4502_HendersonCountyKimberlyMSWLF_GWMR_20170427

#=CL#
March 16, 2017
LIMS USE: FR - MICHAEL BALDWIN
LIMS OBJECT ID: 92333045
92333045
Project:
Pace Project No.:
RE:
Mr. Michael Baldwin
Kimberly Clark
32 Smyth Avenue
Hendersonville, NC 28793
South Landfill MW's
Dear Mr. Baldwin:
Enclosed are the analytical results for sample(s) received by the laboratory on March 10, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 31
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92333045
South Landfill MW's
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 31
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92333045
South Landfill MW's
Lab ID Sample ID Matrix Date Collected Date Received
92333045001 MW-1S Water 03/10/17 13:30 03/10/17 15:50
92333045002 MW-2S Water 03/10/17 00:00 03/10/17 15:50
92333045003 MW-3S Water 03/10/17 00:00 03/10/17 15:50
92333045004 MW-4S Water 03/10/17 14:15 03/10/17 15:50
92333045005 MW-5S Water 03/10/17 14:30 03/10/17 15:50
92333045006 MW-6S Water 03/10/17 14:00 03/10/17 15:50
92333045007 MW-7S Water 03/10/17 13:50 03/10/17 15:50
92333045008 TVL BLK Water 03/10/17 09:00 03/10/17 15:50
92333045009 EQ BLANK Water 03/10/17 09:05 03/10/17 15:50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 31
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92333045
South Landfill MW's
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92333045001 MW-1S EPA 8260 63 PASI-CZDO
92333045004 MW-4S EPA 8260 63 PASI-CZDO
92333045005 MW-5S EPA 8260 63 PASI-CZDO
92333045006 MW-6S EPA 8260 63 PASI-CZDO
92333045007 MW-7S EPA 8260 63 PASI-CZDO
92333045008 TVL BLK EPA 8260 63 PASI-CZDO
92333045009 EQ BLANK EPA 8260 63 PASI-CZDO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92333045
South Landfill MW's
Sample:MW-1S Lab ID:92333045001 Collected:03/10/17 13:30 Received:03/10/17 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Mark
Swann 03/10/17 13:301
Collected Date 3/10/17 03/10/17 13:301
Collected Time 13:30 03/10/17 13:301
Field pH 5.3 Std. Units 03/10/17 13:300.10 0.10 1
Field Temperature 14.2 deg C 03/10/17 13:300.50 0.50 1
Static Water Level 17.98 feet 03/10/17 13:301
Field Specific Conductance 213 umhos/cm 03/10/17 13:301.0 1.0 1
Turbidity 9.76 NTU 03/10/17 13:301.0 1.0 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/13/17 16:34 67-64-125.0 10.0 1
Benzene ND ug/L 03/13/17 16:34 71-43-21.0 0.25 1
Bromobenzene ND ug/L 03/13/17 16:34 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 03/13/17 16:34 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 03/13/17 16:34 75-27-41.0 0.18 1
Bromoform ND ug/L 03/13/17 16:34 75-25-21.0 0.26 1
Bromomethane ND ug/L 03/13/17 16:34 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 03/13/17 16:34 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 03/13/17 16:34 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/13/17 16:34 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/13/17 16:34 75-00-31.0 0.54 1
Chloroform ND ug/L 03/13/17 16:34 67-66-31.0 0.14 1
Chloromethane 0.11J ug/L 03/13/17 16:34 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 03/13/17 16:34 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 03/13/17 16:34 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 03/13/17 16:34 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 03/13/17 16:34 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/13/17 16:34 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/13/17 16:34 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/13/17 16:34 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 03/13/17 16:34 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 03/13/17 16:34 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 03/13/17 16:34 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 03/13/17 16:34 75-34-31.0 0.32 1
1,2-Dichloroethane 0.29J ug/L 03/13/17 16:34 107-06-2 B1.0 0.24 1
1,1-Dichloroethene ND ug/L 03/13/17 16:34 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/13/17 16:34 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/13/17 16:34 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 03/13/17 16:34 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/13/17 16:34 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 03/13/17 16:34 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 03/13/17 16:34 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 03/13/17 16:34 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 03/13/17 16:34 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 03/13/17 16:34 108-20-31.0 0.12 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/16/2017 04:58 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92333045
South Landfill MW's
Sample:MW-1S Lab ID:92333045001 Collected:03/10/17 13:30 Received:03/10/17 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level
Ethylbenzene ND ug/L 03/13/17 16:34 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 03/13/17 16:34 87-68-31.0 0.71 1
2-Hexanone ND ug/L 03/13/17 16:34 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 03/13/17 16:34 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 03/13/17 16:34 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/13/17 16:34 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 03/13/17 16:34 1634-04-41.0 0.21 1
Naphthalene ND ug/L 03/13/17 16:34 91-20-31.0 0.24 1
Styrene ND ug/L 03/13/17 16:34 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/13/17 16:34 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/13/17 16:34 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 03/13/17 16:34 127-18-41.0 0.46 1
Toluene ND ug/L 03/13/17 16:34 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 03/13/17 16:34 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 03/13/17 16:34 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 03/13/17 16:34 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/13/17 16:34 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/13/17 16:34 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/13/17 16:34 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/13/17 16:34 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/13/17 16:34 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 03/13/17 16:34 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/13/17 16:34 1330-20-71.0 0.66 1
m&p-Xylene ND ug/L 03/13/17 16:34 179601-23-12.0 0.66 1
o-Xylene ND ug/L 03/13/17 16:34 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)100 %03/13/17 16:34 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %03/13/17 16:34 17060-07-070-130 1
Toluene-d8 (S)103 %03/13/17 16:34 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/16/2017 04:58 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92333045
South Landfill MW's
Sample:MW-2S Lab ID:92333045002 Collected:03/10/17 00:00 Received:03/10/17 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Mark
Swann 03/10/17 11:501
Collected Date 3/10/17 03/10/17 11:501
Collected Time 11:50 03/10/17 11:501
Field pH 6.3 Std. Units 03/10/17 11:500.10 0.10 1
Field Temperature 14.5 deg C 03/10/17 11:500.50 0.50 1
Static Water Level 7.00 feet 03/10/17 11:501
Field Specific Conductance 145 umhos/cm 03/10/17 11:501.0 1.0 1
Turbidity 32.59 NTU 03/10/17 11:501.0 1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/16/2017 04:58 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92333045
South Landfill MW's
Sample:MW-3S Lab ID:92333045003 Collected:03/10/17 00:00 Received:03/10/17 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Mark
Swann 03/10/17 11:551
Collected Date 3/10/17 03/10/17 11:551
Collected Time 11:55 03/10/17 11:551
Field pH 5.3 Std. Units 03/10/17 11:550.10 0.10 1
Field Temperature 14.2 deg C 03/10/17 11:550.50 0.50 1
Static Water Level 8.18 feet 03/10/17 11:551
Field Specific Conductance 170 umhos/cm 03/10/17 11:551.0 1.0 1
Turbidity 5.97 NTU 03/10/17 11:551.0 1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/16/2017 04:58 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92333045
South Landfill MW's
Sample:MW-4S Lab ID:92333045004 Collected:03/10/17 14:15 Received:03/10/17 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Mark
Swann 03/10/17 14:151
Collected Date 3/10/17 03/10/17 14:151
Collected Time 14:15 03/10/17 14:151
Field pH 5.6 Std. Units 03/10/17 14:150.10 0.10 1
Field Temperature 12.9 deg C 03/10/17 14:150.50 0.50 1
Static Water Level 6.30 feet 03/10/17 14:151
Field Specific Conductance 192 umhos/cm 03/10/17 14:151.0 1.0 1
Turbidity 11.41 NTU 03/10/17 14:151.0 1.0 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/13/17 17:09 67-64-125.0 10.0 1
Benzene ND ug/L 03/13/17 17:09 71-43-21.0 0.25 1
Bromobenzene ND ug/L 03/13/17 17:09 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 03/13/17 17:09 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 03/13/17 17:09 75-27-41.0 0.18 1
Bromoform ND ug/L 03/13/17 17:09 75-25-21.0 0.26 1
Bromomethane ND ug/L 03/13/17 17:09 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 03/13/17 17:09 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 03/13/17 17:09 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/13/17 17:09 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/13/17 17:09 75-00-31.0 0.54 1
Chloroform ND ug/L 03/13/17 17:09 67-66-31.0 0.14 1
Chloromethane ND ug/L 03/13/17 17:09 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 03/13/17 17:09 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 03/13/17 17:09 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 03/13/17 17:09 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 03/13/17 17:09 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/13/17 17:09 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/13/17 17:09 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/13/17 17:09 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 03/13/17 17:09 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 03/13/17 17:09 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 03/13/17 17:09 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 03/13/17 17:09 75-34-31.0 0.32 1
1,2-Dichloroethane 0.30J ug/L 03/13/17 17:09 107-06-2 B1.0 0.24 1
1,1-Dichloroethene ND ug/L 03/13/17 17:09 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/13/17 17:09 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/13/17 17:09 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 03/13/17 17:09 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/13/17 17:09 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 03/13/17 17:09 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 03/13/17 17:09 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 03/13/17 17:09 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 03/13/17 17:09 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 03/13/17 17:09 108-20-31.0 0.12 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/16/2017 04:58 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92333045
South Landfill MW's
Sample:MW-4S Lab ID:92333045004 Collected:03/10/17 14:15 Received:03/10/17 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level
Ethylbenzene ND ug/L 03/13/17 17:09 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 03/13/17 17:09 87-68-31.0 0.71 1
2-Hexanone ND ug/L 03/13/17 17:09 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 03/13/17 17:09 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 03/13/17 17:09 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/13/17 17:09 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 03/13/17 17:09 1634-04-41.0 0.21 1
Naphthalene ND ug/L 03/13/17 17:09 91-20-31.0 0.24 1
Styrene ND ug/L 03/13/17 17:09 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/13/17 17:09 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/13/17 17:09 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 03/13/17 17:09 127-18-41.0 0.46 1
Toluene ND ug/L 03/13/17 17:09 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 03/13/17 17:09 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 03/13/17 17:09 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 03/13/17 17:09 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/13/17 17:09 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/13/17 17:09 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/13/17 17:09 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/13/17 17:09 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/13/17 17:09 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 03/13/17 17:09 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/13/17 17:09 1330-20-71.0 0.66 1
m&p-Xylene ND ug/L 03/13/17 17:09 179601-23-12.0 0.66 1
o-Xylene ND ug/L 03/13/17 17:09 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)100 %03/13/17 17:09 460-00-470-130 1
1,2-Dichloroethane-d4 (S)93 %03/13/17 17:09 17060-07-070-130 1
Toluene-d8 (S)102 %03/13/17 17:09 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/16/2017 04:58 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 10 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92333045
South Landfill MW's
Sample:MW-5S Lab ID:92333045005 Collected:03/10/17 14:30 Received:03/10/17 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Mark
Swann 03/10/17 14:301
Collected Date 3/10/17 03/10/17 14:301
Collected Time 14:30 03/10/17 14:301
Field pH 5.6 Std. Units 03/10/17 14:300.10 0.10 1
Field Temperature 12.2 deg C 03/10/17 14:300.50 0.50 1
Static Water Level 5.66 feet 03/10/17 14:301
Field Specific Conductance 133 umhos/cm 03/10/17 14:301.0 1.0 1
Turbidity 1.68 NTU 03/10/17 14:301.0 1.0 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/13/17 17:26 67-64-125.0 10.0 1
Benzene ND ug/L 03/13/17 17:26 71-43-21.0 0.25 1
Bromobenzene ND ug/L 03/13/17 17:26 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 03/13/17 17:26 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 03/13/17 17:26 75-27-41.0 0.18 1
Bromoform ND ug/L 03/13/17 17:26 75-25-21.0 0.26 1
Bromomethane ND ug/L 03/13/17 17:26 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 03/13/17 17:26 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 03/13/17 17:26 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/13/17 17:26 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/13/17 17:26 75-00-31.0 0.54 1
Chloroform ND ug/L 03/13/17 17:26 67-66-31.0 0.14 1
Chloromethane ND ug/L 03/13/17 17:26 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 03/13/17 17:26 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 03/13/17 17:26 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 03/13/17 17:26 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 03/13/17 17:26 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/13/17 17:26 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/13/17 17:26 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/13/17 17:26 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 03/13/17 17:26 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 03/13/17 17:26 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 03/13/17 17:26 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 03/13/17 17:26 75-34-31.0 0.32 1
1,2-Dichloroethane 0.39J ug/L 03/13/17 17:26 107-06-2 B1.0 0.24 1
1,1-Dichloroethene ND ug/L 03/13/17 17:26 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/13/17 17:26 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/13/17 17:26 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 03/13/17 17:26 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/13/17 17:26 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 03/13/17 17:26 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 03/13/17 17:26 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 03/13/17 17:26 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 03/13/17 17:26 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 03/13/17 17:26 108-20-31.0 0.12 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/16/2017 04:58 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 11 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92333045
South Landfill MW's
Sample:MW-5S Lab ID:92333045005 Collected:03/10/17 14:30 Received:03/10/17 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level
Ethylbenzene ND ug/L 03/13/17 17:26 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 03/13/17 17:26 87-68-31.0 0.71 1
2-Hexanone ND ug/L 03/13/17 17:26 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 03/13/17 17:26 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 03/13/17 17:26 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/13/17 17:26 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 03/13/17 17:26 1634-04-41.0 0.21 1
Naphthalene ND ug/L 03/13/17 17:26 91-20-31.0 0.24 1
Styrene ND ug/L 03/13/17 17:26 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/13/17 17:26 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/13/17 17:26 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 03/13/17 17:26 127-18-41.0 0.46 1
Toluene ND ug/L 03/13/17 17:26 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 03/13/17 17:26 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 03/13/17 17:26 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 03/13/17 17:26 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/13/17 17:26 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/13/17 17:26 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/13/17 17:26 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/13/17 17:26 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/13/17 17:26 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 03/13/17 17:26 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/13/17 17:26 1330-20-71.0 0.66 1
m&p-Xylene ND ug/L 03/13/17 17:26 179601-23-12.0 0.66 1
o-Xylene ND ug/L 03/13/17 17:26 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)97 %03/13/17 17:26 460-00-470-130 1
1,2-Dichloroethane-d4 (S)91 %03/13/17 17:26 17060-07-070-130 1
Toluene-d8 (S)103 %03/13/17 17:26 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/16/2017 04:58 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 12 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92333045
South Landfill MW's
Sample:MW-6S Lab ID:92333045006 Collected:03/10/17 14:00 Received:03/10/17 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Mark
Swann 03/10/17 14:001
Collected Date 3/10/17 03/10/17 14:001
Collected Time 14:00 03/10/17 14:001
Field pH 6.8 Std. Units 03/10/17 14:000.10 0.10 1
Field Temperature 13.1 deg C 03/10/17 14:000.50 0.50 1
Static Water Level 9.27 feet 03/10/17 14:001
Field Specific Conductance 80 umhos/cm 03/10/17 14:001.0 1.0 1
Turbidity 14.82 NTU 03/10/17 14:001.0 1.0 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/13/17 17:44 67-64-125.0 10.0 1
Benzene ND ug/L 03/13/17 17:44 71-43-21.0 0.25 1
Bromobenzene ND ug/L 03/13/17 17:44 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 03/13/17 17:44 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 03/13/17 17:44 75-27-41.0 0.18 1
Bromoform ND ug/L 03/13/17 17:44 75-25-21.0 0.26 1
Bromomethane ND ug/L 03/13/17 17:44 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 03/13/17 17:44 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 03/13/17 17:44 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/13/17 17:44 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/13/17 17:44 75-00-31.0 0.54 1
Chloroform ND ug/L 03/13/17 17:44 67-66-31.0 0.14 1
Chloromethane 0.14J ug/L 03/13/17 17:44 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 03/13/17 17:44 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 03/13/17 17:44 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 03/13/17 17:44 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 03/13/17 17:44 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/13/17 17:44 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/13/17 17:44 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/13/17 17:44 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 03/13/17 17:44 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 03/13/17 17:44 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 03/13/17 17:44 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 03/13/17 17:44 75-34-31.0 0.32 1
1,2-Dichloroethane 0.29J ug/L 03/13/17 17:44 107-06-2 B1.0 0.24 1
1,1-Dichloroethene ND ug/L 03/13/17 17:44 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/13/17 17:44 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/13/17 17:44 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 03/13/17 17:44 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/13/17 17:44 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 03/13/17 17:44 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 03/13/17 17:44 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 03/13/17 17:44 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 03/13/17 17:44 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 03/13/17 17:44 108-20-31.0 0.12 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/16/2017 04:58 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 13 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92333045
South Landfill MW's
Sample:MW-6S Lab ID:92333045006 Collected:03/10/17 14:00 Received:03/10/17 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level
Ethylbenzene ND ug/L 03/13/17 17:44 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 03/13/17 17:44 87-68-31.0 0.71 1
2-Hexanone ND ug/L 03/13/17 17:44 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 03/13/17 17:44 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 03/13/17 17:44 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/13/17 17:44 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 03/13/17 17:44 1634-04-41.0 0.21 1
Naphthalene ND ug/L 03/13/17 17:44 91-20-31.0 0.24 1
Styrene ND ug/L 03/13/17 17:44 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/13/17 17:44 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/13/17 17:44 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 03/13/17 17:44 127-18-41.0 0.46 1
Toluene ND ug/L 03/13/17 17:44 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 03/13/17 17:44 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 03/13/17 17:44 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 03/13/17 17:44 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/13/17 17:44 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/13/17 17:44 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/13/17 17:44 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/13/17 17:44 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/13/17 17:44 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 03/13/17 17:44 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/13/17 17:44 1330-20-71.0 0.66 1
m&p-Xylene ND ug/L 03/13/17 17:44 179601-23-12.0 0.66 1
o-Xylene ND ug/L 03/13/17 17:44 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)98 %03/13/17 17:44 460-00-470-130 1
1,2-Dichloroethane-d4 (S)91 %03/13/17 17:44 17060-07-070-130 1
Toluene-d8 (S)101 %03/13/17 17:44 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/16/2017 04:58 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 14 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92333045
South Landfill MW's
Sample:MW-7S Lab ID:92333045007 Collected:03/10/17 13:50 Received:03/10/17 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Mark
Swann 03/10/17 13:501
Collected Date 3/10/17 03/10/17 13:501
Collected Time 13:50 03/10/17 13:501
Field pH 6.2 Std. Units 03/10/17 13:500.10 0.10 1
Field Temperature 12.8 deg C 03/10/17 13:500.50 0.50 1
Static Water Level 6.49 feet 03/10/17 13:501
Field Specific Conductance 155 umhos/cm 03/10/17 13:501.0 1.0 1
Turbidity 7.05 NTU 03/10/17 13:501.0 1.0 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/13/17 18:01 67-64-125.0 10.0 1
Benzene ND ug/L 03/13/17 18:01 71-43-21.0 0.25 1
Bromobenzene ND ug/L 03/13/17 18:01 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 03/13/17 18:01 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 03/13/17 18:01 75-27-41.0 0.18 1
Bromoform ND ug/L 03/13/17 18:01 75-25-21.0 0.26 1
Bromomethane ND ug/L 03/13/17 18:01 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 03/13/17 18:01 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 03/13/17 18:01 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/13/17 18:01 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/13/17 18:01 75-00-31.0 0.54 1
Chloroform ND ug/L 03/13/17 18:01 67-66-31.0 0.14 1
Chloromethane ND ug/L 03/13/17 18:01 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 03/13/17 18:01 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 03/13/17 18:01 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 03/13/17 18:01 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 03/13/17 18:01 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/13/17 18:01 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/13/17 18:01 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/13/17 18:01 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 03/13/17 18:01 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 03/13/17 18:01 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 03/13/17 18:01 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 03/13/17 18:01 75-34-31.0 0.32 1
1,2-Dichloroethane 0.30J ug/L 03/13/17 18:01 107-06-2 B1.0 0.24 1
1,1-Dichloroethene ND ug/L 03/13/17 18:01 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/13/17 18:01 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/13/17 18:01 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 03/13/17 18:01 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/13/17 18:01 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 03/13/17 18:01 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 03/13/17 18:01 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 03/13/17 18:01 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 03/13/17 18:01 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 03/13/17 18:01 108-20-31.0 0.12 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/16/2017 04:58 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 15 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92333045
South Landfill MW's
Sample:MW-7S Lab ID:92333045007 Collected:03/10/17 13:50 Received:03/10/17 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level
Ethylbenzene ND ug/L 03/13/17 18:01 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 03/13/17 18:01 87-68-31.0 0.71 1
2-Hexanone ND ug/L 03/13/17 18:01 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 03/13/17 18:01 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 03/13/17 18:01 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/13/17 18:01 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 03/13/17 18:01 1634-04-41.0 0.21 1
Naphthalene ND ug/L 03/13/17 18:01 91-20-31.0 0.24 1
Styrene ND ug/L 03/13/17 18:01 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/13/17 18:01 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/13/17 18:01 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 03/13/17 18:01 127-18-41.0 0.46 1
Toluene ND ug/L 03/13/17 18:01 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 03/13/17 18:01 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 03/13/17 18:01 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 03/13/17 18:01 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/13/17 18:01 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/13/17 18:01 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/13/17 18:01 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/13/17 18:01 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/13/17 18:01 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 03/13/17 18:01 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/13/17 18:01 1330-20-71.0 0.66 1
m&p-Xylene ND ug/L 03/13/17 18:01 179601-23-12.0 0.66 1
o-Xylene ND ug/L 03/13/17 18:01 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)97 %03/13/17 18:01 460-00-470-130 1
1,2-Dichloroethane-d4 (S)91 %03/13/17 18:01 17060-07-070-130 1
Toluene-d8 (S)102 %03/13/17 18:01 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/16/2017 04:58 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 16 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92333045
South Landfill MW's
Sample:TVL BLK Lab ID:92333045008 Collected:03/10/17 09:00 Received:03/10/17 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/13/17 15:42 67-64-125.0 10.0 1
Benzene ND ug/L 03/13/17 15:42 71-43-21.0 0.25 1
Bromobenzene ND ug/L 03/13/17 15:42 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 03/13/17 15:42 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 03/13/17 15:42 75-27-41.0 0.18 1
Bromoform ND ug/L 03/13/17 15:42 75-25-21.0 0.26 1
Bromomethane ND ug/L 03/13/17 15:42 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 03/13/17 15:42 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 03/13/17 15:42 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/13/17 15:42 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/13/17 15:42 75-00-31.0 0.54 1
Chloroform ND ug/L 03/13/17 15:42 67-66-31.0 0.14 1
Chloromethane ND ug/L 03/13/17 15:42 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 03/13/17 15:42 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 03/13/17 15:42 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 03/13/17 15:42 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 03/13/17 15:42 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/13/17 15:42 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/13/17 15:42 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/13/17 15:42 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 03/13/17 15:42 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 03/13/17 15:42 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 03/13/17 15:42 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 03/13/17 15:42 75-34-31.0 0.32 1
1,2-Dichloroethane 0.28J ug/L 03/13/17 15:42 107-06-2 B1.0 0.24 1
1,1-Dichloroethene ND ug/L 03/13/17 15:42 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/13/17 15:42 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/13/17 15:42 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 03/13/17 15:42 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/13/17 15:42 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 03/13/17 15:42 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 03/13/17 15:42 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 03/13/17 15:42 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 03/13/17 15:42 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 03/13/17 15:42 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 03/13/17 15:42 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 03/13/17 15:42 87-68-31.0 0.71 1
2-Hexanone ND ug/L 03/13/17 15:42 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 03/13/17 15:42 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 03/13/17 15:42 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/13/17 15:42 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 03/13/17 15:42 1634-04-41.0 0.21 1
Naphthalene ND ug/L 03/13/17 15:42 91-20-31.0 0.24 1
Styrene ND ug/L 03/13/17 15:42 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/13/17 15:42 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/13/17 15:42 79-34-51.0 0.40 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/16/2017 04:58 PM
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Asheville, NC 28804
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Page 17 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92333045
South Landfill MW's
Sample:TVL BLK Lab ID:92333045008 Collected:03/10/17 09:00 Received:03/10/17 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level
Tetrachloroethene ND ug/L 03/13/17 15:42 127-18-41.0 0.46 1
Toluene ND ug/L 03/13/17 15:42 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 03/13/17 15:42 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 03/13/17 15:42 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 03/13/17 15:42 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/13/17 15:42 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/13/17 15:42 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/13/17 15:42 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/13/17 15:42 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/13/17 15:42 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 03/13/17 15:42 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/13/17 15:42 1330-20-71.0 0.66 1
m&p-Xylene ND ug/L 03/13/17 15:42 179601-23-12.0 0.66 1
o-Xylene ND ug/L 03/13/17 15:42 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)100 %03/13/17 15:42 460-00-470-130 1
1,2-Dichloroethane-d4 (S)93 %03/13/17 15:42 17060-07-070-130 1
Toluene-d8 (S)101 %03/13/17 15:42 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/16/2017 04:58 PM
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Page 18 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92333045
South Landfill MW's
Sample:EQ BLANK Lab ID:92333045009 Collected:03/10/17 09:05 Received:03/10/17 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/13/17 15:25 67-64-125.0 10.0 1
Benzene ND ug/L 03/13/17 15:25 71-43-21.0 0.25 1
Bromobenzene ND ug/L 03/13/17 15:25 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 03/13/17 15:25 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 03/13/17 15:25 75-27-41.0 0.18 1
Bromoform ND ug/L 03/13/17 15:25 75-25-21.0 0.26 1
Bromomethane ND ug/L 03/13/17 15:25 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 03/13/17 15:25 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 03/13/17 15:25 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/13/17 15:25 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/13/17 15:25 75-00-31.0 0.54 1
Chloroform ND ug/L 03/13/17 15:25 67-66-31.0 0.14 1
Chloromethane ND ug/L 03/13/17 15:25 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 03/13/17 15:25 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 03/13/17 15:25 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 03/13/17 15:25 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 03/13/17 15:25 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/13/17 15:25 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/13/17 15:25 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/13/17 15:25 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 03/13/17 15:25 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 03/13/17 15:25 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 03/13/17 15:25 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 03/13/17 15:25 75-34-31.0 0.32 1
1,2-Dichloroethane 0.34J ug/L 03/13/17 15:25 107-06-2 B1.0 0.24 1
1,1-Dichloroethene ND ug/L 03/13/17 15:25 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/13/17 15:25 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/13/17 15:25 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 03/13/17 15:25 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/13/17 15:25 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 03/13/17 15:25 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 03/13/17 15:25 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 03/13/17 15:25 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 03/13/17 15:25 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 03/13/17 15:25 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 03/13/17 15:25 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 03/13/17 15:25 87-68-31.0 0.71 1
2-Hexanone ND ug/L 03/13/17 15:25 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 03/13/17 15:25 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 03/13/17 15:25 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/13/17 15:25 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 03/13/17 15:25 1634-04-41.0 0.21 1
Naphthalene ND ug/L 03/13/17 15:25 91-20-31.0 0.24 1
Styrene ND ug/L 03/13/17 15:25 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/13/17 15:25 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/13/17 15:25 79-34-51.0 0.40 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/16/2017 04:58 PM
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Page 19 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92333045
South Landfill MW's
Sample:EQ BLANK Lab ID:92333045009 Collected:03/10/17 09:05 Received:03/10/17 15:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level
Tetrachloroethene ND ug/L 03/13/17 15:25 127-18-41.0 0.46 1
Toluene ND ug/L 03/13/17 15:25 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 03/13/17 15:25 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 03/13/17 15:25 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 03/13/17 15:25 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/13/17 15:25 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/13/17 15:25 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/13/17 15:25 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/13/17 15:25 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/13/17 15:25 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 03/13/17 15:25 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/13/17 15:25 1330-20-71.0 0.66 1
m&p-Xylene ND ug/L 03/13/17 15:25 179601-23-12.0 0.66 1
o-Xylene ND ug/L 03/13/17 15:25 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)102 %03/13/17 15:25 460-00-470-130 1
1,2-Dichloroethane-d4 (S)93 %03/13/17 15:25 17060-07-070-130 1
Toluene-d8 (S)103 %03/13/17 15:25 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/16/2017 04:58 PM
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[phone]
Page 20 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92333045
South Landfill MW's
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
351919
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:92333045001, 92333045004, 92333045005, 92333045006, 92333045007, 92333045008, 92333045009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1952224
Associated Lab Samples:92333045001, 92333045004, 92333045005, 92333045006, 92333045007, 92333045008, 92333045009
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 03/13/17 14:500.33
1,1,1-Trichloroethane ug/L ND 1.0 03/13/17 14:500.48
1,1,2,2-Tetrachloroethane ug/L ND 1.0 03/13/17 14:500.40
1,1,2-Trichloroethane ug/L ND 1.0 03/13/17 14:500.29
1,1-Dichloroethane ug/L ND 1.0 03/13/17 14:500.32
1,1-Dichloroethene ug/L ND 1.0 03/13/17 14:500.56
1,1-Dichloropropene ug/L ND 1.0 03/13/17 14:500.49
1,2,3-Trichlorobenzene ug/L ND 1.0 03/13/17 14:500.33
1,2,3-Trichloropropane ug/L ND 1.0 03/13/17 14:500.41
1,2,4-Trichlorobenzene ug/L ND 1.0 03/13/17 14:500.35
1,2-Dibromo-3-chloropropane ug/L ND 2.0 03/13/17 14:502.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 03/13/17 14:500.27
1,2-Dichlorobenzene ug/L ND 1.0 03/13/17 14:500.30
1,2-Dichloroethane ug/L ND 1.0 03/13/17 14:500.24
1,2-Dichloropropane ug/L ND 1.0 03/13/17 14:500.27
1,3-Dichlorobenzene ug/L ND 1.0 03/13/17 14:500.24
1,3-Dichloropropane ug/L ND 1.0 03/13/17 14:500.28
1,4-Dichlorobenzene ug/L ND 1.0 03/13/17 14:500.33
2,2-Dichloropropane ug/L ND 1.0 03/13/17 14:500.13
2-Butanone (MEK)ug/L ND 5.0 03/13/17 14:500.96
2-Chlorotoluene ug/L ND 1.0 03/13/17 14:500.35
2-Hexanone ug/L ND 5.0 03/13/17 14:500.46
4-Chlorotoluene ug/L ND 1.0 03/13/17 14:500.31
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 03/13/17 14:500.33
Acetone ug/L ND 25.0 03/13/17 14:5010.0
Benzene ug/L ND 1.0 03/13/17 14:500.25
Bromobenzene ug/L ND 1.0 03/13/17 14:500.30
Bromochloromethane ug/L ND 1.0 03/13/17 14:500.17
Bromodichloromethane ug/L ND 1.0 03/13/17 14:500.18
Bromoform ug/L ND 1.0 03/13/17 14:500.26
Bromomethane ug/L ND 2.0 03/13/17 14:500.29
Carbon tetrachloride ug/L ND 1.0 03/13/17 14:500.25
Chlorobenzene ug/L ND 1.0 03/13/17 14:500.23
Chloroethane ug/L ND 1.0 03/13/17 14:500.54
Chloroform ug/L ND 1.0 03/13/17 14:500.14
Chloromethane ug/L ND 1.0 03/13/17 14:500.11
cis-1,2-Dichloroethene ug/L ND 1.0 03/13/17 14:500.19
cis-1,3-Dichloropropene ug/L ND 1.0 03/13/17 14:500.13
Dibromochloromethane ug/L ND 1.0 03/13/17 14:500.21
Dibromomethane ug/L ND 1.0 03/13/17 14:500.21
Dichlorodifluoromethane ug/L ND 1.0 03/13/17 14:500.21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/16/2017 04:58 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 21 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92333045
South Landfill MW's
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1952224
Associated Lab Samples:92333045001, 92333045004, 92333045005, 92333045006, 92333045007, 92333045008, 92333045009
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L ND 1.0 03/13/17 14:500.12
Ethylbenzene ug/L ND 1.0 03/13/17 14:500.30
Hexachloro-1,3-butadiene ug/L ND 1.0 03/13/17 14:500.71
m&p-Xylene ug/L ND 2.0 03/13/17 14:500.66
Methyl-tert-butyl ether ug/L ND 1.0 03/13/17 14:500.21
Methylene Chloride ug/L ND 2.0 03/13/17 14:500.97
Naphthalene ug/L ND 1.0 03/13/17 14:500.24
o-Xylene ug/L ND 1.0 03/13/17 14:500.23
p-Isopropyltoluene ug/L ND 1.0 03/13/17 14:500.31
Styrene ug/L ND 1.0 03/13/17 14:500.26
Tetrachloroethene ug/L ND 1.0 03/13/17 14:500.46
Toluene ug/L ND 1.0 03/13/17 14:500.26
trans-1,2-Dichloroethene ug/L ND 1.0 03/13/17 14:500.49
trans-1,3-Dichloropropene ug/L ND 1.0 03/13/17 14:500.26
Trichloroethene ug/L ND 1.0 03/13/17 14:500.47
Trichlorofluoromethane ug/L ND 1.0 03/13/17 14:500.20
Vinyl acetate ug/L ND 2.0 03/13/17 14:500.35
Vinyl chloride ug/L ND 1.0 03/13/17 14:500.62
Xylene (Total)ug/L ND 1.0 03/13/17 14:500.66
1,2-Dichloroethane-d4 (S)%93 70-130 03/13/17 14:50
4-Bromofluorobenzene (S)%99 70-130 03/13/17 14:50
Toluene-d8 (S)%101 70-130 03/13/17 14:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1952225LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.150 98 70-130
1,1,1-Trichloroethane ug/L 52.850 106 70-130
1,1,2,2-Tetrachloroethane ug/L 52.650 105 70-130
1,1,2-Trichloroethane ug/L 53.050 106 70-130
1,1-Dichloroethane ug/L 51.750 103 70-130
1,1-Dichloroethene ug/L 55.650 111 70-132
1,1-Dichloropropene ug/L 55.250 110 70-130
1,2,3-Trichlorobenzene ug/L 51.450 103 70-135
1,2,3-Trichloropropane ug/L 51.650 103 70-130
1,2,4-Trichlorobenzene ug/L 52.250 104 70-134
1,2-Dibromo-3-chloropropane ug/L 50.350 101 70-130
1,2-Dibromoethane (EDB)ug/L 53.450 107 70-130
1,2-Dichlorobenzene ug/L 53.550 107 70-130
1,2-Dichloroethane ug/L 48.350 97 70-130
1,2-Dichloropropane ug/L 53.450 107 70-130
1,3-Dichlorobenzene ug/L 52.050 104 70-130
1,3-Dichloropropane ug/L 54.750 109 70-130
1,4-Dichlorobenzene ug/L 50.950 102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/16/2017 04:58 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 22 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92333045
South Landfill MW's
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1952225LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 53.350 107 58-145
2-Butanone (MEK)ug/L 96.0100 96 70-145
2-Chlorotoluene ug/L 53.550 107 70-130
2-Hexanone ug/L 102100 102 70-144
4-Chlorotoluene ug/L 53.250 106 70-130
4-Methyl-2-pentanone (MIBK)ug/L 99.5100 99 70-140
Acetone ug/L 96.3100 96 50-175
Benzene ug/L 54.750 109 70-130
Bromobenzene ug/L 52.850 106 70-130
Bromochloromethane ug/L 52.050 104 70-130
Bromodichloromethane ug/L 55.850 112 70-130
Bromoform ug/L 46.250 92 70-130
Bromomethane ug/L 56.750 113 54-130
Carbon tetrachloride ug/L 53.950 108 70-132
Chlorobenzene ug/L 53.850 108 70-130
Chloroethane ug/L 49.450 99 64-134
Chloroform ug/L 50.750 101 70-130
Chloromethane ug/L 50.950 102 64-130
cis-1,2-Dichloroethene ug/L 52.050 104 70-131
cis-1,3-Dichloropropene ug/L 54.850 110 70-130
Dibromochloromethane ug/L 48.250 96 70-130
Dibromomethane ug/L 50.750 101 70-131
Dichlorodifluoromethane ug/L 40.650 81 56-130
Diisopropyl ether ug/L 52.350 105 70-130
Ethylbenzene ug/L 52.850 106 70-130
Hexachloro-1,3-butadiene ug/L 51.750 103 70-130
m&p-Xylene ug/L 105100 105 70-130
Methyl-tert-butyl ether ug/L 54.550 109 70-130
Methylene Chloride ug/L 50.350 101 63-130
Naphthalene ug/L 51.750 103 70-138
o-Xylene ug/L 52.550 105 70-130
p-Isopropyltoluene ug/L 51.950 104 70-130
Styrene ug/L 53.950 108 70-130
Tetrachloroethene ug/L 52.050 104 70-130
Toluene ug/L 52.250 104 70-130
trans-1,2-Dichloroethene ug/L 52.150 104 70-130
trans-1,3-Dichloropropene ug/L 54.550 109 70-132
Trichloroethene ug/L 52.950 106 70-130
Trichlorofluoromethane ug/L 51.850 104 62-133
Vinyl acetate ug/L 111100 111 66-157
Vinyl chloride ug/L 43.550 87 50-150
Xylene (Total)ug/L 158150 105 70-130
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/16/2017 04:58 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 23 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92333045
South Landfill MW's
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1952226MATRIX SPIKE SAMPLE:
MSSpike
Result
92333002004
1,1,1,2-Tetrachloroethane ug/L 19.720 98 70-130ND
1,1,1-Trichloroethane ug/L 22.120 111 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.920 104 70-130ND
1,1,2-Trichloroethane ug/L 21.020 105 70-130ND
1,1-Dichloroethane ug/L 21.320 107 70-130ND
1,1-Dichloroethene ug/L 23.720 119 70-166ND
1,1-Dichloropropene ug/L 23.420 117 70-130ND
1,2,3-Trichlorobenzene ug/L 21.520 108 70-130ND
1,2,3-Trichloropropane ug/L 21.220 106 70-130ND
1,2,4-Trichlorobenzene ug/L 20.720 104 70-130ND
1,2-Dibromo-3-chloropropane ug/L 20.320 102 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.420 107 70-130ND
1,2-Dichlorobenzene ug/L 21.820 109 70-130ND
1,2-Dichloroethane ug/L 19.520 96 70-130ND
1,2-Dichloropropane ug/L 22.420 112 70-130ND
1,3-Dichlorobenzene ug/L 21.720 108 70-130ND
1,3-Dichloropropane ug/L 21.920 110 70-130ND
1,4-Dichlorobenzene ug/L 21.720 109 70-130ND
2,2-Dichloropropane ug/L 20.220 101 70-130ND
2-Butanone (MEK)ug/L 43.040 107 70-130ND
2-Chlorotoluene ug/L 22.820 114 70-130ND
2-Hexanone ug/L 44.240 111 70-130ND
4-Chlorotoluene ug/L 22.420 112 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 43.740 109 70-130ND
Acetone ug/L 42.340 92 70-130ND
Benzene ug/L 23.120 115 70-148ND
Bromobenzene ug/L 21.920 110 70-130ND
Bromochloromethane ug/L 20.520 103 70-130ND
Bromodichloromethane ug/L 22.520 113 70-130ND
Bromoform ug/L 18.320 91 70-130ND
Bromomethane ug/L 20.120 101 70-130ND
Carbon tetrachloride ug/L 22.920 115 70-130ND
Chlorobenzene ug/L 22.720 114 70-146ND
Chloroethane ug/L 20.720 104 70-130ND
Chloroform ug/L 21.220 106 70-130ND
Chloromethane ug/L 21.420 103 70-130ND
cis-1,2-Dichloroethene ug/L 20.720 104 70-130ND
cis-1,3-Dichloropropene ug/L 21.320 107 70-130ND
Dibromochloromethane ug/L 19.520 97 70-130ND
Dibromomethane ug/L 21.320 107 70-130ND
Dichlorodifluoromethane ug/L 18.220 91 70-130ND
Diisopropyl ether ug/L 20.720 104 70-130ND
Ethylbenzene ug/L 22.620 113 70-130ND
Hexachloro-1,3-butadiene ug/L 20.920 105 70-130ND
m&p-Xylene ug/L 44.940 112 70-130ND
Methyl-tert-butyl ether ug/L 20.620 103 70-130ND
Methylene Chloride ug/L 20.020 100 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/16/2017 04:58 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 24 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92333045
South Landfill MW's
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1952226MATRIX SPIKE SAMPLE:
MSSpike
Result
92333002004
Naphthalene ug/L 21.720 108 70-130ND
o-Xylene ug/L 21.820 109 70-130ND
p-Isopropyltoluene ug/L 21.320 106 70-130ND
Styrene ug/L 22.120 110 70-130ND
Tetrachloroethene ug/L 22.120 110 70-130ND
Toluene ug/L 22.620 113 70-155ND
trans-1,2-Dichloroethene ug/L 22.520 113 70-130ND
trans-1,3-Dichloropropene ug/L 20.620 103 70-130ND
Trichloroethene ug/L 22.920 115 69-151ND
Trichlorofluoromethane ug/L 24.020 120 70-130ND
Vinyl acetate ug/L 38.040 95 70-130ND
Vinyl chloride ug/L 17.920 89 70-130ND
1,2-Dichloroethane-d4 (S)%92 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92333045001
1952227SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L 0.35J 300.29J
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Chlorotoluene ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Chlorotoluene ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Benzene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/16/2017 04:58 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 25 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92333045
South Landfill MW's
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92333045001
1952227SAMPLE DUPLICATE:
Bromobenzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 300.11J
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Diisopropyl ether ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
o-Xylene ug/L ND 30ND
p-Isopropyltoluene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%93 192
4-Bromofluorobenzene (S)%99 1100
Toluene-d8 (S)%102 0103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/16/2017 04:58 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 26 of 31
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92333045
South Landfill MW's
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/16/2017 04:58 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 27 of 31
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92333045
South Landfill MW's
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92333045001 MW-1S
92333045002 MW-2S
92333045003 MW-3S
92333045004 MW-4S
92333045005 MW-5S
92333045006 MW-6S
92333045007 MW-7S
92333045001 351919MW-1S EPA 8260
92333045004 351919MW-4S EPA 8260
92333045005 351919MW-5S EPA 8260
92333045006 351919MW-6S EPA 8260
92333045007 351919MW-7S EPA 8260
92333045008 351919TVL BLK EPA 8260
92333045009 351919EQ BLANK EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/16/2017 04:58 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 28 of 31
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