3406_PiedmontLF_MSWLFclosed_GWMR_20170620

WASTE MANAGEMENT
Closed Site Management Group
1850 Parkway Place
Suite 600
Marietta, GA 30067
Ph. 770-590-2936
Cell: 404-354-3132

June 20, 2017

Ms. Jackie Drummond
NC Department of Environmental Quality
Division of Waste Management – Solid Waste Section
1646 Mail Service Center
Raleigh, North Carolina 27699-1646

RE: 2017 Annual Water Quality Monitoring Report
Piedmont Landfill and Recycling Center, Kernersville, North Carolina
Permit Number 34-06

Dear Ms. Drummond:

Waste Management of Carolinas is submitting the 2017 Annual Water Quality Monitoring
Report (WQMR) for the Piedmont landfill and Recycling Center, Permit No. 34-06. Per the
North Carolina Department of Environmental Quality approval letter dated October 8, 2015,
the routine groundwater and surface monitoring frequency for Piedmont Landfill is reduced
from semiannual to annual. The report package includes an Environmental Monitoring
Reporting Form and the complete WQMR and laboratory data in electronic format. Samples
were collected by Professional Technical Support Services (ProTech) on March 14-15, 2017,
and leachate samples by Joyce Engineering on May 3, 2017. All samples were transported to
the Test America, Inc. laboratory in Arvada, Colorado for analysis.

The Piedmont Landfill and Recycling Center is a closed municipal solid waste facility that last
received waste in 2004 and entered into post closure care in accordance with Rule .1627(d) of
the North Carolina Solid Waste Management Regulations (NCSWMR) as of October 29, 2004.
All points at the facility are currently being monitored under a Detection Monitoring Program
under Rule .1633 of the NCSWMR.

An exceedance of the NC2L groundwater standard for chromium was detected in well MW-03;
however, an Alternate Source Demonstration for chromium was submitted on July 26, 2010,
and was approved by the Solid Waste Section (SWS) in a letter dated April 28, 2011. There
were no other exceedances of Groundwater Protection Standards for any NCSWMR Appendix
I constituents during the 2017 annual sampling event.

A copy of this report will be placed into the site’s operating record in accordance with Rule
.1633(c)(1) of the NCSWMR.

The next sampling event for the Piedmont Landfill and Recycling Center is scheduled for the
first quarter of 2018 in accordance with the Water Quality Monitoring Plan, Revised December
2015, and approved by the SWS in a letter dated January 12, 2016. If you have any questions
or concerns regarding this report, please call me at [phone].

Sincerely,
Waste Management of Carolinas, Inc.

Alexander Lacsamana, P.E.
District Manager, Closed Sites

Enclosure

cc: Van Burbach, Ph.D., P.G. – Joyce Engineering

PREPARED FOR:
PIEDMONT LANDFILL & RECYCLING CENTER
9901 FREEMAN ROAD
KERNERSVILLE, NORTH CAROLINA 27284

PIEDMONT LANDFILL & RECYCLING CENTER
PERMIT # 34-06

2017 ANNUAL
WATER QUALITY MONITORING REPORT

JUNE 2017

PREPARED BY:

2211 WEST MEADOWVIEW ROAD, SUITE 101
GREENSBORO, NORTH CAROLINA 27407
NC LICENSE NUMBER: C-0782
PHONE: [phone]
FAX: [phone]
JOYCE PROJECT NO. 00392.1701.12

2211 West Meadowview Rd.
Boone Building, Suite 101
Greensboro, NC 27407
tel: [phone]
fax: [phone]

www.JoyceEngineering.com

June 20, 2017

Alexander Lacsamana, PE
District Manager
Waste Management Closed Site Management Group
1850 Parkway Place, Suite 600
Marietta, GA 30067

RE: 2017 Annual Water Quality Monitoring Report
Piedmont Landfill & Recycling Center, Permit No. 34-06
JOYCE Project No. 392.1701.12, Task 01

Dear Mr. Lacsamana:

The purpose of this report is to provide you with a complete submittal to satisfy the
groundwater monitoring compliance requirements for the closed Piedmont Landfill and
Recycling Center’s annual groundwater monitoring event for 2017. This report may also serve
to fulfill the notification requirements of Rule .1635 (g) of the North Carolina Solid Waste
Management Regulations (NCSWMR). An Environmental Monitoring Reporting Form (EMRF)
for this event is attached.

Sampling for the event was performed on March 14-15, 2017, by ProTech. During this
annual event, the site compliance wells and surface water monitoring points were sampled and
analyzed for the NC Appendix I list of constituents. The site leachate was also sampled on May
3, 2017, to be included with this event for the required list of parameters. The laboratory
analytical reports, field data logs, and chains of custody are provided as Appendix A of this
report.

MONITORING NETWORK:
The current monitoring network for this facility was accepted by the North Carolina
Department of Environmental Quality (NCDEQ) in a letter dated January 12, 2016, in response
to the facility’s revised Water Quality Monitoring Plan dated December 2015. The current
network consists of 11 monitoring wells: MW-01, MW-02, MW-03, MW-04, MW-05, MW-07,
MW-08, MW-9R, MW-10, MW-11, and MW-12. MW-01 is an upgradient background well and
the others are downgradient compliance wells. The locations of the monitoring wells are shown
on Drawing 1 (presented in Appendix B). Table 1 presents the construction data for the
monitoring wells. The monitoring wells are sampled annually in accordance with the North
Carolina Solid Waste Management Regulations (NCSWMR) and the Water Quality Monitoring
Plan for this facility.
Mr. Al Lacsamana
June 20, 2017
Page 2 of 5

Surface water at the facility is monitored annually in conjunction with the groundwater
sampling events. Samples are collected from four surface water monitoring points: S-02, S-03,
S-04, and S-05. Surface point S-01 was removed from the monitoring program as approved in a
letter from the North Carolina Department of Natural Resources (DENR), now the NCDEQ,
dated July 15, 2010. The locations of the surface water points are shown on Drawing 1.

MONITORING PROGRAM HISTORY:
The site entered into an Assessment Monitoring Program for background wells MW-01
and MW-06 and downgradient well MW-09 after volatile organic constituents were detected in
MW-09 during the second semiannual event of 1996. Two organic compounds (chloroethane
and 1,1-dichloroethane) were historically detected in monitoring well MW-09. Chloroethane
exhibited a declining trend to the point where chloroethane was reported at less than the
laboratory reporting limit during the January 1998 sampling event. The concentration of
1,1-dichloroethane in MW-09 also decreased below the laboratory reporting limit during the July
1998 sampling event. Following receipt of approval from DENR, all wells at the site reverted to
the Detection Monitoring Program as of the second semiannual event in 1999, as allowed by
15A NCAC 13B.1634 (b).

Monitoring well MW-09 was replaced by well MW-09R in November 1999. No
chloroethane concentration above the laboratory reporting limit or Solid Waste Section Limit
(SWSL) has been detected in MW-09R since the well was installed; however, 1,1-dichloroethane
was detected in MW-09R at a concentration of 23 g/L during the initial sampling event
conducted in January 2000. The concentration of 1,1-dichlorothane remained relatively
consistent until 2009, ranging in concentration from 7 g/L to 28 g/L; however, it has not been
detected at quantifiable levels since September 2009. The constituent cis-1,2-dichloroethene
was detected in MW-09R above the laboratory reporting limit for the first time during the July
2002 event at a concentration of 6.5 g/L, and has been detected at concentrations ranging from
5-28 µg/L; however, it has not been detected at quantifiable levels since September 2009. The
presence of organic constituents in MW-09 and MW-09R is attributed to landfill gas (LFG). The
LFG extraction network was expanded in this area in January 2003, and the recent decrease in
concentrations of organic constituents in this well is attributed to the control of LFG.

Due to the detection of 1,1-dichloroethane in MW-09R during the first semiannual event
in 2000, the site performed Assessment Monitoring on wells MW-01, MW-06, and MW-09R
through the second semiannual event of 2001. Following DENR approval of an August 20, 2001
request by Waste Management, MW-01 and MW-06 again reverted to Detection Monitoring.
Monitoring well MW-09R was sampled for the NC Appendix I list of constituents plus detected
Appendix II constituents during the first semiannual event each year and NC Appendix II list of
constituents during the second semiannual event until the DENR approved reverting back to
detection monitoring in a letter dated March 15, 2012.

Mr. Al Lacsamana
June 20, 2017
Page 3 of 5

In the September 2007 sampling event, benzene and vinyl chloride were detected in
MW-02 at concentrations in exceedance of the groundwater standards established in 15A NCAC
2L.020 (NC2L). A resampling event confirmed the vinyl chloride, but not the benzene
exceedance. An Alternate Source Demonstration (ASD) was submitted to DENR on March 14,
2008. The ASD demonstrated that the organic constituents detected in MW-02 are related to
LFG impacts. In January 2008, improvements to the active LFG recovery system at the site
were initiated to help mitigate these impacts. The ASD was accepted by DENR in a letter dated
May 7, 2008 with the condition that if vinyl chloride and benzene concentrations in MW-02 are
not sufficiently reduced by spring 2009, MW-02 would enter Assessment Monitoring. Neither
benzene nor vinyl chloride have had confirmed detections above the NC2L standards in MW-02
since September 2008, so MW-02 remains in detection monitoring.

During the March 2010 sampling event, chromium was detected in MW-03 at a
statistically significant concentration above the NC2L groundwater standard. An ASD was
submitted on July 26, 2010 for the chromium demonstrating that the chromium was naturally
occurring in the soil and groundwater of the facility. DENR approved the ASD for chromium at
the facility in a letter dated April 28, 2011.

A Request to Reduce Monitoring Requirements was submitted to the NCDEQ by Joyce
Engineering in a report dated September 23, 2015, on behalf of Waste Management. The report
requested that the frequency of water quality sampling be reduced from semiannual to annual,
and it requested the removal of wells MW-4D, MW-6, MW-11D, and MW-12D from the
compliance network. NCDEQ approved the request in a letter dated October 8, 2015. A revised
Water Quality Monitoring Plan for the Piedmont Landfill & Recycling Center, Permit 34-06,
was then submitted to the NCDEQ in December 2015, reflecting the approved changes. The
revised Water Quality Monitoring Plan, was approved for the facility by the NCDEQ in a letter
dated January 12, 2016.

DETECTION MONITORING EVENT:
MW-01, MW-02, MW-03, MW-04, MW-05, MW-07, MW-08, MW-9R, MW-10, MW-11,
MW-12, and Surface Water Points: S-02, S-03, S-04, and S-05
The 2017 annual sampling event was conducted by ProTech on March 14-15, 2017.
Eleven monitoring wells and four surface water points were sampled for the NC Appendix I list
of constituents. The laboratory analytical reports, field data logs, and chains of custody for the
2017 annual event are provided in Appendix A of this report. Table 2 presents the quantified
detections above the NCDEQ Solid Waste Section Reporting limits (SWSL) for the 2017
sampling event. Table 3 presents the exceedances of 15A NCAC 2L.0202 Groundwater
Standards (NC2L Standards) or the NCDEQ Solid Waste Section Groundwater Protection
Standards (GWPS) for the 2017 sampling event. Table 4 presents the field parameters for the
March 2017 sampling event.

Mr. Al Lacsamana
June 20, 2017
Page 4 of 5

Organic Constituents
There were no quantified detections (above the SWSL) of any Appendix I organic
constituents in any of the monitoring wells or surface water points during the 2017 Annual
sampling event.

Inorganic Constituents
Two inorganic constituents had quantified detections (above the SWSL) in one or more
monitoring wells. These included barium in MW-02 and chromium in MW-03. Zinc in MW-08
was blank-qualified by a detection in the field blank. Chromium was detected above the NC2L
Standard in MW-03. An ASD for chromium was approved by the NCDEQ in a letter dated April
28, 2011; therefore, the detections are not considered regulatory exceedances of Groundwater
Protection Standards (GPS). No other Appendix I inorganic constituents were detected above
the SWSL or the NC2L or GWPS in any monitoring well. There were no quantified detections
(above the SWSL) of any inorganic constituents in any of the surface water samples collected
during the 2017 annual sampling event.

SUBMITTAL OF LEACHATE ANALYTICAL DATA:
Appendix A to this report contains the leachate monitoring results for the May 3, 2017,
sampling event as requested in the Solid Waste Section memo dated November 13, 1996, and
confirmed by DEQ as required in May 2017. The leachate was analyzed for NC Appendix I
constituents, alkalinity, carbonate alkalinity, bicarbonate alkalinity, TDS, TOC, chloride,
ammonia, sulfate, nitrate, phosphorus, BOD, COD, TSS, mercury, indicator metals (calcium,
iron, magnesium, manganese, sodium, and potassium), and the required field parameters.

SUBMITTAL OF GROUNDWATER MAP AND FLOW CALCULATIONS:
Appendix B to this report contains the groundwater surface potentiometric surface map
(Drawing 1) and groundwater flow rates for this event. In summary, the 2017 sampling results
and groundwater flow assessment indicate that the site monitoring network is effective in
monitoring for the release of solid waste constituents to the environment.

CONCLUSIONS/CLOSURE:
There were no organic constituents with quantified detections (above the SWSL)
reported for any monitoring wells or surface water points during the 2017 annual monitoring
event. Two inorganic constituents had quantified detections in two monitoring wells, and
chromium was detected above the NC2L groundwater standard in MW-03. An ASD was
submitted on July 26, 2010, for the exceedance of chromium during the March 2010 sampling
event. On April 28, 2011, DENR, now NCDEQ, approved the ASD for chromium at the facility.
MW-03 will continue to be monitored in accordance with the Detection Monitoring Program.

Mr. Al Lacsamana
June 20, 2017
Page 5 of 5

The current approved monitoring network will continue to be monitored in accordance
with the Detection Monitoring Program and surface water points will continue to be monitored
as required by the NCDEQ. The frequency of groundwater and surface water monitoring for the
closed Piedmont Landfill and Recycling Center has changed to annual as approved by NCDEQ
in correspondence dated October 8, 2015. Therefore the next groundwater and surface water
monitoring event is scheduled for the first quarter of 2018. If you have any questions, feel free
to contact me at [phone].

Sincerely,
JOYCE ENGINEERING

G. Van Ness Burbach, PhD, P.G.
Senior Technical Consultant

Attachments: Environmental Monitoring Reporting Form
Tables
Appendix A – Laboratory Analytical Reports
Appendix B – Groundwater Flow Regime Report

TABLES

TABLE 1: MONITORING WELL CONSTRUCTION DATA LATITUDE LONGITUDEGround SurfaceTOC(inches)Top Bottom Top BottomMW-0107/13/89 N36° 11' 39.28" W80° 02' 15.38" 821.40 823.93 2.00 49.00 772.40 47.00 774.40 44.00 49.00 777.4 772.40 45.94 777.99 WEATHERED GNEISS BEDROCKMW-0208/05/89 N36° 11' 50.38" W80° 02' 18.24" 767.30 778.04 2.00 25.50 741.80 - - 20.20 25.20 747.1 742.10 DRY DRY SAPROLITE (SILTY SAND)MW-0308/06/89 N36° 11' 54.05" W80° 02' 36.88" 767.30 770.08 2.00 38.00 729.30 - - 32.50 37.50 734.8 729.80 27.22 742.86 SAPROLITE (SILTY SAND)MW-0407/14/89 N36° 11' 39.58" W80° 02' 37.28" 754.50 756.92 2.00 27.00 727.50 - - 20.00 25.00 734.5 729.50 15.98 740.94 SAPROLITE (SILTY SAND)MW-04D#02/18/94 N36° 11' 39.77" W80° 02' 37.18" 754.30 757.33 2.00 62.00 692.30 62.00 692.30 53.25 58.25 701.05 696.05 15.20 742.13 SAPROLITE/WEATHERED BEDROCKMW-0508/02/89 N36° 11' 45.46" W80° 02' 50.50" 740.40 743.17 2.00 20.50 719.90 - - 14.45 19.45 725.95 720.95 5.69 737.48 SAPROLITE (SILTY SAND)MW-0608/09/93 N36° 11' 41.27" W80° 02' 13.01" 798.00 800.82 2.00 26.80 771.20 - - 20.90 25.90 777.1 772.10 DRY DRY SAPROLITE (SILTY SAND)MW-0708/25/94 N36° 11' 50.96" W80° 02' 32.64" 768.87 771.57 2.00 33.50 735.37 - - 17.00 32.40 751.87 736.47 27.10 744.47 SAPROLITE (SILTY SAND)MW-0808/31/94 N36° 11' 41.12" W80° 02' 43.97" 746.15 748.95 2.00 22.00 724.15 - - 5.00 20.00 741.15 726.15 9.94 739.01 SAPROLITE (SILTY SAND)MW-0908/30/94 N36° 11' 48.79" W80° 02' 50.54" 767.82 770.62 2.00 35.00 732.82 - - 19.81 34.81 748.01 733.01 - - SAPROLITE (SAND)/BEDROCKMW-09R11/09/99 N36° 11' 48.82" W80° 02' 50.74" 762.95 764.95 2.00 41.20 721.75 28.00 734.95 32.00 42.50 730.95 720.45 27.71 737.24 BEDROCKMW-1010/24/94 N36° 11' 50.64" W80° 02' 28.61" 774.20 777.20 2.00 38.00 736.20 - - 20.00 36.99 754.2 737.21 33.52 743.68 SAPROLITE (CLAYEY SILT/SILT)MW-1111/17/94 N36° 11' 50.44" W80° 02' 21.49" 774.30 776.80 2.00 35.00 739.30 - - 19.01 34.22 755.29 740.08 30.28 746.52 SAPROLITE (SILT/SANDY SILT)MW-11D11/15/94 N36° 11' 50.56" W80° 02' 21.46" 773.86 776.36 2.00 93.50 680.36 - - 81.82 91.79 692.04 682.07 30.22 746.14 SAPROLITE (SANDY SILT/GRAVELY SILT)MW-1210/21/94 N36° 11' 37.16" W80° 02' 33.26" 748.58 751.48 2.00 18.00 730.58 - - 3.33 17.22 745.25 731.36 7.27 744.21 SAPROLITE (SILTY CLAY/SANDY SILT)MW-12D10/27/94 N36° 11' 37.11" W80° 02' 33.16" 748.73 751.53 2.00 43.30 705.43 - - 31.98 42.20 716.75 706.53 7.08 744.45 SAPROLITE (SILTY GRAVEL)TOC = Top of PVC Well Casing. BGS = Below ground surface. AMSL = Above mean sea level.# MW-4D originally called PZ-13. * Groundwater data from September 16-17, 2015.LITHOLOGY OF SCREENED INTERVALTOP OF BEDROCKDepth (feet BGS)Elevation (feet AMSL)GROUNDWATER *Depth to Water (feet below TOC)Water Table Elevation (feet AMSL)Depth (feet BGS)Elevation (feet AMSL)SCREENED INTERVALWELL IDINSTAL. DATEDepth (feet BGS)Elevation (feet AMSL)CASING DIAMETER(feet AMSL)WELL ELEVATIONS TOTAL DEPTH WELL LOCATIONPiedmont Landfill and Recycling Center , Permit # 34-06Joyce Engineering
WELL ID PARAMETER RESULT UNITS SWSL COLLECT DATE3406-MW02 Barium, Total 160 µg/L 100 03/16/20163406-MW03 Chromium, Total 11 µg/L 10 03/16/2016WELL ID PARAMETER RESULT UNITS SWSLNC2L/ GWPS*GPS COLLECT DATE3406-MW03 Chromium, Total 11 µg/L 10 10 ASD 03/16/2016Table Notes:µg/L = Micrograms per LiterSWSL = NC Solid Waste Section Reporting LimitLaboratory Reporting Limit is used if a SWSL is not established.NC2L = NC Groundwater Standard from 15A NCAC 2L.0202GWPS = NC Solid Waste Section Groundwater Protection Standard (for constituents without a NC2L).GPS = Groundwater Protection Standard for facility as defined by 15A NCAC 13B.1634(g)ASD = Alternate Source Demonstration. The ASD for Chromium in the soil was approved by NC DENR 04/28/2011.Detections exclude blank-qualified data.TABLE 2: Quantified Detections above NC SWSLsTABLE 3: Exceedances of NC Groundwater or Surface Water StandardsPiedmont Landfill and Recycling Center, Permit # 34-06Joyce Engineering
TABLE 4: Field Parameters
WELL ID # PARAMETER RESULT UNITS COLLECT DATE
3406-MW01 Well Elevation 823.93 ft/msl 03/15/2017
3406-MW01 Depth to Water 44.38 ft 03/15/2017
3406-MW01 Dissolved Oxygen 3.5 mg/L 03/15/2017
3406-MW01 Groundwater Elevation (feet) 779.55 ft/msl 03/15/2017
3406-MW01 Oxygen Reduction Potential (mV) 157.7 millivolts 03/15/2017
3406-MW01 pH (field) 6.15 s.u. 03/15/2017
3406-MW01 SpecCond (field) 68 umhos/cm 03/15/2017
3406-MW01 Temp (oC) 12.5 Degrees C 03/15/2017
3406-MW01 Turbidity 3.4 NTU 03/15/2017
3406-MW02 Well Elevation 778.04 ft/msl 03/15/2017
3406-MW02 Depth to Water 29.14 ft 03/15/2017
3406-MW02 Dissolved Oxygen 1.9 mg/L 03/15/2017
3406-MW02 Groundwater Elevation (feet) 748.9 ft/msl 03/15/2017
3406-MW02 Oxygen Reduction Potential (mV) 261.4 millivolts 03/15/2017
3406-MW02 pH (field) 5.51 s.u. 03/15/2017
3406-MW02 SpecCond (field) 145 umhos/cm 03/15/2017
3406-MW02 Temp (oC) 11.7 Degrees C 03/15/2017
3406-MW02 Turbidity 1.5 NTU 03/15/2017
3406-MW03 Well Elevation 24.02 ft 03/15/2017
3406-MW03 Depth to Water 25.57 ft/msl 03/15/2017
3406-MW03 Dissolved Oxygen 4.2 mg/L 03/15/2017
3406-MW03 Groundwater Elevation (feet) 744.51 ft/msl 03/15/2017
3406-MW03 Oxygen Reduction Potential (mV) 62.1 millivolts 03/15/2017
3406-MW03 pH (field) 6.17 s.u. 03/15/2017
3406-MW03 SpecCond (field) 176 umhos/cm 03/15/2017
3406-MW03 Temp (oC) 10.1 Degrees C 03/15/2017
3406-MW03 Turbidity 3.4 NTU 03/15/2017
3406-MW04 Well Elevation 12.50 ft 03/15/2017
3406-MW04 Depth to Water 12.94 ft/msl 03/15/2017
3406-MW04 Dissolved Oxygen 0.0 mg/L 03/15/2017
3406-MW04 Groundwater Elevation (feet) 743.98 ft/msl 03/15/2017
3406-MW04 Oxygen Reduction Potential (mV) 233 millivolts 03/15/2017
3406-MW04 pH (field) 5.25 s.u. 03/15/2017
3406-MW04 SpecCond (field) 96 umhos/cm 03/15/2017
3406-MW04 Temp (oC) 14.6 Degrees C 03/15/2017
3406-MW04 Turbidity 6.5 NTU 03/15/2017
3406-MW05 Well Elevation 743.17 ft/msl 03/15/2017
3406-MW05 Depth to Water 4.43 ft 03/15/2017
3406-MW05 Dissolved Oxygen 1.1 mg/L 03/15/2017
3406-MW05 Groundwater Elevation (feet) 738.74 ft/msl 03/15/2017
3406-MW05 Oxygen Reduction Potential (mV) 168 millivolts 03/15/2017
3406-MW05 pH (field) 6 s.u. 03/15/2017
3406-MW05 SpecCond (field) 349 umhos/cm 03/15/2017
3406-MW05 Temp (oC) 13.3 Degrees C 03/15/2017
3406-MW05 Turbidity 2.3 NTU 03/15/2017
Piedmont Landfill and Recycling Center, Permit # 34-06 1 of 4 Joyce Engineering
TABLE 4: Field Parameters
WELL ID # PARAMETER RESULT UNITS COLLECT DATE
3406-MW07 Well Elevation 771.57 ft/msl 03/15/2017
3406-MW07 Depth to Water 24.8 ft 03/15/2017
3406-MW07 Dissolved Oxygen 5.3 mg/L 03/15/2017
3406-MW07 Groundwater Elevation (feet) 746.77 ft/msl 03/15/2017
3406-MW07 Oxygen Reduction Potential (mV) 128 millivolts 03/15/2017
3406-MW07 pH (field) 6.32 s.u. 03/15/2017
3406-MW07 SpecCond (field) 147 umhos/cm 03/15/2017
3406-MW07 Temp (oC) 14.2 Degrees C 03/15/2017
3406-MW07 Turbidity 6 NTU 03/15/2017
3406-MW08 Well Elevation 748.95 ft/msl 03/15/2017
3406-MW08 Depth to Water 5.33 ft 03/15/2017
3406-MW08 Dissolved Oxygen 0.7 mg/L 03/15/2017
3406-MW08 Groundwater Elevation (feet) 743.62 ft/msl 03/15/2017
3406-MW08 Oxygen Reduction Potential (mV) 157.8 millivolts 03/15/2017
3406-MW08 pH (field) 6.32 s.u. 03/15/2017
3406-MW08 SpecCond (field) 147 umhos/cm 03/15/2017
3406-MW08 Temp (oC) 14.2 Degrees C 03/15/2017
3406-MW08 Turbidity 6 NTU 03/15/2017
3406-MW09R Well Elevation 22.97 ft 03/15/2017
3406-MW09R Depth to Water 26 ft/msl 03/15/2017
3406-MW09R Dissolved Oxygen 2.7 mg/L 03/15/2017
3406-MW09R Groundwater Elevation (feet) 738.95 ft/msl 03/15/2017
3406-MW09R Oxygen Reduction Potential (mV) 44.2 millivolts 03/15/2017
3406-MW09R pH (field) 6.19 s.u. 03/15/2017
3406-MW09R SpecCond (field) 314 umhos/cm 03/15/2017
3406-MW09R Temp (oC) 24.5 Degrees C 03/15/2017
3406-MW09R Turbidity 2.0 NTU 03/15/2017
3406-MW10 Well Elevation 777.20 ft/msl 03/15/2017
3406-MW10 Depth to Water 31.07 ft 03/15/2017
3406-MW10 Dissolved Oxygen 3.9 mg/L 03/15/2017
3406-MW10 Groundwater Elevation (feet) 746.13 ft/msl 03/15/2017
3406-MW10 Oxygen Reduction Potential (mV) 235.3 millivolts 03/15/2017
3406-MW10 pH (field) 5.98 s.u. 03/15/2017
3406-MW10 SpecCond (field) 93 umhos/cm 03/15/2017
3406-MW10 Temp (oC) 9.6 Degrees C 03/15/2017
3406-MW10 Turbidity 6.8 NTU 03/15/2017
3406-MW11 Well Elevation 27.34 ft 03/15/2017
3406-MW11 Depth to Water 28.8 ft/msl 03/15/2017
3406-MW11 Dissolved Oxygen 2.2 mg/L 03/15/2017
3406-MW11 Groundwater Elevation (feet) 748 ft/msl 03/15/2017
3406-MW11 Oxygen Reduction Potential (mV) 156 millivolts 03/15/2017
3406-MW11 pH (field) 5.71 s.u. 03/15/2017
3406-MW11 SpecCond (field) 185 umhos/cm 03/15/2017
3406-MW11 Temp (oC) 13.8 Degrees C 03/15/2017
3406-MW11 Turbidity 3.1 NTU 03/15/2017
Piedmont Landfill and Recycling Center, Permit # 34-06 2 of 4 Joyce Engineering
TABLE 4: Field Parameters
WELL ID # PARAMETER RESULT UNITS COLLECT DATE
3406-MW12 Well Elevation 751.48 ft/msl 03/15/2017
3406-MW12 Depth to Water 6.08 ft 03/15/2017
3406-MW12 Dissolved Oxygen 1.5 mg/L 03/15/2017
3406-MW12 Groundwater Elevation (feet) 745.4 ft/msl 03/15/2017
3406-MW12 Oxygen Reduction Potential (mV) 96.2 millivolts 03/15/2017
3406-MW12 pH (field) 5.88 s.u. 03/15/2017
3406-MW12 SpecCond (field) 141 umhos/cm 03/15/2017
3406-MW12 Temp (oC) 12.9 Degrees C 03/15/2017
3406-MW12 Turbidity 6.7 NTU 03/15/2017
3406-S02 Dissolved Oxygen 7.9 mg/L 03/14/2017
3406-S02 Oxygen Reduction Potential (mV) 109.3 millivolts 03/14/2017
3406-S02 pH (field) 6.13 s.u. 03/14/2017
3406-S02 SpecCond (field) 119 umhos/cm 03/14/2017
3406-S02 Temp (oC) 9.5 Degrees C 03/14/2017
3406-S02 Turbidity 14.3 NTU 03/14/2017
3406-S03 Dissolved Oxygen 8.5 mg/L 03/14/2017
3406-S03 Oxygen Reduction Potential (mV) 203.9 millivolts 03/14/2017
3406-S03 pH (field) 4.97 s.u. 03/14/2017
3406-S03 SpecCond (field) 95 umhos/cm 03/14/2017
3406-S03 Temp (oC) 9.1 Degrees C 03/14/2017
3406-S03 Turbidity 22.9 NTU 03/14/2017
3406-S04 Dissolved Oxygen 8.3 mg/L 03/14/2017
3406-S04 Oxygen Reduction Potential (mV) 214 millivolts 03/14/2017
3406-S04 pH (field) 5.48 s.u. 03/14/2017
3406-S04 SpecCond (field) 96 umhos/cm 03/14/2017
3406-S04 Temp (oC) 9.9 Degrees C 03/14/2017
3406-S04 Turbidity 19.6 NTU 03/14/2017
3406-S05 Dissolved Oxygen 7.9 mg/L 03/14/2017
3406-S05 Oxygen Reduction Potential (mV) 164.3 millivolts 03/14/2017
3406-S05 pH (field) 5.82 s.u. 03/14/2017
3406-S05 SpecCond (field) 175 umhos/cm 03/14/2017
3406-S05 Temp (oC) 10.1 Degrees C 03/14/2017
3406-S05 Turbidity 11.9 NTU 03/14/2017
3406-T01 Dissolved Oxygen 1.9 mg/L 05/03/2017
3406-T01 Oxygen Reduction Potential (mV) 33.3 millivolts 05/03/2017
3406-T01 pH (field) 7.45 s.u. 05/03/2017
3406-T01 SpecCond (field) 3999 umhos/cm 05/03/2017
3406-T01 Temp (oC) 21.6 Degrees C 05/03/2017
3406-T01 Turbidity 38.7 NTU 05/03/2017
Piedmont Landfill and Recycling Center, Permit # 34-06 3 of 4 Joyce Engineering
TABLE 4: Field Parameters
WELL ID # PARAMETER RESULT UNITS COLLECT DATE
3406-01FB Dissolved Oxygen 0.8 mg/L 03/15/2017
3406-01FB Oxygen Reduction Potential (mV) 41.3 millivolts 03/15/2017
3406-01FB pH (field) 6.74 s.u. 03/15/2017
3406-01FB SpecCond (field) 6 umhos/cm 03/15/2017
3406-01FB Temp (oC) 17.2 Degrees C 03/15/2017
3406-01FB Turbidity 0.0 NTU 03/15/2017
Notes: ft/msl = feet above mean sea level
ft = feet
mg/L = milligrams per Liter
mV = millivolts
s.u. = Standard Units of pH
umhos/cm = micro-mhos per centimeter
Degrees C = degrees Centigrade
NTU = Nephelometric Turbidity Units
Piedmont Landfill and Recycling Center, Permit # 34-06 4 of 4 Joyce Engineering

APPENDIX A

LABORATORY ANALYTICAL REPORTS

Including Field Data Logs and Chains of Custody

ANALYTICAL REPORT
Job Number: 280-94905-1
Job Description: 134|Piedmont Landfill
For:
Waste Management
1850 Parkway Place
Suite 600
Marietta, GA 30067
Attention: Mr. Al Lacsamana
_____________________________________________
Approved for release.
Betsy A Sara
Project Manager II
3/30/2017 12:46 PM
Betsy A Sara, Project Manager II
4955 Yarrow Street, Arvada, CO, 80002
[phone]
[e-mail]
03/30/2017
cc:Mr. Van Burbach
The test results in this report relate only to the samples in this report and meet all requirements of NELAC, with any
exceptions noted. Pursuant to NELAP, this report shall not be reproduced except in full, without the written approval of
the laboratory. All questions regarding this report should be directed to the TestAmerica Denver Project Manager.

The Lab Certification ID# is 4025.

Reporting limits are adjusted for sample size used, dilutions and moisture content if applicable.
TestAmerica Laboratories, Inc.
TestAmerica Denver 4955 Yarrow Street, Arvada, CO 80002
Tel [phone] Fax [phone] www.testamericainc.com
03/30/2017Page 1 of 102
Table of Contents
Cover Title Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Report Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Executive Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
Method / Analyst Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12
Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13
Sample Datasheets . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .14
Data Qualifiers . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .64
QC Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .65
Qc Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .66
Surrogate Recovery Report . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .70
Qc Reports . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .71
Laboratory Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .81
Client Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .88
Sample Receipt Checklist . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .102
03/30/2017Page 2 of 102
CASE NARRATIVE
Client: Waste Management
Project: 134|Piedmont Landfill
Report Number: 280-94905-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
The reporting limits (RLs) in this report are North Carolina SWSLs.
Sample Receiving
The samples were received on 03/16/2017; the samples arrived in good condition, properly preserved and on ice. The temperature of the
cooler at receipt was 0.3 C.
Holding Times
The holding times were within established control limits.
Method Blanks
All Method Blanks were within established control limits.
Laboratory Control Samples (LCS)
All Laboratory Control Samples were within established control limits.
Matrix Spike and Matrix Spike Duplicate (MS/MSD)
All MS/MSD samples were within established control limits.
Metals
The Instrument Blank was above the upper control limit for Total Copper during Method 6020A analysis. Because the data are considered
to be biased high and Total Copper was not detected in the samples above the reporting limit, corrective action was deemed
unnecessary.
03/30/2017Page 3 of 102
EXECUTIVE SUMMARY - Detections
Client: Waste Management Job Number: 280-94905-1
Analyte Result
Reporting
Limit Units Method
Lab Sample ID Client Sample ID
Qualifier
280-94905-1 3406-MW09R
5.0 ug/L 8260B0.91 J1,1-Dichloroethane
ft/msl Field Sampling764.95Well Elevation
ft Field Sampling26.00Depth to water
ft/msl Field Sampling738.95Groundwater Elevation
SU Field Sampling6.24Field pH
umhos/cm Field Sampling343Field Conductivity
Degrees C Field Sampling13.7Field Temperature
NTU Field Sampling1.8Field Turbidity
mg/L Field Sampling2.7Field Dissolved Oxygen
millivolts Field Sampling17.7Field EH/ORP
Total Recoverable
100 ug/L 6010C11JBarium
10 ug/L 6010C0.69 JChromium
25 ug/L 6010C6.5 JVanadium
10 ug/L 6020A1.2 J ^Copper
10 ug/L 6020A2.4 JZinc
280-94905-2 3406-MW07
ft/msl Field Sampling771.57Well Elevation
ft Field Sampling24.80Depth to water
ft/msl Field Sampling746.77Groundwater Elevation
SU Field Sampling6.32Field pH
umhos/cm Field Sampling147Field Conductivity
Degrees C Field Sampling14.2Field Temperature
NTU Field Sampling6.0Field Turbidity
mg/L Field Sampling5.3Field Dissolved Oxygen
millivolts Field Sampling128.0Field EH/ORP
Total Recoverable
100 ug/L 6010C4.6 JBarium
10 ug/L 6010C1.1 JChromium
25 ug/L 6010C6.8 JVanadium
10 ug/L 6020A3.2 J ^Copper
10 ug/L 6020A2.9 JZinc
TestAmerica Denver 03/30/2017Page 4 of 102
EXECUTIVE SUMMARY - Detections
Client: Waste Management Job Number: 280-94905-1
Analyte Result
Reporting
Limit Units Method
Lab Sample ID Client Sample ID
Qualifier
280-94905-3 3406-MW11
ft/msl Field Sampling776.80Well Elevation
ft Field Sampling28.80Depth to water
ft/msl Field Sampling748.00Groundwater Elevation
SU Field Sampling5.71Field pH
umhos/cm Field Sampling185Field Conductivity
Degrees C Field Sampling13.8Field Temperature
NTU Field Sampling3.1Field Turbidity
mg/L Field Sampling2.2Field Dissolved Oxygen
millivolts Field Sampling156.0Field EH/ORP
Total Recoverable
100 ug/L 6010C66JBarium
25 ug/L 6010C1.2 JVanadium
10 ug/L 6020A0.70 J ^Copper
10 ug/L 6020A6.7 JZinc
280-94905-4 3406-MW05
ft/msl Field Sampling743.17Well Elevation
ft Field Sampling4.43Depth to water
ft/msl Field Sampling738.74Groundwater Elevation
SU Field Sampling6.00Field pH
umhos/cm Field Sampling349Field Conductivity
Degrees C Field Sampling13.3Field Temperature
NTU Field Sampling2.3Field Turbidity
mg/L Field Sampling1.1Field Dissolved Oxygen
millivolts Field Sampling168.0Field EH/ORP
Total Recoverable
100 ug/L 6010C39JBarium
10 ug/L 6010C8.0 JChromium
50 ug/L 6010C3.3 JNickel
25 ug/L 6010C6.3 JVanadium
TestAmerica Denver 03/30/2017Page 5 of 102
EXECUTIVE SUMMARY - Detections
Client: Waste Management Job Number: 280-94905-1
Analyte Result
Reporting
Limit Units Method
Lab Sample ID Client Sample ID
Qualifier
280-94905-5 3406-MW04
ft/msl Field Sampling756.92Well Elevation
ft Field Sampling12.94Depth to water
ft/msl Field Sampling743.98Groundwater Elevation
SU Field Sampling5.25Field pH
umhos/cm Field Sampling96Field Conductivity
Degrees C Field Sampling14.6Field Temperature
NTU Field Sampling6.5Field Turbidity
mg/L Field Sampling0.0Field Dissolved Oxygen
millivolts Field Sampling233Field EH/ORP
Total Recoverable
100 ug/L 6010C79JBarium
10 ug/L 6010C2.0 JCobalt
10 ug/L 6020A7.6 JZinc
280-94905-6 3406-MW12
ft/msl Field Sampling751.48Well Elevation
ft Field Sampling6.08Depth to water
ft/msl Field Sampling745.40Groundwater Elevation
SU Field Sampling5.88Field pH
umhos/cm Field Sampling141Field Conductivity
Degrees C Field Sampling12.9Field Temperature
NTU Field Sampling6.7Field Turbidity
mg/L Field Sampling1.5Field Dissolved Oxygen
millivolts Field Sampling96.2Field EH/ORP
Total Recoverable
100 ug/L 6010C23JBarium
10 ug/L 6010C2.0 JChromium
25 ug/L 6010C2.8 JVanadium
10 ug/L 6020A2.0 JZinc
TestAmerica Denver 03/30/2017Page 6 of 102
EXECUTIVE SUMMARY - Detections
Client: Waste Management Job Number: 280-94905-1
Analyte Result
Reporting
Limit Units Method
Lab Sample ID Client Sample ID
Qualifier
280-94905-7 3406-MW08
ft/msl Field Sampling748.95Well Elevation
ft Field Sampling5.82Depth to water
ft/msl Field Sampling743.13Groundwater Elevation
SU Field Sampling5.40Field pH
umhos/cm Field Sampling94Field Conductivity
Degrees C Field Sampling9.5Field Temperature
NTU Field Sampling7.9Field Turbidity
mg/L Field Sampling2.5Field Dissolved Oxygen
millivolts Field Sampling118.6Field EH/ORP
Total Recoverable
100 ug/L 6010C160Barium
10 ug/L 6020A2.9 J ^Copper
10 ug/L 6020A0.87 JSelenium
10 ug/L 6020A21Zinc
280-94905-8 3406-MW02
ft/msl Field Sampling778.04Well Elevation
ft Field Sampling29.14Depth to water
ft/msl Field Sampling748.90Groundwater Elevation
SU Field Sampling5.51Field pH
umhos/cm Field Sampling145Field Conductivity
Degrees C Field Sampling11.7Field Temperature
NTU Field Sampling1.5Field Turbidity
mg/L Field Sampling1.9Field Dissolved Oxygen
millivolts Field Sampling261.4Field EH/ORP
Total Recoverable
100 ug/L 6010C95JBarium
10 ug/L 6010C0.87 JChromium
TestAmerica Denver 03/30/2017Page 7 of 102
EXECUTIVE SUMMARY - Detections
Client: Waste Management Job Number: 280-94905-1
Analyte Result
Reporting
Limit Units Method
Lab Sample ID Client Sample ID
Qualifier
280-94905-9 3406-MW10
ft/msl Field Sampling777.20Well Elevation
ft Field Sampling31.07Depth to water
ft/msl Field Sampling746.13Groundwater Elevation
SU Field Sampling5.98Field pH
umhos/cm Field Sampling93Field Conductivity
Degrees C Field Sampling9.6Field Temperature
NTU Field Sampling6.8Field Turbidity
mg/L Field Sampling3.9Field Dissolved Oxygen
millivolts Field Sampling235.3Field EH/ORP
Total Recoverable
100 ug/L 6010C5.7 JBarium
10 ug/L 6010C7.8 JChromium
25 ug/L 6010C2.6 JVanadium
10 ug/L 6020A3.4 JZinc
280-94905-10 3406-MW03
5.0 ug/L 8260B0.33 J1,1-Dichloroethane
ft/msl Field Sampling770.08Well Elevation
ft Field Sampling25.57Depth to water
ft/msl Field Sampling744.51Groundwater Elevation
SU Field Sampling6.17Field pH
umhos/cm Field Sampling173Field Conductivity
Degrees C Field Sampling10.1Field Temperature
NTU Field Sampling3.4Field Turbidity
mg/L Field Sampling4.2Field Dissolved Oxygen
millivolts Field Sampling62.1Field EH/ORP
Total Recoverable
100 ug/L 6010C18JBarium
10 ug/L 6010C11Chromium
25 ug/L 6010C8.0 JVanadium
10 ug/L 6020A2.3 JZinc
TestAmerica Denver 03/30/2017Page 8 of 102
EXECUTIVE SUMMARY - Detections
Client: Waste Management Job Number: 280-94905-1
Analyte Result
Reporting
Limit Units Method
Lab Sample ID Client Sample ID
Qualifier
280-94905-11FB 3406-01FB
100 ug/L 8260B7.5 JAcetone
1.0 ug/L 8260B0.45 JEthylbenzene
1.0 ug/L 8260B5.5Styrene
1.0 ug/L 8260B0.50 JToluene
SU Field Sampling6.74Field pH
umhos/cm Field Sampling6Field Conductivity
Degrees C Field Sampling17.2Field Temperature
NTU Field Sampling0.0Field Turbidity
mg/L Field Sampling0.8Field Dissolved Oxygen
millivolts Field Sampling41.3Field EH/ORP
Total Recoverable
10 ug/L 6020A11Zinc
280-94905-12 3406-MW01
ft/msl Field Sampling823.93Well Elevation
ft Field Sampling44.38Depth to water
ft/msl Field Sampling779.55Groundwater Elevation
SU Field Sampling6.15Field pH
umhos/cm Field Sampling68Field Conductivity
Degrees C Field Sampling12.5Field Temperature
NTU Field Sampling3.4Field Turbidity
mg/L Field Sampling3.5Field Dissolved Oxygen
millivolts Field Sampling157.7Field EH/ORP
Total Recoverable
100 ug/L 6010C56JBarium
10 ug/L 6010C0.85 JChromium
TestAmerica Denver 03/30/2017Page 9 of 102
METHOD SUMMARY
Client: Waste Management Job Number: 280-94905-1
Preparation MethodMethodLab LocationDescription
Matrix:Water
Volatile Organic Compounds (GC/MS)TAL DEN SW846 8260B
Purge and Trap TAL DEN SW846 5030B
Metals (ICP)TAL DEN SW846 6010C
Preparation, Total Recoverable or Dissolved Metals TAL DEN SW846 3005A
Metals (ICP/MS)TAL DEN SW846 6020A
Preparation, Total Recoverable or Dissolved Metals TAL DEN SW846 3005A
Field Sampling TAL DEN EPA Field Sampling
Lab References:
TAL DEN = TestAmerica Denver
Method References:
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its
Updates.
TestAmerica Denver 03/30/2017Page 10 of 102
METHOD / ANALYST SUMMARY
Client: Waste Management Job Number: 280-94905-1
Method Analyst Analyst ID
Lines, Jeremy N JNLSW846 8260B
Broander, Laura L LLBSW846 6010C
Lackey, Cara M CMLSW846 6010C
Trudell, Lynn-Anne M LMTSW846 6020A
Krisorn, Chamaiporn 1 C1KEPA Field Sampling
TestAmerica Denver
03/30/2017Page 11 of 102
SAMPLE SUMMARY
Client: Waste Management Job Number: 280-94905-1
Client Sample IDLab Sample ID Client Matrix Sampled Received
Date/Time Date/Time
280-94905-1 3406-MW09R Water 03/15/2017 1157 03/16/2017 0855
280-94905-2 3406-MW07 Water 03/15/2017 1112 03/16/2017 0855
280-94905-3 3406-MW11 Water 03/15/2017 1020 03/16/2017 0855
280-94905-4 3406-MW05 Water 03/15/2017 0900 03/16/2017 0855
280-94905-5 3406-MW04 Water 03/15/2017 0816 03/16/2017 0855
280-94905-6 3406-MW12 Water 03/15/2017 0825 03/16/2017 0855
280-94905-7 3406-MW08 Water 03/15/2017 0952 03/16/2017 0855
280-94905-8 3406-MW02 Water 03/15/2017 1044 03/16/2017 0855
280-94905-9 3406-MW10 Water 03/15/2017 1115 03/16/2017 0855
280-94905-10 3406-MW03 Water 03/15/2017 1210 03/16/2017 0855
280-94905-11FB 3406-01FB Water 03/15/2017 1320 03/16/2017 0855
280-94905-12 3406-MW01 Water 03/15/2017 1300 03/16/2017 0855
280-94905-13TB TRIP BLANK Water 03/15/2017 0000 03/16/2017 0855
TestAmerica Denver 03/30/2017Page 12 of 102
SAMPLE RESULTS
TestAmerica Denver
03/30/2017Page 13 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW09R
Client Matrix:
280-94905-1
Water
Date Sampled: 03/15/2017 1157
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/23/2017 2214
03/23/2017 2214
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4626.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.211,1,1,2-Tetrachloroethane
ND 1.00.161,1,1-Trichloroethane
ND 3.00.211,1,2,2-Tetrachloroethane
ND 1.00.271,1,2-Trichloroethane
0.91 J 5.00.221,1-Dichloroethane
ND 5.00.231,1-Dichloroethene
ND 1.00.331,2,3-Trichloropropane
ND 130.471,2-Dibromo-3-Chloropropane
ND 1.00.181,2-Dibromoethane
ND 5.00.151,2-Dichlorobenzene
ND 1.00.131,2-Dichloroethane
ND 1.00.181,2-Dichloropropane
ND 1.00.161,4-Dichlorobenzene
ND 1002.02-Butanone (MEK)
ND 501.72-Hexanone
ND 1000.984-Methyl-2-pentanone (MIBK)
ND 1001.9Acetone
ND 2001.4Acrylonitrile
ND 1.00.16Benzene
ND 3.00.10Bromochloromethane
ND 1.00.17Bromodichloromethane
ND 3.00.19Bromoform
ND 100.21Bromomethane
ND 1000.45Carbon disulfide
ND 1.00.19Carbon tetrachloride
ND 3.00.17Chlorobenzene
ND 100.41Chloroethane
ND 5.00.16Chloroform
ND 1.00.30Chloromethane
ND 5.00.15cis-1,2-Dichloroethene
ND 1.00.16cis-1,3-Dichloropropene
ND 3.00.17Dibromochloromethane
ND 100.17Dibromomethane
ND 1.00.16Ethylbenzene
ND 100.23Iodomethane
ND 1.00.32Methylene Chloride
ND 1.00.17Styrene
ND 1.00.20Tetrachloroethene
ND 1.00.17Toluene
ND 5.00.15trans-1,2-Dichloroethene
ND 1.00.19trans-1,3-Dichloropropene
ND 1000.80trans-1,4-Dichloro-2-butene
ND 1.00.16Trichloroethene
ND 1.00.29Trichlorofluoromethane
ND 500.94Vinyl acetate
ND 1.00.10Vinyl chloride
TestAmerica Denver 03/30/2017Page 14 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW09R
Client Matrix:
280-94905-1
Water
Date Sampled: 03/15/2017 1157
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/23/2017 2214
03/23/2017 2214
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4626.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.19Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
114 70 - 1271,2-Dichloroethane-d4 (Surr)
105 78 - 1204-Bromofluorobenzene (Surr)
111 77 - 120Dibromofluoromethane (Surr)
106 80 - 125Toluene-d8 (Surr)
TestAmerica Denver 03/30/2017Page 15 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW07
Client Matrix:
280-94905-2
Water
Date Sampled: 03/15/2017 1112
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/24/2017 0044
03/24/2017 0044
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4633.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.211,1,1,2-Tetrachloroethane
ND 1.00.161,1,1-Trichloroethane
ND 3.00.211,1,2,2-Tetrachloroethane
ND 1.00.271,1,2-Trichloroethane
ND 5.00.221,1-Dichloroethane
ND 5.00.231,1-Dichloroethene
ND 1.00.331,2,3-Trichloropropane
ND 130.471,2-Dibromo-3-Chloropropane
ND 1.00.181,2-Dibromoethane
ND 5.00.151,2-Dichlorobenzene
ND 1.00.131,2-Dichloroethane
ND 1.00.181,2-Dichloropropane
ND 1.00.161,4-Dichlorobenzene
ND 1002.02-Butanone (MEK)
ND 501.72-Hexanone
ND 1000.984-Methyl-2-pentanone (MIBK)
ND 1001.9Acetone
ND 2001.4Acrylonitrile
ND 1.00.16Benzene
ND 3.00.10Bromochloromethane
ND 1.00.17Bromodichloromethane
ND 3.00.19Bromoform
ND 100.21Bromomethane
ND 1000.45Carbon disulfide
ND 1.00.19Carbon tetrachloride
ND 3.00.17Chlorobenzene
ND 100.41Chloroethane
ND 5.00.16Chloroform
ND 1.00.30Chloromethane
ND 5.00.15cis-1,2-Dichloroethene
ND 1.00.16cis-1,3-Dichloropropene
ND 3.00.17Dibromochloromethane
ND 100.17Dibromomethane
ND 1.00.16Ethylbenzene
ND 100.23Iodomethane
ND 1.00.32Methylene Chloride
ND 1.00.17Styrene
ND 1.00.20Tetrachloroethene
ND 1.00.17Toluene
ND 5.00.15trans-1,2-Dichloroethene
ND 1.00.19trans-1,3-Dichloropropene
ND 1000.80trans-1,4-Dichloro-2-butene
ND 1.00.16Trichloroethene
ND 1.00.29Trichlorofluoromethane
ND 500.94Vinyl acetate
ND 1.00.10Vinyl chloride
TestAmerica Denver 03/30/2017Page 16 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW07
Client Matrix:
280-94905-2
Water
Date Sampled: 03/15/2017 1112
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/24/2017 0044
03/24/2017 0044
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4633.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.19Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
119 70 - 1271,2-Dichloroethane-d4 (Surr)
103 78 - 1204-Bromofluorobenzene (Surr)
116 77 - 120Dibromofluoromethane (Surr)
108 80 - 125Toluene-d8 (Surr)
TestAmerica Denver 03/30/2017Page 17 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW11
Client Matrix:
280-94905-3
Water
Date Sampled: 03/15/2017 1020
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/24/2017 0106
03/24/2017 0106
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4634.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.211,1,1,2-Tetrachloroethane
ND 1.00.161,1,1-Trichloroethane
ND 3.00.211,1,2,2-Tetrachloroethane
ND 1.00.271,1,2-Trichloroethane
ND 5.00.221,1-Dichloroethane
ND 5.00.231,1-Dichloroethene
ND 1.00.331,2,3-Trichloropropane
ND 130.471,2-Dibromo-3-Chloropropane
ND 1.00.181,2-Dibromoethane
ND 5.00.151,2-Dichlorobenzene
ND 1.00.131,2-Dichloroethane
ND 1.00.181,2-Dichloropropane
ND 1.00.161,4-Dichlorobenzene
ND 1002.02-Butanone (MEK)
ND 501.72-Hexanone
ND 1000.984-Methyl-2-pentanone (MIBK)
ND 1001.9Acetone
ND 2001.4Acrylonitrile
ND 1.00.16Benzene
ND 3.00.10Bromochloromethane
ND 1.00.17Bromodichloromethane
ND 3.00.19Bromoform
ND 100.21Bromomethane
ND 1000.45Carbon disulfide
ND 1.00.19Carbon tetrachloride
ND 3.00.17Chlorobenzene
ND 100.41Chloroethane
ND 5.00.16Chloroform
ND 1.00.30Chloromethane
ND 5.00.15cis-1,2-Dichloroethene
ND 1.00.16cis-1,3-Dichloropropene
ND 3.00.17Dibromochloromethane
ND 100.17Dibromomethane
ND 1.00.16Ethylbenzene
ND 100.23Iodomethane
ND 1.00.32Methylene Chloride
ND 1.00.17Styrene
ND 1.00.20Tetrachloroethene
ND 1.00.17Toluene
ND 5.00.15trans-1,2-Dichloroethene
ND 1.00.19trans-1,3-Dichloropropene
ND 1000.80trans-1,4-Dichloro-2-butene
ND 1.00.16Trichloroethene
ND 1.00.29Trichlorofluoromethane
ND 500.94Vinyl acetate
ND 1.00.10Vinyl chloride
TestAmerica Denver 03/30/2017Page 18 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW11
Client Matrix:
280-94905-3
Water
Date Sampled: 03/15/2017 1020
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/24/2017 0106
03/24/2017 0106
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4634.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.19Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
123 70 - 1271,2-Dichloroethane-d4 (Surr)
103 78 - 1204-Bromofluorobenzene (Surr)
117 77 - 120Dibromofluoromethane (Surr)
107 80 - 125Toluene-d8 (Surr)
TestAmerica Denver 03/30/2017Page 19 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW05
Client Matrix:
280-94905-4
Water
Date Sampled: 03/15/2017 0900
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/24/2017 0127
03/24/2017 0127
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4635.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.211,1,1,2-Tetrachloroethane
ND 1.00.161,1,1-Trichloroethane
ND 3.00.211,1,2,2-Tetrachloroethane
ND 1.00.271,1,2-Trichloroethane
ND 5.00.221,1-Dichloroethane
ND 5.00.231,1-Dichloroethene
ND 1.00.331,2,3-Trichloropropane
ND 130.471,2-Dibromo-3-Chloropropane
ND 1.00.181,2-Dibromoethane
ND 5.00.151,2-Dichlorobenzene
ND 1.00.131,2-Dichloroethane
ND 1.00.181,2-Dichloropropane
ND 1.00.161,4-Dichlorobenzene
ND 1002.02-Butanone (MEK)
ND 501.72-Hexanone
ND 1000.984-Methyl-2-pentanone (MIBK)
ND 1001.9Acetone
ND 2001.4Acrylonitrile
ND 1.00.16Benzene
ND 3.00.10Bromochloromethane
ND 1.00.17Bromodichloromethane
ND 3.00.19Bromoform
ND 100.21Bromomethane
ND 1000.45Carbon disulfide
ND 1.00.19Carbon tetrachloride
ND 3.00.17Chlorobenzene
ND 100.41Chloroethane
ND 5.00.16Chloroform
ND 1.00.30Chloromethane
ND 5.00.15cis-1,2-Dichloroethene
ND 1.00.16cis-1,3-Dichloropropene
ND 3.00.17Dibromochloromethane
ND 100.17Dibromomethane
ND 1.00.16Ethylbenzene
ND 100.23Iodomethane
ND 1.00.32Methylene Chloride
ND 1.00.17Styrene
ND 1.00.20Tetrachloroethene
ND 1.00.17Toluene
ND 5.00.15trans-1,2-Dichloroethene
ND 1.00.19trans-1,3-Dichloropropene
ND 1000.80trans-1,4-Dichloro-2-butene
ND 1.00.16Trichloroethene
ND 1.00.29Trichlorofluoromethane
ND 500.94Vinyl acetate
ND 1.00.10Vinyl chloride
TestAmerica Denver 03/30/2017Page 20 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW05
Client Matrix:
280-94905-4
Water
Date Sampled: 03/15/2017 0900
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/24/2017 0127
03/24/2017 0127
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4635.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.19Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
116 70 - 1271,2-Dichloroethane-d4 (Surr)
98 78 - 1204-Bromofluorobenzene (Surr)
111 77 - 120Dibromofluoromethane (Surr)
102 80 - 125Toluene-d8 (Surr)
TestAmerica Denver 03/30/2017Page 21 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW04
Client Matrix:
280-94905-5
Water
Date Sampled: 03/15/2017 0816
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/24/2017 0149
03/24/2017 0149
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4636.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.211,1,1,2-Tetrachloroethane
ND 1.00.161,1,1-Trichloroethane
ND 3.00.211,1,2,2-Tetrachloroethane
ND 1.00.271,1,2-Trichloroethane
ND 5.00.221,1-Dichloroethane
ND 5.00.231,1-Dichloroethene
ND 1.00.331,2,3-Trichloropropane
ND 130.471,2-Dibromo-3-Chloropropane
ND 1.00.181,2-Dibromoethane
ND 5.00.151,2-Dichlorobenzene
ND 1.00.131,2-Dichloroethane
ND 1.00.181,2-Dichloropropane
ND 1.00.161,4-Dichlorobenzene
ND 1002.02-Butanone (MEK)
ND 501.72-Hexanone
ND 1000.984-Methyl-2-pentanone (MIBK)
ND 1001.9Acetone
ND 2001.4Acrylonitrile
ND 1.00.16Benzene
ND 3.00.10Bromochloromethane
ND 1.00.17Bromodichloromethane
ND 3.00.19Bromoform
ND 100.21Bromomethane
ND 1000.45Carbon disulfide
ND 1.00.19Carbon tetrachloride
ND 3.00.17Chlorobenzene
ND 100.41Chloroethane
ND 5.00.16Chloroform
ND 1.00.30Chloromethane
ND 5.00.15cis-1,2-Dichloroethene
ND 1.00.16cis-1,3-Dichloropropene
ND 3.00.17Dibromochloromethane
ND 100.17Dibromomethane
ND 1.00.16Ethylbenzene
ND 100.23Iodomethane
ND 1.00.32Methylene Chloride
ND 1.00.17Styrene
ND 1.00.20Tetrachloroethene
ND 1.00.17Toluene
ND 5.00.15trans-1,2-Dichloroethene
ND 1.00.19trans-1,3-Dichloropropene
ND 1000.80trans-1,4-Dichloro-2-butene
ND 1.00.16Trichloroethene
ND 1.00.29Trichlorofluoromethane
ND 500.94Vinyl acetate
ND 1.00.10Vinyl chloride
TestAmerica Denver 03/30/2017Page 22 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW04
Client Matrix:
280-94905-5
Water
Date Sampled: 03/15/2017 0816
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/24/2017 0149
03/24/2017 0149
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4636.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.19Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
122 70 - 1271,2-Dichloroethane-d4 (Surr)
103 78 - 1204-Bromofluorobenzene (Surr)
116 77 - 120Dibromofluoromethane (Surr)
107 80 - 125Toluene-d8 (Surr)
TestAmerica Denver 03/30/2017Page 23 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW12
Client Matrix:
280-94905-6
Water
Date Sampled: 03/15/2017 0825
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/24/2017 0210
03/24/2017 0210
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4637.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.211,1,1,2-Tetrachloroethane
ND 1.00.161,1,1-Trichloroethane
ND 3.00.211,1,2,2-Tetrachloroethane
ND 1.00.271,1,2-Trichloroethane
ND 5.00.221,1-Dichloroethane
ND 5.00.231,1-Dichloroethene
ND 1.00.331,2,3-Trichloropropane
ND 130.471,2-Dibromo-3-Chloropropane
ND 1.00.181,2-Dibromoethane
ND 5.00.151,2-Dichlorobenzene
ND 1.00.131,2-Dichloroethane
ND 1.00.181,2-Dichloropropane
ND 1.00.161,4-Dichlorobenzene
ND 1002.02-Butanone (MEK)
ND 501.72-Hexanone
ND 1000.984-Methyl-2-pentanone (MIBK)
ND 1001.9Acetone
ND 2001.4Acrylonitrile
ND 1.00.16Benzene
ND 3.00.10Bromochloromethane
ND 1.00.17Bromodichloromethane
ND 3.00.19Bromoform
ND 100.21Bromomethane
ND 1000.45Carbon disulfide
ND 1.00.19Carbon tetrachloride
ND 3.00.17Chlorobenzene
ND 100.41Chloroethane
ND 5.00.16Chloroform
ND 1.00.30Chloromethane
ND 5.00.15cis-1,2-Dichloroethene
ND 1.00.16cis-1,3-Dichloropropene
ND 3.00.17Dibromochloromethane
ND 100.17Dibromomethane
ND 1.00.16Ethylbenzene
ND 100.23Iodomethane
ND 1.00.32Methylene Chloride
ND 1.00.17Styrene
ND 1.00.20Tetrachloroethene
ND 1.00.17Toluene
ND 5.00.15trans-1,2-Dichloroethene
ND 1.00.19trans-1,3-Dichloropropene
ND 1000.80trans-1,4-Dichloro-2-butene
ND 1.00.16Trichloroethene
ND 1.00.29Trichlorofluoromethane
ND 500.94Vinyl acetate
ND 1.00.10Vinyl chloride
TestAmerica Denver 03/30/2017Page 24 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW12
Client Matrix:
280-94905-6
Water
Date Sampled: 03/15/2017 0825
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/24/2017 0210
03/24/2017 0210
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4637.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.19Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
123 70 - 1271,2-Dichloroethane-d4 (Surr)
105 78 - 1204-Bromofluorobenzene (Surr)
116 77 - 120Dibromofluoromethane (Surr)
106 80 - 125Toluene-d8 (Surr)
TestAmerica Denver 03/30/2017Page 25 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW08
Client Matrix:
280-94905-7
Water
Date Sampled: 03/15/2017 0952
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/24/2017 0231
03/24/2017 0231
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4638.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.211,1,1,2-Tetrachloroethane
ND 1.00.161,1,1-Trichloroethane
ND 3.00.211,1,2,2-Tetrachloroethane
ND 1.00.271,1,2-Trichloroethane
ND 5.00.221,1-Dichloroethane
ND 5.00.231,1-Dichloroethene
ND 1.00.331,2,3-Trichloropropane
ND 130.471,2-Dibromo-3-Chloropropane
ND 1.00.181,2-Dibromoethane
ND 5.00.151,2-Dichlorobenzene
ND 1.00.131,2-Dichloroethane
ND 1.00.181,2-Dichloropropane
ND 1.00.161,4-Dichlorobenzene
ND 1002.02-Butanone (MEK)
ND 501.72-Hexanone
ND 1000.984-Methyl-2-pentanone (MIBK)
ND 1001.9Acetone
ND 2001.4Acrylonitrile
ND 1.00.16Benzene
ND 3.00.10Bromochloromethane
ND 1.00.17Bromodichloromethane
ND 3.00.19Bromoform
ND 100.21Bromomethane
ND 1000.45Carbon disulfide
ND 1.00.19Carbon tetrachloride
ND 3.00.17Chlorobenzene
ND 100.41Chloroethane
ND 5.00.16Chloroform
ND 1.00.30Chloromethane
ND 5.00.15cis-1,2-Dichloroethene
ND 1.00.16cis-1,3-Dichloropropene
ND 3.00.17Dibromochloromethane
ND 100.17Dibromomethane
ND 1.00.16Ethylbenzene
ND 100.23Iodomethane
ND 1.00.32Methylene Chloride
ND 1.00.17Styrene
ND 1.00.20Tetrachloroethene
ND 1.00.17Toluene
ND 5.00.15trans-1,2-Dichloroethene
ND 1.00.19trans-1,3-Dichloropropene
ND 1000.80trans-1,4-Dichloro-2-butene
ND 1.00.16Trichloroethene
ND 1.00.29Trichlorofluoromethane
ND 500.94Vinyl acetate
ND 1.00.10Vinyl chloride
TestAmerica Denver 03/30/2017Page 26 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW08
Client Matrix:
280-94905-7
Water
Date Sampled: 03/15/2017 0952
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/24/2017 0231
03/24/2017 0231
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4638.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.19Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
124 70 - 1271,2-Dichloroethane-d4 (Surr)
101 78 - 1204-Bromofluorobenzene (Surr)
118 77 - 120Dibromofluoromethane (Surr)
107 80 - 125Toluene-d8 (Surr)
TestAmerica Denver 03/30/2017Page 27 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW02
Client Matrix:
280-94905-8
Water
Date Sampled: 03/15/2017 1044
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/24/2017 0253
03/24/2017 0253
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4639.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.211,1,1,2-Tetrachloroethane
ND 1.00.161,1,1-Trichloroethane
ND 3.00.211,1,2,2-Tetrachloroethane
ND 1.00.271,1,2-Trichloroethane
ND 5.00.221,1-Dichloroethane
ND 5.00.231,1-Dichloroethene
ND 1.00.331,2,3-Trichloropropane
ND 130.471,2-Dibromo-3-Chloropropane
ND 1.00.181,2-Dibromoethane
ND 5.00.151,2-Dichlorobenzene
ND 1.00.131,2-Dichloroethane
ND 1.00.181,2-Dichloropropane
ND 1.00.161,4-Dichlorobenzene
ND 1002.02-Butanone (MEK)
ND 501.72-Hexanone
ND 1000.984-Methyl-2-pentanone (MIBK)
ND 1001.9Acetone
ND 2001.4Acrylonitrile
ND 1.00.16Benzene
ND 3.00.10Bromochloromethane
ND 1.00.17Bromodichloromethane
ND 3.00.19Bromoform
ND 100.21Bromomethane
ND 1000.45Carbon disulfide
ND 1.00.19Carbon tetrachloride
ND 3.00.17Chlorobenzene
ND 100.41Chloroethane
ND 5.00.16Chloroform
ND 1.00.30Chloromethane
ND 5.00.15cis-1,2-Dichloroethene
ND 1.00.16cis-1,3-Dichloropropene
ND 3.00.17Dibromochloromethane
ND 100.17Dibromomethane
ND 1.00.16Ethylbenzene
ND 100.23Iodomethane
ND 1.00.32Methylene Chloride
ND 1.00.17Styrene
ND 1.00.20Tetrachloroethene
ND 1.00.17Toluene
ND 5.00.15trans-1,2-Dichloroethene
ND 1.00.19trans-1,3-Dichloropropene
ND 1000.80trans-1,4-Dichloro-2-butene
ND 1.00.16Trichloroethene
ND 1.00.29Trichlorofluoromethane
ND 500.94Vinyl acetate
ND 1.00.10Vinyl chloride
TestAmerica Denver 03/30/2017Page 28 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW02
Client Matrix:
280-94905-8
Water
Date Sampled: 03/15/2017 1044
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/24/2017 0253
03/24/2017 0253
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4639.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.19Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
98 70 - 1271,2-Dichloroethane-d4 (Surr)
96 78 - 1204-Bromofluorobenzene (Surr)
100 77 - 120Dibromofluoromethane (Surr)
105 80 - 125Toluene-d8 (Surr)
TestAmerica Denver 03/30/2017Page 29 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW10
Client Matrix:
280-94905-9
Water
Date Sampled: 03/15/2017 1115
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/24/2017 0314
03/24/2017 0314
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4640.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.211,1,1,2-Tetrachloroethane
ND 1.00.161,1,1-Trichloroethane
ND 3.00.211,1,2,2-Tetrachloroethane
ND 1.00.271,1,2-Trichloroethane
ND 5.00.221,1-Dichloroethane
ND 5.00.231,1-Dichloroethene
ND 1.00.331,2,3-Trichloropropane
ND 130.471,2-Dibromo-3-Chloropropane
ND 1.00.181,2-Dibromoethane
ND 5.00.151,2-Dichlorobenzene
ND 1.00.131,2-Dichloroethane
ND 1.00.181,2-Dichloropropane
ND 1.00.161,4-Dichlorobenzene
ND 1002.02-Butanone (MEK)
ND 501.72-Hexanone
ND 1000.984-Methyl-2-pentanone (MIBK)
ND 1001.9Acetone
ND 2001.4Acrylonitrile
ND 1.00.16Benzene
ND 3.00.10Bromochloromethane
ND 1.00.17Bromodichloromethane
ND 3.00.19Bromoform
ND 100.21Bromomethane
ND 1000.45Carbon disulfide
ND 1.00.19Carbon tetrachloride
ND 3.00.17Chlorobenzene
ND 100.41Chloroethane
ND 5.00.16Chloroform
ND 1.00.30Chloromethane
ND 5.00.15cis-1,2-Dichloroethene
ND 1.00.16cis-1,3-Dichloropropene
ND 3.00.17Dibromochloromethane
ND 100.17Dibromomethane
ND 1.00.16Ethylbenzene
ND 100.23Iodomethane
ND 1.00.32Methylene Chloride
ND 1.00.17Styrene
ND 1.00.20Tetrachloroethene
ND 1.00.17Toluene
ND 5.00.15trans-1,2-Dichloroethene
ND 1.00.19trans-1,3-Dichloropropene
ND 1000.80trans-1,4-Dichloro-2-butene
ND 1.00.16Trichloroethene
ND 1.00.29Trichlorofluoromethane
ND 500.94Vinyl acetate
ND 1.00.10Vinyl chloride
TestAmerica Denver 03/30/2017Page 30 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW10
Client Matrix:
280-94905-9
Water
Date Sampled: 03/15/2017 1115
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/24/2017 0314
03/24/2017 0314
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4640.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.19Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
109 70 - 1271,2-Dichloroethane-d4 (Surr)
94 78 - 1204-Bromofluorobenzene (Surr)
106 77 - 120Dibromofluoromethane (Surr)
99 80 - 125Toluene-d8 (Surr)
TestAmerica Denver 03/30/2017Page 31 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW03
Client Matrix:
280-94905-10
Water
Date Sampled: 03/15/2017 1210
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/24/2017 0336
03/24/2017 0336
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4641.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.211,1,1,2-Tetrachloroethane
ND 1.00.161,1,1-Trichloroethane
ND 3.00.211,1,2,2-Tetrachloroethane
ND 1.00.271,1,2-Trichloroethane
0.33 J 5.00.221,1-Dichloroethane
ND 5.00.231,1-Dichloroethene
ND 1.00.331,2,3-Trichloropropane
ND 130.471,2-Dibromo-3-Chloropropane
ND 1.00.181,2-Dibromoethane
ND 5.00.151,2-Dichlorobenzene
ND 1.00.131,2-Dichloroethane
ND 1.00.181,2-Dichloropropane
ND 1.00.161,4-Dichlorobenzene
ND 1002.02-Butanone (MEK)
ND 501.72-Hexanone
ND 1000.984-Methyl-2-pentanone (MIBK)
ND 1001.9Acetone
ND 2001.4Acrylonitrile
ND 1.00.16Benzene
ND 3.00.10Bromochloromethane
ND 1.00.17Bromodichloromethane
ND 3.00.19Bromoform
ND 100.21Bromomethane
ND 1000.45Carbon disulfide
ND 1.00.19Carbon tetrachloride
ND 3.00.17Chlorobenzene
ND 100.41Chloroethane
ND 5.00.16Chloroform
ND 1.00.30Chloromethane
ND 5.00.15cis-1,2-Dichloroethene
ND 1.00.16cis-1,3-Dichloropropene
ND 3.00.17Dibromochloromethane
ND 100.17Dibromomethane
ND 1.00.16Ethylbenzene
ND 100.23Iodomethane
ND 1.00.32Methylene Chloride
ND 1.00.17Styrene
ND 1.00.20Tetrachloroethene
ND 1.00.17Toluene
ND 5.00.15trans-1,2-Dichloroethene
ND 1.00.19trans-1,3-Dichloropropene
ND 1000.80trans-1,4-Dichloro-2-butene
ND 1.00.16Trichloroethene
ND 1.00.29Trichlorofluoromethane
ND 500.94Vinyl acetate
ND 1.00.10Vinyl chloride
TestAmerica Denver 03/30/2017Page 32 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW03
Client Matrix:
280-94905-10
Water
Date Sampled: 03/15/2017 1210
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/24/2017 0336
03/24/2017 0336
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4641.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.19Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
112 70 - 1271,2-Dichloroethane-d4 (Surr)
94 78 - 1204-Bromofluorobenzene (Surr)
107 77 - 120Dibromofluoromethane (Surr)
97 80 - 125Toluene-d8 (Surr)
TestAmerica Denver 03/30/2017Page 33 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-01FB
Client Matrix:
280-94905-11FB
Water
Date Sampled: 03/15/2017 1320
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/24/2017 0357
03/24/2017 0357
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4642.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.211,1,1,2-Tetrachloroethane
ND 1.00.161,1,1-Trichloroethane
ND 3.00.211,1,2,2-Tetrachloroethane
ND 1.00.271,1,2-Trichloroethane
ND 5.00.221,1-Dichloroethane
ND 5.00.231,1-Dichloroethene
ND 1.00.331,2,3-Trichloropropane
ND 130.471,2-Dibromo-3-Chloropropane
ND 1.00.181,2-Dibromoethane
ND 5.00.151,2-Dichlorobenzene
ND 1.00.131,2-Dichloroethane
ND 1.00.181,2-Dichloropropane
ND 1.00.161,4-Dichlorobenzene
ND 1002.02-Butanone (MEK)
ND 501.72-Hexanone
ND 1000.984-Methyl-2-pentanone (MIBK)
7.5 J 1001.9Acetone
ND 2001.4Acrylonitrile
ND 1.00.16Benzene
ND 3.00.10Bromochloromethane
ND 1.00.17Bromodichloromethane
ND 3.00.19Bromoform
ND 100.21Bromomethane
ND 1000.45Carbon disulfide
ND 1.00.19Carbon tetrachloride
ND 3.00.17Chlorobenzene
ND 100.41Chloroethane
ND 5.00.16Chloroform
ND 1.00.30Chloromethane
ND 5.00.15cis-1,2-Dichloroethene
ND 1.00.16cis-1,3-Dichloropropene
ND 3.00.17Dibromochloromethane
ND 100.17Dibromomethane
0.45 J 1.00.16Ethylbenzene
ND 100.23Iodomethane
ND 1.00.32Methylene Chloride
5.5 1.00.17Styrene
ND 1.00.20Tetrachloroethene
0.50 J 1.00.17Toluene
ND 5.00.15trans-1,2-Dichloroethene
ND 1.00.19trans-1,3-Dichloropropene
ND 1000.80trans-1,4-Dichloro-2-butene
ND 1.00.16Trichloroethene
ND 1.00.29Trichlorofluoromethane
ND 500.94Vinyl acetate
ND 1.00.10Vinyl chloride
TestAmerica Denver 03/30/2017Page 34 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-01FB
Client Matrix:
280-94905-11FB
Water
Date Sampled: 03/15/2017 1320
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/24/2017 0357
03/24/2017 0357
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4642.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.19Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
113 70 - 1271,2-Dichloroethane-d4 (Surr)
94 78 - 1204-Bromofluorobenzene (Surr)
106 77 - 120Dibromofluoromethane (Surr)
95 80 - 125Toluene-d8 (Surr)
TestAmerica Denver 03/30/2017Page 35 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW01
Client Matrix:
280-94905-12
Water
Date Sampled: 03/15/2017 1300
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/24/2017 0419
03/24/2017 0419
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4643.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.211,1,1,2-Tetrachloroethane
ND 1.00.161,1,1-Trichloroethane
ND 3.00.211,1,2,2-Tetrachloroethane
ND 1.00.271,1,2-Trichloroethane
ND 5.00.221,1-Dichloroethane
ND 5.00.231,1-Dichloroethene
ND 1.00.331,2,3-Trichloropropane
ND 130.471,2-Dibromo-3-Chloropropane
ND 1.00.181,2-Dibromoethane
ND 5.00.151,2-Dichlorobenzene
ND 1.00.131,2-Dichloroethane
ND 1.00.181,2-Dichloropropane
ND 1.00.161,4-Dichlorobenzene
ND 1002.02-Butanone (MEK)
ND 501.72-Hexanone
ND 1000.984-Methyl-2-pentanone (MIBK)
ND 1001.9Acetone
ND 2001.4Acrylonitrile
ND 1.00.16Benzene
ND 3.00.10Bromochloromethane
ND 1.00.17Bromodichloromethane
ND 3.00.19Bromoform
ND 100.21Bromomethane
ND 1000.45Carbon disulfide
ND 1.00.19Carbon tetrachloride
ND 3.00.17Chlorobenzene
ND 100.41Chloroethane
ND 5.00.16Chloroform
ND 1.00.30Chloromethane
ND 5.00.15cis-1,2-Dichloroethene
ND 1.00.16cis-1,3-Dichloropropene
ND 3.00.17Dibromochloromethane
ND 100.17Dibromomethane
ND 1.00.16Ethylbenzene
ND 100.23Iodomethane
ND 1.00.32Methylene Chloride
ND 1.00.17Styrene
ND 1.00.20Tetrachloroethene
ND 1.00.17Toluene
ND 5.00.15trans-1,2-Dichloroethene
ND 1.00.19trans-1,3-Dichloropropene
ND 1000.80trans-1,4-Dichloro-2-butene
ND 1.00.16Trichloroethene
ND 1.00.29Trichlorofluoromethane
ND 500.94Vinyl acetate
ND 1.00.10Vinyl chloride
TestAmerica Denver 03/30/2017Page 36 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW01
Client Matrix:
280-94905-12
Water
Date Sampled: 03/15/2017 1300
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/24/2017 0419
03/24/2017 0419
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4643.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.19Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
121 70 - 1271,2-Dichloroethane-d4 (Surr)
103 78 - 1204-Bromofluorobenzene (Surr)
115 77 - 120Dibromofluoromethane (Surr)
108 80 - 125Toluene-d8 (Surr)
TestAmerica Denver 03/30/2017Page 37 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
TRIP BLANK
Client Matrix:
280-94905-13TB
Water
Date Sampled: 03/15/2017 0000
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/24/2017 0440
03/24/2017 0440
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4644.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.211,1,1,2-Tetrachloroethane
ND 1.00.161,1,1-Trichloroethane
ND 3.00.211,1,2,2-Tetrachloroethane
ND 1.00.271,1,2-Trichloroethane
ND 5.00.221,1-Dichloroethane
ND 5.00.231,1-Dichloroethene
ND 1.00.331,2,3-Trichloropropane
ND 130.471,2-Dibromo-3-Chloropropane
ND 1.00.181,2-Dibromoethane
ND 5.00.151,2-Dichlorobenzene
ND 1.00.131,2-Dichloroethane
ND 1.00.181,2-Dichloropropane
ND 1.00.161,4-Dichlorobenzene
ND 1002.02-Butanone (MEK)
ND 501.72-Hexanone
ND 1000.984-Methyl-2-pentanone (MIBK)
ND 1001.9Acetone
ND 2001.4Acrylonitrile
ND 1.00.16Benzene
ND 3.00.10Bromochloromethane
ND 1.00.17Bromodichloromethane
ND 3.00.19Bromoform
ND 100.21Bromomethane
ND 1000.45Carbon disulfide
ND 1.00.19Carbon tetrachloride
ND 3.00.17Chlorobenzene
ND 100.41Chloroethane
ND 5.00.16Chloroform
ND 1.00.30Chloromethane
ND 5.00.15cis-1,2-Dichloroethene
ND 1.00.16cis-1,3-Dichloropropene
ND 3.00.17Dibromochloromethane
ND 100.17Dibromomethane
ND 1.00.16Ethylbenzene
ND 100.23Iodomethane
ND 1.00.32Methylene Chloride
ND 1.00.17Styrene
ND 1.00.20Tetrachloroethene
ND 1.00.17Toluene
ND 5.00.15trans-1,2-Dichloroethene
ND 1.00.19trans-1,3-Dichloropropene
ND 1000.80trans-1,4-Dichloro-2-butene
ND 1.00.16Trichloroethene
ND 1.00.29Trichlorofluoromethane
ND 500.94Vinyl acetate
ND 1.00.10Vinyl chloride
TestAmerica Denver 03/30/2017Page 38 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
TRIP BLANK
Client Matrix:
280-94905-13TB
Water
Date Sampled: 03/15/2017 0000
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/24/2017 0440
03/24/2017 0440
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4644.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.19Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
108 70 - 1271,2-Dichloroethane-d4 (Surr)
105 78 - 1204-Bromofluorobenzene (Surr)
109 77 - 120Dibromofluoromethane (Surr)
112 80 - 125Toluene-d8 (Surr)
TestAmerica Denver 03/30/2017Page 39 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW09R
Client Matrix:
280-94905-1
Water
Date Sampled: 03/15/2017 1157
Date Received: 03/16/2017 0855
6010C Metals (ICP)-Total Recoverable
6010C Instrument ID:
Lab File ID:51a032417.csv
Dilution:1.0 Initial Weight/Volume:50 mL
03/24/2017 2356 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_051
Analysis Date:
Prep Date:
Analysis Batch:280-366869
280-366366Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
11 J 1000.82Barium
0.69 J 100.66Chromium
ND 101.2Cobalt
ND 502.6Nickel
ND 100.93Silver
6010C Instrument ID:
Lab File ID:51a032717.csv
Dilution:1.0 Initial Weight/Volume:50 mL
03/27/2017 2358 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_051
Analysis Date:
Prep Date:
Analysis Batch:280-367053
280-366366Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 1.00.47Beryllium
ND 102.7Lead
6.5 J 251.1Vanadium
6020A Metals (ICP/MS)-Total Recoverable
6020A Instrument ID:
Lab File ID:219SMPL_li032417.D
Dilution:1.0 Initial Weight/Volume:50 mL
03/25/2017 0213 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_077
Analysis Date:
Prep Date:
Analysis Batch:280-366863
280-366367Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 6.00.40Antimony
ND 100.33Arsenic
ND 1.00.27Cadmium
1.2 J ^100.56Copper
ND 100.70Selenium
ND 5.50.050Thallium
2.4 J 102.0Zinc
TestAmerica Denver 03/30/2017Page 40 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW07
Client Matrix:
280-94905-2
Water
Date Sampled: 03/15/2017 1112
Date Received: 03/16/2017 0855
6010C Metals (ICP)-Total Recoverable
6010C Instrument ID:
Lab File ID:51a032417.csv
Dilution:1.0 Initial Weight/Volume:50 mL
03/25/2017 0039 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_051
Analysis Date:
Prep Date:
Analysis Batch:280-366869
280-366366Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
4.6 J 1000.82Barium
1.1 J 100.66Chromium
ND 101.2Cobalt
ND 502.6Nickel
ND 100.93Silver
6010C Instrument ID:
Lab File ID:51a032717.csv
Dilution:1.0 Initial Weight/Volume:50 mL
03/28/2017 0052 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_051
Analysis Date:
Prep Date:
Analysis Batch:280-367053
280-366366Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 1.00.47Beryllium
ND 102.7Lead
6.8 J 251.1Vanadium
6020A Metals (ICP/MS)-Total Recoverable
6020A Instrument ID:
Lab File ID:222SMPL_li032417.D
Dilution:1.0 Initial Weight/Volume:50 mL
03/25/2017 0224 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_077
Analysis Date:
Prep Date:
Analysis Batch:280-366863
280-366367Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 6.00.40Antimony
ND 100.33Arsenic
ND 1.00.27Cadmium
3.2 J ^100.56Copper
ND 100.70Selenium
ND 5.50.050Thallium
2.9 J 102.0Zinc
TestAmerica Denver 03/30/2017Page 41 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW11
Client Matrix:
280-94905-3
Water
Date Sampled: 03/15/2017 1020
Date Received: 03/16/2017 0855
6010C Metals (ICP)-Total Recoverable
6010C Instrument ID:
Lab File ID:51a032417.csv
Dilution:1.0 Initial Weight/Volume:50 mL
03/24/2017 2359 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_051
Analysis Date:
Prep Date:
Analysis Batch:280-366869
280-366366Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
66 J 1000.82Barium
ND 100.66Chromium
ND 101.2Cobalt
ND 502.6Nickel
ND 100.93Silver
6010C Instrument ID:
Lab File ID:51a032717.csv
Dilution:1.0 Initial Weight/Volume:50 mL
03/28/2017 0012 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_051
Analysis Date:
Prep Date:
Analysis Batch:280-367053
280-366366Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 1.00.47Beryllium
ND 102.7Lead
1.2 J 251.1Vanadium
6020A Metals (ICP/MS)-Total Recoverable
6020A Instrument ID:
Lab File ID:223SMPL_li032417.D
Dilution:1.0 Initial Weight/Volume:50 mL
03/25/2017 0228 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_077
Analysis Date:
Prep Date:
Analysis Batch:280-366863
280-366367Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 6.00.40Antimony
ND 100.33Arsenic
ND 1.00.27Cadmium
0.70 J ^100.56Copper
ND 100.70Selenium
ND 5.50.050Thallium
6.7 J 102.0Zinc
TestAmerica Denver 03/30/2017Page 42 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW05
Client Matrix:
280-94905-4
Water
Date Sampled: 03/15/2017 0900
Date Received: 03/16/2017 0855
6010C Metals (ICP)-Total Recoverable
6010C Instrument ID:
Lab File ID:51a032417.csv
Dilution:1.0 Initial Weight/Volume:50 mL
03/25/2017 0002 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_051
Analysis Date:
Prep Date:
Analysis Batch:280-366869
280-366366Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
39 J 1000.82Barium
8.0 J 100.66Chromium
ND 101.2Cobalt
3.3 J 502.6Nickel
ND 100.93Silver
6010C Instrument ID:
Lab File ID:51a032717.csv
Dilution:1.0 Initial Weight/Volume:50 mL
03/28/2017 0015 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_051
Analysis Date:
Prep Date:
Analysis Batch:280-367053
280-366366Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 1.00.47Beryllium
ND 102.7Lead
6.3 J 251.1Vanadium
6020A Metals (ICP/MS)-Total Recoverable
6020A Instrument ID:
Lab File ID:224SMPL_li032417.D
Dilution:1.0 Initial Weight/Volume:50 mL
03/25/2017 0231 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_077
Analysis Date:
Prep Date:
Analysis Batch:280-366863
280-366367Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 6.00.40Antimony
ND 100.33Arsenic
ND 1.00.27Cadmium
ND 100.56Copper
ND 100.70Selenium
ND 5.50.050Thallium
ND 102.0Zinc
TestAmerica Denver 03/30/2017Page 43 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW04
Client Matrix:
280-94905-5
Water
Date Sampled: 03/15/2017 0816
Date Received: 03/16/2017 0855
6010C Metals (ICP)-Total Recoverable
6010C Instrument ID:
Lab File ID:51a032417.csv
Dilution:1.0 Initial Weight/Volume:50 mL
03/25/2017 0005 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_051
Analysis Date:
Prep Date:
Analysis Batch:280-366869
280-366366Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
79 J 1000.82Barium
ND 100.66Chromium
2.0 J 101.2Cobalt
ND 502.6Nickel
ND 100.93Silver
6010C Instrument ID:
Lab File ID:51a032717.csv
Dilution:1.0 Initial Weight/Volume:50 mL
03/28/2017 0018 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_051
Analysis Date:
Prep Date:
Analysis Batch:280-367053
280-366366Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 1.00.47Beryllium
ND 102.7Lead
ND 251.1Vanadium
6020A Metals (ICP/MS)-Total Recoverable
6020A Instrument ID:
Lab File ID:228SMPL_li032417.D
Dilution:1.0 Initial Weight/Volume:50 mL
03/25/2017 0247 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_077
Analysis Date:
Prep Date:
Analysis Batch:280-366863
280-366367Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 6.00.40Antimony
ND 100.33Arsenic
ND 1.00.27Cadmium
ND 100.56Copper
ND 100.70Selenium
ND 5.50.050Thallium
7.6 J 102.0Zinc
TestAmerica Denver 03/30/2017Page 44 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW12
Client Matrix:
280-94905-6
Water
Date Sampled: 03/15/2017 0825
Date Received: 03/16/2017 0855
6010C Metals (ICP)-Total Recoverable
6010C Instrument ID:
Lab File ID:51a032417.csv
Dilution:1.0 Initial Weight/Volume:50 mL
03/25/2017 0008 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_051
Analysis Date:
Prep Date:
Analysis Batch:280-366869
280-366366Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
23 J 1000.82Barium
2.0 J 100.66Chromium
ND 101.2Cobalt
ND 502.6Nickel
ND 100.93Silver
6010C Instrument ID:
Lab File ID:51a032717.csv
Dilution:1.0 Initial Weight/Volume:50 mL
03/28/2017 0021 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_051
Analysis Date:
Prep Date:
Analysis Batch:280-367053
280-366366Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 1.00.47Beryllium
ND 102.7Lead
2.8 J 251.1Vanadium
6020A Metals (ICP/MS)-Total Recoverable
6020A Instrument ID:
Lab File ID:229SMPL_li032417.D
Dilution:1.0 Initial Weight/Volume:50 mL
03/25/2017 0250 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_077
Analysis Date:
Prep Date:
Analysis Batch:280-366863
280-366367Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 6.00.40Antimony
ND 100.33Arsenic
ND 1.00.27Cadmium
ND 100.56Copper
ND 100.70Selenium
ND 5.50.050Thallium
2.0 J 102.0Zinc
TestAmerica Denver 03/30/2017Page 45 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW08
Client Matrix:
280-94905-7
Water
Date Sampled: 03/15/2017 0952
Date Received: 03/16/2017 0855
6010C Metals (ICP)-Total Recoverable
6010C Instrument ID:
Lab File ID:51a032417.csv
Dilution:1.0 Initial Weight/Volume:50 mL
03/25/2017 0013 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_051
Analysis Date:
Prep Date:
Analysis Batch:280-366869
280-366366Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
160 1000.82Barium
ND 100.66Chromium
ND 101.2Cobalt
ND 502.6Nickel
ND 100.93Silver
6010C Instrument ID:
Lab File ID:51a032717.csv
Dilution:1.0 Initial Weight/Volume:50 mL
03/28/2017 0023 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_051
Analysis Date:
Prep Date:
Analysis Batch:280-367053
280-366366Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 1.00.47Beryllium
ND 102.7Lead
ND 251.1Vanadium
6020A Metals (ICP/MS)-Total Recoverable
6020A Instrument ID:
Lab File ID:230SMPL_li032417.D
Dilution:1.0 Initial Weight/Volume:50 mL
03/25/2017 0254 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_077
Analysis Date:
Prep Date:
Analysis Batch:280-366863
280-366367Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 6.00.40Antimony
ND 100.33Arsenic
ND 1.00.27Cadmium
2.9 J ^100.56Copper
0.87 J 100.70Selenium
ND 5.50.050Thallium
21 102.0Zinc
TestAmerica Denver 03/30/2017Page 46 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW02
Client Matrix:
280-94905-8
Water
Date Sampled: 03/15/2017 1044
Date Received: 03/16/2017 0855
6010C Metals (ICP)-Total Recoverable
6010C Instrument ID:
Lab File ID:51a032417.csv
Dilution:1.0 Initial Weight/Volume:50 mL
03/25/2017 0025 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_051
Analysis Date:
Prep Date:
Analysis Batch:280-366869
280-366366Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
95 J 1000.82Barium
0.87 J 100.66Chromium
ND 101.2Cobalt
ND 502.6Nickel
ND 100.93Silver
6010C Instrument ID:
Lab File ID:51a032717.csv
Dilution:1.0 Initial Weight/Volume:50 mL
03/28/2017 0026 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_051
Analysis Date:
Prep Date:
Analysis Batch:280-367053
280-366366Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 1.00.47Beryllium
ND 102.7Lead
ND 251.1Vanadium
6020A Metals (ICP/MS)-Total Recoverable
6020A Instrument ID:
Lab File ID:231SMPL_li032417.D
Dilution:1.0 Initial Weight/Volume:50 mL
03/25/2017 0258 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_077
Analysis Date:
Prep Date:
Analysis Batch:280-366863
280-366367Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 6.00.40Antimony
ND 100.33Arsenic
ND 1.00.27Cadmium
ND 100.56Copper
ND 100.70Selenium
ND 5.50.050Thallium
ND 102.0Zinc
TestAmerica Denver 03/30/2017Page 47 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW10
Client Matrix:
280-94905-9
Water
Date Sampled: 03/15/2017 1115
Date Received: 03/16/2017 0855
6010C Metals (ICP)-Total Recoverable
6010C Instrument ID:
Lab File ID:51a032417.csv
Dilution:1.0 Initial Weight/Volume:50 mL
03/25/2017 0028 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_051
Analysis Date:
Prep Date:
Analysis Batch:280-366869
280-366366Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
5.7 J 1000.82Barium
7.8 J 100.66Chromium
ND 101.2Cobalt
ND 502.6Nickel
ND 100.93Silver
6010C Instrument ID:
Lab File ID:51a032717.csv
Dilution:1.0 Initial Weight/Volume:50 mL
03/28/2017 0029 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_051
Analysis Date:
Prep Date:
Analysis Batch:280-367053
280-366366Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 1.00.47Beryllium
ND 102.7Lead
2.6 J 251.1Vanadium
6020A Metals (ICP/MS)-Total Recoverable
6020A Instrument ID:
Lab File ID:232SMPL_li032417.D
Dilution:1.0 Initial Weight/Volume:50 mL
03/25/2017 0302 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_077
Analysis Date:
Prep Date:
Analysis Batch:280-366863
280-366367Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 6.00.40Antimony
ND 100.33Arsenic
ND 1.00.27Cadmium
ND 100.56Copper
ND 100.70Selenium
ND 5.50.050Thallium
3.4 J 102.0Zinc
TestAmerica Denver 03/30/2017Page 48 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW03
Client Matrix:
280-94905-10
Water
Date Sampled: 03/15/2017 1210
Date Received: 03/16/2017 0855
6010C Metals (ICP)-Total Recoverable
6010C Instrument ID:
Lab File ID:51a032417.csv
Dilution:1.0 Initial Weight/Volume:50 mL
03/25/2017 0031 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_051
Analysis Date:
Prep Date:
Analysis Batch:280-366869
280-366366Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
18 J 1000.82Barium
11 100.66Chromium
ND 101.2Cobalt
ND 502.6Nickel
ND 100.93Silver
6010C Instrument ID:
Lab File ID:51a032717.csv
Dilution:1.0 Initial Weight/Volume:50 mL
03/28/2017 0032 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_051
Analysis Date:
Prep Date:
Analysis Batch:280-367053
280-366366Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 1.00.47Beryllium
ND 102.7Lead
8.0 J 251.1Vanadium
6020A Metals (ICP/MS)-Total Recoverable
6020A Instrument ID:
Lab File ID:233SMPL_li032417.D
Dilution:1.0 Initial Weight/Volume:50 mL
03/25/2017 0305 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_077
Analysis Date:
Prep Date:
Analysis Batch:280-366863
280-366367Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 6.00.40Antimony
ND 100.33Arsenic
ND 1.00.27Cadmium
ND 100.56Copper
ND 100.70Selenium
ND 5.50.050Thallium
2.3 J 102.0Zinc
TestAmerica Denver 03/30/2017Page 49 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-01FB
Client Matrix:
280-94905-11FB
Water
Date Sampled: 03/15/2017 1320
Date Received: 03/16/2017 0855
6010C Metals (ICP)-Total Recoverable
6010C Instrument ID:
Lab File ID:51a032417.csv
Dilution:1.0 Initial Weight/Volume:50 mL
03/25/2017 0034 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_051
Analysis Date:
Prep Date:
Analysis Batch:280-366869
280-366366Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 1000.82Barium
ND 100.66Chromium
ND 101.2Cobalt
ND 502.6Nickel
ND 100.93Silver
6010C Instrument ID:
Lab File ID:51a032717.csv
Dilution:1.0 Initial Weight/Volume:50 mL
03/28/2017 0035 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_051
Analysis Date:
Prep Date:
Analysis Batch:280-367053
280-366366Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 1.00.47Beryllium
ND 102.7Lead
ND 251.1Vanadium
6020A Metals (ICP/MS)-Total Recoverable
6020A Instrument ID:
Lab File ID:234SMPL_li032417.D
Dilution:1.0 Initial Weight/Volume:50 mL
03/25/2017 0309 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_077
Analysis Date:
Prep Date:
Analysis Batch:280-366863
280-366367Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 6.00.40Antimony
ND 100.33Arsenic
ND 1.00.27Cadmium
ND 100.56Copper
ND 100.70Selenium
ND 5.50.050Thallium
11 102.0Zinc
TestAmerica Denver 03/30/2017Page 50 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Client Sample ID:
Lab Sample ID:
3406-MW01
Client Matrix:
280-94905-12
Water
Date Sampled: 03/15/2017 1300
Date Received: 03/16/2017 0855
6010C Metals (ICP)-Total Recoverable
6010C Instrument ID:
Lab File ID:51a032417.csv
Dilution:1.0 Initial Weight/Volume:50 mL
03/25/2017 0037 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_051
Analysis Date:
Prep Date:
Analysis Batch:280-366869
280-366366Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
56 J 1000.82Barium
0.85 J 100.66Chromium
ND 101.2Cobalt
ND 502.6Nickel
ND 100.93Silver
6010C Instrument ID:
Lab File ID:51a032717.csv
Dilution:1.0 Initial Weight/Volume:50 mL
03/28/2017 0038 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_051
Analysis Date:
Prep Date:
Analysis Batch:280-367053
280-366366Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 1.00.47Beryllium
ND 102.7Lead
ND 251.1Vanadium
6020A Metals (ICP/MS)-Total Recoverable
6020A Instrument ID:
Lab File ID:235SMPL_li032417.D
Dilution:1.0 Initial Weight/Volume:50 mL
03/25/2017 0313 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_077
Analysis Date:
Prep Date:
Analysis Batch:280-366863
280-366367Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 6.00.40Antimony
ND 100.33Arsenic
ND 1.00.27Cadmium
ND 100.56Copper
ND 100.70Selenium
ND 5.50.050Thallium
ND 102.0Zinc
TestAmerica Denver 03/30/2017Page 51 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Field Service / Mobile Lab
Client Sample ID:
Lab Sample ID:
3406-MW09R
Client Matrix:
280-94905-1
Water
Date Sampled: 03/15/2017 1157
Date Received: 03/16/2017 0855
Result Qual Units Dil Method
Analysis Date Analyzed
Date PreparedAnalyteBatch
Well Elevation 764.95 ft/msl 1.0 Field
Sampling
280-365966 03/15/2017 0957
Depth to water 26.00 ft 1.0 Field
Sampling
280-365966 03/15/2017 0957
Groundwater Elevation 738.95 ft/msl 1.0 Field
Sampling
280-365966 03/15/2017 0957
Field pH 6.24 SU 1.0 Field
Sampling
280-365966 03/15/2017 0957
Field Conductivity 343 umhos/cm 1.0 Field
Sampling
280-365966 03/15/2017 0957
Field Temperature 13.7 Degrees C 1.0 Field
Sampling
280-365966 03/15/2017 0957
Field Turbidity 1.8 NTU 1.0 Field
Sampling
280-365966 03/15/2017 0957
Field Dissolved Oxygen 2.7 mg/L 1.0 Field
Sampling
280-365966 03/15/2017 0957
Field EH/ORP 17.7 millivolts 1.0 Field
Sampling
280-365966 03/15/2017 0957
TestAmerica Denver 03/30/2017Page 52 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Field Service / Mobile Lab
Client Sample ID:
Lab Sample ID:
3406-MW07
Client Matrix:
280-94905-2
Water
Date Sampled: 03/15/2017 1112
Date Received: 03/16/2017 0855
Result Qual Units Dil Method
Analysis Date Analyzed
Date PreparedAnalyteBatch
Well Elevation 771.57 ft/msl 1.0 Field
Sampling
280-365966 03/15/2017 0912
Depth to water 24.80 ft 1.0 Field
Sampling
280-365966 03/15/2017 0912
Groundwater Elevation 746.77 ft/msl 1.0 Field
Sampling
280-365966 03/15/2017 0912
Field pH 6.32 SU 1.0 Field
Sampling
280-365966 03/15/2017 0912
Field Conductivity 147 umhos/cm 1.0 Field
Sampling
280-365966 03/15/2017 0912
Field Temperature 14.2 Degrees C 1.0 Field
Sampling
280-365966 03/15/2017 0912
Field Turbidity 6.0 NTU 1.0 Field
Sampling
280-365966 03/15/2017 0912
Field Dissolved Oxygen 5.3 mg/L 1.0 Field
Sampling
280-365966 03/15/2017 0912
Field EH/ORP 128.0 millivolts 1.0 Field
Sampling
280-365966 03/15/2017 0912
TestAmerica Denver 03/30/2017Page 53 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Field Service / Mobile Lab
Client Sample ID:
Lab Sample ID:
3406-MW11
Client Matrix:
280-94905-3
Water
Date Sampled: 03/15/2017 1020
Date Received: 03/16/2017 0855
Result Qual Units Dil Method
Analysis Date Analyzed
Date PreparedAnalyteBatch
Well Elevation 776.80 ft/msl 1.0 Field
Sampling
280-365966 03/15/2017 0820
Depth to water 28.80 ft 1.0 Field
Sampling
280-365966 03/15/2017 0820
Groundwater Elevation 748.00 ft/msl 1.0 Field
Sampling
280-365966 03/15/2017 0820
Field pH 5.71 SU 1.0 Field
Sampling
280-365966 03/15/2017 0820
Field Conductivity 185 umhos/cm 1.0 Field
Sampling
280-365966 03/15/2017 0820
Field Temperature 13.8 Degrees C 1.0 Field
Sampling
280-365966 03/15/2017 0820
Field Turbidity 3.1 NTU 1.0 Field
Sampling
280-365966 03/15/2017 0820
Field Dissolved Oxygen 2.2 mg/L 1.0 Field
Sampling
280-365966 03/15/2017 0820
Field EH/ORP 156.0 millivolts 1.0 Field
Sampling
280-365966 03/15/2017 0820
TestAmerica Denver 03/30/2017Page 54 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Field Service / Mobile Lab
Client Sample ID:
Lab Sample ID:
3406-MW05
Client Matrix:
280-94905-4
Water
Date Sampled: 03/15/2017 0900
Date Received: 03/16/2017 0855
Result Qual Units Dil Method
Analysis Date Analyzed
Date PreparedAnalyteBatch
Well Elevation 743.17 ft/msl 1.0 Field
Sampling
280-365966 03/15/2017 0700
Depth to water 4.43 ft 1.0 Field
Sampling
280-365966 03/15/2017 0700
Groundwater Elevation 738.74 ft/msl 1.0 Field
Sampling
280-365966 03/15/2017 0700
Field pH 6.00 SU 1.0 Field
Sampling
280-365966 03/15/2017 0700
Field Conductivity 349 umhos/cm 1.0 Field
Sampling
280-365966 03/15/2017 0700
Field Temperature 13.3 Degrees C 1.0 Field
Sampling
280-365966 03/15/2017 0700
Field Turbidity 2.3 NTU 1.0 Field
Sampling
280-365966 03/15/2017 0700
Field Dissolved Oxygen 1.1 mg/L 1.0 Field
Sampling
280-365966 03/15/2017 0700
Field EH/ORP 168.0 millivolts 1.0 Field
Sampling
280-365966 03/15/2017 0700
TestAmerica Denver 03/30/2017Page 55 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Field Service / Mobile Lab
Client Sample ID:
Lab Sample ID:
3406-MW04
Client Matrix:
280-94905-5
Water
Date Sampled: 03/15/2017 0816
Date Received: 03/16/2017 0855
Result Qual Units Dil Method
Analysis Date Analyzed
Date PreparedAnalyteBatch
Well Elevation 756.92 ft/msl 1.0 Field
Sampling
280-365966 03/15/2017 0616
Depth to water 12.94 ft 1.0 Field
Sampling
280-365966 03/15/2017 0616
Groundwater Elevation 743.98 ft/msl 1.0 Field
Sampling
280-365966 03/15/2017 0616
Field pH 5.25 SU 1.0 Field
Sampling
280-365966 03/15/2017 0616
Field Conductivity 96 umhos/cm 1.0 Field
Sampling
280-365966 03/15/2017 0616
Field Temperature 14.6 Degrees C 1.0 Field
Sampling
280-365966 03/15/2017 0616
Field Turbidity 6.5 NTU 1.0 Field
Sampling
280-365966 03/15/2017 0616
Field Dissolved Oxygen 0.0 mg/L 1.0 Field
Sampling
280-365966 03/15/2017 0616
Field EH/ORP 233 millivolts 1.0 Field
Sampling
280-365966 03/15/2017 0616
TestAmerica Denver 03/30/2017Page 56 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Field Service / Mobile Lab
Client Sample ID:
Lab Sample ID:
3406-MW12
Client Matrix:
280-94905-6
Water
Date Sampled: 03/15/2017 0825
Date Received: 03/16/2017 0855
Result Qual Units Dil Method
Analysis Date Analyzed
Date PreparedAnalyteBatch
Well Elevation 751.48 ft/msl 1.0 Field
Sampling
280-365966 03/15/2017 0625
Depth to water 6.08 ft 1.0 Field
Sampling
280-365966 03/15/2017 0625
Groundwater Elevation 745.40 ft/msl 1.0 Field
Sampling
280-365966 03/15/2017 0625
Field pH 5.88 SU 1.0 Field
Sampling
280-365966 03/15/2017 0625
Field Conductivity 141 umhos/cm 1.0 Field
Sampling
280-365966 03/15/2017 0625
Field Temperature 12.9 Degrees C 1.0 Field
Sampling
280-365966 03/15/2017 0625
Field Turbidity 6.7 NTU 1.0 Field
Sampling
280-365966 03/15/2017 0625
Field Dissolved Oxygen 1.5 mg/L 1.0 Field
Sampling
280-365966 03/15/2017 0625
Field EH/ORP 96.2 millivolts 1.0 Field
Sampling
280-365966 03/15/2017 0625
TestAmerica Denver 03/30/2017Page 57 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Field Service / Mobile Lab
Client Sample ID:
Lab Sample ID:
3406-MW08
Client Matrix:
280-94905-7
Water
Date Sampled: 03/15/2017 0952
Date Received: 03/16/2017 0855
Result Qual Units Dil Method
Analysis Date Analyzed
Date PreparedAnalyteBatch
Well Elevation 748.95 ft/msl 1.0 Field
Sampling
280-365966 03/15/2017 0752
Depth to water 5.82 ft 1.0 Field
Sampling
280-365966 03/15/2017 0752
Groundwater Elevation 743.13 ft/msl 1.0 Field
Sampling
280-365966 03/15/2017 0752
Field pH 5.40 SU 1.0 Field
Sampling
280-365966 03/15/2017 0752
Field Conductivity 94 umhos/cm 1.0 Field
Sampling
280-365966 03/15/2017 0752
Field Temperature 9.5 Degrees C 1.0 Field
Sampling
280-365966 03/15/2017 0752
Field Turbidity 7.9 NTU 1.0 Field
Sampling
280-365966 03/15/2017 0752
Field Dissolved Oxygen 2.5 mg/L 1.0 Field
Sampling
280-365966 03/15/2017 0752
Field EH/ORP 118.6 millivolts 1.0 Field
Sampling
280-365966 03/15/2017 0752
TestAmerica Denver 03/30/2017Page 58 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Field Service / Mobile Lab
Client Sample ID:
Lab Sample ID:
3406-MW02
Client Matrix:
280-94905-8
Water
Date Sampled: 03/15/2017 1044
Date Received: 03/16/2017 0855
Result Qual Units Dil Method
Analysis Date Analyzed
Date PreparedAnalyteBatch
Well Elevation 778.04 ft/msl 1.0 Field
Sampling
280-365966 03/15/2017 0844
Depth to water 29.14 ft 1.0 Field
Sampling
280-365966 03/15/2017 0844
Groundwater Elevation 748.90 ft/msl 1.0 Field
Sampling
280-365966 03/15/2017 0844
Field pH 5.51 SU 1.0 Field
Sampling
280-365966 03/15/2017 0844
Field Conductivity 145 umhos/cm 1.0 Field
Sampling
280-365966 03/15/2017 0844
Field Temperature 11.7 Degrees C 1.0 Field
Sampling
280-365966 03/15/2017 0844
Field Turbidity 1.5 NTU 1.0 Field
Sampling
280-365966 03/15/2017 0844
Field Dissolved Oxygen 1.9 mg/L 1.0 Field
Sampling
280-365966 03/15/2017 0844
Field EH/ORP 261.4 millivolts 1.0 Field
Sampling
280-365966 03/15/2017 0844
TestAmerica Denver 03/30/2017Page 59 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Field Service / Mobile Lab
Client Sample ID:
Lab Sample ID:
3406-MW10
Client Matrix:
280-94905-9
Water
Date Sampled: 03/15/2017 1115
Date Received: 03/16/2017 0855
Result Qual Units Dil Method
Analysis Date Analyzed
Date PreparedAnalyteBatch
Well Elevation 777.20 ft/msl 1.0 Field
Sampling
280-365966 03/15/2017 0915
Depth to water 31.07 ft 1.0 Field
Sampling
280-365966 03/15/2017 0915
Groundwater Elevation 746.13 ft/msl 1.0 Field
Sampling
280-365966 03/15/2017 0915
Field pH 5.98 SU 1.0 Field
Sampling
280-365966 03/15/2017 0915
Field Conductivity 93 umhos/cm 1.0 Field
Sampling
280-365966 03/15/2017 0915
Field Temperature 9.6 Degrees C 1.0 Field
Sampling
280-365966 03/15/2017 0915
Field Turbidity 6.8 NTU 1.0 Field
Sampling
280-365966 03/15/2017 0915
Field Dissolved Oxygen 3.9 mg/L 1.0 Field
Sampling
280-365966 03/15/2017 0915
Field EH/ORP 235.3 millivolts 1.0 Field
Sampling
280-365966 03/15/2017 0915
TestAmerica Denver 03/30/2017Page 60 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Field Service / Mobile Lab
Client Sample ID:
Lab Sample ID:
3406-MW03
Client Matrix:
280-94905-10
Water
Date Sampled: 03/15/2017 1210
Date Received: 03/16/2017 0855
Result Qual Units Dil Method
Analysis Date Analyzed
Date PreparedAnalyteBatch
Well Elevation 770.08 ft/msl 1.0 Field
Sampling
280-365966 03/15/2017 1010
Depth to water 25.57 ft 1.0 Field
Sampling
280-365966 03/15/2017 1010
Groundwater Elevation 744.51 ft/msl 1.0 Field
Sampling
280-365966 03/15/2017 1010
Field pH 6.17 SU 1.0 Field
Sampling
280-365966 03/15/2017 1010
Field Conductivity 173 umhos/cm 1.0 Field
Sampling
280-365966 03/15/2017 1010
Field Temperature 10.1 Degrees C 1.0 Field
Sampling
280-365966 03/15/2017 1010
Field Turbidity 3.4 NTU 1.0 Field
Sampling
280-365966 03/15/2017 1010
Field Dissolved Oxygen 4.2 mg/L 1.0 Field
Sampling
280-365966 03/15/2017 1010
Field EH/ORP 62.1 millivolts 1.0 Field
Sampling
280-365966 03/15/2017 1010
TestAmerica Denver 03/30/2017Page 61 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Field Service / Mobile Lab
Client Sample ID:
Lab Sample ID:
3406-01FB
Client Matrix:
280-94905-11FB
Water
Date Sampled: 03/15/2017 1320
Date Received: 03/16/2017 0855
Result Qual Units Dil Method
Analysis Date Analyzed
Date PreparedAnalyteBatch
Field pH 6.74 SU 1.0 Field
Sampling
280-365966 03/15/2017 1120
Field Conductivity 6 umhos/cm 1.0 Field
Sampling
280-365966 03/15/2017 1120
Field Temperature 17.2 Degrees C 1.0 Field
Sampling
280-365966 03/15/2017 1120
Field Turbidity 0.0 NTU 1.0 Field
Sampling
280-365966 03/15/2017 1120
Field Dissolved Oxygen 0.8 mg/L 1.0 Field
Sampling
280-365966 03/15/2017 1120
Field EH/ORP 41.3 millivolts 1.0 Field
Sampling
280-365966 03/15/2017 1120
TestAmerica Denver 03/30/2017Page 62 of 102
Analytical Data
Client: Waste Management Job Number: 280-94905-1
Field Service / Mobile Lab
Client Sample ID:
Lab Sample ID:
3406-MW01
Client Matrix:
280-94905-12
Water
Date Sampled: 03/15/2017 1300
Date Received: 03/16/2017 0855
Result Qual Units Dil Method
Analysis Date Analyzed
Date PreparedAnalyteBatch
Well Elevation 823.93 ft/msl 1.0 Field
Sampling
280-365966 03/15/2017 1100
Depth to water 44.38 ft 1.0 Field
Sampling
280-365966 03/15/2017 1100
Groundwater Elevation 779.55 ft/msl 1.0 Field
Sampling
280-365966 03/15/2017 1100
Field pH 6.15 SU 1.0 Field
Sampling
280-365966 03/15/2017 1100
Field Conductivity 68 umhos/cm 1.0 Field
Sampling
280-365966 03/15/2017 1100
Field Temperature 12.5 Degrees C 1.0 Field
Sampling
280-365966 03/15/2017 1100
Field Turbidity 3.4 NTU 1.0 Field
Sampling
280-365966 03/15/2017 1100
Field Dissolved Oxygen 3.5 mg/L 1.0 Field
Sampling
280-365966 03/15/2017 1100
Field EH/ORP 157.7 millivolts 1.0 Field
Sampling
280-365966 03/15/2017 1100
TestAmerica Denver 03/30/2017Page 63 of 102
DATA REPORTING QUALIFIERS
Client: Waste Management Job Number: 280-94905-1
Lab Section Qualifier Description
GC/MS VOA
Result is less than the RL but greater than or equal to the MDL and the
concentration is an approximate value.
J
Metals
ICV,CCV,ICB,CCB, ISA, ISB, CRI, CRA, DLCK or MRL standard:
Instrument related QC is outside acceptance limits.
^
Result is less than the RL but greater than or equal to the MDL and the
concentration is an approximate value.
J
TestAmerica Denver 03/30/2017Page 64 of 102
QUALITY CONTROL RESULTS
TestAmerica Denver
03/30/2017Page 65 of 102
Quality Control Results
Client: Waste Management Job Number: 280-94905-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
GC/MS VOA
Analysis Batch:280-366626
Lab Control Sample Water 8260BLCS 280-366626/4 T
Method Blank Water 8260BMB 280-366626/6 T
Water3406-MW09R 8260B280-94905-1 T
Matrix Spike Water 8260B280-94905-1MS T
Matrix Spike Duplicate Water 8260B280-94905-1MSD T
Water3406-MW07 8260B280-94905-2 T
Water3406-MW11 8260B280-94905-3 T
Water3406-MW05 8260B280-94905-4 T
Water3406-MW04 8260B280-94905-5 T
Water3406-MW12 8260B280-94905-6 T
Water3406-MW08 8260B280-94905-7 T
Water3406-MW02 8260B280-94905-8 T
Water3406-MW10 8260B280-94905-9 T
Water3406-MW03 8260B280-94905-10 T
Water3406-01FB 8260B280-94905-11FB T
Water3406-MW01 8260B280-94905-12 T
WaterTRIP BLANK 8260B280-94905-13TB T
Report Basis
T = Total
TestAmerica Denver
03/30/2017Page 66 of 102
Quality Control Results
Client: Waste Management Job Number: 280-94905-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
Metals
Prep Batch: 280-366366
Lab Control Sample Water 3005ALCS 280-366366/2-A R
Method Blank Water 3005AMB 280-366366/1-A R
Matrix Spike Water 3005A280-94901-A-2-B MS R
Matrix Spike Duplicate Water 3005A280-94901-A-2-C MSD R
Water3406-MW09R 3005A280-94905-1 R
Water3406-MW07 3005A280-94905-2 R
Matrix Spike Water 3005A280-94905-2MS R
Matrix Spike Duplicate Water 3005A280-94905-2MSD R
Water3406-MW11 3005A280-94905-3 R
Water3406-MW05 3005A280-94905-4 R
Water3406-MW04 3005A280-94905-5 R
Water3406-MW12 3005A280-94905-6 R
Water3406-MW08 3005A280-94905-7 R
Water3406-MW02 3005A280-94905-8 R
Water3406-MW10 3005A280-94905-9 R
Water3406-MW03 3005A280-94905-10 R
Water3406-01FB 3005A280-94905-11FB R
Water3406-MW01 3005A280-94905-12 R
Prep Batch: 280-366367
Lab Control Sample Water 3005ALCS 280-366367/2-A R
Method Blank Water 3005AMB 280-366367/1-A R
Water3406-MW09R 3005A280-94905-1 R
Matrix Spike Water 3005A280-94905-1MS R
Matrix Spike Duplicate Water 3005A280-94905-1MSD R
Water3406-MW07 3005A280-94905-2 R
Water3406-MW11 3005A280-94905-3 R
Water3406-MW05 3005A280-94905-4 R
Water3406-MW04 3005A280-94905-5 R
Water3406-MW12 3005A280-94905-6 R
Water3406-MW08 3005A280-94905-7 R
Water3406-MW02 3005A280-94905-8 R
Water3406-MW10 3005A280-94905-9 R
Water3406-MW03 3005A280-94905-10 R
Water3406-01FB 3005A280-94905-11FB R
Water3406-MW01 3005A280-94905-12 R
TestAmerica Denver
03/30/2017Page 67 of 102
Quality Control Results
Client: Waste Management Job Number: 280-94905-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
Metals
Analysis Batch:280-366863
Lab Control Sample Water 280-3663676020ALCS 280-366367/2-A R
Method Blank Water 280-3663676020AMB 280-366367/1-A R
Water 280-3663673406-MW09R 6020A280-94905-1 R
Matrix Spike Water 280-3663676020A280-94905-1MS R
Matrix Spike Duplicate Water 280-3663676020A280-94905-1MSD R
Water 280-3663673406-MW07 6020A280-94905-2 R
Water 280-3663673406-MW11 6020A280-94905-3 R
Water 280-3663673406-MW05 6020A280-94905-4 R
Water 280-3663673406-MW04 6020A280-94905-5 R
Water 280-3663673406-MW12 6020A280-94905-6 R
Water 280-3663673406-MW08 6020A280-94905-7 R
Water 280-3663673406-MW02 6020A280-94905-8 R
Water 280-3663673406-MW10 6020A280-94905-9 R
Water 280-3663673406-MW03 6020A280-94905-10 R
Water 280-3663673406-01FB 6020A280-94905-11FB R
Water 280-3663673406-MW01 6020A280-94905-12 R
Analysis Batch:280-366869
Lab Control Sample Water 280-3663666010CLCS 280-366366/2-A R
Method Blank Water 280-3663666010CMB 280-366366/1-A R
Water 280-3663663406-MW09R 6010C280-94905-1 R
Water 280-3663663406-MW07 6010C280-94905-2 R
Matrix Spike Water 280-3663666010C280-94905-2MS R
Matrix Spike Duplicate Water 280-3663666010C280-94905-2MSD R
Water 280-3663663406-MW11 6010C280-94905-3 R
Water 280-3663663406-MW05 6010C280-94905-4 R
Water 280-3663663406-MW04 6010C280-94905-5 R
Water 280-3663663406-MW12 6010C280-94905-6 R
Water 280-3663663406-MW08 6010C280-94905-7 R
Water 280-3663663406-MW02 6010C280-94905-8 R
Water 280-3663663406-MW10 6010C280-94905-9 R
Water 280-3663663406-MW03 6010C280-94905-10 R
Water 280-3663663406-01FB 6010C280-94905-11FB R
Water 280-3663663406-MW01 6010C280-94905-12 R
TestAmerica Denver
03/30/2017Page 68 of 102
Quality Control Results
Client: Waste Management Job Number: 280-94905-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
Metals
Analysis Batch:280-367053
Lab Control Sample Water 280-3663666010CLCS 280-366366/2-A R
Method Blank Water 280-3663666010CMB 280-366366/1-A R
Matrix Spike Water 280-3663666010C280-94901-A-2-B MS R
Matrix Spike Duplicate Water 280-3663666010C280-94901-A-2-C MSD R
Water 280-3663663406-MW09R 6010C280-94905-1 R
Water 280-3663663406-MW07 6010C280-94905-2 R
Matrix Spike Water 280-3663666010C280-94905-2MS R
Matrix Spike Duplicate Water 280-3663666010C280-94905-2MSD R
Water 280-3663663406-MW11 6010C280-94905-3 R
Water 280-3663663406-MW05 6010C280-94905-4 R
Water 280-3663663406-MW04 6010C280-94905-5 R
Water 280-3663663406-MW12 6010C280-94905-6 R
Water 280-3663663406-MW08 6010C280-94905-7 R
Water 280-3663663406-MW02 6010C280-94905-8 R
Water 280-3663663406-MW10 6010C280-94905-9 R
Water 280-3663663406-MW03 6010C280-94905-10 R
Water 280-3663663406-01FB 6010C280-94905-11FB R
Water 280-3663663406-MW01 6010C280-94905-12 R
Report Basis
R = Total Recoverable
Field Service / Mobile Lab
Analysis Batch:280-365966
Water3406-MW09R Field Sampling280-94905-1 T
Water3406-MW07 Field Sampling280-94905-2 T
Water3406-MW11 Field Sampling280-94905-3 T
Water3406-MW05 Field Sampling280-94905-4 T
Water3406-MW04 Field Sampling280-94905-5 T
Water3406-MW12 Field Sampling280-94905-6 T
Water3406-MW08 Field Sampling280-94905-7 T
Water3406-MW02 Field Sampling280-94905-8 T
Water3406-MW10 Field Sampling280-94905-9 T
Water3406-MW03 Field Sampling280-94905-10 T
Water3406-01FB Field Sampling280-94905-11FB T
Water3406-MW01 Field Sampling280-94905-12 T
Report Basis
T = Total
TestAmerica Denver
03/30/2017Page 69 of 102
Quality Control Results
Job Number: 280-94905-1Client: Waste Management
Surrogate Recovery Report
8260B Volatile Organic Compounds (GC/MS)
Client Matrix: Water
Lab Sample ID Client Sample ID
DCA BFB DBFM TOL
%Rec %Rec %Rec %Rec
280-94905-1 3406-MW09R 114 105 111 106
280-94905-2 3406-MW07 119 103 116 108
280-94905-3 3406-MW11 123 103 117 107
280-94905-4 3406-MW05 116 98 111 102
280-94905-5 3406-MW04 122 103 116 107
280-94905-6 3406-MW12 123 105 116 106
280-94905-7 3406-MW08 124 101 118 107
280-94905-8 3406-MW02 98 96 100 105
280-94905-9 3406-MW10 109 94 106 99
280-94905-10 3406-MW03 112 94 107 97
280-94905-11 3406-01FB 113 94 106 95
280-94905-12 3406-MW01 121 103 115 108
280-94905-13 TRIP BLANK 108 105 109 112
MB 280-366626/6 121 104 117 109
LCS 280-366626/4 112 97 108 102
280-94905-1 MS 3406-MW09R MS 117 102 116 107
280-94905-1 MSD 3406-MW09R MSD 118 102 115 108
Surrogate Acceptance Limits
DCA = 1,2-Dichloroethane-d4 (Surr)70-127
BFB = 4-Bromofluorobenzene (Surr)78-120
DBFM = Dibromofluoromethane (Surr)77-120
TOL = Toluene-d8 (Surr)80-125
TestAmerica Denver
03/30/2017Page 70 of 102
Quality Control Results
Job Number: 280-94905-1Client: Waste Management
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 280-366626
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
MS9_4622.D
20 mL
20 mLUnits:ug/L
Method: 8260B
Preparation: 5030B
VMS_MS9MB 280-366626/6
Analysis Date:03/23/2017 2042
Analysis Batch:
Prep Batch:
Leach Batch:
N/A
N/A
280-366626
Prep Date:
Leach Date:
03/23/2017 2042
N/A
Analyte RLMDLQualResult
ND 5.00.211,1,1,2-Tetrachloroethane
ND 1.00.161,1,1-Trichloroethane
ND 3.00.211,1,2,2-Tetrachloroethane
ND 1.00.271,1,2-Trichloroethane
ND 5.00.221,1-Dichloroethane
ND 5.00.231,1-Dichloroethene
ND 1.00.331,2,3-Trichloropropane
ND 130.471,2-Dibromo-3-Chloropropane
ND 1.00.181,2-Dibromoethane
ND 5.00.151,2-Dichlorobenzene
ND 1.00.131,2-Dichloroethane
ND 1.00.181,2-Dichloropropane
ND 1.00.161,4-Dichlorobenzene
ND 1002.02-Butanone (MEK)
ND 501.72-Hexanone
ND 1000.984-Methyl-2-pentanone (MIBK)
ND 1001.9Acetone
ND 2001.4Acrylonitrile
ND 1.00.16Benzene
ND 3.00.10Bromochloromethane
ND 1.00.17Bromodichloromethane
ND 3.00.19Bromoform
ND 100.21Bromomethane
ND 1000.45Carbon disulfide
ND 1.00.19Carbon tetrachloride
ND 3.00.17Chlorobenzene
ND 100.41Chloroethane
ND 5.00.16Chloroform
ND 1.00.30Chloromethane
ND 5.00.15cis-1,2-Dichloroethene
ND 1.00.16cis-1,3-Dichloropropene
ND 3.00.17Dibromochloromethane
ND 100.17Dibromomethane
ND 1.00.16Ethylbenzene
ND 100.23Iodomethane
ND 1.00.32Methylene Chloride
ND 1.00.17Styrene
ND 1.00.20Tetrachloroethene
ND 1.00.17Toluene
ND 5.00.15trans-1,2-Dichloroethene
ND 1.00.19trans-1,3-Dichloropropene
ND 1000.80trans-1,4-Dichloro-2-butene
ND 1.00.16Trichloroethene
ND 1.00.29Trichlorofluoromethane
ND 500.94Vinyl acetate
TestAmerica Denver 03/30/2017Page 71 of 102
Quality Control Results
Job Number: 280-94905-1Client: Waste Management
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 280-366626
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
MS9_4622.D
20 mL
20 mLUnits:ug/L
Method: 8260B
Preparation: 5030B
VMS_MS9MB 280-366626/6
Analysis Date:03/23/2017 2042
Analysis Batch:
Prep Batch:
Leach Batch:
N/A
N/A
280-366626
Prep Date:
Leach Date:
03/23/2017 2042
N/A
Analyte RLMDLQualResult
ND 1.00.10Vinyl chloride
ND 5.00.19Xylenes, Total
Surrogate % Rec Acceptance Limits
1,2-Dichloroethane-d4 (Surr)121 70 - 127
4-Bromofluorobenzene (Surr)104 78 - 120
Dibromofluoromethane (Surr)117 77 - 120
Toluene-d8 (Surr)109 80 - 125
Water
1.0
Lab Control Sample - Batch: 280-366626
Client Matrix:
Lab Sample ID:
Dilution:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
MS9_4621.D
20 mL
20 mLUnits:ug/L
Method: 8260B
Preparation: 5030B
VMS_MS9LCS 280-366626/4
Analysis Date:03/23/2017 2021
Analysis Batch:
Prep Batch:
Leach Batch:
280-366626
N/A
N/A
Prep Date:
Leach Date:
03/23/2017 2021
N/A
Analyte QualLimit% Rec.ResultSpike Amount
5.00 4.83 97 65 - 1351,1,1-Trichloroethane
5.00 4.84 97 J65 - 1351,1-Dichloroethane
5.00 4.42 88 J65 - 1361,1-Dichloroethene
5.00 5.04 101 64 - 1351,2-Dichloropropane
5.00 4.18 84 65 - 1351,3-Dichlorobenzene
5.00 4.86 97 65 - 135Benzene
5.00 4.70 94 65 - 135Bromodichloromethane
5.00 4.90 98 65 - 135Carbon tetrachloride
5.00 4.33 87 65 - 135Chlorobenzene
5.00 4.90 98 J65 - 135Chloroform
5.00 4.29 86 65 - 135Ethylbenzene
5.00 4.42 88 54 - 141Methylene Chloride
5.00 4.22 84 65 - 135Tetrachloroethene
5.00 4.77 95 65 - 135Toluene
5.00 4.85 97 J65 - 135trans-1,2-Dichloroethene
5.00 4.57 91 65 - 135Trichloroethene
Surrogate % Rec Acceptance Limits
1,2-Dichloroethane-d4 (Surr)112 70 - 127
4-Bromofluorobenzene (Surr)97 78 - 120
Dibromofluoromethane (Surr)108 77 - 120
Toluene-d8 (Surr)102 80 - 125
TestAmerica Denver 03/30/2017Page 72 of 102
Quality Control Results
Job Number: 280-94905-1Client: Waste Management
Dilution:
Dilution:
Water
1.0
1.0
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix:Water
MS9_4627.D
20 mL
20 mL
20 mL
MS9_4628.D
20 mL
20 mL
20 mL
Method: 8260B
Preparation: 5030B
VMS_MS9
VMS_MS9
280-94905-1
280-94905-1
MS Lab Sample ID:
MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-366626
03/23/2017 2235
N/A
Analysis Date:
Prep Date:
Leach Date:
Analysis Batch:
Prep Batch:
Leach Batch:
280-366626
N/A
N/A
Analysis Date:
Prep Date:
Leach Date:
03/23/2017 2257
03/23/2017 2257
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
280-366626
N/A
N/A
03/23/2017 2235
Analyte RPD LimitRPDLimit
% Rec.
MS MSD MS Qual MSD Qual
110 105 65 - 135 5 201,1,1-Trichloroethane
110 102 65 - 135 6 211,1-Dichloroethane
102 97 65 - 136 5 20 J1,1-Dichloroethene
115 111 64 - 135 4 201,2-Dichloropropane
96 92 65 - 135 4 201,3-Dichlorobenzene
112 107 65 - 135 5 20Benzene
108 105 65 - 135 3 20Bromodichloromethane
111 107 65 - 135 4 21Carbon tetrachloride
98 95 65 - 135 3 20Chlorobenzene
115 109 65 - 135 5 20Chloroform
98 94 65 - 135 4 20Ethylbenzene
96 91 54 - 141 5 26Methylene Chloride
98 94 65 - 135 4 20Tetrachloroethene
110 105 65 - 135 5 20Toluene
111 105 65 - 135 5 24trans-1,2-Dichloroethene
106 101 65 - 135 5 20Trichloroethene
Surrogate Acceptance LimitsMS % Rec MSD % Rec
1,2-Dichloroethane-d4 (Surr)117 118 70 - 127
4-Bromofluorobenzene (Surr)102 102 78 - 120
Dibromofluoromethane (Surr)116 115 77 - 120
Toluene-d8 (Surr)107 108 80 - 125
TestAmerica Denver 03/30/2017Page 73 of 102
Quality Control Results
Job Number: 280-94905-1Client: Waste Management
Water
03/23/2017 2235 03/23/2017 2257
Dilution:Dilution:1.0 1.0
Client Matrix:Client Matrix:Water
Method: 8260B
Preparation: 5030B
Units:ug/L280-94905-1 280-94905-1MS Lab Sample ID:MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-366626
Analysis Date:
Prep Date:
Leach Date:
03/23/2017 2235
N/A
Analysis Date:
Prep Date:
Leach Date:
03/23/2017 2257
N/A
Amount
Sample
Analyte Result/Qual Amount Result/Qual Result/Qual
MS MSDMS Spike MSD Spike
ND 5.00 5.00 5.48 5.231,1,1-Trichloroethane
0.91 J 5.00 5.00 6.39 6.031,1-Dichloroethane
ND 5.00 5.00 5.11 4.87 J1,1-Dichloroethene
ND 5.00 5.00 5.76 5.551,2-Dichloropropane
ND 5.00 5.00 4.80 4.611,3-Dichlorobenzene
ND 5.00 5.00 5.60 5.34Benzene
ND 5.00 5.00 5.42 5.25Bromodichloromethane
ND 5.00 5.00 5.56 5.33Carbon tetrachloride
ND 5.00 5.00 4.90 4.74Chlorobenzene
ND 5.00 5.00 5.74 5.45Chloroform
ND 5.00 5.00 4.89 4.69Ethylbenzene
ND 5.00 5.00 4.78 4.56Methylene Chloride
ND 5.00 5.00 4.88 4.69Tetrachloroethene
ND 5.00 5.00 5.52 5.26Toluene
ND 5.00 5.00 5.54 5.27trans-1,2-Dichloroethene
ND 5.00 5.00 5.30 5.06Trichloroethene
TestAmerica Denver 03/30/2017Page 74 of 102
Quality Control Results
Job Number: 280-94905-1Client: Waste Management
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 280-366366
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
51a032417.csv
50 mL
50 mLUnits:ug/L
Method: 6010C
Preparation: 3005A
Total Recoverable
MT_051MB 280-366366/1-A
Analysis Date:03/24/2017 2316
Analysis Batch:
Prep Batch:
Leach Batch:N/A
280-366869
280-366366
Prep Date:
Leach Date:
03/24/2017 0740
N/A
Analyte RLMDLQualResult
ND 1000.82Barium
ND 100.66Chromium
ND 101.2Cobalt
ND 502.6Nickel
ND 100.93Silver
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 280-366366
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
51a032717.csv
50 mL
50 mLUnits:ug/L
Method: 6010C
Preparation: 3005A
Total Recoverable
MT_051MB 280-366366/1-A
Analysis Date:03/27/2017 2335
Analysis Batch:
Prep Batch:
Leach Batch:N/A
280-367053
280-366366
Prep Date:
Leach Date:
03/24/2017 0740
N/A
Analyte RLMDLQualResult
ND 1.00.47Beryllium
ND 102.7Lead
ND 251.1Vanadium
TestAmerica Denver 03/30/2017Page 75 of 102
Quality Control Results
Job Number: 280-94905-1Client: Waste Management
Water
1.0
Lab Control Sample - Batch: 280-366366
Client Matrix:
Lab Sample ID:
Dilution:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
51a032417.csv
50 mL
50 mLUnits:ug/L
Method: 6010C
Preparation: 3005A
Total Recoverable
MT_051LCS 280-366366/2-A
Analysis Date:03/24/2017 2319
Analysis Batch:
Prep Batch:
Leach Batch:
280-366869
280-366366
N/A
Prep Date:
Leach Date:
03/24/2017 0740
N/A
Analyte QualLimit% Rec.ResultSpike Amount
2000 2170 108 90 - 112Barium
200 222 111 90 - 113Chromium
500 541 108 89 - 111Cobalt
500 538 108 89 - 111Nickel
50.0 57.7 115 86 - 115Silver
Water
1.0
Lab Control Sample - Batch: 280-366366
Client Matrix:
Lab Sample ID:
Dilution:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
51a032717.csv
50 mL
50 mLUnits:ug/L
Method: 6010C
Preparation: 3005A
Total Recoverable
MT_051LCS 280-366366/2-A
Analysis Date:03/27/2017 2338
Analysis Batch:
Prep Batch:
Leach Batch:
280-367053
280-366366
N/A
Prep Date:
Leach Date:
03/24/2017 0740
N/A
Analyte QualLimit% Rec.ResultSpike Amount
50.0 49.1 98 89 - 113Beryllium
500 491 98 89 - 110Lead
500 495 99 90 - 111Vanadium
TestAmerica Denver 03/30/2017Page 76 of 102
Quality Control Results
Job Number: 280-94905-1Client: Waste Management
Dilution:
Dilution:
Water
1.0
1.0
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix:Water
51a032417.csv
50 mL
50 mL
51a032417.csv
50 mL
50 mL
Method: 6010C
Preparation: 3005A
Total Recoverable
MT_051
MT_051
280-94905-2
280-94905-2
MS Lab Sample ID:
MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-366366
03/25/2017 0042
N/A
Analysis Date:
Prep Date:
Leach Date:
Analysis Batch:
Prep Batch:
Leach Batch:
280-366869
280-366366
N/A
Analysis Date:
Prep Date:
Leach Date:
03/25/2017 0045
03/24/2017 0740
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
280-366869
280-366366
N/A
03/24/2017 0740
Analyte RPD LimitRPDLimit
% Rec.
MS MSD MS Qual MSD Qual
110 111 85 - 120 1 20Barium
107 109 73 - 135 1 20Chromium
105 106 82 - 119 1 20Cobalt
104 105 84 - 120 1 20Nickel
112 113 75 - 141 1 20Silver
Dilution:
Dilution:
Water
1.0
1.0
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix:Water
51a032717.csv
50 mL
50 mL
51a032717.csv
50 mL
50 mL
Method: 6010C
Preparation: 3005A
Total Recoverable
MT_051
MT_051
280-94905-2
280-94905-2
MS Lab Sample ID:
MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-366366
03/28/2017 0058
N/A
Analysis Date:
Prep Date:
Leach Date:
Analysis Batch:
Prep Batch:
Leach Batch:
280-367053
280-366366
N/A
Analysis Date:
Prep Date:
Leach Date:
03/28/2017 0101
03/24/2017 0740
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
280-367053
280-366366
N/A
03/24/2017 0740
Analyte RPD LimitRPDLimit
% Rec.
MS MSD MS Qual MSD Qual
99 97 79 - 121 1 20Beryllium
98 96 89 - 121 2 20Lead
99 97 85 - 120 2 20Vanadium
TestAmerica Denver 03/30/2017Page 77 of 102
Quality Control Results
Job Number: 280-94905-1Client: Waste Management
Water
03/25/2017 0042 03/25/2017 0045
Dilution:Dilution:1.0 1.0
Client Matrix:Client Matrix:Water
Method: 6010C
Preparation: 3005A
Total Recoverable
Units:ug/L280-94905-2 280-94905-2MS Lab Sample ID:MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-366366
Analysis Date:
Prep Date:
Leach Date:
03/24/2017 0740
N/A
Analysis Date:
Prep Date:
Leach Date:
03/24/2017 0740
N/A
Amount
Sample
Analyte Result/Qual Amount Result/Qual Result/Qual
MS MSDMS Spike MSD Spike
4.6 J 2000 2000 2210 2220Barium
1.1 J 200 200 215 218Chromium
ND 500 500 525 529Cobalt
ND 500 500 519 524Nickel
ND 50.0 50.0 56.1 56.5Silver
Water
03/28/2017 0058 03/28/2017 0101
Dilution:Dilution:1.0 1.0
Client Matrix:Client Matrix:Water
Method: 6010C
Preparation: 3005A
Total Recoverable
Units:ug/L280-94905-2 280-94905-2MS Lab Sample ID:MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-366366
Analysis Date:
Prep Date:
Leach Date:
03/24/2017 0740
N/A
Analysis Date:
Prep Date:
Leach Date:
03/24/2017 0740
N/A
Amount
Sample
Analyte Result/Qual Amount Result/Qual Result/Qual
MS MSDMS Spike MSD Spike
ND 50.0 50.0 49.3 48.6Beryllium
ND 500 500 488 480Lead
6.8 J 500 500 501 493Vanadium
TestAmerica Denver 03/30/2017Page 78 of 102
Quality Control Results
Job Number: 280-94905-1Client: Waste Management
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 280-366367
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
206_BLK_li032417.D
50 mL
50 mLUnits:ug/L
Method: 6020A
Preparation: 3005A
Total Recoverable
MT_077MB 280-366367/1-A
Analysis Date:03/25/2017 0123
Analysis Batch:
Prep Batch:
Leach Batch:N/A
280-366863
280-366367
Prep Date:
Leach Date:
03/24/2017 0740
N/A
Analyte RLMDLQualResult
ND 6.00.40Antimony
ND 100.33Arsenic
ND 1.00.27Cadmium
ND 100.56Copper
ND 100.70Selenium
ND 5.50.050Thallium
ND 102.0Zinc
Water
1.0
Lab Control Sample - Batch: 280-366367
Client Matrix:
Lab Sample ID:
Dilution:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
207_LCS_li032417.D
50 mL
50 mLUnits:ug/L
Method: 6020A
Preparation: 3005A
Total Recoverable
MT_077LCS 280-366367/2-A
Analysis Date:03/25/2017 0127
Analysis Batch:
Prep Batch:
Leach Batch:
280-366863
280-366367
N/A
Prep Date:
Leach Date:
03/24/2017 0740
N/A
Analyte QualLimit% Rec.ResultSpike Amount
40.0 37.6 94 85 - 115Antimony
40.0 38.4 96 85 - 117Arsenic
40.0 39.9 100 85 - 115Cadmium
40.0 40.4 101 85 - 119Copper
40.0 38.6 97 77 - 122Selenium
40.0 40.1 100 85 - 118Thallium
40.0 39.4 98 83 - 122Zinc
TestAmerica Denver 03/30/2017Page 79 of 102
Quality Control Results
Job Number: 280-94905-1Client: Waste Management
Dilution:
Dilution:
Water
1.0
1.0
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix:Water
220SMPL_li032417.D
50 mL
50 mL
221SMPL_li032417.D
50 mL
50 mL
Method: 6020A
Preparation: 3005A
Total Recoverable
MT_077
MT_077
280-94905-1
280-94905-1
MS Lab Sample ID:
MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-366367
03/25/2017 0216
N/A
Analysis Date:
Prep Date:
Leach Date:
Analysis Batch:
Prep Batch:
Leach Batch:
280-366863
280-366367
N/A
Analysis Date:
Prep Date:
Leach Date:
03/25/2017 0220
03/24/2017 0740
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
280-366863
280-366367
N/A
03/24/2017 0740
Analyte RPD LimitRPDLimit
% Rec.
MS MSD MS Qual MSD Qual
100 94 85 - 115 6 20Antimony
95 93 85 - 117 3 20Arsenic
98 96 85 - 115 3 20Cadmium
97 96 85 - 119 1 20Copper
96 92 77 - 122 5 20Selenium
99 97 85 - 118 3 20Thallium
94 87 83 - 122 7 20Zinc
Water
03/25/2017 0216 03/25/2017 0220
Dilution:Dilution:1.0 1.0
Client Matrix:Client Matrix:Water
Method: 6020A
Preparation: 3005A
Total Recoverable
Units:ug/L280-94905-1 280-94905-1MS Lab Sample ID:MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-366367
Analysis Date:
Prep Date:
Leach Date:
03/24/2017 0740
N/A
Analysis Date:
Prep Date:
Leach Date:
03/24/2017 0740
N/A
Amount
Sample
Analyte Result/Qual Amount Result/Qual Result/Qual
MS MSDMS Spike MSD Spike
ND 40.0 40.0 39.9 37.6Antimony
ND 40.0 40.0 38.1 37.2Arsenic
ND 40.0 40.0 39.4 38.3Cadmium
1.2 J 40.0 40.0 39.8 39.4Copper
ND 40.0 40.0 38.5 36.8Selenium
ND 40.0 40.0 39.6 38.6Thallium
2.4 J 40.0 40.0 40.2 37.4Zinc
TestAmerica Denver 03/30/2017Page 80 of 102
Quality Control Results
Client: Waste Management Job Number: 280-94905-1
Laboratory Chronicle
03/16/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:03/15/2017 11:57
280-94905-1 3406-MW09R
P:5030B 280-94905-D-1 280-366626 03/23/2017 22:14 JNLTAL DEN1
A:8260B 280-94905-D-1 280-366626 03/23/2017 22:14 JNLTAL DEN1
P:3005A 280-94905-A-1-A 280-366869 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94905-A-1-A 280-366869 280-366366 03/24/2017 23:56 CMLTAL DEN1
P:3005A 280-94905-A-1-A 280-367053 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94905-A-1-A 280-367053 280-366366 03/27/2017 23:58 LLBTAL DEN1
P:3005A 280-94905-A-1-B 280-366863 280-366367 03/24/2017 07:40 SURTAL DEN1
A:6020A 280-94905-A-1-B 280-366863 280-366367 03/25/2017 02:13 LMTTAL DEN1
A:Field Sampling 280-94905-A-1 280-365966 03/15/2017 09:57 C1KTAL DEN1
03/16/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:03/15/2017 11:57
280-94905-1 MS 3406-MW09R
P:5030B 280-94905-C-1 MS 280-366626 03/23/2017 22:35 JNLTAL DEN1
A:8260B 280-94905-C-1 MS 280-366626 03/23/2017 22:35 JNLTAL DEN1
P:3005A 280-94905-A-1-C MS 280-366863 280-366367 03/24/2017 07:40 SURTAL DEN1
A:6020A 280-94905-A-1-C MS 280-366863 280-366367 03/25/2017 02:16 LMTTAL DEN1
03/16/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:03/15/2017 11:57
280-94905-1 MSD 3406-MW09R
P:5030B 280-94905-C-1 MSD 280-366626 03/23/2017 22:57 JNLTAL DEN1
A:8260B 280-94905-C-1 MSD 280-366626 03/23/2017 22:57 JNLTAL DEN1
P:3005A 280-94905-A-1-D
MSD
280-366863 280-366367 03/24/2017 07:40 SURTAL DEN1
A:6020A 280-94905-A-1-D
MSD
280-366863 280-366367 03/25/2017 02:20 LMTTAL DEN1
A = Analytical Method P = Prep Method TestAmerica Denver
03/30/2017Page 81 of 102
Quality Control Results
Client: Waste Management Job Number: 280-94905-1
Laboratory Chronicle
03/16/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:03/15/2017 11:12
280-94905-2 3406-MW07
P:5030B 280-94905-D-2 280-366626 03/24/2017 00:44 JNLTAL DEN1
A:8260B 280-94905-D-2 280-366626 03/24/2017 00:44 JNLTAL DEN1
P:3005A 280-94905-A-2-A 280-366869 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94905-A-2-A 280-366869 280-366366 03/25/2017 00:39 CMLTAL DEN1
P:3005A 280-94905-A-2-A 280-367053 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94905-A-2-A 280-367053 280-366366 03/28/2017 00:52 LLBTAL DEN1
P:3005A 280-94905-A-2-D 280-366863 280-366367 03/24/2017 07:40 SURTAL DEN1
A:6020A 280-94905-A-2-D 280-366863 280-366367 03/25/2017 02:24 LMTTAL DEN1
A:Field Sampling 280-94905-A-2 280-365966 03/15/2017 09:12 C1KTAL DEN1
03/16/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:03/15/2017 11:12
280-94905-2 MS 3406-MW07
P:3005A 280-94905-A-2-B MS 280-366869 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94905-A-2-B MS 280-366869 280-366366 03/25/2017 00:42 CMLTAL DEN1
P:3005A 280-94905-A-2-B MS 280-367053 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94905-A-2-B MS 280-367053 280-366366 03/28/2017 00:58 LLBTAL DEN1
03/16/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:03/15/2017 11:12
280-94905-2 MSD 3406-MW07
P:3005A 280-94905-A-2-C
MSD
280-366869 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94905-A-2-C
MSD
280-366869 280-366366 03/25/2017 00:45 CMLTAL DEN1
P:3005A 280-94905-A-2-C
MSD
280-367053 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94905-A-2-C
MSD
280-367053 280-366366 03/28/2017 01:01 LLBTAL DEN1
A = Analytical Method P = Prep Method TestAmerica Denver
03/30/2017Page 82 of 102
Quality Control Results
Client: Waste Management Job Number: 280-94905-1
Laboratory Chronicle
03/16/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:03/15/2017 10:20
280-94905-3 3406-MW11
P:5030B 280-94905-D-3 280-366626 03/24/2017 01:06 JNLTAL DEN1
A:8260B 280-94905-D-3 280-366626 03/24/2017 01:06 JNLTAL DEN1
P:3005A 280-94905-A-3-A 280-366869 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94905-A-3-A 280-366869 280-366366 03/24/2017 23:59 CMLTAL DEN1
P:3005A 280-94905-A-3-A 280-367053 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94905-A-3-A 280-367053 280-366366 03/28/2017 00:12 LLBTAL DEN1
P:3005A 280-94905-A-3-B 280-366863 280-366367 03/24/2017 07:40 SURTAL DEN1
A:6020A 280-94905-A-3-B 280-366863 280-366367 03/25/2017 02:28 LMTTAL DEN1
A:Field Sampling 280-94905-A-3 280-365966 03/15/2017 08:20 C1KTAL DEN1
03/16/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:03/15/2017 09:00
280-94905-4 3406-MW05
P:5030B 280-94905-D-4 280-366626 03/24/2017 01:27 JNLTAL DEN1
A:8260B 280-94905-D-4 280-366626 03/24/2017 01:27 JNLTAL DEN1
P:3005A 280-94905-A-4-A 280-366869 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94905-A-4-A 280-366869 280-366366 03/25/2017 00:02 CMLTAL DEN1
P:3005A 280-94905-A-4-A 280-367053 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94905-A-4-A 280-367053 280-366366 03/28/2017 00:15 LLBTAL DEN1
P:3005A 280-94905-A-4-B 280-366863 280-366367 03/24/2017 07:40 SURTAL DEN1
A:6020A 280-94905-A-4-B 280-366863 280-366367 03/25/2017 02:31 LMTTAL DEN1
A:Field Sampling 280-94905-A-4 280-365966 03/15/2017 07:00 C1KTAL DEN1
03/16/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:03/15/2017 08:16
280-94905-5 3406-MW04
P:5030B 280-94905-D-5 280-366626 03/24/2017 01:49 JNLTAL DEN1
A:8260B 280-94905-D-5 280-366626 03/24/2017 01:49 JNLTAL DEN1
P:3005A 280-94905-A-5-A 280-366869 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94905-A-5-A 280-366869 280-366366 03/25/2017 00:05 CMLTAL DEN1
P:3005A 280-94905-A-5-A 280-367053 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94905-A-5-A 280-367053 280-366366 03/28/2017 00:18 LLBTAL DEN1
P:3005A 280-94905-A-5-B 280-366863 280-366367 03/24/2017 07:40 SURTAL DEN1
A:6020A 280-94905-A-5-B 280-366863 280-366367 03/25/2017 02:47 LMTTAL DEN1
A:Field Sampling 280-94905-A-5 280-365966 03/15/2017 06:16 C1KTAL DEN1
A = Analytical Method P = Prep Method TestAmerica Denver
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Quality Control Results
Client: Waste Management Job Number: 280-94905-1
Laboratory Chronicle
03/16/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:03/15/2017 08:25
280-94905-6 3406-MW12
P:5030B 280-94905-D-6 280-366626 03/24/2017 02:10 JNLTAL DEN1
A:8260B 280-94905-D-6 280-366626 03/24/2017 02:10 JNLTAL DEN1
P:3005A 280-94905-A-6-A 280-366869 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94905-A-6-A 280-366869 280-366366 03/25/2017 00:08 CMLTAL DEN1
P:3005A 280-94905-A-6-A 280-367053 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94905-A-6-A 280-367053 280-366366 03/28/2017 00:21 LLBTAL DEN1
P:3005A 280-94905-A-6-B 280-366863 280-366367 03/24/2017 07:40 SURTAL DEN1
A:6020A 280-94905-A-6-B 280-366863 280-366367 03/25/2017 02:50 LMTTAL DEN1
A:Field Sampling 280-94905-A-6 280-365966 03/15/2017 06:25 C1KTAL DEN1
03/16/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:03/15/2017 09:52
280-94905-7 3406-MW08
P:5030B 280-94905-C-7 280-366626 03/24/2017 02:31 JNLTAL DEN1
A:8260B 280-94905-C-7 280-366626 03/24/2017 02:31 JNLTAL DEN1
P:3005A 280-94905-A-7-A 280-366869 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94905-A-7-A 280-366869 280-366366 03/25/2017 00:13 CMLTAL DEN1
P:3005A 280-94905-A-7-A 280-367053 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94905-A-7-A 280-367053 280-366366 03/28/2017 00:23 LLBTAL DEN1
P:3005A 280-94905-A-7-B 280-366863 280-366367 03/24/2017 07:40 SURTAL DEN1
A:6020A 280-94905-A-7-B 280-366863 280-366367 03/25/2017 02:54 LMTTAL DEN1
A:Field Sampling 280-94905-A-7 280-365966 03/15/2017 07:52 C1KTAL DEN1
03/16/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:03/15/2017 10:44
280-94905-8 3406-MW02
P:5030B 280-94905-D-8 280-366626 03/24/2017 02:53 JNLTAL DEN1
A:8260B 280-94905-D-8 280-366626 03/24/2017 02:53 JNLTAL DEN1
P:3005A 280-94905-A-8-A 280-366869 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94905-A-8-A 280-366869 280-366366 03/25/2017 00:25 CMLTAL DEN1
P:3005A 280-94905-A-8-A 280-367053 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94905-A-8-A 280-367053 280-366366 03/28/2017 00:26 LLBTAL DEN1
P:3005A 280-94905-A-8-B 280-366863 280-366367 03/24/2017 07:40 SURTAL DEN1
A:6020A 280-94905-A-8-B 280-366863 280-366367 03/25/2017 02:58 LMTTAL DEN1
A:Field Sampling 280-94905-A-8 280-365966 03/15/2017 08:44 C1KTAL DEN1
A = Analytical Method P = Prep Method TestAmerica Denver
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Quality Control Results
Client: Waste Management Job Number: 280-94905-1
Laboratory Chronicle
03/16/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:03/15/2017 11:15
280-94905-9 3406-MW10
P:5030B 280-94905-D-9 280-366626 03/24/2017 03:14 JNLTAL DEN1
A:8260B 280-94905-D-9 280-366626 03/24/2017 03:14 JNLTAL DEN1
P:3005A 280-94905-A-9-A 280-366869 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94905-A-9-A 280-366869 280-366366 03/25/2017 00:28 CMLTAL DEN1
P:3005A 280-94905-A-9-A 280-367053 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94905-A-9-A 280-367053 280-366366 03/28/2017 00:29 LLBTAL DEN1
P:3005A 280-94905-A-9-B 280-366863 280-366367 03/24/2017 07:40 SURTAL DEN1
A:6020A 280-94905-A-9-B 280-366863 280-366367 03/25/2017 03:02 LMTTAL DEN1
A:Field Sampling 280-94905-A-9 280-365966 03/15/2017 09:15 C1KTAL DEN1
03/16/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:03/15/2017 12:10
280-94905-10 3406-MW03
P:5030B 280-94905-D-10 280-366626 03/24/2017 03:36 JNLTAL DEN1
A:8260B 280-94905-D-10 280-366626 03/24/2017 03:36 JNLTAL DEN1
P:3005A 280-94905-A-10-A 280-366869 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94905-A-10-A 280-366869 280-366366 03/25/2017 00:31 CMLTAL DEN1
P:3005A 280-94905-A-10-A 280-367053 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94905-A-10-A 280-367053 280-366366 03/28/2017 00:32 LLBTAL DEN1
P:3005A 280-94905-A-10-B 280-366863 280-366367 03/24/2017 07:40 SURTAL DEN1
A:6020A 280-94905-A-10-B 280-366863 280-366367 03/25/2017 03:05 LMTTAL DEN1
A:Field Sampling 280-94905-A-10 280-365966 03/15/2017 10:10 C1KTAL DEN1
03/16/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:03/15/2017 13:20
280-94905-11 3406-01FB
P:5030B 280-94905-D-11 280-366626 03/24/2017 03:57 JNLTAL DEN1
A:8260B 280-94905-D-11 280-366626 03/24/2017 03:57 JNLTAL DEN1
P:3005A 280-94905-A-11-A 280-366869 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94905-A-11-A 280-366869 280-366366 03/25/2017 00:34 CMLTAL DEN1
P:3005A 280-94905-A-11-A 280-367053 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94905-A-11-A 280-367053 280-366366 03/28/2017 00:35 LLBTAL DEN1
P:3005A 280-94905-A-11-B 280-366863 280-366367 03/24/2017 07:40 SURTAL DEN1
A:6020A 280-94905-A-11-B 280-366863 280-366367 03/25/2017 03:09 LMTTAL DEN1
A:Field Sampling 280-94905-A-11 280-365966 03/15/2017 11:20 C1KTAL DEN1
A = Analytical Method P = Prep Method TestAmerica Denver
03/30/2017Page 85 of 102
Quality Control Results
Client: Waste Management Job Number: 280-94905-1
Laboratory Chronicle
03/16/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:03/15/2017 13:00
280-94905-12 3406-MW01
P:5030B 280-94905-B-12 280-366626 03/24/2017 04:19 JNLTAL DEN1
A:8260B 280-94905-B-12 280-366626 03/24/2017 04:19 JNLTAL DEN1
P:3005A 280-94905-A-12-A 280-366869 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94905-A-12-A 280-366869 280-366366 03/25/2017 00:37 CMLTAL DEN1
P:3005A 280-94905-A-12-A 280-367053 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94905-A-12-A 280-367053 280-366366 03/28/2017 00:38 LLBTAL DEN1
P:3005A 280-94905-A-12-B 280-366863 280-366367 03/24/2017 07:40 SURTAL DEN1
A:6020A 280-94905-A-12-B 280-366863 280-366367 03/25/2017 03:13 LMTTAL DEN1
A:Field Sampling 280-94905-A-12 280-365966 03/15/2017 11:00 C1KTAL DEN1
03/16/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:03/15/2017 00:00
280-94905-13 TRIP BLANK
P:5030B 280-94905-A-13 280-366626 03/24/2017 04:40 JNLTAL DEN1
A:8260B 280-94905-A-13 280-366626 03/24/2017 04:40 JNLTAL DEN1
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:N/A Received Date/Time:N/A
MB N/A
P:5030B MB 280-366626/6 280-366626 03/23/2017 20:42 JNLTAL DEN1
A:8260B MB 280-366626/6 280-366626 03/23/2017 20:42 JNLTAL DEN1
P:3005A MB 280-366366/1-A 280-366869 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C MB 280-366366/1-A 280-366869 280-366366 03/24/2017 23:16 CMLTAL DEN1
P:3005A MB 280-366366/1-A 280-367053 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C MB 280-366366/1-A 280-367053 280-366366 03/27/2017 23:35 LLBTAL DEN1
P:3005A MB 280-366367/1-A 280-366863 280-366367 03/24/2017 07:40 SURTAL DEN1
A:6020A MB 280-366367/1-A 280-366863 280-366367 03/25/2017 01:23 LMTTAL DEN1
A = Analytical Method P = Prep Method TestAmerica Denver
03/30/2017Page 86 of 102
Quality Control Results
Client: Waste Management Job Number: 280-94905-1
Laboratory Chronicle
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:N/A Received Date/Time:N/A
LCS N/A
P:5030B LCS 280-366626/4 280-366626 03/23/2017 20:21 JNLTAL DEN1
A:8260B LCS 280-366626/4 280-366626 03/23/2017 20:21 JNLTAL DEN1
P:3005A LCS 280-366366/2-A 280-366869 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C LCS 280-366366/2-A 280-366869 280-366366 03/24/2017 23:19 CMLTAL DEN1
P:3005A LCS 280-366366/2-A 280-367053 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C LCS 280-366366/2-A 280-367053 280-366366 03/27/2017 23:38 LLBTAL DEN1
P:3005A LCS 280-366367/2-A 280-366863 280-366367 03/24/2017 07:40 SURTAL DEN1
A:6020A LCS 280-366367/2-A 280-366863 280-366367 03/25/2017 01:27 LMTTAL DEN1
Lab References:
TAL DEN = TestAmerica Denver
A = Analytical Method P = Prep Method TestAmerica Denver
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Login Sample Receipt Checklist
Client: Waste Management Job Number: 280-94905-1
Login Number: 94905
Question Answer Comment
Creator: Woodworth, Sean P
List Source: TestAmerica Denver
List Number: 1
N/ARadioactivity either was not measured or, if measured, is at or below
background
TrueThe cooler's custody seal, if present, is intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the sample IDs on the containers and
the COC.
TrueSamples are received within Holding Time (Excluding tests with immediate
HTs)..
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueVOA sample vials do not have headspace or bubble is <6mm (1/4") in
diameter.
TrueIf necessary, staff have been informed of any short hold time or quick TAT
needs
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
TrueSampling Company provided.
TrueSamples received within 48 hours of sampling.
TrueSamples requiring field filtration have been filtered in the field.
TrueChlorine Residual checked.
TestAmerica Denver 03/30/2017Page 102 of 102
ANALYTICAL REPORT
Job Number: 280-94901-1
Job Description: 134|Piedmont Landfill
For:
Waste Management
1850 Parkway Place
Suite 600
Marietta, GA 30067
Attention: Mr. Al Lacsamana
_____________________________________________
Approved for release.
Danielle M Harrington
Project Manager II
3/29/2017 11:22 AM
Designee for
Betsy A Sara, Project Manager II
4955 Yarrow Street, Arvada, CO, 80002
[phone]
[e-mail]
03/29/2017
cc:Mr. Van Burbach
The test results in this report relate only to the samples in this report and meet all requirements of NELAC, with any
exceptions noted. Pursuant to NELAP, this report shall not be reproduced except in full, without the written approval of
the laboratory. All questions regarding this report should be directed to the TestAmerica Denver Project Manager.

The Lab Certification ID# is 4025.

Reporting limits are adjusted for sample size used, dilutions and moisture content if applicable.
TestAmerica Laboratories, Inc.
TestAmerica Denver 4955 Yarrow Street, Arvada, CO 80002
Tel [phone] Fax [phone] www.testamericainc.com
Page 1 of 50
CASE NARRATIVE
Client: Waste Management
Project: 134|Piedmont Landfill
Report Number: 280-94901-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
This report may include reporting limits (RLs) less than TestAmerica’s standard reporting limit. The reported sample results and
associated reporting limits are being used specifically to meet the needs of this project. Note that data are not normally reported to these
levels without qualification because they are inherently less reliable and potentially less defensible than required by the latest industry
standards.
Sample Receiving
The samples were received on 03/16/2017; the samples arrived in good condition, properly preserved and on ice. The temperature of the
cooler at receipt was 3.1C.
Holding Times
The holding times were within established control limits.
Method Blanks
All Method Blanks were within established control limits.
Laboratory Control Samples (LCS)
All Laboratory Control Samples were within established control limits.
Matrix Spike and Matrix Spike Duplicate (MS/MSD)
The Method 8260B MS/MSD performed on the sample 3406-S02 exhibited a RPD result outside the RPD limit for Acetone. A short
compound list was reported for the Method 8260B MS/MSD and therefore Acetone is not reported in the MS/MSD section. Because the
corresponding Matrix Spike and Matrix Spike Duplicate recoveries, Laboratory Control Sample, and Method Blank sample were within
control limits, this anomaly is considered to be due to matrix interference and no corrective action was taken.
All other MS/MSD samples were within established control limits.
Metals
Copper is present in the continuing calibration blank associated with QC batch 280-366863. This is an indicator that data may be biased
high. As no detectable concentrations of Copper are present in the associated samples, corrective action is deemed unnecessary.
Page 2 of 50
EXECUTIVE SUMMARY - Detections
Client: Waste Management Job Number: 280-94901-1
Analyte Result
Reporting
Limit Units Method
Lab Sample ID Client Sample ID
Qualifier
280-94901-1 3406-S02
SU Field Sampling6.13Field pH
umhos/cm Field Sampling119Field Conductivity
Degrees C Field Sampling9.5Field Temperature
NTU Field Sampling14.3Field Turbidity
mg/L Field Sampling7.9Field Dissolved Oxygen
millivolts Field Sampling109.3Field EH/ORP
Total Recoverable
100 ug/L 6010C37JBarium
10 ug/L 6010C1.8 JChromium
25 ug/L 6010C2.9 JVanadium
6.0 ug/L 6020A0.41 JAntimony
10 ug/L 6020A0.33 JArsenic
10 ug/L 6020A1.8 J ^Copper
10 ug/L 6020A4.4 JZinc
280-94901-2 3406-S05
5.0 ug/L 8260B0.21 Jcis-1,2-Dichloroethene
SU Field Sampling5.82Field pH
umhos/cm Field Sampling175Field Conductivity
Degrees C Field Sampling10.1Field Temperature
NTU Field Sampling11.9Field Turbidity
mg/L Field Sampling7.9Field Dissolved Oxygen
millivolts Field Sampling164.3Field EH/ORP
Total Recoverable
100 ug/L 6010C43JBarium
10 ug/L 6010C1.1 JChromium
10 ug/L 6010C1.2 JCobalt
25 ug/L 6010C1.3 JVanadium
10 ug/L 6020A1.3 J ^Copper
5.5 ug/L 6020A0.065 JThallium
10 ug/L 6020A2.5 JZinc
TestAmerica Denver Page 3 of 50
EXECUTIVE SUMMARY - Detections
Client: Waste Management Job Number: 280-94901-1
Analyte Result
Reporting
Limit Units Method
Lab Sample ID Client Sample ID
Qualifier
280-94901-3 3406-S04
100 ug/L 8260B2.7 JAcetone
SU Field Sampling5.48Field pH
umhos/cm Field Sampling96Field Conductivity
Degrees C Field Sampling9.9Field Temperature
NTU Field Sampling19.6Field Turbidity
mg/L Field Sampling8.3Field Dissolved Oxygen
millivolts Field Sampling214.0Field EH/ORP
Total Recoverable
100 ug/L 6010C29JBarium
10 ug/L 6010C1.2 JChromium
25 ug/L 6010C2.4 JVanadium
10 ug/L 6020A1.2 J ^Copper
10 ug/L 6020A3.0 JZinc
280-94901-4 3406-S03
SU Field Sampling4.97Field pH
umhos/cm Field Sampling95Field Conductivity
Degrees C Field Sampling9.1Field Temperature
NTU Field Sampling22.9Field Turbidity
mg/L Field Sampling8.5Field Dissolved Oxygen
millivolts Field Sampling203.9Field EH/ORP
Total Recoverable
100 ug/L 6010C29JBarium
10 ug/L 6010C1.7 JChromium
25 ug/L 6010C3.4 JVanadium
10 ug/L 6020A1.0 J ^Copper
10 ug/L 6020A2.1 JZinc
TestAmerica Denver Page 4 of 50
METHOD SUMMARY
Client: Waste Management Job Number: 280-94901-1
Preparation MethodMethodLab LocationDescription
Matrix:Water
Volatile Organic Compounds (GC/MS)TAL DEN SW846 8260B
Purge and Trap TAL DEN SW846 5030B
Metals (ICP)TAL DEN SW846 6010C
Preparation, Total Recoverable or Dissolved Metals TAL DEN SW846 3005A
Metals (ICP/MS)TAL DEN SW846 6020A
Preparation, Total Recoverable or Dissolved Metals TAL DEN SW846 3005A
Field Sampling TAL DEN EPA Field Sampling
Lab References:
TAL DEN = TestAmerica Denver
Method References:
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its
Updates.
TestAmerica Denver Page 5 of 50
METHOD / ANALYST SUMMARY
Client: Waste Management Job Number: 280-94901-1
Method Analyst Analyst ID
Lines, Jeremy N JNLSW846 8260B
Broander, Laura L LLBSW846 6010C
Lackey, Cara M CMLSW846 6010C
Trudell, Lynn-Anne M LMTSW846 6020A
Krisorn, Chamaiporn 1 C1KEPA Field Sampling
TestAmerica Denver
Page 6 of 50
SAMPLE SUMMARY
Client: Waste Management Job Number: 280-94901-1
Client Sample IDLab Sample ID Client Matrix Sampled Received
Date/Time Date/Time
280-94901-1 3406-S02 Water 03/14/2017 1430 03/16/2017 0855
280-94901-2 3406-S05 Water 03/14/2017 1405 03/16/2017 0855
280-94901-3 3406-S04 Water 03/14/2017 1345 03/16/2017 0855
280-94901-4 3406-S03 Water 03/14/2017 1330 03/16/2017 0855
280-94901-5TB TRIP BLANK Water 03/14/2017 0000 03/16/2017 0855
TestAmerica Denver Page 7 of 50
SAMPLE RESULTS
TestAmerica Denver
Page 8 of 50
Analytical Data
Client: Waste Management Job Number: 280-94901-1
Client Sample ID:
Lab Sample ID:
3406-S02
Client Matrix:
280-94901-1
Water
Date Sampled: 03/14/2017 1430
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/23/2017 2109
03/23/2017 2109
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4623.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.211,1,1,2-Tetrachloroethane
ND 1.00.161,1,1-Trichloroethane
ND 3.00.211,1,2,2-Tetrachloroethane
ND 1.00.271,1,2-Trichloroethane
ND 5.00.221,1-Dichloroethane
ND 5.00.231,1-Dichloroethene
ND 1.00.331,2,3-Trichloropropane
ND 130.471,2-Dibromo-3-Chloropropane
ND 1.00.181,2-Dibromoethane
ND 5.00.151,2-Dichlorobenzene
ND 1.00.131,2-Dichloroethane
ND 1.00.181,2-Dichloropropane
ND 1.00.161,4-Dichlorobenzene
ND 1002.02-Butanone (MEK)
ND 501.72-Hexanone
ND 1000.984-Methyl-2-pentanone (MIBK)
ND F2 1001.9Acetone
ND 2001.4Acrylonitrile
ND 1.00.16Benzene
ND 3.00.10Bromochloromethane
ND 1.00.17Bromodichloromethane
ND 3.00.19Bromoform
ND 100.21Bromomethane
ND 1000.45Carbon disulfide
ND 1.00.19Carbon tetrachloride
ND 3.00.17Chlorobenzene
ND 100.41Chloroethane
ND 5.00.16Chloroform
ND 1.00.30Chloromethane
ND 5.00.15cis-1,2-Dichloroethene
ND 1.00.16cis-1,3-Dichloropropene
ND 3.00.17Dibromochloromethane
ND 100.17Dibromomethane
ND 1.00.16Ethylbenzene
ND 100.23Iodomethane
ND 1.00.32Methylene Chloride
ND 1.00.17Styrene
ND 1.00.20Tetrachloroethene
ND 1.00.17Toluene
ND 5.00.15trans-1,2-Dichloroethene
ND 1.00.19trans-1,3-Dichloropropene
ND 1000.80trans-1,4-Dichloro-2-butene
ND 1.00.16Trichloroethene
ND 1.00.29Trichlorofluoromethane
ND 500.94Vinyl acetate
ND 1.00.10Vinyl chloride
TestAmerica Denver Page 9 of 50
Analytical Data
Client: Waste Management Job Number: 280-94901-1
Client Sample ID:
Lab Sample ID:
3406-S02
Client Matrix:
280-94901-1
Water
Date Sampled: 03/14/2017 1430
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/23/2017 2109
03/23/2017 2109
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4623.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.19Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
95 70 - 1271,2-Dichloroethane-d4 (Surr)
95 78 - 1204-Bromofluorobenzene (Surr)
97 77 - 120Dibromofluoromethane (Surr)
103 80 - 125Toluene-d8 (Surr)
TestAmerica Denver Page 10 of 50
Analytical Data
Client: Waste Management Job Number: 280-94901-1
Client Sample ID:
Lab Sample ID:
3406-S05
Client Matrix:
280-94901-2
Water
Date Sampled: 03/14/2017 1405
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/23/2017 2318
03/23/2017 2318
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4629.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.211,1,1,2-Tetrachloroethane
ND 1.00.161,1,1-Trichloroethane
ND 3.00.211,1,2,2-Tetrachloroethane
ND 1.00.271,1,2-Trichloroethane
ND 5.00.221,1-Dichloroethane
ND 5.00.231,1-Dichloroethene
ND 1.00.331,2,3-Trichloropropane
ND 130.471,2-Dibromo-3-Chloropropane
ND 1.00.181,2-Dibromoethane
ND 5.00.151,2-Dichlorobenzene
ND 1.00.131,2-Dichloroethane
ND 1.00.181,2-Dichloropropane
ND 1.00.161,4-Dichlorobenzene
ND 1002.02-Butanone (MEK)
ND 501.72-Hexanone
ND 1000.984-Methyl-2-pentanone (MIBK)
ND 1001.9Acetone
ND 2001.4Acrylonitrile
ND 1.00.16Benzene
ND 3.00.10Bromochloromethane
ND 1.00.17Bromodichloromethane
ND 3.00.19Bromoform
ND 100.21Bromomethane
ND 1000.45Carbon disulfide
ND 1.00.19Carbon tetrachloride
ND 3.00.17Chlorobenzene
ND 100.41Chloroethane
ND 5.00.16Chloroform
ND 1.00.30Chloromethane
0.21 J 5.00.15cis-1,2-Dichloroethene
ND 1.00.16cis-1,3-Dichloropropene
ND 3.00.17Dibromochloromethane
ND 100.17Dibromomethane
ND 1.00.16Ethylbenzene
ND 100.23Iodomethane
ND 1.00.32Methylene Chloride
ND 1.00.17Styrene
ND 1.00.20Tetrachloroethene
ND 1.00.17Toluene
ND 5.00.15trans-1,2-Dichloroethene
ND 1.00.19trans-1,3-Dichloropropene
ND 1000.80trans-1,4-Dichloro-2-butene
ND 1.00.16Trichloroethene
ND 1.00.29Trichlorofluoromethane
ND 500.94Vinyl acetate
ND 1.00.10Vinyl chloride
TestAmerica Denver Page 11 of 50
Analytical Data
Client: Waste Management Job Number: 280-94901-1
Client Sample ID:
Lab Sample ID:
3406-S05
Client Matrix:
280-94901-2
Water
Date Sampled: 03/14/2017 1405
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/23/2017 2318
03/23/2017 2318
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4629.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.19Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
104 70 - 1271,2-Dichloroethane-d4 (Surr)
105 78 - 1204-Bromofluorobenzene (Surr)
105 77 - 120Dibromofluoromethane (Surr)
111 80 - 125Toluene-d8 (Surr)
TestAmerica Denver Page 12 of 50
Analytical Data
Client: Waste Management Job Number: 280-94901-1
Client Sample ID:
Lab Sample ID:
3406-S04
Client Matrix:
280-94901-3
Water
Date Sampled: 03/14/2017 1345
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/23/2017 2340
03/23/2017 2340
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4630.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.211,1,1,2-Tetrachloroethane
ND 1.00.161,1,1-Trichloroethane
ND 3.00.211,1,2,2-Tetrachloroethane
ND 1.00.271,1,2-Trichloroethane
ND 5.00.221,1-Dichloroethane
ND 5.00.231,1-Dichloroethene
ND 1.00.331,2,3-Trichloropropane
ND 130.471,2-Dibromo-3-Chloropropane
ND 1.00.181,2-Dibromoethane
ND 5.00.151,2-Dichlorobenzene
ND 1.00.131,2-Dichloroethane
ND 1.00.181,2-Dichloropropane
ND 1.00.161,4-Dichlorobenzene
ND 1002.02-Butanone (MEK)
ND 501.72-Hexanone
ND 1000.984-Methyl-2-pentanone (MIBK)
2.7 J 1001.9Acetone
ND 2001.4Acrylonitrile
ND 1.00.16Benzene
ND 3.00.10Bromochloromethane
ND 1.00.17Bromodichloromethane
ND 3.00.19Bromoform
ND 100.21Bromomethane
ND 1000.45Carbon disulfide
ND 1.00.19Carbon tetrachloride
ND 3.00.17Chlorobenzene
ND 100.41Chloroethane
ND 5.00.16Chloroform
ND 1.00.30Chloromethane
ND 5.00.15cis-1,2-Dichloroethene
ND 1.00.16cis-1,3-Dichloropropene
ND 3.00.17Dibromochloromethane
ND 100.17Dibromomethane
ND 1.00.16Ethylbenzene
ND 100.23Iodomethane
ND 1.00.32Methylene Chloride
ND 1.00.17Styrene
ND 1.00.20Tetrachloroethene
ND 1.00.17Toluene
ND 5.00.15trans-1,2-Dichloroethene
ND 1.00.19trans-1,3-Dichloropropene
ND 1000.80trans-1,4-Dichloro-2-butene
ND 1.00.16Trichloroethene
ND 1.00.29Trichlorofluoromethane
ND 500.94Vinyl acetate
ND 1.00.10Vinyl chloride
TestAmerica Denver Page 13 of 50
Analytical Data
Client: Waste Management Job Number: 280-94901-1
Client Sample ID:
Lab Sample ID:
3406-S04
Client Matrix:
280-94901-3
Water
Date Sampled: 03/14/2017 1345
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/23/2017 2340
03/23/2017 2340
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4630.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.19Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
119 70 - 1271,2-Dichloroethane-d4 (Surr)
101 78 - 1204-Bromofluorobenzene (Surr)
115 77 - 120Dibromofluoromethane (Surr)
106 80 - 125Toluene-d8 (Surr)
TestAmerica Denver Page 14 of 50
Analytical Data
Client: Waste Management Job Number: 280-94901-1
Client Sample ID:
Lab Sample ID:
3406-S03
Client Matrix:
280-94901-4
Water
Date Sampled: 03/14/2017 1330
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/24/2017 0001
03/24/2017 0001
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4631.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.211,1,1,2-Tetrachloroethane
ND 1.00.161,1,1-Trichloroethane
ND 3.00.211,1,2,2-Tetrachloroethane
ND 1.00.271,1,2-Trichloroethane
ND 5.00.221,1-Dichloroethane
ND 5.00.231,1-Dichloroethene
ND 1.00.331,2,3-Trichloropropane
ND 130.471,2-Dibromo-3-Chloropropane
ND 1.00.181,2-Dibromoethane
ND 5.00.151,2-Dichlorobenzene
ND 1.00.131,2-Dichloroethane
ND 1.00.181,2-Dichloropropane
ND 1.00.161,4-Dichlorobenzene
ND 1002.02-Butanone (MEK)
ND 501.72-Hexanone
ND 1000.984-Methyl-2-pentanone (MIBK)
ND 1001.9Acetone
ND 2001.4Acrylonitrile
ND 1.00.16Benzene
ND 3.00.10Bromochloromethane
ND 1.00.17Bromodichloromethane
ND 3.00.19Bromoform
ND 100.21Bromomethane
ND 1000.45Carbon disulfide
ND 1.00.19Carbon tetrachloride
ND 3.00.17Chlorobenzene
ND 100.41Chloroethane
ND 5.00.16Chloroform
ND 1.00.30Chloromethane
ND 5.00.15cis-1,2-Dichloroethene
ND 1.00.16cis-1,3-Dichloropropene
ND 3.00.17Dibromochloromethane
ND 100.17Dibromomethane
ND 1.00.16Ethylbenzene
ND 100.23Iodomethane
ND 1.00.32Methylene Chloride
ND 1.00.17Styrene
ND 1.00.20Tetrachloroethene
ND 1.00.17Toluene
ND 5.00.15trans-1,2-Dichloroethene
ND 1.00.19trans-1,3-Dichloropropene
ND 1000.80trans-1,4-Dichloro-2-butene
ND 1.00.16Trichloroethene
ND 1.00.29Trichlorofluoromethane
ND 500.94Vinyl acetate
ND 1.00.10Vinyl chloride
TestAmerica Denver Page 15 of 50
Analytical Data
Client: Waste Management Job Number: 280-94901-1
Client Sample ID:
Lab Sample ID:
3406-S03
Client Matrix:
280-94901-4
Water
Date Sampled: 03/14/2017 1330
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/24/2017 0001
03/24/2017 0001
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4631.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.19Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
115 70 - 1271,2-Dichloroethane-d4 (Surr)
99 78 - 1204-Bromofluorobenzene (Surr)
111 77 - 120Dibromofluoromethane (Surr)
102 80 - 125Toluene-d8 (Surr)
TestAmerica Denver Page 16 of 50
Analytical Data
Client: Waste Management Job Number: 280-94901-1
Client Sample ID:
Lab Sample ID:
TRIP BLANK
Client Matrix:
280-94901-5TB
Water
Date Sampled: 03/14/2017 0000
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/24/2017 0023
03/24/2017 0023
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4632.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.211,1,1,2-Tetrachloroethane
ND 1.00.161,1,1-Trichloroethane
ND 3.00.211,1,2,2-Tetrachloroethane
ND 1.00.271,1,2-Trichloroethane
ND 5.00.221,1-Dichloroethane
ND 5.00.231,1-Dichloroethene
ND 1.00.331,2,3-Trichloropropane
ND 130.471,2-Dibromo-3-Chloropropane
ND 1.00.181,2-Dibromoethane
ND 5.00.151,2-Dichlorobenzene
ND 1.00.131,2-Dichloroethane
ND 1.00.181,2-Dichloropropane
ND 1.00.161,4-Dichlorobenzene
ND 1002.02-Butanone (MEK)
ND 501.72-Hexanone
ND 1000.984-Methyl-2-pentanone (MIBK)
ND 1001.9Acetone
ND 2001.4Acrylonitrile
ND 1.00.16Benzene
ND 3.00.10Bromochloromethane
ND 1.00.17Bromodichloromethane
ND 3.00.19Bromoform
ND 100.21Bromomethane
ND 1000.45Carbon disulfide
ND 1.00.19Carbon tetrachloride
ND 3.00.17Chlorobenzene
ND 100.41Chloroethane
ND 5.00.16Chloroform
ND 1.00.30Chloromethane
ND 5.00.15cis-1,2-Dichloroethene
ND 1.00.16cis-1,3-Dichloropropene
ND 3.00.17Dibromochloromethane
ND 100.17Dibromomethane
ND 1.00.16Ethylbenzene
ND 100.23Iodomethane
ND 1.00.32Methylene Chloride
ND 1.00.17Styrene
ND 1.00.20Tetrachloroethene
ND 1.00.17Toluene
ND 5.00.15trans-1,2-Dichloroethene
ND 1.00.19trans-1,3-Dichloropropene
ND 1000.80trans-1,4-Dichloro-2-butene
ND 1.00.16Trichloroethene
ND 1.00.29Trichlorofluoromethane
ND 500.94Vinyl acetate
ND 1.00.10Vinyl chloride
TestAmerica Denver Page 17 of 50
Analytical Data
Client: Waste Management Job Number: 280-94901-1
Client Sample ID:
Lab Sample ID:
TRIP BLANK
Client Matrix:
280-94901-5TB
Water
Date Sampled: 03/14/2017 0000
Date Received: 03/16/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
03/24/2017 0023
03/24/2017 0023
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
MS9_4632.D
20 mL
20 mL
5030B
VMS_MS9
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-366626
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.19Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
112 70 - 1271,2-Dichloroethane-d4 (Surr)
95 78 - 1204-Bromofluorobenzene (Surr)
106 77 - 120Dibromofluoromethane (Surr)
99 80 - 125Toluene-d8 (Surr)
TestAmerica Denver Page 18 of 50
Analytical Data
Client: Waste Management Job Number: 280-94901-1
Client Sample ID:
Lab Sample ID:
3406-S02
Client Matrix:
280-94901-1
Water
Date Sampled: 03/14/2017 1430
Date Received: 03/16/2017 0855
6010C Metals (ICP)-Total Recoverable
6010C Instrument ID:
Lab File ID:51a032417.csv
Dilution:1.0 Initial Weight/Volume:50 mL
03/24/2017 2322 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_051
Analysis Date:
Prep Date:
Analysis Batch:280-366869
280-366366Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
37 J 1000.82Barium
1.8 J 100.66Chromium
ND 101.2Cobalt
ND 502.6Nickel
ND 100.93Silver
6010C Instrument ID:
Lab File ID:51a032717.csv
Dilution:1.0 Initial Weight/Volume:50 mL
03/27/2017 2340 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_051
Analysis Date:
Prep Date:
Analysis Batch:280-367053
280-366366Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 1.00.47Beryllium
ND 102.7Lead
2.9 J 251.1Vanadium
6020A Metals (ICP/MS)-Total Recoverable
6020A Instrument ID:
Lab File ID:208SMPL_li032417.D
Dilution:1.0 Initial Weight/Volume:50 mL
03/25/2017 0131 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_077
Analysis Date:
Prep Date:
Analysis Batch:280-366863
280-366367Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
0.41 J 6.00.40Antimony
0.33 J 100.33Arsenic
ND 1.00.27Cadmium
1.8 J ^100.56Copper
ND 100.70Selenium
ND 5.50.050Thallium
4.4 J 102.0Zinc
TestAmerica Denver Page 19 of 50
Analytical Data
Client: Waste Management Job Number: 280-94901-1
Client Sample ID:
Lab Sample ID:
3406-S05
Client Matrix:
280-94901-2
Water
Date Sampled: 03/14/2017 1405
Date Received: 03/16/2017 0855
6010C Metals (ICP)-Total Recoverable
6010C Instrument ID:
Lab File ID:51a032417.csv
Dilution:1.0 Initial Weight/Volume:50 mL
03/24/2017 2325 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_051
Analysis Date:
Prep Date:
Analysis Batch:280-366869
280-366366Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
43 J 1000.82Barium
1.1 J 100.66Chromium
1.2 J 101.2Cobalt
ND 502.6Nickel
ND 100.93Silver
6010C Instrument ID:
Lab File ID:51a032717.csv
Dilution:1.0 Initial Weight/Volume:50 mL
03/27/2017 2343 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_051
Analysis Date:
Prep Date:
Analysis Batch:280-367053
280-366366Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 1.00.47Beryllium
ND 102.7Lead
1.3 J 251.1Vanadium
6020A Metals (ICP/MS)-Total Recoverable
6020A Instrument ID:
Lab File ID:213SMPL_li032417.D
Dilution:1.0 Initial Weight/Volume:50 mL
03/25/2017 0150 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_077
Analysis Date:
Prep Date:
Analysis Batch:280-366863
280-366367Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 6.00.40Antimony
ND 100.33Arsenic
ND 1.00.27Cadmium
1.3 J ^100.56Copper
ND 100.70Selenium
0.065 J 5.50.050Thallium
2.5 J 102.0Zinc
TestAmerica Denver Page 20 of 50
Analytical Data
Client: Waste Management Job Number: 280-94901-1
Client Sample ID:
Lab Sample ID:
3406-S04
Client Matrix:
280-94901-3
Water
Date Sampled: 03/14/2017 1345
Date Received: 03/16/2017 0855
6010C Metals (ICP)-Total Recoverable
6010C Instrument ID:
Lab File ID:51a032417.csv
Dilution:1.0 Initial Weight/Volume:50 mL
03/24/2017 2350 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_051
Analysis Date:
Prep Date:
Analysis Batch:280-366869
280-366366Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
29 J 1000.82Barium
1.2 J 100.66Chromium
ND 101.2Cobalt
ND 502.6Nickel
ND 100.93Silver
6010C Instrument ID:
Lab File ID:51a032717.csv
Dilution:1.0 Initial Weight/Volume:50 mL
03/27/2017 2352 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_051
Analysis Date:
Prep Date:
Analysis Batch:280-367053
280-366366Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 1.00.47Beryllium
ND 102.7Lead
2.4 J 251.1Vanadium
6020A Metals (ICP/MS)-Total Recoverable
6020A Instrument ID:
Lab File ID:214SMPL_li032417.D
Dilution:1.0 Initial Weight/Volume:50 mL
03/25/2017 0154 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_077
Analysis Date:
Prep Date:
Analysis Batch:280-366863
280-366367Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 6.00.40Antimony
ND 100.33Arsenic
ND 1.00.27Cadmium
1.2 J ^100.56Copper
ND 100.70Selenium
ND 5.50.050Thallium
3.0 J 102.0Zinc
TestAmerica Denver Page 21 of 50
Analytical Data
Client: Waste Management Job Number: 280-94901-1
Client Sample ID:
Lab Sample ID:
3406-S03
Client Matrix:
280-94901-4
Water
Date Sampled: 03/14/2017 1330
Date Received: 03/16/2017 0855
6010C Metals (ICP)-Total Recoverable
6010C Instrument ID:
Lab File ID:51a032417.csv
Dilution:1.0 Initial Weight/Volume:50 mL
03/24/2017 2353 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_051
Analysis Date:
Prep Date:
Analysis Batch:280-366869
280-366366Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
29 J 1000.82Barium
1.7 J 100.66Chromium
ND 101.2Cobalt
ND 502.6Nickel
ND 100.93Silver
6010C Instrument ID:
Lab File ID:51a032717.csv
Dilution:1.0 Initial Weight/Volume:50 mL
03/27/2017 2355 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_051
Analysis Date:
Prep Date:
Analysis Batch:280-367053
280-366366Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 1.00.47Beryllium
ND 102.7Lead
3.4 J 251.1Vanadium
6020A Metals (ICP/MS)-Total Recoverable
6020A Instrument ID:
Lab File ID:218SMPL_li032417.D
Dilution:1.0 Initial Weight/Volume:50 mL
03/25/2017 0209 Final Weight/Volume:50 mL
03/24/2017 0740
3005A
MT_077
Analysis Date:
Prep Date:
Analysis Batch:280-366863
280-366367Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 6.00.40Antimony
ND 100.33Arsenic
ND 1.00.27Cadmium
1.0 J ^100.56Copper
ND 100.70Selenium
ND 5.50.050Thallium
2.1 J 102.0Zinc
TestAmerica Denver Page 22 of 50
Analytical Data
Client: Waste Management Job Number: 280-94901-1
Field Service / Mobile Lab
Client Sample ID:
Lab Sample ID:
3406-S02
Client Matrix:
280-94901-1
Water
Date Sampled: 03/14/2017 1430
Date Received: 03/16/2017 0855
Result Qual Units Dil Method
Analysis Date Analyzed
Date PreparedAnalyteBatch
Field pH 6.13 SU 1.0 Field
Sampling
280-365966 03/14/2017 1230
Field Conductivity 119 umhos/cm 1.0 Field
Sampling
280-365966 03/14/2017 1230
Field Temperature 9.5 Degrees C 1.0 Field
Sampling
280-365966 03/14/2017 1230
Field Turbidity 14.3 NTU 1.0 Field
Sampling
280-365966 03/14/2017 1230
Field Dissolved Oxygen 7.9 mg/L 1.0 Field
Sampling
280-365966 03/14/2017 1230
Field EH/ORP 109.3 millivolts 1.0 Field
Sampling
280-365966 03/14/2017 1230
TestAmerica Denver Page 23 of 50
Analytical Data
Client: Waste Management Job Number: 280-94901-1
Field Service / Mobile Lab
Client Sample ID:
Lab Sample ID:
3406-S05
Client Matrix:
280-94901-2
Water
Date Sampled: 03/14/2017 1405
Date Received: 03/16/2017 0855
Result Qual Units Dil Method
Analysis Date Analyzed
Date PreparedAnalyteBatch
Field pH 5.82 SU 1.0 Field
Sampling
280-365966 03/14/2017 1205
Field Conductivity 175 umhos/cm 1.0 Field
Sampling
280-365966 03/14/2017 1205
Field Temperature 10.1 Degrees C 1.0 Field
Sampling
280-365966 03/14/2017 1205
Field Turbidity 11.9 NTU 1.0 Field
Sampling
280-365966 03/14/2017 1205
Field Dissolved Oxygen 7.9 mg/L 1.0 Field
Sampling
280-365966 03/14/2017 1205
Field EH/ORP 164.3 millivolts 1.0 Field
Sampling
280-365966 03/14/2017 1205
TestAmerica Denver Page 24 of 50
Analytical Data
Client: Waste Management Job Number: 280-94901-1
Field Service / Mobile Lab
Client Sample ID:
Lab Sample ID:
3406-S04
Client Matrix:
280-94901-3
Water
Date Sampled: 03/14/2017 1345
Date Received: 03/16/2017 0855
Result Qual Units Dil Method
Analysis Date Analyzed
Date PreparedAnalyteBatch
Field pH 5.48 SU 1.0 Field
Sampling
280-365966 03/14/2017 1145
Field Conductivity 96 umhos/cm 1.0 Field
Sampling
280-365966 03/14/2017 1145
Field Temperature 9.9 Degrees C 1.0 Field
Sampling
280-365966 03/14/2017 1145
Field Turbidity 19.6 NTU 1.0 Field
Sampling
280-365966 03/14/2017 1145
Field Dissolved Oxygen 8.3 mg/L 1.0 Field
Sampling
280-365966 03/14/2017 1145
Field EH/ORP 214.0 millivolts 1.0 Field
Sampling
280-365966 03/14/2017 1145
TestAmerica Denver Page 25 of 50
Analytical Data
Client: Waste Management Job Number: 280-94901-1
Field Service / Mobile Lab
Client Sample ID:
Lab Sample ID:
3406-S03
Client Matrix:
280-94901-4
Water
Date Sampled: 03/14/2017 1330
Date Received: 03/16/2017 0855
Result Qual Units Dil Method
Analysis Date Analyzed
Date PreparedAnalyteBatch
Field pH 4.97 SU 1.0 Field
Sampling
280-365966 03/14/2017 1130
Field Conductivity 95 umhos/cm 1.0 Field
Sampling
280-365966 03/14/2017 1130
Field Temperature 9.1 Degrees C 1.0 Field
Sampling
280-365966 03/14/2017 1130
Field Turbidity 22.9 NTU 1.0 Field
Sampling
280-365966 03/14/2017 1130
Field Dissolved Oxygen 8.5 mg/L 1.0 Field
Sampling
280-365966 03/14/2017 1130
Field EH/ORP 203.9 millivolts 1.0 Field
Sampling
280-365966 03/14/2017 1130
TestAmerica Denver Page 26 of 50
DATA REPORTING QUALIFIERS
Client: Waste Management Job Number: 280-94901-1
Lab Section Qualifier Description
GC/MS VOA
MS/MSD RPD exceeds control limitsF2
Result is less than the RL but greater than or equal to the MDL and the
concentration is an approximate value.
J
Metals
ICV,CCV,ICB,CCB, ISA, ISB, CRI, CRA, DLCK or MRL standard:
Instrument related QC is outside acceptance limits.
^
Result is less than the RL but greater than or equal to the MDL and the
concentration is an approximate value.
J
TestAmerica Denver Page 27 of 50
QUALITY CONTROL RESULTS
TestAmerica Denver
Page 28 of 50
Quality Control Results
Client: Waste Management Job Number: 280-94901-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
GC/MS VOA
Analysis Batch:280-366626
Lab Control Sample Water 8260BLCS 280-366626/4 T
Method Blank Water 8260BMB 280-366626/6 T
Water3406-S02 8260B280-94901-1 T
Matrix Spike Water 8260B280-94901-1MS T
Matrix Spike Duplicate Water 8260B280-94901-1MSD T
Water3406-S05 8260B280-94901-2 T
Water3406-S04 8260B280-94901-3 T
Water3406-S03 8260B280-94901-4 T
WaterTRIP BLANK 8260B280-94901-5TB T
Report Basis
T = Total
Metals
Prep Batch: 280-366366
Lab Control Sample Water 3005ALCS 280-366366/2-A R
Method Blank Water 3005AMB 280-366366/1-A R
Water3406-S02 3005A280-94901-1 R
Water3406-S05 3005A280-94901-2 R
Matrix Spike Water 3005A280-94901-2MS R
Matrix Spike Duplicate Water 3005A280-94901-2MSD R
Water3406-S04 3005A280-94901-3 R
Water3406-S03 3005A280-94901-4 R
Matrix Spike Water 3005A280-94905-A-2-B MS R
Matrix Spike Duplicate Water 3005A280-94905-A-2-C MSD R
Prep Batch: 280-366367
Lab Control Sample Water 3005ALCS 280-366367/2-A R
Method Blank Water 3005AMB 280-366367/1-A R
Water3406-S02 3005A280-94901-1 R
Matrix Spike Water 3005A280-94901-1MS R
Matrix Spike Duplicate Water 3005A280-94901-1MSD R
Water3406-S05 3005A280-94901-2 R
Water3406-S04 3005A280-94901-3 R
Water3406-S03 3005A280-94901-4 R
Analysis Batch:280-366863
Lab Control Sample Water 280-3663676020ALCS 280-366367/2-A R
Method Blank Water 280-3663676020AMB 280-366367/1-A R
Water 280-3663673406-S02 6020A280-94901-1 R
Matrix Spike Water 280-3663676020A280-94901-1MS R
Matrix Spike Duplicate Water 280-3663676020A280-94901-1MSD R
Water 280-3663673406-S05 6020A280-94901-2 R
Water 280-3663673406-S04 6020A280-94901-3 R
Water 280-3663673406-S03 6020A280-94901-4 R
TestAmerica Denver
Page 29 of 50
Quality Control Results
Client: Waste Management Job Number: 280-94901-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
Metals
Analysis Batch:280-366869
Lab Control Sample Water 280-3663666010CLCS 280-366366/2-A R
Method Blank Water 280-3663666010CMB 280-366366/1-A R
Water 280-3663663406-S02 6010C280-94901-1 R
Water 280-3663663406-S05 6010C280-94901-2 R
Matrix Spike Water 280-3663666010C280-94901-2MS R
Matrix Spike Duplicate Water 280-3663666010C280-94901-2MSD R
Water 280-3663663406-S04 6010C280-94901-3 R
Water 280-3663663406-S03 6010C280-94901-4 R
Analysis Batch:280-367053
Lab Control Sample Water 280-3663666010CLCS 280-366366/2-A R
Method Blank Water 280-3663666010CMB 280-366366/1-A R
Water 280-3663663406-S02 6010C280-94901-1 R
Water 280-3663663406-S05 6010C280-94901-2 R
Matrix Spike Duplicate Water 280-3663666010C280-94901-2MSD R
Water 280-3663663406-S04 6010C280-94901-3 R
Water 280-3663663406-S03 6010C280-94901-4 R
Matrix Spike Water 280-3663666010C280-94905-A-2-B MS R
Matrix Spike Duplicate Water 280-3663666010C280-94905-A-2-C MSD R
Report Basis
R = Total Recoverable
Field Service / Mobile Lab
Analysis Batch:280-365966
Water3406-S02 Field Sampling280-94901-1 T
Water3406-S05 Field Sampling280-94901-2 T
Water3406-S04 Field Sampling280-94901-3 T
Water3406-S03 Field Sampling280-94901-4 T
Report Basis
T = Total
TestAmerica Denver
Page 30 of 50
Quality Control Results
Job Number: 280-94901-1Client: Waste Management
Surrogate Recovery Report
8260B Volatile Organic Compounds (GC/MS)
Client Matrix: Water
Lab Sample ID Client Sample ID
DCA BFB DBFM TOL
%Rec %Rec %Rec %Rec
280-94901-1 3406-S02 95 95 97 103
280-94901-2 3406-S05 104 105 105 111
280-94901-3 3406-S04 119 101 115 106
280-94901-4 3406-S03 115 99 111 102
280-94901-5 TRIP BLANK 112 95 106 99
MB 280-366626/6 121 104 117 109
LCS 280-366626/4 112 97 108 102
280-94901-1 MS 3406-S02 MS 106 95 105 103
280-94901-1 MSD 3406-S02 MSD 110 95 107 100
Surrogate Acceptance Limits
DCA = 1,2-Dichloroethane-d4 (Surr)70-127
BFB = 4-Bromofluorobenzene (Surr)78-120
DBFM = Dibromofluoromethane (Surr)77-120
TOL = Toluene-d8 (Surr)80-125
TestAmerica Denver
Page 31 of 50
Quality Control Results
Job Number: 280-94901-1Client: Waste Management
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 280-366626
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
MS9_4622.D
20 mL
20 mLUnits:ug/L
Method: 8260B
Preparation: 5030B
VMS_MS9MB 280-366626/6
Analysis Date:03/23/2017 2042
Analysis Batch:
Prep Batch:
Leach Batch:
N/A
N/A
280-366626
Prep Date:
Leach Date:
03/23/2017 2042
N/A
Analyte RLMDLQualResult
ND 5.00.211,1,1,2-Tetrachloroethane
ND 1.00.161,1,1-Trichloroethane
ND 3.00.211,1,2,2-Tetrachloroethane
ND 1.00.271,1,2-Trichloroethane
ND 5.00.221,1-Dichloroethane
ND 5.00.231,1-Dichloroethene
ND 1.00.331,2,3-Trichloropropane
ND 130.471,2-Dibromo-3-Chloropropane
ND 1.00.181,2-Dibromoethane
ND 5.00.151,2-Dichlorobenzene
ND 1.00.131,2-Dichloroethane
ND 1.00.181,2-Dichloropropane
ND 1.00.161,4-Dichlorobenzene
ND 1002.02-Butanone (MEK)
ND 501.72-Hexanone
ND 1000.984-Methyl-2-pentanone (MIBK)
ND 1001.9Acetone
ND 2001.4Acrylonitrile
ND 1.00.16Benzene
ND 3.00.10Bromochloromethane
ND 1.00.17Bromodichloromethane
ND 3.00.19Bromoform
ND 100.21Bromomethane
ND 1000.45Carbon disulfide
ND 1.00.19Carbon tetrachloride
ND 3.00.17Chlorobenzene
ND 100.41Chloroethane
ND 5.00.16Chloroform
ND 1.00.30Chloromethane
ND 5.00.15cis-1,2-Dichloroethene
ND 1.00.16cis-1,3-Dichloropropene
ND 3.00.17Dibromochloromethane
ND 100.17Dibromomethane
ND 1.00.16Ethylbenzene
ND 100.23Iodomethane
ND 1.00.32Methylene Chloride
ND 1.00.17Styrene
ND 1.00.20Tetrachloroethene
ND 1.00.17Toluene
ND 5.00.15trans-1,2-Dichloroethene
ND 1.00.19trans-1,3-Dichloropropene
ND 1000.80trans-1,4-Dichloro-2-butene
ND 1.00.16Trichloroethene
ND 1.00.29Trichlorofluoromethane
ND 500.94Vinyl acetate
TestAmerica Denver Page 32 of 50
Quality Control Results
Job Number: 280-94901-1Client: Waste Management
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 280-366626
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
MS9_4622.D
20 mL
20 mLUnits:ug/L
Method: 8260B
Preparation: 5030B
VMS_MS9MB 280-366626/6
Analysis Date:03/23/2017 2042
Analysis Batch:
Prep Batch:
Leach Batch:
N/A
N/A
280-366626
Prep Date:
Leach Date:
03/23/2017 2042
N/A
Analyte RLMDLQualResult
ND 1.00.10Vinyl chloride
ND 5.00.19Xylenes, Total
Surrogate % Rec Acceptance Limits
1,2-Dichloroethane-d4 (Surr)121 70 - 127
4-Bromofluorobenzene (Surr)104 78 - 120
Dibromofluoromethane (Surr)117 77 - 120
Toluene-d8 (Surr)109 80 - 125
Water
1.0
Lab Control Sample - Batch: 280-366626
Client Matrix:
Lab Sample ID:
Dilution:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
MS9_4621.D
20 mL
20 mLUnits:ug/L
Method: 8260B
Preparation: 5030B
VMS_MS9LCS 280-366626/4
Analysis Date:03/23/2017 2021
Analysis Batch:
Prep Batch:
Leach Batch:
280-366626
N/A
N/A
Prep Date:
Leach Date:
03/23/2017 2021
N/A
Analyte QualLimit% Rec.ResultSpike Amount
5.00 4.83 97 65 - 1351,1,1-Trichloroethane
5.00 4.84 97 J65 - 1351,1-Dichloroethane
5.00 4.42 88 J65 - 1361,1-Dichloroethene
5.00 5.04 101 64 - 1351,2-Dichloropropane
5.00 4.18 84 65 - 1351,3-Dichlorobenzene
5.00 4.86 97 65 - 135Benzene
5.00 4.70 94 65 - 135Bromodichloromethane
5.00 4.90 98 65 - 135Carbon tetrachloride
5.00 4.33 87 65 - 135Chlorobenzene
5.00 4.90 98 J65 - 135Chloroform
5.00 4.29 86 65 - 135Ethylbenzene
5.00 4.42 88 54 - 141Methylene Chloride
5.00 4.22 84 65 - 135Tetrachloroethene
5.00 4.77 95 65 - 135Toluene
5.00 4.85 97 J65 - 135trans-1,2-Dichloroethene
5.00 4.57 91 65 - 135Trichloroethene
Surrogate % Rec Acceptance Limits
1,2-Dichloroethane-d4 (Surr)112 70 - 127
4-Bromofluorobenzene (Surr)97 78 - 120
Dibromofluoromethane (Surr)108 77 - 120
Toluene-d8 (Surr)102 80 - 125
TestAmerica Denver Page 33 of 50
Quality Control Results
Job Number: 280-94901-1Client: Waste Management
Dilution:
Dilution:
Water
1.0
1.0
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix:Water
MS9_4624.D
20 mL
20 mL
20 mL
MS9_4625.D
20 mL
20 mL
20 mL
Method: 8260B
Preparation: 5030B
VMS_MS9
VMS_MS9
280-94901-1
280-94901-1
MS Lab Sample ID:
MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-366626
03/23/2017 2131
N/A
Analysis Date:
Prep Date:
Leach Date:
Analysis Batch:
Prep Batch:
Leach Batch:
280-366626
N/A
N/A
Analysis Date:
Prep Date:
Leach Date:
03/23/2017 2152
03/23/2017 2152
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
280-366626
N/A
N/A
03/23/2017 2131
Analyte RPD LimitRPDLimit
% Rec.
MS MSD MS Qual MSD Qual
101 103 65 - 135 3 201,1,1-Trichloroethane
98 103 65 - 135 6 21 J1,1-Dichloroethane
92 96 65 - 136 3 20 J J1,1-Dichloroethene
99 107 64 - 135 7 201,2-Dichloropropane
86 89 65 - 135 3 201,3-Dichlorobenzene
99 104 65 - 135 5 20Benzene
95 102 65 - 135 7 20Bromodichloromethane
101 105 65 - 135 3 21Carbon tetrachloride
89 93 65 - 135 3 20Chlorobenzene
100 104 65 - 135 4 20 JChloroform
89 91 65 - 135 2 20Ethylbenzene
80 92 54 - 141 14 26Methylene Chloride
88 89 65 - 135 1 20Tetrachloroethene
98 103 65 - 135 5 20Toluene
98 103 65 - 135 4 24 Jtrans-1,2-Dichloroethene
95 98 65 - 135 3 20Trichloroethene
Surrogate Acceptance LimitsMS % Rec MSD % Rec
1,2-Dichloroethane-d4 (Surr)106 110 70 - 127
4-Bromofluorobenzene (Surr)95 95 78 - 120
Dibromofluoromethane (Surr)105 107 77 - 120
Toluene-d8 (Surr)103 100 80 - 125
TestAmerica Denver Page 34 of 50
Quality Control Results
Job Number: 280-94901-1Client: Waste Management
Water
03/23/2017 2131 03/23/2017 2152
Dilution:Dilution:1.0 1.0
Client Matrix:Client Matrix:Water
Method: 8260B
Preparation: 5030B
Units:ug/L280-94901-1 280-94901-1MS Lab Sample ID:MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-366626
Analysis Date:
Prep Date:
Leach Date:
03/23/2017 2131
N/A
Analysis Date:
Prep Date:
Leach Date:
03/23/2017 2152
N/A
Amount
Sample
Analyte Result/Qual Amount Result/Qual Result/Qual
MS MSDMS Spike MSD Spike
ND 5.00 5.00 5.04 5.171,1,1-Trichloroethane
ND 5.00 5.00 4.89 5.17J1,1-Dichloroethane
ND 5.00 5.00 4.62 4.78J J1,1-Dichloroethene
ND 5.00 5.00 4.97 5.351,2-Dichloropropane
ND 5.00 5.00 4.32 4.461,3-Dichlorobenzene
ND 5.00 5.00 4.94 5.19Benzene
ND 5.00 5.00 4.74 5.09Bromodichloromethane
ND 5.00 5.00 5.07 5.23Carbon tetrachloride
ND 5.00 5.00 4.47 4.63Chlorobenzene
ND 5.00 5.00 4.98 5.21JChloroform
ND 5.00 5.00 4.44 4.53Ethylbenzene
ND 5.00 5.00 4.00 4.59Methylene Chloride
ND 5.00 5.00 4.41 4.46Tetrachloroethene
ND 5.00 5.00 4.88 5.15Toluene
ND 5.00 5.00 4.92 5.13Jtrans-1,2-Dichloroethene
ND 5.00 5.00 4.76 4.90Trichloroethene
TestAmerica Denver Page 35 of 50
Quality Control Results
Job Number: 280-94901-1Client: Waste Management
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 280-366366
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
51a032417.csv
50 mL
50 mLUnits:ug/L
Method: 6010C
Preparation: 3005A
Total Recoverable
MT_051MB 280-366366/1-A
Analysis Date:03/24/2017 2316
Analysis Batch:
Prep Batch:
Leach Batch:N/A
280-366869
280-366366
Prep Date:
Leach Date:
03/24/2017 0740
N/A
Analyte RLMDLQualResult
ND 1000.82Barium
ND 100.66Chromium
ND 101.2Cobalt
ND 502.6Nickel
ND 100.93Silver
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 280-366366
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
51a032717.csv
50 mL
50 mLUnits:ug/L
Method: 6010C
Preparation: 3005A
Total Recoverable
MT_051MB 280-366366/1-A
Analysis Date:03/27/2017 2335
Analysis Batch:
Prep Batch:
Leach Batch:N/A
280-367053
280-366366
Prep Date:
Leach Date:
03/24/2017 0740
N/A
Analyte RLMDLQualResult
ND 1.00.47Beryllium
ND 102.7Lead
ND 251.1Vanadium
TestAmerica Denver Page 36 of 50
Quality Control Results
Job Number: 280-94901-1Client: Waste Management
Water
1.0
Lab Control Sample - Batch: 280-366366
Client Matrix:
Lab Sample ID:
Dilution:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
51a032417.csv
50 mL
50 mLUnits:ug/L
Method: 6010C
Preparation: 3005A
Total Recoverable
MT_051LCS 280-366366/2-A
Analysis Date:03/24/2017 2319
Analysis Batch:
Prep Batch:
Leach Batch:
280-366869
280-366366
N/A
Prep Date:
Leach Date:
03/24/2017 0740
N/A
Analyte QualLimit% Rec.ResultSpike Amount
2000 2170 108 90 - 112Barium
200 222 111 90 - 113Chromium
500 541 108 89 - 111Cobalt
500 538 108 89 - 111Nickel
50.0 57.7 115 86 - 115Silver
Water
1.0
Lab Control Sample - Batch: 280-366366
Client Matrix:
Lab Sample ID:
Dilution:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
51a032717.csv
50 mL
50 mLUnits:ug/L
Method: 6010C
Preparation: 3005A
Total Recoverable
MT_051LCS 280-366366/2-A
Analysis Date:03/27/2017 2338
Analysis Batch:
Prep Batch:
Leach Batch:
280-367053
280-366366
N/A
Prep Date:
Leach Date:
03/24/2017 0740
N/A
Analyte QualLimit% Rec.ResultSpike Amount
50.0 49.1 98 89 - 113Beryllium
500 491 98 89 - 110Lead
500 495 99 90 - 111Vanadium
TestAmerica Denver Page 37 of 50
Quality Control Results
Job Number: 280-94901-1Client: Waste Management
Dilution:
Dilution:
Water
1.0
1.0
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix:Water
51a032717.csv
50 mL
50 mL
51a032717.csv
50 mL
50 mL
Method: 6010C
Preparation: 3005A
Total Recoverable
MT_051
MT_051
280-94905-A-2-B MS
280-94905-A-2-C MSD
MS Lab Sample ID:
MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-366366
03/28/2017 0058
N/A
Analysis Date:
Prep Date:
Leach Date:
Analysis Batch:
Prep Batch:
Leach Batch:
280-367053
280-366366
N/A
Analysis Date:
Prep Date:
Leach Date:
03/28/2017 0101
03/24/2017 0740
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
280-367053
280-366366
N/A
03/24/2017 0740
Analyte RPD LimitRPDLimit
% Rec.
MS MSD MS Qual MSD Qual
101 99 85 - 120 2 20Barium
99 97 79 - 121 1 20Beryllium
99 98 73 - 135 1 20Chromium
94 93 82 - 119 2 20Cobalt
98 96 89 - 121 2 20Lead
95 94 84 - 120 1 20Nickel
99 97 85 - 120 2 20Vanadium
101 100 75 - 141 1 20Silver
Water
03/28/2017 0058 03/28/2017 0101
Dilution:Dilution:1.0 1.0
Client Matrix:Client Matrix:Water
Method: 6010C
Preparation: 3005A
Total Recoverable
Units:ug/L280-94905-A-2-B MS 280-94905-A-2-C MSDMS Lab Sample ID:MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-366366
Analysis Date:
Prep Date:
Leach Date:
03/24/2017 0740
N/A
Analysis Date:
Prep Date:
Leach Date:
03/24/2017 0740
N/A
Amount
Sample
Analyte Result/Qual Amount Result/Qual Result/Qual
MS MSDMS Spike MSD Spike
5.1 J 2000 2000 2030 1990Barium
ND 50.0 50.0 49.3 48.6Beryllium
1.1 J 200 200 200 198Chromium
ND 500 500 470 463Cobalt
ND 500 500 488 480Lead
ND 500 500 475 469Nickel
6.8 J 500 500 501 493Vanadium
ND 50.0 50.0 50.6 49.9Silver
TestAmerica Denver Page 38 of 50
Quality Control Results
Job Number: 280-94901-1Client: Waste Management
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 280-366367
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
206_BLK_li032417.D
50 mL
50 mLUnits:ug/L
Method: 6020A
Preparation: 3005A
Total Recoverable
MT_077MB 280-366367/1-A
Analysis Date:03/25/2017 0123
Analysis Batch:
Prep Batch:
Leach Batch:N/A
280-366863
280-366367
Prep Date:
Leach Date:
03/24/2017 0740
N/A
Analyte RLMDLQualResult
ND 6.00.40Antimony
ND 100.33Arsenic
ND 1.00.27Cadmium
ND 100.56Copper
ND 100.70Selenium
ND 5.50.050Thallium
ND 102.0Zinc
Water
1.0
Lab Control Sample - Batch: 280-366367
Client Matrix:
Lab Sample ID:
Dilution:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
207_LCS_li032417.D
50 mL
50 mLUnits:ug/L
Method: 6020A
Preparation: 3005A
Total Recoverable
MT_077LCS 280-366367/2-A
Analysis Date:03/25/2017 0127
Analysis Batch:
Prep Batch:
Leach Batch:
280-366863
280-366367
N/A
Prep Date:
Leach Date:
03/24/2017 0740
N/A
Analyte QualLimit% Rec.ResultSpike Amount
40.0 37.6 94 85 - 115Antimony
40.0 38.4 96 85 - 117Arsenic
40.0 39.9 100 85 - 115Cadmium
40.0 40.4 101 85 - 119Copper
40.0 38.6 97 77 - 122Selenium
40.0 40.1 100 85 - 118Thallium
40.0 39.4 98 83 - 122Zinc
TestAmerica Denver Page 39 of 50
Quality Control Results
Job Number: 280-94901-1Client: Waste Management
Dilution:
Dilution:
Water
1.0
1.0
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix:Water
210SMPL_li032417.D
50 mL
50 mL
211SMPL_li032417.D
50 mL
50 mL
Method: 6020A
Preparation: 3005A
Total Recoverable
MT_077
MT_077
280-94901-1
280-94901-1
MS Lab Sample ID:
MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-366367
03/25/2017 0139
N/A
Analysis Date:
Prep Date:
Leach Date:
Analysis Batch:
Prep Batch:
Leach Batch:
280-366863
280-366367
N/A
Analysis Date:
Prep Date:
Leach Date:
03/25/2017 0142
03/24/2017 0740
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
280-366863
280-366367
N/A
03/24/2017 0740
Analyte RPD LimitRPDLimit
% Rec.
MS MSD MS Qual MSD Qual
92 93 85 - 115 1 20Antimony
94 92 85 - 117 2 20Arsenic
97 96 85 - 115 1 20Cadmium
101 101 85 - 119 0 20Copper
94 94 77 - 122 0 20Selenium
99 100 85 - 118 1 20Thallium
94 96 83 - 122 2 20Zinc
Water
03/25/2017 0139 03/25/2017 0142
Dilution:Dilution:1.0 1.0
Client Matrix:Client Matrix:Water
Method: 6020A
Preparation: 3005A
Total Recoverable
Units:ug/L280-94901-1 280-94901-1MS Lab Sample ID:MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-366367
Analysis Date:
Prep Date:
Leach Date:
03/24/2017 0740
N/A
Analysis Date:
Prep Date:
Leach Date:
03/24/2017 0740
N/A
Amount
Sample
Analyte Result/Qual Amount Result/Qual Result/Qual
MS MSDMS Spike MSD Spike
0.41 J 40.0 40.0 37.2 37.4Antimony
0.33 J 40.0 40.0 37.6 36.9Arsenic
ND 40.0 40.0 38.9 38.4Cadmium
1.8 J 40.0 40.0 42.0 42.0Copper
ND 40.0 40.0 37.7 37.7Selenium
ND 40.0 40.0 39.6 40.1Thallium
4.4 J 40.0 40.0 42.0 42.7Zinc
TestAmerica Denver Page 40 of 50
Quality Control Results
Client: Waste Management Job Number: 280-94901-1
Laboratory Chronicle
03/16/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:03/14/2017 14:30
280-94901-1 3406-S02
P:5030B 280-94901-D-1 280-366626 03/23/2017 21:09 JNLTAL DEN1
A:8260B 280-94901-D-1 280-366626 03/23/2017 21:09 JNLTAL DEN1
P:3005A 280-94901-A-1-A 280-366869 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94901-A-1-A 280-366869 280-366366 03/24/2017 23:22 CMLTAL DEN1
P:3005A 280-94901-A-1-A 280-367053 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94901-A-1-A 280-367053 280-366366 03/27/2017 23:40 LLBTAL DEN1
P:3005A 280-94901-A-1-B 280-366863 280-366367 03/24/2017 07:40 SURTAL DEN1
A:6020A 280-94901-A-1-B 280-366863 280-366367 03/25/2017 01:31 LMTTAL DEN1
A:Field Sampling 280-94901-A-1 280-365966 03/14/2017 12:30 C1KTAL DEN1
03/16/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:03/14/2017 14:30
280-94901-1 MS 3406-S02
P:5030B 280-94901-C-1 MS 280-366626 03/23/2017 21:31 JNLTAL DEN1
A:8260B 280-94901-C-1 MS 280-366626 03/23/2017 21:31 JNLTAL DEN1
P:3005A 280-94901-A-1-C MS 280-366863 280-366367 03/24/2017 07:40 SURTAL DEN1
A:6020A 280-94901-A-1-C MS 280-366863 280-366367 03/25/2017 01:39 LMTTAL DEN1
03/16/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:03/14/2017 14:30
280-94901-1 MSD 3406-S02
P:5030B 280-94901-C-1 MSD 280-366626 03/23/2017 21:52 JNLTAL DEN1
A:8260B 280-94901-C-1 MSD 280-366626 03/23/2017 21:52 JNLTAL DEN1
P:3005A 280-94901-A-1-D
MSD
280-366863 280-366367 03/24/2017 07:40 SURTAL DEN1
A:6020A 280-94901-A-1-D
MSD
280-366863 280-366367 03/25/2017 01:42 LMTTAL DEN1
A = Analytical Method P = Prep Method TestAmerica Denver
Page 41 of 50
Quality Control Results
Client: Waste Management Job Number: 280-94901-1
Laboratory Chronicle
03/16/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:03/14/2017 14:05
280-94901-2 3406-S05
P:5030B 280-94901-D-2 280-366626 03/23/2017 23:18 JNLTAL DEN1
A:8260B 280-94901-D-2 280-366626 03/23/2017 23:18 JNLTAL DEN1
P:3005A 280-94901-A-2-A 280-366869 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94901-A-2-A 280-366869 280-366366 03/24/2017 23:25 CMLTAL DEN1
P:3005A 280-94901-A-2-A 280-367053 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94901-A-2-A 280-367053 280-366366 03/27/2017 23:43 LLBTAL DEN1
P:3005A 280-94901-A-2-D 280-366863 280-366367 03/24/2017 07:40 SURTAL DEN1
A:6020A 280-94901-A-2-D 280-366863 280-366367 03/25/2017 01:50 LMTTAL DEN1
A:Field Sampling 280-94901-A-2 280-365966 03/14/2017 12:05 C1KTAL DEN1
03/16/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:03/14/2017 14:05
280-94901-2 MS 3406-S05
P:3005A 280-94901-A-2-B MS 280-366869 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94901-A-2-B MS 280-366869 280-366366 03/24/2017 23:42 CMLTAL DEN1
03/16/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:03/14/2017 14:05
280-94901-2 MSD 3406-S05
P:3005A 280-94901-A-2-C
MSD
280-366869 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94901-A-2-C
MSD
280-366869 280-366366 03/24/2017 23:45 CMLTAL DEN1
P:3005A 280-94901-A-2-C
MSD
280-367053 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94901-A-2-C
MSD
280-367053 280-366366 03/27/2017 23:49 LLBTAL DEN1
A = Analytical Method P = Prep Method TestAmerica Denver
Page 42 of 50
Quality Control Results
Client: Waste Management Job Number: 280-94901-1
Laboratory Chronicle
03/16/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:03/14/2017 13:45
280-94901-3 3406-S04
P:5030B 280-94901-D-3 280-366626 03/23/2017 23:40 JNLTAL DEN1
A:8260B 280-94901-D-3 280-366626 03/23/2017 23:40 JNLTAL DEN1
P:3005A 280-94901-A-3-A 280-366869 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94901-A-3-A 280-366869 280-366366 03/24/2017 23:50 CMLTAL DEN1
P:3005A 280-94901-A-3-A 280-367053 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94901-A-3-A 280-367053 280-366366 03/27/2017 23:52 LLBTAL DEN1
P:3005A 280-94901-A-3-B 280-366863 280-366367 03/24/2017 07:40 SURTAL DEN1
A:6020A 280-94901-A-3-B 280-366863 280-366367 03/25/2017 01:54 LMTTAL DEN1
A:Field Sampling 280-94901-A-3 280-365966 03/14/2017 11:45 C1KTAL DEN1
03/16/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:03/14/2017 13:30
280-94901-4 3406-S03
P:5030B 280-94901-D-4 280-366626 03/24/2017 00:01 JNLTAL DEN1
A:8260B 280-94901-D-4 280-366626 03/24/2017 00:01 JNLTAL DEN1
P:3005A 280-94901-A-4-A 280-366869 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94901-A-4-A 280-366869 280-366366 03/24/2017 23:53 CMLTAL DEN1
P:3005A 280-94901-A-4-A 280-367053 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94901-A-4-A 280-367053 280-366366 03/27/2017 23:55 LLBTAL DEN1
P:3005A 280-94901-A-4-B 280-366863 280-366367 03/24/2017 07:40 SURTAL DEN1
A:6020A 280-94901-A-4-B 280-366863 280-366367 03/25/2017 02:09 LMTTAL DEN1
A:Field Sampling 280-94901-A-4 280-365966 03/14/2017 11:30 C1KTAL DEN1
03/16/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:03/14/2017 00:00
280-94901-5 TRIP BLANK
P:5030B 280-94901-A-5 280-366626 03/24/2017 00:23 JNLTAL DEN1
A:8260B 280-94901-A-5 280-366626 03/24/2017 00:23 JNLTAL DEN1
A = Analytical Method P = Prep Method TestAmerica Denver
Page 43 of 50
Quality Control Results
Client: Waste Management Job Number: 280-94901-1
Laboratory Chronicle
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:N/A Received Date/Time:N/A
MB N/A
P:5030B MB 280-366626/6 280-366626 03/23/2017 20:42 JNLTAL DEN1
A:8260B MB 280-366626/6 280-366626 03/23/2017 20:42 JNLTAL DEN1
P:3005A MB 280-366366/1-A 280-366869 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C MB 280-366366/1-A 280-366869 280-366366 03/24/2017 23:16 CMLTAL DEN1
P:3005A MB 280-366366/1-A 280-367053 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C MB 280-366366/1-A 280-367053 280-366366 03/27/2017 23:35 LLBTAL DEN1
P:3005A MB 280-366367/1-A 280-366863 280-366367 03/24/2017 07:40 SURTAL DEN1
A:6020A MB 280-366367/1-A 280-366863 280-366367 03/25/2017 01:23 LMTTAL DEN1
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:N/A Received Date/Time:N/A
LCS N/A
P:5030B LCS 280-366626/4 280-366626 03/23/2017 20:21 JNLTAL DEN1
A:8260B LCS 280-366626/4 280-366626 03/23/2017 20:21 JNLTAL DEN1
P:3005A LCS 280-366366/2-A 280-366869 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C LCS 280-366366/2-A 280-366869 280-366366 03/24/2017 23:19 CMLTAL DEN1
P:3005A LCS 280-366366/2-A 280-367053 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C LCS 280-366366/2-A 280-367053 280-366366 03/27/2017 23:38 LLBTAL DEN1
P:3005A LCS 280-366367/2-A 280-366863 280-366367 03/24/2017 07:40 SURTAL DEN1
A:6020A LCS 280-366367/2-A 280-366863 280-366367 03/25/2017 01:27 LMTTAL DEN1
03/16/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:03/15/2017 11:12
MS N/A
P:3005A 280-94905-A-2-B MS 280-367053 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94905-A-2-B MS 280-367053 280-366366 03/28/2017 00:58 LLBTAL DEN1
03/16/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:03/15/2017 11:12
MSD N/A
P:3005A 280-94905-A-2-C
MSD
280-367053 280-366366 03/24/2017 07:40 SURTAL DEN1
A:6010C 280-94905-A-2-C
MSD
280-367053 280-366366 03/28/2017 01:01 LLBTAL DEN1
Lab References:
TAL DEN = TestAmerica Denver
A = Analytical Method P = Prep Method TestAmerica Denver
Page 44 of 50
Page 45 of 50
Page 46 of 50
Page 47 of 50
Page 48 of 50
Page 49 of 50
Login Sample Receipt Checklist
Client: Waste Management Job Number: 280-94901-1
Login Number: 94901
Question Answer Comment
Creator: Woodworth, Sean P
List Source: TestAmerica Denver
List Number: 1
N/ARadioactivity either was not measured or, if measured, is at or below
background
TrueThe cooler's custody seal, if present, is intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the sample IDs on the containers and
the COC.
TrueSamples are received within Holding Time (Excluding tests with immediate
HTs)..
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueVOA sample vials do not have headspace or bubble is <6mm (1/4") in
diameter.
TrueIf necessary, staff have been informed of any short hold time or quick TAT
needs
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
TrueSampling Company provided.
TrueSamples received within 48 hours of sampling.
TrueSamples requiring field filtration have been filtered in the field.
TrueChlorine Residual checked.
TestAmerica Denver Page 50 of 50
ANALYTICAL REPORT
Job Number: 280-96675-1
Job Description: 134|Piedmont Landfill
For:
Waste Management
1850 Parkway Place
Suite 600
Marietta, GA 30067
Attention: Mr. Al Lacsamana
_____________________________________________
Approved for release.
Betsy A Sara
Project Manager II
5/23/2017 3:50 PM
Betsy A Sara, Project Manager II
4955 Yarrow Street, Arvada, CO, 80002
[phone]
[e-mail]
05/23/2017
cc:Mr. Van Burbach
The test results in this report relate only to the samples in this report and meet all requirements of NELAC, with any
exceptions noted. Pursuant to NELAP, this report shall not be reproduced except in full, without the written approval of
the laboratory. All questions regarding this report should be directed to the TestAmerica Denver Project Manager.

The Lab Certification ID# is 4025.

Reporting limits are adjusted for sample size used, dilutions and moisture content if applicable.
TestAmerica Laboratories, Inc.
TestAmerica Denver 4955 Yarrow Street, Arvada, CO 80002
Tel [phone] Fax [phone] www.testamericainc.com
05/23/2017Page 1 of 69
Table of Contents
Cover Title Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Report Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Executive Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Method / Analyst Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Sample Datasheets . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Data Qualifiers . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .17
QC Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .18
Qc Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .19
Surrogate Recovery Report . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .24
Qc Reports . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .25
Laboratory Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61
Client Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .67
Sample Receipt Checklist . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .69
05/23/2017Page 2 of 69
CASE NARRATIVE
Client: Waste Management
Project: 134|Piedmont Landfill
Report Number: 280-96675-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
This report may include reporting limits (RLs) less than TestAmerica’s standard reporting limit. The reported sample results and
associated reporting limits are being used specifically to meet the needs of this project. Note that data are not normally reported to these
levels without qualification because they are inherently less reliable and potentially less defensible than required by the latest industry
standards.
Sample Receiving
The samples were received on 05/04/2017; the samples arrived in good condition, properly preserved and on ice. The temperature of the
cooler at receipt was 0.1 C.
Holding Times
The holding times were within established control limits.
Method Blanks
Total Barium, Total Sodium Method 6010C, Total Alkalinity and Bicarbonate Alkalinity Method 2320B were detected in the Method Blanks
below the project established reporting limit. No corrective action is taken for any values in Method Blanks that are below the requested
reporting limits.
All other Method Blanks were within established control limits.
Laboratory Control Samples (LCS)
All Laboratory Control Samples were within established control limits.
Matrix Spike and Matrix Spike Duplicate (MS/MSD)
The Matrix Spikes and Matrix Spike Duplicates performed on samples from other clients exhibited recoveries outside control limits for
1,2-Dichloroethane Method 8260B, Total Phosphorus Method 365.1 and Chemical Oxygen Demand (COD) Method 410.4. Because the
corresponding Laboratory Control Samples and the Method Blank samples were within control limits, these anomalies may be due to
matrix interference and no corrective action was taken.
All other MS/MSD samples were within established control limits.
Organics
The prepreserved hydrochloric acid preserved vials for Method 8260B analysis for the sample 3406-T01 exhibited pH values greater than
2. This is non-compliant with Method 8260B which requires samples to be preserved with hydrochloric acid to a pH of less than 2.
Because this sample is a leachate sample, a buffering effect was suspected.
Metals
The Method 6010C Continuing Calibration Verification (CCV) sample was above the control limits for Total Sodium. Because the sample
3406-T01 exhibited a detection of Total Sodium greater than ten times the reporting limit, corrective action was deemed unnecessary.
The bracketing Continuing Calibration Verification Samples (CCV) surrounding the Method Blank were above control limits for Total
Sodium during Method 6010C analysis. Because the data are considered to be biased high and Total Sodium was not detected in the
Method Blank sample above the reporting limit, corrective action was deemed unnecessary.
05/23/2017Page 3 of 69
EXECUTIVE SUMMARY - Detections
Client: Waste Management Job Number: 280-96675-1
Analyte Result
Reporting
Limit Units Method
Lab Sample ID Client Sample ID
Qualifier
280-96675-1 3406-T01
10 ug/L 8260B0.15 J1,2-Dichlorobenzene
3.0 ug/L 8260B4.01,4-Dichlorobenzene
100 ug/L 8260B4.7 J4-Methyl-2-pentanone (MIBK)
100 ug/L 8260B160Acetone
3.0 ug/L 8260B1.9 JBenzene
3.0 ug/L 8260B0.40 JChlorobenzene
5.0 ug/L 8260B0.63 Jcis-1,2-Dichloroethene
5.0 ug/L 8260B2.0 JEthylbenzene
5.0 ug/L 8260B1.2 JToluene
4.0 ug/L 8260B6.0Xylenes, Total
SU Field Sampling7.45Field pH
umhos/cm Field Sampling3999Field Conductivity
Degrees C Field Sampling21.3Field Temperature
NTU Field Sampling57.5Field Turbidity
mg/L Field Sampling2.1Field Dissolved Oxygen
millivolts Field Sampling30.4Field EH/ORP
6.0 mg/L 300.01400Chloride
10 mg/L 300.071Sulfate
20 mg/L 350.1840Ammonia
1.0 mg/L 365.113Phosphorus, Total
500 mg/L 410.4660Chemical Oxygen Demand
5.0 mg/L SM 2320B3100BTotal Alkalinity
5.0 mg/L SM 2320B3100BBicarbonate Alkalinity as CaCO3
40 mg/L SM 2540C3800Total Dissolved Solids
4.0 mg/L SM 2540D29Total Suspended Solids
10 mg/L SM 5310B270Total Organic Carbon - Average
25 mg/L SM5210B48Biochemical Oxygen Demand
Total Recoverable
100 ug/L 6010C190BBarium
10 ug/L 6010C80Chromium
10 ug/L 6010C23Cobalt
200 ug/L 6010C45000Calcium
15 ug/L 6010C150Copper
50 ug/L 6010C180Nickel
100 ug/L 6010C11000Iron
20 ug/L 6010C32Zinc
25 ug/L 6010C45Vanadium
200 ug/L 6010C38000Magnesium
10 ug/L 6010C610Manganese
3000 ug/L 6010C280000Potassium
5000 ug/L 6010C1200000B ^Sodium
2.0 ug/L 6020A6.7Antimony
5.0 ug/L 6020A35Arsenic
TestAmerica Denver 05/23/2017Page 4 of 69
METHOD SUMMARY
Client: Waste Management Job Number: 280-96675-1
Preparation MethodMethodLab LocationDescription
Matrix:Water
Volatile Organic Compounds (GC/MS)TAL DEN SW846 8260B
Purge and Trap TAL DEN SW846 5030B
Metals (ICP)TAL DEN SW846 6010C
Preparation, Total Recoverable or Dissolved Metals TAL DEN SW846 3005A
Metals (ICP/MS)TAL DEN SW846 6020A
Preparation, Total Recoverable or Dissolved Metals TAL DEN SW846 3005A
Mercury (CVAA)TAL DEN SW846 7470A
Preparation, Mercury TAL DEN SW846 7470A
Anions, Ion Chromatography TAL DEN MCAWW 300.0
Nitrogen, Ammonia TAL DEN MCAWW 350.1
Phosphorus, Total TAL DEN EPA 365.1
Phosphorus, Total TAL DEN MCAWW 365.2/365.3/365
COD TAL DEN MCAWW 410.4
Nitrogen, Nitrate-Nitrite TAL DEN SM Nitrate by calc
Alkalinity TAL DEN SM SM 2320B
Solids, Total Dissolved (TDS)TAL DEN SM SM 2540C
Solids, Total Suspended (TSS)TAL DEN SM SM 2540D
Organic Carbon, Total (TOC)TAL DEN SM SM 5310B
BOD, 5 Day TAL DEN SM SM5210B
Field Sampling TAL DEN EPA Field Sampling
Lab References:
TAL DEN = TestAmerica Denver
Method References:
EPA = US Environmental Protection Agency
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SM = "Standard Methods For The Examination Of Water And Wastewater"
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its
Updates.
TestAmerica Denver 05/23/2017Page 5 of 69
METHOD / ANALYST SUMMARY
Client: Waste Management Job Number: 280-96675-1
Method Analyst Analyst ID
Dukes, Aaron D ADDSW846 8260B
Broander, Laura L LLBSW846 6010C
Rhoades, Chris R CRRSW846 6010C
Mooney, Joseph C JMSW846 6020A
Henning, Christopher D CDHSW846 7470A
Krisorn, Chamaiporn 1 C1KEPA Field Sampling
Benson, Alex F AFBMCAWW 300.0
Spedale, Morgan A MASMCAWW 350.1
Spedale, Morgan A MASEPA 365.1
Jewell, Connie C CCJMCAWW 410.4
Sullivan, Roxanne K RKSSM Nitrate by calc
Duplin, Alysha 1 A1DSM SM 2320B
Pedrick, Joshua A JAPSM SM 2540C
Cherry, Scott V SVCSM SM 2540D
Jewell, Connie C CCJSM SM 5310B
Martinez, Rut S RSMSM SM5210B
TestAmerica Denver
05/23/2017Page 6 of 69
SAMPLE SUMMARY
Client: Waste Management Job Number: 280-96675-1
Client Sample IDLab Sample ID Client Matrix Sampled Received
Date/Time Date/Time
280-96675-1 3406-T01 Water 05/03/2017 1650 05/04/2017 0855
280-96675-2TB TRIP BLANK Water 05/03/2017 1600 05/04/2017 0855
TestAmerica Denver 05/23/2017Page 7 of 69
SAMPLE RESULTS
TestAmerica Denver
05/23/2017Page 8 of 69
Analytical Data
Client: Waste Management Job Number: 280-96675-1
Client Sample ID:
Lab Sample ID:
3406-T01
Client Matrix:
280-96675-1
Water
Date Sampled: 05/03/2017 1650
Date Received: 05/04/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
05/17/2017 1959
05/17/2017 1959
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
G5150.D
20 mL
20 mL
5030B
VMS_G
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-373992
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.211,1,1,2-Tetrachloroethane
ND 5.00.161,1,1-Trichloroethane
ND 3.00.211,1,2,2-Tetrachloroethane
ND 5.00.271,1,2-Trichloroethane
ND 5.00.221,1-Dichloroethane
ND 5.00.231,1-Dichloroethene
ND 8.00.331,2,3-Trichloropropane
ND 130.471,2-Dibromo-3-Chloropropane
ND 3.00.181,2-Dibromoethane
0.15 J 100.151,2-Dichlorobenzene
ND 3.00.131,2-Dichloroethane
ND 3.00.181,2-Dichloropropane
4.0 3.00.161,4-Dichlorobenzene
ND 1002.02-Butanone (MEK)
ND 501.72-Hexanone
4.7 J 1000.984-Methyl-2-pentanone (MIBK)
160 1001.9Acetone
ND 2001.4Acrylonitrile
1.9 J 3.00.16Benzene
ND 3.00.10Bromochloromethane
ND 3.00.17Bromodichloromethane
ND 3.00.19Bromoform
ND 100.21Bromomethane
ND 1000.45Carbon disulfide
ND 5.50.19Carbon tetrachloride
0.40 J 3.00.17Chlorobenzene
ND 100.41Chloroethane
ND 5.00.16Chloroform
ND 5.50.30Chloromethane
0.63 J 5.00.15cis-1,2-Dichloroethene
ND 5.50.16cis-1,3-Dichloropropene
ND 3.00.17Dibromochloromethane
ND 100.17Dibromomethane
2.0 J 5.00.16Ethylbenzene
ND 100.23Iodomethane
ND 5.50.32Methylene Chloride
ND 100.17Styrene
ND 3.00.20Tetrachloroethene
1.2 J 5.00.17Toluene
ND 5.00.15trans-1,2-Dichloroethene
ND 5.50.19trans-1,3-Dichloropropene
ND 1000.80trans-1,4-Dichloro-2-butene
ND 3.00.16Trichloroethene
ND 5.00.29Trichlorofluoromethane
ND 500.94Vinyl acetate
ND 5.50.10Vinyl chloride
TestAmerica Denver 05/23/2017Page 9 of 69
Analytical Data
Client: Waste Management Job Number: 280-96675-1
Client Sample ID:
Lab Sample ID:
3406-T01
Client Matrix:
280-96675-1
Water
Date Sampled: 05/03/2017 1650
Date Received: 05/04/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
05/17/2017 1959
05/17/2017 1959
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
G5150.D
20 mL
20 mL
5030B
VMS_G
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-373992
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
6.0 4.00.19Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
124 70 - 1271,2-Dichloroethane-d4 (Surr)
94 78 - 1204-Bromofluorobenzene (Surr)
106 77 - 120Dibromofluoromethane (Surr)
99 80 - 125Toluene-d8 (Surr)
TestAmerica Denver 05/23/2017Page 10 of 69
Analytical Data
Client: Waste Management Job Number: 280-96675-1
Client Sample ID:
Lab Sample ID:
TRIP BLANK
Client Matrix:
280-96675-2TB
Water
Date Sampled: 05/03/2017 1600
Date Received: 05/04/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
05/17/2017 1832
05/17/2017 1832
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
G5146.D
20 mL
20 mL
5030B
VMS_G
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-373992
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 5.00.211,1,1,2-Tetrachloroethane
ND 5.00.161,1,1-Trichloroethane
ND 3.00.211,1,2,2-Tetrachloroethane
ND 5.00.271,1,2-Trichloroethane
ND 5.00.221,1-Dichloroethane
ND 5.00.231,1-Dichloroethene
ND 8.00.331,2,3-Trichloropropane
ND 130.471,2-Dibromo-3-Chloropropane
ND 3.00.181,2-Dibromoethane
ND 100.151,2-Dichlorobenzene
ND 3.00.131,2-Dichloroethane
ND 3.00.181,2-Dichloropropane
ND 3.00.161,4-Dichlorobenzene
ND 1002.02-Butanone (MEK)
ND 501.72-Hexanone
ND 1000.984-Methyl-2-pentanone (MIBK)
ND 1001.9Acetone
ND 2001.4Acrylonitrile
ND 3.00.16Benzene
ND 3.00.10Bromochloromethane
ND 3.00.17Bromodichloromethane
ND 3.00.19Bromoform
ND 100.21Bromomethane
ND 1000.45Carbon disulfide
ND 5.50.19Carbon tetrachloride
ND 3.00.17Chlorobenzene
ND 100.41Chloroethane
ND 5.00.16Chloroform
ND 5.50.30Chloromethane
ND 5.00.15cis-1,2-Dichloroethene
ND 5.50.16cis-1,3-Dichloropropene
ND 3.00.17Dibromochloromethane
ND 100.17Dibromomethane
ND 5.00.16Ethylbenzene
ND 100.23Iodomethane
ND 5.50.32Methylene Chloride
ND 100.17Styrene
ND 3.00.20Tetrachloroethene
ND 5.00.17Toluene
ND 5.00.15trans-1,2-Dichloroethene
ND 5.50.19trans-1,3-Dichloropropene
ND 1000.80trans-1,4-Dichloro-2-butene
ND 3.00.16Trichloroethene
ND 5.00.29Trichlorofluoromethane
ND 500.94Vinyl acetate
ND 5.50.10Vinyl chloride
TestAmerica Denver 05/23/2017Page 11 of 69
Analytical Data
Client: Waste Management Job Number: 280-96675-1
Client Sample ID:
Lab Sample ID:
TRIP BLANK
Client Matrix:
280-96675-2TB
Water
Date Sampled: 05/03/2017 1600
Date Received: 05/04/2017 0855
8260B Volatile Organic Compounds (GC/MS)
Dilution:
05/17/2017 1832
05/17/2017 1832
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
G5146.D
20 mL
20 mL
5030B
VMS_G
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
280-373992
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 4.00.19Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
99 70 - 1271,2-Dichloroethane-d4 (Surr)
94 78 - 1204-Bromofluorobenzene (Surr)
96 77 - 120Dibromofluoromethane (Surr)
107 80 - 125Toluene-d8 (Surr)
TestAmerica Denver 05/23/2017Page 12 of 69
Analytical Data
Client: Waste Management Job Number: 280-96675-1
Client Sample ID:
Lab Sample ID:
3406-T01
Client Matrix:
280-96675-1
Water
Date Sampled: 05/03/2017 1650
Date Received: 05/04/2017 0855
6010C Metals (ICP)-Total Recoverable
6010C Instrument ID:
Lab File ID:25F051517.asc
Dilution:1.0 Initial Weight/Volume:50 mL
05/16/2017 0644 Final Weight/Volume:50 mL
05/15/2017 0716
3005A
MT_025
Analysis Date:
Prep Date:
Analysis Batch:280-373731
280-372301Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
190 B 1000.82Barium
80 100.66Chromium
23 101.2Cobalt
45000 20035Calcium
150 154.2Copper
ND 102.7Lead
180 502.6Nickel
32 204.5Zinc
45 251.1Vanadium
38000 20011Magnesium
610 100.26Manganese
ND 156.3Selenium
ND 100.93Silver
6010C Instrument ID:
Lab File ID:25B051617.asc
Dilution:1.0 Initial Weight/Volume:50 mL
05/16/2017 2039 Final Weight/Volume:50 mL
05/15/2017 0716
3005A
MT_025
Analysis Date:
Prep Date:
Analysis Batch:280-373855
280-372301Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
11000 10022Iron
1200000 B ^5000120Sodium
6010C Instrument ID:
Lab File ID:25Q051717.asc
Dilution:1.0 Initial Weight/Volume:50 mL
05/17/2017 0908 Final Weight/Volume:50 mL
05/15/2017 0716
3005A
MT_025
Analysis Date:
Prep Date:
Analysis Batch:280-373928
280-372301Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
280000 3000240Potassium
6020A Metals (ICP/MS)-Total Recoverable
6020A Instrument ID:
Lab File ID:143SMPL.d
Dilution:1.0 Initial Weight/Volume:50 mL
05/16/2017 0206 Final Weight/Volume:50 mL
05/15/2017 0716
3005A
MT_078
Analysis Date:
Prep Date:
Analysis Batch:280-373738
280-372302Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
TestAmerica Denver 05/23/2017Page 13 of 69
Analytical Data
Client: Waste Management Job Number: 280-96675-1
Client Sample ID:
Lab Sample ID:
3406-T01
Client Matrix:
280-96675-1
Water
Date Sampled: 05/03/2017 1650
Date Received: 05/04/2017 0855
6020A Metals (ICP/MS)-Total Recoverable
Analyte Result (ug/L)Qualifier MDL RL
6.7 2.00.40Antimony
35 5.00.33Arsenic
ND 1.00.080Beryllium
ND 1.00.27Cadmium
ND 1.00.050Thallium
7470A Mercury (CVAA)
7470A Instrument ID:
Lab File ID:170519aa.txt
Dilution:1.0 Initial Weight/Volume:30 mL
05/19/2017 1800 Final Weight/Volume:50 mL
05/19/2017 1135
7470A
MT_033
Analysis Date:
Prep Date:
Analysis Batch:280-374456
280-374242Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
ND 0.200.027Mercury
TestAmerica Denver 05/23/2017Page 14 of 69
Analytical Data
Client: Waste Management Job Number: 280-96675-1
General Chemistry
Client Sample ID:
Lab Sample ID:
3406-T01
Client Matrix:
280-96675-1
Water
Date Sampled: 05/03/2017 1650
Date Received: 05/04/2017 0855
Analyte Result Qual Units MDL RL Dil Method
Chloride 1400 mg/L 5.1 6.0 20 300.0
Analysis Date: 05/17/2017 1316Analysis Batch: 280-373891
Sulfate 71 mg/L 0.46 10 2.0 300.0
Analysis Date: 05/17/2017 1259Analysis Batch: 280-373891
Ammonia 840 mg/L 11 20 500 350.1
Analysis Date: 05/16/2017 1519Analysis Batch: 280-373940
Phosphorus, Total 13 mg/L 0.10 1.0 10 365.1
Analysis Date: 05/16/2017 1254Analysis Batch: 280-373778
Prep Batch: 280-373136 Prep Date: 05/11/2017 1039
Chemical Oxygen Demand 660 mg/L 41 500 10 410.4
Analysis Date: 05/18/2017 0912Analysis Batch: 280-374088
Nitrate as N ND mg/L 0.019 0.50 1.0 Nitrate by calc
Analysis Date: 05/19/2017 1151Analysis Batch: 280-374303
Total Alkalinity 3100 B mg/L 1.1 5.0 1.0 SM 2320B
Analysis Date: 05/12/2017 1839Analysis Batch: 280-373408
Bicarbonate Alkalinity as CaCO3 3100 B mg/L 1.1 5.0 1.0 SM 2320B
Analysis Date: 05/12/2017 1839Analysis Batch: 280-373408
Carbonate Alkalinity as CaCO3 ND mg/L 1.1 5.0 1.0 SM 2320B
Analysis Date: 05/12/2017 1839Analysis Batch: 280-373408
Total Dissolved Solids 3800 mg/L 19 40 1.0 SM 2540C
Analysis Date: 05/09/2017 0904Analysis Batch: 280-372777
Total Suspended Solids 29 mg/L 1.1 4.0 1.0 SM 2540D
Analysis Date: 05/05/2017 1437Analysis Batch: 280-372423
Total Organic Carbon - Average 270 mg/L 1.6 10 10 SM 5310B
Analysis Date: 05/11/2017 0822Analysis Batch: 280-373201
Biochemical Oxygen Demand 48 mg/L 3.0 25 5.0 SM5210B
Analysis Date: 05/04/2017 1655Analysis Batch: 280-372247
TestAmerica Denver 05/23/2017Page 15 of 69
Analytical Data
Client: Waste Management Job Number: 280-96675-1
Field Service / Mobile Lab
Client Sample ID:
Lab Sample ID:
3406-T01
Client Matrix:
280-96675-1
Water
Date Sampled: 05/03/2017 1650
Date Received: 05/04/2017 0855
Result Qual Units Dil Method
Analysis Date Analyzed
Date PreparedAnalyteBatch
Field pH 7.45 SU 1.0 Field
Sampling
280-372309 05/03/2017 1450
Field Conductivity 3999 umhos/cm 1.0 Field
Sampling
280-372309 05/03/2017 1450
Field Temperature 21.3 Degrees C 1.0 Field
Sampling
280-372309 05/03/2017 1450
Field Turbidity 57.5 NTU 1.0 Field
Sampling
280-372309 05/03/2017 1450
Field Dissolved Oxygen 2.1 mg/L 1.0 Field
Sampling
280-372309 05/03/2017 1450
Field EH/ORP 30.4 millivolts 1.0 Field
Sampling
280-372309 05/03/2017 1450
TestAmerica Denver 05/23/2017Page 16 of 69
DATA REPORTING QUALIFIERS
Client: Waste Management Job Number: 280-96675-1
Lab Section Qualifier Description
GC/MS VOA
MS and/or MSD Recovery is outside acceptance limits.F1
Result is less than the RL but greater than or equal to the MDL and the
concentration is an approximate value.
J
Metals
Compound was found in the blank and sample.B
ICV,CCV,ICB,CCB, ISA, ISB, CRI, CRA, DLCK or MRL standard:
Instrument related QC is outside acceptance limits.
^
MS, MSD: The analyte present in the original sample is greater than 4
times the matrix spike concentration; therefore, control limits are not
applicable.
4
Result is less than the RL but greater than or equal to the MDL and the
concentration is an approximate value.
J
General Chemistry
Compound was found in the blank and sample.B
MS and/or MSD Recovery is outside acceptance limits.F1
Result is less than the RL but greater than or equal to the MDL and the
concentration is an approximate value.
J
TestAmerica Denver 05/23/2017Page 17 of 69
QUALITY CONTROL RESULTS
TestAmerica Denver
05/23/2017Page 18 of 69
Quality Control Results
Client: Waste Management Job Number: 280-96675-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
GC/MS VOA
Analysis Batch:280-373992
Lab Control Sample Water 8260BLCS 280-373992/4 T
Method Blank Water 8260BMB 280-373992/6 T
Water3406-T01 8260B280-96675-1 T
WaterTRIP BLANK 8260B280-96675-2TB T
Matrix Spike Water 8260B280-96884-G-1 MS T
Matrix Spike Duplicate Water 8260B280-96884-G-1 MSD T
Report Basis
T = Total
Metals
Prep Batch: 280-372301
Lab Control Sample Water 3005ALCS 280-372301/2-A R
Method Blank Water 3005AMB 280-372301/1-A R
Water3406-T01 3005A280-96675-1 R
Matrix Spike Water 3005A280-96675-1MS R
Matrix Spike Duplicate Water 3005A280-96675-1MSD R
Prep Batch: 280-372302
Lab Control Sample Water 3005ALCS 280-372302/2-A R
Method Blank Water 3005AMB 280-372302/1-A R
Water3406-T01 3005A280-96675-1 R
Matrix Spike Water 3005A280-96675-1MS R
Matrix Spike Duplicate Water 3005A280-96675-1MSD R
Analysis Batch:280-373731
Lab Control Sample Water 280-3723016010CLCS 280-372301/2-A R
Method Blank Water 280-3723016010CMB 280-372301/1-A R
Water 280-3723013406-T01 6010C280-96675-1 R
Matrix Spike Water 280-3723016010C280-96675-1MS R
Matrix Spike Duplicate Water 280-3723016010C280-96675-1MSD R
Analysis Batch:280-373738
Lab Control Sample Water 280-3723026020ALCS 280-372302/2-A R
Method Blank Water 280-3723026020AMB 280-372302/1-A R
Water 280-3723023406-T01 6020A280-96675-1 R
Matrix Spike Water 280-3723026020A280-96675-1MS R
Matrix Spike Duplicate Water 280-3723026020A280-96675-1MSD R
Analysis Batch:280-373855
Lab Control Sample Water 280-3723016010CLCS 280-372301/2-A R
Method Blank Water 280-3723016010CMB 280-372301/1-A R
Water 280-3723013406-T01 6010C280-96675-1 R
Matrix Spike Water 280-3723016010C280-96675-1MS R
TestAmerica Denver
05/23/2017Page 19 of 69
Quality Control Results
Client: Waste Management Job Number: 280-96675-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
Metals
Analysis Batch:280-373855
Matrix Spike Duplicate Water 280-3723016010C280-96675-1MSD R
Analysis Batch:280-373928
Lab Control Sample Water 280-3723016010CLCS 280-372301/2-A R
Method Blank Water 280-3723016010CMB 280-372301/1-A R
Water 280-3723013406-T01 6010C280-96675-1 R
Matrix Spike Water 280-3723016010C280-96675-1MS R
Matrix Spike Duplicate Water 280-3723016010C280-96675-1MSD R
Prep Batch: 280-374242
Lab Control Sample Water 7470ALCS 280-374242/2-A T
Method Blank Water 7470AMB 280-374242/1-A T
Matrix Spike Water 7470A280-96372-H-3-B MS T
Matrix Spike Duplicate Water 7470A280-96372-H-3-C MSD T
Water3406-T01 7470A280-96675-1 T
Analysis Batch:280-374456
Lab Control Sample Water 280-3742427470ALCS 280-374242/2-A T
Method Blank Water 280-3742427470AMB 280-374242/1-A T
Matrix Spike Water 280-3742427470A280-96372-H-3-B MS T
Matrix Spike Duplicate Water 280-3742427470A280-96372-H-3-C MSD T
Water 280-3742423406-T01 7470A280-96675-1 T
Report Basis
R = Total Recoverable
T = Total
Field Service / Mobile Lab
Analysis Batch:280-372309
Water3406-T01 Field Sampling280-96675-1 T
Report Basis
T = Total
TestAmerica Denver
05/23/2017Page 20 of 69
Quality Control Results
Client: Waste Management Job Number: 280-96675-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
General Chemistry
Analysis Batch:280-372247
Lab Control Sample Water SM5210BLCS 280-372247/3 T
Method Blank Water SM5210BMB 280-372247/4 T
Water3406-T01 SM5210B280-96675-1 T
Duplicate Water SM5210B280-96678-M-1 DU T
Analysis Batch:280-372423
Lab Control Sample Water SM 2540DLCS 280-372423/1 T
Lab Control Sample Duplicate Water SM 2540DLCSD 280-372423/2 T
Method Blank Water SM 2540DMB 280-372423/3 T
Water3406-T01 SM 2540D280-96675-1 T
Duplicate Water SM 2540D280-96712-A-1 DU T
Analysis Batch:280-372777
Lab Control Sample Water SM 2540CLCS 280-372777/2 T
Method Blank Water SM 2540CMB 280-372777/1 T
Water3406-T01 SM 2540C280-96675-1 T
Duplicate Water SM 2540C280-96684-A-1 DU T
Prep Batch: 280-373136
Lab Control Sample Water 365.2/365.3/365LCS 280-373136/9-A T
Lab Control Sample Duplicate Water 365.2/365.3/365LCSD 280-373136/10-A T
Method Blank Water 365.2/365.3/365MB 280-373136/11-A T
Water3406-T01 365.2/365.3/365280-96675-1 T
Matrix Spike Water 365.2/365.3/365280-96926-A-5-B MS T
Matrix Spike Duplicate Water 365.2/365.3/365280-96926-A-5-C MSD T
Analysis Batch:280-373201
Lab Control Sample Water SM 5310BLCS 280-373201/45 T
Method Blank Water SM 5310BMB 280-373201/46 T
Matrix Spike Water SM 5310B280-96660-D-3 MS T
Matrix Spike Duplicate Water SM 5310B280-96660-D-3 MSD T
Water3406-T01 SM 5310B280-96675-1 T
Analysis Batch:280-373202
Lab Control Sample Water SM 5310BLCS 280-373202/45 T
Method Blank Water SM 5310BMB 280-373202/46 T
Matrix Spike Water SM 5310B280-96660-D-3 MS T
Matrix Spike Duplicate Water SM 5310B280-96660-D-3 MSD T
Water3406-T01 SM 5310B280-96675-1 T
TestAmerica Denver
05/23/2017Page 21 of 69
Quality Control Results
Client: Waste Management Job Number: 280-96675-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
General Chemistry
Analysis Batch:280-373408
Lab Control Sample Water SM 2320BLCS 280-373408/30 T
Lab Control Sample Water SM 2320BLCS 280-373408/4 T
Method Blank Water SM 2320BMB 280-373408/31 T
Method Blank Water SM 2320BMB 280-373408/5 T
Water3406-T01 SM 2320B280-96675-1 T
Duplicate Water SM 2320B280-96675-1DU T
Analysis Batch:280-373778
Lab Control Sample Water 280-373136365.1LCS 280-373136/9-A T
Lab Control Sample Duplicate Water 280-373136365.1LCSD 280-373136/10-A T
Method Blank Water 280-373136365.1MB 280-373136/11-A T
Water 280-3731363406-T01 365.1280-96675-1 T
Matrix Spike Water 280-373136365.1280-96926-A-5-B MS T
Matrix Spike Duplicate Water 280-373136365.1280-96926-A-5-C MSD T
Analysis Batch:280-373891
Lab Control Sample Water 300.0LCS 280-373891/4 T
Lab Control Sample Duplicate Water 300.0LCSD 280-373891/5 T
Method Blank Water 300.0MB 280-373891/6 T
Water3406-T01 300.0280-96675-1 T
Duplicate Water 300.0280-96903-E-2 DU T
Matrix Spike Water 300.0280-96903-E-2 MS T
Matrix Spike Duplicate Water 300.0280-96903-E-2 MSD T
Analysis Batch:280-373940
Lab Control Sample Water 350.1LCS 280-373940/101 T
Lab Control Sample Duplicate Water 350.1LCSD 280-373940/102 T
Method Blank Water 350.1MB 280-373940/103 T
Water3406-T01 350.1280-96675-1 T
Matrix Spike Water 350.1280-96745-A-11 MS T
Matrix Spike Duplicate Water 350.1280-96745-A-11 MSD T
Analysis Batch:280-374088
Lab Control Sample Water 410.4LCS 280-374088/3 T
Lab Control Sample Duplicate Water 410.4LCSD 280-374088/4 T
Method Blank Water 410.4MB 280-374088/5 T
Matrix Spike Water 410.4280-96659-B-1 MS T
Matrix Spike Duplicate Water 410.4280-96659-B-1 MSD T
Water3406-T01 410.4280-96675-1 T
Analysis Batch:280-374303
Method Blank Water Nitrate by calcMB 280-374303/1 T
Water3406-T01 Nitrate by calc280-96675-1 T
TestAmerica Denver
05/23/2017Page 22 of 69
Quality Control Results
Client: Waste Management Job Number: 280-96675-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
Report Basis
T = Total
TestAmerica Denver
05/23/2017Page 23 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
Surrogate Recovery Report
8260B Volatile Organic Compounds (GC/MS)
Client Matrix: Water
Lab Sample ID Client Sample ID
DCA BFB DBFM TOL
%Rec %Rec %Rec %Rec
280-96675-1 3406-T01 124 94 106 99
280-96675-2 TRIP BLANK 99 94 96 107
MB 280-373992/6 115 97 107 107
LCS 280-373992/4 112 96 103 100
280-96884-G-1 MS 112 93 103 103
280-96884-G-1 MSD 115 99 105 100
Surrogate Acceptance Limits
DCA = 1,2-Dichloroethane-d4 (Surr)70-127
BFB = 4-Bromofluorobenzene (Surr)78-120
DBFM = Dibromofluoromethane (Surr)77-120
TOL = Toluene-d8 (Surr)80-125
TestAmerica Denver
05/23/2017Page 24 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 280-373992
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
G5144.D
20 mL
20 mLUnits:ug/L
Method: 8260B
Preparation: 5030B
VMS_GMB 280-373992/6
Analysis Date:05/17/2017 1750
Analysis Batch:
Prep Batch:
Leach Batch:
N/A
N/A
280-373992
Prep Date:
Leach Date:
05/17/2017 1750
N/A
Analyte RLMDLQualResult
ND 5.00.211,1,1,2-Tetrachloroethane
ND 5.00.161,1,1-Trichloroethane
ND 3.00.211,1,2,2-Tetrachloroethane
ND 5.00.271,1,2-Trichloroethane
ND 5.00.221,1-Dichloroethane
ND 5.00.231,1-Dichloroethene
ND 8.00.331,2,3-Trichloropropane
ND 130.471,2-Dibromo-3-Chloropropane
ND 3.00.181,2-Dibromoethane
ND 100.151,2-Dichlorobenzene
ND 3.00.131,2-Dichloroethane
ND 3.00.181,2-Dichloropropane
ND 3.00.161,4-Dichlorobenzene
ND 1002.02-Butanone (MEK)
ND 501.72-Hexanone
ND 1000.984-Methyl-2-pentanone (MIBK)
ND 1001.9Acetone
ND 2001.4Acrylonitrile
ND 3.00.16Benzene
ND 3.00.10Bromochloromethane
ND 3.00.17Bromodichloromethane
ND 3.00.19Bromoform
ND 100.21Bromomethane
ND 1000.45Carbon disulfide
ND 5.50.19Carbon tetrachloride
ND 3.00.17Chlorobenzene
ND 100.41Chloroethane
ND 5.00.16Chloroform
ND 5.50.30Chloromethane
ND 5.00.15cis-1,2-Dichloroethene
ND 5.50.16cis-1,3-Dichloropropene
ND 3.00.17Dibromochloromethane
ND 100.17Dibromomethane
ND 5.00.16Ethylbenzene
ND 100.23Iodomethane
ND 5.50.32Methylene Chloride
ND 100.17Styrene
ND 3.00.20Tetrachloroethene
ND 5.00.17Toluene
ND 5.00.15trans-1,2-Dichloroethene
ND 5.50.19trans-1,3-Dichloropropene
ND 1000.80trans-1,4-Dichloro-2-butene
ND 3.00.16Trichloroethene
ND 5.00.29Trichlorofluoromethane
ND 500.94Vinyl acetate
TestAmerica Denver 05/23/2017Page 25 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 280-373992
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
G5144.D
20 mL
20 mLUnits:ug/L
Method: 8260B
Preparation: 5030B
VMS_GMB 280-373992/6
Analysis Date:05/17/2017 1750
Analysis Batch:
Prep Batch:
Leach Batch:
N/A
N/A
280-373992
Prep Date:
Leach Date:
05/17/2017 1750
N/A
Analyte RLMDLQualResult
ND 5.50.10Vinyl chloride
ND 4.00.19Xylenes, Total
Surrogate % Rec Acceptance Limits
1,2-Dichloroethane-d4 (Surr)115 70 - 127
4-Bromofluorobenzene (Surr)97 78 - 120
Dibromofluoromethane (Surr)107 77 - 120
Toluene-d8 (Surr)107 80 - 125
TestAmerica Denver 05/23/2017Page 26 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
Water
1.0
Lab Control Sample - Batch: 280-373992
Client Matrix:
Lab Sample ID:
Dilution:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
G5145.D
20 mL
20 mLUnits:ug/L
Method: 8260B
Preparation: 5030B
VMS_GLCS 280-373992/4
Analysis Date:05/17/2017 1811
Analysis Batch:
Prep Batch:
Leach Batch:
280-373992
N/A
N/A
Prep Date:
Leach Date:
05/17/2017 1811
N/A
Analyte QualLimit% Rec.ResultSpike Amount
5.00 4.28 86 J65 - 1351,1,1,2-Tetrachloroethane
5.00 4.36 87 J65 - 1351,1,1-Trichloroethane
5.00 3.89 78 58 - 1351,1,2,2-Tetrachloroethane
5.00 4.40 88 J64 - 1351,1,2-Trichloroethane
5.00 4.19 84 J65 - 1351,1-Dichloroethane
5.00 3.80 76 J65 - 1361,1-Dichloroethene
5.00 4.47 89 J65 - 1351,2,3-Trichloropropane
5.00 4.00 80 J57 - 1351,2-Dibromo-3-Chloropropane
5.00 4.25 85 65 - 1351,2-Dibromoethane
5.00 3.91 78 J65 - 1351,2-Dichlorobenzene
5.00 4.88 98 65 - 1351,2-Dichloroethane
5.00 4.36 87 64 - 1351,2-Dichloropropane
5.00 4.14 83 65 - 1351,3-Dichlorobenzene
5.00 4.12 82 65 - 1351,4-Dichlorobenzene
20.0 25.1 125 J44 - 1772-Butanone (MEK)
20.0 22.3 111 J57 - 1392-Hexanone
20.0 23.5 118 J60 - 1504-Methyl-2-pentanone (MIBK)
20.0 26.3 132 J39 - 156Acetone
50.0 41.4 83 J56 - 135Acrylonitrile
5.00 4.09 82 65 - 135Benzene
5.00 4.26 85 65 - 135Bromochloromethane
5.00 4.64 93 65 - 135Bromodichloromethane
5.00 3.86 77 62 - 135Bromoform
5.00 5.04 101 J45 - 135Bromomethane
5.00 3.66 73 J55 - 143Carbon disulfide
5.00 4.30 86 J65 - 135Carbon tetrachloride
5.00 3.81 76 65 - 135Chlorobenzene
5.00 5.20 104 J46 - 136Chloroethane
5.00 4.44 89 J65 - 135Chloroform
5.00 5.05 101 J34 - 145Chloromethane
5.00 3.98 80 J65 - 135cis-1,2-Dichloroethene
5.00 3.96 79 J65 - 135cis-1,3-Dichloropropene
5.00 3.87 77 65 - 135Dibromochloromethane
5.00 4.31 86 J65 - 135Dibromomethane
5.00 3.97 79 J65 - 135Ethylbenzene
5.00 3.88 78 J65 - 142Iodomethane
5.00 4.51 90 J54 - 141Methylene Chloride
5.00 3.88 78 J65 - 135Styrene
5.00 3.89 78 65 - 135Tetrachloroethene
5.00 4.04 81 J65 - 135Toluene
5.00 3.95 79 J65 - 135trans-1,2-Dichloroethene
5.00 4.17 83 J65 - 135trans-1,3-Dichloropropene
5.00 4.10 82 J53 - 135trans-1,4-Dichloro-2-butene
5.00 4.03 81 65 - 135Trichloroethene
5.00 5.43 109 53 - 137Trichlorofluoromethane
10.0 6.75 68 J11 - 187Vinyl acetate
TestAmerica Denver 05/23/2017Page 27 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
Water
1.0
Lab Control Sample - Batch: 280-373992
Client Matrix:
Lab Sample ID:
Dilution:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
G5145.D
20 mL
20 mLUnits:ug/L
Method: 8260B
Preparation: 5030B
VMS_GLCS 280-373992/4
Analysis Date:05/17/2017 1811
Analysis Batch:
Prep Batch:
Leach Batch:
280-373992
N/A
N/A
Prep Date:
Leach Date:
05/17/2017 1811
N/A
Analyte QualLimit% Rec.ResultSpike Amount
5.00 4.99 100 J40 - 137Vinyl chloride
10.0 7.97 80 65 - 135Xylenes, Total
Surrogate % Rec Acceptance Limits
1,2-Dichloroethane-d4 (Surr)112 70 - 127
4-Bromofluorobenzene (Surr)96 78 - 120
Dibromofluoromethane (Surr)103 77 - 120
Toluene-d8 (Surr)100 80 - 125
TestAmerica Denver 05/23/2017Page 28 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
Dilution:
Dilution:
Water
1.0
1.0
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix:Water
G5155.D
20 mL
20 mL
20 mL
G5156.D
20 mL
20 mL
20 mL
Method: 8260B
Preparation: 5030B
VMS_G
VMS_G
280-96884-G-1 MS
280-96884-G-1 MSD
MS Lab Sample ID:
MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-373992
05/17/2017 2144
N/A
Analysis Date:
Prep Date:
Leach Date:
Analysis Batch:
Prep Batch:
Leach Batch:
280-373992
N/A
N/A
Analysis Date:
Prep Date:
Leach Date:
05/17/2017 2205
05/17/2017 2205
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
280-373992
N/A
N/A
05/17/2017 2144
Analyte RPD LimitRPDLimit
% Rec.
MS MSD MS Qual MSD Qual
106 117 65 - 135 10 201,1,1,2-Tetrachloroethane
111 116 65 - 135 5 201,1,1-Trichloroethane
91 105 58 - 135 15 201,1,2,2-Tetrachloroethane
104 123 64 - 135 17 271,1,2-Trichloroethane
106 110 65 - 135 4 211,1-Dichloroethane
95 100 65 - 136 5 20 J J1,1-Dichloroethene
105 120 65 - 135 13 23 J J1,2,3-Trichloropropane
92 109 57 - 135 17 22 J J1,2-Dibromo-3-Chloropropane
105 110 65 - 135 5 271,2-Dibromoethane
98 106 65 - 135 8 20 J J1,2-Dichlorobenzene
135 149 65 - 135 10 20 F11,2-Dichloroethane
100 117 64 - 135 15 201,2-Dichloropropane
98 108 65 - 135 9 201,3-Dichlorobenzene
102 108 65 - 135 6 231,4-Dichlorobenzene
119 98 44 - 177 19 32 J J2-Butanone (MEK)
89 106 57 - 139 17 25 J J2-Hexanone
102 119 60 - 150 15 22 J J4-Methyl-2-pentanone (MIBK)
115 126 39 - 156 9 23 J JAcetone
101 113 56 - 135 11 30 J JAcrylonitrile
99 109 65 - 135 10 20Benzene
102 119 65 - 135 15 29Bromochloromethane
110 121 65 - 135 9 20Bromodichloromethane
99 111 62 - 135 11 27Bromoform
92 100 45 - 135 8 33 J JBromomethane
89 98 55 - 143 10 20 J JCarbon disulfide
108 114 65 - 135 5 21 JCarbon tetrachloride
94 107 65 - 135 13 20Chlorobenzene
103 106 46 - 136 3 25 J JChloroethane
109 116 65 - 135 7 20Chloroform
91 96 34 - 145 6 24 J JChloromethane
97 109 65 - 135 12 20 Jcis-1,2-Dichloroethene
94 105 65 - 135 11 26 J Jcis-1,3-Dichloropropene
100 110 65 - 135 10 20Dibromochloromethane
TestAmerica Denver 05/23/2017Page 29 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
Dilution:
Dilution:
Water
1.0
1.0
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix:Water
G5155.D
20 mL
20 mL
20 mL
G5156.D
20 mL
20 mL
20 mL
Method: 8260B
Preparation: 5030B
VMS_G
VMS_G
280-96884-G-1 MS
280-96884-G-1 MSD
MS Lab Sample ID:
MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-373992
05/17/2017 2144
N/A
Analysis Date:
Prep Date:
Leach Date:
Analysis Batch:
Prep Batch:
Leach Batch:
280-373992
N/A
N/A
Analysis Date:
Prep Date:
Leach Date:
05/17/2017 2205
05/17/2017 2205
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
280-373992
N/A
N/A
05/17/2017 2144
Analyte RPD LimitRPDLimit
% Rec.
MS MSD MS Qual MSD Qual
107 116 65 - 135 8 26 J JDibromomethane
96 109 65 - 135 12 20 JEthylbenzene
94 107 65 - 142 13 25 J JIodomethane
96 109 54 - 141 13 26 J JMethylene Chloride
97 106 65 - 135 9 26 J JStyrene
96 106 65 - 135 10 20Tetrachloroethene
101 111 65 - 135 10 20Toluene
99 111 65 - 135 12 24 Jtrans-1,2-Dichloroethene
106 114 65 - 135 8 26 Jtrans-1,3-Dichloropropene
99 116 53 - 135 16 25 J Jtrans-1,4-Dichloro-2-butene
97 107 65 - 135 10 20Trichloroethene
98 103 53 - 137 4 27 JTrichlorofluoromethane
153 150 11 - 187 2 24 J JVinyl acetate
92 96 40 - 137 5 24 J JVinyl chloride
100 109 65 - 135 9 20Xylenes, Total
Surrogate Acceptance LimitsMS % Rec MSD % Rec
1,2-Dichloroethane-d4 (Surr)112 115 70 - 127
4-Bromofluorobenzene (Surr)93 99 78 - 120
Dibromofluoromethane (Surr)103 105 77 - 120
Toluene-d8 (Surr)103 100 80 - 125
TestAmerica Denver 05/23/2017Page 30 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
Water
05/17/2017 2144 05/17/2017 2205
Dilution:Dilution:1.0 1.0
Client Matrix:Client Matrix:Water
Method: 8260B
Preparation: 5030B
Units:ug/L280-96884-G-1 MS 280-96884-G-1 MSDMS Lab Sample ID:MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-373992
Analysis Date:
Prep Date:
Leach Date:
05/17/2017 2144
N/A
Analysis Date:
Prep Date:
Leach Date:
05/17/2017 2205
N/A
Amount
Sample
Analyte Result/Qual Amount Result/Qual Result/Qual
MS MSDMS Spike MSD Spike
ND 5.00 5.00 5.28 5.841,1,1,2-Tetrachloroethane
ND 5.00 5.00 5.54 5.821,1,1-Trichloroethane
ND 5.00 5.00 4.53 5.261,1,2,2-Tetrachloroethane
ND 5.00 5.00 5.18 6.131,1,2-Trichloroethane
ND 5.00 5.00 5.30 5.511,1-Dichloroethane
ND 5.00 5.00 4.75 4.99J J1,1-Dichloroethene
ND 5.00 5.00 5.25 5.98J J1,2,3-Trichloropropane
ND 5.00 5.00 4.60 5.45J J1,2-Dibromo-3-Chloropropane
ND 5.00 5.00 5.24 5.521,2-Dibromoethane
ND 5.00 5.00 4.90 5.28J J1,2-Dichlorobenzene
ND 5.00 5.00 6.75 7.43 F11,2-Dichloroethane
ND 5.00 5.00 5.01 5.831,2-Dichloropropane
ND 5.00 5.00 4.92 5.401,3-Dichlorobenzene
ND 5.00 5.00 5.09 5.421,4-Dichlorobenzene
ND 20.0 20.0 23.7 19.5J J2-Butanone (MEK)
ND 20.0 20.0 17.8 21.2J J2-Hexanone
ND 20.0 20.0 20.4 23.7J J4-Methyl-2-pentanone (MIBK)
ND 20.0 20.0 23.0 25.2J JAcetone
ND 50.0 50.0 50.6 56.7J JAcrylonitrile
ND 5.00 5.00 4.95 5.46Benzene
ND 5.00 5.00 5.11 5.95Bromochloromethane
ND 5.00 5.00 5.52 6.04Bromodichloromethane
ND 5.00 5.00 4.94 5.53Bromoform
ND 5.00 5.00 4.61 4.99J JBromomethane
ND 5.00 5.00 4.46 4.92J JCarbon disulfide
ND 5.00 5.00 5.42 5.71JCarbon tetrachloride
ND 5.00 5.00 4.69 5.33Chlorobenzene
ND 5.00 5.00 5.15 5.31J JChloroethane
ND 5.00 5.00 5.43 5.81Chloroform
ND 5.00 5.00 4.54 4.82J JChloromethane
ND 5.00 5.00 4.83 5.44Jcis-1,2-Dichloroethene
ND 5.00 5.00 4.69 5.24J Jcis-1,3-Dichloropropene
ND 5.00 5.00 4.99 5.52Dibromochloromethane
ND 5.00 5.00 5.35 5.80J JDibromomethane
ND 5.00 5.00 4.80 5.44JEthylbenzene
ND 5.00 5.00 4.69 5.35J JIodomethane
ND 5.00 5.00 4.80 5.47J JMethylene Chloride
ND 5.00 5.00 4.86 5.32J JStyrene
ND 5.00 5.00 4.80 5.28Tetrachloroethene
ND 5.00 5.00 5.04 5.57Toluene
ND 5.00 5.00 4.94 5.57Jtrans-1,2-Dichloroethene
ND 5.00 5.00 5.30 5.72Jtrans-1,3-Dichloropropene
ND 5.00 5.00 4.94 5.79J Jtrans-1,4-Dichloro-2-butene
TestAmerica Denver 05/23/2017Page 31 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
Water
05/17/2017 2144 05/17/2017 2205
Dilution:Dilution:1.0 1.0
Client Matrix:Client Matrix:Water
Method: 8260B
Preparation: 5030B
Units:ug/L280-96884-G-1 MS 280-96884-G-1 MSDMS Lab Sample ID:MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-373992
Analysis Date:
Prep Date:
Leach Date:
05/17/2017 2144
N/A
Analysis Date:
Prep Date:
Leach Date:
05/17/2017 2205
N/A
Amount
Sample
Analyte Result/Qual Amount Result/Qual Result/Qual
MS MSDMS Spike MSD Spike
ND 5.00 5.00 4.86 5.37Trichloroethene
ND 5.00 5.00 4.91 5.13JTrichlorofluoromethane
ND 10.0 10.0 15.3 15.0J JVinyl acetate
ND 5.00 5.00 4.58 4.82J JVinyl chloride
ND 10.0 10.0 9.95 10.9Xylenes, Total
TestAmerica Denver 05/23/2017Page 32 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 280-372301
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
25F051517.asc
50 mL
50 mLUnits:ug/L
Method: 6010C
Preparation: 3005A
Total Recoverable
MT_025MB 280-372301/1-A
Analysis Date:05/16/2017 0639
Analysis Batch:
Prep Batch:
Leach Batch:N/A
280-373731
280-372301
Prep Date:
Leach Date:
05/15/2017 0716
N/A
Analyte RLMDLQualResult
0.850 J 1000.82Barium
ND 100.66Chromium
ND 101.2Cobalt
ND 20035Calcium
ND 154.2Copper
ND 102.7Lead
ND 502.6Nickel
ND 204.5Zinc
ND 251.1Vanadium
ND 20011Magnesium
ND 100.26Manganese
ND 156.3Selenium
ND 100.93Silver
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 280-372301
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
25B051617.asc
50 mL
50 mLUnits:ug/L
Method: 6010C
Preparation: 3005A
Total Recoverable
MT_025MB 280-372301/1-A
Analysis Date:05/16/2017 2034
Analysis Batch:
Prep Batch:
Leach Batch:N/A
280-373855
280-372301
Prep Date:
Leach Date:
05/15/2017 0716
N/A
Analyte RLMDLQualResult
ND 10022Iron
196 J ^5000120Sodium
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 280-372301
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
25Q051717.asc
50 mL
50 mLUnits:ug/L
Method: 6010C
Preparation: 3005A
Total Recoverable
MT_025MB 280-372301/1-A
Analysis Date:05/17/2017 0903
Analysis Batch:
Prep Batch:
Leach Batch:N/A
280-373928
280-372301
Prep Date:
Leach Date:
05/15/2017 0716
N/A
Analyte RLMDLQualResult
ND 3000240Potassium
TestAmerica Denver 05/23/2017Page 33 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
Water
1.0
Lab Control Sample - Batch: 280-372301
Client Matrix:
Lab Sample ID:
Dilution:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
25F051517.asc
50 mL
50 mLUnits:ug/L
Method: 6010C
Preparation: 3005A
Total Recoverable
MT_025LCS 280-372301/2-A
Analysis Date:05/16/2017 0641
Analysis Batch:
Prep Batch:
Leach Batch:
280-373731
280-372301
N/A
Prep Date:
Leach Date:
05/15/2017 0716
N/A
Analyte QualLimit% Rec.ResultSpike Amount
2000 2210 111 90 - 112Barium
200 215 108 90 - 113Chromium
500 521 104 89 - 111Cobalt
50000 53900 108 90 - 111Calcium
250 272 109 86 - 112Copper
500 527 105 89 - 110Lead
500 517 103 89 - 111Nickel
500 540 108 85 - 111Zinc
500 502 100 90 - 111Vanadium
50000 52700 105 90 - 113Magnesium
500 520 104 90 - 110Manganese
2000 2180 109 85 - 112Selenium
50.0 56.0 112 86 - 115Silver
Water
1.0
Lab Control Sample - Batch: 280-372301
Client Matrix:
Lab Sample ID:
Dilution:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
25B051617.asc
50 mL
50 mLUnits:ug/L
Method: 6010C
Preparation: 3005A
Total Recoverable
MT_025LCS 280-372301/2-A
Analysis Date:05/16/2017 2036
Analysis Batch:
Prep Batch:
Leach Batch:
280-373855
280-372301
N/A
Prep Date:
Leach Date:
05/15/2017 0716
N/A
Analyte QualLimit% Rec.ResultSpike Amount
1000 1130 113 89 - 115Iron
50000 55400 111 ^90 - 115Sodium
Water
1.0
Lab Control Sample - Batch: 280-372301
Client Matrix:
Lab Sample ID:
Dilution:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
25Q051717.asc
50 mL
50 mLUnits:ug/L
Method: 6010C
Preparation: 3005A
Total Recoverable
MT_025LCS 280-372301/2-A
Analysis Date:05/17/2017 0906
Analysis Batch:
Prep Batch:
Leach Batch:
280-373928
280-372301
N/A
Prep Date:
Leach Date:
05/15/2017 0716
N/A
Analyte QualLimit% Rec.ResultSpike Amount
50000 52200 104 89 - 114Potassium
TestAmerica Denver 05/23/2017Page 34 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
Dilution:
Dilution:
Water
1.0
1.0
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix:Water
25F051517.asc
50 mL
50 mL
25F051517.asc
50 mL
50 mL
Method: 6010C
Preparation: 3005A
Total Recoverable
MT_025
MT_025
280-96675-1
280-96675-1
MS Lab Sample ID:
MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-372301
05/16/2017 0649
N/A
Analysis Date:
Prep Date:
Leach Date:
Analysis Batch:
Prep Batch:
Leach Batch:
280-373731
280-372301
N/A
Analysis Date:
Prep Date:
Leach Date:
05/16/2017 0651
05/15/2017 0716
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
280-373731
280-372301
N/A
05/15/2017 0716
Analyte RPD LimitRPDLimit
% Rec.
MS MSD MS Qual MSD Qual
109 111 85 - 120 1 20Barium
105 109 73 - 135 3 20Chromium
100 102 82 - 119 2 20Cobalt
107 110 48 - 153 2 20Calcium
108 112 82 - 129 2 20Copper
97 100 89 - 121 3 20Lead
100 104 84 - 120 3 20Nickel
109 110 60 - 137 1 20Zinc
101 103 85 - 120 2 20Vanadium
103 107 62 - 146 2 20Magnesium
104 110 79 - 121 2 20Manganese
109 113 71 - 140 4 20Selenium
115 119 75 - 141 3 20Silver
TestAmerica Denver 05/23/2017Page 35 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
Dilution:
Dilution:
Water
1.0
1.0
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix:Water
25B051617.asc
50 mL
50 mL
25B051617.asc
50 mL
50 mL
Method: 6010C
Preparation: 3005A
Total Recoverable
MT_025
MT_025
280-96675-1
280-96675-1
MS Lab Sample ID:
MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-372301
05/16/2017 2044
N/A
Analysis Date:
Prep Date:
Leach Date:
Analysis Batch:
Prep Batch:
Leach Batch:
280-373855
280-372301
N/A
Analysis Date:
Prep Date:
Leach Date:
05/16/2017 2046
05/15/2017 0716
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
280-373855
280-372301
N/A
05/15/2017 0716
Analyte RPD LimitRPDLimit
% Rec.
MS MSD MS Qual MSD Qual
111 125 52 - 155 1 20 4 4Iron
130 170 70 - 203 2 20 ^ 4 ^ 4Sodium
Dilution:
Dilution:
Water
1.0
1.0
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix:Water
25Q051717.asc
50 mL
50 mL
25Q051717.asc
50 mL
50 mL
Method: 6010C
Preparation: 3005A
Total Recoverable
MT_025
MT_025
280-96675-1
280-96675-1
MS Lab Sample ID:
MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-372301
05/17/2017 0913
N/A
Analysis Date:
Prep Date:
Leach Date:
Analysis Batch:
Prep Batch:
Leach Batch:
280-373928
280-372301
N/A
Analysis Date:
Prep Date:
Leach Date:
05/17/2017 0916
05/15/2017 0716
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
280-373928
280-372301
N/A
05/15/2017 0716
Analyte RPD LimitRPDLimit
% Rec.
MS MSD MS Qual MSD Qual
102 114 76 - 132 2 20 4 4Potassium
TestAmerica Denver 05/23/2017Page 36 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
Water
05/16/2017 0649 05/16/2017 0651
Dilution:Dilution:1.0 1.0
Client Matrix:Client Matrix:Water
Method: 6010C
Preparation: 3005A
Total Recoverable
Units:ug/L280-96675-1 280-96675-1MS Lab Sample ID:MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-372301
Analysis Date:
Prep Date:
Leach Date:
05/15/2017 0716
N/A
Analysis Date:
Prep Date:
Leach Date:
05/15/2017 0716
N/A
Amount
Sample
Analyte Result/Qual Amount Result/Qual Result/Qual
MS MSDMS Spike MSD Spike
190 2000 2000 2380 2410Barium
80 200 200 290 298Chromium
23 500 500 522 535Cobalt
45000 50000 50000 99100 101000Calcium
150 250 250 424 434Copper
ND 500 500 487 502Lead
180 500 500 673 693Nickel
32 500 500 578 585Zinc
45 500 500 548 558Vanadium
38000 50000 50000 89900 91900Magnesium
610 500 500 1130 1150Manganese
ND 2000 2000 2170 2250Selenium
ND 50.0 50.0 57.6 59.5Silver
Water
05/16/2017 2044 05/16/2017 2046
Dilution:Dilution:1.0 1.0
Client Matrix:Client Matrix:Water
Method: 6010C
Preparation: 3005A
Total Recoverable
Units:ug/L280-96675-1 280-96675-1MS Lab Sample ID:MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-372301
Analysis Date:
Prep Date:
Leach Date:
05/15/2017 0716
N/A
Analysis Date:
Prep Date:
Leach Date:
05/15/2017 0716
N/A
Amount
Sample
Analyte Result/Qual Amount Result/Qual Result/Qual
MS MSDMS Spike MSD Spike
11000 1000 1000 11900 120004 4Iron
1200000 50000 50000 1240000 1260000^ 4 ^ 4Sodium
TestAmerica Denver 05/23/2017Page 37 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
Water
05/17/2017 0913 05/17/2017 0916
Dilution:Dilution:1.0 1.0
Client Matrix:Client Matrix:Water
Method: 6010C
Preparation: 3005A
Total Recoverable
Units:ug/L280-96675-1 280-96675-1MS Lab Sample ID:MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-372301
Analysis Date:
Prep Date:
Leach Date:
05/15/2017 0716
N/A
Analysis Date:
Prep Date:
Leach Date:
05/15/2017 0716
N/A
Amount
Sample
Analyte Result/Qual Amount Result/Qual Result/Qual
MS MSDMS Spike MSD Spike
280000 50000 50000 329000 3350004 4Potassium
TestAmerica Denver 05/23/2017Page 38 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 280-372302
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
141_BLK.d
50 mL
50 mLUnits:ug/L
Method: 6020A
Preparation: 3005A
Total Recoverable
MT_078MB 280-372302/1-A
Analysis Date:05/16/2017 0157
Analysis Batch:
Prep Batch:
Leach Batch:N/A
280-373738
280-372302
Prep Date:
Leach Date:
05/15/2017 0716
N/A
Analyte RLMDLQualResult
ND 2.00.40Antimony
ND 5.00.33Arsenic
ND 1.00.080Beryllium
ND 1.00.27Cadmium
ND 1.00.050Thallium
Water
1.0
Lab Control Sample - Batch: 280-372302
Client Matrix:
Lab Sample ID:
Dilution:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
142_LCS.d
50 mL
50 mLUnits:ug/L
Method: 6020A
Preparation: 3005A
Total Recoverable
MT_078LCS 280-372302/2-A
Analysis Date:05/16/2017 0202
Analysis Batch:
Prep Batch:
Leach Batch:
280-373738
280-372302
N/A
Prep Date:
Leach Date:
05/15/2017 0716
N/A
Analyte QualLimit% Rec.ResultSpike Amount
40.0 41.4 104 85 - 115Antimony
40.0 42.1 105 85 - 117Arsenic
40.0 40.2 100 80 - 125Beryllium
40.0 44.0 110 85 - 115Cadmium
40.0 43.5 109 85 - 118Thallium
TestAmerica Denver 05/23/2017Page 39 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
Dilution:
Dilution:
Water
1.0
1.0
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix:Water
145SMPL.d
50 mL
50 mL
146SMPL.d
50 mL
50 mL
Method: 6020A
Preparation: 3005A
Total Recoverable
MT_078
MT_078
280-96675-1
280-96675-1
MS Lab Sample ID:
MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-372302
05/16/2017 0216
N/A
Analysis Date:
Prep Date:
Leach Date:
Analysis Batch:
Prep Batch:
Leach Batch:
280-373738
280-372302
N/A
Analysis Date:
Prep Date:
Leach Date:
05/16/2017 0221
05/15/2017 0716
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
280-373738
280-372302
N/A
05/15/2017 0716
Analyte RPD LimitRPDLimit
% Rec.
MS MSD MS Qual MSD Qual
104 107 85 - 115 3 20Antimony
110 108 85 - 117 1 20Arsenic
101 103 80 - 125 2 20Beryllium
101 103 85 - 115 2 20Cadmium
99 99 85 - 118 0 20Thallium
Water
05/16/2017 0216 05/16/2017 0221
Dilution:Dilution:1.0 1.0
Client Matrix:Client Matrix:Water
Method: 6020A
Preparation: 3005A
Total Recoverable
Units:ug/L280-96675-1 280-96675-1MS Lab Sample ID:MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-372302
Analysis Date:
Prep Date:
Leach Date:
05/15/2017 0716
N/A
Analysis Date:
Prep Date:
Leach Date:
05/15/2017 0716
N/A
Amount
Sample
Analyte Result/Qual Amount Result/Qual Result/Qual
MS MSDMS Spike MSD Spike
6.7 40.0 40.0 48.2 49.5Antimony
35 40.0 40.0 78.8 78.4Arsenic
ND 40.0 40.0 40.5 41.3Beryllium
ND 40.0 40.0 40.4 41.3Cadmium
ND 40.0 40.0 39.6 39.8Thallium
TestAmerica Denver 05/23/2017Page 40 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 280-374242
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
170519aa.txt
30 mL
50 mLUnits:ug/L
Method: 7470A
Preparation: 7470A
MT_033MB 280-374242/1-A
Analysis Date:05/19/2017 1736
Analysis Batch:
Prep Batch:
Leach Batch:N/A
280-374456
280-374242
Prep Date:
Leach Date:
05/19/2017 1135
N/A
Analyte RLMDLQualResult
ND 0.200.027Mercury
Water
1.0
Lab Control Sample - Batch: 280-374242
Client Matrix:
Lab Sample ID:
Dilution:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
170519aa.txt
30 mL
50 mLUnits:ug/L
Method: 7470A
Preparation: 7470A
MT_033LCS 280-374242/2-A
Analysis Date:05/19/2017 1738
Analysis Batch:
Prep Batch:
Leach Batch:
280-374456
280-374242
N/A
Prep Date:
Leach Date:
05/19/2017 1135
N/A
Analyte QualLimit% Rec.ResultSpike Amount
5.00 5.04 101 84 - 120Mercury
Dilution:
Dilution:
Water
1.0
1.0
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix:Water
170519aa.txt
30 mL
50 mL
170519aa.txt
30 mL
50 mL
Method: 7470A
Preparation: 7470A
MT_033
MT_033
280-96372-H-3-B MS
280-96372-H-3-C MSD
MS Lab Sample ID:
MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-374242
05/19/2017 1747
N/A
Analysis Date:
Prep Date:
Leach Date:
Analysis Batch:
Prep Batch:
Leach Batch:
280-374456
280-374242
N/A
Analysis Date:
Prep Date:
Leach Date:
05/19/2017 1749
05/19/2017 1135
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
280-374456
280-374242
N/A
05/19/2017 1135
Analyte RPD LimitRPDLimit
% Rec.
MS MSD MS Qual MSD Qual
99 96 75 - 125 3 20Mercury
TestAmerica Denver 05/23/2017Page 41 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
Water
05/19/2017 1747 05/19/2017 1749
Dilution:Dilution:1.0 1.0
Client Matrix:Client Matrix:Water
Method: 7470A
Preparation: 7470A
Units:ug/L280-96372-H-3-B MS 280-96372-H-3-C MSDMS Lab Sample ID:MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-374242
Analysis Date:
Prep Date:
Leach Date:
05/19/2017 1135
N/A
Analysis Date:
Prep Date:
Leach Date:
05/19/2017 1135
N/A
Amount
Sample
Analyte Result/Qual Amount Result/Qual Result/Qual
MS MSDMS Spike MSD Spike
ND 5.00 5.00 4.93 4.80Mercury
TestAmerica Denver 05/23/2017Page 42 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 280-373891
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
06.0000.d
5 mL
5 mLUnits:mg/L
Method: 300.0
Preparation: N/A
WC_IonChrom6MB 280-373891/6
Analysis Date:05/17/2017 1035
Analysis Batch:
Prep Batch:
Leach Batch:
N/A
N/A
280-373891
Prep Date:
Leach Date:
N/A
N/A
Analyte RLMDLQualResult
ND 0.300.25Chloride
ND 5.00.23Sulfate
Water
1.0
Method Reporting Limit Check - Batch: 280-373891
Client Matrix:
Lab Sample ID:
Dilution:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
03.0000.d
5 mL
5 mLUnits:mg/L
Method: 300.0
Preparation: N/A
WC_IonChrom6MRL 280-373891/3
Analysis Date:05/17/2017 0942
Analysis Batch:
Prep Batch:
Leach Batch:
280-373891
N/A
N/A
Prep Date:
Leach Date:
N/A
N/A
Analyte QualLimit% Rec.ResultSpike Amount
2.50 2.41 96 J50 - 150Chloride
2.50 2.37 95 J50 - 150Sulfate
Dilution:
Dilution:
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 280-373891
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix:Water
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
mg/L
04.0000.d
5 mL
5 mL
25 uL
05.0000.d
5 mL
5 mL
25 uL
mg/L
Method: 300.0
Preparation: N/A
WC_IonChrom6
WC_IonChrom6
LCS 280-373891/4
LCSD 280-373891/5
Analysis Date:
Prep Date:
Leach Date:
05/17/2017 0959
N/A
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
280-373891
N/A
N/A
Analysis Date:
Prep Date:
Leach Date:
05/17/2017 1017
N/A
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
280-373891
N/A
N/A
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
103103 90 - 110 0 10Chloride
102102 90 - 110 0 10Sulfate
TestAmerica Denver 05/23/2017Page 43 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
Water
05/17/2017 0959
Dilution:Dilution:1.0 1.0
Client Matrix:
LCSD Lab Sample ID:
Client Matrix:Water
Laboratory Control/
Laboratory Duplicate Data Report - Batch: 280-373891
Method: 300.0
Preparation: N/A
Units:mg/LLCS 280-373891/4 LCSD 280-373891/5LCS Lab Sample ID:
Analysis Date:
Prep Date:
Leach Date:
Analysis Date:
Prep Date:
Leach Date:
05/17/2017 1017
N/A
N/A
N/A
N/A
LCSD
Result/Qual
LCS
Result/Qual
LCSD Spike
Amount
LCS Spike
AmountAnalyte
103103100100Chloride
102102100100Sulfate
Dilution:
Dilution:
Water
10
10
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix:Water
11.0000.d
5 mL
5 mL
25 uL
12.0000.d
5 mL
5 mL
25 uL
Method: 300.0
Preparation: N/A
WC_IonChrom6
WC_IonChrom6
280-96903-E-2 MS
280-96903-E-2 MSD
MS Lab Sample ID:
MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-373891
05/17/2017 1205
N/A
N/A
Analysis Date:
Prep Date:
Leach Date:
Analysis Batch:
Prep Batch:
Leach Batch:
280-373891
N/A
N/A
Analysis Date:
Prep Date:
Leach Date:
05/17/2017 1223
N/A
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
280-373891
N/A
N/A
Analyte RPD LimitRPDLimit
% Rec.
MS MSD MS Qual MSD Qual
106 106 80 - 120 1 20Chloride
91 84 80 - 120 2 20Sulfate
TestAmerica Denver 05/23/2017Page 44 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
Water
05/17/2017 1205 05/17/2017 1223
Dilution:Dilution:10 10
Client Matrix:Client Matrix:Water
Method: 300.0
Preparation: N/A
Units:mg/L280-96903-E-2 MS 280-96903-E-2 MSDMS Lab Sample ID:MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-373891
Analysis Date:
Prep Date:
Leach Date:
N/A
N/A
Analysis Date:
Prep Date:
Leach Date:
N/A
N/A
Amount
Sample
Analyte Result/Qual Amount Result/Qual Result/Qual
MS MSDMS Spike MSD Spike
2.9 J 250 250 269 267Chloride
810 250 250 1040 1020Sulfate
mg/LUnits:
Water
Dilution:10
Duplicate - Batch: 280-373891
Lab Sample ID:
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
10.0000.d
5 mL
5 mL
Method: 300.0
Preparation: N/A
WC_IonChrom6280-96903-E-2 DU
Analysis Date:05/17/2017 1148
Analysis Batch:
Prep Batch:
Leach Batch:
280-373891
N/A
N/A
Prep Date:25 uL
Leach Date:
N/A
N/A
Analyte QualLimitRPDResultSample Result/Qual
2.792.9 J 3 15 JChloride
801810 1 15Sulfate
TestAmerica Denver 05/23/2017Page 45 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 280-373940
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
C:\FLOW_4\051617A.RST
1.0 mL
1.0 mLUnits:mg/L
Method: 350.1
Preparation: N/A
WC_Alp 3MB 280-373940/103
Analysis Date:05/16/2017 1525
Analysis Batch:
Prep Batch:
Leach Batch:
N/A
N/A
280-373940
Prep Date:
Leach Date:
N/A
N/A
Analyte RLMDLQualResult
ND 0.0400.022Ammonia
Dilution:
Dilution:
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 280-373940
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix:Water
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
mg/L
C:\FLOW_4\051617A.RST
100 mL
100 mL
C:\FLOW_4\051617A.RST
100 mL
100 mLmg/L
Method: 350.1
Preparation: N/A
WC_Alp 3
WC_Alp 3
LCS 280-373940/101
LCSD 280-373940/102
Analysis Date:
Prep Date:
Leach Date:
05/16/2017 1521
N/A
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
280-373940
N/A
N/A
Analysis Date:
Prep Date:
Leach Date:
05/16/2017 1523
N/A
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
280-373940
N/A
N/A
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
9193 90 - 110 2 10Ammonia
Water
05/16/2017 1521
Dilution:Dilution:1.0 1.0
Client Matrix:
LCSD Lab Sample ID:
Client Matrix:Water
Laboratory Control/
Laboratory Duplicate Data Report - Batch: 280-373940
Method: 350.1
Preparation: N/A
Units:mg/LLCS 280-373940/101 LCSD 280-373940/102LCS Lab Sample ID:
Analysis Date:
Prep Date:
Leach Date:
Analysis Date:
Prep Date:
Leach Date:
05/16/2017 1523
N/A
N/A
N/A
N/A
LCSD
Result/Qual
LCS
Result/Qual
LCSD Spike
Amount
LCS Spike
AmountAnalyte
2.282.332.50 2.50Ammonia
TestAmerica Denver 05/23/2017Page 46 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
Dilution:
Dilution:
Water
1.0
1.0
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix:Water
C:\FLOW_4\051617A.RST
10 mL
10 mL
C:\FLOW_4\051617A.RST
10 mL
10 mL
Method: 350.1
Preparation: N/A
WC_Alp 3
WC_Alp 3
280-96745-A-11 MS
280-96745-A-11 MSD
MS Lab Sample ID:
MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-373940
05/16/2017 1451
N/A
N/A
Analysis Date:
Prep Date:
Leach Date:
Analysis Batch:
Prep Batch:
Leach Batch:
280-373940
N/A
N/A
Analysis Date:
Prep Date:
Leach Date:
05/16/2017 1453
N/A
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
280-373940
N/A
N/A
Analyte RPD LimitRPDLimit
% Rec.
MS MSD MS Qual MSD Qual
106 100 90 - 110 5 10Ammonia
Water
05/16/2017 1451 05/16/2017 1453
Dilution:Dilution:1.0 1.0
Client Matrix:Client Matrix:Water
Method: 350.1
Preparation: N/A
Units:mg/L280-96745-A-11 MS 280-96745-A-11 MSDMS Lab Sample ID:MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-373940
Analysis Date:
Prep Date:
Leach Date:
N/A
N/A
Analysis Date:
Prep Date:
Leach Date:
N/A
N/A
Amount
Sample
Analyte Result/Qual Amount Result/Qual Result/Qual
MS MSDMS Spike MSD Spike
ND 1.00 1.00 1.06 1.00Ammonia
TestAmerica Denver 05/23/2017Page 47 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 280-373136
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
051617tphos.xls
50 mL
50 mLUnits:mg/L
Method: 365.1
Preparation: 365.2/365.3/365
WC_KonelabMB 280-373136/11-A
Analysis Date:05/16/2017 1254
Analysis Batch:
Prep Batch:
Leach Batch:N/A
280-373778
280-373136
Prep Date:
Leach Date:
05/11/2017 1039
N/A
Analyte RLMDLQualResult
ND 0.0500.0050Phosphorus, Total
Dilution:
Dilution:
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 280-373136
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix:Water
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
mg/L
051617tphos.xls
50 mL
50 mL
051617tphos.xls
50 mL
50 mLmg/L
Method: 365.1
Preparation: 365.2/365.3/365
WC_Konelab
WC_Konelab
LCS 280-373136/9-A
LCSD 280-373136/10-A
Analysis Date:
Prep Date:
Leach Date:
05/16/2017 1254
05/11/2017 1039
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
280-373778
280-373136
N/A
Analysis Date:
Prep Date:
Leach Date:
05/16/2017 1254
05/11/2017 1039
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
280-373778
280-373136
N/A
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
104103 90 - 110 1 10Phosphorus, Total
Water
05/16/2017 1254
Dilution:Dilution:1.0 1.0
Client Matrix:
LCSD Lab Sample ID:
Client Matrix:Water
Laboratory Control/
Laboratory Duplicate Data Report - Batch: 280-373136
Method: 365.1
Preparation: 365.2/365.3/365
Units:mg/LLCS 280-373136/9-A LCSD 280-373136/10-ALCS Lab Sample ID:
Analysis Date:
Prep Date:
Leach Date:
05/11/2017 1039
Analysis Date:
Prep Date:
Leach Date:
05/16/2017 1254
05/11/2017 1039
N/AN/A
LCSD
Result/Qual
LCS
Result/Qual
LCSD Spike
Amount
LCS Spike
AmountAnalyte
0.5190.5150.500 0.500Phosphorus, Total
TestAmerica Denver 05/23/2017Page 48 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
Dilution:
Dilution:
Water
1.0
1.0
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix:Water
051617tphos.xls
50 mL
50 mL
051617tphos.xls
50 mL
50 mL
Method: 365.1
Preparation: 365.2/365.3/365
WC_Konelab
WC_Konelab
280-96926-A-5-B MS
280-96926-A-5-C MSD
MS Lab Sample ID:
MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-373136
05/16/2017 1254
N/A
Analysis Date:
Prep Date:
Leach Date:
Analysis Batch:
Prep Batch:
Leach Batch:
280-373778
280-373136
N/A
Analysis Date:
Prep Date:
Leach Date:
05/16/2017 1254
05/11/2017 1039
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
280-373778
280-373136
N/A
05/11/2017 1039
Analyte RPD LimitRPDLimit
% Rec.
MS MSD MS Qual MSD Qual
91 88 90 - 110 1 10 F1Phosphorus, Total
Water
05/16/2017 1254 05/16/2017 1254
Dilution:Dilution:1.0 1.0
Client Matrix:Client Matrix:Water
Method: 365.1
Preparation: 365.2/365.3/365
Units:mg/L280-96926-A-5-B MS 280-96926-A-5-C MSDMS Lab Sample ID:MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-373136
Analysis Date:
Prep Date:
Leach Date:
05/11/2017 1039
N/A
Analysis Date:
Prep Date:
Leach Date:
05/11/2017 1039
N/A
Amount
Sample
Analyte Result/Qual Amount Result/Qual Result/Qual
MS MSDMS Spike MSD Spike
0.81 0.500 0.500 1.27 1.25 F1Phosphorus, Total
TestAmerica Denver 05/23/2017Page 49 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 280-374088
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
2 mL
2 mLUnits:mg/L
Method: 410.4
Preparation: N/A
N/A
WC_Genesys20MB 280-374088/5
Analysis Date:05/18/2017 0912
Analysis Batch:
Prep Batch:
Leach Batch:
N/A
N/A
280-374088
Prep Date:
Leach Date:
N/A
N/A
Analyte RLMDLQualResult
ND 504.1Chemical Oxygen Demand
Dilution:
Dilution:
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 280-374088
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix:Water
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
mg/L
100 mL
100 mL
100 mL
100 mLmg/L
Method: 410.4
Preparation: N/A
N/A
N/A
WC_Genesys20
WC_Genesys20
LCS 280-374088/3
LCSD 280-374088/4
Analysis Date:
Prep Date:
Leach Date:
05/18/2017 0912
N/A
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
280-374088
N/A
N/A
Analysis Date:
Prep Date:
Leach Date:
05/18/2017 0912
N/A
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
280-374088
N/A
N/A
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
9791 90 - 110 7 11Chemical Oxygen Demand
Water
05/18/2017 0912
Dilution:Dilution:1.0 1.0
Client Matrix:
LCSD Lab Sample ID:
Client Matrix:Water
Laboratory Control/
Laboratory Duplicate Data Report - Batch: 280-374088
Method: 410.4
Preparation: N/A
Units:mg/LLCS 280-374088/3 LCSD 280-374088/4LCS Lab Sample ID:
Analysis Date:
Prep Date:
Leach Date:
Analysis Date:
Prep Date:
Leach Date:
05/18/2017 0912
N/A
N/A
N/A
N/A
LCSD
Result/Qual
LCS
Result/Qual
LCSD Spike
Amount
LCS Spike
AmountAnalyte
96.890.6100100Chemical Oxygen Demand
TestAmerica Denver 05/23/2017Page 50 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
Dilution:
Dilution:
Water
1.0
1.0
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix:Water
100 mL
100 mL
100 mL
100 mL
Method: 410.4
Preparation: N/A
N/A
N/A
WC_Genesys20
WC_Genesys20
280-96659-B-1 MS
280-96659-B-1 MSD
MS Lab Sample ID:
MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-374088
05/18/2017 0912
N/A
N/A
Analysis Date:
Prep Date:
Leach Date:
Analysis Batch:
Prep Batch:
Leach Batch:
280-374088
N/A
N/A
Analysis Date:
Prep Date:
Leach Date:
05/18/2017 0912
N/A
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
280-374088
N/A
N/A
Analyte RPD LimitRPDLimit
% Rec.
MS MSD MS Qual MSD Qual
114 109 90 - 110 4 11 F1Chemical Oxygen Demand
Water
05/18/2017 0912 05/18/2017 0912
Dilution:Dilution:1.0 1.0
Client Matrix:Client Matrix:Water
Method: 410.4
Preparation: N/A
Units:mg/L280-96659-B-1 MS 280-96659-B-1 MSDMS Lab Sample ID:MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-374088
Analysis Date:
Prep Date:
Leach Date:
N/A
N/A
Analysis Date:
Prep Date:
Leach Date:
N/A
N/A
Amount
Sample
Analyte Result/Qual Amount Result/Qual Result/Qual
MS MSDMS Spike MSD Spike
ND 50.0 50.0 56.9 54.4F1Chemical Oxygen Demand
TestAmerica Denver 05/23/2017Page 51 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 280-374303
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:Units:mg/L
Method: Nitrate by calc
Preparation: N/A
N/A
No Equipment AssignedMB 280-374303/1
Analysis Date:05/19/2017 1151
Analysis Batch:
Prep Batch:
Leach Batch:
N/A
N/A
280-374303
Prep Date:
Leach Date:
N/A
N/A
Analyte RLMDLQualResult
ND 0.500.019Nitrate as N
TestAmerica Denver 05/23/2017Page 52 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 280-373408
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
alk high 051217.TXT
Units:mg/L
Method: SM 2320B
Preparation: N/A
WC-AT3MB 280-373408/5
Analysis Date:05/12/2017 1734
Analysis Batch:
Prep Batch:
Leach Batch:
N/A
N/A
280-373408
Prep Date:
Leach Date:
N/A
N/A
Analyte RLMDLQualResult
2.79 J 5.01.1Total Alkalinity
2.79 J 5.01.1Bicarbonate Alkalinity as CaCO3
ND 5.01.1Carbonate Alkalinity as CaCO3
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 280-373408
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
alk high 051217.TXT
Units:mg/L
Method: SM 2320B
Preparation: N/A
WC-AT3MB 280-373408/31
Analysis Date:05/12/2017 1932
Analysis Batch:
Prep Batch:
Leach Batch:
N/A
N/A
280-373408
Prep Date:
Leach Date:
N/A
N/A
Analyte RLMDLQualResult
4.41 J 5.01.1Total Alkalinity
4.41 J 5.01.1Bicarbonate Alkalinity as CaCO3
ND 5.01.1Carbonate Alkalinity as CaCO3
TestAmerica Denver 05/23/2017Page 53 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
Water
1.0
Lab Control Sample - Batch: 280-373408
Client Matrix:
Lab Sample ID:
Dilution:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
alk high 051217.TXT
Units:mg/L
Method: SM 2320B
Preparation: N/A
WC-AT3LCS 280-373408/4
Analysis Date:05/12/2017 1730
Analysis Batch:
Prep Batch:
Leach Batch:
280-373408
N/A
N/A
Prep Date:
Leach Date:
N/A
N/A
Analyte QualLimit% Rec.ResultSpike Amount
1000 964 96 90 - 110Total Alkalinity
Water
1.0
Lab Control Sample - Batch: 280-373408
Client Matrix:
Lab Sample ID:
Dilution:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
alk high 051217.TXT
Units:mg/L
Method: SM 2320B
Preparation: N/A
WC-AT3LCS 280-373408/30
Analysis Date:05/12/2017 1928
Analysis Batch:
Prep Batch:
Leach Batch:
280-373408
N/A
N/A
Prep Date:
Leach Date:
N/A
N/A
Analyte QualLimit% Rec.ResultSpike Amount
1000 978 98 90 - 110Total Alkalinity
mg/LUnits:
Water
Dilution:1.0
Duplicate - Batch: 280-373408
Lab Sample ID:
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
alk high 051217.TXT
Method: SM 2320B
Preparation: N/A
WC-AT3280-96675-1
Analysis Date:05/12/2017 1941
Analysis Batch:
Prep Batch:
Leach Batch:
280-373408
N/A
N/A
Prep Date:
Leach Date:
N/A
N/A
Analyte QualLimitRPDResultSample Result/Qual
23902500 4 10Total Alkalinity
TestAmerica Denver 05/23/2017Page 54 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 280-372777
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
100 mL
100 mLUnits:mg/L
Method: SM 2540C
Preparation: N/A
N/A
No Equipment AssignedMB 280-372777/1
Analysis Date:05/09/2017 0904
Analysis Batch:
Prep Batch:
Leach Batch:
N/A
N/A
280-372777
Prep Date:
Leach Date:
N/A
N/A
Analyte RLMDLQualResult
ND 104.7Total Dissolved Solids
Water
1.0
Lab Control Sample - Batch: 280-372777
Client Matrix:
Lab Sample ID:
Dilution:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
100 mL
100 mLUnits:mg/L
Method: SM 2540C
Preparation: N/A
N/A
No Equipment AssignedLCS 280-372777/2
Analysis Date:05/09/2017 0904
Analysis Batch:
Prep Batch:
Leach Batch:
280-372777
N/A
N/A
Prep Date:
Leach Date:
N/A
N/A
Analyte QualLimit% Rec.ResultSpike Amount
500 493 99 86 - 110Total Dissolved Solids
mg/LUnits:
Water
Dilution:1.0
Duplicate - Batch: 280-372777
Lab Sample ID:
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
100 mL
100 mL
Method: SM 2540C
Preparation: N/A
N/A
No Equipment Assigned280-96684-A-1 DU
Analysis Date:05/09/2017 0904
Analysis Batch:
Prep Batch:
Leach Batch:
280-372777
N/A
N/A
Prep Date:
Leach Date:
N/A
N/A
Analyte QualLimitRPDResultSample Result/Qual
390380 4 10Total Dissolved Solids
TestAmerica Denver 05/23/2017Page 55 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 280-372423
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
250 mL
250 mLUnits:mg/L
Method: SM 2540D
Preparation: N/A
N/A
No Equipment AssignedMB 280-372423/3
Analysis Date:05/05/2017 1437
Analysis Batch:
Prep Batch:
Leach Batch:
N/A
N/A
280-372423
Prep Date:
Leach Date:
N/A
N/A
Analyte RLMDLQualResult
ND 4.01.1Total Suspended Solids
Dilution:
Dilution:
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 280-372423
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix:Water
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
mg/L
250 mL
250 mL
250 mL
250 mLmg/L
Method: SM 2540D
Preparation: N/A
N/A
N/A
No Equipment Assigned
No Equipment Assigned
LCS 280-372423/1
LCSD 280-372423/2
Analysis Date:
Prep Date:
Leach Date:
05/05/2017 1437
N/A
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
280-372423
N/A
N/A
Analysis Date:
Prep Date:
Leach Date:
05/05/2017 1437
N/A
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
280-372423
N/A
N/A
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
9497 86 - 114 3 20Total Suspended Solids
Water
05/05/2017 1437
Dilution:Dilution:1.0 1.0
Client Matrix:
LCSD Lab Sample ID:
Client Matrix:Water
Laboratory Control/
Laboratory Duplicate Data Report - Batch: 280-372423
Method: SM 2540D
Preparation: N/A
Units:mg/LLCS 280-372423/1 LCSD 280-372423/2LCS Lab Sample ID:
Analysis Date:
Prep Date:
Leach Date:
Analysis Date:
Prep Date:
Leach Date:
05/05/2017 1437
N/A
N/A
N/A
N/A
LCSD
Result/Qual
LCS
Result/Qual
LCSD Spike
Amount
LCS Spike
AmountAnalyte
94.496.8100100Total Suspended Solids
TestAmerica Denver 05/23/2017Page 56 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
mg/LUnits:
Water
Dilution:1.0
Duplicate - Batch: 280-372423
Lab Sample ID:
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
250 mL
250 mL
Method: SM 2540D
Preparation: N/A
N/A
No Equipment Assigned280-96712-A-1 DU
Analysis Date:05/05/2017 1437
Analysis Batch:
Prep Batch:
Leach Batch:
280-372423
N/A
N/A
Prep Date:
Leach Date:
N/A
N/A
Analyte QualLimitRPDResultSample Result/Qual
3.603.6 J 0 10 JTotal Suspended Solids
TestAmerica Denver 05/23/2017Page 57 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 280-373201
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
051017.txt
Units:mg/L
Method: SM 5310B
Preparation: N/A
WC_SHI3MB 280-373201/46
Analysis Date:05/11/2017 0535
Analysis Batch:
Prep Batch:
Leach Batch:
N/A
N/A
280-373201
Prep Date:
Leach Date:
N/A
N/A
Analyte RLMDLQualResult
ND 1.00.16Total Organic Carbon - Average
Water
1.0
Lab Control Sample - Batch: 280-373201
Client Matrix:
Lab Sample ID:
Dilution:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
051017.txt
100 mLUnits:mg/L
Method: SM 5310B
Preparation: N/A
WC_SHI3LCS 280-373201/45
Analysis Date:05/11/2017 0520
Analysis Batch:
Prep Batch:
Leach Batch:
280-373201
N/A
N/A
Prep Date:
Leach Date:
N/A
N/A
Analyte QualLimit% Rec.ResultSpike Amount
25.0 26.8 107 88 - 112Total Organic Carbon - Average
Dilution:
Dilution:
Water
1.0
1.0
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix:Water
051017.txt
50 mL
051017.txt
50 mL
Method: SM 5310B
Preparation: N/A
WC_SHI3
WC_SHI3
280-96660-D-3 MS
280-96660-D-3 MSD
MS Lab Sample ID:
MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-373201
05/11/2017 0619
N/A
N/A
Analysis Date:
Prep Date:
Leach Date:
Analysis Batch:
Prep Batch:
Leach Batch:
280-373201
N/A
N/A
Analysis Date:
Prep Date:
Leach Date:
05/11/2017 0633
N/A
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
280-373201
N/A
N/A
Analyte RPD LimitRPDLimit
% Rec.
MS MSD MS Qual MSD Qual
107 106 88 - 112 1 15Total Organic Carbon - Average
TestAmerica Denver 05/23/2017Page 58 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
Water
05/11/2017 0619 05/11/2017 0633
Dilution:Dilution:1.0 1.0
Client Matrix:Client Matrix:Water
Method: SM 5310B
Preparation: N/A
Units:mg/L280-96660-D-3 MS 280-96660-D-3 MSDMS Lab Sample ID:MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 280-373201
Analysis Date:
Prep Date:
Leach Date:
N/A
N/A
Analysis Date:
Prep Date:
Leach Date:
N/A
N/A
Amount
Sample
Analyte Result/Qual Amount Result/Qual Result/Qual
MS MSDMS Spike MSD Spike
2.0 25.0 25.0 28.7 28.6Total Organic Carbon - Average
TestAmerica Denver 05/23/2017Page 59 of 69
Quality Control Results
Job Number: 280-96675-1Client: Waste Management
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 280-372247
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:300 mLUnits:mg/L
Method: SM5210B
Preparation: N/A
N/A
No Equipment AssignedMB 280-372247/4
Analysis Date:05/04/2017 1654
Analysis Batch:
Prep Batch:
Leach Batch:
N/A
N/A
280-372247
Prep Date:
Leach Date:
N/A
N/A
Analyte RLMDLQualResult
ND 2.00.24Biochemical Oxygen Demand
Water
1.0
Lab Control Sample - Batch: 280-372247
Client Matrix:
Lab Sample ID:
Dilution:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:300 mLUnits:mg/L
Method: SM5210B
Preparation: N/A
N/A
No Equipment AssignedLCS 280-372247/3
Analysis Date:05/04/2017 1654
Analysis Batch:
Prep Batch:
Leach Batch:
280-372247
N/A
N/A
Prep Date:
Leach Date:
N/A
N/A
Analyte QualLimit% Rec.ResultSpike Amount
198 177 90 85 - 115Biochemical Oxygen Demand
mg/LUnits:
Water
Dilution:1.0
Duplicate - Batch: 280-372247
Lab Sample ID:
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:300 mL
Method: SM5210B
Preparation: N/A
N/A
No Equipment Assigned280-96678-M-1 DU
Analysis Date:05/04/2017 1655
Analysis Batch:
Prep Batch:
Leach Batch:
280-372247
N/A
N/A
Prep Date:
Leach Date:
N/A
N/A
Analyte QualLimitRPDResultSample Result/Qual
10.39.8 4 20Biochemical Oxygen Demand
TestAmerica Denver 05/23/2017Page 60 of 69
Quality Control Results
Client: Waste Management Job Number: 280-96675-1
Laboratory Chronicle
05/04/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:05/03/2017 16:50
280-96675-1 3406-T01
P:5030B 280-96675-L-1 280-373992 05/17/2017 19:59 ADDTAL DEN1
A:8260B 280-96675-L-1 280-373992 05/17/2017 19:59 ADDTAL DEN1
P:3005A 280-96675-F-1-A 280-373731 280-372301 05/15/2017 07:16 TEBTAL DEN1
A:6010C 280-96675-F-1-A 280-373731 280-372301 05/16/2017 06:44 LLBTAL DEN1
P:3005A 280-96675-F-1-A 280-373855 280-372301 05/15/2017 07:16 TEBTAL DEN1
A:6010C 280-96675-F-1-A 280-373855 280-372301 05/16/2017 20:39 CRRTAL DEN1
P:3005A 280-96675-F-1-A 280-373928 280-372301 05/15/2017 07:16 TEBTAL DEN1
A:6010C 280-96675-F-1-A 280-373928 280-372301 05/17/2017 09:08 CRRTAL DEN1
P:3005A 280-96675-F-1-D 280-373738 280-372302 05/15/2017 07:16 TEBTAL DEN1
A:6020A 280-96675-F-1-D 280-373738 280-372302 05/16/2017 02:06 JMTAL DEN1
P:7470A 280-96675-F-1-G 280-374456 280-374242 05/19/2017 11:35 CDHTAL DEN1
A:7470A 280-96675-F-1-G 280-374456 280-374242 05/19/2017 18:00 CDHTAL DEN1
A:300.0 280-96675-B-1 280-373891 05/17/2017 12:59 AFBTAL DEN2
A:300.0 280-96675-B-1 280-373891 05/17/2017 13:16 AFBTAL DEN20
A:350.1 280-96675-D-1 280-373940 05/16/2017 15:19 MASTAL DEN500
P:365.2/365.3/36
5
280-96675-G-1-A 280-373778 280-373136 05/11/2017 10:39 MASTAL DEN10
A:365.1 280-96675-G-1-A 280-373778 280-373136 05/16/2017 12:54 MASTAL DEN10
A:410.4 280-96675-D-1 280-374088 05/18/2017 09:12 CCJTAL DEN10
A:Nitrate by calc 280-96675-A-1 280-374303 05/19/2017 11:51 RKSTAL DEN1
A:SM 2320B 280-96675-C-1 280-373408 05/12/2017 18:39 A1DTAL DEN1
A:SM 2540C 280-96675-B-1 280-372777 05/09/2017 09:04 JAPTAL DEN1
A:SM 2540D 280-96675-B-1 280-372423 05/05/2017 14:37 SVCTAL DEN1
A:SM 5310B 280-96675-G-1 280-373201 05/11/2017 08:22 CCJTAL DEN10
A:SM5210B 280-96675-C-1 280-372247 05/04/2017 16:55 RSMTAL DEN5
A:Field Sampling 280-96675-A-1 280-372309 05/03/2017 14:50 C1KTAL DEN1
05/04/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:05/03/2017 16:50
280-96675-1 MS 3406-T01
P:3005A 280-96675-F-1-B MS 280-373731 280-372301 05/15/2017 07:16 TEBTAL DEN1
A:6010C 280-96675-F-1-B MS 280-373731 280-372301 05/16/2017 06:49 LLBTAL DEN1
P:3005A 280-96675-F-1-B MS 280-373855 280-372301 05/15/2017 07:16 TEBTAL DEN1
A:6010C 280-96675-F-1-B MS 280-373855 280-372301 05/16/2017 20:44 CRRTAL DEN1
P:3005A 280-96675-F-1-B MS 280-373928 280-372301 05/15/2017 07:16 TEBTAL DEN1
A:6010C 280-96675-F-1-B MS 280-373928 280-372301 05/17/2017 09:13 CRRTAL DEN1
P:3005A 280-96675-F-1-E MS 280-373738 280-372302 05/15/2017 07:16 TEBTAL DEN1
A:6020A 280-96675-F-1-E MS 280-373738 280-372302 05/16/2017 02:16 JMTAL DEN1
A = Analytical Method P = Prep Method TestAmerica Denver
05/23/2017Page 61 of 69
Quality Control Results
Client: Waste Management Job Number: 280-96675-1
Laboratory Chronicle
05/04/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:05/03/2017 16:50
280-96675-1 MSD 3406-T01
P:3005A 280-96675-F-1-C
MSD
280-373731 280-372301 05/15/2017 07:16 TEBTAL DEN1
A:6010C 280-96675-F-1-C
MSD
280-373731 280-372301 05/16/2017 06:51 LLBTAL DEN1
P:3005A 280-96675-F-1-C
MSD
280-373855 280-372301 05/15/2017 07:16 TEBTAL DEN1
A:6010C 280-96675-F-1-C
MSD
280-373855 280-372301 05/16/2017 20:46 CRRTAL DEN1
P:3005A 280-96675-F-1-C
MSD
280-373928 280-372301 05/15/2017 07:16 TEBTAL DEN1
A:6010C 280-96675-F-1-C
MSD
280-373928 280-372301 05/17/2017 09:16 CRRTAL DEN1
P:3005A 280-96675-F-1-F
MSD
280-373738 280-372302 05/15/2017 07:16 TEBTAL DEN1
A:6020A 280-96675-F-1-F
MSD
280-373738 280-372302 05/16/2017 02:21 JMTAL DEN1
05/04/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:05/03/2017 16:50
280-96675-1 DU 3406-T01
A:SM 2320B 280-96675-B-1 DU 280-373408 05/12/2017 19:41 A1DTAL DEN1
05/04/2017 08:55
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:05/03/2017 16:00
280-96675-2 TRIP BLANK
P:5030B 280-96675-A-2 280-373992 05/17/2017 18:32 ADDTAL DEN1
A:8260B 280-96675-A-2 280-373992 05/17/2017 18:32 ADDTAL DEN1
A = Analytical Method P = Prep Method TestAmerica Denver
05/23/2017Page 62 of 69
Quality Control Results
Client: Waste Management Job Number: 280-96675-1
Laboratory Chronicle
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:N/A Received Date/Time:N/A
MB N/A
P:5030B MB 280-373992/6 280-373992 05/17/2017 17:50 ADDTAL DEN1
A:8260B MB 280-373992/6 280-373992 05/17/2017 17:50 ADDTAL DEN1
P:3005A MB 280-372301/1-A 280-373731 280-372301 05/15/2017 07:16 TEBTAL DEN1
A:6010C MB 280-372301/1-A 280-373731 280-372301 05/16/2017 06:39 LLBTAL DEN1
P:3005A MB 280-372301/1-A 280-373855 280-372301 05/15/2017 07:16 TEBTAL DEN1
A:6010C MB 280-372301/1-A 280-373855 280-372301 05/16/2017 20:34 CRRTAL DEN1
P:3005A MB 280-372301/1-A 280-373928 280-372301 05/15/2017 07:16 TEBTAL DEN1
A:6010C MB 280-372301/1-A 280-373928 280-372301 05/17/2017 09:03 CRRTAL DEN1
P:3005A MB 280-372302/1-A 280-373738 280-372302 05/15/2017 07:16 TEBTAL DEN1
A:6020A MB 280-372302/1-A 280-373738 280-372302 05/16/2017 01:57 JMTAL DEN1
P:7470A MB 280-374242/1-A 280-374456 280-374242 05/19/2017 11:35 CDHTAL DEN1
A:7470A MB 280-374242/1-A 280-374456 280-374242 05/19/2017 17:36 CDHTAL DEN1
A:300.0 MB 280-373891/6 280-373891 05/17/2017 10:35 AFBTAL DEN1
A:350.1 MB 280-373940/103 280-373940 05/16/2017 15:25 MASTAL DEN1
P:365.2/365.3/36
5
MB 280-373136/11-A 280-373778 280-373136 05/11/2017 10:39 MASTAL DEN1
A:365.1 MB 280-373136/11-A 280-373778 280-373136 05/16/2017 12:54 MASTAL DEN1
A:410.4 MB 280-374088/5 280-374088 05/18/2017 09:12 CCJTAL DEN1
A:Nitrate by calc MB 280-374303/1 280-374303 05/19/2017 11:51 RKSTAL DEN1
A:SM 2320B MB 280-373408/5 280-373408 05/12/2017 17:34 A1DTAL DEN1
A:SM 2320B MB 280-373408/31 280-373408 05/12/2017 19:32 A1DTAL DEN1
A:SM 2540C MB 280-372777/1 280-372777 05/09/2017 09:04 JAPTAL DEN1
A:SM 2540D MB 280-372423/3 280-372423 05/05/2017 14:37 SVCTAL DEN1
A:SM 5310B MB 280-373201/46 280-373201 05/11/2017 05:35 CCJTAL DEN1
A:SM5210B MB 280-372247/4 280-372247 05/04/2017 16:54 RSMTAL DEN1
A = Analytical Method P = Prep Method TestAmerica Denver
05/23/2017Page 63 of 69
Quality Control Results
Client: Waste Management Job Number: 280-96675-1
Laboratory Chronicle
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:N/A Received Date/Time:N/A
LCS N/A
P:5030B LCS 280-373992/4 280-373992 05/17/2017 18:11 ADDTAL DEN1
A:8260B LCS 280-373992/4 280-373992 05/17/2017 18:11 ADDTAL DEN1
P:3005A LCS 280-372301/2-A 280-373731 280-372301 05/15/2017 07:16 TEBTAL DEN1
A:6010C LCS 280-372301/2-A 280-373731 280-372301 05/16/2017 06:41 LLBTAL DEN1
P:3005A LCS 280-372301/2-A 280-373855 280-372301 05/15/2017 07:16 TEBTAL DEN1
A:6010C LCS 280-372301/2-A 280-373855 280-372301 05/16/2017 20:36 CRRTAL DEN1
P:3005A LCS 280-372301/2-A 280-373928 280-372301 05/15/2017 07:16 TEBTAL DEN1
A:6010C LCS 280-372301/2-A 280-373928 280-372301 05/17/2017 09:06 CRRTAL DEN1
P:3005A LCS 280-372302/2-A 280-373738 280-372302 05/15/2017 07:16 TEBTAL DEN1
A:6020A LCS 280-372302/2-A 280-373738 280-372302 05/16/2017 02:02 JMTAL DEN1
P:7470A LCS 280-374242/2-A 280-374456 280-374242 05/19/2017 11:35 CDHTAL DEN1
A:7470A LCS 280-374242/2-A 280-374456 280-374242 05/19/2017 17:38 CDHTAL DEN1
A:300.0 LCS 280-373891/4 280-373891 05/17/2017 09:59 AFBTAL DEN1
A:350.1 LCS 280-373940/101 280-373940 05/16/2017 15:21 MASTAL DEN1
P:365.2/365.3/36
5
LCS 280-373136/9-A 280-373778 280-373136 05/11/2017 10:39 MASTAL DEN1
A:365.1 LCS 280-373136/9-A 280-373778 280-373136 05/16/2017 12:54 MASTAL DEN1
A:410.4 LCS 280-374088/3 280-374088 05/18/2017 09:12 CCJTAL DEN1
A:SM 2320B LCS 280-373408/4 280-373408 05/12/2017 17:30 A1DTAL DEN1
A:SM 2320B LCS 280-373408/30 280-373408 05/12/2017 19:28 A1DTAL DEN1
A:SM 2540C LCS 280-372777/2 280-372777 05/09/2017 09:04 JAPTAL DEN1
A:SM 2540D LCS 280-372423/1 280-372423 05/05/2017 14:37 SVCTAL DEN1
A:SM 5310B LCS 280-373201/45 280-373201 05/11/2017 05:20 CCJTAL DEN1
A:SM5210B LCS 280-372247/3 280-372247 05/04/2017 16:54 RSMTAL DEN1
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:N/A Received Date/Time:N/A
LCSD N/A
A:300.0 LCSD 280-373891/5 280-373891 05/17/2017 10:17 AFBTAL DEN1
A:350.1 LCSD
280-373940/102
280-373940 05/16/2017 15:23 MASTAL DEN1
P:365.2/365.3/36
5
LCSD
280-373136/10-A
280-373778 280-373136 05/11/2017 10:39 MASTAL DEN1
A:365.1 LCSD
280-373136/10-A
280-373778 280-373136 05/16/2017 12:54 MASTAL DEN1
A:410.4 LCSD 280-374088/4 280-374088 05/18/2017 09:12 CCJTAL DEN1
A:SM 2540D LCSD 280-372423/2 280-372423 05/05/2017 14:37 SVCTAL DEN1
A = Analytical Method P = Prep Method TestAmerica Denver
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Quality Control Results
Client: Waste Management Job Number: 280-96675-1
Laboratory Chronicle
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:N/A Received Date/Time:N/A
MRL N/A
A:300.0 MRL 280-373891/3 280-373891 05/17/2017 09:42 AFBTAL DEN1
05/09/2017 09:15
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:05/08/2017 10:15
MS N/A
P:5030B 280-96884-G-1 MS 280-373992 05/17/2017 21:44 ADDTAL DEN1
A:8260B 280-96884-G-1 MS 280-373992 05/17/2017 21:44 ADDTAL DEN1
P:7470A 280-96372-H-3-B MS 280-374456 280-374242 05/19/2017 11:35 CDHTAL DEN1
A:7470A 280-96372-H-3-B MS 280-374456 280-374242 05/19/2017 17:47 CDHTAL DEN1
A:300.0 280-96903-E-2 MS 280-373891 05/17/2017 12:05 AFBTAL DEN10
A:350.1 280-96745-A-11 MS 280-373940 05/16/2017 14:51 MASTAL DEN1
P:365.2/365.3/36
5
280-96926-A-5-B MS 280-373778 280-373136 05/11/2017 10:39 MASTAL DEN1
A:365.1 280-96926-A-5-B MS 280-373778 280-373136 05/16/2017 12:54 MASTAL DEN1
A:410.4 280-96659-B-1 MS 280-374088 05/18/2017 09:12 CCJTAL DEN1
A:SM 5310B 280-96660-D-3 MS 280-373201 05/11/2017 06:19 CCJTAL DEN1
05/09/2017 09:15
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:05/08/2017 10:15
MSD N/A
P:5030B 280-96884-G-1 MSD 280-373992 05/17/2017 22:05 ADDTAL DEN1
A:8260B 280-96884-G-1 MSD 280-373992 05/17/2017 22:05 ADDTAL DEN1
P:7470A 280-96372-H-3-C
MSD
280-374456 280-374242 05/19/2017 11:35 CDHTAL DEN1
A:7470A 280-96372-H-3-C
MSD
280-374456 280-374242 05/19/2017 17:49 CDHTAL DEN1
A:300.0 280-96903-E-2 MSD 280-373891 05/17/2017 12:23 AFBTAL DEN10
A:350.1 280-96745-A-11 MSD 280-373940 05/16/2017 14:53 MASTAL DEN1
P:365.2/365.3/36
5
280-96926-A-5-C
MSD
280-373778 280-373136 05/11/2017 10:39 MASTAL DEN1
A:365.1 280-96926-A-5-C
MSD
280-373778 280-373136 05/16/2017 12:54 MASTAL DEN1
A:410.4 280-96659-B-1 MSD 280-374088 05/18/2017 09:12 CCJTAL DEN1
A:SM 5310B 280-96660-D-3 MSD 280-373201 05/11/2017 06:33 CCJTAL DEN1
A = Analytical Method P = Prep Method TestAmerica Denver
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Quality Control Results
Client: Waste Management Job Number: 280-96675-1
Laboratory Chronicle
05/09/2017 09:35
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time:Received Date/Time:05/07/2017 06:00
DU N/A
A:300.0 280-96903-E-2 DU 280-373891 05/17/2017 11:48 AFBTAL DEN10
A:SM 2540C 280-96684-A-1 DU 280-372777 05/09/2017 09:04 JAPTAL DEN1
A:SM 2540D 280-96712-A-1 DU 280-372423 05/05/2017 14:37 SVCTAL DEN1
A:SM5210B 280-96678-M-1 DU 280-372247 05/04/2017 16:55 RSMTAL DEN1
Lab References:
TAL DEN = TestAmerica Denver
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05/23/2017Page 66 of 69
05/23/2017Page 67 of 69
05/23/2017Page 68 of 69
Login Sample Receipt Checklist
Client: Waste Management Job Number: 280-96675-1
Login Number: 96675
Question Answer Comment
Creator: Woodworth, Sean P
List Source: TestAmerica Denver
List Number: 1
N/ARadioactivity either was not measured or, if measured, is at or below
background
TrueThe cooler's custody seal, if present, is intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the sample IDs on the containers and
the COC.
TrueSamples are received within Holding Time (Excluding tests with immediate
HTs)..
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueVOA sample vials do not have headspace or bubble is <6mm (1/4") in
diameter.
TrueIf necessary, staff have been informed of any short hold time or quick TAT
needs
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
TrueSampling Company provided.
TrueSamples received within 48 hours of sampling.
TrueSamples requiring field filtration have been filtered in the field.
TrueChlorine Residual checked.
TestAmerica Denver 05/23/2017Page 69 of 69

APPENDIX B

GROUNDWATER FLOW REGIME REPORT

Including Drawing 1 and Tables 5 & 6

Piedmont Landfill and Recycling Center, Permit # 34-06 Joyce Engineering
Groundwater Flow Regime Report May 2017
1

Piedmont Landfill & Recycling Center
Permit 34-06

APPENDIX B:

Groundwater Flow Regime Report – March 2017

On behalf of Waste Management, Joyce Engineering has reviewed groundwater flow
rates and flow directions at the Piedmont Landfill and Recycling Center for the annual
groundwater sampling event of 2017. The groundwater flow and direction calculations
presented in this report are based on groundwater elevation data obtained by ProTech on March
15, 2017. The information provided in this report will satisfy, in part, the environmental
reporting requirements of Piedmont Landfill's Municipal Solid Waste Permit.

The groundwater level measurements taken during the above referenced sampling event
were used to construct the groundwater surface contour map attached to this report as Drawing
1. A summary of groundwater elevations obtained during this and previous sampling events is
provided in Table 5. The potentiometric contours and the groundwater flow directions presented
in Drawing 1 were used to calculate hydraulic gradients for the site. The hydraulic gradient
calculations are provided in Table 6. The hydraulic gradients (i) ranged from 0.018 ft/ft to 0.027
ft/ft. These gradients are generally consistent with past interpretations for the site.

An effective porosity value (n) of 41 percent was used in the equation based on an
average of six laboratory-derived porosities as reported in the April 1994 Design Hydrogeologic
Study, prepared by RUST Environment & Infrastructure. Hydraulic conductivities (K) were also
taken from the Design Hydrogeologic Study, and were based on slug test data from piezometers
located nearest the respective groundwater flow paths. Using the gradient (i) along each flow
path, the linear flow velocity (V) was estimated using the modified Darcy equation: V = i K/n.
The flow rate calculations are presented in Table 6.

As shown on Drawing 1, groundwater flow at the site is generally to the northwest;
however, a hydraulic divide runs through the site such that the local groundwater flow on the
northeast side of the landfill is toward the north while groundwater flow on the southwest side of
the landfill is toward the southwest. The velocity along the flow segments shown on Drawing 1
were as follows:

SEGMENT VELOCITY DIRECTION
Segment i1 20.0 ft/yr NW to N
Segment i2 10.8 ft/yr W to SW
Segment i3 9.6 ft/yr N
Segment i4 7.7 ft/yr SW

Piedmont Landfill and Recycling Center, Permit # 34-06 Joyce Engineering
Groundwater Flow Regime Report May 2017
2

The average groundwater flow rate for the 2017 event was approximately 12.8 feet/year.
These groundwater flow directions and velocities are consistent with those calculated during
other recent events.

The groundwater measurements obtained during the 2017 annual event are generally
consistent with those obtained during previous sampling events. Based on this information, it is
our opinion that the groundwater monitoring system continues to be adequate for the detection of
the release of solid waste constituents to the environment.

Prepared by: _______________________________
G. Van Ness Burbach, Ph.D., P.G.
Sr. Technical Consultant

2211 West Meadowview Road, Suite 101
Greensboro, North Carolina 27407

Attachments: Drawing 1 – Groundwater Potentiometric Surface Map
Table 5 – Historical Groundwater Elevations
Table 6 – Groundwater Flow Rate Calculations

7
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0 78076077078
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77076077075076078079080077079
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79075076077075076075077078075075076077078079080081082083084085086087088089090091091090089088087086085084082081080079078077086080081
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0 740750750750760770780790800800810830840850750760770780790800810810800790780770750740740810800790780770760750740740850840830820810800790780770760750
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780750755760765770775775770765760755750745 740740745745745780i2i1SITEENTRANCEGUILFORDCOUNTYFORSYTHCOUNTYMW-09R738.95MW-09ABANDONED (NM)MW-12DNMMW-12745.40MW-04743.98MW-05738.74MW-08743.13MW-01779.55MW-06NMMW-11748.00MW-11DNMMW-03744.51MW-4DNMMW-02748.90MW-10746.13MW-07746.77750750740740i3i4CENTERLINE OF STREAMGROUNDWATER MONITORING WELL LOCATION ANDIDENTIFICATION WITH STATIC WATER LEVEL ELEVATION (FEETAMSL)GROUNDWATER SURFACE CONTOUR [FEETABOVE MEAN SEA LEVEL (AMSL)]EXISTING 2' TOPOGRAPHIC CONTOUREXISTING 10' TOPOGRAPHIC CONTOUREXISTING ROADLEGEND1.2.3.4.5.6.7.TOPOGRAPHIC CONTOUR INTERVAL = 2 FEET.GROUNDWATER SURFACE CONTOUR INTERVAL = 5 FEET.STATIC WATER LEVELS MEASURED ON 03/15/17.GROUNDWATER CONTOURS BASED ON LINEAR INTERPOLATION BETWEEN ANDEXTRAPOLATION FROM KNOWN DATA, TOPOGRAPHIC CONTOURS, AND KNOWNFIELD CONDITIONS. THEREFORE, GROUNDWATER CONTOURS MAY NOT REFLECTACTUAL GROUNDWATER CONDITIONS.TOPOGRAPHIC MAP AND SURVEYED WELL LOCATIONS PROVIDED TO JOYCEENGINEERING, INC. BY PIEDMONT LANDFILL.GROUNDWATER CONTOUR LINES SHOW THE WATER TABLE SHAPE ANDELEVATION. THESE CONTOURS ARE INFERRED LINES FOLLOWING THEGROUNDWATER SURFACE AT A CONSTANT ELEVATION ABOVE SEA LEVEL. THEGROUNDWATER FLOW DIRECTION IS GENERALLY PERPENDICULAR TO THEGROUNDWATER SURFACE CONTOURS, SIMILAR TO THE RELATIONSHIP BETWEENSURFACE WATER FLOW AND TOPOGRAPHIC CONTOURS.THE LOCATIONS OF SURFACE WATER MONITORING POINTS ARE APPROXIMATEAS SHOWN.APPROXIMATE LIMITS OF WASTEPROPERTY LINESEGMENT USED FOR GRADIENT CALCULATIONSGROUNDWATER FLOW DIRECTIONNOTES:i740SURFACE WATER MONITORING POINTSMW-9R741.98FLOW PATH LENGTHii= 1,280 LF= 1,191 LF= 670 LF= 836 LFiiPROJECT NO.APPROVED
CHECKED
DRAWN
DESIGNED
DATE
DATE REVISIONS AND RECORD OF ISSUE BYNO APPCKSCALE All rights reserved.
Ó Joyce Engineering, Inc.DRAWING NO.N:\Dwgs\Drawings-Current\WMI\Piedmont\GW EVENT MAPS\GW EVENT 03-17.dwg Layout=Layout1
2211 W. MEADOWVIEW ROAD
GREENSBORO, NC 27407
PHONE: [phone]PIEDMONT LANDFILL AND RECYCLING CENTER
KERNERSVILLE, NORTH CAROLINA
20171AS NOTEDGROUNDWATER SURFACE MAP
MARCH 15, 2017
PERMIT NO. 34-06
DG
RWH
ACE
GVB
04/11/170(FEET)GRAPHIC SCALE400200100
TABLE 5: HISTORICAL GROUNDWATER ELEVATIONSWell ID: MW-01 MW-02 MW-03 MW-04 MW-04D MW-05 MW-06 MW-07 MW-08 MW-09 MW-09R MW-10 MW-11 MW-11D MW-12 MW-12DTOC Elevation:823.93 778.04 770.08 756.92 757.33 743.17 800.82 771.57 748.95 770.62 764.95 777.20 776.80 776.36 751.48 751.53Well Depth:49.0 35.5 38.0 27.0 62.0 20.5 29.6 31.3 18.8 35.0 43.0 38.0 35.0 93.5 18.0 43.330-Jan-1998 781.82 750.71 746.26 745.46 745.46 738.49 779.84 744.32 744.30 737.47 NA 744.42 749.08 747.66 746.58 747.0521-Jul-1998 784.78 750.06 746.76 743.92 743.78 737.14 781.04 745.07 741.20 738.96 NA 744.35 748.95 748.58 745.88 746.1114-Jan-1999 780.98 749.16 744.91 744.27 744.16 737.60 777.86 743.57 742.68 736.62 NA 743.63 748.09 747.74 745.93 746.1127-Jul-1999 780.48 749.08 744.86 743.26 743.28 734.04 777.52 743.92 740.53 737.12 NA 743.62 748.05 747.75 745.53 745.6820-Jan-2000 780.30 748.51 744.83 744.77 744.43 737.82 777.27 743.87 743.18 NA 737.14 743.90 748.36 747.97 746.28 746.5312-Jul-2001 780.10 748.73 745.30 742.88 743.06 737.08 776.81 744.25 740.40 NA 738.12 743.66 747.77 747.44 745.45 745.7124-Jan-2001 778.93 748.91 744.43 744.69 744.73 737.72 775.84 743.40 743.41 NA 737.35 743.49 747.85 747.54 746.06 746.5417,18-Jul-2001 779.59 748.41 744.61 742.72 742.78 736.76 776.08 743.92 739.99 NA 737.77 743.35 749.45 747.09 745.45 745.4030,31-Jan-2002 777.29 748.14 743.08 743.09 743.49 737.37 773.72 742.57 742.17 NA 736.40 742.74 747.35 747.03 745.14 742.4217,18-Jul-2002 776.47 747.29 742.88 741.80 741.93 736.48 772.97 742.57 738.97 NA 735.86 742.30 746.54 746.21 744.27 744.4420,21-Jan-2003 777.12 748.14 745.45 743.87 743.96 737.40 775.08 744.06 742.51 NA 738.06 743.60 748.05 746.57 745.50 745.9223,24-Jul-2003 782.10 749.48 748.08 743.92 743.83 738.07 778.39 745.53 742.74 NA 741.80 744.60 748.40 748.16 745.83 746.0821,22-Jan-2004 781.75 748.89 746.57 743.77 743.84 737.36 778.02 744.37 742.30 NA 739.10 743.91 747.86 747.47 745.87 746.0727,28-Jul-2004 780.80 748.24 745.18 742.27 742.43 736.77 776.65 743.96 739.65 NA 738.45 743.37 747.26 746.96 745.03 745.3119,20-Jan-2005 780.38 749.11 745.43 744.35 744.37 737.97 777.46 744.56 743.35 NA 739.05 744.95 748.39 747.75 746.02 746.3911,12,13-Jul-2005 780.55 748.59 744.82 742.81 742.87 735.22 777.51 744.96 740.87 NA 739.20 744.51 747.60 747.26 745.21 745.4316,17,18-Jan-2006 778.76 748.58 744.75 744.03 744.13 737.77 776.53 744.19 743.40 NA 737.95 744.21 747.70 747.36 745.73 746.0910,11,12-Jul-2006 779.27 748.17 744.47 743.69 743.58 737.39 776.09 744.08 741.90 NA 738.07 744.00 747.05 746.76 745.51 745.7722, 23, 24-Jan-2007 781.16 749.52 745.64 744.30 744.30 738.22 778.37 745.67 743.79 NA 739.33 745.14 748.40 747.94 745.95 746.3312,13-Sep-2007 781.71 747.84 743.58 741.65 741.58 736.57 773.75 744.06 738.53 NA 737.60 743.15 746.70 746.26 744.48 744.4419-Mar-2008 780.19 749.02 744.26 744.04 744.04 737.91 777.94 744.85 743.34 NA 737.35 744.87 747.99 747.62 745.42 746.0511-Sep-2008 779.78 747.53 743.05 742.03 741.98 736.92 775.93 743.93 739.86 NA 736.89 743.55 746.55 746.14 744.54 744.6511-Mar-2009 779.55 749.34 744.67 743.91 744.14 737.96 777.02 745.84 743.52 NA 738.35 747.67 748.13 747.76 745.37 746.0116-Sep-2009 780.08 747.87 743.28 741.69 741.56 736.64 775.82 744.64 738.49 NA 737.13 743.37 746.84 746.36 744.41 744.3810-Mar-2010 781.45 750.17 745.87 744.22 744.21 738.17 779.04 748.14 743.24 NA 741.16 748.24 749.06 748.61 745.33 746.2316-Sep-2010 781.85 748.47 744.64 742.51 742.53 737.22 777.86 745.57 740.03 NA 737.90 744.90 747.42 747.07 744.86 745.0815-Mar-2011 780.68 749.36 745.05 743.89 744.35 738.29 778.17 746.17 743.74 NA 738.35 745.14 748.42 747.47 744.91 745.6314-Sep-2011 779.51 747.58 742.58 742.01 741.95 736.34 775.42 744.48 739.28 NA 736.20 742.70 746.64 746.26 744.35 744.6614-Mar-2012 779.74 748.97 744.85 743.92 743.91 738.05 777.61 746.82 742.95 NA 738.28 746.07 748.02 747.48 745.37 745.7212-Sep-2012 779.25 748.01 743.26 742.42 742.35 737.39 775.87 744.70 740.40 NA 737.13 744.40 746.82 746.53 744.57 744.9120-Mar-2013 778.80 749.52 744.09 744.22 744.15 738.26 777.37 746.86 743.31 NA 738.28 747.16 748.46 748.05 745.25 746.1018-Sep-2013 780.36 748.53 744.23 742.68 742.60 737.61 777.12 745.97 740.20 NA 737.95 744.95 747.49 747.11 744.72 745.2319-Mar-2014 779.73 749.82 744.80 744.73 744.65 738.97 777.92 748.47 744.45 NA 738.93 747.67 748.84 748.42 745.61 746.4017-Sep-2014 780.05 748.14 743.93 742.40 742.31 737.67 776.56 745.44 739.57 NA 738.10 744.27 747.12 746.80 744.62 744.9318-Mar-2015 778.22 749.23 744.35 744.19 744.13 738.49 776.65 746.59 743.36 NA 738.72 746.72 748.20 747.75 745.40 746.0316,17-Sep-2015 777.99 747.54 742.86 740.94 742.13 737.48 DRY 744.47 739.01 NA 737.24 743.68 746.52 746.14 744.21 744.4516-Mar-2016 780.66 750.37 746.06 744.42 NM 738.86 NM 749.62 743.62 NA 741.98 749.74 749.46 NM 745.66 NM15-Mar-2017 779.55 748.90 744.51 743.98 NM 738.74 NM 746.77 743.13 NA 738.95 746.13 748.00 NM 745.40 NMNotes:TOC = Top of PVC casing. All depths in feet measured from TOC. All water level elevations are reported in feet above mean sea level. TOC elevation for MW-02 is revised reflecting improvements made to the well in July 2001 prior to sampling. NA = data not available.DRY = Indicates the monitoring well was found dry or with water level too low to gauge in the field. NM = Not Measured. Piedmont Landfill and Recycling Center, Permit # 34-06Joyce Engineering
TABLE 6:GROUNDWATER FLOW RATE CALCULATIONSElevation Gradient Velocity(ft AMSL)(i, ft/ft) (V, ft/yr)780745780750755740755740AVERAGE:0.023 12.8Notes:An effective porosity (“n” ) of 41% was based on average laboratory-derived porosity as reported in the April 1994 Design Hydrogeologic Study, prepared by RUST Environment & Infrastructure.Hydraulic conductivities (“K”) were also taken from the Design Hydrogeologic Study, and were based on slug test data from piezometers originally located nearest the respective groundwater flow paths. Groundwater Linear Flow Velocity calculated using the modified Darcy equation: V = i K / n .Gradient Calculation Segments are shown on Drawing 1.i 21.70E-04 0.41 1191 W-SW 0.025i 40.027836 SW 0.018 7.720.01280 NW-N10.8GRADIENT CALCULATION SEGMENTFLOW DIRECTIONMarch 15, 2017i 1FLOW SEGMENT LENGTH (ft)2.90E-04EFFECTIVE POROSITY (n, unitless)0.41HYDRAULIC CONDUCTIVITY (K, cm/s)HYDRAULIC CONDUCTIVITY (K, ft/s)1.70E-04 0.419.51E-065.58E-065.58E-060.022 9.6i 31.70E-04 5.58E-06 0.41 670 N Piedmont Landfill and Recycling Center, Permit # 34-06Joyce Engineering