5802_MadisonCountyMSWLF_WQMR_20170630

June 2017
Madison County Closed Solid Waste Facility, Permit No. 58-02
Spring 2017
Semiannual Water Quality Monitoring Report
Prepared for Madison County, North Carolina

Project Number: C61500-01.01
P:\Madison County\Reports\2017\5802 - Closed\FINAL5802April2017 Semiannual Water Quality Report.docx
June 2017
Madison County Closed Solid Waste Facility, Permit No. 58-02
Spring 2017
Semiannual Water Quality Monitoring Report
Prepared for
Madison County, North Carolina
Post Office Box 579
Marshall, North Carolina 28753
Prepared by
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801

____________________________________________
Alec Macbeth, P.G.
Project Geologist

Spring 2017 Semiannual
Water Quality Monitoring Report 1 June 2017
TABLE OF CONTENTS
1 Introduction ................................................................................................................................ 3
2 Methods ....................................................................................................................................... 4
2.1 Groundwater Purging and Sampling Methods ....................................................................................... 4
2.1.1 Monitoring Well Sampling Methods ........................................................................................... 4
2.1.2 Domestic Well Sampling Methods ............................................................................................... 5
2.1.3 Surface Water Sampling Methods ................................................................................................ 5
2.2 Sample Handling, Documentation, and Analysis .................................................................................... 6
3 Findings ........................................................................................................................................ 7
3.1 Analytical Results ................................................................................................................................................. 7
3.1.1 Groundwater Monitoring Wells ..................................................................................................... 8
3.1.2 Surface Water ........................................................................................................................................ 8
3.1.3 Domestic Water Well ......................................................................................................................... 9
4 Site Hydrogeology .................................................................................................................... 11
5 Summary .................................................................................................................................... 12
5.1 Future Activities ................................................................................................................................................ 12
6 References ................................................................................................................................. 13

TABLES
Table 1 Summary of Laboratory Analyses Performed on Samples
Table 2 Summary of Detected Constituents
FIGURES
Figure 1 Site Location Map
Figure 2 Sample Location Map
APPENDICES
Appendix A Sampling Logs and Equipment Documentation and Instrument Calibration Data
Sheets
Appendix B Report of Laboratory Analysis and Chain-of-Custody Documentation

Spring 2017 Semiannual
Water Quality Monitoring Report 2 June 2017
ABBREVIATIONS
µg/L micrograms per liter
µS/cm microsiemens per centimeter
Anchor QEA Anchor QEA of North Carolina, PLLC
CFR Code of Federal Regulations
Closed Landfill closed MSW landfill
DEQ North Carolina Department of Environmental Quality
DO dissolved oxygen
DWM Division of Waste Management
EDD Electronic Data Deliverable
EPA U.S. Environmental Protection Agency
ft-TOC feet below the top of the well casing
IMAC interim maximum allowable concentrations
J-flag indicates analytical result is qualified by the laboratory as estimated and is
flagged with a “J” qualifier
MDL method detection limit
mg/L milligrams per liter
MRL method reporting limit
MSW Municipal Solid Waste
mV millivolt
NCAC North Carolina Administrative Code
NTU Nephelometric turbidity units
ORP oxidation reduction potential
PVC polyvinyl chloride
RCRA Resource Conservation and Recovery Act
SC specific conductivity
SESD Science and Ecosystem Support Division
SU Standard Units
SWM Solid Waste Management
SWS Solid Waste Section
SWSL Solid Waste Section Limit
TestAmerica TestAmerica Laboratories, Inc.
VOC volatile organic compound

Spring 2017 Semiannual
Water Quality Monitoring Report 3 June 2017
1 Introduction
Anchor QEA of North Carolina, PLLC (Anchor QEA) is pleased to present the results of the spring
2017 water quality monitoring event at the Madison County Closed Solid Waste Facility.
The Madison County Solid Waste Department maintains a closed municipal solid waste (MSW)
landfill (Closed Landfill) (the Site) located near the intersection of US Highway 25/70 Bypass and
Long Branch Road (State Route 1582) in Madison County, North Carolina. The general Site location is
presented on Figure 1.
The Closed Landfill is permitted by the North Carolina Department of Environmental Quality (DEQ),
Division of Waste Management (DWM) under Permit No. 58-02, which requires semiannual
monitoring of groundwater and surface water quality.
This report is being submitted in accordance with monitoring requirements for closed landfills as
stipulated in the DEQ DWM Permit No. 58-02 issued to the Madison County Solid Waste Department
and with regulations codified in the DEQ Solid Waste Management (SWM) Rules Title 15A,
Subchapter 13B, Section .1600, of the North Carolina Administrative Code.
This report describes the first semiannual groundwater and surface water quality monitoring event
performed in 2017.
The water quality monitoring network for the Closed Landfill consists of four compliance monitoring
wells (MW-01 OLD, MW-02 OLD, MW-03 OLD, and MW-04 OLD), a background groundwater quality
sampling location (BG SPRING OLD), two surface water sampling locations (SW-01 OLD [upstream]
and SW-02 OLD [downstream]) located along Profitt Branch, and one domestic water supply well
sample (DW-01 OLD) from a home located west of and downgradient of the Landfill. See Figure 2 for
approximate locations of these sampling locations.

Spring 2017 Semiannual
Water Quality Monitoring Report 4 June 2017
2 Methods
Groundwater samples and surface water samples were collected at the Closed Landfill by
Anchor QEA personnel on April 5, 2017.
2.1 Groundwater Purging and Sampling Methods
2.1.1 Monitoring Well Sampling Methods
2.1.1.1 Monitoring Wells MW-01 OLD, MW-02 OLD, and BG SPRING OLD
Prior to collecting groundwater samples from the monitoring wells, the static water level and the
total well depth were measured and recorded to calculate the well’s volume. At each sample location,
an initial round of field parameters consisting of pH, specific conductivity (SC), dissolved
oxygen (DO), oxidation-reduction potential (ORP), turbidity, and temperature was measured and
recorded. Water-level measurements and field parameters are included on the sampling logs
(Appendix A). Groundwater monitoring wells MW-01 OLD and MW-02 OLD and sampling point BG
SPRING OLD were then purged using a new disposable polyethylene bailer (BG SPRING OLD is
described in the following paragraph). These wells are purged and sampled with a disposable bailer
due to poor well access. As each consecutive well volume was removed with the bailer, an additional
round of groundwater parameters was recorded. Each well was purged until a minimum of three well
volumes were removed and field parameters stabilized or until the well had been bailed dry.
Monitoring well MW-02 OLD, which was bailed dry, was allowed to recharge prior to collecting one
final round of field parameters and the groundwater sample.
The water sample collected from background sampling location BG SPRING OLD is treated as a
groundwater sample for the following reasons:
• Groundwater does not discharge to the ground surface at the sampling point.
• Construction of the sampling point is similar to that of a temporary monitoring well or
piezometer and is located upslope and upgradient of a springhead.
• The sampling point is constructed of a polyvinyl chloride (PVC) casing extending below
ground surface and has a screened interval from which groundwater is collected and
recharges.
2.1.1.2 Monitoring Wells MW-03 OLD and MW-04 OLD
Monitoring wells MW-03 OLD and MW-04 OLD were purged and sampled with a bladder pump
using low-flow techniques in accordance with the procedures described in “Low-Flow (Minimal
Drawdown) Ground-Water Sampling Procedures”, U.S. Environmental Protection Agency (EPA),
Groundwater Issues (Puls and Barcelona 1996). During purging, pH, SC, DO, ORP, turbidity, and
temperature were measured and recorded approximately every 3 minutes. Well purging continued

Spring 2017 Semiannual
Water Quality Monitoring Report 5 June 2017
until these parameters stabilized for three consecutive readings. The required stabilization criteria
were determined by the EPA Region 4 Science and Ecosystem Support Division (SESD) Operating
Procedure: Groundwater Sampling (EPA 2013) and are as follows:
• pH values within +/- 0.1 pH unit
• SC values within +/- 3 percent
• Temperature, DO, and turbidity values within +/- 10 percent
• ORP values within +/- 10 millivolts
Following stabilization of these parameters, a groundwater sample was collected by a technician
wearing a new pair of non-reactive nitrile gloves. Each sample was placed directly into
laboratory-supplied sample containers. Low-flow sampling logs are included in Appendix A.
2.1.2 Surface Water Sampling Methods
Surface water samples SW-01 OLD and SW-02 OLD were collected at designated locations along
Profitt Branch, which flows adjacent to the southern Site boundary in a west-to-east direction
(Figure 2). The surface water sample collected at the SW-01 OLD location is assumed to represent
surface water quality upstream of the Closed Landfill, and the surface water sample collected at the
SW-02 OLD location is assumed to represent surface water quality downstream of the Closed
Landfill. One set of field parameters, including temperature, pH, SC, DO, ORP, and turbidity, was
measured and recorded at each surface water sampling location prior to sample collection
(Appendix A). One surface water sample was collected from each sampling location using
laboratory-supplied sample containers by a technician wearing a new pair of disposable nitrile
gloves. The sample from SW-01 OLD was collected using a decontaminated plastic syringe due to
shallow surface water flow.
2.1.3 Domestic Well Sampling Methods
Anchor QEA personnel sampled one domestic water supply well (DW-01 OLD), owned by Mrs. J.V.
Edwards, on April 5, 2017. The well was purged and sampled using the dedicated pump existing in
the well. Groundwater was accessed from a spigot in the basement of Mrs. J. V. Edwards’ house
because a spigot does not exist at the wellhead. Sampling personnel recorded one round of field
parameters initially at the start of the purge and then one round for every 10 gallons purged from
the well. Prior to sample collection, a total of 30 gallons of water was purged from the well. Field
parameters are presented in Appendix A. A groundwater sample was collected from the domestic
well using laboratory-supplied sample containers by a technician wearing a new pair of disposable
nitrile gloves.

Spring 2017 Semiannual
Water Quality Monitoring Report 6 June 2017
2.2 Sample Handling, Documentation, and Analysis
Field parameters and additional observations pertaining to water quality sampling at the Closed
Landfill sampling locations are provided on the sampling logs provided in Appendix A. Following
sample collection, groundwater and surface water samples were immediately placed on ice in sample
coolers for transport to TestAmerica Laboratories, Inc. (TestAmerica), a laboratory certified in North
Carolina and located in Nashville, Tennessee. Anchor QEA submitted all collected groundwater and
surface water samples to TestAmerica for analysis as follows:
• Appendix I volatile organic compounds (VOCs) using EPA Approved Method 8260B
‒ Appendix I parameters are identified in Appendix I of the Code of Federal Regulations,
Title 40, Part 258 (40 CFR 258).
• Eight Resource Conservation and Recovery Act (RCRA) metals using EPA Approved Methods
6010D and 7470A
A summary of laboratory analyses performed on samples is provided in Table 1. Trip blanks,
provided by the laboratory and stored in each sample cooler, were analyzed for Appendix I VOCs.
Proper chain-of-custody documentation procedures were followed during collection and transport of
each sample. The laboratory analytical reports and chain-of-custody documentation are included in
Appendix B. Water-level measurements, field parameters, and observations pertaining to water
quality are included in Appendix A.

Spring 2017 Semiannual
Water Quality Monitoring Report 7 June 2017
3 Findings
3.1 Analytical Results
The field parameter data and laboratory analytical results for the groundwater, surface water, and
trip blank samples collected at the Closed Landfill are included in Appendices A and B, respectively,
and also submitted separately to the DEQ DWM Solid Waste Section (SWS) in the Electronic Data
Deliverable (EDD) format (a format most recently updated on May 5, 2010).
As stipulated in the May 2010 DWM documents referenced in the paragraph above, non-detections
were reported at the method detection limit (MDL), and all concentrations exceeding the applicable
laboratory-specific MDL were reported and appropriately qualified (see Table 2). The MDL is the
minimum concentration of a substance that can be measured and reported by a laboratory with
99 percent confidence that the analyte concentration is greater than zero. All detections were
compared to analyte-specific Solid Waste Section Limits (SWSLs) established by the SWS. The SWSL
is the lowest concentration of an analyte in a sample that can be quantitatively determined with
suitable precision and accuracy. The method reporting limit (MRL) is the minimum concentration of a
target analyte that can be accurately determined by the referenced method and is listed in the
“Report Limit” (RL) column in the TestAmerica report of laboratory analysis (see Appendix B). If the
reported concentration is above the laboratory MDL and below the MRL, the analytical result is
reported by the laboratory as estimated and is flagged with a “J” qualifier (non-italicized J-flag). If the
reported concentration is greater than the laboratory MRL and less than the SWSL, the analytical
result is qualified by Anchor QEA as estimated and is flagged with a “J” qualifier (italicized J-flag).
Detected concentrations of analytes in groundwater samples were compared to current groundwater
quality standards specified in Title 15A, North Carolina Administrative Code (NCAC), Subchapter 2L
.0202, and referred to as 2L standards. Detected concentrations of analytes in groundwater with no
established 2L standards were compared to the interim maximum allowable concentrations (IMACs)
for Class GA and GSA groundwater (in accordance with Title 15A, NCAC, Subchapter 02L .0202 [c]), if
established. Detections of analytes in surface water samples were compared to Title 15A, NCAC,
Subchapter 2B .0200 surface water quality standards (2B standards). Concentrations below respective
SWSLs are not discussed in the text of this report unless they exceed their contaminant-specific 2L or
2B water quality standard.
Table 2 presents the summary of field parameter results and laboratory analytical results for detected
constituents. The following discussion outlines constituents that were detected above applicable
SWSLs, as well as constituents detected at concentrations that exceeded their respective 2L
standards (including IMACs, if applicable) or 2B standards.

Spring 2017 Semiannual
Water Quality Monitoring Report 8 June 2017
3.1.1 Groundwater Monitoring Wells
The following sections summarize the results of laboratory and field parameter analyses of
groundwater samples.
3.1.1.1 RCRA Metals
Five metals were detected in groundwater samples collected from one or more monitoring wells
(Table 2). Two of these metals (barium and lead) were detected at concentrations greater than their
respective SWSLs. The concentration of barium exceeded its 2L standard of 700 micrograms per
liter (µg/L) in the samples collected from compliance monitoring wells MW-03 OLD and MW-04 OLD.
Lead, detected at 15.7 µg/L, exceeded its 2L standard of 15 µg/L in monitoring well MW-03 OLD.
Detected metals above 2L standards are consistent with historical data.
3.1.1.2 Appendix I VOCs
Eight VOCs were detected in groundwater samples collected from one or more monitoring wells.
Four VOCs (1,4-dichlorobenzene, benzene, chlorobenzene, and ethylbenzene) were detected in
excess of their respective SWSLs in one or more monitoring wells (Table 2). Benzene was the only
VOC detected at a concentration above its 2L standard of 1 µg/L. This occurred in one monitoring
well, MW-03 OLD at 1.92 µg/L. VOC detections are consistent with historical data.
3.1.1.3 Field Parameters
The pH readings obtained on April 5, 2017 from monitoring wells MW-01 OLD, MW-03 OLD, and
MW-04 OLD (6.23 Standard Units [SU] to 6.37 SU) were below the range for pH (6.5 to 8.5 SU)
specified in the 2L standard (see Table 2).
Turbidity in the monitoring wells ranged between 5.59 nephelometric turbidity units (NTUs) in
monitoring well MW-02 OLD to 104 NTUs (BG-Spring OLD). Measured DO values ranged between
2.13 milligrams per liter (mg/L) in MW-03 OLD to 8.14 mg/L in MW-02 OLD. Specific conductivity
values ranged between 82 microsiemens per centimeter (µS/cm) in BG-Spring OLD to 739 µS/cm in
MW-03 OLD. ORP values in the monitoring wells ranged between -42.8 millivolts (mV) in MW-03
OLD to 236.9 mV in BG-Spring OLD (Table 2). These parameters do not have established
groundwater quality standards. Concentrations of field parameters are generally consistent with
historical concentrations.
3.1.2 Surface Water
The following sections summarize the results of laboratory and field parameter analyses of surface
water samples SW-01 OLD and SW-02 OLD.

Spring 2017 Semiannual
Water Quality Monitoring Report 9 June 2017
3.1.2.1 RCRA Metals
Barium was the only metal detected in the surface water samples at concentrations above the
applicable MDL. This metal was detected at concentrations below both the SWSL and 2B standard in
both SW-01 OLD and SW-02 OLD (Table 2).
3.1.2.2 Appendix I VOCs
No VOCs were detected in either the upstream or downstream surface water samples collected from
the Closed Landfill.
3.1.2.3 Field Parameters
The pH readings collected from both surface water sample locations were within the 2B standard
range established at 6.0 to 9.0 SU.
The turbidity readings collected from SW-01 OLD and SW-02 OLD were 19.6 NTUs and 16.4 NTUs,
respectively. Both readings were below the 2B standard of 50 NTUs.
DO was recorded within the 2B standard for both surface water samples collected. The established
2B standard for DO in class C waters is “greater than 5.0 mg/L.” Collected DO readings were 9.26
mg/L and 9.81 mg/L for surface water samples SW-01 OLD and SW-02 OLD, respectively.
Specific conductivity measurements in SW-01 OLD and SW-02 OLD were recorded at 164 µS/cm and
130 µS/cm, respectively. ORP values for these samples were recorded at 135.9 mV and 216.1 mV,
respectively (Table 2). These parameters do not have established surface water quality standards.
3.1.3 Domestic Water Well
The following sections summarize the results of laboratory and field parameter analyses of the
domestic well sample DW-01 OLD.
3.1.3.1 RCRA Metals
Three metals (barium, chromium, and lead) were detected in the sample collected from the domestic
well DW-01 OLD. Only barium was detected at a concentration (171 µg/L) greater than its SWSL, but
below its 2L groundwater standard. This concentration is also well below the national primary
drinking water standard for barium of 2,000 µg/L. The other two metals, chromium and lead, were
detected at concentrations of 6.1 J µg/L and 6.6 J µg/L respectively, below the SWSL and 2L
groundwater standard.
3.1.3.2 Appendix I VOCs
No Appendix I VOCs were detected in the domestic well sample.

Spring 2017 Semiannual
Water Quality Monitoring Report 10 June 2017
3.1.3.3 Field Parameters
The pH reading obtained from the domestic well was outside the 2L standard range for groundwater
established at 6.5-8.5 SU. The turbidity reading collected from this sample location was recorded at
38.0 NTUs. DO measured in DW-01 OLD was 6.19 mg/L. The recorded specific conductivity value at
this sample location was 113 µS/cm, and the recorded ORP value was 212.1 mV.

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Water Quality Monitoring Report 11 June 2017
4 Site Hydrogeology
Groundwater levels were measured in the four compliance monitoring wells (MW-01 OLD, MW-02
OLD, MW-03 OLD, and MW-04 OLD) at the Closed Landfill at depths of approximately 5.40 feet
below the top of the well casing (ft-TOC), 7.35 ft-TOC, 43.09 ft-TOC, and 46.18 ft-TOC, respectively
(Appendix A).
Monitoring wells MW-03 OLD and MW-04 OLD are installed in bedrock east of the Edwards/Madison
County property line near the top of a ridge within the landfill parcel. Monitoring wells MW-01 OLD
and MW-02 OLD are located in topographic drainages and are screened in the water table aquifer.
Locations of monitoring wells at the Site are not situated such that groundwater flow direction may
be accurately calculated based on data from these wells. However, within the unconsolidated soil, the
shallow groundwater is interpreted to generally flow in directions that mimic topography, which is
generally southward toward Profitt Branch. The Site is situated on the southwest side of a knoll with
an elevation of approximately 2,100 feet above mean sea level and drains to Profitt Branch.

Spring 2017 Semiannual
Water Quality Monitoring Report 12 June 2017
5 Summary
Anchor QEA completed the first semiannual water quality monitoring event of 2017 at the Madison
County Closed Solid Waste Facility on April 5, 2017.
Table 2 of this report, field sampling logs (Appendix A), and the TestAmerica Reports of Laboratory
Analysis (Appendix B) provide detailed analytical results and field data related to groundwater and
surface water quality at the Closed Landfill.
5.1 Future Activities
Anchor QEA will continue to measure field parameters and collect water quality samples from
groundwater and surface water monitoring points associated with the Closed Landfill. Water quality
samples will be submitted to a North Carolina-certified laboratory for analysis for RCRA metals and
Appendix I VOCs on a semiannual basis. The next sampling event is scheduled for October 2017.

Spring 2017 Semiannual
Water Quality Monitoring Report 13 June 2017
6 References
DENR DWM SWS (North Carolina Department of Environment and Natural Resources Division of
Waste Management Solid Waste Section), 2006. New Guidelines for Electronic Submittal of
Environmental Monitoring Data. October 27, 2006
DENR DWM SWS, 2007. Addendum to October 27, 2006, NC SWS Memorandum Regarding New
Guidelines for Electronic Submittal of Environmental Data. February 23, 2007.
EPA (U.S. Environmental Protection Agency), 1996. Low-Flow (Minimal Drawdown) Ground-Water
Sampling Procedures. OSWER, EPA/540/S-95/504.
EPA, revised 2013. SESD Operating Procedure: Groundwater Sampling. March 6, 2013.

Tables
Table 1
Summary of Laboratory Analyses Performed on Samples
Spring 2017 Semiannual Water Quality Monitoring Report
Madison County Closed Municipal Solid Waste Landfill
Page 1 of 1
June 2017
GROUNDWATER SAMPLES
VOCs RCRA Metals
EPA 8260B
EPA 6010D
EPA 7470A
58-02 MW-01 OLD 04/05/2017 X X
58-02 MW-02 OLD 04/05/2017 X X
58-02 MW-03 OLD 04/05/2017 X X
58-02 MW-04 OLD 04/05/2017 X X
58-02 BG SPRING OLD 04/05/2017 X X
SURFACE WATER SAMPLES
VOCs RCRA Metals
EPA 8260B
EPA 6010D
EPA 7470A
58-02 SW-01 OLD 04/05/2017 X X
58-02 SW-02 OLD 04/05/2017 X X
Domestic Well Sample
VOCs RCRA Metals
EPA 8260B EPA 6010D
EPA 7470A
58-02 DW-01 OLD 04/05/2017 X X
QUALITY CONTROL SAMPLES
VOCs
EPA 8260B
58-02 TRIP BLANK (OLD)04/05/2017 X
58-02 TRIP BLANK (BACKGROUND)04/05/2017 X
Notes:
Analyses include Appendix I constituents per 40 CFR Part 258.
VOCs Volatile organic compounds.
FACILITY
PERMIT WELL ID COLLECT DATE
FACILITY
PERMIT SAMPLE ID COLLECT DATE
FACILITY
PERMIT SAMPLE ID COLLECT DATE
FACILITY
PERMIT SAMPLE ID COLLECT DATE
Table 2
Summary of Detected Constituents
Spring 2017 Semiannual Water Quality Monitoring Report
Madison County Closed Municipal Solid Waste Landfill
Page 1 of 1
June 2017
Metals VOCs (Appendix I)Field Parameters
Lab Certification 387 387 5445 (pH only)
Lab Method EPA 6010D EPA 8260B
Barium Cadmium Chromium Lead Selenium
1,1-Dichloro-
ethane
1,4-Dichloro-
benzene Acetone Benzene
Chloro-
benzene
Chloro-
ethane
cis-1,2-
Dichloro-
ethene
Ethyl-
benzene pH Turbidity
Dissolved
Oxygen Temperature
Specific
Conductivity
Oxidation
Reduction
Potential
CAS Number 7440-39-3 7440-39-3 7440-47-3 7439-92-1 7782-49-2 75-34-3 106-46-7 67-64-1 71-43-2 108-90-7 75-00-3 156-59-2 100-41-4 SW320 SW330 7782-44-7 SW325 SW323 SW336
SWS ID 15 34 51 131 183 75 71 3 16 39 41 78 110 320 330 356 325 323 336
Units µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L SU NTU mg/L °C µS/cm mV
Sample ID Collect Date Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result
Monitoring Well Samples
MW-01 OLD 04/05/2017 125 0.500 U 3.00 U 3.4 J 5.00 U 0.240 U 0.316 J 2.66 U 0.200 U 0.180 U 0.360 U 0.210 U 0.190 U 6.37 59.3 7.42 10.02 122 212.8
MW-02 OLD 04/05/2017 44.9 J 0.500 U 3.00 U 3.5 J 5.00 U 0.653 J 0.170 U 2.66 U 0.200 U 0.180 U 0.360 U 0.210 U 0.190 U 7.28 5.59 8.14 13.25 172 114.2
MW-03 OLD 04/05/2017 778 0.8 J 3.00 U 15.7 5.2 J 0.240 U 3.35 2.89 J 1.92 5.81 0.771 J 0.210 U 6.17 6.23 5.77 2.13 12.52 739 -42.8
MW-04 OLD 04/05/2017 728 0.500 U 3.00 U 6.2 J 5.5 J 0.240 U 1.84 5.22 J 0.275 J 3.30 0.776 J 0.374 J 0.190 U 6.23 8.16 3.44 12.04 652 63.3
BG SPRING OLD 04/05/2017 101 0.500 U 6.7 J 2.00 U 5.00 U 0.240 U 0.170 U 2.66 U 0.200 U 0.180 U 0.360 U 0.210 U 0.190 U 6.50 104 6.44 12.22 82 236.9
Surface Water Samples
SW-01 OLD 04/05/2017 81.6 J 0.500 U 3.00 U 2.00 U 5.00 U 0.240 U 0.170 U 2.66 U 0.200 U 0.180 U 0.360 U 0.210 U 0.190 U 7.22 19.6 9.26 11.25 164 135.9
SW-02 OLD 04/05/2017 58.9 J 0.500 U 3.00 U 2.00 U 5.00 U 0.240 U 0.170 U 2.66 U 0.200 U 0.180 U 0.360 U 0.210 U 0.190 U 6.62 16.4 9.81 10.38 130 216.1
Domestic Well Sample
DW-01 OLD 04/05/2017 171 0.500 U 6.1 J 6.6 J 5.00 U 0.240 U 0.170 U 2.66 U 0.200 U 0.180 U 0.360 U 0.210 U 0.190 U 6.32 38.0 6.19 15.12 113 212.1
Quality Control Samples
TRIP BLANK (OLD)04/05/2017 NA NA NA NA NA 0.240 U 0.170 U 2.66 U 0.200 U 0.180 U 0.360 U 0.210 U 0.190 U NA NA NA NA NA NA
TRIP BLANK (BACKGROUND)04/05/2017 NA NA NA NA NA 0.240 U 0.170 U 2.66 U 0.200 U 0.180 U 0.360 U 0.210 U 0.190 U NA NA NA NA NA NA
MDL 5.00 0.500 3.00 2.00 5.00 0.240 0.170 2.66 0.200 0.180 0.360 0.210 0.190 NA NA NA NA NA NA
MRL 10.0 1.00 5.0 5.0 10.0 1.0 1.0 25.0 1.0 1.0 1.0 1.0 1.0 NA NA NE NE NE NE
SWSL 100 1 10 10 10 5 1 100 1 3 10 5 1 NE NE NE NE NE NE
2L 700 2 10 15 20 6 6 6,000 1 50 3,000 70 600 6.5-8.5 NE NE NE NE NE
IMAC NE NE NE NE NE NE NE NE NE NE NE 60 NE NE NE NE NE NE NE
GWPS NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE
2B 200,000 0.15 35 0.54 5 100 100 2,000 51 140 NE 720 97 6.0-9.0 50 > 5.0 NE NE NE
Notes:
Detections Only detected constituents are listed on this table. Please refer to the TestAmerica laboratory analysis reports for further details.
Lab Method The analytical method used to analyze the constituents.
CAS Number A unique number assigned by the Chemical Abstracts Service (CAS) to all identified parameters.
SWS ID The Solid Waste Section Identification Number.
Units Micrograms per liter (µg/L) for analytical results, Standard Units (SU) for pH, nephelometric turbidity units (NTU) for turbidity, and milligrams per liter (mg/L) for dissolved oxygen.
Collect Date The date on which the sample was collected in the field.
Result Analytical data reported by the laboratory or field data collected by Anchor QEA.
MDL The method detection limit, which is the minimum concentration of a substance that can be measured and reported with 99 percent confidence that the analyte concentration is greater than zero.
MRL The method reporting limit, which is the minimum concentration of a target analyte that can be accurately determined by the referenced method.
SWSL The Solid Waste Section Limit. This limit (identified by DEQ) is the lowest amount of analyte in a sample that can be quantitatively determined with suitable precision and accuracy.
U A laboratory data qualifier used for parameters not detected at concentrations above MDL.
J A laboratory data qualifier used for parameters detected at estimated concentrations above MDL but below MRL.
J Assigned by Anchor QEA to reflect a detected concentration that is greater than MRL and MDL but less than the SWSL.
2L Groundwater standards from "North Carolina Administrative Code, Title 15A: Department of Environmental Quality, Subchapter 2L - Groundwater Classifications and Standards," DEQ (amended April 1, 2013).
IMAC Interim Maximum Allowable Concentration. IMAC concentrations are listed in Appendix #1 of the 2L.
GWPS
2B
NE Not Established
NA Not Applicable
463 Bold cells indicate a result in exceedance of the SWSL.
6.29 Shaded cells indicate a result in exceedance of the 2L, IMAC, GWP, or 2B standard.
Parameter
"GWPS" is the Groundwater Protection Standard pursuant to "15A NCAC 13B .1634," DEQ. Current standards were obtained from the NC DEQ Solid Waste Section Environmental Monitoring List (last updated June 13, 2011). GWPS is used only if 2L or IMAC standards are not
established for specific constituent.
The surface water standard per "North Carolina Administrative Code, Title 15A: Department of Environmental Quality, Subchapter 2B - Surface Water and Wetland Standards" (last amended March, 2016) or standard obtained from National Criteria per EPA table (current as of
May 15, 2013).

Figures
[0 2,000 4,0001,000
Feet
LEGEND:
Landfill Parcel
Publish Date: 2017/05/17, 10:50 AM | User: alesueurFilepath: P:\Madison County\Figures\GIS\GIS User\MXDs\2017\Spring\5802F1-Site Location Map Closed AQ.mxd
Figure 1Site Location Map
Madison County Closed Landfill Water Quality ReportMadison County Closed MSW Landfill, Permit #58-02, Marshall, NC
SOURCE(S):Basemap: USGS 1:24,000 Scale Topo Maps,Marshall Quadrangle, 1990.Parcels: Madison County GIS
Anchor QEA of North Carolina, PLLC
#I#I@A
@A
@A
@A
@A@A
%Flow Direction
21252
15
5
2055 2185
2 0 3 5
2135
2165
2065 217520352175
2175
23152065
196521452035 21851925 20952055 21152 0 5 5
213521052115
1 97 5
2045
1935
2 0 9 5
2045
2125
208523052125
2035
211520752125
2025
20652 0 1 5
2 1 6 5
1985
2 1 5 51945
2 0 5 5
1965
2145213521152
0
4
5 22952105 210520952 2 3 5
2085
2225
2
0
55
2
2
8
5
2 0 85
221 5
20452205
2
0
75
1 9 9 5
211520152275
2 0 6 5 2 1 2 5
1955
2
2
6
5
202522552
00
5
208520952075205521052065204522452185
2055 2065
2175
1975 20752 1 9 520952085
2035
1985 216521552 1 4 5
21352125
2115
1995 206520752105
2 0 3 5
2005
2015 20252045
SW-02 OLD
SW-01 OLD
MW-02 OLD
BG SPRING OLD
DW-01 OLD
MW-01 OLD
MW-04 OLD
MW-03 OLD
U TUT
PROFITT BRANCH
PROFITT BRANCH LUUNG BR RDKENPAK LNLONG BRANCH RD
[
0 400200
Feet
NOTES:1. Sample locations are approximateas indicated on map.
LEGEND:
@A Monitoring Well Location
#ISurface Water Sample Location
Landfill Parcel Boundary
Elevation Contours (10 feet)
Roads
Streams
Publish Date: 2017/05/17, 10:56 AM | User: alesueurFilepath: P:\Madison County\Figures\GIS\GIS User\MXDs\2017\Spring\5802AprF2 -Sample Location Map Closed AQ.mxd
Figure 2Sample Location Map
Madison County Closed Landfill Water Quality ReportMadison County Closed MSW Landfill, Permit #58-02, Marshall, NC
SOURCES:Basemap: NC OneMap 2010Contours and Roads: NCDOTStreams: NC OneMapParcel Boundary: Madison County GIS
Anchor QEA of North Carolina, PLLC

Appendix A
Sampling Logs and Equipment
Documentation and Instrument
Calibration Data Sheets

Appendix B
Report of Laboratory Analysis and
Chain-of-Custody Documentation

ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: [phone]
TestAmerica Job ID: 490-125734-1
Client Project/Site: Madison CO Closed Landfill
Revision: 1
For:
Anchor QEA of North Carolina PLLC
231 W Haywood Street
Asheville, North Carolina 28801
Attn: Brian Gant
Authorized for release by:
5/8/2017 4:43:52 PM
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison CO Closed Landfill
TestAmerica Job ID: 490-125734-1
Page 2 of 33 TestAmerica Nashville5/8/2017
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .16
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .25
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .27
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .29
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .30
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .31
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .33
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Sample Summary
TestAmerica Job ID: 490-125734-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison CO Closed Landfill
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-125734-1 MW-01 OLD Water 04/05/17 09:36 04/06/17 09:30
490-125734-2 MW-02 OLD Water 04/05/17 12:25 04/06/17 09:30
490-125734-3 MW-03 OLD Water 04/05/17 10:54 04/06/17 09:30
490-125734-4 MW-04 OLD Water 04/05/17 11:46 04/06/17 09:30
490-125734-5 Trip Blank Water 04/05/17 00:01 04/06/17 09:30
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Case Narrative
Client: Anchor QEA of North Carolina PLLC TestAmerica Job ID: 490-125734-1
Project/Site: Madison CO Closed Landfill
Job ID: 490-125734-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-125734-1
REVISED REPORT: Revised to report only RCRA 8 metals per the client's initial request for analysis. This report replaces the one
generated on 04/24/17 @ 1631.
Comments
No additional comments.
Receipt
The samples were received on 4/6/2017 9:30 AM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 1.4º C.
GC/MS VOA
Method 8260B: The RPD of the laboratory control sample (LCS) and laboratory control sample duplicate (LCSD) for analytical batch
490-421674 recovered outside control limits for the following analytes: 1,2-Dichloroethane and Ethylene Dibromide.
Method 8260B: The method blank for analytical batch 490-421674 contained Methylene chloride above the method detection limit. This
target analyte concentration was less than the reporting limit (RL); therefore, re-extraction and/or re-analysis of samples was not
performed.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
Method 6020B: The method blank for 490-423514 contained Vanadium above the method detection limit (MDL). Associated samples
were not re-analyzed because results were less than the reporting limit (RL) OR practical quantitation limit (PQL).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
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Definitions/Glossary
TestAmerica Job ID: 490-125734-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison CO Closed Landfill
Qualifiers
GC/MS VOA
Qualifier Description
*RPD of the LCS and LCSD exceeds the control limits
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Metals
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Client Sample Results
TestAmerica Job ID: 490-125734-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison CO Closed Landfill
Lab Sample ID: 490-125734-1Client Sample ID: MW-01 OLD
Matrix: WaterDate Collected: 04/05/17 09:36
Date Received: 04/06/17 09:30
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 04/12/17 20:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 04/12/17 20:00 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/12/17 20:00 1Benzene<0.200
1.00 0.150 ug/L 04/12/17 20:00 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/12/17 20:00 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/12/17 20:00 1Bromoform<0.290
1.00 0.350 ug/L 04/12/17 20:00 1Bromomethane<0.350
50.0 2.64 ug/L 04/12/17 20:00 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 04/12/17 20:00 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/12/17 20:00 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/12/17 20:00 1Chlorobenzene<0.180
1.00 0.360 ug/L 04/12/17 20:00 1Chloroethane<0.360
1.00 0.230 ug/L 04/12/17 20:00 1Chloroform<0.230
1.00 0.360 ug/L 04/12/17 20:00 1Chloromethane<0.360
1.00 0.210 ug/L 04/12/17 20:00 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 04/12/17 20:00 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/12/17 20:00 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/12/17 20:00 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/12/17 20:00 11,2-Dibromoethane (EDB)<0.210 *
1.00 0.450 ug/L 04/12/17 20:00 1Dibromomethane<0.450
1.00 0.190 ug/L 04/12/17 20:00 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 04/12/17 20:00 11,4-Dichlorobenzene 0.316 J
1.00 0.240 ug/L 04/12/17 20:00 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 04/12/17 20:00 11,2-Dichloroethane <0.200 *
1.00 0.250 ug/L 04/12/17 20:00 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/12/17 20:00 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 04/12/17 20:00 1Ethylbenzene<0.190
10.0 1.28 ug/L 04/12/17 20:00 12-Hexanone <1.28
10.0 1.50 ug/L 04/12/17 20:00 1Iodomethane<1.50
5.00 1.00 ug/L 04/12/17 20:00 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/12/17 20:00 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/12/17 20:00 1Styrene<0.280
1.00 0.150 ug/L 04/12/17 20:00 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/12/17 20:00 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/12/17 20:00 1Tetrachloroethene<0.140
1.00 0.170 ug/L 04/12/17 20:00 1Toluene<0.170
5.00 0.460 ug/L 04/12/17 20:00 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/12/17 20:00 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 04/12/17 20:00 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/12/17 20:00 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/12/17 20:00 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/12/17 20:00 1Trichloroethene<0.200
1.00 0.210 ug/L 04/12/17 20:00 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 04/12/17 20:00 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/12/17 20:00 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/12/17 20:00 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/12/17 20:00 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-125734-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison CO Closed Landfill
Lab Sample ID: 490-125734-1Client Sample ID: MW-01 OLD
Matrix: WaterDate Collected: 04/05/17 09:36
Date Received: 04/06/17 09:30
4-Bromofluorobenzene (Surr)104 70-130 04/12/17 20:00 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)109 04/12/17 20:00 170-130
1,2-Dichloroethane-d4 (Surr)115 04/12/17 20:00 170-130
Toluene-d8 (Surr)102 04/12/17 20:00 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 04/19/17 22:23 04/20/17 21:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 04/19/17 22:23 04/20/17 21:03 1Barium0.125
0.00100 0.000500 mg/L 04/19/17 22:23 04/20/17 21:03 1Cadmium<0.000500
0.00500 0.00300 mg/L 04/19/17 22:23 04/20/17 21:03 1Chromium<0.00300
0.00500 0.00200 mg/L 04/19/17 22:23 04/20/17 21:03 1Lead0.00340 J
0.0100 0.00500 mg/L 04/19/17 22:23 04/23/17 04:29 1Selenium<0.00500
0.00500 0.00300 mg/L 04/19/17 22:23 04/20/17 21:03 1Silver<0.00300
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 04/13/17 07:33 04/13/17 13:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-125734-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison CO Closed Landfill
Lab Sample ID: 490-125734-2Client Sample ID: MW-02 OLD
Matrix: WaterDate Collected: 04/05/17 12:25
Date Received: 04/06/17 09:30
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 04/12/17 20:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 04/12/17 20:27 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/12/17 20:27 1Benzene<0.200
1.00 0.150 ug/L 04/12/17 20:27 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/12/17 20:27 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/12/17 20:27 1Bromoform<0.290
1.00 0.350 ug/L 04/12/17 20:27 1Bromomethane<0.350
50.0 2.64 ug/L 04/12/17 20:27 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 04/12/17 20:27 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/12/17 20:27 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/12/17 20:27 1Chlorobenzene<0.180
1.00 0.360 ug/L 04/12/17 20:27 1Chloroethane<0.360
1.00 0.230 ug/L 04/12/17 20:27 1Chloroform<0.230
1.00 0.360 ug/L 04/12/17 20:27 1Chloromethane<0.360
1.00 0.210 ug/L 04/12/17 20:27 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 04/12/17 20:27 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/12/17 20:27 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/12/17 20:27 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/12/17 20:27 11,2-Dibromoethane (EDB)<0.210 *
1.00 0.450 ug/L 04/12/17 20:27 1Dibromomethane<0.450
1.00 0.190 ug/L 04/12/17 20:27 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 04/12/17 20:27 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 04/12/17 20:27 11,1-Dichloroethane 0.653 J
1.00 0.200 ug/L 04/12/17 20:27 11,2-Dichloroethane <0.200 *
1.00 0.250 ug/L 04/12/17 20:27 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/12/17 20:27 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 04/12/17 20:27 1Ethylbenzene<0.190
10.0 1.28 ug/L 04/12/17 20:27 12-Hexanone <1.28
10.0 1.50 ug/L 04/12/17 20:27 1Iodomethane<1.50
5.00 1.00 ug/L 04/12/17 20:27 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/12/17 20:27 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/12/17 20:27 1Styrene<0.280
1.00 0.150 ug/L 04/12/17 20:27 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/12/17 20:27 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/12/17 20:27 1Tetrachloroethene<0.140
1.00 0.170 ug/L 04/12/17 20:27 1Toluene<0.170
5.00 0.460 ug/L 04/12/17 20:27 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/12/17 20:27 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 04/12/17 20:27 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/12/17 20:27 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/12/17 20:27 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/12/17 20:27 1Trichloroethene<0.200
1.00 0.210 ug/L 04/12/17 20:27 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 04/12/17 20:27 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/12/17 20:27 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/12/17 20:27 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/12/17 20:27 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-125734-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison CO Closed Landfill
Lab Sample ID: 490-125734-2Client Sample ID: MW-02 OLD
Matrix: WaterDate Collected: 04/05/17 12:25
Date Received: 04/06/17 09:30
4-Bromofluorobenzene (Surr)105 70-130 04/12/17 20:27 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)108 04/12/17 20:27 170-130
1,2-Dichloroethane-d4 (Surr)113 04/12/17 20:27 170-130
Toluene-d8 (Surr)101 04/12/17 20:27 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 04/19/17 22:23 04/20/17 21:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 04/19/17 22:23 04/20/17 21:08 1Barium0.0449
0.00100 0.000500 mg/L 04/19/17 22:23 04/20/17 21:08 1Cadmium<0.000500
0.00500 0.00300 mg/L 04/19/17 22:23 04/20/17 21:08 1Chromium<0.00300
0.00500 0.00200 mg/L 04/19/17 22:23 04/20/17 21:08 1Lead0.00350 J
0.0100 0.00500 mg/L 04/19/17 22:23 04/23/17 04:34 1Selenium<0.00500
0.00500 0.00300 mg/L 04/19/17 22:23 04/20/17 21:08 1Silver<0.00300
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 04/13/17 07:33 04/13/17 14:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-125734-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison CO Closed Landfill
Lab Sample ID: 490-125734-3Client Sample ID: MW-03 OLD
Matrix: WaterDate Collected: 04/05/17 10:54
Date Received: 04/06/17 09:30
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 2.89 J 25.0 2.66 ug/L 04/12/17 20:53 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 04/12/17 20:53 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/12/17 20:53 1Benzene1.92
1.00 0.150 ug/L 04/12/17 20:53 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/12/17 20:53 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/12/17 20:53 1Bromoform<0.290
1.00 0.350 ug/L 04/12/17 20:53 1Bromomethane<0.350
50.0 2.64 ug/L 04/12/17 20:53 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 04/12/17 20:53 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/12/17 20:53 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/12/17 20:53 1Chlorobenzene5.81
1.00 0.360 ug/L 04/12/17 20:53 1Chloroethane0.771 J
1.00 0.230 ug/L 04/12/17 20:53 1Chloroform<0.230
1.00 0.360 ug/L 04/12/17 20:53 1Chloromethane<0.360
1.00 0.210 ug/L 04/12/17 20:53 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 04/12/17 20:53 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/12/17 20:53 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/12/17 20:53 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/12/17 20:53 11,2-Dibromoethane (EDB)<0.210 *
1.00 0.450 ug/L 04/12/17 20:53 1Dibromomethane<0.450
1.00 0.190 ug/L 04/12/17 20:53 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 04/12/17 20:53 11,4-Dichlorobenzene 3.35
1.00 0.240 ug/L 04/12/17 20:53 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 04/12/17 20:53 11,2-Dichloroethane <0.200 *
1.00 0.250 ug/L 04/12/17 20:53 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/12/17 20:53 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 04/12/17 20:53 1Ethylbenzene6.17
10.0 1.28 ug/L 04/12/17 20:53 12-Hexanone <1.28
10.0 1.50 ug/L 04/12/17 20:53 1Iodomethane<1.50
5.00 1.00 ug/L 04/12/17 20:53 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/12/17 20:53 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/12/17 20:53 1Styrene<0.280
1.00 0.150 ug/L 04/12/17 20:53 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/12/17 20:53 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/12/17 20:53 1Tetrachloroethene<0.140
1.00 0.170 ug/L 04/12/17 20:53 1Toluene<0.170
5.00 0.460 ug/L 04/12/17 20:53 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/12/17 20:53 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 04/12/17 20:53 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/12/17 20:53 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/12/17 20:53 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/12/17 20:53 1Trichloroethene<0.200
1.00 0.210 ug/L 04/12/17 20:53 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 04/12/17 20:53 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/12/17 20:53 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/12/17 20:53 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/12/17 20:53 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-125734-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison CO Closed Landfill
Lab Sample ID: 490-125734-3Client Sample ID: MW-03 OLD
Matrix: WaterDate Collected: 04/05/17 10:54
Date Received: 04/06/17 09:30
4-Bromofluorobenzene (Surr)103 70-130 04/12/17 20:53 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)106 04/12/17 20:53 170-130
1,2-Dichloroethane-d4 (Surr)112 04/12/17 20:53 170-130
Toluene-d8 (Surr)100 04/12/17 20:53 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 04/19/17 22:23 04/20/17 21:14 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 04/19/17 22:23 04/20/17 21:14 1Barium0.778
0.00100 0.000500 mg/L 04/19/17 22:23 04/20/17 21:14 1Cadmium0.000800 J
0.00500 0.00300 mg/L 04/19/17 22:23 04/20/17 21:14 1Chromium<0.00300
0.00500 0.00200 mg/L 04/19/17 22:23 04/20/17 21:14 1Lead0.0157
0.0100 0.00500 mg/L 04/19/17 22:23 04/23/17 04:39 1Selenium0.00520 J
0.00500 0.00300 mg/L 04/19/17 22:23 04/20/17 21:14 1Silver<0.00300
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 04/13/17 07:33 04/13/17 14:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-125734-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison CO Closed Landfill
Lab Sample ID: 490-125734-4Client Sample ID: MW-04 OLD
Matrix: WaterDate Collected: 04/05/17 11:46
Date Received: 04/06/17 09:30
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 5.22 J 25.0 2.66 ug/L 04/12/17 21:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 04/12/17 21:20 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/12/17 21:20 1Benzene0.275 J
1.00 0.150 ug/L 04/12/17 21:20 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/12/17 21:20 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/12/17 21:20 1Bromoform<0.290
1.00 0.350 ug/L 04/12/17 21:20 1Bromomethane<0.350
50.0 2.64 ug/L 04/12/17 21:20 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 04/12/17 21:20 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/12/17 21:20 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/12/17 21:20 1Chlorobenzene3.30
1.00 0.360 ug/L 04/12/17 21:20 1Chloroethane0.776 J
1.00 0.230 ug/L 04/12/17 21:20 1Chloroform<0.230
1.00 0.360 ug/L 04/12/17 21:20 1Chloromethane<0.360
1.00 0.210 ug/L 04/12/17 21:20 1cis-1,2-Dichloroethene 0.374 J
1.00 0.170 ug/L 04/12/17 21:20 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/12/17 21:20 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/12/17 21:20 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/12/17 21:20 11,2-Dibromoethane (EDB)<0.210 *
1.00 0.450 ug/L 04/12/17 21:20 1Dibromomethane<0.450
1.00 0.190 ug/L 04/12/17 21:20 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 04/12/17 21:20 11,4-Dichlorobenzene 1.84
1.00 0.240 ug/L 04/12/17 21:20 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 04/12/17 21:20 11,2-Dichloroethane <0.200 *
1.00 0.250 ug/L 04/12/17 21:20 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/12/17 21:20 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 04/12/17 21:20 1Ethylbenzene<0.190
10.0 1.28 ug/L 04/12/17 21:20 12-Hexanone <1.28
10.0 1.50 ug/L 04/12/17 21:20 1Iodomethane<1.50
5.00 1.00 ug/L 04/12/17 21:20 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/12/17 21:20 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/12/17 21:20 1Styrene<0.280
1.00 0.150 ug/L 04/12/17 21:20 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/12/17 21:20 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/12/17 21:20 1Tetrachloroethene<0.140
1.00 0.170 ug/L 04/12/17 21:20 1Toluene<0.170
5.00 0.460 ug/L 04/12/17 21:20 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/12/17 21:20 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 04/12/17 21:20 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/12/17 21:20 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/12/17 21:20 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/12/17 21:20 1Trichloroethene<0.200
1.00 0.210 ug/L 04/12/17 21:20 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 04/12/17 21:20 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/12/17 21:20 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/12/17 21:20 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/12/17 21:20 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-125734-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison CO Closed Landfill
Lab Sample ID: 490-125734-4Client Sample ID: MW-04 OLD
Matrix: WaterDate Collected: 04/05/17 11:46
Date Received: 04/06/17 09:30
4-Bromofluorobenzene (Surr)105 70-130 04/12/17 21:20 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)106 04/12/17 21:20 170-130
1,2-Dichloroethane-d4 (Surr)114 04/12/17 21:20 170-130
Toluene-d8 (Surr)101 04/12/17 21:20 170-130
Method: 6010D - Metals (ICP)
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 04/19/17 22:23 04/20/17 21:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00500 mg/L 04/19/17 22:23 04/20/17 21:19 1Barium0.728
0.00100 0.000500 mg/L 04/19/17 22:23 04/20/17 21:19 1Cadmium<0.000500
0.00500 0.00300 mg/L 04/19/17 22:23 04/20/17 21:19 1Chromium<0.00300
0.00500 0.00200 mg/L 04/19/17 22:23 04/20/17 21:19 1Lead0.00620
0.0100 0.00500 mg/L 04/19/17 22:23 04/23/17 04:44 1Selenium0.00550 J
0.00500 0.00300 mg/L 04/19/17 22:23 04/20/17 21:19 1Silver<0.00300
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 04/13/17 07:33 04/13/17 14:07 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-125734-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison CO Closed Landfill
Lab Sample ID: 490-125734-5Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 04/05/17 00:01
Date Received: 04/06/17 09:30
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 04/12/17 18:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 04/12/17 18:40 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/12/17 18:40 1Benzene<0.200
1.00 0.150 ug/L 04/12/17 18:40 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/12/17 18:40 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/12/17 18:40 1Bromoform<0.290
1.00 0.350 ug/L 04/12/17 18:40 1Bromomethane<0.350
50.0 2.64 ug/L 04/12/17 18:40 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 04/12/17 18:40 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/12/17 18:40 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/12/17 18:40 1Chlorobenzene<0.180
1.00 0.360 ug/L 04/12/17 18:40 1Chloroethane<0.360
1.00 0.230 ug/L 04/12/17 18:40 1Chloroform<0.230
1.00 0.360 ug/L 04/12/17 18:40 1Chloromethane<0.360
1.00 0.210 ug/L 04/12/17 18:40 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 04/12/17 18:40 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/12/17 18:40 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/12/17 18:40 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/12/17 18:40 11,2-Dibromoethane (EDB)<0.210 *
1.00 0.450 ug/L 04/12/17 18:40 1Dibromomethane<0.450
1.00 0.190 ug/L 04/12/17 18:40 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 04/12/17 18:40 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 04/12/17 18:40 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 04/12/17 18:40 11,2-Dichloroethane <0.200 *
1.00 0.250 ug/L 04/12/17 18:40 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/12/17 18:40 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 04/12/17 18:40 1Ethylbenzene<0.190
10.0 1.28 ug/L 04/12/17 18:40 12-Hexanone <1.28
10.0 1.50 ug/L 04/12/17 18:40 1Iodomethane<1.50
5.00 1.00 ug/L 04/12/17 18:40 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/12/17 18:40 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/12/17 18:40 1Styrene<0.280
1.00 0.150 ug/L 04/12/17 18:40 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/12/17 18:40 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/12/17 18:40 1Tetrachloroethene<0.140
1.00 0.170 ug/L 04/12/17 18:40 1Toluene<0.170
5.00 0.460 ug/L 04/12/17 18:40 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/12/17 18:40 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 04/12/17 18:40 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/12/17 18:40 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/12/17 18:40 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/12/17 18:40 1Trichloroethene<0.200
1.00 0.210 ug/L 04/12/17 18:40 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 04/12/17 18:40 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/12/17 18:40 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/12/17 18:40 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/12/17 18:40 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-125734-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison CO Closed Landfill
Lab Sample ID: 490-125734-5Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 04/05/17 00:01
Date Received: 04/06/17 09:30
4-Bromofluorobenzene (Surr)104 70-130 04/12/17 18:40 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)105 04/12/17 18:40 170-130
1,2-Dichloroethane-d4 (Surr)112 04/12/17 18:40 170-130
Toluene-d8 (Surr)100 04/12/17 18:40 170-130
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QC Sample Results
TestAmerica Job ID: 490-125734-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison CO Closed Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-421674/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 421674
RL MDL
Acetone <2.66 25.0 2.66 ug/L 04/12/17 15:59 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.500 0.50010.0 ug/L 04/12/17 15:59 1Acrylonitrile
<0.200 0.2001.00 ug/L 04/12/17 15:59 1Benzene
<0.150 0.1501.00 ug/L 04/12/17 15:59 1Bromochloromethane
<0.170 0.1701.00 ug/L 04/12/17 15:59 1Bromodichloromethane
<0.290 0.2901.00 ug/L 04/12/17 15:59 1Bromoform
<0.350 0.3501.00 ug/L 04/12/17 15:59 1Bromomethane
<2.64 2.6450.0 ug/L 04/12/17 15:59 12-Butanone (MEK)
<0.220 0.2201.00 ug/L 04/12/17 15:59 1Carbon disulfide
<0.180 0.1801.00 ug/L 04/12/17 15:59 1Carbon tetrachloride
<0.180 0.1801.00 ug/L 04/12/17 15:59 1Chlorobenzene
<0.360 0.3601.00 ug/L 04/12/17 15:59 1Chloroethane
<0.230 0.2301.00 ug/L 04/12/17 15:59 1Chloroform
<0.360 0.3601.00 ug/L 04/12/17 15:59 1Chloromethane
<0.210 0.2101.00 ug/L 04/12/17 15:59 1cis-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 04/12/17 15:59 1cis-1,3-Dichloropropene
<0.250 0.2501.00 ug/L 04/12/17 15:59 1Dibromochloromethane
<0.940 0.94010.0 ug/L 04/12/17 15:59 11,2-Dibromo-3-Chloropropane
<0.210 0.2101.00 ug/L 04/12/17 15:59 11,2-Dibromoethane (EDB)
<0.450 0.4501.00 ug/L 04/12/17 15:59 1Dibromomethane
<0.190 0.1901.00 ug/L 04/12/17 15:59 11,2-Dichlorobenzene
<0.170 0.1701.00 ug/L 04/12/17 15:59 11,4-Dichlorobenzene
<0.240 0.2401.00 ug/L 04/12/17 15:59 11,1-Dichloroethane
<0.200 0.2001.00 ug/L 04/12/17 15:59 11,2-Dichloroethane
<0.250 0.2501.00 ug/L 04/12/17 15:59 11,1-Dichloroethene
<0.250 0.2501.00 ug/L 04/12/17 15:59 11,2-Dichloropropane
<0.190 0.1901.00 ug/L 04/12/17 15:59 1Ethylbenzene
<1.28 1.2810.0 ug/L 04/12/17 15:59 12-Hexanone
<1.50 1.5010.0 ug/L 04/12/17 15:59 1Iodomethane
1.380 J 1.005.00 ug/L 04/12/17 15:59 1Methylene Chloride
<0.810 0.81010.0 ug/L 04/12/17 15:59 14-Methyl-2-pentanone (MIBK)
<0.280 0.2801.00 ug/L 04/12/17 15:59 1Styrene
<0.150 0.1501.00 ug/L 04/12/17 15:59 11,1,1,2-Tetrachloroethane
<0.190 0.1901.00 ug/L 04/12/17 15:59 11,1,2,2-Tetrachloroethane
<0.140 0.1401.00 ug/L 04/12/17 15:59 1Tetrachloroethene
<0.170 0.1701.00 ug/L 04/12/17 15:59 1Toluene
<0.460 0.4605.00 ug/L 04/12/17 15:59 1trans-1,4-Dichloro-2-butene
<0.230 0.2301.00 ug/L 04/12/17 15:59 1trans-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 04/12/17 15:59 1trans-1,3-Dichloropropene
<0.190 0.1901.00 ug/L 04/12/17 15:59 11,1,1-Trichloroethane
<0.190 0.1901.00 ug/L 04/12/17 15:59 11,1,2-Trichloroethane
<0.200 0.2001.00 ug/L 04/12/17 15:59 1Trichloroethene
<0.210 0.2101.00 ug/L 04/12/17 15:59 1Trichlorofluoromethane
<0.230 0.2301.00 ug/L 04/12/17 15:59 11,2,3-Trichloropropane
<1.71 1.7110.0 ug/L 04/12/17 15:59 1Vinyl acetate
<0.180 0.1801.00 ug/L 04/12/17 15:59 1Vinyl chloride
<0.580 0.5803.00 ug/L 04/12/17 15:59 1Xylenes, Total
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QC Sample Results
TestAmerica Job ID: 490-125734-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison CO Closed Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-421674/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 421674
4-Bromofluorobenzene (Surr)101 70-130 04/12/17 15:59 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
108 04/12/17 15:59 1Dibromofluoromethane (Surr)70-130
113 04/12/17 15:59 11,2-Dichloroethane-d4 (Surr)70-130
102 04/12/17 15:59 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-421674/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 421674
Acetone 100 101.0 ug/L 101 39-150
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Acrylonitrile 200 211.4 ug/L 106 63-135
Benzene 20.0 21.97 ug/L 110 70-130
Bromochloromethane 20.0 22.61 ug/L 113 70-130
Bromodichloromethane 20.0 24.11 ug/L 121 70-130
Bromoform 20.0 20.41 ug/L 102 70-137
Bromomethane 20.0 14.11 ug/L 71 53-150
2-Butanone (MEK)100 117.8 ug/L 118 55-143
Carbon disulfide 20.0 21.48 ug/L 107 64-135
Carbon tetrachloride 20.0 24.19 ug/L 121 70-147
Chlorobenzene 20.0 20.90 ug/L 105 70-130
Chloroethane 20.0 19.54 ug/L 98 60-138
Chloroform 20.0 22.15 ug/L 111 70-130
Chloromethane 20.0 18.21 ug/L 91 33-150
cis-1,2-Dichloroethene 20.0 21.95 ug/L 110 70-130
cis-1,3-Dichloropropene 20.0 22.10 ug/L 111 70-133
Dibromochloromethane 20.0 22.25 ug/L 111 70-133
1,2-Dibromo-3-Chloropropane 20.0 18.99 ug/L 95 45-138
1,2-Dibromoethane (EDB)20.0 22.96 ug/L 115 70-130
Dibromomethane 20.0 22.47 ug/L 112 70-130
1,2-Dichlorobenzene 20.0 20.41 ug/L 102 70-130
1,4-Dichlorobenzene 20.0 20.41 ug/L 102 70-130
1,1-Dichloroethane 20.0 21.77 ug/L 109 70-130
1,2-Dichloroethane 20.0 24.07 ug/L 120 70-130
1,1-Dichloroethene 20.0 21.75 ug/L 109 70-132
1,2-Dichloropropane 20.0 21.55 ug/L 108 70-130
Ethylbenzene 20.0 20.59 ug/L 103 70-130
2-Hexanone 100 106.5 ug/L 107 54-142
Iodomethane 20.0 16.92 ug/L 85 40-150
Methylene Chloride 20.0 22.03 ug/L 110 70-130
4-Methyl-2-pentanone (MIBK)100 109.2 ug/L 109 60-137
Styrene 20.0 20.67 ug/L 103 70-130
1,1,1,2-Tetrachloroethane 20.0 20.94 ug/L 105 70-130
1,1,2,2-Tetrachloroethane 20.0 22.19 ug/L 111 69-131
Tetrachloroethene 20.0 22.32 ug/L 112 70-130
Toluene 20.0 21.32 ug/L 107 70-130
trans-1,4-Dichloro-2-butene 20.0 27.65 ug/L 138 41-150
trans-1,2-Dichloroethene 20.0 22.58 ug/L 113 70-130
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QC Sample Results
TestAmerica Job ID: 490-125734-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison CO Closed Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-421674/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 421674
trans-1,3-Dichloropropene 20.0 21.79 ug/L 109 63-142
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,1,1-Trichloroethane 20.0 23.29 ug/L 116 70-135
1,1,2-Trichloroethane 20.0 22.61 ug/L 113 70-130
Trichloroethene 20.0 22.98 ug/L 115 70-130
Trichlorofluoromethane 20.0 20.79 ug/L 104 59-150
1,2,3-Trichloropropane 20.0 21.85 ug/L 109 70-131
Vinyl acetate 40.0 49.16 ug/L 123 54-146
Vinyl chloride 20.0 20.89 ug/L 104 57-137
Xylenes, Total 40.0 40.53 ug/L 101 70-132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
102
LCS LCS
Qualifier Limits%Recovery
110Dibromofluoromethane (Surr)70 -130
1091,2-Dichloroethane-d4 (Surr)70 -130
101Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-421674/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 421674
Acetone 100 88.21 ug/L 88 39-150 14 23
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acrylonitrile 200 202.8 ug/L 101 63-135 4 16
Benzene 20.0 19.78 ug/L 99 70-130 11 12
Bromochloromethane 20.0 20.37 ug/L 102 70-130 10 16
Bromodichloromethane 20.0 20.99 ug/L 105 70-130 14 14
Bromoform 20.0 18.03 ug/L 90 70-137 12 14
Bromomethane 20.0 15.35 ug/L 77 53-150 8 19
2-Butanone (MEK)100 101.8 ug/L 102 55-143 15 19
Carbon disulfide 20.0 19.21 ug/L 96 64-135 11 16
Carbon tetrachloride 20.0 22.34 ug/L 112 70-147 8 16
Chlorobenzene 20.0 18.93 ug/L 95 70-130 10 12
Chloroethane 20.0 20.42 ug/L 102 60-138 4 15
Chloroform 20.0 19.86 ug/L 99 70-130 11 14
Chloromethane 20.0 19.13 ug/L 96 33-150 5 20
cis-1,2-Dichloroethene 20.0 19.95 ug/L 100 70-130 10 15
cis-1,3-Dichloropropene 20.0 19.58 ug/L 98 70-133 12 15
Dibromochloromethane 20.0 19.52 ug/L 98 70-133 13 13
1,2-Dibromo-3-Chloropropane 20.0 16.28 ug/L 81 45-138 15 19
1,2-Dibromoethane (EDB)20.0 20.04 *ug/L 100 70-130 14 13
Dibromomethane 20.0 20.34 ug/L 102 70-130 10 14
1,2-Dichlorobenzene 20.0 18.33 ug/L 92 70-130 11 12
1,4-Dichlorobenzene 20.0 18.63 ug/L 93 70-130 9 12
1,1-Dichloroethane 20.0 19.93 ug/L 100 70-130 9 17
1,2-Dichloroethane 20.0 20.53 *ug/L 103 70-130 16 13
1,1-Dichloroethene 20.0 19.93 ug/L 100 70-132 9 20
1,2-Dichloropropane 20.0 19.39 ug/L 97 70-130 11 15
Ethylbenzene 20.0 18.69 ug/L 93 70-130 10 12
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QC Sample Results
TestAmerica Job ID: 490-125734-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison CO Closed Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-421674/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 421674
2-Hexanone 100 94.39 ug/L 94 54-142 12 17
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Iodomethane 20.0 16.86 ug/L 84 40-150 0 20
Methylene Chloride 20.0 19.37 ug/L 97 70-130 13 15
4-Methyl-2-pentanone (MIBK)100 95.67 ug/L 96 60-137 13 21
Styrene 20.0 18.61 ug/L 93 70-130 10 12
1,1,1,2-Tetrachloroethane 20.0 19.14 ug/L 96 70-130 9 13
1,1,2,2-Tetrachloroethane 20.0 19.52 ug/L 98 69-131 13 15
Tetrachloroethene 20.0 20.28 ug/L 101 70-130 10 17
Toluene 20.0 19.26 ug/L 96 70-130 10 13
trans-1,4-Dichloro-2-butene 20.0 25.50 ug/L 127 41-150 8 20
trans-1,2-Dichloroethene 20.0 19.98 ug/L 100 70-130 12 15
trans-1,3-Dichloropropene 20.0 19.70 ug/L 99 63-142 10 13
1,1,1-Trichloroethane 20.0 21.52 ug/L 108 70-135 8 15
1,1,2-Trichloroethane 20.0 20.62 ug/L 103 70-130 9 13
Trichloroethene 20.0 20.21 ug/L 101 70-130 13 14
Trichlorofluoromethane 20.0 22.75 ug/L 114 59-150 9 22
1,2,3-Trichloropropane 20.0 19.25 ug/L 96 70-131 13 14
Vinyl acetate 40.0 42.37 ug/L 106 54-146 15 20
Vinyl chloride 20.0 22.33 ug/L 112 57-137 7 15
Xylenes, Total 40.0 36.38 ug/L 91 70-132 11 11
4-Bromofluorobenzene (Surr)70 -130
Surrogate
103
LCSD LCSD
Qualifier Limits%Recovery
103Dibromofluoromethane (Surr)70 -130
1101,2-Dichloroethane-d4 (Surr)70 -130
101Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix SpikeLab Sample ID: 490-125799-B-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 421674
Acetone 3.13 J 100 80.63 ug/L 77 39-150
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acrylonitrile <0.500 200 183.7 ug/L 92 50-135
Benzene <0.200 20.0 19.62 ug/L 98 55-147
Bromochloromethane <0.150 20.0 19.93 ug/L 100 59-132
Bromodichloromethane <0.170 20.0 20.69 ug/L 103 70-140
Bromoform <0.290 20.0 16.06 ug/L 80 53-150
Bromomethane <0.350 20.0 15.55 ug/L 78 30-150
2-Butanone (MEK)<2.64 100 89.53 ug/L 90 50-143
Carbon disulfide <0.220 20.0 17.09 ug/L 85 35-150
Carbon tetrachloride <0.180 20.0 20.75 ug/L 104 56-150
Chlorobenzene <0.180 20.0 18.71 ug/L 94 70-130
Chloroethane <0.360 20.0 19.05 ug/L 95 58-141
Chloroform <0.230 20.0 19.78 ug/L 99 66-138
Chloromethane <0.360 20.0 17.53 ug/L 88 10-150
cis-1,2-Dichloroethene <0.210 20.0 19.85 ug/L 99 68-131
cis-1,3-Dichloropropene <0.170 20.0 18.70 ug/L 93 70-133
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QC Sample Results
TestAmerica Job ID: 490-125734-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison CO Closed Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-125799-B-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 421674
Dibromochloromethane <0.250 20.0 18.26 ug/L 91 66-140
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
1,2-Dibromo-3-Chloropropane <0.940 20.0 14.39 ug/L 72 38-138
1,2-Dibromoethane (EDB)<0.210 *20.0 19.01 ug/L 95 65-137
Dibromomethane <0.450 20.0 19.30 ug/L 96 70-130
1,2-Dichlorobenzene <0.190 20.0 17.76 ug/L 89 70-130
1,4-Dichlorobenzene <0.170 20.0 18.31 ug/L 92 70-130
1,1-Dichloroethane <0.240 20.0 19.93 ug/L 100 61-139
1,2-Dichloroethane <0.200 *20.0 19.60 ug/L 98 64-136
1,1-Dichloroethene <0.250 20.0 19.65 ug/L 98 54-150
1,2-Dichloropropane <0.250 20.0 19.47 ug/L 97 67-130
Ethylbenzene <0.190 20.0 19.09 ug/L 95 65-139
2-Hexanone <1.28 100 86.22 ug/L 86 44-150
Iodomethane <1.50 20.0 15.50 ug/L 78 34-150
Methylene Chloride <1.00 20.0 18.93 ug/L 95 64-130
4-Methyl-2-pentanone (MIBK)<0.810 100 89.16 ug/L 89 50-140
Styrene <0.280 20.0 18.12 ug/L 91 70-130
1,1,1,2-Tetrachloroethane <0.150 20.0 18.28 ug/L 91 70-131
1,1,2,2-Tetrachloroethane <0.190 20.0 18.79 ug/L 94 56-145
Tetrachloroethene <0.140 20.0 19.97 ug/L 100 57-138
Toluene <0.170 20.0 20.59 ug/L 103 64-136
trans-1,4-Dichloro-2-butene <0.460 20.0 23.51 ug/L 118 39-150
trans-1,2-Dichloroethene <0.230 20.0 19.98 ug/L 100 59-143
trans-1,3-Dichloropropene <0.170 20.0 18.52 ug/L 93 63-142
1,1,1-Trichloroethane <0.190 20.0 21.21 ug/L 106 68-144
1,1,2-Trichloroethane <0.190 20.0 19.41 ug/L 97 70-130
Trichloroethene <0.200 20.0 20.37 ug/L 102 63-135
Trichlorofluoromethane <0.210 20.0 21.62 ug/L 108 44-150
1,2,3-Trichloropropane <0.230 20.0 18.38 ug/L 92 65-131
Vinyl acetate <1.71 40.0 38.26 ug/L 96 43-146
Vinyl chloride <0.180 20.0 20.11 ug/L 101 57-150
Xylenes, Total <0.580 40.0 37.03 ug/L 93 69-132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
106
MS MS
Qualifier Limits%Recovery
106Dibromofluoromethane (Surr)70 -130
1071,2-Dichloroethane-d4 (Surr)70 -130
102Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-125799-C-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 421674
Acetone 3.13 J 100 84.83 ug/L 82 39-150 5 28
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acrylonitrile <0.500 200 183.1 ug/L 92 50-135 0 23
Benzene <0.200 20.0 19.78 ug/L 99 55-147 1 22
Bromochloromethane <0.150 20.0 20.14 ug/L 101 59-132 1 21
Bromodichloromethane <0.170 20.0 20.77 ug/L 104 70-140 0 196
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QC Sample Results
TestAmerica Job ID: 490-125734-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison CO Closed Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-125799-C-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 421674
Bromoform <0.290 20.0 16.50 ug/L 82 53-150 3 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Bromomethane <0.350 20.0 16.46 ug/L 82 30-150 6 44
2-Butanone (MEK)<2.64 100 96.14 ug/L 96 50-143 7 28
Carbon disulfide <0.220 20.0 17.31 ug/L 87 35-150 1 34
Carbon tetrachloride <0.180 20.0 21.32 ug/L 107 56-150 3 18
Chlorobenzene <0.180 20.0 18.82 ug/L 94 70-130 1 15
Chloroethane <0.360 20.0 18.86 ug/L 94 58-141 1 31
Chloroform <0.230 20.0 19.93 ug/L 100 66-138 1 21
Chloromethane <0.360 20.0 16.44 ug/L 82 10-150 6 43
cis-1,2-Dichloroethene <0.210 20.0 19.73 ug/L 99 68-131 1 21
cis-1,3-Dichloropropene <0.170 20.0 18.27 ug/L 91 70-133 2 19
Dibromochloromethane <0.250 20.0 18.55 ug/L 93 66-140 2 19
1,2-Dibromo-3-Chloropropane <0.940 20.0 14.77 ug/L 74 38-138 3 26
1,2-Dibromoethane (EDB)<0.210 *20.0 18.92 ug/L 95 65-137 0 21
Dibromomethane <0.450 20.0 19.32 ug/L 97 70-130 0 19
1,2-Dichlorobenzene <0.190 20.0 17.67 ug/L 88 70-130 0 15
1,4-Dichlorobenzene <0.170 20.0 17.95 ug/L 90 70-130 2 14
1,1-Dichloroethane <0.240 20.0 19.52 ug/L 98 61-139 2 23
1,2-Dichloroethane <0.200 *20.0 19.85 ug/L 99 64-136 1 22
1,1-Dichloroethene <0.250 20.0 19.99 ug/L 100 54-150 2 24
1,2-Dichloropropane <0.250 20.0 19.39 ug/L 97 67-130 0 19
Ethylbenzene <0.190 20.0 18.89 ug/L 94 65-139 1 18
2-Hexanone <1.28 100 91.07 ug/L 91 44-150 5 21
Iodomethane <1.50 20.0 16.19 ug/L 81 34-150 4 37
Methylene Chloride <1.00 20.0 18.24 ug/L 91 64-130 4 22
4-Methyl-2-pentanone (MIBK)<0.810 100 93.36 ug/L 93 50-140 5 24
Styrene <0.280 20.0 18.52 ug/L 93 70-130 2 16
1,1,1,2-Tetrachloroethane <0.150 20.0 18.68 ug/L 93 70-131 2 16
1,1,2,2-Tetrachloroethane <0.190 20.0 19.29 ug/L 96 56-145 3 19
Tetrachloroethene <0.140 20.0 20.76 ug/L 104 57-138 4 17
Toluene <0.170 20.0 19.46 ug/L 97 64-136 6 18
trans-1,4-Dichloro-2-butene <0.460 20.0 22.52 ug/L 113 39-150 4 28
trans-1,2-Dichloroethene <0.230 20.0 19.95 ug/L 100 59-143 0 25
trans-1,3-Dichloropropene <0.170 20.0 18.50 ug/L 92 63-142 0 18
1,1,1-Trichloroethane <0.190 20.0 21.86 ug/L 109 68-144 3 17
1,1,2-Trichloroethane <0.190 20.0 19.86 ug/L 99 70-130 2 18
Trichloroethene <0.200 20.0 19.95 ug/L 100 63-135 2 17
Trichlorofluoromethane <0.210 20.0 21.74 ug/L 109 44-150 1 32
1,2,3-Trichloropropane <0.230 20.0 18.70 ug/L 94 65-131 2 19
Vinyl acetate <1.71 40.0 39.15 ug/L 98 43-146 2 20
Vinyl chloride <0.180 20.0 20.51 ug/L 103 57-150 2 37
Xylenes, Total <0.580 40.0 37.01 ug/L 93 69-132 0 17
4-Bromofluorobenzene (Surr)70 -130
Surrogate
106
MSD MSD
Qualifier Limits%Recovery
107Dibromofluoromethane (Surr)70 -130
1051,2-Dichloroethane-d4 (Surr)70 -130
102Toluene-d8 (Surr)70 -130
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Page 21 of 33 5/8/2017
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QC Sample Results
TestAmerica Job ID: 490-125734-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison CO Closed Landfill
Method: 6010D - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 490-423512/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 423913 Prep Batch: 423512
RL MDL
Arsenic <0.00860 0.0100 0.00860 mg/L 04/19/17 22:23 04/20/17 19:59 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.00500 0.005000.0100 mg/L 04/19/17 22:23 04/20/17 19:59 1Barium
<0.000500 0.0005000.00100 mg/L 04/19/17 22:23 04/20/17 19:59 1Cadmium
<0.00300 0.003000.00500 mg/L 04/19/17 22:23 04/20/17 19:59 1Chromium
<0.00200 0.002000.00500 mg/L 04/19/17 22:23 04/20/17 19:59 1Lead
<0.00300 0.003000.00500 mg/L 04/19/17 22:23 04/20/17 19:59 1Silver
Client Sample ID: Method BlankLab Sample ID: MB 490-423512/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 424419 Prep Batch: 423512
RL MDL
Selenium <0.00500 0.0100 0.00500 mg/L 04/19/17 22:23 04/23/17 03:37 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-423512/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 423913 Prep Batch: 423512
Arsenic 0.100 0.08600 mg/L 86 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Barium 0.100 0.09510 mg/L 95 80-120
Cadmium 0.100 0.08880 mg/L 89 80-120
Chromium 0.100 0.09270 mg/L 93 80-120
Lead 0.100 0.09190 mg/L 92 80-120
Silver 0.100 0.09550 mg/L 96 80-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-423512/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 424419 Prep Batch: 423512
Selenium 0.100 0.09600 mg/L 96 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-423512/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 423913 Prep Batch: 423512
Arsenic 0.100 0.08560 mg/L 86 80-120 0 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Barium 0.100 0.09210 mg/L 92 80-120 3 20
Cadmium 0.100 0.08850 mg/L 89 80-120 0 20
Chromium 0.100 0.09340 mg/L 93 80-120 1 20
Lead 0.100 0.08980 mg/L 90 80-120 2 20
Silver 0.100 0.09450 mg/L 95 80-120 1 20
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QC Sample Results
TestAmerica Job ID: 490-125734-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison CO Closed Landfill
Method: 6010D - Metals (ICP) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-423512/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 424419 Prep Batch: 423512
Selenium 0.100 0.09590 mg/L 96 80-120 0 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Client Sample ID: Matrix SpikeLab Sample ID: 490-126186-B-1-B MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 423913 Prep Batch: 423512
Arsenic <0.00860 0.100 0.09020 mg/L 90 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Barium 0.0142 0.100 0.1055 mg/L 91 75-125
Cadmium <0.000500 L 0.100 0.08000 mg/L 80 75-125
Chromium <0.00300 0.100 0.08620 mg/L 86 75-125
Lead <0.00200 0.100 0.08320 mg/L 83 75-125
Silver <0.00300 0.100 0.09850 mg/L 99 75-125
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-126186-B-1-C MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 423913 Prep Batch: 423512
Arsenic <0.00860 0.100 0.09970 mg/L 100 75-125 10 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Barium 0.0142 0.100 0.1086 mg/L 94 75-125 3 20
Cadmium <0.000500 L 0.100 0.08310 mg/L 83 75-125 4 20
Chromium <0.00300 0.100 0.09140 mg/L 91 75-125 6 20
Lead <0.00200 0.100 0.08700 mg/L 87 75-125 4 20
Silver <0.00300 0.100 0.1040 mg/L 104 75-125 5 20
Method: 7470A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 490-421871/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 422047 Prep Batch: 421871
RL MDL
Mercury 0.1001 J 0.200 0.100 ug/L 04/13/17 07:33 04/13/17 13:02 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-421871/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 422047 Prep Batch: 421871
Mercury 1.00 1.085 ug/L 109 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-421871/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 422047 Prep Batch: 421871
Mercury 1.00 1.033 ug/L 103 80-120 5 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
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QC Sample Results
TestAmerica Job ID: 490-125734-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison CO Closed Landfill
Method: 7470A - Mercury (CVAA) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 460-131124-B-2-C MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 422047 Prep Batch: 421871
Mercury <0.100 1.00 1.228 ug/L 123 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 460-131124-B-2-D MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 422047 Prep Batch: 421871
Mercury <0.100 1.00 1.180 ug/L 118 75-125 4 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
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QC Association Summary
TestAmerica Job ID: 490-125734-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison CO Closed Landfill
GC/MS VOA
Analysis Batch: 421674
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B490-125734-1 MW-01 OLD Total/NA
Water 8260B490-125734-2 MW-02 OLD Total/NA
Water 8260B490-125734-3 MW-03 OLD Total/NA
Water 8260B490-125734-4 MW-04 OLD Total/NA
Water 8260B490-125734-5 Trip Blank Total/NA
Water 8260BMB 490-421674/6 Method Blank Total/NA
Water 8260BLCS 490-421674/3 Lab Control Sample Total/NA
Water 8260BLCSD 490-421674/4 Lab Control Sample Dup Total/NA
Water 8260B490-125799-B-1 MS Matrix Spike Total/NA
Water 8260B490-125799-C-1 MSD Matrix Spike Duplicate Total/NA
Metals
Prep Batch: 421871
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A490-125734-1 MW-01 OLD Total/NA
Water 7470A490-125734-2 MW-02 OLD Total/NA
Water 7470A490-125734-3 MW-03 OLD Total/NA
Water 7470A490-125734-4 MW-04 OLD Total/NA
Water 7470AMB 490-421871/1-A Method Blank Total/NA
Water 7470ALCS 490-421871/2-A Lab Control Sample Total/NA
Water 7470ALCSD 490-421871/3-A Lab Control Sample Dup Total/NA
Water 7470A460-131124-B-2-C MS Matrix Spike Total/NA
Water 7470A460-131124-B-2-D MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 422047
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 421871490-125734-1 MW-01 OLD Total/NA
Water 7470A 421871490-125734-2 MW-02 OLD Total/NA
Water 7470A 421871490-125734-3 MW-03 OLD Total/NA
Water 7470A 421871490-125734-4 MW-04 OLD Total/NA
Water 7470A 421871MB 490-421871/1-A Method Blank Total/NA
Water 7470A 421871LCS 490-421871/2-A Lab Control Sample Total/NA
Water 7470A 421871LCSD 490-421871/3-A Lab Control Sample Dup Total/NA
Water 7470A 421871460-131124-B-2-C MS Matrix Spike Total/NA
Water 7470A 421871460-131124-B-2-D MSD Matrix Spike Duplicate Total/NA
Prep Batch: 423512
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-125734-1 MW-01 OLD Total/NA
Water 3010A490-125734-2 MW-02 OLD Total/NA
Water 3010A490-125734-3 MW-03 OLD Total/NA
Water 3010A490-125734-4 MW-04 OLD Total/NA
Water 3010AMB 490-423512/1-A Method Blank Total/NA
Water 3010ALCS 490-423512/2-A Lab Control Sample Total/NA
Water 3010ALCSD 490-423512/3-A Lab Control Sample Dup Total/NA
Water 3010A490-126186-B-1-B MS Matrix Spike Total/NA
Water 3010A490-126186-B-1-C MSD Matrix Spike Duplicate Total/NA
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QC Association Summary
TestAmerica Job ID: 490-125734-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison CO Closed Landfill
Metals (Continued)
Analysis Batch: 423913
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010D 423512490-125734-1 MW-01 OLD Total/NA
Water 6010D 423512490-125734-2 MW-02 OLD Total/NA
Water 6010D 423512490-125734-3 MW-03 OLD Total/NA
Water 6010D 423512490-125734-4 MW-04 OLD Total/NA
Water 6010D 423512MB 490-423512/1-A Method Blank Total/NA
Water 6010D 423512LCS 490-423512/2-A Lab Control Sample Total/NA
Water 6010D 423512LCSD 490-423512/3-A Lab Control Sample Dup Total/NA
Water 6010D 423512490-126186-B-1-B MS Matrix Spike Total/NA
Water 6010D 423512490-126186-B-1-C MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 424419
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010D 423512490-125734-1 MW-01 OLD Total/NA
Water 6010D 423512490-125734-2 MW-02 OLD Total/NA
Water 6010D 423512490-125734-3 MW-03 OLD Total/NA
Water 6010D 423512490-125734-4 MW-04 OLD Total/NA
Water 6010D 423512MB 490-423512/1-A Method Blank Total/NA
Water 6010D 423512LCS 490-423512/2-A Lab Control Sample Total/NA
Water 6010D 423512LCSD 490-423512/3-A Lab Control Sample Dup Total/NA
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Lab Chronicle
Client: Anchor QEA of North Carolina PLLC TestAmerica Job ID: 490-125734-1
Project/Site: Madison CO Closed Landfill
Client Sample ID: MW-01 OLD Lab Sample ID: 490-125734-1
Matrix: WaterDate Collected: 04/05/17 09:36
Date Received: 04/06/17 09:30
Analysis 8260B JJR04/12/17 20:001 TAL NSH421674
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3010A 423512 04/19/17 22:23 JSF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 423913 04/20/17 21:03 LCS TAL NSHTotal/NA
Prep 3010A 423512 04/19/17 22:23 JSF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 424419 04/23/17 04:29 RDF TAL NSHTotal/NA
Prep 7470A 421871 04/13/17 07:33 CAH TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 422047 04/13/17 13:59 CAH TAL NSHTotal/NA
Client Sample ID: MW-02 OLD Lab Sample ID: 490-125734-2
Matrix: WaterDate Collected: 04/05/17 12:25
Date Received: 04/06/17 09:30
Analysis 8260B JJR04/12/17 20:271 TAL NSH421674
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3010A 423512 04/19/17 22:23 JSF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 423913 04/20/17 21:08 LCS TAL NSHTotal/NA
Prep 3010A 423512 04/19/17 22:23 JSF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 424419 04/23/17 04:34 RDF TAL NSHTotal/NA
Prep 7470A 421871 04/13/17 07:33 CAH TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 422047 04/13/17 14:02 CAH TAL NSHTotal/NA
Client Sample ID: MW-03 OLD Lab Sample ID: 490-125734-3
Matrix: WaterDate Collected: 04/05/17 10:54
Date Received: 04/06/17 09:30
Analysis 8260B JJR04/12/17 20:531 TAL NSH421674
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3010A 423512 04/19/17 22:23 JSF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 423913 04/20/17 21:14 LCS TAL NSHTotal/NA
Prep 3010A 423512 04/19/17 22:23 JSF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 424419 04/23/17 04:39 RDF TAL NSHTotal/NA
Prep 7470A 421871 04/13/17 07:33 CAH TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 422047 04/13/17 14:05 CAH TAL NSHTotal/NA
Client Sample ID: MW-04 OLD Lab Sample ID: 490-125734-4
Matrix: WaterDate Collected: 04/05/17 11:46
Date Received: 04/06/17 09:30
Analysis 8260B JJR04/12/17 21:201 TAL NSH421674
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3010A 423512 04/19/17 22:23 JSF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 423913 04/20/17 21:19 LCS TAL NSHTotal/NA
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Lab Chronicle
Client: Anchor QEA of North Carolina PLLC TestAmerica Job ID: 490-125734-1
Project/Site: Madison CO Closed Landfill
Client Sample ID: MW-04 OLD Lab Sample ID: 490-125734-4
Matrix: WaterDate Collected: 04/05/17 11:46
Date Received: 04/06/17 09:30
Prep 3010A JSF04/19/17 22:23 TAL NSH423512
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 50 mL 50 mL
Analysis 6010D 1 424419 04/23/17 04:44 RDF TAL NSHTotal/NA
Prep 7470A 421871 04/13/17 07:33 CAH TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 422047 04/13/17 14:07 CAH TAL NSHTotal/NA
Client Sample ID: Trip Blank Lab Sample ID: 490-125734-5
Matrix: WaterDate Collected: 04/05/17 00:01
Date Received: 04/06/17 09:30
Analysis 8260B JJR04/12/17 18:401 TAL NSH421674
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
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Method Summary
TestAmerica Job ID: 490-125734-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison CO Closed Landfill
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL NSH
SW8466010DMetals (ICP)TAL NSH
SW8467470AMercury (CVAA)TAL NSH
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
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Accreditation/Certification Summary
Client: Anchor QEA of North Carolina PLLC TestAmerica Job ID: 490-125734-1
Project/Site: Madison CO Closed Landfill
Laboratory: TestAmerica Nashville
The accreditations/certifications listed below are applicable to this report.
Authority Program EPA Region Identification Number Expiration Date
North Carolina (WW/SW)3874State Program 12-31-17
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Login Sample Receipt Checklist
Client: Anchor QEA of North Carolina PLLC Job Number: 490-125734-1
Login Number: 125734
Question Answer Comment
Creator: West, Derrick D
List Source: TestAmerica Nashville
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Nashville
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ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: [phone]
TestAmerica Job ID: 490-125742-1
Client Project/Site: Madison Co Closed Landfill
For:
Anchor QEA of North Carolina PLLC
231 W Haywood Street
Asheville, North Carolina 28801
Attn: Brian Gant
Authorized for release by:
4/20/2017 1:27:11 PM
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison Co Closed Landfill
TestAmerica Job ID: 490-125742-1
Page 2 of 33 TestAmerica Nashville4/20/2017
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .16
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .25
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .27
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .29
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .30
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .31
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .33
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Sample Summary
TestAmerica Job ID: 490-125742-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison Co Closed Landfill
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-125742-1 BG Spring OLD Water 04/05/17 14:10 04/06/17 09:30
490-125742-2 SW-01 OLD Water 04/05/17 12:35 04/06/17 09:30
490-125742-3 SW-02 OLD Water 04/05/17 13:40 04/06/17 09:30
490-125742-4 DW-01 OLD Water 04/05/17 13:20 04/06/17 09:30
490-125742-5 Trip Blank Water 04/05/17 00:01 04/06/17 09:30
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Case Narrative
Client: Anchor QEA of North Carolina PLLC TestAmerica Job ID: 490-125742-1
Project/Site: Madison Co Closed Landfill
Job ID: 490-125742-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-125742-1
Comments
No additional comments.
Receipt
The samples were received on 4/6/2017 9:30 AM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 1.8º C.
GC/MS VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
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Definitions/Glossary
TestAmerica Job ID: 490-125742-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison Co Closed Landfill
Qualifiers
GC/MS VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
Metals
Qualifier Description
F1 MS and/or MSD Recovery is outside acceptance limits.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Client Sample Results
TestAmerica Job ID: 490-125742-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-125742-1Client Sample ID: BG Spring OLD
Matrix: WaterDate Collected: 04/05/17 14:10
Date Received: 04/06/17 09:30
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 04/12/17 14:25 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 04/12/17 14:25 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/12/17 14:25 1Benzene<0.200
1.00 0.150 ug/L 04/12/17 14:25 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/12/17 14:25 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/12/17 14:25 1Bromoform<0.290
1.00 0.350 ug/L 04/12/17 14:25 1Bromomethane<0.350
50.0 2.64 ug/L 04/12/17 14:25 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 04/12/17 14:25 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/12/17 14:25 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/12/17 14:25 1Chlorobenzene<0.180
1.00 0.360 ug/L 04/12/17 14:25 1Chloroethane<0.360
1.00 0.230 ug/L 04/12/17 14:25 1Chloroform<0.230
1.00 0.360 ug/L 04/12/17 14:25 1Chloromethane<0.360
1.00 0.210 ug/L 04/12/17 14:25 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 04/12/17 14:25 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/12/17 14:25 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/12/17 14:25 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/12/17 14:25 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 04/12/17 14:25 1Dibromomethane<0.450
1.00 0.190 ug/L 04/12/17 14:25 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 04/12/17 14:25 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 04/12/17 14:25 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 04/12/17 14:25 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 04/12/17 14:25 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/12/17 14:25 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 04/12/17 14:25 1Ethylbenzene<0.190
10.0 1.28 ug/L 04/12/17 14:25 12-Hexanone <1.28
10.0 1.50 ug/L 04/12/17 14:25 1Iodomethane<1.50
5.00 1.00 ug/L 04/12/17 14:25 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/12/17 14:25 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/12/17 14:25 1Styrene<0.280
1.00 0.150 ug/L 04/12/17 14:25 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/12/17 14:25 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/12/17 14:25 1Tetrachloroethene<0.140
1.00 0.170 ug/L 04/12/17 14:25 1Toluene<0.170
5.00 0.460 ug/L 04/12/17 14:25 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/12/17 14:25 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 04/12/17 14:25 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/12/17 14:25 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/12/17 14:25 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/12/17 14:25 1Trichloroethene<0.200
1.00 0.210 ug/L 04/12/17 14:25 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 04/12/17 14:25 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/12/17 14:25 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/12/17 14:25 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/12/17 14:25 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-125742-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-125742-1Client Sample ID: BG Spring OLD
Matrix: WaterDate Collected: 04/05/17 14:10
Date Received: 04/06/17 09:30
4-Bromofluorobenzene (Surr)88 70-130 04/12/17 14:25 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)96 04/12/17 14:25 170-130
1,2-Dichloroethane-d4 (Surr)91 04/12/17 14:25 170-130
Toluene-d8 (Surr)90 04/12/17 14:25 170-130
Method: 6010D - Metals (ICP)
RL MDL
Silver <0.00300 0.00500 0.00300 mg/L 04/17/17 16:25 04/20/17 01:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00860 mg/L 04/17/17 16:25 04/20/17 01:01 1Arsenic<0.00860
0.0100 0.00500 mg/L 04/17/17 16:25 04/20/17 01:01 1Barium0.101
0.00100 0.000500 mg/L 04/17/17 16:25 04/20/17 01:01 1Cadmium<0.000500
0.00500 0.00300 mg/L 04/17/17 16:25 04/20/17 01:01 1Chromium0.00670
0.00500 0.00200 mg/L 04/17/17 16:25 04/20/17 01:01 1Lead<0.00200
0.0100 0.00500 mg/L 04/17/17 16:25 04/20/17 01:01 1Selenium<0.00500
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 04/13/17 07:33 04/13/17 14:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-125742-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-125742-2Client Sample ID: SW-01 OLD
Matrix: WaterDate Collected: 04/05/17 12:35
Date Received: 04/06/17 09:30
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 04/12/17 19:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 04/12/17 19:21 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/12/17 19:21 1Benzene<0.200
1.00 0.150 ug/L 04/12/17 19:21 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/12/17 19:21 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/12/17 19:21 1Bromoform<0.290
1.00 0.350 ug/L 04/12/17 19:21 1Bromomethane<0.350
50.0 2.64 ug/L 04/12/17 19:21 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 04/12/17 19:21 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/12/17 19:21 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/12/17 19:21 1Chlorobenzene<0.180
1.00 0.360 ug/L 04/12/17 19:21 1Chloroethane<0.360
1.00 0.230 ug/L 04/12/17 19:21 1Chloroform<0.230
1.00 0.360 ug/L 04/12/17 19:21 1Chloromethane<0.360
1.00 0.210 ug/L 04/12/17 19:21 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 04/12/17 19:21 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/12/17 19:21 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/12/17 19:21 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/12/17 19:21 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 04/12/17 19:21 1Dibromomethane<0.450
1.00 0.190 ug/L 04/12/17 19:21 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 04/12/17 19:21 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 04/12/17 19:21 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 04/12/17 19:21 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 04/12/17 19:21 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/12/17 19:21 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 04/12/17 19:21 1Ethylbenzene<0.190
10.0 1.28 ug/L 04/12/17 19:21 12-Hexanone <1.28
10.0 1.50 ug/L 04/12/17 19:21 1Iodomethane<1.50
5.00 1.00 ug/L 04/12/17 19:21 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/12/17 19:21 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/12/17 19:21 1Styrene<0.280
1.00 0.150 ug/L 04/12/17 19:21 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/12/17 19:21 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/12/17 19:21 1Tetrachloroethene<0.140
1.00 0.170 ug/L 04/12/17 19:21 1Toluene<0.170
5.00 0.460 ug/L 04/12/17 19:21 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/12/17 19:21 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 04/12/17 19:21 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/12/17 19:21 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/12/17 19:21 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/12/17 19:21 1Trichloroethene<0.200
1.00 0.210 ug/L 04/12/17 19:21 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 04/12/17 19:21 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/12/17 19:21 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/12/17 19:21 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/12/17 19:21 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-125742-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-125742-2Client Sample ID: SW-01 OLD
Matrix: WaterDate Collected: 04/05/17 12:35
Date Received: 04/06/17 09:30
4-Bromofluorobenzene (Surr)87 70-130 04/12/17 19:21 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)94 04/12/17 19:21 170-130
1,2-Dichloroethane-d4 (Surr)84 04/12/17 19:21 170-130
Toluene-d8 (Surr)91 04/12/17 19:21 170-130
Method: 6010D - Metals (ICP)
RL MDL
Silver <0.00300 0.00500 0.00300 mg/L 04/17/17 16:25 04/20/17 01:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00860 mg/L 04/17/17 16:25 04/20/17 01:06 1Arsenic<0.00860
0.0100 0.00500 mg/L 04/17/17 16:25 04/20/17 01:06 1Barium0.0816
0.00100 0.000500 mg/L 04/17/17 16:25 04/20/17 01:06 1Cadmium<0.000500
0.00500 0.00300 mg/L 04/17/17 16:25 04/20/17 01:06 1Chromium<0.00300
0.00500 0.00200 mg/L 04/17/17 16:25 04/20/17 01:06 1Lead<0.00200
0.0100 0.00500 mg/L 04/17/17 16:25 04/20/17 01:06 1Selenium<0.00500
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 04/13/17 07:33 04/13/17 14:13 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-125742-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-125742-3Client Sample ID: SW-02 OLD
Matrix: WaterDate Collected: 04/05/17 13:40
Date Received: 04/06/17 09:30
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 04/12/17 19:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 04/12/17 19:51 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/12/17 19:51 1Benzene<0.200
1.00 0.150 ug/L 04/12/17 19:51 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/12/17 19:51 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/12/17 19:51 1Bromoform<0.290
1.00 0.350 ug/L 04/12/17 19:51 1Bromomethane<0.350
50.0 2.64 ug/L 04/12/17 19:51 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 04/12/17 19:51 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/12/17 19:51 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/12/17 19:51 1Chlorobenzene<0.180
1.00 0.360 ug/L 04/12/17 19:51 1Chloroethane<0.360
1.00 0.230 ug/L 04/12/17 19:51 1Chloroform<0.230
1.00 0.360 ug/L 04/12/17 19:51 1Chloromethane<0.360
1.00 0.210 ug/L 04/12/17 19:51 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 04/12/17 19:51 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/12/17 19:51 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/12/17 19:51 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/12/17 19:51 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 04/12/17 19:51 1Dibromomethane<0.450
1.00 0.190 ug/L 04/12/17 19:51 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 04/12/17 19:51 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 04/12/17 19:51 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 04/12/17 19:51 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 04/12/17 19:51 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/12/17 19:51 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 04/12/17 19:51 1Ethylbenzene<0.190
10.0 1.28 ug/L 04/12/17 19:51 12-Hexanone <1.28
10.0 1.50 ug/L 04/12/17 19:51 1Iodomethane<1.50
5.00 1.00 ug/L 04/12/17 19:51 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/12/17 19:51 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/12/17 19:51 1Styrene<0.280
1.00 0.150 ug/L 04/12/17 19:51 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/12/17 19:51 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/12/17 19:51 1Tetrachloroethene<0.140
1.00 0.170 ug/L 04/12/17 19:51 1Toluene<0.170
5.00 0.460 ug/L 04/12/17 19:51 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/12/17 19:51 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 04/12/17 19:51 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/12/17 19:51 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/12/17 19:51 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/12/17 19:51 1Trichloroethene<0.200
1.00 0.210 ug/L 04/12/17 19:51 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 04/12/17 19:51 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/12/17 19:51 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/12/17 19:51 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/12/17 19:51 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-125742-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-125742-3Client Sample ID: SW-02 OLD
Matrix: WaterDate Collected: 04/05/17 13:40
Date Received: 04/06/17 09:30
4-Bromofluorobenzene (Surr)89 70-130 04/12/17 19:51 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)96 04/12/17 19:51 170-130
1,2-Dichloroethane-d4 (Surr)89 04/12/17 19:51 170-130
Toluene-d8 (Surr)90 04/12/17 19:51 170-130
Method: 6010D - Metals (ICP)
RL MDL
Silver <0.00300 0.00500 0.00300 mg/L 04/17/17 16:25 04/20/17 01:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00860 mg/L 04/17/17 16:25 04/20/17 01:11 1Arsenic<0.00860
0.0100 0.00500 mg/L 04/17/17 16:25 04/20/17 01:11 1Barium0.0589
0.00100 0.000500 mg/L 04/17/17 16:25 04/20/17 01:11 1Cadmium<0.000500
0.00500 0.00300 mg/L 04/17/17 16:25 04/20/17 01:11 1Chromium<0.00300
0.00500 0.00200 mg/L 04/17/17 16:25 04/20/17 01:11 1Lead<0.00200
0.0100 0.00500 mg/L 04/17/17 16:25 04/20/17 01:11 1Selenium<0.00500
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 04/13/17 07:33 04/13/17 14:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-125742-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-125742-4Client Sample ID: DW-01 OLD
Matrix: WaterDate Collected: 04/05/17 13:20
Date Received: 04/06/17 09:30
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 04/12/17 20:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 04/12/17 20:20 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/12/17 20:20 1Benzene<0.200
1.00 0.150 ug/L 04/12/17 20:20 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/12/17 20:20 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/12/17 20:20 1Bromoform<0.290
1.00 0.350 ug/L 04/12/17 20:20 1Bromomethane<0.350
50.0 2.64 ug/L 04/12/17 20:20 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 04/12/17 20:20 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/12/17 20:20 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/12/17 20:20 1Chlorobenzene<0.180
1.00 0.360 ug/L 04/12/17 20:20 1Chloroethane<0.360
1.00 0.230 ug/L 04/12/17 20:20 1Chloroform<0.230
1.00 0.360 ug/L 04/12/17 20:20 1Chloromethane<0.360
1.00 0.210 ug/L 04/12/17 20:20 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 04/12/17 20:20 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/12/17 20:20 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/12/17 20:20 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/12/17 20:20 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 04/12/17 20:20 1Dibromomethane<0.450
1.00 0.190 ug/L 04/12/17 20:20 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 04/12/17 20:20 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 04/12/17 20:20 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 04/12/17 20:20 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 04/12/17 20:20 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/12/17 20:20 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 04/12/17 20:20 1Ethylbenzene<0.190
10.0 1.28 ug/L 04/12/17 20:20 12-Hexanone <1.28
10.0 1.50 ug/L 04/12/17 20:20 1Iodomethane<1.50
5.00 1.00 ug/L 04/12/17 20:20 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/12/17 20:20 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/12/17 20:20 1Styrene<0.280
1.00 0.150 ug/L 04/12/17 20:20 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/12/17 20:20 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/12/17 20:20 1Tetrachloroethene<0.140
1.00 0.170 ug/L 04/12/17 20:20 1Toluene<0.170
5.00 0.460 ug/L 04/12/17 20:20 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/12/17 20:20 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 04/12/17 20:20 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/12/17 20:20 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/12/17 20:20 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/12/17 20:20 1Trichloroethene<0.200
1.00 0.210 ug/L 04/12/17 20:20 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 04/12/17 20:20 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/12/17 20:20 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/12/17 20:20 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/12/17 20:20 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-125742-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-125742-4Client Sample ID: DW-01 OLD
Matrix: WaterDate Collected: 04/05/17 13:20
Date Received: 04/06/17 09:30
4-Bromofluorobenzene (Surr)90 70-130 04/12/17 20:20 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)94 04/12/17 20:20 170-130
1,2-Dichloroethane-d4 (Surr)85 04/12/17 20:20 170-130
Toluene-d8 (Surr)92 04/12/17 20:20 170-130
Method: 6010D - Metals (ICP)
RL MDL
Silver <0.00300 0.00500 0.00300 mg/L 04/17/17 16:25 04/20/17 01:16 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0100 0.00860 mg/L 04/17/17 16:25 04/20/17 01:16 1Arsenic<0.00860
0.0100 0.00500 mg/L 04/17/17 16:25 04/20/17 01:16 1Barium0.171
0.00100 0.000500 mg/L 04/17/17 16:25 04/20/17 01:16 1Cadmium<0.000500
0.00500 0.00300 mg/L 04/17/17 16:25 04/20/17 01:16 1Chromium0.00610
0.00500 0.00200 mg/L 04/17/17 16:25 04/20/17 01:16 1Lead0.00660
0.0100 0.00500 mg/L 04/17/17 16:25 04/20/17 01:16 1Selenium<0.00500
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury <0.100 0.200 0.100 ug/L 04/13/17 07:33 04/13/17 14:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-125742-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-125742-5Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 04/05/17 00:01
Date Received: 04/06/17 09:30
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone <2.66 25.0 2.66 ug/L 04/12/17 13:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 0.500 ug/L 04/12/17 13:56 1Acrylonitrile<0.500
1.00 0.200 ug/L 04/12/17 13:56 1Benzene<0.200
1.00 0.150 ug/L 04/12/17 13:56 1Bromochloromethane<0.150
1.00 0.170 ug/L 04/12/17 13:56 1Bromodichloromethane<0.170
1.00 0.290 ug/L 04/12/17 13:56 1Bromoform<0.290
1.00 0.350 ug/L 04/12/17 13:56 1Bromomethane<0.350
50.0 2.64 ug/L 04/12/17 13:56 12-Butanone (MEK)<2.64
1.00 0.220 ug/L 04/12/17 13:56 1Carbon disulfide <0.220
1.00 0.180 ug/L 04/12/17 13:56 1Carbon tetrachloride <0.180
1.00 0.180 ug/L 04/12/17 13:56 1Chlorobenzene<0.180
1.00 0.360 ug/L 04/12/17 13:56 1Chloroethane<0.360
1.00 0.230 ug/L 04/12/17 13:56 1Chloroform<0.230
1.00 0.360 ug/L 04/12/17 13:56 1Chloromethane<0.360
1.00 0.210 ug/L 04/12/17 13:56 1cis-1,2-Dichloroethene <0.210
1.00 0.170 ug/L 04/12/17 13:56 1cis-1,3-Dichloropropene <0.170
1.00 0.250 ug/L 04/12/17 13:56 1Dibromochloromethane<0.250
10.0 0.940 ug/L 04/12/17 13:56 11,2-Dibromo-3-Chloropropane <0.940
1.00 0.210 ug/L 04/12/17 13:56 11,2-Dibromoethane (EDB)<0.210
1.00 0.450 ug/L 04/12/17 13:56 1Dibromomethane<0.450
1.00 0.190 ug/L 04/12/17 13:56 11,2-Dichlorobenzene <0.190
1.00 0.170 ug/L 04/12/17 13:56 11,4-Dichlorobenzene <0.170
1.00 0.240 ug/L 04/12/17 13:56 11,1-Dichloroethane <0.240
1.00 0.200 ug/L 04/12/17 13:56 11,2-Dichloroethane <0.200
1.00 0.250 ug/L 04/12/17 13:56 11,1-Dichloroethene <0.250
1.00 0.250 ug/L 04/12/17 13:56 11,2-Dichloropropane <0.250
1.00 0.190 ug/L 04/12/17 13:56 1Ethylbenzene<0.190
10.0 1.28 ug/L 04/12/17 13:56 12-Hexanone <1.28
10.0 1.50 ug/L 04/12/17 13:56 1Iodomethane<1.50
5.00 1.00 ug/L 04/12/17 13:56 1Methylene Chloride <1.00
10.0 0.810 ug/L 04/12/17 13:56 14-Methyl-2-pentanone (MIBK)<0.810
1.00 0.280 ug/L 04/12/17 13:56 1Styrene<0.280
1.00 0.150 ug/L 04/12/17 13:56 11,1,1,2-Tetrachloroethane <0.150
1.00 0.190 ug/L 04/12/17 13:56 11,1,2,2-Tetrachloroethane <0.190
1.00 0.140 ug/L 04/12/17 13:56 1Tetrachloroethene<0.140
1.00 0.170 ug/L 04/12/17 13:56 1Toluene<0.170
5.00 0.460 ug/L 04/12/17 13:56 1trans-1,4-Dichloro-2-butene <0.460
1.00 0.230 ug/L 04/12/17 13:56 1trans-1,2-Dichloroethene <0.230
1.00 0.170 ug/L 04/12/17 13:56 1trans-1,3-Dichloropropene <0.170
1.00 0.190 ug/L 04/12/17 13:56 11,1,1-Trichloroethane <0.190
1.00 0.190 ug/L 04/12/17 13:56 11,1,2-Trichloroethane <0.190
1.00 0.200 ug/L 04/12/17 13:56 1Trichloroethene<0.200
1.00 0.210 ug/L 04/12/17 13:56 1Trichlorofluoromethane<0.210
1.00 0.230 ug/L 04/12/17 13:56 11,2,3-Trichloropropane <0.230
10.0 1.71 ug/L 04/12/17 13:56 1Vinyl acetate <1.71
1.00 0.180 ug/L 04/12/17 13:56 1Vinyl chloride <0.180
3.00 0.580 ug/L 04/12/17 13:56 1Xylenes, Total <0.580
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Client Sample Results
TestAmerica Job ID: 490-125742-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison Co Closed Landfill
Lab Sample ID: 490-125742-5Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 04/05/17 00:01
Date Received: 04/06/17 09:30
4-Bromofluorobenzene (Surr)90 70-130 04/12/17 13:56 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)96 04/12/17 13:56 170-130
1,2-Dichloroethane-d4 (Surr)89 04/12/17 13:56 170-130
Toluene-d8 (Surr)92 04/12/17 13:56 170-130
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Page 15 of 33 4/20/2017
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QC Sample Results
TestAmerica Job ID: 490-125742-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison Co Closed Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-421162/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 421627
RL MDL
Acetone <2.66 25.0 2.66 ug/L 04/12/17 15:25 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.500 0.50010.0 ug/L 04/12/17 15:25 1Acrylonitrile
<0.200 0.2001.00 ug/L 04/12/17 15:25 1Benzene
<0.150 0.1501.00 ug/L 04/12/17 15:25 1Bromochloromethane
0.2424 J 0.1701.00 ug/L 04/12/17 15:25 1Bromodichloromethane
<0.290 0.2901.00 ug/L 04/12/17 15:25 1Bromoform
<0.350 0.3501.00 ug/L 04/12/17 15:25 1Bromomethane
<2.64 2.6450.0 ug/L 04/12/17 15:25 12-Butanone (MEK)
<0.220 0.2201.00 ug/L 04/12/17 15:25 1Carbon disulfide
<0.180 0.1801.00 ug/L 04/12/17 15:25 1Carbon tetrachloride
<0.180 0.1801.00 ug/L 04/12/17 15:25 1Chlorobenzene
<0.360 0.3601.00 ug/L 04/12/17 15:25 1Chloroethane
6.014 0.2301.00 ug/L 04/12/17 15:25 1Chloroform
<0.360 0.3601.00 ug/L 04/12/17 15:25 1Chloromethane
<0.210 0.2101.00 ug/L 04/12/17 15:25 1cis-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 04/12/17 15:25 1cis-1,3-Dichloropropene
<0.250 0.2501.00 ug/L 04/12/17 15:25 1Dibromochloromethane
<0.940 0.94010.0 ug/L 04/12/17 15:25 11,2-Dibromo-3-Chloropropane
<0.210 0.2101.00 ug/L 04/12/17 15:25 11,2-Dibromoethane (EDB)
<0.450 0.4501.00 ug/L 04/12/17 15:25 1Dibromomethane
<0.190 0.1901.00 ug/L 04/12/17 15:25 11,2-Dichlorobenzene
<0.170 0.1701.00 ug/L 04/12/17 15:25 11,4-Dichlorobenzene
<0.240 0.2401.00 ug/L 04/12/17 15:25 11,1-Dichloroethane
<0.200 0.2001.00 ug/L 04/12/17 15:25 11,2-Dichloroethane
<0.250 0.2501.00 ug/L 04/12/17 15:25 11,1-Dichloroethene
<0.250 0.2501.00 ug/L 04/12/17 15:25 11,2-Dichloropropane
<0.190 0.1901.00 ug/L 04/12/17 15:25 1Ethylbenzene
<1.28 1.2810.0 ug/L 04/12/17 15:25 12-Hexanone
<1.50 1.5010.0 ug/L 04/12/17 15:25 1Iodomethane
1.010 J 1.005.00 ug/L 04/12/17 15:25 1Methylene Chloride
<0.810 0.81010.0 ug/L 04/12/17 15:25 14-Methyl-2-pentanone (MIBK)
<0.280 0.2801.00 ug/L 04/12/17 15:25 1Styrene
<0.150 0.1501.00 ug/L 04/12/17 15:25 11,1,1,2-Tetrachloroethane
<0.190 0.1901.00 ug/L 04/12/17 15:25 11,1,2,2-Tetrachloroethane
<0.140 0.1401.00 ug/L 04/12/17 15:25 1Tetrachloroethene
<0.170 0.1701.00 ug/L 04/12/17 15:25 1Toluene
<0.460 0.4605.00 ug/L 04/12/17 15:25 1trans-1,4-Dichloro-2-butene
<0.230 0.2301.00 ug/L 04/12/17 15:25 1trans-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 04/12/17 15:25 1trans-1,3-Dichloropropene
<0.190 0.1901.00 ug/L 04/12/17 15:25 11,1,1-Trichloroethane
<0.190 0.1901.00 ug/L 04/12/17 15:25 11,1,2-Trichloroethane
<0.200 0.2001.00 ug/L 04/12/17 15:25 1Trichloroethene
<0.210 0.2101.00 ug/L 04/12/17 15:25 1Trichlorofluoromethane
<0.230 0.2301.00 ug/L 04/12/17 15:25 11,2,3-Trichloropropane
<1.71 1.7110.0 ug/L 04/12/17 15:25 1Vinyl acetate
<0.180 0.1801.00 ug/L 04/12/17 15:25 1Vinyl chloride
<0.580 0.5803.00 ug/L 04/12/17 15:25 1Xylenes, Total
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QC Sample Results
TestAmerica Job ID: 490-125742-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison Co Closed Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-421162/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 421627
4-Bromofluorobenzene (Surr)90 70-130 04/12/17 15:25 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
97 04/12/17 15:25 1Dibromofluoromethane (Surr)70-130
88 04/12/17 15:25 11,2-Dichloroethane-d4 (Surr)70-130
91 04/12/17 15:25 1Toluene-d8 (Surr)70-130
Client Sample ID: Method BlankLab Sample ID: MB 490-421627/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 421627
RL MDL
Acetone <2.66 25.0 2.66 ug/L 04/12/17 13:26 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.500 0.50010.0 ug/L 04/12/17 13:26 1Acrylonitrile
<0.200 0.2001.00 ug/L 04/12/17 13:26 1Benzene
<0.150 0.1501.00 ug/L 04/12/17 13:26 1Bromochloromethane
<0.170 0.1701.00 ug/L 04/12/17 13:26 1Bromodichloromethane
<0.290 0.2901.00 ug/L 04/12/17 13:26 1Bromoform
<0.350 0.3501.00 ug/L 04/12/17 13:26 1Bromomethane
<2.64 2.6450.0 ug/L 04/12/17 13:26 12-Butanone (MEK)
<0.220 0.2201.00 ug/L 04/12/17 13:26 1Carbon disulfide
<0.180 0.1801.00 ug/L 04/12/17 13:26 1Carbon tetrachloride
<0.180 0.1801.00 ug/L 04/12/17 13:26 1Chlorobenzene
<0.360 0.3601.00 ug/L 04/12/17 13:26 1Chloroethane
<0.230 0.2301.00 ug/L 04/12/17 13:26 1Chloroform
<0.360 0.3601.00 ug/L 04/12/17 13:26 1Chloromethane
<0.210 0.2101.00 ug/L 04/12/17 13:26 1cis-1,2-Dichloroethene
<0.170 0.1701.00 ug/L 04/12/17 13:26 1cis-1,3-Dichloropropene
<0.250 0.2501.00 ug/L 04/12/17 13:26 1Dibromochloromethane
<0.940 0.94010.0 ug/L 04/12/17 13:26 11,2-Dibromo-3-Chloropropane
<0.210 0.2101.00 ug/L 04/12/17 13:26 11,2-Dibromoethane (EDB)
<0.450 0.4501.00 ug/L 04/12/17 13:26 1Dibromomethane
<0.190 0.1901.00 ug/L 04/12/17 13:26 11,2-Dichlorobenzene
<0.170 0.1701.00 ug/L 04/12/17 13:26 11,4-Dichlorobenzene
<0.240 0.2401.00 ug/L 04/12/17 13:26 11,1-Dichloroethane
<0.200 0.2001.00 ug/L 04/12/17 13:26 11,2-Dichloroethane
<0.250 0.2501.00 ug/L 04/12/17 13:26 11,1-Dichloroethene
<0.250 0.2501.00 ug/L 04/12/17 13:26 11,2-Dichloropropane
<0.190 0.1901.00 ug/L 04/12/17 13:26 1Ethylbenzene
<1.28 1.2810.0 ug/L 04/12/17 13:26 12-Hexanone
<1.50 1.5010.0 ug/L 04/12/17 13:26 1Iodomethane
<1.00 1.005.00 ug/L 04/12/17 13:26 1Methylene Chloride
<0.810 0.81010.0 ug/L 04/12/17 13:26 14-Methyl-2-pentanone (MIBK)
<0.280 0.2801.00 ug/L 04/12/17 13:26 1Styrene
<0.150 0.1501.00 ug/L 04/12/17 13:26 11,1,1,2-Tetrachloroethane
<0.190 0.1901.00 ug/L 04/12/17 13:26 11,1,2,2-Tetrachloroethane
<0.140 0.1401.00 ug/L 04/12/17 13:26 1Tetrachloroethene
<0.170 0.1701.00 ug/L 04/12/17 13:26 1Toluene
<0.460 0.4605.00 ug/L 04/12/17 13:26 1trans-1,4-Dichloro-2-butene
<0.230 0.2301.00 ug/L 04/12/17 13:26 1trans-1,2-Dichloroethene
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QC Sample Results
TestAmerica Job ID: 490-125742-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison Co Closed Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-421627/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 421627
RL MDL
trans-1,3-Dichloropropene <0.170 1.00 0.170 ug/L 04/12/17 13:26 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.190 0.1901.00 ug/L 04/12/17 13:26 11,1,1-Trichloroethane
<0.190 0.1901.00 ug/L 04/12/17 13:26 11,1,2-Trichloroethane
<0.200 0.2001.00 ug/L 04/12/17 13:26 1Trichloroethene
<0.210 0.2101.00 ug/L 04/12/17 13:26 1Trichlorofluoromethane
<0.230 0.2301.00 ug/L 04/12/17 13:26 11,2,3-Trichloropropane
<1.71 1.7110.0 ug/L 04/12/17 13:26 1Vinyl acetate
<0.180 0.1801.00 ug/L 04/12/17 13:26 1Vinyl chloride
<0.580 0.5803.00 ug/L 04/12/17 13:26 1Xylenes, Total
4-Bromofluorobenzene (Surr)88 70-130 04/12/17 13:26 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
96 04/12/17 13:26 1Dibromofluoromethane (Surr)70-130
89 04/12/17 13:26 11,2-Dichloroethane-d4 (Surr)70-130
100 04/12/17 13:26 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-421627/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 421627
Acetone 100 99.68 ug/L 100 39-150
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Acrylonitrile 200 189.9 ug/L 95 63-135
Benzene 20.0 19.89 ug/L 99 70-130
Bromochloromethane 20.0 22.61 ug/L 113 70-130
Bromodichloromethane 20.0 20.64 ug/L 103 70-130
Bromoform 20.0 21.44 ug/L 107 70-137
Bromomethane 20.0 22.90 ug/L 115 53-150
2-Butanone (MEK)100 99.17 ug/L 99 55-143
Carbon disulfide 20.0 20.22 ug/L 101 64-135
Carbon tetrachloride 20.0 20.07 ug/L 100 70-147
Chlorobenzene 20.0 18.34 ug/L 92 70-130
Chloroethane 20.0 23.04 ug/L 115 60-138
Chloroform 20.0 18.43 ug/L 92 70-130
Chloromethane 20.0 19.73 ug/L 99 33-150
cis-1,2-Dichloroethene 20.0 19.26 ug/L 96 70-130
cis-1,3-Dichloropropene 20.0 19.23 ug/L 96 70-133
Dibromochloromethane 20.0 19.97 ug/L 100 70-133
1,2-Dibromo-3-Chloropropane 20.0 18.46 ug/L 92 45-138
1,2-Dibromoethane (EDB)20.0 18.81 ug/L 94 70-130
Dibromomethane 20.0 21.72 ug/L 109 70-130
1,2-Dichlorobenzene 20.0 19.17 ug/L 96 70-130
1,4-Dichlorobenzene 20.0 19.40 ug/L 97 70-130
1,1-Dichloroethane 20.0 18.92 ug/L 95 70-130
1,2-Dichloroethane 20.0 19.61 ug/L 98 70-130
1,1-Dichloroethene 20.0 19.22 ug/L 96 70-132
1,2-Dichloropropane 20.0 19.27 ug/L 96 70-130
Ethylbenzene 20.0 17.94 ug/L 90 70-130
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QC Sample Results
TestAmerica Job ID: 490-125742-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison Co Closed Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-421627/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 421627
2-Hexanone 100 77.11 ug/L 77 54-142
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Iodomethane 20.0 24.96 ug/L 125 40-150
Methylene Chloride 20.0 21.99 ug/L 110 70-130
4-Methyl-2-pentanone (MIBK)100 91.43 ug/L 91 60-137
Styrene 20.0 18.51 ug/L 93 70-130
1,1,1,2-Tetrachloroethane 20.0 19.78 ug/L 99 70-130
1,1,2,2-Tetrachloroethane 20.0 18.45 ug/L 92 69-131
Tetrachloroethene 20.0 18.85 ug/L 94 70-130
Toluene 20.0 18.22 ug/L 91 70-130
trans-1,4-Dichloro-2-butene 20.0 17.62 ug/L 88 41-150
trans-1,2-Dichloroethene 20.0 18.50 ug/L 92 70-130
trans-1,3-Dichloropropene 20.0 18.05 ug/L 90 63-142
1,1,1-Trichloroethane 20.0 19.71 ug/L 99 70-135
1,1,2-Trichloroethane 20.0 18.35 ug/L 92 70-130
Trichloroethene 20.0 19.62 ug/L 98 70-130
Trichlorofluoromethane 20.0 23.89 ug/L 119 59-150
1,2,3-Trichloropropane 20.0 19.23 ug/L 96 70-131
Vinyl acetate 40.0 47.20 ug/L 118 54-146
Vinyl chloride 20.0 22.97 ug/L 115 57-137
Xylenes, Total 40.0 36.42 ug/L 91 70-132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
89
LCS LCS
Qualifier Limits%Recovery
100Dibromofluoromethane (Surr)70 -130
911,2-Dichloroethane-d4 (Surr)70 -130
90Toluene-d8 (Surr)70 -130
Client Sample ID: BG Spring OLDLab Sample ID: 490-125742-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 421627
Acetone <2.66 100 103.3 ug/L 103 39-150
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acrylonitrile <0.500 200 215.9 ug/L 108 50-135
Benzene <0.200 20.0 22.46 ug/L 112 55-147
Bromochloromethane <0.150 20.0 25.00 ug/L 125 59-132
Bromodichloromethane <0.170 20.0 23.30 ug/L 117 70-140
Bromoform <0.290 20.0 22.65 ug/L 113 53-150
Bromomethane <0.350 20.0 23.60 ug/L 118 30-150
2-Butanone (MEK)<2.64 100 115.2 ug/L 115 50-143
Carbon disulfide <0.220 20.0 22.66 ug/L 113 35-150
Carbon tetrachloride <0.180 20.0 23.90 ug/L 120 56-150
Chlorobenzene <0.180 20.0 21.21 ug/L 106 70-130
Chloroethane <0.360 20.0 23.79 ug/L 119 58-141
Chloroform <0.230 20.0 22.27 ug/L 111 66-138
Chloromethane <0.360 20.0 20.86 ug/L 104 10-150
cis-1,2-Dichloroethene <0.210 20.0 22.37 ug/L 112 68-131
cis-1,3-Dichloropropene <0.170 20.0 21.41 ug/L 107 70-133
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QC Sample Results
TestAmerica Job ID: 490-125742-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison Co Closed Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: BG Spring OLDLab Sample ID: 490-125742-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 421627
Dibromochloromethane <0.250 20.0 22.05 ug/L 110 66-140
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
1,2-Dibromo-3-Chloropropane <0.940 20.0 19.12 ug/L 96 38-138
1,2-Dibromoethane (EDB)<0.210 20.0 20.49 ug/L 102 65-137
Dibromomethane <0.450 20.0 23.76 ug/L 119 70-130
1,2-Dichlorobenzene <0.190 20.0 20.29 ug/L 101 70-130
1,4-Dichlorobenzene <0.170 20.0 20.66 ug/L 103 70-130
1,1-Dichloroethane <0.240 20.0 22.06 ug/L 110 61-139
1,2-Dichloroethane <0.200 20.0 21.72 ug/L 109 64-136
1,1-Dichloroethene <0.250 20.0 23.87 ug/L 119 54-150
1,2-Dichloropropane <0.250 20.0 21.80 ug/L 109 67-130
Ethylbenzene <0.190 20.0 19.64 ug/L 98 65-139
2-Hexanone <1.28 100 82.01 ug/L 82 44-150
Iodomethane <1.50 20.0 26.14 ug/L 131 34-150
Methylene Chloride <1.00 20.0 23.28 ug/L 116 64-130
4-Methyl-2-pentanone (MIBK)<0.810 100 97.98 ug/L 98 50-140
Styrene <0.280 20.0 20.56 ug/L 103 70-130
1,1,1,2-Tetrachloroethane <0.150 20.0 21.98 ug/L 110 70-131
1,1,2,2-Tetrachloroethane <0.190 20.0 19.89 ug/L 99 56-145
Tetrachloroethene <0.140 20.0 21.13 ug/L 106 57-138
Toluene <0.170 20.0 21.56 ug/L 108 64-136
trans-1,4-Dichloro-2-butene <0.460 20.0 17.76 ug/L 89 39-150
trans-1,2-Dichloroethene <0.230 20.0 21.91 ug/L 110 59-143
trans-1,3-Dichloropropene <0.170 20.0 18.60 ug/L 93 63-142
1,1,1-Trichloroethane <0.190 20.0 23.45 ug/L 117 68-144
1,1,2-Trichloroethane <0.190 20.0 20.58 ug/L 103 70-130
Trichloroethene <0.200 20.0 22.83 ug/L 114 63-135
Trichlorofluoromethane <0.210 20.0 26.55 ug/L 133 44-150
1,2,3-Trichloropropane <0.230 20.0 21.25 ug/L 106 65-131
Vinyl acetate <1.71 40.0 45.81 ug/L 115 43-146
Vinyl chloride <0.180 20.0 23.42 ug/L 117 57-150
Xylenes, Total <0.580 40.0 38.55 ug/L 96 69-132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
86
MS MS
Qualifier Limits%Recovery
99Dibromofluoromethane (Surr)70 -130
891,2-Dichloroethane-d4 (Surr)70 -130
92Toluene-d8 (Surr)70 -130
Client Sample ID: BG Spring OLDLab Sample ID: 490-125742-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 421627
Acetone <2.66 100 122.4 ug/L 122 39-150 17 28
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acrylonitrile <0.500 200 224.9 ug/L 112 50-135 4 23
Benzene <0.200 20.0 23.90 ug/L 120 55-147 6 22
Bromochloromethane <0.150 20.0 26.33 ug/L 132 59-132 5 21
Bromodichloromethane <0.170 20.0 24.75 ug/L 124 70-140 6 196
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QC Sample Results
TestAmerica Job ID: 490-125742-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison Co Closed Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: BG Spring OLDLab Sample ID: 490-125742-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 421627
Bromoform <0.290 20.0 23.92 ug/L 120 53-150 5 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Bromomethane <0.350 20.0 26.42 ug/L 132 30-150 11 44
2-Butanone (MEK)<2.64 100 115.6 ug/L 116 50-143 0 28
Carbon disulfide <0.220 20.0 24.11 ug/L 121 35-150 6 34
Carbon tetrachloride <0.180 20.0 25.14 ug/L 126 56-150 5 18
Chlorobenzene <0.180 20.0 22.28 ug/L 111 70-130 5 15
Chloroethane <0.360 20.0 26.57 ug/L 133 58-141 11 31
Chloroform <0.230 20.0 23.47 ug/L 117 66-138 5 21
Chloromethane <0.360 20.0 22.84 ug/L 114 10-150 9 43
cis-1,2-Dichloroethene <0.210 20.0 23.91 ug/L 120 68-131 7 21
cis-1,3-Dichloropropene <0.170 20.0 22.96 ug/L 115 70-133 7 19
Dibromochloromethane <0.250 20.0 23.32 ug/L 117 66-140 6 19
1,2-Dibromo-3-Chloropropane <0.940 20.0 19.11 ug/L 96 38-138 0 26
1,2-Dibromoethane (EDB)<0.210 20.0 21.58 ug/L 108 65-137 5 21
Dibromomethane <0.450 20.0 24.80 ug/L 124 70-130 4 19
1,2-Dichlorobenzene <0.190 20.0 20.47 ug/L 102 70-130 1 15
1,4-Dichlorobenzene <0.170 20.0 20.17 ug/L 101 70-130 2 14
1,1-Dichloroethane <0.240 20.0 24.06 ug/L 120 61-139 9 23
1,2-Dichloroethane <0.200 20.0 23.22 ug/L 116 64-136 7 22
1,1-Dichloroethene <0.250 20.0 26.08 ug/L 130 54-150 9 24
1,2-Dichloropropane <0.250 20.0 23.09 ug/L 115 67-130 6 19
Ethylbenzene <0.190 20.0 20.74 ug/L 104 65-139 5 18
2-Hexanone <1.28 100 88.21 ug/L 88 44-150 7 21
Iodomethane <1.50 20.0 28.91 ug/L 145 34-150 10 37
Methylene Chloride <1.00 20.0 24.86 ug/L 124 64-130 7 22
4-Methyl-2-pentanone (MIBK)<0.810 100 104.8 ug/L 105 50-140 7 24
Styrene <0.280 20.0 21.36 ug/L 107 70-130 4 16
1,1,1,2-Tetrachloroethane <0.150 20.0 23.48 ug/L 117 70-131 7 16
1,1,2,2-Tetrachloroethane <0.190 20.0 20.65 ug/L 103 56-145 4 19
Tetrachloroethene <0.140 20.0 20.92 ug/L 105 57-138 1 17
Toluene <0.170 20.0 23.26 ug/L 116 64-136 8 18
trans-1,4-Dichloro-2-butene <0.460 20.0 18.23 ug/L 91 39-150 3 28
trans-1,2-Dichloroethene <0.230 20.0 23.13 ug/L 116 59-143 5 25
trans-1,3-Dichloropropene <0.170 20.0 20.66 ug/L 103 63-142 11 18
1,1,1-Trichloroethane <0.190 20.0 24.92 ug/L 125 68-144 6 17
1,1,2-Trichloroethane <0.190 20.0 21.77 ug/L 109 70-130 6 18
Trichloroethene <0.200 20.0 23.92 ug/L 120 63-135 5 17
Trichlorofluoromethane <0.210 20.0 27.56 ug/L 138 44-150 4 32
1,2,3-Trichloropropane <0.230 20.0 22.08 ug/L 110 65-131 4 19
Vinyl acetate <1.71 40.0 50.53 ug/L 126 43-146 10 20
Vinyl chloride <0.180 20.0 26.32 ug/L 132 57-150 12 37
Xylenes, Total <0.580 40.0 40.63 ug/L 102 69-132 5 17
4-Bromofluorobenzene (Surr)70 -130
Surrogate
89
MSD MSD
Qualifier Limits%Recovery
97Dibromofluoromethane (Surr)70 -130
931,2-Dichloroethane-d4 (Surr)70 -130
95Toluene-d8 (Surr)70 -130
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QC Sample Results
TestAmerica Job ID: 490-125742-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison Co Closed Landfill
Method: 6010D - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 490-422808/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 423523 Prep Batch: 422808
RL MDL
Silver <0.00300 0.00500 0.00300 mg/L 04/17/17 16:25 04/19/17 22:51 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.00860 0.008600.0100 mg/L 04/17/17 16:25 04/19/17 22:51 1Arsenic
<0.00500 0.005000.0100 mg/L 04/17/17 16:25 04/19/17 22:51 1Barium
<0.000500 0.0005000.00100 mg/L 04/17/17 16:25 04/19/17 22:51 1Cadmium
<0.00300 0.003000.00500 mg/L 04/17/17 16:25 04/19/17 22:51 1Chromium
<0.00200 0.002000.00500 mg/L 04/17/17 16:25 04/19/17 22:51 1Lead
<0.00500 0.005000.0100 mg/L 04/17/17 16:25 04/19/17 22:51 1Selenium
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-422808/22-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 423523 Prep Batch: 422808
Silver 0.0500 0.05480 mg/L 110 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-422808/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 423523 Prep Batch: 422808
Arsenic 0.100 0.09820 mg/L 98 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Barium 0.100 0.1015 mg/L 102 80-120
Cadmium 0.100 0.1019 mg/L 102 80-120
Chromium 0.100 0.1010 mg/L 101 80-120
Lead 0.100 0.1040 mg/L 104 80-120
Selenium 0.100 0.09730 mg/L 97 80-120
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-422808/23-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 423523 Prep Batch: 422808
Silver 0.0500 0.05410 mg/L 108 80-120 1 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-422808/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 423523 Prep Batch: 422808
Arsenic 0.100 0.09900 mg/L 99 80-120 1 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Barium 0.100 0.1053 mg/L 105 80-120 4 20
Cadmium 0.100 0.1035 mg/L 104 80-120 2 20
Chromium 0.100 0.1029 mg/L 103 80-120 2 20
Lead 0.100 0.1070 mg/L 107 80-120 3 20
Selenium 0.100 0.09980 mg/L 100 80-120 3 20
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-125742-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison Co Closed Landfill
Method: 6010D - Metals (ICP) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-125629-D-1-C MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 423523 Prep Batch: 422808
Silver <0.00300 F1 0.100 0.06260 F1 mg/L 63 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Arsenic <0.00860 0.100 0.1015 mg/L 102 75-125
Barium 0.103 0.100 0.2058 mg/L 103 75-125
Cadmium <0.000500 0.100 0.1031 mg/L 103 75-125
Chromium <0.00300 0.100 0.1048 mg/L 105 75-125
Lead <0.00200 0.100 0.1044 mg/L 104 75-125
Selenium <0.00500 0.100 0.09800 mg/L 98 75-125
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-125629-D-1-D MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 423523 Prep Batch: 422808
Silver <0.00300 F1 0.100 0.06070 F1 mg/L 61 75-125 3 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Arsenic <0.00860 0.100 0.09950 mg/L 100 75-125 2 20
Barium 0.103 0.100 0.2060 mg/L 103 75-125 0 20
Cadmium <0.000500 0.100 0.1032 mg/L 103 75-125 0 20
Chromium <0.00300 0.100 0.1029 mg/L 103 75-125 2 20
Lead <0.00200 0.100 0.1049 mg/L 105 75-125 0 20
Selenium <0.00500 0.100 0.09800 mg/L 98 75-125 0 20
Method: 7470A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 490-421871/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 422047 Prep Batch: 421871
RL MDL
Mercury 0.1001 J 0.200 0.100 ug/L 04/13/17 07:33 04/13/17 13:02 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-421871/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 422047 Prep Batch: 421871
Mercury 1.00 1.085 ug/L 109 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-421871/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 422047 Prep Batch: 421871
Mercury 1.00 1.033 ug/L 103 80-120 5 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-125742-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison Co Closed Landfill
Method: 7470A - Mercury (CVAA) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 460-131124-B-2-C MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 422047 Prep Batch: 421871
Mercury <0.100 1.00 1.228 ug/L 123 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 460-131124-B-2-D MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 422047 Prep Batch: 421871
Mercury <0.100 1.00 1.180 ug/L 118 75-125 4 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
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QC Association Summary
TestAmerica Job ID: 490-125742-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison Co Closed Landfill
GC/MS VOA
Leach Batch: 421162
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 1311MB 490-421162/1-A Method Blank Total/NA
Analysis Batch: 421627
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B490-125742-1 BG Spring OLD Total/NA
Water 8260B490-125742-2 SW-01 OLD Total/NA
Water 8260B490-125742-3 SW-02 OLD Total/NA
Water 8260B490-125742-4 DW-01 OLD Total/NA
Water 8260B490-125742-5 Trip Blank Total/NA
Water 8260B 421162MB 490-421162/1-A Method Blank Total/NA
Water 8260BMB 490-421627/6 Method Blank Total/NA
Water 8260BLCS 490-421627/3 Lab Control Sample Total/NA
Water 8260B490-125742-1 MS BG Spring OLD Total/NA
Water 8260B490-125742-1 MSD BG Spring OLD Total/NA
Metals
Prep Batch: 421871
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A490-125742-1 BG Spring OLD Total/NA
Water 7470A490-125742-2 SW-01 OLD Total/NA
Water 7470A490-125742-3 SW-02 OLD Total/NA
Water 7470A490-125742-4 DW-01 OLD Total/NA
Water 7470AMB 490-421871/1-A Method Blank Total/NA
Water 7470ALCS 490-421871/2-A Lab Control Sample Total/NA
Water 7470ALCSD 490-421871/3-A Lab Control Sample Dup Total/NA
Water 7470A460-131124-B-2-C MS Matrix Spike Total/NA
Water 7470A460-131124-B-2-D MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 422047
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 421871490-125742-1 BG Spring OLD Total/NA
Water 7470A 421871490-125742-2 SW-01 OLD Total/NA
Water 7470A 421871490-125742-3 SW-02 OLD Total/NA
Water 7470A 421871490-125742-4 DW-01 OLD Total/NA
Water 7470A 421871MB 490-421871/1-A Method Blank Total/NA
Water 7470A 421871LCS 490-421871/2-A Lab Control Sample Total/NA
Water 7470A 421871LCSD 490-421871/3-A Lab Control Sample Dup Total/NA
Water 7470A 421871460-131124-B-2-C MS Matrix Spike Total/NA
Water 7470A 421871460-131124-B-2-D MSD Matrix Spike Duplicate Total/NA
Prep Batch: 422808
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-125742-1 BG Spring OLD Total/NA
Water 3010A490-125742-2 SW-01 OLD Total/NA
Water 3010A490-125742-3 SW-02 OLD Total/NA
Water 3010A490-125742-4 DW-01 OLD Total/NA
Water 3010AMB 490-422808/1-A Method Blank Total/NA
Water 3010ALCS 490-422808/22-A Lab Control Sample Total/NA
Water 3010ALCS 490-422808/2-A Lab Control Sample Total/NA
TestAmerica Nashville
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QC Association Summary
TestAmerica Job ID: 490-125742-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison Co Closed Landfill
Metals (Continued)
Prep Batch: 422808 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010ALCSD 490-422808/23-A Lab Control Sample Dup Total/NA
Water 3010ALCSD 490-422808/3-A Lab Control Sample Dup Total/NA
Water 3010A490-125629-D-1-C MS Matrix Spike Total/NA
Water 3010A490-125629-D-1-D MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 423523
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010D 422808490-125742-1 BG Spring OLD Total/NA
Water 6010D 422808490-125742-2 SW-01 OLD Total/NA
Water 6010D 422808490-125742-3 SW-02 OLD Total/NA
Water 6010D 422808490-125742-4 DW-01 OLD Total/NA
Water 6010D 422808MB 490-422808/1-A Method Blank Total/NA
Water 6010D 422808LCS 490-422808/22-A Lab Control Sample Total/NA
Water 6010D 422808LCS 490-422808/2-A Lab Control Sample Total/NA
Water 6010D 422808LCSD 490-422808/23-A Lab Control Sample Dup Total/NA
Water 6010D 422808LCSD 490-422808/3-A Lab Control Sample Dup Total/NA
Water 6010D 422808490-125629-D-1-C MS Matrix Spike Total/NA
Water 6010D 422808490-125629-D-1-D MSD Matrix Spike Duplicate Total/NA
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Lab Chronicle
Client: Anchor QEA of North Carolina PLLC TestAmerica Job ID: 490-125742-1
Project/Site: Madison Co Closed Landfill
Client Sample ID: BG Spring OLD Lab Sample ID: 490-125742-1
Matrix: WaterDate Collected: 04/05/17 14:10
Date Received: 04/06/17 09:30
Analysis 8260B JRV04/12/17 14:251 TAL NSH421627
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 422808 04/17/17 16:25 JSF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 423523 04/20/17 01:01 LCS TAL NSHTotal/NA
Prep 7470A 421871 04/13/17 07:33 CAH TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 422047 04/13/17 14:10 CAH TAL NSHTotal/NA
Client Sample ID: SW-01 OLD Lab Sample ID: 490-125742-2
Matrix: WaterDate Collected: 04/05/17 12:35
Date Received: 04/06/17 09:30
Analysis 8260B JRV04/12/17 19:211 TAL NSH421627
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 422808 04/17/17 16:25 JSF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 423523 04/20/17 01:06 LCS TAL NSHTotal/NA
Prep 7470A 421871 04/13/17 07:33 CAH TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 422047 04/13/17 14:13 CAH TAL NSHTotal/NA
Client Sample ID: SW-02 OLD Lab Sample ID: 490-125742-3
Matrix: WaterDate Collected: 04/05/17 13:40
Date Received: 04/06/17 09:30
Analysis 8260B JRV04/12/17 19:511 TAL NSH421627
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 422808 04/17/17 16:25 JSF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 423523 04/20/17 01:11 LCS TAL NSHTotal/NA
Prep 7470A 421871 04/13/17 07:33 CAH TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 422047 04/13/17 14:21 CAH TAL NSHTotal/NA
Client Sample ID: DW-01 OLD Lab Sample ID: 490-125742-4
Matrix: WaterDate Collected: 04/05/17 13:20
Date Received: 04/06/17 09:30
Analysis 8260B JRV04/12/17 20:201 TAL NSH421627
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Prep 3010A 422808 04/17/17 16:25 JSF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6010D 1 423523 04/20/17 01:16 LCS TAL NSHTotal/NA
Prep 7470A 421871 04/13/17 07:33 CAH TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 422047 04/13/17 14:24 CAH TAL NSHTotal/NA
TestAmerica Nashville
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Lab Chronicle
Client: Anchor QEA of North Carolina PLLC TestAmerica Job ID: 490-125742-1
Project/Site: Madison Co Closed Landfill
Client Sample ID: Trip Blank Lab Sample ID: 490-125742-5
Matrix: WaterDate Collected: 04/05/17 00:01
Date Received: 04/06/17 09:30
Analysis 8260B JRV04/12/17 13:561 TAL NSH421627
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10 mL 10 mL
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
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Method Summary
TestAmerica Job ID: 490-125742-1Client: Anchor QEA of North Carolina PLLC
Project/Site: Madison Co Closed Landfill
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL NSH
SW8466010DMetals (ICP)TAL NSH
SW8467470AMercury (CVAA)TAL NSH
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
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Accreditation/Certification Summary
Client: Anchor QEA of North Carolina PLLC TestAmerica Job ID: 490-125742-1
Project/Site: Madison Co Closed Landfill
Laboratory: TestAmerica Nashville
The accreditations/certifications listed below are applicable to this report.
Authority Program EPA Region Identification Number Expiration Date
North Carolina (WW/SW)3874State Program 12-31-17
TestAmerica Nashville
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Login Sample Receipt Checklist
Client: Anchor QEA of North Carolina PLLC Job Number: 490-125742-1
Login Number: 125742
Question Answer Comment
Creator: Ngo, Phiet
List Source: TestAmerica Nashville
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Nashville
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