0 1
Xylenes (total)110 05/01/2017 174110910070-1300.0 1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 107 70-130
1,2-Dichloroethane-d4 105 70-130
Toluene-d8 104 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 118 of 130
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Shealy Environmental Services, Inc.
Dissolved Gases - MB
Batch:
Sample ID:SQ41108-001
41108
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Ethane 10 05/03/2017 1304U102.5 ug/L1
Ethene 10 05/03/2017 1304U102.5 ug/L1
Methane 2.9 05/03/2017 1304J102.5 ug/L1
Propane 15 05/03/2017 1304U153.5 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 119 of 130
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Shealy Environmental Services, Inc.
Dissolved Gases - LCS
Batch:
Sample ID:SQ41108-002
41108
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Ethane 460 05/03/2017 12458255070-1301
Ethene 430 05/03/2017 12458352070-1301
Methane 230 05/03/2017 12457930070-1301
Propane 690 05/03/2017 1245N16742070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 120 of 130
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Shealy Environmental Services, Inc.
Dissolved Gases - MB
Batch:
Sample ID:SQ41344-001
41344
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Ethane 10 05/05/2017 1450U102.5 ug/L1
Ethene 10 05/05/2017 1450U102.5 ug/L1
Methane 2.6 05/05/2017 1450J102.5 ug/L1
Propane 15 05/05/2017 1450U153.5 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 121 of 130
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Shealy Environmental Services, Inc.
Dissolved Gases - LCS
Batch:
Sample ID:SQ41344-002
41344
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Ethane 640 05/05/2017 142911655070-1301
Ethene 590 05/05/2017 142911552070-1301
Methane 330 05/05/2017 142911130070-1301
Propane 970 05/05/2017 142911981070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 122 of 130
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Shealy Environmental Services, Inc.
ICP-MS Metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:SQ40785-001
40785 3005A
04/28/2017 1749Analytical Method:6020B
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Antimony 6.0 05/02/2017 2336U6.0 0.50 ug/L1
Arsenic 10 05/02/2017 2336U101.3 ug/L1
Barium 100 05/02/2017 2336U1000.63 ug/L1
Beryllium 1.0 05/02/2017 2336U1.0 0.13 ug/L1
Cadmium 1.0 05/02/2017 2336U1.0 0.13 ug/L1
Chromium 10 05/02/2017 2336U101.3 ug/L1
Cobalt 10 05/02/2017 2336U100.63 ug/L1
Copper 10 05/02/2017 2336U100.63 ug/L1
Lead 10 05/02/2017 2336U100.25 ug/L1
Nickel 50 05/02/2017 2336U501.3 ug/L1
Selenium 10 05/02/2017 2336U101.3 ug/L1
Silver 10 05/02/2017 2336U100.25 ug/L1
Sodium 400 05/02/2017 2336U40050ug/L1
Thallium 5.5 05/02/2017 2336U5.5 0.13 ug/L1
Vanadium 25 05/02/2017 2336U251.5 ug/L1
Zinc 10 05/02/2017 2336U102.5 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 123 of 130
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Shealy Environmental Services, Inc.
ICP-MS Metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:SQ40785-002
40785 3005A
04/28/2017 1749Analytical Method:6020B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Antimony 100 05/02/2017 234110310080-1201
Arsenic 110 05/02/2017 234110710080-1201
Barium 110 05/02/2017 234110610080-1201
Beryllium 110 05/02/2017 234110710080-1201
Cadmium 100 05/02/2017 234110410080-1201
Chromium 100 05/02/2017 234110210080-1201
Cobalt 110 05/02/2017 234110610080-1201
Copper 110 05/02/2017 234110810080-1201
Lead 100 05/02/2017 234110310080-1201
Nickel 110 05/02/2017 234110610080-1201
Selenium 100 05/02/2017 234110410080-1201
Silver 100 05/02/2017 234110210080-1201
Sodium 1000 05/02/2017 2341101100080-1201
Thallium 100 05/02/2017 234110510080-1201
Vanadium 110 05/02/2017 234110610080-1201
Zinc 110 05/02/2017 234110610080-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 124 of 130
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Shealy Environmental Services, Inc.
ICP-MS Metals - MS
Batch:Prep Method:
Prep Date:
Sample ID:SD28007-001MS
40785 3005A
04/28/2017 1749Analytical Method:6020B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
Antimony 100 05/02/2017 235210310070-1300.0 1
Arsenic 100 05/02/2017 23529910070-1302.1 1
Barium 260 05/02/2017 235210510070-1301601
Beryllium 100 05/02/2017 235210310070-1300.0 1
Cadmium 95 05/02/2017 23529510070-1300.0 1
Chromium 97 05/02/2017 23529710070-1300.0 1
Cobalt 96 05/02/2017 23529610070-1300.0 1
Copper 95 05/02/2017 23529410070-1300.97 1
Lead 100 05/02/2017 235210410070-1300.28 1
Nickel 96 05/02/2017 23529410070-1302.8 1
Selenium 99 05/02/2017 23529010070-1309.4 1
Silver 92 05/02/2017 23529210070-1300.0 1
Thallium 100 05/02/2017 235210410070-1300.0 1
Vanadium 110 05/02/2017 235210310070-1309.6 1
Zinc 88 05/02/2017 23528810070-1300.0 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 125 of 130
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Shealy Environmental Services, Inc.
ICP-MS Metals - MSD
Batch:Prep Method:
Prep Date:
Sample ID:SD28007-001MD
40785 3005A
04/28/2017 1749Analytical Method:6020B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
Antimony 100 05/02/2017 235810210070-1301.1 200.0 1
Arsenic 98 05/02/2017 23589610070-1303.7 202.1 1
Barium 260 05/02/2017 235810010070-1302.0 201601
Beryllium 100 05/02/2017 235810310070-1300.29 200.0 1
Cadmium 95 05/02/2017 23589510070-1300.074 200.0 1
Chromium 91 05/02/2017 23589110070-1306.3 200.0 1
Cobalt 93 05/02/2017 23589310070-1304.0 200.0 1
Copper 92 05/02/2017 23589110070-1303.1 200.97 1
Lead 100 05/02/2017 235810310070-1300.48 200.28 1
Nickel 93 05/02/2017 23589010070-1304.1 202.8 1
Selenium 94 05/02/2017 23588410070-1305.9 209.4 1
Silver 91 05/02/2017 23589110070-1300.35 200.0 1
Thallium 100 05/02/2017 235810410070-1300.096 200.0 1
Vanadium 110 05/02/2017 23589510070-1307.0 209.6 1
Zinc 87 05/02/2017 23588710070-1300.85 200.0 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 126 of 130
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Shealy Environmental Services, Inc.
CVAA - MB
Batch:Prep Method:
Prep Date:
Sample ID:SQ40848-001
40848 7470A
05/01/2017 1334Analytical Method:7470A
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Mercury 0.00010 05/04/2017 1605U0.00010 0.000028 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 127 of 130
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Shealy Environmental Services, Inc.
CVAA - LCS
Batch:Prep Method:
Prep Date:
Sample ID:SQ40848-002
40848 7470A
05/01/2017 1334Analytical Method:7470A
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Mercury 0.0020 05/04/2017 16071000.0020 80-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 128 of 130
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Shealy Environmental Services, Inc.
CVAA - MS
Batch:Prep Method:
Prep Date:
Sample ID:SD28007-006MS
40848 7470A
05/01/2017 1334Analytical Method:7470A
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Mercury 0.0021 05/02/2017 09511040.0020 85-1150.0 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 129 of 130
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Shealy Environmental Services, Inc.
CVAA - MSD
Batch:Prep Method:
Prep Date:
Sample ID:SD28007-006MD
40848 7470A
05/01/2017 1334Analytical Method:7470A
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Mercury 0.0021 05/02/2017 09531060.0020 85-1152.5 200.0 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 130 of 130
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Shealy Environmental Services, Inc.
Chain of Custody
and
Miscellaneous Documents
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
SHEALY ENVIRONMENTAL SERVICES, INC.
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
SHEALY ENVIRONMENTAL SERVICES, INC.
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
SHEALY ENVIRONMENTAL SERVICES, INC.
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
CDM Smith
5400 Glenwood Avenue
Suite 400
Raleigh, NC 27612
Attention: Mathew Colone
SD29002Lot Number:
Feltonsville LandfillProject Name:
05/09/2017Date Completed:
Catherine S. Dover
Project Manager
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
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SHEALY ENVIRONMENTAL SERVICES, INC.
Case Narrative
CDM Smith
Lot Number: SD29002
SC DHEC No: 32010 NC Field Parameters No: 5639 NELAC No: E87653 NC DENR No: 329
Project Name: Feltonsville Landfill
Project Number:
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
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Sample Summary
CDM Smith
Lot Number: SD29002
Project Name: Feltonsville Landfill
Project Number:
Sample Number Sample ID Matrix Date Sampled Date Received
001 04/28/2017 1430MW-4 Aqueous 04/29/2017
002 04/28/2017 1235MW-8 Aqueous 04/29/2017
003 04/28/2017 1320MW-11 Aqueous 04/29/2017
004 04/28/2017 1045MW-13 Aqueous 04/29/2017
005 04/28/2017 1120MW-14 Aqueous 04/29/2017
006 04/27/2017 1630MW-24 Aqueous
007 04/27/2017 1645MW-25 Aqueous
008 04/28/2017 1015MW-15 Aqueous 04/29/2017
009 04/28/2017 1315MW-17 Aqueous 04/29/2017
010 04/28/2017 1405MW-23 Aqueous 04/29/2017
011 04/28/2017 1415MW-22 Aqueous 04/29/2017
012 04/28/2017 1440MW-21 Aqueous 04/29/2017
013 04/28/2017 1450MW-26 Aqueous 04/29/2017
014 04/28/2017 1515MW-27 Aqueous 04/29/2017
015 04/28/2017 1545EQ BLANK Aqueous 04/29/2017
016 04/28/2017TRIP BLANK Aqueous 04/29/2017
017 04/28/2017 1315SW-1 Aqueous 04/29/2017
018 04/28/2017 1535SW-2 Aqueous 04/29/2017
019 04/28/2017 1505SW-3 Aqueous 04/29/2017
020 04/28/2017TRIP BLANK2 Aqueous 04/29/2017
(20 samples)
Page: 3 of 114
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Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-4
SD29002-001
04/28/2017 1430
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/01/2017 2227 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.74 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 0.73 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 4.2 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.57 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.54 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 4 of 114
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-4
SD29002-001
04/28/2017 1430
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/01/2017 2227 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 101 70-130
1,2-Dichloroethane-d4 103 70-130
Toluene-d8 104 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
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ICP-MS Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-4
SD29002-001
04/28/2017 1430
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 05/04/2017 1204 BNW 05/01/2017 0900 40840
2 3005A 6020B 1 05/05/2017 2211 MJI 05/01/2017 0900 40840
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020B 6.0 U 1ug/L0.506.0
Arsenic 7440-38-2 6020B 10 U 1ug/L1.310
Barium 7440-39-3 6020B 33 J 1ug/L0.63100
Beryllium 7440-41-7 6020B 1.0 U 1ug/L0.131.0
Cadmium 7440-43-9 6020B 1.0 U 2ug/L0.131.0
Chromium 7440-47-3 6020B 10 U 1ug/L1.310
Cobalt 7440-48-4 6020B 10 U 1ug/L0.6310
Copper 7440-50-8 6020B 10 U 1ug/L0.6310
Lead 7439-92-1 6020B 10 U 1ug/L0.2510
Nickel 7440-02-0 6020B 50 U 1ug/L1.350
Selenium 7782-49-2 6020B 10 U 1ug/L1.310
Silver 7440-22-4 6020B 10 U 1ug/L0.2510
Thallium 7440-28-0 6020B 5.5 U 1ug/L0.135.5
Vanadium 7440-62-2 6020B 5.6 J 1ug/L1.525
Zinc 7440-66-6 6020B 3.6 J 1ug/L2.510
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
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CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-4
SD29002-001
04/28/2017 1430
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 05/02/2017 1130 COH 05/02/2017 0901 40929
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Mercury 7439-97-6 7470A 0.00010 U 1mg/L0.0000280.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
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Shealy Environmental Services, Inc.
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-8
SD29002-002
04/28/2017 1235
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 05/02/2017 1737 BWS 40944
1 (BOD, 5 day) SM 5210B-2011 1 05/04/2017 0745 SLU 04/29/2017 1240 11313
1 (Chloride) 300.0 1 04/29/2017 1250 TAF 41011
1 (CO2 (calcula) SM 4500-CO2 D 1 05/02/2017 1737 BWS
1 (COD) SM 5220D-2011 1 05/06/2017 1117 TAF 05/04/2017 1037
1 (Nitrate - N) 300.0 1 04/29/2017 1250 TAF 40902
1 (Sulfate) 300.0 1 04/29/2017 1250 TAF 41010
1 (Sulfide) SM 4500-S2 F-2011 1 05/01/2017 1623 BWS 40932
1 (TDS) SM 2540C-2011 1 05/02/2017 1204 MGM 40919
1 (TOC) SM 5310C-2011 1 05/01/2017 2147 BWS 40876
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Alkalinity SM 2320B-20 120 1mg/L2.010
BOD, 5 day SM 5210B-20 2.0 U 1mg/L0.182.0
Chloride 300.0 7.3 1mg/L0.201.0
CO2 (calculation)124-38-9 SM 4500-CO2 110 1mg/L27
COD SM 5220D-20 10 U 1mg/L8.010
Nitrate - N 300.0 0.042 1mg/L0.00500.020
Sulfate 300.0 1.0 U 1mg/L0.201.0
Sulfide 18496-25-8 SM 4500-S2 1.0 U 1mg/L0.621.0
TDS SM 2540C-20 210 1mg/L3.410
TOC SM 5310C-20 0.74 J 1mg/L0.601.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 8 of 114
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Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-8
SD29002-002
04/28/2017 1235
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/01/2017 2248 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 1.2 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.60 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 1.2 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
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Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-8
SD29002-002
04/28/2017 1235
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/01/2017 2248 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 101 70-130
1,2-Dichloroethane-d4 105 70-130
Toluene-d8 103 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
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Dissolved Gases
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-8
SD29002-002
04/28/2017 1235
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 05/03/2017 1517 TML 41108
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Ethane 74-84-0 RSK - 175 10 U 1ug/L2.510
Ethene 74-85-1 RSK - 175 10 U 1ug/L2.510
Methane 74-82-8 RSK - 175 64 B 1ug/L2.510
Propane 74-98-6 RSK - 175 15 U 1ug/L3.515
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
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ICP-MS Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-8
SD29002-002
04/28/2017 1235
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 05/04/2017 1242 BNW 05/01/2017 0900 40840
2 3005A 6020B 1 05/05/2017 2238 MJI 05/01/2017 0900 40840
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020B 0.67 J 1ug/L0.506.0
Arsenic 7440-38-2 6020B 10 U 1ug/L1.310
Barium 7440-39-3 6020B 120 1ug/L0.63100
Beryllium 7440-41-7 6020B 1.0 U 1ug/L0.131.0
Cadmium 7440-43-9 6020B 1.0 U 2ug/L0.131.0
Chromium 7440-47-3 6020B 3.2 J 1ug/L1.310
Cobalt 7440-48-4 6020B 3.9 J 1ug/L0.6310
Copper 7440-50-8 6020B 4.6 J 1ug/L0.6310
Lead 7439-92-1 6020B 0.27 J 1ug/L0.2510
Nickel 7440-02-0 6020B 30 J 1ug/L1.350
Selenium 7782-49-2 6020B 10 U 1ug/L1.310
Silver 7440-22-4 6020B 10 U 1ug/L0.2510
Sodium 7440-23-5 6020B 6400 1ug/L50400
Thallium 7440-28-0 6020B 5.5 U 1ug/L0.135.5
Vanadium 7440-62-2 6020B 14 J 1ug/L1.525
Zinc 7440-66-6 6020B 3.9 J 1ug/L2.510
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 12 of 114
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Shealy Environmental Services, Inc.
CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-8
SD29002-002
04/28/2017 1235
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 05/02/2017 1132 COH 05/02/2017 0901 40929
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Mercury 7439-97-6 7470A 0.00010 U 1mg/L0.0000280.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 13 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-11
SD29002-003
04/28/2017 1320
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/01/2017 2310 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 14 of 114
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-11
SD29002-003
04/28/2017 1320
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/01/2017 2310 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 104 70-130
1,2-Dichloroethane-d4 107 70-130
Toluene-d8 105 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 15 of 114
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Shealy Environmental Services, Inc.
ICP-MS Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-11
SD29002-003
04/28/2017 1320
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 05/04/2017 1247 BNW 05/01/2017 0900 40840
2 3005A 6020B 1 05/05/2017 2244 MJI 05/01/2017 0900 40840
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020B 6.0 U 1ug/L0.506.0
Arsenic 7440-38-2 6020B 10 U 1ug/L1.310
Barium 7440-39-3 6020B 96 J 1ug/L0.63100
Beryllium 7440-41-7 6020B 1.0 U 1ug/L0.131.0
Cadmium 7440-43-9 6020B 1.0 U 2ug/L0.131.0
Chromium 7440-47-3 6020B 10 U 1ug/L1.310
Cobalt 7440-48-4 6020B 3.9 J 1ug/L0.6310
Copper 7440-50-8 6020B 10 U 1ug/L0.6310
Lead 7439-92-1 6020B 10 U 1ug/L0.2510
Nickel 7440-02-0 6020B 1.5 J 1ug/L1.350
Selenium 7782-49-2 6020B 10 U 1ug/L1.310
Silver 7440-22-4 6020B 10 U 1ug/L0.2510
Thallium 7440-28-0 6020B 5.5 U 1ug/L0.135.5
Vanadium 7440-62-2 6020B 2.3 J 1ug/L1.525
Zinc 7440-66-6 6020B 9.8 J 1ug/L2.510
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 16 of 114
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Shealy Environmental Services, Inc.
CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-11
SD29002-003
04/28/2017 1320
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 05/02/2017 1134 COH 05/02/2017 0901 40929
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Mercury 7439-97-6 7470A 0.00010 U 1mg/L0.0000280.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 17 of 114
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Shealy Environmental Services, Inc.
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-13
SD29002-004
04/28/2017 1045
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 05/02/2017 1743 BWS 40944
1 (BOD, 5 day) SM 5210B-2011 1 05/04/2017 0745 SLU 04/29/2017 1240 11313
1 (Chloride) 300.0 1 04/29/2017 1338 TAF 41011
1 (CO2 (calcula) SM 4500-CO2 D 1 05/02/2017 1743 BWS
1 (COD) SM 5220D-2011 1 05/06/2017 1117 TAF 05/04/2017 1037
1 (Nitrate - N) 300.0 1 04/29/2017 1338 TAF 40902
1 (Sulfate) 300.0 1 04/29/2017 1338 TAF 41010
1 (Sulfide) SM 4500-S2 F-2011 1 05/01/2017 1623 BWS 40932
1 (TOC) SM 5310C-2011 1 05/01/2017 2235 BWS 40876
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Alkalinity SM 2320B-20 190 1mg/L2.010
BOD, 5 day SM 5210B-20 2.0 U 1mg/L0.182.0
Chloride 300.0 29 1mg/L0.201.0
CO2 (calculation)124-38-9 SM 4500-CO2 420 1mg/L27
COD SM 5220D-20 16 1mg/L8.010
Nitrate - N 300.0 0.091 1mg/L0.00500.020
Sulfate 300.0 9.1 1mg/L0.201.0
Sulfide 18496-25-8 SM 4500-S2 1.0 U 1mg/L0.621.0
TOC SM 5310C-20 5.5 1mg/L0.601.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 18 of 114
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-13
SD29002-004
04/28/2017 1045
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/01/2017 2331 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 1.3 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 11 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 2.2 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 1.0 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 19 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-13
SD29002-004
04/28/2017 1045
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/01/2017 2331 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 102 70-130
1,2-Dichloroethane-d4 105 70-130
Toluene-d8 103 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 20 of 114
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Shealy Environmental Services, Inc.
Dissolved Gases
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-13
SD29002-004
04/28/2017 1045
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 05/03/2017 1530 TML 41108
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Ethane 74-84-0 RSK - 175 10 U 1ug/L2.510
Ethene 74-85-1 RSK - 175 10 U 1ug/L2.510
Methane 74-82-8 RSK - 175 170 B 1ug/L2.510
Propane 74-98-6 RSK - 175 15 U 1ug/L3.515
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 21 of 114
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Shealy Environmental Services, Inc.
ICP-MS Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-13
SD29002-004
04/28/2017 1045
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 05/04/2017 1253 BNW 05/01/2017 0900 40840
2 3005A 6020B 1 05/05/2017 2249 MJI 05/01/2017 0900 40840
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020B 6.0 U 1ug/L0.506.0
Arsenic 7440-38-2 6020B 2.6 J 1ug/L1.310
Barium 7440-39-3 6020B 380 1ug/L0.63100
Beryllium 7440-41-7 6020B 1.0 U 1ug/L0.131.0
Cadmium 7440-43-9 6020B 0.16 J 2ug/L0.131.0
Chromium 7440-47-3 6020B 10 U 1ug/L1.310
Cobalt 7440-48-4 6020B 5.7 J 1ug/L0.6310
Copper 7440-50-8 6020B 5.5 J 1ug/L0.6310
Lead 7439-92-1 6020B 10 U 1ug/L0.2510
Nickel 7440-02-0 6020B 24 J 1ug/L1.350
Selenium 7782-49-2 6020B 4.8 J 1ug/L1.310
Silver 7440-22-4 6020B 10 U 1ug/L0.2510
Thallium 7440-28-0 6020B 5.5 U 1ug/L0.135.5
Vanadium 7440-62-2 6020B 3.2 J 1ug/L1.525
Zinc 7440-66-6 6020B 38 1ug/L2.510
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 22 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-13
SD29002-004
04/28/2017 1045
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 05/02/2017 1136 COH 05/02/2017 0901 40929
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Mercury 7439-97-6 7470A 0.00036 1mg/L0.0000280.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 23 of 114
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Shealy Environmental Services, Inc.
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-14
SD29002-005
04/28/2017 1120
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 05/02/2017 1803 BWS 40944
1 (BOD, 5 day) SM 5210B-2011 1 05/04/2017 0745 SLU 04/29/2017 1240 11313
1 (Chloride) 300.0 1 04/29/2017 1350 TAF 41011
1 (CO2 (calcula) SM 4500-CO2 D 1 05/02/2017 1803 BWS
1 (COD) SM 5220D-2011 1 05/06/2017 1117 TAF 05/04/2017 1037
1 (Nitrate - N) 300.0 1 04/29/2017 1350 TAF 40902
1 (Sulfate) 300.0 1 04/29/2017 1350 TAF 41010
1 (Sulfide) SM 4500-S2 F-2011 1 05/01/2017 1623 BWS 40932
1 (TOC) SM 5310C-2011 1 05/01/2017 2252 BWS 40876
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Alkalinity SM 2320B-20 180 1mg/L2.010
BOD, 5 day SM 5210B-20 3.4 1mg/L0.182.0
Chloride 300.0 45 1mg/L0.201.0
CO2 (calculation)124-38-9 SM 4500-CO2 180 1mg/L27
COD SM 5220D-20 8.4 J 1mg/L8.010
Nitrate - N 300.0 0.019 J 1mg/L0.00500.020
Sulfate 300.0 3.4 1mg/L0.201.0
Sulfide 18496-25-8 SM 4500-S2 1.0 U 1mg/L0.621.0
TOC SM 5310C-20 2.8 1mg/L0.601.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 24 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-14
SD29002-005
04/28/2017 1120
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/01/2017 2353 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.80 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.43 J 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.62 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 25 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-14
SD29002-005
04/28/2017 1120
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/01/2017 2353 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 105 70-130
1,2-Dichloroethane-d4 106 70-130
Toluene-d8 103 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 26 of 114
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Shealy Environmental Services, Inc.
Dissolved Gases
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-14
SD29002-005
04/28/2017 1120
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 05/03/2017 1543 TML 41108
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Ethane 74-84-0 RSK - 175 10 U 1ug/L2.510
Ethene 74-85-1 RSK - 175 10 U 1ug/L2.510
Methane 74-82-8 RSK - 175 30 B 1ug/L2.510
Propane 74-98-6 RSK - 175 15 U 1ug/L3.515
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 27 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
ICP-MS Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-14
SD29002-005
04/28/2017 1120
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 05/04/2017 1258 BNW 05/01/2017 0900 40840
2 3005A 6020B 1 05/05/2017 2305 MJI 05/01/2017 0900 40840
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020B 1.1 J 1ug/L0.506.0
Arsenic 7440-38-2 6020B 10 U 1ug/L1.310
Barium 7440-39-3 6020B 120 1ug/L0.63100
Beryllium 7440-41-7 6020B 1.0 U 1ug/L0.131.0
Cadmium 7440-43-9 6020B 1.0 U 2ug/L0.131.0
Chromium 7440-47-3 6020B 10 U 1ug/L1.310
Cobalt 7440-48-4 6020B 10 U 1ug/L0.6310
Copper 7440-50-8 6020B 5.5 J 1ug/L0.6310
Lead 7439-92-1 6020B 10 U 1ug/L0.2510
Nickel 7440-02-0 6020B 4.6 J 1ug/L1.350
Selenium 7782-49-2 6020B 1.6 J 1ug/L1.310
Silver 7440-22-4 6020B 10 U 1ug/L0.2510
Thallium 7440-28-0 6020B 5.5 U 1ug/L0.135.5
Vanadium 7440-62-2 6020B 5.5 J 1ug/L1.525
Zinc 7440-66-6 6020B 5.0 J 1ug/L2.510
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 28 of 114
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Shealy Environmental Services, Inc.
CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-14
SD29002-005
04/28/2017 1120
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 05/02/2017 1138 COH 05/02/2017 0901 40929
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Mercury 7439-97-6 7470A 0.00043 1mg/L0.0000280.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 29 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-15
SD29002-008
04/28/2017 1015
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/02/2017 0014 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 3.2 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.92 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.56 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.61 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 30 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-15
SD29002-008
04/28/2017 1015
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/02/2017 0014 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 104 70-130
1,2-Dichloroethane-d4 104 70-130
Toluene-d8 104 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 31 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
ICP-MS Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-15
SD29002-008
04/28/2017 1015
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 05/04/2017 1303 BNW 05/01/2017 0900 40840
2 3005A 6020B 1 05/05/2017 2310 MJI 05/01/2017 0900 40840
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020B 6.0 U 1ug/L0.506.0
Arsenic 7440-38-2 6020B 10 U 1ug/L1.310
Barium 7440-39-3 6020B 190 1ug/L0.63100
Beryllium 7440-41-7 6020B 1.0 U 1ug/L0.131.0
Cadmium 7440-43-9 6020B 0.27 J 2ug/L0.131.0
Chromium 7440-47-3 6020B 10 U 1ug/L1.310
Cobalt 7440-48-4 6020B 10 U 1ug/L0.6310
Copper 7440-50-8 6020B 5.5 J 1ug/L0.6310
Lead 7439-92-1 6020B 10 U 1ug/L0.2510
Nickel 7440-02-0 6020B 23 J 1ug/L1.350
Selenium 7782-49-2 6020B 3.9 J 1ug/L1.310
Silver 7440-22-4 6020B 10 U 1ug/L0.2510
Thallium 7440-28-0 6020B 5.5 U 1ug/L0.135.5
Vanadium 7440-62-2 6020B 2.7 J 1ug/L1.525
Zinc 7440-66-6 6020B 5.6 J 1ug/L2.510
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 32 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-15
SD29002-008
04/28/2017 1015
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 05/02/2017 1141 COH 05/02/2017 0901 40929
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Mercury 7439-97-6 7470A 0.00012 1mg/L0.0000280.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 33 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-17
SD29002-009
04/28/2017 1315
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/02/2017 0036 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 1.8 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 12 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 1.4 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 34 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-17
SD29002-009
04/28/2017 1315
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/02/2017 0036 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 110 70-130
1,2-Dichloroethane-d4 108 70-130
Toluene-d8 108 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 35 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
ICP-MS Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-17
SD29002-009
04/28/2017 1315
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 05/04/2017 1309 BNW 05/01/2017 0900 40840
2 3005A 6020B 1 05/05/2017 2316 MJI 05/01/2017 0900 40840
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020B 6.0 U 1ug/L0.506.0
Arsenic 7440-38-2 6020B 8.9 J 1ug/L1.310
Barium 7440-39-3 6020B 100 1ug/L0.63100
Beryllium 7440-41-7 6020B 1.0 U 1ug/L0.131.0
Cadmium 7440-43-9 6020B 1.0 U 2ug/L0.131.0
Chromium 7440-47-3 6020B 10 U 1ug/L1.310
Cobalt 7440-48-4 6020B 10 U 1ug/L0.6310
Copper 7440-50-8 6020B 1.5 J 1ug/L0.6310
Lead 7439-92-1 6020B 0.50 J 1ug/L0.2510
Nickel 7440-02-0 6020B 2.9 J 1ug/L1.350
Selenium 7782-49-2 6020B 2.1 J 1ug/L1.310
Silver 7440-22-4 6020B 10 U 1ug/L0.2510
Thallium 7440-28-0 6020B 5.5 U 1ug/L0.135.5
Vanadium 7440-62-2 6020B 2.8 J 1ug/L1.525
Zinc 7440-66-6 6020B 5.7 J 1ug/L2.510
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 36 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-17
SD29002-009
04/28/2017 1315
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 05/02/2017 1147 COH 05/02/2017 0901 40929
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Mercury 7439-97-6 7470A 0.00010 U 1mg/L0.0000280.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 37 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-23
SD29002-010
04/28/2017 1405
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/02/2017 0057 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 11 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 38 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-23
SD29002-010
04/28/2017 1405
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/02/2017 0057 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 103 70-130
1,2-Dichloroethane-d4 106 70-130
Toluene-d8 101 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 39 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
ICP-MS Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-23
SD29002-010
04/28/2017 1405
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 05/04/2017 1314 BNW 05/01/2017 0900 40840
2 3005A 6020B 1 05/05/2017 2321 MJI 05/01/2017 0900 40840
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020B 6.0 U 1ug/L0.506.0
Arsenic 7440-38-2 6020B 2.3 J 1ug/L1.310
Barium 7440-39-3 6020B 210 1ug/L0.63100
Beryllium 7440-41-7 6020B 1.0 U 1ug/L0.131.0
Cadmium 7440-43-9 6020B 1.0 U 2ug/L0.131.0
Chromium 7440-47-3 6020B 10 U 1ug/L1.310
Cobalt 7440-48-4 6020B 2.4 J 1ug/L0.6310
Copper 7440-50-8 6020B 0.78 J 1ug/L0.6310
Lead 7439-92-1 6020B 10 U 1ug/L0.2510
Nickel 7440-02-0 6020B 50 U 1ug/L1.350
Selenium 7782-49-2 6020B 7.8 J 1ug/L1.310
Silver 7440-22-4 6020B 10 U 1ug/L0.2510
Thallium 7440-28-0 6020B 5.5 U 1ug/L0.135.5
Vanadium 7440-62-2 6020B 6.3 J 1ug/L1.525
Zinc 7440-66-6 6020B 15 1ug/L2.510
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 40 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-23
SD29002-010
04/28/2017 1405
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 05/02/2017 1149 COH 05/02/2017 0901 40929
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Mercury 7439-97-6 7470A 0.000041 J 1mg/L0.0000280.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 41 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-22
SD29002-011
04/28/2017 1415
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/02/2017 0119 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 2.4 J 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 42 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-22
SD29002-011
04/28/2017 1415
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/02/2017 0119 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 103 70-130
1,2-Dichloroethane-d4 105 70-130
Toluene-d8 103 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 43 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
ICP-MS Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-22
SD29002-011
04/28/2017 1415
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 05/04/2017 1320 BNW 05/01/2017 0900 40840
2 3005A 6020B 1 05/05/2017 2327 MJI 05/01/2017 0900 40840
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020B 6.0 U 1ug/L0.506.0
Arsenic 7440-38-2 6020B 5.6 J 1ug/L1.310
Barium 7440-39-3 6020B 240 1ug/L0.63100
Beryllium 7440-41-7 6020B 1.0 U 1ug/L0.131.0
Cadmium 7440-43-9 6020B 1.0 U 2ug/L0.131.0
Chromium 7440-47-3 6020B 10 U 1ug/L1.310
Cobalt 7440-48-4 6020B 4.3 J 1ug/L0.6310
Copper 7440-50-8 6020B 1.9 J 1ug/L0.6310
Lead 7439-92-1 6020B 0.54 J 1ug/L0.2510
Nickel 7440-02-0 6020B 1.6 J 1ug/L1.350
Selenium 7782-49-2 6020B 5.1 J 1ug/L1.310
Silver 7440-22-4 6020B 10 U 1ug/L0.2510
Thallium 7440-28-0 6020B 5.5 U 1ug/L0.135.5
Vanadium 7440-62-2 6020B 4.1 J 1ug/L1.525
Zinc 7440-66-6 6020B 4.9 J 1ug/L2.510
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 44 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-22
SD29002-011
04/28/2017 1415
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 05/02/2017 1156 COH 05/02/2017 0901 40929
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Mercury 7439-97-6 7470A 0.00010 U 1mg/L0.0000280.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 45 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-21
SD29002-012
04/28/2017 1440
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/02/2017 0140 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 46 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-21
SD29002-012
04/28/2017 1440
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/02/2017 0140 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 102 70-130
1,2-Dichloroethane-d4 106 70-130
Toluene-d8 104 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 47 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
ICP-MS Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-21
SD29002-012
04/28/2017 1440
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 05/04/2017 1325 BNW 05/01/2017 0900 40840
2 3005A 6020B 1 05/05/2017 2332 MJI 05/01/2017 0900 40840
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020B 6.0 U 1ug/L0.506.0
Arsenic 7440-38-2 6020B 10 U 1ug/L1.310
Barium 7440-39-3 6020B 8.3 J 1ug/L0.63100
Beryllium 7440-41-7 6020B 1.0 U 1ug/L0.131.0
Cadmium 7440-43-9 6020B 1.0 U 2ug/L0.131.0
Chromium 7440-47-3 6020B 10 U 1ug/L1.310
Cobalt 7440-48-4 6020B 10 U 1ug/L0.6310
Copper 7440-50-8 6020B 10 U 1ug/L0.6310
Lead 7439-92-1 6020B 0.81 J 1ug/L0.2510
Nickel 7440-02-0 6020B 50 U 1ug/L1.350
Selenium 7782-49-2 6020B 10 U 1ug/L1.310
Silver 7440-22-4 6020B 10 U 1ug/L0.2510
Thallium 7440-28-0 6020B 5.5 U 1ug/L0.135.5
Vanadium 7440-62-2 6020B 3.2 J 1ug/L1.525
Zinc 7440-66-6 6020B 10 U 1ug/L2.510
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 48 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-21
SD29002-012
04/28/2017 1440
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 05/02/2017 1158 COH 05/02/2017 0901 40929
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Mercury 7439-97-6 7470A 0.00010 U 1mg/L0.0000280.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 49 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-26
SD29002-013
04/28/2017 1450
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/02/2017 0202 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 2.1 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 3.3 1ug/L0.400.50
Chloroethane 75-00-3 8260B 2.6 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 1.9 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.95 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 50 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-26
SD29002-013
04/28/2017 1450
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/02/2017 0202 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 0.67 J 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 100 70-130
1,2-Dichloroethane-d4 105 70-130
Toluene-d8 101 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 51 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
ICP-MS Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-26
SD29002-013
04/28/2017 1450
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 05/04/2017 1330 BNW 05/01/2017 0900 40840
2 3005A 6020B 1 05/05/2017 2337 MJI 05/01/2017 0900 40840
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020B 6.0 U 1ug/L0.506.0
Arsenic 7440-38-2 6020B 1.5 J 1ug/L1.310
Barium 7440-39-3 6020B 81 J 1ug/L0.63100
Beryllium 7440-41-7 6020B 0.66 J 1ug/L0.131.0
Cadmium 7440-43-9 6020B 0.13 J 2ug/L0.131.0
Chromium 7440-47-3 6020B 10 U 1ug/L1.310
Cobalt 7440-48-4 6020B 14 1ug/L0.6310
Copper 7440-50-8 6020B 2.3 J 1ug/L0.6310
Lead 7439-92-1 6020B 1.4 J 1ug/L0.2510
Nickel 7440-02-0 6020B 6.9 J 1ug/L1.350
Selenium 7782-49-2 6020B 5.0 J 1ug/L1.310
Silver 7440-22-4 6020B 10 U 1ug/L0.2510
Thallium 7440-28-0 6020B 5.5 U 1ug/L0.135.5
Vanadium 7440-62-2 6020B 3.3 J 1ug/L1.525
Zinc 7440-66-6 6020B 17 1ug/L2.510
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 52 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-26
SD29002-013
04/28/2017 1450
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 05/02/2017 1200 COH 05/02/2017 0901 40929
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Mercury 7439-97-6 7470A 0.000028 J 1mg/L0.0000280.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 53 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-27
SD29002-014
04/28/2017 1515
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/02/2017 0223 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 4.2 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 9.4 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 1.8 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.40 J 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.51 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.60 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 54 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-27
SD29002-014
04/28/2017 1515
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/02/2017 0223 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 104 70-130
1,2-Dichloroethane-d4 107 70-130
Toluene-d8 103 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 55 of 114
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Shealy Environmental Services, Inc.
ICP-MS Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-27
SD29002-014
04/28/2017 1515
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 05/04/2017 1347 BNW 05/01/2017 0900 40840
2 3005A 6020B 1 05/05/2017 2343 MJI 05/01/2017 0900 40840
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020B 0.53 J 1ug/L0.506.0
Arsenic 7440-38-2 6020B 2.1 J 1ug/L1.310
Barium 7440-39-3 6020B 120 1ug/L0.63100
Beryllium 7440-41-7 6020B 1.0 U 1ug/L0.131.0
Cadmium 7440-43-9 6020B 1.0 U 2ug/L0.131.0
Chromium 7440-47-3 6020B 10 U 1ug/L1.310
Cobalt 7440-48-4 6020B 10 U 1ug/L0.6310
Copper 7440-50-8 6020B 1.9 J 1ug/L0.6310
Lead 7439-92-1 6020B 0.78 J 1ug/L0.2510
Nickel 7440-02-0 6020B 50 U 1ug/L1.350
Selenium 7782-49-2 6020B 1.5 J 1ug/L1.310
Silver 7440-22-4 6020B 10 U 1ug/L0.2510
Thallium 7440-28-0 6020B 5.5 U 1ug/L0.135.5
Vanadium 7440-62-2 6020B 21 J 1ug/L1.525
Zinc 7440-66-6 6020B 5.5 J 1ug/L2.510
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 56 of 114
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Shealy Environmental Services, Inc.
CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-27
SD29002-014
04/28/2017 1515
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 05/02/2017 1203 COH 05/02/2017 0901 40929
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Mercury 7439-97-6 7470A 0.000054 J 1mg/L0.0000280.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 57 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
EQ BLANK
SD29002-015
04/28/2017 1545
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/02/2017 0245 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 3.1 J 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 8.2 J 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 58 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
EQ BLANK
SD29002-015
04/28/2017 1545
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/02/2017 0245 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 103 70-130
1,2-Dichloroethane-d4 108 70-130
Toluene-d8 105 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 59 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
ICP-MS Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
EQ BLANK
SD29002-015
04/28/2017 1545
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 05/04/2017 1352 BNW 05/01/2017 0900 40840
2 3005A 6020B 1 05/05/2017 2348 MJI 05/01/2017 0900 40840
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020B 6.0 U 1ug/L0.506.0
Arsenic 7440-38-2 6020B 10 U 1ug/L1.310
Barium 7440-39-3 6020B 100 U 1ug/L0.63100
Beryllium 7440-41-7 6020B 1.0 U 1ug/L0.131.0
Cadmium 7440-43-9 6020B 1.0 U 2ug/L0.131.0
Chromium 7440-47-3 6020B 10 U 1ug/L1.310
Cobalt 7440-48-4 6020B 10 U 1ug/L0.6310
Copper 7440-50-8 6020B 10 U 1ug/L0.6310
Lead 7439-92-1 6020B 10 U 1ug/L0.2510
Nickel 7440-02-0 6020B 50 U 1ug/L1.350
Selenium 7782-49-2 6020B 10 U 1ug/L1.310
Silver 7440-22-4 6020B 10 U 1ug/L0.2510
Thallium 7440-28-0 6020B 5.5 U 1ug/L0.135.5
Vanadium 7440-62-2 6020B 1.7 J 1ug/L1.525
Zinc 7440-66-6 6020B 10 U 1ug/L2.510
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 60 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
EQ BLANK
SD29002-015
04/28/2017 1545
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 05/02/2017 1205 COH 05/02/2017 0901 40929
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Mercury 7439-97-6 7470A 0.00010 U 1mg/L0.0000280.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 61 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
TRIP BLANK
SD29002-016
04/28/2017
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/02/2017 0306 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 62 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
TRIP BLANK
SD29002-016
04/28/2017
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/02/2017 0306 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 101 70-130
1,2-Dichloroethane-d4 107 70-130
Toluene-d8 104 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 63 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
SW-1
SD29002-017
04/28/2017 1315
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/02/2017 0328 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 64 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
SW-1
SD29002-017
04/28/2017 1315
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/02/2017 0328 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 102 70-130
1,2-Dichloroethane-d4 109 70-130
Toluene-d8 103 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 65 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
ICP-MS Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
SW-1
SD29002-017
04/28/2017 1315
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 05/04/2017 1357 BNW 05/01/2017 0900 40840
2 3005A 6020B 1 05/05/2017 2353 MJI 05/01/2017 0900 40840
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020B 6.0 U 1ug/L0.506.0
Arsenic 7440-38-2 6020B 10 U 1ug/L1.310
Barium 7440-39-3 6020B 40 J 1ug/L0.63100
Beryllium 7440-41-7 6020B 1.0 U 1ug/L0.131.0
Cadmium 7440-43-9 6020B 1.0 U 2ug/L0.131.0
Chromium 7440-47-3 6020B 10 U 1ug/L1.310
Cobalt 7440-48-4 6020B 10 U 1ug/L0.6310
Copper 7440-50-8 6020B 1.6 J 1ug/L0.6310
Lead 7439-92-1 6020B 0.45 J 1ug/L0.2510
Nickel 7440-02-0 6020B 50 U 1ug/L1.350
Selenium 7782-49-2 6020B 10 U 1ug/L1.310
Silver 7440-22-4 6020B 10 U 1ug/L0.2510
Thallium 7440-28-0 6020B 5.5 U 1ug/L0.135.5
Vanadium 7440-62-2 6020B 3.3 J 1ug/L1.525
Zinc 7440-66-6 6020B 3.3 J 1ug/L2.510
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 66 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
SW-1
SD29002-017
04/28/2017 1315
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 05/02/2017 1207 COH 05/02/2017 0901 40929
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Mercury 7439-97-6 7470A 0.00010 U 1mg/L0.0000280.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 67 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
SW-2
SD29002-018
04/28/2017 1535
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/02/2017 0349 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 68 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
SW-2
SD29002-018
04/28/2017 1535
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/02/2017 0349 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 100 70-130
1,2-Dichloroethane-d4 104 70-130
Toluene-d8 102 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 69 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
ICP-MS Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
SW-2
SD29002-018
04/28/2017 1535
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 05/04/2017 1403 BNW 05/01/2017 0900 40840
2 3005A 6020B 1 05/06/2017 0010 MJI 05/01/2017 0900 40840
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020B 6.0 U 1ug/L0.506.0
Arsenic 7440-38-2 6020B 10 U 1ug/L1.310
Barium 7440-39-3 6020B 66 J 1ug/L0.63100
Beryllium 7440-41-7 6020B 1.0 U 1ug/L0.131.0
Cadmium 7440-43-9 6020B 1.0 U 2ug/L0.131.0
Chromium 7440-47-3 6020B 10 U 1ug/L1.310
Cobalt 7440-48-4 6020B 10 U 1ug/L0.6310
Copper 7440-50-8 6020B 1.5 J 1ug/L0.6310
Lead 7439-92-1 6020B 1.0 J 1ug/L0.2510
Nickel 7440-02-0 6020B 50 U 1ug/L1.350
Selenium 7782-49-2 6020B 1.5 J 1ug/L1.310
Silver 7440-22-4 6020B 10 U 1ug/L0.2510
Thallium 7440-28-0 6020B 5.5 U 1ug/L0.135.5
Vanadium 7440-62-2 6020B 4.0 J 1ug/L1.525
Zinc 7440-66-6 6020B 6.8 J 1ug/L2.510
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 70 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
SW-2
SD29002-018
04/28/2017 1535
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 05/02/2017 1213 COH 05/02/2017 0901 40929
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Mercury 7439-97-6 7470A 0.00010 U 1mg/L0.0000280.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 71 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
SW-3
SD29002-019
04/28/2017 1505
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/02/2017 0411 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 2.4 J 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
Dichlorodifluoromethane 75-71-8 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 72 of 114
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
SW-3
SD29002-019
04/28/2017 1505
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 05/02/2017 0411 ECP 40923
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 104 70-130
1,2-Dichloroethane-d4 105 70-130
Toluene-d8 103 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
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ICP-MS Metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
SW-3
SD29002-019
04/28/2017 1505
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 05/04/2017 1408 BNW 05/01/2017 0900 40840
2 3005A 6020B 1 05/06/2017 0015 MJI 05/01/2017 0900 40840
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Antimony 7440-36-0 6020B 6.0 U 1ug/L0.506.0
Arsenic 7440-38-2 6020B 10 U 1ug/L1.310
Barium 7440-39-3 6020B 41 J 1ug/L0.63100
Beryllium 7440-41-7 6020B 1.0 U 1ug/L0.131.0
Cadmium 7440-43-9 6020B 0.16 J 2ug/L0.131.0
Chromium 7440-47-3 6020B 10 U 1ug/L1.310
Cobalt 7440-48-4 6020B 10 U 1ug/L0.6310
Copper 7440-50-8 6020B 1.6 J 1ug/L0.6310
Lead 7439-92-1 6020B 0.68 J 1ug/L0.2510
Nickel 7440-02-0 6020B 50 U 1ug/L1.350
Selenium 7782-49-2 6020B 10 U 1ug/L1.310
Silver 7440-22-4 6020B 10 U 1ug/L0.2510
Thallium 7440-28-0 6020B 5.5 U 1ug/L0.135.5
Vanadium 7440-62-2 6020B 3.6 J 1ug/L1.525
Zinc 7440-66-6 6020B 4.6 J 1ug/L2.510
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
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CVAA
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
SW-3
SD29002-019
04/28/2017 1505
04/29/2017
Aqueous
Project Name: Feltonsville Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 05/02/2017 1216 COH 05/02/2017 0901 40929
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Mercury 7439-97-6 7470A 0.00010 U 1mg/L0.0000280.00010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
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QC Summary
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Shealy Environmental Services, Inc.
Inorganic non-metals - MB
Batch:
Sample ID:SQ40876-001
40876
Analytical Method:SM 5310C-2011
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
TOC 1.0 05/01/2017 1549U1.0 0.60 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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Shealy Environmental Services, Inc.
Inorganic non-metals - LCS
Batch:
Sample ID:SQ40876-002
40876
Analytical Method:SM 5310C-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
TOC 19 05/01/2017 1605952090-1101
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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Inorganic non-metals - MB
Batch:
Sample ID:SQ40902-001
40902
Analytical Method:300.0
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Nitrate - N 0.020 04/29/2017 0949U0.020 0.0050 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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Shealy Environmental Services, Inc.
Inorganic non-metals - LCS
Batch:
Sample ID:SQ40902-002
40902
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Nitrate - N 0.84 04/29/2017 10011050.80 90-1101
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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Shealy Environmental Services, Inc.
Inorganic non-metals - MS
Batch:
Sample ID:SD29002-002MS
40902
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Nitrate - N 0.84 04/29/2017 13141000.80 90-1100.042 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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Shealy Environmental Services, Inc.
Inorganic non-metals - MSD
Batch:
Sample ID:SD29002-002MD
40902
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Nitrate - N 0.81 04/29/2017 1326960.80 90-1104.1 200.042 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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Shealy Environmental Services, Inc.
Inorganic non-metals - MB
Batch:
Sample ID:SQ40919-001
40919
Analytical Method:SM 2540C-2011
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
TDS 10 05/02/2017 1204U103.4 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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Shealy Environmental Services, Inc.
Inorganic non-metals - LCS
Batch:
Sample ID:SQ40919-002
40919
Analytical Method:SM 2540C-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
TDS 1500 05/02/2017 120497150090-1101
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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Shealy Environmental Services, Inc.
Inorganic non-metals - MB
Batch:
Sample ID:SQ40932-001
40932
Analytical Method:SM 4500-S2 F-2011
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Sulfide 1.0 05/01/2017 1623U1.0 0.62 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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Shealy Environmental Services, Inc.
Inorganic non-metals - LCS
Batch:
Sample ID:SQ40932-002
40932
Analytical Method:SM 4500-S2 F-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Sulfide 9.4 05/01/2017 1623941080-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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Shealy Environmental Services, Inc.
Inorganic non-metals - MB
Batch:
Sample ID:SQ40944-001
40944
Analytical Method:SM 2320B-2011
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Alkalinity 10 05/02/2017 1544U102.0 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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Shealy Environmental Services, Inc.
Inorganic non-metals - LCS
Batch:
Sample ID:SQ40944-002
40944
Analytical Method:SM 2320B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Alkalinity 96 05/02/2017 15509610090-1101
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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Shealy Environmental Services, Inc.
Inorganic non-metals - MB
Batch:
Sample ID:SQ41010-001
41010
Analytical Method:300.0
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Sulfate 1.0 04/29/2017 0949U1.0 0.20 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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Shealy Environmental Services, Inc.
Inorganic non-metals - LCS
Batch:
Sample ID:SQ41010-002
41010
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Sulfate 22 04/29/2017 10011082090-1101
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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Inorganic non-metals - MS
Batch:
Sample ID:SD29002-002MS
41010
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Sulfate 19 04/29/2017 1314962090-1100.0 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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Inorganic non-metals - MSD
Batch:
Sample ID:SD29002-002MD
41010
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Sulfate 18 04/29/2017 1326922090-1104.4 200.0 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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Inorganic non-metals - MB
Batch:
Sample ID:SQ41011-001
41011
Analytical Method:300.0
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Chloride 1.0 04/29/2017 0949U1.0 0.20 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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Shealy Environmental Services, Inc.
Inorganic non-metals - LCS
Batch:
Sample ID:SQ41011-002
41011
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Chloride 20 04/29/2017 1001992090-1101
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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Shealy Environmental Services, Inc.
Inorganic non-metals - MS
Batch:
Sample ID:SD29002-002MS
41011
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Chloride 26 04/29/2017 1314942090-1107.3 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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Inorganic non-metals - MSD
Batch:
Sample ID:SD29002-002MD
41011
Analytical Method:300.0
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Chloride 25 04/29/2017 1326902090-1102.9 207.3 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:SQ40923-001
40923 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Acetone 10 05/01/2017 2142U102.0 ug/L1
Acrylonitrile 5.0 05/01/2017 2142U5.0 0.80 ug/L1
Benzene 0.50 05/01/2017 2142U0.50 0.40 ug/L1
Bromochloromethane 0.50 05/01/2017 2142U0.50 0.40 ug/L1
Bromodichloromethane 0.50 05/01/2017 2142U0.50 0.40 ug/L1
Bromoform 0.50 05/01/2017 2142U0.50 0.40 ug/L1
Bromomethane (Methyl bromide)0.50 05/01/2017 2142U0.50 0.40 ug/L1
2-Butanone (MEK)10 05/01/2017 2142U102.0 ug/L1
Carbon disulfide 0.50 05/01/2017 2142U0.50 0.40 ug/L1
Carbon tetrachloride 0.50 05/01/2017 2142U0.50 0.40 ug/L1
Chlorobenzene 0.50 05/01/2017 2142U0.50 0.40 ug/L1
Chloroethane 0.50 05/01/2017 2142U0.50 0.40 ug/L1
Chloroform 0.50 05/01/2017 2142U0.50 0.40 ug/L1
Chloromethane (Methyl chloride)0.50 05/01/2017 2142U0.50 0.40 ug/L1
1,2-Dibromo-3-chloropropane (DBCP)0.50 05/01/2017 2142U0.50 0.40 ug/L1
Dibromochloromethane 0.50 05/01/2017 2142U0.50 0.40 ug/L1
1,2-Dibromoethane (EDB)0.50 05/01/2017 2142U0.50 0.40 ug/L1
Dibromomethane (Methylene bromide)0.50 05/01/2017 2142U0.50 0.40 ug/L1
trans-1,4-Dichloro-2-butene 2.0 05/01/2017 2142U2.0 0.40 ug/L1
1,2-Dichlorobenzene 0.50 05/01/2017 2142U0.50 0.40 ug/L1
1,4-Dichlorobenzene 0.50 05/01/2017 2142U0.50 0.40 ug/L1
Dichlorodifluoromethane 0.50 05/01/2017 2142U0.50 0.40 ug/L1
1,1-Dichloroethane 0.50 05/01/2017 2142U0.50 0.40 ug/L1
1,2-Dichloroethane 0.50 05/01/2017 2142U0.50 0.40 ug/L1
cis-1,2-Dichloroethene 0.50 05/01/2017 2142U0.50 0.40 ug/L1
1,1-Dichloroethene 0.50 05/01/2017 2142U0.50 0.40 ug/L1
trans-1,2-Dichloroethene 0.50 05/01/2017 2142U0.50 0.40 ug/L1
1,2-Dichloropropane 0.50 05/01/2017 2142U0.50 0.40 ug/L1
cis-1,3-Dichloropropene 0.50 05/01/2017 2142U0.50 0.40 ug/L1
trans-1,3-Dichloropropene 0.50 05/01/2017 2142U0.50 0.40 ug/L1
Ethylbenzene 0.50 05/01/2017 2142U0.50 0.40 ug/L1
2-Hexanone 10 05/01/2017 2142U102.0 ug/L1
Methyl iodide (Iodomethane)5.0 05/01/2017 2142U5.0 0.40 ug/L1
4-Methyl-2-pentanone 10 05/01/2017 2142U102.0 ug/L1
Methylene chloride 0.50 05/01/2017 2142U0.50 0.40 ug/L1
Styrene 0.50 05/01/2017 2142U0.50 0.40 ug/L1
1,1,1,2-Tetrachloroethane 0.50 05/01/2017 2142U0.50 0.40 ug/L1
1,1,2,2-Tetrachloroethane 0.50 05/01/2017 2142U0.50 0.40 ug/L1
Tetrachloroethene 0.50 05/01/2017 2142U0.50 0.40 ug/L1
Toluene 0.50 05/01/2017 2142U0.50 0.40 ug/L1
1,1,1-Trichloroethane 0.50 05/01/2017 2142U0.50 0.40 ug/L1
1,1,2-Trichloroethane 0.50 05/01/2017 2142U0.50 0.40 ug/L1
Trichloroethene 0.50 05/01/2017 2142U0.50 0.40 ug/L1
Trichlorofluoromethane 0.50 05/01/2017 2142U0.50 0.40 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 97 of 114
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:SQ40923-001
40923 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
1,2,3-Trichloropropane 0.50 05/01/2017 2142U0.50 0.40 ug/L1
Vinyl acetate 5.0 05/01/2017 2142U5.0 1.2 ug/L1
Vinyl chloride 0.50 05/01/2017 2142U0.50 0.40 ug/L1
Xylenes (total)1.0 05/01/2017 2142U1.0 0.40 ug/L1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 104 70-130
1,2-Dichloroethane-d4 104 70-130
Toluene-d8 105 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 98 of 114
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:SQ40923-002
40923 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Acetone 120 05/01/2017 204311610060-1401
Acrylonitrile 120 05/01/2017 204312310060-1401
Benzene 54 05/01/2017 20431095070-1301
Bromochloromethane 58 05/01/2017 20431165070-1301
Bromodichloromethane 55 05/01/2017 20431115070-1301
Bromoform 53 05/01/2017 20431065070-1301
Bromomethane (Methyl bromide)52 05/01/2017 20431035060-1401
2-Butanone (MEK)110 05/01/2017 204311110060-1401
Carbon disulfide 57 05/01/2017 20431135060-1401
Carbon tetrachloride 51 05/01/2017 20431025070-1301
Chlorobenzene 55 05/01/2017 20431115070-1301
Chloroethane 54 05/01/2017 20431085060-1401
Chloroform 59 05/01/2017 20431175070-1301
Chloromethane (Methyl chloride)52 05/01/2017 20431055060-1401
1,2-Dibromo-3-chloropropane (DBCP)49 05/01/2017 2043975070-1301
Dibromochloromethane 56 05/01/2017 20431115070-1301
1,2-Dibromoethane (EDB)53 05/01/2017 20431055070-1301
Dibromomethane (Methylene bromide)54 05/01/2017 20431085070-1301
trans-1,4-Dichloro-2-butene 50 05/01/2017 20431005034-1421
1,2-Dichlorobenzene 53 05/01/2017 20431065070-1301
1,4-Dichlorobenzene 53 05/01/2017 20431075070-1301
Dichlorodifluoromethane 50 05/01/2017 2043995060-1401
1,1-Dichloroethane 59 05/01/2017 20431185070-1301
1,2-Dichloroethane 55 05/01/2017 20431095070-1301
cis-1,2-Dichloroethene 59 05/01/2017 20431185070-1301
1,1-Dichloroethene 55 05/01/2017 20431115070-1301
trans-1,2-Dichloroethene 60 05/01/2017 20431205070-1301
1,2-Dichloropropane 56 05/01/2017 20431125070-1301
cis-1,3-Dichloropropene 56 05/01/2017 20431125070-1301
trans-1,3-Dichloropropene 55 05/01/2017 20431095070-1301
Ethylbenzene 55 05/01/2017 20431095070-1301
2-Hexanone 94 05/01/2017 20439410060-1401
Methyl iodide (Iodomethane)56 05/01/2017 20431135070-1301
4-Methyl-2-pentanone 100 05/01/2017 204310210060-1401
Methylene chloride 55 05/01/2017 20431105070-1301
Styrene 56 05/01/2017 20431115070-1301
1,1,1,2-Tetrachloroethane 52 05/01/2017 20431055070-1301
1,1,2,2-Tetrachloroethane 49 05/01/2017 2043985070-1301
Tetrachloroethene 58 05/01/2017 20431165070-1301
Toluene 58 05/01/2017 20431165070-1301
1,1,1-Trichloroethane 52 05/01/2017 20431055070-1301
1,1,2-Trichloroethane 52 05/01/2017 20431045070-1301
Trichloroethene 55 05/01/2017 20431115070-1301
Trichlorofluoromethane 54 05/01/2017 20431075060-1401
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 99 of 114
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:SQ40923-002
40923 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
1,2,3-Trichloropropane 54 05/01/2017 20431095070-1301
Vinyl acetate 51 05/01/2017 20431015060-1401
Vinyl chloride 56 05/01/2017 20431125060-1401
Xylenes (total)110 05/01/2017 204310810070-1301
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 102 70-130
1,2-Dichloroethane-d4 102 70-130
Toluene-d8 104 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 100 of 114
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS - Duplicate
Batch:Prep Method:
Sample ID:SD29002-001DU
40923 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q Analysis Date% RPD
% RPD
Limit
Sample
Amount
Dil(ug/L)(ug/L)
Acetone 1.0 05/02/2017 0537U0.00 20ND1
Acrylonitrile 1.0 05/02/2017 0537U0.00 20ND1
Benzene 1.0 05/02/2017 0537U0.00 20ND1
Bromochloromethane 1.0 05/02/2017 0537U0.00 20ND1
Bromodichloromethane 1.0 05/02/2017 0537U0.00 20ND1
Bromoform 1.0 05/02/2017 0537U0.00 20ND1
Bromomethane (Methyl bromide)1.0 05/02/2017 0537U0.00 20ND1
2-Butanone (MEK)1.0 05/02/2017 0537U0.00 20ND1
Carbon disulfide 1.0 05/02/2017 0537U0.00 20ND1
Carbon tetrachloride 1.0 05/02/2017 0537U0.00 20ND1
Chlorobenzene 1.0 05/02/2017 0537U0.00 20ND1
Chloroethane 1.0 05/02/2017 0537U0.00 20ND1
Chloroform 0.79 05/02/2017 05376.3 200.74 1
Chloromethane (Methyl chloride)1.0 05/02/2017 0537U0.00 20ND1
1,2-Dibromo-3-chloropropane (DBCP)1.0 05/02/2017 0537U0.00 20ND1
Dibromochloromethane 1.0 05/02/2017 0537U0.00 20ND1
1,2-Dibromoethane (EDB)1.0 05/02/2017 0537U0.00 20ND1
Dibromomethane (Methylene bromide)1.0 05/02/2017 0537U0.00 20ND1
trans-1,4-Dichloro-2-butene 1.0 05/02/2017 0537U0.00 20ND1
1,2-Dichlorobenzene 1.0 05/02/2017 0537U0.00 20ND1
1,4-Dichlorobenzene 1.0 05/02/2017 0537U0.00 20ND1
Dichlorodifluoromethane 0.81 05/02/2017 05379.5 200.73 1
1,1-Dichloroethane 4.2 05/02/2017 05370.19 204.2 1
1,2-Dichloroethane 1.0 05/02/2017 0537U0.00 20ND1
1,1-Dichloroethene 1.0 05/02/2017 0537U0.00 20ND1
cis-1,2-Dichloroethene 0.46 05/02/2017 0537+21 200.57 1
trans-1,2-Dichloroethene 1.0 05/02/2017 0537U0.00 20ND1
1,2-Dichloropropane 1.0 05/02/2017 0537U0.00 20ND1
cis-1,3-Dichloropropene 1.0 05/02/2017 0537U0.00 20ND1
trans-1,3-Dichloropropene 1.0 05/02/2017 0537U0.00 20ND1
Ethylbenzene 1.0 05/02/2017 0537U0.00 20ND1
2-Hexanone 1.0 05/02/2017 0537U0.00 20ND1
Methyl iodide (Iodomethane)1.0 05/02/2017 0537U0.00 20ND1
4-Methyl-2-pentanone 1.0 05/02/2017 0537U0.00 20ND1
Methylene chloride 1.0 05/02/2017 0537U0.00 20ND1
Styrene 1.0 05/02/2017 0537U0.00 20ND1
1,1,1,2-Tetrachloroethane 1.0 05/02/2017 0537U0.00 20ND1
1,1,2,2-Tetrachloroethane 1.0 05/02/2017 0537U0.00 20ND1
Tetrachloroethene 0.51 05/02/2017 05375.0 200.54 1
Toluene 1.0 05/02/2017 0537U0.00 20ND1
1,1,1-Trichloroethane 1.0 05/02/2017 0537U0.00 20ND1
1,1,2-Trichloroethane 1.0 05/02/2017 0537U0.00 20ND1
Trichloroethene 1.0 05/02/2017 0537U0.00 20ND1
Trichlorofluoromethane 1.0 05/02/2017 0537U0.00 20ND1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 101 of 114
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS - Duplicate
Batch:Prep Method:
Sample ID:SD29002-001DU
40923 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q Analysis Date% RPD
% RPD
Limit
Sample
Amount
Dil(ug/L)(ug/L)
1,2,3-Trichloropropane 1.0 05/02/2017 0537U0.00 20ND1
Vinyl acetate 1.0 05/02/2017 0537U0.00 20ND1
Vinyl chloride 1.0 05/02/2017 0537U0.00 20ND1
Xylenes (total)1.0 05/02/2017 0537U0.00 20ND1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 108 70-130
1,2-Dichloroethane-d4 109 70-130
Toluene-d8 105 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 102 of 114
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Sample ID:SD29002-002MS
40923 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
Acetone 110 05/02/2017 055910810060-1400.0 1
Acrylonitrile 130 05/02/2017 055913210060-1400.0 1
Benzene 57 05/02/2017 05591135070-1300.0 1
Bromochloromethane 60 05/02/2017 05591205070-1300.0 1
Bromodichloromethane 58 05/02/2017 05591165070-1300.0 1
Bromoform 53 05/02/2017 05591055070-1300.0 1
Bromomethane (Methyl bromide)59 05/02/2017 05591185060-1400.0 1
2-Butanone (MEK)110 05/02/2017 055910710060-1400.0 1
Carbon disulfide 61 05/02/2017 05591225060-1400.0 1
Carbon tetrachloride 58 05/02/2017 05591155070-1300.0 1
Chlorobenzene 56 05/02/2017 05591125070-1300.0 1
Chloroethane 59 05/02/2017 05591195060-1400.0 1
Chloroform 63 05/02/2017 05591265070-1300.0 1
Chloromethane (Methyl chloride)59 05/02/2017 05591185020-1580.0 1
1,2-Dibromo-3-chloropropane (DBCP)47 05/02/2017 0559955070-1300.0 1
Dibromochloromethane 56 05/02/2017 05591125070-1300.0 1
1,2-Dibromoethane (EDB)52 05/02/2017 05591045070-1300.0 1
Dibromomethane (Methylene bromide)55 05/02/2017 05591095070-1300.0 1
trans-1,4-Dichloro-2-butene 47 05/02/2017 0559935034-1420.0 1
1,2-Dichlorobenzene 53 05/02/2017 05591075070-1300.0 1
1,4-Dichlorobenzene 52 05/02/2017 05591045070-1300.0 1
Dichlorodifluoromethane 57 05/02/2017 05591135060-1400.0 1
1,1-Dichloroethane 65 05/02/2017 05591285070-1301.2 1
1,2-Dichloroethane 59 05/02/2017 05591175070-1300.0 1
1,1-Dichloroethene 61 05/02/2017 05591215070-1300.60 1
cis-1,2-Dichloroethene 61 05/02/2017 05591225070-1300.0 1
trans-1,2-Dichloroethene 65 05/02/2017 05591285070-1301.2 1
1,2-Dichloropropane 58 05/02/2017 05591165070-1300.0 1
cis-1,3-Dichloropropene 56 05/02/2017 05591125070-1300.0 1
trans-1,3-Dichloropropene 54 05/02/2017 05591075070-1300.0 1
Ethylbenzene 55 05/02/2017 05591115070-1300.0 1
2-Hexanone 91 05/02/2017 05599110060-1400.0 1
Methyl iodide (Iodomethane)63 05/02/2017 05591265070-1300.0 1
4-Methyl-2-pentanone 100 05/02/2017 055910110060-1400.0 1
Methylene chloride 57 05/02/2017 05591135070-1300.0 1
Styrene 56 05/02/2017 05591125070-1300.0 1
1,1,1,2-Tetrachloroethane 53 05/02/2017 05591075070-1300.0 1
1,1,2,2-Tetrachloroethane 50 05/02/2017 05591015070-1300.0 1
Tetrachloroethene 59 05/02/2017 05591185070-1300.0 1
Toluene 59 05/02/2017 05591185070-1300.0 1
1,1,1-Trichloroethane 58 05/02/2017 05591155070-1300.0 1
1,1,2-Trichloroethane 52 05/02/2017 05591035070-1300.0 1
Trichloroethene 55 05/02/2017 05591105070-1300.0 1
Trichlorofluoromethane 66 05/02/2017 05591325060-1400.0 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 103 of 114
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Shealy Environmental Services, Inc.
Volatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Sample ID:SD29002-002MS
40923 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
1,2,3-Trichloropropane 52 05/02/2017 05591045070-1300.0 1
Vinyl acetate 54 05/02/2017 05591085029-1970.0 1
Vinyl chloride 63 05/02/2017 05591265060-1400.0 1
Xylenes (total)110 05/02/2017 055910810070-1300.0 1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 101 70-130
1,2-Dichloroethane-d4 105 70-130
Toluene-d8 102 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 104 of 114
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Shealy Environmental Services, Inc.
Dissolved Gases - MB
Batch:
Sample ID:SQ41108-001
41108
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Ethane 10 05/03/2017 1304U102.5 ug/L1
Ethene 10 05/03/2017 1304U102.5 ug/L1
Methane 2.9 05/03/2017 1304J102.5 ug/L1
Propane 15 05/03/2017 1304U153.5 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 105 of 114
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Shealy Environmental Services, Inc.
Dissolved Gases - LCS
Batch:
Sample ID:SQ41108-002
41108
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Ethane 460 05/03/2017 12458255070-1301
Ethene 430 05/03/2017 12458352070-1301
Methane 230 05/03/2017 12457930070-1301
Propane 690 05/03/2017 1245N16742070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 106 of 114
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Shealy Environmental Services, Inc.
ICP-MS Metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:SQ40840-001
40840 3005A
05/01/2017 900Analytical Method:6020B
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Antimony 6.0 05/04/2017 1153U6.0 0.50 ug/L1
Arsenic 10 05/04/2017 1153U101.3 ug/L1
Barium 100 05/04/2017 1153U1000.63 ug/L1
Beryllium 1.0 05/04/2017 1153U1.0 0.13 ug/L1
Cadmium 1.0 05/05/2017 2201U1.0 0.13 ug/L1
Chromium 10 05/04/2017 1153U101.3 ug/L1
Cobalt 10 05/04/2017 1153U100.63 ug/L1
Copper 10 05/04/2017 1153U100.63 ug/L1
Lead 10 05/04/2017 1153U100.25 ug/L1
Nickel 50 05/04/2017 1153U501.3 ug/L1
Selenium 10 05/04/2017 1153U101.3 ug/L1
Silver 10 05/04/2017 1153U100.25 ug/L1
Sodium 400 05/04/2017 1153U40050ug/L1
Thallium 5.5 05/04/2017 1153U5.5 0.13 ug/L1
Vanadium 25 05/04/2017 1153U251.5 ug/L1
Zinc 10 05/04/2017 1153U102.5 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 107 of 114
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Shealy Environmental Services, Inc.
ICP-MS Metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:SQ40840-002
40840 3005A
05/01/2017 900Analytical Method:6020B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Antimony 98 05/04/2017 11599810080-1201
Arsenic 100 05/04/2017 115910410080-1201
Barium 98 05/04/2017 11599810080-1201
Beryllium 100 05/04/2017 115910110080-1201
Cadmium 100 05/05/2017 220610010080-1201
Chromium 97 05/04/2017 11599710080-1201
Cobalt 100 05/04/2017 115910010080-1201
Copper 100 05/04/2017 115910410080-1201
Lead 100 05/04/2017 115910010080-1201
Nickel 100 05/04/2017 115910010080-1201
Selenium 110 05/04/2017 115910610080-1201
Silver 100 05/04/2017 115910210080-1201
Sodium 970 05/04/2017 115997100080-1201
Thallium 100 05/04/2017 115910010080-1201
Vanadium 100 05/04/2017 115910010080-1201
Zinc 110 05/04/2017 115910610080-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 108 of 114
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Shealy Environmental Services, Inc.
ICP-MS Metals - MS
Batch:Prep Method:
Prep Date:
Sample ID:SD29002-001MS
40840 3005A
05/01/2017 900Analytical Method:6020B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
Antimony 100 05/04/2017 121010010070-1300.0 1
Arsenic 100 05/04/2017 121010310070-1300.0 1
Barium 130 05/04/2017 12109910070-130331
Beryllium 99 05/04/2017 12109910070-1300.0 1
Cadmium 98 05/05/2017 22179810070-1300.0 1
Chromium 93 05/04/2017 12109310070-1300.0 1
Cobalt 96 05/04/2017 12109610070-1300.0 1
Copper 98 05/04/2017 12109810070-1300.0 1
Lead 100 05/04/2017 121010010070-1300.0 1
Nickel 94 05/04/2017 12109410070-1300.0 1
Selenium 98 05/04/2017 12109810070-1300.0 1
Silver 100 05/04/2017 121010110070-1300.0 1
Thallium 100 05/04/2017 121010110070-1300.0 1
Vanadium 100 05/04/2017 12109610070-1305.6 1
Zinc 100 05/04/2017 12109710070-1303.6 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 109 of 114
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Shealy Environmental Services, Inc.
ICP-MS Metals - MSD
Batch:Prep Method:
Prep Date:
Sample ID:SD29002-001MD
40840 3005A
05/01/2017 900Analytical Method:6020B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
Antimony 98 05/04/2017 12159810070-1302.5 200.0 1
Arsenic 100 05/04/2017 121510210070-1300.78 200.0 1
Barium 130 05/04/2017 12159710070-1301.3 20331
Beryllium 98 05/04/2017 12159810070-1301.1 200.0 1
Cadmium 97 05/05/2017 22229710070-1300.92 200.0 1
Chromium 92 05/04/2017 12159210070-1300.92 200.0 1
Cobalt 95 05/04/2017 12159510070-1301.6 200.0 1
Copper 97 05/04/2017 12159710070-1300.46 200.0 1
Lead 99 05/04/2017 12159910070-1301.5 200.0 1
Nickel 93 05/04/2017 12159310070-1301.4 200.0 1
Selenium 98 05/04/2017 12159810070-1300.67 200.0 1
Silver 99 05/04/2017 12159910070-1302.6 200.0 1
Thallium 100 05/04/2017 121510010070-1301.1 200.0 1
Vanadium 100 05/04/2017 12159510070-1300.89 205.6 1
Zinc 100 05/04/2017 12159610070-1300.50 203.6 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 110 of 114
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Shealy Environmental Services, Inc.
CVAA - MB
Batch:Prep Method:
Prep Date:
Sample ID:SQ40929-001
40929 7470A
05/02/2017 901Analytical Method:7470A
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Mercury 0.00010 05/02/2017 1121U0.00010 0.000028 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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Shealy Environmental Services, Inc.
CVAA - LCS
Batch:Prep Method:
Prep Date:
Sample ID:SQ40929-002
40929 7470A
05/02/2017 901Analytical Method:7470A
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Mercury 0.0022 05/02/2017 11231080.0020 80-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
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Shealy Environmental Services, Inc.
CVAA - MS
Batch:Prep Method:
Prep Date:
Sample ID:SD29002-010MS
40929 7470A
05/02/2017 901Analytical Method:7470A
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Mercury 0.0015 05/02/2017 1152N700.0020 85-1150.000041 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 113 of 114
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Shealy Environmental Services, Inc.
CVAA - MSD
Batch:Prep Method:
Prep Date:
Sample ID:SD29002-010MD
40929 7470A
05/02/2017 901Analytical Method:7470A
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Mercury 0.0014 05/02/2017 1154N690.0020 85-1151.8 200.000041 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 114 of 114
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Shealy Environmental Services, Inc.
Chain of Custody
and
Miscellaneous Documents
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Shealy Environmental Services, Inc.
SHEALY ENVIRONMENTAL SERVICES, INC.
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
SHEALY ENVIRONMENTAL SERVICES, INC.
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
SHEALY ENVIRONMENTAL SERVICES, INC.
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
SHEALY ENVIRONMENTAL SERVICES, INC.
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Pace Analytical Energy Services LLC
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
Report ID: 22501 - 922953 Page 1 of 27
Cathy Dover
Shealy Environmental Services, Inc.
106 Vantage Point Drive
West Columbia, SC 29172
May 12, 2017
RE:
Pace Workorder:
FELTONSVILLE LF / SD28008
Dear Cathy Dover:
22501
Enclosed are the analytical results for sample(s) received by the laboratory on Wednesday, May 03, 2017.
Results reported herein conform to the most current NELAC standards, where applicable, unless otherwise
narrated in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Enclosures
Ruth Welsh 05/12/2017
Ruth.Welsh@pacelabs.com
Total Number of Pages ____
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Please email PAESfeedback@pacelabs.com.
Customer Service Representative
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Report ID: 22501 - 922953 Page 2 of 27
LABORATORY ACCREDITATIONS & CERTIFICATIONS
Pennsylvania Department of Environmental Protection, Bureau of Laboratories
02-00538
NELAP Non-Potable Water and Solid & Hazardous Waste
Accreditor:
Accreditation ID:
Scope:
West Virginia Department of Environmental Protection, Division of Water and Waste
Management
395
Non-Potable Water
Accreditor:
Accreditation ID:
Scope:
South Carolina Department of Health and Environmental Control, Office of Environmental
Laboratory Certification
89009003
Clean Water Act (CWA); Resource Conservation and Recovery Act (RCRA)
Accreditor:
Accreditation ID:
Scope:
NELAP: New Jersey, Department of Environmental Protection
PA026
Non-Potable Water; Solid and Chemical Materials
Accreditor:
Accreditation ID:
Scope:
NELAP: New York, Department of Health Wadsworth Center
11815
Non-Potable Water; Solid and Hazardous Waste
Accreditor:
Accreditation ID:
Scope:
State of Connecticut, Department of Public Health, Division of Environmental Health
PH-0263
Clean Water Act (CWA) Resource Conservation and Recovery Act (RCRA)
Accreditor:
Accreditation ID:
Scope:
NELAP: Texas, Commission on Environmental Quality
T104704453-09-TX
Non-Potable Water
Accreditor:
Accreditation ID:
Scope:
State of New Hampshire
299409
Non-potable water
Accreditor:
Accreditation ID:
Scope:
State of Georgia
Chapter 391-3-26
As per the Georgia EPD Rules and Regulations for Commercial Laboratories, PAES is
accredited by the Pennsylvania Department of Environmental Protection Bureau of
Laboratories under the National Environmental Laboratory Approval Program (NELAC).
Accreditor:
Accreditation ID:
Scope:
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Report ID: 22501 - 922953 Page 3 of 27
SAMPLE SUMMARY
Workorder:22501 FELTONSVILLE LF / SD28008
Lab ID Sample ID Matrix Date Collected Date Received
225010001 MW-2 Water 4/27/2017 10:20 5/3/2017 09:45
225010002 MW-8 Water 4/28/2017 12:35 5/3/2017 09:45
225010003 MW-8 Bubble Strip 4/28/2017 12:35 5/3/2017 09:45
225010004 MW-9 Water 4/27/2017 13:00 5/3/2017 09:45
225010005 MW-9 Bubble Strip 4/27/2017 13:00 5/3/2017 09:45
225010006 MW-10 Water 4/27/2017 14:05 5/3/2017 09:45
225010007 MW-10 Bubble Strip 4/27/2017 14:05 5/3/2017 09:45
225010008 MW-12 Water 4/27/2017 16:15 5/3/2017 09:45
225010009 MW-12 Bubble Strip 4/27/2017 16:15 5/3/2017 09:45
225010010 MW-13 Water 4/28/2017 10:45 5/3/2017 09:45
225010011 MW-13 Bubble Strip 4/28/2017 10:45 5/3/2017 09:45
225010012 MW-14 Water 4/28/2017 11:20 5/3/2017 09:45
225010013 MW-14 Bubble Strip 4/28/2017 11:20 5/3/2017 09:45
225010014 MW-19 Water 4/27/2017 13:20 5/3/2017 09:45
225010015 MW-19 Bubble Strip 4/27/2017 13:20 5/3/2017 09:45
225010016 MW-29 Water 4/27/2017 11:00 5/3/2017 09:45
225010017 MW-29 Bubble Strip 4/27/2017 11:00 5/3/2017 09:45
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Fax: (412) 826-3433
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Report ID: 22501 - 922953 Page 4 of 27
PROJECT SUMMARY
Workorder:22501 FELTONSVILLE LF / SD28008
Workorder Comments
The analysis for volatile fatty acids, method AM23G, was reported at dilution for samples 22501 (0001, 0008) due to the measured
chloride concentration within the sample; matrix interfering compound.
Sample Comments
Lab ID:225010007 Sample ID:MW-10 Sample Type:N
Sample headspace vial not sufficiently pressurized for analysis. Vial pressurized with an equal volume of UHP Nitrogen and
analyzed. Results reported at a dilution.
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ANALYTICAL RESULTS
Workorder:22501 FELTONSVILLE LF / SD28008
5/3/2017 09:45
MW-2
Matrix:Water
RegLmtParameters
Lab ID:
Sample ID:
RegLmt
225010001
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
4/27/2017 10:20
EDonors - PAES
Analysis Desc: AM23G Analytical Method: AM23G
Lactic Acid <2.0 mg/l 2.0 10 5/5/2017 20:23 KB d,B0.060
Acetic Acid <1.0 mg/l 1.0 10 5/5/2017 20:23 KB d,B0.070
Propionic Acid <1.0 mg/l 1.0 10 5/5/2017 20:23 KB d,B0.090
Formic Acid <1.0 mg/l 1.0 10 5/5/2017 20:23 KB d,B0.050
Butyric Acid <1.0 mg/l 1.0 10 5/5/2017 20:23 KB d0.070
Pyruvic Acid <1.0 mg/l 1.0 10 5/5/2017 20:23 KB d0.070
i-Pentanoic Acid <1.0 mg/l 1.0 10 5/5/2017 20:23 KB d0.070
Pentanoic Acid <1.0 mg/l 1.0 10 5/5/2017 20:23 KB d0.060
i-Hexanoic Acid <2.0 mg/l 2.0 10 5/5/2017 20:23 KB d0.040
Hexanoic Acid <2.0 mg/l 2.0 10 5/5/2017 20:23 KB d0.070
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Phone: (412) 826-5245
Fax: (412) 826-3433
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ANALYTICAL RESULTS
Workorder:22501 FELTONSVILLE LF / SD28008
5/3/2017 09:45
MW-8
Matrix:Water
RegLmtParameters
Lab ID:
Sample ID:
RegLmt
225010002
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
4/28/2017 12:35
EDonors - PAES
Analysis Desc: AM23G Analytical Method: AM23G
Lactic Acid <0.20 mg/l 0.20 1 5/5/2017 23:33 KB B0.0060
Acetic Acid <0.10 mg/l 0.10 1 5/5/2017 23:33 KB B0.0070
Propionic Acid <0.10 mg/l 0.10 1 5/5/2017 23:33 KB B0.0090
Formic Acid <0.10 mg/l 0.10 1 5/5/2017 23:33 KB B0.0050
Butyric Acid <0.10 mg/l 0.10 1 5/5/2017 23:33 KB0.0070
Pyruvic Acid <0.10 mg/l 0.10 1 5/5/2017 23:33 KB0.0070
i-Pentanoic Acid <0.10 mg/l 0.10 1 5/5/2017 23:33 KB0.0070
Pentanoic Acid <0.10 mg/l 0.10 1 5/5/2017 23:33 KB0.0060
i-Hexanoic Acid <0.20 mg/l 0.20 1 5/5/2017 23:33 KB0.0040
Hexanoic Acid <0.20 mg/l 0.20 1 5/5/2017 23:33 KB0.0070
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Fax: (412) 826-3433
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Report ID: 22501 - 922953 Page 7 of 27
ANALYTICAL RESULTS
Workorder:22501 FELTONSVILLE LF / SD28008
5/3/2017 09:45
MW-8
Matrix:Bubble Strip
RegLmtParameters
Lab ID:
Sample ID:
RegLmt
225010003
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
4/28/2017 12:35
RISK - PAES
Analysis Desc: AM20GAX Analytical Method: AM20GAX
Hydrogen 13 nM 0.60 1 5/10/2017 07:49 TD n0.075
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ANALYTICAL RESULTS
Workorder:22501 FELTONSVILLE LF / SD28008
5/3/2017 09:45
MW-9
Matrix:Water
RegLmtParameters
Lab ID:
Sample ID:
RegLmt
225010004
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
4/27/2017 13:00
EDonors - PAES
Analysis Desc: AM23G Analytical Method: AM23G
Lactic Acid <0.20 mg/l 0.20 1 5/6/2017 00:36 KB B0.0060
Acetic Acid 2.7 mg/l 0.10 1 5/6/2017 00:36 KB B0.0070
Propionic Acid <0.10 mg/l 0.10 1 5/6/2017 00:36 KB B0.0090
Formic Acid <0.10 mg/l 0.10 1 5/6/2017 00:36 KB B0.0050
Butyric Acid <0.10 mg/l 0.10 1 5/6/2017 00:36 KB0.0070
Pyruvic Acid <0.10 mg/l 0.10 1 5/6/2017 00:36 KB0.0070
i-Pentanoic Acid <0.10 mg/l 0.10 1 5/6/2017 00:36 KB0.0070
Pentanoic Acid <0.10 mg/l 0.10 1 5/6/2017 00:36 KB0.0060
i-Hexanoic Acid <0.20 mg/l 0.20 1 5/6/2017 00:36 KB0.0040
Hexanoic Acid <0.20 mg/l 0.20 1 5/6/2017 00:36 KB0.0070
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Report ID: 22501 - 922953 Page 9 of 27
ANALYTICAL RESULTS
Workorder:22501 FELTONSVILLE LF / SD28008
5/3/2017 09:45
MW-9
Matrix:Bubble Strip
RegLmtParameters
Lab ID:
Sample ID:
RegLmt
225010005
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
4/27/2017 13:00
RISK - PAES
Analysis Desc: AM20GAX Analytical Method: AM20GAX
Hydrogen 2.6 nM 0.60 1 5/10/2017 08:02 TD n0.075
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ANALYTICAL RESULTS
Workorder:22501 FELTONSVILLE LF / SD28008
5/3/2017 09:45
MW-10
Matrix:Water
RegLmtParameters
Lab ID:
Sample ID:
RegLmt
225010006
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
4/27/2017 14:05
EDonors - PAES
Analysis Desc: AM23G Analytical Method: AM23G
Lactic Acid <0.20 mg/l 0.20 1 5/6/2017 01:40 KB B0.0060
Acetic Acid <0.10 mg/l 0.10 1 5/6/2017 01:40 KB B0.0070
Propionic Acid <0.10 mg/l 0.10 1 5/6/2017 01:40 KB B0.0090
Formic Acid <0.10 mg/l 0.10 1 5/6/2017 01:40 KB B0.0050
Butyric Acid <0.10 mg/l 0.10 1 5/6/2017 01:40 KB0.0070
Pyruvic Acid <0.10 mg/l 0.10 1 5/6/2017 01:40 KB0.0070
i-Pentanoic Acid <0.10 mg/l 0.10 1 5/6/2017 01:40 KB0.0070
Pentanoic Acid <0.10 mg/l 0.10 1 5/6/2017 01:40 KB0.0060
i-Hexanoic Acid <0.20 mg/l 0.20 1 5/6/2017 01:40 KB0.0040
Hexanoic Acid <0.20 mg/l 0.20 1 5/6/2017 01:40 KB0.0070
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ANALYTICAL RESULTS
Workorder:22501 FELTONSVILLE LF / SD28008
5/3/2017 09:45
MW-10
Matrix:Bubble Strip
RegLmtParameters
Lab ID:
Sample ID:
RegLmt
225010007
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
4/27/2017 14:05
RISK - PAES
Analysis Desc: AM20GAX Analytical Method: AM20GAX
Hydrogen 3.5 nM 1.2 2 5/10/2017 08:21 TD d,n0.15
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ANALYTICAL RESULTS
Workorder:22501 FELTONSVILLE LF / SD28008
5/3/2017 09:45
MW-12
Matrix:Water
RegLmtParameters
Lab ID:
Sample ID:
RegLmt
225010008
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
4/27/2017 16:15
EDonors - PAES
Analysis Desc: AM23G Analytical Method: AM23G
Lactic Acid <2.0 mg/l 2.0 10 5/6/2017 02:43 KB d,B0.060
Acetic Acid <1.0 mg/l 1.0 10 5/6/2017 02:43 KB d,B0.070
Propionic Acid <1.0 mg/l 1.0 10 5/6/2017 02:43 KB d,B0.090
Formic Acid <1.0 mg/l 1.0 10 5/6/2017 02:43 KB d,B0.050
Butyric Acid <1.0 mg/l 1.0 10 5/6/2017 02:43 KB d0.070
Pyruvic Acid <1.0 mg/l 1.0 10 5/6/2017 02:43 KB d0.070
i-Pentanoic Acid <1.0 mg/l 1.0 10 5/6/2017 02:43 KB d0.070
Pentanoic Acid <1.0 mg/l 1.0 10 5/6/2017 02:43 KB d0.060
i-Hexanoic Acid <2.0 mg/l 2.0 10 5/6/2017 02:43 KB d0.040
Hexanoic Acid <2.0 mg/l 2.0 10 5/6/2017 02:43 KB d0.070
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ANALYTICAL RESULTS
Workorder:22501 FELTONSVILLE LF / SD28008
5/3/2017 09:45
MW-12
Matrix:Bubble Strip
RegLmtParameters
Lab ID:
Sample ID:
RegLmt
225010009
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
4/27/2017 16:15
RISK - PAES
Analysis Desc: AM20GAX Analytical Method: AM20GAX
Hydrogen 3.3 nM 0.60 1 5/10/2017 08:33 TD n0.075
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ANALYTICAL RESULTS
Workorder:22501 FELTONSVILLE LF / SD28008
5/3/2017 09:45
MW-13
Matrix:Water
RegLmtParameters
Lab ID:
Sample ID:
RegLmt
225010010
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
4/28/2017 10:45
EDonors - PAES
Analysis Desc: AM23G Analytical Method: AM23G
Lactic Acid <0.20 mg/l 0.20 1 5/6/2017 03:46 KB B0.0060
Acetic Acid <0.10 mg/l 0.10 1 5/6/2017 03:46 KB B0.0070
Propionic Acid <0.10 mg/l 0.10 1 5/6/2017 03:46 KB B0.0090
Formic Acid <0.10 mg/l 0.10 1 5/6/2017 03:46 KB B0.0050
Butyric Acid <0.10 mg/l 0.10 1 5/6/2017 03:46 KB0.0070
Pyruvic Acid <0.10 mg/l 0.10 1 5/6/2017 03:46 KB0.0070
i-Pentanoic Acid <0.10 mg/l 0.10 1 5/6/2017 03:46 KB0.0070
Pentanoic Acid <0.10 mg/l 0.10 1 5/6/2017 03:46 KB0.0060
i-Hexanoic Acid <0.20 mg/l 0.20 1 5/6/2017 03:46 KB0.0040
Hexanoic Acid <0.20 mg/l 0.20 1 5/6/2017 03:46 KB0.0070
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ANALYTICAL RESULTS
Workorder:22501 FELTONSVILLE LF / SD28008
5/3/2017 09:45
MW-13
Matrix:Bubble Strip
RegLmtParameters
Lab ID:
Sample ID:
RegLmt
225010011
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
4/28/2017 10:45
RISK - PAES
Analysis Desc: AM20GAX Analytical Method: AM20GAX
Hydrogen 2.3 nM 0.60 1 5/10/2017 08:46 TD n0.075
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ANALYTICAL RESULTS
Workorder:22501 FELTONSVILLE LF / SD28008
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MW-14
Matrix:Water
RegLmtParameters
Lab ID:
Sample ID:
RegLmt
225010012
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
4/28/2017 11:20
EDonors - PAES
Analysis Desc: AM23G Analytical Method: AM23G
Lactic Acid <0.20 mg/l 0.20 1 5/6/2017 04:50 KB B0.0060
Acetic Acid <0.10 mg/l 0.10 1 5/6/2017 04:50 KB B0.0070
Propionic Acid <0.10 mg/l 0.10 1 5/6/2017 04:50 KB B0.0090
Formic Acid <0.10 mg/l 0.10 1 5/6/2017 04:50 KB B0.0050
Butyric Acid <0.10 mg/l 0.10 1 5/6/2017 04:50 KB0.0070
Pyruvic Acid <0.10 mg/l 0.10 1 5/6/2017 04:50 KB0.0070
i-Pentanoic Acid <0.10 mg/l 0.10 1 5/6/2017 04:50 KB0.0070
Pentanoic Acid <0.10 mg/l 0.10 1 5/6/2017 04:50 KB0.0060
i-Hexanoic Acid <0.20 mg/l 0.20 1 5/6/2017 04:50 KB0.0040
Hexanoic Acid <0.20 mg/l 0.20 1 5/6/2017 04:50 KB0.0070
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Report ID: 22501 - 922953 Page 17 of 27
ANALYTICAL RESULTS
Workorder:22501 FELTONSVILLE LF / SD28008
5/3/2017 09:45
MW-14
Matrix:Bubble Strip
RegLmtParameters
Lab ID:
Sample ID:
RegLmt
225010013
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
4/28/2017 11:20
RISK - PAES
Analysis Desc: AM20GAX Analytical Method: AM20GAX
Hydrogen 3.7 nM 0.60 1 5/10/2017 08:58 TD n0.075
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ANALYTICAL RESULTS
Workorder:22501 FELTONSVILLE LF / SD28008
5/3/2017 09:45
MW-19
Matrix:Water
RegLmtParameters
Lab ID:
Sample ID:
RegLmt
225010014
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
4/27/2017 13:20
EDonors - PAES
Analysis Desc: AM23G Analytical Method: AM23G
Lactic Acid <0.20 mg/l 0.20 1 5/6/2017 05:53 KB B0.0060
Acetic Acid <0.10 mg/l 0.10 1 5/6/2017 05:53 KB B0.0070
Propionic Acid <0.10 mg/l 0.10 1 5/6/2017 05:53 KB B0.0090
Formic Acid <0.10 mg/l 0.10 1 5/6/2017 05:53 KB B0.0050
Butyric Acid <0.10 mg/l 0.10 1 5/6/2017 05:53 KB0.0070
Pyruvic Acid <0.10 mg/l 0.10 1 5/6/2017 05:53 KB0.0070
i-Pentanoic Acid <0.10 mg/l 0.10 1 5/6/2017 05:53 KB0.0070
Pentanoic Acid <0.10 mg/l 0.10 1 5/6/2017 05:53 KB0.0060
i-Hexanoic Acid <0.20 mg/l 0.20 1 5/6/2017 05:53 KB0.0040
Hexanoic Acid <0.20 mg/l 0.20 1 5/6/2017 05:53 KB0.0070
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ANALYTICAL RESULTS
Workorder:22501 FELTONSVILLE LF / SD28008
5/3/2017 09:45
MW-19
Matrix:Bubble Strip
RegLmtParameters
Lab ID:
Sample ID:
RegLmt
225010015
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
4/27/2017 13:20
RISK - PAES
Analysis Desc: AM20GAX Analytical Method: AM20GAX
Hydrogen 38 nM 0.60 1 5/10/2017 09:10 TD n0.075
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ANALYTICAL RESULTS
Workorder:22501 FELTONSVILLE LF / SD28008
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MW-29
Matrix:Water
RegLmtParameters
Lab ID:
Sample ID:
RegLmt
225010016
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
4/27/2017 11:00
EDonors - PAES
Analysis Desc: AM23G Analytical Method: AM23G
Lactic Acid <0.20 mg/l 0.20 1 5/6/2017 06:56 KB B0.0060
Acetic Acid <0.10 mg/l 0.10 1 5/6/2017 06:56 KB B0.0070
Propionic Acid <0.10 mg/l 0.10 1 5/6/2017 06:56 KB B0.0090
Formic Acid <0.10 mg/l 0.10 1 5/6/2017 06:56 KB B0.0050
Butyric Acid <0.10 mg/l 0.10 1 5/6/2017 06:56 KB0.0070
Pyruvic Acid <0.10 mg/l 0.10 1 5/6/2017 06:56 KB0.0070
i-Pentanoic Acid <0.10 mg/l 0.10 1 5/6/2017 06:56 KB0.0070
Pentanoic Acid <0.10 mg/l 0.10 1 5/6/2017 06:56 KB0.0060
i-Hexanoic Acid <0.20 mg/l 0.20 1 5/6/2017 06:56 KB0.0040
Hexanoic Acid <0.20 mg/l 0.20 1 5/6/2017 06:56 KB0.0070
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Report ID: 22501 - 922953 Page 21 of 27
ANALYTICAL RESULTS
Workorder:22501 FELTONSVILLE LF / SD28008
5/3/2017 09:45
MW-29
Matrix:Bubble Strip
RegLmtParameters
Lab ID:
Sample ID:
RegLmt
225010017
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
4/27/2017 11:00
RISK - PAES
Analysis Desc: AM20GAX Analytical Method: AM20GAX
Hydrogen 2.2 nM 0.60 1 5/10/2017 09:23 TD n0.075
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ANALYTICAL RESULTS QUALIFIERS
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DEFINITIONS/QUALIFIERS
U
J
Indicates the compound was analyzed for, but not detected at or above the noted concentration.
Estimated concentration greater than the set method detection limit (MDL) and less than the set reporting limit (PQL).
MDL Method Detection Limit. Can be used synonymously with LOD; Limit Of Detection.
PQL Practical Quanitation Limit. Can be used synonymously with LOQ; Limit Of Quantitation.
ND Not detected at or above reporting limit.
DF Dilution Factor.
S Surrogate.
RPD Relative Percent Difference.
% Rec Percent Recovery.
The laboratory does not hold NELAP/TNI accreditation for this method or analyte.n
The analyte was detected in the associated blank.B
The analyte concentration was determined from a dilution.d
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QUALITY CONTROL DATA
Workorder:22501 FELTONSVILLE LF / SD28008
QC Batch:
QC Batch Method:
EDON/3328
AM23G
Analysis Method:AM23G
Associated Lab Samples:225010001, 225010002, 225010004, 225010006, 225010008, 225010010, 225010012, 225010014, 225010016
METHOD BLANK:48603
Parameter Units Result
Blank
Limit
Reporting
Qualifiers
EDonors
Lactic Acid <0.20mg/l 0.20 B
Acetic Acid <0.10mg/l 0.10 B
Propionic Acid <0.10mg/l 0.10 B
Formic Acid <0.10mg/l 0.10 B
Butyric Acid <0.10mg/l 0.10
Pyruvic Acid <0.10mg/l 0.10
i-Pentanoic Acid <0.10mg/l 0.10
Pentanoic Acid <0.10mg/l 0.10
i-Hexanoic Acid <0.20mg/l 0.20
Hexanoic Acid <0.20mg/l 0.20
LABORATORY CONTROL SAMPLE:
Parameter Units Conc.
Spike
Result
LCS
Qualifiers
LCS
% Rec
% Rec
Limits
48604
EDonors
Lactic Acid 2mg/l 2.0 B9970-130
Acetic Acid 2mg/l 2.0 B10070-130
Propionic Acid 2mg/l 2.1 B10370-130
Formic Acid 2mg/l 1.8 B8970-130
Butyric Acid 2mg/l 2.0 101 70-130
Pyruvic Acid 2mg/l 2.1 105 70-130
i-Pentanoic Acid 2mg/l 2.0 98 70-130
Pentanoic Acid 2mg/l 1.9 96 70-130
i-Hexanoic Acid 2mg/l 1.9 94 70-130
Hexanoic Acid 2mg/l 1.6 83 70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
Parameter Units Conc.
Spike
Result
MS
48605 48606
MSD
Result % Rec
MS MSD
% Rec
% Rec
Limit RPD RPD
Max
QualifiersResult
Original
225010001Original:
EDonors
Lactic Acid mg/l 20 19 96 70-130 d,B19971300.079
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QUALITY CONTROL DATA
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MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
Parameter Units Conc.
Spike
Result
MS
48605 48606
MSD
Result % Rec
MS MSD
% Rec
% Rec
Limit RPD RPD
Max
QualifiersResult
Original
225010001Original:
Acetic Acid mg/l 20 20 101 70-130 d,B211020.99 300.3
Propionic Acid mg/l 20 21 105 70-130 d,B211050300.087
Formic Acid mg/l 20 18 88 70-130 d,B18880300.14
Butyric Acid mg/l 20 21 104 70-130 d211040300.017
Pyruvic Acid mg/l 20 22 108 70-130 d221080300.014
i-Pentanoic Acid mg/l 20 21 104 70-130 d211050.96 300.008
Pentanoic Acid mg/l 20 21 106 70-130 d211060300
i-Hexanoic Acid mg/l 20 22 113 70-130 d221102.7 300
Hexanoic Acid mg/l 20 20 100 70-130 d201022300
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QUALITY CONTROL DATA
Workorder:22501 FELTONSVILLE LF / SD28008
QC Batch:
QC Batch Method:
DISG/6099
AM20GAX
Analysis Method:AM20GAX
Associated Lab Samples:225010003, 225010005, 225010007, 225010009, 225010011, 225010013, 225010015, 225010017
METHOD BLANK:48679
Parameter Units Result
Blank
Limit
Reporting
Qualifiers
RISK
Hydrogen <0.60nM 0.60 n
LABORATORY CONTROL SAMPLE & LCSD:
Parameter Units Conc.
Spike
Result
LCS
48680 48681
LCSD
Result % Rec
LCS LCSD
% Rec
% Rec
Limit RPD RPD
Max
Qualifiers
RISK
Hydrogen nM 24 22 90 80-120 n22911.1 20
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QUALITY CONTROL DATA QUALIFIERS
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QUALITY CONTROL PARAMETER QUALIFIERS
The analyte was detected in the associated blank.B
The analyte concentration was determined from a dilution.d
The laboratory does not hold NELAP/TNI accreditation for this method or analyte.n
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Workorder:22501 FELTONSVILLE LF / SD28008
Lab ID Sample ID Prep Method Analysis MethodPrep Batch Batch
Analysis
225010001 MW-2 EDON/3328AM23G
225010002 MW-8 EDON/3328AM23G
225010004 MW-9 EDON/3328AM23G
225010006 MW-10 EDON/3328AM23G
225010008 MW-12 EDON/3328AM23G
225010010 MW-13 EDON/3328AM23G
225010012 MW-14 EDON/3328AM23G
225010014 MW-19 EDON/3328AM23G
225010016 MW-29 EDON/3328AM23G
225010003 MW-8 DISG/6099AM20GAX
225010005 MW-9 DISG/6099AM20GAX
225010007 MW-10 DISG/6099AM20GAX
225010009 MW-12 DISG/6099AM20GAX
225010011 MW-13 DISG/6099AM20GAX
225010013 MW-14 DISG/6099AM20GAX
225010015 MW-19 DISG/6099AM20GAX
225010017 MW-29 DISG/6099AM20GAX
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