RA-2352_15092_CA_RMR_20151204

APPENDIX E 
Analytical Report 520193
for
Terraquest Environmental Consultants, P.C.
Project Manager: Ryan Kerins
CW Chambers Store
03-DEC-15
02794
6017 Financial Dr., Norcross, GA 30071
Ph:[phone] Fax:[phone]
Xenco-Houston (EPA Lab code: TX00122):
Texas (T104704215-15-19), Arizona (AZ0765), Florida (E871002), Louisiana (03054)
Oklahoma (9218)
Xenco-Atlanta (EPA Lab Code: GA00046):
Florida (E87429), North Carolina (483), South Carolina (98015), Kentucky (85), DoD ( L10-135)
Texas (T104704477), Louisiana (04176), USDA (P330-07-00105)
Xenco-Lakeland: Florida (E84098)
Xenco-Odessa (EPA Lab code: TX00158): Texas (T104704400-TX)
Xenco-Dallas (EPA Lab code: TX01468): Texas (T104704295-TX)
Xenco Phoenix (EPA Lab Code: AZ00901): Arizona(AZ0757)
Xenco-Phoenix Mobile (EPA Lab code: AZ00901): Arizona (AZM757)
Xenco Tucson (EPA Lab code:AZ000989): Arizona (AZ0758)
Collected By: Client
Page 1 of 67 Final 1.000

Page 2 of 67 Final 1.000
Table of Contents
Cover Page 1
Cover Letter 3
Sample ID Cross Reference 4
Explanation of Qualifiers (Flags) 5
Hits Summary 6
Certificate of Analysis (Detailed Report) 13
Summary of Quality control 51
Blank Summary 59
Chain of Custody 64
Sample Receipt Conformance Report 67
Houston - Dallas - Odessa - San Antonio - Tampa - Lakeland - Atlanta - Phoenix - Oklahoma - Latin America
Recipient of the Prestigious Small Business Administration Award of Excellence in 1994.
Certified and approved by numerous States and Agencies.
A Small Business and Minority Status Company that delivers SERVICE and QUALITY
Project Manager: Ryan Kerins
Terraquest Environmental Consultants, P.C.
100 E. Ruffin Street
Mebane, NC 27302

Reference: XENCO Report No(s): 520193
CW Chambers Store
Project Address: NC
Ryan Kerins:
We are reporting to you the results of the analyses performed on the samples received under the project name
referenced above and identified with the XENCO Report Number(s) 520193. All results being reported under
this Report Number apply to the samples analyzed and properly identified with a Laboratory ID number.
Subcontracted analyses are identified in this report with either the NELAC certification number of the
subcontract lab in the analyst ID field, or the complete subcontracted report attached to this report.
Unless otherwise noted in a Case Narrative, all data reported in this Analytical Report are in compliance with
NELAC standards. The uncertainty of measurement associated with the results of analysis reported is
available upon request. Should insufficient sample be provided to the laboratory to meet the method and
NELAC Matrix Duplicate and Matrix Spike requirements, then the data will be analyzed, evaluated and
reported using all other available quality control measures.
The validity and integrity of this report will remain intact as long as it is accompanied by this letter and
reproduced in full, unless written approval is granted by XENCO Laboratories. This report will be filed for at
least 5 years in our archives after which time it will be destroyed without further notice, unless otherwise
arranged with you. The samples received, and described as recorded in Report No. 520193 will be filed for
60 days, and after that time they will be properly disposed without further notice, unless otherwise arranged
with you. We reserve the right to return to you any unused samples, extracts or solutions related to them if we
consider so necessary (e.g., samples identified as hazardous waste, sample sizes exceeding analytical standard
practices, controlled substances under regulated protocols, etc).
We thank you for selecting XENCO Laboratories to serve your analytical needs. If you have any questions
concerning this report, please feel free to contact us at any time.
Respectfully,
03-DEC-15
Chad Bechtold
Page 3 of 67 Final 1.000
Sample Cross Reference 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
Sample Id
MW1A
MW2A
MW3
MW4
MW10
MW12
MW13
MW14
MW16
MW17
MW18
MW19
MW20
MW21
MW22
MW23
MW24
MW25
MW26
11-24-15 14:20
11-24-15 14:29
11-24-15 14:41
11-24-15 14:13
11-24-15 13:58
11-24-15 14:34
11-24-15 14:40
11-24-15 14:10
11-24-15 14:05
11-24-15 14:00
11-24-15 14:36
11-24-15 14:07
11-24-15 14:31
11-24-15 14:04
11-24-15 14:27
11-24-15 14:25
11-24-15 14:22
11-24-15 14:18
11-24-15 14:15
Date Collected Lab Sample Id
520193-001
520193-002
520193-003
520193-004
520193-005
520193-006
520193-007
520193-008
520193-009
520193-010
520193-011
520193-012
520193-013
520193-014
520193-015
520193-016
520193-017
520193-018
520193-019

Sample DepthMatrix
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
Page 4 of 67 Final 1.000
Houston - Dallas - San Antonio - Atlanta - Midland/Odessa - Tampa/Lakeland - Phoenix - Latin America
4143 Greenbriar Dr, Stafford, TX 77477
9701 Harry Hines Blvd , Dallas, TX 75220
5332 Blackberry Drive, San Antonio TX 78238
2505 North Falkenburg Rd, Tampa, FL 33619
12600 West I-20 East, Odessa, TX 79765
6017 Financial Drive, Norcross, GA 30071
3725 E. Atlanta Ave, Phoenix, AZ 85040
Phone Fax
[phone] [phone]
[phone] [phone]
[phone] [phone]
[phone] [phone]
[phone] [phone]
[phone] [phone]
[phone]
Recipient of the Prestigious Small Business Administration Award of Excellence in 1994.
Certified and approved by numerous States and Agencies.
A Small Business and Minority Status Company that delivers SERVICE and QUALITY
Flagging Criteria
X In our quality control review of the data a QC deficiency was observed and flagged as noted. MS/MSD recoveries were found to be
outside of the laboratory control limits due to possible matrix /chemical interference, or a concentration of target analyte high enough
to affect the recovery of the spike concentration. This condition could also affect the relative percent difference in the MS/MSD.
B A target analyte or common laboratory contaminant was identified in the method blank. Its presence indicates possible field or
laboratory contamination.
D The sample(s) were diluted due to targets detected over the highest point of the calibration curve, or due to matrix interference.
Dilution factors are included in the final results. The result is from a diluted sample.
E The data exceeds the upper calibration limit; therefore, the concentration is reported as estimated.
F RPD exceeded lab control limits.
J The target analyte was positively identified below the quantitation limit and above the detection limit.
U Analyte was not detected.
L The LCS data for this analytical batch was reported below the laboratory control limits for this analyte. The department supervisor and
QA Director reviewed data. The samples were either reanalyzed or flagged as estimated concentrations.
H The LCS data for this analytical batch was reported above the laboratory control limits. Supporting QC Data were reviewed by the
Department Supervisor and QA Director. Data were determined to be valid for reporting.
K Sample analyzed outside of recommended hold time.
JN A combination of the "N" and the "J" qualifier. The analysis indicates that the analyte is "tentatively identified" and the associated
numerical value may not be consistent with the amount actually present in the environmental sample.
** Surrogate recovered outside laboratory control limit.
BRL Below Reporting Limit.
RL Reporting Limit
MDL Method Detection Limit SDL Sample Detection Limit LOD Limit of Detection
PQL Practical Quantitation Limit MQL Method Quantitation Limit LOQ Limit of Quantitation
DL Method Detection Limit
NC Non-Calculable
+ NELAC certification not offered for this compound.

* (Next to analyte name or method description) = Outside XENCO's scope of NELAC accreditation
Page 5 of 67 Final 1.000
Hits Summary 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42
11.25.15 09.42
Date Received :
Date Received :
% Moisture :
% Moisture :
11.24.15 14.20
11.24.15 14.29
Date Collected :
Date Collected :
520193-001
520193-002
Lab Sample Id :
Lab Sample Id :
Ground Water
Ground Water
Matrix :
Matrix :
MW1A
MW2A
Sample Id :
Sample Id :
VOCs by GC/MS by SM6200B
VOCs by GC/MS by SM6200B
Analytical Method :
Analytical Method :
SM6200B_PREP
SM6200B_PREP
Prep Method:
Prep Method:
11.30.15 06.34
11.30.15 06.34
Date Prep:
Date Prep:
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Acetone
Benzene
Ethylbenzene
Isopropyl ether
Methyl tert-butyl ether (MTBE)
Naphthalene
n-Propylbenzene
Toluene
m,p-Xylenes
o-Xylene
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Benzene
Ethylbenzene
Isopropyl ether
Methyl tert-butyl ether (MTBE)
Naphthalene
Toluene
m,p-Xylenes
o-Xylene
Parameter
Parameter
Result
Result
D
Flag
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
Units
100
100
100
500
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
Dil
Dil
Cas Number
Cas Number
95-63-6
108-67-8
67-64-1
71-43-2
100-41-4
108-20-3
1634-04-4
91-20-3
103-65-1
108-88-3
179601-23-1
95-47-6
95-63-6
108-67-8
71-43-2
100-41-4
108-20-3
1634-04-4
91-20-3
108-88-3
179601-23-1
95-47-6
1750
492
832
9260
1910
500
190
457
123
8760
6940
3360
545
228
282
122
177
577
580
2200
2310
1680
982462
982462
Seq Number
Seq Number
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 16.28
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
Analysis Date
Analysis Date
Page 6 of 67 Final 1.000
Hits Summary 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42
11.25.15 09.42
Date Received :
Date Received :
% Moisture :
% Moisture :
11.24.15 13.58
11.24.15 14.10
Date Collected :
Date Collected :
520193-005
520193-008
Lab Sample Id :
Lab Sample Id :
Ground Water
Ground Water
Matrix :
Matrix :
MW10
MW14
Sample Id :
Sample Id :
VOCs by GC/MS by SM6200B
VOCs by GC/MS by SM6200B
Analytical Method :
Analytical Method :
SM6200B_PREP
SM6200B_PREP
Prep Method:
Prep Method:
11.29.15 15.31
11.29.15 15.31
Date Prep:
Date Prep:
Isopropyl ether
Methyl tert-butyl ether (MTBE)
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
4-Isopropyltoluene
Ethylbenzene
Isopropylbenzene
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
m,p-Xylenes
o-Xylene
Parameter
Parameter
Result
Result
J
Flag
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
Dil
Dil
Cas Number
Cas Number
108-20-3
1634-04-4
95-63-6
108-67-8
99-87-6
100-41-4
98-82-8
91-20-3
104-51-8
103-65-1
135-98-8
179601-23-1
95-47-6
6.75
46.0
13.9
0.920
0.540
0.320
1.79
2.97
2.29
1.65
0.960
8.06
8.87
982296
982296
Seq Number
Seq Number
11.29.15 21.03
11.29.15 21.03
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
Analysis Date
Analysis Date
Page 7 of 67 Final 1.000
Hits Summary 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received :
% Moisture :
11.24.15 14.31 Date Collected : 520193-013Lab Sample Id :
Ground WaterMatrix : MW20Sample Id :
VOCs by GC/MS by SM6200B
VOCs by GC/MS by SM6200B
Analytical Method :
Analytical Method :
SM6200B_PREP
SM6200B_PREP
Prep Method:
Prep Method:
11.30.15 06.34
12.01.15 11.42
Date Prep:
Date Prep:
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Naphthalene
n-Propylbenzene
Styrene
Toluene
o-Xylene
Benzene
Ethylbenzene
m,p-Xylenes
Parameter
Parameter
Result
Result
D
D
D
Flag
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
Units
5
5
5
5
5
5
5
5
5
5
50
50
50
Dil
Dil
Cas Number
Cas Number
95-63-6
108-67-8
108-20-3
98-82-8
1634-04-4
91-20-3
103-65-1
100-42-5
108-88-3
95-47-6
71-43-2
100-41-4
179601-23-1
342
102
47.5
26.8
126
247
63.1
9.60
100
57.6
1470
551
989
982462
982462
Seq Number
Seq Number
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
12.01.15 15.59
12.01.15 15.59
12.01.15 15.59
Analysis Date
Analysis Date
Page 8 of 67 Final 1.000
Hits Summary 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received :
% Moisture :
11.24.15 14.04 Date Collected : 520193-014Lab Sample Id :
Ground WaterMatrix : MW21Sample Id :
VOCs by GC/MS by SM6200B
VOCs by GC/MS by SM6200B
Analytical Method :
Analytical Method :
SM6200B_PREP
SM6200B_PREP
Prep Method:
Prep Method:
11.29.15 15.31
11.30.15 06.34
Date Prep:
Date Prep:
1,3,5-Trimethylbenzene
4-Isopropyltoluene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
1,2,4-Trimethylbenzene
Benzene
Ethylbenzene
Naphthalene
Toluene
m,p-Xylenes
o-Xylene
Parameter
Parameter
Result
Result
D
D
D
D
D
D
D
Flag
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
Units
1
1
1
1
1
1
1
1
1
50
50
50
50
50
50
50
Dil
Dil
Cas Number
Cas Number
108-67-8
99-87-6
108-20-3
98-82-8
1634-04-4
104-51-8
103-65-1
135-98-8
100-42-5
95-63-6
71-43-2
100-41-4
91-20-3
108-88-3
179601-23-1
95-47-6
45.9
1.92
24.3
16.2
17.3
8.66
32.0
2.53
5.78
178
1720
279
334
351
369
125
982296
982296
Seq Number
Seq Number
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 11.12
11.30.15 11.12
11.30.15 11.12
11.30.15 11.12
11.30.15 11.12
11.30.15 11.12
11.30.15 11.12
Analysis Date
Analysis Date
Page 9 of 67 Final 1.000
Hits Summary 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42
11.25.15 09.42
Date Received :
Date Received :
% Moisture :
% Moisture :
11.24.15 14.27
11.24.15 14.25
Date Collected :
Date Collected :
520193-015
520193-016
Lab Sample Id :
Lab Sample Id :
Ground Water
Ground Water
Matrix :
Matrix :
MW22
MW23
Sample Id :
Sample Id :
VOCs by GC/MS by SM6200B
VOCs by GC/MS by SM6200B
Analytical Method :
Analytical Method :
SM6200B_PREP
SM6200B_PREP
Prep Method:
Prep Method:
11.30.15 06.34
11.30.15 06.34
Date Prep:
Date Prep:
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Benzene
Ethylbenzene
Methylene Chloride
Naphthalene
n-Propylbenzene
Styrene
Toluene
m,p-Xylenes
o-Xylene
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Acetone
Benzene
Ethylbenzene
Isopropyl ether
Methyl tert-butyl ether (MTBE)
Naphthalene
n-Propylbenzene
Styrene
Toluene
m,p-Xylenes
o-Xylene
Parameter
Parameter
Result
Result
D
J
D
D
Flag
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
Units
100
100
100
100
100
100
100
100
500
100
100
100
100
100
500
100
100
100
100
100
100
500
100
100
Dil
Dil
Cas Number
Cas Number
95-63-6
108-67-8
71-43-2
100-41-4
75-09-2
91-20-3
103-65-1
100-42-5
108-88-3
179601-23-1
95-47-6
95-63-6
108-67-8
67-64-1
71-43-2
100-41-4
108-20-3
1634-04-4
91-20-3
103-65-1
100-42-5
108-88-3
179601-23-1
95-47-6
2770
628
2050
1540
117
1610
103
253
25600
9160
4810
2000
491
110
23100
2540
825
717
1120
231
105
26700
9540
4480
982462
982462
Seq Number
Seq Number
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 16.59
11.30.15 14.17
11.30.15 14.17
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 17.30
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 17.30
11.30.15 14.50
11.30.15 14.50
Analysis Date
Analysis Date
Page 10 of 67 Final 1.000
Hits Summary 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42
11.25.15 09.42
Date Received :
Date Received :
% Moisture :
% Moisture :
11.24.15 14.22
11.24.15 14.18
Date Collected :
Date Collected :
520193-017
520193-018
Lab Sample Id :
Lab Sample Id :
Ground Water
Ground Water
Matrix :
Matrix :
MW24
MW25
Sample Id :
Sample Id :
VOCs by GC/MS by SM6200B
VOCs by GC/MS by SM6200B
Analytical Method :
Analytical Method :
SM6200B_PREP
SM6200B_PREP
Prep Method:
Prep Method:
11.30.15 06.34
11.30.15 06.34
Date Prep:
Date Prep:
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
2-Butanone (MEK)
Acetone
Benzene
Ethylbenzene
Isopropyl ether
Methyl tert-butyl ether (MTBE)
Naphthalene
n-Propylbenzene
Toluene
m,p-Xylenes
o-Xylene
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Benzene
Ethylbenzene
Naphthalene
n-Propylbenzene
Toluene
m,p-Xylenes
o-Xylene
Parameter
Parameter
Result
Result
D
D
Flag
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
Units
100
100
100
100
500
100
100
100
100
100
500
100
100
100
100
100
100
100
100
100
100
100
Dil
Dil
Cas Number
Cas Number
95-63-6
108-67-8
78-93-3
67-64-1
71-43-2
100-41-4
108-20-3
1634-04-4
91-20-3
103-65-1
108-88-3
179601-23-1
95-47-6
95-63-6
108-67-8
71-43-2
100-41-4
91-20-3
103-65-1
108-88-3
179601-23-1
95-47-6
2480
557
4300
486
18700
2420
2090
4780
1460
219
31500
10100
4980
2690
705
149
989
745
211
1950
4430
2910
982462
982462
Seq Number
Seq Number
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 18.01
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 18.01
11.30.15 15.23
11.30.15 15.23
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
Analysis Date
Analysis Date
Page 11 of 67 Final 1.000
Hits Summary 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received :
% Moisture :
11.24.15 14.15 Date Collected : 520193-019Lab Sample Id :
Ground WaterMatrix : MW26Sample Id :
VOCs by GC/MS by SM6200B
VOCs by GC/MS by SM6200B
Analytical Method :
Analytical Method :
SM6200B_PREP
SM6200B_PREP
Prep Method:
Prep Method:
11.30.15 06.34
12.01.15 11.42
Date Prep:
Date Prep:
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichloroethane
1,3,5-Trimethylbenzene
2-Butanone (MEK)
Benzene
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Naphthalene
n-Propylbenzene
m,p-Xylenes
o-Xylene
Toluene
Parameter
Parameter
Result
Result
J
D
Flag
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
Units
100
100
100
100
100
100
100
100
100
100
100
100
100
100
500
Dil
Dil
Cas Number
Cas Number
95-63-6
106-93-4
107-06-2
108-67-8
78-93-3
71-43-2
100-41-4
108-20-3
98-82-8
1634-04-4
91-20-3
103-65-1
179601-23-1
95-47-6
108-88-3
2820
209
329
699
799
7810
3640
707
111
185
1340
342
13500
6290
28100
982462
982462
Seq Number
Seq Number
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
12.01.15 14.32
Analysis Date
Analysis Date
Page 12 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.20 Date Collected:520193-001Lab Sample Id:
Ground WaterMatrix: MW1ASample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.30.15 06.34 Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
18.0
7.60
7.00
11.3
12.1
10.4
6.00
11.8
13.8
6.90
10.3
18.0
9.40
9.00
12.2
8.70
9.80
13.3
6.70
9.70
37.8
8.80
35.2
9.00
8.90
25.3
35.2
59.5
13.2
11.2
12.4
15.9
9.70
9.90
10.5
17.7
4.20
17.2
8.50
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
D
U
U
U
U
U
U
U
U
U
U
U
100
50.0
50.0
50.0
50.0
50.0
50.0
200
100
100
50.0
100
50.0
50.0
50.0
50.0
50.0
50.0
50.0
20.0
2000
20.0
40.0
50.0
50.0
40.0
200
250
50.0
50.0
50.0
200
100
50.0
50.0
50.0
50.0
50.0
50.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
500
100
100
100
100
100
100
100
100
100
100
100
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
1750
U
U
U
U
492
U
U
U
U
U
U
U
U
U
U
832
9260
U
U
U
U
U
U
U
U
U
U
U
982462Seq Number:
RL MDL
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 16.28
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
Analysis Date
% Moisture:
Page 13 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.20 Date Collected:520193-001Lab Sample Id:
Ground WaterMatrix: MW1ASample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.30.15 06.34 Date Prep:
MWETech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
11.4
10.0
6.70
300
9.20
9.20
9.80
16.9
19.0
9.40
6.00
6.50
9.20
7.40
8.90
5.40
5.70
18.8
11.0
13.9
5.40
72.0
8.10
17.6
12.2
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
50.0
100
100
5000
50.0
50.0
50.0
50.0
50.0
200
200
100
50.0
50.0
50.0
50.0
50.0
50.0
100
50.0
50.0
100
50.0
100
50.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
1910
500
U
190
U
457
U
123
U
U
U
U
8760
U
U
U
U
U
U
6940
3360
982462Seq Number:
RL MDL
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
94
102
102
11.30.15 13.10
11.30.15 13.10
11.30.15 13.10
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 14 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.29 Date Collected:520193-002Lab Sample Id:
Ground WaterMatrix: MW2ASample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.30.15 06.34 Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
18.0
7.60
7.00
11.3
12.1
10.4
6.00
11.8
13.8
6.90
10.3
18.0
9.40
9.00
12.2
8.70
9.80
13.3
6.70
9.70
37.8
8.80
35.2
9.00
8.90
25.3
35.2
11.9
13.2
11.2
12.4
15.9
9.70
9.90
10.5
17.7
4.20
17.2
8.50
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
100
50.0
50.0
50.0
50.0
50.0
50.0
200
100
100
50.0
100
50.0
50.0
50.0
50.0
50.0
50.0
50.0
20.0
2000
20.0
40.0
50.0
50.0
40.0
200
50.0
50.0
50.0
50.0
200
100
50.0
50.0
50.0
50.0
50.0
50.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
545
U
U
U
U
228
U
U
U
U
U
U
U
U
U
U
U
282
U
U
U
U
U
U
U
U
U
U
U
982462Seq Number:
RL MDL
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
Analysis Date
% Moisture:
Page 15 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.29 Date Collected:520193-002Lab Sample Id:
Ground WaterMatrix: MW2ASample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.30.15 06.34 Date Prep:
MWETech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
11.4
10.0
6.70
300
9.20
9.20
9.80
16.9
19.0
9.40
6.00
6.50
9.20
7.40
8.90
5.40
5.70
18.8
11.0
13.9
5.40
72.0
8.10
17.6
12.2
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
50.0
100
100
5000
50.0
50.0
50.0
50.0
50.0
200
200
100
50.0
50.0
50.0
50.0
50.0
50.0
100
50.0
50.0
100
50.0
100
50.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
122
177
U
577
U
580
U
U
U
U
U
U
2200
U
U
U
U
U
U
2310
1680
982462Seq Number:
RL MDL
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
96
102
100
11.30.15 13.44
11.30.15 13.44
11.30.15 13.44
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 16 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.41 Date Collected:520193-003Lab Sample Id:
Ground WaterMatrix: MW3Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.29.15 15.31 Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
0.400
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982296Seq Number:
RL MDL
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
Analysis Date
% Moisture:
Page 17 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.41 Date Collected:520193-003Lab Sample Id:
Ground WaterMatrix: MW3Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.29.15 15.31 Date Prep:
MWETech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
0.114
0.100
0.0670
3.00
0.0920
0.0920
0.0980
0.169
0.190
0.0940
0.0600
0.0650
0.0920
0.0740
0.0890
0.0540
0.0570
0.188
0.110
0.139
0.0540
0.720
0.0810
0.176
0.122
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.500
1.00
1.00
50.0
0.500
0.500
0.500
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982296Seq Number:
RL MDL
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
102
106
108
11.29.15 20.36
11.29.15 20.36
11.29.15 20.36
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 18 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.13 Date Collected:520193-004Lab Sample Id:
Ground WaterMatrix: MW4Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.30.15 06.34 Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
0.400
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982462Seq Number:
RL MDL
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
Analysis Date
% Moisture:
Page 19 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.13 Date Collected:520193-004Lab Sample Id:
Ground WaterMatrix: MW4Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.30.15 06.34 Date Prep:
MWETech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
0.114
0.100
0.0670
3.00
0.0920
0.0920
0.0980
0.169
0.190
0.0940
0.0600
0.0650
0.0920
0.0740
0.0890
0.0540
0.0570
0.188
0.110
0.139
0.0540
0.720
0.0810
0.176
0.122
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.500
1.00
1.00
50.0
0.500
0.500
0.500
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982462Seq Number:
RL MDL
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
103
102
102
11.30.15 18.33
11.30.15 18.33
11.30.15 18.33
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 20 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 13.58 Date Collected:520193-005Lab Sample Id:
Ground WaterMatrix: MW10Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.29.15 15.31 Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
0.400
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982296Seq Number:
RL MDL
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
Analysis Date
% Moisture:
Page 21 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 13.58 Date Collected:520193-005Lab Sample Id:
Ground WaterMatrix: MW10Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.29.15 15.31 Date Prep:
MWETech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
0.114
0.100
0.0670
3.00
0.0920
0.0920
0.0980
0.169
0.190
0.0940
0.0600
0.0650
0.0920
0.0740
0.0890
0.0540
0.0570
0.188
0.110
0.139
0.0540
0.720
0.0810
0.176
0.122
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.500
1.00
1.00
50.0
0.500
0.500
0.500
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
U
6.75
U
46.0
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982296Seq Number:
RL MDL
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
102
103
108
11.29.15 21.03
11.29.15 21.03
11.29.15 21.03
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 22 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.34 Date Collected:520193-006Lab Sample Id:
Ground WaterMatrix: MW12Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.29.15 15.31 Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
0.400
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982296Seq Number:
RL MDL
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
Analysis Date
% Moisture:
Page 23 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.34 Date Collected:520193-006Lab Sample Id:
Ground WaterMatrix: MW12Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.29.15 15.31 Date Prep:
MWETech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
0.114
0.100
0.0670
3.00
0.0920
0.0920
0.0980
0.169
0.190
0.0940
0.0600
0.0650
0.0920
0.0740
0.0890
0.0540
0.0570
0.188
0.110
0.139
0.0540
0.720
0.0810
0.176
0.122
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.500
1.00
1.00
50.0
0.500
0.500
0.500
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982296Seq Number:
RL MDL
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
102
102
104
11.29.15 21.29
11.29.15 21.29
11.29.15 21.29
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 24 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.40 Date Collected:520193-007Lab Sample Id:
Ground WaterMatrix: MW13Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.29.15 15.31 Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
0.400
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982296Seq Number:
RL MDL
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
Analysis Date
% Moisture:
Page 25 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.40 Date Collected:520193-007Lab Sample Id:
Ground WaterMatrix: MW13Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.29.15 15.31 Date Prep:
MWETech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
0.114
0.100
0.0670
3.00
0.0920
0.0920
0.0980
0.169
0.190
0.0940
0.0600
0.0650
0.0920
0.0740
0.0890
0.0540
0.0570
0.188
0.110
0.139
0.0540
0.720
0.0810
0.176
0.122
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.500
1.00
1.00
50.0
0.500
0.500
0.500
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982296Seq Number:
RL MDL
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
106
103
107
11.29.15 21.56
11.29.15 21.56
11.29.15 21.56
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 26 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.10 Date Collected:520193-008Lab Sample Id:
Ground WaterMatrix: MW14Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.29.15 15.31 Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
0.400
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
13.9
U
U
U
U
0.920
U
U
U
U
U
U
U
U
0.540
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982296Seq Number:
RL MDL
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
Analysis Date
% Moisture:
Page 27 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.10 Date Collected:520193-008Lab Sample Id:
Ground WaterMatrix: MW14Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.29.15 15.31 Date Prep:
MWETech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
0.114
0.100
0.0670
3.00
0.0920
0.0920
0.0980
0.169
0.190
0.0940
0.0600
0.0650
0.0920
0.0740
0.0890
0.0540
0.0570
0.188
0.110
0.139
0.0540
0.720
0.0810
0.176
0.122
Result
U
U
U
U
J
U
U
U
U
U
U
U
U
U
U
U
U
U
0.500
1.00
1.00
50.0
0.500
0.500
0.500
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
0.320
U
1.79
U
U
2.97
2.29
1.65
0.960
U
U
U
U
U
U
U
U
U
U
8.06
8.87
982296Seq Number:
RL MDL
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
108
101
108
11.29.15 22.23
11.29.15 22.23
11.29.15 22.23
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 28 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.05 Date Collected:520193-009Lab Sample Id:
Ground WaterMatrix: MW16Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.29.15 15.31 Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
0.400
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982296Seq Number:
RL MDL
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
Analysis Date
% Moisture:
Page 29 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.05 Date Collected:520193-009Lab Sample Id:
Ground WaterMatrix: MW16Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.29.15 15.31 Date Prep:
MWETech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
0.114
0.100
0.0670
3.00
0.0920
0.0920
0.0980
0.169
0.190
0.0940
0.0600
0.0650
0.0920
0.0740
0.0890
0.0540
0.0570
0.188
0.110
0.139
0.0540
0.720
0.0810
0.176
0.122
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.500
1.00
1.00
50.0
0.500
0.500
0.500
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982296Seq Number:
RL MDL
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
104
106
109
11.29.15 22.50
11.29.15 22.50
11.29.15 22.50
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 30 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.00 Date Collected:520193-010Lab Sample Id:
Ground WaterMatrix: MW17Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.29.15 15.31 Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
0.400
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982296Seq Number:
RL MDL
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
Analysis Date
% Moisture:
Page 31 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.00 Date Collected:520193-010Lab Sample Id:
Ground WaterMatrix: MW17Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.29.15 15.31 Date Prep:
MWETech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
0.114
0.100
0.0670
3.00
0.0920
0.0920
0.0980
0.169
0.190
0.0940
0.0600
0.0650
0.0920
0.0740
0.0890
0.0540
0.0570
0.188
0.110
0.139
0.0540
0.720
0.0810
0.176
0.122
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.500
1.00
1.00
50.0
0.500
0.500
0.500
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982296Seq Number:
RL MDL
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
106
103
104
11.29.15 23.16
11.29.15 23.16
11.29.15 23.16
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 32 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.36 Date Collected:520193-011Lab Sample Id:
Ground WaterMatrix: MW18Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.29.15 15.31 Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
0.400
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982296Seq Number:
RL MDL
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
Analysis Date
% Moisture:
Page 33 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.36 Date Collected:520193-011Lab Sample Id:
Ground WaterMatrix: MW18Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.29.15 15.31 Date Prep:
MWETech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
0.114
0.100
0.0670
3.00
0.0920
0.0920
0.0980
0.169
0.190
0.0940
0.0600
0.0650
0.0920
0.0740
0.0890
0.0540
0.0570
0.188
0.110
0.139
0.0540
0.720
0.0810
0.176
0.122
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.500
1.00
1.00
50.0
0.500
0.500
0.500
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982296Seq Number:
RL MDL
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
104
105
109
11.30.15 00.10
11.30.15 00.10
11.30.15 00.10
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 34 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.07 Date Collected:520193-012Lab Sample Id:
Ground WaterMatrix: MW19Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.29.15 15.31 Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
0.400
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982296Seq Number:
RL MDL
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
Analysis Date
% Moisture:
Page 35 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.07 Date Collected:520193-012Lab Sample Id:
Ground WaterMatrix: MW19Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.29.15 15.31 Date Prep:
MWETech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
0.114
0.100
0.0670
3.00
0.0920
0.0920
0.0980
0.169
0.190
0.0940
0.0600
0.0650
0.0920
0.0740
0.0890
0.0540
0.0570
0.188
0.110
0.139
0.0540
0.720
0.0810
0.176
0.122
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.500
1.00
1.00
50.0
0.500
0.500
0.500
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982296Seq Number:
RL MDL
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
108
103
109
11.29.15 23.43
11.29.15 23.43
11.29.15 23.43
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 36 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.31 Date Collected:520193-013Lab Sample Id:
Ground WaterMatrix: MW20Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.30.15 06.34 Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
0.900
0.380
0.350
0.565
0.605
0.520
0.300
0.590
0.690
0.345
0.515
0.900
0.470
0.450
0.610
0.435
0.490
0.665
0.335
0.485
1.89
0.440
1.76
0.450
0.445
1.27
1.76
5.95
0.660
0.560
0.620
0.795
0.485
0.495
0.525
0.885
0.210
0.860
0.425
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
D
U
U
U
U
U
U
U
U
U
U
U
5.00
2.50
2.50
2.50
2.50
2.50
2.50
10.0
5.00
5.00
2.50
5.00
2.50
2.50
2.50
2.50
2.50
2.50
2.50
1.00
100
1.00
2.00
2.50
2.50
2.00
10.0
25.0
2.50
2.50
2.50
10.0
5.00
2.50
2.50
2.50
2.50
2.50
2.50
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
50
5
5
5
5
5
5
5
5
5
5
5
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
342
U
U
U
U
102
U
U
U
U
U
U
U
U
U
U
U
1470
U
U
U
U
U
U
U
U
U
U
U
982462Seq Number:
RL MDL
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
12.01.15 15.59
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
Analysis Date
% Moisture:
Page 37 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.31 Date Collected:520193-013Lab Sample Id:
Ground WaterMatrix: MW20Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.30.15 06.34 Date Prep:
MWETech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
0.570
0.500
0.335
15.0
4.60
0.460
0.490
0.845
0.950
0.470
0.300
0.325
0.460
0.370
0.445
0.270
0.285
0.940
0.550
0.695
0.270
3.60
0.405
8.80
0.610
Result
U
U
U
U
D
U
U
U
U
U
U
U
U
U
U
U
D
2.50
5.00
5.00
250
25.0
2.50
2.50
2.50
2.50
10.0
10.0
5.00
2.50
2.50
2.50
2.50
2.50
2.50
5.00
2.50
2.50
5.00
2.50
50.0
2.50
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
5
5
5
5
50
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
50
5
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
551
47.5
26.8
126
U
247
U
63.1
U
9.60
U
U
100
U
U
U
U
U
U
989
57.6
982462Seq Number:
RL MDL
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
12.01.15 15.59
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
12.01.15 15.59
11.30.15 10.44
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
100
101
104
11.30.15 10.44
11.30.15 10.44
11.30.15 10.44
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 38 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.04 Date Collected:520193-014Lab Sample Id:
Ground WaterMatrix: MW21Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.29.15 15.31 Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
5.15
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
5.95
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
Result
U
U
U
U
U
U
U
U
U
U
D
U
U
U
U
U
U
U
U
U
U
U
U
U
U
D
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
25.0
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
0.400
2.00
25.0
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
50
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
50
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
178
U
U
U
U
45.9
U
U
U
U
U
U
U
U
1.92
U
U
1720
U
U
U
U
U
U
U
U
U
U
U
982296Seq Number:
RL MDL
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 11.12
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 11.12
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
Analysis Date
% Moisture:
Page 39 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.04 Date Collected:520193-014Lab Sample Id:
Ground WaterMatrix: MW21Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.29.15 15.31 Date Prep:
MWETech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
0.114
0.100
0.0670
3.00
4.60
0.0920
0.0980
0.169
0.190
4.70
0.0600
0.0650
0.0920
0.0740
0.0890
0.0540
2.85
0.188
0.110
0.139
0.0540
0.720
0.0810
8.80
6.10
Result
U
U
U
U
D
U
D
U
U
D
U
U
U
U
U
U
D
D
0.500
1.00
1.00
50.0
25.0
0.500
0.500
0.500
0.500
100
2.00
1.00
0.500
0.500
0.500
0.500
25.0
0.500
1.00
0.500
0.500
1.00
0.500
50.0
25.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
50
1
1
1
1
50
1
1
1
1
1
1
50
1
1
1
1
1
1
50
50
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
279
24.3
16.2
17.3
U
334
8.66
32.0
2.53
5.78
U
U
351
U
U
U
U
U
U
369
125
982296Seq Number:
RL MDL
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 11.12
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 11.12
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 11.12
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
11.30.15 11.12
11.30.15 11.12
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
126
101
104
11.30.15 00.37
11.30.15 00.37
11.30.15 00.37
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 40 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.27 Date Collected:520193-015Lab Sample Id:
Ground WaterMatrix: MW22Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.30.15 06.34 Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
18.0
7.60
7.00
11.3
12.1
10.4
6.00
11.8
13.8
6.90
10.3
18.0
9.40
9.00
12.2
8.70
9.80
13.3
6.70
9.70
37.8
8.80
35.2
9.00
8.90
25.3
35.2
11.9
13.2
11.2
12.4
15.9
9.70
9.90
10.5
17.7
4.20
17.2
8.50
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
100
50.0
50.0
50.0
50.0
50.0
50.0
200
100
100
50.0
100
50.0
50.0
50.0
50.0
50.0
50.0
50.0
20.0
2000
20.0
40.0
50.0
50.0
40.0
200
50.0
50.0
50.0
50.0
200
100
50.0
50.0
50.0
50.0
50.0
50.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
2770
U
U
U
U
628
U
U
U
U
U
U
U
U
U
U
U
2050
U
U
U
U
U
U
U
U
U
U
U
982462Seq Number:
RL MDL
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
Analysis Date
% Moisture:
Page 41 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.27 Date Collected:520193-015Lab Sample Id:
Ground WaterMatrix: MW22Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.30.15 06.34 Date Prep:
MWETech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
11.4
10.0
6.70
300
9.20
9.20
9.80
16.9
19.0
9.40
6.00
6.50
9.20
7.40
8.90
5.40
28.5
18.8
11.0
13.9
5.40
72.0
8.10
17.6
12.2
Result
U
U
U
U
U
U
U
U
U
U
U
D
U
U
U
U
U
U
50.0
100
100
5000
50.0
50.0
50.0
50.0
50.0
200
200
100
50.0
50.0
50.0
50.0
250
50.0
100
50.0
50.0
100
50.0
100
50.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
500
100
100
100
100
100
100
100
100
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
1540
U
U
U
117
1610
U
103
U
253
U
U
25600
U
U
U
U
U
U
9160
4810
982462Seq Number:
RL MDL
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 16.59
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
97
99
102
11.30.15 14.17
11.30.15 14.17
11.30.15 14.17
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 42 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.25 Date Collected:520193-016Lab Sample Id:
Ground WaterMatrix: MW23Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.30.15 06.34 Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
18.0
7.60
7.00
11.3
12.1
10.4
6.00
11.8
13.8
6.90
10.3
18.0
9.40
9.00
12.2
8.70
9.80
13.3
6.70
9.70
37.8
8.80
35.2
9.00
8.90
25.3
35.2
59.5
13.2
11.2
12.4
15.9
9.70
9.90
10.5
17.7
4.20
17.2
8.50
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
J
D
U
U
U
U
U
U
U
U
U
U
U
100
50.0
50.0
50.0
50.0
50.0
50.0
200
100
100
50.0
100
50.0
50.0
50.0
50.0
50.0
50.0
50.0
20.0
2000
20.0
40.0
50.0
50.0
40.0
200
250
50.0
50.0
50.0
200
100
50.0
50.0
50.0
50.0
50.0
50.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
500
100
100
100
100
100
100
100
100
100
100
100
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
2000
U
U
U
U
491
U
U
U
U
U
U
U
U
U
U
110
23100
U
U
U
U
U
U
U
U
U
U
U
982462Seq Number:
RL MDL
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 17.30
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
Analysis Date
% Moisture:
Page 43 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.25 Date Collected:520193-016Lab Sample Id:
Ground WaterMatrix: MW23Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.30.15 06.34 Date Prep:
MWETech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
11.4
10.0
6.70
300
9.20
9.20
9.80
16.9
19.0
9.40
6.00
6.50
9.20
7.40
8.90
5.40
28.5
18.8
11.0
13.9
5.40
72.0
8.10
17.6
12.2
Result
U
U
U
U
U
U
U
U
U
U
D
U
U
U
U
U
U
50.0
100
100
5000
50.0
50.0
50.0
50.0
50.0
200
200
100
50.0
50.0
50.0
50.0
250
50.0
100
50.0
50.0
100
50.0
100
50.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
500
100
100
100
100
100
100
100
100
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
2540
825
U
717
U
1120
U
231
U
105
U
U
26700
U
U
U
U
U
U
9540
4480
982462Seq Number:
RL MDL
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 17.30
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
98
100
103
11.30.15 14.50
11.30.15 14.50
11.30.15 14.50
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 44 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.22 Date Collected:520193-017Lab Sample Id:
Ground WaterMatrix: MW24Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.30.15 06.34 Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
18.0
7.60
7.00
11.3
12.1
10.4
6.00
11.8
13.8
6.90
10.3
18.0
9.40
9.00
12.2
8.70
9.80
13.3
6.70
9.70
37.8
8.80
35.2
9.00
8.90
25.3
35.2
59.5
13.2
11.2
12.4
15.9
9.70
9.90
10.5
17.7
4.20
17.2
8.50
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
D
U
U
U
U
U
U
U
U
U
U
U
100
50.0
50.0
50.0
50.0
50.0
50.0
200
100
100
50.0
100
50.0
50.0
50.0
50.0
50.0
50.0
50.0
20.0
2000
20.0
40.0
50.0
50.0
40.0
200
250
50.0
50.0
50.0
200
100
50.0
50.0
50.0
50.0
50.0
50.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
500
100
100
100
100
100
100
100
100
100
100
100
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
2480
U
U
U
U
557
U
U
U
U
4300
U
U
U
U
U
486
18700
U
U
U
U
U
U
U
U
U
U
U
982462Seq Number:
RL MDL
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 18.01
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
Analysis Date
% Moisture:
Page 45 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.22 Date Collected:520193-017Lab Sample Id:
Ground WaterMatrix: MW24Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.30.15 06.34 Date Prep:
MWETech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
11.4
10.0
6.70
300
9.20
9.20
9.80
16.9
19.0
9.40
6.00
6.50
9.20
7.40
8.90
5.40
28.5
18.8
11.0
13.9
5.40
72.0
8.10
17.6
12.2
Result
U
U
U
U
U
U
U
U
U
U
U
D
U
U
U
U
U
U
50.0
100
100
5000
50.0
50.0
50.0
50.0
50.0
200
200
100
50.0
50.0
50.0
50.0
250
50.0
100
50.0
50.0
100
50.0
100
50.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
500
100
100
100
100
100
100
100
100
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
2420
2090
U
4780
U
1460
U
219
U
U
U
U
31500
U
U
U
U
U
U
10100
4980
982462Seq Number:
RL MDL
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 18.01
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
96
99
104
11.30.15 15.23
11.30.15 15.23
11.30.15 15.23
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 46 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.18 Date Collected:520193-018Lab Sample Id:
Ground WaterMatrix: MW25Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.30.15 06.34 Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
18.0
7.60
7.00
11.3
12.1
10.4
6.00
11.8
13.8
6.90
10.3
18.0
9.40
9.00
12.2
8.70
9.80
13.3
6.70
9.70
37.8
8.80
35.2
9.00
8.90
25.3
35.2
11.9
13.2
11.2
12.4
15.9
9.70
9.90
10.5
17.7
4.20
17.2
8.50
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
100
50.0
50.0
50.0
50.0
50.0
50.0
200
100
100
50.0
100
50.0
50.0
50.0
50.0
50.0
50.0
50.0
20.0
2000
20.0
40.0
50.0
50.0
40.0
200
50.0
50.0
50.0
50.0
200
100
50.0
50.0
50.0
50.0
50.0
50.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
2690
U
U
U
U
705
U
U
U
U
U
U
U
U
U
U
U
149
U
U
U
U
U
U
U
U
U
U
U
982462Seq Number:
RL MDL
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
Analysis Date
% Moisture:
Page 47 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.18 Date Collected:520193-018Lab Sample Id:
Ground WaterMatrix: MW25Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.30.15 06.34 Date Prep:
MWETech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
11.4
10.0
6.70
300
9.20
9.20
9.80
16.9
19.0
9.40
6.00
6.50
9.20
7.40
8.90
5.40
5.70
18.8
11.0
13.9
5.40
72.0
8.10
17.6
12.2
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
50.0
100
100
5000
50.0
50.0
50.0
50.0
50.0
200
200
100
50.0
50.0
50.0
50.0
50.0
50.0
100
50.0
50.0
100
50.0
100
50.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
989
U
U
U
U
745
U
211
U
U
U
U
1950
U
U
U
U
U
U
4430
2910
982462Seq Number:
RL MDL
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
95
100
104
11.30.15 12.10
11.30.15 12.10
11.30.15 12.10
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 48 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.15 Date Collected:520193-019Lab Sample Id:
Ground WaterMatrix: MW26Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.30.15 06.34 Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
18.0
7.60
7.00
11.3
12.1
10.4
6.00
11.8
13.8
6.90
10.3
18.0
9.40
9.00
12.2
8.70
9.80
13.3
6.70
9.70
37.8
8.80
35.2
9.00
8.90
25.3
35.2
11.9
13.2
11.2
12.4
15.9
9.70
9.90
10.5
17.7
4.20
17.2
8.50
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
J
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
100
50.0
50.0
50.0
50.0
50.0
50.0
200
100
100
50.0
100
50.0
50.0
50.0
50.0
50.0
50.0
50.0
20.0
2000
20.0
40.0
50.0
50.0
40.0
200
50.0
50.0
50.0
50.0
200
100
50.0
50.0
50.0
50.0
50.0
50.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
2820
209
U
329
U
699
U
U
U
U
799
U
U
U
U
U
U
7810
U
U
U
U
U
U
U
U
U
U
U
982462Seq Number:
RL MDL
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
Analysis Date
% Moisture:
Page 49 of 67 Final 1.000
Certificate of Analytical Results 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
11.25.15 09.42 Date Received:
11.24.15 14.15 Date Collected:520193-019Lab Sample Id:
Ground WaterMatrix: MW26Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.30.15 06.34 Date Prep:
MWETech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
11.4
10.0
6.70
300
9.20
9.20
9.80
16.9
19.0
9.40
6.00
6.50
9.20
7.40
8.90
5.40
28.5
18.8
11.0
13.9
5.40
72.0
8.10
17.6
12.2
Result
U
U
U
U
U
U
U
U
U
U
D
U
U
U
U
U
U
50.0
100
100
5000
50.0
50.0
50.0
50.0
50.0
200
200
100
50.0
50.0
50.0
50.0
250
50.0
100
50.0
50.0
100
50.0
100
50.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
500
100
100
100
100
100
100
100
100
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
3640
707
111
185
U
1340
U
342
U
U
U
U
28100
U
U
U
U
U
U
13500
6290
982462Seq Number:
RL MDL
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
12.01.15 14.32
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
98
102
103
11.30.15 15.56
11.30.15 15.56
11.30.15 15.56
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 50 of 67 Final 1.000
QC Summary 520193
Terraquest Environmental Consultants, P.C.
CW Chambers Store
701456-1-BLKMB Sample Id:
WaterMatrix:
VOCs by GC/MS by SM6200B Analytical Method:SM6200B_PREPPrep Method:
11.29.15Date Prep:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Parameter %RPD Flag
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
11
14
11
11
15
14
12
13
5
11
10
10
11
13
13
12
12
11
10
9
15
11
9
11
11
15
3
12
11
9
12
12
7
6
11
14
5
4
1
12
15
9
12
11
12
12
12
9
15
9
10
9
982296Seq Number:
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
Analysis
Date
Limits
75-127
62-128
77-129
86-120
82-114
73-123
83-125
57-127
79-118
59-125
84-118
83-126
83-128
56-133
85-121
86-118
90-126
85-121
88-121
76-126
66-133
80-128
70-130
82-130
80-128
74-129
51-143
81-123
84-114
89-127
79-129
73-140
53-143
66-136
88-118
73-139
70-123
72-118
65-125
85-125
92-126
48-143
61-133
87-123
77-125
82-115
53-149
75-119
52-116
83-130
84-122
86-120
LCSD
%Rec
113
88
109
115
103
100
105
125
88
120
109
116
111
108
108
109
112
115
108
108
112
105
126
106
111
119
88
107
109
106
113
124
89
100
108
123
107
93
79
105
116
62
110
110
110
108
111
100
115
109
107
104
LCSD
Result
28.2
22.0
27.2
28.8
25.7
25.0
26.2
31.2
22.0
30.1
27.3
28.9
27.7
26.9
27.1
27.2
28.1
28.7
27.0
27.1
55.9
26.2
62.9
26.5
27.7
59.7
44.1
26.8
27.3
26.6
28.3
31.1
22.2
25.0
27.0
30.7
26.7
23.2
19.8
26.2
29.1
15.6
1100
27.4
27.5
27.0
55.5
25.1
28.8
27.3
26.8
26.0
LCS
%Rec
101
102
97
103
89
87
93
109
92
108
99
104
99
95
95
96
100
103
98
99
96
94
115
95
99
103
91
95
98
116
100
110
83
94
97
107
102
97
78
93
100
57
98
98
98
96
99
92
100
100
97
95
25.2
25.4
24.3
25.8
22.2
21.8
23.2
27.3
23.1
26.9
24.8
26.1
24.8
23.7
23.7
24.1
24.9
25.7
24.4
24.8
48.2
23.4
57.6
23.8
24.7
51.5
45.3
23.8
24.5
29.0
25.0
27.6
20.8
23.5
24.3
26.8
25.5
24.2
19.6
23.3
25.0
14.3
975
24.5
24.5
23.9
49.3
23.0
24.9
25.0
24.2
23.8
Spike
Amount
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
50.0
25.0
25.0
50.0
50.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
1000
25.0
25.0
25.0
50.0
25.0
25.0
25.0
25.0
25.0
MB
Result
<0.180
<0.0760
<0.0700
<0.113
<0.121
<0.104
<0.0600
<0.118
<0.138
<0.0690
<0.103
<0.180
<0.0940
<0.0900
<0.122
<0.0870
<0.0980
<0.133
<0.0670
<0.0970
<0.378
<0.0880
<0.352
<0.0900
<0.0890
<0.253
<0.352
<0.119
<0.132
<0.112
<0.124
<0.159
<0.0970
<0.0990
<0.105
<0.177
<0.0420
<0.172
<0.0850
<0.114
<0.100
<0.0670
<3.00
<0.0920
<0.0920
<0.0980
<0.169
<0.190
<0.0940
<0.0600
<0.0650
<0.0920
701456-1-BKSLCS Sample Id:701456-1-BSDLCSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsLCS
Result
Page 51 of 67 Final 1.000
QC Summary 520193
Terraquest Environmental Consultants, P.C.
CW Chambers Store
701456-1-BLKMB Sample Id:
WaterMatrix:
VOCs by GC/MS by SM6200B Analytical Method:SM6200B_PREPPrep Method:
11.29.15Date Prep:
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter %RPD Flag
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
9
10
11
11
11
13
12
9
16
12
11
8
982296Seq Number:
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
Analysis
Date
Limits
85-123
79-126
64-131
89-116
78-118
86-127
82-119
46-144
58-141
76-122
90-125
86-119
LCSD
%Rec
111
107
108
108
105
124
107
87
116
88
110
109
LCSD
Result
27.8
26.8
26.9
27.1
26.3
30.9
26.8
21.7
29.1
22.0
55.1
27.2
LCS
%Rec
102
97
96
97
94
109
95
79
99
78
99
100
25.5
24.2
24.1
24.3
23.5
27.2
23.7
19.8
24.8
19.6
49.6
25.0
Spike
Amount
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
MB
Result
<0.0740
<0.0890
<0.0540
<0.0570
<0.188
<0.110
<0.139
<0.0540
<0.720
<0.0810
<0.176
<0.122
701456-1-BKSLCS Sample Id:701456-1-BSDLCSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsLCS
Result
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Surrogate LCSD
Flag
11.29.15 16:28
11.29.15 16:28
11.29.15 16:28
Analysis
Date
Limits
65-126
86-111
83-116
LCSD
%Rec
102
101
105
LCS
%Rec
99
100
107
MB
%Rec
104
105
111
%
%
%
UnitsLCS
Flag
MB
Flag
Page 52 of 67 Final 1.000
QC Summary 520193
Terraquest Environmental Consultants, P.C.
CW Chambers Store
701555-1-BLKMB Sample Id:
WaterMatrix:
VOCs by GC/MS by SM6200B Analytical Method:SM6200B_PREPPrep Method:
11.30.15Date Prep:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Parameter %RPD Flag
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
6
7
0
4
2
0
4
0
7
2
4
3
4
2
3
3
2
4
3
3
4
3
1
3
4
1
7
2
1
1
1
2
8
0
4
5
9
11
3
4
3
15
3
4
3
4
2
1
5
5
4
2
982462Seq Number:
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
Analysis
Date
Limits
75-127
62-128
77-129
86-120
82-114
73-123
83-125
57-127
79-118
59-125
84-118
83-126
83-128
56-133
85-121
86-118
90-126
85-121
88-121
76-126
66-133
80-128
70-130
82-130
80-128
74-129
51-143
81-123
84-114
89-127
79-129
73-140
53-143
66-136
88-118
73-139
70-123
72-118
65-125
85-125
92-126
48-143
61-133
87-123
77-125
82-115
53-149
75-119
52-116
83-130
84-122
86-120
LCSD
%Rec
104
105
102
105
103
100
104
116
100
114
106
105
106
102
104
106
108
105
104
111
111
103
115
105
105
111
98
106
106
106
109
117
87
106
102
110
103
98
80
104
112
55
108
105
105
104
106
106
98
105
106
103
LCSD
Result
25.9
26.3
25.6
26.3
25.7
24.9
25.9
28.9
24.9
28.4
26.5
26.3
26.4
25.5
26.1
26.5
26.9
26.3
26.1
27.7
55.7
25.7
57.3
26.2
26.3
55.7
48.9
26.4
26.6
26.6
27.3
29.2
21.7
26.6
25.5
27.6
25.7
24.5
19.9
26.0
28.0
13.8
1080
26.2
26.3
26.1
53.2
26.6
24.5
26.2
26.4
25.7
LCS
%Rec
110
113
102
109
105
100
108
116
93
116
111
108
110
104
108
110
110
110
107
114
107
106
113
108
109
112
92
108
108
108
110
114
94
106
106
116
112
109
82
108
116
64
111
109
108
108
104
108
103
110
110
105
27.5
28.3
25.5
27.3
26.3
25.0
27.0
28.9
23.2
29.1
27.7
27.0
27.5
26.1
27.0
27.4
27.4
27.4
26.8
28.6
53.4
26.6
56.5
27.0
27.3
56.2
45.8
26.9
26.9
26.9
27.6
28.6
23.4
26.6
26.6
29.0
28.0
27.3
20.5
27.1
28.9
16.1
1110
27.3
27.1
27.1
52.2
27.0
25.8
27.6
27.4
26.3
Spike
Amount
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
50.0
25.0
25.0
50.0
50.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
1000
25.0
25.0
25.0
50.0
25.0
25.0
25.0
25.0
25.0
MB
Result
<0.180
<0.0760
<0.0700
<0.113
<0.121
<0.104
<0.0600
<0.118
<0.138
<0.0690
<0.103
<0.180
<0.0940
<0.0900
<0.122
<0.0870
<0.0980
<0.133
<0.0670
<0.0970
<0.378
<0.0880
<0.352
<0.0900
<0.0890
<0.253
<0.352
<0.119
<0.132
<0.112
<0.124
<0.159
<0.0970
<0.0990
<0.105
<0.177
<0.0420
<0.172
<0.0850
<0.114
<0.100
<0.0670
<3.00
<0.0920
<0.0920
<0.0980
<0.169
<0.190
<0.0940
<0.0600
<0.0650
<0.0920
701555-1-BKSLCS Sample Id:701555-1-BSDLCSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsLCS
Result
Page 53 of 67 Final 1.000
QC Summary 520193
Terraquest Environmental Consultants, P.C.
CW Chambers Store
701555-1-BLK
701601-1-BLK
MB Sample Id:
MB Sample Id:
Water
Water
Matrix:
Matrix:
VOCs by GC/MS by SM6200B
VOCs by GC/MS by SM6200B
Analytical Method:
Analytical Method:
SM6200B_PREP
SM6200B_PREP
Prep Method:
Prep Method:
11.30.15
12.01.15
Date Prep:
Date Prep:
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Benzene
Ethylbenzene
Toluene
m,p-Xylenes
Parameter
Parameter
%RPD
%RPD
Flag
Flag
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
RPD
Limit
2
5
4
4
2
6
1
6
6
1
5
4
1
1
1
2
982462
982542
Seq Number:
Seq Number:
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
12.01.15 12:45
12.01.15 12:45
12.01.15 12:45
12.01.15 12:45
Analysis
Date
Analysis
Date
Limits
Limits
85-123
79-126
64-131
89-116
78-118
86-127
82-119
46-144
58-141
76-122
90-125
86-119
81-123
87-123
89-116
90-125
LCSD
%Rec
LCSD
%Rec
108
102
103
102
105
109
106
87
108
86
103
104
111
110
109
110
LCSD
Result
LCSD
Result
27.1
25.6
25.7
25.6
26.3
27.2
26.5
21.7
26.9
21.6
51.4
26.0
27.8
27.6
27.3
54.9
LCS
%Rec
LCS
%Rec
110
108
107
106
108
116
107
92
102
88
108
108
110
109
108
107
27.6
26.9
26.8
26.6
26.9
28.9
26.7
23.1
25.4
21.9
54.1
27.1
27.6
27.2
26.9
53.6
Spike
Amount
Spike
Amount
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
25.0
25.0
25.0
50.0
MB
Result
MB
Result
<0.0740
<0.0890
<0.0540
<0.0570
<0.188
<0.110
<0.139
<0.0540
<0.720
<0.0810
<0.176
<0.122
<0.119
<0.0920
<0.0570
<0.176
701555-1-BKS
701601-1-BKS
LCS Sample Id:
LCS Sample Id:
701555-1-BSD
701601-1-BSD
LCSD Sample Id:
LCSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
Units
LCS
Result
LCS
Result
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Surrogate
Surrogate
LCSD
Flag
LCSD
Flag
11.30.15 08:00
11.30.15 08:00
11.30.15 08:00
12.01.15 12:45
12.01.15 12:45
12.01.15 12:45
Analysis
Date
Analysis
Date
Limits
Limits
65-126
86-111
83-116
65-126
86-111
83-116
LCSD
%Rec
LCSD
%Rec
98
102
102
98
98
102
LCS
%Rec
LCS
%Rec
95
100
104
96
101
101
MB
%Rec
MB
%Rec
98
102
101
96
103
102
%
%
%
%
%
%
Units
Units
LCS
Flag
LCS
Flag
MB
Flag
MB
Flag
Page 54 of 67 Final 1.000
QC Summary 520193
Terraquest Environmental Consultants, P.C.
CW Chambers Store
519948-022Parent Sample Id:
Ground WaterMatrix:
VOCs by GC/MS by SM6200B Analytical Method:SM6200B_PREPPrep Method:
11.29.15Date Prep:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Parameter %RPD Flag
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
0
7
3
1
3
5
0
2
3
1
1
2
0
2
3
3
2
0
4
1
2
3
2
3
2
19
3
4
4
2
1
1
2
2
1
2
6
8
5
1
5
1
2
2
2
2
2
2
0
3
3
3
982296Seq Number:
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
Analysis
Date
Limits
76-126
63-128
79-133
82-126
77-120
67-123
76-126
41-136
77-125
41-132
53-141
82-130
83-128
59-134
79-125
69-125
83-126
85-124
82-121
56-122
66-136
73-129
63-140
76-129
73-126
71-140
47-138
70-135
76-120
83-132
66-132
63-143
60-134
59-139
83-120
68-140
67-125
72-120
59-128
80-125
74-122
48-138
55-140
70-140
77-125
75-117
51-155
75-119
34-135
73-128
75-125
77-122
MSD
%Rec
106
97
108
116
95
88
102
114
104
106
102
114
103
106
105
99
102
117
100
73
118
97
125
96
98
105
107
103
101
103
108
116
84
97
101
116
96
96
73
98
110
62
118
103
105
101
105
88
109
95
98
96
MSD
Result
26.5
24.2
27.0
29.0
23.7
21.9
25.5
28.5
26.1
26.6
25.6
28.5
25.8
26.6
26.2
24.7
25.6
29.2
25.0
18.2
59.2
24.2
62.4
24.1
24.6
52.3
53.4
25.7
25.3
25.8
27.0
28.9
21.0
24.2
25.2
28.9
24.0
23.9
18.3
24.6
27.5
15.5
1180
25.7
26.3
25.3
52.7
22.1
27.2
23.7
24.4
24.0
MS
%Rec
106
90
111
117
98
92
102
112
107
108
104
117
103
108
108
102
104
117
104
73
121
100
123
99
101
126
110
107
106
105
110
117
86
99
102
118
90
88
77
100
115
62
120
105
107
103
108
86
109
98
101
99
26.6
22.5
27.8
29.2
24.4
23.1
25.5
27.9
26.8
26.9
25.9
29.2
25.8
27.1
26.9
25.4
26.1
29.2
26.1
18.3
60.6
25.0
61.3
24.8
25.2
63.0
54.8
26.7
26.4
26.2
27.4
29.2
21.5
24.8
25.4
29.4
22.6
22.1
19.3
24.9
28.8
15.6
1200
26.3
26.7
25.8
53.9
21.6
27.2
24.4
25.2
24.7
Spike
Amount
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
50.0
25.0
25.0
50.0
50.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
1000
25.0
25.0
25.0
50.0
25.0
25.0
25.0
25.0
25.0
Parent
Result
<0.180
<0.0760
<0.0700
<0.113
<0.121
<0.104
<0.0600
<0.118
<0.138
<0.0690
<0.103
<0.180
<0.0940
<0.0900
<0.122
<0.0870
<0.0980
<0.133
<0.0670
<0.0970
<0.378
<0.0880
<0.352
<0.0900
<0.0890
<0.253
<0.352
<0.119
<0.132
<0.112
<0.124
<0.159
<0.0970
<0.0990
<0.105
<0.177
<0.0420
<0.172
<0.0850
<0.114
<0.100
<0.0670
<3.00
<0.0920
<0.0920
<0.0980
<0.169
<0.190
<0.0940
<0.0600
<0.0650
<0.0920
519948-022 SMS Sample Id:519948-022 SDMSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsMS
Result
Page 55 of 67 Final 1.000
QC Summary 520193
Terraquest Environmental Consultants, P.C.
CW Chambers Store
519948-022Parent Sample Id:
Ground WaterMatrix:
VOCs by GC/MS by SM6200B Analytical Method:SM6200B_PREPPrep Method:
11.29.15Date Prep:
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter %RPD Flag
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
2
3
3
3
0
2
4
4
0
8
2
2
982296Seq Number:
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
Analysis
Date
Limits
54-137
74-124
57-130
81-125
69-122
73-129
73-124
49-139
57-134
70-121
65-151
58-148
MSD
%Rec
101
99
100
101
96
115
101
82
82
80
103
101
MSD
Result
25.2
24.8
25.1
25.2
24.1
28.7
25.2
20.5
20.5
20.1
51.7
25.2
MS
%Rec
103
102
103
104
96
113
104
85
82
87
106
103
25.8
25.5
25.8
26.0
24.1
28.2
26.1
21.3
20.4
21.7
53.0
25.8
Spike
Amount
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
Parent
Result
<0.0740
<0.0890
<0.0540
<0.0570
<0.188
<0.110
<0.139
<0.0540
<0.720
<0.0810
<0.176
<0.122
519948-022 SMS Sample Id:519948-022 SDMSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsMS
Result
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Surrogate MSD
Flag
11.30.15 02:30
11.30.15 02:30
11.30.15 02:30
Analysis
Date
Limits
65-126
86-111
83-116
MSD
%Rec
106
102
105
MS
%Rec
104
104
105
%
%
%
UnitsMS
Flag
Page 56 of 67 Final 1.000
QC Summary 520193
Terraquest Environmental Consultants, P.C.
CW Chambers Store
520193-004Parent Sample Id:
Ground WaterMatrix:
VOCs by GC/MS by SM6200B Analytical Method:SM6200B_PREPPrep Method:
11.30.15Date Prep:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Parameter %RPD Flag
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
3
5
2
1
3
10
1
4
5
1
1
3
3
0
3
2
3
0
5
10
12
1
6
3
3
5
3
2
1
5
0
4
4
5
1
3
5
2
1
4
0
5
3
0
3
0
2
8
13
0
1
2
982462Seq Number:
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
Analysis
Date
Limits
76-126
63-128
79-133
82-126
77-120
67-123
76-126
41-136
77-125
41-132
53-141
82-130
83-128
59-134
79-125
69-125
83-126
85-124
82-121
56-122
66-136
73-129
63-140
76-129
73-126
71-140
47-138
70-135
76-120
83-132
66-132
63-143
60-134
59-139
83-120
68-140
67-125
72-120
59-128
80-125
74-122
48-138
55-140
70-140
77-125
75-117
51-155
75-119
34-135
73-128
75-125
77-122
MSD
%Rec
98
93
97
106
88
84
95
105
91
100
92
104
94
98
99
92
94
101
93
91
120
90
111
90
92
112
104
96
94
116
102
112
78
92
93
107
98
97
70
94
102
60
116
95
97
93
102
91
118
92
91
90
MSD
Result
24.4
23.2
24.2
26.4
22.1
21.1
23.7
26.2
22.7
24.9
23.1
25.9
23.6
24.6
24.8
22.9
23.6
25.3
23.3
22.8
60.0
22.4
55.3
22.5
23.0
56.1
51.8
23.9
23.4
29.1
25.4
28.1
19.5
23.0
23.3
26.8
24.4
24.3
17.6
23.4
25.5
15.0
1160
23.8
24.3
23.2
50.8
22.8
29.5
23.1
22.7
22.5
MS
%Rec
101
98
99
105
91
94
96
100
95
99
94
107
98
98
96
93
97
102
98
101
107
90
117
92
95
118
100
98
94
111
101
108
81
97
94
110
102
100
70
97
102
63
113
95
100
92
103
98
104
92
92
92
25.2
24.4
24.7
26.2
22.7
23.4
23.9
25.1
23.8
24.7
23.4
26.7
24.4
24.5
24.0
23.3
24.2
25.4
24.4
25.2
53.4
22.6
58.6
23.1
23.8
58.8
50.1
24.5
23.6
27.7
25.3
27.1
20.2
24.2
23.6
27.6
25.6
24.9
17.5
24.3
25.6
15.7
1130
23.8
25.0
23.1
51.7
24.6
25.9
23.0
22.9
22.9
Spike
Amount
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
50.0
25.0
25.0
50.0
50.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
1000
25.0
25.0
25.0
50.0
25.0
25.0
25.0
25.0
25.0
Parent
Result
<0.180
<0.0760
<0.0700
<0.113
<0.121
<0.104
<0.0600
<0.118
<0.138
<0.0690
<0.103
<0.180
<0.0940
<0.0900
<0.122
<0.0870
<0.0980
<0.133
<0.0670
<0.0970
<0.378
<0.0880
<0.352
<0.0900
<0.0890
<0.253
<0.352
<0.119
<0.132
<0.112
<0.124
<0.159
<0.0970
<0.0990
<0.105
<0.177
<0.0420
<0.172
<0.0850
<0.114
<0.100
<0.0670
<3.00
<0.0920
<0.0920
<0.0980
<0.169
<0.190
<0.0940
<0.0600
<0.0650
<0.0920
520193-004 SMS Sample Id:520193-004 SDMSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsMS
Result
Page 57 of 67 Final 1.000
QC Summary 520193
Terraquest Environmental Consultants, P.C.
CW Chambers Store
520193-004Parent Sample Id:
Ground WaterMatrix:
VOCs by GC/MS by SM6200B Analytical Method:SM6200B_PREPPrep Method:
11.30.15Date Prep:
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter %RPD Flag
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
3
4
6
1
3
1
3
10
1
6
4
2
982462Seq Number:
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
Analysis
Date
Limits
54-137
74-124
57-130
81-125
69-122
73-129
73-124
49-139
57-134
70-121
65-151
58-148
MSD
%Rec
97
91
91
94
94
103
94
80
93
76
94
94
MSD
Result
24.3
22.8
22.8
23.5
23.4
25.7
23.5
20.1
23.3
18.9
47.1
23.5
MS
%Rec
100
95
96
95
96
102
96
89
94
80
98
96
25.0
23.7
24.1
23.8
24.1
25.4
24.1
22.3
23.6
20.0
48.8
24.0
Spike
Amount
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
Parent
Result
<0.0740
<0.0890
<0.0540
<0.0570
<0.188
<0.110
<0.139
<0.0540
<0.720
<0.0810
<0.176
<0.122
520193-004 SMS Sample Id:520193-004 SDMSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsMS
Result
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Surrogate MSD
Flag
11.30.15 19:04
11.30.15 19:04
11.30.15 19:04
Analysis
Date
Limits
65-126
86-111
83-116
MSD
%Rec
100
100
104
MS
%Rec
102
100
104
%
%
%
UnitsMS
Flag
Page 58 of 67 Final 1.000
Blank Summary 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
701456-1-BLKLab Sample Id:
WATERMatrix: 701456-1-BLK Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.29.15 15:31Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
Parameter
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
0.114
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
0.400
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
156-59-2
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982296Seq Number:
MDLRL
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
Analysis
Date
Page 59 of 67 Final 1.000
Blank Summary 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
701456-1-BLKLab Sample Id:
WATERMatrix: 701456-1-BLK Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.29.15 15:31Date Prep:
MWETech:
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
0.100
0.0670
3.00
0.0920
0.0920
0.0980
0.169
0.190
0.0940
0.0600
0.0650
0.0920
0.0740
0.0890
0.0540
0.0570
0.188
0.110
0.139
0.0540
0.720
0.0810
0.176
0.122
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
1.00
50.0
0.500
0.500
0.500
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982296Seq Number:
MDLRL
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
11.29.15 17:52
Analysis
Date
Page 60 of 67 Final 1.000
Blank Summary 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
701555-1-BLKLab Sample Id:
WATERMatrix: 701555-1-BLK Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.30.15 06:34Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
Parameter
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
0.114
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
0.400
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
156-59-2
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982462Seq Number:
MDLRL
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
Analysis
Date
Page 61 of 67 Final 1.000
Blank Summary 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
701555-1-BLKLab Sample Id:
WATERMatrix: 701555-1-BLK Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
11.30.15 06:34Date Prep:
MWETech:
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
0.100
0.0670
3.00
0.0920
0.0920
0.0980
0.169
0.190
0.0940
0.0600
0.0650
0.0920
0.0740
0.0890
0.0540
0.0570
0.188
0.110
0.139
0.0540
0.720
0.0810
0.176
0.122
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
1.00
50.0
0.500
0.500
0.500
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
982462Seq Number:
MDLRL
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
11.30.15 09:19
Analysis
Date
Page 62 of 67 Final 1.000
Blank Summary 520193
Terraquest Environmental Consultants, P.C., Mebane, NC
CW Chambers Store
701601-1-BLKLab Sample Id:
WATERMatrix: 701601-1-BLK Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
12.01.15 11:42Date Prep:
MWETech:
Benzene
Ethylbenzene
Toluene
m,p-Xylenes
Parameter
0.119
0.0920
0.0570
0.176
Result
U
U
U
U
0.500
0.500
0.500
1.00
Flag
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
DilCas Number
71-43-2
100-41-4
108-88-3
179601-23-1
U
U
U
U
982542Seq Number:
MDLRL
12.01.15 14:06
12.01.15 14:06
12.01.15 14:06
12.01.15 14:06
Analysis
Date
Page 63 of 67 Final 1.000
Page 64 of 67 Final 1.000
Page 65 of 67 Final 1.000
Page 66 of 67 Final 1.000
Prelogin/Nonconformance Report- Sample Log-In
XENCO Laboratories
520193Work Order #:
11/25/2015 09:42:00 AMDate/ Time Received:
Terraquest Environmental Consultants, PClient:
Sample Receipt Checklist
Checklist completed by: Date:
Checklist reviewed by:Date:
Chad Bechtold
11/27/2015
12/02/2015
#2 *Shipping container in good condition?
#3 *Samples received on ice?
#4 *Custody Seals intact on shipping container/ cooler?
#5 Custody Seals intact on sample bottles?
#6 *Custody Seals Signed and dated?
#7 *Chain of Custody present?
#8 Sample instructions complete on Chain of Custody?
#9 Any missing/extra samples?
#10 Chain of Custody signed when relinquished/ received?
#11 Chain of Custody agrees with sample label(s)?
#12 Container label(s) legible and intact?
#13 Sample matrix/ properties agree with Chain of Custody?
#14 Samples in proper container/ bottle?
#15 Samples properly preserved?
#16 Sample container(s) intact?
#17 Sufficient sample amount for indicated test(s)?
#18 All samples received within hold time?
#19 Subcontract of sample(s)?
#20 VOC samples have zero headspace (less than 1/4 inch bubble)?
#21 <2 for all samples preserved with HNO3,HCL, H2SO4? Except for
samples for the analysis of HEM or HEM-SGT which are verified by the
analysts.
#22 >10 for all samples preserved with NaAsO2+NaOH, ZnAc+NaOH?
Yes
Yes
N/A
N/A
N/A
Yes
Yes
No
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
No
Yes
N/A
N/A

#1 *Temperature of cooler(s)?1.3
Acceptable Temperature Range: 0 - 6 degC
Air and Metal samples Acceptable Range: Ambient
* Must be completed for after-hours delivery of samples prior to placing in the refrigerator
Analyst: PH Device/Lot#:
Comments
Dario Lagunas
Temperature Measuring device used : #61
Page 67 of 67 Final 1.000