8602_SurryCountyMtAiry_MSWLF_MtAiry_20170817

Surry County Closed C&D and Closed MSWLF, Mt. Airy
Mt. Airy, North Carolina
December 2016
Permit Number: 86-02
Semi-Annual Water Quality Monitoring Report
Prepared for
Municipal Engineering Services Company, P.A.Garner and Boone, North Carolina
MESCO Project Number: G17024.0
P.O. Box 97
Garner, NC 27529
License No. C-0281

with Corrective Action Update
TABLE OF CONTENTS
SECTION
Introduction Page 1
Background Page 1
Sampling Procedures Page 2
Field Parameter Data Page 2
Laboratory Results Page 3
Quality Control Samples Page 3
Groundwater Samples Page 3
Surface Water Samples Page 4
Corrective Action Update Page 4
MNA Analysis (AOCs Northern, Southern and MW-11) Page 4
Enhanced Bioremediation via Substrate Injection (AOC Southern and Northern) Page 5
MW-11 AOC Investigations Page 5
Groundwater and Surface Water Characterization Page 6
Findings Page 6
Closing Page 7
SHEETS
Topographic Map with Site Location Sheet 1
Single Event Potentiometric Map of Uppermost Aquifer Sheet 2
FIGURES
Total VOC Concentrations Pre/Post Injection Comparison Figure 1
Bromide Tracer Concentrations Time Series Graph and Table Figure 2
Total Cumulative VOC Concentrations Time Series Graphs/Table Figure 3
TABLES
Groundwater Monitoring Well Construction Table Table 1
Field Observations of Monitoring Locations Table 2
Field Parameter Data Summary Table 3
Sampling and Analysis Summary Table 4
Detections Above SWSL, GWP, 2L, 2B or MCL (Appendix 1) Table 5
Hydrologic Properties at Monitoring Well Locations Table 6
APPENDICIES
Laboratory Analysis Report and Chains of Custody Appendix A
Field Sampling Parameter Data Sheet(s) Appendix B
August 17, 2017
Ms. Jaclynne Drummond
Solid Waste Section (SWS)
2090 US 70 Highway
Swannanoa, NC 28778
Re: Semi-Annual Water Quality Monitoring Report with Corrective Action Update
Surry County Closed C&D and Closed MSWLF, Mount Airy
Permit No. 86-02
MESCO Project No. G16025.0
Event Date(s): December 1-3, 2016
Dear Ms. Drummond:
Introduction
On behalf of Surry County, Municipal Engineering Services Company, P.A. (MESCO) is pleased to present this Semi-Annual
Water Quality Report with Corrective Action Update for the fall 2016 event performed at the Surry County closed
construction and demolition (C&D) and closed municipal solid waste landfill (MSWLF)-Mount Airy. NCDENR Solid
Waste Rules 15A NCAC 13B.1632 requires that Surry County provide this report to the NC Solid Waste Section (SWS) on a
semi-annual basis. This report documents the quality of the ground and surface waters during this monitoring event
performed on December 1-3, 2016. Laboratory analytical results indicate volatile organic compounds (VOCs) in
concentrations in excess of SWSL and 2L Standards continue to persist in samples collected from three wells that monitor
the uppermost aquifer. The surface water samples collected from the local discharge feature remain unimpacted. Corrective
action to remediate VOCs in groundwater is ongoing within all three areas of concern (AOC) as defined in the Corrective
Action Plan (CAP) as Northern, Southern and MW-11 and conditions continue to improve with updated information
presented herein.
Background
The Surry County closed C&D and MSWLF, permit #86-02, is located at 237 Landfill Road in Mt. Airy North Carolina. The
site location topographic map is depicted in the attached Sheet 1. Prior to becoming a C&D landfill the site operated as a
MSW unlined sanitary landfill that consisted of two units. The northern unit was closed prior to October 1991. The southern
unit is comprised of two contiguous portions. The first part stopped receiving waste prior to October 1991 and the second
part stopped receiving waste prior to January 1, 1999. Both portions of the southern unit were properly closed with a low
permeability cohesive cap per the Transition Plan. The top portion of the southern unit served as an exclusive C&D landfill
until prior to June 1, 2008 at which time it was properly closed with another cohesive cap in accordance with the Closure
Plan. For continuity, both the northern and the southern units are monitored and reported together.
Water quality at this facility has been monitored at least semi-annually since 1989 with historical data available since 1994.
1

This event was performed in accordance with the NC SWS rules/regulations as promulgated in 15A NCAC 13B and as a
condition of the post-closure portion of the permit to operate.memorandums this report contains sampling procedures, field
and laboratory results, groundwater and surface water characterization, and findings. This report also contains a table of
detections compared to Standards, field data results table, groundwater flow directions/rates table, field observations of the
monitoring network table, a potentiometric map of the uppermost aquifer, histograms of historical detections, statistical
trend analysis, laboratory analytical reports with chains-of-custody (C-O-C) and quality assurance/quality control data.
Sampling Procedures
The water quality monitoring program, current as of this event date, includes sampling locations and parameters as outlined
in the Water Quality Sampling and Analysis Plan (SAP) (DIN:18936) dated April 30, 2013 and approved by the SWS (DIN:
18938) on May 10, 2013. Monitoring locations are shown on the enclosed potentiometric map (Sheet 2). MESCO
personnel collected water samples from 20 downgradient groundwater monitoring wells (MW-3R, MW-4, MW-6 through
MW-11, MW-12S, MW-12D, MW-13 through MW-23), one background well (MW-1), four surface water locations (SW-1,
SW-2, SW-3 and SW-4), and the water supply well (SCALEHOUSE) that serves the facility. Data from two surface water
points (SWN-1 and SWN-2) designated in the SAP for the adjacent Subtitle D Lined MSWLF are presented because this
local discharge feature is shared by both permits. Quality control measures implemented during this event included the
quantification of potential artifact contaminants via equipment (EB), field (FB) and travel (TB) blanks. Samples were not
analyzed from the six injection wells (IW-1), (IW-2/MW-2), (IW-3/MW-3RS), (IW-4/MW-4), (IW-5/MW-5) and (IW-6/MW-
8) since they are exempt due to the presence of injectant residue which would yield unrepresentative water quality results.
A summary of the construction of the water monitoring wells is presented on Table 1. The function and integrity of all
monitoring locations were visually evaluated and no deficiencies identified as documented on Table 2. The depth to water in
each well was electronically gaged prior to purging to quantify the static water level elevation. Low-flow pumping
methodology or bailing was utilized to adequately purge the wells to a minimum of three times the volume of standing water
in the well or until dry. Surface water samples were collected from Stoney Creek discharge feature at previously designated
locations. During well purging and surface water sample collection the required field parameters were recorded. The
samples were then placed into laboratory-prepared, pre-preserved containers via a new disposable polyethylene bailer.
Samples were collected, kept on ice, and transported to a NC-certified laboratory under proper C-O-C protocols within the
specified hold times for each analysis.
Field Parameter Data
Stabilized field parameters were recorded during purging which included depth to water, pH, dissolved oxygen (DO),
temperature, oxidation reduction potential (ORP), specific conductance and turbidity. The field parameter data indicates the
monitored groundwater is slightly acidic, reducing conditions, with relatively low specific conductance which is generally
consistent relative to each other and congruent with data historically reported. Field parameter data recorded at the surface
water locations were neutral in regard to pH and low specific conductance which is consistent with uncontaminated water. A
summary of the field parameter data is presented in Table 3 and the field sampling data sheet is enclosed in Appendix B.
2
Laboratory Results
Pace Analytical Laboratory (PACE) of Huntersville and Asheville, NC performed the laboratory analysis of groundwater and
surface water samples for the total recoverable constituents listed in 40 CFR Appendix I. Pace and Microseeps analyzed
samples collected from seven wells for monitored natural attenuation (MNA) parameters. Additionally, Pace reported
bromide levels in a sample collected from MW-16 to assess migration of the tracer previously injected along with the
remediation substrates. A sampling and analysis table summarizing the locations, constituents, and methods is presented on
Table 4. Laboratory results and C-O-Cs are contained in Appendix A.
Water samples were analyzed to the laboratory specific Method Detection Limits (MDL), which are quantifiable at or below
the current Solid Waste Section detection limits (SWSL). Table 5 summarizes constituents detected in groundwater and
surface water samples that attain or were above the current SWSL, Groundwater Protection Standards (GWP), North
Carolina Groundwater Standards (2L), the applicable North Carolina Surface Water Standards (2B) for a class C waterbody,
and Maximum Contaminant Levels (MCL) also known as “Federal Primary Drinking Water Standards”.
Quality Control Samples
No contaminants were detected in any of the quality control blanks above Standards, therefore the data set is believe to not be
significantly impacted by high bias or false positives.
Groundwater Samples
Metals
Five total metals were detected above 2L/GWP Standards in samples collected from 13 wells including the upgradient
background well (MW-1) during this event. Total metals detected above 2L/GWP Standards were:
Cd Cr Co Tl Va
2L/GWP STD 2 10 1 0.28 0.3
MW-1 (BG Well)6.8 12
MW-6 80.4 8.3
MW-7 54.2
MW-9 174 6.4
MW-11 4.4 J
MW-13 6.8 J
MW-15 2.6 J
MW-16 10.7 621 21
MW-17 31.7 6.3
MW-18 3
MW-19 2.9 J
MW-20 19
MW-21 5.2 J
J = Detected below SWSL therefore value considered an estimate. All concentrations in ug/L.
3
Volatile Organic Compounds
One or more VOC(s) were detected above their respective 2L Standard in samples collected from 5 monitoring wells (MW-9,
MW-11, MW-15, MW-16 and MW-22).
Benzene 1,2-DCA 1,1-DCA 1,4-DCB VC
2L STD 1 0.38 6 6 0.03
MCL STD 5 5 NE 75 5
MW-9 1.5 8.2
MW-11 1
MW-15 8.2 1.5
MW-16 2.3 1.6 17.9 4.5
MW-22 6.5
Concentrations in ug/L
The majority of the monitoring locations that were found to contain VOCs included a mixture of dissolved phase aromatic
hydrocarbons and chlorinated aliphatic hydrocarbons. The only constituent detected above the EPA established maximum
contaminant levels (MCLs) primary “Drinking Water Standards” was vinyl chloride in sample MW-9. A site map depicting
the concentrations and estimated horizontal extent of VOCs that exceeded the 2L Standard during this event is presented on
Sheet 2.
The on-site water supply well (SCALEHOUSE) continues to lack detections in exceedance of current groundwater or
drinking water Standards.
Surface Water Samples
Contaminants were not detected above NC 2B Surface Water Standards in any of the surface water samples.
Corrective Action Update
Groundwater remediation continues to be implemented per the approved Corrective Action Plan (CAP) at the three
designated areas of concern (AOC) (Northern, Southern and MW-11). A Corrective Action Evaluation Report (CAER) (DIN:
19361) was submitted on May 1, 2013 which demonstrated that the plumes continue to decrease and was approved by the the
SWS on July 24, 2013 (DIN:19366). A historical summary of corrective actions performed to date are briefly presented in
the following sections.
MNA Analysis (AOCs Northern, Southern and MW-11)
Semi-annual MNA monitoring of a subset of 12 wells for the full suite of SWS recommended parameters was initiated on
May 18, 2010 and performed for four consecutive semi-annual events to establish a baseline. A revised SAP prescribing 7
wells with various targeted MNA constituents was approved by the SWS and initiated during an event performed in May
2013. MNA monitoring was performed during this event for the parameters and frequency as listed in the current SAP.
MNA parameters quantified during this event included VFA, methane, ethane, ethene, hydrogen, alkalinity, sulfate, sulfide,
chloride, TOC, COD, ferrous iron, turbidity, DO and ORP. MNA parameters are presented on Table 6.
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Enhanced Bioremediation via Substrate Injection (AOC Southern and Northern)
Per the SWS approved Corrective Action Plan enhanced bioremediation via substrate and tracer injection was initiated in the
Southern and Northern AOCs in accordance with requirements outlined in the Injection Well Permit Application and Well
Permit No. WI0400176 (5/6/11) in an effort to reduce low level aliphatic and aromatic chlorinated hydrocarbons in
groundwater to below the 2L Standards. An edible oil substate (EOS)-water emulsion with sodium bromide tracer was
injected into four wells (IW-1, IW-2, IW-3 and IW-5) on November 2-3, 2011. Similar substrates were injected into
monitoring wells MW-4/IW-4 and MW-8/IW-6 on October 24-25, 2012. Details of the injection events are provided in the
Injection Event Record dated November 4, 2011 and January 10, 2013.
As directed in the UIC Injection Well Permit renewed on April 15, 2013 semi-annual post-injection water quality monitoring
of wells located downgradient of viable injection points (MW-3R, MW-7, MW-9, MW-12S, MW-13, MW-14, MW-15, MW-
16, MW-17, MW-18, MW-19, MW-20, MW-21, MW-22, MW-23) and upgradient background well MW-1 was also
performed in conjunction with this semi-annual event. Total VOC concentrations reported during this event were lower at all
locations when compared to the respective moving averages of the five events preceding injection in the selected wells
downgradient of the injection points (Figure 1).
Evaluation of injection wells (IW-1, IW-2, IW-3, IW-4, IW-5, IW-6) continues to indicate that a considerable amount of white
highly turbid (>1,000 NTU) viscous residual organic substrate and its byproducts remain in each of these wells rendering
them unsuitable for representative water quality analysis. The viscosity of the water in the injection wells during this May
2014 event precludes sample collection as either a bailer will not descend or the check valve fails. IW-1 was verified to not
be a viable injection well as less than 3 gallons of substrate was able to be injected into the low permeable fractured bedrock
and injectant levels have remained above static conditions for over a year. For all intents and purposes IW-1 injection did not
occur nor will be possible in the future.
In an attempt to track migration of injectants bromide was targeted at MW-16. MW-16, located 86 feet downgradient of
IW-3, is the only location exhibiting tracer levels which may potentially indicate injectant communication. Based on the
average linear velocity rates of IW-3 and MW-16 reported since injection the injectant was expected to reach MW-16 in May
2012. Bromide concentrations at MW-16 have been variable and were at the highest observed levels during this event
(Figure 2). Calculations performed following injection indicates that reported levels of bromide injected was insufficient to
provide clear evidence of migration within the uppermost aquifer.
MW-11 AOC Investigations
The CAP designated MW-11 as an area of concern due to detections of VOCs detected in exceedance of 2L Standards. MW-
11 is located within the compliance boundary near the northern property line which is hydraulically upgradient of the closed
northern landfill. The northern landfill closed before October 1991 which was before adoption of NC Section .1600 rules that
address assessment and corrective action. VOCs have historically been detected in excess of the 2L Standard at MW-11
which include a mixture of aromatics (fuel hydrocarbons) and chlorinated hydocarbons (solvents). Over the past 4 years (8
semi-annual events) the only constituent detected in excess of 2L Standard and SWSL was 1,2-dichloropropane. During this
event levels of 1,2-dichloropropane fell remain above the 2L Standard but fell below the SWSL thus “j-qualified”. The CAP
prescribed MNA and enhanced biodegredation to remediate MW-11 AOC. MNA has been performed continuously
5
semiannually at MW-11 the past 6 years. Enhanced biodegredation has not been initiated at MW-11 AOC since
hydrogeologic conditions relative to the source and property boundaries preclude it as an effective technique. MW-11 is
positioned hydraulically upgradient of the source and is within the review boundary. A well was attempted to be installed at
the property line 110 feet north of MW-11 on January 26, 2015 to delineate the extent of contamination. The potentiometric
head at B-11R was expected to be at 25 feet (1132 ft amsl) but the boring encountered very competent rock at 9 ft and
remained dry to 55 ft. (1102 ft amsl) for over 48 hours so was abandoned.
Groundwater and Surface Water Characterization
A potentiometric map constructed from water elevations taken from the uppermost aquifer which consists of both saprolite
and the hydraulically connected upper portion of the fractured bedrock system is enclosed as Sheet 2. Groundwater flow
directions and velocity rates were calculated through modified Darcy's equation as shown on Table 7. Consistent with
previous events the groundwater apparently flows in a general southeasterly direction towards the tributaries of the Ararat
River. The calculated average linear velocity of groundwater indicates an approximate average of 842 ft/yr in the wells
screened in regolith and 593 ft/yr in the wells screened in the bedrock. The consistent disparity in flow rates between wells is
indicative of heterogeneous geologic conditions and/or a product of the limitations of the linear velocity equation when
applied to anisotropic conditions which are characteristic of the geology of the Piedmont. Streams located within the facility
boundaries were observed to be of low volume and flow with low turbidity.
Findings
The metals are believed to be natural originating from erosion of natural deposits rather than anthropogenic.
The on-site supply well and the surface water points remain unimpacted as indicated by the lack of detections in excess of the
applicable Standards. The on-site supply well is not considered potable thus bottled water is provided for consumption and
“Non-Potable Water” warning signs were observed.
One or more Appendix I VOC(s) continue to be detected in quantifiable levels above the 2L Standard in samples collected
from the uppermost aquifer at five locations (MW-9, MW-11, MW-15, MW-16 and MW-22). All VOC concentrations
remain within their own respective historically identified range.
Qualitative evaluation of VOC concentrations indicate a decreasing trend over time and distance from the landfill. Total
cumulative VOC concentrations during this event decreased at all locations compared to their respective five event averages
preceding corrective action except for MW-9, MW-17 and MW-20 (Figure 3). Results of statistical temporal trend analysis,
using Sen's Slope Estimator at a 95% confidence level, compared to when corrective action began 5.5 years ago indicate that
none of the individual well's cumulative VOC concentrations have increased and the Southern AOC and cumulative site-wide
levels continue to exhibit a decreasing trend.
The area of the uppermost aquifer beyond the compliance boundary containing quantifiable concentrations of VOCs in
exceedance of the 2L Standard during this event is estimated at 0.0 acres in the Northern AOC, 0.0 acres in the MW-11 AOC
and 6 acres in the Southern AOC for a total facility wide area of 6 acres (Sheet 2). This is an estimated 25% retraction of
facility-wide plume area (from 8 acres to 6 acres) compared to when corrective action was initiated 5.5 years ago.
6
Sheets
Topographic Map with Site Location
SHEET 1
Surry County Landfill, Mt. Airy
237 Landfill Road
Mount Airy, NC 28621
Lat: 36-26-30.065
Long:-80-34-15.314
Northing:983356.18
Easting:1537885.48
Closed Unlined C&D Landfill
Closed Unlined Sanitary Landfill
Active Lined MSW Landfill
Surry Co Property Line
Figures
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1
Figure 1
October 22, 2009 – December 3, 2016
Well ID
INJECTION WELL (IW-1) UNSUCCESSFUL INJECTION SO DOWNGRADIENT WELLS NOT SHOWN
INJECTION WELL (IW-2) MONITORED DOWNGRADIENT BY MW-12S, MW-13 & MW-18
MW-12S 0.00 0.00 0.00 0.00 5.40 1.08 0.00 -1.08 -100
MW-13 61.00 50.60 74.20 87.30 72.50 69.12 18.60 -50.52 -73
MW-18 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0
INJECTION WELL (IW-3) MONITORED DOWNGRADIENT BY MW-3R & MW-16
MW-3R 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0
MW-16 137.90 113.60 135.70 121.20 116.30 124.94 69.80 -55.14 -44
INJECTION WELL (IW-4) MONITORED DOWNGRADIENT BY MW-14, MW-21 & MW-23
MW-14 15.20 15.60 15.60 8.20 17.00 14.32 0.00 -14.32 -100
MW-21 52.10 50.70 51.38 39.10 32.41 45.14 15.37 -29.77 -66
MW-23 4.30 0.00 0.00 0.00 0.00 0.86 0.00 -0.86 -100
INJECTION WELL (IW-5) MONITORED DOWNGRADIENT BY MW-15 & MW-19
MW-15 96.13 63.89 55.00 78.10 64.06 71.44 70.94 -0.50 -1
MW-19 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0
INJECTION WELL (IW-6) NOT SHOWN AS NO WELLS DOWNGRADIENT WITHIN ZONE OF INFLUENCE
Total Cumulative VOC Concentrations Pre/Post Injection Comparison
Oct
2009
(ug/L)
May
2010
(ug/L)
Oct
2010
(ug/L)
May
2011
(ug/L)
Oct
2011
(ug/L)
Average of
first Five
Corrective
Action
Events
(ug/L)
Dec
2016
(ug/L)
Difference
(ug/L)
Difference
(%)
Statistical Trend*
Between Oct
2009-Dec 2016
No Trend
Downward
No Trend
No Trend
Downward
No Trend
Downward
No Trend
No Trend
No Trend
* = Statistical Trend analysis via Sen's Slope Estimator at a 95% confidence level11/3/2011 (INJECTED)11/3/2011 (INJECTED)11/3/2011 (INJECTED)10/24/2013 (INJECTED)
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1
Figure 2
Bromide Tracer Concentrations Time Series Graph and Table
February 9, 2012 – December 2, 2016
Date MW-16
2/9/2012 0.038 (j)
5/30/2012 0.130 (j)
8/20/2012 0.260 (j)
10/23/2012 0.280 (j)
5/30/2013 0.140 (j)
10/31/2013 0.110 (j)
5/28/2014 0.220 (j)
10/22/2014 0.350 (j)
5/28/2015 0.290 (j)
11/22/2015 0.22 (j)
6/16/2016 0.19 (j)
12/2/2016 0.58 (j)
(j) = The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL),
* = May 25, 2012 Calculated date injectant expected to reach MW-16 using average flow rates of IW-3 and MW-16 (155 ft/yr) since injection occurred.
0.00
0.10
0.20
0.30
0.40
0.50
0.60
0.70
Bromide Tracer Levels in MW-16
Located 87 feet Downgradient of IW-3 which was Injected on November 2, 2011
MW-16
Datemg/LDate injectant expected
to reach
MW-16*Date injectant expected to reach MW-16*
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1
Figure 3
Total Cumulative VOC Concentrations Time Series Graphs/Table
October 22, 2009 – December 3, 2016
AOC Well ID Dec 2016 Difference Difference
(%)Oct 2009 – Dec 2016
Background MW-1 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend
Southern
IW-2 (MW-2)105.25 207.00 207.93 159.90 79.10 151.84 NS NS No Trend
IW-3 (MW-3RS)202.90 127.50 127.50 144.00 127.60 145.90 NS NS No Trend
MW-3R 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend
IW-4 (MW-4)27.00 24.20 24.20 27.60 23.50 25.30 NS NS No Trend
IW-5 (MW-5)35.00 46.50 46.50 47.40 34.80 42.04 NS NS No Trend
MW-12S 0.00 0.00 0.00 0.00 5.40 1.08 0.00 -1.08 -100 No Trend
MW-12D 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend
MW-13 61.00 50.60 74.20 87.30 72.50 69.12 31.74 -37.38 -54 Downward
MW-14 15.20 15.60 15.60 8.20 17.00 14.32 10.90 -3.42 -24 Downward
MW-15 96.13 55.00 55.00 78.10 64.06 69.66 45.67 -23.99 -34 No Trend
MW-16 137.90 113.60 135.70 121.20 116.30 124.94 82.98 -41.96 -34 Downward
MW-17 20.34 8.40 8.85 0.00 5.77 8.67 13.42 4.75 55 No Trend
MW-18 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend
MW-19 0.00 0.00 0.00 0.00 0.00 0.00 3.70 3.70 0 No Trend
MW-21 52.10 50.70 51.38 39.10 32.41 45.14 22.23 -22.91 -51 Downward
MW-22 28.90 23.80 23.80 11.66 5.20 18.67 0.00 -18.67 -100 Downward
MW-23 4.30 0.00 0.00 0.00 0.00 0.86 0.00 -0.86 -100 No Trend
Combined Total 786.02 722.90 770.66 724.46 583.64 717.54 470.24 -247.30 -34 Downward
Northern
MW-6 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend
MW-7 7.40 9.40 11.20 9.70 8.80 9.30 0.00 -9.30 -100 No Trend
IW-6 (MW-8)22.00 23.90 16.00 12.30 12.60 17.36 NS NS No Trend
MW-9 23.50 20.40 23.20 25.80 22.90 23.16 35.50 12.34 53 No Trend
MW-20 0.00 0.00 0.00 0.00 0.00 0.00 0.87 0.87 0 No Trend
Combined Total 52.90 53.70 50.40 47.80 44.30 49.82 48.97 -0.85 -2 No Trend
MW-11 MW-11 10.10 6.00 6.00 5.44 23.20 10.15 5.80 -4.35 -43 No Trend
SITEWIDE Combined Total 849.02 782.60 827.06 777.70 651.14 777.50 525.01 -252.49 -32 Downward
Oct
2009
May
2010
Oct
2010
May
2011
Oct
2011
Average of
first Five Corrective
Action
Events Statistical Trend*
(ug/L)(ug/L)(ug/L)(ug/L)(ug/L)(ug/L)(ug/L)(ug/L)
79.10 NS
127.60 NS
18.10 NS
34.80 NS
12.60 NS
NS = Not sampled this event so most recent concentration shown and used in calculations
* = Statistical trend analysis via Sen's Slope Estimator at a 95% Confidence Level
Tables
Table 1
Groundwater Monitoring Well Construction Table
December 1-3, 2016
Well
Diameter
Total Well
Depth
Top of
Screen
Depth
Screen
Length
Top of
Casing
Elevation
Ground
Elevation
Groundwater
Elevation
Depth to
Water
(inches)(ft bgs)(ft bgs)(ft)(ft amsl)(ft amsl)(ft amsl)(ft btoc)
MW-1 11/28/89 2 40 30 10 Clay 1134.35 1133.15 1108.20 26.15 36.439211 -80.568133
IW-2 (was MW-2)11/28/89 2 70 60 10 Clay 1068.86 1068.36 1028.65 40.21 36.435833 -80.568894
MW-3R 9/27/94 2 101 86 15 Rock 1017.50 1015.00 975.39 42.11 36.434725 -80.571989
IW-3 (was MW-3RS)5/17/01 2 52 37 15 Rock 1020.57 1018.24 988.01 32.56 36.434656 -80.571858
IW-4 (was MW-4)8/30/94 2 55.4 40.4 15 Rock 1026.26 1025.06 991.95 34.31 36.434686 -80.569200
IW-5 (was MW-5)8/27/94 2 63 48 15 Rock 1080.18 1077.78 <1039.50 >40.68 36.434614 -80.570436
MW-6 9/7/94 2 29.7 14.7 15 Rock 1067.67 1065.61 1044.66 23.01 36.437431 -80.571067
MW-7 8/23/94 2 23 8 15 Rock 1073.50 1071.50 1060.24 13.26 36.438439 -80.570722
IW-6 (was MW-8)8/16/94 2 54 39 15 Rock 1088.45 1086.45 1045.26 43.19 36.439278 -80.570381
MW-9 8/22/94 2 43.8 28.8 15 Rock 1094.07 1092.07 1060.85 33.22 36.439289 -80.571508
MW-11 8/15/94 2 40 25 15 Rock 1151.80 1150.40 1127.51 24.29 36.441589 -80.569558
MW-12S 5/31/01 2 51 11 40 Rock 1025.80 1023.25 1011.65 14.15 36.435942 -80.567972
MW-12D 5/30/01 2 100 90 10 Rock 1027.05 1023.75 1027.05 0.00 36.435964 -80.567994
MW-13 5/30/06 2 35.78 20.78 15 Saprolite 1008.48 1005.75 982.79 25.69 36.435036 -80.568183
MW-14 5/30/06 2 48.03 33.03 15 Rock 1018.80 1016.11 981.39 37.41 36.434267 -80.569239
MW-15 6/22/06 2 57 42 15 Rock 1075.96 1073.23 1026.32 49.64 36.433797 -80.570467
MW-16 6/21/06 2 36.3 21.3 15 Rock 999.54 996.67 972.39 27.15 36.434536 -80.572117
MW-17 6/1/07 2 15.32 5.32 10 Rock 965.43 962.26 955.72 9.71 36.433558 -80.572517
MW-18 6/1/07 2 18.15 8.15 10 Saprolite 983.00 980.00 973.95 9.05 36.435453 -80.567050
MW-19 6/1/07 2 17.1 7.1 10 PWR 946.27 942.97 937.41 8.86 36.432231 -80.570556
MW-20 6/1/07 2 25.64 10.64 15 Rock 1082.19 1079.12 1062.74 19.45 36.439025 -80.571650
MW-21 6/1/07 2 15.41 5.41 10 Saprolite/PWR 965.36 962.22 959.42 5.94 36.434214 -80.568717
MW-22 6/1/07 2 16.04 6.04 10 Saprolite 953.40 950.23 948.35 5.05 36.432928 -80.571678
MW-23 6/1/07 2 17.1 7.1 10 Sandy Silt 955.31 952.09 947.85 7.46 36.432828 -80.569156
NOTE:
bgs = below ground surface
amsl= above mean sea level
btoc = below top of casing (PVC well casing)
Monitoring Well Date
Installed
Geology of
Screened
Interval
Latitude Longitude
Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1
Table 2
Field Observations of Monitoring Locations
December 1-3, 2016
Location
Viable
Monitoring
Location
Lack of Any
Evidence of
Tampering
Locked on
Arrival &
Departure
Hinge/Hasp
Operational
Tagged
or
Labeled
Concrete
Surface Pad
Appears
Effective
Comments
MW-1 Yes Yes Yes Yes Yes Yes
IW-1 No Yes Yes Yes Yes Yes Fouled since injection 11/2/11.
IW-2 (was MW-2)No Yes Yes Yes Yes Yes Fouled since injection 11/2/11.
MW-3R Yes Yes Yes Yes Yes Yes
IW-3 (was MW-3RS)No Yes Yes Yes Yes Yes Fouled since injection 11/2/11.
IW-4 (was MW-4)No Yes Yes Yes Yes Yes Fouled since injection 10/24/12.
IW-5 (was MW-5)No Yes Yes Yes Yes Yes Fouled since injection 11/2/11. Bailer would not descend
MW-6 Yes Yes Yes Yes Yes Yes
MW-7 Yes Yes Yes Yes Yes Yes
IW-6 (was MW-8)No Yes Yes Yes Yes Yes Fouled since injection 10/24/12.
MW-9 Yes Yes Yes Yes Yes Yes
MW-11 Yes Yes Yes Yes Yes Yes
MW-12S Yes Yes Yes Yes Yes Yes
MW-12D Yes Yes Yes Yes Yes Yes Flowing artesian
MW-13 Yes Yes Yes Yes Yes Yes
MW-14 Yes Yes Yes Yes Yes Yes
MW-15 Yes Yes Yes Yes Yes Yes
MW-16 Yes Yes Yes Yes Yes Yes
MW-17 Yes Yes Yes Yes Yes Yes
MW-18 Yes Yes Yes Yes Yes Yes
MW-19 Yes Yes Yes Yes Yes Yes
MW-20 Yes Yes Yes Yes Yes Yes
MW-21 Yes Yes Yes Yes Yes Yes
MW-22 Yes Yes Yes Yes Yes Yes
MW-23 Yes Yes Yes Yes Yes Yes
SW-1 Yes -----Low gage height & flow
SW-2 Yes -----Low gage height & flow
SW-3 Yes -----Low gage height & flow
SW-4 Yes -----Low gage height & flow
SWN-1 Yes -----Low gage height & flow
SWN-2 Yes -----Low gage height & flow
SCALEHOUSE Yes -----Sample from spigot next to well which is typical
Any unusual field conditions, observations, or events:
Visual markers (10 ft PVC pipes) remain secured to each monitoring well case
Injection wells (IW-1, IW-2, IW-3, IW-4, IW-5 and IW-6) exempt from laboratory analysis as SWS approved on May 10, 2013 (DIN:18938)
Stormwater control improvements performed since May 2012 event.
Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1
Table 3
Field Parameter Data Summary
December 1-3, 2016
Parameter
Depth to
Water*
Water
Elevation
TOC
Elevation Temp.ORP DO pH
Specific
Conductance TDS Turbidity
Units ft (btoc)ft (amsl)ft (amsl) C mV mg/L SU umhos/cm mg/L Visual or NTU
MW-1 26.15 1108.20 1134.35 16.4 214 2.4 6.4 321 NR Clear
IW-2 40.21 1028.65 1068.86 NR NR NR NR NR NR >1000
MW-3R 42.11 975.39 1017.50 15.9 117 0.9 8.3 307 NR Clear
IW-3 32.56 988.01 1020.57 NR NR NR NR NR NR >1000
IW-4 34.31 991.95 1026.26 NR NR NR NR NR NR >1000
IW-5 >40.68 <1039.50 1080.18 NR NR NR NR NR NR NR
MW-6 23.01 1044.66 1067.67 15.1 -35 0.9 6.9 423 NR Slight
MW-7 13.26 1060.24 1073.50 16.1 191 0.7 6.5 312 NR Clear
IW-6 43.19 1045.26 1088.45 NR NR NR NR NR NR >1000
MW-9 33.22 1060.85 1094.07 15.9 -23 0.9 6.1 421 NR Clear
MW-11 24.29 1127.51 1151.80 15.5 126 3.1 5.2 431 NR Clear
MW-12S 14.15 1011.65 1025.80 15.1 -91 0.9 6.9 162 NR Slight
MW-12D 0.00 1027.05 1027.05 14.8 55 3.1 6.1 290 NR Slight
MW-13 25.69 982.79 1008.48 14.9 193 0.9 6.1 215 NR Slight
MW-14 37.41 981.39 1018.80 14.9 117 2.1 5.4 126 NR Slight
MW-15 49.64 1026.32 1075.96 15.1 19 0.9 5.9 163 NR Very Turbid
MW-16 27.15 972.39 999.54 15.2 133 0.5 6.0 421 NR Clear
MW-17 9.71 955.72 965.43 15.1 138 0.6 5.9 419 NR Clear
MW-18 9.05 973.95 983.00 15.2 224 4.4 6.5 200 NR Clear
MW-19 8.86 937.41 946.27 15.3 206 4.1 5.8 36 NR Clear
MW-20 19.45 1062.74 1082.19 16.1 119 1.5 6.5 73 NR Slight
MW-21 5.94 959.42 965.36 15.3 226 3.5 5.9 173 NR Clear
MW-22 5.05 948.35 953.40 15.1 137 1.1 6.1 193 NR Clear
MW-23 7.46 947.85 955.31 15.1 293 3.1 6.4 123 NR Clear
Scalehouse na na na 14.9 301 4.3 7.0 730 NR Clear
Minimum 0.00 937.41 946.27 14.8 -91 0.5 5.2 36 NR Clear
Average 23.12 1009.47 1034.58 15.4 133 2.0 -277 NR Slight
Maximum 49.64 1127.51 1151.80 16.4 301 4.4 8.3 730 NR Very Turbid
SW-1 ---11.8 NR NR 7.0 240 NR Clear
SW-2 ---12.1 NR NR 6.9 310 NR Slight
SW-3 ---12.2 NR NR 7.1 340 NR Clear
SW-4 ---12.4 NR NR 6.9 280 NR Clear
SWN-1 ---12.5 NR NR 7.1 30 NR Clear
SWN-2 ---12.9 NR NR 7.1 160 NR Clear
Minimum ---11.8 NR NR 6.9 30 NR Clear
Average ---12.3 NR NR -227 NR Clear
Maximum ---12.9 NR NR 7.1 340 NR Slight
btoc = Below top of casing
amsl = Above mean sea level
na = Not available
NR = No reading attempted
Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1
Table 4
Sampling and Analysis Summary
December 1-3, 2016
Tracer
VOCsTotal MetalsVFAHydrogenMethane/Ethene/EthaneDissolved CO2AlkalinitySulfateSulfideChlorideTOCCODIron, ferrousNitrateDissolved Oxygen (DO)Oxidation Reduction Potential (ORP)TemperatureConductivityTotal Dissolved Solids (TDS)pHTurbidityBromideLab EPA 8260B Lab EPA 6000/7000AM23GAM20GAXAM20GAXField Hach KitEPA 310.2EPA 300.0Lab SM18 4500-S DEPA 300.0SM 5310BSM 5220DLab EPA 6010Lab EPA 9014Field MeterField MeterField MeterField MeterField MeterField MeterField Meter or VisualEPA 300.0IW-1
MW-1 X X X X X X X X X X X X X X X X X X
IW-2
MW-3R X X X X X X X X
IW-3
IW-4
IW-5
MW-6 X X X X X X X X
MW-7 X X X X X X X X X X X X X X X X X X
IW-6
MW-9 X X X X X X X X X X X X X X X X X X
MW-11 X X X X X X X X X X X X X X X X X X
MW-12S X X X X X X X X
MW-12D X X X X X X X X
MW-13 X X X X X X X X
MW-14 X X X X X X X X X X X X X X X X X X
MW-15 X X X X X X X X
MW-16 X X X X X X X X X
MW-17 X X X X X X X X
MW-18 X X X X X X X X
MW-19 X X X X X X X X
MW-20 X X X X X X X X
MW-21 X X X X X X X X X X X X X X X X X X
MW-22 X X X X X X X X
MW-23 X X X X X X X X
Scalehouse X X X X X X X X
SW-1 X X X X X X
SW-2 X X X X X X
SW-3 X X X X X X
SW-4 X X X X X X
SWN-1 X X X X X X
SWN-2 X X X X X X
EB X X
FB X X
TB X
Injection wells exempt from monitoring except for turbidity and WLR per SWS approved SAP [18936]
Not sampled as injection well exempt
App I = Appendix I List from current 40 CFR 258
Not sampled as injection well exempt
Not sampled as injection well exempt
Not sampled as injection well exempt
Not sampled as injection well exempt
App. I MNA Field Parameter
Not sampled as injection well exempt
Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1
Table 5A
Detections in Groundwater Samples
December 1-3, 2016
Parameter Name Units SWSL 2L/GWP
Std
MCL MW-1 MW-3R MW-6 MW-7 MW-9 MW-11 MW-12S MW-12D MW-13 MW-14 MW-15 MW-16 MW-17 MW-18 MW-19 MW-20 MW-21 MW-22 MW-23 SCALE
HOUSE
EB FB TB
Arsenic, total ug/L 10 10 10 2.7 J <2.5 <2.5 <2.5 <2.5 2.8 J 2.6 J <2.5 <2.5 <2.5 3.1 J 2.9 J 2.6 J <2.5 <2.5 <2.5 2.5 J <2.5 5.6 J 3 J 3.3 J 3.4 J --
Barium, total ug/L 100 700 2000 289 7.2 J 122 61.8 J 55.3 J 34.4 J 17.8 J 7.3 J 67.7 J 32.9 J 20.6 J 150 77.7 J 10.8 J 57.6 J 35.7 J 69.4 J 18.4 J 38.8 J 12.8 J <2.5 <2.5 --
Cadmium, total ug/L 1 2 5 6.8
(N)
1 <0.5 <0.5 <0.5 <0.5 <0.5 0.93 J <0.5 <0.5 <0.5 0.52 J <0.5 3 (N)<0.5 <0.5 <0.5 <0.5 0.53 J <0.5 <0.5 <0.5 --
Chromium, total ug/L 10 10 100 5.8 J <2.5 2.8 J <2.5 3 J <2.5 2.6 J <2.5 2.7 J <2.5 <2.5 10.7
(N)
4.2 J <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 --
Cobalt, total ug/L 10 1 NE 12 (N)<2.5 80.4
(N)
54.2
(N)
174
(N)
4.4 J
(N)
<2.5 <2.5 6.8 J (N)<2.5 <2.5 621 (N)31.7
(N)
<2.5 <2.5 19 (N)5.2 J
(N)
<2.5 <2.5 <2.5 <2.5 <2.5 --
Copper, total ug/L 10 1000 1300 7 J <2.5 <2.5 <2.5 <2.5 4.2 J <2.5 <2.5 <2.5 <2.5 <2.5 6.2 J <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 24.7 <2.5 <2.5 --
Lead, total ug/L 10 15 15 3.4 J <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 7.6 J <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 --
Nickel, total ug/L 50 100 NE 8.7 J <2.5 5.1 J <2.5 5.4 J <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 25.4 J 7.5 J <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 --
Thallium, total ug/L 5.5 0.28 2 <5 <5 8.3 (N)<5 6.4 (N)<5 <5 <5 <5 <5 <5 21 (N)6.3 (N)<5 <5 <5 <5 <5 <5 <5 <5 <5 --
Vanadium, total ug/L 25 0.3 NE <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 2.6 J <2.5 <2.5 <2.5 2.9 J <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 --
Zinc, total ug/L 10 1000 NE 113 <5 <5 8.7 J 8.1 J 8.5 J <5 <5 12.1 <5 <5 16.9 6.4 J 8.7 J 5.8 J 9.5 J 7.5 J <5 <5 11.9 <5 <5 --
1,1-Dichloroethane ug/L 5 6 NE <0.32 <0.32 <0.32 <0.32 1.5 J 0.41 J <0.32 <0.32 3.6 J 3.3 J 8.2 (L)1.9 J 0.37 J <0.32 1.5 J <0.32 4 J 1.1 J 0.61 J <0.32 <0.32 <0.32 <0.32
1,2-Dichlorobenzene ug/L 5 20 NE <0.3 <0.3 <0.3 <0.3 1.1 J <0.3 <0.3 <0.3 <0.3 <0.3 <0.3 2.3 J 1.2 J <0.3 <0.3 <0.3 <0.3 0.7 J <0.3 <0.3 <0.3 <0.3 <0.3
1,2-Dichloroethane ug/L 1 0.4 5 <0.24 <0.24 <0.24 <0.24 <0.24 0.32 J <0.24 <0.24 0.79 J
(L)
<0.24 0.51 J
(L)
3.1 (L)0.4 J <0.24 <0.24 <0.24 0.38 J 0.64 J
(L)
<0.24 <0.24 <0.24 <0.24 <0.24
1,2-Dichloropropane ug/L 1 0.6 5 <0.27 <0.27 <0.27 <0.27 <0.27 1 (L)<0.27 <0.27 <0.27 <0.27 <0.27 1.6 (L)<0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27 <0.27
1,4-Dichlorobenzene ug/L 1 6 75 <0.33 <0.33 0.48 J 1.3 4.5 1.7 <0.33 <0.33 3.5 <0.33 3.1 17.9
(L)
3.4 <0.33 <0.33 <0.33 <0.33 6.5 (L)<0.33 <0.33 <0.33 <0.33 <0.33
Benzene ug/L 1 1 5 <0.25 <0.25 0.4 J <0.25 1.5 (L)0.44 J <0.25 <0.25 <0.25 <0.25 0.76 J 2.3 (L)0.57 J <0.25 <0.25 <0.25 <0.25 0.43 J <0.25 <0.25 <0.25 <0.25 <0.25
Chlorobenzene ug/L 3 50 100 <0.23 <0.23 0.42 J 2.4 J 1.4 J 0.53 J <0.23 <0.23 1.2 J <0.23 2 J 7.2 3 J <0.23 <0.23 <0.23 <0.23 2 J <0.23 <0.23 <0.23 <0.23 <0.23
Chloroethane ug/L 10 3000 NE <0.54 <0.54 <0.54 <0.54 3.5 J <0.54 <0.54 <0.54 0.74 J <0.54 <0.54 <0.54 0.68 J <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54 <0.54
Chloromethane ug/L 1 3 NE <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 0.34 J <0.11 0.28 J <0.11 <0.11 <0.11 <0.11 0.2 J <0.11 <0.11 <0.11 0.22
J
<0.11 0.5 J
cis-1,2-Dichloroethene ug/L 5 70 70 <0.19 <0.19 <0.19 <0.19 13.8 1.4 J <0.19 <0.19 21 6.1 27.7 41.9 1.2 J <0.19 2.2 J 0.87 J 16.8 2.6 J 0.72 J 0.3 J <0.19 <0.19 <0.19
Tetrachloroethene ug/L 1 0.7 5 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 0.57 J <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46
Toluene ug/L 1 600 1000 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 2.6 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26 <0.26
Trichloroethene ug/L 1 3 5 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 0.91 J 0.59 J 1.9 <0.47 <0.47 <0.47 <0.47 <0.47 0.85 J <0.47 <0.47 <0.47 <0.47 <0.47 <0.47
Vinyl chloride ug/L 1 0.03 5 <0.62 <0.62 <0.62 <0.62 8.2 (L)<0.62 <0.62 <0.62 <0.62 <0.62 1.5 (L)4.5 (L)<0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62
RED FONT
YELLOW SHADE
J Detected >Lab Method Detection Limit (MDL)<SWSL "J-QUALIFED" May be considered an estimated value
<Non-Detects Shown relative to MDL
(L)Leachate &/or Landfill Gas (anthropogenic) is Preliminary Cause Assigned to Detection. A definitive source of the detection was not determined as part of this report.
(N)Erosion of Natural Deposits (not anthropogenic) is Preliminary Cause Assigned to Detection. A definitive source of the detection was not determined as part of this report.
>MCL "FED DRINKING WATER STANDARD"
METALS LISTED IN 40 CFR 258 APPENDIX I
VOLATILE ORGANIC COMPOUNDS (VOCS) LISTED IN 40 CFR 258 APPENDIX I
>2L/GWP STANDARD "NC GROUNDWATER STANDARDS" ADOPTED BY NC SWS
Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1
Table 5B
Detections in Surface Water Samples
November 29-30, 2016
Parameter
Name
Units SWSL 2B Std MCL SW-1 SW-2 SW-3 SW-4 SW-A SW-B SWN-1 SWN-2
Barium, total ug/L 100 200000 2000 27.5
J
30.4
J
22.2
J
24.4
J
----31.1 J 25.3 J
Lead, total ug/L 10 25 15 <2.5 3.4 J <2.5 2.5 J ----<2.5 <2.5
Zinc, total ug/L 10 50 NE <5 <5 <5 5.4 J ----<5 5.3 J
RED FONT
YELLOW SHADE
J Detected >Lab Method Detection Limit (MDL)<SWSL "J-QUALIFED" May be considered an estimated value
<Non-Detects Shown relative to MDL
METALS LISTED IN 40 CFR 258 APPENDIX I
>2B STANDARD "NC SURFACE WATER STANDARDS" ADOPTED BY NC SWS
>MCL "FED DRINKING WATER STANDARD"
Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1
Table 6
MNA Parameter Data Summary
December 1-3, 2016
MW-1 MW-7 MW-9 MW-11 MW-14 MW-15 MW-21
12/3/16 12/3/16 12/2/16 12/3/16 12/2/16 12/1/16 12/3/16
VFA – Acetic Acid AM23G 7 ug/L 82 26 21 30 31 380 32
VFA – Butyric Acid AM23G 7 ug/L 41 <7 <7 <7 <7 <7 <7
VFA – Lactic Acid AM23G 6 ug/L 42 26 95 18 28 <6 120
VFA – Propionic Acid AM23G 9 ug/L 110 <9 <9 <9 <9 <9 <9
VFA – Pyruvic Acid AM23G 7 ug/L 16 13 <7 <7 <7 <7 <7
Hydrogen AM20GAX 0.075 nM 1.5 1.4 1.6 1.6 1.5 1.6 1.6
Methane AM20GAX 0.027 ug/L 450 45 660 1100 280 1600 4.9
Ethene AM20GAX 0.003 ug/L 0.036 0.016 0.93 0.3 0.013 <.003 0.0059
Ethane AM20GAX 0.001 ug/L 0.0096 0.13 30 0.083 0.0053 <.001 0.0042
CO2-Dissolved Field HACH Kit 10 mg/L 80 >100 >100 >100 >100 >100 >100
Alkalinity SM 2320B 1000 ug/L 132000 53200 39300 35300 42400 47700 41000
Sulfate EPA 300.0 1000 ug/L 8580 3740 2090 7510 2880 1790 2570
Sulfide SM 4500-S2D 100 ug/L <100 <100 <100 699 <100 121 <100
Chloride SM 4500-Cl-E 500 ug/L 3930 25000 29400 9580 4180 1930 29900
TOC SM 5310B 500 ug/L <500 2680 1540 1920 2870 591 2430
COD SM 5220D 12500 ug/L 27000 27000 27000 14000 <12500 <12500 19000
BOD SM5210B NS ug/L NS NS NS NS NS NS NS
Ferrous Iron EPA 6010 500 ug/L <500 <500 4700 2600 <500 2500 <500
Nitrate EPA 353.2 NS ug/L NS NS NS NS NS NS NS
Temperature Field Instrument 0 C 16.4 16.1 15.9 15.5 14.9 15.1 15.3
ORP Field Instrument -900 mV 214 191 -23 126 117 19 226
DO Field Instrument 0 mg/L 2.4 0.7 0.9 3.1 2.1 0.9 3.5
pH Field Instrument 0 SU 6.4 6.5 6.1 5.2 5.4 5.9 5.9
Specific Conductance Field Instrument 0 us/cm 321 312 421 431 126 163 173TurbidityVisual0VisualClearClearClearClearSlightVeryClear
Notes:
VFA = Volatile Fatty Acids
MDL* = Lab Method Detection Limit or lowest field measurement possible. Constituents detected below quantifiable limits are shown as < MDL value.
>100 = CO2 Concentration exceeds maximum capability of method used.
NS = Not Sampled
Parameters Method MDL*Units
Surry County Closed CDLF and CLosed MSWLF, Mt. Airy Page 1 of 1
Table 7
Hydrogeologic Propeties at Monitoring Well Locations
December 1-3, 2016
Effective
Porosity
Hydraulic
Gradient
Groundwater
Average
Linear
Velocity Rate
Minimum
Distance
From
Upgradient
EOW
Ground
Water
Depth
Groundwater
Potentiometric
Elevation
(cm/second)(ft/day)(%)(feet/feet)(feet/year)(ft)(feet
btoc)(feet amsl)
MW-1 4.30E-05 0.122 15 0.057 17 S53W 0 26.15 1108.20 Clay
IW-2 4.30E-05 0.122 15 0.225 67 S40E -40.21 1028.65 Clay
MW-7 8.10E-04 2.296 15 0.101 563 N69W 704 13.26 1060.24 PWR/Fractured Rock
IW-6 4.40E-04 1.247 15 0.081 246 S47W -43.19 1045.26 PWR/Fractured Rock
MW-9 1.90E-04 0.539 15 0.506 663 S55E 614 33.22 1060.85 Sandy Silt
MW-13 2.06E-04 0.584 23 0.604 560 S29E 1850 25.69 982.79 Saprolite
MW-18 2.04E-03 5.783 15 0.271 na S26E 0 9.05 973.95 Saprolite
MW-19 1.10E-03 3.118 3 0.053 2,004 S12W 2663 8.86 937.41 PWR
MW-21 1.28E-03 3.628 3 0.024 1,053 S79E 2041 5.94 959.42 Saprolite/PWR
MW-22 9.88E-04 2.801 15 0.092 627 S28W 2506 5.05 948.35 Saprolite
MW-23 3.04E-04 0.862 15 0.064 134 S32E 2610 7.46 947.85 Sandy Silt
Minimum 4.30E-05 0.122 3 0.024 17 -0 5.05 937.41 -
Average 6.77E-04 1.918 14 0.189 593 -1443 19.83 1004.82 -
Maximum 2.04E-03 5.783 23 0.604 2,004 -2663 43.19 1108.2 -
MW-3R 2.40E-04 0.680 5 na na S61W 1,994 42.11 975.39 Fractured Rock
IW-3 2.40E-05 0.068 5 0.301 150 S37W -32.56 988.01 Fractured Rock
IW-4 1.10E-04 0.312 5 0.786 1,790 S45E -34.31 991.95 Fractured Rock
IW-5 1.50E-05 0.043 5 --S58E ---Fractured Rock
MW-6 1.90E-05 0.054 5 0.191 75 S82W 963 23.01 1044.66 Fractured Rock
MW-11 3.10E-04 0.879 5 0.087 557 S48W 0 24.29 1127.51 Fractured Rock
MW-12S na na 3 0.273 na S40E 0 14.15 1011.65 Fractured Rock
MW-12D 1.30E-06 0.004 5 na na S40E 0 0.00 1027.05 Fractured Rock
MW-14 7.45E-03 21.118 3 0.058 14,776 S74E 2098 37.41 981.39 Fractured Rock
MW-15 7.21E-05 0.204 3 0.379 943 S08E 49.64 1026.32 Fractured Rock
MW-16 2.82E-05 0.080 3 0.152 148 S53W 2089 27.15 972.39 Fractured Rock
MW-17 2.94E-04 0.833 3 0.233 2,368 S24W 2547 9.71 955.72 Rock
MW-20 1.92E-04 0.544 3 0.106 702 S20E 692 19.45 1062.74 Rock
Minimum 1.30E-06 0.004 3 0.058 75 -0 0.00 955.72 -
Average 1.19E-04 0.336 4 0.257 842 -1154 26.15 1013.73 -
Maximum 3.10E-04 0.879 5 0.786 2,368 -2547 49.64 1127.51 -
NOTE:Values for hydraulic conductivity determined via slug test by GAI, MESCO, or Joyce.
Hydrologic gradient from water levels recorded on December 1-3, 2016.
Wells screened entirely in rock were not utilized for flow directions/gradients.
Screens that traverse both rock and regolith assumed flow in regolith dominates.
Hydraulic Conducitivity value and flow rate for MW-14 was considered an outlier; therefore not included in the average or maximum.
na = Not available/applicable
Average Linear Velocity (Q) is defined by modified Darcy's equation:
K= hydraulic conductivity
where ne= effective porosity
dh= head difference
dl= horizontal distance
Well
Hydraulic
Conductivity Flow
Direction
Screened Interval
Lithology
Surry County Closed CDLFand Closed MSWLF, Mt. Airy Page 1 of 1
Appendix A
Laboratory Analysis Reports
Chains of Custody
#=CL#
December 19, 2016
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92321701
92321701
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
Surry Closed-Mt Airy (AM)
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory between December 02,
2016 and December 06, 2016. The results relate only to the samples included in this report. Results
reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's
Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 29
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92321701
Surry Closed-Mt Airy (AM)
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 2 of 29
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92321701
Surry Closed-Mt Airy (AM)
Lab ID Sample ID Matrix Date Collected Date Received
92321701001 MW-12D Water 12/01/16 13:30 12/02/16 07:09
92321701002 MW-6 Water 12/02/16 10:50 12/06/16 08:31
92321701003 MW-11 Water 12/03/16 09:05 12/06/16 08:31
92321701004 SCALEHOUSE Water 12/03/16 11:50 12/06/16 08:31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
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[phone]
Page 3 of 29
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92321701
Surry Closed-Mt Airy (AM)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92321701001 MW-12D EPA 6010 15 PASI-AJMW, SH1
EPA 8260 50 PASI-CGAW
92321701002 MW-6 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 50 PASI-CGAW
92321701003 MW-11 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 50 PASI-CGAW
92321701004 SCALEHOUSE EPA 6010 15 PASI-AJMW, SH1
EPA 8260 50 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 4 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321701
Surry Closed-Mt Airy (AM)
Sample:MW-12D Lab ID:92321701001 Collected:12/01/16 13:30 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/13/16 04:32 7440-36-012/06/16 22:256.0 3.8 1
Arsenic ND ug/L 12/13/16 18:38 7440-38-212/06/16 22:2510.0 2.5 1
Barium 7.3J ug/L 12/13/16 04:32 7440-39-312/06/16 22:251002.5 1
Beryllium ND ug/L 12/13/16 04:32 7440-41-712/06/16 22:251.0 0.50 1
Cadmium 0.93J ug/L 12/13/16 04:32 7440-43-912/06/16 22:251.0 0.50 1
Chromium ND ug/L 12/13/16 04:32 7440-47-312/06/16 22:2510.0 2.5 1
Cobalt ND ug/L 12/13/16 04:32 7440-48-412/06/16 22:2510.0 2.5 1
Copper ND ug/L 12/13/16 04:32 7440-50-812/06/16 22:2510.0 2.5 1
Lead ND ug/L 12/13/16 04:32 7439-92-112/06/16 22:2510.0 2.5 1
Nickel ND ug/L 12/13/16 04:32 7440-02-012/06/16 22:2550.0 2.5 1
Selenium ND ug/L 12/13/16 18:38 7782-49-212/06/16 22:2510.0 5.0 1
Silver ND ug/L 12/13/16 04:32 7440-22-412/06/16 22:2510.0 2.5 1
Thallium ND ug/L 12/13/16 18:38 7440-28-012/06/16 22:255.5 5.0 1
Vanadium ND ug/L 12/13/16 04:32 7440-62-212/06/16 22:2525.0 2.5 1
Zinc ND ug/L 12/13/16 04:32 7440-66-612/06/16 22:2510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/07/16 18:15 67-64-110010.0 1
Acrylonitrile ND ug/L 12/07/16 18:15 107-13-12001.9 1
Benzene ND ug/L 12/07/16 18:15 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/07/16 18:15 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/07/16 18:15 75-27-41.0 0.18 1
Bromoform ND ug/L 12/07/16 18:15 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/07/16 18:15 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/07/16 18:15 78-93-31000.96 1
Carbon disulfide ND ug/L 12/07/16 18:15 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/07/16 18:15 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/07/16 18:15 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/07/16 18:15 75-00-310.0 0.54 1
Chloroform ND ug/L 12/07/16 18:15 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/07/16 18:15 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/07/16 18:15 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/07/16 18:15 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/07/16 18:15 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/07/16 18:15 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/07/16 18:15 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/07/16 18:15 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/07/16 18:15 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/07/16 18:15 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/07/16 18:15 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/07/16 18:15 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/07/16 18:15 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/07/16 18:15 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/07/16 18:15 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/07/16 18:15 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/07/16 18:15 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 03:36 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321701
Surry Closed-Mt Airy (AM)
Sample:MW-12D Lab ID:92321701001 Collected:12/01/16 13:30 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/07/16 18:15 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/07/16 18:15 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/07/16 18:15 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/07/16 18:15 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/07/16 18:15 108-10-11000.33 1
Styrene ND ug/L 12/07/16 18:15 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/07/16 18:15 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/07/16 18:15 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/07/16 18:15 127-18-41.0 0.46 1
Toluene ND ug/L 12/07/16 18:15 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/07/16 18:15 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/07/16 18:15 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/07/16 18:15 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/07/16 18:15 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/07/16 18:15 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/07/16 18:15 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/07/16 18:15 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/07/16 18:15 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %12/07/16 18:15 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %12/07/16 18:15 17060-07-070-130 1
Toluene-d8 (S)107 %12/07/16 18:15 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 03:36 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321701
Surry Closed-Mt Airy (AM)
Sample:MW-6 Lab ID:92321701002 Collected:12/02/16 10:50 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/16/16 23:39 7440-36-012/14/16 21:406.0 3.8 1
Arsenic ND ug/L 12/18/16 19:54 7440-38-212/14/16 21:4010.0 2.5 1
Barium 122 ug/L 12/16/16 23:39 7440-39-312/14/16 21:401002.5 1
Beryllium ND ug/L 12/16/16 23:39 7440-41-712/14/16 21:401.0 0.50 1
Cadmium ND ug/L 12/16/16 23:39 7440-43-912/14/16 21:401.0 0.50 1
Chromium 2.8J ug/L 12/16/16 23:39 7440-47-312/14/16 21:4010.0 2.5 1
Cobalt 80.4 ug/L 12/16/16 23:39 7440-48-412/14/16 21:4010.0 2.5 1
Copper ND ug/L 12/16/16 23:39 7440-50-812/14/16 21:4010.0 2.5 1
Lead ND ug/L 12/16/16 23:39 7439-92-112/14/16 21:4010.0 2.5 1
Nickel 5.1J ug/L 12/16/16 23:39 7440-02-012/14/16 21:4050.0 2.5 1
Selenium ND ug/L 12/16/16 23:39 7782-49-212/14/16 21:4010.0 5.0 1
Silver ND ug/L 12/16/16 23:39 7440-22-412/14/16 21:4010.0 2.5 1
Thallium 8.3 ug/L 12/16/16 23:39 7440-28-012/14/16 21:405.5 5.0 1
Vanadium ND ug/L 12/16/16 23:39 7440-62-212/14/16 21:4025.0 2.5 1
Zinc ND ug/L 12/16/16 23:39 7440-66-612/14/16 21:4010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/07/16 18:33 67-64-110010.0 1
Acrylonitrile ND ug/L 12/07/16 18:33 107-13-12001.9 1
Benzene 0.40J ug/L 12/07/16 18:33 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/07/16 18:33 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/07/16 18:33 75-27-41.0 0.18 1
Bromoform ND ug/L 12/07/16 18:33 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/07/16 18:33 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/07/16 18:33 78-93-31000.96 1
Carbon disulfide ND ug/L 12/07/16 18:33 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/07/16 18:33 56-23-51.0 0.25 1
Chlorobenzene 0.42J ug/L 12/07/16 18:33 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/07/16 18:33 75-00-310.0 0.54 1
Chloroform ND ug/L 12/07/16 18:33 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/07/16 18:33 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/07/16 18:33 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/07/16 18:33 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/07/16 18:33 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/07/16 18:33 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/07/16 18:33 95-50-15.0 0.30 1
1,4-Dichlorobenzene 0.48J ug/L 12/07/16 18:33 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/07/16 18:33 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/07/16 18:33 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/07/16 18:33 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/07/16 18:33 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/07/16 18:33 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/07/16 18:33 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/07/16 18:33 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/07/16 18:33 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/07/16 18:33 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 03:36 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321701
Surry Closed-Mt Airy (AM)
Sample:MW-6 Lab ID:92321701002 Collected:12/02/16 10:50 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/07/16 18:33 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/07/16 18:33 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/07/16 18:33 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/07/16 18:33 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/07/16 18:33 108-10-11000.33 1
Styrene ND ug/L 12/07/16 18:33 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/07/16 18:33 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/07/16 18:33 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/07/16 18:33 127-18-41.0 0.46 1
Toluene ND ug/L 12/07/16 18:33 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/07/16 18:33 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/07/16 18:33 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/07/16 18:33 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/07/16 18:33 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/07/16 18:33 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/07/16 18:33 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/07/16 18:33 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/07/16 18:33 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %12/07/16 18:33 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %12/07/16 18:33 17060-07-070-130 1
Toluene-d8 (S)103 %12/07/16 18:33 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 03:36 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321701
Surry Closed-Mt Airy (AM)
Sample:MW-11 Lab ID:92321701003 Collected:12/03/16 09:05 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/16/16 23:42 7440-36-012/14/16 21:406.0 3.8 1
Arsenic 2.8J ug/L 12/18/16 19:58 7440-38-212/14/16 21:4010.0 2.5 1
Barium 34.4J ug/L 12/16/16 23:42 7440-39-312/14/16 21:401002.5 1
Beryllium ND ug/L 12/16/16 23:42 7440-41-712/14/16 21:401.0 0.50 1
Cadmium ND ug/L 12/16/16 23:42 7440-43-912/14/16 21:401.0 0.50 1
Chromium ND ug/L 12/16/16 23:42 7440-47-312/14/16 21:4010.0 2.5 1
Cobalt 4.4J ug/L 12/16/16 23:42 7440-48-412/14/16 21:4010.0 2.5 1
Copper 4.2J ug/L 12/16/16 23:42 7440-50-812/14/16 21:4010.0 2.5 1
Lead ND ug/L 12/16/16 23:42 7439-92-112/14/16 21:4010.0 2.5 1
Nickel ND ug/L 12/16/16 23:42 7440-02-012/14/16 21:4050.0 2.5 1
Selenium ND ug/L 12/16/16 23:42 7782-49-212/14/16 21:4010.0 5.0 1
Silver ND ug/L 12/16/16 23:42 7440-22-412/14/16 21:4010.0 2.5 1
Thallium ND ug/L 12/16/16 23:42 7440-28-012/14/16 21:405.5 5.0 1
Vanadium ND ug/L 12/16/16 23:42 7440-62-212/14/16 21:4025.0 2.5 1
Zinc 8.5J ug/L 12/16/16 23:42 7440-66-612/14/16 21:4010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/07/16 18:50 67-64-110010.0 1
Acrylonitrile ND ug/L 12/07/16 18:50 107-13-12001.9 1
Benzene 0.44J ug/L 12/07/16 18:50 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/07/16 18:50 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/07/16 18:50 75-27-41.0 0.18 1
Bromoform ND ug/L 12/07/16 18:50 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/07/16 18:50 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/07/16 18:50 78-93-31000.96 1
Carbon disulfide ND ug/L 12/07/16 18:50 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/07/16 18:50 56-23-51.0 0.25 1
Chlorobenzene 0.53J ug/L 12/07/16 18:50 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/07/16 18:50 75-00-310.0 0.54 1
Chloroform ND ug/L 12/07/16 18:50 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/07/16 18:50 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/07/16 18:50 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/07/16 18:50 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/07/16 18:50 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/07/16 18:50 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/07/16 18:50 95-50-15.0 0.30 1
1,4-Dichlorobenzene 1.7 ug/L 12/07/16 18:50 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/07/16 18:50 110-57-61001.0 1
1,1-Dichloroethane 0.41J ug/L 12/07/16 18:50 75-34-35.0 0.32 1
1,2-Dichloroethane 0.32J ug/L 12/07/16 18:50 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/07/16 18:50 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 1.4J ug/L 12/07/16 18:50 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/07/16 18:50 156-60-55.0 0.49 1
1,2-Dichloropropane 1.0 ug/L 12/07/16 18:50 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/07/16 18:50 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/07/16 18:50 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 03:36 PM
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[phone]
Page 9 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321701
Surry Closed-Mt Airy (AM)
Sample:MW-11 Lab ID:92321701003 Collected:12/03/16 09:05 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/07/16 18:50 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/07/16 18:50 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/07/16 18:50 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/07/16 18:50 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/07/16 18:50 108-10-11000.33 1
Styrene ND ug/L 12/07/16 18:50 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/07/16 18:50 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/07/16 18:50 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/07/16 18:50 127-18-41.0 0.46 1
Toluene ND ug/L 12/07/16 18:50 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/07/16 18:50 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/07/16 18:50 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/07/16 18:50 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/07/16 18:50 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/07/16 18:50 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/07/16 18:50 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/07/16 18:50 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/07/16 18:50 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)96 %12/07/16 18:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %12/07/16 18:50 17060-07-070-130 1
Toluene-d8 (S)103 %12/07/16 18:50 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 03:36 PM
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[phone]
Page 10 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321701
Surry Closed-Mt Airy (AM)
Sample:SCALEHOUSE Lab ID:92321701004 Collected:12/03/16 11:50 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/16/16 23:45 7440-36-012/14/16 21:406.0 3.8 1
Arsenic 3.0J ug/L 12/18/16 20:10 7440-38-212/14/16 21:4010.0 2.5 1
Barium 12.8J ug/L 12/16/16 23:45 7440-39-312/14/16 21:401002.5 1
Beryllium ND ug/L 12/16/16 23:45 7440-41-712/14/16 21:401.0 0.50 1
Cadmium ND ug/L 12/16/16 23:45 7440-43-912/14/16 21:401.0 0.50 1
Chromium ND ug/L 12/16/16 23:45 7440-47-312/14/16 21:4010.0 2.5 1
Cobalt ND ug/L 12/16/16 23:45 7440-48-412/14/16 21:4010.0 2.5 1
Copper 24.7 ug/L 12/16/16 23:45 7440-50-812/14/16 21:4010.0 2.5 1
Lead ND ug/L 12/16/16 23:45 7439-92-112/14/16 21:4010.0 2.5 1
Nickel ND ug/L 12/16/16 23:45 7440-02-012/14/16 21:4050.0 2.5 1
Selenium ND ug/L 12/16/16 23:45 7782-49-212/14/16 21:4010.0 5.0 1
Silver ND ug/L 12/16/16 23:45 7440-22-412/14/16 21:4010.0 2.5 1
Thallium ND ug/L 12/16/16 23:45 7440-28-012/14/16 21:405.5 5.0 1
Vanadium ND ug/L 12/16/16 23:45 7440-62-212/14/16 21:4025.0 2.5 1
Zinc 11.9 ug/L 12/16/16 23:45 7440-66-612/14/16 21:4010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/07/16 19:08 67-64-110010.0 1
Acrylonitrile ND ug/L 12/07/16 19:08 107-13-12001.9 1
Benzene ND ug/L 12/07/16 19:08 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/07/16 19:08 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/07/16 19:08 75-27-41.0 0.18 1
Bromoform ND ug/L 12/07/16 19:08 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/07/16 19:08 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/07/16 19:08 78-93-31000.96 1
Carbon disulfide ND ug/L 12/07/16 19:08 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/07/16 19:08 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/07/16 19:08 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/07/16 19:08 75-00-310.0 0.54 1
Chloroform ND ug/L 12/07/16 19:08 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/07/16 19:08 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/07/16 19:08 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/07/16 19:08 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/07/16 19:08 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/07/16 19:08 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/07/16 19:08 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/07/16 19:08 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/07/16 19:08 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/07/16 19:08 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/07/16 19:08 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/07/16 19:08 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.30J ug/L 12/07/16 19:08 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/07/16 19:08 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/07/16 19:08 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/07/16 19:08 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/07/16 19:08 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 03:36 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 11 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321701
Surry Closed-Mt Airy (AM)
Sample:SCALEHOUSE Lab ID:92321701004 Collected:12/03/16 11:50 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/07/16 19:08 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/07/16 19:08 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/07/16 19:08 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/07/16 19:08 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/07/16 19:08 108-10-11000.33 1
Styrene ND ug/L 12/07/16 19:08 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/07/16 19:08 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/07/16 19:08 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/07/16 19:08 127-18-41.0 0.46 1
Toluene ND ug/L 12/07/16 19:08 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/07/16 19:08 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/07/16 19:08 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/07/16 19:08 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/07/16 19:08 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/07/16 19:08 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/07/16 19:08 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/07/16 19:08 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/07/16 19:08 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %12/07/16 19:08 460-00-470-130 1
1,2-Dichloroethane-d4 (S)94 %12/07/16 19:08 17060-07-070-130 1
Toluene-d8 (S)112 %12/07/16 19:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 03:36 PM
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Huntersville, NC 28078
[phone]
Page 12 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321701
Surry Closed-Mt Airy (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
339341
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92321701001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1881715
Associated Lab Samples:92321701001
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 12/13/16 17:273.8
Arsenic ug/L ND 10.0 12/13/16 17:272.5
Barium ug/L ND 100 12/13/16 03:202.5
Beryllium ug/L ND 1.0 12/13/16 03:200.50
Cadmium ug/L ND 1.0 12/13/16 17:270.50
Chromium ug/L ND 10.0 12/13/16 03:202.5
Cobalt ug/L ND 10.0 12/13/16 17:272.5
Copper ug/L ND 10.0 12/13/16 17:272.5
Lead ug/L ND 10.0 12/13/16 03:202.5
Nickel ug/L ND 50.0 12/13/16 03:202.5
Selenium ug/L ND 10.0 12/13/16 17:275.0
Silver ug/L ND 10.0 12/13/16 03:202.5
Thallium ug/L ND 5.5 12/13/16 17:275.0
Vanadium ug/L ND 25.0 12/13/16 03:202.5
Zinc ug/L ND 10.0 12/13/16 03:205.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1881716LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 506500 101 80-120
Arsenic ug/L 491500 98 80-120
Barium ug/L 482500 96 80-120
Beryllium ug/L 498500 100 80-120
Cadmium ug/L 499500 100 80-120
Chromium ug/L 508500 102 80-120
Cobalt ug/L 510500 102 80-120
Copper ug/L 507500 101 80-120
Lead ug/L 477500 95 80-120
Nickel ug/L 474500 95 80-120
Selenium ug/L 503500 101 80-120
Silver ug/L 237250 95 80-120
Thallium ug/L 439500 88 80-120
Vanadium ug/L 487500 97 80-120
Zinc ug/L 513500 103 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 03:36 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321701
Surry Closed-Mt Airy (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1881717MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321678002
1881718
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 97 75-12597 0 25500ND483483
Arsenic ug/L 500 94 75-12593 1 25500ND468464
Barium ug/L 500 94 75-12598 3 2550030.4J 502 519
Beryllium ug/L 500 97 75-12597 0 25500ND488487
Cadmium ug/L 500 95 75-12596 1 25500ND478482
Chromium ug/L 500 100 75-12599 1 25500ND498494
Cobalt ug/L 500 97 75-12597 0 25500ND484486
Copper ug/L 500 98 75-12598 0 25500ND490493
Lead ug/L 500 92 75-12592 1 255003.4J 463 461
Nickel ug/L 500 92 75-12593 0 25500ND462463
Selenium ug/L 500 97 75-12597 1 25500ND487484
Silver ug/L 250 93 75-12593 0 25250ND232232
Thallium ug/L 500 85 75-12584 2 25500ND426419
Vanadium ug/L 500 95 75-12595 1 25500ND478475
Zinc ug/L 500 100 75-125100 1 25500ND504500
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 03:36 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321701
Surry Closed-Mt Airy (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
340698
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92321701002, 92321701003, 92321701004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1889943
Associated Lab Samples:92321701002, 92321701003, 92321701004
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 12/16/16 23:243.8
Arsenic ug/L ND 10.0 12/18/16 19:392.5
Barium ug/L ND 100 12/16/16 23:242.5
Beryllium ug/L ND 1.0 12/16/16 23:240.50
Cadmium ug/L ND 1.0 12/16/16 23:240.50
Chromium ug/L ND 10.0 12/16/16 23:242.5
Cobalt ug/L ND 10.0 12/16/16 23:242.5
Copper ug/L ND 10.0 12/16/16 23:242.5
Lead ug/L ND 10.0 12/16/16 23:242.5
Nickel ug/L ND 50.0 12/16/16 23:242.5
Selenium ug/L ND 10.0 12/16/16 23:245.0
Silver ug/L ND 10.0 12/16/16 23:242.5
Thallium ug/L ND 5.5 12/16/16 23:245.0
Vanadium ug/L ND 25.0 12/16/16 23:242.5
Zinc ug/L ND 10.0 12/16/16 23:245.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1889944LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 514500 103 80-120
Arsenic ug/L 508500 102 80-120
Barium ug/L 526500 105 80-120
Beryllium ug/L 495500 99 80-120
Cadmium ug/L 506500 101 80-120
Chromium ug/L 504500 101 80-120
Cobalt ug/L 524500 105 80-120
Copper ug/L 538500 108 80-120
Lead ug/L 520500 104 80-120
Nickel ug/L 494500 99 80-120
Selenium ug/L 526500 105 80-120
Silver ug/L 256250 103 80-120
Thallium ug/L 523500 105 80-120
Vanadium ug/L 496500 99 80-120
Zinc ug/L 522500 104 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 03:36 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321701
Surry Closed-Mt Airy (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1889945MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92322158002
1889946
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 102 75-125102 1 25500ND514511
Arsenic ug/L 500 99 75-125100 1 255003.4J 497 501
Barium ug/L 500 106 75-125105 1 25500ND530524
Beryllium ug/L 500 98 75-12598 0 25500ND489491
Cadmium ug/L 500 99 75-125100 0 25500ND497499
Chromium ug/L 500 99 75-125100 1 25500ND496502
Cobalt ug/L 500 105 75-125104 1 25500ND526520
Copper ug/L 500 105 75-125106 0 25500ND528530
Lead ug/L 500 104 75-125103 1 25500ND522517
Nickel ug/L 500 98 75-12598 0 25500ND488490
Selenium ug/L 500 104 75-125104 0 25500ND522519
Silver ug/L 250 100 75-125101 1 25250ND250253
Thallium ug/L 500 104 75-125105 1 25500ND522529
Vanadium ug/L 500 97 75-12598 1 25500ND486492
Zinc ug/L 500 104 75-125103 1 25500ND519516
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 03:36 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321701
Surry Closed-Mt Airy (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
339770
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92321701001, 92321701002, 92321701003, 92321701004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1884326
Associated Lab Samples:92321701001, 92321701002, 92321701003, 92321701004
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 12/07/16 14:240.33
1,1,1-Trichloroethane ug/L ND 1.0 12/07/16 14:240.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 12/07/16 14:240.40
1,1,2-Trichloroethane ug/L ND 1.0 12/07/16 14:240.29
1,1-Dichloroethane ug/L ND 5.0 12/07/16 14:240.32
1,1-Dichloroethene ug/L ND 5.0 12/07/16 14:240.56
1,2,3-Trichloropropane ug/L ND 1.0 12/07/16 14:240.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 12/07/16 14:242.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 12/07/16 14:240.27
1,2-Dichlorobenzene ug/L ND 5.0 12/07/16 14:240.30
1,2-Dichloroethane ug/L ND 1.0 12/07/16 14:240.24
1,2-Dichloropropane ug/L ND 1.0 12/07/16 14:240.27
1,4-Dichlorobenzene ug/L ND 1.0 12/07/16 14:240.33
2-Butanone (MEK)ug/L ND 100 12/07/16 14:240.96
2-Hexanone ug/L ND 50.0 12/07/16 14:240.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 12/07/16 14:240.33
Acetone ug/L ND 100 12/07/16 14:2410.0
Acrylonitrile ug/L ND 200 12/07/16 14:241.9
Benzene ug/L ND 1.0 12/07/16 14:240.25
Bromochloromethane ug/L ND 3.0 12/07/16 14:240.17
Bromodichloromethane ug/L ND 1.0 12/07/16 14:240.18
Bromoform ug/L ND 3.0 12/07/16 14:240.26
Bromomethane ug/L ND 10.0 12/07/16 14:240.29
Carbon disulfide ug/L ND 100 12/07/16 14:241.2
Carbon tetrachloride ug/L ND 1.0 12/07/16 14:240.25
Chlorobenzene ug/L ND 3.0 12/07/16 14:240.23
Chloroethane ug/L ND 10.0 12/07/16 14:240.54
Chloroform ug/L ND 5.0 12/07/16 14:240.14
Chloromethane ug/L ND 1.0 12/07/16 14:240.11
cis-1,2-Dichloroethene ug/L ND 5.0 12/07/16 14:240.19
cis-1,3-Dichloropropene ug/L ND 1.0 12/07/16 14:240.13
Dibromochloromethane ug/L ND 3.0 12/07/16 14:240.21
Dibromomethane ug/L ND 10.0 12/07/16 14:240.21
Ethylbenzene ug/L ND 1.0 12/07/16 14:240.30
Iodomethane ug/L ND 10.0 12/07/16 14:240.32
Methylene Chloride ug/L ND 1.0 12/07/16 14:240.97
Styrene ug/L ND 1.0 12/07/16 14:240.26
Tetrachloroethene ug/L ND 1.0 12/07/16 14:240.46
Toluene ug/L ND 1.0 12/07/16 14:240.26
trans-1,2-Dichloroethene ug/L ND 5.0 12/07/16 14:240.49
trans-1,3-Dichloropropene ug/L ND 1.0 12/07/16 14:240.26
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 03:36 PM
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Page 17 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321701
Surry Closed-Mt Airy (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1884326
Associated Lab Samples:92321701001, 92321701002, 92321701003, 92321701004
Matrix:Water
AnalyzedMDL
trans-1,4-Dichloro-2-butene ug/L ND 100 12/07/16 14:241.0
Trichloroethene ug/L ND 1.0 12/07/16 14:240.47
Trichlorofluoromethane ug/L ND 1.0 12/07/16 14:240.20
Vinyl acetate ug/L ND 50.0 12/07/16 14:240.35
Vinyl chloride ug/L ND 1.0 12/07/16 14:240.62
Xylene (Total)ug/L ND 5.0 12/07/16 14:240.66
1,2-Dichloroethane-d4 (S)%91 70-130 12/07/16 14:24
4-Bromofluorobenzene (S)%98 70-130 12/07/16 14:24
Toluene-d8 (S)%107 70-130 12/07/16 14:24
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1884327LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.150 100 80-125
1,1,1-Trichloroethane ug/L 48.650 97 71-129
1,1,2,2-Tetrachloroethane ug/L 48.450 97 79-124
1,1,2-Trichloroethane ug/L 47.450 95 85-125
1,1-Dichloroethane ug/L 46.550 93 73-126
1,1-Dichloroethene ug/L 49.150 98 66-135
1,2,3-Trichloropropane ug/L 47.850 96 75-130
1,2-Dibromo-3-chloropropane ug/L 44.450 89 71-133
1,2-Dibromoethane (EDB)ug/L 50.350 101 83-124
1,2-Dichlorobenzene ug/L 47.450 95 80-133
1,2-Dichloroethane ug/L 44.150 88 67-128
1,2-Dichloropropane ug/L 46.650 93 75-132
1,4-Dichlorobenzene ug/L 47.750 95 78-130
2-Butanone (MEK)ug/L 98.7J100 99 61-144
2-Hexanone ug/L 92.2100 92 68-143
4-Methyl-2-pentanone (MIBK)ug/L 87.4J100 87 72-135
Acetone ug/L 97.1J100 97 48-146
Acrylonitrile ug/L 229250 92 40-160
Benzene ug/L 49.150 98 80-125
Bromochloromethane ug/L 48.250 96 71-125
Bromodichloromethane ug/L 49.550 99 78-124
Bromoform ug/L 42.150 84 71-128
Bromomethane ug/L 48.350 97 40-160
Carbon disulfide ug/L 45.9J50 92 50-160
Carbon tetrachloride ug/L 50.450 101 69-131
Chlorobenzene ug/L 47.150 94 81-122
Chloroethane ug/L 49.850 100 39-148
Chloroform ug/L 46.150 92 73-127
Chloromethane ug/L 47.750 95 44-146
cis-1,2-Dichloroethene ug/L 45.950 92 74-124
cis-1,3-Dichloropropene ug/L 50.150 100 72-132
REPORT OF LABORATORY ANALYSIS
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Page 18 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321701
Surry Closed-Mt Airy (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1884327LABORATORY CONTROL SAMPLE:
LCSSpike
Dibromochloromethane ug/L 52.450 105 78-125
Dibromomethane ug/L 46.950 94 82-120
Ethylbenzene ug/L 47.150 94 79-121
Iodomethane ug/L 87.5100 87 39-154
Methylene Chloride ug/L 48.850 98 64-133
Styrene ug/L 47.350 95 84-126
Tetrachloroethene ug/L 46.250 92 78-122
Toluene ug/L 46.350 93 80-121
trans-1,2-Dichloroethene ug/L 47.750 95 71-127
trans-1,3-Dichloropropene ug/L 47.950 96 69-141
trans-1,4-Dichloro-2-butene ug/L 44.0J50 88 40-160
Trichloroethene ug/L 49.550 99 78-122
Trichlorofluoromethane ug/L 55.750 111 53-137
Vinyl acetate ug/L 102100 102 40-160
Vinyl chloride ug/L 44.650 89 58-137
Xylene (Total)ug/L 143150 95 81-126
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1884329MATRIX SPIKE SAMPLE:
MSSpike
Result
92321720005
1,1,1,2-Tetrachloroethane ug/L 19.720 98 70-130ND
1,1,1-Trichloroethane ug/L 21.820 109 70-130ND
1,1,2,2-Tetrachloroethane ug/L 18.620 93 70-130ND
1,1,2-Trichloroethane ug/L 20.020 100 70-130ND
1,1-Dichloroethane ug/L 20.320 102 70-130ND
1,1-Dichloroethene ug/L 23.020 115 70-166ND
1,2,3-Trichloropropane ug/L 18.020 90 70-130ND
1,2-Dibromo-3-chloropropane ug/L 17.720 89 70-130ND
1,2-Dibromoethane (EDB)ug/L 19.220 96 70-130ND
1,2-Dichlorobenzene ug/L 20.020 100 70-130ND
1,2-Dichloroethane ug/L 19.620 98 70-130ND
1,2-Dichloropropane ug/L 20.120 100 70-130ND
1,4-Dichlorobenzene ug/L 21.220 100 70-1301.3
2-Butanone (MEK)ug/L 32.3J40 81 70-130ND
2-Hexanone ug/L 33.9J40 85 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 35.1J40 88 70-130ND
Acetone ug/L 32.7J40 82 70-130ND
Acrylonitrile ug/L 90.5J100 91 70-130ND
Benzene ug/L 21.720 109 70-148ND
Bromochloromethane ug/L 20.420 102 70-130ND
Bromodichloromethane ug/L 21.220 106 70-130ND
Bromoform ug/L 17.220 86 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 03:36 PM
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Page 19 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321701
Surry Closed-Mt Airy (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1884329MATRIX SPIKE SAMPLE:
MSSpike
Result
92321720005
Bromomethane ug/L 15.420 77 70-130ND
Carbon disulfide ug/L 21.9J20 110 70-130ND
Carbon tetrachloride ug/L 23.220 116 70-130ND
Chlorobenzene ug/L 22.420 100 70-1462.4J
Chloroethane ug/L 23.820 119 70-130ND
Chloroform ug/L 20.420 102 70-130ND
Chloromethane ug/L 20.720 103 70-130ND
cis-1,2-Dichloroethene ug/L 21.120 105 70-130ND
cis-1,3-Dichloropropene ug/L 19.620 98 70-130ND
Dibromochloromethane ug/L 19.920 100 70-130ND
Dibromomethane ug/L 20.220 101 70-130ND
Ethylbenzene ug/L 20.220 101 70-130ND
Iodomethane ug/L 38.440 96 70-130ND
Methylene Chloride ug/L 21.020 105 70-130ND
Styrene ug/L 20.120 100 70-130ND
Tetrachloroethene ug/L 19.520 98 70-130ND
Toluene ug/L 21.020 105 70-155ND
trans-1,2-Dichloroethene ug/L 22.020 110 70-130ND
trans-1,3-Dichloropropene ug/L 18.620 93 70-130ND
trans-1,4-Dichloro-2-butene ug/L 17.2J20 86 70-130ND
Trichloroethene ug/L 21.220 106 69-151ND
Trichlorofluoromethane ug/L 25.820 129 70-130ND
Vinyl acetate ug/L 30.7J40 77 70-130ND
Vinyl chloride ug/L 19.420 97 70-130ND
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92321720004
1884328SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 03:36 PM
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Page 20 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321701
Surry Closed-Mt Airy (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92321720004
1884328SAMPLE DUPLICATE:
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%96 096
4-Bromofluorobenzene (S)%98 199
Toluene-d8 (S)%103 4108
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 03:36 PM
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Page 21 of 29
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92321701
Surry Closed-Mt Airy (AM)
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
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Page 22 of 29
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92321701
Surry Closed-Mt Airy (AM)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92321701001 339341 339662MW-12D EPA 3010A EPA 6010
92321701002 340698 340963MW-6 EPA 3010A EPA 6010
92321701003 340698 340963MW-11 EPA 3010A EPA 6010
92321701004 340698 340963SCALEHOUSEEPA 3010A EPA 6010
92321701001 339770MW-12D EPA 8260
92321701002 339770MW-6 EPA 8260
92321701003 339770MW-11 EPA 8260
92321701004 339770SCALEHOUSEEPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 03:36 PM
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[phone]
Page 23 of 29
Page 24 of 29
Page 25 of 29
Page 26 of 29
Page 27 of 29
Page 28 of 29
Page 29 of 29
#=CL#
December 19, 2016
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92321720
92321720
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
Surry Closed- Mt Airy (UIC)
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory between December 02,
2016 and December 06, 2016. The results relate only to the samples included in this report. Results
reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's
Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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Page 1 of 66
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
Greenwood Certification IDs
816 Durst Avenue East, Greenwood, SC 29649
South Carolina Laboratory ID #: 24562
North Carolina Divison of Water Resources Certification
number 25
Florida Certification number E87633
Virginia VELAP ID: 460250
Asbestos NVLAP accreditation: 101410-0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Lab ID Sample ID Matrix Date Collected Date Received
92321720001 MW-3R Water 12/01/16 11:50 12/02/16 07:09
92321720002 MW-12S Water 12/01/16 14:00 12/02/16 07:09
92321720003 MW-15 Water 12/01/16 16:00 12/02/16 07:09
92321720004 MW-1 Water 12/03/16 11:10 12/06/16 08:31
92321720005 MW-7 Water 12/03/16 10:05 12/06/16 08:31
92321720006 MW-9 Water 12/02/16 16:00 12/06/16 08:31
92321720008 MW-13 Water 12/02/16 13:00 12/06/16 08:31
92321720009 MW-14 Water 12/02/16 14:00 12/06/16 08:31
92321720011 MW-16 Water 12/02/16 11:50 12/06/16 08:31
92321720012 MW-17 Water 12/02/16 12:05 12/06/16 08:31
92321720013 MW-18 Water 12/02/16 09:15 12/06/16 08:31
92321720014 MW-19 Water 12/02/16 10:00 12/06/16 08:31
92321720015 MW-20 Water 12/02/16 15:30 12/06/16 08:31
92321720016 MW-21 Water 12/02/16 17:00 12/06/16 08:31
92321720017 MW-22 Water 12/02/16 10:40 12/06/16 08:31
92321720018 MW-23 Water 12/02/16 11:30 12/06/16 08:31
REPORT OF LABORATORY ANALYSIS
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Page 3 of 66
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92321720001 MW-3R EPA 6010 15 PASI-AJMW
EPA 8260 50 PASI-CGAW
92321720002 MW-12S EPA 6010 15 PASI-AJMW
EPA 8260 50 PASI-CGAW
92321720003 MW-15 EPA 6010 15 PASI-AJMW
EPA 8260 50 PASI-CGAW
92321720004 MW-1 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 50 PASI-CGAW
92321720005 MW-7 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 50 PASI-CGAW
92321720006 MW-9 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 50 PASI-CGAW
92321720008 MW-13 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 50 PASI-CGAW
92321720009 MW-14 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 50 PASI-CGAW
92321720011 MW-16 EPA 9056A 1 PASI-WCDC
EPA 6010 15 PASI-AJMW, SH1
EPA 8260 50 PASI-CGAW
92321720012 MW-17 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 50 PASI-CGAW
92321720013 MW-18 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 50 PASI-CGAW
92321720014 MW-19 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 50 PASI-CGAW
92321720015 MW-20 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 50 PASI-CGAW
92321720016 MW-21 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 50 PASI-CGAW
92321720017 MW-22 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 50 PASI-CGAW
92321720018 MW-23 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Sample:MW-3R Lab ID:92321720001 Collected:12/01/16 11:50 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/13/16 13:32 7440-36-012/09/16 04:356.0 3.8 1
Arsenic ND ug/L 12/13/16 13:32 7440-38-212/09/16 04:3510.0 2.5 1
Barium 7.2J ug/L 12/13/16 13:32 7440-39-312/09/16 04:351002.5 1
Beryllium ND ug/L 12/13/16 13:32 7440-41-712/09/16 04:351.0 0.50 1
Cadmium 1.0 ug/L 12/13/16 13:32 7440-43-912/09/16 04:351.0 0.50 1
Chromium ND ug/L 12/13/16 13:32 7440-47-312/09/16 04:3510.0 2.5 1
Cobalt ND ug/L 12/13/16 13:32 7440-48-412/09/16 04:3510.0 2.5 1
Copper ND ug/L 12/13/16 13:32 7440-50-812/09/16 04:3510.0 2.5 1
Lead ND ug/L 12/13/16 13:32 7439-92-112/09/16 04:3510.0 2.5 1
Nickel ND ug/L 12/13/16 13:32 7440-02-012/09/16 04:3550.0 2.5 1
Selenium ND ug/L 12/13/16 13:32 7782-49-212/09/16 04:3510.0 5.0 1
Silver ND ug/L 12/13/16 13:32 7440-22-412/09/16 04:3510.0 2.5 1
Thallium ND ug/L 12/13/16 13:32 7440-28-012/09/16 04:355.5 5.0 1
Vanadium ND ug/L 12/13/16 13:32 7440-62-212/09/16 04:3525.0 2.5 1
Zinc ND ug/L 12/13/16 13:32 7440-66-612/09/16 04:3510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/07/16 19:26 67-64-110010.0 1
Acrylonitrile ND ug/L 12/07/16 19:26 107-13-12001.9 1
Benzene ND ug/L 12/07/16 19:26 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/07/16 19:26 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/07/16 19:26 75-27-41.0 0.18 1
Bromoform ND ug/L 12/07/16 19:26 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/07/16 19:26 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/07/16 19:26 78-93-31000.96 1
Carbon disulfide ND ug/L 12/07/16 19:26 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/07/16 19:26 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/07/16 19:26 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/07/16 19:26 75-00-310.0 0.54 1
Chloroform ND ug/L 12/07/16 19:26 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/07/16 19:26 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/07/16 19:26 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/07/16 19:26 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/07/16 19:26 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/07/16 19:26 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/07/16 19:26 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/07/16 19:26 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/07/16 19:26 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/07/16 19:26 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/07/16 19:26 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/07/16 19:26 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/07/16 19:26 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/07/16 19:26 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/07/16 19:26 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/07/16 19:26 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/07/16 19:26 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 66
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Sample:MW-3R Lab ID:92321720001 Collected:12/01/16 11:50 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/07/16 19:26 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/07/16 19:26 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/07/16 19:26 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/07/16 19:26 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/07/16 19:26 108-10-11000.33 1
Styrene ND ug/L 12/07/16 19:26 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/07/16 19:26 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/07/16 19:26 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/07/16 19:26 127-18-41.0 0.46 1
Toluene ND ug/L 12/07/16 19:26 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/07/16 19:26 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/07/16 19:26 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/07/16 19:26 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/07/16 19:26 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/07/16 19:26 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/07/16 19:26 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/07/16 19:26 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/07/16 19:26 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %12/07/16 19:26 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %12/07/16 19:26 17060-07-070-130 1
Toluene-d8 (S)109 %12/07/16 19:26 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 66
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Sample:MW-12S Lab ID:92321720002 Collected:12/01/16 14:00 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/13/16 13:36 7440-36-012/09/16 04:356.0 3.8 1
Arsenic 2.6J ug/L 12/13/16 13:36 7440-38-2 B12/09/16 04:3510.0 2.5 1
Barium 17.8J ug/L 12/13/16 13:36 7440-39-312/09/16 04:351002.5 1
Beryllium ND ug/L 12/13/16 13:36 7440-41-712/09/16 04:351.0 0.50 1
Cadmium ND ug/L 12/13/16 13:36 7440-43-912/09/16 04:351.0 0.50 1
Chromium 2.6J ug/L 12/13/16 13:36 7440-47-312/09/16 04:3510.0 2.5 1
Cobalt ND ug/L 12/13/16 13:36 7440-48-412/09/16 04:3510.0 2.5 1
Copper ND ug/L 12/13/16 13:36 7440-50-812/09/16 04:3510.0 2.5 1
Lead ND ug/L 12/13/16 13:36 7439-92-112/09/16 04:3510.0 2.5 1
Nickel ND ug/L 12/13/16 13:36 7440-02-012/09/16 04:3550.0 2.5 1
Selenium ND ug/L 12/13/16 13:36 7782-49-212/09/16 04:3510.0 5.0 1
Silver ND ug/L 12/13/16 13:36 7440-22-412/09/16 04:3510.0 2.5 1
Thallium ND ug/L 12/13/16 13:36 7440-28-012/09/16 04:355.5 5.0 1
Vanadium ND ug/L 12/13/16 13:36 7440-62-212/09/16 04:3525.0 2.5 1
Zinc ND ug/L 12/13/16 13:36 7440-66-612/09/16 04:3510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/07/16 19:44 67-64-110010.0 1
Acrylonitrile ND ug/L 12/07/16 19:44 107-13-12001.9 1
Benzene ND ug/L 12/07/16 19:44 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/07/16 19:44 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/07/16 19:44 75-27-41.0 0.18 1
Bromoform ND ug/L 12/07/16 19:44 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/07/16 19:44 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/07/16 19:44 78-93-31000.96 1
Carbon disulfide ND ug/L 12/07/16 19:44 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/07/16 19:44 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/07/16 19:44 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/07/16 19:44 75-00-310.0 0.54 1
Chloroform ND ug/L 12/07/16 19:44 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/07/16 19:44 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/07/16 19:44 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/07/16 19:44 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/07/16 19:44 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/07/16 19:44 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/07/16 19:44 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/07/16 19:44 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/07/16 19:44 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/07/16 19:44 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/07/16 19:44 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/07/16 19:44 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/07/16 19:44 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/07/16 19:44 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/07/16 19:44 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/07/16 19:44 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/07/16 19:44 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 66
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Sample:MW-12S Lab ID:92321720002 Collected:12/01/16 14:00 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/07/16 19:44 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/07/16 19:44 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/07/16 19:44 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/07/16 19:44 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/07/16 19:44 108-10-11000.33 1
Styrene ND ug/L 12/07/16 19:44 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/07/16 19:44 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/07/16 19:44 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/07/16 19:44 127-18-41.0 0.46 1
Toluene ND ug/L 12/07/16 19:44 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/07/16 19:44 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/07/16 19:44 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/07/16 19:44 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/07/16 19:44 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/07/16 19:44 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/07/16 19:44 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/07/16 19:44 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/07/16 19:44 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %12/07/16 19:44 460-00-470-130 1
1,2-Dichloroethane-d4 (S)90 %12/07/16 19:44 17060-07-070-130 1
Toluene-d8 (S)116 %12/07/16 19:44 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 66
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Sample:MW-15 Lab ID:92321720003 Collected:12/01/16 16:00 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/13/16 13:39 7440-36-012/09/16 04:356.0 3.8 1
Arsenic 3.1J ug/L 12/13/16 13:39 7440-38-2 B12/09/16 04:3510.0 2.5 1
Barium 20.6J ug/L 12/13/16 13:39 7440-39-312/09/16 04:351002.5 1
Beryllium ND ug/L 12/13/16 13:39 7440-41-712/09/16 04:351.0 0.50 1
Cadmium ND ug/L 12/13/16 13:39 7440-43-912/09/16 04:351.0 0.50 1
Chromium ND ug/L 12/13/16 13:39 7440-47-312/09/16 04:3510.0 2.5 1
Cobalt ND ug/L 12/13/16 13:39 7440-48-412/09/16 04:3510.0 2.5 1
Copper ND ug/L 12/13/16 13:39 7440-50-812/09/16 04:3510.0 2.5 1
Lead ND ug/L 12/13/16 13:39 7439-92-112/09/16 04:3510.0 2.5 1
Nickel ND ug/L 12/13/16 13:39 7440-02-012/09/16 04:3550.0 2.5 1
Selenium ND ug/L 12/13/16 13:39 7782-49-212/09/16 04:3510.0 5.0 1
Silver ND ug/L 12/13/16 13:39 7440-22-412/09/16 04:3510.0 2.5 1
Thallium ND ug/L 12/13/16 13:39 7440-28-012/09/16 04:355.5 5.0 1
Vanadium 2.6J ug/L 12/13/16 13:39 7440-62-212/09/16 04:3525.0 2.5 1
Zinc ND ug/L 12/13/16 13:39 7440-66-612/09/16 04:3510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/07/16 20:01 67-64-110010.0 1
Acrylonitrile ND ug/L 12/07/16 20:01 107-13-12001.9 1
Benzene 0.76J ug/L 12/07/16 20:01 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/07/16 20:01 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/07/16 20:01 75-27-41.0 0.18 1
Bromoform ND ug/L 12/07/16 20:01 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/07/16 20:01 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/07/16 20:01 78-93-31000.96 1
Carbon disulfide ND ug/L 12/07/16 20:01 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/07/16 20:01 56-23-51.0 0.25 1
Chlorobenzene 2.0J ug/L 12/07/16 20:01 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/07/16 20:01 75-00-310.0 0.54 1
Chloroform ND ug/L 12/07/16 20:01 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/07/16 20:01 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/07/16 20:01 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/07/16 20:01 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/07/16 20:01 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/07/16 20:01 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/07/16 20:01 95-50-15.0 0.30 1
1,4-Dichlorobenzene 3.1 ug/L 12/07/16 20:01 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/07/16 20:01 110-57-61001.0 1
1,1-Dichloroethane 8.2 ug/L 12/07/16 20:01 75-34-35.0 0.32 1
1,2-Dichloroethane 0.51J ug/L 12/07/16 20:01 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/07/16 20:01 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 27.7 ug/L 12/07/16 20:01 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/07/16 20:01 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/07/16 20:01 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/07/16 20:01 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/07/16 20:01 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 66
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Sample:MW-15 Lab ID:92321720003 Collected:12/01/16 16:00 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/07/16 20:01 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/07/16 20:01 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/07/16 20:01 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/07/16 20:01 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/07/16 20:01 108-10-11000.33 1
Styrene ND ug/L 12/07/16 20:01 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/07/16 20:01 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/07/16 20:01 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/07/16 20:01 127-18-41.0 0.46 1
Toluene ND ug/L 12/07/16 20:01 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/07/16 20:01 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/07/16 20:01 79-00-51.0 0.29 1
Trichloroethene 1.9 ug/L 12/07/16 20:01 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/07/16 20:01 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/07/16 20:01 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/07/16 20:01 108-05-450.0 0.35 1
Vinyl chloride 1.5 ug/L 12/07/16 20:01 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/07/16 20:01 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %12/07/16 20:01 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %12/07/16 20:01 17060-07-070-130 1
Toluene-d8 (S)106 %12/07/16 20:01 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 66
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Sample:MW-1 Lab ID:92321720004 Collected:12/03/16 11:10 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/16/16 23:48 7440-36-012/14/16 21:406.0 3.8 1
Arsenic 2.7J ug/L 12/18/16 20:13 7440-38-212/14/16 21:4010.0 2.5 1
Barium 289 ug/L 12/16/16 23:48 7440-39-312/14/16 21:401002.5 1
Beryllium ND ug/L 12/16/16 23:48 7440-41-712/14/16 21:401.0 0.50 1
Cadmium 6.8 ug/L 12/16/16 23:48 7440-43-912/14/16 21:401.0 0.50 1
Chromium 5.8J ug/L 12/16/16 23:48 7440-47-312/14/16 21:4010.0 2.5 1
Cobalt 12.0 ug/L 12/16/16 23:48 7440-48-412/14/16 21:4010.0 2.5 1
Copper 7.0J ug/L 12/16/16 23:48 7440-50-812/14/16 21:4010.0 2.5 1
Lead 3.4J ug/L 12/16/16 23:48 7439-92-112/14/16 21:4010.0 2.5 1
Nickel 8.7J ug/L 12/16/16 23:48 7440-02-012/14/16 21:4050.0 2.5 1
Selenium ND ug/L 12/16/16 23:48 7782-49-212/14/16 21:4010.0 5.0 1
Silver ND ug/L 12/16/16 23:48 7440-22-412/14/16 21:4010.0 2.5 1
Thallium ND ug/L 12/16/16 23:48 7440-28-012/14/16 21:405.5 5.0 1
Vanadium ND ug/L 12/16/16 23:48 7440-62-212/14/16 21:4025.0 2.5 1
Zinc 113 ug/L 12/16/16 23:48 7440-66-612/14/16 21:4010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/07/16 20:19 67-64-110010.0 1
Acrylonitrile ND ug/L 12/07/16 20:19 107-13-12001.9 1
Benzene ND ug/L 12/07/16 20:19 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/07/16 20:19 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/07/16 20:19 75-27-41.0 0.18 1
Bromoform ND ug/L 12/07/16 20:19 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/07/16 20:19 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/07/16 20:19 78-93-31000.96 1
Carbon disulfide ND ug/L 12/07/16 20:19 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/07/16 20:19 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/07/16 20:19 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/07/16 20:19 75-00-310.0 0.54 1
Chloroform ND ug/L 12/07/16 20:19 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/07/16 20:19 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/07/16 20:19 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/07/16 20:19 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/07/16 20:19 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/07/16 20:19 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/07/16 20:19 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/07/16 20:19 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/07/16 20:19 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/07/16 20:19 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/07/16 20:19 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/07/16 20:19 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/07/16 20:19 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/07/16 20:19 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/07/16 20:19 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/07/16 20:19 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/07/16 20:19 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 66
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Sample:MW-1 Lab ID:92321720004 Collected:12/03/16 11:10 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/07/16 20:19 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/07/16 20:19 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/07/16 20:19 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/07/16 20:19 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/07/16 20:19 108-10-11000.33 1
Styrene ND ug/L 12/07/16 20:19 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/07/16 20:19 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/07/16 20:19 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/07/16 20:19 127-18-41.0 0.46 1
Toluene ND ug/L 12/07/16 20:19 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/07/16 20:19 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/07/16 20:19 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/07/16 20:19 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/07/16 20:19 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/07/16 20:19 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/07/16 20:19 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/07/16 20:19 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/07/16 20:19 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %12/07/16 20:19 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %12/07/16 20:19 17060-07-070-130 1
Toluene-d8 (S)108 %12/07/16 20:19 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 66
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Sample:MW-7 Lab ID:92321720005 Collected:12/03/16 10:05 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/16/16 23:52 7440-36-012/14/16 21:406.0 3.8 1
Arsenic ND ug/L 12/18/16 20:17 7440-38-212/14/16 21:4010.0 2.5 1
Barium 61.8J ug/L 12/16/16 23:52 7440-39-312/14/16 21:401002.5 1
Beryllium ND ug/L 12/16/16 23:52 7440-41-712/14/16 21:401.0 0.50 1
Cadmium ND ug/L 12/16/16 23:52 7440-43-912/14/16 21:401.0 0.50 1
Chromium ND ug/L 12/16/16 23:52 7440-47-312/14/16 21:4010.0 2.5 1
Cobalt 54.2 ug/L 12/16/16 23:52 7440-48-412/14/16 21:4010.0 2.5 1
Copper ND ug/L 12/16/16 23:52 7440-50-812/14/16 21:4010.0 2.5 1
Lead ND ug/L 12/16/16 23:52 7439-92-112/14/16 21:4010.0 2.5 1
Nickel ND ug/L 12/16/16 23:52 7440-02-012/14/16 21:4050.0 2.5 1
Selenium ND ug/L 12/16/16 23:52 7782-49-212/14/16 21:4010.0 5.0 1
Silver ND ug/L 12/16/16 23:52 7440-22-412/14/16 21:4010.0 2.5 1
Thallium ND ug/L 12/16/16 23:52 7440-28-012/14/16 21:405.5 5.0 1
Vanadium ND ug/L 12/16/16 23:52 7440-62-212/14/16 21:4025.0 2.5 1
Zinc 8.7J ug/L 12/16/16 23:52 7440-66-612/14/16 21:4010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/07/16 20:55 67-64-110010.0 1
Acrylonitrile ND ug/L 12/07/16 20:55 107-13-12001.9 1
Benzene ND ug/L 12/07/16 20:55 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/07/16 20:55 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/07/16 20:55 75-27-41.0 0.18 1
Bromoform ND ug/L 12/07/16 20:55 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/07/16 20:55 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/07/16 20:55 78-93-31000.96 1
Carbon disulfide ND ug/L 12/07/16 20:55 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/07/16 20:55 56-23-51.0 0.25 1
Chlorobenzene 2.4J ug/L 12/07/16 20:55 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/07/16 20:55 75-00-310.0 0.54 1
Chloroform ND ug/L 12/07/16 20:55 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/07/16 20:55 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/07/16 20:55 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/07/16 20:55 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/07/16 20:55 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/07/16 20:55 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/07/16 20:55 95-50-15.0 0.30 1
1,4-Dichlorobenzene 1.3 ug/L 12/07/16 20:55 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/07/16 20:55 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/07/16 20:55 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/07/16 20:55 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/07/16 20:55 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/07/16 20:55 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/07/16 20:55 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/07/16 20:55 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/07/16 20:55 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/07/16 20:55 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 66
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Sample:MW-7 Lab ID:92321720005 Collected:12/03/16 10:05 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/07/16 20:55 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/07/16 20:55 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/07/16 20:55 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/07/16 20:55 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/07/16 20:55 108-10-11000.33 1
Styrene ND ug/L 12/07/16 20:55 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/07/16 20:55 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/07/16 20:55 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/07/16 20:55 127-18-41.0 0.46 1
Toluene ND ug/L 12/07/16 20:55 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/07/16 20:55 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/07/16 20:55 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/07/16 20:55 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/07/16 20:55 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/07/16 20:55 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/07/16 20:55 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/07/16 20:55 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/07/16 20:55 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %12/07/16 20:55 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %12/07/16 20:55 17060-07-070-130 1
Toluene-d8 (S)106 %12/07/16 20:55 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 66
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Sample:MW-9 Lab ID:92321720006 Collected:12/02/16 16:00 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/17/16 00:04 7440-36-012/14/16 21:406.0 3.8 1
Arsenic ND ug/L 12/18/16 20:20 7440-38-212/14/16 21:4010.0 2.5 1
Barium 55.3J ug/L 12/17/16 00:04 7440-39-312/14/16 21:401002.5 1
Beryllium ND ug/L 12/17/16 00:04 7440-41-712/14/16 21:401.0 0.50 1
Cadmium ND ug/L 12/17/16 00:04 7440-43-912/14/16 21:401.0 0.50 1
Chromium 3.0J ug/L 12/17/16 00:04 7440-47-312/14/16 21:4010.0 2.5 1
Cobalt 174 ug/L 12/17/16 00:04 7440-48-412/14/16 21:4010.0 2.5 1
Copper ND ug/L 12/17/16 00:04 7440-50-812/14/16 21:4010.0 2.5 1
Lead ND ug/L 12/17/16 00:04 7439-92-112/14/16 21:4010.0 2.5 1
Nickel 5.4J ug/L 12/17/16 00:04 7440-02-012/14/16 21:4050.0 2.5 1
Selenium ND ug/L 12/17/16 00:04 7782-49-212/14/16 21:4010.0 5.0 1
Silver ND ug/L 12/17/16 00:04 7440-22-412/14/16 21:4010.0 2.5 1
Thallium 6.4 ug/L 12/17/16 00:04 7440-28-012/14/16 21:405.5 5.0 1
Vanadium ND ug/L 12/17/16 00:04 7440-62-212/14/16 21:4025.0 2.5 1
Zinc 8.1J ug/L 12/17/16 00:04 7440-66-612/14/16 21:4010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/07/16 21:12 67-64-110010.0 1
Acrylonitrile ND ug/L 12/07/16 21:12 107-13-12001.9 1
Benzene 1.5 ug/L 12/07/16 21:12 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/07/16 21:12 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/07/16 21:12 75-27-41.0 0.18 1
Bromoform ND ug/L 12/07/16 21:12 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/07/16 21:12 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/07/16 21:12 78-93-31000.96 1
Carbon disulfide ND ug/L 12/07/16 21:12 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/07/16 21:12 56-23-51.0 0.25 1
Chlorobenzene 1.4J ug/L 12/07/16 21:12 108-90-73.0 0.23 1
Chloroethane 3.5J ug/L 12/07/16 21:12 75-00-310.0 0.54 1
Chloroform ND ug/L 12/07/16 21:12 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/07/16 21:12 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/07/16 21:12 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/07/16 21:12 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/07/16 21:12 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/07/16 21:12 74-95-310.0 0.21 1
1,2-Dichlorobenzene 1.1J ug/L 12/07/16 21:12 95-50-15.0 0.30 1
1,4-Dichlorobenzene 4.5 ug/L 12/07/16 21:12 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/07/16 21:12 110-57-61001.0 1
1,1-Dichloroethane 1.5J ug/L 12/07/16 21:12 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/07/16 21:12 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/07/16 21:12 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 13.8 ug/L 12/07/16 21:12 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/07/16 21:12 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/07/16 21:12 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/07/16 21:12 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/07/16 21:12 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 66
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Sample:MW-9 Lab ID:92321720006 Collected:12/02/16 16:00 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/07/16 21:12 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/07/16 21:12 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/07/16 21:12 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/07/16 21:12 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/07/16 21:12 108-10-11000.33 1
Styrene ND ug/L 12/07/16 21:12 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/07/16 21:12 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/07/16 21:12 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/07/16 21:12 127-18-41.0 0.46 1
Toluene ND ug/L 12/07/16 21:12 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/07/16 21:12 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/07/16 21:12 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/07/16 21:12 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/07/16 21:12 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/07/16 21:12 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/07/16 21:12 108-05-450.0 0.35 1
Vinyl chloride 8.2 ug/L 12/07/16 21:12 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/07/16 21:12 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %12/07/16 21:12 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %12/07/16 21:12 17060-07-070-130 1
Toluene-d8 (S)107 %12/07/16 21:12 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 66
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Sample:MW-13 Lab ID:92321720008 Collected:12/02/16 13:00 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/17/16 00:07 7440-36-012/14/16 21:406.0 3.8 1
Arsenic ND ug/L 12/18/16 20:23 7440-38-212/14/16 21:4010.0 2.5 1
Barium 67.7J ug/L 12/17/16 00:07 7440-39-312/14/16 21:401002.5 1
Beryllium ND ug/L 12/17/16 00:07 7440-41-712/14/16 21:401.0 0.50 1
Cadmium ND ug/L 12/17/16 00:07 7440-43-912/14/16 21:401.0 0.50 1
Chromium 2.7J ug/L 12/17/16 00:07 7440-47-312/14/16 21:4010.0 2.5 1
Cobalt 6.8J ug/L 12/17/16 00:07 7440-48-412/14/16 21:4010.0 2.5 1
Copper ND ug/L 12/17/16 00:07 7440-50-812/14/16 21:4010.0 2.5 1
Lead ND ug/L 12/17/16 00:07 7439-92-112/14/16 21:4010.0 2.5 1
Nickel ND ug/L 12/17/16 00:07 7440-02-012/14/16 21:4050.0 2.5 1
Selenium ND ug/L 12/17/16 00:07 7782-49-212/14/16 21:4010.0 5.0 1
Silver ND ug/L 12/17/16 00:07 7440-22-412/14/16 21:4010.0 2.5 1
Thallium ND ug/L 12/17/16 00:07 7440-28-012/14/16 21:405.5 5.0 1
Vanadium ND ug/L 12/17/16 00:07 7440-62-212/14/16 21:4025.0 2.5 1
Zinc 12.1 ug/L 12/17/16 00:07 7440-66-612/14/16 21:4010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/07/16 21:30 67-64-110010.0 1
Acrylonitrile ND ug/L 12/07/16 21:30 107-13-12001.9 1
Benzene ND ug/L 12/07/16 21:30 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/07/16 21:30 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/07/16 21:30 75-27-41.0 0.18 1
Bromoform ND ug/L 12/07/16 21:30 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/07/16 21:30 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/07/16 21:30 78-93-31000.96 1
Carbon disulfide ND ug/L 12/07/16 21:30 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/07/16 21:30 56-23-51.0 0.25 1
Chlorobenzene 1.2J ug/L 12/07/16 21:30 108-90-73.0 0.23 1
Chloroethane 0.74J ug/L 12/07/16 21:30 75-00-310.0 0.54 1
Chloroform ND ug/L 12/07/16 21:30 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/07/16 21:30 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/07/16 21:30 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/07/16 21:30 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/07/16 21:30 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/07/16 21:30 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/07/16 21:30 95-50-15.0 0.30 1
1,4-Dichlorobenzene 3.5 ug/L 12/07/16 21:30 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/07/16 21:30 110-57-61001.0 1
1,1-Dichloroethane 3.6J ug/L 12/07/16 21:30 75-34-35.0 0.32 1
1,2-Dichloroethane 0.79J ug/L 12/07/16 21:30 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/07/16 21:30 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 21.0 ug/L 12/07/16 21:30 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/07/16 21:30 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/07/16 21:30 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/07/16 21:30 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/07/16 21:30 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 66
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Sample:MW-13 Lab ID:92321720008 Collected:12/02/16 13:00 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/07/16 21:30 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/07/16 21:30 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/07/16 21:30 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/07/16 21:30 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/07/16 21:30 108-10-11000.33 1
Styrene ND ug/L 12/07/16 21:30 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/07/16 21:30 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/07/16 21:30 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/07/16 21:30 127-18-41.0 0.46 1
Toluene ND ug/L 12/07/16 21:30 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/07/16 21:30 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/07/16 21:30 79-00-51.0 0.29 1
Trichloroethene 0.91J ug/L 12/07/16 21:30 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/07/16 21:30 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/07/16 21:30 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/07/16 21:30 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/07/16 21:30 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/07/16 21:30 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)96 %12/07/16 21:30 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %12/07/16 21:30 17060-07-070-130 1
Toluene-d8 (S)106 %12/07/16 21:30 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 66
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Sample:MW-14 Lab ID:92321720009 Collected:12/02/16 14:00 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/17/16 00:10 7440-36-012/14/16 21:406.0 3.8 1
Arsenic ND ug/L 12/18/16 20:26 7440-38-212/14/16 21:4010.0 2.5 1
Barium 32.9J ug/L 12/17/16 00:10 7440-39-312/14/16 21:401002.5 1
Beryllium ND ug/L 12/17/16 00:10 7440-41-712/14/16 21:401.0 0.50 1
Cadmium ND ug/L 12/17/16 00:10 7440-43-912/14/16 21:401.0 0.50 1
Chromium ND ug/L 12/17/16 00:10 7440-47-312/14/16 21:4010.0 2.5 1
Cobalt ND ug/L 12/17/16 00:10 7440-48-412/14/16 21:4010.0 2.5 1
Copper ND ug/L 12/17/16 00:10 7440-50-812/14/16 21:4010.0 2.5 1
Lead ND ug/L 12/17/16 00:10 7439-92-112/14/16 21:4010.0 2.5 1
Nickel ND ug/L 12/17/16 00:10 7440-02-012/14/16 21:4050.0 2.5 1
Selenium ND ug/L 12/17/16 00:10 7782-49-212/14/16 21:4010.0 5.0 1
Silver ND ug/L 12/17/16 00:10 7440-22-412/14/16 21:4010.0 2.5 1
Thallium ND ug/L 12/17/16 00:10 7440-28-012/14/16 21:405.5 5.0 1
Vanadium ND ug/L 12/17/16 00:10 7440-62-212/14/16 21:4025.0 2.5 1
Zinc ND ug/L 12/17/16 00:10 7440-66-612/14/16 21:4010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/07/16 21:48 67-64-110010.0 1
Acrylonitrile ND ug/L 12/07/16 21:48 107-13-12001.9 1
Benzene ND ug/L 12/07/16 21:48 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/07/16 21:48 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/07/16 21:48 75-27-41.0 0.18 1
Bromoform ND ug/L 12/07/16 21:48 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/07/16 21:48 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/07/16 21:48 78-93-31000.96 1
Carbon disulfide ND ug/L 12/07/16 21:48 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/07/16 21:48 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/07/16 21:48 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/07/16 21:48 75-00-310.0 0.54 1
Chloroform ND ug/L 12/07/16 21:48 67-66-35.0 0.14 1
Chloromethane 0.34J ug/L 12/07/16 21:48 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/07/16 21:48 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/07/16 21:48 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/07/16 21:48 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/07/16 21:48 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/07/16 21:48 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/07/16 21:48 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/07/16 21:48 110-57-61001.0 1
1,1-Dichloroethane 3.3J ug/L 12/07/16 21:48 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/07/16 21:48 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/07/16 21:48 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 6.1 ug/L 12/07/16 21:48 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/07/16 21:48 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/07/16 21:48 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/07/16 21:48 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/07/16 21:48 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 66
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Sample:MW-14 Lab ID:92321720009 Collected:12/02/16 14:00 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/07/16 21:48 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/07/16 21:48 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/07/16 21:48 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/07/16 21:48 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/07/16 21:48 108-10-11000.33 1
Styrene ND ug/L 12/07/16 21:48 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/07/16 21:48 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/07/16 21:48 79-34-53.0 0.40 1
Tetrachloroethene 0.57J ug/L 12/07/16 21:48 127-18-41.0 0.46 1
Toluene ND ug/L 12/07/16 21:48 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/07/16 21:48 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/07/16 21:48 79-00-51.0 0.29 1
Trichloroethene 0.59J ug/L 12/07/16 21:48 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/07/16 21:48 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/07/16 21:48 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/07/16 21:48 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/07/16 21:48 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/07/16 21:48 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %12/07/16 21:48 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %12/07/16 21:48 17060-07-070-130 1
Toluene-d8 (S)107 %12/07/16 21:48 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 66
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Sample:MW-16 Lab ID:92321720011 Collected:12/02/16 11:50 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 9056A9056 IC Anions 28 Days, GWD
Bromide 0.58 mg/L 12/12/16 21:50 24959-67-90.10 0.10 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/17/16 00:13 7440-36-012/14/16 21:406.0 3.8 1
Arsenic 2.9J ug/L 12/18/16 20:29 7440-38-212/14/16 21:4010.0 2.5 1
Barium 150 ug/L 12/17/16 00:13 7440-39-312/14/16 21:401002.5 1
Beryllium ND ug/L 12/17/16 00:13 7440-41-712/14/16 21:401.0 0.50 1
Cadmium 0.52J ug/L 12/17/16 00:13 7440-43-912/14/16 21:401.0 0.50 1
Chromium 10.7 ug/L 12/17/16 00:13 7440-47-312/14/16 21:4010.0 2.5 1
Cobalt 621 ug/L 12/17/16 00:13 7440-48-412/14/16 21:4010.0 2.5 1
Copper 6.2J ug/L 12/17/16 00:13 7440-50-812/14/16 21:4010.0 2.5 1
Lead 7.6J ug/L 12/17/16 00:13 7439-92-112/14/16 21:4010.0 2.5 1
Nickel 25.4J ug/L 12/17/16 00:13 7440-02-012/14/16 21:4050.0 2.5 1
Selenium ND ug/L 12/17/16 00:13 7782-49-212/14/16 21:4010.0 5.0 1
Silver ND ug/L 12/17/16 00:13 7440-22-412/14/16 21:4010.0 2.5 1
Thallium 21.0 ug/L 12/17/16 00:13 7440-28-012/14/16 21:405.5 5.0 1
Vanadium ND ug/L 12/17/16 00:13 7440-62-212/14/16 21:4025.0 2.5 1
Zinc 16.9 ug/L 12/17/16 00:13 7440-66-612/14/16 21:4010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/08/16 01:25 67-64-110010.0 1
Acrylonitrile ND ug/L 12/08/16 01:25 107-13-12001.9 1
Benzene 2.3 ug/L 12/08/16 01:25 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/08/16 01:25 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/08/16 01:25 75-27-41.0 0.18 1
Bromoform ND ug/L 12/08/16 01:25 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/08/16 01:25 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/08/16 01:25 78-93-31000.96 1
Carbon disulfide ND ug/L 12/08/16 01:25 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/08/16 01:25 56-23-51.0 0.25 1
Chlorobenzene 7.2 ug/L 12/08/16 01:25 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/08/16 01:25 75-00-310.0 0.54 1
Chloroform ND ug/L 12/08/16 01:25 67-66-35.0 0.14 1
Chloromethane 0.28J ug/L 12/08/16 01:25 74-87-3 B1.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/08/16 01:25 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/08/16 01:25 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/08/16 01:25 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/08/16 01:25 74-95-310.0 0.21 1
1,2-Dichlorobenzene 2.3J ug/L 12/08/16 01:25 95-50-15.0 0.30 1
1,4-Dichlorobenzene 17.9 ug/L 12/08/16 01:25 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/08/16 01:25 110-57-61001.0 1
1,1-Dichloroethane 1.9J ug/L 12/08/16 01:25 75-34-35.0 0.32 1
1,2-Dichloroethane 3.1 ug/L 12/08/16 01:25 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/08/16 01:25 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 41.9 ug/L 12/08/16 01:25 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/08/16 01:25 156-60-55.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 66
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Sample:MW-16 Lab ID:92321720011 Collected:12/02/16 11:50 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane 1.6 ug/L 12/08/16 01:25 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/08/16 01:25 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/08/16 01:25 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 12/08/16 01:25 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/08/16 01:25 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/08/16 01:25 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/08/16 01:25 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/08/16 01:25 108-10-11000.33 1
Styrene ND ug/L 12/08/16 01:25 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/08/16 01:25 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/08/16 01:25 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/08/16 01:25 127-18-41.0 0.46 1
Toluene ND ug/L 12/08/16 01:25 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/08/16 01:25 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/08/16 01:25 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/08/16 01:25 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/08/16 01:25 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/08/16 01:25 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/08/16 01:25 108-05-450.0 0.35 1
Vinyl chloride 4.5 ug/L 12/08/16 01:25 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/08/16 01:25 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %12/08/16 01:25 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %12/08/16 01:25 17060-07-070-130 1
Toluene-d8 (S)107 %12/08/16 01:25 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 66
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Sample:MW-17 Lab ID:92321720012 Collected:12/02/16 12:05 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/17/16 00:16 7440-36-012/14/16 21:406.0 3.8 1
Arsenic 2.6J ug/L 12/18/16 20:33 7440-38-212/14/16 21:4010.0 2.5 1
Barium 77.7J ug/L 12/17/16 00:16 7440-39-312/14/16 21:401002.5 1
Beryllium ND ug/L 12/17/16 00:16 7440-41-712/14/16 21:401.0 0.50 1
Cadmium ND ug/L 12/17/16 00:16 7440-43-912/14/16 21:401.0 0.50 1
Chromium 4.2J ug/L 12/17/16 00:16 7440-47-312/14/16 21:4010.0 2.5 1
Cobalt 31.7 ug/L 12/17/16 00:16 7440-48-412/14/16 21:4010.0 2.5 1
Copper ND ug/L 12/17/16 00:16 7440-50-812/14/16 21:4010.0 2.5 1
Lead ND ug/L 12/17/16 00:16 7439-92-112/14/16 21:4010.0 2.5 1
Nickel 7.5J ug/L 12/17/16 00:16 7440-02-012/14/16 21:4050.0 2.5 1
Selenium ND ug/L 12/17/16 00:16 7782-49-212/14/16 21:4010.0 5.0 1
Silver ND ug/L 12/17/16 00:16 7440-22-412/14/16 21:4010.0 2.5 1
Thallium 6.3 ug/L 12/17/16 00:16 7440-28-012/14/16 21:405.5 5.0 1
Vanadium ND ug/L 12/17/16 00:16 7440-62-212/14/16 21:4025.0 2.5 1
Zinc 6.4J ug/L 12/17/16 00:16 7440-66-612/14/16 21:4010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/07/16 22:06 67-64-110010.0 1
Acrylonitrile ND ug/L 12/07/16 22:06 107-13-12001.9 1
Benzene 0.57J ug/L 12/07/16 22:06 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/07/16 22:06 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/07/16 22:06 75-27-41.0 0.18 1
Bromoform ND ug/L 12/07/16 22:06 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/07/16 22:06 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/07/16 22:06 78-93-31000.96 1
Carbon disulfide ND ug/L 12/07/16 22:06 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/07/16 22:06 56-23-51.0 0.25 1
Chlorobenzene 3.0J ug/L 12/07/16 22:06 108-90-73.0 0.23 1
Chloroethane 0.68J ug/L 12/07/16 22:06 75-00-310.0 0.54 1
Chloroform ND ug/L 12/07/16 22:06 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/07/16 22:06 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/07/16 22:06 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/07/16 22:06 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/07/16 22:06 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/07/16 22:06 74-95-310.0 0.21 1
1,2-Dichlorobenzene 1.2J ug/L 12/07/16 22:06 95-50-15.0 0.30 1
1,4-Dichlorobenzene 3.4 ug/L 12/07/16 22:06 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/07/16 22:06 110-57-61001.0 1
1,1-Dichloroethane 0.37J ug/L 12/07/16 22:06 75-34-35.0 0.32 1
1,2-Dichloroethane 0.40J ug/L 12/07/16 22:06 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/07/16 22:06 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 1.2J ug/L 12/07/16 22:06 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/07/16 22:06 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/07/16 22:06 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/07/16 22:06 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/07/16 22:06 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 66
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Sample:MW-17 Lab ID:92321720012 Collected:12/02/16 12:05 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/07/16 22:06 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/07/16 22:06 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/07/16 22:06 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/07/16 22:06 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/07/16 22:06 108-10-11000.33 1
Styrene ND ug/L 12/07/16 22:06 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/07/16 22:06 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/07/16 22:06 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/07/16 22:06 127-18-41.0 0.46 1
Toluene 2.6 ug/L 12/07/16 22:06 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/07/16 22:06 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/07/16 22:06 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/07/16 22:06 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/07/16 22:06 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/07/16 22:06 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/07/16 22:06 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/07/16 22:06 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/07/16 22:06 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %12/07/16 22:06 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %12/07/16 22:06 17060-07-070-130 1
Toluene-d8 (S)106 %12/07/16 22:06 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 66
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Sample:MW-18 Lab ID:92321720013 Collected:12/02/16 09:15 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/17/16 00:20 7440-36-012/14/16 21:406.0 3.8 1
Arsenic ND ug/L 12/18/16 20:36 7440-38-212/14/16 21:4010.0 2.5 1
Barium 10.8J ug/L 12/17/16 00:20 7440-39-312/14/16 21:401002.5 1
Beryllium ND ug/L 12/17/16 00:20 7440-41-712/14/16 21:401.0 0.50 1
Cadmium 3.0 ug/L 12/17/16 00:20 7440-43-912/14/16 21:401.0 0.50 1
Chromium ND ug/L 12/17/16 00:20 7440-47-312/14/16 21:4010.0 2.5 1
Cobalt ND ug/L 12/17/16 00:20 7440-48-412/14/16 21:4010.0 2.5 1
Copper ND ug/L 12/17/16 00:20 7440-50-812/14/16 21:4010.0 2.5 1
Lead ND ug/L 12/17/16 00:20 7439-92-112/14/16 21:4010.0 2.5 1
Nickel ND ug/L 12/17/16 00:20 7440-02-012/14/16 21:4050.0 2.5 1
Selenium ND ug/L 12/17/16 00:20 7782-49-212/14/16 21:4010.0 5.0 1
Silver ND ug/L 12/17/16 00:20 7440-22-412/14/16 21:4010.0 2.5 1
Thallium ND ug/L 12/17/16 00:20 7440-28-012/14/16 21:405.5 5.0 1
Vanadium ND ug/L 12/17/16 00:20 7440-62-212/14/16 21:4025.0 2.5 1
Zinc 8.7J ug/L 12/17/16 00:20 7440-66-612/14/16 21:4010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/07/16 22:23 67-64-110010.0 1
Acrylonitrile ND ug/L 12/07/16 22:23 107-13-12001.9 1
Benzene ND ug/L 12/07/16 22:23 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/07/16 22:23 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/07/16 22:23 75-27-41.0 0.18 1
Bromoform ND ug/L 12/07/16 22:23 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/07/16 22:23 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/07/16 22:23 78-93-31000.96 1
Carbon disulfide ND ug/L 12/07/16 22:23 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/07/16 22:23 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/07/16 22:23 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/07/16 22:23 75-00-310.0 0.54 1
Chloroform ND ug/L 12/07/16 22:23 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/07/16 22:23 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/07/16 22:23 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/07/16 22:23 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/07/16 22:23 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/07/16 22:23 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/07/16 22:23 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/07/16 22:23 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/07/16 22:23 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/07/16 22:23 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/07/16 22:23 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/07/16 22:23 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/07/16 22:23 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/07/16 22:23 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/07/16 22:23 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/07/16 22:23 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/07/16 22:23 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 66
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Sample:MW-18 Lab ID:92321720013 Collected:12/02/16 09:15 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/07/16 22:23 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/07/16 22:23 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/07/16 22:23 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/07/16 22:23 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/07/16 22:23 108-10-11000.33 1
Styrene ND ug/L 12/07/16 22:23 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/07/16 22:23 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/07/16 22:23 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/07/16 22:23 127-18-41.0 0.46 1
Toluene ND ug/L 12/07/16 22:23 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/07/16 22:23 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/07/16 22:23 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/07/16 22:23 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/07/16 22:23 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/07/16 22:23 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/07/16 22:23 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/07/16 22:23 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/07/16 22:23 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %12/07/16 22:23 460-00-470-130 1
1,2-Dichloroethane-d4 (S)93 %12/07/16 22:23 17060-07-070-130 1
Toluene-d8 (S)107 %12/07/16 22:23 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 66
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Sample:MW-19 Lab ID:92321720014 Collected:12/02/16 10:00 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/17/16 00:23 7440-36-012/14/16 21:406.0 3.8 1
Arsenic ND ug/L 12/18/16 20:39 7440-38-212/14/16 21:4010.0 2.5 1
Barium 57.6J ug/L 12/17/16 00:23 7440-39-312/14/16 21:401002.5 1
Beryllium ND ug/L 12/17/16 00:23 7440-41-712/14/16 21:401.0 0.50 1
Cadmium ND ug/L 12/17/16 00:23 7440-43-912/14/16 21:401.0 0.50 1
Chromium ND ug/L 12/17/16 00:23 7440-47-312/14/16 21:4010.0 2.5 1
Cobalt ND ug/L 12/17/16 00:23 7440-48-412/14/16 21:4010.0 2.5 1
Copper ND ug/L 12/17/16 00:23 7440-50-812/14/16 21:4010.0 2.5 1
Lead ND ug/L 12/17/16 00:23 7439-92-112/14/16 21:4010.0 2.5 1
Nickel ND ug/L 12/17/16 00:23 7440-02-012/14/16 21:4050.0 2.5 1
Selenium ND ug/L 12/17/16 00:23 7782-49-212/14/16 21:4010.0 5.0 1
Silver ND ug/L 12/17/16 00:23 7440-22-412/14/16 21:4010.0 2.5 1
Thallium ND ug/L 12/17/16 00:23 7440-28-012/14/16 21:405.5 5.0 1
Vanadium 2.9J ug/L 12/17/16 00:23 7440-62-212/14/16 21:4025.0 2.5 1
Zinc 5.8J ug/L 12/17/16 00:23 7440-66-612/14/16 21:4010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/07/16 22:41 67-64-110010.0 1
Acrylonitrile ND ug/L 12/07/16 22:41 107-13-12001.9 1
Benzene ND ug/L 12/07/16 22:41 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/07/16 22:41 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/07/16 22:41 75-27-41.0 0.18 1
Bromoform ND ug/L 12/07/16 22:41 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/07/16 22:41 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/07/16 22:41 78-93-31000.96 1
Carbon disulfide ND ug/L 12/07/16 22:41 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/07/16 22:41 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/07/16 22:41 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/07/16 22:41 75-00-310.0 0.54 1
Chloroform ND ug/L 12/07/16 22:41 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/07/16 22:41 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/07/16 22:41 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/07/16 22:41 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/07/16 22:41 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/07/16 22:41 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/07/16 22:41 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/07/16 22:41 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/07/16 22:41 110-57-61001.0 1
1,1-Dichloroethane 1.5J ug/L 12/07/16 22:41 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/07/16 22:41 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/07/16 22:41 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 2.2J ug/L 12/07/16 22:41 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/07/16 22:41 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/07/16 22:41 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/07/16 22:41 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/07/16 22:41 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 66
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Sample:MW-19 Lab ID:92321720014 Collected:12/02/16 10:00 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/07/16 22:41 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/07/16 22:41 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/07/16 22:41 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/07/16 22:41 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/07/16 22:41 108-10-11000.33 1
Styrene ND ug/L 12/07/16 22:41 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/07/16 22:41 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/07/16 22:41 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/07/16 22:41 127-18-41.0 0.46 1
Toluene ND ug/L 12/07/16 22:41 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/07/16 22:41 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/07/16 22:41 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/07/16 22:41 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/07/16 22:41 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/07/16 22:41 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/07/16 22:41 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/07/16 22:41 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/07/16 22:41 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)95 %12/07/16 22:41 460-00-470-130 1
1,2-Dichloroethane-d4 (S)93 %12/07/16 22:41 17060-07-070-130 1
Toluene-d8 (S)106 %12/07/16 22:41 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 66
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Sample:MW-20 Lab ID:92321720015 Collected:12/02/16 15:30 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/17/16 00:26 7440-36-012/14/16 21:406.0 3.8 1
Arsenic ND ug/L 12/18/16 20:51 7440-38-212/14/16 21:4010.0 2.5 1
Barium 35.7J ug/L 12/17/16 00:26 7440-39-312/14/16 21:401002.5 1
Beryllium ND ug/L 12/17/16 00:26 7440-41-712/14/16 21:401.0 0.50 1
Cadmium ND ug/L 12/17/16 00:26 7440-43-912/14/16 21:401.0 0.50 1
Chromium ND ug/L 12/17/16 00:26 7440-47-312/14/16 21:4010.0 2.5 1
Cobalt 19.0 ug/L 12/17/16 00:26 7440-48-412/14/16 21:4010.0 2.5 1
Copper ND ug/L 12/17/16 00:26 7440-50-812/14/16 21:4010.0 2.5 1
Lead ND ug/L 12/17/16 00:26 7439-92-112/14/16 21:4010.0 2.5 1
Nickel ND ug/L 12/17/16 00:26 7440-02-012/14/16 21:4050.0 2.5 1
Selenium ND ug/L 12/17/16 00:26 7782-49-212/14/16 21:4010.0 5.0 1
Silver ND ug/L 12/17/16 00:26 7440-22-412/14/16 21:4010.0 2.5 1
Thallium ND ug/L 12/17/16 00:26 7440-28-012/14/16 21:405.5 5.0 1
Vanadium ND ug/L 12/17/16 00:26 7440-62-212/14/16 21:4025.0 2.5 1
Zinc 9.5J ug/L 12/17/16 00:26 7440-66-612/14/16 21:4010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/07/16 22:59 67-64-110010.0 1
Acrylonitrile ND ug/L 12/07/16 22:59 107-13-12001.9 1
Benzene ND ug/L 12/07/16 22:59 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/07/16 22:59 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/07/16 22:59 75-27-41.0 0.18 1
Bromoform ND ug/L 12/07/16 22:59 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/07/16 22:59 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/07/16 22:59 78-93-31000.96 1
Carbon disulfide ND ug/L 12/07/16 22:59 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/07/16 22:59 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/07/16 22:59 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/07/16 22:59 75-00-310.0 0.54 1
Chloroform ND ug/L 12/07/16 22:59 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/07/16 22:59 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/07/16 22:59 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/07/16 22:59 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/07/16 22:59 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/07/16 22:59 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/07/16 22:59 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/07/16 22:59 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/07/16 22:59 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/07/16 22:59 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/07/16 22:59 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/07/16 22:59 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.87J ug/L 12/07/16 22:59 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/07/16 22:59 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/07/16 22:59 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/07/16 22:59 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/07/16 22:59 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 66
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Sample:MW-20 Lab ID:92321720015 Collected:12/02/16 15:30 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/07/16 22:59 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/07/16 22:59 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/07/16 22:59 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/07/16 22:59 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/07/16 22:59 108-10-11000.33 1
Styrene ND ug/L 12/07/16 22:59 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/07/16 22:59 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/07/16 22:59 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/07/16 22:59 127-18-41.0 0.46 1
Toluene ND ug/L 12/07/16 22:59 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/07/16 22:59 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/07/16 22:59 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/07/16 22:59 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/07/16 22:59 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/07/16 22:59 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/07/16 22:59 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/07/16 22:59 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/07/16 22:59 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %12/07/16 22:59 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %12/07/16 22:59 17060-07-070-130 1
Toluene-d8 (S)107 %12/07/16 22:59 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 66
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Sample:MW-21 Lab ID:92321720016 Collected:12/02/16 17:00 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/17/16 00:29 7440-36-012/14/16 21:406.0 3.8 1
Arsenic 2.5J ug/L 12/18/16 20:55 7440-38-212/14/16 21:4010.0 2.5 1
Barium 69.4J ug/L 12/17/16 00:29 7440-39-312/14/16 21:401002.5 1
Beryllium ND ug/L 12/17/16 00:29 7440-41-712/14/16 21:401.0 0.50 1
Cadmium ND ug/L 12/17/16 00:29 7440-43-912/14/16 21:401.0 0.50 1
Chromium ND ug/L 12/17/16 00:29 7440-47-312/14/16 21:4010.0 2.5 1
Cobalt 5.2J ug/L 12/17/16 00:29 7440-48-412/14/16 21:4010.0 2.5 1
Copper ND ug/L 12/17/16 00:29 7440-50-812/14/16 21:4010.0 2.5 1
Lead ND ug/L 12/17/16 00:29 7439-92-112/14/16 21:4010.0 2.5 1
Nickel ND ug/L 12/17/16 00:29 7440-02-012/14/16 21:4050.0 2.5 1
Selenium ND ug/L 12/17/16 00:29 7782-49-212/14/16 21:4010.0 5.0 1
Silver ND ug/L 12/17/16 00:29 7440-22-412/14/16 21:4010.0 2.5 1
Thallium ND ug/L 12/17/16 00:29 7440-28-012/14/16 21:405.5 5.0 1
Vanadium ND ug/L 12/17/16 00:29 7440-62-212/14/16 21:4025.0 2.5 1
Zinc 7.5J ug/L 12/17/16 00:29 7440-66-612/14/16 21:4010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/07/16 23:17 67-64-110010.0 1
Acrylonitrile ND ug/L 12/07/16 23:17 107-13-12001.9 1
Benzene ND ug/L 12/07/16 23:17 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/07/16 23:17 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/07/16 23:17 75-27-41.0 0.18 1
Bromoform ND ug/L 12/07/16 23:17 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/07/16 23:17 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/07/16 23:17 78-93-31000.96 1
Carbon disulfide ND ug/L 12/07/16 23:17 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/07/16 23:17 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/07/16 23:17 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/07/16 23:17 75-00-310.0 0.54 1
Chloroform ND ug/L 12/07/16 23:17 67-66-35.0 0.14 1
Chloromethane 0.20J ug/L 12/07/16 23:17 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/07/16 23:17 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/07/16 23:17 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/07/16 23:17 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/07/16 23:17 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/07/16 23:17 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/07/16 23:17 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/07/16 23:17 110-57-61001.0 1
1,1-Dichloroethane 4.0J ug/L 12/07/16 23:17 75-34-35.0 0.32 1
1,2-Dichloroethane 0.38J ug/L 12/07/16 23:17 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/07/16 23:17 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 16.8 ug/L 12/07/16 23:17 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/07/16 23:17 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/07/16 23:17 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/07/16 23:17 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/07/16 23:17 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 66
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Sample:MW-21 Lab ID:92321720016 Collected:12/02/16 17:00 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/07/16 23:17 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/07/16 23:17 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/07/16 23:17 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/07/16 23:17 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/07/16 23:17 108-10-11000.33 1
Styrene ND ug/L 12/07/16 23:17 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/07/16 23:17 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/07/16 23:17 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/07/16 23:17 127-18-41.0 0.46 1
Toluene ND ug/L 12/07/16 23:17 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/07/16 23:17 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/07/16 23:17 79-00-51.0 0.29 1
Trichloroethene 0.85J ug/L 12/07/16 23:17 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/07/16 23:17 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/07/16 23:17 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/07/16 23:17 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/07/16 23:17 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/07/16 23:17 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %12/07/16 23:17 460-00-470-130 1
1,2-Dichloroethane-d4 (S)94 %12/07/16 23:17 17060-07-070-130 1
Toluene-d8 (S)105 %12/07/16 23:17 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 66
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Sample:MW-22 Lab ID:92321720017 Collected:12/02/16 10:40 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/17/16 00:32 7440-36-012/14/16 21:406.0 3.8 1
Arsenic ND ug/L 12/18/16 20:58 7440-38-212/14/16 21:4010.0 2.5 1
Barium 18.4J ug/L 12/17/16 00:32 7440-39-312/14/16 21:401002.5 1
Beryllium ND ug/L 12/17/16 00:32 7440-41-712/14/16 21:401.0 0.50 1
Cadmium ND ug/L 12/17/16 00:32 7440-43-912/14/16 21:401.0 0.50 1
Chromium ND ug/L 12/17/16 00:32 7440-47-312/14/16 21:4010.0 2.5 1
Cobalt ND ug/L 12/17/16 00:32 7440-48-412/14/16 21:4010.0 2.5 1
Copper ND ug/L 12/17/16 00:32 7440-50-812/14/16 21:4010.0 2.5 1
Lead ND ug/L 12/17/16 00:32 7439-92-112/14/16 21:4010.0 2.5 1
Nickel ND ug/L 12/17/16 00:32 7440-02-012/14/16 21:4050.0 2.5 1
Selenium ND ug/L 12/17/16 00:32 7782-49-212/14/16 21:4010.0 5.0 1
Silver ND ug/L 12/17/16 00:32 7440-22-412/14/16 21:4010.0 2.5 1
Thallium ND ug/L 12/17/16 00:32 7440-28-012/14/16 21:405.5 5.0 1
Vanadium ND ug/L 12/17/16 00:32 7440-62-212/14/16 21:4025.0 2.5 1
Zinc ND ug/L 12/17/16 00:32 7440-66-612/14/16 21:4010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/07/16 23:35 67-64-110010.0 1
Acrylonitrile ND ug/L 12/07/16 23:35 107-13-12001.9 1
Benzene 0.43J ug/L 12/07/16 23:35 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/07/16 23:35 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/07/16 23:35 75-27-41.0 0.18 1
Bromoform ND ug/L 12/07/16 23:35 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/07/16 23:35 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/07/16 23:35 78-93-31000.96 1
Carbon disulfide ND ug/L 12/07/16 23:35 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/07/16 23:35 56-23-51.0 0.25 1
Chlorobenzene 2.0J ug/L 12/07/16 23:35 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/07/16 23:35 75-00-310.0 0.54 1
Chloroform ND ug/L 12/07/16 23:35 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/07/16 23:35 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/07/16 23:35 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/07/16 23:35 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/07/16 23:35 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/07/16 23:35 74-95-310.0 0.21 1
1,2-Dichlorobenzene 0.70J ug/L 12/07/16 23:35 95-50-15.0 0.30 1
1,4-Dichlorobenzene 6.5 ug/L 12/07/16 23:35 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/07/16 23:35 110-57-61001.0 1
1,1-Dichloroethane 1.1J ug/L 12/07/16 23:35 75-34-35.0 0.32 1
1,2-Dichloroethane 0.64J ug/L 12/07/16 23:35 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/07/16 23:35 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 2.6J ug/L 12/07/16 23:35 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/07/16 23:35 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/07/16 23:35 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/07/16 23:35 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/07/16 23:35 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 66
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Sample:MW-22 Lab ID:92321720017 Collected:12/02/16 10:40 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/07/16 23:35 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/07/16 23:35 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/07/16 23:35 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/07/16 23:35 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/07/16 23:35 108-10-11000.33 1
Styrene ND ug/L 12/07/16 23:35 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/07/16 23:35 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/07/16 23:35 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/07/16 23:35 127-18-41.0 0.46 1
Toluene ND ug/L 12/07/16 23:35 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/07/16 23:35 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/07/16 23:35 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/07/16 23:35 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/07/16 23:35 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/07/16 23:35 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/07/16 23:35 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/07/16 23:35 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/07/16 23:35 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %12/07/16 23:35 460-00-470-130 1
1,2-Dichloroethane-d4 (S)94 %12/07/16 23:35 17060-07-070-130 1
Toluene-d8 (S)109 %12/07/16 23:35 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 66
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Sample:MW-23 Lab ID:92321720018 Collected:12/02/16 11:30 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/17/16 00:44 7440-36-012/14/16 21:406.0 3.8 1
Arsenic 5.6J ug/L 12/17/16 00:44 7440-38-212/14/16 21:4010.0 2.5 1
Barium 38.8J ug/L 12/17/16 00:44 7440-39-312/14/16 21:401002.5 1
Beryllium ND ug/L 12/17/16 00:44 7440-41-712/14/16 21:401.0 0.50 1
Cadmium 0.53J ug/L 12/17/16 00:44 7440-43-912/14/16 21:401.0 0.50 1
Chromium ND ug/L 12/17/16 00:44 7440-47-312/14/16 21:4010.0 2.5 1
Cobalt ND ug/L 12/17/16 00:44 7440-48-412/14/16 21:4010.0 2.5 1
Copper ND ug/L 12/17/16 00:44 7440-50-812/14/16 21:4010.0 2.5 1
Lead ND ug/L 12/17/16 00:44 7439-92-112/14/16 21:4010.0 2.5 1
Nickel ND ug/L 12/17/16 00:44 7440-02-012/14/16 21:4050.0 2.5 1
Selenium ND ug/L 12/17/16 00:44 7782-49-212/14/16 21:4010.0 5.0 1
Silver ND ug/L 12/17/16 00:44 7440-22-412/14/16 21:4010.0 2.5 1
Thallium ND ug/L 12/17/16 00:44 7440-28-012/14/16 21:405.5 5.0 1
Vanadium ND ug/L 12/17/16 00:44 7440-62-212/14/16 21:4025.0 2.5 1
Zinc ND ug/L 12/17/16 00:44 7440-66-612/14/16 21:4010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/08/16 00:10 67-64-110010.0 1
Acrylonitrile ND ug/L 12/08/16 00:10 107-13-12001.9 1
Benzene ND ug/L 12/08/16 00:10 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/08/16 00:10 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/08/16 00:10 75-27-41.0 0.18 1
Bromoform ND ug/L 12/08/16 00:10 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/08/16 00:10 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/08/16 00:10 78-93-31000.96 1
Carbon disulfide ND ug/L 12/08/16 00:10 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/08/16 00:10 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/08/16 00:10 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/08/16 00:10 75-00-310.0 0.54 1
Chloroform ND ug/L 12/08/16 00:10 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/08/16 00:10 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/08/16 00:10 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/08/16 00:10 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/08/16 00:10 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/08/16 00:10 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/08/16 00:10 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/08/16 00:10 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/08/16 00:10 110-57-61001.0 1
1,1-Dichloroethane 0.61J ug/L 12/08/16 00:10 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/08/16 00:10 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/08/16 00:10 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.72J ug/L 12/08/16 00:10 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/08/16 00:10 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/08/16 00:10 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/08/16 00:10 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/08/16 00:10 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 66
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Sample:MW-23 Lab ID:92321720018 Collected:12/02/16 11:30 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/08/16 00:10 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/08/16 00:10 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/08/16 00:10 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/08/16 00:10 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/08/16 00:10 108-10-11000.33 1
Styrene ND ug/L 12/08/16 00:10 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/08/16 00:10 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/08/16 00:10 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/08/16 00:10 127-18-41.0 0.46 1
Toluene ND ug/L 12/08/16 00:10 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/08/16 00:10 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/08/16 00:10 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/08/16 00:10 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/08/16 00:10 75-69-4 M11.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/08/16 00:10 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/08/16 00:10 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/08/16 00:10 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/08/16 00:10 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)95 %12/08/16 00:10 460-00-470-130 1
1,2-Dichloroethane-d4 (S)94 %12/08/16 00:10 17060-07-070-130 1
Toluene-d8 (S)107 %12/08/16 00:10 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 66
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
340395
EPA 9056A
EPA 9056A
9056 IC Anions, GWD
Associated Lab Samples:92321720011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1887931
Associated Lab Samples:92321720011
Matrix:Water
AnalyzedMDL
Bromide mg/L ND 0.10 12/12/16 14:480.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1887932LABORATORY CONTROL SAMPLE:
LCSSpike
Bromide mg/L 2.42.5 96 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1887933MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92322329001
1887934
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromide mg/L 2.5 97 90-11095 2 202.50.21 2.6 2.6
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1887935MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321720011
1887936
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromide mg/L 2.5 98 90-11099 1 202.50.58 3.0 3.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 66
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
339672
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92321720001, 92321720002, 92321720003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1883876
Associated Lab Samples:92321720001, 92321720002, 92321720003
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 12/13/16 13:093.8
Arsenic ug/L 2.9J 10.0 12/13/16 13:092.5
Barium ug/L ND 100 12/13/16 13:092.5
Beryllium ug/L ND 1.0 12/13/16 13:090.50
Cadmium ug/L ND 1.0 12/13/16 13:090.50
Chromium ug/L ND 10.0 12/13/16 13:092.5
Cobalt ug/L ND 10.0 12/13/16 13:092.5
Copper ug/L ND 10.0 12/13/16 13:092.5
Lead ug/L ND 10.0 12/13/16 13:092.5
Nickel ug/L ND 50.0 12/13/16 13:092.5
Selenium ug/L ND 10.0 12/13/16 13:095.0
Silver ug/L ND 10.0 12/13/16 13:092.5
Thallium ug/L ND 5.5 12/13/16 13:095.0
Vanadium ug/L ND 25.0 12/13/16 13:092.5
Zinc ug/L ND 10.0 12/13/16 13:095.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1883877LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 490500 98 80-120
Arsenic ug/L 475500 95 80-120
Barium ug/L 493500 99 80-120
Beryllium ug/L 486500 97 80-120
Cadmium ug/L 487500 97 80-120
Chromium ug/L 496500 99 80-120
Cobalt ug/L 500500 100 80-120
Copper ug/L 501500 100 80-120
Lead ug/L 492500 98 80-120
Nickel ug/L 484500 97 80-120
Selenium ug/L 467500 93 80-120
Silver ug/L 246250 98 80-120
Thallium ug/L 485500 97 80-120
Vanadium ug/L 487500 97 80-120
Zinc ug/L 480500 96 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 66
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1883878MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321691015
1883879
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 98 75-12598 1 25500ND492488
Arsenic ug/L 500 97 75-12595 2 25500ND483475
Barium ug/L 500 99 75-12599 0 2550025.0J 520 519
Beryllium ug/L 500 98 75-12598 0 25500ND490489
Cadmium ug/L 500 97 75-12597 0 25500ND487486
Chromium ug/L 500 99 75-12599 1 25500ND498495
Cobalt ug/L 500 101 75-125100 1 25500ND503500
Copper ug/L 500 102 75-125101 0 25500ND508506
Lead ug/L 500 98 75-12598 0 25500ND492490
Nickel ug/L 500 97 75-12597 0 25500ND485484
Selenium ug/L 500 96 75-12595 1 25500ND481476
Silver ug/L 250 99 75-12598 1 25250ND248246
Thallium ug/L 500 98 75-12597 0 25500ND488486
Vanadium ug/L 500 98 75-12598 0 25500ND492490
Zinc ug/L 500 97 75-12596 1 25500ND486483
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 66
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
340698
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92321720004, 92321720005, 92321720006, 92321720008, 92321720009, 92321720011, 92321720012,
92321720013, 92321720014, 92321720015, 92321720016, 92321720017, 92321720018
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1889943
Associated Lab Samples:92321720004, 92321720005, 92321720006, 92321720008, 92321720009, 92321720011, 92321720012,
92321720013, 92321720014, 92321720015, 92321720016, 92321720017, 92321720018
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 12/16/16 23:243.8
Arsenic ug/L ND 10.0 12/18/16 19:392.5
Barium ug/L ND 100 12/16/16 23:242.5
Beryllium ug/L ND 1.0 12/16/16 23:240.50
Cadmium ug/L ND 1.0 12/16/16 23:240.50
Chromium ug/L ND 10.0 12/16/16 23:242.5
Cobalt ug/L ND 10.0 12/16/16 23:242.5
Copper ug/L ND 10.0 12/16/16 23:242.5
Lead ug/L ND 10.0 12/16/16 23:242.5
Nickel ug/L ND 50.0 12/16/16 23:242.5
Selenium ug/L ND 10.0 12/16/16 23:245.0
Silver ug/L ND 10.0 12/16/16 23:242.5
Thallium ug/L ND 5.5 12/16/16 23:245.0
Vanadium ug/L ND 25.0 12/16/16 23:242.5
Zinc ug/L ND 10.0 12/16/16 23:245.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1889944LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 514500 103 80-120
Arsenic ug/L 508500 102 80-120
Barium ug/L 526500 105 80-120
Beryllium ug/L 495500 99 80-120
Cadmium ug/L 506500 101 80-120
Chromium ug/L 504500 101 80-120
Cobalt ug/L 524500 105 80-120
Copper ug/L 538500 108 80-120
Lead ug/L 520500 104 80-120
Nickel ug/L 494500 99 80-120
Selenium ug/L 526500 105 80-120
Silver ug/L 256250 103 80-120
Thallium ug/L 523500 105 80-120
Vanadium ug/L 496500 99 80-120
Zinc ug/L 522500 104 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 66
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1889945MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92322158002
1889946
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 102 75-125102 1 25500ND514511
Arsenic ug/L 500 99 75-125100 1 255003.4J 497 501
Barium ug/L 500 106 75-125105 1 25500ND530524
Beryllium ug/L 500 98 75-12598 0 25500ND489491
Cadmium ug/L 500 99 75-125100 0 25500ND497499
Chromium ug/L 500 99 75-125100 1 25500ND496502
Cobalt ug/L 500 105 75-125104 1 25500ND526520
Copper ug/L 500 105 75-125106 0 25500ND528530
Lead ug/L 500 104 75-125103 1 25500ND522517
Nickel ug/L 500 98 75-12598 0 25500ND488490
Selenium ug/L 500 104 75-125104 0 25500ND522519
Silver ug/L 250 100 75-125101 1 25250ND250253
Thallium ug/L 500 104 75-125105 1 25500ND522529
Vanadium ug/L 500 97 75-12598 1 25500ND486492
Zinc ug/L 500 104 75-125103 1 25500ND519516
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 66
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
339770
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92321720001, 92321720002, 92321720003, 92321720004, 92321720005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1884326
Associated Lab Samples:92321720001, 92321720002, 92321720003, 92321720004, 92321720005
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 12/07/16 14:240.33
1,1,1-Trichloroethane ug/L ND 1.0 12/07/16 14:240.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 12/07/16 14:240.40
1,1,2-Trichloroethane ug/L ND 1.0 12/07/16 14:240.29
1,1-Dichloroethane ug/L ND 5.0 12/07/16 14:240.32
1,1-Dichloroethene ug/L ND 5.0 12/07/16 14:240.56
1,2,3-Trichloropropane ug/L ND 1.0 12/07/16 14:240.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 12/07/16 14:242.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 12/07/16 14:240.27
1,2-Dichlorobenzene ug/L ND 5.0 12/07/16 14:240.30
1,2-Dichloroethane ug/L ND 1.0 12/07/16 14:240.24
1,2-Dichloropropane ug/L ND 1.0 12/07/16 14:240.27
1,4-Dichlorobenzene ug/L ND 1.0 12/07/16 14:240.33
2-Butanone (MEK)ug/L ND 100 12/07/16 14:240.96
2-Hexanone ug/L ND 50.0 12/07/16 14:240.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 12/07/16 14:240.33
Acetone ug/L ND 100 12/07/16 14:2410.0
Acrylonitrile ug/L ND 200 12/07/16 14:241.9
Benzene ug/L ND 1.0 12/07/16 14:240.25
Bromochloromethane ug/L ND 3.0 12/07/16 14:240.17
Bromodichloromethane ug/L ND 1.0 12/07/16 14:240.18
Bromoform ug/L ND 3.0 12/07/16 14:240.26
Bromomethane ug/L ND 10.0 12/07/16 14:240.29
Carbon disulfide ug/L ND 100 12/07/16 14:241.2
Carbon tetrachloride ug/L ND 1.0 12/07/16 14:240.25
Chlorobenzene ug/L ND 3.0 12/07/16 14:240.23
Chloroethane ug/L ND 10.0 12/07/16 14:240.54
Chloroform ug/L ND 5.0 12/07/16 14:240.14
Chloromethane ug/L ND 1.0 12/07/16 14:240.11
cis-1,2-Dichloroethene ug/L ND 5.0 12/07/16 14:240.19
cis-1,3-Dichloropropene ug/L ND 1.0 12/07/16 14:240.13
Dibromochloromethane ug/L ND 3.0 12/07/16 14:240.21
Dibromomethane ug/L ND 10.0 12/07/16 14:240.21
Ethylbenzene ug/L ND 1.0 12/07/16 14:240.30
Iodomethane ug/L ND 10.0 12/07/16 14:240.32
Methylene Chloride ug/L ND 1.0 12/07/16 14:240.97
Styrene ug/L ND 1.0 12/07/16 14:240.26
Tetrachloroethene ug/L ND 1.0 12/07/16 14:240.46
Toluene ug/L ND 1.0 12/07/16 14:240.26
trans-1,2-Dichloroethene ug/L ND 5.0 12/07/16 14:240.49
trans-1,3-Dichloropropene ug/L ND 1.0 12/07/16 14:240.26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 66
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1884326
Associated Lab Samples:92321720001, 92321720002, 92321720003, 92321720004, 92321720005
Matrix:Water
AnalyzedMDL
trans-1,4-Dichloro-2-butene ug/L ND 100 12/07/16 14:241.0
Trichloroethene ug/L ND 1.0 12/07/16 14:240.47
Trichlorofluoromethane ug/L ND 1.0 12/07/16 14:240.20
Vinyl acetate ug/L ND 50.0 12/07/16 14:240.35
Vinyl chloride ug/L ND 1.0 12/07/16 14:240.62
Xylene (Total)ug/L ND 5.0 12/07/16 14:240.66
1,2-Dichloroethane-d4 (S)%91 70-130 12/07/16 14:24
4-Bromofluorobenzene (S)%98 70-130 12/07/16 14:24
Toluene-d8 (S)%107 70-130 12/07/16 14:24
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1884327LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.150 100 80-125
1,1,1-Trichloroethane ug/L 48.650 97 71-129
1,1,2,2-Tetrachloroethane ug/L 48.450 97 79-124
1,1,2-Trichloroethane ug/L 47.450 95 85-125
1,1-Dichloroethane ug/L 46.550 93 73-126
1,1-Dichloroethene ug/L 49.150 98 66-135
1,2,3-Trichloropropane ug/L 47.850 96 75-130
1,2-Dibromo-3-chloropropane ug/L 44.450 89 71-133
1,2-Dibromoethane (EDB)ug/L 50.350 101 83-124
1,2-Dichlorobenzene ug/L 47.450 95 80-133
1,2-Dichloroethane ug/L 44.150 88 67-128
1,2-Dichloropropane ug/L 46.650 93 75-132
1,4-Dichlorobenzene ug/L 47.750 95 78-130
2-Butanone (MEK)ug/L 98.7J100 99 61-144
2-Hexanone ug/L 92.2100 92 68-143
4-Methyl-2-pentanone (MIBK)ug/L 87.4J100 87 72-135
Acetone ug/L 97.1J100 97 48-146
Acrylonitrile ug/L 229250 92 40-160
Benzene ug/L 49.150 98 80-125
Bromochloromethane ug/L 48.250 96 71-125
Bromodichloromethane ug/L 49.550 99 78-124
Bromoform ug/L 42.150 84 71-128
Bromomethane ug/L 48.350 97 40-160
Carbon disulfide ug/L 45.9J50 92 50-160
Carbon tetrachloride ug/L 50.450 101 69-131
Chlorobenzene ug/L 47.150 94 81-122
Chloroethane ug/L 49.850 100 39-148
Chloroform ug/L 46.150 92 73-127
Chloromethane ug/L 47.750 95 44-146
cis-1,2-Dichloroethene ug/L 45.950 92 74-124
cis-1,3-Dichloropropene ug/L 50.150 100 72-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 66
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1884327LABORATORY CONTROL SAMPLE:
LCSSpike
Dibromochloromethane ug/L 52.450 105 78-125
Dibromomethane ug/L 46.950 94 82-120
Ethylbenzene ug/L 47.150 94 79-121
Iodomethane ug/L 87.5100 87 39-154
Methylene Chloride ug/L 48.850 98 64-133
Styrene ug/L 47.350 95 84-126
Tetrachloroethene ug/L 46.250 92 78-122
Toluene ug/L 46.350 93 80-121
trans-1,2-Dichloroethene ug/L 47.750 95 71-127
trans-1,3-Dichloropropene ug/L 47.950 96 69-141
trans-1,4-Dichloro-2-butene ug/L 44.0J50 88 40-160
Trichloroethene ug/L 49.550 99 78-122
Trichlorofluoromethane ug/L 55.750 111 53-137
Vinyl acetate ug/L 102100 102 40-160
Vinyl chloride ug/L 44.650 89 58-137
Xylene (Total)ug/L 143150 95 81-126
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1884329MATRIX SPIKE SAMPLE:
MSSpike
Result
92321720005
1,1,1,2-Tetrachloroethane ug/L 19.720 98 70-130ND
1,1,1-Trichloroethane ug/L 21.820 109 70-130ND
1,1,2,2-Tetrachloroethane ug/L 18.620 93 70-130ND
1,1,2-Trichloroethane ug/L 20.020 100 70-130ND
1,1-Dichloroethane ug/L 20.320 102 70-130ND
1,1-Dichloroethene ug/L 23.020 115 70-166ND
1,2,3-Trichloropropane ug/L 18.020 90 70-130ND
1,2-Dibromo-3-chloropropane ug/L 17.720 89 70-130ND
1,2-Dibromoethane (EDB)ug/L 19.220 96 70-130ND
1,2-Dichlorobenzene ug/L 20.020 100 70-130ND
1,2-Dichloroethane ug/L 19.620 98 70-130ND
1,2-Dichloropropane ug/L 20.120 100 70-130ND
1,4-Dichlorobenzene ug/L 21.220 100 70-1301.3
2-Butanone (MEK)ug/L 32.3J40 81 70-130ND
2-Hexanone ug/L 33.9J40 85 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 35.1J40 88 70-130ND
Acetone ug/L 32.7J40 82 70-130ND
Acrylonitrile ug/L 90.5J100 91 70-130ND
Benzene ug/L 21.720 109 70-148ND
Bromochloromethane ug/L 20.420 102 70-130ND
Bromodichloromethane ug/L 21.220 106 70-130ND
Bromoform ug/L 17.220 86 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 66
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1884329MATRIX SPIKE SAMPLE:
MSSpike
Result
92321720005
Bromomethane ug/L 15.420 77 70-130ND
Carbon disulfide ug/L 21.9J20 110 70-130ND
Carbon tetrachloride ug/L 23.220 116 70-130ND
Chlorobenzene ug/L 22.420 100 70-1462.4J
Chloroethane ug/L 23.820 119 70-130ND
Chloroform ug/L 20.420 102 70-130ND
Chloromethane ug/L 20.720 103 70-130ND
cis-1,2-Dichloroethene ug/L 21.120 105 70-130ND
cis-1,3-Dichloropropene ug/L 19.620 98 70-130ND
Dibromochloromethane ug/L 19.920 100 70-130ND
Dibromomethane ug/L 20.220 101 70-130ND
Ethylbenzene ug/L 20.220 101 70-130ND
Iodomethane ug/L 38.440 96 70-130ND
Methylene Chloride ug/L 21.020 105 70-130ND
Styrene ug/L 20.120 100 70-130ND
Tetrachloroethene ug/L 19.520 98 70-130ND
Toluene ug/L 21.020 105 70-155ND
trans-1,2-Dichloroethene ug/L 22.020 110 70-130ND
trans-1,3-Dichloropropene ug/L 18.620 93 70-130ND
trans-1,4-Dichloro-2-butene ug/L 17.2J20 86 70-130ND
Trichloroethene ug/L 21.220 106 69-151ND
Trichlorofluoromethane ug/L 25.820 129 70-130ND
Vinyl acetate ug/L 30.7J40 77 70-130ND
Vinyl chloride ug/L 19.420 97 70-130ND
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92321720004
1884328SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 66
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92321720004
1884328SAMPLE DUPLICATE:
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%96 096
4-Bromofluorobenzene (S)%98 199
Toluene-d8 (S)%103 4108
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 66
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
339832
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92321720006, 92321720008, 92321720009, 92321720012, 92321720013, 92321720014, 92321720015,
92321720016, 92321720017, 92321720018
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1884816
Associated Lab Samples:92321720006, 92321720008, 92321720009, 92321720012, 92321720013, 92321720014, 92321720015,
92321720016, 92321720017, 92321720018
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 12/07/16 14:420.33
1,1,1-Trichloroethane ug/L ND 1.0 12/07/16 14:420.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 12/07/16 14:420.40
1,1,2-Trichloroethane ug/L ND 1.0 12/07/16 14:420.29
1,1-Dichloroethane ug/L ND 5.0 12/07/16 14:420.32
1,1-Dichloroethene ug/L ND 5.0 12/07/16 14:420.56
1,2,3-Trichloropropane ug/L ND 1.0 12/07/16 14:420.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 12/07/16 14:422.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 12/07/16 14:420.27
1,2-Dichlorobenzene ug/L ND 5.0 12/07/16 14:420.30
1,2-Dichloroethane ug/L ND 1.0 12/07/16 14:420.24
1,2-Dichloropropane ug/L ND 1.0 12/07/16 14:420.27
1,4-Dichlorobenzene ug/L ND 1.0 12/07/16 14:420.33
2-Butanone (MEK)ug/L ND 100 12/07/16 14:420.96
2-Hexanone ug/L ND 50.0 12/07/16 14:420.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 12/07/16 14:420.33
Acetone ug/L ND 100 12/07/16 14:4210.0
Acrylonitrile ug/L ND 200 12/07/16 14:421.9
Benzene ug/L ND 1.0 12/07/16 14:420.25
Bromochloromethane ug/L ND 3.0 12/07/16 14:420.17
Bromodichloromethane ug/L ND 1.0 12/07/16 14:420.18
Bromoform ug/L ND 3.0 12/07/16 14:420.26
Bromomethane ug/L ND 10.0 12/07/16 14:420.29
Carbon disulfide ug/L ND 100 12/07/16 14:421.2
Carbon tetrachloride ug/L ND 1.0 12/07/16 14:420.25
Chlorobenzene ug/L ND 3.0 12/07/16 14:420.23
Chloroethane ug/L ND 10.0 12/07/16 14:420.54
Chloroform ug/L ND 5.0 12/07/16 14:420.14
Chloromethane ug/L ND 1.0 12/07/16 14:420.11
cis-1,2-Dichloroethene ug/L ND 5.0 12/07/16 14:420.19
cis-1,3-Dichloropropene ug/L ND 1.0 12/07/16 14:420.13
Dibromochloromethane ug/L ND 3.0 12/07/16 14:420.21
Dibromomethane ug/L ND 10.0 12/07/16 14:420.21
Ethylbenzene ug/L ND 1.0 12/07/16 14:420.30
Iodomethane ug/L ND 10.0 12/07/16 14:420.32
Methylene Chloride ug/L ND 1.0 12/07/16 14:420.97
Styrene ug/L ND 1.0 12/07/16 14:420.26
Tetrachloroethene ug/L ND 1.0 12/07/16 14:420.46
Toluene ug/L ND 1.0 12/07/16 14:420.26
trans-1,2-Dichloroethene ug/L ND 5.0 12/07/16 14:420.49
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 66
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1884816
Associated Lab Samples:92321720006, 92321720008, 92321720009, 92321720012, 92321720013, 92321720014, 92321720015,
92321720016, 92321720017, 92321720018
Matrix:Water
AnalyzedMDL
trans-1,3-Dichloropropene ug/L ND 1.0 12/07/16 14:420.26
trans-1,4-Dichloro-2-butene ug/L ND 100 12/07/16 14:421.0
Trichloroethene ug/L ND 1.0 12/07/16 14:420.47
Trichlorofluoromethane ug/L ND 1.0 12/07/16 14:420.20
Vinyl acetate ug/L ND 50.0 12/07/16 14:420.35
Vinyl chloride ug/L ND 1.0 12/07/16 14:420.62
Xylene (Total)ug/L ND 5.0 12/07/16 14:420.66
1,2-Dichloroethane-d4 (S)%94 70-130 12/07/16 14:42
4-Bromofluorobenzene (S)%97 70-130 12/07/16 14:42
Toluene-d8 (S)%106 70-130 12/07/16 14:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1884817LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.250 98 80-125
1,1,1-Trichloroethane ug/L 50.950 102 71-129
1,1,2,2-Tetrachloroethane ug/L 44.550 89 79-124
1,1,2-Trichloroethane ug/L 46.750 93 85-125
1,1-Dichloroethane ug/L 49.850 100 73-126
1,1-Dichloroethene ug/L 52.350 105 66-135
1,2,3-Trichloropropane ug/L 44.850 90 75-130
1,2-Dibromo-3-chloropropane ug/L 43.750 87 71-133
1,2-Dibromoethane (EDB)ug/L 49.750 99 83-124
1,2-Dichlorobenzene ug/L 46.150 92 80-133
1,2-Dichloroethane ug/L 46.650 93 67-128
1,2-Dichloropropane ug/L 46.050 92 75-132
1,4-Dichlorobenzene ug/L 45.750 91 78-130
2-Butanone (MEK)ug/L 95.4J100 95 61-144
2-Hexanone ug/L 84.6100 85 68-143
4-Methyl-2-pentanone (MIBK)ug/L 80.8J100 81 72-135
Acetone ug/L 95.3J100 95 48-146
Acrylonitrile ug/L 230250 92 40-160
Benzene ug/L 49.350 99 80-125
Bromochloromethane ug/L 50.950 102 71-125
Bromodichloromethane ug/L 50.050 100 78-124
Bromoform ug/L 40.250 80 71-128
Bromomethane ug/L 56.550 113 40-160
Carbon disulfide ug/L 48.4J50 97 50-160
Carbon tetrachloride ug/L 51.450 103 69-131
Chlorobenzene ug/L 46.250 92 81-122
Chloroethane ug/L 54.250 108 39-148
Chloroform ug/L 49.350 99 73-127
Chloromethane ug/L 49.050 98 44-146
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 66
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1884817LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 48.250 96 74-124
cis-1,3-Dichloropropene ug/L 50.450 101 72-132
Dibromochloromethane ug/L 52.550 105 78-125
Dibromomethane ug/L 45.650 91 82-120
Ethylbenzene ug/L 46.650 93 79-121
Iodomethane ug/L 101100 101 39-154
Methylene Chloride ug/L 51.650 103 64-133
Styrene ug/L 49.250 98 84-126
Tetrachloroethene ug/L 47.350 95 78-122
Toluene ug/L 45.450 91 80-121
trans-1,2-Dichloroethene ug/L 50.250 100 71-127
trans-1,3-Dichloropropene ug/L 46.450 93 69-141
trans-1,4-Dichloro-2-butene ug/L 41.0J50 82 40-160
Trichloroethene ug/L 49.850 100 78-122
Trichlorofluoromethane ug/L 59.750 119 53-137
Vinyl acetate ug/L 102100 102 40-160
Vinyl chloride ug/L 47.550 95 58-137
Xylene (Total)ug/L 146150 98 81-126
1,2-Dichloroethane-d4 (S)%108 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%94 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1884819MATRIX SPIKE SAMPLE:
MSSpike
Result
92321720018
1,1,1,2-Tetrachloroethane ug/L 18.720 93 70-130ND
1,1,1-Trichloroethane ug/L 22.520 113 70-130ND
1,1,2,2-Tetrachloroethane ug/L 17.320 86 70-130ND
1,1,2-Trichloroethane ug/L 18.420 92 70-130ND
1,1-Dichloroethane ug/L 22.020 107 70-1300.61J
1,1-Dichloroethene ug/L 23.620 118 70-166ND
1,2,3-Trichloropropane ug/L 17.720 89 70-130ND
1,2-Dibromo-3-chloropropane ug/L 18.220 91 70-130ND
1,2-Dibromoethane (EDB)ug/L 19.320 97 70-130ND
1,2-Dichlorobenzene ug/L 18.920 94 70-130ND
1,2-Dichloroethane ug/L 19.720 98 70-130ND
1,2-Dichloropropane ug/L 19.020 95 70-130ND
1,4-Dichlorobenzene ug/L 19.220 96 70-130ND
2-Butanone (MEK)ug/L 35.9J40 90 70-130ND
2-Hexanone ug/L 32.5J40 81 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 32.0J40 80 70-130ND
Acetone ug/L 31.1J40 78 70-130ND
Acrylonitrile ug/L 88.4J100 88 70-130ND
Benzene ug/L 21.320 106 70-148ND
Bromochloromethane ug/L 21.120 106 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 66
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1884819MATRIX SPIKE SAMPLE:
MSSpike
Result
92321720018
Bromodichloromethane ug/L 20.520 103 70-130ND
Bromoform ug/L 16.420 82 70-130ND
Bromomethane ug/L 14.120 71 70-130ND
Carbon disulfide ug/L 21.8J20 109 70-130ND
Carbon tetrachloride ug/L 24.920 124 70-130ND
Chlorobenzene ug/L 20.020 100 70-146ND
Chloroethane ug/L 23.620 118 70-130ND
Chloroform ug/L 21.420 107 70-130ND
Chloromethane ug/L 20.520 102 70-130ND
cis-1,2-Dichloroethene ug/L 21.820 105 70-1300.72J
cis-1,3-Dichloropropene ug/L 18.920 95 70-130ND
Dibromochloromethane ug/L 19.020 95 70-130ND
Dibromomethane ug/L 19.720 99 70-130ND
Ethylbenzene ug/L 21.520 108 70-130ND
Iodomethane ug/L 32.940 82 70-130ND
Methylene Chloride ug/L 21.720 109 70-130ND
Styrene ug/L 21.020 105 70-130ND
Tetrachloroethene ug/L 19.920 99 70-130ND
Toluene ug/L 20.320 101 70-155ND
trans-1,2-Dichloroethene ug/L 22.720 114 70-130ND
trans-1,3-Dichloropropene ug/L 17.620 88 70-130ND
trans-1,4-Dichloro-2-butene ug/L 16.1J20 81 70-130ND
Trichloroethene ug/L 21.520 107 69-151ND
Trichlorofluoromethane ug/L 27.3 M12013670-130ND
Vinyl acetate ug/L 30.4J40 76 70-130ND
Vinyl chloride ug/L 19.720 99 70-130ND
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%106 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92321720017
1884818SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 1.1J 3 301.1J
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L 0.79J 300.70J
1,2-Dichloroethane ug/L 0.63J 300.64J
1,2-Dichloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 66
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92321720017
1884818SAMPLE DUPLICATE:
1,4-Dichlorobenzene ug/L 6.1 6 306.5
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L 0.39J 300.43J
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L 2.0J 2 302.0J
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 2.5J 1 302.6J
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%95 194
4-Bromofluorobenzene (S)%99 197
Toluene-d8 (S)%111 2109
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 66
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
339833
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92321720011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1884856
Associated Lab Samples:92321720011
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 12/08/16 00:040.33
1,1,1-Trichloroethane ug/L ND 1.0 12/08/16 00:040.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 12/08/16 00:040.40
1,1,2-Trichloroethane ug/L ND 1.0 12/08/16 00:040.29
1,1-Dichloroethane ug/L ND 5.0 12/08/16 00:040.32
1,1-Dichloroethene ug/L ND 5.0 12/08/16 00:040.56
1,2,3-Trichloropropane ug/L ND 1.0 12/08/16 00:040.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 12/08/16 00:042.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 12/08/16 00:040.27
1,2-Dichlorobenzene ug/L ND 5.0 12/08/16 00:040.30
1,2-Dichloroethane ug/L ND 1.0 12/08/16 00:040.24
1,2-Dichloropropane ug/L ND 1.0 12/08/16 00:040.27
1,4-Dichlorobenzene ug/L ND 1.0 12/08/16 00:040.33
2-Butanone (MEK)ug/L ND 100 12/08/16 00:040.96
2-Hexanone ug/L ND 50.0 12/08/16 00:040.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 12/08/16 00:040.33
Acetone ug/L ND 100 12/08/16 00:0410.0
Acrylonitrile ug/L ND 200 12/08/16 00:041.9
Benzene ug/L ND 1.0 12/08/16 00:040.25
Bromochloromethane ug/L ND 3.0 12/08/16 00:040.17
Bromodichloromethane ug/L ND 1.0 12/08/16 00:040.18
Bromoform ug/L ND 3.0 12/08/16 00:040.26
Bromomethane ug/L ND 10.0 12/08/16 00:040.29
Carbon disulfide ug/L ND 100 12/08/16 00:041.2
Carbon tetrachloride ug/L ND 1.0 12/08/16 00:040.25
Chlorobenzene ug/L ND 3.0 12/08/16 00:040.23
Chloroethane ug/L ND 10.0 12/08/16 00:040.54
Chloroform ug/L ND 5.0 12/08/16 00:040.14
Chloromethane ug/L 0.25J 1.0 12/08/16 00:040.11
cis-1,2-Dichloroethene ug/L ND 5.0 12/08/16 00:040.19
cis-1,3-Dichloropropene ug/L ND 1.0 12/08/16 00:040.13
Dibromochloromethane ug/L ND 3.0 12/08/16 00:040.21
Dibromomethane ug/L ND 10.0 12/08/16 00:040.21
Ethylbenzene ug/L ND 1.0 12/08/16 00:040.30
Iodomethane ug/L ND 10.0 12/08/16 00:040.32
Methylene Chloride ug/L ND 1.0 12/08/16 00:040.97
Styrene ug/L ND 1.0 12/08/16 00:040.26
Tetrachloroethene ug/L ND 1.0 12/08/16 00:040.46
Toluene ug/L ND 1.0 12/08/16 00:040.26
trans-1,2-Dichloroethene ug/L ND 5.0 12/08/16 00:040.49
trans-1,3-Dichloropropene ug/L ND 1.0 12/08/16 00:040.26
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1884856
Associated Lab Samples:92321720011
Matrix:Water
AnalyzedMDL
trans-1,4-Dichloro-2-butene ug/L ND 100 12/08/16 00:041.0
Trichloroethene ug/L ND 1.0 12/08/16 00:040.47
Trichlorofluoromethane ug/L ND 1.0 12/08/16 00:040.20
Vinyl acetate ug/L ND 50.0 12/08/16 00:040.35
Vinyl chloride ug/L ND 1.0 12/08/16 00:040.62
Xylene (Total)ug/L ND 5.0 12/08/16 00:040.66
1,2-Dichloroethane-d4 (S)%88 70-130 12/08/16 00:04
4-Bromofluorobenzene (S)%100 70-130 12/08/16 00:04
Toluene-d8 (S)%109 70-130 12/08/16 00:04
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1884857LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 57.450 115 80-125
1,1,1-Trichloroethane ug/L 52.450 105 71-129
1,1,2,2-Tetrachloroethane ug/L 54.550 109 79-124
1,1,2-Trichloroethane ug/L 55.750 111 85-125
1,1-Dichloroethane ug/L 47.750 95 73-126
1,1-Dichloroethene ug/L 44.750 89 66-135
1,2,3-Trichloropropane ug/L 54.350 109 75-130
1,2-Dibromo-3-chloropropane ug/L 56.650 113 71-133
1,2-Dibromoethane (EDB)ug/L 59.250 118 83-124
1,2-Dichlorobenzene ug/L 54.950 110 80-133
1,2-Dichloroethane ug/L 49.450 99 67-128
1,2-Dichloropropane ug/L 51.450 103 75-132
1,4-Dichlorobenzene ug/L 51.450 103 78-130
2-Butanone (MEK)ug/L 107100 107 61-144
2-Hexanone ug/L 124100 124 68-143
4-Methyl-2-pentanone (MIBK)ug/L 111100 111 72-135
Acetone ug/L 115100 115 48-146
Acrylonitrile ug/L 264250 106 40-160
Benzene ug/L 54.350 109 80-125
Bromochloromethane ug/L 49.550 99 71-125
Bromodichloromethane ug/L 55.650 111 78-124
Bromoform ug/L 55.950 112 71-128
Bromomethane ug/L 35.050 70 40-160
Carbon disulfide ug/L 45.3J50 91 50-160
Carbon tetrachloride ug/L 54.350 109 69-131
Chlorobenzene ug/L 51.650 103 81-122
Chloroethane ug/L 48.650 97 39-148
Chloroform ug/L 49.750 99 73-127
Chloromethane ug/L 35.550 71 44-146
cis-1,2-Dichloroethene ug/L 47.850 96 74-124
cis-1,3-Dichloropropene ug/L 50.150 100 72-132
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
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Page 53 of 66
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1884857LABORATORY CONTROL SAMPLE:
LCSSpike
Dibromochloromethane ug/L 52.850 106 78-125
Dibromomethane ug/L 50.350 101 82-120
Ethylbenzene ug/L 51.850 104 79-121
Iodomethane ug/L 85.2100 85 39-154
Methylene Chloride ug/L 44.150 88 64-133
Styrene ug/L 51.950 104 84-126
Tetrachloroethene ug/L 49.850 100 78-122
Toluene ug/L 49.250 98 80-121
trans-1,2-Dichloroethene ug/L 44.850 90 71-127
trans-1,3-Dichloropropene ug/L 55.450 111 69-141
trans-1,4-Dichloro-2-butene ug/L 61.3J50 123 40-160
Trichloroethene ug/L 54.950 110 78-122
Trichlorofluoromethane ug/L 50.950 102 53-137
Vinyl acetate ug/L 97.0100 97 40-160
Vinyl chloride ug/L 41.450 83 58-137
Xylene (Total)ug/L 151150 101 81-126
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%95 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1884859MATRIX SPIKE SAMPLE:
MSSpike
Result
92321900011
1,1,1,2-Tetrachloroethane ug/L 20.720 103 70-130ND
1,1,1-Trichloroethane ug/L 22.220 111 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.920 104 70-130ND
1,1,2-Trichloroethane ug/L 20.420 102 70-130ND
1,1-Dichloroethane ug/L 21.720 109 70-130ND
1,1-Dichloroethene ug/L 21.020 105 70-166ND
1,2,3-Trichloropropane ug/L 21.320 107 70-130ND
1,2-Dibromo-3-chloropropane ug/L 22.220 111 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.020 105 70-130ND
1,2-Dichlorobenzene ug/L 22.220 111 70-130ND
1,2-Dichloroethane ug/L 21.120 105 70-130ND
1,2-Dichloropropane ug/L 21.020 105 70-130ND
1,4-Dichlorobenzene ug/L 20.720 104 70-130ND
2-Butanone (MEK)ug/L 42.1J40 105 70-130ND
2-Hexanone ug/L 47.0J40 117 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 44.0J40 110 70-130ND
Acetone ug/L 41.2J40 101 70-130ND
Acrylonitrile ug/L 113J100 113 70-130ND
Benzene ug/L 22.920 114 70-148ND
Bromochloromethane ug/L 21.920 109 70-130ND
Bromodichloromethane ug/L 22.920 115 70-130ND
Bromoform ug/L 19.620 98 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
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Page 54 of 66
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1884859MATRIX SPIKE SAMPLE:
MSSpike
Result
92321900011
Bromomethane ug/L 17.720 88 70-130ND
Carbon disulfide ug/L 21.1J20 105 70-130ND
Carbon tetrachloride ug/L 24.420 122 70-130ND
Chlorobenzene ug/L 21.720 109 70-146ND
Chloroethane ug/L 21.520 107 70-130ND
Chloroform ug/L 21.720 109 70-130ND
Chloromethane ug/L 15.520 77 70-130ND
cis-1,2-Dichloroethene ug/L 21.420 107 70-130ND
cis-1,3-Dichloropropene ug/L 18.620 93 70-130ND
Dibromochloromethane ug/L 19.720 99 70-130ND
Dibromomethane ug/L 21.820 109 70-130ND
Ethylbenzene ug/L 22.420 112 70-130ND
Iodomethane ug/L 29.340 73 70-130ND
Methylene Chloride ug/L 18.520 92 70-130ND
Styrene ug/L 20.420 102 70-130ND
Tetrachloroethene ug/L 20.920 104 70-130ND
Toluene ug/L 22.520 112 70-155ND
trans-1,2-Dichloroethene ug/L 20.320 101 70-130ND
trans-1,3-Dichloropropene ug/L 19.320 97 70-130ND
trans-1,4-Dichloro-2-butene ug/L 18.7J20 94 70-130ND
Trichloroethene ug/L 21.820 109 69-151ND
Trichlorofluoromethane ug/L 23.020 115 70-130ND
Vinyl acetate ug/L 28.8J40 72 70-130ND
Vinyl chloride ug/L 18.920 94 70-130ND
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92321900010
1884858SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
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Page 55 of 66
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92321900010
1884858SAMPLE DUPLICATE:
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L 0.26J 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%90 192
4-Bromofluorobenzene (S)%100 1101
Toluene-d8 (S)%112 4107
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
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Page 56 of 66
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
Pace Analytical Services - GreenwoodPASI-W
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
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[phone]
Page 57 of 66
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92321720
Surry Closed- Mt Airy (UIC)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92321720011 340395MW-16 EPA 9056A
92321720001 339672 340243MW-3R EPA 3010A EPA 6010
92321720002 339672 340243MW-12S EPA 3010A EPA 6010
92321720003 339672 340243MW-15 EPA 3010A EPA 6010
92321720004 340698 340963MW-1 EPA 3010A EPA 6010
92321720005 340698 340963MW-7 EPA 3010A EPA 6010
92321720006 340698 340963MW-9 EPA 3010A EPA 6010
92321720008 340698 340963MW-13 EPA 3010A EPA 6010
92321720009 340698 340963MW-14 EPA 3010A EPA 6010
92321720011 340698 340963MW-16 EPA 3010A EPA 6010
92321720012 340698 340963MW-17 EPA 3010A EPA 6010
92321720013 340698 340963MW-18 EPA 3010A EPA 6010
92321720014 340698 340963MW-19 EPA 3010A EPA 6010
92321720015 340698 340963MW-20 EPA 3010A EPA 6010
92321720016 340698 340963MW-21 EPA 3010A EPA 6010
92321720017 340698 340963MW-22 EPA 3010A EPA 6010
92321720018 340698 340963MW-23 EPA 3010A EPA 6010
92321720001 339770MW-3R EPA 8260
92321720002 339770MW-12S EPA 8260
92321720003 339770MW-15 EPA 8260
92321720004 339770MW-1 EPA 8260
92321720005 339770MW-7 EPA 8260
92321720006 339832MW-9 EPA 8260
92321720008 339832MW-13 EPA 8260
92321720009 339832MW-14 EPA 8260
92321720011 339833MW-16 EPA 8260
92321720012 339832MW-17 EPA 8260
92321720013 339832MW-18 EPA 8260
92321720014 339832MW-19 EPA 8260
92321720015 339832MW-20 EPA 8260
92321720016 339832MW-21 EPA 8260
92321720017 339832MW-22 EPA 8260
92321720018 339832MW-23 EPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 06:06 PM
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[phone]
Page 58 of 66
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Page 60 of 66
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Page 64 of 66
Page 65 of 66
Page 66 of 66
#=CL#
December 22, 2016
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92321678
92321678
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
SURRY CLOSED-MT. AIRY (MNA)
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory between December 02,
2016 and December 06, 2016. The results relate only to the samples included in this report. Results
reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's
Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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Page 1 of 79
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 2 of 79
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Lab ID Sample ID Matrix Date Collected Date Received
92321678001 SW-1 Water 11/29/16 13:15 12/02/16 07:09
92321678002 SW-2 Water 11/29/16 13:30 12/02/16 07:09
92321678003 SW-3 Water 11/29/16 13:45 12/02/16 07:09
92321678004 SW-4 Water 11/29/16 13:00 12/02/16 07:09
92321678005 SWN-1 Water 11/30/16 08:20 12/02/16 07:09
92321678006 SWN-2 Water 11/30/16 14:10 12/02/16 07:09
92321678007 SW-A Water 11/29/16 14:20 12/02/16 07:09
92321678008 SW-B Water 11/29/16 14:20 12/02/16 07:09
92321678009 MW-1 Water 12/03/16 11:10 12/06/16 08:31
92321678010 MW-7 Water 12/03/16 10:05 12/06/16 08:31
92321678011 MW-9 Water 12/02/16 16:00 12/06/16 08:31
92321678012 MW-11 Water 12/03/16 09:05 12/06/16 08:31
92321678013 MW-14 Water 12/02/16 14:00 12/06/16 08:31
92321678014 MW-21 Water 12/02/16 17:00 12/06/16 08:31
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 3 of 79
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92321678001 SW-1 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CZDO
92321678002 SW-2 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 50 PASI-CZDO
92321678003 SW-3 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CZDO
92321678004 SW-4 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 50 PASI-CZDO
92321678005 SWN-1 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 50 PASI-CZDO
92321678006 SWN-2 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 50 PASI-CZDO
92321678007 SW-A EPA 8260 50 PASI-CZDO
92321678008 SW-B EPA 8260 50 PASI-CZDO
92321678009 MW-1 SM 2320B 1 PASI-AKDF
SM 3500-Fe B 1 PASI-ACJH1
SM 4500-S2D 1 PASI-AEWS
EPA 300.0 1 PASI-AAES2
SM 4500-Cl-E 1 PASI-AWRC
SM 5220D 1 PASI-AMDW
SM 5310B 1 PASI-AAES2
92321678010 MW-7 SM 2320B 1 PASI-AKDF
SM 3500-Fe B 1 PASI-ACJH1
SM 4500-S2D 1 PASI-AEWS
EPA 300.0 1 PASI-AAES2
SM 4500-Cl-E 1 PASI-AWRC
SM 5220D 1 PASI-AMDW
SM 5310B 1 PASI-AAES2
92321678011 MW-9 SM 2320B 1 PASI-AKDF
SM 3500-Fe B 1 PASI-ACJH1
SM 4500-S2D 1 PASI-AEWS
EPA 300.0 1 PASI-AAES2
SM 4500-Cl-E 1 PASI-AWRC
SM 5220D 1 PASI-AMDW
SM 5310B 1 PASI-AAES2
92321678012 MW-11 SM 2320B 1 PASI-AKDF
SM 3500-Fe B 1 PASI-ACJH1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 4 of 79
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
SM 4500-S2D 1 PASI-AEWS
EPA 300.0 1 PASI-AAES2
SM 4500-Cl-E 1 PASI-AWRC
SM 5220D 1 PASI-AMDW
SM 5310B 1 PASI-AAES2
92321678013 MW-14 SM 2320B 1 PASI-AKDF
SM 3500-Fe B 1 PASI-ACJH1
SM 4500-S2D 1 PASI-AEWS
EPA 300.0 1 PASI-AAES2
SM 4500-Cl-E 1 PASI-AWRC
SM 5220D 1 PASI-AMDW
SM 5310B 1 PASI-AAES2
92321678014 MW-21 SM 2320B 1 PASI-AKDF
SM 3500-Fe B 1 PASI-ACJH1
SM 4500-S2D 1 PASI-AEWS
EPA 300.0 1 PASI-AAES2
SM 4500-Cl-E 1 PASI-AWRC
SM 5220D 1 PASI-AMDW
SM 5310B 1 PASI-AAES2
REPORT OF LABORATORY ANALYSIS
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Page 5 of 79
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Sample:SW-1 Lab ID:92321678001 Collected:11/29/16 13:15 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/09/16 02:28 7440-36-012/06/16 03:306.0 3.8 1
Arsenic ND ug/L 12/09/16 02:28 7440-38-212/06/16 03:3010.0 2.5 1
Barium 27.5J ug/L 12/09/16 02:28 7440-39-312/06/16 03:301002.5 1
Beryllium ND ug/L 12/09/16 02:28 7440-41-712/06/16 03:301.0 0.50 1
Cadmium ND ug/L 12/09/16 02:28 7440-43-912/06/16 03:301.0 0.50 1
Chromium ND ug/L 12/09/16 02:28 7440-47-312/06/16 03:3010.0 2.5 1
Cobalt ND ug/L 12/09/16 02:28 7440-48-412/06/16 03:3010.0 2.5 1
Copper ND ug/L 12/09/16 02:28 7440-50-812/06/16 03:3010.0 2.5 1
Lead ND ug/L 12/09/16 02:28 7439-92-112/06/16 03:3010.0 2.5 1
Nickel ND ug/L 12/09/16 02:28 7440-02-012/06/16 03:3050.0 2.5 1
Selenium ND ug/L 12/09/16 02:28 7782-49-212/06/16 03:3010.0 5.0 1
Silver ND ug/L 12/09/16 02:28 7440-22-412/06/16 03:3010.0 2.5 1
Thallium ND ug/L 12/09/16 02:28 7440-28-012/06/16 03:305.5 5.0 1
Vanadium ND ug/L 12/09/16 02:28 7440-62-212/06/16 03:3025.0 2.5 1
Zinc ND ug/L 12/09/16 02:28 7440-66-612/06/16 03:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/08/16 00:00 67-64-110010.0 1
Acrylonitrile ND ug/L 12/08/16 00:00 107-13-12001.9 1
Benzene ND ug/L 12/08/16 00:00 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/08/16 00:00 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/08/16 00:00 75-27-41.0 0.18 1
Bromoform ND ug/L 12/08/16 00:00 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/08/16 00:00 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/08/16 00:00 78-93-31000.96 1
Carbon disulfide ND ug/L 12/08/16 00:00 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/08/16 00:00 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/08/16 00:00 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/08/16 00:00 75-00-310.0 0.54 1
Chloroform ND ug/L 12/08/16 00:00 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/08/16 00:00 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/08/16 00:00 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/08/16 00:00 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/08/16 00:00 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/08/16 00:00 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/08/16 00:00 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/08/16 00:00 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/08/16 00:00 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/08/16 00:00 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/08/16 00:00 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/08/16 00:00 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/08/16 00:00 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/08/16 00:00 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/08/16 00:00 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/08/16 00:00 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/08/16 00:00 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 79
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Sample:SW-1 Lab ID:92321678001 Collected:11/29/16 13:15 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/08/16 00:00 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/08/16 00:00 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/08/16 00:00 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/08/16 00:00 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/08/16 00:00 108-10-11000.33 1
Styrene ND ug/L 12/08/16 00:00 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/08/16 00:00 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/08/16 00:00 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/08/16 00:00 127-18-41.0 0.46 1
Toluene ND ug/L 12/08/16 00:00 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/08/16 00:00 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/08/16 00:00 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/08/16 00:00 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/08/16 00:00 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/08/16 00:00 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/08/16 00:00 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/08/16 00:00 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/08/16 00:00 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)95 %12/08/16 00:00 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %12/08/16 00:00 17060-07-070-130 1
Toluene-d8 (S)100 %12/08/16 00:00 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 79
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Sample:SW-2 Lab ID:92321678002 Collected:11/29/16 13:30 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/13/16 17:33 7440-36-012/06/16 22:256.0 3.8 1
Arsenic ND ug/L 12/13/16 17:33 7440-38-212/06/16 22:2510.0 2.5 1
Barium 30.4J ug/L 12/13/16 03:26 7440-39-312/06/16 22:251002.5 1
Beryllium ND ug/L 12/13/16 03:26 7440-41-712/06/16 22:251.0 0.50 1
Cadmium ND ug/L 12/13/16 17:33 7440-43-912/06/16 22:251.0 0.50 1
Chromium ND ug/L 12/13/16 03:26 7440-47-312/06/16 22:2510.0 2.5 1
Cobalt ND ug/L 12/13/16 17:33 7440-48-412/06/16 22:2510.0 2.5 1
Copper ND ug/L 12/13/16 17:33 7440-50-812/06/16 22:2510.0 2.5 1
Lead 3.4J ug/L 12/13/16 03:26 7439-92-112/06/16 22:2510.0 2.5 1
Nickel ND ug/L 12/13/16 03:26 7440-02-012/06/16 22:2550.0 2.5 1
Selenium ND ug/L 12/13/16 17:33 7782-49-212/06/16 22:2510.0 5.0 1
Silver ND ug/L 12/13/16 03:26 7440-22-412/06/16 22:2510.0 2.5 1
Thallium ND ug/L 12/13/16 17:33 7440-28-012/06/16 22:255.5 5.0 1
Vanadium ND ug/L 12/13/16 03:26 7440-62-212/06/16 22:2525.0 2.5 1
Zinc ND ug/L 12/13/16 03:26 7440-66-612/06/16 22:2510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/08/16 00:17 67-64-110010.0 1
Acrylonitrile ND ug/L 12/08/16 00:17 107-13-12001.9 1
Benzene ND ug/L 12/08/16 00:17 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/08/16 00:17 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/08/16 00:17 75-27-41.0 0.18 1
Bromoform ND ug/L 12/08/16 00:17 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/08/16 00:17 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/08/16 00:17 78-93-31000.96 1
Carbon disulfide ND ug/L 12/08/16 00:17 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/08/16 00:17 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/08/16 00:17 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/08/16 00:17 75-00-310.0 0.54 1
Chloroform ND ug/L 12/08/16 00:17 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/08/16 00:17 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/08/16 00:17 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/08/16 00:17 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/08/16 00:17 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/08/16 00:17 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/08/16 00:17 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/08/16 00:17 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/08/16 00:17 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/08/16 00:17 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/08/16 00:17 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/08/16 00:17 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/08/16 00:17 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/08/16 00:17 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/08/16 00:17 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/08/16 00:17 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/08/16 00:17 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 79
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Sample:SW-2 Lab ID:92321678002 Collected:11/29/16 13:30 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/08/16 00:17 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/08/16 00:17 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/08/16 00:17 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/08/16 00:17 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/08/16 00:17 108-10-11000.33 1
Styrene ND ug/L 12/08/16 00:17 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/08/16 00:17 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/08/16 00:17 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/08/16 00:17 127-18-41.0 0.46 1
Toluene ND ug/L 12/08/16 00:17 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/08/16 00:17 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/08/16 00:17 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/08/16 00:17 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/08/16 00:17 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/08/16 00:17 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/08/16 00:17 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/08/16 00:17 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/08/16 00:17 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)94 %12/08/16 00:17 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %12/08/16 00:17 17060-07-070-130 1
Toluene-d8 (S)100 %12/08/16 00:17 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 79
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Sample:SW-3 Lab ID:92321678003 Collected:11/29/16 13:45 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/13/16 17:51 7440-36-012/06/16 22:256.0 3.8 1
Arsenic ND ug/L 12/13/16 17:51 7440-38-212/06/16 22:2510.0 2.5 1
Barium 22.2J ug/L 12/13/16 17:51 7440-39-312/06/16 22:251002.5 1
Beryllium ND ug/L 12/13/16 17:51 7440-41-712/06/16 22:251.0 0.50 1
Cadmium ND ug/L 12/13/16 17:51 7440-43-912/06/16 22:251.0 0.50 1
Chromium ND ug/L 12/13/16 17:51 7440-47-312/06/16 22:2510.0 2.5 1
Cobalt ND ug/L 12/13/16 17:51 7440-48-412/06/16 22:2510.0 2.5 1
Copper ND ug/L 12/13/16 17:51 7440-50-812/06/16 22:2510.0 2.5 1
Lead ND ug/L 12/13/16 17:51 7439-92-112/06/16 22:2510.0 2.5 1
Nickel ND ug/L 12/13/16 17:51 7440-02-012/06/16 22:2550.0 2.5 1
Selenium ND ug/L 12/13/16 17:51 7782-49-212/06/16 22:2510.0 5.0 1
Silver ND ug/L 12/13/16 17:51 7440-22-412/06/16 22:2510.0 2.5 1
Thallium ND ug/L 12/13/16 17:51 7440-28-012/06/16 22:255.5 5.0 1
Vanadium ND ug/L 12/13/16 17:51 7440-62-212/06/16 22:2525.0 2.5 1
Zinc ND ug/L 12/13/16 17:51 7440-66-612/06/16 22:2510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/08/16 00:34 67-64-110010.0 1
Acrylonitrile ND ug/L 12/08/16 00:34 107-13-12001.9 1
Benzene ND ug/L 12/08/16 00:34 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/08/16 00:34 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/08/16 00:34 75-27-41.0 0.18 1
Bromoform ND ug/L 12/08/16 00:34 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/08/16 00:34 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/08/16 00:34 78-93-31000.96 1
Carbon disulfide ND ug/L 12/08/16 00:34 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/08/16 00:34 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/08/16 00:34 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/08/16 00:34 75-00-310.0 0.54 1
Chloroform ND ug/L 12/08/16 00:34 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/08/16 00:34 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/08/16 00:34 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/08/16 00:34 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/08/16 00:34 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/08/16 00:34 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/08/16 00:34 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/08/16 00:34 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/08/16 00:34 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/08/16 00:34 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/08/16 00:34 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/08/16 00:34 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/08/16 00:34 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/08/16 00:34 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/08/16 00:34 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/08/16 00:34 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/08/16 00:34 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 79
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Sample:SW-3 Lab ID:92321678003 Collected:11/29/16 13:45 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/08/16 00:34 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/08/16 00:34 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/08/16 00:34 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/08/16 00:34 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/08/16 00:34 108-10-11000.33 1
Styrene ND ug/L 12/08/16 00:34 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/08/16 00:34 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/08/16 00:34 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/08/16 00:34 127-18-41.0 0.46 1
Toluene ND ug/L 12/08/16 00:34 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/08/16 00:34 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/08/16 00:34 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/08/16 00:34 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/08/16 00:34 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/08/16 00:34 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/08/16 00:34 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/08/16 00:34 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/08/16 00:34 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)94 %12/08/16 00:34 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %12/08/16 00:34 17060-07-070-130 1
Toluene-d8 (S)99 %12/08/16 00:34 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 79
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Sample:SW-4 Lab ID:92321678004 Collected:11/29/16 13:00 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/13/16 03:48 7440-36-012/06/16 22:256.0 3.8 1
Arsenic ND ug/L 12/13/16 17:54 7440-38-212/06/16 22:2510.0 2.5 1
Barium 24.4J ug/L 12/13/16 03:48 7440-39-312/06/16 22:251002.5 1
Beryllium ND ug/L 12/13/16 03:48 7440-41-712/06/16 22:251.0 0.50 1
Cadmium ND ug/L 12/13/16 03:48 7440-43-912/06/16 22:251.0 0.50 1
Chromium ND ug/L 12/13/16 03:48 7440-47-312/06/16 22:2510.0 2.5 1
Cobalt ND ug/L 12/13/16 03:48 7440-48-412/06/16 22:2510.0 2.5 1
Copper ND ug/L 12/13/16 03:48 7440-50-812/06/16 22:2510.0 2.5 1
Lead 2.5J ug/L 12/13/16 03:48 7439-92-112/06/16 22:2510.0 2.5 1
Nickel ND ug/L 12/13/16 03:48 7440-02-012/06/16 22:2550.0 2.5 1
Selenium ND ug/L 12/13/16 17:54 7782-49-212/06/16 22:2510.0 5.0 1
Silver ND ug/L 12/13/16 03:48 7440-22-412/06/16 22:2510.0 2.5 1
Thallium ND ug/L 12/13/16 17:54 7440-28-012/06/16 22:255.5 5.0 1
Vanadium ND ug/L 12/13/16 03:48 7440-62-212/06/16 22:2525.0 2.5 1
Zinc 5.4J ug/L 12/13/16 03:48 7440-66-612/06/16 22:2510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/08/16 00:51 67-64-110010.0 1
Acrylonitrile ND ug/L 12/08/16 00:51 107-13-12001.9 1
Benzene ND ug/L 12/08/16 00:51 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/08/16 00:51 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/08/16 00:51 75-27-41.0 0.18 1
Bromoform ND ug/L 12/08/16 00:51 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/08/16 00:51 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/08/16 00:51 78-93-31000.96 1
Carbon disulfide ND ug/L 12/08/16 00:51 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/08/16 00:51 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/08/16 00:51 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/08/16 00:51 75-00-310.0 0.54 1
Chloroform ND ug/L 12/08/16 00:51 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/08/16 00:51 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/08/16 00:51 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/08/16 00:51 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/08/16 00:51 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/08/16 00:51 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/08/16 00:51 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/08/16 00:51 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/08/16 00:51 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/08/16 00:51 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/08/16 00:51 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/08/16 00:51 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/08/16 00:51 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/08/16 00:51 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/08/16 00:51 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/08/16 00:51 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/08/16 00:51 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 79
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Sample:SW-4 Lab ID:92321678004 Collected:11/29/16 13:00 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/08/16 00:51 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/08/16 00:51 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/08/16 00:51 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/08/16 00:51 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/08/16 00:51 108-10-11000.33 1
Styrene ND ug/L 12/08/16 00:51 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/08/16 00:51 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/08/16 00:51 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/08/16 00:51 127-18-41.0 0.46 1
Toluene ND ug/L 12/08/16 00:51 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/08/16 00:51 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/08/16 00:51 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/08/16 00:51 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/08/16 00:51 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/08/16 00:51 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/08/16 00:51 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/08/16 00:51 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/08/16 00:51 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)95 %12/08/16 00:51 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %12/08/16 00:51 17060-07-070-130 1
Toluene-d8 (S)98 %12/08/16 00:51 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 79
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Sample:SWN-1 Lab ID:92321678005 Collected:11/30/16 08:20 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/13/16 03:51 7440-36-012/06/16 22:256.0 3.8 1
Arsenic ND ug/L 12/13/16 17:58 7440-38-212/06/16 22:2510.0 2.5 1
Barium 31.1J ug/L 12/13/16 03:51 7440-39-312/06/16 22:251002.5 1
Beryllium ND ug/L 12/13/16 03:51 7440-41-712/06/16 22:251.0 0.50 1
Cadmium ND ug/L 12/13/16 03:51 7440-43-912/06/16 22:251.0 0.50 1
Chromium ND ug/L 12/13/16 03:51 7440-47-312/06/16 22:2510.0 2.5 1
Cobalt ND ug/L 12/13/16 03:51 7440-48-412/06/16 22:2510.0 2.5 1
Copper ND ug/L 12/13/16 03:51 7440-50-812/06/16 22:2510.0 2.5 1
Lead ND ug/L 12/13/16 03:51 7439-92-112/06/16 22:2510.0 2.5 1
Nickel ND ug/L 12/13/16 03:51 7440-02-012/06/16 22:2550.0 2.5 1
Selenium ND ug/L 12/13/16 17:58 7782-49-212/06/16 22:2510.0 5.0 1
Silver ND ug/L 12/13/16 03:51 7440-22-412/06/16 22:2510.0 2.5 1
Thallium ND ug/L 12/13/16 17:58 7440-28-012/06/16 22:255.5 5.0 1
Vanadium ND ug/L 12/13/16 03:51 7440-62-212/06/16 22:2525.0 2.5 1
Zinc ND ug/L 12/13/16 03:51 7440-66-612/06/16 22:2510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/08/16 01:08 67-64-110010.0 1
Acrylonitrile ND ug/L 12/08/16 01:08 107-13-12001.9 1
Benzene ND ug/L 12/08/16 01:08 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/08/16 01:08 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/08/16 01:08 75-27-41.0 0.18 1
Bromoform ND ug/L 12/08/16 01:08 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/08/16 01:08 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/08/16 01:08 78-93-31000.96 1
Carbon disulfide ND ug/L 12/08/16 01:08 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/08/16 01:08 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/08/16 01:08 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/08/16 01:08 75-00-310.0 0.54 1
Chloroform ND ug/L 12/08/16 01:08 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/08/16 01:08 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/08/16 01:08 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/08/16 01:08 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/08/16 01:08 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/08/16 01:08 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/08/16 01:08 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/08/16 01:08 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/08/16 01:08 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/08/16 01:08 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/08/16 01:08 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/08/16 01:08 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/08/16 01:08 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/08/16 01:08 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/08/16 01:08 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/08/16 01:08 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/08/16 01:08 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 79
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Sample:SWN-1 Lab ID:92321678005 Collected:11/30/16 08:20 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/08/16 01:08 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/08/16 01:08 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/08/16 01:08 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/08/16 01:08 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/08/16 01:08 108-10-11000.33 1
Styrene ND ug/L 12/08/16 01:08 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/08/16 01:08 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/08/16 01:08 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/08/16 01:08 127-18-41.0 0.46 1
Toluene ND ug/L 12/08/16 01:08 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/08/16 01:08 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/08/16 01:08 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/08/16 01:08 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/08/16 01:08 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/08/16 01:08 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/08/16 01:08 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/08/16 01:08 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/08/16 01:08 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)95 %12/08/16 01:08 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %12/08/16 01:08 17060-07-070-130 1
Toluene-d8 (S)100 %12/08/16 01:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 79
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Sample:SWN-2 Lab ID:92321678006 Collected:11/30/16 14:10 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/13/16 03:54 7440-36-012/06/16 22:256.0 3.8 1
Arsenic ND ug/L 12/13/16 18:01 7440-38-212/06/16 22:2510.0 2.5 1
Barium 25.3J ug/L 12/13/16 03:54 7440-39-312/06/16 22:251002.5 1
Beryllium ND ug/L 12/13/16 03:54 7440-41-712/06/16 22:251.0 0.50 1
Cadmium ND ug/L 12/13/16 03:54 7440-43-912/06/16 22:251.0 0.50 1
Chromium ND ug/L 12/13/16 03:54 7440-47-312/06/16 22:2510.0 2.5 1
Cobalt ND ug/L 12/13/16 03:54 7440-48-412/06/16 22:2510.0 2.5 1
Copper ND ug/L 12/13/16 03:54 7440-50-812/06/16 22:2510.0 2.5 1
Lead ND ug/L 12/13/16 03:54 7439-92-112/06/16 22:2510.0 2.5 1
Nickel ND ug/L 12/13/16 03:54 7440-02-012/06/16 22:2550.0 2.5 1
Selenium ND ug/L 12/13/16 18:01 7782-49-212/06/16 22:2510.0 5.0 1
Silver ND ug/L 12/13/16 03:54 7440-22-412/06/16 22:2510.0 2.5 1
Thallium ND ug/L 12/13/16 18:01 7440-28-012/06/16 22:255.5 5.0 1
Vanadium ND ug/L 12/13/16 03:54 7440-62-212/06/16 22:2525.0 2.5 1
Zinc 5.3J ug/L 12/13/16 03:54 7440-66-612/06/16 22:2510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/08/16 01:26 67-64-110010.0 1
Acrylonitrile ND ug/L 12/08/16 01:26 107-13-12001.9 1
Benzene ND ug/L 12/08/16 01:26 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/08/16 01:26 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/08/16 01:26 75-27-41.0 0.18 1
Bromoform ND ug/L 12/08/16 01:26 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/08/16 01:26 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/08/16 01:26 78-93-31000.96 1
Carbon disulfide ND ug/L 12/08/16 01:26 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/08/16 01:26 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/08/16 01:26 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/08/16 01:26 75-00-310.0 0.54 1
Chloroform ND ug/L 12/08/16 01:26 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/08/16 01:26 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/08/16 01:26 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/08/16 01:26 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/08/16 01:26 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/08/16 01:26 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/08/16 01:26 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/08/16 01:26 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/08/16 01:26 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/08/16 01:26 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/08/16 01:26 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/08/16 01:26 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/08/16 01:26 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/08/16 01:26 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/08/16 01:26 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/08/16 01:26 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/08/16 01:26 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 79
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Sample:SWN-2 Lab ID:92321678006 Collected:11/30/16 14:10 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/08/16 01:26 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/08/16 01:26 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/08/16 01:26 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/08/16 01:26 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/08/16 01:26 108-10-11000.33 1
Styrene ND ug/L 12/08/16 01:26 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/08/16 01:26 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/08/16 01:26 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/08/16 01:26 127-18-41.0 0.46 1
Toluene ND ug/L 12/08/16 01:26 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/08/16 01:26 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/08/16 01:26 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/08/16 01:26 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/08/16 01:26 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/08/16 01:26 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/08/16 01:26 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/08/16 01:26 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/08/16 01:26 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)95 %12/08/16 01:26 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %12/08/16 01:26 17060-07-070-130 1
Toluene-d8 (S)97 %12/08/16 01:26 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 79
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Sample:SW-A Lab ID:92321678007 Collected:11/29/16 14:20 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/08/16 01:43 67-64-110010.0 1
Acrylonitrile ND ug/L 12/08/16 01:43 107-13-12001.9 1
Benzene ND ug/L 12/08/16 01:43 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/08/16 01:43 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/08/16 01:43 75-27-41.0 0.18 1
Bromoform ND ug/L 12/08/16 01:43 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/08/16 01:43 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/08/16 01:43 78-93-31000.96 1
Carbon disulfide ND ug/L 12/08/16 01:43 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/08/16 01:43 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/08/16 01:43 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/08/16 01:43 75-00-310.0 0.54 1
Chloroform ND ug/L 12/08/16 01:43 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/08/16 01:43 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/08/16 01:43 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/08/16 01:43 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/08/16 01:43 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/08/16 01:43 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/08/16 01:43 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/08/16 01:43 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/08/16 01:43 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/08/16 01:43 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/08/16 01:43 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/08/16 01:43 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/08/16 01:43 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/08/16 01:43 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/08/16 01:43 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/08/16 01:43 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/08/16 01:43 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 12/08/16 01:43 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/08/16 01:43 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/08/16 01:43 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/08/16 01:43 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/08/16 01:43 108-10-11000.33 1
Styrene ND ug/L 12/08/16 01:43 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/08/16 01:43 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/08/16 01:43 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/08/16 01:43 127-18-41.0 0.46 1
Toluene ND ug/L 12/08/16 01:43 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/08/16 01:43 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/08/16 01:43 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/08/16 01:43 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/08/16 01:43 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/08/16 01:43 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/08/16 01:43 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/08/16 01:43 75-01-41.0 0.62 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
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Page 18 of 79
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Sample:SW-A Lab ID:92321678007 Collected:11/29/16 14:20 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Xylene (Total)ND ug/L 12/08/16 01:43 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)95 %12/08/16 01:43 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %12/08/16 01:43 17060-07-070-130 1
Toluene-d8 (S)99 %12/08/16 01:43 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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Page 19 of 79
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Sample:SW-B Lab ID:92321678008 Collected:11/29/16 14:20 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/08/16 02:00 67-64-110010.0 1
Acrylonitrile ND ug/L 12/08/16 02:00 107-13-12001.9 1
Benzene ND ug/L 12/08/16 02:00 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/08/16 02:00 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/08/16 02:00 75-27-41.0 0.18 1
Bromoform ND ug/L 12/08/16 02:00 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/08/16 02:00 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/08/16 02:00 78-93-31000.96 1
Carbon disulfide ND ug/L 12/08/16 02:00 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/08/16 02:00 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/08/16 02:00 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/08/16 02:00 75-00-310.0 0.54 1
Chloroform ND ug/L 12/08/16 02:00 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/08/16 02:00 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/08/16 02:00 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/08/16 02:00 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/08/16 02:00 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/08/16 02:00 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/08/16 02:00 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/08/16 02:00 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/08/16 02:00 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/08/16 02:00 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/08/16 02:00 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/08/16 02:00 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/08/16 02:00 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/08/16 02:00 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/08/16 02:00 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/08/16 02:00 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/08/16 02:00 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 12/08/16 02:00 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/08/16 02:00 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/08/16 02:00 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/08/16 02:00 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/08/16 02:00 108-10-11000.33 1
Styrene ND ug/L 12/08/16 02:00 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/08/16 02:00 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/08/16 02:00 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/08/16 02:00 127-18-41.0 0.46 1
Toluene ND ug/L 12/08/16 02:00 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/08/16 02:00 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/08/16 02:00 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/08/16 02:00 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/08/16 02:00 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/08/16 02:00 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/08/16 02:00 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/08/16 02:00 75-01-41.0 0.62 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 79
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Sample:SW-B Lab ID:92321678008 Collected:11/29/16 14:20 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Xylene (Total)ND ug/L 12/08/16 02:00 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)95 %12/08/16 02:00 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %12/08/16 02:00 17060-07-070-130 1
Toluene-d8 (S)100 %12/08/16 02:00 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
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Page 21 of 79
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Sample:MW-1 Lab ID:92321678009 Collected:12/03/16 11:10 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 132000 ug/L 12/08/16 02:44500010001
Analytical Method: SM 3500-Fe BIron, Ferrous
Iron, Ferrous ND mg/L 12/13/16 03:39 H3,N20.50 0.50 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 12/08/16 09:45 18496-25-810001001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 8580J ug/L 12/09/16 18:08 14808-79-825000010001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 3930 ug/L 12/19/16 18:41 16887-00-610005001
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 27000 ug/L 12/08/16 00:2825000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon ND ug/L 12/17/16 03:43 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 79
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Sample:MW-7 Lab ID:92321678010 Collected:12/03/16 10:05 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 53200 ug/L 12/08/16 02:55500010001
Analytical Method: SM 3500-Fe BIron, Ferrous
Iron, Ferrous ND mg/L 12/13/16 03:39 H3,N20.50 0.50 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 12/08/16 10:15 18496-25-810001001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 3740J ug/L 12/09/16 18:17 14808-79-825000010001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 25000 ug/L 12/19/16 18:44 16887-00-6400020004
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 27000 ug/L 12/08/16 00:2825000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 2680 ug/L 12/17/16 03:53 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 79
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Sample:MW-9 Lab ID:92321678011 Collected:12/02/16 16:00 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 39300 ug/L 12/08/16 01:45500010001
Analytical Method: SM 3500-Fe BIron, Ferrous
Iron, Ferrous 4.7 mg/L 12/13/16 03:39 H3,N21.0 1.0 2
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 12/08/16 09:45 18496-25-810001001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 2090J ug/L 12/09/16 18:45 14808-79-825000010001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 29400 ug/L 12/19/16 18:45 16887-00-6400020004
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 27000 ug/L 12/08/16 00:2825000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 1540 ug/L 12/17/16 04:06 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 79
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Sample:MW-11 Lab ID:92321678012 Collected:12/03/16 09:05 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 35300 ug/L 12/08/16 03:26500010001
Analytical Method: SM 3500-Fe BIron, Ferrous
Iron, Ferrous 2.6 mg/L 12/13/16 03:39 H3,N20.50 0.50 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide 699J ug/L 12/08/16 10:15 18496-25-810001001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 7510J ug/L 12/09/16 18:54 14808-79-825000010001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 9580 ug/L 12/19/16 18:46 16887-00-6400020004
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 14000J ug/L 12/08/16 00:2825000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 1920 ug/L 12/17/16 04:20 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 79
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Sample:MW-14 Lab ID:92321678013 Collected:12/02/16 14:00 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 42400 ug/L 12/08/16 01:57500010001
Analytical Method: SM 3500-Fe BIron, Ferrous
Iron, Ferrous ND mg/L 12/13/16 03:39 H3,N20.50 0.50 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 12/08/16 09:45 18496-25-810001001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 2880J ug/L 12/09/16 19:03 14808-79-825000010001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 4180 ug/L 12/19/16 18:47 16887-00-610005001
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand ND ug/L 12/08/16 00:2825000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 2870 ug/L 12/17/16 04:35 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 79
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Sample:MW-21 Lab ID:92321678014 Collected:12/02/16 17:00 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 41000 ug/L 12/08/16 02:33500010001
Analytical Method: SM 3500-Fe BIron, Ferrous
Iron, Ferrous ND mg/L 12/13/16 03:39 H3,N20.50 0.50 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 12/08/16 09:45 18496-25-810001001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 2570J ug/L 12/09/16 19:12 14808-79-825000010001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 29900 ug/L 12/19/16 18:47 16887-00-6 M110005001
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 19000J ug/L 12/08/16 00:2825000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 2430 ug/L 12/17/16 04:47 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 79
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
339257
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92321678001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1881364
Associated Lab Samples:92321678001
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 12/09/16 00:573.8
Arsenic ug/L 2.7J 10.0 12/09/16 00:572.5
Barium ug/L ND 100 12/09/16 00:572.5
Beryllium ug/L ND 1.0 12/09/16 00:570.50
Cadmium ug/L ND 1.0 12/09/16 00:570.50
Chromium ug/L ND 10.0 12/09/16 00:572.5
Cobalt ug/L ND 10.0 12/09/16 00:572.5
Copper ug/L ND 10.0 12/09/16 00:572.5
Lead ug/L ND 10.0 12/09/16 00:572.5
Nickel ug/L ND 50.0 12/09/16 00:572.5
Selenium ug/L ND 10.0 12/09/16 00:575.0
Silver ug/L ND 10.0 12/09/16 00:572.5
Thallium ug/L ND 5.5 12/09/16 00:575.0
Vanadium ug/L ND 25.0 12/09/16 00:572.5
Zinc ug/L ND 10.0 12/09/16 00:575.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1881365LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 440500 88 80-120
Arsenic ug/L 447500 89 80-120
Barium ug/L 458500 92 80-120
Beryllium ug/L 482500 96 80-120
Cadmium ug/L 448500 90 80-120
Chromium ug/L 482500 96 80-120
Cobalt ug/L 461500 92 80-120
Copper ug/L 475500 95 80-120
Lead ug/L 455500 91 80-120
Nickel ug/L 447500 89 80-120
Selenium ug/L 450500 90 80-120
Silver ug/L 235250 94 80-120
Thallium ug/L 447500 89 80-120
Vanadium ug/L 463500 93 80-120
Zinc ug/L 483500 97 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 79
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1881366MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92320983001
1881367
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 88 75-12586 3 25500ND442428
Arsenic ug/L 500 88 75-12587 2 25500ND444434
Barium ug/L 500 92 75-12589 4 25500ND460443
Beryllium ug/L 500 96 75-12595 1 25500ND478474
Cadmium ug/L 500 89 75-12586 3 25500ND444431
Chromium ug/L 500 96 75-12593 3 25500ND480468
Cobalt ug/L 500 92 75-12590 2 25500ND462452
Copper ug/L 500 94 75-12591 4 25500ND471455
Lead ug/L 500 91 75-12589 2 25500ND454446
Nickel ug/L 500 89 75-12587 3 25500ND446434
Selenium ug/L 500 88 75-12586 3 25500ND442431
Silver ug/L 250 93 75-12593 0 25250ND234233
Thallium ug/L 500 90 75-12589 0 25500ND450449
Vanadium ug/L 500 92 75-12593 1 25500ND462466
Zinc ug/L 500 97 75-12597 0 25500ND487488
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 79
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
339341
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92321678002, 92321678003, 92321678004, 92321678005, 92321678006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1881715
Associated Lab Samples:92321678002, 92321678003, 92321678004, 92321678005, 92321678006
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 12/13/16 17:273.8
Arsenic ug/L ND 10.0 12/13/16 17:272.5
Barium ug/L ND 100 12/13/16 03:202.5
Beryllium ug/L ND 1.0 12/13/16 03:200.50
Cadmium ug/L ND 1.0 12/13/16 17:270.50
Chromium ug/L ND 10.0 12/13/16 03:202.5
Cobalt ug/L ND 10.0 12/13/16 17:272.5
Copper ug/L ND 10.0 12/13/16 17:272.5
Lead ug/L ND 10.0 12/13/16 03:202.5
Nickel ug/L ND 50.0 12/13/16 03:202.5
Selenium ug/L ND 10.0 12/13/16 17:275.0
Silver ug/L ND 10.0 12/13/16 03:202.5
Thallium ug/L ND 5.5 12/13/16 17:275.0
Vanadium ug/L ND 25.0 12/13/16 03:202.5
Zinc ug/L ND 10.0 12/13/16 03:205.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1881716LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 506500 101 80-120
Arsenic ug/L 491500 98 80-120
Barium ug/L 482500 96 80-120
Beryllium ug/L 498500 100 80-120
Cadmium ug/L 499500 100 80-120
Chromium ug/L 508500 102 80-120
Cobalt ug/L 510500 102 80-120
Copper ug/L 507500 101 80-120
Lead ug/L 477500 95 80-120
Nickel ug/L 474500 95 80-120
Selenium ug/L 503500 101 80-120
Silver ug/L 237250 95 80-120
Thallium ug/L 439500 88 80-120
Vanadium ug/L 487500 97 80-120
Zinc ug/L 513500 103 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 79
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1881717MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321678002
1881718
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 97 75-12597 0 25500ND483483
Arsenic ug/L 500 94 75-12593 1 25500ND468464
Barium ug/L 500 94 75-12598 3 2550030.4J 502 519
Beryllium ug/L 500 97 75-12597 0 25500ND488487
Cadmium ug/L 500 95 75-12596 1 25500ND478482
Chromium ug/L 500 100 75-12599 1 25500ND498494
Cobalt ug/L 500 97 75-12597 0 25500ND484486
Copper ug/L 500 98 75-12598 0 25500ND490493
Lead ug/L 500 92 75-12592 1 255003.4J 463 461
Nickel ug/L 500 92 75-12593 0 25500ND462463
Selenium ug/L 500 97 75-12597 1 25500ND487484
Silver ug/L 250 93 75-12593 0 25250ND232232
Thallium ug/L 500 85 75-12584 2 25500ND426419
Vanadium ug/L 500 95 75-12595 1 25500ND478475
Zinc ug/L 500 100 75-125100 1 25500ND504500
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 79
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
339748
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92321678001, 92321678002, 92321678003, 92321678004, 92321678005, 92321678006, 92321678007,
92321678008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1884227
Associated Lab Samples:92321678001, 92321678002, 92321678003, 92321678004, 92321678005, 92321678006, 92321678007,
92321678008
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 12/07/16 21:260.33
1,1,1-Trichloroethane ug/L ND 1.0 12/07/16 21:260.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 12/07/16 21:260.40
1,1,2-Trichloroethane ug/L ND 1.0 12/07/16 21:260.29
1,1-Dichloroethane ug/L ND 5.0 12/07/16 21:260.32
1,1-Dichloroethene ug/L ND 5.0 12/07/16 21:260.56
1,2,3-Trichloropropane ug/L ND 1.0 12/07/16 21:260.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 12/07/16 21:262.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 12/07/16 21:260.27
1,2-Dichlorobenzene ug/L ND 5.0 12/07/16 21:260.30
1,2-Dichloroethane ug/L ND 1.0 12/07/16 21:260.24
1,2-Dichloropropane ug/L ND 1.0 12/07/16 21:260.27
1,4-Dichlorobenzene ug/L ND 1.0 12/07/16 21:260.33
2-Butanone (MEK)ug/L ND 100 12/07/16 21:260.96
2-Hexanone ug/L ND 50.0 12/07/16 21:260.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 12/07/16 21:260.33
Acetone ug/L ND 100 12/07/16 21:2610.0
Acrylonitrile ug/L ND 200 12/07/16 21:261.9
Benzene ug/L ND 1.0 12/07/16 21:260.25
Bromochloromethane ug/L ND 3.0 12/07/16 21:260.17
Bromodichloromethane ug/L ND 1.0 12/07/16 21:260.18
Bromoform ug/L ND 3.0 12/07/16 21:260.26
Bromomethane ug/L ND 10.0 12/07/16 21:260.29
Carbon disulfide ug/L ND 100 12/07/16 21:261.2
Carbon tetrachloride ug/L ND 1.0 12/07/16 21:260.25
Chlorobenzene ug/L ND 3.0 12/07/16 21:260.23
Chloroethane ug/L ND 10.0 12/07/16 21:260.54
Chloroform ug/L ND 5.0 12/07/16 21:260.14
Chloromethane ug/L ND 1.0 12/07/16 21:260.11
cis-1,2-Dichloroethene ug/L ND 5.0 12/07/16 21:260.19
cis-1,3-Dichloropropene ug/L ND 1.0 12/07/16 21:260.13
Dibromochloromethane ug/L ND 3.0 12/07/16 21:260.21
Dibromomethane ug/L ND 10.0 12/07/16 21:260.21
Ethylbenzene ug/L ND 1.0 12/07/16 21:260.30
Iodomethane ug/L ND 10.0 12/07/16 21:260.32
Methylene Chloride ug/L ND 1.0 12/07/16 21:260.97
Styrene ug/L ND 1.0 12/07/16 21:260.26
Tetrachloroethene ug/L ND 1.0 12/07/16 21:260.46
Toluene ug/L ND 1.0 12/07/16 21:260.26
trans-1,2-Dichloroethene ug/L ND 5.0 12/07/16 21:260.49
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 79
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1884227
Associated Lab Samples:92321678001, 92321678002, 92321678003, 92321678004, 92321678005, 92321678006, 92321678007,
92321678008
Matrix:Water
AnalyzedMDL
trans-1,3-Dichloropropene ug/L ND 1.0 12/07/16 21:260.26
trans-1,4-Dichloro-2-butene ug/L ND 100 12/07/16 21:261.0
Trichloroethene ug/L ND 1.0 12/07/16 21:260.47
Trichlorofluoromethane ug/L ND 1.0 12/07/16 21:260.20
Vinyl acetate ug/L ND 50.0 12/07/16 21:260.35
Vinyl chloride ug/L ND 1.0 12/07/16 21:260.62
Xylene (Total)ug/L ND 5.0 12/07/16 21:260.66
1,2-Dichloroethane-d4 (S)%100 70-130 12/07/16 21:26
4-Bromofluorobenzene (S)%95 70-130 12/07/16 21:26
Toluene-d8 (S)%98 70-130 12/07/16 21:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1884228LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 46.550 93 80-125
1,1,1-Trichloroethane ug/L 46.450 93 71-129
1,1,2,2-Tetrachloroethane ug/L 48.750 97 79-124
1,1,2-Trichloroethane ug/L 46.150 92 85-125
1,1-Dichloroethane ug/L 48.950 98 73-126
1,1-Dichloroethene ug/L 50.050 100 66-135
1,2,3-Trichloropropane ug/L 47.650 95 75-130
1,2-Dibromo-3-chloropropane ug/L 50.250 100 71-133
1,2-Dibromoethane (EDB)ug/L 48.850 98 83-124
1,2-Dichlorobenzene ug/L 49.650 99 80-133
1,2-Dichloroethane ug/L 43.850 88 67-128
1,2-Dichloropropane ug/L 46.450 93 75-132
1,4-Dichlorobenzene ug/L 47.650 95 78-130
2-Butanone (MEK)ug/L 108100 108 61-144
2-Hexanone ug/L 108100 108 68-143
4-Methyl-2-pentanone (MIBK)ug/L 100100 100 72-135
Acetone ug/L 113100 113 48-146
Acrylonitrile ug/L 268250 107 40-160
Benzene ug/L 49.250 98 80-125
Bromochloromethane ug/L 48.550 97 71-125
Bromodichloromethane ug/L 47.650 95 78-124
Bromoform ug/L 44.850 90 71-128
Bromomethane ug/L 41.650 83 40-160
Carbon disulfide ug/L 54.1J50 108 50-160
Carbon tetrachloride ug/L 46.850 94 69-131
Chlorobenzene ug/L 46.850 94 81-122
Chloroethane ug/L 46.550 93 39-148
Chloroform ug/L 47.550 95 73-127
Chloromethane ug/L 49.450 99 44-146
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 79
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1884228LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 48.250 96 74-124
cis-1,3-Dichloropropene ug/L 46.450 93 72-132
Dibromochloromethane ug/L 48.750 97 78-125
Dibromomethane ug/L 45.450 91 82-120
Ethylbenzene ug/L 48.450 97 79-121
Iodomethane ug/L 91.7100 92 39-154
Methylene Chloride ug/L 49.250 98 64-133
Styrene ug/L 48.250 96 84-126
Tetrachloroethene ug/L 42.550 85 78-122
Toluene ug/L 47.250 94 80-121
trans-1,2-Dichloroethene ug/L 49.650 99 71-127
trans-1,3-Dichloropropene ug/L 46.350 93 69-141
trans-1,4-Dichloro-2-butene ug/L 57.6J50 115 40-160
Trichloroethene ug/L 45.450 91 78-122
Trichlorofluoromethane ug/L 52.050 104 53-137
Vinyl acetate ug/L 106100 106 40-160
Vinyl chloride ug/L 42.650 85 58-137
Xylene (Total)ug/L 143150 96 81-126
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1884229MATRIX SPIKE SAMPLE:
MSSpike
Result
92321673001
1,1,1,2-Tetrachloroethane ug/L 19.920 100 70-130ND
1,1,1-Trichloroethane ug/L 20.620 103 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.020 100 70-130ND
1,1,2-Trichloroethane ug/L 19.620 98 70-130ND
1,1-Dichloroethane ug/L 21.120 106 70-130ND
1,1-Dichloroethene ug/L 23.120 115 70-166ND
1,2,3-Trichloropropane ug/L 18.820 94 70-130ND
1,2-Dibromo-3-chloropropane ug/L 20.220 101 70-130ND
1,2-Dibromoethane (EDB)ug/L 20.420 102 70-130ND
1,2-Dichlorobenzene ug/L 20.520 102 70-130ND
1,2-Dichloroethane ug/L 19.720 98 70-130ND
1,2-Dichloropropane ug/L 19.420 97 70-130ND
1,4-Dichlorobenzene ug/L 19.820 99 70-130ND
2-Butanone (MEK)ug/L 42.5J40 106 70-130ND
2-Hexanone ug/L 42.4J40 106 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 40.4J40 101 70-130ND
Acetone ug/L 42.4J40 89 70-130ND
Acrylonitrile ug/L 111J100 111 70-130ND
Benzene ug/L 21.520 108 70-148ND
Bromochloromethane ug/L 21.320 107 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 79
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1884229MATRIX SPIKE SAMPLE:
MSSpike
Result
92321673001
Bromodichloromethane ug/L 20.320 102 70-130ND
Bromoform ug/L 18.120 90 70-130ND
Bromomethane ug/L 17.620 88 70-130ND
Carbon disulfide ug/L 25.2J20 123 70-130ND
Carbon tetrachloride ug/L 20.420 102 70-130ND
Chlorobenzene ug/L 20.320 101 70-146ND
Chloroethane ug/L 21.020 105 70-130ND
Chloroform ug/L 20.520 102 70-130ND
Chloromethane ug/L 23.020 112 70-1300.66J
cis-1,2-Dichloroethene ug/L 21.320 107 70-130ND
cis-1,3-Dichloropropene ug/L 18.420 92 70-130ND
Dibromochloromethane ug/L 20.420 102 70-130ND
Dibromomethane ug/L 19.220 96 70-130ND
Ethylbenzene ug/L 20.820 104 70-130ND
Iodomethane ug/L 37.840 95 70-130ND
Methylene Chloride ug/L 20.420 102 70-130ND
Styrene ug/L 20.220 101 70-130ND
Tetrachloroethene ug/L 18.420 92 70-130ND
Toluene ug/L 20.720 103 70-155ND
trans-1,2-Dichloroethene ug/L 22.520 113 70-130ND
trans-1,3-Dichloropropene ug/L 18.520 93 70-130ND
trans-1,4-Dichloro-2-butene ug/L 17.3J20 86 70-130ND
Trichloroethene ug/L 20.120 101 69-151ND
Trichlorofluoromethane ug/L 23.620 118 70-130ND
Vinyl acetate ug/L 35.7J40 89 70-130ND
Vinyl chloride ug/L 19.220 96 70-130ND
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%95 70-130
Toluene-d8 (S)%96 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92321673002
1884230SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 5.4 4 305.2
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 79
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92321673002
1884230SAMPLE DUPLICATE:
1,4-Dichlorobenzene ug/L 0.70J 300.71J
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 3016.3J
Acrylonitrile ug/L ND 30ND
Benzene ug/L 0.71J 300.74J
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L 0.73J 30ND
Carbon disulfide ug/L 4.3J 301.6J
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L 1.7J 24 301.4
Chloroform ug/L ND 30ND
Chloromethane ug/L 9.6 27 3012.6
cis-1,2-Dichloroethene ug/L 2.6J 1 302.6
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L 0.95J 300.90J
Trichlorofluoromethane ug/L 1.5 11 301.3
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%89 12100
4-Bromofluorobenzene (S)%99 495
Toluene-d8 (S)%107 898
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 79
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
339686
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92321678009, 92321678010, 92321678011, 92321678012, 92321678013, 92321678014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1883899
Associated Lab Samples:92321678009, 92321678010, 92321678011, 92321678012, 92321678013, 92321678014
Matrix:Water
AnalyzedMDL
Alkalinity, Total as CaCO3 ug/L ND 5000 12/07/16 22:511000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1883900LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 ug/L 4920050000 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1883901MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321915018
1883902
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L M1500004780-12040 16 2550000ND2360020000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1883903MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321678013
1883904
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L 50000 98 80-120100 1 2550000424009150092600
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 79
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
340277
SM 3500-Fe B
SM 3500-Fe B
Iron, Ferrous
Associated Lab Samples:92321678009, 92321678010, 92321678011, 92321678012, 92321678013, 92321678014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1887534
Associated Lab Samples:92321678009, 92321678010, 92321678011, 92321678012, 92321678013, 92321678014
Matrix:Water
AnalyzedMDL
Iron, Ferrous mg/L ND 0.50 N212/13/16 03:390.50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1887535LABORATORY CONTROL SAMPLE:
LCSSpike
Iron, Ferrous mg/L 1.5 N21.5 102 90-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92321732001
1887536SAMPLE DUPLICATE:
Iron, Ferrous mg/L 2.5 H1,N21102.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 79
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
339811
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92321678009, 92321678011, 92321678013, 92321678014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1884626
Associated Lab Samples:92321678009, 92321678011, 92321678013, 92321678014
Matrix:Water
AnalyzedMDL
Sulfide ug/L ND 1000 12/08/16 09:45100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1884627LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 512J500 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1884628MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321792004
1884629
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 105 80-120105 0 10500ND526J524J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1884630MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321792014
1884631
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 106 80-120106 0 10500ND582J582J
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
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Page 39 of 79
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
339813
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92321678010, 92321678012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1884638
Associated Lab Samples:92321678010, 92321678012
Matrix:Water
AnalyzedMDL
Sulfide ug/L ND 1000 12/08/16 10:15100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1884639LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 524J500 105 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1884640MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321678010
1884641
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 84 80-12084 1 10500ND441J438J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1884642MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321905009
1884643
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 105 80-120105 0 10500ND526J524J
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 79
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
340189
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92321678009, 92321678010, 92321678011, 92321678012, 92321678013, 92321678014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1886795
Associated Lab Samples:92321678009, 92321678010, 92321678011, 92321678012, 92321678013, 92321678014
Matrix:Water
AnalyzedMDL
Sulfate ug/L ND 250000 12/09/16 15:061000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1886796LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 18900J20000 94 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1886797MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321623024
1886798
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L M6200009890-11058 2 1020000398 mg/L 417000J 409000J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1886799MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321900004
1886800
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L 20000 99 90-110101 1 10200001000029800J30200J
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
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Huntersville, NC 28078
[phone]
Page 41 of 79
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
341242
SM 4500-Cl-E
SM 4500-Cl-E
4500 Chloride
Associated Lab Samples:92321678009, 92321678010, 92321678011, 92321678012, 92321678013, 92321678014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1893040
Associated Lab Samples:92321678009, 92321678010, 92321678011, 92321678012, 92321678013, 92321678014
Matrix:Water
AnalyzedMDL
Chloride ug/L ND 1000 12/19/16 18:33500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1893041LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride ug/L 2040020000 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1893042MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92322679001
1893043
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L M6100006990-11071 0 101000076.9 mg/L 83800 84000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1893044MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321678014
1893045
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L M1100008890-11092 1 1010000299003880039100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
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Huntersville, NC 28078
[phone]
Page 42 of 79
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
339822
SM 5220D
SM 5220D
5220D COD
Associated Lab Samples:92321678009, 92321678010, 92321678011, 92321678012, 92321678013, 92321678014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1884712
Associated Lab Samples:92321678009, 92321678010, 92321678011, 92321678012, 92321678013, 92321678014
Matrix:Water
AnalyzedMDL
Chemical Oxygen Demand ug/L ND 25000 12/08/16 00:2812500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1884713LABORATORY CONTROL SAMPLE:
LCSSpike
Chemical Oxygen Demand ug/L 777000750000 104 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1884714MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92322011002
1884715
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L 750000 97 90-11097 0 3750000195 mg/L 925000 923000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1884716MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92322129001
1884717
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L 750000 101 90-110100 1 3750000141 mg/L 898000 893000
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
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Huntersville, NC 28078
[phone]
Page 43 of 79
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
341127
SM 5310B
SM 5310B
5310B TOC
Associated Lab Samples:92321678009, 92321678010, 92321678011, 92321678012, 92321678013, 92321678014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1892535
Associated Lab Samples:92321678009, 92321678010, 92321678011, 92321678012, 92321678013, 92321678014
Matrix:Water
AnalyzedMDL
Total Organic Carbon ug/L ND 1000 12/17/16 00:59500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1892537LABORATORY CONTROL SAMPLE:
LCSSpike
Total Organic Carbon ug/L 2500025000 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1892538MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92322890020
1892539
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Total Organic Carbon ug/L 25000 100 90-110100 0 1025000ND2500025000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1892540MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92322867001
1892541
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Total Organic Carbon ug/L M1250008690-11090 3 10250008.0 mg/L 29500 30500
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
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Page 44 of 79
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analysis conducted outside the EPA method holding time.H1
Sample was received or analysis requested beyond the recognized method holding time.H3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6
The lab does not hold NELAC/TNI accreditation for this parameter.N2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 79
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92321678001 339257 339658SW-1 EPA 3010A EPA 6010
92321678002 339341 339662SW-2 EPA 3010A EPA 6010
92321678003 339341 339662SW-3 EPA 3010A EPA 6010
92321678004 339341 339662SW-4 EPA 3010A EPA 6010
92321678005 339341 339662SWN-1 EPA 3010A EPA 6010
92321678006 339341 339662SWN-2 EPA 3010A EPA 6010
92321678001 339748SW-1 EPA 8260
92321678002 339748SW-2 EPA 8260
92321678003 339748SW-3 EPA 8260
92321678004 339748SW-4 EPA 8260
92321678005 339748SWN-1 EPA 8260
92321678006 339748SWN-2 EPA 8260
92321678007 339748SW-A EPA 8260
92321678008 339748SW-B EPA 8260
92321678009 339686MW-1 SM 2320B
92321678010 339686MW-7 SM 2320B
92321678011 339686MW-9 SM 2320B
92321678012 339686MW-11 SM 2320B
92321678013 339686MW-14 SM 2320B
92321678014 339686MW-21 SM 2320B
92321678009 340277MW-1 SM 3500-Fe B
92321678010 340277MW-7 SM 3500-Fe B
92321678011 340277MW-9 SM 3500-Fe B
92321678012 340277MW-11 SM 3500-Fe B
92321678013 340277MW-14 SM 3500-Fe B
92321678014 340277MW-21 SM 3500-Fe B
92321678009 339811MW-1 SM 4500-S2D
92321678010 339813MW-7 SM 4500-S2D
92321678011 339811MW-9 SM 4500-S2D
92321678012 339813MW-11 SM 4500-S2D
92321678013 339811MW-14 SM 4500-S2D
92321678014 339811MW-21 SM 4500-S2D
92321678009 340189MW-1 EPA 300.0
92321678010 340189MW-7 EPA 300.0
92321678011 340189MW-9 EPA 300.0
92321678012 340189MW-11 EPA 300.0
92321678013 340189MW-14 EPA 300.0
92321678014 340189MW-21 EPA 300.0
92321678009 341242MW-1 SM 4500-Cl-E
92321678010 341242MW-7 SM 4500-Cl-E
92321678011 341242MW-9 SM 4500-Cl-E
92321678012 341242MW-11 SM 4500-Cl-E
92321678013 341242MW-14 SM 4500-Cl-E
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
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Huntersville, NC 28078
[phone]
Page 46 of 79
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92321678014 341242MW-21 SM 4500-Cl-E
92321678009 339822MW-1 SM 5220D
92321678010 339822MW-7 SM 5220D
92321678011 339822MW-9 SM 5220D
92321678012 339822MW-11 SM 5220D
92321678013 339822MW-14 SM 5220D
92321678014 339822MW-21 SM 5220D
92321678009 341127MW-1 SM 5310B
92321678010 341127MW-7 SM 5310B
92321678011 341127MW-9 SM 5310B
92321678012 341127MW-11 SM 5310B
92321678013 341127MW-14 SM 5310B
92321678014 341127MW-21 SM 5310B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/22/2016 12:17 PM
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Huntersville, NC 28078
[phone]
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#=CL#
May 24, 2017
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92321678
92321678
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
SURRY CLOSED-MT. AIRY (MNA)
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on December 06, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Huntersville, NC 28078
[phone]
Page 1 of 51
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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Huntersville, NC 28078
[phone]
Page 2 of 51
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Lab ID Sample ID Matrix Date Collected Date Received
92321678009 MW-1 Water 12/03/16 11:10 12/06/16 08:31
92321678010 MW-7 Water 12/03/16 10:05 12/06/16 08:31
92321678011 MW-9 Water 12/02/16 16:00 12/06/16 08:31
92321678012 MW-11 Water 12/03/16 09:05 12/06/16 08:31
92321678013 MW-14 Water 12/02/16 14:00 12/06/16 08:31
92321678014 MW-21 Water 12/02/16 17:00 12/06/16 08:31
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 3 of 51
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92321678009 MW-1 SM 2320B 1 PASI-AKDF
SM 3500-Fe B 1 PASI-ACJH1
SM 4500-S2D 1 PASI-AEWS
EPA 300.0 1 PASI-AAES2
SM 4500-Cl-E 1 PASI-AWRC
SM 5220D 1 PASI-AMDW
SM 5310B 1 PASI-AAES2
92321678010 MW-7 SM 2320B 1 PASI-AKDF
SM 3500-Fe B 1 PASI-ACJH1
SM 4500-S2D 1 PASI-AEWS
EPA 300.0 1 PASI-AAES2
SM 4500-Cl-E 1 PASI-AWRC
SM 5220D 1 PASI-AMDW
SM 5310B 1 PASI-AAES2
92321678011 MW-9 SM 2320B 1 PASI-AKDF
SM 3500-Fe B 1 PASI-ACJH1
SM 4500-S2D 1 PASI-AEWS
EPA 300.0 1 PASI-AAES2
SM 4500-Cl-E 1 PASI-AWRC
SM 5220D 1 PASI-AMDW
SM 5310B 1 PASI-AAES2
92321678012 MW-11 SM 2320B 1 PASI-AKDF
SM 3500-Fe B 1 PASI-ACJH1
SM 4500-S2D 1 PASI-AEWS
EPA 300.0 1 PASI-AAES2
SM 4500-Cl-E 1 PASI-AWRC
SM 5220D 1 PASI-AMDW
SM 5310B 1 PASI-AAES2
92321678013 MW-14 SM 2320B 1 PASI-AKDF
SM 3500-Fe B 1 PASI-ACJH1
SM 4500-S2D 1 PASI-AEWS
EPA 300.0 1 PASI-AAES2
SM 4500-Cl-E 1 PASI-AWRC
SM 5220D 1 PASI-AMDW
SM 5310B 1 PASI-AAES2
92321678014 MW-21 SM 2320B 1 PASI-AKDF
SM 3500-Fe B 1 PASI-ACJH1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
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Page 4 of 51
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
SM 4500-S2D 1 PASI-AEWS
EPA 300.0 1 PASI-AAES2
SM 4500-Cl-E 1 PASI-AWRC
SM 5220D 1 PASI-AMDW
SM 5310B 1 PASI-AAES2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Sample:MW-1 Lab ID:92321678009 Collected:12/03/16 11:10 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 132000 ug/L 12/08/16 02:44500010001
Analytical Method: SM 3500-Fe BIron, Ferrous
Iron, Ferrous ND mg/L 12/13/16 03:39 H3,N20.50 0.50 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 12/08/16 09:45 18496-25-810001001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 8580J ug/L 12/09/16 18:08 14808-79-825000010001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 3930 ug/L 12/19/16 18:41 16887-00-610005001
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 27000 ug/L 12/08/16 00:2825000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon ND ug/L 12/17/16 03:43 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/24/2017 12:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Sample:MW-7 Lab ID:92321678010 Collected:12/03/16 10:05 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 53200 ug/L 12/08/16 02:55500010001
Analytical Method: SM 3500-Fe BIron, Ferrous
Iron, Ferrous ND mg/L 12/13/16 03:39 H3,N20.50 0.50 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 12/08/16 10:15 18496-25-810001001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 3740J ug/L 12/09/16 18:17 14808-79-825000010001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 25000 ug/L 12/19/16 18:44 16887-00-6400020004
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 27000 ug/L 12/08/16 00:2825000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 2680 ug/L 12/17/16 03:53 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/24/2017 12:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Sample:MW-9 Lab ID:92321678011 Collected:12/02/16 16:00 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 39300 ug/L 12/08/16 01:45500010001
Analytical Method: SM 3500-Fe BIron, Ferrous
Iron, Ferrous 4.7 mg/L 12/13/16 03:39 H3,N21.0 1.0 2
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 12/08/16 09:45 18496-25-810001001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 2090J ug/L 12/09/16 18:45 14808-79-825000010001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 29400 ug/L 12/19/16 18:45 16887-00-6400020004
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 27000 ug/L 12/08/16 00:2825000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 1540 ug/L 12/17/16 04:06 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/24/2017 12:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Sample:MW-11 Lab ID:92321678012 Collected:12/03/16 09:05 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 35300 ug/L 12/08/16 03:26500010001
Analytical Method: SM 3500-Fe BIron, Ferrous
Iron, Ferrous 2.6 mg/L 12/13/16 03:39 H3,N20.50 0.50 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide 699J ug/L 12/08/16 10:15 18496-25-810001001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 7510J ug/L 12/09/16 18:54 14808-79-825000010001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 9580 ug/L 12/19/16 18:46 16887-00-6400020004
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 14000J ug/L 12/08/16 00:2825000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 1920 ug/L 12/17/16 04:20 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/24/2017 12:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Sample:MW-14 Lab ID:92321678013 Collected:12/02/16 14:00 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 42400 ug/L 12/08/16 01:57500010001
Analytical Method: SM 3500-Fe BIron, Ferrous
Iron, Ferrous ND mg/L 12/13/16 03:39 H3,N20.50 0.50 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 12/08/16 09:45 18496-25-810001001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 2880J ug/L 12/09/16 19:03 14808-79-825000010001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 4180 ug/L 12/19/16 18:47 16887-00-610005001
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand ND ug/L 12/08/16 00:2825000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 2870 ug/L 12/17/16 04:35 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/24/2017 12:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Sample:MW-21 Lab ID:92321678014 Collected:12/02/16 17:00 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 41000 ug/L 12/08/16 02:33500010001
Analytical Method: SM 3500-Fe BIron, Ferrous
Iron, Ferrous ND mg/L 12/13/16 03:39 H3,N20.50 0.50 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 12/08/16 09:45 18496-25-810001001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 2570J ug/L 12/09/16 19:12 14808-79-825000010001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 29900 ug/L 12/19/16 18:47 16887-00-6 M110005001
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 19000J ug/L 12/08/16 00:2825000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 2430 ug/L 12/17/16 04:47 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/24/2017 12:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 51
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
339686
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92321678009, 92321678010, 92321678011, 92321678012, 92321678013, 92321678014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1883899
Associated Lab Samples:92321678009, 92321678010, 92321678011, 92321678012, 92321678013, 92321678014
Matrix:Water
AnalyzedMDL
Alkalinity, Total as CaCO3 ug/L ND 5000 12/07/16 22:511000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1883900LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 ug/L 4920050000 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1883901MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321915018
1883902
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L M1500004780-12040 16 2550000ND2360020000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1883903MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321678013
1883904
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L 50000 98 80-120100 1 2550000424009150092600
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/24/2017 12:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 51
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
340277
SM 3500-Fe B
SM 3500-Fe B
Iron, Ferrous
Associated Lab Samples:92321678009, 92321678010, 92321678011, 92321678012, 92321678013, 92321678014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1887534
Associated Lab Samples:92321678009, 92321678010, 92321678011, 92321678012, 92321678013, 92321678014
Matrix:Water
AnalyzedMDL
Iron, Ferrous mg/L ND 0.50 N212/13/16 03:390.50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1887535LABORATORY CONTROL SAMPLE:
LCSSpike
Iron, Ferrous mg/L 1.5 N21.5 102 90-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92321732001
1887536SAMPLE DUPLICATE:
Iron, Ferrous mg/L 2.5 H1,N21102.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/24/2017 12:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 51
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
339811
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92321678009, 92321678011, 92321678013, 92321678014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1884626
Associated Lab Samples:92321678009, 92321678011, 92321678013, 92321678014
Matrix:Water
AnalyzedMDL
Sulfide ug/L ND 1000 12/08/16 09:45100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1884627LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 512J500 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1884628MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321792004
1884629
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 105 80-120105 0 10500ND526J524J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1884630MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321792014
1884631
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 106 80-120106 0 10500ND582J582J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/24/2017 12:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 51
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
339813
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92321678010, 92321678012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1884638
Associated Lab Samples:92321678010, 92321678012
Matrix:Water
AnalyzedMDL
Sulfide ug/L ND 1000 12/08/16 10:15100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1884639LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 524J500 105 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1884640MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321678010
1884641
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 84 80-12084 1 10500ND441J438J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1884642MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321905009
1884643
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 105 80-120105 0 10500ND526J524J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/24/2017 12:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 51
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
340189
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92321678009, 92321678010, 92321678011, 92321678012, 92321678013, 92321678014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1886795
Associated Lab Samples:92321678009, 92321678010, 92321678011, 92321678012, 92321678013, 92321678014
Matrix:Water
AnalyzedMDL
Sulfate ug/L ND 250000 12/09/16 15:06500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1886796LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 18900J250000 8 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1886797MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321623024
1886798
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L M6250000890-1105 2 10250000398 mg/L 417000J 409000J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1886799MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321900004
1886800
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L 250000 8 90-1108 1 102500001000029800J30200J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/24/2017 12:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 51
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
341242
SM 4500-Cl-E
SM 4500-Cl-E
4500 Chloride
Associated Lab Samples:92321678009, 92321678010, 92321678011, 92321678012, 92321678013, 92321678014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1893040
Associated Lab Samples:92321678009, 92321678010, 92321678011, 92321678012, 92321678013, 92321678014
Matrix:Water
AnalyzedMDL
Chloride ug/L ND 1000 12/19/16 18:33500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1893041LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride ug/L 2040020000 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1893042MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92322679001
1893043
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L M6100006990-11071 0 101000076.9 mg/L 83800 84000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1893044MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321678014
1893045
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L M1100008890-11092 1 1010000299003880039100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/24/2017 12:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 51
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
339822
SM 5220D
SM 5220D
5220D COD
Associated Lab Samples:92321678009, 92321678010, 92321678011, 92321678012, 92321678013, 92321678014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1884712
Associated Lab Samples:92321678009, 92321678010, 92321678011, 92321678012, 92321678013, 92321678014
Matrix:Water
AnalyzedMDL
Chemical Oxygen Demand ug/L ND 25000 12/08/16 00:2812500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1884713LABORATORY CONTROL SAMPLE:
LCSSpike
Chemical Oxygen Demand ug/L 777000750000 104 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1884714MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92322011002
1884715
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L 750000 97 90-11097 0 3750000195 mg/L 925000 923000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1884716MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92322129001
1884717
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L 750000 101 90-110100 1 3750000141 mg/L 898000 893000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/24/2017 12:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 51
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
341127
SM 5310B
SM 5310B
5310B TOC
Associated Lab Samples:92321678009, 92321678010, 92321678011, 92321678012, 92321678013, 92321678014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1892535
Associated Lab Samples:92321678009, 92321678010, 92321678011, 92321678012, 92321678013, 92321678014
Matrix:Water
AnalyzedMDL
Total Organic Carbon ug/L ND 1000 12/17/16 00:59500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1892537LABORATORY CONTROL SAMPLE:
LCSSpike
Total Organic Carbon ug/L 2500025000 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1892538MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92322890020
1892539
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Total Organic Carbon ug/L 25000 100 90-110100 0 1025000ND2500025000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1892540MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92322867001
1892541
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Total Organic Carbon ug/L M1250008690-11090 3 10250008.0 mg/L 29500 30500
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/24/2017 12:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 51
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
ANALYTE QUALIFIERS
Analysis conducted outside the EPA method holding time.H1
Sample was received or analysis requested beyond the recognized method holding time.H3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6
The lab does not hold NELAC/TNI accreditation for this parameter.N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/24/2017 12:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92321678
SURRY CLOSED-MT. AIRY (MNA)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92321678009 339686MW-1 SM 2320B
92321678010 339686MW-7 SM 2320B
92321678011 339686MW-9 SM 2320B
92321678012 339686MW-11 SM 2320B
92321678013 339686MW-14 SM 2320B
92321678014 339686MW-21 SM 2320B
92321678009 340277MW-1 SM 3500-Fe B
92321678010 340277MW-7 SM 3500-Fe B
92321678011 340277MW-9 SM 3500-Fe B
92321678012 340277MW-11 SM 3500-Fe B
92321678013 340277MW-14 SM 3500-Fe B
92321678014 340277MW-21 SM 3500-Fe B
92321678009 339811MW-1 SM 4500-S2D
92321678010 339813MW-7 SM 4500-S2D
92321678011 339811MW-9 SM 4500-S2D
92321678012 339813MW-11 SM 4500-S2D
92321678013 339811MW-14 SM 4500-S2D
92321678014 339811MW-21 SM 4500-S2D
92321678009 340189MW-1 EPA 300.0
92321678010 340189MW-7 EPA 300.0
92321678011 340189MW-9 EPA 300.0
92321678012 340189MW-11 EPA 300.0
92321678013 340189MW-14 EPA 300.0
92321678014 340189MW-21 EPA 300.0
92321678009 341242MW-1 SM 4500-Cl-E
92321678010 341242MW-7 SM 4500-Cl-E
92321678011 341242MW-9 SM 4500-Cl-E
92321678012 341242MW-11 SM 4500-Cl-E
92321678013 341242MW-14 SM 4500-Cl-E
92321678014 341242MW-21 SM 4500-Cl-E
92321678009 339822MW-1 SM 5220D
92321678010 339822MW-7 SM 5220D
92321678011 339822MW-9 SM 5220D
92321678012 339822MW-11 SM 5220D
92321678013 339822MW-14 SM 5220D
92321678014 339822MW-21 SM 5220D
92321678009 341127MW-1 SM 5310B
92321678010 341127MW-7 SM 5310B
92321678011 341127MW-9 SM 5310B
92321678012 341127MW-11 SM 5310B
92321678013 341127MW-14 SM 5310B
92321678014 341127MW-21 SM 5310B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/24/2017 12:28 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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Pace Analytical Energy Services LLC
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
Report ID: 21214 - 925296 Page 1 of 24
Trey Carter
Pace Analytical Charlotte
9800 Kincey Ave
Suite 100
Huntersville, NC 28078
May 17, 2017
RE:
Pace Workorder:
SURRY CLOSED-MT.AIRY
Dear Trey Carter:
21214
Enclosed are the analytical results for sample(s) received by the laboratory on Thursday, December 08, 2016.
Results reported herein conform to the most current NELAC standards, where applicable, unless otherwise
narrated in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Enclosures
Ruth Welsh 05/17/2017
[e-mail]
Total Number of Pages ____
As a valued client we would appreciate your comments on our service.
Please email [e-mail].
Customer Service Representative
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LABORATORY ACCREDITATIONS & CERTIFICATIONS
Pennsylvania Department of Environmental Protection, Bureau of Laboratories
02-00538
NELAP Non-Potable Water and Solid & Hazardous Waste
Accreditor:
Accreditation ID:
Scope:
West Virginia Department of Environmental Protection, Division of Water and Waste
Management
395
Non-Potable Water
Accreditor:
Accreditation ID:
Scope:
South Carolina Department of Health and Environmental Control, Office of Environmental
Laboratory Certification
89009003
Clean Water Act (CWA); Resource Conservation and Recovery Act (RCRA)
Accreditor:
Accreditation ID:
Scope:
NELAP: New Jersey, Department of Environmental Protection
PA026
Non-Potable Water; Solid and Chemical Materials
Accreditor:
Accreditation ID:
Scope:
NELAP: New York, Department of Health Wadsworth Center
11815
Non-Potable Water; Solid and Hazardous Waste
Accreditor:
Accreditation ID:
Scope:
State of Connecticut, Department of Public Health, Division of Environmental Health
PH-0263
Clean Water Act (CWA) Resource Conservation and Recovery Act (RCRA)
Accreditor:
Accreditation ID:
Scope:
NELAP: Texas, Commission on Environmental Quality
T104704453-09-TX
Non-Potable Water
Accreditor:
Accreditation ID:
Scope:
State of New Hampshire
299409
Non-potable water
Accreditor:
Accreditation ID:
Scope:
State of Georgia
Chapter 391-3-26
As per the Georgia EPD Rules and Regulations for Commercial Laboratories, PAES is
accredited by the Pennsylvania Department of Environmental Protection Bureau of
Laboratories under the National Environmental Laboratory Approval Program (NELAC).
Accreditor:
Accreditation ID:
Scope:
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SAMPLE SUMMARY
Workorder:21214 SURRY CLOSED-MT.AIRY
Lab ID Sample ID Matrix Date Collected Date Received
212140001 MW-1 Water 12/3/2016 11:10 12/8/2016 12:15
212140002 MW-1 Bubble Strip 12/3/2016 11:10 12/8/2016 12:15
212140003 MW-7 Water 12/3/2016 10:05 12/8/2016 12:15
212140004 MW-7 Bubble Strip 12/3/2016 10:05 12/8/2016 12:15
212140005 MW-9 Water 12/2/2016 16:00 12/8/2016 12:15
212140006 MW-9 Bubble Strip 12/2/2016 16:00 12/8/2016 12:15
212140007 MW-11 Water 12/3/2016 09:05 12/8/2016 12:15
212140008 MW-11 Bubble Strip 12/3/2016 09:05 12/8/2016 12:15
212140009 MW-14 Water 12/2/2016 14:00 12/8/2016 12:15
212140010 MW-14 Bubble Strip 12/2/2016 14:00 12/8/2016 12:15
212140011 MW-21 Water 12/2/2016 17:00 12/8/2016 12:15
212140012 MW-21 Bubble Strip 12/2/2016 17:00 12/8/2016 12:15
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PROJECT SUMMARY
Workorder:21214 SURRY CLOSED-MT.AIRY
Workorder Comments
The container pH for samples 21214 (0003, 0011) were measured as below the expected pH (< 10) for those samples preserved
with trisodium phosphate, as assigned to PAES method AM20GAx.
This report was reissued on 5-17-2017 to change the format to report results with data qualifiers.
Batch Comments
Batch:EDON/3187 - Low Level Volatile Fatty Acids
The matrix spike and/or spike duplicate, recovery or relative percent difference; accuracy influenced by the concentration of the
reference sample 212050001. Analyte Lactic, Acetic, Propionic, Butyric and Pentanoic acids. Batch acceptance based on
laboratory control sample recovery.
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ANALYTICAL RESULTS
Workorder:21214 SURRY CLOSED-MT.AIRY
12/8/2016 12:15
MW-1
Matrix:Water
RegLmtParameters
Lab ID:
Sample ID:
RegLmt
212140001
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
12/3/2016 11:10
EDonors - PAES
Analysis Desc: AM23G Analytical Method: AM23G
Lactic Acid 0.042J mg/l 0.20 1 12/9/2016 11:31 MD M3,B,M50.0060
Acetic Acid 0.082J mg/l 0.10 1 12/9/2016 11:31 MD M3,B,M50.0070
Propionic Acid 0.11 mg/l 0.10 1 12/9/2016 11:31 MD M3,M50.0090
Formic Acid 0.068J mg/l 0.10 1 12/9/2016 11:31 MD B0.0050
Butyric Acid 0.041J mg/l 0.10 1 12/9/2016 11:31 MD M3,M50.0070
Pyruvic Acid 0.016J mg/l 0.10 1 12/9/2016 11:31 MD0.0070
i-Pentanoic Acid 0.029J mg/l 0.10 1 12/9/2016 11:31 MD0.0070
Pentanoic Acid 0.018J mg/l 0.10 1 12/9/2016 11:31 MD M3,M50.0060
i-Hexanoic Acid 0.0040U mg/l 0.20 1 12/9/2016 11:31 MD0.0040
Hexanoic Acid 0.0070U mg/l 0.20 1 12/9/2016 11:31 MD0.0070
RISK - PAES
Analysis Desc: AM20GAX Analytical Method: AM20GAX
Methane 450 ug/l 0.50 1 12/12/2016 13:31 BW n0.027
Ethane 0.0096J ug/l 0.10 1 12/12/2016 13:31 BW n0.0030
Ethene 0.036J ug/l 0.10 1 12/12/2016 13:31 BW n0.0010
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Report ID: 21214 - 925296 Page 6 of 24
ANALYTICAL RESULTS
Workorder:21214 SURRY CLOSED-MT.AIRY
12/8/2016 12:15
MW-1
Matrix:Bubble Strip
RegLmtParameters
Lab ID:
Sample ID:
RegLmt
212140002
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
12/3/2016 11:10
RISK - PAES
Analysis Desc: AM20GAX Analytical Method: AM20GAX
Hydrogen 1.5 nM 0.60 1 12/12/2016 14:15 MM n0.075
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ANALYTICAL RESULTS
Workorder:21214 SURRY CLOSED-MT.AIRY
12/8/2016 12:15
MW-7
Matrix:Water
RegLmtParameters
Lab ID:
Sample ID:
RegLmt
212140003
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
12/3/2016 10:05
EDonors - PAES
Analysis Desc: AM23G Analytical Method: AM23G
Lactic Acid 0.26 mg/l 0.20 1 12/9/2016 12:25 MD M3,B,M50.0060
Acetic Acid 0.026J mg/l 0.10 1 12/9/2016 12:25 MD M3,B,M50.0070
Propionic Acid 0.0090U mg/l 0.10 1 12/9/2016 12:25 MD M3,M50.0090
Formic Acid 0.057J mg/l 0.10 1 12/9/2016 12:25 MD B0.0050
Butyric Acid 0.0070U mg/l 0.10 1 12/9/2016 12:25 MD M3,M50.0070
Pyruvic Acid 0.013J mg/l 0.10 1 12/9/2016 12:25 MD0.0070
i-Pentanoic Acid 0.0070U mg/l 0.10 1 12/9/2016 12:25 MD0.0070
Pentanoic Acid 0.0060U mg/l 0.10 1 12/9/2016 12:25 MD M3,M50.0060
i-Hexanoic Acid 0.0040U mg/l 0.20 1 12/9/2016 12:25 MD0.0040
Hexanoic Acid 0.0070U mg/l 0.20 1 12/9/2016 12:25 MD0.0070
RISK - PAES
Analysis Desc: AM20GAX Analytical Method: AM20GAX
Methane 45 ug/l 0.50 1 12/12/2016 13:40 BW n0.027
Ethane 0.13 ug/l 0.10 1 12/12/2016 13:40 BW n0.0030
Ethene 0.016J ug/l 0.10 1 12/12/2016 13:40 BW n0.0010
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Report ID: 21214 - 925296 Page 8 of 24
ANALYTICAL RESULTS
Workorder:21214 SURRY CLOSED-MT.AIRY
12/8/2016 12:15
MW-7
Matrix:Bubble Strip
RegLmtParameters
Lab ID:
Sample ID:
RegLmt
212140004
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
12/3/2016 10:05
RISK - PAES
Analysis Desc: AM20GAX Analytical Method: AM20GAX
Hydrogen 1.4 nM 0.60 1 12/12/2016 14:45 MM n0.075
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ANALYTICAL RESULTS
Workorder:21214 SURRY CLOSED-MT.AIRY
12/8/2016 12:15
MW-9
Matrix:Water
RegLmtParameters
Lab ID:
Sample ID:
RegLmt
212140005
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
12/2/2016 16:00
EDonors - PAES
Analysis Desc: AM23G Analytical Method: AM23G
Lactic Acid 0.095J mg/l 0.20 1 12/9/2016 13:18 MD M3,B,M50.0060
Acetic Acid 0.021J mg/l 0.10 1 12/9/2016 13:18 MD M3,B,M50.0070
Propionic Acid 0.0090U mg/l 0.10 1 12/9/2016 13:18 MD M3,M50.0090
Formic Acid 0.045J mg/l 0.10 1 12/9/2016 13:18 MD B0.0050
Butyric Acid 0.0070U mg/l 0.10 1 12/9/2016 13:18 MD M3,M50.0070
Pyruvic Acid 0.0070U mg/l 0.10 1 12/9/2016 13:18 MD0.0070
i-Pentanoic Acid 0.0070U mg/l 0.10 1 12/9/2016 13:18 MD0.0070
Pentanoic Acid 0.0060U mg/l 0.10 1 12/9/2016 13:18 MD M3,M50.0060
i-Hexanoic Acid 0.0040U mg/l 0.20 1 12/9/2016 13:18 MD0.0040
Hexanoic Acid 0.0070U mg/l 0.20 1 12/9/2016 13:18 MD0.0070
RISK - PAES
Analysis Desc: AM20GAX Analytical Method: AM20GAX
Methane 660 ug/l 0.50 1 12/12/2016 13:50 BW n0.027
Ethane 30 ug/l 0.10 1 12/12/2016 13:50 BW n0.0030
Ethene 0.93 ug/l 0.10 1 12/12/2016 13:50 BW n0.0010
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ANALYTICAL RESULTS
Workorder:21214 SURRY CLOSED-MT.AIRY
12/8/2016 12:15
MW-9
Matrix:Bubble Strip
RegLmtParameters
Lab ID:
Sample ID:
RegLmt
212140006
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
12/2/2016 16:00
RISK - PAES
Analysis Desc: AM20GAX Analytical Method: AM20GAX
Hydrogen 1.6 nM 0.60 1 12/12/2016 14:57 MM n0.075
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ANALYTICAL RESULTS
Workorder:21214 SURRY CLOSED-MT.AIRY
12/8/2016 12:15
MW-11
Matrix:Water
RegLmtParameters
Lab ID:
Sample ID:
RegLmt
212140007
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
12/3/2016 09:05
EDonors - PAES
Analysis Desc: AM23G Analytical Method: AM23G
Lactic Acid 0.018J mg/l 0.20 1 12/9/2016 14:11 MD M3,B,M50.0060
Acetic Acid 0.030J mg/l 0.10 1 12/9/2016 14:11 MD M3,B,M50.0070
Propionic Acid 0.0090U mg/l 0.10 1 12/9/2016 14:11 MD M3,M50.0090
Formic Acid 0.038J mg/l 0.10 1 12/9/2016 14:11 MD B0.0050
Butyric Acid 0.0070U mg/l 0.10 1 12/9/2016 14:11 MD M3,M50.0070
Pyruvic Acid 0.0070U mg/l 0.10 1 12/9/2016 14:11 MD0.0070
i-Pentanoic Acid 0.0070U mg/l 0.10 1 12/9/2016 14:11 MD0.0070
Pentanoic Acid 0.0060U mg/l 0.10 1 12/9/2016 14:11 MD M3,M50.0060
i-Hexanoic Acid 0.0040U mg/l 0.20 1 12/9/2016 14:11 MD0.0040
Hexanoic Acid 0.0070U mg/l 0.20 1 12/9/2016 14:11 MD0.0070
RISK - PAES
Analysis Desc: AM20GAX Analytical Method: AM20GAX
Methane 1100 ug/l 0.50 1 12/13/2016 08:06 BW n0.027
Ethane 0.083J ug/l 0.10 1 12/13/2016 08:06 BW n0.0030
Ethene 0.30 ug/l 0.10 1 12/13/2016 08:06 BW n0.0010
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ANALYTICAL RESULTS
Workorder:21214 SURRY CLOSED-MT.AIRY
12/8/2016 12:15
MW-11
Matrix:Bubble Strip
RegLmtParameters
Lab ID:
Sample ID:
RegLmt
212140008
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
12/3/2016 09:05
RISK - PAES
Analysis Desc: AM20GAX Analytical Method: AM20GAX
Hydrogen 1.6 nM 0.60 1 12/12/2016 15:10 MM n0.075
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ANALYTICAL RESULTS
Workorder:21214 SURRY CLOSED-MT.AIRY
12/8/2016 12:15
MW-14
Matrix:Water
RegLmtParameters
Lab ID:
Sample ID:
RegLmt
212140009
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
12/2/2016 14:00
EDonors - PAES
Analysis Desc: AM23G Analytical Method: AM23G
Lactic Acid 0.028J mg/l 0.20 1 12/9/2016 15:05 MD M3,B,M50.0060
Acetic Acid 0.031J mg/l 0.10 1 12/9/2016 15:05 MD M3,B,M50.0070
Propionic Acid 0.0090U mg/l 0.10 1 12/9/2016 15:05 MD M3,M50.0090
Formic Acid 0.033J mg/l 0.10 1 12/9/2016 15:05 MD B0.0050
Butyric Acid 0.0070U mg/l 0.10 1 12/9/2016 15:05 MD M3,M50.0070
Pyruvic Acid 0.0070U mg/l 0.10 1 12/9/2016 15:05 MD0.0070
i-Pentanoic Acid 0.0070U mg/l 0.10 1 12/9/2016 15:05 MD0.0070
Pentanoic Acid 0.0060U mg/l 0.10 1 12/9/2016 15:05 MD M3,M50.0060
i-Hexanoic Acid 0.0040U mg/l 0.20 1 12/9/2016 15:05 MD0.0040
Hexanoic Acid 0.0070U mg/l 0.20 1 12/9/2016 15:05 MD0.0070
RISK - PAES
Analysis Desc: AM20GAX Analytical Method: AM20GAX
Methane 280 ug/l 0.50 1 12/13/2016 08:29 BW n0.027
Ethane 0.0053J ug/l 0.10 1 12/13/2016 08:29 BW n0.0030
Ethene 0.013J ug/l 0.10 1 12/13/2016 08:29 BW n0.0010
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ANALYTICAL RESULTS
Workorder:21214 SURRY CLOSED-MT.AIRY
12/8/2016 12:15
MW-14
Matrix:Bubble Strip
RegLmtParameters
Lab ID:
Sample ID:
RegLmt
212140010
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
12/2/2016 14:00
RISK - PAES
Analysis Desc: AM20GAX Analytical Method: AM20GAX
Hydrogen 1.5 nM 0.60 1 12/12/2016 15:26 MM n0.075
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ANALYTICAL RESULTS
Workorder:21214 SURRY CLOSED-MT.AIRY
12/8/2016 12:15
MW-21
Matrix:Water
RegLmtParameters
Lab ID:
Sample ID:
RegLmt
212140011
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
12/2/2016 17:00
EDonors - PAES
Analysis Desc: AM23G Analytical Method: AM23G
Lactic Acid 0.12J mg/l 0.20 1 12/9/2016 15:58 MD M3,B,M50.0060
Acetic Acid 0.032J mg/l 0.10 1 12/9/2016 15:58 MD M3,B,M50.0070
Propionic Acid 0.0090U mg/l 0.10 1 12/9/2016 15:58 MD M3,M50.0090
Formic Acid 0.085J mg/l 0.10 1 12/9/2016 15:58 MD B0.0050
Butyric Acid 0.0070U mg/l 0.10 1 12/9/2016 15:58 MD M3,M50.0070
Pyruvic Acid 0.0070U mg/l 0.10 1 12/9/2016 15:58 MD0.0070
i-Pentanoic Acid 0.0070U mg/l 0.10 1 12/9/2016 15:58 MD0.0070
Pentanoic Acid 0.0060U mg/l 0.10 1 12/9/2016 15:58 MD M3,M50.0060
i-Hexanoic Acid 0.0040U mg/l 0.20 1 12/9/2016 15:58 MD0.0040
Hexanoic Acid 0.0070U mg/l 0.20 1 12/9/2016 15:58 MD0.0070
RISK - PAES
Analysis Desc: AM20GAX Analytical Method: AM20GAX
Methane 4.9 ug/l 0.50 1 12/13/2016 08:43 BW n0.027
Ethane 0.0042J ug/l 0.10 1 12/13/2016 08:43 BW n0.0030
Ethene 0.0059J ug/l 0.10 1 12/13/2016 08:43 BW n0.0010
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Report ID: 21214 - 925296 Page 16 of 24
ANALYTICAL RESULTS
Workorder:21214 SURRY CLOSED-MT.AIRY
12/8/2016 12:15
MW-21
Matrix:Bubble Strip
RegLmtParameters
Lab ID:
Sample ID:
RegLmt
212140012
Results Units PQL DF ByAnalyzedMDL Qualifiers
Date Collected:
Date Received:
12/2/2016 17:00
RISK - PAES
Analysis Desc: AM20GAX Analytical Method: AM20GAX
Hydrogen 1.6 nM 0.60 1 12/12/2016 15:39 MM n0.075
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ANALYTICAL RESULTS QUALIFIERS
Workorder:21214 SURRY CLOSED-MT.AIRY
DEFINITIONS/QUALIFIERS
U
J
Indicates the compound was analyzed for, but not detected at or above the noted concentration.
Estimated concentration greater than the set method detection limit (MDL) and less than the set reporting limit (PQL).
MDL Method Detection Limit. Can be used synonymously with LOD; Limit Of Detection.
PQL Practical Quanitation Limit. Can be used synonymously with LOQ; Limit Of Quantitation.
ND Not detected at or above reporting limit.
DF Dilution Factor.
S Surrogate.
RPD Relative Percent Difference.
% Rec Percent Recovery.
The laboratory does not hold NELAP/TNI accreditation for this method or analyte.n
The analyte was detected in the associated blank.B
The matrix spike duplicate sample recovery was outside laboratory control limits.M5
The matrix spike sample recovery was outside laboratory control limits.M3
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This report shall not be reproduced, except in full,
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QUALITY CONTROL DATA
Workorder:21214 SURRY CLOSED-MT.AIRY
QC Batch:
QC Batch Method:
EDON/3187
AM23G
Analysis Method:AM23G
Associated Lab Samples:212140001, 212140003, 212140005, 212140007, 212140009, 212140011
METHOD BLANK:45959
Parameter Units Result
Blank
Limit
Reporting
Qualifiers
EDonors
Lactic Acid 0.080Jmg/l 0.0060 M3,B,M5
Acetic Acid 0.017Jmg/l 0.0070 M3,B,M5
Propionic Acid 0.0090Umg/l 0.0090 M3,M5
Formic Acid 0.029Jmg/l 0.0050 B
Butyric Acid 0.0070Umg/l 0.0070 M3,M5
Pyruvic Acid 0.0070Umg/l 0.0070
i-Pentanoic Acid 0.0070Umg/l 0.0070
Pentanoic Acid 0.0060Umg/l 0.0060 M3,M5
i-Hexanoic Acid 0.0040Umg/l 0.0040
Hexanoic Acid 0.0070Umg/l 0.0070
LABORATORY CONTROL SAMPLE:
Parameter Units Conc.
Spike
Result
LCS
Qualifiers
LCS
% Rec
% Rec
Limits
45960
EDonors
Lactic Acid 2mg/l 1.9 M3,B,M59570-130
Acetic Acid 2mg/l 1.9 M3,B,M59670-130
Propionic Acid 2mg/l 2.0 M3,M59970-130
Formic Acid 2mg/l 1.8 B9170-130
Butyric Acid 2mg/l 2.0 M3,M59970-130
Pyruvic Acid 2mg/l 1.9 97 70-130
i-Pentanoic Acid 2mg/l 2.0 100 70-130
Pentanoic Acid 2mg/l 1.9 M3,M59770-130
i-Hexanoic Acid 2mg/l 1.9 97 70-130
Hexanoic Acid 2mg/l 2.0 98 70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
Parameter Units Conc.
Spike
Result
MS
45961 45962
MSD
Result % Rec
MS MSD
% Rec
% Rec
Limit RPD RPD
Max
QualifiersResult
Original
212050001Original:
EDonors
Lactic Acid mg/l 2 0.91 19 70-130 M3,B,M50.89 18 5.4 300.53
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QUALITY CONTROL DATA
Workorder:21214 SURRY CLOSED-MT.AIRY
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
Parameter Units Conc.
Spike
Result
MS
45961 45962
MSD
Result % Rec
MS MSD
% Rec
% Rec
Limit RPD RPD
Max
QualifiersResult
Original
212050001Original:
Acetic Acid mg/l 2 0.0070U -3630 70-130 M3,B,M50.0070U -3630 0 3073
Propionic Acid mg/l 2 0.0090U -1680 70-130 M3,M50.0090U -1680 0 3034
Formic Acid mg/l 2 3.9 86 70-130 B3.9 87 1.2 302.2
Butyric Acid mg/l 2 0.0070U -2940 70-130 M3,M50.0070U -2940 0 3059
Pyruvic Acid mg/l 2 3.5 93 70-1303.5 93 0 301.6
i-Pentanoic Acid mg/l 2 2.5 100 70-1302.5 101 1 300.51
Pentanoic Acid mg/l 2 8.5 170 70-130 M3,M58.2 157 8 305.1
i-Hexanoic Acid mg/l 2 2.0 96 70-1301.9 90 6.5 300.1
Hexanoic Acid mg/l 2 8.6 111 70-1308.2 93 18 306.4
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Report ID: 21214 - 925296 Page 20 of 24
QUALITY CONTROL DATA
Workorder:21214 SURRY CLOSED-MT.AIRY
QC Batch:
QC Batch Method:
DISG/5803
AM20GAX
Analysis Method:AM20GAX
Associated Lab Samples:212140001, 212140003, 212140005
METHOD BLANK:45983
Parameter Units Result
Blank
Limit
Reporting
Qualifiers
RISK
Methane 0.027Uug/l 0.027 n
Ethane 0.0030Uug/l 0.0030 n
Ethene 0.0010Uug/l 0.0010 n
LABORATORY CONTROL SAMPLE & LCSD:
Parameter Units Conc.
Spike
Result
LCS
45985 45987
LCSD
Result % Rec
LCS LCSD
% Rec
% Rec
Limit RPD RPD
Max
Qualifiers
RISK
Methane ug/l 750 760 102 80-120 n750100220
Ethane ug/l 38 37 98 80-120 n3797120
Ethene ug/l 35 34 97 80-120 n3496120
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Report ID: 21214 - 925296 Page 21 of 24
QUALITY CONTROL DATA
Workorder:21214 SURRY CLOSED-MT.AIRY
QC Batch:
QC Batch Method:
DISG/5804
AM20GAX
Analysis Method:AM20GAX
Associated Lab Samples:212140007, 212140009, 212140011
METHOD BLANK:45989
Parameter Units Result
Blank
Limit
Reporting
Qualifiers
RISK
Methane 0.027Uug/l 0.027 n
Ethane 0.0030Uug/l 0.0030 n
Ethene 0.0010Uug/l 0.0010 n
LABORATORY CONTROL SAMPLE & LCSD:
Parameter Units Conc.
Spike
Result
LCS
45990 45991
LCSD
Result % Rec
LCS LCSD
% Rec
% Rec
Limit RPD RPD
Max
Qualifiers
RISK
Methane ug/l 750 760 102 80-120 n7801041.9 20
Ethane ug/l 38 37 99 80-120 n3798120
Ethene ug/l 35 34 97 80-120 n3497020
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This report shall not be reproduced, except in full,
Report ID: 21214 - 925296 Page 22 of 24
QUALITY CONTROL DATA
Workorder:21214 SURRY CLOSED-MT.AIRY
QC Batch:
QC Batch Method:
DISG/5806
AM20GAX
Analysis Method:AM20GAX
Associated Lab Samples:212140002, 212140004, 212140006, 212140008, 212140010, 212140012
METHOD BLANK:46004
Parameter Units Result
Blank
Limit
Reporting
Qualifiers
RISK
Hydrogen 0.075UnM 0.075 n
LABORATORY CONTROL SAMPLE & LCSD:
Parameter Units Conc.
Spike
Result
LCS
46005 46006
LCSD
Result % Rec
LCS LCSD
% Rec
% Rec
Limit RPD RPD
Max
Qualifiers
RISK
Hydrogen nM 24 27 111 80-120 n271100.9 20
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QUALITY CONTROL DATA QUALIFIERS
Workorder:21214 SURRY CLOSED-MT.AIRY
QUALITY CONTROL PARAMETER QUALIFIERS
The analyte was detected in the associated blank.B
The matrix spike sample recovery was outside laboratory control limits.M3
The matrix spike duplicate sample recovery was outside laboratory control limits.M5
The analyte concentration was determined from a dilution.d
The laboratory does not hold NELAP/TNI accreditation for this method or analyte.n
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Workorder:21214 SURRY CLOSED-MT.AIRY
Lab ID Sample ID Prep Method Analysis MethodPrep Batch Batch
Analysis
212140001 MW-1 EDON/3187AM23G
212140003 MW-7 EDON/3187AM23G
212140005 MW-9 EDON/3187AM23G
212140007 MW-11 EDON/3187AM23G
212140009 MW-14 EDON/3187AM23G
212140011 MW-21 EDON/3187AM23G
212140001 MW-1 DISG/5803AM20GAX
212140003 MW-7 DISG/5803AM20GAX
212140005 MW-9 DISG/5803AM20GAX
212140007 MW-11 DISG/5804AM20GAX
212140009 MW-14 DISG/5804AM20GAX
212140011 MW-21 DISG/5804AM20GAX
212140002 MW-1 DISG/5806AM20GAX
212140004 MW-7 DISG/5806AM20GAX
212140006 MW-9 DISG/5806AM20GAX
212140008 MW-11 DISG/5806AM20GAX
212140010 MW-14 DISG/5806AM20GAX
212140012 MW-21 DISG/5806AM20GAX
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#=CL#
December 16, 2016
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92321732
92321732
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
Surry Closed-Mt. Airy (MNA)
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on December 02, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 1 of 35
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92321732
Surry Closed-Mt. Airy (MNA)
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92321732
Surry Closed-Mt. Airy (MNA)
Lab ID Sample ID Matrix Date Collected Date Received
92321732001 MW-15 Water 12/01/16 14:00 12/02/16 07:09
REPORT OF LABORATORY ANALYSIS
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#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92321732
Surry Closed-Mt. Airy (MNA)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92321732001 MW-15 SM 2320B 1 PASI-AKDF
SM 3500-Fe B 1 PASI-ACJH1
SM 4500-S2D 1 PASI-AEWS
EPA 300.0 1 PASI-AAES2
SM 4500-Cl-E 1 PASI-AWRC
SM 5220D 1 PASI-AMDW
SM 5310B 1 PASI-AAES2
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321732
Surry Closed-Mt. Airy (MNA)
Sample:MW-15 Lab ID:92321732001 Collected:12/01/16 14:00 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 47700 ug/L 12/06/16 04:07500010001
Analytical Method: SM 3500-Fe BIron, Ferrous
Iron, Ferrous 2.5 mg/L 12/13/16 03:39 H1,N20.50 0.50 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide 121J ug/L 12/05/16 15:00 18496-25-810001001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 1790J ug/L 12/08/16 03:36 14808-79-825000010001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 1930 ug/L 12/07/16 18:53 16887-00-610005001
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand ND ug/L 12/06/16 00:2225000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 591J ug/L 12/14/16 20:14 7440-44-010005001
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321732
Surry Closed-Mt. Airy (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
339291
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92321732001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1881486
Associated Lab Samples:92321732001
Matrix:Water
AnalyzedMDL
Alkalinity, Total as CaCO3 ug/L ND 5000 12/05/16 21:561000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1881487LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 ug/L 4750050000 95 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1881488MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321642041
1881489
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L 50000 99 80-12098 0 2550000ND4930049200
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1881490MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321730005
1881491
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L 50000 106 80-12088 2 2550000410 mg/L 463000 454000
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321732
Surry Closed-Mt. Airy (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
340277
SM 3500-Fe B
SM 3500-Fe B
Iron, Ferrous
Associated Lab Samples:92321732001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1887534
Associated Lab Samples:92321732001
Matrix:Water
AnalyzedMDL
Iron, Ferrous mg/L ND 0.50 N212/13/16 03:390.50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1887535LABORATORY CONTROL SAMPLE:
LCSSpike
Iron, Ferrous mg/L 1.5 N21.5 102 90-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92321732001
1887536SAMPLE DUPLICATE:
Iron, Ferrous mg/L 2.5 H1,N21102.5
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321732
Surry Closed-Mt. Airy (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
339319
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92321732001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1881556
Associated Lab Samples:92321732001
Matrix:Water
AnalyzedMDL
Sulfide ug/L ND 1000 12/05/16 15:00100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1881557LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 484J500 97 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1881558MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321642041
1881559
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 100 80-120100 0 10500ND500J499J
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321732
Surry Closed-Mt. Airy (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
339763
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92321732001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1884283
Associated Lab Samples:92321732001
Matrix:Water
AnalyzedMDL
Sulfate ug/L ND 250000 12/08/16 00:071000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1884284LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 19800J20000 99 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1884285MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321623044
1884286
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L 20000 93 90-11093 1 10200003.9 mg/L 22600J 22400J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1884287MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321663001
1884288
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L 20000 94 90-11095 0 102000025.1 mg/L 43900J 44000J
REPORT OF LABORATORY ANALYSIS
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Page 9 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321732
Surry Closed-Mt. Airy (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
339806
SM 4500-Cl-E
SM 4500-Cl-E
4500 Chloride
Associated Lab Samples:92321732001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1884587
Associated Lab Samples:92321732001
Matrix:Water
AnalyzedMDL
Chloride ug/L ND 1000 12/07/16 18:19500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1884588LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride ug/L 2120020000 106 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1884589MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92320983006
1884590
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L M11000021190-110213 1 101000096303080030900
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1884591MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92320983015
1884592
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L 10000 107 90-110106 1 1010000145002520025000
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321732
Surry Closed-Mt. Airy (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
339404
SM 5220D
SM 5220D
5220D COD
Associated Lab Samples:92321732001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1882284
Associated Lab Samples:92321732001
Matrix:Water
AnalyzedMDL
Chemical Oxygen Demand ug/L ND 25000 12/06/16 00:2212500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1882285LABORATORY CONTROL SAMPLE:
LCSSpike
Chemical Oxygen Demand ug/L 757000750000 101 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1882286MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321525002
1882287
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L M6750000-53 90-110-27 2 375000011000
mg/L
1060000
0
1080000
0
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1882288MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321681001
1882289
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L 750000 102 90-110102 0 375000032.0 mg/L 797000 797000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321732
Surry Closed-Mt. Airy (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
340598
SM 5310B
SM 5310B
5310B TOC
Associated Lab Samples:92321732001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1888910
Associated Lab Samples:92321732001
Matrix:Water
AnalyzedMDL
Total Organic Carbon ug/L ND 1000 12/14/16 15:26500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1888911LABORATORY CONTROL SAMPLE:
LCSSpike
Total Organic Carbon ug/L 2520025000 101 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1888912MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92322500014
1888913
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Total Organic Carbon ug/L 25000 101 90-110102 1 1025000ND2530025600
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1888914MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92322946001
1888915
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Total Organic Carbon ug/L 25000 102 90-110102 0 10250005.1 mg/L 30700 30600
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 35
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92321732
Surry Closed-Mt. Airy (MNA)
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
ANALYTE QUALIFIERS
Analysis conducted outside the EPA method holding time.H1
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6
The lab does not hold NELAC/TNI accreditation for this parameter.N2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 03:48 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 35
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92321732
Surry Closed-Mt. Airy (MNA)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92321732001 339291MW-15 SM 2320B
92321732001 340277MW-15 SM 3500-Fe B
92321732001 339319MW-15 SM 4500-S2D
92321732001 339763MW-15 EPA 300.0
92321732001 339806MW-15 SM 4500-Cl-E
92321732001 339404MW-15 SM 5220D
92321732001 340598MW-15 SM 5310B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/16/2016 03:48 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 35
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Page 35 of 35
#=CL#
December 19, 2016
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92321732
92321732
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
Surry Closed-Mt. Airy (MNA)
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on December 02, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
Report revised on 12.19.16 to update revised subcontracting report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 35
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92321732
Surry Closed-Mt. Airy (MNA)
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 35
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92321732
Surry Closed-Mt. Airy (MNA)
Lab ID Sample ID Matrix Date Collected Date Received
92321732001 MW-15 Water 12/01/16 14:00 12/02/16 07:09
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 35
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92321732
Surry Closed-Mt. Airy (MNA)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92321732001 MW-15 SM 2320B 1 PASI-AKDF
SM 3500-Fe B 1 PASI-ACJH1
SM 4500-S2D 1 PASI-AEWS
EPA 300.0 1 PASI-AAES2
SM 4500-Cl-E 1 PASI-AWRC
SM 5220D 1 PASI-AMDW
SM 5310B 1 PASI-AAES2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92321732
Surry Closed-Mt. Airy (MNA)
Sample:MW-15 Lab ID:92321732001 Collected:12/01/16 14:00 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 47700 ug/L 12/06/16 04:07500010001
Analytical Method: SM 3500-Fe BIron, Ferrous
Iron, Ferrous 2.5 mg/L 12/13/16 03:39 H1,N20.50 0.50 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide 121J ug/L 12/05/16 15:00 18496-25-810001001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 1790J ug/L 12/08/16 03:36 14808-79-825000010001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 1930 ug/L 12/07/16 18:53 16887-00-610005001
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand ND ug/L 12/06/16 00:2225000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 591J ug/L 12/14/16 20:14 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 10:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321732
Surry Closed-Mt. Airy (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
339291
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92321732001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1881486
Associated Lab Samples:92321732001
Matrix:Water
AnalyzedMDL
Alkalinity, Total as CaCO3 ug/L ND 5000 12/05/16 21:561000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1881487LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 ug/L 4750050000 95 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1881488MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321642041
1881489
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L 50000 99 80-12098 0 2550000ND4930049200
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1881490MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321730005
1881491
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L 50000 106 80-12088 2 2550000410 mg/L 463000 454000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 10:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321732
Surry Closed-Mt. Airy (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
340277
SM 3500-Fe B
SM 3500-Fe B
Iron, Ferrous
Associated Lab Samples:92321732001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1887534
Associated Lab Samples:92321732001
Matrix:Water
AnalyzedMDL
Iron, Ferrous mg/L ND 0.50 N212/13/16 03:390.50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1887535LABORATORY CONTROL SAMPLE:
LCSSpike
Iron, Ferrous mg/L 1.5 N21.5 102 90-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92321732001
1887536SAMPLE DUPLICATE:
Iron, Ferrous mg/L 2.5 H1,N21102.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 10:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321732
Surry Closed-Mt. Airy (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
339319
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92321732001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1881556
Associated Lab Samples:92321732001
Matrix:Water
AnalyzedMDL
Sulfide ug/L ND 1000 12/05/16 15:00100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1881557LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 484J500 97 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1881558MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321642041
1881559
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 100 80-120100 0 10500ND500J499J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 10:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321732
Surry Closed-Mt. Airy (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
339763
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92321732001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1884283
Associated Lab Samples:92321732001
Matrix:Water
AnalyzedMDL
Sulfate ug/L ND 250000 12/08/16 00:071000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1884284LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 19800J20000 99 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1884285MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321623044
1884286
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L 20000 93 90-11093 1 10200003.9 mg/L 22600J 22400J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1884287MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321663001
1884288
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L 20000 94 90-11095 0 102000025.1 mg/L 43900J 44000J
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 10:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321732
Surry Closed-Mt. Airy (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
339806
SM 4500-Cl-E
SM 4500-Cl-E
4500 Chloride
Associated Lab Samples:92321732001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1884587
Associated Lab Samples:92321732001
Matrix:Water
AnalyzedMDL
Chloride ug/L ND 1000 12/07/16 18:19500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1884588LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride ug/L 2120020000 106 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1884589MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92320983006
1884590
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L M11000021190-110213 1 101000096303080030900
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1884591MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92320983015
1884592
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L 10000 107 90-110106 1 1010000145002520025000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 10:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321732
Surry Closed-Mt. Airy (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
339404
SM 5220D
SM 5220D
5220D COD
Associated Lab Samples:92321732001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1882284
Associated Lab Samples:92321732001
Matrix:Water
AnalyzedMDL
Chemical Oxygen Demand ug/L ND 25000 12/06/16 00:2212500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1882285LABORATORY CONTROL SAMPLE:
LCSSpike
Chemical Oxygen Demand ug/L 757000750000 101 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1882286MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321525002
1882287
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L M6750000-53 90-110-27 2 375000011000
mg/L
1060000
0
1080000
0
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1882288MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321681001
1882289
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L 750000 102 90-110102 0 375000032.0 mg/L 797000 797000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 10:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92321732
Surry Closed-Mt. Airy (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
340598
SM 5310B
SM 5310B
5310B TOC
Associated Lab Samples:92321732001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1888910
Associated Lab Samples:92321732001
Matrix:Water
AnalyzedMDL
Total Organic Carbon ug/L ND 1000 12/14/16 15:26500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1888911LABORATORY CONTROL SAMPLE:
LCSSpike
Total Organic Carbon ug/L 2520025000 101 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1888912MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92322500014
1888913
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Total Organic Carbon ug/L 25000 101 90-110102 1 1025000ND2530025600
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1888914MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92322946001
1888915
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Total Organic Carbon ug/L 25000 102 90-110102 0 10250005.1 mg/L 30700 30600
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 10:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 35
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92321732
Surry Closed-Mt. Airy (MNA)
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
ANALYTE QUALIFIERS
Analysis conducted outside the EPA method holding time.H1
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6
The lab does not hold NELAC/TNI accreditation for this parameter.N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 10:16 AM
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9800 Kincey Ave. Suite 100
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Page 13 of 35
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92321732
Surry Closed-Mt. Airy (MNA)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92321732001 339291MW-15 SM 2320B
92321732001 340277MW-15 SM 3500-Fe B
92321732001 339319MW-15 SM 4500-S2D
92321732001 339763MW-15 EPA 300.0
92321732001 339806MW-15 SM 4500-Cl-E
92321732001 339404MW-15 SM 5220D
92321732001 340598MW-15 SM 5310B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/19/2016 10:16 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 35
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#=CL#
December 21, 2016
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92322158
92322158
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
Surry Blanks
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on December 06, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 24
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92322158
Surry Blanks
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 24
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92322158
Surry Blanks
Lab ID Sample ID Matrix Date Collected Date Received
92322158001 EB Water 12/03/16 07:00 12/06/16 08:31
92322158002 FB Water 12/03/16 07:10 12/06/16 08:31
92322158003 TB Water 12/03/16 00:00 12/06/16 08:31
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 3 of 24
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92322158
Surry Blanks
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92322158001 EB EPA 6010 15 PASI-AJMW
EPA 8260 50 PASI-CGAW
92322158002 FB EPA 6010 15 PASI-AJMW, SH1
EPA 8260 50 PASI-CGAW
92322158003 TB EPA 8260 50 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92322158
Surry Blanks
Sample:EB Lab ID:92322158001 Collected:12/03/16 07:00 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/13/16 14:56 7440-36-012/09/16 04:356.0 3.8 1
Arsenic 3.3J ug/L 12/13/16 14:56 7440-38-2 B12/09/16 04:3510.0 2.5 1
Barium ND ug/L 12/13/16 14:56 7440-39-312/09/16 04:351002.5 1
Beryllium ND ug/L 12/13/16 14:56 7440-41-712/09/16 04:351.0 0.50 1
Cadmium ND ug/L 12/13/16 14:56 7440-43-912/09/16 04:351.0 0.50 1
Chromium ND ug/L 12/13/16 14:56 7440-47-312/09/16 04:3510.0 2.5 1
Cobalt ND ug/L 12/13/16 14:56 7440-48-412/09/16 04:3510.0 2.5 1
Copper ND ug/L 12/13/16 14:56 7440-50-812/09/16 04:3510.0 2.5 1
Lead ND ug/L 12/13/16 14:56 7439-92-112/09/16 04:3510.0 2.5 1
Nickel ND ug/L 12/13/16 14:56 7440-02-012/09/16 04:3550.0 2.5 1
Selenium ND ug/L 12/13/16 14:56 7782-49-212/09/16 04:3510.0 5.0 1
Silver ND ug/L 12/13/16 14:56 7440-22-412/09/16 04:3510.0 2.5 1
Thallium ND ug/L 12/13/16 14:56 7440-28-012/09/16 04:355.5 5.0 1
Vanadium ND ug/L 12/13/16 14:56 7440-62-212/09/16 04:3525.0 2.5 1
Zinc ND ug/L 12/13/16 14:56 7440-66-612/09/16 04:3510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/08/16 00:36 67-64-110010.0 1
Acrylonitrile ND ug/L 12/08/16 00:36 107-13-12001.9 1
Benzene ND ug/L 12/08/16 00:36 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/08/16 00:36 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/08/16 00:36 75-27-41.0 0.18 1
Bromoform ND ug/L 12/08/16 00:36 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/08/16 00:36 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/08/16 00:36 78-93-31000.96 1
Carbon disulfide ND ug/L 12/08/16 00:36 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/08/16 00:36 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/08/16 00:36 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/08/16 00:36 75-00-310.0 0.54 1
Chloroform ND ug/L 12/08/16 00:36 67-66-35.0 0.14 1
Chloromethane 0.22J ug/L 12/08/16 00:36 74-87-3 B1.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/08/16 00:36 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/08/16 00:36 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/08/16 00:36 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/08/16 00:36 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/08/16 00:36 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/08/16 00:36 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/08/16 00:36 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/08/16 00:36 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/08/16 00:36 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/08/16 00:36 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/08/16 00:36 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/08/16 00:36 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/08/16 00:36 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/08/16 00:36 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/08/16 00:36 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/21/2016 09:37 AM
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Page 5 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92322158
Surry Blanks
Sample:EB Lab ID:92322158001 Collected:12/03/16 07:00 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/08/16 00:36 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/08/16 00:36 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/08/16 00:36 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/08/16 00:36 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/08/16 00:36 108-10-11000.33 1
Styrene ND ug/L 12/08/16 00:36 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/08/16 00:36 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/08/16 00:36 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/08/16 00:36 127-18-41.0 0.46 1
Toluene ND ug/L 12/08/16 00:36 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/08/16 00:36 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/08/16 00:36 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/08/16 00:36 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/08/16 00:36 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/08/16 00:36 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/08/16 00:36 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/08/16 00:36 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/08/16 00:36 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %12/08/16 00:36 460-00-470-130 1
1,2-Dichloroethane-d4 (S)89 %12/08/16 00:36 17060-07-070-130 1
Toluene-d8 (S)112 %12/08/16 00:36 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/21/2016 09:37 AM
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Page 6 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92322158
Surry Blanks
Sample:FB Lab ID:92322158002 Collected:12/03/16 07:10 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/16/16 23:30 7440-36-012/14/16 21:406.0 3.8 1
Arsenic 3.4J ug/L 12/18/16 19:45 7440-38-212/14/16 21:4010.0 2.5 1
Barium ND ug/L 12/16/16 23:30 7440-39-312/14/16 21:401002.5 1
Beryllium ND ug/L 12/16/16 23:30 7440-41-712/14/16 21:401.0 0.50 1
Cadmium ND ug/L 12/16/16 23:30 7440-43-912/14/16 21:401.0 0.50 1
Chromium ND ug/L 12/16/16 23:30 7440-47-312/14/16 21:4010.0 2.5 1
Cobalt ND ug/L 12/16/16 23:30 7440-48-412/14/16 21:4010.0 2.5 1
Copper ND ug/L 12/16/16 23:30 7440-50-812/14/16 21:4010.0 2.5 1
Lead ND ug/L 12/16/16 23:30 7439-92-112/14/16 21:4010.0 2.5 1
Nickel ND ug/L 12/16/16 23:30 7440-02-012/14/16 21:4050.0 2.5 1
Selenium ND ug/L 12/16/16 23:30 7782-49-212/14/16 21:4010.0 5.0 1
Silver ND ug/L 12/16/16 23:30 7440-22-412/14/16 21:4010.0 2.5 1
Thallium ND ug/L 12/16/16 23:30 7440-28-012/14/16 21:405.5 5.0 1
Vanadium ND ug/L 12/16/16 23:30 7440-62-212/14/16 21:4025.0 2.5 1
Zinc ND ug/L 12/16/16 23:30 7440-66-612/14/16 21:4010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/08/16 00:52 67-64-110010.0 1
Acrylonitrile ND ug/L 12/08/16 00:52 107-13-12001.9 1
Benzene ND ug/L 12/08/16 00:52 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/08/16 00:52 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/08/16 00:52 75-27-41.0 0.18 1
Bromoform ND ug/L 12/08/16 00:52 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/08/16 00:52 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/08/16 00:52 78-93-31000.96 1
Carbon disulfide ND ug/L 12/08/16 00:52 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/08/16 00:52 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/08/16 00:52 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/08/16 00:52 75-00-310.0 0.54 1
Chloroform ND ug/L 12/08/16 00:52 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/08/16 00:52 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/08/16 00:52 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/08/16 00:52 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/08/16 00:52 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/08/16 00:52 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/08/16 00:52 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/08/16 00:52 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/08/16 00:52 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/08/16 00:52 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/08/16 00:52 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/08/16 00:52 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/08/16 00:52 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/08/16 00:52 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/08/16 00:52 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/08/16 00:52 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/08/16 00:52 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/21/2016 09:37 AM
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Huntersville, NC 28078
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Page 7 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92322158
Surry Blanks
Sample:FB Lab ID:92322158002 Collected:12/03/16 07:10 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/08/16 00:52 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/08/16 00:52 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/08/16 00:52 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/08/16 00:52 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/08/16 00:52 108-10-11000.33 1
Styrene ND ug/L 12/08/16 00:52 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/08/16 00:52 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/08/16 00:52 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/08/16 00:52 127-18-41.0 0.46 1
Toluene ND ug/L 12/08/16 00:52 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/08/16 00:52 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/08/16 00:52 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/08/16 00:52 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/08/16 00:52 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/08/16 00:52 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/08/16 00:52 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/08/16 00:52 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/08/16 00:52 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %12/08/16 00:52 460-00-470-130 1
1,2-Dichloroethane-d4 (S)90 %12/08/16 00:52 17060-07-070-130 1
Toluene-d8 (S)108 %12/08/16 00:52 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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Page 8 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92322158
Surry Blanks
Sample:TB Lab ID:92322158003 Collected:12/03/16 00:00 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/08/16 01:08 67-64-110010.0 1
Acrylonitrile ND ug/L 12/08/16 01:08 107-13-12001.9 1
Benzene ND ug/L 12/08/16 01:08 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/08/16 01:08 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/08/16 01:08 75-27-41.0 0.18 1
Bromoform ND ug/L 12/08/16 01:08 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/08/16 01:08 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/08/16 01:08 78-93-31000.96 1
Carbon disulfide ND ug/L 12/08/16 01:08 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/08/16 01:08 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/08/16 01:08 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/08/16 01:08 75-00-310.0 0.54 1
Chloroform ND ug/L 12/08/16 01:08 67-66-35.0 0.14 1
Chloromethane 0.50J ug/L 12/08/16 01:08 74-87-3 B1.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/08/16 01:08 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/08/16 01:08 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/08/16 01:08 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/08/16 01:08 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/08/16 01:08 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/08/16 01:08 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/08/16 01:08 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/08/16 01:08 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/08/16 01:08 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/08/16 01:08 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/08/16 01:08 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/08/16 01:08 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/08/16 01:08 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/08/16 01:08 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/08/16 01:08 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 12/08/16 01:08 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/08/16 01:08 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/08/16 01:08 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/08/16 01:08 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/08/16 01:08 108-10-11000.33 1
Styrene ND ug/L 12/08/16 01:08 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/08/16 01:08 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/08/16 01:08 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/08/16 01:08 127-18-41.0 0.46 1
Toluene ND ug/L 12/08/16 01:08 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/08/16 01:08 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/08/16 01:08 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/08/16 01:08 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/08/16 01:08 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/08/16 01:08 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/08/16 01:08 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/08/16 01:08 75-01-41.0 0.62 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/21/2016 09:37 AM
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Page 9 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92322158
Surry Blanks
Sample:TB Lab ID:92322158003 Collected:12/03/16 00:00 Received:12/06/16 08:31 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Xylene (Total)ND ug/L 12/08/16 01:08 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %12/08/16 01:08 460-00-470-130 1
1,2-Dichloroethane-d4 (S)87 %12/08/16 01:08 17060-07-070-130 1
Toluene-d8 (S)114 %12/08/16 01:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/21/2016 09:37 AM
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Page 10 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92322158
Surry Blanks
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
339672
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92322158001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1883876
Associated Lab Samples:92322158001
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 12/13/16 13:093.8
Arsenic ug/L 2.9J 10.0 12/13/16 13:092.5
Barium ug/L ND 100 12/13/16 13:092.5
Beryllium ug/L ND 1.0 12/13/16 13:090.50
Cadmium ug/L ND 1.0 12/13/16 13:090.50
Chromium ug/L ND 10.0 12/13/16 13:092.5
Cobalt ug/L ND 10.0 12/13/16 13:092.5
Copper ug/L ND 10.0 12/13/16 13:092.5
Lead ug/L ND 10.0 12/13/16 13:092.5
Nickel ug/L ND 50.0 12/13/16 13:092.5
Selenium ug/L ND 10.0 12/13/16 13:095.0
Silver ug/L ND 10.0 12/13/16 13:092.5
Thallium ug/L ND 5.5 12/13/16 13:095.0
Vanadium ug/L ND 25.0 12/13/16 13:092.5
Zinc ug/L ND 10.0 12/13/16 13:095.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1883877LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 490500 98 80-120
Arsenic ug/L 475500 95 80-120
Barium ug/L 493500 99 80-120
Beryllium ug/L 486500 97 80-120
Cadmium ug/L 487500 97 80-120
Chromium ug/L 496500 99 80-120
Cobalt ug/L 500500 100 80-120
Copper ug/L 501500 100 80-120
Lead ug/L 492500 98 80-120
Nickel ug/L 484500 97 80-120
Selenium ug/L 467500 93 80-120
Silver ug/L 246250 98 80-120
Thallium ug/L 485500 97 80-120
Vanadium ug/L 487500 97 80-120
Zinc ug/L 480500 96 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/21/2016 09:37 AM
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Page 11 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92322158
Surry Blanks
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1883878MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321691015
1883879
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 98 75-12598 1 25500ND492488
Arsenic ug/L 500 97 75-12595 2 25500ND483475
Barium ug/L 500 99 75-12599 0 2550025.0J 520 519
Beryllium ug/L 500 98 75-12598 0 25500ND490489
Cadmium ug/L 500 97 75-12597 0 25500ND487486
Chromium ug/L 500 99 75-12599 1 25500ND498495
Cobalt ug/L 500 101 75-125100 1 25500ND503500
Copper ug/L 500 102 75-125101 0 25500ND508506
Lead ug/L 500 98 75-12598 0 25500ND492490
Nickel ug/L 500 97 75-12597 0 25500ND485484
Selenium ug/L 500 96 75-12595 1 25500ND481476
Silver ug/L 250 99 75-12598 1 25250ND248246
Thallium ug/L 500 98 75-12597 0 25500ND488486
Vanadium ug/L 500 98 75-12598 0 25500ND492490
Zinc ug/L 500 97 75-12596 1 25500ND486483
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/21/2016 09:37 AM
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Page 12 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92322158
Surry Blanks
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
340698
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92322158002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1889943
Associated Lab Samples:92322158002
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 12/16/16 23:243.8
Arsenic ug/L ND 10.0 12/18/16 19:392.5
Barium ug/L ND 100 12/16/16 23:242.5
Beryllium ug/L ND 1.0 12/16/16 23:240.50
Cadmium ug/L ND 1.0 12/16/16 23:240.50
Chromium ug/L ND 10.0 12/16/16 23:242.5
Cobalt ug/L ND 10.0 12/16/16 23:242.5
Copper ug/L ND 10.0 12/16/16 23:242.5
Lead ug/L ND 10.0 12/16/16 23:242.5
Nickel ug/L ND 50.0 12/16/16 23:242.5
Selenium ug/L ND 10.0 12/16/16 23:245.0
Silver ug/L ND 10.0 12/16/16 23:242.5
Thallium ug/L ND 5.5 12/16/16 23:245.0
Vanadium ug/L ND 25.0 12/16/16 23:242.5
Zinc ug/L ND 10.0 12/16/16 23:245.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1889944LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 514500 103 80-120
Arsenic ug/L 508500 102 80-120
Barium ug/L 526500 105 80-120
Beryllium ug/L 495500 99 80-120
Cadmium ug/L 506500 101 80-120
Chromium ug/L 504500 101 80-120
Cobalt ug/L 524500 105 80-120
Copper ug/L 538500 108 80-120
Lead ug/L 520500 104 80-120
Nickel ug/L 494500 99 80-120
Selenium ug/L 526500 105 80-120
Silver ug/L 256250 103 80-120
Thallium ug/L 523500 105 80-120
Vanadium ug/L 496500 99 80-120
Zinc ug/L 522500 104 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/21/2016 09:37 AM
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Huntersville, NC 28078
[phone]
Page 13 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92322158
Surry Blanks
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1889945MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92322158002
1889946
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 102 75-125102 1 25500ND514511
Arsenic ug/L 500 99 75-125100 1 255003.4J 497 501
Barium ug/L 500 106 75-125105 1 25500ND530524
Beryllium ug/L 500 98 75-12598 0 25500ND489491
Cadmium ug/L 500 99 75-125100 0 25500ND497499
Chromium ug/L 500 99 75-125100 1 25500ND496502
Cobalt ug/L 500 105 75-125104 1 25500ND526520
Copper ug/L 500 105 75-125106 0 25500ND528530
Lead ug/L 500 104 75-125103 1 25500ND522517
Nickel ug/L 500 98 75-12598 0 25500ND488490
Selenium ug/L 500 104 75-125104 0 25500ND522519
Silver ug/L 250 100 75-125101 1 25250ND250253
Thallium ug/L 500 104 75-125105 1 25500ND522529
Vanadium ug/L 500 97 75-12598 1 25500ND486492
Zinc ug/L 500 104 75-125103 1 25500ND519516
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/21/2016 09:37 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92322158
Surry Blanks
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
339833
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92322158001, 92322158002, 92322158003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1884856
Associated Lab Samples:92322158001, 92322158002, 92322158003
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 12/08/16 00:040.33
1,1,1-Trichloroethane ug/L ND 1.0 12/08/16 00:040.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 12/08/16 00:040.40
1,1,2-Trichloroethane ug/L ND 1.0 12/08/16 00:040.29
1,1-Dichloroethane ug/L ND 5.0 12/08/16 00:040.32
1,1-Dichloroethene ug/L ND 5.0 12/08/16 00:040.56
1,2,3-Trichloropropane ug/L ND 1.0 12/08/16 00:040.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 12/08/16 00:042.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 12/08/16 00:040.27
1,2-Dichlorobenzene ug/L ND 5.0 12/08/16 00:040.30
1,2-Dichloroethane ug/L ND 1.0 12/08/16 00:040.24
1,2-Dichloropropane ug/L ND 1.0 12/08/16 00:040.27
1,4-Dichlorobenzene ug/L ND 1.0 12/08/16 00:040.33
2-Butanone (MEK)ug/L ND 100 12/08/16 00:040.96
2-Hexanone ug/L ND 50.0 12/08/16 00:040.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 12/08/16 00:040.33
Acetone ug/L ND 100 12/08/16 00:0410.0
Acrylonitrile ug/L ND 200 12/08/16 00:041.9
Benzene ug/L ND 1.0 12/08/16 00:040.25
Bromochloromethane ug/L ND 3.0 12/08/16 00:040.17
Bromodichloromethane ug/L ND 1.0 12/08/16 00:040.18
Bromoform ug/L ND 3.0 12/08/16 00:040.26
Bromomethane ug/L ND 10.0 12/08/16 00:040.29
Carbon disulfide ug/L ND 100 12/08/16 00:041.2
Carbon tetrachloride ug/L ND 1.0 12/08/16 00:040.25
Chlorobenzene ug/L ND 3.0 12/08/16 00:040.23
Chloroethane ug/L ND 10.0 12/08/16 00:040.54
Chloroform ug/L ND 5.0 12/08/16 00:040.14
Chloromethane ug/L 0.25J 1.0 12/08/16 00:040.11
cis-1,2-Dichloroethene ug/L ND 5.0 12/08/16 00:040.19
cis-1,3-Dichloropropene ug/L ND 1.0 12/08/16 00:040.13
Dibromochloromethane ug/L ND 3.0 12/08/16 00:040.21
Dibromomethane ug/L ND 10.0 12/08/16 00:040.21
Ethylbenzene ug/L ND 1.0 12/08/16 00:040.30
Iodomethane ug/L ND 10.0 12/08/16 00:040.32
Methylene Chloride ug/L ND 1.0 12/08/16 00:040.97
Styrene ug/L ND 1.0 12/08/16 00:040.26
Tetrachloroethene ug/L ND 1.0 12/08/16 00:040.46
Toluene ug/L ND 1.0 12/08/16 00:040.26
trans-1,2-Dichloroethene ug/L ND 5.0 12/08/16 00:040.49
trans-1,3-Dichloropropene ug/L ND 1.0 12/08/16 00:040.26
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/21/2016 09:37 AM
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Page 15 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92322158
Surry Blanks
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1884856
Associated Lab Samples:92322158001, 92322158002, 92322158003
Matrix:Water
AnalyzedMDL
trans-1,4-Dichloro-2-butene ug/L ND 100 12/08/16 00:041.0
Trichloroethene ug/L ND 1.0 12/08/16 00:040.47
Trichlorofluoromethane ug/L ND 1.0 12/08/16 00:040.20
Vinyl acetate ug/L ND 50.0 12/08/16 00:040.35
Vinyl chloride ug/L ND 1.0 12/08/16 00:040.62
Xylene (Total)ug/L ND 5.0 12/08/16 00:040.66
1,2-Dichloroethane-d4 (S)%88 70-130 12/08/16 00:04
4-Bromofluorobenzene (S)%100 70-130 12/08/16 00:04
Toluene-d8 (S)%109 70-130 12/08/16 00:04
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1884857LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 57.450 115 80-125
1,1,1-Trichloroethane ug/L 52.450 105 71-129
1,1,2,2-Tetrachloroethane ug/L 54.550 109 79-124
1,1,2-Trichloroethane ug/L 55.750 111 85-125
1,1-Dichloroethane ug/L 47.750 95 73-126
1,1-Dichloroethene ug/L 44.750 89 66-135
1,2,3-Trichloropropane ug/L 54.350 109 75-130
1,2-Dibromo-3-chloropropane ug/L 56.650 113 71-133
1,2-Dibromoethane (EDB)ug/L 59.250 118 83-124
1,2-Dichlorobenzene ug/L 54.950 110 80-133
1,2-Dichloroethane ug/L 49.450 99 67-128
1,2-Dichloropropane ug/L 51.450 103 75-132
1,4-Dichlorobenzene ug/L 51.450 103 78-130
2-Butanone (MEK)ug/L 107100 107 61-144
2-Hexanone ug/L 124100 124 68-143
4-Methyl-2-pentanone (MIBK)ug/L 111100 111 72-135
Acetone ug/L 115100 115 48-146
Acrylonitrile ug/L 264250 106 40-160
Benzene ug/L 54.350 109 80-125
Bromochloromethane ug/L 49.550 99 71-125
Bromodichloromethane ug/L 55.650 111 78-124
Bromoform ug/L 55.950 112 71-128
Bromomethane ug/L 35.050 70 40-160
Carbon disulfide ug/L 45.3J50 91 50-160
Carbon tetrachloride ug/L 54.350 109 69-131
Chlorobenzene ug/L 51.650 103 81-122
Chloroethane ug/L 48.650 97 39-148
Chloroform ug/L 49.750 99 73-127
Chloromethane ug/L 35.550 71 44-146
cis-1,2-Dichloroethene ug/L 47.850 96 74-124
cis-1,3-Dichloropropene ug/L 50.150 100 72-132
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/21/2016 09:37 AM
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Page 16 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92322158
Surry Blanks
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1884857LABORATORY CONTROL SAMPLE:
LCSSpike
Dibromochloromethane ug/L 52.850 106 78-125
Dibromomethane ug/L 50.350 101 82-120
Ethylbenzene ug/L 51.850 104 79-121
Iodomethane ug/L 85.2100 85 39-154
Methylene Chloride ug/L 44.150 88 64-133
Styrene ug/L 51.950 104 84-126
Tetrachloroethene ug/L 49.850 100 78-122
Toluene ug/L 49.250 98 80-121
trans-1,2-Dichloroethene ug/L 44.850 90 71-127
trans-1,3-Dichloropropene ug/L 55.450 111 69-141
trans-1,4-Dichloro-2-butene ug/L 61.3J50 123 40-160
Trichloroethene ug/L 54.950 110 78-122
Trichlorofluoromethane ug/L 50.950 102 53-137
Vinyl acetate ug/L 97.0100 97 40-160
Vinyl chloride ug/L 41.450 83 58-137
Xylene (Total)ug/L 151150 101 81-126
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%95 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1884859MATRIX SPIKE SAMPLE:
MSSpike
Result
92321900011
1,1,1,2-Tetrachloroethane ug/L 20.720 103 70-130ND
1,1,1-Trichloroethane ug/L 22.220 111 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.920 104 70-130ND
1,1,2-Trichloroethane ug/L 20.420 102 70-130ND
1,1-Dichloroethane ug/L 21.720 109 70-130ND
1,1-Dichloroethene ug/L 21.020 105 70-166ND
1,2,3-Trichloropropane ug/L 21.320 107 70-130ND
1,2-Dibromo-3-chloropropane ug/L 22.220 111 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.020 105 70-130ND
1,2-Dichlorobenzene ug/L 22.220 111 70-130ND
1,2-Dichloroethane ug/L 21.120 105 70-130ND
1,2-Dichloropropane ug/L 21.020 105 70-130ND
1,4-Dichlorobenzene ug/L 20.720 104 70-130ND
2-Butanone (MEK)ug/L 42.1J40 105 70-130ND
2-Hexanone ug/L 47.0J40 117 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 44.0J40 110 70-130ND
Acetone ug/L 41.2J40 101 70-130ND
Acrylonitrile ug/L 113J100 113 70-130ND
Benzene ug/L 22.920 114 70-148ND
Bromochloromethane ug/L 21.920 109 70-130ND
Bromodichloromethane ug/L 22.920 115 70-130ND
Bromoform ug/L 19.620 98 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/21/2016 09:37 AM
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Page 17 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92322158
Surry Blanks
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1884859MATRIX SPIKE SAMPLE:
MSSpike
Result
92321900011
Bromomethane ug/L 17.720 88 70-130ND
Carbon disulfide ug/L 21.1J20 105 70-130ND
Carbon tetrachloride ug/L 24.420 122 70-130ND
Chlorobenzene ug/L 21.720 109 70-146ND
Chloroethane ug/L 21.520 107 70-130ND
Chloroform ug/L 21.720 109 70-130ND
Chloromethane ug/L 15.520 77 70-130ND
cis-1,2-Dichloroethene ug/L 21.420 107 70-130ND
cis-1,3-Dichloropropene ug/L 18.620 93 70-130ND
Dibromochloromethane ug/L 19.720 99 70-130ND
Dibromomethane ug/L 21.820 109 70-130ND
Ethylbenzene ug/L 22.420 112 70-130ND
Iodomethane ug/L 29.340 73 70-130ND
Methylene Chloride ug/L 18.520 92 70-130ND
Styrene ug/L 20.420 102 70-130ND
Tetrachloroethene ug/L 20.920 104 70-130ND
Toluene ug/L 22.520 112 70-155ND
trans-1,2-Dichloroethene ug/L 20.320 101 70-130ND
trans-1,3-Dichloropropene ug/L 19.320 97 70-130ND
trans-1,4-Dichloro-2-butene ug/L 18.7J20 94 70-130ND
Trichloroethene ug/L 21.820 109 69-151ND
Trichlorofluoromethane ug/L 23.020 115 70-130ND
Vinyl acetate ug/L 28.8J40 72 70-130ND
Vinyl chloride ug/L 18.920 94 70-130ND
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92321900010
1884858SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/21/2016 09:37 AM
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Page 18 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92322158
Surry Blanks
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92321900010
1884858SAMPLE DUPLICATE:
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L 0.26J 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%90 192
4-Bromofluorobenzene (S)%100 1101
Toluene-d8 (S)%112 4107
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/21/2016 09:37 AM
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Page 19 of 24
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92322158
Surry Blanks
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/21/2016 09:37 AM
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Page 20 of 24
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92322158
Surry Blanks
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92322158001 339672 340243EBEPA 3010A EPA 6010
92322158002 340698 340963FBEPA 3010A EPA 6010
92322158001 339833EBEPA 8260
92322158002 339833FBEPA 8260
92322158003 339833TBEPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/21/2016 09:37 AM
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Page 21 of 24
Page 22 of 24
Page 23 of 24
Page 24 of 24
#=CL#
January 10, 2017
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92325731
92325731
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
Surry MSWLF SWs
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on December 02, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 1 of 34
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92325731
Surry MSWLF SWs
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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Page 2 of 34
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92325731
Surry MSWLF SWs
Lab ID Sample ID Matrix Date Collected Date Received
92321678001 SW-1 Water 11/29/16 13:15 12/02/16 07:09
92321678002 SW-2 Water 11/29/16 13:30 12/02/16 07:09
92321678003 SW-3 Water 11/29/16 13:45 12/02/16 07:09
92321678004 SW-4 Water 11/29/16 13:00 12/02/16 07:09
92321678005 SWN-1 Water 11/30/16 08:20 12/02/16 07:09
92321678006 SWN-2 Water 11/30/16 14:10 12/02/16 07:09
92321678007 SW-A Water 11/29/16 14:20 12/02/16 07:09
92321678008 SW-B Water 11/29/16 14:20 12/02/16 07:09
REPORT OF LABORATORY ANALYSIS
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Page 3 of 34
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92325731
Surry MSWLF SWs
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92321678001 SW-1 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CZDO
92321678002 SW-2 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 50 PASI-CZDO
92321678003 SW-3 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CZDO
92321678004 SW-4 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 50 PASI-CZDO
92321678005 SWN-1 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 50 PASI-CZDO
92321678006 SWN-2 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 50 PASI-CZDO
92321678007 SW-A EPA 8260 50 PASI-CZDO
92321678008 SW-B EPA 8260 50 PASI-CZDO
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 4 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325731
Surry MSWLF SWs
Sample:SW-1 Lab ID:92321678001 Collected:11/29/16 13:15 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/09/16 02:28 7440-36-012/06/16 03:306.0 3.8 1
Arsenic ND ug/L 12/09/16 02:28 7440-38-212/06/16 03:3010.0 2.5 1
Barium 27.5J ug/L 12/09/16 02:28 7440-39-312/06/16 03:301002.5 1
Beryllium ND ug/L 12/09/16 02:28 7440-41-712/06/16 03:301.0 0.50 1
Cadmium ND ug/L 12/09/16 02:28 7440-43-912/06/16 03:301.0 0.50 1
Chromium ND ug/L 12/09/16 02:28 7440-47-312/06/16 03:3010.0 2.5 1
Cobalt ND ug/L 12/09/16 02:28 7440-48-412/06/16 03:3010.0 2.5 1
Copper ND ug/L 12/09/16 02:28 7440-50-812/06/16 03:3010.0 2.5 1
Lead ND ug/L 12/09/16 02:28 7439-92-112/06/16 03:3010.0 2.5 1
Nickel ND ug/L 12/09/16 02:28 7440-02-012/06/16 03:3050.0 2.5 1
Selenium ND ug/L 12/09/16 02:28 7782-49-212/06/16 03:3010.0 5.0 1
Silver ND ug/L 12/09/16 02:28 7440-22-412/06/16 03:3010.0 2.5 1
Thallium ND ug/L 12/09/16 02:28 7440-28-012/06/16 03:305.5 5.0 1
Vanadium ND ug/L 12/09/16 02:28 7440-62-212/06/16 03:3025.0 2.5 1
Zinc ND ug/L 12/09/16 02:28 7440-66-612/06/16 03:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/08/16 00:00 67-64-110010.0 1
Acrylonitrile ND ug/L 12/08/16 00:00 107-13-12001.9 1
Benzene ND ug/L 12/08/16 00:00 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/08/16 00:00 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/08/16 00:00 75-27-41.0 0.18 1
Bromoform ND ug/L 12/08/16 00:00 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/08/16 00:00 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/08/16 00:00 78-93-31000.96 1
Carbon disulfide ND ug/L 12/08/16 00:00 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/08/16 00:00 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/08/16 00:00 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/08/16 00:00 75-00-310.0 0.54 1
Chloroform ND ug/L 12/08/16 00:00 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/08/16 00:00 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/08/16 00:00 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/08/16 00:00 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/08/16 00:00 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/08/16 00:00 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/08/16 00:00 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/08/16 00:00 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/08/16 00:00 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/08/16 00:00 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/08/16 00:00 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/08/16 00:00 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/08/16 00:00 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/08/16 00:00 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/08/16 00:00 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/08/16 00:00 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/08/16 00:00 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/10/2017 11:48 AM
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Page 5 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325731
Surry MSWLF SWs
Sample:SW-1 Lab ID:92321678001 Collected:11/29/16 13:15 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/08/16 00:00 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/08/16 00:00 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/08/16 00:00 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/08/16 00:00 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/08/16 00:00 108-10-11000.33 1
Styrene ND ug/L 12/08/16 00:00 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/08/16 00:00 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/08/16 00:00 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/08/16 00:00 127-18-41.0 0.46 1
Toluene ND ug/L 12/08/16 00:00 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/08/16 00:00 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/08/16 00:00 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/08/16 00:00 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/08/16 00:00 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/08/16 00:00 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/08/16 00:00 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/08/16 00:00 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/08/16 00:00 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)95 %12/08/16 00:00 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %12/08/16 00:00 17060-07-070-130 1
Toluene-d8 (S)100 %12/08/16 00:00 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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Page 6 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325731
Surry MSWLF SWs
Sample:SW-2 Lab ID:92321678002 Collected:11/29/16 13:30 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/13/16 17:33 7440-36-012/06/16 22:256.0 3.8 1
Arsenic ND ug/L 12/13/16 17:33 7440-38-212/06/16 22:2510.0 2.5 1
Barium 30.4J ug/L 12/13/16 03:26 7440-39-312/06/16 22:251002.5 1
Beryllium ND ug/L 12/13/16 03:26 7440-41-712/06/16 22:251.0 0.50 1
Cadmium ND ug/L 12/13/16 17:33 7440-43-912/06/16 22:251.0 0.50 1
Chromium ND ug/L 12/13/16 03:26 7440-47-312/06/16 22:2510.0 2.5 1
Cobalt ND ug/L 12/13/16 17:33 7440-48-412/06/16 22:2510.0 2.5 1
Copper ND ug/L 12/13/16 17:33 7440-50-812/06/16 22:2510.0 2.5 1
Lead 3.4J ug/L 12/13/16 03:26 7439-92-112/06/16 22:2510.0 2.5 1
Nickel ND ug/L 12/13/16 03:26 7440-02-012/06/16 22:2550.0 2.5 1
Selenium ND ug/L 12/13/16 17:33 7782-49-212/06/16 22:2510.0 5.0 1
Silver ND ug/L 12/13/16 03:26 7440-22-412/06/16 22:2510.0 2.5 1
Thallium ND ug/L 12/13/16 17:33 7440-28-012/06/16 22:255.5 5.0 1
Vanadium ND ug/L 12/13/16 03:26 7440-62-212/06/16 22:2525.0 2.5 1
Zinc ND ug/L 12/13/16 03:26 7440-66-612/06/16 22:2510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/08/16 00:17 67-64-110010.0 1
Acrylonitrile ND ug/L 12/08/16 00:17 107-13-12001.9 1
Benzene ND ug/L 12/08/16 00:17 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/08/16 00:17 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/08/16 00:17 75-27-41.0 0.18 1
Bromoform ND ug/L 12/08/16 00:17 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/08/16 00:17 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/08/16 00:17 78-93-31000.96 1
Carbon disulfide ND ug/L 12/08/16 00:17 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/08/16 00:17 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/08/16 00:17 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/08/16 00:17 75-00-310.0 0.54 1
Chloroform ND ug/L 12/08/16 00:17 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/08/16 00:17 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/08/16 00:17 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/08/16 00:17 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/08/16 00:17 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/08/16 00:17 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/08/16 00:17 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/08/16 00:17 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/08/16 00:17 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/08/16 00:17 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/08/16 00:17 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/08/16 00:17 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/08/16 00:17 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/08/16 00:17 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/08/16 00:17 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/08/16 00:17 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/08/16 00:17 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
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Page 7 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325731
Surry MSWLF SWs
Sample:SW-2 Lab ID:92321678002 Collected:11/29/16 13:30 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/08/16 00:17 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/08/16 00:17 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/08/16 00:17 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/08/16 00:17 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/08/16 00:17 108-10-11000.33 1
Styrene ND ug/L 12/08/16 00:17 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/08/16 00:17 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/08/16 00:17 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/08/16 00:17 127-18-41.0 0.46 1
Toluene ND ug/L 12/08/16 00:17 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/08/16 00:17 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/08/16 00:17 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/08/16 00:17 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/08/16 00:17 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/08/16 00:17 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/08/16 00:17 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/08/16 00:17 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/08/16 00:17 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)94 %12/08/16 00:17 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %12/08/16 00:17 17060-07-070-130 1
Toluene-d8 (S)100 %12/08/16 00:17 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/10/2017 11:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325731
Surry MSWLF SWs
Sample:SW-3 Lab ID:92321678003 Collected:11/29/16 13:45 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/13/16 17:51 7440-36-012/06/16 22:256.0 3.8 1
Arsenic ND ug/L 12/13/16 17:51 7440-38-212/06/16 22:2510.0 2.5 1
Barium 22.2J ug/L 12/13/16 17:51 7440-39-312/06/16 22:251002.5 1
Beryllium ND ug/L 12/13/16 17:51 7440-41-712/06/16 22:251.0 0.50 1
Cadmium ND ug/L 12/13/16 17:51 7440-43-912/06/16 22:251.0 0.50 1
Chromium ND ug/L 12/13/16 17:51 7440-47-312/06/16 22:2510.0 2.5 1
Cobalt ND ug/L 12/13/16 17:51 7440-48-412/06/16 22:2510.0 2.5 1
Copper ND ug/L 12/13/16 17:51 7440-50-812/06/16 22:2510.0 2.5 1
Lead ND ug/L 12/13/16 17:51 7439-92-112/06/16 22:2510.0 2.5 1
Nickel ND ug/L 12/13/16 17:51 7440-02-012/06/16 22:2550.0 2.5 1
Selenium ND ug/L 12/13/16 17:51 7782-49-212/06/16 22:2510.0 5.0 1
Silver ND ug/L 12/13/16 17:51 7440-22-412/06/16 22:2510.0 2.5 1
Thallium ND ug/L 12/13/16 17:51 7440-28-012/06/16 22:255.5 5.0 1
Vanadium ND ug/L 12/13/16 17:51 7440-62-212/06/16 22:2525.0 2.5 1
Zinc ND ug/L 12/13/16 17:51 7440-66-612/06/16 22:2510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/08/16 00:34 67-64-110010.0 1
Acrylonitrile ND ug/L 12/08/16 00:34 107-13-12001.9 1
Benzene ND ug/L 12/08/16 00:34 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/08/16 00:34 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/08/16 00:34 75-27-41.0 0.18 1
Bromoform ND ug/L 12/08/16 00:34 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/08/16 00:34 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/08/16 00:34 78-93-31000.96 1
Carbon disulfide ND ug/L 12/08/16 00:34 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/08/16 00:34 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/08/16 00:34 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/08/16 00:34 75-00-310.0 0.54 1
Chloroform ND ug/L 12/08/16 00:34 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/08/16 00:34 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/08/16 00:34 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/08/16 00:34 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/08/16 00:34 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/08/16 00:34 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/08/16 00:34 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/08/16 00:34 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/08/16 00:34 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/08/16 00:34 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/08/16 00:34 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/08/16 00:34 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/08/16 00:34 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/08/16 00:34 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/08/16 00:34 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/08/16 00:34 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/08/16 00:34 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/10/2017 11:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325731
Surry MSWLF SWs
Sample:SW-3 Lab ID:92321678003 Collected:11/29/16 13:45 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/08/16 00:34 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/08/16 00:34 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/08/16 00:34 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/08/16 00:34 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/08/16 00:34 108-10-11000.33 1
Styrene ND ug/L 12/08/16 00:34 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/08/16 00:34 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/08/16 00:34 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/08/16 00:34 127-18-41.0 0.46 1
Toluene ND ug/L 12/08/16 00:34 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/08/16 00:34 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/08/16 00:34 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/08/16 00:34 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/08/16 00:34 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/08/16 00:34 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/08/16 00:34 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/08/16 00:34 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/08/16 00:34 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)94 %12/08/16 00:34 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %12/08/16 00:34 17060-07-070-130 1
Toluene-d8 (S)99 %12/08/16 00:34 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/10/2017 11:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325731
Surry MSWLF SWs
Sample:SW-4 Lab ID:92321678004 Collected:11/29/16 13:00 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/13/16 03:48 7440-36-012/06/16 22:256.0 3.8 1
Arsenic ND ug/L 12/13/16 17:54 7440-38-212/06/16 22:2510.0 2.5 1
Barium 24.4J ug/L 12/13/16 03:48 7440-39-312/06/16 22:251002.5 1
Beryllium ND ug/L 12/13/16 03:48 7440-41-712/06/16 22:251.0 0.50 1
Cadmium ND ug/L 12/13/16 03:48 7440-43-912/06/16 22:251.0 0.50 1
Chromium ND ug/L 12/13/16 03:48 7440-47-312/06/16 22:2510.0 2.5 1
Cobalt ND ug/L 12/13/16 03:48 7440-48-412/06/16 22:2510.0 2.5 1
Copper ND ug/L 12/13/16 03:48 7440-50-812/06/16 22:2510.0 2.5 1
Lead 2.5J ug/L 12/13/16 03:48 7439-92-112/06/16 22:2510.0 2.5 1
Nickel ND ug/L 12/13/16 03:48 7440-02-012/06/16 22:2550.0 2.5 1
Selenium ND ug/L 12/13/16 17:54 7782-49-212/06/16 22:2510.0 5.0 1
Silver ND ug/L 12/13/16 03:48 7440-22-412/06/16 22:2510.0 2.5 1
Thallium ND ug/L 12/13/16 17:54 7440-28-012/06/16 22:255.5 5.0 1
Vanadium ND ug/L 12/13/16 03:48 7440-62-212/06/16 22:2525.0 2.5 1
Zinc 5.4J ug/L 12/13/16 03:48 7440-66-612/06/16 22:2510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/08/16 00:51 67-64-110010.0 1
Acrylonitrile ND ug/L 12/08/16 00:51 107-13-12001.9 1
Benzene ND ug/L 12/08/16 00:51 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/08/16 00:51 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/08/16 00:51 75-27-41.0 0.18 1
Bromoform ND ug/L 12/08/16 00:51 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/08/16 00:51 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/08/16 00:51 78-93-31000.96 1
Carbon disulfide ND ug/L 12/08/16 00:51 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/08/16 00:51 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/08/16 00:51 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/08/16 00:51 75-00-310.0 0.54 1
Chloroform ND ug/L 12/08/16 00:51 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/08/16 00:51 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/08/16 00:51 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/08/16 00:51 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/08/16 00:51 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/08/16 00:51 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/08/16 00:51 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/08/16 00:51 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/08/16 00:51 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/08/16 00:51 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/08/16 00:51 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/08/16 00:51 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/08/16 00:51 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/08/16 00:51 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/08/16 00:51 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/08/16 00:51 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/08/16 00:51 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/10/2017 11:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325731
Surry MSWLF SWs
Sample:SW-4 Lab ID:92321678004 Collected:11/29/16 13:00 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/08/16 00:51 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/08/16 00:51 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/08/16 00:51 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/08/16 00:51 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/08/16 00:51 108-10-11000.33 1
Styrene ND ug/L 12/08/16 00:51 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/08/16 00:51 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/08/16 00:51 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/08/16 00:51 127-18-41.0 0.46 1
Toluene ND ug/L 12/08/16 00:51 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/08/16 00:51 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/08/16 00:51 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/08/16 00:51 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/08/16 00:51 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/08/16 00:51 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/08/16 00:51 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/08/16 00:51 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/08/16 00:51 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)95 %12/08/16 00:51 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %12/08/16 00:51 17060-07-070-130 1
Toluene-d8 (S)98 %12/08/16 00:51 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/10/2017 11:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325731
Surry MSWLF SWs
Sample:SWN-1 Lab ID:92321678005 Collected:11/30/16 08:20 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/13/16 03:51 7440-36-012/06/16 22:256.0 3.8 1
Arsenic ND ug/L 12/13/16 17:58 7440-38-212/06/16 22:2510.0 2.5 1
Barium 31.1J ug/L 12/13/16 03:51 7440-39-312/06/16 22:251002.5 1
Beryllium ND ug/L 12/13/16 03:51 7440-41-712/06/16 22:251.0 0.50 1
Cadmium ND ug/L 12/13/16 03:51 7440-43-912/06/16 22:251.0 0.50 1
Chromium ND ug/L 12/13/16 03:51 7440-47-312/06/16 22:2510.0 2.5 1
Cobalt ND ug/L 12/13/16 03:51 7440-48-412/06/16 22:2510.0 2.5 1
Copper ND ug/L 12/13/16 03:51 7440-50-812/06/16 22:2510.0 2.5 1
Lead ND ug/L 12/13/16 03:51 7439-92-112/06/16 22:2510.0 2.5 1
Nickel ND ug/L 12/13/16 03:51 7440-02-012/06/16 22:2550.0 2.5 1
Selenium ND ug/L 12/13/16 17:58 7782-49-212/06/16 22:2510.0 5.0 1
Silver ND ug/L 12/13/16 03:51 7440-22-412/06/16 22:2510.0 2.5 1
Thallium ND ug/L 12/13/16 17:58 7440-28-012/06/16 22:255.5 5.0 1
Vanadium ND ug/L 12/13/16 03:51 7440-62-212/06/16 22:2525.0 2.5 1
Zinc ND ug/L 12/13/16 03:51 7440-66-612/06/16 22:2510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/08/16 01:08 67-64-110010.0 1
Acrylonitrile ND ug/L 12/08/16 01:08 107-13-12001.9 1
Benzene ND ug/L 12/08/16 01:08 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/08/16 01:08 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/08/16 01:08 75-27-41.0 0.18 1
Bromoform ND ug/L 12/08/16 01:08 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/08/16 01:08 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/08/16 01:08 78-93-31000.96 1
Carbon disulfide ND ug/L 12/08/16 01:08 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/08/16 01:08 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/08/16 01:08 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/08/16 01:08 75-00-310.0 0.54 1
Chloroform ND ug/L 12/08/16 01:08 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/08/16 01:08 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/08/16 01:08 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/08/16 01:08 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/08/16 01:08 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/08/16 01:08 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/08/16 01:08 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/08/16 01:08 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/08/16 01:08 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/08/16 01:08 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/08/16 01:08 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/08/16 01:08 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/08/16 01:08 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/08/16 01:08 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/08/16 01:08 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/08/16 01:08 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/08/16 01:08 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/10/2017 11:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325731
Surry MSWLF SWs
Sample:SWN-1 Lab ID:92321678005 Collected:11/30/16 08:20 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/08/16 01:08 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/08/16 01:08 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/08/16 01:08 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/08/16 01:08 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/08/16 01:08 108-10-11000.33 1
Styrene ND ug/L 12/08/16 01:08 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/08/16 01:08 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/08/16 01:08 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/08/16 01:08 127-18-41.0 0.46 1
Toluene ND ug/L 12/08/16 01:08 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/08/16 01:08 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/08/16 01:08 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/08/16 01:08 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/08/16 01:08 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/08/16 01:08 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/08/16 01:08 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/08/16 01:08 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/08/16 01:08 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)95 %12/08/16 01:08 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %12/08/16 01:08 17060-07-070-130 1
Toluene-d8 (S)100 %12/08/16 01:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/10/2017 11:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325731
Surry MSWLF SWs
Sample:SWN-2 Lab ID:92321678006 Collected:11/30/16 14:10 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 12/13/16 03:54 7440-36-012/06/16 22:256.0 3.8 1
Arsenic ND ug/L 12/13/16 18:01 7440-38-212/06/16 22:2510.0 2.5 1
Barium 25.3J ug/L 12/13/16 03:54 7440-39-312/06/16 22:251002.5 1
Beryllium ND ug/L 12/13/16 03:54 7440-41-712/06/16 22:251.0 0.50 1
Cadmium ND ug/L 12/13/16 03:54 7440-43-912/06/16 22:251.0 0.50 1
Chromium ND ug/L 12/13/16 03:54 7440-47-312/06/16 22:2510.0 2.5 1
Cobalt ND ug/L 12/13/16 03:54 7440-48-412/06/16 22:2510.0 2.5 1
Copper ND ug/L 12/13/16 03:54 7440-50-812/06/16 22:2510.0 2.5 1
Lead ND ug/L 12/13/16 03:54 7439-92-112/06/16 22:2510.0 2.5 1
Nickel ND ug/L 12/13/16 03:54 7440-02-012/06/16 22:2550.0 2.5 1
Selenium ND ug/L 12/13/16 18:01 7782-49-212/06/16 22:2510.0 5.0 1
Silver ND ug/L 12/13/16 03:54 7440-22-412/06/16 22:2510.0 2.5 1
Thallium ND ug/L 12/13/16 18:01 7440-28-012/06/16 22:255.5 5.0 1
Vanadium ND ug/L 12/13/16 03:54 7440-62-212/06/16 22:2525.0 2.5 1
Zinc 5.3J ug/L 12/13/16 03:54 7440-66-612/06/16 22:2510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/08/16 01:26 67-64-110010.0 1
Acrylonitrile ND ug/L 12/08/16 01:26 107-13-12001.9 1
Benzene ND ug/L 12/08/16 01:26 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/08/16 01:26 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/08/16 01:26 75-27-41.0 0.18 1
Bromoform ND ug/L 12/08/16 01:26 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/08/16 01:26 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/08/16 01:26 78-93-31000.96 1
Carbon disulfide ND ug/L 12/08/16 01:26 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/08/16 01:26 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/08/16 01:26 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/08/16 01:26 75-00-310.0 0.54 1
Chloroform ND ug/L 12/08/16 01:26 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/08/16 01:26 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/08/16 01:26 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/08/16 01:26 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/08/16 01:26 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/08/16 01:26 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/08/16 01:26 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/08/16 01:26 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/08/16 01:26 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/08/16 01:26 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/08/16 01:26 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/08/16 01:26 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/08/16 01:26 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/08/16 01:26 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/08/16 01:26 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/08/16 01:26 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/08/16 01:26 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/10/2017 11:48 AM
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Page 15 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325731
Surry MSWLF SWs
Sample:SWN-2 Lab ID:92321678006 Collected:11/30/16 14:10 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 12/08/16 01:26 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/08/16 01:26 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/08/16 01:26 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/08/16 01:26 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/08/16 01:26 108-10-11000.33 1
Styrene ND ug/L 12/08/16 01:26 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/08/16 01:26 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/08/16 01:26 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/08/16 01:26 127-18-41.0 0.46 1
Toluene ND ug/L 12/08/16 01:26 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/08/16 01:26 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/08/16 01:26 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/08/16 01:26 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/08/16 01:26 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/08/16 01:26 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/08/16 01:26 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/08/16 01:26 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 12/08/16 01:26 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)95 %12/08/16 01:26 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %12/08/16 01:26 17060-07-070-130 1
Toluene-d8 (S)97 %12/08/16 01:26 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/10/2017 11:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 16 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325731
Surry MSWLF SWs
Sample:SW-A Lab ID:92321678007 Collected:11/29/16 14:20 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/08/16 01:43 67-64-110010.0 1
Acrylonitrile ND ug/L 12/08/16 01:43 107-13-12001.9 1
Benzene ND ug/L 12/08/16 01:43 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/08/16 01:43 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/08/16 01:43 75-27-41.0 0.18 1
Bromoform ND ug/L 12/08/16 01:43 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/08/16 01:43 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/08/16 01:43 78-93-31000.96 1
Carbon disulfide ND ug/L 12/08/16 01:43 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/08/16 01:43 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/08/16 01:43 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/08/16 01:43 75-00-310.0 0.54 1
Chloroform ND ug/L 12/08/16 01:43 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/08/16 01:43 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/08/16 01:43 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/08/16 01:43 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/08/16 01:43 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/08/16 01:43 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/08/16 01:43 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/08/16 01:43 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/08/16 01:43 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/08/16 01:43 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/08/16 01:43 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/08/16 01:43 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/08/16 01:43 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/08/16 01:43 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/08/16 01:43 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/08/16 01:43 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/08/16 01:43 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 12/08/16 01:43 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/08/16 01:43 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/08/16 01:43 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/08/16 01:43 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/08/16 01:43 108-10-11000.33 1
Styrene ND ug/L 12/08/16 01:43 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/08/16 01:43 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/08/16 01:43 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/08/16 01:43 127-18-41.0 0.46 1
Toluene ND ug/L 12/08/16 01:43 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/08/16 01:43 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/08/16 01:43 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/08/16 01:43 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/08/16 01:43 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/08/16 01:43 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/08/16 01:43 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/08/16 01:43 75-01-41.0 0.62 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/10/2017 11:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325731
Surry MSWLF SWs
Sample:SW-A Lab ID:92321678007 Collected:11/29/16 14:20 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Xylene (Total)ND ug/L 12/08/16 01:43 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)95 %12/08/16 01:43 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %12/08/16 01:43 17060-07-070-130 1
Toluene-d8 (S)99 %12/08/16 01:43 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/10/2017 11:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325731
Surry MSWLF SWs
Sample:SW-B Lab ID:92321678008 Collected:11/29/16 14:20 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 12/08/16 02:00 67-64-110010.0 1
Acrylonitrile ND ug/L 12/08/16 02:00 107-13-12001.9 1
Benzene ND ug/L 12/08/16 02:00 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 12/08/16 02:00 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 12/08/16 02:00 75-27-41.0 0.18 1
Bromoform ND ug/L 12/08/16 02:00 75-25-23.0 0.26 1
Bromomethane ND ug/L 12/08/16 02:00 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 12/08/16 02:00 78-93-31000.96 1
Carbon disulfide ND ug/L 12/08/16 02:00 75-15-01001.2 1
Carbon tetrachloride ND ug/L 12/08/16 02:00 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 12/08/16 02:00 108-90-73.0 0.23 1
Chloroethane ND ug/L 12/08/16 02:00 75-00-310.0 0.54 1
Chloroform ND ug/L 12/08/16 02:00 67-66-35.0 0.14 1
Chloromethane ND ug/L 12/08/16 02:00 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 12/08/16 02:00 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 12/08/16 02:00 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 12/08/16 02:00 106-93-41.0 0.27 1
Dibromomethane ND ug/L 12/08/16 02:00 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 12/08/16 02:00 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 12/08/16 02:00 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 12/08/16 02:00 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 12/08/16 02:00 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 12/08/16 02:00 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 12/08/16 02:00 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 12/08/16 02:00 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 12/08/16 02:00 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 12/08/16 02:00 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 12/08/16 02:00 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 12/08/16 02:00 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 12/08/16 02:00 100-41-41.0 0.30 1
2-Hexanone ND ug/L 12/08/16 02:00 591-78-650.0 0.46 1
Iodomethane ND ug/L 12/08/16 02:00 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 12/08/16 02:00 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 12/08/16 02:00 108-10-11000.33 1
Styrene ND ug/L 12/08/16 02:00 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 12/08/16 02:00 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 12/08/16 02:00 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 12/08/16 02:00 127-18-41.0 0.46 1
Toluene ND ug/L 12/08/16 02:00 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 12/08/16 02:00 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 12/08/16 02:00 79-00-51.0 0.29 1
Trichloroethene ND ug/L 12/08/16 02:00 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 12/08/16 02:00 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 12/08/16 02:00 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 12/08/16 02:00 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 12/08/16 02:00 75-01-41.0 0.62 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/10/2017 11:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325731
Surry MSWLF SWs
Sample:SW-B Lab ID:92321678008 Collected:11/29/16 14:20 Received:12/02/16 07:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Xylene (Total)ND ug/L 12/08/16 02:00 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)95 %12/08/16 02:00 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %12/08/16 02:00 17060-07-070-130 1
Toluene-d8 (S)100 %12/08/16 02:00 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/10/2017 11:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325731
Surry MSWLF SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
339257
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92321678001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1881364
Associated Lab Samples:92321678001
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 12/09/16 00:573.8
Arsenic ug/L 2.7J 10.0 12/09/16 00:572.5
Barium ug/L ND 100 12/09/16 00:572.5
Beryllium ug/L ND 1.0 12/09/16 00:570.50
Cadmium ug/L ND 1.0 12/09/16 00:570.50
Chromium ug/L ND 10.0 12/09/16 00:572.5
Cobalt ug/L ND 10.0 12/09/16 00:572.5
Copper ug/L ND 10.0 12/09/16 00:572.5
Lead ug/L ND 10.0 12/09/16 00:572.5
Nickel ug/L ND 50.0 12/09/16 00:572.5
Selenium ug/L ND 10.0 12/09/16 00:575.0
Silver ug/L ND 10.0 12/09/16 00:572.5
Thallium ug/L ND 5.5 12/09/16 00:575.0
Vanadium ug/L ND 25.0 12/09/16 00:572.5
Zinc ug/L ND 10.0 12/09/16 00:575.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1881365LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 440500 88 80-120
Arsenic ug/L 447500 89 80-120
Barium ug/L 458500 92 80-120
Beryllium ug/L 482500 96 80-120
Cadmium ug/L 448500 90 80-120
Chromium ug/L 482500 96 80-120
Cobalt ug/L 461500 92 80-120
Copper ug/L 475500 95 80-120
Lead ug/L 455500 91 80-120
Nickel ug/L 447500 89 80-120
Selenium ug/L 450500 90 80-120
Silver ug/L 235250 94 80-120
Thallium ug/L 447500 89 80-120
Vanadium ug/L 463500 93 80-120
Zinc ug/L 483500 97 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/10/2017 11:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325731
Surry MSWLF SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1881366MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92320983001
1881367
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 88 75-12586 3 25500ND442428
Arsenic ug/L 500 88 75-12587 2 25500ND444434
Barium ug/L 500 92 75-12589 4 25500ND460443
Beryllium ug/L 500 96 75-12595 1 25500ND478474
Cadmium ug/L 500 89 75-12586 3 25500ND444431
Chromium ug/L 500 96 75-12593 3 25500ND480468
Cobalt ug/L 500 92 75-12590 2 25500ND462452
Copper ug/L 500 94 75-12591 4 25500ND471455
Lead ug/L 500 91 75-12589 2 25500ND454446
Nickel ug/L 500 89 75-12587 3 25500ND446434
Selenium ug/L 500 88 75-12586 3 25500ND442431
Silver ug/L 250 93 75-12593 0 25250ND234233
Thallium ug/L 500 90 75-12589 0 25500ND450449
Vanadium ug/L 500 92 75-12593 1 25500ND462466
Zinc ug/L 500 97 75-12597 0 25500ND487488
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/10/2017 11:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325731
Surry MSWLF SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
339341
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92321678002, 92321678003, 92321678004, 92321678005, 92321678006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1881715
Associated Lab Samples:92321678002, 92321678003, 92321678004, 92321678005, 92321678006
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 12/13/16 17:273.8
Arsenic ug/L ND 10.0 12/13/16 17:272.5
Barium ug/L ND 100 12/13/16 03:202.5
Beryllium ug/L ND 1.0 12/13/16 03:200.50
Cadmium ug/L ND 1.0 12/13/16 17:270.50
Chromium ug/L ND 10.0 12/13/16 03:202.5
Cobalt ug/L ND 10.0 12/13/16 17:272.5
Copper ug/L ND 10.0 12/13/16 17:272.5
Lead ug/L ND 10.0 12/13/16 03:202.5
Nickel ug/L ND 50.0 12/13/16 03:202.5
Selenium ug/L ND 10.0 12/13/16 17:275.0
Silver ug/L ND 10.0 12/13/16 03:202.5
Thallium ug/L ND 5.5 12/13/16 17:275.0
Vanadium ug/L ND 25.0 12/13/16 03:202.5
Zinc ug/L ND 10.0 12/13/16 03:205.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1881716LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 506500 101 80-120
Arsenic ug/L 491500 98 80-120
Barium ug/L 482500 96 80-120
Beryllium ug/L 498500 100 80-120
Cadmium ug/L 499500 100 80-120
Chromium ug/L 508500 102 80-120
Cobalt ug/L 510500 102 80-120
Copper ug/L 507500 101 80-120
Lead ug/L 477500 95 80-120
Nickel ug/L 474500 95 80-120
Selenium ug/L 503500 101 80-120
Silver ug/L 237250 95 80-120
Thallium ug/L 439500 88 80-120
Vanadium ug/L 487500 97 80-120
Zinc ug/L 513500 103 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/10/2017 11:48 AM
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9800 Kincey Ave. Suite 100
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Page 23 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325731
Surry MSWLF SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1881717MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92321678002
1881718
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 97 75-12597 0 25500ND483483
Arsenic ug/L 500 94 75-12593 1 25500ND468464
Barium ug/L 500 94 75-12598 3 2550030.4J 502 519
Beryllium ug/L 500 97 75-12597 0 25500ND488487
Cadmium ug/L 500 95 75-12596 1 25500ND478482
Chromium ug/L 500 100 75-12599 1 25500ND498494
Cobalt ug/L 500 97 75-12597 0 25500ND484486
Copper ug/L 500 98 75-12598 0 25500ND490493
Lead ug/L 500 92 75-12592 1 255003.4J 463 461
Nickel ug/L 500 92 75-12593 0 25500ND462463
Selenium ug/L 500 97 75-12597 1 25500ND487484
Silver ug/L 250 93 75-12593 0 25250ND232232
Thallium ug/L 500 85 75-12584 2 25500ND426419
Vanadium ug/L 500 95 75-12595 1 25500ND478475
Zinc ug/L 500 100 75-125100 1 25500ND504500
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/10/2017 11:48 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325731
Surry MSWLF SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
339748
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92321678001, 92321678002, 92321678003, 92321678004, 92321678005, 92321678006, 92321678007,
92321678008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1884227
Associated Lab Samples:92321678001, 92321678002, 92321678003, 92321678004, 92321678005, 92321678006, 92321678007,
92321678008
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 12/07/16 21:260.33
1,1,1-Trichloroethane ug/L ND 1.0 12/07/16 21:260.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 12/07/16 21:260.40
1,1,2-Trichloroethane ug/L ND 1.0 12/07/16 21:260.29
1,1-Dichloroethane ug/L ND 5.0 12/07/16 21:260.32
1,1-Dichloroethene ug/L ND 5.0 12/07/16 21:260.56
1,2,3-Trichloropropane ug/L ND 1.0 12/07/16 21:260.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 12/07/16 21:262.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 12/07/16 21:260.27
1,2-Dichlorobenzene ug/L ND 5.0 12/07/16 21:260.30
1,2-Dichloroethane ug/L ND 1.0 12/07/16 21:260.24
1,2-Dichloropropane ug/L ND 1.0 12/07/16 21:260.27
1,4-Dichlorobenzene ug/L ND 1.0 12/07/16 21:260.33
2-Butanone (MEK)ug/L ND 100 12/07/16 21:260.96
2-Hexanone ug/L ND 50.0 12/07/16 21:260.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 12/07/16 21:260.33
Acetone ug/L ND 100 12/07/16 21:2610.0
Acrylonitrile ug/L ND 200 12/07/16 21:261.9
Benzene ug/L ND 1.0 12/07/16 21:260.25
Bromochloromethane ug/L ND 3.0 12/07/16 21:260.17
Bromodichloromethane ug/L ND 1.0 12/07/16 21:260.18
Bromoform ug/L ND 3.0 12/07/16 21:260.26
Bromomethane ug/L ND 10.0 12/07/16 21:260.29
Carbon disulfide ug/L ND 100 12/07/16 21:261.2
Carbon tetrachloride ug/L ND 1.0 12/07/16 21:260.25
Chlorobenzene ug/L ND 3.0 12/07/16 21:260.23
Chloroethane ug/L ND 10.0 12/07/16 21:260.54
Chloroform ug/L ND 5.0 12/07/16 21:260.14
Chloromethane ug/L ND 1.0 12/07/16 21:260.11
cis-1,2-Dichloroethene ug/L ND 5.0 12/07/16 21:260.19
cis-1,3-Dichloropropene ug/L ND 1.0 12/07/16 21:260.13
Dibromochloromethane ug/L ND 3.0 12/07/16 21:260.21
Dibromomethane ug/L ND 10.0 12/07/16 21:260.21
Ethylbenzene ug/L ND 1.0 12/07/16 21:260.30
Iodomethane ug/L ND 10.0 12/07/16 21:260.32
Methylene Chloride ug/L ND 1.0 12/07/16 21:260.97
Styrene ug/L ND 1.0 12/07/16 21:260.26
Tetrachloroethene ug/L ND 1.0 12/07/16 21:260.46
Toluene ug/L ND 1.0 12/07/16 21:260.26
trans-1,2-Dichloroethene ug/L ND 5.0 12/07/16 21:260.49
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/10/2017 11:48 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325731
Surry MSWLF SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1884227
Associated Lab Samples:92321678001, 92321678002, 92321678003, 92321678004, 92321678005, 92321678006, 92321678007,
92321678008
Matrix:Water
AnalyzedMDL
trans-1,3-Dichloropropene ug/L ND 1.0 12/07/16 21:260.26
trans-1,4-Dichloro-2-butene ug/L ND 100 12/07/16 21:261.0
Trichloroethene ug/L ND 1.0 12/07/16 21:260.47
Trichlorofluoromethane ug/L ND 1.0 12/07/16 21:260.20
Vinyl acetate ug/L ND 50.0 12/07/16 21:260.35
Vinyl chloride ug/L ND 1.0 12/07/16 21:260.62
Xylene (Total)ug/L ND 5.0 12/07/16 21:260.66
1,2-Dichloroethane-d4 (S)%100 70-130 12/07/16 21:26
4-Bromofluorobenzene (S)%95 70-130 12/07/16 21:26
Toluene-d8 (S)%98 70-130 12/07/16 21:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1884228LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 46.550 93 80-125
1,1,1-Trichloroethane ug/L 46.450 93 71-129
1,1,2,2-Tetrachloroethane ug/L 48.750 97 79-124
1,1,2-Trichloroethane ug/L 46.150 92 85-125
1,1-Dichloroethane ug/L 48.950 98 73-126
1,1-Dichloroethene ug/L 50.050 100 66-135
1,2,3-Trichloropropane ug/L 47.650 95 75-130
1,2-Dibromo-3-chloropropane ug/L 50.250 100 71-133
1,2-Dibromoethane (EDB)ug/L 48.850 98 83-124
1,2-Dichlorobenzene ug/L 49.650 99 80-133
1,2-Dichloroethane ug/L 43.850 88 67-128
1,2-Dichloropropane ug/L 46.450 93 75-132
1,4-Dichlorobenzene ug/L 47.650 95 78-130
2-Butanone (MEK)ug/L 108100 108 61-144
2-Hexanone ug/L 108100 108 68-143
4-Methyl-2-pentanone (MIBK)ug/L 100100 100 72-135
Acetone ug/L 113100 113 48-146
Acrylonitrile ug/L 268250 107 40-160
Benzene ug/L 49.250 98 80-125
Bromochloromethane ug/L 48.550 97 71-125
Bromodichloromethane ug/L 47.650 95 78-124
Bromoform ug/L 44.850 90 71-128
Bromomethane ug/L 41.650 83 40-160
Carbon disulfide ug/L 54.1J50 108 50-160
Carbon tetrachloride ug/L 46.850 94 69-131
Chlorobenzene ug/L 46.850 94 81-122
Chloroethane ug/L 46.550 93 39-148
Chloroform ug/L 47.550 95 73-127
Chloromethane ug/L 49.450 99 44-146
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/10/2017 11:48 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325731
Surry MSWLF SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1884228LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 48.250 96 74-124
cis-1,3-Dichloropropene ug/L 46.450 93 72-132
Dibromochloromethane ug/L 48.750 97 78-125
Dibromomethane ug/L 45.450 91 82-120
Ethylbenzene ug/L 48.450 97 79-121
Iodomethane ug/L 91.7100 92 39-154
Methylene Chloride ug/L 49.250 98 64-133
Styrene ug/L 48.250 96 84-126
Tetrachloroethene ug/L 42.550 85 78-122
Toluene ug/L 47.250 94 80-121
trans-1,2-Dichloroethene ug/L 49.650 99 71-127
trans-1,3-Dichloropropene ug/L 46.350 93 69-141
trans-1,4-Dichloro-2-butene ug/L 57.6J50 115 40-160
Trichloroethene ug/L 45.450 91 78-122
Trichlorofluoromethane ug/L 52.050 104 53-137
Vinyl acetate ug/L 106100 106 40-160
Vinyl chloride ug/L 42.650 85 58-137
Xylene (Total)ug/L 143150 96 81-126
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1884229MATRIX SPIKE SAMPLE:
MSSpike
Result
92321673001
1,1,1,2-Tetrachloroethane ug/L 19.920 100 70-130ND
1,1,1-Trichloroethane ug/L 20.620 103 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.020 100 70-130ND
1,1,2-Trichloroethane ug/L 19.620 98 70-130ND
1,1-Dichloroethane ug/L 21.120 106 70-130ND
1,1-Dichloroethene ug/L 23.120 115 70-166ND
1,2,3-Trichloropropane ug/L 18.820 94 70-130ND
1,2-Dibromo-3-chloropropane ug/L 20.220 101 70-130ND
1,2-Dibromoethane (EDB)ug/L 20.420 102 70-130ND
1,2-Dichlorobenzene ug/L 20.520 102 70-130ND
1,2-Dichloroethane ug/L 19.720 98 70-130ND
1,2-Dichloropropane ug/L 19.420 97 70-130ND
1,4-Dichlorobenzene ug/L 19.820 99 70-130ND
2-Butanone (MEK)ug/L 42.5J40 106 70-130ND
2-Hexanone ug/L 42.4J40 106 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 40.4J40 101 70-130ND
Acetone ug/L 42.4J40 89 70-130ND
Acrylonitrile ug/L 111J100 111 70-130ND
Benzene ug/L 21.520 108 70-148ND
Bromochloromethane ug/L 21.320 107 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/10/2017 11:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325731
Surry MSWLF SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1884229MATRIX SPIKE SAMPLE:
MSSpike
Result
92321673001
Bromodichloromethane ug/L 20.320 102 70-130ND
Bromoform ug/L 18.120 90 70-130ND
Bromomethane ug/L 17.620 88 70-130ND
Carbon disulfide ug/L 25.2J20 123 70-130ND
Carbon tetrachloride ug/L 20.420 102 70-130ND
Chlorobenzene ug/L 20.320 101 70-146ND
Chloroethane ug/L 21.020 105 70-130ND
Chloroform ug/L 20.520 102 70-130ND
Chloromethane ug/L 23.020 112 70-1300.66J
cis-1,2-Dichloroethene ug/L 21.320 107 70-130ND
cis-1,3-Dichloropropene ug/L 18.420 92 70-130ND
Dibromochloromethane ug/L 20.420 102 70-130ND
Dibromomethane ug/L 19.220 96 70-130ND
Ethylbenzene ug/L 20.820 104 70-130ND
Iodomethane ug/L 37.840 95 70-130ND
Methylene Chloride ug/L 20.420 102 70-130ND
Styrene ug/L 20.220 101 70-130ND
Tetrachloroethene ug/L 18.420 92 70-130ND
Toluene ug/L 20.720 103 70-155ND
trans-1,2-Dichloroethene ug/L 22.520 113 70-130ND
trans-1,3-Dichloropropene ug/L 18.520 93 70-130ND
trans-1,4-Dichloro-2-butene ug/L 17.3J20 86 70-130ND
Trichloroethene ug/L 20.120 101 69-151ND
Trichlorofluoromethane ug/L 23.620 118 70-130ND
Vinyl acetate ug/L 35.7J40 89 70-130ND
Vinyl chloride ug/L 19.220 96 70-130ND
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%95 70-130
Toluene-d8 (S)%96 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92321673002
1884230SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 5.4 4 305.2
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/10/2017 11:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 34
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325731
Surry MSWLF SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92321673002
1884230SAMPLE DUPLICATE:
1,4-Dichlorobenzene ug/L 0.70J 300.71J
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 3016.3J
Acrylonitrile ug/L ND 30ND
Benzene ug/L 0.71J 300.74J
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L 0.73J 30ND
Carbon disulfide ug/L 4.3J 301.6J
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L 1.7J 24 301.4
Chloroform ug/L ND 30ND
Chloromethane ug/L 9.6 27 3012.6
cis-1,2-Dichloroethene ug/L 2.6J 1 302.6
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L 0.95J 300.90J
Trichlorofluoromethane ug/L 1.5 11 301.3
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%89 12100
4-Bromofluorobenzene (S)%99 495
Toluene-d8 (S)%107 898
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/10/2017 11:48 AM
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Page 29 of 34
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92325731
Surry MSWLF SWs
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/10/2017 11:48 AM
Pace Analytical Services, LLC
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[phone]
Page 30 of 34
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92325731
Surry MSWLF SWs
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92321678001 339257 339658SW-1 EPA 3010A EPA 6010
92321678002 339341 339662SW-2 EPA 3010A EPA 6010
92321678003 339341 339662SW-3 EPA 3010A EPA 6010
92321678004 339341 339662SW-4 EPA 3010A EPA 6010
92321678005 339341 339662SWN-1 EPA 3010A EPA 6010
92321678006 339341 339662SWN-2 EPA 3010A EPA 6010
92321678001 339748SW-1 EPA 8260
92321678002 339748SW-2 EPA 8260
92321678003 339748SW-3 EPA 8260
92321678004 339748SW-4 EPA 8260
92321678005 339748SWN-1 EPA 8260
92321678006 339748SWN-2 EPA 8260
92321678007 339748SW-A EPA 8260
92321678008 339748SW-B EPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/10/2017 11:48 AM
Pace Analytical Services, LLC
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[phone]
Page 31 of 34
Page 32 of 34
Page 33 of 34
Page 34 of 34
Appendix B
Field Sampling Parameter Data Sheet(s)