RA-2352_15092_CA_MRP_20150825

Analytical Report 513506
for
Terraquest Environmental Consultants, P.C.
Project Manager: Ryan Kerins
Chambers Store
22-AUG-15
02794
6017 Financial Dr., Norcross, GA 30071
Ph:[phone] Fax:[phone]
Xenco-Houston (EPA Lab code: TX00122):
Texas (T104704215-15-19), Arizona (AZ0765), Florida (E871002), Louisiana (03054)
Oklahoma (9218)
Xenco-Atlanta (EPA Lab Code: GA00046):
Florida (E87429), North Carolina (483), South Carolina (98015), Kentucky (85), DoD ( L10-135)
Texas (T104704477), Louisiana (04176), USDA (P330-07-00105)
Xenco-Lakeland: Florida (E84098)
Xenco-Odessa (EPA Lab code: TX00158): Texas (T104704400-TX)
Xenco-Dallas (EPA Lab code: TX01468): Texas (T104704295-TX)
Xenco Phoenix (EPA Lab Code: AZ00901): Arizona(AZ0757)
Xenco-Phoenix Mobile (EPA Lab code: AZ00901): Arizona (AZM757)
Xenco Tucson (EPA Lab code:AZ000989): Arizona (AZ0758)
Collected By: Client
Page 1 of 43 Final 1.000

Page 2 of 43 Final 1.000
Table of Contents
Cover Page 1
Cover Letter 3
Sample ID Cross Reference 4
Explanation of Qualifiers (Flags) 5
Hits Summary 6
Certificate of Analysis (Detailed Report) 11
Summary of Quality control 29
Blank Summary 37
Chain of Custody 41
Sample Receipt Conformance Report 43
Houston - Dallas - Odessa - San Antonio - Tampa - Lakeland - Atlanta - Phoenix - Oklahoma - Latin America
Recipient of the Prestigious Small Business Administration Award of Excellence in 1994.
Certified and approved by numerous States and Agencies.
A Small Business and Minority Status Company that delivers SERVICE and QUALITY
Project Manager: Ryan Kerins
Terraquest Environmental Consultants, P.C.
100 E. Ruffin Street
Mebane, NC 27302

Reference: XENCO Report No(s): 513506
Chambers Store
Project Address: NC
Ryan Kerins:
We are reporting to you the results of the analyses performed on the samples received under the project name
referenced above and identified with the XENCO Report Number(s) 513506. All results being reported under
this Report Number apply to the samples analyzed and properly identified with a Laboratory ID number.
Subcontracted analyses are identified in this report with either the NELAC certification number of the
subcontract lab in the analyst ID field, or the complete subcontracted report attached to this report.
Unless otherwise noted in a Case Narrative, all data reported in this Analytical Report are in compliance with
NELAC standards. The uncertainty of measurement associated with the results of analysis reported is
available upon request. Should insufficient sample be provided to the laboratory to meet the method and
NELAC Matrix Duplicate and Matrix Spike requirements, then the data will be analyzed, evaluated and
reported using all other available quality control measures.
The validity and integrity of this report will remain intact as long as it is accompanied by this letter and
reproduced in full, unless written approval is granted by XENCO Laboratories. This report will be filed for at
least 5 years in our archives after which time it will be destroyed without further notice, unless otherwise
arranged with you. The samples received, and described as recorded in Report No. 513506 will be filed for
60 days, and after that time they will be properly disposed without further notice, unless otherwise arranged
with you. We reserve the right to return to you any unused samples, extracts or solutions related to them if we
consider so necessary (e.g., samples identified as hazardous waste, sample sizes exceeding analytical standard
practices, controlled substances under regulated protocols, etc).
We thank you for selecting XENCO Laboratories to serve your analytical needs. If you have any questions
concerning this report, please feel free to contact us at any time.
Respectfully,
22-AUG-15
Project Manager
Debbie Simmons
Page 3 of 43 Final 1.000
Sample Cross Reference 513506
Terraquest Environmental Consultants, P.C., Mebane, NC
Chambers Store
Sample Id
MW1A
MW2A
MW20
MW21
MW22
MW23
MW24
MW25
MW26
08-13-15 13:05
08-13-15 13:11
08-13-15 13:20
08-13-15 13:26
08-13-15 13:35
08-13-15 13:47
08-13-15 13:54
08-13-15 14:02
08-13-15 14:15
Date Collected Lab Sample Id
513506-001
513506-002
513506-003
513506-004
513506-005
513506-006
513506-007
513506-008
513506-009

Sample DepthMatrix
W
W
W
W
W
W
W
W
W
Page 4 of 43 Final 1.000
Houston - Dallas - San Antonio - Atlanta - Midland/Odessa - Tampa/Lakeland - Phoenix - Latin America
4143 Greenbriar Dr, Stafford, TX 77477
9701 Harry Hines Blvd , Dallas, TX 75220
5332 Blackberry Drive, San Antonio TX 78238
2505 North Falkenburg Rd, Tampa, FL 33619
12600 West I-20 East, Odessa, TX 79765
6017 Financial Drive, Norcross, GA 30071
3725 E. Atlanta Ave, Phoenix, AZ 85040
Phone Fax
[phone] [phone]
[phone] [phone]
[phone] [phone]
[phone] [phone]
[phone] [phone]
[phone] [phone]
[phone]
Recipient of the Prestigious Small Business Administration Award of Excellence in 1994.
Certified and approved by numerous States and Agencies.
A Small Business and Minority Status Company that delivers SERVICE and QUALITY
Flagging Criteria
X In our quality control review of the data a QC deficiency was observed and flagged as noted. MS/MSD recoveries were found to be
outside of the laboratory control limits due to possible matrix /chemical interference, or a concentration of target analyte high enough
to affect the recovery of the spike concentration. This condition could also affect the relative percent difference in the MS/MSD.
B A target analyte or common laboratory contaminant was identified in the method blank. Its presence indicates possible field or
laboratory contamination.
D The sample(s) were diluted due to targets detected over the highest point of the calibration curve, or due to matrix interference.
Dilution factors are included in the final results. The result is from a diluted sample.
E The data exceeds the upper calibration limit; therefore, the concentration is reported as estimated.
F RPD exceeded lab control limits.
J The target analyte was positively identified below the quantitation limit and above the detection limit.
U Analyte was not detected.
L The LCS data for this analytical batch was reported below the laboratory control limits for this analyte. The department supervisor and
QA Director reviewed data. The samples were either reanalyzed or flagged as estimated concentrations.
H The LCS data for this analytical batch was reported above the laboratory control limits. Supporting QC Data were reviewed by the
Department Supervisor and QA Director. Data were determined to be valid for reporting.
K Sample analyzed outside of recommended hold time.
JN A combination of the "N" and the "J" qualifier. The analysis indicates that the analyte is "tentatively identified" and the associated
numerical value may not be consistent with the amount actually present in the environmental sample.
** Surrogate recovered outside laboratory control limit.
BRL Below Reporting Limit.
RL Reporting Limit
MDL Method Detection Limit SDL Sample Detection Limit LOD Limit of Detection
PQL Practical Quantitation Limit MQL Method Quantitation Limit LOQ Limit of Quantitation
DL Method Detection Limit
NC Non-Calculable
+ NELAC certification not offered for this compound.

* (Next to analyte name or method description) = Outside XENCO's scope of NELAC accreditation
Page 5 of 43 Final 1.000
Hits Summary 513506
Terraquest Environmental Consultants, P.C., Mebane, NC
Chambers Store
08.14.15 09.50
08.14.15 09.50
Date Received :
Date Received :
% Moisture :
% Moisture :
08.13.15 13.05
08.13.15 13.11
Date Collected :
Date Collected :
513506-001
513506-002
Lab Sample Id :
Lab Sample Id :
Ground Water
Ground Water
Matrix :
Matrix :
MW1A
MW2A
Sample Id :
Sample Id :
VOCs by GC/MS by SM6200B
VOCs by GC/MS by SM6200B
Analytical Method :
Analytical Method :
SM6200B_PREP
SM6200B_PREP
Prep Method:
Prep Method:
08.20.15 09.03
08.20.15 09.03
Date Prep:
Date Prep:
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichloroethane
1,3,5-Trimethylbenzene
2-Butanone (MEK)
Acetone
Benzene
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Naphthalene
n-Propylbenzene
Toluene
m,p-Xylenes
o-Xylene
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
2-Butanone (MEK)
2-Hexanone
Acetone
Benzene
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Naphthalene
n-Propylbenzene
Styrene
Toluene
m,p-Xylenes
o-Xylene
Parameter
Parameter
Result
Result
D
D
J
D
D
Flag
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
Units
20
20
20
20
20
20
200
20
20
20
20
20
20
200
20
20
50
50
50
50
50
500
50
50
50
50
50
50
50
500
50
50
Dil
Dil
Cas Number
Cas Number
95-63-6
106-93-4
107-06-2
108-67-8
78-93-3
67-64-1
71-43-2
100-41-4
108-20-3
98-82-8
1634-04-4
91-20-3
103-65-1
108-88-3
179601-23-1
95-47-6
95-63-6
108-67-8
78-93-3
591-78-6
67-64-1
71-43-2
100-41-4
108-20-3
98-82-8
1634-04-4
91-20-3
103-65-1
100-42-5
108-88-3
179601-23-1
95-47-6
940
40.4
95.2
267
511
318
7400
1280
401
32.8
137
424
84.2
3770
3840
1880
1970
513
609
186
108
7210
2250
481
66.5
584
876
164
163
20200
9000
4130
975118
975118
Seq Number
Seq Number
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.59
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.59
08.20.15 18.32
08.20.15 18.32
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.21.15 02.34
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.21.15 02.34
08.20.15 19.55
08.20.15 19.55
Analysis Date
Analysis Date
Page 6 of 43 Final 1.000
Hits Summary 513506
Terraquest Environmental Consultants, P.C., Mebane, NC
Chambers Store
08.14.15 09.50
08.14.15 09.50
Date Received :
Date Received :
% Moisture :
% Moisture :
08.13.15 13.20
08.13.15 13.26
Date Collected :
Date Collected :
513506-003
513506-004
Lab Sample Id :
Lab Sample Id :
Ground Water
Ground Water
Matrix :
Matrix :
MW20
MW21
Sample Id :
Sample Id :
VOCs by GC/MS by SM6200B
VOCs by GC/MS by SM6200B
Analytical Method :
Analytical Method :
SM6200B_PREP
SM6200B_PREP
Prep Method:
Prep Method:
08.20.15 09.03
08.20.15 09.03
Date Prep:
Date Prep:
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Benzene
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Naphthalene
n-Propylbenzene
Styrene
tert-Butylbenzene
Toluene
m,p-Xylenes
o-Xylene
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
2-Butanone (MEK)
Acetone
Benzene
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Propylbenzene
Toluene
m,p-Xylenes
o-Xylene
Parameter
Parameter
Result
Result
DX
DX
DX
J
D
J
Flag
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
Units
10
10
100
100
10
10
10
10
10
10
10
10
100
10
10
10
10
10
100
10
10
10
10
10
10
10
10
10
10
Dil
Dil
Cas Number
Cas Number
95-63-6
108-67-8
71-43-2
100-41-4
108-20-3
98-82-8
1634-04-4
91-20-3
103-65-1
100-42-5
98-06-6
108-88-3
179601-23-1
95-47-6
95-63-6
108-67-8
78-93-3
67-64-1
71-43-2
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
103-65-1
108-88-3
179601-23-1
95-47-6
801
239
4020
1490
128
65.8
349
492
155
20.9
15.8
239
2280
131
298
75.9
16.0
67.0
4090
545
49.9
27.9
48.0
2.30
370
52.7
248
293
129
975121
975121
Seq Number
Seq Number
08.21.15 03.01
08.21.15 03.01
08.21.15 03.28
08.21.15 03.28
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.28
08.21.15 03.01
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 04.21
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
Analysis Date
Analysis Date
Page 7 of 43 Final 1.000
Hits Summary 513506
Terraquest Environmental Consultants, P.C., Mebane, NC
Chambers Store
08.14.15 09.50
08.14.15 09.50
Date Received :
Date Received :
% Moisture :
% Moisture :
08.13.15 13.35
08.13.15 13.47
Date Collected :
Date Collected :
513506-005
513506-006
Lab Sample Id :
Lab Sample Id :
Ground Water
Ground Water
Matrix :
Matrix :
MW22
MW23
Sample Id :
Sample Id :
VOCs by GC/MS by SM6200B
VOCs by GC/MS by SM6200B
Analytical Method :
Analytical Method :
SM6200B_PREP
SM6200B_PREP
Prep Method:
Prep Method:
08.20.15 09.03
08.20.15 09.03
Date Prep:
Date Prep:
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Benzene
Ethylbenzene
Naphthalene
n-Propylbenzene
Styrene
Toluene
m,p-Xylenes
o-Xylene
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
2-Butanone (MEK)
Acetone
Benzene
Ethylbenzene
Isopropyl ether
Methyl tert-butyl ether (MTBE)
Naphthalene
n-Propylbenzene
Toluene
m,p-Xylenes
o-Xylene
Parameter
Parameter
Result
Result
D
D
D
Flag
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
Units
100
100
100
100
100
100
100
500
100
100
100
100
100
100
500
100
100
100
100
100
500
100
100
Dil
Dil
Cas Number
Cas Number
95-63-6
108-67-8
71-43-2
100-41-4
91-20-3
103-65-1
100-42-5
108-88-3
179601-23-1
95-47-6
95-63-6
108-67-8
78-93-3
67-64-1
71-43-2
100-41-4
108-20-3
1634-04-4
91-20-3
103-65-1
108-88-3
179601-23-1
95-47-6
2360
573
3610
2570
1070
188
340
42500
11000
5420
1680
423
3400
269
23000
2190
865
807
795
212
22900
7840
3680
975121
975121
Seq Number
Seq Number
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 05.16
08.21.15 04.48
08.21.15 04.48
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 06.09
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 06.09
08.21.15 05.43
08.21.15 05.43
Analysis Date
Analysis Date
Page 8 of 43 Final 1.000
Hits Summary 513506
Terraquest Environmental Consultants, P.C., Mebane, NC
Chambers Store
08.14.15 09.50
08.14.15 09.50
Date Received :
Date Received :
% Moisture :
% Moisture :
08.13.15 13.54
08.13.15 14.02
Date Collected :
Date Collected :
513506-007
513506-008
Lab Sample Id :
Lab Sample Id :
Ground Water
Ground Water
Matrix :
Matrix :
MW24
MW25
Sample Id :
Sample Id :
VOCs by GC/MS by SM6200B
VOCs by GC/MS by SM6200B
Analytical Method :
Analytical Method :
SM6200B_PREP
SM6200B_PREP
Prep Method:
Prep Method:
08.20.15 09.03
08.20.15 09.03
Date Prep:
Date Prep:
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
2-Butanone (MEK)
Acetone
Benzene
Ethylbenzene
Isopropyl ether
Methyl tert-butyl ether (MTBE)
Naphthalene
n-Propylbenzene
Toluene
m,p-Xylenes
o-Xylene
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
2-Butanone (MEK)
2-Hexanone
Benzene
Ethylbenzene
Isopropylbenzene
Naphthalene
n-Propylbenzene
sec-Butylbenzene
tert-Butylbenzene
Toluene
m,p-Xylenes
o-Xylene
Parameter
Parameter
Result
Result
D
D
D
J
D
D
D
D
Flag
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
Units
100
100
100
100
500
100
100
100
100
100
500
100
100
100
10
10
10
10
100
10
10
10
10
10
100
100
100
Dil
Dil
Cas Number
Cas Number
95-63-6
108-67-8
78-93-3
67-64-1
71-43-2
100-41-4
108-20-3
1634-04-4
91-20-3
103-65-1
108-88-3
179601-23-1
95-47-6
95-63-6
108-67-8
78-93-3
591-78-6
71-43-2
100-41-4
98-82-8
91-20-3
103-65-1
135-98-8
98-06-6
108-88-3
179601-23-1
95-47-6
1870
464
5760
627
22100
2700
2680
6010
891
209
37600
9920
4740
2280
624
42.4
162
175
915
94.2
697
241
11.5
31.9
3400
3920
2530
975121
975121
Seq Number
Seq Number
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 07.03
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 07.03
08.21.15 06.36
08.21.15 06.36
08.21.15 07.56
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.56
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.56
08.21.15 07.56
08.21.15 07.56
Analysis Date
Analysis Date
Page 9 of 43 Final 1.000
Hits Summary 513506
Terraquest Environmental Consultants, P.C., Mebane, NC
Chambers Store
08.14.15 09.50 Date Received :
% Moisture :
08.13.15 14.15 Date Collected : 513506-009Lab Sample Id :
Ground WaterMatrix : MW26Sample Id :
VOCs by GC/MS by SM6200B Analytical Method :SM6200B_PREPPrep Method:
08.20.15 09.03 Date Prep:
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichloroethane
1,3,5-Trimethylbenzene
2-Butanone (MEK)
Benzene
Ethylbenzene
Isopropyl ether
Methyl tert-butyl ether (MTBE)
Naphthalene
n-Propylbenzene
Toluene
m,p-Xylenes
o-Xylene
Parameter Result
D
D
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
100
100
100
100
100
500
100
100
100
100
100
500
100
100
DilCas Number
95-63-6
106-93-4
107-06-2
108-67-8
78-93-3
71-43-2
100-41-4
108-20-3
1634-04-4
91-20-3
103-65-1
108-88-3
179601-23-1
95-47-6
2240
343
528
569
2060
10300
3290
1130
282
971
277
30200
11700
5450
975121Seq Number
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.48
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.48
08.21.15 08.22
08.21.15 08.22
Analysis Date
Page 10 of 43 Final 1.000
Certificate of Analytical Results 513506
Terraquest Environmental Consultants, P.C., Mebane, NC
Chambers Store
08.14.15 09.50 Date Received:
08.13.15 13.05 Date Collected:513506-001Lab Sample Id:
Ground WaterMatrix: MW1ASample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
08.20.15 09.03 Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
3.60
1.52
1.40
2.26
2.42
2.08
1.20
2.36
2.76
1.38
2.06
3.60
1.88
1.80
2.44
1.74
1.96
2.66
1.34
1.94
7.56
1.76
7.04
1.80
1.78
5.06
7.04
23.8
2.64
2.24
2.48
3.18
1.94
1.98
2.10
3.54
0.840
3.44
1.70
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
D
U
U
U
U
U
U
U
U
U
U
U
20.0
10.0
10.0
10.0
10.0
10.0
10.0
40.0
20.0
20.0
10.0
20.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
4.00
400
4.00
8.00
10.0
10.0
8.00
40.0
100
10.0
10.0
10.0
40.0
20.0
10.0
10.0
10.0
10.0
10.0
10.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
200
20
20
20
20
20
20
20
20
20
20
20
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
940
40.4
U
95.2
U
267
U
U
U
U
511
U
U
U
U
U
318
7400
U
U
U
U
U
U
U
U
U
U
U
975118Seq Number:
RL MDL
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.59
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
Analysis Date
% Moisture:
Page 11 of 43 Final 1.000
Certificate of Analytical Results 513506
Terraquest Environmental Consultants, P.C., Mebane, NC
Chambers Store
08.14.15 09.50 Date Received:
08.13.15 13.05 Date Collected:513506-001Lab Sample Id:
Ground WaterMatrix: MW1ASample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
08.20.15 09.03 Date Prep:
MWETech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
2.28
2.00
1.34
60.1
1.84
1.84
1.96
3.38
3.80
1.88
1.20
1.30
1.84
1.48
1.78
1.08
11.4
3.76
2.20
2.78
1.08
14.4
1.62
3.52
2.44
Result
U
U
U
U
U
U
U
U
U
U
D
U
U
U
U
U
U
10.0
20.0
20.0
1000
10.0
10.0
10.0
10.0
10.0
40.0
40.0
20.0
10.0
10.0
10.0
10.0
100
10.0
20.0
10.0
10.0
20.0
10.0
20.0
10.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
200
20
20
20
20
20
20
20
20
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
1280
401
32.8
137
U
424
U
84.2
U
U
U
U
3770
U
U
U
U
U
U
3840
1880
975118Seq Number:
RL MDL
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.59
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
96
99
99
08.20.15 18.32
08.20.15 18.32
08.20.15 18.32
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 12 of 43 Final 1.000
Certificate of Analytical Results 513506
Terraquest Environmental Consultants, P.C., Mebane, NC
Chambers Store
08.14.15 09.50 Date Received:
08.13.15 13.11 Date Collected:513506-002Lab Sample Id:
Ground WaterMatrix: MW2ASample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
08.20.15 09.03 Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
9.00
3.80
3.50
5.65
6.05
5.20
3.00
5.90
6.90
3.45
5.15
9.00
4.70
4.50
6.10
4.35
4.90
6.65
3.35
4.85
18.9
4.40
17.6
4.50
4.45
12.7
17.6
59.5
6.60
5.60
6.20
7.95
4.85
4.95
5.25
8.85
2.10
8.60
4.25
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
J
U
U
U
U
D
U
U
U
U
U
U
U
U
U
U
U
50.0
25.0
25.0
25.0
25.0
25.0
25.0
100
50.0
50.0
25.0
50.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
10.0
1000
10.0
20.0
25.0
25.0
20.0
100
250
25.0
25.0
25.0
100
50.0
25.0
25.0
25.0
25.0
25.0
25.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
500
50
50
50
50
50
50
50
50
50
50
50
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
1970
U
U
U
U
513
U
U
U
U
609
U
186
U
U
U
108
7210
U
U
U
U
U
U
U
U
U
U
U
975118Seq Number:
RL MDL
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.21.15 02.34
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
Analysis Date
% Moisture:
Page 13 of 43 Final 1.000
Certificate of Analytical Results 513506
Terraquest Environmental Consultants, P.C., Mebane, NC
Chambers Store
08.14.15 09.50 Date Received:
08.13.15 13.11 Date Collected:513506-002Lab Sample Id:
Ground WaterMatrix: MW2ASample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
08.20.15 09.03 Date Prep:
MWETech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
5.70
5.00
3.35
150
4.60
4.60
4.90
8.45
9.50
4.70
3.00
3.25
4.60
3.70
4.45
2.70
28.5
9.40
5.50
6.95
2.70
36.0
4.05
8.80
6.10
Result
U
U
U
U
U
U
U
U
U
D
U
U
U
U
U
U
25.0
50.0
50.0
2500
25.0
25.0
25.0
25.0
25.0
100
100
50.0
25.0
25.0
25.0
25.0
250
25.0
50.0
25.0
25.0
50.0
25.0
50.0
25.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
500
50
50
50
50
50
50
50
50
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
2250
481
66.5
584
U
876
U
164
U
163
U
U
20200
U
U
U
U
U
U
9000
4130
975118Seq Number:
RL MDL
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.21.15 02.34
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
100
100
99
08.20.15 19.55
08.20.15 19.55
08.20.15 19.55
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 14 of 43 Final 1.000
Certificate of Analytical Results 513506
Terraquest Environmental Consultants, P.C., Mebane, NC
Chambers Store
08.14.15 09.50 Date Received:
08.13.15 13.20 Date Collected:513506-003Lab Sample Id:
Ground WaterMatrix: MW20Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
08.20.15 09.03 Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
1.80
0.760
0.700
1.13
1.21
1.04
0.600
1.18
1.38
0.690
1.03
1.80
0.940
0.900
1.22
0.870
0.980
1.33
0.670
0.970
3.78
0.880
3.52
0.900
0.890
2.53
3.52
11.9
1.32
1.12
1.24
1.59
0.970
0.990
1.05
1.77
0.420
1.72
0.850
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
UX
U
U
U
U
U
DX
U
U
U
U
U
U
U
U
U
U
U
10.0
5.00
5.00
5.00
5.00
5.00
5.00
20.0
10.0
10.0
5.00
10.0
5.00
5.00
5.00
5.00
5.00
5.00
5.00
2.00
200
2.00
4.00
5.00
5.00
4.00
20.0
50.0
5.00
5.00
5.00
20.0
10.0
5.00
5.00
5.00
5.00
5.00
5.00
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
100
10
10
10
10
10
10
10
10
10
10
10
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
801
U
U
U
U
239
U
U
U
U
U
U
U
U
U
U
U
4020
U
U
U
U
U
U
U
U
U
U
U
975121Seq Number:
RL MDL
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.28
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
Analysis Date
% Moisture:
Page 15 of 43 Final 1.000
Certificate of Analytical Results 513506
Terraquest Environmental Consultants, P.C., Mebane, NC
Chambers Store
08.14.15 09.50 Date Received:
08.13.15 13.20 Date Collected:513506-003Lab Sample Id:
Ground WaterMatrix: MW20Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
08.20.15 09.03 Date Prep:
MWETech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
1.14
1.00
0.670
30.0
9.20
0.920
0.980
1.69
1.90
0.940
0.600
0.650
0.920
0.740
0.890
0.540
0.570
1.88
1.10
1.39
0.540
7.20
0.810
17.6
1.22
Result
U
U
U
U
DX
U
UX
U
U
U
U
U
U
U
U
DX
5.00
10.0
10.0
500
50.0
5.00
5.00
5.00
5.00
20.0
20.0
10.0
5.00
5.00
5.00
5.00
5.00
5.00
10.0
5.00
5.00
10.0
5.00
100
5.00
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
10
10
10
10
100
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
100
10
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
1490
128
65.8
349
U
492
U
155
U
20.9
15.8
U
239
U
U
U
U
U
U
2280
131
975121Seq Number:
RL MDL
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.28
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
08.21.15 03.28
08.21.15 03.01
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
103
99
100
08.21.15 03.01
08.21.15 03.01
08.21.15 03.01
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 16 of 43 Final 1.000
Certificate of Analytical Results 513506
Terraquest Environmental Consultants, P.C., Mebane, NC
Chambers Store
08.14.15 09.50 Date Received:
08.13.15 13.26 Date Collected:513506-004Lab Sample Id:
Ground WaterMatrix: MW21Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
08.20.15 09.03 Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
1.80
0.760
0.700
1.13
1.21
1.04
0.600
1.18
1.38
0.690
1.03
1.80
0.940
0.900
1.22
0.870
0.980
1.33
0.670
0.970
3.78
0.880
3.52
0.900
0.890
2.53
3.52
11.9
1.32
1.12
1.24
1.59
0.970
0.990
1.05
1.77
0.420
1.72
0.850
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
J
U
U
U
U
U
D
U
U
U
U
U
U
U
U
U
U
U
10.0
5.00
5.00
5.00
5.00
5.00
5.00
20.0
10.0
10.0
5.00
10.0
5.00
5.00
5.00
5.00
5.00
5.00
5.00
2.00
200
2.00
4.00
5.00
5.00
4.00
20.0
50.0
5.00
5.00
5.00
20.0
10.0
5.00
5.00
5.00
5.00
5.00
5.00
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
100
10
10
10
10
10
10
10
10
10
10
10
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
298
U
U
U
U
75.9
U
U
U
U
16.0
U
U
U
U
U
67.0
4090
U
U
U
U
U
U
U
U
U
U
U
975121Seq Number:
RL MDL
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 04.21
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
Analysis Date
% Moisture:
Page 17 of 43 Final 1.000
Certificate of Analytical Results 513506
Terraquest Environmental Consultants, P.C., Mebane, NC
Chambers Store
08.14.15 09.50 Date Received:
08.13.15 13.26 Date Collected:513506-004Lab Sample Id:
Ground WaterMatrix: MW21Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
08.20.15 09.03 Date Prep:
MWETech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
1.14
1.00
0.670
30.0
0.920
0.920
0.980
1.69
1.90
0.940
0.600
0.650
0.920
0.740
0.890
0.540
0.570
1.88
1.10
1.39
0.540
7.20
0.810
1.76
1.22
Result
U
U
U
U
J
U
U
U
U
U
U
U
U
U
U
U
5.00
10.0
10.0
500
5.00
5.00
5.00
5.00
5.00
20.0
20.0
10.0
5.00
5.00
5.00
5.00
5.00
5.00
10.0
5.00
5.00
10.0
5.00
10.0
5.00
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
545
49.9
27.9
48.0
2.30
370
U
52.7
U
U
U
U
248
U
U
U
U
U
U
293
129
975121Seq Number:
RL MDL
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
102
100
98
08.21.15 03.55
08.21.15 03.55
08.21.15 03.55
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 18 of 43 Final 1.000
Certificate of Analytical Results 513506
Terraquest Environmental Consultants, P.C., Mebane, NC
Chambers Store
08.14.15 09.50 Date Received:
08.13.15 13.35 Date Collected:513506-005Lab Sample Id:
Ground WaterMatrix: MW22Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
08.20.15 09.03 Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
18.0
7.60
7.00
11.3
12.1
10.4
6.00
11.8
13.8
6.90
10.3
18.0
9.40
9.00
12.2
8.70
9.80
13.3
6.70
9.70
37.8
8.80
35.2
9.00
8.90
25.3
35.2
11.9
13.2
11.2
12.4
15.9
9.70
9.90
10.5
17.7
4.20
17.2
8.50
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
100
50.0
50.0
50.0
50.0
50.0
50.0
200
100
100
50.0
100
50.0
50.0
50.0
50.0
50.0
50.0
50.0
20.0
2000
20.0
40.0
50.0
50.0
40.0
200
50.0
50.0
50.0
50.0
200
100
50.0
50.0
50.0
50.0
50.0
50.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
2360
U
U
U
U
573
U
U
U
U
U
U
U
U
U
U
U
3610
U
U
U
U
U
U
U
U
U
U
U
975121Seq Number:
RL MDL
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
Analysis Date
% Moisture:
Page 19 of 43 Final 1.000
Certificate of Analytical Results 513506
Terraquest Environmental Consultants, P.C., Mebane, NC
Chambers Store
08.14.15 09.50 Date Received:
08.13.15 13.35 Date Collected:513506-005Lab Sample Id:
Ground WaterMatrix: MW22Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
08.20.15 09.03 Date Prep:
MWETech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
11.4
10.0
6.70
300
9.20
9.20
9.80
16.9
19.0
9.40
6.00
6.50
9.20
7.40
8.90
5.40
28.5
18.8
11.0
13.9
5.40
72.0
8.10
17.6
12.2
Result
U
U
U
U
U
U
U
U
U
U
U
U
D
U
U
U
U
U
U
50.0
100
100
5000
50.0
50.0
50.0
50.0
50.0
200
200
100
50.0
50.0
50.0
50.0
250
50.0
100
50.0
50.0
100
50.0
100
50.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
500
100
100
100
100
100
100
100
100
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
2570
U
U
U
U
1070
U
188
U
340
U
U
42500
U
U
U
U
U
U
11000
5420
975121Seq Number:
RL MDL
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 05.16
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
99
100
97
08.21.15 04.48
08.21.15 04.48
08.21.15 04.48
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 20 of 43 Final 1.000
Certificate of Analytical Results 513506
Terraquest Environmental Consultants, P.C., Mebane, NC
Chambers Store
08.14.15 09.50 Date Received:
08.13.15 13.47 Date Collected:513506-006Lab Sample Id:
Ground WaterMatrix: MW23Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
08.20.15 09.03 Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
18.0
7.60
7.00
11.3
12.1
10.4
6.00
11.8
13.8
6.90
10.3
18.0
9.40
9.00
12.2
8.70
9.80
13.3
6.70
9.70
37.8
8.80
35.2
9.00
8.90
25.3
35.2
59.5
13.2
11.2
12.4
15.9
9.70
9.90
10.5
17.7
4.20
17.2
8.50
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
D
U
U
U
U
U
U
U
U
U
U
U
100
50.0
50.0
50.0
50.0
50.0
50.0
200
100
100
50.0
100
50.0
50.0
50.0
50.0
50.0
50.0
50.0
20.0
2000
20.0
40.0
50.0
50.0
40.0
200
250
50.0
50.0
50.0
200
100
50.0
50.0
50.0
50.0
50.0
50.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
500
100
100
100
100
100
100
100
100
100
100
100
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
1680
U
U
U
U
423
U
U
U
U
3400
U
U
U
U
U
269
23000
U
U
U
U
U
U
U
U
U
U
U
975121Seq Number:
RL MDL
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 06.09
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
Analysis Date
% Moisture:
Page 21 of 43 Final 1.000
Certificate of Analytical Results 513506
Terraquest Environmental Consultants, P.C., Mebane, NC
Chambers Store
08.14.15 09.50 Date Received:
08.13.15 13.47 Date Collected:513506-006Lab Sample Id:
Ground WaterMatrix: MW23Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
08.20.15 09.03 Date Prep:
MWETech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
11.4
10.0
6.70
300
9.20
9.20
9.80
16.9
19.0
9.40
6.00
6.50
9.20
7.40
8.90
5.40
28.5
18.8
11.0
13.9
5.40
72.0
8.10
17.6
12.2
Result
U
U
U
U
U
U
U
U
U
U
U
D
U
U
U
U
U
U
50.0
100
100
5000
50.0
50.0
50.0
50.0
50.0
200
200
100
50.0
50.0
50.0
50.0
250
50.0
100
50.0
50.0
100
50.0
100
50.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
500
100
100
100
100
100
100
100
100
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
2190
865
U
807
U
795
U
212
U
U
U
U
22900
U
U
U
U
U
U
7840
3680
975121Seq Number:
RL MDL
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 06.09
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
100
99
97
08.21.15 05.43
08.21.15 05.43
08.21.15 05.43
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 22 of 43 Final 1.000
Certificate of Analytical Results 513506
Terraquest Environmental Consultants, P.C., Mebane, NC
Chambers Store
08.14.15 09.50 Date Received:
08.13.15 13.54 Date Collected:513506-007Lab Sample Id:
Ground WaterMatrix: MW24Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
08.20.15 09.03 Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
18.0
7.60
7.00
11.3
12.1
10.4
6.00
11.8
13.8
6.90
10.3
18.0
9.40
9.00
12.2
8.70
9.80
13.3
6.70
9.70
37.8
8.80
35.2
9.00
8.90
25.3
35.2
59.5
13.2
11.2
12.4
15.9
9.70
9.90
10.5
17.7
4.20
17.2
8.50
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
D
U
U
U
U
U
U
U
U
U
U
U
100
50.0
50.0
50.0
50.0
50.0
50.0
200
100
100
50.0
100
50.0
50.0
50.0
50.0
50.0
50.0
50.0
20.0
2000
20.0
40.0
50.0
50.0
40.0
200
250
50.0
50.0
50.0
200
100
50.0
50.0
50.0
50.0
50.0
50.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
500
100
100
100
100
100
100
100
100
100
100
100
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
1870
U
U
U
U
464
U
U
U
U
5760
U
U
U
U
U
627
22100
U
U
U
U
U
U
U
U
U
U
U
975121Seq Number:
RL MDL
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 07.03
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
Analysis Date
% Moisture:
Page 23 of 43 Final 1.000
Certificate of Analytical Results 513506
Terraquest Environmental Consultants, P.C., Mebane, NC
Chambers Store
08.14.15 09.50 Date Received:
08.13.15 13.54 Date Collected:513506-007Lab Sample Id:
Ground WaterMatrix: MW24Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
08.20.15 09.03 Date Prep:
MWETech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
11.4
10.0
6.70
300
9.20
9.20
9.80
16.9
19.0
9.40
6.00
6.50
9.20
7.40
8.90
5.40
28.5
18.8
11.0
13.9
5.40
72.0
8.10
17.6
12.2
Result
U
U
U
U
U
U
U
U
U
U
U
D
U
U
U
U
U
U
50.0
100
100
5000
50.0
50.0
50.0
50.0
50.0
200
200
100
50.0
50.0
50.0
50.0
250
50.0
100
50.0
50.0
100
50.0
100
50.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
500
100
100
100
100
100
100
100
100
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
2700
2680
U
6010
U
891
U
209
U
U
U
U
37600
U
U
U
U
U
U
9920
4740
975121Seq Number:
RL MDL
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 07.03
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
96
99
96
08.21.15 06.36
08.21.15 06.36
08.21.15 06.36
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 24 of 43 Final 1.000
Certificate of Analytical Results 513506
Terraquest Environmental Consultants, P.C., Mebane, NC
Chambers Store
08.14.15 09.50 Date Received:
08.13.15 14.02 Date Collected:513506-008Lab Sample Id:
Ground WaterMatrix: MW25Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
08.20.15 09.03 Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
1.80
0.760
0.700
1.13
1.21
1.04
0.600
1.18
1.38
0.690
10.3
1.80
0.940
0.900
1.22
0.870
0.980
1.33
0.670
0.970
3.78
0.880
3.52
0.900
0.890
2.53
3.52
1.19
1.32
1.12
1.24
1.59
0.970
0.990
1.05
1.77
0.420
1.72
0.850
Result
U
U
U
U
U
U
U
U
U
U
D
U
U
U
U
U
U
U
U
J
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
10.0
5.00
5.00
5.00
5.00
5.00
5.00
20.0
10.0
10.0
50.0
10.0
5.00
5.00
5.00
5.00
5.00
5.00
5.00
2.00
200
2.00
4.00
5.00
5.00
4.00
20.0
5.00
5.00
5.00
5.00
20.0
10.0
5.00
5.00
5.00
5.00
5.00
5.00
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
10
10
10
10
10
10
10
10
10
10
100
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
2280
U
U
U
U
624
U
U
U
U
42.4
U
162
U
U
U
U
175
U
U
U
U
U
U
U
U
U
U
U
975121Seq Number:
RL MDL
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.56
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
Analysis Date
% Moisture:
Page 25 of 43 Final 1.000
Certificate of Analytical Results 513506
Terraquest Environmental Consultants, P.C., Mebane, NC
Chambers Store
08.14.15 09.50 Date Received:
08.13.15 14.02 Date Collected:513506-008Lab Sample Id:
Ground WaterMatrix: MW25Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
08.20.15 09.03 Date Prep:
MWETech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
1.14
1.00
0.670
30.0
9.20
0.920
0.980
1.69
1.90
0.940
0.600
0.650
0.920
0.740
0.890
0.540
5.70
1.88
1.10
1.39
0.540
7.20
0.810
17.6
12.2
Result
U
U
U
U
D
U
U
U
U
U
U
D
U
U
U
U
U
U
D
D
5.00
10.0
10.0
500
50.0
5.00
5.00
5.00
5.00
20.0
20.0
10.0
5.00
5.00
5.00
5.00
50.0
5.00
10.0
5.00
5.00
10.0
5.00
100
50.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
10
10
10
10
100
10
10
10
10
10
10
10
10
10
10
10
100
10
10
10
10
10
10
100
100
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
915
U
94.2
U
U
697
U
241
11.5
U
31.9
U
3400
U
U
U
U
U
U
3920
2530
975121Seq Number:
RL MDL
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.56
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.56
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
08.21.15 07.56
08.21.15 07.56
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
96
99
97
08.21.15 07.29
08.21.15 07.29
08.21.15 07.29
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 26 of 43 Final 1.000
Certificate of Analytical Results 513506
Terraquest Environmental Consultants, P.C., Mebane, NC
Chambers Store
08.14.15 09.50 Date Received:
08.13.15 14.15 Date Collected:513506-009Lab Sample Id:
Ground WaterMatrix: MW26Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
08.20.15 09.03 Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
Parameter
18.0
7.60
7.00
11.3
12.1
10.4
6.00
11.8
13.8
6.90
10.3
18.0
9.40
9.00
12.2
8.70
9.80
13.3
6.70
9.70
37.8
8.80
35.2
9.00
8.90
25.3
35.2
59.5
13.2
11.2
12.4
15.9
9.70
9.90
10.5
17.7
4.20
17.2
8.50
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
D
U
U
U
U
U
U
U
U
U
U
U
100
50.0
50.0
50.0
50.0
50.0
50.0
200
100
100
50.0
100
50.0
50.0
50.0
50.0
50.0
50.0
50.0
20.0
2000
20.0
40.0
50.0
50.0
40.0
200
250
50.0
50.0
50.0
200
100
50.0
50.0
50.0
50.0
50.0
50.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
500
100
100
100
100
100
100
100
100
100
100
100
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
U
U
U
U
U
U
U
U
U
U
2240
343
U
528
U
569
U
U
U
U
2060
U
U
U
U
U
U
10300
U
U
U
U
U
U
U
U
U
U
U
975121Seq Number:
RL MDL
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.48
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
Analysis Date
% Moisture:
Page 27 of 43 Final 1.000
Certificate of Analytical Results 513506
Terraquest Environmental Consultants, P.C., Mebane, NC
Chambers Store
08.14.15 09.50 Date Received:
08.13.15 14.15 Date Collected:513506-009Lab Sample Id:
Ground WaterMatrix: MW26Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
08.20.15 09.03 Date Prep:
MWETech:
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
11.4
10.0
6.70
300
9.20
9.20
9.80
16.9
19.0
9.40
6.00
6.50
9.20
7.40
8.90
5.40
28.5
18.8
11.0
13.9
5.40
72.0
8.10
17.6
12.2
Result
U
U
U
U
U
U
U
U
U
U
U
D
U
U
U
U
U
U
50.0
100
100
5000
50.0
50.0
50.0
50.0
50.0
200
200
100
50.0
50.0
50.0
50.0
250
50.0
100
50.0
50.0
100
50.0
100
50.0
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
500
100
100
100
100
100
100
100
100
DilCas Number
156-59-2
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
3290
1130
U
282
U
971
U
277
U
U
U
U
30200
U
U
U
U
U
U
11700
5450
975121Seq Number:
RL MDL
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.48
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
Analysis Date
Surrogate
65-126
86-111
83-116
%
Recovery Flag
%
%
%
94
100
98
08.21.15 08.22
08.21.15 08.22
08.21.15 08.22
Cas Number
17060-07-0
460-00-4
2037-26-5
Units Analysis Date
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Limits
% Moisture:
Page 28 of 43 Final 1.000
QC Summary 513506
Terraquest Environmental Consultants, P.C.
Chambers Store
696985-1-BLKMB Sample Id:
WaterMatrix:
VOCs by GC/MS by SM6200B Analytical Method:SM6200B_PREPPrep Method:
08.20.15Date Prep:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Parameter %RPD Flag
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
7
14
6
4
11
12
10
8
19
6
5
2
9
3
1
5
5
2
6
5
5
4
1
4
6
6
9
6
3
7
6
1
4
12
6
2
4
9
6
8
1
9
11
5
7
3
6
2
5
7
3
6
975118Seq Number:
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
Analysis
Date
Limits
75-127
62-128
77-129
86-120
82-114
73-123
83-125
57-127
79-118
59-125
84-118
83-126
83-128
56-133
85-121
86-118
90-126
85-121
88-121
76-126
66-133
80-128
70-130
82-130
80-128
74-129
51-143
81-123
84-114
89-127
79-129
73-140
53-143
66-136
88-118
73-139
70-123
72-118
65-125
85-125
92-126
48-143
61-133
87-123
77-125
82-115
53-149
75-119
52-116
83-130
84-122
86-120
LCSD
%Rec
106
101
98
96
101
105
107
94
104
96
92
100
91
101
101
93
92
96
91
106
104
92
105
92
93
99
111
99
92
113
113
116
104
108
92
98
95
101
100
100
106
109
108
95
109
92
107
119
98
95
92
90
LCSD
Result
26.4
25.2
24.5
24.1
25.3
26.3
26.7
23.5
26.1
23.9
23.0
25.1
22.7
25.2
25.3
23.3
23.1
24.1
22.7
26.6
52.2
22.9
52.5
23.0
23.3
49.4
55.4
24.7
23.1
28.3
28.3
29.1
26.1
27.1
23.1
24.5
23.8
25.2
25.1
24.9
26.6
27.3
1080
23.7
27.3
23.1
53.7
29.8
24.5
23.7
22.9
22.5
LCS
%Rec
113
116
104
100
113
119
118
102
86
102
97
102
99
104
102
98
98
98
96
112
110
95
104
96
99
105
121
105
96
122
120
117
109
122
98
100
99
111
106
108
108
120
121
100
117
95
114
117
103
102
95
96
28.3
29.0
26.0
25.0
28.2
29.8
29.6
25.4
21.6
25.5
24.3
25.6
24.8
26.0
25.6
24.4
24.4
24.5
24.0
28.1
54.9
23.8
51.9
24.0
24.8
52.6
60.6
26.3
23.9
30.4
30.1
29.3
27.2
30.6
24.6
25.0
24.7
27.7
26.6
27.0
26.9
29.9
1210
24.9
29.2
23.7
56.8
29.2
25.8
25.5
23.7
23.9
Spike
Amount
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
50.0
25.0
25.0
50.0
50.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
1000
25.0
25.0
25.0
50.0
25.0
25.0
25.0
25.0
25.0
MB
Result
<0.180
<0.0760
<0.0700
<0.113
<0.121
<0.104
<0.0600
<0.118
<0.138
<0.0690
<0.103
<0.180
<0.0940
<0.0900
<0.122
<0.0870
<0.0980
<0.133
<0.0670
<0.0970
<0.378
<0.0880
<0.352
<0.0900
<0.0890
<0.253
<0.352
<0.119
<0.132
<0.112
<0.124
<0.159
<0.0970
<0.0990
<0.105
<0.177
<0.0420
<0.172
<0.0850
<0.114
<0.100
<0.0670
<3.00
<0.0920
<0.0920
<0.0980
<0.169
<0.190
<0.0940
<0.0600
<0.0650
<0.0920
696985-1-BKSLCS Sample Id:696985-1-BSDLCSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsLCS
Result
Page 29 of 43 Final 1.000
QC Summary 513506
Terraquest Environmental Consultants, P.C.
Chambers Store
696985-1-BLKMB Sample Id:
WaterMatrix:
VOCs by GC/MS by SM6200B Analytical Method:SM6200B_PREPPrep Method:
08.20.15Date Prep:
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter %RPD Flag
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
7
3
0
7
8
3
10
2
4
4
7
9
975118Seq Number:
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
Analysis
Date
Limits
85-123
79-126
64-131
89-116
78-118
86-127
82-119
46-144
58-141
76-122
90-125
86-119
LCSD
%Rec
97
92
104
93
110
89
91
118
107
106
94
94
LCSD
Result
24.3
22.9
26.1
23.2
27.4
22.2
22.8
29.5
26.8
26.5
46.9
23.5
LCS
%Rec
104
95
104
100
102
92
100
120
112
110
100
103
26.1
23.7
26.1
25.0
25.4
22.9
25.1
30.0
27.9
27.6
50.2
25.7
Spike
Amount
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
MB
Result
<0.0740
<0.0890
<0.0540
<0.0570
<0.188
<0.110
<0.139
<0.0540
<0.720
<0.0810
<0.176
<0.122
696985-1-BKSLCS Sample Id:696985-1-BSDLCSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsLCS
Result
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Surrogate LCSD
Flag
08.20.15 10:03
08.20.15 10:03
08.20.15 10:03
Analysis
Date
Limits
65-126
86-111
83-116
LCSD
%Rec
99
99
97
LCS
%Rec
100
97
99
MB
%Rec
102
104
96
%
%
%
UnitsLCS
Flag
MB
Flag
Page 30 of 43 Final 1.000
QC Summary 513506
Terraquest Environmental Consultants, P.C.
Chambers Store
696986-1-BLKMB Sample Id:
WaterMatrix:
VOCs by GC/MS by SM6200B Analytical Method:SM6200B_PREPPrep Method:
08.20.15Date Prep:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Parameter %RPD Flag
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
0
13
1
1
1
1
3
3
8
0
0
1
2
2
2
0
0
2
2
1
5
0
4
2
1
5
1
0
1
4
0
2
1
3
1
2
0
10
4
1
2
1
5
0
1
0
2
16
3
1
0
0
975121Seq Number:
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
Analysis
Date
Limits
75-127
62-128
77-129
86-120
82-114
73-123
83-125
57-127
79-118
59-125
84-118
83-126
83-128
56-133
85-121
86-118
90-126
85-121
88-121
76-126
66-133
80-128
70-130
82-130
80-128
74-129
51-143
81-123
84-114
89-127
79-129
73-140
53-143
66-136
88-118
73-139
70-123
72-118
65-125
85-125
92-126
48-143
61-133
87-123
77-125
82-115
53-149
75-119
52-116
83-130
84-122
86-120
LCSD
%Rec
107
107
102
102
99
96
104
97
92
97
92
104
95
99
103
94
96
104
93
86
109
94
115
92
93
117
107
102
96
114
116
117
95
110
96
103
100
109
87
103
114
75
119
98
107
94
104
110
103
94
94
92
LCSD
Result
26.7
26.7
25.6
25.5
24.7
23.9
26.1
24.3
22.9
24.3
22.9
26.1
23.7
24.7
25.7
23.5
24.0
26.0
23.2
21.5
54.7
23.5
57.3
23.1
23.3
58.3
53.7
25.6
24.0
28.5
29.0
29.3
23.8
27.6
24.1
25.8
25.1
27.3
21.8
25.8
28.4
18.8
1190
24.6
26.7
23.6
52.1
27.5
25.8
23.4
23.5
23.1
LCS
%Rec
107
94
103
103
98
97
101
100
100
97
92
105
96
101
105
94
96
106
95
85
115
94
119
94
94
122
106
103
95
118
116
115
96
108
98
101
101
99
84
102
116
74
113
99
106
94
103
94
106
94
94
92
26.7
23.5
25.8
25.8
24.5
24.2
25.3
25.0
24.9
24.2
23.0
26.3
24.1
25.3
26.2
23.4
24.0
26.4
23.7
21.2
57.3
23.6
59.4
23.5
23.5
61.1
53.2
25.7
23.8
29.6
28.9
28.8
24.1
26.9
24.4
25.3
25.2
24.8
21.0
25.5
28.9
18.6
1130
24.7
26.4
23.6
51.3
23.4
26.5
23.6
23.6
23.0
Spike
Amount
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
50.0
25.0
25.0
50.0
50.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
1000
25.0
25.0
25.0
50.0
25.0
25.0
25.0
25.0
25.0
MB
Result
<0.180
<0.0760
<0.0700
<0.113
<0.121
<0.104
<0.0600
<0.118
<0.138
<0.0690
<0.103
<0.180
<0.0940
<0.0900
<0.122
<0.0870
<0.0980
<0.133
<0.0670
<0.0970
<0.378
<0.0880
<0.352
<0.0900
<0.0890
<0.253
<0.352
<0.119
<0.132
<0.112
<0.124
<0.159
<0.0970
<0.0990
<0.105
<0.177
<0.0420
<0.172
<0.0850
<0.114
<0.100
<0.0670
<3.00
<0.0920
<0.0920
<0.0980
<0.169
<0.190
<0.0940
<0.0600
<0.0650
<0.0920
696986-1-BKSLCS Sample Id:696986-1-BSDLCSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsLCS
Result
Page 31 of 43 Final 1.000
QC Summary 513506
Terraquest Environmental Consultants, P.C.
Chambers Store
696986-1-BLKMB Sample Id:
WaterMatrix:
VOCs by GC/MS by SM6200B Analytical Method:SM6200B_PREPPrep Method:
08.20.15Date Prep:
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter %RPD Flag
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
1
0
0
1
1
2
0
1
5
2
1
0
975121Seq Number:
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
Analysis
Date
Limits
85-123
79-126
64-131
89-116
78-118
86-127
82-119
46-144
58-141
76-122
90-125
86-119
LCSD
%Rec
101
94
100
97
100
95
94
104
113
90
97
97
LCSD
Result
25.2
23.4
24.9
24.2
24.9
23.7
23.6
25.9
28.3
22.5
48.5
24.3
LCS
%Rec
102
94
100
98
101
97
94
103
119
88
98
97
25.4
23.5
25.0
24.5
25.2
24.2
23.6
25.7
29.7
22.0
48.8
24.3
Spike
Amount
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
MB
Result
<0.0740
<0.0890
<0.0540
<0.0570
<0.188
<0.110
<0.139
<0.0540
<0.720
<0.0810
<0.176
<0.122
696986-1-BKSLCS Sample Id:696986-1-BSDLCSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsLCS
Result
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Surrogate LCSD
Flag
08.21.15 00:19
08.21.15 00:19
08.21.15 00:19
Analysis
Date
Limits
65-126
86-111
83-116
LCSD
%Rec
96
99
97
LCS
%Rec
98
99
98
MB
%Rec
97
100
97
%
%
%
UnitsLCS
Flag
MB
Flag
Page 32 of 43 Final 1.000
QC Summary 513506
Terraquest Environmental Consultants, P.C.
Chambers Store
513500-004Parent Sample Id:
Ground WaterMatrix:
VOCs by GC/MS by SM6200B Analytical Method:SM6200B_PREPPrep Method:
08.20.15Date Prep:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Parameter %RPD
X
X
XF
X
Flag
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
1
3
4
0
3
0
5
2
3
4
7
0
5
2
4
6
6
1
5
1
200
6
0
8
4
12
2
5
5
3
4
1
6
1
1
0
2
2
3
5
0
4
11
2
2
7
0
5
6
6
8
7
975118Seq Number:
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
Analysis
Date
Limits
76-126
63-128
79-133
82-126
77-120
67-123
76-126
41-136
77-125
41-132
53-141
82-130
83-128
59-134
79-125
69-125
83-126
85-124
82-121
56-122
66-136
73-129
63-140
76-129
73-126
71-140
47-138
70-135
76-120
83-132
66-132
63-143
60-134
59-139
83-120
68-140
67-125
72-120
59-128
80-125
74-122
48-138
55-140
70-140
77-125
75-117
51-155
75-119
34-135
73-128
75-125
77-122
MSD
%Rec
92
88
99
97
86
90
93
88
92
84
78
98
83
92
92
79
80
94
79
82
0
78
116
77
80
108
112
88
82
103
100
107
90
90
82
90
84
88
86
86
94
98
103
83
99
77
102
86
97
81
78
77
MSD
Result
23.1
22.1
24.8
24.2
21.5
22.6
23.2
22.0
22.9
21.1
19.6
24.5
20.7
23.0
22.9
19.7
19.9
23.6
19.7
20.4
<0.378
19.4
58.0
19.2
20.0
53.8
55.8
22.1
20.6
25.8
25.1
26.8
22.6
22.4
20.6
22.4
20.9
21.9
21.5
21.4
23.5
24.4
1030
20.8
24.7
19.3
50.8
21.6
24.3
20.3
19.4
19.2
MS
%Rec
94
91
103
97
89
90
98
90
94
88
84
98
87
94
95
84
85
96
83
80
117
82
116
83
84
122
113
93
87
106
104
106
96
91
83
90
85
90
89
90
94
102
115
85
101
83
101
82
104
86
84
82
23.4
22.8
25.8
24.3
22.2
22.6
24.4
22.5
23.6
21.9
21.0
24.4
21.8
23.4
23.8
20.9
21.2
23.9
20.8
20.1
58.4
20.5
57.9
20.7
20.9
60.8
56.7
23.2
21.7
26.5
26.1
26.5
23.9
22.7
20.8
22.5
21.3
22.4
22.2
22.4
23.5
25.5
1150
21.3
25.3
20.8
50.6
20.5
25.9
21.6
21.0
20.6
Spike
Amount
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
50.0
25.0
25.0
50.0
50.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
1000
25.0
25.0
25.0
50.0
25.0
25.0
25.0
25.0
25.0
Parent
Result
<0.180
<0.0760
<0.0700
<0.113
<0.121
<0.104
<0.0600
<0.118
<0.138
<0.0690
<0.103
<0.180
<0.0940
<0.0900
<0.122
<0.0870
<0.0980
<0.133
<0.0670
<0.0970
<0.378
<0.0880
<0.352
<0.0900
<0.0890
<0.253
<0.352
<0.119
<0.132
<0.112
<0.124
<0.159
<0.0970
<0.0990
<0.105
<0.177
<0.0420
<0.172
<0.0850
<0.114
<0.100
<0.0670
<3.00
<0.0920
<0.0920
<0.0980
<0.169
<0.190
<0.0940
<0.0600
<0.0650
<0.0920
513500-004 SMS Sample Id:513500-004 SDMSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsMS
Result
Page 33 of 43 Final 1.000
QC Summary 513506
Terraquest Environmental Consultants, P.C.
Chambers Store
513500-004Parent Sample Id:
Ground WaterMatrix:
VOCs by GC/MS by SM6200B Analytical Method:SM6200B_PREPPrep Method:
08.20.15Date Prep:
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter %RPD Flag
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
0
6
4
4
0
0
4
3
7
2
3
3
975118Seq Number:
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
Analysis
Date
Limits
54-137
74-124
57-130
81-125
69-122
73-129
73-124
49-139
57-134
70-121
65-151
58-148
MSD
%Rec
85
79
84
82
94
80
83
94
94
84
82
81
MSD
Result
21.3
19.8
21.1
20.6
23.5
20.1
20.8
23.6
23.5
21.1
40.8
20.3
MS
%Rec
86
84
88
86
94
80
87
92
100
86
84
84
21.4
21.0
22.0
21.4
23.6
20.1
21.7
23.0
25.1
21.6
42.0
21.0
Spike
Amount
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
Parent
Result
<0.0740
<0.0890
<0.0540
<0.0570
<0.188
<0.110
<0.139
<0.0540
<0.720
<0.0810
<0.176
<0.122
513500-004 SMS Sample Id:513500-004 SDMSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsMS
Result
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Surrogate MSD
Flag
08.20.15 20:22
08.20.15 20:22
08.20.15 20:22
Analysis
Date
Limits
65-126
86-111
83-116
MSD
%Rec
98
98
98
MS
%Rec
99
101
96
%
%
%
UnitsMS
Flag
Page 34 of 43 Final 1.000
QC Summary 513506
Terraquest Environmental Consultants, P.C.
Chambers Store
513506-003Parent Sample Id:
Ground WaterMatrix:
VOCs by GC/MS by SM6200B Analytical Method:SM6200B_PREPPrep Method:
08.20.15Date Prep:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Parameter %RPD
X
X
X
X
Flag
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
4
1
2
4
6
5
5
1
1
3
5
1
5
2
4
4
3
3
5
4
4
5
2
5
3
9
3
3
6
4
5
5
4
4
4
5
8
7
2
0
1
3
2
5
6
5
2
5
1
4
5
4
975121Seq Number:
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
Analysis
Date
Limits
76-126
63-128
79-133
82-126
77-120
67-123
76-126
41-136
77-125
41-132
53-141
82-130
83-128
59-134
79-125
69-125
83-126
85-124
82-121
56-122
66-136
73-129
63-140
76-129
73-126
71-140
47-138
70-135
76-120
83-132
66-132
63-143
60-134
59-139
83-120
68-140
67-125
72-120
59-128
80-125
74-122
48-138
55-140
70-140
77-125
75-117
51-155
75-119
34-135
73-128
75-125
77-122
MSD
%Rec
94
104
91
93
96
90
97
87
81
89
66
95
88
94
98
82
90
94
86
93
104
126
99
98
90
95
102
0
87
106
109
111
96
99
90
93
100
108
86
100
107
73
102
40
99
87
94
111
80
20
84
91
MSD
Result
236
260
228
233
239
226
242
218
202
223
965
238
220
235
246
445
225
236
216
232
519
315
497
244
226
477
508
4020
218
266
273
277
240
247
225
232
249
270
215
251
268
183
10200
1610
376
284
818
278
693
51.0
366
227
MS
%Rec
98
103
93
97
101
95
102
88
82
92
84
96
93
96
102
90
93
97
91
97
99
132
101
103
94
104
99
44
92
111
114
117
100
103
94
97
108
101
88
100
109
75
100
72
108
94
97
117
84
21
92
95
246
258
232
243
253
238
254
221
205
229
1010
241
232
240
255
464
232
242
228
242
497
330
507
257
234
520
493
4140
231
278
286
292
250
257
235
243
269
253
220
250
272
188
9950
1690
399
300
836
293
702
53.3
385
237
Spike
Amount
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
500
250
500
250
250
500
500
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
10000
250
250
250
500
250
250
250
250
250
Parent
Result
<1.80
<0.760
<0.700
<1.13
<1.21
<1.04
<0.600
<1.18
<1.38
<0.690
801
<1.80
<0.940
<0.900
<1.22
239
<0.980
<1.33
<0.670
<0.970
<3.78
<0.880
<3.52
<0.900
<0.890
<2.53
<3.52
4030
<1.32
<1.12
<1.24
<1.59
<0.970
<0.990
<1.05
<1.77
<0.420
<1.72
<0.850
<1.14
<1.00
<0.670
<30.0
1510
128
65.8
349
<1.90
492
<0.600
155
<0.920
513506-003 SMS Sample Id:513506-003 SDMSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsMS
Result
Page 35 of 43 Final 1.000
QC Summary 513506
Terraquest Environmental Consultants, P.C.
Chambers Store
513506-003Parent Sample Id:
Ground WaterMatrix:
VOCs by GC/MS by SM6200B Analytical Method:SM6200B_PREPPrep Method:
08.20.15Date Prep:
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter %RPD
X
Flag
20
20
20
20
20
20
20
20
20
20
20
20
RPD
Limit
4
4
5
4
5
1
5
7
5
0
4
5
975121Seq Number:
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
Analysis
Date
Limits
54-137
74-124
57-130
81-125
69-122
73-129
73-124
49-139
57-134
70-121
65-151
58-148
MSD
%Rec
94
82
92
83
94
88
89
87
107
86
50
87
MSD
Result
256
222
230
446
236
220
222
217
268
216
2430
349
MS
%Rec
98
86
96
90
99
89
93
81
113
87
70
94
266
231
241
465
248
222
233
203
283
217
2530
366
Spike
Amount
250
250
250
250
250
250
250
250
250
250
500
250
Parent
Result
20.9
15.8
<0.540
239
<1.88
<1.10
<1.39
<0.540
<7.20
<0.810
2180
131
513506-003 SMS Sample Id:513506-003 SDMSD Sample Id:
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UnitsMS
Result
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Surrogate MSD
Flag
08.21.15 10:13
08.21.15 10:13
08.21.15 10:13
Analysis
Date
Limits
65-126
86-111
83-116
MSD
%Rec
100
98
98
MS
%Rec
96
100
98
%
%
%
UnitsMS
Flag
Page 36 of 43 Final 1.000
Blank Summary 513506
Terraquest Environmental Consultants, P.C., Mebane, NC
Chambers Store
696985-1-BLKLab Sample Id:
WATERMatrix: 696985-1-BLK Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
08.20.15 09:03Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
Parameter
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
0.114
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
0.400
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
156-59-2
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
975118Seq Number:
MDLRL
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
Analysis
Date
Page 37 of 43 Final 1.000
Blank Summary 513506
Terraquest Environmental Consultants, P.C., Mebane, NC
Chambers Store
696985-1-BLKLab Sample Id:
WATERMatrix: 696985-1-BLK Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
08.20.15 09:03Date Prep:
MWETech:
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
0.100
0.0670
3.00
0.0920
0.0920
0.0980
0.169
0.190
0.0940
0.0600
0.0650
0.0920
0.0740
0.0890
0.0540
0.0570
0.188
0.110
0.139
0.0540
0.720
0.0810
0.176
0.122
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
1.00
50.0
0.500
0.500
0.500
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
975118Seq Number:
MDLRL
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
08.20.15 11:50
Analysis
Date
Page 38 of 43 Final 1.000
Blank Summary 513506
Terraquest Environmental Consultants, P.C., Mebane, NC
Chambers Store
696986-1-BLKLab Sample Id:
WATERMatrix: 696986-1-BLK Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
08.20.15 09:03Date Prep:
MWETech:
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
Parameter
0.180
0.0760
0.0700
0.113
0.121
0.104
0.0600
0.118
0.138
0.0690
0.103
0.180
0.0940
0.0900
0.122
0.0870
0.0980
0.133
0.0670
0.0970
0.378
0.0880
0.352
0.0900
0.0890
0.253
0.352
0.119
0.132
0.112
0.124
0.159
0.0970
0.0990
0.105
0.177
0.0420
0.172
0.0850
0.114
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
0.500
0.500
0.500
0.500
0.500
0.500
2.00
1.00
1.00
0.500
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
0.200
20.0
0.200
0.400
0.500
0.500
0.400
2.00
0.500
0.500
0.500
0.500
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
563-58-6
87-61-6
96-18-4
120-82-1
95-63-6
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
142-28-9
106-46-7
594-20-7
78-93-3
95-49-8
591-78-6
106-43-4
99-87-6
108-10-1
67-64-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
56-23-5
108-90-7
124-48-1
75-00-3
67-66-3
74-87-3
156-59-2
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
975121Seq Number:
MDLRL
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
Analysis
Date
Page 39 of 43 Final 1.000
Blank Summary 513506
Terraquest Environmental Consultants, P.C., Mebane, NC
Chambers Store
696986-1-BLKLab Sample Id:
WATERMatrix: 696986-1-BLK Sample Id:
VOCs by GC/MS by SM6200B Analytical Method:
ZHOAnalyst:
SM6200B_PREPPrep Method:
08.20.15 09:03Date Prep:
MWETech:
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Parameter
0.100
0.0670
3.00
0.0920
0.0920
0.0980
0.169
0.190
0.0940
0.0600
0.0650
0.0920
0.0740
0.0890
0.0540
0.0570
0.188
0.110
0.139
0.0540
0.720
0.0810
0.176
0.122
Result
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1.00
1.00
50.0
0.500
0.500
0.500
0.500
0.500
2.00
2.00
1.00
0.500
0.500
0.500
0.500
0.500
0.500
1.00
0.500
0.500
1.00
0.500
1.00
0.500
Flag
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Units
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
DilCas Number
10061-01-5
75-71-8
64-17-5
100-41-4
108-20-3
98-82-8
1634-04-4
75-09-2
91-20-3
104-51-8
103-65-1
135-98-8
100-42-5
98-06-6
127-18-4
108-88-3
156-60-5
10061-02-6
79-01-6
75-69-4
108-05-4
75-01-4
179601-23-1
95-47-6
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
975121Seq Number:
MDLRL
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
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08.21.15 02:07
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08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
08.21.15 02:07
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08.21.15 02:07
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Analysis
Date
Page 40 of 43 Final 1.000
Page 41 of 43 Final 1.000
Page 42 of 43 Final 1.000
Prelogin/Nonconformance Report- Sample Log-In
XENCO Laboratories
513506Work Order #:
08/14/2015 09:50:00 AMDate/ Time Received:
Terraquest Environmental Consultants, PClient:
Sample Receipt Checklist
Checklist completed by: Date:
Checklist reviewed by:Date:
Debbie Simmons
08/15/2015
08/17/2015
#2 *Shipping container in good condition?
#3 *Samples received on ice?
#4 *Custody Seals intact on shipping container/ cooler?
#5 Custody Seals intact on sample bottles?
#6 *Custody Seals Signed and dated?
#7 *Chain of Custody present?
#8 Sample instructions complete on Chain of Custody?
#9 Any missing/extra samples?
#10 Chain of Custody signed when relinquished/ received?
#11 Chain of Custody agrees with sample label(s)?
#12 Container label(s) legible and intact?
#13 Sample matrix/ properties agree with Chain of Custody?
#14 Samples in proper container/ bottle?
#15 Samples properly preserved?
#16 Sample container(s) intact?
#17 Sufficient sample amount for indicated test(s)?
#18 All samples received within hold time?
#19 Subcontract of sample(s)?
#20 VOC samples have zero headspace (less than 1/4 inch bubble)?
#21 <2 for all samples preserved with HNO3,HCL, H2SO4? Except for
samples for the analysis of HEM or HEM-SGT which are verified by the
analysts.
#22 >10 for all samples preserved with NaAsO2+NaOH, ZnAc+NaOH?
Yes
Yes
N/A
N/A
N/A
Yes
Yes
No
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
No
Yes
N/A
N/A

#1 *Temperature of cooler(s)?1.5
Acceptable Temperature Range: 0 - 6 degC
Air and Metal samples Acceptable Range: Ambient
* Must be completed for after-hours delivery of samples prior to placing in the refrigerator
Analyst: PH Device/Lot#:
Comments
Dario Lagunas
Temperature Measuring device used : #61
Page 43 of 43 Final 1.000