5603_McDowellCountyMSWLF_GWMR_20171025

December 2017
Old Fort Industrial Solid Waste Landfill
Permit Number 56-03
McDowell County, North Carolina
2017 Annual Water Quality Monitoring Report
Prepared for ABF Environmental

Project Number: C61476-01.01.02
\\Asheville1\Asheville\Projects\ABF Environmental\Report\2017\Final 5603Dec2017WaterQualityReport.docx
December 2017
Old Fort Industrial Solid Waste Landfill
Permit Number 56-03
McDowell County, North Carolina
2017 Annual Water Quality Monitoring Report

Alec Macbeth, PG
Project Geologist

Prepared for
ABF Environmental
28200 Orchard Lake Road, Suite 101 Farmington Hills, Michigan 48334
Prepared by
Anchor QEA of North Carolina, PLLC
231 Haywood Street Asheville, North Carolina

2017 Annual Water Quality Report i December 2017
TABLE OF CONTENTS
1 Introduction ................................................................................................................................ 1
2 Methods ....................................................................................................................................... 2
2.1 Groundwater and Surface Water Sampling .............................................................................................. 2
2.1.1 Groundwater Purging and Sampling Methods ........................................................................ 2
2.1.2 Surface Water Samples ..................................................................................................................... 3
2.2 Sample Handling, Documentation, and Analysis .................................................................................... 3
3 Findings ........................................................................................................................................ 5
3.1 Groundwater Samples ....................................................................................................................................... 5
3.1.1 RCRA Metals .......................................................................................................................................... 5
3.1.2 Field Parameters .................................................................................................................................. 5
3.2 Surface Water Samples ..................................................................................................................................... 5
3.2.1 RCRA Metals .......................................................................................................................................... 5
3.2.2 Field Parameters .................................................................................................................................. 6
4 Summary ...................................................................................................................................... 7
4.1 Future Activities ................................................................................................................................................... 7
5 References ................................................................................................................................... 8

TABLES
Table 1 Summary of Laboratory Analyses Performed on Samples
Table 2 Summary of Analytical Results
FIGURES
Figure 1 Site Location Map
Figure 2 Sample Location Map
APPENDICES
Appendix A Sampling Logs and Equipment Documentation and Instrument Calibration Data
Sheets
Appendix B Report of Laboratory Analysis and Chain-of-Custody Documentation

2017 Annual Water Quality Report ii December 2017
ABBREVIATIONS
µS/cm microsiemens per centimeter
DEQ North Carolina Department of Environmental Quality
DO dissolved oxygen
DWM North Carolina Department of Environmental Quality, Division of Waste
Management
EDD Electronic Data Deliverable
EPA U.S. Environmental Protection Agency
IAC International Automotive Components
IMAC interim maximum allowable concentration
MDL method detection limit
mg/L milligrams per liter
MRL method reporting limit
mV millivolts
NCAC North Carolina Administrative Code
NTU nephelometric turbidity unit
ORP oxidation reduction potential
RCRA Resource Conservation and Recovery Act
SU Standard Unit
SWSL Solid Waste Section Limit

2017 Annual Water Quality Report 1 December 2017
1 Introduction
The International Automotive Components (IAC) Group North America owns and manages the Old
Fort Industrial Solid Waste Landfill (Old Fort Landfill, Site) located on State Road 1240 in Old Fort,
McDowell County, North Carolina (Figure 1). The landfill is approximately 86 acres in size and is
located approximately 5 miles southeast of the IAC plant.
Previously, the landfill was owned and operated by Collins & Aikman for the disposal of solid waste
related to carpet products. In 2007, IAC acquired the landfill and has not used it for waste disposal
since the acquisition. IAC has subsequently closed the Old Fort Landfill. As a result, a Revised
Workplan for Landfill Investigation and Closure (RJN Environmental, Inc. [RJN] 2010) and a Final
Investigation Report (RJN 2011) were prepared by RJN, to initiate landfill closure activities. The Final
Investigation Report summarizes landfill closure investigation procedures, completed activities, and
sampled media analytical results.
State regulations for landfills are enforced by the North Carolina Department of Environmental
Quality (DEQ), Division of Waste Management (DWM). The subject landfill is permitted by the DWM
under Permit No. 56-03.
This report is being submitted in general accordance with (1) our proposal to ABF Environmental
dated August 21, 2017, and (2) requirements stipulated in the DEQ Solid Waste Management Rules,
Title 15A, Subchapter 13B, Section .0500 of the North Carolina Administrative Code (15A NCAC 13B
.0500).
The water quality monitoring network for the Old Fort Landfill consists of five compliance monitoring
wells (upgradient monitoring wells MW-1 and MW-1A, and downgradient monitoring wells MW-2,
MW-3, and MW-4) and four surface water sampling locations (SW-1, SW-2, SW-3, and SW-4),
associated with various tributaries and drainage points on Site.
This 2017 Annual Water Quality Report describes the groundwater and surface water quality
sampling event performed on October 25, 2017. Samples associated with the landfill were collected
by personnel from Anchor QEA of North Carolina, PLLC (Anchor QEA), and analyzed by Pace
Analytical Services, Inc. (Pace). This water quality monitoring report was prepared by Anchor QEA.

2017 Annual Water Quality Report 2 December 2017
2 Methods
2.1 Groundwater and Surface Water Sampling
Old Fort Landfill monitoring wells (MW-1, MW-2, MW-3, and MW-4) and surface water sample
locations (SW-1, SW-2, SW-3, and SW-4) were sampled by Anchor QEA personnel on October 25,
2017 (Table 1). MW-1A, located adjacent to MW-1, was not sampled during this event, to maintain
consistency with historical sampling events. Approximate sample locations are depicted in Figure 2.
Table 1 provides a summary of all groundwater and surface water samples collected and the analyses
performed on each sample. Field sampling logs are included in Appendix A.
2.1.1 Groundwater Purging and Sampling Methods
Monitoring wells MW-1, MW-3, and MW-4 were purged and sampled using low-flow techniques in
accordance with the procedures described in “Low-Flow (Minimal Drawdown) Ground-Water
Sampling Procedures” (U.S. Environmental Protection Agency [EPA] 1996). During purging, the pH,
specific conductivity, dissolved oxygen (DO), oxidation reduction potential (ORP), turbidity, and
temperature were measured and recorded approximately every 3 minutes. Well purging continued
until these parameters stabilized, as determined by three successive readings in which each
parameter was within a set range of values, as follows:
• pH +/- 0.1 unit
• Specific conductivity +/- 3 percent
• Temperature +/- 10 percent
• DO +/- 10 percent
• Turbidity +/- 10 percent
• ORP +/- 10 millivolts
Once these parameters stabilized, a groundwater sample was collected in laboratory-supplied
sample containers by Anchor QEA technicians wearing new nitrile gloves.
Monitoring well MW-2 was purged and sampled using a new disposable polyethylene bailer. This
well was not sampled using low-flow techniques, due to poor well access. The monitoring well was
purged of three successive well volumes prior to sample collection. During purging, the pH, specific
conductivity, DO, ORP, turbidity, and temperature were measured and recorded at the start of
purging and after each consecutive well volume was purged. After the third consecutive well volume
was purged, technicians collected a sample in laboratory-supplied sample containers, wearing new
nitrile gloves.

2017 Annual Water Quality Report 3 December 2017
2.1.2 Surface Water Samples
Surface water samples SW-1 and SW-2 were collected from locations along an unnamed tributary,
downstream of the landfill, as indicated by signage demarking monitoring locations adjacent to the
surface water. Surface water sample SW-3 was collected from a location along the same tributary,
indicated by respective signage. SW-4 was collected from a tributary in close proximity to monitoring
well MW-4, also indicated by signage, and was located downstream of a stormwater discharge pipe
that directs runoff away from the landfill cap.
2.2 Sample Handling, Documentation, and Analysis
Water quality parameters and water level measurements are presented in the field logs in Appendix
A, and in Section 3 of this report, as well as in the Electronic Data Deliverable (EDD) submitted
separately from this report. Following sample collection, groundwater and surface water samples
were immediately placed on ice in a sample cooler. Once all samples were collected, they were
transported to Pace, a laboratory certified in North Carolina. Anchor QEA submitted the samples for
analysis for Resource Conservation and Recovery Act (RCRA) metals using EPA Methods 200.7 and
245.1.
Proper chain-of-custody documentation procedures were followed during collection and transport of
collected samples. The Report of Laboratory Analysis and chain-of-custody documentation are
included in Appendix B. Laboratory analyses performed on the samples are summarized in Table 1.
Detections of analytes are reported as follows:
• Non-Detects—Constituents of interest that are not detected are reported to the laboratory
method detection limit (MDL), which is the minimum concentration of a substance that can be
reported by a laboratory with 99 percent confidence that the concentration is greater than
zero.
• Solid Waste Section Limit (SWSL)—The lowest concentration of an analyte that can be
quantitatively determined with suitable precision and accuracy, as established by the DWM
Solid Waste Section. Concentrations below the respective SWSLs are not discussed in the text
of this report unless they exceed constituent-specific water quality standards.
• “J” Flag— The method reporting limit (MRL) is the minimum concentration of a target analyte
that can be accurately determined by the referenced method. (The MRL is referred to as the
Practical Quantitation Limit in the Pace Report of Laboratory Analysis.) If the reported
concentration is greater than the MDL, but less than the MRL, then the analytical result is an
estimate and is flagged with a “J” qualifier. If the reported concentration is greater than the
MRL, but less than the SWSL, then the analytical result is an estimate and is flagged with an
italicized “J” qualifier.
• 2L standards—Detected concentrations of analytes in groundwater samples are compared to
the current groundwater quality standards specified in 15A NCAC 2L.0202, referred to as 2L

2017 Annual Water Quality Report 4 December 2017
standards. Constituents with no established 2L standard are compared to the interim
maximum allowable concentrations (IMACs), in accordance with 15A NCAC 02L .0202 [c].
• 2B standards—Detected concentrations of analytes in surface water samples are compared to
15A NCAC 2B surface water quality standards, referred to as 2B standards.
Table 2 presents analytical results for all analytes detected in groundwater and surface water
samples, and identifies analytes detected above their established SWSLs, 2L standards (including
IMACs, if applicable), or 2B standards.
In the EDD (provided to the DEQ as a separate document), the identification of a well (“WELL ID” in
the table) consists of the name of the well prefaced by the unhyphenated facility permit number. For
example, monitoring well MW-1 is identified in the EDD as “5603-MW1.” In the tables and figures of
this report, however, the identification of a well consists of the name of the well without the facility
permit number.

2017 Annual Water Quality Report 5 December 2017
3 Findings
The laboratory analytical results and field parameter data for the groundwater and surface water
samples collected at the Old Fort Landfill are provided in the report of laboratory analysis issued by
Pace, included as Appendix B. In addition, all laboratory results are summarized in the EDD format as
specified by the DWM Solid Waste Section on May 5, 2010.
3.1 Groundwater Samples
The following subsections summarize the detections of RCRA metals and field parameters in
groundwater.
3.1.1 RCRA Metals
Arsenic and barium were detected in one or more groundwater samples collected from the
monitoring wells. All detections were reported at concentrations below the SWSL. Metals were not
detected at or above their respective 2L standards.
3.1.2 Field Parameters
The field pH readings obtained from the groundwater samples collected from the monitoring wells,
with the exception of MW-1, were below the range of 6.5 to 8.5 Standard Units (SUs) specified in 15A
NCAC 02L .0202[c] (Table 2).
Specific conductivity values obtained from the groundwater samples ranged from 22 microsiemens
per centimeter (µS/cm, MW-4) to 81 µS/cm (MW-1). DO concentrations ranged from 2.25 milligrams
per liter (mg/L, MW-2) to 6.51 mg/L (MW-3). ORP values obtained from the groundwater samples
ranged from -77.4 millivolts (mV, MW-1) to 276.4 mV (MW-4). Turbidity values ranged from 7.29
nephelometric turbidity units (NTUs, MW-3) to 10.9 NTUs (MW-4). These field parameters do not
have established groundwater standards. A full summary of field parameter data is presented in
Table 2.
3.2 Surface Water Samples
The following subsections summarize the detections of RCRA metals and field parameters in surface
water.
3.2.1 RCRA Metals
Barium and chromium were detected in one or more collected surface water samples. Barium was
detected in three surface water samples (SW-1, SW-2, and SW-4) at concentrations above the SWSL,
but well below the applicable 2B standard. Barium was detected in the sample from SW-3 at an
estimated concentration below the SWSL and applicable 2B standard. Chromium was detected at a

2017 Annual Water Quality Report 6 December 2017
concentration of 15.8 micrograms per liter in surface water sample SW-3. This detection was above
the SWSL, but below the 2B standard established for chromium. A full summary of detections can be
found in Table 2.
3.2.2 Field Parameters
The field pH reading of 5.66 SU measured in surface water sample SW-4 (Table 2) was outside the
established 2B standard range of 6.0 to 9.0 SU at the time of sample collection. All other surface
water pH measurements were within the 2B standard range.
DO readings measured in the surface water samples ranged from 6.86 mg/L (SW-4) to 11.69 mg/L
(SW-3). All DO readings are in compliance with the established 2B standard for DO.
None of the turbidity readings measured in the four surface water samples exceeded the 2B standard
of 25 NTUs. Turbidity readings ranged from 4.96 NTUs (SW-4) to 9.35 NTUs (SW-3).
Specific conductivity readings measured in the surface water samples ranged from 24 µS/cm (SW-3)
to 90 µS/cm (SW-1). ORP values measured in the surface water samples ranged from 67.3 mV (SW-4)
to 208.8 mV (SW-3). Specific conductivity and ORP do not have established 2B standards. A full
summary of field parameters collected in the surface water samples can be found in Table 2.

2017 Annual Water Quality Report 7 December 2017
4 Summary
Anchor QEA collected groundwater and surface water samples on October 25, 2017, at the Old Fort
Landfill.
Tables 1 and 2, the field logs in Appendix A, the Pace Report of Laboratory Analysis in Appendix B,
and the EDD provide a detailed presentation of analytical results and field data representing the
groundwater and surface water quality at the Old Fort Landfill. Analytical results are summarized as
follows:
• Groundwater
‒ pH—Below the 2L standard range of 6.5 to 8.5 SU in samples collected from monitoring
wells MW-2, MW-3, and MW-4
‒ Metals—Barium was detected in the four samples at concentrations below the 2L
standard. Arsenic was detected in the sample collected from MW-2 at a concentration
below the 2L standard.
• Surface water
‒ pH—Below the 2B standard range in the sample collected from surface water location
SW-4
‒ Metals—Barium was detected above the SWSL, but well below the respective 2B
standard, in the samples collected from surface water locations SW-1, SW-2, and SW-4.
Barium was detected in the sample from SW-3 at an estimated concentration below the
SWSL and applicable 2B standard. Chromium was detected at a concentration above
the SWSL, but below the 2B surface water standard in the sample collected from surface
water location SW-3.
4.1 Future Activities
Anchor QEA will continue to collect groundwater and surface water samples and report the analytical
results for monitoring on an annual basis at the Old Fort Landfill. The next water quality sampling
event is scheduled for October 2018.

2017 Annual Water Quality Report 8 December 2017
5 References
DENR (Department of Environment and Natural Resources, Division of Waste Management, Solid
Waste Section), 2006. New Guidelines for Electronic Submittal of Environmental Monitoring
Data. October 27, 2006.
DENR, 2007. Addendum to October 27, 2006, NC SWS Memorandum Regarding New Guidelines for
Electronic Submittal of Environmental Data. February 23, 2007.
EPA (U.S. Environmental Protection Agency), 1996. “Low-Flow (Minimal Drawdown) Ground-Water
Sampling Procedures.” Groundwater Issues. April 1996.
RJN (RJN Environmental, Inc.), 2010. Revised Workplan for Landfill Investigation and Closure.
November 4, 2010.
RJN, 2011. Final Investigation Report. June 7, 2011.

Tables
Table 1
Summary of Laboratory Analyses Performed on Samples
GROUNDWATER SAMPLES
EPA 200.7 EPA 245.1
56-03 MW-1 10/25/2017 X X
56-03 MW-2 10/25/2017 X X
56-03 MW-3 10/25/2017 X X
56-03 MW-4 10/25/2017 X X
SURFACE WATER SAMPLES
EPA 200.7 EPA 245.1
56-03 SW-1 10/25/2017 X X
56-03 SW-2 10/25/2017 X X
56-03 SW-3 10/25/2017 X X
56-03 SW-4 10/25/2017 X X
Notes:
Metals: Analysis includes the following RCRA metals: arsenic, barium, cadmium, chromium, lead, mercury, selenium, and
silver, in accordance with permit requirements.
Well ID Collect Date
Metals
Sample ID Collect Date
Metals
Facility Permit
Facility Permit
2017 Annual Water Quality Monitoring Report
Old Fort Industrial Solid Waste Landfill
December 2017
Page 1 of 1
Table 2
Summary of Analytical Results
Parameter Arsenic Barium Chromium Temperature
Specific
Conductivity
Dissolved
Oxygen pH
Oxidation-
Reduction
Potential Turbidity
CAS Number 7440-38-2 7440-39-3 7440-47-3 SW325 SW323 7782-44-7 SW320 SW336 SW330
SWS ID 14 15 51 325 323 356 320 336 330
Units µg/L µg/L µg/L °Celsius µS/cm mg/L SU mV NTU
Sample ID Collect Date Result Result Result Result Result Result Result Result Result
MW-1 10/25/2017 5.0 U 9.2 J 2.5 U 15.03 81 3.62 7.01 -77.4 9.75
MW-2 10/25/2017 5.0 J 38.5 J 2.5 U 12.75 75 2.25 6.09 50.7 8.46
MW-3 10/25/2017 5.0 U 94.8 J 2.5 U 12.47 52 6.51 5.57 242.2 7.29
MW-4 10/25/2017 5.0 U 31.0 J 2.5 U 14.15 22 3.93 4.97 276.4 10.9
SW-1 10/25/2017 5.0 U 129 2.5 U 11.61 90 11.34 6.31 81.1 6.35
SW-2 10/25/2017 5.0 U 130 2.5 U 11.62 83 10.97 6.52 91.9 8.44
SW-3 10/25/2017 5.0 U 12.6 J 15.8 11.07 24 11.69 6.09 208.8 9.35
SW-4 10/25/2017 5.0 U 335 2.5 U 13.90 85 6.86 5.66 67.3 4.96
MDL 5.0 5.0 2.50 NA NA NA NA NA NA
MRL 10.0 10.0 5.0 NA NA NA NA NA NA
SWSL 10 100 10 NE NE NE NE NE NE
2L 700 700 10 NE NE NE 6.5-8.5 NE NE
IMAC NE NE NE NE NE NE NE NE NE
2B 10 200,000 35 NE NE > 5.0 mg/L 6.0-9.0 NE 25
Notes:
Parameters Only detected constituents are listed on this table. Please refer to the Pace Report of Laboratory Analysis (Appendix B) for further details.
Lab Method The EPA approved analytical method used to analyze the constituents.
CAS Number A unique number assigned by the Chemical Abstracts Service (CAS) to all identified parameters
SWS ID Solid Waste Section parameter Identification Number
Units
RCRA Resource Conservation and Recovery Act
MDL
MRL
SWSL
U A laboratory data qualifier used for parameters not detected at concentrations above the MDL
J A laboratory data qualifier used for parameters detected at estimated concentrations above the MDL but below the MRL and SWSL
J Assigned by Anchor QEA to reflect a detected concentration that is greater than the MRL and MDL but less than the SWSL
2L
IMAC Interim maximum allowable concentration. IMAC concentrations are listed in Appendix #1 of the 2L standards.
2B
NE not established
NA not applicable
129 A bold entry Indicates a result in exceedance of the SWSL
5.57 A shaded cell indicates the result is in exceedance of the 2L standard, IMAC, GWP Standard, or 2B standard.
40200.7, 245.1Laboratory CertificationLaboratory Methods
The method reporting limit, which is the minimum concentration of a target analyte that can be accurately determined by the referenced method. The MRL is also
represented as the PQL in the Pace Laboratory Report of Analysis.
Micrograms per liter (µg/L) for analytical results, Standard Units (SU) for pH, nephelometric turbidity units (NTU) for turbidity, and milligrams per liter (mg/L) for
dissolved oxygen
Groundwater standards from North Carolina Administrative Code, Title 15A: Department of Environmental Quality, Subchapter 2L - Groundwater Classifications and
Standards (Amended April 1, 2013)
Surface water standard, per North Carolina Administrative Code, Title 15A: Department of Environmental Quality, Subchapter 2B - Surface Water and Wetland
Standards (last amended March, 2016), or the standard obtained from National Criteria per the EPA table (current as of May 15, 2013)
The method detection limit, which is the minimum concentration of a substance that can be measured and reported with 99% confidence that the
analyte concentration is greater than zero
Solid Waste Section Limit. This limit (identified by the DEQ) is the lowest amount of analyte in a sample that can be quantitatively determined with
suitable precision and accuracy
Field Parameters
5445 (pH only)
Groundwater Samples
Surface Water Samples
Metals (RCRA)
2017 Annual Water Quality Monitoring Report
Old Fort Industrial Solid Waste Landfill
December 2017
Page 1 of 1

Figures
[0 2,000
Feet
LEGEND:
Landfill Property Boundary
Publish Date: 2017/12/20, 9:29 AM | User: alesueurFilepath: \\Asheville1\Asheville\Projects\ABF Environmental\Figures\2017\Figure 1 Site Location Map.mxd
SOURCES:Basemap: National Geographic 7.5 Minute TopographicMaps, Old Fort Quandrangle (1994), Marion WestQuadrangle (1994), Moffitt Hill Quadrangle (1994), andSugar Hill Quadrangle (1987)
Figure 1Site Location Map
Old Fort Landfill - Permit Number 56-03State Road 1240, Old Fort, McDowell County, North Carolina
!U!U!U
!U
!U
#*
#*
#*
#*
MW-1A
MW-1MW-4
MW-2
MW-3 SW-4
SW-3
SW-2
SW-1
Brevard CreekBrevard Creek142014801560
13601520
15401540
1420
14
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15001400Unnamed TributaryUnnamed TributaryPublish Date: 2017/12/20, 9:34 AM | User: alesueurFilepath: \\Asheville1\Asheville\Projects\ABF Environmental\Figures\2017\Figure 2 - Sample Location Map.mxd
[
0 300
Feet
NOTES:1. Sample locations areapproximate.2. Location of Unnamed Tributaryis approximate.
Figure 2Sample Location Map
Old Fort Landfill - Permit Number 56-03State Road 1240, Old Fort, McDowell County, North Carolina
LEGEND:
#*Approximate Surface Water
Sample Location
!U Approximate Monitoring WellLocation
Topographic Contours(20-Foot Interval)
Streams
Landfill Property Boundary
SOURCES:1. Basemap - NC OneMap 20132. Parcel and Stream - McDowellCounty GIS3. Contour Lines - NC Lidar 2007

Appendix A
Sampling Logs and Equipment
Documentation and Instrument
Calibration Data Sheets

Appendix B
Report of Laboratory Analysis and
Chain-of-Custody Documentation
#=CL#
November 07, 2017
LIMS USE: FR - BRIAN GANT
LIMS OBJECT ID: 92360630
92360630
Project:
Pace Project No.:
RE:
Brian Gant
Anchor QEA
231 Haywood Street
Asheville, NC 28804
Old Fort Landfill
Dear Brian Gant:
Enclosed are the analytical results for sample(s) received by the laboratory on October 25, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Revised Report. MDLs and J-Flags added.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lorri Patton
[e-mail]
Project Manager
1(828)254-7176
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 20
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92360630
Old Fort Landfill
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 20
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92360630
Old Fort Landfill
Lab ID Sample ID Matrix Date Collected Date Received
92360630001 MW-1 Water 10/25/17 13:51 10/25/17 14:50
92360630002 MW-2 Water 10/25/17 12:00 10/25/17 14:50
92360630003 MW-3 Water 10/25/17 11:17 10/25/17 14:50
92360630004 MW-4 Water 10/25/17 10:12 10/25/17 14:50
92360630005 SW-1 Water 10/25/17 12:05 10/25/17 14:50
92360630006 SW-2 Water 10/25/17 12:10 10/25/17 14:50
92360630007 SW-3 Water 10/25/17 11:24 10/25/17 14:50
92360630008 SW-4 Water 10/25/17 10:26 10/25/17 14:50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 20
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92360630
Old Fort Landfill
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92360630001 MW-1 EPA 200.7 7 PASI-ASH1
EPA 245.1 1 PASI-AWAB
92360630002 MW-2 EPA 200.7 7 PASI-ASH1
EPA 245.1 1 PASI-AWAB
92360630003 MW-3 EPA 200.7 7 PASI-ASH1
EPA 245.1 1 PASI-AWAB
92360630004 MW-4 EPA 200.7 7 PASI-ASH1
EPA 245.1 1 PASI-AWAB
92360630005 SW-1 EPA 200.7 7 PASI-ASH1
EPA 245.1 1 PASI-AWAB
92360630006 SW-2 EPA 200.7 7 PASI-ASH1
EPA 245.1 1 PASI-AWAB
92360630007 SW-3 EPA 200.7 7 PASI-ASH1
EPA 245.1 1 PASI-AWAB
92360630008 SW-4 EPA 200.7 7 PASI-ASH1
EPA 245.1 1 PASI-AWAB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92360630
Old Fort Landfill
Sample:MW-1 Lab ID:92360630001 Collected:10/25/17 13:51 Received:10/25/17 14:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7200.7 MET ICP
Arsenic ND ug/L 10/30/17 14:41 7440-38-210/27/17 14:1010.0 5.0 1
Barium 9.2 ug/L 10/30/17 14:41 7440-39-310/27/17 14:105.0 2.5 1
Cadmium ND ug/L 10/30/17 14:41 7440-43-910/27/17 14:101.0 0.50 1
Chromium ND ug/L 10/30/17 14:41 7440-47-310/27/17 14:105.0 2.5 1
Lead ND ug/L 10/30/17 14:41 7439-92-110/27/17 14:105.0 2.5 1
Selenium ND ug/L 10/30/17 14:41 7782-49-210/27/17 14:1010.0 5.0 1
Silver ND ug/L 10/30/17 14:41 7440-22-410/27/17 14:105.0 2.5 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1245.1 Mercury
Mercury ND ug/L 10/31/17 13:26 7439-97-610/25/17 23:450.20 0.070 1
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92360630
Old Fort Landfill
Sample:MW-2 Lab ID:92360630002 Collected:10/25/17 12:00 Received:10/25/17 14:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7200.7 MET ICP
Arsenic 5.0J ug/L 10/30/17 14:51 7440-38-210/27/17 14:1010.0 5.0 1
Barium 38.5 ug/L 10/30/17 14:51 7440-39-310/27/17 14:105.0 2.5 1
Cadmium ND ug/L 10/30/17 14:51 7440-43-910/27/17 14:101.0 0.50 1
Chromium ND ug/L 10/30/17 14:51 7440-47-310/27/17 14:105.0 2.5 1
Lead ND ug/L 10/30/17 14:51 7439-92-110/27/17 14:105.0 2.5 1
Selenium ND ug/L 10/30/17 14:51 7782-49-210/27/17 14:1010.0 5.0 1
Silver ND ug/L 10/30/17 14:51 7440-22-410/27/17 14:105.0 2.5 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1245.1 Mercury
Mercury ND ug/L 10/31/17 13:28 7439-97-610/25/17 23:450.20 0.070 1
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92360630
Old Fort Landfill
Sample:MW-3 Lab ID:92360630003 Collected:10/25/17 11:17 Received:10/25/17 14:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7200.7 MET ICP
Arsenic ND ug/L 10/30/17 14:54 7440-38-210/27/17 14:1010.0 5.0 1
Barium 94.8 ug/L 10/30/17 14:54 7440-39-310/27/17 14:105.0 2.5 1
Cadmium ND ug/L 10/30/17 14:54 7440-43-910/27/17 14:101.0 0.50 1
Chromium ND ug/L 10/30/17 14:54 7440-47-310/27/17 14:105.0 2.5 1
Lead ND ug/L 10/30/17 14:54 7439-92-110/27/17 14:105.0 2.5 1
Selenium ND ug/L 10/30/17 14:54 7782-49-210/27/17 14:1010.0 5.0 1
Silver ND ug/L 10/30/17 14:54 7440-22-410/27/17 14:105.0 2.5 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1245.1 Mercury
Mercury ND ug/L 10/31/17 13:31 7439-97-610/25/17 23:450.20 0.070 1
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92360630
Old Fort Landfill
Sample:MW-4 Lab ID:92360630004 Collected:10/25/17 10:12 Received:10/25/17 14:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7200.7 MET ICP
Arsenic ND ug/L 10/30/17 15:00 7440-38-210/27/17 14:1010.0 5.0 1
Barium 31.0 ug/L 10/30/17 15:00 7440-39-310/27/17 14:105.0 2.5 1
Cadmium ND ug/L 10/30/17 15:00 7440-43-910/27/17 14:101.0 0.50 1
Chromium ND ug/L 10/30/17 15:00 7440-47-310/27/17 14:105.0 2.5 1
Lead ND ug/L 10/30/17 15:00 7439-92-110/27/17 14:105.0 2.5 1
Selenium ND ug/L 10/30/17 15:00 7782-49-210/27/17 14:1010.0 5.0 1
Silver ND ug/L 10/30/17 15:00 7440-22-410/27/17 14:105.0 2.5 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1245.1 Mercury
Mercury ND ug/L 10/31/17 13:40 7439-97-610/25/17 23:450.20 0.070 1
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92360630
Old Fort Landfill
Sample:SW-1 Lab ID:92360630005 Collected:10/25/17 12:05 Received:10/25/17 14:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7200.7 MET ICP
Arsenic ND ug/L 10/30/17 15:03 7440-38-210/27/17 14:1010.0 5.0 1
Barium 129 ug/L 10/30/17 15:03 7440-39-310/27/17 14:105.0 2.5 1
Cadmium ND ug/L 10/30/17 15:03 7440-43-910/27/17 14:101.0 0.50 1
Chromium ND ug/L 10/30/17 15:03 7440-47-310/27/17 14:105.0 2.5 1
Lead ND ug/L 10/30/17 15:03 7439-92-110/27/17 14:105.0 2.5 1
Selenium ND ug/L 10/30/17 15:03 7782-49-210/27/17 14:1010.0 5.0 1
Silver ND ug/L 10/30/17 15:03 7440-22-410/27/17 14:105.0 2.5 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1245.1 Mercury
Mercury ND ug/L 10/31/17 13:42 7439-97-610/25/17 23:450.20 0.070 1
REPORT OF LABORATORY ANALYSIS
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Page 9 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92360630
Old Fort Landfill
Sample:SW-2 Lab ID:92360630006 Collected:10/25/17 12:10 Received:10/25/17 14:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7200.7 MET ICP
Arsenic ND ug/L 10/30/17 15:06 7440-38-210/27/17 14:1010.0 5.0 1
Barium 130 ug/L 10/30/17 15:06 7440-39-310/27/17 14:105.0 2.5 1
Cadmium ND ug/L 10/30/17 15:06 7440-43-910/27/17 14:101.0 0.50 1
Chromium ND ug/L 10/30/17 15:06 7440-47-310/27/17 14:105.0 2.5 1
Lead ND ug/L 10/30/17 15:06 7439-92-110/27/17 14:105.0 2.5 1
Selenium ND ug/L 10/30/17 15:06 7782-49-210/27/17 14:1010.0 5.0 1
Silver ND ug/L 10/30/17 15:06 7440-22-410/27/17 14:105.0 2.5 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1245.1 Mercury
Mercury ND ug/L 10/31/17 13:45 7439-97-610/25/17 23:450.20 0.070 1
REPORT OF LABORATORY ANALYSIS
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Asheville, NC 28804
[phone]
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92360630
Old Fort Landfill
Sample:SW-3 Lab ID:92360630007 Collected:10/25/17 11:24 Received:10/25/17 14:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7200.7 MET ICP
Arsenic ND ug/L 10/30/17 15:10 7440-38-210/27/17 14:1010.0 5.0 1
Barium 12.6 ug/L 10/30/17 15:10 7440-39-310/27/17 14:105.0 2.5 1
Cadmium ND ug/L 10/30/17 15:10 7440-43-910/27/17 14:101.0 0.50 1
Chromium 15.8 ug/L 10/30/17 15:10 7440-47-310/27/17 14:105.0 2.5 1
Lead ND ug/L 10/30/17 15:10 7439-92-110/27/17 14:105.0 2.5 1
Selenium ND ug/L 10/30/17 15:10 7782-49-210/27/17 14:1010.0 5.0 1
Silver ND ug/L 10/30/17 15:10 7440-22-410/27/17 14:105.0 2.5 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1245.1 Mercury
Mercury ND ug/L 10/31/17 13:47 7439-97-610/25/17 23:450.20 0.070 1
REPORT OF LABORATORY ANALYSIS
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[phone]
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92360630
Old Fort Landfill
Sample:SW-4 Lab ID:92360630008 Collected:10/25/17 10:26 Received:10/25/17 14:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7200.7 MET ICP
Arsenic ND ug/L 10/30/17 15:13 7440-38-210/27/17 14:1010.0 5.0 1
Barium 335 ug/L 10/30/17 15:13 7440-39-310/27/17 14:105.0 2.5 1
Cadmium ND ug/L 10/30/17 15:13 7440-43-910/27/17 14:101.0 0.50 1
Chromium ND ug/L 10/30/17 15:13 7440-47-310/27/17 14:105.0 2.5 1
Lead ND ug/L 10/30/17 15:13 7439-92-110/27/17 14:105.0 2.5 1
Selenium ND ug/L 10/30/17 15:13 7782-49-210/27/17 14:1010.0 5.0 1
Silver ND ug/L 10/30/17 15:13 7440-22-410/27/17 14:105.0 2.5 1
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1245.1 Mercury
Mercury ND ug/L 10/31/17 13:49 7439-97-610/25/17 23:450.20 0.070 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/07/2017 10:59 AM
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Asheville, NC 28804
[phone]
Page 12 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92360630
Old Fort Landfill
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
383997
EPA 245.1
EPA 245.1
245.1 Mercury
Associated Lab Samples:92360630001, 92360630002, 92360630003, 92360630004, 92360630005, 92360630006, 92360630007,
92360630008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2128313
Associated Lab Samples:92360630001, 92360630002, 92360630003, 92360630004, 92360630005, 92360630006, 92360630007,
92360630008
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 10/31/17 13:140.070
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2128314LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.72.5 109 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2128315MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92360010003
2128316
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 98 70-13099 1 202.5ND 2.5 2.5
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2128317MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92360106002
2128318
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 96 70-130102 5 202.5ND 2.4 2.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/07/2017 10:59 AM
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[phone]
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92360630
Old Fort Landfill
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
384205
EPA 200.7
EPA 200.7
200.7 MET
Associated Lab Samples:92360630001, 92360630002, 92360630003, 92360630004, 92360630005, 92360630006, 92360630007,
92360630008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2129473
Associated Lab Samples:92360630001, 92360630002, 92360630003, 92360630004, 92360630005, 92360630006, 92360630007,
92360630008
Matrix:Water
AnalyzedMDL
Arsenic ug/L ND 10.0 10/30/17 13:365.0
Barium ug/L ND 5.0 10/30/17 13:362.5
Cadmium ug/L ND 1.0 10/30/17 13:360.50
Chromium ug/L ND 5.0 10/30/17 13:362.5
Lead ug/L ND 5.0 10/30/17 13:362.5
Selenium ug/L ND 10.0 10/30/17 13:365.0
Silver ug/L ND 5.0 10/30/17 13:362.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2129474LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 460500 92 85-115
Barium ug/L 467500 93 85-115
Cadmium ug/L 463500 93 85-115
Chromium ug/L 444500 89 85-115
Lead ug/L 462500 92 85-115
Selenium ug/L 473500 95 85-115
Silver ug/L 232250 93 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2129475MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92359931001
2129476
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L 500 96 70-13095 1 20500ND482479
Barium ug/L 500 94 70-13094 0 2050020.8 490 492
Cadmium ug/L 500 94 70-13094 0 20500ND468470
Chromium ug/L 500 88 70-13089 1 20500ND442445
Lead ug/L 500 90 70-13090 0 20500ND450452
Selenium ug/L 500 95 70-13095 0 20500ND474476
Silver ug/L 250 93 70-13093 1 20250ND233235
REPORT OF LABORATORY ANALYSIS
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Asheville, NC 28804
[phone]
Page 14 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92360630
Old Fort Landfill
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2129477MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92360524006
2129478
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L 500 90 70-13093 3 20500ND455470
Barium ug/L 500 91 70-13093 1 2050047.6 504 510
Cadmium ug/L 500 91 70-13092 2 20500ND453461
Chromium ug/L 500 88 70-13089 2 20500ND438446
Lead ug/L 500 89 70-13091 2 20500ND446455
Selenium ug/L 500 90 70-13093 3 20500ND454466
Silver ug/L 250 91 70-13092 2 20250ND227231
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/07/2017 10:59 AM
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Page 15 of 20
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92360630
Old Fort Landfill
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
REPORT OF LABORATORY ANALYSIS
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Page 16 of 20
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92360630
Old Fort Landfill
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92360630001 384205 384415MW-1 EPA 200.7 EPA 200.7
92360630002 384205 384415MW-2 EPA 200.7 EPA 200.7
92360630003 384205 384415MW-3 EPA 200.7 EPA 200.7
92360630004 384205 384415MW-4 EPA 200.7 EPA 200.7
92360630005 384205 384415SW-1 EPA 200.7 EPA 200.7
92360630006 384205 384415SW-2 EPA 200.7 EPA 200.7
92360630007 384205 384415SW-3 EPA 200.7 EPA 200.7
92360630008 384205 384415SW-4 EPA 200.7 EPA 200.7
92360630001 383997 384028MW-1 EPA 245.1 EPA 245.1
92360630002 383997 384028MW-2 EPA 245.1 EPA 245.1
92360630003 383997 384028MW-3 EPA 245.1 EPA 245.1
92360630004 383997 384028MW-4 EPA 245.1 EPA 245.1
92360630005 383997 384028SW-1 EPA 245.1 EPA 245.1
92360630006 383997 384028SW-2 EPA 245.1 EPA 245.1
92360630007 383997 384028SW-3 EPA 245.1 EPA 245.1
92360630008 383997 384028SW-4 EPA 245.1 EPA 245.1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/07/2017 10:59 AM
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[phone]
Page 17 of 20
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