1701_CaswellCoMSW_GWMR_20171121

Semi-Annual Monitoring Report
October 2017
Caswell County Landfill Permit No 17-01
Yanceyville, North Carolina
S&ME Project No. 1584-07-034A
PREPARED FOR:
Caswell County
Post Office Box 98
Yanceyville, North Carolina 27379
PREPARED BY:
S&ME, Inc.
8646 West Market Street, Suite 105
Greensboro, NC 27409
November 21, 2017
S&ME, Inc. | 8646 West Market Street, Suite 105 | Greensboro, NC 27409 | p 336.288.7180 | www.smeinc.com
November 21, 2017
Caswell County
P.O. Box 98
Yanceyville, North Carolina 27379
Attention: Mr. Tim Smith
Reference: Semi-Annual Monitoring Report – October 2017
Caswell County Landfill Permit No 17-01
Yanceyville, North Carolina
S&ME Project No. 1584-07-034A
Dear Mr. Smith:
S&ME Inc. (S&ME) has completed the first semi-annual monitoring event for 2017 at the closed Caswell County
Landfill site. The monitoring activities were authorized by Caswell County, County Manager, Mr. Bryan Miller and
were completed in general accordance with S&ME proposal 43-1700189 dated March 7, 2017. This report
summarizes our understanding of the project, our field services, and the results of laboratory analyses performed
on the samples collected. If you have any questions regarding this document, and our associated findings and
recommendations; please contact Edmund Henriques at your convenience.
Sincerely,
S&ME, Inc.
Edmund Q.B. Henriques, PG B. Summers Long
Project Manager / Senior Geologist Staff Scientist
NC Licensed Geologist No. 1216
Semi-Annual Monitoring Report – October 2017
Caswell County Landfill Permit No 17-01
Yanceyville, North Carolina
S&ME Project No. 1584-07-034A
November 21, 2017 1
Table of Contents
1.0 Executive Summary .......................................................................................................... 2
2.0 Introduction ....................................................................................................................... 2
3.0 Scope of Services ............................................................................................................... 3
4.0 Methods Employed ........................................................................................................... 3
4.1 Monitoring Well Sampling ............................................................................................................ 3
4.2 Groundwater Flow Direction ....................................................................................................... 4
4.3 Surface Water Sampling ................................................................................................................ 4
5.0 Results ................................................................................................................................. 5
5.1 Groundwater Analytical Results .................................................................................................. 5
5.1.1 Metals (8-RCRA): ............................................................................................................................. 5
5.1.2 Volatile Organic Compounds: ........................................................................................................... 5
5.2 Surface Water Analytical Results ................................................................................................. 6
5.3 Quality Control ............................................................................................................................... 6
5.4 Preliminary Analysis of Cause and Significance of 2L Exceedances ...................................... 6
6.0 References ........................................................................................................................... 7
Appendices
Appendix I – Figures
Appendix II – Tables
Appendix III – Groundwater Sampling Field Data Sheets
Appendix IV – Laboratory Analytical Report
Appendix V – NCDEQ EDD (CD only)
Semi-Annual Monitoring Report – October 2017
Caswell County Landfill Permit No 17-01
Yanceyville, North Carolina
S&ME Project No. 1584-07-034A
November 21, 2017 2
1.0 Executive Summary
Six monitoring wells at the Caswell County Landfill were sampled on October 30, 2017. The six wells (MW-1, MW-
2, MW-3, MW-4, MW-5, and MW-6) comprise the groundwater monitoring system for the closed Caswell County
Landfill. This sampling event was conducted in general accordance with North Carolina Solid Waste Management
Guidelines. Samples collected from monitoring wells MW-1, MW-2, MW-3, MW-4, MW-5, and MW-6 and surface
water samples SW-1 and SW-2 were submitted for analysis of the North Carolina Landfill Appendix I volatile
organic constituents plus eight RCRA Metals. The samples were analyzed by PACE Analytical Services, Inc., a
North Carolina certified laboratory.
Analytical results of the six groundwater samples report that volatile organic constituent benzene was detected in
monitoring wells MW-2, MW-4, and MW-5 at concentrations greater than the corresponding 15A North Carolina
Administrative Code (NCAC) 2L.0200 groundwater quality standards (2L Standard) of 1 µg/L during this event.
Volatile organic constituent 1,4-dichlorobenzene was detected in the groundwater samples collected from wells
MW-2, MW-4, and MW-5 at concentrations greater than the corresponding 2L Standard of 6 µg/L. During this
event, no other volatile organic compounds were detected in the monitoring wells sampled at concentrations
greater than the corresponding 2L Standards. Utilizing a facility compliance boundary located 500 feet from the
limits of waste or at the property boundary, whichever is closer to the waste, monitoring wells MW-5 and MW-6
would be located outside of the compliance boundary.
During this monitoring event, barium was detected at concentrations greater than the method detection limit in
the two stream sample locations. Barium was detected in up-gradient background surface water sample SW-1
and down-gradient sample SW-2 at similar concentrations. The reported concentrations were below their
respective 15A NCAC 2B Surface Water Standard for Class C surface waters. There were no other metals detected
above the method detection limit in the surface water samples collected during this sampling event.
It is believed that the cause of the 2L Standards exceedances for Benzene and 1,4-Dichlorobenzene at the Caswell
County Landfill is from percolation of landfill constituents from the waste management units into the uppermost
groundwater aquifer. Due to the detection of these exceedances above the 2L Standards in the compliance wells,
S&ME recommends that a water supply well receptor survey be completed for the Caswell County Landfill and the
development of an assessment plan to address the 2L Standards exceedances in accordance with regulatory
requirements.
2.0 Introduction
The Caswell County Landfill (Permit No. 17-01) is located at 162 Landfill Road, Yanceyville, North Carolina 27379.
The landfill is a closed facility that ceased operation in 1994, and currently monitors water quality under a Post
Closure Care Plan on a semi-annual basis. The facility uses a network of six (6) groundwater monitoring wells to
monitor groundwater quality at the facility, as depicted in Appendix I, Figure 1. The groundwater monitoring
network is made up of one up-gradient monitoring well (MW-1) and five down-gradient compliance monitoring
wells (MW-2, MW-3, MW-4, MW-5, and MW-6). The collected groundwater samples are to be analyzed in
accordance with 15A NCAC 13B .0500 et seq for the North Carolina Landfill Appendix I volatile organic constituent
Semi-Annual Monitoring Report – October 2017
Caswell County Landfill Permit No 17-01
Yanceyville, North Carolina
S&ME Project No. 1584-07-034A
November 21, 2017 3
suite plus the eight RCRA metals. The monitoring wells are typically purged and groundwater samples collected
using new, disposable, Teflon bailers, or a sterile peristaltic pump with new Teflon tubing.
The facility also typically monitors surface water quality at the stream that crosses the down-gradient region of the
facility. As conditions allow, during each semi-annual monitoring event, two surface water samples are collected
from this stream at designated sampling points. Stream sampling location SW-1 is the upstream sampling location
to the south of the waste management unit. Stream sampling location SW-2 is the downstream sampling location.
S&ME Inc. (S&ME) has completed the second semi-annual monitoring event for 2017 at the closed Caswell
County Landfill site. The monitoring activities were authorized by County Manager, Mr. Bryan Miller and were
completed in general accordance with S&ME proposal 43-1700189 dated March 7, 2017. This report summarizes
our understanding of the project, our field services, and the results of laboratory analyses performed on the
samples collected for the second semi-annual water quality monitoring event for 2017.
3.0 Scope of Services
S&ME has performed the second semi-annual groundwater sampling of the six (6) network groundwater
monitoring wells for the 2017 groundwater monitoring year. The groundwater monitoring wells were purged,
sampled, and the groundwater samples collected from MW-1 through MW-6 were analyzed for the North
Carolina Appendix I volatile organic constituents and the eight RCRA metals. This semi-annual groundwater
monitoring report has been prepared to summarize the October 30, 2107 groundwater monitoring event and
includes:
•Summary Tables of the laboratory analytical data from each sampling event,
•Development of a current potentiometric map,
•A discussion of findings and results,
•An electronic copy of this report will be sent to the North Carolina Department of Environmental Quality
(NCDEQ)
4.0 Methods Employed
4.1 Monitoring Well Sampling
Groundwater monitoring well sampling took place on October 30, 2017. The monitoring well locations with
respect to the facility layout are shown on Figure 1. Prior to sample collection each well was opened and the
static water level measured relative to the top edge of the PVC well casing. The total well depth was used to
determine the volume of water in the wells at the time of sampling. These data are summarized in Table 1 and
Table 2.
Monitor wells MW-1, MW-2 and MW-4 were manually purged using a new, Teflon bailer prior to collecting the
water samples. Each well was purged of up to three times the well volume or purged until the well went dry prior
to the collection of the groundwater sample. The bailer was lowered, by hand, using a nylon rope into the well in
Semi-Annual Monitoring Report – October 2017
Caswell County Landfill Permit No 17-01
Yanceyville, North Carolina
S&ME Project No. 1584-07-034A
November 21, 2017 4
such a manner as to minimize agitation of the groundwater. The purge water from each of these wells was
monitored for pH, conductivity, and temperature. Table 2 provides a summary of the measured field parameters.
Monitor wells MW-3, MW-5, and MW-6 were purged and sampled using a peristaltic pump. New tubing was used
at each well. Each well was purged of up to three times the well volume or purged until the well was dry prior to
the collection of the groundwater sample. The purge water from each of these wells was monitored for pH,
conductivity, and temperature. The field data collected during sampling was recorded on the groundwater
sampling field data sheets included in Appendix III of this report.
Immediately upon collection, each groundwater sample was placed in laboratory supplied containers, place in a
cooler with ice, and placed under chain-of custody. The sampling technician wore new nitrile gloves that were
changed between wells to reduce the possibility of cross contamination.
All groundwater samples were then sent to PACE Analytical Services, Inc. (PACE) in Huntersville, North Carolina to
be analyzed for Appendix I volatile organic constituents and the eight RCRA metals.
4.2 Groundwater Flow Direction
The static water levels in the monitoring wells were measured on October 30, 2017. On this date, the depths to
the water table ranged from 10.26 feet below top of well casing at MW-5 to 24.34 feet below the top of well
casing at MW-4. Groundwater elevation data are presented in Table 1. Ground surface elevations at each well
location were extrapolated from surface topography illustrated on Plan Sheet No. 3 of the Caswell County Landfill
Closure Plans prepared by Dewberry and Davis in March 1994. Estimated elevations for monitoring well top of
casings represent the sum of the estimated ground surface elevation plus the height of the top of casing above
the ground surface. The groundwater elevation at each monitoring well was approximated by taking the
difference of the estimated top of casing elevation and the depth to water measured at each monitoring well. A
groundwater contour map was constructed using the calculated groundwater elevation data from the October 30,
2017, sampling event and is presented as Appendix I, Figure 2. The groundwater elevation data collected during
this monitoring event indicates that the groundwater beneath the landfill generally flows easterly toward the
unnamed tributary of Bear Branch.
4.3 Surface Water Sampling
Surface water sampling took place on October 30, 2017. Two stream samples (SW-1 and SW-2) were collected
from an unnamed tributary of Bear Branch, which flows along the eastern portion of the facility and flows toward
the north away from the Landfill. Surface water sample (SW-1) was collected from an upstream position with
respect to the waste management unit and SW-2 was collected downstream of the waste management unit. The
surface water samples were collected by immersing laboratory supplied containers directly into the stream at the
locations to be sampled. After collection, the surface water samples were placed in a cooler with ice and placed
under chain-of-custody. All stream samples were analyzed for the North Carolina Appendix I volatile organic
constituents as well as the 8 RCRA metals by PACE Analytical Services, Inc.; a North Carolina certified laboratory.
Semi-Annual Monitoring Report – October 2017
Caswell County Landfill Permit No 17-01
Yanceyville, North Carolina
S&ME Project No. 1584-07-034A
November 21, 2017 5
5.0 Results
The following sections provide a discussion of the groundwater and surface water sampling results for the
October 30, 2017, semi-annual monitoring event. The laboratory analytical report is included in Appendix IV.
Appendix V contains a CD with the field and analytical laboratory data provided in the NCDEQ electronic data
deliverable (EDD) format.
5.1 Groundwater Analytical Results
The results of the laboratory analyses for the groundwater monitoring well samples are summarized in Table 3,
which also provides the corresponding 15A North Carolina Administrative Code (NCAC) 2L.0200 groundwater
quality standards (2L Standard) for reference. Table 4 provides a summary of the constituents detected at
concentrations greater than their respective 2L Standards. The following summarizes the groundwater sample
analyses for the six monitoring wells (MW-1, MW-2, MW-3, MW-4, MW-5, and MW-6) sampled on October 30,
2017.
5.1.1 Metals (8-RCRA):
•Arsenic was detected in the duplicate sample collected from monitoring well MW-4 at a concentration
below its corresponding 2L Standard;
•Barium was detected in samples collected from monitoring wells MW-1 through MW-6 at concentrations
below its corresponding 2L Standard;
•Chromium was detected in the samples collected from monitoring well MW-4 and from the duplicate
sample collected from MW-4 at concentrations less than its corresponding 2L Standard;
•Lead was detected in samples collected from monitoring wells MW-1, MW-2, and MW-4 at concentrations
below its corresponding 2L Standard.
The analytical results for the detected metals (totals) are summarized in Table 3.
5.1.2 Volatile Organic Compounds:
•Benzene was detected in the groundwater samples collected from monitoring wells MW-2, MW-4, and
MW-5 at concentrations greater than its 2L Standard established at 1 µg/L.
•1,4-Dichlorobenzene was detected in the groundwater samples collected from wells MW-2, MW-4, and
MW-5 at concentrations greater than its 2L Standard established at 6 µg/L.
•Chlorobenzene, chloroethane, 1,2-dichlorobenzene, 1,1-dichloroethane, cis 1,2-dichloroethene, 2-
hexanone, 4-methyl 2-pentanone (MIBK), toluene, and xylenes (total) were detected in one or more
groundwater samples during this monitoring event; however, each of the reported concentrations of
these constituents was less than their respective 2L Standard. No other volatile organic compounds were
detected above their respective method detection limit in the monitoring wells sampled during this event.
The analytical results for the detected volatile organic compounds are summarized in Table 3. Table 4 provides a
summary of the constituents and concentrations which appear to exceed to the corresponding 2L standards.
Semi-Annual Monitoring Report – October 2017
Caswell County Landfill Permit No 17-01
Yanceyville, North Carolina
S&ME Project No. 1584-07-034A
November 21, 2017 6
5.2 Surface Water Analytical Results
There were no volatile organic constituents detected above the method detection limits in the stream samples
SW-1 or SW-2 during the October 30, 2017, semi-annual monitoring event. The metal barium was detected in
samples SW-1 and SW-2, at similar concentrations. The reported concentrations are below the respective 15A
NCAC 2B Surface Water Standard for barium for Class C surface waters. There were no other metals detected
above the method detection limit in the surface water samples collected during this sampling event. The results of
the surface water sample analyses are summarized on Table 5 and Table 6.
5.3 Quality Control
A qualitative review of the data was performed to verify that the detected concentrations in the laboratory report
were of known quality. A formal, quantitative data validation was not performed. Laboratory-assigned data
qualifiers were evaluated to verify that rejected or unsupportable data were not included in the dataset. Quality
control data provided in the laboratory reports were also reviewed. No rejected or otherwise unacceptable quality
data were reported from the laboratory.
During this event a duplicate sample was collected from monitoring well MW-4 and the sample was analyzed for
the Appendix I Volatile Organic Compounds and the 8-RCRA metals. The detected barium concentrations in the
sample identified as MW-4 and the concentrations detected in the duplicate sample show very good correlation.
A Trip Blank accompanied the sample kit during shipment, sample collection, and shipment of the collected
samples back to the laboratory. The Trip Blank sample was analyzed for Appendix I Volatile Organic Compounds.
The results of the duplicate, trip blank, and laboratory QC sample analyses are included in Appendix II.
5.4 Preliminary Analysis of Cause and Significance of 2L Exceedances
It is believed that the cause of the 2L Standard exceedances reported for benzene and 1,4-dichlorobenzene within
the hydrogeologic regime at the Caswell County Landfill is caused from percolation of landfill constituents from
the waste management units into the uppermost groundwater aquifer.
Previously, S&ME reviewed the 2000 aerial photograph of the Caswell County Landfill and surrounding vicinity as
a preliminary analysis of the proximity of potential receptor water well users to the compliance monitoring wells in
which 2L Standard exceedances occurred during the July 2010 groundwater monitoring event. Based on the aerial
photograph for the year 2000, the nearest suspect residential home is located approximately 900 feet northeast of
compliance monitoring well MW-5, which is the furthest down-gradient monitoring well on the landfill side of the
unnamed tributary of Bear Branch. The observed suspect residential homes are topographically up-gradient and
on the other side of the unnamed tributary of Bear Branch from the Caswell County Landfill. At this time, S&ME
has no information regarding the current use of groundwater as a potable water source for these homes or the
availability of public water in the vicinity of the landfill.
Due to the detection of exceedances of the 2L Standard in the compliance wells, S&ME recommends that a
detailed water supply well receptor survey be completed for the Caswell County Landfill and the development of
an assessment plan to address the regulatory requirements associated with the 2L Standard exceedances.
Semi-Annual Monitoring Report – October 2017
Caswell County Landfill Permit No 17-01
Yanceyville, North Carolina
S&ME Project No. 1584-07-034A
November 21, 2017 7
6.0 References
North Carolina Administrative Code, Title 15A, Department of Environment, Health and Natural Resources,
Division of Environmental Management, Subchapter 2L, Classifications and Water Quality Standards Applicable to
the Groundwaters of North Carolina, Sections .0100, .0200, and .0300; from the Environmental Management
Commission Raleigh, North Carolina.
North Carolina Administrative Code, Title 15A, Department of Environment, Health and Natural Resources,
Division of Environmental Management, Subchapter 2B, Classifications and Water Quality Standards Applicable to
the Surface Waters of North Carolina, Section .0200; from the Environmental Management Commission, Raleigh,
North Carolina.
North Carolina Administrative Code, Title 15A, Department of Environment, Health and Natural Resources,
Division of Solid Waste Management, subchapter 13B, Solid Waste Management, Section .1600.
Appendices
Appendix I – Figures
560570570570
560550
540
530
520510500490490GRAVEL ACCESS ROADMW-6MW-5MW-3MW-2MW-4MW-1KEY- MONITORING WELL LOCATIONAPPROXIMATE LIMITSOF SOLID WASTEEXISTINGSTORMWATER/SEDIMENTPONDCLOSED LANDFILL AREALGV-3LGV-4LGV-5LGV-6LGV-2LGV-1- APPROXIMATE LOCATION OF LANDFILL GAS VENTSFIGURE NO.Drawing path: Q:\1584\2007\07-034 - CASWELL COUNTY LANDFILL\A\11-17\Caswell County Landfill.dwg
PROJECT NUMBERDATE:SCALE: (IN FEET)GRAPHIC SCALE0120240 (IN FEET)GRAPHIC SCALECASWELL COUNTY LANDFILL
YANCEYVILLE, NORTH CAROLINA1NOV. 2017SITE PLANAS SHOWN1584-07-034AN
560570570570
56055
0
540
530
520510500490490GRAVEL ACCESS
ROAD
490.0
500.
0
510.
0
520.
0
530.
0
540.0550.0
485.0
495.0
505.
0
515.
0
525.
0
535.
0
545.0
MW-6MW-5MW-3MW-2MW-4MW-1(480.66)(489.84)(500.40)(503.06)(507.53)(551.66)EXISTINGSTORMWATER/SEDIMENTPONDCLOSED LANDFILL AREAKEY- MONITORING WELL LOCATION- GROUNDWATER CONTOUR- GROUNDWATER ELEVATION MEASURED IN MONITORING WELL ON 10/30/17- GROUNDWATER FLOW DIRECTION(500.40)FIGURE NO.Drawing path: Q:\1584\2007\07-034 - CASWELL COUNTY LANDFILL\A\11-17\Caswell County Landfill.dwg
PROJECT NUMBERDATE:SCALE: (IN FEET)GRAPHIC SCALE0120240 (IN FEET)GRAPHIC SCALECASWELL COUNTY LANDFILL
YANCEYVILLE, NORTH CAROLINA2NOV. 2017GROUNDWATER CONTOUR MAPAS SHOWN1584-07-034ANOTE- GROUNDWATER MEASUREMENT FOR MONITORING WELL MW-4 NOT INCLUDED IN CONTOUR CALCULATIONN
Appendix II – Tables
Well ID
Date
Installed
Total
Depth
Well
Diameter
Depth to
Top of
Screen
Well
Screen
Interval Geology of Screened Northing Easting
Ground
Elevation
Top of
Casing
Elevation
Depth to
Groundwater1 Groundwater
Elevation
Interval NAD 83 NAD 83 estimated estimated 10/30/2017 10/30/2017
(feet)(inches)(feet)(feet bgs)(feet msl.)(feet msl.)(feet)(μs/cm)
MW-1 6/10/1985 24.5 2 13 13 - 23 partially weather rock 36.43826 -79.37108 572 574 22.34 551.66
MW-2 6/10/1985 22.3 2 10.5 10.5 - 20.5 partially weather rock 36.43912 -79.36756 526 528 20.47 507.53
MW-3 6/10/1985 17.8 2 8 8 - 18 partially weather rock 36.43948 -79.36728 511 513 12.60 500.40
MW-4 3/12/1992 36 2 29 29 - 34 rock 36.43909 -79.36759 526 527.4 24.34 503.06
MW-5 3/16/1992 24.7 2 12.6 12.6 - 22.6 rock 36.43939 -79.36679 498 500.1 10.26 489.84
MW-6 3/13/1992 16.2 2 7.8 7.8 - 17.8 rock 36.43941 -79.3664 489 491.1 10.44 480.66
Top of casing elevations estimated from Dewberry & Davis topographic map. No survey data available
Well Construction details obtained from Well Construction Records provided by Caswell County
feet bgs. = feet below ground surface
feet msl. = feet mean sea level
Depth to Groundwater1 = below assumed top of casing elevation
Groundwater Elevation = calculated groundwater elevation
S&ME PROJECT NO. 1584-07-034A
TABLE 1
WELL CONSTRUCTION AND GROUNDWATER ELEVATION DATA
PERMIT # 17-01
CASWELL COUNTY LANDFILL
YANCEYVILLE, NORTH CAROLINA
T:\Projects\2007\ENV\034 Caswell County Landfill Groundwater Monitoring\2017 GW Sampling\Fall 2017\Caswell County Landfill Report Tables BSL.xlsx
TABLE 2
SUMMARY OF GROUNDWATER SAMPLING FIELD PARAMETERS
PERMIT # 17-01
CASWELL COUNTY LANDFILL
YANCEYVILLE, NORTH CAROLINA
S&ME PROJECT NO. 1584-07-034A
DATE WELL WELL DEPTH TO WATER ODOR PURGE PUMP WELL EVAC PURGED TEMP pH SPECIFIC
ID DEPTH WATER ELEVATION METHOD RATE VOLUME VOLUME DRY?CONDUCTANCE
(feet)(feet)(feet)(mL/min)(gallons)(gallons)(yes/no)(deg C)(SU)(μs/cm)
10/30/2017 MW-1 24.5 22.34 551.66 None bailer NA 0.35 1.1 No 15.30 6.60 1477.0
10/30/2017 MW-2 22.3 20.47 507.53 None bailer NA 0.30 0.9 Yes 14.30 6.70 1335.0
10/30/2017 MW-3 17.8 12.60 500.40 None pump 100 0.85 2.5 No 14.60 6.60 728.0
10/30/2017 MW-4 36.0 24.34 503.06 None bailer NA 1.90 5.7 Yes 14.30 6.70 1376.0
10/30/2017 MW-5 24.7 10.26 489.84 None pump 200 2.35 7.1 No 15.20 6.60 1143.0
10/30/2017 MW-6 16.2 10.44 480.66 None pump 200 0.93 2.8 No 16.00 6.60 102.0
Notes:
1. TEMP = groundwater temperature, measured in degrees Celsius
2. Pump Rate, measured in milliliters/minute
3. Specific Conductance, measured in μs/cm indicates micro Siemens per centimeter.
4. SU indicates Standard Units.
5. EVAC = evacuated volume of groundwater
6. NA = not applicable
TABLE 3
SUMMARY OF GROUNDWATER ANALYSES RESULTS - DETECTIONS
PERMIT # 17-01
CASWELL COUNTY LANDFILL SUMMARY OF GROUNDWATER ANALYSES RESULTS - DETECTIONS
YANCEYVILLE, NORTH CAROLINA
S&ME PROJECT NO. 1584-07-034A
NC SWSL Report NCAC 2L NCDEQ Federal
Well ID MW-1 MW-2 MW-3 MW-4 MW-5 MW-6 Duplicate Limit Standards IMAC MCLs
Sample ID 1701-MW1 1701-MW2 1701-MW3 1701-MW4 1701-MW5 1701-MW6 1701-Duplicate
Date Collected 10/30/17 10/30/17 10/30/17 10/30/17 10/30/17 10/30/17 10/30/17
Detected Analytes (µg/L)(µg/L)(µg/L)(µg/L)(µg/L)(µg/L)(µg/L)(µg/L)(µg/L)(µg/L)(µg/L)(µg/L)
16 Benzene <1.0 2.2 0.81 J 1.7 1.4 <1.0 1.7 1 1.0 1 --5
39 Chlorobenzene <1.0 31.7 13.6 28.3 10.1 <1.0 26.6 3 1.0 50 --100
41 Chloroethane <1.0 <1.0 <1.0 1.2 1.7 <1.0 0.71 J 10 1.0 3,000 --NS
69 1,2-Dichlorobenzene <1.0 1.7 0.97 J 1.9 2.4 <1.0 1.9 5 1.0 20 --600
71 1,4-Dichlorobenzene <1.0 12.4 4.8 12.2 16.1 <1.0 12.2 1 1.0 6 --75
75 1,1-Dichloroethane <1.0 <1.0 <1.0 <1.0 0.74 J <1.0 <1.0 5 1.0 6 --NS
78 cis-1,2-Dichloroethene <1.0 0.26 J <1.0 0.29 J 0.40 J <1.0 0.33 J 5 1.0 70 --700
147 4-Methyl 2-Pentanone (MIBK)<5.0 <5.0 <5.0 1.7 J <5.0 <5.0 <5.0 100 5.0 NS 560 NS
196 Toluene <1.0 0.40 J <1.0 <1.0 0.30 J <1.0 <1.0 1 1.0 600 --1
346 Xylenes <2.0 0.50 J <2.0 0.47 J 0.34 J <2.0 0.52 J 5 2.0 500 --10
NC SWSL Report NCAC 2L NCDEQ Federal
Well ID MW-1 MW-2 MW-3 MW-4 MW-5 MW-6 Duplicate Limit Standards IMAC MCLs
Sample ID 1701-MW1 1701-MW2 1701-MW3 1701-MW4 1701-MW5 1701-MW6 1701-Duplicate
Date Collected 10/30/17 10/30/17 10/30/17 10/30/17 10/30/17 10/30/17 10/30/17
Detected Analytes (µg/L)(µg/L)(µg/L)(µg/L)(µg/L)(µg/L)(µg/L)(µg/L)(µg/L)(µg/L)(µg/L)(µg/L)
14 Arsenic <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 7.2 J 10 10 10 --NS
15 Barium 41.6 103 68.1 59.2 51.2 15.0 49.0 100 10 700 --2,000
51 Chromium <5.0 <5.0 <5.0 4.9 J <5.0 <5.0 3.6 J 10 5 10 --1,000
131 Lead 3.4 J 4.8 J <5.0 6.2 <5.0 <5.0 <5.0 10 5 15 --NS
µg/L =concentrations reported in micrograms per liter
NC SWSL = North Carolina Solid Waste Section Limit
NCAC 2L Standards = 15A North Carolina Administrative Code 2L .0200, GW Quality Standards for Class GA groundwater.
concentrations in bold exceed the corresponding 2L Standard
NCDEQ IMAC = Interim Maximum Allowed Concentration, NCDEQ
Federal MCL = Maximum Contamiant Levels, USEPA
NS = no NCAC 2L Standard or MCL listed (USEPA)
na = not analyzed
Solid
Waste
Section
ID #
Sample Locations
Sample Locations
Appendix I Volatile Organic Compounds
Solid
Waste
Section
ID #
8-RCRA Metals
TABLE 4
SUMMARY OF GROUNDWATER EXCEEDANCES
PERMIT # 17-01
CASWELL COUNTY LANDFILL
YANCEYVILLE, NORTH CAROLINA
S&ME PROJECT NO. 1584-07-034A
Well ID MW-2 MW-4 MW-5 NC SWSL NCAC 2L NCDEQ Federal
Sample ID 1701-MW2 1701-MW4 1701-MW5 Standards IMAC MCLs
Date Collected 10/30/17 10/30/17 10/30/17
Detected Analytes (µg/L)(µg/L)(µg/L)(µg/L)(µg/L)(µg/L)(µg/L)
16 Benzene 2.2 1.7 1.4 1 1 --5
71 1,4-Dichlorobenzene 12.4 12.2 16.1 1 6 --75
µg/L =concentrations reported in micrograms per liter
NC SWSL = North Carolina Solid Waste Section Limit
NCAC 2L Standards = 15A North Carolina Administrative Code 2L .0200, GW Quality Standards
for Class GA groundwater.
Concentration greater than the NCAC 2L Standards are shown in bold
NCDEQ IMAC = Interim Maximum Allowed Concentration, NCDEQ
Federal MCL =Maximum Contamiant Levels, USEPA
NS = no MCL listed, USEPA
Solid
Waste
Section
IDs
PERMIT # 17-01
CASWELL COUNTY LANDFILL
YANCEYVILLE, NORTH CAROLINA
S&ME PROJECT NO. 1584-07-034A
NC SWSL Report NCAC 2B
Sample Location SW-1 SW-2 Limit Standards
Sample ID 1701-SW1 1701-SW2
Date Collected 10/30/17 10/30/17
Detected Analytes (µg/L)(µg/L)(µg/L)(µg/L)(µg/L)
all target analytes < report limit < report limit analyte specific analyte specific analyte specific
NC SWSL Report NCAC 2B
Sample Location SW-1 SW-2 Limit Standards*
Sample ID 1701-SW1 1701-SW2
Date Collected 10/30/17 10/30/17
Detected Analytes (µg/L)(µg/L)(µg/L)(µg/L)(µg/L)
15 Barium 25.1 29.7 100 5.0 1000
µg/L =concentrations reported in micrograms per liter
NC SWSL = North Carolina Solid Waste Section Limit
8-RCRA Metals
Solid Waste
Section ID #
Sample Locations
TABLE 5
SUMMARY OF SURFACE WATER ANALYSES RESULTS - DETECTIONS
Appendix I Volatile Organic Compounds
Solid Waste
Section ID #
Sample Locations
PERMIT # 17-01
CASWELL COUNTY LANDFILL
YANCEYVILLE, NORTH CAROLINA
S&ME PROJECT NO. 1584-07-034A
Sample Location SW-1 SW-2 NC SWSL NCAC 2B
Sample ID 1701-SW1 1701-SW2 Standards*
Date Collected 10/30/17 10/30/17
Detected Analytes (µg/L)(µg/L)(µg/L)(µg/L)
µg/L =concentrations reported in micrograms per liter
NC SWSL = North Carolina Solid Waste Section Limit
* = Title 15A NCAC 2B Standards for all Water Supply Classifications
No exceedances
Appendix I VOCs and 8-RCRA Metals
Solid Waste
Section IDs
TABLE 6
SUMMARY OF 2B SURFACE WATER STANDARD EXCEEDANCES
Appendix III – Groundwater Sampling Field Data Sheets
Location:Purge Date:
Project No.:Purge Time:
Source Well:Sample Date:
Sample Time:
Locked?:Yes:x No:Weather:
Sampled By:Air Temp:
feet
feet
2.16 feet
Purge Method
Sample Method Start Stop
Purge Rate ml/min
Control Settings On:sec.Start Stop
Off:sec.
Pressure:psi
2" well:
height:2.16 x .163 =0.35208
gallons x liters
Yes No x
*Stabilization Parameters
Time Date Temp pH Conductivity *ORP *D.O.*Turbidity DTW
Final Readings 1600 10/30/2017 15.30 6.60 1477.000 1.00
* C units mS/cm mV mg/L NTU
Sample Collection Time
Was well purged dry
Field Analyses
Volume of water in well
Volume of water removed 1.1
Depth to well bottom from measuring point:24.50
Height of water column:
Bailer
GROUNDWATER SAMPLING FIELD DATA
Water Level & Well Data
Depth to water from measuring point:22.34
1600
Sunny
Measuring point:Top of Casing
Well Purging & Sample Collection
Bailer Purge Time
55 *F
Caswell County Landfill
1584-07-034A
1701-MW-1
Gary Simcox
Monday, October 30, 2017
Monday, October 30, 2017
Location:Purge Date:
Project No.:Purge Time:
Source Well:Sample Date:
Sample Time:
Locked?:Yes:x No:Weather:
Sampled By:Air Temp:
feet
feet
1.83 feet
Purge Method
Sample Method Start Stop
Purge Rate ml/min
Control Settings On:sec.Start Stop
Off:sec.
Pressure:psi
2" well:
height:1.83 x .163 =0.29829
gallons x liters
Yes x No
*Stabilization Parameters
Time Date Temp pH Conductivity *ORP *D.O.*Turbidity DTW
Final Readings 1000 10/30/2017 14.30 6.70 1335.000 1.00
* C units mS/cm mV mg/L
Depth to well bottom from measuring point:22.30
Height of water column:
Monday, October 30, 2017
Monday, October 30, 2017
Caswell County Landfill
1584-07-034A
1701-MW-2
GROUNDWATER SAMPLING FIELD DATA
Water Level & Well Data
Depth to water from measuring point:20.47
1000
Sunny
45*FGary Simcox
Bailer
Measuring point:Top of Casing
Well Purging & Sample Collection
Bailer Purge Time
Sample Collection Time
Was well purged dry
Field Analyses
Volume of water in well
Volume of water removed 0.89
Location:Purge Date:
Project No.:Purge Time:
Source Well:Sample Date:
Sample Time:
Locked?:Yes:x No:Weather:
Sampled By:Air Temp:
feet
feet
feet
Purge Method
Sample Method Start 1115 Stop 1155
Purge Rate ml/min
Control Settings On:sec.Start 1155 Stop 1200
Off:sec.
Pressure:psi
2" well:
height:5.20 x .163 =0.8476
gallons liters x
Yes No x
*Stabilization Parameters
Time Date Temp pH Conductivity *ORP *D.O.*Turbidity DTW
1115 10/30/2017
1125 10/30/2017 14.20 6.50 741.00 1.00
1135 10/30/2017 14.50 6.40 729.00 1.00
1145 10/30/2017 14.50 6.60 730.00 1.00
1155 10/30/2017 14.60 6.60 728.00 1.00
<
Final Readings 1155 10/30/2017 14.60 6.60 728.00 1.00
* C units mS/cm mV mg/L
Was well purged dry
Field Analyses
Volume of water in well
Volume of water removed 2.54
Peristaltic Pump Purge Time
Peristaltic Pump
100 Sample Collection Time
Measuring point:Top of Casing
Well Purging & Sample Collection
Depth to well bottom from measuring point:17.80
Height of water column:5.20
GROUNDWATER SAMPLING FIELD DATA
Water Level & Well Data
Depth to water from measuring point:12.60
1200
Sunny
45 *F
Caswell County Landfill
1584-07-034A
1701-MW-3
Gary Simcox
Monday, October 30, 2017
Monday, October 30, 2017
Location:Purge Date:
Project No.:Purge Time:
Source Well:Sample Date:
Sample Time:
Locked?:Yes:x No:Weather:
Sampled By:Air Temp:
feet
feet
feet
Purge Method
Sample Method Start Stop
Purge Rate ml/min
Control Settings On:sec.Start Stop
Off:sec.
Pressure:psi
Note: Duplicate sample taken at this location. (0700)
2" well:
height:11.66 x .163 =1.90058
gallons x liters
Yes X No
*Stabilization Parameters
Time Date Temp pH Conductivity *ORP *D.O.*Turbidity DTW
1015 10/30/2017 14.50 6.90 1370.00 1.00
1020 10/30/2017 14.50 6.80 1350.00 1.00
1025 10/30/2017 14.30 6.70 1376.00 1.00
Final Readings 1025 10/30/2017 14.30 6.70 1376.00 1.00
* C units mS/cm mV mg/L
GROUNDWATER SAMPLING FIELD DATA
Water Level & Well Data
Depth to water from measuring point:24.34
1030
Sunny
45*F
Caswell County Landfill
1584-07-034A
1701-MW-4
Gary Simcox
Monday, October 30, 2017
Field Analyses
Well Purging & Sample Collection
Bailer Purge Time
Volume of water in well
Volume of water removed 5.70
Was well purged dry
Sample Collection Time
Bailer
Height of water column:
Monday, October 30, 2017
11.66
Measuring point:Top of Casing
Depth to well bottom from measuring point:36.00
Location:Purge Date:
Project No.:Purge Time:
Source Well:Sample Date:
Sample Time:
Locked?:Yes:x No:Weather:
Sampled By:Air Temp:
feet
feet
feet
Purge Method
Sample Method Start 1230 Stop 1310
Purge Rate ml/min
Control Settings On: 3.0 sec.Start 1310 Stop 1315
Off: 27.0 sec.
Pressure: 26 psi
2" well:
height:14.44 x .163 =2.35372
gallons liters x
Yes No x
*Stabilization Parameters
Time Date Temp pH Conductivity *ORP *D.O.*Turbidity DTW
1230 10/30/2017
1240 10/30/2017 15.00 6.60 1130.00 1.00
1250 10/30/2017 15.10 6.60 1138.00 1.00
1300 10/30/2017 15.10 6.60 1143.00 1.00
1310 10/30/2017 15.20 6.60 1143.00 1.00
Final Readings 1310 10/30/2017 15.20 6.60 1143.00 1.00
* C units mS/cm mV mg/L NTU
Was well purged dry
Field Analyses
Volume of water in well
Volume of water removed 7.06
Peristaltic Pump Purge Time
Peristaltic Pump
200 Sample Collection Time
Measuring point:Top of Casing
Well Purging & Sample Collection
Depth to well bottom from measuring point:24.70
Height of water column:14.44
GROUNDWATER SAMPLING FIELD DATA
Water Level & Well Data
Depth to water from measuring point:10.26
1315
Sunny
50 *F
Caswell County Landfill
1584-07-034A
1701-MW-5
Gary Simcox
Tuesday, January 10, 1900
Monday, October 30, 2017
Location:Purge Date:
Project No.:Purge Time:
Source Well:Sample Date:
Sample Time:
Locked?:Yes:x No:Weather:
Sampled By:Air Temp:
feet
feet
feet
Purge Method
Sample Method Start 1345 Stop 1425
Purge Rate ml/min
Control Settings On:sec.Start 1425 Stop 1430
Off:sec.
Pressure:psi
2" well:
height:5.76 x .163 =0.93888
gallons liters x
Yes No x
*Stabilization Parameters
Time Date Temp pH Conductivity *ORP *D.O.*Turbidity DTW
1355 10/30/2017
1405 10/30/2017 15.90 6.60 115.00 1.00
1415 10/30/2017 16.00 6.60 113.00 1.00
1425 10/30/2017 16.00 6.60 102.00 1.00
Final Readings 1425 10/30/2017 16.00 6.60 102.00 1.00
* C units mS/cm mV mg/L
Was well purged dry
Field Analyses
Volume of water in well
Volume of water removed 2.82
Peristaltic Pump Purge Time
Peristaltic Pump
200 Sample Collection Time
Measuring point:Top of Casing
Well Purging & Sample Collection
Depth to well bottom from measuring point:16.20
Height of water column:5.76
GROUNDWATER SAMPLING FIELD DATA
Water Level & Well Data
Depth to water from measuring point:10.44
1430
Sunny
50 *F
Caswell County Landfill
1584-07-034A
1701-MW-6
Gary Simcox
Monday, October 30, 2017
Monday, October 30, 2017
Location:Purge Date:
Project No.:Purge Time:
Source Well:Sample Date:
Sample Time:
Locked?:Yes:x No:Weather:
Sampled By:Air Temp:
feet
feet
feet
Purge Method
Sample Method Start Stop
Purge Rate ml/min
Control Settings On:sec.Start Stop
Off:sec.
Pressure:psi
2" well:
height:0 x .163 =0
gallons liters
Yes No x
*Stabilization Parameters
Time Date Temp pH Conductivity *ORP *D.O.*Turbidity DTW
Final Readings 1515 10/30/2017 10.80 7.70 123.000
* C units mS/cm mV mg/L NTU
Was well purged dry
Field Analyses
Volume of water in well
Volume of water removed
Purge Time
Sample Collection Time
Measuring point:
Well Purging & Sample Collection
Depth to well bottom from measuring point:
Height of water column:
GROUNDWATER SAMPLING FIELD DATA
Water Level & Well Data
Depth to water from measuring point:
1515
Sunny
55 *F
Caswell County Landfill
1584-07-034A
1701-SW-1
Gary Simcox
Monday, October 30, 2017
Monday, October 30, 2017
Location:Purge Date:
Project No.:Purge Time:
Source Well:Sample Date:
Sample Time:
Locked?:Yes:x No:Weather:
Sampled By:Air Temp:
feet
feet
feet
Purge Method
Sample Method Start Stop
Purge Rate ml/min
Control Settings On:sec.Start Stop
Off:sec.
Pressure:psi
2" well:
height:0 x .163 =0
gallons liters x
Yes No x
*Stabilization Parameters
Time Date Temp pH Conductivity *ORP *D.O.*Turbidity DTW
Final Readings 1445 10/30/2017 10.70 7.80 152.000
* C units mS/cm mV mg/L NTU
GROUNDWATER SAMPLING FIELD DATA
:
Depth to water from measuring point:
1445
Sunny
55 *F
Caswell County Landfill
1584-07-034A
1701-SW-2
Gary Simcox
Monday, October 30, 2017
Depth to well bottom from measuring point:
Monday, October 30, 2017
Height of water column:
Measuring point:
Well Purging & Sample Collection
Purge Time
Sample Collection Time
Was well purged dry
Field Analyses
Volume of water in well
Volume of water removed
Appendix IV – Laboratory Analytical Report
#=CL#
November 09, 2017
LIMS USE: FR - TIM SMITH
LIMS OBJECT ID: 92361242
92361242
Project:
Pace Project No.:
RE:
Tim Smith
Caswell County Landfill
162 Landfill Road
Yanceyville, NC 27379
CASWELL CO LF 1584-07-034
Dear Tim Smith:
Enclosed are the analytical results for sample(s) received by the laboratory on October 31, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
[phone]
Enclosures
cc:Mr. Ed Henriques, S&ME, Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 1 of 31
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92361242
CASWELL CO LF 1584-07-034
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 2 of 31
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92361242
CASWELL CO LF 1584-07-034
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92361242001 1701-MW-1 EPA 6010 7 PASI-ASER, SH1
EPA 7470 1 PASI-AWAB
EPA 8260 51 PASI-CGAW
92361242002 1701-MW-2 EPA 6010 7 PASI-ASER, SH1
EPA 7470 1 PASI-AWAB
EPA 8260 51 PASI-CGAW
92361242003 1701-MW-3 EPA 6010 7 PASI-ASER, SH1
EPA 7470 1 PASI-AWAB
EPA 8260 51 PASI-CGAW
92361242004 1701-MW-4 EPA 6010 7 PASI-ASER, SH1
EPA 7470 1 PASI-AWAB
EPA 8260 51 PASI-CGAW
92361242005 1701-MW-5 EPA 6010 7 PASI-ASER, SH1
EPA 7470 1 PASI-AWAB
EPA 8260 51 PASI-CGAW
92361242006 1701-MW-6 EPA 6010 7 PASI-ASER, SH1
EPA 7470 1 PASI-AWAB
EPA 8260 51 PASI-CGAW
92361242007 1701-SW-1 EPA 6010 7 PASI-ASER, SH1
EPA 7470 1 PASI-AWAB
EPA 8260 51 PASI-CGAW
92361242008 1701-SW-2 EPA 6010 7 PASI-ASER, SH1
EPA 7470 1 PASI-AWAB
EPA 8260 51 PASI-CGAW
92361242009 1701-DUPLICATE EPA 6010 7 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8260 51 PASI-CGAW
92361242010 1701-TRIP BLANK EPA 8260 51 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 3 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92361242
CASWELL CO LF 1584-07-034
Sample:1701-MW-1 Lab ID:92361242001 Collected:10/30/17 16:00 Received:10/31/17 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Arsenic ND ug/L 11/04/17 15:44 7440-38-211/02/17 02:3010.0 1
Barium 41.6 ug/L 11/04/17 01:58 7440-39-311/02/17 02:305.0 1
Cadmium ND ug/L 11/04/17 01:58 7440-43-911/02/17 02:301.0 1
Chromium ND ug/L 11/04/17 01:58 7440-47-311/02/17 02:305.0 1
Lead 3.4J ug/L 11/04/17 01:58 7439-92-111/02/17 02:305.0 1
Selenium ND ug/L 11/04/17 01:58 7782-49-211/02/17 02:3010.0 1
Silver ND ug/L 11/04/17 01:58 7440-22-411/02/17 02:305.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 11/07/17 13:32 7439-97-611/07/17 09:250.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/02/17 21:46 67-64-125.0 1
Acrylonitrile ND ug/L 11/02/17 21:46 107-13-110.0 1
Benzene ND ug/L 11/02/17 21:46 71-43-21.0 1
Bromochloromethane ND ug/L 11/02/17 21:46 74-97-51.0 1
Bromodichloromethane ND ug/L 11/02/17 21:46 75-27-41.0 1
Bromoform ND ug/L 11/02/17 21:46 75-25-21.0 1
Bromomethane ND ug/L 11/02/17 21:46 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/02/17 21:46 78-93-35.0 1
Carbon disulfide ND ug/L 11/02/17 21:46 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/02/17 21:46 56-23-51.0 1
Chlorobenzene ND ug/L 11/02/17 21:46 108-90-71.0 1
Chloroethane ND ug/L 11/02/17 21:46 75-00-31.0 1
Chloroform ND ug/L 11/02/17 21:46 67-66-31.0 1
Chloromethane ND ug/L 11/02/17 21:46 74-87-31.0 1
Dibromochloromethane ND ug/L 11/02/17 21:46 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/02/17 21:46 106-93-41.0 1
Dibromomethane ND ug/L 11/02/17 21:46 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/02/17 21:46 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 11/02/17 21:46 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/02/17 21:46 110-57-61.0 1
1,1-Dichloroethane ND ug/L 11/02/17 21:46 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/02/17 21:46 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/02/17 21:46 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/02/17 21:46 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/02/17 21:46 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/02/17 21:46 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 11/02/17 21:46 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/02/17 21:46 10061-02-61.0 1
Ethylbenzene ND ug/L 11/02/17 21:46 100-41-41.0 1
2-Hexanone ND ug/L 11/02/17 21:46 591-78-65.0 1
Iodomethane ND ug/L 11/02/17 21:46 74-88-45.0 1
Methylene Chloride ND ug/L 11/02/17 21:46 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/02/17 21:46 108-10-15.0 1
Styrene ND ug/L 11/02/17 21:46 100-42-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/09/2017 04:44 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 4 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92361242
CASWELL CO LF 1584-07-034
Sample:1701-MW-1 Lab ID:92361242001 Collected:10/30/17 16:00 Received:10/31/17 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,1,2-Tetrachloroethane ND ug/L 11/02/17 21:46 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/02/17 21:46 79-34-51.0 1
Tetrachloroethene ND ug/L 11/02/17 21:46 127-18-41.0 1
Toluene ND ug/L 11/02/17 21:46 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 11/02/17 21:46 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/02/17 21:46 79-00-51.0 1
Trichloroethene ND ug/L 11/02/17 21:46 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/02/17 21:46 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/02/17 21:46 96-18-41.0 1
Vinyl acetate ND ug/L 11/02/17 21:46 108-05-42.0 1
Vinyl chloride ND ug/L 11/02/17 21:46 75-01-41.0 1
Xylene (Total)ND ug/L 11/02/17 21:46 1330-20-71.0 1
m&p-Xylene ND ug/L 11/02/17 21:46 179601-23-12.0 1
o-Xylene ND ug/L 11/02/17 21:46 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)103 %11/02/17 21:46 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %11/02/17 21:46 17060-07-070-130 1
Toluene-d8 (S)103 %11/02/17 21:46 2037-26-570-130 1
Sample:1701-MW-2 Lab ID:92361242002 Collected:10/30/17 10:00 Received:10/31/17 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Arsenic ND ug/L 11/04/17 15:53 7440-38-211/02/17 02:3010.0 1
Barium 103 ug/L 11/04/17 02:14 7440-39-311/02/17 02:305.0 1
Cadmium ND ug/L 11/04/17 02:14 7440-43-911/02/17 02:301.0 1
Chromium ND ug/L 11/04/17 02:14 7440-47-311/02/17 02:305.0 1
Lead 4.8J ug/L 11/04/17 02:14 7439-92-111/02/17 02:305.0 1
Selenium ND ug/L 11/04/17 02:14 7782-49-211/02/17 02:3010.0 1
Silver ND ug/L 11/04/17 02:14 7440-22-411/02/17 02:305.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 11/07/17 13:35 7439-97-611/07/17 09:250.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/02/17 22:04 67-64-125.0 1
Acrylonitrile ND ug/L 11/02/17 22:04 107-13-110.0 1
Benzene 2.2 ug/L 11/02/17 22:04 71-43-21.0 1
Bromochloromethane ND ug/L 11/02/17 22:04 74-97-51.0 1
Bromodichloromethane ND ug/L 11/02/17 22:04 75-27-41.0 1
Bromoform ND ug/L 11/02/17 22:04 75-25-21.0 1
Bromomethane ND ug/L 11/02/17 22:04 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/02/17 22:04 78-93-35.0 1
Carbon disulfide ND ug/L 11/02/17 22:04 75-15-02.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/09/2017 04:44 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 5 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92361242
CASWELL CO LF 1584-07-034
Sample:1701-MW-2 Lab ID:92361242002 Collected:10/30/17 10:00 Received:10/31/17 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Carbon tetrachloride ND ug/L 11/02/17 22:04 56-23-51.0 1
Chlorobenzene 31.7 ug/L 11/02/17 22:04 108-90-71.0 1
Chloroethane ND ug/L 11/02/17 22:04 75-00-31.0 1
Chloroform ND ug/L 11/02/17 22:04 67-66-31.0 1
Chloromethane ND ug/L 11/02/17 22:04 74-87-31.0 1
Dibromochloromethane ND ug/L 11/02/17 22:04 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/02/17 22:04 106-93-41.0 1
Dibromomethane ND ug/L 11/02/17 22:04 74-95-31.0 1
1,2-Dichlorobenzene 1.7 ug/L 11/02/17 22:04 95-50-11.0 1
1,4-Dichlorobenzene 12.4 ug/L 11/02/17 22:04 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/02/17 22:04 110-57-61.0 1
1,1-Dichloroethane ND ug/L 11/02/17 22:04 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/02/17 22:04 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/02/17 22:04 75-35-41.0 1
cis-1,2-Dichloroethene 0.26J ug/L 11/02/17 22:04 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/02/17 22:04 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/02/17 22:04 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 11/02/17 22:04 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/02/17 22:04 10061-02-61.0 1
Ethylbenzene ND ug/L 11/02/17 22:04 100-41-41.0 1
2-Hexanone ND ug/L 11/02/17 22:04 591-78-65.0 1
Iodomethane ND ug/L 11/02/17 22:04 74-88-45.0 1
Methylene Chloride ND ug/L 11/02/17 22:04 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/02/17 22:04 108-10-15.0 1
Styrene ND ug/L 11/02/17 22:04 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/02/17 22:04 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/02/17 22:04 79-34-51.0 1
Tetrachloroethene ND ug/L 11/02/17 22:04 127-18-41.0 1
Toluene 0.40J ug/L 11/02/17 22:04 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 11/02/17 22:04 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/02/17 22:04 79-00-51.0 1
Trichloroethene ND ug/L 11/02/17 22:04 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/02/17 22:04 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/02/17 22:04 96-18-41.0 1
Vinyl acetate ND ug/L 11/02/17 22:04 108-05-42.0 1
Vinyl chloride ND ug/L 11/02/17 22:04 75-01-41.0 1
Xylene (Total)ND ug/L 11/02/17 22:04 1330-20-71.0 1
m&p-Xylene ND ug/L 11/02/17 22:04 179601-23-12.0 1
o-Xylene 0.50J ug/L 11/02/17 22:04 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)101 %11/02/17 22:04 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %11/02/17 22:04 17060-07-070-130 1
Toluene-d8 (S)101 %11/02/17 22:04 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/09/2017 04:44 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 6 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92361242
CASWELL CO LF 1584-07-034
Sample:1701-MW-3 Lab ID:92361242003 Collected:10/30/17 12:00 Received:10/31/17 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Arsenic ND ug/L 11/04/17 15:56 7440-38-211/02/17 02:3010.0 1
Barium 68.1 ug/L 11/04/17 02:17 7440-39-311/02/17 02:305.0 1
Cadmium ND ug/L 11/04/17 02:17 7440-43-911/02/17 02:301.0 1
Chromium ND ug/L 11/04/17 02:17 7440-47-311/02/17 02:305.0 1
Lead ND ug/L 11/04/17 02:17 7439-92-111/02/17 02:305.0 1
Selenium ND ug/L 11/04/17 02:17 7782-49-211/02/17 02:3010.0 1
Silver ND ug/L 11/04/17 02:17 7440-22-411/02/17 02:305.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 11/07/17 13:37 7439-97-611/07/17 09:250.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/02/17 22:21 67-64-125.0 1
Acrylonitrile ND ug/L 11/02/17 22:21 107-13-110.0 1
Benzene 0.81J ug/L 11/02/17 22:21 71-43-21.0 1
Bromochloromethane ND ug/L 11/02/17 22:21 74-97-51.0 1
Bromodichloromethane ND ug/L 11/02/17 22:21 75-27-41.0 1
Bromoform ND ug/L 11/02/17 22:21 75-25-21.0 1
Bromomethane ND ug/L 11/02/17 22:21 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/02/17 22:21 78-93-35.0 1
Carbon disulfide ND ug/L 11/02/17 22:21 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/02/17 22:21 56-23-51.0 1
Chlorobenzene 13.6 ug/L 11/02/17 22:21 108-90-71.0 1
Chloroethane ND ug/L 11/02/17 22:21 75-00-31.0 1
Chloroform ND ug/L 11/02/17 22:21 67-66-31.0 1
Chloromethane ND ug/L 11/02/17 22:21 74-87-31.0 1
Dibromochloromethane ND ug/L 11/02/17 22:21 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/02/17 22:21 106-93-41.0 1
Dibromomethane ND ug/L 11/02/17 22:21 74-95-31.0 1
1,2-Dichlorobenzene 0.97J ug/L 11/02/17 22:21 95-50-11.0 1
1,4-Dichlorobenzene 4.8 ug/L 11/02/17 22:21 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/02/17 22:21 110-57-61.0 1
1,1-Dichloroethane ND ug/L 11/02/17 22:21 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/02/17 22:21 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/02/17 22:21 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/02/17 22:21 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/02/17 22:21 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/02/17 22:21 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 11/02/17 22:21 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/02/17 22:21 10061-02-61.0 1
Ethylbenzene ND ug/L 11/02/17 22:21 100-41-41.0 1
2-Hexanone ND ug/L 11/02/17 22:21 591-78-65.0 1
Iodomethane ND ug/L 11/02/17 22:21 74-88-45.0 1
Methylene Chloride ND ug/L 11/02/17 22:21 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/02/17 22:21 108-10-15.0 1
Styrene ND ug/L 11/02/17 22:21 100-42-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/09/2017 04:44 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 7 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92361242
CASWELL CO LF 1584-07-034
Sample:1701-MW-3 Lab ID:92361242003 Collected:10/30/17 12:00 Received:10/31/17 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,1,2-Tetrachloroethane ND ug/L 11/02/17 22:21 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/02/17 22:21 79-34-51.0 1
Tetrachloroethene ND ug/L 11/02/17 22:21 127-18-41.0 1
Toluene ND ug/L 11/02/17 22:21 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 11/02/17 22:21 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/02/17 22:21 79-00-51.0 1
Trichloroethene ND ug/L 11/02/17 22:21 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/02/17 22:21 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/02/17 22:21 96-18-41.0 1
Vinyl acetate ND ug/L 11/02/17 22:21 108-05-42.0 1
Vinyl chloride ND ug/L 11/02/17 22:21 75-01-41.0 1
Xylene (Total)ND ug/L 11/02/17 22:21 1330-20-71.0 1
m&p-Xylene ND ug/L 11/02/17 22:21 179601-23-12.0 1
o-Xylene ND ug/L 11/02/17 22:21 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)101 %11/02/17 22:21 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %11/02/17 22:21 17060-07-070-130 1
Toluene-d8 (S)99 %11/02/17 22:21 2037-26-570-130 1
Sample:1701-MW-4 Lab ID:92361242004 Collected:10/30/17 10:30 Received:10/31/17 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Arsenic ND ug/L 11/04/17 16:00 7440-38-211/02/17 02:3010.0 1
Barium 59.2 ug/L 11/04/17 02:20 7440-39-311/02/17 02:305.0 1
Cadmium ND ug/L 11/04/17 02:20 7440-43-911/02/17 02:301.0 1
Chromium 4.9J ug/L 11/04/17 02:20 7440-47-311/02/17 02:305.0 1
Lead 6.2 ug/L 11/04/17 02:20 7439-92-111/02/17 02:305.0 1
Selenium ND ug/L 11/04/17 02:20 7782-49-211/02/17 02:3010.0 1
Silver ND ug/L 11/04/17 02:20 7440-22-411/02/17 02:305.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 11/07/17 13:39 7439-97-611/07/17 09:250.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/02/17 22:39 67-64-125.0 1
Acrylonitrile ND ug/L 11/02/17 22:39 107-13-110.0 1
Benzene 1.7 ug/L 11/02/17 22:39 71-43-21.0 1
Bromochloromethane ND ug/L 11/02/17 22:39 74-97-51.0 1
Bromodichloromethane ND ug/L 11/02/17 22:39 75-27-41.0 1
Bromoform ND ug/L 11/02/17 22:39 75-25-21.0 1
Bromomethane ND ug/L 11/02/17 22:39 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/02/17 22:39 78-93-35.0 1
Carbon disulfide ND ug/L 11/02/17 22:39 75-15-02.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/09/2017 04:44 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 8 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92361242
CASWELL CO LF 1584-07-034
Sample:1701-MW-4 Lab ID:92361242004 Collected:10/30/17 10:30 Received:10/31/17 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Carbon tetrachloride ND ug/L 11/02/17 22:39 56-23-51.0 1
Chlorobenzene 28.3 ug/L 11/02/17 22:39 108-90-71.0 1
Chloroethane 1.2 ug/L 11/02/17 22:39 75-00-31.0 1
Chloroform ND ug/L 11/02/17 22:39 67-66-31.0 1
Chloromethane ND ug/L 11/02/17 22:39 74-87-31.0 1
Dibromochloromethane ND ug/L 11/02/17 22:39 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/02/17 22:39 106-93-41.0 1
Dibromomethane ND ug/L 11/02/17 22:39 74-95-31.0 1
1,2-Dichlorobenzene 1.9 ug/L 11/02/17 22:39 95-50-11.0 1
1,4-Dichlorobenzene 12.2 ug/L 11/02/17 22:39 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/02/17 22:39 110-57-61.0 1
1,1-Dichloroethane ND ug/L 11/02/17 22:39 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/02/17 22:39 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/02/17 22:39 75-35-41.0 1
cis-1,2-Dichloroethene 0.29J ug/L 11/02/17 22:39 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/02/17 22:39 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/02/17 22:39 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 11/02/17 22:39 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/02/17 22:39 10061-02-61.0 1
Ethylbenzene ND ug/L 11/02/17 22:39 100-41-41.0 1
2-Hexanone ND ug/L 11/02/17 22:39 591-78-65.0 1
Iodomethane ND ug/L 11/02/17 22:39 74-88-45.0 1
Methylene Chloride ND ug/L 11/02/17 22:39 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)1.7J ug/L 11/02/17 22:39 108-10-15.0 1
Styrene ND ug/L 11/02/17 22:39 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/02/17 22:39 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/02/17 22:39 79-34-51.0 1
Tetrachloroethene ND ug/L 11/02/17 22:39 127-18-41.0 1
Toluene ND ug/L 11/02/17 22:39 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 11/02/17 22:39 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/02/17 22:39 79-00-51.0 1
Trichloroethene ND ug/L 11/02/17 22:39 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/02/17 22:39 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/02/17 22:39 96-18-41.0 1
Vinyl acetate ND ug/L 11/02/17 22:39 108-05-42.0 1
Vinyl chloride ND ug/L 11/02/17 22:39 75-01-41.0 1
Xylene (Total)ND ug/L 11/02/17 22:39 1330-20-71.0 1
m&p-Xylene ND ug/L 11/02/17 22:39 179601-23-12.0 1
o-Xylene 0.47J ug/L 11/02/17 22:39 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)100 %11/02/17 22:39 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %11/02/17 22:39 17060-07-070-130 1
Toluene-d8 (S)103 %11/02/17 22:39 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/09/2017 04:44 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 9 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92361242
CASWELL CO LF 1584-07-034
Sample:1701-MW-5 Lab ID:92361242005 Collected:10/30/17 13:15 Received:10/31/17 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Arsenic ND ug/L 11/04/17 16:03 7440-38-211/02/17 02:3010.0 1
Barium 51.2 ug/L 11/04/17 02:23 7440-39-311/02/17 02:305.0 1
Cadmium ND ug/L 11/04/17 02:23 7440-43-911/02/17 02:301.0 1
Chromium ND ug/L 11/04/17 02:23 7440-47-311/02/17 02:305.0 1
Lead ND ug/L 11/04/17 02:23 7439-92-111/02/17 02:305.0 1
Selenium ND ug/L 11/04/17 02:23 7782-49-211/02/17 02:3010.0 1
Silver ND ug/L 11/04/17 02:23 7440-22-411/02/17 02:305.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 11/07/17 13:42 7439-97-611/07/17 09:250.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/02/17 22:56 67-64-125.0 1
Acrylonitrile ND ug/L 11/02/17 22:56 107-13-110.0 1
Benzene 1.4 ug/L 11/02/17 22:56 71-43-21.0 1
Bromochloromethane ND ug/L 11/02/17 22:56 74-97-51.0 1
Bromodichloromethane ND ug/L 11/02/17 22:56 75-27-41.0 1
Bromoform ND ug/L 11/02/17 22:56 75-25-21.0 1
Bromomethane ND ug/L 11/02/17 22:56 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/02/17 22:56 78-93-35.0 1
Carbon disulfide ND ug/L 11/02/17 22:56 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/02/17 22:56 56-23-51.0 1
Chlorobenzene 10.1 ug/L 11/02/17 22:56 108-90-71.0 1
Chloroethane 1.7 ug/L 11/02/17 22:56 75-00-31.0 1
Chloroform ND ug/L 11/02/17 22:56 67-66-31.0 1
Chloromethane ND ug/L 11/02/17 22:56 74-87-31.0 1
Dibromochloromethane ND ug/L 11/02/17 22:56 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/02/17 22:56 106-93-41.0 1
Dibromomethane ND ug/L 11/02/17 22:56 74-95-31.0 1
1,2-Dichlorobenzene 2.4 ug/L 11/02/17 22:56 95-50-11.0 1
1,4-Dichlorobenzene 16.1 ug/L 11/02/17 22:56 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/02/17 22:56 110-57-61.0 1
1,1-Dichloroethane 0.74J ug/L 11/02/17 22:56 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/02/17 22:56 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/02/17 22:56 75-35-41.0 1
cis-1,2-Dichloroethene 0.40J ug/L 11/02/17 22:56 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/02/17 22:56 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/02/17 22:56 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 11/02/17 22:56 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/02/17 22:56 10061-02-61.0 1
Ethylbenzene ND ug/L 11/02/17 22:56 100-41-41.0 1
2-Hexanone ND ug/L 11/02/17 22:56 591-78-65.0 1
Iodomethane ND ug/L 11/02/17 22:56 74-88-45.0 1
Methylene Chloride ND ug/L 11/02/17 22:56 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/02/17 22:56 108-10-15.0 1
Styrene ND ug/L 11/02/17 22:56 100-42-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/09/2017 04:44 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 10 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92361242
CASWELL CO LF 1584-07-034
Sample:1701-MW-5 Lab ID:92361242005 Collected:10/30/17 13:15 Received:10/31/17 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,1,2-Tetrachloroethane ND ug/L 11/02/17 22:56 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/02/17 22:56 79-34-51.0 1
Tetrachloroethene ND ug/L 11/02/17 22:56 127-18-41.0 1
Toluene 0.30J ug/L 11/02/17 22:56 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 11/02/17 22:56 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/02/17 22:56 79-00-51.0 1
Trichloroethene ND ug/L 11/02/17 22:56 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/02/17 22:56 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/02/17 22:56 96-18-41.0 1
Vinyl acetate ND ug/L 11/02/17 22:56 108-05-42.0 1
Vinyl chloride ND ug/L 11/02/17 22:56 75-01-41.0 1
Xylene (Total)ND ug/L 11/02/17 22:56 1330-20-71.0 1
m&p-Xylene ND ug/L 11/02/17 22:56 179601-23-12.0 1
o-Xylene 0.34J ug/L 11/02/17 22:56 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)98 %11/02/17 22:56 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %11/02/17 22:56 17060-07-070-130 1
Toluene-d8 (S)110 %11/02/17 22:56 2037-26-570-130 1
Sample:1701-MW-6 Lab ID:92361242006 Collected:10/30/17 14:30 Received:10/31/17 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Arsenic ND ug/L 11/04/17 16:06 7440-38-211/02/17 02:3010.0 1
Barium 15.0 ug/L 11/04/17 02:26 7440-39-311/02/17 02:305.0 1
Cadmium ND ug/L 11/04/17 02:26 7440-43-911/02/17 02:301.0 1
Chromium ND ug/L 11/04/17 02:26 7440-47-311/02/17 02:305.0 1
Lead ND ug/L 11/04/17 02:26 7439-92-111/02/17 02:305.0 1
Selenium ND ug/L 11/04/17 02:26 7782-49-211/02/17 02:3010.0 1
Silver ND ug/L 11/04/17 02:26 7440-22-411/02/17 02:305.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 11/07/17 13:44 7439-97-611/07/17 09:250.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/02/17 23:14 67-64-125.0 1
Acrylonitrile ND ug/L 11/02/17 23:14 107-13-110.0 1
Benzene ND ug/L 11/02/17 23:14 71-43-21.0 1
Bromochloromethane ND ug/L 11/02/17 23:14 74-97-51.0 1
Bromodichloromethane ND ug/L 11/02/17 23:14 75-27-41.0 1
Bromoform ND ug/L 11/02/17 23:14 75-25-21.0 1
Bromomethane ND ug/L 11/02/17 23:14 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/02/17 23:14 78-93-35.0 1
Carbon disulfide ND ug/L 11/02/17 23:14 75-15-02.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/09/2017 04:44 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 11 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92361242
CASWELL CO LF 1584-07-034
Sample:1701-MW-6 Lab ID:92361242006 Collected:10/30/17 14:30 Received:10/31/17 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Carbon tetrachloride ND ug/L 11/02/17 23:14 56-23-51.0 1
Chlorobenzene ND ug/L 11/02/17 23:14 108-90-71.0 1
Chloroethane ND ug/L 11/02/17 23:14 75-00-31.0 1
Chloroform ND ug/L 11/02/17 23:14 67-66-31.0 1
Chloromethane ND ug/L 11/02/17 23:14 74-87-31.0 1
Dibromochloromethane ND ug/L 11/02/17 23:14 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/02/17 23:14 106-93-41.0 1
Dibromomethane ND ug/L 11/02/17 23:14 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/02/17 23:14 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 11/02/17 23:14 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/02/17 23:14 110-57-61.0 1
1,1-Dichloroethane ND ug/L 11/02/17 23:14 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/02/17 23:14 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/02/17 23:14 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/02/17 23:14 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/02/17 23:14 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/02/17 23:14 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 11/02/17 23:14 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/02/17 23:14 10061-02-61.0 1
Ethylbenzene ND ug/L 11/02/17 23:14 100-41-41.0 1
2-Hexanone ND ug/L 11/02/17 23:14 591-78-65.0 1
Iodomethane ND ug/L 11/02/17 23:14 74-88-45.0 1
Methylene Chloride ND ug/L 11/02/17 23:14 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/02/17 23:14 108-10-15.0 1
Styrene ND ug/L 11/02/17 23:14 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/02/17 23:14 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/02/17 23:14 79-34-51.0 1
Tetrachloroethene ND ug/L 11/02/17 23:14 127-18-41.0 1
Toluene ND ug/L 11/02/17 23:14 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 11/02/17 23:14 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/02/17 23:14 79-00-51.0 1
Trichloroethene ND ug/L 11/02/17 23:14 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/02/17 23:14 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/02/17 23:14 96-18-41.0 1
Vinyl acetate ND ug/L 11/02/17 23:14 108-05-42.0 1
Vinyl chloride ND ug/L 11/02/17 23:14 75-01-41.0 1
Xylene (Total)ND ug/L 11/02/17 23:14 1330-20-71.0 1
m&p-Xylene ND ug/L 11/02/17 23:14 179601-23-12.0 1
o-Xylene ND ug/L 11/02/17 23:14 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)101 %11/02/17 23:14 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %11/02/17 23:14 17060-07-070-130 1
Toluene-d8 (S)106 %11/02/17 23:14 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/09/2017 04:44 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 12 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92361242
CASWELL CO LF 1584-07-034
Sample:1701-SW-1 Lab ID:92361242007 Collected:10/30/17 15:15 Received:10/31/17 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Arsenic ND ug/L 11/04/17 16:09 7440-38-211/02/17 02:3010.0 1
Barium 25.1 ug/L 11/04/17 02:29 7440-39-311/02/17 02:305.0 1
Cadmium ND ug/L 11/04/17 02:29 7440-43-911/02/17 02:301.0 1
Chromium ND ug/L 11/04/17 02:29 7440-47-311/02/17 02:305.0 1
Lead ND ug/L 11/04/17 02:29 7439-92-111/02/17 02:305.0 1
Selenium ND ug/L 11/04/17 02:29 7782-49-211/02/17 02:3010.0 1
Silver ND ug/L 11/04/17 02:29 7440-22-411/02/17 02:305.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 11/07/17 13:51 7439-97-611/07/17 09:250.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/02/17 23:32 67-64-125.0 1
Acrylonitrile ND ug/L 11/02/17 23:32 107-13-110.0 1
Benzene ND ug/L 11/02/17 23:32 71-43-21.0 1
Bromochloromethane ND ug/L 11/02/17 23:32 74-97-51.0 1
Bromodichloromethane ND ug/L 11/02/17 23:32 75-27-41.0 1
Bromoform ND ug/L 11/02/17 23:32 75-25-21.0 1
Bromomethane ND ug/L 11/02/17 23:32 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/02/17 23:32 78-93-35.0 1
Carbon disulfide ND ug/L 11/02/17 23:32 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/02/17 23:32 56-23-51.0 1
Chlorobenzene ND ug/L 11/02/17 23:32 108-90-71.0 1
Chloroethane ND ug/L 11/02/17 23:32 75-00-31.0 1
Chloroform ND ug/L 11/02/17 23:32 67-66-31.0 1
Chloromethane ND ug/L 11/02/17 23:32 74-87-31.0 1
Dibromochloromethane ND ug/L 11/02/17 23:32 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/02/17 23:32 106-93-41.0 1
Dibromomethane ND ug/L 11/02/17 23:32 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/02/17 23:32 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 11/02/17 23:32 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/02/17 23:32 110-57-61.0 1
1,1-Dichloroethane ND ug/L 11/02/17 23:32 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/02/17 23:32 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/02/17 23:32 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/02/17 23:32 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/02/17 23:32 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/02/17 23:32 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 11/02/17 23:32 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/02/17 23:32 10061-02-61.0 1
Ethylbenzene ND ug/L 11/02/17 23:32 100-41-41.0 1
2-Hexanone ND ug/L 11/02/17 23:32 591-78-65.0 1
Iodomethane ND ug/L 11/02/17 23:32 74-88-45.0 1
Methylene Chloride ND ug/L 11/02/17 23:32 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/02/17 23:32 108-10-15.0 1
Styrene ND ug/L 11/02/17 23:32 100-42-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/09/2017 04:44 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 13 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92361242
CASWELL CO LF 1584-07-034
Sample:1701-SW-1 Lab ID:92361242007 Collected:10/30/17 15:15 Received:10/31/17 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,1,2-Tetrachloroethane ND ug/L 11/02/17 23:32 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/02/17 23:32 79-34-51.0 1
Tetrachloroethene ND ug/L 11/02/17 23:32 127-18-41.0 1
Toluene ND ug/L 11/02/17 23:32 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 11/02/17 23:32 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/02/17 23:32 79-00-51.0 1
Trichloroethene ND ug/L 11/02/17 23:32 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/02/17 23:32 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/02/17 23:32 96-18-41.0 1
Vinyl acetate ND ug/L 11/02/17 23:32 108-05-42.0 1
Vinyl chloride ND ug/L 11/02/17 23:32 75-01-41.0 1
Xylene (Total)ND ug/L 11/02/17 23:32 1330-20-71.0 1
m&p-Xylene ND ug/L 11/02/17 23:32 179601-23-12.0 1
o-Xylene ND ug/L 11/02/17 23:32 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)97 %11/02/17 23:32 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %11/02/17 23:32 17060-07-070-130 1
Toluene-d8 (S)102 %11/02/17 23:32 2037-26-570-130 1
Sample:1701-SW-2 Lab ID:92361242008 Collected:10/30/17 14:45 Received:10/31/17 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Arsenic ND ug/L 11/04/17 16:12 7440-38-211/02/17 02:3010.0 1
Barium 29.7 ug/L 11/04/17 02:32 7440-39-311/02/17 02:305.0 1
Cadmium ND ug/L 11/04/17 02:32 7440-43-911/02/17 02:301.0 1
Chromium ND ug/L 11/04/17 02:32 7440-47-311/02/17 02:305.0 1
Lead ND ug/L 11/04/17 02:32 7439-92-111/02/17 02:305.0 1
Selenium ND ug/L 11/04/17 02:32 7782-49-211/02/17 02:3010.0 1
Silver ND ug/L 11/04/17 02:32 7440-22-411/02/17 02:305.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 11/07/17 13:54 7439-97-611/07/17 09:250.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/02/17 23:49 67-64-125.0 1
Acrylonitrile ND ug/L 11/02/17 23:49 107-13-110.0 1
Benzene ND ug/L 11/02/17 23:49 71-43-21.0 1
Bromochloromethane ND ug/L 11/02/17 23:49 74-97-51.0 1
Bromodichloromethane ND ug/L 11/02/17 23:49 75-27-41.0 1
Bromoform ND ug/L 11/02/17 23:49 75-25-21.0 1
Bromomethane ND ug/L 11/02/17 23:49 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/02/17 23:49 78-93-35.0 1
Carbon disulfide ND ug/L 11/02/17 23:49 75-15-02.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/09/2017 04:44 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 14 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92361242
CASWELL CO LF 1584-07-034
Sample:1701-SW-2 Lab ID:92361242008 Collected:10/30/17 14:45 Received:10/31/17 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Carbon tetrachloride ND ug/L 11/02/17 23:49 56-23-51.0 1
Chlorobenzene ND ug/L 11/02/17 23:49 108-90-71.0 1
Chloroethane ND ug/L 11/02/17 23:49 75-00-31.0 1
Chloroform ND ug/L 11/02/17 23:49 67-66-31.0 1
Chloromethane ND ug/L 11/02/17 23:49 74-87-31.0 1
Dibromochloromethane ND ug/L 11/02/17 23:49 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/02/17 23:49 106-93-41.0 1
Dibromomethane ND ug/L 11/02/17 23:49 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/02/17 23:49 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 11/02/17 23:49 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/02/17 23:49 110-57-61.0 1
1,1-Dichloroethane ND ug/L 11/02/17 23:49 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/02/17 23:49 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/02/17 23:49 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/02/17 23:49 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/02/17 23:49 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/02/17 23:49 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 11/02/17 23:49 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/02/17 23:49 10061-02-61.0 1
Ethylbenzene ND ug/L 11/02/17 23:49 100-41-41.0 1
2-Hexanone ND ug/L 11/02/17 23:49 591-78-65.0 1
Iodomethane ND ug/L 11/02/17 23:49 74-88-45.0 1
Methylene Chloride ND ug/L 11/02/17 23:49 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/02/17 23:49 108-10-15.0 1
Styrene ND ug/L 11/02/17 23:49 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/02/17 23:49 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/02/17 23:49 79-34-51.0 1
Tetrachloroethene ND ug/L 11/02/17 23:49 127-18-41.0 1
Toluene ND ug/L 11/02/17 23:49 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 11/02/17 23:49 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/02/17 23:49 79-00-51.0 1
Trichloroethene ND ug/L 11/02/17 23:49 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/02/17 23:49 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/02/17 23:49 96-18-41.0 1
Vinyl acetate ND ug/L 11/02/17 23:49 108-05-42.0 1
Vinyl chloride ND ug/L 11/02/17 23:49 75-01-41.0 1
Xylene (Total)ND ug/L 11/02/17 23:49 1330-20-71.0 1
m&p-Xylene ND ug/L 11/02/17 23:49 179601-23-12.0 1
o-Xylene ND ug/L 11/02/17 23:49 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)99 %11/02/17 23:49 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %11/02/17 23:49 17060-07-070-130 1
Toluene-d8 (S)101 %11/02/17 23:49 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/09/2017 04:44 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 15 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92361242
CASWELL CO LF 1584-07-034
Sample:1701-DUPLICATE Lab ID:92361242009 Collected:10/30/17 07:00 Received:10/31/17 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Arsenic 7.2J ug/L 11/08/17 22:10 7440-38-211/07/17 01:1510.0 1
Barium 49.0 ug/L 11/08/17 22:10 7440-39-311/07/17 01:155.0 1
Cadmium ND ug/L 11/08/17 22:10 7440-43-911/07/17 01:151.0 1
Chromium 3.6J ug/L 11/08/17 22:10 7440-47-3 P811/07/17 01:155.0 1
Lead ND ug/L 11/08/17 22:10 7439-92-111/07/17 01:155.0 1
Selenium ND ug/L 11/08/17 22:10 7782-49-211/07/17 01:1510.0 1
Silver ND ug/L 11/08/17 22:10 7440-22-411/07/17 01:155.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 11/07/17 13:56 7439-97-611/07/17 09:250.20 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/03/17 00:07 67-64-125.0 1
Acrylonitrile ND ug/L 11/03/17 00:07 107-13-110.0 1
Benzene 1.7 ug/L 11/03/17 00:07 71-43-21.0 1
Bromochloromethane ND ug/L 11/03/17 00:07 74-97-51.0 1
Bromodichloromethane ND ug/L 11/03/17 00:07 75-27-41.0 1
Bromoform ND ug/L 11/03/17 00:07 75-25-21.0 1
Bromomethane ND ug/L 11/03/17 00:07 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/03/17 00:07 78-93-35.0 1
Carbon disulfide ND ug/L 11/03/17 00:07 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/03/17 00:07 56-23-51.0 1
Chlorobenzene 26.6 ug/L 11/03/17 00:07 108-90-71.0 1
Chloroethane 0.71J ug/L 11/03/17 00:07 75-00-31.0 1
Chloroform ND ug/L 11/03/17 00:07 67-66-31.0 1
Chloromethane ND ug/L 11/03/17 00:07 74-87-31.0 1
Dibromochloromethane ND ug/L 11/03/17 00:07 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/03/17 00:07 106-93-41.0 1
Dibromomethane ND ug/L 11/03/17 00:07 74-95-31.0 1
1,2-Dichlorobenzene 1.9 ug/L 11/03/17 00:07 95-50-11.0 1
1,4-Dichlorobenzene 12.2 ug/L 11/03/17 00:07 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/03/17 00:07 110-57-61.0 1
1,1-Dichloroethane ND ug/L 11/03/17 00:07 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/03/17 00:07 107-06-21.0 1
1,1-Dichloroethene ND ug/L 11/03/17 00:07 75-35-41.0 1
cis-1,2-Dichloroethene 0.33J ug/L 11/03/17 00:07 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/03/17 00:07 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/03/17 00:07 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 11/03/17 00:07 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/03/17 00:07 10061-02-61.0 1
Ethylbenzene ND ug/L 11/03/17 00:07 100-41-41.0 1
2-Hexanone ND ug/L 11/03/17 00:07 591-78-65.0 1
Iodomethane ND ug/L 11/03/17 00:07 74-88-45.0 1
Methylene Chloride ND ug/L 11/03/17 00:07 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/03/17 00:07 108-10-15.0 1
Styrene ND ug/L 11/03/17 00:07 100-42-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/09/2017 04:44 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 16 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92361242
CASWELL CO LF 1584-07-034
Sample:1701-DUPLICATE Lab ID:92361242009 Collected:10/30/17 07:00 Received:10/31/17 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1,1,2-Tetrachloroethane ND ug/L 11/03/17 00:07 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/03/17 00:07 79-34-51.0 1
Tetrachloroethene ND ug/L 11/03/17 00:07 127-18-41.0 1
Toluene ND ug/L 11/03/17 00:07 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 11/03/17 00:07 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/03/17 00:07 79-00-51.0 1
Trichloroethene ND ug/L 11/03/17 00:07 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/03/17 00:07 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/03/17 00:07 96-18-41.0 1
Vinyl acetate ND ug/L 11/03/17 00:07 108-05-42.0 1
Vinyl chloride ND ug/L 11/03/17 00:07 75-01-41.0 1
Xylene (Total)ND ug/L 11/03/17 00:07 1330-20-71.0 1
m&p-Xylene ND ug/L 11/03/17 00:07 179601-23-12.0 1
o-Xylene 0.52J ug/L 11/03/17 00:07 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)101 %11/03/17 00:07 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %11/03/17 00:07 17060-07-070-130 1
Toluene-d8 (S)103 %11/03/17 00:07 2037-26-570-130 1
Sample:1701-TRIP BLANK Lab ID:92361242010 Collected:10/30/17 00:00 Received:10/31/17 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 11/02/17 19:43 67-64-125.0 1
Acrylonitrile ND ug/L 11/02/17 19:43 107-13-110.0 1
Benzene ND ug/L 11/02/17 19:43 71-43-21.0 1
Bromochloromethane ND ug/L 11/02/17 19:43 74-97-51.0 1
Bromodichloromethane ND ug/L 11/02/17 19:43 75-27-41.0 1
Bromoform ND ug/L 11/02/17 19:43 75-25-21.0 1
Bromomethane ND ug/L 11/02/17 19:43 74-83-92.0 1
2-Butanone (MEK)ND ug/L 11/02/17 19:43 78-93-35.0 1
Carbon disulfide ND ug/L 11/02/17 19:43 75-15-02.0 1
Carbon tetrachloride ND ug/L 11/02/17 19:43 56-23-51.0 1
Chlorobenzene ND ug/L 11/02/17 19:43 108-90-71.0 1
Chloroethane ND ug/L 11/02/17 19:43 75-00-31.0 1
Chloroform ND ug/L 11/02/17 19:43 67-66-31.0 1
Chloromethane ND ug/L 11/02/17 19:43 74-87-31.0 1
Dibromochloromethane ND ug/L 11/02/17 19:43 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 11/02/17 19:43 106-93-41.0 1
Dibromomethane ND ug/L 11/02/17 19:43 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 11/02/17 19:43 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 11/02/17 19:43 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 11/02/17 19:43 110-57-61.0 1
1,1-Dichloroethane ND ug/L 11/02/17 19:43 75-34-31.0 1
1,2-Dichloroethane ND ug/L 11/02/17 19:43 107-06-21.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/09/2017 04:44 PM
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Eden, NC 27288
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Page 17 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92361242
CASWELL CO LF 1584-07-034
Sample:1701-TRIP BLANK Lab ID:92361242010 Collected:10/30/17 00:00 Received:10/31/17 10:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1-Dichloroethene ND ug/L 11/02/17 19:43 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 11/02/17 19:43 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 11/02/17 19:43 156-60-51.0 1
1,2-Dichloropropane ND ug/L 11/02/17 19:43 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 11/02/17 19:43 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 11/02/17 19:43 10061-02-61.0 1
Ethylbenzene ND ug/L 11/02/17 19:43 100-41-41.0 1
2-Hexanone ND ug/L 11/02/17 19:43 591-78-65.0 1
Iodomethane ND ug/L 11/02/17 19:43 74-88-45.0 1
Methylene Chloride ND ug/L 11/02/17 19:43 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/02/17 19:43 108-10-15.0 1
Styrene ND ug/L 11/02/17 19:43 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 11/02/17 19:43 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 11/02/17 19:43 79-34-51.0 1
Tetrachloroethene ND ug/L 11/02/17 19:43 127-18-41.0 1
Toluene ND ug/L 11/02/17 19:43 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 11/02/17 19:43 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 11/02/17 19:43 79-00-51.0 1
Trichloroethene ND ug/L 11/02/17 19:43 79-01-61.0 1
Trichlorofluoromethane ND ug/L 11/02/17 19:43 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/02/17 19:43 96-18-41.0 1
Vinyl acetate ND ug/L 11/02/17 19:43 108-05-42.0 1
Vinyl chloride ND ug/L 11/02/17 19:43 75-01-41.0 1
Xylene (Total)ND ug/L 11/02/17 19:43 1330-20-71.0 1
m&p-Xylene ND ug/L 11/02/17 19:43 179601-23-12.0 1
o-Xylene ND ug/L 11/02/17 19:43 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)102 %11/02/17 19:43 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %11/02/17 19:43 17060-07-070-130 1
Toluene-d8 (S)106 %11/02/17 19:43 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/09/2017 04:44 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 18 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92361242
CASWELL CO LF 1584-07-034
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
385522
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92361242001, 92361242002, 92361242003, 92361242004, 92361242005, 92361242006, 92361242007,
92361242008, 92361242009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2138018
Associated Lab Samples:92361242001, 92361242002, 92361242003, 92361242004, 92361242005, 92361242006, 92361242007,
92361242008, 92361242009
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 11/07/17 13:06
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2138019LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.42.5 97 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2138020MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92361124001
2138021
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury ug/L 2.5 87 75-12599 132.5ND 2.2 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/09/2017 04:44 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 19 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92361242
CASWELL CO LF 1584-07-034
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
384924
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92361242001, 92361242002, 92361242003, 92361242004, 92361242005, 92361242006, 92361242007,
92361242008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2133824
Associated Lab Samples:92361242001, 92361242002, 92361242003, 92361242004, 92361242005, 92361242006, 92361242007,
92361242008
Matrix:Water
Analyzed
Arsenic ug/L ND 10.0 11/04/17 14:41
Barium ug/L ND 5.0 11/04/17 01:01
Cadmium ug/L ND 1.0 11/04/17 01:01
Chromium ug/L ND 5.0 11/04/17 01:01
Lead ug/L ND 5.0 11/04/17 01:01
Selenium ug/L ND 10.0 11/04/17 01:01
Silver ug/L ND 5.0 11/04/17 01:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2133825LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 486500 97 80-120
Barium ug/L 523500 105 80-120
Cadmium ug/L 504500 101 80-120
Chromium ug/L 486500 97 80-120
Lead ug/L 490500 98 80-120
Selenium ug/L 507500 101 80-120
Silver ug/L 249250 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2133826MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92361374002
2133827
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic ug/L 500 97 75-12597 0500ND487486
Barium ug/L 500 103 75-125105 15000.057
mg/L 572 580
Cadmium ug/L 500 99 75-125100 1500ND497500
Chromium ug/L 500 96 75-12597 1500ND482486
Lead ug/L 500 95 75-12596 1500ND476480
Selenium ug/L 500 99 75-125100 1500ND495501
Silver ug/L 250 98 75-125100 2250ND245249
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/09/2017 04:44 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 20 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92361242
CASWELL CO LF 1584-07-034
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
385483
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92361242009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2137841
Associated Lab Samples:92361242009
Matrix:Water
Analyzed
Arsenic ug/L ND 10.0 11/08/17 21:26
Barium ug/L ND 5.0 11/08/17 21:26
Cadmium ug/L ND 1.0 11/08/17 21:26
Chromium ug/L ND 5.0 11/09/17 15:15
Lead ug/L ND 5.0 11/08/17 21:26
Selenium ug/L ND 10.0 11/08/17 21:26
Silver ug/L ND 5.0 11/08/17 21:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2137842LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 465500 93 80-120
Barium ug/L 487500 97 80-120
Cadmium ug/L 477500 95 80-120
Chromium ug/L 474500 95 80-120
Lead ug/L 469500 94 80-120
Selenium ug/L 483500 97 80-120
Silver ug/L 240250 96 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2137843MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92361332001
2137844
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic ug/L 500 93 75-12594 1500ND468471
Barium ug/L 500 98 75-125100 150025.9 516 524
Cadmium ug/L 500 96 75-12596 0500ND481482
Chromium ug/L 500 95 75-12596 1500ND476479
Lead ug/L 500 94 75-12594 0500ND470471
Selenium ug/L 500 96 75-12596 0500ND479478
Silver ug/L 250 97 75-12597 1250ND242243
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/09/2017 04:44 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 21 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92361242
CASWELL CO LF 1584-07-034
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
385076
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92361242001, 92361242002, 92361242003, 92361242004, 92361242005, 92361242006, 92361242007,
92361242008, 92361242009, 92361242010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2134722
Associated Lab Samples:92361242001, 92361242002, 92361242003, 92361242004, 92361242005, 92361242006, 92361242007,
92361242008, 92361242009, 92361242010
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 11/02/17 18:15
1,1,1-Trichloroethane ug/L ND 1.0 11/02/17 18:15
1,1,2,2-Tetrachloroethane ug/L ND 1.0 11/02/17 18:15
1,1,2-Trichloroethane ug/L ND 1.0 11/02/17 18:15
1,1-Dichloroethane ug/L ND 1.0 11/02/17 18:15
1,1-Dichloroethene ug/L ND 1.0 11/02/17 18:15
1,2,3-Trichloropropane ug/L ND 1.0 11/02/17 18:15
1,2-Dibromoethane (EDB)ug/L ND 1.0 11/02/17 18:15
1,2-Dichlorobenzene ug/L ND 1.0 11/02/17 18:15
1,2-Dichloroethane ug/L ND 1.0 11/02/17 18:15
1,2-Dichloropropane ug/L ND 1.0 11/02/17 18:15
1,4-Dichlorobenzene ug/L ND 1.0 11/02/17 18:15
2-Butanone (MEK)ug/L ND 5.0 11/02/17 18:15
2-Hexanone ug/L ND 5.0 11/02/17 18:15
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 11/02/17 18:15
Acetone ug/L ND 25.0 11/02/17 18:15
Acrylonitrile ug/L ND 10.0 11/02/17 18:15
Benzene ug/L ND 1.0 11/02/17 18:15
Bromochloromethane ug/L ND 1.0 11/02/17 18:15
Bromodichloromethane ug/L ND 1.0 11/02/17 18:15
Bromoform ug/L ND 1.0 11/02/17 18:15
Bromomethane ug/L ND 2.0 11/02/17 18:15
Carbon disulfide ug/L ND 2.0 11/02/17 18:15
Carbon tetrachloride ug/L ND 1.0 11/02/17 18:15
Chlorobenzene ug/L ND 1.0 11/02/17 18:15
Chloroethane ug/L ND 1.0 11/02/17 18:15
Chloroform ug/L ND 1.0 11/02/17 18:15
Chloromethane ug/L ND 1.0 11/02/17 18:15
cis-1,2-Dichloroethene ug/L ND 1.0 11/02/17 18:15
cis-1,3-Dichloropropene ug/L ND 1.0 11/02/17 18:15
Dibromochloromethane ug/L ND 1.0 11/02/17 18:15
Dibromomethane ug/L ND 1.0 11/02/17 18:15
Ethylbenzene ug/L ND 1.0 11/02/17 18:15
Iodomethane ug/L ND 5.0 11/02/17 18:15
m&p-Xylene ug/L ND 2.0 11/02/17 18:15
Methylene Chloride ug/L ND 1.0 11/02/17 18:15
o-Xylene ug/L ND 1.0 11/02/17 18:15
Styrene ug/L ND 1.0 11/02/17 18:15
Tetrachloroethene ug/L ND 1.0 11/02/17 18:15
Toluene ug/L ND 1.0 11/02/17 18:15
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/09/2017 04:44 PM
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205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 22 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92361242
CASWELL CO LF 1584-07-034
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2134722
Associated Lab Samples:92361242001, 92361242002, 92361242003, 92361242004, 92361242005, 92361242006, 92361242007,
92361242008, 92361242009, 92361242010
Matrix:Water
Analyzed
trans-1,2-Dichloroethene ug/L ND 1.0 11/02/17 18:15
trans-1,3-Dichloropropene ug/L ND 1.0 11/02/17 18:15
trans-1,4-Dichloro-2-butene ug/L ND 1.0 11/02/17 18:15
Trichloroethene ug/L ND 1.0 11/02/17 18:15
Trichlorofluoromethane ug/L ND 1.0 11/02/17 18:15
Vinyl acetate ug/L ND 2.0 11/02/17 18:15
Vinyl chloride ug/L ND 1.0 11/02/17 18:15
Xylene (Total)ug/L ND 1.0 11/02/17 18:15
1,2-Dichloroethane-d4 (S)%102 70-130 11/02/17 18:15
4-Bromofluorobenzene (S)%101 70-130 11/02/17 18:15
Toluene-d8 (S)%102 70-130 11/02/17 18:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2134723LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.150 98 80-125
1,1,1-Trichloroethane ug/L 45.850 92 71-129
1,1,2,2-Tetrachloroethane ug/L 44.850 90 79-124
1,1,2-Trichloroethane ug/L 48.350 97 85-125
1,1-Dichloroethane ug/L 45.750 91 73-126
1,1-Dichloroethene ug/L 46.950 94 66-135
1,2,3-Trichloropropane ug/L 46.750 93 75-130
1,2-Dibromoethane (EDB)ug/L 50.250 100 83-124
1,2-Dichlorobenzene ug/L 45.850 92 80-133
1,2-Dichloroethane ug/L 46.650 93 67-128
1,2-Dichloropropane ug/L 50.850 102 75-132
1,4-Dichlorobenzene ug/L 46.050 92 78-130
2-Butanone (MEK)ug/L 91.7100 92 61-144
2-Hexanone ug/L 87.2100 87 68-143
4-Methyl-2-pentanone (MIBK)ug/L 92.0100 92 72-135
Acetone ug/L 94.4100 94 48-146
Acrylonitrile ug/L 231250 93 40-160
Benzene ug/L 46.050 92 80-125
Bromochloromethane ug/L 44.850 90 71-125
Bromodichloromethane ug/L 47.050 94 78-124
Bromoform ug/L 46.550 93 71-128
Bromomethane ug/L 51.150 102 40-160
Carbon disulfide ug/L 47.350 95 50-160
Carbon tetrachloride ug/L 44.750 89 69-131
Chlorobenzene ug/L 47.250 94 81-122
Chloroethane ug/L 52.650 105 39-148
Chloroform ug/L 42.350 85 73-127
Chloromethane ug/L 47.850 96 44-146
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/09/2017 04:44 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 23 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92361242
CASWELL CO LF 1584-07-034
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2134723LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 46.950 94 74-124
cis-1,3-Dichloropropene ug/L 50.150 100 72-132
Dibromochloromethane ug/L 49.850 100 78-125
Dibromomethane ug/L 46.550 93 82-120
Ethylbenzene ug/L 46.450 93 79-121
Iodomethane ug/L 85.7100 86 39-154
m&p-Xylene ug/L 93.8100 94 81-124
Methylene Chloride ug/L 50.850 102 64-133
o-Xylene ug/L 45.250 90 79-131
Styrene ug/L 45.750 91 84-126
Tetrachloroethene ug/L 49.050 98 78-122
Toluene ug/L 45.150 90 80-121
trans-1,2-Dichloroethene ug/L 47.050 94 71-127
trans-1,3-Dichloropropene ug/L 49.250 98 69-141
trans-1,4-Dichloro-2-butene ug/L 47.650 95 40-160
Trichloroethene ug/L 47.750 95 78-122
Trichlorofluoromethane ug/L 47.650 95 53-137
Vinyl acetate ug/L 115100 115 40-160
Vinyl chloride ug/L 45.550 91 58-137
Xylene (Total)ug/L 139150 93 81-126
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%94 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2134725MATRIX SPIKE SAMPLE:
MSSpike
Result
92361124002
1,1,1,2-Tetrachloroethane ug/L 19.820 99 70-130ND
1,1,1-Trichloroethane ug/L 20.820 104 70-130ND
1,1,2,2-Tetrachloroethane ug/L 18.620 93 70-130ND
1,1,2-Trichloroethane ug/L 19.020 95 70-130ND
1,1-Dichloroethane ug/L 20.020 100 70-130ND
1,1-Dichloroethene ug/L 23.620 118 70-166ND
1,2,3-Trichloropropane ug/L 19.720 98 70-130ND
1,2-Dibromoethane (EDB)ug/L 19.620 98 70-130ND
1,2-Dichlorobenzene ug/L 20.520 103 70-130ND
1,2-Dichloroethane ug/L 20.620 103 70-130ND
1,2-Dichloropropane ug/L 22.020 110 70-130ND
1,4-Dichlorobenzene ug/L 20.420 102 70-130ND
2-Butanone (MEK)ug/L 36.740 92 70-130ND
2-Hexanone ug/L 36.140 90 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 40.940 102 70-130ND
Acetone ug/L 41.240 103 70-130ND
Acrylonitrile ug/L 101100 101 70-130ND
Benzene ug/L 20.020 100 70-148ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/09/2017 04:44 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 24 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92361242
CASWELL CO LF 1584-07-034
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2134725MATRIX SPIKE SAMPLE:
MSSpike
Result
92361124002
Bromochloromethane ug/L 20.320 102 70-130ND
Bromodichloromethane ug/L 20.220 101 70-130ND
Bromoform ug/L 17.420 87 70-130ND
Bromomethane ug/L 13.2 M1206670-130ND
Carbon disulfide ug/L 22.720 113 70-130ND
Carbon tetrachloride ug/L 20.920 105 70-130ND
Chlorobenzene ug/L 19.720 99 70-146ND
Chloroethane ug/L 26.1 M12013170-130ND
Chloroform ug/L 18.520 92 70-130ND
Chloromethane ug/L 18.520 93 70-130ND
cis-1,2-Dichloroethene ug/L 22.020 110 70-130ND
cis-1,3-Dichloropropene ug/L 20.020 100 70-130ND
Dibromochloromethane ug/L 18.520 93 70-130ND
Dibromomethane ug/L 20.420 102 70-130ND
Ethylbenzene ug/L 19.720 98 70-130ND
Iodomethane ug/L 18.3 M1404670-130ND
m&p-Xylene ug/L 39.840 99 70-130ND
Methylene Chloride ug/L 20.520 102 70-130ND
o-Xylene ug/L 19.120 95 70-130ND
Styrene ug/L 17.020 85 70-130ND
Tetrachloroethene ug/L 21.020 105 70-130ND
Toluene ug/L 20.520 103 70-155ND
trans-1,2-Dichloroethene ug/L 21.020 105 70-130ND
trans-1,3-Dichloropropene ug/L 19.820 99 70-130ND
trans-1,4-Dichloro-2-butene ug/L 12.8 M1206470-130ND
Trichloroethene ug/L 21.120 106 69-151ND
Trichlorofluoromethane ug/L 22.620 113 70-130ND
Vinyl acetate ug/L 37.440 93 70-130ND
Vinyl chloride ug/L 22.120 110 70-130ND
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%95 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92361124001
2134724SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1-Dichloroethane ug/L NDND
1,1-Dichloroethene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/09/2017 04:44 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 25 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92361242
CASWELL CO LF 1584-07-034
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92361124001
2134724SAMPLE DUPLICATE:
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Hexanone ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
Acrylonitrile ug/L NDND
Benzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon disulfide ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L 0.40J0.43J
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L 0.96J1.0
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Ethylbenzene ug/L NDND
Iodomethane ug/L NDND
m&p-Xylene ug/L NDND
Methylene Chloride ug/L NDND
o-Xylene ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
trans-1,4-Dichloro-2-butene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl acetate ug/L NDND
Vinyl chloride ug/L NDND
Xylene (Total)ug/L NDND
1,2-Dichloroethane-d4 (S)%105 0105
4-Bromofluorobenzene (S)%98 098
Toluene-d8 (S)%118 12105
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/09/2017 04:44 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 26 of 31
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92361242
CASWELL CO LF 1584-07-034
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Analyte was detected in the method blank. All associated samples had concentrations of at least ten times greater than
the blank or were below the reporting limit.P8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/09/2017 04:44 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 27 of 31
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92361242
CASWELL CO LF 1584-07-034
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92361242001 384924 3850031701-MW-1 EPA 3010A EPA 6010
92361242002 384924 3850031701-MW-2 EPA 3010A EPA 6010
92361242003 384924 3850031701-MW-3 EPA 3010A EPA 6010
92361242004 384924 3850031701-MW-4 EPA 3010A EPA 6010
92361242005 384924 3850031701-MW-5 EPA 3010A EPA 6010
92361242006 384924 3850031701-MW-6 EPA 3010A EPA 6010
92361242007 384924 3850031701-SW-1 EPA 3010A EPA 6010
92361242008 384924 3850031701-SW-2 EPA 3010A EPA 6010
92361242009 385483 3855611701-DUPLICATE EPA 3010A EPA 6010
92361242001 385522 3855521701-MW-1 EPA 7470 EPA 7470
92361242002 385522 3855521701-MW-2 EPA 7470 EPA 7470
92361242003 385522 3855521701-MW-3 EPA 7470 EPA 7470
92361242004 385522 3855521701-MW-4 EPA 7470 EPA 7470
92361242005 385522 3855521701-MW-5 EPA 7470 EPA 7470
92361242006 385522 3855521701-MW-6 EPA 7470 EPA 7470
92361242007 385522 3855521701-SW-1 EPA 7470 EPA 7470
92361242008 385522 3855521701-SW-2 EPA 7470 EPA 7470
92361242009 385522 3855521701-DUPLICATE EPA 7470 EPA 7470
92361242001 3850761701-MW-1 EPA 8260
92361242002 3850761701-MW-2 EPA 8260
92361242003 3850761701-MW-3 EPA 8260
92361242004 3850761701-MW-4 EPA 8260
92361242005 3850761701-MW-5 EPA 8260
92361242006 3850761701-MW-6 EPA 8260
92361242007 3850761701-SW-1 EPA 8260
92361242008 3850761701-SW-2 EPA 8260
92361242009 3850761701-DUPLICATE EPA 8260
92361242010 3850761701-TRIP BLANK EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/09/2017 04:44 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 28 of 31
Page 29 of 31
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Page 31 of 31
Appendix V – NCDEQ EDD (CD only)