5601_McDowellCountyMSWLFPaceProject_SampleReport_20170914

#=CL#
September 14, 2017
LIMS USE: FR - RANDELL THOMAS
LIMS OBJECT ID: 92353331
92353331
Project:
Pace Project No.:
RE:
Mr. Randell Thomas
McDowell County Landfill
60 East Court St
Marion, NC 28752
LANDFILL MW'S 8/29
Dear Mr. Thomas:
Enclosed are the analytical results for sample(s) received by the laboratory on August 30, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 44
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 44
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Lab ID Sample ID Matrix Date Collected Date Received
92353331001 MW-1 Water 08/29/17 13:00 08/30/17 08:20
92353331002 MW-2 Water 08/29/17 14:15 08/30/17 08:20
92353331003 MW-3 Water 08/29/17 13:30 08/30/17 08:20
92353331004 MW-4 Water 08/29/17 13:45 08/30/17 08:20
92353331005 TVL BLK Water 08/29/17 08:00 08/30/17 08:20
92353331006 EQUIP BLK Water 08/29/17 12:30 08/30/17 08:20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 44
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92353331001 MW-1 EPA 6010 15 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8260 63 PASI-CGAW
92353331002 MW-2 EPA 6010 15 PASI-ASH1
EPA 7470 1 PASI-AKAL
EPA 8260 63 PASI-CGAW
92353331003 MW-3 EPA 6010 15 PASI-ASH1
EPA 7470 1 PASI-AKAL
EPA 8260 63 PASI-CGAW
92353331004 MW-4 EPA 6010 15 PASI-ASH1
EPA 7470 1 PASI-AKAL
EPA 8260 63 PASI-CGAW
92353331005 TVL BLK EPA 8260 63 PASI-CZDO
92353331006 EQUIP BLK EPA 6010 15 PASI-ASH1
EPA 7470 1 PASI-AKAL
EPA 8260 63 PASI-CZDO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Sample:MW-1 Lab ID:92353331001 Collected:08/29/17 13:00 Received:08/30/17 08:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Mark
Swann 08/31/17 09:271
Collected Date 8/29/17 08/31/17 09:271
Collected Time 13:00 08/31/17 09:271
Field pH 5.1 Std. Units 08/31/17 09:270.10 0.10 1
Field Temperature 21.6 deg C 08/31/17 09:270.50 0.50 1
Static Water Level 20.89 feet 08/31/17 09:271
Field Specific Conductance 425 umhos/cm 08/31/17 09:271.0 1.0 1
Turbidity 5.69 NTU 08/31/17 09:271.0 1.0 1
Odor No odor 08/31/17 09:271
Appearance Clear 08/31/17 09:271
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony 3.9U ug/L 09/14/17 03:16 7440-36-009/12/17 21:255.0 3.9 1
Arsenic 5.0U ug/L 09/14/17 03:16 7440-38-209/12/17 21:2510.0 5.0 1
Barium 172 ug/L 09/14/17 03:16 7440-39-309/12/17 21:255.0 2.5 1
Beryllium 0.50U ug/L 09/14/17 03:16 7440-41-709/12/17 21:251.0 0.50 1
Cadmium 0.50U ug/L 09/14/17 03:16 7440-43-909/12/17 21:251.0 0.50 1
Chromium 2.5U ug/L 09/14/17 03:16 7440-47-309/12/17 21:255.0 2.5 1
Cobalt 2.5U ug/L 09/14/17 03:16 7440-48-409/12/17 21:255.0 2.5 1
Copper 2.5U ug/L 09/14/17 03:16 7440-50-809/12/17 21:255.0 2.5 1
Lead 2.5U ug/L 09/14/17 03:16 7439-92-109/12/17 21:255.0 2.5 1
Nickel 2.5U ug/L 09/14/17 03:16 7440-02-009/12/17 21:255.0 2.5 1
Selenium 6.9J ug/L 09/14/17 03:16 7782-49-209/12/17 21:2510.0 5.0 1
Silver 2.5U ug/L 09/14/17 03:16 7440-22-409/12/17 21:255.0 2.5 1
Thallium 5.0U ug/L 09/14/17 03:16 7440-28-009/12/17 21:2510.0 5.0 1
Vanadium 2.5U ug/L 09/14/17 03:16 7440-62-209/12/17 21:255.0 2.5 1
Zinc 9.5J ug/L 09/14/17 03:16 7440-66-609/12/17 21:2510.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 0.10U ug/L 09/12/17 14:54 7439-97-609/11/17 14:500.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 10.0U ug/L 09/02/17 06:03 67-64-125.0 10.0 1
Benzene 0.25U ug/L 09/02/17 06:03 71-43-21.0 0.25 1
Bromobenzene 0.30U ug/L 09/02/17 06:03 108-86-11.0 0.30 1
Bromochloromethane 0.17U ug/L 09/02/17 06:03 74-97-51.0 0.17 1
Bromodichloromethane 0.18U ug/L 09/02/17 06:03 75-27-41.0 0.18 1
Bromoform 0.26U ug/L 09/02/17 06:03 75-25-21.0 0.26 1
Bromomethane 0.29U ug/L 09/02/17 06:03 74-83-92.0 0.29 1
2-Butanone (MEK)0.96U ug/L 09/02/17 06:03 78-93-35.0 0.96 1
Carbon tetrachloride 0.25U ug/L 09/02/17 06:03 56-23-51.0 0.25 1
Chlorobenzene 0.23U ug/L 09/02/17 06:03 108-90-71.0 0.23 1
Chloroethane 0.54U ug/L 09/02/17 06:03 75-00-31.0 0.54 1
Chloroform 0.14U ug/L 09/02/17 06:03 67-66-31.0 0.14 1
Chloromethane 0.11U ug/L 09/02/17 06:03 74-87-31.0 0.11 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Sample:MW-1 Lab ID:92353331001 Collected:08/29/17 13:00 Received:08/30/17 08:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level Landfill
2-Chlorotoluene 0.35U ug/L 09/02/17 06:03 95-49-81.0 0.35 1
4-Chlorotoluene 0.31U ug/L 09/02/17 06:03 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane 2.0U ug/L 09/02/17 06:03 96-12-82.0 2.0 1
Dibromochloromethane 0.21U ug/L 09/02/17 06:03 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)0.27U ug/L 09/02/17 06:03 106-93-41.0 0.27 1
Dibromomethane 0.21U ug/L 09/02/17 06:03 74-95-31.0 0.21 1
1,2-Dichlorobenzene 0.30U ug/L 09/02/17 06:03 95-50-11.0 0.30 1
1,3-Dichlorobenzene 0.24U ug/L 09/02/17 06:03 541-73-11.0 0.24 1
1,4-Dichlorobenzene 0.33U ug/L 09/02/17 06:03 106-46-71.0 0.33 1
Dichlorodifluoromethane 0.21U ug/L 09/02/17 06:03 75-71-81.0 0.21 1
1,1-Dichloroethane 0.32U ug/L 09/02/17 06:03 75-34-31.0 0.32 1
1,2-Dichloroethane 0.24U ug/L 09/02/17 06:03 107-06-21.0 0.24 1
1,1-Dichloroethene 0.56U ug/L 09/02/17 06:03 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 0.19U ug/L 09/02/17 06:03 156-59-21.0 0.19 1
trans-1,2-Dichloroethene 0.49U ug/L 09/02/17 06:03 156-60-51.0 0.49 1
1,2-Dichloropropane 0.27U ug/L 09/02/17 06:03 78-87-51.0 0.27 1
1,3-Dichloropropane 0.28U ug/L 09/02/17 06:03 142-28-91.0 0.28 1
2,2-Dichloropropane 0.13U ug/L 09/02/17 06:03 594-20-71.0 0.13 1
1,1-Dichloropropene 0.49U ug/L 09/02/17 06:03 563-58-61.0 0.49 1
cis-1,3-Dichloropropene 0.13U ug/L 09/02/17 06:03 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene 0.26U ug/L 09/02/17 06:03 10061-02-61.0 0.26 1
Diisopropyl ether 0.12U ug/L 09/02/17 06:03 108-20-31.0 0.12 1
Ethylbenzene 0.30U ug/L 09/02/17 06:03 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene 0.71U ug/L 09/02/17 06:03 87-68-31.0 0.71 1
2-Hexanone 0.46U ug/L 09/02/17 06:03 591-78-65.0 0.46 1
p-Isopropyltoluene 0.31U ug/L 09/02/17 06:03 99-87-61.0 0.31 1
Methylene Chloride 0.97U ug/L 09/02/17 06:03 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)0.33U ug/L 09/02/17 06:03 108-10-15.0 0.33 1
Methyl-tert-butyl ether 0.21U ug/L 09/02/17 06:03 1634-04-41.0 0.21 1
Naphthalene 0.24U ug/L 09/02/17 06:03 91-20-31.0 0.24 1
Styrene 0.26U ug/L 09/02/17 06:03 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane 0.33U ug/L 09/02/17 06:03 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane 0.40U ug/L 09/02/17 06:03 79-34-51.0 0.40 1
Tetrachloroethene 0.46U ug/L 09/02/17 06:03 127-18-41.0 0.46 1
Toluene 0.26U ug/L 09/02/17 06:03 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene 0.33U ug/L 09/02/17 06:03 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene 0.35U ug/L 09/02/17 06:03 120-82-11.0 0.35 1
1,1,1-Trichloroethane 0.48U ug/L 09/02/17 06:03 71-55-61.0 0.48 1
1,1,2-Trichloroethane 0.29U ug/L 09/02/17 06:03 79-00-51.0 0.29 1
Trichloroethene 0.47U ug/L 09/02/17 06:03 79-01-61.0 0.47 1
Trichlorofluoromethane 0.20U ug/L 09/02/17 06:03 75-69-41.0 0.20 1
1,2,3-Trichloropropane 0.41U ug/L 09/02/17 06:03 96-18-41.0 0.41 1
Vinyl acetate 0.35U ug/L 09/02/17 06:03 108-05-42.0 0.35 1
Vinyl chloride 0.62U ug/L 09/02/17 06:03 75-01-41.0 0.62 1
Xylene (Total)0.66U ug/L 09/02/17 06:03 1330-20-71.0 0.66 1
m&p-Xylene 0.66U ug/L 09/02/17 06:03 179601-23-12.0 0.66 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Sample:MW-1 Lab ID:92353331001 Collected:08/29/17 13:00 Received:08/30/17 08:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level Landfill
o-Xylene 0.23U ug/L 09/02/17 06:03 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)104 %09/02/17 06:03 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %09/02/17 06:03 17060-07-070-130 1
Toluene-d8 (S)106 %09/02/17 06:03 2037-26-570-130 1
Sample:MW-2 Lab ID:92353331002 Collected:08/29/17 14:15 Received:08/30/17 08:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Mark
Swann 08/31/17 09:291
Collected Date 8/29/17 08/31/17 09:291
Collected Time 14:15 08/31/17 09:291
Field pH 5.9 Std. Units 08/31/17 09:290.10 0.10 1
Field Temperature 16.9 deg C 08/31/17 09:290.50 0.50 1
Static Water Level 40.21 feet 08/31/17 09:291
Field Specific Conductance 714 umhos/cm 08/31/17 09:291.0 1.0 1
Turbidity 10.00 NTU 08/31/17 09:291.0 1.0 1
Odor Organic
odor 08/31/17 09:291
Appearance Clear 08/31/17 09:291
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony 3.9U ug/L 09/14/17 03:25 7440-36-009/12/17 21:255.0 3.9 1
Arsenic 5.0U ug/L 09/14/17 03:25 7440-38-209/12/17 21:2510.0 5.0 1
Barium 164 ug/L 09/14/17 03:25 7440-39-309/12/17 21:255.0 2.5 1
Beryllium 0.50U ug/L 09/14/17 03:25 7440-41-709/12/17 21:251.0 0.50 1
Cadmium 0.50U ug/L 09/14/17 03:25 7440-43-909/12/17 21:251.0 0.50 1
Chromium 3.6J ug/L 09/14/17 03:25 7440-47-309/12/17 21:255.0 2.5 1
Cobalt 22.0 ug/L 09/14/17 03:25 7440-48-409/12/17 21:255.0 2.5 1
Copper 2.5U ug/L 09/14/17 03:25 7440-50-809/12/17 21:255.0 2.5 1
Lead 3.8J ug/L 09/14/17 03:25 7439-92-109/12/17 21:255.0 2.5 1
Nickel 7.0 ug/L 09/14/17 03:25 7440-02-009/12/17 21:255.0 2.5 1
Selenium 5.0U ug/L 09/14/17 03:25 7782-49-209/12/17 21:2510.0 5.0 1
Silver 2.5U ug/L 09/14/17 03:25 7440-22-409/12/17 21:255.0 2.5 1
Thallium 5.0J ug/L 09/14/17 03:25 7440-28-009/12/17 21:2510.0 5.0 1
Vanadium 17.9 ug/L 09/14/17 03:25 7440-62-209/12/17 21:255.0 2.5 1
Zinc 12.0 ug/L 09/14/17 03:25 7440-66-609/12/17 21:2510.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 0.10U ug/L 09/07/17 02:24 7439-97-609/06/17 02:100.20 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Sample:MW-2 Lab ID:92353331002 Collected:08/29/17 14:15 Received:08/30/17 08:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 10.0U ug/L 09/02/17 06:21 67-64-125.0 10.0 1
Benzene 1.7 ug/L 09/02/17 06:21 71-43-21.0 0.25 1
Bromobenzene 0.30U ug/L 09/02/17 06:21 108-86-11.0 0.30 1
Bromochloromethane 0.17U ug/L 09/02/17 06:21 74-97-51.0 0.17 1
Bromodichloromethane 0.18U ug/L 09/02/17 06:21 75-27-41.0 0.18 1
Bromoform 0.26U ug/L 09/02/17 06:21 75-25-21.0 0.26 1
Bromomethane 0.29U ug/L 09/02/17 06:21 74-83-92.0 0.29 1
2-Butanone (MEK)0.96U ug/L 09/02/17 06:21 78-93-35.0 0.96 1
Carbon tetrachloride 0.25U ug/L 09/02/17 06:21 56-23-51.0 0.25 1
Chlorobenzene 4.4 ug/L 09/02/17 06:21 108-90-71.0 0.23 1
Chloroethane 0.90J ug/L 09/02/17 06:21 75-00-31.0 0.54 1
Chloroform 0.14U ug/L 09/02/17 06:21 67-66-31.0 0.14 1
Chloromethane 0.11U ug/L 09/02/17 06:21 74-87-31.0 0.11 1
2-Chlorotoluene 0.35U ug/L 09/02/17 06:21 95-49-81.0 0.35 1
4-Chlorotoluene 0.31U ug/L 09/02/17 06:21 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane 2.0U ug/L 09/02/17 06:21 96-12-82.0 2.0 1
Dibromochloromethane 0.21U ug/L 09/02/17 06:21 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)0.27U ug/L 09/02/17 06:21 106-93-41.0 0.27 1
Dibromomethane 0.21U ug/L 09/02/17 06:21 74-95-31.0 0.21 1
1,2-Dichlorobenzene 1.9 ug/L 09/02/17 06:21 95-50-11.0 0.30 1
1,3-Dichlorobenzene 0.24U ug/L 09/02/17 06:21 541-73-11.0 0.24 1
1,4-Dichlorobenzene 6.4 ug/L 09/02/17 06:21 106-46-71.0 0.33 1
Dichlorodifluoromethane 0.21U ug/L 09/02/17 06:21 75-71-81.0 0.21 1
1,1-Dichloroethane 0.85J ug/L 09/02/17 06:21 75-34-31.0 0.32 1
1,2-Dichloroethane 0.36J ug/L 09/02/17 06:21 107-06-21.0 0.24 1
1,1-Dichloroethene 0.56U ug/L 09/02/17 06:21 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 20.3 ug/L 09/02/17 06:21 156-59-21.0 0.19 1
trans-1,2-Dichloroethene 0.49U ug/L 09/02/17 06:21 156-60-51.0 0.49 1
1,2-Dichloropropane 0.27U ug/L 09/02/17 06:21 78-87-51.0 0.27 1
1,3-Dichloropropane 0.28U ug/L 09/02/17 06:21 142-28-91.0 0.28 1
2,2-Dichloropropane 0.13U ug/L 09/02/17 06:21 594-20-71.0 0.13 1
1,1-Dichloropropene 0.49U ug/L 09/02/17 06:21 563-58-61.0 0.49 1
cis-1,3-Dichloropropene 0.13U ug/L 09/02/17 06:21 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene 0.26U ug/L 09/02/17 06:21 10061-02-61.0 0.26 1
Diisopropyl ether 0.97J ug/L 09/02/17 06:21 108-20-31.0 0.12 1
Ethylbenzene 0.30U ug/L 09/02/17 06:21 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene 0.71U ug/L 09/02/17 06:21 87-68-31.0 0.71 1
2-Hexanone 0.46U ug/L 09/02/17 06:21 591-78-65.0 0.46 1
p-Isopropyltoluene 0.31U ug/L 09/02/17 06:21 99-87-61.0 0.31 1
Methylene Chloride 0.97U ug/L 09/02/17 06:21 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)0.33U ug/L 09/02/17 06:21 108-10-15.0 0.33 1
Methyl-tert-butyl ether 0.84J ug/L 09/02/17 06:21 1634-04-41.0 0.21 1
Naphthalene 0.24U ug/L 09/02/17 06:21 91-20-31.0 0.24 1
Styrene 0.26U ug/L 09/02/17 06:21 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane 0.33U ug/L 09/02/17 06:21 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane 0.40U ug/L 09/02/17 06:21 79-34-51.0 0.40 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Sample:MW-2 Lab ID:92353331002 Collected:08/29/17 14:15 Received:08/30/17 08:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level Landfill
Tetrachloroethene 0.46U ug/L 09/02/17 06:21 127-18-41.0 0.46 1
Toluene 0.26U ug/L 09/02/17 06:21 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene 0.33U ug/L 09/02/17 06:21 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene 0.61J ug/L 09/02/17 06:21 120-82-11.0 0.35 1
1,1,1-Trichloroethane 0.48U ug/L 09/02/17 06:21 71-55-61.0 0.48 1
1,1,2-Trichloroethane 0.29U ug/L 09/02/17 06:21 79-00-51.0 0.29 1
Trichloroethene 0.47U ug/L 09/02/17 06:21 79-01-61.0 0.47 1
Trichlorofluoromethane 0.20U ug/L 09/02/17 06:21 75-69-41.0 0.20 1
1,2,3-Trichloropropane 0.41U ug/L 09/02/17 06:21 96-18-41.0 0.41 1
Vinyl acetate 0.35U ug/L 09/02/17 06:21 108-05-42.0 0.35 1
Vinyl chloride 1.3 ug/L 09/02/17 06:21 75-01-41.0 0.62 1
Xylene (Total)0.66U ug/L 09/02/17 06:21 1330-20-71.0 0.66 1
m&p-Xylene 0.66U ug/L 09/02/17 06:21 179601-23-12.0 0.66 1
o-Xylene 0.23U ug/L 09/02/17 06:21 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)102 %09/02/17 06:21 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %09/02/17 06:21 17060-07-070-130 1
Toluene-d8 (S)103 %09/02/17 06:21 2037-26-570-130 1
Sample:MW-3 Lab ID:92353331003 Collected:08/29/17 13:30 Received:08/30/17 08:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Mark
Swann
08/31/17 09:301
Collected Date 8/29/17 08/31/17 09:301
Collected Time 13:30 08/31/17 09:301
Field pH 5.9 Std. Units 08/31/17 09:300.10 0.10 1
Field Temperature 17.4 deg C 08/31/17 09:300.50 0.50 1
Static Water Level 44.98 feet 08/31/17 09:301
Field Specific Conductance 724 umhos/cm 08/31/17 09:301.0 1.0 1
Turbidity 102.5 NTU 08/31/17 09:301.0 1.0 1
Odor No odor 08/31/17 09:301
Appearance Cloudy
w/finesolids
08/31/17 09:301
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony 3.9U ug/L 09/14/17 03:28 7440-36-009/12/17 21:255.0 3.9 1
Arsenic 5.0U ug/L 09/14/17 03:28 7440-38-209/12/17 21:2510.0 5.0 1
Barium 810 ug/L 09/14/17 03:28 7440-39-309/12/17 21:255.0 2.5 1
Beryllium 0.90J ug/L 09/14/17 03:28 7440-41-709/12/17 21:251.0 0.50 1
Cadmium 0.50U ug/L 09/14/17 03:28 7440-43-909/12/17 21:251.0 0.50 1
Chromium 2.5U ug/L 09/14/17 03:28 7440-47-309/12/17 21:255.0 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Sample:MW-3 Lab ID:92353331003 Collected:08/29/17 13:30 Received:08/30/17 08:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Cobalt 4.8J ug/L 09/14/17 03:28 7440-48-409/12/17 21:255.0 2.5 1
Copper 2.5U ug/L 09/14/17 03:28 7440-50-809/12/17 21:255.0 2.5 1
Lead 2.5U ug/L 09/14/17 03:28 7439-92-109/12/17 21:255.0 2.5 1
Nickel 2.7J ug/L 09/14/17 03:28 7440-02-009/12/17 21:255.0 2.5 1
Selenium 5.0U ug/L 09/14/17 03:28 7782-49-209/12/17 21:2510.0 5.0 1
Silver 2.5U ug/L 09/14/17 03:28 7440-22-409/12/17 21:255.0 2.5 1
Thallium 5.0U ug/L 09/14/17 03:28 7440-28-009/12/17 21:2510.0 5.0 1
Vanadium 4.2J ug/L 09/14/17 03:28 7440-62-209/12/17 21:255.0 2.5 1
Zinc 18.2 ug/L 09/14/17 03:28 7440-66-609/12/17 21:2510.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 0.10U ug/L 09/07/17 02:26 7439-97-609/06/17 02:100.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 10.0U ug/L 09/02/17 06:39 67-64-125.0 10.0 1
Benzene 0.25U ug/L 09/02/17 06:39 71-43-21.0 0.25 1
Bromobenzene 0.30U ug/L 09/02/17 06:39 108-86-11.0 0.30 1
Bromochloromethane 0.17U ug/L 09/02/17 06:39 74-97-51.0 0.17 1
Bromodichloromethane 0.18U ug/L 09/02/17 06:39 75-27-41.0 0.18 1
Bromoform 0.26U ug/L 09/02/17 06:39 75-25-21.0 0.26 1
Bromomethane 0.29U ug/L 09/02/17 06:39 74-83-92.0 0.29 1
2-Butanone (MEK)0.96U ug/L 09/02/17 06:39 78-93-35.0 0.96 1
Carbon tetrachloride 0.25U ug/L 09/02/17 06:39 56-23-51.0 0.25 1
Chlorobenzene 0.23U ug/L 09/02/17 06:39 108-90-71.0 0.23 1
Chloroethane 0.54U ug/L 09/02/17 06:39 75-00-31.0 0.54 1
Chloroform 0.14U ug/L 09/02/17 06:39 67-66-31.0 0.14 1
Chloromethane 0.11U ug/L 09/02/17 06:39 74-87-31.0 0.11 1
2-Chlorotoluene 0.35U ug/L 09/02/17 06:39 95-49-81.0 0.35 1
4-Chlorotoluene 0.31U ug/L 09/02/17 06:39 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane 2.0U ug/L 09/02/17 06:39 96-12-82.0 2.0 1
Dibromochloromethane 0.21U ug/L 09/02/17 06:39 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)0.27U ug/L 09/02/17 06:39 106-93-41.0 0.27 1
Dibromomethane 0.21U ug/L 09/02/17 06:39 74-95-31.0 0.21 1
1,2-Dichlorobenzene 0.30U ug/L 09/02/17 06:39 95-50-11.0 0.30 1
1,3-Dichlorobenzene 0.24U ug/L 09/02/17 06:39 541-73-11.0 0.24 1
1,4-Dichlorobenzene 0.33U ug/L 09/02/17 06:39 106-46-71.0 0.33 1
Dichlorodifluoromethane 0.21U ug/L 09/02/17 06:39 75-71-81.0 0.21 1
1,1-Dichloroethane 0.32U ug/L 09/02/17 06:39 75-34-31.0 0.32 1
1,2-Dichloroethane 0.24U ug/L 09/02/17 06:39 107-06-21.0 0.24 1
1,1-Dichloroethene 0.56U ug/L 09/02/17 06:39 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 0.19U ug/L 09/02/17 06:39 156-59-21.0 0.19 1
trans-1,2-Dichloroethene 0.49U ug/L 09/02/17 06:39 156-60-51.0 0.49 1
1,2-Dichloropropane 0.27U ug/L 09/02/17 06:39 78-87-51.0 0.27 1
1,3-Dichloropropane 0.28U ug/L 09/02/17 06:39 142-28-91.0 0.28 1
2,2-Dichloropropane 0.13U ug/L 09/02/17 06:39 594-20-71.0 0.13 1
1,1-Dichloropropene 0.49U ug/L 09/02/17 06:39 563-58-61.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 10 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Sample:MW-3 Lab ID:92353331003 Collected:08/29/17 13:30 Received:08/30/17 08:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene 0.13U ug/L 09/02/17 06:39 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene 0.26U ug/L 09/02/17 06:39 10061-02-61.0 0.26 1
Diisopropyl ether 0.12U ug/L 09/02/17 06:39 108-20-31.0 0.12 1
Ethylbenzene 0.30U ug/L 09/02/17 06:39 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene 0.71U ug/L 09/02/17 06:39 87-68-31.0 0.71 1
2-Hexanone 0.46U ug/L 09/02/17 06:39 591-78-65.0 0.46 1
p-Isopropyltoluene 0.31U ug/L 09/02/17 06:39 99-87-61.0 0.31 1
Methylene Chloride 0.97U ug/L 09/02/17 06:39 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)0.33U ug/L 09/02/17 06:39 108-10-15.0 0.33 1
Methyl-tert-butyl ether 0.21U ug/L 09/02/17 06:39 1634-04-41.0 0.21 1
Naphthalene 0.24U ug/L 09/02/17 06:39 91-20-31.0 0.24 1
Styrene 0.26U ug/L 09/02/17 06:39 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane 0.33U ug/L 09/02/17 06:39 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane 0.40U ug/L 09/02/17 06:39 79-34-51.0 0.40 1
Tetrachloroethene 0.46U ug/L 09/02/17 06:39 127-18-41.0 0.46 1
Toluene 0.26U ug/L 09/02/17 06:39 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene 0.33U ug/L 09/02/17 06:39 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene 0.35U ug/L 09/02/17 06:39 120-82-11.0 0.35 1
1,1,1-Trichloroethane 0.48U ug/L 09/02/17 06:39 71-55-61.0 0.48 1
1,1,2-Trichloroethane 0.29U ug/L 09/02/17 06:39 79-00-51.0 0.29 1
Trichloroethene 0.47U ug/L 09/02/17 06:39 79-01-61.0 0.47 1
Trichlorofluoromethane 0.28J ug/L 09/02/17 06:39 75-69-41.0 0.20 1
1,2,3-Trichloropropane 0.41U ug/L 09/02/17 06:39 96-18-41.0 0.41 1
Vinyl acetate 0.35U ug/L 09/02/17 06:39 108-05-42.0 0.35 1
Vinyl chloride 0.62U ug/L 09/02/17 06:39 75-01-41.0 0.62 1
Xylene (Total)0.66U ug/L 09/02/17 06:39 1330-20-71.0 0.66 1
m&p-Xylene 0.66U ug/L 09/02/17 06:39 179601-23-12.0 0.66 1
o-Xylene 0.23U ug/L 09/02/17 06:39 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)102 %09/02/17 06:39 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %09/02/17 06:39 17060-07-070-130 1
Toluene-d8 (S)103 %09/02/17 06:39 2037-26-570-130 1
Sample:MW-4 Lab ID:92353331004 Collected:08/29/17 13:45 Received:08/30/17 08:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Collected By Mark
Swann 08/31/17 09:311
Collected Date 8/29/17 08/31/17 09:311
Collected Time 13:45 08/31/17 09:311
Field pH 6.6 Std. Units 08/31/17 09:310.10 0.10 1
Field Temperature 15.6 deg C 08/31/17 09:310.50 0.50 1
Static Water Level 22.15 feet 08/31/17 09:311
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 11 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Sample:MW-4 Lab ID:92353331004 Collected:08/29/17 13:45 Received:08/30/17 08:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method:Monitoring Well Data
Field Specific Conductance 106 umhos/cm 08/31/17 09:311.0 1.0 1
Turbidity 22.5 NTU 08/31/17 09:311.0 1.0 1
Odor No odor 08/31/17 09:311
Appearance Clear 08/31/17 09:311
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony 3.9U ug/L 09/14/17 03:32 7440-36-009/12/17 21:255.0 3.9 1
Arsenic 5.0U ug/L 09/14/17 03:32 7440-38-209/12/17 21:2510.0 5.0 1
Barium 114 ug/L 09/14/17 03:32 7440-39-309/12/17 21:255.0 2.5 1
Beryllium 0.50U ug/L 09/14/17 03:32 7440-41-709/12/17 21:251.0 0.50 1
Cadmium 0.50U ug/L 09/14/17 03:32 7440-43-909/12/17 21:251.0 0.50 1
Chromium 2.5U ug/L 09/14/17 03:32 7440-47-309/12/17 21:255.0 2.5 1
Cobalt 2.5U ug/L 09/14/17 03:32 7440-48-409/12/17 21:255.0 2.5 1
Copper 2.7J ug/L 09/14/17 03:32 7440-50-809/12/17 21:255.0 2.5 1
Lead 3.8J ug/L 09/14/17 03:32 7439-92-109/12/17 21:255.0 2.5 1
Nickel 2.5U ug/L 09/14/17 03:32 7440-02-009/12/17 21:255.0 2.5 1
Selenium 5.0U ug/L 09/14/17 03:32 7782-49-209/12/17 21:2510.0 5.0 1
Silver 2.5U ug/L 09/14/17 03:32 7440-22-409/12/17 21:255.0 2.5 1
Thallium 5.0U ug/L 09/14/17 03:32 7440-28-009/12/17 21:2510.0 5.0 1
Vanadium 21.3 ug/L 09/14/17 03:32 7440-62-209/12/17 21:255.0 2.5 1
Zinc 10.8 ug/L 09/14/17 03:32 7440-66-609/12/17 21:2510.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 0.10U ug/L 09/07/17 02:29 7439-97-609/06/17 02:100.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 10.0U ug/L 09/02/17 06:56 67-64-125.0 10.0 1
Benzene 0.25U ug/L 09/02/17 06:56 71-43-21.0 0.25 1
Bromobenzene 0.30U ug/L 09/02/17 06:56 108-86-11.0 0.30 1
Bromochloromethane 0.17U ug/L 09/02/17 06:56 74-97-51.0 0.17 1
Bromodichloromethane 0.18U ug/L 09/02/17 06:56 75-27-41.0 0.18 1
Bromoform 0.26U ug/L 09/02/17 06:56 75-25-21.0 0.26 1
Bromomethane 0.29U ug/L 09/02/17 06:56 74-83-92.0 0.29 1
2-Butanone (MEK)0.96U ug/L 09/02/17 06:56 78-93-35.0 0.96 1
Carbon tetrachloride 0.25U ug/L 09/02/17 06:56 56-23-51.0 0.25 1
Chlorobenzene 0.23U ug/L 09/02/17 06:56 108-90-71.0 0.23 1
Chloroethane 0.54U ug/L 09/02/17 06:56 75-00-31.0 0.54 1
Chloroform 0.14U ug/L 09/02/17 06:56 67-66-31.0 0.14 1
Chloromethane 0.11U ug/L 09/02/17 06:56 74-87-31.0 0.11 1
2-Chlorotoluene 0.35U ug/L 09/02/17 06:56 95-49-81.0 0.35 1
4-Chlorotoluene 0.31U ug/L 09/02/17 06:56 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane 2.0U ug/L 09/02/17 06:56 96-12-82.0 2.0 1
Dibromochloromethane 0.21U ug/L 09/02/17 06:56 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)0.27U ug/L 09/02/17 06:56 106-93-41.0 0.27 1
Dibromomethane 0.21U ug/L 09/02/17 06:56 74-95-31.0 0.21 1
1,2-Dichlorobenzene 0.30U ug/L 09/02/17 06:56 95-50-11.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 12 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Sample:MW-4 Lab ID:92353331004 Collected:08/29/17 13:45 Received:08/30/17 08:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,3-Dichlorobenzene 0.24U ug/L 09/02/17 06:56 541-73-11.0 0.24 1
1,4-Dichlorobenzene 0.33U ug/L 09/02/17 06:56 106-46-71.0 0.33 1
Dichlorodifluoromethane 0.21U ug/L 09/02/17 06:56 75-71-81.0 0.21 1
1,1-Dichloroethane 0.32U ug/L 09/02/17 06:56 75-34-31.0 0.32 1
1,2-Dichloroethane 0.24U ug/L 09/02/17 06:56 107-06-21.0 0.24 1
1,1-Dichloroethene 0.56U ug/L 09/02/17 06:56 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 0.19U ug/L 09/02/17 06:56 156-59-21.0 0.19 1
trans-1,2-Dichloroethene 0.49U ug/L 09/02/17 06:56 156-60-51.0 0.49 1
1,2-Dichloropropane 0.27U ug/L 09/02/17 06:56 78-87-51.0 0.27 1
1,3-Dichloropropane 0.28U ug/L 09/02/17 06:56 142-28-91.0 0.28 1
2,2-Dichloropropane 0.13U ug/L 09/02/17 06:56 594-20-71.0 0.13 1
1,1-Dichloropropene 0.49U ug/L 09/02/17 06:56 563-58-61.0 0.49 1
cis-1,3-Dichloropropene 0.13U ug/L 09/02/17 06:56 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene 0.26U ug/L 09/02/17 06:56 10061-02-61.0 0.26 1
Diisopropyl ether 0.12U ug/L 09/02/17 06:56 108-20-31.0 0.12 1
Ethylbenzene 0.30U ug/L 09/02/17 06:56 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene 0.71U ug/L 09/02/17 06:56 87-68-31.0 0.71 1
2-Hexanone 0.46U ug/L 09/02/17 06:56 591-78-65.0 0.46 1
p-Isopropyltoluene 0.31U ug/L 09/02/17 06:56 99-87-61.0 0.31 1
Methylene Chloride 0.97U ug/L 09/02/17 06:56 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)0.33U ug/L 09/02/17 06:56 108-10-15.0 0.33 1
Methyl-tert-butyl ether 0.21U ug/L 09/02/17 06:56 1634-04-41.0 0.21 1
Naphthalene 0.24U ug/L 09/02/17 06:56 91-20-31.0 0.24 1
Styrene 0.26U ug/L 09/02/17 06:56 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane 0.33U ug/L 09/02/17 06:56 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane 0.40U ug/L 09/02/17 06:56 79-34-51.0 0.40 1
Tetrachloroethene 0.46U ug/L 09/02/17 06:56 127-18-41.0 0.46 1
Toluene 0.26U ug/L 09/02/17 06:56 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene 0.33U ug/L 09/02/17 06:56 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene 0.35U ug/L 09/02/17 06:56 120-82-11.0 0.35 1
1,1,1-Trichloroethane 0.48U ug/L 09/02/17 06:56 71-55-61.0 0.48 1
1,1,2-Trichloroethane 0.29U ug/L 09/02/17 06:56 79-00-51.0 0.29 1
Trichloroethene 0.47U ug/L 09/02/17 06:56 79-01-61.0 0.47 1
Trichlorofluoromethane 0.20U ug/L 09/02/17 06:56 75-69-41.0 0.20 1
1,2,3-Trichloropropane 0.41U ug/L 09/02/17 06:56 96-18-41.0 0.41 1
Vinyl acetate 0.35U ug/L 09/02/17 06:56 108-05-42.0 0.35 1
Vinyl chloride 0.62U ug/L 09/02/17 06:56 75-01-41.0 0.62 1
Xylene (Total)0.66U ug/L 09/02/17 06:56 1330-20-71.0 0.66 1
m&p-Xylene 0.66U ug/L 09/02/17 06:56 179601-23-12.0 0.66 1
o-Xylene 0.23U ug/L 09/02/17 06:56 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)103 %09/02/17 06:56 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %09/02/17 06:56 17060-07-070-130 1
Toluene-d8 (S)105 %09/02/17 06:56 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 13 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Sample:TVL BLK Lab ID:92353331005 Collected:08/29/17 08:00 Received:08/30/17 08:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 10.0U ug/L 09/05/17 18:21 67-64-125.0 10.0 1
Benzene 0.25U ug/L 09/05/17 18:21 71-43-21.0 0.25 1
Bromobenzene 0.30U ug/L 09/05/17 18:21 108-86-11.0 0.30 1
Bromochloromethane 0.17U ug/L 09/05/17 18:21 74-97-51.0 0.17 1
Bromodichloromethane 0.18U ug/L 09/05/17 18:21 75-27-41.0 0.18 1
Bromoform 0.26U ug/L 09/05/17 18:21 75-25-21.0 0.26 1
Bromomethane 0.29U ug/L 09/05/17 18:21 74-83-92.0 0.29 1
2-Butanone (MEK)0.96U ug/L 09/05/17 18:21 78-93-35.0 0.96 1
Carbon tetrachloride 0.25U ug/L 09/05/17 18:21 56-23-51.0 0.25 1
Chlorobenzene 0.23U ug/L 09/05/17 18:21 108-90-71.0 0.23 1
Chloroethane 0.54U ug/L 09/05/17 18:21 75-00-31.0 0.54 1
Chloroform 0.14U ug/L 09/05/17 18:21 67-66-31.0 0.14 1
Chloromethane 0.11U ug/L 09/05/17 18:21 74-87-31.0 0.11 1
2-Chlorotoluene 0.35U ug/L 09/05/17 18:21 95-49-81.0 0.35 1
4-Chlorotoluene 0.31U ug/L 09/05/17 18:21 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane 2.0U ug/L 09/05/17 18:21 96-12-82.0 2.0 1
Dibromochloromethane 0.21U ug/L 09/05/17 18:21 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)0.27U ug/L 09/05/17 18:21 106-93-41.0 0.27 1
Dibromomethane 0.21U ug/L 09/05/17 18:21 74-95-31.0 0.21 1
1,2-Dichlorobenzene 0.30U ug/L 09/05/17 18:21 95-50-11.0 0.30 1
1,3-Dichlorobenzene 0.24U ug/L 09/05/17 18:21 541-73-11.0 0.24 1
1,4-Dichlorobenzene 0.33U ug/L 09/05/17 18:21 106-46-71.0 0.33 1
Dichlorodifluoromethane 0.21U ug/L 09/05/17 18:21 75-71-81.0 0.21 1
1,1-Dichloroethane 0.32U ug/L 09/05/17 18:21 75-34-31.0 0.32 1
1,2-Dichloroethane 0.24U ug/L 09/05/17 18:21 107-06-21.0 0.24 1
1,1-Dichloroethene 0.56U ug/L 09/05/17 18:21 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 0.19U ug/L 09/05/17 18:21 156-59-21.0 0.19 1
trans-1,2-Dichloroethene 0.49U ug/L 09/05/17 18:21 156-60-51.0 0.49 1
1,2-Dichloropropane 0.27U ug/L 09/05/17 18:21 78-87-51.0 0.27 1
1,3-Dichloropropane 0.28U ug/L 09/05/17 18:21 142-28-91.0 0.28 1
2,2-Dichloropropane 0.13U ug/L 09/05/17 18:21 594-20-71.0 0.13 1
1,1-Dichloropropene 0.49U ug/L 09/05/17 18:21 563-58-61.0 0.49 1
cis-1,3-Dichloropropene 0.13U ug/L 09/05/17 18:21 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene 0.26U ug/L 09/05/17 18:21 10061-02-61.0 0.26 1
Diisopropyl ether 0.12U ug/L 09/05/17 18:21 108-20-31.0 0.12 1
Ethylbenzene 0.30U ug/L 09/05/17 18:21 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene 0.71U ug/L 09/05/17 18:21 87-68-31.0 0.71 1
2-Hexanone 0.46U ug/L 09/05/17 18:21 591-78-65.0 0.46 1
p-Isopropyltoluene 0.31U ug/L 09/05/17 18:21 99-87-61.0 0.31 1
Methylene Chloride 0.97U ug/L 09/05/17 18:21 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)0.33U ug/L 09/05/17 18:21 108-10-15.0 0.33 1
Methyl-tert-butyl ether 0.21U ug/L 09/05/17 18:21 1634-04-41.0 0.21 1
Naphthalene 0.24U ug/L 09/05/17 18:21 91-20-31.0 0.24 1
Styrene 0.26U ug/L 09/05/17 18:21 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane 0.33U ug/L 09/05/17 18:21 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane 0.40U ug/L 09/05/17 18:21 79-34-51.0 0.40 1
REPORT OF LABORATORY ANALYSIS
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Page 14 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Sample:TVL BLK Lab ID:92353331005 Collected:08/29/17 08:00 Received:08/30/17 08:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level Landfill
Tetrachloroethene 0.46U ug/L 09/05/17 18:21 127-18-41.0 0.46 1
Toluene 0.26U ug/L 09/05/17 18:21 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene 0.33U ug/L 09/05/17 18:21 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene 0.35U ug/L 09/05/17 18:21 120-82-11.0 0.35 1
1,1,1-Trichloroethane 0.48U ug/L 09/05/17 18:21 71-55-61.0 0.48 1
1,1,2-Trichloroethane 0.29U ug/L 09/05/17 18:21 79-00-51.0 0.29 1
Trichloroethene 0.47U ug/L 09/05/17 18:21 79-01-61.0 0.47 1
Trichlorofluoromethane 0.20U ug/L 09/05/17 18:21 75-69-41.0 0.20 1
1,2,3-Trichloropropane 0.41U ug/L 09/05/17 18:21 96-18-41.0 0.41 1
Vinyl acetate 0.35U ug/L 09/05/17 18:21 108-05-42.0 0.35 1
Vinyl chloride 0.62U ug/L 09/05/17 18:21 75-01-41.0 0.62 1
Xylene (Total)0.66U ug/L 09/05/17 18:21 1330-20-71.0 0.66 1
m&p-Xylene 0.66U ug/L 09/05/17 18:21 179601-23-12.0 0.66 1
o-Xylene 0.23U ug/L 09/05/17 18:21 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)94 %09/05/17 18:21 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %09/05/17 18:21 17060-07-070-130 1
Toluene-d8 (S)102 %09/05/17 18:21 2037-26-570-130 1
Sample:EQUIP BLK Lab ID:92353331006 Collected:08/29/17 12:30 Received:08/30/17 08:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony 3.9U ug/L 09/14/17 03:35 7440-36-009/12/17 21:255.0 3.9 1
Arsenic 5.0U ug/L 09/14/17 03:35 7440-38-209/12/17 21:2510.0 5.0 1
Barium 2.5U ug/L 09/14/17 03:35 7440-39-309/12/17 21:255.0 2.5 1
Beryllium 0.50U ug/L 09/14/17 03:35 7440-41-709/12/17 21:251.0 0.50 1
Cadmium 0.50U ug/L 09/14/17 03:35 7440-43-909/12/17 21:251.0 0.50 1
Chromium 2.5U ug/L 09/14/17 03:35 7440-47-309/12/17 21:255.0 2.5 1
Cobalt 2.5U ug/L 09/14/17 03:35 7440-48-409/12/17 21:255.0 2.5 1
Copper 2.9J ug/L 09/14/17 03:35 7440-50-809/12/17 21:255.0 2.5 1
Lead 2.5U ug/L 09/14/17 03:35 7439-92-109/12/17 21:255.0 2.5 1
Nickel 2.5U ug/L 09/14/17 03:35 7440-02-009/12/17 21:255.0 2.5 1
Selenium 5.0U ug/L 09/14/17 03:35 7782-49-209/12/17 21:2510.0 5.0 1
Silver 2.5U ug/L 09/14/17 03:35 7440-22-409/12/17 21:255.0 2.5 1
Thallium 5.0U ug/L 09/14/17 03:35 7440-28-009/12/17 21:2510.0 5.0 1
Vanadium 2.5U ug/L 09/14/17 03:35 7440-62-209/12/17 21:255.0 2.5 1
Zinc 5.0U ug/L 09/14/17 03:35 7440-66-609/12/17 21:2510.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 0.10U ug/L 09/07/17 02:31 7439-97-609/06/17 02:100.20 0.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
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Page 15 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Sample:EQUIP BLK Lab ID:92353331006 Collected:08/29/17 12:30 Received:08/30/17 08:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 10.0U ug/L 09/07/17 21:43 67-64-125.0 10.0 1
Benzene 0.25U ug/L 09/07/17 21:43 71-43-21.0 0.25 1
Bromobenzene 0.30U ug/L 09/07/17 21:43 108-86-11.0 0.30 1
Bromochloromethane 0.17U ug/L 09/07/17 21:43 74-97-51.0 0.17 1
Bromodichloromethane 0.18U ug/L 09/07/17 21:43 75-27-41.0 0.18 1
Bromoform 0.26U ug/L 09/07/17 21:43 75-25-21.0 0.26 1
Bromomethane 0.29U ug/L 09/07/17 21:43 74-83-92.0 0.29 1
2-Butanone (MEK)0.96U ug/L 09/07/17 21:43 78-93-35.0 0.96 1
Carbon tetrachloride 0.25U ug/L 09/07/17 21:43 56-23-51.0 0.25 1
Chlorobenzene 0.23U ug/L 09/07/17 21:43 108-90-71.0 0.23 1
Chloroethane 0.54U ug/L 09/07/17 21:43 75-00-31.0 0.54 1
Chloroform 0.14U ug/L 09/07/17 21:43 67-66-31.0 0.14 1
Chloromethane 0.11U ug/L 09/07/17 21:43 74-87-31.0 0.11 1
2-Chlorotoluene 0.35U ug/L 09/07/17 21:43 95-49-81.0 0.35 1
4-Chlorotoluene 0.31U ug/L 09/07/17 21:43 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane 2.0U ug/L 09/07/17 21:43 96-12-82.0 2.0 1
Dibromochloromethane 0.21U ug/L 09/07/17 21:43 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)0.27U ug/L 09/07/17 21:43 106-93-41.0 0.27 1
Dibromomethane 0.21U ug/L 09/07/17 21:43 74-95-31.0 0.21 1
1,2-Dichlorobenzene 0.30U ug/L 09/07/17 21:43 95-50-11.0 0.30 1
1,3-Dichlorobenzene 0.24U ug/L 09/07/17 21:43 541-73-11.0 0.24 1
1,4-Dichlorobenzene 0.33U ug/L 09/07/17 21:43 106-46-71.0 0.33 1
Dichlorodifluoromethane 0.21U ug/L 09/07/17 21:43 75-71-81.0 0.21 1
1,1-Dichloroethane 0.32U ug/L 09/07/17 21:43 75-34-31.0 0.32 1
1,2-Dichloroethane 0.24U ug/L 09/07/17 21:43 107-06-21.0 0.24 1
1,1-Dichloroethene 0.56U ug/L 09/07/17 21:43 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 0.19U ug/L 09/07/17 21:43 156-59-21.0 0.19 1
trans-1,2-Dichloroethene 0.49U ug/L 09/07/17 21:43 156-60-51.0 0.49 1
1,2-Dichloropropane 0.27U ug/L 09/07/17 21:43 78-87-51.0 0.27 1
1,3-Dichloropropane 0.28U ug/L 09/07/17 21:43 142-28-91.0 0.28 1
2,2-Dichloropropane 0.13U ug/L 09/07/17 21:43 594-20-71.0 0.13 1
1,1-Dichloropropene 0.49U ug/L 09/07/17 21:43 563-58-61.0 0.49 1
cis-1,3-Dichloropropene 0.13U ug/L 09/07/17 21:43 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene 0.26U ug/L 09/07/17 21:43 10061-02-61.0 0.26 1
Diisopropyl ether 0.12U ug/L 09/07/17 21:43 108-20-31.0 0.12 1
Ethylbenzene 0.30U ug/L 09/07/17 21:43 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene 0.71U ug/L 09/07/17 21:43 87-68-31.0 0.71 1
2-Hexanone 0.46U ug/L 09/07/17 21:43 591-78-65.0 0.46 1
p-Isopropyltoluene 0.31U ug/L 09/07/17 21:43 99-87-61.0 0.31 1
Methylene Chloride 0.97U ug/L 09/07/17 21:43 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)0.33U ug/L 09/07/17 21:43 108-10-15.0 0.33 1
Methyl-tert-butyl ether 0.21U ug/L 09/07/17 21:43 1634-04-41.0 0.21 1
Naphthalene 0.24U ug/L 09/07/17 21:43 91-20-31.0 0.24 1
Styrene 0.26U ug/L 09/07/17 21:43 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane 0.33U ug/L 09/07/17 21:43 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane 0.40U ug/L 09/07/17 21:43 79-34-51.0 0.40 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 16 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Sample:EQUIP BLK Lab ID:92353331006 Collected:08/29/17 12:30 Received:08/30/17 08:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 82608260 MSV Low Level Landfill
Tetrachloroethene 0.46U ug/L 09/07/17 21:43 127-18-41.0 0.46 1
Toluene 0.26U ug/L 09/07/17 21:43 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene 0.33U ug/L 09/07/17 21:43 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene 0.35U ug/L 09/07/17 21:43 120-82-11.0 0.35 1
1,1,1-Trichloroethane 0.48U ug/L 09/07/17 21:43 71-55-61.0 0.48 1
1,1,2-Trichloroethane 0.29U ug/L 09/07/17 21:43 79-00-51.0 0.29 1
Trichloroethene 0.47U ug/L 09/07/17 21:43 79-01-61.0 0.47 1
Trichlorofluoromethane 0.20U ug/L 09/07/17 21:43 75-69-41.0 0.20 1
1,2,3-Trichloropropane 0.41U ug/L 09/07/17 21:43 96-18-41.0 0.41 1
Vinyl acetate 0.35U ug/L 09/07/17 21:43 108-05-42.0 0.35 1
Vinyl chloride 0.62U ug/L 09/07/17 21:43 75-01-41.0 0.62 1
Xylene (Total)0.66U ug/L 09/07/17 21:43 1330-20-71.0 0.66 1
m&p-Xylene 0.66U ug/L 09/07/17 21:43 179601-23-12.0 0.66 1
o-Xylene 0.23U ug/L 09/07/17 21:43 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)101 %09/07/17 21:43 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %09/07/17 21:43 17060-07-070-130 1
Toluene-d8 (S)107 %09/07/17 21:43 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
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Asheville, NC 28804
[phone]
Page 17 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
375868
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92353331002, 92353331003, 92353331004, 92353331006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2081971
Associated Lab Samples:92353331002, 92353331003, 92353331004, 92353331006
Matrix:Water
AnalyzedMDL
Mercury ug/L 0.10U 0.20 09/07/17 01:240.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2081972LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.12.5 85 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2081975MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92353414022
2081976
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L M12.5 55 75-12560 9 252.5ND 1.4 1.5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
Pace Analytical Services, LLC
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Asheville, NC 28804
[phone]
Page 18 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
377063
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92353331001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2089008
Associated Lab Samples:92353331001
Matrix:Water
AnalyzedMDL
Mercury ug/L 0.10U 0.20 09/12/17 14:420.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2089009LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.62.5 104 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2089010MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92353513014
2089011
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 95 75-12594 2 252.5ND 2.4 2.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 19 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
377234
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92353331001, 92353331002, 92353331003, 92353331004, 92353331006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2090151
Associated Lab Samples:92353331001, 92353331002, 92353331003, 92353331004, 92353331006
Matrix:Water
AnalyzedMDL
Antimony ug/L 3.9U 5.0 09/14/17 03:013.9
Arsenic ug/L 5.0U 10.0 09/14/17 03:015.0
Barium ug/L 2.5U 5.0 09/14/17 03:012.5
Beryllium ug/L 0.50U 1.0 09/14/17 03:010.50
Cadmium ug/L 0.50U 1.0 09/14/17 03:010.50
Chromium ug/L 2.5U 5.0 09/14/17 03:012.5
Cobalt ug/L 2.5U 5.0 09/14/17 03:012.5
Copper ug/L 2.5U 5.0 09/14/17 03:012.5
Lead ug/L 2.5U 5.0 09/14/17 03:012.5
Nickel ug/L 2.5U 5.0 09/14/17 03:012.5
Selenium ug/L 5.0U 10.0 09/14/17 03:015.0
Silver ug/L 2.5U 5.0 09/14/17 03:012.5
Thallium ug/L 5.0U 10.0 09/14/17 03:015.0
Vanadium ug/L 2.5U 5.0 09/14/17 03:012.5
Zinc ug/L 5.0U 10.0 09/14/17 03:015.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2090152LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 468500 94 80-120
Arsenic ug/L 460500 92 80-120
Barium ug/L 460500 92 80-120
Beryllium ug/L 469500 94 80-120
Cadmium ug/L 468500 94 80-120
Chromium ug/L 460500 92 80-120
Cobalt ug/L 470500 94 80-120
Copper ug/L 474500 95 80-120
Lead ug/L 464500 93 80-120
Nickel ug/L 458500 92 80-120
Selenium ug/L 473500 95 80-120
Silver ug/L 236250 94 80-120
Thallium ug/L 469500 94 80-120
Vanadium ug/L 460500 92 80-120
Zinc ug/L 464500 93 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
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Asheville, NC 28804
[phone]
Page 20 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2090153MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92353331001
2090154
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 96 75-12595 1 205003.9U 478 474
Arsenic ug/L 500 95 75-12593 2 205005.0U 477 466
Barium ug/L 500 96 75-12593 2 20500172652638
Beryllium ug/L 500 98 75-12595 2 205000.50U 488 476
Cadmium ug/L 500 96 75-12594 1 205000.50U 479 472
Chromium ug/L 500 95 75-12593 2 205002.5U 476 466
Cobalt ug/L 500 96 75-12594 2 205002.5U 480 473
Copper ug/L 500 99 75-12597 2 205002.5U 495 487
Lead ug/L 500 94 75-12592 2 205002.5U 468 459
Nickel ug/L 500 93 75-12591 2 205002.5U 464 456
Selenium ug/L 500 96 75-12594 3 205006.9J 488 475
Silver ug/L 250 96 75-12594 3 202502.5U 242 235
Thallium ug/L 500 92 75-12591 1 205005.0U 463 457
Vanadium ug/L 500 96 75-12594 2 205002.5U 480 471
Zinc ug/L 500 96 75-12594 2 205009.5J 489 480
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 21 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
376144
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92353331001, 92353331002, 92353331003, 92353331004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2083816
Associated Lab Samples:92353331001, 92353331002, 92353331003, 92353331004
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L 0.33U 1.0 09/01/17 21:310.33
1,1,1-Trichloroethane ug/L 0.48U 1.0 09/01/17 21:310.48
1,1,2,2-Tetrachloroethane ug/L 0.40U 1.0 09/01/17 21:310.40
1,1,2-Trichloroethane ug/L 0.29U 1.0 09/01/17 21:310.29
1,1-Dichloroethane ug/L 0.32U 1.0 09/01/17 21:310.32
1,1-Dichloroethene ug/L 0.56U 1.0 09/01/17 21:310.56
1,1-Dichloropropene ug/L 0.49U 1.0 09/01/17 21:310.49
1,2,3-Trichlorobenzene ug/L 0.33U 1.0 09/01/17 21:310.33
1,2,3-Trichloropropane ug/L 0.41U 1.0 09/01/17 21:310.41
1,2,4-Trichlorobenzene ug/L 0.35U 1.0 09/01/17 21:310.35
1,2-Dibromo-3-chloropropane ug/L 2.0U 2.0 09/01/17 21:312.0
1,2-Dibromoethane (EDB)ug/L 0.27U 1.0 09/01/17 21:310.27
1,2-Dichlorobenzene ug/L 0.30U 1.0 09/01/17 21:310.30
1,2-Dichloroethane ug/L 0.24U 1.0 09/01/17 21:310.24
1,2-Dichloropropane ug/L 0.27U 1.0 09/01/17 21:310.27
1,3-Dichlorobenzene ug/L 0.24U 1.0 09/01/17 21:310.24
1,3-Dichloropropane ug/L 0.28U 1.0 09/01/17 21:310.28
1,4-Dichlorobenzene ug/L 0.33U 1.0 09/01/17 21:310.33
2,2-Dichloropropane ug/L 0.13U 1.0 09/01/17 21:310.13
2-Butanone (MEK)ug/L 0.96U 5.0 09/01/17 21:310.96
2-Chlorotoluene ug/L 0.35U 1.0 09/01/17 21:310.35
2-Hexanone ug/L 0.46U 5.0 09/01/17 21:310.46
4-Chlorotoluene ug/L 0.31U 1.0 09/01/17 21:310.31
4-Methyl-2-pentanone (MIBK)ug/L 0.33U 5.0 09/01/17 21:310.33
Acetone ug/L 10.0U 25.0 09/01/17 21:3110.0
Benzene ug/L 0.25U 1.0 09/01/17 21:310.25
Bromobenzene ug/L 0.30U 1.0 09/01/17 21:310.30
Bromochloromethane ug/L 0.17U 1.0 09/01/17 21:310.17
Bromodichloromethane ug/L 0.18U 1.0 09/01/17 21:310.18
Bromoform ug/L 0.26U 1.0 09/01/17 21:310.26
Bromomethane ug/L 0.29U 2.0 09/01/17 21:310.29
Carbon tetrachloride ug/L 0.25U 1.0 09/01/17 21:310.25
Chlorobenzene ug/L 0.23U 1.0 09/01/17 21:310.23
Chloroethane ug/L 0.54U 1.0 09/01/17 21:310.54
Chloroform ug/L 0.14U 1.0 09/01/17 21:310.14
Chloromethane ug/L 0.11U 1.0 09/01/17 21:310.11
cis-1,2-Dichloroethene ug/L 0.19U 1.0 09/01/17 21:310.19
cis-1,3-Dichloropropene ug/L 0.13U 1.0 09/01/17 21:310.13
Dibromochloromethane ug/L 0.21U 1.0 09/01/17 21:310.21
Dibromomethane ug/L 0.21U 1.0 09/01/17 21:310.21
Dichlorodifluoromethane ug/L 0.21U 1.0 09/01/17 21:310.21
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
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Page 22 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2083816
Associated Lab Samples:92353331001, 92353331002, 92353331003, 92353331004
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L 0.12U 1.0 09/01/17 21:310.12
Ethylbenzene ug/L 0.30U 1.0 09/01/17 21:310.30
Hexachloro-1,3-butadiene ug/L 1.1 1.0 09/01/17 21:310.71
m&p-Xylene ug/L 0.66U 2.0 09/01/17 21:310.66
Methyl-tert-butyl ether ug/L 0.21U 1.0 09/01/17 21:310.21
Methylene Chloride ug/L 0.97U 1.0 09/01/17 21:310.97
Naphthalene ug/L 0.24U 1.0 09/01/17 21:310.24
o-Xylene ug/L 0.23U 1.0 09/01/17 21:310.23
p-Isopropyltoluene ug/L 0.31U 1.0 09/01/17 21:310.31
Styrene ug/L 0.26U 1.0 09/01/17 21:310.26
Tetrachloroethene ug/L 0.46U 1.0 09/01/17 21:310.46
Toluene ug/L 0.26U 1.0 09/01/17 21:310.26
trans-1,2-Dichloroethene ug/L 0.49U 1.0 09/01/17 21:310.49
trans-1,3-Dichloropropene ug/L 0.26U 1.0 09/01/17 21:310.26
Trichloroethene ug/L 0.47U 1.0 09/01/17 21:310.47
Trichlorofluoromethane ug/L 0.20U 1.0 09/01/17 21:310.20
Vinyl acetate ug/L 0.35U 2.0 09/01/17 21:310.35
Vinyl chloride ug/L 0.62U 1.0 09/01/17 21:310.62
Xylene (Total)ug/L 0.66U 1.0 09/01/17 21:310.66
1,2-Dichloroethane-d4 (S)%95 70-130 09/01/17 21:31
4-Bromofluorobenzene (S)%102 70-130 09/01/17 21:31
Toluene-d8 (S)%107 70-130 09/01/17 21:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2083817LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 48.250 96 80-125
1,1,1-Trichloroethane ug/L 45.550 91 71-129
1,1,2,2-Tetrachloroethane ug/L 44.350 89 79-124
1,1,2-Trichloroethane ug/L 46.150 92 85-125
1,1-Dichloroethane ug/L 43.850 88 73-126
1,1-Dichloroethene ug/L 44.550 89 66-135
1,1-Dichloropropene ug/L 49.150 98 74-135
1,2,3-Trichlorobenzene ug/L 46.650 93 73-135
1,2,3-Trichloropropane ug/L 47.050 94 75-130
1,2,4-Trichlorobenzene ug/L 47.250 94 75-134
1,2-Dibromo-3-chloropropane ug/L 44.350 89 71-133
1,2-Dibromoethane (EDB)ug/L 50.250 100 83-124
1,2-Dichlorobenzene ug/L 48.350 97 80-133
1,2-Dichloroethane ug/L 47.050 94 67-128
1,2-Dichloropropane ug/L 45.750 91 75-132
1,3-Dichlorobenzene ug/L 48.250 96 77-130
1,3-Dichloropropane ug/L 50.550 101 76-131
1,4-Dichlorobenzene ug/L 48.750 97 78-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
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Page 23 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2083817LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 45.950 92 40-160
2-Butanone (MEK)ug/L 113100 113 61-144
2-Chlorotoluene ug/L 46.050 92 74-132
2-Hexanone ug/L 101100 101 68-143
4-Chlorotoluene ug/L 47.050 94 76-133
4-Methyl-2-pentanone (MIBK)ug/L 98.4100 98 72-135
Acetone ug/L 129100 129 48-146
Benzene ug/L 47.750 95 80-125
Bromobenzene ug/L 47.750 95 75-125
Bromochloromethane ug/L 45.050 90 71-125
Bromodichloromethane ug/L 47.350 95 78-124
Bromoform ug/L 40.550 81 71-128
Bromomethane ug/L 44.150 88 40-160
Carbon tetrachloride ug/L 45.950 92 69-131
Chlorobenzene ug/L 47.950 96 81-122
Chloroethane ug/L 50.550 101 39-148
Chloroform ug/L 44.550 89 73-127
Chloromethane ug/L 44.250 88 44-146
cis-1,2-Dichloroethene ug/L 48.250 96 74-124
cis-1,3-Dichloropropene ug/L 48.450 97 72-132
Dibromochloromethane ug/L 45.850 92 78-125
Dibromomethane ug/L 45.050 90 82-120
Dichlorodifluoromethane ug/L 40.050 80 34-157
Diisopropyl ether ug/L 52.350 105 69-135
Ethylbenzene ug/L 47.050 94 79-121
Hexachloro-1,3-butadiene ug/L 45.650 91 72-131
m&p-Xylene ug/L 92.1100 92 81-124
Methyl-tert-butyl ether ug/L 51.850 104 74-131
Methylene Chloride ug/L 48.750 97 64-133
Naphthalene ug/L 46.250 92 73-133
o-Xylene ug/L 46.850 94 79-131
p-Isopropyltoluene ug/L 46.750 93 80-131
Styrene ug/L 45.950 92 84-126
Tetrachloroethene ug/L 45.850 92 78-122
Toluene ug/L 45.350 91 80-121
trans-1,2-Dichloroethene ug/L 45.850 92 71-127
trans-1,3-Dichloropropene ug/L 48.650 97 69-141
Trichloroethene ug/L 49.750 99 78-122
Trichlorofluoromethane ug/L 45.850 92 53-137
Vinyl acetate ug/L 107100 107 40-160
Vinyl chloride ug/L 43.450 87 58-137
Xylene (Total)ug/L 139150 93 81-126
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%97 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
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Page 24 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2083819MATRIX SPIKE SAMPLE:
MSSpike
Result
92353331004
1,1,1,2-Tetrachloroethane ug/L 18.820 94 70-1300.33U
1,1,1-Trichloroethane ug/L 22.420 112 70-1300.48U
1,1,2,2-Tetrachloroethane ug/L 17.620 88 70-1300.40U
1,1,2-Trichloroethane ug/L 19.220 96 70-1300.29U
1,1-Dichloroethane ug/L 20.820 104 70-1300.32U
1,1-Dichloroethene ug/L 22.620 113 70-1660.56U
1,1-Dichloropropene ug/L 22.420 112 70-1300.49U
1,2,3-Trichlorobenzene ug/L 19.820 99 70-1300.33U
1,2,3-Trichloropropane ug/L 19.320 97 70-1300.41U
1,2,4-Trichlorobenzene ug/L 20.120 100 70-1300.35U
1,2-Dibromo-3-chloropropane ug/L 18.720 93 70-1302.0U
1,2-Dibromoethane (EDB)ug/L 20.520 103 70-1300.27U
1,2-Dichlorobenzene ug/L 20.320 101 70-1300.30U
1,2-Dichloroethane ug/L 20.820 104 70-1300.24U
1,2-Dichloropropane ug/L 20.520 102 70-1300.27U
1,3-Dichlorobenzene ug/L 20.020 100 70-1300.24U
1,3-Dichloropropane ug/L 20.120 101 70-1300.28U
1,4-Dichlorobenzene ug/L 20.220 101 70-1300.33U
2,2-Dichloropropane ug/L 20.920 105 70-1300.13U
2-Butanone (MEK)ug/L 40.240 101 70-1300.96U
2-Chlorotoluene ug/L 20.020 100 70-1300.35U
2-Hexanone ug/L 40.940 102 70-1300.46U
4-Chlorotoluene ug/L 20.720 103 70-1300.31U
4-Methyl-2-pentanone (MIBK)ug/L 40.740 102 70-1300.33U
Acetone ug/L 45.540 114 70-13010.0U
Benzene ug/L 21.220 106 70-1480.25U
Bromobenzene ug/L 20.520 103 70-1300.30U
Bromochloromethane ug/L 21.320 107 70-1300.17U
Bromodichloromethane ug/L 20.520 102 70-1300.18U
Bromoform ug/L 17.520 88 70-1300.26U
Bromomethane ug/L 24.320 121 70-1300.29U
Carbon tetrachloride ug/L 21.920 110 70-1300.25U
Chlorobenzene ug/L 21.320 106 70-1460.23U
Chloroethane ug/L 25.620 128 70-1300.54U
Chloroform ug/L 22.120 110 70-1300.14U
Chloromethane ug/L 21.920 110 70-1300.11U
cis-1,2-Dichloroethene ug/L 23.020 115 70-1300.19U
cis-1,3-Dichloropropene ug/L 20.520 103 70-1300.13U
Dibromochloromethane ug/L 18.920 94 70-1300.21U
Dibromomethane ug/L 19.420 97 70-1300.21U
Dichlorodifluoromethane ug/L 20.220 101 70-1300.21U
Diisopropyl ether ug/L 21.320 106 70-1300.12U
Ethylbenzene ug/L 20.920 104 70-1300.30U
Hexachloro-1,3-butadiene ug/L 21.420 107 70-1300.71U
m&p-Xylene ug/L 42.240 105 70-1300.66U
Methyl-tert-butyl ether ug/L 20.320 102 70-1300.21U
Methylene Chloride ug/L 23.220 116 70-1300.97U
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
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Page 25 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2083819MATRIX SPIKE SAMPLE:
MSSpike
Result
92353331004
Naphthalene ug/L 18.520 92 70-1300.24U
o-Xylene ug/L 20.820 104 70-1300.23U
p-Isopropyltoluene ug/L 19.520 98 70-1300.31U
Styrene ug/L 20.420 102 70-1300.26U
Tetrachloroethene ug/L 20.220 101 70-1300.46U
Toluene ug/L 21.020 105 70-1550.26U
trans-1,2-Dichloroethene ug/L 22.920 114 70-1300.49U
trans-1,3-Dichloropropene ug/L 19.920 100 70-1300.26U
Trichloroethene ug/L 21.920 109 69-1510.47U
Trichlorofluoromethane ug/L 24.620 123 70-1300.20U
Vinyl acetate ug/L 40.540 101 70-1300.35U
Vinyl chloride ug/L 22.020 110 70-1300.62U
1,2-Dichloroethane-d4 (S)%104 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92353331003
2083818SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L 0.33U 300.33U
1,1,1-Trichloroethane ug/L 0.48U 300.48U
1,1,2,2-Tetrachloroethane ug/L 0.40U 300.40U
1,1,2-Trichloroethane ug/L 0.29U 300.29U
1,1-Dichloroethane ug/L 0.32U 300.32U
1,1-Dichloroethene ug/L 0.56U 300.56U
1,1-Dichloropropene ug/L 0.49U 300.49U
1,2,3-Trichlorobenzene ug/L 0.33U 300.33U
1,2,3-Trichloropropane ug/L 0.41U 300.41U
1,2,4-Trichlorobenzene ug/L 0.35U 300.35U
1,2-Dibromo-3-chloropropane ug/L 2.0U 302.0U
1,2-Dibromoethane (EDB)ug/L 0.27U 300.27U
1,2-Dichlorobenzene ug/L 0.30U 300.30U
1,2-Dichloroethane ug/L 0.24U 300.24U
1,2-Dichloropropane ug/L 0.27U 300.27U
1,3-Dichlorobenzene ug/L 0.24U 300.24U
1,3-Dichloropropane ug/L 0.28U 300.28U
1,4-Dichlorobenzene ug/L 0.33U 300.33U
2,2-Dichloropropane ug/L 0.13U 300.13U
2-Butanone (MEK)ug/L 0.96U 300.96U
2-Chlorotoluene ug/L 0.35U 300.35U
2-Hexanone ug/L 0.46U 300.46U
4-Chlorotoluene ug/L 0.31U 300.31U
4-Methyl-2-pentanone (MIBK)ug/L 0.33U 300.33U
Acetone ug/L 10.0U 3010.0U
Benzene ug/L 0.25U 300.25U
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
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Page 26 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92353331003
2083818SAMPLE DUPLICATE:
Bromobenzene ug/L 0.30U 300.30U
Bromochloromethane ug/L 0.17U 300.17U
Bromodichloromethane ug/L 0.18U 300.18U
Bromoform ug/L 0.26U 300.26U
Bromomethane ug/L 0.29U 300.29U
Carbon tetrachloride ug/L 0.25U 300.25U
Chlorobenzene ug/L 0.23U 300.23U
Chloroethane ug/L 0.54U 300.54U
Chloroform ug/L 0.14U 300.14U
Chloromethane ug/L 0.11U 300.11U
cis-1,2-Dichloroethene ug/L 0.19U 300.19U
cis-1,3-Dichloropropene ug/L 0.13U 300.13U
Dibromochloromethane ug/L 0.21U 300.21U
Dibromomethane ug/L 0.21U 300.21U
Dichlorodifluoromethane ug/L 0.21U 300.21U
Diisopropyl ether ug/L 0.12U 300.12U
Ethylbenzene ug/L 0.30U 300.30U
Hexachloro-1,3-butadiene ug/L 0.71U 300.71U
m&p-Xylene ug/L 0.66U 300.66U
Methyl-tert-butyl ether ug/L 0.21U 300.21U
Methylene Chloride ug/L 0.97U 300.97U
Naphthalene ug/L 0.24U 300.24U
o-Xylene ug/L 0.23U 300.23U
p-Isopropyltoluene ug/L 0.31U 300.31U
Styrene ug/L 0.26U 300.26U
Tetrachloroethene ug/L 0.46U 300.46U
Toluene ug/L 0.26U 300.26U
trans-1,2-Dichloroethene ug/L 0.49U 300.49U
trans-1,3-Dichloropropene ug/L 0.26U 300.26U
Trichloroethene ug/L 0.47U 300.47U
Trichlorofluoromethane ug/L 0.39J 300.28J
Vinyl acetate ug/L 0.35U 300.35U
Vinyl chloride ug/L 0.62U 300.62U
Xylene (Total)ug/L 0.66U 300.66U
1,2-Dichloroethane-d4 (S)%96 096
4-Bromofluorobenzene (S)%100 2102
Toluene-d8 (S)%110 7103
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
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Asheville, NC 28804
[phone]
Page 27 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
376357
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92353331005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2085013
Associated Lab Samples:92353331005
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L 0.33U 1.0 09/05/17 16:030.33
1,1,1-Trichloroethane ug/L 0.48U 1.0 09/05/17 16:030.48
1,1,2,2-Tetrachloroethane ug/L 0.40U 1.0 09/05/17 16:030.40
1,1,2-Trichloroethane ug/L 0.29U 1.0 09/05/17 16:030.29
1,1-Dichloroethane ug/L 0.32U 1.0 09/05/17 16:030.32
1,1-Dichloroethene ug/L 0.56U 1.0 09/05/17 16:030.56
1,1-Dichloropropene ug/L 0.49U 1.0 09/05/17 16:030.49
1,2,3-Trichlorobenzene ug/L 0.33U 1.0 09/05/17 16:030.33
1,2,3-Trichloropropane ug/L 0.41U 1.0 09/05/17 16:030.41
1,2,4-Trichlorobenzene ug/L 0.35U 1.0 09/05/17 16:030.35
1,2-Dibromo-3-chloropropane ug/L 2.0U 2.0 09/05/17 16:032.0
1,2-Dibromoethane (EDB)ug/L 0.27U 1.0 09/05/17 16:030.27
1,2-Dichlorobenzene ug/L 0.30U 1.0 09/05/17 16:030.30
1,2-Dichloroethane ug/L 0.24U 1.0 09/05/17 16:030.24
1,2-Dichloropropane ug/L 0.27U 1.0 09/05/17 16:030.27
1,3-Dichlorobenzene ug/L 0.24U 1.0 09/05/17 16:030.24
1,3-Dichloropropane ug/L 0.28U 1.0 09/05/17 16:030.28
1,4-Dichlorobenzene ug/L 0.33U 1.0 09/05/17 16:030.33
2,2-Dichloropropane ug/L 0.13U 1.0 09/05/17 16:030.13
2-Butanone (MEK)ug/L 0.96U 5.0 09/05/17 16:030.96
2-Chlorotoluene ug/L 0.35U 1.0 09/05/17 16:030.35
2-Hexanone ug/L 0.46U 5.0 09/05/17 16:030.46
4-Chlorotoluene ug/L 0.31U 1.0 09/05/17 16:030.31
4-Methyl-2-pentanone (MIBK)ug/L 0.33U 5.0 09/05/17 16:030.33
Acetone ug/L 10.0U 25.0 09/05/17 16:0310.0
Benzene ug/L 0.25U 1.0 09/05/17 16:030.25
Bromobenzene ug/L 0.30U 1.0 09/05/17 16:030.30
Bromochloromethane ug/L 0.17U 1.0 09/05/17 16:030.17
Bromodichloromethane ug/L 0.18U 1.0 09/05/17 16:030.18
Bromoform ug/L 0.26U 1.0 09/05/17 16:030.26
Bromomethane ug/L 0.29U 2.0 09/05/17 16:030.29
Carbon tetrachloride ug/L 0.25U 1.0 09/05/17 16:030.25
Chlorobenzene ug/L 0.23U 1.0 09/05/17 16:030.23
Chloroethane ug/L 0.54U 1.0 09/05/17 16:030.54
Chloroform ug/L 0.34J 1.0 09/05/17 16:030.14
Chloromethane ug/L 0.11U 1.0 09/05/17 16:030.11
cis-1,2-Dichloroethene ug/L 0.19U 1.0 09/05/17 16:030.19
cis-1,3-Dichloropropene ug/L 0.13U 1.0 09/05/17 16:030.13
Dibromochloromethane ug/L 0.21U 1.0 09/05/17 16:030.21
Dibromomethane ug/L 0.21U 1.0 09/05/17 16:030.21
Dichlorodifluoromethane ug/L 0.21U 1.0 09/05/17 16:030.21
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
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Page 28 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2085013
Associated Lab Samples:92353331005
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L 0.12U 1.0 09/05/17 16:030.12
Ethylbenzene ug/L 0.30U 1.0 09/05/17 16:030.30
Hexachloro-1,3-butadiene ug/L 0.71U 1.0 09/05/17 16:030.71
m&p-Xylene ug/L 0.66U 2.0 09/05/17 16:030.66
Methyl-tert-butyl ether ug/L 0.21U 1.0 09/05/17 16:030.21
Methylene Chloride ug/L 0.97U 1.0 09/05/17 16:030.97
Naphthalene ug/L 0.24U 1.0 09/05/17 16:030.24
o-Xylene ug/L 0.23U 1.0 09/05/17 16:030.23
p-Isopropyltoluene ug/L 0.31U 1.0 09/05/17 16:030.31
Styrene ug/L 0.26U 1.0 09/05/17 16:030.26
Tetrachloroethene ug/L 0.46U 1.0 09/05/17 16:030.46
Toluene ug/L 0.26U 1.0 09/05/17 16:030.26
trans-1,2-Dichloroethene ug/L 0.49U 1.0 09/05/17 16:030.49
trans-1,3-Dichloropropene ug/L 0.26U 1.0 09/05/17 16:030.26
Trichloroethene ug/L 0.47U 1.0 09/05/17 16:030.47
Trichlorofluoromethane ug/L 0.20U 1.0 09/05/17 16:030.20
Vinyl acetate ug/L 0.35U 2.0 09/05/17 16:030.35
Vinyl chloride ug/L 0.62U 1.0 09/05/17 16:030.62
Xylene (Total)ug/L 0.66U 1.0 09/05/17 16:030.66
1,2-Dichloroethane-d4 (S)%105 70-130 09/05/17 16:03
4-Bromofluorobenzene (S)%95 70-130 09/05/17 16:03
Toluene-d8 (S)%102 70-130 09/05/17 16:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2085014LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 47.850 96 80-125
1,1,1-Trichloroethane ug/L 52.350 105 71-129
1,1,2,2-Tetrachloroethane ug/L 47.950 96 79-124
1,1,2-Trichloroethane ug/L 48.550 97 85-125
1,1-Dichloroethane ug/L 53.350 107 73-126
1,1-Dichloroethene ug/L 50.750 101 66-135
1,1-Dichloropropene ug/L 54.350 109 74-135
1,2,3-Trichlorobenzene ug/L 53.150 106 73-135
1,2,3-Trichloropropane ug/L 50.250 100 75-130
1,2,4-Trichlorobenzene ug/L 53.150 106 75-134
1,2-Dibromo-3-chloropropane ug/L 53.450 107 71-133
1,2-Dibromoethane (EDB)ug/L 50.850 102 83-124
1,2-Dichlorobenzene ug/L 49.450 99 80-133
1,2-Dichloroethane ug/L 51.350 103 67-128
1,2-Dichloropropane ug/L 50.450 101 75-132
1,3-Dichlorobenzene ug/L 48.450 97 77-130
1,3-Dichloropropane ug/L 50.350 101 76-131
1,4-Dichlorobenzene ug/L 48.150 96 78-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
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Page 29 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2085014LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 54.150 108 40-160
2-Butanone (MEK)ug/L 124100 124 61-144
2-Chlorotoluene ug/L 48.350 97 74-132
2-Hexanone ug/L 106100 106 68-143
4-Chlorotoluene ug/L 49.450 99 76-133
4-Methyl-2-pentanone (MIBK)ug/L 104100 104 72-135
Acetone ug/L 141100 141 48-146
Benzene ug/L 48.350 97 80-125
Bromobenzene ug/L 49.250 98 75-125
Bromochloromethane ug/L 54.850 110 71-125
Bromodichloromethane ug/L 48.750 97 78-124
Bromoform ug/L 53.750 107 71-128
Bromomethane ug/L 53.050 106 40-160
Carbon tetrachloride ug/L 45.350 91 69-131
Chlorobenzene ug/L 48.550 97 81-122
Chloroethane ug/L 55.150 110 39-148
Chloroform ug/L 53.050 106 73-127
Chloromethane ug/L 59.250 118 44-146
cis-1,2-Dichloroethene ug/L 54.450 109 74-124
cis-1,3-Dichloropropene ug/L 51.850 104 72-132
Dibromochloromethane ug/L 51.850 104 78-125
Dibromomethane ug/L 50.250 100 82-120
Dichlorodifluoromethane ug/L 54.550 109 34-157
Diisopropyl ether ug/L 57.650 115 69-135
Ethylbenzene ug/L 49.150 98 79-121
Hexachloro-1,3-butadiene ug/L 51.850 104 72-131
m&p-Xylene ug/L 98.4100 98 81-124
Methyl-tert-butyl ether ug/L 57.050 114 74-131
Methylene Chloride ug/L 56.150 112 64-133
Naphthalene ug/L 54.350 109 73-133
o-Xylene ug/L 49.450 99 79-131
p-Isopropyltoluene ug/L 49.950 100 80-131
Styrene ug/L 51.050 102 84-126
Tetrachloroethene ug/L 46.750 93 78-122
Toluene ug/L 49.250 98 80-121
trans-1,2-Dichloroethene ug/L 53.750 107 71-127
trans-1,3-Dichloropropene ug/L 50.550 101 69-141
Trichloroethene ug/L 47.850 96 78-122
Trichlorofluoromethane ug/L 53.050 106 53-137
Vinyl acetate ug/L 130100 130 40-160
Vinyl chloride ug/L 54.650 109 58-137
Xylene (Total)ug/L 148150 99 81-126
1,2-Dichloroethane-d4 (S)%110 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
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Asheville, NC 28804
[phone]
Page 30 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2085015MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92352957001
2085016
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 100 110 70-130105 4 30100ND110105
1,1,1-Trichloroethane ug/L 100 116 70-130114 1 30100ND116114
1,1,2,2-Tetrachloroethane ug/L 100 109 70-130105 4 30100ND109105
1,1,2-Trichloroethane ug/L 100 111 70-130108 3 30100ND111108
1,1-Dichloroethane ug/L 100 115 70-130114 1 30100ND115114
1,1-Dichloroethene ug/L 100 112 70-166109 2 30100ND112109
1,1-Dichloropropene ug/L 100 118 70-130117 1 30100ND118117
1,2,3-Trichlorobenzene ug/L 100 116 70-130117 0 30100ND116117
1,2,3-Trichloropropane ug/L 100 110 70-130104 6 30100ND110104
1,2,4-Trichlorobenzene ug/L 100 116 70-130120 3 30100ND116120
1,2-Dibromo-3-
chloropropane ug/L 100 112 70-130103 8 30100ND112103
1,2-Dibromoethane (EDB)ug/L 100 115 70-130113 2 30100ND115113
1,2-Dichlorobenzene ug/L 100 112 70-130111 1 30100ND112111
1,2-Dichloroethane ug/L 100 105 70-130103 2 301002.3J 108 105
1,2-Dichloropropane ug/L 100 116 70-130111 4 30100ND116111
1,3-Dichlorobenzene ug/L 100 112 70-130108 4 30100ND112108
1,3-Dichloropropane ug/L 100 114 70-130113 1 30100ND114113
1,4-Dichlorobenzene ug/L 100 111 70-130106 4 301002.0J 113 108
2,2-Dichloropropane ug/L 100 105 70-130103 2 30100ND105103
2-Butanone (MEK)ug/L M120015070-130133 2 30200128015801550
2-Chlorotoluene ug/L 100 110 70-130108 1 30100ND110108
2-Hexanone ug/L 200 119 70-130115 3 30200ND239231
4-Chlorotoluene ug/L 100 112 70-130111 2 30100ND112111
4-Methyl-2-pentanone
(MIBK)ug/L 200 120 70-130113 5 3020040.5J 280 267
Acetone ug/L M120014470-130108 4 30200136016501580
Benzene ug/L 100 113 70-148110 2 301007.8 121 118
Bromobenzene ug/L 100 114 70-130113 1 30100ND114113
Bromochloromethane ug/L 100 115 70-130113 2 30100ND115113
Bromodichloromethane ug/L 100 107 70-130100 6 30100ND107100
Bromoform ug/L M11008270-13064 25 30100ND82.0 63.9
Bromomethane ug/L 100 100 70-130101 1 30100ND99.5 101
Carbon tetrachloride ug/L 100 112 70-130109 3 30100ND112109
Chlorobenzene ug/L 100 114 70-146112 2 30100ND114112
Chloroethane ug/L 100 119 70-130109 9 30100ND119109
Chloroform ug/L 100 116 70-130110 6 30100ND116110
Chloromethane ug/L M110013570-130120 12 30100ND135120
cis-1,2-Dichloroethene ug/L 100 117 70-130115 2 30100ND117115
cis-1,3-Dichloropropene ug/L 100 110 70-130107 3 30100ND110107
Dibromochloromethane ug/L 100 105 70-13091 15 30100ND10590.5
Dibromomethane ug/L 100 115 70-130113 1 30100ND115113
Dichlorodifluoromethane ug/L 100 116 70-130112 3 30100ND116112
Diisopropyl ether ug/L 100 118 70-130117 1 30100ND118117
Ethylbenzene ug/L 100 118 70-130114 3 3010017.8 136 132
Hexachloro-1,3-butadiene ug/L 100 118 70-130125 5 30100ND118125
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
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[phone]
Page 31 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2085015MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92352957001
2085016
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
m&p-Xylene ug/L 200 116 70-130112 4 3020012.1 244 235
Methyl-tert-butyl ether ug/L 100 115 70-130114 1 30100ND115114
Methylene Chloride ug/L 100 124 70-130121 3 30100ND124121
Naphthalene ug/L 100 117 70-130118 1 301004.2J 121 122
o-Xylene ug/L 100 114 70-130111 2 301007.3 121 118
p-Isopropyltoluene ug/L 100 116 70-130114 1 30100ND116114
Styrene ug/L 100 117 70-130113 3 30100ND117113
Tetrachloroethene ug/L 100 113 70-130109 3 30100ND113109
Toluene ug/L 100 116 70-155112 3 301009.4 125 121
trans-1,2-Dichloroethene ug/L 100 116 70-130115 1 30100ND116115
trans-1,3-Dichloropropene ug/L 100 110 70-130103 7 30100ND110103
Trichloroethene ug/L 100 117 69-151111 5 30100ND117111
Trichlorofluoromethane ug/L 100 118 70-130118 0 30100ND118118
Vinyl acetate ug/L M120013570-130134 1 30200ND270267
Vinyl chloride ug/L 100 119 70-130119 0 30100ND119119
1,2-Dichloroethane-d4 (S)%99 70-13099
4-Bromofluorobenzene (S)%100 70-13099
Toluene-d8 (S)%100 70-13098
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 32 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
376736
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92353331006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2087241
Associated Lab Samples:92353331006
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L 0.33U 1.0 09/07/17 14:300.33
1,1,1-Trichloroethane ug/L 0.48U 1.0 09/07/17 14:300.48
1,1,2,2-Tetrachloroethane ug/L 0.40U 1.0 09/07/17 14:300.40
1,1,2-Trichloroethane ug/L 0.29U 1.0 09/07/17 14:300.29
1,1-Dichloroethane ug/L 0.32U 1.0 09/07/17 14:300.32
1,1-Dichloroethene ug/L 0.56U 1.0 09/07/17 14:300.56
1,1-Dichloropropene ug/L 0.49U 1.0 09/07/17 14:300.49
1,2,3-Trichlorobenzene ug/L 0.33U 1.0 09/07/17 14:300.33
1,2,3-Trichloropropane ug/L 0.41U 1.0 09/07/17 14:300.41
1,2,4-Trichlorobenzene ug/L 0.35U 1.0 09/07/17 14:300.35
1,2-Dibromo-3-chloropropane ug/L 2.0U 2.0 09/07/17 14:302.0
1,2-Dibromoethane (EDB)ug/L 0.27U 1.0 09/07/17 14:300.27
1,2-Dichlorobenzene ug/L 0.30U 1.0 09/07/17 14:300.30
1,2-Dichloroethane ug/L 0.24U 1.0 09/07/17 14:300.24
1,2-Dichloropropane ug/L 0.27U 1.0 09/07/17 14:300.27
1,3-Dichlorobenzene ug/L 0.24U 1.0 09/07/17 14:300.24
1,3-Dichloropropane ug/L 0.28U 1.0 09/07/17 14:300.28
1,4-Dichlorobenzene ug/L 0.33U 1.0 09/07/17 14:300.33
2,2-Dichloropropane ug/L 0.13U 1.0 09/07/17 14:300.13
2-Butanone (MEK)ug/L 0.96U 5.0 09/07/17 14:300.96
2-Chlorotoluene ug/L 0.35U 1.0 09/07/17 14:300.35
2-Hexanone ug/L 0.46U 5.0 09/07/17 14:300.46
4-Chlorotoluene ug/L 0.31U 1.0 09/07/17 14:300.31
4-Methyl-2-pentanone (MIBK)ug/L 0.33U 5.0 09/07/17 14:300.33
Acetone ug/L 10.0U 25.0 09/07/17 14:3010.0
Benzene ug/L 0.25U 1.0 09/07/17 14:300.25
Bromobenzene ug/L 0.30U 1.0 09/07/17 14:300.30
Bromochloromethane ug/L 0.17U 1.0 09/07/17 14:300.17
Bromodichloromethane ug/L 0.18U 1.0 09/07/17 14:300.18
Bromoform ug/L 0.26U 1.0 09/07/17 14:300.26
Bromomethane ug/L 0.29U 2.0 09/07/17 14:300.29
Carbon tetrachloride ug/L 0.25U 1.0 09/07/17 14:300.25
Chlorobenzene ug/L 0.23U 1.0 09/07/17 14:300.23
Chloroethane ug/L 0.54U 1.0 09/07/17 14:300.54
Chloroform ug/L 0.14U 1.0 09/07/17 14:300.14
Chloromethane ug/L 0.11U 1.0 09/07/17 14:300.11
cis-1,2-Dichloroethene ug/L 0.19U 1.0 09/07/17 14:300.19
cis-1,3-Dichloropropene ug/L 0.13U 1.0 09/07/17 14:300.13
Dibromochloromethane ug/L 0.21U 1.0 09/07/17 14:300.21
Dibromomethane ug/L 0.21U 1.0 09/07/17 14:300.21
Dichlorodifluoromethane ug/L 0.21U 1.0 09/07/17 14:300.21
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
Pace Analytical Services, LLC
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Asheville, NC 28804
[phone]
Page 33 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2087241
Associated Lab Samples:92353331006
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L 0.12U 1.0 09/07/17 14:300.12
Ethylbenzene ug/L 0.30U 1.0 09/07/17 14:300.30
Hexachloro-1,3-butadiene ug/L 0.71U 1.0 09/07/17 14:300.71
m&p-Xylene ug/L 0.66U 2.0 09/07/17 14:300.66
Methyl-tert-butyl ether ug/L 0.21U 1.0 09/07/17 14:300.21
Methylene Chloride ug/L 0.97U 1.0 09/07/17 14:300.97
Naphthalene ug/L 0.24U 1.0 09/07/17 14:300.24
o-Xylene ug/L 0.23U 1.0 09/07/17 14:300.23
p-Isopropyltoluene ug/L 0.31U 1.0 09/07/17 14:300.31
Styrene ug/L 0.26U 1.0 09/07/17 14:300.26
Tetrachloroethene ug/L 0.46U 1.0 09/07/17 14:300.46
Toluene ug/L 0.26U 1.0 09/07/17 14:300.26
trans-1,2-Dichloroethene ug/L 0.49U 1.0 09/07/17 14:300.49
trans-1,3-Dichloropropene ug/L 0.26U 1.0 09/07/17 14:300.26
Trichloroethene ug/L 0.47U 1.0 09/07/17 14:300.47
Trichlorofluoromethane ug/L 0.20U 1.0 09/07/17 14:300.20
Vinyl acetate ug/L 0.35U 2.0 09/07/17 14:300.35
Vinyl chloride ug/L 0.62U 1.0 09/07/17 14:300.62
Xylene (Total)ug/L 0.66U 1.0 09/07/17 14:300.66
1,2-Dichloroethane-d4 (S)%103 70-130 09/07/17 14:30
4-Bromofluorobenzene (S)%101 70-130 09/07/17 14:30
Toluene-d8 (S)%106 70-130 09/07/17 14:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2087242LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 45.550 91 80-125
1,1,1-Trichloroethane ug/L 48.650 97 71-129
1,1,2,2-Tetrachloroethane ug/L 47.150 94 79-124
1,1,2-Trichloroethane ug/L 49.550 99 85-125
1,1-Dichloroethane ug/L 45.950 92 73-126
1,1-Dichloroethene ug/L 44.050 88 66-135
1,1-Dichloropropene ug/L 51.250 102 74-135
1,2,3-Trichlorobenzene ug/L 51.250 102 73-135
1,2,3-Trichloropropane ug/L 47.050 94 75-130
1,2,4-Trichlorobenzene ug/L 50.450 101 75-134
1,2-Dibromo-3-chloropropane ug/L 46.950 94 71-133
1,2-Dibromoethane (EDB)ug/L 50.350 101 83-124
1,2-Dichlorobenzene ug/L 49.350 99 80-133
1,2-Dichloroethane ug/L 45.850 92 67-128
1,2-Dichloropropane ug/L 50.650 101 75-132
1,3-Dichlorobenzene ug/L 49.450 99 77-130
1,3-Dichloropropane ug/L 50.250 100 76-131
1,4-Dichlorobenzene ug/L 49.550 99 78-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
Pace Analytical Services, LLC
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Asheville, NC 28804
[phone]
Page 34 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2087242LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 49.650 99 40-160
2-Butanone (MEK)ug/L 97.7100 98 61-144
2-Chlorotoluene ug/L 47.150 94 74-132
2-Hexanone ug/L 98.8100 99 68-143
4-Chlorotoluene ug/L 49.250 98 76-133
4-Methyl-2-pentanone (MIBK)ug/L 100100 100 72-135
Acetone ug/L 105100 105 48-146
Benzene ug/L 49.650 99 80-125
Bromobenzene ug/L 50.450 101 75-125
Bromochloromethane ug/L 48.350 97 71-125
Bromodichloromethane ug/L 47.950 96 78-124
Bromoform ug/L 42.650 85 71-128
Bromomethane ug/L 52.050 104 40-160
Carbon tetrachloride ug/L 49.750 99 69-131
Chlorobenzene ug/L 48.450 97 81-122
Chloroethane ug/L 46.450 93 39-148
Chloroform ug/L 46.850 94 73-127
Chloromethane ug/L 51.350 103 44-146
cis-1,2-Dichloroethene ug/L 46.450 93 74-124
cis-1,3-Dichloropropene ug/L 52.550 105 72-132
Dibromochloromethane ug/L 45.950 92 78-125
Dibromomethane ug/L 48.850 98 82-120
Dichlorodifluoromethane ug/L 43.250 86 34-157
Diisopropyl ether ug/L 51.850 104 69-135
Ethylbenzene ug/L 47.950 96 79-121
Hexachloro-1,3-butadiene ug/L 49.250 98 72-131
m&p-Xylene ug/L 93.4100 93 81-124
Methyl-tert-butyl ether ug/L 50.950 102 74-131
Methylene Chloride ug/L 46.550 93 64-133
Naphthalene ug/L 51.650 103 73-133
o-Xylene ug/L 46.450 93 79-131
p-Isopropyltoluene ug/L 49.750 99 80-131
Styrene ug/L 47.750 95 84-126
Tetrachloroethene ug/L 48.150 96 78-122
Toluene ug/L 48.850 98 80-121
trans-1,2-Dichloroethene ug/L 46.850 94 71-127
trans-1,3-Dichloropropene ug/L 45.950 92 69-141
Trichloroethene ug/L 52.850 106 78-122
Trichlorofluoromethane ug/L 45.950 92 53-137
Vinyl acetate ug/L 104100 104 40-160
Vinyl chloride ug/L 46.550 93 58-137
Xylene (Total)ug/L 140150 93 81-126
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%97 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
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[phone]
Page 35 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2087983MATRIX SPIKE SAMPLE:
MSSpike
Result
92354056001
1,1,1,2-Tetrachloroethane ug/L 19.920 99 70-130ND
1,1,1-Trichloroethane ug/L 23.320 117 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.520 102 70-130ND
1,1,2-Trichloroethane ug/L 22.020 110 70-130ND
1,1-Dichloroethane ug/L 22.120 111 70-130ND
1,1-Dichloroethene ug/L 22.320 112 70-166ND
1,1-Dichloropropene ug/L 24.520 122 70-130ND
1,2,3-Trichlorobenzene ug/L 21.920 110 70-130ND
1,2,3-Trichloropropane ug/L 20.420 102 70-130ND
1,2,4-Trichlorobenzene ug/L 21.420 107 70-130ND
1,2-Dibromo-3-chloropropane ug/L 18.520 93 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.520 107 70-130ND
1,2-Dichlorobenzene ug/L 20.720 103 70-130ND
1,2-Dichloroethane ug/L 21.720 108 70-130ND
1,2-Dichloropropane ug/L 23.620 118 70-130ND
1,3-Dichlorobenzene ug/L 20.920 105 70-130ND
1,3-Dichloropropane ug/L 22.220 111 70-130ND
1,4-Dichlorobenzene ug/L 21.220 106 70-130ND
2,2-Dichloropropane ug/L 23.720 119 70-130ND
2-Butanone (MEK)ug/L 38.840 97 70-130ND
2-Chlorotoluene ug/L 20.720 104 70-130ND
2-Hexanone ug/L 41.040 103 70-130ND
4-Chlorotoluene ug/L 21.220 106 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 42.240 105 70-130ND
Acetone ug/L 40.440 101 70-130ND
Benzene ug/L 23.020 115 70-148ND
Bromobenzene ug/L 21.620 108 70-130ND
Bromochloromethane ug/L 23.620 118 70-130ND
Bromodichloromethane ug/L 22.020 110 70-130ND
Bromoform ug/L 18.420 92 70-130ND
Bromomethane ug/L 26.020 130 70-130ND
Carbon tetrachloride ug/L 23.420 117 70-130ND
Chlorobenzene ug/L 21.720 109 70-146ND
Chloroethane ug/L 22.920 115 70-130ND
Chloroform ug/L 22.620 113 70-130ND
Chloromethane ug/L 26.7 M12013370-130ND
cis-1,2-Dichloroethene ug/L 22.420 112 70-130ND
cis-1,3-Dichloropropene ug/L 23.320 117 70-130ND
Dibromochloromethane ug/L 20.020 100 70-130ND
Dibromomethane ug/L 22.420 112 70-130ND
Dichlorodifluoromethane ug/L 21.120 106 70-130ND
Diisopropyl ether ug/L 22.120 110 70-130ND
Ethylbenzene ug/L 22.120 111 70-130ND
Hexachloro-1,3-butadiene ug/L 21.820 109 70-130ND
m&p-Xylene ug/L 42.440 106 70-130ND
Methyl-tert-butyl ether ug/L 22.120 110 70-130ND
Methylene Chloride ug/L 21.120 105 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 36 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2087983MATRIX SPIKE SAMPLE:
MSSpike
Result
92354056001
Naphthalene ug/L 20.420 102 70-130ND
o-Xylene ug/L 20.920 105 70-130ND
p-Isopropyltoluene ug/L 21.520 108 70-130ND
Styrene ug/L 21.420 107 70-130ND
Tetrachloroethene ug/L 21.420 107 70-130ND
Toluene ug/L 23.320 116 70-155ND
trans-1,2-Dichloroethene ug/L 22.820 114 70-130ND
trans-1,3-Dichloropropene ug/L 20.620 103 70-130ND
Trichloroethene ug/L 24.420 122 69-151ND
Trichlorofluoromethane ug/L 24.420 122 70-130ND
Vinyl acetate ug/L 45.840 114 70-130ND
Vinyl chloride ug/L 23.320 116 70-130ND
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92354056002
2087984SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L 0.33U 30ND
1,1,1-Trichloroethane ug/L 0.48U 30ND
1,1,2,2-Tetrachloroethane ug/L 0.40U 30ND
1,1,2-Trichloroethane ug/L 0.29U 30ND
1,1-Dichloroethane ug/L 0.32U 30ND
1,1-Dichloroethene ug/L 0.56U 30ND
1,1-Dichloropropene ug/L 0.49U 30ND
1,2,3-Trichlorobenzene ug/L 0.33U 30ND
1,2,3-Trichloropropane ug/L 0.41U 30ND
1,2,4-Trichlorobenzene ug/L 0.35U 30ND
1,2-Dibromo-3-chloropropane ug/L 2.0U 30ND
1,2-Dibromoethane (EDB)ug/L 0.27U 30ND
1,2-Dichlorobenzene ug/L 0.30U 30ND
1,2-Dichloroethane ug/L 0.24U 30ND
1,2-Dichloropropane ug/L 0.27U 30ND
1,3-Dichlorobenzene ug/L 0.24U 30ND
1,3-Dichloropropane ug/L 0.28U 30ND
1,4-Dichlorobenzene ug/L 0.33U 30ND
2,2-Dichloropropane ug/L 0.13U 30ND
2-Butanone (MEK)ug/L 0.96U 30ND
2-Chlorotoluene ug/L 0.35U 30ND
2-Hexanone ug/L 0.46U 30ND
4-Chlorotoluene ug/L 0.31U 30ND
4-Methyl-2-pentanone (MIBK)ug/L 0.33U 30ND
Acetone ug/L 10.0U 30ND
Benzene ug/L 0.25U 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 37 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92354056002
2087984SAMPLE DUPLICATE:
Bromobenzene ug/L 0.30U 30ND
Bromochloromethane ug/L 0.17U 30ND
Bromodichloromethane ug/L 0.18U 30ND
Bromoform ug/L 0.26U 30ND
Bromomethane ug/L 0.29U 30ND
Carbon tetrachloride ug/L 0.25U 30ND
Chlorobenzene ug/L 0.23U 30ND
Chloroethane ug/L 0.54U 30ND
Chloroform ug/L 0.14U 30ND
Chloromethane ug/L 0.11U 30ND
cis-1,2-Dichloroethene ug/L 0.19U 30ND
cis-1,3-Dichloropropene ug/L 0.13U 30ND
Dibromochloromethane ug/L 0.21U 30ND
Dibromomethane ug/L 0.21U 30ND
Dichlorodifluoromethane ug/L 0.21U 30ND
Diisopropyl ether ug/L 0.12U 30ND
Ethylbenzene ug/L 0.30U 30ND
Hexachloro-1,3-butadiene ug/L 0.71U 30ND
m&p-Xylene ug/L 0.66U 30ND
Methyl-tert-butyl ether ug/L 0.21U 30ND
Methylene Chloride ug/L 0.97U 30ND
Naphthalene ug/L 0.24U 30ND
o-Xylene ug/L 0.23U 30ND
p-Isopropyltoluene ug/L 0.31U 30ND
Styrene ug/L 0.26U 30ND
Tetrachloroethene ug/L 0.46U 30ND
Toluene ug/L 0.26U 30ND
trans-1,2-Dichloroethene ug/L 0.49U 30ND
trans-1,3-Dichloropropene ug/L 0.26U 30ND
Trichloroethene ug/L 0.47U 30ND
Trichlorofluoromethane ug/L 0.20U 30ND
Vinyl acetate ug/L 0.35U 30ND
Vinyl chloride ug/L 0.62U 30ND
Xylene (Total)ug/L 0.66U 30ND
1,2-Dichloroethane-d4 (S)%104 0103
4-Bromofluorobenzene (S)%99 1101
Toluene-d8 (S)%105 1106
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 38 of 44
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 39 of 44
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92353331
LANDFILL MW'S 8/29
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92353331001 MW-1
92353331002 MW-2
92353331003 MW-3
92353331004 MW-4
92353331001 377234 377501MW-1 EPA 3010A EPA 6010
92353331002 377234 377501MW-2 EPA 3010A EPA 6010
92353331003 377234 377501MW-3 EPA 3010A EPA 6010
92353331004 377234 377501MW-4 EPA 3010A EPA 6010
92353331006 377234 377501EQUIP BLK EPA 3010A EPA 6010
92353331001 377063 377191MW-1 EPA 7470 EPA 7470
92353331002 375868 376427MW-2 EPA 7470 EPA 7470
92353331003 375868 376427MW-3 EPA 7470 EPA 7470
92353331004 375868 376427MW-4 EPA 7470 EPA 7470
92353331006 375868 376427EQUIP BLK EPA 7470 EPA 7470
92353331001 376144MW-1 EPA 8260
92353331002 376144MW-2 EPA 8260
92353331003 376144MW-3 EPA 8260
92353331004 376144MW-4 EPA 8260
92353331005 376357TVL BLK EPA 8260
92353331006 376736EQUIP BLK EPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/14/2017 01:26 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 40 of 44
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