RA-1137_7489_CA_MRP_20180730_2nd Qtr 2018 NPDES

102-A Woodwinds Industrial Court
Cary NC, 27511
919.467.3090 919.467.3515Phone:FAX:
ENCO Workorder(s): CB08873
Durham, NC 27703
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Enclosure(s)
Project Number: 7023, Project Name/Desc: Dixie
Attn: Justin Abreu
EMS Environmental (EM001)
117 South Hoover Road
Chuck Smith
Project Manager
Tuesday, July 10, 2018
RE: Laboratory Results for
Dear Justin Abreu,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Friday, June 22, 2018.
Enclosure(s)
Page 1 of 28This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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SAMPLE SUMMARY/LABORATORY CHRONICLE
Influent 2nd Qtr 2018 CB08873-01RE1 Sampled:06/22/18 11:49 Received:06/22/18 13:40Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
SM 6200B-1997 07/06/18 07/03/18 11:59 07/05/18 15:20Same
Effluent 2nd Qtr 2018 CB08873-02 Sampled:06/22/18 12:06 Received:06/22/18 13:40Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
EPA 1664B 07/20/18 07/02/18 12:10 07/03/18 18:01EPA 1664B
EPA 420.1 07/20/18 07/02/18 10:15 07/03/18 09:30Same
EPA 6010D 06/25/18 06/22/18 14:23 07/09/18 14:4112/19/18SM18 3030C
EPA 625 06/29/18 06/25/18 09:50 06/26/18 23:1308/04/18Same
SM 2540D-1997 06/29/18 06/26/18 07:44 06/26/18 07:44NO PREP
SM 6200B-1997 07/06/18 06/28/18 09:55 06/29/18 05:29Same
Trip Blank CB08873-03 Sampled:06/22/18 11:49 Received:06/22/18 13:40Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
SM 6200B-1997 07/06/18 06/28/18 09:55 06/29/18 05:59Same
Page 2 of 28This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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SAMPLE DETECTION SUMMARY
Lab ID:Client ID:Influent 2nd Qtr 2018 CB08873-01RE1
Analyte MethodUnitsPQLResultsFlag NotesMDL
12 1.0 ug/L SM 6200B-1997 1,2,4-Trimethylbenzene 0.067
3.8 1.0 ug/L SM 6200B-1997 1,3,5-Trimethylbenzene 0.10
20 1.0 ug/L SM 6200B-1997 Benzene 0.050
2.0 1.0 ug/L SM 6200B-1997 Ethylbenzene 0.10
1.2 1.0 ug/L SM 6200B-1997 Isopropyl Ether 0.21
17 2.0 ug/L SM 6200B-1997 m,p-Xylenes 0.18
11 1.0 ug/L SM 6200B-1997 Methyl-tert-Butyl Ether 0.12
23 1.0 ug/L SM 6200B-1997 Naphthalene 0.086
1.5 1.0 ug/L SM 6200B-1997 n-Butyl Benzene 0.074
19 1.0 ug/L SM 6200B-1997 o-Xylene 0.088
14 1.0 ug/L SM 6200B-1997 Toluene 0.053
36 1.0 ug/L SM 6200B-1997 Xylenes (Total)0.22
Page 3 of 28This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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ANALYTICAL RESULTS
Influent 2nd Qtr 2018Description:Lab Sample ID:CB08873-01 06/22/18 13:40Received:
CB08873Work Order:06/22/18 11:49Sampled:Waste WaterMatrix:
James DodsonSampled By:Project:Dixie
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 07/05/18 15:201,1,1,2-Tetrachloroethane [630-20-6]^0.091 MRK8F290231.00.091 U 1
ug/L SM 6200B-1997 07/05/18 15:201,1,1-Trichloroethane [71-55-6]^0.15 MRK8F290231.00.15 U 1
ug/L SM 6200B-1997 07/05/18 15:201,1,2,2-Tetrachloroethane [79-34-5]^0.085 MRK8F290231.00.085 U 1
ug/L SM 6200B-1997 07/05/18 15:201,1,2-Trichloroethane [79-00-5]^0.068 MRK8F290231.00.068 U 1
ug/L SM 6200B-1997 07/05/18 15:201,1-Dichloroethane [75-34-3]^0.050 MRK8F290231.00.050 U 1
ug/L SM 6200B-1997 07/05/18 15:201,1-Dichloroethene [75-35-4]^0.15 MRK8F290231.00.15 U 1
ug/L SM 6200B-1997 07/05/18 15:201,1-Dichloropropene [563-58-6]^0.063 MRK8F290231.00.063 U 1
ug/L SM 6200B-1997 07/05/18 15:201,2,3-Trichlorobenzene [87-61-6]^0.25 MRK8F290231.00.25 U 1
ug/L SM 6200B-1997 07/05/18 15:201,2,3-Trichloropropane [96-18-4]^0.15 MRK8F290231.00.15 U 1
ug/L SM 6200B-1997 07/05/18 15:201,2,4-Trichlorobenzene [120-82-1]^0.097 MRK8F290231.00.097 U 1
ug/L SM 6200B-1997 07/05/18 15:201,2,4-Trimethylbenzene [95-63-6]^0.067 MRK8F290231.012 1
ug/L SM 6200B-1997 07/05/18 15:201,2-Dibromo-3-chloropropane [96-12-8]^0.48 MRK8F290231.00.48 U 1
ug/L SM 6200B-1997 07/05/18 15:201,2-Dibromoethane [106-93-4]^0.42 MRK8F290231.00.42 U 1
ug/L SM 6200B-1997 07/05/18 15:201,2-Dichlorobenzene [95-50-1]^0.052 MRK8F290231.00.052 U 1
ug/L SM 6200B-1997 07/05/18 15:201,2-Dichloroethane [107-06-2]^0.082 MRK8F290231.00.082 U 1
ug/L SM 6200B-1997 07/05/18 15:201,2-Dichloropropane [78-87-5]^0.098 MRK8F290231.00.098 U 1
ug/L SM 6200B-1997 07/05/18 15:201,3,5-Trimethylbenzene [108-67-8]^0.10 MRK8F290231.03.8 1
ug/L SM 6200B-1997 07/05/18 15:201,3-Dichlorobenzene [541-73-1]^0.092 MRK8F290231.00.092 U 1
ug/L SM 6200B-1997 07/05/18 15:201,3-Dichloropropane [142-28-9]^0.15 MRK8F290231.00.15 U 1
ug/L SM 6200B-1997 07/05/18 15:201,4-Dichlorobenzene [106-46-7]^0.10 MRK8F290231.00.10 U 1
ug/L SM 6200B-1997 07/05/18 15:202,2-Dichloropropane [594-20-7]^0.12 MRK8F290231.00.12 U 1
ug/L SM 6200B-1997 07/05/18 15:202-Chlorotoluene [95-49-8]^0.10 MRK8F290231.00.10 U 1
ug/L SM 6200B-1997 07/05/18 15:204-Chlorotoluene [106-43-4]^0.10 MRK8F290231.00.10 U 1
ug/L SM 6200B-1997 07/05/18 15:204-Isopropyltoluene [99-87-6]^0.066 MRK8F290231.00.066 U 1
ug/L SM 6200B-1997 07/05/18 15:20Benzene [71-43-2]^0.050 MRK8F290231.020 1
ug/L SM 6200B-1997 07/05/18 15:20Bromobenzene [108-86-1]^0.13 MRK8F290231.00.13 U 1
ug/L SM 6200B-1997 07/05/18 15:20Bromochloromethane [74-97-5]^0.11 MRK8F290231.00.11 U 1
ug/L SM 6200B-1997 07/05/18 15:20Bromodichloromethane [75-27-4]^0.10 MRK8F290231.00.10 U 1
ug/L SM 6200B-1997 07/05/18 15:20Bromoform [75-25-2]^0.20 MRK8F290231.00.20 U 1
ug/L SM 6200B-1997 07/05/18 15:20Bromomethane [74-83-9]^0.28 MRK8F290231.00.28 U 1
ug/L SM 6200B-1997 07/05/18 15:20Carbon Tetrachloride [56-23-5]^0.082 MRK8F290231.00.082 U 1
ug/L SM 6200B-1997 07/05/18 15:20Chlorobenzene [108-90-7]^0.069 MRK8F290231.00.069 U 1
ug/L SM 6200B-1997 07/05/18 15:20Chloroethane [75-00-3]^0.18 MRK8F290231.00.18 U 1
ug/L SM 6200B-1997 07/05/18 15:20Chloroform [67-66-3]^0.083 MRK8F290231.00.083 U 1
ug/L SM 6200B-1997 07/05/18 15:20Chloromethane [74-87-3]^0.050 MRK8F290231.00.050 U 1
ug/L SM 6200B-1997 07/05/18 15:20cis-1,2-Dichloroethene [156-59-2]^0.075 MRK8F290231.00.075 U 1
ug/L SM 6200B-1997 07/05/18 15:20cis-1,3-Dichloropropene [10061-01-5]^0.073 MRK8F290231.00.073 U 1
ug/L SM 6200B-1997 07/05/18 15:20Dibromochloromethane [124-48-1]^0.067 MRK8F290231.00.067 U 1
ug/L SM 6200B-1997 07/05/18 15:20Dibromomethane [74-95-3]^0.13 MRK8F290231.00.13 U 1
ug/L SM 6200B-1997 07/05/18 15:20Dichlorodifluoromethane [75-71-8]^0.091 MRK8F290231.00.091 U 1
ug/L SM 6200B-1997 07/05/18 15:20Ethylbenzene [100-41-4]^0.10 MRK8F290231.02.0 1
ug/L SM 6200B-1997 07/05/18 15:20Freon 113 [76-13-1]^0.35 MRK8F290231.00.35 U 1
ug/L SM 6200B-1997 07/05/18 15:20Hexachlorobutadiene [87-68-3]^0.15 MRK8F290231.00.15 U 1
ug/L SM 6200B-1997 07/05/18 15:20Isopropyl Ether [108-20-3]^0.21 MRK8F290231.01.2 1
ug/L SM 6200B-1997 07/05/18 15:20Isopropylbenzene [98-82-8]^0.13 MRK8F290231.00.13 U 1
ug/L SM 6200B-1997 07/05/18 15:20m,p-Xylenes [108-38-3/106-42-3]^0.18 MRK8F290232.017 1
ug/L SM 6200B-1997 07/05/18 15:20Methylene Chloride [75-09-2]^0.070 MRK8F290232.00.070 U 1
Page 4 of 28This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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ANALYTICAL RESULTS
Influent 2nd Qtr 2018Description:Lab Sample ID:CB08873-01 06/22/18 13:40Received:
CB08873Work Order:06/22/18 11:49Sampled:Waste WaterMatrix:
James DodsonSampled By:Project:Dixie
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 07/05/18 15:20Methyl-tert-Butyl Ether [1634-04-4]^0.12 MRK8F290231.011 1
ug/L SM 6200B-1997 07/05/18 15:20Naphthalene [91-20-3]^0.086 MRK8F290231.023 1
ug/L SM 6200B-1997 07/05/18 15:20n-Butyl Benzene [104-51-8]^0.074 MRK8F290231.01.5 1
ug/L SM 6200B-1997 07/05/18 15:20n-Propyl Benzene [103-65-1]^0.073 MRK8F290231.00.073 U 1
ug/L SM 6200B-1997 07/05/18 15:20o-Xylene [95-47-6]^0.088 MRK8F290231.019 1
ug/L SM 6200B-1997 07/05/18 15:20sec-Butylbenzene [135-98-8]^0.053 MRK8F290231.00.053 U 1
ug/L SM 6200B-1997 07/05/18 15:20Styrene [100-42-5]^0.082 MRK8F290231.00.082 U 1
ug/L SM 6200B-1997 07/05/18 15:20tert-Butylbenzene [98-06-6]^0.094 MRK8F290231.00.094 U 1
ug/L SM 6200B-1997 07/05/18 15:20Tetrachloroethene [127-18-4]^0.099 MRK8F290231.00.099 U 1
ug/L SM 6200B-1997 07/05/18 15:20Toluene [108-88-3]^0.053 MRK8F290231.014 1
ug/L SM 6200B-1997 07/05/18 15:20trans-1,2-Dichloroethene [156-60-5]^0.11 MRK8F290231.00.11 U 1
ug/L SM 6200B-1997 07/05/18 15:20trans-1,3-Dichloropropene [10061-02-6]^0.080 MRK8F290231.00.080 U 1
ug/L SM 6200B-1997 07/05/18 15:20Trichloroethene [79-01-6]^0.13 MRK8F290231.00.13 U 1
ug/L SM 6200B-1997 07/05/18 15:20Trichlorofluoromethane [75-69-4]^0.15 MRK8F290231.00.15 U 1
ug/L SM 6200B-1997 07/05/18 15:20Vinyl chloride [75-01-4]^0.083 MRK8F290231.00.083 U 1
ug/L SM 6200B-1997 07/05/18 15:20Xylenes (Total) [1330-20-7]^0.22 MRK8F290231.036 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 70-13089 %MRKSM 6200B-1997 07/05/18 15:208F290234550.0 1
Dibromofluoromethane 70-13074 %MRKSM 6200B-1997 07/05/18 15:208F290233750.0 1
Toluene-d8 70-13078 %MRKSM 6200B-1997 07/05/18 15:208F290233950.0 1
Page 5 of 28This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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ANALYTICAL RESULTS
Effluent 2nd Qtr 2018Description:Lab Sample ID:CB08873-02 06/22/18 13:40Received:
CB08873Work Order:06/22/18 12:06Sampled:Waste WaterMatrix:
James DodsonSampled By:Project:Dixie
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 06/29/18 05:291,1,1,2-Tetrachloroethane [630-20-6]^0.091 MRK8F280151.00.091 U 1
ug/L SM 6200B-1997 06/29/18 05:291,1,1-Trichloroethane [71-55-6]^0.15 MRK8F280151.00.15 U 1
ug/L SM 6200B-1997 06/29/18 05:291,1,2,2-Tetrachloroethane [79-34-5]^0.085 MRK8F280151.00.085 U 1
ug/L SM 6200B-1997 06/29/18 05:291,1,2-Trichloroethane [79-00-5]^0.068 MRK8F280151.00.068 U 1
ug/L SM 6200B-1997 06/29/18 05:291,1-Dichloroethane [75-34-3]^0.050 MRK8F280151.00.050 U 1
ug/L SM 6200B-1997 06/29/18 05:291,1-Dichloroethene [75-35-4]^0.15 MRK8F280151.00.15 U 1
ug/L SM 6200B-1997 06/29/18 05:291,1-Dichloropropene [563-58-6]^0.063 MRK8F280151.00.063 U 1
ug/L SM 6200B-1997 06/29/18 05:291,2,3-Trichlorobenzene [87-61-6]^0.25 MRK8F280151.00.25 U 1
ug/L SM 6200B-1997 06/29/18 05:291,2,3-Trichloropropane [96-18-4]^0.15 MRK8F280151.00.15 U 1
ug/L SM 6200B-1997 06/29/18 05:291,2,4-Trichlorobenzene [120-82-1]^0.097 MRK8F280151.00.097 U 1
ug/L SM 6200B-1997 06/29/18 05:291,2,4-Trimethylbenzene [95-63-6]^0.067 MRK8F280151.00.067 U 1
ug/L SM 6200B-1997 06/29/18 05:291,2-Dibromo-3-chloropropane [96-12-8]^0.48 MRK8F280151.00.48 U 1
ug/L SM 6200B-1997 06/29/18 05:291,2-Dibromoethane [106-93-4]^0.42 MRK8F280151.00.42 U 1
ug/L SM 6200B-1997 06/29/18 05:291,2-Dichlorobenzene [95-50-1]^0.052 MRK8F280151.00.052 U 1
ug/L SM 6200B-1997 06/29/18 05:291,2-Dichloroethane [107-06-2]^0.082 MRK8F280151.00.082 U 1
ug/L SM 6200B-1997 06/29/18 05:291,2-Dichloropropane [78-87-5]^0.098 MRK8F280151.00.098 U 1
ug/L SM 6200B-1997 06/29/18 05:291,3,5-Trimethylbenzene [108-67-8]^0.10 MRK8F280151.00.10 U 1
ug/L SM 6200B-1997 06/29/18 05:291,3-Dichlorobenzene [541-73-1]^0.092 MRK8F280151.00.092 U 1
ug/L SM 6200B-1997 06/29/18 05:291,3-Dichloropropane [142-28-9]^0.15 MRK8F280151.00.15 U 1
ug/L SM 6200B-1997 06/29/18 05:291,4-Dichlorobenzene [106-46-7]^0.10 MRK8F280151.00.10 U 1
ug/L SM 6200B-1997 06/29/18 05:292,2-Dichloropropane [594-20-7]^0.12 MRK8F280151.00.12 U 1
ug/L SM 6200B-1997 06/29/18 05:292-Chlorotoluene [95-49-8]^0.10 MRK8F280151.00.10 U 1
ug/L SM 6200B-1997 06/29/18 05:294-Chlorotoluene [106-43-4]^0.10 MRK8F280151.00.10 U 1
ug/L SM 6200B-1997 06/29/18 05:294-Isopropyltoluene [99-87-6]^0.066 MRK8F280151.00.066 U 1
ug/L SM 6200B-1997 06/29/18 05:29Benzene [71-43-2]^0.050 MRK8F280151.00.050 U 1
ug/L SM 6200B-1997 06/29/18 05:29Bromobenzene [108-86-1]^0.13 MRK8F280151.00.13 U 1
ug/L SM 6200B-1997 06/29/18 05:29Bromochloromethane [74-97-5]^0.11 MRK8F280151.00.11 U 1
ug/L SM 6200B-1997 06/29/18 05:29Bromodichloromethane [75-27-4]^0.10 MRK8F280151.00.10 U 1
ug/L SM 6200B-1997 06/29/18 05:29Bromoform [75-25-2]^0.20 MRK8F280151.00.20 U 1
ug/L SM 6200B-1997 06/29/18 05:29Bromomethane [74-83-9]^0.28 MRK8F280151.00.28 U 1
ug/L SM 6200B-1997 06/29/18 05:29Carbon Tetrachloride [56-23-5]^0.082 MRK8F280151.00.082 U 1
ug/L SM 6200B-1997 06/29/18 05:29Chlorobenzene [108-90-7]^0.069 MRK8F280151.00.069 U 1
ug/L SM 6200B-1997 06/29/18 05:29Chloroethane [75-00-3]^0.18 MRK8F280151.00.18 U 1
ug/L SM 6200B-1997 06/29/18 05:29Chloroform [67-66-3]^0.083 MRK8F280151.00.083 U 1
ug/L SM 6200B-1997 06/29/18 05:29Chloromethane [74-87-3]^0.050 MRK8F280151.00.050 U 1
ug/L SM 6200B-1997 06/29/18 05:29cis-1,2-Dichloroethene [156-59-2]^0.075 MRK8F280151.00.075 U 1
ug/L SM 6200B-1997 06/29/18 05:29cis-1,3-Dichloropropene [10061-01-5]^0.073 MRK8F280151.00.073 U 1
ug/L SM 6200B-1997 06/29/18 05:29Dibromochloromethane [124-48-1]^0.067 MRK8F280151.00.067 U 1
ug/L SM 6200B-1997 06/29/18 05:29Dibromomethane [74-95-3]^0.13 MRK8F280151.00.13 U 1
ug/L SM 6200B-1997 06/29/18 05:29Dichlorodifluoromethane [75-71-8]^0.091 MRK8F280151.00.091 U 1
ug/L SM 6200B-1997 06/29/18 05:29Ethylbenzene [100-41-4]^0.10 MRK8F280151.00.10 U 1
ug/L SM 6200B-1997 06/29/18 05:29Freon 113 [76-13-1]^0.35 MRK8F280151.00.35 U 1
ug/L SM 6200B-1997 06/29/18 05:29Hexachlorobutadiene [87-68-3]^0.15 MRK8F280151.00.15 U 1
ug/L SM 6200B-1997 06/29/18 05:29Isopropyl Ether [108-20-3]^0.21 MRK8F280151.00.21 U 1
ug/L SM 6200B-1997 06/29/18 05:29Isopropylbenzene [98-82-8]^0.13 MRK8F280151.00.13 U 1
ug/L SM 6200B-1997 06/29/18 05:29m,p-Xylenes [108-38-3/106-42-3]^0.18 MRK8F280152.00.18 U 1
ug/L SM 6200B-1997 06/29/18 05:29Methylene Chloride [75-09-2]^0.070 MRK8F280152.00.070 U 1
Page 6 of 28This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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ANALYTICAL RESULTS
Effluent 2nd Qtr 2018Description:Lab Sample ID:CB08873-02 06/22/18 13:40Received:
CB08873Work Order:06/22/18 12:06Sampled:Waste WaterMatrix:
James DodsonSampled By:Project:Dixie
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 06/29/18 05:29Methyl-tert-Butyl Ether [1634-04-4]^0.12 MRK8F280151.00.12 U 1
ug/L SM 6200B-1997 06/29/18 05:29Naphthalene [91-20-3]^0.086 MRK8F280151.00.086 U 1
ug/L SM 6200B-1997 06/29/18 05:29n-Butyl Benzene [104-51-8]^0.074 MRK8F280151.00.074 U 1
ug/L SM 6200B-1997 06/29/18 05:29n-Propyl Benzene [103-65-1]^0.073 MRK8F280151.00.073 U 1
ug/L SM 6200B-1997 06/29/18 05:29o-Xylene [95-47-6]^0.088 MRK8F280151.00.088 U 1
ug/L SM 6200B-1997 06/29/18 05:29sec-Butylbenzene [135-98-8]^0.053 MRK8F280151.00.053 U 1
ug/L SM 6200B-1997 06/29/18 05:29Styrene [100-42-5]^0.082 MRK8F280151.00.082 U 1
ug/L SM 6200B-1997 06/29/18 05:29tert-Butylbenzene [98-06-6]^0.094 MRK8F280151.00.094 U 1
ug/L SM 6200B-1997 06/29/18 05:29Tetrachloroethene [127-18-4]^0.099 MRK8F280151.00.099 U 1
ug/L SM 6200B-1997 06/29/18 05:29Toluene [108-88-3]^0.053 MRK8F280151.00.053 U 1
ug/L SM 6200B-1997 06/29/18 05:29trans-1,2-Dichloroethene [156-60-5]^0.11 MRK8F280151.00.11 U 1
ug/L SM 6200B-1997 06/29/18 05:29trans-1,3-Dichloropropene [10061-02-6]^0.080 MRK8F280151.00.080 U 1
ug/L SM 6200B-1997 06/29/18 05:29Trichloroethene [79-01-6]^0.13 MRK8F280151.00.13 U 1
ug/L SM 6200B-1997 06/29/18 05:29Trichlorofluoromethane [75-69-4]^0.15 MRK8F280151.00.15 U 1
ug/L SM 6200B-1997 06/29/18 05:29Vinyl chloride [75-01-4]^0.083 MRK8F280151.00.083 U 1
ug/L SM 6200B-1997 06/29/18 05:29Xylenes (Total) [1330-20-7]^0.22 MRK8F280151.00.22 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 70-13085 %MRKSM 6200B-1997 06/29/18 05:298F280154350.0 1
Dibromofluoromethane 70-13087 %MRKSM 6200B-1997 06/29/18 05:298F280154450.0 1
Toluene-d8 70-13082 %MRKSM 6200B-1997 06/29/18 05:298F280154150.0 1
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 625 06/26/18 23:132-Methylnaphthalene [91-57-6]^1.5 DFM8F25012101.5 U 1
ug/L EPA 625 06/26/18 23:13Acenaphthene [83-32-9]^1.4 DFM8F25012101.4 U 1
ug/L EPA 625 06/26/18 23:13Acenaphthylene [208-96-8]^1.2 DFM8F25012101.2 U 1
ug/L EPA 625 06/26/18 23:13Anthracene [120-12-7]^1.6 DFM8F25012101.6 U 1
ug/L EPA 625 06/26/18 23:13Benzo(a)anthracene [56-55-3]^1.3 DFM8F25012101.3 U 1
ug/L EPA 625 06/26/18 23:13Benzo(a)pyrene [50-32-8]^1.3 DFM8F25012101.3 U 1
ug/L EPA 625 06/26/18 23:13Benzo(b)fluoranthene [205-99-2]^1.0 DFM8F25012101.0 U 1
ug/L EPA 625 06/26/18 23:13Benzo(g,h,i)perylene [191-24-2]^2.4 DFM8F25012102.4 U 1
ug/L EPA 625 06/26/18 23:13Benzo(k)fluoranthene [207-08-9]^1.3 DFM8F25012101.3 U 1
ug/L EPA 625 06/26/18 23:13Chrysene [218-01-9]^2.0 DFM8F25012102.0 U 1
ug/L EPA 625 06/26/18 23:13Dibenzo(a,h)anthracene [53-70-3]^2.3 DFM8F25012102.3 U 1
ug/L EPA 625 06/26/18 23:13Fluoranthene [206-44-0]^2.1 DFM8F25012102.1 U 1
ug/L EPA 625 06/26/18 23:13Fluorene [86-73-7]^1.7 DFM8F25012101.7 U 1
ug/L EPA 625 06/26/18 23:13Indeno(1,2,3-cd)pyrene [193-39-5]^2.2 DFM8F25012102.2 U 1
ug/L EPA 625 06/26/18 23:13Naphthalene [91-20-3]^1.3 DFM8F25012101.3 U 1
ug/L EPA 625 06/26/18 23:13Phenanthrene [85-01-8]^1.4 DFM8F25012101.4 U 1
ug/L EPA 625 06/26/18 23:13Pyrene [129-00-0]^2.1 DFM8F25012102.1 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2-Fluorobiphenyl 15-13980 %DFMEPA 625 06/26/18 23:138F250124050.0 1
Nitrobenzene-d5 16-14074 %DFMEPA 625 06/26/18 23:138F250123750.0 1
Terphenyl-d14 23-16489 %DFMEPA 625 06/26/18 23:138F250124450.0 1
Page 7 of 28This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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ANALYTICAL RESULTS
Effluent 2nd Qtr 2018Description:Lab Sample ID:CB08873-02 06/22/18 13:40Received:
CB08873Work Order:06/22/18 12:06Sampled:Waste WaterMatrix:
James DodsonSampled By:Project:Dixie
Metals (acid extractable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 6010D 07/09/18 14:41Lead [7439-92-1]^3.10 JDH8F2203210.03.10 U 1
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/L SM 2540D-1997 06/26/18 07:44Total Suspended Solids^2.5 LBG8F260012.52.5 U 1
Classical Chemistry Parameters
^ - ENCO Orlando certified analyte [NC 424]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/L EPA 420.1 07/03/18 09:30Phenolics^0.034 DMM8G020160.0500.034 U 1
Classical Chemistry Parameters
^ - ENCO Jacksonville certified analyte [NC 442]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/L EPA 1664B 07/03/18 18:01Oil & Grease (HEM) [C-0007]^2.40 SMA8G020075.002.40 U 1
Page 8 of 28This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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ANALYTICAL RESULTS
Trip BlankDescription:Lab Sample ID:CB08873-03 06/22/18 13:40Received:
CB08873Work Order:06/22/18 11:49Sampled:WaterMatrix:
ENCOSampled By:Project:Dixie
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 06/29/18 05:591,1,1,2-Tetrachloroethane [630-20-6]^0.091 MRK8F280151.00.091 U 1
ug/L SM 6200B-1997 06/29/18 05:591,1,1-Trichloroethane [71-55-6]^0.15 MRK8F280151.00.15 U 1
ug/L SM 6200B-1997 06/29/18 05:591,1,2,2-Tetrachloroethane [79-34-5]^0.085 MRK8F280151.00.085 U 1
ug/L SM 6200B-1997 06/29/18 05:591,1,2-Trichloroethane [79-00-5]^0.068 MRK8F280151.00.068 U 1
ug/L SM 6200B-1997 06/29/18 05:591,1-Dichloroethane [75-34-3]^0.050 MRK8F280151.00.050 U 1
ug/L SM 6200B-1997 06/29/18 05:591,1-Dichloroethene [75-35-4]^0.15 MRK8F280151.00.15 U 1
ug/L SM 6200B-1997 06/29/18 05:591,1-Dichloropropene [563-58-6]^0.063 MRK8F280151.00.063 U 1
ug/L SM 6200B-1997 06/29/18 05:591,2,3-Trichlorobenzene [87-61-6]^0.25 MRK8F280151.00.25 U 1
ug/L SM 6200B-1997 06/29/18 05:591,2,3-Trichloropropane [96-18-4]^0.15 MRK8F280151.00.15 U 1
ug/L SM 6200B-1997 06/29/18 05:591,2,4-Trichlorobenzene [120-82-1]^0.097 MRK8F280151.00.097 U 1
ug/L SM 6200B-1997 06/29/18 05:591,2,4-Trimethylbenzene [95-63-6]^0.067 MRK8F280151.00.067 U 1
ug/L SM 6200B-1997 06/29/18 05:591,2-Dibromo-3-chloropropane [96-12-8]^0.48 MRK8F280151.00.48 U 1
ug/L SM 6200B-1997 06/29/18 05:591,2-Dibromoethane [106-93-4]^0.42 MRK8F280151.00.42 U 1
ug/L SM 6200B-1997 06/29/18 05:591,2-Dichlorobenzene [95-50-1]^0.052 MRK8F280151.00.052 U 1
ug/L SM 6200B-1997 06/29/18 05:591,2-Dichloroethane [107-06-2]^0.082 MRK8F280151.00.082 U 1
ug/L SM 6200B-1997 06/29/18 05:591,2-Dichloropropane [78-87-5]^0.098 MRK8F280151.00.098 U 1
ug/L SM 6200B-1997 06/29/18 05:591,3,5-Trimethylbenzene [108-67-8]^0.10 MRK8F280151.00.10 U 1
ug/L SM 6200B-1997 06/29/18 05:591,3-Dichlorobenzene [541-73-1]^0.092 MRK8F280151.00.092 U 1
ug/L SM 6200B-1997 06/29/18 05:591,3-Dichloropropane [142-28-9]^0.15 MRK8F280151.00.15 U 1
ug/L SM 6200B-1997 06/29/18 05:591,4-Dichlorobenzene [106-46-7]^0.10 MRK8F280151.00.10 U 1
ug/L SM 6200B-1997 06/29/18 05:592,2-Dichloropropane [594-20-7]^0.12 MRK8F280151.00.12 U 1
ug/L SM 6200B-1997 06/29/18 05:592-Chlorotoluene [95-49-8]^0.10 MRK8F280151.00.10 U 1
ug/L SM 6200B-1997 06/29/18 05:594-Chlorotoluene [106-43-4]^0.10 MRK8F280151.00.10 U 1
ug/L SM 6200B-1997 06/29/18 05:594-Isopropyltoluene [99-87-6]^0.066 MRK8F280151.00.066 U 1
ug/L SM 6200B-1997 06/29/18 05:59Benzene [71-43-2]^0.050 MRK8F280151.00.050 U 1
ug/L SM 6200B-1997 06/29/18 05:59Bromobenzene [108-86-1]^0.13 MRK8F280151.00.13 U 1
ug/L SM 6200B-1997 06/29/18 05:59Bromochloromethane [74-97-5]^0.11 MRK8F280151.00.11 U 1
ug/L SM 6200B-1997 06/29/18 05:59Bromodichloromethane [75-27-4]^0.10 MRK8F280151.00.10 U 1
ug/L SM 6200B-1997 06/29/18 05:59Bromoform [75-25-2]^0.20 MRK8F280151.00.20 U 1
ug/L SM 6200B-1997 06/29/18 05:59Bromomethane [74-83-9]^0.28 MRK8F280151.00.28 U 1
ug/L SM 6200B-1997 06/29/18 05:59Carbon Tetrachloride [56-23-5]^0.082 MRK8F280151.00.082 U 1
ug/L SM 6200B-1997 06/29/18 05:59Chlorobenzene [108-90-7]^0.069 MRK8F280151.00.069 U 1
ug/L SM 6200B-1997 06/29/18 05:59Chloroethane [75-00-3]^0.18 MRK8F280151.00.18 U 1
ug/L SM 6200B-1997 06/29/18 05:59Chloroform [67-66-3]^0.083 MRK8F280151.00.083 U 1
ug/L SM 6200B-1997 06/29/18 05:59Chloromethane [74-87-3]^0.050 MRK8F280151.00.050 U 1
ug/L SM 6200B-1997 06/29/18 05:59cis-1,2-Dichloroethene [156-59-2]^0.075 MRK8F280151.00.075 U 1
ug/L SM 6200B-1997 06/29/18 05:59cis-1,3-Dichloropropene [10061-01-5]^0.073 MRK8F280151.00.073 U 1
ug/L SM 6200B-1997 06/29/18 05:59Dibromochloromethane [124-48-1]^0.067 MRK8F280151.00.067 U 1
ug/L SM 6200B-1997 06/29/18 05:59Dibromomethane [74-95-3]^0.13 MRK8F280151.00.13 U 1
ug/L SM 6200B-1997 06/29/18 05:59Dichlorodifluoromethane [75-71-8]^0.091 MRK8F280151.00.091 U 1
ug/L SM 6200B-1997 06/29/18 05:59Ethylbenzene [100-41-4]^0.10 MRK8F280151.00.10 U 1
ug/L SM 6200B-1997 06/29/18 05:59Freon 113 [76-13-1]^0.35 MRK8F280151.00.35 U 1
ug/L SM 6200B-1997 06/29/18 05:59Hexachlorobutadiene [87-68-3]^0.15 MRK8F280151.00.15 U 1
ug/L SM 6200B-1997 06/29/18 05:59Isopropyl Ether [108-20-3]^0.21 MRK8F280151.00.21 U 1
ug/L SM 6200B-1997 06/29/18 05:59Isopropylbenzene [98-82-8]^0.13 MRK8F280151.00.13 U 1
ug/L SM 6200B-1997 06/29/18 05:59m,p-Xylenes [108-38-3/106-42-3]^0.18 MRK8F280152.00.18 U 1
ug/L SM 6200B-1997 06/29/18 05:59Methylene Chloride [75-09-2]^0.070 MRK8F280152.00.070 U 1
Page 9 of 28This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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ANALYTICAL RESULTS
Trip BlankDescription:Lab Sample ID:CB08873-03 06/22/18 13:40Received:
CB08873Work Order:06/22/18 11:49Sampled:WaterMatrix:
ENCOSampled By:Project:Dixie
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 06/29/18 05:59Methyl-tert-Butyl Ether [1634-04-4]^0.12 MRK8F280151.00.12 U 1
ug/L SM 6200B-1997 06/29/18 05:59Naphthalene [91-20-3]^0.086 MRK8F280151.00.086 U 1
ug/L SM 6200B-1997 06/29/18 05:59n-Butyl Benzene [104-51-8]^0.074 MRK8F280151.00.074 U 1
ug/L SM 6200B-1997 06/29/18 05:59n-Propyl Benzene [103-65-1]^0.073 MRK8F280151.00.073 U 1
ug/L SM 6200B-1997 06/29/18 05:59o-Xylene [95-47-6]^0.088 MRK8F280151.00.088 U 1
ug/L SM 6200B-1997 06/29/18 05:59sec-Butylbenzene [135-98-8]^0.053 MRK8F280151.00.053 U 1
ug/L SM 6200B-1997 06/29/18 05:59Styrene [100-42-5]^0.082 MRK8F280151.00.082 U 1
ug/L SM 6200B-1997 06/29/18 05:59tert-Butylbenzene [98-06-6]^0.094 MRK8F280151.00.094 U 1
ug/L SM 6200B-1997 06/29/18 05:59Tetrachloroethene [127-18-4]^0.099 MRK8F280151.00.099 U 1
ug/L SM 6200B-1997 06/29/18 05:59Toluene [108-88-3]^0.053 MRK8F280151.00.053 U 1
ug/L SM 6200B-1997 06/29/18 05:59trans-1,2-Dichloroethene [156-60-5]^0.11 MRK8F280151.00.11 U 1
ug/L SM 6200B-1997 06/29/18 05:59trans-1,3-Dichloropropene [10061-02-6]^0.080 MRK8F280151.00.080 U 1
ug/L SM 6200B-1997 06/29/18 05:59Trichloroethene [79-01-6]^0.13 MRK8F280151.00.13 U 1
ug/L SM 6200B-1997 06/29/18 05:59Trichlorofluoromethane [75-69-4]^0.15 MRK8F280151.00.15 U 1
ug/L SM 6200B-1997 06/29/18 05:59Vinyl chloride [75-01-4]^0.083 MRK8F280151.00.083 U 1
ug/L SM 6200B-1997 06/29/18 05:59Xylenes (Total) [1330-20-7]^0.22 MRK8F280151.00.22 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 70-13082 %MRKSM 6200B-1997 06/29/18 05:598F280154150.0 1
Dibromofluoromethane 70-13085 %MRKSM 6200B-1997 06/29/18 05:598F280154350.0 1
Toluene-d8 70-13081 %MRKSM 6200B-1997 06/29/18 05:598F280154150.0 1
Page 10 of 28This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 8F28015 - EPA 5030B_MS
Prepared: 06/28/2018 09:55 Analyzed: 06/28/2018 23:25Blank (8F28015-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.00.091 U 1,1,1,2-Tetrachloroethane
ug/L1.00.15 U 1,1,1-Trichloroethane
ug/L1.00.085 U 1,1,2,2-Tetrachloroethane
ug/L1.00.068 U 1,1,2-Trichloroethane
ug/L1.00.050 U 1,1-Dichloroethane
ug/L1.00.15 U 1,1-Dichloroethene
ug/L1.00.063 U 1,1-Dichloropropene
ug/L1.00.25 U 1,2,3-Trichlorobenzene
ug/L1.00.15 U 1,2,3-Trichloropropane
ug/L1.00.097 U 1,2,4-Trichlorobenzene
ug/L1.00.067 U 1,2,4-Trimethylbenzene
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.42 U 1,2-Dibromoethane
ug/L1.00.052 U 1,2-Dichlorobenzene
ug/L1.00.082 U 1,2-Dichloroethane
ug/L1.00.098 U 1,2-Dichloropropane
ug/L1.00.10 U 1,3,5-Trimethylbenzene
ug/L1.00.092 U 1,3-Dichlorobenzene
ug/L1.00.15 U 1,3-Dichloropropane
ug/L1.00.10 U 1,4-Dichlorobenzene
ug/L1.00.12 U 2,2-Dichloropropane
ug/L1.00.10 U 2-Chlorotoluene
ug/L1.00.10 U 4-Chlorotoluene
ug/L1.00.066 U 4-Isopropyltoluene
ug/L1.00.050 U Benzene
ug/L1.00.13 U Bromobenzene
ug/L1.00.11 U Bromochloromethane
ug/L1.00.10 U Bromodichloromethane
ug/L1.00.20 U Bromoform
ug/L1.00.28 U Bromomethane
ug/L1.00.082 U Carbon Tetrachloride
ug/L1.00.069 U Chlorobenzene
ug/L1.00.18 U Chloroethane
ug/L1.00.083 U Chloroform
ug/L1.00.050 U Chloromethane
ug/L1.00.075 U cis-1,2-Dichloroethene
ug/L1.00.073 U cis-1,3-Dichloropropene
ug/L1.00.067 U Dibromochloromethane
ug/L1.00.13 U Dibromomethane
ug/L1.00.091 U Dichlorodifluoromethane
ug/L1.00.10 U Ethylbenzene
ug/L1.00.35 U Freon 113
ug/L1.00.15 U Hexachlorobutadiene
ug/L1.00.21 U Isopropyl Ether
ug/L1.00.13 U Isopropylbenzene
ug/L2.00.18 U m,p-Xylenes
ug/L2.00.070 U Methylene Chloride
ug/L1.00.12 U Methyl-tert-Butyl Ether
ug/L1.00.086 U Naphthalene
Page 11 of 28This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 8F28015 - EPA 5030B_MS - Continued
Prepared: 06/28/2018 09:55 Analyzed: 06/28/2018 23:25Blank (8F28015-BLK1) Continued
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.00.074 U n-Butyl Benzene
ug/L1.00.073 U n-Propyl Benzene
ug/L1.00.088 U o-Xylene
ug/L1.00.053 U sec-Butylbenzene
ug/L1.00.082 U Styrene
ug/L1.00.094 U tert-Butylbenzene
ug/L1.00.099 U Tetrachloroethene
ug/L1.00.053 U Toluene
ug/L1.00.11 U trans-1,2-Dichloroethene
ug/L1.00.080 U trans-1,3-Dichloropropene
ug/L1.00.13 U Trichloroethene
ug/L1.00.15 U Trichlorofluoromethane
ug/L1.00.083 U Vinyl chloride
ug/L1.00.22 U Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 8341
ug/L 50.0 70-130Dibromofluoromethane8542
ug/L 50.0 70-130Toluene-d8 8341
Prepared: 06/28/2018 09:55 Analyzed: 06/28/2018 21:24LCS (8F28015-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 70-13011623 1,1,1,2-Tetrachloroethane
ug/L1.0 20.0 70-13012325 1,1,1-Trichloroethane
ug/L1.0 20.0 70-13010020 1,1,2,2-Tetrachloroethane
ug/L1.0 20.0 70-13010020 1,1,2-Trichloroethane
ug/L1.0 20.0 70-13011323 1,1-Dichloroethane
ug/L1.0 20.0 70-13010721 1,1-Dichloroethene
ug/L1.0 20.0 70-13010220 1,1-Dichloropropene
ug/L1.0 20.0 70-13010521 1,2,3-Trichlorobenzene
ug/L1.0 20.0 70-13010621 1,2,3-Trichloropropane
ug/L1.0 20.0 70-13010020 1,2,4-Trichlorobenzene
ug/L1.0 20.0 70-13011122 1,2,4-Trimethylbenzene
ug/L1.0 20.0 70-13010721 1,2-Dibromo-3-chloropropane
ug/L1.0 20.0 70-13010421 1,2-Dibromoethane
ug/L1.0 20.0 70-13010621 1,2-Dichlorobenzene
ug/L1.0 20.0 70-13012425 1,2-Dichloroethane
ug/L1.0 20.0 70-1309820 1,2-Dichloropropane
ug/L1.0 20.0 70-13010922 1,3,5-Trimethylbenzene
ug/L1.0 20.0 70-13010521 1,3-Dichlorobenzene
ug/L1.0 20.0 70-1309619 1,3-Dichloropropane
ug/L1.0 20.0 70-13010621 1,4-Dichlorobenzene
ug/L1.0 20.0 70-1309820 2,2-Dichloropropane
ug/L1.0 20.0 70-13011022 2-Chlorotoluene
ug/L1.0 20.0 70-13010621 4-Chlorotoluene
ug/L1.0 20.0 70-13010621 4-Isopropyltoluene
ug/L1.0 20.0 70-13010120 Benzene
ug/L1.0 20.0 70-13010020 Bromobenzene
ug/L1.0 20.0 70-13011423 Bromochloromethane
ug/L1.0 20.0 70-13013026 Bromodichloromethane
Page 12 of 28This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 8F28015 - EPA 5030B_MS - Continued
Prepared: 06/28/2018 09:55 Analyzed: 06/28/2018 21:24LCS (8F28015-BS1) Continued
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 70-13010621 Bromoform
ug/L1.0 20.0 60-14010120 Bromomethane
ug/L1.0 20.0 70-13012625 Carbon Tetrachloride
ug/L1.0 20.0 70-13010220 Chlorobenzene
ug/L1.0 20.0 60-14011423 Chloroethane
ug/L1.0 20.0 70-13011122 Chloroform
ug/L1.0 20.0 60-14010220 Chloromethane
ug/L1.0 20.0 70-1309820 cis-1,2-Dichloroethene
ug/L1.0 20.0 70-13010621 cis-1,3-Dichloropropene
ug/L1.0 20.0 70-13011022 Dibromochloromethane
ug/L1.0 20.0 70-13011323 Dibromomethane
ug/L1.0 20.0 60-14012425 Dichlorodifluoromethane
ug/L1.0 20.0 70-1309118 Ethylbenzene
ug/L1.0 20.0 70-1309419 Freon 113
ug/L1.0 20.0 70-13011323 Hexachlorobutadiene
ug/L1.0 20.0 70-1309419 Isopropyl Ether
ug/L1.0 20.0 70-13010521 Isopropylbenzene
ug/L2.0 40.0 70-1309839 m,p-Xylenes
ug/L2.0 20.0 70-1309519 Methylene Chloride
ug/L1.0 20.0 70-13010521 Methyl-tert-Butyl Ether
ug/L1.0 20.0 70-13010421 Naphthalene
ug/L1.0 20.0 70-13010521 n-Butyl Benzene
ug/L1.0 20.0 70-1309319 n-Propyl Benzene
ug/L1.0 20.0 70-13010120 o-Xylene
ug/L1.0 20.0 70-13010621 sec-Butylbenzene
ug/L1.0 20.0 70-13010020 Styrene
ug/L1.0 20.0 70-13010421 tert-Butylbenzene
ug/L1.0 20.0 70-13010020 Tetrachloroethene
ug/L1.0 20.0 70-1309218 Toluene
ug/L1.0 20.0 70-13010421 trans-1,2-Dichloroethene
ug/L1.0 20.0 70-13011323 trans-1,3-Dichloropropene
ug/L1.0 20.0 70-13010721 Trichloroethene
ug/L1.0 20.0 60-14012525 Trichlorofluoromethane
ug/L1.0 20.0 60-14011022 Vinyl chloride
ug/L1.0 60.0 70-1309959 Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 7940
ug/L 50.0 70-130Dibromofluoromethane8341
ug/L 50.0 70-130Toluene-d8 8341
Prepared: 06/28/2018 09:55 Analyzed: 06/28/2018 21:54Matrix Spike (8F28015-MS1)
Source: CB08046-04
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 71-1171100.091 U22 1,1,1,2-Tetrachloroethane
ug/L1.0 20.0 72-1431250.15 U25 1,1,1-Trichloroethane
ug/L1.0 20.0 59-1331020.085 U20 1,1,2,2-Tetrachloroethane
ug/L1.0 20.0 67-118960.068 U19 1,1,2-Trichloroethane
ug/L1.0 20.0 79-1411070.050 U21 1,1-Dichloroethane
ug/L1.0 20.0 75-1331120.15 U22 1,1-Dichloroethene
ug/L1.0 20.0 70-1291070.063 U21 1,1-Dichloropropene
Page 13 of 28This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 8F28015 - EPA 5030B_MS - Continued
Prepared: 06/28/2018 09:55 Analyzed: 06/28/2018 21:54Matrix Spike (8F28015-MS1) Continued
Source: CB08046-04
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 62-117970.25 U19 1,2,3-Trichlorobenzene
ug/L1.0 20.0 58-1401090.15 U22 1,2,3-Trichloropropane
ug/L1.0 20.0 59-122950.097 U19 1,2,4-Trichlorobenzene
ug/L1.0 20.0 74-1231080.067 U22 1,2,4-Trimethylbenzene
ug/L1.0 20.0 37-1571120.48 U22 1,2-Dibromo-3-chloropropane
ug/L1.0 20.0 66-1231020.42 U20 1,2-Dibromoethane
ug/L1.0 20.0 76-1161000.052 U20 1,2-Dichlorobenzene
ug/L1.0 20.0 72-1511190.082 U24 1,2-Dichloroethane
ug/L1.0 20.0 78-125940.098 U19 1,2-Dichloropropane
ug/L1.0 20.0 77-1291060.10 U21 1,3,5-Trimethylbenzene
ug/L1.0 20.0 76-1191030.092 U21 1,3-Dichlorobenzene
ug/L1.0 20.0 60-129940.15 U19 1,3-Dichloropropane
ug/L1.0 20.0 76-1221020.10 U20 1,4-Dichlorobenzene
ug/L1.0 20.0 21-1671010.12 U20 2,2-Dichloropropane
ug/L1.0 20.0 73-1351060.10 U21 2-Chlorotoluene
ug/L1.0 20.0 76-1341040.10 U21 4-Chlorotoluene
ug/L1.0 20.0 75-1271050.066 U21 4-Isopropyltoluene
ug/L1.0 20.0 81-134970.050 U19 Benzene
ug/L1.0 20.0 72-115940.13 U19 Bromobenzene
ug/L1.0 20.0 74-1281090.11 U22 Bromochloromethane
ug/L1.0 20.0 72-1291250.10 U25 Bromodichloromethane
ug/L1.0 20.0 73-1191070.20 U21 Bromoform
ug/L1.0 20.0 38-189960.28 U19 Bromomethane
ug/L1.0 20.0 68-1421370.082 U27 Carbon Tetrachloride
ug/L1.0 20.0 83-117990.069 U20 Chlorobenzene
ug/L1.0 20.0 45-2131120.18 U22 Chloroethane
ug/L1.0 20.0 78-1381050.083 U21 Chloroform
ug/L1.0 20.0 56-171960.050 U19 Chloromethane
ug/L1.0 20.0 69-120910.075 U18 cis-1,2-Dichloroethene
ug/L1.0 20.0 63-1251000.073 U20 cis-1,3-Dichloropropene
ug/L1.0 20.0 73-1171060.067 U21 Dibromochloromethane
ug/L1.0 20.0 76-1241110.13 U22 Dibromomethane
ug/L1.0 20.0 25-1611530.091 U31 Dichlorodifluoromethane
ug/L1.0 20.0 68-124890.10 U18 Ethylbenzene
ug/L1.0 20.0 0-2001150.35 U23 Freon 113
ug/L1.0 20.0 63-1141030.15 U21 Hexachlorobutadiene
ug/L1.0 20.0 70-130910.21 U18 Isopropyl Ether
ug/L1.0 20.0 81-1361060.13 U21 Isopropylbenzene
ug/L2.0 40.0 79-121960.18 U38 m,p-Xylenes
ug/L2.0 20.0 68-128910.070 U18 Methylene Chloride
ug/L1.0 20.0 10-1271010.12 U20 Methyl-tert-Butyl Ether
ug/L1.0 20.0 50-1271000.086 U20 Naphthalene
ug/L1.0 20.0 68-1261000.074 U20 n-Butyl Benzene
ug/L1.0 20.0 76-125930.073 U19 n-Propyl Benzene
ug/L1.0 20.0 71-125980.088 U20 o-Xylene
ug/L1.0 20.0 75-1221050.053 U21 sec-Butylbenzene
ug/L1.0 20.0 73-120970.082 U19 Styrene
ug/L1.0 20.0 70-1371030.094 U21 tert-Butylbenzene
ug/L1.0 20.0 40-1811020.099 U20 Tetrachloroethene
Page 14 of 28This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 8F28015 - EPA 5030B_MS - Continued
Prepared: 06/28/2018 09:55 Analyzed: 06/28/2018 21:54Matrix Spike (8F28015-MS1) Continued
Source: CB08046-04
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 71-118920.053 U18 Toluene
ug/L1.0 20.0 75-1391010.11 U20 trans-1,2-Dichloroethene
ug/L1.0 20.0 62-1521090.080 U22 trans-1,3-Dichloropropene
ug/L1.0 20.0 75-1151120.13 U22 Trichloroethene
ug/L1.0 20.0 68-1831410.15 U28 Trichlorofluoromethane
ug/L1.0 20.0 49-1501130.083 U23 Vinyl chloride
ug/L1.0 60.0 77-121970.22 U58 Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 8040
ug/L 50.0 70-130Dibromofluoromethane8141
ug/L 50.0 70-130Toluene-d8 8241
Prepared: 06/28/2018 09:55 Analyzed: 06/28/2018 22:24Matrix Spike Dup (8F28015-MSD1)
Source: CB08046-04
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 1671-117108 20.091 U22 1,1,1,2-Tetrachloroethane
ug/L1.0 20.0 1872-143120 40.15 U24 1,1,1-Trichloroethane
ug/L1.0 20.0 1659-13395 70.085 U19 1,1,2,2-Tetrachloroethane
ug/L1.0 20.0 1867-11895 20.068 U19 1,1,2-Trichloroethane
ug/L1.0 20.0 1979-141106 0.70.050 U21 1,1-Dichloroethane
ug/L1.0 20.0 2075-133111 10.15 U22 1,1-Dichloroethene
ug/L1.0 20.0 1770-129106 10.063 U21 1,1-Dichloropropene
ug/L1.0 20.0 1762-11795 20.25 U19 1,2,3-Trichlorobenzene
ug/L1.0 20.0 1758-14099 100.15 U20 1,2,3-Trichloropropane
ug/L1.0 20.0 1759-12294 10.097 U19 1,2,4-Trichlorobenzene
ug/L1.0 20.0 1874-123105 30.067 U21 1,2,4-Trimethylbenzene
ug/L1.0 20.0 1837-157108 30.48 U22 1,2-Dibromo-3-chloropropane
ug/L1.0 20.0 1566-12398 40.42 U20 1,2-Dibromoethane
ug/L1.0 20.0 1676-11698 30.052 U20 1,2-Dichlorobenzene
ug/L1.0 20.0 1672-151118 10.082 U24 1,2-Dichloroethane
ug/L1.0 20.0 1978-12593 20.098 U19 1,2-Dichloropropane
ug/L1.0 20.0 1677-129102 40.10 U20 1,3,5-Trimethylbenzene
ug/L1.0 20.0 1776-119100 30.092 U20 1,3-Dichlorobenzene
ug/L1.0 20.0 1660-12991 30.15 U18 1,3-Dichloropropane
ug/L1.0 20.0 1676-122100 10.10 U20 1,4-Dichlorobenzene
ug/L1.0 20.0 2021-16796 40.12 U19 2,2-Dichloropropane
ug/L1.0 20.0 1673-135103 30.10 U21 2-Chlorotoluene
ug/L1.0 20.0 1676-134101 30.10 U20 4-Chlorotoluene
ug/L1.0 20.0 1775-127100 60.066 U20 4-Isopropyltoluene
ug/L1.0 20.0 1781-13494 30.050 U19 Benzene
ug/L1.0 20.0 1772-11591 20.13 U18 Bromobenzene
ug/L1.0 20.0 1874-128108 10.11 U22 Bromochloromethane
ug/L1.0 20.0 1672-129121 30.10 U24 Bromodichloromethane
ug/L1.0 20.0 4473-119106 0.80.20 U21 Bromoform
ug/L1.0 20.0 2738-18999 30.28 U20 Bromomethane
ug/L1.0 20.0 1768-142128 60.082 U26 Carbon Tetrachloride
ug/L1.0 20.0 1683-11795 40.069 U19 Chlorobenzene
ug/L1.0 20.0 2645-213108 40.18 U22 Chloroethane
ug/L1.0 20.0 1778-138102 30.083 U20 Chloroform
ug/L1.0 20.0 2856-17192 40.050 U18 Chloromethane
Page 15 of 28This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 8F28015 - EPA 5030B_MS - Continued
Prepared: 06/28/2018 09:55 Analyzed: 06/28/2018 22:24Matrix Spike Dup (8F28015-MSD1) Continued
Source: CB08046-04
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 1869-12092 10.075 U18 cis-1,2-Dichloroethene
ug/L1.0 20.0 1763-12597 30.073 U19 cis-1,3-Dichloropropene
ug/L1.0 20.0 1673-117102 40.067 U20 Dibromochloromethane
ug/L1.0 20.0 1576-124110 0.70.13 U22 Dibromomethane
ug/L1.0 20.0 4825-161145 50.091 U29 Dichlorodifluoromethane
ug/L1.0 20.0 1668-12486 40.10 U17 Ethylbenzene
ug/L1.0 20.0 250-200108 60.35 U22 Freon 113
ug/L1.0 20.0 1963-114101 20.15 U20 Hexachlorobutadiene
ug/L1.0 20.0 3070-13089 20.21 U18 Isopropyl Ether
ug/L1.0 20.0 1681-136100 60.13 U20 Isopropylbenzene
ug/L2.0 40.0 1679-12192 40.18 U37 m,p-Xylenes
ug/L2.0 20.0 1768-12889 20.070 U18 Methylene Chloride
ug/L1.0 20.0 2110-127101 0.80.12 U20 Methyl-tert-Butyl Ether
ug/L1.0 20.0 1950-12798 20.086 U20 Naphthalene
ug/L1.0 20.0 1568-12697 30.074 U19 n-Butyl Benzene
ug/L1.0 20.0 1676-12589 40.073 U18 n-Propyl Benzene
ug/L1.0 20.0 1571-12594 50.088 U19 o-Xylene
ug/L1.0 20.0 1775-122102 30.053 U20 sec-Butylbenzene
ug/L1.0 20.0 2373-12091 70.082 U18 Styrene
ug/L1.0 20.0 2270-13798 40.094 U20 tert-Butylbenzene
ug/L1.0 20.0 2640-18197 40.099 U19 Tetrachloroethene
ug/L1.0 20.0 1771-11888 40.053 U18 Toluene
ug/L1.0 20.0 1975-13998 30.11 U20 trans-1,2-Dichloroethene
ug/L1.0 20.0 1662-152106 30.080 U21 trans-1,3-Dichloropropene
ug/L1.0 20.0 1875-115105 60.13 U21 Trichloroethene
ug/L1.0 20.0 2268-183136 30.15 U27 Trichlorofluoromethane
ug/L1.0 20.0 2749-150108 40.083 U22 Vinyl chloride
ug/L1.0 60.0 1677-12193 40.22 U56 Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 7839
ug/L 50.0 70-130Dibromofluoromethane8241
ug/L 50.0 70-130Toluene-d8 8141
Batch 8F29023 - EPA 5030B_MS
Prepared: 07/03/2018 11:59 Analyzed: 07/05/2018 12:49Blank (8F29023-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.00.091 U 1,1,1,2-Tetrachloroethane
ug/L1.00.15 U 1,1,1-Trichloroethane
ug/L1.00.085 U 1,1,2,2-Tetrachloroethane
ug/L1.00.068 U 1,1,2-Trichloroethane
ug/L1.00.050 U 1,1-Dichloroethane
ug/L1.00.15 U 1,1-Dichloroethene
ug/L1.00.063 U 1,1-Dichloropropene
ug/L1.00.25 U 1,2,3-Trichlorobenzene
ug/L1.00.15 U 1,2,3-Trichloropropane
ug/L1.00.097 U 1,2,4-Trichlorobenzene
ug/L1.00.067 U 1,2,4-Trimethylbenzene
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
Page 16 of 28This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 8F29023 - EPA 5030B_MS - Continued
Prepared: 07/03/2018 11:59 Analyzed: 07/05/2018 12:49Blank (8F29023-BLK1) Continued
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.00.42 U 1,2-Dibromoethane
ug/L1.00.052 U 1,2-Dichlorobenzene
ug/L1.00.082 U 1,2-Dichloroethane
ug/L1.00.098 U 1,2-Dichloropropane
ug/L1.00.10 U 1,3,5-Trimethylbenzene
ug/L1.00.092 U 1,3-Dichlorobenzene
ug/L1.00.15 U 1,3-Dichloropropane
ug/L1.00.10 U 1,4-Dichlorobenzene
ug/L1.00.12 U 2,2-Dichloropropane
ug/L1.00.10 U 2-Chlorotoluene
ug/L1.00.10 U 4-Chlorotoluene
ug/L1.00.066 U 4-Isopropyltoluene
ug/L1.00.050 U Benzene
ug/L1.00.13 U Bromobenzene
ug/L1.00.11 U Bromochloromethane
ug/L1.00.10 U Bromodichloromethane
ug/L1.00.20 U Bromoform
ug/L1.00.28 U Bromomethane
ug/L1.00.082 U Carbon Tetrachloride
ug/L1.00.069 U Chlorobenzene
ug/L1.00.18 U Chloroethane
ug/L1.00.083 U Chloroform
ug/L1.00.050 U Chloromethane
ug/L1.00.075 U cis-1,2-Dichloroethene
ug/L1.00.073 U cis-1,3-Dichloropropene
ug/L1.00.067 U Dibromochloromethane
ug/L1.00.13 U Dibromomethane
ug/L1.00.091 U Dichlorodifluoromethane
ug/L1.00.10 U Ethylbenzene
ug/L1.00.35 U Freon 113
ug/L1.00.15 U Hexachlorobutadiene
ug/L1.00.21 U Isopropyl Ether
ug/L1.00.13 U Isopropylbenzene
ug/L2.00.18 U m,p-Xylenes
ug/L2.00.070 U Methylene Chloride
ug/L1.00.12 U Methyl-tert-Butyl Ether
ug/L1.00.086 U Naphthalene
ug/L1.00.074 U n-Butyl Benzene
ug/L1.00.073 U n-Propyl Benzene
ug/L1.00.088 U o-Xylene
ug/L1.00.053 U sec-Butylbenzene
ug/L1.00.082 U Styrene
ug/L1.00.094 U tert-Butylbenzene
ug/L1.00.099 U Tetrachloroethene
ug/L1.00.053 U Toluene
ug/L1.00.11 U trans-1,2-Dichloroethene
ug/L1.00.080 U trans-1,3-Dichloropropene
ug/L1.00.13 U Trichloroethene
ug/L1.00.15 U Trichlorofluoromethane
Page 17 of 28This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 8F29023 - EPA 5030B_MS - Continued
Prepared: 07/03/2018 11:59 Analyzed: 07/05/2018 12:49Blank (8F29023-BLK1) Continued
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.00.083 U Vinyl chloride
ug/L1.00.22 U Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 8643
ug/L 50.0 70-130Dibromofluoromethane7437
ug/L 50.0 70-130Toluene-d8 7738
Prepared: 07/03/2018 11:59 Analyzed: 07/05/2018 11:49LCS (8F29023-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 70-13010120 1,1,1,2-Tetrachloroethane
ug/L1.0 20.0 70-1309719 1,1,1-Trichloroethane
ug/L1.0 20.0 70-1309419 1,1,2,2-Tetrachloroethane
ug/L1.0 20.0 70-1309519 1,1,2-Trichloroethane
ug/L1.0 20.0 70-1309719 1,1-Dichloroethane
ug/L1.0 20.0 70-1309118 1,1-Dichloroethene
ug/L1.0 20.0 70-1309619 1,1-Dichloropropene
ug/L1.0 20.0 70-13010521 1,2,3-Trichlorobenzene
ug/L1.0 20.0 70-1309619 1,2,3-Trichloropropane
ug/L1.0 20.0 70-13010721 1,2,4-Trichlorobenzene
ug/L1.0 20.0 70-13010321 1,2,4-Trimethylbenzene
ug/L1.0 20.0 70-1309218 1,2-Dibromo-3-chloropropane
ug/L1.0 20.0 70-13010020 1,2-Dibromoethane
ug/L1.0 20.0 70-13010220 1,2-Dichlorobenzene
ug/L1.0 20.0 70-13010220 1,2-Dichloroethane
ug/L1.0 20.0 70-1309619 1,2-Dichloropropane
ug/L1.0 20.0 70-13010020 1,3,5-Trimethylbenzene
ug/L1.0 20.0 70-13010521 1,3-Dichlorobenzene
ug/L1.0 20.0 70-1309018 1,3-Dichloropropane
ug/L1.0 20.0 70-13010120 1,4-Dichlorobenzene
ug/L1.0 20.0 70-1309920 2,2-Dichloropropane
ug/L1.0 20.0 70-13010020 2-Chlorotoluene
ug/L1.0 20.0 70-1309820 4-Chlorotoluene
ug/L1.0 20.0 70-13010120 4-Isopropyltoluene
ug/L1.0 20.0 70-1309619 Benzene
ug/L1.0 20.0 70-1309920 Bromobenzene
ug/L1.0 20.0 70-13011022 Bromochloromethane
ug/L1.0 20.0 70-13011022 Bromodichloromethane
ug/L1.0 20.0 70-13010321 Bromoform
ug/L1.0 20.0 60-1407114 Bromomethane
ug/L1.0 20.0 70-13010120 Carbon Tetrachloride
ug/L1.0 20.0 70-1309519 Chlorobenzene
ug/L1.0 20.0 60-1408216 Chloroethane
ug/L1.0 20.0 70-1308918 Chloroform
ug/L1.0 20.0 60-1409018 Chloromethane
ug/L1.0 20.0 70-1309619 cis-1,2-Dichloroethene
ug/L1.0 20.0 70-13010421 cis-1,3-Dichloropropene
ug/L1.0 20.0 70-1309719 Dibromochloromethane
ug/L1.0 20.0 70-13010721 Dibromomethane
ug/L1.0 20.0 60-1409820 Dichlorodifluoromethane
Page 18 of 28This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 8F29023 - EPA 5030B_MS - Continued
Prepared: 07/03/2018 11:59 Analyzed: 07/05/2018 11:49LCS (8F29023-BS1) Continued
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 70-1308617 Ethylbenzene
ug/L1.0 20.0 70-1308818 Freon 113
ug/L1.0 20.0 70-13012525 Hexachlorobutadiene
ug/L1.0 20.0 70-1308918 Isopropyl Ether
ug/L1.0 20.0 70-13010220 Isopropylbenzene
ug/L2.0 40.0 70-1308936 m,p-Xylenes
ug/L2.0 20.0 70-1308216 Methylene Chloride
ug/L1.0 20.0 70-1309719 Methyl-tert-Butyl Ether
ug/L1.0 20.0 70-13010220 Naphthalene
ug/L1.0 20.0 70-1309619 n-Butyl Benzene
ug/L1.0 20.0 70-1308617 n-Propyl Benzene
ug/L1.0 20.0 70-1309519 o-Xylene
ug/L1.0 20.0 70-13010120 sec-Butylbenzene
ug/L1.0 20.0 70-1309820 Styrene
ug/L1.0 20.0 70-13010020 tert-Butylbenzene
ug/L1.0 20.0 70-13010220 Tetrachloroethene
ug/L1.0 20.0 70-1308918 Toluene
ug/L1.0 20.0 70-1309218 trans-1,2-Dichloroethene
ug/L1.0 20.0 70-13010020 trans-1,3-Dichloropropene
ug/L1.0 20.0 70-13010822 Trichloroethene
ug/L1.0 20.0 60-1408216 Trichlorofluoromethane
ug/L1.0 20.0 60-1408417 Vinyl chloride
ug/L1.0 60.0 70-1309155 Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 8241
ug/L 50.0 70-130Dibromofluoromethane7136
ug/L 50.0 70-130Toluene-d8 7939
Prepared: 07/03/2018 11:59 Analyzed: 07/05/2018 10:16Matrix Spike (8F29023-MS1)
Source: CB10060-03
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 71-1171040.091 U21 1,1,1,2-Tetrachloroethane
ug/L1.0 20.0 72-1431020.15 U20 1,1,1-Trichloroethane
ug/L1.0 20.0 59-133950.085 U19 1,1,2,2-Tetrachloroethane
ug/L1.0 20.0 67-118950.068 U19 1,1,2-Trichloroethane
ug/L1.0 20.0 79-1411010.050 U20 1,1-Dichloroethane
ug/L1.0 20.0 75-133960.15 U19 1,1-Dichloroethene
ug/L1.0 20.0 70-129990.063 U20 1,1-Dichloropropene
ug/L1.0 20.0 62-1171020.4321 1,2,3-Trichlorobenzene
ug/L1.0 20.0 58-140970.15 U19 1,2,3-Trichloropropane
ug/L1.0 20.0 59-1221000.097 U20 1,2,4-Trichlorobenzene
ug/L1.0 20.0 74-1231010.067 U20 1,2,4-Trimethylbenzene
ug/L1.0 20.0 37-157950.48 U19 1,2-Dibromo-3-chloropropane
ug/L1.0 20.0 66-123990.42 U20 1,2-Dibromoethane
ug/L1.0 20.0 76-116990.052 U20 1,2-Dichlorobenzene
ug/L1.0 20.0 72-1511010.082 U20 1,2-Dichloroethane
ug/L1.0 20.0 78-125960.098 U19 1,2-Dichloropropane
ug/L1.0 20.0 77-129990.10 U20 1,3,5-Trimethylbenzene
ug/L1.0 20.0 76-1191010.092 U20 1,3-Dichlorobenzene
ug/L1.0 20.0 60-129900.15 U18 1,3-Dichloropropane
Page 19 of 28This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 8F29023 - EPA 5030B_MS - Continued
Prepared: 07/03/2018 11:59 Analyzed: 07/05/2018 10:16Matrix Spike (8F29023-MS1) Continued
Source: CB10060-03
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 76-122970.10 U19 1,4-Dichlorobenzene
ug/L1.0 20.0 21-167340.12 U6.8 2,2-Dichloropropane
ug/L1.0 20.0 73-135980.10 U20 2-Chlorotoluene
ug/L1.0 20.0 76-134970.10 U19 4-Chlorotoluene
ug/L1.0 20.0 75-127980.066 U20 4-Isopropyltoluene
ug/L1.0 20.0 81-134980.050 U20 Benzene
ug/L1.0 20.0 72-1151000.13 U20 Bromobenzene
ug/L1.0 20.0 74-1281090.11 U22 Bromochloromethane
ug/L1.0 20.0 72-1291120.10 U22 Bromodichloromethane
ug/L1.0 20.0 73-1191040.20 U21 Bromoform
ug/L1.0 20.0 38-189680.28 U14 Bromomethane
ug/L1.0 20.0 68-1421100.082 U22 Carbon Tetrachloride
ug/L1.0 20.0 83-117960.069 U19 Chlorobenzene
ug/L1.0 20.0 45-213880.18 U18 Chloroethane
ug/L1.0 20.0 78-138950.083 U19 Chloroform
ug/L1.0 20.0 56-171940.050 U19 Chloromethane
ug/L1.0 20.0 69-120980.075 U20 cis-1,2-Dichloroethene
ug/L1.0 20.0 63-125890.073 U18 cis-1,3-Dichloropropene
ug/L1.0 20.0 73-1171010.067 U20 Dibromochloromethane
ug/L1.0 20.0 76-1241050.13 U21 Dibromomethane
ug/L1.0 20.0 25-1611000.091 U20 Dichlorodifluoromethane
ug/L1.0 20.0 68-124880.10 U18 Ethylbenzene
ug/L1.0 20.0 0-200980.35 U20 Freon 113
ug/L1.0 20.0 63-1141111.123 Hexachlorobutadiene
ug/L1.0 20.0 70-130900.21 U18 Isopropyl Ether
ug/L1.0 20.0 81-1361040.13 U21 Isopropylbenzene
ug/L2.0 40.0 79-121900.18 U36 m,p-Xylenes
ug/L2.0 20.0 68-128840.070 U17 Methylene Chloride
ug/L1.0 20.0 10-127960.12 U19 Methyl-tert-Butyl Ether
ug/L1.0 20.0 50-1271010.4221 Naphthalene
ug/L1.0 20.0 68-126890.074 U18 n-Butyl Benzene
ug/L1.0 20.0 76-125860.073 U17 n-Propyl Benzene
ug/L1.0 20.0 71-125970.088 U19 o-Xylene
ug/L1.0 20.0 75-1221000.053 U20 sec-Butylbenzene
ug/L1.0 20.0 73-120990.082 U20 Styrene
ug/L1.0 20.0 70-1371020.094 U20 tert-Butylbenzene
ug/L1.0 20.0 40-1811070.099 U21 Tetrachloroethene
ug/L1.0 20.0 71-118900.053 U18 Toluene
ug/L1.0 20.0 75-139980.11 U20 trans-1,2-Dichloroethene
ug/L1.0 20.0 62-152860.080 U17 trans-1,3-Dichloropropene
ug/L1.0 20.0 75-1151100.13 U22 Trichloroethene
ug/L1.0 20.0 68-183900.15 U18 Trichlorofluoromethane
ug/L1.0 20.0 49-150900.083 U18 Vinyl chloride
ug/L1.0 60.0 77-121930.22 U56 Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 8342
ug/L 50.0 70-130Dibromofluoromethane7336
ug/L 50.0 70-130Toluene-d8 7939
Page 20 of 28This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 8F29023 - EPA 5030B_MS - Continued
Prepared: 07/03/2018 11:59 Analyzed: 07/05/2018 11:16Matrix Spike Dup (8F29023-MSD1)
Source: CB10060-03
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 1671-117100 40.091 U20 1,1,1,2-Tetrachloroethane
ug/L1.0 20.0 1872-14399 30.15 U20 1,1,1-Trichloroethane
ug/L1.0 20.0 1659-13395 0.60.085 U19 1,1,2,2-Tetrachloroethane
ug/L1.0 20.0 1867-11893 20.068 U19 1,1,2-Trichloroethane
ug/L1.0 20.0 1979-14194 70.050 U19 1,1-Dichloroethane
ug/L1.0 20.0 2075-13393 30.15 U19 1,1-Dichloroethene
ug/L1.0 20.0 1770-12998 0.70.063 U20 1,1-Dichloropropene
ug/L1.0 20.0 1762-117102 0.30.4321 1,2,3-Trichlorobenzene
ug/L1.0 20.0 1758-14096 10.15 U19 1,2,3-Trichloropropane
ug/L1.0 20.0 1759-122102 20.097 U20 1,2,4-Trichlorobenzene
ug/L1.0 20.0 1874-12396 60.067 U19 1,2,4-Trimethylbenzene
ug/L1.0 20.0 1837-15792 20.48 U18 1,2-Dibromo-3-chloropropane
ug/L1.0 20.0 1566-12398 0.40.42 U20 1,2-Dibromoethane
ug/L1.0 20.0 1676-11698 0.70.052 U20 1,2-Dichlorobenzene
ug/L1.0 20.0 1672-15193 80.082 U19 1,2-Dichloroethane
ug/L1.0 20.0 1978-12592 40.098 U18 1,2-Dichloropropane
ug/L1.0 20.0 1677-12994 50.10 U19 1,3,5-Trimethylbenzene
ug/L1.0 20.0 1776-11998 20.092 U20 1,3-Dichlorobenzene
ug/L1.0 20.0 1660-12987 40.15 U17 1,3-Dichloropropane
ug/L1.0 20.0 1676-12295 20.10 U19 1,4-Dichlorobenzene
ug/L1.0 20.0 2021-16744 260.12 U8.9 QM-072,2-Dichloropropane
ug/L1.0 20.0 1673-13593 50.10 U19 2-Chlorotoluene
ug/L1.0 20.0 1676-13492 50.10 U18 4-Chlorotoluene
ug/L1.0 20.0 1775-12796 20.066 U19 4-Isopropyltoluene
ug/L1.0 20.0 1781-13492 60.050 U18 Benzene
ug/L1.0 20.0 1772-11595 50.13 U19 Bromobenzene
ug/L1.0 20.0 1874-128104 50.11 U21 Bromochloromethane
ug/L1.0 20.0 1672-129105 60.10 U21 Bromodichloromethane
ug/L1.0 20.0 4473-119102 30.20 U20 Bromoform
ug/L1.0 20.0 2738-18965 40.28 U13 Bromomethane
ug/L1.0 20.0 1768-142106 40.082 U21 Carbon Tetrachloride
ug/L1.0 20.0 1683-11792 40.069 U18 Chlorobenzene
ug/L1.0 20.0 2645-21382 80.18 U16 Chloroethane
ug/L1.0 20.0 1778-13887 90.083 U17 Chloroform
ug/L1.0 20.0 2856-17189 60.050 U18 Chloromethane
ug/L1.0 20.0 1869-12092 60.075 U18 cis-1,2-Dichloroethene
ug/L1.0 20.0 1763-12590 10.073 U18 cis-1,3-Dichloropropene
ug/L1.0 20.0 1673-11796 50.067 U19 Dibromochloromethane
ug/L1.0 20.0 1576-124103 20.13 U21 Dibromomethane
ug/L1.0 20.0 4825-161114 130.091 U23 Dichlorodifluoromethane
ug/L1.0 20.0 1668-12484 50.10 U17 Ethylbenzene
ug/L1.0 20.0 250-200101 30.35 U20 Freon 113
ug/L1.0 20.0 1963-114120 71.125 QM-07Hexachlorobutadiene
ug/L1.0 20.0 3070-13085 60.21 U17 Isopropyl Ether
ug/L1.0 20.0 1681-13699 50.13 U20 Isopropylbenzene
ug/L2.0 40.0 1679-12186 50.18 U34 m,p-Xylenes
ug/L2.0 20.0 1768-12880 60.070 U16 Methylene Chloride
ug/L1.0 20.0 2110-12795 20.12 U19 Methyl-tert-Butyl Ether
ug/L1.0 20.0 1950-127101 0.40.4221 Naphthalene
Page 21 of 28This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 8F29023 - EPA 5030B_MS - Continued
Prepared: 07/03/2018 11:59 Analyzed: 07/05/2018 11:16Matrix Spike Dup (8F29023-MSD1) Continued
Source: CB10060-03
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 1568-12690 0.80.074 U18 n-Butyl Benzene
ug/L1.0 20.0 1676-12583 30.073 U17 n-Propyl Benzene
ug/L1.0 20.0 1571-12592 60.088 U18 o-Xylene
ug/L1.0 20.0 1775-12299 10.053 U20 sec-Butylbenzene
ug/L1.0 20.0 2373-12095 40.082 U19 Styrene
ug/L1.0 20.0 2270-13798 40.094 U20 tert-Butylbenzene
ug/L1.0 20.0 2640-181127 170.099 U25 Tetrachloroethene
ug/L1.0 20.0 1771-11887 40.053 U17 Toluene
ug/L1.0 20.0 1975-13989 90.11 U18 trans-1,2-Dichloroethene
ug/L1.0 20.0 1662-15288 20.080 U18 trans-1,3-Dichloropropene
ug/L1.0 20.0 1875-115105 40.13 U21 Trichloroethene
ug/L1.0 20.0 2268-18391 0.90.15 U18 Trichlorofluoromethane
ug/L1.0 20.0 2749-15088 20.083 U18 Vinyl chloride
ug/L1.0 60.0 1677-12188 50.22 U53 Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 8342
ug/L 50.0 70-130Dibromofluoromethane7236
ug/L 50.0 70-130Toluene-d8 7839
Semivolatile Organic Compounds by GCMS - Quality Control
Batch 8F25012 - EPA 3510C_MS
Prepared: 06/25/2018 09:50 Analyzed: 06/26/2018 14:22Blank (8F25012-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L101.5 U 2-Methylnaphthalene
ug/L101.4 U Acenaphthene
ug/L101.2 U Acenaphthylene
ug/L101.6 U Anthracene
ug/L101.3 U Benzo(a)anthracene
ug/L101.3 U Benzo(a)pyrene
ug/L101.0 U Benzo(b)fluoranthene
ug/L102.4 U Benzo(g,h,i)perylene
ug/L101.3 U Benzo(k)fluoranthene
ug/L102.0 U Chrysene
ug/L102.3 U Dibenzo(a,h)anthracene
ug/L102.1 U Fluoranthene
ug/L101.7 U Fluorene
ug/L102.2 U Indeno(1,2,3-cd)pyrene
ug/L101.3 U Naphthalene
ug/L101.4 U Phenanthrene
ug/L102.1 U Pyrene
ug/L 50.0 15-1392-Fluorobiphenyl 8040
ug/L 50.0 16-140Nitrobenzene-d5 7337
ug/L 50.0 23-164Terphenyl-d14 10452
Prepared: 06/25/2018 09:50 Analyzed: 06/26/2018 14:53LCS (8F25012-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
Page 22 of 28This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch 8F25012 - EPA 3510C_MS - Continued
Prepared: 06/25/2018 09:50 Analyzed: 06/26/2018 14:53LCS (8F25012-BS1) Continued
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L10 50.0 33-1117738 2-Methylnaphthalene
ug/L10 50.0 47-1458643 Acenaphthene
ug/L10 50.0 33-1458341 Acenaphthylene
ug/L10 50.0 27-1338945 Anthracene
ug/L10 50.0 33-1438743 Benzo(a)anthracene
ug/L10 50.0 17-1639146 Benzo(a)pyrene
ug/L10 50.0 24-1598442 Benzo(b)fluoranthene
ug/L10 50.0 10-2199547 Benzo(g,h,i)perylene
ug/L10 50.0 11-1629246 Benzo(k)fluoranthene
ug/L10 50.0 17-1688844 Chrysene
ug/L10 50.0 10-22710352 Dibenzo(a,h)anthracene
ug/L10 50.0 26-1378743 Fluoranthene
ug/L10 50.0 59-1218643 Fluorene
ug/L10 50.0 10-1719749 Indeno(1,2,3-cd)pyrene
ug/L10 50.0 21-1337738 Naphthalene
ug/L10 50.0 54-1208945 Phenanthrene
ug/L10 50.0 65-1348844 Pyrene
ug/L 50.0 15-1392-Fluorobiphenyl 8140
ug/L 50.0 16-140Nitrobenzene-d5 7739
ug/L 50.0 23-164Terphenyl-d14 9045
Prepared: 06/25/2018 09:50 Analyzed: 06/26/2018 15:25Matrix Spike (8F25012-MS1)
Source: CB09217-01
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L10 50.0 33-111811.5 U40 2-Methylnaphthalene
ug/L10 50.0 47-145891.4 U44 Acenaphthene
ug/L10 50.0 33-145861.2 U43 Acenaphthylene
ug/L10 50.0 27-133911.6 U46 Anthracene
ug/L10 50.0 33-143901.3 U45 Benzo(a)anthracene
ug/L10 50.0 17-163951.3 U48 Benzo(a)pyrene
ug/L10 50.0 24-159891.0 U45 Benzo(b)fluoranthene
ug/L10 50.0 10-219952.4 U48 Benzo(g,h,i)perylene
ug/L10 50.0 11-162951.3 U47 Benzo(k)fluoranthene
ug/L10 50.0 17-168912.0 U46 Chrysene
ug/L10 50.0 10-2271032.3 U52 Dibenzo(a,h)anthracene
ug/L10 50.0 26-137812.1 U41 Fluoranthene
ug/L10 50.0 59-121881.7 U44 Fluorene
ug/L10 50.0 10-1711002.2 U50 Indeno(1,2,3-cd)pyrene
ug/L10 50.0 21-133801.3 U40 Naphthalene
ug/L10 50.0 54-120921.4 U46 Phenanthrene
ug/L10 50.0 52-115822.1 U41 Pyrene
ug/L 50.0 15-1392-Fluorobiphenyl 8643
ug/L 50.0 16-140Nitrobenzene-d5 8040
ug/L 50.0 23-164Terphenyl-d14 8141
Prepared: 06/25/2018 09:50 Analyzed: 06/26/2018 15:56Matrix Spike Dup (8F25012-MSD1)
Source: CB09217-01
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
Page 23 of 28This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch 8F25012 - EPA 3510C_MS - Continued
Prepared: 06/25/2018 09:50 Analyzed: 06/26/2018 15:56Matrix Spike Dup (8F25012-MSD1) Continued
Source: CB09217-01
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L10 50.0 2533-11179 21.5 U39 2-Methylnaphthalene
ug/L10 50.0 2547-14586 31.4 U43 Acenaphthene
ug/L10 50.0 2533-14583 31.2 U41 Acenaphthylene
ug/L10 50.0 2527-13388 31.6 U44 Anthracene
ug/L10 50.0 2533-14385 61.3 U42 Benzo(a)anthracene
ug/L10 50.0 2517-16391 51.3 U45 Benzo(a)pyrene
ug/L10 50.0 2524-15987 31.0 U43 Benzo(b)fluoranthene
ug/L10 50.0 2510-21982 152.4 U41 Benzo(g,h,i)perylene
ug/L10 50.0 2511-16293 21.3 U47 Benzo(k)fluoranthene
ug/L10 50.0 2517-16885 72.0 U43 Chrysene
ug/L10 50.0 2510-22790 132.3 U45 Dibenzo(a,h)anthracene
ug/L10 50.0 2526-13790 112.1 U45 Fluoranthene
ug/L10 50.0 2559-12188 0.51.7 U44 Fluorene
ug/L10 50.0 2510-17187 142.2 U43 Indeno(1,2,3-cd)pyrene
ug/L10 50.0 2521-13378 31.3 U39 Naphthalene
ug/L10 50.0 2554-12087 61.4 U44 Phenanthrene
ug/L10 50.0 2552-11590 102.1 U45 Pyrene
ug/L 50.0 15-1392-Fluorobiphenyl 8543
ug/L 50.0 16-140Nitrobenzene-d5 8040
ug/L 50.0 23-164Terphenyl-d14 9447
Metals (acid extractable) by EPA 6000/7000 Series Methods - Quality Control
Batch 8F22032 - SM18 3030C
Prepared: 06/22/2018 14:23 Analyzed: 07/09/2018 14:39Blank (8F22032-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L10.03.10 U Lead
Prepared: 06/22/2018 14:23 Analyzed: 07/09/2018 14:44LCS (8F22032-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L10.0 200 80-120115231 Lead
Prepared: 06/22/2018 14:23 Analyzed: 07/09/2018 14:46Matrix Spike (8F22032-MS1)
Source: CB08873-02
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L10.0 200 75-1251203.10 U239 Lead
Prepared: 06/22/2018 14:23 Analyzed: 07/09/2018 14:48Matrix Spike Dup (8F22032-MSD1)
Source: CB08873-02
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L10.0 200 2075-125121 0.93.10 U242 Lead
Prepared: 06/22/2018 14:23 Analyzed: 07/09/2018 14:51Post Spike (8F22032-PS1)
Source: CB08873-02
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
Page 24 of 28This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Metals (acid extractable) by EPA 6000/7000 Series Methods - Quality Control
Batch 8F22032 - SM18 3030C - Continued
Prepared: 06/22/2018 14:23 Analyzed: 07/09/2018 14:51Post Spike (8F22032-PS1) Continued
Source: CB08873-02
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L0.00935 0.190 80-1201810.0007860.345 QM-08Lead
Classical Chemistry Parameters - Quality Control
Batch 8F26001 - NO PREP
Prepared & Analyzed: 06/26/2018 07:44Blank (8F26001-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L2.52.5 U Total Suspended Solids
Prepared & Analyzed: 06/26/2018 07:44LCS (8F26001-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L2.5 100 80-120100100 Total Suspended Solids
Prepared & Analyzed: 06/26/2018 07:44Duplicate (8F26001-DUP1)
Source: CB06958-01
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L50 202270260 Total Suspended Solids
Prepared & Analyzed: 06/26/2018 07:44Duplicate (8F26001-DUP2)
Source: CB07173-01
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L12 2025049 Total Suspended Solids
Classical Chemistry Parameters - Quality Control
Batch 8G02016 - NO PREP
Prepared: 07/02/2018 10:15 Analyzed: 07/03/2018 09:30Blank (8G02016-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L0.0500.034 U Phenolics
Prepared: 07/02/2018 10:15 Analyzed: 07/03/2018 09:30LCS (8G02016-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L0.050 0.500 90-1101010.51 Phenolics
Prepared: 07/02/2018 10:15 Analyzed: 07/03/2018 09:30Matrix Spike (8G02016-MS1)
Source: AB04120-01
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L0.050 0.500 90-110980.034 U0.49 Phenolics
Prepared: 07/02/2018 10:15 Analyzed: 07/03/2018 09:30Matrix Spike Dup (8G02016-MSD1)
Source: AB04120-01
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 8G02016 - NO PREP - Continued
Prepared: 07/02/2018 10:15 Analyzed: 07/03/2018 09:30Matrix Spike Dup (8G02016-MSD1) Continued
Source: AB04120-01
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L0.050 0.500 1090-11097 10.034 U0.48 Phenolics
Classical Chemistry Parameters - Quality Control
Batch 8G02007 - EPA 1664B
Prepared: 07/02/2018 12:10 Analyzed: 07/03/2018 18:01Blank (8G02007-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L5.002.40 U Oil & Grease (HEM)
Prepared: 07/02/2018 12:10 Analyzed: 07/03/2018 18:01LCS (8G02007-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L5.00 159 78-11487139 Oil & Grease (HEM)
Prepared: 07/02/2018 12:10 Analyzed: 07/03/2018 18:01LCS Dup (8G02007-BSD1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L5.00 159 1878-114106 19167 QM-12Oil & Grease (HEM)
Prepared: 07/02/2018 12:10 Analyzed: 07/03/2018 18:01Matrix Spike (8G02007-MS1)
Source: BB02867-02
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L5.00 150 78-114892.40 U134 Oil & Grease (HEM)
Page 26 of 28This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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FLAGS/NOTES AND DEFINITIONS
The sample was analyzed at dilution.
The analyte was detected in the associated method blank.
The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
MRL
E
U
J
D
B
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.PQL
The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was
accepted based on acceptable LCS recovery.
QM-07
Post-digestion spike did not meet method requirements due to confirmed matrix effects
(dilution test).
QM-08
Precision between duplicate samples was outside acceptance limits.QM-12
Page 27 of 28This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL