8602_SurryCountyMtAiry_MSWLF_GWMR_20171031

Surry County Closed C&D and Closed MSWLF, Mt. Airy
Mt. Airy, North Carolina
May 2017
Permit Number: 86-02
Semi-Annual Water Quality Monitoring Report
Prepared for
Municipal Engineering Services Company, P.A.Garner and Boone, North Carolina
MESCO Project Number: G17024.0
P.O. Box 97
Garner, NC 27529
License No. C-0281

with Corrective Action Update
TABLE OF CONTENTS
SECTION
Introduction Page 1
Background Page 2
Sampling Procedures Page 2
Field Parameter Data Page 2
Laboratory Results Page 3
Quality Control Samples Page 3
Groundwater Samples Page 4
Surface Water Samples Page 5
Corrective Action Update Page 5
MNA Analysis (AOCs Northern, Southern and MW-11) Page 5
Enhanced Bioremediation via Substrate Injection (AOC Southern and Northern) Page 5
MW-11 AOC Investigations Page 6
Groundwater and Surface Water Characterization Page 7
Findings Page 7
Closing Page 8
SHEETS
Topographic Map with Site Location Sheet 1
Single Event Potentiometric Map of Uppermost Aquifer Sheet 2
FIGURES
Total Cumulative VOC Concentrations Pre/Post Injection Comparison Figure 1
Total Cumulative VOC Concentrations Time Series Graphs/Table Figure 2

TABLES
Groundwater Monitoring Well Construction Table Table 1
Field Observations of Monitoring Locations Table 2
Field Parameter Data Summary Table 3
Sampling and Analysis Summary Table 4
Groundwater and QC Sample Detections Table 5
Surface Water Sample Detections Table 6
MNA Parameter Data Summary Table 7
Hydrologic Properties at Monitoring Well Locations Table 8
APPENDICIES
Laboratory Analysis Report and Chains of Custody Appendix A
Field Sampling Parameter Data Sheet(s) Appendix B
October 31, 2017

Ms. Jaclynne Drummond
Solid Waste Section (SWS)
2090 US 70 Highway
Swannanoa, NC 28778
Re: Semi-Annual Water Quality Monitoring Report with Corrective Action Update
Surry County Closed C&D and Closed MSWLF, Mount Airy
Permit No. 86-02
MESCO Project No. G17025.0
Event Date(s): May 31-June 1, 2017
Dear Ms. Drummond:
Introduction
On behalf of Surry County, Municipal Engineering Services Company, P.A. (MESCO) is pleased to present this Semi-
Annual Water Quality Report with Corrective Action Update for the spring 2017 event performed at the Surry County
closed construction and demolition (C&D) and closed municipal solid waste landfill (MSWLF)-Mount Airy.
NCDENR Solid Waste Rules 15A NCAC 13B.1632 requires that Surry County provide this report to the NC Solid
Waste Section (SWS) on a semi-annual basis. This report documents the quality of the ground and surface waters
during this monitoring event performed on May 31-June 1, 2017. Laboratory analytical results, which included
targeting Appendix II constituents, indicate volatile organic compounds (VOCs) in concentrations in excess of SWSL
and 2L Standards continue to persist in samples collected from three wells that monitor the uppermost aquifer. The
surface water samples collected from the local discharge feature remain unimpacted. Corrective action to remediate
VOCs in groundwater is ongoing within all three areas of concern (AOC) as defined in the Corrective Action Plan
(CAP) and improvement has been observed with updated information presented herein.

Background
The Surry County closed C&D and MSWLF, permit #86-02, is located at 237 Landfill Road in Mt. Airy North
Carolina. The site location topographic map is depicted in the attached Sheet 1. Prior to becoming a C&D landfill
the site operated as a MSW unlined sanitary landfill that consisted of two units. The northern unit was closed prior to
October 1991. The southern unit is comprised of two contiguous portions. The first part stopped receiving waste
prior to October 1991 and the second part stopped receiving waste prior to January 1, 1999. Both portions of the
southern unit were properly closed with a low permeability cohesive cap per the Transition Plan. The top portion of
the southern unit served as an exclusive C&D landfill until prior to June 1, 2008 at which time it was properly closed
with another cohesive cap in accordance with the Closure Plan. For continuity, both the northern and the southern
units are monitored and reported together.
Water quality at this facility has been monitored at least semi-annually since 1989 with historical data available since
1994. This event was performed in accordance with the NC SWS rules/regulations as promulgated in 15A NCAC
13B and as a condition of the post-closure portion of the permit to operate and memorandums this report contains
sampling procedures, field and laboratory results, groundwater and surface water characterization, and findings. This
report also contains a table of detections compared to Standards, field data results table, groundwater flow
directions/rates table, field observations of the monitoring network table, a potentiometric map of the uppermost
aquifer, histograms of historical detections, statistical trend analysis, laboratory analytical reports with chains-of-
custody (C-O-C) and quality assurance/quality control data.
Sampling Procedures
The water quality monitoring program, current as of this event date, includes sampling locations and parameters as
outlined in the Water Quality Sampling and Analysis Plan (SAP) (DIN:18936) dated April 30, 2013 and approved by
the SWS (DIN: 18938) on May 10, 2013. Monitoring locations are shown on the enclosed potentiometric map
(Sheet 2). MESCO personnel collected water samples from 20 downgradient groundwater monitoring wells (MW-
3R, MW-4, MW-6 through MW-11, MW-12S, MW-12D, MW-13 through MW-23), one background well (MW-1),
four surface water locations (SW-1, SW-2, SW-3 and SW-4), and the water supply well (SCALEHOUSE) that serves
the facility. Data from two surface water points (SWN-1 and SWN-2) designated in the SAP for the adjacent Subtitle
D Lined MSWLF are presented because this local discharge feature is shared by both permits. Quality control
measures implemented during this event included the quantification of potential artifact contaminants via equipment
(EB), field (FB) and travel (TB) blanks. Samples were not analyzed from the six injection wells (IW-1), (IW-2/MW-
2), (IW-3/MW-3RS), (IW-4/MW-4), (IW-5/MW-5) and (IW-6/MW-8) since they are exempt due to the presence of
injectant residue which would yield unrepresentative water quality results.
2
A summary of the construction of the water monitoring wells is presented on Table 1. The function and integrity of
all monitoring locations were visually evaluated as documented on Table 2. The depth to water in each well was
electronically gaged prior to purging to quantify the static water level elevation. Low-flow pumping methodology or
bailing was utilized to adequately purge the wells to a minimum of three times the volume of standing water in the
well or until dry. Surface water samples were collected from Stoney Creek discharge feature at previously designated
locations. During well purging and surface water sample collection the required field parameters were recorded. The
samples were then placed into laboratory-prepared, pre-preserved containers via a new disposable polyethylene
bailer. Samples were collected, kept on ice, and transported to a NC-certified laboratory under proper C-O-C
protocols within the specified hold times for each analysis.
Field Parameter Data
Stabilized field parameters were recorded during purging which included depth to water, pH, dissolved oxygen (DO),
temperature, oxidation reduction potential (ORP), specific conductance and turbidity. The field parameter data
indicates the monitored groundwater is slightly acidic, reducing conditions, with relatively low specific conductance
which is generally consistent relative to each other and congruent with data historically reported. Field parameter
data recorded at the surface water locations were neutral in regard to pH and low specific conductance which is
consistent with uncontaminated water. A summary of the field parameter data is presented in Table 3 and the field
sampling data sheet is enclosed in Appendix B.
Laboratory Results
Pace Analytical Laboratory (PACE) of Huntersville and Asheville, NC performed the laboratory analysis of
groundwater and surface water samples for the total recoverable constituents listed in 40 CFR Appendix I and II.
Pace also analyzed samples collected from seven wells for monitored natural attenuation (MNA) parameters. A
sampling and analysis table summarizing the locations, constituents, and methods is presented on Table 4.
Laboratory results and C-O-Cs are contained in Appendix A.
Water samples were analyzed to the laboratory-established Method Detection Limits (MDL), which are at or below
the current Solid Waste Section Limit (SWSL). Table 5 summarizes constituents detected in groundwater and QC
samples that attain or were above the current SWSL, SWS adopted Groundwater Protection Standards (GWP), North
Carolina Groundwater Standards (2L) or the Maximum Contaminant Level (MCL) commonly referenced as the
Federal “Drinking Water Standard”. Table 6 lists the constituents detected in surface water and QC samples
compared to the SWSL, the North Carolina Surface Water Standards (2B) for a Class C water-body and the MCL.
Quality Control Samples
Acetone was detected in EB and FB and chloromethane was found in TB. Acetone was also detected in the majority
of ground and surface water samples in comparable levels which is inconsistent with previous events. The detections
of acetone are believed to be lab induced false positives. Since acetone levels were below regulatory Standards the
acetone detections are largely inconsequential. However, acetone concentrations were not included when calculating
the total cumulative VOCs which were used for statistical trend analysis.
3
Groundwater Samples
Six metals were detected above the NC 2L/GWP Standard in samples collected from 13 wells including the
background well (MW-1) as summarized in the following table.
Metals Detected Above 2L/GWP Standards in Groundwater
Cd Cr Co Pb Tl Va
SWSL 1 10 10 10 5.5 25
2L/GWP STD.2 10 1 15 0.28 0.3
MW-1 (BG Well)21
MW-6 51.6 0.3 j
MW-7 50.7
MW-9 166 0.33 j
MW-11 11.7
MW-13 11
MW-14 12.4 13.1 18 j
MW-15 2.7 j 3.1 j
MW-16 242
MW-19 4.1 j 8.2 j
MW-20 12.3 0.32 j
MW-21 4.8 j
MW-23 2.1
Concentrations in ug/L j = “j-qualified” since below the SWSL thus value is considered an estimate
Seven VOCs were detected above the NC 2L Standard in samples collected from five wells as summarized in the
following table.
VOCs Detected Above 2L Standards in Groundwater
1,2-DCA 1,2-DCB 1,2-DCE 1,2-DCA Acetone Benzene VC
SWSL 5 5 1 1 100 1 1
2L STD.6 20 0.4 6 6000 1 0.03
MW-9 2.4 18.7
MW-13 0.96 j
MW-15 9.7 0.58 j 1.6
MW-16 0.81 j 1.3
MW-21 0.49 j
Concentrations in ug/L. j = “j-qualified” since below the SWSL thus value is considered an estimate
4
The majority of the monitoring locations that were found to contain VOCs included a mixture of dissolved phase
aromatic hydrocarbons and chlorinated aliphatic hydrocarbons. The only constituent which originated from an
anthropogenic source in levels above the EPA established maximum contaminant levels (MCLs) primary “Drinking
Water Standards” was vinyl chloride in sample MW-9. A site map depicting the concentrations and estimated
horizontal extent of VOCs that exceeded the 2L Standard during this event is presented on Sheet 2.
The on-site water supply well (SCALEHOUSE) continues to lack detections in exceedance of current groundwater or
drinking water Standards.
Surface Water Samples
Contaminants were not detected in any of the surface water samples above any established NC 2B Surface Water
Standards.
Corrective Action Update
Groundwater remediation continues to be implemented per the approved Corrective Action Plan (CAP) at the three
designated areas of concern (AOC) (Northern, Southern and MW-11). A Corrective Action Evaluation Report
(CAER) (DIN: 19361) was submitted on May 1, 2013 which demonstrated that the plumes continue to decrease and
was approved by the the SWS on July 24, 2013 (DIN:19366). A historical summary of corrective actions performed
to date are briefly presented in the following sections.
MNA Analysis (AOCs Northern, Southern and MW-11)
Semi-annual MNA monitoring of a subset of 12 wells for the full suite of SWS recommended parameters was
initiated on May 18, 2010 and performed for four consecutive semi-annual events to establish a baseline. A revised
SAP prescribing 7 wells with various targeted MNA constituents was approved by the SWS and initiated during an
event performed in May 2013. MNA monitoring was performed during this event for the parameters and frequency
as listed in the current SAP. MNA parameters quantified during this event included alkalinity, sulfate, sulfide,
chloride, TOC, COD, ferrous iron, CO2, turbidity, DO and ORP. MNA parameters are presented on Table 7.
Enhanced Bioremediation via Substrate Injection (AOC Southern and Northern)
Per the SWS approved Corrective Action Plan enhanced bioremediation via substrate and tracer injection was
initiated in the Southern and Northern AOCs in accordance with requirements outlined in the Injection Well Permit
Application and Well Permit No. WI0400176 (5/6/11) in an effort to reduce low level aliphatic and aromatic
chlorinated hydrocarbons in groundwater to below the 2L Standards. An edible oil substate (EOS)-water emulsion
with sodium bromide tracer was injected into four wells (IW-1, IW-2, IW-3 and IW-5) on November 2-3, 2011.
Similar substrates were injected into monitoring wells MW-4/IW-4 and MW-8/IW-6 on October 24-25, 2012. Details
of the injection events are provided in the Injection Event Record dated November 4, 2011 and January 10, 2013.
5
As directed in the UIC Injection Well Permit renewed on April 15, 2013 semi-annual post-injection water quality
monitoring of wells located downgradient of viable injection points (MW-3R, MW-7, MW-9, MW-12S, MW-13,
MW-14, MW-15, MW-16, MW-17, MW-18, MW-19, MW-20, MW-21, MW-22, MW-23) and upgradient background
well MW-1 was also performed in conjunction with this semi-annual event. Total VOC concentrations reported
during this event were lower at all locations when compared to the respective moving averages of the five events
preceding injection in the selected wells downgradient of the injection points (Figure 1).
Evaluation of injection wells (IW-1, IW-2, IW-3, IW-4, IW-5, IW-6) continues to indicate that a considerable amount
of white highly turbid (>1,000 NTU) viscous residual organic substrate and its byproducts remain in each of these
wells rendering them unsuitable for representative water quality analysis. The viscosity of the water in the injection
wells during this May 2014 event precludes sample collection as either a bailer will not descend or the check valve
fails. IW-1 was verified to not be a viable injection well as less than 3 gallons of substrate was able to be injected
into the low permeable fractured bedrock and injectant levels have remained above static conditions for over a year.
For all intents and purposes IW-1 injection did not occur nor will be possible in the future.
MW-11 AOC Investigations
The CAP designated MW-11 as an area of concern due to detections of VOCs detected in exceedance of 2L
Standards. MW-11 is located within the compliance boundary near the northern property line which is hydraulically
upgradient of the closed northern landfill. The northern landfill closed before October 1991 which was before
adoption of NC Section .1600 rules that address assessment and corrective action. VOCs have historically been
detected in excess of the 2L Standard at MW-11 which include a mixture of aromatics (fuel hydrocarbons) and
chlorinated hydocarbons (solvents). Over the past 4 years (8 semi-annual events) the only constituent detected in
excess of 2L Standard and SWSL was 1,2-dichloropropane. During this event levels of 1,2-dichloropropane fell
remain above the 2L Standard but fell below the SWSL thus “j-qualified”. The CAP prescribed MNA and enhanced
biodegredation to remediate MW-11 AOC. MNA has been performed continuously semiannually at MW-11 the past
6 years. Enhanced biodegredation has not been initiated at MW-11 AOC since hydrogeologic conditions relative to
the source and property boundaries preclude it as an effective technique. MW-11 is positioned hydraulically
upgradient of the source and is within the review boundary. A well was attempted to be installed at the property line
110 feet north of MW-11 on January 26, 2015 to delineate the extent of contamination. The potentiometric head at
B-11R was expected to be at 25 feet (1132 ft amsl) but the boring encountered very competent rock at 9 ft and
remained dry to 55 ft. (1102 ft amsl) for over 48 hours so was abandoned.
6
Groundwater and Surface Water Characterization
A potentiometric map constructed from water elevations taken from the uppermost aquifer which consists of both
saprolite and the hydraulically connected upper portion of the fractured bedrock system is enclosed as Sheet 2.
Groundwater flow directions and velocity rates were calculated through modified Darcy's equation as shown on Table
8. Consistent with previous events the groundwater apparently flows in a general southeasterly direction towards the
tributaries of the Ararat River. The calculated average linear velocity of groundwater indicates an approximate
average of 873 ft/yr in the wells screened in regolith and 297 ft/yr in the wells screened in the bedrock. The
consistent disparity in flow rates between wells is indicative of heterogeneous geologic conditions and/or a product of
the limitations of the linear velocity equation when applied to anisotropic conditions which are characteristic of the
geology of the Piedmont. Streams located within the facility boundaries were observed to be of high volume and
flow with low turbidity in response to recent rainfall.
Findings
The inorganic detections are believed to be a product of erosion of natural deposits and not an anthropogenic source.
An ASD which provides technical site specific facts and site specific analytical data including evaluations of interwell
(background), intrawell (baseline), metals in leachate, dissolved compared to total metals and a discussion that
substantiating evidence that the metals are not anthropogenic was not approved by the SWS. The SWS requested that
the ASD be amended to include additional information. More time will be needed to collect additional field data
prior to amending the ASD.
The on-site supply well and the surface water points remain unimpacted as indicated by the lack of detections in
excess of the applicable Standards. The on-site supply well is not considered potable thus bottled water is provided
for consumption and “Non-Potable Water” warning signs were observed.
One or more Appendix I VOC(s) continue to be detected in quantifiable levels above the 2L Standard in samples
collected from the uppermost aquifer at three locations (MW-9, MW-17 and MW-20). All VOC concentrations
remain within their own respective historically identified range with the exception of vinyl chloride in sample MW-9.
Qualitative evaluation of VOC concentrations indicate a decreasing trend over time and distance from the landfill.
Total cumulative VOC concentrations during this event decreased at all locations compared to their respective five
event averages preceding corrective action except for MW-9, MW-19 and MW-20 (Figure 2). Results of statistical
temporal trend analysis, using Sen's Slope Estimator at a 95% confidence level, compared to when corrective action
began 6.5 years ago indicate that none of the individual well's cumulative VOC concentrations, except MW-9, have
increased. The Southern AOC and cumulative site-wide VOC levels continue to exhibit a decreasing trend.
The area of the uppermost aquifer beyond the compliance boundary containing quantifiable concentrations of VOCs
in exceedance of the 2L Standard during this event is estimated at 0.0 acres in the Northern AOC, 0.0 acres in the
MW-11 AOC and 5.3 acres in the Southern AOC for a total facility wide area of 5.3 acres (Sheet 2). This is an
estimated 34% retraction of facility-wide plume area (from 8 acres to 5.3 acres) compared to when corrective action
was initiated 6.5 years ago.
7
Figures
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1
Figure 1
October 22, 2009 – June 1, 2017
Well ID
INJECTION WELL (IW-1) UNSUCCESSFUL INJECTION SO DOWNGRADIENT WELLS NOT SHOWN
INJECTION WELL (IW-2) MONITORED DOWNGRADIENT BY MW-12S, MW-13 & MW-18
MW-12S 0.00 0.00 0.00 0.00 5.40 1.08 0.00 -1.08 -100
MW-13 61.00 50.60 74.20 87.30 72.50 69.12 39.24 -29.88 -43
MW-18 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0
INJECTION WELL (IW-3) MONITORED DOWNGRADIENT BY MW-3R & MW-16
MW-3R 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0
MW-16 137.90 113.60 135.70 121.20 116.30 124.94 21.21 -103.73 -83
INJECTION WELL (IW-4) MONITORED DOWNGRADIENT BY MW-14, MW-21 & MW-23
MW-14 15.20 15.60 15.60 8.20 17.00 14.32 7.46 -6.86 -48
MW-21 52.10 50.70 51.38 39.10 32.41 45.14 24.14 -21.00 -47
MW-23 4.30 0.00 0.00 0.00 0.00 0.86 0.82 -0.04 -5
INJECTION WELL (IW-5) MONITORED DOWNGRADIENT BY MW-15 & MW-19
MW-15 96.13 63.89 55.00 78.10 64.06 71.44 53.93 -17.51 -25
MW-19 0.00 0.00 0.00 0.00 0.00 0.00 1.01 1.01 0
INJECTION WELL (IW-6) NOT SHOWN AS NO WELLS DOWNGRADIENT WITHIN ZONE OF INFLUENCE
Total Cumulative VOC Concentrations Pre/Post Injection Comparison
Oct
2009
(ug/L)
May
2010
(ug/L)
Oct
2010
(ug/L)
May
2011
(ug/L)
Oct
2011
(ug/L)
Average of
first Five
Corrective
Action
Events
(ug/L)
May
2017
(ug/L)
Difference
(ug/L)
Difference
(%)
Statistical Trend*
Between Oct
2009-May 2017
No Trend
Downward
No Trend
No Trend
Downward
Downward
Downward
No Trend
Downward
No Trend
* = Statistical Trend analysis via Sen's Slope Estimator at a 95% confidence level11/3/2011 (INJECTED)11/3/2011 (INJECTED)11/3/2011 (INJECTED)10/24/2013 (INJECTED)
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1
Figure 2
Total Cumulative VOC Concentrations Time Series Graphs/Table
October 22, 2009 – May 31, 2017
AOC Well ID Difference Difference
(%)Oct 2009 – May 2017
Background MW-1 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend
Southern
IW-2 (MW-2)105.25 207.00 207.93 159.90 79.10 151.84 NS NS No Trend
IW-3 (MW-3RS)202.90 127.50 127.50 144.00 127.60 145.90 NS NS No Trend
MW-3R 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend
IW-4 (MW-4)27.00 24.20 24.20 27.60 23.50 25.30 NS NS No Trend
IW-5 (MW-5)35.00 46.50 46.50 47.40 34.80 42.04 NS NS No Trend
MW-12S 0.00 0.00 0.00 0.00 5.40 1.08 0.00 -1.08 -100 No Trend
MW-12D 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend
MW-13 61.00 50.60 74.20 87.30 72.50 69.12 39.24 -29.88 -43 Downward
MW-14 15.20 15.60 15.60 8.20 17.00 14.32 7.46 -6.86 -48 Downward
MW-15 96.13 55.00 55.00 78.10 64.06 69.66 53.93 -15.73 -23 Downward
MW-16 137.90 113.60 135.70 121.20 116.30 124.94 21.21 -103.73 -83 Downward
MW-17 20.34 8.40 8.85 0.00 5.77 8.67 0.00 -8.67 -100 No Trend
MW-18 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend
MW-19 0.00 0.00 0.00 0.00 0.00 0.00 1.01 1.01 0 No Trend
MW-21 52.10 50.70 51.38 39.10 32.41 45.14 24.14 -21.00 -47 Downward
MW-22 28.90 23.80 23.80 11.66 5.20 18.67 3.09 -15.58 -83 Downward
MW-23 4.30 0.00 0.00 0.00 0.00 0.86 0.82 -0.04 -5 No Trend
Combined Total 786.02 722.90 770.66 724.46 583.64 717.54 410.50 -307.04 -43 Downward
Northern
MW-6 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 No Trend
MW-7 7.40 9.40 11.20 9.70 8.80 9.30 0.00 -9.30 -100 Downward
IW-6 (MW-8)22.00 23.90 16.00 12.30 12.60 17.36 NS NS No Trend
MW-9 23.50 20.40 23.20 25.80 22.90 23.16 54.50 31.34 135 Upward
MW-20 0.00 0.00 0.00 0.00 0.00 0.00 0.64 0.64 0 No Trend
Combined Total 52.90 53.70 50.40 47.80 44.30 49.82 67.74 17.92 36 No Trend
MW-11 MW-11 10.10 6.00 6.00 5.44 23.20 10.15 6.24 -3.91 -39 No Trend
SITEWIDE Combined Total 849.02 782.60 827.06 777.70 651.14 777.50 484.48 -293.02 -38 Downward
Oct
2009
May
2010
Oct
2010
May
2011
Oct
2011
Average of
first Five
Corrective
Action
Events May 2017 A Statistical Trend*
(ug/L)(ug/L)(ug/L)(ug/L)(ug/L)(ug/L)(ug/L)(ug/L)
79.10 NS
127.60 NS
18.10 NS
34.80 NS
12.60 NS
NS = Not sampled this event so most recent concentration shown and used in calculations
* = Statistical trend analysis via Sen's Slope Estimator at a 95% Confidence Level
A = Arsenic concentrations in May 2017 not included in calculations since likely false positives
Sheets
Topographic Map with Site Location
SHEET 1
Surry County Landfill, Mt. Airy
237 Landfill Road
Mount Airy, NC 28621
Lat: 36-26-30.065
Long:-80-34-15.314
Northing:983356.18
Easting:1537885.48
Closed Unlined C&D Landfill
Closed Unlined Sanitary Landfill
Active Lined MSW Landfill
Surry Co Property Line
Table
Table 1
Groundwater Monitoring Well Construction Table
May 30-31, 2017
Well
Diameter
Total Well
Depth
Top of
Screen
Depth
Screen
Length
Top of
Casing
Elevation
Ground
Elevation
Groundwater
Elevation
Depth to
Water
(inches)(ft bgs)(ft bgs)(ft)(ft amsl)(ft amsl)(ft amsl)(ft btoc)
MW-1 11/28/89 2 40 30 10 Clay 1134.35 1133.15 1113.41 20.94 36.439211 -80.568133
IW-2 (was MW-2)11/28/89 2 70 60 10 Clay 1068.86 1068.36 1027.91 40.95 36.435833 -80.568894
MW-3R 9/27/94 2 101 86 15 Rock 1017.50 1015.00 978.22 39.28 36.434725 -80.571989
IW-3 (was MW-3RS)5/17/01 2 52 37 15 Rock 1020.57 1018.24 990.47 30.10 36.434656 -80.571858
IW-4 (was MW-4)8/30/94 2 55.4 40.4 15 Rock 1026.26 1025.06 990.94 35.32 36.434686 -80.569200
IW-5 (was MW-5)8/27/94 2 63 48 15 Rock 1080.18 1077.78 <1039.50 >40.68 36.434614 -80.570436
MW-6 9/7/94 2 29.7 14.7 15 Rock 1067.67 1065.61 1046.31 21.36 36.437431 -80.571067
MW-7 8/23/94 2 23 8 15 Rock 1073.50 1071.50 1062.12 11.38 36.438439 -80.570722
IW-6 (was MW-8)8/16/94 2 54 39 15 Rock 1088.45 1086.45 1046.15 42.30 36.439278 -80.570381
MW-9 8/22/94 2 43.8 28.8 15 Rock 1094.07 1092.07 1061.26 32.81 36.439289 -80.571508
MW-11 8/15/94 2 40 25 15 Rock 1151.80 1150.40 1131.30 20.50 36.441589 -80.569558
MW-12S 5/31/01 2 51 11 40 Rock 1025.80 1023.25 1013.01 12.79 36.435942 -80.567972
MW-12D 5/30/01 2 100 90 10 Rock 1027.05 1023.75 1027.05 0.00 36.435964 -80.567994
MW-13 5/30/06 2 35.78 20.78 15 Saprolite 1008.48 1005.75 983.38 25.10 36.435036 -80.568183
MW-14 5/30/06 2 48.03 33.03 15 Rock 1018.80 1016.11 983.95 34.85 36.434267 -80.569239
MW-15 6/22/06 2 57 42 15 Rock 1075.96 1073.23 1023.54 52.42 36.433797 -80.570467
MW-16 6/21/06 2 36.3 21.3 15 Rock 999.54 996.67 975.32 24.22 36.434536 -80.572117
MW-17 6/1/07 2 15.32 5.32 10 Rock 965.43 962.26 957.88 7.55 36.433558 -80.572517
MW-18 6/1/07 2 18.15 8.15 10 Saprolite 983.00 980.00 974.60 8.40 36.435453 -80.567050
MW-19 6/1/07 2 17.1 7.1 10 PWR 946.27 942.97 937.26 9.01 36.432231 -80.570556
MW-20 6/1/07 2 25.64 10.64 15 Rock 1082.19 1079.12 1063.08 19.11 36.439025 -80.571650
MW-21 6/1/07 2 15.41 5.41 10 Saprolite/PWR 965.36 962.22 959.91 5.45 36.434214 -80.568717
MW-22 6/1/07 2 16.04 6.04 10 Saprolite 953.40 950.23 948.69 4.71 36.432928 -80.571678
MW-23 6/1/07 2 17.1 7.1 10 Sandy Silt 955.31 952.09 948.46 6.85 36.432828 -80.569156
NOTE:
bgs = below ground surface
amsl= above mean sea level
btoc = below top of casing (PVC well casing)
Monitoring Well Date
Installed
Geology of
Screened
Interval
Latitude Longitude
Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1
Table 2
Field Observations of Monitoring Locations
May 31 - June 1, 2017
Location
Viable
Monitoring
Location
Lack of Any
Evidence of
Tampering
Locked on
Arrival &
Departure
Hinge/Hasp
Operational
Tagged
or
Labeled
Concrete
Surface Pad
Appears
Effective
Comments
MW-1 Yes Yes Yes Yes Yes Yes Pad cracked
IW-1 No Yes Yes Yes Yes Yes Fouled since injection 11/2/11.
IW-2 (was MW-2)No Yes Yes Yes Yes Yes Fouled since injection 11/2/11. No pad visible
MW-3R Yes Yes Yes Yes Yes Yes No pad
IW-3 (was MW-3RS)No Yes Yes Yes Yes Yes Fouled since injection 11/2/11.
IW-4 (was MW-4)No Yes Yes Yes Yes Yes Fouled since injection 10/24/12.
IW-5 (was MW-5)No Yes Yes Yes Yes Yes Fouled since injection 11/2/11. Bailer would not descend
MW-6 Yes Yes Yes Yes Yes Yes No pad, red purge water
MW-7 Yes Yes Yes Yes Yes Yes No pad
IW-6 (was MW-8)No Yes Yes Yes Yes Yes Fouled since injection 10/24/12. No pad. Lock replaced
MW-9 Yes Yes Yes Yes Yes Yes
MW-11 Yes Yes Yes Yes Yes Yes No pad
MW-12S Yes Yes Yes Yes Yes Yes
MW-12D Yes Yes Yes Yes Yes Yes Flowing artesian
MW-13 Yes Yes Yes Yes Yes Yes Can hear water cascade in well
MW-14 Yes Yes Yes Yes Yes Yes
MW-15 Yes Yes Yes Yes Yes Yes
MW-16 Yes Yes Yes Yes Yes Yes Red purge water
MW-17 Yes Yes Yes Yes Yes Yes
MW-18 Yes Yes Yes Yes Yes Yes
MW-19 Yes Yes Yes Yes Yes Yes
MW-20 Yes Yes Yes Yes Yes Yes
MW-21 Yes Yes Yes Yes Yes Yes
MW-22 Yes Yes Yes Yes Yes Yes
MW-23 Yes Yes Yes Yes Yes Yes
SW-1 Yes -----High gage height & flow
SW-2 Yes -----High gage height & flow
SW-3 Yes -----High gage height & flow
SW-4 Yes -----High gage height & flow
SWN-1 Yes -----High gage height & flow
SWN-2 Yes -----High gage height & flow
SCALEHOUSE Yes -----Sample from spigot next to well which is typical
Any unusual field conditions, observations, or events:
Visual markers (10 ft PVC pipes) remain secured to each monitoring well case
Rain several evenings during event. Therfore surface waters were higher than normal
Injection wells (IW-1, IW-2, IW-3, IW-4, IW-5 and IW-6) exempt from laboratory analysis as SWS approved on May 10, 2013 (DIN:18938)
Stormwater control improvements performed since May 2012 event.
Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1
Table 3
Field Parameter Data Summary
May 31 - June 1, 2017
Parameter
Depth to
Water
Water
Elevation
TOC
Elevation Temp.ORP DO pH
Specific
Conductance TDS Turbidity
Units ft (btoc)ft (amsl)ft (amsl) C mV mg/L SU umhos/cm mg/L Visual or NTU
MW-1 20.94 1108.20 1134.35 15.3 191 2.6 6.3 210 NR 6.7
IW-2 40.95 1028.65 1068.86 NR NR NR NR NR NR >1000
MW-3R 39.28 975.39 1017.50 15.3 NR NR 7.0 317 NR Clear
IW-3 30.10 975.39 1020.57 NR NR NR NR NR NR >1000
IW-4 35.32 990.94 1026.26 NR NR NR NR NR NR >1000
IW-5 NR <1039.50 1080.18 NR NR NR NR NR NR NR
MW-6 21.36 1044.66 1067.67 14.6 NR NR 6.7 246 NR Slight
MW-7 11.38 1060.24 1073.50 15.3 203 1.8 5.5 227 NR 19.8
IW-6 42.30 1045.26 1088.45 NR NR NR NR NR NR >1000
MW-9 32.81 1060.85 1094.07 15.4 -19 0.5 6.1 427 NR 6.3
MW-11 20.50 1127.51 1151.80 15.7 36 3.0 6.5 320 NR 3.3
MW-12S 12.79 1011.65 1025.80 15.5 NR NR 6.3 193 NR Clear
MW-12D 0.00 1027.05 1027.05 15.3 NR NR 6.1 262 NR Slight
MW-13 25.10 982.79 1008.48 14.2 NR NR 5.5 231 NR Clear
MW-14 34.85 981.39 1018.80 14.0 37 0.9 6.0 73 NR 19.8
MW-15 52.42 1026.32 1075.96 15.3 34 0.6 5.7 129 NR 701
MW-16 24.22 972.39 999.54 14.5 NR NR 6.1 367 NR Clear
MW-17 7.55 955.72 965.43 14.4 NR NR 6.3 226 NR Clear
MW-18 8.40 973.95 983.00 13.9 NR NR 6.1 306 NR Clear
MW-19 9.01 937.41 946.27 13.8 NR NR 5.8 31 NR Clear
MW-20 19.11 1062.74 1082.19 14.4 NR NR 6.2 109 NR Slight
MW-21 5.45 959.42 965.36 14.1 138 2.2 5.6 192 NR 101
MW-22 4.71 948.35 953.40 15.1 NR NR 5.7 319 NR Clear
MW-23 6.85 947.85 955.31 13.5 NR NR 6.1 49 NR Slight
Scalehouse na na na 17.5 NR NR 7.6 242 NR Clear
Minimum 0.00 937.41 946.27 13.5 -19 0.5 5.5 31 NR Clear
Average 21.97 1008.87 1034.58 14.9 89 1.7 6.2 224 NR Slight
Maximum 52.42 1127.51 1151.80 17.5 203 3.0 7.6 427 NR >1000
SW-1 ---15.3 NR NR 7.9 74 NR Clear
SW-2 ---16.9 NR NR 7.3 110 NR Clear
SW-3 ---17.8 NR NR 7.1 281 NR Clear
SW-4 ---17.3 NR NR 7.7 73 NR Clear
SWN-1 ---17.0 NR NR 7.3 39 NR Clear
SWN-2 ---16.9 NR NR 7.4 41 NR Clear
Minimum ---17.8 NR NR 7.9 281 NR Clear
Average ---16.9 NR NR 7.5 103 NR Clear
Maximum ---17.8 NR NR 7.9 281 NR Clear
btoc = Below top of casing
amsl = Above mean sea level
na = Not available
NR = No reading attempted
Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1
Table 4
Sampling and Analysis Summary
May 31-June 1, 2017
Tracer
VOCsTotal MetalsVOCs (App II)Total Metals (App II)Herbicides-Chlorinated App IISemivolatile Organics (SVOCs) App IIPesticides App IITotal CyanideSulfideVFAHydrogenMethane/Ethene/EthaneDissolved CO2AlkalinitySulfateSulfideChlorideTOCCODIron, ferrousNitrateDissolved Oxygen (DO)Oxidation Reduction Potential (ORP)TemperatureConductivityTotal Dissolved Solids (TDS)pHTurbidityBromideLab EPA 8260B Lab EPA 6000/7000Lab EPA 8260B Lab EPA 6000/7000 Lab SW8151ALab EPA 8270D Lab EPA 8081BLab EPA 9014Lab SM18 4500-S DAM23GAM20GAXAM20GAXField Hach KitEPA 310.2EPA 300.0Lab SM18 4500-S DEPA 300.0SM 5310BSM 5220DLab EPA 6010Lab EPA 9014Field MeterField MeterField MeterField MeterField MeterField MeterField Meter or VisualEPA 300.0IW-1
MW-1 X X X X X X X X X X X X X X X X X X X X X
IW-2
MW-3R X X X X X X
IW-3
IW-4
IW-5
MW-6 X X X X X X
MW-7 X X X X X X X X X X X X X X X X
IW-6
MW-9 X X X X X X X X X X X X X X X X X X X X X
MW-11 X X X X X X X X X X X X X
MW-12S X X X X X X
MW-12D X X X X X X
MW-13 X X X X X X X X X X X
MW-14 X X X X X X X X X X X X X X X X
MW-15 X X X X X X X X X X X X X X X X X X X X X
MW-16 X X X X X X X X X X X
MW-17 X X X X X X X X X X X
MW-18 X X X X X X
MW-19 X X X X X X
MW-20 X X X X X X
MW-21 X X X X X X X X X X X X X X X X X X X X X
MW-22 X X X X X X X X X X X
MW-23 X X X X X X
Scalehouse X X X X X X X X X X X
SW-1 X X X X X X
SW-2 X X X X X X
SW-3 X X X X X X
SW-4 X X X X X X
SWN-1 X X X X X X
SWN-2 X X X X X X
EB X X X
FB X X
TB X
Injection wells exempt from monitoring except for turbidity and WLR per SWS approved SAP [18936]
Not sampled since injection wells are exempt
App I & II Lists = From current 40 CFR 258
Not sampled since injection wells are exempt
Not sampled since injection wells are exempt
Not sampled since injection wells are exempt
Not sampled since injection wells are exempt
Not sampled since injection wells are exempt
App. IIApp. I MNA Field Parameter
Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1
Table 5
Groundwater and QC Sample Detections
May 31- June 1, 2017
MW-1 MW-3R MW-6 MW-7 MW-9 MW-11 MW-12D MW-12S MW-13 MW-14 MW-15 MW-16 MW-17 MW-18 MW-19 MW-20 MW-21 MW-22 MW-23 SCALEHOUSE EB FB TBBSSSSSSSSSSSSSSSSSSSupply Well QC QC QC
Barium, total 2.5 100 700 2000 92.9 J 7.4 J 92.4 J 55.1 J 48.2 J 40.7 J 7.3 J 23.5 J 85.7 J 84 J 49.2 J 68 J 27.5 J 28.4 J 70.2 J 27.6 J 60.5 J 56.9 J 33.8 J 14.4 J --
Beryllium, total 0.5 1 4 4 0.61 J --
Cadmium, total 0.5 1 2 5 0.89 J 1.3 1.4 0.66 J 1.5 0.52 J 0.63 J 2.1 (N)--
Chromium, total 2.5 10 10 100 3.2 J 2.8 J 12.4 (N)7 J 2.6 J 5.6 J --
Cobalt, total 2.5 10 1 NE 51.6 (N)50.7 (N)166 (N)11.7 (N)11 (N)13.1 (N)2.7 J (N)242 (N)4.1 J (N)12.3 (N)4.8 J (N)--
Copper, total 2.5 10 1000 1300 356 4.2 J 2.7 J 3.5 J 6.9 J 3.8 J 122 4.4 J 5 J --
Lead, total 2.5 10 15 15 21 (N)2.8 J 2.6 J 3 J 2.7 J 9.2 J 3 J --
Nickel, total 2.5 50 100 NE 4.5 J 3.6 J 6.6 J 2.7 J 2.8 J 2.6 J 8.6 J 3.1 J 13.2 J 3.2 J 2.6 J --
Thallium, total 0.02 5.5 0.28 2 0.026 J 0.3 J (N)0.11 J 0.33 J (N)0.061 J 0.12 J 0.16 J 0.091 J 0.2 J 0.054 J 0.081 J 0.32 J
(N)
0.11 J 0.024 J --
Vanadium, total 2.5 25 0.3 NE 18 J (N)3.1 J (N)8.2 J (N)--
Zinc, total 5 10 1000 NE 256 10.7 10.7 38.3 19.4 6.6 J 8.4 J 36.1 10.7 14.7 5.1 J 10.7 20.2 7.7 J 5.3 J 6.3 J 6.5 J 16 --
1,1-Dichloroethane 0.32 5 6 NE 2.4 J 0.37 J 4 J 2.6 J 9.7 (L)0.58 J 0.36 J 4.1 J 0.63 J 0.43 J
1,2-Dichlorobenzene 0.3 5 20 NE 1.5 J 0.48 J
1,2-Dichloroethane 0.24 1 0.4 5 0.96 J (L)0.58 J
(L)
0.81 J
(L)
0.49 J (L)
1,4-Dichlorobenzene 0.33 1 6 75 2.2 5.7 2.5 3.6 3.7 4.3 1.1
Acetone 10 100 6000 NE 29.5 J 21.4 J 13.5 J 20.7 J 16.1 J 14.4 J 11 J 15.2 J 12.9 J 14.4 J 10.2 JBenzene0.25 1 1 5 0.3 J 2.4 (L)0.62 J 0.65 J 0.44 J
Chlorobenzene 0.23 3 50 100 3.9 2.2 J 0.87 J 1.6 J 2.4 J 1.8 J 0.25 J 0.42 J
Chloroethane 0.54 10 3000 NE 1.9 J
Chloromethane 0.11 1 3 NE 0.32 J 0.14 J 0.14 J
cis-1,2-Dichloroethene 0.19 5 70 70 0.28 J 19.7 1 J 28.1 4 J 33.3 11.5 0.65 J 0.64 J 18.6 0.94 J 0.39 J 0.22 J
Tetrachloroethene 0.46 1 0.7 5 0.54 J
Toluene 0.26 1 600 1000 0.88 J
Trichloroethene 0.47 1 3 5 0.98 J 2 0.7 J
Vinyl chloride 0.62 1 0.03 2 18.7 (L)1.6 (L)1.3 (L)
Acrolein 1.6 53 4 NE ------2.1 J --------------
Allyl chloride 1.5 10 NE NE ------8.2 J --------------4.1 J
Cyanide 4 10 70 NE --------------4.6 J 12.7 5.2 J ------4.7 J ------
Tin, total 2.5 100 2000 NE 3.9 J ------------5.3 J ----------
Red Bold Above Established MCL/2L/GWP Std.
No regulatory compliance significance.
MDL = Method Detection Limit, SWSL = Solid Waste Section Limit, 2L/GWP Standard = NC 2L and IMAC Standards adopted by SWS, MCL = Maximum Contaminant Level for Drinking Water
J = "J-qualified". Concentration detected between MDL and SWSL. Considered estimated value
(N) Preliminary source is believed to be Natural originating from erosion of natural deposits. Source not anthropogenic.
(L) Prelilminary source is believed to be anthropogenic with leachate or landfill gas as transport mechanism
A definitive source of the detections was not determined as part of this report.
BG = Background Well Sample, QC = Quality Control Sample, S = Sentinal Well Sample
Metals (Appendix I)
VOCs (Appendix I)
Assessement Monitoring Parameters (Appendix II)
Yellow Highlighted Above Established Federal MCL Drinking Water Std.
Units ug/L, Blank cells means Not Detected, -- means not tested
Parameter Name MDL SWSL 2L/GWP
Std MCL
Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1
Table 6
Surface Water and QC Sample Detections
June 1, 2017
SWN-1 SW-1 SW-2 SW-3 SW-4 SW-A SW-B SWN-2 EB FB TB
U D D D D D D D QC QC QC
Barium, total 2.5 100 200000 2000 21.3 J 26.8 J 17 J 21.8 J 22 J ----20.4 J --
Cobalt, total 2.5 10 270 NE 16.8 8 J ------
Thallium, total 0.02 5.5 0.47 2 0.048 J 0.054 J ------
Vanadium, total 2.5 25 NE NE ----2.8 J --
Zinc, total 5 10 50 NE 9.1 J 7.4 J 7 J ----5.4 J --
Acetone 10 100 2000 NE 13.3 J 19.3 J 12.2 J 11.6 J 14.4 J 10.2 J
Chloromethane 0.11 1 550 NE 0.13 J 0.13 J 0.14 J
cis-1,2-Dichloroethene 0.19 5 4900 70 2.4 J
Red Bold Above Established 2B Std.Regulatory compliance Standard
Yellow Highlighted Above Established Federal MCL Drinking Water Std. No regulatory compliance significance.
MDL = Method Detection Limit, SWSL = Solid Waste Section Limit, 2B Standard = NC 2B Surface Water Standards adopted by SWS, MCL = Maximum Contaminant Level for Drinking Water
J = "J-qualified". Concentration detected between MDL and SWSL. Considered estimated value
U = Upstream of monitored unit, D= Downstream of monitored unit
Units ug/L, Blank cells means Not Detected, -- means not tested
Parameter Name MDL SWSL 2B Std MCL
Metals (Appendix I)
VOCs (Appendix I)
Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1
Table 7
MNA Parameter Data Summary
May 31 - June 1, 2017
MW-1 MW-7 MW-9 MW-11 MW-14 MW-15 MW-21
6/1/17 6/1/17 6/1/17 6/1/17 6/1/17 5/31/17 5/31/17
VFA – Acetic Acid AM23G NS ug/L NS NS NS NS NS NS NS
VFA – Butyric Acid AM23G NS ug/L NS NS NS NS NS NS NS
VFA – Lactic Acid AM23G NS ug/L NS NS NS NS NS NS NS
VFA – Propionic Acid AM23G NS ug/L NS NS NS NS NS NS NS
VFA – Pyruvic Acid AM23G NS ug/L NS NS NS NS NS NS NS
Hydrogen AM20GAX NS nM NS NS NS NS NS NS NS
Methane AM20GAX NS ug/L NS NS NS NS NS NS NS
Ethene AM20GAX NS ug/L NS NS NS NS NS NS NS
Ethane AM20GAX NS ug/L NS NS NS NS NS NS NS
CO2-Dissolved Field HACH Kit 10 mg/L 20 >100 >100 >100 >100 >100 >100
Alkalinity SM 2320B 1000 ug/L 42200 69200 44800 NS NS 43700 34900
Sulfate EPA 300.0 1000 ug/L 8830 5520 984 NS 2060 1180 1380
Sulfide SM 4500-S2D 100 ug/L <100 <100 <100 NS 115 NS NS
Chloride SM 4500-Cl-E 500 ug/L 3770 31200 28300 NS 2280 1450 28800
TOC SM 5310B 500 ug/L 605 2400 2250 NS 1420 675 1200
COD SM 5220D 12500 ug/L <12500 20000 23000 NS 13000 <12500 <12500
BOD SM5210B NS ug/L NS NS NS NS NS NS NS
Ferrous Iron EPA 6010 500 ug/L <500 <500 1300 NS <500 1700 <500
Nitrate EPA 353.2 NS ug/L NS NS NS NS NS NS NS
Temperature Field Instrument 0 C 15.3 15.3 15.4 15.7 14.0 15.3 14.1
ORP Field Instrument -900 mV 191 203 -19 36 37 34 138
DO Field Instrument 0 mg/L 2.6 1.8 0.5 3 0.9 0.6 2.2
pH Field Instrument 0 SU 6.3 5.5 6.1 6.5 6 5.7 5.6
Specific Conductance Field Instrument 0 us/cm 210 227 427 320 73 129 192TurbidityVisual0Visual6.7 19.8 6.3 3.3 19.8 701 101
Notes:
VFA = Volatile Fatty Acids
MDL* = Lab Method Detection Limit or lowest field measurement possible. Constituents detected below quantifiable limits are shown as < MDL value.
>100 = CO2 Concentration exceeds maximum capability of method used.
NS = Not Sampled
Parameters Method MDL*Units
Surry County Closed CDLF and CLosed MSWLF, Mt. Airy Page 1 of 1
Table 8
Hydrogeolofic Properties at Monitoring Well Locations
May 31-June 1, 2017
Effective
Porosity
Hydraulic
Gradient
Groundwater Average
Linear Velocity Rate
Minimum
Distance From
Upgradient
EOW
Ground Water
Depth
Groundwater
Potentiometric
Elevation
(cm/second)(ft/day)(%)(feet/feet)(feet/year)(ft)(feet btoc)(feet amsl)
MW-1 4.30E-05 0.12 15 0.054 16 S20W 0 20.94 1113.41 Clay
IW-2 4.30E-05 0.12 15 0.238 71 S50E -40.95 1027.91 Clay
MW-7 8.10E-04 2.30 15 0.891 4,977 N69W 704 11.38 1062.12 PWR / Fractured Rock
IW-6 4.40E-04 1.25 15 0.101 305 S51E -42.30 1046.15 PWR / Fractured Rock
MW-9 1.90E-04 0.54 15 0.069 90 S54E 614 32.81 1061.26 Sandy Silt
MW-13 2.06E-04 0.58 23 0.464 430 S29W 1850 25.10 983.38 Saprolite
MW-18 2.04E-03 5.78 15 0.142 na S24E 0 8.40 974.60 Saprolite
MW-19 1.10E-03 3.12 3 0.056 2,121 S12W 2663 9.01 937.26 PWR
MW-21 1.28E-03 3.63 3 0.003 124 S66E 2041 5.45 959.91 Saprolite/PWR
MW-22 9.88E-04 2.80 15 0.073 498 S28W 2506 4.71 948.69 Saprolite
MW-23 3.04E-04 0.86 15 0.046 96 S32E 2610 6.85 948.46 Sandy Silt
Minimum 4.30E-05 0.12 3 0.003 16 -0 4.71 937.26 -
Average 6.77E-04 1.92 14 0.194 873 -1443 18.90 1005.74 -Maximum 2.04E-03 5.78 23 0.891 4,977 -2663 42.30 1113.41 -
MW-3R 2.40E-04 0.68 5 na na na 1,994 39.28 978.22 Fractured Rock
IW-3 2.40E-05 0.07 5 0.394 196 S37W -30.10 990.47 Fractured Rock
IW-4 1.10E-04 0.31 5 0.139 317 S45E -35.32 990.94 Fractured Rock
IW-5 1.50E-05 0.04 5 --S61E ---Fractured Rock
MW-6 1.90E-05 0.05 5 0.174 68 S85W 963 21.36 1046.31 Fractured Rock
MW-11 3.10E-04 0.88 5 0.040 256 S18W 0 20.50 1131.30 Fractured Rock
MW-12S na na 3 0.179 na S07E 0 12.79 1013.01 Fractured Rock
MW-12D 1.30E-06 0.00 5 na na na 0 0.00 1027.05 Fractured Rock
MW-14 7.45E-03 21.12 3 0.163 41,990 S74E 2098 34.85 983.95 Fractured Rock
MW-15 7.21E-05 0.20 3 0.212 528 S08E 52.42 1023.54 Fractured Rock
MW-16 2.82E-05 0.08 3 0.094 91 S53W 2089 24.22 975.32 Fractured Rock
MW-17 2.94E-04 0.83 3 0.027 272 S77W 2547 7.55 957.88 Rock
MW-20 1.92E-04 0.54 3 0.097 644 S22E 692 19.11 1063.08 Rock
Minimum 1.30E-06 0.00 3 0.027 68 -0 0.00 957.88 -
Average 7.30E-04 2.07 4 0.152 297 -1154 24.79 1015.09 -Maximum 7.45E-03 21.12 5 0.394 644 -2547 52.42 1131.30 -
NOTE: Values for hydraulic conductivity determined via slug test by GAI, MESCO, or Joyce.
Hydrologic gradient from water levels recorded on May 31-June 1, 2017.
Wells screened entirely in rock were not utilized for flow directions/gradients.
Screens that traverse both rock and regolith assumed flow in regolith dominates.
Hydraulic Conducitivity value and flow rate for MW-14 was considered an outlier; therefore not included in the average or maximum.
na = Not available/applicable
Average Linear Velocity (Q) is defined by modified Darcy's equation:
K= hydraulic conductivity
where ne= effective porosity
dh= head difference
dl= horizontal distance
Well Hydraulic Conductivity
Flow
Direction
Screened Interval
Lithology
dl
dh
n
KQ
e

Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1
Appendix A
Laboratory Analysis Reports
Chains of Custody
#=CL#
June 19, 2017
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92342784
92342784
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
SURRY CLOSED-MT. AIRY (AM)
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on June 02, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 54
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Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
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West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 54
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Lab ID Sample ID Matrix Date Collected Date Received
92342784001 MW-6 Water 06/01/17 15:00 06/02/17 08:00
92342784002 MW-12D Water 06/01/17 09:35 06/02/17 08:00
92342784003 MW-11 Water 06/01/17 12:02 06/02/17 08:00
92342784004 SCALE HOUSE Water 06/01/17 16:22 06/02/17 08:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 54
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92342784001 MW-6 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92342784002 MW-12D EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92342784003 MW-11 EPA 8081 21 PASI-CRES
EPA 8082 8 PASI-CHSK
EPA 8151 6 PASI-OLJM
EPA 6010 15 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CGAW
SM 4500-S2D 1 PASI-AMVC
SM 4500-CN-E 1 PASI-AAES2
92342784004 SCALE HOUSE EPA 8081 21 PASI-CRES
EPA 8082 8 PASI-CHSK
EPA 8151 6 PASI-OLJM
EPA 6010 15 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CGAW
SM 4500-S2D 1 PASI-AMVC
SM 4500-CN-E 1 PASI-AAES2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Sample:MW-6 Lab ID:92342784001 Collected:06/01/17 15:00 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/14/17 22:31 7440-36-006/04/17 16:406.0 3.9 1
Arsenic ND ug/L 06/14/17 22:31 7440-38-206/04/17 16:4010.0 5.0 1
Barium 92.4J ug/L 06/14/17 22:31 7440-39-306/04/17 16:401002.5 1
Beryllium ND ug/L 06/14/17 22:31 7440-41-706/04/17 16:401.0 0.50 1
Cadmium ND ug/L 06/14/17 22:31 7440-43-906/04/17 16:401.0 0.50 1
Chromium 3.2J ug/L 06/14/17 22:31 7440-47-306/04/17 16:4010.0 2.5 1
Cobalt 51.6 ug/L 06/14/17 22:31 7440-48-406/04/17 16:4010.0 2.5 1
Copper ND ug/L 06/14/17 22:31 7440-50-806/04/17 16:4010.0 2.5 1
Lead 2.8J ug/L 06/14/17 22:31 7439-92-106/04/17 16:4010.0 2.5 1
Nickel 3.6J ug/L 06/14/17 22:31 7440-02-006/04/17 16:4050.0 2.5 1
Selenium ND ug/L 06/14/17 22:31 7782-49-206/04/17 16:4010.0 5.0 1
Silver ND ug/L 06/14/17 22:31 7440-22-406/04/17 16:4010.0 2.5 1
Vanadium ND ug/L 06/14/17 22:31 7440-62-206/04/17 16:4025.0 2.5 1
Zinc 10.7 ug/L 06/14/17 22:31 7440-66-606/04/17 16:4010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.30J ug/L 06/09/17 20:20 7440-28-006/06/17 02:455.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/04/17 15:00 67-64-110010.0 1
Acrylonitrile ND ug/L 06/04/17 15:00 107-13-12001.9 1
Benzene ND ug/L 06/04/17 15:00 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 15:00 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 15:00 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 15:00 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 15:00 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 15:00 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 15:00 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 15:00 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/17 15:00 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 15:00 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 15:00 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/17 15:00 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 15:00 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 15:00 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 15:00 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 15:00 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 15:00 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/04/17 15:00 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 15:00 110-57-6 L11001.0 1
1,1-Dichloroethane ND ug/L 06/04/17 15:00 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 15:00 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 15:00 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/17 15:00 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 15:00 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 15:00 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Sample:MW-6 Lab ID:92342784001 Collected:06/01/17 15:00 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 06/04/17 15:00 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 15:00 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 15:00 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/04/17 15:00 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 15:00 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/04/17 15:00 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 15:00 108-10-11000.33 1
Styrene ND ug/L 06/04/17 15:00 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 15:00 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 15:00 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 15:00 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 15:00 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/04/17 15:00 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 15:00 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 15:00 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 15:00 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 15:00 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 15:00 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 15:00 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/17 15:00 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %06/04/17 15:00 460-00-470-130 1
1,2-Dichloroethane-d4 (S)88 %06/04/17 15:00 17060-07-070-130 1
Toluene-d8 (S)110 %06/04/17 15:00 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Sample:MW-12D Lab ID:92342784002 Collected:06/01/17 09:35 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/14/17 22:34 7440-36-006/04/17 16:406.0 3.9 1
Arsenic ND ug/L 06/14/17 22:34 7440-38-206/04/17 16:4010.0 5.0 1
Barium 7.3J ug/L 06/14/17 22:34 7440-39-306/04/17 16:401002.5 1
Beryllium ND ug/L 06/14/17 22:34 7440-41-706/04/17 16:401.0 0.50 1
Cadmium 1.4 ug/L 06/14/17 22:34 7440-43-906/04/17 16:401.0 0.50 1
Chromium ND ug/L 06/14/17 22:34 7440-47-306/04/17 16:4010.0 2.5 1
Cobalt ND ug/L 06/14/17 22:34 7440-48-406/04/17 16:4010.0 2.5 1
Copper ND ug/L 06/14/17 22:34 7440-50-806/04/17 16:4010.0 2.5 1
Lead ND ug/L 06/14/17 22:34 7439-92-106/04/17 16:4010.0 2.5 1
Nickel ND ug/L 06/14/17 22:34 7440-02-006/04/17 16:4050.0 2.5 1
Selenium ND ug/L 06/14/17 22:34 7782-49-206/04/17 16:4010.0 5.0 1
Silver ND ug/L 06/14/17 22:34 7440-22-406/04/17 16:4010.0 2.5 1
Vanadium ND ug/L 06/14/17 22:34 7440-62-206/04/17 16:4025.0 2.5 1
Zinc ND ug/L 06/14/17 22:34 7440-66-606/04/17 16:4010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/09/17 20:28 7440-28-006/06/17 02:455.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/04/17 15:18 67-64-110010.0 1
Acrylonitrile ND ug/L 06/04/17 15:18 107-13-12001.9 1
Benzene ND ug/L 06/04/17 15:18 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 15:18 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 15:18 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 15:18 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 15:18 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 15:18 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 15:18 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 15:18 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/17 15:18 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 15:18 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 15:18 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/17 15:18 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 15:18 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 15:18 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 15:18 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 15:18 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 15:18 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/04/17 15:18 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 15:18 110-57-6 L11001.0 1
1,1-Dichloroethane ND ug/L 06/04/17 15:18 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 15:18 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 15:18 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/17 15:18 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 15:18 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 15:18 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Sample:MW-12D Lab ID:92342784002 Collected:06/01/17 09:35 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 06/04/17 15:18 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 15:18 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 15:18 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/04/17 15:18 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 15:18 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/04/17 15:18 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 15:18 108-10-11000.33 1
Styrene ND ug/L 06/04/17 15:18 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 15:18 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 15:18 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 15:18 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 15:18 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/04/17 15:18 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 15:18 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 15:18 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 15:18 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 15:18 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 15:18 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 15:18 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/17 15:18 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)96 %06/04/17 15:18 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %06/04/17 15:18 17060-07-070-130 1
Toluene-d8 (S)109 %06/04/17 15:18 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Sample:MW-11 Lab ID:92342784003 Collected:06/01/17 12:02 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/06/17 12:16 309-00-206/05/17 17:300.050 0.050 1
alpha-BHC ND ug/L 06/06/17 12:16 319-84-606/05/17 17:300.050 0.050 1
beta-BHC ND ug/L 06/06/17 12:16 319-85-706/05/17 17:300.050 0.050 1
delta-BHC ND ug/L 06/06/17 12:16 319-86-806/05/17 17:300.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/06/17 12:16 58-89-906/05/17 17:300.050 0.050 1
Chlordane (Technical)ND ug/L 06/06/17 12:16 57-74-906/05/17 17:300.50 0.20 1
4,4'-DDD ND ug/L 06/06/17 12:16 72-54-806/05/17 17:300.10 0.050 1
4,4'-DDE ND ug/L 06/06/17 12:16 72-55-906/05/17 17:300.10 0.050 1
4,4'-DDT ND ug/L 06/06/17 12:16 50-29-306/05/17 17:300.10 0.050 1
Dieldrin ND ug/L 06/06/17 12:16 60-57-106/05/17 17:300.075 0.050 1
Endosulfan I ND ug/L 06/06/17 12:16 959-98-806/05/17 17:300.10 0.050 1
Endosulfan II ND ug/L 06/06/17 12:16 33213-65-906/05/17 17:300.10 0.050 1
Endosulfan sulfate ND ug/L 06/06/17 12:16 1031-07-806/05/17 17:300.10 0.050 1
Endrin ND ug/L 06/06/17 12:16 72-20-806/05/17 17:300.10 0.050 1
Endrin aldehyde ND ug/L 06/06/17 12:16 7421-93-406/05/17 17:300.10 0.050 1
Heptachlor ND ug/L 06/06/17 12:16 76-44-806/05/17 17:300.050 0.050 1
Heptachlor epoxide ND ug/L 06/06/17 12:16 1024-57-306/05/17 17:300.075 0.050 1
Methoxychlor ND ug/L 06/06/17 12:16 72-43-506/05/17 17:301.0 0.15 1
Toxaphene ND ug/L 06/06/17 12:16 8001-35-206/05/17 17:301.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)99 %06/06/17 12:16 877-09-806/05/17 17:3020-130 1
Decachlorobiphenyl (S)63 %06/06/17 12:16 2051-24-306/05/17 17:3020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/06/17 18:47 12674-11-206/05/17 17:300.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/06/17 18:47 11104-28-206/05/17 17:300.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/06/17 18:47 11141-16-506/05/17 17:300.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/06/17 18:47 53469-21-906/05/17 17:300.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/06/17 18:47 12672-29-606/05/17 17:300.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/06/17 18:47 11097-69-106/05/17 17:300.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/06/17 18:47 11096-82-506/05/17 17:300.50 0.50 1
Surrogates
Decachlorobiphenyl (S)56 %06/06/17 18:47 2051-24-306/05/17 17:3010-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/10/17 05:36 94-75-706/07/17 16:000.97 0.23 1
Dinoseb ND ug/L 06/10/17 05:36 88-85-706/07/17 16:000.20 0.059 1
Pentachlorophenol ND ug/L 06/10/17 05:36 87-86-506/07/17 16:000.029 0.018 1
2,4,5-T ND ug/L 06/10/17 05:36 93-76-506/07/17 16:000.20 0.044 1
2,4,5-TP (Silvex)ND ug/L 06/10/17 05:36 93-72-106/07/17 16:000.20 0.051 1
Surrogates
2,4-DCAA (S)86 %06/10/17 05:36 19719-28-906/07/17 16:0039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/14/17 22:37 7440-36-006/04/17 16:406.0 3.9 1
Arsenic ND ug/L 06/14/17 22:37 7440-38-206/04/17 16:4010.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Sample:MW-11 Lab ID:92342784003 Collected:06/01/17 12:02 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Barium 40.7J ug/L 06/14/17 22:37 7440-39-306/04/17 16:401002.5 1
Beryllium ND ug/L 06/14/17 22:37 7440-41-706/04/17 16:401.0 0.50 1
Cadmium 1.3 ug/L 06/14/17 22:37 7440-43-906/04/17 16:401.0 0.50 1
Chromium ND ug/L 06/14/17 22:37 7440-47-306/04/17 16:4010.0 2.5 1
Cobalt 11.7 ug/L 06/14/17 22:37 7440-48-406/04/17 16:4010.0 2.5 1
Copper 2.7J ug/L 06/14/17 22:37 7440-50-806/04/17 16:4010.0 2.5 1
Lead 2.6J ug/L 06/14/17 22:37 7439-92-106/04/17 16:4010.0 2.5 1
Nickel 2.7J ug/L 06/14/17 22:37 7440-02-006/04/17 16:4050.0 2.5 1
Selenium ND ug/L 06/14/17 22:37 7782-49-206/04/17 16:4010.0 5.0 1
Silver ND ug/L 06/14/17 22:37 7440-22-406/04/17 16:4010.0 2.5 1
Tin ND ug/L 06/14/17 22:37 7440-31-506/04/17 16:401002.5 1
Vanadium ND ug/L 06/14/17 22:37 7440-62-206/04/17 16:4025.0 2.5 1
Zinc 19.4 ug/L 06/14/17 22:37 7440-66-606/04/17 16:4010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.061J ug/L 06/09/17 16:26 7440-28-006/03/17 02:255.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 03:12 7439-97-606/04/17 20:450.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/14/17 18:56 83-32-906/07/17 17:1010.0 1.6 1
Acenaphthylene ND ug/L 06/14/17 18:56 208-96-806/07/17 17:1010.0 1.5 1
Acetophenone ND ug/L 06/14/17 18:56 98-86-206/07/17 17:1010.0 1.9 1
2-Acetylaminofluorene ND ug/L 06/14/17 18:56 53-96-3 L206/07/17 17:1020.0 1.6 1
4-Aminobiphenyl ND ug/L 06/14/17 18:56 92-67-106/07/17 17:1020.0 1.7 1
Anthracene ND ug/L 06/14/17 18:56 120-12-706/07/17 17:1010.0 1.7 1
Benzo(a)anthracene ND ug/L 06/14/17 18:56 56-55-306/07/17 17:1010.0 2.1 1
Benzo(a)pyrene ND ug/L 06/14/17 18:56 50-32-806/07/17 17:1010.0 2.2 1
Benzo(b)fluoranthene ND ug/L 06/14/17 18:56 205-99-206/07/17 17:1010.0 2.2 1
Benzo(g,h,i)perylene ND ug/L 06/14/17 18:56 191-24-206/07/17 17:1010.0 2.1 1
Benzo(k)fluoranthene ND ug/L 06/14/17 18:56 207-08-906/07/17 17:1010.0 2.0 1
Benzyl alcohol ND ug/L 06/14/17 18:56 100-51-606/07/17 17:1020.0 3.1 1
4-Bromophenylphenyl ether ND ug/L 06/14/17 18:56 101-55-306/07/17 17:1010.0 1.5 1
Butylbenzylphthalate ND ug/L 06/14/17 18:56 85-68-706/07/17 17:1010.0 2.5 1
4-Chloro-3-methylphenol ND ug/L 06/14/17 18:56 59-50-706/07/17 17:1020.0 2.8 1
4-Chloroaniline ND ug/L 06/14/17 18:56 106-47-806/07/17 17:1020.0 2.8 1
Chlorobenzilate ND ug/L 06/14/17 18:56 510-15-606/07/17 17:1010.0 2.2 1
bis(2-Chloroethoxy)methane ND ug/L 06/14/17 18:56 111-91-106/07/17 17:1010.0 1.6 1
bis(2-Chloroethyl) ether ND ug/L 06/14/17 18:56 111-44-406/07/17 17:1010.0 1.7 1
2-Chloronaphthalene ND ug/L 06/14/17 18:56 91-58-706/07/17 17:1010.0 1.6 1
2-Chlorophenol ND ug/L 06/14/17 18:56 95-57-806/07/17 17:1010.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/14/17 18:56 7005-72-306/07/17 17:1010.0 1.6 1
Chrysene ND ug/L 06/14/17 18:56 218-01-906/07/17 17:1010.0 2.1 1
Diallate ND ug/L 06/14/17 18:56 2303-16-406/07/17 17:1010.0 1.6 1
Dibenz(a,h)anthracene ND ug/L 06/14/17 18:56 53-70-306/07/17 17:1010.0 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Sample:MW-11 Lab ID:92342784003 Collected:06/01/17 12:02 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Dibenzofuran ND ug/L 06/14/17 18:56 132-64-906/07/17 17:1010.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 06/14/17 18:56 91-94-106/07/17 17:1020.0 3.9 1
2,4-Dichlorophenol ND ug/L 06/14/17 18:56 120-83-206/07/17 17:1010.0 1.6 1
2,6-Dichlorophenol ND ug/L 06/14/17 18:56 87-65-006/07/17 17:1010.0 1.5 1
Diethylphthalate ND ug/L 06/14/17 18:56 84-66-206/07/17 17:1060001.6 1
Dimethoate ND ug/L 06/14/17 18:56 60-51-506/07/17 17:1020.0 1.8 1
P-Dimethylaminoazobenzene ND ug/L 06/14/17 18:56 60-11-706/07/17 17:1010.0 1.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/14/17 18:56 57-97-606/07/17 17:1010.0 2.4 1
3,3'-Dimethylbenzidine ND ug/L 06/14/17 18:56 119-93-706/07/17 17:1010.0 3.9 1
2,4-Dimethylphenol ND ug/L 06/14/17 18:56 105-67-906/07/17 17:1010.0 1.6 1
Dimethylphthalate ND ug/L 06/14/17 18:56 131-11-306/07/17 17:1010.0 1.4 1
Di-n-butylphthalate ND ug/L 06/14/17 18:56 84-74-206/07/17 17:1010.0 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/14/17 18:56 534-52-106/07/17 17:1050.0 2.2 1
1,3-Dinitrobenzene ND ug/L 06/14/17 18:56 99-65-006/07/17 17:1020.0 1.3 1
2,4-Dinitrophenol ND ug/L 06/14/17 18:56 51-28-506/07/17 17:1050.0 5.1 1
2,4-Dinitrotoluene ND ug/L 06/14/17 18:56 121-14-206/07/17 17:1010.0 1.5 1
2,6-Dinitrotoluene ND ug/L 06/14/17 18:56 606-20-206/07/17 17:1010.0 1.4 1
Di-n-octylphthalate ND ug/L 06/14/17 18:56 117-84-006/07/17 17:1010.0 1.5 1
Diphenylamine ND ug/L 06/14/17 18:56 122-39-406/07/17 17:1010.0 1.4 1
Disulfoton ND ug/L 06/14/17 18:56 298-04-406/07/17 17:1010.0 1.5 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/14/17 18:56 117-81-706/07/17 17:1015.0 2.3 1
Ethyl methanesulfonate ND ug/L 06/14/17 18:56 62-50-006/07/17 17:1020.0 1.6 1
Famphur ND ug/L 06/14/17 18:56 52-85-706/07/17 17:1020.0 5.7 1
Fluoranthene ND ug/L 06/14/17 18:56 206-44-006/07/17 17:1010.0 2.2 1
Fluorene ND ug/L 06/14/17 18:56 86-73-706/07/17 17:1010.0 1.6 1
Hexachlorobenzene ND ug/L 06/14/17 18:56 118-74-106/07/17 17:1010.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 06/14/17 18:56 77-47-406/07/17 17:1010.0 1.3 1
Hexachloroethane ND ug/L 06/14/17 18:56 67-72-106/07/17 17:1010.0 1.8 1
Hexachloropropene ND ug/L 06/14/17 18:56 1888-71-706/07/17 17:1010.0 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/14/17 18:56 193-39-506/07/17 17:1010.0 2.0 1
Isodrin ND ug/L 06/14/17 18:56 465-73-606/07/17 17:1020.0 2.5 1
Isophorone ND ug/L 06/14/17 18:56 78-59-106/07/17 17:1010.0 1.5 1
Isosafrole ND ug/L 06/14/17 18:56 120-58-106/07/17 17:1010.0 1.5 1
Kepone ND ug/L 06/14/17 18:56 143-50-006/07/17 17:1020.0 4.5 1
Methapyrilene ND ug/L 06/14/17 18:56 91-80-506/07/17 17:101003.0 1
3-Methylcholanthrene ND ug/L 06/14/17 18:56 56-49-506/07/17 17:1010.0 2.7 1
Methyl methanesulfonate ND ug/L 06/14/17 18:56 66-27-306/07/17 17:1010.0 1.1 1
2-Methylnaphthalene ND ug/L 06/14/17 18:56 91-57-606/07/17 17:1010.0 1.4 1
Methyl parathion ND ug/L 06/14/17 18:56 298-00-006/07/17 17:1010.0 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 06/14/17 18:56 95-48-706/07/17 17:1010.0 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/14/17 18:56 15831-10-406/07/17 17:1010.0 1.4 1
1-Naphthalenamine ND ug/L 06/14/17 18:56 134-32-706/07/17 17:1010.0 1.3 1
2-Naphthalenamine ND ug/L 06/14/17 18:56 91-59-806/07/17 17:1010.0 2.2 1
1,4-Naphthoquinone ND ug/L 06/14/17 18:56 130-15-406/07/17 17:1010.0 0.99 1
2-Nitroaniline ND ug/L 06/14/17 18:56 88-74-406/07/17 17:1050.0 2.3 1
3-Nitroaniline ND ug/L 06/14/17 18:56 99-09-206/07/17 17:1050.0 2.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Sample:MW-11 Lab ID:92342784003 Collected:06/01/17 12:02 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Nitroaniline ND ug/L 06/14/17 18:56 100-01-606/07/17 17:1020.0 3.4 1
Nitrobenzene ND ug/L 06/14/17 18:56 98-95-306/07/17 17:1010.0 1.6 1
2-Nitrophenol ND ug/L 06/14/17 18:56 88-75-506/07/17 17:1010.0 1.6 1
4-Nitrophenol ND ug/L 06/14/17 18:56 100-02-706/07/17 17:1050.0 4.3 1
5-Nitro-o-toluidine ND ug/L 06/14/17 18:56 99-55-806/07/17 17:1010.0 1.9 1
N-Nitrosodiethylamine ND ug/L 06/14/17 18:56 55-18-506/07/17 17:1020.0 1.4 1
N-Nitrosodimethylamine ND ug/L 06/14/17 18:56 62-75-906/07/17 17:1010.0 1.6 1
N-Nitroso-di-n-butylamine ND ug/L 06/14/17 18:56 924-16-306/07/17 17:1010.0 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 06/14/17 18:56 621-64-706/07/17 17:1010.0 1.7 1
N-Nitrosodiphenylamine ND ug/L 06/14/17 18:56 86-30-606/07/17 17:1010.0 1.4 1
N-Nitrosomethylethylamine ND ug/L 06/14/17 18:56 10595-95-606/07/17 17:1010.0 1.4 1
N-Nitrosopiperidine ND ug/L 06/14/17 18:56 100-75-406/07/17 17:1020.0 1.7 1
N-Nitrosopyrrolidine ND ug/L 06/14/17 18:56 930-55-206/07/17 17:1010.0 1.7 1
O,O,O-Triethylphosphorothioate ND ug/L 06/14/17 18:56 126-68-106/07/17 17:1010.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/14/17 18:56 108-60-106/07/17 17:1010.0 1.8 1
Parathion (Ethyl parathion)ND ug/L 06/14/17 18:56 56-38-206/07/17 17:1010.0 1.5 1
Pentachlorobenzene ND ug/L 06/14/17 18:56 608-93-506/07/17 17:1010.0 1.5 1
Pentachloronitrobenzene ND ug/L 06/14/17 18:56 82-68-806/07/17 17:1020.0 1.7 1
Pentachlorophenol ND ug/L 06/14/17 18:56 87-86-506/07/17 17:1025.0 3.5 1
Phenacetin ND ug/L 06/14/17 18:56 62-44-206/07/17 17:1020.0 1.9 1
Phenanthrene ND ug/L 06/14/17 18:56 85-01-806/07/17 17:1010.0 1.6 1
Phenol ND ug/L 06/14/17 18:56 108-95-206/07/17 17:1010.0 1.3 1
p-Phenylenediamine ND ug/L 06/14/17 18:56 106-50-306/07/17 17:1010.0 2.2 1
Phorate ND ug/L 06/14/17 18:56 298-02-206/07/17 17:1010.0 1.7 1
Pronamide ND ug/L 06/14/17 18:56 23950-58-506/07/17 17:1010.0 2.0 1
Pyrene ND ug/L 06/14/17 18:56 129-00-006/07/17 17:1010.0 2.2 1
Safrole ND ug/L 06/14/17 18:56 94-59-706/07/17 17:1010.0 1.3 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/14/17 18:56 95-94-306/07/17 17:1010.0 1.3 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/14/17 18:56 58-90-206/07/17 17:1010.0 2.9 1
Thionazin ND ug/L 06/14/17 18:56 297-97-206/07/17 17:1020.0 1.7 1
O-Toluidine ND ug/L 06/14/17 18:56 95-53-406/07/17 17:1010.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 06/14/17 18:56 95-95-406/07/17 17:1010.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/14/17 18:56 88-06-206/07/17 17:1010.0 1.4 1
1,3,5-Trinitrobenzene ND ug/L 06/14/17 18:56 99-35-406/07/17 17:1010.0 1.2 1
Surrogates
Nitrobenzene-d5 (S)67 %06/14/17 18:56 4165-60-006/07/17 17:1021-110 1
2-Fluorobiphenyl (S)82 %06/14/17 18:56 321-60-806/07/17 17:1027-110 1
Terphenyl-d14 (S)75 %06/14/17 18:56 1718-51-006/07/17 17:1031-107 1
Phenol-d6 (S)22 %06/14/17 18:56 13127-88-306/07/17 17:1010-110 1
2-Fluorophenol (S)36 %06/14/17 18:56 367-12-406/07/17 17:1012-110 1
2,4,6-Tribromophenol (S)78 %06/14/17 18:56 118-79-606/07/17 17:1027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 21.4J ug/L 06/04/17 15:36 67-64-110010.0 1
Acetonitrile ND ug/L 06/04/17 15:36 75-05-855.0 2.2 1
Acrolein ND ug/L 06/04/17 15:36 107-02-853.0 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Sample:MW-11 Lab ID:92342784003 Collected:06/01/17 12:02 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acrylonitrile ND ug/L 06/04/17 15:36 107-13-12001.9 1
Allyl chloride 8.2J ug/L 06/04/17 15:36 107-05-110.0 1.5 1
Benzene 0.62J ug/L 06/04/17 15:36 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 15:36 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 15:36 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 15:36 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 15:36 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 15:36 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 15:36 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 15:36 56-23-51.0 0.25 1
Chlorobenzene 0.87J ug/L 06/04/17 15:36 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 15:36 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 15:36 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/17 15:36 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/04/17 15:36 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 15:36 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 15:36 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 15:36 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 15:36 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 15:36 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/04/17 15:36 541-73-15.0 0.24 1
1,4-Dichlorobenzene 2.5 ug/L 06/04/17 15:36 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 15:36 110-57-6 L11001.0 1
Dichlorodifluoromethane ND ug/L 06/04/17 15:36 75-71-85.0 0.21 1
1,1-Dichloroethane 0.37J ug/L 06/04/17 15:36 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 15:36 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 15:36 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 1.0J ug/L 06/04/17 15:36 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 15:36 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 15:36 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/04/17 15:36 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/04/17 15:36 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/04/17 15:36 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/04/17 15:36 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 15:36 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 15:36 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/04/17 15:36 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/04/17 15:36 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/04/17 15:36 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 15:36 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/04/17 15:36 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/04/17 15:36 126-98-71000.93 1
Methylene Chloride ND ug/L 06/04/17 15:36 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/04/17 15:36 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 15:36 108-10-11000.33 1
Naphthalene ND ug/L 06/04/17 15:36 91-20-310.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Sample:MW-11 Lab ID:92342784003 Collected:06/01/17 12:02 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Propionitrile ND ug/L 06/04/17 15:36 107-12-01503.6 1
Styrene ND ug/L 06/04/17 15:36 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 15:36 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 15:36 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 15:36 127-18-41.0 0.46 1
Toluene 0.88J ug/L 06/04/17 15:36 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/04/17 15:36 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/04/17 15:36 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 15:36 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 15:36 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 15:36 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 15:36 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 15:36 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 15:36 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/17 15:36 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %06/04/17 15:36 460-00-470-130 1
1,2-Dichloroethane-d4 (S)90 %06/04/17 15:36 17060-07-070-130 1
Toluene-d8 (S)108 %06/04/17 15:36 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/06/17 21:30 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/14/17 11:46 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Sample:SCALE HOUSE Lab ID:92342784004 Collected:06/01/17 16:22 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/06/17 12:34 309-00-206/05/17 17:300.050 0.050 1
alpha-BHC ND ug/L 06/06/17 12:34 319-84-606/05/17 17:300.050 0.050 1
beta-BHC ND ug/L 06/06/17 12:34 319-85-706/05/17 17:300.050 0.050 1
delta-BHC ND ug/L 06/06/17 12:34 319-86-806/05/17 17:300.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/06/17 12:34 58-89-906/05/17 17:300.050 0.050 1
Chlordane (Technical)ND ug/L 06/06/17 12:34 57-74-906/05/17 17:300.50 0.20 1
4,4'-DDD ND ug/L 06/06/17 12:34 72-54-806/05/17 17:300.10 0.050 1
4,4'-DDE ND ug/L 06/06/17 12:34 72-55-906/05/17 17:300.10 0.050 1
4,4'-DDT ND ug/L 06/06/17 12:34 50-29-306/05/17 17:300.10 0.050 1
Dieldrin ND ug/L 06/06/17 12:34 60-57-106/05/17 17:300.075 0.050 1
Endosulfan I ND ug/L 06/06/17 12:34 959-98-806/05/17 17:300.10 0.050 1
Endosulfan II ND ug/L 06/06/17 12:34 33213-65-906/05/17 17:300.10 0.050 1
Endosulfan sulfate ND ug/L 06/06/17 12:34 1031-07-806/05/17 17:300.10 0.050 1
Endrin ND ug/L 06/06/17 12:34 72-20-806/05/17 17:300.10 0.050 1
Endrin aldehyde ND ug/L 06/06/17 12:34 7421-93-406/05/17 17:300.10 0.050 1
Heptachlor ND ug/L 06/06/17 12:34 76-44-806/05/17 17:300.050 0.050 1
Heptachlor epoxide ND ug/L 06/06/17 12:34 1024-57-306/05/17 17:300.075 0.050 1
Methoxychlor ND ug/L 06/06/17 12:34 72-43-506/05/17 17:301.0 0.15 1
Toxaphene ND ug/L 06/06/17 12:34 8001-35-206/05/17 17:301.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)76 %06/06/17 12:34 877-09-806/05/17 17:3020-130 1
Decachlorobiphenyl (S)82 %06/06/17 12:34 2051-24-306/05/17 17:3020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/06/17 19:08 12674-11-206/05/17 17:300.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/06/17 19:08 11104-28-206/05/17 17:300.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/06/17 19:08 11141-16-506/05/17 17:300.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/06/17 19:08 53469-21-906/05/17 17:300.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/06/17 19:08 12672-29-606/05/17 17:300.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/06/17 19:08 11097-69-106/05/17 17:300.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/06/17 19:08 11096-82-506/05/17 17:300.50 0.50 1
Surrogates
Decachlorobiphenyl (S)78 %06/06/17 19:08 2051-24-306/05/17 17:3010-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/10/17 06:06 94-75-706/07/17 16:000.98 0.23 1
Dinoseb ND ug/L 06/10/17 06:06 88-85-706/07/17 16:000.20 0.059 1
Pentachlorophenol ND ug/L 06/10/17 06:06 87-86-506/07/17 16:000.030 0.018 1
2,4,5-T ND ug/L 06/10/17 06:06 93-76-506/07/17 16:000.20 0.044 1
2,4,5-TP (Silvex)ND ug/L 06/10/17 06:06 93-72-106/07/17 16:000.20 0.051 1
Surrogates
2,4-DCAA (S)90 %06/10/17 06:06 19719-28-906/07/17 16:0039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/14/17 22:40 7440-36-006/04/17 16:406.0 3.9 1
Arsenic ND ug/L 06/14/17 22:40 7440-38-206/04/17 16:4010.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Sample:SCALE HOUSE Lab ID:92342784004 Collected:06/01/17 16:22 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Barium 14.4J ug/L 06/14/17 22:40 7440-39-306/04/17 16:401002.5 1
Beryllium ND ug/L 06/14/17 22:40 7440-41-706/04/17 16:401.0 0.50 1
Cadmium ND ug/L 06/14/17 22:40 7440-43-906/04/17 16:401.0 0.50 1
Chromium ND ug/L 06/14/17 22:40 7440-47-306/04/17 16:4010.0 2.5 1
Cobalt ND ug/L 06/14/17 22:40 7440-48-406/04/17 16:4010.0 2.5 1
Copper ND ug/L 06/14/17 22:40 7440-50-806/04/17 16:4010.0 2.5 1
Lead ND ug/L 06/14/17 22:40 7439-92-106/04/17 16:4010.0 2.5 1
Nickel ND ug/L 06/14/17 22:40 7440-02-006/04/17 16:4050.0 2.5 1
Selenium ND ug/L 06/14/17 22:40 7782-49-206/04/17 16:4010.0 5.0 1
Silver ND ug/L 06/14/17 22:40 7440-22-406/04/17 16:4010.0 2.5 1
Tin ND ug/L 06/14/17 22:40 7440-31-506/04/17 16:401002.5 1
Vanadium ND ug/L 06/14/17 22:40 7440-62-206/04/17 16:4025.0 2.5 1
Zinc 16.0 ug/L 06/14/17 22:40 7440-66-606/04/17 16:4010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/09/17 16:28 7440-28-006/03/17 02:255.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 03:14 7439-97-606/04/17 20:450.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/14/17 19:25 83-32-906/07/17 17:1010.0 1.6 1
Acenaphthylene ND ug/L 06/14/17 19:25 208-96-806/07/17 17:1010.0 1.5 1
Acetophenone ND ug/L 06/14/17 19:25 98-86-206/07/17 17:1010.0 1.9 1
2-Acetylaminofluorene ND ug/L 06/14/17 19:25 53-96-3 L206/07/17 17:1020.0 1.6 1
4-Aminobiphenyl ND ug/L 06/14/17 19:25 92-67-106/07/17 17:1020.0 1.7 1
Anthracene ND ug/L 06/14/17 19:25 120-12-706/07/17 17:1010.0 1.7 1
Benzo(a)anthracene ND ug/L 06/14/17 19:25 56-55-306/07/17 17:1010.0 2.1 1
Benzo(a)pyrene ND ug/L 06/14/17 19:25 50-32-806/07/17 17:1010.0 2.2 1
Benzo(b)fluoranthene ND ug/L 06/14/17 19:25 205-99-206/07/17 17:1010.0 2.2 1
Benzo(g,h,i)perylene ND ug/L 06/14/17 19:25 191-24-206/07/17 17:1010.0 2.1 1
Benzo(k)fluoranthene ND ug/L 06/14/17 19:25 207-08-906/07/17 17:1010.0 2.0 1
Benzyl alcohol ND ug/L 06/14/17 19:25 100-51-606/07/17 17:1020.0 3.1 1
4-Bromophenylphenyl ether ND ug/L 06/14/17 19:25 101-55-306/07/17 17:1010.0 1.5 1
Butylbenzylphthalate ND ug/L 06/14/17 19:25 85-68-706/07/17 17:1010.0 2.5 1
4-Chloro-3-methylphenol ND ug/L 06/14/17 19:25 59-50-706/07/17 17:1020.0 2.8 1
4-Chloroaniline ND ug/L 06/14/17 19:25 106-47-806/07/17 17:1020.0 2.8 1
Chlorobenzilate ND ug/L 06/14/17 19:25 510-15-606/07/17 17:1010.0 2.2 1
bis(2-Chloroethoxy)methane ND ug/L 06/14/17 19:25 111-91-106/07/17 17:1010.0 1.6 1
bis(2-Chloroethyl) ether ND ug/L 06/14/17 19:25 111-44-406/07/17 17:1010.0 1.7 1
2-Chloronaphthalene ND ug/L 06/14/17 19:25 91-58-706/07/17 17:1010.0 1.6 1
2-Chlorophenol ND ug/L 06/14/17 19:25 95-57-806/07/17 17:1010.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/14/17 19:25 7005-72-306/07/17 17:1010.0 1.6 1
Chrysene ND ug/L 06/14/17 19:25 218-01-906/07/17 17:1010.0 2.1 1
Diallate ND ug/L 06/14/17 19:25 2303-16-406/07/17 17:1010.0 1.6 1
Dibenz(a,h)anthracene ND ug/L 06/14/17 19:25 53-70-306/07/17 17:1010.0 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Sample:SCALE HOUSE Lab ID:92342784004 Collected:06/01/17 16:22 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Dibenzofuran ND ug/L 06/14/17 19:25 132-64-906/07/17 17:1010.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 06/14/17 19:25 91-94-106/07/17 17:1020.0 3.9 1
2,4-Dichlorophenol ND ug/L 06/14/17 19:25 120-83-206/07/17 17:1010.0 1.6 1
2,6-Dichlorophenol ND ug/L 06/14/17 19:25 87-65-006/07/17 17:1010.0 1.5 1
Diethylphthalate ND ug/L 06/14/17 19:25 84-66-206/07/17 17:1060001.6 1
Dimethoate ND ug/L 06/14/17 19:25 60-51-506/07/17 17:1020.0 1.8 1
P-Dimethylaminoazobenzene ND ug/L 06/14/17 19:25 60-11-706/07/17 17:1010.0 1.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/14/17 19:25 57-97-606/07/17 17:1010.0 2.4 1
3,3'-Dimethylbenzidine ND ug/L 06/14/17 19:25 119-93-706/07/17 17:1010.0 3.9 1
2,4-Dimethylphenol ND ug/L 06/14/17 19:25 105-67-906/07/17 17:1010.0 1.6 1
Dimethylphthalate ND ug/L 06/14/17 19:25 131-11-306/07/17 17:1010.0 1.4 1
Di-n-butylphthalate ND ug/L 06/14/17 19:25 84-74-206/07/17 17:1010.0 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/14/17 19:25 534-52-106/07/17 17:1050.0 2.2 1
1,3-Dinitrobenzene ND ug/L 06/14/17 19:25 99-65-006/07/17 17:1020.0 1.3 1
2,4-Dinitrophenol ND ug/L 06/14/17 19:25 51-28-506/07/17 17:1050.0 5.1 1
2,4-Dinitrotoluene ND ug/L 06/14/17 19:25 121-14-206/07/17 17:1010.0 1.5 1
2,6-Dinitrotoluene ND ug/L 06/14/17 19:25 606-20-206/07/17 17:1010.0 1.4 1
Di-n-octylphthalate ND ug/L 06/14/17 19:25 117-84-006/07/17 17:1010.0 1.5 1
Diphenylamine ND ug/L 06/14/17 19:25 122-39-406/07/17 17:1010.0 1.4 1
Disulfoton ND ug/L 06/14/17 19:25 298-04-406/07/17 17:1010.0 1.5 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/14/17 19:25 117-81-706/07/17 17:1015.0 2.3 1
Ethyl methanesulfonate ND ug/L 06/14/17 19:25 62-50-006/07/17 17:1020.0 1.6 1
Famphur ND ug/L 06/14/17 19:25 52-85-706/07/17 17:1020.0 5.7 1
Fluoranthene ND ug/L 06/14/17 19:25 206-44-006/07/17 17:1010.0 2.2 1
Fluorene ND ug/L 06/14/17 19:25 86-73-706/07/17 17:1010.0 1.6 1
Hexachlorobenzene ND ug/L 06/14/17 19:25 118-74-106/07/17 17:1010.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 06/14/17 19:25 77-47-406/07/17 17:1010.0 1.3 1
Hexachloroethane ND ug/L 06/14/17 19:25 67-72-106/07/17 17:1010.0 1.8 1
Hexachloropropene ND ug/L 06/14/17 19:25 1888-71-706/07/17 17:1010.0 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/14/17 19:25 193-39-506/07/17 17:1010.0 2.0 1
Isodrin ND ug/L 06/14/17 19:25 465-73-606/07/17 17:1020.0 2.5 1
Isophorone ND ug/L 06/14/17 19:25 78-59-106/07/17 17:1010.0 1.5 1
Isosafrole ND ug/L 06/14/17 19:25 120-58-106/07/17 17:1010.0 1.5 1
Kepone ND ug/L 06/14/17 19:25 143-50-006/07/17 17:1020.0 4.5 1
Methapyrilene ND ug/L 06/14/17 19:25 91-80-506/07/17 17:101003.0 1
3-Methylcholanthrene ND ug/L 06/14/17 19:25 56-49-506/07/17 17:1010.0 2.7 1
Methyl methanesulfonate ND ug/L 06/14/17 19:25 66-27-306/07/17 17:1010.0 1.1 1
2-Methylnaphthalene ND ug/L 06/14/17 19:25 91-57-606/07/17 17:1010.0 1.4 1
Methyl parathion ND ug/L 06/14/17 19:25 298-00-006/07/17 17:1010.0 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 06/14/17 19:25 95-48-706/07/17 17:1010.0 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/14/17 19:25 15831-10-406/07/17 17:1010.0 1.4 1
1-Naphthalenamine ND ug/L 06/14/17 19:25 134-32-706/07/17 17:1010.0 1.3 1
2-Naphthalenamine ND ug/L 06/14/17 19:25 91-59-806/07/17 17:1010.0 2.2 1
1,4-Naphthoquinone ND ug/L 06/14/17 19:25 130-15-406/07/17 17:1010.0 0.99 1
2-Nitroaniline ND ug/L 06/14/17 19:25 88-74-406/07/17 17:1050.0 2.3 1
3-Nitroaniline ND ug/L 06/14/17 19:25 99-09-206/07/17 17:1050.0 2.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Sample:SCALE HOUSE Lab ID:92342784004 Collected:06/01/17 16:22 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Nitroaniline ND ug/L 06/14/17 19:25 100-01-606/07/17 17:1020.0 3.4 1
Nitrobenzene ND ug/L 06/14/17 19:25 98-95-306/07/17 17:1010.0 1.6 1
2-Nitrophenol ND ug/L 06/14/17 19:25 88-75-506/07/17 17:1010.0 1.6 1
4-Nitrophenol ND ug/L 06/14/17 19:25 100-02-706/07/17 17:1050.0 4.3 1
5-Nitro-o-toluidine ND ug/L 06/14/17 19:25 99-55-806/07/17 17:1010.0 1.9 1
N-Nitrosodiethylamine ND ug/L 06/14/17 19:25 55-18-506/07/17 17:1020.0 1.4 1
N-Nitrosodimethylamine ND ug/L 06/14/17 19:25 62-75-906/07/17 17:1010.0 1.6 1
N-Nitroso-di-n-butylamine ND ug/L 06/14/17 19:25 924-16-306/07/17 17:1010.0 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 06/14/17 19:25 621-64-706/07/17 17:1010.0 1.7 1
N-Nitrosodiphenylamine ND ug/L 06/14/17 19:25 86-30-606/07/17 17:1010.0 1.4 1
N-Nitrosomethylethylamine ND ug/L 06/14/17 19:25 10595-95-606/07/17 17:1010.0 1.4 1
N-Nitrosopiperidine ND ug/L 06/14/17 19:25 100-75-406/07/17 17:1020.0 1.7 1
N-Nitrosopyrrolidine ND ug/L 06/14/17 19:25 930-55-206/07/17 17:1010.0 1.7 1
O,O,O-Triethylphosphorothioate ND ug/L 06/14/17 19:25 126-68-106/07/17 17:1010.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/14/17 19:25 108-60-106/07/17 17:1010.0 1.8 1
Parathion (Ethyl parathion)ND ug/L 06/14/17 19:25 56-38-206/07/17 17:1010.0 1.5 1
Pentachlorobenzene ND ug/L 06/14/17 19:25 608-93-506/07/17 17:1010.0 1.5 1
Pentachloronitrobenzene ND ug/L 06/14/17 19:25 82-68-806/07/17 17:1020.0 1.7 1
Pentachlorophenol ND ug/L 06/14/17 19:25 87-86-506/07/17 17:1025.0 3.5 1
Phenacetin ND ug/L 06/14/17 19:25 62-44-206/07/17 17:1020.0 1.9 1
Phenanthrene ND ug/L 06/14/17 19:25 85-01-806/07/17 17:1010.0 1.6 1
Phenol ND ug/L 06/14/17 19:25 108-95-206/07/17 17:1010.0 1.3 1
p-Phenylenediamine ND ug/L 06/14/17 19:25 106-50-306/07/17 17:1010.0 2.2 1
Phorate ND ug/L 06/14/17 19:25 298-02-206/07/17 17:1010.0 1.7 1
Pronamide ND ug/L 06/14/17 19:25 23950-58-506/07/17 17:1010.0 2.0 1
Pyrene ND ug/L 06/14/17 19:25 129-00-006/07/17 17:1010.0 2.2 1
Safrole ND ug/L 06/14/17 19:25 94-59-706/07/17 17:1010.0 1.3 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/14/17 19:25 95-94-306/07/17 17:1010.0 1.3 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/14/17 19:25 58-90-206/07/17 17:1010.0 2.9 1
Thionazin ND ug/L 06/14/17 19:25 297-97-206/07/17 17:1020.0 1.7 1
O-Toluidine ND ug/L 06/14/17 19:25 95-53-406/07/17 17:1010.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 06/14/17 19:25 95-95-406/07/17 17:1010.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/14/17 19:25 88-06-206/07/17 17:1010.0 1.4 1
1,3,5-Trinitrobenzene ND ug/L 06/14/17 19:25 99-35-406/07/17 17:1010.0 1.2 1
Surrogates
Nitrobenzene-d5 (S)82 %06/14/17 19:25 4165-60-006/07/17 17:1021-110 1
2-Fluorobiphenyl (S)97 %06/14/17 19:25 321-60-806/07/17 17:1027-110 1
Terphenyl-d14 (S)89 %06/14/17 19:25 1718-51-006/07/17 17:1031-107 1
Phenol-d6 (S)28 %06/14/17 19:25 13127-88-306/07/17 17:1010-110 1
2-Fluorophenol (S)43 %06/14/17 19:25 367-12-406/07/17 17:1012-110 1
2,4,6-Tribromophenol (S)90 %06/14/17 19:25 118-79-606/07/17 17:1027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 12.9J ug/L 06/04/17 15:53 67-64-110010.0 1
Acetonitrile ND ug/L 06/04/17 15:53 75-05-855.0 2.2 1
Acrolein ND ug/L 06/04/17 15:53 107-02-8 M153.0 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Sample:SCALE HOUSE Lab ID:92342784004 Collected:06/01/17 16:22 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acrylonitrile ND ug/L 06/04/17 15:53 107-13-12001.9 1
Allyl chloride 4.1J ug/L 06/04/17 15:53 107-05-110.0 1.5 1
Benzene ND ug/L 06/04/17 15:53 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 15:53 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 15:53 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 15:53 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 15:53 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 15:53 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 15:53 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 15:53 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/17 15:53 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 15:53 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 15:53 67-66-35.0 0.14 1
Chloromethane 0.14J ug/L 06/04/17 15:53 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/04/17 15:53 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 15:53 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 15:53 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 15:53 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 15:53 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 15:53 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/04/17 15:53 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/04/17 15:53 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 15:53 110-57-6 L11001.0 1
Dichlorodifluoromethane ND ug/L 06/04/17 15:53 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/04/17 15:53 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 15:53 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 15:53 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.22J ug/L 06/04/17 15:53 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 15:53 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 15:53 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/04/17 15:53 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/04/17 15:53 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/04/17 15:53 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/04/17 15:53 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 15:53 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 15:53 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/04/17 15:53 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/04/17 15:53 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/04/17 15:53 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 15:53 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/04/17 15:53 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/04/17 15:53 126-98-71000.93 1
Methylene Chloride ND ug/L 06/04/17 15:53 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/04/17 15:53 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 15:53 108-10-11000.33 1
Naphthalene ND ug/L 06/04/17 15:53 91-20-310.0 0.24 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
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Page 19 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Sample:SCALE HOUSE Lab ID:92342784004 Collected:06/01/17 16:22 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Propionitrile ND ug/L 06/04/17 15:53 107-12-01503.6 1
Styrene ND ug/L 06/04/17 15:53 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 15:53 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 15:53 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 15:53 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 15:53 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/04/17 15:53 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/04/17 15:53 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 15:53 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 15:53 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 15:53 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 15:53 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 15:53 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 15:53 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/17 15:53 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %06/04/17 15:53 460-00-470-130 1
1,2-Dichloroethane-d4 (S)88 %06/04/17 15:53 17060-07-070-130 1
Toluene-d8 (S)108 %06/04/17 15:53 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/06/17 21:30 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/14/17 11:47 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
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[phone]
Page 20 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363333
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92342784003, 92342784004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014275
Associated Lab Samples:92342784003, 92342784004
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 06/07/17 02:150.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014276LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.32.5 93 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014277MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342769001
2014278
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L M1125075-1250 25125NDNDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363321
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92342784001, 92342784002, 92342784003, 92342784004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014222
Associated Lab Samples:92342784001, 92342784002, 92342784003, 92342784004
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 5.0 06/14/17 21:193.9
Arsenic ug/L ND 10.0 06/14/17 21:195.0
Barium ug/L ND 5.0 06/14/17 21:192.5
Beryllium ug/L ND 1.0 06/14/17 21:190.50
Cadmium ug/L ND 1.0 06/14/17 21:190.50
Chromium ug/L ND 5.0 06/14/17 21:192.5
Cobalt ug/L ND 5.0 06/14/17 21:192.5
Copper ug/L ND 5.0 06/14/17 21:192.5
Lead ug/L ND 5.0 06/14/17 21:192.5
Nickel ug/L ND 5.0 06/14/17 21:192.5
Selenium ug/L ND 10.0 06/14/17 21:195.0
Silver ug/L ND 5.0 06/14/17 21:192.5
Tin ug/L ND 5.0 06/14/17 21:192.5
Vanadium ug/L ND 5.0 06/14/17 21:192.5
Zinc ug/L ND 10.0 06/14/17 21:195.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014223LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 496500 99 80-120
Arsenic ug/L 475500 95 80-120
Barium ug/L 511500 102 80-120
Beryllium ug/L 457500 91 80-120
Cadmium ug/L 512500 102 80-120
Chromium ug/L 463500 93 80-120
Cobalt ug/L 498500 100 80-120
Copper ug/L 494500 99 80-120
Lead ug/L 486500 97 80-120
Nickel ug/L 463500 93 80-120
Selenium ug/L 501500 100 80-120
Silver ug/L 235250 94 80-120
Tin ug/L 485500 97 80-120
Vanadium ug/L 456500 91 80-120
Zinc ug/L 472500 94 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014224MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342605016
2014225
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 103 75-125100 3 20500ND517501
Arsenic ug/L 500 100 75-12597 2 20500174672657
Barium ug/L 500 108 75-125104 3 205008.0 546 530
Beryllium ug/L 500 96 75-12594 2 205000.73J 481 471
Cadmium ug/L 500 108 75-125105 3 205001.7 540 524
Chromium ug/L 500 97 75-12594 3 20500ND486470
Cobalt ug/L 500 104 75-125100 3 2050075.0 594 577
Copper ug/L 500 104 75-125102 3 20500ND522509
Lead ug/L 500 100 75-12597 3 205004.4J 506 491
Nickel ug/L 500 96 75-12593 3 205003.2J 481 466
Selenium ug/L 500 102 75-125100 2 20500ND511501
Silver ug/L 250 99 75-12595 4 20250ND246238
Tin ug/L 500 101 75-12597 4 20500ND503484
Vanadium ug/L 500 96 75-12593 3 20500ND482466
Zinc ug/L 500 98 75-12595 3 205005.8J 495 479
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363273
EPA 3010A
EPA 6020B
6020 MET
Associated Lab Samples:92342784003, 92342784004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014038
Associated Lab Samples:92342784003, 92342784004
Matrix:Water
AnalyzedMDL
Thallium ug/L ND 0.10 06/09/17 16:010.020
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014039LABORATORY CONTROL SAMPLE:
LCSSpike
Thallium ug/L 91.8100 92 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014040MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342600010
2014041
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Thallium ug/L 100 91 75-12593 3 20100ND90.7 93.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363479
EPA 3010A
EPA 6020B
6020 MET
Associated Lab Samples:92342784001, 92342784002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2015143
Associated Lab Samples:92342784001, 92342784002
Matrix:Water
AnalyzedMDL
Thallium ug/L ND 0.10 06/09/17 20:050.020
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2015144LABORATORY CONTROL SAMPLE:
LCSSpike
Thallium ug/L 93.7100 94 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015145MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342730002
2015146
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Thallium ug/L 100 94 75-12595 0 201000.048J 94.4 94.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363311
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92342784001, 92342784002, 92342784003, 92342784004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014186
Associated Lab Samples:92342784001, 92342784002, 92342784003, 92342784004
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/04/17 06:590.33
1,1,1-Trichloroethane ug/L ND 1.0 06/04/17 06:590.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 06/04/17 06:590.40
1,1,2-Trichloroethane ug/L ND 1.0 06/04/17 06:590.29
1,1-Dichloroethane ug/L ND 5.0 06/04/17 06:590.32
1,1-Dichloroethene ug/L ND 5.0 06/04/17 06:590.56
1,1-Dichloropropene ug/L ND 5.0 06/04/17 06:590.49
1,2,3-Trichloropropane ug/L ND 1.0 06/04/17 06:590.41
1,2,4-Trichlorobenzene ug/L ND 10.0 06/04/17 06:590.35
1,2-Dibromo-3-chloropropane ug/L ND 13.0 06/04/17 06:592.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/04/17 06:590.27
1,2-Dichlorobenzene ug/L ND 5.0 06/04/17 06:590.30
1,2-Dichloroethane ug/L ND 1.0 06/04/17 06:590.24
1,2-Dichloropropane ug/L ND 1.0 06/04/17 06:590.27
1,3-Dichlorobenzene ug/L ND 5.0 06/04/17 06:590.24
1,3-Dichloropropane ug/L ND 1.0 06/04/17 06:590.28
1,4-Dichlorobenzene ug/L ND 1.0 06/04/17 06:590.33
2,2-Dichloropropane ug/L ND 15.0 06/04/17 06:590.13
2-Butanone (MEK)ug/L ND 100 06/04/17 06:590.96
2-Hexanone ug/L ND 50.0 06/04/17 06:590.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 06/04/17 06:590.33
Acetone ug/L ND 100 06/04/17 06:5910.0
Acetonitrile ug/L ND 55.0 06/04/17 06:592.2
Acrolein ug/L ND 53.0 06/04/17 06:591.6
Acrylonitrile ug/L ND 200 06/04/17 06:591.9
Allyl chloride ug/L ND 10.0 06/04/17 06:591.5
Benzene ug/L ND 1.0 06/04/17 06:590.25
Bromochloromethane ug/L ND 3.0 06/04/17 06:590.17
Bromodichloromethane ug/L ND 1.0 06/04/17 06:590.18
Bromoform ug/L ND 3.0 06/04/17 06:590.26
Bromomethane ug/L ND 10.0 06/04/17 06:590.29
Carbon disulfide ug/L ND 100 06/04/17 06:591.2
Carbon tetrachloride ug/L ND 1.0 06/04/17 06:590.25
Chlorobenzene ug/L ND 3.0 06/04/17 06:590.23
Chloroethane ug/L ND 10.0 06/04/17 06:590.54
Chloroform ug/L ND 5.0 06/04/17 06:590.14
Chloromethane ug/L ND 1.0 06/04/17 06:590.11
Chloroprene ug/L ND 20.0 06/04/17 06:590.27
cis-1,2-Dichloroethene ug/L ND 5.0 06/04/17 06:590.19
cis-1,3-Dichloropropene ug/L ND 1.0 06/04/17 06:590.13
Dibromochloromethane ug/L ND 3.0 06/04/17 06:590.21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014186
Associated Lab Samples:92342784001, 92342784002, 92342784003, 92342784004
Matrix:Water
AnalyzedMDL
Dibromomethane ug/L ND 10.0 06/04/17 06:590.21
Dichlorodifluoromethane ug/L ND 5.0 06/04/17 06:590.21
Ethyl methacrylate ug/L ND 10.0 06/04/17 06:590.20
Ethylbenzene ug/L ND 1.0 06/04/17 06:590.30
Hexachloro-1,3-butadiene ug/L ND 10.0 06/04/17 06:590.71
Iodomethane ug/L ND 10.0 06/04/17 06:590.32
Isobutanol ug/L ND 100 06/04/17 06:5935.0
Methacrylonitrile ug/L ND 100 06/04/17 06:590.93
Methyl methacrylate ug/L ND 30.0 06/04/17 06:592.0
Methylene Chloride ug/L ND 1.0 06/04/17 06:590.97
Naphthalene ug/L ND 10.0 06/04/17 06:590.24
Propionitrile ug/L ND 150 06/04/17 06:593.6
Styrene ug/L ND 1.0 06/04/17 06:590.26
Tetrachloroethene ug/L ND 1.0 06/04/17 06:590.46
Toluene ug/L ND 1.0 06/04/17 06:590.26
trans-1,2-Dichloroethene ug/L ND 5.0 06/04/17 06:590.49
trans-1,3-Dichloropropene ug/L ND 1.0 06/04/17 06:590.26
trans-1,4-Dichloro-2-butene ug/L ND 100 06/04/17 06:591.0
Trichloroethene ug/L ND 1.0 06/04/17 06:590.47
Trichlorofluoromethane ug/L ND 1.0 06/04/17 06:590.20
Vinyl acetate ug/L ND 50.0 06/04/17 06:590.35
Vinyl chloride ug/L ND 1.0 06/04/17 06:590.62
Xylene (Total)ug/L ND 5.0 06/04/17 06:590.66
1,2-Dichloroethane-d4 (S)%89 70-130 06/04/17 06:59
4-Bromofluorobenzene (S)%99 70-130 06/04/17 06:59
Toluene-d8 (S)%106 70-130 06/04/17 06:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014187LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.750 99 80-125
1,1,1-Trichloroethane ug/L 50.850 102 71-129
1,1,2,2-Tetrachloroethane ug/L 53.150 106 79-124
1,1,2-Trichloroethane ug/L 51.550 103 85-125
1,1-Dichloroethane ug/L 52.350 105 73-126
1,1-Dichloroethene ug/L 51.650 103 66-135
1,1-Dichloropropene ug/L 50.150 100 74-135
1,2,3-Trichloropropane ug/L 47.050 94 75-130
1,2,4-Trichlorobenzene ug/L 43.750 87 75-134
1,2-Dibromo-3-chloropropane ug/L 47.350 95 71-133
1,2-Dibromoethane (EDB)ug/L 54.150 108 83-124
1,2-Dichlorobenzene ug/L 48.250 96 80-133
1,2-Dichloroethane ug/L 48.450 97 67-128
1,2-Dichloropropane ug/L 52.750 105 75-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
Page 27 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014187LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 47.950 96 77-130
1,3-Dichloropropane ug/L 55.150 110 76-131
1,4-Dichlorobenzene ug/L 45.650 91 78-130
2,2-Dichloropropane ug/L 46.450 93 40-160
2-Butanone (MEK)ug/L 138100 138 61-144
2-Hexanone ug/L 108100 108 68-143
4-Methyl-2-pentanone (MIBK)ug/L 107100 107 72-135
Acetone ug/L 123100 123 48-146
Acetonitrile ug/L 524500 105 62-150
Acrolein ug/L 339250 136 24-160
Acrylonitrile ug/L 286250 114 40-160
Allyl chloride ug/L 47.450 95 66-137
Benzene ug/L 52.550 105 80-125
Bromochloromethane ug/L 48.350 97 71-125
Bromodichloromethane ug/L 48.550 97 78-124
Bromoform ug/L 48.550 97 71-128
Bromomethane ug/L 44.850 90 40-160
Carbon disulfide ug/L 52.8J50 106 50-160
Carbon tetrachloride ug/L 44.250 88 69-131
Chlorobenzene ug/L 49.950 100 81-122
Chloroethane ug/L 43.650 87 39-148
Chloroform ug/L 52.250 104 73-127
Chloromethane ug/L 58.150 116 44-146
Chloroprene ug/L 49.150 98 75-145
cis-1,2-Dichloroethene ug/L 54.050 108 74-124
cis-1,3-Dichloropropene ug/L 52.450 105 72-132
Dibromochloromethane ug/L 48.750 97 78-125
Dibromomethane ug/L 46.050 92 82-120
Dichlorodifluoromethane ug/L 45.450 91 34-157
Ethyl methacrylate ug/L 48.250 96 82-121
Ethylbenzene ug/L 48.050 96 79-121
Hexachloro-1,3-butadiene ug/L 46.050 92 72-131
Iodomethane ug/L 95.1100 95 39-154
Isobutanol ug/L 12601000 126 34-160
Methacrylonitrile ug/L 616500 123 74-134
Methyl methacrylate ug/L 46.950 94 84-124
Methylene Chloride ug/L 53.350 107 64-133
Naphthalene ug/L 51.150 102 73-133
Propionitrile ug/L 640500 128 73-140
Styrene ug/L 48.350 97 84-126
Tetrachloroethene ug/L 47.950 96 78-122
Toluene ug/L 48.350 97 80-121
trans-1,2-Dichloroethene ug/L 53.850 108 71-127
trans-1,3-Dichloropropene ug/L 51.450 103 69-141
trans-1,4-Dichloro-2-butene ug/L 99.7J L15019940-160
Trichloroethene ug/L 49.550 99 78-122
Trichlorofluoromethane ug/L 46.550 93 53-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
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[phone]
Page 28 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014187LABORATORY CONTROL SAMPLE:
LCSSpike
Vinyl acetate ug/L 103100 103 40-160
Vinyl chloride ug/L 46.950 94 58-137
Xylene (Total)ug/L 141150 94 81-126
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%95 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2014189MATRIX SPIKE SAMPLE:
MSSpike
Result
92342784004
1,1,1,2-Tetrachloroethane ug/L 19.220 96 70-130ND
1,1,1-Trichloroethane ug/L 22.820 114 70-130ND
1,1,2,2-Tetrachloroethane ug/L 21.320 106 70-130ND
1,1,2-Trichloroethane ug/L 21.120 105 70-130ND
1,1-Dichloroethane ug/L 24.120 120 70-130ND
1,1-Dichloroethene ug/L 24.120 120 70-166ND
1,1-Dichloropropene ug/L 23.320 116 70-130ND
1,2,3-Trichloropropane ug/L 20.320 102 70-130ND
1,2,4-Trichlorobenzene ug/L 23.520 118 70-130ND
1,2-Dibromo-3-chloropropane ug/L 19.720 99 70-130ND
1,2-Dibromoethane (EDB)ug/L 20.620 103 70-130ND
1,2-Dichlorobenzene ug/L 22.020 110 70-130ND
1,2-Dichloroethane ug/L 20.720 104 70-130ND
1,2-Dichloropropane ug/L 22.820 114 70-130ND
1,3-Dichlorobenzene ug/L 23.320 117 70-130ND
1,3-Dichloropropane ug/L 21.520 107 70-130ND
1,4-Dichlorobenzene ug/L 21.820 109 70-130ND
2,2-Dichloropropane ug/L 22.820 114 70-130ND
2-Butanone (MEK)ug/L 46.8J40 117 70-130ND
2-Hexanone ug/L 41.2J40 103 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 42.3J40 106 70-130ND
Acetone ug/L 49.1J40 90 70-13012.9J
Acetonitrile ug/L 222200 111 70-130ND
Acrolein ug/L 132 M110013270-130ND
Acrylonitrile ug/L 111J100 111 70-130ND
Allyl chloride ug/L 23.620 98 70-1304.1J
Benzene ug/L 23.720 119 70-148ND
Bromochloromethane ug/L 21.920 109 70-130ND
Bromodichloromethane ug/L 22.420 112 70-130ND
Bromoform ug/L 17.720 88 70-130ND
Bromomethane ug/L 23.220 116 70-130ND
Carbon disulfide ug/L 24.5J20 123 70-130ND
Carbon tetrachloride ug/L 21.220 106 70-130ND
Chlorobenzene ug/L 22.520 112 70-146ND
Chloroethane ug/L 18.920 94 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2014189MATRIX SPIKE SAMPLE:
MSSpike
Result
92342784004
Chloroform ug/L 22.320 111 70-130ND
Chloromethane ug/L 24.420 121 70-1300.14J
Chloroprene ug/L 21.920 109 70-130ND
cis-1,2-Dichloroethene ug/L 24.820 123 70-1300.22J
cis-1,3-Dichloropropene ug/L 22.520 113 70-130ND
Dibromochloromethane ug/L 19.220 96 70-130ND
Dibromomethane ug/L 21.320 107 70-130ND
Dichlorodifluoromethane ug/L 20.220 101 70-130ND
Ethyl methacrylate ug/L 19.520 97 70-130ND
Ethylbenzene ug/L 22.220 111 70-130ND
Hexachloro-1,3-butadiene ug/L 23.520 118 70-130ND
Iodomethane ug/L 44.240 110 70-130ND
Isobutanol ug/L 475400 119 70-130ND
Methacrylonitrile ug/L 221200 111 70-130ND
Methyl methacrylate ug/L 19.8J20 99 70-130ND
Methylene Chloride ug/L 22.620 113 70-130ND
Naphthalene ug/L 24.520 123 70-130ND
Propionitrile ug/L 235200 118 70-130ND
Styrene ug/L 21.320 107 70-130ND
Tetrachloroethene ug/L 20.720 103 70-130ND
Toluene ug/L 22.220 111 70-155ND
trans-1,2-Dichloroethene ug/L 23.720 118 70-130ND
trans-1,3-Dichloropropene ug/L 22.020 110 70-130ND
trans-1,4-Dichloro-2-butene ug/L 24.7J20 124 70-130ND
Trichloroethene ug/L 23.520 117 69-151ND
Trichlorofluoromethane ug/L 22.520 112 70-130ND
Vinyl acetate ug/L 38.6J40 96 70-130ND
Vinyl chloride ug/L 21.520 107 70-130ND
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%94 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342784003
2014188SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 0.35J 300.37J
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342784003
2014188SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L 0.86J 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L 2.4 5 302.5
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L 13.9J 3021.4J
Acetonitrile ug/L ND 30ND
Acrolein ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Allyl chloride ug/L ND 308.2J
Benzene ug/L 0.52J 300.62J
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L 0.97J 300.87J
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L 0.11J 30ND
Chloroprene ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 1.0J 3 301.0J
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L 0.31J 30ND
Ethyl methacrylate ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Isobutanol ug/L ND 30ND
Methacrylonitrile ug/L ND 30ND
Methyl methacrylate ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
Propionitrile ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L 0.91J 300.88J
trans-1,2-Dichloroethene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342784003
2014188SAMPLE DUPLICATE:
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%90 090
4-Bromofluorobenzene (S)%98 299
Toluene-d8 (S)%105 3108
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363426
EPA 3510
EPA 8081
8081A GCS Pesticides
Associated Lab Samples:92342784003, 92342784004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014786
Associated Lab Samples:92342784003, 92342784004
Matrix:Water
AnalyzedMDL
4,4'-DDD ug/L ND 0.10 06/06/17 13:280.050
4,4'-DDE ug/L ND 0.10 06/06/17 13:280.050
4,4'-DDT ug/L ND 0.10 06/06/17 13:280.050
Aldrin ug/L ND 0.050 06/06/17 13:280.050
alpha-BHC ug/L ND 0.050 06/06/17 13:280.050
beta-BHC ug/L ND 0.050 06/06/17 13:280.050
Chlordane (Technical)ug/L ND 0.50 06/06/17 13:280.20
delta-BHC ug/L ND 0.050 06/06/17 13:280.050
Dieldrin ug/L ND 0.075 06/06/17 13:280.050
Endosulfan I ug/L ND 0.10 06/06/17 13:280.050
Endosulfan II ug/L ND 0.10 06/06/17 13:280.050
Endosulfan sulfate ug/L ND 0.10 06/06/17 13:280.050
Endrin ug/L ND 0.10 06/06/17 13:280.050
Endrin aldehyde ug/L ND 0.10 06/06/17 13:280.050
gamma-BHC (Lindane)ug/L ND 0.050 06/06/17 13:280.050
Heptachlor ug/L ND 0.050 06/06/17 13:280.050
Heptachlor epoxide ug/L ND 0.075 06/06/17 13:280.050
Methoxychlor ug/L ND 1.0 06/06/17 13:280.15
Toxaphene ug/L ND 1.5 06/06/17 13:280.20
Decachlorobiphenyl (S)%78 20-130 06/06/17 13:28
Tetrachloro-m-xylene (S)%51 20-130 06/06/17 13:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014787LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2014788
4,4'-DDD ug/L 0.22.25 90 20-150920.23 2 30
4,4'-DDE ug/L 0.21.25 84 20-150790.20 7 30
4,4'-DDT ug/L 0.23.25 94 20-150950.24 1 30
Aldrin ug/L 0.16.25 64 20-150600.15 8 30
alpha-BHC ug/L 0.19.25 79 20-150780.19 1 30
beta-BHC ug/L 0.17.25 70 20-150750.19 7 30
delta-BHC ug/L 0.21.25 84 20-150790.20 7 30
Dieldrin ug/L 0.21.25 86 20-150830.21 3 30
Endosulfan I ug/L 0.22.25 87 20-150840.21 3 30
Endosulfan II ug/L 0.23.25 91 20-150900.22 1 30
Endosulfan sulfate ug/L 0.24.25 97 20-150970.24 0 30
Endrin ug/L 0.23.25 93 20-150930.23 0 30
Endrin aldehyde ug/L 0.21.25 87 20-150890.22 3 30
gamma-BHC (Lindane)ug/L 0.21.25 83 20-150850.21 2 30
Heptachlor ug/L 0.17.25 68 20-150620.15 9 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014787LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2014788
Heptachlor epoxide ug/L 0.20.25 82 20-150700.17 16 30
Methoxychlor ug/L 0.72J.74 97 20-150970.72J 1 30
Decachlorobiphenyl (S)%78 20-13064
Tetrachloro-m-xylene (S)%81 20-13069
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363427
EPA 3510
EPA 8082
8082 GCS PCB
Associated Lab Samples:92342784003, 92342784004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014798
Associated Lab Samples:92342784003, 92342784004
Matrix:Water
AnalyzedMDL
PCB-1016 (Aroclor 1016)ug/L ND 0.50 06/06/17 20:100.50
PCB-1221 (Aroclor 1221)ug/L ND 0.50 06/06/17 20:100.50
PCB-1232 (Aroclor 1232)ug/L ND 0.50 06/06/17 20:100.50
PCB-1242 (Aroclor 1242)ug/L ND 0.50 06/06/17 20:100.50
PCB-1248 (Aroclor 1248)ug/L ND 0.50 06/06/17 20:100.50
PCB-1254 (Aroclor 1254)ug/L ND 0.50 06/06/17 20:100.50
PCB-1260 (Aroclor 1260)ug/L ND 0.50 06/06/17 20:100.50
Decachlorobiphenyl (S)%75 10-132 06/06/17 20:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014799LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2014800
PCB-1016 (Aroclor 1016)ug/L 3.35 66 50-150693.5 5 30
PCB-1260 (Aroclor 1260)ug/L 3.25 63 50-150603.0 5 30
Decachlorobiphenyl (S)%34 10-13237
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
373221
EPA 8151
EPA 8151
8151A GCS Herbicides
Associated Lab Samples:92342784003, 92342784004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2017562
Associated Lab Samples:92342784003, 92342784004
Matrix:Water
AnalyzedMDL
2,4,5-T ug/L ND 0.19 06/09/17 20:420.042
2,4,5-TP (Silvex)ug/L ND 0.19 06/09/17 20:420.049
2,4-D ug/L ND 0.94 06/09/17 20:420.22
Dinoseb ug/L ND 0.19 06/09/17 20:420.057
Pentachlorophenol ug/L ND 0.028 06/09/17 20:420.017
2,4-DCAA (S)%74 39-139 06/09/17 20:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2017563LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-T ug/L 1.31.2 109 37-133
2,4,5-TP (Silvex)ug/L 1.31.2 110 53-134
2,4-D ug/L 5.56 91 35-124
Dinoseb ug/L 1.21.2 99 13-116
Pentachlorophenol ug/L 0.17.18 94 39-170
2,4-DCAA (S)%85 39-139
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2018719MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35316294004
2018720
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,4,5-T ug/L 1.2 100 37-13390 3 401.40.043U 1.2 1.2
2,4,5-TP (Silvex)ug/L 1.2 97 53-13488 2 401.40.050U 1.2 1.2
2,4-D ug/L 6 84 35-12476 3 406.80.23U 5.1 5.2
Dinoseb ug/L 1.2 91 13-11672 11 401.40.058U 1.1 0.98
Pentachlorophenol ug/L M1,R1.18 82 39-17028 89 40.20.017U 0.15 0.057
2,4-DCAA (S)%69 39-13985 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
364049
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92342784003, 92342784004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2018678
Associated Lab Samples:92342784003, 92342784004
Matrix:Water
AnalyzedMDL
1,2,4,5-Tetrachlorobenzene ug/L ND 10.0 06/14/17 13:231.3
1,3,5-Trinitrobenzene ug/L ND 10.0 06/14/17 13:231.2
1,3-Dinitrobenzene ug/L ND 20.0 06/14/17 13:231.3
1,4-Naphthoquinone ug/L ND 10.0 06/14/17 13:230.99
1-Naphthalenamine ug/L ND 10.0 06/14/17 13:231.3
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 06/14/17 13:231.8
2,3,4,6-Tetrachlorophenol ug/L ND 10.0 06/14/17 13:232.9
2,4,5-Trichlorophenol ug/L ND 10.0 06/14/17 13:231.5
2,4,6-Trichlorophenol ug/L ND 10.0 06/14/17 13:231.4
2,4-Dichlorophenol ug/L ND 10.0 06/14/17 13:231.6
2,4-Dimethylphenol ug/L ND 10.0 06/14/17 13:231.6
2,4-Dinitrophenol ug/L ND 50.0 06/14/17 13:235.1
2,4-Dinitrotoluene ug/L ND 10.0 06/14/17 13:231.5
2,6-Dichlorophenol ug/L ND 10.0 06/14/17 13:231.5
2,6-Dinitrotoluene ug/L ND 10.0 06/14/17 13:231.4
2-Acetylaminofluorene ug/L ND 20.0 06/14/17 13:231.6
2-Chloronaphthalene ug/L ND 10.0 06/14/17 13:231.6
2-Chlorophenol ug/L ND 10.0 06/14/17 13:231.5
2-Methylnaphthalene ug/L ND 10.0 06/14/17 13:231.4
2-Methylphenol(o-Cresol)ug/L ND 10.0 06/14/17 13:231.6
2-Naphthalenamine ug/L ND 10.0 06/14/17 13:232.2
2-Nitroaniline ug/L ND 50.0 06/14/17 13:232.3
2-Nitrophenol ug/L ND 10.0 06/14/17 13:231.6
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 06/14/17 13:231.4
3,3'-Dichlorobenzidine ug/L ND 20.0 06/14/17 13:233.9
3,3'-Dimethylbenzidine ug/L ND 10.0 06/14/17 13:233.9
3-Methylcholanthrene ug/L ND 10.0 06/14/17 13:232.7
3-Nitroaniline ug/L ND 50.0 06/14/17 13:232.7
4,6-Dinitro-2-methylphenol ug/L ND 50.0 06/14/17 13:232.2
4-Aminobiphenyl ug/L ND 20.0 06/14/17 13:231.7
4-Bromophenylphenyl ether ug/L ND 10.0 06/14/17 13:231.5
4-Chloro-3-methylphenol ug/L ND 20.0 06/14/17 13:232.8
4-Chloroaniline ug/L ND 20.0 06/14/17 13:232.8
4-Chlorophenylphenyl ether ug/L ND 10.0 06/14/17 13:231.6
4-Nitroaniline ug/L ND 20.0 06/14/17 13:233.4
4-Nitrophenol ug/L ND 50.0 06/14/17 13:234.3
5-Nitro-o-toluidine ug/L ND 10.0 06/14/17 13:231.9
7,12-Dimethylbenz(a)anthracene ug/L ND 10.0 06/14/17 13:232.4
Acenaphthene ug/L ND 10.0 06/14/17 13:231.6
Acenaphthylene ug/L ND 10.0 06/14/17 13:231.5
Acetophenone ug/L ND 10.0 06/14/17 13:231.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2018678
Associated Lab Samples:92342784003, 92342784004
Matrix:Water
AnalyzedMDL
Anthracene ug/L ND 10.0 06/14/17 13:231.7
Benzo(a)anthracene ug/L ND 10.0 06/14/17 13:232.1
Benzo(a)pyrene ug/L ND 10.0 06/14/17 13:232.2
Benzo(b)fluoranthene ug/L ND 10.0 06/14/17 13:232.2
Benzo(g,h,i)perylene ug/L ND 10.0 06/14/17 13:232.1
Benzo(k)fluoranthene ug/L ND 10.0 06/14/17 13:232.0
Benzyl alcohol ug/L ND 20.0 06/14/17 13:233.1
bis(2-Chloroethoxy)methane ug/L ND 10.0 06/14/17 13:231.6
bis(2-Chloroethyl) ether ug/L ND 10.0 06/14/17 13:231.7
bis(2-Ethylhexyl)phthalate ug/L ND 15.0 06/14/17 13:232.3
Butylbenzylphthalate ug/L ND 10.0 06/14/17 13:232.5
Chlorobenzilate ug/L ND 10.0 06/14/17 13:232.2
Chrysene ug/L ND 10.0 06/14/17 13:232.1
Di-n-butylphthalate ug/L ND 10.0 06/14/17 13:232.0
Di-n-octylphthalate ug/L ND 10.0 06/14/17 13:231.5
Diallate ug/L ND 10.0 06/14/17 13:231.6
Dibenz(a,h)anthracene ug/L ND 10.0 06/14/17 13:232.0
Dibenzofuran ug/L ND 10.0 06/14/17 13:231.7
Diethylphthalate ug/L ND 6000 06/14/17 13:231.6
Dimethoate ug/L ND 20.0 06/14/17 13:231.8
Dimethylphthalate ug/L ND 10.0 06/14/17 13:231.4
Diphenylamine ug/L ND 10.0 06/14/17 13:231.4
Disulfoton ug/L ND 10.0 06/14/17 13:231.5
Ethyl methanesulfonate ug/L ND 20.0 06/14/17 13:231.6
Famphur ug/L ND 20.0 06/14/17 13:235.7
Fluoranthene ug/L ND 10.0 06/14/17 13:232.2
Fluorene ug/L ND 10.0 06/14/17 13:231.6
Hexachlorobenzene ug/L ND 10.0 06/14/17 13:231.7
Hexachlorocyclopentadiene ug/L ND 10.0 06/14/17 13:231.3
Hexachloroethane ug/L ND 10.0 06/14/17 13:231.8
Hexachloropropene ug/L ND 10.0 06/14/17 13:231.2
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 06/14/17 13:232.0
Isodrin ug/L ND 20.0 06/14/17 13:232.5
Isophorone ug/L ND 10.0 06/14/17 13:231.5
Isosafrole ug/L ND 10.0 06/14/17 13:231.5
Kepone ug/L ND 20.0 06/14/17 13:234.5
Methapyrilene ug/L ND 100 06/14/17 13:233.0
Methyl methanesulfonate ug/L ND 10.0 06/14/17 13:231.1
Methyl parathion ug/L ND 10.0 06/14/17 13:231.6
N-Nitroso-di-n-butylamine ug/L ND 10.0 06/14/17 13:231.6
N-Nitroso-di-n-propylamine ug/L ND 10.0 06/14/17 13:231.7
N-Nitrosodiethylamine ug/L ND 20.0 06/14/17 13:231.4
N-Nitrosodimethylamine ug/L ND 10.0 06/14/17 13:231.6
N-Nitrosodiphenylamine ug/L ND 10.0 06/14/17 13:231.4
N-Nitrosomethylethylamine ug/L ND 10.0 06/14/17 13:231.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2018678
Associated Lab Samples:92342784003, 92342784004
Matrix:Water
AnalyzedMDL
N-Nitrosopiperidine ug/L ND 20.0 06/14/17 13:231.7
N-Nitrosopyrrolidine ug/L ND 10.0 06/14/17 13:231.7
Nitrobenzene ug/L ND 10.0 06/14/17 13:231.6
O,O,O-Triethylphosphorothioate ug/L ND 10.0 06/14/17 13:231.7
O-Toluidine ug/L ND 10.0 06/14/17 13:231.7
P-Dimethylaminoazobenzene ug/L ND 10.0 06/14/17 13:231.0
p-Phenylenediamine ug/L ND 10.0 06/14/17 13:232.2
Parathion (Ethyl parathion)ug/L ND 10.0 06/14/17 13:231.5
Pentachlorobenzene ug/L ND 10.0 06/14/17 13:231.5
Pentachloronitrobenzene ug/L ND 20.0 06/14/17 13:231.7
Pentachlorophenol ug/L ND 25.0 06/14/17 13:233.5
Phenacetin ug/L ND 20.0 06/14/17 13:231.9
Phenanthrene ug/L ND 10.0 06/14/17 13:231.6
Phenol ug/L ND 10.0 06/14/17 13:231.3
Phorate ug/L ND 10.0 06/14/17 13:231.7
Pronamide ug/L ND 10.0 06/14/17 13:232.0
Pyrene ug/L ND 10.0 06/14/17 13:232.2
Safrole ug/L ND 10.0 06/14/17 13:231.3
Thionazin ug/L ND 20.0 06/14/17 13:231.7
2,4,6-Tribromophenol (S)%74 27-110 06/14/17 13:23
2-Fluorobiphenyl (S)%77 27-110 06/14/17 13:23
2-Fluorophenol (S)%37 12-110 06/14/17 13:23
Nitrobenzene-d5 (S)%62 21-110 06/14/17 13:23
Phenol-d6 (S)%25 10-110 06/14/17 13:23
Terphenyl-d14 (S)%87 31-107 06/14/17 13:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2018679LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4,5-Tetrachlorobenzene ug/L 34.450 69 16-129
1,3,5-Trinitrobenzene ug/L 32.650 65 55-125
1,3-Dinitrobenzene ug/L 42.550 85 30-122
1,4-Naphthoquinone ug/L 41.850 84 31-120
1-Naphthalenamine ug/L 27.050 54 37-126
2,2'-Oxybis(1-chloropropane)ug/L 52.950 106 18-120
2,3,4,6-Tetrachlorophenol ug/L 82.350 165 54-276
2,4,5-Trichlorophenol ug/L 43.150 86 43-113
2,4,6-Trichlorophenol ug/L 50.850 102 42-120
2,4-Dichlorophenol ug/L 42.750 85 30-120
2,4-Dimethylphenol ug/L 37.950 76 29-111
2,4-Dinitrophenol ug/L 246250 98 19-132
2,4-Dinitrotoluene ug/L 45.150 90 58-128
2,6-Dichlorophenol ug/L 43.650 87 54-128
2,6-Dinitrotoluene ug/L 47.050 94 54-129
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2018679LABORATORY CONTROL SAMPLE:
LCSSpike
2-Acetylaminofluorene ug/L 38.7 L2507781-160
2-Chloronaphthalene ug/L 53.050 106 43-117
2-Chlorophenol ug/L 41.950 84 37-120
2-Methylnaphthalene ug/L 37.650 75 33-120
2-Methylphenol(o-Cresol)ug/L 34.350 69 31-120
2-Naphthalenamine ug/L 34.150 68 41-136
2-Nitroaniline ug/L 88.7100 89 48-121
2-Nitrophenol ug/L 40.750 81 25-116
3&4-Methylphenol(m&p Cresol)ug/L 29.850 60 23-120
3,3'-Dichlorobenzidine ug/L 88.8250 36 10-154
3,3'-Dimethylbenzidine ug/L 41.5100 42 10-157
3-Methylcholanthrene ug/L 46.850 94 65-130
3-Nitroaniline ug/L 107100 107 43-115
4,6-Dinitro-2-methylphenol ug/L 87.7100 88 44-124
4-Aminobiphenyl ug/L 25.750 51 21-125
4-Bromophenylphenyl ether ug/L 34.850 70 34-113
4-Chloro-3-methylphenol ug/L 73.8100 74 31-110
4-Chloroaniline ug/L 87.8100 88 20-120
4-Chlorophenylphenyl ether ug/L 41.750 83 34-116
4-Nitroaniline ug/L 111100 111 46-128
4-Nitrophenol ug/L 79.5250 32 11-120
5-Nitro-o-toluidine ug/L 45.650 91 78-160
7,12-Dimethylbenz(a)anthracene ug/L 46.050 92 47-124
Acenaphthene ug/L 47.250 94 48-114
Acenaphthylene ug/L 48.650 97 48-112
Acetophenone ug/L 42.450 85 24-120
Anthracene ug/L 43.250 86 57-118
Benzo(a)anthracene ug/L 42.850 86 56-121
Benzo(a)pyrene ug/L 45.950 92 55-127
Benzo(b)fluoranthene ug/L 48.850 98 53-128
Benzo(g,h,i)perylene ug/L 39.650 79 54-125
Benzo(k)fluoranthene ug/L 46.150 92 51-123
Benzyl alcohol ug/L 77.8100 78 27-120
bis(2-Chloroethoxy)methane ug/L 33.250 66 32-120
bis(2-Chloroethyl) ether ug/L 34.250 68 33-111
bis(2-Ethylhexyl)phthalate ug/L 43.050 86 50-145
Butylbenzylphthalate ug/L 45.050 90 54-138
Chlorobenzilate ug/L 42.850 86 65-132
Chrysene ug/L 42.650 85 58-127
Di-n-butylphthalate ug/L 46.050 92 56-125
Di-n-octylphthalate ug/L 41.150 82 50-134
Diallate ug/L 33.150 66 47-123
Dibenz(a,h)anthracene ug/L 43.750 87 53-129
Dibenzofuran ug/L 48.350 97 45-120
Diethylphthalate ug/L 46.7J50 93 53-120
Dimethoate ug/L 39.750 79 57-139
Dimethylphthalate ug/L 48.650 97 55-116
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2018679LABORATORY CONTROL SAMPLE:
LCSSpike
Diphenylamine ug/L 44.950 90 42-120
Disulfoton ug/L 33.350 67 49-156
Ethyl methanesulfonate ug/L 31.050 62 43-120
Famphur ug/L 107100 107 40-160
Fluoranthene ug/L 44.450 89 57-125
Fluorene ug/L 46.550 93 53-118
Hexachlorobenzene ug/L 39.850 80 49-116
Hexachlorocyclopentadiene ug/L 35.450 71 26-158
Hexachloroethane ug/L 25.850 52 30-114
Hexachloropropene ug/L 24.150 48 13-137
Indeno(1,2,3-cd)pyrene ug/L 42.150 84 55-128
Isodrin ug/L 40.050 80 68-129
Isophorone ug/L 36.550 73 31-118
Isosafrole ug/L 40.950 82 48-107
Kepone ug/L 65.8100 66 10-124
Methapyrilene ug/L 21.0J50 42 40-160
Methyl methanesulfonate ug/L 46.350 93 25-114
Methyl parathion ug/L 42.950 86 58-137
N-Nitroso-di-n-butylamine ug/L 35.450 71 36-115
N-Nitroso-di-n-propylamine ug/L 43.850 88 32-119
N-Nitrosodiethylamine ug/L 34.650 69 47-115
N-Nitrosodimethylamine ug/L 23.150 46 13-120
N-Nitrosodiphenylamine ug/L 44.950 90 43-120
N-Nitrosomethylethylamine ug/L 28.050 56 39-120
N-Nitrosopiperidine ug/L 41.650 83 43-113
N-Nitrosopyrrolidine ug/L 41.750 83 32-110
Nitrobenzene ug/L 31.550 63 33-110
O,O,O-Triethylphosphorothioate ug/L 38.150 76 51-127
O-Toluidine ug/L 32.150 64 27-120
P-Dimethylaminoazobenzene ug/L 17.3100 17 10-120
p-Phenylenediamine ug/L 37.650 75 72-143
Parathion (Ethyl parathion)ug/L 35.450 71 56-140
Pentachlorobenzene ug/L 42.950 86 30-137
Pentachloronitrobenzene ug/L 44.150 88 70-124
Pentachlorophenol ug/L 97.2250 39 10-137
Phenacetin ug/L 37.050 74 60-130
Phenanthrene ug/L 43.150 86 57-117
Phenol ug/L 18.950 38 10-120
Phorate ug/L 32.650 65 55-126
Pronamide ug/L 40.450 81 75-124
Pyrene ug/L 45.350 91 55-122
Safrole ug/L 41.450 83 41-120
Thionazin ug/L 35.250 70 63-137
2,4,6-Tribromophenol (S)%90 27-110
2-Fluorobiphenyl (S)%90 27-110
2-Fluorophenol (S)%46 12-110
Nitrobenzene-d5 (S)%67 21-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2018679LABORATORY CONTROL SAMPLE:
LCSSpike
Phenol-d6 (S)%34 10-110
Terphenyl-d14 (S)%91 31-107
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2022108MATRIX SPIKE SAMPLE:
MSSpike
Result
92342530002
1,2,4,5-Tetrachlorobenzene ug/L 37.750 75 50-150ND
1,3,5-Trinitrobenzene ug/L 33.650 67 50-150ND
1,3-Dinitrobenzene ug/L 41.450 83 50-150ND
1,4-Naphthoquinone ug/L 44.850 90 50-150ND
1-Naphthalenamine ug/L 14.2 M1502850-150ND
2,2'-Oxybis(1-chloropropane)ug/L 52.050 104 50-150ND
2,3,4,6-Tetrachlorophenol ug/L 85.5 M15017150-150ND
2,4,5-Trichlorophenol ug/L 44.750 89 19-105ND
2,4,6-Trichlorophenol ug/L 52.450 105 13-108ND
2,4-Dichlorophenol ug/L 39.550 79 29-111ND
2,4-Dimethylphenol ug/L 36.250 72 21-103ND
2,4-Dinitrophenol ug/L 207250 83 10-109ND
2,4-Dinitrotoluene ug/L 46.750 93 27-104ND
2,6-Dichlorophenol ug/L 40.550 81 50-150ND
2,6-Dinitrotoluene ug/L 48.550 97 28-101ND
2-Acetylaminofluorene ug/L 36.850 73 50-150ND
2-Chloronaphthalene ug/L 58.1 M15011614-102ND
2-Chlorophenol ug/L 36.350 73 16-110ND
2-Methylnaphthalene ug/L 36.850 74 13-110ND
2-Methylphenol(o-Cresol)ug/L 29.750 59 19-110ND
2-Naphthalenamine ug/L 11.5 M1502350-150ND
2-Nitroaniline ug/L 95.3100 95 26-103ND
2-Nitrophenol ug/L 36.550 73 20-110ND
3&4-Methylphenol(m&p Cresol)ug/L 25.550 51 20-110ND
3,3'-Dichlorobenzidine ug/L 78.3250 31 25-112ND
3,3'-Dimethylbenzidine ug/L 20.1 M11002050-150ND
3-Methylcholanthrene ug/L 44.550 89 50-150ND
3-Nitroaniline ug/L 104100 104 29-110ND
4,6-Dinitro-2-methylphenol ug/L 73.6100 74 10-117ND
4-Aminobiphenyl ug/L 21.2 M1504250-150ND
4-Bromophenylphenyl ether ug/L 35.350 71 20-105ND
4-Chloro-3-methylphenol ug/L 69.2100 69 22-110ND
4-Chloroaniline ug/L 59.4100 59 20-100ND
4-Chlorophenylphenyl ether ug/L 45.050 90 19-102ND
4-Nitroaniline ug/L 112 M110011229-110ND
4-Nitrophenol ug/L 78.0250 31 10-110ND
5-Nitro-o-toluidine ug/L 46.350 93 50-150ND
7,12-Dimethylbenz(a)anthracene ug/L 46.550 93 50-150ND
Acenaphthene ug/L 50.250 100 17-100ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2022108MATRIX SPIKE SAMPLE:
MSSpike
Result
92342530002
Acenaphthylene ug/L 51.2 M15010221-100ND
Acetophenone ug/L 36.550 73 50-150ND
Anthracene ug/L 44.450 89 24-109ND
Benzo(a)anthracene ug/L 41.650 83 22-117ND
Benzo(a)pyrene ug/L 44.750 89 23-104ND
Benzo(b)fluoranthene ug/L 48.950 98 23-103ND
Benzo(g,h,i)perylene ug/L 40.550 81 18-111ND
Benzo(k)fluoranthene ug/L 45.150 90 22-113ND
Benzyl alcohol ug/L 63.0100 63 19-101ND
bis(2-Chloroethoxy)methane ug/L 31.850 64 22-110ND
bis(2-Chloroethyl) ether ug/L 33.150 66 16-110ND
bis(2-Ethylhexyl)phthalate ug/L 44.850 90 23-102ND
Butylbenzylphthalate ug/L 45.650 91 25-110ND
Chlorobenzilate ug/L 42.750 85 50-150ND
Chrysene ug/L 42.250 84 23-115ND
Di-n-butylphthalate ug/L 48.350 97 26-110ND
Di-n-octylphthalate ug/L 41.550 83 22-110ND
Diallate ug/L 35.250 70 50-150ND
Dibenz(a,h)anthracene ug/L 42.050 84 21-112ND
Dibenzofuran ug/L 51.250 102 19-102ND
Diethylphthalate ug/L 50.2J50 100 29-110ND
Dimethoate ug/L 42.950 86 50-150ND
Dimethylphthalate ug/L 51.550 103 27-110ND
Diphenylamine ug/L 45.850 92 50-150ND
Disulfoton ug/L 35.450 71 50-150ND
Ethyl methanesulfonate ug/L 27.450 55 50-150ND
Famphur ug/L 130100 130 50-150ND
Fluoranthene ug/L 45.850 92 23-112ND
Fluorene ug/L 49.150 98 22-104ND
Hexachlorobenzene ug/L 40.050 80 21-116ND
Hexachlorocyclopentadiene ug/L 35.950 72 10-110ND
Hexachloroethane ug/L 27.250 54 10-110ND
Hexachloropropene ug/L 25.550 51 50-150ND
Indeno(1,2,3-cd)pyrene ug/L 42.450 85 20-113ND
Isodrin ug/L 42.350 85 50-150ND
Isophorone ug/L 35.650 71 50-150ND
Isosafrole ug/L 43.650 87 50-150ND
Kepone ug/L 72.4100 72 50-150ND
Methapyrilene ug/L 33.3J50 67 50-150ND
Methyl methanesulfonate ug/L 42.550 85 50-150ND
Methyl parathion ug/L 42.950 86 50-150ND
N-Nitroso-di-n-butylamine ug/L 32.350 65 50-150ND
N-Nitroso-di-n-propylamine ug/L 37.250 74 21-105ND
N-Nitrosodiethylamine ug/L 28.750 57 50-150ND
N-Nitrosodimethylamine ug/L 20.750 41 10-110ND
N-Nitrosodiphenylamine ug/L 45.850 92 23-107ND
N-Nitrosomethylethylamine ug/L 23.7 M1504750-150ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2022108MATRIX SPIKE SAMPLE:
MSSpike
Result
92342530002
N-Nitrosopiperidine ug/L 37.250 74 50-150ND
N-Nitrosopyrrolidine ug/L 28.650 57 50-150ND
Nitrobenzene ug/L 30.450 61 20-110ND
O,O,O-Triethylphosphorothioate ug/L 36.850 74 50-150ND
O-Toluidine ug/L 20.6 M1504150-150ND
P-Dimethylaminoazobenzene ug/L 16.8 M11001750-150ND
p-Phenylenediamine ug/L 35.250 70 50-150ND
Parathion (Ethyl parathion)ug/L 36.650 73 50-150ND
Pentachlorobenzene ug/L 44.750 89 50-150ND
Pentachloronitrobenzene ug/L 44.850 90 50-150ND
Pentachlorophenol ug/L 88.9250 36 10-118ND
Phenacetin ug/L 37.150 74 50-150ND
Phenanthrene ug/L 44.850 90 24-106ND
Phenol ug/L 15.350 31 12-110ND
Phorate ug/L 33.650 67 50-150ND
Pronamide ug/L 41.650 83 50-150ND
Pyrene ug/L 45.050 90 24-114ND
Safrole ug/L 38.450 77 50-150ND
Thionazin ug/L 38.050 76 50-150ND
2,4,6-Tribromophenol (S)%87 27-110
2-Fluorobiphenyl (S)%95 27-110
2-Fluorophenol (S)%39 12-110
Nitrobenzene-d5 (S)%62 21-110
Phenol-d6 (S)%27 10-110
Terphenyl-d14 (S)%74 31-107
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342530004
2018681SAMPLE DUPLICATE:
1,2,4,5-Tetrachlorobenzene ug/L ND 30ND
1,3,5-Trinitrobenzene ug/L ND 30ND
1,3-Dinitrobenzene ug/L ND 30ND
1,4-Naphthoquinone ug/L ND 30ND
1-Naphthalenamine ug/L ND 30ND
2,2'-Oxybis(1-chloropropane)ug/L ND 30ND
2,3,4,6-Tetrachlorophenol ug/L ND 30ND
2,4,5-Trichlorophenol ug/L ND 30ND
2,4,6-Trichlorophenol ug/L ND 30ND
2,4-Dichlorophenol ug/L ND 30ND
2,4-Dimethylphenol ug/L ND 30ND
2,4-Dinitrophenol ug/L ND 30ND
2,4-Dinitrotoluene ug/L ND 30ND
2,6-Dichlorophenol ug/L ND 30ND
2,6-Dinitrotoluene ug/L ND 30ND
2-Acetylaminofluorene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
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Page 44 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342530004
2018681SAMPLE DUPLICATE:
2-Chloronaphthalene ug/L ND 30ND
2-Chlorophenol ug/L ND 30ND
2-Methylnaphthalene ug/L ND 30ND
2-Methylphenol(o-Cresol)ug/L ND 30ND
2-Naphthalenamine ug/L ND 30ND
2-Nitroaniline ug/L ND 30ND
2-Nitrophenol ug/L ND 30ND
3&4-Methylphenol(m&p Cresol)ug/L ND 30ND
3,3'-Dichlorobenzidine ug/L ND 30ND
3,3'-Dimethylbenzidine ug/L ND 30ND
3-Methylcholanthrene ug/L ND 30ND
3-Nitroaniline ug/L ND 30ND
4,6-Dinitro-2-methylphenol ug/L ND 30ND
4-Aminobiphenyl ug/L ND 30ND
4-Bromophenylphenyl ether ug/L ND 30ND
4-Chloro-3-methylphenol ug/L ND 30ND
4-Chloroaniline ug/L ND 30ND
4-Chlorophenylphenyl ether ug/L ND 30ND
4-Nitroaniline ug/L ND 30ND
4-Nitrophenol ug/L ND 30ND
5-Nitro-o-toluidine ug/L NDND
7,12-Dimethylbenz(a)anthracene ug/L ND 30ND
Acenaphthene ug/L ND 30ND
Acenaphthylene ug/L ND 30ND
Acetophenone ug/L ND 30ND
Anthracene ug/L ND 30ND
Benzo(a)anthracene ug/L ND 30ND
Benzo(a)pyrene ug/L ND 30ND
Benzo(b)fluoranthene ug/L ND 30ND
Benzo(g,h,i)perylene ug/L ND 30ND
Benzo(k)fluoranthene ug/L ND 30ND
Benzyl alcohol ug/L ND 30ND
bis(2-Chloroethoxy)methane ug/L ND 30ND
bis(2-Chloroethyl) ether ug/L ND 30ND
bis(2-Ethylhexyl)phthalate ug/L ND 30ND
Butylbenzylphthalate ug/L ND 30ND
Chlorobenzilate ug/L ND 30ND
Chrysene ug/L ND 30ND
Di-n-butylphthalate ug/L ND 30ND
Di-n-octylphthalate ug/L ND 30ND
Diallate ug/L ND 30ND
Dibenz(a,h)anthracene ug/L ND 30ND
Dibenzofuran ug/L ND 30ND
Diethylphthalate ug/L ND 30ND
Dimethoate ug/L ND 30ND
Dimethylphthalate ug/L ND 30ND
Diphenylamine ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
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[phone]
Page 45 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342530004
2018681SAMPLE DUPLICATE:
Disulfoton ug/L ND 30ND
Ethyl methanesulfonate ug/L ND 30ND
Famphur ug/L ND 30ND
Fluoranthene ug/L ND 30ND
Fluorene ug/L ND 30ND
Hexachlorobenzene ug/L ND 30ND
Hexachlorocyclopentadiene ug/L ND 30ND
Hexachloroethane ug/L ND 30ND
Hexachloropropene ug/L ND 30ND
Indeno(1,2,3-cd)pyrene ug/L ND 30ND
Isodrin ug/L ND 30ND
Isophorone ug/L ND 30ND
Isosafrole ug/L ND 30ND
Kepone ug/L ND 30ND
Methapyrilene ug/L ND 30ND
Methyl methanesulfonate ug/L ND 30ND
Methyl parathion ug/L ND 30ND
N-Nitroso-di-n-butylamine ug/L ND 30ND
N-Nitroso-di-n-propylamine ug/L ND 30ND
N-Nitrosodiethylamine ug/L ND 30ND
N-Nitrosodimethylamine ug/L ND 30ND
N-Nitrosodiphenylamine ug/L ND 30ND
N-Nitrosomethylethylamine ug/L ND 30ND
N-Nitrosopiperidine ug/L ND 30ND
N-Nitrosopyrrolidine ug/L ND 30ND
Nitrobenzene ug/L ND 30ND
O,O,O-Triethylphosphorothioate ug/L ND 30ND
O-Toluidine ug/L ND 30ND
P-Dimethylaminoazobenzene ug/L ND 30ND
p-Phenylenediamine ug/L ND 30ND
Parathion (Ethyl parathion)ug/L ND 30ND
Pentachlorobenzene ug/L ND 30ND
Pentachloronitrobenzene ug/L ND 30ND
Pentachlorophenol ug/L ND 30ND
Phenacetin ug/L ND 30ND
Phenanthrene ug/L ND 30ND
Phenol ug/L ND 30ND
Phorate ug/L ND 30ND
Pronamide ug/L ND 30ND
Pyrene ug/L ND 30ND
Safrole ug/L ND 30ND
Thionazin ug/L ND 30ND
2,4,6-Tribromophenol (S)%88 2371
2-Fluorobiphenyl (S)%88 2370
2-Fluorophenol (S)%40 2332
Nitrobenzene-d5 (S)%69 2057
Phenol-d6 (S)%27 2820
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
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Huntersville, NC 28078
[phone]
Page 46 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342530004
2018681SAMPLE DUPLICATE:
Terphenyl-d14 (S)%60 2476
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
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Huntersville, NC 28078
[phone]
Page 47 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363647
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92342784003, 92342784004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2016111
Associated Lab Samples:92342784003, 92342784004
Matrix:Water
AnalyzedMDL
Sulfide ug/L ND 1000 06/06/17 21:30100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2016112LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 528J500 106 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2016113MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342742003
2016114
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 102 80-120107 5 10500ND546J573J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2016115MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342742013
2016116
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 105 80-120111 5 10500ND526J553J
REPORT OF LABORATORY ANALYSIS
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Huntersville, NC 28078
[phone]
Page 48 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
364584
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92342784003, 92342784004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2021203
Associated Lab Samples:92342784003, 92342784004
Matrix:Water
AnalyzedMDL
Cyanide ug/L ND 10.0 06/14/17 11:344.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2021204LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 99.1100 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2021205MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92343009001
2021206
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L 100 93 80-12087 7 10100ND94.3 88.3
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2021207MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342553005
2021208
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L M11005880-12057 1 101005.5J 63.2 62.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 49 of 54
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
Pace Analytical Services - Ormond BeachPASI-O
ANALYTE QUALIFIERS
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
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Huntersville, NC 28078
[phone]
Page 50 of 54
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92342784
SURRY CLOSED-MT. AIRY (AM)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92342784003 363426 363552MW-11 EPA 3510 EPA 8081
92342784004 363426 363552SCALE HOUSE EPA 3510 EPA 8081
92342784003 363427 363555MW-11 EPA 3510 EPA 8082
92342784004 363427 363555SCALE HOUSE EPA 3510 EPA 8082
92342784003 373221 373976MW-11 EPA 8151 EPA 8151
92342784004 373221 373976SCALE HOUSE EPA 8151 EPA 8151
92342784001 363321 364621MW-6 EPA 3010A EPA 6010
92342784002 363321 364621MW-12D EPA 3010A EPA 6010
92342784003 363321 364621MW-11 EPA 3010A EPA 6010
92342784004 363321 364621SCALE HOUSE EPA 3010A EPA 6010
92342784001 363479 363773MW-6 EPA 3010A EPA 6020B
92342784002 363479 363773MW-12D EPA 3010A EPA 6020B
92342784003 363273 363378MW-11 EPA 3010A EPA 6020B
92342784004 363273 363378SCALE HOUSE EPA 3010A EPA 6020B
92342784003 363333 363334MW-11 EPA 7470 EPA 7470
92342784004 363333 363334SCALE HOUSE EPA 7470 EPA 7470
92342784003 364049 364817MW-11 EPA 3510 EPA 8270
92342784004 364049 364817SCALE HOUSE EPA 3510 EPA 8270
92342784001 363311MW-6 EPA 8260
92342784002 363311MW-12D EPA 8260
92342784003 363311MW-11 EPA 8260
92342784004 363311SCALE HOUSE EPA 8260
92342784003 363647MW-11 SM 4500-S2D
92342784004 363647SCALE HOUSE SM 4500-S2D
92342784003 364584MW-11 SM 4500-CN-E
92342784004 364584SCALE HOUSE SM 4500-CN-E
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:26 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 54
Page 52 of 54
Page 53 of 54
Page 54 of 54
#=CL#
June 19, 2017
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92342478
92342478
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
SURRY CLOSED-MT. AIRY (UIC)
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory between May 31, 2017
and June 02, 2017. The results relate only to the samples included in this report. Results reported
herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality
Assurance Manual, where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 166
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Certification: #346
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
Nevada Certification: FL NELAC Reciprocity
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
Wyoming Certification: FL NELAC Reciprocity
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 2 of 166
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Lab ID Sample ID Matrix Date Collected Date Received
92342478001 MW-3R Water 05/31/17 08:05 05/31/17 15:00
92342478002 MW-23 Water 05/31/17 10:10 05/31/17 15:00
92342478003 MW-15 Water 05/31/17 09:30 05/31/17 15:00
92342478004 MW-1 Water 06/01/17 12:35 06/02/17 08:00
92342478005 MW-9 Water 06/01/17 15:40 06/02/17 08:00
92342478006 MW-7 Water 06/01/17 14:45 06/02/17 08:00
92342478007 MW-12S Water 06/01/17 09:50 06/02/17 08:00
92342478008 MW-14 Water 06/01/17 09:00 06/02/17 08:00
92342478009 MW-18 Water 06/01/17 10:15 06/02/17 08:00
92342478010 MW-19 Water 05/31/17 09:00 06/02/17 08:00
92342478011 MW-20 Water 06/01/17 15:30 06/02/17 08:00
92342530001 MW-13 Water 05/31/17 17:35 06/01/17 07:55
92342530002 MW-16 Water 05/31/17 16:50 06/01/17 07:55
92342530003 MW-17 Water 05/31/17 16:30 06/01/17 07:55
92342530004 MW-21 Water 05/31/17 17:20 06/01/17 07:55
92342530005 MW-22 Water 05/31/17 16:10 06/01/17 07:55
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Huntersville, NC 28078
[phone]
Page 3 of 166
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92342478001 MW-3R EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CZDO
92342478002 MW-23 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CZDO
92342478003 MW-15 EPA 8081 21 PASI-CRES
EPA 8082 8 PASI-CHSK
EPA 8151 6 PASI-OLJM
EPA 6010 15 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CZDO
SM 4500-S2D 1 PASI-AMVC
SM 4500-CN-E 1 PASI-AAES2
92342478004 MW-1 EPA 8081 21 PASI-CRES
EPA 8082 8 PASI-CHSK
EPA 8151 6 PASI-OLJM
EPA 6010 15 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CGAW
92342478005 MW-9 EPA 8081 21 PASI-CRES
EPA 8082 8 PASI-CHSK
EPA 8151 6 PASI-OLJM
EPA 6010 15 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AWAB
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CGAW
92342478006 MW-7 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92342478007 MW-12S EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 4 of 166
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8260 50 PASI-CGAW
92342478008 MW-14 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92342478009 MW-18 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92342478010 MW-19 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92342478011 MW-20 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92342530001 MW-13 EPA 8081 21 PASI-CRES
EPA 8082 8 PASI-CHSK
EPA 8151 6 PASI-OLJM
EPA 6010 15 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CZDO
SM 4500-S2D 1 PASI-AMVC
SM 4500-CN-E 1 PASI-AAES2
92342530002 MW-16 EPA 8081 21 PASI-CRES
EPA 8082 8 PASI-CHSK
EPA 8151 6 PASI-OLJM
EPA 6010 15 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CZDO
SM 4500-S2D 1 PASI-AMVC
SM 4500-CN-E 1 PASI-AAES2
92342530003 MW-17 EPA 8081 21 PASI-CRES
EPA 8082 8 PASI-CHSK
EPA 8151 6 PASI-OLJM
EPA 6010 15 PASI-ASH1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 166
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CZDO
SM 4500-S2D 1 PASI-AMVC
SM 4500-CN-E 1 PASI-AAES2
92342530004 MW-21 EPA 8081 21 PASI-CRES
EPA 8082 8 PASI-CHSK
EPA 8151 6 PASI-OLJM
EPA 6010 15 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CGAW
SM 4500-S2D 1 PASI-AMVC
SM 4500-CN-E 1 PASI-AAES2
92342530005 MW-22 EPA 8081 21 PASI-CRES
EPA 8082 8 PASI-CHSK
EPA 8151 6 PASI-OLJM
EPA 6010 15 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CZDO
SM 4500-S2D 1 PASI-AMVC
SM 4500-CN-E 1 PASI-AAES2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-3R Lab ID:92342478001 Collected:05/31/17 08:05 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/09/17 18:25 7440-36-006/02/17 15:206.0 3.9 1
Arsenic ND ug/L 06/09/17 18:25 7440-38-206/02/17 15:2010.0 5.0 1
Barium 7.4J ug/L 06/09/17 18:25 7440-39-306/02/17 15:201002.5 1
Beryllium ND ug/L 06/09/17 18:25 7440-41-706/02/17 15:201.0 0.50 1
Cadmium ND ug/L 06/09/17 18:25 7440-43-906/02/17 15:201.0 0.50 1
Chromium ND ug/L 06/09/17 18:25 7440-47-306/02/17 15:2010.0 2.5 1
Cobalt ND ug/L 06/09/17 18:25 7440-48-406/02/17 15:2010.0 2.5 1
Copper 4.2J ug/L 06/09/17 18:25 7440-50-806/02/17 15:2010.0 2.5 1
Lead ND ug/L 06/09/17 18:25 7439-92-106/02/17 15:2010.0 2.5 1
Nickel ND ug/L 06/09/17 18:25 7440-02-006/02/17 15:2050.0 2.5 1
Selenium ND ug/L 06/09/17 18:25 7782-49-206/02/17 15:2010.0 5.0 1
Silver ND ug/L 06/09/17 18:25 7440-22-406/02/17 15:2010.0 2.5 1
Vanadium ND ug/L 06/09/17 18:25 7440-62-206/02/17 15:2025.0 2.5 1
Zinc ND ug/L 06/09/17 18:25 7440-66-606/02/17 15:2010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/07/17 15:40 7440-28-006/03/17 02:255.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/02/17 01:30 67-64-110010.0 1
Acrylonitrile ND ug/L 06/02/17 01:30 107-13-12001.9 1
Benzene ND ug/L 06/02/17 01:30 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/02/17 01:30 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/02/17 01:30 75-27-41.0 0.18 1
Bromoform ND ug/L 06/02/17 01:30 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/02/17 01:30 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/02/17 01:30 78-93-31000.96 1
Carbon disulfide ND ug/L 06/02/17 01:30 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/02/17 01:30 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/02/17 01:30 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/02/17 01:30 75-00-310.0 0.54 1
Chloroform ND ug/L 06/02/17 01:30 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/02/17 01:30 74-87-3 M11.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/02/17 01:30 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/02/17 01:30 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/02/17 01:30 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/02/17 01:30 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/02/17 01:30 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/02/17 01:30 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/02/17 01:30 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/02/17 01:30 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/02/17 01:30 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/02/17 01:30 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/02/17 01:30 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/02/17 01:30 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/02/17 01:30 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-3R Lab ID:92342478001 Collected:05/31/17 08:05 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 06/02/17 01:30 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/02/17 01:30 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/02/17 01:30 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/02/17 01:30 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/02/17 01:30 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/02/17 01:30 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/02/17 01:30 108-10-11000.33 1
Styrene ND ug/L 06/02/17 01:30 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/02/17 01:30 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/02/17 01:30 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/02/17 01:30 127-18-41.0 0.46 1
Toluene ND ug/L 06/02/17 01:30 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/02/17 01:30 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/02/17 01:30 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/02/17 01:30 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/02/17 01:30 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/02/17 01:30 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/02/17 01:30 108-05-4 M150.0 0.35 1
Vinyl chloride ND ug/L 06/02/17 01:30 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/02/17 01:30 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)115 %06/02/17 01:30 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %06/02/17 01:30 17060-07-070-130 1
Toluene-d8 (S)112 %06/02/17 01:30 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-23 Lab ID:92342478002 Collected:05/31/17 10:10 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/09/17 18:28 7440-36-006/02/17 15:206.0 3.9 1
Arsenic ND ug/L 06/09/17 18:28 7440-38-206/02/17 15:2010.0 5.0 1
Barium 33.8J ug/L 06/09/17 18:28 7440-39-306/02/17 15:201002.5 1
Beryllium ND ug/L 06/09/17 18:28 7440-41-706/02/17 15:201.0 0.50 1
Cadmium 2.1 ug/L 06/09/17 18:28 7440-43-906/02/17 15:201.0 0.50 1
Chromium ND ug/L 06/09/17 18:28 7440-47-306/02/17 15:2010.0 2.5 1
Cobalt ND ug/L 06/09/17 18:28 7440-48-406/02/17 15:2010.0 2.5 1
Copper 5.0J ug/L 06/09/17 18:28 7440-50-806/02/17 15:2010.0 2.5 1
Lead ND ug/L 06/09/17 18:28 7439-92-106/02/17 15:2010.0 2.5 1
Nickel ND ug/L 06/09/17 18:28 7440-02-006/02/17 15:2050.0 2.5 1
Selenium ND ug/L 06/09/17 18:28 7782-49-206/02/17 15:2010.0 5.0 1
Silver ND ug/L 06/09/17 18:28 7440-22-406/02/17 15:2010.0 2.5 1
Vanadium ND ug/L 06/09/17 18:28 7440-62-206/02/17 15:2025.0 2.5 1
Zinc 6.5J ug/L 06/09/17 18:28 7440-66-606/02/17 15:2010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.024J ug/L 06/06/17 18:59 7440-28-006/03/17 02:255.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/02/17 01:47 67-64-110010.0 1
Acrylonitrile ND ug/L 06/02/17 01:47 107-13-12001.9 1
Benzene ND ug/L 06/02/17 01:47 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/02/17 01:47 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/02/17 01:47 75-27-41.0 0.18 1
Bromoform ND ug/L 06/02/17 01:47 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/02/17 01:47 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/02/17 01:47 78-93-31000.96 1
Carbon disulfide ND ug/L 06/02/17 01:47 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/02/17 01:47 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/02/17 01:47 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/02/17 01:47 75-00-310.0 0.54 1
Chloroform ND ug/L 06/02/17 01:47 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/02/17 01:47 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/02/17 01:47 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/02/17 01:47 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/02/17 01:47 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/02/17 01:47 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/02/17 01:47 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/02/17 01:47 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/02/17 01:47 110-57-61001.0 1
1,1-Dichloroethane 0.43J ug/L 06/02/17 01:47 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/02/17 01:47 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/02/17 01:47 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.39J ug/L 06/02/17 01:47 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/02/17 01:47 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/02/17 01:47 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-23 Lab ID:92342478002 Collected:05/31/17 10:10 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 06/02/17 01:47 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/02/17 01:47 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/02/17 01:47 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/02/17 01:47 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/02/17 01:47 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/02/17 01:47 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/02/17 01:47 108-10-11000.33 1
Styrene ND ug/L 06/02/17 01:47 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/02/17 01:47 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/02/17 01:47 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/02/17 01:47 127-18-41.0 0.46 1
Toluene ND ug/L 06/02/17 01:47 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/02/17 01:47 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/02/17 01:47 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/02/17 01:47 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/02/17 01:47 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/02/17 01:47 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/02/17 01:47 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/02/17 01:47 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/02/17 01:47 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)113 %06/02/17 01:47 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %06/02/17 01:47 17060-07-070-130 1
Toluene-d8 (S)111 %06/02/17 01:47 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-15 Lab ID:92342478003 Collected:05/31/17 09:30 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/06/17 19:11 309-00-206/02/17 10:090.050 0.050 1
alpha-BHC ND ug/L 06/06/17 19:11 319-84-606/02/17 10:090.050 0.050 1
beta-BHC ND ug/L 06/06/17 19:11 319-85-706/02/17 10:090.050 0.050 1
delta-BHC ND ug/L 06/06/17 19:11 319-86-806/02/17 10:090.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/06/17 19:11 58-89-906/02/17 10:090.050 0.050 1
Chlordane (Technical)ND ug/L 06/06/17 19:11 57-74-906/02/17 10:090.50 0.20 1
4,4'-DDD ND ug/L 06/06/17 19:11 72-54-806/02/17 10:090.10 0.050 1
4,4'-DDE ND ug/L 06/06/17 19:11 72-55-906/02/17 10:090.10 0.050 1
4,4'-DDT ND ug/L 06/06/17 19:11 50-29-306/02/17 10:090.10 0.050 1
Dieldrin ND ug/L 06/06/17 19:11 60-57-106/02/17 10:090.075 0.050 1
Endosulfan I ND ug/L 06/06/17 19:11 959-98-806/02/17 10:090.10 0.050 1
Endosulfan II ND ug/L 06/06/17 19:11 33213-65-906/02/17 10:090.10 0.050 1
Endosulfan sulfate ND ug/L 06/06/17 19:11 1031-07-806/02/17 10:090.10 0.050 1
Endrin ND ug/L 06/06/17 19:11 72-20-806/02/17 10:090.10 0.050 1
Endrin aldehyde ND ug/L 06/06/17 19:11 7421-93-406/02/17 10:090.10 0.050 1
Heptachlor ND ug/L 06/06/17 19:11 76-44-806/02/17 10:090.050 0.050 1
Heptachlor epoxide ND ug/L 06/06/17 19:11 1024-57-306/02/17 10:090.075 0.050 1
Methoxychlor ND ug/L 06/06/17 19:11 72-43-506/02/17 10:091.0 0.15 1
Toxaphene ND ug/L 06/06/17 19:11 8001-35-206/02/17 10:091.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)95 %06/06/17 19:11 877-09-806/02/17 10:0920-130 1
Decachlorobiphenyl (S)54 %06/06/17 19:11 2051-24-306/02/17 10:0920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/02/17 19:52 12674-11-206/02/17 10:090.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/02/17 19:52 11104-28-206/02/17 10:090.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/02/17 19:52 11141-16-506/02/17 10:090.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/02/17 19:52 53469-21-906/02/17 10:090.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/02/17 19:52 12672-29-606/02/17 10:090.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/02/17 19:52 11097-69-106/02/17 10:090.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/02/17 19:52 11096-82-506/02/17 10:090.50 0.50 1
Surrogates
Decachlorobiphenyl (S)47 %06/02/17 19:52 2051-24-306/02/17 10:0910-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/06/17 06:46 94-75-706/02/17 16:300.91 0.22 1
Dinoseb ND ug/L 06/06/17 06:46 88-85-706/02/17 16:300.18 0.055 1
Pentachlorophenol ND ug/L 06/06/17 06:46 87-86-506/02/17 16:300.028 0.017 1
2,4,5-T ND ug/L 06/06/17 06:46 93-76-506/02/17 16:300.18 0.041 1
2,4,5-TP (Silvex)ND ug/L 06/06/17 06:46 93-72-106/02/17 16:300.18 0.048 1
Surrogates
2,4-DCAA (S)75 %06/06/17 06:46 19719-28-906/02/17 16:3039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/09/17 16:27 7440-36-006/02/17 15:206.0 3.9 1
Arsenic ND ug/L 06/09/17 16:27 7440-38-206/02/17 15:2010.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-15 Lab ID:92342478003 Collected:05/31/17 09:30 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Barium 49.2J ug/L 06/09/17 16:27 7440-39-306/02/17 15:201002.5 1
Beryllium ND ug/L 06/09/17 16:27 7440-41-706/02/17 15:201.0 0.50 1
Cadmium ND ug/L 06/09/17 16:27 7440-43-906/02/17 15:201.0 0.50 1
Chromium ND ug/L 06/09/17 16:27 7440-47-306/02/17 15:2010.0 2.5 1
Cobalt 2.7J ug/L 06/09/17 16:27 7440-48-406/02/17 15:2010.0 2.5 1
Copper ND ug/L 06/09/17 16:27 7440-50-806/02/17 15:2010.0 2.5 1
Lead ND ug/L 06/09/17 16:27 7439-92-106/02/17 15:2010.0 2.5 1
Nickel 3.1J ug/L 06/09/17 16:27 7440-02-006/02/17 15:2050.0 2.5 1
Selenium ND ug/L 06/09/17 16:27 7782-49-206/02/17 15:2010.0 5.0 1
Silver ND ug/L 06/09/17 16:27 7440-22-406/02/17 15:2010.0 2.5 1
Tin ND ug/L 06/09/17 16:27 7440-31-506/02/17 15:201002.5 1
Vanadium 3.1J ug/L 06/09/17 16:27 7440-62-206/02/17 15:2025.0 2.5 1
Zinc 10.7 ug/L 06/09/17 16:27 7440-66-606/02/17 15:2010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.091J ug/L 06/06/17 19:01 7440-28-006/03/17 02:255.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 02:29 7439-97-606/04/17 20:450.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/13/17 18:57 83-32-906/07/17 16:1010.0 1.6 1
Acenaphthylene ND ug/L 06/13/17 18:57 208-96-806/07/17 16:1010.0 1.5 1
Acetophenone ND ug/L 06/13/17 18:57 98-86-206/07/17 16:1010.0 1.9 1
2-Acetylaminofluorene ND ug/L 06/13/17 18:57 53-96-3 L206/07/17 16:1020.0 1.6 1
4-Aminobiphenyl ND ug/L 06/13/17 18:57 92-67-106/07/17 16:1020.0 1.7 1
Anthracene ND ug/L 06/13/17 18:57 120-12-706/07/17 16:1010.0 1.7 1
Benzo(a)anthracene ND ug/L 06/13/17 18:57 56-55-306/07/17 16:1010.0 2.1 1
Benzo(a)pyrene ND ug/L 06/13/17 18:57 50-32-806/07/17 16:1010.0 2.2 1
Benzo(b)fluoranthene ND ug/L 06/13/17 18:57 205-99-206/07/17 16:1010.0 2.2 1
Benzo(g,h,i)perylene ND ug/L 06/13/17 18:57 191-24-206/07/17 16:1010.0 2.1 1
Benzo(k)fluoranthene ND ug/L 06/13/17 18:57 207-08-906/07/17 16:1010.0 2.0 1
Benzyl alcohol ND ug/L 06/13/17 18:57 100-51-6 L206/07/17 16:1020.0 3.1 1
4-Bromophenylphenyl ether ND ug/L 06/13/17 18:57 101-55-306/07/17 16:1010.0 1.5 1
Butylbenzylphthalate ND ug/L 06/13/17 18:57 85-68-706/07/17 16:1010.0 2.5 1
4-Chloro-3-methylphenol ND ug/L 06/13/17 18:57 59-50-706/07/17 16:1020.0 2.8 1
4-Chloroaniline ND ug/L 06/13/17 18:57 106-47-806/07/17 16:1020.0 2.8 1
Chlorobenzilate ND ug/L 06/13/17 18:57 510-15-606/07/17 16:1010.0 2.2 1
bis(2-Chloroethoxy)methane ND ug/L 06/13/17 18:57 111-91-1 L206/07/17 16:1010.0 1.6 1
bis(2-Chloroethyl) ether ND ug/L 06/13/17 18:57 111-44-4 L206/07/17 16:1010.0 1.7 1
2-Chloronaphthalene ND ug/L 06/13/17 18:57 91-58-7 L206/07/17 16:1010.0 1.6 1
2-Chlorophenol ND ug/L 06/13/17 18:57 95-57-8 L206/07/17 16:1010.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/13/17 18:57 7005-72-306/07/17 16:1010.0 1.6 1
Chrysene ND ug/L 06/13/17 18:57 218-01-906/07/17 16:1010.0 2.1 1
Diallate ND ug/L 06/13/17 18:57 2303-16-406/07/17 16:1010.0 1.6 1
Dibenz(a,h)anthracene ND ug/L 06/13/17 18:57 53-70-306/07/17 16:1010.0 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
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Page 12 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-15 Lab ID:92342478003 Collected:05/31/17 09:30 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Dibenzofuran ND ug/L 06/13/17 18:57 132-64-906/07/17 16:1010.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 06/13/17 18:57 91-94-106/07/17 16:1020.0 3.9 1
2,4-Dichlorophenol ND ug/L 06/13/17 18:57 120-83-2 L206/07/17 16:1010.0 1.6 1
2,6-Dichlorophenol ND ug/L 06/13/17 18:57 87-65-0 L206/07/17 16:1010.0 1.5 1
Diethylphthalate ND ug/L 06/13/17 18:57 84-66-206/07/17 16:1060001.6 1
Dimethoate ND ug/L 06/13/17 18:57 60-51-506/07/17 16:1020.0 1.8 1
P-Dimethylaminoazobenzene ND ug/L 06/13/17 18:57 60-11-706/07/17 16:1010.0 1.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/13/17 18:57 57-97-606/07/17 16:1010.0 2.4 1
3,3'-Dimethylbenzidine ND ug/L 06/13/17 18:57 119-93-706/07/17 16:1010.0 3.9 1
2,4-Dimethylphenol ND ug/L 06/13/17 18:57 105-67-9 L206/07/17 16:1010.0 1.6 1
Dimethylphthalate ND ug/L 06/13/17 18:57 131-11-306/07/17 16:1010.0 1.4 1
Di-n-butylphthalate ND ug/L 06/13/17 18:57 84-74-206/07/17 16:1010.0 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/13/17 18:57 534-52-106/07/17 16:1050.0 2.2 1
1,3-Dinitrobenzene ND ug/L 06/13/17 18:57 99-65-006/07/17 16:1020.0 1.3 1
2,4-Dinitrophenol ND ug/L 06/13/17 18:57 51-28-506/07/17 16:1050.0 5.1 1
2,4-Dinitrotoluene ND ug/L 06/13/17 18:57 121-14-206/07/17 16:1010.0 1.5 1
2,6-Dinitrotoluene ND ug/L 06/13/17 18:57 606-20-206/07/17 16:1010.0 1.4 1
Di-n-octylphthalate ND ug/L 06/13/17 18:57 117-84-006/07/17 16:1010.0 1.5 1
Diphenylamine ND ug/L 06/13/17 18:57 122-39-406/07/17 16:1010.0 1.4 1
Disulfoton ND ug/L 06/13/17 18:57 298-04-406/07/17 16:1010.0 1.5 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/13/17 18:57 117-81-706/07/17 16:1015.0 2.3 1
Ethyl methanesulfonate ND ug/L 06/13/17 18:57 62-50-0 L206/07/17 16:1020.0 1.6 1
Famphur ND ug/L 06/13/17 18:57 52-85-706/07/17 16:1020.0 5.7 1
Fluoranthene ND ug/L 06/13/17 18:57 206-44-006/07/17 16:1010.0 2.2 1
Fluorene ND ug/L 06/13/17 18:57 86-73-706/07/17 16:1010.0 1.6 1
Hexachlorobenzene ND ug/L 06/13/17 18:57 118-74-106/07/17 16:1010.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 06/13/17 18:57 77-47-4 L206/07/17 16:1010.0 1.3 1
Hexachloroethane ND ug/L 06/13/17 18:57 67-72-1 L206/07/17 16:1010.0 1.8 1
Hexachloropropene ND ug/L 06/13/17 18:57 1888-71-706/07/17 16:1010.0 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/13/17 18:57 193-39-506/07/17 16:1010.0 2.0 1
Isodrin ND ug/L 06/13/17 18:57 465-73-606/07/17 16:1020.0 2.5 1
Isophorone ND ug/L 06/13/17 18:57 78-59-1 L206/07/17 16:1010.0 1.5 1
Isosafrole ND ug/L 06/13/17 18:57 120-58-1 L206/07/17 16:1010.0 1.5 1
Kepone ND ug/L 06/13/17 18:57 143-50-006/07/17 16:1020.0 4.5 1
Methapyrilene ND ug/L 06/13/17 18:57 91-80-506/07/17 16:101003.0 1
3-Methylcholanthrene ND ug/L 06/13/17 18:57 56-49-506/07/17 16:1010.0 2.7 1
Methyl methanesulfonate ND ug/L 06/13/17 18:57 66-27-306/07/17 16:1010.0 1.1 1
2-Methylnaphthalene ND ug/L 06/13/17 18:57 91-57-6 L206/07/17 16:1010.0 1.4 1
Methyl parathion ND ug/L 06/13/17 18:57 298-00-006/07/17 16:1010.0 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 06/13/17 18:57 95-48-7 L206/07/17 16:1010.0 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/13/17 18:57 15831-10-4 L206/07/17 16:1010.0 1.4 1
1-Naphthalenamine ND ug/L 06/13/17 18:57 134-32-706/07/17 16:1010.0 1.3 1
2-Naphthalenamine ND ug/L 06/13/17 18:57 91-59-806/07/17 16:1010.0 2.2 1
1,4-Naphthoquinone ND ug/L 06/13/17 18:57 130-15-406/07/17 16:1010.0 0.99 1
2-Nitroaniline ND ug/L 06/13/17 18:57 88-74-406/07/17 16:1050.0 2.3 1
3-Nitroaniline ND ug/L 06/13/17 18:57 99-09-206/07/17 16:1050.0 2.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-15 Lab ID:92342478003 Collected:05/31/17 09:30 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Nitroaniline ND ug/L 06/13/17 18:57 100-01-606/07/17 16:1020.0 3.4 1
Nitrobenzene ND ug/L 06/13/17 18:57 98-95-3 L206/07/17 16:1010.0 1.6 1
2-Nitrophenol ND ug/L 06/13/17 18:57 88-75-5 L206/07/17 16:1010.0 1.6 1
4-Nitrophenol ND ug/L 06/13/17 18:57 100-02-706/07/17 16:1050.0 4.3 1
5-Nitro-o-toluidine ND ug/L 06/13/17 18:57 99-55-8 L206/07/17 16:1010.0 1.9 1
N-Nitrosodiethylamine ND ug/L 06/13/17 18:57 55-18-5 L206/07/17 16:1020.0 1.4 1
N-Nitrosodimethylamine ND ug/L 06/13/17 18:57 62-75-906/07/17 16:1010.0 1.6 1
N-Nitroso-di-n-butylamine ND ug/L 06/13/17 18:57 924-16-3 L206/07/17 16:1010.0 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 06/13/17 18:57 621-64-7 L206/07/17 16:1010.0 1.7 1
N-Nitrosodiphenylamine ND ug/L 06/13/17 18:57 86-30-606/07/17 16:1010.0 1.4 1
N-Nitrosomethylethylamine ND ug/L 06/13/17 18:57 10595-95-6 L206/07/17 16:1010.0 1.4 1
N-Nitrosopiperidine ND ug/L 06/13/17 18:57 100-75-4 L206/07/17 16:1020.0 1.7 1
N-Nitrosopyrrolidine ND ug/L 06/13/17 18:57 930-55-2 L206/07/17 16:1010.0 1.7 1
O,O,O-Triethylphosphorothioate ND ug/L 06/13/17 18:57 126-68-1 L206/07/17 16:1010.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/13/17 18:57 108-60-106/07/17 16:1010.0 1.8 1
Parathion (Ethyl parathion)ND ug/L 06/13/17 18:57 56-38-2 L206/07/17 16:1010.0 1.5 1
Pentachlorobenzene ND ug/L 06/13/17 18:57 608-93-506/07/17 16:1010.0 1.5 1
Pentachloronitrobenzene ND ug/L 06/13/17 18:57 82-68-806/07/17 16:1020.0 1.7 1
Pentachlorophenol ND ug/L 06/13/17 18:57 87-86-506/07/17 16:1025.0 3.5 1
Phenacetin ND ug/L 06/13/17 18:57 62-44-206/07/17 16:1020.0 1.9 1
Phenanthrene ND ug/L 06/13/17 18:57 85-01-806/07/17 16:1010.0 1.6 1
Phenol ND ug/L 06/13/17 18:57 108-95-206/07/17 16:1010.0 1.3 1
p-Phenylenediamine ND ug/L 06/13/17 18:57 106-50-3 L206/07/17 16:1010.0 2.2 1
Phorate ND ug/L 06/13/17 18:57 298-02-2 L206/07/17 16:1010.0 1.7 1
Pronamide ND ug/L 06/13/17 18:57 23950-58-5 L206/07/17 16:1010.0 2.0 1
Pyrene ND ug/L 06/13/17 18:57 129-00-006/07/17 16:1010.0 2.2 1
Safrole ND ug/L 06/13/17 18:57 94-59-7 L206/07/17 16:1010.0 1.3 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/13/17 18:57 95-94-306/07/17 16:1010.0 1.3 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/13/17 18:57 58-90-206/07/17 16:1010.0 2.9 1
Thionazin ND ug/L 06/13/17 18:57 297-97-2 L206/07/17 16:1020.0 1.7 1
O-Toluidine ND ug/L 06/13/17 18:57 95-53-4 L206/07/17 16:1010.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 06/13/17 18:57 95-95-406/07/17 16:1010.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/13/17 18:57 88-06-206/07/17 16:1010.0 1.4 1
1,3,5-Trinitrobenzene ND ug/L 06/13/17 18:57 99-35-4 L206/07/17 16:1010.0 1.2 1
Surrogates
Nitrobenzene-d5 (S)80 %06/13/17 18:57 4165-60-0 1g06/07/17 16:1021-110 1
2-Fluorobiphenyl (S)101 %06/13/17 18:57 321-60-806/07/17 16:1027-110 1
Terphenyl-d14 (S)104 %06/13/17 18:57 1718-51-006/07/17 16:1031-107 1
Phenol-d6 (S)33 %06/13/17 18:57 13127-88-306/07/17 16:1010-110 1
2-Fluorophenol (S)49 %06/13/17 18:57 367-12-406/07/17 16:1012-110 1
2,4,6-Tribromophenol (S)86 %06/13/17 18:57 118-79-606/07/17 16:1027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/02/17 02:22 67-64-110010.0 1
Acetonitrile ND ug/L 06/02/17 02:22 75-05-855.0 2.2 1
Acrolein ND ug/L 06/02/17 02:22 107-02-853.0 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-15 Lab ID:92342478003 Collected:05/31/17 09:30 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acrylonitrile ND ug/L 06/02/17 02:22 107-13-12001.9 1
Allyl chloride ND ug/L 06/02/17 02:22 107-05-110.0 1.5 1
Benzene 0.65J ug/L 06/02/17 02:22 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/02/17 02:22 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/02/17 02:22 75-27-41.0 0.18 1
Bromoform ND ug/L 06/02/17 02:22 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/02/17 02:22 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/02/17 02:22 78-93-31000.96 1
Carbon disulfide ND ug/L 06/02/17 02:22 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/02/17 02:22 56-23-51.0 0.25 1
Chlorobenzene 2.4J ug/L 06/02/17 02:22 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/02/17 02:22 75-00-310.0 0.54 1
Chloroform ND ug/L 06/02/17 02:22 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/02/17 02:22 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/02/17 02:22 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/02/17 02:22 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/02/17 02:22 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/02/17 02:22 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/02/17 02:22 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/02/17 02:22 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/02/17 02:22 541-73-15.0 0.24 1
1,4-Dichlorobenzene 3.7 ug/L 06/02/17 02:22 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/02/17 02:22 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/02/17 02:22 75-71-85.0 0.21 1
1,1-Dichloroethane 9.7 ug/L 06/02/17 02:22 75-34-35.0 0.32 1
1,2-Dichloroethane 0.58J ug/L 06/02/17 02:22 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/02/17 02:22 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 33.3 ug/L 06/02/17 02:22 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/02/17 02:22 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/02/17 02:22 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/02/17 02:22 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/02/17 02:22 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/02/17 02:22 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/02/17 02:22 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/02/17 02:22 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/02/17 02:22 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/02/17 02:22 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/02/17 02:22 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/02/17 02:22 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/02/17 02:22 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/02/17 02:22 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/02/17 02:22 126-98-71000.93 1
Methylene Chloride ND ug/L 06/02/17 02:22 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/02/17 02:22 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/02/17 02:22 108-10-11000.33 1
Naphthalene ND ug/L 06/02/17 02:22 91-20-310.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-15 Lab ID:92342478003 Collected:05/31/17 09:30 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Propionitrile ND ug/L 06/02/17 02:22 107-12-01503.6 1
Styrene ND ug/L 06/02/17 02:22 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/02/17 02:22 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/02/17 02:22 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/02/17 02:22 127-18-41.0 0.46 1
Toluene ND ug/L 06/02/17 02:22 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/02/17 02:22 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/02/17 02:22 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/02/17 02:22 79-00-51.0 0.29 1
Trichloroethene 2.0 ug/L 06/02/17 02:22 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/02/17 02:22 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/02/17 02:22 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/02/17 02:22 108-05-450.0 0.35 1
Vinyl chloride 1.6 ug/L 06/02/17 02:22 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/02/17 02:22 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)114 %06/02/17 02:22 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %06/02/17 02:22 17060-07-070-130 1
Toluene-d8 (S)111 %06/02/17 02:22 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/06/17 22:15 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 4.6J ug/L 06/01/17 17:39 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
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Page 16 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-1 Lab ID:92342478004 Collected:06/01/17 12:35 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/06/17 12:52 309-00-206/05/17 17:300.050 0.050 1
alpha-BHC ND ug/L 06/06/17 12:52 319-84-606/05/17 17:300.050 0.050 1
beta-BHC ND ug/L 06/06/17 12:52 319-85-706/05/17 17:300.050 0.050 1
delta-BHC ND ug/L 06/06/17 12:52 319-86-806/05/17 17:300.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/06/17 12:52 58-89-906/05/17 17:300.050 0.050 1
Chlordane (Technical)ND ug/L 06/06/17 12:52 57-74-906/05/17 17:300.50 0.20 1
4,4'-DDD ND ug/L 06/06/17 12:52 72-54-806/05/17 17:300.10 0.050 1
4,4'-DDE ND ug/L 06/06/17 12:52 72-55-906/05/17 17:300.10 0.050 1
4,4'-DDT ND ug/L 06/06/17 12:52 50-29-306/05/17 17:300.10 0.050 1
Dieldrin ND ug/L 06/06/17 12:52 60-57-106/05/17 17:300.075 0.050 1
Endosulfan I ND ug/L 06/06/17 12:52 959-98-806/05/17 17:300.10 0.050 1
Endosulfan II ND ug/L 06/06/17 12:52 33213-65-906/05/17 17:300.10 0.050 1
Endosulfan sulfate ND ug/L 06/06/17 12:52 1031-07-806/05/17 17:300.10 0.050 1
Endrin ND ug/L 06/06/17 12:52 72-20-806/05/17 17:300.10 0.050 1
Endrin aldehyde ND ug/L 06/06/17 12:52 7421-93-406/05/17 17:300.10 0.050 1
Heptachlor ND ug/L 06/06/17 12:52 76-44-806/05/17 17:300.050 0.050 1
Heptachlor epoxide ND ug/L 06/06/17 12:52 1024-57-306/05/17 17:300.075 0.050 1
Methoxychlor ND ug/L 06/06/17 12:52 72-43-506/05/17 17:301.0 0.15 1
Toxaphene ND ug/L 06/06/17 12:52 8001-35-206/05/17 17:301.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)73 %06/06/17 12:52 877-09-806/05/17 17:3020-130 1
Decachlorobiphenyl (S)72 %06/06/17 12:52 2051-24-306/05/17 17:3020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/06/17 19:29 12674-11-206/05/17 17:300.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/06/17 19:29 11104-28-206/05/17 17:300.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/06/17 19:29 11141-16-506/05/17 17:300.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/06/17 19:29 53469-21-906/05/17 17:300.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/06/17 19:29 12672-29-606/05/17 17:300.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/06/17 19:29 11097-69-106/05/17 17:300.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/06/17 19:29 11096-82-506/05/17 17:300.50 0.50 1
Surrogates
Decachlorobiphenyl (S)70 %06/06/17 19:29 2051-24-306/05/17 17:3010-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/10/17 04:37 94-75-706/07/17 16:000.98 0.23 1
Dinoseb ND ug/L 06/10/17 04:37 88-85-706/07/17 16:000.20 0.059 1
Pentachlorophenol ND ug/L 06/10/17 04:37 87-86-506/07/17 16:000.030 0.018 1
2,4,5-T ND ug/L 06/10/17 04:37 93-76-506/07/17 16:000.20 0.044 1
2,4,5-TP (Silvex)ND ug/L 06/10/17 04:37 93-72-106/07/17 16:000.20 0.051 1
Surrogates
2,4-DCAA (S)81 %06/10/17 04:37 19719-28-906/07/17 16:0039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/14/17 22:43 7440-36-006/04/17 16:406.0 3.9 1
Arsenic ND ug/L 06/14/17 22:43 7440-38-206/04/17 16:4010.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-1 Lab ID:92342478004 Collected:06/01/17 12:35 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Barium 92.9J ug/L 06/14/17 22:43 7440-39-306/04/17 16:401002.5 1
Beryllium ND ug/L 06/14/17 22:43 7440-41-706/04/17 16:401.0 0.50 1
Cadmium 0.89J ug/L 06/14/17 22:43 7440-43-906/04/17 16:401.0 0.50 1
Chromium ND ug/L 06/14/17 22:43 7440-47-306/04/17 16:4010.0 2.5 1
Cobalt ND ug/L 06/14/17 22:43 7440-48-406/04/17 16:4010.0 2.5 1
Copper 356 ug/L 06/14/17 22:43 7440-50-806/04/17 16:4010.0 2.5 1
Lead 21.0 ug/L 06/14/17 22:43 7439-92-106/04/17 16:4010.0 2.5 1
Nickel 4.5J ug/L 06/14/17 22:43 7440-02-006/04/17 16:4050.0 2.5 1
Selenium ND ug/L 06/14/17 22:43 7782-49-206/04/17 16:4010.0 5.0 1
Silver ND ug/L 06/14/17 22:43 7440-22-406/04/17 16:4010.0 2.5 1
Tin 3.9J ug/L 06/14/17 22:43 7440-31-506/04/17 16:401002.5 1
Vanadium ND ug/L 06/14/17 22:43 7440-62-206/04/17 16:4025.0 2.5 1
Zinc 256 ug/L 06/14/17 22:43 7440-66-606/04/17 16:4010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.026J ug/L 06/09/17 16:30 7440-28-006/03/17 02:255.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/06/17 10:06 7439-97-606/05/17 20:000.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/14/17 19:54 83-32-906/07/17 17:1010.0 1.6 1
Acenaphthylene ND ug/L 06/14/17 19:54 208-96-806/07/17 17:1010.0 1.5 1
Acetophenone ND ug/L 06/14/17 19:54 98-86-206/07/17 17:1010.0 1.9 1
2-Acetylaminofluorene ND ug/L 06/14/17 19:54 53-96-3 L206/07/17 17:1020.0 1.6 1
4-Aminobiphenyl ND ug/L 06/14/17 19:54 92-67-106/07/17 17:1020.0 1.7 1
Anthracene ND ug/L 06/14/17 19:54 120-12-706/07/17 17:1010.0 1.7 1
Benzo(a)anthracene ND ug/L 06/14/17 19:54 56-55-306/07/17 17:1010.0 2.1 1
Benzo(a)pyrene ND ug/L 06/14/17 19:54 50-32-806/07/17 17:1010.0 2.2 1
Benzo(b)fluoranthene ND ug/L 06/14/17 19:54 205-99-206/07/17 17:1010.0 2.2 1
Benzo(g,h,i)perylene ND ug/L 06/14/17 19:54 191-24-206/07/17 17:1010.0 2.1 1
Benzo(k)fluoranthene ND ug/L 06/14/17 19:54 207-08-906/07/17 17:1010.0 2.0 1
Benzyl alcohol ND ug/L 06/14/17 19:54 100-51-606/07/17 17:1020.0 3.1 1
4-Bromophenylphenyl ether ND ug/L 06/14/17 19:54 101-55-306/07/17 17:1010.0 1.5 1
Butylbenzylphthalate ND ug/L 06/14/17 19:54 85-68-706/07/17 17:1010.0 2.5 1
4-Chloro-3-methylphenol ND ug/L 06/14/17 19:54 59-50-706/07/17 17:1020.0 2.8 1
4-Chloroaniline ND ug/L 06/14/17 19:54 106-47-806/07/17 17:1020.0 2.8 1
Chlorobenzilate ND ug/L 06/14/17 19:54 510-15-606/07/17 17:1010.0 2.2 1
bis(2-Chloroethoxy)methane ND ug/L 06/14/17 19:54 111-91-106/07/17 17:1010.0 1.6 1
bis(2-Chloroethyl) ether ND ug/L 06/14/17 19:54 111-44-406/07/17 17:1010.0 1.7 1
2-Chloronaphthalene ND ug/L 06/14/17 19:54 91-58-706/07/17 17:1010.0 1.6 1
2-Chlorophenol ND ug/L 06/14/17 19:54 95-57-806/07/17 17:1010.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/14/17 19:54 7005-72-306/07/17 17:1010.0 1.6 1
Chrysene ND ug/L 06/14/17 19:54 218-01-906/07/17 17:1010.0 2.1 1
Diallate ND ug/L 06/14/17 19:54 2303-16-406/07/17 17:1010.0 1.6 1
Dibenz(a,h)anthracene ND ug/L 06/14/17 19:54 53-70-306/07/17 17:1010.0 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-1 Lab ID:92342478004 Collected:06/01/17 12:35 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Dibenzofuran ND ug/L 06/14/17 19:54 132-64-906/07/17 17:1010.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 06/14/17 19:54 91-94-106/07/17 17:1020.0 3.9 1
2,4-Dichlorophenol ND ug/L 06/14/17 19:54 120-83-206/07/17 17:1010.0 1.6 1
2,6-Dichlorophenol ND ug/L 06/14/17 19:54 87-65-006/07/17 17:1010.0 1.5 1
Diethylphthalate ND ug/L 06/14/17 19:54 84-66-206/07/17 17:1060001.6 1
Dimethoate ND ug/L 06/14/17 19:54 60-51-506/07/17 17:1020.0 1.8 1
P-Dimethylaminoazobenzene ND ug/L 06/14/17 19:54 60-11-706/07/17 17:1010.0 1.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/14/17 19:54 57-97-606/07/17 17:1010.0 2.4 1
3,3'-Dimethylbenzidine ND ug/L 06/14/17 19:54 119-93-706/07/17 17:1010.0 3.9 1
2,4-Dimethylphenol ND ug/L 06/14/17 19:54 105-67-906/07/17 17:1010.0 1.6 1
Dimethylphthalate ND ug/L 06/14/17 19:54 131-11-306/07/17 17:1010.0 1.4 1
Di-n-butylphthalate ND ug/L 06/14/17 19:54 84-74-206/07/17 17:1010.0 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/14/17 19:54 534-52-106/07/17 17:1050.0 2.2 1
1,3-Dinitrobenzene ND ug/L 06/14/17 19:54 99-65-006/07/17 17:1020.0 1.3 1
2,4-Dinitrophenol ND ug/L 06/14/17 19:54 51-28-506/07/17 17:1050.0 5.1 1
2,4-Dinitrotoluene ND ug/L 06/14/17 19:54 121-14-206/07/17 17:1010.0 1.5 1
2,6-Dinitrotoluene ND ug/L 06/14/17 19:54 606-20-206/07/17 17:1010.0 1.4 1
Di-n-octylphthalate ND ug/L 06/14/17 19:54 117-84-006/07/17 17:1010.0 1.5 1
Diphenylamine ND ug/L 06/14/17 19:54 122-39-406/07/17 17:1010.0 1.4 1
Disulfoton ND ug/L 06/14/17 19:54 298-04-406/07/17 17:1010.0 1.5 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/14/17 19:54 117-81-706/07/17 17:1015.0 2.3 1
Ethyl methanesulfonate ND ug/L 06/14/17 19:54 62-50-006/07/17 17:1020.0 1.6 1
Famphur ND ug/L 06/14/17 19:54 52-85-706/07/17 17:1020.0 5.7 1
Fluoranthene ND ug/L 06/14/17 19:54 206-44-006/07/17 17:1010.0 2.2 1
Fluorene ND ug/L 06/14/17 19:54 86-73-706/07/17 17:1010.0 1.6 1
Hexachlorobenzene ND ug/L 06/14/17 19:54 118-74-106/07/17 17:1010.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 06/14/17 19:54 77-47-406/07/17 17:1010.0 1.3 1
Hexachloroethane ND ug/L 06/14/17 19:54 67-72-106/07/17 17:1010.0 1.8 1
Hexachloropropene ND ug/L 06/14/17 19:54 1888-71-706/07/17 17:1010.0 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/14/17 19:54 193-39-506/07/17 17:1010.0 2.0 1
Isodrin ND ug/L 06/14/17 19:54 465-73-606/07/17 17:1020.0 2.5 1
Isophorone ND ug/L 06/14/17 19:54 78-59-106/07/17 17:1010.0 1.5 1
Isosafrole ND ug/L 06/14/17 19:54 120-58-106/07/17 17:1010.0 1.5 1
Kepone ND ug/L 06/14/17 19:54 143-50-006/07/17 17:1020.0 4.5 1
Methapyrilene ND ug/L 06/14/17 19:54 91-80-506/07/17 17:101003.0 1
3-Methylcholanthrene ND ug/L 06/14/17 19:54 56-49-506/07/17 17:1010.0 2.7 1
Methyl methanesulfonate ND ug/L 06/14/17 19:54 66-27-306/07/17 17:1010.0 1.1 1
2-Methylnaphthalene ND ug/L 06/14/17 19:54 91-57-606/07/17 17:1010.0 1.4 1
Methyl parathion ND ug/L 06/14/17 19:54 298-00-006/07/17 17:1010.0 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 06/14/17 19:54 95-48-706/07/17 17:1010.0 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/14/17 19:54 15831-10-406/07/17 17:1010.0 1.4 1
1-Naphthalenamine ND ug/L 06/14/17 19:54 134-32-706/07/17 17:1010.0 1.3 1
2-Naphthalenamine ND ug/L 06/14/17 19:54 91-59-806/07/17 17:1010.0 2.2 1
1,4-Naphthoquinone ND ug/L 06/14/17 19:54 130-15-406/07/17 17:1010.0 0.99 1
2-Nitroaniline ND ug/L 06/14/17 19:54 88-74-406/07/17 17:1050.0 2.3 1
3-Nitroaniline ND ug/L 06/14/17 19:54 99-09-206/07/17 17:1050.0 2.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-1 Lab ID:92342478004 Collected:06/01/17 12:35 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Nitroaniline ND ug/L 06/14/17 19:54 100-01-606/07/17 17:1020.0 3.4 1
Nitrobenzene ND ug/L 06/14/17 19:54 98-95-306/07/17 17:1010.0 1.6 1
2-Nitrophenol ND ug/L 06/14/17 19:54 88-75-506/07/17 17:1010.0 1.6 1
4-Nitrophenol ND ug/L 06/14/17 19:54 100-02-706/07/17 17:1050.0 4.3 1
5-Nitro-o-toluidine ND ug/L 06/14/17 19:54 99-55-806/07/17 17:1010.0 1.9 1
N-Nitrosodiethylamine ND ug/L 06/14/17 19:54 55-18-506/07/17 17:1020.0 1.4 1
N-Nitrosodimethylamine ND ug/L 06/14/17 19:54 62-75-906/07/17 17:1010.0 1.6 1
N-Nitroso-di-n-butylamine ND ug/L 06/14/17 19:54 924-16-306/07/17 17:1010.0 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 06/14/17 19:54 621-64-706/07/17 17:1010.0 1.7 1
N-Nitrosodiphenylamine ND ug/L 06/14/17 19:54 86-30-606/07/17 17:1010.0 1.4 1
N-Nitrosomethylethylamine ND ug/L 06/14/17 19:54 10595-95-606/07/17 17:1010.0 1.4 1
N-Nitrosopiperidine ND ug/L 06/14/17 19:54 100-75-406/07/17 17:1020.0 1.7 1
N-Nitrosopyrrolidine ND ug/L 06/14/17 19:54 930-55-206/07/17 17:1010.0 1.7 1
O,O,O-Triethylphosphorothioate ND ug/L 06/14/17 19:54 126-68-106/07/17 17:1010.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/14/17 19:54 108-60-106/07/17 17:1010.0 1.8 1
Parathion (Ethyl parathion)ND ug/L 06/14/17 19:54 56-38-206/07/17 17:1010.0 1.5 1
Pentachlorobenzene ND ug/L 06/14/17 19:54 608-93-506/07/17 17:1010.0 1.5 1
Pentachloronitrobenzene ND ug/L 06/14/17 19:54 82-68-806/07/17 17:1020.0 1.7 1
Pentachlorophenol ND ug/L 06/14/17 19:54 87-86-506/07/17 17:1025.0 3.5 1
Phenacetin ND ug/L 06/14/17 19:54 62-44-206/07/17 17:1020.0 1.9 1
Phenanthrene ND ug/L 06/14/17 19:54 85-01-806/07/17 17:1010.0 1.6 1
Phenol ND ug/L 06/14/17 19:54 108-95-206/07/17 17:1010.0 1.3 1
p-Phenylenediamine ND ug/L 06/14/17 19:54 106-50-306/07/17 17:1010.0 2.2 1
Phorate ND ug/L 06/14/17 19:54 298-02-206/07/17 17:1010.0 1.7 1
Pronamide ND ug/L 06/14/17 19:54 23950-58-506/07/17 17:1010.0 2.0 1
Pyrene ND ug/L 06/14/17 19:54 129-00-006/07/17 17:1010.0 2.2 1
Safrole ND ug/L 06/14/17 19:54 94-59-706/07/17 17:1010.0 1.3 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/14/17 19:54 95-94-306/07/17 17:1010.0 1.3 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/14/17 19:54 58-90-206/07/17 17:1010.0 2.9 1
Thionazin ND ug/L 06/14/17 19:54 297-97-206/07/17 17:1020.0 1.7 1
O-Toluidine ND ug/L 06/14/17 19:54 95-53-406/07/17 17:1010.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 06/14/17 19:54 95-95-406/07/17 17:1010.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/14/17 19:54 88-06-206/07/17 17:1010.0 1.4 1
1,3,5-Trinitrobenzene ND ug/L 06/14/17 19:54 99-35-406/07/17 17:1010.0 1.2 1
Surrogates
Nitrobenzene-d5 (S)63 %06/14/17 19:54 4165-60-006/07/17 17:1021-110 1
2-Fluorobiphenyl (S)84 %06/14/17 19:54 321-60-806/07/17 17:1027-110 1
Terphenyl-d14 (S)82 %06/14/17 19:54 1718-51-006/07/17 17:1031-107 1
Phenol-d6 (S)25 %06/14/17 19:54 13127-88-306/07/17 17:1010-110 1
2-Fluorophenol (S)38 %06/14/17 19:54 367-12-406/07/17 17:1012-110 1
2,4,6-Tribromophenol (S)74 %06/14/17 19:54 118-79-606/07/17 17:1027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/04/17 22:05 67-64-110010.0 1
Acetonitrile ND ug/L 06/04/17 22:05 75-05-855.0 2.2 1
Acrolein ND ug/L 06/04/17 22:05 107-02-853.0 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-1 Lab ID:92342478004 Collected:06/01/17 12:35 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acrylonitrile ND ug/L 06/04/17 22:05 107-13-12001.9 1
Allyl chloride ND ug/L 06/04/17 22:05 107-05-110.0 1.5 1
Benzene ND ug/L 06/04/17 22:05 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 22:05 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 22:05 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 22:05 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 22:05 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 22:05 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 22:05 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 22:05 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/17 22:05 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 22:05 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 22:05 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/17 22:05 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/04/17 22:05 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 22:05 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 22:05 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 22:05 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 22:05 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 22:05 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/04/17 22:05 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/04/17 22:05 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 22:05 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/04/17 22:05 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/04/17 22:05 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 22:05 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 22:05 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/17 22:05 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 22:05 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 22:05 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/04/17 22:05 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/04/17 22:05 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/04/17 22:05 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/04/17 22:05 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 22:05 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 22:05 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/04/17 22:05 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/04/17 22:05 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/04/17 22:05 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 22:05 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/04/17 22:05 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/04/17 22:05 126-98-71000.93 1
Methylene Chloride ND ug/L 06/04/17 22:05 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/04/17 22:05 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 22:05 108-10-11000.33 1
Naphthalene ND ug/L 06/04/17 22:05 91-20-310.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 21 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-1 Lab ID:92342478004 Collected:06/01/17 12:35 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Propionitrile ND ug/L 06/04/17 22:05 107-12-01503.6 1
Styrene ND ug/L 06/04/17 22:05 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 22:05 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 22:05 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 22:05 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 22:05 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/04/17 22:05 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/04/17 22:05 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 22:05 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 22:05 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 22:05 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 22:05 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 22:05 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 22:05 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/17 22:05 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)116 %06/04/17 22:05 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %06/04/17 22:05 17060-07-070-130 1
Toluene-d8 (S)110 %06/04/17 22:05 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-9 Lab ID:92342478005 Collected:06/01/17 15:40 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/06/17 13:10 309-00-206/05/17 17:300.050 0.050 1
alpha-BHC ND ug/L 06/06/17 13:10 319-84-606/05/17 17:300.050 0.050 1
beta-BHC ND ug/L 06/06/17 13:10 319-85-706/05/17 17:300.050 0.050 1
delta-BHC ND ug/L 06/06/17 13:10 319-86-806/05/17 17:300.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/06/17 13:10 58-89-906/05/17 17:300.050 0.050 1
Chlordane (Technical)ND ug/L 06/06/17 13:10 57-74-906/05/17 17:300.50 0.20 1
4,4'-DDD ND ug/L 06/06/17 13:10 72-54-806/05/17 17:300.10 0.050 1
4,4'-DDE ND ug/L 06/06/17 13:10 72-55-906/05/17 17:300.10 0.050 1
4,4'-DDT ND ug/L 06/06/17 13:10 50-29-306/05/17 17:300.10 0.050 1
Dieldrin ND ug/L 06/06/17 13:10 60-57-106/05/17 17:300.075 0.050 1
Endosulfan I ND ug/L 06/06/17 13:10 959-98-806/05/17 17:300.10 0.050 1
Endosulfan II ND ug/L 06/06/17 13:10 33213-65-906/05/17 17:300.10 0.050 1
Endosulfan sulfate ND ug/L 06/06/17 13:10 1031-07-806/05/17 17:300.10 0.050 1
Endrin ND ug/L 06/06/17 13:10 72-20-806/05/17 17:300.10 0.050 1
Endrin aldehyde ND ug/L 06/06/17 13:10 7421-93-406/05/17 17:300.10 0.050 1
Heptachlor ND ug/L 06/06/17 13:10 76-44-806/05/17 17:300.050 0.050 1
Heptachlor epoxide ND ug/L 06/06/17 13:10 1024-57-306/05/17 17:300.075 0.050 1
Methoxychlor ND ug/L 06/06/17 13:10 72-43-506/05/17 17:301.0 0.15 1
Toxaphene ND ug/L 06/06/17 13:10 8001-35-206/05/17 17:301.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)65 %06/06/17 13:10 877-09-806/05/17 17:3020-130 1
Decachlorobiphenyl (S)67 %06/06/17 13:10 2051-24-306/05/17 17:3020-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/06/17 19:50 12674-11-206/05/17 17:300.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/06/17 19:50 11104-28-206/05/17 17:300.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/06/17 19:50 11141-16-506/05/17 17:300.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/06/17 19:50 53469-21-906/05/17 17:300.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/06/17 19:50 12672-29-606/05/17 17:300.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/06/17 19:50 11097-69-106/05/17 17:300.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/06/17 19:50 11096-82-506/05/17 17:300.50 0.50 1
Surrogates
Decachlorobiphenyl (S)69 %06/06/17 19:50 2051-24-306/05/17 17:3010-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/10/17 05:06 94-75-706/07/17 16:000.98 0.23 1
Dinoseb ND ug/L 06/10/17 05:06 88-85-706/07/17 16:000.20 0.059 1
Pentachlorophenol ND ug/L 06/10/17 05:06 87-86-506/07/17 16:000.030 0.018 1
2,4,5-T ND ug/L 06/10/17 05:06 93-76-506/07/17 16:000.20 0.044 1
2,4,5-TP (Silvex)ND ug/L 06/10/17 05:06 93-72-106/07/17 16:000.20 0.051 1
Surrogates
2,4-DCAA (S)88 %06/10/17 05:06 19719-28-906/07/17 16:0039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/14/17 22:47 7440-36-006/04/17 16:406.0 3.9 1
Arsenic ND ug/L 06/14/17 22:47 7440-38-206/04/17 16:4010.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-9 Lab ID:92342478005 Collected:06/01/17 15:40 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Barium 48.2J ug/L 06/14/17 22:47 7440-39-306/04/17 16:401002.5 1
Beryllium ND ug/L 06/14/17 22:47 7440-41-706/04/17 16:401.0 0.50 1
Cadmium ND ug/L 06/14/17 22:47 7440-43-906/04/17 16:401.0 0.50 1
Chromium ND ug/L 06/14/17 22:47 7440-47-306/04/17 16:4010.0 2.5 1
Cobalt 166 ug/L 06/14/17 22:47 7440-48-406/04/17 16:4010.0 2.5 1
Copper ND ug/L 06/14/17 22:47 7440-50-806/04/17 16:4010.0 2.5 1
Lead ND ug/L 06/14/17 22:47 7439-92-106/04/17 16:4010.0 2.5 1
Nickel 6.6J ug/L 06/14/17 22:47 7440-02-006/04/17 16:4050.0 2.5 1
Selenium ND ug/L 06/14/17 22:47 7782-49-206/04/17 16:4010.0 5.0 1
Silver ND ug/L 06/14/17 22:47 7440-22-406/04/17 16:4010.0 2.5 1
Tin ND ug/L 06/14/17 22:47 7440-31-506/04/17 16:401002.5 1
Vanadium ND ug/L 06/14/17 22:47 7440-62-206/04/17 16:4025.0 2.5 1
Zinc 38.3 ug/L 06/14/17 22:47 7440-66-606/04/17 16:4010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.33J ug/L 06/09/17 16:31 7440-28-006/03/17 02:255.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/06/17 10:09 7439-97-606/05/17 20:000.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/14/17 20:23 83-32-906/07/17 17:1010.0 1.6 1
Acenaphthylene ND ug/L 06/14/17 20:23 208-96-806/07/17 17:1010.0 1.5 1
Acetophenone ND ug/L 06/14/17 20:23 98-86-206/07/17 17:1010.0 1.9 1
2-Acetylaminofluorene ND ug/L 06/14/17 20:23 53-96-3 L206/07/17 17:1020.0 1.6 1
4-Aminobiphenyl ND ug/L 06/14/17 20:23 92-67-106/07/17 17:1020.0 1.7 1
Anthracene ND ug/L 06/14/17 20:23 120-12-706/07/17 17:1010.0 1.7 1
Benzo(a)anthracene ND ug/L 06/14/17 20:23 56-55-306/07/17 17:1010.0 2.1 1
Benzo(a)pyrene ND ug/L 06/14/17 20:23 50-32-806/07/17 17:1010.0 2.2 1
Benzo(b)fluoranthene ND ug/L 06/14/17 20:23 205-99-206/07/17 17:1010.0 2.2 1
Benzo(g,h,i)perylene ND ug/L 06/14/17 20:23 191-24-206/07/17 17:1010.0 2.1 1
Benzo(k)fluoranthene ND ug/L 06/14/17 20:23 207-08-906/07/17 17:1010.0 2.0 1
Benzyl alcohol ND ug/L 06/14/17 20:23 100-51-606/07/17 17:1020.0 3.1 1
4-Bromophenylphenyl ether ND ug/L 06/14/17 20:23 101-55-306/07/17 17:1010.0 1.5 1
Butylbenzylphthalate ND ug/L 06/14/17 20:23 85-68-706/07/17 17:1010.0 2.5 1
4-Chloro-3-methylphenol ND ug/L 06/14/17 20:23 59-50-706/07/17 17:1020.0 2.8 1
4-Chloroaniline ND ug/L 06/14/17 20:23 106-47-806/07/17 17:1020.0 2.8 1
Chlorobenzilate ND ug/L 06/14/17 20:23 510-15-606/07/17 17:1010.0 2.2 1
bis(2-Chloroethoxy)methane ND ug/L 06/14/17 20:23 111-91-106/07/17 17:1010.0 1.6 1
bis(2-Chloroethyl) ether ND ug/L 06/14/17 20:23 111-44-406/07/17 17:1010.0 1.7 1
2-Chloronaphthalene ND ug/L 06/14/17 20:23 91-58-706/07/17 17:1010.0 1.6 1
2-Chlorophenol ND ug/L 06/14/17 20:23 95-57-806/07/17 17:1010.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/14/17 20:23 7005-72-306/07/17 17:1010.0 1.6 1
Chrysene ND ug/L 06/14/17 20:23 218-01-906/07/17 17:1010.0 2.1 1
Diallate ND ug/L 06/14/17 20:23 2303-16-406/07/17 17:1010.0 1.6 1
Dibenz(a,h)anthracene ND ug/L 06/14/17 20:23 53-70-306/07/17 17:1010.0 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-9 Lab ID:92342478005 Collected:06/01/17 15:40 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Dibenzofuran ND ug/L 06/14/17 20:23 132-64-906/07/17 17:1010.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 06/14/17 20:23 91-94-106/07/17 17:1020.0 3.9 1
2,4-Dichlorophenol ND ug/L 06/14/17 20:23 120-83-206/07/17 17:1010.0 1.6 1
2,6-Dichlorophenol ND ug/L 06/14/17 20:23 87-65-006/07/17 17:1010.0 1.5 1
Diethylphthalate ND ug/L 06/14/17 20:23 84-66-206/07/17 17:1060001.6 1
Dimethoate ND ug/L 06/14/17 20:23 60-51-506/07/17 17:1020.0 1.8 1
P-Dimethylaminoazobenzene ND ug/L 06/14/17 20:23 60-11-706/07/17 17:1010.0 1.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/14/17 20:23 57-97-606/07/17 17:1010.0 2.4 1
3,3'-Dimethylbenzidine ND ug/L 06/14/17 20:23 119-93-706/07/17 17:1010.0 3.9 1
2,4-Dimethylphenol ND ug/L 06/14/17 20:23 105-67-906/07/17 17:1010.0 1.6 1
Dimethylphthalate ND ug/L 06/14/17 20:23 131-11-306/07/17 17:1010.0 1.4 1
Di-n-butylphthalate ND ug/L 06/14/17 20:23 84-74-206/07/17 17:1010.0 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/14/17 20:23 534-52-106/07/17 17:1050.0 2.2 1
1,3-Dinitrobenzene ND ug/L 06/14/17 20:23 99-65-006/07/17 17:1020.0 1.3 1
2,4-Dinitrophenol ND ug/L 06/14/17 20:23 51-28-506/07/17 17:1050.0 5.1 1
2,4-Dinitrotoluene ND ug/L 06/14/17 20:23 121-14-206/07/17 17:1010.0 1.5 1
2,6-Dinitrotoluene ND ug/L 06/14/17 20:23 606-20-206/07/17 17:1010.0 1.4 1
Di-n-octylphthalate ND ug/L 06/14/17 20:23 117-84-006/07/17 17:1010.0 1.5 1
Diphenylamine ND ug/L 06/14/17 20:23 122-39-406/07/17 17:1010.0 1.4 1
Disulfoton ND ug/L 06/14/17 20:23 298-04-406/07/17 17:1010.0 1.5 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/14/17 20:23 117-81-706/07/17 17:1015.0 2.3 1
Ethyl methanesulfonate ND ug/L 06/14/17 20:23 62-50-006/07/17 17:1020.0 1.6 1
Famphur ND ug/L 06/14/17 20:23 52-85-706/07/17 17:1020.0 5.7 1
Fluoranthene ND ug/L 06/14/17 20:23 206-44-006/07/17 17:1010.0 2.2 1
Fluorene ND ug/L 06/14/17 20:23 86-73-706/07/17 17:1010.0 1.6 1
Hexachlorobenzene ND ug/L 06/14/17 20:23 118-74-106/07/17 17:1010.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 06/14/17 20:23 77-47-406/07/17 17:1010.0 1.3 1
Hexachloroethane ND ug/L 06/14/17 20:23 67-72-106/07/17 17:1010.0 1.8 1
Hexachloropropene ND ug/L 06/14/17 20:23 1888-71-706/07/17 17:1010.0 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/14/17 20:23 193-39-506/07/17 17:1010.0 2.0 1
Isodrin ND ug/L 06/14/17 20:23 465-73-606/07/17 17:1020.0 2.5 1
Isophorone ND ug/L 06/14/17 20:23 78-59-106/07/17 17:1010.0 1.5 1
Isosafrole ND ug/L 06/14/17 20:23 120-58-106/07/17 17:1010.0 1.5 1
Kepone ND ug/L 06/14/17 20:23 143-50-006/07/17 17:1020.0 4.5 1
Methapyrilene ND ug/L 06/14/17 20:23 91-80-506/07/17 17:101003.0 1
3-Methylcholanthrene ND ug/L 06/14/17 20:23 56-49-506/07/17 17:1010.0 2.7 1
Methyl methanesulfonate ND ug/L 06/14/17 20:23 66-27-306/07/17 17:1010.0 1.1 1
2-Methylnaphthalene ND ug/L 06/14/17 20:23 91-57-606/07/17 17:1010.0 1.4 1
Methyl parathion ND ug/L 06/14/17 20:23 298-00-006/07/17 17:1010.0 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 06/14/17 20:23 95-48-706/07/17 17:1010.0 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/14/17 20:23 15831-10-406/07/17 17:1010.0 1.4 1
1-Naphthalenamine ND ug/L 06/14/17 20:23 134-32-706/07/17 17:1010.0 1.3 1
2-Naphthalenamine ND ug/L 06/14/17 20:23 91-59-806/07/17 17:1010.0 2.2 1
1,4-Naphthoquinone ND ug/L 06/14/17 20:23 130-15-406/07/17 17:1010.0 0.99 1
2-Nitroaniline ND ug/L 06/14/17 20:23 88-74-406/07/17 17:1050.0 2.3 1
3-Nitroaniline ND ug/L 06/14/17 20:23 99-09-206/07/17 17:1050.0 2.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-9 Lab ID:92342478005 Collected:06/01/17 15:40 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Nitroaniline ND ug/L 06/14/17 20:23 100-01-606/07/17 17:1020.0 3.4 1
Nitrobenzene ND ug/L 06/14/17 20:23 98-95-306/07/17 17:1010.0 1.6 1
2-Nitrophenol ND ug/L 06/14/17 20:23 88-75-506/07/17 17:1010.0 1.6 1
4-Nitrophenol ND ug/L 06/14/17 20:23 100-02-706/07/17 17:1050.0 4.3 1
5-Nitro-o-toluidine ND ug/L 06/14/17 20:23 99-55-806/07/17 17:1010.0 1.9 1
N-Nitrosodiethylamine ND ug/L 06/14/17 20:23 55-18-506/07/17 17:1020.0 1.4 1
N-Nitrosodimethylamine ND ug/L 06/14/17 20:23 62-75-906/07/17 17:1010.0 1.6 1
N-Nitroso-di-n-butylamine ND ug/L 06/14/17 20:23 924-16-306/07/17 17:1010.0 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 06/14/17 20:23 621-64-706/07/17 17:1010.0 1.7 1
N-Nitrosodiphenylamine ND ug/L 06/14/17 20:23 86-30-606/07/17 17:1010.0 1.4 1
N-Nitrosomethylethylamine ND ug/L 06/14/17 20:23 10595-95-606/07/17 17:1010.0 1.4 1
N-Nitrosopiperidine ND ug/L 06/14/17 20:23 100-75-406/07/17 17:1020.0 1.7 1
N-Nitrosopyrrolidine ND ug/L 06/14/17 20:23 930-55-206/07/17 17:1010.0 1.7 1
O,O,O-Triethylphosphorothioate ND ug/L 06/14/17 20:23 126-68-106/07/17 17:1010.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/14/17 20:23 108-60-106/07/17 17:1010.0 1.8 1
Parathion (Ethyl parathion)ND ug/L 06/14/17 20:23 56-38-206/07/17 17:1010.0 1.5 1
Pentachlorobenzene ND ug/L 06/14/17 20:23 608-93-506/07/17 17:1010.0 1.5 1
Pentachloronitrobenzene ND ug/L 06/14/17 20:23 82-68-806/07/17 17:1020.0 1.7 1
Pentachlorophenol ND ug/L 06/14/17 20:23 87-86-506/07/17 17:1025.0 3.5 1
Phenacetin ND ug/L 06/14/17 20:23 62-44-206/07/17 17:1020.0 1.9 1
Phenanthrene ND ug/L 06/14/17 20:23 85-01-806/07/17 17:1010.0 1.6 1
Phenol ND ug/L 06/14/17 20:23 108-95-206/07/17 17:1010.0 1.3 1
p-Phenylenediamine ND ug/L 06/14/17 20:23 106-50-306/07/17 17:1010.0 2.2 1
Phorate ND ug/L 06/14/17 20:23 298-02-206/07/17 17:1010.0 1.7 1
Pronamide ND ug/L 06/14/17 20:23 23950-58-506/07/17 17:1010.0 2.0 1
Pyrene ND ug/L 06/14/17 20:23 129-00-006/07/17 17:1010.0 2.2 1
Safrole ND ug/L 06/14/17 20:23 94-59-706/07/17 17:1010.0 1.3 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/14/17 20:23 95-94-306/07/17 17:1010.0 1.3 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/14/17 20:23 58-90-206/07/17 17:1010.0 2.9 1
Thionazin ND ug/L 06/14/17 20:23 297-97-206/07/17 17:1020.0 1.7 1
O-Toluidine ND ug/L 06/14/17 20:23 95-53-406/07/17 17:1010.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 06/14/17 20:23 95-95-406/07/17 17:1010.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/14/17 20:23 88-06-206/07/17 17:1010.0 1.4 1
1,3,5-Trinitrobenzene ND ug/L 06/14/17 20:23 99-35-406/07/17 17:1010.0 1.2 1
Surrogates
Nitrobenzene-d5 (S)70 %06/14/17 20:23 4165-60-006/07/17 17:1021-110 1
2-Fluorobiphenyl (S)84 %06/14/17 20:23 321-60-806/07/17 17:1027-110 1
Terphenyl-d14 (S)84 %06/14/17 20:23 1718-51-006/07/17 17:1031-107 1
Phenol-d6 (S)24 %06/14/17 20:23 13127-88-306/07/17 17:1010-110 1
2-Fluorophenol (S)38 %06/14/17 20:23 367-12-406/07/17 17:1012-110 1
2,4,6-Tribromophenol (S)78 %06/14/17 20:23 118-79-606/07/17 17:1027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 29.5J ug/L 06/04/17 22:23 67-64-110010.0 1
Acetonitrile ND ug/L 06/04/17 22:23 75-05-855.0 2.2 1
Acrolein 2.1J ug/L 06/04/17 22:23 107-02-853.0 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-9 Lab ID:92342478005 Collected:06/01/17 15:40 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acrylonitrile ND ug/L 06/04/17 22:23 107-13-12001.9 1
Allyl chloride ND ug/L 06/04/17 22:23 107-05-110.0 1.5 1
Benzene 2.4 ug/L 06/04/17 22:23 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 22:23 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 22:23 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 22:23 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 22:23 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 22:23 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 22:23 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 22:23 56-23-51.0 0.25 1
Chlorobenzene 2.2J ug/L 06/04/17 22:23 108-90-73.0 0.23 1
Chloroethane 1.9J ug/L 06/04/17 22:23 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 22:23 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/17 22:23 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/04/17 22:23 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 22:23 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 22:23 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 22:23 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 22:23 74-95-310.0 0.21 1
1,2-Dichlorobenzene 1.5J ug/L 06/04/17 22:23 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/04/17 22:23 541-73-15.0 0.24 1
1,4-Dichlorobenzene 5.7 ug/L 06/04/17 22:23 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 22:23 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/04/17 22:23 75-71-85.0 0.21 1
1,1-Dichloroethane 2.4J ug/L 06/04/17 22:23 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 22:23 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 22:23 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 19.7 ug/L 06/04/17 22:23 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 22:23 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 22:23 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/04/17 22:23 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/04/17 22:23 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/04/17 22:23 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/04/17 22:23 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 22:23 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 22:23 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/04/17 22:23 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/04/17 22:23 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/04/17 22:23 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 22:23 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/04/17 22:23 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/04/17 22:23 126-98-71000.93 1
Methylene Chloride ND ug/L 06/04/17 22:23 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/04/17 22:23 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 22:23 108-10-11000.33 1
Naphthalene ND ug/L 06/04/17 22:23 91-20-310.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-9 Lab ID:92342478005 Collected:06/01/17 15:40 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Propionitrile ND ug/L 06/04/17 22:23 107-12-01503.6 1
Styrene ND ug/L 06/04/17 22:23 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 22:23 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 22:23 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 22:23 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 22:23 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/04/17 22:23 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/04/17 22:23 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 22:23 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 22:23 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 22:23 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 22:23 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 22:23 108-05-450.0 0.35 1
Vinyl chloride 18.7 ug/L 06/04/17 22:23 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/17 22:23 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)107 %06/04/17 22:23 460-00-470-130 1
1,2-Dichloroethane-d4 (S)93 %06/04/17 22:23 17060-07-070-130 1
Toluene-d8 (S)109 %06/04/17 22:23 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-7 Lab ID:92342478006 Collected:06/01/17 14:45 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/14/17 22:50 7440-36-006/04/17 16:406.0 3.9 1
Arsenic ND ug/L 06/14/17 22:50 7440-38-206/04/17 16:4010.0 5.0 1
Barium 55.1J ug/L 06/14/17 22:50 7440-39-306/04/17 16:401002.5 1
Beryllium ND ug/L 06/14/17 22:50 7440-41-706/04/17 16:401.0 0.50 1
Cadmium ND ug/L 06/14/17 22:50 7440-43-906/04/17 16:401.0 0.50 1
Chromium ND ug/L 06/14/17 22:50 7440-47-306/04/17 16:4010.0 2.5 1
Cobalt 50.7 ug/L 06/14/17 22:50 7440-48-406/04/17 16:4010.0 2.5 1
Copper ND ug/L 06/14/17 22:50 7440-50-806/04/17 16:4010.0 2.5 1
Lead ND ug/L 06/14/17 22:50 7439-92-106/04/17 16:4010.0 2.5 1
Nickel ND ug/L 06/14/17 22:50 7440-02-006/04/17 16:4050.0 2.5 1
Selenium ND ug/L 06/14/17 22:50 7782-49-206/04/17 16:4010.0 5.0 1
Silver ND ug/L 06/14/17 22:50 7440-22-406/04/17 16:4010.0 2.5 1
Vanadium ND ug/L 06/14/17 22:50 7440-62-206/04/17 16:4025.0 2.5 1
Zinc 10.7 ug/L 06/14/17 22:50 7440-66-606/04/17 16:4010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.11J ug/L 06/09/17 16:33 7440-28-006/03/17 02:255.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/04/17 22:41 67-64-110010.0 1
Acrylonitrile ND ug/L 06/04/17 22:41 107-13-12001.9 1
Benzene 0.30J ug/L 06/04/17 22:41 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 22:41 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 22:41 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 22:41 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 22:41 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 22:41 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 22:41 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 22:41 56-23-51.0 0.25 1
Chlorobenzene 3.9 ug/L 06/04/17 22:41 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 22:41 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 22:41 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/17 22:41 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 22:41 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 22:41 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 22:41 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 22:41 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 22:41 95-50-15.0 0.30 1
1,4-Dichlorobenzene 2.2 ug/L 06/04/17 22:41 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 22:41 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/04/17 22:41 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 22:41 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 22:41 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.28J ug/L 06/04/17 22:41 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 22:41 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 22:41 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-7 Lab ID:92342478006 Collected:06/01/17 14:45 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 06/04/17 22:41 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 22:41 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 22:41 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/04/17 22:41 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 22:41 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/04/17 22:41 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 22:41 108-10-11000.33 1
Styrene ND ug/L 06/04/17 22:41 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 22:41 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 22:41 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 22:41 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 22:41 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/04/17 22:41 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 22:41 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 22:41 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 22:41 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 22:41 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 22:41 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 22:41 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/17 22:41 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)108 %06/04/17 22:41 460-00-470-130 1
1,2-Dichloroethane-d4 (S)89 %06/04/17 22:41 17060-07-070-130 1
Toluene-d8 (S)110 %06/04/17 22:41 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-12S Lab ID:92342478007 Collected:06/01/17 09:50 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/09/17 18:50 7440-36-006/04/17 17:056.0 3.9 1
Arsenic ND ug/L 06/09/17 18:50 7440-38-206/04/17 17:0510.0 5.0 1
Barium 23.5J ug/L 06/09/17 18:50 7440-39-306/04/17 17:051002.5 1
Beryllium ND ug/L 06/09/17 18:50 7440-41-706/04/17 17:051.0 0.50 1
Cadmium 0.66J ug/L 06/09/17 18:50 7440-43-906/04/17 17:051.0 0.50 1
Chromium ND ug/L 06/09/17 18:50 7440-47-306/04/17 17:0510.0 2.5 1
Cobalt ND ug/L 06/09/17 18:50 7440-48-406/04/17 17:0510.0 2.5 1
Copper 3.5J ug/L 06/09/17 18:50 7440-50-806/04/17 17:0510.0 2.5 1
Lead ND ug/L 06/09/17 18:50 7439-92-106/04/17 17:0510.0 2.5 1
Nickel 2.8J ug/L 06/09/17 18:50 7440-02-006/04/17 17:0550.0 2.5 1
Selenium ND ug/L 06/09/17 18:50 7782-49-206/04/17 17:0510.0 5.0 1
Silver ND ug/L 06/09/17 18:50 7440-22-406/04/17 17:0510.0 2.5 1
Vanadium ND ug/L 06/09/17 18:50 7440-62-206/04/17 17:0525.0 2.5 1
Zinc 6.6J ug/L 06/09/17 18:50 7440-66-606/04/17 17:0510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/09/17 16:44 7440-28-006/03/17 02:255.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/04/17 22:58 67-64-110010.0 1
Acrylonitrile ND ug/L 06/04/17 22:58 107-13-12001.9 1
Benzene ND ug/L 06/04/17 22:58 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 22:58 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 22:58 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 22:58 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 22:58 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 22:58 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 22:58 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 22:58 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/17 22:58 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 22:58 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 22:58 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/17 22:58 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 22:58 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 22:58 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 22:58 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 22:58 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 22:58 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/04/17 22:58 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 22:58 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/04/17 22:58 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 22:58 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 22:58 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/17 22:58 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 22:58 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 22:58 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-12S Lab ID:92342478007 Collected:06/01/17 09:50 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 06/04/17 22:58 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 22:58 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 22:58 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/04/17 22:58 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 22:58 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/04/17 22:58 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 22:58 108-10-11000.33 1
Styrene ND ug/L 06/04/17 22:58 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 22:58 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 22:58 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 22:58 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 22:58 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/04/17 22:58 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 22:58 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 22:58 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 22:58 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 22:58 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 22:58 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 22:58 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/17 22:58 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %06/04/17 22:58 460-00-470-130 1
1,2-Dichloroethane-d4 (S)87 %06/04/17 22:58 17060-07-070-130 1
Toluene-d8 (S)107 %06/04/17 22:58 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-14 Lab ID:92342478008 Collected:06/01/17 09:00 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/09/17 19:08 7440-36-006/04/17 17:056.0 3.9 1
Arsenic ND ug/L 06/09/17 19:08 7440-38-206/04/17 17:0510.0 5.0 1
Barium 84.0J ug/L 06/09/17 19:08 7440-39-306/04/17 17:051002.5 1
Beryllium ND ug/L 06/09/17 19:08 7440-41-706/04/17 17:051.0 0.50 1
Cadmium ND ug/L 06/09/17 19:08 7440-43-906/04/17 17:051.0 0.50 1
Chromium 12.4 ug/L 06/09/17 19:08 7440-47-306/04/17 17:0510.0 2.5 1
Cobalt 13.1 ug/L 06/09/17 19:08 7440-48-406/04/17 17:0510.0 2.5 1
Copper 6.9J ug/L 06/09/17 19:08 7440-50-806/04/17 17:0510.0 2.5 1
Lead 3.0J ug/L 06/09/17 19:08 7439-92-106/04/17 17:0510.0 2.5 1
Nickel 8.6J ug/L 06/09/17 19:08 7440-02-006/04/17 17:0550.0 2.5 1
Selenium ND ug/L 06/09/17 19:08 7782-49-206/04/17 17:0510.0 5.0 1
Silver ND ug/L 06/09/17 19:08 7440-22-406/04/17 17:0510.0 2.5 1
Vanadium 18.0J ug/L 06/09/17 19:08 7440-62-206/04/17 17:0525.0 2.5 1
Zinc 36.1 ug/L 06/09/17 19:08 7440-66-606/04/17 17:0510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.16J ug/L 06/09/17 16:46 7440-28-006/03/17 02:255.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 13.5J ug/L 06/04/17 23:16 67-64-110010.0 1
Acrylonitrile ND ug/L 06/04/17 23:16 107-13-12001.9 1
Benzene ND ug/L 06/04/17 23:16 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 23:16 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 23:16 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 23:16 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 23:16 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 23:16 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 23:16 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 23:16 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/17 23:16 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 23:16 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 23:16 67-66-35.0 0.14 1
Chloromethane 0.32J ug/L 06/04/17 23:16 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 23:16 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 23:16 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 23:16 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 23:16 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 23:16 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/04/17 23:16 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 23:16 110-57-61001.0 1
1,1-Dichloroethane 2.6J ug/L 06/04/17 23:16 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 23:16 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 23:16 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 4.0J ug/L 06/04/17 23:16 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 23:16 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 23:16 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-14 Lab ID:92342478008 Collected:06/01/17 09:00 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 06/04/17 23:16 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 23:16 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 23:16 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/04/17 23:16 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 23:16 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/04/17 23:16 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 23:16 108-10-11000.33 1
Styrene ND ug/L 06/04/17 23:16 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 23:16 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 23:16 79-34-53.0 0.40 1
Tetrachloroethene 0.54J ug/L 06/04/17 23:16 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 23:16 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/04/17 23:16 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 23:16 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 23:16 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 23:16 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 23:16 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 23:16 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 23:16 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/17 23:16 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %06/04/17 23:16 460-00-470-130 1
1,2-Dichloroethane-d4 (S)90 %06/04/17 23:16 17060-07-070-130 1
Toluene-d8 (S)108 %06/04/17 23:16 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-18 Lab ID:92342478009 Collected:06/01/17 10:15 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/09/17 19:11 7440-36-006/04/17 17:056.0 3.9 1
Arsenic ND ug/L 06/09/17 19:11 7440-38-206/04/17 17:0510.0 5.0 1
Barium 28.4J ug/L 06/09/17 19:11 7440-39-306/04/17 17:051002.5 1
Beryllium ND ug/L 06/09/17 19:11 7440-41-706/04/17 17:051.0 0.50 1
Cadmium ND ug/L 06/09/17 19:11 7440-43-906/04/17 17:051.0 0.50 1
Chromium 2.6J ug/L 06/09/17 19:11 7440-47-306/04/17 17:0510.0 2.5 1
Cobalt ND ug/L 06/09/17 19:11 7440-48-406/04/17 17:0510.0 2.5 1
Copper 122 ug/L 06/09/17 19:11 7440-50-806/04/17 17:0510.0 2.5 1
Lead 9.2J ug/L 06/09/17 19:11 7439-92-106/04/17 17:0510.0 2.5 1
Nickel ND ug/L 06/09/17 19:11 7440-02-006/04/17 17:0550.0 2.5 1
Selenium ND ug/L 06/09/17 19:11 7782-49-206/04/17 17:0510.0 5.0 1
Silver ND ug/L 06/09/17 19:11 7440-22-406/04/17 17:0510.0 2.5 1
Vanadium ND ug/L 06/09/17 19:11 7440-62-206/04/17 17:0525.0 2.5 1
Zinc 10.7 ug/L 06/09/17 19:11 7440-66-606/04/17 17:0510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/09/17 16:47 7440-28-006/03/17 02:255.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/04/17 23:34 67-64-110010.0 1
Acrylonitrile ND ug/L 06/04/17 23:34 107-13-12001.9 1
Benzene ND ug/L 06/04/17 23:34 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 23:34 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 23:34 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 23:34 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 23:34 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 23:34 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 23:34 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 23:34 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/17 23:34 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 23:34 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 23:34 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/17 23:34 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 23:34 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 23:34 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 23:34 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 23:34 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 23:34 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/04/17 23:34 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 23:34 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/04/17 23:34 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 23:34 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 23:34 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/17 23:34 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 23:34 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 23:34 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-18 Lab ID:92342478009 Collected:06/01/17 10:15 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 06/04/17 23:34 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 23:34 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 23:34 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/04/17 23:34 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 23:34 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/04/17 23:34 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 23:34 108-10-11000.33 1
Styrene ND ug/L 06/04/17 23:34 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 23:34 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 23:34 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 23:34 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 23:34 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/04/17 23:34 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 23:34 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 23:34 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 23:34 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 23:34 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 23:34 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 23:34 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/17 23:34 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %06/04/17 23:34 460-00-470-130 1
1,2-Dichloroethane-d4 (S)88 %06/04/17 23:34 17060-07-070-130 1
Toluene-d8 (S)115 %06/04/17 23:34 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-19 Lab ID:92342478010 Collected:05/31/17 09:00 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/09/17 19:15 7440-36-006/04/17 17:056.0 3.9 1
Arsenic ND ug/L 06/09/17 19:15 7440-38-206/04/17 17:0510.0 5.0 1
Barium 70.2J ug/L 06/09/17 19:15 7440-39-306/04/17 17:051002.5 1
Beryllium 0.61J ug/L 06/09/17 19:15 7440-41-706/04/17 17:051.0 0.50 1
Cadmium ND ug/L 06/09/17 19:15 7440-43-906/04/17 17:051.0 0.50 1
Chromium 5.6J ug/L 06/09/17 19:15 7440-47-306/04/17 17:0510.0 2.5 1
Cobalt 4.1J ug/L 06/09/17 19:15 7440-48-406/04/17 17:0510.0 2.5 1
Copper 4.4J ug/L 06/09/17 19:15 7440-50-806/04/17 17:0510.0 2.5 1
Lead 3.0J ug/L 06/09/17 19:15 7439-92-106/04/17 17:0510.0 2.5 1
Nickel ND ug/L 06/09/17 19:15 7440-02-006/04/17 17:0550.0 2.5 1
Selenium ND ug/L 06/09/17 19:15 7782-49-206/04/17 17:0510.0 5.0 1
Silver ND ug/L 06/09/17 19:15 7440-22-406/04/17 17:0510.0 2.5 1
Vanadium 8.2J ug/L 06/09/17 19:15 7440-62-206/04/17 17:0525.0 2.5 1
Zinc 20.2 ug/L 06/09/17 19:15 7440-66-606/04/17 17:0510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.081J ug/L 06/09/17 16:49 7440-28-006/03/17 02:255.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/04/17 23:52 67-64-110010.0 1
Acrylonitrile ND ug/L 06/04/17 23:52 107-13-12001.9 1
Benzene ND ug/L 06/04/17 23:52 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 23:52 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 23:52 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 23:52 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 23:52 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 23:52 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 23:52 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 23:52 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/17 23:52 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 23:52 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 23:52 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/17 23:52 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 23:52 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 23:52 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 23:52 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 23:52 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 23:52 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/04/17 23:52 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 23:52 110-57-61001.0 1
1,1-Dichloroethane 0.36J ug/L 06/04/17 23:52 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 23:52 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 23:52 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.65J ug/L 06/04/17 23:52 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 23:52 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 23:52 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-19 Lab ID:92342478010 Collected:05/31/17 09:00 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 06/04/17 23:52 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 23:52 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 23:52 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/04/17 23:52 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 23:52 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/04/17 23:52 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 23:52 108-10-11000.33 1
Styrene ND ug/L 06/04/17 23:52 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 23:52 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 23:52 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 23:52 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 23:52 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/04/17 23:52 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 23:52 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 23:52 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 23:52 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 23:52 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 23:52 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 23:52 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/17 23:52 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %06/04/17 23:52 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %06/04/17 23:52 17060-07-070-130 1
Toluene-d8 (S)109 %06/04/17 23:52 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-20 Lab ID:92342478011 Collected:06/01/17 15:30 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/09/17 19:18 7440-36-006/04/17 17:056.0 3.9 1
Arsenic ND ug/L 06/09/17 19:18 7440-38-206/04/17 17:0510.0 5.0 1
Barium 27.6J ug/L 06/09/17 19:18 7440-39-306/04/17 17:051002.5 1
Beryllium ND ug/L 06/09/17 19:18 7440-41-706/04/17 17:051.0 0.50 1
Cadmium ND ug/L 06/09/17 19:18 7440-43-906/04/17 17:051.0 0.50 1
Chromium ND ug/L 06/09/17 19:18 7440-47-306/04/17 17:0510.0 2.5 1
Cobalt 12.3 ug/L 06/09/17 19:18 7440-48-406/04/17 17:0510.0 2.5 1
Copper ND ug/L 06/09/17 19:18 7440-50-806/04/17 17:0510.0 2.5 1
Lead ND ug/L 06/09/17 19:18 7439-92-106/04/17 17:0510.0 2.5 1
Nickel ND ug/L 06/09/17 19:18 7440-02-006/04/17 17:0550.0 2.5 1
Selenium ND ug/L 06/09/17 19:18 7782-49-206/04/17 17:0510.0 5.0 1
Silver ND ug/L 06/09/17 19:18 7440-22-406/04/17 17:0510.0 2.5 1
Vanadium ND ug/L 06/09/17 19:18 7440-62-206/04/17 17:0525.0 2.5 1
Zinc 7.7J ug/L 06/09/17 19:18 7440-66-606/04/17 17:0510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.32J ug/L 06/09/17 16:51 7440-28-006/03/17 02:255.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 14.4J ug/L 06/05/17 00:27 67-64-1 M110010.0 1
Acrylonitrile ND ug/L 06/05/17 00:27 107-13-12001.9 1
Benzene ND ug/L 06/05/17 00:27 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/05/17 00:27 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/05/17 00:27 75-27-41.0 0.18 1
Bromoform ND ug/L 06/05/17 00:27 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/05/17 00:27 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/05/17 00:27 78-93-31000.96 1
Carbon disulfide ND ug/L 06/05/17 00:27 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/05/17 00:27 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/05/17 00:27 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/05/17 00:27 75-00-310.0 0.54 1
Chloroform ND ug/L 06/05/17 00:27 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/05/17 00:27 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/05/17 00:27 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/05/17 00:27 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/05/17 00:27 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/05/17 00:27 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/05/17 00:27 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/05/17 00:27 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/05/17 00:27 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/05/17 00:27 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/05/17 00:27 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/05/17 00:27 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.64J ug/L 06/05/17 00:27 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/05/17 00:27 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/05/17 00:27 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-20 Lab ID:92342478011 Collected:06/01/17 15:30 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 06/05/17 00:27 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/05/17 00:27 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/05/17 00:27 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/05/17 00:27 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/05/17 00:27 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/05/17 00:27 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/05/17 00:27 108-10-11000.33 1
Styrene ND ug/L 06/05/17 00:27 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/05/17 00:27 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/05/17 00:27 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/05/17 00:27 127-18-41.0 0.46 1
Toluene ND ug/L 06/05/17 00:27 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/05/17 00:27 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/05/17 00:27 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/05/17 00:27 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/05/17 00:27 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/05/17 00:27 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/05/17 00:27 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/05/17 00:27 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/05/17 00:27 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %06/05/17 00:27 460-00-470-130 1
1,2-Dichloroethane-d4 (S)89 %06/05/17 00:27 17060-07-070-130 1
Toluene-d8 (S)110 %06/05/17 00:27 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-13 Lab ID:92342530001 Collected:05/31/17 17:35 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/06/17 22:13 309-00-206/02/17 10:090.050 0.050 1
alpha-BHC ND ug/L 06/06/17 22:13 319-84-606/02/17 10:090.050 0.050 1
beta-BHC ND ug/L 06/06/17 22:13 319-85-706/02/17 10:090.050 0.050 1
delta-BHC ND ug/L 06/06/17 22:13 319-86-806/02/17 10:090.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/06/17 22:13 58-89-906/02/17 10:090.050 0.050 1
Chlordane (Technical)ND ug/L 06/06/17 22:13 57-74-906/02/17 10:090.50 0.20 1
4,4'-DDD ND ug/L 06/06/17 22:13 72-54-806/02/17 10:090.10 0.050 1
4,4'-DDE ND ug/L 06/06/17 22:13 72-55-906/02/17 10:090.10 0.050 1
4,4'-DDT ND ug/L 06/06/17 22:13 50-29-306/02/17 10:090.10 0.050 1
Dieldrin ND ug/L 06/06/17 22:13 60-57-106/02/17 10:090.075 0.050 1
Endosulfan I ND ug/L 06/06/17 22:13 959-98-806/02/17 10:090.10 0.050 1
Endosulfan II ND ug/L 06/06/17 22:13 33213-65-906/02/17 10:090.10 0.050 1
Endosulfan sulfate ND ug/L 06/06/17 22:13 1031-07-806/02/17 10:090.10 0.050 1
Endrin ND ug/L 06/06/17 22:13 72-20-806/02/17 10:090.10 0.050 1
Endrin aldehyde ND ug/L 06/06/17 22:13 7421-93-406/02/17 10:090.10 0.050 1
Heptachlor ND ug/L 06/06/17 22:13 76-44-806/02/17 10:090.050 0.050 1
Heptachlor epoxide ND ug/L 06/06/17 22:13 1024-57-306/02/17 10:090.075 0.050 1
Methoxychlor ND ug/L 06/06/17 22:13 72-43-506/02/17 10:091.0 0.15 1
Toxaphene ND ug/L 06/06/17 22:13 8001-35-206/02/17 10:091.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)53 %06/06/17 22:13 877-09-806/02/17 10:0920-130 1
Decachlorobiphenyl (S)50 %06/06/17 22:13 2051-24-306/02/17 10:0920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/03/17 20:42 12674-11-206/02/17 10:090.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/03/17 20:42 11104-28-206/02/17 10:090.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/03/17 20:42 11141-16-506/02/17 10:090.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/03/17 20:42 53469-21-906/02/17 10:090.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/03/17 20:42 12672-29-606/02/17 10:090.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/03/17 20:42 11097-69-106/02/17 10:090.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/03/17 20:42 11096-82-506/02/17 10:090.50 0.50 1
Surrogates
Decachlorobiphenyl (S)44 %06/03/17 20:42 2051-24-306/02/17 10:0910-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/10/17 00:39 94-75-706/07/17 16:001.0 0.24 1
Dinoseb ND ug/L 06/10/17 00:39 88-85-706/07/17 16:000.20 0.061 1
Pentachlorophenol ND ug/L 06/10/17 00:39 87-86-506/07/17 16:000.030 0.018 1
2,4,5-T ND ug/L 06/10/17 00:39 93-76-506/07/17 16:000.20 0.045 1
2,4,5-TP (Silvex)ND ug/L 06/10/17 00:39 93-72-106/07/17 16:000.20 0.052 1
Surrogates
2,4-DCAA (S)66 %06/10/17 00:39 19719-28-906/07/17 16:0039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/09/17 21:26 7440-36-006/02/17 11:256.0 3.9 1
Arsenic ND ug/L 06/09/17 21:26 7440-38-206/02/17 11:2510.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-13 Lab ID:92342530001 Collected:05/31/17 17:35 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Barium 85.7J ug/L 06/09/17 21:26 7440-39-306/02/17 11:251002.5 1
Beryllium ND ug/L 06/09/17 21:26 7440-41-706/02/17 11:251.0 0.50 1
Cadmium 1.5 ug/L 06/09/17 21:26 7440-43-906/02/17 11:251.0 0.50 1
Chromium 2.8J ug/L 06/09/17 21:26 7440-47-306/02/17 11:2510.0 2.5 1
Cobalt 11.0 ug/L 06/09/17 21:26 7440-48-406/02/17 11:2510.0 2.5 1
Copper ND ug/L 06/09/17 21:26 7440-50-806/02/17 11:2510.0 2.5 1
Lead ND ug/L 06/09/17 21:26 7439-92-106/02/17 11:2510.0 2.5 1
Nickel 2.6J ug/L 06/09/17 21:26 7440-02-006/02/17 11:2550.0 2.5 1
Selenium ND ug/L 06/09/17 21:26 7782-49-206/02/17 11:2510.0 5.0 1
Silver ND ug/L 06/09/17 21:26 7440-22-406/02/17 11:2510.0 2.5 1
Tin ND ug/L 06/09/17 21:26 7440-31-506/02/17 11:251002.5 1
Vanadium ND ug/L 06/09/17 21:26 7440-62-206/02/17 11:2525.0 2.5 1
Zinc 8.4J ug/L 06/09/17 21:26 7440-66-606/02/17 11:2510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.12J ug/L 06/09/17 17:12 7440-28-006/06/17 02:455.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 01:43 7439-97-606/05/17 20:000.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/14/17 15:31 83-32-906/07/17 17:1010.0 1.6 1
Acenaphthylene ND ug/L 06/14/17 15:31 208-96-806/07/17 17:1010.0 1.5 1
Acetophenone ND ug/L 06/14/17 15:31 98-86-206/07/17 17:1010.0 1.9 1
2-Acetylaminofluorene ND ug/L 06/14/17 15:31 53-96-3 L206/07/17 17:1020.0 1.6 1
4-Aminobiphenyl ND ug/L 06/14/17 15:31 92-67-106/07/17 17:1020.0 1.7 1
Anthracene ND ug/L 06/14/17 15:31 120-12-706/07/17 17:1010.0 1.7 1
Benzo(a)anthracene ND ug/L 06/14/17 15:31 56-55-306/07/17 17:1010.0 2.1 1
Benzo(a)pyrene ND ug/L 06/14/17 15:31 50-32-806/07/17 17:1010.0 2.2 1
Benzo(b)fluoranthene ND ug/L 06/14/17 15:31 205-99-206/07/17 17:1010.0 2.2 1
Benzo(g,h,i)perylene ND ug/L 06/14/17 15:31 191-24-206/07/17 17:1010.0 2.1 1
Benzo(k)fluoranthene ND ug/L 06/14/17 15:31 207-08-906/07/17 17:1010.0 2.0 1
Benzyl alcohol ND ug/L 06/14/17 15:31 100-51-606/07/17 17:1020.0 3.1 1
4-Bromophenylphenyl ether ND ug/L 06/14/17 15:31 101-55-306/07/17 17:1010.0 1.5 1
Butylbenzylphthalate ND ug/L 06/14/17 15:31 85-68-706/07/17 17:1010.0 2.5 1
4-Chloro-3-methylphenol ND ug/L 06/14/17 15:31 59-50-706/07/17 17:1020.0 2.8 1
4-Chloroaniline ND ug/L 06/14/17 15:31 106-47-806/07/17 17:1020.0 2.8 1
Chlorobenzilate ND ug/L 06/14/17 15:31 510-15-606/07/17 17:1010.0 2.2 1
bis(2-Chloroethoxy)methane ND ug/L 06/14/17 15:31 111-91-106/07/17 17:1010.0 1.6 1
bis(2-Chloroethyl) ether ND ug/L 06/14/17 15:31 111-44-406/07/17 17:1010.0 1.7 1
2-Chloronaphthalene ND ug/L 06/14/17 15:31 91-58-706/07/17 17:1010.0 1.6 1
2-Chlorophenol ND ug/L 06/14/17 15:31 95-57-806/07/17 17:1010.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/14/17 15:31 7005-72-306/07/17 17:1010.0 1.6 1
Chrysene ND ug/L 06/14/17 15:31 218-01-906/07/17 17:1010.0 2.1 1
Diallate ND ug/L 06/14/17 15:31 2303-16-406/07/17 17:1010.0 1.6 1
Dibenz(a,h)anthracene ND ug/L 06/14/17 15:31 53-70-306/07/17 17:1010.0 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-13 Lab ID:92342530001 Collected:05/31/17 17:35 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Dibenzofuran ND ug/L 06/14/17 15:31 132-64-906/07/17 17:1010.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 06/14/17 15:31 91-94-106/07/17 17:1020.0 3.9 1
2,4-Dichlorophenol ND ug/L 06/14/17 15:31 120-83-206/07/17 17:1010.0 1.6 1
2,6-Dichlorophenol ND ug/L 06/14/17 15:31 87-65-006/07/17 17:1010.0 1.5 1
Diethylphthalate ND ug/L 06/14/17 15:31 84-66-206/07/17 17:1060001.6 1
Dimethoate ND ug/L 06/14/17 15:31 60-51-506/07/17 17:1020.0 1.8 1
P-Dimethylaminoazobenzene ND ug/L 06/14/17 15:31 60-11-706/07/17 17:1010.0 1.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/14/17 15:31 57-97-606/07/17 17:1010.0 2.4 1
3,3'-Dimethylbenzidine ND ug/L 06/14/17 15:31 119-93-706/07/17 17:1010.0 3.9 1
2,4-Dimethylphenol ND ug/L 06/14/17 15:31 105-67-906/07/17 17:1010.0 1.6 1
Dimethylphthalate ND ug/L 06/14/17 15:31 131-11-306/07/17 17:1010.0 1.4 1
Di-n-butylphthalate ND ug/L 06/14/17 15:31 84-74-206/07/17 17:1010.0 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/14/17 15:31 534-52-106/07/17 17:1050.0 2.2 1
1,3-Dinitrobenzene ND ug/L 06/14/17 15:31 99-65-006/07/17 17:1020.0 1.3 1
2,4-Dinitrophenol ND ug/L 06/14/17 15:31 51-28-506/07/17 17:1050.0 5.1 1
2,4-Dinitrotoluene ND ug/L 06/14/17 15:31 121-14-206/07/17 17:1010.0 1.5 1
2,6-Dinitrotoluene ND ug/L 06/14/17 15:31 606-20-206/07/17 17:1010.0 1.4 1
Di-n-octylphthalate ND ug/L 06/14/17 15:31 117-84-006/07/17 17:1010.0 1.5 1
Diphenylamine ND ug/L 06/14/17 15:31 122-39-406/07/17 17:1010.0 1.4 1
Disulfoton ND ug/L 06/14/17 15:31 298-04-406/07/17 17:1010.0 1.5 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/14/17 15:31 117-81-706/07/17 17:1015.0 2.3 1
Ethyl methanesulfonate ND ug/L 06/14/17 15:31 62-50-006/07/17 17:1020.0 1.6 1
Famphur ND ug/L 06/14/17 15:31 52-85-706/07/17 17:1020.0 5.7 1
Fluoranthene ND ug/L 06/14/17 15:31 206-44-006/07/17 17:1010.0 2.2 1
Fluorene ND ug/L 06/14/17 15:31 86-73-706/07/17 17:1010.0 1.6 1
Hexachlorobenzene ND ug/L 06/14/17 15:31 118-74-106/07/17 17:1010.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 06/14/17 15:31 77-47-406/07/17 17:1010.0 1.3 1
Hexachloroethane ND ug/L 06/14/17 15:31 67-72-106/07/17 17:1010.0 1.8 1
Hexachloropropene ND ug/L 06/14/17 15:31 1888-71-706/07/17 17:1010.0 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/14/17 15:31 193-39-506/07/17 17:1010.0 2.0 1
Isodrin ND ug/L 06/14/17 15:31 465-73-606/07/17 17:1020.0 2.5 1
Isophorone ND ug/L 06/14/17 15:31 78-59-106/07/17 17:1010.0 1.5 1
Isosafrole ND ug/L 06/14/17 15:31 120-58-106/07/17 17:1010.0 1.5 1
Kepone ND ug/L 06/14/17 15:31 143-50-006/07/17 17:1020.0 4.5 1
Methapyrilene ND ug/L 06/14/17 15:31 91-80-506/07/17 17:101003.0 1
3-Methylcholanthrene ND ug/L 06/14/17 15:31 56-49-506/07/17 17:1010.0 2.7 1
Methyl methanesulfonate ND ug/L 06/14/17 15:31 66-27-306/07/17 17:1010.0 1.1 1
2-Methylnaphthalene ND ug/L 06/14/17 15:31 91-57-606/07/17 17:1010.0 1.4 1
Methyl parathion ND ug/L 06/14/17 15:31 298-00-006/07/17 17:1010.0 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 06/14/17 15:31 95-48-706/07/17 17:1010.0 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/14/17 15:31 15831-10-406/07/17 17:1010.0 1.4 1
1-Naphthalenamine ND ug/L 06/14/17 15:31 134-32-706/07/17 17:1010.0 1.3 1
2-Naphthalenamine ND ug/L 06/14/17 15:31 91-59-806/07/17 17:1010.0 2.2 1
1,4-Naphthoquinone ND ug/L 06/14/17 15:31 130-15-406/07/17 17:1010.0 0.99 1
2-Nitroaniline ND ug/L 06/14/17 15:31 88-74-406/07/17 17:1050.0 2.3 1
3-Nitroaniline ND ug/L 06/14/17 15:31 99-09-206/07/17 17:1050.0 2.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
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Page 43 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-13 Lab ID:92342530001 Collected:05/31/17 17:35 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Nitroaniline ND ug/L 06/14/17 15:31 100-01-606/07/17 17:1020.0 3.4 1
Nitrobenzene ND ug/L 06/14/17 15:31 98-95-306/07/17 17:1010.0 1.6 1
2-Nitrophenol ND ug/L 06/14/17 15:31 88-75-506/07/17 17:1010.0 1.6 1
4-Nitrophenol ND ug/L 06/14/17 15:31 100-02-706/07/17 17:1050.0 4.3 1
5-Nitro-o-toluidine ND ug/L 06/14/17 15:31 99-55-806/07/17 17:1010.0 1.9 1
N-Nitrosodiethylamine ND ug/L 06/14/17 15:31 55-18-506/07/17 17:1020.0 1.4 1
N-Nitrosodimethylamine ND ug/L 06/14/17 15:31 62-75-906/07/17 17:1010.0 1.6 1
N-Nitroso-di-n-butylamine ND ug/L 06/14/17 15:31 924-16-306/07/17 17:1010.0 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 06/14/17 15:31 621-64-706/07/17 17:1010.0 1.7 1
N-Nitrosodiphenylamine ND ug/L 06/14/17 15:31 86-30-606/07/17 17:1010.0 1.4 1
N-Nitrosomethylethylamine ND ug/L 06/14/17 15:31 10595-95-606/07/17 17:1010.0 1.4 1
N-Nitrosopiperidine ND ug/L 06/14/17 15:31 100-75-406/07/17 17:1020.0 1.7 1
N-Nitrosopyrrolidine ND ug/L 06/14/17 15:31 930-55-206/07/17 17:1010.0 1.7 1
O,O,O-Triethylphosphorothioate ND ug/L 06/14/17 15:31 126-68-106/07/17 17:1010.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/14/17 15:31 108-60-106/07/17 17:1010.0 1.8 1
Parathion (Ethyl parathion)ND ug/L 06/14/17 15:31 56-38-206/07/17 17:1010.0 1.5 1
Pentachlorobenzene ND ug/L 06/14/17 15:31 608-93-506/07/17 17:1010.0 1.5 1
Pentachloronitrobenzene ND ug/L 06/14/17 15:31 82-68-806/07/17 17:1020.0 1.7 1
Pentachlorophenol ND ug/L 06/14/17 15:31 87-86-506/07/17 17:1025.0 3.5 1
Phenacetin ND ug/L 06/14/17 15:31 62-44-206/07/17 17:1020.0 1.9 1
Phenanthrene ND ug/L 06/14/17 15:31 85-01-806/07/17 17:1010.0 1.6 1
Phenol ND ug/L 06/14/17 15:31 108-95-206/07/17 17:1010.0 1.3 1
p-Phenylenediamine ND ug/L 06/14/17 15:31 106-50-306/07/17 17:1010.0 2.2 1
Phorate ND ug/L 06/14/17 15:31 298-02-206/07/17 17:1010.0 1.7 1
Pronamide ND ug/L 06/14/17 15:31 23950-58-506/07/17 17:1010.0 2.0 1
Pyrene ND ug/L 06/14/17 15:31 129-00-006/07/17 17:1010.0 2.2 1
Safrole ND ug/L 06/14/17 15:31 94-59-706/07/17 17:1010.0 1.3 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/14/17 15:31 95-94-306/07/17 17:1010.0 1.3 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/14/17 15:31 58-90-206/07/17 17:1010.0 2.9 1
Thionazin ND ug/L 06/14/17 15:31 297-97-206/07/17 17:1020.0 1.7 1
O-Toluidine ND ug/L 06/14/17 15:31 95-53-406/07/17 17:1010.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 06/14/17 15:31 95-95-406/07/17 17:1010.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/14/17 15:31 88-06-206/07/17 17:1010.0 1.4 1
1,3,5-Trinitrobenzene ND ug/L 06/14/17 15:31 99-35-406/07/17 17:1010.0 1.2 1
Surrogates
Nitrobenzene-d5 (S)48 %06/14/17 15:31 4165-60-006/07/17 17:1021-110 1
2-Fluorobiphenyl (S)52 %06/14/17 15:31 321-60-806/07/17 17:1027-110 1
Terphenyl-d14 (S)31 %06/14/17 15:31 1718-51-006/07/17 17:1031-107 1
Phenol-d6 (S)18 %06/14/17 15:31 13127-88-306/07/17 17:1010-110 1
2-Fluorophenol (S)27 %06/14/17 15:31 367-12-406/07/17 17:1012-110 1
2,4,6-Tribromophenol (S)53 %06/14/17 15:31 118-79-606/07/17 17:1027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/02/17 09:19 67-64-110010.0 1
Acetonitrile ND ug/L 06/02/17 09:19 75-05-855.0 2.2 1
Acrolein ND ug/L 06/02/17 09:19 107-02-853.0 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-13 Lab ID:92342530001 Collected:05/31/17 17:35 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acrylonitrile ND ug/L 06/02/17 09:19 107-13-12001.9 1
Allyl chloride ND ug/L 06/02/17 09:19 107-05-110.0 1.5 1
Benzene ND ug/L 06/02/17 09:19 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/02/17 09:19 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/02/17 09:19 75-27-41.0 0.18 1
Bromoform ND ug/L 06/02/17 09:19 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/02/17 09:19 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/02/17 09:19 78-93-31000.96 1
Carbon disulfide ND ug/L 06/02/17 09:19 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/02/17 09:19 56-23-51.0 0.25 1
Chlorobenzene 1.6J ug/L 06/02/17 09:19 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/02/17 09:19 75-00-310.0 0.54 1
Chloroform ND ug/L 06/02/17 09:19 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/02/17 09:19 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/02/17 09:19 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/02/17 09:19 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/02/17 09:19 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/02/17 09:19 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/02/17 09:19 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/02/17 09:19 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/02/17 09:19 541-73-15.0 0.24 1
1,4-Dichlorobenzene 3.6 ug/L 06/02/17 09:19 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/02/17 09:19 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/02/17 09:19 75-71-85.0 0.21 1
1,1-Dichloroethane 4.0J ug/L 06/02/17 09:19 75-34-35.0 0.32 1
1,2-Dichloroethane 0.96J ug/L 06/02/17 09:19 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/02/17 09:19 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 28.1 ug/L 06/02/17 09:19 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/02/17 09:19 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/02/17 09:19 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/02/17 09:19 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/02/17 09:19 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/02/17 09:19 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/02/17 09:19 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/02/17 09:19 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/02/17 09:19 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/02/17 09:19 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/02/17 09:19 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/02/17 09:19 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/02/17 09:19 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/02/17 09:19 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/02/17 09:19 126-98-71000.93 1
Methylene Chloride ND ug/L 06/02/17 09:19 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/02/17 09:19 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/02/17 09:19 108-10-11000.33 1
Naphthalene ND ug/L 06/02/17 09:19 91-20-310.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-13 Lab ID:92342530001 Collected:05/31/17 17:35 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Propionitrile ND ug/L 06/02/17 09:19 107-12-01503.6 1
Styrene ND ug/L 06/02/17 09:19 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/02/17 09:19 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/02/17 09:19 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/02/17 09:19 127-18-41.0 0.46 1
Toluene ND ug/L 06/02/17 09:19 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/02/17 09:19 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/02/17 09:19 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/02/17 09:19 79-00-51.0 0.29 1
Trichloroethene 0.98J ug/L 06/02/17 09:19 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/02/17 09:19 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/02/17 09:19 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/02/17 09:19 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/02/17 09:19 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/02/17 09:19 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)117 %06/02/17 09:19 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %06/02/17 09:19 17060-07-070-130 1
Toluene-d8 (S)111 %06/02/17 09:19 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/06/17 23:00 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/07/17 13:31 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-16 Lab ID:92342530002 Collected:05/31/17 16:50 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/06/17 22:31 309-00-206/02/17 10:090.050 0.050 1
alpha-BHC ND ug/L 06/06/17 22:31 319-84-606/02/17 10:090.050 0.050 1
beta-BHC ND ug/L 06/06/17 22:31 319-85-706/02/17 10:090.050 0.050 1
delta-BHC ND ug/L 06/06/17 22:31 319-86-806/02/17 10:090.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/06/17 22:31 58-89-906/02/17 10:090.050 0.050 1
Chlordane (Technical)ND ug/L 06/06/17 22:31 57-74-906/02/17 10:090.50 0.20 1
4,4'-DDD ND ug/L 06/06/17 22:31 72-54-806/02/17 10:090.10 0.050 1
4,4'-DDE ND ug/L 06/06/17 22:31 72-55-906/02/17 10:090.10 0.050 1
4,4'-DDT ND ug/L 06/06/17 22:31 50-29-306/02/17 10:090.10 0.050 1
Dieldrin ND ug/L 06/06/17 22:31 60-57-106/02/17 10:090.075 0.050 1
Endosulfan I ND ug/L 06/06/17 22:31 959-98-806/02/17 10:090.10 0.050 1
Endosulfan II ND ug/L 06/06/17 22:31 33213-65-906/02/17 10:090.10 0.050 1
Endosulfan sulfate ND ug/L 06/06/17 22:31 1031-07-806/02/17 10:090.10 0.050 1
Endrin ND ug/L 06/06/17 22:31 72-20-806/02/17 10:090.10 0.050 1
Endrin aldehyde ND ug/L 06/06/17 22:31 7421-93-406/02/17 10:090.10 0.050 1
Heptachlor ND ug/L 06/06/17 22:31 76-44-806/02/17 10:090.050 0.050 1
Heptachlor epoxide ND ug/L 06/06/17 22:31 1024-57-306/02/17 10:090.075 0.050 1
Methoxychlor ND ug/L 06/06/17 22:31 72-43-506/02/17 10:091.0 0.15 1
Toxaphene ND ug/L 06/06/17 22:31 8001-35-206/02/17 10:091.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)94 %06/06/17 22:31 877-09-806/02/17 10:0920-130 1
Decachlorobiphenyl (S)70 %06/06/17 22:31 2051-24-306/02/17 10:0920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/03/17 12:43 12674-11-206/02/17 10:090.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/03/17 12:43 11104-28-206/02/17 10:090.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/03/17 12:43 11141-16-506/02/17 10:090.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/03/17 12:43 53469-21-906/02/17 10:090.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/03/17 12:43 12672-29-606/02/17 10:090.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/03/17 12:43 11097-69-106/02/17 10:090.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/03/17 12:43 11096-82-506/02/17 10:090.50 0.50 1
Surrogates
Decachlorobiphenyl (S)84 %06/03/17 12:43 2051-24-306/02/17 10:0910-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/10/17 01:09 94-75-706/07/17 16:000.98 0.23 1
Dinoseb ND ug/L 06/10/17 01:09 88-85-706/07/17 16:000.20 0.059 1
Pentachlorophenol ND ug/L 06/10/17 01:09 87-86-506/07/17 16:000.030 0.018 1
2,4,5-T ND ug/L 06/10/17 01:09 93-76-506/07/17 16:000.20 0.044 1
2,4,5-TP (Silvex)ND ug/L 06/10/17 01:09 93-72-106/07/17 16:000.20 0.051 1
Surrogates
2,4-DCAA (S)78 %06/10/17 01:09 19719-28-906/07/17 16:0039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/09/17 21:29 7440-36-006/02/17 11:256.0 3.9 1
Arsenic ND ug/L 06/09/17 21:29 7440-38-206/02/17 11:2510.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-16 Lab ID:92342530002 Collected:05/31/17 16:50 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Barium 68.0J ug/L 06/09/17 21:29 7440-39-306/02/17 11:251002.5 1
Beryllium ND ug/L 06/09/17 21:29 7440-41-706/02/17 11:251.0 0.50 1
Cadmium 0.52J ug/L 06/09/17 21:29 7440-43-906/02/17 11:251.0 0.50 1
Chromium 7.0J ug/L 06/09/17 21:29 7440-47-306/02/17 11:2510.0 2.5 1
Cobalt 242 ug/L 06/09/17 21:29 7440-48-406/02/17 11:2510.0 2.5 1
Copper 3.8J ug/L 06/09/17 21:29 7440-50-806/02/17 11:2510.0 2.5 1
Lead 2.7J ug/L 06/09/17 21:29 7439-92-106/02/17 11:2510.0 2.5 1
Nickel 13.2J ug/L 06/09/17 21:29 7440-02-006/02/17 11:2550.0 2.5 1
Selenium ND ug/L 06/09/17 21:29 7782-49-206/02/17 11:2510.0 5.0 1
Silver ND ug/L 06/09/17 21:29 7440-22-406/02/17 11:2510.0 2.5 1
Tin ND ug/L 06/09/17 21:29 7440-31-506/02/17 11:251002.5 1
Vanadium ND ug/L 06/09/17 21:29 7440-62-206/02/17 11:2525.0 2.5 1
Zinc 14.7 ug/L 06/09/17 21:29 7440-66-606/02/17 11:2510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.20J ug/L 06/09/17 17:14 7440-28-006/06/17 02:455.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 01:46 7439-97-606/05/17 20:000.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/14/17 16:00 83-32-906/07/17 17:1010.0 1.6 1
Acenaphthylene ND ug/L 06/14/17 16:00 208-96-8 M106/07/17 17:1010.0 1.5 1
Acetophenone ND ug/L 06/14/17 16:00 98-86-206/07/17 17:1010.0 1.9 1
2-Acetylaminofluorene ND ug/L 06/14/17 16:00 53-96-3 L206/07/17 17:1020.0 1.6 1
4-Aminobiphenyl ND ug/L 06/14/17 16:00 92-67-1 M106/07/17 17:1020.0 1.7 1
Anthracene ND ug/L 06/14/17 16:00 120-12-706/07/17 17:1010.0 1.7 1
Benzo(a)anthracene ND ug/L 06/14/17 16:00 56-55-306/07/17 17:1010.0 2.1 1
Benzo(a)pyrene ND ug/L 06/14/17 16:00 50-32-806/07/17 17:1010.0 2.2 1
Benzo(b)fluoranthene ND ug/L 06/14/17 16:00 205-99-206/07/17 17:1010.0 2.2 1
Benzo(g,h,i)perylene ND ug/L 06/14/17 16:00 191-24-206/07/17 17:1010.0 2.1 1
Benzo(k)fluoranthene ND ug/L 06/14/17 16:00 207-08-906/07/17 17:1010.0 2.0 1
Benzyl alcohol ND ug/L 06/14/17 16:00 100-51-606/07/17 17:1020.0 3.1 1
4-Bromophenylphenyl ether ND ug/L 06/14/17 16:00 101-55-306/07/17 17:1010.0 1.5 1
Butylbenzylphthalate ND ug/L 06/14/17 16:00 85-68-706/07/17 17:1010.0 2.5 1
4-Chloro-3-methylphenol ND ug/L 06/14/17 16:00 59-50-706/07/17 17:1020.0 2.8 1
4-Chloroaniline ND ug/L 06/14/17 16:00 106-47-806/07/17 17:1020.0 2.8 1
Chlorobenzilate ND ug/L 06/14/17 16:00 510-15-606/07/17 17:1010.0 2.2 1
bis(2-Chloroethoxy)methane ND ug/L 06/14/17 16:00 111-91-106/07/17 17:1010.0 1.6 1
bis(2-Chloroethyl) ether ND ug/L 06/14/17 16:00 111-44-406/07/17 17:1010.0 1.7 1
2-Chloronaphthalene ND ug/L 06/14/17 16:00 91-58-7 M106/07/17 17:1010.0 1.6 1
2-Chlorophenol ND ug/L 06/14/17 16:00 95-57-806/07/17 17:1010.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/14/17 16:00 7005-72-306/07/17 17:1010.0 1.6 1
Chrysene ND ug/L 06/14/17 16:00 218-01-906/07/17 17:1010.0 2.1 1
Diallate ND ug/L 06/14/17 16:00 2303-16-406/07/17 17:1010.0 1.6 1
Dibenz(a,h)anthracene ND ug/L 06/14/17 16:00 53-70-306/07/17 17:1010.0 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 48 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-16 Lab ID:92342530002 Collected:05/31/17 16:50 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Dibenzofuran ND ug/L 06/14/17 16:00 132-64-906/07/17 17:1010.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 06/14/17 16:00 91-94-106/07/17 17:1020.0 3.9 1
2,4-Dichlorophenol ND ug/L 06/14/17 16:00 120-83-206/07/17 17:1010.0 1.6 1
2,6-Dichlorophenol ND ug/L 06/14/17 16:00 87-65-006/07/17 17:1010.0 1.5 1
Diethylphthalate ND ug/L 06/14/17 16:00 84-66-206/07/17 17:1060001.6 1
Dimethoate ND ug/L 06/14/17 16:00 60-51-506/07/17 17:1020.0 1.8 1
P-Dimethylaminoazobenzene ND ug/L 06/14/17 16:00 60-11-7 M106/07/17 17:1010.0 1.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/14/17 16:00 57-97-606/07/17 17:1010.0 2.4 1
3,3'-Dimethylbenzidine ND ug/L 06/14/17 16:00 119-93-7 M106/07/17 17:1010.0 3.9 1
2,4-Dimethylphenol ND ug/L 06/14/17 16:00 105-67-906/07/17 17:1010.0 1.6 1
Dimethylphthalate ND ug/L 06/14/17 16:00 131-11-306/07/17 17:1010.0 1.4 1
Di-n-butylphthalate ND ug/L 06/14/17 16:00 84-74-206/07/17 17:1010.0 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/14/17 16:00 534-52-106/07/17 17:1050.0 2.2 1
1,3-Dinitrobenzene ND ug/L 06/14/17 16:00 99-65-006/07/17 17:1020.0 1.3 1
2,4-Dinitrophenol ND ug/L 06/14/17 16:00 51-28-506/07/17 17:1050.0 5.1 1
2,4-Dinitrotoluene ND ug/L 06/14/17 16:00 121-14-206/07/17 17:1010.0 1.5 1
2,6-Dinitrotoluene ND ug/L 06/14/17 16:00 606-20-206/07/17 17:1010.0 1.4 1
Di-n-octylphthalate ND ug/L 06/14/17 16:00 117-84-006/07/17 17:1010.0 1.5 1
Diphenylamine ND ug/L 06/14/17 16:00 122-39-406/07/17 17:1010.0 1.4 1
Disulfoton ND ug/L 06/14/17 16:00 298-04-406/07/17 17:1010.0 1.5 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/14/17 16:00 117-81-706/07/17 17:1015.0 2.3 1
Ethyl methanesulfonate ND ug/L 06/14/17 16:00 62-50-006/07/17 17:1020.0 1.6 1
Famphur ND ug/L 06/14/17 16:00 52-85-706/07/17 17:1020.0 5.7 1
Fluoranthene ND ug/L 06/14/17 16:00 206-44-006/07/17 17:1010.0 2.2 1
Fluorene ND ug/L 06/14/17 16:00 86-73-706/07/17 17:1010.0 1.6 1
Hexachlorobenzene ND ug/L 06/14/17 16:00 118-74-106/07/17 17:1010.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 06/14/17 16:00 77-47-406/07/17 17:1010.0 1.3 1
Hexachloroethane ND ug/L 06/14/17 16:00 67-72-106/07/17 17:1010.0 1.8 1
Hexachloropropene ND ug/L 06/14/17 16:00 1888-71-706/07/17 17:1010.0 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/14/17 16:00 193-39-506/07/17 17:1010.0 2.0 1
Isodrin ND ug/L 06/14/17 16:00 465-73-606/07/17 17:1020.0 2.5 1
Isophorone ND ug/L 06/14/17 16:00 78-59-106/07/17 17:1010.0 1.5 1
Isosafrole ND ug/L 06/14/17 16:00 120-58-106/07/17 17:1010.0 1.5 1
Kepone ND ug/L 06/14/17 16:00 143-50-006/07/17 17:1020.0 4.5 1
Methapyrilene ND ug/L 06/14/17 16:00 91-80-506/07/17 17:101003.0 1
3-Methylcholanthrene ND ug/L 06/14/17 16:00 56-49-506/07/17 17:1010.0 2.7 1
Methyl methanesulfonate ND ug/L 06/14/17 16:00 66-27-306/07/17 17:1010.0 1.1 1
2-Methylnaphthalene ND ug/L 06/14/17 16:00 91-57-606/07/17 17:1010.0 1.4 1
Methyl parathion ND ug/L 06/14/17 16:00 298-00-006/07/17 17:1010.0 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 06/14/17 16:00 95-48-706/07/17 17:1010.0 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/14/17 16:00 15831-10-406/07/17 17:1010.0 1.4 1
1-Naphthalenamine ND ug/L 06/14/17 16:00 134-32-7 M106/07/17 17:1010.0 1.3 1
2-Naphthalenamine ND ug/L 06/14/17 16:00 91-59-8 M106/07/17 17:1010.0 2.2 1
1,4-Naphthoquinone ND ug/L 06/14/17 16:00 130-15-406/07/17 17:1010.0 0.99 1
2-Nitroaniline ND ug/L 06/14/17 16:00 88-74-406/07/17 17:1050.0 2.3 1
3-Nitroaniline ND ug/L 06/14/17 16:00 99-09-206/07/17 17:1050.0 2.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-16 Lab ID:92342530002 Collected:05/31/17 16:50 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Nitroaniline ND ug/L 06/14/17 16:00 100-01-6 M106/07/17 17:1020.0 3.4 1
Nitrobenzene ND ug/L 06/14/17 16:00 98-95-306/07/17 17:1010.0 1.6 1
2-Nitrophenol ND ug/L 06/14/17 16:00 88-75-506/07/17 17:1010.0 1.6 1
4-Nitrophenol ND ug/L 06/14/17 16:00 100-02-706/07/17 17:1050.0 4.3 1
5-Nitro-o-toluidine ND ug/L 06/14/17 16:00 99-55-806/07/17 17:1010.0 1.9 1
N-Nitrosodiethylamine ND ug/L 06/14/17 16:00 55-18-506/07/17 17:1020.0 1.4 1
N-Nitrosodimethylamine ND ug/L 06/14/17 16:00 62-75-906/07/17 17:1010.0 1.6 1
N-Nitroso-di-n-butylamine ND ug/L 06/14/17 16:00 924-16-306/07/17 17:1010.0 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 06/14/17 16:00 621-64-706/07/17 17:1010.0 1.7 1
N-Nitrosodiphenylamine ND ug/L 06/14/17 16:00 86-30-606/07/17 17:1010.0 1.4 1
N-Nitrosomethylethylamine ND ug/L 06/14/17 16:00 10595-95-6 M106/07/17 17:1010.0 1.4 1
N-Nitrosopiperidine ND ug/L 06/14/17 16:00 100-75-406/07/17 17:1020.0 1.7 1
N-Nitrosopyrrolidine ND ug/L 06/14/17 16:00 930-55-206/07/17 17:1010.0 1.7 1
O,O,O-Triethylphosphorothioate ND ug/L 06/14/17 16:00 126-68-106/07/17 17:1010.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/14/17 16:00 108-60-106/07/17 17:1010.0 1.8 1
Parathion (Ethyl parathion)ND ug/L 06/14/17 16:00 56-38-206/07/17 17:1010.0 1.5 1
Pentachlorobenzene ND ug/L 06/14/17 16:00 608-93-506/07/17 17:1010.0 1.5 1
Pentachloronitrobenzene ND ug/L 06/14/17 16:00 82-68-806/07/17 17:1020.0 1.7 1
Pentachlorophenol ND ug/L 06/14/17 16:00 87-86-506/07/17 17:1025.0 3.5 1
Phenacetin ND ug/L 06/14/17 16:00 62-44-206/07/17 17:1020.0 1.9 1
Phenanthrene ND ug/L 06/14/17 16:00 85-01-806/07/17 17:1010.0 1.6 1
Phenol ND ug/L 06/14/17 16:00 108-95-206/07/17 17:1010.0 1.3 1
p-Phenylenediamine ND ug/L 06/14/17 16:00 106-50-306/07/17 17:1010.0 2.2 1
Phorate ND ug/L 06/14/17 16:00 298-02-206/07/17 17:1010.0 1.7 1
Pronamide ND ug/L 06/14/17 16:00 23950-58-506/07/17 17:1010.0 2.0 1
Pyrene ND ug/L 06/14/17 16:00 129-00-006/07/17 17:1010.0 2.2 1
Safrole ND ug/L 06/14/17 16:00 94-59-706/07/17 17:1010.0 1.3 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/14/17 16:00 95-94-306/07/17 17:1010.0 1.3 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/14/17 16:00 58-90-2 M106/07/17 17:1010.0 2.9 1
Thionazin ND ug/L 06/14/17 16:00 297-97-206/07/17 17:1020.0 1.7 1
O-Toluidine ND ug/L 06/14/17 16:00 95-53-4 M106/07/17 17:1010.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 06/14/17 16:00 95-95-406/07/17 17:1010.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/14/17 16:00 88-06-206/07/17 17:1010.0 1.4 1
1,3,5-Trinitrobenzene ND ug/L 06/14/17 16:00 99-35-406/07/17 17:1010.0 1.2 1
Surrogates
Nitrobenzene-d5 (S)54 %06/14/17 16:00 4165-60-006/07/17 17:1021-110 1
2-Fluorobiphenyl (S)66 %06/14/17 16:00 321-60-806/07/17 17:1027-110 1
Terphenyl-d14 (S)66 %06/14/17 16:00 1718-51-006/07/17 17:1031-107 1
Phenol-d6 (S)21 %06/14/17 16:00 13127-88-306/07/17 17:1010-110 1
2-Fluorophenol (S)32 %06/14/17 16:00 367-12-406/07/17 17:1012-110 1
2,4,6-Tribromophenol (S)73 %06/14/17 16:00 118-79-606/07/17 17:1027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 20.7J ug/L 06/02/17 09:36 67-64-110010.0 1
Acetonitrile ND ug/L 06/02/17 09:36 75-05-855.0 2.2 1
Acrolein ND ug/L 06/02/17 09:36 107-02-853.0 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-16 Lab ID:92342530002 Collected:05/31/17 16:50 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acrylonitrile ND ug/L 06/02/17 09:36 107-13-12001.9 1
Allyl chloride ND ug/L 06/02/17 09:36 107-05-110.0 1.5 1
Benzene 0.44J ug/L 06/02/17 09:36 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/02/17 09:36 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/02/17 09:36 75-27-41.0 0.18 1
Bromoform ND ug/L 06/02/17 09:36 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/02/17 09:36 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/02/17 09:36 78-93-31000.96 1
Carbon disulfide ND ug/L 06/02/17 09:36 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/02/17 09:36 56-23-51.0 0.25 1
Chlorobenzene 1.8J ug/L 06/02/17 09:36 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/02/17 09:36 75-00-310.0 0.54 1
Chloroform ND ug/L 06/02/17 09:36 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/02/17 09:36 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/02/17 09:36 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/02/17 09:36 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/02/17 09:36 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/02/17 09:36 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/02/17 09:36 74-95-310.0 0.21 1
1,2-Dichlorobenzene 0.48J ug/L 06/02/17 09:36 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/02/17 09:36 541-73-15.0 0.24 1
1,4-Dichlorobenzene 4.3 ug/L 06/02/17 09:36 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/02/17 09:36 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/02/17 09:36 75-71-85.0 0.21 1
1,1-Dichloroethane 0.58J ug/L 06/02/17 09:36 75-34-35.0 0.32 1
1,2-Dichloroethane 0.81J ug/L 06/02/17 09:36 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/02/17 09:36 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 11.5 ug/L 06/02/17 09:36 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/02/17 09:36 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/02/17 09:36 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/02/17 09:36 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/02/17 09:36 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/02/17 09:36 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/02/17 09:36 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/02/17 09:36 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/02/17 09:36 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/02/17 09:36 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/02/17 09:36 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/02/17 09:36 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/02/17 09:36 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/02/17 09:36 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/02/17 09:36 126-98-71000.93 1
Methylene Chloride ND ug/L 06/02/17 09:36 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/02/17 09:36 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/02/17 09:36 108-10-11000.33 1
Naphthalene ND ug/L 06/02/17 09:36 91-20-310.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-16 Lab ID:92342530002 Collected:05/31/17 16:50 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Propionitrile ND ug/L 06/02/17 09:36 107-12-01503.6 1
Styrene ND ug/L 06/02/17 09:36 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/02/17 09:36 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/02/17 09:36 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/02/17 09:36 127-18-41.0 0.46 1
Toluene ND ug/L 06/02/17 09:36 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/02/17 09:36 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/02/17 09:36 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/02/17 09:36 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/02/17 09:36 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/02/17 09:36 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/02/17 09:36 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/02/17 09:36 108-05-450.0 0.35 1
Vinyl chloride 1.3 ug/L 06/02/17 09:36 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/02/17 09:36 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)117 %06/02/17 09:36 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %06/02/17 09:36 17060-07-070-130 1
Toluene-d8 (S)112 %06/02/17 09:36 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/06/17 23:00 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 12.7 ug/L 06/07/17 13:32 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-17 Lab ID:92342530003 Collected:05/31/17 16:30 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/06/17 22:49 309-00-206/02/17 10:090.050 0.050 1
alpha-BHC ND ug/L 06/06/17 22:49 319-84-606/02/17 10:090.050 0.050 1
beta-BHC ND ug/L 06/06/17 22:49 319-85-706/02/17 10:090.050 0.050 1
delta-BHC ND ug/L 06/06/17 22:49 319-86-806/02/17 10:090.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/06/17 22:49 58-89-906/02/17 10:090.050 0.050 1
Chlordane (Technical)ND ug/L 06/06/17 22:49 57-74-906/02/17 10:090.50 0.20 1
4,4'-DDD ND ug/L 06/06/17 22:49 72-54-806/02/17 10:090.10 0.050 1
4,4'-DDE ND ug/L 06/06/17 22:49 72-55-906/02/17 10:090.10 0.050 1
4,4'-DDT ND ug/L 06/06/17 22:49 50-29-306/02/17 10:090.10 0.050 1
Dieldrin ND ug/L 06/06/17 22:49 60-57-106/02/17 10:090.075 0.050 1
Endosulfan I ND ug/L 06/06/17 22:49 959-98-806/02/17 10:090.10 0.050 1
Endosulfan II ND ug/L 06/06/17 22:49 33213-65-906/02/17 10:090.10 0.050 1
Endosulfan sulfate ND ug/L 06/06/17 22:49 1031-07-806/02/17 10:090.10 0.050 1
Endrin ND ug/L 06/06/17 22:49 72-20-806/02/17 10:090.10 0.050 1
Endrin aldehyde ND ug/L 06/06/17 22:49 7421-93-406/02/17 10:090.10 0.050 1
Heptachlor ND ug/L 06/06/17 22:49 76-44-806/02/17 10:090.050 0.050 1
Heptachlor epoxide ND ug/L 06/06/17 22:49 1024-57-306/02/17 10:090.075 0.050 1
Methoxychlor ND ug/L 06/06/17 22:49 72-43-506/02/17 10:091.0 0.15 1
Toxaphene ND ug/L 06/06/17 22:49 8001-35-206/02/17 10:091.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)91 %06/06/17 22:49 877-09-806/02/17 10:0920-130 1
Decachlorobiphenyl (S)71 %06/06/17 22:49 2051-24-306/02/17 10:0920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/03/17 14:27 12674-11-206/02/17 10:090.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/03/17 14:27 11104-28-206/02/17 10:090.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/03/17 14:27 11141-16-506/02/17 10:090.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/03/17 14:27 53469-21-906/02/17 10:090.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/03/17 14:27 12672-29-606/02/17 10:090.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/03/17 14:27 11097-69-106/02/17 10:090.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/03/17 14:27 11096-82-506/02/17 10:090.50 0.50 1
Surrogates
Decachlorobiphenyl (S)77 %06/03/17 14:27 2051-24-306/02/17 10:0910-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/10/17 01:38 94-75-706/07/17 16:000.97 0.23 1
Dinoseb ND ug/L 06/10/17 01:38 88-85-706/07/17 16:000.20 0.059 1
Pentachlorophenol ND ug/L 06/10/17 01:38 87-86-506/07/17 16:000.029 0.018 1
2,4,5-T ND ug/L 06/10/17 01:38 93-76-506/07/17 16:000.20 0.043 1
2,4,5-TP (Silvex)ND ug/L 06/10/17 01:38 93-72-106/07/17 16:000.20 0.051 1
Surrogates
2,4-DCAA (S)75 %06/10/17 01:38 19719-28-906/07/17 16:0039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/09/17 21:32 7440-36-006/02/17 11:256.0 3.9 1
Arsenic ND ug/L 06/09/17 21:32 7440-38-206/02/17 11:2510.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-17 Lab ID:92342530003 Collected:05/31/17 16:30 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Barium 27.5J ug/L 06/09/17 21:32 7440-39-306/02/17 11:251002.5 1
Beryllium ND ug/L 06/09/17 21:32 7440-41-706/02/17 11:251.0 0.50 1
Cadmium ND ug/L 06/09/17 21:32 7440-43-906/02/17 11:251.0 0.50 1
Chromium ND ug/L 06/09/17 21:32 7440-47-306/02/17 11:2510.0 2.5 1
Cobalt ND ug/L 06/09/17 21:32 7440-48-406/02/17 11:2510.0 2.5 1
Copper ND ug/L 06/09/17 21:32 7440-50-806/02/17 11:2510.0 2.5 1
Lead ND ug/L 06/09/17 21:32 7439-92-106/02/17 11:2510.0 2.5 1
Nickel 3.2J ug/L 06/09/17 21:32 7440-02-006/02/17 11:2550.0 2.5 1
Selenium ND ug/L 06/09/17 21:32 7782-49-206/02/17 11:2510.0 5.0 1
Silver ND ug/L 06/09/17 21:32 7440-22-406/02/17 11:2510.0 2.5 1
Tin 5.3J ug/L 06/09/17 21:32 7440-31-506/02/17 11:251002.5 1
Vanadium ND ug/L 06/09/17 21:32 7440-62-206/02/17 11:2525.0 2.5 1
Zinc 5.1J ug/L 06/09/17 21:32 7440-66-606/02/17 11:2510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.054J ug/L 06/09/17 17:16 7440-28-006/06/17 02:455.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 01:48 7439-97-606/05/17 20:000.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/14/17 16:29 83-32-906/07/17 17:1010.0 1.6 1
Acenaphthylene ND ug/L 06/14/17 16:29 208-96-806/07/17 17:1010.0 1.5 1
Acetophenone ND ug/L 06/14/17 16:29 98-86-206/07/17 17:1010.0 1.9 1
2-Acetylaminofluorene ND ug/L 06/14/17 16:29 53-96-3 L206/07/17 17:1020.0 1.6 1
4-Aminobiphenyl ND ug/L 06/14/17 16:29 92-67-106/07/17 17:1020.0 1.7 1
Anthracene ND ug/L 06/14/17 16:29 120-12-706/07/17 17:1010.0 1.7 1
Benzo(a)anthracene ND ug/L 06/14/17 16:29 56-55-306/07/17 17:1010.0 2.1 1
Benzo(a)pyrene ND ug/L 06/14/17 16:29 50-32-806/07/17 17:1010.0 2.2 1
Benzo(b)fluoranthene ND ug/L 06/14/17 16:29 205-99-206/07/17 17:1010.0 2.2 1
Benzo(g,h,i)perylene ND ug/L 06/14/17 16:29 191-24-206/07/17 17:1010.0 2.1 1
Benzo(k)fluoranthene ND ug/L 06/14/17 16:29 207-08-906/07/17 17:1010.0 2.0 1
Benzyl alcohol ND ug/L 06/14/17 16:29 100-51-606/07/17 17:1020.0 3.1 1
4-Bromophenylphenyl ether ND ug/L 06/14/17 16:29 101-55-306/07/17 17:1010.0 1.5 1
Butylbenzylphthalate ND ug/L 06/14/17 16:29 85-68-706/07/17 17:1010.0 2.5 1
4-Chloro-3-methylphenol ND ug/L 06/14/17 16:29 59-50-706/07/17 17:1020.0 2.8 1
4-Chloroaniline ND ug/L 06/14/17 16:29 106-47-806/07/17 17:1020.0 2.8 1
Chlorobenzilate ND ug/L 06/14/17 16:29 510-15-606/07/17 17:1010.0 2.2 1
bis(2-Chloroethoxy)methane ND ug/L 06/14/17 16:29 111-91-106/07/17 17:1010.0 1.6 1
bis(2-Chloroethyl) ether ND ug/L 06/14/17 16:29 111-44-406/07/17 17:1010.0 1.7 1
2-Chloronaphthalene ND ug/L 06/14/17 16:29 91-58-706/07/17 17:1010.0 1.6 1
2-Chlorophenol ND ug/L 06/14/17 16:29 95-57-806/07/17 17:1010.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/14/17 16:29 7005-72-306/07/17 17:1010.0 1.6 1
Chrysene ND ug/L 06/14/17 16:29 218-01-906/07/17 17:1010.0 2.1 1
Diallate ND ug/L 06/14/17 16:29 2303-16-406/07/17 17:1010.0 1.6 1
Dibenz(a,h)anthracene ND ug/L 06/14/17 16:29 53-70-306/07/17 17:1010.0 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-17 Lab ID:92342530003 Collected:05/31/17 16:30 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Dibenzofuran ND ug/L 06/14/17 16:29 132-64-906/07/17 17:1010.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 06/14/17 16:29 91-94-106/07/17 17:1020.0 3.9 1
2,4-Dichlorophenol ND ug/L 06/14/17 16:29 120-83-206/07/17 17:1010.0 1.6 1
2,6-Dichlorophenol ND ug/L 06/14/17 16:29 87-65-006/07/17 17:1010.0 1.5 1
Diethylphthalate ND ug/L 06/14/17 16:29 84-66-206/07/17 17:1060001.6 1
Dimethoate ND ug/L 06/14/17 16:29 60-51-506/07/17 17:1020.0 1.8 1
P-Dimethylaminoazobenzene ND ug/L 06/14/17 16:29 60-11-706/07/17 17:1010.0 1.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/14/17 16:29 57-97-606/07/17 17:1010.0 2.4 1
3,3'-Dimethylbenzidine ND ug/L 06/14/17 16:29 119-93-706/07/17 17:1010.0 3.9 1
2,4-Dimethylphenol ND ug/L 06/14/17 16:29 105-67-906/07/17 17:1010.0 1.6 1
Dimethylphthalate ND ug/L 06/14/17 16:29 131-11-306/07/17 17:1010.0 1.4 1
Di-n-butylphthalate ND ug/L 06/14/17 16:29 84-74-206/07/17 17:1010.0 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/14/17 16:29 534-52-106/07/17 17:1050.0 2.2 1
1,3-Dinitrobenzene ND ug/L 06/14/17 16:29 99-65-006/07/17 17:1020.0 1.3 1
2,4-Dinitrophenol ND ug/L 06/14/17 16:29 51-28-506/07/17 17:1050.0 5.1 1
2,4-Dinitrotoluene ND ug/L 06/14/17 16:29 121-14-206/07/17 17:1010.0 1.5 1
2,6-Dinitrotoluene ND ug/L 06/14/17 16:29 606-20-206/07/17 17:1010.0 1.4 1
Di-n-octylphthalate ND ug/L 06/14/17 16:29 117-84-006/07/17 17:1010.0 1.5 1
Diphenylamine ND ug/L 06/14/17 16:29 122-39-406/07/17 17:1010.0 1.4 1
Disulfoton ND ug/L 06/14/17 16:29 298-04-406/07/17 17:1010.0 1.5 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/14/17 16:29 117-81-706/07/17 17:1015.0 2.3 1
Ethyl methanesulfonate ND ug/L 06/14/17 16:29 62-50-006/07/17 17:1020.0 1.6 1
Famphur ND ug/L 06/14/17 16:29 52-85-706/07/17 17:1020.0 5.7 1
Fluoranthene ND ug/L 06/14/17 16:29 206-44-006/07/17 17:1010.0 2.2 1
Fluorene ND ug/L 06/14/17 16:29 86-73-706/07/17 17:1010.0 1.6 1
Hexachlorobenzene ND ug/L 06/14/17 16:29 118-74-106/07/17 17:1010.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 06/14/17 16:29 77-47-406/07/17 17:1010.0 1.3 1
Hexachloroethane ND ug/L 06/14/17 16:29 67-72-106/07/17 17:1010.0 1.8 1
Hexachloropropene ND ug/L 06/14/17 16:29 1888-71-706/07/17 17:1010.0 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/14/17 16:29 193-39-506/07/17 17:1010.0 2.0 1
Isodrin ND ug/L 06/14/17 16:29 465-73-606/07/17 17:1020.0 2.5 1
Isophorone ND ug/L 06/14/17 16:29 78-59-106/07/17 17:1010.0 1.5 1
Isosafrole ND ug/L 06/14/17 16:29 120-58-106/07/17 17:1010.0 1.5 1
Kepone ND ug/L 06/14/17 16:29 143-50-006/07/17 17:1020.0 4.5 1
Methapyrilene ND ug/L 06/14/17 16:29 91-80-506/07/17 17:101003.0 1
3-Methylcholanthrene ND ug/L 06/14/17 16:29 56-49-506/07/17 17:1010.0 2.7 1
Methyl methanesulfonate ND ug/L 06/14/17 16:29 66-27-306/07/17 17:1010.0 1.1 1
2-Methylnaphthalene ND ug/L 06/14/17 16:29 91-57-606/07/17 17:1010.0 1.4 1
Methyl parathion ND ug/L 06/14/17 16:29 298-00-006/07/17 17:1010.0 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 06/14/17 16:29 95-48-706/07/17 17:1010.0 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/14/17 16:29 15831-10-406/07/17 17:1010.0 1.4 1
1-Naphthalenamine ND ug/L 06/14/17 16:29 134-32-706/07/17 17:1010.0 1.3 1
2-Naphthalenamine ND ug/L 06/14/17 16:29 91-59-806/07/17 17:1010.0 2.2 1
1,4-Naphthoquinone ND ug/L 06/14/17 16:29 130-15-406/07/17 17:1010.0 0.99 1
2-Nitroaniline ND ug/L 06/14/17 16:29 88-74-406/07/17 17:1050.0 2.3 1
3-Nitroaniline ND ug/L 06/14/17 16:29 99-09-206/07/17 17:1050.0 2.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-17 Lab ID:92342530003 Collected:05/31/17 16:30 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Nitroaniline ND ug/L 06/14/17 16:29 100-01-606/07/17 17:1020.0 3.4 1
Nitrobenzene ND ug/L 06/14/17 16:29 98-95-306/07/17 17:1010.0 1.6 1
2-Nitrophenol ND ug/L 06/14/17 16:29 88-75-506/07/17 17:1010.0 1.6 1
4-Nitrophenol ND ug/L 06/14/17 16:29 100-02-706/07/17 17:1050.0 4.3 1
5-Nitro-o-toluidine ND ug/L 06/14/17 16:29 99-55-806/07/17 17:1010.0 1.9 1
N-Nitrosodiethylamine ND ug/L 06/14/17 16:29 55-18-506/07/17 17:1020.0 1.4 1
N-Nitrosodimethylamine ND ug/L 06/14/17 16:29 62-75-906/07/17 17:1010.0 1.6 1
N-Nitroso-di-n-butylamine ND ug/L 06/14/17 16:29 924-16-306/07/17 17:1010.0 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 06/14/17 16:29 621-64-706/07/17 17:1010.0 1.7 1
N-Nitrosodiphenylamine ND ug/L 06/14/17 16:29 86-30-606/07/17 17:1010.0 1.4 1
N-Nitrosomethylethylamine ND ug/L 06/14/17 16:29 10595-95-606/07/17 17:1010.0 1.4 1
N-Nitrosopiperidine ND ug/L 06/14/17 16:29 100-75-406/07/17 17:1020.0 1.7 1
N-Nitrosopyrrolidine ND ug/L 06/14/17 16:29 930-55-206/07/17 17:1010.0 1.7 1
O,O,O-Triethylphosphorothioate ND ug/L 06/14/17 16:29 126-68-106/07/17 17:1010.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/14/17 16:29 108-60-106/07/17 17:1010.0 1.8 1
Parathion (Ethyl parathion)ND ug/L 06/14/17 16:29 56-38-206/07/17 17:1010.0 1.5 1
Pentachlorobenzene ND ug/L 06/14/17 16:29 608-93-506/07/17 17:1010.0 1.5 1
Pentachloronitrobenzene ND ug/L 06/14/17 16:29 82-68-806/07/17 17:1020.0 1.7 1
Pentachlorophenol ND ug/L 06/14/17 16:29 87-86-506/07/17 17:1025.0 3.5 1
Phenacetin ND ug/L 06/14/17 16:29 62-44-206/07/17 17:1020.0 1.9 1
Phenanthrene ND ug/L 06/14/17 16:29 85-01-806/07/17 17:1010.0 1.6 1
Phenol ND ug/L 06/14/17 16:29 108-95-206/07/17 17:1010.0 1.3 1
p-Phenylenediamine ND ug/L 06/14/17 16:29 106-50-306/07/17 17:1010.0 2.2 1
Phorate ND ug/L 06/14/17 16:29 298-02-206/07/17 17:1010.0 1.7 1
Pronamide ND ug/L 06/14/17 16:29 23950-58-506/07/17 17:1010.0 2.0 1
Pyrene ND ug/L 06/14/17 16:29 129-00-006/07/17 17:1010.0 2.2 1
Safrole ND ug/L 06/14/17 16:29 94-59-706/07/17 17:1010.0 1.3 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/14/17 16:29 95-94-306/07/17 17:1010.0 1.3 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/14/17 16:29 58-90-206/07/17 17:1010.0 2.9 1
Thionazin ND ug/L 06/14/17 16:29 297-97-206/07/17 17:1020.0 1.7 1
O-Toluidine ND ug/L 06/14/17 16:29 95-53-406/07/17 17:1010.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 06/14/17 16:29 95-95-406/07/17 17:1010.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/14/17 16:29 88-06-206/07/17 17:1010.0 1.4 1
1,3,5-Trinitrobenzene ND ug/L 06/14/17 16:29 99-35-406/07/17 17:1010.0 1.2 1
Surrogates
Nitrobenzene-d5 (S)72 %06/14/17 16:29 4165-60-006/07/17 17:1021-110 1
2-Fluorobiphenyl (S)95 %06/14/17 16:29 321-60-806/07/17 17:1027-110 1
Terphenyl-d14 (S)86 %06/14/17 16:29 1718-51-006/07/17 17:1031-107 1
Phenol-d6 (S)26 %06/14/17 16:29 13127-88-306/07/17 17:1010-110 1
2-Fluorophenol (S)40 %06/14/17 16:29 367-12-406/07/17 17:1012-110 1
2,4,6-Tribromophenol (S)92 %06/14/17 16:29 118-79-606/07/17 17:1027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 16.1J ug/L 06/02/17 09:54 67-64-110010.0 1
Acetonitrile ND ug/L 06/02/17 09:54 75-05-855.0 2.2 1
Acrolein ND ug/L 06/02/17 09:54 107-02-853.0 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-17 Lab ID:92342530003 Collected:05/31/17 16:30 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acrylonitrile ND ug/L 06/02/17 09:54 107-13-12001.9 1
Allyl chloride ND ug/L 06/02/17 09:54 107-05-110.0 1.5 1
Benzene ND ug/L 06/02/17 09:54 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/02/17 09:54 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/02/17 09:54 75-27-41.0 0.18 1
Bromoform ND ug/L 06/02/17 09:54 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/02/17 09:54 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/02/17 09:54 78-93-31000.96 1
Carbon disulfide ND ug/L 06/02/17 09:54 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/02/17 09:54 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/02/17 09:54 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/02/17 09:54 75-00-310.0 0.54 1
Chloroform ND ug/L 06/02/17 09:54 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/02/17 09:54 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/02/17 09:54 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/02/17 09:54 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/02/17 09:54 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/02/17 09:54 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/02/17 09:54 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/02/17 09:54 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/02/17 09:54 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/02/17 09:54 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/02/17 09:54 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/02/17 09:54 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/02/17 09:54 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/02/17 09:54 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/02/17 09:54 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/02/17 09:54 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/02/17 09:54 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/02/17 09:54 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/02/17 09:54 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/02/17 09:54 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/02/17 09:54 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/02/17 09:54 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/02/17 09:54 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/02/17 09:54 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/02/17 09:54 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/02/17 09:54 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/02/17 09:54 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/02/17 09:54 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/02/17 09:54 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/02/17 09:54 126-98-71000.93 1
Methylene Chloride ND ug/L 06/02/17 09:54 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/02/17 09:54 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/02/17 09:54 108-10-11000.33 1
Naphthalene ND ug/L 06/02/17 09:54 91-20-310.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 57 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-17 Lab ID:92342530003 Collected:05/31/17 16:30 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Propionitrile ND ug/L 06/02/17 09:54 107-12-01503.6 1
Styrene ND ug/L 06/02/17 09:54 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/02/17 09:54 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/02/17 09:54 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/02/17 09:54 127-18-41.0 0.46 1
Toluene ND ug/L 06/02/17 09:54 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/02/17 09:54 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/02/17 09:54 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/02/17 09:54 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/02/17 09:54 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/02/17 09:54 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/02/17 09:54 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/02/17 09:54 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/02/17 09:54 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/02/17 09:54 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)113 %06/02/17 09:54 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %06/02/17 09:54 17060-07-070-130 1
Toluene-d8 (S)112 %06/02/17 09:54 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/06/17 23:00 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 5.2J ug/L 06/07/17 13:33 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-21 Lab ID:92342530004 Collected:05/31/17 17:20 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/06/17 23:07 309-00-206/02/17 10:090.050 0.050 1
alpha-BHC ND ug/L 06/06/17 23:07 319-84-606/02/17 10:090.050 0.050 1
beta-BHC ND ug/L 06/06/17 23:07 319-85-706/02/17 10:090.050 0.050 1
delta-BHC ND ug/L 06/06/17 23:07 319-86-806/02/17 10:090.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/06/17 23:07 58-89-906/02/17 10:090.050 0.050 1
Chlordane (Technical)ND ug/L 06/06/17 23:07 57-74-906/02/17 10:090.50 0.20 1
4,4'-DDD ND ug/L 06/06/17 23:07 72-54-806/02/17 10:090.10 0.050 1
4,4'-DDE ND ug/L 06/06/17 23:07 72-55-906/02/17 10:090.10 0.050 1
4,4'-DDT ND ug/L 06/06/17 23:07 50-29-306/02/17 10:090.10 0.050 1
Dieldrin ND ug/L 06/06/17 23:07 60-57-106/02/17 10:090.075 0.050 1
Endosulfan I ND ug/L 06/06/17 23:07 959-98-806/02/17 10:090.10 0.050 1
Endosulfan II ND ug/L 06/06/17 23:07 33213-65-906/02/17 10:090.10 0.050 1
Endosulfan sulfate ND ug/L 06/06/17 23:07 1031-07-806/02/17 10:090.10 0.050 1
Endrin ND ug/L 06/06/17 23:07 72-20-806/02/17 10:090.10 0.050 1
Endrin aldehyde ND ug/L 06/06/17 23:07 7421-93-406/02/17 10:090.10 0.050 1
Heptachlor ND ug/L 06/06/17 23:07 76-44-806/02/17 10:090.050 0.050 1
Heptachlor epoxide ND ug/L 06/06/17 23:07 1024-57-306/02/17 10:090.075 0.050 1
Methoxychlor ND ug/L 06/06/17 23:07 72-43-506/02/17 10:091.0 0.15 1
Toxaphene ND ug/L 06/06/17 23:07 8001-35-206/02/17 10:091.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)71 %06/06/17 23:07 877-09-806/02/17 10:0920-130 1
Decachlorobiphenyl (S)78 %06/06/17 23:07 2051-24-306/02/17 10:0920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/03/17 15:09 12674-11-206/02/17 10:090.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/03/17 15:09 11104-28-206/02/17 10:090.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/03/17 15:09 11141-16-506/02/17 10:090.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/03/17 15:09 53469-21-906/02/17 10:090.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/03/17 15:09 12672-29-606/02/17 10:090.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/03/17 15:09 11097-69-106/02/17 10:090.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/03/17 15:09 11096-82-506/02/17 10:090.50 0.50 1
Surrogates
Decachlorobiphenyl (S)79 %06/03/17 15:09 2051-24-306/02/17 10:0910-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/10/17 02:08 94-75-706/07/17 16:000.99 0.24 1
Dinoseb ND ug/L 06/10/17 02:08 88-85-706/07/17 16:000.20 0.060 1
Pentachlorophenol ND ug/L 06/10/17 02:08 87-86-506/07/17 16:000.030 0.018 1
2,4,5-T ND ug/L 06/10/17 02:08 93-76-506/07/17 16:000.20 0.044 1
2,4,5-TP (Silvex)ND ug/L 06/10/17 02:08 93-72-106/07/17 16:000.20 0.052 1
Surrogates
2,4-DCAA (S)74 %06/10/17 02:08 19719-28-906/07/17 16:0039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/09/17 21:45 7440-36-006/02/17 11:256.0 3.9 1
Arsenic ND ug/L 06/09/17 21:45 7440-38-206/02/17 11:2510.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-21 Lab ID:92342530004 Collected:05/31/17 17:20 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Barium 60.5J ug/L 06/09/17 21:45 7440-39-306/02/17 11:251002.5 1
Beryllium ND ug/L 06/09/17 21:45 7440-41-706/02/17 11:251.0 0.50 1
Cadmium ND ug/L 06/09/17 21:45 7440-43-906/02/17 11:251.0 0.50 1
Chromium ND ug/L 06/09/17 21:45 7440-47-306/02/17 11:2510.0 2.5 1
Cobalt 4.8J ug/L 06/09/17 21:45 7440-48-406/02/17 11:2510.0 2.5 1
Copper ND ug/L 06/09/17 21:45 7440-50-806/02/17 11:2510.0 2.5 1
Lead ND ug/L 06/09/17 21:45 7439-92-106/02/17 11:2510.0 2.5 1
Nickel ND ug/L 06/09/17 21:45 7440-02-006/02/17 11:2550.0 2.5 1
Selenium ND ug/L 06/09/17 21:45 7782-49-206/02/17 11:2510.0 5.0 1
Silver ND ug/L 06/09/17 21:45 7440-22-406/02/17 11:2510.0 2.5 1
Tin ND ug/L 06/09/17 21:45 7440-31-506/02/17 11:251002.5 1
Vanadium ND ug/L 06/09/17 21:45 7440-62-206/02/17 11:2525.0 2.5 1
Zinc 5.3J ug/L 06/09/17 21:45 7440-66-606/02/17 11:2510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/09/17 17:18 7440-28-006/06/17 02:455.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 01:50 7439-97-606/05/17 20:000.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/14/17 16:59 83-32-906/07/17 17:1010.0 1.6 1
Acenaphthylene ND ug/L 06/14/17 16:59 208-96-806/07/17 17:1010.0 1.5 1
Acetophenone ND ug/L 06/14/17 16:59 98-86-206/07/17 17:1010.0 1.9 1
2-Acetylaminofluorene ND ug/L 06/14/17 16:59 53-96-3 L206/07/17 17:1020.0 1.6 1
4-Aminobiphenyl ND ug/L 06/14/17 16:59 92-67-106/07/17 17:1020.0 1.7 1
Anthracene ND ug/L 06/14/17 16:59 120-12-706/07/17 17:1010.0 1.7 1
Benzo(a)anthracene ND ug/L 06/14/17 16:59 56-55-306/07/17 17:1010.0 2.1 1
Benzo(a)pyrene ND ug/L 06/14/17 16:59 50-32-806/07/17 17:1010.0 2.2 1
Benzo(b)fluoranthene ND ug/L 06/14/17 16:59 205-99-206/07/17 17:1010.0 2.2 1
Benzo(g,h,i)perylene ND ug/L 06/14/17 16:59 191-24-206/07/17 17:1010.0 2.1 1
Benzo(k)fluoranthene ND ug/L 06/14/17 16:59 207-08-906/07/17 17:1010.0 2.0 1
Benzyl alcohol ND ug/L 06/14/17 16:59 100-51-606/07/17 17:1020.0 3.1 1
4-Bromophenylphenyl ether ND ug/L 06/14/17 16:59 101-55-306/07/17 17:1010.0 1.5 1
Butylbenzylphthalate ND ug/L 06/14/17 16:59 85-68-706/07/17 17:1010.0 2.5 1
4-Chloro-3-methylphenol ND ug/L 06/14/17 16:59 59-50-706/07/17 17:1020.0 2.8 1
4-Chloroaniline ND ug/L 06/14/17 16:59 106-47-806/07/17 17:1020.0 2.8 1
Chlorobenzilate ND ug/L 06/14/17 16:59 510-15-606/07/17 17:1010.0 2.2 1
bis(2-Chloroethoxy)methane ND ug/L 06/14/17 16:59 111-91-106/07/17 17:1010.0 1.6 1
bis(2-Chloroethyl) ether ND ug/L 06/14/17 16:59 111-44-406/07/17 17:1010.0 1.7 1
2-Chloronaphthalene ND ug/L 06/14/17 16:59 91-58-706/07/17 17:1010.0 1.6 1
2-Chlorophenol ND ug/L 06/14/17 16:59 95-57-806/07/17 17:1010.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/14/17 16:59 7005-72-306/07/17 17:1010.0 1.6 1
Chrysene ND ug/L 06/14/17 16:59 218-01-906/07/17 17:1010.0 2.1 1
Diallate ND ug/L 06/14/17 16:59 2303-16-406/07/17 17:1010.0 1.6 1
Dibenz(a,h)anthracene ND ug/L 06/14/17 16:59 53-70-306/07/17 17:1010.0 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-21 Lab ID:92342530004 Collected:05/31/17 17:20 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Dibenzofuran ND ug/L 06/14/17 16:59 132-64-906/07/17 17:1010.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 06/14/17 16:59 91-94-106/07/17 17:1020.0 3.9 1
2,4-Dichlorophenol ND ug/L 06/14/17 16:59 120-83-206/07/17 17:1010.0 1.6 1
2,6-Dichlorophenol ND ug/L 06/14/17 16:59 87-65-006/07/17 17:1010.0 1.5 1
Diethylphthalate ND ug/L 06/14/17 16:59 84-66-206/07/17 17:1060001.6 1
Dimethoate ND ug/L 06/14/17 16:59 60-51-506/07/17 17:1020.0 1.8 1
P-Dimethylaminoazobenzene ND ug/L 06/14/17 16:59 60-11-706/07/17 17:1010.0 1.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/14/17 16:59 57-97-606/07/17 17:1010.0 2.4 1
3,3'-Dimethylbenzidine ND ug/L 06/14/17 16:59 119-93-706/07/17 17:1010.0 3.9 1
2,4-Dimethylphenol ND ug/L 06/14/17 16:59 105-67-906/07/17 17:1010.0 1.6 1
Dimethylphthalate ND ug/L 06/14/17 16:59 131-11-306/07/17 17:1010.0 1.4 1
Di-n-butylphthalate ND ug/L 06/14/17 16:59 84-74-206/07/17 17:1010.0 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/14/17 16:59 534-52-106/07/17 17:1050.0 2.2 1
1,3-Dinitrobenzene ND ug/L 06/14/17 16:59 99-65-006/07/17 17:1020.0 1.3 1
2,4-Dinitrophenol ND ug/L 06/14/17 16:59 51-28-506/07/17 17:1050.0 5.1 1
2,4-Dinitrotoluene ND ug/L 06/14/17 16:59 121-14-206/07/17 17:1010.0 1.5 1
2,6-Dinitrotoluene ND ug/L 06/14/17 16:59 606-20-206/07/17 17:1010.0 1.4 1
Di-n-octylphthalate ND ug/L 06/14/17 16:59 117-84-006/07/17 17:1010.0 1.5 1
Diphenylamine ND ug/L 06/14/17 16:59 122-39-406/07/17 17:1010.0 1.4 1
Disulfoton ND ug/L 06/14/17 16:59 298-04-406/07/17 17:1010.0 1.5 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/14/17 16:59 117-81-706/07/17 17:1015.0 2.3 1
Ethyl methanesulfonate ND ug/L 06/14/17 16:59 62-50-006/07/17 17:1020.0 1.6 1
Famphur ND ug/L 06/14/17 16:59 52-85-706/07/17 17:1020.0 5.7 1
Fluoranthene ND ug/L 06/14/17 16:59 206-44-006/07/17 17:1010.0 2.2 1
Fluorene ND ug/L 06/14/17 16:59 86-73-706/07/17 17:1010.0 1.6 1
Hexachlorobenzene ND ug/L 06/14/17 16:59 118-74-106/07/17 17:1010.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 06/14/17 16:59 77-47-406/07/17 17:1010.0 1.3 1
Hexachloroethane ND ug/L 06/14/17 16:59 67-72-106/07/17 17:1010.0 1.8 1
Hexachloropropene ND ug/L 06/14/17 16:59 1888-71-706/07/17 17:1010.0 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/14/17 16:59 193-39-506/07/17 17:1010.0 2.0 1
Isodrin ND ug/L 06/14/17 16:59 465-73-606/07/17 17:1020.0 2.5 1
Isophorone ND ug/L 06/14/17 16:59 78-59-106/07/17 17:1010.0 1.5 1
Isosafrole ND ug/L 06/14/17 16:59 120-58-106/07/17 17:1010.0 1.5 1
Kepone ND ug/L 06/14/17 16:59 143-50-006/07/17 17:1020.0 4.5 1
Methapyrilene ND ug/L 06/14/17 16:59 91-80-506/07/17 17:101003.0 1
3-Methylcholanthrene ND ug/L 06/14/17 16:59 56-49-506/07/17 17:1010.0 2.7 1
Methyl methanesulfonate ND ug/L 06/14/17 16:59 66-27-306/07/17 17:1010.0 1.1 1
2-Methylnaphthalene ND ug/L 06/14/17 16:59 91-57-606/07/17 17:1010.0 1.4 1
Methyl parathion ND ug/L 06/14/17 16:59 298-00-006/07/17 17:1010.0 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 06/14/17 16:59 95-48-706/07/17 17:1010.0 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/14/17 16:59 15831-10-406/07/17 17:1010.0 1.4 1
1-Naphthalenamine ND ug/L 06/14/17 16:59 134-32-706/07/17 17:1010.0 1.3 1
2-Naphthalenamine ND ug/L 06/14/17 16:59 91-59-806/07/17 17:1010.0 2.2 1
1,4-Naphthoquinone ND ug/L 06/14/17 16:59 130-15-406/07/17 17:1010.0 0.99 1
2-Nitroaniline ND ug/L 06/14/17 16:59 88-74-406/07/17 17:1050.0 2.3 1
3-Nitroaniline ND ug/L 06/14/17 16:59 99-09-206/07/17 17:1050.0 2.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-21 Lab ID:92342530004 Collected:05/31/17 17:20 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Nitroaniline ND ug/L 06/14/17 16:59 100-01-606/07/17 17:1020.0 3.4 1
Nitrobenzene ND ug/L 06/14/17 16:59 98-95-306/07/17 17:1010.0 1.6 1
2-Nitrophenol ND ug/L 06/14/17 16:59 88-75-506/07/17 17:1010.0 1.6 1
4-Nitrophenol ND ug/L 06/14/17 16:59 100-02-706/07/17 17:1050.0 4.3 1
5-Nitro-o-toluidine ND ug/L 06/14/17 16:59 99-55-806/07/17 17:1010.0 1.9 1
N-Nitrosodiethylamine ND ug/L 06/14/17 16:59 55-18-506/07/17 17:1020.0 1.4 1
N-Nitrosodimethylamine ND ug/L 06/14/17 16:59 62-75-906/07/17 17:1010.0 1.6 1
N-Nitroso-di-n-butylamine ND ug/L 06/14/17 16:59 924-16-306/07/17 17:1010.0 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 06/14/17 16:59 621-64-706/07/17 17:1010.0 1.7 1
N-Nitrosodiphenylamine ND ug/L 06/14/17 16:59 86-30-606/07/17 17:1010.0 1.4 1
N-Nitrosomethylethylamine ND ug/L 06/14/17 16:59 10595-95-606/07/17 17:1010.0 1.4 1
N-Nitrosopiperidine ND ug/L 06/14/17 16:59 100-75-406/07/17 17:1020.0 1.7 1
N-Nitrosopyrrolidine ND ug/L 06/14/17 16:59 930-55-206/07/17 17:1010.0 1.7 1
O,O,O-Triethylphosphorothioate ND ug/L 06/14/17 16:59 126-68-106/07/17 17:1010.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/14/17 16:59 108-60-106/07/17 17:1010.0 1.8 1
Parathion (Ethyl parathion)ND ug/L 06/14/17 16:59 56-38-206/07/17 17:1010.0 1.5 1
Pentachlorobenzene ND ug/L 06/14/17 16:59 608-93-506/07/17 17:1010.0 1.5 1
Pentachloronitrobenzene ND ug/L 06/14/17 16:59 82-68-806/07/17 17:1020.0 1.7 1
Pentachlorophenol ND ug/L 06/14/17 16:59 87-86-506/07/17 17:1025.0 3.5 1
Phenacetin ND ug/L 06/14/17 16:59 62-44-206/07/17 17:1020.0 1.9 1
Phenanthrene ND ug/L 06/14/17 16:59 85-01-806/07/17 17:1010.0 1.6 1
Phenol ND ug/L 06/14/17 16:59 108-95-206/07/17 17:1010.0 1.3 1
p-Phenylenediamine ND ug/L 06/14/17 16:59 106-50-306/07/17 17:1010.0 2.2 1
Phorate ND ug/L 06/14/17 16:59 298-02-206/07/17 17:1010.0 1.7 1
Pronamide ND ug/L 06/14/17 16:59 23950-58-506/07/17 17:1010.0 2.0 1
Pyrene ND ug/L 06/14/17 16:59 129-00-006/07/17 17:1010.0 2.2 1
Safrole ND ug/L 06/14/17 16:59 94-59-706/07/17 17:1010.0 1.3 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/14/17 16:59 95-94-306/07/17 17:1010.0 1.3 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/14/17 16:59 58-90-206/07/17 17:1010.0 2.9 1
Thionazin ND ug/L 06/14/17 16:59 297-97-206/07/17 17:1020.0 1.7 1
O-Toluidine ND ug/L 06/14/17 16:59 95-53-406/07/17 17:1010.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 06/14/17 16:59 95-95-406/07/17 17:1010.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/14/17 16:59 88-06-206/07/17 17:1010.0 1.4 1
1,3,5-Trinitrobenzene ND ug/L 06/14/17 16:59 99-35-406/07/17 17:1010.0 1.2 1
Surrogates
Nitrobenzene-d5 (S)57 %06/14/17 16:59 4165-60-006/07/17 17:1021-110 1
2-Fluorobiphenyl (S)70 %06/14/17 16:59 321-60-806/07/17 17:1027-110 1
Terphenyl-d14 (S)76 %06/14/17 16:59 1718-51-006/07/17 17:1031-107 1
Phenol-d6 (S)20 %06/14/17 16:59 13127-88-306/07/17 17:1010-110 1
2-Fluorophenol (S)32 %06/14/17 16:59 367-12-406/07/17 17:1012-110 1
2,4,6-Tribromophenol (S)71 %06/14/17 16:59 118-79-606/07/17 17:1027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 11.0J ug/L 06/04/17 07:52 67-64-110010.0 1
Acetonitrile ND ug/L 06/04/17 07:52 75-05-855.0 2.2 1
Acrolein ND ug/L 06/04/17 07:52 107-02-853.0 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
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Page 62 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-21 Lab ID:92342530004 Collected:05/31/17 17:20 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acrylonitrile ND ug/L 06/04/17 07:52 107-13-12001.9 1
Allyl chloride ND ug/L 06/04/17 07:52 107-05-110.0 1.5 1
Benzene ND ug/L 06/04/17 07:52 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 07:52 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 07:52 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 07:52 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 07:52 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 07:52 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 07:52 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 07:52 56-23-51.0 0.25 1
Chlorobenzene 0.25J ug/L 06/04/17 07:52 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 07:52 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 07:52 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/17 07:52 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/04/17 07:52 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 07:52 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 07:52 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 07:52 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 07:52 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 07:52 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/04/17 07:52 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/04/17 07:52 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 07:52 110-57-6 L11001.0 1
Dichlorodifluoromethane ND ug/L 06/04/17 07:52 75-71-85.0 0.21 1
1,1-Dichloroethane 4.1J ug/L 06/04/17 07:52 75-34-35.0 0.32 1
1,2-Dichloroethane 0.49J ug/L 06/04/17 07:52 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 07:52 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 18.6 ug/L 06/04/17 07:52 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 07:52 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 07:52 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/04/17 07:52 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/04/17 07:52 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/04/17 07:52 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/04/17 07:52 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 07:52 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 07:52 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/04/17 07:52 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/04/17 07:52 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/04/17 07:52 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 07:52 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/04/17 07:52 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/04/17 07:52 126-98-71000.93 1
Methylene Chloride ND ug/L 06/04/17 07:52 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/04/17 07:52 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 07:52 108-10-11000.33 1
Naphthalene ND ug/L 06/04/17 07:52 91-20-310.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 63 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-21 Lab ID:92342530004 Collected:05/31/17 17:20 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Propionitrile ND ug/L 06/04/17 07:52 107-12-01503.6 1
Styrene ND ug/L 06/04/17 07:52 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 07:52 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 07:52 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 07:52 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 07:52 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/04/17 07:52 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/04/17 07:52 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 07:52 79-00-51.0 0.29 1
Trichloroethene 0.70J ug/L 06/04/17 07:52 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 07:52 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 07:52 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 07:52 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 07:52 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/17 07:52 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)105 %06/04/17 07:52 460-00-470-130 1
1,2-Dichloroethane-d4 (S)90 %06/04/17 07:52 17060-07-070-130 1
Toluene-d8 (S)109 %06/04/17 07:52 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/06/17 23:00 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/07/17 13:34 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-22 Lab ID:92342530005 Collected:05/31/17 16:10 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/06/17 23:25 309-00-206/02/17 10:090.050 0.050 1
alpha-BHC ND ug/L 06/06/17 23:25 319-84-606/02/17 10:090.050 0.050 1
beta-BHC ND ug/L 06/06/17 23:25 319-85-706/02/17 10:090.050 0.050 1
delta-BHC ND ug/L 06/06/17 23:25 319-86-806/02/17 10:090.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/06/17 23:25 58-89-906/02/17 10:090.050 0.050 1
Chlordane (Technical)ND ug/L 06/06/17 23:25 57-74-906/02/17 10:090.50 0.20 1
4,4'-DDD ND ug/L 06/06/17 23:25 72-54-806/02/17 10:090.10 0.050 1
4,4'-DDE ND ug/L 06/06/17 23:25 72-55-906/02/17 10:090.10 0.050 1
4,4'-DDT ND ug/L 06/06/17 23:25 50-29-306/02/17 10:090.10 0.050 1
Dieldrin ND ug/L 06/06/17 23:25 60-57-106/02/17 10:090.075 0.050 1
Endosulfan I ND ug/L 06/06/17 23:25 959-98-806/02/17 10:090.10 0.050 1
Endosulfan II ND ug/L 06/06/17 23:25 33213-65-906/02/17 10:090.10 0.050 1
Endosulfan sulfate ND ug/L 06/06/17 23:25 1031-07-806/02/17 10:090.10 0.050 1
Endrin ND ug/L 06/06/17 23:25 72-20-806/02/17 10:090.10 0.050 1
Endrin aldehyde ND ug/L 06/06/17 23:25 7421-93-406/02/17 10:090.10 0.050 1
Heptachlor ND ug/L 06/06/17 23:25 76-44-806/02/17 10:090.050 0.050 1
Heptachlor epoxide ND ug/L 06/06/17 23:25 1024-57-306/02/17 10:090.075 0.050 1
Methoxychlor ND ug/L 06/06/17 23:25 72-43-506/02/17 10:091.0 0.15 1
Toxaphene ND ug/L 06/06/17 23:25 8001-35-206/02/17 10:091.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)72 %06/06/17 23:25 877-09-806/02/17 10:0920-130 1
Decachlorobiphenyl (S)62 %06/06/17 23:25 2051-24-306/02/17 10:0920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/03/17 15:30 12674-11-206/02/17 10:090.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/03/17 15:30 11104-28-206/02/17 10:090.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/03/17 15:30 11141-16-506/02/17 10:090.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/03/17 15:30 53469-21-906/02/17 10:090.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/03/17 15:30 12672-29-606/02/17 10:090.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/03/17 15:30 11097-69-106/02/17 10:090.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/03/17 15:30 11096-82-506/02/17 10:090.50 0.50 1
Surrogates
Decachlorobiphenyl (S)65 %06/03/17 15:30 2051-24-306/02/17 10:0910-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/10/17 03:08 94-75-706/07/17 16:000.98 0.23 1
Dinoseb ND ug/L 06/10/17 03:08 88-85-706/07/17 16:000.20 0.060 1
Pentachlorophenol ND ug/L 06/10/17 03:08 87-86-506/07/17 16:000.030 0.018 1
2,4,5-T ND ug/L 06/10/17 03:08 93-76-506/07/17 16:000.20 0.044 1
2,4,5-TP (Silvex)ND ug/L 06/10/17 03:08 93-72-106/07/17 16:000.20 0.051 1
Surrogates
2,4-DCAA (S)64 %06/10/17 03:08 19719-28-906/07/17 16:0039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/09/17 21:48 7440-36-006/02/17 11:256.0 3.9 1
Arsenic ND ug/L 06/09/17 21:48 7440-38-206/02/17 11:2510.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-22 Lab ID:92342530005 Collected:05/31/17 16:10 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Barium 56.9J ug/L 06/09/17 21:48 7440-39-306/02/17 11:251002.5 1
Beryllium ND ug/L 06/09/17 21:48 7440-41-706/02/17 11:251.0 0.50 1
Cadmium 0.63J ug/L 06/09/17 21:48 7440-43-906/02/17 11:251.0 0.50 1
Chromium ND ug/L 06/09/17 21:48 7440-47-306/02/17 11:2510.0 2.5 1
Cobalt ND ug/L 06/09/17 21:48 7440-48-406/02/17 11:2510.0 2.5 1
Copper ND ug/L 06/09/17 21:48 7440-50-806/02/17 11:2510.0 2.5 1
Lead ND ug/L 06/09/17 21:48 7439-92-106/02/17 11:2510.0 2.5 1
Nickel 2.6J ug/L 06/09/17 21:48 7440-02-006/02/17 11:2550.0 2.5 1
Selenium ND ug/L 06/09/17 21:48 7782-49-206/02/17 11:2510.0 5.0 1
Silver ND ug/L 06/09/17 21:48 7440-22-406/02/17 11:2510.0 2.5 1
Tin ND ug/L 06/09/17 21:48 7440-31-506/02/17 11:251002.5 1
Vanadium ND ug/L 06/09/17 21:48 7440-62-206/02/17 11:2525.0 2.5 1
Zinc 6.3J ug/L 06/09/17 21:48 7440-66-606/02/17 11:2510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.11J ug/L 06/09/17 17:20 7440-28-006/06/17 02:455.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 01:53 7439-97-606/05/17 20:000.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/14/17 17:57 83-32-906/07/17 17:1010.0 1.6 1
Acenaphthylene ND ug/L 06/14/17 17:57 208-96-806/07/17 17:1010.0 1.5 1
Acetophenone ND ug/L 06/14/17 17:57 98-86-206/07/17 17:1010.0 1.9 1
2-Acetylaminofluorene ND ug/L 06/14/17 17:57 53-96-3 L206/07/17 17:1020.0 1.6 1
4-Aminobiphenyl ND ug/L 06/14/17 17:57 92-67-106/07/17 17:1020.0 1.7 1
Anthracene ND ug/L 06/14/17 17:57 120-12-706/07/17 17:1010.0 1.7 1
Benzo(a)anthracene ND ug/L 06/14/17 17:57 56-55-306/07/17 17:1010.0 2.1 1
Benzo(a)pyrene ND ug/L 06/14/17 17:57 50-32-806/07/17 17:1010.0 2.2 1
Benzo(b)fluoranthene ND ug/L 06/14/17 17:57 205-99-206/07/17 17:1010.0 2.2 1
Benzo(g,h,i)perylene ND ug/L 06/14/17 17:57 191-24-206/07/17 17:1010.0 2.1 1
Benzo(k)fluoranthene ND ug/L 06/14/17 17:57 207-08-906/07/17 17:1010.0 2.0 1
Benzyl alcohol ND ug/L 06/14/17 17:57 100-51-606/07/17 17:1020.0 3.1 1
4-Bromophenylphenyl ether ND ug/L 06/14/17 17:57 101-55-306/07/17 17:1010.0 1.5 1
Butylbenzylphthalate ND ug/L 06/14/17 17:57 85-68-706/07/17 17:1010.0 2.5 1
4-Chloro-3-methylphenol ND ug/L 06/14/17 17:57 59-50-706/07/17 17:1020.0 2.8 1
4-Chloroaniline ND ug/L 06/14/17 17:57 106-47-806/07/17 17:1020.0 2.8 1
Chlorobenzilate ND ug/L 06/14/17 17:57 510-15-606/07/17 17:1010.0 2.2 1
bis(2-Chloroethoxy)methane ND ug/L 06/14/17 17:57 111-91-106/07/17 17:1010.0 1.6 1
bis(2-Chloroethyl) ether ND ug/L 06/14/17 17:57 111-44-406/07/17 17:1010.0 1.7 1
2-Chloronaphthalene ND ug/L 06/14/17 17:57 91-58-706/07/17 17:1010.0 1.6 1
2-Chlorophenol ND ug/L 06/14/17 17:57 95-57-806/07/17 17:1010.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/14/17 17:57 7005-72-306/07/17 17:1010.0 1.6 1
Chrysene ND ug/L 06/14/17 17:57 218-01-906/07/17 17:1010.0 2.1 1
Diallate ND ug/L 06/14/17 17:57 2303-16-406/07/17 17:1010.0 1.6 1
Dibenz(a,h)anthracene ND ug/L 06/14/17 17:57 53-70-306/07/17 17:1010.0 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-22 Lab ID:92342530005 Collected:05/31/17 16:10 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Dibenzofuran ND ug/L 06/14/17 17:57 132-64-906/07/17 17:1010.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 06/14/17 17:57 91-94-106/07/17 17:1020.0 3.9 1
2,4-Dichlorophenol ND ug/L 06/14/17 17:57 120-83-206/07/17 17:1010.0 1.6 1
2,6-Dichlorophenol ND ug/L 06/14/17 17:57 87-65-006/07/17 17:1010.0 1.5 1
Diethylphthalate ND ug/L 06/14/17 17:57 84-66-206/07/17 17:1060001.6 1
Dimethoate ND ug/L 06/14/17 17:57 60-51-506/07/17 17:1020.0 1.8 1
P-Dimethylaminoazobenzene ND ug/L 06/14/17 17:57 60-11-706/07/17 17:1010.0 1.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/14/17 17:57 57-97-606/07/17 17:1010.0 2.4 1
3,3'-Dimethylbenzidine ND ug/L 06/14/17 17:57 119-93-706/07/17 17:1010.0 3.9 1
2,4-Dimethylphenol ND ug/L 06/14/17 17:57 105-67-906/07/17 17:1010.0 1.6 1
Dimethylphthalate ND ug/L 06/14/17 17:57 131-11-306/07/17 17:1010.0 1.4 1
Di-n-butylphthalate ND ug/L 06/14/17 17:57 84-74-206/07/17 17:1010.0 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/14/17 17:57 534-52-106/07/17 17:1050.0 2.2 1
1,3-Dinitrobenzene ND ug/L 06/14/17 17:57 99-65-006/07/17 17:1020.0 1.3 1
2,4-Dinitrophenol ND ug/L 06/14/17 17:57 51-28-506/07/17 17:1050.0 5.1 1
2,4-Dinitrotoluene ND ug/L 06/14/17 17:57 121-14-206/07/17 17:1010.0 1.5 1
2,6-Dinitrotoluene ND ug/L 06/14/17 17:57 606-20-206/07/17 17:1010.0 1.4 1
Di-n-octylphthalate ND ug/L 06/14/17 17:57 117-84-006/07/17 17:1010.0 1.5 1
Diphenylamine ND ug/L 06/14/17 17:57 122-39-406/07/17 17:1010.0 1.4 1
Disulfoton ND ug/L 06/14/17 17:57 298-04-406/07/17 17:1010.0 1.5 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/14/17 17:57 117-81-706/07/17 17:1015.0 2.3 1
Ethyl methanesulfonate ND ug/L 06/14/17 17:57 62-50-006/07/17 17:1020.0 1.6 1
Famphur ND ug/L 06/14/17 17:57 52-85-706/07/17 17:1020.0 5.7 1
Fluoranthene ND ug/L 06/14/17 17:57 206-44-006/07/17 17:1010.0 2.2 1
Fluorene ND ug/L 06/14/17 17:57 86-73-706/07/17 17:1010.0 1.6 1
Hexachlorobenzene ND ug/L 06/14/17 17:57 118-74-106/07/17 17:1010.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 06/14/17 17:57 77-47-406/07/17 17:1010.0 1.3 1
Hexachloroethane ND ug/L 06/14/17 17:57 67-72-106/07/17 17:1010.0 1.8 1
Hexachloropropene ND ug/L 06/14/17 17:57 1888-71-706/07/17 17:1010.0 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/14/17 17:57 193-39-506/07/17 17:1010.0 2.0 1
Isodrin ND ug/L 06/14/17 17:57 465-73-606/07/17 17:1020.0 2.5 1
Isophorone ND ug/L 06/14/17 17:57 78-59-106/07/17 17:1010.0 1.5 1
Isosafrole ND ug/L 06/14/17 17:57 120-58-106/07/17 17:1010.0 1.5 1
Kepone ND ug/L 06/14/17 17:57 143-50-006/07/17 17:1020.0 4.5 1
Methapyrilene ND ug/L 06/14/17 17:57 91-80-506/07/17 17:101003.0 1
3-Methylcholanthrene ND ug/L 06/14/17 17:57 56-49-506/07/17 17:1010.0 2.7 1
Methyl methanesulfonate ND ug/L 06/14/17 17:57 66-27-306/07/17 17:1010.0 1.1 1
2-Methylnaphthalene ND ug/L 06/14/17 17:57 91-57-606/07/17 17:1010.0 1.4 1
Methyl parathion ND ug/L 06/14/17 17:57 298-00-006/07/17 17:1010.0 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 06/14/17 17:57 95-48-706/07/17 17:1010.0 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/14/17 17:57 15831-10-406/07/17 17:1010.0 1.4 1
1-Naphthalenamine ND ug/L 06/14/17 17:57 134-32-706/07/17 17:1010.0 1.3 1
2-Naphthalenamine ND ug/L 06/14/17 17:57 91-59-806/07/17 17:1010.0 2.2 1
1,4-Naphthoquinone ND ug/L 06/14/17 17:57 130-15-406/07/17 17:1010.0 0.99 1
2-Nitroaniline ND ug/L 06/14/17 17:57 88-74-406/07/17 17:1050.0 2.3 1
3-Nitroaniline ND ug/L 06/14/17 17:57 99-09-206/07/17 17:1050.0 2.7 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-22 Lab ID:92342530005 Collected:05/31/17 16:10 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Nitroaniline ND ug/L 06/14/17 17:57 100-01-606/07/17 17:1020.0 3.4 1
Nitrobenzene ND ug/L 06/14/17 17:57 98-95-306/07/17 17:1010.0 1.6 1
2-Nitrophenol ND ug/L 06/14/17 17:57 88-75-506/07/17 17:1010.0 1.6 1
4-Nitrophenol ND ug/L 06/14/17 17:57 100-02-706/07/17 17:1050.0 4.3 1
5-Nitro-o-toluidine ND ug/L 06/14/17 17:57 99-55-806/07/17 17:1010.0 1.9 1
N-Nitrosodiethylamine ND ug/L 06/14/17 17:57 55-18-506/07/17 17:1020.0 1.4 1
N-Nitrosodimethylamine ND ug/L 06/14/17 17:57 62-75-906/07/17 17:1010.0 1.6 1
N-Nitroso-di-n-butylamine ND ug/L 06/14/17 17:57 924-16-306/07/17 17:1010.0 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 06/14/17 17:57 621-64-706/07/17 17:1010.0 1.7 1
N-Nitrosodiphenylamine ND ug/L 06/14/17 17:57 86-30-606/07/17 17:1010.0 1.4 1
N-Nitrosomethylethylamine ND ug/L 06/14/17 17:57 10595-95-606/07/17 17:1010.0 1.4 1
N-Nitrosopiperidine ND ug/L 06/14/17 17:57 100-75-406/07/17 17:1020.0 1.7 1
N-Nitrosopyrrolidine ND ug/L 06/14/17 17:57 930-55-206/07/17 17:1010.0 1.7 1
O,O,O-Triethylphosphorothioate ND ug/L 06/14/17 17:57 126-68-106/07/17 17:1010.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/14/17 17:57 108-60-106/07/17 17:1010.0 1.8 1
Parathion (Ethyl parathion)ND ug/L 06/14/17 17:57 56-38-206/07/17 17:1010.0 1.5 1
Pentachlorobenzene ND ug/L 06/14/17 17:57 608-93-506/07/17 17:1010.0 1.5 1
Pentachloronitrobenzene ND ug/L 06/14/17 17:57 82-68-806/07/17 17:1020.0 1.7 1
Pentachlorophenol ND ug/L 06/14/17 17:57 87-86-506/07/17 17:1025.0 3.5 1
Phenacetin ND ug/L 06/14/17 17:57 62-44-206/07/17 17:1020.0 1.9 1
Phenanthrene ND ug/L 06/14/17 17:57 85-01-806/07/17 17:1010.0 1.6 1
Phenol ND ug/L 06/14/17 17:57 108-95-206/07/17 17:1010.0 1.3 1
p-Phenylenediamine ND ug/L 06/14/17 17:57 106-50-306/07/17 17:1010.0 2.2 1
Phorate ND ug/L 06/14/17 17:57 298-02-206/07/17 17:1010.0 1.7 1
Pronamide ND ug/L 06/14/17 17:57 23950-58-506/07/17 17:1010.0 2.0 1
Pyrene ND ug/L 06/14/17 17:57 129-00-006/07/17 17:1010.0 2.2 1
Safrole ND ug/L 06/14/17 17:57 94-59-706/07/17 17:1010.0 1.3 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/14/17 17:57 95-94-306/07/17 17:1010.0 1.3 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/14/17 17:57 58-90-206/07/17 17:1010.0 2.9 1
Thionazin ND ug/L 06/14/17 17:57 297-97-206/07/17 17:1020.0 1.7 1
O-Toluidine ND ug/L 06/14/17 17:57 95-53-406/07/17 17:1010.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 06/14/17 17:57 95-95-406/07/17 17:1010.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/14/17 17:57 88-06-206/07/17 17:1010.0 1.4 1
1,3,5-Trinitrobenzene ND ug/L 06/14/17 17:57 99-35-406/07/17 17:1010.0 1.2 1
Surrogates
Nitrobenzene-d5 (S)74 %06/14/17 17:57 4165-60-006/07/17 17:1021-110 1
2-Fluorobiphenyl (S)89 %06/14/17 17:57 321-60-806/07/17 17:1027-110 1
Terphenyl-d14 (S)89 %06/14/17 17:57 1718-51-006/07/17 17:1031-107 1
Phenol-d6 (S)24 %06/14/17 17:57 13127-88-306/07/17 17:1010-110 1
2-Fluorophenol (S)37 %06/14/17 17:57 367-12-406/07/17 17:1012-110 1
2,4,6-Tribromophenol (S)86 %06/14/17 17:57 118-79-606/07/17 17:1027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 15.2J ug/L 06/02/17 10:29 67-64-110010.0 1
Acetonitrile ND ug/L 06/02/17 10:29 75-05-855.0 2.2 1
Acrolein ND ug/L 06/02/17 10:29 107-02-853.0 1.6 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
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Page 68 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-22 Lab ID:92342530005 Collected:05/31/17 16:10 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acrylonitrile ND ug/L 06/02/17 10:29 107-13-12001.9 1
Allyl chloride ND ug/L 06/02/17 10:29 107-05-110.0 1.5 1
Benzene ND ug/L 06/02/17 10:29 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/02/17 10:29 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/02/17 10:29 75-27-41.0 0.18 1
Bromoform ND ug/L 06/02/17 10:29 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/02/17 10:29 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/02/17 10:29 78-93-31000.96 1
Carbon disulfide ND ug/L 06/02/17 10:29 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/02/17 10:29 56-23-51.0 0.25 1
Chlorobenzene 0.42J ug/L 06/02/17 10:29 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/02/17 10:29 75-00-310.0 0.54 1
Chloroform ND ug/L 06/02/17 10:29 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/02/17 10:29 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/02/17 10:29 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/02/17 10:29 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/02/17 10:29 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/02/17 10:29 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/02/17 10:29 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/02/17 10:29 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/02/17 10:29 541-73-15.0 0.24 1
1,4-Dichlorobenzene 1.1 ug/L 06/02/17 10:29 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/02/17 10:29 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/02/17 10:29 75-71-85.0 0.21 1
1,1-Dichloroethane 0.63J ug/L 06/02/17 10:29 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/02/17 10:29 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/02/17 10:29 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.94J ug/L 06/02/17 10:29 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/02/17 10:29 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/02/17 10:29 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/02/17 10:29 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/02/17 10:29 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/02/17 10:29 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/02/17 10:29 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/02/17 10:29 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/02/17 10:29 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/02/17 10:29 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/02/17 10:29 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/02/17 10:29 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/02/17 10:29 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/02/17 10:29 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/02/17 10:29 126-98-71000.93 1
Methylene Chloride ND ug/L 06/02/17 10:29 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/02/17 10:29 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/02/17 10:29 108-10-11000.33 1
Naphthalene ND ug/L 06/02/17 10:29 91-20-310.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 166
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Sample:MW-22 Lab ID:92342530005 Collected:05/31/17 16:10 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Propionitrile ND ug/L 06/02/17 10:29 107-12-01503.6 1
Styrene ND ug/L 06/02/17 10:29 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/02/17 10:29 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/02/17 10:29 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/02/17 10:29 127-18-41.0 0.46 1
Toluene ND ug/L 06/02/17 10:29 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/02/17 10:29 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/02/17 10:29 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/02/17 10:29 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/02/17 10:29 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/02/17 10:29 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/02/17 10:29 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/02/17 10:29 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/02/17 10:29 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/02/17 10:29 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)126 %06/02/17 10:29 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %06/02/17 10:29 17060-07-070-130 1
Toluene-d8 (S)99 %06/02/17 10:29 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/06/17 23:00 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 4.7J ug/L 06/07/17 13:35 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 70 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363333
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92342478003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014275
Associated Lab Samples:92342478003
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 06/07/17 02:150.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014276LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.32.5 93 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014277MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342769001
2014278
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L M1125075-1250 25125NDNDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363457
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92342530001, 92342530002, 92342530003, 92342530004, 92342530005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2015058
Associated Lab Samples:92342530001, 92342530002, 92342530003, 92342530004, 92342530005
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 06/07/17 00:470.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2015059LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.42.5 96 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015060MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342619002
2015061
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 100 75-125101 1 252.5ND 2.5 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363459
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92342478004, 92342478005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2015066
Associated Lab Samples:92342478004, 92342478005
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 06/06/17 09:310.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2015067LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.42.5 95 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015068MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342658001
2015069
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L M1,R12.5 93 75-12562 40 252.5ND 2.4 1.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 73 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363009
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92342478001, 92342478002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2012414
Associated Lab Samples:92342478001, 92342478002
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 5.0 06/09/17 17:073.9
Arsenic ug/L ND 10.0 06/09/17 17:075.0
Barium ug/L ND 5.0 06/09/17 17:072.5
Beryllium ug/L ND 1.0 06/09/17 17:070.50
Cadmium ug/L ND 1.0 06/09/17 17:070.50
Chromium ug/L ND 5.0 06/09/17 17:072.5
Cobalt ug/L ND 5.0 06/09/17 17:072.5
Copper ug/L ND 5.0 06/09/17 17:072.5
Lead ug/L ND 5.0 06/09/17 17:072.5
Nickel ug/L ND 5.0 06/09/17 17:072.5
Selenium ug/L ND 10.0 06/09/17 17:075.0
Silver ug/L ND 5.0 06/09/17 17:072.5
Vanadium ug/L ND 5.0 06/09/17 17:072.5
Zinc ug/L ND 10.0 06/09/17 17:075.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012415LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 512500 102 80-120
Arsenic ug/L 488500 98 80-120
Barium ug/L 518500 104 80-120
Beryllium ug/L 518500 104 80-120
Cadmium ug/L 504500 101 80-120
Chromium ug/L 513500 103 80-120
Cobalt ug/L 520500 104 80-120
Copper ug/L 532500 106 80-120
Lead ug/L 504500 101 80-120
Nickel ug/L 507500 101 80-120
Selenium ug/L 490500 98 80-120
Silver ug/L 254250 102 80-120
Vanadium ug/L 511500 102 80-120
Zinc ug/L 512500 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2012416MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342475013
2012417
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 98 75-125100 2 20500ND490502
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 74 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2012416MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342475013
2012417
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L 500 95 75-12599 4 20500ND477494
Barium ug/L 500 102 75-125104 2 2050030.9 539 552
Beryllium ug/L 500 102 75-125105 3 205000.60J 510 524
Cadmium ug/L 500 99 75-125101 3 20500ND493505
Chromium ug/L 500 101 75-125104 3 205006.2 511 525
Cobalt ug/L 500 99 75-125103 3 20500ND499515
Copper ug/L 500 103 75-125106 3 205007.1 524 538
Lead ug/L 500 97 75-12599 2 205002.7J 486 498
Nickel ug/L 500 98 75-125101 3 205004.2J 492 507
Selenium ug/L 500 98 75-125101 2 20500ND496508
Silver ug/L 250 100 75-125102 2 20250ND251256
Vanadium ug/L 500 100 75-125103 3 2050019.2 518 534
Zinc ug/L 500 100 75-125104 3 205009.5J 512 528
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 75 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363010
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92342478003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2012421
Associated Lab Samples:92342478003
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 5.0 06/09/17 14:553.9
Arsenic ug/L ND 10.0 06/09/17 14:555.0
Barium ug/L ND 5.0 06/11/17 04:042.5
Beryllium ug/L ND 1.0 06/11/17 04:040.50
Cadmium ug/L ND 1.0 06/09/17 14:550.50
Chromium ug/L ND 5.0 06/09/17 14:552.5
Cobalt ug/L ND 5.0 06/09/17 14:552.5
Copper ug/L ND 5.0 06/11/17 04:042.5
Lead ug/L ND 5.0 06/09/17 14:552.5
Nickel ug/L ND 5.0 06/09/17 14:552.5
Selenium ug/L ND 10.0 06/09/17 14:555.0
Silver ug/L ND 5.0 06/11/17 04:042.5
Tin ug/L ND 5.0 06/09/17 14:552.5
Vanadium ug/L ND 5.0 06/09/17 14:552.5
Zinc ug/L ND 10.0 06/09/17 14:555.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012422LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 506500 101 80-120
Arsenic ug/L 486500 97 80-120
Barium ug/L 507500 101 80-120
Beryllium ug/L 475500 95 80-120
Cadmium ug/L 500500 100 80-120
Chromium ug/L 500500 100 80-120
Cobalt ug/L 503500 101 80-120
Copper ug/L 500500 100 80-120
Lead ug/L 494500 99 80-120
Nickel ug/L 491500 98 80-120
Selenium ug/L 507500 101 80-120
Silver ug/L 248250 99 80-120
Tin ug/L 505500 101 80-120
Vanadium ug/L 495500 99 80-120
Zinc ug/L 503500 101 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 76 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2012423MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342479004
2012424
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 98 75-12597 1 20500ND492487
Arsenic ug/L 500 96 75-12594 1 20500ND481475
Barium ug/L 500 100 75-12597 3 2050069.9J 572 555
Beryllium ug/L 500 94 75-12599 6 20500ND469498
Cadmium ug/L 500 99 75-12597 2 205004.6 498 488
Chromium ug/L 500 99 75-12597 2 205003.1J 498 488
Cobalt ug/L 500 99 75-12597 2 20500ND497488
Copper ug/L 500 99 75-125100 2 20500ND496504
Lead ug/L 500 96 75-12595 2 20500ND485476
Nickel ug/L 500 97 75-12595 2 205002.5J 488 476
Selenium ug/L 500 100 75-12598 2 20500ND501491
Silver ug/L 250 97 75-12599 2 20250ND243248
Tin ug/L 500 100 75-12598 2 20500ND499490
Vanadium ug/L 500 98 75-12597 1 205005.3J 495 488
Zinc ug/L 500 99 75-12597 1 2050013.0 507 499
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 77 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363146
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92342530001, 92342530002, 92342530003, 92342530004, 92342530005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2013277
Associated Lab Samples:92342530001, 92342530002, 92342530003, 92342530004, 92342530005
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 5.0 06/09/17 20:333.9
Arsenic ug/L ND 10.0 06/09/17 20:335.0
Barium ug/L ND 5.0 06/09/17 20:332.5
Beryllium ug/L ND 1.0 06/09/17 20:330.50
Cadmium ug/L ND 1.0 06/09/17 20:330.50
Chromium ug/L ND 5.0 06/10/17 16:232.5
Cobalt ug/L ND 5.0 06/09/17 20:332.5
Copper ug/L ND 5.0 06/09/17 20:332.5
Lead ug/L ND 5.0 06/09/17 20:332.5
Nickel ug/L ND 5.0 06/10/17 16:232.5
Selenium ug/L ND 10.0 06/09/17 20:335.0
Silver ug/L ND 5.0 06/09/17 20:332.5
Tin ug/L ND 5.0 06/09/17 20:332.5
Vanadium ug/L ND 5.0 06/09/17 20:332.5
Zinc ug/L ND 10.0 06/09/17 20:335.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2013278LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 493500 99 80-120
Arsenic ug/L 474500 95 80-120
Barium ug/L 497500 99 80-120
Beryllium ug/L 497500 99 80-120
Cadmium ug/L 496500 99 80-120
Chromium ug/L 494500 99 80-120
Cobalt ug/L 494500 99 80-120
Copper ug/L 496500 99 80-120
Lead ug/L 489500 98 80-120
Nickel ug/L 485500 97 80-120
Selenium ug/L 495500 99 80-120
Silver ug/L 247250 99 80-120
Tin ug/L 492500 98 80-120
Vanadium ug/L 484500 97 80-120
Zinc ug/L 496500 99 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 78 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2013279MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342472012
2013280
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 98 75-125101 2 20500ND491503
Arsenic ug/L 500 94 75-12597 2 20500ND472483
Barium ug/L 500 98 75-125102 3 205000.091
mg/L 582 602
Beryllium ug/L 500 99 75-125102 3 20500ND494510
Cadmium ug/L 500 99 75-125101 2 20500ND495506
Chromium ug/L 500 99 75-125102 3 20500ND493508
Cobalt ug/L 500 98 75-125101 2 20500ND492503
Copper ug/L 500 99 75-125101 3 20500ND494508
Lead ug/L 500 97 75-12599 2 20500ND485496
Nickel ug/L 500 97 75-12599 2 205000.016
mg/L 500 510
Selenium ug/L 500 98 75-125101 3 20500ND490507
Silver ug/L 250 99 75-125101 2 20250ND247252
Tin ug/L 500 99 75-125100 2 20500ND494503
Vanadium ug/L 500 96 75-12599 3 20500ND482495
Zinc ug/L 500 98 75-125101 2 205000.066
mg/L 557 569
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 79 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363321
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92342478004, 92342478005, 92342478006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014222
Associated Lab Samples:92342478004, 92342478005, 92342478006
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 5.0 06/14/17 21:193.9
Arsenic ug/L ND 10.0 06/14/17 21:195.0
Barium ug/L ND 5.0 06/14/17 21:192.5
Beryllium ug/L ND 1.0 06/14/17 21:190.50
Cadmium ug/L ND 1.0 06/14/17 21:190.50
Chromium ug/L ND 5.0 06/14/17 21:192.5
Cobalt ug/L ND 5.0 06/14/17 21:192.5
Copper ug/L ND 5.0 06/14/17 21:192.5
Lead ug/L ND 5.0 06/14/17 21:192.5
Nickel ug/L ND 5.0 06/14/17 21:192.5
Selenium ug/L ND 10.0 06/14/17 21:195.0
Silver ug/L ND 5.0 06/14/17 21:192.5
Tin ug/L ND 5.0 06/14/17 21:192.5
Vanadium ug/L ND 5.0 06/14/17 21:192.5
Zinc ug/L ND 10.0 06/14/17 21:195.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014223LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 496500 99 80-120
Arsenic ug/L 475500 95 80-120
Barium ug/L 511500 102 80-120
Beryllium ug/L 457500 91 80-120
Cadmium ug/L 512500 102 80-120
Chromium ug/L 463500 93 80-120
Cobalt ug/L 498500 100 80-120
Copper ug/L 494500 99 80-120
Lead ug/L 486500 97 80-120
Nickel ug/L 463500 93 80-120
Selenium ug/L 501500 100 80-120
Silver ug/L 235250 94 80-120
Tin ug/L 485500 97 80-120
Vanadium ug/L 456500 91 80-120
Zinc ug/L 472500 94 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 80 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014224MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342605016
2014225
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 103 75-125100 3 20500ND517501
Arsenic ug/L 500 100 75-12597 2 20500174672657
Barium ug/L 500 108 75-125104 3 205008.0 546 530
Beryllium ug/L 500 96 75-12594 2 205000.73J 481 471
Cadmium ug/L 500 108 75-125105 3 205001.7 540 524
Chromium ug/L 500 97 75-12594 3 20500ND486470
Cobalt ug/L 500 104 75-125100 3 2050075.0 594 577
Copper ug/L 500 104 75-125102 3 20500ND522509
Lead ug/L 500 100 75-12597 3 205004.4J 506 491
Nickel ug/L 500 96 75-12593 3 205003.2J 481 466
Selenium ug/L 500 102 75-125100 2 20500ND511501
Silver ug/L 250 99 75-12595 4 20250ND246238
Tin ug/L 500 101 75-12597 4 20500ND503484
Vanadium ug/L 500 96 75-12593 3 20500ND482466
Zinc ug/L 500 98 75-12595 3 205005.8J 495 479
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 81 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363322
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92342478007, 92342478008, 92342478009, 92342478010, 92342478011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014226
Associated Lab Samples:92342478007, 92342478008, 92342478009, 92342478010, 92342478011
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 5.0 06/09/17 18:443.9
Arsenic ug/L ND 10.0 06/09/17 18:445.0
Barium ug/L ND 5.0 06/09/17 18:442.5
Beryllium ug/L ND 1.0 06/09/17 18:440.50
Cadmium ug/L ND 1.0 06/09/17 18:440.50
Chromium ug/L ND 5.0 06/09/17 18:442.5
Cobalt ug/L ND 5.0 06/09/17 18:442.5
Copper ug/L ND 5.0 06/09/17 18:442.5
Lead ug/L ND 5.0 06/09/17 18:442.5
Nickel ug/L ND 5.0 06/09/17 18:442.5
Selenium ug/L ND 10.0 06/09/17 18:445.0
Silver ug/L ND 5.0 06/09/17 18:442.5
Vanadium ug/L ND 5.0 06/09/17 18:442.5
Zinc ug/L ND 10.0 06/09/17 18:445.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014227LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 515500 103 80-120
Arsenic ug/L 496500 99 80-120
Barium ug/L 514500 103 80-120
Beryllium ug/L 510500 102 80-120
Cadmium ug/L 516500 103 80-120
Chromium ug/L 507500 101 80-120
Cobalt ug/L 514500 103 80-120
Copper ug/L 520500 104 80-120
Lead ug/L 508500 102 80-120
Nickel ug/L 505500 101 80-120
Selenium ug/L 521500 104 80-120
Silver ug/L 258250 103 80-120
Vanadium ug/L 499500 100 80-120
Zinc ug/L 514500 103 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014228MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342478007
2014229
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 103 75-12598 6 20500ND518489
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 82 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014228MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342478007
2014229
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L 500 101 75-12596 6 20500ND506479
Barium ug/L 500 104 75-12599 5 2050023.5J 544 519
Beryllium ug/L 500 104 75-12598 5 20500ND518492
Cadmium ug/L 500 104 75-12599 5 205000.66J 520 495
Chromium ug/L 500 103 75-12599 4 20500ND516497
Cobalt ug/L 500 102 75-12597 5 20500ND513490
Copper ug/L 500 105 75-125100 5 205003.5J 526 503
Lead ug/L 500 100 75-12596 4 20500ND503482
Nickel ug/L 500 100 75-12596 4 205002.8J 503 481
Selenium ug/L 500 104 75-12599 5 20500ND522497
Silver ug/L 250 104 75-12599 5 20250ND260249
Vanadium ug/L 500 102 75-12598 4 20500ND513491
Zinc ug/L 500 103 75-12599 4 205006.6J 522 500
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 83 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363272
EPA 3010A
EPA 6020B
6020 MET
Associated Lab Samples:92342478001, 92342478002, 92342478003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014034
Associated Lab Samples:92342478001, 92342478002, 92342478003
Matrix:Water
AnalyzedMDL
Thallium ug/L ND 0.10 06/06/17 18:130.020
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014035LABORATORY CONTROL SAMPLE:
LCSSpike
Thallium ug/L 94.5100 95 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014036MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342297004
2014037
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Thallium ug/L 100 97 75-12595 2 201000.30J 97.2 95.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 84 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363273
EPA 3010A
EPA 6020B
6020 MET
Associated Lab Samples:92342478004, 92342478005, 92342478006, 92342478007, 92342478008, 92342478009, 92342478010,
92342478011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014038
Associated Lab Samples:92342478004, 92342478005, 92342478006, 92342478007, 92342478008, 92342478009, 92342478010,
92342478011
Matrix:Water
AnalyzedMDL
Thallium ug/L ND 0.10 06/09/17 16:010.020
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014039LABORATORY CONTROL SAMPLE:
LCSSpike
Thallium ug/L 91.8100 92 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014040MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342600010
2014041
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Thallium ug/L 100 91 75-12593 3 20100ND90.7 93.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 85 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363478
EPA 3010A
EPA 6020B
6020 MET
Associated Lab Samples:92342530001, 92342530002, 92342530003, 92342530004, 92342530005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2015139
Associated Lab Samples:92342530001, 92342530002, 92342530003, 92342530004, 92342530005
Matrix:Water
AnalyzedMDL
Thallium ug/L ND 0.10 06/09/17 16:550.020
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2015140LABORATORY CONTROL SAMPLE:
LCSSpike
Thallium ug/L 90.8100 91 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015141MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342795001
2015142
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Thallium ug/L 100 92 75-12596 4 201000.090J 91.9 96.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 86 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363024
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92342478001, 92342478002, 92342478003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2012502
Associated Lab Samples:92342478001, 92342478002, 92342478003
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/02/17 00:550.33
1,1,1-Trichloroethane ug/L ND 1.0 06/02/17 00:550.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 06/02/17 00:550.40
1,1,2-Trichloroethane ug/L ND 1.0 06/02/17 00:550.29
1,1-Dichloroethane ug/L ND 5.0 06/02/17 00:550.32
1,1-Dichloroethene ug/L ND 5.0 06/02/17 00:550.56
1,1-Dichloropropene ug/L ND 5.0 06/02/17 00:550.49
1,2,3-Trichloropropane ug/L ND 1.0 06/02/17 00:550.41
1,2,4-Trichlorobenzene ug/L ND 10.0 06/02/17 00:550.35
1,2-Dibromo-3-chloropropane ug/L ND 13.0 06/02/17 00:552.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/02/17 00:550.27
1,2-Dichlorobenzene ug/L ND 5.0 06/02/17 00:550.30
1,2-Dichloroethane ug/L ND 1.0 06/02/17 00:550.24
1,2-Dichloropropane ug/L ND 1.0 06/02/17 00:550.27
1,3-Dichlorobenzene ug/L ND 5.0 06/02/17 00:550.24
1,3-Dichloropropane ug/L ND 1.0 06/02/17 00:550.28
1,4-Dichlorobenzene ug/L ND 1.0 06/02/17 00:550.33
2,2-Dichloropropane ug/L ND 15.0 06/02/17 00:550.13
2-Butanone (MEK)ug/L ND 100 06/02/17 00:550.96
2-Hexanone ug/L ND 50.0 06/02/17 00:550.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 06/02/17 00:550.33
Acetone ug/L ND 100 06/02/17 00:5510.0
Acetonitrile ug/L ND 55.0 06/02/17 00:552.2
Acrolein ug/L ND 53.0 06/02/17 00:551.6
Acrylonitrile ug/L ND 200 06/02/17 00:551.9
Allyl chloride ug/L ND 10.0 06/02/17 00:551.5
Benzene ug/L ND 1.0 06/02/17 00:550.25
Bromochloromethane ug/L ND 3.0 06/02/17 00:550.17
Bromodichloromethane ug/L ND 1.0 06/02/17 00:550.18
Bromoform ug/L ND 3.0 06/02/17 00:550.26
Bromomethane ug/L ND 10.0 06/02/17 00:550.29
Carbon disulfide ug/L ND 100 06/02/17 00:551.2
Carbon tetrachloride ug/L ND 1.0 06/02/17 00:550.25
Chlorobenzene ug/L ND 3.0 06/02/17 00:550.23
Chloroethane ug/L ND 10.0 06/02/17 00:550.54
Chloroform ug/L ND 5.0 06/02/17 00:550.14
Chloromethane ug/L ND 1.0 06/02/17 00:550.11
Chloroprene ug/L ND 20.0 06/02/17 00:550.27
cis-1,2-Dichloroethene ug/L ND 5.0 06/02/17 00:550.19
cis-1,3-Dichloropropene ug/L ND 1.0 06/02/17 00:550.13
Dibromochloromethane ug/L ND 3.0 06/02/17 00:550.21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 87 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2012502
Associated Lab Samples:92342478001, 92342478002, 92342478003
Matrix:Water
AnalyzedMDL
Dibromomethane ug/L ND 10.0 06/02/17 00:550.21
Dichlorodifluoromethane ug/L ND 5.0 06/02/17 00:550.21
Ethyl methacrylate ug/L ND 10.0 06/02/17 00:550.20
Ethylbenzene ug/L ND 1.0 06/02/17 00:550.30
Hexachloro-1,3-butadiene ug/L ND 10.0 06/02/17 00:550.71
Iodomethane ug/L ND 10.0 06/02/17 00:550.32
Isobutanol ug/L ND 100 06/02/17 00:5535.0
Methacrylonitrile ug/L ND 100 06/02/17 00:550.93
Methyl methacrylate ug/L ND 30.0 06/02/17 00:552.0
Methylene Chloride ug/L ND 1.0 06/02/17 00:550.97
Naphthalene ug/L ND 10.0 06/02/17 00:550.24
Propionitrile ug/L ND 150 06/02/17 00:553.6
Styrene ug/L ND 1.0 06/02/17 00:550.26
Tetrachloroethene ug/L ND 1.0 06/02/17 00:550.46
Toluene ug/L ND 1.0 06/02/17 00:550.26
trans-1,2-Dichloroethene ug/L ND 5.0 06/02/17 00:550.49
trans-1,3-Dichloropropene ug/L ND 1.0 06/02/17 00:550.26
trans-1,4-Dichloro-2-butene ug/L ND 100 06/02/17 00:551.0
Trichloroethene ug/L ND 1.0 06/02/17 00:550.47
Trichlorofluoromethane ug/L ND 1.0 06/02/17 00:550.20
Vinyl acetate ug/L ND 50.0 06/02/17 00:550.35
Vinyl chloride ug/L ND 1.0 06/02/17 00:550.62
Xylene (Total)ug/L ND 5.0 06/02/17 00:550.66
1,2-Dichloroethane-d4 (S)%99 70-130 06/02/17 00:55
4-Bromofluorobenzene (S)%115 70-130 06/02/17 00:55
Toluene-d8 (S)%110 70-130 06/02/17 00:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012503LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.950 102 80-125
1,1,1-Trichloroethane ug/L 46.350 93 71-129
1,1,2,2-Tetrachloroethane ug/L 54.250 108 79-124
1,1,2-Trichloroethane ug/L 50.150 100 85-125
1,1-Dichloroethane ug/L 44.050 88 73-126
1,1-Dichloroethene ug/L 38.450 77 66-135
1,1-Dichloropropene ug/L 50.350 101 74-135
1,2,3-Trichloropropane ug/L 54.550 109 75-130
1,2,4-Trichlorobenzene ug/L 43.150 86 75-134
1,2-Dibromo-3-chloropropane ug/L 46.850 94 71-133
1,2-Dibromoethane (EDB)ug/L 51.850 104 83-124
1,2-Dichlorobenzene ug/L 45.750 91 80-133
1,2-Dichloroethane ug/L 44.150 88 67-128
1,2-Dichloropropane ug/L 47.550 95 75-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 88 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012503LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 46.750 93 77-130
1,3-Dichloropropane ug/L 52.150 104 76-131
1,4-Dichlorobenzene ug/L 46.850 94 78-130
2,2-Dichloropropane ug/L 42.650 85 40-160
2-Butanone (MEK)ug/L 105100 105 61-144
2-Hexanone ug/L 99.7100 100 68-143
4-Methyl-2-pentanone (MIBK)ug/L 103100 103 72-135
Acetone ug/L 107100 107 48-146
Acetonitrile ug/L 527500 105 62-150
Acrolein ug/L 280250 112 24-160
Acrylonitrile ug/L 234250 94 40-160
Allyl chloride ug/L 41.550 83 66-137
Benzene ug/L 47.550 95 80-125
Bromochloromethane ug/L 45.750 91 71-125
Bromodichloromethane ug/L 47.150 94 78-124
Bromoform ug/L 57.550 115 71-128
Bromomethane ug/L 50.350 101 40-160
Carbon disulfide ug/L 40.5J50 81 50-160
Carbon tetrachloride ug/L 47.050 94 69-131
Chlorobenzene ug/L 46.650 93 81-122
Chloroethane ug/L 46.950 94 39-148
Chloroform ug/L 42.950 86 73-127
Chloromethane ug/L 52.850 106 44-146
Chloroprene ug/L 46.050 92 75-145
cis-1,2-Dichloroethene ug/L 45.450 91 74-124
cis-1,3-Dichloropropene ug/L 50.650 101 72-132
Dibromochloromethane ug/L 53.650 107 78-125
Dibromomethane ug/L 45.150 90 82-120
Dichlorodifluoromethane ug/L 39.350 79 34-157
Ethyl methacrylate ug/L 52.150 104 82-121
Ethylbenzene ug/L 48.150 96 79-121
Hexachloro-1,3-butadiene ug/L 44.250 88 72-131
Iodomethane ug/L 71.3100 71 39-154
Isobutanol ug/L 10501000 105 34-160
Methacrylonitrile ug/L 520500 104 74-134
Methyl methacrylate ug/L 46.950 94 84-124
Methylene Chloride ug/L 48.250 96 64-133
Naphthalene ug/L 45.250 90 73-133
Propionitrile ug/L 503500 101 73-140
Styrene ug/L 51.050 102 84-126
Tetrachloroethene ug/L 49.050 98 78-122
Toluene ug/L 48.250 96 80-121
trans-1,2-Dichloroethene ug/L 44.550 89 71-127
trans-1,3-Dichloropropene ug/L 53.150 106 69-141
trans-1,4-Dichloro-2-butene ug/L 63.5J50 127 40-160
Trichloroethene ug/L 48.850 98 78-122
Trichlorofluoromethane ug/L 45.950 92 53-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 89 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012503LABORATORY CONTROL SAMPLE:
LCSSpike
Vinyl acetate ug/L 92.9100 93 40-160
Vinyl chloride ug/L 41.950 84 58-137
Xylene (Total)ug/L 147150 98 81-126
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%113 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2012504MATRIX SPIKE SAMPLE:
MSSpike
Result
92342478001
1,1,1,2-Tetrachloroethane ug/L 19.520 98 70-130ND
1,1,1-Trichloroethane ug/L 22.420 112 70-130ND
1,1,2,2-Tetrachloroethane ug/L 21.420 107 70-130ND
1,1,2-Trichloroethane ug/L 18.020 90 70-130ND
1,1-Dichloroethane ug/L 21.820 109 70-130ND
1,1-Dichloroethene ug/L 25.920 129 70-166ND
1,1-Dichloropropene ug/L 22.920 114 70-130ND
1,2,3-Trichloropropane ug/L 20.920 105 70-130ND
1,2,4-Trichlorobenzene ug/L 18.520 92 70-130ND
1,2-Dibromo-3-chloropropane ug/L 16.920 85 70-130ND
1,2-Dibromoethane (EDB)ug/L 16.920 85 70-130ND
1,2-Dichlorobenzene ug/L 19.720 98 70-130ND
1,2-Dichloroethane ug/L 19.820 99 70-130ND
1,2-Dichloropropane ug/L 21.120 105 70-130ND
1,3-Dichlorobenzene ug/L 19.920 99 70-130ND
1,3-Dichloropropane ug/L 16.920 85 70-130ND
1,4-Dichlorobenzene ug/L 19.920 99 70-130ND
2,2-Dichloropropane ug/L 17.220 86 70-130ND
2-Butanone (MEK)ug/L 32.6J40 82 70-130ND
2-Hexanone ug/L 31.4J40 78 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 30.1J40 75 70-130ND
Acetone ug/L 39.6J40 99 70-130ND
Acetonitrile ug/L 182200 91 70-130ND
Acrolein ug/L 110100 110 70-130ND
Acrylonitrile ug/L 94.7J100 95 70-130ND
Allyl chloride ug/L 21.220 106 70-130ND
Benzene ug/L 21.020 105 70-148ND
Bromochloromethane ug/L 22.220 111 70-130ND
Bromodichloromethane ug/L 20.620 103 70-130ND
Bromoform ug/L 20.120 100 70-130ND
Bromomethane ug/L 22.620 113 70-130ND
Carbon disulfide ug/L 25.5J20 127 70-130ND
Carbon tetrachloride ug/L 21.620 108 70-130ND
Chlorobenzene ug/L 20.520 102 70-146ND
Chloroethane ug/L 23.920 119 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 90 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2012504MATRIX SPIKE SAMPLE:
MSSpike
Result
92342478001
Chloroform ug/L 20.520 102 70-130ND
Chloromethane ug/L 26.6 M12013370-130ND
Chloroprene ug/L 20.920 105 70-130ND
cis-1,2-Dichloroethene ug/L 22.120 110 70-130ND
cis-1,3-Dichloropropene ug/L 16.120 80 70-130ND
Dibromochloromethane ug/L 16.720 83 70-130ND
Dibromomethane ug/L 19.520 98 70-130ND
Dichlorodifluoromethane ug/L 17.420 87 70-130ND
Ethyl methacrylate ug/L 15.220 76 70-130ND
Ethylbenzene ug/L 21.720 109 70-130ND
Hexachloro-1,3-butadiene ug/L 18.920 94 70-130ND
Iodomethane ug/L 42.440 106 70-130ND
Isobutanol ug/L 301400 75 70-130ND
Methacrylonitrile ug/L 188200 94 70-130ND
Methyl methacrylate ug/L 17.4J20 87 70-130ND
Methylene Chloride ug/L 21.720 108 70-130ND
Naphthalene ug/L 17.820 89 70-130ND
Propionitrile ug/L 188200 94 70-130ND
Styrene ug/L 22.420 112 70-130ND
Tetrachloroethene ug/L 17.220 86 70-130ND
Toluene ug/L 18.620 93 70-155ND
trans-1,2-Dichloroethene ug/L 21.820 109 70-130ND
trans-1,3-Dichloropropene ug/L 17.120 85 70-130ND
trans-1,4-Dichloro-2-butene ug/L 18.9J20 94 70-130ND
Trichloroethene ug/L 21.920 109 69-151ND
Trichlorofluoromethane ug/L 23.620 118 70-130ND
Vinyl acetate ug/L 25.4J M1406470-130ND
Vinyl chloride ug/L 21.320 106 70-130ND
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%116 70-130
Toluene-d8 (S)%85 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342478002
2012505SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 0.48J 300.43J
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 91 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342478002
2012505SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acetonitrile ug/L ND 30ND
Acrolein ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Allyl chloride ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
Chloroprene ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 0.43J 300.39J
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Ethyl methacrylate ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Isobutanol ug/L ND 30ND
Methacrylonitrile ug/L ND 30ND
Methyl methacrylate ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
Propionitrile ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 92 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342478002
2012505SAMPLE DUPLICATE:
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%103 3100
4-Bromofluorobenzene (S)%114 1113
Toluene-d8 (S)%113 1111
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 93 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363026
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92342530001, 92342530002, 92342530003, 92342530005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2012510
Associated Lab Samples:92342530001, 92342530002, 92342530003, 92342530005
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/02/17 01:120.33
1,1,1-Trichloroethane ug/L ND 1.0 06/02/17 01:120.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 06/02/17 01:120.40
1,1,2-Trichloroethane ug/L ND 1.0 06/02/17 01:120.29
1,1-Dichloroethane ug/L ND 5.0 06/02/17 01:120.32
1,1-Dichloroethene ug/L ND 5.0 06/02/17 01:120.56
1,1-Dichloropropene ug/L ND 5.0 06/02/17 01:120.49
1,2,3-Trichloropropane ug/L ND 1.0 06/02/17 01:120.41
1,2,4-Trichlorobenzene ug/L ND 10.0 06/02/17 01:120.35
1,2-Dibromo-3-chloropropane ug/L ND 13.0 06/02/17 01:122.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/02/17 01:120.27
1,2-Dichlorobenzene ug/L ND 5.0 06/02/17 01:120.30
1,2-Dichloroethane ug/L ND 1.0 06/02/17 01:120.24
1,2-Dichloropropane ug/L ND 1.0 06/02/17 01:120.27
1,3-Dichlorobenzene ug/L ND 5.0 06/02/17 01:120.24
1,3-Dichloropropane ug/L ND 1.0 06/02/17 01:120.28
1,4-Dichlorobenzene ug/L ND 1.0 06/02/17 01:120.33
2,2-Dichloropropane ug/L ND 15.0 06/02/17 01:120.13
2-Butanone (MEK)ug/L ND 100 06/02/17 01:120.96
2-Hexanone ug/L ND 50.0 06/02/17 01:120.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 06/02/17 01:120.33
Acetone ug/L ND 100 06/02/17 01:1210.0
Acetonitrile ug/L ND 55.0 06/02/17 01:122.2
Acrolein ug/L ND 53.0 06/02/17 01:121.6
Acrylonitrile ug/L ND 200 06/02/17 01:121.9
Allyl chloride ug/L ND 10.0 06/02/17 01:121.5
Benzene ug/L ND 1.0 06/02/17 01:120.25
Bromochloromethane ug/L ND 3.0 06/02/17 01:120.17
Bromodichloromethane ug/L ND 1.0 06/02/17 01:120.18
Bromoform ug/L ND 3.0 06/02/17 01:120.26
Bromomethane ug/L ND 10.0 06/02/17 01:120.29
Carbon disulfide ug/L ND 100 06/02/17 01:121.2
Carbon tetrachloride ug/L ND 1.0 06/02/17 01:120.25
Chlorobenzene ug/L ND 3.0 06/02/17 01:120.23
Chloroethane ug/L ND 10.0 06/02/17 01:120.54
Chloroform ug/L ND 5.0 06/02/17 01:120.14
Chloromethane ug/L ND 1.0 06/02/17 01:120.11
Chloroprene ug/L ND 20.0 06/02/17 01:120.27
cis-1,2-Dichloroethene ug/L ND 5.0 06/02/17 01:120.19
cis-1,3-Dichloropropene ug/L ND 1.0 06/02/17 01:120.13
Dibromochloromethane ug/L ND 3.0 06/02/17 01:120.21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
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Page 94 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2012510
Associated Lab Samples:92342530001, 92342530002, 92342530003, 92342530005
Matrix:Water
AnalyzedMDL
Dibromomethane ug/L ND 10.0 06/02/17 01:120.21
Dichlorodifluoromethane ug/L ND 5.0 06/02/17 01:120.21
Ethyl methacrylate ug/L ND 10.0 06/02/17 01:120.20
Ethylbenzene ug/L ND 1.0 06/02/17 01:120.30
Hexachloro-1,3-butadiene ug/L ND 10.0 06/02/17 01:120.71
Iodomethane ug/L ND 10.0 06/02/17 01:120.32
Isobutanol ug/L ND 100 06/02/17 01:1235.0
Methacrylonitrile ug/L ND 100 06/02/17 01:120.93
Methyl methacrylate ug/L ND 30.0 06/02/17 01:122.0
Methylene Chloride ug/L ND 1.0 06/02/17 01:120.97
Naphthalene ug/L ND 10.0 06/02/17 01:120.24
Propionitrile ug/L ND 150 06/02/17 01:123.6
Styrene ug/L ND 1.0 06/02/17 01:120.26
Tetrachloroethene ug/L ND 1.0 06/02/17 01:120.46
Toluene ug/L ND 1.0 06/02/17 01:120.26
trans-1,2-Dichloroethene ug/L ND 5.0 06/02/17 01:120.49
trans-1,3-Dichloropropene ug/L ND 1.0 06/02/17 01:120.26
trans-1,4-Dichloro-2-butene ug/L ND 100 06/02/17 01:121.0
Trichloroethene ug/L ND 1.0 06/02/17 01:120.47
Trichlorofluoromethane ug/L ND 1.0 06/02/17 01:120.20
Vinyl acetate ug/L ND 50.0 06/02/17 01:120.35
Vinyl chloride ug/L ND 1.0 06/02/17 01:120.62
Xylene (Total)ug/L ND 5.0 06/02/17 01:120.66
1,2-Dichloroethane-d4 (S)%102 70-130 06/02/17 01:12
4-Bromofluorobenzene (S)%114 70-130 06/02/17 01:12
Toluene-d8 (S)%111 70-130 06/02/17 01:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012511LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.850 102 80-125
1,1,1-Trichloroethane ug/L 45.550 91 71-129
1,1,2,2-Tetrachloroethane ug/L 55.150 110 79-124
1,1,2-Trichloroethane ug/L 51.250 102 85-125
1,1-Dichloroethane ug/L 43.350 87 73-126
1,1-Dichloroethene ug/L 37.050 74 66-135
1,1-Dichloropropene ug/L 49.650 99 74-135
1,2,3-Trichloropropane ug/L 55.250 110 75-130
1,2,4-Trichlorobenzene ug/L 44.450 89 75-134
1,2-Dibromo-3-chloropropane ug/L 48.050 96 71-133
1,2-Dibromoethane (EDB)ug/L 51.950 104 83-124
1,2-Dichlorobenzene ug/L 46.250 92 80-133
1,2-Dichloroethane ug/L 42.250 84 67-128
1,2-Dichloropropane ug/L 47.850 96 75-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 95 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012511LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 47.550 95 77-130
1,3-Dichloropropane ug/L 51.950 104 76-131
1,4-Dichlorobenzene ug/L 47.250 94 78-130
2,2-Dichloropropane ug/L 42.050 84 40-160
2-Butanone (MEK)ug/L 104100 104 61-144
2-Hexanone ug/L 104100 104 68-143
4-Methyl-2-pentanone (MIBK)ug/L 106100 106 72-135
Acetone ug/L 103100 103 48-146
Acetonitrile ug/L 501500 100 62-150
Acrolein ug/L 342250 137 24-160
Acrylonitrile ug/L 230250 92 40-160
Allyl chloride ug/L 39.950 80 66-137
Benzene ug/L 47.950 96 80-125
Bromochloromethane ug/L 44.650 89 71-125
Bromodichloromethane ug/L 46.850 94 78-124
Bromoform ug/L 57.350 115 71-128
Bromomethane ug/L 51.450 103 40-160
Carbon disulfide ug/L 42.2J50 84 50-160
Carbon tetrachloride ug/L 47.050 94 69-131
Chlorobenzene ug/L 46.850 94 81-122
Chloroethane ug/L 47.250 94 39-148
Chloroform ug/L 44.050 88 73-127
Chloromethane ug/L 51.050 102 44-146
Chloroprene ug/L 45.550 91 75-145
cis-1,2-Dichloroethene ug/L 44.550 89 74-124
cis-1,3-Dichloropropene ug/L 51.450 103 72-132
Dibromochloromethane ug/L 54.750 109 78-125
Dibromomethane ug/L 45.750 91 82-120
Dichlorodifluoromethane ug/L 38.350 77 34-157
Ethyl methacrylate ug/L 52.550 105 82-121
Ethylbenzene ug/L 48.250 96 79-121
Hexachloro-1,3-butadiene ug/L 40.450 81 72-131
Iodomethane ug/L 90.6100 91 39-154
Isobutanol ug/L 10601000 106 34-160
Methacrylonitrile ug/L 514500 103 74-134
Methyl methacrylate ug/L 48.050 96 84-124
Methylene Chloride ug/L 46.650 93 64-133
Naphthalene ug/L 46.350 93 73-133
Propionitrile ug/L 489500 98 73-140
Styrene ug/L 51.350 103 84-126
Tetrachloroethene ug/L 49.250 98 78-122
Toluene ug/L 48.650 97 80-121
trans-1,2-Dichloroethene ug/L 43.750 87 71-127
trans-1,3-Dichloropropene ug/L 53.550 107 69-141
trans-1,4-Dichloro-2-butene ug/L 61.6J50 123 40-160
Trichloroethene ug/L 49.450 99 78-122
Trichlorofluoromethane ug/L 41.050 82 53-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 96 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012511LABORATORY CONTROL SAMPLE:
LCSSpike
Vinyl acetate ug/L 91.3100 91 40-160
Vinyl chloride ug/L 40.850 82 58-137
Xylene (Total)ug/L 147150 98 81-126
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%112 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2013904MATRIX SPIKE SAMPLE:
MSSpike
Result
92342317013
1,1,1,2-Tetrachloroethane ug/L 21.420 107 70-130ND
1,1,1-Trichloroethane ug/L 22.220 111 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.320 101 70-130ND
1,1,2-Trichloroethane ug/L 21.520 108 70-130ND
1,1-Dichloroethane ug/L 22.020 110 70-130ND
1,1-Dichloroethene ug/L 24.020 120 70-166ND
1,1-Dichloropropene ug/L 22.520 113 70-130ND
1,2,3-Trichloropropane ug/L 19.820 99 70-130ND
1,2,4-Trichlorobenzene ug/L 22.420 112 70-130ND
1,2-Dibromo-3-chloropropane ug/L 20.620 103 70-130ND
1,2-Dibromoethane (EDB)ug/L 20.420 102 70-130ND
1,2-Dichlorobenzene ug/L 21.020 105 70-130ND
1,2-Dichloroethane ug/L 22.020 110 70-130ND
1,2-Dichloropropane ug/L 21.920 109 70-130ND
1,3-Dichlorobenzene ug/L 20.320 101 70-130ND
1,3-Dichloropropane ug/L 21.420 107 70-130ND
1,4-Dichlorobenzene ug/L 19.920 99 70-130ND
2,2-Dichloropropane ug/L 11.5J M1205770-130ND
2-Butanone (MEK)ug/L 40.8J40 102 70-130ND
2-Hexanone ug/L 39.5J40 99 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 41.2J40 103 70-130ND
Acetone ug/L 52.9J40 104 70-13011.2J
Acetonitrile ug/L 196200 98 70-130ND
Acrolein ug/L 120100 120 70-130ND
Acrylonitrile ug/L 102J100 102 70-130ND
Allyl chloride ug/L 17.920 89 70-130ND
Benzene ug/L 21.920 110 70-148ND
Bromochloromethane ug/L 23.320 116 70-130ND
Bromodichloromethane ug/L 22.220 111 70-130ND
Bromoform ug/L 15.920 80 70-130ND
Bromomethane ug/L 27.0 M12013570-130ND
Carbon disulfide ug/L 22.8J20 114 70-130ND
Carbon tetrachloride ug/L 22.020 110 70-130ND
Chlorobenzene ug/L 21.020 105 70-146ND
Chloroethane ug/L 19.020 95 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 97 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2013904MATRIX SPIKE SAMPLE:
MSSpike
Result
92342317013
Chloroform ug/L 22.820 114 70-130ND
Chloromethane ug/L 18.720 93 70-130ND
Chloroprene ug/L 20.120 101 70-130ND
cis-1,2-Dichloroethene ug/L 23.120 115 70-130ND
cis-1,3-Dichloropropene ug/L 19.820 99 70-130ND
Dibromochloromethane ug/L 20.820 104 70-130ND
Dibromomethane ug/L 22.120 110 70-130ND
Dichlorodifluoromethane ug/L 18.720 93 70-130ND
Ethyl methacrylate ug/L 19.520 97 70-130ND
Ethylbenzene ug/L 21.320 107 70-130ND
Hexachloro-1,3-butadiene ug/L 22.320 112 70-130ND
Iodomethane ug/L 42.340 106 70-130ND
Isobutanol ug/L 361400 90 70-130ND
Methacrylonitrile ug/L 211200 105 70-130ND
Methyl methacrylate ug/L 19.9J20 100 70-130ND
Methylene Chloride ug/L 18.520 92 70-130ND
Naphthalene ug/L 25.220 126 70-130ND
Propionitrile ug/L 201200 100 70-130ND
Styrene ug/L 20.820 104 70-130ND
Tetrachloroethene ug/L 19.020 95 70-130ND
Toluene ug/L 22.520 112 70-155ND
trans-1,2-Dichloroethene ug/L 22.520 112 70-130ND
trans-1,3-Dichloropropene ug/L 18.920 94 70-130ND
trans-1,4-Dichloro-2-butene ug/L 14.6J20 73 70-130ND
Trichloroethene ug/L 21.620 108 69-151ND
Trichlorofluoromethane ug/L 23.020 115 70-130ND
Vinyl acetate ug/L 23.3J M1405870-130ND
Vinyl chloride ug/L 21.020 105 70-130ND
1,2-Dichloroethane-d4 (S)%110 70-130
4-Bromofluorobenzene (S)%96 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342317012
2012513SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 98 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342317012
2012513SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L 10.4J 3012.1J
Acetonitrile ug/L ND 30ND
Acrolein ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Allyl chloride ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
Chloroprene ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Ethyl methacrylate ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Isobutanol ug/L ND 30ND
Methacrylonitrile ug/L ND 30ND
Methyl methacrylate ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
Propionitrile ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 99 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342317012
2012513SAMPLE DUPLICATE:
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L 1.2 17 301.0
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%99 099
4-Bromofluorobenzene (S)%112 7119
Toluene-d8 (S)%83 30112
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 100 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363307
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92342530004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014180
Associated Lab Samples:92342530004
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/04/17 06:410.33
1,1,1-Trichloroethane ug/L ND 1.0 06/04/17 06:410.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 06/04/17 06:410.40
1,1,2-Trichloroethane ug/L ND 1.0 06/04/17 06:410.29
1,1-Dichloroethane ug/L ND 5.0 06/04/17 06:410.32
1,1-Dichloroethene ug/L ND 5.0 06/04/17 06:410.56
1,1-Dichloropropene ug/L ND 5.0 06/04/17 06:410.49
1,2,3-Trichloropropane ug/L ND 1.0 06/04/17 06:410.41
1,2,4-Trichlorobenzene ug/L ND 10.0 06/04/17 06:410.35
1,2-Dibromo-3-chloropropane ug/L ND 13.0 06/04/17 06:412.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/04/17 06:410.27
1,2-Dichlorobenzene ug/L ND 5.0 06/04/17 06:410.30
1,2-Dichloroethane ug/L ND 1.0 06/04/17 06:410.24
1,2-Dichloropropane ug/L ND 1.0 06/04/17 06:410.27
1,3-Dichlorobenzene ug/L ND 5.0 06/04/17 06:410.24
1,3-Dichloropropane ug/L ND 1.0 06/04/17 06:410.28
1,4-Dichlorobenzene ug/L ND 1.0 06/04/17 06:410.33
2,2-Dichloropropane ug/L ND 15.0 06/04/17 06:410.13
2-Butanone (MEK)ug/L ND 100 06/04/17 06:410.96
2-Hexanone ug/L ND 50.0 06/04/17 06:410.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 06/04/17 06:410.33
Acetone ug/L ND 100 06/04/17 06:4110.0
Acetonitrile ug/L ND 55.0 06/04/17 06:412.2
Acrolein ug/L ND 53.0 06/04/17 06:411.6
Acrylonitrile ug/L ND 200 06/04/17 06:411.9
Allyl chloride ug/L ND 10.0 06/04/17 06:411.5
Benzene ug/L ND 1.0 06/04/17 06:410.25
Bromochloromethane ug/L ND 3.0 06/04/17 06:410.17
Bromodichloromethane ug/L ND 1.0 06/04/17 06:410.18
Bromoform ug/L ND 3.0 06/04/17 06:410.26
Bromomethane ug/L ND 10.0 06/04/17 06:410.29
Carbon disulfide ug/L ND 100 06/04/17 06:411.2
Carbon tetrachloride ug/L ND 1.0 06/04/17 06:410.25
Chlorobenzene ug/L ND 3.0 06/04/17 06:410.23
Chloroethane ug/L ND 10.0 06/04/17 06:410.54
Chloroform ug/L ND 5.0 06/04/17 06:410.14
Chloromethane ug/L ND 1.0 06/04/17 06:410.11
Chloroprene ug/L ND 20.0 06/04/17 06:410.27
cis-1,2-Dichloroethene ug/L ND 5.0 06/04/17 06:410.19
cis-1,3-Dichloropropene ug/L ND 1.0 06/04/17 06:410.13
Dibromochloromethane ug/L ND 3.0 06/04/17 06:410.21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 101 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014180
Associated Lab Samples:92342530004
Matrix:Water
AnalyzedMDL
Dibromomethane ug/L ND 10.0 06/04/17 06:410.21
Dichlorodifluoromethane ug/L ND 5.0 06/04/17 06:410.21
Ethyl methacrylate ug/L ND 10.0 06/04/17 06:410.20
Ethylbenzene ug/L ND 1.0 06/04/17 06:410.30
Hexachloro-1,3-butadiene ug/L 1.6J 10.0 06/04/17 06:410.71
Iodomethane ug/L ND 10.0 06/04/17 06:410.32
Isobutanol ug/L ND 100 06/04/17 06:4135.0
Methacrylonitrile ug/L ND 100 06/04/17 06:410.93
Methyl methacrylate ug/L ND 30.0 06/04/17 06:412.0
Methylene Chloride ug/L ND 1.0 06/04/17 06:410.97
Naphthalene ug/L ND 10.0 06/04/17 06:410.24
Propionitrile ug/L ND 150 06/04/17 06:413.6
Styrene ug/L ND 1.0 06/04/17 06:410.26
Tetrachloroethene ug/L ND 1.0 06/04/17 06:410.46
Toluene ug/L ND 1.0 06/04/17 06:410.26
trans-1,2-Dichloroethene ug/L ND 5.0 06/04/17 06:410.49
trans-1,3-Dichloropropene ug/L ND 1.0 06/04/17 06:410.26
trans-1,4-Dichloro-2-butene ug/L ND 100 06/04/17 06:411.0
Trichloroethene ug/L ND 1.0 06/04/17 06:410.47
Trichlorofluoromethane ug/L ND 1.0 06/04/17 06:410.20
Vinyl acetate ug/L ND 50.0 06/04/17 06:410.35
Vinyl chloride ug/L ND 1.0 06/04/17 06:410.62
Xylene (Total)ug/L ND 5.0 06/04/17 06:410.66
1,2-Dichloroethane-d4 (S)%89 70-130 06/04/17 06:41
4-Bromofluorobenzene (S)%113 70-130 06/04/17 06:41
Toluene-d8 (S)%106 70-130 06/04/17 06:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014181LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.150 100 80-125
1,1,1-Trichloroethane ug/L 48.850 98 71-129
1,1,2,2-Tetrachloroethane ug/L 57.050 114 79-124
1,1,2-Trichloroethane ug/L 51.150 102 85-125
1,1-Dichloroethane ug/L 49.950 100 73-126
1,1-Dichloroethene ug/L 44.750 89 66-135
1,1-Dichloropropene ug/L 49.950 100 74-135
1,2,3-Trichloropropane ug/L 47.350 95 75-130
1,2,4-Trichlorobenzene ug/L 48.050 96 75-134
1,2-Dibromo-3-chloropropane ug/L 48.750 97 71-133
1,2-Dibromoethane (EDB)ug/L 56.350 113 83-124
1,2-Dichlorobenzene ug/L 50.950 102 80-133
1,2-Dichloroethane ug/L 45.750 91 67-128
1,2-Dichloropropane ug/L 54.450 109 75-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 102 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014181LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 48.350 97 77-130
1,3-Dichloropropane ug/L 54.650 109 76-131
1,4-Dichlorobenzene ug/L 47.750 95 78-130
2,2-Dichloropropane ug/L 44.650 89 40-160
2-Butanone (MEK)ug/L 136100 136 61-144
2-Hexanone ug/L 110100 110 68-143
4-Methyl-2-pentanone (MIBK)ug/L 109100 109 72-135
Acetone ug/L 116100 116 48-146
Acetonitrile ug/L 541500 108 62-150
Acrolein ug/L 336250 134 24-160
Acrylonitrile ug/L 274250 110 40-160
Allyl chloride ug/L 47.150 94 66-137
Benzene ug/L 52.550 105 80-125
Bromochloromethane ug/L 47.850 96 71-125
Bromodichloromethane ug/L 49.350 99 78-124
Bromoform ug/L 48.150 96 71-128
Bromomethane ug/L 41.950 84 40-160
Carbon disulfide ug/L 50.8J50 102 50-160
Carbon tetrachloride ug/L 44.550 89 69-131
Chlorobenzene ug/L 51.450 103 81-122
Chloroethane ug/L 43.750 87 39-148
Chloroform ug/L 48.350 97 73-127
Chloromethane ug/L 53.850 108 44-146
Chloroprene ug/L 47.050 94 75-145
cis-1,2-Dichloroethene ug/L 51.050 102 74-124
cis-1,3-Dichloropropene ug/L 53.850 108 72-132
Dibromochloromethane ug/L 47.750 95 78-125
Dibromomethane ug/L 48.550 97 82-120
Dichlorodifluoromethane ug/L 41.350 83 34-157
Ethyl methacrylate ug/L 46.650 93 82-121
Ethylbenzene ug/L 50.350 101 79-121
Hexachloro-1,3-butadiene ug/L 41.650 83 72-131
Iodomethane ug/L 95.3100 95 39-154
Isobutanol ug/L 12001000 120 34-160
Methacrylonitrile ug/L 566500 113 74-134
Methyl methacrylate ug/L 50.850 102 84-124
Methylene Chloride ug/L 49.950 100 64-133
Naphthalene ug/L 52.950 106 73-133
Propionitrile ug/L 623500 125 73-140
Styrene ug/L 49.750 99 84-126
Tetrachloroethene ug/L 45.950 92 78-122
Toluene ug/L 49.650 99 80-121
trans-1,2-Dichloroethene ug/L 51.450 103 71-127
trans-1,3-Dichloropropene ug/L 53.350 107 69-141
trans-1,4-Dichloro-2-butene ug/L 94.0J L15018840-160
Trichloroethene ug/L 50.650 101 78-122
Trichlorofluoromethane ug/L 45.050 90 53-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 103 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014181LABORATORY CONTROL SAMPLE:
LCSSpike
Vinyl acetate ug/L 96.4100 96 40-160
Vinyl chloride ug/L 45.150 90 58-137
Xylene (Total)ug/L 141150 94 81-126
1,2-Dichloroethane-d4 (S)%90 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2014183MATRIX SPIKE SAMPLE:
MSSpike
Result
92342730006
1,1,1,2-Tetrachloroethane ug/L 19.120 96 70-130ND
1,1,1-Trichloroethane ug/L 22.520 112 70-130ND
1,1,2,2-Tetrachloroethane ug/L 22.020 110 70-130ND
1,1,2-Trichloroethane ug/L 20.120 100 70-130ND
1,1-Dichloroethane ug/L 22.320 112 70-130ND
1,1-Dichloroethene ug/L 23.020 115 70-166ND
1,1-Dichloropropene ug/L 24.220 121 70-130ND
1,2,3-Trichloropropane ug/L 18.120 90 70-130ND
1,2,4-Trichlorobenzene ug/L 19.220 96 70-130ND
1,2-Dibromo-3-chloropropane ug/L 18.920 94 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.120 106 70-130ND
1,2-Dichlorobenzene ug/L 21.220 106 70-130ND
1,2-Dichloroethane ug/L 20.320 101 70-130ND
1,2-Dichloropropane ug/L 22.920 115 70-130ND
1,3-Dichlorobenzene ug/L 20.020 100 70-130ND
1,3-Dichloropropane ug/L 20.620 103 70-130ND
1,4-Dichlorobenzene ug/L 20.220 101 70-130ND
2,2-Dichloropropane ug/L 22.220 111 70-130ND
2-Butanone (MEK)ug/L 46.6J40 116 70-130ND
2-Hexanone ug/L 44.9J40 112 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 42.0J40 105 70-130ND
Acetone ug/L 49.1J40 94 70-13011.6J
Acetonitrile ug/L 232200 116 70-130ND
Acrolein ug/L 128100 128 70-130ND
Acrylonitrile ug/L 113J100 113 70-130ND
Allyl chloride ug/L 23.220 116 70-130ND
Benzene ug/L 23.220 116 70-148ND
Bromochloromethane ug/L 20.920 105 70-130ND
Bromodichloromethane ug/L 21.320 106 70-130ND
Bromoform ug/L 17.320 86 70-130ND
Bromomethane ug/L 22.420 112 70-130ND
Carbon disulfide ug/L 23.6J20 118 70-130ND
Carbon tetrachloride ug/L 21.020 105 70-130ND
Chlorobenzene ug/L 22.020 110 70-146ND
Chloroethane ug/L 20.920 104 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 104 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2014183MATRIX SPIKE SAMPLE:
MSSpike
Result
92342730006
Chloroform ug/L 22.820 114 70-130ND
Chloromethane ug/L 24.620 123 70-130ND
Chloroprene ug/L 21.820 109 70-130ND
cis-1,2-Dichloroethene ug/L 22.820 114 70-130ND
cis-1,3-Dichloropropene ug/L 22.420 112 70-130ND
Dibromochloromethane ug/L 19.520 98 70-130ND
Dibromomethane ug/L 21.820 109 70-130ND
Dichlorodifluoromethane ug/L 18.220 91 70-130ND
Ethyl methacrylate ug/L 20.420 102 70-130ND
Ethylbenzene ug/L 22.320 112 70-130ND
Hexachloro-1,3-butadiene ug/L 20.520 103 70-130ND
Iodomethane ug/L 41.240 103 70-130ND
Isobutanol ug/L 463400 116 70-130ND
Methacrylonitrile ug/L 217200 108 70-130ND
Methyl methacrylate ug/L 19.4J20 97 70-130ND
Methylene Chloride ug/L 21.820 109 70-130ND
Naphthalene ug/L 22.620 113 70-130ND
Propionitrile ug/L 228200 114 70-130ND
Styrene ug/L 20.920 104 70-130ND
Tetrachloroethene ug/L 20.820 104 70-130ND
Toluene ug/L 22.520 113 70-155ND
trans-1,2-Dichloroethene ug/L 23.920 119 70-130ND
trans-1,3-Dichloropropene ug/L 22.720 114 70-130ND
trans-1,4-Dichloro-2-butene ug/L 28.2J M02014170-130ND
Trichloroethene ug/L 22.520 112 69-151ND
Trichlorofluoromethane ug/L 21.720 109 70-130ND
Vinyl acetate ug/L 40.5J40 101 70-130ND
Vinyl chloride ug/L 21.220 106 70-130ND
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%104 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342730005
2014182SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 105 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342730005
2014182SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L 13.6J 30ND
Acetonitrile ug/L ND 30ND
Acrolein ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Allyl chloride ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L 0.16J 300.13J
Chloroprene ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Ethyl methacrylate ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Isobutanol ug/L ND 30ND
Methacrylonitrile ug/L ND 30ND
Methyl methacrylate ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
Propionitrile ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 106 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342730005
2014182SAMPLE DUPLICATE:
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%87 692
4-Bromofluorobenzene (S)%100 2102
Toluene-d8 (S)%108 1109
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 107 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363328
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92342478004, 92342478005, 92342478006, 92342478007, 92342478008, 92342478009, 92342478010,
92342478011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014255
Associated Lab Samples:92342478004, 92342478005, 92342478006, 92342478007, 92342478008, 92342478009, 92342478010,
92342478011
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/04/17 20:010.33
1,1,1-Trichloroethane ug/L ND 1.0 06/04/17 20:010.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 06/04/17 20:010.40
1,1,2-Trichloroethane ug/L ND 1.0 06/04/17 20:010.29
1,1-Dichloroethane ug/L ND 5.0 06/04/17 20:010.32
1,1-Dichloroethene ug/L ND 5.0 06/04/17 20:010.56
1,1-Dichloropropene ug/L ND 5.0 06/04/17 20:010.49
1,2,3-Trichloropropane ug/L ND 1.0 06/04/17 20:010.41
1,2,4-Trichlorobenzene ug/L ND 10.0 06/04/17 20:010.35
1,2-Dibromo-3-chloropropane ug/L ND 13.0 06/04/17 20:012.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/04/17 20:010.27
1,2-Dichlorobenzene ug/L ND 5.0 06/04/17 20:010.30
1,2-Dichloroethane ug/L ND 1.0 06/04/17 20:010.24
1,2-Dichloropropane ug/L ND 1.0 06/04/17 20:010.27
1,3-Dichlorobenzene ug/L ND 5.0 06/04/17 20:010.24
1,3-Dichloropropane ug/L ND 1.0 06/04/17 20:010.28
1,4-Dichlorobenzene ug/L ND 1.0 06/04/17 20:010.33
2,2-Dichloropropane ug/L ND 15.0 06/04/17 20:010.13
2-Butanone (MEK)ug/L ND 100 06/04/17 20:010.96
2-Hexanone ug/L ND 50.0 06/04/17 20:010.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 06/04/17 20:010.33
Acetone ug/L ND 100 06/04/17 20:0110.0
Acetonitrile ug/L ND 55.0 06/04/17 20:012.2
Acrolein ug/L ND 53.0 06/04/17 20:011.6
Acrylonitrile ug/L ND 200 06/04/17 20:011.9
Allyl chloride ug/L ND 10.0 06/04/17 20:011.5
Benzene ug/L ND 1.0 06/04/17 20:010.25
Bromochloromethane ug/L ND 3.0 06/04/17 20:010.17
Bromodichloromethane ug/L ND 1.0 06/04/17 20:010.18
Bromoform ug/L ND 3.0 06/04/17 20:010.26
Bromomethane ug/L ND 10.0 06/04/17 20:010.29
Carbon disulfide ug/L ND 100 06/04/17 20:011.2
Carbon tetrachloride ug/L ND 1.0 06/04/17 20:010.25
Chlorobenzene ug/L ND 3.0 06/04/17 20:010.23
Chloroethane ug/L ND 10.0 06/04/17 20:010.54
Chloroform ug/L ND 5.0 06/04/17 20:010.14
Chloromethane ug/L ND 1.0 06/04/17 20:010.11
Chloroprene ug/L ND 20.0 06/04/17 20:010.27
cis-1,2-Dichloroethene ug/L ND 5.0 06/04/17 20:010.19
cis-1,3-Dichloropropene ug/L ND 1.0 06/04/17 20:010.13
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 108 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014255
Associated Lab Samples:92342478004, 92342478005, 92342478006, 92342478007, 92342478008, 92342478009, 92342478010,
92342478011
Matrix:Water
AnalyzedMDL
Dibromochloromethane ug/L ND 3.0 06/04/17 20:010.21
Dibromomethane ug/L ND 10.0 06/04/17 20:010.21
Dichlorodifluoromethane ug/L ND 5.0 06/04/17 20:010.21
Ethyl methacrylate ug/L ND 10.0 06/04/17 20:010.20
Ethylbenzene ug/L ND 1.0 06/04/17 20:010.30
Hexachloro-1,3-butadiene ug/L ND 10.0 06/04/17 20:010.71
Iodomethane ug/L ND 10.0 06/04/17 20:010.32
Isobutanol ug/L ND 100 06/04/17 20:0135.0
Methacrylonitrile ug/L ND 100 06/04/17 20:010.93
Methyl methacrylate ug/L ND 30.0 06/04/17 20:012.0
Methylene Chloride ug/L ND 1.0 06/04/17 20:010.97
Naphthalene ug/L ND 10.0 06/04/17 20:010.24
Propionitrile ug/L ND 150 06/04/17 20:013.6
Styrene ug/L ND 1.0 06/04/17 20:010.26
Tetrachloroethene ug/L ND 1.0 06/04/17 20:010.46
Toluene ug/L ND 1.0 06/04/17 20:010.26
trans-1,2-Dichloroethene ug/L ND 5.0 06/04/17 20:010.49
trans-1,3-Dichloropropene ug/L ND 1.0 06/04/17 20:010.26
trans-1,4-Dichloro-2-butene ug/L ND 100 06/04/17 20:011.0
Trichloroethene ug/L ND 1.0 06/04/17 20:010.47
Trichlorofluoromethane ug/L ND 1.0 06/04/17 20:010.20
Vinyl acetate ug/L ND 50.0 06/04/17 20:010.35
Vinyl chloride ug/L ND 1.0 06/04/17 20:010.62
Xylene (Total)ug/L ND 5.0 06/04/17 20:010.66
1,2-Dichloroethane-d4 (S)%85 70-130 06/04/17 20:01
4-Bromofluorobenzene (S)%100 70-130 06/04/17 20:01
Toluene-d8 (S)%115 70-130 06/04/17 20:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014256LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 46.650 93 80-125
1,1,1-Trichloroethane ug/L 50.750 101 71-129
1,1,2,2-Tetrachloroethane ug/L 49.850 100 79-124
1,1,2-Trichloroethane ug/L 48.950 98 85-125
1,1-Dichloroethane ug/L 49.650 99 73-126
1,1-Dichloroethene ug/L 46.950 94 66-135
1,1-Dichloropropene ug/L 51.950 104 74-135
1,2,3-Trichloropropane ug/L 46.550 93 75-130
1,2,4-Trichlorobenzene ug/L 46.550 93 75-134
1,2-Dibromo-3-chloropropane ug/L 46.750 93 71-133
1,2-Dibromoethane (EDB)ug/L 54.550 109 83-124
1,2-Dichlorobenzene ug/L 47.550 95 80-133
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 109 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014256LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloroethane ug/L 47.050 94 67-128
1,2-Dichloropropane ug/L 53.450 107 75-132
1,3-Dichlorobenzene ug/L 48.150 96 77-130
1,3-Dichloropropane ug/L 54.150 108 76-131
1,4-Dichlorobenzene ug/L 47.950 96 78-130
2,2-Dichloropropane ug/L 50.750 101 40-160
2-Butanone (MEK)ug/L 126100 126 61-144
2-Hexanone ug/L 101100 101 68-143
4-Methyl-2-pentanone (MIBK)ug/L 94.9J100 95 72-135
Acetone ug/L 115100 115 48-146
Acetonitrile ug/L 525500 105 62-150
Acrolein ug/L 320250 128 24-160
Acrylonitrile ug/L 268250 107 40-160
Allyl chloride ug/L 47.650 95 66-137
Benzene ug/L 52.150 104 80-125
Bromochloromethane ug/L 48.950 98 71-125
Bromodichloromethane ug/L 48.550 97 78-124
Bromoform ug/L 43.150 86 71-128
Bromomethane ug/L 42.150 84 40-160
Carbon disulfide ug/L 49.3J50 99 50-160
Carbon tetrachloride ug/L 45.150 90 69-131
Chlorobenzene ug/L 48.850 98 81-122
Chloroethane ug/L 40.850 82 39-148
Chloroform ug/L 50.950 102 73-127
Chloromethane ug/L 49.950 100 44-146
Chloroprene ug/L 49.350 99 75-145
cis-1,2-Dichloroethene ug/L 52.550 105 74-124
cis-1,3-Dichloropropene ug/L 54.150 108 72-132
Dibromochloromethane ug/L 47.550 95 78-125
Dibromomethane ug/L 44.250 88 82-120
Dichlorodifluoromethane ug/L 41.150 82 34-157
Ethyl methacrylate ug/L 45.750 91 82-121
Ethylbenzene ug/L 50.150 100 79-121
Hexachloro-1,3-butadiene ug/L 43.550 87 72-131
Iodomethane ug/L 91.7100 92 39-154
Isobutanol ug/L 11301000 113 34-160
Methacrylonitrile ug/L 563500 113 74-134
Methyl methacrylate ug/L 43.550 87 84-124
Methylene Chloride ug/L 53.650 107 64-133
Naphthalene ug/L 48.650 97 73-133
Propionitrile ug/L 562500 112 73-140
Styrene ug/L 51.050 102 84-126
Tetrachloroethene ug/L 44.850 90 78-122
Toluene ug/L 46.450 93 80-121
trans-1,2-Dichloroethene ug/L 52.350 105 71-127
trans-1,3-Dichloropropene ug/L 52.450 105 69-141
trans-1,4-Dichloro-2-butene ug/L 68.3J50 137 40-160
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 110 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014256LABORATORY CONTROL SAMPLE:
LCSSpike
Trichloroethene ug/L 50.450 101 78-122
Trichlorofluoromethane ug/L 45.450 91 53-137
Vinyl acetate ug/L 99.2100 99 40-160
Vinyl chloride ug/L 41.950 84 58-137
Xylene (Total)ug/L 149150 99 81-126
1,2-Dichloroethane-d4 (S)%103 70-130
4-Bromofluorobenzene (S)%107 70-130
Toluene-d8 (S)%96 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2014258MATRIX SPIKE SAMPLE:
MSSpike
Result
92342478011
1,1,1,2-Tetrachloroethane ug/L 20.020 100 70-130ND
1,1,1-Trichloroethane ug/L 23.020 115 70-130ND
1,1,2,2-Tetrachloroethane ug/L 22.120 110 70-130ND
1,1,2-Trichloroethane ug/L 22.220 111 70-130ND
1,1-Dichloroethane ug/L 23.120 116 70-130ND
1,1-Dichloroethene ug/L 23.020 115 70-166ND
1,1-Dichloropropene ug/L 23.320 116 70-130ND
1,2,3-Trichloropropane ug/L 19.520 98 70-130ND
1,2,4-Trichlorobenzene ug/L 19.320 97 70-130ND
1,2-Dibromo-3-chloropropane ug/L 18.220 91 70-130ND
1,2-Dibromoethane (EDB)ug/L 19.720 99 70-130ND
1,2-Dichlorobenzene ug/L 20.920 105 70-130ND
1,2-Dichloroethane ug/L 21.320 106 70-130ND
1,2-Dichloropropane ug/L 24.120 120 70-130ND
1,3-Dichlorobenzene ug/L 21.720 108 70-130ND
1,3-Dichloropropane ug/L 20.420 102 70-130ND
1,4-Dichlorobenzene ug/L 21.120 105 70-130ND
2,2-Dichloropropane ug/L 21.220 106 70-130ND
2-Butanone (MEK)ug/L 47.7J40 119 70-130ND
2-Hexanone ug/L 40.9J40 102 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 43.2J40 108 70-130ND
Acetone ug/L 93.5J M14019870-13014.4J
Acetonitrile ug/L 219200 110 70-130ND
Acrolein ug/L 117100 117 70-130ND
Acrylonitrile ug/L 114J100 114 70-130ND
Allyl chloride ug/L 26.8 M12013470-130ND
Benzene ug/L 23.420 117 70-148ND
Bromochloromethane ug/L 21.420 107 70-130ND
Bromodichloromethane ug/L 22.420 112 70-130ND
Bromoform ug/L 16.520 83 70-130ND
Bromomethane ug/L 19.820 99 70-130ND
Carbon disulfide ug/L 23.4J20 117 70-130ND
Carbon tetrachloride ug/L 22.420 112 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 111 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2014258MATRIX SPIKE SAMPLE:
MSSpike
Result
92342478011
Chlorobenzene ug/L 22.120 110 70-146ND
Chloroethane ug/L 21.720 108 70-130ND
Chloroform ug/L 23.220 116 70-130ND
Chloromethane ug/L 25.820 129 70-130ND
Chloroprene ug/L 22.820 114 70-130ND
cis-1,2-Dichloroethene ug/L 24.520 119 70-1300.64J
cis-1,3-Dichloropropene ug/L 23.420 117 70-130ND
Dibromochloromethane ug/L 18.420 92 70-130ND
Dibromomethane ug/L 21.720 108 70-130ND
Dichlorodifluoromethane ug/L 19.220 96 70-130ND
Ethyl methacrylate ug/L 19.420 97 70-130ND
Ethylbenzene ug/L 23.020 115 70-130ND
Hexachloro-1,3-butadiene ug/L 19.320 96 70-130ND
Iodomethane ug/L 41.640 104 70-130ND
Isobutanol ug/L 419400 105 70-130ND
Methacrylonitrile ug/L 230200 115 70-130ND
Methyl methacrylate ug/L 19.7J20 98 70-130ND
Methylene Chloride ug/L 23.220 116 70-130ND
Naphthalene ug/L 21.620 108 70-130ND
Propionitrile ug/L 243200 121 70-130ND
Styrene ug/L 22.320 112 70-130ND
Tetrachloroethene ug/L 19.420 97 70-130ND
Toluene ug/L 22.720 113 70-155ND
trans-1,2-Dichloroethene ug/L 25.020 125 70-130ND
trans-1,3-Dichloropropene ug/L 21.820 109 70-130ND
trans-1,4-Dichloro-2-butene ug/L 21.3J20 106 70-130ND
Trichloroethene ug/L 23.820 119 69-151ND
Trichlorofluoromethane ug/L 22.120 111 70-130ND
Vinyl acetate ug/L 37.6J40 94 70-130ND
Vinyl chloride ug/L 21.820 109 70-130ND
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%109 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342478010
2014257SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 0.50J 300.36J
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 112 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342478010
2014257SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acetonitrile ug/L ND 30ND
Acrolein ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Allyl chloride ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L 0.29J 30ND
Chloroprene ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 0.88J 300.65J
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Ethyl methacrylate ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Isobutanol ug/L ND 30ND
Methacrylonitrile ug/L ND 30ND
Methyl methacrylate ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
Propionitrile ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 113 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342478010
2014257SAMPLE DUPLICATE:
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%92 092
4-Bromofluorobenzene (S)%105 2103
Toluene-d8 (S)%108 2109
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 114 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363163
EPA 3510
EPA 8081
8081A GCS Pesticides
Associated Lab Samples:92342478003, 92342530001, 92342530002, 92342530003, 92342530004, 92342530005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2013349
Associated Lab Samples:92342478003, 92342530001, 92342530002, 92342530003, 92342530004, 92342530005
Matrix:Water
AnalyzedMDL
4,4'-DDD ug/L ND 0.10 06/06/17 20:060.050
4,4'-DDE ug/L ND 0.10 06/06/17 20:060.050
4,4'-DDT ug/L ND 0.10 06/06/17 20:060.050
Aldrin ug/L ND 0.050 06/06/17 20:060.050
alpha-BHC ug/L ND 0.050 06/06/17 20:060.050
beta-BHC ug/L ND 0.050 06/06/17 20:060.050
Chlordane (Technical)ug/L ND 0.50 06/06/17 20:060.20
delta-BHC ug/L ND 0.050 06/06/17 20:060.050
Dieldrin ug/L ND 0.075 06/06/17 20:060.050
Endosulfan I ug/L ND 0.10 06/06/17 20:060.050
Endosulfan II ug/L ND 0.10 06/06/17 20:060.050
Endosulfan sulfate ug/L ND 0.10 06/06/17 20:060.050
Endrin ug/L ND 0.10 06/06/17 20:060.050
Endrin aldehyde ug/L ND 0.10 06/06/17 20:060.050
gamma-BHC (Lindane)ug/L ND 0.050 06/06/17 20:060.050
Heptachlor ug/L ND 0.050 06/06/17 20:060.050
Heptachlor epoxide ug/L ND 0.075 06/06/17 20:060.050
Methoxychlor ug/L ND 1.0 06/06/17 20:060.15
Toxaphene ug/L ND 1.5 06/06/17 20:060.20
Decachlorobiphenyl (S)%95 20-130 06/06/17 20:06
Tetrachloro-m-xylene (S)%80 20-130 06/06/17 20:06
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2013350LABORATORY CONTROL SAMPLE:
LCSSpike
4,4'-DDD ug/L 0.24.25 98 20-150
4,4'-DDE ug/L 0.22.25 89 20-150
4,4'-DDT ug/L 0.26.25 105 20-150
Aldrin ug/L 0.18.25 73 20-150
alpha-BHC ug/L 0.20.25 79 20-150
beta-BHC ug/L 0.19.25 78 20-150
delta-BHC ug/L 0.23.25 92 20-150
Dieldrin ug/L 0.23.25 91 20-150
Endosulfan I ug/L 0.23.25 92 20-150
Endosulfan II ug/L 0.24.25 99 20-150
Endosulfan sulfate ug/L 0.26.25 105 20-150
Endrin ug/L 0.25.25 100 20-150
Endrin aldehyde ug/L 0.23.25 94 20-150
gamma-BHC (Lindane)ug/L 0.22.25 88 20-150
Heptachlor ug/L 0.18.25 75 20-150
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 115 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2013350LABORATORY CONTROL SAMPLE:
LCSSpike
Heptachlor epoxide ug/L 0.21.25 83 20-150
Methoxychlor ug/L 0.76J.74 102 20-150
Decachlorobiphenyl (S)%86 20-130
Tetrachloro-m-xylene (S)%54 20-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2013351MATRIX SPIKE SAMPLE:
MSSpike
Result
92342479004
4,4'-DDD ug/L 0.22.25 89 20-150ND
4,4'-DDE ug/L 0.21.25 84 20-150ND
4,4'-DDT ug/L 0.24.25 98 20-150ND
Aldrin ug/L 0.18.25 71 20-150ND
alpha-BHC ug/L 0.19.25 77 20-150ND
beta-BHC ug/L 0.17.25 69 20-150ND
delta-BHC ug/L 0.21.25 84 20-150ND
Dieldrin ug/L 0.21.25 84 20-150ND
Endosulfan I ug/L 0.21.25 87 20-150ND
Endosulfan II ug/L 0.23.25 91 20-150ND
Endosulfan sulfate ug/L 0.25.25 99 20-150ND
Endrin ug/L 0.23.25 93 20-150ND
Endrin aldehyde ug/L 0.23.25 95 20-150ND
gamma-BHC (Lindane)ug/L 0.20.25 81 20-150ND
Heptachlor ug/L 0.18.25 74 20-150ND
Heptachlor epoxide ug/L 0.20.25 83 20-150ND
Methoxychlor ug/L 0.70J.74 94 20-150ND
Decachlorobiphenyl (S)%47 20-130
Tetrachloro-m-xylene (S)%76 20-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342479005
2013352SAMPLE DUPLICATE:
4,4'-DDD ug/L ND 30ND
4,4'-DDE ug/L ND 30ND
4,4'-DDT ug/L ND 30ND
Aldrin ug/L ND 30ND
alpha-BHC ug/L ND 30ND
beta-BHC ug/L ND 30ND
Chlordane (Technical)ug/L ND 30ND
delta-BHC ug/L ND 30ND
Dieldrin ug/L ND 30ND
Endosulfan I ug/L ND 30ND
Endosulfan II ug/L ND 30ND
Endosulfan sulfate ug/L ND 30ND
Endrin ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 116 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342479005
2013352SAMPLE DUPLICATE:
Endrin aldehyde ug/L ND 30ND
gamma-BHC (Lindane)ug/L ND 30ND
Heptachlor ug/L ND 30ND
Heptachlor epoxide ug/L ND 30ND
Methoxychlor ug/L ND 30ND
Toxaphene ug/L ND 30ND
Decachlorobiphenyl (S)%68 2184
Tetrachloro-m-xylene (S)%87 15101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 117 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363426
EPA 3510
EPA 8081
8081A GCS Pesticides
Associated Lab Samples:92342478004, 92342478005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014786
Associated Lab Samples:92342478004, 92342478005
Matrix:Water
AnalyzedMDL
4,4'-DDD ug/L ND 0.10 06/06/17 13:280.050
4,4'-DDE ug/L ND 0.10 06/06/17 13:280.050
4,4'-DDT ug/L ND 0.10 06/06/17 13:280.050
Aldrin ug/L ND 0.050 06/06/17 13:280.050
alpha-BHC ug/L ND 0.050 06/06/17 13:280.050
beta-BHC ug/L ND 0.050 06/06/17 13:280.050
Chlordane (Technical)ug/L ND 0.50 06/06/17 13:280.20
delta-BHC ug/L ND 0.050 06/06/17 13:280.050
Dieldrin ug/L ND 0.075 06/06/17 13:280.050
Endosulfan I ug/L ND 0.10 06/06/17 13:280.050
Endosulfan II ug/L ND 0.10 06/06/17 13:280.050
Endosulfan sulfate ug/L ND 0.10 06/06/17 13:280.050
Endrin ug/L ND 0.10 06/06/17 13:280.050
Endrin aldehyde ug/L ND 0.10 06/06/17 13:280.050
gamma-BHC (Lindane)ug/L ND 0.050 06/06/17 13:280.050
Heptachlor ug/L ND 0.050 06/06/17 13:280.050
Heptachlor epoxide ug/L ND 0.075 06/06/17 13:280.050
Methoxychlor ug/L ND 1.0 06/06/17 13:280.15
Toxaphene ug/L ND 1.5 06/06/17 13:280.20
Decachlorobiphenyl (S)%78 20-130 06/06/17 13:28
Tetrachloro-m-xylene (S)%51 20-130 06/06/17 13:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014787LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2014788
4,4'-DDD ug/L 0.22.25 90 20-150920.23 2 30
4,4'-DDE ug/L 0.21.25 84 20-150790.20 7 30
4,4'-DDT ug/L 0.23.25 94 20-150950.24 1 30
Aldrin ug/L 0.16.25 64 20-150600.15 8 30
alpha-BHC ug/L 0.19.25 79 20-150780.19 1 30
beta-BHC ug/L 0.17.25 70 20-150750.19 7 30
delta-BHC ug/L 0.21.25 84 20-150790.20 7 30
Dieldrin ug/L 0.21.25 86 20-150830.21 3 30
Endosulfan I ug/L 0.22.25 87 20-150840.21 3 30
Endosulfan II ug/L 0.23.25 91 20-150900.22 1 30
Endosulfan sulfate ug/L 0.24.25 97 20-150970.24 0 30
Endrin ug/L 0.23.25 93 20-150930.23 0 30
Endrin aldehyde ug/L 0.21.25 87 20-150890.22 3 30
gamma-BHC (Lindane)ug/L 0.21.25 83 20-150850.21 2 30
Heptachlor ug/L 0.17.25 68 20-150620.15 9 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 118 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014787LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2014788
Heptachlor epoxide ug/L 0.20.25 82 20-150700.17 16 30
Methoxychlor ug/L 0.72J.74 97 20-150970.72J 1 30
Decachlorobiphenyl (S)%78 20-13064
Tetrachloro-m-xylene (S)%81 20-13069
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 119 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363162
EPA 3510
EPA 8082
8082 GCS PCB
Associated Lab Samples:92342478003, 92342530001, 92342530002, 92342530003, 92342530004, 92342530005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2013345
Associated Lab Samples:92342478003, 92342530001, 92342530002, 92342530003, 92342530004, 92342530005
Matrix:Water
AnalyzedMDL
PCB-1016 (Aroclor 1016)ug/L ND 0.50 06/03/17 13:250.50
PCB-1221 (Aroclor 1221)ug/L ND 0.50 06/03/17 13:250.50
PCB-1232 (Aroclor 1232)ug/L ND 0.50 06/03/17 13:250.50
PCB-1242 (Aroclor 1242)ug/L ND 0.50 06/03/17 13:250.50
PCB-1248 (Aroclor 1248)ug/L ND 0.50 06/03/17 13:250.50
PCB-1254 (Aroclor 1254)ug/L ND 0.50 06/03/17 13:250.50
PCB-1260 (Aroclor 1260)ug/L ND 0.50 06/03/17 13:250.50
Decachlorobiphenyl (S)%93 10-132 06/03/17 13:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2013346LABORATORY CONTROL SAMPLE:
LCSSpike
PCB-1016 (Aroclor 1016)ug/L 1.92.5 76 50-150
PCB-1260 (Aroclor 1260)ug/L 2.32.5 91 50-150
Decachlorobiphenyl (S)%64 10-132
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2013347MATRIX SPIKE SAMPLE:
MSSpike
Result
92342530001
PCB-1016 (Aroclor 1016)ug/L 1.52.5 61 50-150ND
PCB-1260 (Aroclor 1260)ug/L 1.42.5 55 50-150ND
Decachlorobiphenyl (S)%32 10-132
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342530003
2013348SAMPLE DUPLICATE:
PCB-1016 (Aroclor 1016)ug/L ND 30ND
PCB-1221 (Aroclor 1221)ug/L ND 30ND
PCB-1232 (Aroclor 1232)ug/L ND 30ND
PCB-1242 (Aroclor 1242)ug/L ND 30ND
PCB-1248 (Aroclor 1248)ug/L ND 30ND
PCB-1254 (Aroclor 1254)ug/L ND 30ND
PCB-1260 (Aroclor 1260)ug/L ND 30ND
Decachlorobiphenyl (S)%59 2777
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 120 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363427
EPA 3510
EPA 8082
8082 GCS PCB
Associated Lab Samples:92342478004, 92342478005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014798
Associated Lab Samples:92342478004, 92342478005
Matrix:Water
AnalyzedMDL
PCB-1016 (Aroclor 1016)ug/L ND 0.50 06/06/17 20:100.50
PCB-1221 (Aroclor 1221)ug/L ND 0.50 06/06/17 20:100.50
PCB-1232 (Aroclor 1232)ug/L ND 0.50 06/06/17 20:100.50
PCB-1242 (Aroclor 1242)ug/L ND 0.50 06/06/17 20:100.50
PCB-1248 (Aroclor 1248)ug/L ND 0.50 06/06/17 20:100.50
PCB-1254 (Aroclor 1254)ug/L ND 0.50 06/06/17 20:100.50
PCB-1260 (Aroclor 1260)ug/L ND 0.50 06/06/17 20:100.50
Decachlorobiphenyl (S)%75 10-132 06/06/17 20:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014799LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2014800
PCB-1016 (Aroclor 1016)ug/L 3.35 66 50-150693.5 5 30
PCB-1260 (Aroclor 1260)ug/L 3.25 63 50-150603.0 5 30
Decachlorobiphenyl (S)%34 10-13237
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 121 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
372315
EPA 8151
EPA 8151
8151A GCS Herbicides
Associated Lab Samples:92342478003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2012657
Associated Lab Samples:92342478003
Matrix:Water
AnalyzedMDL
2,4,5-T ug/L ND 0.19 06/06/17 01:190.042
2,4,5-TP (Silvex)ug/L ND 0.19 06/06/17 01:190.049
2,4-D ug/L ND 0.94 06/06/17 01:190.22
Dinoseb ug/L ND 0.19 06/06/17 01:190.057
Pentachlorophenol ug/L ND 0.028 06/06/17 01:190.017
2,4-DCAA (S)%94 39-139 06/06/17 01:19
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012658LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2013105
2,4,5-T ug/L 1.21.2 100 37-133971.2 3 40
2,4,5-TP (Silvex)ug/L 1.11.2 92 53-134971.2 5 40
2,4-D ug/L 5.56 91 35-124955.7 5 40
Dinoseb ug/L 0.891.2 74 13-116831.0 12 40
Pentachlorophenol ug/L 0.22.18 122 39-1701240.22 2 40
2,4-DCAA (S)%83 39-13985 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 122 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
373221
EPA 8151
EPA 8151
8151A GCS Herbicides
Associated Lab Samples:92342478004, 92342478005, 92342530001, 92342530002, 92342530003, 92342530004, 92342530005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2017562
Associated Lab Samples:92342478004, 92342478005, 92342530001, 92342530002, 92342530003, 92342530004, 92342530005
Matrix:Water
AnalyzedMDL
2,4,5-T ug/L ND 0.19 06/09/17 20:420.042
2,4,5-TP (Silvex)ug/L ND 0.19 06/09/17 20:420.049
2,4-D ug/L ND 0.94 06/09/17 20:420.22
Dinoseb ug/L ND 0.19 06/09/17 20:420.057
Pentachlorophenol ug/L ND 0.028 06/09/17 20:420.017
2,4-DCAA (S)%74 39-139 06/09/17 20:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2017563LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-T ug/L 1.31.2 109 37-133
2,4,5-TP (Silvex)ug/L 1.31.2 110 53-134
2,4-D ug/L 5.56 91 35-124
Dinoseb ug/L 1.21.2 99 13-116
Pentachlorophenol ug/L 0.17.18 94 39-170
2,4-DCAA (S)%85 39-139
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2018719MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35316294004
2018720
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,4,5-T ug/L 1.2 100 37-13390 3 401.40.043U 1.2 1.2
2,4,5-TP (Silvex)ug/L 1.2 97 53-13488 2 401.40.050U 1.2 1.2
2,4-D ug/L 6 84 35-12476 3 406.80.23U 5.1 5.2
Dinoseb ug/L 1.2 91 13-11672 11 401.40.058U 1.1 0.98
Pentachlorophenol ug/L M1,R1.18 82 39-17028 89 40.20.017U 0.15 0.057
2,4-DCAA (S)%69 39-13985 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 123 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363842
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92342478003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2017031
Associated Lab Samples:92342478003
Matrix:Water
AnalyzedMDL
1,2,4,5-Tetrachlorobenzene ug/L ND 10.0 06/13/17 11:371.3
1,3,5-Trinitrobenzene ug/L ND 10.0 06/13/17 11:371.2
1,3-Dinitrobenzene ug/L ND 20.0 06/13/17 11:371.3
1,4-Naphthoquinone ug/L ND 10.0 06/13/17 11:370.99
1-Naphthalenamine ug/L ND 10.0 06/13/17 11:371.3
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 06/13/17 11:371.8
2,3,4,6-Tetrachlorophenol ug/L ND 10.0 06/13/17 11:372.9
2,4,5-Trichlorophenol ug/L ND 10.0 06/13/17 11:371.5
2,4,6-Trichlorophenol ug/L ND 10.0 06/13/17 11:371.4
2,4-Dichlorophenol ug/L ND 10.0 06/13/17 11:371.6
2,4-Dimethylphenol ug/L ND 10.0 06/13/17 11:371.6
2,4-Dinitrophenol ug/L ND 50.0 06/13/17 11:375.1
2,4-Dinitrotoluene ug/L ND 10.0 06/13/17 11:371.5
2,6-Dichlorophenol ug/L ND 10.0 06/13/17 11:371.5
2,6-Dinitrotoluene ug/L ND 10.0 06/13/17 11:371.4
2-Acetylaminofluorene ug/L ND 20.0 06/13/17 11:371.6
2-Chloronaphthalene ug/L ND 10.0 06/13/17 11:371.6
2-Chlorophenol ug/L ND 10.0 06/13/17 11:371.5
2-Methylnaphthalene ug/L ND 10.0 06/13/17 11:371.4
2-Methylphenol(o-Cresol)ug/L ND 10.0 06/13/17 11:371.6
2-Naphthalenamine ug/L ND 10.0 06/13/17 11:372.2
2-Nitroaniline ug/L ND 50.0 06/13/17 11:372.3
2-Nitrophenol ug/L ND 10.0 06/13/17 11:371.6
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 06/13/17 11:371.4
3,3'-Dichlorobenzidine ug/L ND 20.0 06/13/17 11:373.9
3,3'-Dimethylbenzidine ug/L ND 10.0 06/13/17 11:373.9
3-Methylcholanthrene ug/L ND 10.0 06/13/17 11:372.7
3-Nitroaniline ug/L ND 50.0 06/13/17 11:372.7
4,6-Dinitro-2-methylphenol ug/L ND 50.0 06/13/17 11:372.2
4-Aminobiphenyl ug/L ND 20.0 06/13/17 11:371.7
4-Bromophenylphenyl ether ug/L ND 10.0 06/13/17 11:371.5
4-Chloro-3-methylphenol ug/L ND 20.0 06/13/17 11:372.8
4-Chloroaniline ug/L ND 20.0 06/13/17 11:372.8
4-Chlorophenylphenyl ether ug/L ND 10.0 06/13/17 11:371.6
4-Nitroaniline ug/L ND 20.0 06/13/17 11:373.4
4-Nitrophenol ug/L ND 50.0 06/13/17 11:374.3
5-Nitro-o-toluidine ug/L ND 10.0 06/13/17 11:371.9
7,12-Dimethylbenz(a)anthracene ug/L ND 10.0 06/13/17 11:372.4
Acenaphthene ug/L ND 10.0 06/13/17 11:371.6
Acenaphthylene ug/L ND 10.0 06/13/17 11:371.5
Acetophenone ug/L ND 10.0 06/13/17 11:371.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 124 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2017031
Associated Lab Samples:92342478003
Matrix:Water
AnalyzedMDL
Anthracene ug/L ND 10.0 06/13/17 11:371.7
Benzo(a)anthracene ug/L ND 10.0 06/13/17 11:372.1
Benzo(a)pyrene ug/L ND 10.0 06/13/17 11:372.2
Benzo(b)fluoranthene ug/L ND 10.0 06/13/17 11:372.2
Benzo(g,h,i)perylene ug/L ND 10.0 06/13/17 11:372.1
Benzo(k)fluoranthene ug/L ND 10.0 06/13/17 11:372.0
Benzyl alcohol ug/L ND 20.0 06/13/17 11:373.1
bis(2-Chloroethoxy)methane ug/L ND 10.0 06/13/17 11:371.6
bis(2-Chloroethyl) ether ug/L ND 10.0 06/13/17 11:371.7
bis(2-Ethylhexyl)phthalate ug/L ND 15.0 06/13/17 11:372.3
Butylbenzylphthalate ug/L ND 10.0 06/13/17 11:372.5
Chlorobenzilate ug/L ND 10.0 06/13/17 11:372.2
Chrysene ug/L ND 10.0 06/13/17 11:372.1
Di-n-butylphthalate ug/L ND 10.0 06/13/17 11:372.0
Di-n-octylphthalate ug/L ND 10.0 06/13/17 11:371.5
Diallate ug/L ND 10.0 06/13/17 11:371.6
Dibenz(a,h)anthracene ug/L ND 10.0 06/13/17 11:372.0
Dibenzofuran ug/L ND 10.0 06/13/17 11:371.7
Diethylphthalate ug/L ND 6000 06/13/17 11:371.6
Dimethoate ug/L ND 20.0 06/13/17 11:371.8
Dimethylphthalate ug/L ND 10.0 06/13/17 11:371.4
Diphenylamine ug/L ND 10.0 06/13/17 11:371.4
Disulfoton ug/L ND 10.0 06/13/17 11:371.5
Ethyl methanesulfonate ug/L ND 20.0 06/13/17 11:371.6
Famphur ug/L ND 20.0 06/13/17 11:375.7
Fluoranthene ug/L ND 10.0 06/13/17 11:372.2
Fluorene ug/L ND 10.0 06/13/17 11:371.6
Hexachlorobenzene ug/L ND 10.0 06/13/17 11:371.7
Hexachlorocyclopentadiene ug/L ND 10.0 06/13/17 11:371.3
Hexachloroethane ug/L ND 10.0 06/13/17 11:371.8
Hexachloropropene ug/L ND 10.0 06/13/17 11:371.2
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 06/13/17 11:372.0
Isodrin ug/L ND 20.0 06/13/17 11:372.5
Isophorone ug/L ND 10.0 06/13/17 11:371.5
Isosafrole ug/L ND 10.0 06/13/17 11:371.5
Kepone ug/L ND 20.0 06/13/17 11:374.5
Methapyrilene ug/L ND 100 06/13/17 11:373.0
Methyl methanesulfonate ug/L ND 10.0 06/13/17 11:371.1
Methyl parathion ug/L ND 10.0 06/13/17 11:371.6
N-Nitroso-di-n-butylamine ug/L ND 10.0 06/13/17 11:371.6
N-Nitroso-di-n-propylamine ug/L ND 10.0 06/13/17 11:371.7
N-Nitrosodiethylamine ug/L ND 20.0 06/13/17 11:371.4
N-Nitrosodimethylamine ug/L ND 10.0 06/13/17 11:371.6
N-Nitrosodiphenylamine ug/L ND 10.0 06/13/17 11:371.4
N-Nitrosomethylethylamine ug/L ND 10.0 06/13/17 11:371.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 125 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2017031
Associated Lab Samples:92342478003
Matrix:Water
AnalyzedMDL
N-Nitrosopiperidine ug/L ND 20.0 06/13/17 11:371.7
N-Nitrosopyrrolidine ug/L ND 10.0 06/13/17 11:371.7
Nitrobenzene ug/L ND 10.0 06/13/17 11:371.6
O,O,O-Triethylphosphorothioate ug/L ND 10.0 06/13/17 11:371.7
O-Toluidine ug/L ND 10.0 06/13/17 11:371.7
P-Dimethylaminoazobenzene ug/L ND 10.0 06/13/17 11:371.0
p-Phenylenediamine ug/L ND 10.0 06/13/17 11:372.2
Parathion (Ethyl parathion)ug/L ND 10.0 06/13/17 11:371.5
Pentachlorobenzene ug/L ND 10.0 06/13/17 11:371.5
Pentachloronitrobenzene ug/L ND 20.0 06/13/17 11:371.7
Pentachlorophenol ug/L ND 25.0 06/13/17 11:373.5
Phenacetin ug/L ND 20.0 06/13/17 11:371.9
Phenanthrene ug/L ND 10.0 06/13/17 11:371.6
Phenol ug/L ND 10.0 06/13/17 11:371.3
Phorate ug/L ND 10.0 06/13/17 11:371.7
Pronamide ug/L ND 10.0 06/13/17 11:372.0
Pyrene ug/L ND 10.0 06/13/17 11:372.2
Safrole ug/L ND 10.0 06/13/17 11:371.3
Thionazin ug/L ND 20.0 06/13/17 11:371.7
2,4,6-Tribromophenol (S)%76 27-110 06/13/17 11:37
2-Fluorobiphenyl (S)%85 27-110 06/13/17 11:37
2-Fluorophenol (S)%41 12-110 06/13/17 11:37
Nitrobenzene-d5 (S)%69 21-110 06/13/17 11:37
Phenol-d6 (S)%27 10-110 06/13/17 11:37
Terphenyl-d14 (S)%90 31-107 06/13/17 11:37
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2017032LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4,5-Tetrachlorobenzene ug/L 11.950 24 16-129
1,3,5-Trinitrobenzene ug/L 26.1 L2505255-125
1,3-Dinitrobenzene ug/L 31.850 64 30-122
1,4-Naphthoquinone ug/L 29.250 58 31-120
1-Naphthalenamine ug/L 21.450 43 37-126
2,2'-Oxybis(1-chloropropane)ug/L 16.950 34 18-120
2,3,4,6-Tetrachlorophenol ug/L 62.950 126 54-276
2,4,5-Trichlorophenol ug/L 28.150 56 43-113
2,4,6-Trichlorophenol ug/L 28.050 56 42-120
2,4-Dichlorophenol ug/L 14.4 L2502930-120
2,4-Dimethylphenol ug/L 12.6 L2502529-111
2,4-Dinitrophenol ug/L 170250 68 19-132
2,4-Dinitrotoluene ug/L 35.550 71 58-128
2,6-Dichlorophenol ug/L 13.0 L2502654-128
2,6-Dinitrotoluene ug/L 34.850 70 54-129
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 126 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2017032LABORATORY CONTROL SAMPLE:
LCSSpike
2-Acetylaminofluorene ug/L 27.9 L2505681-160
2-Chloronaphthalene ug/L 20.7 L2504143-117
2-Chlorophenol ug/L 12.6 L2502537-120
2-Methylnaphthalene ug/L 12.5 L2502533-120
2-Methylphenol(o-Cresol)ug/L 9.8J L2502031-120
2-Naphthalenamine ug/L 26.850 54 41-136
2-Nitroaniline ug/L 68.2100 68 48-121
2-Nitrophenol ug/L 11.3 L2502325-116
3&4-Methylphenol(m&p Cresol)ug/L 7.8J L2501623-120
3,3'-Dichlorobenzidine ug/L 66.9250 27 10-154
3,3'-Dimethylbenzidine ug/L 37.3100 37 10-157
3-Methylcholanthrene ug/L 37.250 74 65-130
3-Nitroaniline ug/L 82.7100 83 43-115
4,6-Dinitro-2-methylphenol ug/L 63.9100 64 44-124
4-Aminobiphenyl ug/L 25.650 51 21-125
4-Bromophenylphenyl ether ug/L 26.950 54 34-113
4-Chloro-3-methylphenol ug/L 44.0100 44 31-110
4-Chloroaniline ug/L 33.6100 34 20-120
4-Chlorophenylphenyl ether ug/L 28.050 56 34-116
4-Nitroaniline ug/L 89.4100 89 46-128
4-Nitrophenol ug/L 64.6250 26 11-120
5-Nitro-o-toluidine ug/L 36.3 L2507378-160
7,12-Dimethylbenz(a)anthracene ug/L 37.650 75 47-124
Acenaphthene ug/L 26.450 53 48-114
Acenaphthylene ug/L 26.450 53 48-112
Acetophenone ug/L 12.650 25 24-120
Anthracene ug/L 35.050 70 57-118
Benzo(a)anthracene ug/L 33.050 66 56-121
Benzo(a)pyrene ug/L 37.150 74 55-127
Benzo(b)fluoranthene ug/L 39.850 80 53-128
Benzo(g,h,i)perylene ug/L 33.550 67 54-125
Benzo(k)fluoranthene ug/L 38.950 78 51-123
Benzyl alcohol ug/L 21.4 L21002127-120
bis(2-Chloroethoxy)methane ug/L 10.4 L2502132-120
bis(2-Chloroethyl) ether ug/L 11.0 L2502233-111
bis(2-Ethylhexyl)phthalate ug/L 34.750 69 50-145
Butylbenzylphthalate ug/L 35.850 72 54-138
Chlorobenzilate ug/L 33.950 68 65-132
Chrysene ug/L 33.050 66 58-127
Di-n-butylphthalate ug/L 38.450 77 56-125
Di-n-octylphthalate ug/L 31.150 62 50-134
Diallate ug/L 26.750 53 47-123
Dibenz(a,h)anthracene ug/L 36.250 72 53-129
Dibenzofuran ug/L 29.750 59 45-120
Diethylphthalate ug/L 38.5J50 77 53-120
Dimethoate ug/L 34.350 69 57-139
Dimethylphthalate ug/L 38.450 77 55-116
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
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Page 127 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2017032LABORATORY CONTROL SAMPLE:
LCSSpike
Diphenylamine ug/L 35.350 71 42-120
Disulfoton ug/L 26.750 53 49-156
Ethyl methanesulfonate ug/L 9.5J L2501943-120
Famphur ug/L 122100 122 40-160
Fluoranthene ug/L 35.750 71 57-125
Fluorene ug/L 32.550 65 53-118
Hexachlorobenzene ug/L 31.550 63 49-116
Hexachlorocyclopentadiene ug/L 9.5J L2501926-158
Hexachloroethane ug/L 8.3J L2501730-114
Hexachloropropene ug/L 7.0J50 14 13-137
Indeno(1,2,3-cd)pyrene ug/L 35.250 70 55-128
Isodrin ug/L 34.450 69 68-129
Isophorone ug/L 13.3 L2502731-118
Isosafrole ug/L 19.0 L2503848-107
Kepone ug/L 69.7100 70 10-124
Methapyrilene ug/L 22.4J50 45 40-160
Methyl methanesulfonate ug/L 15.950 32 25-114
Methyl parathion ug/L 33.750 67 58-137
N-Nitroso-di-n-butylamine ug/L 15.0 L2503036-115
N-Nitroso-di-n-propylamine ug/L 12.8 L2502632-119
N-Nitrosodiethylamine ug/L 10.9J L2502247-115
N-Nitrosodimethylamine ug/L 8.7J50 17 13-120
N-Nitrosodiphenylamine ug/L 35.350 71 43-120
N-Nitrosomethylethylamine ug/L 9.7J L2501939-120
N-Nitrosopiperidine ug/L 12.1J L2502443-113
N-Nitrosopyrrolidine ug/L 12.5 L2502532-110
Nitrobenzene ug/L 10.8 L2502233-110
O,O,O-Triethylphosphorothioate ug/L 10.6 L2502151-127
O-Toluidine ug/L 10.0 L2502027-120
P-Dimethylaminoazobenzene ug/L 13.5100 13 10-120
p-Phenylenediamine ug/L 25.7 L2505172-143
Parathion (Ethyl parathion)ug/L 27.4 L2505556-140
Pentachlorobenzene ug/L 25.050 50 30-137
Pentachloronitrobenzene ug/L 37.150 74 70-124
Pentachlorophenol ug/L 70.3250 28 10-137
Phenacetin ug/L 29.950 60 60-130
Phenanthrene ug/L 35.350 71 57-117
Phenol ug/L 5.6J50 11 10-120
Phorate ug/L 26.1 L2505255-126
Pronamide ug/L 33.2 L2506675-124
Pyrene ug/L 37.050 74 55-122
Safrole ug/L 11.8 L2502441-120
Thionazin ug/L 29.4 L2505963-137
2,4,6-Tribromophenol (S)%69 27-110
2-Fluorobiphenyl (S)%37 27-110
2-Fluorophenol (S)%15 12-110
Nitrobenzene-d5 (S)%23 21-110
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
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Huntersville, NC 28078
[phone]
Page 128 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2017032LABORATORY CONTROL SAMPLE:
LCSSpike
Phenol-d6 (S)%10 10-110
Terphenyl-d14 (S)%72 31-107
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2017033MATRIX SPIKE SAMPLE:
MSSpike
Result
92342479002
1,2,4,5-Tetrachlorobenzene ug/L 32.250 64 50-150ND
1,3,5-Trinitrobenzene ug/L 30.050 60 50-150ND
1,3-Dinitrobenzene ug/L 38.350 77 50-150ND
1,4-Naphthoquinone ug/L 49.050 98 50-150ND
1-Naphthalenamine ug/L 19.0 M1503850-150ND
2,2'-Oxybis(1-chloropropane)ug/L 53.850 108 50-150ND
2,3,4,6-Tetrachlorophenol ug/L 75.8 M15015250-150ND
2,4,5-Trichlorophenol ug/L 39.750 79 19-105ND
2,4,6-Trichlorophenol ug/L 46.550 93 13-108ND
2,4-Dichlorophenol ug/L 39.050 78 29-111ND
2,4-Dimethylphenol ug/L 36.950 74 21-103ND
2,4-Dinitrophenol ug/L 223250 89 10-109ND
2,4-Dinitrotoluene ug/L 41.450 83 27-104ND
2,6-Dichlorophenol ug/L 40.350 81 50-150ND
2,6-Dinitrotoluene ug/L 43.650 87 28-101ND
2-Acetylaminofluorene ug/L 30.150 60 50-150ND
2-Chloronaphthalene ug/L 46.650 93 14-102ND
2-Chlorophenol ug/L 37.550 75 16-110ND
2-Methylnaphthalene ug/L 34.550 69 13-110ND
2-Methylphenol(o-Cresol)ug/L 32.650 65 19-110ND
2-Naphthalenamine ug/L 8.3J M1501750-150ND
2-Nitroaniline ug/L 88.7100 89 26-103ND
2-Nitrophenol ug/L 37.550 75 20-110ND
3&4-Methylphenol(m&p Cresol)ug/L 28.350 57 20-110ND
3,3'-Dichlorobenzidine ug/L 61.8250 25 25-112ND
3,3'-Dimethylbenzidine ug/L 7.8J M1100850-150ND
3-Methylcholanthrene ug/L 38.450 76 50-150ND
3-Nitroaniline ug/L 97.2100 97 29-110ND
4,6-Dinitro-2-methylphenol ug/L 77.9100 78 10-117ND
4-Aminobiphenyl ug/L 21.1 M1504250-150ND
4-Bromophenylphenyl ether ug/L 32.350 65 20-105ND
4-Chloro-3-methylphenol ug/L 67.6100 68 22-110ND
4-Chloroaniline ug/L 74.3100 74 20-100ND
4-Chlorophenylphenyl ether ug/L 39.150 78 19-102ND
4-Nitroaniline ug/L 105100 105 29-110ND
4-Nitrophenol ug/L 77.4250 31 10-110ND
5-Nitro-o-toluidine ug/L 41.850 84 50-150ND
7,12-Dimethylbenz(a)anthracene ug/L 41.050 81 50-150ND
Acenaphthene ug/L 44.650 89 17-100ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
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[phone]
Page 129 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2017033MATRIX SPIKE SAMPLE:
MSSpike
Result
92342479002
Acenaphthylene ug/L 45.850 92 21-100ND
Acetophenone ug/L 40.050 80 50-150ND
Anthracene ug/L 40.150 80 24-109ND
Benzo(a)anthracene ug/L 35.450 71 22-117ND
Benzo(a)pyrene ug/L 40.450 81 23-104ND
Benzo(b)fluoranthene ug/L 45.150 90 23-103ND
Benzo(g,h,i)perylene ug/L 37.750 75 18-111ND
Benzo(k)fluoranthene ug/L 41.350 83 22-113ND
Benzyl alcohol ug/L 66.1100 66 19-101ND
bis(2-Chloroethoxy)methane ug/L 32.150 64 22-110ND
bis(2-Chloroethyl) ether ug/L 33.250 66 16-110ND
bis(2-Ethylhexyl)phthalate ug/L 35.450 71 23-102ND
Butylbenzylphthalate ug/L 36.750 73 25-110ND
Chlorobenzilate ug/L 34.450 68 50-150ND
Chrysene ug/L 35.450 71 23-115ND
Di-n-butylphthalate ug/L 42.450 85 26-110ND
Di-n-octylphthalate ug/L 33.750 67 22-110ND
Diallate ug/L 31.350 63 50-150ND
Dibenz(a,h)anthracene ug/L 40.050 80 21-112ND
Dibenzofuran ug/L 45.750 91 19-102ND
Diethylphthalate ug/L 44.8J50 90 29-110ND
Dimethoate ug/L 40.850 82 50-150ND
Dimethylphthalate ug/L 46.750 93 27-110ND
Diphenylamine ug/L 38.550 77 50-150ND
Disulfoton ug/L 27.850 56 50-150ND
Ethyl methanesulfonate ug/L 29.750 59 50-150ND
Famphur ug/L 160 M110016050-150ND
Fluoranthene ug/L 41.850 84 23-112ND
Fluorene ug/L 43.850 88 22-104ND
Hexachlorobenzene ug/L 36.350 73 21-116ND
Hexachlorocyclopentadiene ug/L 33.750 67 10-110ND
Hexachloroethane ug/L 23.550 47 10-110ND
Hexachloropropene ug/L 21.5 M1504350-150ND
Indeno(1,2,3-cd)pyrene ug/L 39.350 79 20-113ND
Isodrin ug/L 37.950 76 50-150ND
Isophorone ug/L 35.850 72 50-150ND
Isosafrole ug/L 38.150 76 50-150ND
Kepone ug/L 96.4100 96 50-150ND
Methapyrilene ug/L 6.9J M1501450-150ND
Methyl methanesulfonate ug/L 48.550 97 50-150ND
Methyl parathion ug/L 40.050 80 50-150ND
N-Nitroso-di-n-butylamine ug/L 33.850 68 50-150ND
N-Nitroso-di-n-propylamine ug/L 43.050 86 21-105ND
N-Nitrosodiethylamine ug/L 33.450 67 50-150ND
N-Nitrosodimethylamine ug/L 23.350 47 10-110ND
N-Nitrosodiphenylamine ug/L 38.550 77 23-107ND
N-Nitrosomethylethylamine ug/L 26.650 53 50-150ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 130 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2017033MATRIX SPIKE SAMPLE:
MSSpike
Result
92342479002
N-Nitrosopiperidine ug/L 38.550 77 50-150ND
N-Nitrosopyrrolidine ug/L 37.850 76 50-150ND
Nitrobenzene ug/L 31.450 63 20-110ND
O,O,O-Triethylphosphorothioate ug/L 37.050 74 50-150ND
O-Toluidine ug/L 26.650 53 50-150ND
P-Dimethylaminoazobenzene ug/L 11.2 M11001150-150ND
p-Phenylenediamine ug/L 35.550 71 50-150ND
Parathion (Ethyl parathion)ug/L 32.050 64 50-150ND
Pentachlorobenzene ug/L 40.250 80 50-150ND
Pentachloronitrobenzene ug/L 41.750 83 50-150ND
Pentachlorophenol ug/L 83.9250 34 10-118ND
Phenacetin ug/L 35.050 70 50-150ND
Phenanthrene ug/L 40.550 81 24-106ND
Phenol ug/L 16.550 33 12-110ND
Phorate ug/L 30.050 60 50-150ND
Pronamide ug/L 37.650 75 50-150ND
Pyrene ug/L 36.350 73 24-114ND
Safrole ug/L 38.050 76 50-150ND
Thionazin ug/L 34.450 69 50-150ND
2,4,6-Tribromophenol (S)%78 27-110
2-Fluorobiphenyl (S)%88 27-110
2-Fluorophenol (S)%42 12-110
Nitrobenzene-d5 (S)%66 21-110
Phenol-d6 (S)%30 10-110
Terphenyl-d14 (S)%61 31-107
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342479007
2018660SAMPLE DUPLICATE:
1,2,4,5-Tetrachlorobenzene ug/L ND 30ND
1,3,5-Trinitrobenzene ug/L ND 30ND
1,3-Dinitrobenzene ug/L ND 30ND
1,4-Naphthoquinone ug/L ND 30ND
1-Naphthalenamine ug/L ND 30ND
2,2'-Oxybis(1-chloropropane)ug/L ND 30ND
2,3,4,6-Tetrachlorophenol ug/L ND 30ND
2,4,5-Trichlorophenol ug/L ND 30ND
2,4,6-Trichlorophenol ug/L ND 30ND
2,4-Dichlorophenol ug/L ND 30ND
2,4-Dimethylphenol ug/L ND 30ND
2,4-Dinitrophenol ug/L ND 30ND
2,4-Dinitrotoluene ug/L ND 30ND
2,6-Dichlorophenol ug/L ND 30ND
2,6-Dinitrotoluene ug/L ND 30ND
2-Acetylaminofluorene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 131 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342479007
2018660SAMPLE DUPLICATE:
2-Chloronaphthalene ug/L ND 30ND
2-Chlorophenol ug/L ND 30ND
2-Methylnaphthalene ug/L ND 30ND
2-Methylphenol(o-Cresol)ug/L ND 30ND
2-Naphthalenamine ug/L ND 30ND
2-Nitroaniline ug/L ND 30ND
2-Nitrophenol ug/L ND 30ND
3&4-Methylphenol(m&p Cresol)ug/L ND 30ND
3,3'-Dichlorobenzidine ug/L ND 30ND
3,3'-Dimethylbenzidine ug/L ND 30ND
3-Methylcholanthrene ug/L ND 30ND
3-Nitroaniline ug/L ND 30ND
4,6-Dinitro-2-methylphenol ug/L ND 30ND
4-Aminobiphenyl ug/L ND 30ND
4-Bromophenylphenyl ether ug/L ND 30ND
4-Chloro-3-methylphenol ug/L ND 30ND
4-Chloroaniline ug/L ND 30ND
4-Chlorophenylphenyl ether ug/L ND 30ND
4-Nitroaniline ug/L ND 30ND
4-Nitrophenol ug/L ND 30ND
5-Nitro-o-toluidine ug/L NDND
7,12-Dimethylbenz(a)anthracene ug/L ND 30ND
Acenaphthene ug/L ND 30ND
Acenaphthylene ug/L ND 30ND
Acetophenone ug/L ND 30ND
Anthracene ug/L ND 30ND
Benzo(a)anthracene ug/L ND 30ND
Benzo(a)pyrene ug/L ND 30ND
Benzo(b)fluoranthene ug/L ND 30ND
Benzo(g,h,i)perylene ug/L ND 30ND
Benzo(k)fluoranthene ug/L ND 30ND
Benzyl alcohol ug/L ND 30ND
bis(2-Chloroethoxy)methane ug/L ND 30ND
bis(2-Chloroethyl) ether ug/L ND 30ND
bis(2-Ethylhexyl)phthalate ug/L ND 30ND
Butylbenzylphthalate ug/L ND 30ND
Chlorobenzilate ug/L ND 30ND
Chrysene ug/L ND 30ND
Di-n-butylphthalate ug/L ND 30ND
Di-n-octylphthalate ug/L ND 30ND
Diallate ug/L ND 30ND
Dibenz(a,h)anthracene ug/L ND 30ND
Dibenzofuran ug/L ND 30ND
Diethylphthalate ug/L ND 30ND
Dimethoate ug/L ND 30ND
Dimethylphthalate ug/L ND 30ND
Diphenylamine ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 132 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342479007
2018660SAMPLE DUPLICATE:
Disulfoton ug/L ND 30ND
Ethyl methanesulfonate ug/L ND 30ND
Famphur ug/L ND 30ND
Fluoranthene ug/L ND 30ND
Fluorene ug/L ND 30ND
Hexachlorobenzene ug/L ND 30ND
Hexachlorocyclopentadiene ug/L ND 30ND
Hexachloroethane ug/L ND 30ND
Hexachloropropene ug/L ND 30ND
Indeno(1,2,3-cd)pyrene ug/L ND 30ND
Isodrin ug/L ND 30ND
Isophorone ug/L ND 30ND
Isosafrole ug/L ND 30ND
Kepone ug/L ND 30ND
Methapyrilene ug/L ND 30ND
Methyl methanesulfonate ug/L ND 30ND
Methyl parathion ug/L ND 30ND
N-Nitroso-di-n-butylamine ug/L ND 30ND
N-Nitroso-di-n-propylamine ug/L ND 30ND
N-Nitrosodiethylamine ug/L ND 30ND
N-Nitrosodimethylamine ug/L ND 30ND
N-Nitrosodiphenylamine ug/L ND 30ND
N-Nitrosomethylethylamine ug/L ND 30ND
N-Nitrosopiperidine ug/L ND 30ND
N-Nitrosopyrrolidine ug/L ND 30ND
Nitrobenzene ug/L ND 30ND
O,O,O-Triethylphosphorothioate ug/L ND 30ND
O-Toluidine ug/L ND 30ND
P-Dimethylaminoazobenzene ug/L ND 30ND
p-Phenylenediamine ug/L ND 30ND
Parathion (Ethyl parathion)ug/L ND 30ND
Pentachlorobenzene ug/L ND 30ND
Pentachloronitrobenzene ug/L ND 30ND
Pentachlorophenol ug/L ND 30ND
Phenacetin ug/L ND 30ND
Phenanthrene ug/L ND 30ND
Phenol ug/L ND 30ND
Phorate ug/L ND 30ND
Pronamide ug/L ND 30ND
Pyrene ug/L ND 30ND
Safrole ug/L ND 30ND
Thionazin ug/L ND 30ND
2,4,6-Tribromophenol (S)%84 689
2-Fluorobiphenyl (S)%100 1090
2-Fluorophenol (S)%41 744
Nitrobenzene-d5 (S)%81 1372
Phenol-d6 (S)%26 728
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 133 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342479007
2018660SAMPLE DUPLICATE:
Terphenyl-d14 (S)%81 1998
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 134 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
364049
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92342478004, 92342478005, 92342530001, 92342530002, 92342530003, 92342530004, 92342530005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2018678
Associated Lab Samples:92342478004, 92342478005, 92342530001, 92342530002, 92342530003, 92342530004, 92342530005
Matrix:Water
AnalyzedMDL
1,2,4,5-Tetrachlorobenzene ug/L ND 10.0 06/14/17 13:231.3
1,3,5-Trinitrobenzene ug/L ND 10.0 06/14/17 13:231.2
1,3-Dinitrobenzene ug/L ND 20.0 06/14/17 13:231.3
1,4-Naphthoquinone ug/L ND 10.0 06/14/17 13:230.99
1-Naphthalenamine ug/L ND 10.0 06/14/17 13:231.3
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 06/14/17 13:231.8
2,3,4,6-Tetrachlorophenol ug/L ND 10.0 06/14/17 13:232.9
2,4,5-Trichlorophenol ug/L ND 10.0 06/14/17 13:231.5
2,4,6-Trichlorophenol ug/L ND 10.0 06/14/17 13:231.4
2,4-Dichlorophenol ug/L ND 10.0 06/14/17 13:231.6
2,4-Dimethylphenol ug/L ND 10.0 06/14/17 13:231.6
2,4-Dinitrophenol ug/L ND 50.0 06/14/17 13:235.1
2,4-Dinitrotoluene ug/L ND 10.0 06/14/17 13:231.5
2,6-Dichlorophenol ug/L ND 10.0 06/14/17 13:231.5
2,6-Dinitrotoluene ug/L ND 10.0 06/14/17 13:231.4
2-Acetylaminofluorene ug/L ND 20.0 06/14/17 13:231.6
2-Chloronaphthalene ug/L ND 10.0 06/14/17 13:231.6
2-Chlorophenol ug/L ND 10.0 06/14/17 13:231.5
2-Methylnaphthalene ug/L ND 10.0 06/14/17 13:231.4
2-Methylphenol(o-Cresol)ug/L ND 10.0 06/14/17 13:231.6
2-Naphthalenamine ug/L ND 10.0 06/14/17 13:232.2
2-Nitroaniline ug/L ND 50.0 06/14/17 13:232.3
2-Nitrophenol ug/L ND 10.0 06/14/17 13:231.6
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 06/14/17 13:231.4
3,3'-Dichlorobenzidine ug/L ND 20.0 06/14/17 13:233.9
3,3'-Dimethylbenzidine ug/L ND 10.0 06/14/17 13:233.9
3-Methylcholanthrene ug/L ND 10.0 06/14/17 13:232.7
3-Nitroaniline ug/L ND 50.0 06/14/17 13:232.7
4,6-Dinitro-2-methylphenol ug/L ND 50.0 06/14/17 13:232.2
4-Aminobiphenyl ug/L ND 20.0 06/14/17 13:231.7
4-Bromophenylphenyl ether ug/L ND 10.0 06/14/17 13:231.5
4-Chloro-3-methylphenol ug/L ND 20.0 06/14/17 13:232.8
4-Chloroaniline ug/L ND 20.0 06/14/17 13:232.8
4-Chlorophenylphenyl ether ug/L ND 10.0 06/14/17 13:231.6
4-Nitroaniline ug/L ND 20.0 06/14/17 13:233.4
4-Nitrophenol ug/L ND 50.0 06/14/17 13:234.3
5-Nitro-o-toluidine ug/L ND 10.0 06/14/17 13:231.9
7,12-Dimethylbenz(a)anthracene ug/L ND 10.0 06/14/17 13:232.4
Acenaphthene ug/L ND 10.0 06/14/17 13:231.6
Acenaphthylene ug/L ND 10.0 06/14/17 13:231.5
Acetophenone ug/L ND 10.0 06/14/17 13:231.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 135 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2018678
Associated Lab Samples:92342478004, 92342478005, 92342530001, 92342530002, 92342530003, 92342530004, 92342530005
Matrix:Water
AnalyzedMDL
Anthracene ug/L ND 10.0 06/14/17 13:231.7
Benzo(a)anthracene ug/L ND 10.0 06/14/17 13:232.1
Benzo(a)pyrene ug/L ND 10.0 06/14/17 13:232.2
Benzo(b)fluoranthene ug/L ND 10.0 06/14/17 13:232.2
Benzo(g,h,i)perylene ug/L ND 10.0 06/14/17 13:232.1
Benzo(k)fluoranthene ug/L ND 10.0 06/14/17 13:232.0
Benzyl alcohol ug/L ND 20.0 06/14/17 13:233.1
bis(2-Chloroethoxy)methane ug/L ND 10.0 06/14/17 13:231.6
bis(2-Chloroethyl) ether ug/L ND 10.0 06/14/17 13:231.7
bis(2-Ethylhexyl)phthalate ug/L ND 15.0 06/14/17 13:232.3
Butylbenzylphthalate ug/L ND 10.0 06/14/17 13:232.5
Chlorobenzilate ug/L ND 10.0 06/14/17 13:232.2
Chrysene ug/L ND 10.0 06/14/17 13:232.1
Di-n-butylphthalate ug/L ND 10.0 06/14/17 13:232.0
Di-n-octylphthalate ug/L ND 10.0 06/14/17 13:231.5
Diallate ug/L ND 10.0 06/14/17 13:231.6
Dibenz(a,h)anthracene ug/L ND 10.0 06/14/17 13:232.0
Dibenzofuran ug/L ND 10.0 06/14/17 13:231.7
Diethylphthalate ug/L ND 6000 06/14/17 13:231.6
Dimethoate ug/L ND 20.0 06/14/17 13:231.8
Dimethylphthalate ug/L ND 10.0 06/14/17 13:231.4
Diphenylamine ug/L ND 10.0 06/14/17 13:231.4
Disulfoton ug/L ND 10.0 06/14/17 13:231.5
Ethyl methanesulfonate ug/L ND 20.0 06/14/17 13:231.6
Famphur ug/L ND 20.0 06/14/17 13:235.7
Fluoranthene ug/L ND 10.0 06/14/17 13:232.2
Fluorene ug/L ND 10.0 06/14/17 13:231.6
Hexachlorobenzene ug/L ND 10.0 06/14/17 13:231.7
Hexachlorocyclopentadiene ug/L ND 10.0 06/14/17 13:231.3
Hexachloroethane ug/L ND 10.0 06/14/17 13:231.8
Hexachloropropene ug/L ND 10.0 06/14/17 13:231.2
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 06/14/17 13:232.0
Isodrin ug/L ND 20.0 06/14/17 13:232.5
Isophorone ug/L ND 10.0 06/14/17 13:231.5
Isosafrole ug/L ND 10.0 06/14/17 13:231.5
Kepone ug/L ND 20.0 06/14/17 13:234.5
Methapyrilene ug/L ND 100 06/14/17 13:233.0
Methyl methanesulfonate ug/L ND 10.0 06/14/17 13:231.1
Methyl parathion ug/L ND 10.0 06/14/17 13:231.6
N-Nitroso-di-n-butylamine ug/L ND 10.0 06/14/17 13:231.6
N-Nitroso-di-n-propylamine ug/L ND 10.0 06/14/17 13:231.7
N-Nitrosodiethylamine ug/L ND 20.0 06/14/17 13:231.4
N-Nitrosodimethylamine ug/L ND 10.0 06/14/17 13:231.6
N-Nitrosodiphenylamine ug/L ND 10.0 06/14/17 13:231.4
N-Nitrosomethylethylamine ug/L ND 10.0 06/14/17 13:231.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 136 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2018678
Associated Lab Samples:92342478004, 92342478005, 92342530001, 92342530002, 92342530003, 92342530004, 92342530005
Matrix:Water
AnalyzedMDL
N-Nitrosopiperidine ug/L ND 20.0 06/14/17 13:231.7
N-Nitrosopyrrolidine ug/L ND 10.0 06/14/17 13:231.7
Nitrobenzene ug/L ND 10.0 06/14/17 13:231.6
O,O,O-Triethylphosphorothioate ug/L ND 10.0 06/14/17 13:231.7
O-Toluidine ug/L ND 10.0 06/14/17 13:231.7
P-Dimethylaminoazobenzene ug/L ND 10.0 06/14/17 13:231.0
p-Phenylenediamine ug/L ND 10.0 06/14/17 13:232.2
Parathion (Ethyl parathion)ug/L ND 10.0 06/14/17 13:231.5
Pentachlorobenzene ug/L ND 10.0 06/14/17 13:231.5
Pentachloronitrobenzene ug/L ND 20.0 06/14/17 13:231.7
Pentachlorophenol ug/L ND 25.0 06/14/17 13:233.5
Phenacetin ug/L ND 20.0 06/14/17 13:231.9
Phenanthrene ug/L ND 10.0 06/14/17 13:231.6
Phenol ug/L ND 10.0 06/14/17 13:231.3
Phorate ug/L ND 10.0 06/14/17 13:231.7
Pronamide ug/L ND 10.0 06/14/17 13:232.0
Pyrene ug/L ND 10.0 06/14/17 13:232.2
Safrole ug/L ND 10.0 06/14/17 13:231.3
Thionazin ug/L ND 20.0 06/14/17 13:231.7
2,4,6-Tribromophenol (S)%74 27-110 06/14/17 13:23
2-Fluorobiphenyl (S)%77 27-110 06/14/17 13:23
2-Fluorophenol (S)%37 12-110 06/14/17 13:23
Nitrobenzene-d5 (S)%62 21-110 06/14/17 13:23
Phenol-d6 (S)%25 10-110 06/14/17 13:23
Terphenyl-d14 (S)%87 31-107 06/14/17 13:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2018679LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4,5-Tetrachlorobenzene ug/L 34.450 69 16-129
1,3,5-Trinitrobenzene ug/L 32.650 65 55-125
1,3-Dinitrobenzene ug/L 42.550 85 30-122
1,4-Naphthoquinone ug/L 41.850 84 31-120
1-Naphthalenamine ug/L 27.050 54 37-126
2,2'-Oxybis(1-chloropropane)ug/L 52.950 106 18-120
2,3,4,6-Tetrachlorophenol ug/L 82.350 165 54-276
2,4,5-Trichlorophenol ug/L 43.150 86 43-113
2,4,6-Trichlorophenol ug/L 50.850 102 42-120
2,4-Dichlorophenol ug/L 42.750 85 30-120
2,4-Dimethylphenol ug/L 37.950 76 29-111
2,4-Dinitrophenol ug/L 246250 98 19-132
2,4-Dinitrotoluene ug/L 45.150 90 58-128
2,6-Dichlorophenol ug/L 43.650 87 54-128
2,6-Dinitrotoluene ug/L 47.050 94 54-129
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 137 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2018679LABORATORY CONTROL SAMPLE:
LCSSpike
2-Acetylaminofluorene ug/L 38.7 L2507781-160
2-Chloronaphthalene ug/L 53.050 106 43-117
2-Chlorophenol ug/L 41.950 84 37-120
2-Methylnaphthalene ug/L 37.650 75 33-120
2-Methylphenol(o-Cresol)ug/L 34.350 69 31-120
2-Naphthalenamine ug/L 34.150 68 41-136
2-Nitroaniline ug/L 88.7100 89 48-121
2-Nitrophenol ug/L 40.750 81 25-116
3&4-Methylphenol(m&p Cresol)ug/L 29.850 60 23-120
3,3'-Dichlorobenzidine ug/L 88.8250 36 10-154
3,3'-Dimethylbenzidine ug/L 41.5100 42 10-157
3-Methylcholanthrene ug/L 46.850 94 65-130
3-Nitroaniline ug/L 107100 107 43-115
4,6-Dinitro-2-methylphenol ug/L 87.7100 88 44-124
4-Aminobiphenyl ug/L 25.750 51 21-125
4-Bromophenylphenyl ether ug/L 34.850 70 34-113
4-Chloro-3-methylphenol ug/L 73.8100 74 31-110
4-Chloroaniline ug/L 87.8100 88 20-120
4-Chlorophenylphenyl ether ug/L 41.750 83 34-116
4-Nitroaniline ug/L 111100 111 46-128
4-Nitrophenol ug/L 79.5250 32 11-120
5-Nitro-o-toluidine ug/L 45.650 91 78-160
7,12-Dimethylbenz(a)anthracene ug/L 46.050 92 47-124
Acenaphthene ug/L 47.250 94 48-114
Acenaphthylene ug/L 48.650 97 48-112
Acetophenone ug/L 42.450 85 24-120
Anthracene ug/L 43.250 86 57-118
Benzo(a)anthracene ug/L 42.850 86 56-121
Benzo(a)pyrene ug/L 45.950 92 55-127
Benzo(b)fluoranthene ug/L 48.850 98 53-128
Benzo(g,h,i)perylene ug/L 39.650 79 54-125
Benzo(k)fluoranthene ug/L 46.150 92 51-123
Benzyl alcohol ug/L 77.8100 78 27-120
bis(2-Chloroethoxy)methane ug/L 33.250 66 32-120
bis(2-Chloroethyl) ether ug/L 34.250 68 33-111
bis(2-Ethylhexyl)phthalate ug/L 43.050 86 50-145
Butylbenzylphthalate ug/L 45.050 90 54-138
Chlorobenzilate ug/L 42.850 86 65-132
Chrysene ug/L 42.650 85 58-127
Di-n-butylphthalate ug/L 46.050 92 56-125
Di-n-octylphthalate ug/L 41.150 82 50-134
Diallate ug/L 33.150 66 47-123
Dibenz(a,h)anthracene ug/L 43.750 87 53-129
Dibenzofuran ug/L 48.350 97 45-120
Diethylphthalate ug/L 46.7J50 93 53-120
Dimethoate ug/L 39.750 79 57-139
Dimethylphthalate ug/L 48.650 97 55-116
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 138 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2018679LABORATORY CONTROL SAMPLE:
LCSSpike
Diphenylamine ug/L 44.950 90 42-120
Disulfoton ug/L 33.350 67 49-156
Ethyl methanesulfonate ug/L 31.050 62 43-120
Famphur ug/L 107100 107 40-160
Fluoranthene ug/L 44.450 89 57-125
Fluorene ug/L 46.550 93 53-118
Hexachlorobenzene ug/L 39.850 80 49-116
Hexachlorocyclopentadiene ug/L 35.450 71 26-158
Hexachloroethane ug/L 25.850 52 30-114
Hexachloropropene ug/L 24.150 48 13-137
Indeno(1,2,3-cd)pyrene ug/L 42.150 84 55-128
Isodrin ug/L 40.050 80 68-129
Isophorone ug/L 36.550 73 31-118
Isosafrole ug/L 40.950 82 48-107
Kepone ug/L 65.8100 66 10-124
Methapyrilene ug/L 21.0J50 42 40-160
Methyl methanesulfonate ug/L 46.350 93 25-114
Methyl parathion ug/L 42.950 86 58-137
N-Nitroso-di-n-butylamine ug/L 35.450 71 36-115
N-Nitroso-di-n-propylamine ug/L 43.850 88 32-119
N-Nitrosodiethylamine ug/L 34.650 69 47-115
N-Nitrosodimethylamine ug/L 23.150 46 13-120
N-Nitrosodiphenylamine ug/L 44.950 90 43-120
N-Nitrosomethylethylamine ug/L 28.050 56 39-120
N-Nitrosopiperidine ug/L 41.650 83 43-113
N-Nitrosopyrrolidine ug/L 41.750 83 32-110
Nitrobenzene ug/L 31.550 63 33-110
O,O,O-Triethylphosphorothioate ug/L 38.150 76 51-127
O-Toluidine ug/L 32.150 64 27-120
P-Dimethylaminoazobenzene ug/L 17.3100 17 10-120
p-Phenylenediamine ug/L 37.650 75 72-143
Parathion (Ethyl parathion)ug/L 35.450 71 56-140
Pentachlorobenzene ug/L 42.950 86 30-137
Pentachloronitrobenzene ug/L 44.150 88 70-124
Pentachlorophenol ug/L 97.2250 39 10-137
Phenacetin ug/L 37.050 74 60-130
Phenanthrene ug/L 43.150 86 57-117
Phenol ug/L 18.950 38 10-120
Phorate ug/L 32.650 65 55-126
Pronamide ug/L 40.450 81 75-124
Pyrene ug/L 45.350 91 55-122
Safrole ug/L 41.450 83 41-120
Thionazin ug/L 35.250 70 63-137
2,4,6-Tribromophenol (S)%90 27-110
2-Fluorobiphenyl (S)%90 27-110
2-Fluorophenol (S)%46 12-110
Nitrobenzene-d5 (S)%67 21-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 139 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2018679LABORATORY CONTROL SAMPLE:
LCSSpike
Phenol-d6 (S)%34 10-110
Terphenyl-d14 (S)%91 31-107
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2022108MATRIX SPIKE SAMPLE:
MSSpike
Result
92342530002
1,2,4,5-Tetrachlorobenzene ug/L 37.750 75 50-150ND
1,3,5-Trinitrobenzene ug/L 33.650 67 50-150ND
1,3-Dinitrobenzene ug/L 41.450 83 50-150ND
1,4-Naphthoquinone ug/L 44.850 90 50-150ND
1-Naphthalenamine ug/L 14.2 M1502850-150ND
2,2'-Oxybis(1-chloropropane)ug/L 52.050 104 50-150ND
2,3,4,6-Tetrachlorophenol ug/L 85.5 M15017150-150ND
2,4,5-Trichlorophenol ug/L 44.750 89 19-105ND
2,4,6-Trichlorophenol ug/L 52.450 105 13-108ND
2,4-Dichlorophenol ug/L 39.550 79 29-111ND
2,4-Dimethylphenol ug/L 36.250 72 21-103ND
2,4-Dinitrophenol ug/L 207250 83 10-109ND
2,4-Dinitrotoluene ug/L 46.750 93 27-104ND
2,6-Dichlorophenol ug/L 40.550 81 50-150ND
2,6-Dinitrotoluene ug/L 48.550 97 28-101ND
2-Acetylaminofluorene ug/L 36.850 73 50-150ND
2-Chloronaphthalene ug/L 58.1 M15011614-102ND
2-Chlorophenol ug/L 36.350 73 16-110ND
2-Methylnaphthalene ug/L 36.850 74 13-110ND
2-Methylphenol(o-Cresol)ug/L 29.750 59 19-110ND
2-Naphthalenamine ug/L 11.5 M1502350-150ND
2-Nitroaniline ug/L 95.3100 95 26-103ND
2-Nitrophenol ug/L 36.550 73 20-110ND
3&4-Methylphenol(m&p Cresol)ug/L 25.550 51 20-110ND
3,3'-Dichlorobenzidine ug/L 78.3250 31 25-112ND
3,3'-Dimethylbenzidine ug/L 20.1 M11002050-150ND
3-Methylcholanthrene ug/L 44.550 89 50-150ND
3-Nitroaniline ug/L 104100 104 29-110ND
4,6-Dinitro-2-methylphenol ug/L 73.6100 74 10-117ND
4-Aminobiphenyl ug/L 21.2 M1504250-150ND
4-Bromophenylphenyl ether ug/L 35.350 71 20-105ND
4-Chloro-3-methylphenol ug/L 69.2100 69 22-110ND
4-Chloroaniline ug/L 59.4100 59 20-100ND
4-Chlorophenylphenyl ether ug/L 45.050 90 19-102ND
4-Nitroaniline ug/L 112 M110011229-110ND
4-Nitrophenol ug/L 78.0250 31 10-110ND
5-Nitro-o-toluidine ug/L 46.350 93 50-150ND
7,12-Dimethylbenz(a)anthracene ug/L 46.550 93 50-150ND
Acenaphthene ug/L 50.250 100 17-100ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 140 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2022108MATRIX SPIKE SAMPLE:
MSSpike
Result
92342530002
Acenaphthylene ug/L 51.2 M15010221-100ND
Acetophenone ug/L 36.550 73 50-150ND
Anthracene ug/L 44.450 89 24-109ND
Benzo(a)anthracene ug/L 41.650 83 22-117ND
Benzo(a)pyrene ug/L 44.750 89 23-104ND
Benzo(b)fluoranthene ug/L 48.950 98 23-103ND
Benzo(g,h,i)perylene ug/L 40.550 81 18-111ND
Benzo(k)fluoranthene ug/L 45.150 90 22-113ND
Benzyl alcohol ug/L 63.0100 63 19-101ND
bis(2-Chloroethoxy)methane ug/L 31.850 64 22-110ND
bis(2-Chloroethyl) ether ug/L 33.150 66 16-110ND
bis(2-Ethylhexyl)phthalate ug/L 44.850 90 23-102ND
Butylbenzylphthalate ug/L 45.650 91 25-110ND
Chlorobenzilate ug/L 42.750 85 50-150ND
Chrysene ug/L 42.250 84 23-115ND
Di-n-butylphthalate ug/L 48.350 97 26-110ND
Di-n-octylphthalate ug/L 41.550 83 22-110ND
Diallate ug/L 35.250 70 50-150ND
Dibenz(a,h)anthracene ug/L 42.050 84 21-112ND
Dibenzofuran ug/L 51.250 102 19-102ND
Diethylphthalate ug/L 50.2J50 100 29-110ND
Dimethoate ug/L 42.950 86 50-150ND
Dimethylphthalate ug/L 51.550 103 27-110ND
Diphenylamine ug/L 45.850 92 50-150ND
Disulfoton ug/L 35.450 71 50-150ND
Ethyl methanesulfonate ug/L 27.450 55 50-150ND
Famphur ug/L 130100 130 50-150ND
Fluoranthene ug/L 45.850 92 23-112ND
Fluorene ug/L 49.150 98 22-104ND
Hexachlorobenzene ug/L 40.050 80 21-116ND
Hexachlorocyclopentadiene ug/L 35.950 72 10-110ND
Hexachloroethane ug/L 27.250 54 10-110ND
Hexachloropropene ug/L 25.550 51 50-150ND
Indeno(1,2,3-cd)pyrene ug/L 42.450 85 20-113ND
Isodrin ug/L 42.350 85 50-150ND
Isophorone ug/L 35.650 71 50-150ND
Isosafrole ug/L 43.650 87 50-150ND
Kepone ug/L 72.4100 72 50-150ND
Methapyrilene ug/L 33.3J50 67 50-150ND
Methyl methanesulfonate ug/L 42.550 85 50-150ND
Methyl parathion ug/L 42.950 86 50-150ND
N-Nitroso-di-n-butylamine ug/L 32.350 65 50-150ND
N-Nitroso-di-n-propylamine ug/L 37.250 74 21-105ND
N-Nitrosodiethylamine ug/L 28.750 57 50-150ND
N-Nitrosodimethylamine ug/L 20.750 41 10-110ND
N-Nitrosodiphenylamine ug/L 45.850 92 23-107ND
N-Nitrosomethylethylamine ug/L 23.7 M1504750-150ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 141 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2022108MATRIX SPIKE SAMPLE:
MSSpike
Result
92342530002
N-Nitrosopiperidine ug/L 37.250 74 50-150ND
N-Nitrosopyrrolidine ug/L 28.650 57 50-150ND
Nitrobenzene ug/L 30.450 61 20-110ND
O,O,O-Triethylphosphorothioate ug/L 36.850 74 50-150ND
O-Toluidine ug/L 20.6 M1504150-150ND
P-Dimethylaminoazobenzene ug/L 16.8 M11001750-150ND
p-Phenylenediamine ug/L 35.250 70 50-150ND
Parathion (Ethyl parathion)ug/L 36.650 73 50-150ND
Pentachlorobenzene ug/L 44.750 89 50-150ND
Pentachloronitrobenzene ug/L 44.850 90 50-150ND
Pentachlorophenol ug/L 88.9250 36 10-118ND
Phenacetin ug/L 37.150 74 50-150ND
Phenanthrene ug/L 44.850 90 24-106ND
Phenol ug/L 15.350 31 12-110ND
Phorate ug/L 33.650 67 50-150ND
Pronamide ug/L 41.650 83 50-150ND
Pyrene ug/L 45.050 90 24-114ND
Safrole ug/L 38.450 77 50-150ND
Thionazin ug/L 38.050 76 50-150ND
2,4,6-Tribromophenol (S)%87 27-110
2-Fluorobiphenyl (S)%95 27-110
2-Fluorophenol (S)%39 12-110
Nitrobenzene-d5 (S)%62 21-110
Phenol-d6 (S)%27 10-110
Terphenyl-d14 (S)%74 31-107
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342530004
2018681SAMPLE DUPLICATE:
1,2,4,5-Tetrachlorobenzene ug/L ND 30ND
1,3,5-Trinitrobenzene ug/L ND 30ND
1,3-Dinitrobenzene ug/L ND 30ND
1,4-Naphthoquinone ug/L ND 30ND
1-Naphthalenamine ug/L ND 30ND
2,2'-Oxybis(1-chloropropane)ug/L ND 30ND
2,3,4,6-Tetrachlorophenol ug/L ND 30ND
2,4,5-Trichlorophenol ug/L ND 30ND
2,4,6-Trichlorophenol ug/L ND 30ND
2,4-Dichlorophenol ug/L ND 30ND
2,4-Dimethylphenol ug/L ND 30ND
2,4-Dinitrophenol ug/L ND 30ND
2,4-Dinitrotoluene ug/L ND 30ND
2,6-Dichlorophenol ug/L ND 30ND
2,6-Dinitrotoluene ug/L ND 30ND
2-Acetylaminofluorene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 142 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342530004
2018681SAMPLE DUPLICATE:
2-Chloronaphthalene ug/L ND 30ND
2-Chlorophenol ug/L ND 30ND
2-Methylnaphthalene ug/L ND 30ND
2-Methylphenol(o-Cresol)ug/L ND 30ND
2-Naphthalenamine ug/L ND 30ND
2-Nitroaniline ug/L ND 30ND
2-Nitrophenol ug/L ND 30ND
3&4-Methylphenol(m&p Cresol)ug/L ND 30ND
3,3'-Dichlorobenzidine ug/L ND 30ND
3,3'-Dimethylbenzidine ug/L ND 30ND
3-Methylcholanthrene ug/L ND 30ND
3-Nitroaniline ug/L ND 30ND
4,6-Dinitro-2-methylphenol ug/L ND 30ND
4-Aminobiphenyl ug/L ND 30ND
4-Bromophenylphenyl ether ug/L ND 30ND
4-Chloro-3-methylphenol ug/L ND 30ND
4-Chloroaniline ug/L ND 30ND
4-Chlorophenylphenyl ether ug/L ND 30ND
4-Nitroaniline ug/L ND 30ND
4-Nitrophenol ug/L ND 30ND
5-Nitro-o-toluidine ug/L NDND
7,12-Dimethylbenz(a)anthracene ug/L ND 30ND
Acenaphthene ug/L ND 30ND
Acenaphthylene ug/L ND 30ND
Acetophenone ug/L ND 30ND
Anthracene ug/L ND 30ND
Benzo(a)anthracene ug/L ND 30ND
Benzo(a)pyrene ug/L ND 30ND
Benzo(b)fluoranthene ug/L ND 30ND
Benzo(g,h,i)perylene ug/L ND 30ND
Benzo(k)fluoranthene ug/L ND 30ND
Benzyl alcohol ug/L ND 30ND
bis(2-Chloroethoxy)methane ug/L ND 30ND
bis(2-Chloroethyl) ether ug/L ND 30ND
bis(2-Ethylhexyl)phthalate ug/L ND 30ND
Butylbenzylphthalate ug/L ND 30ND
Chlorobenzilate ug/L ND 30ND
Chrysene ug/L ND 30ND
Di-n-butylphthalate ug/L ND 30ND
Di-n-octylphthalate ug/L ND 30ND
Diallate ug/L ND 30ND
Dibenz(a,h)anthracene ug/L ND 30ND
Dibenzofuran ug/L ND 30ND
Diethylphthalate ug/L ND 30ND
Dimethoate ug/L ND 30ND
Dimethylphthalate ug/L ND 30ND
Diphenylamine ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 143 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342530004
2018681SAMPLE DUPLICATE:
Disulfoton ug/L ND 30ND
Ethyl methanesulfonate ug/L ND 30ND
Famphur ug/L ND 30ND
Fluoranthene ug/L ND 30ND
Fluorene ug/L ND 30ND
Hexachlorobenzene ug/L ND 30ND
Hexachlorocyclopentadiene ug/L ND 30ND
Hexachloroethane ug/L ND 30ND
Hexachloropropene ug/L ND 30ND
Indeno(1,2,3-cd)pyrene ug/L ND 30ND
Isodrin ug/L ND 30ND
Isophorone ug/L ND 30ND
Isosafrole ug/L ND 30ND
Kepone ug/L ND 30ND
Methapyrilene ug/L ND 30ND
Methyl methanesulfonate ug/L ND 30ND
Methyl parathion ug/L ND 30ND
N-Nitroso-di-n-butylamine ug/L ND 30ND
N-Nitroso-di-n-propylamine ug/L ND 30ND
N-Nitrosodiethylamine ug/L ND 30ND
N-Nitrosodimethylamine ug/L ND 30ND
N-Nitrosodiphenylamine ug/L ND 30ND
N-Nitrosomethylethylamine ug/L ND 30ND
N-Nitrosopiperidine ug/L ND 30ND
N-Nitrosopyrrolidine ug/L ND 30ND
Nitrobenzene ug/L ND 30ND
O,O,O-Triethylphosphorothioate ug/L ND 30ND
O-Toluidine ug/L ND 30ND
P-Dimethylaminoazobenzene ug/L ND 30ND
p-Phenylenediamine ug/L ND 30ND
Parathion (Ethyl parathion)ug/L ND 30ND
Pentachlorobenzene ug/L ND 30ND
Pentachloronitrobenzene ug/L ND 30ND
Pentachlorophenol ug/L ND 30ND
Phenacetin ug/L ND 30ND
Phenanthrene ug/L ND 30ND
Phenol ug/L ND 30ND
Phorate ug/L ND 30ND
Pronamide ug/L ND 30ND
Pyrene ug/L ND 30ND
Safrole ug/L ND 30ND
Thionazin ug/L ND 30ND
2,4,6-Tribromophenol (S)%88 2371
2-Fluorobiphenyl (S)%88 2370
2-Fluorophenol (S)%40 2332
Nitrobenzene-d5 (S)%69 2057
Phenol-d6 (S)%27 2820
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 144 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342530004
2018681SAMPLE DUPLICATE:
Terphenyl-d14 (S)%60 2476
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 145 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363621
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92342478003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2015987
Associated Lab Samples:92342478003
Matrix:Water
AnalyzedMDL
Sulfide ug/L ND 1000 06/06/17 22:15100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2015988LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 464J500 93 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015989MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342281006
2015990
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L R15008780-120105 19 10500ND433J524J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015991MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342472017
2015992
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 85 80-12085 0 10500ND470J468J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 146 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363623
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92342530001, 92342530002, 92342530003, 92342530004, 92342530005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2016031
Associated Lab Samples:92342530001, 92342530002, 92342530003, 92342530004, 92342530005
Matrix:Water
AnalyzedMDL
Sulfide ug/L ND 1000 06/06/17 23:00100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2016032LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 470J500 94 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2016033MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342317011
2016034
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 91 80-12093 2 10500ND454J463J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2016035MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342530004
2016036
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 82 80-12085 4 10500ND408J423J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 147 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
362992
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92342478003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2012287
Associated Lab Samples:92342478003
Matrix:Water
AnalyzedMDL
Cyanide ug/L ND 10.0 06/01/17 17:524.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012288LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 109100 109 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2012289MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342479002
2012290
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L 100 104 80-12096 8 101004.4J 109 100
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2012291MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342478003
2012292
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L 100 93 80-12099 6 101004.6J 97.4 103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 148 of 166
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363513
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92342530001, 92342530002, 92342530003, 92342530004, 92342530005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2015224
Associated Lab Samples:92342530001, 92342530002, 92342530003, 92342530004, 92342530005
Matrix:Water
AnalyzedMDL
Cyanide ug/L ND 10.0 06/07/17 13:524.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2015225LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 101100 101 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015226MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342317015
2015227
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L 100 94 80-12091 2 10100ND97.6 95.4
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015228MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342712006
2015229
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L M1,R11002980-12019 27 101000.013
mg/L 41.2 31.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 149 of 166
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
Pace Analytical Services - Ormond BeachPASI-O
BATCH QUALIFIERS
Batch: 372970
A matrix spike/matrix spike duplicate was not performed for this batch due to insufficient sample volume.[M5]
ANALYTE QUALIFIERS
Sample re-extracted outside method hold time. Results of re-analysis confirmed original analysis performed within hold
time.1g
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 150 of 166
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92342478003 363163 363590MW-15 EPA 3510 EPA 8081
92342530001 363163 363590MW-13 EPA 3510 EPA 8081
92342530002 363163 363590MW-16 EPA 3510 EPA 8081
92342530003 363163 363590MW-17 EPA 3510 EPA 8081
92342530004 363163 363590MW-21 EPA 3510 EPA 8081
92342530005 363163 363590MW-22 EPA 3510 EPA 8081
92342478004 363426 363552MW-1 EPA 3510 EPA 8081
92342478005 363426 363552MW-9 EPA 3510 EPA 8081
92342478003 363162 363349MW-15 EPA 3510 EPA 8082
92342530001 363162 363349MW-13 EPA 3510 EPA 8082
92342530002 363162 363349MW-16 EPA 3510 EPA 8082
92342530003 363162 363349MW-17 EPA 3510 EPA 8082
92342530004 363162 363349MW-21 EPA 3510 EPA 8082
92342530005 363162 363349MW-22 EPA 3510 EPA 8082
92342478004 363427 363555MW-1 EPA 3510 EPA 8082
92342478005 363427 363555MW-9 EPA 3510 EPA 8082
92342478003 372315 372970MW-15 EPA 8151 EPA 8151
92342530001 373221 373976MW-13 EPA 8151 EPA 8151
92342530002 373221 373976MW-16 EPA 8151 EPA 8151
92342530003 373221 373976MW-17 EPA 8151 EPA 8151
92342530004 373221 373976MW-21 EPA 8151 EPA 8151
92342530005 373221 373976MW-22 EPA 8151 EPA 8151
92342478004 373221 373976MW-1 EPA 8151 EPA 8151
92342478005 373221 373976MW-9 EPA 8151 EPA 8151
92342478001 363009 363688MW-3R EPA 3010A EPA 6010
92342478002 363009 363688MW-23 EPA 3010A EPA 6010
92342478003 363010 363689MW-15 EPA 3010A EPA 6010
92342530001 363146 364135MW-13 EPA 3010A EPA 6010
92342530002 363146 364135MW-16 EPA 3010A EPA 6010
92342530003 363146 364135MW-17 EPA 3010A EPA 6010
92342530004 363146 364135MW-21 EPA 3010A EPA 6010
92342530005 363146 364135MW-22 EPA 3010A EPA 6010
92342478004 363321 364621MW-1 EPA 3010A EPA 6010
92342478005 363321 364621MW-9 EPA 3010A EPA 6010
92342478006 363321 364621MW-7 EPA 3010A EPA 6010
92342478007 363322 363795MW-12S EPA 3010A EPA 6010
92342478008 363322 363795MW-14 EPA 3010A EPA 6010
92342478009 363322 363795MW-18 EPA 3010A EPA 6010
92342478010 363322 363795MW-19 EPA 3010A EPA 6010
92342478011 363322 363795MW-20 EPA 3010A EPA 6010
92342478001 363272 363377MW-3R EPA 3010A EPA 6020B
92342478002 363272 363377MW-23 EPA 3010A EPA 6020B
92342478003 363272 363377MW-15 EPA 3010A EPA 6020B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 151 of 166
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92342530001 363478 363771MW-13 EPA 3010A EPA 6020B
92342530002 363478 363771MW-16 EPA 3010A EPA 6020B
92342530003 363478 363771MW-17 EPA 3010A EPA 6020B
92342530004 363478 363771MW-21 EPA 3010A EPA 6020B
92342530005 363478 363771MW-22 EPA 3010A EPA 6020B
92342478004 363273 363378MW-1 EPA 3010A EPA 6020B
92342478005 363273 363378MW-9 EPA 3010A EPA 6020B
92342478006 363273 363378MW-7 EPA 3010A EPA 6020B
92342478007 363273 363378MW-12S EPA 3010A EPA 6020B
92342478008 363273 363378MW-14 EPA 3010A EPA 6020B
92342478009 363273 363378MW-18 EPA 3010A EPA 6020B
92342478010 363273 363378MW-19 EPA 3010A EPA 6020B
92342478011 363273 363378MW-20 EPA 3010A EPA 6020B
92342478003 363333 363334MW-15 EPA 7470 EPA 7470
92342530001 363457 363483MW-13 EPA 7470 EPA 7470
92342530002 363457 363483MW-16 EPA 7470 EPA 7470
92342530003 363457 363483MW-17 EPA 7470 EPA 7470
92342530004 363457 363483MW-21 EPA 7470 EPA 7470
92342530005 363457 363483MW-22 EPA 7470 EPA 7470
92342478004 363459 363485MW-1 EPA 7470 EPA 7470
92342478005 363459 363485MW-9 EPA 7470 EPA 7470
92342478003 363842 364328MW-15 EPA 3510 EPA 8270
92342530001 364049 364817MW-13 EPA 3510 EPA 8270
92342530002 364049 364817MW-16 EPA 3510 EPA 8270
92342530003 364049 364817MW-17 EPA 3510 EPA 8270
92342530004 364049 364817MW-21 EPA 3510 EPA 8270
92342530005 364049 364817MW-22 EPA 3510 EPA 8270
92342478004 364049 364817MW-1 EPA 3510 EPA 8270
92342478005 364049 364817MW-9 EPA 3510 EPA 8270
92342478001 363024MW-3R EPA 8260
92342478002 363024MW-23 EPA 8260
92342478003 363024MW-15 EPA 8260
92342530001 363026MW-13 EPA 8260
92342530002 363026MW-16 EPA 8260
92342530003 363026MW-17 EPA 8260
92342530004 363307MW-21 EPA 8260
92342530005 363026MW-22 EPA 8260
92342478004 363328MW-1 EPA 8260
92342478005 363328MW-9 EPA 8260
92342478006 363328MW-7 EPA 8260
92342478007 363328MW-12S EPA 8260
92342478008 363328MW-14 EPA 8260
92342478009 363328MW-18 EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 152 of 166
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92342478
SURRY CLOSED-MT. AIRY (UIC)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92342478010 363328MW-19 EPA 8260
92342478011 363328MW-20 EPA 8260
92342478003 363621MW-15 SM 4500-S2D
92342530001 363623MW-13 SM 4500-S2D
92342530002 363623MW-16 SM 4500-S2D
92342530003 363623MW-17 SM 4500-S2D
92342530004 363623MW-21 SM 4500-S2D
92342530005 363623MW-22 SM 4500-S2D
92342478003 362992MW-15 SM 4500-CN-E
92342530001 363513MW-13 SM 4500-CN-E
92342530002 363513MW-16 SM 4500-CN-E
92342530003 363513MW-17 SM 4500-CN-E
92342530004 363513MW-21 SM 4500-CN-E
92342530005 363513MW-22 SM 4500-CN-E
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 01:10 PM
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9800 Kincey Ave. Suite 100
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[phone]
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#=CL#
June 26, 2017
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92342553
92342553
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
SURRY CLOSED-MT. AIRY (MNA)
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory between June 01, 2017
and June 02, 2017. The results relate only to the samples included in this report. Results reported
herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality
Assurance Manual, where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
Page 1 of 33
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92342553
SURRY CLOSED-MT. AIRY (MNA)
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
Page 2 of 33
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92342553
SURRY CLOSED-MT. AIRY (MNA)
Lab ID Sample ID Matrix Date Collected Date Received
92342553001 MW-15 Water 05/31/17 17:00 06/01/17 07:55
92342553002 MW-21 Water 05/31/17 17:20 06/01/17 07:55
92342553003 MW-1 Water 06/01/17 12:35 06/02/17 08:00
92342553004 MW-7 Water 06/01/17 14:45 06/02/17 08:00
92342553005 MW-9 Water 06/01/17 15:40 06/02/17 08:00
92342553006 MW-14 Water 06/01/17 09:00 06/02/17 08:00
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
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[phone]
Page 3 of 33
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92342553
SURRY CLOSED-MT. AIRY (MNA)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92342553001 MW-15 SM 2320B 1 PASI-AKDF1
SM 3500-Fe B 1 PASI-ACJH1
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-ADMN
SM 5220D 1 PASI-ACJH1
SM 5310B 1 PASI-AKDF1
92342553002 MW-21 SM 2320B 1 PASI-AKDF1
SM 3500-Fe B 1 PASI-ACJH1
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-ADMN
SM 5220D 1 PASI-ACJH1
SM 5310B 1 PASI-AKDF1
92342553003 MW-1 SM 2320B 1 PASI-AKDF1
SM 3500-Fe B 1 PASI-ACJH1
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-ACJH1
SM 4500-CN-E 1 PASI-AAES2
SM 5220D 1 PASI-ACJH1
SM 5310B 1 PASI-AKDF1
92342553004 MW-7 SM 2320B 1 PASI-AKDF1
SM 3500-Fe B 1 PASI-ACJH1
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-ACJH1
SM 5220D 1 PASI-ACJH1
SM 5310B 1 PASI-AKDF1
92342553005 MW-9 SM 2320B 1 PASI-AKDF1
SM 3500-Fe B 1 PASI-ACJH1
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-ACJH1
SM 4500-CN-E 1 PASI-AAES2
SM 5220D 1 PASI-ACJH1
SM 5310B 1 PASI-AKDF1
92342553006 MW-14 SM 2320B 1 PASI-AKDF1
SM 3500-Fe B 1 PASI-ACJH1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
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[phone]
Page 4 of 33
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92342553
SURRY CLOSED-MT. AIRY (MNA)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
SM 4500-S2D 1 PASI-AMVC
EPA 300.0 1 PASI-ACDC
SM 4500-Cl-E 1 PASI-ACJH1
SM 5220D 1 PASI-ACJH1
SM 5310B 1 PASI-AKDF1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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Page 5 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342553
SURRY CLOSED-MT. AIRY (MNA)
Sample:MW-15 Lab ID:92342553001 Collected:05/31/17 17:00 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 43700 ug/L 06/03/17 09:30500010001
Analytical Method: SM 3500-Fe BIron, Ferrous
Iron, Ferrous 1.7 mg/L 06/06/17 01:32 H1,N20.50 0.50 1
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 1180J ug/L 06/05/17 18:27 14808-79-82500005001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 1450 ug/L 06/05/17 11:22 16887-00-610005001
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand ND ug/L 06/09/17 04:3025000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 675J ug/L 06/03/17 00:35 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/26/2017 04:24 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 6 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342553
SURRY CLOSED-MT. AIRY (MNA)
Sample:MW-21 Lab ID:92342553002 Collected:05/31/17 17:20 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 34900 ug/L 06/03/17 09:42500010001
Analytical Method: SM 3500-Fe BIron, Ferrous
Iron, Ferrous ND mg/L 06/06/17 01:32 H1,N20.50 0.50 1
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 1380J ug/L 06/05/17 19:36 14808-79-82500005001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 28800 ug/L 06/05/17 11:26 16887-00-610005001
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand ND ug/L 06/09/17 04:3025000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 1200 ug/L 06/03/17 00:46 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/26/2017 04:24 PM
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Page 7 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342553
SURRY CLOSED-MT. AIRY (MNA)
Sample:MW-1 Lab ID:92342553003 Collected:06/01/17 12:35 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 42200 ug/L 06/06/17 01:12500010001
Analytical Method: SM 3500-Fe BIron, Ferrous
Iron, Ferrous ND mg/L 06/06/17 01:32 H1,N20.50 0.50 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/06/17 21:30 18496-25-810001001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 8830J ug/L 06/10/17 19:44 14808-79-82500005001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 3770 ug/L 06/14/17 02:48 16887-00-610005001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/24/17 18:46 57-12-5 H110.0 4.0 1
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand ND ug/L 06/09/17 04:3025000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 605J ug/L 06/07/17 03:09 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/26/2017 04:24 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 8 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342553
SURRY CLOSED-MT. AIRY (MNA)
Sample:MW-7 Lab ID:92342553004 Collected:06/01/17 14:45 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 69200 ug/L 06/06/17 01:24500010001
Analytical Method: SM 3500-Fe BIron, Ferrous
Iron, Ferrous ND mg/L 06/06/17 01:32 H1,N20.50 0.50 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/06/17 21:30 18496-25-810001001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 5520J ug/L 06/10/17 20:01 14808-79-82500005001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 31200 ug/L 06/14/17 02:49 16887-00-610005001
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 20000J ug/L 06/09/17 04:3025000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 2400 ug/L 06/07/17 03:20 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/26/2017 04:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342553
SURRY CLOSED-MT. AIRY (MNA)
Sample:MW-9 Lab ID:92342553005 Collected:06/01/17 15:40 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 44800 ug/L 06/06/17 01:55500010001
Analytical Method: SM 3500-Fe BIron, Ferrous
Iron, Ferrous 1.3 mg/L 06/06/17 01:32 H1,N20.50 0.50 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/06/17 21:30 18496-25-810001001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 984J ug/L 06/10/17 20:17 14808-79-82500005001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 28300 ug/L 06/14/17 02:50 16887-00-610005001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 5.5J ug/L 06/14/17 11:48 57-12-5 M110.0 4.0 1
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 23000J ug/L 06/09/17 04:3025000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 2250 ug/L 06/07/17 03:34 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/26/2017 04:24 PM
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Page 10 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342553
SURRY CLOSED-MT. AIRY (MNA)
Sample:MW-14 Lab ID:92342553006 Collected:06/01/17 09:00 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 31600 ug/L 06/06/17 02:06500010001
Analytical Method: SM 3500-Fe BIron, Ferrous
Iron, Ferrous ND mg/L 06/06/17 01:32 H1,N20.50 0.50 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide 115J ug/L 06/06/17 21:30 18496-25-810001001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 2060J ug/L 06/11/17 01:18 14808-79-82500005001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 2280 ug/L 06/14/17 02:51 16887-00-610005001
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 13000J ug/L 06/09/17 04:3025000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 1420 ug/L 06/07/17 03:49 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/26/2017 04:24 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342553
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363125
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92342553001, 92342553002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2013190
Associated Lab Samples:92342553001, 92342553002
Matrix:Water
AnalyzedMDL
Alkalinity, Total as CaCO3 ug/L ND 5000 06/05/17 12:061000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2013191LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 ug/L 5110050000 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2013192MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342496001
2013193
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L 50000 103 80-12095 5 255000019.6 mg/L 70800 67200
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2013194MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342317011
2013195
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L 50000 102 80-120100 1 2550000323008310082500
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/26/2017 04:24 PM
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Huntersville, NC 28078
[phone]
Page 12 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342553
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363343
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92342553003, 92342553004, 92342553005, 92342553006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014291
Associated Lab Samples:92342553003, 92342553004, 92342553005, 92342553006
Matrix:Water
AnalyzedMDL
Alkalinity, Total as CaCO3 ug/L ND 5000 06/05/17 20:551000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014292LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 ug/L 5080050000 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014293MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342317017
2014294
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L 50000 110 80-12097 1 2550000587000642000636000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014295MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342317020
2014296
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L M1500006580-12068 1 2550000135000167000169000
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/26/2017 04:24 PM
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Page 13 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342553
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363473
SM 3500-Fe B
SM 3500-Fe B
Iron, Ferrous
Associated Lab Samples:92342553001, 92342553002, 92342553003, 92342553004, 92342553005, 92342553006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2015125
Associated Lab Samples:92342553001, 92342553002, 92342553003, 92342553004, 92342553005, 92342553006
Matrix:Water
AnalyzedMDL
Iron, Ferrous mg/L ND 0.50 N206/06/17 01:320.50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2015126LABORATORY CONTROL SAMPLE:
LCSSpike
Iron, Ferrous mg/L 1.5 N21.5 102 90-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342553001
2015127SAMPLE DUPLICATE:
Iron, Ferrous mg/L 1.7 H1,N22101.7
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/26/2017 04:24 PM
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[phone]
Page 14 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342553
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363647
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92342553003, 92342553004, 92342553005, 92342553006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2016111
Associated Lab Samples:92342553003, 92342553004, 92342553005, 92342553006
Matrix:Water
AnalyzedMDL
Sulfide ug/L ND 1000 06/06/17 21:30100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2016112LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 528J500 106 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2016113MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342742003
2016114
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 102 80-120107 5 10500ND546J573J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2016115MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342742013
2016116
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 105 80-120111 5 10500ND526J553J
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/26/2017 04:24 PM
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Page 15 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342553
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363396
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92342553001, 92342553002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014592
Associated Lab Samples:92342553001, 92342553002
Matrix:Water
AnalyzedMDL
Sulfate ug/L ND 250000 06/05/17 16:44500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014593LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 50400J50000 101 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014594MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342317015
2014595
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L 50000 101 90-110103 2 10500001820068600J69700J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014596MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342600004
2014597
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L M1,R150000390-11078 47 10500005840060100J97400J
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/26/2017 04:24 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 16 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342553
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
364291
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92342553003, 92342553004, 92342553005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2020011
Associated Lab Samples:92342553003, 92342553004, 92342553005
Matrix:Water
AnalyzedMDL
Sulfate ug/L ND 250000 06/10/17 11:47500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2020012LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 50200J50000 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2020015MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92343524006
2020016
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L 50000 98 90-110101 2 105000014.8 mg/L 63800J 65100J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2020039MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92343485001
2020040
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L M6500005990-11057 0 10500001830 mg/L 1860000
J
1860000
J
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/26/2017 04:24 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 17 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342553
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
364314
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92342553006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2020086
Associated Lab Samples:92342553006
Matrix:Water
AnalyzedMDL
Sulfate ug/L ND 250000 06/11/17 00:44500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2020087LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 49000J50000 98 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2020088MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342553006
2020089
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L 50000 103 90-110105 2 10500002060J53600J54700J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2020090MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92343524013
2020091
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L 50000 107 90-110104 2 105000013.6 mg/L 67100J 65800J
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/26/2017 04:24 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342553
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363371
SM 4500-Cl-E
SM 4500-Cl-E
4500 Chloride
Associated Lab Samples:92342553001, 92342553002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014368
Associated Lab Samples:92342553001, 92342553002
Matrix:Water
AnalyzedMDL
Chloride ug/L ND 1000 06/05/17 10:58500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014369LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride ug/L 1960020000 98 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014370MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342674001
2014371
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L M11000048990-110492 0 101000080.8 mg/L 130000 130000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014372MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342496003
2014373
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L 10000 100 90-110100 0 10100002.3 mg/L 12300 12200
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/26/2017 04:24 PM
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Huntersville, NC 28078
[phone]
Page 19 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342553
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
364538
SM 4500-Cl-E
SM 4500-Cl-E
4500 Chloride
Associated Lab Samples:92342553003, 92342553004, 92342553005, 92342553006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2021020
Associated Lab Samples:92342553003, 92342553004, 92342553005, 92342553006
Matrix:Water
AnalyzedMDL
Chloride ug/L ND 1000 06/14/17 03:57500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2021021LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride ug/L 2040020000 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2021022MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342317019
2021023
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L M6,R110000-22 90-110-1450 58 1010000318000315000173000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2021024MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92343251002
2021025
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L 10000 96 90-11096 0 101000023.3 mg/L 32900 32900
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/26/2017 04:24 PM
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Huntersville, NC 28078
[phone]
Page 20 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342553
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
364584
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92342553005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2021203
Associated Lab Samples:92342553005
Matrix:Water
AnalyzedMDL
Cyanide ug/L ND 10.0 06/14/17 11:344.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2021204LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 99.1100 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2021205MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92343009001
2021206
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L 100 93 80-12087 7 10100ND94.3 88.3
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2021207MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342553005
2021208
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L M11005880-12057 1 101005.5J 63.2 62.7
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/26/2017 04:24 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342553
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
366221
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92342553003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2030002
Associated Lab Samples:92342553003
Matrix:Water
AnalyzedMDL
Cyanide ug/L ND 10.0 06/24/17 20:314.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2030003LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 103100 103 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2030004MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92345320006
2030005
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L 100 99 80-12098 2 10100ND103101
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2030006MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92345112002
2030007
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L M1100-6 80-1203 101000.012
mg/L 5.8J 15.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2017 04:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342553
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
364072
SM 5220D
SM 5220D
5220D COD
Associated Lab Samples:92342553001, 92342553002, 92342553003, 92342553004, 92342553005, 92342553006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2018787
Associated Lab Samples:92342553001, 92342553002, 92342553003, 92342553004, 92342553005, 92342553006
Matrix:Water
AnalyzedMDL
Chemical Oxygen Demand ug/L ND 25000 06/09/17 04:3012500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2018788LABORATORY CONTROL SAMPLE:
LCSSpike
Chemical Oxygen Demand ug/L 755000750000 101 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2018789MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92343255002
2018790
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L M1,R17500009090-11082 6 3750000469 mg/L 1140000 1080000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2018791MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342740001
2018792
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L 750000 106 90-110103 3 375000081.0 mg/L 877000 855000
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/26/2017 04:24 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342553
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363127
SM 5310B
SM 5310B
5310B TOC
Associated Lab Samples:92342553001, 92342553002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2013202
Associated Lab Samples:92342553001, 92342553002
Matrix:Water
AnalyzedMDL
Total Organic Carbon ug/L ND 1000 06/02/17 22:46500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2013203LABORATORY CONTROL SAMPLE:
LCSSpike
Total Organic Carbon ug/L 2370025000 95 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2013204MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342496002
2013205
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Total Organic Carbon ug/L 25000 90 90-11093 3 10250001.7 mg/L 24100 24900
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/26/2017 04:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342553
SURRY CLOSED-MT. AIRY (MNA)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363536
SM 5310B
SM 5310B
5310B TOC
Associated Lab Samples:92342553003, 92342553004, 92342553005, 92342553006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2015350
Associated Lab Samples:92342553003, 92342553004, 92342553005, 92342553006
Matrix:Water
AnalyzedMDL
Total Organic Carbon ug/L ND 1000 06/07/17 08:18500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2015351LABORATORY CONTROL SAMPLE:
LCSSpike
Total Organic Carbon ug/L 2520025000 101 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015352MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342745003
2015353
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Total Organic Carbon ug/L M1250008690-11086 0 10250006.6 mg/L 28100 28000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2017 04:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 33
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92342553
SURRY CLOSED-MT. AIRY (MNA)
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
ANALYTE QUALIFIERS
Analysis conducted outside the EPA method holding time.H1
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6
The lab does not hold NELAC/TNI accreditation for this parameter.N2
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/26/2017 04:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 33
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92342553
SURRY CLOSED-MT. AIRY (MNA)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92342553001 363125MW-15 SM 2320B
92342553002 363125MW-21 SM 2320B
92342553003 363343MW-1 SM 2320B
92342553004 363343MW-7 SM 2320B
92342553005 363343MW-9 SM 2320B
92342553006 363343MW-14 SM 2320B
92342553001 363473MW-15 SM 3500-Fe B
92342553002 363473MW-21 SM 3500-Fe B
92342553003 363473MW-1 SM 3500-Fe B
92342553004 363473MW-7 SM 3500-Fe B
92342553005 363473MW-9 SM 3500-Fe B
92342553006 363473MW-14 SM 3500-Fe B
92342553003 363647MW-1 SM 4500-S2D
92342553004 363647MW-7 SM 4500-S2D
92342553005 363647MW-9 SM 4500-S2D
92342553006 363647MW-14 SM 4500-S2D
92342553001 363396MW-15 EPA 300.0
92342553002 363396MW-21 EPA 300.0
92342553003 364291MW-1 EPA 300.0
92342553004 364291MW-7 EPA 300.0
92342553005 364291MW-9 EPA 300.0
92342553006 364314MW-14 EPA 300.0
92342553001 363371MW-15 SM 4500-Cl-E
92342553002 363371MW-21 SM 4500-Cl-E
92342553003 364538MW-1 SM 4500-Cl-E
92342553004 364538MW-7 SM 4500-Cl-E
92342553005 364538MW-9 SM 4500-Cl-E
92342553006 364538MW-14 SM 4500-Cl-E
92342553003 366221MW-1 SM 4500-CN-E
92342553005 364584MW-9 SM 4500-CN-E
92342553001 364072MW-15 SM 5220D
92342553002 364072MW-21 SM 5220D
92342553003 364072MW-1 SM 5220D
92342553004 364072MW-7 SM 5220D
92342553005 364072MW-9 SM 5220D
92342553006 364072MW-14 SM 5220D
92342553001 363127MW-15 SM 5310B
92342553002 363127MW-21 SM 5310B
92342553003 363536MW-1 SM 5310B
92342553004 363536MW-7 SM 5310B
92342553005 363536MW-9 SM 5310B
92342553006 363536MW-14 SM 5310B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/26/2017 04:24 PM
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Huntersville, NC 28078
[phone]
Page 27 of 33
Page 28 of 33
Page 29 of 33
Page 30 of 33
Page 31 of 33
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Page 33 of 33
#=CL#
June 16, 2017
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92342549
92342549
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
SURRY MSWLF SWS
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory between June 01, 2017
and June 02, 2017. The results relate only to the samples included in this report. Results reported
herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality
Assurance Manual, where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 44
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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Huntersville, NC 28078
[phone]
Page 2 of 44
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Lab ID Sample ID Matrix Date Collected Date Received
92342549001 SW-3 Water 05/31/17 00:00 06/01/17 07:55
92342730001 SW-1 Water 06/01/17 10:25 06/02/17 08:00
92342730002 SW-2 Water 06/01/17 16:00 06/02/17 08:00
92342730004 SW-4 Water 06/01/17 10:35 06/02/17 08:00
92342730005 SWN-1 Water 06/01/17 11:00 06/02/17 08:00
92342730006 SWN-2 Water 06/01/17 14:00 06/02/17 08:00
92342730007 SW-A Water 06/01/17 12:10 06/02/17 08:00
92342730008 SW-B Water 06/01/17 12:30 06/02/17 08:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 44
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92342549001 SW-3 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92342730001 SW-1 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92342730002 SW-2 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92342730004 SW-4 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92342730005 SWN-1 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92342730006 SWN-2 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92342730007 SW-A EPA 8260 50 PASI-CGAW
92342730008 SW-B EPA 8260 50 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Sample:SW-3 Lab ID:92342549001 Collected:05/31/17 00:00 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/09/17 21:51 7440-36-006/02/17 11:256.0 3.9 1
Arsenic ND ug/L 06/09/17 21:51 7440-38-206/02/17 11:2510.0 5.0 1
Barium 21.8J ug/L 06/09/17 21:51 7440-39-306/02/17 11:251002.5 1
Beryllium ND ug/L 06/09/17 21:51 7440-41-706/02/17 11:251.0 0.50 1
Cadmium ND ug/L 06/09/17 21:51 7440-43-906/02/17 11:251.0 0.50 1
Chromium ND ug/L 06/09/17 21:51 7440-47-306/02/17 11:2510.0 2.5 1
Cobalt 8.0J ug/L 06/09/17 21:51 7440-48-406/02/17 11:2510.0 2.5 1
Copper ND ug/L 06/09/17 21:51 7440-50-806/02/17 11:2510.0 2.5 1
Lead ND ug/L 06/09/17 21:51 7439-92-106/02/17 11:2510.0 2.5 1
Nickel ND ug/L 06/09/17 21:51 7440-02-006/02/17 11:2550.0 2.5 1
Selenium ND ug/L 06/09/17 21:51 7782-49-206/02/17 11:2510.0 5.0 1
Silver ND ug/L 06/09/17 21:51 7440-22-406/02/17 11:2510.0 2.5 1
Vanadium ND ug/L 06/09/17 21:51 7440-62-206/02/17 11:2525.0 2.5 1
Zinc 7.4J ug/L 06/09/17 21:51 7440-66-606/02/17 11:2510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/09/17 17:22 7440-28-006/06/17 02:455.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/04/17 08:10 67-64-110010.0 1
Acrylonitrile ND ug/L 06/04/17 08:10 107-13-12001.9 1
Benzene ND ug/L 06/04/17 08:10 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 08:10 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 08:10 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 08:10 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 08:10 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 08:10 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 08:10 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 08:10 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/17 08:10 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 08:10 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 08:10 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/17 08:10 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 08:10 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 08:10 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 08:10 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 08:10 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 08:10 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/04/17 08:10 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 08:10 110-57-6 L11001.0 1
1,1-Dichloroethane ND ug/L 06/04/17 08:10 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 08:10 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 08:10 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/17 08:10 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 08:10 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 08:10 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Sample:SW-3 Lab ID:92342549001 Collected:05/31/17 00:00 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 06/04/17 08:10 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 08:10 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 08:10 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/04/17 08:10 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 08:10 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/04/17 08:10 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 08:10 108-10-11000.33 1
Styrene ND ug/L 06/04/17 08:10 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 08:10 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 08:10 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 08:10 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 08:10 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/04/17 08:10 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 08:10 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 08:10 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 08:10 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 08:10 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 08:10 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 08:10 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/17 08:10 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %06/04/17 08:10 460-00-470-130 1
1,2-Dichloroethane-d4 (S)90 %06/04/17 08:10 17060-07-070-130 1
Toluene-d8 (S)107 %06/04/17 08:10 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Sample:SW-1 Lab ID:92342730001 Collected:06/01/17 10:25 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/14/17 22:06 7440-36-006/04/17 16:406.0 3.9 1
Arsenic ND ug/L 06/14/17 22:06 7440-38-206/04/17 16:4010.0 5.0 1
Barium 26.8J ug/L 06/14/17 22:06 7440-39-306/04/17 16:401002.5 1
Beryllium ND ug/L 06/14/17 22:06 7440-41-706/04/17 16:401.0 0.50 1
Cadmium ND ug/L 06/14/17 22:06 7440-43-906/04/17 16:401.0 0.50 1
Chromium ND ug/L 06/14/17 22:06 7440-47-306/04/17 16:4010.0 2.5 1
Cobalt ND ug/L 06/14/17 22:06 7440-48-406/04/17 16:4010.0 2.5 1
Copper ND ug/L 06/14/17 22:06 7440-50-806/04/17 16:4010.0 2.5 1
Lead ND ug/L 06/14/17 22:06 7439-92-106/04/17 16:4010.0 2.5 1
Nickel ND ug/L 06/14/17 22:06 7440-02-006/04/17 16:4050.0 2.5 1
Selenium ND ug/L 06/14/17 22:06 7782-49-206/04/17 16:4010.0 5.0 1
Silver ND ug/L 06/14/17 22:06 7440-22-406/04/17 16:4010.0 2.5 1
Vanadium ND ug/L 06/14/17 22:06 7440-62-206/04/17 16:4025.0 2.5 1
Zinc ND ug/L 06/14/17 22:06 7440-66-606/04/17 16:4010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/09/17 17:51 7440-28-006/06/17 02:455.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/04/17 11:43 67-64-110010.0 1
Acrylonitrile ND ug/L 06/04/17 11:43 107-13-12001.9 1
Benzene ND ug/L 06/04/17 11:43 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 11:43 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 11:43 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 11:43 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 11:43 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 11:43 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 11:43 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 11:43 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/17 11:43 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 11:43 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 11:43 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/17 11:43 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 11:43 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 11:43 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 11:43 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 11:43 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 11:43 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/04/17 11:43 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 11:43 110-57-6 L11001.0 1
1,1-Dichloroethane ND ug/L 06/04/17 11:43 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 11:43 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 11:43 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/17 11:43 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 11:43 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 11:43 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Sample:SW-1 Lab ID:92342730001 Collected:06/01/17 10:25 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 06/04/17 11:43 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 11:43 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 11:43 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/04/17 11:43 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 11:43 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/04/17 11:43 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 11:43 108-10-11000.33 1
Styrene ND ug/L 06/04/17 11:43 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 11:43 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 11:43 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 11:43 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 11:43 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/04/17 11:43 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 11:43 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 11:43 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 11:43 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 11:43 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 11:43 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 11:43 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/17 11:43 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %06/04/17 11:43 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %06/04/17 11:43 17060-07-070-130 1
Toluene-d8 (S)108 %06/04/17 11:43 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Sample:SW-2 Lab ID:92342730002 Collected:06/01/17 16:00 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/14/17 22:09 7440-36-006/04/17 16:406.0 3.9 1
Arsenic ND ug/L 06/14/17 22:09 7440-38-206/04/17 16:4010.0 5.0 1
Barium 17.0J ug/L 06/14/17 22:09 7440-39-306/04/17 16:401002.5 1
Beryllium ND ug/L 06/14/17 22:09 7440-41-706/04/17 16:401.0 0.50 1
Cadmium ND ug/L 06/14/17 22:09 7440-43-906/04/17 16:401.0 0.50 1
Chromium ND ug/L 06/14/17 22:09 7440-47-306/04/17 16:4010.0 2.5 1
Cobalt 16.8 ug/L 06/14/17 22:09 7440-48-406/04/17 16:4010.0 2.5 1
Copper ND ug/L 06/14/17 22:09 7440-50-806/04/17 16:4010.0 2.5 1
Lead ND ug/L 06/14/17 22:09 7439-92-106/04/17 16:4010.0 2.5 1
Nickel ND ug/L 06/14/17 22:09 7440-02-006/04/17 16:4050.0 2.5 1
Selenium ND ug/L 06/14/17 22:09 7782-49-206/04/17 16:4010.0 5.0 1
Silver ND ug/L 06/14/17 22:09 7440-22-406/04/17 16:4010.0 2.5 1
Vanadium ND ug/L 06/14/17 22:09 7440-62-206/04/17 16:4025.0 2.5 1
Zinc ND ug/L 06/14/17 22:09 7440-66-606/04/17 16:4010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.048J ug/L 06/09/17 20:09 7440-28-006/06/17 02:455.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 13.3J ug/L 06/04/17 12:01 67-64-110010.0 1
Acrylonitrile ND ug/L 06/04/17 12:01 107-13-12001.9 1
Benzene ND ug/L 06/04/17 12:01 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 12:01 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 12:01 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 12:01 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 12:01 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 12:01 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 12:01 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 12:01 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/17 12:01 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 12:01 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 12:01 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/17 12:01 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 12:01 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 12:01 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 12:01 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 12:01 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 12:01 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/04/17 12:01 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 12:01 110-57-6 L11001.0 1
1,1-Dichloroethane ND ug/L 06/04/17 12:01 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 12:01 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 12:01 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 2.4J ug/L 06/04/17 12:01 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 12:01 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 12:01 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Sample:SW-2 Lab ID:92342730002 Collected:06/01/17 16:00 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 06/04/17 12:01 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 12:01 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 12:01 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/04/17 12:01 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 12:01 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/04/17 12:01 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 12:01 108-10-11000.33 1
Styrene ND ug/L 06/04/17 12:01 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 12:01 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 12:01 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 12:01 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 12:01 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/04/17 12:01 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 12:01 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 12:01 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 12:01 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 12:01 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 12:01 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 12:01 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/17 12:01 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)108 %06/04/17 12:01 460-00-470-130 1
1,2-Dichloroethane-d4 (S)90 %06/04/17 12:01 17060-07-070-130 1
Toluene-d8 (S)108 %06/04/17 12:01 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Sample:SW-4 Lab ID:92342730004 Collected:06/01/17 10:35 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/14/17 22:12 7440-36-006/04/17 16:406.0 3.9 1
Arsenic ND ug/L 06/14/17 22:12 7440-38-206/04/17 16:4010.0 5.0 1
Barium 22.0J ug/L 06/14/17 22:12 7440-39-306/04/17 16:401002.5 1
Beryllium ND ug/L 06/14/17 22:12 7440-41-706/04/17 16:401.0 0.50 1
Cadmium ND ug/L 06/14/17 22:12 7440-43-906/04/17 16:401.0 0.50 1
Chromium ND ug/L 06/14/17 22:12 7440-47-306/04/17 16:4010.0 2.5 1
Cobalt ND ug/L 06/14/17 22:12 7440-48-406/04/17 16:4010.0 2.5 1
Copper ND ug/L 06/14/17 22:12 7440-50-806/04/17 16:4010.0 2.5 1
Lead ND ug/L 06/14/17 22:12 7439-92-106/04/17 16:4010.0 2.5 1
Nickel ND ug/L 06/14/17 22:12 7440-02-006/04/17 16:4050.0 2.5 1
Selenium ND ug/L 06/14/17 22:12 7782-49-206/04/17 16:4010.0 5.0 1
Silver ND ug/L 06/14/17 22:12 7440-22-406/04/17 16:4010.0 2.5 1
Vanadium ND ug/L 06/14/17 22:12 7440-62-206/04/17 16:4025.0 2.5 1
Zinc 7.0J ug/L 06/14/17 22:12 7440-66-606/04/17 16:4010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.054J ug/L 06/09/17 20:14 7440-28-006/06/17 02:455.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 19.3J ug/L 06/04/17 12:19 67-64-110010.0 1
Acrylonitrile ND ug/L 06/04/17 12:19 107-13-12001.9 1
Benzene ND ug/L 06/04/17 12:19 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 12:19 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 12:19 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 12:19 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 12:19 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 12:19 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 12:19 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 12:19 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/17 12:19 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 12:19 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 12:19 67-66-35.0 0.14 1
Chloromethane 0.13J ug/L 06/04/17 12:19 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 12:19 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 12:19 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 12:19 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 12:19 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 12:19 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/04/17 12:19 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 12:19 110-57-6 L11001.0 1
1,1-Dichloroethane ND ug/L 06/04/17 12:19 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 12:19 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 12:19 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/17 12:19 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 12:19 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 12:19 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Sample:SW-4 Lab ID:92342730004 Collected:06/01/17 10:35 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 06/04/17 12:19 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 12:19 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 12:19 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/04/17 12:19 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 12:19 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/04/17 12:19 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 12:19 108-10-11000.33 1
Styrene ND ug/L 06/04/17 12:19 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 12:19 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 12:19 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 12:19 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 12:19 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/04/17 12:19 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 12:19 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 12:19 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 12:19 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 12:19 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 12:19 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 12:19 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/17 12:19 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)104 %06/04/17 12:19 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %06/04/17 12:19 17060-07-070-130 1
Toluene-d8 (S)108 %06/04/17 12:19 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Sample:SWN-1 Lab ID:92342730005 Collected:06/01/17 11:00 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/14/17 22:24 7440-36-006/04/17 16:406.0 3.9 1
Arsenic ND ug/L 06/14/17 22:24 7440-38-206/04/17 16:4010.0 5.0 1
Barium 21.3J ug/L 06/14/17 22:24 7440-39-306/04/17 16:401002.5 1
Beryllium ND ug/L 06/14/17 22:24 7440-41-706/04/17 16:401.0 0.50 1
Cadmium ND ug/L 06/14/17 22:24 7440-43-906/04/17 16:401.0 0.50 1
Chromium ND ug/L 06/14/17 22:24 7440-47-306/04/17 16:4010.0 2.5 1
Cobalt ND ug/L 06/14/17 22:24 7440-48-406/04/17 16:4010.0 2.5 1
Copper ND ug/L 06/14/17 22:24 7440-50-806/04/17 16:4010.0 2.5 1
Lead ND ug/L 06/14/17 22:24 7439-92-106/04/17 16:4010.0 2.5 1
Nickel ND ug/L 06/14/17 22:24 7440-02-006/04/17 16:4050.0 2.5 1
Selenium ND ug/L 06/14/17 22:24 7782-49-206/04/17 16:4010.0 5.0 1
Silver ND ug/L 06/14/17 22:24 7440-22-406/04/17 16:4010.0 2.5 1
Vanadium ND ug/L 06/14/17 22:24 7440-62-206/04/17 16:4025.0 2.5 1
Zinc 9.1J ug/L 06/14/17 22:24 7440-66-606/04/17 16:4010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/09/17 20:16 7440-28-006/06/17 02:455.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/04/17 12:37 67-64-110010.0 1
Acrylonitrile ND ug/L 06/04/17 12:37 107-13-12001.9 1
Benzene ND ug/L 06/04/17 12:37 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 12:37 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 12:37 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 12:37 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 12:37 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 12:37 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 12:37 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 12:37 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/17 12:37 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 12:37 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 12:37 67-66-35.0 0.14 1
Chloromethane 0.13J ug/L 06/04/17 12:37 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 12:37 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 12:37 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 12:37 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 12:37 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 12:37 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/04/17 12:37 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 12:37 110-57-6 L11001.0 1
1,1-Dichloroethane ND ug/L 06/04/17 12:37 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 12:37 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 12:37 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/17 12:37 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 12:37 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 12:37 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Sample:SWN-1 Lab ID:92342730005 Collected:06/01/17 11:00 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 06/04/17 12:37 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 12:37 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 12:37 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/04/17 12:37 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 12:37 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/04/17 12:37 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 12:37 108-10-11000.33 1
Styrene ND ug/L 06/04/17 12:37 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 12:37 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 12:37 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 12:37 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 12:37 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/04/17 12:37 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 12:37 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 12:37 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 12:37 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 12:37 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 12:37 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 12:37 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/17 12:37 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %06/04/17 12:37 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %06/04/17 12:37 17060-07-070-130 1
Toluene-d8 (S)109 %06/04/17 12:37 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Sample:SWN-2 Lab ID:92342730006 Collected:06/01/17 14:00 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/14/17 22:28 7440-36-006/04/17 16:406.0 3.9 1
Arsenic ND ug/L 06/14/17 22:28 7440-38-206/04/17 16:4010.0 5.0 1
Barium 20.4J ug/L 06/14/17 22:28 7440-39-306/04/17 16:401002.5 1
Beryllium ND ug/L 06/14/17 22:28 7440-41-706/04/17 16:401.0 0.50 1
Cadmium ND ug/L 06/14/17 22:28 7440-43-906/04/17 16:401.0 0.50 1
Chromium ND ug/L 06/14/17 22:28 7440-47-306/04/17 16:4010.0 2.5 1
Cobalt ND ug/L 06/14/17 22:28 7440-48-406/04/17 16:4010.0 2.5 1
Copper ND ug/L 06/14/17 22:28 7440-50-806/04/17 16:4010.0 2.5 1
Lead ND ug/L 06/14/17 22:28 7439-92-106/04/17 16:4010.0 2.5 1
Nickel ND ug/L 06/14/17 22:28 7440-02-006/04/17 16:4050.0 2.5 1
Selenium ND ug/L 06/14/17 22:28 7782-49-206/04/17 16:4010.0 5.0 1
Silver ND ug/L 06/14/17 22:28 7440-22-406/04/17 16:4010.0 2.5 1
Vanadium 2.8J ug/L 06/14/17 22:28 7440-62-206/04/17 16:4025.0 2.5 1
Zinc 5.4J ug/L 06/14/17 22:28 7440-66-606/04/17 16:4010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/09/17 20:18 7440-28-006/06/17 02:455.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 11.6J ug/L 06/04/17 12:55 67-64-110010.0 1
Acrylonitrile ND ug/L 06/04/17 12:55 107-13-12001.9 1
Benzene ND ug/L 06/04/17 12:55 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 12:55 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 12:55 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 12:55 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 12:55 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 12:55 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 12:55 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 12:55 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/17 12:55 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 12:55 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 12:55 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/17 12:55 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 12:55 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 12:55 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 12:55 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 12:55 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 12:55 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/04/17 12:55 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 12:55 110-57-6 L1,M01001.0 1
1,1-Dichloroethane ND ug/L 06/04/17 12:55 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 12:55 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 12:55 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/17 12:55 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 12:55 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 12:55 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Sample:SWN-2 Lab ID:92342730006 Collected:06/01/17 14:00 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 06/04/17 12:55 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 12:55 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 12:55 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/04/17 12:55 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 12:55 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/04/17 12:55 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 12:55 108-10-11000.33 1
Styrene ND ug/L 06/04/17 12:55 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 12:55 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 12:55 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 12:55 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 12:55 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/04/17 12:55 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 12:55 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 12:55 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 12:55 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 12:55 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 12:55 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 12:55 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/17 12:55 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)106 %06/04/17 12:55 460-00-470-130 1
1,2-Dichloroethane-d4 (S)88 %06/04/17 12:55 17060-07-070-130 1
Toluene-d8 (S)123 %06/04/17 12:55 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Sample:SW-A Lab ID:92342730007 Collected:06/01/17 12:10 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 12.2J ug/L 06/04/17 14:24 67-64-110010.0 1
Acrylonitrile ND ug/L 06/04/17 14:24 107-13-12001.9 1
Benzene ND ug/L 06/04/17 14:24 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 14:24 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 14:24 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 14:24 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 14:24 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 14:24 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 14:24 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 14:24 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/17 14:24 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 14:24 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 14:24 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/17 14:24 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 14:24 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 14:24 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 14:24 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 14:24 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 14:24 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/04/17 14:24 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 14:24 110-57-6 L11001.0 1
1,1-Dichloroethane ND ug/L 06/04/17 14:24 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 14:24 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 14:24 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/17 14:24 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 14:24 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 14:24 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 06/04/17 14:24 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 14:24 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 14:24 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/04/17 14:24 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 14:24 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/04/17 14:24 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 14:24 108-10-11000.33 1
Styrene ND ug/L 06/04/17 14:24 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 14:24 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 14:24 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 14:24 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 14:24 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/04/17 14:24 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 14:24 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 14:24 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 14:24 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 14:24 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 14:24 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 14:24 75-01-41.0 0.62 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Sample:SW-A Lab ID:92342730007 Collected:06/01/17 12:10 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Xylene (Total)ND ug/L 06/04/17 14:24 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)105 %06/04/17 14:24 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %06/04/17 14:24 17060-07-070-130 1
Toluene-d8 (S)104 %06/04/17 14:24 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Sample:SW-B Lab ID:92342730008 Collected:06/01/17 12:30 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/04/17 14:42 67-64-110010.0 1
Acrylonitrile ND ug/L 06/04/17 14:42 107-13-12001.9 1
Benzene ND ug/L 06/04/17 14:42 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 14:42 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 14:42 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 14:42 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 14:42 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 14:42 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 14:42 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 14:42 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/17 14:42 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 14:42 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 14:42 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/17 14:42 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 14:42 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 14:42 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 14:42 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 14:42 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 14:42 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/04/17 14:42 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 14:42 110-57-6 L11001.0 1
1,1-Dichloroethane ND ug/L 06/04/17 14:42 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 14:42 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 14:42 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/17 14:42 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 14:42 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 14:42 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 06/04/17 14:42 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 14:42 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 14:42 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/04/17 14:42 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 14:42 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/04/17 14:42 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 14:42 108-10-11000.33 1
Styrene ND ug/L 06/04/17 14:42 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 14:42 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 14:42 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 14:42 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 14:42 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/04/17 14:42 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 14:42 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 14:42 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 14:42 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 14:42 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 14:42 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 14:42 75-01-41.0 0.62 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Sample:SW-B Lab ID:92342730008 Collected:06/01/17 12:30 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Xylene (Total)ND ug/L 06/04/17 14:42 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %06/04/17 14:42 460-00-470-130 1
1,2-Dichloroethane-d4 (S)87 %06/04/17 14:42 17060-07-070-130 1
Toluene-d8 (S)108 %06/04/17 14:42 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363146
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92342549001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2013277
Associated Lab Samples:92342549001
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 5.0 06/09/17 20:333.9
Arsenic ug/L ND 10.0 06/09/17 20:335.0
Barium ug/L ND 5.0 06/09/17 20:332.5
Beryllium ug/L ND 1.0 06/09/17 20:330.50
Cadmium ug/L ND 1.0 06/09/17 20:330.50
Chromium ug/L ND 5.0 06/10/17 16:232.5
Cobalt ug/L ND 5.0 06/09/17 20:332.5
Copper ug/L ND 5.0 06/09/17 20:332.5
Lead ug/L ND 5.0 06/09/17 20:332.5
Nickel ug/L ND 5.0 06/10/17 16:232.5
Selenium ug/L ND 10.0 06/09/17 20:335.0
Silver ug/L ND 5.0 06/09/17 20:332.5
Vanadium ug/L ND 5.0 06/09/17 20:332.5
Zinc ug/L ND 10.0 06/09/17 20:335.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2013278LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 493500 99 80-120
Arsenic ug/L 474500 95 80-120
Barium ug/L 497500 99 80-120
Beryllium ug/L 497500 99 80-120
Cadmium ug/L 496500 99 80-120
Chromium ug/L 494500 99 80-120
Cobalt ug/L 494500 99 80-120
Copper ug/L 496500 99 80-120
Lead ug/L 489500 98 80-120
Nickel ug/L 485500 97 80-120
Selenium ug/L 495500 99 80-120
Silver ug/L 247250 99 80-120
Vanadium ug/L 484500 97 80-120
Zinc ug/L 496500 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2013279MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342472012
2013280
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 98 75-125101 2 20500ND491503
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2013279MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342472012
2013280
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L 500 94 75-12597 2 20500ND472483
Barium ug/L 500 98 75-125102 3 205000.091
mg/L 582 602
Beryllium ug/L 500 99 75-125102 3 20500ND494510
Cadmium ug/L 500 99 75-125101 2 20500ND495506
Chromium ug/L 500 99 75-125102 3 20500ND493508
Cobalt ug/L 500 98 75-125101 2 20500ND492503
Copper ug/L 500 99 75-125101 3 20500ND494508
Lead ug/L 500 97 75-12599 2 20500ND485496
Nickel ug/L 500 97 75-12599 2 205000.016
mg/L 500 510
Selenium ug/L 500 98 75-125101 3 20500ND490507
Silver ug/L 250 99 75-125101 2 20250ND247252
Vanadium ug/L 500 96 75-12599 3 20500ND482495
Zinc ug/L 500 98 75-125101 2 205000.066
mg/L 557 569
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363321
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92342730001, 92342730002, 92342730004, 92342730005, 92342730006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014222
Associated Lab Samples:92342730001, 92342730002, 92342730004, 92342730005, 92342730006
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 5.0 06/14/17 21:193.9
Arsenic ug/L ND 10.0 06/14/17 21:195.0
Barium ug/L ND 5.0 06/14/17 21:192.5
Beryllium ug/L ND 1.0 06/14/17 21:190.50
Cadmium ug/L ND 1.0 06/14/17 21:190.50
Chromium ug/L ND 5.0 06/14/17 21:192.5
Cobalt ug/L ND 5.0 06/14/17 21:192.5
Copper ug/L ND 5.0 06/14/17 21:192.5
Lead ug/L ND 5.0 06/14/17 21:192.5
Nickel ug/L ND 5.0 06/14/17 21:192.5
Selenium ug/L ND 10.0 06/14/17 21:195.0
Silver ug/L ND 5.0 06/14/17 21:192.5
Vanadium ug/L ND 5.0 06/14/17 21:192.5
Zinc ug/L ND 10.0 06/14/17 21:195.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014223LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 496500 99 80-120
Arsenic ug/L 475500 95 80-120
Barium ug/L 511500 102 80-120
Beryllium ug/L 457500 91 80-120
Cadmium ug/L 512500 102 80-120
Chromium ug/L 463500 93 80-120
Cobalt ug/L 498500 100 80-120
Copper ug/L 494500 99 80-120
Lead ug/L 486500 97 80-120
Nickel ug/L 463500 93 80-120
Selenium ug/L 501500 100 80-120
Silver ug/L 235250 94 80-120
Vanadium ug/L 456500 91 80-120
Zinc ug/L 472500 94 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014224MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342605016
2014225
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 103 75-125100 3 20500ND517501
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014224MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342605016
2014225
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L 500 100 75-12597 2 20500174672657
Barium ug/L 500 108 75-125104 3 205008.0 546 530
Beryllium ug/L 500 96 75-12594 2 205000.73J 481 471
Cadmium ug/L 500 108 75-125105 3 205001.7 540 524
Chromium ug/L 500 97 75-12594 3 20500ND486470
Cobalt ug/L 500 104 75-125100 3 2050075.0 594 577
Copper ug/L 500 104 75-125102 3 20500ND522509
Lead ug/L 500 100 75-12597 3 205004.4J 506 491
Nickel ug/L 500 96 75-12593 3 205003.2J 481 466
Selenium ug/L 500 102 75-125100 2 20500ND511501
Silver ug/L 250 99 75-12595 4 20250ND246238
Vanadium ug/L 500 96 75-12593 3 20500ND482466
Zinc ug/L 500 98 75-12595 3 205005.8J 495 479
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363478
EPA 3010A
EPA 6020B
6020 MET
Associated Lab Samples:92342549001, 92342730001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2015139
Associated Lab Samples:92342549001, 92342730001
Matrix:Water
AnalyzedMDL
Thallium ug/L ND 0.10 06/09/17 16:550.020
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2015140LABORATORY CONTROL SAMPLE:
LCSSpike
Thallium ug/L 90.8100 91 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015141MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342795001
2015142
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Thallium ug/L 100 92 75-12596 4 201000.090J 91.9 96.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363479
EPA 3010A
EPA 6020B
6020 MET
Associated Lab Samples:92342730002, 92342730004, 92342730005, 92342730006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2015143
Associated Lab Samples:92342730002, 92342730004, 92342730005, 92342730006
Matrix:Water
AnalyzedMDL
Thallium ug/L ND 0.10 06/09/17 20:050.020
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2015144LABORATORY CONTROL SAMPLE:
LCSSpike
Thallium ug/L 93.7100 94 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015145MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342730002
2015146
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Thallium ug/L 100 94 75-12595 0 201000.048J 94.4 94.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363307
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92342549001, 92342730001, 92342730002, 92342730004, 92342730005, 92342730006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014180
Associated Lab Samples:92342549001, 92342730001, 92342730002, 92342730004, 92342730005, 92342730006
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/04/17 06:410.33
1,1,1-Trichloroethane ug/L ND 1.0 06/04/17 06:410.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 06/04/17 06:410.40
1,1,2-Trichloroethane ug/L ND 1.0 06/04/17 06:410.29
1,1-Dichloroethane ug/L ND 5.0 06/04/17 06:410.32
1,1-Dichloroethene ug/L ND 5.0 06/04/17 06:410.56
1,2,3-Trichloropropane ug/L ND 1.0 06/04/17 06:410.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 06/04/17 06:412.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/04/17 06:410.27
1,2-Dichlorobenzene ug/L ND 5.0 06/04/17 06:410.30
1,2-Dichloroethane ug/L ND 1.0 06/04/17 06:410.24
1,2-Dichloropropane ug/L ND 1.0 06/04/17 06:410.27
1,4-Dichlorobenzene ug/L ND 1.0 06/04/17 06:410.33
2-Butanone (MEK)ug/L ND 100 06/04/17 06:410.96
2-Hexanone ug/L ND 50.0 06/04/17 06:410.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 06/04/17 06:410.33
Acetone ug/L ND 100 06/04/17 06:4110.0
Acrylonitrile ug/L ND 200 06/04/17 06:411.9
Benzene ug/L ND 1.0 06/04/17 06:410.25
Bromochloromethane ug/L ND 3.0 06/04/17 06:410.17
Bromodichloromethane ug/L ND 1.0 06/04/17 06:410.18
Bromoform ug/L ND 3.0 06/04/17 06:410.26
Bromomethane ug/L ND 10.0 06/04/17 06:410.29
Carbon disulfide ug/L ND 100 06/04/17 06:411.2
Carbon tetrachloride ug/L ND 1.0 06/04/17 06:410.25
Chlorobenzene ug/L ND 3.0 06/04/17 06:410.23
Chloroethane ug/L ND 10.0 06/04/17 06:410.54
Chloroform ug/L ND 5.0 06/04/17 06:410.14
Chloromethane ug/L ND 1.0 06/04/17 06:410.11
cis-1,2-Dichloroethene ug/L ND 5.0 06/04/17 06:410.19
cis-1,3-Dichloropropene ug/L ND 1.0 06/04/17 06:410.13
Dibromochloromethane ug/L ND 3.0 06/04/17 06:410.21
Dibromomethane ug/L ND 10.0 06/04/17 06:410.21
Ethylbenzene ug/L ND 1.0 06/04/17 06:410.30
Iodomethane ug/L ND 10.0 06/04/17 06:410.32
Methylene Chloride ug/L ND 1.0 06/04/17 06:410.97
Styrene ug/L ND 1.0 06/04/17 06:410.26
Tetrachloroethene ug/L ND 1.0 06/04/17 06:410.46
Toluene ug/L ND 1.0 06/04/17 06:410.26
trans-1,2-Dichloroethene ug/L ND 5.0 06/04/17 06:410.49
trans-1,3-Dichloropropene ug/L ND 1.0 06/04/17 06:410.26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014180
Associated Lab Samples:92342549001, 92342730001, 92342730002, 92342730004, 92342730005, 92342730006
Matrix:Water
AnalyzedMDL
trans-1,4-Dichloro-2-butene ug/L ND 100 06/04/17 06:411.0
Trichloroethene ug/L ND 1.0 06/04/17 06:410.47
Trichlorofluoromethane ug/L ND 1.0 06/04/17 06:410.20
Vinyl acetate ug/L ND 50.0 06/04/17 06:410.35
Vinyl chloride ug/L ND 1.0 06/04/17 06:410.62
Xylene (Total)ug/L ND 5.0 06/04/17 06:410.66
1,2-Dichloroethane-d4 (S)%89 70-130 06/04/17 06:41
4-Bromofluorobenzene (S)%113 70-130 06/04/17 06:41
Toluene-d8 (S)%106 70-130 06/04/17 06:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014181LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.150 100 80-125
1,1,1-Trichloroethane ug/L 48.850 98 71-129
1,1,2,2-Tetrachloroethane ug/L 57.050 114 79-124
1,1,2-Trichloroethane ug/L 51.150 102 85-125
1,1-Dichloroethane ug/L 49.950 100 73-126
1,1-Dichloroethene ug/L 44.750 89 66-135
1,2,3-Trichloropropane ug/L 47.350 95 75-130
1,2-Dibromo-3-chloropropane ug/L 48.750 97 71-133
1,2-Dibromoethane (EDB)ug/L 56.350 113 83-124
1,2-Dichlorobenzene ug/L 50.950 102 80-133
1,2-Dichloroethane ug/L 45.750 91 67-128
1,2-Dichloropropane ug/L 54.450 109 75-132
1,4-Dichlorobenzene ug/L 47.750 95 78-130
2-Butanone (MEK)ug/L 136100 136 61-144
2-Hexanone ug/L 110100 110 68-143
4-Methyl-2-pentanone (MIBK)ug/L 109100 109 72-135
Acetone ug/L 116100 116 48-146
Acrylonitrile ug/L 274250 110 40-160
Benzene ug/L 52.550 105 80-125
Bromochloromethane ug/L 47.850 96 71-125
Bromodichloromethane ug/L 49.350 99 78-124
Bromoform ug/L 48.150 96 71-128
Bromomethane ug/L 41.950 84 40-160
Carbon disulfide ug/L 50.8J50 102 50-160
Carbon tetrachloride ug/L 44.550 89 69-131
Chlorobenzene ug/L 51.450 103 81-122
Chloroethane ug/L 43.750 87 39-148
Chloroform ug/L 48.350 97 73-127
Chloromethane ug/L 53.850 108 44-146
cis-1,2-Dichloroethene ug/L 51.050 102 74-124
cis-1,3-Dichloropropene ug/L 53.850 108 72-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014181LABORATORY CONTROL SAMPLE:
LCSSpike
Dibromochloromethane ug/L 47.750 95 78-125
Dibromomethane ug/L 48.550 97 82-120
Ethylbenzene ug/L 50.350 101 79-121
Iodomethane ug/L 95.3100 95 39-154
Methylene Chloride ug/L 49.950 100 64-133
Styrene ug/L 49.750 99 84-126
Tetrachloroethene ug/L 45.950 92 78-122
Toluene ug/L 49.650 99 80-121
trans-1,2-Dichloroethene ug/L 51.450 103 71-127
trans-1,3-Dichloropropene ug/L 53.350 107 69-141
trans-1,4-Dichloro-2-butene ug/L 94.0J L15018840-160
Trichloroethene ug/L 50.650 101 78-122
Trichlorofluoromethane ug/L 45.050 90 53-137
Vinyl acetate ug/L 96.4100 96 40-160
Vinyl chloride ug/L 45.150 90 58-137
Xylene (Total)ug/L 141150 94 81-126
1,2-Dichloroethane-d4 (S)%90 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2014183MATRIX SPIKE SAMPLE:
MSSpike
Result
92342730006
1,1,1,2-Tetrachloroethane ug/L 19.120 96 70-130ND
1,1,1-Trichloroethane ug/L 22.520 112 70-130ND
1,1,2,2-Tetrachloroethane ug/L 22.020 110 70-130ND
1,1,2-Trichloroethane ug/L 20.120 100 70-130ND
1,1-Dichloroethane ug/L 22.320 112 70-130ND
1,1-Dichloroethene ug/L 23.020 115 70-166ND
1,2,3-Trichloropropane ug/L 18.120 90 70-130ND
1,2-Dibromo-3-chloropropane ug/L 18.920 94 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.120 106 70-130ND
1,2-Dichlorobenzene ug/L 21.220 106 70-130ND
1,2-Dichloroethane ug/L 20.320 101 70-130ND
1,2-Dichloropropane ug/L 22.920 115 70-130ND
1,4-Dichlorobenzene ug/L 20.220 101 70-130ND
2-Butanone (MEK)ug/L 46.6J40 116 70-130ND
2-Hexanone ug/L 44.9J40 112 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 42.0J40 105 70-130ND
Acetone ug/L 49.1J40 94 70-13011.6J
Acrylonitrile ug/L 113J100 113 70-130ND
Benzene ug/L 23.220 116 70-148ND
Bromochloromethane ug/L 20.920 105 70-130ND
Bromodichloromethane ug/L 21.320 106 70-130ND
Bromoform ug/L 17.320 86 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2014183MATRIX SPIKE SAMPLE:
MSSpike
Result
92342730006
Bromomethane ug/L 22.420 112 70-130ND
Carbon disulfide ug/L 23.6J20 118 70-130ND
Carbon tetrachloride ug/L 21.020 105 70-130ND
Chlorobenzene ug/L 22.020 110 70-146ND
Chloroethane ug/L 20.920 104 70-130ND
Chloroform ug/L 22.820 114 70-130ND
Chloromethane ug/L 24.620 123 70-130ND
cis-1,2-Dichloroethene ug/L 22.820 114 70-130ND
cis-1,3-Dichloropropene ug/L 22.420 112 70-130ND
Dibromochloromethane ug/L 19.520 98 70-130ND
Dibromomethane ug/L 21.820 109 70-130ND
Ethylbenzene ug/L 22.320 112 70-130ND
Iodomethane ug/L 41.240 103 70-130ND
Methylene Chloride ug/L 21.820 109 70-130ND
Styrene ug/L 20.920 104 70-130ND
Tetrachloroethene ug/L 20.820 104 70-130ND
Toluene ug/L 22.520 113 70-155ND
trans-1,2-Dichloroethene ug/L 23.920 119 70-130ND
trans-1,3-Dichloropropene ug/L 22.720 114 70-130ND
trans-1,4-Dichloro-2-butene ug/L 28.2J M02014170-130ND
Trichloroethene ug/L 22.520 112 69-151ND
Trichlorofluoromethane ug/L 21.720 109 70-130ND
Vinyl acetate ug/L 40.5J40 101 70-130ND
Vinyl chloride ug/L 21.220 106 70-130ND
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%104 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342730005
2014182SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342730005
2014182SAMPLE DUPLICATE:
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L 13.6J 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L 0.16J 300.13J
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%87 692
4-Bromofluorobenzene (S)%100 2102
Toluene-d8 (S)%108 1109
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363311
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92342730007, 92342730008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014186
Associated Lab Samples:92342730007, 92342730008
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/04/17 06:590.33
1,1,1-Trichloroethane ug/L ND 1.0 06/04/17 06:590.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 06/04/17 06:590.40
1,1,2-Trichloroethane ug/L ND 1.0 06/04/17 06:590.29
1,1-Dichloroethane ug/L ND 5.0 06/04/17 06:590.32
1,1-Dichloroethene ug/L ND 5.0 06/04/17 06:590.56
1,2,3-Trichloropropane ug/L ND 1.0 06/04/17 06:590.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 06/04/17 06:592.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/04/17 06:590.27
1,2-Dichlorobenzene ug/L ND 5.0 06/04/17 06:590.30
1,2-Dichloroethane ug/L ND 1.0 06/04/17 06:590.24
1,2-Dichloropropane ug/L ND 1.0 06/04/17 06:590.27
1,4-Dichlorobenzene ug/L ND 1.0 06/04/17 06:590.33
2-Butanone (MEK)ug/L ND 100 06/04/17 06:590.96
2-Hexanone ug/L ND 50.0 06/04/17 06:590.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 06/04/17 06:590.33
Acetone ug/L ND 100 06/04/17 06:5910.0
Acrylonitrile ug/L ND 200 06/04/17 06:591.9
Benzene ug/L ND 1.0 06/04/17 06:590.25
Bromochloromethane ug/L ND 3.0 06/04/17 06:590.17
Bromodichloromethane ug/L ND 1.0 06/04/17 06:590.18
Bromoform ug/L ND 3.0 06/04/17 06:590.26
Bromomethane ug/L ND 10.0 06/04/17 06:590.29
Carbon disulfide ug/L ND 100 06/04/17 06:591.2
Carbon tetrachloride ug/L ND 1.0 06/04/17 06:590.25
Chlorobenzene ug/L ND 3.0 06/04/17 06:590.23
Chloroethane ug/L ND 10.0 06/04/17 06:590.54
Chloroform ug/L ND 5.0 06/04/17 06:590.14
Chloromethane ug/L ND 1.0 06/04/17 06:590.11
cis-1,2-Dichloroethene ug/L ND 5.0 06/04/17 06:590.19
cis-1,3-Dichloropropene ug/L ND 1.0 06/04/17 06:590.13
Dibromochloromethane ug/L ND 3.0 06/04/17 06:590.21
Dibromomethane ug/L ND 10.0 06/04/17 06:590.21
Ethylbenzene ug/L ND 1.0 06/04/17 06:590.30
Iodomethane ug/L ND 10.0 06/04/17 06:590.32
Methylene Chloride ug/L ND 1.0 06/04/17 06:590.97
Styrene ug/L ND 1.0 06/04/17 06:590.26
Tetrachloroethene ug/L ND 1.0 06/04/17 06:590.46
Toluene ug/L ND 1.0 06/04/17 06:590.26
trans-1,2-Dichloroethene ug/L ND 5.0 06/04/17 06:590.49
trans-1,3-Dichloropropene ug/L ND 1.0 06/04/17 06:590.26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014186
Associated Lab Samples:92342730007, 92342730008
Matrix:Water
AnalyzedMDL
trans-1,4-Dichloro-2-butene ug/L ND 100 06/04/17 06:591.0
Trichloroethene ug/L ND 1.0 06/04/17 06:590.47
Trichlorofluoromethane ug/L ND 1.0 06/04/17 06:590.20
Vinyl acetate ug/L ND 50.0 06/04/17 06:590.35
Vinyl chloride ug/L ND 1.0 06/04/17 06:590.62
Xylene (Total)ug/L ND 5.0 06/04/17 06:590.66
1,2-Dichloroethane-d4 (S)%89 70-130 06/04/17 06:59
4-Bromofluorobenzene (S)%99 70-130 06/04/17 06:59
Toluene-d8 (S)%106 70-130 06/04/17 06:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014187LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.750 99 80-125
1,1,1-Trichloroethane ug/L 50.850 102 71-129
1,1,2,2-Tetrachloroethane ug/L 53.150 106 79-124
1,1,2-Trichloroethane ug/L 51.550 103 85-125
1,1-Dichloroethane ug/L 52.350 105 73-126
1,1-Dichloroethene ug/L 51.650 103 66-135
1,2,3-Trichloropropane ug/L 47.050 94 75-130
1,2-Dibromo-3-chloropropane ug/L 47.350 95 71-133
1,2-Dibromoethane (EDB)ug/L 54.150 108 83-124
1,2-Dichlorobenzene ug/L 48.250 96 80-133
1,2-Dichloroethane ug/L 48.450 97 67-128
1,2-Dichloropropane ug/L 52.750 105 75-132
1,4-Dichlorobenzene ug/L 45.650 91 78-130
2-Butanone (MEK)ug/L 138100 138 61-144
2-Hexanone ug/L 108100 108 68-143
4-Methyl-2-pentanone (MIBK)ug/L 107100 107 72-135
Acetone ug/L 123100 123 48-146
Acrylonitrile ug/L 286250 114 40-160
Benzene ug/L 52.550 105 80-125
Bromochloromethane ug/L 48.350 97 71-125
Bromodichloromethane ug/L 48.550 97 78-124
Bromoform ug/L 48.550 97 71-128
Bromomethane ug/L 44.850 90 40-160
Carbon disulfide ug/L 52.8J50 106 50-160
Carbon tetrachloride ug/L 44.250 88 69-131
Chlorobenzene ug/L 49.950 100 81-122
Chloroethane ug/L 43.650 87 39-148
Chloroform ug/L 52.250 104 73-127
Chloromethane ug/L 58.150 116 44-146
cis-1,2-Dichloroethene ug/L 54.050 108 74-124
cis-1,3-Dichloropropene ug/L 52.450 105 72-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014187LABORATORY CONTROL SAMPLE:
LCSSpike
Dibromochloromethane ug/L 48.750 97 78-125
Dibromomethane ug/L 46.050 92 82-120
Ethylbenzene ug/L 48.050 96 79-121
Iodomethane ug/L 95.1100 95 39-154
Methylene Chloride ug/L 53.350 107 64-133
Styrene ug/L 48.350 97 84-126
Tetrachloroethene ug/L 47.950 96 78-122
Toluene ug/L 48.350 97 80-121
trans-1,2-Dichloroethene ug/L 53.850 108 71-127
trans-1,3-Dichloropropene ug/L 51.450 103 69-141
trans-1,4-Dichloro-2-butene ug/L 99.7J L15019940-160
Trichloroethene ug/L 49.550 99 78-122
Trichlorofluoromethane ug/L 46.550 93 53-137
Vinyl acetate ug/L 103100 103 40-160
Vinyl chloride ug/L 46.950 94 58-137
Xylene (Total)ug/L 141150 94 81-126
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%95 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2014189MATRIX SPIKE SAMPLE:
MSSpike
Result
92342784004
1,1,1,2-Tetrachloroethane ug/L 19.220 96 70-130ND
1,1,1-Trichloroethane ug/L 22.820 114 70-130ND
1,1,2,2-Tetrachloroethane ug/L 21.320 106 70-130ND
1,1,2-Trichloroethane ug/L 21.120 105 70-130ND
1,1-Dichloroethane ug/L 24.120 120 70-130ND
1,1-Dichloroethene ug/L 24.120 120 70-166ND
1,2,3-Trichloropropane ug/L 20.320 102 70-130ND
1,2-Dibromo-3-chloropropane ug/L 19.720 99 70-130ND
1,2-Dibromoethane (EDB)ug/L 20.620 103 70-130ND
1,2-Dichlorobenzene ug/L 22.020 110 70-130ND
1,2-Dichloroethane ug/L 20.720 104 70-130ND
1,2-Dichloropropane ug/L 22.820 114 70-130ND
1,4-Dichlorobenzene ug/L 21.820 109 70-130ND
2-Butanone (MEK)ug/L 46.8J40 117 70-130ND
2-Hexanone ug/L 41.2J40 103 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 42.3J40 106 70-130ND
Acetone ug/L 49.1J40 90 70-13012.9J
Acrylonitrile ug/L 111J100 111 70-130ND
Benzene ug/L 23.720 119 70-148ND
Bromochloromethane ug/L 21.920 109 70-130ND
Bromodichloromethane ug/L 22.420 112 70-130ND
Bromoform ug/L 17.720 88 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
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Page 34 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2014189MATRIX SPIKE SAMPLE:
MSSpike
Result
92342784004
Bromomethane ug/L 23.220 116 70-130ND
Carbon disulfide ug/L 24.5J20 123 70-130ND
Carbon tetrachloride ug/L 21.220 106 70-130ND
Chlorobenzene ug/L 22.520 112 70-146ND
Chloroethane ug/L 18.920 94 70-130ND
Chloroform ug/L 22.320 111 70-130ND
Chloromethane ug/L 24.420 121 70-1300.14J
cis-1,2-Dichloroethene ug/L 24.820 123 70-1300.22J
cis-1,3-Dichloropropene ug/L 22.520 113 70-130ND
Dibromochloromethane ug/L 19.220 96 70-130ND
Dibromomethane ug/L 21.320 107 70-130ND
Ethylbenzene ug/L 22.220 111 70-130ND
Iodomethane ug/L 44.240 110 70-130ND
Methylene Chloride ug/L 22.620 113 70-130ND
Styrene ug/L 21.320 107 70-130ND
Tetrachloroethene ug/L 20.720 103 70-130ND
Toluene ug/L 22.220 111 70-155ND
trans-1,2-Dichloroethene ug/L 23.720 118 70-130ND
trans-1,3-Dichloropropene ug/L 22.020 110 70-130ND
trans-1,4-Dichloro-2-butene ug/L 24.7J20 124 70-130ND
Trichloroethene ug/L 23.520 117 69-151ND
Trichlorofluoromethane ug/L 22.520 112 70-130ND
Vinyl acetate ug/L 38.6J40 96 70-130ND
Vinyl chloride ug/L 21.520 107 70-130ND
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%94 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342784003
2014188SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 0.35J 300.37J
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L 0.86J 30ND
1,4-Dichlorobenzene ug/L 2.4 5 302.5
2-Butanone (MEK)ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
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Page 35 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342784003
2014188SAMPLE DUPLICATE:
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L 13.9J 3021.4J
Acrylonitrile ug/L ND 30ND
Benzene ug/L 0.52J 300.62J
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L 0.97J 300.87J
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L 0.11J 30ND
cis-1,2-Dichloroethene ug/L 1.0J 3 301.0J
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L 0.91J 300.88J
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%90 090
4-Bromofluorobenzene (S)%98 299
Toluene-d8 (S)%105 3108
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
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[phone]
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
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Page 37 of 44
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92342549001 363146 364135SW-3 EPA 3010A EPA 6010
92342730001 363321 364621SW-1 EPA 3010A EPA 6010
92342730002 363321 364621SW-2 EPA 3010A EPA 6010
92342730004 363321 364621SW-4 EPA 3010A EPA 6010
92342730005 363321 364621SWN-1 EPA 3010A EPA 6010
92342730006 363321 364621SWN-2 EPA 3010A EPA 6010
92342549001 363478 363771SW-3 EPA 3010A EPA 6020B
92342730001 363478 363771SW-1 EPA 3010A EPA 6020B
92342730002 363479 363773SW-2 EPA 3010A EPA 6020B
92342730004 363479 363773SW-4 EPA 3010A EPA 6020B
92342730005 363479 363773SWN-1 EPA 3010A EPA 6020B
92342730006 363479 363773SWN-2 EPA 3010A EPA 6020B
92342549001 363307SW-3 EPA 8260
92342730001 363307SW-1 EPA 8260
92342730002 363307SW-2 EPA 8260
92342730004 363307SW-4 EPA 8260
92342730005 363307SWN-1 EPA 8260
92342730006 363307SWN-2 EPA 8260
92342730007 363311SW-A EPA 8260
92342730008 363311SW-B EPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
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[phone]
Page 38 of 44
Page 39 of 44
Page 40 of 44
Page 41 of 44
Page 42 of 44
Page 43 of 44
Page 44 of 44
#=CL#
June 15, 2017
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92342727
92342727
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
SURRY BANKS
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on June 02, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 1 of 28
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92342727
SURRY BANKS
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 2 of 28
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92342727
SURRY BANKS
Lab ID Sample ID Matrix Date Collected Date Received
92342727001 EB Water 06/01/17 18:00 06/02/17 08:00
92342727002 FB Water 06/01/17 17:55 06/02/17 08:00
92342727003 TB Water 06/01/17 00:00 06/02/17 08:00
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 3 of 28
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92342727
SURRY BANKS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92342727001 EB EPA 6010 15 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AWAB
EPA 8260 67 PASI-CGAW
SM 4500-CN-E 1 PASI-AAES2
92342727002 FB EPA 6010 15 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AWAB
EPA 8260 67 PASI-CGAW
92342727003 TB EPA 8260 67 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 4 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342727
SURRY BANKS
Sample:EB Lab ID:92342727001 Collected:06/01/17 18:00 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/14/17 21:59 7440-36-006/04/17 16:406.0 3.9 1
Arsenic ND ug/L 06/14/17 21:59 7440-38-206/04/17 16:4010.0 5.0 1
Barium ND ug/L 06/14/17 21:59 7440-39-306/04/17 16:401002.5 1
Beryllium ND ug/L 06/14/17 21:59 7440-41-706/04/17 16:401.0 0.50 1
Cadmium ND ug/L 06/14/17 21:59 7440-43-906/04/17 16:401.0 0.50 1
Chromium ND ug/L 06/14/17 21:59 7440-47-306/04/17 16:4010.0 2.5 1
Cobalt ND ug/L 06/14/17 21:59 7440-48-406/04/17 16:4010.0 2.5 1
Copper ND ug/L 06/14/17 21:59 7440-50-806/04/17 16:4010.0 2.5 1
Lead ND ug/L 06/14/17 21:59 7439-92-106/04/17 16:4010.0 2.5 1
Nickel ND ug/L 06/14/17 21:59 7440-02-006/04/17 16:4050.0 2.5 1
Selenium ND ug/L 06/14/17 21:59 7782-49-206/04/17 16:4010.0 5.0 1
Silver ND ug/L 06/14/17 21:59 7440-22-406/04/17 16:4010.0 2.5 1
Tin ND ug/L 06/14/17 21:59 7440-31-506/04/17 16:401002.5 1
Vanadium ND ug/L 06/14/17 21:59 7440-62-206/04/17 16:4025.0 2.5 1
Zinc ND ug/L 06/14/17 21:59 7440-66-606/04/17 16:4010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/09/17 17:47 7440-28-006/06/17 02:455.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/06/17 09:42 7439-97-606/05/17 20:000.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 14.4J ug/L 06/04/17 21:12 67-64-110010.0 1
Acetonitrile ND ug/L 06/04/17 21:12 75-05-855.0 2.2 1
Acrolein ND ug/L 06/04/17 21:12 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 06/04/17 21:12 107-13-12001.9 1
Allyl chloride ND ug/L 06/04/17 21:12 107-05-110.0 1.5 1
Benzene ND ug/L 06/04/17 21:12 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 21:12 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 21:12 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 21:12 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 21:12 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 21:12 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 21:12 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 21:12 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/17 21:12 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 21:12 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 21:12 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/17 21:12 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/04/17 21:12 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 21:12 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 21:12 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 21:12 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 21:12 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 21:12 95-50-15.0 0.30 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
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Page 5 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342727
SURRY BANKS
Sample:EB Lab ID:92342727001 Collected:06/01/17 18:00 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,3-Dichlorobenzene ND ug/L 06/04/17 21:12 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/04/17 21:12 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 21:12 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/04/17 21:12 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/04/17 21:12 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 21:12 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 21:12 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/17 21:12 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 21:12 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 21:12 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/04/17 21:12 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/04/17 21:12 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/04/17 21:12 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/04/17 21:12 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 21:12 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 21:12 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/04/17 21:12 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/04/17 21:12 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/04/17 21:12 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 21:12 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/04/17 21:12 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/04/17 21:12 126-98-71000.93 1
Methylene Chloride ND ug/L 06/04/17 21:12 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/04/17 21:12 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 21:12 108-10-11000.33 1
Naphthalene ND ug/L 06/04/17 21:12 91-20-310.0 0.24 1
Propionitrile ND ug/L 06/04/17 21:12 107-12-01503.6 1
Styrene ND ug/L 06/04/17 21:12 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 21:12 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 21:12 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 21:12 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 21:12 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/04/17 21:12 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/04/17 21:12 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 21:12 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 21:12 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 21:12 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 21:12 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 21:12 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 21:12 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/17 21:12 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)109 %06/04/17 21:12 460-00-470-130 1
1,2-Dichloroethane-d4 (S)87 %06/04/17 21:12 17060-07-070-130 1
Toluene-d8 (S)106 %06/04/17 21:12 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
Pace Analytical Services, LLC
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[phone]
Page 6 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342727
SURRY BANKS
Sample:EB Lab ID:92342727001 Collected:06/01/17 18:00 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/07/17 13:50 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
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[phone]
Page 7 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342727
SURRY BANKS
Sample:FB Lab ID:92342727002 Collected:06/01/17 17:55 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/14/17 22:03 7440-36-006/04/17 16:406.0 3.9 1
Arsenic ND ug/L 06/14/17 22:03 7440-38-206/04/17 16:4010.0 5.0 1
Barium ND ug/L 06/14/17 22:03 7440-39-306/04/17 16:401002.5 1
Beryllium ND ug/L 06/14/17 22:03 7440-41-706/04/17 16:401.0 0.50 1
Cadmium ND ug/L 06/14/17 22:03 7440-43-906/04/17 16:401.0 0.50 1
Chromium ND ug/L 06/14/17 22:03 7440-47-306/04/17 16:4010.0 2.5 1
Cobalt ND ug/L 06/14/17 22:03 7440-48-406/04/17 16:4010.0 2.5 1
Copper ND ug/L 06/14/17 22:03 7440-50-806/04/17 16:4010.0 2.5 1
Lead ND ug/L 06/14/17 22:03 7439-92-106/04/17 16:4010.0 2.5 1
Nickel ND ug/L 06/14/17 22:03 7440-02-006/04/17 16:4050.0 2.5 1
Selenium ND ug/L 06/14/17 22:03 7782-49-206/04/17 16:4010.0 5.0 1
Silver ND ug/L 06/14/17 22:03 7440-22-406/04/17 16:4010.0 2.5 1
Tin ND ug/L 06/14/17 22:03 7440-31-506/04/17 16:401002.5 1
Vanadium ND ug/L 06/14/17 22:03 7440-62-206/04/17 16:4025.0 2.5 1
Zinc ND ug/L 06/14/17 22:03 7440-66-606/04/17 16:4010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/09/17 17:49 7440-28-006/06/17 02:455.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/06/17 09:45 7439-97-606/05/17 20:000.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 10.2J ug/L 06/04/17 21:30 67-64-110010.0 1
Acetonitrile ND ug/L 06/04/17 21:30 75-05-855.0 2.2 1
Acrolein ND ug/L 06/04/17 21:30 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 06/04/17 21:30 107-13-12001.9 1
Allyl chloride ND ug/L 06/04/17 21:30 107-05-110.0 1.5 1
Benzene ND ug/L 06/04/17 21:30 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 21:30 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 21:30 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 21:30 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 21:30 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 21:30 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 21:30 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 21:30 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/17 21:30 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 21:30 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 21:30 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/17 21:30 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/04/17 21:30 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 21:30 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 21:30 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 21:30 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 21:30 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 21:30 95-50-15.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
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Page 8 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342727
SURRY BANKS
Sample:FB Lab ID:92342727002 Collected:06/01/17 17:55 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,3-Dichlorobenzene ND ug/L 06/04/17 21:30 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/04/17 21:30 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 21:30 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/04/17 21:30 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/04/17 21:30 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 21:30 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 21:30 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/17 21:30 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 21:30 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 21:30 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/04/17 21:30 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/04/17 21:30 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/04/17 21:30 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/04/17 21:30 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 21:30 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 21:30 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/04/17 21:30 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/04/17 21:30 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/04/17 21:30 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 21:30 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/04/17 21:30 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/04/17 21:30 126-98-71000.93 1
Methylene Chloride ND ug/L 06/04/17 21:30 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/04/17 21:30 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 21:30 108-10-11000.33 1
Naphthalene ND ug/L 06/04/17 21:30 91-20-310.0 0.24 1
Propionitrile ND ug/L 06/04/17 21:30 107-12-01503.6 1
Styrene ND ug/L 06/04/17 21:30 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 21:30 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 21:30 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 21:30 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 21:30 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/04/17 21:30 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/04/17 21:30 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 21:30 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 21:30 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 21:30 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 21:30 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 21:30 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 21:30 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/17 21:30 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %06/04/17 21:30 460-00-470-130 1
1,2-Dichloroethane-d4 (S)89 %06/04/17 21:30 17060-07-070-130 1
Toluene-d8 (S)106 %06/04/17 21:30 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
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Page 9 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342727
SURRY BANKS
Sample:TB Lab ID:92342727003 Collected:06/01/17 00:00 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/04/17 21:48 67-64-110010.0 1
Acetonitrile ND ug/L 06/04/17 21:48 75-05-855.0 2.2 1
Acrolein ND ug/L 06/04/17 21:48 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 06/04/17 21:48 107-13-12001.9 1
Allyl chloride ND ug/L 06/04/17 21:48 107-05-110.0 1.5 1
Benzene ND ug/L 06/04/17 21:48 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 21:48 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 21:48 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 21:48 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 21:48 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 21:48 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 21:48 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 21:48 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/17 21:48 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 21:48 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 21:48 67-66-35.0 0.14 1
Chloromethane 0.14J ug/L 06/04/17 21:48 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/04/17 21:48 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 21:48 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 21:48 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 21:48 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 21:48 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 21:48 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/04/17 21:48 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/04/17 21:48 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 21:48 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/04/17 21:48 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/04/17 21:48 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 21:48 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 21:48 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/17 21:48 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 21:48 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 21:48 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/04/17 21:48 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/04/17 21:48 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/04/17 21:48 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/04/17 21:48 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 21:48 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 21:48 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/04/17 21:48 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/04/17 21:48 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/04/17 21:48 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 21:48 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/04/17 21:48 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/04/17 21:48 126-98-71000.93 1
Methylene Chloride ND ug/L 06/04/17 21:48 75-09-21.0 0.97 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
Pace Analytical Services, LLC
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[phone]
Page 10 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342727
SURRY BANKS
Sample:TB Lab ID:92342727003 Collected:06/01/17 00:00 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Methyl methacrylate ND ug/L 06/04/17 21:48 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 21:48 108-10-11000.33 1
Naphthalene ND ug/L 06/04/17 21:48 91-20-310.0 0.24 1
Propionitrile ND ug/L 06/04/17 21:48 107-12-01503.6 1
Styrene ND ug/L 06/04/17 21:48 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 21:48 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 21:48 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 21:48 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 21:48 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/04/17 21:48 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/04/17 21:48 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 21:48 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 21:48 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 21:48 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 21:48 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 21:48 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 21:48 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/17 21:48 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %06/04/17 21:48 460-00-470-130 1
1,2-Dichloroethane-d4 (S)89 %06/04/17 21:48 17060-07-070-130 1
Toluene-d8 (S)107 %06/04/17 21:48 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 11 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342727
SURRY BANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363459
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92342727001, 92342727002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2015066
Associated Lab Samples:92342727001, 92342727002
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 06/06/17 09:310.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2015067LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.42.5 95 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015068MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342658001
2015069
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L M1,R12.5 93 75-12562 40 252.5ND 2.4 1.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342727
SURRY BANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363321
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92342727001, 92342727002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014222
Associated Lab Samples:92342727001, 92342727002
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 5.0 06/14/17 21:193.9
Arsenic ug/L ND 10.0 06/14/17 21:195.0
Barium ug/L ND 5.0 06/14/17 21:192.5
Beryllium ug/L ND 1.0 06/14/17 21:190.50
Cadmium ug/L ND 1.0 06/14/17 21:190.50
Chromium ug/L ND 5.0 06/14/17 21:192.5
Cobalt ug/L ND 5.0 06/14/17 21:192.5
Copper ug/L ND 5.0 06/14/17 21:192.5
Lead ug/L ND 5.0 06/14/17 21:192.5
Nickel ug/L ND 5.0 06/14/17 21:192.5
Selenium ug/L ND 10.0 06/14/17 21:195.0
Silver ug/L ND 5.0 06/14/17 21:192.5
Tin ug/L ND 5.0 06/14/17 21:192.5
Vanadium ug/L ND 5.0 06/14/17 21:192.5
Zinc ug/L ND 10.0 06/14/17 21:195.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014223LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 496500 99 80-120
Arsenic ug/L 475500 95 80-120
Barium ug/L 511500 102 80-120
Beryllium ug/L 457500 91 80-120
Cadmium ug/L 512500 102 80-120
Chromium ug/L 463500 93 80-120
Cobalt ug/L 498500 100 80-120
Copper ug/L 494500 99 80-120
Lead ug/L 486500 97 80-120
Nickel ug/L 463500 93 80-120
Selenium ug/L 501500 100 80-120
Silver ug/L 235250 94 80-120
Tin ug/L 485500 97 80-120
Vanadium ug/L 456500 91 80-120
Zinc ug/L 472500 94 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342727
SURRY BANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014224MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342605016
2014225
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 103 75-125100 3 20500ND517501
Arsenic ug/L 500 100 75-12597 2 20500174672657
Barium ug/L 500 108 75-125104 3 205008.0 546 530
Beryllium ug/L 500 96 75-12594 2 205000.73J 481 471
Cadmium ug/L 500 108 75-125105 3 205001.7 540 524
Chromium ug/L 500 97 75-12594 3 20500ND486470
Cobalt ug/L 500 104 75-125100 3 2050075.0 594 577
Copper ug/L 500 104 75-125102 3 20500ND522509
Lead ug/L 500 100 75-12597 3 205004.4J 506 491
Nickel ug/L 500 96 75-12593 3 205003.2J 481 466
Selenium ug/L 500 102 75-125100 2 20500ND511501
Silver ug/L 250 99 75-12595 4 20250ND246238
Tin ug/L 500 101 75-12597 4 20500ND503484
Vanadium ug/L 500 96 75-12593 3 20500ND482466
Zinc ug/L 500 98 75-12595 3 205005.8J 495 479
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342727
SURRY BANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363478
EPA 3010A
EPA 6020B
6020 MET
Associated Lab Samples:92342727001, 92342727002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2015139
Associated Lab Samples:92342727001, 92342727002
Matrix:Water
AnalyzedMDL
Thallium ug/L ND 0.10 06/09/17 16:550.020
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2015140LABORATORY CONTROL SAMPLE:
LCSSpike
Thallium ug/L 90.8100 91 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015141MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342795001
2015142
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Thallium ug/L 100 92 75-12596 4 201000.090J 91.9 96.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342727
SURRY BANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363328
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92342727001, 92342727002, 92342727003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014255
Associated Lab Samples:92342727001, 92342727002, 92342727003
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/04/17 20:010.33
1,1,1-Trichloroethane ug/L ND 1.0 06/04/17 20:010.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 06/04/17 20:010.40
1,1,2-Trichloroethane ug/L ND 1.0 06/04/17 20:010.29
1,1-Dichloroethane ug/L ND 5.0 06/04/17 20:010.32
1,1-Dichloroethene ug/L ND 5.0 06/04/17 20:010.56
1,1-Dichloropropene ug/L ND 5.0 06/04/17 20:010.49
1,2,3-Trichloropropane ug/L ND 1.0 06/04/17 20:010.41
1,2,4-Trichlorobenzene ug/L ND 10.0 06/04/17 20:010.35
1,2-Dibromo-3-chloropropane ug/L ND 13.0 06/04/17 20:012.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/04/17 20:010.27
1,2-Dichlorobenzene ug/L ND 5.0 06/04/17 20:010.30
1,2-Dichloroethane ug/L ND 1.0 06/04/17 20:010.24
1,2-Dichloropropane ug/L ND 1.0 06/04/17 20:010.27
1,3-Dichlorobenzene ug/L ND 5.0 06/04/17 20:010.24
1,3-Dichloropropane ug/L ND 1.0 06/04/17 20:010.28
1,4-Dichlorobenzene ug/L ND 1.0 06/04/17 20:010.33
2,2-Dichloropropane ug/L ND 15.0 06/04/17 20:010.13
2-Butanone (MEK)ug/L ND 100 06/04/17 20:010.96
2-Hexanone ug/L ND 50.0 06/04/17 20:010.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 06/04/17 20:010.33
Acetone ug/L ND 100 06/04/17 20:0110.0
Acetonitrile ug/L ND 55.0 06/04/17 20:012.2
Acrolein ug/L ND 53.0 06/04/17 20:011.6
Acrylonitrile ug/L ND 200 06/04/17 20:011.9
Allyl chloride ug/L ND 10.0 06/04/17 20:011.5
Benzene ug/L ND 1.0 06/04/17 20:010.25
Bromochloromethane ug/L ND 3.0 06/04/17 20:010.17
Bromodichloromethane ug/L ND 1.0 06/04/17 20:010.18
Bromoform ug/L ND 3.0 06/04/17 20:010.26
Bromomethane ug/L ND 10.0 06/04/17 20:010.29
Carbon disulfide ug/L ND 100 06/04/17 20:011.2
Carbon tetrachloride ug/L ND 1.0 06/04/17 20:010.25
Chlorobenzene ug/L ND 3.0 06/04/17 20:010.23
Chloroethane ug/L ND 10.0 06/04/17 20:010.54
Chloroform ug/L ND 5.0 06/04/17 20:010.14
Chloromethane ug/L ND 1.0 06/04/17 20:010.11
Chloroprene ug/L ND 20.0 06/04/17 20:010.27
cis-1,2-Dichloroethene ug/L ND 5.0 06/04/17 20:010.19
cis-1,3-Dichloropropene ug/L ND 1.0 06/04/17 20:010.13
Dibromochloromethane ug/L ND 3.0 06/04/17 20:010.21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342727
SURRY BANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014255
Associated Lab Samples:92342727001, 92342727002, 92342727003
Matrix:Water
AnalyzedMDL
Dibromomethane ug/L ND 10.0 06/04/17 20:010.21
Dichlorodifluoromethane ug/L ND 5.0 06/04/17 20:010.21
Ethyl methacrylate ug/L ND 10.0 06/04/17 20:010.20
Ethylbenzene ug/L ND 1.0 06/04/17 20:010.30
Hexachloro-1,3-butadiene ug/L ND 10.0 06/04/17 20:010.71
Iodomethane ug/L ND 10.0 06/04/17 20:010.32
Isobutanol ug/L ND 100 06/04/17 20:0135.0
Methacrylonitrile ug/L ND 100 06/04/17 20:010.93
Methyl methacrylate ug/L ND 30.0 06/04/17 20:012.0
Methylene Chloride ug/L ND 1.0 06/04/17 20:010.97
Naphthalene ug/L ND 10.0 06/04/17 20:010.24
Propionitrile ug/L ND 150 06/04/17 20:013.6
Styrene ug/L ND 1.0 06/04/17 20:010.26
Tetrachloroethene ug/L ND 1.0 06/04/17 20:010.46
Toluene ug/L ND 1.0 06/04/17 20:010.26
trans-1,2-Dichloroethene ug/L ND 5.0 06/04/17 20:010.49
trans-1,3-Dichloropropene ug/L ND 1.0 06/04/17 20:010.26
trans-1,4-Dichloro-2-butene ug/L ND 100 06/04/17 20:011.0
Trichloroethene ug/L ND 1.0 06/04/17 20:010.47
Trichlorofluoromethane ug/L ND 1.0 06/04/17 20:010.20
Vinyl acetate ug/L ND 50.0 06/04/17 20:010.35
Vinyl chloride ug/L ND 1.0 06/04/17 20:010.62
Xylene (Total)ug/L ND 5.0 06/04/17 20:010.66
1,2-Dichloroethane-d4 (S)%85 70-130 06/04/17 20:01
4-Bromofluorobenzene (S)%100 70-130 06/04/17 20:01
Toluene-d8 (S)%115 70-130 06/04/17 20:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014256LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 46.650 93 80-125
1,1,1-Trichloroethane ug/L 50.750 101 71-129
1,1,2,2-Tetrachloroethane ug/L 49.850 100 79-124
1,1,2-Trichloroethane ug/L 48.950 98 85-125
1,1-Dichloroethane ug/L 49.650 99 73-126
1,1-Dichloroethene ug/L 46.950 94 66-135
1,1-Dichloropropene ug/L 51.950 104 74-135
1,2,3-Trichloropropane ug/L 46.550 93 75-130
1,2,4-Trichlorobenzene ug/L 46.550 93 75-134
1,2-Dibromo-3-chloropropane ug/L 46.750 93 71-133
1,2-Dibromoethane (EDB)ug/L 54.550 109 83-124
1,2-Dichlorobenzene ug/L 47.550 95 80-133
1,2-Dichloroethane ug/L 47.050 94 67-128
1,2-Dichloropropane ug/L 53.450 107 75-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342727
SURRY BANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014256LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 48.150 96 77-130
1,3-Dichloropropane ug/L 54.150 108 76-131
1,4-Dichlorobenzene ug/L 47.950 96 78-130
2,2-Dichloropropane ug/L 50.750 101 40-160
2-Butanone (MEK)ug/L 126100 126 61-144
2-Hexanone ug/L 101100 101 68-143
4-Methyl-2-pentanone (MIBK)ug/L 94.9J100 95 72-135
Acetone ug/L 115100 115 48-146
Acetonitrile ug/L 525500 105 62-150
Acrolein ug/L 320250 128 24-160
Acrylonitrile ug/L 268250 107 40-160
Allyl chloride ug/L 47.650 95 66-137
Benzene ug/L 52.150 104 80-125
Bromochloromethane ug/L 48.950 98 71-125
Bromodichloromethane ug/L 48.550 97 78-124
Bromoform ug/L 43.150 86 71-128
Bromomethane ug/L 42.150 84 40-160
Carbon disulfide ug/L 49.3J50 99 50-160
Carbon tetrachloride ug/L 45.150 90 69-131
Chlorobenzene ug/L 48.850 98 81-122
Chloroethane ug/L 40.850 82 39-148
Chloroform ug/L 50.950 102 73-127
Chloromethane ug/L 49.950 100 44-146
Chloroprene ug/L 49.350 99 75-145
cis-1,2-Dichloroethene ug/L 52.550 105 74-124
cis-1,3-Dichloropropene ug/L 54.150 108 72-132
Dibromochloromethane ug/L 47.550 95 78-125
Dibromomethane ug/L 44.250 88 82-120
Dichlorodifluoromethane ug/L 41.150 82 34-157
Ethyl methacrylate ug/L 45.750 91 82-121
Ethylbenzene ug/L 50.150 100 79-121
Hexachloro-1,3-butadiene ug/L 43.550 87 72-131
Iodomethane ug/L 91.7100 92 39-154
Isobutanol ug/L 11301000 113 34-160
Methacrylonitrile ug/L 563500 113 74-134
Methyl methacrylate ug/L 43.550 87 84-124
Methylene Chloride ug/L 53.650 107 64-133
Naphthalene ug/L 48.650 97 73-133
Propionitrile ug/L 562500 112 73-140
Styrene ug/L 51.050 102 84-126
Tetrachloroethene ug/L 44.850 90 78-122
Toluene ug/L 46.450 93 80-121
trans-1,2-Dichloroethene ug/L 52.350 105 71-127
trans-1,3-Dichloropropene ug/L 52.450 105 69-141
trans-1,4-Dichloro-2-butene ug/L 68.3J50 137 40-160
Trichloroethene ug/L 50.450 101 78-122
Trichlorofluoromethane ug/L 45.450 91 53-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342727
SURRY BANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014256LABORATORY CONTROL SAMPLE:
LCSSpike
Vinyl acetate ug/L 99.2100 99 40-160
Vinyl chloride ug/L 41.950 84 58-137
Xylene (Total)ug/L 149150 99 81-126
1,2-Dichloroethane-d4 (S)%103 70-130
4-Bromofluorobenzene (S)%107 70-130
Toluene-d8 (S)%96 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2014258MATRIX SPIKE SAMPLE:
MSSpike
Result
92342478011
1,1,1,2-Tetrachloroethane ug/L 20.020 100 70-130ND
1,1,1-Trichloroethane ug/L 23.020 115 70-130ND
1,1,2,2-Tetrachloroethane ug/L 22.120 110 70-130ND
1,1,2-Trichloroethane ug/L 22.220 111 70-130ND
1,1-Dichloroethane ug/L 23.120 116 70-130ND
1,1-Dichloroethene ug/L 23.020 115 70-166ND
1,1-Dichloropropene ug/L 23.320 116 70-130ND
1,2,3-Trichloropropane ug/L 19.520 98 70-130ND
1,2,4-Trichlorobenzene ug/L 19.320 97 70-130ND
1,2-Dibromo-3-chloropropane ug/L 18.220 91 70-130ND
1,2-Dibromoethane (EDB)ug/L 19.720 99 70-130ND
1,2-Dichlorobenzene ug/L 20.920 105 70-130ND
1,2-Dichloroethane ug/L 21.320 106 70-130ND
1,2-Dichloropropane ug/L 24.120 120 70-130ND
1,3-Dichlorobenzene ug/L 21.720 108 70-130ND
1,3-Dichloropropane ug/L 20.420 102 70-130ND
1,4-Dichlorobenzene ug/L 21.120 105 70-130ND
2,2-Dichloropropane ug/L 21.220 106 70-130ND
2-Butanone (MEK)ug/L 47.7J40 119 70-130ND
2-Hexanone ug/L 40.9J40 102 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 43.2J40 108 70-130ND
Acetone ug/L 93.5J M14019870-13014.4J
Acetonitrile ug/L 219200 110 70-130ND
Acrolein ug/L 117100 117 70-130ND
Acrylonitrile ug/L 114J100 114 70-130ND
Allyl chloride ug/L 26.8 M12013470-130ND
Benzene ug/L 23.420 117 70-148ND
Bromochloromethane ug/L 21.420 107 70-130ND
Bromodichloromethane ug/L 22.420 112 70-130ND
Bromoform ug/L 16.520 83 70-130ND
Bromomethane ug/L 19.820 99 70-130ND
Carbon disulfide ug/L 23.4J20 117 70-130ND
Carbon tetrachloride ug/L 22.420 112 70-130ND
Chlorobenzene ug/L 22.120 110 70-146ND
Chloroethane ug/L 21.720 108 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342727
SURRY BANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2014258MATRIX SPIKE SAMPLE:
MSSpike
Result
92342478011
Chloroform ug/L 23.220 116 70-130ND
Chloromethane ug/L 25.820 129 70-130ND
Chloroprene ug/L 22.820 114 70-130ND
cis-1,2-Dichloroethene ug/L 24.520 119 70-1300.64J
cis-1,3-Dichloropropene ug/L 23.420 117 70-130ND
Dibromochloromethane ug/L 18.420 92 70-130ND
Dibromomethane ug/L 21.720 108 70-130ND
Dichlorodifluoromethane ug/L 19.220 96 70-130ND
Ethyl methacrylate ug/L 19.420 97 70-130ND
Ethylbenzene ug/L 23.020 115 70-130ND
Hexachloro-1,3-butadiene ug/L 19.320 96 70-130ND
Iodomethane ug/L 41.640 104 70-130ND
Isobutanol ug/L 419400 105 70-130ND
Methacrylonitrile ug/L 230200 115 70-130ND
Methyl methacrylate ug/L 19.7J20 98 70-130ND
Methylene Chloride ug/L 23.220 116 70-130ND
Naphthalene ug/L 21.620 108 70-130ND
Propionitrile ug/L 243200 121 70-130ND
Styrene ug/L 22.320 112 70-130ND
Tetrachloroethene ug/L 19.420 97 70-130ND
Toluene ug/L 22.720 113 70-155ND
trans-1,2-Dichloroethene ug/L 25.020 125 70-130ND
trans-1,3-Dichloropropene ug/L 21.820 109 70-130ND
trans-1,4-Dichloro-2-butene ug/L 21.3J20 106 70-130ND
Trichloroethene ug/L 23.820 119 69-151ND
Trichlorofluoromethane ug/L 22.120 111 70-130ND
Vinyl acetate ug/L 37.6J40 94 70-130ND
Vinyl chloride ug/L 21.820 109 70-130ND
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%109 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342478010
2014257SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 0.50J 300.36J
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342727
SURRY BANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342478010
2014257SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acetonitrile ug/L ND 30ND
Acrolein ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Allyl chloride ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L 0.29J 30ND
Chloroprene ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 0.88J 300.65J
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Ethyl methacrylate ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Isobutanol ug/L ND 30ND
Methacrylonitrile ug/L ND 30ND
Methyl methacrylate ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
Propionitrile ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342727
SURRY BANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342478010
2014257SAMPLE DUPLICATE:
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%92 092
4-Bromofluorobenzene (S)%105 2103
Toluene-d8 (S)%108 2109
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342727
SURRY BANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363513
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92342727001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2015224
Associated Lab Samples:92342727001
Matrix:Water
AnalyzedMDL
Cyanide ug/L ND 10.0 06/07/17 13:524.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2015225LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 101100 101 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015226MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342317015
2015227
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L 100 94 80-12091 2 10100ND97.6 95.4
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015228MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342712006
2015229
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L M1,R11002980-12019 27 101000.013
mg/L 41.2 31.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 28
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92342727
SURRY BANKS
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92342727
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Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92342727001 363321 364621EBEPA 3010A EPA 6010
92342727002 363321 364621FBEPA 3010A EPA 6010
92342727001 363478 363771EBEPA 3010A EPA 6020B
92342727002 363478 363771FBEPA 3010A EPA 6020B
92342727001 363459 363485EBEPA 7470 EPA 7470
92342727002 363459 363485FBEPA 7470 EPA 7470
92342727001 363328EBEPA 8260
92342727002 363328FBEPA 8260
92342727003 363328TBEPA 8260
92342727001 363513EBSM 4500-CN-E
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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Appendix B
Field Sampling Parameter Data Sheet(s)