5301_LeeCountyMSWLF_GWMR_20171201

TERRAQUEST ENVIRONMENTAL CONSULTANTS, P.C. 
100 E. RUFFIN ST., MEBANE, NC 27302 
(919)‐563‐9091 PHONE 
(919)‐563‐9095 FAX 

November 30, 2017 

Jaclynne Drummond 
Compliance Hydrogeologist 
NCDEQ, Division of Waste Management  
Solid Waste Section, Asheville Regional Office 
2090 US Highway 70, Swannanoa, NC 28778 

Re: Semi‐Annual Groundwater Monitoring Event (October 2017) 
 Lee County Landfill ‐ Sanford, NC 
 NCDWM – Solid Waste Section Permit # 53‐01 
 Terraquest Project No. 02296 

Dear Ms. Drummond: 

On behalf of the Lee County Department of Public Works, Terraquest Environmental 
Consultants, P.C. is reporting the results of a biannual ground and surface water sampling event 
that took pace at the Lee County Landfill in Sanford, NC on October 17, 2017.  In accordance 
with NCDWM‐SW’s reporting requirements, a Solid Waste Section Environmental Monitoring 
Reporting Form is attached.  The data from the event including analytical results, groundwater 
elevations, and field measured groundwater parameter data is summarized on the attached 
Table 1.  The location of the site is shown of Figure 1, the vicinity of the site on Figure 2, and 
site’s layout on Figure 3.  Figure 4 presents the recent potentiometric surface.  The full 
analytical report is also attached.  The following summarizes the event: 

On October 17, 2017, Terraquest personnel sampled monitoring wells MW5, MW6, MW9, 
MW12, MW13, and MW14.  Monitoring well MW4 was dry and could not be sampled as was 
the surface water location.  All water samples were analyzed per SW‐846 8260B (VOCs) and 
SW‐846 7470A (mercury) and 6010C (RCRA Metals).  All water samples were collected following 
technical methods and standard procedures as outlined on the enclosed sheets.  Terraquest 
personnel also collected dissolved oxygen, pH, temperature, and conductivity measurements 
from each of the sampled monitoring wells following purging of the well.  These measurements 
are listed on the attached Table.   

The analytical results revealed detectable concentrations of petroleum‐type compounds in 
monitoring well MW12 only.  Benzene, 1,2‐dichloroethane, and 1,4‐dichlorobenzene were 
reported at concentrations in excess of the standard set forth under Title 15A of the North 
Carolina Administrative Code Subchapter 2L .0202(g).  Results of the RCRA Metals analysis 

TERRAQUEST ENVIRONMENTAL CONSULTANTS, P.C. 
100 E. RUFFIN ST., MEBANE, NC 27302 
(919)‐563‐9091 PHONE 
(919)‐563‐9095 FAX 
indicate that all of the monitoring wells had a detection of at least one metal.  The analytical 
results are summarized in the attached table.   

A potentiometric surface map (Figure 4) depicting an interpreted groundwater flow direction at 
the site as measured on October 17, 2017 is attached.  Based upon the water levels in 
monitoring wells, the groundwater flow direction is to the southeast toward Mare Brand Creek.  
This flow direction conforms with historical flow directions.  The attached table  lists the 
groundwater elevations for the monitoring wells. 

If you have any questions regarding the sampling event or analytical report, please contact 
Ryan Kerins at (919)‐563‐9091 or Mr. Joseph Cherry of the Lee County Public Works 
Department at (919)‐774‐8440.  Thank you. 

Sincerely, 

TERRAQUEST ENVIRONMENTAL CONSULTANTS, P.C. 

Ryan D. Kerins         Michael J. Brown P.G.    
Project Manager       President 

Analytical Report
L7J0207
Project
Lee County Landfill
Project Number
02296
October 30, 2017
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Mebane, NC 27302
Minority Women Business Enterprise
Small Disadvantaged Business Enterprise
Page 1 of 30
1412 Tech Blvd Phone #:[phone]
Website:www.ftsanalytical.comTampa, FL 33619
Minority Women Business Enterprise
Small Disadvantaged Business Enterprise
October 30, 2017
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Ryan Kerins
RE: Lee County Landfill
We are reporting the results of the analyses performed on the samples recieved on 10/19/2017 under the
project name referenced above and identified as the lab Work Order L7J0207. All results being reported
under this Report apply to the samples analyzed and properly identified with a Laboratory ID number.
Subcontracted analyses are identified in this report with either the NELAC certification number of the
subcontracted lab, or the complete subcontracted report attached to this report.
Unless otherwise noted in a Case Narrative, all data reported in this Analytical Report are in compliance with
NELAC standards. The uncertainty of measurement associated with the results of analysis reported is
available upon request. Should insufficient sample be provided to the laboratory to meet the method and
NELAC Matrix Duplicate and Matrix Spike requirements, then the data will be analyzed, evaluated and
reporting using all other available quality control methods.
The validity and integrity of this report will remain intact as long as it is accompanied by this letter and
reproduced in full, unless written approval is granted by FTS Analytical Laboratories. This report will be filed
for at least 5 years in our archives after which time it will be destroyed without further notice, unless
otherwise agreed upon. The samples received, and described as recorded in Work Order L7J0207 will be
filed for 60 days, and after that time they will be properly disposed without further notice, unless otherwise
agreed upon. We reserve the right to return to you any unused samples, extracts, or solutions if we
consider so necessary (e.g., samples identified as hazardous waste, sample sizes exceeding standard
practices, controlled/regulated substances, etc.)
We thank you for selecting FTS Analytical to serve your analytical needs. If you have any questions
concerning this report, please do not hesitate to contact us at any time. We will be happy to help.
Mebane, NC 27302
Sincerely,
Chad Bechtold
VP of Client Services
Page 2 of 30
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 10/30/17 14:39
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Samples in this Report
Sample Lab ID Matrix Date Sampled Date Received
MW5 WaterL7J0207-01 19-Oct-2017 09:3917-Oct-2017 12:45
MW6 WaterL7J0207-02 19-Oct-2017 09:3917-Oct-2017 11:35
MW9 WaterL7J0207-03 19-Oct-2017 09:3917-Oct-2017 11:25
MW12 WaterL7J0207-04 19-Oct-2017 09:3917-Oct-2017 12:30
MW13 WaterL7J0207-05 19-Oct-2017 09:3917-Oct-2017 11:10
MW14 WaterL7J0207-06 19-Oct-2017 09:3917-Oct-2017 11:00
TRIP BLANK WaterL7J0207-07 19-Oct-2017 09:3917-Oct-2017 00:00
Page 3 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 3 of 30
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 10/30/17 14:39
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Analysis Case Narrative

Method 7470A
Batch B7J0305
The batch non-client Matrix Spike (MS) and Matrix Spike Duplicate (MSD) recoveries for Mercury were not reported due to
matrix interference. However, the Laboratory Control Sample (LCS) and Laboratory Control Sample Duplicate (LCSD)
recoveries met acceptance criteria.
Page 4 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 4 of 30
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 10/30/17 14:39
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Hits Summary
Sample: MW5
MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte
Lab ID: L7J0207-01
0.0100 mg/L0.00400 10.0335 10/24/17 12:30 7440-38-2 EPA 6010CArsenic
0.0500 mg/L0.00200 10.809 10/24/17 12:30 7440-39-3 EPA 6010CBarium
0.00500 mg/L0.000300 1J0.00421 10/24/17 12:30 7440-43-9 EPA 6010CCadmium
0.0100 mg/L0.000300 10.0317 10/24/17 12:30 7440-47-3 EPA 6010CChromium
0.0100 mg/L0.00330 10.0897 10/24/17 12:30 7439-92-1 EPA 6010CLead
Sample: MW6
MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte
Lab ID: L7J0207-02
0.0100 mg/L0.00400 1J0.00412 10/24/17 12:37 7440-38-2 EPA 6010CArsenic
0.0500 mg/L0.00200 1J0.0397 10/24/17 12:37 7440-39-3 EPA 6010CBarium
Sample: MW9
MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte
Lab ID: L7J0207-03
0.0500 mg/L0.00200 10.195 10/24/17 12:45 7440-39-3 EPA 6010CBarium
0.0100 mg/L0.000300 1J0.00886 10/24/17 12:45 7440-47-3 EPA 6010CChromium
0.0100 mg/L0.00330 10.0156 10/24/17 12:45 7439-92-1 EPA 6010CLead
Sample: MW12
MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte
Lab ID: L7J0207-04
0.0100 mg/L0.00400 10.0106 10/24/17 12:47 7440-38-2 EPA 6010CArsenic
0.0500 mg/L0.00200 11.54 10/24/17 12:47 7440-39-3 EPA 6010CBarium
1.00 ug/L0.110 14.38 10/20/17 15:50 75-34-3 EPA 8260B APP I1,1-Dichloroethane
0.00500 mg/L0.000300 1J0.00368 10/24/17 12:47 7440-43-9 EPA 6010CCadmium
0.0100 mg/L0.000300 1J0.00700 10/24/17 12:47 7440-47-3 EPA 6010CChromium
1.00 ug/L0.140 1J0.430 10/20/17 15:50 95-50-1 EPA 8260B APP I1,2-Dichlorobenzene
0.0100 mg/L0.00330 10.0396 10/24/17 12:47 7439-92-1 EPA 6010CLead
1.00 ug/L0.170 13.55 10/20/17 15:50 106-46-7 EPA 8260B APP I1,4-Dichlorobenzene
1.00 ug/L0.160 13.45 10/20/17 15:50 71-43-2 EPA 8260B APP IBenzene
1.00 ug/L0.150 112.8 10/20/17 15:50 108-90-7 EPA 8260B APP IChlorobenzene
1.00 ug/L0.260 134.3 10/20/17 15:50 75-00-3 EPA 8260B APP IChloroethane
1.00 ug/L0.140 1J0.460 10/20/17 15:50 108-88-3 EPA 8260B APP IToluene
1.00 ug/L0.200 1J0.420 10/20/17 15:50 1330-20-7 EPA 8260B APP ITotal Xylenes
Page 5 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 5 of 30
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 10/30/17 14:39
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Hits Summary
(Continued)
Sample: MW13
MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte
Lab ID: L7J0207-05
0.0100 mg/L0.00400 10.0226 10/24/17 12:49 7440-38-2 EPA 6010CArsenic
0.0500 mg/L0.00200 10.530 10/24/17 12:49 7440-39-3 EPA 6010CBarium
0.00500 mg/L0.000300 1J0.00207 10/24/17 12:49 7440-43-9 EPA 6010CCadmium
0.0100 mg/L0.000300 10.0184 10/24/17 12:49 7440-47-3 EPA 6010CChromium
0.0100 mg/L0.00330 10.0578 10/24/17 12:49 7439-92-1 EPA 6010CLead
Sample: MW14
MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte
Lab ID: L7J0207-06
0.0100 mg/L0.00400 1J0.00788 10/24/17 12:51 7440-38-2 EPA 6010CArsenic
0.0500 mg/L0.00200 10.353 10/24/17 12:51 7440-39-3 EPA 6010CBarium
0.00500 mg/L0.000300 1J0.00200 10/24/17 12:51 7440-43-9 EPA 6010CCadmium
0.0100 mg/L0.000300 10.0342 10/24/17 12:51 7440-47-3 EPA 6010CChromium
0.0100 mg/L0.00330 10.710 10/24/17 12:51 7439-92-1 EPA 6010CLead
Sample: TRIP BLANK
MethodCAS #Date AnalyzedDilUnitsMDLResultRLQual Analyte
Lab ID: L7J0207-07
1.00 ug/L0.140 1J0.520 10/20/17 14:20 108-88-3 EPA 8260B APP IToluene
1.00 ug/L0.200 1J0.460 10/20/17 14:20 1330-20-7 EPA 8260B APP ITotal Xylenes
Page 6 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 6 of 30
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 10/30/17 14:39
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results

ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: L7J0207-01 (Water)
Client Sample ID: MW5
RL Dil Date Prepared
Sampled: 10/17/17 12:45
CAS #
7 RCRA Metals by Method 6010C
Analyst:ALGLaboratory:FTS - Florida
0.0100 mg/L0.00400 10.0335 10/24/17 12:3010/23/17 13:40 7440-38-2Arsenic
0.0500 mg/L0.00200 10.809 10/24/17 12:3010/23/17 13:40 7440-39-3Barium
0.00500 mg/L0.000300 10.00421 J 10/24/17 12:3010/23/17 13:40 7440-43-9Cadmium
0.0100 mg/L0.000300 10.0317 10/24/17 12:3010/23/17 13:40 7440-47-3Chromium
0.0100 mg/L0.00330 10.0897 10/24/17 12:3010/23/17 13:40 7439-92-1Lead
0.0500 mg/L0.0113 10.0113 U 10/24/17 12:3010/23/17 13:40 7782-49-2Selenium
0.0500 mg/L0.000600 10.000600 U 10/24/17 12:3010/23/17 13:40 7440-22-4Silver
Appendix I Low Level VOCs by Method 8260B
Analyst:JFLLaboratory:FTS - Florida
1.00 ug/L0.240 10.240 U 10/20/17 14:4310/20/17 11:55 630-20-61,1,1,2-Tetrachloroethane
1.00 ug/L0.160 10.160 U 10/20/17 14:4310/20/17 11:55 71-55-61,1,1-Trichloroethane
1.00 ug/L0.180 10.180 U 10/20/17 14:4310/20/17 11:55 79-34-51,1,2,2-Tetrachloroethane
1.00 ug/L0.250 10.250 U 10/20/17 14:4310/20/17 11:55 79-00-51,1,2-Trichloroethane
1.00 ug/L0.110 10.110 U 10/20/17 14:4310/20/17 11:55 75-34-31,1-Dichloroethane
1.00 ug/L0.200 10.200 U 10/20/17 14:4310/20/17 11:55 75-35-41,1-Dichloroethene
1.00 ug/L0.210 10.210 U 10/20/17 14:4310/20/17 11:55 96-18-41,2,3-Trichloropropane
1.00 ug/L0.190 10.190 U 10/20/17 14:4310/20/17 11:55 96-12-81,2-Dibromo-3-Chloropropane (DBCP)
1.00 ug/L0.180 10.180 U 10/20/17 14:4310/20/17 11:55 106-93-41,2-Dibromoethane (EDB)
1.00 ug/L0.140 10.140 U 10/20/17 14:4310/20/17 11:55 95-50-11,2-Dichlorobenzene
1.00 ug/L0.180 10.180 U 10/20/17 14:4310/20/17 11:55 107-06-21,2-Dichloroethane
1.00 ug/L0.150 10.150 U 10/20/17 14:4310/20/17 11:55 78-87-51,2-Dichloropropane
1.00 ug/L0.170 10.170 U 10/20/17 14:4310/20/17 11:55 106-46-71,4-Dichlorobenzene
2.00 ug/L0.280 10.280 U 10/20/17 14:4310/20/17 11:55 78-93-32-Butanone (MEK)
2.00 ug/L0.320 10.320 U 10/20/17 14:4310/20/17 11:55 591-78-62-Hexanone
2.00 ug/L0.260 10.260 U 10/20/17 14:4310/20/17 11:55 108-10-14-Methyl-2-pentanone (MIBK)
10.0 ug/L0.350 10.350 U 10/20/17 14:4310/20/17 11:55 67-64-1Acetone
2.00 ug/L0.490 10.490 U 10/20/17 14:4310/20/17 11:55 107-13-1Acrylonitrile
1.00 ug/L0.160 10.160 U 10/20/17 14:4310/20/17 11:55 71-43-2Benzene
1.00 ug/L0.200 10.200 U 10/20/17 14:4310/20/17 11:55 74-97-5Bromochloromethane
1.00 ug/L0.250 10.250 U 10/20/17 14:4310/20/17 11:55 75-27-4Bromodichloromethane
1.00 ug/L0.170 10.170 U 10/20/17 14:4310/20/17 11:55 75-25-2Bromoform
1.00 ug/L0.250 10.250 U 10/20/17 14:4310/20/17 11:55 74-83-9Bromomethane (Methyl Bromide)
1.00 ug/L0.260 10.260 U 10/20/17 14:4310/20/17 11:55 75-15-0Carbon disulfide
1.00 ug/L0.330 10.330 U 10/20/17 14:4310/20/17 11:55 56-23-5Carbon tetrachloride
1.00 ug/L0.150 10.150 U 10/20/17 14:4310/20/17 11:55 108-90-7Chlorobenzene
1.00 ug/L0.260 10.260 U 10/20/17 14:4310/20/17 11:55 75-00-3Chloroethane
1.00 ug/L0.160 10.160 U 10/20/17 14:4310/20/17 11:55 67-66-3Chloroform
1.00 ug/L0.250 10.250 U 10/20/17 14:4310/20/17 11:55 74-87-3Chloromethane (Methyl Chloride)
Page 7 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 7 of 30
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 10/30/17 14:39
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: L7J0207-01 (Water)
Client Sample ID: MW5 (Continued)
RL Dil Date Prepared
Sampled: 10/17/17 12:45
CAS #
Appendix I Low Level VOCs by Method 8260B (Continued)
Analyst:JFLLaboratory:FTS - Florida
1.00 ug/L0.210 10.210 U 10/20/17 14:4310/20/17 11:55 156-59-2cis-1,2-Dichloroethene
1.00 ug/L0.100 10.100 U 10/20/17 14:4310/20/17 11:55 10061-01-5cis-1,3-Dichloropropene
1.00 ug/L0.150 10.150 U 10/20/17 14:4310/20/17 11:55 124-48-1Dibromochloromethane
1.00 ug/L0.240 10.240 U 10/20/17 14:4310/20/17 11:55 74-95-3Dibromomethane
1.00 ug/L0.190 10.190 U 10/20/17 14:4310/20/17 11:55 100-41-4Ethylbenzene
1.00 ug/L0.310 10.310 U 10/20/17 14:4310/20/17 11:55 74-88-4Iodomethane (Methyl Iodide)
2.00 ug/L0.510 10.510 U 10/20/17 14:4310/20/17 11:55 179601-23-1m,p-Xylenes
1.00 ug/L0.420 10.420 U 10/20/17 14:4310/20/17 11:55 75-09-2Methylene Chloride
1.00 ug/L0.200 10.200 U 10/20/17 14:4310/20/17 11:55 95-47-6o-Xylene
1.00 ug/L0.180 10.180 U 10/20/17 14:4310/20/17 11:55 100-42-5Styrene
1.00 ug/L0.160 10.160 U 10/20/17 14:4310/20/17 11:55 127-18-4Tetrachloroethylene
1.00 ug/L0.140 10.140 U 10/20/17 14:4310/20/17 11:55 108-88-3Toluene
1.00 ug/L0.200 10.200 U 10/20/17 14:4310/20/17 11:55 1330-20-7Total Xylenes
1.00 ug/L0.210 10.210 U 10/20/17 14:4310/20/17 11:55 156-60-5trans-1,2-Dichloroethene
1.00 ug/L0.110 10.110 U 10/20/17 14:4310/20/17 11:55 1006-10-26trans-1,3-Dichloropropene
1.00 ug/L0.190 10.190 U 10/20/17 14:4310/20/17 11:55 110-57-6trans-1,4-Dichloro-2-butene
1.00 ug/L0.190 10.190 U 10/20/17 14:4310/20/17 11:55 79-01-6Trichloroethylene
1.00 ug/L0.530 10.530 U 10/20/17 14:4310/20/17 11:55 75-69-4Trichlorofluoromethane
1.00 ug/L0.720 10.720 U 10/20/17 14:4310/20/17 11:55 108-05-4Vinyl acetate
1.00 ug/L0.190 10.190 U 10/20/17 14:4310/20/17 11:55 75-01-4Vinyl chloride
Surrogate: 1,2-Dichloroethane-D4 (SUR)53-15991%10/20/17 14:43 10706-07-0
Surrogate: 4-Bromofluorobenzene (SUR)30-18683%10/20/17 14:43 460-00-4
Surrogate: Toluene-D8 (SUR)70-13093%10/20/17 14:43 2037-26-5
Total Mercury Analysis by Method 7470A
Analyst:JEBLaboratory:FTS - Florida
0.000200 mg/L0.0000700 10.0000700 U 10/25/17 14:0210/24/17 14:00 7439-97-6Mercury
VOCs by Method 8260B
Analyst:JFLLaboratory:FTS - Florida
5.00 ug/L0.236 10.236 U 10/20/17 14:4310/20/17 11:55 109-99-9Tetrahydrofuran
Page 8 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 8 of 30
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 10/30/17 14:39
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: L7J0207-02 (Water)
Client Sample ID: MW6
RL Dil Date Prepared
Sampled: 10/17/17 11:35
CAS #
7 RCRA Metals by Method 6010C
Analyst:ALGLaboratory:FTS - Florida
0.0100 mg/L0.00400 10.00412 J 10/24/17 12:3710/23/17 13:40 7440-38-2Arsenic
0.0500 mg/L0.00200 10.0397 J 10/24/17 12:3710/23/17 13:40 7440-39-3Barium
0.00500 mg/L0.000300 10.000300 U 10/24/17 12:3710/23/17 13:40 7440-43-9Cadmium
0.0100 mg/L0.000300 10.000300 U 10/24/17 12:3710/23/17 13:40 7440-47-3Chromium
0.0100 mg/L0.00330 10.00330 U 10/24/17 12:3710/23/17 13:40 7439-92-1Lead
0.0500 mg/L0.0113 10.0113 U 10/24/17 12:3710/23/17 13:40 7782-49-2Selenium
0.0500 mg/L0.000600 10.000600 U 10/24/17 12:3710/23/17 13:40 7440-22-4Silver
Appendix I Low Level VOCs by Method 8260B
Analyst:JFLLaboratory:FTS - Florida
1.00 ug/L0.240 10.240 U 10/20/17 15:0510/20/17 11:55 630-20-61,1,1,2-Tetrachloroethane
1.00 ug/L0.160 10.160 U 10/20/17 15:0510/20/17 11:55 71-55-61,1,1-Trichloroethane
1.00 ug/L0.180 10.180 U 10/20/17 15:0510/20/17 11:55 79-34-51,1,2,2-Tetrachloroethane
1.00 ug/L0.250 10.250 U 10/20/17 15:0510/20/17 11:55 79-00-51,1,2-Trichloroethane
1.00 ug/L0.110 10.110 U 10/20/17 15:0510/20/17 11:55 75-34-31,1-Dichloroethane
1.00 ug/L0.200 10.200 U 10/20/17 15:0510/20/17 11:55 75-35-41,1-Dichloroethene
1.00 ug/L0.210 10.210 U 10/20/17 15:0510/20/17 11:55 96-18-41,2,3-Trichloropropane
1.00 ug/L0.190 10.190 U 10/20/17 15:0510/20/17 11:55 96-12-81,2-Dibromo-3-Chloropropane (DBCP)
1.00 ug/L0.180 10.180 U 10/20/17 15:0510/20/17 11:55 106-93-41,2-Dibromoethane (EDB)
1.00 ug/L0.140 10.140 U 10/20/17 15:0510/20/17 11:55 95-50-11,2-Dichlorobenzene
1.00 ug/L0.180 10.180 U 10/20/17 15:0510/20/17 11:55 107-06-21,2-Dichloroethane
1.00 ug/L0.150 10.150 U 10/20/17 15:0510/20/17 11:55 78-87-51,2-Dichloropropane
1.00 ug/L0.170 10.170 U 10/20/17 15:0510/20/17 11:55 106-46-71,4-Dichlorobenzene
2.00 ug/L0.280 10.280 U 10/20/17 15:0510/20/17 11:55 78-93-32-Butanone (MEK)
2.00 ug/L0.320 10.320 U 10/20/17 15:0510/20/17 11:55 591-78-62-Hexanone
2.00 ug/L0.260 10.260 U 10/20/17 15:0510/20/17 11:55 108-10-14-Methyl-2-pentanone (MIBK)
10.0 ug/L0.350 10.350 U 10/20/17 15:0510/20/17 11:55 67-64-1Acetone
2.00 ug/L0.490 10.490 U 10/20/17 15:0510/20/17 11:55 107-13-1Acrylonitrile
1.00 ug/L0.160 10.160 U 10/20/17 15:0510/20/17 11:55 71-43-2Benzene
1.00 ug/L0.200 10.200 U 10/20/17 15:0510/20/17 11:55 74-97-5Bromochloromethane
1.00 ug/L0.250 10.250 U 10/20/17 15:0510/20/17 11:55 75-27-4Bromodichloromethane
1.00 ug/L0.170 10.170 U 10/20/17 15:0510/20/17 11:55 75-25-2Bromoform
1.00 ug/L0.250 10.250 U 10/20/17 15:0510/20/17 11:55 74-83-9Bromomethane (Methyl Bromide)
1.00 ug/L0.260 10.260 U 10/20/17 15:0510/20/17 11:55 75-15-0Carbon disulfide
1.00 ug/L0.330 10.330 U 10/20/17 15:0510/20/17 11:55 56-23-5Carbon tetrachloride
1.00 ug/L0.150 10.150 U 10/20/17 15:0510/20/17 11:55 108-90-7Chlorobenzene
1.00 ug/L0.260 10.260 U 10/20/17 15:0510/20/17 11:55 75-00-3Chloroethane
1.00 ug/L0.160 10.160 U 10/20/17 15:0510/20/17 11:55 67-66-3Chloroform
1.00 ug/L0.250 10.250 U 10/20/17 15:0510/20/17 11:55 74-87-3Chloromethane (Methyl Chloride)
1.00 ug/L0.210 10.210 U 10/20/17 15:0510/20/17 11:55 156-59-2cis-1,2-Dichloroethene
Page 9 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 9 of 30
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 10/30/17 14:39
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: L7J0207-02 (Water)
Client Sample ID: MW6 (Continued)
RL Dil Date Prepared
Sampled: 10/17/17 11:35
CAS #
Appendix I Low Level VOCs by Method 8260B (Continued)
Analyst:JFLLaboratory:FTS - Florida
1.00 ug/L0.100 10.100 U 10/20/17 15:0510/20/17 11:55 10061-01-5cis-1,3-Dichloropropene
1.00 ug/L0.150 10.150 U 10/20/17 15:0510/20/17 11:55 124-48-1Dibromochloromethane
1.00 ug/L0.240 10.240 U 10/20/17 15:0510/20/17 11:55 74-95-3Dibromomethane
1.00 ug/L0.190 10.190 U 10/20/17 15:0510/20/17 11:55 100-41-4Ethylbenzene
1.00 ug/L0.310 10.310 U 10/20/17 15:0510/20/17 11:55 74-88-4Iodomethane (Methyl Iodide)
2.00 ug/L0.510 10.510 U 10/20/17 15:0510/20/17 11:55 179601-23-1m,p-Xylenes
1.00 ug/L0.420 10.420 U 10/20/17 15:0510/20/17 11:55 75-09-2Methylene Chloride
1.00 ug/L0.200 10.200 U 10/20/17 15:0510/20/17 11:55 95-47-6o-Xylene
1.00 ug/L0.180 10.180 U 10/20/17 15:0510/20/17 11:55 100-42-5Styrene
1.00 ug/L0.160 10.160 U 10/20/17 15:0510/20/17 11:55 127-18-4Tetrachloroethylene
1.00 ug/L0.140 10.140 U 10/20/17 15:0510/20/17 11:55 108-88-3Toluene
1.00 ug/L0.200 10.200 U 10/20/17 15:0510/20/17 11:55 1330-20-7Total Xylenes
1.00 ug/L0.210 10.210 U 10/20/17 15:0510/20/17 11:55 156-60-5trans-1,2-Dichloroethene
1.00 ug/L0.110 10.110 U 10/20/17 15:0510/20/17 11:55 1006-10-26trans-1,3-Dichloropropene
1.00 ug/L0.190 10.190 U 10/20/17 15:0510/20/17 11:55 110-57-6trans-1,4-Dichloro-2-butene
1.00 ug/L0.190 10.190 U 10/20/17 15:0510/20/17 11:55 79-01-6Trichloroethylene
1.00 ug/L0.530 10.530 U 10/20/17 15:0510/20/17 11:55 75-69-4Trichlorofluoromethane
1.00 ug/L0.720 10.720 U 10/20/17 15:0510/20/17 11:55 108-05-4Vinyl acetate
1.00 ug/L0.190 10.190 U 10/20/17 15:0510/20/17 11:55 75-01-4Vinyl chloride
Surrogate: 1,2-Dichloroethane-D4 (SUR)53-15990%10/20/17 15:05 10706-07-0
Surrogate: 4-Bromofluorobenzene (SUR)30-18679%10/20/17 15:05 460-00-4
Surrogate: Toluene-D8 (SUR)70-13096%10/20/17 15:05 2037-26-5
Total Mercury Analysis by Method 7470A
Analyst:JEBLaboratory:FTS - Florida
0.000200 mg/L0.0000700 10.0000700 U 10/25/17 14:0210/24/17 14:00 7439-97-6Mercury
VOCs by Method 8260B
Analyst:JFLLaboratory:FTS - Florida
5.00 ug/L0.236 10.236 U 10/20/17 15:0510/20/17 11:55 109-99-9Tetrahydrofuran
Page 10 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 10 of 30
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 10/30/17 14:39
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: L7J0207-03 (Water)
Client Sample ID: MW9
RL Dil Date Prepared
Sampled: 10/17/17 11:25
CAS #
7 RCRA Metals by Method 6010C
Analyst:ALGLaboratory:FTS - Florida
0.0100 mg/L0.00400 10.00400 U 10/24/17 12:4510/23/17 13:40 7440-38-2Arsenic
0.0500 mg/L0.00200 10.195 10/24/17 12:4510/23/17 13:40 7440-39-3Barium
0.00500 mg/L0.000300 10.000300 U 10/24/17 12:4510/23/17 13:40 7440-43-9Cadmium
0.0100 mg/L0.000300 10.00886 J 10/24/17 12:4510/23/17 13:40 7440-47-3Chromium
0.0100 mg/L0.00330 10.0156 10/24/17 12:4510/23/17 13:40 7439-92-1Lead
0.0500 mg/L0.0113 10.0113 U 10/24/17 12:4510/23/17 13:40 7782-49-2Selenium
0.0500 mg/L0.000600 10.000600 U 10/24/17 12:4510/23/17 13:40 7440-22-4Silver
Appendix I Low Level VOCs by Method 8260B
Analyst:JFLLaboratory:FTS - Florida
1.00 ug/L0.240 10.240 U 10/20/17 15:2810/20/17 11:55 630-20-61,1,1,2-Tetrachloroethane
1.00 ug/L0.160 10.160 U 10/20/17 15:2810/20/17 11:55 71-55-61,1,1-Trichloroethane
1.00 ug/L0.180 10.180 U 10/20/17 15:2810/20/17 11:55 79-34-51,1,2,2-Tetrachloroethane
1.00 ug/L0.250 10.250 U 10/20/17 15:2810/20/17 11:55 79-00-51,1,2-Trichloroethane
1.00 ug/L0.110 10.110 U 10/20/17 15:2810/20/17 11:55 75-34-31,1-Dichloroethane
1.00 ug/L0.200 10.200 U 10/20/17 15:2810/20/17 11:55 75-35-41,1-Dichloroethene
1.00 ug/L0.210 10.210 U 10/20/17 15:2810/20/17 11:55 96-18-41,2,3-Trichloropropane
1.00 ug/L0.190 10.190 U 10/20/17 15:2810/20/17 11:55 96-12-81,2-Dibromo-3-Chloropropane (DBCP)
1.00 ug/L0.180 10.180 U 10/20/17 15:2810/20/17 11:55 106-93-41,2-Dibromoethane (EDB)
1.00 ug/L0.140 10.140 U 10/20/17 15:2810/20/17 11:55 95-50-11,2-Dichlorobenzene
1.00 ug/L0.180 10.180 U 10/20/17 15:2810/20/17 11:55 107-06-21,2-Dichloroethane
1.00 ug/L0.150 10.150 U 10/20/17 15:2810/20/17 11:55 78-87-51,2-Dichloropropane
1.00 ug/L0.170 10.170 U 10/20/17 15:2810/20/17 11:55 106-46-71,4-Dichlorobenzene
2.00 ug/L0.280 10.280 U 10/20/17 15:2810/20/17 11:55 78-93-32-Butanone (MEK)
2.00 ug/L0.320 10.320 U 10/20/17 15:2810/20/17 11:55 591-78-62-Hexanone
2.00 ug/L0.260 10.260 U 10/20/17 15:2810/20/17 11:55 108-10-14-Methyl-2-pentanone (MIBK)
10.0 ug/L0.350 10.350 U 10/20/17 15:2810/20/17 11:55 67-64-1Acetone
2.00 ug/L0.490 10.490 U 10/20/17 15:2810/20/17 11:55 107-13-1Acrylonitrile
1.00 ug/L0.160 10.160 U 10/20/17 15:2810/20/17 11:55 71-43-2Benzene
1.00 ug/L0.200 10.200 U 10/20/17 15:2810/20/17 11:55 74-97-5Bromochloromethane
1.00 ug/L0.250 10.250 U 10/20/17 15:2810/20/17 11:55 75-27-4Bromodichloromethane
1.00 ug/L0.170 10.170 U 10/20/17 15:2810/20/17 11:55 75-25-2Bromoform
1.00 ug/L0.250 10.250 U 10/20/17 15:2810/20/17 11:55 74-83-9Bromomethane (Methyl Bromide)
1.00 ug/L0.260 10.260 U 10/20/17 15:2810/20/17 11:55 75-15-0Carbon disulfide
1.00 ug/L0.330 10.330 U 10/20/17 15:2810/20/17 11:55 56-23-5Carbon tetrachloride
1.00 ug/L0.150 10.150 U 10/20/17 15:2810/20/17 11:55 108-90-7Chlorobenzene
1.00 ug/L0.260 10.260 U 10/20/17 15:2810/20/17 11:55 75-00-3Chloroethane
1.00 ug/L0.160 10.160 U 10/20/17 15:2810/20/17 11:55 67-66-3Chloroform
1.00 ug/L0.250 10.250 U 10/20/17 15:2810/20/17 11:55 74-87-3Chloromethane (Methyl Chloride)
1.00 ug/L0.210 10.210 U 10/20/17 15:2810/20/17 11:55 156-59-2cis-1,2-Dichloroethene
Page 11 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 11 of 30
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 10/30/17 14:39
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: L7J0207-03 (Water)
Client Sample ID: MW9 (Continued)
RL Dil Date Prepared
Sampled: 10/17/17 11:25
CAS #
Appendix I Low Level VOCs by Method 8260B (Continued)
Analyst:JFLLaboratory:FTS - Florida
1.00 ug/L0.100 10.100 U 10/20/17 15:2810/20/17 11:55 10061-01-5cis-1,3-Dichloropropene
1.00 ug/L0.150 10.150 U 10/20/17 15:2810/20/17 11:55 124-48-1Dibromochloromethane
1.00 ug/L0.240 10.240 U 10/20/17 15:2810/20/17 11:55 74-95-3Dibromomethane
1.00 ug/L0.190 10.190 U 10/20/17 15:2810/20/17 11:55 100-41-4Ethylbenzene
1.00 ug/L0.310 10.310 U 10/20/17 15:2810/20/17 11:55 74-88-4Iodomethane (Methyl Iodide)
2.00 ug/L0.510 10.510 U 10/20/17 15:2810/20/17 11:55 179601-23-1m,p-Xylenes
1.00 ug/L0.420 10.420 U 10/20/17 15:2810/20/17 11:55 75-09-2Methylene Chloride
1.00 ug/L0.200 10.200 U 10/20/17 15:2810/20/17 11:55 95-47-6o-Xylene
1.00 ug/L0.180 10.180 U 10/20/17 15:2810/20/17 11:55 100-42-5Styrene
1.00 ug/L0.160 10.160 U 10/20/17 15:2810/20/17 11:55 127-18-4Tetrachloroethylene
1.00 ug/L0.140 10.140 U 10/20/17 15:2810/20/17 11:55 108-88-3Toluene
1.00 ug/L0.200 10.200 U 10/20/17 15:2810/20/17 11:55 1330-20-7Total Xylenes
1.00 ug/L0.210 10.210 U 10/20/17 15:2810/20/17 11:55 156-60-5trans-1,2-Dichloroethene
1.00 ug/L0.110 10.110 U 10/20/17 15:2810/20/17 11:55 1006-10-26trans-1,3-Dichloropropene
1.00 ug/L0.190 10.190 U 10/20/17 15:2810/20/17 11:55 110-57-6trans-1,4-Dichloro-2-butene
1.00 ug/L0.190 10.190 U 10/20/17 15:2810/20/17 11:55 79-01-6Trichloroethylene
1.00 ug/L0.530 10.530 U 10/20/17 15:2810/20/17 11:55 75-69-4Trichlorofluoromethane
1.00 ug/L0.720 10.720 U 10/20/17 15:2810/20/17 11:55 108-05-4Vinyl acetate
1.00 ug/L0.190 10.190 U 10/20/17 15:2810/20/17 11:55 75-01-4Vinyl chloride
Surrogate: 1,2-Dichloroethane-D4 (SUR)53-15993%10/20/17 15:28 10706-07-0
Surrogate: 4-Bromofluorobenzene (SUR)30-18680%10/20/17 15:28 460-00-4
Surrogate: Toluene-D8 (SUR)70-13094%10/20/17 15:28 2037-26-5
Total Mercury Analysis by Method 7470A
Analyst:JEBLaboratory:FTS - Florida
0.000200 mg/L0.0000700 10.0000700 U 10/25/17 14:0210/24/17 14:00 7439-97-6Mercury
VOCs by Method 8260B
Analyst:JFLLaboratory:FTS - Florida
5.00 ug/L0.236 10.236 U 10/20/17 15:2810/20/17 11:55 109-99-9Tetrahydrofuran
Page 12 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 12 of 30
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 10/30/17 14:39
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: L7J0207-04 (Water)
Client Sample ID: MW12
RL Dil Date Prepared
Sampled: 10/17/17 12:30
CAS #
7 RCRA Metals by Method 6010C
Analyst:ALGLaboratory:FTS - Florida
0.0100 mg/L0.00400 10.0106 10/24/17 12:4710/23/17 13:40 7440-38-2Arsenic
0.0500 mg/L0.00200 11.54 10/24/17 12:4710/23/17 13:40 7440-39-3Barium
0.00500 mg/L0.000300 10.00368 J 10/24/17 12:4710/23/17 13:40 7440-43-9Cadmium
0.0100 mg/L0.000300 10.00700 J 10/24/17 12:4710/23/17 13:40 7440-47-3Chromium
0.0100 mg/L0.00330 10.0396 10/24/17 12:4710/23/17 13:40 7439-92-1Lead
0.0500 mg/L0.0113 10.0113 U 10/24/17 12:4710/23/17 13:40 7782-49-2Selenium
0.0500 mg/L0.000600 10.000600 U 10/24/17 12:4710/23/17 13:40 7440-22-4Silver
Appendix I Low Level VOCs by Method 8260B
Analyst:JFLLaboratory:FTS - Florida
1.00 ug/L0.240 10.240 U 10/20/17 15:5010/20/17 11:55 630-20-61,1,1,2-Tetrachloroethane
1.00 ug/L0.160 10.160 U 10/20/17 15:5010/20/17 11:55 71-55-61,1,1-Trichloroethane
1.00 ug/L0.180 10.180 U 10/20/17 15:5010/20/17 11:55 79-34-51,1,2,2-Tetrachloroethane
1.00 ug/L0.250 10.250 U 10/20/17 15:5010/20/17 11:55 79-00-51,1,2-Trichloroethane
1.00 ug/L0.110 14.38 10/20/17 15:5010/20/17 11:55 75-34-31,1-Dichloroethane
1.00 ug/L0.200 10.200 U 10/20/17 15:5010/20/17 11:55 75-35-41,1-Dichloroethene
1.00 ug/L0.210 10.210 U 10/20/17 15:5010/20/17 11:55 96-18-41,2,3-Trichloropropane
1.00 ug/L0.190 10.190 U 10/20/17 15:5010/20/17 11:55 96-12-81,2-Dibromo-3-Chloropropane (DBCP)
1.00 ug/L0.180 10.180 U 10/20/17 15:5010/20/17 11:55 106-93-41,2-Dibromoethane (EDB)
1.00 ug/L0.140 10.430 J 10/20/17 15:5010/20/17 11:55 95-50-11,2-Dichlorobenzene
1.00 ug/L0.180 10.180 U 10/20/17 15:5010/20/17 11:55 107-06-21,2-Dichloroethane
1.00 ug/L0.150 10.150 U 10/20/17 15:5010/20/17 11:55 78-87-51,2-Dichloropropane
1.00 ug/L0.170 13.55 10/20/17 15:5010/20/17 11:55 106-46-71,4-Dichlorobenzene
2.00 ug/L0.280 10.280 U 10/20/17 15:5010/20/17 11:55 78-93-32-Butanone (MEK)
2.00 ug/L0.320 10.320 U 10/20/17 15:5010/20/17 11:55 591-78-62-Hexanone
2.00 ug/L0.260 10.260 U 10/20/17 15:5010/20/17 11:55 108-10-14-Methyl-2-pentanone (MIBK)
10.0 ug/L0.350 10.350 U 10/20/17 15:5010/20/17 11:55 67-64-1Acetone
2.00 ug/L0.490 10.490 U 10/20/17 15:5010/20/17 11:55 107-13-1Acrylonitrile
1.00 ug/L0.160 13.45 10/20/17 15:5010/20/17 11:55 71-43-2Benzene
1.00 ug/L0.200 10.200 U 10/20/17 15:5010/20/17 11:55 74-97-5Bromochloromethane
1.00 ug/L0.250 10.250 U 10/20/17 15:5010/20/17 11:55 75-27-4Bromodichloromethane
1.00 ug/L0.170 10.170 U 10/20/17 15:5010/20/17 11:55 75-25-2Bromoform
1.00 ug/L0.250 10.250 U 10/20/17 15:5010/20/17 11:55 74-83-9Bromomethane (Methyl Bromide)
1.00 ug/L0.260 10.260 U 10/20/17 15:5010/20/17 11:55 75-15-0Carbon disulfide
1.00 ug/L0.330 10.330 U 10/20/17 15:5010/20/17 11:55 56-23-5Carbon tetrachloride
1.00 ug/L0.150 112.8 10/20/17 15:5010/20/17 11:55 108-90-7Chlorobenzene
1.00 ug/L0.260 134.3 10/20/17 15:5010/20/17 11:55 75-00-3Chloroethane
1.00 ug/L0.160 10.160 U 10/20/17 15:5010/20/17 11:55 67-66-3Chloroform
1.00 ug/L0.250 10.250 U 10/20/17 15:5010/20/17 11:55 74-87-3Chloromethane (Methyl Chloride)
1.00 ug/L0.210 10.210 U 10/20/17 15:5010/20/17 11:55 156-59-2cis-1,2-Dichloroethene
Page 13 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 13 of 30
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 10/30/17 14:39
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: L7J0207-04 (Water)
Client Sample ID: MW12 (Continued)
RL Dil Date Prepared
Sampled: 10/17/17 12:30
CAS #
Appendix I Low Level VOCs by Method 8260B (Continued)
Analyst:JFLLaboratory:FTS - Florida
1.00 ug/L0.100 10.100 U 10/20/17 15:5010/20/17 11:55 10061-01-5cis-1,3-Dichloropropene
1.00 ug/L0.150 10.150 U 10/20/17 15:5010/20/17 11:55 124-48-1Dibromochloromethane
1.00 ug/L0.240 10.240 U 10/20/17 15:5010/20/17 11:55 74-95-3Dibromomethane
1.00 ug/L0.190 10.190 U 10/20/17 15:5010/20/17 11:55 100-41-4Ethylbenzene
1.00 ug/L0.310 10.310 U 10/20/17 15:5010/20/17 11:55 74-88-4Iodomethane (Methyl Iodide)
2.00 ug/L0.510 10.510 U 10/20/17 15:5010/20/17 11:55 179601-23-1m,p-Xylenes
1.00 ug/L0.420 10.420 U 10/20/17 15:5010/20/17 11:55 75-09-2Methylene Chloride
1.00 ug/L0.200 10.200 U 10/20/17 15:5010/20/17 11:55 95-47-6o-Xylene
1.00 ug/L0.180 10.180 U 10/20/17 15:5010/20/17 11:55 100-42-5Styrene
1.00 ug/L0.160 10.160 U 10/20/17 15:5010/20/17 11:55 127-18-4Tetrachloroethylene
1.00 ug/L0.140 10.460 J 10/20/17 15:5010/20/17 11:55 108-88-3Toluene
1.00 ug/L0.200 10.420 J 10/20/17 15:5010/20/17 11:55 1330-20-7Total Xylenes
1.00 ug/L0.210 10.210 U 10/20/17 15:5010/20/17 11:55 156-60-5trans-1,2-Dichloroethene
1.00 ug/L0.110 10.110 U 10/20/17 15:5010/20/17 11:55 1006-10-26trans-1,3-Dichloropropene
1.00 ug/L0.190 10.190 U 10/20/17 15:5010/20/17 11:55 110-57-6trans-1,4-Dichloro-2-butene
1.00 ug/L0.190 10.190 U 10/20/17 15:5010/20/17 11:55 79-01-6Trichloroethylene
1.00 ug/L0.530 10.530 U 10/20/17 15:5010/20/17 11:55 75-69-4Trichlorofluoromethane
1.00 ug/L0.720 10.720 U 10/20/17 15:5010/20/17 11:55 108-05-4Vinyl acetate
1.00 ug/L0.190 10.190 U 10/20/17 15:5010/20/17 11:55 75-01-4Vinyl chloride
Surrogate: 1,2-Dichloroethane-D4 (SUR)53-15992%10/20/17 15:50 10706-07-0
Surrogate: 4-Bromofluorobenzene (SUR)30-18683%10/20/17 15:50 460-00-4
Surrogate: Toluene-D8 (SUR)70-13091%10/20/17 15:50 2037-26-5
Total Mercury Analysis by Method 7470A
Analyst:JEBLaboratory:FTS - Florida
0.000200 mg/L0.0000700 10.0000700 U 10/25/17 14:0210/24/17 14:00 7439-97-6Mercury
VOCs by Method 8260B
Analyst:JFLLaboratory:FTS - Florida
5.00 ug/L0.236 10.236 U 10/20/17 15:5010/20/17 11:55 109-99-9Tetrahydrofuran
Page 14 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 14 of 30
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 10/30/17 14:39
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: L7J0207-05 (Water)
Client Sample ID: MW13
RL Dil Date Prepared
Sampled: 10/17/17 11:10
CAS #
7 RCRA Metals by Method 6010C
Analyst:ALGLaboratory:FTS - Florida
0.0100 mg/L0.00400 10.0226 10/24/17 12:4910/23/17 13:40 7440-38-2Arsenic
0.0500 mg/L0.00200 10.530 10/24/17 12:4910/23/17 13:40 7440-39-3Barium
0.00500 mg/L0.000300 10.00207 J 10/24/17 12:4910/23/17 13:40 7440-43-9Cadmium
0.0100 mg/L0.000300 10.0184 10/24/17 12:4910/23/17 13:40 7440-47-3Chromium
0.0100 mg/L0.00330 10.0578 10/24/17 12:4910/23/17 13:40 7439-92-1Lead
0.0500 mg/L0.0113 10.0113 U 10/24/17 12:4910/23/17 13:40 7782-49-2Selenium
0.0500 mg/L0.000600 10.000600 U 10/24/17 12:4910/23/17 13:40 7440-22-4Silver
Appendix I Low Level VOCs by Method 8260B
Analyst:JFLLaboratory:FTS - Florida
1.00 ug/L0.240 10.240 U 10/20/17 16:1310/20/17 11:55 630-20-61,1,1,2-Tetrachloroethane
1.00 ug/L0.160 10.160 U 10/20/17 16:1310/20/17 11:55 71-55-61,1,1-Trichloroethane
1.00 ug/L0.180 10.180 U 10/20/17 16:1310/20/17 11:55 79-34-51,1,2,2-Tetrachloroethane
1.00 ug/L0.250 10.250 U 10/20/17 16:1310/20/17 11:55 79-00-51,1,2-Trichloroethane
1.00 ug/L0.110 10.110 U 10/20/17 16:1310/20/17 11:55 75-34-31,1-Dichloroethane
1.00 ug/L0.200 10.200 U 10/20/17 16:1310/20/17 11:55 75-35-41,1-Dichloroethene
1.00 ug/L0.210 10.210 U 10/20/17 16:1310/20/17 11:55 96-18-41,2,3-Trichloropropane
1.00 ug/L0.190 10.190 U 10/20/17 16:1310/20/17 11:55 96-12-81,2-Dibromo-3-Chloropropane (DBCP)
1.00 ug/L0.180 10.180 U 10/20/17 16:1310/20/17 11:55 106-93-41,2-Dibromoethane (EDB)
1.00 ug/L0.140 10.140 U 10/20/17 16:1310/20/17 11:55 95-50-11,2-Dichlorobenzene
1.00 ug/L0.180 10.180 U 10/20/17 16:1310/20/17 11:55 107-06-21,2-Dichloroethane
1.00 ug/L0.150 10.150 U 10/20/17 16:1310/20/17 11:55 78-87-51,2-Dichloropropane
1.00 ug/L0.170 10.170 U 10/20/17 16:1310/20/17 11:55 106-46-71,4-Dichlorobenzene
2.00 ug/L0.280 10.280 U 10/20/17 16:1310/20/17 11:55 78-93-32-Butanone (MEK)
2.00 ug/L0.320 10.320 U 10/20/17 16:1310/20/17 11:55 591-78-62-Hexanone
2.00 ug/L0.260 10.260 U 10/20/17 16:1310/20/17 11:55 108-10-14-Methyl-2-pentanone (MIBK)
10.0 ug/L0.350 10.350 U 10/20/17 16:1310/20/17 11:55 67-64-1Acetone
2.00 ug/L0.490 10.490 U 10/20/17 16:1310/20/17 11:55 107-13-1Acrylonitrile
1.00 ug/L0.160 10.160 U 10/20/17 16:1310/20/17 11:55 71-43-2Benzene
1.00 ug/L0.200 10.200 U 10/20/17 16:1310/20/17 11:55 74-97-5Bromochloromethane
1.00 ug/L0.250 10.250 U 10/20/17 16:1310/20/17 11:55 75-27-4Bromodichloromethane
1.00 ug/L0.170 10.170 U 10/20/17 16:1310/20/17 11:55 75-25-2Bromoform
1.00 ug/L0.250 10.250 U 10/20/17 16:1310/20/17 11:55 74-83-9Bromomethane (Methyl Bromide)
1.00 ug/L0.260 10.260 U 10/20/17 16:1310/20/17 11:55 75-15-0Carbon disulfide
1.00 ug/L0.330 10.330 U 10/20/17 16:1310/20/17 11:55 56-23-5Carbon tetrachloride
1.00 ug/L0.150 10.150 U 10/20/17 16:1310/20/17 11:55 108-90-7Chlorobenzene
1.00 ug/L0.260 10.260 U 10/20/17 16:1310/20/17 11:55 75-00-3Chloroethane
1.00 ug/L0.160 10.160 U 10/20/17 16:1310/20/17 11:55 67-66-3Chloroform
1.00 ug/L0.250 10.250 U 10/20/17 16:1310/20/17 11:55 74-87-3Chloromethane (Methyl Chloride)
1.00 ug/L0.210 10.210 U 10/20/17 16:1310/20/17 11:55 156-59-2cis-1,2-Dichloroethene
Page 15 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 15 of 30
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 10/30/17 14:39
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: L7J0207-05 (Water)
Client Sample ID: MW13 (Continued)
RL Dil Date Prepared
Sampled: 10/17/17 11:10
CAS #
Appendix I Low Level VOCs by Method 8260B (Continued)
Analyst:JFLLaboratory:FTS - Florida
1.00 ug/L0.100 10.100 U 10/20/17 16:1310/20/17 11:55 10061-01-5cis-1,3-Dichloropropene
1.00 ug/L0.150 10.150 U 10/20/17 16:1310/20/17 11:55 124-48-1Dibromochloromethane
1.00 ug/L0.240 10.240 U 10/20/17 16:1310/20/17 11:55 74-95-3Dibromomethane
1.00 ug/L0.190 10.190 U 10/20/17 16:1310/20/17 11:55 100-41-4Ethylbenzene
1.00 ug/L0.310 10.310 U 10/20/17 16:1310/20/17 11:55 74-88-4Iodomethane (Methyl Iodide)
2.00 ug/L0.510 10.510 U 10/20/17 16:1310/20/17 11:55 179601-23-1m,p-Xylenes
1.00 ug/L0.420 10.420 U 10/20/17 16:1310/20/17 11:55 75-09-2Methylene Chloride
1.00 ug/L0.200 10.200 U 10/20/17 16:1310/20/17 11:55 95-47-6o-Xylene
1.00 ug/L0.180 10.180 U 10/20/17 16:1310/20/17 11:55 100-42-5Styrene
1.00 ug/L0.160 10.160 U 10/20/17 16:1310/20/17 11:55 127-18-4Tetrachloroethylene
1.00 ug/L0.140 10.140 U 10/20/17 16:1310/20/17 11:55 108-88-3Toluene
1.00 ug/L0.200 10.200 U 10/20/17 16:1310/20/17 11:55 1330-20-7Total Xylenes
1.00 ug/L0.210 10.210 U 10/20/17 16:1310/20/17 11:55 156-60-5trans-1,2-Dichloroethene
1.00 ug/L0.110 10.110 U 10/20/17 16:1310/20/17 11:55 1006-10-26trans-1,3-Dichloropropene
1.00 ug/L0.190 10.190 U 10/20/17 16:1310/20/17 11:55 110-57-6trans-1,4-Dichloro-2-butene
1.00 ug/L0.190 10.190 U 10/20/17 16:1310/20/17 11:55 79-01-6Trichloroethylene
1.00 ug/L0.530 10.530 U 10/20/17 16:1310/20/17 11:55 75-69-4Trichlorofluoromethane
1.00 ug/L0.720 10.720 U 10/20/17 16:1310/20/17 11:55 108-05-4Vinyl acetate
1.00 ug/L0.190 10.190 U 10/20/17 16:1310/20/17 11:55 75-01-4Vinyl chloride
Surrogate: 1,2-Dichloroethane-D4 (SUR)53-15991%10/20/17 16:13 10706-07-0
Surrogate: 4-Bromofluorobenzene (SUR)30-18682%10/20/17 16:13 460-00-4
Surrogate: Toluene-D8 (SUR)70-13094%10/20/17 16:13 2037-26-5
Total Mercury Analysis by Method 7470A
Analyst:JEBLaboratory:FTS - Florida
0.000200 mg/L0.0000700 10.0000700 U 10/25/17 14:0210/24/17 14:00 7439-97-6Mercury
VOCs by Method 8260B
Analyst:JFLLaboratory:FTS - Florida
5.00 ug/L0.236 10.236 U 10/20/17 16:1310/20/17 11:55 109-99-9Tetrahydrofuran
Page 16 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 16 of 30
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 10/30/17 14:39
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: L7J0207-06 (Water)
Client Sample ID: MW14
RL Dil Date Prepared
Sampled: 10/17/17 11:00
CAS #
7 RCRA Metals by Method 6010C
Analyst:ALGLaboratory:FTS - Florida
0.0100 mg/L0.00400 10.00788 J 10/24/17 12:5110/23/17 13:40 7440-38-2Arsenic
0.0500 mg/L0.00200 10.353 10/24/17 12:5110/23/17 13:40 7440-39-3Barium
0.00500 mg/L0.000300 10.00200 J 10/24/17 12:5110/23/17 13:40 7440-43-9Cadmium
0.0100 mg/L0.000300 10.0342 10/24/17 12:5110/23/17 13:40 7440-47-3Chromium
0.0100 mg/L0.00330 10.710 10/24/17 12:5110/23/17 13:40 7439-92-1Lead
0.0500 mg/L0.0113 10.0113 U 10/24/17 12:5110/23/17 13:40 7782-49-2Selenium
0.0500 mg/L0.000600 10.000600 U 10/24/17 12:5110/23/17 13:40 7440-22-4Silver
Appendix I Low Level VOCs by Method 8260B
Analyst:JFLLaboratory:FTS - Florida
1.00 ug/L0.240 10.240 U 10/20/17 16:3510/20/17 11:55 630-20-61,1,1,2-Tetrachloroethane
1.00 ug/L0.160 10.160 U 10/20/17 16:3510/20/17 11:55 71-55-61,1,1-Trichloroethane
1.00 ug/L0.180 10.180 U 10/20/17 16:3510/20/17 11:55 79-34-51,1,2,2-Tetrachloroethane
1.00 ug/L0.250 10.250 U 10/20/17 16:3510/20/17 11:55 79-00-51,1,2-Trichloroethane
1.00 ug/L0.110 10.110 U 10/20/17 16:3510/20/17 11:55 75-34-31,1-Dichloroethane
1.00 ug/L0.200 10.200 U 10/20/17 16:3510/20/17 11:55 75-35-41,1-Dichloroethene
1.00 ug/L0.210 10.210 U 10/20/17 16:3510/20/17 11:55 96-18-41,2,3-Trichloropropane
1.00 ug/L0.190 10.190 U 10/20/17 16:3510/20/17 11:55 96-12-81,2-Dibromo-3-Chloropropane (DBCP)
1.00 ug/L0.180 10.180 U 10/20/17 16:3510/20/17 11:55 106-93-41,2-Dibromoethane (EDB)
1.00 ug/L0.140 10.140 U 10/20/17 16:3510/20/17 11:55 95-50-11,2-Dichlorobenzene
1.00 ug/L0.180 10.180 U 10/20/17 16:3510/20/17 11:55 107-06-21,2-Dichloroethane
1.00 ug/L0.150 10.150 U 10/20/17 16:3510/20/17 11:55 78-87-51,2-Dichloropropane
1.00 ug/L0.170 10.170 U 10/20/17 16:3510/20/17 11:55 106-46-71,4-Dichlorobenzene
2.00 ug/L0.280 10.280 U 10/20/17 16:3510/20/17 11:55 78-93-32-Butanone (MEK)
2.00 ug/L0.320 10.320 U 10/20/17 16:3510/20/17 11:55 591-78-62-Hexanone
2.00 ug/L0.260 10.260 U 10/20/17 16:3510/20/17 11:55 108-10-14-Methyl-2-pentanone (MIBK)
10.0 ug/L0.350 10.350 U 10/20/17 16:3510/20/17 11:55 67-64-1Acetone
2.00 ug/L0.490 10.490 U 10/20/17 16:3510/20/17 11:55 107-13-1Acrylonitrile
1.00 ug/L0.160 10.160 U 10/20/17 16:3510/20/17 11:55 71-43-2Benzene
1.00 ug/L0.200 10.200 U 10/20/17 16:3510/20/17 11:55 74-97-5Bromochloromethane
1.00 ug/L0.250 10.250 U 10/20/17 16:3510/20/17 11:55 75-27-4Bromodichloromethane
1.00 ug/L0.170 10.170 U 10/20/17 16:3510/20/17 11:55 75-25-2Bromoform
1.00 ug/L0.250 10.250 U 10/20/17 16:3510/20/17 11:55 74-83-9Bromomethane (Methyl Bromide)
1.00 ug/L0.260 10.260 U 10/20/17 16:3510/20/17 11:55 75-15-0Carbon disulfide
1.00 ug/L0.330 10.330 U 10/20/17 16:3510/20/17 11:55 56-23-5Carbon tetrachloride
1.00 ug/L0.150 10.150 U 10/20/17 16:3510/20/17 11:55 108-90-7Chlorobenzene
1.00 ug/L0.260 10.260 U 10/20/17 16:3510/20/17 11:55 75-00-3Chloroethane
1.00 ug/L0.160 10.160 U 10/20/17 16:3510/20/17 11:55 67-66-3Chloroform
1.00 ug/L0.250 10.250 U 10/20/17 16:3510/20/17 11:55 74-87-3Chloromethane (Methyl Chloride)
1.00 ug/L0.210 10.210 U 10/20/17 16:3510/20/17 11:55 156-59-2cis-1,2-Dichloroethene
Page 17 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 17 of 30
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 10/30/17 14:39
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: L7J0207-06 (Water)
Client Sample ID: MW14 (Continued)
RL Dil Date Prepared
Sampled: 10/17/17 11:00
CAS #
Appendix I Low Level VOCs by Method 8260B (Continued)
Analyst:JFLLaboratory:FTS - Florida
1.00 ug/L0.100 10.100 U 10/20/17 16:3510/20/17 11:55 10061-01-5cis-1,3-Dichloropropene
1.00 ug/L0.150 10.150 U 10/20/17 16:3510/20/17 11:55 124-48-1Dibromochloromethane
1.00 ug/L0.240 10.240 U 10/20/17 16:3510/20/17 11:55 74-95-3Dibromomethane
1.00 ug/L0.190 10.190 U 10/20/17 16:3510/20/17 11:55 100-41-4Ethylbenzene
1.00 ug/L0.310 10.310 U 10/20/17 16:3510/20/17 11:55 74-88-4Iodomethane (Methyl Iodide)
2.00 ug/L0.510 10.510 U 10/20/17 16:3510/20/17 11:55 179601-23-1m,p-Xylenes
1.00 ug/L0.420 10.420 U 10/20/17 16:3510/20/17 11:55 75-09-2Methylene Chloride
1.00 ug/L0.200 10.200 U 10/20/17 16:3510/20/17 11:55 95-47-6o-Xylene
1.00 ug/L0.180 10.180 U 10/20/17 16:3510/20/17 11:55 100-42-5Styrene
1.00 ug/L0.160 10.160 U 10/20/17 16:3510/20/17 11:55 127-18-4Tetrachloroethylene
1.00 ug/L0.140 10.140 U 10/20/17 16:3510/20/17 11:55 108-88-3Toluene
1.00 ug/L0.200 10.200 U 10/20/17 16:3510/20/17 11:55 1330-20-7Total Xylenes
1.00 ug/L0.210 10.210 U 10/20/17 16:3510/20/17 11:55 156-60-5trans-1,2-Dichloroethene
1.00 ug/L0.110 10.110 U 10/20/17 16:3510/20/17 11:55 1006-10-26trans-1,3-Dichloropropene
1.00 ug/L0.190 10.190 U 10/20/17 16:3510/20/17 11:55 110-57-6trans-1,4-Dichloro-2-butene
1.00 ug/L0.190 10.190 U 10/20/17 16:3510/20/17 11:55 79-01-6Trichloroethylene
1.00 ug/L0.530 10.530 U 10/20/17 16:3510/20/17 11:55 75-69-4Trichlorofluoromethane
1.00 ug/L0.720 10.720 U 10/20/17 16:3510/20/17 11:55 108-05-4Vinyl acetate
1.00 ug/L0.190 10.190 U 10/20/17 16:3510/20/17 11:55 75-01-4Vinyl chloride
Surrogate: 1,2-Dichloroethane-D4 (SUR)53-15992%10/20/17 16:35 10706-07-0
Surrogate: 4-Bromofluorobenzene (SUR)30-18683%10/20/17 16:35 460-00-4
Surrogate: Toluene-D8 (SUR)70-13094%10/20/17 16:35 2037-26-5
Total Mercury Analysis by Method 7470A
Analyst:JEBLaboratory:FTS - Florida
0.000200 mg/L0.0000700 10.0000700 U 10/25/17 14:0210/24/17 14:00 7439-97-6Mercury
VOCs by Method 8260B
Analyst:JFLLaboratory:FTS - Florida
5.00 ug/L0.236 10.236 U 10/20/17 16:3510/20/17 11:55 109-99-9Tetrahydrofuran
Page 18 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 18 of 30
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 10/30/17 14:39
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: L7J0207-07 (Water)
Client Sample ID: TRIP BLANK
RL Dil Date Prepared
Sampled: 10/17/17 0:00
CAS #
Appendix I Low Level VOCs by Method 8260B
Analyst:JFLLaboratory:FTS - Florida
1.00 ug/L0.240 10.240 U 10/20/17 14:2010/20/17 11:55 630-20-61,1,1,2-Tetrachloroethane
1.00 ug/L0.160 10.160 U 10/20/17 14:2010/20/17 11:55 71-55-61,1,1-Trichloroethane
1.00 ug/L0.180 10.180 U 10/20/17 14:2010/20/17 11:55 79-34-51,1,2,2-Tetrachloroethane
1.00 ug/L0.250 10.250 U 10/20/17 14:2010/20/17 11:55 79-00-51,1,2-Trichloroethane
1.00 ug/L0.110 10.110 U 10/20/17 14:2010/20/17 11:55 75-34-31,1-Dichloroethane
1.00 ug/L0.200 10.200 U 10/20/17 14:2010/20/17 11:55 75-35-41,1-Dichloroethene
1.00 ug/L0.210 10.210 U 10/20/17 14:2010/20/17 11:55 96-18-41,2,3-Trichloropropane
1.00 ug/L0.190 10.190 U 10/20/17 14:2010/20/17 11:55 96-12-81,2-Dibromo-3-Chloropropane (DBCP)
1.00 ug/L0.180 10.180 U 10/20/17 14:2010/20/17 11:55 106-93-41,2-Dibromoethane (EDB)
1.00 ug/L0.140 10.140 U 10/20/17 14:2010/20/17 11:55 95-50-11,2-Dichlorobenzene
1.00 ug/L0.180 10.180 U 10/20/17 14:2010/20/17 11:55 107-06-21,2-Dichloroethane
1.00 ug/L0.150 10.150 U 10/20/17 14:2010/20/17 11:55 78-87-51,2-Dichloropropane
1.00 ug/L0.170 10.170 U 10/20/17 14:2010/20/17 11:55 106-46-71,4-Dichlorobenzene
2.00 ug/L0.280 10.280 U 10/20/17 14:2010/20/17 11:55 78-93-32-Butanone (MEK)
2.00 ug/L0.320 10.320 U 10/20/17 14:2010/20/17 11:55 591-78-62-Hexanone
2.00 ug/L0.260 10.260 U 10/20/17 14:2010/20/17 11:55 108-10-14-Methyl-2-pentanone (MIBK)
10.0 ug/L0.350 10.350 U 10/20/17 14:2010/20/17 11:55 67-64-1Acetone
2.00 ug/L0.490 10.490 U 10/20/17 14:2010/20/17 11:55 107-13-1Acrylonitrile
1.00 ug/L0.160 10.160 U 10/20/17 14:2010/20/17 11:55 71-43-2Benzene
1.00 ug/L0.200 10.200 U 10/20/17 14:2010/20/17 11:55 74-97-5Bromochloromethane
1.00 ug/L0.250 10.250 U 10/20/17 14:2010/20/17 11:55 75-27-4Bromodichloromethane
1.00 ug/L0.170 10.170 U 10/20/17 14:2010/20/17 11:55 75-25-2Bromoform
1.00 ug/L0.250 10.250 U 10/20/17 14:2010/20/17 11:55 74-83-9Bromomethane (Methyl Bromide)
1.00 ug/L0.260 10.260 U 10/20/17 14:2010/20/17 11:55 75-15-0Carbon disulfide
1.00 ug/L0.330 10.330 U 10/20/17 14:2010/20/17 11:55 56-23-5Carbon tetrachloride
1.00 ug/L0.150 10.150 U 10/20/17 14:2010/20/17 11:55 108-90-7Chlorobenzene
1.00 ug/L0.260 10.260 U 10/20/17 14:2010/20/17 11:55 75-00-3Chloroethane
1.00 ug/L0.160 10.160 U 10/20/17 14:2010/20/17 11:55 67-66-3Chloroform
1.00 ug/L0.250 10.250 U 10/20/17 14:2010/20/17 11:55 74-87-3Chloromethane (Methyl Chloride)
1.00 ug/L0.210 10.210 U 10/20/17 14:2010/20/17 11:55 156-59-2cis-1,2-Dichloroethene
1.00 ug/L0.100 10.100 U 10/20/17 14:2010/20/17 11:55 10061-01-5cis-1,3-Dichloropropene
1.00 ug/L0.150 10.150 U 10/20/17 14:2010/20/17 11:55 124-48-1Dibromochloromethane
1.00 ug/L0.240 10.240 U 10/20/17 14:2010/20/17 11:55 74-95-3Dibromomethane
1.00 ug/L0.190 10.190 U 10/20/17 14:2010/20/17 11:55 100-41-4Ethylbenzene
1.00 ug/L0.310 10.310 U 10/20/17 14:2010/20/17 11:55 74-88-4Iodomethane (Methyl Iodide)
2.00 ug/L0.510 10.510 U 10/20/17 14:2010/20/17 11:55 179601-23-1m,p-Xylenes
1.00 ug/L0.420 10.420 U 10/20/17 14:2010/20/17 11:55 75-09-2Methylene Chloride
1.00 ug/L0.200 10.200 U 10/20/17 14:2010/20/17 11:55 95-47-6o-Xylene
1.00 ug/L0.180 10.180 U 10/20/17 14:2010/20/17 11:55 100-42-5Styrene
1.00 ug/L0.160 10.160 U 10/20/17 14:2010/20/17 11:55 127-18-4Tetrachloroethylene
Page 19 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 19 of 30
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 10/30/17 14:39
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Sample Results
(Continued)
ResultAnalyte MDL Date AnalyzedQual Units
Lab Sample ID: L7J0207-07 (Water)
Client Sample ID: TRIP BLANK (Continued)
RL Dil Date Prepared
Sampled: 10/17/17 0:00
CAS #
Appendix I Low Level VOCs by Method 8260B (Continued)
Analyst:JFLLaboratory:FTS - Florida
1.00 ug/L0.140 10.520 J 10/20/17 14:2010/20/17 11:55 108-88-3Toluene
1.00 ug/L0.200 10.460 J 10/20/17 14:2010/20/17 11:55 1330-20-7Total Xylenes
1.00 ug/L0.210 10.210 U 10/20/17 14:2010/20/17 11:55 156-60-5trans-1,2-Dichloroethene
1.00 ug/L0.110 10.110 U 10/20/17 14:2010/20/17 11:55 1006-10-26trans-1,3-Dichloropropene
1.00 ug/L0.190 10.190 U 10/20/17 14:2010/20/17 11:55 110-57-6trans-1,4-Dichloro-2-butene
1.00 ug/L0.190 10.190 U 10/20/17 14:2010/20/17 11:55 79-01-6Trichloroethylene
1.00 ug/L0.530 10.530 U 10/20/17 14:2010/20/17 11:55 75-69-4Trichlorofluoromethane
1.00 ug/L0.720 10.720 U 10/20/17 14:2010/20/17 11:55 108-05-4Vinyl acetate
1.00 ug/L0.190 10.190 U 10/20/17 14:2010/20/17 11:55 75-01-4Vinyl chloride
Surrogate: 1,2-Dichloroethane-D4 (SUR)53-15992%10/20/17 14:20 10706-07-0
Surrogate: 4-Bromofluorobenzene (SUR)30-18682%10/20/17 14:20 460-00-4
Surrogate: Toluene-D8 (SUR)70-13093%10/20/17 14:20 2037-26-5
VOCs by Method 8260B
Analyst:JFLLaboratory:FTS - Florida
5.00 ug/L0.236 10.236 U 10/20/17 14:2010/20/17 11:55 109-99-9Tetrahydrofuran
Page 20 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 20 of 30
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 10/30/17 14:39
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
VOCs by Method 8260B
MDL
Batch: B7J0252
Prepared & Analyzed: 10/20/2017Blank (B7J0252-BLK1)
5.00 ug/L0.236 U 0.236Tetrahydrofuran
Prepared & Analyzed: 10/20/2017LCS (B7J0252-BS1)
5.00 50.0 70-13075ug/L37.7 0.236Tetrahydrofuran
Prepared & Analyzed: 10/20/2017LCS Dup (B7J0252-BSD1)
5.00 50.0 2070-13077 2ug/L38.5 0.236Tetrahydrofuran
Page 21 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 21 of 30
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 10/30/17 14:39
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
(Continued)
Appendix I Low Level VOCs by Method 8260B
MDL
Batch: B7J0252
Prepared & Analyzed: 10/20/2017Blank (B7J0252-BLK1)
1.00 ug/L0.240 U 0.2401,1,1,2-Tetrachloroethane
1.00 ug/L0.160 U 0.1601,1,1-Trichloroethane
1.00 ug/L0.180 U 0.1801,1,2,2-Tetrachloroethane
1.00 ug/L0.250 U 0.2501,1,2-Trichloroethane
1.00 ug/L0.110 U 0.1101,1-Dichloroethane
1.00 ug/L0.200 U 0.2001,1-Dichloroethene
1.00 ug/L0.210 U 0.2101,2,3-Trichloropropane
1.00 ug/L0.190 U 0.1901,2-Dibromo-3-Chloropropane (DBCP)
1.00 ug/L0.180 U 0.1801,2-Dibromoethane (EDB)
1.00 ug/L0.140 U 0.1401,2-Dichlorobenzene
1.00 ug/L0.180 U 0.1801,2-Dichloroethane
1.00 ug/L0.150 U 0.1501,2-Dichloropropane
1.00 ug/L0.170 U 0.1701,4-Dichlorobenzene
2.00 ug/L0.280 U 0.2802-Butanone (MEK)
2.00 ug/L0.320 U 0.3202-Hexanone
2.00 ug/L0.260 U 0.2604-Methyl-2-pentanone (MIBK)
10.0 ug/L0.350 U 0.350Acetone
2.00 ug/L0.490 U 0.490Acrylonitrile
1.00 ug/L0.160 U 0.160Benzene
1.00 ug/L0.200 U 0.200Bromochloromethane
1.00 ug/L0.250 U 0.250Bromodichloromethane
1.00 ug/L0.170 U 0.170Bromoform
1.00 ug/L0.250 U 0.250Bromomethane (Methyl Bromide)
1.00 ug/L0.260 U 0.260Carbon disulfide
1.00 ug/L0.330 U 0.330Carbon tetrachloride
1.00 ug/L0.150 U 0.150Chlorobenzene
1.00 ug/L0.260 U 0.260Chloroethane
1.00 ug/L0.160 U 0.160Chloroform
1.00 ug/L0.250 U 0.250Chloromethane (Methyl Chloride)
1.00 ug/L0.210 U 0.210cis-1,2-Dichloroethene
1.00 ug/L0.100 U 0.100cis-1,3-Dichloropropene
1.00 ug/L0.150 U 0.150Dibromochloromethane
1.00 ug/L0.240 U 0.240Dibromomethane
1.00 ug/L0.190 U 0.190Ethylbenzene
1.00 ug/L0.310 U 0.310Iodomethane (Methyl Iodide)
2.00 ug/L0.510 U 0.510m,p-Xylenes
1.00 ug/L0.420 U 0.420Methylene Chloride
1.00 ug/L0.200 U 0.200o-Xylene
1.00 ug/L0.180 U 0.180Styrene
1.00 ug/L0.160 U 0.160Tetrachloroethylene
1.00 ug/L0.140 U 0.140Toluene
Page 22 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 22 of 30
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 10/30/17 14:39
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
(Continued)
Appendix I Low Level VOCs by Method 8260B (Continued)
MDL
Batch: B7J0252 (Continued)
Prepared & Analyzed: 10/20/2017Blank (B7J0252-BLK1)
1.00 ug/L0.200 U 0.200Total Xylenes
1.00 ug/L0.210 U 0.210trans-1,2-Dichloroethene
1.00 ug/L0.110 U 0.110trans-1,3-Dichloropropene
1.00 ug/L0.190 U 0.190trans-1,4-Dichloro-2-butene
1.00 ug/L0.190 U 0.190Trichloroethylene
1.00 ug/L0.530 U 0.530Trichlorofluoromethane
1.00 ug/L0.720 U 0.720Vinyl acetate
1.00 ug/L0.190 U 0.190Vinyl chloride
50.0 53-159Surrogate: 1,2-Dichloroethane-D4 (SUR)9447.1 ug/L
50.0 30-186Surrogate: 4-Bromofluorobenzene (SUR)8442.0 ug/L
50.0 70-130Surrogate: Toluene-D8 (SUR)9446.8 ug/L
Prepared & Analyzed: 10/20/2017LCS (B7J0252-BS1)
1.00 50.0 80-130105ug/L52.6 0.2401,1,1,2-Tetrachloroethane
1.00 50.0 65-130111ug/L55.4 0.1601,1,1-Trichloroethane
1.00 50.0 65-13073ug/L36.4 0.1801,1,2,2-Tetrachloroethane
1.00 50.0 75-12590ug/L44.9 0.2501,1,2-Trichloroethane
1.00 50.0 70-13588ug/L44.2 0.1101,1-Dichloroethane
1.00 50.0 70-13097ug/L48.7 0.2001,1-Dichloroethene
1.00 50.0 75-12578ug/L38.9 0.2101,2,3-Trichloropropane
1.00 50.0 50-13073ug/L36.4 0.1901,2-Dibromo-3-Chloropropane (DBCP)
1.00 50.0 80-120100ug/L49.8 0.1801,2-Dibromoethane (EDB)
1.00 50.0 70-120101ug/L50.7 0.1401,2-Dichlorobenzene
1.00 50.0 70-13098ug/L48.8 0.1801,2-Dichloroethane
1.00 50.0 75-12589ug/L44.3 0.1501,2-Dichloropropane
1.00 50.0 75-125105ug/L52.3 0.1701,4-Dichlorobenzene
2.00 100 30-15074ug/L74.0 0.2802-Butanone (MEK)
2.00 100 55-13077ug/L77.3 0.3202-Hexanone
2.00 100 60-13586ug/L85.8 0.2604-Methyl-2-pentanone (MIBK)
10.0 100 40-14072ug/L72.2 0.350Acetone
2.00 125 40-14071ug/L89.3 0.490Acrylonitrile
1.00 50.0 80-12095ug/L47.5 0.160Benzene
1.00 50.0 65-130114ug/L57.2 0.200Bromochloromethane
1.00 50.0 75-12089ug/L44.3 0.250Bromodichloromethane
1.00 50.0 70-13093ug/L46.6 0.170Bromoform
1.00 50.0 30-145102ug/L51.0 0.250Bromomethane (Methyl Bromide)
1.00 50.0 35-16083ug/L41.4 0.260Carbon disulfide
1.00 50.0 65-140111ug/L55.7 0.330Carbon tetrachloride
1.00 50.0 80-120106ug/L52.8 0.150Chlorobenzene
1.00 50.0 60-13584ug/L42.0 0.260Chloroethane
Page 23 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 23 of 30
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 10/30/17 14:39
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
(Continued)
Appendix I Low Level VOCs by Method 8260B (Continued)
MDL
Batch: B7J0252 (Continued)
Prepared & Analyzed: 10/20/2017LCS (B7J0252-BS1)
1.00 50.0 65-135105ug/L52.7 0.160Chloroform
1.00 50.0 40-12579ug/L39.5 0.250Chloromethane (Methyl Chloride)
1.00 50.0 70-125101ug/L50.7 0.210cis-1,2-Dichloroethene
1.00 50.0 70-13091ug/L45.7 0.100cis-1,3-Dichloropropene
1.00 50.0 60-135105ug/L52.3 0.150Dibromochloromethane
1.00 50.0 75-12595ug/L47.6 0.240Dibromomethane
1.00 50.0 75-12599ug/L49.4 0.190Ethylbenzene
1.00 50.0 65-130118ug/L59.2 0.310Iodomethane (Methyl Iodide)
2.00 100 75-130105ug/L1050.510m,p-Xylenes
1.00 50.0 55-140104ug/L52.1 0.420Methylene Chloride
1.00 50.0 80-120101ug/L50.6 0.200o-Xylene
1.00 50.0 65-135105ug/L52.3 0.180Styrene
1.00 50.0 45-150130ug/L64.9 0.160Tetrachloroethylene
1.00 50.0 75-12096ug/L48.0 0.140Toluene
1.00 50.0 60-140101ug/L50.4 0.210trans-1,2-Dichloroethene
1.00 50.0 55-14098ug/L48.9 0.110trans-1,3-Dichloropropene
1.00 50.0 65-135105ug/L52.5 0.190trans-1,4-Dichloro-2-butene
1.00 50.0 70-125106ug/L53.2 0.190Trichloroethylene
1.00 50.0 60-145103ug/L51.4 0.530Trichlorofluoromethane
1.00 50.0 65-13580ug/L40.2 0.720Vinyl acetate
1.00 50.0 50-14588ug/L43.8 0.190Vinyl chloride
50.0 53-159Surrogate: 1,2-Dichloroethane-D4 (SUR)9748.3 ug/L
50.0 30-186Surrogate: 4-Bromofluorobenzene (SUR)8843.9 ug/L
50.0 70-130Surrogate: Toluene-D8 (SUR)9849.0 ug/L
Prepared & Analyzed: 10/20/2017LCS Dup (B7J0252-BSD1)
1.00 50.0 2080-130102 3ug/L51.1 0.2401,1,1,2-Tetrachloroethane
1.00 50.0 2065-130103 7ug/L51.7 0.1601,1,1-Trichloroethane
1.00 50.0 2065-13074 1ug/L37.0 0.1801,1,2,2-Tetrachloroethane
1.00 50.0 2075-12587 3ug/L43.6 0.2501,1,2-Trichloroethane
1.00 50.0 2070-13585 4ug/L42.4 0.1101,1-Dichloroethane
1.00 50.0 2070-13094 3ug/L47.0 0.2001,1-Dichloroethene
1.00 50.0 2075-12578 0.6ug/L39.1 0.2101,2,3-Trichloropropane
1.00 50.0 2050-13072 1ug/L35.9 0.1901,2-Dibromo-3-Chloropropane (DBCP)
1.00 50.0 2080-12096 3ug/L48.2 0.1801,2-Dibromoethane (EDB)
1.00 50.0 2070-120102 0.08ug/L50.8 0.1401,2-Dichlorobenzene
1.00 50.0 2070-13095 3ug/L47.4 0.1801,2-Dichloroethane
1.00 50.0 2075-12586 3ug/L42.9 0.1501,2-Dichloropropane
1.00 50.0 2075-125100 4ug/L50.2 0.1701,4-Dichlorobenzene
2.00 100 2030-15071 4ug/L70.9 0.2802-Butanone (MEK)
Page 24 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 24 of 30
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 10/30/17 14:39
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
(Continued)
Appendix I Low Level VOCs by Method 8260B (Continued)
MDL
Batch: B7J0252 (Continued)
Prepared & Analyzed: 10/20/2017LCS Dup (B7J0252-BSD1)
2.00 100 2055-13077 0.2ug/L77.1 0.3202-Hexanone
2.00 100 2060-13587 2ug/L87.4 0.2604-Methyl-2-pentanone (MIBK)
10.0 100 2040-14072 0.06ug/L72.2 0.350Acetone
2.00 125 2040-14065 10ug/L81.1 0.490Acrylonitrile
1.00 50.0 2080-12090 5ug/L45.1 0.160Benzene
1.00 50.0 2065-130108 6ug/L54.0 0.200Bromochloromethane
1.00 50.0 2075-12085 4ug/L42.5 0.250Bromodichloromethane
1.00 50.0 2070-13095 1ug/L47.3 0.170Bromoform
1.00 50.0 2030-145101 0.9ug/L50.6 0.250Bromomethane (Methyl Bromide)
1.00 50.0 2035-16079 5ug/L39.5 0.260Carbon disulfide
1.00 50.0 2065-14099 12ug/L49.3 0.330Carbon tetrachloride
1.00 50.0 2080-120102 4ug/L50.8 0.150Chlorobenzene
1.00 50.0 2060-13579 6ug/L39.6 0.260Chloroethane
1.00 50.0 2065-135100 5ug/L50.1 0.160Chloroform
1.00 50.0 2040-12579 0.4ug/L39.4 0.250Chloromethane (Methyl Chloride)
1.00 50.0 2070-125100 1ug/L50.1 0.210cis-1,2-Dichloroethene
1.00 50.0 2070-13089 2ug/L44.7 0.100cis-1,3-Dichloropropene
1.00 50.0 2060-135103 2ug/L51.3 0.150Dibromochloromethane
1.00 50.0 2075-12595 0.7ug/L47.3 0.240Dibromomethane
1.00 50.0 2075-12595 4ug/L47.4 0.190Ethylbenzene
1.00 50.0 2065-130113 5ug/L56.4 0.310Iodomethane (Methyl Iodide)
2.00 100 2075-130100 4ug/L1000.510m,p-Xylenes
1.00 50.0 2055-140101 3ug/L50.5 0.420Methylene Chloride
1.00 50.0 2080-12099 2ug/L49.6 0.200o-Xylene
1.00 50.0 2065-135100 5ug/L50.0 0.180Styrene
1.00 50.0 2045-150129 0.4ug/L64.6 0.160Tetrachloroethylene
1.00 50.0 2075-12093 3ug/L46.3 0.140Toluene
1.00 50.0 2060-14099 2ug/L49.3 0.210trans-1,2-Dichloroethene
1.00 50.0 2055-14092 6ug/L46.2 0.110trans-1,3-Dichloropropene
1.00 50.0 2065-135100 5ug/L50.1 0.190trans-1,4-Dichloro-2-butene
1.00 50.0 2070-12599 7ug/L49.7 0.190Trichloroethylene
1.00 50.0 2060-14599 4ug/L49.6 0.530Trichlorofluoromethane
1.00 50.0 2065-13581 0.8ug/L40.5 0.720Vinyl acetate
1.00 50.0 2050-14582 7ug/L40.9 0.190Vinyl chloride
50.0 53-159Surrogate: 1,2-Dichloroethane-D4 (SUR)9447.1 ug/L
50.0 30-186Surrogate: 4-Bromofluorobenzene (SUR)8743.7 ug/L
50.0 70-130Surrogate: Toluene-D8 (SUR)9648.0 ug/L
Page 25 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 25 of 30
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 10/30/17 14:39
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
(Continued)
7 RCRA Metals by Method 6010C
MDL
Batch: B7J0276
Prepared: 10/23/2017 Analyzed: 10/24/2017Blank (B7J0276-BLK1)
0.0100 mg/L0.00400 U 0.00400Arsenic
0.0500 mg/L0.00200 U 0.00200Barium
0.00500 mg/L0.000300 U 0.000300Cadmium
0.0100 mg/L0.000300 U 0.000300Chromium
0.0100 mg/L0.00330 U 0.00330Lead
0.0500 mg/L0.0113 U 0.0113Selenium
0.0500 mg/L0.000600 U 0.000600Silver
Prepared: 10/23/2017 Analyzed: 10/24/2017LCS (B7J0276-BS1)
0.0100 1.00 80-120102mg/L1.02 0.00400Arsenic
0.0500 1.00 80-120102mg/L1.02 0.00200Barium
0.00500 1.00 80-120103mg/L1.03 0.000300Cadmium
0.0100 1.00 80-120103mg/L1.03 0.000300Chromium
0.0100 1.00 80-120103mg/L1.03 0.00330Lead
0.0500 1.00 80-120103mg/L1.03 0.0113Selenium
0.0500 1.00 80-120100mg/L0.997 0.000600Silver
Prepared: 10/23/2017 Analyzed: 10/24/2017LCS Dup (B7J0276-BSD1)
0.0100 1.00 2080-12099 3mg/L0.990 0.00400Arsenic
0.0500 1.00 2080-12099 3mg/L0.990 0.00200Barium
0.00500 1.00 2080-120101 3mg/L1.01 0.000300Cadmium
0.0100 1.00 2080-120100 3mg/L1.00 0.000300Chromium
0.0100 1.00 2080-12099 3mg/L0.993 0.00330Lead
0.0500 1.00 2080-120101 2mg/L1.01 0.0113Selenium
0.0500 1.00 2080-120100 0.6mg/L1.00 0.000600Silver
Prepared: 10/23/2017 Analyzed: 10/24/2017Source: L7J0207-02Duplicate (B7J0276-DUP1)
0.0100 0.00412 20mg/L0.00400 U 0.00400Arsenic
0.0500 0.0397 202mg/L0.0389 J 0.00200Barium
0.00500 ND 20mg/L0.000300 U 0.000300Cadmium
0.0100 ND 20mg/L0.000300 U 0.000300Chromium
0.0100 ND 20mg/L0.00330 U 0.00330Lead
0.0500 ND 20mg/L0.0113 U 0.0113Selenium
0.0500 ND 20mg/L0.000600 U 0.000600Silver
Page 26 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 26 of 30
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 10/30/17 14:39
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
(Continued)
7 RCRA Metals by Method 6010C (Continued)
MDL
Batch: B7J0276 (Continued)
Prepared: 10/23/2017 Analyzed: 10/24/2017Source: L7J0207-02Matrix Spike (B7J0276-MS1)
0.0100 1.00 0.00412 80-12098mg/L0.983 0.00400Arsenic
0.0500 1.00 0.0397 80-12099mg/L1.03 0.00200Barium
0.00500 1.00 ND 80-120101mg/L1.01 0.000300Cadmium
0.0100 1.00 ND 80-120100mg/L1.00 0.000300Chromium
0.0100 1.00 ND 80-12099mg/L0.995 0.00330Lead
0.0500 1.00 ND 80-120100mg/L1.00 0.0113Selenium
0.0500 1.00 ND 80-120100mg/L1.00 0.000600Silver
Prepared: 10/23/2017 Analyzed: 10/24/2017Source: L7J0207-02Matrix Spike Dup (B7J0276-MSD1)
0.0100 1.00 0.00412 2080-12097 0.6mg/L0.977 0.00400Arsenic
0.0500 1.00 0.0397 2080-12098 1mg/L1.02 0.00200Barium
0.00500 1.00 ND 2080-12099 1mg/L0.993 0.000300Cadmium
0.0100 1.00 ND 2080-120100 0.9mg/L0.995 0.000300Chromium
0.0100 1.00 ND 2080-12098 1mg/L0.985 0.00330Lead
0.0500 1.00 ND 2080-12099 0.7mg/L0.994 0.0113Selenium
0.0500 1.00 ND 2080-120100 0.5mg/L1.00 0.000600Silver
Page 27 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 27 of 30
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 10/30/17 14:39
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
Result RL Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitQual Analyte
Quality Control
(Continued)
Total Mercury Analysis by Method 7470A
MDL
Batch: B7J0305
Prepared: 10/24/2017 Analyzed: 10/25/2017Blank (B7J0305-BLK1)
0.000200 mg/L0.0000700 U 0.0000700Mercury
Prepared: 10/24/2017 Analyzed: 10/25/2017LCS (B7J0305-BS1)
0.000200 0.00300 85-115101mg/L0.00303 0.0000700Mercury
Prepared: 10/24/2017 Analyzed: 10/25/2017LCS Dup (B7J0305-BSD1)
0.000200 0.00300 2085-11597 4mg/L0.00290 0.0000700Mercury
Prepared: 10/24/2017 Analyzed: 10/25/2017Source: A7J0035-16Duplicate (B7J0305-DUP1)
0.000200 ND 20mg/L0.0000700 U 0.0000700Mercury
Page 28 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 28 of 30
Project:
Project Number:
Project Manager:
Reported:
Terraquest Environmental Consultants-Mebane
100 E. Ruffin Street
Lee County Landfill
02296
Ryan Kerins 10/30/17 14:39
MWBE SDBE
NELAC DoD Accredited
Mebane, NC 27302
List of Certifications for FTS - Florida
CodeDescriptionNumber ExpiresFacility
LANELAC04176LA Atlanta Lab CERTIFICATE 12/31/2017FTSA
ANC483North Carolina ONLY CERT 12/31/2017FTSL
LFLNELACE84098FL MICROBIOLOGY Lakeland CERT 06/30/2018FTSL
FLNELACE871002Xenco FL CERT 06/30/2018FTSL
AFLNELACE87429FL NELAC CERT Tampa 06/30/2018FTSL
DODLI0-135 DoD CERTIFICATE 11/28/2017FTSL
USDAP330-07-00105 USDA CERTIFICATE FTSL
Notes and Definitions
Item Definition
Dry Sample results reported on a dry weight basis.
U Analyte NOT DETECTED at or above the reporting limit.
A Suspected adol-condensation product.
B Analyte detected in the method blank.
C Confirmed by GC/MS analysis.
E Concentration exceeds calibration range.
K Hold Time exceeded.
N Tentatively Identified Compound.
P >25% difference between primary and secondary columns.
S Quantitation based on single-point calibration.
X General QC Failure see Case Narrative.
J The target analyte was positively identified below the Reporting Limit and above the Method Detection Limit.
RPD Relative Percent Difference
%REC Percent Recovery
Source Sample that was matrix spiked or duplicated.
Page 29 of 30
The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.
No duplication of this report is allowed, except in its entirety.Page 29 of 30
Page 30 of 30
 TECHNICAL METHODS/STANDARD PROCEDURES 

Groundwater Sampling 

Groundwater samples are collected from temporary or permanent monitoring wells according to 
established sampling protocol.  When multiple monitoring wells or sampling points are sampled, 
sampling is completed beginning with the least contaminated well to the most contaminated well, 
if it is known.  When permanent monitoring wells for petroleum sites are sampled, the well is 
purged of a minimum of three well‐bore volumes prior to sample collection in order to assure that 
sampled water is representative of aquifer conditions.  In temporary wells, the first water which 
migrates into the open borehole is sampled.  Samples from both temporary and permanent 
monitoring wells are collected using individually wrapped disposable polyethylene bailers by field 
personnel wearing disposable nitrile gloves.  Only one well is sampled with a given bailer in order to 
prevent sample cross‐contamination.  During both well purging and sampling, proper protective 
clothing and equipment is used and is dependent upon the type and level of contaminants present. 
Also, field personnel change gloves between different samples to reduce the chance of cross‐
contamination. Water samples are transferred from the bailer to laboratory‐prepared sampling 
containers using slow emptying devices to reduce the chance of contamination loss through 
volatilization.  Preservatives, such as acids, are provided by the laboratory in pre‐prepared 
containers in which collected samples are placed if in‐field preservation is necessary.  The samples 
are labeled with the project name, project number, sample identification, required analysis, and 
date and time of collection.  The samples are placed on ice, shipped to a certified laboratory, and 
analyzed before the expiration of an analytical method’s prescribed holding time.  Chain‐of‐custody 
documentation is maintained for each sample collected in the field.   

Surface Water Sampling 

Surface water samples, specifically samples from creeks or streams, are collected from a 
moving/flowing portion of the creek or stream to ensure that stagnant water is not collected.  Field 
personnel are careful to collect samples from flowing areas that are not so turbulent as to cause a 
loss of volatile contaminants which might have been contained in the creek’s/stream’s water.  
Samples are collected by field personnel wearing disposable nitrile gloves.  Field personnel change 
gloves between different locations to reduce the chance of cross‐contamination.  Samples are 
collected directly from the appropriate creek or stream location and placed into the appropriate 
laboratory‐prepared containers.  Preservatives, such as acids, are provided by the laboratory in pre‐
prepared containers in which collected samples are placed if in‐field preservation is necessary. The 
samples are labeled with the project name, project number, sample identification, required 
analysis, and date and time of collection.  The samples are cooled on ice to approximately four 
degrees centigrade, shipped to a certified laboratory, and analyzed before the expiration of an 
analytical method’s prescribed holding time.  Chain‐of‐custody documentation is maintained for 
each sample collected in the field.    

Field Measurements 

Field measurements taken to determine the pH, conductivity, temperature, and dissolved oxygen 
concentration of a particular groundwater sample are taken directly after a particular monitoring 
well has been adequately purged.  This ensures that the groundwater parameter data collected is 
representative of the aquifer conditions at a given location.  Once purging of the monitoring well is 
complete, the decontaminated probe head and cord of the appropriate unit is lowered into the 
required monitoring well.  If the depth to water in a specific monitoring well is greater than the 
length of cord for a particular unit, a new, disposable bailer is slowly lowered into the appropriate 
monitoring well and a representative groundwater sample is retrieved.  A slow pouring device is 
fitted onto the end of the disposable bailer and the sample is slowly poured into a new, disposable 
plastic cup.  Groundwater parameter data are then collected from the groundwater in the cup 
using the required unit.   

For pH, conductivity, and temperature, a Hanna Instruments Model 991300 portable meter is 
utilized.  This unit is periodically calibrated and maintained in accordance with the unit’s operations 
manual by field personnel.  Prior to data collection, the unit is properly decontaminated to prevent 
cross‐contamination.  The unit is decontaminated between each sample.  The procedure used for 
sample measurement involves lowering the meter’s probe into the new, disposable cup containing 
the groundwater sample to be measured and slowly stirring the probe to force groundwater across 
the probe’s membrane.  The measurements displayed by the meter are then recorded.   

For dissolved oxygen concentration measurements, a YSI® Model 55 Handheld Dissolved Oxygen 
System is utilized.  This unit is periodically calibrated and maintained in accordance with the unit’s 
operations manual by field personnel.  Prior to data collection, the unit is properly decontaminated 
to prevent cross‐contamination.  The unit is decontaminated between each sample.  The procedure 
used for sample measurement involves adjusting the unit for the correct altitude where the 
sampling will take place and adjusting the reported units desired.  Once this is done, the unit’s 
probe is inserted into the groundwater sample to be measured and the probe is slowly stirred to 
force the groundwater across the probe’s membrane.  The measurements displayed by the unit are 
then recorded.