9230_GreenwayWasteApex_CDLF_20170804

SPRING 2017 SEMI-ANNUAL WATER QUALITY MONITORING REPORT
GREENWAY WASTE SOLUTIONS OF APEX, LLC
(FORMERLY HIGHWAY 55 C&D LANDFILL)
5940 OLD SMITHFIELD ROAD APEX, NORTH CAROLINA SOLID WASTE FACILITY PERMIT NUMBER 92-30

Prepared For: GREENWAY WASTE SOLUTIONS OF APEX, LLC
19109 W. CATAWBA AVENUE
CORNELIUS, NORTH CAROLINA 28031-5611

Prepared By:

CIVIL & ENVIRONMENTAL CONSULTANTS, INC.
1900 CENTER PARK DRIVE, SUITE A CHARLOTTE NORTH CAROLINA 28217

CEC PROJECT 111-370.003
AUGUST 3, 2017

Edward H. Stephens, L.G. Bruce D. Reilly
Project Manager Senior Project Manager

-i- Spring 2017 Water Quality Monitoring Report August 2017
TABLE OF CONTENTS

1.0 PURPOSE ...........................................................................................................................1
2.0 SITE DESCRIPTION AND BACKGROUND ................................................................2
3.0 DESCRIPTION OF FIELD SAMPLING ACTIVITIES ...............................................3
3.1 Well Water Level Gauging ..................................................................................... 3
3.2 Well Purging ........................................................................................................... 3 3.3 Groundwater Sample Collection ............................................................................. 4
4.0 GROUNDWATER FLOW EVALUATION ...................................................................5 4.1 Groundwater Potentiometric Map........................................................................... 5
4.2 Horizontal Hydraulic Gradients and Groundwater Flow Velocities ....................... 5
5.0 WATER SAMPLE ANALYTICAL PARAMETERS ....................................................7
6.0 GROUNDWATER SAMPLE ANALYTICAL DATA EVALUATION .......................8
7.0 SURFACE WATER SAMPLING DATA ......................................................................12
8.0 DEMONSTRATION LETTERS ON VINYL CHLORIDE AND METALS .............13
9.0 OTHER GROUNDWATER MONITORING ACTIVITIES ......................................14
10.0 CONCLUSIONS AND RECOMMENDATIONS .........................................................15 10.1 Conclusions ........................................................................................................... 15
10.2 Recommendations ................................................................................................. 15

FIGURES
Figure 1 – Site Location Map
Figure 2 – Site Map
Figure 3 – Groundwater Potentiometric Map
TABLES
Table 1 – Summary of Monitoring Well Gauging Data
Table 2 – Summary of Recent Site Groundwater Sample Analytical Detections
Table 3 – Historical Groundwater Data Summary
APPENDIX

Appendix A – Groundwater Sampling Field Logs
Appendix B – Laboratory Data Reports

-ii- Spring 2017 Water Quality Monitoring Report August 2017
Appendix C – Demonstration of Error in Sample Analyses
Appendix D – Detection Well MW-11 Abandonment and Replacement Records

-1- Spring 2017 Water Quality Monitoring Report August 2017

1.0 PURPOSE

On behalf of Greenway Waste Solutions of Apex, LLC (GWS), Civil & Environmental
Consultants, Inc. (CEC) has prepared this Spring 2017 Semi-Annual Water Quality Monitoring
Report for the GWS Landfill (formerly Highway 55 C&D Landfill). This report describes the well
gauging and field sampling activities, and provides a summary of the site groundwater conditions
and acquired groundwater sample data.

-2- Spring 2017 Water Quality Monitoring Report August 2017

2.0 SITE DESCRIPTION AND BACKGROUND

Greenway Waste Solutions of Apex, LLC (GWS) operates the subject landfill facility under Solid
Waste Facility Permit Number 92-30. The facility address is 5940 Old Smithfield Road, Apex,
North Carolina. A Site Location Map is attached as Figure 1. The property is bounded by the
Triangle Expressway (Interstate 540) to the north, the South Wake Landfill to the south, Highway
55 to the east, and private property to the west. A tributary creek forms the southern property
boundary, and a receptor creek forms the western property boundary. The Phase 1 and 2 disposal
areas total approximately 32.6 acres. A Site Map is attached as Figure 2.

The North Carolina Department of Environment and Natural Resources (now Department of
Environmental Quality) – Solid Waste Section (NCDEQ-SWS) issued the original solid waste
facility permit for the landfill facility on August 20, 2002. The facility will be completed in
three phases. The permitted capacity and acreages of each of the phases are listed in the table
below.

Area Gross Capacity (cy) Acreage
Phase 1 858,000 17.8
Phase 2 1,100,000 14.8
Phase 3 900,000 11.2
Totals 2,858,000 43.8

CEC last updated the facility Groundwater Detection Monitoring Plan in May 2016. The updated
plan includes the installation of new detection wells approved for the Phase 3 expansion area and
the addition of two more surface water sampling locations. Whereas, C&D waste has not yet been
disposed in the Phase 5 expansion area, CEC performed the recent monitoring activities to address
the existing Phase 1 and 2 landfill areas.

-3- Spring 2017 Water Quality Monitoring Report August 2017

3.0 DESCRIPTION OF FIELD SAMPLING ACTIVITIES

Field activities associated with the routine Spring 2017 semi-annual water quality monitoring were
conducted by CEC personnel on April 19 and 20, 2017. CEC conducted additional groundwater
sampling on June 15, 2017 to obtain quality control data. Project oversight was provided by an
NC-licensed geologist. Well water levels were gauged, static well water was purged, and
groundwater samples were collected from 11 monitoring wells including wells MW-1, MW-2,
MW-3, MW-4, MW-5, MW-6, MW-7, MW-8, MW-9, MW-10, and MW-11. The approximate
locations of these monitoring points are shown on Figure 2. Also, four surface water samples
(SW-1 through SW-4) were collected from the creek along the western property boundary (SW-1
and SW-2) and the tributary creek along the southern property boundary (SW-3 and SW-4). The
approximate surface water sampling locations are depicted on Figure 2.

3.1 WELL WATER LEVEL GAUGING

Prior to well purging/sampling, the water level in each monitoring well was gauged using an
electronic water level meter. The depth-to-groundwater as measured from a reference point on
each well top-of-casing was recorded to the nearest 0.01-inch on the well sampling field log (see
Appendix A). The water level probe was decontaminated between well measurements.

3.2 WELL PURGING

CEC field personnel employed a peristaltic pump to purge the shallow monitoring wells at a low-
flow rate until targeted analytical parameters were found to stabilize. During each well purge,
specific conductance, pH, dissolved oxygen, and oxidation-reduction potential were frequently
measured with an YSI 556 Water Quality Meter in a flow-through cell to observe and document
the chemical stability of the formation water entering the monitoring well. When parameter values
indicated stable water chemistry, as defined by USEPA Groundwater Sampling Guidelines for
Superfund and RCRA Project Managers (EPA 542-S-02-001, May 2002), the well purge was
considered complete and groundwater samples were then collected. Well purge data was recorded
on the well sampling field logs provided in Appendix A.

-4- Spring 2017 Water Quality Monitoring Report August 2017

3.3 GROUNDWATER SAMPLE COLLECTION

Following the above-described well purging procedures, CEC field personnel collected
groundwater samples from each well employing a peristaltic pump and the same low-flow
pumping protocols used during the well purge. Groundwater samples were collected in laboratory-
supplied sample containers that were labeled and then packed on ice in insulated coolers. The
samples were either hand-delivered by CEC personnel or shipped overnight by FedEx to the
selected analytical laboratory under chain-of-custody protocol.

-5- Spring 2017 Water Quality Monitoring Report August 2017

4.0 GROUNDWATER FLOW EVALUATION

A depth-to-water level measurement was performed relative to the well top-of-casing in each
groundwater monitoring well prior to well purging. A water level elevation was calculated by
subtracting the depth-to-water from the respective surveyed top-of-casing elevation datum.
Monitoring well gauging data are summarized in Table 1.

4.1 GROUNDWATER POTENTIOMETRIC MAP

Calculated static groundwater levels were used to prepare the Spring 2017 groundwater
potentiometric map presented in Figure 3. Shallow groundwater movement beneath the landfill is
semi-radial to the northwest and west toward a tributary creek located to the northwest and the
receptor creek forming the west property boundary, respectively; and to the southwest toward the
tributary creek forming the southern property boundary.

4.2 HORIZONTAL HYDRAULIC GRADIENTS AND GROUNDWATER FLOW
VELOCITIES
The horizontal hydraulic gradient (i) used in the flow velocity calculation below was estimated
between the upgradient well MW-1 and downgradient well MW-5, which are separated by a
distance of approximately 2,700 feet. Based on the calculated groundwater elevations for the April
2017 event, the hydraulic head difference between MW-1 (346.10 ft) and MW-5 (278.23 ft) is
67.87 feet. The head difference (67.87 ft) divided by the well separation distance (2,700 ft) is
0.025, the horizontal hydraulic gradient, unitless.

Slug tests to estimate the horizontal hydraulic conductivity (K) in the vicinity of monitoring well
MW-6 were conducted by Elite Techniques, Inc. in August 2013. The mean K calculated from
the slug test data is 4.54 x 10-5 cm/sec (= 0.13 ft/day). Based on the known typical absence of
significant fracturing within the massive conglomerate beneath the landfill footprint, the mean K
of 10-5 cm/sec would appear to be a higher rate than the norm. Typical values for unfractured rock
from the scientific literature suggest K values of 10-2 ft/year.

-6- Spring 2017 Water Quality Monitoring Report August 2017

An effective porosity (ηe) of 10 percent was estimated based on the fractured conglomerate
comprising the surficial aquifer at the site. Groundwater flow velocity calculations are included
in Table 2.

A groundwater flow velocity was estimated based on the April 2017 groundwater monitoring data.
The flow velocity estimate was calculated by using the following equation:
V = K x i
ηe
Where:
V = groundwater flow velocity (ft/sec)
K = horizontal hydraulic conductivity (ft/sec)
i = horizontal hydraulic gradient (dh/dl, unitless)
dh = difference in hydraulic head between wells (ft)
dl = distance between wells (ft)
ηe = effective porosity (%)

TABLE 1 - AVERAGE GROUNDWATER FLOW VELOCITY ESTIMATE
K (ft/day) i (ft) MW-1A to MW-5 ηe V (ft/day) V (ft/year)

0.13 0.025 0.10 0.033 11.86

Table Notes: V = (K x i)/ ηe Where: V = groundwater flow velocity (ft/sec)
K = horizontal hydraulic conductivity (ft/sec)
i = horizontal hydraulic gradient (dh/dl, unitless)
dh = difference in hydraulic head between wells (ft)
dl = distance between wells (ft) ηe = effective porosity (%)

The groundwater flow velocity calculated for the May 2017 sampling event is approximately 12
feet/year. Flow values in less fractured rock would be on the order of 0.01 to 1.0 ft/year.

-7- Spring 2017 Water Quality Monitoring Report August 2017

5.0 WATER SAMPLE ANALYTICAL PARAMETERS

CEC submitted the routine semi-annual groundwater and surface water samples to TestAmerica
Laboratories, Inc. (TA) for analytical testing. All 11 monitoring well samples and four surface
water samples were analyzed for the following parameters:

Appendix I Volatile Organic Compounds (VOCs) [EPA 8260B] Appendix I Metals [EPA 200.8]
Mercury [EPA 245.1]
Monitoring well samples were also tested for leachate indicator parameters including the following
list:

Alkalinity [SM 2320B] Sulfate EPA 9056A Chloride [9056A] Total Dissolved Solids (TDS) [2540C]
For quality control purposes, CEC also submitted a blind duplicate sample (collected from MW-
8) to TA for analysis of Appendix I VOCs plus THF. In addition, CEC collected a split sample
from MW-8 that was submitted to Pace Analytical Services, Inc. (Pace) laboratory for analysis of
Appendix I VOCs plus THF.

Due to conflicting laboratory analytical results from the initial round of sample analyses, CEC
personnel re-sampled MW-8 on June 15, 2017 and submitted this sample to TA for analysis of
Appendix I VOCs.

-8- Spring 2017 Water Quality Monitoring Report August 2017

6.0 GROUNDWATER SAMPLE ANALYTICAL DATA EVALUATION

The laboratory analytical data reports are provided in Appendix B. Summaries of Appendix I
VOCs, Appendix I metals, and inorganic analytes detected in the collected groundwater samples
at concentrations above their respective laboratory-reported detection limits are provided in Table
3.

Historical Site Data
Data discussed in this section draw inferences to historical well sampling data acquired at the
landfill since 2012. Enviro-Pro, PC conducted the field monitoring activities, sample collection,
and reporting for the routine semi-annual groundwater monitoring events from at least 2009 to
2016. Shealy performed the sample analyses for the semi-annual monitoring events since at least
2012, except for the most recent Spring 2017 monitoring event for which the analyses were
performed by TA. The monitoring reports are submitted to the NCDEQ-SWS – Compliance Unit.

Organic Analytes Detected at Concentrations Exceeding the 2L Standards
For the Spring 2017 monitoring event, TA detected vinyl chloride in MW-8 at a concentration of
4.2 µg/L, which exceeds the 2L Standard of 0.03 µg/L. TA also detected 2.5 µg/L vinyl chloride
in the blind duplicate sample that CEC collected from MW-8. However, for the split sample from
MW-8 that CEC submitted to Pace for VOC analysis, Pace did not detect vinyl chloride above the
laboratory reporting limit of <1.0 µg/L.

For MW-8, unexpected vinyl chloride detections were reported by TA compared to the Pace
results. CEC asked TA to review the results, analysis methodology, instruments used, and
interviewed the analysts in an effort to either validate or discount this first round of 2017 results.
TA brought in their Senior Technical Services Group to review their process. In late May, TA
informed CEC of the following results of their investigation:

1. Search indicated a possibility of conversion of a Freon refrigerant (Freon 151) to vinyl
chloride in the gas chromatograph (GC);

-9- Spring 2017 Water Quality Monitoring Report August 2017

2. Confirmation of this occurred after TA obtained and ran a Freon 151 standard through their
Chicago GCs, resulting in only one of the GCs not converting the Freon 151 to vinyl
chloride;
3. A TA company-wide program was implemented and identified most of their GCs
converting the Freon 151 to vinyl chloride; and
4. TA started, and is continuing, a corrective-action program to identify and change the
component(s) of the GCs converting the Freon. (It is reported that the likely cause is the
Purge and Trap mechanism.)

On June 15, 2017, CEC re-sampled MW-8 and submitted the sample to TA for VOCs analysis.
TA did not detect vinyl chloride in the second sample above the laboratory reporting limit of <0.5
µg/L. The confirmatory sample was analyzed by TA using a GC instrument that they previous
tested and cleared to provide artifact-free vinyl chloride data.

Following the June 2017 confirmation-resampling event, CEC received a letter from Shealy regarding
in-house testing of their GC instruments documenting the results of their independent testing, which
confirmed TA’s findings. Shealy also provided a letter from the supplier of the silica gel component
in the GC purge and trap mechanisms (OI Analytical) that indicated the silica gel component may be
the “active” Freon 151 to vinyl chloride conversion location. The documentation from TA, Shealy,
and OI Analytical can be found in Appendix C.

The confirmed conversion of Freon 151 to vinyl chloride explains the false detection of vinyl
chloride in sample MW-8 at the Highway 55 Landfill. Confirmation of these findings from the
Spring 2017 sampling will continue to take place for the near future as part of the approved
groundwater monitoring plan. CEC will continue to obtain and analyze split samples and blind
duplicates from selected groundwater monitoring wells. TA and Pace are continuing to conduct
reviews of their GCs to eliminate the issue(s) converting the Freon to vinyl chloride.

The presented data and supporting correspondence from the analytical laboratories directly
working on the project clearly show that the vinyl chloride analytical data prior to the Spring 2017
sampling event have to be considered invalid. Any remedial efforts to address vinyl chloride

-10- Spring 2017 Water Quality Monitoring Report August 2017

impacts above the 2L Standards will be based on sample data from the Spring 2017 event and
future sampling events.

Metal Analytes Detected at Concentrations Exceeding the 2L Standards
As highlighted in Table 2, the laboratory test results for the monitoring event show that cobalt and
vanadium exceed the NC Interim Maximum Allowable Concentrations (IMACs) in the majority
of the landfill monitoring well samples. Cobalt was detected above its IMAC of 1 µg/L in MW-
3, MW-4, MW-5, MW-6, MW-7, MW-8, MW-11, SW-3, and SW-4. Vanadium was detected
above its IMAC of 0.3 µg/L in MW-1, MW-2, MW-6, MW-8, MW-9, and SW-3. The uniformity
of these detected cobalt and vanadium concentrations in the respective well samples suggests that
they are representative of naturally occurring levels.

Barium was detected at a concentration of 1,200 µg/L in upgradient well MW-1 and was detected
at 1,400 µg/L in MW-10. These barium levels exceed the 2L Standard of 700 µg/L. MW-1 is an
upgradient monitoring well, which suggests that the detected barium concentration in this well is
likely related to an unknown upgradient source.

Lead was detected at 21 µg/L in MW-6, which is above its 2L Standard of 15 µg/L. Elevated lead
has not been typically reported in any well samples; thus, this lead detection should be confirmed
by additional data collection.

Inorganic Leachate Indicator Parameters
The detections of inorganic parameters are summarized in Table 3. Detected total dissolved solids
(TDS) levels in wells MW-1, MW-2, MW-3, MW-4, MW-10, and MW-11 exceeded its 2L
Standard of 500 mg/L. Detected chloride concentrations in wells MW-1, MW-3, MW-9, and MW-
10 exceeded its 2L Standard of 250 mg/L. The detected sulfate concentration of 260 mg/L in MW-
11 was above the NC 2L Standard of 250 mg/L. The detected mercury concentration of 1.2 mg/L
in upgradient well MW-1 exceeded its 2L Standard of 1 mg/L.

-11- Spring 2017 Water Quality Monitoring Report August 2017

It is important to note that elevated chloride and TDS levels were observed in the upgradient on-
site monitoring well MW-1, as well as downgradient on-site wells. Chloride and TDS levels were
highest in MW-1 and MW-10.

-12- Spring 2017 Water Quality Monitoring Report August 2017

7.0 SURFACE WATER SAMPLING DATA

CEC personnel collected a total of four surface water samples (SW-1 through SW-4), which were
taken from the creek along the western property boundary (SW-1 and SW-2) and the tributary
creek along the southern property boundary (SW-3 and SW-4). The approximate surface water
sampling locations are depicted on Figure 2. Surface water samples were analyzed for the
constituents listed in Appendix I of 40 CFR Part 258. The stream sample analytical results are
summarized in Tables 2 and 3.

No Appendix I VOCs were detected above the laboratory reporting limits in the surface water
samples. Several Appendix I metals including arsenic, barium, cobalt, copper, iron, lead,
manganese, vanadium, and zinc were detected in at least one surface water sample. With the
exception of copper, detected metals concentrations in the upstream background sample (SW-1
and SW-3) were higher than the downstream (SW-2 and SW-4) metals concentrations indicating
that the metals and their concentrations detected in the surface water samples are naturally
occurring. The maximum detected copper level of 16 µg/L in sample SW-4 is well below the NC
surface water protection standards.

-13- Spring 2017 Water Quality Monitoring Report August 2017

8.0 DEMONSTRATION LETTERS ON VINYL CHLORIDE AND METALS

Per 15A NCAC 13B .0544 (b) (1) (I), on behalf of Greenway Waste Solutions of Apex, LLC (GWS),
CEC prepared and submitted letters under separate cover to the NCDEQ-SWS – Compliance Unit
presenting historical data and recent technical findings regarding the laboratory detections of vinyl
chloride and on the presence of background metals in the groundwater underlying the landfill. Copies
of these letters and supporting documentation are included in Appendix C. Both letters present and
discuss data on laboratory error in falsely reporting vinyl chloride due to the Freon conversion and on
the presence of naturally occurring metals in geology and hydrogeology at the landfill.

-14- Spring 2017 Water Quality Monitoring Report August 2017

9.0 OTHER GROUNDWATER MONITORING ACTIVITIES

On behalf of GWS, CEC submitted a request dated May 2, 2107 to the NCDEQ-SWS for the
abandonment and subsequent re-location of detection monitoring well MW-11 in order to expand
on-site road access to the compost storage area and general facility improvements to the landfill.
The NCDEQ-SWS approved this request via email dated May 9, 2017 (see Appendix D). MW-
11 was abandoned-in-place on May 16, 2017 by an NC-certified well driller, Troxler Geologic
Services, Inc. A Well Abandonment Record is included in Appendix D.

According to the NCDEQ-SWS-approved well re-location plan, a replacement well MW-11R will
be installed at the proposed location prior to the Fall 2017 groundwater monitoring event. The
new well will replace the abandoned well in the detection groundwater monitoring network. In
addition, CEC will update the current Groundwater Detection Monitoring Plan (May 2016) to
reflect changes due to the new well locations and any monitoring tables, etc.

-15- Spring 2017 Water Quality Monitoring Report August 2017

10.0 CONCLUSIONS AND RECOMMENDATIONS

10.1 CONCLUSIONS

Routine field activities associated with the Spring 2017 semi-annual water quality monitoring
event were conducted by CEC personnel on April 19 and 20, 2017. Well water levels were gauged,
static well water was purged, and groundwater samples were collected from 11 monitoring wells.
Surface water samples were collected from four creek locations.

Due to a laboratory issue involving the conversion of Freon 151 to VC, CEC re-sampled MW-8
on June 15, 2017 and submitted the confirmatory sample to TestAmerica for VOC analysis. Vinyl
chloride was not detected in the MW-8 re-sample at a concentration above the laboratory reporting
limit of <0.5 µg/L.

Analytical testing detected several leachate indicator parameters including chloride, sulfate, and
TDS at concentrations above the 2L Standards. Chloride and TDS were detected at the most
elevated levels in upgradient well MW-1. An upgradient source for elevated chloride and TDS
has not been identified and is being further investigated.

10.2 RECOMMENDATIONS

It is CEC’s technical opinion based on the quality assurance sampling and analytical data obtained
during the Spring 2017 monitoring event that recent historical vinyl chloride detections in MW-8
are the result of laboratory artifacts. Laboratory instrumentation reviews have determined that
when present Freon 151 will degrade to vinyl chlorine in GC instruments operating with certain
purge and trap columns with a silica gel component. The well re-sample analysis in June 2017 is
the only reported vinyl chloride data that should be representative of site groundwater quality.
Confirmation of these second-round results from the Spring 2017 sampling will continue to take
place for the near future as part of the approved groundwater monitoring plan. CEC will continue
to obtain and analyze split samples and blind duplicates from selected groundwater monitoring

-16- Spring 2017 Water Quality Monitoring Report August 2017

wells. TestAmerica and Pace are continuing to conduct reviews of their GCs to eliminate the
issue(s) converting the Freon to vinyl chloride.

Potential upgradient sources for elevated chloride and TDS detected in upgradient well MW-1 will
be further investigated to evaluate the impact to the site groundwater. To minimize sampling
artifacts and validate certain metals, chloride and TDS data, CEC will carefully monitor turbidity
in the site monitoring wells during the well purge process. CEC will collect samples after
achieving turbidity levels of 20 Nephelometric Turbidity Units (NTUs) or less, if practical.

As a replacement for the recently abandoned MW-11, new detection monitoring well MW-11R
will be installed at a NCDEQ-SWS-approved location prior to the Fall 2017 groundwater
monitoring event. The new well will replace the abandoned well in the detection groundwater
monitoring network. In addition, CEC will update the current Groundwater Detection Monitoring
Plan (May 2016) to reflect changes due to the new well locations and any monitoring tables, etc.

FIGURES

REFERENCE
DATE:DWG SCALE:
DRAWN BY:CHECKED BY:APPROVED BY:
PROJECT NO:
FIGURE NO.:
SITE LOCATION MAP
111-370.0031"=1000'AUGUST 2017
PNP EHS EHS 1
HIGHWAY 55 C&D LANDFILL
GREENWAY WASTE SOLUTIONS OF
APEX, LLC
www.cecinc.com
1900 Center Park Drive - Suite A - Charlotte, NC 28217
Ph: 980.237.0373 · Fax: [phone]
NORTH
DATE:DWG SCALE:
DRAWN BY:CHECKED BY:APPROVED BY:
PROJECT NO:
FIGURE NO.:
SITE MAP
111-370.0031"=250'AUGUST 2017
PNP EHS EHS 2
HIGHWAY 55 C&D LANDFILL
GREENWAY WASTE SOLUTIONS
OF APEX, LLC
REFERENCE www.cecinc.com
1900 Center Park Drive - Suite A - Charlotte, NC 28217
Ph: 980.237.0373 · Fax: [phone]
NORTH
LEGEND
DATE:DWG SCALE:
DRAWN BY:CHECKED BY:APPROVED BY:
PROJECT NO:
FIGURE NO.:
POTENTIOMETRIC CONTOUR MAP
111-370.0031"=250'AUGUST 2017
JKS EHS EHS 3
HIGHWAY 55 C&D LANDFILL
GREENWAY WASTE SOLUTIONS
OF APEX, LLC
www.cecinc.com
1900 Center Park Drive - Suite A - Charlotte, NC 28217
Ph: 980.237.0373 · Fax: [phone]
NORTH
REFERENCE
LEGEND

TABLES

Table 1
Summary of Monitoring Well Gauging Data
Highway 55 C&D Landfill
Apex, North Carolina
CEC Project No. 111-370.003
August 2017
MW ID Well
Depth GRD Elev.Depth to
TOS
Depth to
BOS TOS Elev.BOS Elev.TOC Elev.Depth to
Water (TOC)WL Elev.
Depth to
Water
(TOC)
WL Elev.
MW-1 32 362.06 17 32 345.06 330.06 364.51 17.41 347.1 18.41 346.10
MW-2 20 292.41 5 10 287.41 282.41 294.84 11.43 283.41 8.29 286.55
MW-3 19 285.93 4 19 281.93 266.93 288.57 7.94 280.63 6.45 282.12
MW-4 19 283.49 4 19 279.49 264.49 286.25 8.21 278.04 5.74 280.51
MW-5 19 281.88 4 19 277.88 262.88 284.76 9.18 275.58 6.53 278.23
MW-6 19 284.38 4 19 280.38 265.38 287.07 9.42 277.65 8.06 279.01
MW-7 22 294.75 7 22 287.75 272.75 297.58 11.89 285.69 8.49 289.09
MW-8 30 312.79 15 30 297.79 282.79 315.24 21.35 293.89 18.18 297.06
MW-9 20 311.93 5 20 306.93 291.93 314.89 9.87 305.02 7.83 307.06
MW-10 30 302.01 15 30 287.01 272.01 304.49 21.84 282.65 15.17 289.32
MW-11 20 354.53 5 20 349.53 334.53 356.91 28.50 328.41 28.17 328.74
Units are in feet.GRD Elev. = Surveyed ground elevation. TOC = Surveyed well top-of-casing elevation.
TOS = Top-of-screen.BOS = Botton-of-screen.WL Elev. = Water level elevation.
10/31/2016 4/19/2017
Table 2. Summary of April 2017 Sampling Event
Highway 55 Landfill
CEC Project No. 111-370.003
Well I.D.MW-1 MW-2 MW-3 MW-4 MW-5
Sampling Date 4/19/17 4/20/17 4/20/17 4/19/17 4/19/17
Organics (µg/L)2L Std.
Benzene 1 <0.5 <0.5 <0.5 <0.5 <0.5
Vinyl Chloride 0.03 <0.5 <0.5 <0.5 <0.5 <0.5
1,1-Dichloroethane 6 <1 <1 <1 <1 <1
Tetrahydrofuran NS <10 <10 <10 6.5 <10
Metals (µg/L)
Antimony 1 1.5 B 0.89 BJ <3 <3 <3
Arsenic 10 0.90 J 1.2 1.6 4.4 0.30 J
Barium 700 1200 74 230 130 82
Beryllium 4 <1.0 <1.0 <1.0 <1.0 <1.0
Cadmium 2 <0.50 <0.50 <0.50 <0.50 <0.50
Calcium NS 22,000 69,000 NA NA NA
Chromium 10 <5.0 <5.0 <5.0 6.6 <5.0
Cobalt 1 0.28 J 0.59 J 21 10 10
Copper 1,000 1.1 J 0.79 J 0.81 J <2.0 <2.0
Iron 300 NA NA 4100 <100 540
Lead 15 <0.50 0.51 0.55 0.17 J <0.50
Manganese 50 1,200 590 11,000 16 37
Nickel 100 <2.0 2.8 2.1 8 1.3 J
Vanadium 0.3 4.9 J 2.5 J <5.0 <5.0 <5.0
Zinc 1,000 <20 <20 <20 <20 <20
Indicator Parameters (mg/L)
Alkalinity NS 410 160 470 690 99
Ammonia- N 1.5 0.56 0.052 J NA NA NA
Carbon Dioxide NS 230 380 NA NA NA
Chloride 250 2700 130 530 100 16
Cyanide 70 0.0071 J <0.01 <0.01 <0.01 <0.01
Sulfate 250 3.8 87 140 75 34
Sulfide NS 2 <1 NA NA NA
TDS 500 5600 530 1600 1100 200
Bold values exceed the NCDEQ Standards
2L Std. = 15A NCAC 02L .0202 Groundwater
Standards or Interim Maximum Allowable
Concentrations (IMACs) (Eff. April 1, 2013)
Bold and highlighted values exceed the
NCDEQ Standards yet the analyte
concentrations are within the range of
naturally-occurring levels.
Table 2. Summary of April 2017 Sampling Event
Highway 55 Landfill
CEC Project No. 111-370.003
Well I.D.
Sampling Date
Organics (µg/L)2L Std.
Benzene 1
Vinyl Chloride 0.03
1,1-Dichloroethane 6
Tetrahydrofuran NS
Metals (µg/L)
Antimony 1
Arsenic 10
Barium 700
Beryllium 4
Cadmium 2
Calcium NS
Chromium 10
Cobalt 1
Copper 1,000
Iron 300
Lead 15
Manganese 50
Nickel 100
Vanadium 0.3
Zinc 1,000
Indicator Parameters (mg/L)
Alkalinity NS
Ammonia- N 1.5
Carbon Dioxide NS
Chloride 250
Cyanide 70
Sulfate 250
Sulfide NS
TDS 500
Bold values exceed the NCDEQ Standards
2L Std. = 15A NCAC 02L .0202 Groundwater
Standards or Interim Maximum Allowable
Concentrations (IMACs) (Eff. April 1, 2013)
Bold and highlighted values exceed the
NCDEQ Standards yet the analyte
concentrations are within the range of
naturally-occurring levels.
MW-6 MW-7 MW-8 MW-9 MW-10 MW-11
4/19/17 4/19/17 4/20/17 4/19/17 4/19/17 4/19/17
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5
<0.5 <0.5 4.2 <0.5 <0.5 <0.5
<1 <1 <1 <1 <1 <1
<10 <10 <10 <10 <10 <10
<3 <3 <3 <3 <3 <3
9.7 3.6 1.8 2.3 1.5 1.4
270 61 70 360 1400 420
0.58 J <1.0 <1 <1 <1 0.78 J
0.36 J <0.50 <0.50 <0.50 <0.50 0.72
NA NA NA NA NA NA
3.8 J <5.0 <5.0 <5.0 <5.0 <5
4.2 1.3 1.8 0.77 J <1.0 11
8.9 1.0 J 1.3 J 0.72 J 0.90 J 0.72 J
47,000 300 300 300 300 300
21 0.41 J 0.54 0.23 J <0.50 1.9
10,000 220 220 220 220 220
4.7 1.2 J 3.2 2 <2.0 2.6
14 <5.0 2.0 J 2.0 J <5.0 <5.0
38 B <20 <20 <20 <20 12 J
11 170 250 250 560 74
NA NA NA NA NA NA
NA NA NA NA NA NA
36 42 93 500 2300 170
<0.10 <0.01 <0.01 <0.01 <0.01 <0.01
17 74 26 43 23 26
NA NA NA NA NA NA
130 390 470 210 4900 690
Table 2. Summary of April 2017 Sampling Event
Highway 55 Landfill
CEC Project No. 111-370.003
Well I.D.
Sampling Date
Organics (µg/L)2L Std.
Benzene 1
Vinyl Chloride 0.03
1,1-Dichloroethane 6
Tetrahydrofuran NS
Metals (µg/L)
Antimony 1
Arsenic 10
Barium 700
Beryllium 4
Cadmium 2
Calcium NS
Chromium 10
Cobalt 1
Copper 1,000
Iron 300
Lead 15
Manganese 50
Nickel 100
Vanadium 0.3
Zinc 1,000
Indicator Parameters (mg/L)
Alkalinity NS
Ammonia- N 1.5
Carbon Dioxide NS
Chloride 250
Cyanide 70
Sulfate 250
Sulfide NS
TDS 500
Bold values exceed the NCDEQ Standards
2L Std. = 15A NCAC 02L .0202 Groundwater
Standards or Interim Maximum Allowable
Concentrations (IMACs) (Eff. April 1, 2013)
Bold and highlighted values exceed the
NCDEQ Standards yet the analyte
concentrations are within the range of
naturally-occurring levels.
SW-1 SW-2 SW-3 SW-4
4/20/17 4/20/17 4/20/17 4/20/17
<0.5 <0.5 <0.5 <0.5
<0.5 <0.5 <0.5 <0.5
<1 <1 <1 <1
<10 <10 <10 <10
<1 <1 <1 <1
0.61 J 0.51 J 1.6 1.8
48 47 240 73
<1 <1 <1 <1
<0.50 <0.50 <0.50 <0.50
NA NA NA NA
<5 <5 <5 <5
0.58 J 0.43 J 4.4 1.1
0.95 J 1.2 J 5.8 16
3000 3000 3000 3000
0.38 J 0.26 J 1.2 0.21 J
230 230 230 230
<2.0 <2.0 1.9 J <2.0
<5.0 <5.0 2.7 J <5.0
<20 <20 140 <20
27 36 97 120
NA NA NA NA
NA NA NA NA
28 19 56 44
NA NA NA NA
4 5.8 51 20
NA NA NA NA
84 90 90 280
Table 3. Summary of Recent Site Groundwater Monitoring Data
Highway 55 Landfill
CEC Project No. 111-370.003
Well I.D.
Sampling Date 11/4/13 4/2/14 10/20/14 4/23/15 10/12/15 4/25/16 10/31/16 4/19/17
Organics (µg/L)2L Std.
Benzene 1 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
Bis(2-ethylhexyl)phthalate 3 1.9 J 1.9 J 1.9 J 1.9 J 2.5 J 1.9 J 1.9 J 1.9 J
Carbon Disulfide 700 <1 <1 <1 <1 <1 <1 <1 <1
cis-1,2-Dichloroethene 70 <1 <1 <1 <1 6.8 <1 <1 <1
2,4-Dimethylphenol 100 <1 <1 <1 <1 <1 <1 <1 <1
Diethylphthalate 6,000 <5 <5 <5 <5 <5 <5 <5 <5
2,4 -D 70 <2 <2 <2 <2 0.69 J <2 <2 <2
4-4'-DDT 0.1 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
Dieldrin 0 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
Dinoseb 7 <1 <1 <1 <1 <1 <1 <1 <1
Endosulfan II 40 <0.04 <0.04 <0.04 <0.04 0.04 <0.04 <0.04 <0.04
Endosulfan sulfate 40 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
Endrin 2 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
Endrin aldehyde 2 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
Methylene Chloride 5 <1 <1 <1 <1 0.79 J <1 <1 <1
Trichloroethene 3 <1 <1 <1 <1 0.92 J <1 <1 <1
Vinyl Chloride 0.03 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
Toluene 600 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
Xylenes 500 <<<<<1 <<<
beta-BHC NS <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
1,1-Dichloroethane 6 <1 <1 <1 <1 <1 <1 <1 <1
1,2-Dichloroethane 0.4 <1 <1 <1 <1 <1 <1 <1 <1
1,1-Dichloroethene 350 <1 <1 <1 <1 <1 <1 <1 <1
Tetrachloroethene 0.7 <1 <1 <1 <1 <1 <1 <1 <1
Tetrahydrofuran NS <10 <10 <10 <10 <10 <10 <10 <10
Naphthalene 6 <10 <10 <10 <10 <1 <10 <10 <10
Acetophenone 700 <1 <1 <1 <1 0.35 J <1 <1 <1
Metals (µg/L)
Antimony 1 1.5 B 1.5 B 1.5 B 1.5 B 0.51 BJ 1.5 B 1.5 B 1.5 B
Arsenic 10 <1.0 <1.0 <1.0 <1.0 3.5 J 7.3 <1.0 0.90 J
Barium 700 890 850 760 860 850 940 0.87 1200
Beryllium 4 <1.0 <1.0 <1.0 <1.0 <1.0 0.34 J <1.0 <1.0
Cadmium 2 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50
Calcium NS 22,000 22,000 22,000 22,000 110,000 22,000 22,000 22,000
Chromium 10 <5.0 <5.0 <5.0 <5.0 1.3 J <5.0 <5.0 <5.0
Cobalt 1 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 0.28 J
Copper 1,000 <2.0 <2.0 <2.0 <2.0 2.7 J <2.0 <2.0 1.1 J
Iron 300 NA NA NA NA NA NA NA NA
Lead 15 <0.50 <0.50 <0.50 <0.50 0.46 J <0.50 <0.50 <0.50
Manganese 50 1,200 1,200 1,200 1,200 13,000 1,200 1,200 1,200
Nickel 100 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0
Vanadium 0.3 <5.0 <5.0 <5.0 <5.0 5.1 J 5.9 J <5.0 4.9 J
Zinc 1,000 20 <20 <20 <20 27 9.7 BJ <20 <20
Indicator Parameters (mg/L)
Alkalinity NS NA NA NA NA NA NA NA 410
Ammonia- N 1.5 NA NA NA NA NA NA NA 0.56
Carbon Dioxide NS NA NA NA NA NA NA NA 230
Chloride 250 NA NA NA NA NA NA NA 2700
Cyanide 70 NA NA NA NA NA NA NA 0.0071 J
Sulfate 250 NA NA NA NA NA NA NA 3.8
Sulfide NS NA NA NA NA NA NA NA 2
TDS 500 NA NA NA NA NA NA NA 5600
Bold values exceed the NCDEQ Standards
Bold and highlighted values
exceed the NCDEQ Standards
yet the analyte concentrations
are within the range of naturally-
occurring levels.
2L Std. = 15A NCAC 02L .0202 Groundwater
Standards or Interim Maximum Allowable
Concentrations (IMACs) (Eff. April 1, 2013)
MW-1
Table 3. Summary of Recent Site Groundwater Monitoring Data (cont.)
Highway 55 Landfill
CEC Project No. 111-370.003
Well I.D.
Sampling Date
Organics (µg/L)2L Std.
Benzene 1
Bis(2-ethylhexyl)phthalate 3
Carbon Disulfide 700
cis-1,2-Dichloroethene 70
2,4-Dimethylphenol 100
Diethylphthalate 6,000
2,4 -D 70
4-4'-DDT 0.1
Dieldrin 0
Dinoseb 7
Endosulfan II 40
Endosulfan sulfate 40
Endrin 2
Endrin aldehyde 2
Methylene Chloride 5
Trichloroethene 3
Vinyl Chloride 0.03
Toluene 600
Xylenes 500
beta-BHC NS
1,1-Dichloroethane 6
1,2-Dichloroethane 0.4
1,1-Dichloroethene 350
Tetrachloroethene 0.7
Tetrahydrofuran NS
Naphthalene 6
Acetophenone 700
Metals (µg/L)
Antimony 1
Arsenic 10
Barium 700
Beryllium 4
Cadmium 2
Calcium NS
Chromium 10
Cobalt 1
Copper 1,000
Iron 300
Lead 15
Manganese 50
Nickel 100
Vanadium 0.3
Zinc 1,000
Indicator Parameters (mg/L)
Alkalinity NS
Ammonia- N 1.5
Carbon Dioxide NS
Chloride 250
Cyanide 70
Sulfate 250
Sulfide NS
TDS 500
Bold values exceed the NCDEQ Standards
Bold and highlighted values
exceed the NCDEQ Standards
yet the analyte concentrations
are within the range of naturally-
occurring levels.
2L Std. = 15A NCAC 02L .0202 Groundwater
Standards or Interim Maximum Allowable
Concentrations (IMACs) (Eff. April 1, 2013)
11/4/13 4/2/14 10/20/14 4/23/15 10/12/15 4/25/16 10/31/16 4/20/17
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
1.9 J 1.9 J 1.9 J 1.9 J 2.5 J 1.9 J <5 0.98 J
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 6.8 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<5 <5 <5 <5 <5 <5 0.36 J <5
<2 <2 <2 <2 0.69 J <2 <2 <2
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<1 <1 <1 <1 <1 <1 <1 <1
<0.04 <0.04 <0.04 <0.04 0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<1 <1 <1 <1 0.79 J <1 <1 <1
<1 <1 <1 <1 0.92 J <1 <1 <1
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.63 J <0.5
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
<<<<<1 <1.6 <1
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<10 <10 <10 <10 <10 <10 <10 <10
<10 <10 <10 <10 <1 <10 <1 <10
<1 <1 <1 <1 0.35 J <1 <1 0.49 J
1.5 B 1.5 B 1.5 B 1.5 B 0.51 BJ 1.5 B 0.72 BJ 0.89 BJ
<1.0 <1.0 <1.0 <1.0 4.6 J 3.5 J 3.6 1.2
250 130 120 30 330 37 160 74
<1.0 <1.0 <1.0 <1.0 <1.0 0.24 J <1.0 <1.0
<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50
22,000 22,000 22,000 22,000 110,000 22,000 50,000 69,000
6.2 <5.0 <5.0 <5.0 4.4 J <5.0 <5.0 <5.0
<1.0 <1.0 <1.0 <1.0 3.0 J <1.0 1.9 0.59 J
12 <2.0 <2.0 <2.0 4.5 J 8.4 J 2.9 0.79 J
NA NA NA NA NA NA NA NA
11 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 0.51
1,200 1,200 1,200 1,200 13,000 1,200 240 590
<2.0 <2.0 <2.0 <2.0 8.1 J <2.0 5.6 2.8
<5.0 <5.0 <5.0 <5.0 5.1 J <5.0 <5.0 2.5 J
43 <20 <20 <20 11 J 87 B 32 <20
NA NA NA NA NA NA NA 160
NA NA NA NA NA NA NA 0.052 J
NA NA NA NA NA NA NA 380
NA NA NA NA NA NA NA 130
NA NA NA NA NA NA NA <0.01
NA NA NA NA NA NA NA 87
NA NA NA NA NA NA NA <1
NA NA NA NA NA NA NA 530
MW-2
Table 3. Summary of Recent Site Groundwater Monitoring Data (cont.)
Highway 55 Landfill
CEC Project No. 111-370.003
Well I.D.
Sampling Date
Organics (µg/L)2L Std.
Benzene 1
Bis(2-ethylhexyl)phthalate 3
Carbon Disulfide 700
cis-1,2-Dichloroethene 70
2,4-Dimethylphenol 100
Diethylphthalate 6,000
2,4 -D 70
4-4'-DDT 0.1
Dieldrin 0
Dinoseb 7
Endosulfan II 40
Endosulfan sulfate 40
Endrin 2
Endrin aldehyde 2
Methylene Chloride 5
Trichloroethene 3
Vinyl Chloride 0.03
Toluene 600
Xylenes 500
beta-BHC NS
1,1-Dichloroethane 6
1,2-Dichloroethane 0.4
1,1-Dichloroethene 350
Tetrachloroethene 0.7
Tetrahydrofuran NS
Naphthalene 6
Acetophenone 700
Metals (µg/L)
Antimony 1
Arsenic 10
Barium 700
Beryllium 4
Cadmium 2
Calcium NS
Chromium 10
Cobalt 1
Copper 1,000
Iron 300
Lead 15
Manganese 50
Nickel 100
Vanadium 0.3
Zinc 1,000
Indicator Parameters (mg/L)
Alkalinity NS
Ammonia- N 1.5
Carbon Dioxide NS
Chloride 250
Cyanide 70
Sulfate 250
Sulfide NS
TDS 500
Bold values exceed the NCDEQ Standards
Bold and highlighted values
exceed the NCDEQ Standards
yet the analyte concentrations
are within the range of naturally-
occurring levels.
2L Std. = 15A NCAC 02L .0202 Groundwater
Standards or Interim Maximum Allowable
Concentrations (IMACs) (Eff. April 1, 2013)
11/4/13 4/2/14 10/20/14 4/23/15 10/12/15 4/25/16 10/31/16 4/20/17
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
1.9 J 1.9 J 1.9 J 1.9 J 2.5 J 1.9 J <7.5 <7.5
<1 <1 <1 <1 <1 <1 <2 <2
<1 <1 <1 <1 6.8 <1 2.1 2.1
<1 <1 <1 <1 <1 <1 <7.5 <7.5
<5 <5 <5 <5 <5 <5 <5 <5
<2 <2 <2 <2 0.69 J <2 <2 <2
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<1 <1 <1 <1 <1 <1 <2.3 <2.3
<0.04 <0.04 <0.04 <0.04 0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<1 <1 <1 <1 0.79 J <1 <5 <5
<1 <1 <1 <1 0.92 J <1 <0.5 <0.5
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
<<<<<1 <<1 <1
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.037 <0.037
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<10 <10 <10 <10 <10 <10 <10 <10
<10 <10 <10 <10 <1 <10 <10 <10
<1 <1 <1 <1 0.35 J <1 <3.7 <3.7
1.5 B 1.5 B 1.5 B 1.5 B 0.51 BJ 1.5 B <3 <3
<1.0 <1.0 <1.0 <1.0 3.6 J 5.4 J <1.0 1.6
330 310 310 240 200 330 170 230
<1.0 <1.0 <1.0 <1.0 <1.0 0.24 J <1.0 <1.0
<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50
22,000 22,000 22,000 22,000 110,000 22,000 NA NA
<5.0 <5.0 <5.0 <5.0 1.3 J <5.0 <5.0 <5.0
<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 21
7.1 <2.0 <2.0 <2.0 2.7 J <2.0 <1.0 0.81 J
NA NA NA NA NA NA 4100 4100
<0.50 <0.50 <0.50 <0.50 0.46 J <0.50 <0.50 0.55
1,200 1,200 1,200 1,200 13,000 1,200 11,000 11,000
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 2.1
<5.0 <5.0 <5.0 <5.0 5.1 J <5.0 <5.0 <5.0
21 <20 <20 <20 5.2 J 5.7 BJ <20 <20
NA NA NA NA NA NA NA 470
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA 530
NA NA NA NA NA NA NA <0.01
NA NA NA NA NA NA NA 140
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA 1600
MW-3
Table 3. Summary of Recent Site Groundwater Monitoring Data (cont.)
Highway 55 Landfill
CEC Project No. 111-370.003
Well I.D.
Sampling Date
Organics (µg/L)2L Std.
Benzene 1
Bis(2-ethylhexyl)phthalate 3
Carbon Disulfide 700
cis-1,2-Dichloroethene 70
2,4-Dimethylphenol 100
Diethylphthalate 6,000
2,4 -D 70
4-4'-DDT 0.1
Dieldrin 0
Dinoseb 7
Endosulfan II 40
Endosulfan sulfate 40
Endrin 2
Endrin aldehyde 2
Methylene Chloride 5
Trichloroethene 3
Vinyl Chloride 0.03
Toluene 600
Xylenes 500
beta-BHC NS
1,1-Dichloroethane 6
1,2-Dichloroethane 0.4
1,1-Dichloroethene 350
Tetrachloroethene 0.7
Tetrahydrofuran NS
Naphthalene 6
Acetophenone 700
Metals (µg/L)
Antimony 1
Arsenic 10
Barium 700
Beryllium 4
Cadmium 2
Calcium NS
Chromium 10
Cobalt 1
Copper 1,000
Iron 300
Lead 15
Manganese 50
Nickel 100
Vanadium 0.3
Zinc 1,000
Indicator Parameters (mg/L)
Alkalinity NS
Ammonia- N 1.5
Carbon Dioxide NS
Chloride 250
Cyanide 70
Sulfate 250
Sulfide NS
TDS 500
Bold values exceed the NCDEQ Standards
Bold and highlighted values
exceed the NCDEQ Standards
yet the analyte concentrations
are within the range of naturally-
occurring levels.
2L Std. = 15A NCAC 02L .0202 Groundwater
Standards or Interim Maximum Allowable
Concentrations (IMACs) (Eff. April 1, 2013)
11/4/13 4/2/14 10/20/14 4/23/15 10/12/15 4/25/16 10/31/16 4/19/17
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
1.9 J 1.9 J 1.9 J 1.9 J 2.5 J 1.9 J <5 <7.5
<1 <1 <1 <1 <1 <1 <1 <2
<1 <1 <1 <1 6.8 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <7.5
<5 <5 <5 <5 <5 <5 <5 <5
<2 <2 <2 <2 0.69 J <2 <2 <2
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<1 <1 <1 <1 <1 <1 <1 <2.2
<0.04 <0.04 <0.04 <0.04 0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<1 <1 <1 <1 0.79 J <1 <1 <5
<1 <1 <1 <1 0.92 J <1 <1 <0.5
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
<<<<<1 <1.3 <1
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.038
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<10 <10 <10 47 <10 5.6 2.7 J 6.5
<10 <10 <10 <10 <1 <10 <1 <0.75
<1 <1 <1 <1 0.35 J <1 <1 <3.8
1.5 B 1.5 B 1.5 B 1.5 B 0.51 BJ 1.5 B <1 <3
<1.0 <1.0 <1.0 <1.0 8.6 J 5.1 J 6.1 J 4.4
180 70 150 76 220 15 J 67 J 130
<1.0 <1.0 <1.0 <1.0 <1.0 0.27 J <1.0 <1.0
<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50
22,000 22,000 22,000 22,000 110,000 22,000 NA NA
<5.0 <5.0 <5.0 <5.0 19 3.6 J 2.9 J 6.6
<1.0 <1.0 <1.0 <1.0 12 J 3.2 J <1.0 10
39 <2.0 <2.0 <2.0 <2.0 <2.0 <1.0 <2.0
NA NA NA NA NA NA 4100 <100
<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 0.17 J
1,200 1,200 1,200 1,200 13,000 1,200 11,000 16
<2.0 <2.0 <2.0 <2.0 12 J 8.2 J <2.0 8
<5.0 <5.0 <5.0 <5.0 5.1 J <5.0 3.8 J <5.0
55 21 <20 <20 11 J 5.7 BJ <20 <20
NA NA NA NA NA NA NA 690
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA 100
NA NA NA NA NA NA NA <0.01
NA NA NA NA NA NA NA 75
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA 1100
MW-4
Table 3. Summary of Recent Site Groundwater Monitoring Data (cont.)
Highway 55 Landfill
CEC Project No. 111-370.003
Well I.D.
Sampling Date
Organics (µg/L)2L Std.
Benzene 1
Bis(2-ethylhexyl)phthalate 3
Carbon Disulfide 700
cis-1,2-Dichloroethene 70
2,4-Dimethylphenol 100
Diethylphthalate 6,000
2,4 -D 70
4-4'-DDT 0.1
Dieldrin 0
Dinoseb 7
Endosulfan II 40
Endosulfan sulfate 40
Endrin 2
Endrin aldehyde 2
Methylene Chloride 5
Trichloroethene 3
Vinyl Chloride 0.03
Toluene 600
Xylenes 500
beta-BHC NS
1,1-Dichloroethane 6
1,2-Dichloroethane 0.4
1,1-Dichloroethene 350
Tetrachloroethene 0.7
Tetrahydrofuran NS
Naphthalene 6
Acetophenone 700
Metals (µg/L)
Antimony 1
Arsenic 10
Barium 700
Beryllium 4
Cadmium 2
Calcium NS
Chromium 10
Cobalt 1
Copper 1,000
Iron 300
Lead 15
Manganese 50
Nickel 100
Vanadium 0.3
Zinc 1,000
Indicator Parameters (mg/L)
Alkalinity NS
Ammonia- N 1.5
Carbon Dioxide NS
Chloride 250
Cyanide 70
Sulfate 250
Sulfide NS
TDS 500
Bold values exceed the NCDEQ Standards
Bold and highlighted values
exceed the NCDEQ Standards
yet the analyte concentrations
are within the range of naturally-
occurring levels.
2L Std. = 15A NCAC 02L .0202 Groundwater
Standards or Interim Maximum Allowable
Concentrations (IMACs) (Eff. April 1, 2013)
11/4/13 4/2/14 10/20/14 4/23/15 10/12/15 4/25/16 10/31/16 4/19/17
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
1.9 J 1.9 J 1.9 J 1.9 J 2.5 J 1.9 J <5 <7.8
<1 <1 <1 <1 <1 <1 <1 <2
<1 <1 <1 <1 6.8 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <7.8
<5 <5 <5 <5 <5 <5 0.26 J <5
<2 <2 <2 <2 0.69 J <2 <2 <2
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<1 <1 <1 <1 <1 <1 <1 <2.2
<0.04 <0.04 <0.04 <0.04 0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<1 <1 <1 <1 0.79 J <1 <1 <5
<1 <1 <1 <1 0.92 J <1 <1 <0.5
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
<<<<<1 <<1 <1
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<10 <10 <10 <10 <10 <10 <10 <10
<10 <10 <10 <10 <1 <10 <1 <0.78
<1 <1 <1 <1 0.35 J <1 <1 <3.9
1.5 B 1.5 B 1.5 B 1.5 B 0.51 BJ 1.5 B 0.32 BJ <3
<1.0 <1.0 <1.0 <1.0 <1.0 3.3 J <1.0 0.30 J
140 65 130 56 50 50 41 82
<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50
22,000 22,000 22,000 22,000 110,000 22,000 NA NA
5.3 <5.0 8.1 <5.0 1.1 J <5.0 <5.0 <5.0
<1.0 <1.0 <1.0 <1.0 1.3 J <1.0 <1.0 10
13 <2.0 6.7 <2.0 <2.0 <2.0 <1.0 <2.0
NA NA NA NA NA NA 4100 540
<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50
1,200 1,200 1,200 1,200 1,200 1,200 11,000 37
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 1.3 J
<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0
100 <20 43 <20 8.4 J 0.31 BJ <20 <20
NA NA NA NA NA NA NA 99
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA 16
NA NA NA NA NA NA NA <0.01
NA NA NA NA NA NA NA 34
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA 200
MW-5
Table 3. Summary of Recent Site Groundwater Monitoring Data (cont.)
Highway 55 Landfill
CEC Project No. 111-370.003
Well I.D.
Sampling Date
Organics (µg/L)2L Std.
Benzene 1
Bis(2-ethylhexyl)phthalate 3
Carbon Disulfide 700
cis-1,2-Dichloroethene 70
2,4-Dimethylphenol 100
Diethylphthalate 6,000
2,4 -D 70
4-4'-DDT 0.1
Dieldrin 0
Dinoseb 7
Endosulfan II 40
Endosulfan sulfate 40
Endrin 2
Endrin aldehyde 2
Methylene Chloride 5
Trichloroethene 3
Vinyl Chloride 0.03
Toluene 600
Xylenes 500
beta-BHC NS
1,1-Dichloroethane 6
1,2-Dichloroethane 0.4
1,1-Dichloroethene 350
Tetrachloroethene 0.7
Tetrahydrofuran NS
Naphthalene 6
Acetophenone 700
Metals (µg/L)
Antimony 1
Arsenic 10
Barium 700
Beryllium 4
Cadmium 2
Calcium NS
Chromium 10
Cobalt 1
Copper 1,000
Iron 300
Lead 15
Manganese 50
Nickel 100
Vanadium 0.3
Zinc 1,000
Indicator Parameters (mg/L)
Alkalinity NS
Ammonia- N 1.5
Carbon Dioxide NS
Chloride 250
Cyanide 70
Sulfate 250
Sulfide NS
TDS 500
Bold values exceed the NCDEQ Standards
Bold and highlighted values
exceed the NCDEQ Standards
yet the analyte concentrations
are within the range of naturally-
occurring levels.
2L Std. = 15A NCAC 02L .0202 Groundwater
Standards or Interim Maximum Allowable
Concentrations (IMACs) (Eff. April 1, 2013)
11/4/13 4/2/14 10/20/14 4/23/15 10/12/15 4/25/16 10/31/16 4/19/17
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
1.9 J 1.9 J 1.9 J 1.9 J 2.5 J 1.9 J <7.4 <7.4
<1 <1 <1 <1 <1 <1 <2 <2
<1 <1 <1 <1 6.8 <1 <1 <1
<1 <1 <1 <1 <1 <1 <7.4 <7.4
<5 <5 <5 <5 <5 <5 <5 <5
<2 <2 <2 <2 0.69 J <2 <2 <2
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<1 <1 <1 <1 <1 <1 <2.3 <2.3
<0.04 <0.04 <0.04 <0.04 0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<1 <1 <1 <1 0.79 J <1 <5 <5
<1 <1 <1 <1 0.92 J <1 <0.5 <0.5
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
<<<<<1 <<1 <1
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.037 <0.037
<1 <1 <1 <1 0.97 J <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<10 <10 <10 <10 <10 <10 <10 <10
<10 <10 <10 <10 <1 <10 <0.74 <0.74
<1 <1 <1 <1 0.35 J <1 <3.7 <3.7
1.5 B 1.5 B 1.5 B 1.5 B 0.51 BJ 1.5 B <3 <3
<1.0 <1.0 <1.0 <1.0 3.5 J <1.0 3 J 9.7
62 75 36 <25 60 17 J 33 270
<1.0 <1.0 <1.0 <1.0 <1.0 0.24 J <1.0 0.58 J
<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 0.36 J
22,000 22,000 22,000 22,000 110,000 22,000 NA NA
<5.0 <5.0 <5.0 <5.0 0.74 J <5.0 <5.0 3.8 J
<1.0 <1.0 <1.0 <1.0 <1.0 2.2 J 1.5 J 4.2
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <1.0 8.9
NA NA NA NA NA NA 4100 47,000
<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 21
1,200 1,200 1,200 1,200 1,200 1,200 11,000 10,000
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 4.7
<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 3.4 J 14
<20 <20 <20 <20 4.1 J 6.0 BJ 19 38 B
NA NA NA NA NA NA NA 11
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA 36
NA NA NA NA NA NA NA <0.10
NA NA NA NA NA NA NA 17
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA 130
MW-6
Table 3. Summary of Recent Site Groundwater Monitoring Data (cont.)
Highway 55 Landfill
CEC Project No. 111-370.003
Well I.D.
Sampling Date
Organics (µg/L)2L Std.
Benzene 1
Bis(2-ethylhexyl)phthalate 3
Carbon Disulfide 700
cis-1,2-Dichloroethene 70
2,4-Dimethylphenol 100
Diethylphthalate 6,000
2,4 -D 70
4-4'-DDT 0.1
Dieldrin 0
Dinoseb 7
Endosulfan II 40
Endosulfan sulfate 40
Endrin 2
Endrin aldehyde 2
Methylene Chloride 5
Trichloroethene 3
Vinyl Chloride 0.03
Toluene 600
Xylenes 500
beta-BHC NS
1,1-Dichloroethane 6
1,2-Dichloroethane 0.4
1,1-Dichloroethene 350
Tetrachloroethene 0.7
Tetrahydrofuran NS
Naphthalene 6
Acetophenone 700
Metals (µg/L)
Antimony 1
Arsenic 10
Barium 700
Beryllium 4
Cadmium 2
Calcium NS
Chromium 10
Cobalt 1
Copper 1,000
Iron 300
Lead 15
Manganese 50
Nickel 100
Vanadium 0.3
Zinc 1,000
Indicator Parameters (mg/L)
Alkalinity NS
Ammonia- N 1.5
Carbon Dioxide NS
Chloride 250
Cyanide 70
Sulfate 250
Sulfide NS
TDS 500
Bold values exceed the NCDEQ Standards
Bold and highlighted values
exceed the NCDEQ Standards
yet the analyte concentrations
are within the range of naturally-
occurring levels.
2L Std. = 15A NCAC 02L .0202 Groundwater
Standards or Interim Maximum Allowable
Concentrations (IMACs) (Eff. April 1, 2013)
11/4/13 4/2/14 10/20/14 4/23/15 10/12/15 4/25/16 10/31/16 4/19/17
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
1.9 J 1.9 J 1.9 J 1.9 J 2.5 J 1.9 J <7.5 <7.5
<1 <1 <1 <1 <1 <1 <2 <2
<1 <1 <1 <1 6.8 <1 <1 <1
<1 <1 <1 <1 <1 <1 <7.5 <7.5
<5 <5 <5 <5 <5 <5 <5 <5
<2 <2 <2 <2 0.69 J <2 <2 <2
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<1 <1 <1 <1 <1 <1 <2.4 <2.4
<0.04 <0.04 <0.04 <0.04 0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<1 <1 <1 <1 0.79 J <1 <5 <5
<1 <1 <1 <1 0.92 J <1 <0.5 <0.5
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
<<<<<1 <<1 <1
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.037 <0.037
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<10 <10 <10 <10 <10 <10 <10 <10
<10 <10 <10 <10 <1 <10 <0.75 <0.75
<1 <1 <1 <1 0.35 J <1 <3.8 <3.8
1.5 B 1.5 B 1.5 B 1.5 B 0.51 BJ 1.5 B <3 <3
11 <1.0 <1.0 <1.0 8.0 J 6.6 J 4.6 J 3.6
180 60 40 80 98 62 94 61
<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50
22,000 22,000 22,000 22,000 110,000 22,000 NA NA
11 <5.0 <5.0 <5.0 0.28 J <5.0 <5.0 <5.0
<1.0 <1.0 <1.0 <1.0 1.5 J <1.0 <1.0 1.3
35 <2.0 5.2 <2.0 5.2 <2.0 8.7 J 1.0 J
NA NA NA NA NA NA 4100 300
28 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 0.41 J
1,200 1,200 1,200 1,200 13,000 1,200 11,000 220
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 1.2 J
<5.0 <5.0 <5.0 <5.0 4.4 J <5.0 0.5 J <5.0
92 <20 670 <20 17 J 7.2 BJ 34 <20
NA NA NA NA NA NA NA 170
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA 42
NA NA NA NA NA NA NA <0.01
NA NA NA NA NA NA NA 74
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA 390
MW-7
Table 3. Summary of Recent Site Groundwater Monitoring Data (cont.)
Highway 55 Landfill
CEC Project No. 111-370.003
Well I.D.
Sampling Date
Organics (µg/L)2L Std.
Benzene 1
Bis(2-ethylhexyl)phthalate 3
Carbon Disulfide 700
cis-1,2-Dichloroethene 70
2,4-Dimethylphenol 100
Diethylphthalate 6,000
2,4 -D 70
4-4'-DDT 0.1
Dieldrin 0
Dinoseb 7
Endosulfan II 40
Endosulfan sulfate 40
Endrin 2
Endrin aldehyde 2
Methylene Chloride 5
Trichloroethene 3
Vinyl Chloride 0.03
Toluene 600
Xylenes 500
beta-BHC NS
1,1-Dichloroethane 6
1,2-Dichloroethane 0.4
1,1-Dichloroethene 350
Tetrachloroethene 0.7
Tetrahydrofuran NS
Naphthalene 6
Acetophenone 700
Metals (µg/L)
Antimony 1
Arsenic 10
Barium 700
Beryllium 4
Cadmium 2
Calcium NS
Chromium 10
Cobalt 1
Copper 1,000
Iron 300
Lead 15
Manganese 50
Nickel 100
Vanadium 0.3
Zinc 1,000
Indicator Parameters (mg/L)
Alkalinity NS
Ammonia- N 1.5
Carbon Dioxide NS
Chloride 250
Cyanide 70
Sulfate 250
Sulfide NS
TDS 500
Bold values exceed the NCDEQ Standards
Bold and highlighted values
exceed the NCDEQ Standards
yet the analyte concentrations
are within the range of naturally-
occurring levels.
2L Std. = 15A NCAC 02L .0202 Groundwater
Standards or Interim Maximum Allowable
Concentrations (IMACs) (Eff. April 1, 2013)
11/4/13 4/2/14 10/20/14 4/23/15 10/12/15 4/25/16 10/31/16 4/20/17
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
1.9 J 1.9 J 1.9 J 1.9 J 2.5 J 1.9 J <7.5 <7.5
<1 <1 <1 <1 <1 <1 <2 <2
<1 <1 <1 <1 6.8 <1 <1 <1
<1 <1 <1 <1 <1 <1 <7.5 <7.5
<5 <5 <5 <5 <5 <5 <5 <5
<2 <2 <2 <2 0.69 J <2 <2 <2
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<1 <1 <1 <1 <1 <1 <2.4 <2.4
<0.04 <0.04 <0.04 <0.04 0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<1 <1 <1 <1 0.79 J <1 <5 <5
<1 <1 <1 <1 0.92 J <1 <0.5 <0.5
4.1 <0.5 5.3 <0.5 <0.5 <0.5 2.8 4.2
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
<<<<<1 <<1 <1
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.037 <0.037
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<10 <10 <10 <10 <10 <10 <10 <10
<10 <10 <10 <10 <1 <10 <0.75 <0.75
<1 <1 <1 <1 0.35 J <1 <3.8 <3.8
1.5 B 1.5 B 1.5 B 1.5 B 0.51 BJ 1.5 B <3 <3
21 <1.0 <1.0 <1.0 8.4 J 3.0 J <1.0 1.8
550 48 <25 29 160 43 20 J 70
<1.0 <1.0 <1.0 <1.0 0.26 J <1.0 <1.0 <1
<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50
22,000 22,000 22,000 22,000 110,000 22,000 NA NA
<5.0 <5.0 <5.0 <5.0 8.1 <5.0 1.2 J <5.0
<1.0 <1.0 <1.0 <1.0 6.9 J 2.2 J 1.3 J 1.8
15 6 <2.0 <2.0 11 <2.0 <1.0 1.3 J
NA NA NA NA NA NA 4100 300
<0.50 <0.50 <0.50 <0.50 7.6 J <0.50 <0.50 0.54
1,200 1,200 1,200 1,200 13,000 1,200 11,000 220
<2.0 <2.0 <2.0 <2.0 7.3 J <2.0 <2.0 3.2
<5.0 <5.0 <5.0 <5.0 23 J <5.0 3.2 J 2.0 J
28 37 <20 <20 38 7.8 BJ 7.1 J <20
NA NA NA NA NA NA NA 250
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA 93
NA NA NA NA NA NA NA <0.01
NA NA NA NA NA NA NA 26
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA 470
MW-8
Table 3. Summary of Recent Site Groundwater Monitoring Data (cont.)
Highway 55 Landfill
CEC Project No. 111-370.003
Well I.D.
Sampling Date
Organics (µg/L)2L Std.
Benzene 1
Bis(2-ethylhexyl)phthalate 3
Carbon Disulfide 700
cis-1,2-Dichloroethene 70
2,4-Dimethylphenol 100
Diethylphthalate 6,000
2,4 -D 70
4-4'-DDT 0.1
Dieldrin 0
Dinoseb 7
Endosulfan II 40
Endosulfan sulfate 40
Endrin 2
Endrin aldehyde 2
Methylene Chloride 5
Trichloroethene 3
Vinyl Chloride 0.03
Toluene 600
Xylenes 500
beta-BHC NS
1,1-Dichloroethane 6
1,2-Dichloroethane 0.4
1,1-Dichloroethene 350
Tetrachloroethene 0.7
Tetrahydrofuran NS
Naphthalene 6
Acetophenone 700
Metals (µg/L)
Antimony 1
Arsenic 10
Barium 700
Beryllium 4
Cadmium 2
Calcium NS
Chromium 10
Cobalt 1
Copper 1,000
Iron 300
Lead 15
Manganese 50
Nickel 100
Vanadium 0.3
Zinc 1,000
Indicator Parameters (mg/L)
Alkalinity NS
Ammonia- N 1.5
Carbon Dioxide NS
Chloride 250
Cyanide 70
Sulfate 250
Sulfide NS
TDS 500
Bold values exceed the NCDEQ Standards
Bold and highlighted values
exceed the NCDEQ Standards
yet the analyte concentrations
are within the range of naturally-
occurring levels.
2L Std. = 15A NCAC 02L .0202 Groundwater
Standards or Interim Maximum Allowable
Concentrations (IMACs) (Eff. April 1, 2013)
11/4/13 4/2/14 10/20/14 4/23/15 10/12/15 4/25/16 10/31/16 4/19/17
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
1.9 J 1.9 J 1.9 J 1.9 J 2.5 J 1.9 J <7.5 <7.5
<1 <1 <1 <1 <1 <1 <2 <2
<1 <1 <1 <1 6.8 <1 <1 <1
<1 <1 <1 <1 <1 <1 <7.5 <7.5
<5 <5 <5 <5 <5 <5 <5 <5
<2 <2 <2 <2 0.69 J <2 <2 <2
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<1 <1 <1 <1 <1 <1 <2.4 <2.4
<0.04 <0.04 <0.04 <0.04 0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<1 <1 <1 <1 0.79 J <1 <5 <5
<1 <1 <1 <1 0.92 J <1 <0.5 <0.5
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
<<<<<1 <<1 <1
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.037 <0.037
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<10 <10 <10 <10 <10 <10 <10 <10
<10 <10 <10 <10 <1 <10 <0.75 <0.75
<1 <1 <1 <1 0.35 J <1 <3.8 <3.8
1.5 B 1.5 B 1.5 B 1.5 B 0.51 BJ 1.5 B <3 <3
10 <1.0 <1.0 <1.0 3.4 J 3.1 J <1.0 2.3
310 180 400 210 310 170 320 360
<1.0 <1.0 <1.0 <1.0 <1.0 0.22 J <1.0 <1
<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50
22,000 22,000 22,000 22,000 110,000 22,000 NA NA
9.7 <5.0 10 <5.0 4.1 J <5.0 <5.0 <5.0
<1.0 <1.0 <1.0 <1.0 2.3 J 1.3 J <1.0 0.77 J
7.4 <2.0 9.1 <2.0 2.9 J <2.0 <1.0 0.72 J
NA NA NA NA NA NA 4100 300
<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 0.23 J
1,200 1,200 1,200 1,200 13,000 1,200 11,000 220
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 2
<5.0 <5.0 <5.0 <5.0 9.7 J <5.0 <5.0 2.0 J
57 <20 62 <20 19 J 4.1 BJ <20 <20
NA NA NA NA NA NA NA 250
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA 500
NA NA NA NA NA NA NA <0.01
NA NA NA NA NA NA NA 43
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA 210
MW-9
Table 3. Summary of Recent Site Groundwater Monitoring Data (cont.)
Highway 55 Landfill
CEC Project No. 111-370.003
Well I.D.
Sampling Date
Organics (µg/L)2L Std.
Benzene 1
Bis(2-ethylhexyl)phthalate 3
Carbon Disulfide 700
cis-1,2-Dichloroethene 70
2,4-Dimethylphenol 100
Diethylphthalate 6,000
2,4 -D 70
4-4'-DDT 0.1
Dieldrin 0
Dinoseb 7
Endosulfan II 40
Endosulfan sulfate 40
Endrin 2
Endrin aldehyde 2
Methylene Chloride 5
Trichloroethene 3
Vinyl Chloride 0.03
Toluene 600
Xylenes 500
beta-BHC NS
1,1-Dichloroethane 6
1,2-Dichloroethane 0.4
1,1-Dichloroethene 350
Tetrachloroethene 0.7
Tetrahydrofuran NS
Naphthalene 6
Acetophenone 700
Metals (µg/L)
Antimony 1
Arsenic 10
Barium 700
Beryllium 4
Cadmium 2
Calcium NS
Chromium 10
Cobalt 1
Copper 1,000
Iron 300
Lead 15
Manganese 50
Nickel 100
Vanadium 0.3
Zinc 1,000
Indicator Parameters (mg/L)
Alkalinity NS
Ammonia- N 1.5
Carbon Dioxide NS
Chloride 250
Cyanide 70
Sulfate 250
Sulfide NS
TDS 500
Bold values exceed the NCDEQ Standards
Bold and highlighted values
exceed the NCDEQ Standards
yet the analyte concentrations
are within the range of naturally-
occurring levels.
2L Std. = 15A NCAC 02L .0202 Groundwater
Standards or Interim Maximum Allowable
Concentrations (IMACs) (Eff. April 1, 2013)
11/4/13 4/2/14 10/20/14 4/23/15 10/12/15 4/25/16 10/31/16 4/19/17
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
1.9 J 1.9 J 1.9 J 1.9 J 2.5 J 1.9 J <7.5 <7.5
<1 <1 <1 <1 <1 <1 <2 <2
<1 <1 <1 <1 6.8 <1 <1 <1
<1 <1 <1 <1 <1 <1 <7.5 <7.5
<5 <5 <5 <5 <5 <5 <5 <5
<2 <2 <2 <2 0.69 J <2 <2 <2
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<1 <1 <1 <1 <1 <1 <2.4 <2.4
<0.04 <0.04 <0.04 <0.04 0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<1 <1 <1 <1 0.79 J <1 <5 <5
<1 <1 <1 <1 0.92 J <1 <0.5 <0.5
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
<<<<<1 <<1 <1
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.037 <0.037
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<10 <10 <10 <10 <10 <10 <10 <10
<10 <10 <10 <10 <1 <10 <0.75 <0.75
<1 <1 <1 <1 0.35 J <1 <3.8 <3.8
1.5 B 1.5 B 1.5 B 1.5 B 0.51 BJ 1.5 B <3 <3
<1.0 <1.0 <1.0 <1.0 3.8 J 7.4 J 5.1 1.5
1400 1300 1400 1500 1500 1300 1400 1400
<1.0 <1.0 <1.0 <1.0 <1.0 0.30 J 0.27 J <1
<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50
22,000 22,000 22,000 22,000 110,000 22,000 NA NA
<5.0 <5.0 <5.0 <5.0 1.4 J <5.0 <5.0 <5.0
<1.0 <1.0 <1.0 <1.0 <1.0 1.5 J <1.0 <1.0
<2.0 <2.0 13 <2.0 <2.0 <2.0 <1.0 0.90 J
NA NA NA NA NA NA 4100 300
<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50
1,200 1,200 1,200 1,200 1,200 1,200 11,000 220
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0
<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0
<20 <20 62 <20 24 20 B 34 <20
NA NA NA NA NA NA NA 560
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA 2300
NA NA NA NA NA NA NA <0.01
NA NA NA NA NA NA NA 23
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA 4900
MW-10
Table 3. Summary of Recent Site Groundwater Monitoring Data (cont.)
Highway 55 Landfill
CEC Project No. 111-370.003
Well I.D.
Sampling Date
Organics (µg/L)2L Std.
Benzene 1
Bis(2-ethylhexyl)phthalate 3
Carbon Disulfide 700
cis-1,2-Dichloroethene 70
2,4-Dimethylphenol 100
Diethylphthalate 6,000
2,4 -D 70
4-4'-DDT 0.1
Dieldrin 0
Dinoseb 7
Endosulfan II 40
Endosulfan sulfate 40
Endrin 2
Endrin aldehyde 2
Methylene Chloride 5
Trichloroethene 3
Vinyl Chloride 0.03
Toluene 600
Xylenes 500
beta-BHC NS
1,1-Dichloroethane 6
1,2-Dichloroethane 0.4
1,1-Dichloroethene 350
Tetrachloroethene 0.7
Tetrahydrofuran NS
Naphthalene 6
Acetophenone 700
Metals (µg/L)
Antimony 1
Arsenic 10
Barium 700
Beryllium 4
Cadmium 2
Calcium NS
Chromium 10
Cobalt 1
Copper 1,000
Iron 300
Lead 15
Manganese 50
Nickel 100
Vanadium 0.3
Zinc 1,000
Indicator Parameters (mg/L)
Alkalinity NS
Ammonia- N 1.5
Carbon Dioxide NS
Chloride 250
Cyanide 70
Sulfate 250
Sulfide NS
TDS 500
Bold values exceed the NCDEQ Standards
Bold and highlighted values
exceed the NCDEQ Standards
yet the analyte concentrations
are within the range of naturally-
occurring levels.
2L Std. = 15A NCAC 02L .0202 Groundwater
Standards or Interim Maximum Allowable
Concentrations (IMACs) (Eff. April 1, 2013)
11/4/13 4/2/14 10/20/14 4/23/15 10/12/15 4/25/16 10/31/16 4/19/17
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
1.9 J 1.9 J 1.9 J 1.9 J 2.5 J 1.9 J <7.5 <7.5
<1 <1 <1 <1 <1 <1 <2 <2
<1 <1 <1 <1 6.8 <1 <1 <1
<1 <1 <1 <1 <1 <1 <7.5 <7.5
<5 <5 <5 <5 <5 <5 <5 <5
<2 <2 <2 <2 0.69 J <2 <2 <2
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<1 <1 <1 <1 <1 <1 <2.4 <2.4
<0.04 <0.04 <0.04 <0.04 0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.04
<1 <1 <1 <1 0.79 J <1 <5 <5
<1 <1 <1 <1 0.92 J <1 <0.5 <0.5
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
<<<<<1 <<1 <1
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 <0.037 <0.037
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<10 <10 <10 <10 <10 <10 <10 <10
<10 <10 <10 <10 <1 <10 <0.75 <0.75
<1 <1 <1 <1 0.35 J <1 <3.8 <3.8
1.5 B 1.5 B 1.5 B 1.5 B 0.51 BJ 1.5 B <3 <3
<1.0 <1.0 <1.0 <1.0 <1.0 4.3 J 6 J 1.4
120 1400 190 210 250 300 1400 420
<1.0 <1.0 <1.0 <1.0 0.52 J 0.54 J 0.3 J 0.78 J
<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 0.72
22,000 22,000 22,000 22,000 110,000 22,000 NA NA
<5.0 <5.0 <5.0 <5.0 1.6 J <5.0 <5 <5
<1.0 <1.0 <1.0 <1.0 7.5 J 9.8 J 13 11
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <1.0 0.72 J
NA NA NA NA NA NA 300 300
<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 1.9
1,200 1,200 1,200 1,200 1,200 1,200 220 220
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 2.6
<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0
<20 <20 <20 4900 340 75 B 14 J 12 J
NA NA NA NA NA NA NA 74
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA 170
NA NA NA NA NA NA NA <0.01
NA NA NA NA NA NA NA 26
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA 690
MW-11
Table 3. Summary of Recent Site Groundwater Monitoring Data (cont.)
Highway 55 Landfill
CEC Project No. 111-370.003
Well I.D.
Sampling Date
Organics (µg/L)2L Std.
Benzene 1
Bis(2-ethylhexyl)phthalate 3
Carbon Disulfide 700
cis-1,2-Dichloroethene 70
2,4-Dimethylphenol 100
Diethylphthalate 6,000
2,4 -D 70
4-4'-DDT 0.1
Dieldrin 0
Dinoseb 7
Endosulfan II 40
Endosulfan sulfate 40
Endrin 2
Endrin aldehyde 2
Methylene Chloride 5
Trichloroethene 3
Vinyl Chloride 0.03
Toluene 600
Xylenes 500
beta-BHC NS
1,1-Dichloroethane 6
1,2-Dichloroethane 0.4
1,1-Dichloroethene 350
Tetrachloroethene 0.7
Tetrahydrofuran NS
Naphthalene 6
Acetophenone 700
Metals (µg/L)
Antimony 1
Arsenic 10
Barium 700
Beryllium 4
Cadmium 2
Calcium NS
Chromium 10
Cobalt 1
Copper 1,000
Iron 300
Lead 15
Manganese 50
Nickel 100
Vanadium 0.3
Zinc 1,000
Indicator Parameters (mg/L)
Alkalinity NS
Ammonia- N 1.5
Carbon Dioxide NS
Chloride 250
Cyanide 70
Sulfate 250
Sulfide NS
TDS 500
Bold values exceed the NCDEQ Standards
Bold and highlighted values
exceed the NCDEQ Standards
yet the analyte concentrations
are within the range of naturally-
occurring levels.
2L Std. = 15A NCAC 02L .0202 Groundwater
Standards or Interim Maximum Allowable
Concentrations (IMACs) (Eff. April 1, 2013)
11/4/13 4/2/14 10/20/14 4/23/15 10/12/15 4/25/16 10/31/16 4/20/17
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.65 J <0.5
1.9 J 1.9 J 1.9 J 1.9 J 2.5 J 1.9 J NA NA
<1 <1 <1 <1 <1 <1 <1 <2
<1 <1 <1 <1 6.8 <1 <1 <1
<1 <1 <1 <1 <1 <1 NA NA
<5 <5 <5 <5 <5 <5 NA NA
<2 <2 <2 <2 0.69 J <2 NA NA
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NA NA
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NA NA
<1 <1 <1 <1 <1 <1 NA NA
<0.04 <0.04 <0.04 <0.04 0.04 <0.04 NA NA
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NA NA
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NA NA
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NA NA
<1 <1 <1 <1 0.79 J <1 <1 <5
<1 <1 <1 <1 0.92 J <1 <1 <0.5
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 51 0.95
<<<<<1 <<1 <1
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NA NA
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<10 <10 <10 <10 <10 <10 <10 <10
<10 <10 <10 <10 <1 <10 NA NA
<1 <1 <1 <1 0.35 J <1 NA NA
1.5 B 1.5 B 1.5 B 1.5 B 0.51 BJ 1.5 B <1 <1
<1.0 <1.0 <1.0 <1.0 <1.0 2.5 J 15 0.61 J
69 480 110 82 110 64 520 48
<1.0 <1.0 <1.0 <1.0 <1.0 0.34 <1 <1
<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50
22,000 22,000 22,000 22,000 110,000 22,000 NA NA
<5.0 16 <5.0 <5.0 1.1 J 1.4 J 0.98 J <5
<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 5.2 J 0.58 J
<2.0 19 <2.0 <2.0 <2.0 <2.0 <1.0 0.95 J
NA NA NA NA NA NA 3000 3000
<0.50 16 <0.50 <0.50 <0.50 <0.50 <0.50 0.38 J
1,200 1,200 1,200 1,200 1,200 1,200 230 230
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0 5.3 J <2.0
<5.0 68 <5.0 <5.0 <5.0 5.4 16 J <5.0
<20 150 <20 <20 5.2 J 9.6 BJ 13 J <20
NA NA NA NA NA NA NA 27
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA 28
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA 4
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA 84
SW-1
Table 3. Summary of Recent Site Groundwater Monitoring Data (cont.)
Highway 55 Landfill
CEC Project No. 111-370.003
Well I.D.
Sampling Date
Organics (µg/L)2L Std.
Benzene 1
Bis(2-ethylhexyl)phthalate 3
Carbon Disulfide 700
cis-1,2-Dichloroethene 70
2,4-Dimethylphenol 100
Diethylphthalate 6,000
2,4 -D 70
4-4'-DDT 0.1
Dieldrin 0
Dinoseb 7
Endosulfan II 40
Endosulfan sulfate 40
Endrin 2
Endrin aldehyde 2
Methylene Chloride 5
Trichloroethene 3
Vinyl Chloride 0.03
Toluene 600
Xylenes 500
beta-BHC NS
1,1-Dichloroethane 6
1,2-Dichloroethane 0.4
1,1-Dichloroethene 350
Tetrachloroethene 0.7
Tetrahydrofuran NS
Naphthalene 6
Acetophenone 700
Metals (µg/L)
Antimony 1
Arsenic 10
Barium 700
Beryllium 4
Cadmium 2
Calcium NS
Chromium 10
Cobalt 1
Copper 1,000
Iron 300
Lead 15
Manganese 50
Nickel 100
Vanadium 0.3
Zinc 1,000
Indicator Parameters (mg/L)
Alkalinity NS
Ammonia- N 1.5
Carbon Dioxide NS
Chloride 250
Cyanide 70
Sulfate 250
Sulfide NS
TDS 500
Bold values exceed the NCDEQ Standards
Bold and highlighted values
exceed the NCDEQ Standards
yet the analyte concentrations
are within the range of naturally-
occurring levels.
2L Std. = 15A NCAC 02L .0202 Groundwater
Standards or Interim Maximum Allowable
Concentrations (IMACs) (Eff. April 1, 2013)
11/4/13 4/2/14 10/20/14 4/23/15 10/12/15 4/25/16 10/31/16 4/20/17
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
1.9 J 1.9 J 1.9 J 1.9 J 2.5 J 1.9 J NA NA
<1 <1 <1 <1 <1 <1 <1 <2
<1 <1 <1 <1 6.8 <1 <1 <1
<1 <1 <1 <1 <1 <1 NA NA
<5 <5 <5 <5 <5 <5 NA NA
<2 <2 <2 <2 0.69 J <2 NA NA
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NA NA
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NA NA
<1 <1 <1 <1 <1 <1 NA NA
<0.04 <0.04 <0.04 <0.04 0.04 <0.04 NA NA
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NA NA
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NA NA
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NA NA
<1 <1 <1 <1 0.79 J <1 <1 <5
<1 <1 <1 <1 0.92 J <1 <1 <0.5
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1 <0.5
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1 <0.5
<<<<<1 <<1 <1
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NA NA
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<10 <10 <10 <10 <10 <10 <5 <10
<10 <10 <10 <10 <1 <10 NA NA
<1 <1 <1 <1 0.35 J <1 NA NA
1.5 B 1.5 B 1.5 B 1.5 B 0.51 BJ 1.5 B <1 <1
<1.0 <1.0 <1.0 <1.0 2.2 J <1 0.72 J 0.51 J
130 49 40 120 41 45 290 47
<1.0 <1.0 <1.0 <1.0 <1.0 <1 <0.4 <1
<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.1 <0.50
22,000 22,000 22,000 22,000 110,000 22,000 18,000 NA
<5.0 <5.0 <5.0 5.9 0.91 J 2.8 J 15 J <5
<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 13 J 0.43 J
5 <2.0 <2.0 <2.0 <2.0 <2.0 15 1.2 J
NA NA NA NA NA NA NA 3000
<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 14 0.26 J
1,200 1,200 1,200 1,200 1,200 1,200 170 230
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0 7.3 J <2.0
<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 50 <5.0
57 <20 <20 29 6.0 J 5.4 J 4.3 J <20
NA NA NA NA NA NA NA 36
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA 19
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA 5.8
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA 90
SW-2
Table 3. Summary of Recent Site Groundwater Monitoring Data (cont.)
Highway 55 Landfill
CEC Project No. 111-370.003
Well I.D.
Sampling Date
Organics (µg/L)2L Std.
Benzene 1
Bis(2-ethylhexyl)phthalate 3
Carbon Disulfide 700
cis-1,2-Dichloroethene 70
2,4-Dimethylphenol 100
Diethylphthalate 6,000
2,4 -D 70
4-4'-DDT 0.1
Dieldrin 0
Dinoseb 7
Endosulfan II 40
Endosulfan sulfate 40
Endrin 2
Endrin aldehyde 2
Methylene Chloride 5
Trichloroethene 3
Vinyl Chloride 0.03
Toluene 600
Xylenes 500
beta-BHC NS
1,1-Dichloroethane 6
1,2-Dichloroethane 0.4
1,1-Dichloroethene 350
Tetrachloroethene 0.7
Tetrahydrofuran NS
Naphthalene 6
Acetophenone 700
Metals (µg/L)
Antimony 1
Arsenic 10
Barium 700
Beryllium 4
Cadmium 2
Calcium NS
Chromium 10
Cobalt 1
Copper 1,000
Iron 300
Lead 15
Manganese 50
Nickel 100
Vanadium 0.3
Zinc 1,000
Indicator Parameters (mg/L)
Alkalinity NS
Ammonia- N 1.5
Carbon Dioxide NS
Chloride 250
Cyanide 70
Sulfate 250
Sulfide NS
TDS 500
Bold values exceed the NCDEQ Standards
Bold and highlighted values
exceed the NCDEQ Standards
yet the analyte concentrations
are within the range of naturally-
occurring levels.
2L Std. = 15A NCAC 02L .0202 Groundwater
Standards or Interim Maximum Allowable
Concentrations (IMACs) (Eff. April 1, 2013)
11/4/13 4/2/14 10/20/14 4/23/15 10/12/15 4/25/16 10/31/16 4/20/17
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
1.9 J 1.9 J 1.9 J 1.9 J 2.5 J 1.9 J NA NA
<1 <1 <1 <1 <1 <1 <1 <2
<1 <1 <1 <1 6.8 <1 <1 <1
<1 <1 <1 <1 <1 <1 NA NA
<5 <5 <5 <5 <5 <5 NA NA
<2 <2 <2 <2 0.69 J <2 NA NA
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NA NA
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NA NA
<1 <1 <1 <1 <1 <1 NA NA
<0.04 <0.04 <0.04 <0.04 0.04 <0.04 NA NA
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NA NA
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NA NA
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NA NA
<1 <1 <1 <1 0.79 J <1 <1 <5
<1 <1 <1 <1 0.92 J <1 <1 <0.5
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1 <0.5
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1 <0.5
<<<<<1 <<1 <1
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NA NA
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<10 <10 <10 <10 <10 <10 <5 <10
<10 <10 <10 <10 <1 <10 NA NA
<1 <1 <1 <1 0.35 J <1 NA NA
1.5 B 1.5 B 1.5 B 1.5 B 0.51 BJ 1.5 B <1 <1
<1.0 <1.0 <1.0 <1.0 2.2 J 3.7 J <1 1.6
45 48 120 120 41 100 41 240
<1.0 <1.0 <1.0 <1.0 <1.0 0.34 <1 <1
<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50
22,000 22,000 22,000 22,000 110,000 22,000 18,000 NA
<5.0 <5.0 <5.0 <5.0 <5 7.6 J <5 <5
<1.0 <1.0 <1.0 <1.0 <1.0 3.0 J <5 4.4
<2.0 <2.0 <2.0 <2.0 1.9 J 11 <1.0 5.8
NA NA NA NA NA NA NA 3000
<0.50 <0.50 <0.50 <0.50 <2.0 9.3 J <2.0 1.2
1,200 1,200 1,200 1,200 13,000 1,200 <5.0 230
<2.0 <2.0 <2.0 <2.0 <2.0 4.6 J <2.0 1.9 J
<5.0 <5.0 <5.0 <5.0 <5.0 20 J <5.0 2.7 J
<20 <20 <20 <20 3.9 J 55 B <20 140
NA NA NA NA NA NA NA 97
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA 56
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA 51
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA 90
SW-3
Table 3. Summary of Recent Site Groundwater Monitoring Data (cont.)
Highway 55 Landfill
CEC Project No. 111-370.003
Well I.D.
Sampling Date
Organics (µg/L)2L Std.
Benzene 1
Bis(2-ethylhexyl)phthalate 3
Carbon Disulfide 700
cis-1,2-Dichloroethene 70
2,4-Dimethylphenol 100
Diethylphthalate 6,000
2,4 -D 70
4-4'-DDT 0.1
Dieldrin 0
Dinoseb 7
Endosulfan II 40
Endosulfan sulfate 40
Endrin 2
Endrin aldehyde 2
Methylene Chloride 5
Trichloroethene 3
Vinyl Chloride 0.03
Toluene 600
Xylenes 500
beta-BHC NS
1,1-Dichloroethane 6
1,2-Dichloroethane 0.4
1,1-Dichloroethene 350
Tetrachloroethene 0.7
Tetrahydrofuran NS
Naphthalene 6
Acetophenone 700
Metals (µg/L)
Antimony 1
Arsenic 10
Barium 700
Beryllium 4
Cadmium 2
Calcium NS
Chromium 10
Cobalt 1
Copper 1,000
Iron 300
Lead 15
Manganese 50
Nickel 100
Vanadium 0.3
Zinc 1,000
Indicator Parameters (mg/L)
Alkalinity NS
Ammonia- N 1.5
Carbon Dioxide NS
Chloride 250
Cyanide 70
Sulfate 250
Sulfide NS
TDS 500
Bold values exceed the NCDEQ Standards
Bold and highlighted values
exceed the NCDEQ Standards
yet the analyte concentrations
are within the range of naturally-
occurring levels.
2L Std. = 15A NCAC 02L .0202 Groundwater
Standards or Interim Maximum Allowable
Concentrations (IMACs) (Eff. April 1, 2013)
11/4/13 4/2/14 10/20/14 4/23/15 10/12/15 4/25/16 10/31/16 4/20/17
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
1.9 J 1.9 J 1.9 J 1.9 J 2.5 J 1.9 J NA NA
<1 <1 <1 <1 <1 <1 <1 <2
<1 <1 <1 <1 6.8 <1 <1 <1
<1 <1 <1 <1 <1 <1 NA NA
<5 <5 <5 <5 <5 <5 NA NA
<2 <2 <2 <2 0.69 J <2 NA NA
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NA NA
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NA NA
<1 <1 <1 <1 <1 <1 NA NA
<0.04 <0.04 <0.04 <0.04 0.04 <0.04 NA NA
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NA NA
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NA NA
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NA NA
<1 <1 <1 <1 0.79 J <1 <1 <5
<1 <1 <1 <1 0.92 J <1 <1 <0.5
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1 <0.5
<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1 <0.5
<<<<<1 <<1 <1
<0.04 <0.04 <0.04 <0.04 <0.04 <0.04 NA NA
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<1 <1 <1 <1 <1 <1 <1 <1
<10 <10 <10 <10 <10 <10 <5 <10
<10 <10 <10 <10 <1 <10 NA NA
<1 <1 <1 <1 0.35 J <1 NA NA
1.5 B 1.5 B 1.5 B 1.5 B 0.51 BJ 1.5 B <1 <1
<1.0 <1.0 <1.0 <1.0 <1 <1 13 J 1.8
46 95 39 100 75 45 320 73
<1.0 <1.0 <1.0 <1.0 <1.0 <1 <0.4 <1
<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.1 <0.50
22,000 22,000 22,000 22,000 110,000 22,000 19,000 NA
<5.0 <5.0 <5.0 <5.0 2.6 J <5.0 1.1 J <5
<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5 1.1
<2.0 <2.0 <2.0 <2.0 2.6 J <2.0 5.5 J 16
NA NA NA NA NA NA NA 3000
<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1 0.21 J
1,200 1,200 1,200 1,200 13,000 1,200 170 230
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0 5.6 J <2.0
<5.0 <5.0 <5.0 <5.0 4.8 J <5.0 14 J <5.0
<20 <20 <20 28 9.0 J 13 BJ 8.4 J <20
NA NA NA NA NA NA NA 120
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA 44
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA 20
NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA 280
SW-4

APPENDIX A

APPENDIX B

ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Chicago
2417 Bond Street
University Park, IL 60484
Tel: [phone]
TestAmerica Job ID: 500-126939-1
TestAmerica Sample Delivery Group: 11-370
Client Project/Site: NC Apex Landfill
For:
Civil & Environmental Consultants Inc
1900 Center Park Drive
Suite A
Charlotte, North Carolina 28217
Attn: Phillip Pressley
Authorized for release by:
5/5/2017 2:23:44 PM
Robin Kintz, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Civil & Environmental Consultants Inc
Project/Site: NC Apex Landfill
TestAmerica Job ID: 500-126939-1
SDG: 11-370
Page 2 of 77 TestAmerica Chicago5/5/2017
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .43
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .44
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .49
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .50
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .68
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .74
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .75
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .77
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Case Narrative
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-126939-1
Project/Site: NC Apex Landfill SDG: 11-370
Job ID: 500-126939-1
Laboratory: TestAmerica Chicago
Narrative
Job Narrative
500-126939-1
Comments
No additional comments.
Receipt
The samples were received on 4/21/2017 8:50 AM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperatures of the 2 coolers at receipt time were 3.2º C and 4.8º C.
GC/MS VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Metals
Method(s) 200.8: Due to sample matrix effect on the internal standard (ISTD), a dilution was required for the following sample: MW-6
(500-126939-6). Elevated reporting limits have been reported.
Method(s) 200.8, 6020, 6020A: The internal standard Terbium(Tb) was used to report the elements Tl and Pb in batch 500-382298. This
was due to some samples containing the element Bismuth.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
General Chemistry
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
TestAmerica ChicagoPage 3 of 77 5/5/2017
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Detection Summary
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Client Sample ID: MW-1 Lab Sample ID: 500-126939-1
Arsenic
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.90 200.8
Barium 2.5 ug/L0.37 Total/NA11200200.8
Cobalt 1.0 ug/L0.27 Total/NA10.28 J 200.8
Copper 2.0 ug/L0.63 Total/NA11.1 J 200.8
Silver 0.50 ug/L0.078 Total/NA13.3 200.8
Vanadium 5.0 ug/L2.0 Total/NA14.9 J 200.8
Mercury 0.20 ug/L0.091 Total/NA11.2 245.1
Chloride 200 mg/L170 Total/NA100027009056A
Sulfate 0.40 mg/L0.19 Total/NA23.8 9056A
Alkalinity 5.0 mg/L3.7 Total/NA1410SM 2320B
Total Dissolved Solids 25 mg/L11 Total/NA15600SM 2540C
Client Sample ID: MW-2 Lab Sample ID: 500-126939-2
Arsenic
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA11.2 200.8
Barium 2.5 ug/L0.37 Total/NA174200.8
Cobalt 1.0 ug/L0.27 Total/NA10.59 J 200.8
Copper 2.0 ug/L0.63 Total/NA10.79 J 200.8
Lead 0.50 ug/L0.16 Total/NA10.51 200.8
Nickel 2.0 ug/L0.92 Total/NA12.8 200.8
Vanadium 5.0 ug/L2.0 Total/NA12.5 J 200.8
Chloride 10 mg/L8.5 Total/NA501309056A
Sulfate 10 mg/L4.8 Total/NA50879056A
Alkalinity 5.0 mg/L3.7 Total/NA1160SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1530SM 2540C
Client Sample ID: MW-3 Lab Sample ID: 500-126939-3
Arsenic
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA11.6 200.8
Barium 2.5 ug/L0.37 Total/NA1230200.8
Cobalt 1.0 ug/L0.27 Total/NA121200.8
Copper 2.0 ug/L0.63 Total/NA10.81 J 200.8
Lead 0.50 ug/L0.16 Total/NA10.55 200.8
Nickel 2.0 ug/L0.92 Total/NA12.1 200.8
Chloride 20 mg/L17 Total/NA1005309056A
Sulfate 20 mg/L9.5 Total/NA1001409056A
Alkalinity 5.0 mg/L3.7 Total/NA1470SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA11600SM 2540C
Client Sample ID: MW-4 Lab Sample ID: 500-126939-4
Acetone
RL
5.0 ug/L
MDL
1.7
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA15.9 8260B
Tetrahydrofuran 10 ug/L1.9 Total/NA16.5 J 8260B
Arsenic 1.0 ug/L0.15 Total/NA14.4 200.8
Barium 2.5 ug/L0.37 Total/NA1130200.8
Chromium 5.0 ug/L2.3 Total/NA16.6 200.8
Cobalt 1.0 ug/L0.27 Total/NA110200.8
TestAmerica Chicago
This Detection Summary does not include radiochemical test results.
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Detection Summary
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Client Sample ID: MW-4 (Continued)Lab Sample ID: 500-126939-4
Lead
RL
0.50 ug/L
MDL
0.16
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.17 200.8
Nickel 2.0 ug/L0.92 Total/NA18.0 200.8
Chloride 10 mg/L8.5 Total/NA501009056A
Sulfate 10 mg/L4.8 Total/NA50759056A
Alkalinity 5.0 mg/L3.7 Total/NA1690SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA11100SM 2540C
Client Sample ID: MW-5 Lab Sample ID: 500-126939-5
Arsenic
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.30 200.8
Barium 2.5 ug/L0.37 Total/NA182200.8
Cobalt 1.0 ug/L0.27 Total/NA110200.8
Nickel 2.0 ug/L0.92 Total/NA11.3 J 200.8
Chloride 1.0 mg/L0.85 Total/NA5169056A
Sulfate 1.0 mg/L0.48 Total/NA5349056A
Alkalinity 5.0 mg/L3.7 Total/NA199SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1200SM 2540C
Client Sample ID: MW-6 Lab Sample ID: 500-126939-6
Arsenic
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA19.7 200.8
Barium 5.0 ug/L0.75 Total/NA2270200.8
Beryllium 1.0 ug/L0.43 Total/NA10.58 J 200.8
Cadmium 0.50 ug/L0.15 Total/NA10.36 J 200.8
Chromium 5.0 ug/L2.3 Total/NA13.8 J 200.8
Cobalt 1.0 ug/L0.27 Total/NA14.2 200.8
Copper 2.0 ug/L0.63 Total/NA18.9 200.8
Lead 1.0 ug/L0.31 Total/NA221200.8
Nickel 2.0 ug/L0.92 Total/NA14.7 200.8
Silver 0.50 ug/L0.078 Total/NA10.099 J 200.8
Vanadium 5.0 ug/L2.0 Total/NA114200.8
Zinc 20 ug/L8.1 Total/NA138 B 200.8
Chloride 2.0 mg/L1.7 Total/NA10369056A
Sulfate 2.0 mg/L0.95 Total/NA10179056A
Alkalinity 5.0 mg/L3.7 Total/NA111SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1130SM 2540C
Client Sample ID: MW-7 Lab Sample ID: 500-126939-7
Arsenic
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA13.6 200.8
Barium 2.5 ug/L0.37 Total/NA161200.8
Cobalt 1.0 ug/L0.27 Total/NA11.3 200.8
Copper 2.0 ug/L0.63 Total/NA11.0 J 200.8
Lead 0.50 ug/L0.16 Total/NA10.41 J 200.8
Nickel 2.0 ug/L0.92 Total/NA11.2 J 200.8
Chloride 2.0 mg/L1.7 Total/NA10429056A
Sulfate 2.0 mg/L0.95 Total/NA10749056A
TestAmerica Chicago
This Detection Summary does not include radiochemical test results.
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Detection Summary
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Client Sample ID: MW-7 (Continued)Lab Sample ID: 500-126939-7
Alkalinity
RL
5.0 mg/L
MDL
3.7
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1170SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1390SM 2540C
Client Sample ID: MW-8 Lab Sample ID: 500-126939-8
Vinyl chloride
RL
0.50 ug/L
MDL
0.20
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA14.2 8260B
Arsenic 1.0 ug/L0.15 Total/NA11.8 200.8
Barium 2.5 ug/L0.37 Total/NA170200.8
Cobalt 1.0 ug/L0.27 Total/NA11.8 200.8
Copper 2.0 ug/L0.63 Total/NA11.3 J 200.8
Lead 0.50 ug/L0.16 Total/NA10.54 200.8
Nickel 2.0 ug/L0.92 Total/NA13.2 200.8
Vanadium 5.0 ug/L2.0 Total/NA12.0 J 200.8
Chloride 4.0 mg/L3.4 Total/NA20939056A
Sulfate 4.0 mg/L1.9 Total/NA20269056A
Alkalinity 5.0 mg/L3.7 Total/NA1250SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1470SM 2540C
Client Sample ID: MW-9 Lab Sample ID: 500-126939-9
Arsenic
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA12.3 200.8
Barium 2.5 ug/L0.37 Total/NA1360200.8
Cobalt 1.0 ug/L0.27 Total/NA10.77 J 200.8
Copper 2.0 ug/L0.63 Total/NA10.72 J 200.8
Lead 0.50 ug/L0.16 Total/NA10.23 J 200.8
Nickel 2.0 ug/L0.92 Total/NA12.0 200.8
Vanadium 5.0 ug/L2.0 Total/NA12.0 J 200.8
Chloride 20 mg/L17 Total/NA1005009056A
Sulfate 2.0 mg/L0.95 Total/NA10439056A
Alkalinity 5.0 mg/L3.7 Total/NA1250SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1210SM 2540C
Client Sample ID: MW-10 Lab Sample ID: 500-126939-10
Arsenic
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA11.5 200.8
Barium 2.5 ug/L0.37 Total/NA11400200.8
Copper 2.0 ug/L0.63 Total/NA10.90 J 200.8
Chloride 200 mg/L170 Total/NA100023009056A
Sulfate 1.0 mg/L0.48 Total/NA523 F1 9056A
Alkalinity 5.0 mg/L3.7 Total/NA1560SM 2320B
Total Dissolved Solids 17 mg/L7.2 Total/NA14900SM 2540C
Client Sample ID: MW-11 Lab Sample ID: 500-126939-11
Arsenic
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA11.4 200.8
Barium 2.5 ug/L0.37 Total/NA1420200.8
TestAmerica Chicago
This Detection Summary does not include radiochemical test results.
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Detection Summary
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Client Sample ID: MW-11 (Continued)Lab Sample ID: 500-126939-11
Beryllium
RL
1.0 ug/L
MDL
0.43
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.78 200.8
Cadmium 0.50 ug/L0.15 Total/NA10.72 200.8
Cobalt 1.0 ug/L0.27 Total/NA111200.8
Copper 2.0 ug/L0.63 Total/NA10.72 J 200.8
Lead 0.50 ug/L0.16 Total/NA11.9 200.8
Nickel 2.0 ug/L0.92 Total/NA12.6 200.8
Selenium 2.5 ug/L1.1 Total/NA12.0 J 200.8
Zinc 20 ug/L8.1 Total/NA112 J 200.8
Chloride 10 mg/L8.5 Total/NA501709056A
Sulfate 4.0 mg/L1.9 Total/NA2026 F1 9056A
Alkalinity 5.0 mg/L3.7 Total/NA174SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1690SM 2540C
Client Sample ID: SW-1 Lab Sample ID: 500-126939-12
Toluene
RL
0.50 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA10.95 8260B
Arsenic 1.0 ug/L0.15 Total/NA10.61 J 200.8
Barium 2.5 ug/L0.37 Total/NA148200.8
Cobalt 1.0 ug/L0.27 Total/NA10.58 J 200.8
Copper 2.0 ug/L0.63 Total/NA10.95 J 200.8
Lead 0.50 ug/L0.16 Total/NA10.38 J 200.8
Chloride 1.0 mg/L0.85 Total/NA5289056A
Sulfate 0.40 mg/L0.19 Total/NA24.0 9056A
Alkalinity 5.0 mg/L3.7 Total/NA127SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA184SM 2540C
Client Sample ID: SW-2 Lab Sample ID: 500-126939-13
Arsenic
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.51 200.8
Barium 2.5 ug/L0.37 Total/NA147200.8
Cobalt 1.0 ug/L0.27 Total/NA10.43 J 200.8
Copper 2.0 ug/L0.63 Total/NA11.2 J 200.8
Lead 0.50 ug/L0.16 Total/NA10.26 J 200.8
Chloride 1.0 mg/L0.85 Total/NA5199056A
Sulfate 0.40 mg/L0.19 Total/NA25.8 9056A
Alkalinity 5.0 mg/L3.7 Total/NA136SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA190SM 2540C
Client Sample ID: SW-3 Lab Sample ID: 500-126939-14
Arsenic
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA11.6 200.8
Barium 2.5 ug/L0.37 Total/NA1240200.8
Cobalt 1.0 ug/L0.27 Total/NA14.4 200.8
Copper 2.0 ug/L0.63 Total/NA15.8 200.8
Lead 0.50 ug/L0.16 Total/NA11.2 200.8
Nickel 2.0 ug/L0.92 Total/NA11.9 J 200.8
Vanadium 5.0 ug/L2.0 Total/NA12.7 J 200.8
TestAmerica Chicago
This Detection Summary does not include radiochemical test results.
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Detection Summary
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Client Sample ID: SW-3 (Continued)Lab Sample ID: 500-126939-14
Zinc
RL
20 ug/L
MDL
8.1
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1140200.8
Chloride 10 mg/L8.5 Total/NA50569056A
Sulfate 4.0 mg/L1.9 Total/NA20519056A
Alkalinity 5.0 mg/L3.7 Total/NA197SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1370SM 2540C
Client Sample ID: SW-4 Lab Sample ID: 500-126939-15
Arsenic
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA11.8 200.8
Barium 2.5 ug/L0.37 Total/NA173200.8
Cobalt 1.0 ug/L0.27 Total/NA11.1 200.8
Copper 2.0 ug/L0.63 Total/NA116200.8
Lead 0.50 ug/L0.16 Total/NA10.21 J 200.8
Chloride 2.0 mg/L1.7 Total/NA10449056A
Sulfate 2.0 mg/L0.95 Total/NA10209056A
Alkalinity 5.0 mg/L3.7 Total/NA1120SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1280SM 2540C
Client Sample ID: Duplicate Lab Sample ID: 500-126939-16
Vinyl chloride
RL
0.50 ug/L
MDL
0.20
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA12.5 8260B
TestAmerica Chicago
This Detection Summary does not include radiochemical test results.
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Method Summary
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL CHI
EPA200.8 Metals (ICP/MS)TAL CHI
EPA245.1 Mercury (CVAA)TAL CHI
SW8469056AAnions, Ion Chromatography TAL CHI
SMSM 2320B Alkalinity TAL CHI
SMSM 2540C Solids, Total Dissolved (TDS)TAL CHI
Protocol References:
EPA = US Environmental Protection Agency
SM = "Standard Methods For The Examination Of Water And Wastewater",
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL [phone]
TestAmerica Chicago
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Sample Summary
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
500-126939-1 MW-1 Water 04/19/17 18:25 04/21/17 08:50
500-126939-2 MW-2 Water 04/20/17 12:20 04/21/17 08:50
500-126939-3 MW-3 Water 04/20/17 13:00 04/21/17 08:50
500-126939-4 MW-4 Water 04/19/17 16:25 04/21/17 08:50
500-126939-5 MW-5 Water 04/19/17 15:25 04/21/17 08:50
500-126939-6 MW-6 Water 04/19/17 14:50 04/21/17 08:50
500-126939-7 MW-7 Water 04/19/17 14:10 04/21/17 08:50
500-126939-8 MW-8 Water 04/20/17 08:40 04/21/17 08:50
500-126939-9 MW-9 Water 04/19/17 13:30 04/21/17 08:50
500-126939-10 MW-10 Water 04/19/17 17:10 04/21/17 08:50
500-126939-11 MW-11 Water 04/19/17 17:55 04/21/17 08:50
500-126939-12 SW-1 Water 04/20/17 10:00 04/21/17 08:50
500-126939-13 SW-2 Water 04/20/17 10:30 04/21/17 08:50
500-126939-14 SW-3 Water 04/20/17 11:00 04/21/17 08:50
500-126939-15 SW-4 Water 04/20/17 10:35 04/21/17 08:50
500-126939-16 Duplicate Water 04/20/17 00:00 04/21/17 08:50
TestAmerica Chicago
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Client Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID: 500-126939-1Client Sample ID: MW-1
Matrix: WaterDate Collected: 04/19/17 18:25
Date Received: 04/21/17 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 05/01/17 01:42 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.38 ug/L 05/01/17 01:42 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 05/01/17 01:42 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 05/01/17 01:42 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 05/01/17 01:42 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 05/01/17 01:42 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 05/01/17 01:42 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 05/01/17 01:42 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 05/01/17 01:42 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 05/01/17 01:42 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 05/01/17 01:42 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 05/01/17 01:42 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 05/01/17 01:42 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 05/01/17 01:42 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 05/01/17 01:42 12-Hexanone <5.0
5.0 2.2 ug/L 05/01/17 01:42 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 05/01/17 01:42 1Acetone<5.0
20 4.5 ug/L 05/01/17 01:42 1Acrylonitrile<20
0.50 0.15 ug/L 05/01/17 01:42 1Benzene<0.50
1.0 0.43 ug/L 05/01/17 01:42 1Bromochloromethane<1.0
1.0 0.37 ug/L 05/01/17 01:42 1Bromodichloromethane<1.0
1.0 0.48 ug/L 05/01/17 01:42 1Bromoform<1.0
2.0 0.80 ug/L 05/01/17 01:42 1Bromomethane<2.0
2.0 0.45 ug/L 05/01/17 01:42 1Carbon disulfide <2.0
1.0 0.38 ug/L 05/01/17 01:42 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 05/01/17 01:42 1Chlorobenzene<1.0
1.0 0.51 ug/L 05/01/17 01:42 1Chloroethane<1.0
2.0 0.37 ug/L 05/01/17 01:42 1Chloroform<2.0
1.0 0.32 ug/L 05/01/17 01:42 1Chloromethane<1.0
1.0 0.41 ug/L 05/01/17 01:42 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 05/01/17 01:42 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 05/01/17 01:42 1Dibromochloromethane<1.0
1.0 0.27 ug/L 05/01/17 01:42 1Dibromomethane<1.0
0.50 0.18 ug/L 05/01/17 01:42 1Ethylbenzene<0.50
2.5 0.66 ug/L 05/01/17 01:42 1Iodomethane<2.5
5.0 1.6 ug/L 05/01/17 01:42 1Methylene Chloride <5.0
1.0 0.39 ug/L 05/01/17 01:42 1Styrene<1.0
1.0 0.37 ug/L 05/01/17 01:42 1Tetrachloroethene<1.0
10 1.9 ug/L 05/01/17 01:42 1Tetrahydrofuran<10
0.50 0.15 ug/L 05/01/17 01:42 1Toluene<0.50
1.0 0.35 ug/L 05/01/17 01:42 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 05/01/17 01:42 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 05/01/17 01:42 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 05/01/17 01:42 1Trichloroethene<0.50
1.0 0.43 ug/L 05/01/17 01:42 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 05/01/17 01:42 1Vinyl acetate <2.0
0.50 0.20 ug/L 05/01/17 01:42 1Vinyl chloride <0.50
1.0 0.22 ug/L 05/01/17 01:42 1Xylenes, Total <1.0
TestAmerica Chicago
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Client Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID: 500-126939-1Client Sample ID: MW-1
Matrix: WaterDate Collected: 04/19/17 18:25
Date Received: 04/21/17 08:50
Dibromofluoromethane 92 75-120 05/01/17 01:42 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr)92 05/01/17 01:42 175-126
4-Bromofluorobenzene (Surr)88 05/01/17 01:42 172-124
Toluene-d8 (Surr)93 05/01/17 01:42 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 04/24/17 10:35 04/24/17 18:23 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.15 ug/L 04/24/17 10:35 04/24/17 18:23 1Arsenic0.90 J
2.5 0.37 ug/L 04/24/17 10:35 04/24/17 18:23 1Barium1200
1.0 0.43 ug/L 04/24/17 10:35 04/24/17 18:23 1Beryllium<1.0
0.50 0.15 ug/L 04/24/17 10:35 04/24/17 18:23 1Cadmium<0.50
5.0 2.3 ug/L 04/24/17 10:35 04/24/17 18:23 1Chromium<5.0
1.0 0.27 ug/L 04/24/17 10:35 04/24/17 18:23 1Cobalt0.28 J
2.0 0.63 ug/L 04/24/17 10:35 04/24/17 18:23 1Copper1.1 J
0.50 0.16 ug/L 04/24/17 10:35 04/25/17 12:08 1Lead<0.50
2.0 0.92 ug/L 04/24/17 10:35 04/24/17 18:23 1Nickel<2.0
2.5 1.1 ug/L 04/24/17 10:35 04/24/17 18:23 1Selenium<2.5
0.50 0.078 ug/L 04/24/17 10:35 04/24/17 18:23 1Silver3.3
2.0 0.65 ug/L 04/24/17 10:35 04/25/17 12:08 1Thallium<2.0
5.0 2.0 ug/L 04/24/17 10:35 04/24/17 18:23 1Vanadium4.9 J
20 8.1 ug/L 04/24/17 10:35 04/24/17 18:23 1Zinc<20
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury 1.2 0.20 0.091 ug/L 04/22/17 16:00 04/23/17 09:26 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General Chemistry
RL MDL
Chloride 2700 200 170 mg/L 05/01/17 16:34 1000
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.40 0.19 mg/L 05/01/17 16:21 2Sulfate3.8
5.0 3.7 mg/L 04/25/17 13:43 1Alkalinity410
25 11 mg/L 04/24/17 04:38 1Total Dissolved Solids 5600
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Client Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID: 500-126939-2Client Sample ID: MW-2
Matrix: WaterDate Collected: 04/20/17 12:20
Date Received: 04/21/17 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 05/01/17 02:07 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.38 ug/L 05/01/17 02:07 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 05/01/17 02:07 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 05/01/17 02:07 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 05/01/17 02:07 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 05/01/17 02:07 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 05/01/17 02:07 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 05/01/17 02:07 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 05/01/17 02:07 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 05/01/17 02:07 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 05/01/17 02:07 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 05/01/17 02:07 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 05/01/17 02:07 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 05/01/17 02:07 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 05/01/17 02:07 12-Hexanone <5.0
5.0 2.2 ug/L 05/01/17 02:07 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 05/01/17 02:07 1Acetone<5.0
20 4.5 ug/L 05/01/17 02:07 1Acrylonitrile<20
0.50 0.15 ug/L 05/01/17 02:07 1Benzene<0.50
1.0 0.43 ug/L 05/01/17 02:07 1Bromochloromethane<1.0
1.0 0.37 ug/L 05/01/17 02:07 1Bromodichloromethane<1.0
1.0 0.48 ug/L 05/01/17 02:07 1Bromoform<1.0
2.0 0.80 ug/L 05/01/17 02:07 1Bromomethane<2.0
2.0 0.45 ug/L 05/01/17 02:07 1Carbon disulfide <2.0
1.0 0.38 ug/L 05/01/17 02:07 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 05/01/17 02:07 1Chlorobenzene<1.0
1.0 0.51 ug/L 05/01/17 02:07 1Chloroethane<1.0
2.0 0.37 ug/L 05/01/17 02:07 1Chloroform<2.0
1.0 0.32 ug/L 05/01/17 02:07 1Chloromethane<1.0
1.0 0.41 ug/L 05/01/17 02:07 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 05/01/17 02:07 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 05/01/17 02:07 1Dibromochloromethane<1.0
1.0 0.27 ug/L 05/01/17 02:07 1Dibromomethane<1.0
0.50 0.18 ug/L 05/01/17 02:07 1Ethylbenzene<0.50
2.5 0.66 ug/L 05/01/17 02:07 1Iodomethane<2.5
5.0 1.6 ug/L 05/01/17 02:07 1Methylene Chloride <5.0
1.0 0.39 ug/L 05/01/17 02:07 1Styrene<1.0
1.0 0.37 ug/L 05/01/17 02:07 1Tetrachloroethene<1.0
10 1.9 ug/L 05/01/17 02:07 1Tetrahydrofuran<10
0.50 0.15 ug/L 05/01/17 02:07 1Toluene<0.50
1.0 0.35 ug/L 05/01/17 02:07 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 05/01/17 02:07 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 05/01/17 02:07 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 05/01/17 02:07 1Trichloroethene<0.50
1.0 0.43 ug/L 05/01/17 02:07 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 05/01/17 02:07 1Vinyl acetate <2.0
0.50 0.20 ug/L 05/01/17 02:07 1Vinyl chloride <0.50
1.0 0.22 ug/L 05/01/17 02:07 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID: 500-126939-2Client Sample ID: MW-2
Matrix: WaterDate Collected: 04/20/17 12:20
Date Received: 04/21/17 08:50
Dibromofluoromethane 90 75-120 05/01/17 02:07 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr)93 05/01/17 02:07 175-126
4-Bromofluorobenzene (Surr)89 05/01/17 02:07 172-124
Toluene-d8 (Surr)92 05/01/17 02:07 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 04/24/17 10:35 04/24/17 18:27 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.15 ug/L 04/24/17 10:35 04/24/17 18:27 1Arsenic1.2
2.5 0.37 ug/L 04/24/17 10:35 04/24/17 18:27 1Barium74
1.0 0.43 ug/L 04/24/17 10:35 04/24/17 18:27 1Beryllium<1.0
0.50 0.15 ug/L 04/24/17 10:35 04/24/17 18:27 1Cadmium<0.50
5.0 2.3 ug/L 04/24/17 10:35 04/24/17 18:27 1Chromium<5.0
1.0 0.27 ug/L 04/24/17 10:35 04/24/17 18:27 1Cobalt0.59 J
2.0 0.63 ug/L 04/24/17 10:35 04/24/17 18:27 1Copper0.79 J
0.50 0.16 ug/L 04/24/17 10:35 04/25/17 12:11 1Lead0.51
2.0 0.92 ug/L 04/24/17 10:35 04/24/17 18:27 1Nickel2.8
2.5 1.1 ug/L 04/24/17 10:35 04/24/17 18:27 1Selenium<2.5
0.50 0.078 ug/L 04/24/17 10:35 04/24/17 18:27 1Silver<0.50
2.0 0.65 ug/L 04/24/17 10:35 04/25/17 12:11 1Thallium<2.0
5.0 2.0 ug/L 04/24/17 10:35 04/24/17 18:27 1Vanadium2.5 J
20 8.1 ug/L 04/24/17 10:35 04/24/17 18:27 1Zinc<20
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 04/22/17 16:00 04/23/17 09:38 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General Chemistry
RL MDL
Chloride 130 10 8.5 mg/L 05/01/17 15:18 50
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10 4.8 mg/L 05/01/17 15:18 50Sulfate87
5.0 3.7 mg/L 04/25/17 13:58 1Alkalinity160
10 4.3 mg/L 04/25/17 04:13 1Total Dissolved Solids 530
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Client Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID: 500-126939-3Client Sample ID: MW-3
Matrix: WaterDate Collected: 04/20/17 13:00
Date Received: 04/21/17 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 05/01/17 02:33 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.38 ug/L 05/01/17 02:33 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 05/01/17 02:33 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 05/01/17 02:33 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 05/01/17 02:33 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 05/01/17 02:33 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 05/01/17 02:33 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 05/01/17 02:33 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 05/01/17 02:33 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 05/01/17 02:33 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 05/01/17 02:33 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 05/01/17 02:33 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 05/01/17 02:33 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 05/01/17 02:33 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 05/01/17 02:33 12-Hexanone <5.0
5.0 2.2 ug/L 05/01/17 02:33 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 05/01/17 02:33 1Acetone<5.0
20 4.5 ug/L 05/01/17 02:33 1Acrylonitrile<20
0.50 0.15 ug/L 05/01/17 02:33 1Benzene<0.50
1.0 0.43 ug/L 05/01/17 02:33 1Bromochloromethane<1.0
1.0 0.37 ug/L 05/01/17 02:33 1Bromodichloromethane<1.0
1.0 0.48 ug/L 05/01/17 02:33 1Bromoform<1.0
2.0 0.80 ug/L 05/01/17 02:33 1Bromomethane<2.0
2.0 0.45 ug/L 05/01/17 02:33 1Carbon disulfide <2.0
1.0 0.38 ug/L 05/01/17 02:33 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 05/01/17 02:33 1Chlorobenzene<1.0
1.0 0.51 ug/L 05/01/17 02:33 1Chloroethane<1.0
2.0 0.37 ug/L 05/01/17 02:33 1Chloroform<2.0
1.0 0.32 ug/L 05/01/17 02:33 1Chloromethane<1.0
1.0 0.41 ug/L 05/01/17 02:33 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 05/01/17 02:33 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 05/01/17 02:33 1Dibromochloromethane<1.0
1.0 0.27 ug/L 05/01/17 02:33 1Dibromomethane<1.0
0.50 0.18 ug/L 05/01/17 02:33 1Ethylbenzene<0.50
2.5 0.66 ug/L 05/01/17 02:33 1Iodomethane<2.5
5.0 1.6 ug/L 05/01/17 02:33 1Methylene Chloride <5.0
1.0 0.39 ug/L 05/01/17 02:33 1Styrene<1.0
1.0 0.37 ug/L 05/01/17 02:33 1Tetrachloroethene<1.0
10 1.9 ug/L 05/01/17 02:33 1Tetrahydrofuran<10
0.50 0.15 ug/L 05/01/17 02:33 1Toluene<0.50
1.0 0.35 ug/L 05/01/17 02:33 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 05/01/17 02:33 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 05/01/17 02:33 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 05/01/17 02:33 1Trichloroethene<0.50
1.0 0.43 ug/L 05/01/17 02:33 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 05/01/17 02:33 1Vinyl acetate <2.0
0.50 0.20 ug/L 05/01/17 02:33 1Vinyl chloride <0.50
1.0 0.22 ug/L 05/01/17 02:33 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID: 500-126939-3Client Sample ID: MW-3
Matrix: WaterDate Collected: 04/20/17 13:00
Date Received: 04/21/17 08:50
Dibromofluoromethane 92 75-120 05/01/17 02:33 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr)97 05/01/17 02:33 175-126
4-Bromofluorobenzene (Surr)90 05/01/17 02:33 172-124
Toluene-d8 (Surr)93 05/01/17 02:33 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 04/24/17 10:35 04/24/17 18:49 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.15 ug/L 04/24/17 10:35 04/24/17 18:49 1Arsenic1.6
2.5 0.37 ug/L 04/24/17 10:35 04/24/17 18:49 1Barium230
1.0 0.43 ug/L 04/24/17 10:35 04/24/17 18:49 1Beryllium<1.0
0.50 0.15 ug/L 04/24/17 10:35 04/24/17 18:49 1Cadmium<0.50
5.0 2.3 ug/L 04/24/17 10:35 04/24/17 18:49 1Chromium<5.0
1.0 0.27 ug/L 04/24/17 10:35 04/24/17 18:49 1Cobalt21
2.0 0.63 ug/L 04/24/17 10:35 04/24/17 18:49 1Copper0.81 J
0.50 0.16 ug/L 04/24/17 10:35 04/25/17 12:34 1Lead0.55
2.0 0.92 ug/L 04/24/17 10:35 04/24/17 18:49 1Nickel2.1
2.5 1.1 ug/L 04/24/17 10:35 04/24/17 18:49 1Selenium<2.5
0.50 0.078 ug/L 04/24/17 10:35 04/24/17 18:49 1Silver<0.50
2.0 0.65 ug/L 04/24/17 10:35 04/25/17 12:34 1Thallium<2.0
5.0 2.0 ug/L 04/24/17 10:35 04/24/17 18:49 1Vanadium<5.0
20 8.1 ug/L 04/24/17 10:35 04/24/17 18:49 1Zinc<20
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 04/22/17 16:00 04/23/17 09:40 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General Chemistry
RL MDL
Chloride 530 20 17 mg/L 05/01/17 15:56 100
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
20 9.5 mg/L 05/01/17 15:56 100Sulfate140
5.0 3.7 mg/L 04/25/17 14:06 1Alkalinity470
10 4.3 mg/L 04/25/17 04:18 1Total Dissolved Solids 1600
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Client Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID: 500-126939-4Client Sample ID: MW-4
Matrix: WaterDate Collected: 04/19/17 16:25
Date Received: 04/21/17 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 05/01/17 02:58 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.38 ug/L 05/01/17 02:58 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 05/01/17 02:58 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 05/01/17 02:58 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 05/01/17 02:58 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 05/01/17 02:58 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 05/01/17 02:58 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 05/01/17 02:58 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 05/01/17 02:58 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 05/01/17 02:58 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 05/01/17 02:58 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 05/01/17 02:58 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 05/01/17 02:58 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 05/01/17 02:58 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 05/01/17 02:58 12-Hexanone <5.0
5.0 2.2 ug/L 05/01/17 02:58 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 05/01/17 02:58 1Acetone5.9
20 4.5 ug/L 05/01/17 02:58 1Acrylonitrile<20
0.50 0.15 ug/L 05/01/17 02:58 1Benzene<0.50
1.0 0.43 ug/L 05/01/17 02:58 1Bromochloromethane<1.0
1.0 0.37 ug/L 05/01/17 02:58 1Bromodichloromethane<1.0
1.0 0.48 ug/L 05/01/17 02:58 1Bromoform<1.0
2.0 0.80 ug/L 05/01/17 02:58 1Bromomethane<2.0
2.0 0.45 ug/L 05/01/17 02:58 1Carbon disulfide <2.0
1.0 0.38 ug/L 05/01/17 02:58 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 05/01/17 02:58 1Chlorobenzene<1.0
1.0 0.51 ug/L 05/01/17 02:58 1Chloroethane<1.0
2.0 0.37 ug/L 05/01/17 02:58 1Chloroform<2.0
1.0 0.32 ug/L 05/01/17 02:58 1Chloromethane<1.0
1.0 0.41 ug/L 05/01/17 02:58 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 05/01/17 02:58 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 05/01/17 02:58 1Dibromochloromethane<1.0
1.0 0.27 ug/L 05/01/17 02:58 1Dibromomethane<1.0
0.50 0.18 ug/L 05/01/17 02:58 1Ethylbenzene<0.50
2.5 0.66 ug/L 05/01/17 02:58 1Iodomethane<2.5
5.0 1.6 ug/L 05/01/17 02:58 1Methylene Chloride <5.0
1.0 0.39 ug/L 05/01/17 02:58 1Styrene<1.0
1.0 0.37 ug/L 05/01/17 02:58 1Tetrachloroethene<1.0
10 1.9 ug/L 05/01/17 02:58 1Tetrahydrofuran6.5 J
0.50 0.15 ug/L 05/01/17 02:58 1Toluene<0.50
1.0 0.35 ug/L 05/01/17 02:58 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 05/01/17 02:58 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 05/01/17 02:58 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 05/01/17 02:58 1Trichloroethene<0.50
1.0 0.43 ug/L 05/01/17 02:58 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 05/01/17 02:58 1Vinyl acetate <2.0
0.50 0.20 ug/L 05/01/17 02:58 1Vinyl chloride <0.50
1.0 0.22 ug/L 05/01/17 02:58 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID: 500-126939-4Client Sample ID: MW-4
Matrix: WaterDate Collected: 04/19/17 16:25
Date Received: 04/21/17 08:50
Dibromofluoromethane 92 75-120 05/01/17 02:58 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr)94 05/01/17 02:58 175-126
4-Bromofluorobenzene (Surr)91 05/01/17 02:58 172-124
Toluene-d8 (Surr)94 05/01/17 02:58 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 04/24/17 10:35 04/24/17 18:53 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.15 ug/L 04/24/17 10:35 04/24/17 18:53 1Arsenic4.4
2.5 0.37 ug/L 04/24/17 10:35 04/24/17 18:53 1Barium130
1.0 0.43 ug/L 04/24/17 10:35 04/24/17 18:53 1Beryllium<1.0
0.50 0.15 ug/L 04/24/17 10:35 04/24/17 18:53 1Cadmium<0.50
5.0 2.3 ug/L 04/24/17 10:35 04/24/17 18:53 1Chromium6.6
1.0 0.27 ug/L 04/24/17 10:35 04/24/17 18:53 1Cobalt10
2.0 0.63 ug/L 04/24/17 10:35 04/24/17 18:53 1Copper<2.0
0.50 0.16 ug/L 04/24/17 10:35 04/25/17 12:38 1Lead0.17 J
2.0 0.92 ug/L 04/24/17 10:35 04/24/17 18:53 1Nickel8.0
2.5 1.1 ug/L 04/24/17 10:35 04/24/17 18:53 1Selenium<2.5
0.50 0.078 ug/L 04/24/17 10:35 04/24/17 18:53 1Silver<0.50
2.0 0.65 ug/L 04/24/17 10:35 04/25/17 12:38 1Thallium<2.0
5.0 2.0 ug/L 04/24/17 10:35 04/24/17 18:53 1Vanadium<5.0
20 8.1 ug/L 04/24/17 10:35 04/24/17 18:53 1Zinc<20
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 04/22/17 16:00 04/23/17 09:41 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General Chemistry
RL MDL
Chloride 100 10 8.5 mg/L 05/01/17 16:08 50
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
10 4.8 mg/L 05/01/17 16:08 50Sulfate75
5.0 3.7 mg/L 04/25/17 13:19 1Alkalinity690
10 4.3 mg/L 04/25/17 04:21 1Total Dissolved Solids 1100
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Client Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID: 500-126939-5Client Sample ID: MW-5
Matrix: WaterDate Collected: 04/19/17 15:25
Date Received: 04/21/17 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 05/01/17 03:23 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.38 ug/L 05/01/17 03:23 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 05/01/17 03:23 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 05/01/17 03:23 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 05/01/17 03:23 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 05/01/17 03:23 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 05/01/17 03:23 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 05/01/17 03:23 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 05/01/17 03:23 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 05/01/17 03:23 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 05/01/17 03:23 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 05/01/17 03:23 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 05/01/17 03:23 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 05/01/17 03:23 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 05/01/17 03:23 12-Hexanone <5.0
5.0 2.2 ug/L 05/01/17 03:23 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 05/01/17 03:23 1Acetone<5.0
20 4.5 ug/L 05/01/17 03:23 1Acrylonitrile<20
0.50 0.15 ug/L 05/01/17 03:23 1Benzene<0.50
1.0 0.43 ug/L 05/01/17 03:23 1Bromochloromethane<1.0
1.0 0.37 ug/L 05/01/17 03:23 1Bromodichloromethane<1.0
1.0 0.48 ug/L 05/01/17 03:23 1Bromoform<1.0
2.0 0.80 ug/L 05/01/17 03:23 1Bromomethane<2.0
2.0 0.45 ug/L 05/01/17 03:23 1Carbon disulfide <2.0
1.0 0.38 ug/L 05/01/17 03:23 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 05/01/17 03:23 1Chlorobenzene<1.0
1.0 0.51 ug/L 05/01/17 03:23 1Chloroethane<1.0
2.0 0.37 ug/L 05/01/17 03:23 1Chloroform<2.0
1.0 0.32 ug/L 05/01/17 03:23 1Chloromethane<1.0
1.0 0.41 ug/L 05/01/17 03:23 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 05/01/17 03:23 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 05/01/17 03:23 1Dibromochloromethane<1.0
1.0 0.27 ug/L 05/01/17 03:23 1Dibromomethane<1.0
0.50 0.18 ug/L 05/01/17 03:23 1Ethylbenzene<0.50
2.5 0.66 ug/L 05/01/17 03:23 1Iodomethane<2.5
5.0 1.6 ug/L 05/01/17 03:23 1Methylene Chloride <5.0
1.0 0.39 ug/L 05/01/17 03:23 1Styrene<1.0
1.0 0.37 ug/L 05/01/17 03:23 1Tetrachloroethene<1.0
10 1.9 ug/L 05/01/17 03:23 1Tetrahydrofuran<10
0.50 0.15 ug/L 05/01/17 03:23 1Toluene<0.50
1.0 0.35 ug/L 05/01/17 03:23 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 05/01/17 03:23 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 05/01/17 03:23 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 05/01/17 03:23 1Trichloroethene<0.50
1.0 0.43 ug/L 05/01/17 03:23 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 05/01/17 03:23 1Vinyl acetate <2.0
0.50 0.20 ug/L 05/01/17 03:23 1Vinyl chloride <0.50
1.0 0.22 ug/L 05/01/17 03:23 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID: 500-126939-5Client Sample ID: MW-5
Matrix: WaterDate Collected: 04/19/17 15:25
Date Received: 04/21/17 08:50
Dibromofluoromethane 93 75-120 05/01/17 03:23 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr)94 05/01/17 03:23 175-126
4-Bromofluorobenzene (Surr)90 05/01/17 03:23 172-124
Toluene-d8 (Surr)91 05/01/17 03:23 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 04/24/17 10:35 04/24/17 18:57 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.15 ug/L 04/24/17 10:35 04/24/17 18:57 1Arsenic0.30 J
2.5 0.37 ug/L 04/24/17 10:35 04/24/17 18:57 1Barium82
1.0 0.43 ug/L 04/24/17 10:35 04/24/17 18:57 1Beryllium<1.0
0.50 0.15 ug/L 04/24/17 10:35 04/24/17 18:57 1Cadmium<0.50
5.0 2.3 ug/L 04/24/17 10:35 04/24/17 18:57 1Chromium<5.0
1.0 0.27 ug/L 04/24/17 10:35 04/24/17 18:57 1Cobalt10
2.0 0.63 ug/L 04/24/17 10:35 04/24/17 18:57 1Copper<2.0
0.50 0.16 ug/L 04/24/17 10:35 04/25/17 12:43 1Lead<0.50
2.0 0.92 ug/L 04/24/17 10:35 04/24/17 18:57 1Nickel1.3 J
2.5 1.1 ug/L 04/24/17 10:35 04/24/17 18:57 1Selenium<2.5
0.50 0.078 ug/L 04/24/17 10:35 04/24/17 18:57 1Silver<0.50
2.0 0.65 ug/L 04/24/17 10:35 04/25/17 12:43 1Thallium<2.0
5.0 2.0 ug/L 04/24/17 10:35 04/24/17 18:57 1Vanadium<5.0
20 8.1 ug/L 04/24/17 10:35 04/24/17 18:57 1Zinc<20
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 04/22/17 16:00 04/23/17 09:42 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General Chemistry
RL MDL
Chloride 16 1.0 0.85 mg/L 05/02/17 14:07 5
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.48 mg/L 05/02/17 14:07 5Sulfate34
5.0 3.7 mg/L 04/25/17 14:12 1Alkalinity99
10 4.3 mg/L 04/25/17 04:23 1Total Dissolved Solids 200
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Client Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID: 500-126939-6Client Sample ID: MW-6
Matrix: WaterDate Collected: 04/19/17 14:50
Date Received: 04/21/17 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 05/01/17 03:48 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.38 ug/L 05/01/17 03:48 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 05/01/17 03:48 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 05/01/17 03:48 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 05/01/17 03:48 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 05/01/17 03:48 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 05/01/17 03:48 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 05/01/17 03:48 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 05/01/17 03:48 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 05/01/17 03:48 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 05/01/17 03:48 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 05/01/17 03:48 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 05/01/17 03:48 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 05/01/17 03:48 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 05/01/17 03:48 12-Hexanone <5.0
5.0 2.2 ug/L 05/01/17 03:48 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 05/01/17 03:48 1Acetone<5.0
20 4.5 ug/L 05/01/17 03:48 1Acrylonitrile<20
0.50 0.15 ug/L 05/01/17 03:48 1Benzene<0.50
1.0 0.43 ug/L 05/01/17 03:48 1Bromochloromethane<1.0
1.0 0.37 ug/L 05/01/17 03:48 1Bromodichloromethane<1.0
1.0 0.48 ug/L 05/01/17 03:48 1Bromoform<1.0
2.0 0.80 ug/L 05/01/17 03:48 1Bromomethane<2.0
2.0 0.45 ug/L 05/01/17 03:48 1Carbon disulfide <2.0
1.0 0.38 ug/L 05/01/17 03:48 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 05/01/17 03:48 1Chlorobenzene<1.0
1.0 0.51 ug/L 05/01/17 03:48 1Chloroethane<1.0
2.0 0.37 ug/L 05/01/17 03:48 1Chloroform<2.0
1.0 0.32 ug/L 05/01/17 03:48 1Chloromethane<1.0
1.0 0.41 ug/L 05/01/17 03:48 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 05/01/17 03:48 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 05/01/17 03:48 1Dibromochloromethane<1.0
1.0 0.27 ug/L 05/01/17 03:48 1Dibromomethane<1.0
0.50 0.18 ug/L 05/01/17 03:48 1Ethylbenzene<0.50
2.5 0.66 ug/L 05/01/17 03:48 1Iodomethane<2.5
5.0 1.6 ug/L 05/01/17 03:48 1Methylene Chloride <5.0
1.0 0.39 ug/L 05/01/17 03:48 1Styrene<1.0
1.0 0.37 ug/L 05/01/17 03:48 1Tetrachloroethene<1.0
10 1.9 ug/L 05/01/17 03:48 1Tetrahydrofuran<10
0.50 0.15 ug/L 05/01/17 03:48 1Toluene<0.50
1.0 0.35 ug/L 05/01/17 03:48 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 05/01/17 03:48 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 05/01/17 03:48 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 05/01/17 03:48 1Trichloroethene<0.50
1.0 0.43 ug/L 05/01/17 03:48 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 05/01/17 03:48 1Vinyl acetate <2.0
0.50 0.20 ug/L 05/01/17 03:48 1Vinyl chloride <0.50
1.0 0.22 ug/L 05/01/17 03:48 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID: 500-126939-6Client Sample ID: MW-6
Matrix: WaterDate Collected: 04/19/17 14:50
Date Received: 04/21/17 08:50
Dibromofluoromethane 93 75-120 05/01/17 03:48 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr)94 05/01/17 03:48 175-126
4-Bromofluorobenzene (Surr)90 05/01/17 03:48 172-124
Toluene-d8 (Surr)92 05/01/17 03:48 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 04/24/17 10:35 04/24/17 19:01 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.15 ug/L 04/24/17 10:35 04/24/17 19:01 1Arsenic9.7
5.0 0.75 ug/L 04/24/17 10:35 04/25/17 12:50 2Barium270
1.0 0.43 ug/L 04/24/17 10:35 04/25/17 12:47 1Beryllium0.58 J
0.50 0.15 ug/L 04/24/17 10:35 04/24/17 19:01 1Cadmium0.36 J
5.0 2.3 ug/L 04/24/17 10:35 04/25/17 12:47 1Chromium3.8 J
1.0 0.27 ug/L 04/24/17 10:35 04/25/17 12:47 1Cobalt4.2
2.0 0.63 ug/L 04/24/17 10:35 04/24/17 19:01 1Copper8.9
1.0 0.31 ug/L 04/24/17 10:35 04/25/17 12:50 2Lead21
2.0 0.92 ug/L 04/24/17 10:35 04/25/17 12:47 1Nickel4.7
2.5 1.1 ug/L 04/24/17 10:35 04/24/17 19:01 1Selenium<2.5
0.50 0.078 ug/L 04/24/17 10:35 04/24/17 19:01 1Silver0.099 J
4.0 1.3 ug/L 04/24/17 10:35 04/25/17 12:50 2Thallium<4.0
5.0 2.0 ug/L 04/24/17 10:35 04/25/17 12:47 1Vanadium14
20 8.1 ug/L 04/24/17 10:35 04/24/17 19:01 1Zinc38 B
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 04/22/17 16:00 04/23/17 09:44 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General Chemistry
RL MDL
Chloride 36 2.0 1.7 mg/L 05/01/17 17:49 10
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.0 0.95 mg/L 05/01/17 17:49 10Sulfate17
5.0 3.7 mg/L 04/25/17 14:17 1Alkalinity11
10 4.3 mg/L 04/25/17 04:26 1Total Dissolved Solids 130
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Client Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID: 500-126939-7Client Sample ID: MW-7
Matrix: WaterDate Collected: 04/19/17 14:10
Date Received: 04/21/17 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 05/01/17 04:13 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.38 ug/L 05/01/17 04:13 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 05/01/17 04:13 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 05/01/17 04:13 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 05/01/17 04:13 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 05/01/17 04:13 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 05/01/17 04:13 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 05/01/17 04:13 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 05/01/17 04:13 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 05/01/17 04:13 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 05/01/17 04:13 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 05/01/17 04:13 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 05/01/17 04:13 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 05/01/17 04:13 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 05/01/17 04:13 12-Hexanone <5.0
5.0 2.2 ug/L 05/01/17 04:13 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 05/01/17 04:13 1Acetone<5.0
20 4.5 ug/L 05/01/17 04:13 1Acrylonitrile<20
0.50 0.15 ug/L 05/01/17 04:13 1Benzene<0.50
1.0 0.43 ug/L 05/01/17 04:13 1Bromochloromethane<1.0
1.0 0.37 ug/L 05/01/17 04:13 1Bromodichloromethane<1.0
1.0 0.48 ug/L 05/01/17 04:13 1Bromoform<1.0
2.0 0.80 ug/L 05/01/17 04:13 1Bromomethane<2.0
2.0 0.45 ug/L 05/01/17 04:13 1Carbon disulfide <2.0
1.0 0.38 ug/L 05/01/17 04:13 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 05/01/17 04:13 1Chlorobenzene<1.0
1.0 0.51 ug/L 05/01/17 04:13 1Chloroethane<1.0
2.0 0.37 ug/L 05/01/17 04:13 1Chloroform<2.0
1.0 0.32 ug/L 05/01/17 04:13 1Chloromethane<1.0
1.0 0.41 ug/L 05/01/17 04:13 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 05/01/17 04:13 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 05/01/17 04:13 1Dibromochloromethane<1.0
1.0 0.27 ug/L 05/01/17 04:13 1Dibromomethane<1.0
0.50 0.18 ug/L 05/01/17 04:13 1Ethylbenzene<0.50
2.5 0.66 ug/L 05/01/17 04:13 1Iodomethane<2.5
5.0 1.6 ug/L 05/01/17 04:13 1Methylene Chloride <5.0
1.0 0.39 ug/L 05/01/17 04:13 1Styrene<1.0
1.0 0.37 ug/L 05/01/17 04:13 1Tetrachloroethene<1.0
10 1.9 ug/L 05/01/17 04:13 1Tetrahydrofuran<10
0.50 0.15 ug/L 05/01/17 04:13 1Toluene<0.50
1.0 0.35 ug/L 05/01/17 04:13 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 05/01/17 04:13 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 05/01/17 04:13 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 05/01/17 04:13 1Trichloroethene<0.50
1.0 0.43 ug/L 05/01/17 04:13 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 05/01/17 04:13 1Vinyl acetate <2.0
0.50 0.20 ug/L 05/01/17 04:13 1Vinyl chloride <0.50
1.0 0.22 ug/L 05/01/17 04:13 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID: 500-126939-7Client Sample ID: MW-7
Matrix: WaterDate Collected: 04/19/17 14:10
Date Received: 04/21/17 08:50
Dibromofluoromethane 93 75-120 05/01/17 04:13 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr)94 05/01/17 04:13 175-126
4-Bromofluorobenzene (Surr)88 05/01/17 04:13 172-124
Toluene-d8 (Surr)91 05/01/17 04:13 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 04/24/17 10:35 04/24/17 19:04 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.15 ug/L 04/24/17 10:35 04/24/17 19:04 1Arsenic3.6
2.5 0.37 ug/L 04/24/17 10:35 04/24/17 19:04 1Barium61
1.0 0.43 ug/L 04/24/17 10:35 04/24/17 19:04 1Beryllium<1.0
0.50 0.15 ug/L 04/24/17 10:35 04/24/17 19:04 1Cadmium<0.50
5.0 2.3 ug/L 04/24/17 10:35 04/24/17 19:04 1Chromium<5.0
1.0 0.27 ug/L 04/24/17 10:35 04/24/17 19:04 1Cobalt1.3
2.0 0.63 ug/L 04/24/17 10:35 04/24/17 19:04 1Copper1.0 J
0.50 0.16 ug/L 04/24/17 10:35 04/25/17 12:58 1Lead0.41 J
2.0 0.92 ug/L 04/24/17 10:35 04/24/17 19:04 1Nickel1.2 J
2.5 1.1 ug/L 04/24/17 10:35 04/24/17 19:04 1Selenium<2.5
0.50 0.078 ug/L 04/24/17 10:35 04/24/17 19:04 1Silver<0.50
2.0 0.65 ug/L 04/24/17 10:35 04/25/17 12:58 1Thallium<2.0
5.0 2.0 ug/L 04/24/17 10:35 04/24/17 19:04 1Vanadium<5.0
20 8.1 ug/L 04/24/17 10:35 04/24/17 19:04 1Zinc<20
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 04/22/17 16:00 04/23/17 09:45 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General Chemistry
RL MDL
Chloride 42 2.0 1.7 mg/L 05/01/17 18:27 10
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.0 0.95 mg/L 05/01/17 18:27 10Sulfate74
5.0 3.7 mg/L 04/25/17 14:23 1Alkalinity170
10 4.3 mg/L 04/25/17 04:28 1Total Dissolved Solids 390
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Client Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID: 500-126939-8Client Sample ID: MW-8
Matrix: WaterDate Collected: 04/20/17 08:40
Date Received: 04/21/17 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 05/01/17 04:39 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.38 ug/L 05/01/17 04:39 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 05/01/17 04:39 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 05/01/17 04:39 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 05/01/17 04:39 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 05/01/17 04:39 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 05/01/17 04:39 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 05/01/17 04:39 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 05/01/17 04:39 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 05/01/17 04:39 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 05/01/17 04:39 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 05/01/17 04:39 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 05/01/17 04:39 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 05/01/17 04:39 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 05/01/17 04:39 12-Hexanone <5.0
5.0 2.2 ug/L 05/01/17 04:39 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 05/01/17 04:39 1Acetone<5.0
20 4.5 ug/L 05/01/17 04:39 1Acrylonitrile<20
0.50 0.15 ug/L 05/01/17 04:39 1Benzene<0.50
1.0 0.43 ug/L 05/01/17 04:39 1Bromochloromethane<1.0
1.0 0.37 ug/L 05/01/17 04:39 1Bromodichloromethane<1.0
1.0 0.48 ug/L 05/01/17 04:39 1Bromoform<1.0
2.0 0.80 ug/L 05/01/17 04:39 1Bromomethane<2.0
2.0 0.45 ug/L 05/01/17 04:39 1Carbon disulfide <2.0
1.0 0.38 ug/L 05/01/17 04:39 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 05/01/17 04:39 1Chlorobenzene<1.0
1.0 0.51 ug/L 05/01/17 04:39 1Chloroethane<1.0
2.0 0.37 ug/L 05/01/17 04:39 1Chloroform<2.0
1.0 0.32 ug/L 05/01/17 04:39 1Chloromethane<1.0
1.0 0.41 ug/L 05/01/17 04:39 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 05/01/17 04:39 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 05/01/17 04:39 1Dibromochloromethane<1.0
1.0 0.27 ug/L 05/01/17 04:39 1Dibromomethane<1.0
0.50 0.18 ug/L 05/01/17 04:39 1Ethylbenzene<0.50
2.5 0.66 ug/L 05/01/17 04:39 1Iodomethane<2.5
5.0 1.6 ug/L 05/01/17 04:39 1Methylene Chloride <5.0
1.0 0.39 ug/L 05/01/17 04:39 1Styrene<1.0
1.0 0.37 ug/L 05/01/17 04:39 1Tetrachloroethene<1.0
10 1.9 ug/L 05/01/17 04:39 1Tetrahydrofuran<10
0.50 0.15 ug/L 05/01/17 04:39 1Toluene<0.50
1.0 0.35 ug/L 05/01/17 04:39 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 05/01/17 04:39 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 05/01/17 04:39 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 05/01/17 04:39 1Trichloroethene<0.50
1.0 0.43 ug/L 05/01/17 04:39 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 05/01/17 04:39 1Vinyl acetate <2.0
0.50 0.20 ug/L 05/01/17 04:39 1Vinyl chloride 4.2
1.0 0.22 ug/L 05/01/17 04:39 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID: 500-126939-8Client Sample ID: MW-8
Matrix: WaterDate Collected: 04/20/17 08:40
Date Received: 04/21/17 08:50
Dibromofluoromethane 94 75-120 05/01/17 04:39 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr)97 05/01/17 04:39 175-126
4-Bromofluorobenzene (Surr)90 05/01/17 04:39 172-124
Toluene-d8 (Surr)93 05/01/17 04:39 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 04/24/17 10:35 04/24/17 19:08 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.15 ug/L 04/24/17 10:35 04/24/17 19:08 1Arsenic1.8
2.5 0.37 ug/L 04/24/17 10:35 04/24/17 19:08 1Barium70
1.0 0.43 ug/L 04/24/17 10:35 04/24/17 19:08 1Beryllium<1.0
0.50 0.15 ug/L 04/24/17 10:35 04/24/17 19:08 1Cadmium<0.50
5.0 2.3 ug/L 04/24/17 10:35 04/24/17 19:08 1Chromium<5.0
1.0 0.27 ug/L 04/24/17 10:35 04/24/17 19:08 1Cobalt1.8
2.0 0.63 ug/L 04/24/17 10:35 04/24/17 19:08 1Copper1.3 J
0.50 0.16 ug/L 04/24/17 10:35 04/25/17 13:02 1Lead0.54
2.0 0.92 ug/L 04/24/17 10:35 04/24/17 19:08 1Nickel3.2
2.5 1.1 ug/L 04/24/17 10:35 04/24/17 19:08 1Selenium<2.5
0.50 0.078 ug/L 04/24/17 10:35 04/24/17 19:08 1Silver<0.50
2.0 0.65 ug/L 04/24/17 10:35 04/25/17 13:02 1Thallium<2.0
5.0 2.0 ug/L 04/24/17 10:35 04/24/17 19:08 1Vanadium2.0 J
20 8.1 ug/L 04/24/17 10:35 04/24/17 19:08 1Zinc<20
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 04/22/17 16:00 04/23/17 09:47 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General Chemistry
RL MDL
Chloride 93 4.0 3.4 mg/L 05/01/17 18:40 20
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4.0 1.9 mg/L 05/01/17 18:40 20Sulfate26
5.0 3.7 mg/L 04/25/17 14:30 1Alkalinity250
10 4.3 mg/L 04/25/17 04:31 1Total Dissolved Solids 470
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Client Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID: 500-126939-9Client Sample ID: MW-9
Matrix: WaterDate Collected: 04/19/17 13:30
Date Received: 04/21/17 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 05/01/17 02:06 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.38 ug/L 05/01/17 02:06 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 05/01/17 02:06 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 05/01/17 02:06 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 05/01/17 02:06 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 05/01/17 02:06 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 05/01/17 02:06 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 05/01/17 02:06 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 05/01/17 02:06 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 05/01/17 02:06 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 05/01/17 02:06 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 05/01/17 02:06 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 05/01/17 02:06 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 05/01/17 02:06 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 05/01/17 02:06 12-Hexanone <5.0
5.0 2.2 ug/L 05/01/17 02:06 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 05/01/17 02:06 1Acetone<5.0
20 4.5 ug/L 05/01/17 02:06 1Acrylonitrile<20
0.50 0.15 ug/L 05/01/17 02:06 1Benzene<0.50
1.0 0.43 ug/L 05/01/17 02:06 1Bromochloromethane<1.0
1.0 0.37 ug/L 05/01/17 02:06 1Bromodichloromethane<1.0
1.0 0.48 ug/L 05/01/17 02:06 1Bromoform<1.0
2.0 0.80 ug/L 05/01/17 02:06 1Bromomethane<2.0
2.0 0.45 ug/L 05/01/17 02:06 1Carbon disulfide <2.0
1.0 0.38 ug/L 05/01/17 02:06 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 05/01/17 02:06 1Chlorobenzene<1.0
1.0 0.51 ug/L 05/01/17 02:06 1Chloroethane<1.0
2.0 0.37 ug/L 05/01/17 02:06 1Chloroform<2.0
1.0 0.32 ug/L 05/01/17 02:06 1Chloromethane<1.0
1.0 0.41 ug/L 05/01/17 02:06 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 05/01/17 02:06 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 05/01/17 02:06 1Dibromochloromethane<1.0
1.0 0.27 ug/L 05/01/17 02:06 1Dibromomethane<1.0
0.50 0.18 ug/L 05/01/17 02:06 1Ethylbenzene<0.50
2.5 0.66 ug/L 05/01/17 02:06 1Iodomethane<2.5
5.0 1.6 ug/L 05/01/17 02:06 1Methylene Chloride <5.0
1.0 0.39 ug/L 05/01/17 02:06 1Styrene<1.0
1.0 0.37 ug/L 05/01/17 02:06 1Tetrachloroethene<1.0
10 1.9 ug/L 05/01/17 02:06 1Tetrahydrofuran<10
0.50 0.15 ug/L 05/01/17 02:06 1Toluene<0.50
1.0 0.35 ug/L 05/01/17 02:06 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 05/01/17 02:06 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 05/01/17 02:06 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 05/01/17 02:06 1Trichloroethene<0.50
1.0 0.43 ug/L 05/01/17 02:06 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 05/01/17 02:06 1Vinyl acetate <2.0
0.50 0.20 ug/L 05/01/17 02:06 1Vinyl chloride <0.50
1.0 0.22 ug/L 05/01/17 02:06 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID: 500-126939-9Client Sample ID: MW-9
Matrix: WaterDate Collected: 04/19/17 13:30
Date Received: 04/21/17 08:50
Dibromofluoromethane 99 75-120 05/01/17 02:06 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr)102 05/01/17 02:06 175-126
4-Bromofluorobenzene (Surr)90 05/01/17 02:06 172-124
Toluene-d8 (Surr)97 05/01/17 02:06 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 04/25/17 10:50 04/25/17 15:46 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.15 ug/L 04/25/17 10:50 04/25/17 15:46 1Arsenic2.3
2.5 0.37 ug/L 04/25/17 10:50 04/25/17 15:46 1Barium360
1.0 0.43 ug/L 04/25/17 10:50 04/25/17 15:46 1Beryllium<1.0
0.50 0.15 ug/L 04/25/17 10:50 04/25/17 15:46 1Cadmium<0.50
5.0 2.3 ug/L 04/25/17 10:50 04/25/17 15:46 1Chromium<5.0
1.0 0.27 ug/L 04/25/17 10:50 04/25/17 15:46 1Cobalt0.77 J
2.0 0.63 ug/L 04/25/17 10:50 04/25/17 15:46 1Copper0.72 J
0.50 0.16 ug/L 04/25/17 10:50 04/25/17 15:46 1Lead0.23 J
2.0 0.92 ug/L 04/25/17 10:50 04/25/17 15:46 1Nickel2.0
2.5 1.1 ug/L 04/25/17 10:50 04/25/17 15:46 1Selenium<2.5
0.50 0.078 ug/L 04/25/17 10:50 04/25/17 15:46 1Silver<0.50
2.0 0.65 ug/L 04/25/17 10:50 04/25/17 15:46 1Thallium<2.0
5.0 2.0 ug/L 04/25/17 10:50 04/25/17 15:46 1Vanadium2.0 J
20 8.1 ug/L 04/25/17 10:50 04/25/17 15:46 1Zinc<20
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 04/22/17 16:00 04/23/17 09:48 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General Chemistry
RL MDL
Chloride 500 20 17 mg/L 05/01/17 17:11 100
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.0 0.95 mg/L 05/02/17 14:45 10Sulfate43
5.0 3.7 mg/L 04/25/17 14:37 1Alkalinity250
10 4.3 mg/L 04/25/17 04:34 1Total Dissolved Solids 210
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Client Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID: 500-126939-10Client Sample ID: MW-10
Matrix: WaterDate Collected: 04/19/17 17:10
Date Received: 04/21/17 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 05/01/17 02:35 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.38 ug/L 05/01/17 02:35 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 05/01/17 02:35 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 05/01/17 02:35 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 05/01/17 02:35 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 05/01/17 02:35 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 05/01/17 02:35 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 05/01/17 02:35 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 05/01/17 02:35 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 05/01/17 02:35 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 05/01/17 02:35 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 05/01/17 02:35 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 05/01/17 02:35 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 05/01/17 02:35 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 05/01/17 02:35 12-Hexanone <5.0
5.0 2.2 ug/L 05/01/17 02:35 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 05/01/17 02:35 1Acetone<5.0
20 4.5 ug/L 05/01/17 02:35 1Acrylonitrile<20
0.50 0.15 ug/L 05/01/17 02:35 1Benzene<0.50
1.0 0.43 ug/L 05/01/17 02:35 1Bromochloromethane<1.0
1.0 0.37 ug/L 05/01/17 02:35 1Bromodichloromethane<1.0
1.0 0.48 ug/L 05/01/17 02:35 1Bromoform<1.0
2.0 0.80 ug/L 05/01/17 02:35 1Bromomethane<2.0
2.0 0.45 ug/L 05/01/17 02:35 1Carbon disulfide <2.0
1.0 0.38 ug/L 05/01/17 02:35 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 05/01/17 02:35 1Chlorobenzene<1.0
1.0 0.51 ug/L 05/01/17 02:35 1Chloroethane<1.0
2.0 0.37 ug/L 05/01/17 02:35 1Chloroform<2.0
1.0 0.32 ug/L 05/01/17 02:35 1Chloromethane<1.0
1.0 0.41 ug/L 05/01/17 02:35 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 05/01/17 02:35 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 05/01/17 02:35 1Dibromochloromethane<1.0
1.0 0.27 ug/L 05/01/17 02:35 1Dibromomethane<1.0
0.50 0.18 ug/L 05/01/17 02:35 1Ethylbenzene<0.50
2.5 0.66 ug/L 05/01/17 02:35 1Iodomethane<2.5
5.0 1.6 ug/L 05/01/17 02:35 1Methylene Chloride <5.0
1.0 0.39 ug/L 05/01/17 02:35 1Styrene<1.0
1.0 0.37 ug/L 05/01/17 02:35 1Tetrachloroethene<1.0
10 1.9 ug/L 05/01/17 02:35 1Tetrahydrofuran<10
0.50 0.15 ug/L 05/01/17 02:35 1Toluene<0.50
1.0 0.35 ug/L 05/01/17 02:35 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 05/01/17 02:35 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 05/01/17 02:35 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 05/01/17 02:35 1Trichloroethene<0.50
1.0 0.43 ug/L 05/01/17 02:35 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 05/01/17 02:35 1Vinyl acetate <2.0
0.50 0.20 ug/L 05/01/17 02:35 1Vinyl chloride <0.50
1.0 0.22 ug/L 05/01/17 02:35 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID: 500-126939-10Client Sample ID: MW-10
Matrix: WaterDate Collected: 04/19/17 17:10
Date Received: 04/21/17 08:50
Dibromofluoromethane 97 75-120 05/01/17 02:35 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr)100 05/01/17 02:35 175-126
4-Bromofluorobenzene (Surr)90 05/01/17 02:35 172-124
Toluene-d8 (Surr)97 05/01/17 02:35 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 04/25/17 10:50 04/25/17 16:01 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.15 ug/L 04/25/17 10:50 04/25/17 16:01 1Arsenic1.5
2.5 0.37 ug/L 04/25/17 10:50 04/25/17 16:01 1Barium1400
1.0 0.43 ug/L 04/25/17 10:50 04/25/17 16:01 1Beryllium<1.0
0.50 0.15 ug/L 04/25/17 10:50 04/25/17 16:01 1Cadmium<0.50
5.0 2.3 ug/L 04/25/17 10:50 04/25/17 16:01 1Chromium<5.0
1.0 0.27 ug/L 04/25/17 10:50 04/25/17 16:01 1Cobalt<1.0
2.0 0.63 ug/L 04/25/17 10:50 04/25/17 16:01 1Copper0.90 J
0.50 0.16 ug/L 04/25/17 10:50 04/25/17 16:01 1Lead<0.50
2.0 0.92 ug/L 04/25/17 10:50 04/25/17 16:01 1Nickel<2.0
2.5 1.1 ug/L 04/25/17 10:50 04/25/17 16:01 1Selenium<2.5
0.50 0.078 ug/L 04/25/17 10:50 04/25/17 16:01 1Silver<0.50
2.0 0.65 ug/L 04/25/17 10:50 04/25/17 16:01 1Thallium<2.0
5.0 2.0 ug/L 04/25/17 10:50 04/25/17 16:01 1Vanadium<5.0
20 8.1 ug/L 04/25/17 10:50 04/25/17 16:01 1Zinc<20
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 04/22/17 16:00 04/23/17 09:50 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General Chemistry
RL MDL
Chloride 2300 200 170 mg/L 05/01/17 17:37 1000
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.48 mg/L 05/02/17 14:57 5Sulfate23 F1
5.0 3.7 mg/L 04/25/17 14:49 1Alkalinity560
17 7.2 mg/L 04/25/17 04:36 1Total Dissolved Solids 4900
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Client Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID: 500-126939-11Client Sample ID: MW-11
Matrix: WaterDate Collected: 04/19/17 17:55
Date Received: 04/21/17 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 05/01/17 03:04 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.38 ug/L 05/01/17 03:04 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 05/01/17 03:04 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 05/01/17 03:04 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 05/01/17 03:04 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 05/01/17 03:04 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 05/01/17 03:04 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 05/01/17 03:04 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 05/01/17 03:04 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 05/01/17 03:04 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 05/01/17 03:04 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 05/01/17 03:04 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 05/01/17 03:04 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 05/01/17 03:04 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 05/01/17 03:04 12-Hexanone <5.0
5.0 2.2 ug/L 05/01/17 03:04 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 05/01/17 03:04 1Acetone<5.0
20 4.5 ug/L 05/01/17 03:04 1Acrylonitrile<20
0.50 0.15 ug/L 05/01/17 03:04 1Benzene<0.50
1.0 0.43 ug/L 05/01/17 03:04 1Bromochloromethane<1.0
1.0 0.37 ug/L 05/01/17 03:04 1Bromodichloromethane<1.0
1.0 0.48 ug/L 05/01/17 03:04 1Bromoform<1.0
2.0 0.80 ug/L 05/01/17 03:04 1Bromomethane<2.0
2.0 0.45 ug/L 05/01/17 03:04 1Carbon disulfide <2.0
1.0 0.38 ug/L 05/01/17 03:04 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 05/01/17 03:04 1Chlorobenzene<1.0
1.0 0.51 ug/L 05/01/17 03:04 1Chloroethane<1.0
2.0 0.37 ug/L 05/01/17 03:04 1Chloroform<2.0
1.0 0.32 ug/L 05/01/17 03:04 1Chloromethane<1.0
1.0 0.41 ug/L 05/01/17 03:04 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 05/01/17 03:04 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 05/01/17 03:04 1Dibromochloromethane<1.0
1.0 0.27 ug/L 05/01/17 03:04 1Dibromomethane<1.0
0.50 0.18 ug/L 05/01/17 03:04 1Ethylbenzene<0.50
2.5 0.66 ug/L 05/01/17 03:04 1Iodomethane<2.5
5.0 1.6 ug/L 05/01/17 03:04 1Methylene Chloride <5.0
1.0 0.39 ug/L 05/01/17 03:04 1Styrene<1.0
1.0 0.37 ug/L 05/01/17 03:04 1Tetrachloroethene<1.0
10 1.9 ug/L 05/01/17 03:04 1Tetrahydrofuran<10
0.50 0.15 ug/L 05/01/17 03:04 1Toluene<0.50
1.0 0.35 ug/L 05/01/17 03:04 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 05/01/17 03:04 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 05/01/17 03:04 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 05/01/17 03:04 1Trichloroethene<0.50
1.0 0.43 ug/L 05/01/17 03:04 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 05/01/17 03:04 1Vinyl acetate <2.0
0.50 0.20 ug/L 05/01/17 03:04 1Vinyl chloride <0.50
1.0 0.22 ug/L 05/01/17 03:04 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID: 500-126939-11Client Sample ID: MW-11
Matrix: WaterDate Collected: 04/19/17 17:55
Date Received: 04/21/17 08:50
Dibromofluoromethane 99 75-120 05/01/17 03:04 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr)103 05/01/17 03:04 175-126
4-Bromofluorobenzene (Surr)89 05/01/17 03:04 172-124
Toluene-d8 (Surr)96 05/01/17 03:04 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 04/25/17 10:50 04/25/17 16:05 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.15 ug/L 04/25/17 10:50 04/25/17 16:05 1Arsenic1.4
2.5 0.37 ug/L 04/25/17 10:50 04/25/17 16:05 1Barium420
1.0 0.43 ug/L 04/25/17 10:50 04/25/17 16:05 1Beryllium0.78 J
0.50 0.15 ug/L 04/25/17 10:50 04/25/17 16:05 1Cadmium0.72
5.0 2.3 ug/L 04/25/17 10:50 04/25/17 16:05 1Chromium<5.0
1.0 0.27 ug/L 04/25/17 10:50 04/25/17 16:05 1Cobalt11
2.0 0.63 ug/L 04/25/17 10:50 04/25/17 16:05 1Copper0.72 J
0.50 0.16 ug/L 04/25/17 10:50 04/25/17 16:05 1Lead1.9
2.0 0.92 ug/L 04/25/17 10:50 04/25/17 16:05 1Nickel2.6
2.5 1.1 ug/L 04/25/17 10:50 04/25/17 16:05 1Selenium2.0 J
0.50 0.078 ug/L 04/25/17 10:50 04/25/17 16:05 1Silver<0.50
2.0 0.65 ug/L 04/25/17 10:50 04/25/17 16:05 1Thallium<2.0
5.0 2.0 ug/L 04/25/17 10:50 04/25/17 16:05 1Vanadium<5.0
20 8.1 ug/L 04/25/17 10:50 04/25/17 16:05 1Zinc12 J
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 04/22/17 16:00 04/23/17 09:51 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General Chemistry
RL MDL
Chloride 170 10 8.5 mg/L 05/02/17 15:09 50
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4.0 1.9 mg/L 05/01/17 18:53 20Sulfate26 F1
5.0 3.7 mg/L 04/25/17 14:55 1Alkalinity74
10 4.3 mg/L 04/25/17 04:39 1Total Dissolved Solids 690
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Client Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID: 500-126939-12Client Sample ID: SW-1
Matrix: WaterDate Collected: 04/20/17 10:00
Date Received: 04/21/17 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 05/01/17 03:33 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.38 ug/L 05/01/17 03:33 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 05/01/17 03:33 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 05/01/17 03:33 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 05/01/17 03:33 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 05/01/17 03:33 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 05/01/17 03:33 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 05/01/17 03:33 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 05/01/17 03:33 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 05/01/17 03:33 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 05/01/17 03:33 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 05/01/17 03:33 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 05/01/17 03:33 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 05/01/17 03:33 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 05/01/17 03:33 12-Hexanone <5.0
5.0 2.2 ug/L 05/01/17 03:33 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 05/01/17 03:33 1Acetone<5.0
20 4.5 ug/L 05/01/17 03:33 1Acrylonitrile<20
0.50 0.15 ug/L 05/01/17 03:33 1Benzene<0.50
1.0 0.43 ug/L 05/01/17 03:33 1Bromochloromethane<1.0
1.0 0.37 ug/L 05/01/17 03:33 1Bromodichloromethane<1.0
1.0 0.48 ug/L 05/01/17 03:33 1Bromoform<1.0
2.0 0.80 ug/L 05/01/17 03:33 1Bromomethane<2.0
2.0 0.45 ug/L 05/01/17 03:33 1Carbon disulfide <2.0
1.0 0.38 ug/L 05/01/17 03:33 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 05/01/17 03:33 1Chlorobenzene<1.0
1.0 0.51 ug/L 05/01/17 03:33 1Chloroethane<1.0
2.0 0.37 ug/L 05/01/17 03:33 1Chloroform<2.0
1.0 0.32 ug/L 05/01/17 03:33 1Chloromethane<1.0
1.0 0.41 ug/L 05/01/17 03:33 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 05/01/17 03:33 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 05/01/17 03:33 1Dibromochloromethane<1.0
1.0 0.27 ug/L 05/01/17 03:33 1Dibromomethane<1.0
0.50 0.18 ug/L 05/01/17 03:33 1Ethylbenzene<0.50
2.5 0.66 ug/L 05/01/17 03:33 1Iodomethane<2.5
5.0 1.6 ug/L 05/01/17 03:33 1Methylene Chloride <5.0
1.0 0.39 ug/L 05/01/17 03:33 1Styrene<1.0
1.0 0.37 ug/L 05/01/17 03:33 1Tetrachloroethene<1.0
10 1.9 ug/L 05/01/17 03:33 1Tetrahydrofuran<10
0.50 0.15 ug/L 05/01/17 03:33 1Toluene0.95
1.0 0.35 ug/L 05/01/17 03:33 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 05/01/17 03:33 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 05/01/17 03:33 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 05/01/17 03:33 1Trichloroethene<0.50
1.0 0.43 ug/L 05/01/17 03:33 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 05/01/17 03:33 1Vinyl acetate <2.0
0.50 0.20 ug/L 05/01/17 03:33 1Vinyl chloride <0.50
1.0 0.22 ug/L 05/01/17 03:33 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID: 500-126939-12Client Sample ID: SW-1
Matrix: WaterDate Collected: 04/20/17 10:00
Date Received: 04/21/17 08:50
Dibromofluoromethane 100 75-120 05/01/17 03:33 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr)103 05/01/17 03:33 175-126
4-Bromofluorobenzene (Surr)90 05/01/17 03:33 172-124
Toluene-d8 (Surr)98 05/01/17 03:33 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 04/25/17 10:50 04/25/17 16:16 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.15 ug/L 04/25/17 10:50 04/25/17 16:16 1Arsenic0.61 J
2.5 0.37 ug/L 04/25/17 10:50 04/25/17 16:16 1Barium48
1.0 0.43 ug/L 04/25/17 10:50 04/25/17 16:16 1Beryllium<1.0
0.50 0.15 ug/L 04/25/17 10:50 04/25/17 16:16 1Cadmium<0.50
5.0 2.3 ug/L 04/25/17 10:50 04/25/17 16:16 1Chromium<5.0
1.0 0.27 ug/L 04/25/17 10:50 04/25/17 16:16 1Cobalt0.58 J
2.0 0.63 ug/L 04/25/17 10:50 04/25/17 16:16 1Copper0.95 J
0.50 0.16 ug/L 04/25/17 10:50 04/25/17 16:16 1Lead0.38 J
2.0 0.92 ug/L 04/25/17 10:50 04/25/17 16:16 1Nickel<2.0
2.5 1.1 ug/L 04/25/17 10:50 04/25/17 16:16 1Selenium<2.5
0.50 0.078 ug/L 04/25/17 10:50 04/25/17 16:16 1Silver<0.50
2.0 0.65 ug/L 04/25/17 10:50 04/25/17 16:16 1Thallium<2.0
5.0 2.0 ug/L 04/25/17 10:50 04/25/17 16:16 1Vanadium<5.0
20 8.1 ug/L 04/25/17 10:50 04/25/17 16:16 1Zinc<20
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 04/22/17 16:00 04/23/17 09:56 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General Chemistry
RL MDL
Chloride 28 1.0 0.85 mg/L 05/02/17 15:22 5
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.40 0.19 mg/L 05/01/17 19:31 2Sulfate4.0
5.0 3.7 mg/L 04/25/17 15:00 1Alkalinity27
10 4.3 mg/L 04/25/17 04:42 1Total Dissolved Solids 84
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Client Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID: 500-126939-13Client Sample ID: SW-2
Matrix: WaterDate Collected: 04/20/17 10:30
Date Received: 04/21/17 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 05/01/17 04:03 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.38 ug/L 05/01/17 04:03 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 05/01/17 04:03 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 05/01/17 04:03 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 05/01/17 04:03 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 05/01/17 04:03 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 05/01/17 04:03 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 05/01/17 04:03 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 05/01/17 04:03 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 05/01/17 04:03 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 05/01/17 04:03 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 05/01/17 04:03 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 05/01/17 04:03 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 05/01/17 04:03 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 05/01/17 04:03 12-Hexanone <5.0
5.0 2.2 ug/L 05/01/17 04:03 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 05/01/17 04:03 1Acetone<5.0
20 4.5 ug/L 05/01/17 04:03 1Acrylonitrile<20
0.50 0.15 ug/L 05/01/17 04:03 1Benzene<0.50
1.0 0.43 ug/L 05/01/17 04:03 1Bromochloromethane<1.0
1.0 0.37 ug/L 05/01/17 04:03 1Bromodichloromethane<1.0
1.0 0.48 ug/L 05/01/17 04:03 1Bromoform<1.0
2.0 0.80 ug/L 05/01/17 04:03 1Bromomethane<2.0
2.0 0.45 ug/L 05/01/17 04:03 1Carbon disulfide <2.0
1.0 0.38 ug/L 05/01/17 04:03 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 05/01/17 04:03 1Chlorobenzene<1.0
1.0 0.51 ug/L 05/01/17 04:03 1Chloroethane<1.0
2.0 0.37 ug/L 05/01/17 04:03 1Chloroform<2.0
1.0 0.32 ug/L 05/01/17 04:03 1Chloromethane<1.0
1.0 0.41 ug/L 05/01/17 04:03 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 05/01/17 04:03 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 05/01/17 04:03 1Dibromochloromethane<1.0
1.0 0.27 ug/L 05/01/17 04:03 1Dibromomethane<1.0
0.50 0.18 ug/L 05/01/17 04:03 1Ethylbenzene<0.50
2.5 0.66 ug/L 05/01/17 04:03 1Iodomethane<2.5
5.0 1.6 ug/L 05/01/17 04:03 1Methylene Chloride <5.0
1.0 0.39 ug/L 05/01/17 04:03 1Styrene<1.0
1.0 0.37 ug/L 05/01/17 04:03 1Tetrachloroethene<1.0
10 1.9 ug/L 05/01/17 04:03 1Tetrahydrofuran<10
0.50 0.15 ug/L 05/01/17 04:03 1Toluene<0.50
1.0 0.35 ug/L 05/01/17 04:03 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 05/01/17 04:03 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 05/01/17 04:03 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 05/01/17 04:03 1Trichloroethene<0.50
1.0 0.43 ug/L 05/01/17 04:03 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 05/01/17 04:03 1Vinyl acetate <2.0
0.50 0.20 ug/L 05/01/17 04:03 1Vinyl chloride <0.50
1.0 0.22 ug/L 05/01/17 04:03 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID: 500-126939-13Client Sample ID: SW-2
Matrix: WaterDate Collected: 04/20/17 10:30
Date Received: 04/21/17 08:50
Dibromofluoromethane 99 75-120 05/01/17 04:03 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr)101 05/01/17 04:03 175-126
4-Bromofluorobenzene (Surr)91 05/01/17 04:03 172-124
Toluene-d8 (Surr)97 05/01/17 04:03 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 04/25/17 10:50 04/25/17 16:31 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.15 ug/L 04/25/17 10:50 04/25/17 16:31 1Arsenic0.51 J
2.5 0.37 ug/L 04/25/17 10:50 04/25/17 16:31 1Barium47
1.0 0.43 ug/L 04/25/17 10:50 04/25/17 16:31 1Beryllium<1.0
0.50 0.15 ug/L 04/25/17 10:50 04/25/17 16:31 1Cadmium<0.50
5.0 2.3 ug/L 04/25/17 10:50 04/25/17 16:31 1Chromium<5.0
1.0 0.27 ug/L 04/25/17 10:50 04/25/17 16:31 1Cobalt0.43 J
2.0 0.63 ug/L 04/25/17 10:50 04/25/17 16:31 1Copper1.2 J
0.50 0.16 ug/L 04/25/17 10:50 04/25/17 16:31 1Lead0.26 J
2.0 0.92 ug/L 04/25/17 10:50 04/25/17 16:31 1Nickel<2.0
2.5 1.1 ug/L 04/25/17 10:50 04/25/17 16:31 1Selenium<2.5
0.50 0.078 ug/L 04/25/17 10:50 04/25/17 16:31 1Silver<0.50
2.0 0.65 ug/L 04/25/17 10:50 04/25/17 16:31 1Thallium<2.0
5.0 2.0 ug/L 04/25/17 10:50 04/25/17 16:31 1Vanadium<5.0
20 8.1 ug/L 04/25/17 10:50 04/25/17 16:31 1Zinc<20
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 04/22/17 16:00 04/23/17 09:58 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General Chemistry
RL MDL
Chloride 19 1.0 0.85 mg/L 05/02/17 15:34 5
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.40 0.19 mg/L 05/01/17 19:44 2Sulfate5.8
5.0 3.7 mg/L 04/25/17 15:06 1Alkalinity36
10 4.3 mg/L 04/25/17 04:44 1Total Dissolved Solids 90
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Client Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID: 500-126939-14Client Sample ID: SW-3
Matrix: WaterDate Collected: 04/20/17 11:00
Date Received: 04/21/17 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 05/01/17 04:32 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.38 ug/L 05/01/17 04:32 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 05/01/17 04:32 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 05/01/17 04:32 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 05/01/17 04:32 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 05/01/17 04:32 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 05/01/17 04:32 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 05/01/17 04:32 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 05/01/17 04:32 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 05/01/17 04:32 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 05/01/17 04:32 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 05/01/17 04:32 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 05/01/17 04:32 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 05/01/17 04:32 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 05/01/17 04:32 12-Hexanone <5.0
5.0 2.2 ug/L 05/01/17 04:32 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 05/01/17 04:32 1Acetone<5.0
20 4.5 ug/L 05/01/17 04:32 1Acrylonitrile<20
0.50 0.15 ug/L 05/01/17 04:32 1Benzene<0.50
1.0 0.43 ug/L 05/01/17 04:32 1Bromochloromethane<1.0
1.0 0.37 ug/L 05/01/17 04:32 1Bromodichloromethane<1.0
1.0 0.48 ug/L 05/01/17 04:32 1Bromoform<1.0
2.0 0.80 ug/L 05/01/17 04:32 1Bromomethane<2.0
2.0 0.45 ug/L 05/01/17 04:32 1Carbon disulfide <2.0
1.0 0.38 ug/L 05/01/17 04:32 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 05/01/17 04:32 1Chlorobenzene<1.0
1.0 0.51 ug/L 05/01/17 04:32 1Chloroethane<1.0
2.0 0.37 ug/L 05/01/17 04:32 1Chloroform<2.0
1.0 0.32 ug/L 05/01/17 04:32 1Chloromethane<1.0
1.0 0.41 ug/L 05/01/17 04:32 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 05/01/17 04:32 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 05/01/17 04:32 1Dibromochloromethane<1.0
1.0 0.27 ug/L 05/01/17 04:32 1Dibromomethane<1.0
0.50 0.18 ug/L 05/01/17 04:32 1Ethylbenzene<0.50
2.5 0.66 ug/L 05/01/17 04:32 1Iodomethane<2.5
5.0 1.6 ug/L 05/01/17 04:32 1Methylene Chloride <5.0
1.0 0.39 ug/L 05/01/17 04:32 1Styrene<1.0
1.0 0.37 ug/L 05/01/17 04:32 1Tetrachloroethene<1.0
10 1.9 ug/L 05/01/17 04:32 1Tetrahydrofuran<10
0.50 0.15 ug/L 05/01/17 04:32 1Toluene<0.50
1.0 0.35 ug/L 05/01/17 04:32 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 05/01/17 04:32 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 05/01/17 04:32 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 05/01/17 04:32 1Trichloroethene<0.50
1.0 0.43 ug/L 05/01/17 04:32 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 05/01/17 04:32 1Vinyl acetate <2.0
0.50 0.20 ug/L 05/01/17 04:32 1Vinyl chloride <0.50
1.0 0.22 ug/L 05/01/17 04:32 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID: 500-126939-14Client Sample ID: SW-3
Matrix: WaterDate Collected: 04/20/17 11:00
Date Received: 04/21/17 08:50
Dibromofluoromethane 101 75-120 05/01/17 04:32 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr)103 05/01/17 04:32 175-126
4-Bromofluorobenzene (Surr)91 05/01/17 04:32 172-124
Toluene-d8 (Surr)97 05/01/17 04:32 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 04/25/17 10:50 04/25/17 16:35 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.15 ug/L 04/25/17 10:50 04/25/17 16:35 1Arsenic1.6
2.5 0.37 ug/L 04/25/17 10:50 04/25/17 16:35 1Barium240
1.0 0.43 ug/L 04/25/17 10:50 04/25/17 16:35 1Beryllium<1.0
0.50 0.15 ug/L 04/25/17 10:50 04/25/17 16:35 1Cadmium<0.50
5.0 2.3 ug/L 04/25/17 10:50 04/25/17 16:35 1Chromium<5.0
1.0 0.27 ug/L 04/25/17 10:50 04/25/17 16:35 1Cobalt4.4
2.0 0.63 ug/L 04/25/17 10:50 04/25/17 16:35 1Copper5.8
0.50 0.16 ug/L 04/25/17 10:50 04/25/17 16:35 1Lead1.2
2.0 0.92 ug/L 04/25/17 10:50 04/25/17 16:35 1Nickel1.9 J
2.5 1.1 ug/L 04/25/17 10:50 04/25/17 16:35 1Selenium<2.5
0.50 0.078 ug/L 04/25/17 10:50 04/25/17 16:35 1Silver<0.50
2.0 0.65 ug/L 04/25/17 10:50 04/25/17 16:35 1Thallium<2.0
5.0 2.0 ug/L 04/25/17 10:50 04/25/17 16:35 1Vanadium2.7 J
20 8.1 ug/L 04/25/17 10:50 04/25/17 16:35 1Zinc140
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 04/22/17 16:00 04/23/17 09:59 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General Chemistry
RL MDL
Chloride 56 10 8.5 mg/L 05/01/17 19:56 50
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4.0 1.9 mg/L 05/03/17 15:35 20Sulfate51
5.0 3.7 mg/L 04/25/17 13:25 1Alkalinity97
10 4.3 mg/L 04/25/17 04:47 1Total Dissolved Solids 370
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Client Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID: 500-126939-15Client Sample ID: SW-4
Matrix: WaterDate Collected: 04/20/17 10:35
Date Received: 04/21/17 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 05/01/17 00:47 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.38 ug/L 05/01/17 00:47 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 05/01/17 00:47 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 05/01/17 00:47 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 05/01/17 00:47 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 05/01/17 00:47 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 05/01/17 00:47 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 05/01/17 00:47 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 05/01/17 00:47 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 05/01/17 00:47 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 05/01/17 00:47 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 05/01/17 00:47 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 05/01/17 00:47 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 05/01/17 00:47 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 05/01/17 00:47 12-Hexanone <5.0
5.0 2.2 ug/L 05/01/17 00:47 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 05/01/17 00:47 1Acetone<5.0
20 4.5 ug/L 05/01/17 00:47 1Acrylonitrile<20
0.50 0.15 ug/L 05/01/17 00:47 1Benzene<0.50
1.0 0.43 ug/L 05/01/17 00:47 1Bromochloromethane<1.0
1.0 0.37 ug/L 05/01/17 00:47 1Bromodichloromethane<1.0
1.0 0.48 ug/L 05/01/17 00:47 1Bromoform<1.0
2.0 0.80 ug/L 05/01/17 00:47 1Bromomethane<2.0
2.0 0.45 ug/L 05/01/17 00:47 1Carbon disulfide <2.0
1.0 0.38 ug/L 05/01/17 00:47 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 05/01/17 00:47 1Chlorobenzene<1.0
1.0 0.51 ug/L 05/01/17 00:47 1Chloroethane<1.0
2.0 0.37 ug/L 05/01/17 00:47 1Chloroform<2.0
1.0 0.32 ug/L 05/01/17 00:47 1Chloromethane<1.0
1.0 0.41 ug/L 05/01/17 00:47 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 05/01/17 00:47 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 05/01/17 00:47 1Dibromochloromethane<1.0
1.0 0.27 ug/L 05/01/17 00:47 1Dibromomethane<1.0
0.50 0.18 ug/L 05/01/17 00:47 1Ethylbenzene<0.50
2.5 0.66 ug/L 05/01/17 00:47 1Iodomethane<2.5
5.0 1.6 ug/L 05/01/17 00:47 1Methylene Chloride <5.0
1.0 0.39 ug/L 05/01/17 00:47 1Styrene<1.0
1.0 0.37 ug/L 05/01/17 00:47 1Tetrachloroethene<1.0
10 1.9 ug/L 05/01/17 00:47 1Tetrahydrofuran<10
0.50 0.15 ug/L 05/01/17 00:47 1Toluene<0.50
1.0 0.35 ug/L 05/01/17 00:47 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 05/01/17 00:47 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 05/01/17 00:47 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 05/01/17 00:47 1Trichloroethene<0.50
1.0 0.43 ug/L 05/01/17 00:47 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 05/01/17 00:47 1Vinyl acetate <2.0
0.50 0.20 ug/L 05/01/17 00:47 1Vinyl chloride <0.50
1.0 0.22 ug/L 05/01/17 00:47 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID: 500-126939-15Client Sample ID: SW-4
Matrix: WaterDate Collected: 04/20/17 10:35
Date Received: 04/21/17 08:50
Dibromofluoromethane 92 75-120 05/01/17 00:47 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr)105 05/01/17 00:47 175-126
4-Bromofluorobenzene (Surr)113 05/01/17 00:47 172-124
Toluene-d8 (Surr)100 05/01/17 00:47 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 04/25/17 10:50 04/25/17 16:39 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.15 ug/L 04/25/17 10:50 04/25/17 16:39 1Arsenic1.8
2.5 0.37 ug/L 04/25/17 10:50 04/25/17 16:39 1Barium73
1.0 0.43 ug/L 04/25/17 10:50 04/25/17 16:39 1Beryllium<1.0
0.50 0.15 ug/L 04/25/17 10:50 04/25/17 16:39 1Cadmium<0.50
5.0 2.3 ug/L 04/25/17 10:50 04/25/17 16:39 1Chromium<5.0
1.0 0.27 ug/L 04/25/17 10:50 04/25/17 16:39 1Cobalt1.1
2.0 0.63 ug/L 04/25/17 10:50 04/25/17 16:39 1Copper16
0.50 0.16 ug/L 04/25/17 10:50 04/25/17 16:39 1Lead0.21 J
2.0 0.92 ug/L 04/25/17 10:50 04/25/17 16:39 1Nickel<2.0
2.5 1.1 ug/L 04/25/17 10:50 04/25/17 16:39 1Selenium<2.5
0.50 0.078 ug/L 04/25/17 10:50 04/25/17 16:39 1Silver<0.50
2.0 0.65 ug/L 04/25/17 10:50 04/25/17 16:39 1Thallium<2.0
5.0 2.0 ug/L 04/25/17 10:50 04/25/17 16:39 1Vanadium<5.0
20 8.1 ug/L 04/25/17 10:50 04/25/17 16:39 1Zinc<20
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 04/22/17 16:00 04/23/17 10:00 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General Chemistry
RL MDL
Chloride 44 2.0 1.7 mg/L 05/02/17 15:58 10
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.0 0.95 mg/L 05/02/17 15:58 10Sulfate20
5.0 3.7 mg/L 04/25/17 13:35 1Alkalinity120
10 4.3 mg/L 04/25/17 04:49 1Total Dissolved Solids 280
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Client Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID: 500-126939-16Client Sample ID: Duplicate
Matrix: WaterDate Collected: 04/20/17 00:00
Date Received: 04/21/17 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 05/01/17 01:13 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.38 ug/L 05/01/17 01:13 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 05/01/17 01:13 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 05/01/17 01:13 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 05/01/17 01:13 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 05/01/17 01:13 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 05/01/17 01:13 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 05/01/17 01:13 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 05/01/17 01:13 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 05/01/17 01:13 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 05/01/17 01:13 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 05/01/17 01:13 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 05/01/17 01:13 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 05/01/17 01:13 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 05/01/17 01:13 12-Hexanone <5.0
5.0 2.2 ug/L 05/01/17 01:13 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 05/01/17 01:13 1Acetone<5.0
20 4.5 ug/L 05/01/17 01:13 1Acrylonitrile<20
0.50 0.15 ug/L 05/01/17 01:13 1Benzene<0.50
1.0 0.43 ug/L 05/01/17 01:13 1Bromochloromethane<1.0
1.0 0.37 ug/L 05/01/17 01:13 1Bromodichloromethane<1.0
1.0 0.48 ug/L 05/01/17 01:13 1Bromoform<1.0
2.0 0.80 ug/L 05/01/17 01:13 1Bromomethane<2.0
2.0 0.45 ug/L 05/01/17 01:13 1Carbon disulfide <2.0
1.0 0.38 ug/L 05/01/17 01:13 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 05/01/17 01:13 1Chlorobenzene<1.0
1.0 0.51 ug/L 05/01/17 01:13 1Chloroethane<1.0
2.0 0.37 ug/L 05/01/17 01:13 1Chloroform<2.0
1.0 0.32 ug/L 05/01/17 01:13 1Chloromethane<1.0
1.0 0.41 ug/L 05/01/17 01:13 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 05/01/17 01:13 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 05/01/17 01:13 1Dibromochloromethane<1.0
1.0 0.27 ug/L 05/01/17 01:13 1Dibromomethane<1.0
0.50 0.18 ug/L 05/01/17 01:13 1Ethylbenzene<0.50
2.5 0.66 ug/L 05/01/17 01:13 1Iodomethane<2.5
5.0 1.6 ug/L 05/01/17 01:13 1Methylene Chloride <5.0
1.0 0.39 ug/L 05/01/17 01:13 1Styrene<1.0
1.0 0.37 ug/L 05/01/17 01:13 1Tetrachloroethene<1.0
10 1.9 ug/L 05/01/17 01:13 1Tetrahydrofuran<10
0.50 0.15 ug/L 05/01/17 01:13 1Toluene<0.50
1.0 0.35 ug/L 05/01/17 01:13 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 05/01/17 01:13 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 05/01/17 01:13 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 05/01/17 01:13 1Trichloroethene<0.50
1.0 0.43 ug/L 05/01/17 01:13 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 05/01/17 01:13 1Vinyl acetate <2.0
0.50 0.20 ug/L 05/01/17 01:13 1Vinyl chloride 2.5
1.0 0.22 ug/L 05/01/17 01:13 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Lab Sample ID: 500-126939-16Client Sample ID: Duplicate
Matrix: WaterDate Collected: 04/20/17 00:00
Date Received: 04/21/17 08:50
Dibromofluoromethane 90 75-120 05/01/17 01:13 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
1,2-Dichloroethane-d4 (Surr)104 05/01/17 01:13 175-126
4-Bromofluorobenzene (Surr)110 05/01/17 01:13 172-124
Toluene-d8 (Surr)103 05/01/17 01:13 175-120
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Definitions/Glossary
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Qualifiers
GC/MS VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
Metals
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
F5 Duplicate RPD exceeds limit, and one or both sample results are less than 5 times RL. The data are considered valid because the
absolute difference is less than the RL.
B Compound was found in the blank and sample.
General Chemistry
Qualifier Description
F1 MS and/or MSD Recovery is outside acceptance limits.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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QC Association Summary
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
GC/MS VOA
Analysis Batch: 382992
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B500-126939-1 MW-1 Total/NA
Water 8260B500-126939-2 MW-2 Total/NA
Water 8260B500-126939-3 MW-3 Total/NA
Water 8260B500-126939-4 MW-4 Total/NA
Water 8260B500-126939-5 MW-5 Total/NA
Water 8260B500-126939-6 MW-6 Total/NA
Water 8260B500-126939-7 MW-7 Total/NA
Water 8260B500-126939-8 MW-8 Total/NA
Water 8260BMB 500-382992/6 Method Blank Total/NA
Water 8260BLCS 500-382992/4 Lab Control Sample Total/NA
Analysis Batch: 382996
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B500-126939-15 SW-4 Total/NA
Water 8260B500-126939-16 Duplicate Total/NA
Water 8260BMB 500-382996/6 Method Blank Total/NA
Water 8260BLCS 500-382996/4 Lab Control Sample Total/NA
Analysis Batch: 382998
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B500-126939-9 MW-9 Total/NA
Water 8260B500-126939-10 MW-10 Total/NA
Water 8260B500-126939-11 MW-11 Total/NA
Water 8260B500-126939-12 SW-1 Total/NA
Water 8260B500-126939-13 SW-2 Total/NA
Water 8260B500-126939-14 SW-3 Total/NA
Water 8260BMB 500-382998/6 Method Blank Total/NA
Water 8260BLCS 500-382998/4 Lab Control Sample Total/NA
Water 8260B500-126939-14 MS SW-3 Total/NA
Water 8260B500-126939-14 MSD SW-3 Total/NA
Metals
Prep Batch: 381673
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 245.1500-126939-1 MW-1 Total/NA
Water 245.1500-126939-2 MW-2 Total/NA
Water 245.1500-126939-3 MW-3 Total/NA
Water 245.1500-126939-4 MW-4 Total/NA
Water 245.1500-126939-5 MW-5 Total/NA
Water 245.1500-126939-6 MW-6 Total/NA
Water 245.1500-126939-7 MW-7 Total/NA
Water 245.1500-126939-8 MW-8 Total/NA
Water 245.1500-126939-9 MW-9 Total/NA
Water 245.1500-126939-10 MW-10 Total/NA
Water 245.1500-126939-11 MW-11 Total/NA
Water 245.1500-126939-12 SW-1 Total/NA
Water 245.1500-126939-13 SW-2 Total/NA
Water 245.1500-126939-14 SW-3 Total/NA
Water 245.1500-126939-15 SW-4 Total/NA
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QC Association Summary
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Metals (Continued)
Prep Batch: 381673 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 245.1MB 500-381673/12-A Method Blank Total/NA
Water 245.1LCS 500-381673/13-A Lab Control Sample Total/NA
Water 245.1500-126939-15 MS SW-4 Total/NA
Water 245.1500-126939-15 DU SW-4 Total/NA
Analysis Batch: 381786
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 245.1 381673500-126939-1 MW-1 Total/NA
Water 245.1 381673500-126939-2 MW-2 Total/NA
Water 245.1 381673500-126939-3 MW-3 Total/NA
Water 245.1 381673500-126939-4 MW-4 Total/NA
Water 245.1 381673500-126939-5 MW-5 Total/NA
Water 245.1 381673500-126939-6 MW-6 Total/NA
Water 245.1 381673500-126939-7 MW-7 Total/NA
Water 245.1 381673500-126939-8 MW-8 Total/NA
Water 245.1 381673500-126939-9 MW-9 Total/NA
Water 245.1 381673500-126939-10 MW-10 Total/NA
Water 245.1 381673500-126939-11 MW-11 Total/NA
Water 245.1 381673500-126939-12 SW-1 Total/NA
Water 245.1 381673500-126939-13 SW-2 Total/NA
Water 245.1 381673500-126939-14 SW-3 Total/NA
Water 245.1 381673500-126939-15 SW-4 Total/NA
Water 245.1 381673MB 500-381673/12-A Method Blank Total/NA
Water 245.1 381673LCS 500-381673/13-A Lab Control Sample Total/NA
Water 245.1 381673500-126939-15 MS SW-4 Total/NA
Water 245.1 381673500-126939-15 DU SW-4 Total/NA
Prep Batch: 381890
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 200.8500-126939-1 MW-1 Total/NA
Water 200.8500-126939-2 MW-2 Total/NA
Water 200.8500-126939-3 MW-3 Total/NA
Water 200.8500-126939-4 MW-4 Total/NA
Water 200.8500-126939-5 MW-5 Total/NA
Water 200.8500-126939-6 MW-6 Total/NA
Water 200.8500-126939-7 MW-7 Total/NA
Water 200.8500-126939-8 MW-8 Total/NA
Water 200.8MB 500-381890/1-A Method Blank Total/NA
Water 200.8LCS 500-381890/2-A Lab Control Sample Total/NA
Water 200.8500-126939-2 MS MW-2 Total/NA
Water 200.8500-126939-2 DU MW-2 Total/NA
Analysis Batch: 382074
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 200.8 381890500-126939-1 MW-1 Total/NA
Water 200.8 381890500-126939-2 MW-2 Total/NA
Water 200.8 381890500-126939-3 MW-3 Total/NA
Water 200.8 381890500-126939-4 MW-4 Total/NA
Water 200.8 381890500-126939-5 MW-5 Total/NA
Water 200.8 381890500-126939-6 MW-6 Total/NA
Water 200.8 381890500-126939-7 MW-7 Total/NA
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QC Association Summary
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Metals (Continued)
Analysis Batch: 382074 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 200.8 381890500-126939-8 MW-8 Total/NA
Water 200.8 381890MB 500-381890/1-A Method Blank Total/NA
Water 200.8 381890LCS 500-381890/2-A Lab Control Sample Total/NA
Water 200.8 381890500-126939-2 MS MW-2 Total/NA
Water 200.8 381890500-126939-2 DU MW-2 Total/NA
Prep Batch: 382108
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 200.8500-126939-9 MW-9 Total/NA
Water 200.8500-126939-10 MW-10 Total/NA
Water 200.8500-126939-11 MW-11 Total/NA
Water 200.8500-126939-12 SW-1 Total/NA
Water 200.8500-126939-13 SW-2 Total/NA
Water 200.8500-126939-14 SW-3 Total/NA
Water 200.8500-126939-15 SW-4 Total/NA
Water 200.8MB 500-382108/1-A Method Blank Total/NA
Water 200.8LCS 500-382108/2-A Lab Control Sample Total/NA
Water 200.8500-126939-9 MS MW-9 Total/NA
Water 200.8500-126939-12 MS SW-1 Total/NA
Water 200.8500-126939-9 DU MW-9 Total/NA
Water 200.8500-126939-12 DU SW-1 Total/NA
Analysis Batch: 382298
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 200.8 381890500-126939-1 MW-1 Total/NA
Water 200.8 381890500-126939-2 MW-2 Total/NA
Water 200.8 381890500-126939-3 MW-3 Total/NA
Water 200.8 381890500-126939-4 MW-4 Total/NA
Water 200.8 381890500-126939-5 MW-5 Total/NA
Water 200.8 381890500-126939-6 MW-6 Total/NA
Water 200.8 381890500-126939-6 MW-6 Total/NA
Water 200.8 381890500-126939-7 MW-7 Total/NA
Water 200.8 381890500-126939-8 MW-8 Total/NA
Water 200.8 382108500-126939-9 MW-9 Total/NA
Water 200.8 382108500-126939-10 MW-10 Total/NA
Water 200.8 382108500-126939-11 MW-11 Total/NA
Water 200.8 382108500-126939-12 SW-1 Total/NA
Water 200.8 382108500-126939-13 SW-2 Total/NA
Water 200.8 382108500-126939-14 SW-3 Total/NA
Water 200.8 382108500-126939-15 SW-4 Total/NA
Water 200.8 381890MB 500-381890/1-A Method Blank Total/NA
Water 200.8 382108MB 500-382108/1-A Method Blank Total/NA
Water 200.8 381890LCS 500-381890/2-A Lab Control Sample Total/NA
Water 200.8 382108LCS 500-382108/2-A Lab Control Sample Total/NA
Water 200.8 381890500-126939-2 MS MW-2 Total/NA
Water 200.8 382108500-126939-9 MS MW-9 Total/NA
Water 200.8 382108500-126939-12 MS SW-1 Total/NA
Water 200.8 381890500-126939-2 DU MW-2 Total/NA
Water 200.8 382108500-126939-9 DU MW-9 Total/NA
Water 200.8 382108500-126939-12 DU SW-1 Total/NA
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QC Association Summary
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
General Chemistry
Analysis Batch: 381824
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 2540C500-126939-1 MW-1 Total/NA
Water SM 2540CMB 500-381824/1 Method Blank Total/NA
Water SM 2540CLCS 500-381824/2 Lab Control Sample Total/NA
Analysis Batch: 382034
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 2540C500-126939-2 MW-2 Total/NA
Water SM 2540C500-126939-3 MW-3 Total/NA
Water SM 2540C500-126939-4 MW-4 Total/NA
Water SM 2540C500-126939-5 MW-5 Total/NA
Water SM 2540C500-126939-6 MW-6 Total/NA
Water SM 2540C500-126939-7 MW-7 Total/NA
Water SM 2540C500-126939-8 MW-8 Total/NA
Water SM 2540C500-126939-9 MW-9 Total/NA
Water SM 2540C500-126939-10 MW-10 Total/NA
Water SM 2540C500-126939-11 MW-11 Total/NA
Water SM 2540C500-126939-12 SW-1 Total/NA
Water SM 2540C500-126939-13 SW-2 Total/NA
Water SM 2540C500-126939-14 SW-3 Total/NA
Water SM 2540C500-126939-15 SW-4 Total/NA
Water SM 2540CMB 500-382034/1 Method Blank Total/NA
Water SM 2540CLCS 500-382034/2 Lab Control Sample Total/NA
Water SM 2540C500-126939-2 DU MW-2 Total/NA
Analysis Batch: 382285
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 2320B500-126939-1 MW-1 Total/NA
Water SM 2320B500-126939-2 MW-2 Total/NA
Water SM 2320B500-126939-3 MW-3 Total/NA
Water SM 2320B500-126939-4 MW-4 Total/NA
Water SM 2320B500-126939-5 MW-5 Total/NA
Water SM 2320B500-126939-6 MW-6 Total/NA
Water SM 2320B500-126939-7 MW-7 Total/NA
Water SM 2320B500-126939-8 MW-8 Total/NA
Water SM 2320B500-126939-9 MW-9 Total/NA
Water SM 2320B500-126939-10 MW-10 Total/NA
Water SM 2320B500-126939-11 MW-11 Total/NA
Water SM 2320B500-126939-12 SW-1 Total/NA
Water SM 2320B500-126939-13 SW-2 Total/NA
Water SM 2320B500-126939-14 SW-3 Total/NA
Water SM 2320B500-126939-15 SW-4 Total/NA
Water SM 2320BMB 500-382285/7 Method Blank Total/NA
Water SM 2320BLCS 500-382285/4 Lab Control Sample Total/NA
Water SM 2320B500-126939-1 DU MW-1 Total/NA
Analysis Batch: 383286
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 9056A500-126939-1 MW-1 Total/NA
Water 9056A500-126939-1 MW-1 Total/NA
Water 9056A500-126939-2 MW-2 Total/NA
Water 9056A500-126939-3 MW-3 Total/NA
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QC Association Summary
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
General Chemistry (Continued)
Analysis Batch: 383286 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 9056A500-126939-4 MW-4 Total/NA
Water 9056A500-126939-6 MW-6 Total/NA
Water 9056A500-126939-7 MW-7 Total/NA
Water 9056A500-126939-8 MW-8 Total/NA
Water 9056A500-126939-9 MW-9 Total/NA
Water 9056A500-126939-10 MW-10 Total/NA
Water 9056A500-126939-11 MW-11 Total/NA
Water 9056A500-126939-12 SW-1 Total/NA
Water 9056A500-126939-13 SW-2 Total/NA
Water 9056A500-126939-14 SW-3 Total/NA
Water 9056AMB 500-383286/39 Method Blank Total/NA
Water 9056ALCS 500-383286/3 Lab Control Sample Total/NA
Water 9056A500-126939-11 MS MW-11 Total/NA
Water 9056A500-126939-11 MSD MW-11 Total/NA
Analysis Batch: 383470
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 9056A500-126939-5 MW-5 Total/NA
Water 9056A500-126939-9 MW-9 Total/NA
Water 9056A500-126939-10 MW-10 Total/NA
Water 9056A500-126939-11 MW-11 Total/NA
Water 9056A500-126939-12 SW-1 Total/NA
Water 9056A500-126939-13 SW-2 Total/NA
Water 9056A500-126939-15 SW-4 Total/NA
Water 9056AMB 500-383470/7 Method Blank Total/NA
Water 9056ALCS 500-383470/8 Lab Control Sample Total/NA
Water 9056A500-126939-10 MS MW-10 Total/NA
Water 9056A500-126939-10 MSD MW-10 Total/NA
Analysis Batch: 383685
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 9056A500-126939-14 SW-3 Total/NA
Water 9056AMB 500-383685/4 Method Blank Total/NA
Water 9056ALCS 500-383685/5 Lab Control Sample Total/NA
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Surrogate Summary
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (75-120) (75-126) (72-124) (75-120)
DBFM 12DCE BFB TOL
92 92 88 93500-126939-1
Percent Surrogate Recovery (Acceptance Limits)
MW-1
90 93 89 92500-126939-2 MW-2
92 97 90 93500-126939-3 MW-3
92 94 91 94500-126939-4 MW-4
93 94 90 91500-126939-5 MW-5
93 94 90 92500-126939-6 MW-6
93 94 88 91500-126939-7 MW-7
94 97 90 93500-126939-8 MW-8
99 102 90 97500-126939-9 MW-9
97 100 90 97500-126939-10 MW-10
99 103 89 96500-126939-11 MW-11
100 103 90 98500-126939-12 SW-1
99 101 91 97500-126939-13 SW-2
101 103 91 97500-126939-14 SW-3
95 96 92 100500-126939-14 MS SW-3
97 96 92 100500-126939-14 MSD SW-3
92 105 113 100500-126939-15 SW-4
90 104 110 103500-126939-16 Duplicate
96 92 85 95LCS 500-382992/4 Lab Control Sample
92 100 104 99LCS 500-382996/4 Lab Control Sample
95 96 90 100LCS 500-382998/4 Lab Control Sample
93 93 90 93MB 500-382992/6 Method Blank
91 106 109 102MB 500-382996/6 Method Blank
99 102 89 96MB 500-382998/6 Method Blank
Surrogate Legend
DBFM = Dibromofluoromethane
12DCE = 1,2-Dichloroethane-d4 (Surr)
BFB = 4-Bromofluorobenzene (Surr)
TOL = Toluene-d8 (Surr)
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QC Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 500-382992/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382992
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 04/30/17 19:23 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<1.0 0.381.0 ug/L 04/30/17 19:23 11,1,1-Trichloroethane
<1.0 0.401.0 ug/L 04/30/17 19:23 11,1,2,2-Tetrachloroethane
<1.0 0.351.0 ug/L 04/30/17 19:23 11,1,2-Trichloroethane
<1.0 0.411.0 ug/L 04/30/17 19:23 11,1-Dichloroethane
<1.0 0.391.0 ug/L 04/30/17 19:23 11,1-Dichloroethene
<1.0 0.411.0 ug/L 04/30/17 19:23 11,2,3-Trichloropropane
<5.0 2.05.0 ug/L 04/30/17 19:23 11,2-Dibromo-3-Chloropropane
<1.0 0.391.0 ug/L 04/30/17 19:23 11,2-Dibromoethane
<1.0 0.331.0 ug/L 04/30/17 19:23 11,2-Dichlorobenzene
<1.0 0.391.0 ug/L 04/30/17 19:23 11,2-Dichloroethane
<1.0 0.431.0 ug/L 04/30/17 19:23 11,2-Dichloropropane
<1.0 0.361.0 ug/L 04/30/17 19:23 11,4-Dichlorobenzene
<5.0 2.15.0 ug/L 04/30/17 19:23 12-Butanone (MEK)
<5.0 1.65.0 ug/L 04/30/17 19:23 12-Hexanone
<5.0 2.25.0 ug/L 04/30/17 19:23 14-Methyl-2-pentanone (MIBK)
<5.0 1.75.0 ug/L 04/30/17 19:23 1Acetone
<20 4.520 ug/L 04/30/17 19:23 1Acrylonitrile
<0.50 0.150.50 ug/L 04/30/17 19:23 1Benzene
<1.0 0.431.0 ug/L 04/30/17 19:23 1Bromochloromethane
<1.0 0.371.0 ug/L 04/30/17 19:23 1Bromodichloromethane
<1.0 0.481.0 ug/L 04/30/17 19:23 1Bromoform
<2.0 0.802.0 ug/L 04/30/17 19:23 1Bromomethane
<2.0 0.452.0 ug/L 04/30/17 19:23 1Carbon disulfide
<1.0 0.381.0 ug/L 04/30/17 19:23 1Carbon tetrachloride
<1.0 0.391.0 ug/L 04/30/17 19:23 1Chlorobenzene
<1.0 0.511.0 ug/L 04/30/17 19:23 1Chloroethane
<2.0 0.372.0 ug/L 04/30/17 19:23 1Chloroform
<1.0 0.321.0 ug/L 04/30/17 19:23 1Chloromethane
<1.0 0.411.0 ug/L 04/30/17 19:23 1cis-1,2-Dichloroethene
<1.0 0.421.0 ug/L 04/30/17 19:23 1cis-1,3-Dichloropropene
<1.0 0.491.0 ug/L 04/30/17 19:23 1Dibromochloromethane
<1.0 0.271.0 ug/L 04/30/17 19:23 1Dibromomethane
<0.50 0.180.50 ug/L 04/30/17 19:23 1Ethylbenzene
<2.5 0.662.5 ug/L 04/30/17 19:23 1Iodomethane
<5.0 1.65.0 ug/L 04/30/17 19:23 1Methylene Chloride
<1.0 0.391.0 ug/L 04/30/17 19:23 1Styrene
<1.0 0.371.0 ug/L 04/30/17 19:23 1Tetrachloroethene
<10 1.910 ug/L 04/30/17 19:23 1Tetrahydrofuran
<0.50 0.150.50 ug/L 04/30/17 19:23 1Toluene
<1.0 0.351.0 ug/L 04/30/17 19:23 1trans-1,2-Dichloroethene
<1.0 0.361.0 ug/L 04/30/17 19:23 1trans-1,3-Dichloropropene
<5.0 1.25.0 ug/L 04/30/17 19:23 1trans-1,4-Dichloro-2-butene
<0.50 0.160.50 ug/L 04/30/17 19:23 1Trichloroethene
<1.0 0.431.0 ug/L 04/30/17 19:23 1Trichlorofluoromethane
<2.0 0.912.0 ug/L 04/30/17 19:23 1Vinyl acetate
<0.50 0.200.50 ug/L 04/30/17 19:23 1Vinyl chloride
<1.0 0.221.0 ug/L 04/30/17 19:23 1Xylenes, Total
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QC Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Dibromofluoromethane 93 75-120 04/30/17 19:23 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
93 04/30/17 19:23 11,2-Dichloroethane-d4 (Surr)75-126
90 04/30/17 19:23 14-Bromofluorobenzene (Surr)72-124
93 04/30/17 19:23 1Toluene-d8 (Surr)75-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-382992/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382992
1,1,1,2-Tetrachloroethane 50.0 44.4 ug/L 89 70-125
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
1,1,1-Trichloroethane 50.0 40.2 ug/L 80 70-125
1,1,2,2-Tetrachloroethane 50.0 38.4 ug/L 77 67-127
1,1,2-Trichloroethane 50.0 43.9 ug/L 88 70-122
1,1-Dichloroethane 50.0 47.1 ug/L 94 70-125
1,1-Dichloroethene 50.0 41.0 ug/L 82 67-122
1,2,3-Trichloropropane 50.0 34.7 ug/L 69 50-133
1,2-Dibromo-3-Chloropropane 50.0 32.0 ug/L 64 56-123
1,2-Dibromoethane 50.0 43.3 ug/L 87 70-125
1,2-Dichlorobenzene 50.0 44.7 ug/L 89 70-125
1,2-Dichloroethane 50.0 42.6 ug/L 85 68-127
1,2-Dichloropropane 50.0 49.4 ug/L 99 67-130
1,4-Dichlorobenzene 50.0 44.4 ug/L 89 70-120
2-Butanone (MEK)50.0 35.4 ug/L 71 53-141
2-Hexanone 50.0 32.3 ug/L 65 56-135
4-Methyl-2-pentanone (MIBK)50.0 31.6 ug/L 63 56-133
Acetone 50.0 34.7 ug/L 69 40-143
Acrylonitrile 500 499 ug/L 100 67-140
Benzene 50.0 41.8 ug/L 84 70-120
Bromochloromethane 50.0 45.5 ug/L 91 65-122
Bromodichloromethane 50.0 38.1 ug/L 76 69-120
Bromoform 50.0 39.6 ug/L 79 56-132
Bromomethane 50.0 44.0 ug/L 88 40-130
Carbon disulfide 50.0 37.8 ug/L 76 66-120
Carbon tetrachloride 50.0 40.4 ug/L 81 65-122
Chlorobenzene 50.0 44.6 ug/L 89 70-120
Chloroethane 50.0 35.8 ug/L 72 45-127
Chloroform 50.0 40.3 ug/L 81 70-120
Chloromethane 50.0 40.6 ug/L 81 54-147
cis-1,2-Dichloroethene 50.0 41.7 ug/L 83 70-125
cis-1,3-Dichloropropene 50.0 39.2 ug/L 78 64-127
Dibromochloromethane 50.0 40.2 ug/L 80 68-125
Dibromomethane 50.0 40.6 ug/L 81 70-120
Ethylbenzene 50.0 43.9 ug/L 88 70-120
Iodomethane 50.0 45.7 ug/L 91 61-136
Methylene Chloride 50.0 42.1 ug/L 84 69-125
Styrene 50.0 44.8 ug/L 90 70-120
Tetrachloroethene 50.0 47.4 ug/L 95 70-128
Tetrahydrofuran 100 76.5 ug/L 77 59-139
Toluene 50.0 44.3 ug/L 89 70-125
trans-1,2-Dichloroethene 50.0 42.1 ug/L 84 70-125
trans-1,3-Dichloropropene 50.0 36.9 ug/L 74 62-128
trans-1,4-Dichloro-2-butene 50.0 32.7 ug/L 65 60-130
Trichloroethene 50.0 47.6 ug/L 95 70-125
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QC Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-382992/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382992
Trichlorofluoromethane 50.0 41.6 ug/L 83 70-126
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Vinyl acetate 50.0 26.6 ug/L 53 43-133
Vinyl chloride 50.0 51.2 ug/L 102 64-126
Xylenes, Total 100 86.1 ug/L 86 70-125
Dibromofluoromethane 75 -120
Surrogate
96
LCS LCS
Qualifier Limits%Recovery
921,2-Dichloroethane-d4 (Surr)75 -126
854-Bromofluorobenzene (Surr)72 -124
95Toluene-d8 (Surr)75 -120
Client Sample ID: Method BlankLab Sample ID: MB 500-382996/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382996
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 04/30/17 19:34 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<1.0 0.381.0 ug/L 04/30/17 19:34 11,1,1-Trichloroethane
<1.0 0.401.0 ug/L 04/30/17 19:34 11,1,2,2-Tetrachloroethane
<1.0 0.351.0 ug/L 04/30/17 19:34 11,1,2-Trichloroethane
<1.0 0.411.0 ug/L 04/30/17 19:34 11,1-Dichloroethane
<1.0 0.391.0 ug/L 04/30/17 19:34 11,1-Dichloroethene
<1.0 0.411.0 ug/L 04/30/17 19:34 11,2,3-Trichloropropane
<5.0 2.05.0 ug/L 04/30/17 19:34 11,2-Dibromo-3-Chloropropane
<1.0 0.391.0 ug/L 04/30/17 19:34 11,2-Dibromoethane
<1.0 0.331.0 ug/L 04/30/17 19:34 11,2-Dichlorobenzene
<1.0 0.391.0 ug/L 04/30/17 19:34 11,2-Dichloroethane
<1.0 0.431.0 ug/L 04/30/17 19:34 11,2-Dichloropropane
<1.0 0.361.0 ug/L 04/30/17 19:34 11,4-Dichlorobenzene
<5.0 2.15.0 ug/L 04/30/17 19:34 12-Butanone (MEK)
<5.0 1.65.0 ug/L 04/30/17 19:34 12-Hexanone
<5.0 2.25.0 ug/L 04/30/17 19:34 14-Methyl-2-pentanone (MIBK)
<5.0 1.75.0 ug/L 04/30/17 19:34 1Acetone
<20 4.520 ug/L 04/30/17 19:34 1Acrylonitrile
<0.50 0.150.50 ug/L 04/30/17 19:34 1Benzene
<1.0 0.431.0 ug/L 04/30/17 19:34 1Bromochloromethane
<1.0 0.371.0 ug/L 04/30/17 19:34 1Bromodichloromethane
<1.0 0.481.0 ug/L 04/30/17 19:34 1Bromoform
<2.0 0.802.0 ug/L 04/30/17 19:34 1Bromomethane
<2.0 0.452.0 ug/L 04/30/17 19:34 1Carbon disulfide
<1.0 0.381.0 ug/L 04/30/17 19:34 1Carbon tetrachloride
<1.0 0.391.0 ug/L 04/30/17 19:34 1Chlorobenzene
<1.0 0.511.0 ug/L 04/30/17 19:34 1Chloroethane
<2.0 0.372.0 ug/L 04/30/17 19:34 1Chloroform
<1.0 0.321.0 ug/L 04/30/17 19:34 1Chloromethane
<1.0 0.411.0 ug/L 04/30/17 19:34 1cis-1,2-Dichloroethene
<1.0 0.421.0 ug/L 04/30/17 19:34 1cis-1,3-Dichloropropene
<1.0 0.491.0 ug/L 04/30/17 19:34 1Dibromochloromethane
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QC Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 500-382996/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382996
RL MDL
Dibromomethane <1.0 1.0 0.27 ug/L 04/30/17 19:34 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.50 0.180.50 ug/L 04/30/17 19:34 1Ethylbenzene
<2.5 0.662.5 ug/L 04/30/17 19:34 1Iodomethane
<5.0 1.65.0 ug/L 04/30/17 19:34 1Methylene Chloride
<1.0 0.391.0 ug/L 04/30/17 19:34 1Styrene
<1.0 0.371.0 ug/L 04/30/17 19:34 1Tetrachloroethene
<10 1.910 ug/L 04/30/17 19:34 1Tetrahydrofuran
<0.50 0.150.50 ug/L 04/30/17 19:34 1Toluene
<1.0 0.351.0 ug/L 04/30/17 19:34 1trans-1,2-Dichloroethene
<1.0 0.361.0 ug/L 04/30/17 19:34 1trans-1,3-Dichloropropene
<5.0 1.25.0 ug/L 04/30/17 19:34 1trans-1,4-Dichloro-2-butene
<0.50 0.160.50 ug/L 04/30/17 19:34 1Trichloroethene
<1.0 0.431.0 ug/L 04/30/17 19:34 1Trichlorofluoromethane
<2.0 0.912.0 ug/L 04/30/17 19:34 1Vinyl acetate
<0.50 0.200.50 ug/L 04/30/17 19:34 1Vinyl chloride
<1.0 0.221.0 ug/L 04/30/17 19:34 1Xylenes, Total
Dibromofluoromethane 91 75-120 04/30/17 19:34 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
106 04/30/17 19:34 11,2-Dichloroethane-d4 (Surr)75-126
109 04/30/17 19:34 14-Bromofluorobenzene (Surr)72-124
102 04/30/17 19:34 1Toluene-d8 (Surr)75-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-382996/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382996
1,1,1,2-Tetrachloroethane 50.0 46.3 ug/L 93 70-125
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
1,1,1-Trichloroethane 50.0 46.0 ug/L 92 70-125
1,1,2,2-Tetrachloroethane 50.0 45.0 ug/L 90 67-127
1,1,2-Trichloroethane 50.0 47.5 ug/L 95 70-122
1,1-Dichloroethane 50.0 46.8 ug/L 94 70-125
1,1-Dichloroethene 50.0 42.6 ug/L 85 67-122
1,2,3-Trichloropropane 50.0 42.2 ug/L 84 50-133
1,2-Dibromo-3-Chloropropane 50.0 40.4 ug/L 81 56-123
1,2-Dibromoethane 50.0 44.1 ug/L 88 70-125
1,2-Dichlorobenzene 50.0 47.5 ug/L 95 70-125
1,2-Dichloroethane 50.0 49.3 ug/L 99 68-127
1,2-Dichloropropane 50.0 49.0 ug/L 98 67-130
1,4-Dichlorobenzene 50.0 47.4 ug/L 95 70-120
2-Butanone (MEK)50.0 32.9 ug/L 66 53-141
2-Hexanone 50.0 36.5 ug/L 73 56-135
4-Methyl-2-pentanone (MIBK)50.0 37.5 ug/L 75 56-133
Acetone 50.0 30.4 ug/L 61 40-143
Acrylonitrile 500 461 ug/L 92 67-140
Benzene 50.0 46.0 ug/L 92 70-120
Bromochloromethane 50.0 42.5 ug/L 85 65-122
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QC Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-382996/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382996
Bromodichloromethane 50.0 44.6 ug/L 89 69-120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Bromoform 50.0 50.2 ug/L 100 56-132
Bromomethane 50.0 31.5 ug/L 63 40-130
Carbon disulfide 50.0 39.9 ug/L 80 66-120
Carbon tetrachloride 50.0 45.9 ug/L 92 65-122
Chlorobenzene 50.0 49.2 ug/L 98 70-120
Chloroethane 50.0 36.7 ug/L 73 45-127
Chloroform 50.0 44.8 ug/L 90 70-120
Chloromethane 50.0 42.3 ug/L 85 54-147
cis-1,2-Dichloroethene 50.0 45.7 ug/L 91 70-125
cis-1,3-Dichloropropene 50.0 47.7 ug/L 95 64-127
Dibromochloromethane 50.0 46.3 ug/L 93 68-125
Dibromomethane 50.0 43.5 ug/L 87 70-120
Ethylbenzene 50.0 48.0 ug/L 96 70-120
Iodomethane 50.0 41.2 ug/L 82 61-136
Methylene Chloride 50.0 40.7 ug/L 81 69-125
Styrene 50.0 46.1 ug/L 92 70-120
Tetrachloroethene 50.0 52.3 ug/L 105 70-128
Tetrahydrofuran 100 87.2 ug/L 87 59-139
Toluene 50.0 49.4 ug/L 99 70-125
trans-1,2-Dichloroethene 50.0 43.7 ug/L 87 70-125
trans-1,3-Dichloropropene 50.0 46.5 ug/L 93 62-128
trans-1,4-Dichloro-2-butene 50.0 52.1 ug/L 104 60-130
Trichloroethene 50.0 47.6 ug/L 95 70-125
Trichlorofluoromethane 50.0 41.5 ug/L 83 70-126
Vinyl acetate 50.0 37.9 ug/L 76 43-133
Vinyl chloride 50.0 40.7 ug/L 81 64-126
Xylenes, Total 100 96.8 ug/L 97 70-125
Dibromofluoromethane 75 -120
Surrogate
92
LCS LCS
Qualifier Limits%Recovery
1001,2-Dichloroethane-d4 (Surr)75 -126
1044-Bromofluorobenzene (Surr)72 -124
99Toluene-d8 (Surr)75 -120
Client Sample ID: Method BlankLab Sample ID: MB 500-382998/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382998
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 04/30/17 20:14 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<1.0 0.381.0 ug/L 04/30/17 20:14 11,1,1-Trichloroethane
<1.0 0.401.0 ug/L 04/30/17 20:14 11,1,2,2-Tetrachloroethane
<1.0 0.351.0 ug/L 04/30/17 20:14 11,1,2-Trichloroethane
<1.0 0.411.0 ug/L 04/30/17 20:14 11,1-Dichloroethane
<1.0 0.391.0 ug/L 04/30/17 20:14 11,1-Dichloroethene
<1.0 0.411.0 ug/L 04/30/17 20:14 11,2,3-Trichloropropane
<5.0 2.05.0 ug/L 04/30/17 20:14 11,2-Dibromo-3-Chloropropane
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QC Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 500-382998/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382998
RL MDL
1,2-Dibromoethane <1.0 1.0 0.39 ug/L 04/30/17 20:14 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<1.0 0.331.0 ug/L 04/30/17 20:14 11,2-Dichlorobenzene
<1.0 0.391.0 ug/L 04/30/17 20:14 11,2-Dichloroethane
<1.0 0.431.0 ug/L 04/30/17 20:14 11,2-Dichloropropane
<1.0 0.361.0 ug/L 04/30/17 20:14 11,4-Dichlorobenzene
<5.0 2.15.0 ug/L 04/30/17 20:14 12-Butanone (MEK)
<5.0 1.65.0 ug/L 04/30/17 20:14 12-Hexanone
<5.0 2.25.0 ug/L 04/30/17 20:14 14-Methyl-2-pentanone (MIBK)
<5.0 1.75.0 ug/L 04/30/17 20:14 1Acetone
<20 4.520 ug/L 04/30/17 20:14 1Acrylonitrile
<0.50 0.150.50 ug/L 04/30/17 20:14 1Benzene
<1.0 0.431.0 ug/L 04/30/17 20:14 1Bromochloromethane
<1.0 0.371.0 ug/L 04/30/17 20:14 1Bromodichloromethane
<1.0 0.481.0 ug/L 04/30/17 20:14 1Bromoform
<2.0 0.802.0 ug/L 04/30/17 20:14 1Bromomethane
<2.0 0.452.0 ug/L 04/30/17 20:14 1Carbon disulfide
<1.0 0.381.0 ug/L 04/30/17 20:14 1Carbon tetrachloride
<1.0 0.391.0 ug/L 04/30/17 20:14 1Chlorobenzene
<1.0 0.511.0 ug/L 04/30/17 20:14 1Chloroethane
<2.0 0.372.0 ug/L 04/30/17 20:14 1Chloroform
<1.0 0.321.0 ug/L 04/30/17 20:14 1Chloromethane
<1.0 0.411.0 ug/L 04/30/17 20:14 1cis-1,2-Dichloroethene
<1.0 0.421.0 ug/L 04/30/17 20:14 1cis-1,3-Dichloropropene
<1.0 0.491.0 ug/L 04/30/17 20:14 1Dibromochloromethane
<1.0 0.271.0 ug/L 04/30/17 20:14 1Dibromomethane
<0.50 0.180.50 ug/L 04/30/17 20:14 1Ethylbenzene
<2.5 0.662.5 ug/L 04/30/17 20:14 1Iodomethane
<5.0 1.65.0 ug/L 04/30/17 20:14 1Methylene Chloride
<1.0 0.391.0 ug/L 04/30/17 20:14 1Styrene
<1.0 0.371.0 ug/L 04/30/17 20:14 1Tetrachloroethene
<10 1.910 ug/L 04/30/17 20:14 1Tetrahydrofuran
<0.50 0.150.50 ug/L 04/30/17 20:14 1Toluene
<1.0 0.351.0 ug/L 04/30/17 20:14 1trans-1,2-Dichloroethene
<1.0 0.361.0 ug/L 04/30/17 20:14 1trans-1,3-Dichloropropene
<5.0 1.25.0 ug/L 04/30/17 20:14 1trans-1,4-Dichloro-2-butene
<0.50 0.160.50 ug/L 04/30/17 20:14 1Trichloroethene
<1.0 0.431.0 ug/L 04/30/17 20:14 1Trichlorofluoromethane
<2.0 0.912.0 ug/L 04/30/17 20:14 1Vinyl acetate
<0.50 0.200.50 ug/L 04/30/17 20:14 1Vinyl chloride
<1.0 0.221.0 ug/L 04/30/17 20:14 1Xylenes, Total
Dibromofluoromethane 99 75-120 04/30/17 20:14 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
102 04/30/17 20:14 11,2-Dichloroethane-d4 (Surr)75-126
89 04/30/17 20:14 14-Bromofluorobenzene (Surr)72-124
96 04/30/17 20:14 1Toluene-d8 (Surr)75-120
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QC Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-382998/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382998
1,1,1,2-Tetrachloroethane 50.0 51.3 ug/L 103 70-125
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
1,1,1-Trichloroethane 50.0 44.6 ug/L 89 70-125
1,1,2,2-Tetrachloroethane 50.0 49.7 ug/L 99 67-127
1,1,2-Trichloroethane 50.0 51.4 ug/L 103 70-122
1,1-Dichloroethane 50.0 49.3 ug/L 99 70-125
1,1-Dichloroethene 50.0 46.1 ug/L 92 67-122
1,2,3-Trichloropropane 50.0 44.9 ug/L 90 50-133
1,2-Dibromo-3-Chloropropane 50.0 40.6 ug/L 81 56-123
1,2-Dibromoethane 50.0 49.1 ug/L 98 70-125
1,2-Dichlorobenzene 50.0 48.7 ug/L 97 70-125
1,2-Dichloroethane 50.0 48.7 ug/L 97 68-127
1,2-Dichloropropane 50.0 53.6 ug/L 107 67-130
1,4-Dichlorobenzene 50.0 48.9 ug/L 98 70-120
2-Butanone (MEK)50.0 37.7 ug/L 75 53-141
2-Hexanone 50.0 35.8 ug/L 72 56-135
4-Methyl-2-pentanone (MIBK)50.0 35.7 ug/L 71 56-133
Acetone 50.0 42.0 ug/L 84 40-143
Acrylonitrile 500 491 ug/L 98 67-140
Benzene 50.0 47.2 ug/L 94 70-120
Bromochloromethane 50.0 48.9 ug/L 98 65-122
Bromodichloromethane 50.0 46.6 ug/L 93 69-120
Bromoform 50.0 56.9 ug/L 114 56-132
Bromomethane 50.0 49.8 ug/L 100 40-130
Carbon disulfide 50.0 45.0 ug/L 90 66-120
Carbon tetrachloride 50.0 44.8 ug/L 90 65-122
Chlorobenzene 50.0 52.6 ug/L 105 70-120
Chloroethane 50.0 44.5 ug/L 89 45-127
Chloroform 50.0 46.6 ug/L 93 70-120
Chloromethane 50.0 40.3 ug/L 81 54-147
cis-1,2-Dichloroethene 50.0 47.2 ug/L 94 70-125
cis-1,3-Dichloropropene 50.0 47.7 ug/L 95 64-127
Dibromochloromethane 50.0 50.6 ug/L 101 68-125
Dibromomethane 50.0 49.0 ug/L 98 70-120
Ethylbenzene 50.0 50.5 ug/L 101 70-120
Iodomethane 50.0 39.6 ug/L 79 61-136
Methylene Chloride 50.0 46.3 ug/L 93 69-125
Styrene 50.0 51.7 ug/L 103 70-120
Tetrachloroethene 50.0 52.2 ug/L 104 70-128
Tetrahydrofuran 100 92.0 ug/L 92 59-139
Toluene 50.0 49.8 ug/L 100 70-125
trans-1,2-Dichloroethene 50.0 46.9 ug/L 94 70-125
trans-1,3-Dichloropropene 50.0 47.6 ug/L 95 62-128
trans-1,4-Dichloro-2-butene 50.0 40.2 ug/L 80 60-130
Trichloroethene 50.0 48.6 ug/L 97 70-125
Trichlorofluoromethane 50.0 41.8 ug/L 84 70-126
Vinyl acetate 50.0 26.9 ug/L 54 43-133
Vinyl chloride 50.0 46.8 ug/L 94 64-126
Xylenes, Total 100 100 ug/L 100 70-125
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QC Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Dibromofluoromethane 75 -120
Surrogate
95
LCS LCS
Qualifier Limits%Recovery
961,2-Dichloroethane-d4 (Surr)75 -126
904-Bromofluorobenzene (Surr)72 -124
100Toluene-d8 (Surr)75 -120
Client Sample ID: SW-3Lab Sample ID: 500-126939-14 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382998
1,1,1,2-Tetrachloroethane <1.0 50.0 51.0 ug/L 102 70-125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
1,1,1-Trichloroethane <1.0 50.0 43.1 ug/L 86 70-125
1,1,2,2-Tetrachloroethane <1.0 50.0 50.5 ug/L 101 67-127
1,1,2-Trichloroethane <1.0 50.0 52.4 ug/L 105 70-122
1,1-Dichloroethane <1.0 50.0 48.0 ug/L 96 70-125
1,1-Dichloroethene <1.0 50.0 44.4 ug/L 89 67-122
1,2,3-Trichloropropane <1.0 50.0 44.7 ug/L 89 50-133
1,2-Dibromo-3-Chloropropane <5.0 50.0 42.1 ug/L 84 56-123
1,2-Dibromoethane <1.0 50.0 49.7 ug/L 99 70-125
1,2-Dichlorobenzene <1.0 50.0 48.8 ug/L 98 70-125
1,2-Dichloroethane <1.0 50.0 47.9 ug/L 96 68-127
1,2-Dichloropropane <1.0 50.0 53.0 ug/L 106 67-130
1,4-Dichlorobenzene <1.0 50.0 47.7 ug/L 95 70-120
2-Butanone (MEK)<5.0 50.0 37.3 ug/L 75 53-141
2-Hexanone <5.0 50.0 33.0 ug/L 66 56-135
4-Methyl-2-pentanone (MIBK)<5.0 50.0 34.5 ug/L 69 56-133
Acetone <5.0 50.0 37.5 ug/L 75 40-143
Acrylonitrile <20 500 493 ug/L 99 67-140
Benzene <0.50 50.0 46.0 ug/L 92 70-120
Bromochloromethane <1.0 50.0 48.3 ug/L 97 65-122
Bromodichloromethane <1.0 50.0 46.2 ug/L 92 69-120
Bromoform <1.0 50.0 56.2 ug/L 112 56-132
Bromomethane <2.0 50.0 55.4 ug/L 111 40-130
Carbon disulfide <2.0 50.0 43.1 ug/L 86 66-120
Carbon tetrachloride <1.0 50.0 44.1 ug/L 88 65-122
Chlorobenzene <1.0 50.0 51.6 ug/L 103 70-120
Chloroethane <1.0 50.0 47.4 ug/L 95 45-127
Chloroform <2.0 50.0 46.0 ug/L 92 70-120
Chloromethane <1.0 50.0 37.3 ug/L 75 54-147
cis-1,2-Dichloroethene <1.0 50.0 46.7 ug/L 93 70-125
cis-1,3-Dichloropropene <1.0 50.0 46.3 ug/L 93 64-127
Dibromochloromethane <1.0 50.0 51.0 ug/L 102 68-125
Dibromomethane <1.0 50.0 49.3 ug/L 99 70-120
Ethylbenzene <0.50 50.0 48.5 ug/L 97 70-120
Iodomethane <2.5 50.0 35.3 ug/L 71 61-136
Methylene Chloride <5.0 50.0 46.3 ug/L 93 69-125
Styrene <1.0 50.0 50.0 ug/L 100 70-120
Tetrachloroethene <1.0 50.0 49.7 ug/L 99 70-128
Tetrahydrofuran <10 100 85.1 ug/L 85 59-139
Toluene <0.50 50.0 49.1 ug/L 98 70-125
trans-1,2-Dichloroethene <1.0 50.0 45.4 ug/L 91 70-125
trans-1,3-Dichloropropene <1.0 50.0 46.3 ug/L 93 62-128
trans-1,4-Dichloro-2-butene <5.0 50.0 40.0 ug/L 80 60-130
Trichloroethene <0.50 50.0 47.2 ug/L 94 70-125
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QC Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: SW-3Lab Sample ID: 500-126939-14 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382998
Trichlorofluoromethane <1.0 50.0 41.5 ug/L 83 70-126
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Vinyl acetate <2.0 50.0 27.2 ug/L 54 43-133
Vinyl chloride <0.50 50.0 46.5 ug/L 93 64-126
Xylenes, Total <1.0 100 97.2 ug/L 97 70-125
Dibromofluoromethane 75 -120
Surrogate
95
MS MS
Qualifier Limits%Recovery
961,2-Dichloroethane-d4 (Surr)75 -126
924-Bromofluorobenzene (Surr)72 -124
100Toluene-d8 (Surr)75 -120
Client Sample ID: SW-3Lab Sample ID: 500-126939-14 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382998
1,1,1,2-Tetrachloroethane <1.0 50.0 51.3 ug/L 103 70-125 1 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
1,1,1-Trichloroethane <1.0 50.0 43.7 ug/L 87 70-125 1 20
1,1,2,2-Tetrachloroethane <1.0 50.0 49.9 ug/L 100 67-127 1 20
1,1,2-Trichloroethane <1.0 50.0 51.0 ug/L 102 70-122 3 20
1,1-Dichloroethane <1.0 50.0 49.2 ug/L 98 70-125 2 20
1,1-Dichloroethene <1.0 50.0 44.7 ug/L 89 67-122 1 20
1,2,3-Trichloropropane <1.0 50.0 44.4 ug/L 89 50-133 1 20
1,2-Dibromo-3-Chloropropane <5.0 50.0 39.8 ug/L 80 56-123 6 20
1,2-Dibromoethane <1.0 50.0 49.3 ug/L 99 70-125 1 20
1,2-Dichlorobenzene <1.0 50.0 49.1 ug/L 98 70-125 1 20
1,2-Dichloroethane <1.0 50.0 48.1 ug/L 96 68-127 0 20
1,2-Dichloropropane <1.0 50.0 53.4 ug/L 107 67-130 1 20
1,4-Dichlorobenzene <1.0 50.0 48.0 ug/L 96 70-120 1 20
2-Butanone (MEK)<5.0 50.0 40.3 ug/L 81 53-141 8 20
2-Hexanone <5.0 50.0 33.8 ug/L 68 56-135 2 20
4-Methyl-2-pentanone (MIBK)<5.0 50.0 35.1 ug/L 70 56-133 2 20
Acetone <5.0 50.0 37.0 ug/L 74 40-143 2 20
Acrylonitrile <20 500 492 ug/L 98 67-140 0 20
Benzene <0.50 50.0 46.9 ug/L 94 70-120 2 20
Bromochloromethane <1.0 50.0 48.7 ug/L 97 65-122 1 20
Bromodichloromethane <1.0 50.0 46.5 ug/L 93 69-120 1 20
Bromoform <1.0 50.0 56.3 ug/L 113 56-132 0 20
Bromomethane <2.0 50.0 55.2 ug/L 110 40-130 0 20
Carbon disulfide <2.0 50.0 44.1 ug/L 88 66-120 2 20
Carbon tetrachloride <1.0 50.0 44.6 ug/L 89 65-122 1 20
Chlorobenzene <1.0 50.0 51.6 ug/L 103 70-120 0 20
Chloroethane <1.0 50.0 47.1 ug/L 94 45-127 1 20
Chloroform <2.0 50.0 46.5 ug/L 93 70-120 1 20
Chloromethane <1.0 50.0 40.8 ug/L 82 54-147 9 20
cis-1,2-Dichloroethene <1.0 50.0 47.1 ug/L 94 70-125 1 20
cis-1,3-Dichloropropene <1.0 50.0 46.4 ug/L 93 64-127 0 20
Dibromochloromethane <1.0 50.0 51.2 ug/L 102 68-125 0 20
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QC Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: SW-3Lab Sample ID: 500-126939-14 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382998
Dibromomethane <1.0 50.0 49.4 ug/L 99 70-120 0 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Ethylbenzene <0.50 50.0 48.6 ug/L 97 70-120 0 20
Iodomethane <2.5 50.0 38.6 ug/L 77 61-136 9 20
Methylene Chloride <5.0 50.0 46.7 ug/L 93 69-125 1 20
Styrene <1.0 50.0 50.7 ug/L 101 70-120 2 20
Tetrachloroethene <1.0 50.0 50.7 ug/L 101 70-128 2 20
Tetrahydrofuran <10 100 89.1 ug/L 89 59-139 5 20
Toluene <0.50 50.0 49.6 ug/L 99 70-125 1 20
trans-1,2-Dichloroethene <1.0 50.0 46.3 ug/L 93 70-125 2 20
trans-1,3-Dichloropropene <1.0 50.0 46.0 ug/L 92 62-128 1 20
trans-1,4-Dichloro-2-butene <5.0 50.0 39.2 ug/L 78 60-130 2 20
Trichloroethene <0.50 50.0 47.8 ug/L 96 70-125 1 20
Trichlorofluoromethane <1.0 50.0 41.7 ug/L 83 70-126 0 20
Vinyl acetate <2.0 50.0 26.0 ug/L 52 43-133 5 20
Vinyl chloride <0.50 50.0 46.7 ug/L 93 64-126 0 20
Xylenes, Total <1.0 100 98.1 ug/L 98 70-125 1 20
Dibromofluoromethane 75 -120
Surrogate
97
MSD MSD
Qualifier Limits%Recovery
961,2-Dichloroethane-d4 (Surr)75 -126
924-Bromofluorobenzene (Surr)72 -124
100Toluene-d8 (Surr)75 -120
Method: 200.8 - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 500-381890/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382074 Prep Batch: 381890
RL MDL
Antimony <3.0 3.0 1.3 ug/L 04/24/17 10:35 04/24/17 18:08 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<1.0 0.151.0 ug/L 04/24/17 10:35 04/24/17 18:08 1Arsenic
<2.5 0.372.5 ug/L 04/24/17 10:35 04/24/17 18:08 1Barium
<1.0 0.431.0 ug/L 04/24/17 10:35 04/24/17 18:08 1Beryllium
<0.50 0.150.50 ug/L 04/24/17 10:35 04/24/17 18:08 1Cadmium
<5.0 2.35.0 ug/L 04/24/17 10:35 04/24/17 18:08 1Chromium
<1.0 0.271.0 ug/L 04/24/17 10:35 04/24/17 18:08 1Cobalt
<2.0 0.632.0 ug/L 04/24/17 10:35 04/24/17 18:08 1Copper
<2.0 0.922.0 ug/L 04/24/17 10:35 04/24/17 18:08 1Nickel
<2.5 1.12.5 ug/L 04/24/17 10:35 04/24/17 18:08 1Selenium
<0.50 0.0780.50 ug/L 04/24/17 10:35 04/24/17 18:08 1Silver
<5.0 2.05.0 ug/L 04/24/17 10:35 04/24/17 18:08 1Vanadium
18.3 J 8.120 ug/L 04/24/17 10:35 04/24/17 18:08 1Zinc
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QC Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Method: 200.8 - Metals (ICP/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 500-381890/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382298 Prep Batch: 381890
RL MDL
Lead <0.50 0.50 0.16 ug/L 04/24/17 10:35 04/25/17 11:53 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<2.0 0.652.0 ug/L 04/24/17 10:35 04/25/17 11:53 1Thallium
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-381890/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382074 Prep Batch: 381890
Antimony 500 469 ug/L 94 85-115
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Arsenic 100 92.6 ug/L 93 85-115
Barium 500 484 ug/L 97 85-115
Beryllium 50.0 50.2 ug/L 100 85-115
Cadmium 50.0 48.4 ug/L 97 85-115
Chromium 200 195 ug/L 97 85-115
Cobalt 500 484 ug/L 97 85-115
Copper 250 242 ug/L 97 85-115
Nickel 500 495 ug/L 99 85-115
Selenium 100 94.6 ug/L 95 85-115
Silver 50.0 49.8 ug/L 100 85-115
Vanadium 500 472 ug/L 94 85-115
Zinc 500 484 ug/L 97 85-115
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-381890/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382298 Prep Batch: 381890
Lead 100 100 ug/L 100 85-115
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Thallium 100 101 ug/L 101 85-115
Client Sample ID: MW-2Lab Sample ID: 500-126939-2 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382074 Prep Batch: 381890
Antimony <3.0 500 482 ug/L 96 70-130
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Arsenic 1.2 100 95.7 ug/L 95 70-130
Barium 74 500 539 ug/L 93 70-130
Beryllium <1.0 50.0 46.0 ug/L 92 70-130
Cadmium <0.50 50.0 48.6 ug/L 97 70-130
Chromium <5.0 200 188 ug/L 94 70-130
Cobalt 0.59 J 500 461 ug/L 92 70-130
Copper 0.79 J 250 242 ug/L 97 70-130
Nickel 2.8 500 464 ug/L 92 70-130
Selenium <2.5 100 94.0 ug/L 94 70-130
Silver <0.50 50.0 49.0 ug/L 98 70-130
Vanadium 2.5 J 500 464 ug/L 92 70-130
Zinc <20 500 486 ug/L 97 70-130
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QC Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Method: 200.8 - Metals (ICP/MS) (Continued)
Client Sample ID: MW-2Lab Sample ID: 500-126939-2 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382298 Prep Batch: 381890
Lead 0.51 100 98.1 ug/L 98 70-130
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Thallium <2.0 100 98.4 ug/L 98 70-130
Client Sample ID: MW-2Lab Sample ID: 500-126939-2 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382074 Prep Batch: 381890
Antimony <3.0 <3.0 ug/L NC 20
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Arsenic 1.2 1.30 ug/L 12 20
Barium 74 76.0 ug/L 3 20
Beryllium <1.0 <1.0 ug/L NC 20
Cadmium <0.50 <0.50 ug/L NC 20
Chromium <5.0 <5.0 ug/L NC 20
Cobalt 0.59 J 1.20 F5 ug/L 68 20
Copper 0.79 J 1.19 J F5 ug/L 40 20
Nickel 2.8 3.42 F5 ug/L 22 20
Selenium <2.5 <2.5 ug/L NC 20
Silver <0.50 <0.50 ug/L NC 20
Vanadium 2.5 J 3.10 J ug/L 20 20
Zinc <20 16.8 J ug/L NC 20
Client Sample ID: MW-2Lab Sample ID: 500-126939-2 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382298 Prep Batch: 381890
Lead 0.51 0.448 J ug/L 14 20
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Thallium <2.0 <2.0 ug/L NC 20
Client Sample ID: Method BlankLab Sample ID: MB 500-382108/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382298 Prep Batch: 382108
RL MDL
Antimony <3.0 3.0 1.3 ug/L 04/25/17 10:50 04/25/17 15:38 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<1.0 0.151.0 ug/L 04/25/17 10:50 04/25/17 15:38 1Arsenic
<2.5 0.372.5 ug/L 04/25/17 10:50 04/25/17 15:38 1Barium
<1.0 0.431.0 ug/L 04/25/17 10:50 04/25/17 15:38 1Beryllium
<0.50 0.150.50 ug/L 04/25/17 10:50 04/25/17 15:38 1Cadmium
<5.0 2.35.0 ug/L 04/25/17 10:50 04/25/17 15:38 1Chromium
<1.0 0.271.0 ug/L 04/25/17 10:50 04/25/17 15:38 1Cobalt
<2.0 0.632.0 ug/L 04/25/17 10:50 04/25/17 15:38 1Copper
<0.50 0.160.50 ug/L 04/25/17 10:50 04/25/17 15:38 1Lead
<2.0 0.922.0 ug/L 04/25/17 10:50 04/25/17 15:38 1Nickel
<2.5 1.12.5 ug/L 04/25/17 10:50 04/25/17 15:38 1Selenium
<0.50 0.0780.50 ug/L 04/25/17 10:50 04/25/17 15:38 1Silver
<2.0 0.652.0 ug/L 04/25/17 10:50 04/25/17 15:38 1Thallium
<5.0 2.05.0 ug/L 04/25/17 10:50 04/25/17 15:38 1Vanadium
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QC Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Method: 200.8 - Metals (ICP/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 500-382108/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382298 Prep Batch: 382108
RL MDL
Zinc <20 20 8.1 ug/L 04/25/17 10:50 04/25/17 15:38 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-382108/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382298 Prep Batch: 382108
Antimony 500 512 ug/L 102 85-115
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Arsenic 100 104 ug/L 104 85-115
Barium 500 520 ug/L 104 85-115
Beryllium 50.0 44.7 ug/L 89 85-115
Cadmium 50.0 50.1 ug/L 100 85-115
Chromium 200 189 ug/L 95 85-115
Cobalt 500 468 ug/L 94 85-115
Copper 250 251 ug/L 100 85-115
Lead 100 100 ug/L 100 85-115
Nickel 500 472 ug/L 94 85-115
Selenium 100 104 ug/L 104 85-115
Silver 50.0 50.7 ug/L 101 85-115
Thallium 100 99.2 ug/L 99 85-115
Vanadium 500 471 ug/L 94 85-115
Zinc 500 516 ug/L 103 85-115
Client Sample ID: MW-9Lab Sample ID: 500-126939-9 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382298 Prep Batch: 382108
Antimony <3.0 500 509 ug/L 102 70-130
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Arsenic 2.3 100 109 ug/L 106 70-130
Barium 360 500 876 ug/L 103 70-130
Beryllium <1.0 50.0 43.3 ug/L 87 70-130
Cadmium <0.50 50.0 48.5 ug/L 97 70-130
Chromium <5.0 200 175 ug/L 87 70-130
Cobalt 0.77 J 500 427 ug/L 85 70-130
Copper 0.72 J 250 245 ug/L 98 70-130
Lead 0.23 J 100 94.0 ug/L 94 70-130
Nickel 2.0 500 426 ug/L 85 70-130
Selenium <2.5 100 104 ug/L 104 70-130
Silver <0.50 50.0 48.3 ug/L 97 70-130
Thallium <2.0 100 94.0 ug/L 94 70-130
Vanadium 2.0 J 500 448 ug/L 89 70-130
Zinc <20 500 498 ug/L 100 70-130
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QC Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Method: 200.8 - Metals (ICP/MS) (Continued)
Client Sample ID: SW-1Lab Sample ID: 500-126939-12 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382298 Prep Batch: 382108
Antimony <3.0 500 512 ug/L 102 70-130
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Arsenic 0.61 J 100 106 ug/L 105 70-130
Barium 48 500 558 ug/L 102 70-130
Beryllium <1.0 50.0 47.1 ug/L 94 70-130
Cadmium <0.50 50.0 50.6 ug/L 101 70-130
Chromium <5.0 200 189 ug/L 94 70-130
Cobalt 0.58 J 500 466 ug/L 93 70-130
Copper 0.95 J 250 254 ug/L 101 70-130
Lead 0.38 J 100 97.8 ug/L 97 70-130
Nickel <2.0 500 472 ug/L 94 70-130
Selenium <2.5 100 105 ug/L 105 70-130
Silver <0.50 50.0 50.4 ug/L 101 70-130
Thallium <2.0 100 97.4 ug/L 97 70-130
Vanadium <5.0 500 472 ug/L 94 70-130
Zinc <20 500 517 ug/L 103 70-130
Client Sample ID: MW-9Lab Sample ID: 500-126939-9 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382298 Prep Batch: 382108
Antimony <3.0 <3.0 ug/L NC 20
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Arsenic 2.3 2.34 ug/L 3 20
Barium 360 367 ug/L 1 20
Beryllium <1.0 <1.0 ug/L NC 20
Cadmium <0.50 <0.50 ug/L NC 20
Chromium <5.0 <5.0 ug/L NC 20
Cobalt 0.77 J 0.806 J ug/L 5 20
Copper 0.72 J 1.36 J F5 ug/L 61 20
Lead 0.23 J 0.257 J ug/L 10 20
Nickel 2.0 2.50 F5 ug/L 24 20
Selenium <2.5 <2.5 ug/L NC 20
Silver <0.50 <0.50 ug/L NC 20
Thallium <2.0 <2.0 ug/L NC 20
Vanadium 2.0 J 2.36 J ug/L 16 20
Zinc <20 <20 ug/L NC 20
Client Sample ID: SW-1Lab Sample ID: 500-126939-12 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382298 Prep Batch: 382108
Antimony <3.0 <3.0 ug/L NC 20
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Arsenic 0.61 J 0.553 J ug/L 9 20
Barium 48 48.0 ug/L 0.8 20
Beryllium <1.0 <1.0 ug/L NC 20
Cadmium <0.50 <0.50 ug/L NC 20
Chromium <5.0 <5.0 ug/L NC 20
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QC Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Method: 200.8 - Metals (ICP/MS) (Continued)
Client Sample ID: SW-1Lab Sample ID: 500-126939-12 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382298 Prep Batch: 382108
Cobalt 0.58 J 0.712 J ug/L 20 20
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Copper 0.95 J 0.932 J ug/L 2 20
Lead 0.38 J 0.470 J F5 ug/L 21 20
Nickel <2.0 <2.0 ug/L NC 20
Selenium <2.5 <2.5 ug/L NC 20
Silver <0.50 <0.50 ug/L NC 20
Thallium <2.0 <2.0 ug/L NC 20
Vanadium <5.0 <5.0 ug/L NC 20
Zinc <20 <20 ug/L NC 20
Method: 245.1 - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 500-381673/12-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381786 Prep Batch: 381673
RL MDL
Mercury <0.20 0.20 0.091 ug/L 04/22/17 16:00 04/23/17 09:15 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-381673/13-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381786 Prep Batch: 381673
Mercury 2.00 2.00 ug/L 100 85-115
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: SW-4Lab Sample ID: 500-126939-15 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381786 Prep Batch: 381673
Mercury <0.20 1.00 0.981 ug/L 98 70-130
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: SW-4Lab Sample ID: 500-126939-15 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381786 Prep Batch: 381673
Mercury <0.20 <0.20 ug/L NC 20
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Method: 9056A - Anions, Ion Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 500-383286/39
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383286
RL MDL
Chloride <0.20 0.20 0.17 mg/L 05/01/17 13:23 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.20 0.0950.20 mg/L 05/01/17 13:23 1Sulfate
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QC Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-383286/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383286
Chloride 3.00 2.85 mg/L 95 80-120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Sulfate 5.00 5.23 mg/L 105 80-120
Client Sample ID: MW-11Lab Sample ID: 500-126939-11 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383286
Sulfate 26 F1 50.0 92.4 F1 mg/L 134 80-120
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: MW-11Lab Sample ID: 500-126939-11 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383286
Sulfate 26 F1 50.0 91.3 F1 mg/L 131 80-120 1 15
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Client Sample ID: Method BlankLab Sample ID: MB 500-383470/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383470
RL MDL
Chloride <0.20 0.20 0.17 mg/L 05/02/17 12:54 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.20 0.0950.20 mg/L 05/02/17 12:54 1Sulfate
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-383470/8
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383470
Chloride 3.00 2.79 mg/L 93 80-120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Sulfate 5.00 5.10 mg/L 102 80-120
Client Sample ID: MW-10Lab Sample ID: 500-126939-10 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383470
Sulfate 23 F1 12.5 32.7 F1 mg/L 79 80-120
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: MW-10Lab Sample ID: 500-126939-10 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383470
Sulfate 23 F1 12.5 32.5 F1 mg/L 78 80-120 0 15
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
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QC Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Method: 9056A - Anions, Ion Chromatography (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 500-383685/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383685
RL MDL
Sulfate <0.20 0.20 0.095 mg/L 05/03/17 11:28 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-383685/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 383685
Sulfate 5.00 5.15 mg/L 103 80-120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Method: SM 2320B - Alkalinity
Client Sample ID: Method BlankLab Sample ID: MB 500-382285/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382285
RL MDL
Alkalinity <5.0 5.0 3.7 mg/L 04/25/17 12:40 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-382285/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382285
Alkalinity 100 85.5 mg/L 86 80-120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: MW-1Lab Sample ID: 500-126939-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382285
Alkalinity 410 409 mg/L 0.8 20
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Method: SM 2540C - Solids, Total Dissolved (TDS)
Client Sample ID: Method BlankLab Sample ID: MB 500-381824/1
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381824
RL MDL
Total Dissolved Solids <10 10 4.3 mg/L 04/24/17 03:40 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-381824/2
Matrix: Water Prep Type: Total/NA
Analysis Batch: 381824
Total Dissolved Solids 250 298 mg/L 119 80-120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
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QC Sample Results
TestAmerica Job ID: 500-126939-1Client: Civil & Environmental Consultants Inc
SDG: 11-370Project/Site: NC Apex Landfill
Method: SM 2540C - Solids, Total Dissolved (TDS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 500-382034/1
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382034
RL MDL
Total Dissolved Solids <10 10 4.3 mg/L 04/25/17 04:08 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-382034/2
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382034
Total Dissolved Solids 250 296 mg/L 118 80-120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: MW-2Lab Sample ID: 500-126939-2 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 382034
Total Dissolved Solids 530 528 mg/L 0.4 5
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
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Lab Chronicle
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-126939-1
Project/Site: NC Apex Landfill SDG: 11-370
Client Sample ID: MW-1 Lab Sample ID: 500-126939-1
Matrix: WaterDate Collected: 04/19/17 18:25
Date Received: 04/21/17 08:50
Analysis 8260B 05/01/17 01:42 EMA1 382992 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 381890 04/24/17 10:35 LWN TAL CHITotal/NA
Analysis 200.8 1 382074 04/24/17 18:23 PFK TAL CHITotal/NA
Prep 200.8 381890 04/24/17 10:35 LWN TAL CHITotal/NA
Analysis 200.8 1 382298 04/25/17 12:08 PFK TAL CHITotal/NA
Prep 245.1 381673 04/22/17 16:00 MJD TAL CHITotal/NA
Analysis 245.1 1 381786 04/23/17 09:26 MJD TAL CHITotal/NA
Analysis 9056A 2 383286 05/01/17 16:21 PMF TAL CHITotal/NA
Analysis 9056A 1000 383286 05/01/17 16:34 PMF TAL CHITotal/NA
Analysis SM 2320B 1 382285 04/25/17 13:43 SMO TAL CHITotal/NA
Analysis SM 2540C 1 381824 04/24/17 04:38 CLB TAL CHITotal/NA
Client Sample ID: MW-2 Lab Sample ID: 500-126939-2
Matrix: WaterDate Collected: 04/20/17 12:20
Date Received: 04/21/17 08:50
Analysis 8260B 05/01/17 02:07 EMA1 382992 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 381890 04/24/17 10:35 LWN TAL CHITotal/NA
Analysis 200.8 1 382074 04/24/17 18:27 PFK TAL CHITotal/NA
Prep 200.8 381890 04/24/17 10:35 LWN TAL CHITotal/NA
Analysis 200.8 1 382298 04/25/17 12:11 PFK TAL CHITotal/NA
Prep 245.1 381673 04/22/17 16:00 MJD TAL CHITotal/NA
Analysis 245.1 1 381786 04/23/17 09:38 MJD TAL CHITotal/NA
Analysis 9056A 50 383286 05/01/17 15:18 PMF TAL CHITotal/NA
Analysis SM 2320B 1 382285 04/25/17 13:58 SMO TAL CHITotal/NA
Analysis SM 2540C 1 382034 04/25/17 04:13 CLB TAL CHITotal/NA
Client Sample ID: MW-3 Lab Sample ID: 500-126939-3
Matrix: WaterDate Collected: 04/20/17 13:00
Date Received: 04/21/17 08:50
Analysis 8260B 05/01/17 02:33 EMA1 382992 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 381890 04/24/17 10:35 LWN TAL CHITotal/NA
Analysis 200.8 1 382074 04/24/17 18:49 PFK TAL CHITotal/NA
Prep 200.8 381890 04/24/17 10:35 LWN TAL CHITotal/NA
Analysis 200.8 1 382298 04/25/17 12:34 PFK TAL CHITotal/NA
Prep 245.1 381673 04/22/17 16:00 MJD TAL CHITotal/NA
Analysis 245.1 1 381786 04/23/17 09:40 MJD TAL CHITotal/NA
Analysis 9056A 100 383286 05/01/17 15:56 PMF TAL CHITotal/NA
Analysis SM 2320B 1 382285 04/25/17 14:06 SMO TAL CHITotal/NA
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Lab Chronicle
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-126939-1
Project/Site: NC Apex Landfill SDG: 11-370
Client Sample ID: MW-3 Lab Sample ID: 500-126939-3
Matrix: WaterDate Collected: 04/20/17 13:00
Date Received: 04/21/17 08:50
Analysis SM 2540C 04/25/17 04:18 CLB1 382034 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: MW-4 Lab Sample ID: 500-126939-4
Matrix: WaterDate Collected: 04/19/17 16:25
Date Received: 04/21/17 08:50
Analysis 8260B 05/01/17 02:58 EMA1 382992 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 381890 04/24/17 10:35 LWN TAL CHITotal/NA
Analysis 200.8 1 382074 04/24/17 18:53 PFK TAL CHITotal/NA
Prep 200.8 381890 04/24/17 10:35 LWN TAL CHITotal/NA
Analysis 200.8 1 382298 04/25/17 12:38 PFK TAL CHITotal/NA
Prep 245.1 381673 04/22/17 16:00 MJD TAL CHITotal/NA
Analysis 245.1 1 381786 04/23/17 09:41 MJD TAL CHITotal/NA
Analysis 9056A 50 383286 05/01/17 16:08 PMF TAL CHITotal/NA
Analysis SM 2320B 1 382285 04/25/17 13:19 SMO TAL CHITotal/NA
Analysis SM 2540C 1 382034 04/25/17 04:21 CLB TAL CHITotal/NA
Client Sample ID: MW-5 Lab Sample ID: 500-126939-5
Matrix: WaterDate Collected: 04/19/17 15:25
Date Received: 04/21/17 08:50
Analysis 8260B 05/01/17 03:23 EMA1 382992 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 381890 04/24/17 10:35 LWN TAL CHITotal/NA
Analysis 200.8 1 382074 04/24/17 18:57 PFK TAL CHITotal/NA
Prep 200.8 381890 04/24/17 10:35 LWN TAL CHITotal/NA
Analysis 200.8 1 382298 04/25/17 12:43 PFK TAL CHITotal/NA
Prep 245.1 381673 04/22/17 16:00 MJD TAL CHITotal/NA
Analysis 245.1 1 381786 04/23/17 09:42 MJD TAL CHITotal/NA
Analysis 9056A 5 383470 05/02/17 14:07 PMF TAL CHITotal/NA
Analysis SM 2320B 1 382285 04/25/17 14:12 SMO TAL CHITotal/NA
Analysis SM 2540C 1 382034 04/25/17 04:23 CLB TAL CHITotal/NA
Client Sample ID: MW-6 Lab Sample ID: 500-126939-6
Matrix: WaterDate Collected: 04/19/17 14:50
Date Received: 04/21/17 08:50
Analysis 8260B 05/01/17 03:48 EMA1 382992 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 381890 04/24/17 10:35 LWN TAL CHITotal/NA
Analysis 200.8 1 382074 04/24/17 19:01 PFK TAL CHITotal/NA
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Lab Chronicle
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-126939-1
Project/Site: NC Apex Landfill SDG: 11-370
Client Sample ID: MW-6 Lab Sample ID: 500-126939-6
Matrix: WaterDate Collected: 04/19/17 14:50
Date Received: 04/21/17 08:50
Prep 200.8 04/24/17 10:35 LWN381890 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 200.8 1 382298 04/25/17 12:47 PFK TAL CHITotal/NA
Prep 200.8 381890 04/24/17 10:35 LWN TAL CHITotal/NA
Analysis 200.8 2 382298 04/25/17 12:50 PFK TAL CHITotal/NA
Prep 245.1 381673 04/22/17 16:00 MJD TAL CHITotal/NA
Analysis 245.1 1 381786 04/23/17 09:44 MJD TAL CHITotal/NA
Analysis 9056A 10 383286 05/01/17 17:49 PMF TAL CHITotal/NA
Analysis SM 2320B 1 382285 04/25/17 14:17 SMO TAL CHITotal/NA
Analysis SM 2540C 1 382034 04/25/17 04:26 CLB TAL CHITotal/NA
Client Sample ID: MW-7 Lab Sample ID: 500-126939-7
Matrix: WaterDate Collected: 04/19/17 14:10
Date Received: 04/21/17 08:50
Analysis 8260B 05/01/17 04:13 EMA1 382992 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 381890 04/24/17 10:35 LWN TAL CHITotal/NA
Analysis 200.8 1 382074 04/24/17 19:04 PFK TAL CHITotal/NA
Prep 200.8 381890 04/24/17 10:35 LWN TAL CHITotal/NA
Analysis 200.8 1 382298 04/25/17 12:58 PFK TAL CHITotal/NA
Prep 245.1 381673 04/22/17 16:00 MJD TAL CHITotal/NA
Analysis 245.1 1 381786 04/23/17 09:45 MJD TAL CHITotal/NA
Analysis 9056A 10 383286 05/01/17 18:27 PMF TAL CHITotal/NA
Analysis SM 2320B 1 382285 04/25/17 14:23 SMO TAL CHITotal/NA
Analysis SM 2540C 1 382034 04/25/17 04:28 CLB TAL CHITotal/NA
Client Sample ID: MW-8 Lab Sample ID: 500-126939-8
Matrix: WaterDate Collected: 04/20/17 08:40
Date Received: 04/21/17 08:50
Analysis 8260B 05/01/17 04:39 EMA1 382992 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 381890 04/24/17 10:35 LWN TAL CHITotal/NA
Analysis 200.8 1 382074 04/24/17 19:08 PFK TAL CHITotal/NA
Prep 200.8 381890 04/24/17 10:35 LWN TAL CHITotal/NA
Analysis 200.8 1 382298 04/25/17 13:02 PFK TAL CHITotal/NA
Prep 245.1 381673 04/22/17 16:00 MJD TAL CHITotal/NA
Analysis 245.1 1 381786 04/23/17 09:47 MJD TAL CHITotal/NA
Analysis 9056A 20 383286 05/01/17 18:40 PMF TAL CHITotal/NA
Analysis SM 2320B 1 382285 04/25/17 14:30 SMO TAL CHITotal/NA
Analysis SM 2540C 1 382034 04/25/17 04:31 CLB TAL CHITotal/NA
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Lab Chronicle
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-126939-1
Project/Site: NC Apex Landfill SDG: 11-370
Client Sample ID: MW-9 Lab Sample ID: 500-126939-9
Matrix: WaterDate Collected: 04/19/17 13:30
Date Received: 04/21/17 08:50
Analysis 8260B 05/01/17 02:06 TCT1 382998 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 382108 04/25/17 10:50 LWN TAL CHITotal/NA
Analysis 200.8 1 382298 04/25/17 15:46 PFK TAL CHITotal/NA
Prep 245.1 381673 04/22/17 16:00 MJD TAL CHITotal/NA
Analysis 245.1 1 381786 04/23/17 09:48 MJD TAL CHITotal/NA
Analysis 9056A 10 383470 05/02/17 14:45 PMF TAL CHITotal/NA
Analysis 9056A 100 383286 05/01/17 17:11 PMF TAL CHITotal/NA
Analysis SM 2320B 1 382285 04/25/17 14:37 SMO TAL CHITotal/NA
Analysis SM 2540C 1 382034 04/25/17 04:34 CLB TAL CHITotal/NA
Client Sample ID: MW-10 Lab Sample ID: 500-126939-10
Matrix: WaterDate Collected: 04/19/17 17:10
Date Received: 04/21/17 08:50
Analysis 8260B 05/01/17 02:35 TCT1 382998 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 382108 04/25/17 10:50 LWN TAL CHITotal/NA
Analysis 200.8 1 382298 04/25/17 16:01 PFK TAL CHITotal/NA
Prep 245.1 381673 04/22/17 16:00 MJD TAL CHITotal/NA
Analysis 245.1 1 381786 04/23/17 09:50 MJD TAL CHITotal/NA
Analysis 9056A 5 383470 05/02/17 14:57 PMF TAL CHITotal/NA
Analysis 9056A 1000 383286 05/01/17 17:37 PMF TAL CHITotal/NA
Analysis SM 2320B 1 382285 04/25/17 14:49 SMO TAL CHITotal/NA
Analysis SM 2540C 1 382034 04/25/17 04:36 CLB TAL CHITotal/NA
Client Sample ID: MW-11 Lab Sample ID: 500-126939-11
Matrix: WaterDate Collected: 04/19/17 17:55
Date Received: 04/21/17 08:50
Analysis 8260B 05/01/17 03:04 TCT1 382998 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 382108 04/25/17 10:50 LWN TAL CHITotal/NA
Analysis 200.8 1 382298 04/25/17 16:05 PFK TAL CHITotal/NA
Prep 245.1 381673 04/22/17 16:00 MJD TAL CHITotal/NA
Analysis 245.1 1 381786 04/23/17 09:51 MJD TAL CHITotal/NA
Analysis 9056A 50 383470 05/02/17 15:09 PMF TAL CHITotal/NA
Analysis 9056A 20 383286 05/01/17 18:53 PMF TAL CHITotal/NA
Analysis SM 2320B 1 382285 04/25/17 14:55 SMO TAL CHITotal/NA
Analysis SM 2540C 1 382034 04/25/17 04:39 CLB TAL CHITotal/NA
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Lab Chronicle
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-126939-1
Project/Site: NC Apex Landfill SDG: 11-370
Client Sample ID: SW-1 Lab Sample ID: 500-126939-12
Matrix: WaterDate Collected: 04/20/17 10:00
Date Received: 04/21/17 08:50
Analysis 8260B 05/01/17 03:33 TCT1 382998 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 382108 04/25/17 10:50 LWN TAL CHITotal/NA
Analysis 200.8 1 382298 04/25/17 16:16 PFK TAL CHITotal/NA
Prep 245.1 381673 04/22/17 16:00 MJD TAL CHITotal/NA
Analysis 245.1 1 381786 04/23/17 09:56 MJD TAL CHITotal/NA
Analysis 9056A 5 383470 05/02/17 15:22 PMF TAL CHITotal/NA
Analysis 9056A 2 383286 05/01/17 19:31 PMF TAL CHITotal/NA
Analysis SM 2320B 1 382285 04/25/17 15:00 SMO TAL CHITotal/NA
Analysis SM 2540C 1 382034 04/25/17 04:42 CLB TAL CHITotal/NA
Client Sample ID: SW-2 Lab Sample ID: 500-126939-13
Matrix: WaterDate Collected: 04/20/17 10:30
Date Received: 04/21/17 08:50
Analysis 8260B 05/01/17 04:03 TCT1 382998 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 382108 04/25/17 10:50 LWN TAL CHITotal/NA
Analysis 200.8 1 382298 04/25/17 16:31 PFK TAL CHITotal/NA
Prep 245.1 381673 04/22/17 16:00 MJD TAL CHITotal/NA
Analysis 245.1 1 381786 04/23/17 09:58 MJD TAL CHITotal/NA
Analysis 9056A 5 383470 05/02/17 15:34 PMF TAL CHITotal/NA
Analysis 9056A 2 383286 05/01/17 19:44 PMF TAL CHITotal/NA
Analysis SM 2320B 1 382285 04/25/17 15:06 SMO TAL CHITotal/NA
Analysis SM 2540C 1 382034 04/25/17 04:44 CLB TAL CHITotal/NA
Client Sample ID: SW-3 Lab Sample ID: 500-126939-14
Matrix: WaterDate Collected: 04/20/17 11:00
Date Received: 04/21/17 08:50
Analysis 8260B 05/01/17 04:32 TCT1 382998 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 382108 04/25/17 10:50 LWN TAL CHITotal/NA
Analysis 200.8 1 382298 04/25/17 16:35 PFK TAL CHITotal/NA
Prep 245.1 381673 04/22/17 16:00 MJD TAL CHITotal/NA
Analysis 245.1 1 381786 04/23/17 09:59 MJD TAL CHITotal/NA
Analysis 9056A 20 383685 05/03/17 15:35 PMF TAL CHITotal/NA
Analysis 9056A 50 383286 05/01/17 19:56 PMF TAL CHITotal/NA
Analysis SM 2320B 1 382285 04/25/17 13:25 SMO TAL CHITotal/NA
Analysis SM 2540C 1 382034 04/25/17 04:47 CLB TAL CHITotal/NA
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Lab Chronicle
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-126939-1
Project/Site: NC Apex Landfill SDG: 11-370
Client Sample ID: SW-4 Lab Sample ID: 500-126939-15
Matrix: WaterDate Collected: 04/20/17 10:35
Date Received: 04/21/17 08:50
Analysis 8260B 05/01/17 00:47 TCT1 382996 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 382108 04/25/17 10:50 LWN TAL CHITotal/NA
Analysis 200.8 1 382298 04/25/17 16:39 PFK TAL CHITotal/NA
Prep 245.1 381673 04/22/17 16:00 MJD TAL CHITotal/NA
Analysis 245.1 1 381786 04/23/17 10:00 MJD TAL CHITotal/NA
Analysis 9056A 10 383470 05/02/17 15:58 PMF TAL CHITotal/NA
Analysis SM 2320B 1 382285 04/25/17 13:35 SMO TAL CHITotal/NA
Analysis SM 2540C 1 382034 04/25/17 04:49 CLB TAL CHITotal/NA
Client Sample ID: Duplicate Lab Sample ID: 500-126939-16
Matrix: WaterDate Collected: 04/20/17 00:00
Date Received: 04/21/17 08:50
Analysis 8260B 05/01/17 01:13 TCT1 382996 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Laboratory References:
TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL [phone]
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Accreditation/Certification Summary
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-126939-1
Project/Site: NC Apex Landfill SDG: 11-370
Laboratory: TestAmerica Chicago
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program EPA Region Identification Number Expiration Date
North Carolina (WW/SW)2914State Program 12-31-17
Analysis Method Prep Method Matrix Analyte
The following analytes are included in this report, but accreditation/certification is not offered by the governing authority:
8260B Water trans-1,4-Dichloro-2-butene
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Login Sample Receipt Checklist
Client: Civil & Environmental Consultants Inc Job Number: 500-126939-1
SDG Number: 11-370
Login Number: 126939
Question Answer Comment
Creator: Scott, Sherri L
List Source: TestAmerica Chicago
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.4.8,3.2
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Chicago
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ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Chicago
2417 Bond Street
University Park, IL 60484
Tel: [phone]
TestAmerica Job ID: 500-129772-2
Client Project/Site: NC Highway 55
For:
Civil & Environmental Consultants Inc
1900 Center Park Drive
Suite A
Charlotte, North Carolina 28217
Attn: Phillip Pressley
Authorized for release by:
7/7/2017 3:53:16 PM
Robin Kintz, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 55
TestAmerica Job ID: 500-129772-2
Page 2 of 19 TestAmerica Chicago7/7/2017
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .15
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .16
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .17
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .19
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Case Narrative
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-129772-2
Project/Site: NC Highway 55
Job ID: 500-129772-2
Laboratory: TestAmerica Chicago
Narrative
Job Narrative
500-129772-2
Comments
No additional comments.
Receipt
The samples were received on 6/17/2017 10:20 AM; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperature of the cooler at receipt was 2.0º C.
GC/MS VOA
Method(s) 8260B: The samples with positive detects for Vinyl Chloride in the presence of freon 151 were re-collected and the lab
re-analyzed these on Instrument 25. The lab had determined this instrument to be "inert" to the degradation of freon 151 to Vinyl chloride.
The results for Vinyl Chloride were significantly lower from the original samples. The lab analyzed the Freon 151 standard on this
instrument before and after these samples were analyzed to confirm vinyl chloride was not detected and the instrument continues to be
"inert". The following sample was re-collected and analyzed: MW-8 (500-129772-1).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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Detection Summary
TestAmerica Job ID: 500-129772-2Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 55
Client Sample ID: MW-8 Lab Sample ID: 500-129772-1
No Detections.
TestAmerica Chicago
This Detection Summary does not include radiochemical test results.
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Method Summary
TestAmerica Job ID: 500-129772-2Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 55
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL CHI
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL [phone]
TestAmerica Chicago
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Sample Summary
TestAmerica Job ID: 500-129772-2Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 55
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
500-129772-1 MW-8 Water 06/15/17 18:00 06/17/17 10:20
TestAmerica Chicago
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Client Sample Results
TestAmerica Job ID: 500-129772-2Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 55
Lab Sample ID: 500-129772-1Client Sample ID: MW-8
Matrix: WaterDate Collected: 06/15/17 18:00
Date Received: 06/17/17 10:20
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 06/20/17 00:17 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.38 ug/L 06/20/17 00:17 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 06/20/17 00:17 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 06/20/17 00:17 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 06/20/17 00:17 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 06/20/17 00:17 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 06/20/17 00:17 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 06/20/17 00:17 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 06/20/17 00:17 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 06/20/17 00:17 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 06/20/17 00:17 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 06/20/17 00:17 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 06/20/17 00:17 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 06/20/17 00:17 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 06/20/17 00:17 12-Hexanone <5.0
5.0 2.2 ug/L 06/20/17 00:17 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 06/20/17 00:17 1Acetone<5.0
20 4.5 ug/L 06/20/17 00:17 1Acrylonitrile<20
0.50 0.15 ug/L 06/20/17 00:17 1Benzene<0.50
1.0 0.43 ug/L 06/20/17 00:17 1Bromochloromethane<1.0
1.0 0.37 ug/L 06/20/17 00:17 1Bromodichloromethane<1.0
1.0 0.48 ug/L 06/20/17 00:17 1Bromoform<1.0
2.0 0.80 ug/L 06/20/17 00:17 1Bromomethane<2.0
2.0 0.45 ug/L 06/20/17 00:17 1Carbon disulfide <2.0
1.0 0.38 ug/L 06/20/17 00:17 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 06/20/17 00:17 1Chlorobenzene<1.0
1.0 0.51 ug/L 06/20/17 00:17 1Chloroethane<1.0
2.0 0.37 ug/L 06/20/17 00:17 1Chloroform<2.0
1.0 0.32 ug/L 06/20/17 00:17 1Chloromethane<1.0
1.0 0.41 ug/L 06/20/17 00:17 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 06/20/17 00:17 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 06/20/17 00:17 1Dibromochloromethane<1.0
1.0 0.27 ug/L 06/20/17 00:17 1Dibromomethane<1.0
0.50 0.18 ug/L 06/20/17 00:17 1Ethylbenzene<0.50
2.5 0.66 ug/L 06/20/17 00:17 1Iodomethane<2.5
5.0 1.6 ug/L 06/20/17 00:17 1Methylene Chloride <5.0
1.0 0.39 ug/L 06/20/17 00:17 1Styrene<1.0
1.0 0.37 ug/L 06/20/17 00:17 1Tetrachloroethene<1.0
10 1.9 ug/L 06/20/17 00:17 1Tetrahydrofuran<10
0.50 0.15 ug/L 06/20/17 00:17 1Toluene<0.50
1.0 0.35 ug/L 06/20/17 00:17 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 06/20/17 00:17 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 06/20/17 00:17 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 06/20/17 00:17 1Trichloroethene<0.50
1.0 0.43 ug/L 06/20/17 00:17 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 06/20/17 00:17 1Vinyl acetate <2.0
0.50 0.20 ug/L 06/20/17 00:17 1Vinyl chloride <0.50
1.0 0.22 ug/L 06/20/17 00:17 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-129772-2Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 55
Lab Sample ID: 500-129772-1Client Sample ID: MW-8
Matrix: WaterDate Collected: 06/15/17 18:00
Date Received: 06/17/17 10:20
1,2-Dichloroethane-d4 (Surr)101 75-126 06/20/17 00:17 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
4-Bromofluorobenzene (Surr)88 06/20/17 00:17 172-124
Dibromofluoromethane 106 06/20/17 00:17 175-120
Toluene-d8 (Surr)92 06/20/17 00:17 175-120
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Definitions/Glossary
TestAmerica Job ID: 500-129772-2Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 55
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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QC Association Summary
TestAmerica Job ID: 500-129772-2Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 55
GC/MS VOA
Analysis Batch: 389940
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B500-129772-1 MW-8 Total/NA
Water 8260BMB 500-389940/7 Method Blank Total/NA
Water 8260BLCS 500-389940/5 Lab Control Sample Total/NA
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Surrogate Summary
TestAmerica Job ID: 500-129772-2Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 55
Method: 8260B - Volatile Organic Compounds (GC/MS)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (75-126) (72-124) (75-120) (75-120)
12DCE BFB DBFM TOL
101 88 106 92500-129772-1
Percent Surrogate Recovery (Acceptance Limits)
MW-8
93 89 98 95LCS 500-389940/5 Lab Control Sample
98 88 104 92MB 500-389940/7 Method Blank
Surrogate Legend
12DCE = 1,2-Dichloroethane-d4 (Surr)
BFB = 4-Bromofluorobenzene (Surr)
DBFM = Dibromofluoromethane
TOL = Toluene-d8 (Surr)
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QC Sample Results
TestAmerica Job ID: 500-129772-2Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 55
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 500-389940/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 389940
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 06/19/17 16:29 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<1.0 0.381.0 ug/L 06/19/17 16:29 11,1,1-Trichloroethane
<1.0 0.401.0 ug/L 06/19/17 16:29 11,1,2,2-Tetrachloroethane
<1.0 0.351.0 ug/L 06/19/17 16:29 11,1,2-Trichloroethane
<1.0 0.411.0 ug/L 06/19/17 16:29 11,1-Dichloroethane
<1.0 0.391.0 ug/L 06/19/17 16:29 11,1-Dichloroethene
<1.0 0.411.0 ug/L 06/19/17 16:29 11,2,3-Trichloropropane
<5.0 2.05.0 ug/L 06/19/17 16:29 11,2-Dibromo-3-Chloropropane
<1.0 0.391.0 ug/L 06/19/17 16:29 11,2-Dibromoethane
<1.0 0.331.0 ug/L 06/19/17 16:29 11,2-Dichlorobenzene
<1.0 0.391.0 ug/L 06/19/17 16:29 11,2-Dichloroethane
<1.0 0.431.0 ug/L 06/19/17 16:29 11,2-Dichloropropane
<1.0 0.361.0 ug/L 06/19/17 16:29 11,4-Dichlorobenzene
<5.0 2.15.0 ug/L 06/19/17 16:29 12-Butanone (MEK)
<5.0 1.65.0 ug/L 06/19/17 16:29 12-Hexanone
<5.0 2.25.0 ug/L 06/19/17 16:29 14-Methyl-2-pentanone (MIBK)
<5.0 1.75.0 ug/L 06/19/17 16:29 1Acetone
<20 4.520 ug/L 06/19/17 16:29 1Acrylonitrile
<0.50 0.150.50 ug/L 06/19/17 16:29 1Benzene
<1.0 0.431.0 ug/L 06/19/17 16:29 1Bromochloromethane
<1.0 0.371.0 ug/L 06/19/17 16:29 1Bromodichloromethane
<1.0 0.481.0 ug/L 06/19/17 16:29 1Bromoform
<2.0 0.802.0 ug/L 06/19/17 16:29 1Bromomethane
<2.0 0.452.0 ug/L 06/19/17 16:29 1Carbon disulfide
<1.0 0.381.0 ug/L 06/19/17 16:29 1Carbon tetrachloride
<1.0 0.391.0 ug/L 06/19/17 16:29 1Chlorobenzene
<1.0 0.511.0 ug/L 06/19/17 16:29 1Chloroethane
<2.0 0.372.0 ug/L 06/19/17 16:29 1Chloroform
<1.0 0.321.0 ug/L 06/19/17 16:29 1Chloromethane
<1.0 0.411.0 ug/L 06/19/17 16:29 1cis-1,2-Dichloroethene
<1.0 0.421.0 ug/L 06/19/17 16:29 1cis-1,3-Dichloropropene
<1.0 0.491.0 ug/L 06/19/17 16:29 1Dibromochloromethane
<1.0 0.271.0 ug/L 06/19/17 16:29 1Dibromomethane
<0.50 0.180.50 ug/L 06/19/17 16:29 1Ethylbenzene
<2.5 0.662.5 ug/L 06/19/17 16:29 1Iodomethane
<5.0 1.65.0 ug/L 06/19/17 16:29 1Methylene Chloride
<1.0 0.391.0 ug/L 06/19/17 16:29 1Styrene
<1.0 0.371.0 ug/L 06/19/17 16:29 1Tetrachloroethene
<10 1.910 ug/L 06/19/17 16:29 1Tetrahydrofuran
<0.50 0.150.50 ug/L 06/19/17 16:29 1Toluene
<1.0 0.351.0 ug/L 06/19/17 16:29 1trans-1,2-Dichloroethene
<1.0 0.361.0 ug/L 06/19/17 16:29 1trans-1,3-Dichloropropene
<5.0 1.25.0 ug/L 06/19/17 16:29 1trans-1,4-Dichloro-2-butene
<0.50 0.160.50 ug/L 06/19/17 16:29 1Trichloroethene
<1.0 0.431.0 ug/L 06/19/17 16:29 1Trichlorofluoromethane
<2.0 0.912.0 ug/L 06/19/17 16:29 1Vinyl acetate
<0.50 0.200.50 ug/L 06/19/17 16:29 1Vinyl chloride
<1.0 0.221.0 ug/L 06/19/17 16:29 1Xylenes, Total
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QC Sample Results
TestAmerica Job ID: 500-129772-2Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 55
1,2-Dichloroethane-d4 (Surr)98 75-126 06/19/17 16:29 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
88 06/19/17 16:29 14-Bromofluorobenzene (Surr)72-124
104 06/19/17 16:29 1Dibromofluoromethane75-120
92 06/19/17 16:29 1Toluene-d8 (Surr)75-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-389940/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 389940
1,1,1,2-Tetrachloroethane 50.0 50.6 ug/L 101 70-125
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
1,1,1-Trichloroethane 50.0 43.7 ug/L 87 70-125
1,1,2,2-Tetrachloroethane 50.0 46.5 ug/L 93 67-127
1,1,2-Trichloroethane 50.0 49.6 ug/L 99 70-122
1,1-Dichloroethane 50.0 44.7 ug/L 89 70-125
1,1-Dichloroethene 50.0 45.0 ug/L 90 67-122
1,2,3-Trichloropropane 50.0 40.7 ug/L 81 50-133
1,2-Dibromo-3-Chloropropane 50.0 37.7 ug/L 75 56-123
1,2-Dibromoethane 50.0 49.7 ug/L 99 70-125
1,2-Dichlorobenzene 50.0 47.5 ug/L 95 70-125
1,2-Dichloroethane 50.0 45.6 ug/L 91 68-127
1,2-Dichloropropane 50.0 48.5 ug/L 97 67-130
1,4-Dichlorobenzene 50.0 47.7 ug/L 95 70-120
2-Butanone (MEK)50.0 32.3 ug/L 65 53-141
2-Hexanone 50.0 35.1 ug/L 70 56-135
4-Methyl-2-pentanone (MIBK)50.0 35.9 ug/L 72 56-133
Acetone 50.0 40.2 ug/L 80 40-143
Acrylonitrile 500 486 ug/L 97 67-140
Benzene 50.0 44.8 ug/L 90 70-120
Bromochloromethane 50.0 51.9 ug/L 104 65-122
Bromodichloromethane 50.0 44.9 ug/L 90 69-120
Bromoform 50.0 53.7 ug/L 107 56-132
Bromomethane 50.0 61.9 ug/L 124 40-130
Carbon disulfide 50.0 43.1 ug/L 86 66-120
Carbon tetrachloride 50.0 45.7 ug/L 91 65-122
Chlorobenzene 50.0 48.4 ug/L 97 70-120
Chloroethane 50.0 45.5 ug/L 91 45-127
Chloroform 50.0 45.3 ug/L 91 70-120
Chloromethane 50.0 52.5 ug/L 105 54-147
cis-1,2-Dichloroethene 50.0 47.8 ug/L 96 70-125
cis-1,3-Dichloropropene 50.0 41.2 ug/L 82 64-127
Dibromochloromethane 50.0 50.9 ug/L 102 68-125
Dibromomethane 50.0 48.9 ug/L 98 70-120
Ethylbenzene 50.0 46.2 ug/L 92 70-120
Iodomethane 50.0 36.7 ug/L 73 61-136
Methylene Chloride 50.0 47.3 ug/L 95 69-125
Styrene 50.0 47.7 ug/L 95 70-120
Tetrachloroethene 50.0 49.4 ug/L 99 70-128
Tetrahydrofuran 100 69.1 ug/L 69 59-139
Toluene 50.0 45.2 ug/L 90 70-125
trans-1,2-Dichloroethene 50.0 46.9 ug/L 94 70-125
trans-1,3-Dichloropropene 50.0 41.5 ug/L 83 62-128
trans-1,4-Dichloro-2-butene 50.0 36.7 ug/L 73 60-130
Trichloroethene 50.0 51.3 ug/L 103 70-125
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QC Sample Results
TestAmerica Job ID: 500-129772-2Client: Civil & Environmental Consultants Inc
Project/Site: NC Highway 55
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-389940/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 389940
Trichlorofluoromethane 50.0 44.4 ug/L 89 70-126
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Vinyl acetate 50.0 35.6 ug/L 71 43-133
Vinyl chloride 50.0 41.2 ug/L 82 64-126
Xylenes, Total 100 89.0 ug/L 89 70-125
1,2-Dichloroethane-d4 (Surr)75 -126
Surrogate
93
LCS LCS
Qualifier Limits%Recovery
894-Bromofluorobenzene (Surr)72 -124
98Dibromofluoromethane 75 -120
95Toluene-d8 (Surr)75 -120
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Lab Chronicle
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-129772-2
Project/Site: NC Highway 55
Client Sample ID: MW-8 Lab Sample ID: 500-129772-1
Matrix: WaterDate Collected: 06/15/17 18:00
Date Received: 06/17/17 10:20
Analysis 8260B 06/20/17 00:17 EMA1 389940 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Laboratory References:
TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL [phone]
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Accreditation/Certification Summary
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-129772-2
Project/Site: NC Highway 55
Laboratory: TestAmerica Chicago
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program EPA Region Identification Number Expiration Date
North Carolina (WW/SW)2914State Program 12-31-17
Analysis Method Prep Method Matrix Analyte
The following analytes are included in this report, but accreditation/certification is not offered by the governing authority:
8260B Water trans-1,4-Dichloro-2-butene
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Login Sample Receipt Checklist
Client: Civil & Environmental Consultants Inc Job Number: 500-129772-2
Login Number: 129772
Question Answer Comment
Creator: Sanchez, Ariel M
List Source: TestAmerica Chicago
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
FalseContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
Refer to Job Narrative for details.
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
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#=CL#
April 26, 2017
LIMS USE: FR - ED STEPHENS
LIMS OBJECT ID: 92337907
92337907
Project:
Pace Project No.:
RE:
Ed Stephens
Civil & Environmental Consultants
1900 Center Park Drive
Charlotte, NC 28217
HWY 55 111-370
Dear Ed Stephens:
Enclosed are the analytical results for sample(s) received by the laboratory on April 20, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 16
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92337907
HWY 55 111-370
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 16
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92337907
HWY 55 111-370
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92337907001 SPLIT EPA 8260 63 PASI-CZDO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 16
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92337907
HWY 55 111-370
Sample: SPLIT Lab ID: 92337907001 Collected: 04/20/17 08:40 Received: 04/20/17 14:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 04/26/17 08:47 67-64-125.0 1
Benzene ND ug/L 04/26/17 08:47 71-43-21.0 1
Bromobenzene ND ug/L 04/26/17 08:47 108-86-11.0 1
Bromochloromethane ND ug/L 04/26/17 08:47 74-97-51.0 1
Bromodichloromethane ND ug/L 04/26/17 08:47 75-27-41.0 1
Bromoform ND ug/L 04/26/17 08:47 75-25-21.0 1
Bromomethane ND ug/L 04/26/17 08:47 74-83-92.0 1
2-Butanone (MEK)ND ug/L 04/26/17 08:47 78-93-35.0 1
Carbon tetrachloride ND ug/L 04/26/17 08:47 56-23-51.0 1
Chlorobenzene ND ug/L 04/26/17 08:47 108-90-71.0 1
Chloroethane ND ug/L 04/26/17 08:47 75-00-31.0 1
Chloroform ND ug/L 04/26/17 08:47 67-66-31.0 1
Chloromethane ND ug/L 04/26/17 08:47 74-87-31.0 1
2-Chlorotoluene ND ug/L 04/26/17 08:47 95-49-81.0 1
4-Chlorotoluene ND ug/L 04/26/17 08:47 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 04/26/17 08:47 96-12-82.0 1
Dibromochloromethane ND ug/L 04/26/17 08:47 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 04/26/17 08:47 106-93-41.0 1
Dibromomethane ND ug/L 04/26/17 08:47 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 04/26/17 08:47 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 04/26/17 08:47 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 04/26/17 08:47 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 04/26/17 08:47 75-71-81.0 1
1,1-Dichloroethane ND ug/L 04/26/17 08:47 75-34-31.0 1
1,2-Dichloroethane ND ug/L 04/26/17 08:47 107-06-21.0 1
1,1-Dichloroethene ND ug/L 04/26/17 08:47 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 04/26/17 08:47 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 04/26/17 08:47 156-60-51.0 1
1,2-Dichloropropane ND ug/L 04/26/17 08:47 78-87-51.0 1
1,3-Dichloropropane ND ug/L 04/26/17 08:47 142-28-91.0 1
2,2-Dichloropropane ND ug/L 04/26/17 08:47 594-20-71.0 1
1,1-Dichloropropene ND ug/L 04/26/17 08:47 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 04/26/17 08:47 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 04/26/17 08:47 10061-02-61.0 1
Diisopropyl ether ND ug/L 04/26/17 08:47 108-20-31.0 1
Ethylbenzene ND ug/L 04/26/17 08:47 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 04/26/17 08:47 87-68-31.0 1
2-Hexanone ND ug/L 04/26/17 08:47 591-78-65.0 1
p-Isopropyltoluene ND ug/L 04/26/17 08:47 99-87-61.0 1
Methylene Chloride ND ug/L 04/26/17 08:47 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/26/17 08:47 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 04/26/17 08:47 1634-04-41.0 1
Naphthalene ND ug/L 04/26/17 08:47 91-20-31.0 1
Styrene ND ug/L 04/26/17 08:47 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 04/26/17 08:47 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 04/26/17 08:47 79-34-51.0 1
Tetrachloroethene ND ug/L 04/26/17 08:47 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
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Page 4 of 16
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92337907
HWY 55 111-370
Sample: SPLIT Lab ID: 92337907001 Collected: 04/20/17 08:40 Received: 04/20/17 14:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
Toluene ND ug/L 04/26/17 08:47 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 04/26/17 08:47 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 04/26/17 08:47 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 04/26/17 08:47 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 04/26/17 08:47 79-00-51.0 1
Trichloroethene ND ug/L 04/26/17 08:47 79-01-61.0 1
Trichlorofluoromethane ND ug/L 04/26/17 08:47 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 04/26/17 08:47 96-18-41.0 1
Vinyl acetate ND ug/L 04/26/17 08:47 108-05-42.0 1
Vinyl chloride ND ug/L 04/26/17 08:47 75-01-41.0 1
Xylene (Total)ND ug/L 04/26/17 08:47 1330-20-71.0 1
m&p-Xylene ND ug/L 04/26/17 08:47 179601-23-12.0 1
o-Xylene ND ug/L 04/26/17 08:47 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)99 %04/26/17 08:47 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %04/26/17 08:47 17060-07-070-130 1
Toluene-d8 (S)109 %04/26/17 08:47 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/26/2017 03:42 PM
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Page 5 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92337907
HWY 55 111-370
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
357974
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples: 92337907001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1985695
Associated Lab Samples:92337907001
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 04/26/17 00:42
1,1,1-Trichloroethane ug/L ND 1.0 04/26/17 00:42
1,1,2,2-Tetrachloroethane ug/L ND 1.0 04/26/17 00:42
1,1,2-Trichloroethane ug/L ND 1.0 04/26/17 00:42
1,1-Dichloroethane ug/L ND 1.0 04/26/17 00:42
1,1-Dichloroethene ug/L ND 1.0 04/26/17 00:42
1,1-Dichloropropene ug/L ND 1.0 04/26/17 00:42
1,2,3-Trichlorobenzene ug/L ND 1.0 04/26/17 00:42
1,2,3-Trichloropropane ug/L ND 1.0 04/26/17 00:42
1,2,4-Trichlorobenzene ug/L ND 1.0 04/26/17 00:42
1,2-Dibromo-3-chloropropane ug/L ND 2.0 04/26/17 00:42
1,2-Dibromoethane (EDB)ug/L ND 1.0 04/26/17 00:42
1,2-Dichlorobenzene ug/L ND 1.0 04/26/17 00:42
1,2-Dichloroethane ug/L ND 1.0 04/26/17 00:42
1,2-Dichloropropane ug/L ND 1.0 04/26/17 00:42
1,3-Dichlorobenzene ug/L ND 1.0 04/26/17 00:42
1,3-Dichloropropane ug/L ND 1.0 04/26/17 00:42
1,4-Dichlorobenzene ug/L ND 1.0 04/26/17 00:42
2,2-Dichloropropane ug/L ND 1.0 04/26/17 00:42
2-Butanone (MEK)ug/L ND 5.0 04/26/17 00:42
2-Chlorotoluene ug/L ND 1.0 04/26/17 00:42
2-Hexanone ug/L ND 5.0 04/26/17 00:42
4-Chlorotoluene ug/L ND 1.0 04/26/17 00:42
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 04/26/17 00:42
Acetone ug/L ND 25.0 04/26/17 00:42
Benzene ug/L ND 1.0 04/26/17 00:42
Bromobenzene ug/L ND 1.0 04/26/17 00:42
Bromochloromethane ug/L ND 1.0 04/26/17 00:42
Bromodichloromethane ug/L ND 1.0 04/26/17 00:42
Bromoform ug/L ND 1.0 04/26/17 00:42
Bromomethane ug/L ND 2.0 04/26/17 00:42
Carbon tetrachloride ug/L ND 1.0 04/26/17 00:42
Chlorobenzene ug/L ND 1.0 04/26/17 00:42
Chloroethane ug/L ND 1.0 04/26/17 00:42
Chloroform ug/L ND 1.0 04/26/17 00:42
Chloromethane ug/L ND 1.0 04/26/17 00:42
cis-1,2-Dichloroethene ug/L ND 1.0 04/26/17 00:42
cis-1,3-Dichloropropene ug/L ND 1.0 04/26/17 00:42
Dibromochloromethane ug/L ND 1.0 04/26/17 00:42
Dibromomethane ug/L ND 1.0 04/26/17 00:42
Dichlorodifluoromethane ug/L ND 1.0 04/26/17 00:42
REPORT OF LABORATORY ANALYSIS
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Page 6 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92337907
HWY 55 111-370
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1985695
Associated Lab Samples:92337907001
Matrix: Water
Analyzed
Diisopropyl ether ug/L ND 1.0 04/26/17 00:42
Ethylbenzene ug/L ND 1.0 04/26/17 00:42
Hexachloro-1,3-butadiene ug/L ND 1.0 04/26/17 00:42
m&p-Xylene ug/L ND 2.0 04/26/17 00:42
Methyl-tert-butyl ether ug/L ND 1.0 04/26/17 00:42
Methylene Chloride ug/L ND 2.0 04/26/17 00:42
Naphthalene ug/L ND 1.0 04/26/17 00:42
o-Xylene ug/L ND 1.0 04/26/17 00:42
p-Isopropyltoluene ug/L ND 1.0 04/26/17 00:42
Styrene ug/L ND 1.0 04/26/17 00:42
Tetrachloroethene ug/L ND 1.0 04/26/17 00:42
Toluene ug/L ND 1.0 04/26/17 00:42
trans-1,2-Dichloroethene ug/L ND 1.0 04/26/17 00:42
trans-1,3-Dichloropropene ug/L ND 1.0 04/26/17 00:42
Trichloroethene ug/L ND 1.0 04/26/17 00:42
Trichlorofluoromethane ug/L ND 1.0 04/26/17 00:42
Vinyl acetate ug/L ND 2.0 04/26/17 00:42
Vinyl chloride ug/L ND 1.0 04/26/17 00:42
Xylene (Total)ug/L ND 1.0 04/26/17 00:42
1,2-Dichloroethane-d4 (S)%112 70-130 04/26/17 00:42
4-Bromofluorobenzene (S)%101 70-130 04/26/17 00:42
Toluene-d8 (S)%107 70-130 04/26/17 00:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1985696LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.050 102 70-130
1,1,1-Trichloroethane ug/L 50.550 101 70-130
1,1,2,2-Tetrachloroethane ug/L 51.250 102 70-130
1,1,2-Trichloroethane ug/L 50.050 100 70-130
1,1-Dichloroethane ug/L 52.650 105 70-130
1,1-Dichloroethene ug/L 53.350 107 70-132
1,1-Dichloropropene ug/L 56.550 113 70-130
1,2,3-Trichlorobenzene ug/L 50.250 100 70-135
1,2,3-Trichloropropane ug/L 51.350 103 70-130
1,2,4-Trichlorobenzene ug/L 49.550 99 70-134
1,2-Dibromo-3-chloropropane ug/L 51.550 103 70-130
1,2-Dibromoethane (EDB)ug/L 51.350 103 70-130
1,2-Dichlorobenzene ug/L 50.150 100 70-130
1,2-Dichloroethane ug/L 54.850 110 70-130
1,2-Dichloropropane ug/L 52.650 105 70-130
1,3-Dichlorobenzene ug/L 48.650 97 70-130
1,3-Dichloropropane ug/L 57.050 114 70-130
1,4-Dichlorobenzene ug/L 48.450 97 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/26/2017 03:42 PM
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[phone]
Page 7 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92337907
HWY 55 111-370
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1985696LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 48.650 97 58-145
2-Butanone (MEK)ug/L 111100 111 70-145
2-Chlorotoluene ug/L 51.750 103 70-130
2-Hexanone ug/L 102100 102 70-144
4-Chlorotoluene ug/L 51.650 103 70-130
4-Methyl-2-pentanone (MIBK)ug/L 99.6100 100 70-140
Acetone ug/L 106100 106 50-175
Benzene ug/L 54.050 108 70-130
Bromobenzene ug/L 52.150 104 70-130
Bromochloromethane ug/L 48.650 97 70-130
Bromodichloromethane ug/L 50.850 102 70-130
Bromoform ug/L 47.950 96 70-130
Bromomethane ug/L 43.950 88 54-130
Carbon tetrachloride ug/L 49.050 98 70-132
Chlorobenzene ug/L 51.750 103 70-130
Chloroethane ug/L 50.650 101 64-134
Chloroform ug/L 49.050 98 70-130
Chloromethane ug/L 38.650 77 64-130
cis-1,2-Dichloroethene ug/L 51.450 103 70-131
cis-1,3-Dichloropropene ug/L 53.650 107 70-130
Dibromochloromethane ug/L 50.650 101 70-130
Dibromomethane ug/L 47.050 94 70-131
Dichlorodifluoromethane ug/L 50.050 100 56-130
Diisopropyl ether ug/L 52.250 104 70-130
Ethylbenzene ug/L 51.950 104 70-130
Hexachloro-1,3-butadiene ug/L 51.150 102 70-130
m&p-Xylene ug/L 102100 102 70-130
Methyl-tert-butyl ether ug/L 57.750 115 70-130
Methylene Chloride ug/L 51.150 102 63-130
Naphthalene ug/L 50.950 102 70-138
o-Xylene ug/L 51.650 103 70-130
p-Isopropyltoluene ug/L 47.250 94 70-130
Styrene ug/L 50.650 101 70-130
Tetrachloroethene ug/L 48.850 98 70-130
Toluene ug/L 51.450 103 70-130
trans-1,2-Dichloroethene ug/L 52.750 105 70-130
trans-1,3-Dichloropropene ug/L 53.150 106 70-132
Trichloroethene ug/L 49.750 99 70-130
Trichlorofluoromethane ug/L 56.850 114 62-133
Vinyl acetate ug/L 116100 116 66-157
Vinyl chloride ug/L 49.150 98 50-150
Xylene (Total)ug/L 153150 102 70-130
1,2-Dichloroethane-d4 (S)%116 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/26/2017 03:42 PM
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[phone]
Page 8 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92337907
HWY 55 111-370
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1986418MATRIX SPIKE SAMPLE:
MSSpike
Result
92337621005
1,1,1,2-Tetrachloroethane ug/L 21.020 105 70-130ND
1,1,1-Trichloroethane ug/L 23.920 119 70-130ND
1,1,2,2-Tetrachloroethane ug/L 21.820 109 70-130ND
1,1,2-Trichloroethane ug/L 22.020 110 70-130ND
1,1-Dichloroethane ug/L 24.620 123 70-130ND
1,1-Dichloroethene ug/L 25.620 128 70-166ND
1,1-Dichloropropene ug/L 26.5 M120133 70-130ND
1,2,3-Trichlorobenzene ug/L 22.420 112 70-130ND
1,2,3-Trichloropropane ug/L 21.320 106 70-130ND
1,2,4-Trichlorobenzene ug/L 22.520 112 70-130ND
1,2-Dibromo-3-chloropropane ug/L 23.720 119 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.420 107 70-130ND
1,2-Dichlorobenzene ug/L 22.420 112 70-130ND
1,2-Dichloroethane ug/L 24.820 124 70-130ND
1,2-Dichloropropane ug/L 24.220 121 70-130ND
1,3-Dichlorobenzene ug/L 21.820 109 70-130ND
1,3-Dichloropropane ug/L 24.020 120 70-130ND
1,4-Dichlorobenzene ug/L 22.420 112 70-130ND
2,2-Dichloropropane ug/L 24.620 123 70-130ND
2-Butanone (MEK)ug/L 46.640 116 70-130ND
2-Chlorotoluene ug/L 24.120 121 70-130ND
2-Hexanone ug/L 45.540 114 70-130ND
4-Chlorotoluene ug/L 24.020 120 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 43.240 108 70-130ND
Acetone ug/L 47.140 106 70-130ND
Benzene ug/L 25.120 126 70-148ND
Bromobenzene ug/L 24.020 120 70-130ND
Bromochloromethane ug/L 23.020 115 70-130ND
Bromodichloromethane ug/L 22.620 113 70-130ND
Bromoform ug/L 19.020 95 70-130ND
Bromomethane ug/L 16.320 81 70-130ND
Carbon tetrachloride ug/L 22.920 114 70-130ND
Chlorobenzene ug/L 23.020 115 70-146ND
Chloroethane ug/L 23.120 116 70-130ND
Chloroform ug/L 22.720 113 70-130ND
Chloromethane ug/L 15.820 79 70-130ND
cis-1,2-Dichloroethene ug/L 24.320 122 70-130ND
cis-1,3-Dichloropropene ug/L 24.020 120 70-130ND
Dibromochloromethane ug/L 20.720 103 70-130ND
Dibromomethane ug/L 21.520 108 70-130ND
Dichlorodifluoromethane ug/L 15.320 77 70-130ND
Diisopropyl ether ug/L 22.120 111 70-130ND
Ethylbenzene ug/L 24.220 121 70-130ND
Hexachloro-1,3-butadiene ug/L 24.420 122 70-130ND
m&p-Xylene ug/L 47.940 120 70-130ND
Methyl-tert-butyl ether ug/L 25.920 126 70-130ND
Methylene Chloride ug/L 22.720 114 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/26/2017 03:42 PM
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[phone]
Page 9 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92337907
HWY 55 111-370
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1986418MATRIX SPIKE SAMPLE:
MSSpike
Result
92337621005
Naphthalene ug/L 22.820 114 70-130ND
o-Xylene ug/L 23.720 119 70-130ND
p-Isopropyltoluene ug/L 21.620 108 70-130ND
Styrene ug/L 22.820 114 70-130ND
Tetrachloroethene ug/L 21.520 107 70-130ND
Toluene ug/L 24.520 122 70-155ND
trans-1,2-Dichloroethene ug/L 25.920 130 70-130ND
trans-1,3-Dichloropropene ug/L 23.320 117 70-130ND
Trichloroethene ug/L 23.220 116 69-151ND
Trichlorofluoromethane ug/L 27.1 M120135 70-130ND
Vinyl acetate ug/L 48.340 121 70-130ND
Vinyl chloride ug/L 21.120 106 70-130ND
1,2-Dichloroethane-d4 (S)%118 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92337995004
1986419SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1-Dichloroethane ug/L NDND
1,1-Dichloroethene ug/L NDND
1,1-Dichloropropene ug/L NDND
1,2,3-Trichlorobenzene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2,4-Trichlorobenzene ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,3-Dichlorobenzene ug/L NDND
1,3-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2,2-Dichloropropane ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Chlorotoluene ug/L NDND
2-Hexanone ug/L NDND
4-Chlorotoluene ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
Benzene ug/L NDND
REPORT OF LABORATORY ANALYSIS
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Page 10 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92337907
HWY 55 111-370
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92337995004
1986419SAMPLE DUPLICATE:
Bromobenzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L NDND
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Dichlorodifluoromethane ug/L NDND
Diisopropyl ether ug/L NDND
Ethylbenzene ug/L NDND
Hexachloro-1,3-butadiene ug/L NDND
m&p-Xylene ug/L NDND
Methyl-tert-butyl ether ug/L NDND
Methylene Chloride ug/L NDND
Naphthalene ug/L NDND
o-Xylene ug/L NDND
p-Isopropyltoluene ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl acetate ug/L NDND
Vinyl chloride ug/L NDND
Xylene (Total)ug/L NDND
1,2-Dichloroethane-d4 (S)%106 4110
4-Bromofluorobenzene (S)%102 399
Toluene-d8 (S)%112 2110
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/26/2017 03:42 PM
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[phone]
Page 11 of 16
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92337907
HWY 55 111-370
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/26/2017 03:42 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 16
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92337907
HWY 55 111-370
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92337907001 357974SPLITEPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2017 03:42 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 16
Page 14 of 16
Page 15 of 16
Page 16 of 16

APPENDIX C

August 2, 2017

Ms. Jackie Drummond
Compliance Hydrogeologist
Division of Waste Management - Solid Waste Section North Carolina Department of Environmental Quality
Asheville Regional Office
2090 US Highway 70
Swannanoa, NC 28778
Dear Jackie:

Subject: Highway 55 C&D Landfill – Permit 92-30
Greenway Waste Solutions of Apex, LLC
Demonstration Letter on Background Metals in Groundwater Samples CEC Project 111-370.0003

Per 15A NCAC 13B .0544 (b) (1) (I), Civil & Environmental Consultants, Inc. (CEC), on behalf of
Greenway Waste Solutions of Apex, LLC, is submitting this Demonstration Letter to establish that a
natural variation in groundwater quality has caused contamination at the aforementioned facility. Certain metals have been detected in the groundwater that is sampled and analyzed per the approved
Groundwater Monitoring Plan. These metals are regularly detected at concentrations exceeding their
respective cleanup standards as published in 15A NCAC 02L .0202 (Standards), or published Interim
Maximum Contaminant Levels (IMCL).
This letter presents:
• Statistical analysis used to determine metals of concern;
• Condensed historical information on the detection of metals in groundwater at the landfill;
• Information on the presence of reducing groundwater conditions and its impact on metal
solubility and mobility; and
• Summary of published information on the background presence of selected metals in groundwater and stream sediments.
Attachments include a site plan depicting groundwater monitoring well locations, selected field data
sheets on the latest sampling event; and figures on published stream sediment concentration data for
selected metals.
Ms. Jackie Drummond - NCDEQ
CEC Project 111-370.0003
Page 2
August 2, 2017

Statistical Analyses and Metals of Concern
Semi-annual groundwater monitoring has been performed at the landfill for an extended period.
CEC tabulated and statistically analyzed historical groundwater data for the Facility for the period
2013 thru 2017 to determine metals of concern. The criteria for selection of metals of concern are:
• Any constituent must have a minimum of two detections within 2013 and 2017 above
method detection limit (MDL);
• The geometric mean (GM) of the data for each constituent is then determined using only
values greater than MDL;
• A comparison is made between the GM against the Standard or IMCL (Standard/IMCL);
and
• If the comparison indicates the GM is greater than the Standard/IMCL, then the constituent
is a metal of concern.

Using the monitored wells, the analyses yielded three metals of concern: 1) Cobalt (1 µg/L) – GM of 5.6 µg/L, 9 samples above MDL;
2) Iron (300 µg/L) – GM of 1,669 µg/L, 17 samples above the MDL; and
3) Manganese (50 µg/L) – GM of 1,480 µg/L, 88 samples above the MDL.

Condensed Historical Information The groundwater-monitoring program at the Highway 55 C&D Landfill currently consists of 11
groundwater monitoring wells. Semi-annual sampling and analysis is conducted per the approved
Groundwater Monitoring Plan. For the time period evaluated, Appendix I metals have been analyzed.
The first available data (2013) show that manganese was the first and most prevalent metal detected. Arsenic, barium, chromium, copper, lead, nickel and zinc were observed in the historical records at levels less than their applicable current Standard. Various semi-annual reports submitted by others
state that the detected values represent background concentrations in the Piedmont.

Groundwater Conditions and Its Impact on Bedrock Metal Mobility Two of the metals of concern, iron and manganese, are well recognized as being part of the Triassic
Basin conglomerate. Both of these metals are easily mobilized from the conglomerate when reducing
groundwater conditions are present. Field sampling logs generated by CEC personnel during the last
two low-flow groundwater-sampling events identified a majority of the groundwater wells as having a negative Oxidation-Reduction Potential (ORP) measurement. This negative ORP indicates a reducing environment. A reducing environment allows for the converting insoluble forms of iron and
manganese in the conglomerate to soluble salts resulting in elevated concentrations of these metals in
the groundwater. CEC has also reviewed the historical field notes from 2013 to 2016. There are
notations of high turbidity in some collected samples. Similar to the solubilizing of the iron and manganese in reducing conditions, high-turbidity in the Triassic groundwater is well understood to
increase the total metal concentrations compared to a low-turbidity sample. The revised groundwater
Ms. Jackie Drummond - NCDEQ
CEC Project 111-370.0003
Page 3
August 2, 2017

sampling process of low-sampling now in practice should reduce the likelihood of high turbidity
samples going forwards.

Published Information on Selected Metals in Background
Cobalt is also well understood to be present in the Triassic geology. The Energy, Land and Natural
Resources Division of NCDEQ published maps(1) on the measured concentrations of this metal in
stream sediments. This map can be found in the Attachments. In the map, significant concentrations
of cobalt is observed in sediments. Cobalt in stream sediments has been observed to have
concentrations ranging from 5 to 10 milligrams per liter in the general area of the Facility. Comparing the detected stream sediment concentrations to the GM concentration of 5.6 µg/L, the presence of
cobalt due to naturally occurring background geology is concluded.

Conclusion
The presented data clearly supports the position that each of the six metals of concern detected in the
Facility groundwater are due to their presence in the natural geology. These metals should then be
removed from the Contaminants of Concern for the Facility at this time.

If you have any questions or comments, please feel free to contact me at [phone].
Sincerely,

CIVIL & ENVIRONMENTAL CONSULTANTS, INC.

Bruce D. Reilly, P.E. Scott L. Brown, P.E.
Senior Project Manager Vice President
Attachments

Cc: Mr. John Brown – Greenway Waste Solutions

(1) Hoffman, J.D., and Buttleman, Kim, 1994. National Geochemical Data Base: National Uranium Resource
Evaluation Data for the Conterminous United States, U.S. Geological Survey Digital Data Series DDS-18-
A.

ATTACHMENTS

DATE:DWG SCALE:
DRAWN BY:CHECKED BY:APPROVED BY:
PROJECT NO:
FIGURE NO.:
CHROMIUM STREAM SEDIMENT
111-370.001AS NOTEDJULY 2017
JKS DRAFT DRAFT 1
GREENWAY WASTE SOLUTIONS
AT NORTH MECK, LLC
NORTH MECK LANDFILL
HUNTERSVILLE, NORTH CAROLINA
www.cecinc.com
1900 Center Park Drive - Suite A - Charlotte, NC 28217
Ph: 980.237.0373 · Fax: [phone]
DATE:DWG SCALE:
DRAWN BY:CHECKED BY:APPROVED BY:
PROJECT NO:
FIGURE NO.:
IRON IN STREAM SEDIMENT
111-370.001AS NOTEDJULY 2017
JKS DRAFT DRAFT 2
GREENWAY WASTE SOLUTIONS
AT NORTH MECK, LLC
NORTH MECK LANDFILL
HUNTERSVILLE, NORTH CAROLINA
www.cecinc.com
1900 Center Park Drive - Suite A - Charlotte, NC 28217
Ph: 980.237.0373 · Fax: [phone]
DATE:DWG SCALE:
DRAWN BY:CHECKED BY:APPROVED BY:
PROJECT NO:
FIGURE NO.:
IRON IN STREAM SEDIMENT
111-370.001AS NOTEDJULY 2017
JKS DRAFT DRAFT 3
GREENWAY WASTE SOLUTIONS
AT NORTH MECK, LLC
NORTH MECK LANDFILL
HUNTERSVILLE, NORTH CAROLINA
www.cecinc.com
1900 Center Park Drive - Suite A - Charlotte, NC 28217
Ph: 980.237.0373 · Fax: [phone]
DATE:DWG SCALE:
DRAWN BY:CHECKED BY:APPROVED BY:
PROJECT NO:
FIGURE NO.:
MANGANESE IN STREAM SEDIMENT
111-370.001AS NOTEDJULY 2017
JKS DRAFT DRAFT 4
GREENWAY WASTE SOLUTIONS
AT NORTH MECK, LLC
NORTH MECK LANDFILL
HUNTERSVILLE, NORTH CAROLINA
www.cecinc.com
1900 Center Park Drive - Suite A - Charlotte, NC 28217
Ph: 980.237.0373 · Fax: [phone]
DATE:DWG SCALE:
DRAWN BY:CHECKED BY:APPROVED BY:
PROJECT NO:
FIGURE NO.:
VANADIUM IN STREAM SEDIMENT
111-370.001AS NOTEDJULY 2017
JKS DRAFT DRAFT 5
GREENWAY WASTE SOLUTIONS
AT NORTH MECK, LLC
NORTH MECK LANDFILL
HUNTERSVILLE, NORTH CAROLINA
www.cecinc.com
1900 Center Park Drive - Suite A - Charlotte, NC 28217
Ph: 980.237.0373 · Fax: [phone]
DATE:DWG SCALE:
DRAWN BY:CHECKED BY:APPROVED BY:
PROJECT NO:
FIGURE NO.:
WELL LOCATION MAP
111-370.0031"=250'MAY 2017
PNP EHS EHS 1
HIGHWAY 55 C&D LANDFILL
GREENWAY WASTE SOLUTIONS
OF APEX, LLC
REFERENCE www.cecinc.com
1900 Center Park Drive - Suite A - Charlotte, NC 28217
Ph: 980.237.0373 · Fax: [phone]
NORTH
LEGEND

August 2, 2017

Ms. Jackie Drummond
Compliance Hydrogeologist
Division of Waste Management - Solid Waste Section North Carolina Department of Environmental Quality
Asheville Regional Office
2090 US Highway 70
Swannanoa, NC 28778
Dear Jackie:

Subject: Highway 55 C&D Landfill – Permit 92-30
Greenway Waste Solutions of Apex, LLC
Demonstration Letter on Laboratory Analyses for Vinyl Chloride CEC Project 111-370.0003

Per 15A NCAC 13B .0544 (b) (1) (I), Civil & Environmental Consultants, Inc. (CEC), on behalf of
Greenway Waste Solutions of Apex, LLC has prepared and is submitting this Demonstration Letter
presenting history and recently discovered facts regarding the detections of vinyl chloride in groundwater that is sampled and analyzed per the conditions in the above permit. Vinyl chloride is
groundwater contaminant 145 as listed in 15A NCAC 02L .0202 and has a cleanup standard of 0.03
micrograms per liter (Standard) or the practical quantitation limit whichever is greater. This letter
presents condensed historical information on the detection of vinyl chloride in groundwater at the
landfill and then provides a timeline and facts generated during the investigation of higher than expected detection of vinyl chloride. Attachments include site plan showing well locations and
correspondence from analytical laboratories certified by the state to perform groundwater organic
analyses.

Condensed Historical Information
The groundwater-monitoring program at the Highway 55 C&D Landfill consists of a network of 11
groundwater monitoring wells and has been ongoing since operations at the Landfill started.
Available information on groundwater sampling results starts in the fall of 2009. Semi-annual
sampling takes place and the samples analyzed per the approved groundwater-monitoring plan. CEC has reviewed the available groundwater sampling result data from 2013 until spring of 2017.

Two monitoring wells (MW-2/MW-8) at the Facility contained vinyl chloride at concentrations above
the practical quantitation limit during the fall 2016 sampling. In 2013, the first detection of vinyl
chloride occurred in MW-8. At a permitted facility operated by Greenway Waste Solutions of North Meck a similar vinyl chloride data history exists. As part of CEC’s review of the North Meck vinyl
Ms. Jackie Drummond - NCDEQ
CEC Project 111-370.0003
Page 2
August 2, 2017

chloride history and after detailed review of the historical data for the Highway 55 C&D Landfill,
CEC was tasked with sampling the groundwater monitoring wells in 2017.

For the spring 2017 groundwater-sampling event, CEC obtained split samples and these were
delivered to TestAmerica and Pace Analytical Laboratories. For certain samples, higher than expected values of vinyl chloride were reported by TestAmerica compared against the Pace results.

CEC asked TestAmerica to review the results, analysis methodology, instruments used and interview
the analysts in an effort to either validate or discount this first round of 2017 results. TestAmerica
brought in their Senior Technical Services Group to review their process. In late May, TestAmerica informed CEC of the following results of their investigation:

1. Search indicated a possibility of conversion of a Freon refrigerant (Freon 151) to vinyl
chloride in the GC;
2. Confirmation of this occurred after TestAmerica obtained and ran a Freon 151 standard through their Chicago GCs, resulting only one of the GCs not converting the Freon 151 to
vinyl chloride;
3. A TestAmerica company-wide program was implemented and identified most of their GCs
converting the Freon 151 to vinyl chloride; and
4. TestAmerica started, and is continuing, a corrective-action program to identify and change the component(s) of the GCs converting the Freon. (It is reported that the likely cause is the
Purge and Trap mechanism.)

After receiving the information that the analytical procedure and equipment were the cause of the
higher than expected groundwater vinyl chloride results, CEC resampled MW-8 at the Highway 55 C&D Landfill in June 2017. The comparison of the recent historical vinyl chloride results are shown
in the following table:

Table 1 – Vinyl Chloride Results Fall 2016 to Spring 2017

Results are shown in µg/L BOLD = value exceeds the PQL or Standard of 0.03 µg/L for vinyl chloride
A figure showing the facility’s wells can be found in Attachment B.
CEC received from Shealy and their supplier of the silica gel (OI Analytical) in the Purge and Trap
mechanisms that are part of the GC letters documenting the results of their independent testing
Well I.D. October 2016 Vinyl Chloride
Shealy
April 2017 Vinyl Chloride
TestAmerica
April 2017 Vinyl Chloride
Pace
June 2017 Vinyl Chloride
TestAmerica
MW-8 2.8 4.2 <1.0 <0.5
Ms. Jackie Drummond - NCDEQ
CEC Project 111-370.0003
Page 3
August 2, 2017

confirming TestAmerica’s results. The various pieces of correspondence from TestAmerica, Shealy
and OI Analytical can be found in Attachment C.

Impacts on Compliance Status
The confirmed conversion of Freon 151 to vinyl chloride explains the higher than expected historical
data on vinyl chloride at the Highway 55 C&D Landfill. The groundwater as measured at the Facility
does not exhibit a groundwater violation of the published standards for volatile and semi-volatile
organic compounds. However, CEC and Greenway recognize that only one data point at this time is
considered reliable for vinyl chloride. We are proposing to continue the sampling program specified in the approved groundwater-monitoring plan. Confirmation of these second round results from the
spring 2017 sampling will continue to take place for the near future until the required four rounds of
data show compliance with the Standards. CEC will continue to obtain an analyze split samples and
blind duplicates from selected groundwater monitoring wells as we have recently done. TestAmerica
and Pace are continuing to work through reviews of their GCs to eliminate the issue(s) converting the Freon to vinyl chloride.

Conclusion

CEC on behalf of our client is requesting that NCDEQ discount the vinyl chloride analytical data when reviewing historical information from prior to 2017.

If you have any questions or comments, please feel free to contact me at [phone].

Sincerely,
CIVIL & ENVIRONMENTAL CONSULTANTS, INC.

Bruce D. Reilly, P.E. Scott L. Brown, P.E.
Senior Project Manager Vice President

Attachments
Cc: Mr. John Brown – Greenway Waste Solutions

ATTACHMENTS

1
Reilly, Bruce
From:Stephens, Ed
Sent:Wednesday, July 19, 2017 8:46 AM
To:Reilly, Bruce
Subject:FW: Vinyl chloride
fyi

Ed Stephens, P.G.
Civil & Environmental Consultants, Inc.
1900 Center Park Drive · Suite A · Charlotte, NC 28217
Toll-Free: 855-859-9932· Fax: [phone]
Mobile: [phone] · http://www.cecinc.com
Senior Leadership · Integrated Services · Personal Business Relationships

From: Dan Wright [mailto:[e-mail]]
Sent: Tuesday, January 10, 2017 8:58 AM
To: Stephens, Ed <[e-mail]>
Cc: Michael Kilpatrick <[e-mail]>; Grant Wilton <[e-mail]>
Subject: Vinyl chloride

Morning Ed,

We have solved the vinyl chloride mystery. All the samples that we are detecting vinyl chloride have the tentatively
identified compound 1-chloro-1-fluoroethane (molecular weight 82.5 aka Freon 151) which is breaking down in the
autosampler metal sample pathway to vinyl chloride (molecular weight 62.5). This is likely occurring in the 6 port valve
of the autosampler where actives site are catalyzing HF which accounts for 20 AMUs. I discussed this with Test America
staff since they had the large discrepancy between the two labs. It appears that some autosamplers are most likely to
have the active sites that cause this degradation of Freon 151. They have witnessed this specific issue first hand at Test
America as well.

We have ordered a single standard of Freon 151 which we will run on several instruments to determine if any do not
cause the degradation. This situation is fairly rare, but due to the presence of Freon 151 in these samples the conditions
were right to form vinyl chloride. I will call you to discuss, but wanted to get you in the loop now so you can pass this on
to your client and the applicable regulators.

Once we analyze the Freon 151 standard we should be able to switch out some components in our autosamplers to
remove the active site thus preventing the formation of vinyl chloride. If we demonstrate we can eliminate the
degradation issue we certainly want to talk to you about systematically getting this groundwater work back. We have
supported these sites for many years and appreciate the scope or requirements.

Thanks,

Dan

NOTICE: The information contained in this email and any document attached hereto is intended only for the
2
named recipient(s). If you are not the intended recipient, nor the employee or agent responsible for delivering
this message in confidence to the intended recipient(s), you are hereby notified that you have received this
transmittal in error, and any review, dissemination, distribution or copying of this transmittal or its attachments
is strictly prohibited. If you have received this transmittal and/or attachments in error, please notify me
immediately by reply e-mail and then delete this message, including any attachments.

Page 1 of 3
TestAmerica Chicago

Corrective Action Report
Client: Civil and Environmental Consultants Inc.
Project: NC Landfills
Site: NC North Mecklenburg Landfill, NC Highway 49 Landifll, NC Apex Landfill, NC
Responsible Parties: TestAmerica Chicago
Date Initiated: 05/24/17
Initiator: JoAnn Petruszak-Kmetty
Description of Problem: The client requested that the vinyl chloride (VC) data for job 500-127404 from the North Mecklenburg Landfill - Infill be re-reviewed because the results were “an
order of magnitude greater than the split samples results”. During the review, it
was observed that each sample that had a positive detect for vinyl chloride also had a tentatively identified compound (TIC) identified as 1-chloro-1-fluoroethane (Freon 151). An inquiry was made of the other TestAmerica laboratories and the technical support personnel within TestAmerica to see if others have seen this
correlation.
After a preliminary investigation was performed at three TestAmerica laboratories, the TestAmerica Technical Support Organization (TSO) determined that false positive or high-biased results for vinyl chloride can occur due to the
degradation of 1-chloro-1-fluoroethane (Freon 151) on some VOA GC/MS
instruments. Freon 151 is not a VOA target analyte and it is not commonly found in the environment, but it is present more frequently in landfill leachates and monitoring wells. All of the vinyl chloride artifacts attributable to Freon 151 that we have identified to date are associated with landfill operations.

When samples containing Freon 151 are analyzed on certain VOA GC/MS instruments that ‘activate’ or promote its degradation, vinyl chloride artifacts will

Page 2 of 3
TestAmerica Chicago

be generated. Some VOA instruments are highly ‘activated’ towards Freon 151 degradation, while others are quite ‘inert’. Freon 151 degradation is believed to
occur on active sites in the VOA instrument ‘sample pathway’ that have
developed over time, and may be difficult to reverse. Freon 151 has a characteristic mass spectrum and is easy to identify by library search. It will usually be evident as a significant peak eluting shortly after vinyl chloride.
Corrective Action Plan:
To correct the immediate problem, the following actions were taken: 1) Analyze a Freon 151 standard at ~ 300 ppb concentration on all VOC instruments.
2) Identify VOC instruments as ‘activated’ if VC is > RL, and ‘inert’ if VC is < RL,
in the analysis of the Freon 151 standard. 3) Monitor each presumptive positive detect for VC on an activated instrument for the presence of Freon 151. If Freon 151 is present, re-analyze samples with presumptive positives for VC on an inert instrument.
4) When/where possible, perform maintenance on activated instruments to
eliminate active sites and ensure inert status. 5) Review previous jobs that were analyzed from these sites and identify samples that had Freon 151 and VC detects.
Status as of 6-12-17: The TestAmerica Chicago laboratory has analyzed a Freon 151 standard on each VOA instrument in the laboratory and has identified which instruments are
‘activated’ and which instruments are ‘inert’.
All analysts have been informed of the situation and instructed to re-analyze samples with positive detects for VC and Freon 151 on an instrument which has been determined to be ‘inert’. The laboratory project manager will be informed of
the situation and the client will be notified if data is impacted.
The project manager will flag each known project site that historically has had Freon 151 with a method comment in TALs computer system so that it will appear on the analyst’s backlog upon arrival of samples to the laboratory.

The following jobs have been reviewed and samples containing VC and Freon 151 have been identified: 500-127325, -127370, -127404, -127480, -127268, and -126939. The results have been flagged with a ‘cn’ flag and narrated.

Page 3 of 3
TestAmerica Chicago

The TestAmerica Chicago laboratory is in the process of performing maintenance on the activated instruments to minimize or eliminate the active sites to ensure
an inert status.
Further Corrective Action Needed: 1. Systematically clean or replace sample pathway to identify location of
active site within the instrumentation.
2. 3.

Reviewed by: _____________
JoAnn Petruszak-Kmetty, GC/MS VOA Supervisor Date

Reviewed by: _____________ Robin Kintz, Project Manager Date

Reviewed by:
Terese A. Preston, QA Manager Date
Reviewed by:
Michael J. Healy, Laboratory Director Date

DATE:DWG SCALE:
DRAWN BY:CHECKED BY:APPROVED BY:
PROJECT NO:
FIGURE NO.:
WELL LOCATION MAP
111-370.0031"=250'MAY 2017
PNP EHS EHS 1
HIGHWAY 55 C&D LANDFILL
GREENWAY WASTE SOLUTIONS
OF APEX, LLC
REFERENCE www.cecinc.com
1900 Center Park Drive - Suite A - Charlotte, NC 28217
Ph: 980.237.0373 · Fax: [phone]
NORTH
LEGEND

APPENDIX D

From:Sugg, William P
To:Stephens, Ed
Cc:John Brown; Brown, Scott
Subject:APPROVAL - Detection Groundwater & Methane Monitoring Well Relocation - Hwy 55 LF
Date:Tuesday, May 09, 2017 7:08:52 AM
Attachments:9230-CDLF-2014 - GWS Request to Relocate Monitoring Wells (May 2 2017).pdf
Ed,
Based on a review and evaluation of Greenway Waste Solutions’ request (see below and attached)
for the Hwy 55 C&D Landfill facility , the Section approves relocating monitoring well MW-11 and
methane monitor well MM-9 as proposed on the attached figure. The stated reason for the request
is to accommodate construction of a new access road and for general facility routing improvements.
We agree that relocating these two monitoring wells as proposed will maintain the integrity of the
groundwater monitoring and methane monitoring at the facility.

According to information provided by CEC, MW-11 was last sampled in April 2017 and MM-9 was
last monitored on May 4, 2017. The next scheduled monitoring events at the GWS’s Apex C&D
Landfill facility are: semi-annual groundwater monitoring in October 2017, and quarterly methane
monitoring in August 2017. According to the proposed plan, GWS will abandon (in place) wells MW-
11 and MM-9 and install new wells at the proposed locations prior to the next monitoring events.
The new wells will replace the abandoned wells in their respective monitoring networks.

The Section requests the following for abandoning the wells:
· MW-11 and MM-9 shall be properly abandoned and sealed in accordance with 15A BCAC 2C
.0113, entitled “Abandonment of Wells”, and
· Well abandonment records (GW-30 form) for each decommissioned piezometer, boring,
and groundwater monitoring well must be certified by a Licensed Geologist in accordance
with rule .1623(b)(2)(1) and submitted to the Solid Waste Section in accordance with 15A
NCAC 2C. 0114(b).
· Update the Water Quality Monitoring and Landfill Gas Monitoring Plans (May 2016) to
reflect changes due to the new well locations and any monitoring tables etc.

In addition, please contact me on the schedule for abandonment and installation so that I may
option whether to visit the site during well drilling. If, for some reason, the wells are not abandoned
prior the next scheduled monitoring events, continue collecting and reporting monitoring data from
these wells until further notice.
If you have any questions, feel free to call or email.
Thank you.

Perry Sugg, PG
Permitting Hydrogeologist
Division of Waste Management – Solid Waste Section
NC Department of Environmental Quality
Phone: [phone]
[e-mail]
Physical Address: 217 West Jones St / Raleigh, NC / 27603
Mailing Address: 1646 Mail Service Center / Raleigh, NC / 27699-1646
http://portal.ncdenr.org/web/wm/sw

The NC DEQ’s primary mission is to protect North Carolina's environment and natural resources.  In executing this mission, DEQ operates with the broad-
based understanding that the following three fundamental principles are integral components of its protective mandate: Fundamental Philosophy,
Fundamental Economics, and Fundamental Science.  Ultimately, a collaborative stewardship among the citizens, government regulators, and the
business community will maintain and enhance North Carolina's environment and natural resources for the benefit and enjoyment of everyone living in or
visiting our Great state.

E-mail correspondence to and from this addresss may be subject to the North Carolina Public Records Law and therefore may be disclosed to third parties.

From: Stephens, Ed [mailto:[e-mail]]
Sent: Tuesday, May 02, 2017 2:30 PM
To: Sugg, William P <[e-mail]>
Cc: John Brown <[e-mail]>; Brown, Scott <[e-mail]>
Subject: Revised Detection Groundwater & Methane Monitoring Well Relocation Map - Hwy 55 LF -
111-370.005

Perry,
Per our previous discussions, Greenway Waste Solutions of Apex, LLC (GWS) is requesting the
relocation of detection groundwater monitoring well MW-11 and adjacent landfill gas monitoring
well MM-9 in order to expand on-site road access to the compost storage area and general facility
improvements to this area at the Hwy 55 LF facility. The attached site map depicts the proposed
new well location area to the north of their existing well placements. Please note that MW-3 shown
on the map was the location of a former piezometer that has been abandoned. The new proposed
groundwater monitoring well location is optimal for detecting the locally converging groundwater
flow in this north-central area of the landfill facility. On behalf of GWS, CEC will conduct the current
required monitoring before abandoning the existing wells. With your approval, GWS would like to
abandon these existing wells ASAP to expedite the facility improvements. The well replacements will
be completed prior to the next quarterly monitoring event. Please advise.

Ed Stephens, P.G.Civil & Environmental Consultants, Inc.
1900 Center Park Drive · Suite A · Charlotte, NC 28217
Toll-Free: 855-859-9932· Fax: [phone]
Mobile: [phone] · http://www.cecinc.com
Senior Leadership · Integrated Services · Personal Business Relationships

AABB8AB3456712CDEFGH83456712ABCDEFGHDESCRIPTIONDATENO
REVISION RECORD
1 531/16 ISSUED TO NCDEQ FOR REVIEW
www.cecinc.com
1900 Center Park Drive - Suite A - Charlotte, NC 28217
Ph: 980.237.0373 · Fax: [phone]
DATE:
DWG SCALE:
DRAWN BY:
CHECKED BY:
APPROVED BY:
PROJECT NO:SHEETOFDRAWING NO.:GROUNDWATER MONITORING
WELL PLAN
111-370.003
1"=100'
MAY 2016 CTH
NTB
EHS17 20G600GREENWAY WASTE SOLUTIONS OF APEX, LLC
C&D LANDFILL PHASE III
APEX, NORTH CAROLINA NORTHREFERENCENORTH CAROLINABOARD FOR THELICENSING OFGEOLOGISTSCORPORATE LICENSENO. C-370