8603_SurryCountyElkin_MSWLF_GMWR_20171031

Surry County Closed C&D and Closed MSWLF, Elkin
Elkin, North Carolina
June 2017
Permit Number: 86-03
Semi-Annual Water Quality Monitoring Report
Prepared for
PO Box 97
Garner, NC 27529
License No, C-0281
Municipal Engineering Services Company, P.A.Garner and Boone, North Carolina
MESCO Project Number: G17025.0

TABLE OF CONTENTS
SECTION
Introduction Page 1
Background Page 1
Sampling Procedures Page 2
Field Parameter Data Page 2
Laboratory Results Page 2
Quality Control Samples Page 2
Groundwater Samples Page 3
Surface Water Samples Page 3
Groundwater and Surface Water Characterization Page 3
Findings Page 4
Closing Page 4
FIGURES
Topographic Map with Site Location Figure 1
Single Event Potentiometric Map of Uppermost Aquifer Figure 2

TABLES
Groundwater Monitoring Well Construction Table Table 1
Field Observations of Monitoring Locations Table 2
Field Parameter Data Summary Table 3
Sampling and Analysis Summary Table 4
Groundwater and QC Sample Detections Table 5
Surface Water Sample Detections Table 6
Hydrologic Properties at Monitoring Well Locations Table 7
APPENDICIES
Laboratory Analysis Report and Chains of Custody Appendix A
Field Sampling Parameter Data Sheet(s) Appendix B
October 31, 2017
Ms. Jaclynne Drummond
Solid Waste Section (SWS)
Division of Waste Management
North Carolina Department of Environmental Quality (NCDEQ)
2090 US 70 Highway
Swannanoa, NC 28778
Re: Semi-Annual Water Quality Monitoring Report
Surry County Closed C&D and Closed MSWLF, Elkin
Permit No. 86-03
MESCO Project No. G17025.0
Event Date(s): June 26-27 & 29, 2017
Dear Ms. Drummond;
Introduction
On behalf of Surry County, Municipal Engineering Services Company, P.A. (MESCO) is pleased to present thisSemi-Annual Water Quality Report for the spring 2017 event performed at the Surry County closed construction and
demolition (C&D) and closed municipal solid waste landfill (MSWLF). NCDEQ Solid Waste Rules 15A NCAC
13B.1632 requires that Surry County provide this report to the SWS on a semi-annual basis. This report documents
the quality of the ground and surface waters during this monitoring event performed on June 26-27, 2017.
Laboratory analytical results indicate volatile organic compounds (VOCs) persist within three wells that monitor theuppermost aquifer. The surface water samples collected from the discharge feature remain unimpacted.
Background
The Surry County closed C&D and MSWLF, permit #86-03, is located at Elkin Landfill Road (SR 1191), Elkin,
Surry County, North Carolina. The site location topographic map is depicted in the attached Figure 1. Prior tooperating as a C&D landfill the site operated as an unlined sanitary MSWLF that consisted of two units. The first
area was closed prior to October 1991 with a 24 inch final soil cover. The second area was closed with a cohesive
cap of 18 inches of soil with a minimum permeability of less than 1 x 10-5 cm/sec, and 18 inches of erosive layer
prior to December 31, 1998 in accordance with the Transition Plan. C&D was placed on top of the cohesive capped
unit until 2008.
This event was performed in accordance with the NC SWS rules/regulations as promulgated in 15A NCAC 13B and
as a condition of the post-closure portion of the permit to operate. Water quality at this facility has been monitored
at least semi-annually since 1989 with historical data available since 1994. The SWS approved a modification to the
assessment monitoring program on October 15, 2014 (DIN:21983) which entails a subset of wells be sampled for
Appendix II parameters once every three years.
As specified within 15A NCAC 13B.1632(j), the SWS Environmental Monitoring Report Form and SWS
memorandums, this report contains sampling procedures, field and laboratory results, ground/surface water
characterization, and findings. Well construction summary table, field observations table, field parameter data table,
sampling and analysis summary table, detections compared to Standards tables, a groundwater flow directions/rates
table, potentiometric map, quality assurance/quality control data, and laboratory analytical data results are enclosedherein.

Sampling Procedure
MESCO personnel performed this sampling event utilizing portable monitoring methodology in accordance with the
site-specific Sampling and Analysis Plan (SAP) and the NCDENR SWS guidance document Solid Waste SectionGuidelines for Groundwater, Soil, and Surface Water Sampling revised April 2008. Water samples were collected
from nine downgradient groundwater monitoring wells (MW-2, MW-3, MW-3A, MW-4, MW-5, MW-6, MW-7S,
MW-7D and MW-8), one background well (MW-1), and two surface water points (SW-1 and SW-2). Quality
control (QC) samples were analyzed through an Equipment Blank (EB) and Field Blank (FB). Monitoring
locations are shown on the single-day potentiometric map (Figure 2).
A summary detailing the construction of the water monitoring wells is presented on Table 1. The function and
integrity of all monitoring locations were visually evaluated and documented on Table 2. The depth to water in
each well was electronically gaged prior to purging to quantify the static water level elevation. Pumping
methodology or bailing was utilized to adequately purge the wells to a minimum of three times the volume of
standing water in the well or until dry. Surface water samples were collected from Snow Creek discharge feature atpreviously designated locations. During well purging and surface water sample collection the required field
parameters were recorded. The samples were then placed into laboratory-prepared, pre-preserved containers via a
new disposable polyethylene bailer. Samples were collected, kept on ice, and transported to a NC-certified
laboratory under proper chain of custody (C-O-C) protocols within the specified hold times for each analysis.
Field Parameter Data
Stabilized field parameters were recorded during purging which included depth to water, pH, specific conductance,
temperature and visual turbidity. MW-7D exhibits a higher than normal pH which is likely caused by a reaction
with the limestone in the portland cement grout. A summary of the field parameter data is presented in Table 3 and
the field sampling data sheet is enclosed in Appendix B.
Laboratory Results
All water samples were analyzed for the Appendix I list of VOCs and total unfiltered metals listed in 40 CFR 258.
Pace Analytical Laboratories (PACE) of Huntersville and Asheville, NC performed the laboratory analysis. A
sampling and analysis table summarizing the locations, constituents, and methods is presented as Table 4.
Laboratory results and C-O-Cs are presented in Appendix A.
Water samples were analyzed to the laboratory-established Method Detection Limits (MDL), which are at or below
the current Solid Waste Section Limit (SWSL). Table 5 summarizes constituents detected in groundwater and QC
samples that attain or were above the current SWSL, SWS adopted Groundwater Protection Standards (GWP),
North Carolina Groundwater Standards (2L) or the Maximum Contaminant Level (MCL) commonly referenced as
the Federal “Drinking Water Standard”. Table 6 lists the constituents detected in surface water samples compared
SWSL, the North Carolina Surface Water Standards (2B) for a Class C water-body and the MCL.
Quality Control Samples
Among other constituents acetone was detected in EB and FB and chloromethane was found in FB. Acetone and
chloromethane were also detected in the majority of ground and surface water samples in comparable levels which is
inconsistent with previous events. The detections of acetone are believed to be lab induced false positives. Since
levels were below regulatory Standards the suspected laboratory induced artifact contamination is inconsequentialfor compliance purposes.
2
Groundwater Samples
Three metals were detected above the NC 2L/GWP Standard in samples collected from 7 wells as summarized in the
following table.
Metals Detected Above 2L/GWP Standards in Groundwater
Cd Co Va
SWSL 1 10 25
2L/GWP STD.2 1 0.3
MW-2 8.4 j 6.4 j
MW-3 8.7 j 2.8 j
MW-3A 2.5 56.6 5.3 j
MW-5 4.4
MW-6 18 4.9 j
MW-7D 2.4
MW-8 5.5 3.9 j
Concentrations in ug/L. J = “j-qualified” since below the SWSL thus value is considered an estimate
Three VOCs were detected above the NC 2L Standard in samples collected from 5 wells as summarized in the
following table.
VOCs Detected Above 2L Standards in Groundwater
1,4-DCB Benzene Vinyl Chloride
SWSL 1 1 1
2L/GWP STD.6 1 0.03
MW-2 7.6 1.4
MW-3 1.5 0.71 j
MW-3A 10.4 1.1 2.4
MW-6 1.2
MW-8 1.1
Concentrations in ug/L. j = “j-qualified” since below the SWSL thus value is considered an estimate
A site map depicting the spatial distribution of VOC concentrations exceeding 2L Standards during this sampling
event is shown on Figure 2.
Surface Water Samples
No parameters were detected in either surface water sample in concentrations exceeding the SWSL or applicable 2B
Standard.
Groundwater and Surface Water Characterization
A single-day potentiometric map constructed from groundwater levels collected during this event is presented as
Figure 2. Groundwater flow rates and directions were calculated and are included in Table 6. Groundwater flows
generally southwest, towards the Snow Creek discharge feature. Groundwater average linear velocity rates
calculated from modified Darcy's equation indicate flow rates ranged from approximately 16 ft/yr (MW-3A) to 737
ft/yr (MW-6). Snow Creek, monitored at SW-1 and SW-2, was visually observed to have a low gage height, low
volume and low turbidity.
3
Figures
Topographic Map with Site Location
Surry County Closed MSW/C&D Landfill - Elkin
FIGURE 1
QUADRANGLE LEGEND
1” = 2000'
Landfill Road (Off Joe Mill Ln SR 1121)
Elkin, NC 28621
Lat:36-17-49.4007
Long:-80-46-20.6499
Northing:931704.33
Easting:1477683.95
890FIGURE 2MW-3MW-6987975958883*895891*890937WSW-2WSW-1MW-4921MW-2MW-3AMW-7SMW-7DMW-5(ABANDONED)(ABANDONED)SW-2TRANSFER STATION PAD (CLOSED)MW-1MW-8SW-1897*Groundwater Data at Monitoring Well LocationsJune 26-27, 2017WELL #MW-11042.0054.59987MW-2948.0057.12891*MW-3932.0049.42883*MW-3A926.5031.19895MW-4932.5011.52921MW-5948.5011.35937MW-61004.5046.83958MW-7S901.0111.07890MW-7D900.953.67897**MW-81014.8740.19975* = Elevation not used for groundwater contouring as well screened below static levels.Elevations extrapolated from Light Detection and Ranging (LIDAR) from NCDOT May 2007 Release. Previous surveyed locations and elevations (XY&Z) believed to be inaccurate.TOP OF CASING ELEVATION (FT AMSL)DEPTH TO GROUNDWATER (FT BTOC)GROUNDWATER POTENTIOMETRIC ELEVATION (FT AMSL)
Table
Table 1
Groundwater Monitoring Well Construction Table
June 26 - 27, 2017
Well
Diameter
Total
Well
Depth
Top of
Screen
Depth
Screen
Length
Top of
Casing
Elevation
Ground
Elevation
Groundwater
Elevation
Depth to
Water
(inches)(ft bgs)(ft bgs)(ft)(ft amsl)(ft amsl)(ft amsl)(ft btoc)
MW-1 11/28/89 4 74.56 64.56 10 Soil 1042 1041 985 54.59 36.29711 -80.77236
MW-2 11/08/89 4 79 69 10 Soil 948 947 890 57.12 36.29572 -80.77620
MW-3 11/28/89 4 63 53 10 Soil 932 931 881 49.42 36.29362 -80.77646
MW-3A 09/16/94 2 40 24 16 Fractured Rock 927 924 894 31.19 36.29457 -80.77675
MW-4 09/15/94 2 29 13 16 Fractured Rock 933 929 921 11.52 36.29379 -80.77528
MW-5 09/15/94 2 31 16 15 Fractured Rock 949 845 937 11.35 36.29450 -80.77456
MW-6 09/15/94 2 66 51 15 Fractured Rock 1005 1002 954 46.83 36.29780 -80.77270
MW-7S 06/05/01 2 24 9 15 Fractured Rock 901 889 890 11.07 36.29407 80.77730
MW-7D 06/05/01 2 90 80 10 Fractured Rock 901 889 895 3.67 36.29407 80.77730
MW-8 06/04/01 2 67 52 15 Fractured Rock 1015 1013 973 40.19 36.29739 -80.77246
NOTE:
bgs = below ground surface
amsl= above mean sea level
btoc = below top of casing (PVC well casing)
Monitoring
Well
Date
Installed
Geology of Screened
Interval Latitude Longitude
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1
Table 2
Field Observations of Monitoring Locations
June 26-27, 2017
Sample
Location
Viable
Monitoring
Location
Lack of Any
Evidence of
Tampering
Locked Hinge/Hasp
Operational
Tagged
or
Labeled
Concrete
Surface Pad
Appears to
be Effective
Comments
MW-1 Yes Yes Yes Yes Yes Yes 4” Diameter
MW-2 Yes Yes Yes Yes Yes Yes 4” Diameter. Slow Recharge, hasp replaced
MW-3 Yes Yes Yes Yes Yes Yes 4” Diameter. Slow Recharge
MW-3A Yes Yes Yes Yes Yes Unknown Concrete pad covered with soil
MW-4 Yes Yes Yes Yes Yes Yes
MW-5 Yes Yes Yes Yes Yes Unknown Concrete pad covered with soil. Lock is rusty
MW-6 Yes Yes Yes Yes Yes Yes
MW-7S Yes Yes Yes Yes Yes Yes
MW-7D Yes Yes Yes Yes Yes Yes pH elevated likely grout intrusion
MW-8 Yes Yes Yes Yes Yes Yes
SW-1 Yes -----Low gage & low flow
SW-2 Yes -----Low gage & low flow
Any unusual field conditions, observations, or events:
Vehicle access poor to MW-4 and MW-5 since an erosion ditch blocks path
Facility no longer in operation or occupied since transfer station closed in ~ June 2010.
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1
Table 3
Field Parameter Data Summary
June 26-27, 2017
Depth to
Water
Water
Elevation*
TOC
Elevation*Temp.ORP DO pH
Specific
Conductance TDS
Methane Gas in
Well Headspace
Turbidity of
Metals Sample
ft (btoc)ft (amsl)ft (amsl) C mV mg/L SU umhos/cm mg/L %/Vol Visual
MW-1 54.59 987.41 1042.00 15.7 NR NR 6.3 97 NR NR Clear
MW-2 57.12 890.88 948.00 15.6 NR NR 6.5 1823 NR NR Slight
MW-3 49.42 882.58 932.00 14.9 NR NR 6.1 410 NR NR Slight
MW-3A 31.19 895.31 926.50 12.9 NR NR 6.2 893 NR NR Clear
MW-4 11.52 920.98 932.50 13.1 NR NR 6.3 67 NR NR Clear
MW-5 11.35 937.15 948.50 13.2 NR NR 6.4 98 NR NR Clear
MW-6 46.83 957.67 1004.50 14.9 NR NR 6.3 312 NR NR Clear
MW-7S 11.07 889.94 901.01 12.9 NR NR 8.2 376 NR NR Clear
MW-7D 3.67 897.28 900.95 13.3 NR NR 6.2 261 NR NR Clear
MW-8 40.19 974.68 1014.87 15.6 NR NR 6.1 293 NR NR Clear
Minimum 3.67 882.58 900.95 12.9 NR NR 6.1 67 NR NR Clear
Average 31.70 923.39 955.08 14.2 NR NR 6.5 463 NR NR Clear
Maximum 57.12 987.41 1042.00 15.7 NR NR 8.2 1823 NR NR Slight
SW-1 ---16.8 NR NR 7.2 77 NR -Clear
SW-2 ---16.9 NR NR 7.2 89 NR -Clear
Minimum ---16.8 NR NR 7.2 77 NR -Clear
Average ---16.9 NR NR 7.2 83 NR -Clear
Maximum ---16.9 NR NR 7.2 89 NR -Clear
NR = No Reading attempted
* = Elevation extrapolated from photo inspected LIDAR released in 2007 by NCDOT (Not Surveyed).
btoc = below top of casing
amsl = above mean sea level
Parameter
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1
Table 4
Sampling and Analysis Summary
June 26-27, 2017
VOCs Total Metals TemperatureConductivityTotal Dissolved Solids (TDS)pHTurbidityLab EPA 8260B Lab EPA 6000/7000Field MeterField MeterField MeterField MeterField VisualMW-1 x x x x x x
MW-2 x x x x x x
MW-3 x x x x x x
MW-3A x x x x x x
MW-4 x x x x x x
MW-5 x x x x x x
MW-6 x x x x x x
MW-7S x x x x x x
MW-7D x x x x x x
MW-8 x x x x x x
SW-1 x x x x x x
SW-2 x x x x x x
EB x x
FB x x
TB x
All wells listed on SAP presented
App. I Field Parameter
App I & II = List from current 40 CFR 258
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1
Table 5
Groundwater and QC Sample Detections
June 26,27 & 29, 2017
MW-1 MW-2 MW-3 MW-3A MW-4 MW-5 MW-6 MW-7D MW-7S MW-8 EB FB
B S S S S S S S S S QC QC
Arsenic, total 5 10 10 10 9.9 J
Barium, total 2.5 100 700 2000 27.4 J 319 126 448 23.1 J 25.3 J 71.1 J 11.2 J 60.8 J 47.6 J
Cadmium, total 0.5 1 2 5 2.5 (N)1 4.4 (N)2.4 (N)0.77 J 5.5 (N)
Chromium, total 2.5 10 10 100 2.5 J 2.7 J
Cobalt, total 2.5 10 1 NE 8.4 J (N)8.7 J (N)56.6 (N)18 (N)3.9 J (N)
Copper, total 2.5 10 1000 1300 6.5 J 3.9 J 3.1 J
Nickel, total 2.5 50 100 NE 13 J 66.5 44.9 J 10.2 J
Vanadium, total 2.5 25 0.3 NE 6.4 J (N)2.8 J (N)5.3 J (N)4.9 J (N)
Zinc, total 5 10 1000 NE 17.4 11 6.5 J 14 12.3 10.3 16 5.7 J
1,1-Dichloroethane 0.32 5 6 NE 0.45 J 0.93 J 0.89 J 0.66 J
1,2-Dichlorobenzene 0.3 5 20 NE 4.2 J 3 J 1.4 J 0.91 J
1,4-Dichlorobenzene 0.33 1 6 75 7.6 (L)3.4 10.4 (L)2.1 1.8
Acetone 10 100 6000 NE 13.4 J 33.1 J 11.1 J 10.2 J 21.3 J 34.1 J
Benzene 0.25 1 1 5 1.4 (L)1.5 (L)1.1 (L)0.43 J 1.1 (L)
Chlorobenzene 0.23 3 50 100 4.9 0.74 J 3.6 5.1 1.1 J
Chloromethane 0.11 1 3 NE 0.56 J 0.56 J 0.59 J 0.67 J 0.54 J 0.76 J 0.57 J 0.44 J
cis-1,2-Dichloroethene 0.19 5 70 70 0.56 J 13.4 16.9 2.7 J 0.98 J 7.7 12.3
Tetrachloroethene 0.46 1 0.7 5 0.99 J
Toluene 0.26 1 600 1000 0.47 J 19.1
Trichloroethene 0.47 1 3 5 1.3 0.94 J
Vinyl chloride 0.62 1 0.03 2 0.71 J (L)2.4 (L)1.2 (L)
Red Bold Above Established MCL/2L/GWP Std.
No regulatory compliance significance.
MDL = Method Detection Limit, SWSL = Solid Waste Section Limit, 2L/GWP Standard = NC 2L and IMAC Standards adopted by SWS, MCL = Maximum Contaminant Level for Drinking Water
J = "J-qualified". Concentration detected between MDL and SWSL. Considered estimated value
(N) Preliminary source is believed to be Natural originating from erosion of natural deposits. Source not anthropogenic.
(L) Prelilminary source is believed to be anthropogenic with leachate or landfill gas as transport mechanism
A definitive source of the detections was not determined as part of this report.
-- = Not Tested, J = Detected >MDL<SWSL, < Not Detected above MDL
BG = Background Well Sample, QC = Quality Control Sample, S = Sentinal Well Sample
Yellow Highlighted Above Established Federal MCL Drinking Water Std.
Metals (Appendix I)
VOCs (Appendix I)
Units ug/L, Blank cells means Not Detected, -- means not tested
Parameter Name MDL SWSL 2L/GWP
Std MCL
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1
Table 6
Surface Water Sample Detections
June 26, 27 & 29, 2017
SW-1 SW-2
D D
Barium, total 2.5 100 200000 2000 14.1 J 14.2 J
Zinc, total 5 10 50 NE 5.7 J
Acetone 10 100 2000 NE 10.1 J
Red Bold Above Established 2B Std.Regulatory compliance Standard
No regulatory compliance significance.
MDL = Method Detection Limit, SWSL = Solid Waste Section Limit, 2B Standard = NC 2B Surface Water Standards adopted by SWS, MCL = Maximum Contaminant Level for Drinking Water
J = "J-qualified". Concentration detected between MDL and SWSL. Considered estimated value
U = Upstream of monitored unit, D= Downstream of monitored unit
Metals (Appendix I)
Units ug/L, Blank cells means Not Detected, -- means not tested
Parameter Name MDL SWSL 2B Std MCL
VOCs (Appendix I)
Yellow Highlighted Above Established Federal MCL Drinking Water Std.
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1
Table 7
Hydrologic Properties at Monitoring Locations
June 26-27, 2017
Monitoring
Well
Hydraulic
Conductivity
Effective
Porosity
Hydraulic
Gradient
Groundwater
Average Linear
Velocity Rate
Flow
Direction
Depth to
Groundwater
Groundwater
Potentiometric
Elevation*
Screened Interval
Lithology
(cm/second)(%)(feet/feet)(feet/year)(ft btoc)(ft amsl)
MW-1 9.90E-05 5 0.088 180 S48W 54.59 988 Clay
MW-2 2.00E-05 5 na na na 57.12 890**Clay
MW-3 5.00E-05 5 na na na 49.42 881**Clay
Minimum 2.70E-04 5 0.088 180 -49.42 882 -
Average 3.45E-04 5 0.088 180 -53.71 920 -
Maximum 4.20E-04 5 0.088 180 -57.12 891 -
MW-3A 2.50E-05 5 0.031 16 N49W 31.19 894 Fractured Rock
MW-4 4.20E-04 5 0.007 61 N72W 11.52 921 Fractured Rock
MW-5 2.70E-04 5 0.007 40 N86W 11.35 937 Fractured Rock
MW-6 1.20E-04 5 0.305 757 N11W 46.83 954 Fractured Rock
MW-7S 2.30E-04 5 0.102 486 S81W 11.07 889 Fractured Rock
MW-7D na na na na na 3.67 892**Fractured Rock
MW-8 2.40E-05 5 0.178 89 N24W 40.19 974 Fractured Rock
Minimum 2.40E-05 5 0.007 16 -3.67 889 -
Average 1.82E-04 5 0.105 241 -22.26 924 -
Maximum 4.20E-04 5 0.305 757 -46.83 988 -
NOTE: Effective porosity data obtained from GAI Consultants' January 1995 Groundwater Sampling Report.
Hydraulic conductivity values from MW-7S and MW-8 derived from slug tests performed by Joyce Engineering on July 25, 2001.
Values for MW-1 through MW-6 obtained from GAI consultants' January 1995 Groundwater Sampling Report.
Hydrologic gradient calculated from groundwater elevations recorded June 26, 2017.
Wells screened in both the upper bedrock & unconfined aquifer utilized for flow directions/gradients.
* = Elevation extrapolated from photo inspected LIDAR released 2007 by NCDOT (Not Surveyed).
** = Denotes wells with depressed potentiometric head. Therefore, flow directions and rates not calculable.
Average Linear Velocity Rate (Q ) is defined by modified Darcy's equation:
where
K = hydraulic conductivity
ne = effective porosity
dh = head difference
dl = horizontal distance
dl
dh
n
KQ
e
×-=
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1
Appendix A
Laboratory Analysis Reports
Chains of Custody
#=CL#
July 14, 2017
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92345849
92345849
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
SURRY CO CLOSED MSWLF- ELKIN
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on June 28, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 45
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 45
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Lab ID Sample ID Matrix Date Collected Date Received
92345849001 MW-2 Water 06/26/17 18:00 06/28/17 06:50
92345849002 MW-3 Water 06/26/17 17:35 06/28/17 06:50
92345849003 MW-3A Water 06/26/17 18:40 06/28/17 06:50
92345849004 MW-4 Water 06/27/17 09:30 06/28/17 06:50
92345849005 MW-5 Water 06/27/17 09:55 06/28/17 06:50
92345849006 MW-6 Water 06/27/17 12:00 06/28/17 06:50
92345849007 MW-7S Water 06/26/17 19:10 06/28/17 06:50
92345849008 MW-7D Water 06/26/17 19:45 06/28/17 06:50
92345849009 MW-8 Water 06/27/17 11:05 06/28/17 06:50
92345849010 SW-1 Water 06/27/17 10:10 06/28/17 06:50
92345849011 SW-2 Water 06/27/17 10:35 06/28/17 06:50
92345849012 MW-1 Water 06/27/17 09:00 06/28/17 06:50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 45
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92345849001 MW-2 EPA 6010 14 PASI-ASH1
EPA 8260 50 PASI-CZDO
92345849002 MW-3 EPA 6010 14 PASI-ASH1
EPA 8260 50 PASI-CZDO
92345849003 MW-3A EPA 6010 14 PASI-ASH1
EPA 8260 50 PASI-CZDO
92345849004 MW-4 EPA 6010 14 PASI-ASH1
EPA 8260 50 PASI-CZDO
92345849005 MW-5 EPA 6010 14 PASI-ASH1
EPA 8260 50 PASI-CZDO
92345849006 MW-6 EPA 6010 14 PASI-ASH1
EPA 8260 50 PASI-CZDO
92345849007 MW-7S EPA 6010 14 PASI-ASH1
EPA 8260 50 PASI-CZDO
92345849008 MW-7D EPA 6010 14 PASI-ASH1
EPA 8260 50 PASI-CZDO
92345849009 MW-8 EPA 6010 14 PASI-ASH1
EPA 8260 50 PASI-CZDO
92345849010 SW-1 EPA 6010 14 PASI-ASH1
EPA 8260 50 PASI-CZDO
92345849011 SW-2 EPA 6010 14 PASI-ASH1
EPA 8260 50 PASI-CZDO
92345849012 MW-1 EPA 6010 14 PASI-ASER, SH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CZDO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Sample:MW-2 Lab ID:92345849001 Collected:06/26/17 18:00 Received:06/28/17 06:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 07/07/17 18:57 7440-36-006/29/17 15:306.0 3.9 1
Arsenic 9.9J ug/L 07/07/17 06:11 7440-38-206/29/17 15:3010.0 5.0 1
Barium 319 ug/L 07/07/17 06:11 7440-39-306/29/17 15:301002.5 1
Beryllium ND ug/L 07/07/17 06:11 7440-41-706/29/17 15:301.0 0.50 1
Cadmium ND ug/L 07/07/17 06:11 7440-43-906/29/17 15:301.0 0.50 1
Chromium ND ug/L 07/07/17 06:11 7440-47-306/29/17 15:3010.0 2.5 1
Cobalt 8.4J ug/L 07/07/17 06:11 7440-48-406/29/17 15:3010.0 2.5 1
Copper ND ug/L 07/07/17 06:11 7440-50-806/29/17 15:3010.0 2.5 1
Lead ND ug/L 07/07/17 06:11 7439-92-106/29/17 15:3010.0 2.5 1
Nickel 13.0J ug/L 07/07/17 06:11 7440-02-006/29/17 15:3050.0 2.5 1
Selenium ND ug/L 07/07/17 06:11 7782-49-206/29/17 15:3010.0 5.0 1
Silver ND ug/L 07/07/17 06:11 7440-22-406/29/17 15:3010.0 2.5 1
Vanadium 6.4J ug/L 07/07/17 06:11 7440-62-206/29/17 15:3025.0 2.5 1
Zinc ND ug/L 07/07/17 06:11 7440-66-606/29/17 15:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 13.4J ug/L 06/29/17 17:29 67-64-1 L110010.0 1
Acrylonitrile ND ug/L 06/29/17 17:29 107-13-1 M12001.9 1
Benzene 1.4 ug/L 06/29/17 17:29 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/29/17 17:29 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/29/17 17:29 75-27-41.0 0.18 1
Bromoform ND ug/L 06/29/17 17:29 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/29/17 17:29 74-83-9 M110.0 0.29 1
2-Butanone (MEK)ND ug/L 06/29/17 17:29 78-93-3 M11000.96 1
Carbon disulfide ND ug/L 06/29/17 17:29 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/29/17 17:29 56-23-51.0 0.25 1
Chlorobenzene 4.9 ug/L 06/29/17 17:29 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/29/17 17:29 75-00-310.0 0.54 1
Chloroform ND ug/L 06/29/17 17:29 67-66-35.0 0.14 1
Chloromethane 0.56J ug/L 06/29/17 17:29 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/29/17 17:29 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/29/17 17:29 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/29/17 17:29 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/29/17 17:29 74-95-310.0 0.21 1
1,2-Dichlorobenzene 4.2J ug/L 06/29/17 17:29 95-50-15.0 0.30 1
1,4-Dichlorobenzene 7.6 ug/L 06/29/17 17:29 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/29/17 17:29 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/29/17 17:29 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/29/17 17:29 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/29/17 17:29 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/29/17 17:29 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/29/17 17:29 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/29/17 17:29 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 06/29/17 17:29 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/29/17 17:29 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/29/17 17:29 100-41-41.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Sample:MW-2 Lab ID:92345849001 Collected:06/26/17 18:00 Received:06/28/17 06:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
2-Hexanone ND ug/L 06/29/17 17:29 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/29/17 17:29 74-88-4 M110.0 0.32 1
Methylene Chloride ND ug/L 06/29/17 17:29 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/29/17 17:29 108-10-11000.33 1
Styrene ND ug/L 06/29/17 17:29 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/29/17 17:29 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/29/17 17:29 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/29/17 17:29 127-18-41.0 0.46 1
Toluene 0.47J ug/L 06/29/17 17:29 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/29/17 17:29 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/29/17 17:29 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/29/17 17:29 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/29/17 17:29 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/29/17 17:29 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/29/17 17:29 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/29/17 17:29 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/29/17 17:29 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %06/29/17 17:29 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %06/29/17 17:29 17060-07-070-130 1
Toluene-d8 (S)109 %06/29/17 17:29 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Sample:MW-3 Lab ID:92345849002 Collected:06/26/17 17:35 Received:06/28/17 06:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 07/07/17 19:10 7440-36-006/29/17 15:306.0 3.9 1
Arsenic ND ug/L 07/07/17 06:23 7440-38-206/29/17 15:3010.0 5.0 1
Barium 126 ug/L 07/07/17 06:23 7440-39-306/29/17 15:301002.5 1
Beryllium ND ug/L 07/07/17 06:23 7440-41-706/29/17 15:301.0 0.50 1
Cadmium ND ug/L 07/07/17 06:23 7440-43-906/29/17 15:301.0 0.50 1
Chromium ND ug/L 07/07/17 06:23 7440-47-306/29/17 15:3010.0 2.5 1
Cobalt 8.7J ug/L 07/07/17 06:23 7440-48-406/29/17 15:3010.0 2.5 1
Copper ND ug/L 07/07/17 06:23 7440-50-806/29/17 15:3010.0 2.5 1
Lead ND ug/L 07/07/17 06:23 7439-92-106/29/17 15:3010.0 2.5 1
Nickel 66.5 ug/L 07/07/17 06:23 7440-02-006/29/17 15:3050.0 2.5 1
Selenium ND ug/L 07/07/17 06:23 7782-49-206/29/17 15:3010.0 5.0 1
Silver ND ug/L 07/07/17 06:23 7440-22-406/29/17 15:3010.0 2.5 1
Vanadium 2.8J ug/L 07/07/17 06:23 7440-62-206/29/17 15:3025.0 2.5 1
Zinc 17.4 ug/L 07/07/17 06:23 7440-66-606/29/17 15:3010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 33.1J ug/L 06/29/17 17:46 67-64-1 L110010.0 1
Acrylonitrile ND ug/L 06/29/17 17:46 107-13-12001.9 1
Benzene 1.5 ug/L 06/29/17 17:46 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/29/17 17:46 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/29/17 17:46 75-27-41.0 0.18 1
Bromoform ND ug/L 06/29/17 17:46 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/29/17 17:46 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/29/17 17:46 78-93-31000.96 1
Carbon disulfide ND ug/L 06/29/17 17:46 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/29/17 17:46 56-23-51.0 0.25 1
Chlorobenzene 0.74J ug/L 06/29/17 17:46 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/29/17 17:46 75-00-310.0 0.54 1
Chloroform ND ug/L 06/29/17 17:46 67-66-35.0 0.14 1
Chloromethane 0.59J ug/L 06/29/17 17:46 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/29/17 17:46 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/29/17 17:46 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/29/17 17:46 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/29/17 17:46 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/29/17 17:46 95-50-15.0 0.30 1
1,4-Dichlorobenzene 3.4 ug/L 06/29/17 17:46 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/29/17 17:46 110-57-61001.0 1
1,1-Dichloroethane 0.45J ug/L 06/29/17 17:46 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/29/17 17:46 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/29/17 17:46 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 13.4 ug/L 06/29/17 17:46 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/29/17 17:46 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/29/17 17:46 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 06/29/17 17:46 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/29/17 17:46 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/29/17 17:46 100-41-41.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Sample:MW-3 Lab ID:92345849002 Collected:06/26/17 17:35 Received:06/28/17 06:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
2-Hexanone ND ug/L 06/29/17 17:46 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/29/17 17:46 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/29/17 17:46 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/29/17 17:46 108-10-11000.33 1
Styrene ND ug/L 06/29/17 17:46 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/29/17 17:46 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/29/17 17:46 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/29/17 17:46 127-18-41.0 0.46 1
Toluene 19.1 ug/L 06/29/17 17:46 108-88-3 D61.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/29/17 17:46 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/29/17 17:46 79-00-51.0 0.29 1
Trichloroethene 1.3 ug/L 06/29/17 17:46 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/29/17 17:46 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/29/17 17:46 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/29/17 17:46 108-05-450.0 0.35 1
Vinyl chloride 0.71J ug/L 06/29/17 17:46 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/29/17 17:46 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %06/29/17 17:46 460-00-470-130 1
1,2-Dichloroethane-d4 (S)116 %06/29/17 17:46 17060-07-070-130 1
Toluene-d8 (S)104 %06/29/17 17:46 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Sample:MW-3A Lab ID:92345849003 Collected:06/26/17 18:40 Received:06/28/17 06:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 07/08/17 23:43 7440-36-006/29/17 16:156.0 3.9 1
Arsenic ND ug/L 07/08/17 23:43 7440-38-206/29/17 16:1510.0 5.0 1
Barium 448 ug/L 07/12/17 05:36 7440-39-306/29/17 16:151002.5 1
Beryllium ND ug/L 07/08/17 23:43 7440-41-706/29/17 16:151.0 0.50 1
Cadmium 2.5 ug/L 07/08/17 23:43 7440-43-906/29/17 16:151.0 0.50 1
Chromium ND ug/L 07/08/17 23:43 7440-47-306/29/17 16:1510.0 2.5 1
Cobalt 56.6 ug/L 07/08/17 23:43 7440-48-406/29/17 16:1510.0 2.5 1
Copper ND ug/L 07/08/17 23:43 7440-50-806/29/17 16:1510.0 2.5 1
Lead ND ug/L 07/08/17 23:43 7439-92-106/29/17 16:1510.0 2.5 1
Nickel 44.9J ug/L 07/08/17 23:43 7440-02-006/29/17 16:1550.0 2.5 1
Selenium ND ug/L 07/08/17 23:43 7782-49-206/29/17 16:1510.0 5.0 1
Silver ND ug/L 07/08/17 23:43 7440-22-406/29/17 16:1510.0 2.5 1
Vanadium 5.3J ug/L 07/08/17 23:43 7440-62-206/29/17 16:1525.0 2.5 1
Zinc 11.0 ug/L 07/08/17 23:43 7440-66-606/29/17 16:1510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 11.1J ug/L 06/29/17 18:21 67-64-1 L110010.0 1
Acrylonitrile ND ug/L 06/29/17 18:21 107-13-12001.9 1
Benzene 1.1 ug/L 06/29/17 18:21 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/29/17 18:21 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/29/17 18:21 75-27-41.0 0.18 1
Bromoform ND ug/L 06/29/17 18:21 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/29/17 18:21 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/29/17 18:21 78-93-31000.96 1
Carbon disulfide ND ug/L 06/29/17 18:21 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/29/17 18:21 56-23-51.0 0.25 1
Chlorobenzene 3.6 ug/L 06/29/17 18:21 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/29/17 18:21 75-00-310.0 0.54 1
Chloroform ND ug/L 06/29/17 18:21 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/29/17 18:21 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/29/17 18:21 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/29/17 18:21 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/29/17 18:21 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/29/17 18:21 74-95-310.0 0.21 1
1,2-Dichlorobenzene 3.0J ug/L 06/29/17 18:21 95-50-15.0 0.30 1
1,4-Dichlorobenzene 10.4 ug/L 06/29/17 18:21 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/29/17 18:21 110-57-61001.0 1
1,1-Dichloroethane 0.93J ug/L 06/29/17 18:21 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/29/17 18:21 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/29/17 18:21 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 16.9 ug/L 06/29/17 18:21 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/29/17 18:21 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/29/17 18:21 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 06/29/17 18:21 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/29/17 18:21 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/29/17 18:21 100-41-41.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Sample:MW-3A Lab ID:92345849003 Collected:06/26/17 18:40 Received:06/28/17 06:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
2-Hexanone ND ug/L 06/29/17 18:21 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/29/17 18:21 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/29/17 18:21 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/29/17 18:21 108-10-11000.33 1
Styrene ND ug/L 06/29/17 18:21 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/29/17 18:21 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/29/17 18:21 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/29/17 18:21 127-18-41.0 0.46 1
Toluene ND ug/L 06/29/17 18:21 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/29/17 18:21 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/29/17 18:21 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/29/17 18:21 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/29/17 18:21 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/29/17 18:21 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/29/17 18:21 108-05-450.0 0.35 1
Vinyl chloride 2.4 ug/L 06/29/17 18:21 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/29/17 18:21 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %06/29/17 18:21 460-00-470-130 1
1,2-Dichloroethane-d4 (S)120 %06/29/17 18:21 17060-07-070-130 1
Toluene-d8 (S)107 %06/29/17 18:21 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Sample:MW-4 Lab ID:92345849004 Collected:06/27/17 09:30 Received:06/28/17 06:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 07/08/17 23:52 7440-36-006/29/17 16:156.0 3.9 1
Arsenic ND ug/L 07/08/17 23:52 7440-38-206/29/17 16:1510.0 5.0 1
Barium 23.1J ug/L 07/12/17 05:45 7440-39-306/29/17 16:151002.5 1
Beryllium ND ug/L 07/08/17 23:52 7440-41-706/29/17 16:151.0 0.50 1
Cadmium 1.0 ug/L 07/08/17 23:52 7440-43-906/29/17 16:151.0 0.50 1
Chromium ND ug/L 07/08/17 23:52 7440-47-306/29/17 16:1510.0 2.5 1
Cobalt ND ug/L 07/08/17 23:52 7440-48-406/29/17 16:1510.0 2.5 1
Copper ND ug/L 07/08/17 23:52 7440-50-806/29/17 16:1510.0 2.5 1
Lead ND ug/L 07/08/17 23:52 7439-92-106/29/17 16:1510.0 2.5 1
Nickel ND ug/L 07/08/17 23:52 7440-02-006/29/17 16:1550.0 2.5 1
Selenium ND ug/L 07/08/17 23:52 7782-49-206/29/17 16:1510.0 5.0 1
Silver ND ug/L 07/08/17 23:52 7440-22-406/29/17 16:1510.0 2.5 1
Vanadium ND ug/L 07/08/17 23:52 7440-62-206/29/17 16:1525.0 2.5 1
Zinc ND ug/L 07/08/17 23:52 7440-66-606/29/17 16:1510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/29/17 18:39 67-64-1 L110010.0 1
Acrylonitrile ND ug/L 06/29/17 18:39 107-13-12001.9 1
Benzene ND ug/L 06/29/17 18:39 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/29/17 18:39 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/29/17 18:39 75-27-41.0 0.18 1
Bromoform ND ug/L 06/29/17 18:39 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/29/17 18:39 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/29/17 18:39 78-93-31000.96 1
Carbon disulfide ND ug/L 06/29/17 18:39 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/29/17 18:39 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/29/17 18:39 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/29/17 18:39 75-00-310.0 0.54 1
Chloroform ND ug/L 06/29/17 18:39 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/29/17 18:39 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/29/17 18:39 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/29/17 18:39 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/29/17 18:39 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/29/17 18:39 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/29/17 18:39 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/29/17 18:39 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/29/17 18:39 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/29/17 18:39 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/29/17 18:39 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/29/17 18:39 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/29/17 18:39 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/29/17 18:39 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/29/17 18:39 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 06/29/17 18:39 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/29/17 18:39 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/29/17 18:39 100-41-41.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Sample:MW-4 Lab ID:92345849004 Collected:06/27/17 09:30 Received:06/28/17 06:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
2-Hexanone ND ug/L 06/29/17 18:39 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/29/17 18:39 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/29/17 18:39 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/29/17 18:39 108-10-11000.33 1
Styrene ND ug/L 06/29/17 18:39 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/29/17 18:39 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/29/17 18:39 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/29/17 18:39 127-18-41.0 0.46 1
Toluene ND ug/L 06/29/17 18:39 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/29/17 18:39 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/29/17 18:39 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/29/17 18:39 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/29/17 18:39 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/29/17 18:39 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/29/17 18:39 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/29/17 18:39 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/29/17 18:39 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %06/29/17 18:39 460-00-470-130 1
1,2-Dichloroethane-d4 (S)115 %06/29/17 18:39 17060-07-070-130 1
Toluene-d8 (S)105 %06/29/17 18:39 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Sample:MW-5 Lab ID:92345849005 Collected:06/27/17 09:55 Received:06/28/17 06:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 07/08/17 23:55 7440-36-006/29/17 16:156.0 3.9 1
Arsenic ND ug/L 07/08/17 23:55 7440-38-206/29/17 16:1510.0 5.0 1
Barium 25.3J ug/L 07/12/17 05:48 7440-39-306/29/17 16:151002.5 1
Beryllium ND ug/L 07/08/17 23:55 7440-41-706/29/17 16:151.0 0.50 1
Cadmium 4.4 ug/L 07/08/17 23:55 7440-43-906/29/17 16:151.0 0.50 1
Chromium 2.7J ug/L 07/08/17 23:55 7440-47-306/29/17 16:1510.0 2.5 1
Cobalt ND ug/L 07/08/17 23:55 7440-48-406/29/17 16:1510.0 2.5 1
Copper ND ug/L 07/08/17 23:55 7440-50-806/29/17 16:1510.0 2.5 1
Lead ND ug/L 07/08/17 23:55 7439-92-106/29/17 16:1510.0 2.5 1
Nickel ND ug/L 07/08/17 23:55 7440-02-006/29/17 16:1550.0 2.5 1
Selenium ND ug/L 07/08/17 23:55 7782-49-206/29/17 16:1510.0 5.0 1
Silver ND ug/L 07/08/17 23:55 7440-22-406/29/17 16:1510.0 2.5 1
Vanadium ND ug/L 07/08/17 23:55 7440-62-206/29/17 16:1525.0 2.5 1
Zinc 6.5J ug/L 07/08/17 23:55 7440-66-606/29/17 16:1510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/29/17 18:56 67-64-1 L110010.0 1
Acrylonitrile ND ug/L 06/29/17 18:56 107-13-12001.9 1
Benzene ND ug/L 06/29/17 18:56 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/29/17 18:56 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/29/17 18:56 75-27-41.0 0.18 1
Bromoform ND ug/L 06/29/17 18:56 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/29/17 18:56 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/29/17 18:56 78-93-31000.96 1
Carbon disulfide ND ug/L 06/29/17 18:56 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/29/17 18:56 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/29/17 18:56 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/29/17 18:56 75-00-310.0 0.54 1
Chloroform ND ug/L 06/29/17 18:56 67-66-35.0 0.14 1
Chloromethane 0.67J ug/L 06/29/17 18:56 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/29/17 18:56 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/29/17 18:56 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/29/17 18:56 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/29/17 18:56 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/29/17 18:56 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/29/17 18:56 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/29/17 18:56 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/29/17 18:56 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/29/17 18:56 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/29/17 18:56 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/29/17 18:56 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/29/17 18:56 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/29/17 18:56 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 06/29/17 18:56 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/29/17 18:56 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/29/17 18:56 100-41-41.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Sample:MW-5 Lab ID:92345849005 Collected:06/27/17 09:55 Received:06/28/17 06:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
2-Hexanone ND ug/L 06/29/17 18:56 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/29/17 18:56 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/29/17 18:56 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/29/17 18:56 108-10-11000.33 1
Styrene ND ug/L 06/29/17 18:56 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/29/17 18:56 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/29/17 18:56 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/29/17 18:56 127-18-41.0 0.46 1
Toluene ND ug/L 06/29/17 18:56 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/29/17 18:56 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/29/17 18:56 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/29/17 18:56 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/29/17 18:56 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/29/17 18:56 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/29/17 18:56 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/29/17 18:56 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/29/17 18:56 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %06/29/17 18:56 460-00-470-130 1
1,2-Dichloroethane-d4 (S)114 %06/29/17 18:56 17060-07-070-130 1
Toluene-d8 (S)104 %06/29/17 18:56 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Sample:MW-6 Lab ID:92345849006 Collected:06/27/17 12:00 Received:06/28/17 06:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 07/08/17 23:58 7440-36-006/29/17 16:156.0 3.9 1
Arsenic ND ug/L 07/08/17 23:58 7440-38-206/29/17 16:1510.0 5.0 1
Barium 71.1J ug/L 07/12/17 05:52 7440-39-306/29/17 16:151002.5 1
Beryllium ND ug/L 07/08/17 23:58 7440-41-706/29/17 16:151.0 0.50 1
Cadmium ND ug/L 07/08/17 23:58 7440-43-906/29/17 16:151.0 0.50 1
Chromium ND ug/L 07/08/17 23:58 7440-47-306/29/17 16:1510.0 2.5 1
Cobalt 18.0 ug/L 07/08/17 23:58 7440-48-406/29/17 16:1510.0 2.5 1
Copper ND ug/L 07/08/17 23:58 7440-50-806/29/17 16:1510.0 2.5 1
Lead ND ug/L 07/08/17 23:58 7439-92-106/29/17 16:1510.0 2.5 1
Nickel ND ug/L 07/08/17 23:58 7440-02-006/29/17 16:1550.0 2.5 1
Selenium ND ug/L 07/08/17 23:58 7782-49-206/29/17 16:1510.0 5.0 1
Silver ND ug/L 07/08/17 23:58 7440-22-406/29/17 16:1510.0 2.5 1
Vanadium 4.9J ug/L 07/08/17 23:58 7440-62-206/29/17 16:1525.0 2.5 1
Zinc 14.0 ug/L 07/08/17 23:58 7440-66-606/29/17 16:1510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/29/17 19:13 67-64-1 L110010.0 1
Acrylonitrile ND ug/L 06/29/17 19:13 107-13-12001.9 1
Benzene 0.43J ug/L 06/29/17 19:13 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/29/17 19:13 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/29/17 19:13 75-27-41.0 0.18 1
Bromoform ND ug/L 06/29/17 19:13 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/29/17 19:13 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/29/17 19:13 78-93-31000.96 1
Carbon disulfide ND ug/L 06/29/17 19:13 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/29/17 19:13 56-23-51.0 0.25 1
Chlorobenzene 5.1 ug/L 06/29/17 19:13 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/29/17 19:13 75-00-310.0 0.54 1
Chloroform ND ug/L 06/29/17 19:13 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/29/17 19:13 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/29/17 19:13 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/29/17 19:13 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/29/17 19:13 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/29/17 19:13 74-95-310.0 0.21 1
1,2-Dichlorobenzene 1.4J ug/L 06/29/17 19:13 95-50-15.0 0.30 1
1,4-Dichlorobenzene 2.1 ug/L 06/29/17 19:13 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/29/17 19:13 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/29/17 19:13 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/29/17 19:13 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/29/17 19:13 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 2.7J ug/L 06/29/17 19:13 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/29/17 19:13 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/29/17 19:13 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 06/29/17 19:13 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/29/17 19:13 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/29/17 19:13 100-41-41.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Sample:MW-6 Lab ID:92345849006 Collected:06/27/17 12:00 Received:06/28/17 06:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
2-Hexanone ND ug/L 06/29/17 19:13 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/29/17 19:13 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/29/17 19:13 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/29/17 19:13 108-10-11000.33 1
Styrene ND ug/L 06/29/17 19:13 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/29/17 19:13 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/29/17 19:13 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/29/17 19:13 127-18-41.0 0.46 1
Toluene ND ug/L 06/29/17 19:13 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/29/17 19:13 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/29/17 19:13 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/29/17 19:13 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/29/17 19:13 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/29/17 19:13 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/29/17 19:13 108-05-450.0 0.35 1
Vinyl chloride 1.2 ug/L 06/29/17 19:13 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/29/17 19:13 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %06/29/17 19:13 460-00-470-130 1
1,2-Dichloroethane-d4 (S)115 %06/29/17 19:13 17060-07-070-130 1
Toluene-d8 (S)106 %06/29/17 19:13 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Sample:MW-7S Lab ID:92345849007 Collected:06/26/17 19:10 Received:06/28/17 06:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 07/09/17 00:02 7440-36-006/29/17 16:156.0 3.9 1
Arsenic ND ug/L 07/09/17 00:02 7440-38-206/29/17 16:1510.0 5.0 1
Barium 60.8J ug/L 07/12/17 05:55 7440-39-306/29/17 16:151002.5 1
Beryllium ND ug/L 07/09/17 00:02 7440-41-706/29/17 16:151.0 0.50 1
Cadmium 0.77J ug/L 07/09/17 00:02 7440-43-906/29/17 16:151.0 0.50 1
Chromium ND ug/L 07/09/17 00:02 7440-47-306/29/17 16:1510.0 2.5 1
Cobalt ND ug/L 07/09/17 00:02 7440-48-406/29/17 16:1510.0 2.5 1
Copper 3.9J ug/L 07/09/17 00:02 7440-50-806/29/17 16:1510.0 2.5 1
Lead ND ug/L 07/09/17 00:02 7439-92-106/29/17 16:1510.0 2.5 1
Nickel ND ug/L 07/09/17 00:02 7440-02-006/29/17 16:1550.0 2.5 1
Selenium ND ug/L 07/09/17 00:02 7782-49-206/29/17 16:1510.0 5.0 1
Silver ND ug/L 07/09/17 00:02 7440-22-406/29/17 16:1510.0 2.5 1
Vanadium ND ug/L 07/09/17 00:02 7440-62-206/29/17 16:1525.0 2.5 1
Zinc 10.3 ug/L 07/09/17 00:02 7440-66-606/29/17 16:1510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 10.2J ug/L 06/29/17 19:31 67-64-1 L110010.0 1
Acrylonitrile ND ug/L 06/29/17 19:31 107-13-12001.9 1
Benzene ND ug/L 06/29/17 19:31 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/29/17 19:31 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/29/17 19:31 75-27-41.0 0.18 1
Bromoform ND ug/L 06/29/17 19:31 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/29/17 19:31 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/29/17 19:31 78-93-31000.96 1
Carbon disulfide ND ug/L 06/29/17 19:31 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/29/17 19:31 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/29/17 19:31 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/29/17 19:31 75-00-310.0 0.54 1
Chloroform ND ug/L 06/29/17 19:31 67-66-35.0 0.14 1
Chloromethane 0.76J ug/L 06/29/17 19:31 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/29/17 19:31 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/29/17 19:31 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/29/17 19:31 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/29/17 19:31 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/29/17 19:31 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/29/17 19:31 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/29/17 19:31 110-57-61001.0 1
1,1-Dichloroethane 0.89J ug/L 06/29/17 19:31 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/29/17 19:31 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/29/17 19:31 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 7.7 ug/L 06/29/17 19:31 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/29/17 19:31 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/29/17 19:31 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 06/29/17 19:31 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/29/17 19:31 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/29/17 19:31 100-41-41.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 17 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Sample:MW-7S Lab ID:92345849007 Collected:06/26/17 19:10 Received:06/28/17 06:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
2-Hexanone ND ug/L 06/29/17 19:31 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/29/17 19:31 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/29/17 19:31 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/29/17 19:31 108-10-11000.33 1
Styrene ND ug/L 06/29/17 19:31 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/29/17 19:31 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/29/17 19:31 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/29/17 19:31 127-18-41.0 0.46 1
Toluene ND ug/L 06/29/17 19:31 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/29/17 19:31 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/29/17 19:31 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/29/17 19:31 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/29/17 19:31 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/29/17 19:31 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/29/17 19:31 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/29/17 19:31 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/29/17 19:31 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %06/29/17 19:31 460-00-470-130 1
1,2-Dichloroethane-d4 (S)112 %06/29/17 19:31 17060-07-070-130 1
Toluene-d8 (S)102 %06/29/17 19:31 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Sample:MW-7D Lab ID:92345849008 Collected:06/26/17 19:45 Received:06/28/17 06:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 07/09/17 00:05 7440-36-006/29/17 16:156.0 3.9 1
Arsenic ND ug/L 07/09/17 00:05 7440-38-206/29/17 16:1510.0 5.0 1
Barium 11.2J ug/L 07/12/17 05:58 7440-39-306/29/17 16:151002.5 1
Beryllium ND ug/L 07/09/17 00:05 7440-41-706/29/17 16:151.0 0.50 1
Cadmium 2.4 ug/L 07/09/17 00:05 7440-43-906/29/17 16:151.0 0.50 1
Chromium ND ug/L 07/09/17 00:05 7440-47-306/29/17 16:1510.0 2.5 1
Cobalt ND ug/L 07/09/17 00:05 7440-48-406/29/17 16:1510.0 2.5 1
Copper 6.5J ug/L 07/09/17 00:05 7440-50-806/29/17 16:1510.0 2.5 1
Lead ND ug/L 07/09/17 00:05 7439-92-106/29/17 16:1510.0 2.5 1
Nickel ND ug/L 07/09/17 00:05 7440-02-006/29/17 16:1550.0 2.5 1
Selenium ND ug/L 07/09/17 00:05 7782-49-206/29/17 16:1510.0 5.0 1
Silver ND ug/L 07/09/17 00:05 7440-22-406/29/17 16:1510.0 2.5 1
Vanadium ND ug/L 07/09/17 00:05 7440-62-206/29/17 16:1525.0 2.5 1
Zinc 12.3 ug/L 07/09/17 00:05 7440-66-606/29/17 16:1510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/29/17 19:48 67-64-1 L110010.0 1
Acrylonitrile ND ug/L 06/29/17 19:48 107-13-12001.9 1
Benzene ND ug/L 06/29/17 19:48 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/29/17 19:48 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/29/17 19:48 75-27-41.0 0.18 1
Bromoform ND ug/L 06/29/17 19:48 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/29/17 19:48 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/29/17 19:48 78-93-31000.96 1
Carbon disulfide ND ug/L 06/29/17 19:48 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/29/17 19:48 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/29/17 19:48 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/29/17 19:48 75-00-310.0 0.54 1
Chloroform ND ug/L 06/29/17 19:48 67-66-35.0 0.14 1
Chloromethane 0.54J ug/L 06/29/17 19:48 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/29/17 19:48 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/29/17 19:48 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/29/17 19:48 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/29/17 19:48 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/29/17 19:48 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/29/17 19:48 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/29/17 19:48 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/29/17 19:48 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/29/17 19:48 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/29/17 19:48 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.98J ug/L 06/29/17 19:48 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/29/17 19:48 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/29/17 19:48 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 06/29/17 19:48 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/29/17 19:48 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/29/17 19:48 100-41-41.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Sample:MW-7D Lab ID:92345849008 Collected:06/26/17 19:45 Received:06/28/17 06:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
2-Hexanone ND ug/L 06/29/17 19:48 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/29/17 19:48 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/29/17 19:48 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/29/17 19:48 108-10-11000.33 1
Styrene ND ug/L 06/29/17 19:48 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/29/17 19:48 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/29/17 19:48 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/29/17 19:48 127-18-41.0 0.46 1
Toluene ND ug/L 06/29/17 19:48 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/29/17 19:48 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/29/17 19:48 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/29/17 19:48 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/29/17 19:48 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/29/17 19:48 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/29/17 19:48 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/29/17 19:48 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/29/17 19:48 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %06/29/17 19:48 460-00-470-130 1
1,2-Dichloroethane-d4 (S)114 %06/29/17 19:48 17060-07-070-130 1
Toluene-d8 (S)104 %06/29/17 19:48 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Sample:MW-8 Lab ID:92345849009 Collected:06/27/17 11:05 Received:06/28/17 06:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 07/09/17 00:17 7440-36-006/29/17 16:156.0 3.9 1
Arsenic ND ug/L 07/09/17 00:17 7440-38-206/29/17 16:1510.0 5.0 1
Barium 47.6J ug/L 07/12/17 06:01 7440-39-306/29/17 16:151002.5 1
Beryllium ND ug/L 07/09/17 00:17 7440-41-706/29/17 16:151.0 0.50 1
Cadmium 5.5 ug/L 07/09/17 00:17 7440-43-906/29/17 16:151.0 0.50 1
Chromium ND ug/L 07/09/17 00:17 7440-47-306/29/17 16:1510.0 2.5 1
Cobalt 3.9J ug/L 07/09/17 00:17 7440-48-406/29/17 16:1510.0 2.5 1
Copper 3.1J ug/L 07/09/17 00:17 7440-50-806/29/17 16:1510.0 2.5 1
Lead ND ug/L 07/09/17 00:17 7439-92-106/29/17 16:1510.0 2.5 1
Nickel 10.2J ug/L 07/09/17 00:17 7440-02-006/29/17 16:1550.0 2.5 1
Selenium ND ug/L 07/09/17 00:17 7782-49-206/29/17 16:1510.0 5.0 1
Silver ND ug/L 07/09/17 00:17 7440-22-406/29/17 16:1510.0 2.5 1
Vanadium ND ug/L 07/09/17 00:17 7440-62-206/29/17 16:1525.0 2.5 1
Zinc 16.0 ug/L 07/09/17 00:17 7440-66-606/29/17 16:1510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/29/17 20:05 67-64-1 L110010.0 1
Acrylonitrile ND ug/L 06/29/17 20:05 107-13-12001.9 1
Benzene 1.1 ug/L 06/29/17 20:05 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/29/17 20:05 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/29/17 20:05 75-27-41.0 0.18 1
Bromoform ND ug/L 06/29/17 20:05 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/29/17 20:05 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/29/17 20:05 78-93-31000.96 1
Carbon disulfide ND ug/L 06/29/17 20:05 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/29/17 20:05 56-23-51.0 0.25 1
Chlorobenzene 1.1J ug/L 06/29/17 20:05 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/29/17 20:05 75-00-310.0 0.54 1
Chloroform ND ug/L 06/29/17 20:05 67-66-35.0 0.14 1
Chloromethane 0.57J ug/L 06/29/17 20:05 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/29/17 20:05 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/29/17 20:05 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/29/17 20:05 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/29/17 20:05 74-95-310.0 0.21 1
1,2-Dichlorobenzene 0.91J ug/L 06/29/17 20:05 95-50-15.0 0.30 1
1,4-Dichlorobenzene 1.8 ug/L 06/29/17 20:05 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/29/17 20:05 110-57-61001.0 1
1,1-Dichloroethane 0.66J ug/L 06/29/17 20:05 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/29/17 20:05 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/29/17 20:05 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 12.3 ug/L 06/29/17 20:05 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/29/17 20:05 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/29/17 20:05 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 06/29/17 20:05 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/29/17 20:05 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/29/17 20:05 100-41-41.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Sample:MW-8 Lab ID:92345849009 Collected:06/27/17 11:05 Received:06/28/17 06:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
2-Hexanone ND ug/L 06/29/17 20:05 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/29/17 20:05 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/29/17 20:05 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/29/17 20:05 108-10-11000.33 1
Styrene ND ug/L 06/29/17 20:05 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/29/17 20:05 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/29/17 20:05 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/29/17 20:05 127-18-41.0 0.46 1
Toluene ND ug/L 06/29/17 20:05 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/29/17 20:05 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/29/17 20:05 79-00-51.0 0.29 1
Trichloroethene 0.94J ug/L 06/29/17 20:05 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/29/17 20:05 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/29/17 20:05 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/29/17 20:05 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/29/17 20:05 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/29/17 20:05 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %06/29/17 20:05 460-00-470-130 1
1,2-Dichloroethane-d4 (S)114 %06/29/17 20:05 17060-07-070-130 1
Toluene-d8 (S)106 %06/29/17 20:05 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Sample:SW-1 Lab ID:92345849010 Collected:06/27/17 10:10 Received:06/28/17 06:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 07/09/17 00:20 7440-36-006/29/17 16:156.0 3.9 1
Arsenic ND ug/L 07/09/17 00:20 7440-38-206/29/17 16:1510.0 5.0 1
Barium 14.1J ug/L 07/12/17 06:04 7440-39-306/29/17 16:151002.5 1
Beryllium ND ug/L 07/09/17 00:20 7440-41-706/29/17 16:151.0 0.50 1
Cadmium ND ug/L 07/09/17 00:20 7440-43-906/29/17 16:151.0 0.50 1
Chromium ND ug/L 07/09/17 00:20 7440-47-306/29/17 16:1510.0 2.5 1
Cobalt ND ug/L 07/09/17 00:20 7440-48-406/29/17 16:1510.0 2.5 1
Copper ND ug/L 07/09/17 00:20 7440-50-806/29/17 16:1510.0 2.5 1
Lead ND ug/L 07/09/17 00:20 7439-92-106/29/17 16:1510.0 2.5 1
Nickel ND ug/L 07/09/17 00:20 7440-02-006/29/17 16:1550.0 2.5 1
Selenium ND ug/L 07/09/17 00:20 7782-49-206/29/17 16:1510.0 5.0 1
Silver ND ug/L 07/09/17 00:20 7440-22-406/29/17 16:1510.0 2.5 1
Vanadium ND ug/L 07/09/17 00:20 7440-62-206/29/17 16:1525.0 2.5 1
Zinc ND ug/L 07/09/17 00:20 7440-66-606/29/17 16:1510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/29/17 20:23 67-64-1 L110010.0 1
Acrylonitrile ND ug/L 06/29/17 20:23 107-13-12001.9 1
Benzene ND ug/L 06/29/17 20:23 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/29/17 20:23 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/29/17 20:23 75-27-41.0 0.18 1
Bromoform ND ug/L 06/29/17 20:23 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/29/17 20:23 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/29/17 20:23 78-93-31000.96 1
Carbon disulfide ND ug/L 06/29/17 20:23 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/29/17 20:23 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/29/17 20:23 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/29/17 20:23 75-00-310.0 0.54 1
Chloroform ND ug/L 06/29/17 20:23 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/29/17 20:23 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/29/17 20:23 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/29/17 20:23 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/29/17 20:23 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/29/17 20:23 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/29/17 20:23 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/29/17 20:23 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/29/17 20:23 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/29/17 20:23 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/29/17 20:23 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/29/17 20:23 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/29/17 20:23 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/29/17 20:23 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/29/17 20:23 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 06/29/17 20:23 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/29/17 20:23 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/29/17 20:23 100-41-41.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 23 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Sample:SW-1 Lab ID:92345849010 Collected:06/27/17 10:10 Received:06/28/17 06:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
2-Hexanone ND ug/L 06/29/17 20:23 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/29/17 20:23 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/29/17 20:23 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/29/17 20:23 108-10-11000.33 1
Styrene ND ug/L 06/29/17 20:23 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/29/17 20:23 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/29/17 20:23 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/29/17 20:23 127-18-41.0 0.46 1
Toluene ND ug/L 06/29/17 20:23 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/29/17 20:23 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/29/17 20:23 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/29/17 20:23 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/29/17 20:23 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/29/17 20:23 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/29/17 20:23 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/29/17 20:23 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/29/17 20:23 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %06/29/17 20:23 460-00-470-130 1
1,2-Dichloroethane-d4 (S)112 %06/29/17 20:23 17060-07-070-130 1
Toluene-d8 (S)104 %06/29/17 20:23 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 24 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Sample:SW-2 Lab ID:92345849011 Collected:06/27/17 10:35 Received:06/28/17 06:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 07/09/17 00:23 7440-36-006/29/17 16:156.0 3.9 1
Arsenic ND ug/L 07/09/17 00:23 7440-38-206/29/17 16:1510.0 5.0 1
Barium 14.2J ug/L 07/12/17 06:16 7440-39-306/29/17 16:151002.5 1
Beryllium ND ug/L 07/09/17 00:23 7440-41-706/29/17 16:151.0 0.50 1
Cadmium ND ug/L 07/09/17 00:23 7440-43-906/29/17 16:151.0 0.50 1
Chromium ND ug/L 07/09/17 00:23 7440-47-306/29/17 16:1510.0 2.5 1
Cobalt ND ug/L 07/09/17 00:23 7440-48-406/29/17 16:1510.0 2.5 1
Copper ND ug/L 07/09/17 00:23 7440-50-806/29/17 16:1510.0 2.5 1
Lead ND ug/L 07/09/17 00:23 7439-92-106/29/17 16:1510.0 2.5 1
Nickel ND ug/L 07/09/17 00:23 7440-02-006/29/17 16:1550.0 2.5 1
Selenium ND ug/L 07/09/17 00:23 7782-49-206/29/17 16:1510.0 5.0 1
Silver ND ug/L 07/09/17 00:23 7440-22-406/29/17 16:1510.0 2.5 1
Vanadium ND ug/L 07/09/17 00:23 7440-62-206/29/17 16:1525.0 2.5 1
Zinc 5.7J ug/L 07/09/17 00:23 7440-66-606/29/17 16:1510.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 10.1J ug/L 06/29/17 20:40 67-64-1 L110010.0 1
Acrylonitrile ND ug/L 06/29/17 20:40 107-13-12001.9 1
Benzene ND ug/L 06/29/17 20:40 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/29/17 20:40 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/29/17 20:40 75-27-41.0 0.18 1
Bromoform ND ug/L 06/29/17 20:40 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/29/17 20:40 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/29/17 20:40 78-93-31000.96 1
Carbon disulfide ND ug/L 06/29/17 20:40 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/29/17 20:40 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/29/17 20:40 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/29/17 20:40 75-00-310.0 0.54 1
Chloroform ND ug/L 06/29/17 20:40 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/29/17 20:40 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/29/17 20:40 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/29/17 20:40 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/29/17 20:40 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/29/17 20:40 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/29/17 20:40 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/29/17 20:40 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/29/17 20:40 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/29/17 20:40 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/29/17 20:40 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/29/17 20:40 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/29/17 20:40 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/29/17 20:40 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/29/17 20:40 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 06/29/17 20:40 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/29/17 20:40 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/29/17 20:40 100-41-41.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Sample:SW-2 Lab ID:92345849011 Collected:06/27/17 10:35 Received:06/28/17 06:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
2-Hexanone ND ug/L 06/29/17 20:40 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/29/17 20:40 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/29/17 20:40 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/29/17 20:40 108-10-11000.33 1
Styrene ND ug/L 06/29/17 20:40 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/29/17 20:40 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/29/17 20:40 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/29/17 20:40 127-18-41.0 0.46 1
Toluene ND ug/L 06/29/17 20:40 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/29/17 20:40 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/29/17 20:40 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/29/17 20:40 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/29/17 20:40 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/29/17 20:40 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/29/17 20:40 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/29/17 20:40 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/29/17 20:40 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %06/29/17 20:40 460-00-470-130 1
1,2-Dichloroethane-d4 (S)117 %06/29/17 20:40 17060-07-070-130 1
Toluene-d8 (S)104 %06/29/17 20:40 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Sample:MW-1 Lab ID:92345849012 Collected:06/27/17 09:00 Received:06/28/17 06:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 07/10/17 02:34 7440-36-007/06/17 15:356.0 3.9 1
Arsenic ND ug/L 07/10/17 02:34 7440-38-207/06/17 15:3510.0 5.0 1
Barium 27.4J ug/L 07/10/17 02:34 7440-39-307/06/17 15:351002.5 1
Beryllium ND ug/L 07/10/17 02:34 7440-41-707/06/17 15:351.0 0.50 1
Cadmium ND ug/L 07/10/17 02:34 7440-43-907/06/17 15:351.0 0.50 1
Chromium 2.5J ug/L 07/10/17 02:34 7440-47-307/06/17 15:3510.0 2.5 1
Cobalt ND ug/L 07/10/17 02:34 7440-48-407/06/17 15:3510.0 2.5 1
Copper ND ug/L 07/10/17 02:34 7440-50-807/06/17 15:3510.0 2.5 1
Lead ND ug/L 07/11/17 17:43 7439-92-107/06/17 15:3510.0 2.5 1
Nickel ND ug/L 07/10/17 02:34 7440-02-007/06/17 15:3550.0 2.5 1
Selenium ND ug/L 07/10/17 02:34 7782-49-207/06/17 15:3510.0 5.0 1
Silver ND ug/L 07/10/17 02:34 7440-22-407/06/17 15:3510.0 2.5 1
Vanadium ND ug/L 07/10/17 02:34 7440-62-207/06/17 15:3525.0 2.5 1
Zinc ND ug/L 07/13/17 00:54 7440-66-607/06/17 15:3510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 07/08/17 21:08 7440-28-007/01/17 07:255.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/29/17 20:58 67-64-1 L110010.0 1
Acrylonitrile ND ug/L 06/29/17 20:58 107-13-12001.9 1
Benzene ND ug/L 06/29/17 20:58 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/29/17 20:58 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/29/17 20:58 75-27-41.0 0.18 1
Bromoform ND ug/L 06/29/17 20:58 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/29/17 20:58 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/29/17 20:58 78-93-31000.96 1
Carbon disulfide ND ug/L 06/29/17 20:58 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/29/17 20:58 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/29/17 20:58 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/29/17 20:58 75-00-310.0 0.54 1
Chloroform ND ug/L 06/29/17 20:58 67-66-35.0 0.14 1
Chloromethane 0.56J ug/L 06/29/17 20:58 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/29/17 20:58 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/29/17 20:58 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/29/17 20:58 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/29/17 20:58 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/29/17 20:58 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/29/17 20:58 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/29/17 20:58 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 06/29/17 20:58 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/29/17 20:58 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/29/17 20:58 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.56J ug/L 06/29/17 20:58 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/29/17 20:58 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/29/17 20:58 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Sample:MW-1 Lab ID:92345849012 Collected:06/27/17 09:00 Received:06/28/17 06:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 06/29/17 20:58 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/29/17 20:58 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/29/17 20:58 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/29/17 20:58 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/29/17 20:58 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/29/17 20:58 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/29/17 20:58 108-10-11000.33 1
Styrene ND ug/L 06/29/17 20:58 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/29/17 20:58 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/29/17 20:58 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/29/17 20:58 127-18-41.0 0.46 1
Toluene ND ug/L 06/29/17 20:58 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/29/17 20:58 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/29/17 20:58 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/29/17 20:58 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/29/17 20:58 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/29/17 20:58 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/29/17 20:58 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/29/17 20:58 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/29/17 20:58 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %06/29/17 20:58 460-00-470-130 1
1,2-Dichloroethane-d4 (S)111 %06/29/17 20:58 17060-07-070-130 1
Toluene-d8 (S)102 %06/29/17 20:58 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
366982
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92345849001, 92345849002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2034180
Associated Lab Samples:92345849001, 92345849002
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 5.0 07/07/17 04:433.9
Arsenic ug/L ND 10.0 07/07/17 04:435.0
Barium ug/L ND 5.0 07/07/17 04:432.5
Beryllium ug/L ND 1.0 07/07/17 04:430.50
Cadmium ug/L ND 1.0 07/07/17 04:430.50
Chromium ug/L ND 5.0 07/07/17 04:432.5
Cobalt ug/L ND 5.0 07/07/17 04:432.5
Copper ug/L ND 5.0 07/07/17 04:432.5
Lead ug/L ND 5.0 07/07/17 04:432.5
Nickel ug/L ND 5.0 07/07/17 04:432.5
Selenium ug/L ND 10.0 07/07/17 04:435.0
Silver ug/L ND 5.0 07/07/17 04:432.5
Vanadium ug/L ND 5.0 07/07/17 04:432.5
Zinc ug/L ND 10.0 07/07/17 18:325.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2034181LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 501500 100 80-120
Arsenic ug/L 473500 95 80-120
Barium ug/L 515500 103 80-120
Beryllium ug/L 487500 97 80-120
Cadmium ug/L 513500 103 80-120
Chromium ug/L 510500 102 80-120
Cobalt ug/L 506500 101 80-120
Copper ug/L 485500 97 80-120
Lead ug/L 497500 99 80-120
Nickel ug/L 505500 101 80-120
Selenium ug/L 502500 100 80-120
Silver ug/L 247250 99 80-120
Vanadium ug/L 484500 97 80-120
Zinc ug/L 505500 101 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2034182MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92345833006
2034183
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 102 75-125100 1 20500ND511504
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2034182MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92345833006
2034183
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L 500 97 75-12595 2 20500ND484476
Barium ug/L 500 105 75-125103 1 205008.8 532 526
Beryllium ug/L 500 101 75-125100 1 20500ND505498
Cadmium ug/L 500 104 75-125102 1 20500ND518510
Chromium ug/L 500 104 75-125102 2 20500ND523512
Cobalt ug/L 500 102 75-125100 2 20500ND508500
Copper ug/L 500 100 75-12598 2 20500ND499490
Lead ug/L 500 99 75-12598 2 20500ND497489
Nickel ug/L 500 101 75-12599 2 20500ND505497
Selenium ug/L 500 97 75-12595 2 20500ND488479
Silver ug/L 250 102 75-125100 2 20250ND254250
Vanadium ug/L 500 101 75-12598 2 20500ND505493
Zinc ug/L 500 97 75-12597 0 2050025.9 512 511
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 30 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
366984
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92345849003, 92345849004, 92345849005, 92345849006, 92345849007, 92345849008, 92345849009,
92345849010, 92345849011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2034185
Associated Lab Samples:92345849003, 92345849004, 92345849005, 92345849006, 92345849007, 92345849008, 92345849009,
92345849010, 92345849011
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 5.0 07/08/17 23:373.9
Arsenic ug/L ND 10.0 07/08/17 23:375.0
Barium ug/L ND 5.0 07/12/17 05:212.5
Beryllium ug/L ND 1.0 07/08/17 23:370.50
Cadmium ug/L ND 1.0 07/08/17 23:370.50
Chromium ug/L ND 5.0 07/08/17 23:372.5
Cobalt ug/L ND 5.0 07/08/17 23:372.5
Copper ug/L ND 5.0 07/08/17 23:372.5
Lead ug/L ND 5.0 07/08/17 23:372.5
Nickel ug/L ND 5.0 07/08/17 23:372.5
Selenium ug/L ND 10.0 07/08/17 23:375.0
Silver ug/L ND 5.0 07/08/17 23:372.5
Vanadium ug/L ND 5.0 07/08/17 23:372.5
Zinc ug/L ND 10.0 07/12/17 05:215.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2034189LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 521500 104 80-120
Arsenic ug/L 504500 101 80-120
Barium ug/L 477500 95 80-120
Beryllium ug/L 481500 96 80-120
Cadmium ug/L 500500 100 80-120
Chromium ug/L 485500 97 80-120
Cobalt ug/L 508500 102 80-120
Copper ug/L 512500 102 80-120
Lead ug/L 500500 100 80-120
Nickel ug/L 488500 98 80-120
Selenium ug/L 526500 105 80-120
Silver ug/L 258250 103 80-120
Vanadium ug/L 489500 98 80-120
Zinc ug/L 513500 103 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2034190MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92345849003
2034191
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 105 75-125108 2 20500ND527538
Arsenic ug/L 500 104 75-125106 2 20500ND518528
Barium ug/L 500 95 75-12593 1 20500448922912
Beryllium ug/L 500 99 75-12597 1 20500ND494487
Cadmium ug/L 500 101 75-125102 1 205002.5 508 514
Chromium ug/L 500 98 75-12598 0 20500ND491490
Cobalt ug/L 500 100 75-125101 1 2050056.6 554 562
Copper ug/L 500 103 75-125103 0 20500ND516518
Lead ug/L 500 98 75-12599 2 20500ND490498
Nickel ug/L 500 95 75-12596 1 2050044.9J 521 526
Selenium ug/L 500 104 75-125107 2 20500ND522534
Silver ug/L 250 104 75-125104 0 20250ND260260
Vanadium ug/L 500 101 75-125101 0 205005.3J 508 509
Zinc ug/L 500 101 75-125103 2 2050011.0 516 525
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
367481
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92345849012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2037084
Associated Lab Samples:92345849012
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 5.0 07/10/17 01:383.9
Arsenic ug/L ND 10.0 07/10/17 01:385.0
Barium ug/L ND 5.0 07/10/17 01:382.5
Beryllium ug/L ND 1.0 07/10/17 01:380.50
Cadmium ug/L ND 1.0 07/10/17 01:380.50
Chromium ug/L ND 5.0 07/10/17 01:382.5
Cobalt ug/L ND 5.0 07/10/17 01:382.5
Copper ug/L ND 5.0 07/10/17 01:382.5
Lead ug/L ND 5.0 07/11/17 17:112.5
Nickel ug/L ND 5.0 07/10/17 01:382.5
Selenium ug/L ND 10.0 07/10/17 01:385.0
Silver ug/L ND 5.0 07/10/17 01:382.5
Vanadium ug/L ND 5.0 07/10/17 01:382.5
Zinc ug/L ND 10.0 07/13/17 00:255.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2037085LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 503500 101 80-120
Arsenic ug/L 503500 101 80-120
Barium ug/L 510500 102 80-120
Beryllium ug/L 520500 104 80-120
Cadmium ug/L 513500 103 80-120
Chromium ug/L 515500 103 80-120
Cobalt ug/L 515500 103 80-120
Copper ug/L 516500 103 80-120
Lead ug/L 501500 100 80-120
Nickel ug/L 501500 100 80-120
Selenium ug/L 532500 106 80-120
Silver ug/L 254250 101 80-120
Vanadium ug/L 506500 101 80-120
Zinc ug/L 476500 95 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2037086MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92345832032
2037087
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 101 75-12598 3 20500ND505490
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2037086MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92345832032
2037087
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L 500 99 75-12597 2 20500ND497489
Barium ug/L 500 102 75-125100 3 20500ND512498
Beryllium ug/L 500 105 75-125102 3 20500ND523508
Cadmium ug/L 500 103 75-125101 3 20500ND517503
Chromium ug/L 500 103 75-125101 2 205002.6J 519 507
Cobalt ug/L 500 104 75-125101 3 20500ND520505
Copper ug/L 500 104 75-125102 3 20500ND522509
Lead ug/L 500 102 75-12598 3 20500ND510493
Nickel ug/L 500 101 75-12598 3 20500ND505491
Selenium ug/L 500 105 75-125103 2 20500ND528516
Silver ug/L 250 102 75-125100 2 20250ND255249
Vanadium ug/L 500 102 75-125100 2 20500ND511499
Zinc ug/L 500 112 75-125114 1 20500332894901
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
367201
EPA 3010A
EPA 6020B
6020 MET
Associated Lab Samples:92345849012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2035540
Associated Lab Samples:92345849012
Matrix:Water
AnalyzedMDL
Thallium ug/L ND 0.10 07/08/17 20:220.020
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2035541LABORATORY CONTROL SAMPLE:
LCSSpike
Thallium ug/L 103100 103 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2035542MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92345640003
2035543
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Thallium ug/L 100 100 75-125101 1 20100ND100101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
367099
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92345849001, 92345849002, 92345849003, 92345849004, 92345849005, 92345849006, 92345849007,
92345849008, 92345849009, 92345849010, 92345849011, 92345849012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2034914
Associated Lab Samples:92345849001, 92345849002, 92345849003, 92345849004, 92345849005, 92345849006, 92345849007,
92345849008, 92345849009, 92345849010, 92345849011, 92345849012
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/29/17 12:510.33
1,1,1-Trichloroethane ug/L ND 1.0 06/29/17 12:510.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 06/29/17 12:510.40
1,1,2-Trichloroethane ug/L ND 1.0 06/29/17 12:510.29
1,1-Dichloroethane ug/L ND 5.0 06/29/17 12:510.32
1,1-Dichloroethene ug/L ND 5.0 06/29/17 12:510.56
1,2,3-Trichloropropane ug/L ND 1.0 06/29/17 12:510.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 06/29/17 12:512.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/29/17 12:510.27
1,2-Dichlorobenzene ug/L ND 5.0 06/29/17 12:510.30
1,2-Dichloroethane ug/L ND 1.0 06/29/17 12:510.24
1,2-Dichloropropane ug/L ND 1.0 06/29/17 12:510.27
1,4-Dichlorobenzene ug/L ND 1.0 06/29/17 12:510.33
2-Butanone (MEK)ug/L ND 100 06/29/17 12:510.96
2-Hexanone ug/L ND 50.0 06/29/17 12:510.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 06/29/17 12:510.33
Acetone ug/L ND 100 06/29/17 12:5110.0
Acrylonitrile ug/L ND 200 06/29/17 12:511.9
Benzene ug/L ND 1.0 06/29/17 12:510.25
Bromochloromethane ug/L ND 3.0 06/29/17 12:510.17
Bromodichloromethane ug/L ND 1.0 06/29/17 12:510.18
Bromoform ug/L ND 3.0 06/29/17 12:510.26
Bromomethane ug/L ND 10.0 06/29/17 12:510.29
Carbon disulfide ug/L ND 100 06/29/17 12:511.2
Carbon tetrachloride ug/L ND 1.0 06/29/17 12:510.25
Chlorobenzene ug/L ND 3.0 06/29/17 12:510.23
Chloroethane ug/L ND 10.0 06/29/17 12:510.54
Chloroform ug/L ND 5.0 06/29/17 12:510.14
Chloromethane ug/L ND 1.0 06/29/17 12:510.11
cis-1,2-Dichloroethene ug/L ND 5.0 06/29/17 12:510.19
cis-1,3-Dichloropropene ug/L ND 1.0 06/29/17 12:510.13
Dibromochloromethane ug/L ND 3.0 06/29/17 12:510.21
Dibromomethane ug/L ND 10.0 06/29/17 12:510.21
Ethylbenzene ug/L ND 1.0 06/29/17 12:510.30
Iodomethane ug/L ND 10.0 06/29/17 12:510.32
Methylene Chloride ug/L ND 1.0 06/29/17 12:510.97
Styrene ug/L ND 1.0 06/29/17 12:510.26
Tetrachloroethene ug/L ND 1.0 06/29/17 12:510.46
Toluene ug/L ND 1.0 06/29/17 12:510.26
trans-1,2-Dichloroethene ug/L ND 5.0 06/29/17 12:510.49
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2034914
Associated Lab Samples:92345849001, 92345849002, 92345849003, 92345849004, 92345849005, 92345849006, 92345849007,
92345849008, 92345849009, 92345849010, 92345849011, 92345849012
Matrix:Water
AnalyzedMDL
trans-1,3-Dichloropropene ug/L ND 1.0 06/29/17 12:510.26
trans-1,4-Dichloro-2-butene ug/L ND 100 06/29/17 12:511.0
Trichloroethene ug/L ND 1.0 06/29/17 12:510.47
Trichlorofluoromethane ug/L ND 1.0 06/29/17 12:510.20
Vinyl acetate ug/L ND 50.0 06/29/17 12:510.35
Vinyl chloride ug/L ND 1.0 06/29/17 12:510.62
Xylene (Total)ug/L ND 5.0 06/29/17 12:510.66
1,2-Dichloroethane-d4 (S)%111 70-130 06/29/17 12:51
4-Bromofluorobenzene (S)%100 70-130 06/29/17 12:51
Toluene-d8 (S)%108 70-130 06/29/17 12:51
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2034915LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 48.650 97 80-125
1,1,1-Trichloroethane ug/L 45.950 92 71-129
1,1,2,2-Tetrachloroethane ug/L 47.450 95 79-124
1,1,2-Trichloroethane ug/L 49.450 99 85-125
1,1-Dichloroethane ug/L 45.350 91 73-126
1,1-Dichloroethene ug/L 44.350 89 66-135
1,2,3-Trichloropropane ug/L 48.550 97 75-130
1,2-Dibromo-3-chloropropane ug/L 54.150 108 71-133
1,2-Dibromoethane (EDB)ug/L 48.750 97 83-124
1,2-Dichlorobenzene ug/L 43.950 88 80-133
1,2-Dichloroethane ug/L 45.650 91 67-128
1,2-Dichloropropane ug/L 47.550 95 75-132
1,4-Dichlorobenzene ug/L 43.050 86 78-130
2-Butanone (MEK)ug/L 144100 144 61-144
2-Hexanone ug/L 124100 124 68-143
4-Methyl-2-pentanone (MIBK)ug/L 114100 114 72-135
Acetone ug/L 155 L110015548-146
Acrylonitrile ug/L 321250 128 40-160
Benzene ug/L 46.750 93 80-125
Bromochloromethane ug/L 45.650 91 71-125
Bromodichloromethane ug/L 45.850 92 78-124
Bromoform ug/L 45.850 92 71-128
Bromomethane ug/L 24.650 49 40-160
Carbon disulfide ug/L 44.8J50 90 50-160
Carbon tetrachloride ug/L 43.350 87 69-131
Chlorobenzene ug/L 41.850 84 81-122
Chloroethane ug/L 39.250 78 39-148
Chloroform ug/L 44.250 88 73-127
Chloromethane ug/L 43.150 86 44-146
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2034915LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 47.750 95 74-124
cis-1,3-Dichloropropene ug/L 48.250 96 72-132
Dibromochloromethane ug/L 50.850 102 78-125
Dibromomethane ug/L 47.150 94 82-120
Ethylbenzene ug/L 41.550 83 79-121
Iodomethane ug/L 62.4100 62 39-154
Methylene Chloride ug/L 53.850 108 64-133
Styrene ug/L 43.550 87 84-126
Tetrachloroethene ug/L 40.550 81 78-122
Toluene ug/L 43.450 87 80-121
trans-1,2-Dichloroethene ug/L 45.350 91 71-127
trans-1,3-Dichloropropene ug/L 45.150 90 69-141
trans-1,4-Dichloro-2-butene ug/L 65.2J50 130 40-160
Trichloroethene ug/L 46.450 93 78-122
Trichlorofluoromethane ug/L 41.850 84 53-137
Vinyl acetate ug/L 106100 106 40-160
Vinyl chloride ug/L 45.650 91 58-137
Xylene (Total)ug/L 128150 85 81-126
1,2-Dichloroethane-d4 (S)%109 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2034916MATRIX SPIKE SAMPLE:
MSSpike
Result
92345849001
1,1,1,2-Tetrachloroethane ug/L 19.220 96 70-130ND
1,1,1-Trichloroethane ug/L 19.420 97 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19.720 99 70-130ND
1,1,2-Trichloroethane ug/L 20.520 102 70-130ND
1,1-Dichloroethane ug/L 20.420 102 70-130ND
1,1-Dichloroethene ug/L 20.420 102 70-166ND
1,2,3-Trichloropropane ug/L 20.920 104 70-130ND
1,2-Dibromo-3-chloropropane ug/L 20.620 103 70-130ND
1,2-Dibromoethane (EDB)ug/L 20.120 101 70-130ND
1,2-Dichlorobenzene ug/L 21.920 88 70-1304.2J
1,2-Dichloroethane ug/L 20.420 102 70-130ND
1,2-Dichloropropane ug/L 21.020 105 70-130ND
1,4-Dichlorobenzene ug/L 25.420 89 70-1307.6
2-Butanone (MEK)ug/L 53.5J M14013470-130ND
2-Hexanone ug/L 47.5J40 119 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 48.2J40 121 70-130ND
Acetone ug/L 65.3J40 130 70-13013.4J
Acrylonitrile ug/L 140J M110014070-130ND
Benzene ug/L 21.420 100 70-1481.4
Bromochloromethane ug/L 21.020 105 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2034916MATRIX SPIKE SAMPLE:
MSSpike
Result
92345849001
Bromodichloromethane ug/L 19.720 99 70-130ND
Bromoform ug/L 17.020 85 70-130ND
Bromomethane ug/L 7.9J M1204070-130ND
Carbon disulfide ug/L 20.3J20 102 70-130ND
Carbon tetrachloride ug/L 19.320 97 70-130ND
Chlorobenzene ug/L 23.620 94 70-1464.9
Chloroethane ug/L 20.320 101 70-130ND
Chloroform ug/L 20.020 100 70-130ND
Chloromethane ug/L 21.520 105 70-1300.56J
cis-1,2-Dichloroethene ug/L 21.720 109 70-130ND
cis-1,3-Dichloropropene ug/L 18.420 92 70-130ND
Dibromochloromethane ug/L 19.820 99 70-130ND
Dibromomethane ug/L 20.320 102 70-130ND
Ethylbenzene ug/L 18.720 94 70-130ND
Iodomethane ug/L 25.2 M1406370-130ND
Methylene Chloride ug/L 23.620 118 70-130ND
Styrene ug/L 17.920 89 70-130ND
Tetrachloroethene ug/L 17.520 87 70-130ND
Toluene ug/L 20.320 99 70-1550.47J
trans-1,2-Dichloroethene ug/L 20.320 101 70-130ND
trans-1,3-Dichloropropene ug/L 18.820 94 70-130ND
trans-1,4-Dichloro-2-butene ug/L 15.7J20 79 70-130ND
Trichloroethene ug/L 20.720 104 69-151ND
Trichlorofluoromethane ug/L 21.020 105 70-130ND
Vinyl acetate ug/L 35.8J40 90 70-130ND
Vinyl chloride ug/L 20.920 104 70-130ND
1,2-Dichloroethane-d4 (S)%116 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92345849002
2034917SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 0.43J 300.45J
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
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Page 39 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92345849002
2034917SAMPLE DUPLICATE:
1,4-Dichlorobenzene ug/L 3.9 13 303.4
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L 35.9J 8 3033.1J
Acrylonitrile ug/L ND 30ND
Benzene ug/L 1.8 15 301.5
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L 0.79J 300.74J
Chloroethane ug/L 1.0J 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L 0.84J 300.59J
cis-1,2-Dichloroethene ug/L 14.5 8 3013.4
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L 13.5 D6343019.1
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L 1.2 14 301.3
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L 0.87J 300.71J
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%111 4116
4-Bromofluorobenzene (S)%100 1100
Toluene-d8 (S)%104 0104
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
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Page 40 of 45
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associatedsamples may be biased high.L1
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
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Page 41 of 45
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92345849
SURRY CO CLOSED MSWLF- ELKIN
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92345849001 366982 368005MW-2 EPA 3010A EPA 6010
92345849002 366982 368005MW-3 EPA 3010A EPA 6010
92345849003 366984 368002MW-3A EPA 3010A EPA 6010
92345849004 366984 368002MW-4 EPA 3010A EPA 6010
92345849005 366984 368002MW-5 EPA 3010A EPA 6010
92345849006 366984 368002MW-6 EPA 3010A EPA 6010
92345849007 366984 368002MW-7S EPA 3010A EPA 6010
92345849008 366984 368002MW-7D EPA 3010A EPA 6010
92345849009 366984 368002MW-8 EPA 3010A EPA 6010
92345849010 366984 368002SW-1 EPA 3010A EPA 6010
92345849011 366984 368002SW-2 EPA 3010A EPA 6010
92345849012 367481 368240MW-1 EPA 3010A EPA 6010
92345849012 367201 367790MW-1 EPA 3010A EPA 6020B
92345849001 367099MW-2 EPA 8260
92345849002 367099MW-3 EPA 8260
92345849003 367099MW-3A EPA 8260
92345849004 367099MW-4 EPA 8260
92345849005 367099MW-5 EPA 8260
92345849006 367099MW-6 EPA 8260
92345849007 367099MW-7S EPA 8260
92345849008 367099MW-7D EPA 8260
92345849009 367099MW-8 EPA 8260
92345849010 367099SW-1 EPA 8260
92345849011 367099SW-2 EPA 8260
92345849012 367099MW-1 EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 12:42 AM
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Page 42 of 45
Page 43 of 45
Page 44 of 45
Page 45 of 45
#=CL#
July 14, 2017
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92346321
92346321
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
BLANKS
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on June 30, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 1 of 26
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92346321
BLANKS
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 2 of 26
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92346321
BLANKS
Lab ID Sample ID Matrix Date Collected Date Received
92346321001 EB Water 06/29/17 15:50 06/30/17 06:30
92346321002 FB Water 06/29/17 15:55 06/30/17 06:30
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 3 of 26
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92346321
BLANKS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92346321001 EB EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CZDO
92346321002 FB EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CCAH
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 4 of 26
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92346321
BLANKS
Sample:EB Lab ID:92346321001 Collected:06/29/17 15:50 Received:06/30/17 06:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 07/13/17 20:36 7440-36-007/06/17 16:256.0 3.9 1
Arsenic ND ug/L 07/13/17 20:36 7440-38-207/06/17 16:2510.0 5.0 1
Barium ND ug/L 07/13/17 20:36 7440-39-307/06/17 16:251002.5 1
Beryllium ND ug/L 07/13/17 20:36 7440-41-707/06/17 16:251.0 0.50 1
Cadmium ND ug/L 07/13/17 20:36 7440-43-907/06/17 16:251.0 0.50 1
Chromium ND ug/L 07/13/17 20:36 7440-47-307/06/17 16:2510.0 2.5 1
Cobalt ND ug/L 07/13/17 20:36 7440-48-407/06/17 16:2510.0 2.5 1
Copper ND ug/L 07/13/17 20:36 7440-50-807/06/17 16:2510.0 2.5 1
Lead ND ug/L 07/13/17 20:36 7439-92-107/06/17 16:2510.0 2.5 1
Nickel ND ug/L 07/13/17 20:36 7440-02-007/06/17 16:2550.0 2.5 1
Selenium ND ug/L 07/13/17 20:36 7782-49-207/06/17 16:2510.0 5.0 1
Silver ND ug/L 07/13/17 20:36 7440-22-407/06/17 16:2510.0 2.5 1
Vanadium ND ug/L 07/13/17 20:36 7440-62-207/06/17 16:2525.0 2.5 1
Zinc 5.7J ug/L 07/13/17 20:36 7440-66-607/06/17 16:2510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 07/12/17 13:40 7440-28-007/04/17 05:505.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 21.3J ug/L 07/06/17 16:26 67-64-110010.0 1
Acrylonitrile ND ug/L 07/06/17 16:26 107-13-12001.9 1
Benzene ND ug/L 07/06/17 16:26 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/06/17 16:26 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/06/17 16:26 75-27-41.0 0.18 1
Bromoform ND ug/L 07/06/17 16:26 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/06/17 16:26 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/06/17 16:26 78-93-31000.96 1
Carbon disulfide ND ug/L 07/06/17 16:26 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/06/17 16:26 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/06/17 16:26 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/06/17 16:26 75-00-310.0 0.54 1
Chloroform ND ug/L 07/06/17 16:26 67-66-35.0 0.14 1
Chloromethane ND ug/L 07/06/17 16:26 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/06/17 16:26 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/06/17 16:26 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/06/17 16:26 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/06/17 16:26 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/06/17 16:26 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/06/17 16:26 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/06/17 16:26 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/06/17 16:26 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/06/17 16:26 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/06/17 16:26 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/06/17 16:26 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/06/17 16:26 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/06/17 16:26 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 04:59 PM
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Page 5 of 26
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92346321
BLANKS
Sample:EB Lab ID:92346321001 Collected:06/29/17 15:50 Received:06/30/17 06:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 07/06/17 16:26 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/06/17 16:26 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/06/17 16:26 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/06/17 16:26 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/06/17 16:26 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/06/17 16:26 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/06/17 16:26 108-10-11000.33 1
Styrene ND ug/L 07/06/17 16:26 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/06/17 16:26 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/06/17 16:26 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 07/06/17 16:26 127-18-41.0 0.46 1
Toluene ND ug/L 07/06/17 16:26 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/06/17 16:26 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/06/17 16:26 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/06/17 16:26 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/06/17 16:26 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/06/17 16:26 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/06/17 16:26 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/06/17 16:26 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/06/17 16:26 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %07/06/17 16:26 460-00-470-130 1
1,2-Dichloroethane-d4 (S)94 %07/06/17 16:26 17060-07-070-130 1
Toluene-d8 (S)103 %07/06/17 16:26 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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Page 6 of 26
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92346321
BLANKS
Sample:FB Lab ID:92346321002 Collected:06/29/17 15:55 Received:06/30/17 06:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 07/13/17 20:39 7440-36-007/06/17 16:256.0 3.9 1
Arsenic ND ug/L 07/13/17 20:39 7440-38-207/06/17 16:2510.0 5.0 1
Barium ND ug/L 07/13/17 20:39 7440-39-307/06/17 16:251002.5 1
Beryllium ND ug/L 07/13/17 20:39 7440-41-707/06/17 16:251.0 0.50 1
Cadmium ND ug/L 07/13/17 20:39 7440-43-907/06/17 16:251.0 0.50 1
Chromium ND ug/L 07/13/17 20:39 7440-47-307/06/17 16:2510.0 2.5 1
Cobalt ND ug/L 07/13/17 20:39 7440-48-407/06/17 16:2510.0 2.5 1
Copper ND ug/L 07/13/17 20:39 7440-50-807/06/17 16:2510.0 2.5 1
Lead ND ug/L 07/13/17 20:39 7439-92-107/06/17 16:2510.0 2.5 1
Nickel ND ug/L 07/13/17 20:39 7440-02-007/06/17 16:2550.0 2.5 1
Selenium ND ug/L 07/13/17 20:39 7782-49-207/06/17 16:2510.0 5.0 1
Silver ND ug/L 07/13/17 20:39 7440-22-407/06/17 16:2510.0 2.5 1
Vanadium ND ug/L 07/13/17 20:39 7440-62-207/06/17 16:2525.0 2.5 1
Zinc ND ug/L 07/13/17 20:39 7440-66-607/06/17 16:2510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 07/12/17 13:42 7440-28-007/04/17 05:505.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 34.1J ug/L 07/11/17 16:58 67-64-110010.0 1
Acrylonitrile ND ug/L 07/11/17 16:58 107-13-12001.9 1
Benzene ND ug/L 07/11/17 16:58 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 07/11/17 16:58 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 07/11/17 16:58 75-27-41.0 0.18 1
Bromoform ND ug/L 07/11/17 16:58 75-25-23.0 0.26 1
Bromomethane ND ug/L 07/11/17 16:58 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 07/11/17 16:58 78-93-31000.96 1
Carbon disulfide ND ug/L 07/11/17 16:58 75-15-01001.2 1
Carbon tetrachloride ND ug/L 07/11/17 16:58 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 07/11/17 16:58 108-90-73.0 0.23 1
Chloroethane ND ug/L 07/11/17 16:58 75-00-310.0 0.54 1
Chloroform ND ug/L 07/11/17 16:58 67-66-35.0 0.14 1
Chloromethane 0.44J ug/L 07/11/17 16:58 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 07/11/17 16:58 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 07/11/17 16:58 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 07/11/17 16:58 106-93-41.0 0.27 1
Dibromomethane ND ug/L 07/11/17 16:58 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 07/11/17 16:58 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 07/11/17 16:58 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 07/11/17 16:58 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 07/11/17 16:58 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 07/11/17 16:58 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 07/11/17 16:58 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 07/11/17 16:58 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 07/11/17 16:58 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 07/11/17 16:58 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 04:59 PM
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Page 7 of 26
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92346321
BLANKS
Sample:FB Lab ID:92346321002 Collected:06/29/17 15:55 Received:06/30/17 06:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 07/11/17 16:58 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 07/11/17 16:58 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 07/11/17 16:58 100-41-41.0 0.30 1
2-Hexanone ND ug/L 07/11/17 16:58 591-78-650.0 0.46 1
Iodomethane ND ug/L 07/11/17 16:58 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 07/11/17 16:58 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/11/17 16:58 108-10-11000.33 1
Styrene ND ug/L 07/11/17 16:58 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 07/11/17 16:58 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 07/11/17 16:58 79-34-53.0 0.40 1
Tetrachloroethene 0.99J ug/L 07/11/17 16:58 127-18-41.0 0.46 1
Toluene ND ug/L 07/11/17 16:58 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 07/11/17 16:58 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 07/11/17 16:58 79-00-51.0 0.29 1
Trichloroethene ND ug/L 07/11/17 16:58 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 07/11/17 16:58 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 07/11/17 16:58 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 07/11/17 16:58 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 07/11/17 16:58 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 07/11/17 16:58 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %07/11/17 16:58 460-00-470-130 1
1,2-Dichloroethane-d4 (S)94 %07/11/17 16:58 17060-07-070-130 1
Toluene-d8 (S)105 %07/11/17 16:58 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 04:59 PM
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[phone]
Page 8 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92346321
BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
367845
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92346321001, 92346321002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2038632
Associated Lab Samples:92346321001, 92346321002
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 5.0 07/13/17 19:553.9
Arsenic ug/L ND 10.0 07/13/17 19:555.0
Barium ug/L ND 5.0 07/13/17 19:552.5
Beryllium ug/L ND 1.0 07/13/17 19:550.50
Cadmium ug/L ND 1.0 07/13/17 19:550.50
Chromium ug/L ND 5.0 07/13/17 19:552.5
Cobalt ug/L ND 5.0 07/13/17 19:552.5
Copper ug/L ND 5.0 07/13/17 19:552.5
Lead ug/L ND 5.0 07/13/17 19:552.5
Nickel ug/L ND 5.0 07/13/17 19:552.5
Selenium ug/L ND 10.0 07/13/17 19:555.0
Silver ug/L ND 5.0 07/13/17 19:552.5
Vanadium ug/L ND 5.0 07/13/17 19:552.5
Zinc ug/L ND 10.0 07/13/17 19:555.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2038633LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 536500 107 80-120
Arsenic ug/L 521500 104 80-120
Barium ug/L 565500 113 80-120
Beryllium ug/L 537500 107 80-120
Cadmium ug/L 572500 114 80-120
Chromium ug/L 548500 110 80-120
Cobalt ug/L 556500 111 80-120
Copper ug/L 546500 109 80-120
Lead ug/L 547500 109 80-120
Nickel ug/L 557500 111 80-120
Selenium ug/L 558500 112 80-120
Silver ug/L 265250 106 80-120
Vanadium ug/L 529500 106 80-120
Zinc ug/L 550500 110 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2038634MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92346315006
2038635
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 106 75-125106 1 20500ND531534
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 04:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92346321
BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2038634MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92346315006
2038635
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L 500 105 75-125105 0 20500ND527530
Barium ug/L 500 116 75-125114 1 2050063412101210
Beryllium ug/L 500 107 75-125107 0 20500ND534536
Cadmium ug/L 500 113 75-125114 1 205000.63J 565 571
Chromium ug/L 500 109 75-125108 1 205008.4J 554 550
Cobalt ug/L 500 108 75-125109 1 2050056.4 597 602
Copper ug/L 500 109 75-125109 0 20500ND546546
Lead ug/L 500 105 75-125106 1 205006.1J 531 537
Nickel ug/L 500 107 75-125109 1 205004.9J 541 548
Selenium ug/L 500 105 75-125107 1 20500ND526534
Silver ug/L 250 105 75-125105 0 20250ND264263
Vanadium ug/L 500 106 75-125105 1 20500ND530526
Zinc ug/L 500 107 75-125107 0 2050033.1 569 568
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 04:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92346321
BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
367649
EPA 3010A
EPA 6020B
6020 MET
Associated Lab Samples:92346321001, 92346321002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2037807
Associated Lab Samples:92346321001, 92346321002
Matrix:Water
AnalyzedMDL
Thallium ug/L ND 0.10 07/12/17 13:030.020
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2037808LABORATORY CONTROL SAMPLE:
LCSSpike
Thallium ug/L 100100 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2037809MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92346315001
2037810
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Thallium ug/L 100 100 75-12597 3 201000.13J 100 97.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 04:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92346321
BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
367961
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92346321001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2039240
Associated Lab Samples:92346321001
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 07/06/17 15:170.33
1,1,1-Trichloroethane ug/L ND 1.0 07/06/17 15:170.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 07/06/17 15:170.40
1,1,2-Trichloroethane ug/L ND 1.0 07/06/17 15:170.29
1,1-Dichloroethane ug/L ND 5.0 07/06/17 15:170.32
1,1-Dichloroethene ug/L ND 5.0 07/06/17 15:170.56
1,2,3-Trichloropropane ug/L ND 1.0 07/06/17 15:170.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 07/06/17 15:172.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 07/06/17 15:170.27
1,2-Dichlorobenzene ug/L ND 5.0 07/06/17 15:170.30
1,2-Dichloroethane ug/L ND 1.0 07/06/17 15:170.24
1,2-Dichloropropane ug/L ND 1.0 07/06/17 15:170.27
1,4-Dichlorobenzene ug/L ND 1.0 07/06/17 15:170.33
2-Butanone (MEK)ug/L ND 100 07/06/17 15:170.96
2-Hexanone ug/L ND 50.0 07/06/17 15:170.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 07/06/17 15:170.33
Acetone ug/L ND 100 07/06/17 15:1710.0
Acrylonitrile ug/L ND 200 07/06/17 15:171.9
Benzene ug/L ND 1.0 07/06/17 15:170.25
Bromochloromethane ug/L ND 3.0 07/06/17 15:170.17
Bromodichloromethane ug/L ND 1.0 07/06/17 15:170.18
Bromoform ug/L ND 3.0 07/06/17 15:170.26
Bromomethane ug/L ND 10.0 07/06/17 15:170.29
Carbon disulfide ug/L ND 100 07/06/17 15:171.2
Carbon tetrachloride ug/L ND 1.0 07/06/17 15:170.25
Chlorobenzene ug/L ND 3.0 07/06/17 15:170.23
Chloroethane ug/L ND 10.0 07/06/17 15:170.54
Chloroform ug/L ND 5.0 07/06/17 15:170.14
Chloromethane ug/L ND 1.0 07/06/17 15:170.11
cis-1,2-Dichloroethene ug/L ND 5.0 07/06/17 15:170.19
cis-1,3-Dichloropropene ug/L ND 1.0 07/06/17 15:170.13
Dibromochloromethane ug/L ND 3.0 07/06/17 15:170.21
Dibromomethane ug/L ND 10.0 07/06/17 15:170.21
Ethylbenzene ug/L ND 1.0 07/06/17 15:170.30
Iodomethane ug/L ND 10.0 07/06/17 15:170.32
Methylene Chloride ug/L ND 1.0 07/06/17 15:170.97
Styrene ug/L ND 1.0 07/06/17 15:170.26
Tetrachloroethene ug/L ND 1.0 07/06/17 15:170.46
Toluene ug/L ND 1.0 07/06/17 15:170.26
trans-1,2-Dichloroethene ug/L ND 5.0 07/06/17 15:170.49
trans-1,3-Dichloropropene ug/L ND 1.0 07/06/17 15:170.26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 04:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92346321
BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2039240
Associated Lab Samples:92346321001
Matrix:Water
AnalyzedMDL
trans-1,4-Dichloro-2-butene ug/L ND 100 07/06/17 15:171.0
Trichloroethene ug/L ND 1.0 07/06/17 15:170.47
Trichlorofluoromethane ug/L ND 1.0 07/06/17 15:170.20
Vinyl acetate ug/L ND 50.0 07/06/17 15:170.35
Vinyl chloride ug/L ND 1.0 07/06/17 15:170.62
Xylene (Total)ug/L ND 5.0 07/06/17 15:170.66
1,2-Dichloroethane-d4 (S)%93 70-130 07/06/17 15:17
4-Bromofluorobenzene (S)%98 70-130 07/06/17 15:17
Toluene-d8 (S)%102 70-130 07/06/17 15:17
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2039241LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 56.750 113 80-125
1,1,1-Trichloroethane ug/L 55.950 112 71-129
1,1,2,2-Tetrachloroethane ug/L 55.050 110 79-124
1,1,2-Trichloroethane ug/L 58.150 116 85-125
1,1-Dichloroethane ug/L 52.650 105 73-126
1,1-Dichloroethene ug/L 55.250 110 66-135
1,2,3-Trichloropropane ug/L 53.350 107 75-130
1,2-Dibromo-3-chloropropane ug/L 53.250 106 71-133
1,2-Dibromoethane (EDB)ug/L 59.550 119 83-124
1,2-Dichlorobenzene ug/L 56.850 114 80-133
1,2-Dichloroethane ug/L 50.150 100 67-128
1,2-Dichloropropane ug/L 58.450 117 75-132
1,4-Dichlorobenzene ug/L 56.750 113 78-130
2-Butanone (MEK)ug/L 121100 121 61-144
2-Hexanone ug/L 111100 111 68-143
4-Methyl-2-pentanone (MIBK)ug/L 109100 109 72-135
Acetone ug/L 128100 128 48-146
Acrylonitrile ug/L 271250 109 40-160
Benzene ug/L 59.750 119 80-125
Bromochloromethane ug/L 58.150 116 71-125
Bromodichloromethane ug/L 56.750 113 78-124
Bromoform ug/L 57.650 115 71-128
Bromomethane ug/L 43.750 87 40-160
Carbon disulfide ug/L 58.4J50 117 50-160
Carbon tetrachloride ug/L 55.650 111 69-131
Chlorobenzene ug/L 55.550 111 81-122
Chloroethane ug/L 42.550 85 39-148
Chloroform ug/L 55.150 110 73-127
Chloromethane ug/L 51.450 103 44-146
cis-1,2-Dichloroethene ug/L 54.950 110 74-124
cis-1,3-Dichloropropene ug/L 59.550 119 72-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 04:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92346321
BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2039241LABORATORY CONTROL SAMPLE:
LCSSpike
Dibromochloromethane ug/L 60.450 121 78-125
Dibromomethane ug/L 56.250 112 82-120
Ethylbenzene ug/L 55.650 111 79-121
Iodomethane ug/L 97.2100 97 39-154
Methylene Chloride ug/L 57.150 114 64-133
Styrene ug/L 56.450 113 84-126
Tetrachloroethene ug/L 54.350 109 78-122
Toluene ug/L 55.650 111 80-121
trans-1,2-Dichloroethene ug/L 53.650 107 71-127
trans-1,3-Dichloropropene ug/L 61.050 122 69-141
trans-1,4-Dichloro-2-butene ug/L 75.3J50 151 40-160
Trichloroethene ug/L 54.150 108 78-122
Trichlorofluoromethane ug/L 48.950 98 53-137
Vinyl acetate ug/L 115100 115 40-160
Vinyl chloride ug/L 48.350 97 58-137
Xylene (Total)ug/L 164150 109 81-126
1,2-Dichloroethane-d4 (S)%90 70-130
4-Bromofluorobenzene (S)%96 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2039244MATRIX SPIKE SAMPLE:
MSSpike
Result
92346168001
1,1,1,2-Tetrachloroethane ug/L 18.220 91 70-130ND
1,1,1-Trichloroethane ug/L 19.420 97 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19.320 97 70-130ND
1,1,2-Trichloroethane ug/L 20.320 101 70-130ND
1,1-Dichloroethane ug/L 18.620 93 70-130ND
1,1-Dichloroethene ug/L 19.820 99 70-166ND
1,2,3-Trichloropropane ug/L 19.120 96 70-130ND
1,2-Dibromo-3-chloropropane ug/L 19.520 98 70-130ND
1,2-Dibromoethane (EDB)ug/L 19.720 99 70-130ND
1,2-Dichlorobenzene ug/L 18.720 94 70-130ND
1,2-Dichloroethane ug/L 16.720 83 70-130ND
1,2-Dichloropropane ug/L 19.520 98 70-130ND
1,4-Dichlorobenzene ug/L 21.820 93 70-1303.2
2-Butanone (MEK)ug/L 38.7J40 97 70-130ND
2-Hexanone ug/L 36.3J40 91 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 36.3J40 91 70-130ND
Acetone ug/L 70.1J40 115 70-13024.0J
Acrylonitrile ug/L 98.0J100 98 70-130ND
Benzene ug/L 21.420 103 70-1480.92J
Bromochloromethane ug/L 20.620 103 70-130ND
Bromodichloromethane ug/L 19.820 99 70-130ND
Bromoform ug/L 18.320 91 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 04:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92346321
BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2039244MATRIX SPIKE SAMPLE:
MSSpike
Result
92346168001
Bromomethane ug/L 15.520 78 70-130ND
Carbon disulfide ug/L 21.4J20 107 70-130ND
Carbon tetrachloride ug/L 20.120 101 70-130ND
Chlorobenzene ug/L 20.120 100 70-146ND
Chloroethane ug/L 16.620 83 70-130ND
Chloroform ug/L 19.820 99 70-130ND
Chloromethane ug/L 18.220 87 70-1300.94J
cis-1,2-Dichloroethene ug/L 20.320 95 70-1301.2J
cis-1,3-Dichloropropene ug/L 18.420 92 70-130ND
Dibromochloromethane ug/L 18.920 95 70-130ND
Dibromomethane ug/L 21.520 107 70-130ND
Ethylbenzene ug/L 20.420 102 70-130ND
Iodomethane ug/L 31.840 80 70-130ND
Methylene Chloride ug/L 18.220 91 70-130ND
Styrene ug/L 20.020 100 70-130ND
Tetrachloroethene ug/L 20.620 103 70-130ND
Toluene ug/L 20.220 101 70-155ND
trans-1,2-Dichloroethene ug/L 20.620 103 70-130ND
trans-1,3-Dichloropropene ug/L 18.220 91 70-130ND
trans-1,4-Dichloro-2-butene ug/L 17.9J20 90 70-130ND
Trichloroethene ug/L 19.620 98 69-151ND
Trichlorofluoromethane ug/L 18.920 95 70-130ND
Vinyl acetate ug/L 29.6J40 74 70-130ND
Vinyl chloride ug/L 18.520 93 70-130ND
1,2-Dichloroethane-d4 (S)%89 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92346206002
2039243SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 04:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 15 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92346321
BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92346206002
2039243SAMPLE DUPLICATE:
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L 2.8J 302.1J
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 1.3J 301.3J
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L 779 1 30774
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%97 494
4-Bromofluorobenzene (S)%97 097
Toluene-d8 (S)%101 1102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 04:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92346321
BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
368539
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92346321002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2042426
Associated Lab Samples:92346321002
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 07/11/17 16:060.33
1,1,1-Trichloroethane ug/L ND 1.0 07/11/17 16:060.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 07/11/17 16:060.40
1,1,2-Trichloroethane ug/L ND 1.0 07/11/17 16:060.29
1,1-Dichloroethane ug/L ND 5.0 07/11/17 16:060.32
1,1-Dichloroethene ug/L ND 5.0 07/11/17 16:060.56
1,2,3-Trichloropropane ug/L ND 1.0 07/11/17 16:060.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 07/11/17 16:062.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 07/11/17 16:060.27
1,2-Dichlorobenzene ug/L ND 5.0 07/11/17 16:060.30
1,2-Dichloroethane ug/L ND 1.0 07/11/17 16:060.24
1,2-Dichloropropane ug/L ND 1.0 07/11/17 16:060.27
1,4-Dichlorobenzene ug/L ND 1.0 07/11/17 16:060.33
2-Butanone (MEK)ug/L ND 100 07/11/17 16:060.96
2-Hexanone ug/L ND 50.0 07/11/17 16:060.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 07/11/17 16:060.33
Acetone ug/L ND 100 07/11/17 16:0610.0
Acrylonitrile ug/L ND 200 07/11/17 16:061.9
Benzene ug/L ND 1.0 07/11/17 16:060.25
Bromochloromethane ug/L ND 3.0 07/11/17 16:060.17
Bromodichloromethane ug/L ND 1.0 07/11/17 16:060.18
Bromoform ug/L ND 3.0 07/11/17 16:060.26
Bromomethane ug/L ND 10.0 07/11/17 16:060.29
Carbon disulfide ug/L ND 100 07/11/17 16:061.2
Carbon tetrachloride ug/L ND 1.0 07/11/17 16:060.25
Chlorobenzene ug/L ND 3.0 07/11/17 16:060.23
Chloroethane ug/L ND 10.0 07/11/17 16:060.54
Chloroform ug/L ND 5.0 07/11/17 16:060.14
Chloromethane ug/L ND 1.0 07/11/17 16:060.11
cis-1,2-Dichloroethene ug/L ND 5.0 07/11/17 16:060.19
cis-1,3-Dichloropropene ug/L ND 1.0 07/11/17 16:060.13
Dibromochloromethane ug/L ND 3.0 07/11/17 16:060.21
Dibromomethane ug/L ND 10.0 07/11/17 16:060.21
Ethylbenzene ug/L ND 1.0 07/11/17 16:060.30
Iodomethane ug/L ND 10.0 07/11/17 16:060.32
Methylene Chloride ug/L ND 1.0 07/11/17 16:060.97
Styrene ug/L ND 1.0 07/11/17 16:060.26
Tetrachloroethene ug/L ND 1.0 07/11/17 16:060.46
Toluene ug/L ND 1.0 07/11/17 16:060.26
trans-1,2-Dichloroethene ug/L ND 5.0 07/11/17 16:060.49
trans-1,3-Dichloropropene ug/L ND 1.0 07/11/17 16:060.26
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 04:59 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 17 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92346321
BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2042426
Associated Lab Samples:92346321002
Matrix:Water
AnalyzedMDL
trans-1,4-Dichloro-2-butene ug/L 1.0J 100 07/11/17 16:061.0
Trichloroethene ug/L ND 1.0 07/11/17 16:060.47
Trichlorofluoromethane ug/L ND 1.0 07/11/17 16:060.20
Vinyl acetate ug/L ND 50.0 07/11/17 16:060.35
Vinyl chloride ug/L ND 1.0 07/11/17 16:060.62
Xylene (Total)ug/L ND 5.0 07/11/17 16:060.66
1,2-Dichloroethane-d4 (S)%97 70-130 07/11/17 16:06
4-Bromofluorobenzene (S)%101 70-130 07/11/17 16:06
Toluene-d8 (S)%105 70-130 07/11/17 16:06
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2042427LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.850 100 80-125
1,1,1-Trichloroethane ug/L 48.050 96 71-129
1,1,2,2-Tetrachloroethane ug/L 47.350 95 79-124
1,1,2-Trichloroethane ug/L 48.750 97 85-125
1,1-Dichloroethane ug/L 44.650 89 73-126
1,1-Dichloroethene ug/L 42.150 84 66-135
1,2,3-Trichloropropane ug/L 48.850 98 75-130
1,2-Dibromo-3-chloropropane ug/L 47.950 96 71-133
1,2-Dibromoethane (EDB)ug/L 52.550 105 83-124
1,2-Dichlorobenzene ug/L 50.450 101 80-133
1,2-Dichloroethane ug/L 43.150 86 67-128
1,2-Dichloropropane ug/L 48.850 98 75-132
1,4-Dichlorobenzene ug/L 48.250 96 78-130
2-Butanone (MEK)ug/L 101100 101 61-144
2-Hexanone ug/L 104100 104 68-143
4-Methyl-2-pentanone (MIBK)ug/L 93.7J100 94 72-135
Acetone ug/L 122100 122 48-146
Acrylonitrile ug/L 229250 92 40-160
Benzene ug/L 48.450 97 80-125
Bromochloromethane ug/L 47.250 94 71-125
Bromodichloromethane ug/L 48.350 97 78-124
Bromoform ug/L 43.850 88 71-128
Bromomethane ug/L 51.050 102 40-160
Carbon disulfide ug/L 45.7J50 91 50-160
Carbon tetrachloride ug/L 45.250 90 69-131
Chlorobenzene ug/L 48.350 97 81-122
Chloroethane ug/L 44.750 89 39-148
Chloroform ug/L 47.550 95 73-127
Chloromethane ug/L 38.950 78 44-146
cis-1,2-Dichloroethene ug/L 44.950 90 74-124
cis-1,3-Dichloropropene ug/L 51.950 104 72-132
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 04:59 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 18 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92346321
BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2042427LABORATORY CONTROL SAMPLE:
LCSSpike
Dibromochloromethane ug/L 50.650 101 78-125
Dibromomethane ug/L 47.950 96 82-120
Ethylbenzene ug/L 47.650 95 79-121
Iodomethane ug/L 85.6100 86 39-154
Methylene Chloride ug/L 46.550 93 64-133
Styrene ug/L 48.350 97 84-126
Tetrachloroethene ug/L 47.750 95 78-122
Toluene ug/L 48.350 97 80-121
trans-1,2-Dichloroethene ug/L 45.550 91 71-127
trans-1,3-Dichloropropene ug/L 47.950 96 69-141
trans-1,4-Dichloro-2-butene ug/L 78.0J50 156 40-160
Trichloroethene ug/L 48.150 96 78-122
Trichlorofluoromethane ug/L 42.150 84 53-137
Vinyl acetate ug/L 107100 107 40-160
Vinyl chloride ug/L 39.150 78 58-137
Xylene (Total)ug/L 143150 96 81-126
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2042429MATRIX SPIKE SAMPLE:
MSSpike
Result
92346661001
1,1,1,2-Tetrachloroethane ug/L 21.220 106 70-130ND
1,1,1-Trichloroethane ug/L 22.520 112 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.920 104 70-130ND
1,1,2-Trichloroethane ug/L 21.820 109 70-130ND
1,1-Dichloroethane ug/L 21.620 108 70-130ND
1,1-Dichloroethene ug/L 23.320 117 70-166ND
1,2,3-Trichloropropane ug/L 21.120 105 70-130ND
1,2-Dibromo-3-chloropropane ug/L 20.620 103 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.820 109 70-130ND
1,2-Dichlorobenzene ug/L 22.120 111 70-130ND
1,2-Dichloroethane ug/L 21.920 110 70-130ND
1,2-Dichloropropane ug/L 22.920 115 70-130ND
1,4-Dichlorobenzene ug/L 22.420 112 70-130ND
2-Butanone (MEK)ug/L 40.6J40 101 70-130ND
2-Hexanone ug/L 39.6J40 99 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 41.0J40 102 70-130ND
Acetone ug/L 61.9J M14015570-130ND
Acrylonitrile ug/L 103J100 103 70-130ND
Benzene ug/L 22.920 114 70-148ND
Bromochloromethane ug/L 22.820 114 70-130ND
Bromodichloromethane ug/L 22.520 112 70-130ND
Bromoform ug/L 18.520 93 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 04:59 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 19 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92346321
BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2042429MATRIX SPIKE SAMPLE:
MSSpike
Result
92346661001
Bromomethane ug/L 16.420 82 70-130ND
Carbon disulfide ug/L 22.9J20 114 70-130ND
Carbon tetrachloride ug/L 23.520 117 70-130ND
Chlorobenzene ug/L 21.620 108 70-146ND
Chloroethane ug/L 20.320 102 70-130ND
Chloroform ug/L 21.420 107 70-130ND
Chloromethane ug/L 19.520 96 70-130ND
cis-1,2-Dichloroethene ug/L 22.420 112 70-130ND
cis-1,3-Dichloropropene ug/L 22.620 113 70-130ND
Dibromochloromethane ug/L 21.220 106 70-130ND
Dibromomethane ug/L 21.320 106 70-130ND
Ethylbenzene ug/L 22.220 111 70-130ND
Iodomethane ug/L 34.540 86 70-130ND
Methylene Chloride ug/L 21.020 105 70-130ND
Styrene ug/L 21.220 106 70-130ND
Tetrachloroethene ug/L 22.920 115 70-130ND
Toluene ug/L 22.520 113 70-155ND
trans-1,2-Dichloroethene ug/L 23.020 115 70-130ND
trans-1,3-Dichloropropene ug/L 22.320 111 70-130ND
trans-1,4-Dichloro-2-butene ug/L 23.8J20 119 70-130ND
Trichloroethene ug/L 24.020 120 69-151ND
Trichlorofluoromethane ug/L 24.720 123 70-130ND
Vinyl acetate ug/L 44.1J40 110 70-130ND
Vinyl chloride ug/L 19.820 99 70-130ND
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92346835001
2042428SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 300.52J
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L 0.79J 300.72J
2-Butanone (MEK)ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 04:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 26
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92346321
BLANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92346835001
2042428SAMPLE DUPLICATE:
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L 0.50J 30ND
cis-1,2-Dichloroethene ug/L 0.93J 300.99J
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 300.69J
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L 11.6 2 3011.4
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%96 096
4-Bromofluorobenzene (S)%102 1103
Toluene-d8 (S)%102 0101
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 04:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 26
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92346321
BLANKS
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 04:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 26
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92346321
BLANKS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92346321001 367845 368492EBEPA 3010A EPA 6010
92346321002 367845 368492FBEPA 3010A EPA 6010
92346321001 367649 368460EBEPA 3010A EPA 6020B
92346321002 367649 368460FBEPA 3010A EPA 6020B
92346321001 367961EBEPA 8260
92346321002 368539FBEPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/14/2017 04:59 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 26
Page 24 of 26
Page 25 of 26
Page 26 of 26
Appendix B
Field Sampling Parameter Data Sheet(s)