8606_SurryCounty_MSWLF_GWMR_20171031

Surry County Subtitle D Lined MSWLF
Mt. Airy, North Carolina
May 2017
Permit Number: 86-06
Semi-Annual Water Quality Monitoring Report
Prepared for
Municipal Engineering Services Company, P.A.Garner and Boone, North Carolina
MESCO Project Number: G17025.0
P.O. Box 97
Garner, NC 27529
License No. C-0281

TABLE OF CONTENTS
SECTION
Introduction Page 1
Background Page 1
MW-2 Area Investigations Page 2
MW-6R Area Investigations Page 2
MW-9S Area Investigations Page 2
Sampling Procedures Page 2
Field Parameter Data Page 3
Laboratory Results Page 3
Quality Control Samples Page 3
Groundwater Samples Page 4
Surface Water Samples Page 4
Leachate Samples Page 4
Groundwater and Surface Water Characterization Page 5
Findings Page 5
Closing Page 6
SHEETS
Topographic Map with Site Location Sheet 1
Single Event Potentiometric Map of Uppermost Aquifer Sheet 2
TABLES
Groundwater Monitoring Well Construction Table Table 1
Field Observations of Monitoring Locations Table 2
Field Parameter Data Summary Table 3
Sampling and Analysis Summary Table 4
Groundwater, Leachate and QC Sample Detections Table 5
Surface Water Sample Detections Table 6
Hydrologic Properties at Monitoring Well Locations Table 7
APPENDICIES
Laboratory Analysis Report and Chains of Custody Appendix A
Field Sampling Data Sheet(s) Appendix B
October 31, 2017
Ms. Jaclynne Drummond
Solid Waste Section (SWS)
Division of Waste Management
North Carolina Department of Environmental Quality (NCDEQ)
2090 US Highway 70
Swannanoa, NC 28778
Re: Semi-Annual Water Quality Monitoring Report
Surry County Subtitle D Lined MSWLF, Phases 1 & 2
Permit No. 86-06
MESC0 Project No. G17025.0
Sampling Date(s). May 30-June 1, 2017
Dear Ms Drummond:
Introduction
On behalf of Surry County, Municipal Engineering Services Company, P.A. (MESCO) is pleased to present this
Semi-Annual Water Quality Monitoring Report for an event performed at the Surry County Subtitle D Lined
Municipal Solid Waste Landfill (MSWLF) in the spring of 2017. NCDEQ Solid Waste Rules 15A NCAC 13B.1632
requires that Surry County provide this report to the SWS on a semi-annual basis. This report documents the quality
of the ground and surface waters during this monitoring event performed on May 30-June 1, 2017. A verification
sample was collected from MW-3R in response to detections of semivolatile compounds which were suspected to be
false positives. Assessment monitoring (targeting Appendix II constituents) was initiated site-wide during the
previous spring event (May 2016) and was performed again during this event in response to VOC(s) detected in a
few downgradient wells. The laboratory analytical results indicate that samples collected from two downgradient
wells continue to contain levels of vinyl chloride above NC 2L Groundwater Standards. All detections remain
below Federal “Drinking Water Standards”, contaminants continue to be low in leachate samples and all the surface
water samples continue to appear unimpacted.
Background
The Surry County Subtitle D lined MSWLF, permit #86-06, is located at 237 Landfill Road, Mount Airy, Surry
County, North Carolina. The site location topographic map is depicted in the attached Sheet 1. The lined MSWLF
is comprised of contiguous Phases 1 & 2 which are treated as a single unit in this report.
Water quality at this facility has been monitored at least semi-annually since 1998 with all historical data reviewed
in support of this report. This event was performed in accordance with the NC SWS rules/regulations as
promulgated in 15A NCAC 13B and as a condition of the permit to operate.

As specified within 15A NCAC 13B.1632(j), the SWS Environmental Monitoring Report Form and SWS
memorandums this report contains sampling procedures, field and laboratory results, groundwater and surface water
characterization. Well construction summary table, field observations table, field parameter data table, sampling
and analysis summary table, detections compared to Standards tables, a groundwater flow directions/rates table,
potentiometric map, quality assurance/quality control data, and laboratory analytical data results are enclosed herein.
MW-2 Area Investigations
During this event MESCO investigated the area around MW-2 in an attempt to identify the source of low “j”
qualified concentrations of VOCs detected in samples collected from MW-2. The double lined leachate lagoon
leak detection manhole was observed to be dry, indicating the lagoon has not leaked. Evidence has never been
found suggesting that the lagoon has overflowed. During this and the previous event no constituents were detected
in MW-2 above regulatory Standards. Supplemental surface water sample (SW-A), collected downgradient of MW-
2 continues to appear unimpaired.
MW-6R Area Investigations
During this event MESCO investigated the area around MW-6R in an attempt to identify the source of VOC
detections. MW-6R is located in a ditch that previously conveyed stormwater originating from the lined landfill.
During the construction of Phased 2 in 2009, stormwater originating near the landfill was rerouted so that it no
longer flows adjacent to MW-6R. Landfill gas (LFG) has been detected in migration monitoring probe MGP-5
located less than 75 feet away from MW-6R. Active LFG extraction has been initiated at Lined Phase 1 which
includes vacuum applied at the closest leachate collection system cleanout. Vinyl chloride was detected in sample
MW-6R during this and the previous 8 events above the 2L Standard. There were no detections in a supplemental
surface water sample (SW-B) collected downgradient of MW-6R.
MW-9S Area Investigations
MESCO investigated the area around MW-9S in an attempt to identify the source of VOC detections during this
event. MW-9S is located about 180 feet downgradient of the Phase 2 sump near a previous drainage feature. Low
levels of chlorinated hydrocarbons have consistently been detected in samples collected from MW-9S since before
waste was deposited in Phase 2. Vinyl chloride was detected in sample MW-9S during this and the previous 5
events above the 2L Standard.. VOCs remain absent in the adjacent deeper cluster well MW-9D. LFG has never
been detected from head-space of MW-9S or from adjacent migration probe MGP-12.
Sampling Procedure
MESCO personnel performed this sampling event using portable monitoring methodology in general accordance
with the site-specific SAP from the Phase 2 Design Hydrogeologic Study, approved June 13, 2008. Water samples
were collected from 14 downgradient groundwater monitoring wells (MW-2R, MW-3, MW-4S, MW-4D, MW-5,
MW-6R, MW-8, MW-9S, MW-9D, MW-10, MW-11S, MW-11D, MW-12 and MW-13), one background well
(MW-1), four downstream surface water locations (SW-4 , SWN-2, SW-A and SW-B), four upstream surface water
points (SWN-1, SW-1, SW-2 and SW-3) and a pre-treated leachate sample (LAGOON). Surface water points
SWN-3 and SWN-4 were not sampled because they were dry. Quality control measures included analysis of
equipment blanks (EB) field blanks (FB) and trip blanks (TB). Sampling locations are shown on the potentiometric
map (Sheet 2).
A summary detailing the construction of the water monitoring wells is presented on Table 1. The function and
integrity of all monitoring locations were visually evaluated and no deficiencies identified as documented on Table
2. The depth to water in each well was electronically gaged prior to purging to quantify the static water level
elevation. Low-flow pumping methodology or bailing was utilized to adequately purge the wells to a minimum of
2
three times the volume of standing water in the well or until dry. Surface water samples were collected from Stoney
Creek discharge feature at previously designated locations. During well purging and surface water sample
collection the required field parameters were recorded. The samples were then placed into laboratory-prepared, pre-
preserved containers via a new disposable polyethylene bailer. Samples were collected, kept on ice, and transported
to a NC-certified laboratory under proper C-O-C protocols within the specified hold times for each analysis.
Field Parameter Data
Stabilized field parameters were recorded during purging which included pH, specific conductance, temperature
and visual turbidity. A summary of the field parameter data is presented in Table 3 and the field sampling data
sheet is enclosed in Appendix B.
Laboratory Results
Pace Analytical Services, Inc. (PACE) of Huntersville and Asheville NC performed the laboratory analysis of the
water and leachate samples. Prism Laboratory of Charlotte NC performed the laboratory testing of the MW-3R
verification sample. All groundwater samples were analyzed for the current 40 CFR 258 Appendix II list of
constituents. Surface wasters were tested for the parameters listed in 40 CFR 258 Appendix I. Untreated leachate
was tested for the specific parameters required by the SWS which includes VOCs, total metals, phosphorous, BOD,
COD, sulfide and nitrate. A sampling and analysis table summarizing the locations, constituents and methods is
presented as Table 4.
Water samples were analyzed to the laboratory-established Method Detection Limits (MDL), which are at or below
the current Solid Waste Section Limit (SWSL). Table 5 summarizes constituents detected in groundwater, leachate
and QC samples that attain or were above the current SWSL, SWS adopted Groundwater Protection Standards
(GWP), North Carolina Groundwater Standards (2L) or the Maximum Contaminant Level (MCL) commonly
referenced as the Federal “Drinking Water Standard”. Table 6 lists the constituents detected in surface water
samples compared SWSL, the North Carolina Surface Water Standards (2B) for a Class C water-body and the MCL.
Quality Control Samples
Acetone was detected in EB and FB and chloromethane was found in TB. Acetone was also detected in the majority
of ground and surface water samples in comparable levels which is inconsistent with previous events. The
detections of acetone are believed to be lab induced false positives. Since acetone levels were below regulatory
Standards the acetone detections are largely inconsequential for compliance purposes.
3
Groundwater Samples
Metals
Five metals were detected above the NC 2L/GWP Standard in samples collected from 6 wells, including the
background well, as summarized in the following table.
Metals Detected Above 2L/GWP Standards in Groundwater
Cd Cr Co Tl Va
SWSL 1 10 10 5.5 25
2L/GWP STD.2 10 1 0.28 0.3
MW-1(BG Well)15.8 10.1 14.2 j
MW-4S 4.6 5.3 j
MW-6R
MW-9S 134 0.32 j
MW-10 4 j
MW-11D 10.2 j
Concentrations in ug/L. j = “j-qualified” since below the SWSL thus value is considered an estimate
Volatile Organic Compounds
Vinyl chloride was detected above the NC 2L Standard in samples collected from MW-6R and MW-9S as
summarized in the following table.
VOCs Detected Above 2L Standards in Groundwater Samples
Vinyl Chloride
SWSL 1
2L STD.0.03
MW-6R 1.3
MW-9S 0.67 j
Concentrations in ug/L. j = “j-qualified” since below the SWSL thus value is considered an estimate
Nineteen SVOCs were detected in non-quantifiable (“j-fagged”) with nine above 2L Standards in samples collected
from MW-3R on May 31, 2017. However, no SVOCs were detected from a verification sample collected from
MW-3R on July 8, 2017.
Surface Water Samples
Contaminants were not detected above NC 2B Surface Water Standards in any of the surface water samples.
Leachate Samples
Contaminants including four VOCs above 2L Standards were detected in leachate samples. Contaminant
concentrations detected in leachate samples were higher relative to historical levels with 3 VOCs and 4 metals at
unprecedented levels.
4
Groundwater and Surface Water Characterization
A potentiometric map of the uppermost aquifer constructed from groundwater elevation data recorded during this
monitoring event is on Sheet 2. Groundwater flow rates and directions were calculated and are included in the
hydrologic properties table (Table 7). Groundwater flow directions remain generally in a southerly direction
towards the Ararat River with groundwater velocities calculated by modified Darcy's equation varied considerably
due to the anisotropic geologic conditions. Streams located within the facility boundaries were observed to be of
high volume and flow with low turbidity in response to recent rainfall.
Findings
The inorganic detections are believed to be a product of erosion of natural deposits and not an anthropogenic source.
An ASD which provides technical site specific facts and site specific analytical data including evaluations of
interwell (background), intrawell (baseline), metals in leachate, dissolved compared to total metals and a discussion
that substantiating evidence that the metals are not anthropogenic was not approved by the SWS. The SWS
requested that the ASD be amended to include additional information. More time will be needed to collect
additional field data prior to amending the ASD.
Vinyl chloride has been detected above the 2L Standard in every sample collected from MW-6R over the past 10
events (5 years). Concentrations reported during this event were 1.3 ug/L which is within the historically identified
range (0.88-1.4). MW-6R is located approximately 100 feet downgradient of the Phase 2 liner and within the
compliance boundary. The portion of the aquifer impacted is believed to be small as evidenced by lack of detections
in MW-8 located along the downgradient flow path. The active LFG extraction system is expected to operate
indefinitely which may reduce levels of LFG migrating through the vadose which may mitigate potential
groundwater impacts.
Levels of PCE have been below the 2L Standard in samples collected from MW-2 during the past three events.
MW-2 is located approximately 75 feet downgradient of the leachate lagoon and within the compliance boundary.
Surface water point SW-A, collected directly downgradient of MW-2 tested clean. Based upon all available
evidence, it is unlikely that the contaminants detected in this area will migrate beyond the compliance boundary
which extends beyond the large perennial discharge feature. The discharge feature is expected to remain
unimpacted as all levels of contaminants ever detected in any downgradient groundwater sample are already below
their respective 2B Surface Water Standard.
Vinyl chloride was detected in a sample collected from MW-9S above its 2L Standard for the sixth consecutive
event. Levels reported during this event were the lowest detected which is within the historically identified range of
0.67-1.3 ug/L. Samples collected from MW-9S has consistently contained low levels of chlorinated solvents for
more than five years including before Phase 2 was opened.
Interpretation of results of surface water samples collected along Stoney Creek, including those newly instituted
directly downgradient of MW-2 and MW-6R, continue to indicate the local discharge feature remains unimpacted.
Although not applicable for regulatory compliance purposes it should be noted that no contaminants were detected
above Federally established “Drinking Water Standards”.
5
Sheets
Topographic Map with Site Location
SHEET 1
Surry County Landfill, Mt. Airy
237 Landfill Road
Mount Airy, NC 28621
Lat: 36-26-30.065
Long:-80-34-15.314
Northing:983356.18
Easting:1537885.48
Closed Unlined C&D Landfill
Closed Unlined Sanitary Landfill
Active Lined MSW Landfill
Surry Co Property Line
P.O. BOX 97 GARNER, N.C. 27529
[phone] [phone]
P.O. BOX 349 BOONE, N.C. 28607
LICENSE NUMBER: C-0281SHEET 2MMMSW-3SW-1SW-4MW-3RIW-3MW-15MW-16MW-22MW-23MW-21MW-19MW-12SMW-12D1013.01983.38990.94959.91983.951023.54937.26948.69957.88975.32925.48933.22937.38910.18922.43941.72938.64958.451062.90IW-4919.14*974.59*933.09*923.491027.91933.89IW-5DRY974.60945.52990.47IW-1IW-2MW-17947.85933.80*
Table
Table 1
Groundwater Monitoring Well Construction Table
May 31 - June 1, 2017
Well
Diameter
Total Well
Depth
Top of
Screen
Depth
Screen
Length
Top of
Casing
Elevation
Ground
Elevation
Groundwater
Elevation
Depth to
Water
(inches) (ft bgs) (ft bgs) (ft) (ft amsl) (ft amsl) (ft amsl) (ft btoc)
MW-1 8/14/98 2 68.5 53.5 15 Rock 1127.02 1124.23 1062.90 64.12 36.434494 -80.577989
MW-2 8/16/98 2 23.5 8.5 15 Rock 936.68 933.91 923.49 13.19 36.430833 -80.571161
MW-3R 12/2/98 2 20 5 15 Rock 930.00 928.15 925.48 4.52 36.430714 -80.571575
MW-4S 8/11/98 2 20 5 15 Saprolite 943.23 940.31 933.22 10.01 36.430853 -80.572400
MW-4D 8/11/98 2 45 35 10 Rock 942.80 940.31 933.09 9.71 36.430853 -80.572400
MW-5 8/18/98 2 47.5 32.5 15 Rock 977.86 971.57 933.89 43.97 36.430356 -80.572961
MW-6R 3/22/99 2 79 64 15 Fractured Rock 1004.75 1001.81 937.38 67.37 36.429958 -80.573508
MW-8 9/1/09 2 70.75 55.75 15 Fractured Rock 971.03 968.35 910.18 60.85 36.429283 -80.573453
MW-9S 6/16/06 2 42.28 27.28 15 Fractured Rock 952.83 949.75 922.43 30.40 36.429314 -80.574464
MW-9D 6/16/06 2 65.54 55.54 10 Competent Rock 952.47 949.49 919.14 33.33 36.429314 -80.574464
MW-10 6/16/06 2 47.13 27.13 20 Fractured Rock 970.24 967.35 941.72 28.52 36.429519 -80.575486
MW-11S 9/3/09 2 46.05 31.05 15 Competent Rock 969.09 965.95 938.64 30.45 36.430197 -80.577131
MW-11D 9/3/09 2 65.31 55.31 10 Competent Rock 965.38 962.38 933.80 31.58 36.430197 -80.577131
MW-12 9/4/09 2 65 50 15 Competent Rock 996.66 993.71 945.52 51.14 36.429831 -80.576750
MW-13 9/3/09 2 36.31 21.31 15 Fractured Rock 983.13 979.83 958.45 24.68 36.430625 -80.578531
MLW-A 8/19/98 2 84 69 15 Competent Rock 1095.51 1092.51 #VALUE! NR 36.432881 -80.573539
P2-6S 6/7/06 2 66.38 51.38 15 Fractured Rock 1040.27 1037.36 983.99 56.28 36.431019 -80.578025
P2-6D 6/7/06 2 93.98 83.98 10 Competent Rock 1040.65 1037.56 975.67 64.98 36.431019 -80.578025
P2-11S 6/16/06 2 50.13 40.13 10 Competent Rock 1021.53 1018.40 972.32 49.21 36.430197 -80.577131
P2-11D 6/16/06 2 65.45 60.45 5 Competent Rock 1021.13 1018.73 971.45 49.68 36.430197 -80.577131
P2-12 6/16/06 2 59.56 44.56 15 Competent Rock 986.61 983.54 934.12 52.49 36.429831 -80.576750
NOTE:
1. Ground, datum and TOR elevations are in units of feet, well diameter are in units of inches.
bgs = below ground surface
amsl= above mean sea level
btoc = below top of casing (PVC well casing)
Monitoring
Well
Date
Installed
Geology of
Screened
Interval
Latitude Longitude
Surry County Subtitle D MSWLF Page 1 of 1
Table 2
Field Observations of Monitoring Locations
May 31 - June 1, 2017
Sample
Location
Viable
Monitoring
Location
Lack of Any
Evidence of
Tampering
Locked on
Arrival &
Departure
Hinge/Hasp
Operational
Tagged
or
Labeled
Concrete
Surface Pad
Appears
Effective
Comments
MW-1 Yes Yes Yes Yes Yes Yes Background Well
MW-2 Yes Yes Yes Yes Yes Yes
MW-3R Yes Yes Yes Yes Yes ? Pad covered by soil
MW-4S Yes Yes Yes Yes Yes ?Pad covered by soil
MW-4D Yes Yes Yes Yes Yes ? Pad covered by soil
MW-5 Yes Yes Yes Yes Yes Yes Repaired by Co. in Sept. 2013 Datum may have changed
MW-6R Yes Yes Yes Yes Yes ? County improved surface seal in September 2013
MW-8 Yes Yes Yes Yes Yes Yes County improved vehicle access
MW-9S Yes Yes Yes Yes Yes Yes
MW-9D Yes Yes Yes Yes Yes Yes
MW-10 Yes Yes Yes Yes Yes Yes
MW-11S Yes Yes Yes Yes Yes Yes
MW-11D Yes Yes Yes Yes Yes Yes Very slow recharge
MW-12 Yes Yes Yes Yes Yes Yes Slow recharge
MW-13 Yes Yes Yes Yes Yes Yes
SW-1 Yes - - - - - High gage height & flow
SW-2 Yes - - - - - High gage height & flow
SW-3 Yes - - - - - High gage height & flow
SWN-1 Yes - - - - - High gage height & flow
SWN-2 Yes - - - - - High gage height & flow
SWN-3 No - - - - - Dry
SWN-4 No - - - - - Dry. Always has been
SW-A Yes - - - - - Supplemental sample per SWS verbal request
SW-B Yes - - - - - Supplemental sample per SWS verbal request
LAGOON Yes Yes Yes Yes Yes Yes Sample from invert which is typical
MLW-A Not Observed
P2-6S Not Observed
P2-6D Not Observed
P2-11S Not Observed
P2-11D Not Observed
P2-12 Not Observed
Any unusual field conditions, observations, or events:
Dual lined leachate lagoon leak detection manhole observed to be dry.
Phase 2 has an earthen berm built w/in liner limits which may reduce any potential for overland flow from Phase 2.
Paths leading to wells and around entire facility have been improved by County . All are 4X4 accessible.
Surry County Subtitle D Lined MSWLF Page 1 of 1
Table 3
Field Parameter Data Summary
May 31 - June 1, 2017
Parameter
Depth to
Water
Water
Elevation
TOC
Elevation Temp.ORP DO pH
Specific
Conductance TDS
Methane Gas
in Headspace
Turbidity of
Metals
Sample
Units ft (btoc)ft (amsl)ft (amsl) C mV mg/L SU umhos/cm mg/L (%/Vol)Visual
MW-1 64.12 1062.01 1127.02 15.9 NR NR 6.3 103 NR NR Clear
MW-2 13.19 923.26 936.68 14.1 NR NR 6.0 73 NR NR Slight
MW-3R 4.52 925.19 930.00 15.5 NR NR 5.9 321 NR NR Clear
MW-4S 10.01 934.00 943.23 14.9 NR NR 5.6 109 NR NR Slight
MW-4D 9.71 934.25 942.80 15.1 NR NR 5.9 138 NR NR Clear
MW-5 43.97 934.01 977.86 14.4 NR NR 5.3 121 NR 0 Clear
MW-6R 67.37 938.59 1004.75 15.2 NR NR 5.8 146 NR 0 Clear
MW-8 60.85 909.68 971.03 14.8 NR NR 6.3 161 NR NR Slight
MW-9S 30.40 917.89 952.83 15.0 NR NR 6.2 219 NR NR Clear
MW-9D 33.33 915.98 952.47 15.8 NR NR 6.7 101 NR NR Clear
MW-10 28.52 940.32 970.24 15.1 NR NR 6.0 128 NR NR Slight
MW-11S 30.45 938.31 969.09 14.5 NR NR 6.0 91 NR NR Slight
MW-11D 31.58 932.96 965.38 14.9 NR NR 6.9 121 NR NR Clear
MW-12 51.14 944.96 996.66 14.3 NR NR 6.8 193 NR NR Clear
MW-13 24.68 956.08 983.13 15.9 NR NR 6.0 123 NR NR Clear
MLW-A NR NR 1095.51 NR NR NR NR NR NR NR NR
P2-6S NR NR 1040.27 NR NR NR NR NR NR NR NR
P2-6D NR NR 1040.65 NR NR NR NR NR NR NR NR
P2-11S NR NR 1021.53 NR NR NR NR NR NR NR NR
P2-11D NR NR 1021.13 NR NR NR NR NR NR NR NR
P2-12 NR NR 986.61 NR NR NR NR NR NR NR NR
Minimum 4.52 909.68 930.00 14.10 NR NR 5.30 73.00 NR 0 Clear
Average 33.59 940.50 991.85 15.03 NR NR 6.11 143.20 NR 0 Slight
Maximum 67.37 1062.01 1127.02 15.90 NR NR 6.90 321.00 NR 0 Slight
SW-1 ---15.3 NR NR 7.9 74 NR -Clear
SW-2 ---16.9 NR NR 7.3 110 NR -Clear
SW-3 ---17.8 NR NR 7.1 281 NR -Clear
SW-4 ---17.3 NR NR 7.7 73 NR -Clear
SWN-1 ---17.0 NR NR 7.9 68 NR -Clear
SWN-2 ---16.9 NR NR 7.4 59 NR -Clear
SW-A ---16.9 NR NR 7.3 39 NR -Clear
SW-B ---16.8 NR NR 7.4 41 NR -Clear
Minimum ---15.3 NR NR 7.1 39.0 NR -Clear
Average ---16.9 NR NR 7.5 93.1 NR -Clear
Maximum ---17.8 NR NR 7.9 281.0 NR -Clear
NR = No reading attempted
btoc = Below top of casing
amsl = Above mean sea level
Surry County Subtitle D Lined MSWLF Page 1 of 1
Table 4
Sampling and Analysis Summary
May 30 - June 1, 2017
July 8, 2017 Verification Sample for SVOCs at MW-3R
VOCs Total Metals VOCs (App II)Total Metals (App II)Herbicides-Chlorinated App IISemivolatile Organics (SVOCs) App Pesticides App IITotal CyanideSulfideTemperatureConductivityTotal Dissolved Solids (TDS)pHTurbiditySulfatepHPhosphorusBOD, 5 dayCODNitrateLab EPA 8260B Lab EPA 6000/7000Lab EPA 8260B Lab EPA 6000/7000 Lab SW8151ALab EPA 8270D Lab EPA 8081BLab EPA 9014Lab SM18 4500-S DField MeterField MeterField MeterField MeterField VisualLab EPA 300.0Lab EPA9040Lab EPA365.1Lab SM 5210BLab SM 5220DLab EPA 353.2MW-1 x x x x x x x x x x x
MW-2 x x x x x x x x x x x
MW-3R x x x V x x x x x x x
MW-4S x x x x x x x x x x x
MW-4D x x x x x x x x x x x
MW-5 x x x x x x x x x x x
MW-6R x x x x x x x x x x x
MW-8 x x x x x x x x x x x
MW-9S x x x x x x x x x x x
MW-9D x x x x x x x x x x x
MW-10 x x x x x x x x x x x
MW-11S x x x x x x x x x x x
MW-11D x x x x x x x x x x x
MW-12 x x x x x x x x x x x
MW-13 x x x x x x x x x x x
SWN-1 x x x x x x
SWN-2 x x x x x x
SW-1 x x x x x x
SW-2 x x x x x x
SW-3 x x x x x x
SW-4 x x x x x x
SWN-3
SWN-4
SW-A x x x x x x
SW-B x x x x x x
LAGOON x x x x x x x x x
EB x x x
FB x x
TB x
Appendix I & II = Lists from current 40 CFR 258
App. I App. II Field Parameter Leachate
Not sampled since dry which is typical
Not sampled since dry which is typical
Surry County Subtitle D Lined MSWLF Page 1 of 1
Table 5
Groundwater, Leachate and QC Sample Detections
May 30-June 1, 2017
Verification of SVOCs at MW-3R on July 8, 2017
MW-1 MW-2 MW-4D MW-4S MW-5 MW-6R MW-8 MW-9D MW-9S MW-10 MW-11D MW-11S MW-12 MW-13 TB EB FB LAGOON
B S S S S S S S S S S S S S S S QC QC QC LEACHATE5/31/17 7/8/17
Barium, total 2.5 100 700 2000 78.4 J 36.5 J 50.6 J --46.9 J 69.9 J 69.6 J 58.9 J 71.6 J 40.4 J 104 42.6 J 3.2 J 15.5 J 16.2 J 16.2 J --1680
Beryllium, total 0.5 1 4 4 0.61 J ----Cadmium, total 0.5 1 2 5 0.64 J 0.97 J 1.2 --1.5 4.6 (N)0.69 J --
Chromium, total 2.5 10 10 100 15.8 (N)--3.1 J 5.5 J --54.3 J
Cobalt, total 2.5 10 1 NE 10.1 (N)--134 (N)--62.3 J
Copper, total 2.5 10 1000 1300 22.1 ----Lead, total 2.5 10 15 15 5.7 J ----49.3 J
Nickel, total 2.5 50 100 NE 13.9 J 3 J --2.5 J 10.1 J 2.8 J --41.6 J
Thallium, total 0.02 5.5 0.28 2 0.24 J 0.022 J --0.056 J 0.1 J 0.078 J 0.058 J 0.32 J (N)0.042 J 0.073 J --
Vanadium, total 2.5 25 0.3 NE 14.2 J (N)--5.3 J (N)4 J (N)10.2 J (N)--
Zinc, total 5 10 1000 NE 55.6 --13 11.6 6.2 J 8 J --
1,1-Dichloroethane 0.32 5 6 NE 2.6 J 2.5 J --1.7 J
1,2-Dichloroethane 0.24 1 0.4 5 --31,2-Dichloropropane 0.27 1 0.6 5 1.4
1,4-Dichlorobenzene 0.33 1 6 75 --5.2
Acetone 10 100 6000 NE 12.8 J 10.1 J --13.5 J 10.9 J 13.4 J 14.2 J 12.9 J 14.4 J 10.2 J
Benzene 0.25 1 1 5 --0.5 J 0.48 J 0.48 J 12.4Chlorobenzene0.23 3 50 100 --0.76 J
Chloromethane 0.11 1 3 NE --0.32 J 0.16 J 0.14 J
cis-1,2-Dichloroethene 0.19 5 70 70 1.7 J 3.1 J --0.51 J 4.2 J 0.84 J 4.1 J 0.83 J 1.5 J
Ethylbenzene 0.3 1 600 700 --2.1
Methylene Chloride 0.97 1 5 5 --1.5
Tetrachloroethene 0.46 1 0.7 5 0.68 J --0.57 J
Toluene 0.26 1 600 1000 --2
trans-1,2-Dichloroethene 0.49 5 100 100 --0.81 J 4.5 J
Vinyl chloride 0.62 1 0.03 2 --1.3 (L)0.67 J (L)10.5Xylene (total)0.66 5 500 10000 --11.4
1,2,4,5-Tetrachlorobenzene 1.3 10 2 NE 2 J <2.4 --------
4-Bromophenylphenyl ether 1.5 10 NE NE 1.5 J <1.3 --------4-Chlorophenylphenyl ether 1.6 10 NE NE 1.8 J <1.3 --------
Anthracene 1.7 10 2000 NE 1.8 J <1.4 --------
Benzo[a]anthracene;2.1 10 0.05 NE 2.2 J (A)<1.4 --------
Benzo[a]pyrene 2.2 10 0.005 NE 2.3 J (A)<1.4 --------
Benzo[b]fluoranthene 2.2 10 0.05 NE 2.6 J (A)<1.1 --------
Benzo[ghi]perylene 2.1 10 200 NE 2.5 J <1.4 --------
Benzo[k]fluoranthene 2 10 0.5 NE 2.5 J (A)<1.4 --------
Chrysene 2.1 10 5 NE 2.5 J <1.4 --------
Dibenz[a,h]anthracene 2 10 0.005 NE 2.3 J (A)<1.2 --------
Di-n-octyl phthalate 1.5 10 100 NE 1.5 J <1.3 --------
Hexachlorobenzene 1.7 10 0.02 NE 2.2 J (A)<1.3 --------
Hexachlorocyclopentadiene 1.3 10 50 NE 2.5 J <1.7 --------
Hexachloroethane 1.8 10 2.5 NE 2.3 J <1.7 --------
Hexachloropropene 1.2 10 NE NE 2.1 J <2 --------
Indeno(1,2,3-cd)pyrene 2 10 0.05 NE 2.4 J (A)<3.9 --------
Naphthalene 0.24 10 6 NE --3.5 J
Pentachlorobenzene 1.5 10 NE NE 2.1 J <2.6 --------
Phenanthrene 1.6 10 200 NE 1.8 J <1.5 --------
Cyanide 4 10 70 NE 5.5 J 4.4 J --4.6 J 5.9 J 4.8 J 4.7 J 5.6 J 5.2 J 15.1 4.8 J 4.7 J ----6.4 J
Phosphorus --NE NE NE --------------------------------------49.1 J
Sulfate --250000 250000 NE --------------------------------------18600 J
BOD --NE NE NE --------------------------------------14400
COD --NE NE NE --------------------------------------169000
Nitrate (as N)--10000 10000 NE --------------------------------------17200
pH --NE NE NE --------------------------------------7.4
Red Bold Above Established MCL/2L/GWP Std.
No regulatory compliance significance.
MDL = Method Detection Limit, SWSL = Solid Waste Section Limit, 2L/GWP Standard = NC 2L and IMAC Standards adopted by SWS, MCL = Maximum Contaminant Level for Drinking Water
J = "J-qualified". Concentration detected between MDL and SWSL. Considered estimated value
(N) Preliminary source is believed to be Natural originating from erosion of natural deposits. Source not anthropogenic.
(L) Prelilminary source is believed to be anthropogenic with leachate or landfill gas as transport mechanism
(A) Prelilminary source is lab/field induced artifact contamination. Likely false positive as evidenced by multitude of detections and all ND during verification event.
A definitive source of the detections was not determined as part of this report.
BG = Background Well Sample, QC = Quality Control Sample, S = Sentinal Well Sample
MCL MW-3R
Cyanide (Appendix II)
Yellow Highlighted Above Established Federal MCL Drinking Water Std.
Units ug/L, Blank cells means Not Detected, -- means not tested
Metals (Appendix I)
VOCs (Appendix I)
Pesticides (Appendix II)
Leachate Parameters
Parameter Name MDL SWSL 2L/GW
P Std
Surry County Subtitle D Lined MSWLF Page 1 of 1
Table 6
Surface Water Sample Detections
May 31-June 1, 2017
SW-1 SW-2 SW-3 SWN-1 SW-4 SW-A SW-B SWN-2
U U U U D D D D
Barium, total 2.5 100 200000 2000 26.8 J 17 J 21.8 J 21.3 J 22 J ----20.4 J
Cobalt, total 2.5 10 270 NE 16.8 8 J ----
Thallium, total 0.02 5.5 0.47 2 0.048 J 0.054 J ----
Vanadium, total 2.5 25 NE NE ----2.8 J
Zinc, total 5 10 50 NE 7.4 J 9.1 J 7 J ----5.4 J
Acetone 10 100 2000 NE 13.3 J 19.3 J 12.2 J 11.6 J
Chloromethane 0.11 1 550 NE 0.13 J 0.13 J
cis-1,2-Dichloroethene 0.19 5 4900 70 2.4 J
Red Bold Above Established 2B Std.Regulatory compliance Standard
Yellow Highlighted Above Established Federal MCL Drinking Water Std. No regulatory compliance significance.
MDL = Method Detection Limit, SWSL = Solid Waste Section Limit, 2B Standard = NC 2B Surface Water Standards adopted by SWS, MCL = Maximum Contaminant Level for Drinking Water
J = "J-qualified". Concentration detected between MDL and SWSL. Considered estimated value
U = Upstream of monitored unit, D= Downstream of monitored unit
Units ug/L, Blank cells means Not Detected, -- means not tested
Parameter Name MDL SWSL 2B Std MCL
VOCs (Appendix I)
Metals (Appendix I)
Surry County Subtitle D Lined MSWLF Page 1 of 1
Table 7
Hydrogeologic Prpoperties at Monitoring Locations
May 30 - 31, 2017
Hydraulic
Conductivity
(cm/sec)
Effective
Porosity
Hydraulic
Gradient Flow Rate Depth to
Groundwater
Groundwater
Potentiometric
Elevation
(cm/second)(%)(feet/feet)(feet/year)(feet btoc)(feet amsl)
MW-1 2.45E-04 3 0.257 2,177 N49E 64.12 1062.90 Rock
MW-2 3.20E-04 3 0.169 1,870 S18E 13.19 923.49 Rock
MW-3R 3.20E-04 3 0.118 1,302 S13E 4.52 925.48 Rock
MW-4S 1.50E-04 3 0.079 408 S11E 10.01 933.22 Sandy Silt & Fractured Rock
MW-4D 1.59E-04 3 --S20E 9.71 933.09 Rock
MW-5 3.20E-04 3 0.215 2,371 S60E 43.70 933.89 Rock
MW-6R 3.20E-04 3 0.089 980 S11E 67.37 937.38 Fractured Rock
MW-8 1.08E-03 3 0.005 200 S13E 60.85 910.18 Fractured Rock
MW-9S 7.45E-04 3 0.083 2,132 S31E 30.40 922.43 Fractured Rock
MW-9D 1.07E-05 3 --S31E 33.33 919.14 Competent Rock
MW-10 1.43E-04 3 0.560 2,761 S08E 28.52 941.72 Fractured Rock
MW-11S 6.19E-05 3 0.064 136 S19W 30.45 938.64 Competent Rock
MW-11D na 3 --S11W 37.35 933.80 Competent Rock
MW-12 1.91E-06 3 0.104 7 S22W 51.14 945.52 Competent Rock
MW-13 2.71E-03 3 0.046 4,338 S25W 24.68 958.45 Fractured Rock
P2-12 5.91E-07 3 0.000 0 NR NR Competent Rock
MLW-A na 3 0.000 -na NR NR Competent Rock
Minimum 5.91E-07 3 0.000 0 -4.52 910.18 -
Average 4.39E-04 3 0.128 1,195 -33.96 941.29 -
Maximum 2.71E-03 3 0.560 2,761 -67.37 1062.90 -
NOTE: Hydraulic conductivity and effective porosity values derived from slug tests performed by MESCO.
Hydrologic gradient from water levels recorded on May 30-31, 2017
Flow rate for MW-13 was considered an outlier; therefore not included in the average or maximum.
Flow rate (Q ) is defined by modified Darcy's equation:
where
K = hydraulic conductivity
ne = effective porosity
dh = head difference
dl = horizontal distance
Monitoring
Location
Flow
Direction
Screened Interval
Lithology
dl
dh
n
KQ
e

Surry County Subtitle D Lined MSWLF Page 1 of 1
Appendix A
Laboratory Analysis Reports
Chains of Custody
#=CL#
June 19, 2017
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92342337
92342337
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
SURRY CO. LINED MSWLF
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory between May 31, 2017
and June 01, 2017. The results relate only to the samples included in this report. Results reported
herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality
Assurance Manual, where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 241
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Certification: #346
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
Nevada Certification: FL NELAC Reciprocity
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
Wyoming Certification: FL NELAC Reciprocity
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 241
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Lab ID Sample ID Matrix Date Collected Date Received
92342337001 MW-8 Water 05/30/17 04:30 05/31/17 07:58
92342339001 LAGOON Water 05/30/17 05:15 05/31/17 10:40
92342479001 MW-1 Water 05/31/17 14:00 05/31/17 15:00
92342479002 MW-2 Water 05/31/17 13:15 05/31/17 15:00
92342479003 MW-3R Water 05/31/17 13:25 05/31/17 15:00
92342479004 MW-4S Water 05/31/17 13:00 05/31/17 15:00
92342479005 MW-4D Water 05/31/17 13:15 05/31/17 15:00
92342479006 MW-5 Water 05/31/17 11:00 05/31/17 15:00
92342479007 MW-6R Water 05/31/17 10:40 05/31/17 15:00
92342479009 MW-9S Water 05/31/17 13:50 05/31/17 15:00
92342479010 MW-9D Water 05/31/17 13:30 05/31/17 15:00
92342479011 MW-10 Water 05/31/17 13:05 05/31/17 15:00
92342479012 MW-11S Water 05/31/17 12:30 05/31/17 15:00
92342479013 MW-11D Water 05/31/17 12:10 05/31/17 15:00
92342529001 MW-12 Water 05/31/17 03:20 06/01/17 07:55
92342529002 MW-13 Water 05/31/17 03:30 06/01/17 07:55
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 241
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92342337001 MW-8 EPA 8081 21 PASI-CRES
EPA 8082 8 PASI-CHSK
EPA 8151 6 PASI-OLJM
EPA 6010 15 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8270 111 PASI-CRES
EPA 8260 67 PASI-CZDO
SM 4500-S2D 1 PASI-AMVC
SM 4500-CN-E 1 PASI-AAES2
92342339001 LAGOON EPA 6010 15 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8260 67 PASI-CZDO
SM 5210B 1 PASI-ABRJ
EPA 9040 1 PASI-AMJS1
EPA 300.0 1 PASI-ACDC
EPA 353.2 1 PASI-ABRJ
EPA 365.1 1 PASI-ABRJ
SM 4500-CN-E 1 PASI-AAES2
SM 5220D 1 PASI-AMDW
92342479001 MW-1 EPA 8081 21 PASI-CRES
EPA 8082 8 PASI-CHSK
EPA 8151 6 PASI-OLJM
EPA 6010 15 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CZDO
SM 4500-S2D 1 PASI-AMVC
SM 4500-CN-E 1 PASI-AAES2
92342479002 MW-2 EPA 8081 21 PASI-CRES
EPA 8082 8 PASI-CHSK
EPA 8151 6 PASI-OLJM
EPA 6010 15 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 241
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CZDO
SM 4500-S2D 1 PASI-AMVC
SM 4500-CN-E 1 PASI-AAES2
92342479003 MW-3R EPA 8081 21 PASI-CRES
EPA 8082 8 PASI-CHSK
EPA 8151 6 PASI-OLJM
EPA 6010 15 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CZDO
SM 4500-S2D 1 PASI-AMVC
SM 4500-CN-E 1 PASI-AAES2
92342479004 MW-4S EPA 8081 21 PASI-CRES
EPA 8082 8 PASI-CHSK
EPA 8151 6 PASI-OLJM
EPA 6010 15 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CZDO
SM 4500-S2D 1 PASI-AMVC
SM 4500-CN-E 1 PASI-AAES2
92342479005 MW-4D EPA 8081 21 PASI-CRES
EPA 8082 8 PASI-CHSK
EPA 8151 6 PASI-OLJM
EPA 6010 15 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CZDO
SM 4500-S2D 1 PASI-AMVC
SM 4500-CN-E 1 PASI-AAES2
92342479006 MW-5 EPA 8081 21 PASI-CRES
EPA 8082 8 PASI-CHSK
EPA 8151 6 PASI-OLJM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 241
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 6010 15 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CZDO
SM 4500-S2D 1 PASI-AMVC
SM 4500-CN-E 1 PASI-AAES2
92342479007 MW-6R EPA 8081 21 PASI-CRES
EPA 8082 8 PASI-CHSK
EPA 8151 6 PASI-OLJM
EPA 6010 15 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CZDO
SM 4500-S2D 1 PASI-AMVC
SM 4500-CN-E 1 PASI-AAES2
92342479009 MW-9S EPA 8081 21 PASI-CRES
EPA 8082 8 PASI-CHSK
EPA 8151 6 PASI-OLJM
EPA 6010 15 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8270 111 PASI-CRES
EPA 8260 67 PASI-CZDO
SM 4500-S2D 1 PASI-AMVC
SM 4500-CN-E 1 PASI-AAES2
92342479010 MW-9D EPA 8081 21 PASI-CRES
EPA 8082 8 PASI-CHSK
EPA 8151 6 PASI-OLJM
EPA 6010 15 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CZDO
SM 4500-S2D 1 PASI-AMVC
SM 4500-CN-E 1 PASI-AAES2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 241
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92342479011 MW-10 EPA 8081 21 PASI-CRES
EPA 8082 8 PASI-CHSK
EPA 8151 6 PASI-OLJM
EPA 6010 15 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CZDO
SM 4500-S2D 1 PASI-AMVC
SM 4500-CN-E 1 PASI-AAES2
92342479012 MW-11S EPA 8081 21 PASI-CRES
EPA 8082 8 PASI-CHSK
EPA 8151 6 PASI-OLJM
EPA 6010 15 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8270 111 PASI-CRES
EPA 8260 67 PASI-CZDO
SM 4500-S2D 1 PASI-AMVC
SM 4500-CN-E 1 PASI-AAES2
92342479013 MW-11D EPA 8081 21 PASI-CRES
EPA 8082 8 PASI-CHSK
EPA 8151 6 PASI-OLJM
EPA 6010 15 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CZDO
SM 4500-S2D 1 PASI-AMVC
SM 4500-CN-E 1 PASI-AAES2
92342529001 MW-12 EPA 8081 21 PASI-CRES
EPA 8151 6 PASI-OLJM
EPA 6010 15 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 241
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
SM 4500-S2D 1 PASI-AMVC
SM 4500-CN-E 1 PASI-AAES2
92342529002 MW-13 EPA 8081 21 PASI-CRES
EPA 8151 6 PASI-OLJM
EPA 6010 15 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AKAL
EPA 8270 111 PASI-CBPJ
EPA 8260 67 PASI-CGAW
SM 4500-S2D 1 PASI-AMVC
SM 4500-CN-E 1 PASI-AAES2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-8 Lab ID:92342337001 Collected:05/30/17 04:30 Received:05/31/17 07:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/07/17 23:46 309-00-206/02/17 13:290.050 0.050 1
alpha-BHC ND ug/L 06/07/17 23:46 319-84-606/02/17 13:290.050 0.050 1
beta-BHC ND ug/L 06/07/17 23:46 319-85-706/02/17 13:290.050 0.050 1
delta-BHC ND ug/L 06/07/17 23:46 319-86-806/02/17 13:290.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/07/17 23:46 58-89-906/02/17 13:290.050 0.050 1
Chlordane (Technical)ND ug/L 06/07/17 23:46 57-74-906/02/17 13:290.50 0.20 1
4,4'-DDD ND ug/L 06/07/17 23:46 72-54-806/02/17 13:290.10 0.050 1
4,4'-DDE ND ug/L 06/07/17 23:46 72-55-906/02/17 13:290.10 0.050 1
4,4'-DDT ND ug/L 06/07/17 23:46 50-29-306/02/17 13:290.10 0.050 1
Dieldrin ND ug/L 06/07/17 23:46 60-57-106/02/17 13:290.075 0.050 1
Endosulfan I ND ug/L 06/07/17 23:46 959-98-806/02/17 13:290.10 0.050 1
Endosulfan II ND ug/L 06/07/17 23:46 33213-65-906/02/17 13:290.10 0.050 1
Endosulfan sulfate ND ug/L 06/07/17 23:46 1031-07-806/02/17 13:290.10 0.050 1
Endrin ND ug/L 06/07/17 23:46 72-20-806/02/17 13:290.10 0.050 1
Endrin aldehyde ND ug/L 06/07/17 23:46 7421-93-406/02/17 13:290.10 0.050 1
Heptachlor ND ug/L 06/07/17 23:46 76-44-806/02/17 13:290.050 0.050 1
Heptachlor epoxide ND ug/L 06/07/17 23:46 1024-57-306/02/17 13:290.075 0.050 1
Methoxychlor ND ug/L 06/07/17 23:46 72-43-506/02/17 13:291.0 0.15 1
Toxaphene ND ug/L 06/07/17 23:46 8001-35-206/02/17 13:291.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)97 %06/07/17 23:46 877-09-806/02/17 13:2920-130 1
Decachlorobiphenyl (S)59 %06/07/17 23:46 2051-24-306/02/17 13:2920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/01/17 21:36 12674-11-205/31/17 16:500.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/01/17 21:36 11104-28-205/31/17 16:500.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/01/17 21:36 11141-16-505/31/17 16:500.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/01/17 21:36 53469-21-905/31/17 16:500.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/01/17 21:36 12672-29-605/31/17 16:500.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/01/17 21:36 11097-69-105/31/17 16:500.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/01/17 21:36 11096-82-505/31/17 16:500.50 0.50 1
Surrogates
Decachlorobiphenyl (S)72 %06/01/17 21:36 2051-24-305/31/17 16:5010-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/06/17 07:45 94-75-706/02/17 16:300.94 0.22 1
Dinoseb ND ug/L 06/06/17 07:45 88-85-706/02/17 16:300.19 0.057 1
Pentachlorophenol ND ug/L 06/06/17 07:45 87-86-506/02/17 16:300.028 0.017 1
2,4,5-T ND ug/L 06/06/17 07:45 93-76-506/02/17 16:300.19 0.042 1
2,4,5-TP (Silvex)ND ug/L 06/06/17 07:45 93-72-106/02/17 16:300.19 0.049 1
Surrogates
2,4-DCAA (S)75 %06/06/17 07:45 19719-28-906/02/17 16:3039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/10/17 08:03 7440-36-006/02/17 15:206.0 3.9 1
Arsenic ND ug/L 06/10/17 08:03 7440-38-206/02/17 15:2010.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-8 Lab ID:92342337001 Collected:05/30/17 04:30 Received:05/31/17 07:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Barium 71.6J ug/L 06/10/17 08:03 7440-39-306/02/17 15:201002.5 1
Beryllium ND ug/L 06/10/17 08:03 7440-41-706/02/17 15:201.0 0.50 1
Cadmium ND ug/L 06/10/17 08:03 7440-43-906/02/17 15:201.0 0.50 1
Chromium ND ug/L 06/10/17 08:03 7440-47-306/02/17 15:2010.0 2.5 1
Cobalt ND ug/L 06/10/17 08:03 7440-48-406/02/17 15:2010.0 2.5 1
Copper ND ug/L 06/10/17 08:03 7440-50-806/02/17 15:2010.0 2.5 1
Lead ND ug/L 06/10/17 08:03 7439-92-106/02/17 15:2010.0 2.5 1
Nickel ND ug/L 06/10/17 08:03 7440-02-006/02/17 15:2050.0 2.5 1
Selenium ND ug/L 06/10/17 08:03 7782-49-206/02/17 15:2010.0 5.0 1
Silver ND ug/L 06/10/17 08:03 7440-22-406/02/17 15:2010.0 2.5 1
Tin ND ug/L 06/10/17 08:03 7440-31-506/02/17 15:201002.5 1
Vanadium ND ug/L 06/10/17 08:03 7440-62-206/02/17 15:2025.0 2.5 1
Zinc ND ug/L 06/10/17 08:03 7440-66-606/02/17 15:2010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.058J ug/L 06/06/17 18:55 7440-28-006/03/17 02:255.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 03:31 7439-97-606/06/17 14:590.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/07/17 16:24 83-32-906/06/17 15:0010.0 1.6 1
Acenaphthylene ND ug/L 06/07/17 16:24 208-96-806/06/17 15:0010.0 1.5 1
Acetophenone ND ug/L 06/07/17 16:24 98-86-206/06/17 15:0010.0 1.9 1
2-Acetylaminofluorene ND ug/L 06/07/17 16:24 53-96-306/06/17 15:0020.0 1.6 1
4-Aminobiphenyl ND ug/L 06/07/17 16:24 92-67-106/06/17 15:0020.0 1.7 1
Anthracene ND ug/L 06/07/17 16:24 120-12-706/06/17 15:0010.0 1.7 1
Benzo(a)anthracene ND ug/L 06/07/17 16:24 56-55-306/06/17 15:0010.0 2.1 1
Benzo(a)pyrene ND ug/L 06/07/17 16:24 50-32-806/06/17 15:0010.0 2.2 1
Benzo(b)fluoranthene ND ug/L 06/07/17 16:24 205-99-206/06/17 15:0010.0 2.2 1
Benzo(g,h,i)perylene ND ug/L 06/07/17 16:24 191-24-206/06/17 15:0010.0 2.1 1
Benzo(k)fluoranthene ND ug/L 06/07/17 16:24 207-08-906/06/17 15:0010.0 2.0 1
Benzyl alcohol ND ug/L 06/07/17 16:24 100-51-606/06/17 15:0020.0 3.1 1
4-Bromophenylphenyl ether ND ug/L 06/07/17 16:24 101-55-306/06/17 15:0010.0 1.5 1
Butylbenzylphthalate ND ug/L 06/07/17 16:24 85-68-706/06/17 15:0010.0 2.5 1
4-Chloro-3-methylphenol ND ug/L 06/07/17 16:24 59-50-706/06/17 15:0020.0 2.8 1
4-Chloroaniline ND ug/L 06/07/17 16:24 106-47-806/06/17 15:0020.0 2.8 1
Chlorobenzilate ND ug/L 06/07/17 16:24 510-15-606/06/17 15:0010.0 2.2 1
bis(2-Chloroethoxy)methane ND ug/L 06/07/17 16:24 111-91-106/06/17 15:0010.0 1.6 1
bis(2-Chloroethyl) ether ND ug/L 06/07/17 16:24 111-44-406/06/17 15:0010.0 1.7 1
2-Chloronaphthalene ND ug/L 06/07/17 16:24 91-58-706/06/17 15:0010.0 1.6 1
2-Chlorophenol ND ug/L 06/07/17 16:24 95-57-806/06/17 15:0010.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/07/17 16:24 7005-72-306/06/17 15:0010.0 1.6 1
Chrysene ND ug/L 06/07/17 16:24 218-01-906/06/17 15:0010.0 2.1 1
Diallate ND ug/L 06/07/17 16:24 2303-16-406/06/17 15:0010.0 1.6 1
Dibenz(a,h)anthracene ND ug/L 06/07/17 16:24 53-70-306/06/17 15:0010.0 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-8 Lab ID:92342337001 Collected:05/30/17 04:30 Received:05/31/17 07:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Dibenzofuran ND ug/L 06/07/17 16:24 132-64-906/06/17 15:0010.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 06/07/17 16:24 91-94-106/06/17 15:0020.0 3.9 1
2,4-Dichlorophenol ND ug/L 06/07/17 16:24 120-83-206/06/17 15:0010.0 1.6 1
2,6-Dichlorophenol ND ug/L 06/07/17 16:24 87-65-006/06/17 15:0010.0 1.5 1
Diethylphthalate ND ug/L 06/07/17 16:24 84-66-206/06/17 15:0060001.6 1
Dimethoate ND ug/L 06/07/17 16:24 60-51-506/06/17 15:0020.0 1.8 1
P-Dimethylaminoazobenzene ND ug/L 06/07/17 16:24 60-11-706/06/17 15:0010.0 1.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/07/17 16:24 57-97-606/06/17 15:0010.0 2.4 1
3,3'-Dimethylbenzidine ND ug/L 06/07/17 16:24 119-93-706/06/17 15:0010.0 3.9 1
2,4-Dimethylphenol ND ug/L 06/07/17 16:24 105-67-906/06/17 15:0010.0 1.6 1
Dimethylphthalate ND ug/L 06/07/17 16:24 131-11-306/06/17 15:0010.0 1.4 1
Di-n-butylphthalate ND ug/L 06/07/17 16:24 84-74-206/06/17 15:0010.0 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/07/17 16:24 534-52-106/06/17 15:0050.0 2.2 1
1,3-Dinitrobenzene ND ug/L 06/07/17 16:24 99-65-006/06/17 15:0020.0 1.3 1
2,4-Dinitrophenol ND ug/L 06/07/17 16:24 51-28-506/06/17 15:0050.0 5.1 1
2,4-Dinitrotoluene ND ug/L 06/07/17 16:24 121-14-206/06/17 15:0010.0 1.5 1
2,6-Dinitrotoluene ND ug/L 06/07/17 16:24 606-20-206/06/17 15:0010.0 1.4 1
Di-n-octylphthalate ND ug/L 06/07/17 16:24 117-84-006/06/17 15:0010.0 1.5 1
Diphenylamine ND ug/L 06/07/17 16:24 122-39-406/06/17 15:0010.0 1.4 1
Disulfoton ND ug/L 06/07/17 16:24 298-04-406/06/17 15:0010.0 1.5 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/07/17 16:24 117-81-706/06/17 15:0015.0 2.3 1
Ethyl methanesulfonate ND ug/L 06/07/17 16:24 62-50-006/06/17 15:0020.0 1.6 1
Famphur ND ug/L 06/07/17 16:24 52-85-706/06/17 15:0020.0 5.7 1
Fluoranthene ND ug/L 06/07/17 16:24 206-44-006/06/17 15:0010.0 2.2 1
Fluorene ND ug/L 06/07/17 16:24 86-73-706/06/17 15:0010.0 1.6 1
Hexachlorobenzene ND ug/L 06/07/17 16:24 118-74-106/06/17 15:0010.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 06/07/17 16:24 77-47-406/06/17 15:0010.0 1.3 1
Hexachloroethane ND ug/L 06/07/17 16:24 67-72-106/06/17 15:0010.0 1.8 1
Hexachloropropene ND ug/L 06/07/17 16:24 1888-71-706/06/17 15:0010.0 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/07/17 16:24 193-39-506/06/17 15:0010.0 2.0 1
Isodrin ND ug/L 06/07/17 16:24 465-73-606/06/17 15:0020.0 2.5 1
Isophorone ND ug/L 06/07/17 16:24 78-59-106/06/17 15:0010.0 1.5 1
Isosafrole ND ug/L 06/07/17 16:24 120-58-106/06/17 15:0010.0 1.5 1
Kepone ND ug/L 06/07/17 16:24 143-50-006/06/17 15:0020.0 4.5 1
Methapyrilene ND ug/L 06/07/17 16:24 91-80-5 L206/06/17 15:001003.0 1
3-Methylcholanthrene ND ug/L 06/07/17 16:24 56-49-506/06/17 15:0010.0 2.7 1
Methyl methanesulfonate ND ug/L 06/07/17 16:24 66-27-3 L106/06/17 15:0010.0 1.1 1
2-Methylnaphthalene ND ug/L 06/07/17 16:24 91-57-606/06/17 15:0010.0 1.4 1
Methyl parathion ND ug/L 06/07/17 16:24 298-00-006/06/17 15:0010.0 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 06/07/17 16:24 95-48-706/06/17 15:0010.0 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/07/17 16:24 15831-10-406/06/17 15:0010.0 1.4 1
1-Naphthalenamine ND ug/L 06/07/17 16:24 134-32-706/06/17 15:0010.0 1.3 1
2-Naphthalenamine ND ug/L 06/07/17 16:24 91-59-806/06/17 15:0010.0 2.2 1
1,4-Naphthoquinone ND ug/L 06/07/17 16:24 130-15-406/06/17 15:0010.0 0.99 1
2-Nitroaniline ND ug/L 06/07/17 16:24 88-74-406/06/17 15:0050.0 2.3 1
3-Nitroaniline ND ug/L 06/07/17 16:24 99-09-206/06/17 15:0050.0 2.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-8 Lab ID:92342337001 Collected:05/30/17 04:30 Received:05/31/17 07:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Nitroaniline ND ug/L 06/07/17 16:24 100-01-606/06/17 15:0020.0 3.4 1
Nitrobenzene ND ug/L 06/07/17 16:24 98-95-306/06/17 15:0010.0 1.6 1
2-Nitrophenol ND ug/L 06/07/17 16:24 88-75-506/06/17 15:0010.0 1.6 1
4-Nitrophenol ND ug/L 06/07/17 16:24 100-02-706/06/17 15:0050.0 4.3 1
5-Nitro-o-toluidine ND ug/L 06/07/17 16:24 99-55-806/06/17 15:0010.0 1.9 1
N-Nitrosodiethylamine ND ug/L 06/07/17 16:24 55-18-506/06/17 15:0020.0 1.4 1
N-Nitrosodimethylamine ND ug/L 06/07/17 16:24 62-75-906/06/17 15:0010.0 1.6 1
N-Nitroso-di-n-butylamine ND ug/L 06/07/17 16:24 924-16-306/06/17 15:0010.0 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 06/07/17 16:24 621-64-706/06/17 15:0010.0 1.7 1
N-Nitrosodiphenylamine ND ug/L 06/07/17 16:24 86-30-606/06/17 15:0010.0 1.4 1
N-Nitrosomethylethylamine ND ug/L 06/07/17 16:24 10595-95-606/06/17 15:0010.0 1.4 1
N-Nitrosopiperidine ND ug/L 06/07/17 16:24 100-75-406/06/17 15:0020.0 1.7 1
N-Nitrosopyrrolidine ND ug/L 06/07/17 16:24 930-55-206/06/17 15:0010.0 1.7 1
O,O,O-Triethylphosphorothioate ND ug/L 06/07/17 16:24 126-68-106/06/17 15:0010.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/07/17 16:24 108-60-106/06/17 15:0010.0 1.8 1
Parathion (Ethyl parathion)ND ug/L 06/07/17 16:24 56-38-206/06/17 15:0010.0 1.5 1
Pentachlorobenzene ND ug/L 06/07/17 16:24 608-93-506/06/17 15:0010.0 1.5 1
Pentachloronitrobenzene ND ug/L 06/07/17 16:24 82-68-806/06/17 15:0020.0 1.7 1
Pentachlorophenol ND ug/L 06/07/17 16:24 87-86-506/06/17 15:0025.0 3.5 1
Phenacetin ND ug/L 06/07/17 16:24 62-44-206/06/17 15:0020.0 1.9 1
Phenanthrene ND ug/L 06/07/17 16:24 85-01-806/06/17 15:0010.0 1.6 1
Phenol ND ug/L 06/07/17 16:24 108-95-206/06/17 15:0010.0 1.3 1
p-Phenylenediamine ND ug/L 06/07/17 16:24 106-50-306/06/17 15:0010.0 2.2 1
Phorate ND ug/L 06/07/17 16:24 298-02-206/06/17 15:0010.0 1.7 1
Pronamide ND ug/L 06/07/17 16:24 23950-58-506/06/17 15:0010.0 2.0 1
Pyrene ND ug/L 06/07/17 16:24 129-00-006/06/17 15:0010.0 2.2 1
Safrole ND ug/L 06/07/17 16:24 94-59-706/06/17 15:0010.0 1.3 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/07/17 16:24 95-94-306/06/17 15:0010.0 1.3 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/07/17 16:24 58-90-206/06/17 15:0010.0 2.9 1
Thionazin ND ug/L 06/07/17 16:24 297-97-206/06/17 15:0020.0 1.7 1
O-Toluidine ND ug/L 06/07/17 16:24 95-53-406/06/17 15:0010.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 06/07/17 16:24 95-95-406/06/17 15:0010.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/07/17 16:24 88-06-206/06/17 15:0010.0 1.4 1
1,3,5-Trinitrobenzene ND ug/L 06/07/17 16:24 99-35-406/06/17 15:0010.0 1.2 1
Surrogates
Nitrobenzene-d5 (S)87 %06/07/17 16:24 4165-60-006/06/17 15:0021-110 1
2-Fluorobiphenyl (S)90 %06/07/17 16:24 321-60-806/06/17 15:0027-110 1
Terphenyl-d14 (S)105 %06/07/17 16:24 1718-51-006/06/17 15:0031-107 1
Phenol-d6 (S)28 %06/07/17 16:24 13127-88-306/06/17 15:0010-110 1
2-Fluorophenol (S)46 %06/07/17 16:24 367-12-406/06/17 15:0012-110 1
2,4,6-Tribromophenol (S)89 %06/07/17 16:24 118-79-606/06/17 15:0027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/31/17 17:54 67-64-110010.0 1
Acetonitrile ND ug/L 05/31/17 17:54 75-05-855.0 2.2 1
Acrolein ND ug/L 05/31/17 17:54 107-02-8 L153.0 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-8 Lab ID:92342337001 Collected:05/30/17 04:30 Received:05/31/17 07:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acrylonitrile ND ug/L 05/31/17 17:54 107-13-12001.9 1
Allyl chloride ND ug/L 05/31/17 17:54 107-05-110.0 1.5 1
Benzene ND ug/L 05/31/17 17:54 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/31/17 17:54 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/31/17 17:54 75-27-41.0 0.18 1
Bromoform ND ug/L 05/31/17 17:54 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/31/17 17:54 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/31/17 17:54 78-93-31000.96 1
Carbon disulfide ND ug/L 05/31/17 17:54 75-15-01001.2 1
Carbon tetrachloride ND ug/L 05/31/17 17:54 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 05/31/17 17:54 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/31/17 17:54 75-00-310.0 0.54 1
Chloroform ND ug/L 05/31/17 17:54 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/31/17 17:54 74-87-31.0 0.11 1
Chloroprene ND ug/L 05/31/17 17:54 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 05/31/17 17:54 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 05/31/17 17:54 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/31/17 17:54 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/31/17 17:54 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/31/17 17:54 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 05/31/17 17:54 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 05/31/17 17:54 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/31/17 17:54 110-57-6 L11001.0 1
Dichlorodifluoromethane ND ug/L 05/31/17 17:54 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 05/31/17 17:54 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 05/31/17 17:54 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 05/31/17 17:54 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 05/31/17 17:54 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/31/17 17:54 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 05/31/17 17:54 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 05/31/17 17:54 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 05/31/17 17:54 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 05/31/17 17:54 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 05/31/17 17:54 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/31/17 17:54 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 05/31/17 17:54 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 05/31/17 17:54 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 05/31/17 17:54 87-68-310.0 0.71 1
2-Hexanone ND ug/L 05/31/17 17:54 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/31/17 17:54 74-88-410.0 0.32 1
Isobutanol ND ug/L 05/31/17 17:54 78-83-110035.0 1
Methacrylonitrile ND ug/L 05/31/17 17:54 126-98-71000.93 1
Methylene Chloride ND ug/L 05/31/17 17:54 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 05/31/17 17:54 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/31/17 17:54 108-10-11000.33 1
Naphthalene ND ug/L 05/31/17 17:54 91-20-310.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
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Page 13 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-8 Lab ID:92342337001 Collected:05/30/17 04:30 Received:05/31/17 07:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Propionitrile ND ug/L 05/31/17 17:54 107-12-01503.6 1
Styrene ND ug/L 05/31/17 17:54 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/31/17 17:54 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/31/17 17:54 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/31/17 17:54 127-18-41.0 0.46 1
Toluene ND ug/L 05/31/17 17:54 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 05/31/17 17:54 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 05/31/17 17:54 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/31/17 17:54 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/31/17 17:54 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/31/17 17:54 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/31/17 17:54 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/31/17 17:54 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 05/31/17 17:54 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/31/17 17:54 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %05/31/17 17:54 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %05/31/17 17:54 17060-07-070-130 1
Toluene-d8 (S)109 %05/31/17 17:54 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/01/17 21:00 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 5.6J ug/L 06/01/17 17:23 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:LAGOON Lab ID:92342339001 Collected:05/30/17 05:15 Received:05/31/17 10:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/10/17 08:06 7440-36-0 D306/02/17 15:2060.0 38.7 10
Arsenic ND ug/L 06/10/17 08:06 7440-38-2 D306/02/17 15:2010050.0 10
Barium 1680 ug/L 06/10/17 08:06 7440-39-306/02/17 15:20100025.0 10
Beryllium ND ug/L 06/10/17 08:06 7440-41-7 D306/02/17 15:2010.0 5.0 10
Cadmium ND ug/L 06/10/17 08:06 7440-43-9 D306/02/17 15:2010.0 5.0 10
Chromium 54.3J ug/L 06/10/17 08:06 7440-47-306/02/17 15:2010025.0 10
Cobalt 62.3J ug/L 06/10/17 08:06 7440-48-406/02/17 15:2010025.0 10
Copper ND ug/L 06/10/17 08:06 7440-50-8 D306/02/17 15:2010025.0 10
Lead 49.3J ug/L 06/10/17 08:06 7439-92-1 D306/02/17 15:2010025.0 10
Nickel 41.6J ug/L 06/10/17 08:06 7440-02-0 D306/02/17 15:2050025.0 10
Selenium ND ug/L 06/10/17 08:06 7782-49-2 D306/02/17 15:2010050.0 10
Silver ND ug/L 06/10/17 08:06 7440-22-4 D306/02/17 15:2010025.0 10
Tin ND ug/L 06/10/17 08:06 7440-31-5 D306/02/17 15:20100025.0 10
Vanadium ND ug/L 06/10/17 08:06 7440-62-2 D306/02/17 15:2025025.0 10
Zinc ND ug/L 06/10/17 08:06 7440-66-6 D306/02/17 15:2010050.0 10
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/06/17 15:49 7440-28-006/02/17 03:455.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 03:33 7439-97-606/06/17 14:590.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 05/31/17 18:11 67-64-110010.0 1
Acetonitrile ND ug/L 05/31/17 18:11 75-05-855.0 2.2 1
Acrolein ND ug/L 05/31/17 18:11 107-02-8 L153.0 1.6 1
Acrylonitrile ND ug/L 05/31/17 18:11 107-13-12001.9 1
Allyl chloride ND ug/L 05/31/17 18:11 107-05-110.0 1.5 1
Benzene 12.4 ug/L 05/31/17 18:11 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 05/31/17 18:11 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 05/31/17 18:11 75-27-41.0 0.18 1
Bromoform ND ug/L 05/31/17 18:11 75-25-23.0 0.26 1
Bromomethane ND ug/L 05/31/17 18:11 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 05/31/17 18:11 78-93-31000.96 1
Carbon disulfide ND ug/L 05/31/17 18:11 75-15-01001.2 1
Carbon tetrachloride ND ug/L 05/31/17 18:11 56-23-51.0 0.25 1
Chlorobenzene 0.76J ug/L 05/31/17 18:11 108-90-73.0 0.23 1
Chloroethane ND ug/L 05/31/17 18:11 75-00-310.0 0.54 1
Chloroform ND ug/L 05/31/17 18:11 67-66-35.0 0.14 1
Chloromethane ND ug/L 05/31/17 18:11 74-87-31.0 0.11 1
Chloroprene ND ug/L 05/31/17 18:11 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 05/31/17 18:11 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 05/31/17 18:11 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/31/17 18:11 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/31/17 18:11 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/31/17 18:11 95-50-15.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:LAGOON Lab ID:92342339001 Collected:05/30/17 05:15 Received:05/31/17 10:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,3-Dichlorobenzene ND ug/L 05/31/17 18:11 541-73-15.0 0.24 1
1,4-Dichlorobenzene 5.2 ug/L 05/31/17 18:11 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 05/31/17 18:11 110-57-6 L11001.0 1
Dichlorodifluoromethane ND ug/L 05/31/17 18:11 75-71-85.0 0.21 1
1,1-Dichloroethane 1.7J ug/L 05/31/17 18:11 75-34-35.0 0.32 1
1,2-Dichloroethane 3.0 ug/L 05/31/17 18:11 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 05/31/17 18:11 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 1.5J ug/L 05/31/17 18:11 156-59-25.0 0.19 1
trans-1,2-Dichloroethene 4.5J ug/L 05/31/17 18:11 156-60-55.0 0.49 1
1,2-Dichloropropane 1.4 ug/L 05/31/17 18:11 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 05/31/17 18:11 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 05/31/17 18:11 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 05/31/17 18:11 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 05/31/17 18:11 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/31/17 18:11 10061-02-61.0 0.26 1
Ethylbenzene 2.1 ug/L 05/31/17 18:11 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 05/31/17 18:11 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 05/31/17 18:11 87-68-310.0 0.71 1
2-Hexanone ND ug/L 05/31/17 18:11 591-78-650.0 0.46 1
Iodomethane ND ug/L 05/31/17 18:11 74-88-410.0 0.32 1
Isobutanol ND ug/L 05/31/17 18:11 78-83-110035.0 1
Methacrylonitrile ND ug/L 05/31/17 18:11 126-98-71000.93 1
Methylene Chloride 1.5 ug/L 05/31/17 18:11 75-09-2 C91.0 0.97 1
Methyl methacrylate ND ug/L 05/31/17 18:11 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/31/17 18:11 108-10-11000.33 1
Naphthalene 3.5J ug/L 05/31/17 18:11 91-20-310.0 0.24 1
Propionitrile ND ug/L 05/31/17 18:11 107-12-01503.6 1
Styrene ND ug/L 05/31/17 18:11 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/31/17 18:11 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/31/17 18:11 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 05/31/17 18:11 127-18-41.0 0.46 1
Toluene 2.0 ug/L 05/31/17 18:11 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 05/31/17 18:11 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 05/31/17 18:11 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/31/17 18:11 79-00-51.0 0.29 1
Trichloroethene ND ug/L 05/31/17 18:11 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/31/17 18:11 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/31/17 18:11 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/31/17 18:11 108-05-450.0 0.35 1
Vinyl chloride 10.5 ug/L 05/31/17 18:11 75-01-41.0 0.62 1
Xylene (Total)11.4 ug/L 05/31/17 18:11 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %05/31/17 18:11 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %05/31/17 18:11 17060-07-070-130 1
Toluene-d8 (S)108 %05/31/17 18:11 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:LAGOON Lab ID:92342339001 Collected:05/30/17 05:15 Received:05/31/17 10:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 5210B5210B BOD, 5 day
BOD, 5 day 14400 ug/L 06/06/17 01:13 B2,D606/01/17 04:00200020001
Analytical Method: EPA 90409040 pH
pH 7.4 Std. Units 06/02/17 19:30 H60.10 0.10 1
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 18600J ug/L 06/03/17 14:18 14808-79-8 M12500005001
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate 17200 ug/L 06/01/17 03:32 M11000010.0 1
Analytical Method: EPA 365.1365.1 Phosphorus, Total
Phosphorus 49.1J ug/L 06/02/17 05:50 7723-14-050.0 25.0 1
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 6.4J ug/L 06/01/17 17:24 57-12-510.0 4.0 1
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 169000 ug/L 06/01/17 23:5525000125001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-1 Lab ID:92342479001 Collected:05/31/17 14:00 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/06/17 15:34 309-00-206/02/17 10:090.050 0.050 1
alpha-BHC ND ug/L 06/06/17 15:34 319-84-606/02/17 10:090.050 0.050 1
beta-BHC ND ug/L 06/06/17 15:34 319-85-706/02/17 10:090.050 0.050 1
delta-BHC ND ug/L 06/06/17 15:34 319-86-806/02/17 10:090.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/06/17 15:34 58-89-906/02/17 10:090.050 0.050 1
Chlordane (Technical)ND ug/L 06/06/17 15:34 57-74-906/02/17 10:090.50 0.20 1
4,4'-DDD ND ug/L 06/06/17 15:34 72-54-806/02/17 10:090.10 0.050 1
4,4'-DDE ND ug/L 06/06/17 15:34 72-55-906/02/17 10:090.10 0.050 1
4,4'-DDT ND ug/L 06/06/17 15:34 50-29-306/02/17 10:090.10 0.050 1
Dieldrin ND ug/L 06/06/17 15:34 60-57-106/02/17 10:090.075 0.050 1
Endosulfan I ND ug/L 06/06/17 15:34 959-98-806/02/17 10:090.10 0.050 1
Endosulfan II ND ug/L 06/06/17 15:34 33213-65-906/02/17 10:090.10 0.050 1
Endosulfan sulfate ND ug/L 06/06/17 15:34 1031-07-806/02/17 10:090.10 0.050 1
Endrin ND ug/L 06/06/17 15:34 72-20-806/02/17 10:090.10 0.050 1
Endrin aldehyde ND ug/L 06/06/17 15:34 7421-93-406/02/17 10:090.10 0.050 1
Heptachlor ND ug/L 06/06/17 15:34 76-44-806/02/17 10:090.050 0.050 1
Heptachlor epoxide ND ug/L 06/06/17 15:34 1024-57-306/02/17 10:090.075 0.050 1
Methoxychlor ND ug/L 06/06/17 15:34 72-43-506/02/17 10:091.0 0.15 1
Toxaphene ND ug/L 06/06/17 15:34 8001-35-206/02/17 10:091.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)86 %06/06/17 15:34 877-09-806/02/17 10:0920-130 1
Decachlorobiphenyl (S)71 %06/06/17 15:34 2051-24-306/02/17 10:0920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/02/17 16:24 12674-11-206/02/17 10:090.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/02/17 16:24 11104-28-206/02/17 10:090.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/02/17 16:24 11141-16-506/02/17 10:090.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/02/17 16:24 53469-21-906/02/17 10:090.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/02/17 16:24 12672-29-606/02/17 10:090.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/02/17 16:24 11097-69-106/02/17 10:090.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/02/17 16:24 11096-82-506/02/17 10:090.50 0.50 1
Surrogates
Decachlorobiphenyl (S)66 %06/02/17 16:24 2051-24-306/02/17 10:0910-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/07/17 02:33 94-75-7 L106/05/17 16:501.0 0.25 1
Dinoseb ND ug/L 06/07/17 02:33 88-85-7 L106/05/17 16:500.21 0.063 1
Pentachlorophenol ND ug/L 06/07/17 02:33 87-86-506/05/17 16:500.031 0.019 1
2,4,5-T ND ug/L 06/07/17 02:33 93-76-506/05/17 16:500.21 0.046 1
2,4,5-TP (Silvex)ND ug/L 06/07/17 02:33 93-72-106/05/17 16:500.21 0.054 1
Surrogates
2,4-DCAA (S)113 %06/07/17 02:33 19719-28-906/05/17 16:5039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/09/17 18:31 7440-36-006/02/17 15:206.0 3.9 1
Arsenic ND ug/L 06/09/17 18:31 7440-38-206/02/17 15:2010.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-1 Lab ID:92342479001 Collected:05/31/17 14:00 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Barium 78.4J ug/L 06/09/17 18:31 7440-39-306/02/17 15:201002.5 1
Beryllium 0.61J ug/L 06/09/17 18:31 7440-41-706/02/17 15:201.0 0.50 1
Cadmium 0.64J ug/L 06/09/17 18:31 7440-43-906/02/17 15:201.0 0.50 1
Chromium 15.8 ug/L 06/09/17 18:31 7440-47-306/02/17 15:2010.0 2.5 1
Cobalt 10.1 ug/L 06/09/17 18:31 7440-48-406/02/17 15:2010.0 2.5 1
Copper 22.1 ug/L 06/09/17 18:31 7440-50-806/02/17 15:2010.0 2.5 1
Lead 5.7J ug/L 06/09/17 18:31 7439-92-106/02/17 15:2010.0 2.5 1
Nickel 13.9J ug/L 06/09/17 18:31 7440-02-006/02/17 15:2050.0 2.5 1
Selenium ND ug/L 06/09/17 18:31 7782-49-206/02/17 15:2010.0 5.0 1
Silver ND ug/L 06/09/17 18:31 7440-22-406/02/17 15:2010.0 2.5 1
Tin ND ug/L 06/09/17 18:31 7440-31-506/02/17 15:201002.5 1
Vanadium 14.2J ug/L 06/09/17 18:31 7440-62-206/02/17 15:2025.0 2.5 1
Zinc 55.6 ug/L 06/09/17 18:31 7440-66-606/02/17 15:2010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.24J ug/L 06/06/17 16:48 7440-28-006/01/17 11:305.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 03:59 7439-97-606/06/17 14:590.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/13/17 12:45 83-32-906/07/17 16:1010.0 1.6 1
Acenaphthylene ND ug/L 06/13/17 12:45 208-96-806/07/17 16:1010.0 1.5 1
Acetophenone ND ug/L 06/13/17 12:45 98-86-206/07/17 16:1010.0 1.9 1
2-Acetylaminofluorene ND ug/L 06/13/17 12:45 53-96-3 L206/07/17 16:1020.0 1.6 1
4-Aminobiphenyl ND ug/L 06/13/17 12:45 92-67-106/07/17 16:1020.0 1.7 1
Anthracene ND ug/L 06/13/17 12:45 120-12-706/07/17 16:1010.0 1.7 1
Benzo(a)anthracene ND ug/L 06/13/17 12:45 56-55-306/07/17 16:1010.0 2.1 1
Benzo(a)pyrene ND ug/L 06/13/17 12:45 50-32-806/07/17 16:1010.0 2.2 1
Benzo(b)fluoranthene ND ug/L 06/13/17 12:45 205-99-206/07/17 16:1010.0 2.2 1
Benzo(g,h,i)perylene ND ug/L 06/13/17 12:45 191-24-206/07/17 16:1010.0 2.1 1
Benzo(k)fluoranthene ND ug/L 06/13/17 12:45 207-08-906/07/17 16:1010.0 2.0 1
Benzyl alcohol ND ug/L 06/13/17 12:45 100-51-6 L206/07/17 16:1020.0 3.1 1
4-Bromophenylphenyl ether ND ug/L 06/13/17 12:45 101-55-306/07/17 16:1010.0 1.5 1
Butylbenzylphthalate ND ug/L 06/13/17 12:45 85-68-706/07/17 16:1010.0 2.5 1
4-Chloro-3-methylphenol ND ug/L 06/13/17 12:45 59-50-706/07/17 16:1020.0 2.8 1
4-Chloroaniline ND ug/L 06/13/17 12:45 106-47-806/07/17 16:1020.0 2.8 1
Chlorobenzilate ND ug/L 06/13/17 12:45 510-15-606/07/17 16:1010.0 2.2 1
bis(2-Chloroethoxy)methane ND ug/L 06/13/17 12:45 111-91-1 L206/07/17 16:1010.0 1.6 1
bis(2-Chloroethyl) ether ND ug/L 06/13/17 12:45 111-44-4 L206/07/17 16:1010.0 1.7 1
2-Chloronaphthalene ND ug/L 06/13/17 12:45 91-58-7 L206/07/17 16:1010.0 1.6 1
2-Chlorophenol ND ug/L 06/13/17 12:45 95-57-8 L206/07/17 16:1010.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/13/17 12:45 7005-72-306/07/17 16:1010.0 1.6 1
Chrysene ND ug/L 06/13/17 12:45 218-01-906/07/17 16:1010.0 2.1 1
Diallate ND ug/L 06/13/17 12:45 2303-16-406/07/17 16:1010.0 1.6 1
Dibenz(a,h)anthracene ND ug/L 06/13/17 12:45 53-70-306/07/17 16:1010.0 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 19 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-1 Lab ID:92342479001 Collected:05/31/17 14:00 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Dibenzofuran ND ug/L 06/13/17 12:45 132-64-906/07/17 16:1010.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 06/13/17 12:45 91-94-106/07/17 16:1020.0 3.9 1
2,4-Dichlorophenol ND ug/L 06/13/17 12:45 120-83-2 L206/07/17 16:1010.0 1.6 1
2,6-Dichlorophenol ND ug/L 06/13/17 12:45 87-65-0 L206/07/17 16:1010.0 1.5 1
Diethylphthalate ND ug/L 06/13/17 12:45 84-66-206/07/17 16:1060001.6 1
Dimethoate ND ug/L 06/13/17 12:45 60-51-506/07/17 16:1020.0 1.8 1
P-Dimethylaminoazobenzene ND ug/L 06/13/17 12:45 60-11-706/07/17 16:1010.0 1.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/13/17 12:45 57-97-606/07/17 16:1010.0 2.4 1
3,3'-Dimethylbenzidine ND ug/L 06/13/17 12:45 119-93-706/07/17 16:1010.0 3.9 1
2,4-Dimethylphenol ND ug/L 06/13/17 12:45 105-67-9 L206/07/17 16:1010.0 1.6 1
Dimethylphthalate ND ug/L 06/13/17 12:45 131-11-306/07/17 16:1010.0 1.4 1
Di-n-butylphthalate ND ug/L 06/13/17 12:45 84-74-206/07/17 16:1010.0 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/13/17 12:45 534-52-106/07/17 16:1050.0 2.2 1
1,3-Dinitrobenzene ND ug/L 06/13/17 12:45 99-65-006/07/17 16:1020.0 1.3 1
2,4-Dinitrophenol ND ug/L 06/13/17 12:45 51-28-506/07/17 16:1050.0 5.1 1
2,4-Dinitrotoluene ND ug/L 06/13/17 12:45 121-14-206/07/17 16:1010.0 1.5 1
2,6-Dinitrotoluene ND ug/L 06/13/17 12:45 606-20-206/07/17 16:1010.0 1.4 1
Di-n-octylphthalate ND ug/L 06/13/17 12:45 117-84-006/07/17 16:1010.0 1.5 1
Diphenylamine ND ug/L 06/13/17 12:45 122-39-406/07/17 16:1010.0 1.4 1
Disulfoton ND ug/L 06/13/17 12:45 298-04-406/07/17 16:1010.0 1.5 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/13/17 12:45 117-81-706/07/17 16:1015.0 2.3 1
Ethyl methanesulfonate ND ug/L 06/13/17 12:45 62-50-0 L206/07/17 16:1020.0 1.6 1
Famphur ND ug/L 06/13/17 12:45 52-85-706/07/17 16:1020.0 5.7 1
Fluoranthene ND ug/L 06/13/17 12:45 206-44-006/07/17 16:1010.0 2.2 1
Fluorene ND ug/L 06/13/17 12:45 86-73-706/07/17 16:1010.0 1.6 1
Hexachlorobenzene ND ug/L 06/13/17 12:45 118-74-106/07/17 16:1010.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 06/13/17 12:45 77-47-4 L206/07/17 16:1010.0 1.3 1
Hexachloroethane ND ug/L 06/13/17 12:45 67-72-1 L206/07/17 16:1010.0 1.8 1
Hexachloropropene ND ug/L 06/13/17 12:45 1888-71-706/07/17 16:1010.0 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/13/17 12:45 193-39-506/07/17 16:1010.0 2.0 1
Isodrin ND ug/L 06/13/17 12:45 465-73-606/07/17 16:1020.0 2.5 1
Isophorone ND ug/L 06/13/17 12:45 78-59-1 L206/07/17 16:1010.0 1.5 1
Isosafrole ND ug/L 06/13/17 12:45 120-58-1 L206/07/17 16:1010.0 1.5 1
Kepone ND ug/L 06/13/17 12:45 143-50-006/07/17 16:1020.0 4.5 1
Methapyrilene ND ug/L 06/13/17 12:45 91-80-506/07/17 16:101003.0 1
3-Methylcholanthrene ND ug/L 06/13/17 12:45 56-49-506/07/17 16:1010.0 2.7 1
Methyl methanesulfonate ND ug/L 06/13/17 12:45 66-27-306/07/17 16:1010.0 1.1 1
2-Methylnaphthalene ND ug/L 06/13/17 12:45 91-57-6 L206/07/17 16:1010.0 1.4 1
Methyl parathion ND ug/L 06/13/17 12:45 298-00-006/07/17 16:1010.0 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 06/13/17 12:45 95-48-7 L206/07/17 16:1010.0 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/13/17 12:45 15831-10-4 L206/07/17 16:1010.0 1.4 1
1-Naphthalenamine ND ug/L 06/13/17 12:45 134-32-706/07/17 16:1010.0 1.3 1
2-Naphthalenamine ND ug/L 06/13/17 12:45 91-59-806/07/17 16:1010.0 2.2 1
1,4-Naphthoquinone ND ug/L 06/13/17 12:45 130-15-406/07/17 16:1010.0 0.99 1
2-Nitroaniline ND ug/L 06/13/17 12:45 88-74-406/07/17 16:1050.0 2.3 1
3-Nitroaniline ND ug/L 06/13/17 12:45 99-09-206/07/17 16:1050.0 2.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 20 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-1 Lab ID:92342479001 Collected:05/31/17 14:00 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Nitroaniline ND ug/L 06/13/17 12:45 100-01-606/07/17 16:1020.0 3.4 1
Nitrobenzene ND ug/L 06/13/17 12:45 98-95-3 L206/07/17 16:1010.0 1.6 1
2-Nitrophenol ND ug/L 06/13/17 12:45 88-75-5 L206/07/17 16:1010.0 1.6 1
4-Nitrophenol ND ug/L 06/13/17 12:45 100-02-706/07/17 16:1050.0 4.3 1
5-Nitro-o-toluidine ND ug/L 06/13/17 12:45 99-55-8 L206/07/17 16:1010.0 1.9 1
N-Nitrosodiethylamine ND ug/L 06/13/17 12:45 55-18-5 L206/07/17 16:1020.0 1.4 1
N-Nitrosodimethylamine ND ug/L 06/13/17 12:45 62-75-906/07/17 16:1010.0 1.6 1
N-Nitroso-di-n-butylamine ND ug/L 06/13/17 12:45 924-16-3 L206/07/17 16:1010.0 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 06/13/17 12:45 621-64-7 L206/07/17 16:1010.0 1.7 1
N-Nitrosodiphenylamine ND ug/L 06/13/17 12:45 86-30-606/07/17 16:1010.0 1.4 1
N-Nitrosomethylethylamine ND ug/L 06/13/17 12:45 10595-95-6 L206/07/17 16:1010.0 1.4 1
N-Nitrosopiperidine ND ug/L 06/13/17 12:45 100-75-4 L206/07/17 16:1020.0 1.7 1
N-Nitrosopyrrolidine ND ug/L 06/13/17 12:45 930-55-2 L206/07/17 16:1010.0 1.7 1
O,O,O-Triethylphosphorothioate ND ug/L 06/13/17 12:45 126-68-1 L206/07/17 16:1010.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/13/17 12:45 108-60-106/07/17 16:1010.0 1.8 1
Parathion (Ethyl parathion)ND ug/L 06/13/17 12:45 56-38-2 L206/07/17 16:1010.0 1.5 1
Pentachlorobenzene ND ug/L 06/13/17 12:45 608-93-506/07/17 16:1010.0 1.5 1
Pentachloronitrobenzene ND ug/L 06/13/17 12:45 82-68-806/07/17 16:1020.0 1.7 1
Pentachlorophenol ND ug/L 06/13/17 12:45 87-86-506/07/17 16:1025.0 3.5 1
Phenacetin ND ug/L 06/13/17 12:45 62-44-206/07/17 16:1020.0 1.9 1
Phenanthrene ND ug/L 06/13/17 12:45 85-01-806/07/17 16:1010.0 1.6 1
Phenol ND ug/L 06/13/17 12:45 108-95-206/07/17 16:1010.0 1.3 1
p-Phenylenediamine ND ug/L 06/13/17 12:45 106-50-3 L206/07/17 16:1010.0 2.2 1
Phorate ND ug/L 06/13/17 12:45 298-02-2 L206/07/17 16:1010.0 1.7 1
Pronamide ND ug/L 06/13/17 12:45 23950-58-5 L206/07/17 16:1010.0 2.0 1
Pyrene ND ug/L 06/13/17 12:45 129-00-006/07/17 16:1010.0 2.2 1
Safrole ND ug/L 06/13/17 12:45 94-59-7 L206/07/17 16:1010.0 1.3 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/13/17 12:45 95-94-306/07/17 16:1010.0 1.3 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/13/17 12:45 58-90-206/07/17 16:1010.0 2.9 1
Thionazin ND ug/L 06/13/17 12:45 297-97-2 L206/07/17 16:1020.0 1.7 1
O-Toluidine ND ug/L 06/13/17 12:45 95-53-4 L206/07/17 16:1010.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 06/13/17 12:45 95-95-406/07/17 16:1010.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/13/17 12:45 88-06-206/07/17 16:1010.0 1.4 1
1,3,5-Trinitrobenzene ND ug/L 06/13/17 12:45 99-35-4 L206/07/17 16:1010.0 1.2 1
Surrogates
Nitrobenzene-d5 (S)76 %06/13/17 12:45 4165-60-0 1g06/07/17 16:1021-110 1
2-Fluorobiphenyl (S)92 %06/13/17 12:45 321-60-806/07/17 16:1027-110 1
Terphenyl-d14 (S)85 %06/13/17 12:45 1718-51-006/07/17 16:1031-107 1
Phenol-d6 (S)28 %06/13/17 12:45 13127-88-306/07/17 16:1010-110 1
2-Fluorophenol (S)44 %06/13/17 12:45 367-12-406/07/17 16:1012-110 1
2,4,6-Tribromophenol (S)86 %06/13/17 12:45 118-79-606/07/17 16:1027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 12.8J ug/L 06/02/17 02:39 67-64-110010.0 1
Acetonitrile ND ug/L 06/02/17 02:39 75-05-855.0 2.2 1
Acrolein ND ug/L 06/02/17 02:39 107-02-853.0 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-1 Lab ID:92342479001 Collected:05/31/17 14:00 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acrylonitrile ND ug/L 06/02/17 02:39 107-13-12001.9 1
Allyl chloride ND ug/L 06/02/17 02:39 107-05-110.0 1.5 1
Benzene ND ug/L 06/02/17 02:39 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/02/17 02:39 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/02/17 02:39 75-27-41.0 0.18 1
Bromoform ND ug/L 06/02/17 02:39 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/02/17 02:39 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/02/17 02:39 78-93-31000.96 1
Carbon disulfide ND ug/L 06/02/17 02:39 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/02/17 02:39 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/02/17 02:39 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/02/17 02:39 75-00-310.0 0.54 1
Chloroform ND ug/L 06/02/17 02:39 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/02/17 02:39 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/02/17 02:39 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/02/17 02:39 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/02/17 02:39 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/02/17 02:39 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/02/17 02:39 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/02/17 02:39 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/02/17 02:39 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/02/17 02:39 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/02/17 02:39 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/02/17 02:39 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/02/17 02:39 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/02/17 02:39 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/02/17 02:39 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/02/17 02:39 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/02/17 02:39 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/02/17 02:39 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/02/17 02:39 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/02/17 02:39 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/02/17 02:39 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/02/17 02:39 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/02/17 02:39 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/02/17 02:39 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/02/17 02:39 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/02/17 02:39 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/02/17 02:39 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/02/17 02:39 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/02/17 02:39 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/02/17 02:39 126-98-71000.93 1
Methylene Chloride ND ug/L 06/02/17 02:39 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/02/17 02:39 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/02/17 02:39 108-10-11000.33 1
Naphthalene ND ug/L 06/02/17 02:39 91-20-310.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-1 Lab ID:92342479001 Collected:05/31/17 14:00 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Propionitrile ND ug/L 06/02/17 02:39 107-12-01503.6 1
Styrene ND ug/L 06/02/17 02:39 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/02/17 02:39 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/02/17 02:39 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/02/17 02:39 127-18-41.0 0.46 1
Toluene ND ug/L 06/02/17 02:39 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/02/17 02:39 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/02/17 02:39 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/02/17 02:39 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/02/17 02:39 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/02/17 02:39 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/02/17 02:39 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/02/17 02:39 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/02/17 02:39 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/02/17 02:39 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)116 %06/02/17 02:39 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %06/02/17 02:39 17060-07-070-130 1
Toluene-d8 (S)111 %06/02/17 02:39 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/01/17 21:00 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 5.5J ug/L 06/01/17 17:25 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-2 Lab ID:92342479002 Collected:05/31/17 13:15 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/06/17 15:52 309-00-206/02/17 10:090.050 0.050 1
alpha-BHC ND ug/L 06/06/17 15:52 319-84-606/02/17 10:090.050 0.050 1
beta-BHC ND ug/L 06/06/17 15:52 319-85-706/02/17 10:090.050 0.050 1
delta-BHC ND ug/L 06/06/17 15:52 319-86-806/02/17 10:090.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/06/17 15:52 58-89-906/02/17 10:090.050 0.050 1
Chlordane (Technical)ND ug/L 06/06/17 15:52 57-74-906/02/17 10:090.50 0.20 1
4,4'-DDD ND ug/L 06/06/17 15:52 72-54-806/02/17 10:090.10 0.050 1
4,4'-DDE ND ug/L 06/06/17 15:52 72-55-906/02/17 10:090.10 0.050 1
4,4'-DDT ND ug/L 06/06/17 15:52 50-29-306/02/17 10:090.10 0.050 1
Dieldrin ND ug/L 06/06/17 15:52 60-57-106/02/17 10:090.075 0.050 1
Endosulfan I ND ug/L 06/06/17 15:52 959-98-806/02/17 10:090.10 0.050 1
Endosulfan II ND ug/L 06/06/17 15:52 33213-65-906/02/17 10:090.10 0.050 1
Endosulfan sulfate ND ug/L 06/06/17 15:52 1031-07-806/02/17 10:090.10 0.050 1
Endrin ND ug/L 06/06/17 15:52 72-20-806/02/17 10:090.10 0.050 1
Endrin aldehyde ND ug/L 06/06/17 15:52 7421-93-406/02/17 10:090.10 0.050 1
Heptachlor ND ug/L 06/06/17 15:52 76-44-806/02/17 10:090.050 0.050 1
Heptachlor epoxide ND ug/L 06/06/17 15:52 1024-57-306/02/17 10:090.075 0.050 1
Methoxychlor ND ug/L 06/06/17 15:52 72-43-506/02/17 10:091.0 0.15 1
Toxaphene ND ug/L 06/06/17 15:52 8001-35-206/02/17 10:091.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)93 %06/06/17 15:52 877-09-806/02/17 10:0920-130 1
Decachlorobiphenyl (S)89 %06/06/17 15:52 2051-24-306/02/17 10:0920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/02/17 16:45 12674-11-206/02/17 10:090.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/02/17 16:45 11104-28-206/02/17 10:090.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/02/17 16:45 11141-16-506/02/17 10:090.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/02/17 16:45 53469-21-906/02/17 10:090.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/02/17 16:45 12672-29-606/02/17 10:090.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/02/17 16:45 11097-69-106/02/17 10:090.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/02/17 16:45 11096-82-506/02/17 10:090.50 0.50 1
Surrogates
Decachlorobiphenyl (S)94 %06/02/17 16:45 2051-24-306/02/17 10:0910-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/07/17 03:03 94-75-7 L106/05/17 16:500.98 0.23 1
Dinoseb ND ug/L 06/07/17 03:03 88-85-7 L106/05/17 16:500.20 0.059 1
Pentachlorophenol ND ug/L 06/07/17 03:03 87-86-506/05/17 16:500.030 0.018 1
2,4,5-T ND ug/L 06/07/17 03:03 93-76-506/05/17 16:500.20 0.044 1
2,4,5-TP (Silvex)ND ug/L 06/07/17 03:03 93-72-106/05/17 16:500.20 0.051 1
Surrogates
2,4-DCAA (S)109 %06/07/17 03:03 19719-28-906/05/17 16:5039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/09/17 18:34 7440-36-006/02/17 15:206.0 3.9 1
Arsenic ND ug/L 06/09/17 18:34 7440-38-206/02/17 15:2010.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-2 Lab ID:92342479002 Collected:05/31/17 13:15 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Barium 36.5J ug/L 06/09/17 18:34 7440-39-306/02/17 15:201002.5 1
Beryllium ND ug/L 06/09/17 18:34 7440-41-706/02/17 15:201.0 0.50 1
Cadmium 0.97J ug/L 06/09/17 18:34 7440-43-906/02/17 15:201.0 0.50 1
Chromium ND ug/L 06/09/17 18:34 7440-47-306/02/17 15:2010.0 2.5 1
Cobalt ND ug/L 06/09/17 18:34 7440-48-406/02/17 15:2010.0 2.5 1
Copper ND ug/L 06/09/17 18:34 7440-50-806/02/17 15:2010.0 2.5 1
Lead ND ug/L 06/09/17 18:34 7439-92-106/02/17 15:2010.0 2.5 1
Nickel ND ug/L 06/09/17 18:34 7440-02-006/02/17 15:2050.0 2.5 1
Selenium ND ug/L 06/09/17 18:34 7782-49-206/02/17 15:2010.0 5.0 1
Silver ND ug/L 06/09/17 18:34 7440-22-406/02/17 15:2010.0 2.5 1
Tin ND ug/L 06/09/17 18:34 7440-31-506/02/17 15:201002.5 1
Vanadium ND ug/L 06/09/17 18:34 7440-62-206/02/17 15:2025.0 2.5 1
Zinc ND ug/L 06/09/17 18:34 7440-66-606/02/17 15:2010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.022J ug/L 06/06/17 16:50 7440-28-006/01/17 11:305.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 04:02 7439-97-606/06/17 14:590.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/13/17 13:14 83-32-906/07/17 16:1010.0 1.6 1
Acenaphthylene ND ug/L 06/13/17 13:14 208-96-806/07/17 16:1010.0 1.5 1
Acetophenone ND ug/L 06/13/17 13:14 98-86-206/07/17 16:1010.0 1.9 1
2-Acetylaminofluorene ND ug/L 06/13/17 13:14 53-96-3 L206/07/17 16:1020.0 1.6 1
4-Aminobiphenyl ND ug/L 06/13/17 13:14 92-67-1 M106/07/17 16:1020.0 1.7 1
Anthracene ND ug/L 06/13/17 13:14 120-12-706/07/17 16:1010.0 1.7 1
Benzo(a)anthracene ND ug/L 06/13/17 13:14 56-55-306/07/17 16:1010.0 2.1 1
Benzo(a)pyrene ND ug/L 06/13/17 13:14 50-32-806/07/17 16:1010.0 2.2 1
Benzo(b)fluoranthene ND ug/L 06/13/17 13:14 205-99-206/07/17 16:1010.0 2.2 1
Benzo(g,h,i)perylene ND ug/L 06/13/17 13:14 191-24-206/07/17 16:1010.0 2.1 1
Benzo(k)fluoranthene ND ug/L 06/13/17 13:14 207-08-906/07/17 16:1010.0 2.0 1
Benzyl alcohol ND ug/L 06/13/17 13:14 100-51-6 L206/07/17 16:1020.0 3.1 1
4-Bromophenylphenyl ether ND ug/L 06/13/17 13:14 101-55-306/07/17 16:1010.0 1.5 1
Butylbenzylphthalate ND ug/L 06/13/17 13:14 85-68-706/07/17 16:1010.0 2.5 1
4-Chloro-3-methylphenol ND ug/L 06/13/17 13:14 59-50-706/07/17 16:1020.0 2.8 1
4-Chloroaniline ND ug/L 06/13/17 13:14 106-47-806/07/17 16:1020.0 2.8 1
Chlorobenzilate ND ug/L 06/13/17 13:14 510-15-606/07/17 16:1010.0 2.2 1
bis(2-Chloroethoxy)methane ND ug/L 06/13/17 13:14 111-91-1 L206/07/17 16:1010.0 1.6 1
bis(2-Chloroethyl) ether ND ug/L 06/13/17 13:14 111-44-4 L206/07/17 16:1010.0 1.7 1
2-Chloronaphthalene ND ug/L 06/13/17 13:14 91-58-7 L206/07/17 16:1010.0 1.6 1
2-Chlorophenol ND ug/L 06/13/17 13:14 95-57-8 L206/07/17 16:1010.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/13/17 13:14 7005-72-306/07/17 16:1010.0 1.6 1
Chrysene ND ug/L 06/13/17 13:14 218-01-906/07/17 16:1010.0 2.1 1
Diallate ND ug/L 06/13/17 13:14 2303-16-406/07/17 16:1010.0 1.6 1
Dibenz(a,h)anthracene ND ug/L 06/13/17 13:14 53-70-306/07/17 16:1010.0 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-2 Lab ID:92342479002 Collected:05/31/17 13:15 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Dibenzofuran ND ug/L 06/13/17 13:14 132-64-906/07/17 16:1010.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 06/13/17 13:14 91-94-106/07/17 16:1020.0 3.9 1
2,4-Dichlorophenol ND ug/L 06/13/17 13:14 120-83-2 L206/07/17 16:1010.0 1.6 1
2,6-Dichlorophenol ND ug/L 06/13/17 13:14 87-65-0 L206/07/17 16:1010.0 1.5 1
Diethylphthalate ND ug/L 06/13/17 13:14 84-66-206/07/17 16:1060001.6 1
Dimethoate ND ug/L 06/13/17 13:14 60-51-506/07/17 16:1020.0 1.8 1
P-Dimethylaminoazobenzene ND ug/L 06/13/17 13:14 60-11-7 M106/07/17 16:1010.0 1.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/13/17 13:14 57-97-606/07/17 16:1010.0 2.4 1
3,3'-Dimethylbenzidine ND ug/L 06/13/17 13:14 119-93-7 M106/07/17 16:1010.0 3.9 1
2,4-Dimethylphenol ND ug/L 06/13/17 13:14 105-67-9 L206/07/17 16:1010.0 1.6 1
Dimethylphthalate ND ug/L 06/13/17 13:14 131-11-306/07/17 16:1010.0 1.4 1
Di-n-butylphthalate ND ug/L 06/13/17 13:14 84-74-206/07/17 16:1010.0 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/13/17 13:14 534-52-106/07/17 16:1050.0 2.2 1
1,3-Dinitrobenzene ND ug/L 06/13/17 13:14 99-65-006/07/17 16:1020.0 1.3 1
2,4-Dinitrophenol ND ug/L 06/13/17 13:14 51-28-506/07/17 16:1050.0 5.1 1
2,4-Dinitrotoluene ND ug/L 06/13/17 13:14 121-14-206/07/17 16:1010.0 1.5 1
2,6-Dinitrotoluene ND ug/L 06/13/17 13:14 606-20-206/07/17 16:1010.0 1.4 1
Di-n-octylphthalate ND ug/L 06/13/17 13:14 117-84-006/07/17 16:1010.0 1.5 1
Diphenylamine ND ug/L 06/13/17 13:14 122-39-406/07/17 16:1010.0 1.4 1
Disulfoton ND ug/L 06/13/17 13:14 298-04-406/07/17 16:1010.0 1.5 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/13/17 13:14 117-81-706/07/17 16:1015.0 2.3 1
Ethyl methanesulfonate ND ug/L 06/13/17 13:14 62-50-0 L206/07/17 16:1020.0 1.6 1
Famphur ND ug/L 06/13/17 13:14 52-85-7 M106/07/17 16:1020.0 5.7 1
Fluoranthene ND ug/L 06/13/17 13:14 206-44-006/07/17 16:1010.0 2.2 1
Fluorene ND ug/L 06/13/17 13:14 86-73-706/07/17 16:1010.0 1.6 1
Hexachlorobenzene ND ug/L 06/13/17 13:14 118-74-106/07/17 16:1010.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 06/13/17 13:14 77-47-4 L206/07/17 16:1010.0 1.3 1
Hexachloroethane ND ug/L 06/13/17 13:14 67-72-1 L206/07/17 16:1010.0 1.8 1
Hexachloropropene ND ug/L 06/13/17 13:14 1888-71-7 M106/07/17 16:1010.0 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/13/17 13:14 193-39-506/07/17 16:1010.0 2.0 1
Isodrin ND ug/L 06/13/17 13:14 465-73-606/07/17 16:1020.0 2.5 1
Isophorone ND ug/L 06/13/17 13:14 78-59-1 L206/07/17 16:1010.0 1.5 1
Isosafrole ND ug/L 06/13/17 13:14 120-58-1 L206/07/17 16:1010.0 1.5 1
Kepone ND ug/L 06/13/17 13:14 143-50-006/07/17 16:1020.0 4.5 1
Methapyrilene ND ug/L 06/13/17 13:14 91-80-5 M106/07/17 16:101003.0 1
3-Methylcholanthrene ND ug/L 06/13/17 13:14 56-49-506/07/17 16:1010.0 2.7 1
Methyl methanesulfonate ND ug/L 06/13/17 13:14 66-27-306/07/17 16:1010.0 1.1 1
2-Methylnaphthalene ND ug/L 06/13/17 13:14 91-57-6 L206/07/17 16:1010.0 1.4 1
Methyl parathion ND ug/L 06/13/17 13:14 298-00-006/07/17 16:1010.0 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 06/13/17 13:14 95-48-7 L206/07/17 16:1010.0 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/13/17 13:14 15831-10-4 L206/07/17 16:1010.0 1.4 1
1-Naphthalenamine ND ug/L 06/13/17 13:14 134-32-7 M106/07/17 16:1010.0 1.3 1
2-Naphthalenamine ND ug/L 06/13/17 13:14 91-59-8 M106/07/17 16:1010.0 2.2 1
1,4-Naphthoquinone ND ug/L 06/13/17 13:14 130-15-406/07/17 16:1010.0 0.99 1
2-Nitroaniline ND ug/L 06/13/17 13:14 88-74-406/07/17 16:1050.0 2.3 1
3-Nitroaniline ND ug/L 06/13/17 13:14 99-09-206/07/17 16:1050.0 2.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-2 Lab ID:92342479002 Collected:05/31/17 13:15 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Nitroaniline ND ug/L 06/13/17 13:14 100-01-606/07/17 16:1020.0 3.4 1
Nitrobenzene ND ug/L 06/13/17 13:14 98-95-3 L206/07/17 16:1010.0 1.6 1
2-Nitrophenol ND ug/L 06/13/17 13:14 88-75-5 L206/07/17 16:1010.0 1.6 1
4-Nitrophenol ND ug/L 06/13/17 13:14 100-02-706/07/17 16:1050.0 4.3 1
5-Nitro-o-toluidine ND ug/L 06/13/17 13:14 99-55-8 L206/07/17 16:1010.0 1.9 1
N-Nitrosodiethylamine ND ug/L 06/13/17 13:14 55-18-5 L206/07/17 16:1020.0 1.4 1
N-Nitrosodimethylamine ND ug/L 06/13/17 13:14 62-75-906/07/17 16:1010.0 1.6 1
N-Nitroso-di-n-butylamine ND ug/L 06/13/17 13:14 924-16-3 L206/07/17 16:1010.0 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 06/13/17 13:14 621-64-7 L206/07/17 16:1010.0 1.7 1
N-Nitrosodiphenylamine ND ug/L 06/13/17 13:14 86-30-606/07/17 16:1010.0 1.4 1
N-Nitrosomethylethylamine ND ug/L 06/13/17 13:14 10595-95-6 L206/07/17 16:1010.0 1.4 1
N-Nitrosopiperidine ND ug/L 06/13/17 13:14 100-75-4 L206/07/17 16:1020.0 1.7 1
N-Nitrosopyrrolidine ND ug/L 06/13/17 13:14 930-55-2 L206/07/17 16:1010.0 1.7 1
O,O,O-Triethylphosphorothioate ND ug/L 06/13/17 13:14 126-68-1 L206/07/17 16:1010.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/13/17 13:14 108-60-106/07/17 16:1010.0 1.8 1
Parathion (Ethyl parathion)ND ug/L 06/13/17 13:14 56-38-2 L206/07/17 16:1010.0 1.5 1
Pentachlorobenzene ND ug/L 06/13/17 13:14 608-93-506/07/17 16:1010.0 1.5 1
Pentachloronitrobenzene ND ug/L 06/13/17 13:14 82-68-806/07/17 16:1020.0 1.7 1
Pentachlorophenol ND ug/L 06/13/17 13:14 87-86-506/07/17 16:1025.0 3.5 1
Phenacetin ND ug/L 06/13/17 13:14 62-44-206/07/17 16:1020.0 1.9 1
Phenanthrene ND ug/L 06/13/17 13:14 85-01-806/07/17 16:1010.0 1.6 1
Phenol ND ug/L 06/13/17 13:14 108-95-206/07/17 16:1010.0 1.3 1
p-Phenylenediamine ND ug/L 06/13/17 13:14 106-50-3 L206/07/17 16:1010.0 2.2 1
Phorate ND ug/L 06/13/17 13:14 298-02-2 L206/07/17 16:1010.0 1.7 1
Pronamide ND ug/L 06/13/17 13:14 23950-58-5 L206/07/17 16:1010.0 2.0 1
Pyrene ND ug/L 06/13/17 13:14 129-00-006/07/17 16:1010.0 2.2 1
Safrole ND ug/L 06/13/17 13:14 94-59-7 L206/07/17 16:1010.0 1.3 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/13/17 13:14 95-94-306/07/17 16:1010.0 1.3 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/13/17 13:14 58-90-2 M106/07/17 16:1010.0 2.9 1
Thionazin ND ug/L 06/13/17 13:14 297-97-2 L206/07/17 16:1020.0 1.7 1
O-Toluidine ND ug/L 06/13/17 13:14 95-53-4 L206/07/17 16:1010.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 06/13/17 13:14 95-95-406/07/17 16:1010.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/13/17 13:14 88-06-206/07/17 16:1010.0 1.4 1
1,3,5-Trinitrobenzene ND ug/L 06/13/17 13:14 99-35-4 L206/07/17 16:1010.0 1.2 1
Surrogates
Nitrobenzene-d5 (S)67 %06/13/17 13:14 4165-60-0 1g06/07/17 16:1021-110 1
2-Fluorobiphenyl (S)83 %06/13/17 13:14 321-60-806/07/17 16:1027-110 1
Terphenyl-d14 (S)76 %06/13/17 13:14 1718-51-006/07/17 16:1031-107 1
Phenol-d6 (S)26 %06/13/17 13:14 13127-88-306/07/17 16:1010-110 1
2-Fluorophenol (S)36 %06/13/17 13:14 367-12-406/07/17 16:1012-110 1
2,4,6-Tribromophenol (S)72 %06/13/17 13:14 118-79-606/07/17 16:1027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 10.1J ug/L 06/02/17 02:56 67-64-110010.0 1
Acetonitrile ND ug/L 06/02/17 02:56 75-05-855.0 2.2 1
Acrolein ND ug/L 06/02/17 02:56 107-02-853.0 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-2 Lab ID:92342479002 Collected:05/31/17 13:15 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acrylonitrile ND ug/L 06/02/17 02:56 107-13-12001.9 1
Allyl chloride ND ug/L 06/02/17 02:56 107-05-110.0 1.5 1
Benzene ND ug/L 06/02/17 02:56 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/02/17 02:56 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/02/17 02:56 75-27-41.0 0.18 1
Bromoform ND ug/L 06/02/17 02:56 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/02/17 02:56 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/02/17 02:56 78-93-31000.96 1
Carbon disulfide ND ug/L 06/02/17 02:56 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/02/17 02:56 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/02/17 02:56 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/02/17 02:56 75-00-310.0 0.54 1
Chloroform ND ug/L 06/02/17 02:56 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/02/17 02:56 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/02/17 02:56 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/02/17 02:56 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/02/17 02:56 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/02/17 02:56 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/02/17 02:56 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/02/17 02:56 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/02/17 02:56 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/02/17 02:56 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/02/17 02:56 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/02/17 02:56 75-71-85.0 0.21 1
1,1-Dichloroethane 2.6J ug/L 06/02/17 02:56 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/02/17 02:56 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/02/17 02:56 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 1.7J ug/L 06/02/17 02:56 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/02/17 02:56 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/02/17 02:56 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/02/17 02:56 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/02/17 02:56 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/02/17 02:56 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/02/17 02:56 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/02/17 02:56 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/02/17 02:56 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/02/17 02:56 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/02/17 02:56 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/02/17 02:56 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/02/17 02:56 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/02/17 02:56 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/02/17 02:56 126-98-71000.93 1
Methylene Chloride ND ug/L 06/02/17 02:56 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/02/17 02:56 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/02/17 02:56 108-10-11000.33 1
Naphthalene ND ug/L 06/02/17 02:56 91-20-310.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
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Page 28 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-2 Lab ID:92342479002 Collected:05/31/17 13:15 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Propionitrile ND ug/L 06/02/17 02:56 107-12-01503.6 1
Styrene ND ug/L 06/02/17 02:56 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/02/17 02:56 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/02/17 02:56 79-34-53.0 0.40 1
Tetrachloroethene 0.68J ug/L 06/02/17 02:56 127-18-41.0 0.46 1
Toluene ND ug/L 06/02/17 02:56 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/02/17 02:56 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/02/17 02:56 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/02/17 02:56 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/02/17 02:56 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/02/17 02:56 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/02/17 02:56 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/02/17 02:56 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/02/17 02:56 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/02/17 02:56 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)115 %06/02/17 02:56 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %06/02/17 02:56 17060-07-070-130 1
Toluene-d8 (S)112 %06/02/17 02:56 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/01/17 21:00 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 4.4J ug/L 06/01/17 17:28 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-3R Lab ID:92342479003 Collected:05/31/17 13:25 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/06/17 16:10 309-00-206/02/17 10:090.050 0.050 1
alpha-BHC ND ug/L 06/06/17 16:10 319-84-606/02/17 10:090.050 0.050 1
beta-BHC ND ug/L 06/06/17 16:10 319-85-706/02/17 10:090.050 0.050 1
delta-BHC ND ug/L 06/06/17 16:10 319-86-806/02/17 10:090.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/06/17 16:10 58-89-906/02/17 10:090.050 0.050 1
Chlordane (Technical)ND ug/L 06/06/17 16:10 57-74-906/02/17 10:090.50 0.20 1
4,4'-DDD ND ug/L 06/06/17 16:10 72-54-806/02/17 10:090.10 0.050 1
4,4'-DDE ND ug/L 06/06/17 16:10 72-55-906/02/17 10:090.10 0.050 1
4,4'-DDT ND ug/L 06/06/17 16:10 50-29-306/02/17 10:090.10 0.050 1
Dieldrin ND ug/L 06/06/17 16:10 60-57-106/02/17 10:090.075 0.050 1
Endosulfan I ND ug/L 06/06/17 16:10 959-98-806/02/17 10:090.10 0.050 1
Endosulfan II ND ug/L 06/06/17 16:10 33213-65-906/02/17 10:090.10 0.050 1
Endosulfan sulfate ND ug/L 06/06/17 16:10 1031-07-806/02/17 10:090.10 0.050 1
Endrin ND ug/L 06/06/17 16:10 72-20-806/02/17 10:090.10 0.050 1
Endrin aldehyde ND ug/L 06/06/17 16:10 7421-93-406/02/17 10:090.10 0.050 1
Heptachlor ND ug/L 06/06/17 16:10 76-44-806/02/17 10:090.050 0.050 1
Heptachlor epoxide ND ug/L 06/06/17 16:10 1024-57-306/02/17 10:090.075 0.050 1
Methoxychlor ND ug/L 06/06/17 16:10 72-43-506/02/17 10:091.0 0.15 1
Toxaphene ND ug/L 06/06/17 16:10 8001-35-206/02/17 10:091.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)90 %06/06/17 16:10 877-09-806/02/17 10:0920-130 1
Decachlorobiphenyl (S)79 %06/06/17 16:10 2051-24-306/02/17 10:0920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/02/17 17:05 12674-11-206/02/17 10:090.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/02/17 17:05 11104-28-206/02/17 10:090.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/02/17 17:05 11141-16-506/02/17 10:090.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/02/17 17:05 53469-21-906/02/17 10:090.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/02/17 17:05 12672-29-606/02/17 10:090.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/02/17 17:05 11097-69-106/02/17 10:090.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/02/17 17:05 11096-82-506/02/17 10:090.50 0.50 1
Surrogates
Decachlorobiphenyl (S)76 %06/02/17 17:05 2051-24-306/02/17 10:0910-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/07/17 03:33 94-75-7 L106/05/17 16:500.98 0.23 1
Dinoseb ND ug/L 06/07/17 03:33 88-85-7 L106/05/17 16:500.20 0.060 1
Pentachlorophenol ND ug/L 06/07/17 03:33 87-86-506/05/17 16:500.030 0.018 1
2,4,5-T ND ug/L 06/07/17 03:33 93-76-506/05/17 16:500.20 0.044 1
2,4,5-TP (Silvex)ND ug/L 06/07/17 03:33 93-72-106/05/17 16:500.20 0.051 1
Surrogates
2,4-DCAA (S)101 %06/07/17 03:33 19719-28-906/05/17 16:5039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/09/17 18:38 7440-36-006/02/17 15:206.0 3.9 1
Arsenic ND ug/L 06/09/17 18:38 7440-38-206/02/17 15:2010.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-3R Lab ID:92342479003 Collected:05/31/17 13:25 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Barium 50.6J ug/L 06/09/17 18:38 7440-39-306/02/17 15:201002.5 1
Beryllium ND ug/L 06/09/17 18:38 7440-41-706/02/17 15:201.0 0.50 1
Cadmium 1.2 ug/L 06/09/17 18:38 7440-43-906/02/17 15:201.0 0.50 1
Chromium ND ug/L 06/09/17 18:38 7440-47-306/02/17 15:2010.0 2.5 1
Cobalt ND ug/L 06/09/17 18:38 7440-48-406/02/17 15:2010.0 2.5 1
Copper ND ug/L 06/09/17 18:38 7440-50-806/02/17 15:2010.0 2.5 1
Lead ND ug/L 06/09/17 18:38 7439-92-106/02/17 15:2010.0 2.5 1
Nickel 3.0J ug/L 06/09/17 18:38 7440-02-006/02/17 15:2050.0 2.5 1
Selenium ND ug/L 06/09/17 18:38 7782-49-206/02/17 15:2010.0 5.0 1
Silver ND ug/L 06/09/17 18:38 7440-22-406/02/17 15:2010.0 2.5 1
Tin ND ug/L 06/09/17 18:38 7440-31-506/02/17 15:201002.5 1
Vanadium ND ug/L 06/09/17 18:38 7440-62-206/02/17 15:2025.0 2.5 1
Zinc ND ug/L 06/09/17 18:38 7440-66-606/02/17 15:2010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/06/17 16:52 7440-28-006/01/17 11:305.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 04:04 7439-97-606/06/17 14:590.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/13/17 14:24 83-32-906/07/17 16:1010.0 1.6 1
Acenaphthylene ND ug/L 06/13/17 14:24 208-96-806/07/17 16:1010.0 1.5 1
Acetophenone ND ug/L 06/13/17 14:24 98-86-206/07/17 16:1010.0 1.9 1
2-Acetylaminofluorene ND ug/L 06/13/17 14:24 53-96-3 L206/07/17 16:1020.0 1.6 1
4-Aminobiphenyl ND ug/L 06/13/17 14:24 92-67-106/07/17 16:1020.0 1.7 1
Anthracene 1.8J ug/L 06/13/17 14:24 120-12-706/07/17 16:1010.0 1.7 1
Benzo(a)anthracene 2.2J ug/L 06/13/17 14:24 56-55-306/07/17 16:1010.0 2.1 1
Benzo(a)pyrene 2.3J ug/L 06/13/17 14:24 50-32-806/07/17 16:1010.0 2.2 1
Benzo(b)fluoranthene 2.6J ug/L 06/13/17 14:24 205-99-206/07/17 16:1010.0 2.2 1
Benzo(g,h,i)perylene 2.5J ug/L 06/13/17 14:24 191-24-206/07/17 16:1010.0 2.1 1
Benzo(k)fluoranthene 2.5J ug/L 06/13/17 14:24 207-08-906/07/17 16:1010.0 2.0 1
Benzyl alcohol ND ug/L 06/13/17 14:24 100-51-6 L206/07/17 16:1020.0 3.1 1
4-Bromophenylphenyl ether 1.5J ug/L 06/13/17 14:24 101-55-306/07/17 16:1010.0 1.5 1
Butylbenzylphthalate ND ug/L 06/13/17 14:24 85-68-706/07/17 16:1010.0 2.5 1
4-Chloro-3-methylphenol ND ug/L 06/13/17 14:24 59-50-706/07/17 16:1020.0 2.8 1
4-Chloroaniline ND ug/L 06/13/17 14:24 106-47-806/07/17 16:1020.0 2.8 1
Chlorobenzilate ND ug/L 06/13/17 14:24 510-15-606/07/17 16:1010.0 2.2 1
bis(2-Chloroethoxy)methane ND ug/L 06/13/17 14:24 111-91-1 L206/07/17 16:1010.0 1.6 1
bis(2-Chloroethyl) ether ND ug/L 06/13/17 14:24 111-44-4 L206/07/17 16:1010.0 1.7 1
2-Chloronaphthalene ND ug/L 06/13/17 14:24 91-58-7 L206/07/17 16:1010.0 1.6 1
2-Chlorophenol ND ug/L 06/13/17 14:24 95-57-8 L206/07/17 16:1010.0 1.5 1
4-Chlorophenylphenyl ether 1.8J ug/L 06/13/17 14:24 7005-72-306/07/17 16:1010.0 1.6 1
Chrysene 2.5J ug/L 06/13/17 14:24 218-01-906/07/17 16:1010.0 2.1 1
Diallate ND ug/L 06/13/17 14:24 2303-16-406/07/17 16:1010.0 1.6 1
Dibenz(a,h)anthracene 2.3J ug/L 06/13/17 14:24 53-70-306/07/17 16:1010.0 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-3R Lab ID:92342479003 Collected:05/31/17 13:25 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Dibenzofuran ND ug/L 06/13/17 14:24 132-64-906/07/17 16:1010.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 06/13/17 14:24 91-94-106/07/17 16:1020.0 3.9 1
2,4-Dichlorophenol ND ug/L 06/13/17 14:24 120-83-2 L206/07/17 16:1010.0 1.6 1
2,6-Dichlorophenol ND ug/L 06/13/17 14:24 87-65-0 L206/07/17 16:1010.0 1.5 1
Diethylphthalate ND ug/L 06/13/17 14:24 84-66-206/07/17 16:1060001.6 1
Dimethoate ND ug/L 06/13/17 14:24 60-51-506/07/17 16:1020.0 1.8 1
P-Dimethylaminoazobenzene ND ug/L 06/13/17 14:24 60-11-706/07/17 16:1010.0 1.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/13/17 14:24 57-97-606/07/17 16:1010.0 2.4 1
3,3'-Dimethylbenzidine ND ug/L 06/13/17 14:24 119-93-706/07/17 16:1010.0 3.9 1
2,4-Dimethylphenol ND ug/L 06/13/17 14:24 105-67-9 L206/07/17 16:1010.0 1.6 1
Dimethylphthalate ND ug/L 06/13/17 14:24 131-11-306/07/17 16:1010.0 1.4 1
Di-n-butylphthalate ND ug/L 06/13/17 14:24 84-74-206/07/17 16:1010.0 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/13/17 14:24 534-52-106/07/17 16:1050.0 2.2 1
1,3-Dinitrobenzene ND ug/L 06/13/17 14:24 99-65-006/07/17 16:1020.0 1.3 1
2,4-Dinitrophenol ND ug/L 06/13/17 14:24 51-28-506/07/17 16:1050.0 5.1 1
2,4-Dinitrotoluene ND ug/L 06/13/17 14:24 121-14-206/07/17 16:1010.0 1.5 1
2,6-Dinitrotoluene ND ug/L 06/13/17 14:24 606-20-206/07/17 16:1010.0 1.4 1
Di-n-octylphthalate 1.5J ug/L 06/13/17 14:24 117-84-006/07/17 16:1010.0 1.5 1
Diphenylamine ND ug/L 06/13/17 14:24 122-39-406/07/17 16:1010.0 1.4 1
Disulfoton ND ug/L 06/13/17 14:24 298-04-406/07/17 16:1010.0 1.5 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/13/17 14:24 117-81-706/07/17 16:1015.0 2.3 1
Ethyl methanesulfonate ND ug/L 06/13/17 14:24 62-50-0 L206/07/17 16:1020.0 1.6 1
Famphur ND ug/L 06/13/17 14:24 52-85-706/07/17 16:1020.0 5.7 1
Fluoranthene ND ug/L 06/13/17 14:24 206-44-006/07/17 16:1010.0 2.2 1
Fluorene ND ug/L 06/13/17 14:24 86-73-706/07/17 16:1010.0 1.6 1
Hexachlorobenzene 2.2J ug/L 06/13/17 14:24 118-74-106/07/17 16:1010.0 1.7 1
Hexachlorocyclopentadiene 2.5J ug/L 06/13/17 14:24 77-47-4 L206/07/17 16:1010.0 1.3 1
Hexachloroethane 2.3J ug/L 06/13/17 14:24 67-72-1 L206/07/17 16:1010.0 1.8 1
Hexachloropropene 2.1J ug/L 06/13/17 14:24 1888-71-706/07/17 16:1010.0 1.2 1
Indeno(1,2,3-cd)pyrene 2.4J ug/L 06/13/17 14:24 193-39-506/07/17 16:1010.0 2.0 1
Isodrin ND ug/L 06/13/17 14:24 465-73-606/07/17 16:1020.0 2.5 1
Isophorone ND ug/L 06/13/17 14:24 78-59-1 L206/07/17 16:1010.0 1.5 1
Isosafrole ND ug/L 06/13/17 14:24 120-58-1 L206/07/17 16:1010.0 1.5 1
Kepone ND ug/L 06/13/17 14:24 143-50-006/07/17 16:1020.0 4.5 1
Methapyrilene ND ug/L 06/13/17 14:24 91-80-506/07/17 16:101003.0 1
3-Methylcholanthrene ND ug/L 06/13/17 14:24 56-49-506/07/17 16:1010.0 2.7 1
Methyl methanesulfonate ND ug/L 06/13/17 14:24 66-27-306/07/17 16:1010.0 1.1 1
2-Methylnaphthalene ND ug/L 06/13/17 14:24 91-57-6 L206/07/17 16:1010.0 1.4 1
Methyl parathion ND ug/L 06/13/17 14:24 298-00-006/07/17 16:1010.0 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 06/13/17 14:24 95-48-7 L206/07/17 16:1010.0 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/13/17 14:24 15831-10-4 L206/07/17 16:1010.0 1.4 1
1-Naphthalenamine ND ug/L 06/13/17 14:24 134-32-706/07/17 16:1010.0 1.3 1
2-Naphthalenamine ND ug/L 06/13/17 14:24 91-59-806/07/17 16:1010.0 2.2 1
1,4-Naphthoquinone ND ug/L 06/13/17 14:24 130-15-406/07/17 16:1010.0 0.99 1
2-Nitroaniline ND ug/L 06/13/17 14:24 88-74-406/07/17 16:1050.0 2.3 1
3-Nitroaniline ND ug/L 06/13/17 14:24 99-09-206/07/17 16:1050.0 2.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-3R Lab ID:92342479003 Collected:05/31/17 13:25 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Nitroaniline ND ug/L 06/13/17 14:24 100-01-606/07/17 16:1020.0 3.4 1
Nitrobenzene ND ug/L 06/13/17 14:24 98-95-3 L206/07/17 16:1010.0 1.6 1
2-Nitrophenol ND ug/L 06/13/17 14:24 88-75-5 L206/07/17 16:1010.0 1.6 1
4-Nitrophenol ND ug/L 06/13/17 14:24 100-02-706/07/17 16:1050.0 4.3 1
5-Nitro-o-toluidine ND ug/L 06/13/17 14:24 99-55-8 L206/07/17 16:1010.0 1.9 1
N-Nitrosodiethylamine ND ug/L 06/13/17 14:24 55-18-5 L206/07/17 16:1020.0 1.4 1
N-Nitrosodimethylamine ND ug/L 06/13/17 14:24 62-75-906/07/17 16:1010.0 1.6 1
N-Nitroso-di-n-butylamine ND ug/L 06/13/17 14:24 924-16-3 L206/07/17 16:1010.0 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 06/13/17 14:24 621-64-7 L206/07/17 16:1010.0 1.7 1
N-Nitrosodiphenylamine ND ug/L 06/13/17 14:24 86-30-606/07/17 16:1010.0 1.4 1
N-Nitrosomethylethylamine ND ug/L 06/13/17 14:24 10595-95-6 L206/07/17 16:1010.0 1.4 1
N-Nitrosopiperidine ND ug/L 06/13/17 14:24 100-75-4 L206/07/17 16:1020.0 1.7 1
N-Nitrosopyrrolidine ND ug/L 06/13/17 14:24 930-55-2 L206/07/17 16:1010.0 1.7 1
O,O,O-Triethylphosphorothioate ND ug/L 06/13/17 14:24 126-68-1 L206/07/17 16:1010.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/13/17 14:24 108-60-106/07/17 16:1010.0 1.8 1
Parathion (Ethyl parathion)ND ug/L 06/13/17 14:24 56-38-2 L206/07/17 16:1010.0 1.5 1
Pentachlorobenzene 2.1J ug/L 06/13/17 14:24 608-93-506/07/17 16:1010.0 1.5 1
Pentachloronitrobenzene ND ug/L 06/13/17 14:24 82-68-806/07/17 16:1020.0 1.7 1
Pentachlorophenol ND ug/L 06/13/17 14:24 87-86-506/07/17 16:1025.0 3.5 1
Phenacetin ND ug/L 06/13/17 14:24 62-44-206/07/17 16:1020.0 1.9 1
Phenanthrene 1.8J ug/L 06/13/17 14:24 85-01-806/07/17 16:1010.0 1.6 1
Phenol ND ug/L 06/13/17 14:24 108-95-206/07/17 16:1010.0 1.3 1
p-Phenylenediamine ND ug/L 06/13/17 14:24 106-50-3 L206/07/17 16:1010.0 2.2 1
Phorate ND ug/L 06/13/17 14:24 298-02-2 L206/07/17 16:1010.0 1.7 1
Pronamide ND ug/L 06/13/17 14:24 23950-58-5 L206/07/17 16:1010.0 2.0 1
Pyrene ND ug/L 06/13/17 14:24 129-00-006/07/17 16:1010.0 2.2 1
Safrole ND ug/L 06/13/17 14:24 94-59-7 L206/07/17 16:1010.0 1.3 1
1,2,4,5-Tetrachlorobenzene 2.0J ug/L 06/13/17 14:24 95-94-306/07/17 16:1010.0 1.3 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/13/17 14:24 58-90-206/07/17 16:1010.0 2.9 1
Thionazin ND ug/L 06/13/17 14:24 297-97-2 L206/07/17 16:1020.0 1.7 1
O-Toluidine ND ug/L 06/13/17 14:24 95-53-4 L206/07/17 16:1010.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 06/13/17 14:24 95-95-406/07/17 16:1010.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/13/17 14:24 88-06-206/07/17 16:1010.0 1.4 1
1,3,5-Trinitrobenzene ND ug/L 06/13/17 14:24 99-35-4 L206/07/17 16:1010.0 1.2 1
Surrogates
Nitrobenzene-d5 (S)77 %06/13/17 14:24 4165-60-0 1g06/07/17 16:1021-110 1
2-Fluorobiphenyl (S)91 %06/13/17 14:24 321-60-806/07/17 16:1027-110 1
Terphenyl-d14 (S)68 %06/13/17 14:24 1718-51-006/07/17 16:1031-107 1
Phenol-d6 (S)24 %06/13/17 14:24 13127-88-306/07/17 16:1010-110 1
2-Fluorophenol (S)39 %06/13/17 14:24 367-12-406/07/17 16:1012-110 1
2,4,6-Tribromophenol (S)85 %06/13/17 14:24 118-79-606/07/17 16:1027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/02/17 03:14 67-64-110010.0 1
Acetonitrile ND ug/L 06/02/17 03:14 75-05-855.0 2.2 1
Acrolein ND ug/L 06/02/17 03:14 107-02-853.0 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-3R Lab ID:92342479003 Collected:05/31/17 13:25 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acrylonitrile ND ug/L 06/02/17 03:14 107-13-12001.9 1
Allyl chloride ND ug/L 06/02/17 03:14 107-05-110.0 1.5 1
Benzene ND ug/L 06/02/17 03:14 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/02/17 03:14 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/02/17 03:14 75-27-41.0 0.18 1
Bromoform ND ug/L 06/02/17 03:14 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/02/17 03:14 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/02/17 03:14 78-93-31000.96 1
Carbon disulfide ND ug/L 06/02/17 03:14 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/02/17 03:14 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/02/17 03:14 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/02/17 03:14 75-00-310.0 0.54 1
Chloroform ND ug/L 06/02/17 03:14 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/02/17 03:14 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/02/17 03:14 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/02/17 03:14 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/02/17 03:14 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/02/17 03:14 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/02/17 03:14 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/02/17 03:14 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/02/17 03:14 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/02/17 03:14 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/02/17 03:14 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/02/17 03:14 75-71-85.0 0.21 1
1,1-Dichloroethane 2.5J ug/L 06/02/17 03:14 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/02/17 03:14 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/02/17 03:14 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 3.1J ug/L 06/02/17 03:14 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/02/17 03:14 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/02/17 03:14 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/02/17 03:14 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/02/17 03:14 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/02/17 03:14 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/02/17 03:14 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/02/17 03:14 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/02/17 03:14 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/02/17 03:14 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/02/17 03:14 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/02/17 03:14 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/02/17 03:14 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/02/17 03:14 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/02/17 03:14 126-98-71000.93 1
Methylene Chloride ND ug/L 06/02/17 03:14 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/02/17 03:14 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/02/17 03:14 108-10-11000.33 1
Naphthalene ND ug/L 06/02/17 03:14 91-20-310.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-3R Lab ID:92342479003 Collected:05/31/17 13:25 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Propionitrile ND ug/L 06/02/17 03:14 107-12-01503.6 1
Styrene ND ug/L 06/02/17 03:14 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/02/17 03:14 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/02/17 03:14 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/02/17 03:14 127-18-41.0 0.46 1
Toluene ND ug/L 06/02/17 03:14 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/02/17 03:14 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/02/17 03:14 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/02/17 03:14 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/02/17 03:14 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/02/17 03:14 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/02/17 03:14 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/02/17 03:14 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/02/17 03:14 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/02/17 03:14 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)116 %06/02/17 03:14 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %06/02/17 03:14 17060-07-070-130 1
Toluene-d8 (S)112 %06/02/17 03:14 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/01/17 21:00 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/01/17 17:32 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-4S Lab ID:92342479004 Collected:05/31/17 13:00 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/06/17 16:28 309-00-206/02/17 10:090.050 0.050 1
alpha-BHC ND ug/L 06/06/17 16:28 319-84-606/02/17 10:090.050 0.050 1
beta-BHC ND ug/L 06/06/17 16:28 319-85-706/02/17 10:090.050 0.050 1
delta-BHC ND ug/L 06/06/17 16:28 319-86-806/02/17 10:090.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/06/17 16:28 58-89-906/02/17 10:090.050 0.050 1
Chlordane (Technical)ND ug/L 06/06/17 16:28 57-74-906/02/17 10:090.50 0.20 1
4,4'-DDD ND ug/L 06/06/17 16:28 72-54-806/02/17 10:090.10 0.050 1
4,4'-DDE ND ug/L 06/06/17 16:28 72-55-906/02/17 10:090.10 0.050 1
4,4'-DDT ND ug/L 06/06/17 16:28 50-29-306/02/17 10:090.10 0.050 1
Dieldrin ND ug/L 06/06/17 16:28 60-57-106/02/17 10:090.075 0.050 1
Endosulfan I ND ug/L 06/06/17 16:28 959-98-806/02/17 10:090.10 0.050 1
Endosulfan II ND ug/L 06/06/17 16:28 33213-65-906/02/17 10:090.10 0.050 1
Endosulfan sulfate ND ug/L 06/06/17 16:28 1031-07-806/02/17 10:090.10 0.050 1
Endrin ND ug/L 06/06/17 16:28 72-20-806/02/17 10:090.10 0.050 1
Endrin aldehyde ND ug/L 06/06/17 16:28 7421-93-406/02/17 10:090.10 0.050 1
Heptachlor ND ug/L 06/06/17 16:28 76-44-806/02/17 10:090.050 0.050 1
Heptachlor epoxide ND ug/L 06/06/17 16:28 1024-57-306/02/17 10:090.075 0.050 1
Methoxychlor ND ug/L 06/06/17 16:28 72-43-506/02/17 10:091.0 0.15 1
Toxaphene ND ug/L 06/06/17 16:28 8001-35-206/02/17 10:091.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)88 %06/06/17 16:28 877-09-806/02/17 10:0920-130 1
Decachlorobiphenyl (S)68 %06/06/17 16:28 2051-24-306/02/17 10:0920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/02/17 17:26 12674-11-206/02/17 10:090.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/02/17 17:26 11104-28-206/02/17 10:090.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/02/17 17:26 11141-16-506/02/17 10:090.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/02/17 17:26 53469-21-906/02/17 10:090.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/02/17 17:26 12672-29-606/02/17 10:090.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/02/17 17:26 11097-69-106/02/17 10:090.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/02/17 17:26 11096-82-506/02/17 10:090.50 0.50 1
Surrogates
Decachlorobiphenyl (S)64 %06/02/17 17:26 2051-24-306/02/17 10:0910-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/07/17 04:02 94-75-7 L106/05/17 16:501.0 0.24 1
Dinoseb ND ug/L 06/07/17 04:02 88-85-7 L106/05/17 16:500.20 0.060 1
Pentachlorophenol ND ug/L 06/07/17 04:02 87-86-506/05/17 16:500.030 0.018 1
2,4,5-T ND ug/L 06/07/17 04:02 93-76-506/05/17 16:500.20 0.045 1
2,4,5-TP (Silvex)ND ug/L 06/07/17 04:02 93-72-106/05/17 16:500.20 0.052 1
Surrogates
2,4-DCAA (S)98 %06/07/17 04:02 19719-28-906/05/17 16:5039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/09/17 15:01 7440-36-006/02/17 15:206.0 3.9 1
Arsenic ND ug/L 06/09/17 15:01 7440-38-206/02/17 15:2010.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-4S Lab ID:92342479004 Collected:05/31/17 13:00 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Barium 69.9J ug/L 06/11/17 04:10 7440-39-306/02/17 15:201002.5 1
Beryllium ND ug/L 06/11/17 04:10 7440-41-706/02/17 15:201.0 0.50 1
Cadmium 4.6 ug/L 06/09/17 15:01 7440-43-906/02/17 15:201.0 0.50 1
Chromium 3.1J ug/L 06/09/17 15:01 7440-47-306/02/17 15:2010.0 2.5 1
Cobalt ND ug/L 06/09/17 15:01 7440-48-406/02/17 15:2010.0 2.5 1
Copper ND ug/L 06/11/17 04:10 7440-50-806/02/17 15:2010.0 2.5 1
Lead ND ug/L 06/09/17 15:01 7439-92-106/02/17 15:2010.0 2.5 1
Nickel 2.5J ug/L 06/09/17 15:01 7440-02-006/02/17 15:2050.0 2.5 1
Selenium ND ug/L 06/09/17 15:01 7782-49-206/02/17 15:2010.0 5.0 1
Silver ND ug/L 06/11/17 04:10 7440-22-406/02/17 15:2010.0 2.5 1
Tin ND ug/L 06/09/17 15:01 7440-31-506/02/17 15:201002.5 1
Vanadium 5.3J ug/L 06/09/17 15:01 7440-62-206/02/17 15:2025.0 2.5 1
Zinc 13.0 ug/L 06/09/17 15:01 7440-66-606/02/17 15:2010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.056J ug/L 06/06/17 16:54 7440-28-006/01/17 11:305.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 04:11 7439-97-606/06/17 14:590.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/13/17 14:53 83-32-906/07/17 16:1010.0 1.6 1
Acenaphthylene ND ug/L 06/13/17 14:53 208-96-806/07/17 16:1010.0 1.5 1
Acetophenone ND ug/L 06/13/17 14:53 98-86-206/07/17 16:1010.0 1.9 1
2-Acetylaminofluorene ND ug/L 06/13/17 14:53 53-96-3 L206/07/17 16:1020.0 1.6 1
4-Aminobiphenyl ND ug/L 06/13/17 14:53 92-67-106/07/17 16:1020.0 1.7 1
Anthracene ND ug/L 06/13/17 14:53 120-12-706/07/17 16:1010.0 1.7 1
Benzo(a)anthracene ND ug/L 06/13/17 14:53 56-55-306/07/17 16:1010.0 2.1 1
Benzo(a)pyrene ND ug/L 06/13/17 14:53 50-32-806/07/17 16:1010.0 2.2 1
Benzo(b)fluoranthene ND ug/L 06/13/17 14:53 205-99-206/07/17 16:1010.0 2.2 1
Benzo(g,h,i)perylene ND ug/L 06/13/17 14:53 191-24-206/07/17 16:1010.0 2.1 1
Benzo(k)fluoranthene ND ug/L 06/13/17 14:53 207-08-906/07/17 16:1010.0 2.0 1
Benzyl alcohol ND ug/L 06/13/17 14:53 100-51-6 L206/07/17 16:1020.0 3.1 1
4-Bromophenylphenyl ether ND ug/L 06/13/17 14:53 101-55-306/07/17 16:1010.0 1.5 1
Butylbenzylphthalate ND ug/L 06/13/17 14:53 85-68-706/07/17 16:1010.0 2.5 1
4-Chloro-3-methylphenol ND ug/L 06/13/17 14:53 59-50-706/07/17 16:1020.0 2.8 1
4-Chloroaniline ND ug/L 06/13/17 14:53 106-47-806/07/17 16:1020.0 2.8 1
Chlorobenzilate ND ug/L 06/13/17 14:53 510-15-606/07/17 16:1010.0 2.2 1
bis(2-Chloroethoxy)methane ND ug/L 06/13/17 14:53 111-91-1 L206/07/17 16:1010.0 1.6 1
bis(2-Chloroethyl) ether ND ug/L 06/13/17 14:53 111-44-4 L206/07/17 16:1010.0 1.7 1
2-Chloronaphthalene ND ug/L 06/13/17 14:53 91-58-7 L206/07/17 16:1010.0 1.6 1
2-Chlorophenol ND ug/L 06/13/17 14:53 95-57-8 L206/07/17 16:1010.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/13/17 14:53 7005-72-306/07/17 16:1010.0 1.6 1
Chrysene ND ug/L 06/13/17 14:53 218-01-906/07/17 16:1010.0 2.1 1
Diallate ND ug/L 06/13/17 14:53 2303-16-406/07/17 16:1010.0 1.6 1
Dibenz(a,h)anthracene ND ug/L 06/13/17 14:53 53-70-306/07/17 16:1010.0 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-4S Lab ID:92342479004 Collected:05/31/17 13:00 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Dibenzofuran ND ug/L 06/13/17 14:53 132-64-906/07/17 16:1010.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 06/13/17 14:53 91-94-106/07/17 16:1020.0 3.9 1
2,4-Dichlorophenol ND ug/L 06/13/17 14:53 120-83-2 L206/07/17 16:1010.0 1.6 1
2,6-Dichlorophenol ND ug/L 06/13/17 14:53 87-65-0 L206/07/17 16:1010.0 1.5 1
Diethylphthalate ND ug/L 06/13/17 14:53 84-66-206/07/17 16:1060001.6 1
Dimethoate ND ug/L 06/13/17 14:53 60-51-506/07/17 16:1020.0 1.8 1
P-Dimethylaminoazobenzene ND ug/L 06/13/17 14:53 60-11-706/07/17 16:1010.0 1.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/13/17 14:53 57-97-606/07/17 16:1010.0 2.4 1
3,3'-Dimethylbenzidine ND ug/L 06/13/17 14:53 119-93-706/07/17 16:1010.0 3.9 1
2,4-Dimethylphenol ND ug/L 06/13/17 14:53 105-67-9 L206/07/17 16:1010.0 1.6 1
Dimethylphthalate ND ug/L 06/13/17 14:53 131-11-306/07/17 16:1010.0 1.4 1
Di-n-butylphthalate ND ug/L 06/13/17 14:53 84-74-206/07/17 16:1010.0 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/13/17 14:53 534-52-106/07/17 16:1050.0 2.2 1
1,3-Dinitrobenzene ND ug/L 06/13/17 14:53 99-65-006/07/17 16:1020.0 1.3 1
2,4-Dinitrophenol ND ug/L 06/13/17 14:53 51-28-506/07/17 16:1050.0 5.1 1
2,4-Dinitrotoluene ND ug/L 06/13/17 14:53 121-14-206/07/17 16:1010.0 1.5 1
2,6-Dinitrotoluene ND ug/L 06/13/17 14:53 606-20-206/07/17 16:1010.0 1.4 1
Di-n-octylphthalate ND ug/L 06/13/17 14:53 117-84-006/07/17 16:1010.0 1.5 1
Diphenylamine ND ug/L 06/13/17 14:53 122-39-406/07/17 16:1010.0 1.4 1
Disulfoton ND ug/L 06/13/17 14:53 298-04-406/07/17 16:1010.0 1.5 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/13/17 14:53 117-81-706/07/17 16:1015.0 2.3 1
Ethyl methanesulfonate ND ug/L 06/13/17 14:53 62-50-0 L206/07/17 16:1020.0 1.6 1
Famphur ND ug/L 06/13/17 14:53 52-85-706/07/17 16:1020.0 5.7 1
Fluoranthene ND ug/L 06/13/17 14:53 206-44-006/07/17 16:1010.0 2.2 1
Fluorene ND ug/L 06/13/17 14:53 86-73-706/07/17 16:1010.0 1.6 1
Hexachlorobenzene ND ug/L 06/13/17 14:53 118-74-106/07/17 16:1010.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 06/13/17 14:53 77-47-4 L206/07/17 16:1010.0 1.3 1
Hexachloroethane ND ug/L 06/13/17 14:53 67-72-1 L206/07/17 16:1010.0 1.8 1
Hexachloropropene ND ug/L 06/13/17 14:53 1888-71-706/07/17 16:1010.0 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/13/17 14:53 193-39-506/07/17 16:1010.0 2.0 1
Isodrin ND ug/L 06/13/17 14:53 465-73-606/07/17 16:1020.0 2.5 1
Isophorone ND ug/L 06/13/17 14:53 78-59-1 L206/07/17 16:1010.0 1.5 1
Isosafrole ND ug/L 06/13/17 14:53 120-58-1 L206/07/17 16:1010.0 1.5 1
Kepone ND ug/L 06/13/17 14:53 143-50-006/07/17 16:1020.0 4.5 1
Methapyrilene ND ug/L 06/13/17 14:53 91-80-506/07/17 16:101003.0 1
3-Methylcholanthrene ND ug/L 06/13/17 14:53 56-49-506/07/17 16:1010.0 2.7 1
Methyl methanesulfonate ND ug/L 06/13/17 14:53 66-27-306/07/17 16:1010.0 1.1 1
2-Methylnaphthalene ND ug/L 06/13/17 14:53 91-57-6 L206/07/17 16:1010.0 1.4 1
Methyl parathion ND ug/L 06/13/17 14:53 298-00-006/07/17 16:1010.0 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 06/13/17 14:53 95-48-7 L206/07/17 16:1010.0 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/13/17 14:53 15831-10-4 L206/07/17 16:1010.0 1.4 1
1-Naphthalenamine ND ug/L 06/13/17 14:53 134-32-706/07/17 16:1010.0 1.3 1
2-Naphthalenamine ND ug/L 06/13/17 14:53 91-59-806/07/17 16:1010.0 2.2 1
1,4-Naphthoquinone ND ug/L 06/13/17 14:53 130-15-406/07/17 16:1010.0 0.99 1
2-Nitroaniline ND ug/L 06/13/17 14:53 88-74-406/07/17 16:1050.0 2.3 1
3-Nitroaniline ND ug/L 06/13/17 14:53 99-09-206/07/17 16:1050.0 2.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 38 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-4S Lab ID:92342479004 Collected:05/31/17 13:00 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Nitroaniline ND ug/L 06/13/17 14:53 100-01-606/07/17 16:1020.0 3.4 1
Nitrobenzene ND ug/L 06/13/17 14:53 98-95-3 L206/07/17 16:1010.0 1.6 1
2-Nitrophenol ND ug/L 06/13/17 14:53 88-75-5 L206/07/17 16:1010.0 1.6 1
4-Nitrophenol ND ug/L 06/13/17 14:53 100-02-706/07/17 16:1050.0 4.3 1
5-Nitro-o-toluidine ND ug/L 06/13/17 14:53 99-55-8 L206/07/17 16:1010.0 1.9 1
N-Nitrosodiethylamine ND ug/L 06/13/17 14:53 55-18-5 L206/07/17 16:1020.0 1.4 1
N-Nitrosodimethylamine ND ug/L 06/13/17 14:53 62-75-906/07/17 16:1010.0 1.6 1
N-Nitroso-di-n-butylamine ND ug/L 06/13/17 14:53 924-16-3 L206/07/17 16:1010.0 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 06/13/17 14:53 621-64-7 L206/07/17 16:1010.0 1.7 1
N-Nitrosodiphenylamine ND ug/L 06/13/17 14:53 86-30-606/07/17 16:1010.0 1.4 1
N-Nitrosomethylethylamine ND ug/L 06/13/17 14:53 10595-95-6 L206/07/17 16:1010.0 1.4 1
N-Nitrosopiperidine ND ug/L 06/13/17 14:53 100-75-4 L206/07/17 16:1020.0 1.7 1
N-Nitrosopyrrolidine ND ug/L 06/13/17 14:53 930-55-2 L206/07/17 16:1010.0 1.7 1
O,O,O-Triethylphosphorothioate ND ug/L 06/13/17 14:53 126-68-1 L206/07/17 16:1010.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/13/17 14:53 108-60-106/07/17 16:1010.0 1.8 1
Parathion (Ethyl parathion)ND ug/L 06/13/17 14:53 56-38-2 L206/07/17 16:1010.0 1.5 1
Pentachlorobenzene ND ug/L 06/13/17 14:53 608-93-506/07/17 16:1010.0 1.5 1
Pentachloronitrobenzene ND ug/L 06/13/17 14:53 82-68-806/07/17 16:1020.0 1.7 1
Pentachlorophenol ND ug/L 06/13/17 14:53 87-86-506/07/17 16:1025.0 3.5 1
Phenacetin ND ug/L 06/13/17 14:53 62-44-206/07/17 16:1020.0 1.9 1
Phenanthrene ND ug/L 06/13/17 14:53 85-01-806/07/17 16:1010.0 1.6 1
Phenol ND ug/L 06/13/17 14:53 108-95-206/07/17 16:1010.0 1.3 1
p-Phenylenediamine ND ug/L 06/13/17 14:53 106-50-3 L206/07/17 16:1010.0 2.2 1
Phorate ND ug/L 06/13/17 14:53 298-02-2 L206/07/17 16:1010.0 1.7 1
Pronamide ND ug/L 06/13/17 14:53 23950-58-5 L206/07/17 16:1010.0 2.0 1
Pyrene ND ug/L 06/13/17 14:53 129-00-006/07/17 16:1010.0 2.2 1
Safrole ND ug/L 06/13/17 14:53 94-59-7 L206/07/17 16:1010.0 1.3 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/13/17 14:53 95-94-306/07/17 16:1010.0 1.3 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/13/17 14:53 58-90-206/07/17 16:1010.0 2.9 1
Thionazin ND ug/L 06/13/17 14:53 297-97-2 L206/07/17 16:1020.0 1.7 1
O-Toluidine ND ug/L 06/13/17 14:53 95-53-4 L206/07/17 16:1010.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 06/13/17 14:53 95-95-406/07/17 16:1010.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/13/17 14:53 88-06-206/07/17 16:1010.0 1.4 1
1,3,5-Trinitrobenzene ND ug/L 06/13/17 14:53 99-35-4 L206/07/17 16:1010.0 1.2 1
Surrogates
Nitrobenzene-d5 (S)67 %06/13/17 14:53 4165-60-0 1g06/07/17 16:1021-110 1
2-Fluorobiphenyl (S)83 %06/13/17 14:53 321-60-806/07/17 16:1027-110 1
Terphenyl-d14 (S)54 %06/13/17 14:53 1718-51-006/07/17 16:1031-107 1
Phenol-d6 (S)30 %06/13/17 14:53 13127-88-306/07/17 16:1010-110 1
2-Fluorophenol (S)42 %06/13/17 14:53 367-12-406/07/17 16:1012-110 1
2,4,6-Tribromophenol (S)75 %06/13/17 14:53 118-79-606/07/17 16:1027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/02/17 03:31 67-64-110010.0 1
Acetonitrile ND ug/L 06/02/17 03:31 75-05-855.0 2.2 1
Acrolein ND ug/L 06/02/17 03:31 107-02-853.0 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-4S Lab ID:92342479004 Collected:05/31/17 13:00 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acrylonitrile ND ug/L 06/02/17 03:31 107-13-12001.9 1
Allyl chloride ND ug/L 06/02/17 03:31 107-05-110.0 1.5 1
Benzene ND ug/L 06/02/17 03:31 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/02/17 03:31 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/02/17 03:31 75-27-41.0 0.18 1
Bromoform ND ug/L 06/02/17 03:31 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/02/17 03:31 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/02/17 03:31 78-93-31000.96 1
Carbon disulfide ND ug/L 06/02/17 03:31 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/02/17 03:31 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/02/17 03:31 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/02/17 03:31 75-00-310.0 0.54 1
Chloroform ND ug/L 06/02/17 03:31 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/02/17 03:31 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/02/17 03:31 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/02/17 03:31 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/02/17 03:31 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/02/17 03:31 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/02/17 03:31 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/02/17 03:31 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/02/17 03:31 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/02/17 03:31 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/02/17 03:31 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/02/17 03:31 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/02/17 03:31 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/02/17 03:31 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/02/17 03:31 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/02/17 03:31 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/02/17 03:31 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/02/17 03:31 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/02/17 03:31 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/02/17 03:31 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/02/17 03:31 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/02/17 03:31 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/02/17 03:31 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/02/17 03:31 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/02/17 03:31 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/02/17 03:31 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/02/17 03:31 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/02/17 03:31 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/02/17 03:31 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/02/17 03:31 126-98-71000.93 1
Methylene Chloride ND ug/L 06/02/17 03:31 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/02/17 03:31 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/02/17 03:31 108-10-11000.33 1
Naphthalene ND ug/L 06/02/17 03:31 91-20-310.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-4S Lab ID:92342479004 Collected:05/31/17 13:00 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Propionitrile ND ug/L 06/02/17 03:31 107-12-01503.6 1
Styrene ND ug/L 06/02/17 03:31 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/02/17 03:31 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/02/17 03:31 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/02/17 03:31 127-18-41.0 0.46 1
Toluene ND ug/L 06/02/17 03:31 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/02/17 03:31 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/02/17 03:31 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/02/17 03:31 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/02/17 03:31 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/02/17 03:31 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/02/17 03:31 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/02/17 03:31 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/02/17 03:31 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/02/17 03:31 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)115 %06/02/17 03:31 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %06/02/17 03:31 17060-07-070-130 1
Toluene-d8 (S)114 %06/02/17 03:31 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/01/17 21:00 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 5.9J ug/L 06/01/17 17:33 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-4D Lab ID:92342479005 Collected:05/31/17 13:15 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/06/17 17:05 309-00-206/02/17 10:090.050 0.050 1
alpha-BHC ND ug/L 06/06/17 17:05 319-84-606/02/17 10:090.050 0.050 1
beta-BHC ND ug/L 06/06/17 17:05 319-85-706/02/17 10:090.050 0.050 1
delta-BHC ND ug/L 06/06/17 17:05 319-86-806/02/17 10:090.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/06/17 17:05 58-89-906/02/17 10:090.050 0.050 1
Chlordane (Technical)ND ug/L 06/06/17 17:05 57-74-906/02/17 10:090.50 0.20 1
4,4'-DDD ND ug/L 06/06/17 17:05 72-54-806/02/17 10:090.10 0.050 1
4,4'-DDE ND ug/L 06/06/17 17:05 72-55-906/02/17 10:090.10 0.050 1
4,4'-DDT ND ug/L 06/06/17 17:05 50-29-306/02/17 10:090.10 0.050 1
Dieldrin ND ug/L 06/06/17 17:05 60-57-106/02/17 10:090.075 0.050 1
Endosulfan I ND ug/L 06/06/17 17:05 959-98-806/02/17 10:090.10 0.050 1
Endosulfan II ND ug/L 06/06/17 17:05 33213-65-906/02/17 10:090.10 0.050 1
Endosulfan sulfate ND ug/L 06/06/17 17:05 1031-07-806/02/17 10:090.10 0.050 1
Endrin ND ug/L 06/06/17 17:05 72-20-806/02/17 10:090.10 0.050 1
Endrin aldehyde ND ug/L 06/06/17 17:05 7421-93-406/02/17 10:090.10 0.050 1
Heptachlor ND ug/L 06/06/17 17:05 76-44-806/02/17 10:090.050 0.050 1
Heptachlor epoxide ND ug/L 06/06/17 17:05 1024-57-306/02/17 10:090.075 0.050 1
Methoxychlor ND ug/L 06/06/17 17:05 72-43-506/02/17 10:091.0 0.15 1
Toxaphene ND ug/L 06/06/17 17:05 8001-35-206/02/17 10:091.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)101 %06/06/17 17:05 877-09-806/02/17 10:0920-130 1
Decachlorobiphenyl (S)84 %06/06/17 17:05 2051-24-306/02/17 10:0920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/02/17 17:47 12674-11-206/02/17 10:090.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/02/17 17:47 11104-28-206/02/17 10:090.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/02/17 17:47 11141-16-506/02/17 10:090.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/02/17 17:47 53469-21-906/02/17 10:090.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/02/17 17:47 12672-29-606/02/17 10:090.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/02/17 17:47 11097-69-106/02/17 10:090.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/02/17 17:47 11096-82-506/02/17 10:090.50 0.50 1
Surrogates
Decachlorobiphenyl (S)79 %06/02/17 17:47 2051-24-306/02/17 10:0910-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/07/17 04:32 94-75-7 L106/05/17 16:500.98 0.23 1
Dinoseb ND ug/L 06/07/17 04:32 88-85-7 L106/05/17 16:500.20 0.059 1
Pentachlorophenol ND ug/L 06/07/17 04:32 87-86-506/05/17 16:500.029 0.018 1
2,4,5-T ND ug/L 06/07/17 04:32 93-76-506/05/17 16:500.20 0.044 1
2,4,5-TP (Silvex)ND ug/L 06/07/17 04:32 93-72-106/05/17 16:500.20 0.051 1
Surrogates
2,4-DCAA (S)104 %06/07/17 04:32 19719-28-906/05/17 16:5039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/09/17 16:08 7440-36-006/02/17 15:206.0 3.9 1
Arsenic ND ug/L 06/09/17 16:08 7440-38-206/02/17 15:2010.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-4D Lab ID:92342479005 Collected:05/31/17 13:15 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Barium 46.9J ug/L 06/09/17 16:08 7440-39-306/02/17 15:201002.5 1
Beryllium ND ug/L 06/09/17 16:08 7440-41-706/02/17 15:201.0 0.50 1
Cadmium 1.5 ug/L 06/09/17 16:08 7440-43-906/02/17 15:201.0 0.50 1
Chromium ND ug/L 06/09/17 16:08 7440-47-306/02/17 15:2010.0 2.5 1
Cobalt ND ug/L 06/09/17 16:08 7440-48-406/02/17 15:2010.0 2.5 1
Copper ND ug/L 06/09/17 16:08 7440-50-806/02/17 15:2010.0 2.5 1
Lead ND ug/L 06/09/17 16:08 7439-92-106/02/17 15:2010.0 2.5 1
Nickel ND ug/L 06/09/17 16:08 7440-02-006/02/17 15:2050.0 2.5 1
Selenium ND ug/L 06/09/17 16:08 7782-49-206/02/17 15:2010.0 5.0 1
Silver ND ug/L 06/09/17 16:08 7440-22-406/02/17 15:2010.0 2.5 1
Tin ND ug/L 06/09/17 16:08 7440-31-506/02/17 15:201002.5 1
Vanadium ND ug/L 06/09/17 16:08 7440-62-206/02/17 15:2025.0 2.5 1
Zinc ND ug/L 06/09/17 16:08 7440-66-606/02/17 15:2010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/06/17 16:56 7440-28-006/01/17 11:305.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 04:13 7439-97-606/06/17 14:590.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/13/17 15:23 83-32-906/07/17 16:1010.0 1.6 1
Acenaphthylene ND ug/L 06/13/17 15:23 208-96-806/07/17 16:1010.0 1.5 1
Acetophenone ND ug/L 06/13/17 15:23 98-86-206/07/17 16:1010.0 1.9 1
2-Acetylaminofluorene ND ug/L 06/13/17 15:23 53-96-3 L206/07/17 16:1020.0 1.6 1
4-Aminobiphenyl ND ug/L 06/13/17 15:23 92-67-106/07/17 16:1020.0 1.7 1
Anthracene ND ug/L 06/13/17 15:23 120-12-706/07/17 16:1010.0 1.7 1
Benzo(a)anthracene ND ug/L 06/13/17 15:23 56-55-306/07/17 16:1010.0 2.1 1
Benzo(a)pyrene ND ug/L 06/13/17 15:23 50-32-806/07/17 16:1010.0 2.2 1
Benzo(b)fluoranthene ND ug/L 06/13/17 15:23 205-99-206/07/17 16:1010.0 2.2 1
Benzo(g,h,i)perylene ND ug/L 06/13/17 15:23 191-24-206/07/17 16:1010.0 2.1 1
Benzo(k)fluoranthene ND ug/L 06/13/17 15:23 207-08-906/07/17 16:1010.0 2.0 1
Benzyl alcohol ND ug/L 06/13/17 15:23 100-51-6 L206/07/17 16:1020.0 3.1 1
4-Bromophenylphenyl ether ND ug/L 06/13/17 15:23 101-55-306/07/17 16:1010.0 1.5 1
Butylbenzylphthalate ND ug/L 06/13/17 15:23 85-68-706/07/17 16:1010.0 2.5 1
4-Chloro-3-methylphenol ND ug/L 06/13/17 15:23 59-50-706/07/17 16:1020.0 2.8 1
4-Chloroaniline ND ug/L 06/13/17 15:23 106-47-806/07/17 16:1020.0 2.8 1
Chlorobenzilate ND ug/L 06/13/17 15:23 510-15-606/07/17 16:1010.0 2.2 1
bis(2-Chloroethoxy)methane ND ug/L 06/13/17 15:23 111-91-1 L206/07/17 16:1010.0 1.6 1
bis(2-Chloroethyl) ether ND ug/L 06/13/17 15:23 111-44-4 L206/07/17 16:1010.0 1.7 1
2-Chloronaphthalene ND ug/L 06/13/17 15:23 91-58-7 L206/07/17 16:1010.0 1.6 1
2-Chlorophenol ND ug/L 06/13/17 15:23 95-57-8 L206/07/17 16:1010.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/13/17 15:23 7005-72-306/07/17 16:1010.0 1.6 1
Chrysene ND ug/L 06/13/17 15:23 218-01-906/07/17 16:1010.0 2.1 1
Diallate ND ug/L 06/13/17 15:23 2303-16-406/07/17 16:1010.0 1.6 1
Dibenz(a,h)anthracene ND ug/L 06/13/17 15:23 53-70-306/07/17 16:1010.0 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 43 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-4D Lab ID:92342479005 Collected:05/31/17 13:15 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Dibenzofuran ND ug/L 06/13/17 15:23 132-64-906/07/17 16:1010.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 06/13/17 15:23 91-94-106/07/17 16:1020.0 3.9 1
2,4-Dichlorophenol ND ug/L 06/13/17 15:23 120-83-2 L206/07/17 16:1010.0 1.6 1
2,6-Dichlorophenol ND ug/L 06/13/17 15:23 87-65-0 L206/07/17 16:1010.0 1.5 1
Diethylphthalate ND ug/L 06/13/17 15:23 84-66-206/07/17 16:1060001.6 1
Dimethoate ND ug/L 06/13/17 15:23 60-51-506/07/17 16:1020.0 1.8 1
P-Dimethylaminoazobenzene ND ug/L 06/13/17 15:23 60-11-706/07/17 16:1010.0 1.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/13/17 15:23 57-97-606/07/17 16:1010.0 2.4 1
3,3'-Dimethylbenzidine ND ug/L 06/13/17 15:23 119-93-706/07/17 16:1010.0 3.9 1
2,4-Dimethylphenol ND ug/L 06/13/17 15:23 105-67-9 L206/07/17 16:1010.0 1.6 1
Dimethylphthalate ND ug/L 06/13/17 15:23 131-11-306/07/17 16:1010.0 1.4 1
Di-n-butylphthalate ND ug/L 06/13/17 15:23 84-74-206/07/17 16:1010.0 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/13/17 15:23 534-52-106/07/17 16:1050.0 2.2 1
1,3-Dinitrobenzene ND ug/L 06/13/17 15:23 99-65-006/07/17 16:1020.0 1.3 1
2,4-Dinitrophenol ND ug/L 06/13/17 15:23 51-28-506/07/17 16:1050.0 5.1 1
2,4-Dinitrotoluene ND ug/L 06/13/17 15:23 121-14-206/07/17 16:1010.0 1.5 1
2,6-Dinitrotoluene ND ug/L 06/13/17 15:23 606-20-206/07/17 16:1010.0 1.4 1
Di-n-octylphthalate ND ug/L 06/13/17 15:23 117-84-006/07/17 16:1010.0 1.5 1
Diphenylamine ND ug/L 06/13/17 15:23 122-39-406/07/17 16:1010.0 1.4 1
Disulfoton ND ug/L 06/13/17 15:23 298-04-406/07/17 16:1010.0 1.5 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/13/17 15:23 117-81-706/07/17 16:1015.0 2.3 1
Ethyl methanesulfonate ND ug/L 06/13/17 15:23 62-50-0 L206/07/17 16:1020.0 1.6 1
Famphur ND ug/L 06/13/17 15:23 52-85-706/07/17 16:1020.0 5.7 1
Fluoranthene ND ug/L 06/13/17 15:23 206-44-006/07/17 16:1010.0 2.2 1
Fluorene ND ug/L 06/13/17 15:23 86-73-706/07/17 16:1010.0 1.6 1
Hexachlorobenzene ND ug/L 06/13/17 15:23 118-74-106/07/17 16:1010.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 06/13/17 15:23 77-47-4 L206/07/17 16:1010.0 1.3 1
Hexachloroethane ND ug/L 06/13/17 15:23 67-72-1 L206/07/17 16:1010.0 1.8 1
Hexachloropropene ND ug/L 06/13/17 15:23 1888-71-706/07/17 16:1010.0 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/13/17 15:23 193-39-506/07/17 16:1010.0 2.0 1
Isodrin ND ug/L 06/13/17 15:23 465-73-606/07/17 16:1020.0 2.5 1
Isophorone ND ug/L 06/13/17 15:23 78-59-1 L206/07/17 16:1010.0 1.5 1
Isosafrole ND ug/L 06/13/17 15:23 120-58-1 L206/07/17 16:1010.0 1.5 1
Kepone ND ug/L 06/13/17 15:23 143-50-006/07/17 16:1020.0 4.5 1
Methapyrilene ND ug/L 06/13/17 15:23 91-80-506/07/17 16:101003.0 1
3-Methylcholanthrene ND ug/L 06/13/17 15:23 56-49-506/07/17 16:1010.0 2.7 1
Methyl methanesulfonate ND ug/L 06/13/17 15:23 66-27-306/07/17 16:1010.0 1.1 1
2-Methylnaphthalene ND ug/L 06/13/17 15:23 91-57-6 L206/07/17 16:1010.0 1.4 1
Methyl parathion ND ug/L 06/13/17 15:23 298-00-006/07/17 16:1010.0 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 06/13/17 15:23 95-48-7 L206/07/17 16:1010.0 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/13/17 15:23 15831-10-4 L206/07/17 16:1010.0 1.4 1
1-Naphthalenamine ND ug/L 06/13/17 15:23 134-32-706/07/17 16:1010.0 1.3 1
2-Naphthalenamine ND ug/L 06/13/17 15:23 91-59-806/07/17 16:1010.0 2.2 1
1,4-Naphthoquinone ND ug/L 06/13/17 15:23 130-15-406/07/17 16:1010.0 0.99 1
2-Nitroaniline ND ug/L 06/13/17 15:23 88-74-406/07/17 16:1050.0 2.3 1
3-Nitroaniline ND ug/L 06/13/17 15:23 99-09-206/07/17 16:1050.0 2.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-4D Lab ID:92342479005 Collected:05/31/17 13:15 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Nitroaniline ND ug/L 06/13/17 15:23 100-01-606/07/17 16:1020.0 3.4 1
Nitrobenzene ND ug/L 06/13/17 15:23 98-95-3 L206/07/17 16:1010.0 1.6 1
2-Nitrophenol ND ug/L 06/13/17 15:23 88-75-5 L206/07/17 16:1010.0 1.6 1
4-Nitrophenol ND ug/L 06/13/17 15:23 100-02-706/07/17 16:1050.0 4.3 1
5-Nitro-o-toluidine ND ug/L 06/13/17 15:23 99-55-8 L206/07/17 16:1010.0 1.9 1
N-Nitrosodiethylamine ND ug/L 06/13/17 15:23 55-18-5 L206/07/17 16:1020.0 1.4 1
N-Nitrosodimethylamine ND ug/L 06/13/17 15:23 62-75-906/07/17 16:1010.0 1.6 1
N-Nitroso-di-n-butylamine ND ug/L 06/13/17 15:23 924-16-3 L206/07/17 16:1010.0 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 06/13/17 15:23 621-64-7 L206/07/17 16:1010.0 1.7 1
N-Nitrosodiphenylamine ND ug/L 06/13/17 15:23 86-30-606/07/17 16:1010.0 1.4 1
N-Nitrosomethylethylamine ND ug/L 06/13/17 15:23 10595-95-6 L206/07/17 16:1010.0 1.4 1
N-Nitrosopiperidine ND ug/L 06/13/17 15:23 100-75-4 L206/07/17 16:1020.0 1.7 1
N-Nitrosopyrrolidine ND ug/L 06/13/17 15:23 930-55-2 L206/07/17 16:1010.0 1.7 1
O,O,O-Triethylphosphorothioate ND ug/L 06/13/17 15:23 126-68-1 L206/07/17 16:1010.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/13/17 15:23 108-60-106/07/17 16:1010.0 1.8 1
Parathion (Ethyl parathion)ND ug/L 06/13/17 15:23 56-38-2 L206/07/17 16:1010.0 1.5 1
Pentachlorobenzene ND ug/L 06/13/17 15:23 608-93-506/07/17 16:1010.0 1.5 1
Pentachloronitrobenzene ND ug/L 06/13/17 15:23 82-68-806/07/17 16:1020.0 1.7 1
Pentachlorophenol ND ug/L 06/13/17 15:23 87-86-506/07/17 16:1025.0 3.5 1
Phenacetin ND ug/L 06/13/17 15:23 62-44-206/07/17 16:1020.0 1.9 1
Phenanthrene ND ug/L 06/13/17 15:23 85-01-806/07/17 16:1010.0 1.6 1
Phenol ND ug/L 06/13/17 15:23 108-95-206/07/17 16:1010.0 1.3 1
p-Phenylenediamine ND ug/L 06/13/17 15:23 106-50-3 L206/07/17 16:1010.0 2.2 1
Phorate ND ug/L 06/13/17 15:23 298-02-2 L206/07/17 16:1010.0 1.7 1
Pronamide ND ug/L 06/13/17 15:23 23950-58-5 L206/07/17 16:1010.0 2.0 1
Pyrene ND ug/L 06/13/17 15:23 129-00-006/07/17 16:1010.0 2.2 1
Safrole ND ug/L 06/13/17 15:23 94-59-7 L206/07/17 16:1010.0 1.3 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/13/17 15:23 95-94-306/07/17 16:1010.0 1.3 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/13/17 15:23 58-90-206/07/17 16:1010.0 2.9 1
Thionazin ND ug/L 06/13/17 15:23 297-97-2 L206/07/17 16:1020.0 1.7 1
O-Toluidine ND ug/L 06/13/17 15:23 95-53-4 L206/07/17 16:1010.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 06/13/17 15:23 95-95-406/07/17 16:1010.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/13/17 15:23 88-06-206/07/17 16:1010.0 1.4 1
1,3,5-Trinitrobenzene ND ug/L 06/13/17 15:23 99-35-4 L206/07/17 16:1010.0 1.2 1
Surrogates
Nitrobenzene-d5 (S)74 %06/13/17 15:23 4165-60-0 1g06/07/17 16:1021-110 1
2-Fluorobiphenyl (S)94 %06/13/17 15:23 321-60-806/07/17 16:1027-110 1
Terphenyl-d14 (S)95 %06/13/17 15:23 1718-51-006/07/17 16:1031-107 1
Phenol-d6 (S)39 %06/13/17 15:23 13127-88-306/07/17 16:1010-110 1
2-Fluorophenol (S)43 %06/13/17 15:23 367-12-406/07/17 16:1012-110 1
2,4,6-Tribromophenol (S)85 %06/13/17 15:23 118-79-606/07/17 16:1027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/02/17 03:48 67-64-110010.0 1
Acetonitrile ND ug/L 06/02/17 03:48 75-05-855.0 2.2 1
Acrolein ND ug/L 06/02/17 03:48 107-02-853.0 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-4D Lab ID:92342479005 Collected:05/31/17 13:15 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acrylonitrile ND ug/L 06/02/17 03:48 107-13-12001.9 1
Allyl chloride ND ug/L 06/02/17 03:48 107-05-110.0 1.5 1
Benzene ND ug/L 06/02/17 03:48 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/02/17 03:48 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/02/17 03:48 75-27-41.0 0.18 1
Bromoform ND ug/L 06/02/17 03:48 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/02/17 03:48 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/02/17 03:48 78-93-31000.96 1
Carbon disulfide ND ug/L 06/02/17 03:48 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/02/17 03:48 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/02/17 03:48 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/02/17 03:48 75-00-310.0 0.54 1
Chloroform ND ug/L 06/02/17 03:48 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/02/17 03:48 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/02/17 03:48 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/02/17 03:48 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/02/17 03:48 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/02/17 03:48 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/02/17 03:48 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/02/17 03:48 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/02/17 03:48 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/02/17 03:48 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/02/17 03:48 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/02/17 03:48 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/02/17 03:48 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/02/17 03:48 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/02/17 03:48 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/02/17 03:48 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/02/17 03:48 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/02/17 03:48 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/02/17 03:48 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/02/17 03:48 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/02/17 03:48 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/02/17 03:48 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/02/17 03:48 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/02/17 03:48 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/02/17 03:48 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/02/17 03:48 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/02/17 03:48 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/02/17 03:48 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/02/17 03:48 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/02/17 03:48 126-98-71000.93 1
Methylene Chloride ND ug/L 06/02/17 03:48 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/02/17 03:48 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/02/17 03:48 108-10-11000.33 1
Naphthalene ND ug/L 06/02/17 03:48 91-20-310.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-4D Lab ID:92342479005 Collected:05/31/17 13:15 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Propionitrile ND ug/L 06/02/17 03:48 107-12-01503.6 1
Styrene ND ug/L 06/02/17 03:48 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/02/17 03:48 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/02/17 03:48 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/02/17 03:48 127-18-41.0 0.46 1
Toluene ND ug/L 06/02/17 03:48 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/02/17 03:48 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/02/17 03:48 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/02/17 03:48 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/02/17 03:48 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/02/17 03:48 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/02/17 03:48 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/02/17 03:48 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/02/17 03:48 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/02/17 03:48 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)116 %06/02/17 03:48 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %06/02/17 03:48 17060-07-070-130 1
Toluene-d8 (S)112 %06/02/17 03:48 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/01/17 21:00 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 4.6J ug/L 06/01/17 17:34 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-5 Lab ID:92342479006 Collected:05/31/17 11:00 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/06/17 17:40 309-00-206/02/17 10:090.050 0.050 1
alpha-BHC ND ug/L 06/06/17 17:40 319-84-606/02/17 10:090.050 0.050 1
beta-BHC ND ug/L 06/06/17 17:40 319-85-706/02/17 10:090.050 0.050 1
delta-BHC ND ug/L 06/06/17 17:40 319-86-806/02/17 10:090.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/06/17 17:40 58-89-906/02/17 10:090.050 0.050 1
Chlordane (Technical)ND ug/L 06/06/17 17:40 57-74-906/02/17 10:090.50 0.20 1
4,4'-DDD ND ug/L 06/06/17 17:40 72-54-806/02/17 10:090.10 0.050 1
4,4'-DDE ND ug/L 06/06/17 17:40 72-55-906/02/17 10:090.10 0.050 1
4,4'-DDT ND ug/L 06/06/17 17:40 50-29-306/02/17 10:090.10 0.050 1
Dieldrin ND ug/L 06/06/17 17:40 60-57-106/02/17 10:090.075 0.050 1
Endosulfan I ND ug/L 06/06/17 17:40 959-98-806/02/17 10:090.10 0.050 1
Endosulfan II ND ug/L 06/06/17 17:40 33213-65-906/02/17 10:090.10 0.050 1
Endosulfan sulfate ND ug/L 06/06/17 17:40 1031-07-806/02/17 10:090.10 0.050 1
Endrin ND ug/L 06/06/17 17:40 72-20-806/02/17 10:090.10 0.050 1
Endrin aldehyde ND ug/L 06/06/17 17:40 7421-93-406/02/17 10:090.10 0.050 1
Heptachlor ND ug/L 06/06/17 17:40 76-44-806/02/17 10:090.050 0.050 1
Heptachlor epoxide ND ug/L 06/06/17 17:40 1024-57-306/02/17 10:090.075 0.050 1
Methoxychlor ND ug/L 06/06/17 17:40 72-43-506/02/17 10:091.0 0.15 1
Toxaphene ND ug/L 06/06/17 17:40 8001-35-206/02/17 10:091.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)73 %06/06/17 17:40 877-09-806/02/17 10:0920-130 1
Decachlorobiphenyl (S)75 %06/06/17 17:40 2051-24-306/02/17 10:0920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/02/17 18:08 12674-11-206/02/17 10:090.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/02/17 18:08 11104-28-206/02/17 10:090.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/02/17 18:08 11141-16-506/02/17 10:090.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/02/17 18:08 53469-21-906/02/17 10:090.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/02/17 18:08 12672-29-606/02/17 10:090.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/02/17 18:08 11097-69-106/02/17 10:090.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/02/17 18:08 11096-82-506/02/17 10:090.50 0.50 1
Surrogates
Decachlorobiphenyl (S)69 %06/02/17 18:08 2051-24-306/02/17 10:0910-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/07/17 05:02 94-75-7 L106/05/17 16:500.98 0.23 1
Dinoseb ND ug/L 06/07/17 05:02 88-85-7 L106/05/17 16:500.20 0.060 1
Pentachlorophenol ND ug/L 06/07/17 05:02 87-86-506/05/17 16:500.030 0.018 1
2,4,5-T ND ug/L 06/07/17 05:02 93-76-506/05/17 16:500.20 0.044 1
2,4,5-TP (Silvex)ND ug/L 06/07/17 05:02 93-72-106/05/17 16:500.20 0.051 1
Surrogates
2,4-DCAA (S)98 %06/07/17 05:02 19719-28-906/05/17 16:5039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/09/17 16:11 7440-36-006/02/17 15:206.0 3.9 1
Arsenic ND ug/L 06/09/17 16:11 7440-38-206/02/17 15:2010.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-5 Lab ID:92342479006 Collected:05/31/17 11:00 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Barium 69.6J ug/L 06/09/17 16:11 7440-39-306/02/17 15:201002.5 1
Beryllium ND ug/L 06/09/17 16:11 7440-41-706/02/17 15:201.0 0.50 1
Cadmium 0.69J ug/L 06/09/17 16:11 7440-43-906/02/17 15:201.0 0.50 1
Chromium ND ug/L 06/09/17 16:11 7440-47-306/02/17 15:2010.0 2.5 1
Cobalt ND ug/L 06/09/17 16:11 7440-48-406/02/17 15:2010.0 2.5 1
Copper ND ug/L 06/09/17 16:11 7440-50-806/02/17 15:2010.0 2.5 1
Lead ND ug/L 06/09/17 16:11 7439-92-106/02/17 15:2010.0 2.5 1
Nickel ND ug/L 06/09/17 16:11 7440-02-006/02/17 15:2050.0 2.5 1
Selenium ND ug/L 06/09/17 16:11 7782-49-206/02/17 15:2010.0 5.0 1
Silver ND ug/L 06/09/17 16:11 7440-22-406/02/17 15:2010.0 2.5 1
Tin ND ug/L 06/09/17 16:11 7440-31-506/02/17 15:201002.5 1
Vanadium ND ug/L 06/09/17 16:11 7440-62-206/02/17 15:2025.0 2.5 1
Zinc ND ug/L 06/09/17 16:11 7440-66-606/02/17 15:2010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.10J ug/L 06/06/17 17:04 7440-28-006/01/17 11:305.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 04:16 7439-97-606/06/17 14:590.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/13/17 15:52 83-32-906/07/17 16:1010.0 1.6 1
Acenaphthylene ND ug/L 06/13/17 15:52 208-96-806/07/17 16:1010.0 1.5 1
Acetophenone ND ug/L 06/13/17 15:52 98-86-206/07/17 16:1010.0 1.9 1
2-Acetylaminofluorene ND ug/L 06/13/17 15:52 53-96-3 L206/07/17 16:1020.0 1.6 1
4-Aminobiphenyl ND ug/L 06/13/17 15:52 92-67-106/07/17 16:1020.0 1.7 1
Anthracene ND ug/L 06/13/17 15:52 120-12-706/07/17 16:1010.0 1.7 1
Benzo(a)anthracene ND ug/L 06/13/17 15:52 56-55-306/07/17 16:1010.0 2.1 1
Benzo(a)pyrene ND ug/L 06/13/17 15:52 50-32-806/07/17 16:1010.0 2.2 1
Benzo(b)fluoranthene ND ug/L 06/13/17 15:52 205-99-206/07/17 16:1010.0 2.2 1
Benzo(g,h,i)perylene ND ug/L 06/13/17 15:52 191-24-206/07/17 16:1010.0 2.1 1
Benzo(k)fluoranthene ND ug/L 06/13/17 15:52 207-08-906/07/17 16:1010.0 2.0 1
Benzyl alcohol ND ug/L 06/13/17 15:52 100-51-6 L206/07/17 16:1020.0 3.1 1
4-Bromophenylphenyl ether ND ug/L 06/13/17 15:52 101-55-306/07/17 16:1010.0 1.5 1
Butylbenzylphthalate ND ug/L 06/13/17 15:52 85-68-706/07/17 16:1010.0 2.5 1
4-Chloro-3-methylphenol ND ug/L 06/13/17 15:52 59-50-706/07/17 16:1020.0 2.8 1
4-Chloroaniline ND ug/L 06/13/17 15:52 106-47-806/07/17 16:1020.0 2.8 1
Chlorobenzilate ND ug/L 06/13/17 15:52 510-15-606/07/17 16:1010.0 2.2 1
bis(2-Chloroethoxy)methane ND ug/L 06/13/17 15:52 111-91-1 L206/07/17 16:1010.0 1.6 1
bis(2-Chloroethyl) ether ND ug/L 06/13/17 15:52 111-44-4 L206/07/17 16:1010.0 1.7 1
2-Chloronaphthalene ND ug/L 06/13/17 15:52 91-58-7 L206/07/17 16:1010.0 1.6 1
2-Chlorophenol ND ug/L 06/13/17 15:52 95-57-8 L206/07/17 16:1010.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/13/17 15:52 7005-72-306/07/17 16:1010.0 1.6 1
Chrysene ND ug/L 06/13/17 15:52 218-01-906/07/17 16:1010.0 2.1 1
Diallate ND ug/L 06/13/17 15:52 2303-16-406/07/17 16:1010.0 1.6 1
Dibenz(a,h)anthracene ND ug/L 06/13/17 15:52 53-70-306/07/17 16:1010.0 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-5 Lab ID:92342479006 Collected:05/31/17 11:00 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Dibenzofuran ND ug/L 06/13/17 15:52 132-64-906/07/17 16:1010.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 06/13/17 15:52 91-94-106/07/17 16:1020.0 3.9 1
2,4-Dichlorophenol ND ug/L 06/13/17 15:52 120-83-2 L206/07/17 16:1010.0 1.6 1
2,6-Dichlorophenol ND ug/L 06/13/17 15:52 87-65-0 L206/07/17 16:1010.0 1.5 1
Diethylphthalate ND ug/L 06/13/17 15:52 84-66-206/07/17 16:1060001.6 1
Dimethoate ND ug/L 06/13/17 15:52 60-51-506/07/17 16:1020.0 1.8 1
P-Dimethylaminoazobenzene ND ug/L 06/13/17 15:52 60-11-706/07/17 16:1010.0 1.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/13/17 15:52 57-97-606/07/17 16:1010.0 2.4 1
3,3'-Dimethylbenzidine ND ug/L 06/13/17 15:52 119-93-706/07/17 16:1010.0 3.9 1
2,4-Dimethylphenol ND ug/L 06/13/17 15:52 105-67-9 L206/07/17 16:1010.0 1.6 1
Dimethylphthalate ND ug/L 06/13/17 15:52 131-11-306/07/17 16:1010.0 1.4 1
Di-n-butylphthalate ND ug/L 06/13/17 15:52 84-74-206/07/17 16:1010.0 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/13/17 15:52 534-52-106/07/17 16:1050.0 2.2 1
1,3-Dinitrobenzene ND ug/L 06/13/17 15:52 99-65-006/07/17 16:1020.0 1.3 1
2,4-Dinitrophenol ND ug/L 06/13/17 15:52 51-28-506/07/17 16:1050.0 5.1 1
2,4-Dinitrotoluene ND ug/L 06/13/17 15:52 121-14-206/07/17 16:1010.0 1.5 1
2,6-Dinitrotoluene ND ug/L 06/13/17 15:52 606-20-206/07/17 16:1010.0 1.4 1
Di-n-octylphthalate ND ug/L 06/13/17 15:52 117-84-006/07/17 16:1010.0 1.5 1
Diphenylamine ND ug/L 06/13/17 15:52 122-39-406/07/17 16:1010.0 1.4 1
Disulfoton ND ug/L 06/13/17 15:52 298-04-406/07/17 16:1010.0 1.5 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/13/17 15:52 117-81-706/07/17 16:1015.0 2.3 1
Ethyl methanesulfonate ND ug/L 06/13/17 15:52 62-50-0 L206/07/17 16:1020.0 1.6 1
Famphur ND ug/L 06/13/17 15:52 52-85-706/07/17 16:1020.0 5.7 1
Fluoranthene ND ug/L 06/13/17 15:52 206-44-006/07/17 16:1010.0 2.2 1
Fluorene ND ug/L 06/13/17 15:52 86-73-706/07/17 16:1010.0 1.6 1
Hexachlorobenzene ND ug/L 06/13/17 15:52 118-74-106/07/17 16:1010.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 06/13/17 15:52 77-47-4 L206/07/17 16:1010.0 1.3 1
Hexachloroethane ND ug/L 06/13/17 15:52 67-72-1 L206/07/17 16:1010.0 1.8 1
Hexachloropropene ND ug/L 06/13/17 15:52 1888-71-706/07/17 16:1010.0 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/13/17 15:52 193-39-506/07/17 16:1010.0 2.0 1
Isodrin ND ug/L 06/13/17 15:52 465-73-606/07/17 16:1020.0 2.5 1
Isophorone ND ug/L 06/13/17 15:52 78-59-1 L206/07/17 16:1010.0 1.5 1
Isosafrole ND ug/L 06/13/17 15:52 120-58-1 L206/07/17 16:1010.0 1.5 1
Kepone ND ug/L 06/13/17 15:52 143-50-006/07/17 16:1020.0 4.5 1
Methapyrilene ND ug/L 06/13/17 15:52 91-80-506/07/17 16:101003.0 1
3-Methylcholanthrene ND ug/L 06/13/17 15:52 56-49-506/07/17 16:1010.0 2.7 1
Methyl methanesulfonate ND ug/L 06/13/17 15:52 66-27-306/07/17 16:1010.0 1.1 1
2-Methylnaphthalene ND ug/L 06/13/17 15:52 91-57-6 L206/07/17 16:1010.0 1.4 1
Methyl parathion ND ug/L 06/13/17 15:52 298-00-006/07/17 16:1010.0 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 06/13/17 15:52 95-48-7 L206/07/17 16:1010.0 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/13/17 15:52 15831-10-4 L206/07/17 16:1010.0 1.4 1
1-Naphthalenamine ND ug/L 06/13/17 15:52 134-32-706/07/17 16:1010.0 1.3 1
2-Naphthalenamine ND ug/L 06/13/17 15:52 91-59-806/07/17 16:1010.0 2.2 1
1,4-Naphthoquinone ND ug/L 06/13/17 15:52 130-15-406/07/17 16:1010.0 0.99 1
2-Nitroaniline ND ug/L 06/13/17 15:52 88-74-406/07/17 16:1050.0 2.3 1
3-Nitroaniline ND ug/L 06/13/17 15:52 99-09-206/07/17 16:1050.0 2.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-5 Lab ID:92342479006 Collected:05/31/17 11:00 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Nitroaniline ND ug/L 06/13/17 15:52 100-01-606/07/17 16:1020.0 3.4 1
Nitrobenzene ND ug/L 06/13/17 15:52 98-95-3 L206/07/17 16:1010.0 1.6 1
2-Nitrophenol ND ug/L 06/13/17 15:52 88-75-5 L206/07/17 16:1010.0 1.6 1
4-Nitrophenol ND ug/L 06/13/17 15:52 100-02-706/07/17 16:1050.0 4.3 1
5-Nitro-o-toluidine ND ug/L 06/13/17 15:52 99-55-8 L206/07/17 16:1010.0 1.9 1
N-Nitrosodiethylamine ND ug/L 06/13/17 15:52 55-18-5 L206/07/17 16:1020.0 1.4 1
N-Nitrosodimethylamine ND ug/L 06/13/17 15:52 62-75-906/07/17 16:1010.0 1.6 1
N-Nitroso-di-n-butylamine ND ug/L 06/13/17 15:52 924-16-3 L206/07/17 16:1010.0 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 06/13/17 15:52 621-64-7 L206/07/17 16:1010.0 1.7 1
N-Nitrosodiphenylamine ND ug/L 06/13/17 15:52 86-30-606/07/17 16:1010.0 1.4 1
N-Nitrosomethylethylamine ND ug/L 06/13/17 15:52 10595-95-6 L206/07/17 16:1010.0 1.4 1
N-Nitrosopiperidine ND ug/L 06/13/17 15:52 100-75-4 L206/07/17 16:1020.0 1.7 1
N-Nitrosopyrrolidine ND ug/L 06/13/17 15:52 930-55-2 L206/07/17 16:1010.0 1.7 1
O,O,O-Triethylphosphorothioate ND ug/L 06/13/17 15:52 126-68-1 L206/07/17 16:1010.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/13/17 15:52 108-60-106/07/17 16:1010.0 1.8 1
Parathion (Ethyl parathion)ND ug/L 06/13/17 15:52 56-38-2 L206/07/17 16:1010.0 1.5 1
Pentachlorobenzene ND ug/L 06/13/17 15:52 608-93-506/07/17 16:1010.0 1.5 1
Pentachloronitrobenzene ND ug/L 06/13/17 15:52 82-68-806/07/17 16:1020.0 1.7 1
Pentachlorophenol ND ug/L 06/13/17 15:52 87-86-506/07/17 16:1025.0 3.5 1
Phenacetin ND ug/L 06/13/17 15:52 62-44-206/07/17 16:1020.0 1.9 1
Phenanthrene ND ug/L 06/13/17 15:52 85-01-806/07/17 16:1010.0 1.6 1
Phenol ND ug/L 06/13/17 15:52 108-95-206/07/17 16:1010.0 1.3 1
p-Phenylenediamine ND ug/L 06/13/17 15:52 106-50-3 L206/07/17 16:1010.0 2.2 1
Phorate ND ug/L 06/13/17 15:52 298-02-2 L206/07/17 16:1010.0 1.7 1
Pronamide ND ug/L 06/13/17 15:52 23950-58-5 L206/07/17 16:1010.0 2.0 1
Pyrene ND ug/L 06/13/17 15:52 129-00-006/07/17 16:1010.0 2.2 1
Safrole ND ug/L 06/13/17 15:52 94-59-7 L206/07/17 16:1010.0 1.3 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/13/17 15:52 95-94-306/07/17 16:1010.0 1.3 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/13/17 15:52 58-90-206/07/17 16:1010.0 2.9 1
Thionazin ND ug/L 06/13/17 15:52 297-97-2 L206/07/17 16:1020.0 1.7 1
O-Toluidine ND ug/L 06/13/17 15:52 95-53-4 L206/07/17 16:1010.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 06/13/17 15:52 95-95-406/07/17 16:1010.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/13/17 15:52 88-06-206/07/17 16:1010.0 1.4 1
1,3,5-Trinitrobenzene ND ug/L 06/13/17 15:52 99-35-4 L206/07/17 16:1010.0 1.2 1
Surrogates
Nitrobenzene-d5 (S)84 %06/13/17 15:52 4165-60-0 1g06/07/17 16:1021-110 1
2-Fluorobiphenyl (S)103 %06/13/17 15:52 321-60-806/07/17 16:1027-110 1
Terphenyl-d14 (S)97 %06/13/17 15:52 1718-51-006/07/17 16:1031-107 1
Phenol-d6 (S)27 %06/13/17 15:52 13127-88-306/07/17 16:1010-110 1
2-Fluorophenol (S)44 %06/13/17 15:52 367-12-406/07/17 16:1012-110 1
2,4,6-Tribromophenol (S)90 %06/13/17 15:52 118-79-606/07/17 16:1027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 13.5J ug/L 06/02/17 04:06 67-64-110010.0 1
Acetonitrile ND ug/L 06/02/17 04:06 75-05-855.0 2.2 1
Acrolein ND ug/L 06/02/17 04:06 107-02-853.0 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-5 Lab ID:92342479006 Collected:05/31/17 11:00 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acrylonitrile ND ug/L 06/02/17 04:06 107-13-12001.9 1
Allyl chloride ND ug/L 06/02/17 04:06 107-05-110.0 1.5 1
Benzene ND ug/L 06/02/17 04:06 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/02/17 04:06 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/02/17 04:06 75-27-41.0 0.18 1
Bromoform ND ug/L 06/02/17 04:06 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/02/17 04:06 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/02/17 04:06 78-93-31000.96 1
Carbon disulfide ND ug/L 06/02/17 04:06 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/02/17 04:06 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/02/17 04:06 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/02/17 04:06 75-00-310.0 0.54 1
Chloroform ND ug/L 06/02/17 04:06 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/02/17 04:06 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/02/17 04:06 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/02/17 04:06 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/02/17 04:06 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/02/17 04:06 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/02/17 04:06 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/02/17 04:06 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/02/17 04:06 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/02/17 04:06 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/02/17 04:06 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/02/17 04:06 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/02/17 04:06 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/02/17 04:06 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/02/17 04:06 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.51J ug/L 06/02/17 04:06 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/02/17 04:06 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/02/17 04:06 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/02/17 04:06 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/02/17 04:06 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/02/17 04:06 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/02/17 04:06 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/02/17 04:06 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/02/17 04:06 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/02/17 04:06 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/02/17 04:06 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/02/17 04:06 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/02/17 04:06 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/02/17 04:06 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/02/17 04:06 126-98-71000.93 1
Methylene Chloride ND ug/L 06/02/17 04:06 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/02/17 04:06 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/02/17 04:06 108-10-11000.33 1
Naphthalene ND ug/L 06/02/17 04:06 91-20-310.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
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Page 52 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-5 Lab ID:92342479006 Collected:05/31/17 11:00 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Propionitrile ND ug/L 06/02/17 04:06 107-12-01503.6 1
Styrene ND ug/L 06/02/17 04:06 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/02/17 04:06 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/02/17 04:06 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/02/17 04:06 127-18-41.0 0.46 1
Toluene ND ug/L 06/02/17 04:06 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/02/17 04:06 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/02/17 04:06 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/02/17 04:06 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/02/17 04:06 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/02/17 04:06 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/02/17 04:06 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/02/17 04:06 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/02/17 04:06 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/02/17 04:06 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)118 %06/02/17 04:06 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %06/02/17 04:06 17060-07-070-130 1
Toluene-d8 (S)112 %06/02/17 04:06 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/01/17 21:00 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 4.8J ug/L 06/01/17 17:35 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-6R Lab ID:92342479007 Collected:05/31/17 10:40 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/06/17 17:58 309-00-206/02/17 10:090.050 0.050 1
alpha-BHC ND ug/L 06/06/17 17:58 319-84-606/02/17 10:090.050 0.050 1
beta-BHC ND ug/L 06/06/17 17:58 319-85-706/02/17 10:090.050 0.050 1
delta-BHC ND ug/L 06/06/17 17:58 319-86-806/02/17 10:090.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/06/17 17:58 58-89-906/02/17 10:090.050 0.050 1
Chlordane (Technical)ND ug/L 06/06/17 17:58 57-74-906/02/17 10:090.50 0.20 1
4,4'-DDD ND ug/L 06/06/17 17:58 72-54-806/02/17 10:090.10 0.050 1
4,4'-DDE ND ug/L 06/06/17 17:58 72-55-906/02/17 10:090.10 0.050 1
4,4'-DDT ND ug/L 06/06/17 17:58 50-29-306/02/17 10:090.10 0.050 1
Dieldrin ND ug/L 06/06/17 17:58 60-57-106/02/17 10:090.075 0.050 1
Endosulfan I ND ug/L 06/06/17 17:58 959-98-806/02/17 10:090.10 0.050 1
Endosulfan II ND ug/L 06/06/17 17:58 33213-65-906/02/17 10:090.10 0.050 1
Endosulfan sulfate ND ug/L 06/06/17 17:58 1031-07-806/02/17 10:090.10 0.050 1
Endrin ND ug/L 06/06/17 17:58 72-20-806/02/17 10:090.10 0.050 1
Endrin aldehyde ND ug/L 06/06/17 17:58 7421-93-406/02/17 10:090.10 0.050 1
Heptachlor ND ug/L 06/06/17 17:58 76-44-806/02/17 10:090.050 0.050 1
Heptachlor epoxide ND ug/L 06/06/17 17:58 1024-57-306/02/17 10:090.075 0.050 1
Methoxychlor ND ug/L 06/06/17 17:58 72-43-506/02/17 10:091.0 0.15 1
Toxaphene ND ug/L 06/06/17 17:58 8001-35-206/02/17 10:091.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)96 %06/06/17 17:58 877-09-806/02/17 10:0920-130 1
Decachlorobiphenyl (S)62 %06/06/17 17:58 2051-24-306/02/17 10:0920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/02/17 18:29 12674-11-206/02/17 10:090.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/02/17 18:29 11104-28-206/02/17 10:090.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/02/17 18:29 11141-16-506/02/17 10:090.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/02/17 18:29 53469-21-906/02/17 10:090.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/02/17 18:29 12672-29-606/02/17 10:090.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/02/17 18:29 11097-69-106/02/17 10:090.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/02/17 18:29 11096-82-506/02/17 10:090.50 0.50 1
Surrogates
Decachlorobiphenyl (S)61 %06/02/17 18:29 2051-24-306/02/17 10:0910-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/07/17 05:31 94-75-7 L106/05/17 16:501.0 0.25 1
Dinoseb ND ug/L 06/07/17 05:31 88-85-7 L106/05/17 16:500.21 0.063 1
Pentachlorophenol ND ug/L 06/07/17 05:31 87-86-506/05/17 16:500.032 0.019 1
2,4,5-T ND ug/L 06/07/17 05:31 93-76-506/05/17 16:500.21 0.047 1
2,4,5-TP (Silvex)ND ug/L 06/07/17 05:31 93-72-106/05/17 16:500.21 0.054 1
Surrogates
2,4-DCAA (S)96 %06/07/17 05:31 19719-28-906/05/17 16:5039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/09/17 16:14 7440-36-006/02/17 15:206.0 3.9 1
Arsenic ND ug/L 06/09/17 16:14 7440-38-206/02/17 15:2010.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-6R Lab ID:92342479007 Collected:05/31/17 10:40 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Barium 58.9J ug/L 06/09/17 16:14 7440-39-306/02/17 15:201002.5 1
Beryllium ND ug/L 06/09/17 16:14 7440-41-706/02/17 15:201.0 0.50 1
Cadmium ND ug/L 06/09/17 16:14 7440-43-906/02/17 15:201.0 0.50 1
Chromium ND ug/L 06/09/17 16:14 7440-47-306/02/17 15:2010.0 2.5 1
Cobalt ND ug/L 06/09/17 16:14 7440-48-406/02/17 15:2010.0 2.5 1
Copper ND ug/L 06/09/17 16:14 7440-50-806/02/17 15:2010.0 2.5 1
Lead ND ug/L 06/09/17 16:14 7439-92-106/02/17 15:2010.0 2.5 1
Nickel ND ug/L 06/09/17 16:14 7440-02-006/02/17 15:2050.0 2.5 1
Selenium ND ug/L 06/09/17 16:14 7782-49-206/02/17 15:2010.0 5.0 1
Silver ND ug/L 06/09/17 16:14 7440-22-406/02/17 15:2010.0 2.5 1
Tin ND ug/L 06/09/17 16:14 7440-31-506/02/17 15:201002.5 1
Vanadium ND ug/L 06/09/17 16:14 7440-62-206/02/17 15:2025.0 2.5 1
Zinc ND ug/L 06/09/17 16:14 7440-66-606/02/17 15:2010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.078J ug/L 06/06/17 17:06 7440-28-006/01/17 11:305.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 04:18 7439-97-606/06/17 14:590.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/13/17 16:21 83-32-906/07/17 16:1010.0 1.6 1
Acenaphthylene ND ug/L 06/13/17 16:21 208-96-806/07/17 16:1010.0 1.5 1
Acetophenone ND ug/L 06/13/17 16:21 98-86-206/07/17 16:1010.0 1.9 1
2-Acetylaminofluorene ND ug/L 06/13/17 16:21 53-96-3 L206/07/17 16:1020.0 1.6 1
4-Aminobiphenyl ND ug/L 06/13/17 16:21 92-67-106/07/17 16:1020.0 1.7 1
Anthracene ND ug/L 06/13/17 16:21 120-12-706/07/17 16:1010.0 1.7 1
Benzo(a)anthracene ND ug/L 06/13/17 16:21 56-55-306/07/17 16:1010.0 2.1 1
Benzo(a)pyrene ND ug/L 06/13/17 16:21 50-32-806/07/17 16:1010.0 2.2 1
Benzo(b)fluoranthene ND ug/L 06/13/17 16:21 205-99-206/07/17 16:1010.0 2.2 1
Benzo(g,h,i)perylene ND ug/L 06/13/17 16:21 191-24-206/07/17 16:1010.0 2.1 1
Benzo(k)fluoranthene ND ug/L 06/13/17 16:21 207-08-906/07/17 16:1010.0 2.0 1
Benzyl alcohol ND ug/L 06/13/17 16:21 100-51-6 L206/07/17 16:1020.0 3.1 1
4-Bromophenylphenyl ether ND ug/L 06/13/17 16:21 101-55-306/07/17 16:1010.0 1.5 1
Butylbenzylphthalate ND ug/L 06/13/17 16:21 85-68-706/07/17 16:1010.0 2.5 1
4-Chloro-3-methylphenol ND ug/L 06/13/17 16:21 59-50-706/07/17 16:1020.0 2.8 1
4-Chloroaniline ND ug/L 06/13/17 16:21 106-47-806/07/17 16:1020.0 2.8 1
Chlorobenzilate ND ug/L 06/13/17 16:21 510-15-606/07/17 16:1010.0 2.2 1
bis(2-Chloroethoxy)methane ND ug/L 06/13/17 16:21 111-91-1 L206/07/17 16:1010.0 1.6 1
bis(2-Chloroethyl) ether ND ug/L 06/13/17 16:21 111-44-4 L206/07/17 16:1010.0 1.7 1
2-Chloronaphthalene ND ug/L 06/13/17 16:21 91-58-7 L206/07/17 16:1010.0 1.6 1
2-Chlorophenol ND ug/L 06/13/17 16:21 95-57-8 L206/07/17 16:1010.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/13/17 16:21 7005-72-306/07/17 16:1010.0 1.6 1
Chrysene ND ug/L 06/13/17 16:21 218-01-906/07/17 16:1010.0 2.1 1
Diallate ND ug/L 06/13/17 16:21 2303-16-406/07/17 16:1010.0 1.6 1
Dibenz(a,h)anthracene ND ug/L 06/13/17 16:21 53-70-306/07/17 16:1010.0 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-6R Lab ID:92342479007 Collected:05/31/17 10:40 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Dibenzofuran ND ug/L 06/13/17 16:21 132-64-906/07/17 16:1010.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 06/13/17 16:21 91-94-106/07/17 16:1020.0 3.9 1
2,4-Dichlorophenol ND ug/L 06/13/17 16:21 120-83-2 L206/07/17 16:1010.0 1.6 1
2,6-Dichlorophenol ND ug/L 06/13/17 16:21 87-65-0 L206/07/17 16:1010.0 1.5 1
Diethylphthalate ND ug/L 06/13/17 16:21 84-66-206/07/17 16:1060001.6 1
Dimethoate ND ug/L 06/13/17 16:21 60-51-506/07/17 16:1020.0 1.8 1
P-Dimethylaminoazobenzene ND ug/L 06/13/17 16:21 60-11-706/07/17 16:1010.0 1.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/13/17 16:21 57-97-606/07/17 16:1010.0 2.4 1
3,3'-Dimethylbenzidine ND ug/L 06/13/17 16:21 119-93-706/07/17 16:1010.0 3.9 1
2,4-Dimethylphenol ND ug/L 06/13/17 16:21 105-67-9 L206/07/17 16:1010.0 1.6 1
Dimethylphthalate ND ug/L 06/13/17 16:21 131-11-306/07/17 16:1010.0 1.4 1
Di-n-butylphthalate ND ug/L 06/13/17 16:21 84-74-206/07/17 16:1010.0 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/13/17 16:21 534-52-106/07/17 16:1050.0 2.2 1
1,3-Dinitrobenzene ND ug/L 06/13/17 16:21 99-65-006/07/17 16:1020.0 1.3 1
2,4-Dinitrophenol ND ug/L 06/13/17 16:21 51-28-506/07/17 16:1050.0 5.1 1
2,4-Dinitrotoluene ND ug/L 06/13/17 16:21 121-14-206/07/17 16:1010.0 1.5 1
2,6-Dinitrotoluene ND ug/L 06/13/17 16:21 606-20-206/07/17 16:1010.0 1.4 1
Di-n-octylphthalate ND ug/L 06/13/17 16:21 117-84-006/07/17 16:1010.0 1.5 1
Diphenylamine ND ug/L 06/13/17 16:21 122-39-406/07/17 16:1010.0 1.4 1
Disulfoton ND ug/L 06/13/17 16:21 298-04-406/07/17 16:1010.0 1.5 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/13/17 16:21 117-81-706/07/17 16:1015.0 2.3 1
Ethyl methanesulfonate ND ug/L 06/13/17 16:21 62-50-0 L206/07/17 16:1020.0 1.6 1
Famphur ND ug/L 06/13/17 16:21 52-85-706/07/17 16:1020.0 5.7 1
Fluoranthene ND ug/L 06/13/17 16:21 206-44-006/07/17 16:1010.0 2.2 1
Fluorene ND ug/L 06/13/17 16:21 86-73-706/07/17 16:1010.0 1.6 1
Hexachlorobenzene ND ug/L 06/13/17 16:21 118-74-106/07/17 16:1010.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 06/13/17 16:21 77-47-4 L206/07/17 16:1010.0 1.3 1
Hexachloroethane ND ug/L 06/13/17 16:21 67-72-1 L206/07/17 16:1010.0 1.8 1
Hexachloropropene ND ug/L 06/13/17 16:21 1888-71-706/07/17 16:1010.0 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/13/17 16:21 193-39-506/07/17 16:1010.0 2.0 1
Isodrin ND ug/L 06/13/17 16:21 465-73-606/07/17 16:1020.0 2.5 1
Isophorone ND ug/L 06/13/17 16:21 78-59-1 L206/07/17 16:1010.0 1.5 1
Isosafrole ND ug/L 06/13/17 16:21 120-58-1 L206/07/17 16:1010.0 1.5 1
Kepone ND ug/L 06/13/17 16:21 143-50-006/07/17 16:1020.0 4.5 1
Methapyrilene ND ug/L 06/13/17 16:21 91-80-506/07/17 16:101003.0 1
3-Methylcholanthrene ND ug/L 06/13/17 16:21 56-49-506/07/17 16:1010.0 2.7 1
Methyl methanesulfonate ND ug/L 06/13/17 16:21 66-27-306/07/17 16:1010.0 1.1 1
2-Methylnaphthalene ND ug/L 06/13/17 16:21 91-57-6 L206/07/17 16:1010.0 1.4 1
Methyl parathion ND ug/L 06/13/17 16:21 298-00-006/07/17 16:1010.0 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 06/13/17 16:21 95-48-7 L206/07/17 16:1010.0 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/13/17 16:21 15831-10-4 L206/07/17 16:1010.0 1.4 1
1-Naphthalenamine ND ug/L 06/13/17 16:21 134-32-706/07/17 16:1010.0 1.3 1
2-Naphthalenamine ND ug/L 06/13/17 16:21 91-59-806/07/17 16:1010.0 2.2 1
1,4-Naphthoquinone ND ug/L 06/13/17 16:21 130-15-406/07/17 16:1010.0 0.99 1
2-Nitroaniline ND ug/L 06/13/17 16:21 88-74-406/07/17 16:1050.0 2.3 1
3-Nitroaniline ND ug/L 06/13/17 16:21 99-09-206/07/17 16:1050.0 2.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-6R Lab ID:92342479007 Collected:05/31/17 10:40 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Nitroaniline ND ug/L 06/13/17 16:21 100-01-606/07/17 16:1020.0 3.4 1
Nitrobenzene ND ug/L 06/13/17 16:21 98-95-3 L206/07/17 16:1010.0 1.6 1
2-Nitrophenol ND ug/L 06/13/17 16:21 88-75-5 L206/07/17 16:1010.0 1.6 1
4-Nitrophenol ND ug/L 06/13/17 16:21 100-02-706/07/17 16:1050.0 4.3 1
5-Nitro-o-toluidine ND ug/L 06/13/17 16:21 99-55-8 L206/07/17 16:1010.0 1.9 1
N-Nitrosodiethylamine ND ug/L 06/13/17 16:21 55-18-5 L206/07/17 16:1020.0 1.4 1
N-Nitrosodimethylamine ND ug/L 06/13/17 16:21 62-75-906/07/17 16:1010.0 1.6 1
N-Nitroso-di-n-butylamine ND ug/L 06/13/17 16:21 924-16-3 L206/07/17 16:1010.0 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 06/13/17 16:21 621-64-7 L206/07/17 16:1010.0 1.7 1
N-Nitrosodiphenylamine ND ug/L 06/13/17 16:21 86-30-606/07/17 16:1010.0 1.4 1
N-Nitrosomethylethylamine ND ug/L 06/13/17 16:21 10595-95-6 L206/07/17 16:1010.0 1.4 1
N-Nitrosopiperidine ND ug/L 06/13/17 16:21 100-75-4 L206/07/17 16:1020.0 1.7 1
N-Nitrosopyrrolidine ND ug/L 06/13/17 16:21 930-55-2 L206/07/17 16:1010.0 1.7 1
O,O,O-Triethylphosphorothioate ND ug/L 06/13/17 16:21 126-68-1 L206/07/17 16:1010.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/13/17 16:21 108-60-106/07/17 16:1010.0 1.8 1
Parathion (Ethyl parathion)ND ug/L 06/13/17 16:21 56-38-2 L206/07/17 16:1010.0 1.5 1
Pentachlorobenzene ND ug/L 06/13/17 16:21 608-93-506/07/17 16:1010.0 1.5 1
Pentachloronitrobenzene ND ug/L 06/13/17 16:21 82-68-806/07/17 16:1020.0 1.7 1
Pentachlorophenol ND ug/L 06/13/17 16:21 87-86-506/07/17 16:1025.0 3.5 1
Phenacetin ND ug/L 06/13/17 16:21 62-44-206/07/17 16:1020.0 1.9 1
Phenanthrene ND ug/L 06/13/17 16:21 85-01-806/07/17 16:1010.0 1.6 1
Phenol ND ug/L 06/13/17 16:21 108-95-206/07/17 16:1010.0 1.3 1
p-Phenylenediamine ND ug/L 06/13/17 16:21 106-50-3 L206/07/17 16:1010.0 2.2 1
Phorate ND ug/L 06/13/17 16:21 298-02-2 L206/07/17 16:1010.0 1.7 1
Pronamide ND ug/L 06/13/17 16:21 23950-58-5 L206/07/17 16:1010.0 2.0 1
Pyrene ND ug/L 06/13/17 16:21 129-00-006/07/17 16:1010.0 2.2 1
Safrole ND ug/L 06/13/17 16:21 94-59-7 L206/07/17 16:1010.0 1.3 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/13/17 16:21 95-94-306/07/17 16:1010.0 1.3 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/13/17 16:21 58-90-206/07/17 16:1010.0 2.9 1
Thionazin ND ug/L 06/13/17 16:21 297-97-2 L206/07/17 16:1020.0 1.7 1
O-Toluidine ND ug/L 06/13/17 16:21 95-53-4 L206/07/17 16:1010.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 06/13/17 16:21 95-95-406/07/17 16:1010.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/13/17 16:21 88-06-206/07/17 16:1010.0 1.4 1
1,3,5-Trinitrobenzene ND ug/L 06/13/17 16:21 99-35-4 L206/07/17 16:1010.0 1.2 1
Surrogates
Nitrobenzene-d5 (S)72 %06/13/17 16:21 4165-60-0 1g06/07/17 16:1021-110 1
2-Fluorobiphenyl (S)90 %06/13/17 16:21 321-60-806/07/17 16:1027-110 1
Terphenyl-d14 (S)98 %06/13/17 16:21 1718-51-006/07/17 16:1031-107 1
Phenol-d6 (S)28 %06/13/17 16:21 13127-88-306/07/17 16:1010-110 1
2-Fluorophenol (S)44 %06/13/17 16:21 367-12-406/07/17 16:1012-110 1
2,4,6-Tribromophenol (S)89 %06/13/17 16:21 118-79-606/07/17 16:1027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/02/17 04:23 67-64-110010.0 1
Acetonitrile ND ug/L 06/02/17 04:23 75-05-855.0 2.2 1
Acrolein ND ug/L 06/02/17 04:23 107-02-853.0 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
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Page 57 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-6R Lab ID:92342479007 Collected:05/31/17 10:40 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acrylonitrile ND ug/L 06/02/17 04:23 107-13-12001.9 1
Allyl chloride ND ug/L 06/02/17 04:23 107-05-110.0 1.5 1
Benzene 0.50J ug/L 06/02/17 04:23 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/02/17 04:23 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/02/17 04:23 75-27-41.0 0.18 1
Bromoform ND ug/L 06/02/17 04:23 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/02/17 04:23 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/02/17 04:23 78-93-31000.96 1
Carbon disulfide ND ug/L 06/02/17 04:23 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/02/17 04:23 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/02/17 04:23 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/02/17 04:23 75-00-310.0 0.54 1
Chloroform ND ug/L 06/02/17 04:23 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/02/17 04:23 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/02/17 04:23 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/02/17 04:23 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/02/17 04:23 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/02/17 04:23 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/02/17 04:23 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/02/17 04:23 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/02/17 04:23 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/02/17 04:23 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/02/17 04:23 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/02/17 04:23 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/02/17 04:23 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/02/17 04:23 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/02/17 04:23 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 4.2J ug/L 06/02/17 04:23 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/02/17 04:23 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/02/17 04:23 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/02/17 04:23 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/02/17 04:23 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/02/17 04:23 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/02/17 04:23 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/02/17 04:23 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/02/17 04:23 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/02/17 04:23 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/02/17 04:23 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/02/17 04:23 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/02/17 04:23 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/02/17 04:23 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/02/17 04:23 126-98-71000.93 1
Methylene Chloride ND ug/L 06/02/17 04:23 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/02/17 04:23 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/02/17 04:23 108-10-11000.33 1
Naphthalene ND ug/L 06/02/17 04:23 91-20-310.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-6R Lab ID:92342479007 Collected:05/31/17 10:40 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Propionitrile ND ug/L 06/02/17 04:23 107-12-01503.6 1
Styrene ND ug/L 06/02/17 04:23 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/02/17 04:23 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/02/17 04:23 79-34-53.0 0.40 1
Tetrachloroethene 0.57J ug/L 06/02/17 04:23 127-18-41.0 0.46 1
Toluene ND ug/L 06/02/17 04:23 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/02/17 04:23 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/02/17 04:23 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/02/17 04:23 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/02/17 04:23 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/02/17 04:23 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/02/17 04:23 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/02/17 04:23 108-05-450.0 0.35 1
Vinyl chloride 1.3 ug/L 06/02/17 04:23 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/02/17 04:23 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)113 %06/02/17 04:23 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %06/02/17 04:23 17060-07-070-130 1
Toluene-d8 (S)110 %06/02/17 04:23 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/01/17 21:00 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 4.7J ug/L 06/01/17 17:36 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-9S Lab ID:92342479009 Collected:05/31/17 13:50 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/06/17 18:17 309-00-206/02/17 10:090.050 0.050 1
alpha-BHC ND ug/L 06/06/17 18:17 319-84-606/02/17 10:090.050 0.050 1
beta-BHC ND ug/L 06/06/17 18:17 319-85-706/02/17 10:090.050 0.050 1
delta-BHC ND ug/L 06/06/17 18:17 319-86-806/02/17 10:090.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/06/17 18:17 58-89-906/02/17 10:090.050 0.050 1
Chlordane (Technical)ND ug/L 06/06/17 18:17 57-74-906/02/17 10:090.50 0.20 1
4,4'-DDD ND ug/L 06/06/17 18:17 72-54-806/02/17 10:090.10 0.050 1
4,4'-DDE ND ug/L 06/06/17 18:17 72-55-906/02/17 10:090.10 0.050 1
4,4'-DDT ND ug/L 06/06/17 18:17 50-29-306/02/17 10:090.10 0.050 1
Dieldrin ND ug/L 06/06/17 18:17 60-57-106/02/17 10:090.075 0.050 1
Endosulfan I ND ug/L 06/06/17 18:17 959-98-806/02/17 10:090.10 0.050 1
Endosulfan II ND ug/L 06/06/17 18:17 33213-65-906/02/17 10:090.10 0.050 1
Endosulfan sulfate ND ug/L 06/06/17 18:17 1031-07-806/02/17 10:090.10 0.050 1
Endrin ND ug/L 06/06/17 18:17 72-20-806/02/17 10:090.10 0.050 1
Endrin aldehyde ND ug/L 06/06/17 18:17 7421-93-406/02/17 10:090.10 0.050 1
Heptachlor ND ug/L 06/06/17 18:17 76-44-806/02/17 10:090.050 0.050 1
Heptachlor epoxide ND ug/L 06/06/17 18:17 1024-57-306/02/17 10:090.075 0.050 1
Methoxychlor ND ug/L 06/06/17 18:17 72-43-506/02/17 10:091.0 0.15 1
Toxaphene ND ug/L 06/06/17 18:17 8001-35-206/02/17 10:091.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)71 %06/06/17 18:17 877-09-806/02/17 10:0920-130 1
Decachlorobiphenyl (S)67 %06/06/17 18:17 2051-24-306/02/17 10:0920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/02/17 18:50 12674-11-206/02/17 10:090.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/02/17 18:50 11104-28-206/02/17 10:090.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/02/17 18:50 11141-16-506/02/17 10:090.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/02/17 18:50 53469-21-906/02/17 10:090.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/02/17 18:50 12672-29-606/02/17 10:090.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/02/17 18:50 11097-69-106/02/17 10:090.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/02/17 18:50 11096-82-506/02/17 10:090.50 0.50 1
Surrogates
Decachlorobiphenyl (S)63 %06/02/17 18:50 2051-24-306/02/17 10:0910-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/07/17 06:01 94-75-7 L106/05/17 16:501.0 0.24 1
Dinoseb ND ug/L 06/07/17 06:01 88-85-7 L106/05/17 16:500.20 0.061 1
Pentachlorophenol ND ug/L 06/07/17 06:01 87-86-506/05/17 16:500.030 0.018 1
2,4,5-T ND ug/L 06/07/17 06:01 93-76-506/05/17 16:500.20 0.045 1
2,4,5-TP (Silvex)ND ug/L 06/07/17 06:01 93-72-106/05/17 16:500.20 0.052 1
Surrogates
2,4-DCAA (S)100 %06/07/17 06:01 19719-28-906/05/17 16:5039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/09/17 16:17 7440-36-006/02/17 15:206.0 3.9 1
Arsenic ND ug/L 06/09/17 16:17 7440-38-206/02/17 15:2010.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-9S Lab ID:92342479009 Collected:05/31/17 13:50 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Barium 104 ug/L 06/09/17 16:17 7440-39-306/02/17 15:201002.5 1
Beryllium ND ug/L 06/09/17 16:17 7440-41-706/02/17 15:201.0 0.50 1
Cadmium ND ug/L 06/09/17 16:17 7440-43-906/02/17 15:201.0 0.50 1
Chromium 5.5J ug/L 06/09/17 16:17 7440-47-306/02/17 15:2010.0 2.5 1
Cobalt 134 ug/L 06/09/17 16:17 7440-48-406/02/17 15:2010.0 2.5 1
Copper ND ug/L 06/09/17 16:17 7440-50-806/02/17 15:2010.0 2.5 1
Lead ND ug/L 06/09/17 16:17 7439-92-106/02/17 15:2010.0 2.5 1
Nickel 10.1J ug/L 06/09/17 16:17 7440-02-006/02/17 15:2050.0 2.5 1
Selenium ND ug/L 06/09/17 16:17 7782-49-206/02/17 15:2010.0 5.0 1
Silver ND ug/L 06/09/17 16:17 7440-22-406/02/17 15:2010.0 2.5 1
Tin ND ug/L 06/09/17 16:17 7440-31-506/02/17 15:201002.5 1
Vanadium ND ug/L 06/09/17 16:17 7440-62-206/02/17 15:2025.0 2.5 1
Zinc 11.6 ug/L 06/09/17 16:17 7440-66-606/02/17 15:2010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.32J ug/L 06/06/17 17:07 7440-28-006/01/17 11:305.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 04:21 7439-97-606/06/17 14:590.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/14/17 20:55 83-32-906/14/17 15:0010.0 1.6 1
Acenaphthylene ND ug/L 06/14/17 20:55 208-96-806/14/17 15:0010.0 1.5 1
Acetophenone ND ug/L 06/14/17 20:55 98-86-206/14/17 15:0010.0 1.9 1
2-Acetylaminofluorene ND ug/L 06/14/17 20:55 53-96-306/14/17 15:0020.0 1.6 1
4-Aminobiphenyl ND ug/L 06/14/17 20:55 92-67-106/14/17 15:0020.0 1.7 1
Anthracene ND ug/L 06/14/17 20:55 120-12-706/14/17 15:0010.0 1.7 1
Benzo(a)anthracene ND ug/L 06/14/17 20:55 56-55-306/14/17 15:0010.0 2.1 1
Benzo(a)pyrene ND ug/L 06/14/17 20:55 50-32-806/14/17 15:0010.0 2.2 1
Benzo(b)fluoranthene ND ug/L 06/14/17 20:55 205-99-206/14/17 15:0010.0 2.2 1
Benzo(g,h,i)perylene ND ug/L 06/14/17 20:55 191-24-206/14/17 15:0010.0 2.1 1
Benzo(k)fluoranthene ND ug/L 06/14/17 20:55 207-08-906/14/17 15:0010.0 2.0 1
Benzyl alcohol ND ug/L 06/14/17 20:55 100-51-606/14/17 15:0020.0 3.1 1
4-Bromophenylphenyl ether ND ug/L 06/14/17 20:55 101-55-306/14/17 15:0010.0 1.5 1
Butylbenzylphthalate ND ug/L 06/14/17 20:55 85-68-706/14/17 15:0010.0 2.5 1
4-Chloro-3-methylphenol ND ug/L 06/14/17 20:55 59-50-706/14/17 15:0020.0 2.8 1
4-Chloroaniline ND ug/L 06/14/17 20:55 106-47-806/14/17 15:0020.0 2.8 1
Chlorobenzilate ND ug/L 06/14/17 20:55 510-15-606/14/17 15:0010.0 2.2 1
bis(2-Chloroethoxy)methane ND ug/L 06/14/17 20:55 111-91-106/14/17 15:0010.0 1.6 1
bis(2-Chloroethyl) ether ND ug/L 06/14/17 20:55 111-44-406/14/17 15:0010.0 1.7 1
2-Chloronaphthalene ND ug/L 06/14/17 20:55 91-58-706/14/17 15:0010.0 1.6 1
2-Chlorophenol ND ug/L 06/14/17 20:55 95-57-806/14/17 15:0010.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/14/17 20:55 7005-72-306/14/17 15:0010.0 1.6 1
Chrysene ND ug/L 06/14/17 20:55 218-01-906/14/17 15:0010.0 2.1 1
Diallate ND ug/L 06/14/17 20:55 2303-16-406/14/17 15:0010.0 1.6 1
Dibenz(a,h)anthracene ND ug/L 06/14/17 20:55 53-70-306/14/17 15:0010.0 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-9S Lab ID:92342479009 Collected:05/31/17 13:50 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Dibenzofuran ND ug/L 06/14/17 20:55 132-64-906/14/17 15:0010.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 06/14/17 20:55 91-94-106/14/17 15:0020.0 3.9 1
2,4-Dichlorophenol ND ug/L 06/14/17 20:55 120-83-206/14/17 15:0010.0 1.6 1
2,6-Dichlorophenol ND ug/L 06/14/17 20:55 87-65-006/14/17 15:0010.0 1.5 1
Diethylphthalate ND ug/L 06/14/17 20:55 84-66-206/14/17 15:0060001.6 1
Dimethoate ND ug/L 06/14/17 20:55 60-51-506/14/17 15:0020.0 1.8 1
P-Dimethylaminoazobenzene ND ug/L 06/14/17 20:55 60-11-706/14/17 15:0010.0 1.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/14/17 20:55 57-97-606/14/17 15:0010.0 2.4 1
3,3'-Dimethylbenzidine ND ug/L 06/14/17 20:55 119-93-706/14/17 15:0010.0 3.9 1
2,4-Dimethylphenol ND ug/L 06/14/17 20:55 105-67-906/14/17 15:0010.0 1.6 1
Dimethylphthalate ND ug/L 06/14/17 20:55 131-11-306/14/17 15:0010.0 1.4 1
Di-n-butylphthalate ND ug/L 06/14/17 20:55 84-74-206/14/17 15:0010.0 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/14/17 20:55 534-52-106/14/17 15:0050.0 2.2 1
1,3-Dinitrobenzene ND ug/L 06/14/17 20:55 99-65-006/14/17 15:0020.0 1.3 1
2,4-Dinitrophenol ND ug/L 06/14/17 20:55 51-28-506/14/17 15:0050.0 5.1 1
2,4-Dinitrotoluene ND ug/L 06/14/17 20:55 121-14-206/14/17 15:0010.0 1.5 1
2,6-Dinitrotoluene ND ug/L 06/14/17 20:55 606-20-206/14/17 15:0010.0 1.4 1
Di-n-octylphthalate ND ug/L 06/14/17 20:55 117-84-006/14/17 15:0010.0 1.5 1
Diphenylamine ND ug/L 06/14/17 20:55 122-39-406/14/17 15:0010.0 1.4 1
Disulfoton ND ug/L 06/14/17 20:55 298-04-406/14/17 15:0010.0 1.5 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/14/17 20:55 117-81-706/14/17 15:0015.0 2.3 1
Ethyl methanesulfonate ND ug/L 06/14/17 20:55 62-50-006/14/17 15:0020.0 1.6 1
Famphur ND ug/L 06/14/17 20:55 52-85-706/14/17 15:0020.0 5.7 1
Fluoranthene ND ug/L 06/14/17 20:55 206-44-006/14/17 15:0010.0 2.2 1
Fluorene ND ug/L 06/14/17 20:55 86-73-706/14/17 15:0010.0 1.6 1
Hexachlorobenzene ND ug/L 06/14/17 20:55 118-74-106/14/17 15:0010.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 06/14/17 20:55 77-47-406/14/17 15:0010.0 1.3 1
Hexachloroethane ND ug/L 06/14/17 20:55 67-72-106/14/17 15:0010.0 1.8 1
Hexachloropropene ND ug/L 06/14/17 20:55 1888-71-706/14/17 15:0010.0 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/14/17 20:55 193-39-506/14/17 15:0010.0 2.0 1
Isodrin ND ug/L 06/14/17 20:55 465-73-606/14/17 15:0020.0 2.5 1
Isophorone ND ug/L 06/14/17 20:55 78-59-106/14/17 15:0010.0 1.5 1
Isosafrole ND ug/L 06/14/17 20:55 120-58-106/14/17 15:0010.0 1.5 1
Kepone ND ug/L 06/14/17 20:55 143-50-006/14/17 15:0020.0 4.5 1
Methapyrilene ND ug/L 06/14/17 20:55 91-80-506/14/17 15:001003.0 1
3-Methylcholanthrene ND ug/L 06/14/17 20:55 56-49-506/14/17 15:0010.0 2.7 1
Methyl methanesulfonate ND ug/L 06/14/17 20:55 66-27-306/14/17 15:0010.0 1.1 1
2-Methylnaphthalene ND ug/L 06/14/17 20:55 91-57-606/14/17 15:0010.0 1.4 1
Methyl parathion ND ug/L 06/14/17 20:55 298-00-006/14/17 15:0010.0 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 06/14/17 20:55 95-48-706/14/17 15:0010.0 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/14/17 20:55 15831-10-406/14/17 15:0010.0 1.4 1
1-Naphthalenamine ND ug/L 06/14/17 20:55 134-32-706/14/17 15:0010.0 1.3 1
2-Naphthalenamine ND ug/L 06/14/17 20:55 91-59-806/14/17 15:0010.0 2.2 1
1,4-Naphthoquinone ND ug/L 06/14/17 20:55 130-15-406/14/17 15:0010.0 0.99 1
2-Nitroaniline ND ug/L 06/14/17 20:55 88-74-406/14/17 15:0050.0 2.3 1
3-Nitroaniline ND ug/L 06/14/17 20:55 99-09-206/14/17 15:0050.0 2.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
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Page 62 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-9S Lab ID:92342479009 Collected:05/31/17 13:50 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Nitroaniline ND ug/L 06/14/17 20:55 100-01-606/14/17 15:0020.0 3.4 1
Nitrobenzene ND ug/L 06/14/17 20:55 98-95-306/14/17 15:0010.0 1.6 1
2-Nitrophenol ND ug/L 06/14/17 20:55 88-75-506/14/17 15:0010.0 1.6 1
4-Nitrophenol ND ug/L 06/14/17 20:55 100-02-706/14/17 15:0050.0 4.3 1
5-Nitro-o-toluidine ND ug/L 06/14/17 20:55 99-55-806/14/17 15:0010.0 1.9 1
N-Nitrosodiethylamine ND ug/L 06/14/17 20:55 55-18-506/14/17 15:0020.0 1.4 1
N-Nitrosodimethylamine ND ug/L 06/14/17 20:55 62-75-906/14/17 15:0010.0 1.6 1
N-Nitroso-di-n-butylamine ND ug/L 06/14/17 20:55 924-16-306/14/17 15:0010.0 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 06/14/17 20:55 621-64-706/14/17 15:0010.0 1.7 1
N-Nitrosodiphenylamine ND ug/L 06/14/17 20:55 86-30-606/14/17 15:0010.0 1.4 1
N-Nitrosomethylethylamine ND ug/L 06/14/17 20:55 10595-95-606/14/17 15:0010.0 1.4 1
N-Nitrosopiperidine ND ug/L 06/14/17 20:55 100-75-406/14/17 15:0020.0 1.7 1
N-Nitrosopyrrolidine ND ug/L 06/14/17 20:55 930-55-206/14/17 15:0010.0 1.7 1
O,O,O-Triethylphosphorothioate ND ug/L 06/14/17 20:55 126-68-106/14/17 15:0010.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/14/17 20:55 108-60-106/14/17 15:0010.0 1.8 1
Parathion (Ethyl parathion)ND ug/L 06/14/17 20:55 56-38-206/14/17 15:0010.0 1.5 1
Pentachlorobenzene ND ug/L 06/14/17 20:55 608-93-506/14/17 15:0010.0 1.5 1
Pentachloronitrobenzene ND ug/L 06/14/17 20:55 82-68-806/14/17 15:0020.0 1.7 1
Pentachlorophenol ND ug/L 06/14/17 20:55 87-86-506/14/17 15:0025.0 3.5 1
Phenacetin ND ug/L 06/14/17 20:55 62-44-206/14/17 15:0020.0 1.9 1
Phenanthrene ND ug/L 06/14/17 20:55 85-01-806/14/17 15:0010.0 1.6 1
Phenol ND ug/L 06/14/17 20:55 108-95-206/14/17 15:0010.0 1.3 1
p-Phenylenediamine ND ug/L 06/14/17 20:55 106-50-306/14/17 15:0010.0 2.2 1
Phorate ND ug/L 06/14/17 20:55 298-02-206/14/17 15:0010.0 1.7 1
Pronamide ND ug/L 06/14/17 20:55 23950-58-506/14/17 15:0010.0 2.0 1
Pyrene ND ug/L 06/14/17 20:55 129-00-006/14/17 15:0010.0 2.2 1
Safrole ND ug/L 06/14/17 20:55 94-59-706/14/17 15:0010.0 1.3 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/14/17 20:55 95-94-306/14/17 15:0010.0 1.3 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/14/17 20:55 58-90-206/14/17 15:0010.0 2.9 1
Thionazin ND ug/L 06/14/17 20:55 297-97-206/14/17 15:0020.0 1.7 1
O-Toluidine ND ug/L 06/14/17 20:55 95-53-406/14/17 15:0010.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 06/14/17 20:55 95-95-406/14/17 15:0010.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/14/17 20:55 88-06-206/14/17 15:0010.0 1.4 1
1,3,5-Trinitrobenzene ND ug/L 06/14/17 20:55 99-35-406/14/17 15:0010.0 1.2 1
Surrogates
Nitrobenzene-d5 (S)81 %06/14/17 20:55 4165-60-0 1g06/14/17 15:0021-110 1
2-Fluorobiphenyl (S)93 %06/14/17 20:55 321-60-806/14/17 15:0027-110 1
Terphenyl-d14 (S)91 %06/14/17 20:55 1718-51-006/14/17 15:0031-107 1
Phenol-d6 (S)27 %06/14/17 20:55 13127-88-306/14/17 15:0010-110 1
2-Fluorophenol (S)43 %06/14/17 20:55 367-12-406/14/17 15:0012-110 1
2,4,6-Tribromophenol (S)93 %06/14/17 20:55 118-79-606/14/17 15:0027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 10.9J ug/L 06/02/17 04:40 67-64-110010.0 1
Acetonitrile ND ug/L 06/02/17 04:40 75-05-855.0 2.2 1
Acrolein ND ug/L 06/02/17 04:40 107-02-853.0 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 63 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-9S Lab ID:92342479009 Collected:05/31/17 13:50 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acrylonitrile ND ug/L 06/02/17 04:40 107-13-12001.9 1
Allyl chloride ND ug/L 06/02/17 04:40 107-05-110.0 1.5 1
Benzene 0.48J ug/L 06/02/17 04:40 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/02/17 04:40 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/02/17 04:40 75-27-41.0 0.18 1
Bromoform ND ug/L 06/02/17 04:40 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/02/17 04:40 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/02/17 04:40 78-93-31000.96 1
Carbon disulfide ND ug/L 06/02/17 04:40 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/02/17 04:40 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/02/17 04:40 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/02/17 04:40 75-00-310.0 0.54 1
Chloroform ND ug/L 06/02/17 04:40 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/02/17 04:40 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/02/17 04:40 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/02/17 04:40 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/02/17 04:40 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/02/17 04:40 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/02/17 04:40 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/02/17 04:40 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/02/17 04:40 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/02/17 04:40 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/02/17 04:40 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/02/17 04:40 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/02/17 04:40 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/02/17 04:40 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/02/17 04:40 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 4.1J ug/L 06/02/17 04:40 156-59-25.0 0.19 1
trans-1,2-Dichloroethene 0.81J ug/L 06/02/17 04:40 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/02/17 04:40 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/02/17 04:40 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/02/17 04:40 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/02/17 04:40 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/02/17 04:40 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/02/17 04:40 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/02/17 04:40 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/02/17 04:40 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/02/17 04:40 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/02/17 04:40 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/02/17 04:40 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/02/17 04:40 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/02/17 04:40 126-98-71000.93 1
Methylene Chloride ND ug/L 06/02/17 04:40 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/02/17 04:40 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/02/17 04:40 108-10-11000.33 1
Naphthalene ND ug/L 06/02/17 04:40 91-20-310.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-9S Lab ID:92342479009 Collected:05/31/17 13:50 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Propionitrile ND ug/L 06/02/17 04:40 107-12-01503.6 1
Styrene ND ug/L 06/02/17 04:40 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/02/17 04:40 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/02/17 04:40 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/02/17 04:40 127-18-41.0 0.46 1
Toluene ND ug/L 06/02/17 04:40 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/02/17 04:40 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/02/17 04:40 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/02/17 04:40 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/02/17 04:40 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/02/17 04:40 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/02/17 04:40 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/02/17 04:40 108-05-450.0 0.35 1
Vinyl chloride 0.67J ug/L 06/02/17 04:40 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/02/17 04:40 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)112 %06/02/17 04:40 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %06/02/17 04:40 17060-07-070-130 1
Toluene-d8 (S)114 %06/02/17 04:40 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/01/17 21:00 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 15.1 ug/L 06/01/17 17:37 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-9D Lab ID:92342479010 Collected:05/31/17 13:30 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/06/17 18:35 309-00-206/02/17 10:090.050 0.050 1
alpha-BHC ND ug/L 06/06/17 18:35 319-84-606/02/17 10:090.050 0.050 1
beta-BHC ND ug/L 06/06/17 18:35 319-85-706/02/17 10:090.050 0.050 1
delta-BHC ND ug/L 06/06/17 18:35 319-86-806/02/17 10:090.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/06/17 18:35 58-89-906/02/17 10:090.050 0.050 1
Chlordane (Technical)ND ug/L 06/06/17 18:35 57-74-906/02/17 10:090.50 0.20 1
4,4'-DDD ND ug/L 06/06/17 18:35 72-54-806/02/17 10:090.10 0.050 1
4,4'-DDE ND ug/L 06/06/17 18:35 72-55-906/02/17 10:090.10 0.050 1
4,4'-DDT ND ug/L 06/06/17 18:35 50-29-306/02/17 10:090.10 0.050 1
Dieldrin ND ug/L 06/06/17 18:35 60-57-106/02/17 10:090.075 0.050 1
Endosulfan I ND ug/L 06/06/17 18:35 959-98-806/02/17 10:090.10 0.050 1
Endosulfan II ND ug/L 06/06/17 18:35 33213-65-906/02/17 10:090.10 0.050 1
Endosulfan sulfate ND ug/L 06/06/17 18:35 1031-07-806/02/17 10:090.10 0.050 1
Endrin ND ug/L 06/06/17 18:35 72-20-806/02/17 10:090.10 0.050 1
Endrin aldehyde ND ug/L 06/06/17 18:35 7421-93-406/02/17 10:090.10 0.050 1
Heptachlor ND ug/L 06/06/17 18:35 76-44-806/02/17 10:090.050 0.050 1
Heptachlor epoxide ND ug/L 06/06/17 18:35 1024-57-306/02/17 10:090.075 0.050 1
Methoxychlor ND ug/L 06/06/17 18:35 72-43-506/02/17 10:091.0 0.15 1
Toxaphene ND ug/L 06/06/17 18:35 8001-35-206/02/17 10:091.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)78 %06/06/17 18:35 877-09-806/02/17 10:0920-130 1
Decachlorobiphenyl (S)86 %06/06/17 18:35 2051-24-306/02/17 10:0920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/02/17 19:11 12674-11-206/02/17 10:090.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/02/17 19:11 11104-28-206/02/17 10:090.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/02/17 19:11 11141-16-506/02/17 10:090.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/02/17 19:11 53469-21-906/02/17 10:090.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/02/17 19:11 12672-29-606/02/17 10:090.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/02/17 19:11 11097-69-106/02/17 10:090.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/02/17 19:11 11096-82-506/02/17 10:090.50 0.50 1
Surrogates
Decachlorobiphenyl (S)80 %06/02/17 19:11 2051-24-306/02/17 10:0910-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/07/17 06:31 94-75-7 L106/05/17 16:501.0 0.25 1
Dinoseb ND ug/L 06/07/17 06:31 88-85-7 L106/05/17 16:500.21 0.062 1
Pentachlorophenol ND ug/L 06/07/17 06:31 87-86-506/05/17 16:500.031 0.019 1
2,4,5-T ND ug/L 06/07/17 06:31 93-76-506/05/17 16:500.21 0.046 1
2,4,5-TP (Silvex)ND ug/L 06/07/17 06:31 93-72-106/05/17 16:500.21 0.054 1
Surrogates
2,4-DCAA (S)97 %06/07/17 06:31 19719-28-906/05/17 16:5039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/09/17 16:20 7440-36-006/02/17 15:206.0 3.9 1
Arsenic ND ug/L 06/09/17 16:20 7440-38-206/02/17 15:2010.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-9D Lab ID:92342479010 Collected:05/31/17 13:30 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Barium 40.4J ug/L 06/09/17 16:20 7440-39-306/02/17 15:201002.5 1
Beryllium ND ug/L 06/09/17 16:20 7440-41-706/02/17 15:201.0 0.50 1
Cadmium ND ug/L 06/09/17 16:20 7440-43-906/02/17 15:201.0 0.50 1
Chromium ND ug/L 06/09/17 16:20 7440-47-306/02/17 15:2010.0 2.5 1
Cobalt ND ug/L 06/09/17 16:20 7440-48-406/02/17 15:2010.0 2.5 1
Copper ND ug/L 06/09/17 16:20 7440-50-806/02/17 15:2010.0 2.5 1
Lead ND ug/L 06/09/17 16:20 7439-92-106/02/17 15:2010.0 2.5 1
Nickel ND ug/L 06/09/17 16:20 7440-02-006/02/17 15:2050.0 2.5 1
Selenium ND ug/L 06/09/17 16:20 7782-49-206/02/17 15:2010.0 5.0 1
Silver ND ug/L 06/09/17 16:20 7440-22-406/02/17 15:2010.0 2.5 1
Tin ND ug/L 06/09/17 16:20 7440-31-506/02/17 15:201002.5 1
Vanadium ND ug/L 06/09/17 16:20 7440-62-206/02/17 15:2025.0 2.5 1
Zinc ND ug/L 06/09/17 16:20 7440-66-606/02/17 15:2010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/06/17 17:09 7440-28-006/01/17 11:305.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 04:23 7439-97-606/06/17 14:590.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/13/17 18:00 83-32-906/07/17 16:1010.0 1.6 1
Acenaphthylene ND ug/L 06/13/17 18:00 208-96-806/07/17 16:1010.0 1.5 1
Acetophenone ND ug/L 06/13/17 18:00 98-86-206/07/17 16:1010.0 1.9 1
2-Acetylaminofluorene ND ug/L 06/13/17 18:00 53-96-3 L206/07/17 16:1020.0 1.6 1
4-Aminobiphenyl ND ug/L 06/13/17 18:00 92-67-106/07/17 16:1020.0 1.7 1
Anthracene ND ug/L 06/13/17 18:00 120-12-706/07/17 16:1010.0 1.7 1
Benzo(a)anthracene ND ug/L 06/13/17 18:00 56-55-306/07/17 16:1010.0 2.1 1
Benzo(a)pyrene ND ug/L 06/13/17 18:00 50-32-806/07/17 16:1010.0 2.2 1
Benzo(b)fluoranthene ND ug/L 06/13/17 18:00 205-99-206/07/17 16:1010.0 2.2 1
Benzo(g,h,i)perylene ND ug/L 06/13/17 18:00 191-24-206/07/17 16:1010.0 2.1 1
Benzo(k)fluoranthene ND ug/L 06/13/17 18:00 207-08-906/07/17 16:1010.0 2.0 1
Benzyl alcohol ND ug/L 06/13/17 18:00 100-51-6 L206/07/17 16:1020.0 3.1 1
4-Bromophenylphenyl ether ND ug/L 06/13/17 18:00 101-55-306/07/17 16:1010.0 1.5 1
Butylbenzylphthalate ND ug/L 06/13/17 18:00 85-68-706/07/17 16:1010.0 2.5 1
4-Chloro-3-methylphenol ND ug/L 06/13/17 18:00 59-50-706/07/17 16:1020.0 2.8 1
4-Chloroaniline ND ug/L 06/13/17 18:00 106-47-806/07/17 16:1020.0 2.8 1
Chlorobenzilate ND ug/L 06/13/17 18:00 510-15-606/07/17 16:1010.0 2.2 1
bis(2-Chloroethoxy)methane ND ug/L 06/13/17 18:00 111-91-1 L206/07/17 16:1010.0 1.6 1
bis(2-Chloroethyl) ether ND ug/L 06/13/17 18:00 111-44-4 L206/07/17 16:1010.0 1.7 1
2-Chloronaphthalene ND ug/L 06/13/17 18:00 91-58-7 L206/07/17 16:1010.0 1.6 1
2-Chlorophenol ND ug/L 06/13/17 18:00 95-57-8 L206/07/17 16:1010.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/13/17 18:00 7005-72-306/07/17 16:1010.0 1.6 1
Chrysene ND ug/L 06/13/17 18:00 218-01-906/07/17 16:1010.0 2.1 1
Diallate ND ug/L 06/13/17 18:00 2303-16-406/07/17 16:1010.0 1.6 1
Dibenz(a,h)anthracene ND ug/L 06/13/17 18:00 53-70-306/07/17 16:1010.0 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
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Page 67 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-9D Lab ID:92342479010 Collected:05/31/17 13:30 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Dibenzofuran ND ug/L 06/13/17 18:00 132-64-906/07/17 16:1010.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 06/13/17 18:00 91-94-106/07/17 16:1020.0 3.9 1
2,4-Dichlorophenol ND ug/L 06/13/17 18:00 120-83-2 L206/07/17 16:1010.0 1.6 1
2,6-Dichlorophenol ND ug/L 06/13/17 18:00 87-65-0 L206/07/17 16:1010.0 1.5 1
Diethylphthalate ND ug/L 06/13/17 18:00 84-66-206/07/17 16:1060001.6 1
Dimethoate ND ug/L 06/13/17 18:00 60-51-506/07/17 16:1020.0 1.8 1
P-Dimethylaminoazobenzene ND ug/L 06/13/17 18:00 60-11-706/07/17 16:1010.0 1.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/13/17 18:00 57-97-606/07/17 16:1010.0 2.4 1
3,3'-Dimethylbenzidine ND ug/L 06/13/17 18:00 119-93-706/07/17 16:1010.0 3.9 1
2,4-Dimethylphenol ND ug/L 06/13/17 18:00 105-67-9 L206/07/17 16:1010.0 1.6 1
Dimethylphthalate ND ug/L 06/13/17 18:00 131-11-306/07/17 16:1010.0 1.4 1
Di-n-butylphthalate ND ug/L 06/13/17 18:00 84-74-206/07/17 16:1010.0 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/13/17 18:00 534-52-106/07/17 16:1050.0 2.2 1
1,3-Dinitrobenzene ND ug/L 06/13/17 18:00 99-65-006/07/17 16:1020.0 1.3 1
2,4-Dinitrophenol ND ug/L 06/13/17 18:00 51-28-506/07/17 16:1050.0 5.1 1
2,4-Dinitrotoluene ND ug/L 06/13/17 18:00 121-14-206/07/17 16:1010.0 1.5 1
2,6-Dinitrotoluene ND ug/L 06/13/17 18:00 606-20-206/07/17 16:1010.0 1.4 1
Di-n-octylphthalate ND ug/L 06/13/17 18:00 117-84-006/07/17 16:1010.0 1.5 1
Diphenylamine ND ug/L 06/13/17 18:00 122-39-406/07/17 16:1010.0 1.4 1
Disulfoton ND ug/L 06/13/17 18:00 298-04-406/07/17 16:1010.0 1.5 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/13/17 18:00 117-81-706/07/17 16:1015.0 2.3 1
Ethyl methanesulfonate ND ug/L 06/13/17 18:00 62-50-0 L206/07/17 16:1020.0 1.6 1
Famphur ND ug/L 06/13/17 18:00 52-85-706/07/17 16:1020.0 5.7 1
Fluoranthene ND ug/L 06/13/17 18:00 206-44-006/07/17 16:1010.0 2.2 1
Fluorene ND ug/L 06/13/17 18:00 86-73-706/07/17 16:1010.0 1.6 1
Hexachlorobenzene ND ug/L 06/13/17 18:00 118-74-106/07/17 16:1010.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 06/13/17 18:00 77-47-4 L206/07/17 16:1010.0 1.3 1
Hexachloroethane ND ug/L 06/13/17 18:00 67-72-1 L206/07/17 16:1010.0 1.8 1
Hexachloropropene ND ug/L 06/13/17 18:00 1888-71-706/07/17 16:1010.0 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/13/17 18:00 193-39-506/07/17 16:1010.0 2.0 1
Isodrin ND ug/L 06/13/17 18:00 465-73-606/07/17 16:1020.0 2.5 1
Isophorone ND ug/L 06/13/17 18:00 78-59-1 L206/07/17 16:1010.0 1.5 1
Isosafrole ND ug/L 06/13/17 18:00 120-58-1 L206/07/17 16:1010.0 1.5 1
Kepone ND ug/L 06/13/17 18:00 143-50-006/07/17 16:1020.0 4.5 1
Methapyrilene ND ug/L 06/13/17 18:00 91-80-506/07/17 16:101003.0 1
3-Methylcholanthrene ND ug/L 06/13/17 18:00 56-49-506/07/17 16:1010.0 2.7 1
Methyl methanesulfonate ND ug/L 06/13/17 18:00 66-27-306/07/17 16:1010.0 1.1 1
2-Methylnaphthalene ND ug/L 06/13/17 18:00 91-57-6 L206/07/17 16:1010.0 1.4 1
Methyl parathion ND ug/L 06/13/17 18:00 298-00-006/07/17 16:1010.0 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 06/13/17 18:00 95-48-7 L206/07/17 16:1010.0 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/13/17 18:00 15831-10-4 L206/07/17 16:1010.0 1.4 1
1-Naphthalenamine ND ug/L 06/13/17 18:00 134-32-706/07/17 16:1010.0 1.3 1
2-Naphthalenamine ND ug/L 06/13/17 18:00 91-59-806/07/17 16:1010.0 2.2 1
1,4-Naphthoquinone ND ug/L 06/13/17 18:00 130-15-406/07/17 16:1010.0 0.99 1
2-Nitroaniline ND ug/L 06/13/17 18:00 88-74-406/07/17 16:1050.0 2.3 1
3-Nitroaniline ND ug/L 06/13/17 18:00 99-09-206/07/17 16:1050.0 2.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-9D Lab ID:92342479010 Collected:05/31/17 13:30 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Nitroaniline ND ug/L 06/13/17 18:00 100-01-606/07/17 16:1020.0 3.4 1
Nitrobenzene ND ug/L 06/13/17 18:00 98-95-3 L206/07/17 16:1010.0 1.6 1
2-Nitrophenol ND ug/L 06/13/17 18:00 88-75-5 L206/07/17 16:1010.0 1.6 1
4-Nitrophenol ND ug/L 06/13/17 18:00 100-02-706/07/17 16:1050.0 4.3 1
5-Nitro-o-toluidine ND ug/L 06/13/17 18:00 99-55-8 L206/07/17 16:1010.0 1.9 1
N-Nitrosodiethylamine ND ug/L 06/13/17 18:00 55-18-5 L206/07/17 16:1020.0 1.4 1
N-Nitrosodimethylamine ND ug/L 06/13/17 18:00 62-75-906/07/17 16:1010.0 1.6 1
N-Nitroso-di-n-butylamine ND ug/L 06/13/17 18:00 924-16-3 L206/07/17 16:1010.0 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 06/13/17 18:00 621-64-7 L206/07/17 16:1010.0 1.7 1
N-Nitrosodiphenylamine ND ug/L 06/13/17 18:00 86-30-606/07/17 16:1010.0 1.4 1
N-Nitrosomethylethylamine ND ug/L 06/13/17 18:00 10595-95-6 L206/07/17 16:1010.0 1.4 1
N-Nitrosopiperidine ND ug/L 06/13/17 18:00 100-75-4 L206/07/17 16:1020.0 1.7 1
N-Nitrosopyrrolidine ND ug/L 06/13/17 18:00 930-55-2 L206/07/17 16:1010.0 1.7 1
O,O,O-Triethylphosphorothioate ND ug/L 06/13/17 18:00 126-68-1 L206/07/17 16:1010.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/13/17 18:00 108-60-106/07/17 16:1010.0 1.8 1
Parathion (Ethyl parathion)ND ug/L 06/13/17 18:00 56-38-2 L206/07/17 16:1010.0 1.5 1
Pentachlorobenzene ND ug/L 06/13/17 18:00 608-93-506/07/17 16:1010.0 1.5 1
Pentachloronitrobenzene ND ug/L 06/13/17 18:00 82-68-806/07/17 16:1020.0 1.7 1
Pentachlorophenol ND ug/L 06/13/17 18:00 87-86-506/07/17 16:1025.0 3.5 1
Phenacetin ND ug/L 06/13/17 18:00 62-44-206/07/17 16:1020.0 1.9 1
Phenanthrene ND ug/L 06/13/17 18:00 85-01-806/07/17 16:1010.0 1.6 1
Phenol ND ug/L 06/13/17 18:00 108-95-206/07/17 16:1010.0 1.3 1
p-Phenylenediamine ND ug/L 06/13/17 18:00 106-50-3 L206/07/17 16:1010.0 2.2 1
Phorate ND ug/L 06/13/17 18:00 298-02-2 L206/07/17 16:1010.0 1.7 1
Pronamide ND ug/L 06/13/17 18:00 23950-58-5 L206/07/17 16:1010.0 2.0 1
Pyrene ND ug/L 06/13/17 18:00 129-00-006/07/17 16:1010.0 2.2 1
Safrole ND ug/L 06/13/17 18:00 94-59-7 L206/07/17 16:1010.0 1.3 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/13/17 18:00 95-94-306/07/17 16:1010.0 1.3 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/13/17 18:00 58-90-206/07/17 16:1010.0 2.9 1
Thionazin ND ug/L 06/13/17 18:00 297-97-2 L206/07/17 16:1020.0 1.7 1
O-Toluidine ND ug/L 06/13/17 18:00 95-53-4 L206/07/17 16:1010.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 06/13/17 18:00 95-95-406/07/17 16:1010.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/13/17 18:00 88-06-206/07/17 16:1010.0 1.4 1
1,3,5-Trinitrobenzene ND ug/L 06/13/17 18:00 99-35-4 L206/07/17 16:1010.0 1.2 1
Surrogates
Nitrobenzene-d5 (S)69 %06/13/17 18:00 4165-60-0 1g06/07/17 16:1021-110 1
2-Fluorobiphenyl (S)85 %06/13/17 18:00 321-60-806/07/17 16:1027-110 1
Terphenyl-d14 (S)91 %06/13/17 18:00 1718-51-006/07/17 16:1031-107 1
Phenol-d6 (S)38 %06/13/17 18:00 13127-88-306/07/17 16:1010-110 1
2-Fluorophenol (S)43 %06/13/17 18:00 367-12-406/07/17 16:1012-110 1
2,4,6-Tribromophenol (S)80 %06/13/17 18:00 118-79-606/07/17 16:1027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/02/17 04:58 67-64-110010.0 1
Acetonitrile ND ug/L 06/02/17 04:58 75-05-855.0 2.2 1
Acrolein ND ug/L 06/02/17 04:58 107-02-853.0 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-9D Lab ID:92342479010 Collected:05/31/17 13:30 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acrylonitrile ND ug/L 06/02/17 04:58 107-13-12001.9 1
Allyl chloride ND ug/L 06/02/17 04:58 107-05-110.0 1.5 1
Benzene ND ug/L 06/02/17 04:58 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/02/17 04:58 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/02/17 04:58 75-27-41.0 0.18 1
Bromoform ND ug/L 06/02/17 04:58 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/02/17 04:58 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/02/17 04:58 78-93-31000.96 1
Carbon disulfide ND ug/L 06/02/17 04:58 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/02/17 04:58 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/02/17 04:58 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/02/17 04:58 75-00-310.0 0.54 1
Chloroform ND ug/L 06/02/17 04:58 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/02/17 04:58 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/02/17 04:58 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/02/17 04:58 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/02/17 04:58 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/02/17 04:58 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/02/17 04:58 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/02/17 04:58 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/02/17 04:58 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/02/17 04:58 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/02/17 04:58 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/02/17 04:58 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/02/17 04:58 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/02/17 04:58 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/02/17 04:58 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.84J ug/L 06/02/17 04:58 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/02/17 04:58 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/02/17 04:58 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/02/17 04:58 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/02/17 04:58 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/02/17 04:58 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/02/17 04:58 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/02/17 04:58 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/02/17 04:58 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/02/17 04:58 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/02/17 04:58 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/02/17 04:58 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/02/17 04:58 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/02/17 04:58 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/02/17 04:58 126-98-71000.93 1
Methylene Chloride ND ug/L 06/02/17 04:58 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/02/17 04:58 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/02/17 04:58 108-10-11000.33 1
Naphthalene ND ug/L 06/02/17 04:58 91-20-310.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-9D Lab ID:92342479010 Collected:05/31/17 13:30 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Propionitrile ND ug/L 06/02/17 04:58 107-12-01503.6 1
Styrene ND ug/L 06/02/17 04:58 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/02/17 04:58 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/02/17 04:58 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/02/17 04:58 127-18-41.0 0.46 1
Toluene ND ug/L 06/02/17 04:58 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/02/17 04:58 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/02/17 04:58 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/02/17 04:58 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/02/17 04:58 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/02/17 04:58 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/02/17 04:58 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/02/17 04:58 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/02/17 04:58 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/02/17 04:58 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)113 %06/02/17 04:58 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %06/02/17 04:58 17060-07-070-130 1
Toluene-d8 (S)114 %06/02/17 04:58 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/01/17 21:00 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 5.2J ug/L 06/01/17 17:38 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-10 Lab ID:92342479011 Collected:05/31/17 13:05 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/06/17 18:53 309-00-206/02/17 10:090.050 0.050 1
alpha-BHC ND ug/L 06/06/17 18:53 319-84-606/02/17 10:090.050 0.050 1
beta-BHC ND ug/L 06/06/17 18:53 319-85-706/02/17 10:090.050 0.050 1
delta-BHC ND ug/L 06/06/17 18:53 319-86-806/02/17 10:090.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/06/17 18:53 58-89-906/02/17 10:090.050 0.050 1
Chlordane (Technical)ND ug/L 06/06/17 18:53 57-74-906/02/17 10:090.50 0.20 1
4,4'-DDD ND ug/L 06/06/17 18:53 72-54-806/02/17 10:090.10 0.050 1
4,4'-DDE ND ug/L 06/06/17 18:53 72-55-906/02/17 10:090.10 0.050 1
4,4'-DDT ND ug/L 06/06/17 18:53 50-29-306/02/17 10:090.10 0.050 1
Dieldrin ND ug/L 06/06/17 18:53 60-57-106/02/17 10:090.075 0.050 1
Endosulfan I ND ug/L 06/06/17 18:53 959-98-806/02/17 10:090.10 0.050 1
Endosulfan II ND ug/L 06/06/17 18:53 33213-65-906/02/17 10:090.10 0.050 1
Endosulfan sulfate ND ug/L 06/06/17 18:53 1031-07-806/02/17 10:090.10 0.050 1
Endrin ND ug/L 06/06/17 18:53 72-20-806/02/17 10:090.10 0.050 1
Endrin aldehyde ND ug/L 06/06/17 18:53 7421-93-406/02/17 10:090.10 0.050 1
Heptachlor ND ug/L 06/06/17 18:53 76-44-806/02/17 10:090.050 0.050 1
Heptachlor epoxide ND ug/L 06/06/17 18:53 1024-57-306/02/17 10:090.075 0.050 1
Methoxychlor ND ug/L 06/06/17 18:53 72-43-506/02/17 10:091.0 0.15 1
Toxaphene ND ug/L 06/06/17 18:53 8001-35-206/02/17 10:091.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)58 %06/06/17 18:53 877-09-806/02/17 10:0920-130 1
Decachlorobiphenyl (S)40 %06/06/17 18:53 2051-24-306/02/17 10:0920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/02/17 19:31 12674-11-206/02/17 10:090.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/02/17 19:31 11104-28-206/02/17 10:090.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/02/17 19:31 11141-16-506/02/17 10:090.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/02/17 19:31 53469-21-906/02/17 10:090.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/02/17 19:31 12672-29-606/02/17 10:090.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/02/17 19:31 11097-69-106/02/17 10:090.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/02/17 19:31 11096-82-506/02/17 10:090.50 0.50 1
Surrogates
Decachlorobiphenyl (S)40 %06/02/17 19:31 2051-24-306/02/17 10:0910-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/07/17 07:00 94-75-7 L106/05/17 16:501.0 0.24 1
Dinoseb ND ug/L 06/07/17 07:00 88-85-7 L106/05/17 16:500.20 0.060 1
Pentachlorophenol ND ug/L 06/07/17 07:00 87-86-506/05/17 16:500.030 0.018 1
2,4,5-T ND ug/L 06/07/17 07:00 93-76-506/05/17 16:500.20 0.045 1
2,4,5-TP (Silvex)ND ug/L 06/07/17 07:00 93-72-106/05/17 16:500.20 0.052 1
Surrogates
2,4-DCAA (S)95 %06/07/17 07:00 19719-28-906/05/17 16:5039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/09/17 16:24 7440-36-006/02/17 15:206.0 3.9 1
Arsenic ND ug/L 06/09/17 16:24 7440-38-206/02/17 15:2010.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-10 Lab ID:92342479011 Collected:05/31/17 13:05 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Barium 42.6J ug/L 06/09/17 16:24 7440-39-306/02/17 15:201002.5 1
Beryllium ND ug/L 06/09/17 16:24 7440-41-706/02/17 15:201.0 0.50 1
Cadmium ND ug/L 06/09/17 16:24 7440-43-906/02/17 15:201.0 0.50 1
Chromium ND ug/L 06/09/17 16:24 7440-47-306/02/17 15:2010.0 2.5 1
Cobalt ND ug/L 06/09/17 16:24 7440-48-406/02/17 15:2010.0 2.5 1
Copper ND ug/L 06/09/17 16:24 7440-50-806/02/17 15:2010.0 2.5 1
Lead ND ug/L 06/09/17 16:24 7439-92-106/02/17 15:2010.0 2.5 1
Nickel 2.8J ug/L 06/09/17 16:24 7440-02-006/02/17 15:2050.0 2.5 1
Selenium ND ug/L 06/09/17 16:24 7782-49-206/02/17 15:2010.0 5.0 1
Silver ND ug/L 06/09/17 16:24 7440-22-406/02/17 15:2010.0 2.5 1
Tin ND ug/L 06/09/17 16:24 7440-31-506/02/17 15:201002.5 1
Vanadium 4.0J ug/L 06/09/17 16:24 7440-62-206/02/17 15:2025.0 2.5 1
Zinc 6.2J ug/L 06/09/17 16:24 7440-66-606/02/17 15:2010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.042J ug/L 06/06/17 17:11 7440-28-006/01/17 11:305.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 02:27 7439-97-606/04/17 20:450.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/13/17 18:29 83-32-906/07/17 16:1010.0 1.6 1
Acenaphthylene ND ug/L 06/13/17 18:29 208-96-806/07/17 16:1010.0 1.5 1
Acetophenone ND ug/L 06/13/17 18:29 98-86-206/07/17 16:1010.0 1.9 1
2-Acetylaminofluorene ND ug/L 06/13/17 18:29 53-96-3 L206/07/17 16:1020.0 1.6 1
4-Aminobiphenyl ND ug/L 06/13/17 18:29 92-67-106/07/17 16:1020.0 1.7 1
Anthracene ND ug/L 06/13/17 18:29 120-12-706/07/17 16:1010.0 1.7 1
Benzo(a)anthracene ND ug/L 06/13/17 18:29 56-55-306/07/17 16:1010.0 2.1 1
Benzo(a)pyrene ND ug/L 06/13/17 18:29 50-32-806/07/17 16:1010.0 2.2 1
Benzo(b)fluoranthene ND ug/L 06/13/17 18:29 205-99-206/07/17 16:1010.0 2.2 1
Benzo(g,h,i)perylene ND ug/L 06/13/17 18:29 191-24-206/07/17 16:1010.0 2.1 1
Benzo(k)fluoranthene ND ug/L 06/13/17 18:29 207-08-906/07/17 16:1010.0 2.0 1
Benzyl alcohol ND ug/L 06/13/17 18:29 100-51-6 L206/07/17 16:1020.0 3.1 1
4-Bromophenylphenyl ether ND ug/L 06/13/17 18:29 101-55-306/07/17 16:1010.0 1.5 1
Butylbenzylphthalate ND ug/L 06/13/17 18:29 85-68-706/07/17 16:1010.0 2.5 1
4-Chloro-3-methylphenol ND ug/L 06/13/17 18:29 59-50-706/07/17 16:1020.0 2.8 1
4-Chloroaniline ND ug/L 06/13/17 18:29 106-47-806/07/17 16:1020.0 2.8 1
Chlorobenzilate ND ug/L 06/13/17 18:29 510-15-606/07/17 16:1010.0 2.2 1
bis(2-Chloroethoxy)methane ND ug/L 06/13/17 18:29 111-91-1 L206/07/17 16:1010.0 1.6 1
bis(2-Chloroethyl) ether ND ug/L 06/13/17 18:29 111-44-4 L206/07/17 16:1010.0 1.7 1
2-Chloronaphthalene ND ug/L 06/13/17 18:29 91-58-7 L206/07/17 16:1010.0 1.6 1
2-Chlorophenol ND ug/L 06/13/17 18:29 95-57-8 L206/07/17 16:1010.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/13/17 18:29 7005-72-306/07/17 16:1010.0 1.6 1
Chrysene ND ug/L 06/13/17 18:29 218-01-906/07/17 16:1010.0 2.1 1
Diallate ND ug/L 06/13/17 18:29 2303-16-406/07/17 16:1010.0 1.6 1
Dibenz(a,h)anthracene ND ug/L 06/13/17 18:29 53-70-306/07/17 16:1010.0 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 73 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-10 Lab ID:92342479011 Collected:05/31/17 13:05 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Dibenzofuran ND ug/L 06/13/17 18:29 132-64-906/07/17 16:1010.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 06/13/17 18:29 91-94-106/07/17 16:1020.0 3.9 1
2,4-Dichlorophenol ND ug/L 06/13/17 18:29 120-83-2 L206/07/17 16:1010.0 1.6 1
2,6-Dichlorophenol ND ug/L 06/13/17 18:29 87-65-0 L206/07/17 16:1010.0 1.5 1
Diethylphthalate ND ug/L 06/13/17 18:29 84-66-206/07/17 16:1060001.6 1
Dimethoate ND ug/L 06/13/17 18:29 60-51-506/07/17 16:1020.0 1.8 1
P-Dimethylaminoazobenzene ND ug/L 06/13/17 18:29 60-11-706/07/17 16:1010.0 1.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/13/17 18:29 57-97-606/07/17 16:1010.0 2.4 1
3,3'-Dimethylbenzidine ND ug/L 06/13/17 18:29 119-93-706/07/17 16:1010.0 3.9 1
2,4-Dimethylphenol ND ug/L 06/13/17 18:29 105-67-9 L206/07/17 16:1010.0 1.6 1
Dimethylphthalate ND ug/L 06/13/17 18:29 131-11-306/07/17 16:1010.0 1.4 1
Di-n-butylphthalate ND ug/L 06/13/17 18:29 84-74-206/07/17 16:1010.0 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/13/17 18:29 534-52-106/07/17 16:1050.0 2.2 1
1,3-Dinitrobenzene ND ug/L 06/13/17 18:29 99-65-006/07/17 16:1020.0 1.3 1
2,4-Dinitrophenol ND ug/L 06/13/17 18:29 51-28-506/07/17 16:1050.0 5.1 1
2,4-Dinitrotoluene ND ug/L 06/13/17 18:29 121-14-206/07/17 16:1010.0 1.5 1
2,6-Dinitrotoluene ND ug/L 06/13/17 18:29 606-20-206/07/17 16:1010.0 1.4 1
Di-n-octylphthalate ND ug/L 06/13/17 18:29 117-84-006/07/17 16:1010.0 1.5 1
Diphenylamine ND ug/L 06/13/17 18:29 122-39-406/07/17 16:1010.0 1.4 1
Disulfoton ND ug/L 06/13/17 18:29 298-04-406/07/17 16:1010.0 1.5 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/13/17 18:29 117-81-706/07/17 16:1015.0 2.3 1
Ethyl methanesulfonate ND ug/L 06/13/17 18:29 62-50-0 L206/07/17 16:1020.0 1.6 1
Famphur ND ug/L 06/13/17 18:29 52-85-706/07/17 16:1020.0 5.7 1
Fluoranthene ND ug/L 06/13/17 18:29 206-44-006/07/17 16:1010.0 2.2 1
Fluorene ND ug/L 06/13/17 18:29 86-73-706/07/17 16:1010.0 1.6 1
Hexachlorobenzene ND ug/L 06/13/17 18:29 118-74-106/07/17 16:1010.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 06/13/17 18:29 77-47-4 L206/07/17 16:1010.0 1.3 1
Hexachloroethane ND ug/L 06/13/17 18:29 67-72-1 L206/07/17 16:1010.0 1.8 1
Hexachloropropene ND ug/L 06/13/17 18:29 1888-71-706/07/17 16:1010.0 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/13/17 18:29 193-39-506/07/17 16:1010.0 2.0 1
Isodrin ND ug/L 06/13/17 18:29 465-73-606/07/17 16:1020.0 2.5 1
Isophorone ND ug/L 06/13/17 18:29 78-59-1 L206/07/17 16:1010.0 1.5 1
Isosafrole ND ug/L 06/13/17 18:29 120-58-1 L206/07/17 16:1010.0 1.5 1
Kepone ND ug/L 06/13/17 18:29 143-50-006/07/17 16:1020.0 4.5 1
Methapyrilene ND ug/L 06/13/17 18:29 91-80-506/07/17 16:101003.0 1
3-Methylcholanthrene ND ug/L 06/13/17 18:29 56-49-506/07/17 16:1010.0 2.7 1
Methyl methanesulfonate ND ug/L 06/13/17 18:29 66-27-306/07/17 16:1010.0 1.1 1
2-Methylnaphthalene ND ug/L 06/13/17 18:29 91-57-6 L206/07/17 16:1010.0 1.4 1
Methyl parathion ND ug/L 06/13/17 18:29 298-00-006/07/17 16:1010.0 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 06/13/17 18:29 95-48-7 L206/07/17 16:1010.0 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/13/17 18:29 15831-10-4 L206/07/17 16:1010.0 1.4 1
1-Naphthalenamine ND ug/L 06/13/17 18:29 134-32-706/07/17 16:1010.0 1.3 1
2-Naphthalenamine ND ug/L 06/13/17 18:29 91-59-806/07/17 16:1010.0 2.2 1
1,4-Naphthoquinone ND ug/L 06/13/17 18:29 130-15-406/07/17 16:1010.0 0.99 1
2-Nitroaniline ND ug/L 06/13/17 18:29 88-74-406/07/17 16:1050.0 2.3 1
3-Nitroaniline ND ug/L 06/13/17 18:29 99-09-206/07/17 16:1050.0 2.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 74 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-10 Lab ID:92342479011 Collected:05/31/17 13:05 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Nitroaniline ND ug/L 06/13/17 18:29 100-01-606/07/17 16:1020.0 3.4 1
Nitrobenzene ND ug/L 06/13/17 18:29 98-95-3 L206/07/17 16:1010.0 1.6 1
2-Nitrophenol ND ug/L 06/13/17 18:29 88-75-5 L206/07/17 16:1010.0 1.6 1
4-Nitrophenol ND ug/L 06/13/17 18:29 100-02-706/07/17 16:1050.0 4.3 1
5-Nitro-o-toluidine ND ug/L 06/13/17 18:29 99-55-8 L206/07/17 16:1010.0 1.9 1
N-Nitrosodiethylamine ND ug/L 06/13/17 18:29 55-18-5 L206/07/17 16:1020.0 1.4 1
N-Nitrosodimethylamine ND ug/L 06/13/17 18:29 62-75-906/07/17 16:1010.0 1.6 1
N-Nitroso-di-n-butylamine ND ug/L 06/13/17 18:29 924-16-3 L206/07/17 16:1010.0 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 06/13/17 18:29 621-64-7 L206/07/17 16:1010.0 1.7 1
N-Nitrosodiphenylamine ND ug/L 06/13/17 18:29 86-30-606/07/17 16:1010.0 1.4 1
N-Nitrosomethylethylamine ND ug/L 06/13/17 18:29 10595-95-6 L206/07/17 16:1010.0 1.4 1
N-Nitrosopiperidine ND ug/L 06/13/17 18:29 100-75-4 L206/07/17 16:1020.0 1.7 1
N-Nitrosopyrrolidine ND ug/L 06/13/17 18:29 930-55-2 L206/07/17 16:1010.0 1.7 1
O,O,O-Triethylphosphorothioate ND ug/L 06/13/17 18:29 126-68-1 L206/07/17 16:1010.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/13/17 18:29 108-60-106/07/17 16:1010.0 1.8 1
Parathion (Ethyl parathion)ND ug/L 06/13/17 18:29 56-38-2 L206/07/17 16:1010.0 1.5 1
Pentachlorobenzene ND ug/L 06/13/17 18:29 608-93-506/07/17 16:1010.0 1.5 1
Pentachloronitrobenzene ND ug/L 06/13/17 18:29 82-68-806/07/17 16:1020.0 1.7 1
Pentachlorophenol ND ug/L 06/13/17 18:29 87-86-506/07/17 16:1025.0 3.5 1
Phenacetin ND ug/L 06/13/17 18:29 62-44-206/07/17 16:1020.0 1.9 1
Phenanthrene ND ug/L 06/13/17 18:29 85-01-806/07/17 16:1010.0 1.6 1
Phenol ND ug/L 06/13/17 18:29 108-95-206/07/17 16:1010.0 1.3 1
p-Phenylenediamine ND ug/L 06/13/17 18:29 106-50-3 L206/07/17 16:1010.0 2.2 1
Phorate ND ug/L 06/13/17 18:29 298-02-2 L206/07/17 16:1010.0 1.7 1
Pronamide ND ug/L 06/13/17 18:29 23950-58-5 L206/07/17 16:1010.0 2.0 1
Pyrene ND ug/L 06/13/17 18:29 129-00-006/07/17 16:1010.0 2.2 1
Safrole ND ug/L 06/13/17 18:29 94-59-7 L206/07/17 16:1010.0 1.3 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/13/17 18:29 95-94-306/07/17 16:1010.0 1.3 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/13/17 18:29 58-90-206/07/17 16:1010.0 2.9 1
Thionazin ND ug/L 06/13/17 18:29 297-97-2 L206/07/17 16:1020.0 1.7 1
O-Toluidine ND ug/L 06/13/17 18:29 95-53-4 L206/07/17 16:1010.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 06/13/17 18:29 95-95-406/07/17 16:1010.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/13/17 18:29 88-06-206/07/17 16:1010.0 1.4 1
1,3,5-Trinitrobenzene ND ug/L 06/13/17 18:29 99-35-4 L206/07/17 16:1010.0 1.2 1
Surrogates
Nitrobenzene-d5 (S)31 %06/13/17 18:29 4165-60-0 1g06/07/17 16:1021-110 1
2-Fluorobiphenyl (S)33 %06/13/17 18:29 321-60-806/07/17 16:1027-110 1
Terphenyl-d14 (S)65 %06/13/17 18:29 1718-51-006/07/17 16:1031-107 1
Phenol-d6 (S)18 %06/13/17 18:29 13127-88-306/07/17 16:1010-110 1
2-Fluorophenol (S)24 %06/13/17 18:29 367-12-406/07/17 16:1012-110 1
2,4,6-Tribromophenol (S)46 %06/13/17 18:29 118-79-606/07/17 16:1027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 13.4J ug/L 06/02/17 05:15 67-64-110010.0 1
Acetonitrile ND ug/L 06/02/17 05:15 75-05-855.0 2.2 1
Acrolein ND ug/L 06/02/17 05:15 107-02-853.0 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 75 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-10 Lab ID:92342479011 Collected:05/31/17 13:05 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acrylonitrile ND ug/L 06/02/17 05:15 107-13-12001.9 1
Allyl chloride ND ug/L 06/02/17 05:15 107-05-110.0 1.5 1
Benzene 0.48J ug/L 06/02/17 05:15 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/02/17 05:15 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/02/17 05:15 75-27-41.0 0.18 1
Bromoform ND ug/L 06/02/17 05:15 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/02/17 05:15 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/02/17 05:15 78-93-31000.96 1
Carbon disulfide ND ug/L 06/02/17 05:15 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/02/17 05:15 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/02/17 05:15 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/02/17 05:15 75-00-310.0 0.54 1
Chloroform ND ug/L 06/02/17 05:15 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/02/17 05:15 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/02/17 05:15 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/02/17 05:15 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/02/17 05:15 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/02/17 05:15 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/02/17 05:15 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/02/17 05:15 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/02/17 05:15 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/02/17 05:15 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/02/17 05:15 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/02/17 05:15 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/02/17 05:15 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/02/17 05:15 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/02/17 05:15 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.83J ug/L 06/02/17 05:15 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/02/17 05:15 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/02/17 05:15 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/02/17 05:15 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/02/17 05:15 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/02/17 05:15 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/02/17 05:15 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/02/17 05:15 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/02/17 05:15 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/02/17 05:15 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/02/17 05:15 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/02/17 05:15 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/02/17 05:15 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/02/17 05:15 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/02/17 05:15 126-98-71000.93 1
Methylene Chloride ND ug/L 06/02/17 05:15 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/02/17 05:15 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/02/17 05:15 108-10-11000.33 1
Naphthalene ND ug/L 06/02/17 05:15 91-20-310.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
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Page 76 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-10 Lab ID:92342479011 Collected:05/31/17 13:05 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Propionitrile ND ug/L 06/02/17 05:15 107-12-01503.6 1
Styrene ND ug/L 06/02/17 05:15 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/02/17 05:15 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/02/17 05:15 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/02/17 05:15 127-18-41.0 0.46 1
Toluene ND ug/L 06/02/17 05:15 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/02/17 05:15 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/02/17 05:15 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/02/17 05:15 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/02/17 05:15 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/02/17 05:15 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/02/17 05:15 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/02/17 05:15 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/02/17 05:15 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/02/17 05:15 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)112 %06/02/17 05:15 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %06/02/17 05:15 17060-07-070-130 1
Toluene-d8 (S)111 %06/02/17 05:15 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/01/17 21:00 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/01/17 17:38 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 77 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-11S Lab ID:92342479012 Collected:05/31/17 12:30 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/06/17 19:30 309-00-206/02/17 10:090.050 0.050 1
alpha-BHC ND ug/L 06/06/17 19:30 319-84-606/02/17 10:090.050 0.050 1
beta-BHC ND ug/L 06/06/17 19:30 319-85-706/02/17 10:090.050 0.050 1
delta-BHC ND ug/L 06/06/17 19:30 319-86-806/02/17 10:090.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/06/17 19:30 58-89-906/02/17 10:090.050 0.050 1
Chlordane (Technical)ND ug/L 06/06/17 19:30 57-74-906/02/17 10:090.50 0.20 1
4,4'-DDD ND ug/L 06/06/17 19:30 72-54-806/02/17 10:090.10 0.050 1
4,4'-DDE ND ug/L 06/06/17 19:30 72-55-906/02/17 10:090.10 0.050 1
4,4'-DDT ND ug/L 06/06/17 19:30 50-29-306/02/17 10:090.10 0.050 1
Dieldrin ND ug/L 06/06/17 19:30 60-57-106/02/17 10:090.075 0.050 1
Endosulfan I ND ug/L 06/06/17 19:30 959-98-806/02/17 10:090.10 0.050 1
Endosulfan II ND ug/L 06/06/17 19:30 33213-65-906/02/17 10:090.10 0.050 1
Endosulfan sulfate ND ug/L 06/06/17 19:30 1031-07-806/02/17 10:090.10 0.050 1
Endrin ND ug/L 06/06/17 19:30 72-20-806/02/17 10:090.10 0.050 1
Endrin aldehyde ND ug/L 06/06/17 19:30 7421-93-406/02/17 10:090.10 0.050 1
Heptachlor ND ug/L 06/06/17 19:30 76-44-806/02/17 10:090.050 0.050 1
Heptachlor epoxide ND ug/L 06/06/17 19:30 1024-57-306/02/17 10:090.075 0.050 1
Methoxychlor ND ug/L 06/06/17 19:30 72-43-506/02/17 10:091.0 0.15 1
Toxaphene ND ug/L 06/06/17 19:30 8001-35-206/02/17 10:091.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)52 %06/06/17 19:30 877-09-806/02/17 10:0920-130 1
Decachlorobiphenyl (S)78 %06/06/17 19:30 2051-24-306/02/17 10:0920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/02/17 20:13 12674-11-206/02/17 10:090.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/02/17 20:13 11104-28-206/02/17 10:090.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/02/17 20:13 11141-16-506/02/17 10:090.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/02/17 20:13 53469-21-906/02/17 10:090.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/02/17 20:13 12672-29-606/02/17 10:090.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/02/17 20:13 11097-69-106/02/17 10:090.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/02/17 20:13 11096-82-506/02/17 10:090.50 0.50 1
Surrogates
Decachlorobiphenyl (S)71 %06/02/17 20:13 2051-24-306/02/17 10:0910-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/07/17 08:00 94-75-7 L106/05/17 16:500.99 0.24 1
Dinoseb ND ug/L 06/07/17 08:00 88-85-7 L106/05/17 16:500.20 0.060 1
Pentachlorophenol ND ug/L 06/07/17 08:00 87-86-506/05/17 16:500.030 0.018 1
2,4,5-T ND ug/L 06/07/17 08:00 93-76-506/05/17 16:500.20 0.044 1
2,4,5-TP (Silvex)ND ug/L 06/07/17 08:00 93-72-106/05/17 16:500.20 0.051 1
Surrogates
2,4-DCAA (S)87 %06/07/17 08:00 19719-28-906/05/17 16:5039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/09/17 16:30 7440-36-006/02/17 15:206.0 3.9 1
Arsenic ND ug/L 06/09/17 16:30 7440-38-206/02/17 15:2010.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 78 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-11S Lab ID:92342479012 Collected:05/31/17 12:30 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Barium 15.5J ug/L 06/09/17 16:30 7440-39-306/02/17 15:201002.5 1
Beryllium ND ug/L 06/09/17 16:30 7440-41-706/02/17 15:201.0 0.50 1
Cadmium ND ug/L 06/09/17 16:30 7440-43-906/02/17 15:201.0 0.50 1
Chromium ND ug/L 06/09/17 16:30 7440-47-306/02/17 15:2010.0 2.5 1
Cobalt ND ug/L 06/09/17 16:30 7440-48-406/02/17 15:2010.0 2.5 1
Copper ND ug/L 06/09/17 16:30 7440-50-806/02/17 15:2010.0 2.5 1
Lead ND ug/L 06/09/17 16:30 7439-92-106/02/17 15:2010.0 2.5 1
Nickel ND ug/L 06/09/17 16:30 7440-02-006/02/17 15:2050.0 2.5 1
Selenium ND ug/L 06/09/17 16:30 7782-49-206/02/17 15:2010.0 5.0 1
Silver ND ug/L 06/09/17 16:30 7440-22-406/02/17 15:2010.0 2.5 1
Tin ND ug/L 06/09/17 16:30 7440-31-506/02/17 15:201002.5 1
Vanadium ND ug/L 06/09/17 16:30 7440-62-206/02/17 15:2025.0 2.5 1
Zinc ND ug/L 06/09/17 16:30 7440-66-606/02/17 15:2010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/06/17 17:13 7440-28-006/01/17 11:305.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 02:32 7439-97-606/04/17 20:450.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/14/17 21:25 83-32-906/07/17 16:1010.0 1.6 1
Acenaphthylene ND ug/L 06/14/17 21:25 208-96-806/07/17 16:1010.0 1.5 1
Acetophenone ND ug/L 06/14/17 21:25 98-86-206/07/17 16:1010.0 1.9 1
2-Acetylaminofluorene ND ug/L 06/14/17 21:25 53-96-306/07/17 16:1020.0 1.6 1
4-Aminobiphenyl ND ug/L 06/14/17 21:25 92-67-106/07/17 16:1020.0 1.7 1
Anthracene ND ug/L 06/14/17 21:25 120-12-706/07/17 16:1010.0 1.7 1
Benzo(a)anthracene ND ug/L 06/14/17 21:25 56-55-306/07/17 16:1010.0 2.1 1
Benzo(a)pyrene ND ug/L 06/14/17 21:25 50-32-806/07/17 16:1010.0 2.2 1
Benzo(b)fluoranthene ND ug/L 06/14/17 21:25 205-99-206/07/17 16:1010.0 2.2 1
Benzo(g,h,i)perylene ND ug/L 06/14/17 21:25 191-24-206/07/17 16:1010.0 2.1 1
Benzo(k)fluoranthene ND ug/L 06/14/17 21:25 207-08-906/07/17 16:1010.0 2.0 1
Benzyl alcohol ND ug/L 06/14/17 21:25 100-51-606/07/17 16:1020.0 3.1 1
4-Bromophenylphenyl ether ND ug/L 06/14/17 21:25 101-55-306/07/17 16:1010.0 1.5 1
Butylbenzylphthalate ND ug/L 06/14/17 21:25 85-68-706/07/17 16:1010.0 2.5 1
4-Chloro-3-methylphenol ND ug/L 06/14/17 21:25 59-50-706/07/17 16:1020.0 2.8 1
4-Chloroaniline ND ug/L 06/14/17 21:25 106-47-806/07/17 16:1020.0 2.8 1
Chlorobenzilate ND ug/L 06/14/17 21:25 510-15-606/07/17 16:1010.0 2.2 1
bis(2-Chloroethoxy)methane ND ug/L 06/14/17 21:25 111-91-106/07/17 16:1010.0 1.6 1
bis(2-Chloroethyl) ether ND ug/L 06/14/17 21:25 111-44-406/07/17 16:1010.0 1.7 1
2-Chloronaphthalene ND ug/L 06/14/17 21:25 91-58-706/07/17 16:1010.0 1.6 1
2-Chlorophenol ND ug/L 06/14/17 21:25 95-57-806/07/17 16:1010.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/14/17 21:25 7005-72-306/07/17 16:1010.0 1.6 1
Chrysene ND ug/L 06/14/17 21:25 218-01-906/07/17 16:1010.0 2.1 1
Diallate ND ug/L 06/14/17 21:25 2303-16-406/07/17 16:1010.0 1.6 1
Dibenz(a,h)anthracene ND ug/L 06/14/17 21:25 53-70-306/07/17 16:1010.0 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 79 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-11S Lab ID:92342479012 Collected:05/31/17 12:30 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Dibenzofuran ND ug/L 06/14/17 21:25 132-64-906/07/17 16:1010.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 06/14/17 21:25 91-94-106/07/17 16:1020.0 3.9 1
2,4-Dichlorophenol ND ug/L 06/14/17 21:25 120-83-206/07/17 16:1010.0 1.6 1
2,6-Dichlorophenol ND ug/L 06/14/17 21:25 87-65-006/07/17 16:1010.0 1.5 1
Diethylphthalate ND ug/L 06/14/17 21:25 84-66-206/07/17 16:1060001.6 1
Dimethoate ND ug/L 06/14/17 21:25 60-51-506/07/17 16:1020.0 1.8 1
P-Dimethylaminoazobenzene ND ug/L 06/14/17 21:25 60-11-706/07/17 16:1010.0 1.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/14/17 21:25 57-97-606/07/17 16:1010.0 2.4 1
3,3'-Dimethylbenzidine ND ug/L 06/14/17 21:25 119-93-706/07/17 16:1010.0 3.9 1
2,4-Dimethylphenol ND ug/L 06/14/17 21:25 105-67-906/07/17 16:1010.0 1.6 1
Dimethylphthalate ND ug/L 06/14/17 21:25 131-11-306/07/17 16:1010.0 1.4 1
Di-n-butylphthalate ND ug/L 06/14/17 21:25 84-74-206/07/17 16:1010.0 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/14/17 21:25 534-52-106/07/17 16:1050.0 2.2 1
1,3-Dinitrobenzene ND ug/L 06/14/17 21:25 99-65-006/07/17 16:1020.0 1.3 1
2,4-Dinitrophenol ND ug/L 06/14/17 21:25 51-28-506/07/17 16:1050.0 5.1 1
2,4-Dinitrotoluene ND ug/L 06/14/17 21:25 121-14-206/07/17 16:1010.0 1.5 1
2,6-Dinitrotoluene ND ug/L 06/14/17 21:25 606-20-206/07/17 16:1010.0 1.4 1
Di-n-octylphthalate ND ug/L 06/14/17 21:25 117-84-006/07/17 16:1010.0 1.5 1
Diphenylamine ND ug/L 06/14/17 21:25 122-39-406/07/17 16:1010.0 1.4 1
Disulfoton ND ug/L 06/14/17 21:25 298-04-406/07/17 16:1010.0 1.5 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/14/17 21:25 117-81-706/07/17 16:1015.0 2.3 1
Ethyl methanesulfonate ND ug/L 06/14/17 21:25 62-50-006/07/17 16:1020.0 1.6 1
Famphur ND ug/L 06/14/17 21:25 52-85-706/07/17 16:1020.0 5.7 1
Fluoranthene ND ug/L 06/14/17 21:25 206-44-006/07/17 16:1010.0 2.2 1
Fluorene ND ug/L 06/14/17 21:25 86-73-706/07/17 16:1010.0 1.6 1
Hexachlorobenzene ND ug/L 06/14/17 21:25 118-74-106/07/17 16:1010.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 06/14/17 21:25 77-47-406/07/17 16:1010.0 1.3 1
Hexachloroethane ND ug/L 06/14/17 21:25 67-72-106/07/17 16:1010.0 1.8 1
Hexachloropropene ND ug/L 06/14/17 21:25 1888-71-706/07/17 16:1010.0 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/14/17 21:25 193-39-506/07/17 16:1010.0 2.0 1
Isodrin ND ug/L 06/14/17 21:25 465-73-606/07/17 16:1020.0 2.5 1
Isophorone ND ug/L 06/14/17 21:25 78-59-106/07/17 16:1010.0 1.5 1
Isosafrole ND ug/L 06/14/17 21:25 120-58-106/07/17 16:1010.0 1.5 1
Kepone ND ug/L 06/14/17 21:25 143-50-006/07/17 16:1020.0 4.5 1
Methapyrilene ND ug/L 06/14/17 21:25 91-80-506/07/17 16:101003.0 1
3-Methylcholanthrene ND ug/L 06/14/17 21:25 56-49-506/07/17 16:1010.0 2.7 1
Methyl methanesulfonate ND ug/L 06/14/17 21:25 66-27-306/07/17 16:1010.0 1.1 1
2-Methylnaphthalene ND ug/L 06/14/17 21:25 91-57-606/07/17 16:1010.0 1.4 1
Methyl parathion ND ug/L 06/14/17 21:25 298-00-006/07/17 16:1010.0 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 06/14/17 21:25 95-48-706/07/17 16:1010.0 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/14/17 21:25 15831-10-406/07/17 16:1010.0 1.4 1
1-Naphthalenamine ND ug/L 06/14/17 21:25 134-32-706/07/17 16:1010.0 1.3 1
2-Naphthalenamine ND ug/L 06/14/17 21:25 91-59-806/07/17 16:1010.0 2.2 1
1,4-Naphthoquinone ND ug/L 06/14/17 21:25 130-15-406/07/17 16:1010.0 0.99 1
2-Nitroaniline ND ug/L 06/14/17 21:25 88-74-406/07/17 16:1050.0 2.3 1
3-Nitroaniline ND ug/L 06/14/17 21:25 99-09-206/07/17 16:1050.0 2.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 80 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-11S Lab ID:92342479012 Collected:05/31/17 12:30 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Nitroaniline ND ug/L 06/14/17 21:25 100-01-606/07/17 16:1020.0 3.4 1
Nitrobenzene ND ug/L 06/14/17 21:25 98-95-306/07/17 16:1010.0 1.6 1
2-Nitrophenol ND ug/L 06/14/17 21:25 88-75-506/07/17 16:1010.0 1.6 1
4-Nitrophenol ND ug/L 06/14/17 21:25 100-02-706/07/17 16:1050.0 4.3 1
5-Nitro-o-toluidine ND ug/L 06/14/17 21:25 99-55-806/07/17 16:1010.0 1.9 1
N-Nitrosodiethylamine ND ug/L 06/14/17 21:25 55-18-506/07/17 16:1020.0 1.4 1
N-Nitrosodimethylamine ND ug/L 06/14/17 21:25 62-75-906/07/17 16:1010.0 1.6 1
N-Nitroso-di-n-butylamine ND ug/L 06/14/17 21:25 924-16-306/07/17 16:1010.0 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 06/14/17 21:25 621-64-706/07/17 16:1010.0 1.7 1
N-Nitrosodiphenylamine ND ug/L 06/14/17 21:25 86-30-606/07/17 16:1010.0 1.4 1
N-Nitrosomethylethylamine ND ug/L 06/14/17 21:25 10595-95-606/07/17 16:1010.0 1.4 1
N-Nitrosopiperidine ND ug/L 06/14/17 21:25 100-75-406/07/17 16:1020.0 1.7 1
N-Nitrosopyrrolidine ND ug/L 06/14/17 21:25 930-55-206/07/17 16:1010.0 1.7 1
O,O,O-Triethylphosphorothioate ND ug/L 06/14/17 21:25 126-68-106/07/17 16:1010.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/14/17 21:25 108-60-106/07/17 16:1010.0 1.8 1
Parathion (Ethyl parathion)ND ug/L 06/14/17 21:25 56-38-206/07/17 16:1010.0 1.5 1
Pentachlorobenzene ND ug/L 06/14/17 21:25 608-93-506/07/17 16:1010.0 1.5 1
Pentachloronitrobenzene ND ug/L 06/14/17 21:25 82-68-806/07/17 16:1020.0 1.7 1
Pentachlorophenol ND ug/L 06/14/17 21:25 87-86-506/07/17 16:1025.0 3.5 1
Phenacetin ND ug/L 06/14/17 21:25 62-44-206/07/17 16:1020.0 1.9 1
Phenanthrene ND ug/L 06/14/17 21:25 85-01-806/07/17 16:1010.0 1.6 1
Phenol ND ug/L 06/14/17 21:25 108-95-206/07/17 16:1010.0 1.3 1
p-Phenylenediamine ND ug/L 06/14/17 21:25 106-50-306/07/17 16:1010.0 2.2 1
Phorate ND ug/L 06/14/17 21:25 298-02-206/07/17 16:1010.0 1.7 1
Pronamide ND ug/L 06/14/17 21:25 23950-58-506/07/17 16:1010.0 2.0 1
Pyrene ND ug/L 06/14/17 21:25 129-00-006/07/17 16:1010.0 2.2 1
Safrole ND ug/L 06/14/17 21:25 94-59-706/07/17 16:1010.0 1.3 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/14/17 21:25 95-94-306/07/17 16:1010.0 1.3 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/14/17 21:25 58-90-206/07/17 16:1010.0 2.9 1
Thionazin ND ug/L 06/14/17 21:25 297-97-206/07/17 16:1020.0 1.7 1
O-Toluidine ND ug/L 06/14/17 21:25 95-53-406/07/17 16:1010.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 06/14/17 21:25 95-95-406/07/17 16:1010.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/14/17 21:25 88-06-206/07/17 16:1010.0 1.4 1
1,3,5-Trinitrobenzene ND ug/L 06/14/17 21:25 99-35-406/07/17 16:1010.0 1.2 1
Surrogates
Nitrobenzene-d5 (S)87 %06/14/17 21:25 4165-60-0 1g06/07/17 16:1021-110 1
2-Fluorobiphenyl (S)96 %06/14/17 21:25 321-60-806/07/17 16:1027-110 1
Terphenyl-d14 (S)104 %06/14/17 21:25 1718-51-006/07/17 16:1031-107 1
Phenol-d6 (S)27 %06/14/17 21:25 13127-88-306/07/17 16:1010-110 1
2-Fluorophenol (S)46 %06/14/17 21:25 367-12-406/07/17 16:1012-110 1
2,4,6-Tribromophenol (S)100 %06/14/17 21:25 118-79-606/07/17 16:1027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/02/17 05:33 67-64-110010.0 1
Acetonitrile ND ug/L 06/02/17 05:33 75-05-855.0 2.2 1
Acrolein ND ug/L 06/02/17 05:33 107-02-853.0 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
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Page 81 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-11S Lab ID:92342479012 Collected:05/31/17 12:30 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acrylonitrile ND ug/L 06/02/17 05:33 107-13-12001.9 1
Allyl chloride ND ug/L 06/02/17 05:33 107-05-110.0 1.5 1
Benzene ND ug/L 06/02/17 05:33 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/02/17 05:33 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/02/17 05:33 75-27-41.0 0.18 1
Bromoform ND ug/L 06/02/17 05:33 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/02/17 05:33 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/02/17 05:33 78-93-31000.96 1
Carbon disulfide ND ug/L 06/02/17 05:33 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/02/17 05:33 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/02/17 05:33 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/02/17 05:33 75-00-310.0 0.54 1
Chloroform ND ug/L 06/02/17 05:33 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/02/17 05:33 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/02/17 05:33 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/02/17 05:33 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/02/17 05:33 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/02/17 05:33 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/02/17 05:33 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/02/17 05:33 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/02/17 05:33 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/02/17 05:33 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/02/17 05:33 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/02/17 05:33 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/02/17 05:33 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/02/17 05:33 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/02/17 05:33 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/02/17 05:33 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/02/17 05:33 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/02/17 05:33 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/02/17 05:33 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/02/17 05:33 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/02/17 05:33 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/02/17 05:33 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/02/17 05:33 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/02/17 05:33 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/02/17 05:33 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/02/17 05:33 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/02/17 05:33 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/02/17 05:33 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/02/17 05:33 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/02/17 05:33 126-98-71000.93 1
Methylene Chloride ND ug/L 06/02/17 05:33 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/02/17 05:33 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/02/17 05:33 108-10-11000.33 1
Naphthalene ND ug/L 06/02/17 05:33 91-20-310.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 82 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-11S Lab ID:92342479012 Collected:05/31/17 12:30 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Propionitrile ND ug/L 06/02/17 05:33 107-12-01503.6 1
Styrene ND ug/L 06/02/17 05:33 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/02/17 05:33 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/02/17 05:33 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/02/17 05:33 127-18-41.0 0.46 1
Toluene ND ug/L 06/02/17 05:33 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/02/17 05:33 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/02/17 05:33 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/02/17 05:33 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/02/17 05:33 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/02/17 05:33 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/02/17 05:33 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/02/17 05:33 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/02/17 05:33 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/02/17 05:33 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)115 %06/02/17 05:33 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %06/02/17 05:33 17060-07-070-130 1
Toluene-d8 (S)110 %06/02/17 05:33 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/06/17 22:15 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/01/17 17:44 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 83 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-11D Lab ID:92342479013 Collected:05/31/17 12:10 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/06/17 19:48 309-00-206/02/17 10:090.050 0.050 1
alpha-BHC ND ug/L 06/06/17 19:48 319-84-606/02/17 10:090.050 0.050 1
beta-BHC ND ug/L 06/06/17 19:48 319-85-706/02/17 10:090.050 0.050 1
delta-BHC ND ug/L 06/06/17 19:48 319-86-806/02/17 10:090.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/06/17 19:48 58-89-906/02/17 10:090.050 0.050 1
Chlordane (Technical)ND ug/L 06/06/17 19:48 57-74-906/02/17 10:090.50 0.20 1
4,4'-DDD ND ug/L 06/06/17 19:48 72-54-806/02/17 10:090.10 0.050 1
4,4'-DDE ND ug/L 06/06/17 19:48 72-55-906/02/17 10:090.10 0.050 1
4,4'-DDT ND ug/L 06/06/17 19:48 50-29-306/02/17 10:090.10 0.050 1
Dieldrin ND ug/L 06/06/17 19:48 60-57-106/02/17 10:090.075 0.050 1
Endosulfan I ND ug/L 06/06/17 19:48 959-98-806/02/17 10:090.10 0.050 1
Endosulfan II ND ug/L 06/06/17 19:48 33213-65-906/02/17 10:090.10 0.050 1
Endosulfan sulfate ND ug/L 06/06/17 19:48 1031-07-806/02/17 10:090.10 0.050 1
Endrin ND ug/L 06/06/17 19:48 72-20-806/02/17 10:090.10 0.050 1
Endrin aldehyde ND ug/L 06/06/17 19:48 7421-93-406/02/17 10:090.10 0.050 1
Heptachlor ND ug/L 06/06/17 19:48 76-44-806/02/17 10:090.050 0.050 1
Heptachlor epoxide ND ug/L 06/06/17 19:48 1024-57-306/02/17 10:090.075 0.050 1
Methoxychlor ND ug/L 06/06/17 19:48 72-43-506/02/17 10:091.0 0.15 1
Toxaphene ND ug/L 06/06/17 19:48 8001-35-206/02/17 10:091.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)74 %06/06/17 19:48 877-09-806/02/17 10:0920-130 1
Decachlorobiphenyl (S)86 %06/06/17 19:48 2051-24-306/02/17 10:0920-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 06/02/17 20:34 12674-11-206/02/17 10:090.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 06/02/17 20:34 11104-28-206/02/17 10:090.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 06/02/17 20:34 11141-16-506/02/17 10:090.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 06/02/17 20:34 53469-21-906/02/17 10:090.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 06/02/17 20:34 12672-29-606/02/17 10:090.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 06/02/17 20:34 11097-69-106/02/17 10:090.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 06/02/17 20:34 11096-82-506/02/17 10:090.50 0.50 1
Surrogates
Decachlorobiphenyl (S)82 %06/02/17 20:34 2051-24-306/02/17 10:0910-132 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/07/17 08:29 94-75-7 L106/05/17 16:500.98 0.23 1
Dinoseb ND ug/L 06/07/17 08:29 88-85-7 L106/05/17 16:500.20 0.059 1
Pentachlorophenol ND ug/L 06/07/17 08:29 87-86-506/05/17 16:500.029 0.018 1
2,4,5-T ND ug/L 06/07/17 08:29 93-76-506/05/17 16:500.20 0.044 1
2,4,5-TP (Silvex)ND ug/L 06/07/17 08:29 93-72-106/05/17 16:500.20 0.051 1
Surrogates
2,4-DCAA (S)103 %06/07/17 08:29 19719-28-906/05/17 16:5039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/09/17 17:01 7440-36-006/02/17 15:206.0 3.9 1
Arsenic ND ug/L 06/09/17 17:01 7440-38-206/02/17 15:2010.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 84 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-11D Lab ID:92342479013 Collected:05/31/17 12:10 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Barium 3.2J ug/L 06/09/17 17:01 7440-39-306/02/17 15:201002.5 1
Beryllium ND ug/L 06/09/17 17:01 7440-41-706/02/17 15:201.0 0.50 1
Cadmium ND ug/L 06/09/17 17:01 7440-43-906/02/17 15:201.0 0.50 1
Chromium ND ug/L 06/09/17 17:01 7440-47-306/02/17 15:2010.0 2.5 1
Cobalt ND ug/L 06/09/17 17:01 7440-48-406/02/17 15:2010.0 2.5 1
Copper ND ug/L 06/09/17 17:01 7440-50-806/02/17 15:2010.0 2.5 1
Lead ND ug/L 06/09/17 17:01 7439-92-106/02/17 15:2010.0 2.5 1
Nickel ND ug/L 06/09/17 17:01 7440-02-006/02/17 15:2050.0 2.5 1
Selenium ND ug/L 06/09/17 17:01 7782-49-206/02/17 15:2010.0 5.0 1
Silver ND ug/L 06/09/17 17:01 7440-22-406/02/17 15:2010.0 2.5 1
Tin ND ug/L 06/09/17 17:01 7440-31-506/02/17 15:201002.5 1
Vanadium 10.2J ug/L 06/09/17 17:01 7440-62-206/02/17 15:2025.0 2.5 1
Zinc ND ug/L 06/09/17 17:01 7440-66-606/02/17 15:2010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/06/17 17:15 7440-28-006/01/17 11:305.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 02:34 7439-97-606/04/17 20:450.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/13/17 19:55 83-32-906/07/17 16:1010.0 1.6 1
Acenaphthylene ND ug/L 06/13/17 19:55 208-96-806/07/17 16:1010.0 1.5 1
Acetophenone ND ug/L 06/13/17 19:55 98-86-206/07/17 16:1010.0 1.9 1
2-Acetylaminofluorene ND ug/L 06/13/17 19:55 53-96-3 L206/07/17 16:1020.0 1.6 1
4-Aminobiphenyl ND ug/L 06/13/17 19:55 92-67-106/07/17 16:1020.0 1.7 1
Anthracene ND ug/L 06/13/17 19:55 120-12-706/07/17 16:1010.0 1.7 1
Benzo(a)anthracene ND ug/L 06/13/17 19:55 56-55-306/07/17 16:1010.0 2.1 1
Benzo(a)pyrene ND ug/L 06/13/17 19:55 50-32-806/07/17 16:1010.0 2.2 1
Benzo(b)fluoranthene ND ug/L 06/13/17 19:55 205-99-206/07/17 16:1010.0 2.2 1
Benzo(g,h,i)perylene ND ug/L 06/13/17 19:55 191-24-206/07/17 16:1010.0 2.1 1
Benzo(k)fluoranthene ND ug/L 06/13/17 19:55 207-08-906/07/17 16:1010.0 2.0 1
Benzyl alcohol ND ug/L 06/13/17 19:55 100-51-6 L206/07/17 16:1020.0 3.1 1
4-Bromophenylphenyl ether ND ug/L 06/13/17 19:55 101-55-306/07/17 16:1010.0 1.5 1
Butylbenzylphthalate ND ug/L 06/13/17 19:55 85-68-706/07/17 16:1010.0 2.5 1
4-Chloro-3-methylphenol ND ug/L 06/13/17 19:55 59-50-706/07/17 16:1020.0 2.8 1
4-Chloroaniline ND ug/L 06/13/17 19:55 106-47-806/07/17 16:1020.0 2.8 1
Chlorobenzilate ND ug/L 06/13/17 19:55 510-15-606/07/17 16:1010.0 2.2 1
bis(2-Chloroethoxy)methane ND ug/L 06/13/17 19:55 111-91-1 L206/07/17 16:1010.0 1.6 1
bis(2-Chloroethyl) ether ND ug/L 06/13/17 19:55 111-44-4 L206/07/17 16:1010.0 1.7 1
2-Chloronaphthalene ND ug/L 06/13/17 19:55 91-58-7 L206/07/17 16:1010.0 1.6 1
2-Chlorophenol ND ug/L 06/13/17 19:55 95-57-8 L206/07/17 16:1010.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/13/17 19:55 7005-72-306/07/17 16:1010.0 1.6 1
Chrysene ND ug/L 06/13/17 19:55 218-01-906/07/17 16:1010.0 2.1 1
Diallate ND ug/L 06/13/17 19:55 2303-16-406/07/17 16:1010.0 1.6 1
Dibenz(a,h)anthracene ND ug/L 06/13/17 19:55 53-70-306/07/17 16:1010.0 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 85 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-11D Lab ID:92342479013 Collected:05/31/17 12:10 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Dibenzofuran ND ug/L 06/13/17 19:55 132-64-906/07/17 16:1010.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 06/13/17 19:55 91-94-106/07/17 16:1020.0 3.9 1
2,4-Dichlorophenol ND ug/L 06/13/17 19:55 120-83-2 L206/07/17 16:1010.0 1.6 1
2,6-Dichlorophenol ND ug/L 06/13/17 19:55 87-65-0 L206/07/17 16:1010.0 1.5 1
Diethylphthalate ND ug/L 06/13/17 19:55 84-66-206/07/17 16:1060001.6 1
Dimethoate ND ug/L 06/13/17 19:55 60-51-506/07/17 16:1020.0 1.8 1
P-Dimethylaminoazobenzene ND ug/L 06/13/17 19:55 60-11-706/07/17 16:1010.0 1.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/13/17 19:55 57-97-606/07/17 16:1010.0 2.4 1
3,3'-Dimethylbenzidine ND ug/L 06/13/17 19:55 119-93-706/07/17 16:1010.0 3.9 1
2,4-Dimethylphenol ND ug/L 06/13/17 19:55 105-67-9 L206/07/17 16:1010.0 1.6 1
Dimethylphthalate ND ug/L 06/13/17 19:55 131-11-306/07/17 16:1010.0 1.4 1
Di-n-butylphthalate ND ug/L 06/13/17 19:55 84-74-206/07/17 16:1010.0 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/13/17 19:55 534-52-106/07/17 16:1050.0 2.2 1
1,3-Dinitrobenzene ND ug/L 06/13/17 19:55 99-65-006/07/17 16:1020.0 1.3 1
2,4-Dinitrophenol ND ug/L 06/13/17 19:55 51-28-506/07/17 16:1050.0 5.1 1
2,4-Dinitrotoluene ND ug/L 06/13/17 19:55 121-14-206/07/17 16:1010.0 1.5 1
2,6-Dinitrotoluene ND ug/L 06/13/17 19:55 606-20-206/07/17 16:1010.0 1.4 1
Di-n-octylphthalate ND ug/L 06/13/17 19:55 117-84-006/07/17 16:1010.0 1.5 1
Diphenylamine ND ug/L 06/13/17 19:55 122-39-406/07/17 16:1010.0 1.4 1
Disulfoton ND ug/L 06/13/17 19:55 298-04-406/07/17 16:1010.0 1.5 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/13/17 19:55 117-81-706/07/17 16:1015.0 2.3 1
Ethyl methanesulfonate ND ug/L 06/13/17 19:55 62-50-0 L206/07/17 16:1020.0 1.6 1
Famphur ND ug/L 06/13/17 19:55 52-85-706/07/17 16:1020.0 5.7 1
Fluoranthene ND ug/L 06/13/17 19:55 206-44-006/07/17 16:1010.0 2.2 1
Fluorene ND ug/L 06/13/17 19:55 86-73-706/07/17 16:1010.0 1.6 1
Hexachlorobenzene ND ug/L 06/13/17 19:55 118-74-106/07/17 16:1010.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 06/13/17 19:55 77-47-4 L206/07/17 16:1010.0 1.3 1
Hexachloroethane ND ug/L 06/13/17 19:55 67-72-1 L206/07/17 16:1010.0 1.8 1
Hexachloropropene ND ug/L 06/13/17 19:55 1888-71-706/07/17 16:1010.0 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/13/17 19:55 193-39-506/07/17 16:1010.0 2.0 1
Isodrin ND ug/L 06/13/17 19:55 465-73-606/07/17 16:1020.0 2.5 1
Isophorone ND ug/L 06/13/17 19:55 78-59-1 L206/07/17 16:1010.0 1.5 1
Isosafrole ND ug/L 06/13/17 19:55 120-58-1 L206/07/17 16:1010.0 1.5 1
Kepone ND ug/L 06/13/17 19:55 143-50-006/07/17 16:1020.0 4.5 1
Methapyrilene ND ug/L 06/13/17 19:55 91-80-506/07/17 16:101003.0 1
3-Methylcholanthrene ND ug/L 06/13/17 19:55 56-49-506/07/17 16:1010.0 2.7 1
Methyl methanesulfonate ND ug/L 06/13/17 19:55 66-27-306/07/17 16:1010.0 1.1 1
2-Methylnaphthalene ND ug/L 06/13/17 19:55 91-57-6 L206/07/17 16:1010.0 1.4 1
Methyl parathion ND ug/L 06/13/17 19:55 298-00-006/07/17 16:1010.0 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 06/13/17 19:55 95-48-7 L206/07/17 16:1010.0 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/13/17 19:55 15831-10-4 L206/07/17 16:1010.0 1.4 1
1-Naphthalenamine ND ug/L 06/13/17 19:55 134-32-706/07/17 16:1010.0 1.3 1
2-Naphthalenamine ND ug/L 06/13/17 19:55 91-59-806/07/17 16:1010.0 2.2 1
1,4-Naphthoquinone ND ug/L 06/13/17 19:55 130-15-406/07/17 16:1010.0 0.99 1
2-Nitroaniline ND ug/L 06/13/17 19:55 88-74-406/07/17 16:1050.0 2.3 1
3-Nitroaniline ND ug/L 06/13/17 19:55 99-09-206/07/17 16:1050.0 2.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
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Page 86 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-11D Lab ID:92342479013 Collected:05/31/17 12:10 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Nitroaniline ND ug/L 06/13/17 19:55 100-01-606/07/17 16:1020.0 3.4 1
Nitrobenzene ND ug/L 06/13/17 19:55 98-95-3 L206/07/17 16:1010.0 1.6 1
2-Nitrophenol ND ug/L 06/13/17 19:55 88-75-5 L206/07/17 16:1010.0 1.6 1
4-Nitrophenol ND ug/L 06/13/17 19:55 100-02-706/07/17 16:1050.0 4.3 1
5-Nitro-o-toluidine ND ug/L 06/13/17 19:55 99-55-8 L206/07/17 16:1010.0 1.9 1
N-Nitrosodiethylamine ND ug/L 06/13/17 19:55 55-18-5 L206/07/17 16:1020.0 1.4 1
N-Nitrosodimethylamine ND ug/L 06/13/17 19:55 62-75-906/07/17 16:1010.0 1.6 1
N-Nitroso-di-n-butylamine ND ug/L 06/13/17 19:55 924-16-3 L206/07/17 16:1010.0 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 06/13/17 19:55 621-64-7 L206/07/17 16:1010.0 1.7 1
N-Nitrosodiphenylamine ND ug/L 06/13/17 19:55 86-30-606/07/17 16:1010.0 1.4 1
N-Nitrosomethylethylamine ND ug/L 06/13/17 19:55 10595-95-6 L206/07/17 16:1010.0 1.4 1
N-Nitrosopiperidine ND ug/L 06/13/17 19:55 100-75-4 L206/07/17 16:1020.0 1.7 1
N-Nitrosopyrrolidine ND ug/L 06/13/17 19:55 930-55-2 L206/07/17 16:1010.0 1.7 1
O,O,O-Triethylphosphorothioate ND ug/L 06/13/17 19:55 126-68-1 L206/07/17 16:1010.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/13/17 19:55 108-60-106/07/17 16:1010.0 1.8 1
Parathion (Ethyl parathion)ND ug/L 06/13/17 19:55 56-38-2 L206/07/17 16:1010.0 1.5 1
Pentachlorobenzene ND ug/L 06/13/17 19:55 608-93-506/07/17 16:1010.0 1.5 1
Pentachloronitrobenzene ND ug/L 06/13/17 19:55 82-68-806/07/17 16:1020.0 1.7 1
Pentachlorophenol ND ug/L 06/13/17 19:55 87-86-506/07/17 16:1025.0 3.5 1
Phenacetin ND ug/L 06/13/17 19:55 62-44-206/07/17 16:1020.0 1.9 1
Phenanthrene ND ug/L 06/13/17 19:55 85-01-806/07/17 16:1010.0 1.6 1
Phenol ND ug/L 06/13/17 19:55 108-95-206/07/17 16:1010.0 1.3 1
p-Phenylenediamine ND ug/L 06/13/17 19:55 106-50-3 L206/07/17 16:1010.0 2.2 1
Phorate ND ug/L 06/13/17 19:55 298-02-2 L206/07/17 16:1010.0 1.7 1
Pronamide ND ug/L 06/13/17 19:55 23950-58-5 L206/07/17 16:1010.0 2.0 1
Pyrene ND ug/L 06/13/17 19:55 129-00-006/07/17 16:1010.0 2.2 1
Safrole ND ug/L 06/13/17 19:55 94-59-7 L206/07/17 16:1010.0 1.3 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/13/17 19:55 95-94-306/07/17 16:1010.0 1.3 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/13/17 19:55 58-90-206/07/17 16:1010.0 2.9 1
Thionazin ND ug/L 06/13/17 19:55 297-97-2 L206/07/17 16:1020.0 1.7 1
O-Toluidine ND ug/L 06/13/17 19:55 95-53-4 L206/07/17 16:1010.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 06/13/17 19:55 95-95-406/07/17 16:1010.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/13/17 19:55 88-06-206/07/17 16:1010.0 1.4 1
1,3,5-Trinitrobenzene ND ug/L 06/13/17 19:55 99-35-4 L206/07/17 16:1010.0 1.2 1
Surrogates
Nitrobenzene-d5 (S)83 %06/13/17 19:55 4165-60-0 1g06/07/17 16:1021-110 1
2-Fluorobiphenyl (S)102 %06/13/17 19:55 321-60-806/07/17 16:1027-110 1
Terphenyl-d14 (S)98 %06/13/17 19:55 1718-51-006/07/17 16:1031-107 1
Phenol-d6 (S)43 %06/13/17 19:55 13127-88-306/07/17 16:1010-110 1
2-Fluorophenol (S)61 %06/13/17 19:55 367-12-406/07/17 16:1012-110 1
2,4,6-Tribromophenol (S)85 %06/13/17 19:55 118-79-606/07/17 16:1027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/02/17 05:50 67-64-110010.0 1
Acetonitrile ND ug/L 06/02/17 05:50 75-05-855.0 2.2 1
Acrolein ND ug/L 06/02/17 05:50 107-02-853.0 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 87 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-11D Lab ID:92342479013 Collected:05/31/17 12:10 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acrylonitrile ND ug/L 06/02/17 05:50 107-13-12001.9 1
Allyl chloride ND ug/L 06/02/17 05:50 107-05-110.0 1.5 1
Benzene ND ug/L 06/02/17 05:50 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/02/17 05:50 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/02/17 05:50 75-27-41.0 0.18 1
Bromoform ND ug/L 06/02/17 05:50 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/02/17 05:50 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/02/17 05:50 78-93-31000.96 1
Carbon disulfide ND ug/L 06/02/17 05:50 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/02/17 05:50 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/02/17 05:50 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/02/17 05:50 75-00-310.0 0.54 1
Chloroform ND ug/L 06/02/17 05:50 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/02/17 05:50 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/02/17 05:50 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/02/17 05:50 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/02/17 05:50 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/02/17 05:50 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/02/17 05:50 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/02/17 05:50 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/02/17 05:50 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/02/17 05:50 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/02/17 05:50 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/02/17 05:50 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/02/17 05:50 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/02/17 05:50 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/02/17 05:50 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/02/17 05:50 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/02/17 05:50 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/02/17 05:50 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/02/17 05:50 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/02/17 05:50 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/02/17 05:50 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/02/17 05:50 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/02/17 05:50 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/02/17 05:50 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/02/17 05:50 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/02/17 05:50 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/02/17 05:50 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/02/17 05:50 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/02/17 05:50 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/02/17 05:50 126-98-71000.93 1
Methylene Chloride ND ug/L 06/02/17 05:50 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/02/17 05:50 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/02/17 05:50 108-10-11000.33 1
Naphthalene ND ug/L 06/02/17 05:50 91-20-310.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 88 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-11D Lab ID:92342479013 Collected:05/31/17 12:10 Received:05/31/17 15:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Propionitrile ND ug/L 06/02/17 05:50 107-12-01503.6 1
Styrene ND ug/L 06/02/17 05:50 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/02/17 05:50 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/02/17 05:50 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/02/17 05:50 127-18-41.0 0.46 1
Toluene ND ug/L 06/02/17 05:50 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/02/17 05:50 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/02/17 05:50 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/02/17 05:50 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/02/17 05:50 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/02/17 05:50 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/02/17 05:50 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/02/17 05:50 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/02/17 05:50 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/02/17 05:50 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)115 %06/02/17 05:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %06/02/17 05:50 17060-07-070-130 1
Toluene-d8 (S)111 %06/02/17 05:50 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/07/17 22:30 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/01/17 17:45 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 89 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-12 Lab ID:92342529001 Collected:05/31/17 03:20 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/08/17 00:58 309-00-206/02/17 13:290.050 0.050 1
alpha-BHC ND ug/L 06/08/17 00:58 319-84-606/02/17 13:290.050 0.050 1
beta-BHC ND ug/L 06/08/17 00:58 319-85-706/02/17 13:290.050 0.050 1
delta-BHC ND ug/L 06/08/17 00:58 319-86-806/02/17 13:290.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/08/17 00:58 58-89-906/02/17 13:290.050 0.050 1
Chlordane (Technical)ND ug/L 06/08/17 00:58 57-74-906/02/17 13:290.50 0.20 1
4,4'-DDD ND ug/L 06/08/17 00:58 72-54-806/02/17 13:290.10 0.050 1
4,4'-DDE ND ug/L 06/08/17 00:58 72-55-906/02/17 13:290.10 0.050 1
4,4'-DDT ND ug/L 06/08/17 00:58 50-29-306/02/17 13:290.10 0.050 1
Dieldrin ND ug/L 06/08/17 00:58 60-57-106/02/17 13:290.075 0.050 1
Endosulfan I ND ug/L 06/08/17 00:58 959-98-806/02/17 13:290.10 0.050 1
Endosulfan II ND ug/L 06/08/17 00:58 33213-65-906/02/17 13:290.10 0.050 1
Endosulfan sulfate ND ug/L 06/08/17 00:58 1031-07-806/02/17 13:290.10 0.050 1
Endrin ND ug/L 06/08/17 00:58 72-20-806/02/17 13:290.10 0.050 1
Endrin aldehyde ND ug/L 06/08/17 00:58 7421-93-406/02/17 13:290.10 0.050 1
Heptachlor ND ug/L 06/08/17 00:58 76-44-806/02/17 13:290.050 0.050 1
Heptachlor epoxide ND ug/L 06/08/17 00:58 1024-57-306/02/17 13:290.075 0.050 1
Methoxychlor ND ug/L 06/08/17 00:58 72-43-506/02/17 13:291.0 0.15 1
Toxaphene ND ug/L 06/08/17 00:58 8001-35-206/02/17 13:291.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)71 %06/08/17 00:58 877-09-806/02/17 13:2920-130 1
Decachlorobiphenyl (S)56 %06/08/17 00:58 2051-24-306/02/17 13:2920-130 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/10/17 03:37 94-75-706/07/17 16:000.99 0.23 1
Dinoseb ND ug/L 06/10/17 03:37 88-85-706/07/17 16:000.20 0.060 1
Pentachlorophenol ND ug/L 06/10/17 03:37 87-86-506/07/17 16:000.030 0.018 1
2,4,5-T ND ug/L 06/10/17 03:37 93-76-506/07/17 16:000.20 0.044 1
2,4,5-TP (Silvex)ND ug/L 06/10/17 03:37 93-72-106/07/17 16:000.20 0.051 1
Surrogates
2,4-DCAA (S)89 %06/10/17 03:37 19719-28-906/07/17 16:0039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/09/17 21:19 7440-36-006/02/17 11:256.0 3.9 1
Arsenic ND ug/L 06/09/17 21:19 7440-38-206/02/17 11:2510.0 5.0 1
Barium 16.2J ug/L 06/09/17 21:19 7440-39-306/02/17 11:251002.5 1
Beryllium ND ug/L 06/09/17 21:19 7440-41-706/02/17 11:251.0 0.50 1
Cadmium ND ug/L 06/09/17 21:19 7440-43-906/02/17 11:251.0 0.50 1
Chromium ND ug/L 06/09/17 21:19 7440-47-306/02/17 11:2510.0 2.5 1
Cobalt ND ug/L 06/09/17 21:19 7440-48-406/02/17 11:2510.0 2.5 1
Copper ND ug/L 06/09/17 21:19 7440-50-806/02/17 11:2510.0 2.5 1
Lead ND ug/L 06/09/17 21:19 7439-92-106/02/17 11:2510.0 2.5 1
Nickel ND ug/L 06/09/17 21:19 7440-02-006/02/17 11:2550.0 2.5 1
Selenium ND ug/L 06/09/17 21:19 7782-49-206/02/17 11:2510.0 5.0 1
Silver ND ug/L 06/09/17 21:19 7440-22-406/02/17 11:2510.0 2.5 1
Tin ND ug/L 06/09/17 21:19 7440-31-506/02/17 11:251002.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 90 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-12 Lab ID:92342529001 Collected:05/31/17 03:20 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Vanadium ND ug/L 06/09/17 21:19 7440-62-206/02/17 11:2525.0 2.5 1
Zinc 8.0J ug/L 06/09/17 21:19 7440-66-606/02/17 11:2510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/06/17 19:07 7440-28-006/03/17 02:255.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 01:39 7439-97-606/05/17 20:000.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/14/17 14:32 83-32-906/07/17 17:1010.0 1.6 1
Acenaphthylene ND ug/L 06/14/17 14:32 208-96-806/07/17 17:1010.0 1.5 1
Acetophenone ND ug/L 06/14/17 14:32 98-86-206/07/17 17:1010.0 1.9 1
2-Acetylaminofluorene ND ug/L 06/14/17 14:32 53-96-3 L206/07/17 17:1020.0 1.6 1
4-Aminobiphenyl ND ug/L 06/14/17 14:32 92-67-106/07/17 17:1020.0 1.7 1
Anthracene ND ug/L 06/14/17 14:32 120-12-706/07/17 17:1010.0 1.7 1
Benzo(a)anthracene ND ug/L 06/14/17 14:32 56-55-306/07/17 17:1010.0 2.1 1
Benzo(a)pyrene ND ug/L 06/14/17 14:32 50-32-806/07/17 17:1010.0 2.2 1
Benzo(b)fluoranthene ND ug/L 06/14/17 14:32 205-99-206/07/17 17:1010.0 2.2 1
Benzo(g,h,i)perylene ND ug/L 06/14/17 14:32 191-24-206/07/17 17:1010.0 2.1 1
Benzo(k)fluoranthene ND ug/L 06/14/17 14:32 207-08-906/07/17 17:1010.0 2.0 1
Benzyl alcohol ND ug/L 06/14/17 14:32 100-51-606/07/17 17:1020.0 3.1 1
4-Bromophenylphenyl ether ND ug/L 06/14/17 14:32 101-55-306/07/17 17:1010.0 1.5 1
Butylbenzylphthalate ND ug/L 06/14/17 14:32 85-68-706/07/17 17:1010.0 2.5 1
4-Chloro-3-methylphenol ND ug/L 06/14/17 14:32 59-50-706/07/17 17:1020.0 2.8 1
4-Chloroaniline ND ug/L 06/14/17 14:32 106-47-806/07/17 17:1020.0 2.8 1
Chlorobenzilate ND ug/L 06/14/17 14:32 510-15-606/07/17 17:1010.0 2.2 1
bis(2-Chloroethoxy)methane ND ug/L 06/14/17 14:32 111-91-106/07/17 17:1010.0 1.6 1
bis(2-Chloroethyl) ether ND ug/L 06/14/17 14:32 111-44-406/07/17 17:1010.0 1.7 1
2-Chloronaphthalene ND ug/L 06/14/17 14:32 91-58-706/07/17 17:1010.0 1.6 1
2-Chlorophenol ND ug/L 06/14/17 14:32 95-57-806/07/17 17:1010.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/14/17 14:32 7005-72-306/07/17 17:1010.0 1.6 1
Chrysene ND ug/L 06/14/17 14:32 218-01-906/07/17 17:1010.0 2.1 1
Diallate ND ug/L 06/14/17 14:32 2303-16-406/07/17 17:1010.0 1.6 1
Dibenz(a,h)anthracene ND ug/L 06/14/17 14:32 53-70-306/07/17 17:1010.0 2.0 1
Dibenzofuran ND ug/L 06/14/17 14:32 132-64-906/07/17 17:1010.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 06/14/17 14:32 91-94-106/07/17 17:1020.0 3.9 1
2,4-Dichlorophenol ND ug/L 06/14/17 14:32 120-83-206/07/17 17:1010.0 1.6 1
2,6-Dichlorophenol ND ug/L 06/14/17 14:32 87-65-006/07/17 17:1010.0 1.5 1
Diethylphthalate ND ug/L 06/14/17 14:32 84-66-206/07/17 17:1060001.6 1
Dimethoate ND ug/L 06/14/17 14:32 60-51-506/07/17 17:1020.0 1.8 1
P-Dimethylaminoazobenzene ND ug/L 06/14/17 14:32 60-11-706/07/17 17:1010.0 1.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/14/17 14:32 57-97-606/07/17 17:1010.0 2.4 1
3,3'-Dimethylbenzidine ND ug/L 06/14/17 14:32 119-93-706/07/17 17:1010.0 3.9 1
2,4-Dimethylphenol ND ug/L 06/14/17 14:32 105-67-906/07/17 17:1010.0 1.6 1
Dimethylphthalate ND ug/L 06/14/17 14:32 131-11-306/07/17 17:1010.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 91 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-12 Lab ID:92342529001 Collected:05/31/17 03:20 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Di-n-butylphthalate ND ug/L 06/14/17 14:32 84-74-206/07/17 17:1010.0 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/14/17 14:32 534-52-106/07/17 17:1050.0 2.2 1
1,3-Dinitrobenzene ND ug/L 06/14/17 14:32 99-65-006/07/17 17:1020.0 1.3 1
2,4-Dinitrophenol ND ug/L 06/14/17 14:32 51-28-506/07/17 17:1050.0 5.1 1
2,4-Dinitrotoluene ND ug/L 06/14/17 14:32 121-14-206/07/17 17:1010.0 1.5 1
2,6-Dinitrotoluene ND ug/L 06/14/17 14:32 606-20-206/07/17 17:1010.0 1.4 1
Di-n-octylphthalate ND ug/L 06/14/17 14:32 117-84-006/07/17 17:1010.0 1.5 1
Diphenylamine ND ug/L 06/14/17 14:32 122-39-406/07/17 17:1010.0 1.4 1
Disulfoton ND ug/L 06/14/17 14:32 298-04-406/07/17 17:1010.0 1.5 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/14/17 14:32 117-81-706/07/17 17:1015.0 2.3 1
Ethyl methanesulfonate ND ug/L 06/14/17 14:32 62-50-006/07/17 17:1020.0 1.6 1
Famphur ND ug/L 06/14/17 14:32 52-85-706/07/17 17:1020.0 5.7 1
Fluoranthene ND ug/L 06/14/17 14:32 206-44-006/07/17 17:1010.0 2.2 1
Fluorene ND ug/L 06/14/17 14:32 86-73-706/07/17 17:1010.0 1.6 1
Hexachlorobenzene ND ug/L 06/14/17 14:32 118-74-106/07/17 17:1010.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 06/14/17 14:32 77-47-406/07/17 17:1010.0 1.3 1
Hexachloroethane ND ug/L 06/14/17 14:32 67-72-106/07/17 17:1010.0 1.8 1
Hexachloropropene ND ug/L 06/14/17 14:32 1888-71-706/07/17 17:1010.0 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/14/17 14:32 193-39-506/07/17 17:1010.0 2.0 1
Isodrin ND ug/L 06/14/17 14:32 465-73-606/07/17 17:1020.0 2.5 1
Isophorone ND ug/L 06/14/17 14:32 78-59-106/07/17 17:1010.0 1.5 1
Isosafrole ND ug/L 06/14/17 14:32 120-58-106/07/17 17:1010.0 1.5 1
Kepone ND ug/L 06/14/17 14:32 143-50-006/07/17 17:1020.0 4.5 1
Methapyrilene ND ug/L 06/14/17 14:32 91-80-506/07/17 17:101003.0 1
3-Methylcholanthrene ND ug/L 06/14/17 14:32 56-49-506/07/17 17:1010.0 2.7 1
Methyl methanesulfonate ND ug/L 06/14/17 14:32 66-27-306/07/17 17:1010.0 1.1 1
2-Methylnaphthalene ND ug/L 06/14/17 14:32 91-57-606/07/17 17:1010.0 1.4 1
Methyl parathion ND ug/L 06/14/17 14:32 298-00-006/07/17 17:1010.0 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 06/14/17 14:32 95-48-706/07/17 17:1010.0 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/14/17 14:32 15831-10-406/07/17 17:1010.0 1.4 1
1-Naphthalenamine ND ug/L 06/14/17 14:32 134-32-706/07/17 17:1010.0 1.3 1
2-Naphthalenamine ND ug/L 06/14/17 14:32 91-59-806/07/17 17:1010.0 2.2 1
1,4-Naphthoquinone ND ug/L 06/14/17 14:32 130-15-406/07/17 17:1010.0 0.99 1
2-Nitroaniline ND ug/L 06/14/17 14:32 88-74-406/07/17 17:1050.0 2.3 1
3-Nitroaniline ND ug/L 06/14/17 14:32 99-09-206/07/17 17:1050.0 2.7 1
4-Nitroaniline ND ug/L 06/14/17 14:32 100-01-606/07/17 17:1020.0 3.4 1
Nitrobenzene ND ug/L 06/14/17 14:32 98-95-306/07/17 17:1010.0 1.6 1
2-Nitrophenol ND ug/L 06/14/17 14:32 88-75-506/07/17 17:1010.0 1.6 1
4-Nitrophenol ND ug/L 06/14/17 14:32 100-02-706/07/17 17:1050.0 4.3 1
5-Nitro-o-toluidine ND ug/L 06/14/17 14:32 99-55-806/07/17 17:1010.0 1.9 1
N-Nitrosodiethylamine ND ug/L 06/14/17 14:32 55-18-506/07/17 17:1020.0 1.4 1
N-Nitrosodimethylamine ND ug/L 06/14/17 14:32 62-75-906/07/17 17:1010.0 1.6 1
N-Nitroso-di-n-butylamine ND ug/L 06/14/17 14:32 924-16-306/07/17 17:1010.0 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 06/14/17 14:32 621-64-706/07/17 17:1010.0 1.7 1
N-Nitrosodiphenylamine ND ug/L 06/14/17 14:32 86-30-606/07/17 17:1010.0 1.4 1
N-Nitrosomethylethylamine ND ug/L 06/14/17 14:32 10595-95-606/07/17 17:1010.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 92 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-12 Lab ID:92342529001 Collected:05/31/17 03:20 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
N-Nitrosopiperidine ND ug/L 06/14/17 14:32 100-75-406/07/17 17:1020.0 1.7 1
N-Nitrosopyrrolidine ND ug/L 06/14/17 14:32 930-55-206/07/17 17:1010.0 1.7 1
O,O,O-Triethylphosphorothioate ND ug/L 06/14/17 14:32 126-68-106/07/17 17:1010.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/14/17 14:32 108-60-106/07/17 17:1010.0 1.8 1
Parathion (Ethyl parathion)ND ug/L 06/14/17 14:32 56-38-206/07/17 17:1010.0 1.5 1
Pentachlorobenzene ND ug/L 06/14/17 14:32 608-93-506/07/17 17:1010.0 1.5 1
Pentachloronitrobenzene ND ug/L 06/14/17 14:32 82-68-806/07/17 17:1020.0 1.7 1
Pentachlorophenol ND ug/L 06/14/17 14:32 87-86-506/07/17 17:1025.0 3.5 1
Phenacetin ND ug/L 06/14/17 14:32 62-44-206/07/17 17:1020.0 1.9 1
Phenanthrene ND ug/L 06/14/17 14:32 85-01-806/07/17 17:1010.0 1.6 1
Phenol ND ug/L 06/14/17 14:32 108-95-206/07/17 17:1010.0 1.3 1
p-Phenylenediamine ND ug/L 06/14/17 14:32 106-50-306/07/17 17:1010.0 2.2 1
Phorate ND ug/L 06/14/17 14:32 298-02-206/07/17 17:1010.0 1.7 1
Pronamide ND ug/L 06/14/17 14:32 23950-58-506/07/17 17:1010.0 2.0 1
Pyrene ND ug/L 06/14/17 14:32 129-00-006/07/17 17:1010.0 2.2 1
Safrole ND ug/L 06/14/17 14:32 94-59-706/07/17 17:1010.0 1.3 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/14/17 14:32 95-94-306/07/17 17:1010.0 1.3 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/14/17 14:32 58-90-206/07/17 17:1010.0 2.9 1
Thionazin ND ug/L 06/14/17 14:32 297-97-206/07/17 17:1020.0 1.7 1
O-Toluidine ND ug/L 06/14/17 14:32 95-53-406/07/17 17:1010.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 06/14/17 14:32 95-95-406/07/17 17:1010.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/14/17 14:32 88-06-206/07/17 17:1010.0 1.4 1
1,3,5-Trinitrobenzene ND ug/L 06/14/17 14:32 99-35-406/07/17 17:1010.0 1.2 1
Surrogates
Nitrobenzene-d5 (S)46 %06/14/17 14:32 4165-60-006/07/17 17:1021-110 1
2-Fluorobiphenyl (S)53 %06/14/17 14:32 321-60-806/07/17 17:1027-110 1
Terphenyl-d14 (S)49 %06/14/17 14:32 1718-51-006/07/17 17:1031-107 1
Phenol-d6 (S)14 %06/14/17 14:32 13127-88-306/07/17 17:1010-110 1
2-Fluorophenol (S)24 %06/14/17 14:32 367-12-406/07/17 17:1012-110 1
2,4,6-Tribromophenol (S)50 %06/14/17 14:32 118-79-606/07/17 17:1027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 14.2J ug/L 06/11/17 15:25 67-64-110010.0 1
Acetonitrile ND ug/L 06/11/17 15:25 75-05-855.0 2.2 1
Acrolein ND ug/L 06/11/17 15:25 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 06/11/17 15:25 107-13-12001.9 1
Allyl chloride ND ug/L 06/11/17 15:25 107-05-110.0 1.5 1
Benzene ND ug/L 06/11/17 15:25 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/11/17 15:25 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/11/17 15:25 75-27-41.0 0.18 1
Bromoform ND ug/L 06/11/17 15:25 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/11/17 15:25 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/11/17 15:25 78-93-31000.96 1
Carbon disulfide ND ug/L 06/11/17 15:25 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/11/17 15:25 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/11/17 15:25 108-90-73.0 0.23 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 93 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-12 Lab ID:92342529001 Collected:05/31/17 03:20 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Chloroethane ND ug/L 06/11/17 15:25 75-00-310.0 0.54 1
Chloroform ND ug/L 06/11/17 15:25 67-66-35.0 0.14 1
Chloromethane 0.32J ug/L 06/11/17 15:25 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/11/17 15:25 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/11/17 15:25 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/11/17 15:25 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/11/17 15:25 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/11/17 15:25 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/11/17 15:25 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/11/17 15:25 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/11/17 15:25 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/11/17 15:25 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/11/17 15:25 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/11/17 15:25 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/11/17 15:25 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/11/17 15:25 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/11/17 15:25 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/11/17 15:25 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/11/17 15:25 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/11/17 15:25 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/11/17 15:25 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/11/17 15:25 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/11/17 15:25 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/11/17 15:25 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/11/17 15:25 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/11/17 15:25 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/11/17 15:25 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/11/17 15:25 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/11/17 15:25 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/11/17 15:25 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/11/17 15:25 126-98-71000.93 1
Methylene Chloride ND ug/L 06/11/17 15:25 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/11/17 15:25 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/11/17 15:25 108-10-11000.33 1
Naphthalene ND ug/L 06/11/17 15:25 91-20-310.0 0.24 1
Propionitrile ND ug/L 06/11/17 15:25 107-12-01503.6 1
Styrene ND ug/L 06/11/17 15:25 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/11/17 15:25 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/11/17 15:25 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/11/17 15:25 127-18-41.0 0.46 1
Toluene ND ug/L 06/11/17 15:25 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/11/17 15:25 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/11/17 15:25 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/11/17 15:25 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/11/17 15:25 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/11/17 15:25 75-69-41.0 0.20 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 94 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-12 Lab ID:92342529001 Collected:05/31/17 03:20 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2,3-Trichloropropane ND ug/L 06/11/17 15:25 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/11/17 15:25 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/11/17 15:25 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/11/17 15:25 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)105 %06/11/17 15:25 460-00-470-130 1
1,2-Dichloroethane-d4 (S)111 %06/11/17 15:25 17060-07-070-130 1
Toluene-d8 (S)107 %06/11/17 15:25 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/06/17 23:00 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 4.8J ug/L 06/07/17 13:29 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 95 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-13 Lab ID:92342529002 Collected:05/31/17 03:30 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 06/08/17 01:16 309-00-206/02/17 13:290.050 0.050 1
alpha-BHC ND ug/L 06/08/17 01:16 319-84-606/02/17 13:290.050 0.050 1
beta-BHC ND ug/L 06/08/17 01:16 319-85-706/02/17 13:290.050 0.050 1
delta-BHC ND ug/L 06/08/17 01:16 319-86-806/02/17 13:290.050 0.050 1
gamma-BHC (Lindane)ND ug/L 06/08/17 01:16 58-89-906/02/17 13:290.050 0.050 1
Chlordane (Technical)ND ug/L 06/08/17 01:16 57-74-906/02/17 13:290.50 0.20 1
4,4'-DDD ND ug/L 06/08/17 01:16 72-54-806/02/17 13:290.10 0.050 1
4,4'-DDE ND ug/L 06/08/17 01:16 72-55-906/02/17 13:290.10 0.050 1
4,4'-DDT ND ug/L 06/08/17 01:16 50-29-306/02/17 13:290.10 0.050 1
Dieldrin ND ug/L 06/08/17 01:16 60-57-106/02/17 13:290.075 0.050 1
Endosulfan I ND ug/L 06/08/17 01:16 959-98-806/02/17 13:290.10 0.050 1
Endosulfan II ND ug/L 06/08/17 01:16 33213-65-906/02/17 13:290.10 0.050 1
Endosulfan sulfate ND ug/L 06/08/17 01:16 1031-07-806/02/17 13:290.10 0.050 1
Endrin ND ug/L 06/08/17 01:16 72-20-806/02/17 13:290.10 0.050 1
Endrin aldehyde ND ug/L 06/08/17 01:16 7421-93-406/02/17 13:290.10 0.050 1
Heptachlor ND ug/L 06/08/17 01:16 76-44-806/02/17 13:290.050 0.050 1
Heptachlor epoxide ND ug/L 06/08/17 01:16 1024-57-306/02/17 13:290.075 0.050 1
Methoxychlor ND ug/L 06/08/17 01:16 72-43-506/02/17 13:291.0 0.15 1
Toxaphene ND ug/L 06/08/17 01:16 8001-35-206/02/17 13:291.5 0.20 1
Surrogates
Tetrachloro-m-xylene (S)87 %06/08/17 01:16 877-09-806/02/17 13:2920-130 1
Decachlorobiphenyl (S)74 %06/08/17 01:16 2051-24-306/02/17 13:2920-130 1
Analytical Method: EPA 8151 Preparation Method: EPA 81518151 Chlorinated Herbicides
2,4-D ND ug/L 06/10/17 04:07 94-75-706/07/17 16:001.0 0.24 1
Dinoseb ND ug/L 06/10/17 04:07 88-85-706/07/17 16:000.20 0.061 1
Pentachlorophenol ND ug/L 06/10/17 04:07 87-86-506/07/17 16:000.030 0.018 1
2,4,5-T ND ug/L 06/10/17 04:07 93-76-506/07/17 16:000.20 0.045 1
2,4,5-TP (Silvex)ND ug/L 06/10/17 04:07 93-72-106/07/17 16:000.20 0.052 1
Surrogates
2,4-DCAA (S)81 %06/10/17 04:07 19719-28-906/07/17 16:0039-139 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/09/17 21:23 7440-36-006/02/17 11:256.0 3.9 1
Arsenic ND ug/L 06/09/17 21:23 7440-38-206/02/17 11:2510.0 5.0 1
Barium 16.2J ug/L 06/09/17 21:23 7440-39-306/02/17 11:251002.5 1
Beryllium ND ug/L 06/09/17 21:23 7440-41-706/02/17 11:251.0 0.50 1
Cadmium ND ug/L 06/09/17 21:23 7440-43-906/02/17 11:251.0 0.50 1
Chromium ND ug/L 06/09/17 21:23 7440-47-306/02/17 11:2510.0 2.5 1
Cobalt ND ug/L 06/09/17 21:23 7440-48-406/02/17 11:2510.0 2.5 1
Copper ND ug/L 06/09/17 21:23 7440-50-806/02/17 11:2510.0 2.5 1
Lead ND ug/L 06/09/17 21:23 7439-92-106/02/17 11:2510.0 2.5 1
Nickel ND ug/L 06/09/17 21:23 7440-02-006/02/17 11:2550.0 2.5 1
Selenium ND ug/L 06/09/17 21:23 7782-49-206/02/17 11:2510.0 5.0 1
Silver ND ug/L 06/09/17 21:23 7440-22-406/02/17 11:2510.0 2.5 1
Tin ND ug/L 06/09/17 21:23 7440-31-506/02/17 11:251002.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 96 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-13 Lab ID:92342529002 Collected:05/31/17 03:30 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Vanadium ND ug/L 06/09/17 21:23 7440-62-206/02/17 11:2525.0 2.5 1
Zinc ND ug/L 06/09/17 21:23 7440-66-606/02/17 11:2510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.073J ug/L 06/06/17 19:16 7440-28-006/03/17 02:255.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/07/17 01:41 7439-97-606/05/17 20:000.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 06/14/17 15:02 83-32-906/07/17 17:1010.0 1.6 1
Acenaphthylene ND ug/L 06/14/17 15:02 208-96-806/07/17 17:1010.0 1.5 1
Acetophenone ND ug/L 06/14/17 15:02 98-86-206/07/17 17:1010.0 1.9 1
2-Acetylaminofluorene ND ug/L 06/14/17 15:02 53-96-3 L206/07/17 17:1020.0 1.6 1
4-Aminobiphenyl ND ug/L 06/14/17 15:02 92-67-106/07/17 17:1020.0 1.7 1
Anthracene ND ug/L 06/14/17 15:02 120-12-706/07/17 17:1010.0 1.7 1
Benzo(a)anthracene ND ug/L 06/14/17 15:02 56-55-306/07/17 17:1010.0 2.1 1
Benzo(a)pyrene ND ug/L 06/14/17 15:02 50-32-806/07/17 17:1010.0 2.2 1
Benzo(b)fluoranthene ND ug/L 06/14/17 15:02 205-99-206/07/17 17:1010.0 2.2 1
Benzo(g,h,i)perylene ND ug/L 06/14/17 15:02 191-24-206/07/17 17:1010.0 2.1 1
Benzo(k)fluoranthene ND ug/L 06/14/17 15:02 207-08-906/07/17 17:1010.0 2.0 1
Benzyl alcohol ND ug/L 06/14/17 15:02 100-51-606/07/17 17:1020.0 3.1 1
4-Bromophenylphenyl ether ND ug/L 06/14/17 15:02 101-55-306/07/17 17:1010.0 1.5 1
Butylbenzylphthalate ND ug/L 06/14/17 15:02 85-68-706/07/17 17:1010.0 2.5 1
4-Chloro-3-methylphenol ND ug/L 06/14/17 15:02 59-50-706/07/17 17:1020.0 2.8 1
4-Chloroaniline ND ug/L 06/14/17 15:02 106-47-806/07/17 17:1020.0 2.8 1
Chlorobenzilate ND ug/L 06/14/17 15:02 510-15-606/07/17 17:1010.0 2.2 1
bis(2-Chloroethoxy)methane ND ug/L 06/14/17 15:02 111-91-106/07/17 17:1010.0 1.6 1
bis(2-Chloroethyl) ether ND ug/L 06/14/17 15:02 111-44-406/07/17 17:1010.0 1.7 1
2-Chloronaphthalene ND ug/L 06/14/17 15:02 91-58-706/07/17 17:1010.0 1.6 1
2-Chlorophenol ND ug/L 06/14/17 15:02 95-57-806/07/17 17:1010.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 06/14/17 15:02 7005-72-306/07/17 17:1010.0 1.6 1
Chrysene ND ug/L 06/14/17 15:02 218-01-906/07/17 17:1010.0 2.1 1
Diallate ND ug/L 06/14/17 15:02 2303-16-406/07/17 17:1010.0 1.6 1
Dibenz(a,h)anthracene ND ug/L 06/14/17 15:02 53-70-306/07/17 17:1010.0 2.0 1
Dibenzofuran ND ug/L 06/14/17 15:02 132-64-906/07/17 17:1010.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 06/14/17 15:02 91-94-106/07/17 17:1020.0 3.9 1
2,4-Dichlorophenol ND ug/L 06/14/17 15:02 120-83-206/07/17 17:1010.0 1.6 1
2,6-Dichlorophenol ND ug/L 06/14/17 15:02 87-65-006/07/17 17:1010.0 1.5 1
Diethylphthalate ND ug/L 06/14/17 15:02 84-66-206/07/17 17:1060001.6 1
Dimethoate ND ug/L 06/14/17 15:02 60-51-506/07/17 17:1020.0 1.8 1
P-Dimethylaminoazobenzene ND ug/L 06/14/17 15:02 60-11-706/07/17 17:1010.0 1.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 06/14/17 15:02 57-97-606/07/17 17:1010.0 2.4 1
3,3'-Dimethylbenzidine ND ug/L 06/14/17 15:02 119-93-706/07/17 17:1010.0 3.9 1
2,4-Dimethylphenol ND ug/L 06/14/17 15:02 105-67-906/07/17 17:1010.0 1.6 1
Dimethylphthalate ND ug/L 06/14/17 15:02 131-11-306/07/17 17:1010.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 97 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-13 Lab ID:92342529002 Collected:05/31/17 03:30 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Di-n-butylphthalate ND ug/L 06/14/17 15:02 84-74-206/07/17 17:1010.0 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 06/14/17 15:02 534-52-106/07/17 17:1050.0 2.2 1
1,3-Dinitrobenzene ND ug/L 06/14/17 15:02 99-65-006/07/17 17:1020.0 1.3 1
2,4-Dinitrophenol ND ug/L 06/14/17 15:02 51-28-506/07/17 17:1050.0 5.1 1
2,4-Dinitrotoluene ND ug/L 06/14/17 15:02 121-14-206/07/17 17:1010.0 1.5 1
2,6-Dinitrotoluene ND ug/L 06/14/17 15:02 606-20-206/07/17 17:1010.0 1.4 1
Di-n-octylphthalate ND ug/L 06/14/17 15:02 117-84-006/07/17 17:1010.0 1.5 1
Diphenylamine ND ug/L 06/14/17 15:02 122-39-406/07/17 17:1010.0 1.4 1
Disulfoton ND ug/L 06/14/17 15:02 298-04-406/07/17 17:1010.0 1.5 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/14/17 15:02 117-81-706/07/17 17:1015.0 2.3 1
Ethyl methanesulfonate ND ug/L 06/14/17 15:02 62-50-006/07/17 17:1020.0 1.6 1
Famphur ND ug/L 06/14/17 15:02 52-85-706/07/17 17:1020.0 5.7 1
Fluoranthene ND ug/L 06/14/17 15:02 206-44-006/07/17 17:1010.0 2.2 1
Fluorene ND ug/L 06/14/17 15:02 86-73-706/07/17 17:1010.0 1.6 1
Hexachlorobenzene ND ug/L 06/14/17 15:02 118-74-106/07/17 17:1010.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 06/14/17 15:02 77-47-406/07/17 17:1010.0 1.3 1
Hexachloroethane ND ug/L 06/14/17 15:02 67-72-106/07/17 17:1010.0 1.8 1
Hexachloropropene ND ug/L 06/14/17 15:02 1888-71-706/07/17 17:1010.0 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/14/17 15:02 193-39-506/07/17 17:1010.0 2.0 1
Isodrin ND ug/L 06/14/17 15:02 465-73-606/07/17 17:1020.0 2.5 1
Isophorone ND ug/L 06/14/17 15:02 78-59-106/07/17 17:1010.0 1.5 1
Isosafrole ND ug/L 06/14/17 15:02 120-58-106/07/17 17:1010.0 1.5 1
Kepone ND ug/L 06/14/17 15:02 143-50-006/07/17 17:1020.0 4.5 1
Methapyrilene ND ug/L 06/14/17 15:02 91-80-506/07/17 17:101003.0 1
3-Methylcholanthrene ND ug/L 06/14/17 15:02 56-49-506/07/17 17:1010.0 2.7 1
Methyl methanesulfonate ND ug/L 06/14/17 15:02 66-27-306/07/17 17:1010.0 1.1 1
2-Methylnaphthalene ND ug/L 06/14/17 15:02 91-57-606/07/17 17:1010.0 1.4 1
Methyl parathion ND ug/L 06/14/17 15:02 298-00-006/07/17 17:1010.0 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 06/14/17 15:02 95-48-706/07/17 17:1010.0 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/14/17 15:02 15831-10-406/07/17 17:1010.0 1.4 1
1-Naphthalenamine ND ug/L 06/14/17 15:02 134-32-706/07/17 17:1010.0 1.3 1
2-Naphthalenamine ND ug/L 06/14/17 15:02 91-59-806/07/17 17:1010.0 2.2 1
1,4-Naphthoquinone ND ug/L 06/14/17 15:02 130-15-406/07/17 17:1010.0 0.99 1
2-Nitroaniline ND ug/L 06/14/17 15:02 88-74-406/07/17 17:1050.0 2.3 1
3-Nitroaniline ND ug/L 06/14/17 15:02 99-09-206/07/17 17:1050.0 2.7 1
4-Nitroaniline ND ug/L 06/14/17 15:02 100-01-606/07/17 17:1020.0 3.4 1
Nitrobenzene ND ug/L 06/14/17 15:02 98-95-306/07/17 17:1010.0 1.6 1
2-Nitrophenol ND ug/L 06/14/17 15:02 88-75-506/07/17 17:1010.0 1.6 1
4-Nitrophenol ND ug/L 06/14/17 15:02 100-02-706/07/17 17:1050.0 4.3 1
5-Nitro-o-toluidine ND ug/L 06/14/17 15:02 99-55-806/07/17 17:1010.0 1.9 1
N-Nitrosodiethylamine ND ug/L 06/14/17 15:02 55-18-506/07/17 17:1020.0 1.4 1
N-Nitrosodimethylamine ND ug/L 06/14/17 15:02 62-75-906/07/17 17:1010.0 1.6 1
N-Nitroso-di-n-butylamine ND ug/L 06/14/17 15:02 924-16-306/07/17 17:1010.0 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 06/14/17 15:02 621-64-706/07/17 17:1010.0 1.7 1
N-Nitrosodiphenylamine ND ug/L 06/14/17 15:02 86-30-606/07/17 17:1010.0 1.4 1
N-Nitrosomethylethylamine ND ug/L 06/14/17 15:02 10595-95-606/07/17 17:1010.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 98 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-13 Lab ID:92342529002 Collected:05/31/17 03:30 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
N-Nitrosopiperidine ND ug/L 06/14/17 15:02 100-75-406/07/17 17:1020.0 1.7 1
N-Nitrosopyrrolidine ND ug/L 06/14/17 15:02 930-55-206/07/17 17:1010.0 1.7 1
O,O,O-Triethylphosphorothioate ND ug/L 06/14/17 15:02 126-68-106/07/17 17:1010.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/14/17 15:02 108-60-106/07/17 17:1010.0 1.8 1
Parathion (Ethyl parathion)ND ug/L 06/14/17 15:02 56-38-206/07/17 17:1010.0 1.5 1
Pentachlorobenzene ND ug/L 06/14/17 15:02 608-93-506/07/17 17:1010.0 1.5 1
Pentachloronitrobenzene ND ug/L 06/14/17 15:02 82-68-806/07/17 17:1020.0 1.7 1
Pentachlorophenol ND ug/L 06/14/17 15:02 87-86-506/07/17 17:1025.0 3.5 1
Phenacetin ND ug/L 06/14/17 15:02 62-44-206/07/17 17:1020.0 1.9 1
Phenanthrene ND ug/L 06/14/17 15:02 85-01-806/07/17 17:1010.0 1.6 1
Phenol ND ug/L 06/14/17 15:02 108-95-206/07/17 17:1010.0 1.3 1
p-Phenylenediamine ND ug/L 06/14/17 15:02 106-50-306/07/17 17:1010.0 2.2 1
Phorate ND ug/L 06/14/17 15:02 298-02-206/07/17 17:1010.0 1.7 1
Pronamide ND ug/L 06/14/17 15:02 23950-58-506/07/17 17:1010.0 2.0 1
Pyrene ND ug/L 06/14/17 15:02 129-00-006/07/17 17:1010.0 2.2 1
Safrole ND ug/L 06/14/17 15:02 94-59-706/07/17 17:1010.0 1.3 1
1,2,4,5-Tetrachlorobenzene ND ug/L 06/14/17 15:02 95-94-306/07/17 17:1010.0 1.3 1
2,3,4,6-Tetrachlorophenol ND ug/L 06/14/17 15:02 58-90-206/07/17 17:1010.0 2.9 1
Thionazin ND ug/L 06/14/17 15:02 297-97-206/07/17 17:1020.0 1.7 1
O-Toluidine ND ug/L 06/14/17 15:02 95-53-406/07/17 17:1010.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 06/14/17 15:02 95-95-406/07/17 17:1010.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/14/17 15:02 88-06-206/07/17 17:1010.0 1.4 1
1,3,5-Trinitrobenzene ND ug/L 06/14/17 15:02 99-35-406/07/17 17:1010.0 1.2 1
Surrogates
Nitrobenzene-d5 (S)73 %06/14/17 15:02 4165-60-006/07/17 17:1021-110 1
2-Fluorobiphenyl (S)88 %06/14/17 15:02 321-60-806/07/17 17:1027-110 1
Terphenyl-d14 (S)86 %06/14/17 15:02 1718-51-006/07/17 17:1031-107 1
Phenol-d6 (S)23 %06/14/17 15:02 13127-88-306/07/17 17:1010-110 1
2-Fluorophenol (S)37 %06/14/17 15:02 367-12-406/07/17 17:1012-110 1
2,4,6-Tribromophenol (S)82 %06/14/17 15:02 118-79-606/07/17 17:1027-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 12.9J ug/L 06/04/17 07:34 67-64-110010.0 1
Acetonitrile ND ug/L 06/04/17 07:34 75-05-855.0 2.2 1
Acrolein ND ug/L 06/04/17 07:34 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 06/04/17 07:34 107-13-12001.9 1
Allyl chloride ND ug/L 06/04/17 07:34 107-05-110.0 1.5 1
Benzene ND ug/L 06/04/17 07:34 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 07:34 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 07:34 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 07:34 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 07:34 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 07:34 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 07:34 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 07:34 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/17 07:34 108-90-73.0 0.23 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 99 of 241
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-13 Lab ID:92342529002 Collected:05/31/17 03:30 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Chloroethane ND ug/L 06/04/17 07:34 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 07:34 67-66-35.0 0.14 1
Chloromethane 0.16J ug/L 06/04/17 07:34 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/04/17 07:34 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 07:34 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 07:34 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 07:34 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 07:34 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 07:34 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/04/17 07:34 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/04/17 07:34 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 07:34 110-57-6 L11001.0 1
Dichlorodifluoromethane ND ug/L 06/04/17 07:34 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/04/17 07:34 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 07:34 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 07:34 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/17 07:34 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 07:34 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 07:34 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/04/17 07:34 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/04/17 07:34 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/04/17 07:34 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/04/17 07:34 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 07:34 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 07:34 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/04/17 07:34 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/04/17 07:34 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/04/17 07:34 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 07:34 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/04/17 07:34 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/04/17 07:34 126-98-71000.93 1
Methylene Chloride ND ug/L 06/04/17 07:34 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/04/17 07:34 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 07:34 108-10-11000.33 1
Naphthalene ND ug/L 06/04/17 07:34 91-20-310.0 0.24 1
Propionitrile ND ug/L 06/04/17 07:34 107-12-01503.6 1
Styrene ND ug/L 06/04/17 07:34 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 07:34 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 07:34 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 07:34 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 07:34 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/04/17 07:34 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/04/17 07:34 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 07:34 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 07:34 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 07:34 75-69-41.0 0.20 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Sample:MW-13 Lab ID:92342529002 Collected:05/31/17 03:30 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2,3-Trichloropropane ND ug/L 06/04/17 07:34 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 07:34 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 07:34 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/17 07:34 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)106 %06/04/17 07:34 460-00-470-130 1
1,2-Dichloroethane-d4 (S)88 %06/04/17 07:34 17060-07-070-130 1
Toluene-d8 (S)111 %06/04/17 07:34 2037-26-570-130 1
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 06/06/17 23:00 18496-25-810001001
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide 4.7J ug/L 06/07/17 13:30 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
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9800 Kincey Ave. Suite 100
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Page 101 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363241
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92342337001, 92342339001, 92342479001, 92342479002, 92342479003, 92342479004, 92342479005,
92342479006, 92342479007, 92342479009, 92342479010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2013873
Associated Lab Samples:92342337001, 92342339001, 92342479001, 92342479002, 92342479003, 92342479004, 92342479005,
92342479006, 92342479007, 92342479009, 92342479010
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 06/07/17 03:170.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2013874LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.42.5 94 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2013875MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342281010
2013876
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 92 75-12592 0 252.5ND 2.3 2.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 102 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363333
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92342479011, 92342479012, 92342479013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014275
Associated Lab Samples:92342479011, 92342479012, 92342479013
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 06/07/17 02:150.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014276LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.32.5 93 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014277MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342769001
2014278
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L M1125075-1250 25125NDNDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 103 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363457
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92342529001, 92342529002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2015058
Associated Lab Samples:92342529001, 92342529002
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 06/07/17 00:470.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2015059LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.42.5 96 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015060MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342619002
2015061
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 100 75-125101 1 252.5ND 2.5 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 104 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363006
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92342337001, 92342339001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2012403
Associated Lab Samples:92342337001, 92342339001
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 5.0 06/10/17 07:263.9
Arsenic ug/L ND 10.0 06/10/17 07:265.0
Barium ug/L ND 5.0 06/10/17 07:262.5
Beryllium ug/L ND 1.0 06/10/17 07:260.50
Cadmium ug/L ND 1.0 06/10/17 07:260.50
Chromium ug/L ND 5.0 06/10/17 07:262.5
Cobalt ug/L ND 5.0 06/10/17 07:262.5
Copper ug/L ND 5.0 06/10/17 07:262.5
Lead ug/L ND 5.0 06/10/17 07:262.5
Nickel ug/L ND 5.0 06/10/17 07:262.5
Selenium ug/L ND 10.0 06/10/17 07:265.0
Silver ug/L ND 5.0 06/10/17 07:262.5
Tin ug/L ND 5.0 06/10/17 07:262.5
Vanadium ug/L ND 5.0 06/10/17 07:262.5
Zinc ug/L ND 10.0 06/10/17 07:265.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012404LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 506500 101 80-120
Arsenic ug/L 485500 97 80-120
Barium ug/L 523500 105 80-120
Beryllium ug/L 500500 100 80-120
Cadmium ug/L 526500 105 80-120
Chromium ug/L 508500 102 80-120
Cobalt ug/L 514500 103 80-120
Copper ug/L 509500 102 80-120
Lead ug/L 509500 102 80-120
Nickel ug/L 515500 103 80-120
Selenium ug/L 513500 103 80-120
Silver ug/L 251250 101 80-120
Tin ug/L 514500 103 80-120
Vanadium ug/L 489500 98 80-120
Zinc ug/L 514500 103 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 105 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2012405MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342317001
2012406
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 101 75-125100 0 20500ND503501
Arsenic ug/L 500 96 75-12595 1 20500ND480475
Barium ug/L 500 103 75-125102 0 20500ND513511
Beryllium ug/L 500 98 75-12598 0 20500ND491490
Cadmium ug/L 500 104 75-125103 1 20500ND518516
Chromium ug/L 500 101 75-125100 0 20500ND504501
Cobalt ug/L 500 102 75-125101 0 20500ND509506
Copper ug/L M1500-52 75-125-52 0 20500761501501
Lead ug/L 500 97 75-12597 1 2050018.2 506 501
Nickel ug/L 500 102 75-125101 0 20500ND508506
Selenium ug/L 500 100 75-125100 0 20500ND504503
Silver ug/L 250 100 75-12599 1 20250ND251248
Tin ug/L 500 101 75-125101 1 205004.0J 511 508
Vanadium ug/L 500 97 75-12596 1 20500ND486482
Zinc ug/L M15001175-12510 1 20500455510507
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 106 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363009
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92342479001, 92342479002, 92342479003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2012414
Associated Lab Samples:92342479001, 92342479002, 92342479003
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 5.0 06/09/17 17:073.9
Arsenic ug/L ND 10.0 06/09/17 17:075.0
Barium ug/L ND 5.0 06/09/17 17:072.5
Beryllium ug/L ND 1.0 06/09/17 17:070.50
Cadmium ug/L ND 1.0 06/09/17 17:070.50
Chromium ug/L ND 5.0 06/09/17 17:072.5
Cobalt ug/L ND 5.0 06/09/17 17:072.5
Copper ug/L ND 5.0 06/09/17 17:072.5
Lead ug/L ND 5.0 06/09/17 17:072.5
Nickel ug/L ND 5.0 06/09/17 17:072.5
Selenium ug/L ND 10.0 06/09/17 17:075.0
Silver ug/L ND 5.0 06/09/17 17:072.5
Tin ug/L ND 5.0 06/09/17 17:072.5
Vanadium ug/L ND 5.0 06/09/17 17:072.5
Zinc ug/L ND 10.0 06/09/17 17:075.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012415LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 512500 102 80-120
Arsenic ug/L 488500 98 80-120
Barium ug/L 518500 104 80-120
Beryllium ug/L 518500 104 80-120
Cadmium ug/L 504500 101 80-120
Chromium ug/L 513500 103 80-120
Cobalt ug/L 520500 104 80-120
Copper ug/L 532500 106 80-120
Lead ug/L 504500 101 80-120
Nickel ug/L 507500 101 80-120
Selenium ug/L 490500 98 80-120
Silver ug/L 254250 102 80-120
Tin ug/L 518500 104 80-120
Vanadium ug/L 511500 102 80-120
Zinc ug/L 512500 102 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 107 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2012416MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342475013
2012417
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 98 75-125100 2 20500ND490502
Arsenic ug/L 500 95 75-12599 4 20500ND477494
Barium ug/L 500 102 75-125104 2 2050030.9 539 552
Beryllium ug/L 500 102 75-125105 3 205000.60J 510 524
Cadmium ug/L 500 99 75-125101 3 20500ND493505
Chromium ug/L 500 101 75-125104 3 205006.2 511 525
Cobalt ug/L 500 99 75-125103 3 20500ND499515
Copper ug/L 500 103 75-125106 3 205007.1 524 538
Lead ug/L 500 97 75-12599 2 205002.7J 486 498
Nickel ug/L 500 98 75-125101 3 205004.2J 492 507
Selenium ug/L 500 98 75-125101 2 20500ND496508
Silver ug/L 250 100 75-125102 2 20250ND251256
Tin ug/L 500 99 75-125102 3 205002.5J 498 513
Vanadium ug/L 500 100 75-125103 3 2050019.2 518 534
Zinc ug/L 500 100 75-125104 3 205009.5J 512 528
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 108 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363010
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92342479004, 92342479005, 92342479006, 92342479007, 92342479009, 92342479010, 92342479011,
92342479012, 92342479013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2012421
Associated Lab Samples:92342479004, 92342479005, 92342479006, 92342479007, 92342479009, 92342479010, 92342479011,
92342479012, 92342479013
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 5.0 06/09/17 14:553.9
Arsenic ug/L ND 10.0 06/09/17 14:555.0
Barium ug/L ND 5.0 06/11/17 04:042.5
Beryllium ug/L ND 1.0 06/11/17 04:040.50
Cadmium ug/L ND 1.0 06/09/17 14:550.50
Chromium ug/L ND 5.0 06/09/17 14:552.5
Cobalt ug/L ND 5.0 06/09/17 14:552.5
Copper ug/L ND 5.0 06/11/17 04:042.5
Lead ug/L ND 5.0 06/09/17 14:552.5
Nickel ug/L ND 5.0 06/09/17 14:552.5
Selenium ug/L ND 10.0 06/09/17 14:555.0
Silver ug/L ND 5.0 06/11/17 04:042.5
Tin ug/L ND 5.0 06/09/17 14:552.5
Vanadium ug/L ND 5.0 06/09/17 14:552.5
Zinc ug/L ND 10.0 06/09/17 14:555.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012422LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 506500 101 80-120
Arsenic ug/L 486500 97 80-120
Barium ug/L 507500 101 80-120
Beryllium ug/L 475500 95 80-120
Cadmium ug/L 500500 100 80-120
Chromium ug/L 500500 100 80-120
Cobalt ug/L 503500 101 80-120
Copper ug/L 500500 100 80-120
Lead ug/L 494500 99 80-120
Nickel ug/L 491500 98 80-120
Selenium ug/L 507500 101 80-120
Silver ug/L 248250 99 80-120
Tin ug/L 505500 101 80-120
Vanadium ug/L 495500 99 80-120
Zinc ug/L 503500 101 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 109 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2012423MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342479004
2012424
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 98 75-12597 1 20500ND492487
Arsenic ug/L 500 96 75-12594 1 20500ND481475
Barium ug/L 500 100 75-12597 3 2050069.9J 572 555
Beryllium ug/L 500 94 75-12599 6 20500ND469498
Cadmium ug/L 500 99 75-12597 2 205004.6 498 488
Chromium ug/L 500 99 75-12597 2 205003.1J 498 488
Cobalt ug/L 500 99 75-12597 2 20500ND497488
Copper ug/L 500 99 75-125100 2 20500ND496504
Lead ug/L 500 96 75-12595 2 20500ND485476
Nickel ug/L 500 97 75-12595 2 205002.5J 488 476
Selenium ug/L 500 100 75-12598 2 20500ND501491
Silver ug/L 250 97 75-12599 2 20250ND243248
Tin ug/L 500 100 75-12598 2 20500ND499490
Vanadium ug/L 500 98 75-12597 1 205005.3J 495 488
Zinc ug/L 500 99 75-12597 1 2050013.0 507 499
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 110 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363146
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92342529001, 92342529002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2013277
Associated Lab Samples:92342529001, 92342529002
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 5.0 06/09/17 20:333.9
Arsenic ug/L ND 10.0 06/09/17 20:335.0
Barium ug/L ND 5.0 06/09/17 20:332.5
Beryllium ug/L ND 1.0 06/09/17 20:330.50
Cadmium ug/L ND 1.0 06/09/17 20:330.50
Chromium ug/L ND 5.0 06/10/17 16:232.5
Cobalt ug/L ND 5.0 06/09/17 20:332.5
Copper ug/L ND 5.0 06/09/17 20:332.5
Lead ug/L ND 5.0 06/09/17 20:332.5
Nickel ug/L ND 5.0 06/10/17 16:232.5
Selenium ug/L ND 10.0 06/09/17 20:335.0
Silver ug/L ND 5.0 06/09/17 20:332.5
Tin ug/L ND 5.0 06/09/17 20:332.5
Vanadium ug/L ND 5.0 06/09/17 20:332.5
Zinc ug/L ND 10.0 06/09/17 20:335.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2013278LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 493500 99 80-120
Arsenic ug/L 474500 95 80-120
Barium ug/L 497500 99 80-120
Beryllium ug/L 497500 99 80-120
Cadmium ug/L 496500 99 80-120
Chromium ug/L 494500 99 80-120
Cobalt ug/L 494500 99 80-120
Copper ug/L 496500 99 80-120
Lead ug/L 489500 98 80-120
Nickel ug/L 485500 97 80-120
Selenium ug/L 495500 99 80-120
Silver ug/L 247250 99 80-120
Tin ug/L 492500 98 80-120
Vanadium ug/L 484500 97 80-120
Zinc ug/L 496500 99 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 111 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2013279MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342472012
2013280
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 98 75-125101 2 20500ND491503
Arsenic ug/L 500 94 75-12597 2 20500ND472483
Barium ug/L 500 98 75-125102 3 205000.091
mg/L 582 602
Beryllium ug/L 500 99 75-125102 3 20500ND494510
Cadmium ug/L 500 99 75-125101 2 20500ND495506
Chromium ug/L 500 99 75-125102 3 20500ND493508
Cobalt ug/L 500 98 75-125101 2 20500ND492503
Copper ug/L 500 99 75-125101 3 20500ND494508
Lead ug/L 500 97 75-12599 2 20500ND485496
Nickel ug/L 500 97 75-12599 2 205000.016
mg/L 500 510
Selenium ug/L 500 98 75-125101 3 20500ND490507
Silver ug/L 250 99 75-125101 2 20250ND247252
Tin ug/L 500 99 75-125100 2 20500ND494503
Vanadium ug/L 500 96 75-12599 3 20500ND482495
Zinc ug/L 500 98 75-125101 2 205000.066
mg/L 557 569
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 112 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
362966
EPA 3010A
EPA 6020B
6020 MET
Associated Lab Samples:92342479001, 92342479002, 92342479003, 92342479004, 92342479005, 92342479006, 92342479007,
92342479009, 92342479010, 92342479011, 92342479012, 92342479013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2012156
Associated Lab Samples:92342479001, 92342479002, 92342479003, 92342479004, 92342479005, 92342479006, 92342479007,
92342479009, 92342479010, 92342479011, 92342479012, 92342479013
Matrix:Water
AnalyzedMDL
Thallium ug/L ND 0.10 06/06/17 16:390.020
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012157LABORATORY CONTROL SAMPLE:
LCSSpike
Thallium ug/L 98.2100 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2012158MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342317005
2012159
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Thallium ug/L 100 95 75-12597 1 201000.048J 95.5 96.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 113 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363105
EPA 3010A
EPA 6020B
6020 MET
Associated Lab Samples:92342339001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2013133
Associated Lab Samples:92342339001
Matrix:Water
AnalyzedMDL
Thallium ug/L ND 0.10 06/06/17 15:320.020
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2013134LABORATORY CONTROL SAMPLE:
LCSSpike
Thallium ug/L 90.0100 90 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2013135MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342317006
2013136
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Thallium ug/L 100 100 75-12598 2 20100ND99.8 98.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 114 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363272
EPA 3010A
EPA 6020B
6020 MET
Associated Lab Samples:92342337001, 92342529001, 92342529002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014034
Associated Lab Samples:92342337001, 92342529001, 92342529002
Matrix:Water
AnalyzedMDL
Thallium ug/L ND 0.10 06/06/17 18:130.020
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014035LABORATORY CONTROL SAMPLE:
LCSSpike
Thallium ug/L 94.5100 95 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014036MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342297004
2014037
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Thallium ug/L 100 97 75-12595 2 201000.30J 97.2 95.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 115 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
362875
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92342337001, 92342339001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2011671
Associated Lab Samples:92342337001, 92342339001
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 05/31/17 15:180.33
1,1,1-Trichloroethane ug/L ND 1.0 05/31/17 15:180.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 05/31/17 15:180.40
1,1,2-Trichloroethane ug/L ND 1.0 05/31/17 15:180.29
1,1-Dichloroethane ug/L ND 5.0 05/31/17 15:180.32
1,1-Dichloroethene ug/L ND 5.0 05/31/17 15:180.56
1,1-Dichloropropene ug/L ND 5.0 05/31/17 15:180.49
1,2,3-Trichloropropane ug/L ND 1.0 05/31/17 15:180.41
1,2,4-Trichlorobenzene ug/L ND 10.0 05/31/17 15:180.35
1,2-Dibromo-3-chloropropane ug/L ND 13.0 05/31/17 15:182.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 05/31/17 15:180.27
1,2-Dichlorobenzene ug/L ND 5.0 05/31/17 15:180.30
1,2-Dichloroethane ug/L ND 1.0 05/31/17 15:180.24
1,2-Dichloropropane ug/L ND 1.0 05/31/17 15:180.27
1,3-Dichlorobenzene ug/L ND 5.0 05/31/17 15:180.24
1,3-Dichloropropane ug/L ND 1.0 05/31/17 15:180.28
1,4-Dichlorobenzene ug/L ND 1.0 05/31/17 15:180.33
2,2-Dichloropropane ug/L ND 15.0 05/31/17 15:180.13
2-Butanone (MEK)ug/L ND 100 05/31/17 15:180.96
2-Hexanone ug/L ND 50.0 05/31/17 15:180.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 05/31/17 15:180.33
Acetone ug/L ND 100 05/31/17 15:1810.0
Acetonitrile ug/L ND 55.0 05/31/17 15:182.2
Acrolein ug/L ND 53.0 05/31/17 15:181.6
Acrylonitrile ug/L ND 200 05/31/17 15:181.9
Allyl chloride ug/L ND 10.0 05/31/17 15:181.5
Benzene ug/L ND 1.0 05/31/17 15:180.25
Bromochloromethane ug/L ND 3.0 05/31/17 15:180.17
Bromodichloromethane ug/L ND 1.0 05/31/17 15:180.18
Bromoform ug/L ND 3.0 05/31/17 15:180.26
Bromomethane ug/L ND 10.0 05/31/17 15:180.29
Carbon disulfide ug/L ND 100 05/31/17 15:181.2
Carbon tetrachloride ug/L ND 1.0 05/31/17 15:180.25
Chlorobenzene ug/L ND 3.0 05/31/17 15:180.23
Chloroethane ug/L ND 10.0 05/31/17 15:180.54
Chloroform ug/L ND 5.0 05/31/17 15:180.14
Chloromethane ug/L ND 1.0 05/31/17 15:180.11
Chloroprene ug/L ND 20.0 05/31/17 15:180.27
cis-1,2-Dichloroethene ug/L ND 5.0 05/31/17 15:180.19
cis-1,3-Dichloropropene ug/L ND 1.0 05/31/17 15:180.13
Dibromochloromethane ug/L ND 3.0 05/31/17 15:180.21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 116 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2011671
Associated Lab Samples:92342337001, 92342339001
Matrix:Water
AnalyzedMDL
Dibromomethane ug/L ND 10.0 05/31/17 15:180.21
Dichlorodifluoromethane ug/L ND 5.0 05/31/17 15:180.21
Ethyl methacrylate ug/L ND 10.0 05/31/17 15:180.20
Ethylbenzene ug/L ND 1.0 05/31/17 15:180.30
Hexachloro-1,3-butadiene ug/L ND 10.0 05/31/17 15:180.71
Iodomethane ug/L ND 10.0 05/31/17 15:180.32
Isobutanol ug/L ND 100 05/31/17 15:1835.0
Methacrylonitrile ug/L ND 100 05/31/17 15:180.93
Methyl methacrylate ug/L ND 30.0 05/31/17 15:182.0
Methylene Chloride ug/L ND 1.0 05/31/17 15:180.97
Naphthalene ug/L ND 10.0 05/31/17 15:180.24
Propionitrile ug/L ND 150 05/31/17 15:183.6
Styrene ug/L ND 1.0 05/31/17 15:180.26
Tetrachloroethene ug/L ND 1.0 05/31/17 15:180.46
Toluene ug/L ND 1.0 05/31/17 15:180.26
trans-1,2-Dichloroethene ug/L ND 5.0 05/31/17 15:180.49
trans-1,3-Dichloropropene ug/L ND 1.0 05/31/17 15:180.26
trans-1,4-Dichloro-2-butene ug/L ND 100 05/31/17 15:181.0
Trichloroethene ug/L ND 1.0 05/31/17 15:180.47
Trichlorofluoromethane ug/L ND 1.0 05/31/17 15:180.20
Vinyl acetate ug/L ND 50.0 05/31/17 15:180.35
Vinyl chloride ug/L ND 1.0 05/31/17 15:180.62
Xylene (Total)ug/L ND 5.0 05/31/17 15:180.66
1,2-Dichloroethane-d4 (S)%104 70-130 05/31/17 15:18
4-Bromofluorobenzene (S)%101 70-130 05/31/17 15:18
Toluene-d8 (S)%108 70-130 05/31/17 15:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2011672LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 54.950 110 80-125
1,1,1-Trichloroethane ug/L 51.150 102 71-129
1,1,2,2-Tetrachloroethane ug/L 51.650 103 79-124
1,1,2-Trichloroethane ug/L 49.950 100 85-125
1,1-Dichloroethane ug/L 48.150 96 73-126
1,1-Dichloroethene ug/L 50.050 100 66-135
1,1-Dichloropropene ug/L 53.050 106 74-135
1,2,3-Trichloropropane ug/L 51.350 103 75-130
1,2,4-Trichlorobenzene ug/L 56.550 113 75-134
1,2-Dibromo-3-chloropropane ug/L 57.750 115 71-133
1,2-Dibromoethane (EDB)ug/L 55.050 110 83-124
1,2-Dichlorobenzene ug/L 52.650 105 80-133
1,2-Dichloroethane ug/L 49.650 99 67-128
1,2-Dichloropropane ug/L 53.450 107 75-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 117 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2011672LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 52.350 105 77-130
1,3-Dichloropropane ug/L 56.250 112 76-131
1,4-Dichlorobenzene ug/L 51.250 102 78-130
2,2-Dichloropropane ug/L 52.550 105 40-160
2-Butanone (MEK)ug/L 125100 125 61-144
2-Hexanone ug/L 119100 119 68-143
4-Methyl-2-pentanone (MIBK)ug/L 108100 108 72-135
Acetone ug/L 136100 136 48-146
Acetonitrile ug/L 581500 116 62-150
Acrolein ug/L 442 L125017724-160
Acrylonitrile ug/L 255250 102 40-160
Allyl chloride ug/L 45.450 91 66-137
Benzene ug/L 53.050 106 80-125
Bromochloromethane ug/L 49.250 98 71-125
Bromodichloromethane ug/L 53.250 106 78-124
Bromoform ug/L 45.350 91 71-128
Bromomethane ug/L 39.850 80 40-160
Carbon disulfide ug/L 52.6J50 105 50-160
Carbon tetrachloride ug/L 52.050 104 69-131
Chlorobenzene ug/L 51.350 103 81-122
Chloroethane ug/L 40.750 81 39-148
Chloroform ug/L 50.650 101 73-127
Chloromethane ug/L 53.750 107 44-146
Chloroprene ug/L 50.050 100 75-145
cis-1,2-Dichloroethene ug/L 49.050 98 74-124
cis-1,3-Dichloropropene ug/L 56.150 112 72-132
Dibromochloromethane ug/L 51.750 103 78-125
Dibromomethane ug/L 51.150 102 82-120
Dichlorodifluoromethane ug/L 40.250 80 34-157
Ethyl methacrylate ug/L 52.950 106 82-121
Ethylbenzene ug/L 52.050 104 79-121
Hexachloro-1,3-butadiene ug/L 60.050 120 72-131
Iodomethane ug/L 97.1100 97 39-154
Isobutanol ug/L 12601000 126 34-160
Methacrylonitrile ug/L 555500 111 74-134
Methyl methacrylate ug/L 52.150 104 84-124
Methylene Chloride ug/L 51.150 102 64-133
Naphthalene ug/L 57.950 116 73-133
Propionitrile ug/L 567500 113 73-140
Styrene ug/L 51.350 103 84-126
Tetrachloroethene ug/L 50.550 101 78-122
Toluene ug/L 49.250 98 80-121
trans-1,2-Dichloroethene ug/L 47.750 95 71-127
trans-1,3-Dichloropropene ug/L 57.350 115 69-141
trans-1,4-Dichloro-2-butene ug/L 98.6J L15019740-160
Trichloroethene ug/L 52.750 105 78-122
Trichlorofluoromethane ug/L 47.250 94 53-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 118 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2011672LABORATORY CONTROL SAMPLE:
LCSSpike
Vinyl acetate ug/L 118100 118 40-160
Vinyl chloride ug/L 45.450 91 58-137
Xylene (Total)ug/L 153150 102 81-126
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2011673MATRIX SPIKE SAMPLE:
MSSpike
Result
92342317002
1,1,1,2-Tetrachloroethane ug/L 23.720 118 70-130ND
1,1,1-Trichloroethane ug/L 22.520 112 70-130ND
1,1,2,2-Tetrachloroethane ug/L 19.420 97 70-130ND
1,1,2-Trichloroethane ug/L 21.020 105 70-130ND
1,1-Dichloroethane ug/L 22.120 111 70-130ND
1,1-Dichloroethene ug/L 23.220 116 70-166ND
1,1-Dichloropropene ug/L 23.520 117 70-130ND
1,2,3-Trichloropropane ug/L 19.220 96 70-130ND
1,2,4-Trichlorobenzene ug/L 23.820 119 70-130ND
1,2-Dibromo-3-chloropropane ug/L 26.020 130 70-130ND
1,2-Dibromoethane (EDB)ug/L 23.720 118 70-130ND
1,2-Dichlorobenzene ug/L 22.020 110 70-130ND
1,2-Dichloroethane ug/L 21.520 107 70-130ND
1,2-Dichloropropane ug/L 23.420 117 70-130ND
1,3-Dichlorobenzene ug/L 21.920 109 70-130ND
1,3-Dichloropropane ug/L 24.620 123 70-130ND
1,4-Dichlorobenzene ug/L 22.320 111 70-130ND
2,2-Dichloropropane ug/L 21.720 109 70-130ND
2-Butanone (MEK)ug/L 49.2J40 123 70-130ND
2-Hexanone ug/L 54.1 M14013570-130ND
4-Methyl-2-pentanone (MIBK)ug/L 48.6J40 121 70-130ND
Acetone ug/L 65.4J40 124 70-13015.8J
Acetonitrile ug/L 271 M120013670-130ND
Acrolein ug/L 179 M010017970-130ND
Acrylonitrile ug/L 118J100 118 70-130ND
Allyl chloride ug/L 21.220 98 70-130ND
Benzene ug/L 23.420 117 70-148ND
Bromochloromethane ug/L 23.320 116 70-130ND
Bromodichloromethane ug/L 23.720 119 70-130ND
Bromoform ug/L 19.520 98 70-130ND
Bromomethane ug/L 13.1 M1206670-130ND
Carbon disulfide ug/L 23.0J20 115 70-130ND
Carbon tetrachloride ug/L 23.320 116 70-130ND
Chlorobenzene ug/L 22.920 114 70-146ND
Chloroethane ug/L 20.720 103 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 119 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2011673MATRIX SPIKE SAMPLE:
MSSpike
Result
92342317002
Chloroform ug/L 23.120 116 70-130ND
Chloromethane ug/L 23.320 116 70-130ND
Chloroprene ug/L 23.220 116 70-130ND
cis-1,2-Dichloroethene ug/L 22.220 111 70-130ND
cis-1,3-Dichloropropene ug/L 22.720 114 70-130ND
Dibromochloromethane ug/L 21.720 108 70-130ND
Dibromomethane ug/L 23.320 117 70-130ND
Dichlorodifluoromethane ug/L 18.820 94 70-130ND
Ethyl methacrylate ug/L 23.620 118 70-130ND
Ethylbenzene ug/L 23.720 118 70-130ND
Hexachloro-1,3-butadiene ug/L 22.720 114 70-130ND
Iodomethane ug/L 35.740 89 70-130ND
Isobutanol ug/L 543 M140013670-130ND
Methacrylonitrile ug/L 239200 120 70-130ND
Methyl methacrylate ug/L 22.5J20 112 70-130ND
Methylene Chloride ug/L 22.620 113 70-130ND
Naphthalene ug/L 23.620 118 70-130ND
Propionitrile ug/L 261 M120013170-130ND
Styrene ug/L 22.520 112 70-130ND
Tetrachloroethene ug/L 22.920 114 70-130ND
Toluene ug/L 21.820 109 70-155ND
trans-1,2-Dichloroethene ug/L 22.220 111 70-130ND
trans-1,3-Dichloropropene ug/L 23.320 116 70-130ND
trans-1,4-Dichloro-2-butene ug/L 19.6J20 98 70-130ND
Trichloroethene ug/L 22.720 114 69-151ND
Trichlorofluoromethane ug/L 23.220 116 70-130ND
Vinyl acetate ug/L 42.4J40 106 70-130ND
Vinyl chloride ug/L 21.220 106 70-130ND
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%91 70-130
Toluene-d8 (S)%96 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342317003
2011674SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 120 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342317003
2011674SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acetonitrile ug/L ND 30ND
Acrolein ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Allyl chloride ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
Chloroprene ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L 1.3J 16 301.5
Ethyl methacrylate ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Isobutanol ug/L ND 30ND
Methacrylonitrile ug/L ND 30ND
Methyl methacrylate ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
Propionitrile ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 121 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342317003
2011674SAMPLE DUPLICATE:
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L 1.1 22 301.4
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%108 8100
4-Bromofluorobenzene (S)%104 2106
Toluene-d8 (S)%87 21108
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 122 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363024
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92342479001, 92342479002, 92342479003, 92342479004, 92342479005, 92342479006, 92342479007,
92342479009, 92342479010, 92342479011, 92342479012, 92342479013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2012502
Associated Lab Samples:92342479001, 92342479002, 92342479003, 92342479004, 92342479005, 92342479006, 92342479007,
92342479009, 92342479010, 92342479011, 92342479012, 92342479013
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/02/17 00:550.33
1,1,1-Trichloroethane ug/L ND 1.0 06/02/17 00:550.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 06/02/17 00:550.40
1,1,2-Trichloroethane ug/L ND 1.0 06/02/17 00:550.29
1,1-Dichloroethane ug/L ND 5.0 06/02/17 00:550.32
1,1-Dichloroethene ug/L ND 5.0 06/02/17 00:550.56
1,1-Dichloropropene ug/L ND 5.0 06/02/17 00:550.49
1,2,3-Trichloropropane ug/L ND 1.0 06/02/17 00:550.41
1,2,4-Trichlorobenzene ug/L ND 10.0 06/02/17 00:550.35
1,2-Dibromo-3-chloropropane ug/L ND 13.0 06/02/17 00:552.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/02/17 00:550.27
1,2-Dichlorobenzene ug/L ND 5.0 06/02/17 00:550.30
1,2-Dichloroethane ug/L ND 1.0 06/02/17 00:550.24
1,2-Dichloropropane ug/L ND 1.0 06/02/17 00:550.27
1,3-Dichlorobenzene ug/L ND 5.0 06/02/17 00:550.24
1,3-Dichloropropane ug/L ND 1.0 06/02/17 00:550.28
1,4-Dichlorobenzene ug/L ND 1.0 06/02/17 00:550.33
2,2-Dichloropropane ug/L ND 15.0 06/02/17 00:550.13
2-Butanone (MEK)ug/L ND 100 06/02/17 00:550.96
2-Hexanone ug/L ND 50.0 06/02/17 00:550.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 06/02/17 00:550.33
Acetone ug/L ND 100 06/02/17 00:5510.0
Acetonitrile ug/L ND 55.0 06/02/17 00:552.2
Acrolein ug/L ND 53.0 06/02/17 00:551.6
Acrylonitrile ug/L ND 200 06/02/17 00:551.9
Allyl chloride ug/L ND 10.0 06/02/17 00:551.5
Benzene ug/L ND 1.0 06/02/17 00:550.25
Bromochloromethane ug/L ND 3.0 06/02/17 00:550.17
Bromodichloromethane ug/L ND 1.0 06/02/17 00:550.18
Bromoform ug/L ND 3.0 06/02/17 00:550.26
Bromomethane ug/L ND 10.0 06/02/17 00:550.29
Carbon disulfide ug/L ND 100 06/02/17 00:551.2
Carbon tetrachloride ug/L ND 1.0 06/02/17 00:550.25
Chlorobenzene ug/L ND 3.0 06/02/17 00:550.23
Chloroethane ug/L ND 10.0 06/02/17 00:550.54
Chloroform ug/L ND 5.0 06/02/17 00:550.14
Chloromethane ug/L ND 1.0 06/02/17 00:550.11
Chloroprene ug/L ND 20.0 06/02/17 00:550.27
cis-1,2-Dichloroethene ug/L ND 5.0 06/02/17 00:550.19
cis-1,3-Dichloropropene ug/L ND 1.0 06/02/17 00:550.13
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 123 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2012502
Associated Lab Samples:92342479001, 92342479002, 92342479003, 92342479004, 92342479005, 92342479006, 92342479007,
92342479009, 92342479010, 92342479011, 92342479012, 92342479013
Matrix:Water
AnalyzedMDL
Dibromochloromethane ug/L ND 3.0 06/02/17 00:550.21
Dibromomethane ug/L ND 10.0 06/02/17 00:550.21
Dichlorodifluoromethane ug/L ND 5.0 06/02/17 00:550.21
Ethyl methacrylate ug/L ND 10.0 06/02/17 00:550.20
Ethylbenzene ug/L ND 1.0 06/02/17 00:550.30
Hexachloro-1,3-butadiene ug/L ND 10.0 06/02/17 00:550.71
Iodomethane ug/L ND 10.0 06/02/17 00:550.32
Isobutanol ug/L ND 100 06/02/17 00:5535.0
Methacrylonitrile ug/L ND 100 06/02/17 00:550.93
Methyl methacrylate ug/L ND 30.0 06/02/17 00:552.0
Methylene Chloride ug/L ND 1.0 06/02/17 00:550.97
Naphthalene ug/L ND 10.0 06/02/17 00:550.24
Propionitrile ug/L ND 150 06/02/17 00:553.6
Styrene ug/L ND 1.0 06/02/17 00:550.26
Tetrachloroethene ug/L ND 1.0 06/02/17 00:550.46
Toluene ug/L ND 1.0 06/02/17 00:550.26
trans-1,2-Dichloroethene ug/L ND 5.0 06/02/17 00:550.49
trans-1,3-Dichloropropene ug/L ND 1.0 06/02/17 00:550.26
trans-1,4-Dichloro-2-butene ug/L ND 100 06/02/17 00:551.0
Trichloroethene ug/L ND 1.0 06/02/17 00:550.47
Trichlorofluoromethane ug/L ND 1.0 06/02/17 00:550.20
Vinyl acetate ug/L ND 50.0 06/02/17 00:550.35
Vinyl chloride ug/L ND 1.0 06/02/17 00:550.62
Xylene (Total)ug/L ND 5.0 06/02/17 00:550.66
1,2-Dichloroethane-d4 (S)%99 70-130 06/02/17 00:55
4-Bromofluorobenzene (S)%115 70-130 06/02/17 00:55
Toluene-d8 (S)%110 70-130 06/02/17 00:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012503LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.950 102 80-125
1,1,1-Trichloroethane ug/L 46.350 93 71-129
1,1,2,2-Tetrachloroethane ug/L 54.250 108 79-124
1,1,2-Trichloroethane ug/L 50.150 100 85-125
1,1-Dichloroethane ug/L 44.050 88 73-126
1,1-Dichloroethene ug/L 38.450 77 66-135
1,1-Dichloropropene ug/L 50.350 101 74-135
1,2,3-Trichloropropane ug/L 54.550 109 75-130
1,2,4-Trichlorobenzene ug/L 43.150 86 75-134
1,2-Dibromo-3-chloropropane ug/L 46.850 94 71-133
1,2-Dibromoethane (EDB)ug/L 51.850 104 83-124
1,2-Dichlorobenzene ug/L 45.750 91 80-133
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 124 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012503LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloroethane ug/L 44.150 88 67-128
1,2-Dichloropropane ug/L 47.550 95 75-132
1,3-Dichlorobenzene ug/L 46.750 93 77-130
1,3-Dichloropropane ug/L 52.150 104 76-131
1,4-Dichlorobenzene ug/L 46.850 94 78-130
2,2-Dichloropropane ug/L 42.650 85 40-160
2-Butanone (MEK)ug/L 105100 105 61-144
2-Hexanone ug/L 99.7100 100 68-143
4-Methyl-2-pentanone (MIBK)ug/L 103100 103 72-135
Acetone ug/L 107100 107 48-146
Acetonitrile ug/L 527500 105 62-150
Acrolein ug/L 280250 112 24-160
Acrylonitrile ug/L 234250 94 40-160
Allyl chloride ug/L 41.550 83 66-137
Benzene ug/L 47.550 95 80-125
Bromochloromethane ug/L 45.750 91 71-125
Bromodichloromethane ug/L 47.150 94 78-124
Bromoform ug/L 57.550 115 71-128
Bromomethane ug/L 50.350 101 40-160
Carbon disulfide ug/L 40.5J50 81 50-160
Carbon tetrachloride ug/L 47.050 94 69-131
Chlorobenzene ug/L 46.650 93 81-122
Chloroethane ug/L 46.950 94 39-148
Chloroform ug/L 42.950 86 73-127
Chloromethane ug/L 52.850 106 44-146
Chloroprene ug/L 46.050 92 75-145
cis-1,2-Dichloroethene ug/L 45.450 91 74-124
cis-1,3-Dichloropropene ug/L 50.650 101 72-132
Dibromochloromethane ug/L 53.650 107 78-125
Dibromomethane ug/L 45.150 90 82-120
Dichlorodifluoromethane ug/L 39.350 79 34-157
Ethyl methacrylate ug/L 52.150 104 82-121
Ethylbenzene ug/L 48.150 96 79-121
Hexachloro-1,3-butadiene ug/L 44.250 88 72-131
Iodomethane ug/L 71.3100 71 39-154
Isobutanol ug/L 10501000 105 34-160
Methacrylonitrile ug/L 520500 104 74-134
Methyl methacrylate ug/L 46.950 94 84-124
Methylene Chloride ug/L 48.250 96 64-133
Naphthalene ug/L 45.250 90 73-133
Propionitrile ug/L 503500 101 73-140
Styrene ug/L 51.050 102 84-126
Tetrachloroethene ug/L 49.050 98 78-122
Toluene ug/L 48.250 96 80-121
trans-1,2-Dichloroethene ug/L 44.550 89 71-127
trans-1,3-Dichloropropene ug/L 53.150 106 69-141
trans-1,4-Dichloro-2-butene ug/L 63.5J50 127 40-160
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 125 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012503LABORATORY CONTROL SAMPLE:
LCSSpike
Trichloroethene ug/L 48.850 98 78-122
Trichlorofluoromethane ug/L 45.950 92 53-137
Vinyl acetate ug/L 92.9100 93 40-160
Vinyl chloride ug/L 41.950 84 58-137
Xylene (Total)ug/L 147150 98 81-126
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%113 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2012504MATRIX SPIKE SAMPLE:
MSSpike
Result
92342478001
1,1,1,2-Tetrachloroethane ug/L 19.520 98 70-130ND
1,1,1-Trichloroethane ug/L 22.420 112 70-130ND
1,1,2,2-Tetrachloroethane ug/L 21.420 107 70-130ND
1,1,2-Trichloroethane ug/L 18.020 90 70-130ND
1,1-Dichloroethane ug/L 21.820 109 70-130ND
1,1-Dichloroethene ug/L 25.920 129 70-166ND
1,1-Dichloropropene ug/L 22.920 114 70-130ND
1,2,3-Trichloropropane ug/L 20.920 105 70-130ND
1,2,4-Trichlorobenzene ug/L 18.520 92 70-130ND
1,2-Dibromo-3-chloropropane ug/L 16.920 85 70-130ND
1,2-Dibromoethane (EDB)ug/L 16.920 85 70-130ND
1,2-Dichlorobenzene ug/L 19.720 98 70-130ND
1,2-Dichloroethane ug/L 19.820 99 70-130ND
1,2-Dichloropropane ug/L 21.120 105 70-130ND
1,3-Dichlorobenzene ug/L 19.920 99 70-130ND
1,3-Dichloropropane ug/L 16.920 85 70-130ND
1,4-Dichlorobenzene ug/L 19.920 99 70-130ND
2,2-Dichloropropane ug/L 17.220 86 70-130ND
2-Butanone (MEK)ug/L 32.6J40 82 70-130ND
2-Hexanone ug/L 31.4J40 78 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 30.1J40 75 70-130ND
Acetone ug/L 39.6J40 99 70-130ND
Acetonitrile ug/L 182200 91 70-130ND
Acrolein ug/L 110100 110 70-130ND
Acrylonitrile ug/L 94.7J100 95 70-130ND
Allyl chloride ug/L 21.220 106 70-130ND
Benzene ug/L 21.020 105 70-148ND
Bromochloromethane ug/L 22.220 111 70-130ND
Bromodichloromethane ug/L 20.620 103 70-130ND
Bromoform ug/L 20.120 100 70-130ND
Bromomethane ug/L 22.620 113 70-130ND
Carbon disulfide ug/L 25.5J20 127 70-130ND
Carbon tetrachloride ug/L 21.620 108 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 126 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2012504MATRIX SPIKE SAMPLE:
MSSpike
Result
92342478001
Chlorobenzene ug/L 20.520 102 70-146ND
Chloroethane ug/L 23.920 119 70-130ND
Chloroform ug/L 20.520 102 70-130ND
Chloromethane ug/L 26.6 M12013370-130ND
Chloroprene ug/L 20.920 105 70-130ND
cis-1,2-Dichloroethene ug/L 22.120 110 70-130ND
cis-1,3-Dichloropropene ug/L 16.120 80 70-130ND
Dibromochloromethane ug/L 16.720 83 70-130ND
Dibromomethane ug/L 19.520 98 70-130ND
Dichlorodifluoromethane ug/L 17.420 87 70-130ND
Ethyl methacrylate ug/L 15.220 76 70-130ND
Ethylbenzene ug/L 21.720 109 70-130ND
Hexachloro-1,3-butadiene ug/L 18.920 94 70-130ND
Iodomethane ug/L 42.440 106 70-130ND
Isobutanol ug/L 301400 75 70-130ND
Methacrylonitrile ug/L 188200 94 70-130ND
Methyl methacrylate ug/L 17.4J20 87 70-130ND
Methylene Chloride ug/L 21.720 108 70-130ND
Naphthalene ug/L 17.820 89 70-130ND
Propionitrile ug/L 188200 94 70-130ND
Styrene ug/L 22.420 112 70-130ND
Tetrachloroethene ug/L 17.220 86 70-130ND
Toluene ug/L 18.620 93 70-155ND
trans-1,2-Dichloroethene ug/L 21.820 109 70-130ND
trans-1,3-Dichloropropene ug/L 17.120 85 70-130ND
trans-1,4-Dichloro-2-butene ug/L 18.9J20 94 70-130ND
Trichloroethene ug/L 21.920 109 69-151ND
Trichlorofluoromethane ug/L 23.620 118 70-130ND
Vinyl acetate ug/L 25.4J M1406470-130ND
Vinyl chloride ug/L 21.320 106 70-130ND
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%116 70-130
Toluene-d8 (S)%85 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342478002
2012505SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 0.48J 300.43J
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 127 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342478002
2012505SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acetonitrile ug/L ND 30ND
Acrolein ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Allyl chloride ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
Chloroprene ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 0.43J 300.39J
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Ethyl methacrylate ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Isobutanol ug/L ND 30ND
Methacrylonitrile ug/L ND 30ND
Methyl methacrylate ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
Propionitrile ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 128 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342478002
2012505SAMPLE DUPLICATE:
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%103 3100
4-Bromofluorobenzene (S)%114 1113
Toluene-d8 (S)%113 1111
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 129 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363307
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92342529002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014180
Associated Lab Samples:92342529002
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/04/17 06:410.33
1,1,1-Trichloroethane ug/L ND 1.0 06/04/17 06:410.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 06/04/17 06:410.40
1,1,2-Trichloroethane ug/L ND 1.0 06/04/17 06:410.29
1,1-Dichloroethane ug/L ND 5.0 06/04/17 06:410.32
1,1-Dichloroethene ug/L ND 5.0 06/04/17 06:410.56
1,1-Dichloropropene ug/L ND 5.0 06/04/17 06:410.49
1,2,3-Trichloropropane ug/L ND 1.0 06/04/17 06:410.41
1,2,4-Trichlorobenzene ug/L ND 10.0 06/04/17 06:410.35
1,2-Dibromo-3-chloropropane ug/L ND 13.0 06/04/17 06:412.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/04/17 06:410.27
1,2-Dichlorobenzene ug/L ND 5.0 06/04/17 06:410.30
1,2-Dichloroethane ug/L ND 1.0 06/04/17 06:410.24
1,2-Dichloropropane ug/L ND 1.0 06/04/17 06:410.27
1,3-Dichlorobenzene ug/L ND 5.0 06/04/17 06:410.24
1,3-Dichloropropane ug/L ND 1.0 06/04/17 06:410.28
1,4-Dichlorobenzene ug/L ND 1.0 06/04/17 06:410.33
2,2-Dichloropropane ug/L ND 15.0 06/04/17 06:410.13
2-Butanone (MEK)ug/L ND 100 06/04/17 06:410.96
2-Hexanone ug/L ND 50.0 06/04/17 06:410.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 06/04/17 06:410.33
Acetone ug/L ND 100 06/04/17 06:4110.0
Acetonitrile ug/L ND 55.0 06/04/17 06:412.2
Acrolein ug/L ND 53.0 06/04/17 06:411.6
Acrylonitrile ug/L ND 200 06/04/17 06:411.9
Allyl chloride ug/L ND 10.0 06/04/17 06:411.5
Benzene ug/L ND 1.0 06/04/17 06:410.25
Bromochloromethane ug/L ND 3.0 06/04/17 06:410.17
Bromodichloromethane ug/L ND 1.0 06/04/17 06:410.18
Bromoform ug/L ND 3.0 06/04/17 06:410.26
Bromomethane ug/L ND 10.0 06/04/17 06:410.29
Carbon disulfide ug/L ND 100 06/04/17 06:411.2
Carbon tetrachloride ug/L ND 1.0 06/04/17 06:410.25
Chlorobenzene ug/L ND 3.0 06/04/17 06:410.23
Chloroethane ug/L ND 10.0 06/04/17 06:410.54
Chloroform ug/L ND 5.0 06/04/17 06:410.14
Chloromethane ug/L ND 1.0 06/04/17 06:410.11
Chloroprene ug/L ND 20.0 06/04/17 06:410.27
cis-1,2-Dichloroethene ug/L ND 5.0 06/04/17 06:410.19
cis-1,3-Dichloropropene ug/L ND 1.0 06/04/17 06:410.13
Dibromochloromethane ug/L ND 3.0 06/04/17 06:410.21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 130 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014180
Associated Lab Samples:92342529002
Matrix:Water
AnalyzedMDL
Dibromomethane ug/L ND 10.0 06/04/17 06:410.21
Dichlorodifluoromethane ug/L ND 5.0 06/04/17 06:410.21
Ethyl methacrylate ug/L ND 10.0 06/04/17 06:410.20
Ethylbenzene ug/L ND 1.0 06/04/17 06:410.30
Hexachloro-1,3-butadiene ug/L 1.6J 10.0 06/04/17 06:410.71
Iodomethane ug/L ND 10.0 06/04/17 06:410.32
Isobutanol ug/L ND 100 06/04/17 06:4135.0
Methacrylonitrile ug/L ND 100 06/04/17 06:410.93
Methyl methacrylate ug/L ND 30.0 06/04/17 06:412.0
Methylene Chloride ug/L ND 1.0 06/04/17 06:410.97
Naphthalene ug/L ND 10.0 06/04/17 06:410.24
Propionitrile ug/L ND 150 06/04/17 06:413.6
Styrene ug/L ND 1.0 06/04/17 06:410.26
Tetrachloroethene ug/L ND 1.0 06/04/17 06:410.46
Toluene ug/L ND 1.0 06/04/17 06:410.26
trans-1,2-Dichloroethene ug/L ND 5.0 06/04/17 06:410.49
trans-1,3-Dichloropropene ug/L ND 1.0 06/04/17 06:410.26
trans-1,4-Dichloro-2-butene ug/L ND 100 06/04/17 06:411.0
Trichloroethene ug/L ND 1.0 06/04/17 06:410.47
Trichlorofluoromethane ug/L ND 1.0 06/04/17 06:410.20
Vinyl acetate ug/L ND 50.0 06/04/17 06:410.35
Vinyl chloride ug/L ND 1.0 06/04/17 06:410.62
Xylene (Total)ug/L ND 5.0 06/04/17 06:410.66
1,2-Dichloroethane-d4 (S)%89 70-130 06/04/17 06:41
4-Bromofluorobenzene (S)%113 70-130 06/04/17 06:41
Toluene-d8 (S)%106 70-130 06/04/17 06:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014181LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.150 100 80-125
1,1,1-Trichloroethane ug/L 48.850 98 71-129
1,1,2,2-Tetrachloroethane ug/L 57.050 114 79-124
1,1,2-Trichloroethane ug/L 51.150 102 85-125
1,1-Dichloroethane ug/L 49.950 100 73-126
1,1-Dichloroethene ug/L 44.750 89 66-135
1,1-Dichloropropene ug/L 49.950 100 74-135
1,2,3-Trichloropropane ug/L 47.350 95 75-130
1,2,4-Trichlorobenzene ug/L 48.050 96 75-134
1,2-Dibromo-3-chloropropane ug/L 48.750 97 71-133
1,2-Dibromoethane (EDB)ug/L 56.350 113 83-124
1,2-Dichlorobenzene ug/L 50.950 102 80-133
1,2-Dichloroethane ug/L 45.750 91 67-128
1,2-Dichloropropane ug/L 54.450 109 75-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 131 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014181LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 48.350 97 77-130
1,3-Dichloropropane ug/L 54.650 109 76-131
1,4-Dichlorobenzene ug/L 47.750 95 78-130
2,2-Dichloropropane ug/L 44.650 89 40-160
2-Butanone (MEK)ug/L 136100 136 61-144
2-Hexanone ug/L 110100 110 68-143
4-Methyl-2-pentanone (MIBK)ug/L 109100 109 72-135
Acetone ug/L 116100 116 48-146
Acetonitrile ug/L 541500 108 62-150
Acrolein ug/L 336250 134 24-160
Acrylonitrile ug/L 274250 110 40-160
Allyl chloride ug/L 47.150 94 66-137
Benzene ug/L 52.550 105 80-125
Bromochloromethane ug/L 47.850 96 71-125
Bromodichloromethane ug/L 49.350 99 78-124
Bromoform ug/L 48.150 96 71-128
Bromomethane ug/L 41.950 84 40-160
Carbon disulfide ug/L 50.8J50 102 50-160
Carbon tetrachloride ug/L 44.550 89 69-131
Chlorobenzene ug/L 51.450 103 81-122
Chloroethane ug/L 43.750 87 39-148
Chloroform ug/L 48.350 97 73-127
Chloromethane ug/L 53.850 108 44-146
Chloroprene ug/L 47.050 94 75-145
cis-1,2-Dichloroethene ug/L 51.050 102 74-124
cis-1,3-Dichloropropene ug/L 53.850 108 72-132
Dibromochloromethane ug/L 47.750 95 78-125
Dibromomethane ug/L 48.550 97 82-120
Dichlorodifluoromethane ug/L 41.350 83 34-157
Ethyl methacrylate ug/L 46.650 93 82-121
Ethylbenzene ug/L 50.350 101 79-121
Hexachloro-1,3-butadiene ug/L 41.650 83 72-131
Iodomethane ug/L 95.3100 95 39-154
Isobutanol ug/L 12001000 120 34-160
Methacrylonitrile ug/L 566500 113 74-134
Methyl methacrylate ug/L 50.850 102 84-124
Methylene Chloride ug/L 49.950 100 64-133
Naphthalene ug/L 52.950 106 73-133
Propionitrile ug/L 623500 125 73-140
Styrene ug/L 49.750 99 84-126
Tetrachloroethene ug/L 45.950 92 78-122
Toluene ug/L 49.650 99 80-121
trans-1,2-Dichloroethene ug/L 51.450 103 71-127
trans-1,3-Dichloropropene ug/L 53.350 107 69-141
trans-1,4-Dichloro-2-butene ug/L 94.0J L15018840-160
Trichloroethene ug/L 50.650 101 78-122
Trichlorofluoromethane ug/L 45.050 90 53-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 132 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014181LABORATORY CONTROL SAMPLE:
LCSSpike
Vinyl acetate ug/L 96.4100 96 40-160
Vinyl chloride ug/L 45.150 90 58-137
Xylene (Total)ug/L 141150 94 81-126
1,2-Dichloroethane-d4 (S)%90 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2014183MATRIX SPIKE SAMPLE:
MSSpike
Result
92342730006
1,1,1,2-Tetrachloroethane ug/L 19.120 96 70-130ND
1,1,1-Trichloroethane ug/L 22.520 112 70-130ND
1,1,2,2-Tetrachloroethane ug/L 22.020 110 70-130ND
1,1,2-Trichloroethane ug/L 20.120 100 70-130ND
1,1-Dichloroethane ug/L 22.320 112 70-130ND
1,1-Dichloroethene ug/L 23.020 115 70-166ND
1,1-Dichloropropene ug/L 24.220 121 70-130ND
1,2,3-Trichloropropane ug/L 18.120 90 70-130ND
1,2,4-Trichlorobenzene ug/L 19.220 96 70-130ND
1,2-Dibromo-3-chloropropane ug/L 18.920 94 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.120 106 70-130ND
1,2-Dichlorobenzene ug/L 21.220 106 70-130ND
1,2-Dichloroethane ug/L 20.320 101 70-130ND
1,2-Dichloropropane ug/L 22.920 115 70-130ND
1,3-Dichlorobenzene ug/L 20.020 100 70-130ND
1,3-Dichloropropane ug/L 20.620 103 70-130ND
1,4-Dichlorobenzene ug/L 20.220 101 70-130ND
2,2-Dichloropropane ug/L 22.220 111 70-130ND
2-Butanone (MEK)ug/L 46.6J40 116 70-130ND
2-Hexanone ug/L 44.9J40 112 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 42.0J40 105 70-130ND
Acetone ug/L 49.1J40 94 70-13011.6J
Acetonitrile ug/L 232200 116 70-130ND
Acrolein ug/L 128100 128 70-130ND
Acrylonitrile ug/L 113J100 113 70-130ND
Allyl chloride ug/L 23.220 116 70-130ND
Benzene ug/L 23.220 116 70-148ND
Bromochloromethane ug/L 20.920 105 70-130ND
Bromodichloromethane ug/L 21.320 106 70-130ND
Bromoform ug/L 17.320 86 70-130ND
Bromomethane ug/L 22.420 112 70-130ND
Carbon disulfide ug/L 23.6J20 118 70-130ND
Carbon tetrachloride ug/L 21.020 105 70-130ND
Chlorobenzene ug/L 22.020 110 70-146ND
Chloroethane ug/L 20.920 104 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 133 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2014183MATRIX SPIKE SAMPLE:
MSSpike
Result
92342730006
Chloroform ug/L 22.820 114 70-130ND
Chloromethane ug/L 24.620 123 70-130ND
Chloroprene ug/L 21.820 109 70-130ND
cis-1,2-Dichloroethene ug/L 22.820 114 70-130ND
cis-1,3-Dichloropropene ug/L 22.420 112 70-130ND
Dibromochloromethane ug/L 19.520 98 70-130ND
Dibromomethane ug/L 21.820 109 70-130ND
Dichlorodifluoromethane ug/L 18.220 91 70-130ND
Ethyl methacrylate ug/L 20.420 102 70-130ND
Ethylbenzene ug/L 22.320 112 70-130ND
Hexachloro-1,3-butadiene ug/L 20.520 103 70-130ND
Iodomethane ug/L 41.240 103 70-130ND
Isobutanol ug/L 463400 116 70-130ND
Methacrylonitrile ug/L 217200 108 70-130ND
Methyl methacrylate ug/L 19.4J20 97 70-130ND
Methylene Chloride ug/L 21.820 109 70-130ND
Naphthalene ug/L 22.620 113 70-130ND
Propionitrile ug/L 228200 114 70-130ND
Styrene ug/L 20.920 104 70-130ND
Tetrachloroethene ug/L 20.820 104 70-130ND
Toluene ug/L 22.520 113 70-155ND
trans-1,2-Dichloroethene ug/L 23.920 119 70-130ND
trans-1,3-Dichloropropene ug/L 22.720 114 70-130ND
trans-1,4-Dichloro-2-butene ug/L 28.2J M02014170-130ND
Trichloroethene ug/L 22.520 112 69-151ND
Trichlorofluoromethane ug/L 21.720 109 70-130ND
Vinyl acetate ug/L 40.5J40 101 70-130ND
Vinyl chloride ug/L 21.220 106 70-130ND
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%104 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342730005
2014182SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 134 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342730005
2014182SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L 13.6J 30ND
Acetonitrile ug/L ND 30ND
Acrolein ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Allyl chloride ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L 0.16J 300.13J
Chloroprene ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Ethyl methacrylate ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Isobutanol ug/L ND 30ND
Methacrylonitrile ug/L ND 30ND
Methyl methacrylate ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
Propionitrile ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 135 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342730005
2014182SAMPLE DUPLICATE:
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%87 692
4-Bromofluorobenzene (S)%100 2102
Toluene-d8 (S)%108 1109
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 136 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
364296
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92342529001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2020050
Associated Lab Samples:92342529001
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/11/17 14:150.33
1,1,1-Trichloroethane ug/L ND 1.0 06/11/17 14:150.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 06/11/17 14:150.40
1,1,2-Trichloroethane ug/L ND 1.0 06/11/17 14:150.29
1,1-Dichloroethane ug/L ND 5.0 06/11/17 14:150.32
1,1-Dichloroethene ug/L ND 5.0 06/11/17 14:150.56
1,1-Dichloropropene ug/L ND 5.0 06/11/17 14:150.49
1,2,3-Trichloropropane ug/L ND 1.0 06/11/17 14:150.41
1,2,4-Trichlorobenzene ug/L ND 10.0 06/11/17 14:150.35
1,2-Dibromo-3-chloropropane ug/L ND 13.0 06/11/17 14:152.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/11/17 14:150.27
1,2-Dichlorobenzene ug/L ND 5.0 06/11/17 14:150.30
1,2-Dichloroethane ug/L ND 1.0 06/11/17 14:150.24
1,2-Dichloropropane ug/L ND 1.0 06/11/17 14:150.27
1,3-Dichlorobenzene ug/L ND 5.0 06/11/17 14:150.24
1,3-Dichloropropane ug/L ND 1.0 06/11/17 14:150.28
1,4-Dichlorobenzene ug/L ND 1.0 06/11/17 14:150.33
2,2-Dichloropropane ug/L ND 15.0 06/11/17 14:150.13
2-Butanone (MEK)ug/L ND 100 06/11/17 14:150.96
2-Hexanone ug/L ND 50.0 06/11/17 14:150.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 06/11/17 14:150.33
Acetone ug/L ND 100 06/11/17 14:1510.0
Acetonitrile ug/L ND 55.0 06/11/17 14:152.2
Acrolein ug/L ND 53.0 06/11/17 14:151.6
Acrylonitrile ug/L ND 200 06/11/17 14:151.9
Allyl chloride ug/L ND 10.0 06/11/17 14:151.5
Benzene ug/L ND 1.0 06/11/17 14:150.25
Bromochloromethane ug/L ND 3.0 06/11/17 14:150.17
Bromodichloromethane ug/L ND 1.0 06/11/17 14:150.18
Bromoform ug/L ND 3.0 06/11/17 14:150.26
Bromomethane ug/L ND 10.0 06/11/17 14:150.29
Carbon disulfide ug/L ND 100 06/11/17 14:151.2
Carbon tetrachloride ug/L ND 1.0 06/11/17 14:150.25
Chlorobenzene ug/L ND 3.0 06/11/17 14:150.23
Chloroethane ug/L ND 10.0 06/11/17 14:150.54
Chloroform ug/L ND 5.0 06/11/17 14:150.14
Chloromethane ug/L ND 1.0 06/11/17 14:150.11
Chloroprene ug/L ND 20.0 06/11/17 14:150.27
cis-1,2-Dichloroethene ug/L ND 5.0 06/11/17 14:150.19
cis-1,3-Dichloropropene ug/L ND 1.0 06/11/17 14:150.13
Dibromochloromethane ug/L ND 3.0 06/11/17 14:150.21
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
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[phone]
Page 137 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2020050
Associated Lab Samples:92342529001
Matrix:Water
AnalyzedMDL
Dibromomethane ug/L ND 10.0 06/11/17 14:150.21
Dichlorodifluoromethane ug/L ND 5.0 06/11/17 14:150.21
Ethyl methacrylate ug/L ND 10.0 06/11/17 14:150.20
Ethylbenzene ug/L ND 1.0 06/11/17 14:150.30
Hexachloro-1,3-butadiene ug/L ND 10.0 06/11/17 14:150.71
Iodomethane ug/L ND 10.0 06/11/17 14:150.32
Isobutanol ug/L ND 100 06/11/17 14:1535.0
Methacrylonitrile ug/L ND 100 06/11/17 14:150.93
Methyl methacrylate ug/L ND 30.0 06/11/17 14:152.0
Methylene Chloride ug/L ND 1.0 06/11/17 14:150.97
Naphthalene ug/L ND 10.0 06/11/17 14:150.24
Propionitrile ug/L ND 150 06/11/17 14:153.6
Styrene ug/L ND 1.0 06/11/17 14:150.26
Tetrachloroethene ug/L ND 1.0 06/11/17 14:150.46
Toluene ug/L ND 1.0 06/11/17 14:150.26
trans-1,2-Dichloroethene ug/L ND 5.0 06/11/17 14:150.49
trans-1,3-Dichloropropene ug/L ND 1.0 06/11/17 14:150.26
trans-1,4-Dichloro-2-butene ug/L ND 100 06/11/17 14:151.0
Trichloroethene ug/L ND 1.0 06/11/17 14:150.47
Trichlorofluoromethane ug/L ND 1.0 06/11/17 14:150.20
Vinyl acetate ug/L ND 50.0 06/11/17 14:150.35
Vinyl chloride ug/L ND 1.0 06/11/17 14:150.62
Xylene (Total)ug/L ND 5.0 06/11/17 14:150.66
1,2-Dichloroethane-d4 (S)%111 70-130 06/11/17 14:15
4-Bromofluorobenzene (S)%108 70-130 06/11/17 14:15
Toluene-d8 (S)%105 70-130 06/11/17 14:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2020051LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.750 99 80-125
1,1,1-Trichloroethane ug/L 50.250 100 71-129
1,1,2,2-Tetrachloroethane ug/L 47.050 94 79-124
1,1,2-Trichloroethane ug/L 50.050 100 85-125
1,1-Dichloroethane ug/L 49.950 100 73-126
1,1-Dichloroethene ug/L 53.450 107 66-135
1,1-Dichloropropene ug/L 55.050 110 74-135
1,2,3-Trichloropropane ug/L 46.750 93 75-130
1,2,4-Trichlorobenzene ug/L 48.450 97 75-134
1,2-Dibromo-3-chloropropane ug/L 43.050 86 71-133
1,2-Dibromoethane (EDB)ug/L 49.750 99 83-124
1,2-Dichlorobenzene ug/L 48.550 97 80-133
1,2-Dichloroethane ug/L 46.950 94 67-128
1,2-Dichloropropane ug/L 50.950 102 75-132
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
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Page 138 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2020051LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 48.550 97 77-130
1,3-Dichloropropane ug/L 52.150 104 76-131
1,4-Dichlorobenzene ug/L 49.150 98 78-130
2,2-Dichloropropane ug/L 51.450 103 40-160
2-Butanone (MEK)ug/L 91.5J100 91 61-144
2-Hexanone ug/L 86.6100 87 68-143
4-Methyl-2-pentanone (MIBK)ug/L 87.4J100 87 72-135
Acetone ug/L 100100 100 48-146
Acetonitrile ug/L 440500 88 62-150
Acrolein ug/L 233250 93 24-160
Acrylonitrile ug/L 227250 91 40-160
Allyl chloride ug/L 47.550 95 66-137
Benzene ug/L 52.950 106 80-125
Bromochloromethane ug/L 49.650 99 71-125
Bromodichloromethane ug/L 52.250 104 78-124
Bromoform ug/L 42.650 85 71-128
Bromomethane ug/L 43.850 88 40-160
Carbon disulfide ug/L 52.1J50 104 50-160
Carbon tetrachloride ug/L 49.350 99 69-131
Chlorobenzene ug/L 49.450 99 81-122
Chloroethane ug/L 44.450 89 39-148
Chloroform ug/L 47.850 96 73-127
Chloromethane ug/L 50.050 100 44-146
Chloroprene ug/L 49.750 99 75-145
cis-1,2-Dichloroethene ug/L 49.150 98 74-124
cis-1,3-Dichloropropene ug/L 54.250 108 72-132
Dibromochloromethane ug/L 53.350 107 78-125
Dibromomethane ug/L 46.450 93 82-120
Dichlorodifluoromethane ug/L 48.850 98 34-157
Ethyl methacrylate ug/L 46.750 93 82-121
Ethylbenzene ug/L 51.050 102 79-121
Hexachloro-1,3-butadiene ug/L 52.250 104 72-131
Iodomethane ug/L 85.5100 85 39-154
Isobutanol ug/L 8111000 81 34-160
Methacrylonitrile ug/L 480500 96 74-134
Methyl methacrylate ug/L 47.350 95 84-124
Methylene Chloride ug/L 50.350 101 64-133
Naphthalene ug/L 46.450 93 73-133
Propionitrile ug/L 435500 87 73-140
Styrene ug/L 48.250 96 84-126
Tetrachloroethene ug/L 50.450 101 78-122
Toluene ug/L 50.150 100 80-121
trans-1,2-Dichloroethene ug/L 49.950 100 71-127
trans-1,3-Dichloropropene ug/L 52.450 105 69-141
trans-1,4-Dichloro-2-butene ug/L 57.9J50 116 40-160
Trichloroethene ug/L 51.450 103 78-122
Trichlorofluoromethane ug/L 51.150 102 53-137
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
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[phone]
Page 139 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2020051LABORATORY CONTROL SAMPLE:
LCSSpike
Vinyl acetate ug/L 98.2100 98 40-160
Vinyl chloride ug/L 47.150 94 58-137
Xylene (Total)ug/L 148150 99 81-126
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2020053MATRIX SPIKE SAMPLE:
MSSpike
Result
92343305010
1,1,1,2-Tetrachloroethane ug/L 41.340 103 70-130ND
1,1,1-Trichloroethane ug/L 44.340 111 70-130ND
1,1,2,2-Tetrachloroethane ug/L 40.540 101 70-130ND
1,1,2-Trichloroethane ug/L 41.940 105 70-130ND
1,1-Dichloroethane ug/L 43.340 108 70-130ND
1,1-Dichloroethene ug/L 47.140 118 70-166ND
1,1-Dichloropropene ug/L 47.640 119 70-130ND
1,2,3-Trichloropropane ug/L 39.840 99 70-130ND
1,2,4-Trichlorobenzene ug/L 37.340 93 70-130ND
1,2-Dibromo-3-chloropropane ug/L 34.540 86 70-130
1,2-Dibromoethane (EDB)ug/L 40.840 102 70-130
1,2-Dichlorobenzene ug/L 40.340 101 70-130ND
1,2-Dichloroethane ug/L 43.240 108 70-130ND
1,2-Dichloropropane ug/L 43.440 108 70-130ND
1,3-Dichlorobenzene ug/L 39.840 99 70-130ND
1,3-Dichloropropane ug/L 43.640 109 70-130ND
1,4-Dichlorobenzene ug/L 40.340 101 70-130ND
2,2-Dichloropropane ug/L 32.340 81 70-130ND
2-Butanone (MEK)ug/L 82.0J80 103 70-130ND
2-Hexanone ug/L 69.880 87 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 75.8J80 95 70-130ND
Acetone ug/L 109 M18013670-130ND
Acetonitrile ug/L 415400 104 70-130ND
Acrolein ug/L 177200 88 70-130
Acrylonitrile ug/L 197J200 98 70-130ND
Allyl chloride ug/L 38.640 96 70-130ND
Benzene ug/L 44.240 111 70-148ND
Bromochloromethane ug/L 42.140 105 70-130ND
Bromodichloromethane ug/L 42.840 107 70-130ND
Bromoform ug/L 31.640 79 70-130ND
Bromomethane ug/L 32.740 82 70-130ND
Carbon disulfide ug/L 43.1J40 108 70-130ND
Carbon tetrachloride ug/L 41.140 103 70-130ND
Chlorobenzene ug/L 41.640 104 70-146ND
Chloroethane ug/L 36.340 91 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 140 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2020053MATRIX SPIKE SAMPLE:
MSSpike
Result
92343305010
Chloroform ug/L 44.740 112 70-130ND
Chloromethane ug/L 35.540 88 70-130ND
Chloroprene ug/L 44.440 111 70-130ND
cis-1,2-Dichloroethene ug/L 42.940 107 70-130ND
cis-1,3-Dichloropropene ug/L 42.540 106 70-130ND
Dibromochloromethane ug/L 42.440 106 70-130ND
Dibromomethane ug/L 39.240 98 70-130ND
Dichlorodifluoromethane ug/L 25.6 M1406470-130ND
Ethyl methacrylate ug/L 39.840 99 70-130ND
Ethylbenzene ug/L 43.340 108 70-130ND
Hexachloro-1,3-butadiene ug/L 38.040 95 70-130ND
Iodomethane ug/L 59.780 75 70-130ND
Isobutanol ug/L 595800 74 70-130ND
Methacrylonitrile ug/L 415400 104 70-130ND
Methyl methacrylate ug/L 39.040 98 70-130ND
Methylene Chloride ug/L 43.040 108 70-130ND
Naphthalene ug/L 36.940 92 70-130ND
Propionitrile ug/L 384400 96 70-130ND
Styrene ug/L 40.940 102 70-130ND
Tetrachloroethene ug/L 42.040 105 70-130ND
Toluene ug/L 43.140 108 70-155ND
trans-1,2-Dichloroethene ug/L 43.540 109 70-130ND
trans-1,3-Dichloropropene ug/L 40.640 102 70-130ND
trans-1,4-Dichloro-2-butene ug/L 33.1J40 83 70-130ND
Trichloroethene ug/L 43.040 107 69-151ND
Trichlorofluoromethane ug/L 42.240 105 70-130ND
Vinyl acetate ug/L 59.980 75 70-130ND
Vinyl chloride ug/L 34.440 86 70-130ND
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92343305009
2020052SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 1.6J 9 301.8
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 141 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92343305009
2020052SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L ND 30
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L 14.6J 3031.9
Acetonitrile ug/L ND 30ND
Acrolein ug/L ND 30
Acrylonitrile ug/L ND 30ND
Allyl chloride ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L 0.32J 30ND
Chloroprene ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 0.33J 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Ethyl methacrylate ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Isobutanol ug/L ND 30ND
Methacrylonitrile ug/L ND 30ND
Methyl methacrylate ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
Propionitrile ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 142 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92343305009
2020052SAMPLE DUPLICATE:
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%108 5114
4-Bromofluorobenzene (S)%105 2107
Toluene-d8 (S)%107 2109
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 143 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363163
EPA 3510
EPA 8081
8081A GCS Pesticides
Associated Lab Samples:92342479001, 92342479002, 92342479003, 92342479004, 92342479005, 92342479006, 92342479007,
92342479009, 92342479010, 92342479011, 92342479012, 92342479013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2013349
Associated Lab Samples:92342479001, 92342479002, 92342479003, 92342479004, 92342479005, 92342479006, 92342479007,
92342479009, 92342479010, 92342479011, 92342479012, 92342479013
Matrix:Water
AnalyzedMDL
4,4'-DDD ug/L ND 0.10 06/06/17 20:060.050
4,4'-DDE ug/L ND 0.10 06/06/17 20:060.050
4,4'-DDT ug/L ND 0.10 06/06/17 20:060.050
Aldrin ug/L ND 0.050 06/06/17 20:060.050
alpha-BHC ug/L ND 0.050 06/06/17 20:060.050
beta-BHC ug/L ND 0.050 06/06/17 20:060.050
Chlordane (Technical)ug/L ND 0.50 06/06/17 20:060.20
delta-BHC ug/L ND 0.050 06/06/17 20:060.050
Dieldrin ug/L ND 0.075 06/06/17 20:060.050
Endosulfan I ug/L ND 0.10 06/06/17 20:060.050
Endosulfan II ug/L ND 0.10 06/06/17 20:060.050
Endosulfan sulfate ug/L ND 0.10 06/06/17 20:060.050
Endrin ug/L ND 0.10 06/06/17 20:060.050
Endrin aldehyde ug/L ND 0.10 06/06/17 20:060.050
gamma-BHC (Lindane)ug/L ND 0.050 06/06/17 20:060.050
Heptachlor ug/L ND 0.050 06/06/17 20:060.050
Heptachlor epoxide ug/L ND 0.075 06/06/17 20:060.050
Methoxychlor ug/L ND 1.0 06/06/17 20:060.15
Toxaphene ug/L ND 1.5 06/06/17 20:060.20
Decachlorobiphenyl (S)%95 20-130 06/06/17 20:06
Tetrachloro-m-xylene (S)%80 20-130 06/06/17 20:06
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2013350LABORATORY CONTROL SAMPLE:
LCSSpike
4,4'-DDD ug/L 0.24.25 98 20-150
4,4'-DDE ug/L 0.22.25 89 20-150
4,4'-DDT ug/L 0.26.25 105 20-150
Aldrin ug/L 0.18.25 73 20-150
alpha-BHC ug/L 0.20.25 79 20-150
beta-BHC ug/L 0.19.25 78 20-150
delta-BHC ug/L 0.23.25 92 20-150
Dieldrin ug/L 0.23.25 91 20-150
Endosulfan I ug/L 0.23.25 92 20-150
Endosulfan II ug/L 0.24.25 99 20-150
Endosulfan sulfate ug/L 0.26.25 105 20-150
Endrin ug/L 0.25.25 100 20-150
Endrin aldehyde ug/L 0.23.25 94 20-150
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 144 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2013350LABORATORY CONTROL SAMPLE:
LCSSpike
gamma-BHC (Lindane)ug/L 0.22.25 88 20-150
Heptachlor ug/L 0.18.25 75 20-150
Heptachlor epoxide ug/L 0.21.25 83 20-150
Methoxychlor ug/L 0.76J.74 102 20-150
Decachlorobiphenyl (S)%86 20-130
Tetrachloro-m-xylene (S)%54 20-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2013351MATRIX SPIKE SAMPLE:
MSSpike
Result
92342479004
4,4'-DDD ug/L 0.22.25 89 20-150ND
4,4'-DDE ug/L 0.21.25 84 20-150ND
4,4'-DDT ug/L 0.24.25 98 20-150ND
Aldrin ug/L 0.18.25 71 20-150ND
alpha-BHC ug/L 0.19.25 77 20-150ND
beta-BHC ug/L 0.17.25 69 20-150ND
delta-BHC ug/L 0.21.25 84 20-150ND
Dieldrin ug/L 0.21.25 84 20-150ND
Endosulfan I ug/L 0.21.25 87 20-150ND
Endosulfan II ug/L 0.23.25 91 20-150ND
Endosulfan sulfate ug/L 0.25.25 99 20-150ND
Endrin ug/L 0.23.25 93 20-150ND
Endrin aldehyde ug/L 0.23.25 95 20-150ND
gamma-BHC (Lindane)ug/L 0.20.25 81 20-150ND
Heptachlor ug/L 0.18.25 74 20-150ND
Heptachlor epoxide ug/L 0.20.25 83 20-150ND
Methoxychlor ug/L 0.70J.74 94 20-150ND
Decachlorobiphenyl (S)%47 20-130
Tetrachloro-m-xylene (S)%76 20-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342479005
2013352SAMPLE DUPLICATE:
4,4'-DDD ug/L ND 30ND
4,4'-DDE ug/L ND 30ND
4,4'-DDT ug/L ND 30ND
Aldrin ug/L ND 30ND
alpha-BHC ug/L ND 30ND
beta-BHC ug/L ND 30ND
Chlordane (Technical)ug/L ND 30ND
delta-BHC ug/L ND 30ND
Dieldrin ug/L ND 30ND
Endosulfan I ug/L ND 30ND
Endosulfan II ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 145 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342479005
2013352SAMPLE DUPLICATE:
Endosulfan sulfate ug/L ND 30ND
Endrin ug/L ND 30ND
Endrin aldehyde ug/L ND 30ND
gamma-BHC (Lindane)ug/L ND 30ND
Heptachlor ug/L ND 30ND
Heptachlor epoxide ug/L ND 30ND
Methoxychlor ug/L ND 30ND
Toxaphene ug/L ND 30ND
Decachlorobiphenyl (S)%68 2184
Tetrachloro-m-xylene (S)%87 15101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 146 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363212
EPA 3510
EPA 8081
8081A GCS Pesticides
Associated Lab Samples:92342337001, 92342529001, 92342529002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2013628
Associated Lab Samples:92342337001, 92342529001, 92342529002
Matrix:Water
AnalyzedMDL
4,4'-DDD ug/L ND 0.10 06/08/17 02:460.050
4,4'-DDE ug/L ND 0.10 06/08/17 02:460.050
4,4'-DDT ug/L ND 0.10 06/08/17 02:460.050
Aldrin ug/L ND 0.050 06/08/17 02:460.050
alpha-BHC ug/L ND 0.050 06/08/17 02:460.050
beta-BHC ug/L ND 0.050 06/08/17 02:460.050
Chlordane (Technical)ug/L ND 0.50 06/08/17 02:460.20
delta-BHC ug/L ND 0.050 06/08/17 02:460.050
Dieldrin ug/L ND 0.075 06/08/17 02:460.050
Endosulfan I ug/L ND 0.10 06/08/17 02:460.050
Endosulfan II ug/L ND 0.10 06/08/17 02:460.050
Endosulfan sulfate ug/L ND 0.10 06/08/17 02:460.050
Endrin ug/L ND 0.10 06/08/17 02:460.050
Endrin aldehyde ug/L ND 0.10 06/08/17 02:460.050
gamma-BHC (Lindane)ug/L ND 0.050 06/08/17 02:460.050
Heptachlor ug/L ND 0.050 06/08/17 02:460.050
Heptachlor epoxide ug/L ND 0.075 06/08/17 02:460.050
Methoxychlor ug/L ND 1.0 06/08/17 02:460.15
Toxaphene ug/L ND 1.5 06/08/17 02:460.20
Decachlorobiphenyl (S)%60 20-130 06/08/17 02:46
Tetrachloro-m-xylene (S)%79 20-130 06/08/17 02:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2013629LABORATORY CONTROL SAMPLE:
LCSSpike
4,4'-DDD ug/L 0.11.12 87 20-150
4,4'-DDE ug/L 0.10J.12 81 20-150
4,4'-DDT ug/L 0.11.12 90 20-150
Aldrin ug/L 0.081.12 66 20-150
alpha-BHC ug/L 0.10.12 83 20-150
beta-BHC ug/L 0.089.12 72 20-150
delta-BHC ug/L 0.11.12 88 20-150
Dieldrin ug/L 0.10.12 83 20-150
Endosulfan I ug/L 0.11.12 88 20-150
Endosulfan II ug/L 0.11.12 90 20-150
Endosulfan sulfate ug/L 0.11.12 93 20-150
Endrin ug/L 0.11.12 90 20-150
Endrin aldehyde ug/L 0.098J.12 80 20-150
gamma-BHC (Lindane)ug/L 0.10.12 83 20-150
Heptachlor ug/L 0.099.12 80 20-150
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 147 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2013629LABORATORY CONTROL SAMPLE:
LCSSpike
Heptachlor epoxide ug/L 0.11.12 87 20-150
Methoxychlor ug/L 0.39J.37 105 20-150
Decachlorobiphenyl (S)%54 20-130
Tetrachloro-m-xylene (S)%88 20-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2013630MATRIX SPIKE SAMPLE:
MSSpike
Result
92342317009
4,4'-DDD ug/L 0.13.12 105 20-150ND
4,4'-DDE ug/L 0.20 M1.12 164 20-150ND
4,4'-DDT ug/L 0.12.12 95 20-150ND
Aldrin ug/L 0.069.12 55 20-150ND
alpha-BHC ug/L 0.097.12 78 20-150ND
beta-BHC ug/L 0.085.12 69 20-150ND
delta-BHC ug/L 0.081.12 65 20-150ND
Dieldrin ug/L 0.091.12 74 20-150ND
Endosulfan I ug/L 0.12.12 97 20-150ND
Endosulfan II ug/L 0.091J.12 73 20-150ND
Endosulfan sulfate ug/L 0.096J.12 78 20-150ND
Endrin ug/L 0.14.12 115 20-150ND
Endrin aldehyde ug/L 0.44 M1.12 359 20-150ND
gamma-BHC (Lindane)ug/L 0.084.12 68 20-150ND
Heptachlor ug/L 0.083.12 67 20-150ND
Heptachlor epoxide ug/L 0.12.12 98 20-150ND
Methoxychlor ug/L 0.31J.37 85 20-150ND
Decachlorobiphenyl (S)%66 20-130
Tetrachloro-m-xylene (S)%74 20-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342317019
2013631SAMPLE DUPLICATE:
4,4'-DDD ug/L ND 30ND
4,4'-DDE ug/L ND 30ND
4,4'-DDT ug/L ND 30ND
Aldrin ug/L ND 30ND
alpha-BHC ug/L ND 30ND
beta-BHC ug/L ND 30ND
Chlordane (Technical)ug/L ND 30ND
delta-BHC ug/L ND 30ND
Dieldrin ug/L ND 30ND
Endosulfan I ug/L ND 30ND
Endosulfan II ug/L ND 30ND
Endosulfan sulfate ug/L ND 30ND
Endrin ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 148 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342317019
2013631SAMPLE DUPLICATE:
Endrin aldehyde ug/L ND 30ND
gamma-BHC (Lindane)ug/L ND 30ND
Heptachlor ug/L ND 30ND
Heptachlor epoxide ug/L ND 30ND
Methoxychlor ug/L ND 30ND
Toxaphene ug/L ND 30ND
Decachlorobiphenyl (S)%38 337
Tetrachloro-m-xylene (S)%75 30101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 149 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
362866
EPA 3510
EPA 8082
8082 GCS PCB
Associated Lab Samples:92342337001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2011591
Associated Lab Samples:92342337001
Matrix:Water
AnalyzedMDL
PCB-1016 (Aroclor 1016)ug/L ND 0.50 06/02/17 03:100.50
PCB-1221 (Aroclor 1221)ug/L ND 0.50 06/02/17 03:100.50
PCB-1232 (Aroclor 1232)ug/L ND 0.50 06/02/17 03:100.50
PCB-1242 (Aroclor 1242)ug/L ND 0.50 06/02/17 03:100.50
PCB-1248 (Aroclor 1248)ug/L ND 0.50 06/02/17 03:100.50
PCB-1254 (Aroclor 1254)ug/L ND 0.50 06/02/17 03:100.50
PCB-1260 (Aroclor 1260)ug/L ND 0.50 06/02/17 03:100.50
Decachlorobiphenyl (S)%34 10-132 06/02/17 03:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2011592LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2011593
PCB-1016 (Aroclor 1016)ug/L 2.65 53 50-150552.7 3 30
PCB-1260 (Aroclor 1260)ug/L 2.55 50 50-150562.8 10 30
Decachlorobiphenyl (S)%35 10-13235
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 150 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363162
EPA 3510
EPA 8082
8082 GCS PCB
Associated Lab Samples:92342479001, 92342479002, 92342479003, 92342479004, 92342479005, 92342479006, 92342479007,
92342479009, 92342479010, 92342479011, 92342479012, 92342479013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2013345
Associated Lab Samples:92342479001, 92342479002, 92342479003, 92342479004, 92342479005, 92342479006, 92342479007,
92342479009, 92342479010, 92342479011, 92342479012, 92342479013
Matrix:Water
AnalyzedMDL
PCB-1016 (Aroclor 1016)ug/L ND 0.50 06/03/17 13:250.50
PCB-1221 (Aroclor 1221)ug/L ND 0.50 06/03/17 13:250.50
PCB-1232 (Aroclor 1232)ug/L ND 0.50 06/03/17 13:250.50
PCB-1242 (Aroclor 1242)ug/L ND 0.50 06/03/17 13:250.50
PCB-1248 (Aroclor 1248)ug/L ND 0.50 06/03/17 13:250.50
PCB-1254 (Aroclor 1254)ug/L ND 0.50 06/03/17 13:250.50
PCB-1260 (Aroclor 1260)ug/L ND 0.50 06/03/17 13:250.50
Decachlorobiphenyl (S)%93 10-132 06/03/17 13:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2013346LABORATORY CONTROL SAMPLE:
LCSSpike
PCB-1016 (Aroclor 1016)ug/L 1.92.5 76 50-150
PCB-1260 (Aroclor 1260)ug/L 2.32.5 91 50-150
Decachlorobiphenyl (S)%64 10-132
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2013347MATRIX SPIKE SAMPLE:
MSSpike
Result
92342530001
PCB-1016 (Aroclor 1016)ug/L 1.52.5 61 50-150ND
PCB-1260 (Aroclor 1260)ug/L 1.42.5 55 50-150ND
Decachlorobiphenyl (S)%32 10-132
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342530003
2013348SAMPLE DUPLICATE:
PCB-1016 (Aroclor 1016)ug/L ND 30ND
PCB-1221 (Aroclor 1221)ug/L ND 30ND
PCB-1232 (Aroclor 1232)ug/L ND 30ND
PCB-1242 (Aroclor 1242)ug/L ND 30ND
PCB-1248 (Aroclor 1248)ug/L ND 30ND
PCB-1254 (Aroclor 1254)ug/L ND 30ND
PCB-1260 (Aroclor 1260)ug/L ND 30ND
Decachlorobiphenyl (S)%59 2777
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 151 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
372315
EPA 8151
EPA 8151
8151A GCS Herbicides
Associated Lab Samples:92342337001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2012657
Associated Lab Samples:92342337001
Matrix:Water
AnalyzedMDL
2,4,5-T ug/L ND 0.19 06/06/17 01:190.042
2,4,5-TP (Silvex)ug/L ND 0.19 06/06/17 01:190.049
2,4-D ug/L ND 0.94 06/06/17 01:190.22
Dinoseb ug/L ND 0.19 06/06/17 01:190.057
Pentachlorophenol ug/L ND 0.028 06/06/17 01:190.017
2,4-DCAA (S)%94 39-139 06/06/17 01:19
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012658LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2013105
2,4,5-T ug/L 1.21.2 100 37-133971.2 3 40
2,4,5-TP (Silvex)ug/L 1.11.2 92 53-134971.2 5 40
2,4-D ug/L 5.56 91 35-124955.7 5 40
Dinoseb ug/L 0.891.2 74 13-116831.0 12 40
Pentachlorophenol ug/L 0.22.18 122 39-1701240.22 2 40
2,4-DCAA (S)%83 39-13985 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 152 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
372862
EPA 8151
EPA 8151
8151A GCS Herbicides
Associated Lab Samples:92342479001, 92342479002, 92342479003, 92342479004, 92342479005, 92342479006, 92342479007,
92342479009, 92342479010, 92342479011, 92342479012, 92342479013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2015492
Associated Lab Samples:92342479001, 92342479002, 92342479003, 92342479004, 92342479005, 92342479006, 92342479007,
92342479009, 92342479010, 92342479011, 92342479012, 92342479013
Matrix:Water
AnalyzedMDL
2,4,5-T ug/L ND 0.19 06/07/17 01:340.042
2,4,5-TP (Silvex)ug/L ND 0.19 06/07/17 01:340.049
2,4-D ug/L ND 0.94 06/07/17 01:340.22
Dinoseb ug/L ND 0.19 06/07/17 01:340.057
Pentachlorophenol ug/L ND 0.028 06/07/17 01:340.017
2,4-DCAA (S)%93 39-139 06/07/17 01:34
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2015493LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-T ug/L 1.51.2 129 37-133
2,4,5-TP (Silvex)ug/L 1.51.2 128 53-134
2,4-D ug/L 7.6 L1612635-124
Dinoseb ug/L 1.5 L11.2 124 13-116
Pentachlorophenol ug/L 0.24.18 132 39-170
2,4-DCAA (S)%114 39-139
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015674MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35315473004
2015675
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,4,5-T ug/L 1.5 130 37-133108 36 401.20.043U 1.9 1.3
2,4,5-TP (Silvex)ug/L 1.5 125 53-134119 23 401.20.051U 1.8 1.4
2,4-D ug/L 7.3 120 35-124107 30 4060.23U 8.7 6.5
Dinoseb ug/L 1.5 116 13-11699 34 401.20.059U 1.7 1.2
Pentachlorophenol ug/L .22 124 39-170104 36 40.180.018U 0.27 0.19
2,4-DCAA (S)%114 39-13998 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 153 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
373221
EPA 8151
EPA 8151
8151A GCS Herbicides
Associated Lab Samples:92342529001, 92342529002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2017562
Associated Lab Samples:92342529001, 92342529002
Matrix:Water
AnalyzedMDL
2,4,5-T ug/L ND 0.19 06/09/17 20:420.042
2,4,5-TP (Silvex)ug/L ND 0.19 06/09/17 20:420.049
2,4-D ug/L ND 0.94 06/09/17 20:420.22
Dinoseb ug/L ND 0.19 06/09/17 20:420.057
Pentachlorophenol ug/L ND 0.028 06/09/17 20:420.017
2,4-DCAA (S)%74 39-139 06/09/17 20:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2017563LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-T ug/L 1.31.2 109 37-133
2,4,5-TP (Silvex)ug/L 1.31.2 110 53-134
2,4-D ug/L 5.56 91 35-124
Dinoseb ug/L 1.21.2 99 13-116
Pentachlorophenol ug/L 0.17.18 94 39-170
2,4-DCAA (S)%85 39-139
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2018719MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35316294004
2018720
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,4,5-T ug/L 1.2 100 37-13390 3 401.40.043U 1.2 1.2
2,4,5-TP (Silvex)ug/L 1.2 97 53-13488 2 401.40.050U 1.2 1.2
2,4-D ug/L 6 84 35-12476 3 406.80.23U 5.1 5.2
Dinoseb ug/L 1.2 91 13-11672 11 401.40.058U 1.1 0.98
Pentachlorophenol ug/L M1,R1.18 82 39-17028 89 40.20.017U 0.15 0.057
2,4-DCAA (S)%69 39-13985 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 154 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363548
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92342337001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2015434
Associated Lab Samples:92342337001
Matrix:Water
AnalyzedMDL
1,2,4,5-Tetrachlorobenzene ug/L ND 10.0 06/07/17 15:251.3
1,3,5-Trinitrobenzene ug/L ND 10.0 06/07/17 15:251.2
1,3-Dinitrobenzene ug/L ND 20.0 06/07/17 15:251.3
1,4-Naphthoquinone ug/L ND 10.0 06/07/17 15:250.99
1-Naphthalenamine ug/L ND 10.0 06/07/17 15:251.3
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 06/07/17 15:251.8
2,3,4,6-Tetrachlorophenol ug/L ND 10.0 06/07/17 15:252.9
2,4,5-Trichlorophenol ug/L ND 10.0 06/07/17 15:251.5
2,4,6-Trichlorophenol ug/L ND 10.0 06/07/17 15:251.4
2,4-Dichlorophenol ug/L ND 10.0 06/07/17 15:251.6
2,4-Dimethylphenol ug/L ND 10.0 06/07/17 15:251.6
2,4-Dinitrophenol ug/L ND 50.0 06/07/17 15:255.1
2,4-Dinitrotoluene ug/L ND 10.0 06/07/17 15:251.5
2,6-Dichlorophenol ug/L ND 10.0 06/07/17 15:251.5
2,6-Dinitrotoluene ug/L ND 10.0 06/07/17 15:251.4
2-Acetylaminofluorene ug/L ND 20.0 06/07/17 15:251.6
2-Chloronaphthalene ug/L ND 10.0 06/07/17 15:251.6
2-Chlorophenol ug/L ND 10.0 06/07/17 15:251.5
2-Methylnaphthalene ug/L ND 10.0 06/07/17 15:251.4
2-Methylphenol(o-Cresol)ug/L ND 10.0 06/07/17 15:251.6
2-Naphthalenamine ug/L ND 10.0 06/07/17 15:252.2
2-Nitroaniline ug/L ND 50.0 06/07/17 15:252.3
2-Nitrophenol ug/L ND 10.0 06/07/17 15:251.6
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 06/07/17 15:251.4
3,3'-Dichlorobenzidine ug/L ND 20.0 06/07/17 15:253.9
3,3'-Dimethylbenzidine ug/L ND 10.0 06/07/17 15:253.9
3-Methylcholanthrene ug/L ND 10.0 06/07/17 15:252.7
3-Nitroaniline ug/L ND 50.0 06/07/17 15:252.7
4,6-Dinitro-2-methylphenol ug/L ND 50.0 06/07/17 15:252.2
4-Aminobiphenyl ug/L ND 20.0 06/07/17 15:251.7
4-Bromophenylphenyl ether ug/L ND 10.0 06/07/17 15:251.5
4-Chloro-3-methylphenol ug/L ND 20.0 06/07/17 15:252.8
4-Chloroaniline ug/L ND 20.0 06/07/17 15:252.8
4-Chlorophenylphenyl ether ug/L ND 10.0 06/07/17 15:251.6
4-Nitroaniline ug/L ND 20.0 06/07/17 15:253.4
4-Nitrophenol ug/L ND 50.0 06/07/17 15:254.3
5-Nitro-o-toluidine ug/L ND 10.0 06/07/17 15:251.9
7,12-Dimethylbenz(a)anthracene ug/L ND 10.0 06/07/17 15:252.4
Acenaphthene ug/L ND 10.0 06/07/17 15:251.6
Acenaphthylene ug/L ND 10.0 06/07/17 15:251.5
Acetophenone ug/L ND 10.0 06/07/17 15:251.9
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
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Huntersville, NC 28078
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Page 155 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2015434
Associated Lab Samples:92342337001
Matrix:Water
AnalyzedMDL
Anthracene ug/L ND 10.0 06/07/17 15:251.7
Benzo(a)anthracene ug/L ND 10.0 06/07/17 15:252.1
Benzo(a)pyrene ug/L ND 10.0 06/07/17 15:252.2
Benzo(b)fluoranthene ug/L ND 10.0 06/07/17 15:252.2
Benzo(g,h,i)perylene ug/L ND 10.0 06/07/17 15:252.1
Benzo(k)fluoranthene ug/L ND 10.0 06/07/17 15:252.0
Benzyl alcohol ug/L ND 20.0 06/07/17 15:253.1
bis(2-Chloroethoxy)methane ug/L ND 10.0 06/07/17 15:251.6
bis(2-Chloroethyl) ether ug/L ND 10.0 06/07/17 15:251.7
bis(2-Ethylhexyl)phthalate ug/L ND 15.0 06/07/17 15:252.3
Butylbenzylphthalate ug/L ND 10.0 06/07/17 15:252.5
Chlorobenzilate ug/L ND 10.0 06/07/17 15:252.2
Chrysene ug/L ND 10.0 06/07/17 15:252.1
Di-n-butylphthalate ug/L ND 10.0 06/07/17 15:252.0
Di-n-octylphthalate ug/L ND 10.0 06/07/17 15:251.5
Diallate ug/L ND 10.0 06/07/17 15:251.6
Dibenz(a,h)anthracene ug/L ND 10.0 06/07/17 15:252.0
Dibenzofuran ug/L ND 10.0 06/07/17 15:251.7
Diethylphthalate ug/L ND 6000 06/07/17 15:251.6
Dimethoate ug/L ND 20.0 06/07/17 15:251.8
Dimethylphthalate ug/L ND 10.0 06/07/17 15:251.4
Diphenylamine ug/L ND 10.0 06/07/17 15:251.4
Disulfoton ug/L ND 10.0 06/07/17 15:251.5
Ethyl methanesulfonate ug/L ND 20.0 06/07/17 15:251.6
Famphur ug/L ND 20.0 06/07/17 15:255.7
Fluoranthene ug/L ND 10.0 06/07/17 15:252.2
Fluorene ug/L ND 10.0 06/07/17 15:251.6
Hexachlorobenzene ug/L ND 10.0 06/07/17 15:251.7
Hexachlorocyclopentadiene ug/L ND 10.0 06/07/17 15:251.3
Hexachloroethane ug/L ND 10.0 06/07/17 15:251.8
Hexachloropropene ug/L ND 10.0 06/07/17 15:251.2
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 06/07/17 15:252.0
Isodrin ug/L ND 20.0 06/07/17 15:252.5
Isophorone ug/L ND 10.0 06/07/17 15:251.5
Isosafrole ug/L ND 10.0 06/07/17 15:251.5
Kepone ug/L ND 20.0 06/07/17 15:254.5
Methapyrilene ug/L ND 100 06/07/17 15:253.0
Methyl methanesulfonate ug/L ND 10.0 06/07/17 15:251.1
Methyl parathion ug/L ND 10.0 06/07/17 15:251.6
N-Nitroso-di-n-butylamine ug/L ND 10.0 06/07/17 15:251.6
N-Nitroso-di-n-propylamine ug/L ND 10.0 06/07/17 15:251.7
N-Nitrosodiethylamine ug/L ND 20.0 06/07/17 15:251.4
N-Nitrosodimethylamine ug/L ND 10.0 06/07/17 15:251.6
N-Nitrosodiphenylamine ug/L ND 10.0 06/07/17 15:251.4
N-Nitrosomethylethylamine ug/L ND 10.0 06/07/17 15:251.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
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Huntersville, NC 28078
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Page 156 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2015434
Associated Lab Samples:92342337001
Matrix:Water
AnalyzedMDL
N-Nitrosopiperidine ug/L ND 20.0 06/07/17 15:251.7
N-Nitrosopyrrolidine ug/L ND 10.0 06/07/17 15:251.7
Nitrobenzene ug/L ND 10.0 06/07/17 15:251.6
O,O,O-Triethylphosphorothioate ug/L ND 10.0 06/07/17 15:251.7
O-Toluidine ug/L ND 10.0 06/07/17 15:251.7
P-Dimethylaminoazobenzene ug/L ND 10.0 06/07/17 15:251.0
p-Phenylenediamine ug/L ND 10.0 06/07/17 15:252.2
Parathion (Ethyl parathion)ug/L ND 10.0 06/07/17 15:251.5
Pentachlorobenzene ug/L ND 10.0 06/07/17 15:251.5
Pentachloronitrobenzene ug/L ND 20.0 06/07/17 15:251.7
Pentachlorophenol ug/L ND 25.0 06/07/17 15:253.5
Phenacetin ug/L ND 20.0 06/07/17 15:251.9
Phenanthrene ug/L ND 10.0 06/07/17 15:251.6
Phenol ug/L ND 10.0 06/07/17 15:251.3
Phorate ug/L ND 10.0 06/07/17 15:251.7
Pronamide ug/L ND 10.0 06/07/17 15:252.0
Pyrene ug/L ND 10.0 06/07/17 15:252.2
Safrole ug/L ND 10.0 06/07/17 15:251.3
Thionazin ug/L ND 20.0 06/07/17 15:251.7
2,4,6-Tribromophenol (S)%87 27-110 06/07/17 15:25
2-Fluorobiphenyl (S)%62 27-110 06/07/17 15:25
2-Fluorophenol (S)%35 12-110 06/07/17 15:25
Nitrobenzene-d5 (S)%59 21-110 06/07/17 15:25
Phenol-d6 (S)%32 10-110 06/07/17 15:25
Terphenyl-d14 (S)%95 31-107 06/07/17 15:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2015435LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4,5-Tetrachlorobenzene ug/L 33.750 67 16-129
1,3,5-Trinitrobenzene ug/L 49.150 98 55-125
1,3-Dinitrobenzene ug/L 43.850 88 30-122
1,4-Naphthoquinone ug/L 41.150 82 31-120
1-Naphthalenamine ug/L 25.450 51 37-126
2,2'-Oxybis(1-chloropropane)ug/L 43.450 87 18-120
2,3,4,6-Tetrachlorophenol ug/L 50.450 101 54-276
2,4,5-Trichlorophenol ug/L 46.350 93 43-113
2,4,6-Trichlorophenol ug/L 54.350 109 42-120
2,4-Dichlorophenol ug/L 42.950 86 30-120
2,4-Dimethylphenol ug/L 43.050 86 29-111
2,4-Dinitrophenol ug/L 270250 108 19-132
2,4-Dinitrotoluene ug/L 50.450 101 58-128
2,6-Dichlorophenol ug/L 33.850 68 54-128
2,6-Dinitrotoluene ug/L 52.050 104 54-129
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 157 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2015435LABORATORY CONTROL SAMPLE:
LCSSpike
2-Acetylaminofluorene ug/L 45.950 92 81-160
2-Chloronaphthalene ug/L 53.150 106 43-117
2-Chlorophenol ug/L 43.350 87 37-120
2-Methylnaphthalene ug/L 39.650 79 33-120
2-Methylphenol(o-Cresol)ug/L 35.350 71 31-120
2-Naphthalenamine ug/L 33.450 67 41-136
2-Nitroaniline ug/L 103100 103 48-121
2-Nitrophenol ug/L 43.850 88 25-116
3&4-Methylphenol(m&p Cresol)ug/L 31.050 62 23-120
3,3'-Dichlorobenzidine ug/L 96.8250 39 10-154
3,3'-Dimethylbenzidine ug/L 17.7100 18 10-157
3-Methylcholanthrene ug/L 48.850 98 65-130
3-Nitroaniline ug/L 101100 101 43-115
4,6-Dinitro-2-methylphenol ug/L 98.6100 99 44-124
4-Aminobiphenyl ug/L 24.750 49 21-125
4-Bromophenylphenyl ether ug/L 44.250 88 34-113
4-Chloro-3-methylphenol ug/L 88.8100 89 31-110
4-Chloroaniline ug/L 81.0100 81 20-120
4-Chlorophenylphenyl ether ug/L 48.750 97 34-116
4-Nitroaniline ug/L 101100 101 46-128
4-Nitrophenol ug/L 111250 44 11-120
5-Nitro-o-toluidine ug/L 45.350 91 78-160
7,12-Dimethylbenz(a)anthracene ug/L 43.250 86 47-124
Acenaphthene ug/L 47.050 94 48-114
Acenaphthylene ug/L 45.450 91 48-112
Acetophenone ug/L 47.150 94 24-120
Anthracene ug/L 44.450 89 57-118
Benzo(a)anthracene ug/L 46.650 93 56-121
Benzo(a)pyrene ug/L 47.750 95 55-127
Benzo(b)fluoranthene ug/L 49.750 99 53-128
Benzo(g,h,i)perylene ug/L 47.250 94 54-125
Benzo(k)fluoranthene ug/L 47.250 94 51-123
Benzyl alcohol ug/L 78.9100 79 27-120
bis(2-Chloroethoxy)methane ug/L 42.450 85 32-120
bis(2-Chloroethyl) ether ug/L 45.250 90 33-111
bis(2-Ethylhexyl)phthalate ug/L 55.050 110 50-145
Butylbenzylphthalate ug/L 55.250 110 54-138
Chlorobenzilate ug/L 47.450 95 65-132
Chrysene ug/L 45.950 92 58-127
Di-n-butylphthalate ug/L 51.050 102 56-125
Di-n-octylphthalate ug/L 49.950 100 50-134
Diallate ug/L 45.750 91 47-123
Dibenz(a,h)anthracene ug/L 47.550 95 53-129
Dibenzofuran ug/L 48.550 97 45-120
Diethylphthalate ug/L 53.1J50 106 53-120
Dimethoate ug/L 53.450 107 57-139
Dimethylphthalate ug/L 51.450 103 55-116
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 158 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2015435LABORATORY CONTROL SAMPLE:
LCSSpike
Diphenylamine ug/L 44.850 90 42-120
Disulfoton ug/L 43.150 86 49-156
Ethyl methanesulfonate ug/L 42.350 85 43-120
Famphur ug/L 208100 208 40-160
Fluoranthene ug/L 45.550 91 57-125
Fluorene ug/L 48.750 97 53-118
Hexachlorobenzene ug/L 44.250 88 49-116
Hexachlorocyclopentadiene ug/L 36.050 72 26-158
Hexachloroethane ug/L 29.850 60 30-114
Hexachloropropene ug/L 22.150 44 13-137
Indeno(1,2,3-cd)pyrene ug/L 48.650 97 55-128
Isodrin ug/L 47.050 94 68-129
Isophorone ug/L 42.050 84 31-118
Isosafrole ug/L 38.850 78 48-107
Kepone ug/L 85.8100 86 10-124
Methapyrilene ug/L 14.5J L2502940-160
Methyl methanesulfonate ug/L 70.9 L15014225-114
Methyl parathion ug/L 58.050 116 58-137
N-Nitroso-di-n-butylamine ug/L 29.850 60 36-115
N-Nitroso-di-n-propylamine ug/L 46.150 92 32-119
N-Nitrosodiethylamine ug/L 41.550 83 47-115
N-Nitrosodimethylamine ug/L 27.750 55 13-120
N-Nitrosodiphenylamine ug/L 44.850 90 43-120
N-Nitrosomethylethylamine ug/L 36.550 73 39-120
N-Nitrosopiperidine ug/L 35.050 70 43-113
N-Nitrosopyrrolidine ug/L 40.350 81 32-110
Nitrobenzene ug/L 39.950 80 33-110
O,O,O-Triethylphosphorothioate ug/L 33.850 68 51-127
O-Toluidine ug/L 36.550 73 27-120
P-Dimethylaminoazobenzene ug/L 19.1100 19 10-120
p-Phenylenediamine ug/L 42.450 85 72-143
Parathion (Ethyl parathion)ug/L 51.950 104 56-140
Pentachlorobenzene ug/L 40.050 80 30-137
Pentachloronitrobenzene ug/L 52.450 105 70-124
Pentachlorophenol ug/L 105250 42 10-137
Phenacetin ug/L 49.850 100 60-130
Phenanthrene ug/L 44.350 89 57-117
Phenol ug/L 19.950 40 10-120
Phorate ug/L 47.150 94 55-126
Pronamide ug/L 47.350 95 75-124
Pyrene ug/L 45.050 90 55-122
Safrole ug/L 34.250 68 41-120
Thionazin ug/L 45.650 91 63-137
2,4,6-Tribromophenol (S)%99 27-110
2-Fluorobiphenyl (S)%95 27-110
2-Fluorophenol (S)%55 12-110
Nitrobenzene-d5 (S)%85 21-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 159 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2015435LABORATORY CONTROL SAMPLE:
LCSSpike
Phenol-d6 (S)%39 10-110
Terphenyl-d14 (S)%101 31-107
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2015436MATRIX SPIKE SAMPLE:
MSSpike
Result
10390835001
1,2,4,5-Tetrachlorobenzene ug/L 29.250 58 50-150ND
1,3,5-Trinitrobenzene ug/L 39.950 80 50-150ND
1,3-Dinitrobenzene ug/L 36.350 73 50-150ND
1,4-Naphthoquinone ug/L 35.250 70 50-150ND
1-Naphthalenamine ug/L 8.2J M1501650-150ND
2,2'-Oxybis(1-chloropropane)ug/L 38.550 77 50-150ND
2,3,4,6-Tetrachlorophenol ug/L 44.250 88 50-150ND
2,4,5-Trichlorophenol ug/L 39.850 80 19-105ND
2,4,6-Trichlorophenol ug/L 45.450 91 13-108ND
2,4-Dichlorophenol ug/L 38.050 76 29-111ND
2,4-Dimethylphenol ug/L 38.450 77 21-103ND
2,4-Dinitrophenol ug/L 229250 91 10-109ND
2,4-Dinitrotoluene ug/L 43.250 86 27-104ND
2,6-Dichlorophenol ug/L 30.250 60 50-150ND
2,6-Dinitrotoluene ug/L 45.050 90 28-101ND
2-Acetylaminofluorene ug/L 39.950 80 50-150ND
2-Chloronaphthalene ug/L 43.850 88 14-102ND
2-Chlorophenol ug/L 38.350 77 16-110ND
2-Methylnaphthalene ug/L 36.350 73 13-110ND
2-Methylphenol(o-Cresol)ug/L 32.350 65 19-110ND
2-Naphthalenamine ug/L 9.1J M1501850-150ND
2-Nitroaniline ug/L 88.0100 88 26-103ND
2-Nitrophenol ug/L 37.750 75 20-110ND
3&4-Methylphenol(m&p Cresol)ug/L 28.250 56 20-110ND
3,3'-Dichlorobenzidine ug/L 65.0250 26 25-112ND
3,3'-Dimethylbenzidine ug/L ND M1100050-150ND
3-Methylcholanthrene ug/L 42.750 85 50-150ND
3-Nitroaniline ug/L 75.8100 76 29-110ND
4,6-Dinitro-2-methylphenol ug/L 88.5100 89 10-117ND
4-Aminobiphenyl ug/L 18.1J M1503650-150ND
4-Bromophenylphenyl ether ug/L 40.750 81 20-105ND
4-Chloro-3-methylphenol ug/L 80.2100 80 22-110ND
4-Chloroaniline ug/L 46.1100 46 20-100ND
4-Chlorophenylphenyl ether ug/L 42.850 86 19-102ND
4-Nitroaniline ug/L 83.4100 83 29-110ND
4-Nitrophenol ug/L 97.3250 39 10-110ND
5-Nitro-o-toluidine ug/L 37.050 74 50-150ND
7,12-Dimethylbenz(a)anthracene ug/L 38.650 77 50-150ND
Acenaphthene ug/L 41.450 83 17-100ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 160 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2015436MATRIX SPIKE SAMPLE:
MSSpike
Result
10390835001
Acenaphthylene ug/L 40.150 80 21-100ND
Acetophenone ug/L 40.950 82 50-150ND
Anthracene ug/L 39.350 79 24-109ND
Benzo(a)anthracene ug/L 42.350 85 22-117ND
Benzo(a)pyrene ug/L 41.550 83 23-104ND
Benzo(b)fluoranthene ug/L 43.550 87 23-103ND
Benzo(g,h,i)perylene ug/L 39.850 80 18-111ND
Benzo(k)fluoranthene ug/L 41.750 83 22-113ND
Benzyl alcohol ug/L 64.8100 65 19-101ND
bis(2-Chloroethoxy)methane ug/L 35.850 72 22-110ND
bis(2-Chloroethyl) ether ug/L 39.850 80 16-110ND
bis(2-Ethylhexyl)phthalate ug/L 49.750 99 23-102ND
Butylbenzylphthalate ug/L 50.050 100 25-110ND
Chlorobenzilate ug/L 42.750 85 50-150ND
Chrysene ug/L 42.550 85 23-115ND
Di-n-butylphthalate ug/L 45.150 90 26-110ND
Di-n-octylphthalate ug/L 44.850 90 22-110ND
Diallate ug/L 40.050 80 50-150ND
Dibenz(a,h)anthracene ug/L 40.750 81 21-112ND
Dibenzofuran ug/L 42.250 84 19-102ND
Diethylphthalate ug/L 45.1J50 90 29-110ND
Dimethoate ug/L 46.650 93 50-150ND
Dimethylphthalate ug/L 44.850 90 27-110ND
Diphenylamine ug/L 40.150 80 50-150ND
Disulfoton ug/L 39.050 78 50-150ND
Ethyl methanesulfonate ug/L 35.550 71 50-150ND
Famphur ug/L 205100 205 50-150ND
Fluoranthene ug/L 40.450 81 23-112ND
Fluorene ug/L 41.950 84 22-104ND
Hexachlorobenzene ug/L 39.950 80 21-116ND
Hexachlorocyclopentadiene ug/L 33.950 68 10-110ND
Hexachloroethane ug/L 29.250 58 10-110ND
Hexachloropropene ug/L 22.7 M1504550-150ND
Indeno(1,2,3-cd)pyrene ug/L 40.950 82 20-113ND
Isodrin ug/L 39.550 79 50-150ND
Isophorone ug/L 36.150 72 50-150ND
Isosafrole ug/L 32.650 65 50-150ND
Kepone ug/L 79.9100 80 50-150ND
Methapyrilene ug/L 15.3J M0503150-150ND
Methyl methanesulfonate ug/L 60.150 120 50-150ND
Methyl parathion ug/L 50.250 100 50-150ND
N-Nitroso-di-n-butylamine ug/L 25.550 51 50-150ND
N-Nitroso-di-n-propylamine ug/L 41.850 84 21-105ND
N-Nitrosodiethylamine ug/L 34.650 69 50-150ND
N-Nitrosodimethylamine ug/L 22.650 45 10-110ND
N-Nitrosodiphenylamine ug/L 40.150 80 23-107ND
N-Nitrosomethylethylamine ug/L 30.350 61 50-150ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 161 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2015436MATRIX SPIKE SAMPLE:
MSSpike
Result
10390835001
N-Nitrosopiperidine ug/L 31.250 62 50-150ND
N-Nitrosopyrrolidine ug/L 32.050 64 50-150ND
Nitrobenzene ug/L 34.350 69 20-110ND
O,O,O-Triethylphosphorothioate ug/L 29.350 59 50-150ND
O-Toluidine ug/L 22.2 M1504450-150ND
P-Dimethylaminoazobenzene ug/L 16.6 M11001750-150ND
p-Phenylenediamine ug/L 34.950 70 50-150ND
Parathion (Ethyl parathion)ug/L 44.550 89 50-150ND
Pentachlorobenzene ug/L 33.450 67 50-150ND
Pentachloronitrobenzene ug/L 46.450 93 50-150ND
Pentachlorophenol ug/L 90.9250 36 10-118ND
Phenacetin ug/L 42.950 86 50-150ND
Phenanthrene ug/L 39.550 79 24-106ND
Phenol ug/L 17.550 35 12-110ND
Phorate ug/L 40.950 82 50-150ND
Pronamide ug/L 42.150 84 50-150ND
Pyrene ug/L 42.050 84 24-114ND
Safrole ug/L 30.650 61 50-150ND
Thionazin ug/L 38.750 77 50-150ND
2,4,6-Tribromophenol (S)%87 27-110
2-Fluorobiphenyl (S)%80 27-110
2-Fluorophenol (S)%46 12-110
Nitrobenzene-d5 (S)%73 21-110
Phenol-d6 (S)%34 10-110
Terphenyl-d14 (S)%55 31-107
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
10390835002
2015437SAMPLE DUPLICATE:
1,2,4,5-Tetrachlorobenzene ug/L ND 30ND
1,3,5-Trinitrobenzene ug/L ND 30ND
1,3-Dinitrobenzene ug/L ND 30ND
1,4-Naphthoquinone ug/L ND 30ND
1-Naphthalenamine ug/L ND 30ND
2,2'-Oxybis(1-chloropropane)ug/L ND 30ND
2,3,4,6-Tetrachlorophenol ug/L ND 30ND
2,4,5-Trichlorophenol ug/L ND IO30ND
2,4,6-Trichlorophenol ug/L ND IO30ND
2,4-Dichlorophenol ug/L ND IO30ND
2,4-Dimethylphenol ug/L ND IO30ND
2,4-Dinitrophenol ug/L ND IO30ND
2,4-Dinitrotoluene ug/L ND IO30ND
2,6-Dichlorophenol ug/L ND 30ND
2,6-Dinitrotoluene ug/L ND IO30ND
2-Acetylaminofluorene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 162 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
10390835002
2015437SAMPLE DUPLICATE:
2-Chloronaphthalene ug/L ND IO30ND
2-Chlorophenol ug/L ND 30ND
2-Methylnaphthalene ug/L ND IO30ND
2-Methylphenol(o-Cresol)ug/L ND 30ND
2-Naphthalenamine ug/L ND 30ND
2-Nitroaniline ug/L ND IO30ND
2-Nitrophenol ug/L ND IO30ND
3&4-Methylphenol(m&p Cresol)ug/L ND 30ND
3,3'-Dichlorobenzidine ug/L ND 30ND
3,3'-Dimethylbenzidine ug/L ND 30ND
3-Methylcholanthrene ug/L ND 30ND
3-Nitroaniline ug/L ND IO30ND
4,6-Dinitro-2-methylphenol ug/L ND 30ND
4-Aminobiphenyl ug/L ND 30ND
4-Bromophenylphenyl ether ug/L ND 30ND
4-Chloro-3-methylphenol ug/L ND IO30ND
4-Chloroaniline ug/L ND IO30ND
4-Chlorophenylphenyl ether ug/L ND IO30ND
4-Nitroaniline ug/L ND IO30ND
4-Nitrophenol ug/L ND IO30ND
5-Nitro-o-toluidine ug/L NDND
7,12-Dimethylbenz(a)anthracene ug/L ND 30ND
Acenaphthene ug/L ND IO30ND
Acenaphthylene ug/L ND IO30ND
Acetophenone ug/L ND 30ND
Anthracene ug/L ND 30ND
Benzo(a)anthracene ug/L ND 30ND
Benzo(a)pyrene ug/L ND 30ND
Benzo(b)fluoranthene ug/L ND 30ND
Benzo(g,h,i)perylene ug/L ND 30ND
Benzo(k)fluoranthene ug/L ND 30ND
Benzyl alcohol ug/L ND 30ND
bis(2-Chloroethoxy)methane ug/L ND IO30ND
bis(2-Chloroethyl) ether ug/L ND 30ND
bis(2-Ethylhexyl)phthalate ug/L ND 30ND
Butylbenzylphthalate ug/L ND 30ND
Chlorobenzilate ug/L ND 30ND
Chrysene ug/L ND 30ND
Di-n-butylphthalate ug/L ND 30ND
Di-n-octylphthalate ug/L ND 30ND
Diallate ug/L ND 30ND
Dibenz(a,h)anthracene ug/L ND 30ND
Dibenzofuran ug/L ND IO30ND
Diethylphthalate ug/L ND IO30ND
Dimethoate ug/L ND 30ND
Dimethylphthalate ug/L ND IO30ND
Diphenylamine ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 163 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
10390835002
2015437SAMPLE DUPLICATE:
Disulfoton ug/L ND 30ND
Ethyl methanesulfonate ug/L ND 30ND
Famphur ug/L ND 30ND
Fluoranthene ug/L ND 30ND
Fluorene ug/L ND IO30ND
Hexachlorobenzene ug/L ND 30ND
Hexachlorocyclopentadiene ug/L ND IO30ND
Hexachloroethane ug/L ND 30ND
Hexachloropropene ug/L ND 30ND
Indeno(1,2,3-cd)pyrene ug/L ND 30ND
Isodrin ug/L ND 30ND
Isophorone ug/L ND IO30ND
Isosafrole ug/L ND 30ND
Kepone ug/L ND 30ND
Methapyrilene ug/L ND 30ND
Methyl methanesulfonate ug/L ND 30ND
Methyl parathion ug/L ND 30ND
N-Nitroso-di-n-butylamine ug/L ND 30ND
N-Nitroso-di-n-propylamine ug/L ND 30ND
N-Nitrosodiethylamine ug/L ND 30ND
N-Nitrosodimethylamine ug/L ND 30ND
N-Nitrosodiphenylamine ug/L ND 30ND
N-Nitrosomethylethylamine ug/L ND 30ND
N-Nitrosopiperidine ug/L ND 30ND
N-Nitrosopyrrolidine ug/L ND 30ND
Nitrobenzene ug/L ND IO30ND
O,O,O-Triethylphosphorothioate ug/L ND 30ND
O-Toluidine ug/L ND 30ND
P-Dimethylaminoazobenzene ug/L ND 30ND
p-Phenylenediamine ug/L ND 30ND
Parathion (Ethyl parathion)ug/L ND 30ND
Pentachlorobenzene ug/L ND 30ND
Pentachloronitrobenzene ug/L ND 30ND
Pentachlorophenol ug/L ND 30ND
Phenacetin ug/L ND 30ND
Phenanthrene ug/L ND 30ND
Phenol ug/L ND 30ND
Phorate ug/L ND 30ND
Pronamide ug/L ND 30ND
Pyrene ug/L ND 30ND
Safrole ug/L ND 30ND
Thionazin ug/L ND 30ND
2,4,6-Tribromophenol (S)%71 4844
2-Fluorobiphenyl (S)%51 9119
2-Fluorophenol (S)%27 9410
Nitrobenzene-d5 (S)%47 8718
Phenol-d6 (S)%17 926
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 164 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
10390835002
2015437SAMPLE DUPLICATE:
Terphenyl-d14 (S)%53 254
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 165 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363842
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92342479001, 92342479002, 92342479003, 92342479004, 92342479005, 92342479006, 92342479007,
92342479010, 92342479011, 92342479012, 92342479013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2017031
Associated Lab Samples:92342479001, 92342479002, 92342479003, 92342479004, 92342479005, 92342479006, 92342479007,
92342479010, 92342479011, 92342479012, 92342479013
Matrix:Water
AnalyzedMDL
1,2,4,5-Tetrachlorobenzene ug/L ND 10.0 06/13/17 11:371.3
1,3,5-Trinitrobenzene ug/L ND 10.0 06/13/17 11:371.2
1,3-Dinitrobenzene ug/L ND 20.0 06/13/17 11:371.3
1,4-Naphthoquinone ug/L ND 10.0 06/13/17 11:370.99
1-Naphthalenamine ug/L ND 10.0 06/13/17 11:371.3
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 06/13/17 11:371.8
2,3,4,6-Tetrachlorophenol ug/L ND 10.0 06/13/17 11:372.9
2,4,5-Trichlorophenol ug/L ND 10.0 06/13/17 11:371.5
2,4,6-Trichlorophenol ug/L ND 10.0 06/13/17 11:371.4
2,4-Dichlorophenol ug/L ND 10.0 06/13/17 11:371.6
2,4-Dimethylphenol ug/L ND 10.0 06/13/17 11:371.6
2,4-Dinitrophenol ug/L ND 50.0 06/13/17 11:375.1
2,4-Dinitrotoluene ug/L ND 10.0 06/13/17 11:371.5
2,6-Dichlorophenol ug/L ND 10.0 06/13/17 11:371.5
2,6-Dinitrotoluene ug/L ND 10.0 06/13/17 11:371.4
2-Acetylaminofluorene ug/L ND 20.0 06/13/17 11:371.6
2-Chloronaphthalene ug/L ND 10.0 06/13/17 11:371.6
2-Chlorophenol ug/L ND 10.0 06/13/17 11:371.5
2-Methylnaphthalene ug/L ND 10.0 06/13/17 11:371.4
2-Methylphenol(o-Cresol)ug/L ND 10.0 06/13/17 11:371.6
2-Naphthalenamine ug/L ND 10.0 06/13/17 11:372.2
2-Nitroaniline ug/L ND 50.0 06/13/17 11:372.3
2-Nitrophenol ug/L ND 10.0 06/13/17 11:371.6
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 06/13/17 11:371.4
3,3'-Dichlorobenzidine ug/L ND 20.0 06/13/17 11:373.9
3,3'-Dimethylbenzidine ug/L ND 10.0 06/13/17 11:373.9
3-Methylcholanthrene ug/L ND 10.0 06/13/17 11:372.7
3-Nitroaniline ug/L ND 50.0 06/13/17 11:372.7
4,6-Dinitro-2-methylphenol ug/L ND 50.0 06/13/17 11:372.2
4-Aminobiphenyl ug/L ND 20.0 06/13/17 11:371.7
4-Bromophenylphenyl ether ug/L ND 10.0 06/13/17 11:371.5
4-Chloro-3-methylphenol ug/L ND 20.0 06/13/17 11:372.8
4-Chloroaniline ug/L ND 20.0 06/13/17 11:372.8
4-Chlorophenylphenyl ether ug/L ND 10.0 06/13/17 11:371.6
4-Nitroaniline ug/L ND 20.0 06/13/17 11:373.4
4-Nitrophenol ug/L ND 50.0 06/13/17 11:374.3
5-Nitro-o-toluidine ug/L ND 10.0 06/13/17 11:371.9
7,12-Dimethylbenz(a)anthracene ug/L ND 10.0 06/13/17 11:372.4
Acenaphthene ug/L ND 10.0 06/13/17 11:371.6
Acenaphthylene ug/L ND 10.0 06/13/17 11:371.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 166 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2017031
Associated Lab Samples:92342479001, 92342479002, 92342479003, 92342479004, 92342479005, 92342479006, 92342479007,
92342479010, 92342479011, 92342479012, 92342479013
Matrix:Water
AnalyzedMDL
Acetophenone ug/L ND 10.0 06/13/17 11:371.9
Anthracene ug/L ND 10.0 06/13/17 11:371.7
Benzo(a)anthracene ug/L ND 10.0 06/13/17 11:372.1
Benzo(a)pyrene ug/L ND 10.0 06/13/17 11:372.2
Benzo(b)fluoranthene ug/L ND 10.0 06/13/17 11:372.2
Benzo(g,h,i)perylene ug/L ND 10.0 06/13/17 11:372.1
Benzo(k)fluoranthene ug/L ND 10.0 06/13/17 11:372.0
Benzyl alcohol ug/L ND 20.0 06/13/17 11:373.1
bis(2-Chloroethoxy)methane ug/L ND 10.0 06/13/17 11:371.6
bis(2-Chloroethyl) ether ug/L ND 10.0 06/13/17 11:371.7
bis(2-Ethylhexyl)phthalate ug/L ND 15.0 06/13/17 11:372.3
Butylbenzylphthalate ug/L ND 10.0 06/13/17 11:372.5
Chlorobenzilate ug/L ND 10.0 06/13/17 11:372.2
Chrysene ug/L ND 10.0 06/13/17 11:372.1
Di-n-butylphthalate ug/L ND 10.0 06/13/17 11:372.0
Di-n-octylphthalate ug/L ND 10.0 06/13/17 11:371.5
Diallate ug/L ND 10.0 06/13/17 11:371.6
Dibenz(a,h)anthracene ug/L ND 10.0 06/13/17 11:372.0
Dibenzofuran ug/L ND 10.0 06/13/17 11:371.7
Diethylphthalate ug/L ND 6000 06/13/17 11:371.6
Dimethoate ug/L ND 20.0 06/13/17 11:371.8
Dimethylphthalate ug/L ND 10.0 06/13/17 11:371.4
Diphenylamine ug/L ND 10.0 06/13/17 11:371.4
Disulfoton ug/L ND 10.0 06/13/17 11:371.5
Ethyl methanesulfonate ug/L ND 20.0 06/13/17 11:371.6
Famphur ug/L ND 20.0 06/13/17 11:375.7
Fluoranthene ug/L ND 10.0 06/13/17 11:372.2
Fluorene ug/L ND 10.0 06/13/17 11:371.6
Hexachlorobenzene ug/L ND 10.0 06/13/17 11:371.7
Hexachlorocyclopentadiene ug/L ND 10.0 06/13/17 11:371.3
Hexachloroethane ug/L ND 10.0 06/13/17 11:371.8
Hexachloropropene ug/L ND 10.0 06/13/17 11:371.2
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 06/13/17 11:372.0
Isodrin ug/L ND 20.0 06/13/17 11:372.5
Isophorone ug/L ND 10.0 06/13/17 11:371.5
Isosafrole ug/L ND 10.0 06/13/17 11:371.5
Kepone ug/L ND 20.0 06/13/17 11:374.5
Methapyrilene ug/L ND 100 06/13/17 11:373.0
Methyl methanesulfonate ug/L ND 10.0 06/13/17 11:371.1
Methyl parathion ug/L ND 10.0 06/13/17 11:371.6
N-Nitroso-di-n-butylamine ug/L ND 10.0 06/13/17 11:371.6
N-Nitroso-di-n-propylamine ug/L ND 10.0 06/13/17 11:371.7
N-Nitrosodiethylamine ug/L ND 20.0 06/13/17 11:371.4
N-Nitrosodimethylamine ug/L ND 10.0 06/13/17 11:371.6
N-Nitrosodiphenylamine ug/L ND 10.0 06/13/17 11:371.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 167 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2017031
Associated Lab Samples:92342479001, 92342479002, 92342479003, 92342479004, 92342479005, 92342479006, 92342479007,
92342479010, 92342479011, 92342479012, 92342479013
Matrix:Water
AnalyzedMDL
N-Nitrosomethylethylamine ug/L ND 10.0 06/13/17 11:371.4
N-Nitrosopiperidine ug/L ND 20.0 06/13/17 11:371.7
N-Nitrosopyrrolidine ug/L ND 10.0 06/13/17 11:371.7
Nitrobenzene ug/L ND 10.0 06/13/17 11:371.6
O,O,O-Triethylphosphorothioate ug/L ND 10.0 06/13/17 11:371.7
O-Toluidine ug/L ND 10.0 06/13/17 11:371.7
P-Dimethylaminoazobenzene ug/L ND 10.0 06/13/17 11:371.0
p-Phenylenediamine ug/L ND 10.0 06/13/17 11:372.2
Parathion (Ethyl parathion)ug/L ND 10.0 06/13/17 11:371.5
Pentachlorobenzene ug/L ND 10.0 06/13/17 11:371.5
Pentachloronitrobenzene ug/L ND 20.0 06/13/17 11:371.7
Pentachlorophenol ug/L ND 25.0 06/13/17 11:373.5
Phenacetin ug/L ND 20.0 06/13/17 11:371.9
Phenanthrene ug/L ND 10.0 06/13/17 11:371.6
Phenol ug/L ND 10.0 06/13/17 11:371.3
Phorate ug/L ND 10.0 06/13/17 11:371.7
Pronamide ug/L ND 10.0 06/13/17 11:372.0
Pyrene ug/L ND 10.0 06/13/17 11:372.2
Safrole ug/L ND 10.0 06/13/17 11:371.3
Thionazin ug/L ND 20.0 06/13/17 11:371.7
2,4,6-Tribromophenol (S)%76 27-110 06/13/17 11:37
2-Fluorobiphenyl (S)%85 27-110 06/13/17 11:37
2-Fluorophenol (S)%41 12-110 06/13/17 11:37
Nitrobenzene-d5 (S)%69 21-110 06/13/17 11:37
Phenol-d6 (S)%27 10-110 06/13/17 11:37
Terphenyl-d14 (S)%90 31-107 06/13/17 11:37
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2017032LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4,5-Tetrachlorobenzene ug/L 11.950 24 16-129
1,3,5-Trinitrobenzene ug/L 26.1 L2505255-125
1,3-Dinitrobenzene ug/L 31.850 64 30-122
1,4-Naphthoquinone ug/L 29.250 58 31-120
1-Naphthalenamine ug/L 21.450 43 37-126
2,2'-Oxybis(1-chloropropane)ug/L 16.950 34 18-120
2,3,4,6-Tetrachlorophenol ug/L 62.950 126 54-276
2,4,5-Trichlorophenol ug/L 28.150 56 43-113
2,4,6-Trichlorophenol ug/L 28.050 56 42-120
2,4-Dichlorophenol ug/L 14.4 L2502930-120
2,4-Dimethylphenol ug/L 12.6 L2502529-111
2,4-Dinitrophenol ug/L 170250 68 19-132
2,4-Dinitrotoluene ug/L 35.550 71 58-128
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 168 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2017032LABORATORY CONTROL SAMPLE:
LCSSpike
2,6-Dichlorophenol ug/L 13.0 L2502654-128
2,6-Dinitrotoluene ug/L 34.850 70 54-129
2-Acetylaminofluorene ug/L 27.9 L2505681-160
2-Chloronaphthalene ug/L 20.7 L2504143-117
2-Chlorophenol ug/L 12.6 L2502537-120
2-Methylnaphthalene ug/L 12.5 L2502533-120
2-Methylphenol(o-Cresol)ug/L 9.8J L2502031-120
2-Naphthalenamine ug/L 26.850 54 41-136
2-Nitroaniline ug/L 68.2100 68 48-121
2-Nitrophenol ug/L 11.3 L2502325-116
3&4-Methylphenol(m&p Cresol)ug/L 7.8J L2501623-120
3,3'-Dichlorobenzidine ug/L 66.9250 27 10-154
3,3'-Dimethylbenzidine ug/L 37.3100 37 10-157
3-Methylcholanthrene ug/L 37.250 74 65-130
3-Nitroaniline ug/L 82.7100 83 43-115
4,6-Dinitro-2-methylphenol ug/L 63.9100 64 44-124
4-Aminobiphenyl ug/L 25.650 51 21-125
4-Bromophenylphenyl ether ug/L 26.950 54 34-113
4-Chloro-3-methylphenol ug/L 44.0100 44 31-110
4-Chloroaniline ug/L 33.6100 34 20-120
4-Chlorophenylphenyl ether ug/L 28.050 56 34-116
4-Nitroaniline ug/L 89.4100 89 46-128
4-Nitrophenol ug/L 64.6250 26 11-120
5-Nitro-o-toluidine ug/L 36.3 L2507378-160
7,12-Dimethylbenz(a)anthracene ug/L 37.650 75 47-124
Acenaphthene ug/L 26.450 53 48-114
Acenaphthylene ug/L 26.450 53 48-112
Acetophenone ug/L 12.650 25 24-120
Anthracene ug/L 35.050 70 57-118
Benzo(a)anthracene ug/L 33.050 66 56-121
Benzo(a)pyrene ug/L 37.150 74 55-127
Benzo(b)fluoranthene ug/L 39.850 80 53-128
Benzo(g,h,i)perylene ug/L 33.550 67 54-125
Benzo(k)fluoranthene ug/L 38.950 78 51-123
Benzyl alcohol ug/L 21.4 L21002127-120
bis(2-Chloroethoxy)methane ug/L 10.4 L2502132-120
bis(2-Chloroethyl) ether ug/L 11.0 L2502233-111
bis(2-Ethylhexyl)phthalate ug/L 34.750 69 50-145
Butylbenzylphthalate ug/L 35.850 72 54-138
Chlorobenzilate ug/L 33.950 68 65-132
Chrysene ug/L 33.050 66 58-127
Di-n-butylphthalate ug/L 38.450 77 56-125
Di-n-octylphthalate ug/L 31.150 62 50-134
Diallate ug/L 26.750 53 47-123
Dibenz(a,h)anthracene ug/L 36.250 72 53-129
Dibenzofuran ug/L 29.750 59 45-120
Diethylphthalate ug/L 38.5J50 77 53-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 169 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2017032LABORATORY CONTROL SAMPLE:
LCSSpike
Dimethoate ug/L 34.350 69 57-139
Dimethylphthalate ug/L 38.450 77 55-116
Diphenylamine ug/L 35.350 71 42-120
Disulfoton ug/L 26.750 53 49-156
Ethyl methanesulfonate ug/L 9.5J L2501943-120
Famphur ug/L 122100 122 40-160
Fluoranthene ug/L 35.750 71 57-125
Fluorene ug/L 32.550 65 53-118
Hexachlorobenzene ug/L 31.550 63 49-116
Hexachlorocyclopentadiene ug/L 9.5J L2501926-158
Hexachloroethane ug/L 8.3J L2501730-114
Hexachloropropene ug/L 7.0J50 14 13-137
Indeno(1,2,3-cd)pyrene ug/L 35.250 70 55-128
Isodrin ug/L 34.450 69 68-129
Isophorone ug/L 13.3 L2502731-118
Isosafrole ug/L 19.0 L2503848-107
Kepone ug/L 69.7100 70 10-124
Methapyrilene ug/L 22.4J50 45 40-160
Methyl methanesulfonate ug/L 15.950 32 25-114
Methyl parathion ug/L 33.750 67 58-137
N-Nitroso-di-n-butylamine ug/L 15.0 L2503036-115
N-Nitroso-di-n-propylamine ug/L 12.8 L2502632-119
N-Nitrosodiethylamine ug/L 10.9J L2502247-115
N-Nitrosodimethylamine ug/L 8.7J50 17 13-120
N-Nitrosodiphenylamine ug/L 35.350 71 43-120
N-Nitrosomethylethylamine ug/L 9.7J L2501939-120
N-Nitrosopiperidine ug/L 12.1J L2502443-113
N-Nitrosopyrrolidine ug/L 12.5 L2502532-110
Nitrobenzene ug/L 10.8 L2502233-110
O,O,O-Triethylphosphorothioate ug/L 10.6 L2502151-127
O-Toluidine ug/L 10.0 L2502027-120
P-Dimethylaminoazobenzene ug/L 13.5100 13 10-120
p-Phenylenediamine ug/L 25.7 L2505172-143
Parathion (Ethyl parathion)ug/L 27.4 L2505556-140
Pentachlorobenzene ug/L 25.050 50 30-137
Pentachloronitrobenzene ug/L 37.150 74 70-124
Pentachlorophenol ug/L 70.3250 28 10-137
Phenacetin ug/L 29.950 60 60-130
Phenanthrene ug/L 35.350 71 57-117
Phenol ug/L 5.6J50 11 10-120
Phorate ug/L 26.1 L2505255-126
Pronamide ug/L 33.2 L2506675-124
Pyrene ug/L 37.050 74 55-122
Safrole ug/L 11.8 L2502441-120
Thionazin ug/L 29.4 L2505963-137
2,4,6-Tribromophenol (S)%69 27-110
2-Fluorobiphenyl (S)%37 27-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 170 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2017032LABORATORY CONTROL SAMPLE:
LCSSpike
2-Fluorophenol (S)%15 12-110
Nitrobenzene-d5 (S)%23 21-110
Phenol-d6 (S)%10 10-110
Terphenyl-d14 (S)%72 31-107
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2017033MATRIX SPIKE SAMPLE:
MSSpike
Result
92342479002
1,2,4,5-Tetrachlorobenzene ug/L 32.250 64 50-150ND
1,3,5-Trinitrobenzene ug/L 30.050 60 50-150ND
1,3-Dinitrobenzene ug/L 38.350 77 50-150ND
1,4-Naphthoquinone ug/L 49.050 98 50-150ND
1-Naphthalenamine ug/L 19.0 M1503850-150ND
2,2'-Oxybis(1-chloropropane)ug/L 53.850 108 50-150ND
2,3,4,6-Tetrachlorophenol ug/L 75.8 M15015250-150ND
2,4,5-Trichlorophenol ug/L 39.750 79 19-105ND
2,4,6-Trichlorophenol ug/L 46.550 93 13-108ND
2,4-Dichlorophenol ug/L 39.050 78 29-111ND
2,4-Dimethylphenol ug/L 36.950 74 21-103ND
2,4-Dinitrophenol ug/L 223250 89 10-109ND
2,4-Dinitrotoluene ug/L 41.450 83 27-104ND
2,6-Dichlorophenol ug/L 40.350 81 50-150ND
2,6-Dinitrotoluene ug/L 43.650 87 28-101ND
2-Acetylaminofluorene ug/L 30.150 60 50-150ND
2-Chloronaphthalene ug/L 46.650 93 14-102ND
2-Chlorophenol ug/L 37.550 75 16-110ND
2-Methylnaphthalene ug/L 34.550 69 13-110ND
2-Methylphenol(o-Cresol)ug/L 32.650 65 19-110ND
2-Naphthalenamine ug/L 8.3J M1501750-150ND
2-Nitroaniline ug/L 88.7100 89 26-103ND
2-Nitrophenol ug/L 37.550 75 20-110ND
3&4-Methylphenol(m&p Cresol)ug/L 28.350 57 20-110ND
3,3'-Dichlorobenzidine ug/L 61.8250 25 25-112ND
3,3'-Dimethylbenzidine ug/L 7.8J M1100850-150ND
3-Methylcholanthrene ug/L 38.450 76 50-150ND
3-Nitroaniline ug/L 97.2100 97 29-110ND
4,6-Dinitro-2-methylphenol ug/L 77.9100 78 10-117ND
4-Aminobiphenyl ug/L 21.1 M1504250-150ND
4-Bromophenylphenyl ether ug/L 32.350 65 20-105ND
4-Chloro-3-methylphenol ug/L 67.6100 68 22-110ND
4-Chloroaniline ug/L 74.3100 74 20-100ND
4-Chlorophenylphenyl ether ug/L 39.150 78 19-102ND
4-Nitroaniline ug/L 105100 105 29-110ND
4-Nitrophenol ug/L 77.4250 31 10-110ND
5-Nitro-o-toluidine ug/L 41.850 84 50-150ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 171 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2017033MATRIX SPIKE SAMPLE:
MSSpike
Result
92342479002
7,12-Dimethylbenz(a)anthracene ug/L 41.050 81 50-150ND
Acenaphthene ug/L 44.650 89 17-100ND
Acenaphthylene ug/L 45.850 92 21-100ND
Acetophenone ug/L 40.050 80 50-150ND
Anthracene ug/L 40.150 80 24-109ND
Benzo(a)anthracene ug/L 35.450 71 22-117ND
Benzo(a)pyrene ug/L 40.450 81 23-104ND
Benzo(b)fluoranthene ug/L 45.150 90 23-103ND
Benzo(g,h,i)perylene ug/L 37.750 75 18-111ND
Benzo(k)fluoranthene ug/L 41.350 83 22-113ND
Benzyl alcohol ug/L 66.1100 66 19-101ND
bis(2-Chloroethoxy)methane ug/L 32.150 64 22-110ND
bis(2-Chloroethyl) ether ug/L 33.250 66 16-110ND
bis(2-Ethylhexyl)phthalate ug/L 35.450 71 23-102ND
Butylbenzylphthalate ug/L 36.750 73 25-110ND
Chlorobenzilate ug/L 34.450 68 50-150ND
Chrysene ug/L 35.450 71 23-115ND
Di-n-butylphthalate ug/L 42.450 85 26-110ND
Di-n-octylphthalate ug/L 33.750 67 22-110ND
Diallate ug/L 31.350 63 50-150ND
Dibenz(a,h)anthracene ug/L 40.050 80 21-112ND
Dibenzofuran ug/L 45.750 91 19-102ND
Diethylphthalate ug/L 44.8J50 90 29-110ND
Dimethoate ug/L 40.850 82 50-150ND
Dimethylphthalate ug/L 46.750 93 27-110ND
Diphenylamine ug/L 38.550 77 50-150ND
Disulfoton ug/L 27.850 56 50-150ND
Ethyl methanesulfonate ug/L 29.750 59 50-150ND
Famphur ug/L 160 M110016050-150ND
Fluoranthene ug/L 41.850 84 23-112ND
Fluorene ug/L 43.850 88 22-104ND
Hexachlorobenzene ug/L 36.350 73 21-116ND
Hexachlorocyclopentadiene ug/L 33.750 67 10-110ND
Hexachloroethane ug/L 23.550 47 10-110ND
Hexachloropropene ug/L 21.5 M1504350-150ND
Indeno(1,2,3-cd)pyrene ug/L 39.350 79 20-113ND
Isodrin ug/L 37.950 76 50-150ND
Isophorone ug/L 35.850 72 50-150ND
Isosafrole ug/L 38.150 76 50-150ND
Kepone ug/L 96.4100 96 50-150ND
Methapyrilene ug/L 6.9J M1501450-150ND
Methyl methanesulfonate ug/L 48.550 97 50-150ND
Methyl parathion ug/L 40.050 80 50-150ND
N-Nitroso-di-n-butylamine ug/L 33.850 68 50-150ND
N-Nitroso-di-n-propylamine ug/L 43.050 86 21-105ND
N-Nitrosodiethylamine ug/L 33.450 67 50-150ND
N-Nitrosodimethylamine ug/L 23.350 47 10-110ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 172 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2017033MATRIX SPIKE SAMPLE:
MSSpike
Result
92342479002
N-Nitrosodiphenylamine ug/L 38.550 77 23-107ND
N-Nitrosomethylethylamine ug/L 26.650 53 50-150ND
N-Nitrosopiperidine ug/L 38.550 77 50-150ND
N-Nitrosopyrrolidine ug/L 37.850 76 50-150ND
Nitrobenzene ug/L 31.450 63 20-110ND
O,O,O-Triethylphosphorothioate ug/L 37.050 74 50-150ND
O-Toluidine ug/L 26.650 53 50-150ND
P-Dimethylaminoazobenzene ug/L 11.2 M11001150-150ND
p-Phenylenediamine ug/L 35.550 71 50-150ND
Parathion (Ethyl parathion)ug/L 32.050 64 50-150ND
Pentachlorobenzene ug/L 40.250 80 50-150ND
Pentachloronitrobenzene ug/L 41.750 83 50-150ND
Pentachlorophenol ug/L 83.9250 34 10-118ND
Phenacetin ug/L 35.050 70 50-150ND
Phenanthrene ug/L 40.550 81 24-106ND
Phenol ug/L 16.550 33 12-110ND
Phorate ug/L 30.050 60 50-150ND
Pronamide ug/L 37.650 75 50-150ND
Pyrene ug/L 36.350 73 24-114ND
Safrole ug/L 38.050 76 50-150ND
Thionazin ug/L 34.450 69 50-150ND
2,4,6-Tribromophenol (S)%78 27-110
2-Fluorobiphenyl (S)%88 27-110
2-Fluorophenol (S)%42 12-110
Nitrobenzene-d5 (S)%66 21-110
Phenol-d6 (S)%30 10-110
Terphenyl-d14 (S)%61 31-107
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342479007
2018660SAMPLE DUPLICATE:
1,2,4,5-Tetrachlorobenzene ug/L ND 30ND
1,3,5-Trinitrobenzene ug/L ND 30ND
1,3-Dinitrobenzene ug/L ND 30ND
1,4-Naphthoquinone ug/L ND 30ND
1-Naphthalenamine ug/L ND 30ND
2,2'-Oxybis(1-chloropropane)ug/L ND 30ND
2,3,4,6-Tetrachlorophenol ug/L ND 30ND
2,4,5-Trichlorophenol ug/L ND 30ND
2,4,6-Trichlorophenol ug/L ND 30ND
2,4-Dichlorophenol ug/L ND 30ND
2,4-Dimethylphenol ug/L ND 30ND
2,4-Dinitrophenol ug/L ND 30ND
2,4-Dinitrotoluene ug/L ND 30ND
2,6-Dichlorophenol ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 173 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342479007
2018660SAMPLE DUPLICATE:
2,6-Dinitrotoluene ug/L ND 30ND
2-Acetylaminofluorene ug/L ND 30ND
2-Chloronaphthalene ug/L ND 30ND
2-Chlorophenol ug/L ND 30ND
2-Methylnaphthalene ug/L ND 30ND
2-Methylphenol(o-Cresol)ug/L ND 30ND
2-Naphthalenamine ug/L ND 30ND
2-Nitroaniline ug/L ND 30ND
2-Nitrophenol ug/L ND 30ND
3&4-Methylphenol(m&p Cresol)ug/L ND 30ND
3,3'-Dichlorobenzidine ug/L ND 30ND
3,3'-Dimethylbenzidine ug/L ND 30ND
3-Methylcholanthrene ug/L ND 30ND
3-Nitroaniline ug/L ND 30ND
4,6-Dinitro-2-methylphenol ug/L ND 30ND
4-Aminobiphenyl ug/L ND 30ND
4-Bromophenylphenyl ether ug/L ND 30ND
4-Chloro-3-methylphenol ug/L ND 30ND
4-Chloroaniline ug/L ND 30ND
4-Chlorophenylphenyl ether ug/L ND 30ND
4-Nitroaniline ug/L ND 30ND
4-Nitrophenol ug/L ND 30ND
5-Nitro-o-toluidine ug/L NDND
7,12-Dimethylbenz(a)anthracene ug/L ND 30ND
Acenaphthene ug/L ND 30ND
Acenaphthylene ug/L ND 30ND
Acetophenone ug/L ND 30ND
Anthracene ug/L ND 30ND
Benzo(a)anthracene ug/L ND 30ND
Benzo(a)pyrene ug/L ND 30ND
Benzo(b)fluoranthene ug/L ND 30ND
Benzo(g,h,i)perylene ug/L ND 30ND
Benzo(k)fluoranthene ug/L ND 30ND
Benzyl alcohol ug/L ND 30ND
bis(2-Chloroethoxy)methane ug/L ND 30ND
bis(2-Chloroethyl) ether ug/L ND 30ND
bis(2-Ethylhexyl)phthalate ug/L ND 30ND
Butylbenzylphthalate ug/L ND 30ND
Chlorobenzilate ug/L ND 30ND
Chrysene ug/L ND 30ND
Di-n-butylphthalate ug/L ND 30ND
Di-n-octylphthalate ug/L ND 30ND
Diallate ug/L ND 30ND
Dibenz(a,h)anthracene ug/L ND 30ND
Dibenzofuran ug/L ND 30ND
Diethylphthalate ug/L ND 30ND
Dimethoate ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 174 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342479007
2018660SAMPLE DUPLICATE:
Dimethylphthalate ug/L ND 30ND
Diphenylamine ug/L ND 30ND
Disulfoton ug/L ND 30ND
Ethyl methanesulfonate ug/L ND 30ND
Famphur ug/L ND 30ND
Fluoranthene ug/L ND 30ND
Fluorene ug/L ND 30ND
Hexachlorobenzene ug/L ND 30ND
Hexachlorocyclopentadiene ug/L ND 30ND
Hexachloroethane ug/L ND 30ND
Hexachloropropene ug/L ND 30ND
Indeno(1,2,3-cd)pyrene ug/L ND 30ND
Isodrin ug/L ND 30ND
Isophorone ug/L ND 30ND
Isosafrole ug/L ND 30ND
Kepone ug/L ND 30ND
Methapyrilene ug/L ND 30ND
Methyl methanesulfonate ug/L ND 30ND
Methyl parathion ug/L ND 30ND
N-Nitroso-di-n-butylamine ug/L ND 30ND
N-Nitroso-di-n-propylamine ug/L ND 30ND
N-Nitrosodiethylamine ug/L ND 30ND
N-Nitrosodimethylamine ug/L ND 30ND
N-Nitrosodiphenylamine ug/L ND 30ND
N-Nitrosomethylethylamine ug/L ND 30ND
N-Nitrosopiperidine ug/L ND 30ND
N-Nitrosopyrrolidine ug/L ND 30ND
Nitrobenzene ug/L ND 30ND
O,O,O-Triethylphosphorothioate ug/L ND 30ND
O-Toluidine ug/L ND 30ND
P-Dimethylaminoazobenzene ug/L ND 30ND
p-Phenylenediamine ug/L ND 30ND
Parathion (Ethyl parathion)ug/L ND 30ND
Pentachlorobenzene ug/L ND 30ND
Pentachloronitrobenzene ug/L ND 30ND
Pentachlorophenol ug/L ND 30ND
Phenacetin ug/L ND 30ND
Phenanthrene ug/L ND 30ND
Phenol ug/L ND 30ND
Phorate ug/L ND 30ND
Pronamide ug/L ND 30ND
Pyrene ug/L ND 30ND
Safrole ug/L ND 30ND
Thionazin ug/L ND 30ND
2,4,6-Tribromophenol (S)%84 689
2-Fluorobiphenyl (S)%100 1090
2-Fluorophenol (S)%41 744
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 175 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342479007
2018660SAMPLE DUPLICATE:
Nitrobenzene-d5 (S)%81 1372
Phenol-d6 (S)%26 728
Terphenyl-d14 (S)%81 1998
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 176 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
364049
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92342529001, 92342529002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2018678
Associated Lab Samples:92342529001, 92342529002
Matrix:Water
AnalyzedMDL
1,2,4,5-Tetrachlorobenzene ug/L ND 10.0 06/14/17 13:231.3
1,3,5-Trinitrobenzene ug/L ND 10.0 06/14/17 13:231.2
1,3-Dinitrobenzene ug/L ND 20.0 06/14/17 13:231.3
1,4-Naphthoquinone ug/L ND 10.0 06/14/17 13:230.99
1-Naphthalenamine ug/L ND 10.0 06/14/17 13:231.3
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 06/14/17 13:231.8
2,3,4,6-Tetrachlorophenol ug/L ND 10.0 06/14/17 13:232.9
2,4,5-Trichlorophenol ug/L ND 10.0 06/14/17 13:231.5
2,4,6-Trichlorophenol ug/L ND 10.0 06/14/17 13:231.4
2,4-Dichlorophenol ug/L ND 10.0 06/14/17 13:231.6
2,4-Dimethylphenol ug/L ND 10.0 06/14/17 13:231.6
2,4-Dinitrophenol ug/L ND 50.0 06/14/17 13:235.1
2,4-Dinitrotoluene ug/L ND 10.0 06/14/17 13:231.5
2,6-Dichlorophenol ug/L ND 10.0 06/14/17 13:231.5
2,6-Dinitrotoluene ug/L ND 10.0 06/14/17 13:231.4
2-Acetylaminofluorene ug/L ND 20.0 06/14/17 13:231.6
2-Chloronaphthalene ug/L ND 10.0 06/14/17 13:231.6
2-Chlorophenol ug/L ND 10.0 06/14/17 13:231.5
2-Methylnaphthalene ug/L ND 10.0 06/14/17 13:231.4
2-Methylphenol(o-Cresol)ug/L ND 10.0 06/14/17 13:231.6
2-Naphthalenamine ug/L ND 10.0 06/14/17 13:232.2
2-Nitroaniline ug/L ND 50.0 06/14/17 13:232.3
2-Nitrophenol ug/L ND 10.0 06/14/17 13:231.6
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 06/14/17 13:231.4
3,3'-Dichlorobenzidine ug/L ND 20.0 06/14/17 13:233.9
3,3'-Dimethylbenzidine ug/L ND 10.0 06/14/17 13:233.9
3-Methylcholanthrene ug/L ND 10.0 06/14/17 13:232.7
3-Nitroaniline ug/L ND 50.0 06/14/17 13:232.7
4,6-Dinitro-2-methylphenol ug/L ND 50.0 06/14/17 13:232.2
4-Aminobiphenyl ug/L ND 20.0 06/14/17 13:231.7
4-Bromophenylphenyl ether ug/L ND 10.0 06/14/17 13:231.5
4-Chloro-3-methylphenol ug/L ND 20.0 06/14/17 13:232.8
4-Chloroaniline ug/L ND 20.0 06/14/17 13:232.8
4-Chlorophenylphenyl ether ug/L ND 10.0 06/14/17 13:231.6
4-Nitroaniline ug/L ND 20.0 06/14/17 13:233.4
4-Nitrophenol ug/L ND 50.0 06/14/17 13:234.3
5-Nitro-o-toluidine ug/L ND 10.0 06/14/17 13:231.9
7,12-Dimethylbenz(a)anthracene ug/L ND 10.0 06/14/17 13:232.4
Acenaphthene ug/L ND 10.0 06/14/17 13:231.6
Acenaphthylene ug/L ND 10.0 06/14/17 13:231.5
Acetophenone ug/L ND 10.0 06/14/17 13:231.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 177 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2018678
Associated Lab Samples:92342529001, 92342529002
Matrix:Water
AnalyzedMDL
Anthracene ug/L ND 10.0 06/14/17 13:231.7
Benzo(a)anthracene ug/L ND 10.0 06/14/17 13:232.1
Benzo(a)pyrene ug/L ND 10.0 06/14/17 13:232.2
Benzo(b)fluoranthene ug/L ND 10.0 06/14/17 13:232.2
Benzo(g,h,i)perylene ug/L ND 10.0 06/14/17 13:232.1
Benzo(k)fluoranthene ug/L ND 10.0 06/14/17 13:232.0
Benzyl alcohol ug/L ND 20.0 06/14/17 13:233.1
bis(2-Chloroethoxy)methane ug/L ND 10.0 06/14/17 13:231.6
bis(2-Chloroethyl) ether ug/L ND 10.0 06/14/17 13:231.7
bis(2-Ethylhexyl)phthalate ug/L ND 15.0 06/14/17 13:232.3
Butylbenzylphthalate ug/L ND 10.0 06/14/17 13:232.5
Chlorobenzilate ug/L ND 10.0 06/14/17 13:232.2
Chrysene ug/L ND 10.0 06/14/17 13:232.1
Di-n-butylphthalate ug/L ND 10.0 06/14/17 13:232.0
Di-n-octylphthalate ug/L ND 10.0 06/14/17 13:231.5
Diallate ug/L ND 10.0 06/14/17 13:231.6
Dibenz(a,h)anthracene ug/L ND 10.0 06/14/17 13:232.0
Dibenzofuran ug/L ND 10.0 06/14/17 13:231.7
Diethylphthalate ug/L ND 6000 06/14/17 13:231.6
Dimethoate ug/L ND 20.0 06/14/17 13:231.8
Dimethylphthalate ug/L ND 10.0 06/14/17 13:231.4
Diphenylamine ug/L ND 10.0 06/14/17 13:231.4
Disulfoton ug/L ND 10.0 06/14/17 13:231.5
Ethyl methanesulfonate ug/L ND 20.0 06/14/17 13:231.6
Famphur ug/L ND 20.0 06/14/17 13:235.7
Fluoranthene ug/L ND 10.0 06/14/17 13:232.2
Fluorene ug/L ND 10.0 06/14/17 13:231.6
Hexachlorobenzene ug/L ND 10.0 06/14/17 13:231.7
Hexachlorocyclopentadiene ug/L ND 10.0 06/14/17 13:231.3
Hexachloroethane ug/L ND 10.0 06/14/17 13:231.8
Hexachloropropene ug/L ND 10.0 06/14/17 13:231.2
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 06/14/17 13:232.0
Isodrin ug/L ND 20.0 06/14/17 13:232.5
Isophorone ug/L ND 10.0 06/14/17 13:231.5
Isosafrole ug/L ND 10.0 06/14/17 13:231.5
Kepone ug/L ND 20.0 06/14/17 13:234.5
Methapyrilene ug/L ND 100 06/14/17 13:233.0
Methyl methanesulfonate ug/L ND 10.0 06/14/17 13:231.1
Methyl parathion ug/L ND 10.0 06/14/17 13:231.6
N-Nitroso-di-n-butylamine ug/L ND 10.0 06/14/17 13:231.6
N-Nitroso-di-n-propylamine ug/L ND 10.0 06/14/17 13:231.7
N-Nitrosodiethylamine ug/L ND 20.0 06/14/17 13:231.4
N-Nitrosodimethylamine ug/L ND 10.0 06/14/17 13:231.6
N-Nitrosodiphenylamine ug/L ND 10.0 06/14/17 13:231.4
N-Nitrosomethylethylamine ug/L ND 10.0 06/14/17 13:231.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
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Page 178 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2018678
Associated Lab Samples:92342529001, 92342529002
Matrix:Water
AnalyzedMDL
N-Nitrosopiperidine ug/L ND 20.0 06/14/17 13:231.7
N-Nitrosopyrrolidine ug/L ND 10.0 06/14/17 13:231.7
Nitrobenzene ug/L ND 10.0 06/14/17 13:231.6
O,O,O-Triethylphosphorothioate ug/L ND 10.0 06/14/17 13:231.7
O-Toluidine ug/L ND 10.0 06/14/17 13:231.7
P-Dimethylaminoazobenzene ug/L ND 10.0 06/14/17 13:231.0
p-Phenylenediamine ug/L ND 10.0 06/14/17 13:232.2
Parathion (Ethyl parathion)ug/L ND 10.0 06/14/17 13:231.5
Pentachlorobenzene ug/L ND 10.0 06/14/17 13:231.5
Pentachloronitrobenzene ug/L ND 20.0 06/14/17 13:231.7
Pentachlorophenol ug/L ND 25.0 06/14/17 13:233.5
Phenacetin ug/L ND 20.0 06/14/17 13:231.9
Phenanthrene ug/L ND 10.0 06/14/17 13:231.6
Phenol ug/L ND 10.0 06/14/17 13:231.3
Phorate ug/L ND 10.0 06/14/17 13:231.7
Pronamide ug/L ND 10.0 06/14/17 13:232.0
Pyrene ug/L ND 10.0 06/14/17 13:232.2
Safrole ug/L ND 10.0 06/14/17 13:231.3
Thionazin ug/L ND 20.0 06/14/17 13:231.7
2,4,6-Tribromophenol (S)%74 27-110 06/14/17 13:23
2-Fluorobiphenyl (S)%77 27-110 06/14/17 13:23
2-Fluorophenol (S)%37 12-110 06/14/17 13:23
Nitrobenzene-d5 (S)%62 21-110 06/14/17 13:23
Phenol-d6 (S)%25 10-110 06/14/17 13:23
Terphenyl-d14 (S)%87 31-107 06/14/17 13:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2018679LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4,5-Tetrachlorobenzene ug/L 34.450 69 16-129
1,3,5-Trinitrobenzene ug/L 32.650 65 55-125
1,3-Dinitrobenzene ug/L 42.550 85 30-122
1,4-Naphthoquinone ug/L 41.850 84 31-120
1-Naphthalenamine ug/L 27.050 54 37-126
2,2'-Oxybis(1-chloropropane)ug/L 52.950 106 18-120
2,3,4,6-Tetrachlorophenol ug/L 82.350 165 54-276
2,4,5-Trichlorophenol ug/L 43.150 86 43-113
2,4,6-Trichlorophenol ug/L 50.850 102 42-120
2,4-Dichlorophenol ug/L 42.750 85 30-120
2,4-Dimethylphenol ug/L 37.950 76 29-111
2,4-Dinitrophenol ug/L 246250 98 19-132
2,4-Dinitrotoluene ug/L 45.150 90 58-128
2,6-Dichlorophenol ug/L 43.650 87 54-128
2,6-Dinitrotoluene ug/L 47.050 94 54-129
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 179 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2018679LABORATORY CONTROL SAMPLE:
LCSSpike
2-Acetylaminofluorene ug/L 38.7 L2507781-160
2-Chloronaphthalene ug/L 53.050 106 43-117
2-Chlorophenol ug/L 41.950 84 37-120
2-Methylnaphthalene ug/L 37.650 75 33-120
2-Methylphenol(o-Cresol)ug/L 34.350 69 31-120
2-Naphthalenamine ug/L 34.150 68 41-136
2-Nitroaniline ug/L 88.7100 89 48-121
2-Nitrophenol ug/L 40.750 81 25-116
3&4-Methylphenol(m&p Cresol)ug/L 29.850 60 23-120
3,3'-Dichlorobenzidine ug/L 88.8250 36 10-154
3,3'-Dimethylbenzidine ug/L 41.5100 42 10-157
3-Methylcholanthrene ug/L 46.850 94 65-130
3-Nitroaniline ug/L 107100 107 43-115
4,6-Dinitro-2-methylphenol ug/L 87.7100 88 44-124
4-Aminobiphenyl ug/L 25.750 51 21-125
4-Bromophenylphenyl ether ug/L 34.850 70 34-113
4-Chloro-3-methylphenol ug/L 73.8100 74 31-110
4-Chloroaniline ug/L 87.8100 88 20-120
4-Chlorophenylphenyl ether ug/L 41.750 83 34-116
4-Nitroaniline ug/L 111100 111 46-128
4-Nitrophenol ug/L 79.5250 32 11-120
5-Nitro-o-toluidine ug/L 45.650 91 78-160
7,12-Dimethylbenz(a)anthracene ug/L 46.050 92 47-124
Acenaphthene ug/L 47.250 94 48-114
Acenaphthylene ug/L 48.650 97 48-112
Acetophenone ug/L 42.450 85 24-120
Anthracene ug/L 43.250 86 57-118
Benzo(a)anthracene ug/L 42.850 86 56-121
Benzo(a)pyrene ug/L 45.950 92 55-127
Benzo(b)fluoranthene ug/L 48.850 98 53-128
Benzo(g,h,i)perylene ug/L 39.650 79 54-125
Benzo(k)fluoranthene ug/L 46.150 92 51-123
Benzyl alcohol ug/L 77.8100 78 27-120
bis(2-Chloroethoxy)methane ug/L 33.250 66 32-120
bis(2-Chloroethyl) ether ug/L 34.250 68 33-111
bis(2-Ethylhexyl)phthalate ug/L 43.050 86 50-145
Butylbenzylphthalate ug/L 45.050 90 54-138
Chlorobenzilate ug/L 42.850 86 65-132
Chrysene ug/L 42.650 85 58-127
Di-n-butylphthalate ug/L 46.050 92 56-125
Di-n-octylphthalate ug/L 41.150 82 50-134
Diallate ug/L 33.150 66 47-123
Dibenz(a,h)anthracene ug/L 43.750 87 53-129
Dibenzofuran ug/L 48.350 97 45-120
Diethylphthalate ug/L 46.7J50 93 53-120
Dimethoate ug/L 39.750 79 57-139
Dimethylphthalate ug/L 48.650 97 55-116
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 180 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2018679LABORATORY CONTROL SAMPLE:
LCSSpike
Diphenylamine ug/L 44.950 90 42-120
Disulfoton ug/L 33.350 67 49-156
Ethyl methanesulfonate ug/L 31.050 62 43-120
Famphur ug/L 107100 107 40-160
Fluoranthene ug/L 44.450 89 57-125
Fluorene ug/L 46.550 93 53-118
Hexachlorobenzene ug/L 39.850 80 49-116
Hexachlorocyclopentadiene ug/L 35.450 71 26-158
Hexachloroethane ug/L 25.850 52 30-114
Hexachloropropene ug/L 24.150 48 13-137
Indeno(1,2,3-cd)pyrene ug/L 42.150 84 55-128
Isodrin ug/L 40.050 80 68-129
Isophorone ug/L 36.550 73 31-118
Isosafrole ug/L 40.950 82 48-107
Kepone ug/L 65.8100 66 10-124
Methapyrilene ug/L 21.0J50 42 40-160
Methyl methanesulfonate ug/L 46.350 93 25-114
Methyl parathion ug/L 42.950 86 58-137
N-Nitroso-di-n-butylamine ug/L 35.450 71 36-115
N-Nitroso-di-n-propylamine ug/L 43.850 88 32-119
N-Nitrosodiethylamine ug/L 34.650 69 47-115
N-Nitrosodimethylamine ug/L 23.150 46 13-120
N-Nitrosodiphenylamine ug/L 44.950 90 43-120
N-Nitrosomethylethylamine ug/L 28.050 56 39-120
N-Nitrosopiperidine ug/L 41.650 83 43-113
N-Nitrosopyrrolidine ug/L 41.750 83 32-110
Nitrobenzene ug/L 31.550 63 33-110
O,O,O-Triethylphosphorothioate ug/L 38.150 76 51-127
O-Toluidine ug/L 32.150 64 27-120
P-Dimethylaminoazobenzene ug/L 17.3100 17 10-120
p-Phenylenediamine ug/L 37.650 75 72-143
Parathion (Ethyl parathion)ug/L 35.450 71 56-140
Pentachlorobenzene ug/L 42.950 86 30-137
Pentachloronitrobenzene ug/L 44.150 88 70-124
Pentachlorophenol ug/L 97.2250 39 10-137
Phenacetin ug/L 37.050 74 60-130
Phenanthrene ug/L 43.150 86 57-117
Phenol ug/L 18.950 38 10-120
Phorate ug/L 32.650 65 55-126
Pronamide ug/L 40.450 81 75-124
Pyrene ug/L 45.350 91 55-122
Safrole ug/L 41.450 83 41-120
Thionazin ug/L 35.250 70 63-137
2,4,6-Tribromophenol (S)%90 27-110
2-Fluorobiphenyl (S)%90 27-110
2-Fluorophenol (S)%46 12-110
Nitrobenzene-d5 (S)%67 21-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 181 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2018679LABORATORY CONTROL SAMPLE:
LCSSpike
Phenol-d6 (S)%34 10-110
Terphenyl-d14 (S)%91 31-107
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2022108MATRIX SPIKE SAMPLE:
MSSpike
Result
92342530002
1,2,4,5-Tetrachlorobenzene ug/L 37.750 75 50-150ND
1,3,5-Trinitrobenzene ug/L 33.650 67 50-150ND
1,3-Dinitrobenzene ug/L 41.450 83 50-150ND
1,4-Naphthoquinone ug/L 44.850 90 50-150ND
1-Naphthalenamine ug/L 14.2 M1502850-150ND
2,2'-Oxybis(1-chloropropane)ug/L 52.050 104 50-150ND
2,3,4,6-Tetrachlorophenol ug/L 85.5 M15017150-150ND
2,4,5-Trichlorophenol ug/L 44.750 89 19-105ND
2,4,6-Trichlorophenol ug/L 52.450 105 13-108ND
2,4-Dichlorophenol ug/L 39.550 79 29-111ND
2,4-Dimethylphenol ug/L 36.250 72 21-103ND
2,4-Dinitrophenol ug/L 207250 83 10-109ND
2,4-Dinitrotoluene ug/L 46.750 93 27-104ND
2,6-Dichlorophenol ug/L 40.550 81 50-150ND
2,6-Dinitrotoluene ug/L 48.550 97 28-101ND
2-Acetylaminofluorene ug/L 36.850 73 50-150ND
2-Chloronaphthalene ug/L 58.1 M15011614-102ND
2-Chlorophenol ug/L 36.350 73 16-110ND
2-Methylnaphthalene ug/L 36.850 74 13-110ND
2-Methylphenol(o-Cresol)ug/L 29.750 59 19-110ND
2-Naphthalenamine ug/L 11.5 M1502350-150ND
2-Nitroaniline ug/L 95.3100 95 26-103ND
2-Nitrophenol ug/L 36.550 73 20-110ND
3&4-Methylphenol(m&p Cresol)ug/L 25.550 51 20-110ND
3,3'-Dichlorobenzidine ug/L 78.3250 31 25-112ND
3,3'-Dimethylbenzidine ug/L 20.1 M11002050-150ND
3-Methylcholanthrene ug/L 44.550 89 50-150ND
3-Nitroaniline ug/L 104100 104 29-110ND
4,6-Dinitro-2-methylphenol ug/L 73.6100 74 10-117ND
4-Aminobiphenyl ug/L 21.2 M1504250-150ND
4-Bromophenylphenyl ether ug/L 35.350 71 20-105ND
4-Chloro-3-methylphenol ug/L 69.2100 69 22-110ND
4-Chloroaniline ug/L 59.4100 59 20-100ND
4-Chlorophenylphenyl ether ug/L 45.050 90 19-102ND
4-Nitroaniline ug/L 112 M110011229-110ND
4-Nitrophenol ug/L 78.0250 31 10-110ND
5-Nitro-o-toluidine ug/L 46.350 93 50-150ND
7,12-Dimethylbenz(a)anthracene ug/L 46.550 93 50-150ND
Acenaphthene ug/L 50.250 100 17-100ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 182 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2022108MATRIX SPIKE SAMPLE:
MSSpike
Result
92342530002
Acenaphthylene ug/L 51.2 M15010221-100ND
Acetophenone ug/L 36.550 73 50-150ND
Anthracene ug/L 44.450 89 24-109ND
Benzo(a)anthracene ug/L 41.650 83 22-117ND
Benzo(a)pyrene ug/L 44.750 89 23-104ND
Benzo(b)fluoranthene ug/L 48.950 98 23-103ND
Benzo(g,h,i)perylene ug/L 40.550 81 18-111ND
Benzo(k)fluoranthene ug/L 45.150 90 22-113ND
Benzyl alcohol ug/L 63.0100 63 19-101ND
bis(2-Chloroethoxy)methane ug/L 31.850 64 22-110ND
bis(2-Chloroethyl) ether ug/L 33.150 66 16-110ND
bis(2-Ethylhexyl)phthalate ug/L 44.850 90 23-102ND
Butylbenzylphthalate ug/L 45.650 91 25-110ND
Chlorobenzilate ug/L 42.750 85 50-150ND
Chrysene ug/L 42.250 84 23-115ND
Di-n-butylphthalate ug/L 48.350 97 26-110ND
Di-n-octylphthalate ug/L 41.550 83 22-110ND
Diallate ug/L 35.250 70 50-150ND
Dibenz(a,h)anthracene ug/L 42.050 84 21-112ND
Dibenzofuran ug/L 51.250 102 19-102ND
Diethylphthalate ug/L 50.2J50 100 29-110ND
Dimethoate ug/L 42.950 86 50-150ND
Dimethylphthalate ug/L 51.550 103 27-110ND
Diphenylamine ug/L 45.850 92 50-150ND
Disulfoton ug/L 35.450 71 50-150ND
Ethyl methanesulfonate ug/L 27.450 55 50-150ND
Famphur ug/L 130100 130 50-150ND
Fluoranthene ug/L 45.850 92 23-112ND
Fluorene ug/L 49.150 98 22-104ND
Hexachlorobenzene ug/L 40.050 80 21-116ND
Hexachlorocyclopentadiene ug/L 35.950 72 10-110ND
Hexachloroethane ug/L 27.250 54 10-110ND
Hexachloropropene ug/L 25.550 51 50-150ND
Indeno(1,2,3-cd)pyrene ug/L 42.450 85 20-113ND
Isodrin ug/L 42.350 85 50-150ND
Isophorone ug/L 35.650 71 50-150ND
Isosafrole ug/L 43.650 87 50-150ND
Kepone ug/L 72.4100 72 50-150ND
Methapyrilene ug/L 33.3J50 67 50-150ND
Methyl methanesulfonate ug/L 42.550 85 50-150ND
Methyl parathion ug/L 42.950 86 50-150ND
N-Nitroso-di-n-butylamine ug/L 32.350 65 50-150ND
N-Nitroso-di-n-propylamine ug/L 37.250 74 21-105ND
N-Nitrosodiethylamine ug/L 28.750 57 50-150ND
N-Nitrosodimethylamine ug/L 20.750 41 10-110ND
N-Nitrosodiphenylamine ug/L 45.850 92 23-107ND
N-Nitrosomethylethylamine ug/L 23.7 M1504750-150ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 183 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2022108MATRIX SPIKE SAMPLE:
MSSpike
Result
92342530002
N-Nitrosopiperidine ug/L 37.250 74 50-150ND
N-Nitrosopyrrolidine ug/L 28.650 57 50-150ND
Nitrobenzene ug/L 30.450 61 20-110ND
O,O,O-Triethylphosphorothioate ug/L 36.850 74 50-150ND
O-Toluidine ug/L 20.6 M1504150-150ND
P-Dimethylaminoazobenzene ug/L 16.8 M11001750-150ND
p-Phenylenediamine ug/L 35.250 70 50-150ND
Parathion (Ethyl parathion)ug/L 36.650 73 50-150ND
Pentachlorobenzene ug/L 44.750 89 50-150ND
Pentachloronitrobenzene ug/L 44.850 90 50-150ND
Pentachlorophenol ug/L 88.9250 36 10-118ND
Phenacetin ug/L 37.150 74 50-150ND
Phenanthrene ug/L 44.850 90 24-106ND
Phenol ug/L 15.350 31 12-110ND
Phorate ug/L 33.650 67 50-150ND
Pronamide ug/L 41.650 83 50-150ND
Pyrene ug/L 45.050 90 24-114ND
Safrole ug/L 38.450 77 50-150ND
Thionazin ug/L 38.050 76 50-150ND
2,4,6-Tribromophenol (S)%87 27-110
2-Fluorobiphenyl (S)%95 27-110
2-Fluorophenol (S)%39 12-110
Nitrobenzene-d5 (S)%62 21-110
Phenol-d6 (S)%27 10-110
Terphenyl-d14 (S)%74 31-107
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342530004
2018681SAMPLE DUPLICATE:
1,2,4,5-Tetrachlorobenzene ug/L ND 30ND
1,3,5-Trinitrobenzene ug/L ND 30ND
1,3-Dinitrobenzene ug/L ND 30ND
1,4-Naphthoquinone ug/L ND 30ND
1-Naphthalenamine ug/L ND 30ND
2,2'-Oxybis(1-chloropropane)ug/L ND 30ND
2,3,4,6-Tetrachlorophenol ug/L ND 30ND
2,4,5-Trichlorophenol ug/L ND 30ND
2,4,6-Trichlorophenol ug/L ND 30ND
2,4-Dichlorophenol ug/L ND 30ND
2,4-Dimethylphenol ug/L ND 30ND
2,4-Dinitrophenol ug/L ND 30ND
2,4-Dinitrotoluene ug/L ND 30ND
2,6-Dichlorophenol ug/L ND 30ND
2,6-Dinitrotoluene ug/L ND 30ND
2-Acetylaminofluorene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 184 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342530004
2018681SAMPLE DUPLICATE:
2-Chloronaphthalene ug/L ND 30ND
2-Chlorophenol ug/L ND 30ND
2-Methylnaphthalene ug/L ND 30ND
2-Methylphenol(o-Cresol)ug/L ND 30ND
2-Naphthalenamine ug/L ND 30ND
2-Nitroaniline ug/L ND 30ND
2-Nitrophenol ug/L ND 30ND
3&4-Methylphenol(m&p Cresol)ug/L ND 30ND
3,3'-Dichlorobenzidine ug/L ND 30ND
3,3'-Dimethylbenzidine ug/L ND 30ND
3-Methylcholanthrene ug/L ND 30ND
3-Nitroaniline ug/L ND 30ND
4,6-Dinitro-2-methylphenol ug/L ND 30ND
4-Aminobiphenyl ug/L ND 30ND
4-Bromophenylphenyl ether ug/L ND 30ND
4-Chloro-3-methylphenol ug/L ND 30ND
4-Chloroaniline ug/L ND 30ND
4-Chlorophenylphenyl ether ug/L ND 30ND
4-Nitroaniline ug/L ND 30ND
4-Nitrophenol ug/L ND 30ND
5-Nitro-o-toluidine ug/L NDND
7,12-Dimethylbenz(a)anthracene ug/L ND 30ND
Acenaphthene ug/L ND 30ND
Acenaphthylene ug/L ND 30ND
Acetophenone ug/L ND 30ND
Anthracene ug/L ND 30ND
Benzo(a)anthracene ug/L ND 30ND
Benzo(a)pyrene ug/L ND 30ND
Benzo(b)fluoranthene ug/L ND 30ND
Benzo(g,h,i)perylene ug/L ND 30ND
Benzo(k)fluoranthene ug/L ND 30ND
Benzyl alcohol ug/L ND 30ND
bis(2-Chloroethoxy)methane ug/L ND 30ND
bis(2-Chloroethyl) ether ug/L ND 30ND
bis(2-Ethylhexyl)phthalate ug/L ND 30ND
Butylbenzylphthalate ug/L ND 30ND
Chlorobenzilate ug/L ND 30ND
Chrysene ug/L ND 30ND
Di-n-butylphthalate ug/L ND 30ND
Di-n-octylphthalate ug/L ND 30ND
Diallate ug/L ND 30ND
Dibenz(a,h)anthracene ug/L ND 30ND
Dibenzofuran ug/L ND 30ND
Diethylphthalate ug/L ND 30ND
Dimethoate ug/L ND 30ND
Dimethylphthalate ug/L ND 30ND
Diphenylamine ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 185 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342530004
2018681SAMPLE DUPLICATE:
Disulfoton ug/L ND 30ND
Ethyl methanesulfonate ug/L ND 30ND
Famphur ug/L ND 30ND
Fluoranthene ug/L ND 30ND
Fluorene ug/L ND 30ND
Hexachlorobenzene ug/L ND 30ND
Hexachlorocyclopentadiene ug/L ND 30ND
Hexachloroethane ug/L ND 30ND
Hexachloropropene ug/L ND 30ND
Indeno(1,2,3-cd)pyrene ug/L ND 30ND
Isodrin ug/L ND 30ND
Isophorone ug/L ND 30ND
Isosafrole ug/L ND 30ND
Kepone ug/L ND 30ND
Methapyrilene ug/L ND 30ND
Methyl methanesulfonate ug/L ND 30ND
Methyl parathion ug/L ND 30ND
N-Nitroso-di-n-butylamine ug/L ND 30ND
N-Nitroso-di-n-propylamine ug/L ND 30ND
N-Nitrosodiethylamine ug/L ND 30ND
N-Nitrosodimethylamine ug/L ND 30ND
N-Nitrosodiphenylamine ug/L ND 30ND
N-Nitrosomethylethylamine ug/L ND 30ND
N-Nitrosopiperidine ug/L ND 30ND
N-Nitrosopyrrolidine ug/L ND 30ND
Nitrobenzene ug/L ND 30ND
O,O,O-Triethylphosphorothioate ug/L ND 30ND
O-Toluidine ug/L ND 30ND
P-Dimethylaminoazobenzene ug/L ND 30ND
p-Phenylenediamine ug/L ND 30ND
Parathion (Ethyl parathion)ug/L ND 30ND
Pentachlorobenzene ug/L ND 30ND
Pentachloronitrobenzene ug/L ND 30ND
Pentachlorophenol ug/L ND 30ND
Phenacetin ug/L ND 30ND
Phenanthrene ug/L ND 30ND
Phenol ug/L ND 30ND
Phorate ug/L ND 30ND
Pronamide ug/L ND 30ND
Pyrene ug/L ND 30ND
Safrole ug/L ND 30ND
Thionazin ug/L ND 30ND
2,4,6-Tribromophenol (S)%88 2371
2-Fluorobiphenyl (S)%88 2370
2-Fluorophenol (S)%40 2332
Nitrobenzene-d5 (S)%69 2057
Phenol-d6 (S)%27 2820
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 186 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342530004
2018681SAMPLE DUPLICATE:
Terphenyl-d14 (S)%60 2476
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 187 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
364808
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92342479009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2022377
Associated Lab Samples:92342479009
Matrix:Water
AnalyzedMDL
1,2,4,5-Tetrachlorobenzene ug/L ND 10.0 06/15/17 10:331.3
1,3,5-Trinitrobenzene ug/L ND 10.0 06/15/17 10:331.2
1,3-Dinitrobenzene ug/L ND 20.0 06/15/17 10:331.3
1,4-Naphthoquinone ug/L ND 10.0 06/15/17 10:330.99
1-Naphthalenamine ug/L ND 10.0 06/15/17 10:331.3
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 06/15/17 10:331.8
2,3,4,6-Tetrachlorophenol ug/L ND 10.0 06/15/17 10:332.9
2,4,5-Trichlorophenol ug/L ND 10.0 06/15/17 10:331.5
2,4,6-Trichlorophenol ug/L ND 10.0 06/15/17 10:331.4
2,4-Dichlorophenol ug/L ND 10.0 06/15/17 10:331.6
2,4-Dimethylphenol ug/L ND 10.0 06/15/17 10:331.6
2,4-Dinitrophenol ug/L ND 50.0 06/15/17 10:335.1
2,4-Dinitrotoluene ug/L ND 10.0 06/15/17 10:331.5
2,6-Dichlorophenol ug/L ND 10.0 06/15/17 10:331.5
2,6-Dinitrotoluene ug/L ND 10.0 06/15/17 10:331.4
2-Acetylaminofluorene ug/L ND 20.0 06/15/17 10:331.6
2-Chloronaphthalene ug/L ND 10.0 06/15/17 10:331.6
2-Chlorophenol ug/L ND 10.0 06/15/17 10:331.5
2-Methylnaphthalene ug/L ND 10.0 06/15/17 10:331.4
2-Methylphenol(o-Cresol)ug/L ND 10.0 06/15/17 10:331.6
2-Naphthalenamine ug/L ND 10.0 06/15/17 10:332.2
2-Nitroaniline ug/L ND 50.0 06/15/17 10:332.3
2-Nitrophenol ug/L ND 10.0 06/15/17 10:331.6
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 06/15/17 10:331.4
3,3'-Dichlorobenzidine ug/L ND 20.0 06/15/17 10:333.9
3,3'-Dimethylbenzidine ug/L ND 10.0 06/15/17 10:333.9
3-Methylcholanthrene ug/L ND 10.0 06/15/17 10:332.7
3-Nitroaniline ug/L ND 50.0 06/15/17 10:332.7
4,6-Dinitro-2-methylphenol ug/L ND 50.0 06/15/17 10:332.2
4-Aminobiphenyl ug/L ND 20.0 06/15/17 10:331.7
4-Bromophenylphenyl ether ug/L ND 10.0 06/15/17 10:331.5
4-Chloro-3-methylphenol ug/L ND 20.0 06/15/17 10:332.8
4-Chloroaniline ug/L ND 20.0 06/15/17 10:332.8
4-Chlorophenylphenyl ether ug/L ND 10.0 06/15/17 10:331.6
4-Nitroaniline ug/L ND 20.0 06/15/17 10:333.4
4-Nitrophenol ug/L ND 50.0 06/15/17 10:334.3
5-Nitro-o-toluidine ug/L ND 10.0 06/15/17 10:331.9
7,12-Dimethylbenz(a)anthracene ug/L ND 10.0 06/15/17 10:332.4
Acenaphthene ug/L ND 10.0 06/15/17 10:331.6
Acenaphthylene ug/L ND 10.0 06/15/17 10:331.5
Acetophenone ug/L ND 10.0 06/15/17 10:331.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 188 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2022377
Associated Lab Samples:92342479009
Matrix:Water
AnalyzedMDL
Anthracene ug/L ND 10.0 06/15/17 10:331.7
Benzo(a)anthracene ug/L ND 10.0 06/15/17 10:332.1
Benzo(a)pyrene ug/L ND 10.0 06/15/17 10:332.2
Benzo(b)fluoranthene ug/L ND 10.0 06/15/17 10:332.2
Benzo(g,h,i)perylene ug/L ND 10.0 06/15/17 10:332.1
Benzo(k)fluoranthene ug/L ND 10.0 06/15/17 10:332.0
Benzyl alcohol ug/L ND 20.0 06/15/17 10:333.1
bis(2-Chloroethoxy)methane ug/L ND 10.0 06/15/17 10:331.6
bis(2-Chloroethyl) ether ug/L ND 10.0 06/15/17 10:331.7
bis(2-Ethylhexyl)phthalate ug/L ND 15.0 06/15/17 10:332.3
Butylbenzylphthalate ug/L ND 10.0 06/15/17 10:332.5
Chlorobenzilate ug/L ND 10.0 06/15/17 10:332.2
Chrysene ug/L ND 10.0 06/15/17 10:332.1
Di-n-butylphthalate ug/L ND 10.0 06/15/17 10:332.0
Di-n-octylphthalate ug/L ND 10.0 06/15/17 10:331.5
Diallate ug/L ND 10.0 06/15/17 10:331.6
Dibenz(a,h)anthracene ug/L ND 10.0 06/15/17 10:332.0
Dibenzofuran ug/L ND 10.0 06/15/17 10:331.7
Diethylphthalate ug/L ND 6000 06/15/17 10:331.6
Dimethoate ug/L ND 20.0 06/15/17 10:331.8
Dimethylphthalate ug/L ND 10.0 06/15/17 10:331.4
Diphenylamine ug/L ND 10.0 06/15/17 10:331.4
Disulfoton ug/L ND 10.0 06/15/17 10:331.5
Ethyl methanesulfonate ug/L ND 20.0 06/15/17 10:331.6
Famphur ug/L ND 20.0 06/15/17 10:335.7
Fluoranthene ug/L ND 10.0 06/15/17 10:332.2
Fluorene ug/L ND 10.0 06/15/17 10:331.6
Hexachlorobenzene ug/L ND 10.0 06/15/17 10:331.7
Hexachlorocyclopentadiene ug/L ND 10.0 06/15/17 10:331.3
Hexachloroethane ug/L ND 10.0 06/15/17 10:331.8
Hexachloropropene ug/L ND 10.0 06/15/17 10:331.2
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 06/15/17 10:332.0
Isodrin ug/L ND 20.0 06/15/17 10:332.5
Isophorone ug/L ND 10.0 06/15/17 10:331.5
Isosafrole ug/L ND 10.0 06/15/17 10:331.5
Kepone ug/L ND 20.0 06/15/17 10:334.5
Methapyrilene ug/L ND 100 06/15/17 10:333.0
Methyl methanesulfonate ug/L ND 10.0 06/15/17 10:331.1
Methyl parathion ug/L ND 10.0 06/15/17 10:331.6
N-Nitroso-di-n-butylamine ug/L ND 10.0 06/15/17 10:331.6
N-Nitroso-di-n-propylamine ug/L ND 10.0 06/15/17 10:331.7
N-Nitrosodiethylamine ug/L ND 20.0 06/15/17 10:331.4
N-Nitrosodimethylamine ug/L ND 10.0 06/15/17 10:331.6
N-Nitrosodiphenylamine ug/L ND 10.0 06/15/17 10:331.4
N-Nitrosomethylethylamine ug/L ND 10.0 06/15/17 10:331.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 189 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2022377
Associated Lab Samples:92342479009
Matrix:Water
AnalyzedMDL
N-Nitrosopiperidine ug/L ND 20.0 06/15/17 10:331.7
N-Nitrosopyrrolidine ug/L ND 10.0 06/15/17 10:331.7
Nitrobenzene ug/L ND 10.0 06/15/17 10:331.6
O,O,O-Triethylphosphorothioate ug/L ND 10.0 06/15/17 10:331.7
O-Toluidine ug/L ND 10.0 06/15/17 10:331.7
P-Dimethylaminoazobenzene ug/L ND 10.0 06/15/17 10:331.0
p-Phenylenediamine ug/L ND 10.0 06/15/17 10:332.2
Parathion (Ethyl parathion)ug/L ND 10.0 06/15/17 10:331.5
Pentachlorobenzene ug/L ND 10.0 06/15/17 10:331.5
Pentachloronitrobenzene ug/L ND 20.0 06/15/17 10:331.7
Pentachlorophenol ug/L ND 25.0 06/15/17 10:333.5
Phenacetin ug/L ND 20.0 06/15/17 10:331.9
Phenanthrene ug/L ND 10.0 06/15/17 10:331.6
Phenol ug/L ND 10.0 06/15/17 10:331.3
Phorate ug/L ND 10.0 06/15/17 10:331.7
Pronamide ug/L ND 10.0 06/15/17 10:332.0
Pyrene ug/L ND 10.0 06/15/17 10:332.2
Safrole ug/L ND 10.0 06/15/17 10:331.3
Thionazin ug/L ND 20.0 06/15/17 10:331.7
2,4,6-Tribromophenol (S)%89 27-110 06/15/17 10:33
2-Fluorobiphenyl (S)%94 27-110 06/15/17 10:33
2-Fluorophenol (S)%48 12-110 06/15/17 10:33
Nitrobenzene-d5 (S)%84 21-110 06/15/17 10:33
Phenol-d6 (S)%31 10-110 06/15/17 10:33
Terphenyl-d14 (S)%108 31-107 S306/15/17 10:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2022378LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2022379
1,2,4,5-Tetrachlorobenzene ug/L 31.550 63 16-1296532.4 3 30
1,3,5-Trinitrobenzene ug/L 34.050 68 55-1256733.7 1 30
1,3-Dinitrobenzene ug/L 41.650 83 30-1228542.5 2 30
1,4-Naphthoquinone ug/L 42.050 84 31-1208542.5 1 30
1-Naphthalenamine ug/L 27.850 56 37-1265226.1 6 30
2,2'-Oxybis(1-chloropropane)ug/L 57.850 116 18-12011457.2 1 30
2,3,4,6-Tetrachlorophenol ug/L 81.450 163 54-27616783.6 3 30
2,4,5-Trichlorophenol ug/L 41.550 83 43-1138542.7 3 30
2,4,6-Trichlorophenol ug/L 49.850 100 42-12010050.0 0 30
2,4-Dichlorophenol ug/L 41.650 83 30-1207939.4 5 30
2,4-Dimethylphenol ug/L 38.950 78 29-1117235.8 8 30
2,4-Dinitrophenol ug/L 245250 98 19-132101253 3 30
2,4-Dinitrotoluene ug/L 45.750 91 58-1289346.3 1 30
2,6-Dichlorophenol ug/L 42.350 85 54-1288039.9 6 30
2,6-Dinitrotoluene ug/L 47.550 95 54-1299647.8 0 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 190 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2022378LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2022379
2-Acetylaminofluorene ug/L 37.3 L2507581-1607336.5 2 30
2-Chloronaphthalene ug/L 52.650 105 43-11710753.3 1 30
2-Chlorophenol ug/L 40.550 81 37-1208140.4 0 30
2-Methylnaphthalene ug/L 38.150 76 33-1207236.0 6 30
2-Methylphenol(o-Cresol)ug/L 34.050 68 31-1206733.7 1 30
2-Naphthalenamine ug/L 31.850 64 41-1366331.6 1 30
2-Nitroaniline ug/L 94.2100 94 48-1219292.2 2 30
2-Nitrophenol ug/L 39.850 80 25-1167638.0 5 30
3&4-Methylphenol(m&p Cresol)ug/L 28.550 57 23-1205828.9 1 30
3,3'-Dichlorobenzidine ug/L 88.2250 35 10-1543486.0 2 30
3,3'-Dimethylbenzidine ug/L 46.2 R11004610-1572727.4 51 30
3-Methylcholanthrene ug/L 44.750 89 65-1308743.7 2 30
3-Nitroaniline ug/L 108100 108 43-115107107 1 30
4,6-Dinitro-2-methylphenol ug/L 86.1100 86 44-1248686.0 0 30
4-Aminobiphenyl ug/L 28.450 57 21-1255426.9 5 30
4-Bromophenylphenyl ether ug/L 34.950 70 34-1136834.2 2 30
4-Chloro-3-methylphenol ug/L 73.7100 74 31-1106968.6 7 30
4-Chloroaniline ug/L 87.5100 87 20-1208180.8 8 30
4-Chlorophenylphenyl ether ug/L 43.850 88 34-1168743.5 1 30
4-Nitroaniline ug/L 117100 117 46-128112112 4 30
4-Nitrophenol ug/L 85.8250 34 11-1203383.1 3 30
5-Nitro-o-toluidine ug/L 46.150 92 78-1609245.8 1 30
7,12-Dimethylbenz(a)anthracene ug/L 46.050 92 47-1249145.6 1 30
Acenaphthene ug/L 48.150 96 48-1149648.1 0 30
Acenaphthylene ug/L 48.950 98 48-1129849.1 0 30
Acetophenone ug/L 41.950 84 24-1208140.7 3 30
Anthracene ug/L 44.150 88 57-1188743.5 2 30
Benzo(a)anthracene ug/L 42.650 85 56-1218542.3 1 30
Benzo(a)pyrene ug/L 45.350 91 55-1279044.8 1 30
Benzo(b)fluoranthene ug/L 48.450 97 53-1289748.5 0 30
Benzo(g,h,i)perylene ug/L 41.350 83 54-1258140.4 2 30
Benzo(k)fluoranthene ug/L 47.550 95 51-1239246.0 3 30
Benzyl alcohol ug/L 74.4100 74 27-1207372.9 2 30
bis(2-Chloroethoxy)methane ug/L 34.550 69 32-1206432.2 7 30
bis(2-Chloroethyl) ether ug/L 35.850 72 33-1117637.8 5 30
bis(2-Ethylhexyl)phthalate ug/L 44.150 88 50-1458643.2 2 30
Butylbenzylphthalate ug/L 45.350 91 54-1388944.4 2 30
Chlorobenzilate ug/L 41.050 82 65-1328241.1 0 30
Chrysene ug/L 43.150 86 58-1278442.0 3 30
Di-n-butylphthalate ug/L 48.850 98 56-1259647.9 2 30
Di-n-octylphthalate ug/L 41.550 83 50-1348240.8 2 30
Diallate ug/L 34.050 68 47-1236834.0 0 30
Dibenz(a,h)anthracene ug/L 44.150 88 53-1298643.1 2 30
Dibenzofuran ug/L 49.650 99 45-12010050.1 1 30
Diethylphthalate ug/L 49.2J50 98 53-1209949.7J 1 30
Dimethoate ug/L 43.150 86 57-1398542.4 2 30
Dimethylphthalate ug/L 50.350 101 55-11610150.6 1 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 191 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2022378LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2022379
Diphenylamine ug/L 44.850 90 42-1208944.4 1 30
Disulfoton ug/L 33.650 67 49-1566733.3 1 30
Ethyl methanesulfonate ug/L 31.250 62 43-1206230.8 1 30
Famphur ug/L 125 L110012540-160161161 25 30
Fluoranthene ug/L 47.850 96 57-1259145.6 5 30
Fluorene ug/L 47.950 96 53-1189748.4 1 30
Hexachlorobenzene ug/L 39.550 79 49-1167738.4 3 30
Hexachlorocyclopentadiene ug/L 34.950 70 26-1587436.8 5 30
Hexachloroethane ug/L 25.250 50 30-1145025.2 0 30
Hexachloropropene ug/L 20.050 40 13-1373919.5 2 30
Indeno(1,2,3-cd)pyrene ug/L 42.750 85 55-1288542.6 0 30
Isodrin ug/L 43.350 87 68-1298542.5 2 30
Isophorone ug/L 38.650 77 31-1187135.7 8 30
Isosafrole ug/L 40.050 80 48-1078341.6 4 30
Kepone ug/L 106 L110010610-124127127 18 30
Methapyrilene ug/L ND L250340-1603517.5J 30
Methyl methanesulfonate ug/L 47.850 96 25-1149346.7 2 30
Methyl parathion ug/L 46.450 93 58-1378944.5 4 30
N-Nitroso-di-n-butylamine ug/L 35.550 71 36-1156532.4 9 30
N-Nitroso-di-n-propylamine ug/L 44.250 88 32-1198341.6 6 30
N-Nitrosodiethylamine ug/L 33.350 67 47-1156432.0 4 30
N-Nitrosodimethylamine ug/L 24.250 48 13-1204823.9 1 30
N-Nitrosodiphenylamine ug/L 44.850 90 43-1208944.4 1 30
N-Nitrosomethylethylamine ug/L 27.650 55 39-1205527.3 1 30
N-Nitrosopiperidine ug/L 40.250 80 43-1137437.2 8 30
N-Nitrosopyrrolidine ug/L 35.850 72 32-1106532.3 10 30
Nitrobenzene ug/L 32.650 65 33-1106231.1 5 30
O,O,O-Triethylphosphorothioate ug/L 38.850 78 51-1277436.9 5 30
O-Toluidine ug/L 30.950 62 27-1205929.5 5 30
P-Dimethylaminoazobenzene ug/L 16.3100 16 10-1201716.6 2 30
p-Phenylenediamine ug/L 38.750 77 72-1437537.6 3 30
Parathion (Ethyl parathion)ug/L 37.050 74 56-1407336.7 1 30
Pentachlorobenzene ug/L 41.250 82 30-1378341.6 1 30
Pentachloronitrobenzene ug/L 44.950 90 70-1249045.2 1 30
Pentachlorophenol ug/L 94.1250 38 10-1373791.8 2 30
Phenacetin ug/L 38.250 76 60-1307638.0 1 30
Phenanthrene ug/L 44.450 89 57-1178642.9 3 30
Phenol ug/L 18.950 38 10-1203618.0 5 30
Phorate ug/L 34.050 68 55-1266733.7 1 30
Pronamide ug/L 41.850 84 75-1248140.5 3 30
Pyrene ug/L 44.050 88 55-1228542.7 3 30
Safrole ug/L 39.550 79 41-1207838.9 2 30
Thionazin ug/L 37.350 75 63-1377537.4 0 30
2,4,6-Tribromophenol (S)%84 27-11086
2-Fluorobiphenyl (S)%90 27-11092
2-Fluorophenol (S)%46 12-11047
Nitrobenzene-d5 (S)%69 21-11065
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 192 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2022378LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2022379
Phenol-d6 (S)%32 10-11034
Terphenyl-d14 (S)%100 31-107100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 193 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363078
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92342337001, 92342479001, 92342479002, 92342479003, 92342479004, 92342479005, 92342479006,
92342479007, 92342479009, 92342479010, 92342479011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2013020
Associated Lab Samples:92342337001, 92342479001, 92342479002, 92342479003, 92342479004, 92342479005, 92342479006,
92342479007, 92342479009, 92342479010, 92342479011
Matrix:Water
AnalyzedMDL
Sulfide ug/L ND 1000 06/01/17 21:00100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2013021LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 464J500 93 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2013022MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342281005
2013023
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 99 80-120102 3 10500ND501J516J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2013024MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342337001
2013025
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 100 80-120104 4 10500ND509J532J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 194 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363079
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92342479013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2013030
Associated Lab Samples:92342479013
Matrix:Water
AnalyzedMDL
Sulfide ug/L ND 1000 06/07/17 22:30100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2013031LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 516J500 103 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2013032MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342297004
2013033
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 88 80-12094 7 10500ND454J485J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2013034MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342297005
2013035
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 82 80-12080 1 10500ND422J416J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 195 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363621
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92342479012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2015987
Associated Lab Samples:92342479012
Matrix:Water
AnalyzedMDL
Sulfide ug/L ND 1000 06/06/17 22:15100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2015988LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 464J500 93 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015989MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342281006
2015990
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L R15008780-120105 19 10500ND433J524J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015991MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342472017
2015992
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 85 80-12085 0 10500ND470J468J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 196 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363623
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92342529001, 92342529002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2016031
Associated Lab Samples:92342529001, 92342529002
Matrix:Water
AnalyzedMDL
Sulfide ug/L ND 1000 06/06/17 23:00100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2016032LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 470J500 94 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2016033MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342317011
2016034
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 91 80-12093 2 10500ND454J463J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2016035MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342530004
2016036
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L 500 82 80-12085 4 10500ND408J423J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 197 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
362936
SM 5210B
SM 5210B
5210B BOD, 5 day
Associated Lab Samples:92342339001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2012046
Associated Lab Samples:92342339001
Matrix:Water
AnalyzedMDL
BOD, 5 day ug/L ND 2000 06/06/17 01:132000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012047LABORATORY CONTROL SAMPLE:
LCSSpike
BOD, 5 day ug/L 179000198000 90 84.6-115.4
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342339001
2012048SAMPLE DUPLICATE:
BOD, 5 day ug/L 8400 B2,D6531014400
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 198 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363259
EPA 9040
EPA 9040
9040 pH
Associated Lab Samples:92342339001
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92341574001
2013995SAMPLE DUPLICATE:
pH Std. Units 6.0 H6195.9
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342339001
2013996SAMPLE DUPLICATE:
pH Std. Units 7.5 H6297.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 199 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363281
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92342339001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014072
Associated Lab Samples:92342339001
Matrix:Water
AnalyzedMDL
Sulfate ug/L ND 250000 06/03/17 13:42500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014073LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 52100J50000 104 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014074MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342339001
2014075
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L M1500005190-11054 3 105000018600J44100J45600J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014076MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342710001
2014077
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L M6,R150000-45 90-110155 15 1050000634 mg/L 611000J 711000J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 200 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
362937
EPA 353.2
EPA 353.2
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples:92342339001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2012049
Associated Lab Samples:92342339001
Matrix:Water
AnalyzedMDL
Nitrogen, Nitrate ug/L ND 20.0 06/01/17 03:2910.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012050LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate ug/L 24202500 97 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2012051MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342339001
2012052
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Nitrate ug/L M1250018090-110166 2 102500172002180021400
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2012053MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342318002
2012054
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Nitrate ug/L 2500 97 90-11097 0 102500ND24302430
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 201 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363097
EPA 365.1
EPA 365.1
365.1 Phosphorus, Total
Associated Lab Samples:92342339001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2013098
Associated Lab Samples:92342339001
Matrix:Water
AnalyzedMDL
Phosphorus ug/L ND 50.0 06/02/17 05:3025.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2013099LABORATORY CONTROL SAMPLE:
LCSSpike
Phosphorus ug/L 25502500 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2013100MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92341954001
2013101
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phosphorus ug/L 2500 100 90-110100 0 102500ND25302520
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2013102MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342159003
2013103
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phosphorus ug/L 2500 103 90-110103 0 1025001.8 mg/L 4380 4360
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 202 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
362991
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92342337001, 92342339001, 92342479001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2012281
Associated Lab Samples:92342337001, 92342339001, 92342479001
Matrix:Water
AnalyzedMDL
Cyanide ug/L ND 10.0 06/01/17 17:004.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012282LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 102100 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2012283MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342135005
2012284
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L M11005180-12055 2 101000.12 mg/L 168 172
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2012285MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342417001
2012286
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L M1100080-1200 4 101000.0093
mg/L 9.4J 9.7J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 203 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
362992
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92342479002, 92342479003, 92342479004, 92342479005, 92342479006, 92342479007, 92342479009,
92342479010, 92342479011, 92342479012, 92342479013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2012287
Associated Lab Samples:92342479002, 92342479003, 92342479004, 92342479005, 92342479006, 92342479007, 92342479009,
92342479010, 92342479011, 92342479012, 92342479013
Matrix:Water
AnalyzedMDL
Cyanide ug/L ND 10.0 06/01/17 17:524.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2012288LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 109100 109 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2012289MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342479002
2012290
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L 100 104 80-12096 8 101004.4J 109 100
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2012291MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342478003
2012292
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L 100 93 80-12099 6 101004.6J 97.4 103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 204 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363513
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92342529001, 92342529002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2015224
Associated Lab Samples:92342529001, 92342529002
Matrix:Water
AnalyzedMDL
Cyanide ug/L ND 10.0 06/07/17 13:524.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2015225LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 101100 101 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015226MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342317015
2015227
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L 100 94 80-12091 2 10100ND97.6 95.4
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015228MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342712006
2015229
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L M1,R11002980-12019 27 101000.013
mg/L 41.2 31.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 205 of 241
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363092
SM 5220D
SM 5220D
5220D COD
Associated Lab Samples:92342339001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2013088
Associated Lab Samples:92342339001
Matrix:Water
AnalyzedMDL
Chemical Oxygen Demand ug/L ND 25000 06/01/17 23:5512500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2013089LABORATORY CONTROL SAMPLE:
LCSSpike
Chemical Oxygen Demand ug/L 750000750000 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2013090MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92341190001
2013091
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L M17500004490-11042 0 37500006060 mg/L 6390000 6380000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2013092MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342276001
2013093
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L 750000 101 90-11099 1 375000068.0 mg/L 823000 813000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 206 of 241
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
Pace Analytical Services - Ormond BeachPASI-O
BATCH QUALIFIERS
Batch: 372970
A matrix spike/matrix spike duplicate was not performed for this batch due to insufficient sample volume.[M5]
ANALYTE QUALIFIERS
Sample re-extracted outside method hold time. Results of re-analysis confirmed original analysis performed within hold
time.1g
Oxygen usage is less than 2.0 for all dilutions set. The reported value is an estimated less than value and is calculated
for the dilution using the most amount of sample.B2
Common Laboratory Contaminant.C9
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
Analysis initiated outside of the 15 minute EPA required holding time.H6
The internal standard response was outside the laboratory acceptance limits confirmed by reanalysis. The results
reported are from the most QC compliant analysis.IO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 207 of 241
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
ANALYTE QUALIFIERS
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6
RPD value was outside control limits.R1
Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.S3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 208 of 241
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92342337001 363212 363809MW-8 EPA 3510 EPA 8081
92342479001 363163 363590MW-1 EPA 3510 EPA 8081
92342479002 363163 363590MW-2 EPA 3510 EPA 8081
92342479003 363163 363590MW-3R EPA 3510 EPA 8081
92342479004 363163 363590MW-4S EPA 3510 EPA 8081
92342479005 363163 363590MW-4D EPA 3510 EPA 8081
92342479006 363163 363590MW-5 EPA 3510 EPA 8081
92342479007 363163 363590MW-6R EPA 3510 EPA 8081
92342479009 363163 363590MW-9S EPA 3510 EPA 8081
92342479010 363163 363590MW-9D EPA 3510 EPA 8081
92342479011 363163 363590MW-10 EPA 3510 EPA 8081
92342479012 363163 363590MW-11S EPA 3510 EPA 8081
92342479013 363163 363590MW-11D EPA 3510 EPA 8081
92342529001 363212 363809MW-12 EPA 3510 EPA 8081
92342529002 363212 363809MW-13 EPA 3510 EPA 8081
92342337001 362866 363030MW-8 EPA 3510 EPA 8082
92342479001 363162 363349MW-1 EPA 3510 EPA 8082
92342479002 363162 363349MW-2 EPA 3510 EPA 8082
92342479003 363162 363349MW-3R EPA 3510 EPA 8082
92342479004 363162 363349MW-4S EPA 3510 EPA 8082
92342479005 363162 363349MW-4D EPA 3510 EPA 8082
92342479006 363162 363349MW-5 EPA 3510 EPA 8082
92342479007 363162 363349MW-6R EPA 3510 EPA 8082
92342479009 363162 363349MW-9S EPA 3510 EPA 8082
92342479010 363162 363349MW-9D EPA 3510 EPA 8082
92342479011 363162 363349MW-10 EPA 3510 EPA 8082
92342479012 363162 363349MW-11S EPA 3510 EPA 8082
92342479013 363162 363349MW-11D EPA 3510 EPA 8082
92342337001 372315 372970MW-8 EPA 8151 EPA 8151
92342479001 372862 373232MW-1 EPA 8151 EPA 8151
92342479002 372862 373232MW-2 EPA 8151 EPA 8151
92342479003 372862 373232MW-3R EPA 8151 EPA 8151
92342479004 372862 373232MW-4S EPA 8151 EPA 8151
92342479005 372862 373232MW-4D EPA 8151 EPA 8151
92342479006 372862 373232MW-5 EPA 8151 EPA 8151
92342479007 372862 373232MW-6R EPA 8151 EPA 8151
92342479009 372862 373232MW-9S EPA 8151 EPA 8151
92342479010 372862 373232MW-9D EPA 8151 EPA 8151
92342479011 372862 373232MW-10 EPA 8151 EPA 8151
92342479012 372862 373232MW-11S EPA 8151 EPA 8151
92342479013 372862 373232MW-11D EPA 8151 EPA 8151
92342529001 373221 373976MW-12 EPA 8151 EPA 8151
92342529002 373221 373976MW-13 EPA 8151 EPA 8151
92342337001 363006 363687MW-8 EPA 3010A EPA 6010
92342339001 363006 363687LAGOONEPA 3010A EPA 6010
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 209 of 241
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92342479001 363009 363688MW-1 EPA 3010A EPA 6010
92342479002 363009 363688MW-2 EPA 3010A EPA 6010
92342479003 363009 363688MW-3R EPA 3010A EPA 6010
92342479004 363010 363689MW-4S EPA 3010A EPA 6010
92342479005 363010 363689MW-4D EPA 3010A EPA 6010
92342479006 363010 363689MW-5 EPA 3010A EPA 6010
92342479007 363010 363689MW-6R EPA 3010A EPA 6010
92342479009 363010 363689MW-9S EPA 3010A EPA 6010
92342479010 363010 363689MW-9D EPA 3010A EPA 6010
92342479011 363010 363689MW-10 EPA 3010A EPA 6010
92342479012 363010 363689MW-11S EPA 3010A EPA 6010
92342479013 363010 363689MW-11D EPA 3010A EPA 6010
92342529001 363146 364135MW-12 EPA 3010A EPA 6010
92342529002 363146 364135MW-13 EPA 3010A EPA 6010
92342337001 363272 363377MW-8 EPA 3010A EPA 6020B
92342339001 363105 363113LAGOONEPA 3010A EPA 6020B
92342479001 362966 363181MW-1 EPA 3010A EPA 6020B
92342479002 362966 363181MW-2 EPA 3010A EPA 6020B
92342479003 362966 363181MW-3R EPA 3010A EPA 6020B
92342479004 362966 363181MW-4S EPA 3010A EPA 6020B
92342479005 362966 363181MW-4D EPA 3010A EPA 6020B
92342479006 362966 363181MW-5 EPA 3010A EPA 6020B
92342479007 362966 363181MW-6R EPA 3010A EPA 6020B
92342479009 362966 363181MW-9S EPA 3010A EPA 6020B
92342479010 362966 363181MW-9D EPA 3010A EPA 6020B
92342479011 362966 363181MW-10 EPA 3010A EPA 6020B
92342479012 362966 363181MW-11S EPA 3010A EPA 6020B
92342479013 362966 363181MW-11D EPA 3010A EPA 6020B
92342529001 363272 363377MW-12 EPA 3010A EPA 6020B
92342529002 363272 363377MW-13 EPA 3010A EPA 6020B
92342337001 363241 363571MW-8 EPA 7470 EPA 7470
92342339001 363241 363571LAGOONEPA 7470 EPA 7470
92342479001 363241 363571MW-1 EPA 7470 EPA 7470
92342479002 363241 363571MW-2 EPA 7470 EPA 7470
92342479003 363241 363571MW-3R EPA 7470 EPA 7470
92342479004 363241 363571MW-4S EPA 7470 EPA 7470
92342479005 363241 363571MW-4D EPA 7470 EPA 7470
92342479006 363241 363571MW-5 EPA 7470 EPA 7470
92342479007 363241 363571MW-6R EPA 7470 EPA 7470
92342479009 363241 363571MW-9S EPA 7470 EPA 7470
92342479010 363241 363571MW-9D EPA 7470 EPA 7470
92342479011 363333 363334MW-10 EPA 7470 EPA 7470
92342479012 363333 363334MW-11S EPA 7470 EPA 7470
92342479013 363333 363334MW-11D EPA 7470 EPA 7470
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 210 of 241
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92342529001 363457 363483MW-12 EPA 7470 EPA 7470
92342529002 363457 363483MW-13 EPA 7470 EPA 7470
92342337001 363548 363787MW-8 EPA 3510 EPA 8270
92342479001 363842 364328MW-1 EPA 3510 EPA 8270
92342479002 363842 364328MW-2 EPA 3510 EPA 8270
92342479003 363842 364328MW-3R EPA 3510 EPA 8270
92342479004 363842 364328MW-4S EPA 3510 EPA 8270
92342479005 363842 364328MW-4D EPA 3510 EPA 8270
92342479006 363842 364328MW-5 EPA 3510 EPA 8270
92342479007 363842 364328MW-6R EPA 3510 EPA 8270
92342479009 364808 364328MW-9S EPA 3510 EPA 8270
92342479010 363842 364328MW-9D EPA 3510 EPA 8270
92342479011 363842 364328MW-10 EPA 3510 EPA 8270
92342479012 363842 364328MW-11S EPA 3510 EPA 8270
92342479013 363842 364328MW-11D EPA 3510 EPA 8270
92342529001 364049 364817MW-12 EPA 3510 EPA 8270
92342529002 364049 364817MW-13 EPA 3510 EPA 8270
92342337001 362875MW-8 EPA 8260
92342339001 362875LAGOONEPA 8260
92342479001 363024MW-1 EPA 8260
92342479002 363024MW-2 EPA 8260
92342479003 363024MW-3R EPA 8260
92342479004 363024MW-4S EPA 8260
92342479005 363024MW-4D EPA 8260
92342479006 363024MW-5 EPA 8260
92342479007 363024MW-6R EPA 8260
92342479009 363024MW-9S EPA 8260
92342479010 363024MW-9D EPA 8260
92342479011 363024MW-10 EPA 8260
92342479012 363024MW-11S EPA 8260
92342479013 363024MW-11D EPA 8260
92342529001 364296MW-12 EPA 8260
92342529002 363307MW-13 EPA 8260
92342337001 363078MW-8 SM 4500-S2D
92342479001 363078MW-1 SM 4500-S2D
92342479002 363078MW-2 SM 4500-S2D
92342479003 363078MW-3R SM 4500-S2D
92342479004 363078MW-4S SM 4500-S2D
92342479005 363078MW-4D SM 4500-S2D
92342479006 363078MW-5 SM 4500-S2D
92342479007 363078MW-6R SM 4500-S2D
92342479009 363078MW-9S SM 4500-S2D
92342479010 363078MW-9D SM 4500-S2D
92342479011 363078MW-10 SM 4500-S2D
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 211 of 241
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92342337
SURRY CO. LINED MSWLF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92342479012 363621MW-11S SM 4500-S2D
92342479013 363079MW-11D SM 4500-S2D
92342529001 363623MW-12 SM 4500-S2D
92342529002 363623MW-13 SM 4500-S2D
92342339001 362936 362948LAGOONSM 5210B SM 5210B
92342339001 363259LAGOONEPA 9040
92342339001 363281LAGOONEPA 300.0
92342339001 362937LAGOONEPA 353.2
92342339001 363097LAGOONEPA 365.1
92342337001 362991MW-8 SM 4500-CN-E
92342339001 362991LAGOONSM 4500-CN-E
92342479001 362991MW-1 SM 4500-CN-E
92342479002 362992MW-2 SM 4500-CN-E
92342479003 362992MW-3R SM 4500-CN-E
92342479004 362992MW-4S SM 4500-CN-E
92342479005 362992MW-4D SM 4500-CN-E
92342479006 362992MW-5 SM 4500-CN-E
92342479007 362992MW-6R SM 4500-CN-E
92342479009 362992MW-9S SM 4500-CN-E
92342479010 362992MW-9D SM 4500-CN-E
92342479011 362992MW-10 SM 4500-CN-E
92342479012 362992MW-11S SM 4500-CN-E
92342479013 362992MW-11D SM 4500-CN-E
92342529001 363513MW-12 SM 4500-CN-E
92342529002 363513MW-13 SM 4500-CN-E
92342339001 363092LAGOONSM 5220D
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/19/2017 12:34 PM
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Huntersville, NC 28078
[phone]
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This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
07/25/2017
Municipal Engineering Services Co., PA
Jonathan Pfohl
68 Shipwash Drive
Garner, NC 27529
Project: Surry Lined MSWLF
Lab Submittal Date: 07/12/2017
Prism Work Order: 7070173
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
President/Project Manager
Reviewed ByRobbi A. Jones Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
CCV CCV result is above the control limits. Analyte not detected in the sample. No further action taken.
D RPD value outside of the control limits.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
L Parameter reported with possible low bias. LCS recovery below the QC limit.
LH High LCS recovery. Analyte not detected in the sample(s). No further action taken.
SE Surrogate recovery outside the QC limits due to emulsion.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 16
Sample Receipt Summary
07/25/2017
Prism Work Order: 7070173
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
7070173-01 07/08/17MW-3R 07/12/17Water
Samples were received in good condition at 3.9 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 16
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order:
Summary of Detections
There were no detections reported.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 16
Laboratory Report
07/25/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
68 Shipwash Drive
Project: Surry Lined MSWLFMunicipal Engineering Services Co., PA
Garner, NC 27529
Attn: Jonathan Pfohl
Sample Matrix: Water
Client Sample ID: MW-3R
Prism Sample ID: 7070173-01
Prism Work Order: 7070173
Time Collected: 07/08/17 10:00
Time Submitted: 07/12/17 08:10
Semivolatile Organic Compounds by GC/MS
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.41,2,4,5-Tetrachlorobenzene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.81,2,4-Trichlorobenzene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.61,2-Dichlorobenzene
BRL 8270D P7G01861207/14/17 17:46 JMVug/L 2.81,3,5-Trinitrobenzene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.91,3-Dichlorobenzene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.61,4-Dichlorobenzene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.71,4-Naphthoquinone
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.81,4-Phenylenediamine
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.71-Naphthylamine
BRL 8270D P7G01861107/14/17 17:46 JMVCCVug/L 2.82,3,4,6-Tetrachlorophenol
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.62,4,5-Trichlorophenol
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.82,4,6-Trichlorophenol
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.62,4-Dichlorophenol
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 3.42,4-Dimethylphenol
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.72,4-Dinitrophenol
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.42,4-Dinitrotoluene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.02,6-Dichlorophenol
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.12,6-Dinitrotoluene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.72-Acetylaminofluorene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.72-Chloronaphthalene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.92-Chlorophenol
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.42-Methylnaphthalene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.82-Methylphenol
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.12-Naphthylamine
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.42-Nitroaniline
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.42-Nitrophenol
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.43,3’-Dichlorobenzidine
BRL 8270D P7G01861207/14/17 17:46 JMVug/L 3.13,3·-Dimethylbenzidine
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.53/4-Methylphenol
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.43-Methylcholanthrene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.43-Nitroaniline
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.44,6-Dinitro-2-methylphenol
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.44-Aminobiphenyl
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.34-Bromophenyl phenyl ether
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.44-Chloro-3-methylphenol
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.44-Chloroaniline
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.34-Chlorophenyl phenyl ether
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 0.934-Nitroaniline
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 0.604-Nitrophenol
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.65-Nitro-o-toluidine
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.67,12-Dimethylbenz(a)anthracene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.8Acenaphthene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 16
Laboratory Report
07/25/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
68 Shipwash Drive
Project: Surry Lined MSWLFMunicipal Engineering Services Co., PA
Garner, NC 27529
Attn: Jonathan Pfohl
Sample Matrix: Water
Client Sample ID: MW-3R
Prism Sample ID: 7070173-01
Prism Work Order: 7070173
Time Collected: 07/08/17 10:00
Time Submitted: 07/12/17 08:10
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.0Acenaphthylene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.4Acetophenone
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.4Anthracene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.4Benzo(a)anthracene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.4Benzo(a)pyrene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.1Benzo(b)fluoranthene
BRL 8270D P7G01861207/14/17 17:46 JMVug/L 1.4Benzo(b&k)fluoranthene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.4Benzo(g,h,i)perylene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.4Benzo(k)fluoranthene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.1Benzyl alcohol
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.6bis(2-Chloroethoxy)methane
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.3Bis(2-Chloroethyl)ether
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.0Bis(2-chloroisopropyl)ether
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.3Bis(2-Ethylhexyl)phthalate
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.4Butyl benzyl phthalate
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.5Chlorobenzilate
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.4Chrysene
BRL 8270D P7G01861207/14/17 17:46 JMVug/L 2.8Diallate
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.2Dibenzo(a,h)anthracene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.8Dibenzofuran
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 3.3Diethyl phthalate
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 3.1Dimethoate
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.4Dimethyl phthalate
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.7Di-n-butyl phthalate
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.3Di-n-octyl phthalate
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.8Diphenylamine
BRL 8270D P7G01861207/14/17 17:46 JMVug/L 2.8Disulfoton
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.8Ethyl Methanesulfonate
BRL 8270D P7G01861207/14/17 17:46 JMVug/L 4.3Famphur
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.7Fluoranthene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.7Fluorene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.3Hexachlorobenzene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.1Hexachlorobutadiene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.7Hexachlorocyclopentadiene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.7Hexachloroethane
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.0Hexachloropropene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 3.9Indeno(1,2,3-cd)pyrene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.7Isodrin
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.5Isophorone
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 3.8Isosafrole
BRL 8270D P7G01861207/14/17 17:46 JMVCCVug/L 2.8Kepone
BRL 8270D P7G018611007/14/17 17:46 JMVug/L 12Methapyrilene
BRL 8270D P7G01861207/14/17 17:46 JMVug/L 2.4Methyl Methanesulfonate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 16
Laboratory Report
07/25/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
68 Shipwash Drive
Project: Surry Lined MSWLFMunicipal Engineering Services Co., PA
Garner, NC 27529
Attn: Jonathan Pfohl
Sample Matrix: Water
Client Sample ID: MW-3R
Prism Sample ID: 7070173-01
Prism Work Order: 7070173
Time Collected: 07/08/17 10:00
Time Submitted: 07/12/17 08:10
BRL 8270D P7G01861207/14/17 17:46 JMVug/L 3.4Methyl parathion
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.6Nitrobenzene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.5N-Nitrosodibutylamine
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.8N-Nitrosodiethylamine
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.1N-Nitrosodimethylamine
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.2N-Nitroso-di-n-propylamine
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.3N-Nitrosodiphenylamine
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.5N-Nitrosomethylethylamine
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.4N-Nitrosopiperidine
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.9N-Nitrosopyrrolidine
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.8O,O,O-Triethyl phosphorothioate
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.8o-Toluidine
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 3.0Parathion
BRL 8270D P7G01861207/14/17 17:46 JMVug/L 2.3p-Dimethylaminoazobenzene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.6Pentachlorobenzene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.3Pentachloronitrobenzene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.2Pentachlorophenol
BRL 8270D P7G01861207/14/17 17:46 JMVug/L 3.0Phenacetin
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.5Phenanthrene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 0.98Phenol
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.8Phorate
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.8Pronamide
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.4Pyrene
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 2.2Safrole
BRL 8270D P7G01861107/14/17 17:46 JMVug/L 1.9Thionazin
Surrogate Recovery Control Limits
44-11923 %2-Fluorobiphenyl SE
19-11929 %2-Fluorophenol
44-12020 %Nitrobenzene-d5 SE
11-5220 %Phenol-d5
50-13429 %Terphenyl-d14 SE
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 16
7/25/17
Level II QC Report
68 Shipwash Drive
Project: Surry Lined MSWLFMunicipal Engineering Services Co., PA
Garner, NC 27529
Attn: Jonathan Pfohl
Prism Work Order: 7070173
Time Submitted: 7/12/2017 8:10:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7G0186 - 3510C MS
Blank (P7G0186-BLK1)Prepared: 07/13/17 Analyzed: 07/14/17
1,2,4,5-Tetrachlorobenzene ug/LBRL10
1,2,4-Trichlorobenzene ug/LBRL10
1,2-Dichlorobenzene ug/LBRL10
1,3,5-Trinitrobenzene ug/LBRL20
1,3-Dichlorobenzene ug/LBRL10
1,4-Dichlorobenzene ug/LBRL10
1,4-Naphthoquinone ug/LBRL10
1,4-Phenylenediamine ug/LBRL10
1-Naphthylamine ug/LBRL10
2,3,4,6-Tetrachlorophenol ug/LBRL10
2,4,5-Trichlorophenol ug/LBRL10
2,4,6-Trichlorophenol ug/LBRL10
2,4-Dichlorophenol ug/LBRL10
2,4-Dimethylphenol ug/LBRL10
2,4-Dinitrophenol ug/LBRL10
2,4-Dinitrotoluene ug/LBRL10
2,6-Dichlorophenol ug/LBRL10
2,6-Dinitrotoluene ug/LBRL10
2-Acetylaminofluorene ug/LBRL10
2-Chloronaphthalene ug/LBRL10
2-Chlorophenol ug/LBRL10
2-Methylnaphthalene ug/LBRL10
2-Methylphenol ug/LBRL10
2-Naphthylamine ug/LBRL10
2-Nitroaniline ug/LBRL10
2-Nitrophenol ug/LBRL10
3,3’-Dichlorobenzidine ug/LBRL10
3,3·-Dimethylbenzidine ug/LBRL20
3/4-Methylphenol ug/LBRL10
3-Methylcholanthrene ug/LBRL10
3-Nitroaniline ug/LBRL10
4,6-Dinitro-2-methylphenol ug/LBRL10
4-Aminobiphenyl ug/LBRL10
4-Bromophenyl phenyl ether ug/LBRL10
4-Chloro-3-methylphenol ug/LBRL10
4-Chloroaniline ug/LBRL10
4-Chlorophenyl phenyl ether ug/LBRL10
4-Nitroaniline ug/LBRL10
4-Nitrophenol ug/LBRL10
5-Nitro-o-toluidine ug/LBRL10
7,12-Dimethylbenz(a)anthracene ug/LBRL10
Acenaphthene ug/LBRL10
Acenaphthylene ug/LBRL10
Acetophenone ug/LBRL10
Anthracene ug/LBRL10
Benzo(a)anthracene ug/LBRL10
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 16
7/25/17
Level II QC Report
68 Shipwash Drive
Project: Surry Lined MSWLFMunicipal Engineering Services Co., PA
Garner, NC 27529
Attn: Jonathan Pfohl
Prism Work Order: 7070173
Time Submitted: 7/12/2017 8:10:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7G0186 - 3510C MS
Blank (P7G0186-BLK1)Prepared: 07/13/17 Analyzed: 07/14/17
Benzo(a)pyrene ug/LBRL10
Benzo(b)fluoranthene ug/LBRL10
Benzo(b&k)fluoranthene ug/LBRL20
Benzo(g,h,i)perylene ug/LBRL10
Benzo(k)fluoranthene ug/LBRL10
Benzyl alcohol ug/LBRL10
bis(2-Chloroethoxy)methane ug/LBRL10
Bis(2-Chloroethyl)ether ug/LBRL10
Bis(2-chloroisopropyl)ether ug/LBRL10
Bis(2-Ethylhexyl)phthalate ug/LBRL10
Butyl benzyl phthalate ug/LBRL10
Chlorobenzilate ug/LBRL10
Chrysene ug/LBRL10
Diallate ug/LBRL20
Dibenzo(a,h)anthracene ug/LBRL10
Dibenzofuran ug/LBRL10
Diethyl phthalate ug/LBRL10
Dimethoate ug/LBRL10
Dimethyl phthalate ug/LBRL10
Di-n-butyl phthalate ug/LBRL10
Di-n-octyl phthalate ug/LBRL10
Diphenylamine ug/LBRL10
Disulfoton ug/LBRL20
Ethyl Methanesulfonate ug/LBRL10
Famphur ug/LBRL20
Fluoranthene ug/LBRL10
Fluorene ug/LBRL10
Hexachlorobenzene ug/LBRL10
Hexachlorobutadiene ug/LBRL10
Hexachlorocyclopentadiene ug/LBRL10
Hexachloroethane ug/LBRL10
Hexachloropropene ug/LBRL10
Indeno(1,2,3-cd)pyrene ug/LBRL10
Isodrin ug/LBRL10
Isophorone ug/LBRL10
Isosafrole ug/LBRL10
Kepone ug/LBRL20
Methapyrilene ug/LBRL100
Methyl Methanesulfonate ug/LBRL20
Methyl parathion ug/LBRL20
Nitrobenzene ug/LBRL10
N-Nitrosodibutylamine ug/LBRL10
N-Nitrosodiethylamine ug/LBRL10
N-Nitrosodimethylamine ug/LBRL10
N-Nitroso-di-n-propylamine ug/LBRL10
N-Nitrosodiphenylamine ug/LBRL10
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 16
7/25/17
Level II QC Report
68 Shipwash Drive
Project: Surry Lined MSWLFMunicipal Engineering Services Co., PA
Garner, NC 27529
Attn: Jonathan Pfohl
Prism Work Order: 7070173
Time Submitted: 7/12/2017 8:10:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7G0186 - 3510C MS
Blank (P7G0186-BLK1)Prepared: 07/13/17 Analyzed: 07/14/17
N-Nitrosomethylethylamine ug/LBRL10
N-Nitrosopiperidine ug/LBRL10
N-Nitrosopyrrolidine ug/LBRL10
O,O,O-Triethyl phosphorothioate ug/LBRL10
o-Toluidine ug/LBRL10
Parathion ug/LBRL10
p-Dimethylaminoazobenzene ug/LBRL20
Pentachlorobenzene ug/LBRL10
Pentachloronitrobenzene ug/LBRL10
Pentachlorophenol ug/LBRL10
Phenacetin ug/LBRL20
Phenanthrene ug/LBRL10
Phenol ug/LBRL10
Phorate ug/LBRL10
Pronamide ug/LBRL10
Pyrene ug/LBRL10
Safrole ug/LBRL10
Thionazin ug/LBRL10
ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 7839.1
ug/L 100.0 19-119Surrogate: 2-Fluorophenol 5454.4
ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 7437.0
ug/L 100.0 11-52Surrogate: Phenol-d5 3534.8
ug/L 50.00 50-134Surrogate: Terphenyl-d14 9648.1
LCS (P7G0186-BS1)Prepared: 07/13/17 Analyzed: 07/14/17
1,2,4-Trichlorobenzene ug/L31.7 10 50.00 29-12663
1,2-Dichlorobenzene ug/L31.1 10 50.00 32-11162
1,3-Dichlorobenzene ug/L30.1 10 50.00 28-11060
1,4-Dichlorobenzene ug/L29.9 10 50.00 29-11260
2,4,5-Trichlorophenol ug/L42.0 10 50.00 53-12384
2,4,6-Trichlorophenol ug/L42.4 10 50.00 50-12585
2,4-Dichlorophenol ug/L36.5 10 50.00 47-12173
2,4-Dimethylphenol ug/L45.6 10 50.00 31-12491
2,4-Dinitrophenol ug/L43.3 10 50.00 23-14387
2,4-Dinitrotoluene ug/L45.5 10 50.00 57-12891
2,6-Dinitrotoluene ug/L45.3 10 50.00 57-12491
2-Chloronaphthalene ug/L39.5 10 50.00 40-11679
2-Chlorophenol ug/L37.1 10 50.00 38-11774
2-Methylnaphthalene ug/L36.5 10 50.00 40-12173
2-Methylphenol ug/L35.0 10 50.00 30-11770
2-Nitroaniline ug/L40.3 10 50.00 55-12781
2-Nitrophenol ug/L37.8 10 50.00 47-12376
3,3’-Dichlorobenzidine ug/L45.6 10 50.00 27-12991
3/4-Methylphenol ug/L28.8 10 50.00 29-11058
3-Nitroaniline ug/L40.6 10 50.00 41-12881
4,6-Dinitro-2-methylphenol ug/L42.8 10 50.00 44-13786
4-Bromophenyl phenyl ether ug/L41.1 10 50.00 55-12482
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 16
7/25/17
Level II QC Report
68 Shipwash Drive
Project: Surry Lined MSWLFMunicipal Engineering Services Co., PA
Garner, NC 27529
Attn: Jonathan Pfohl
Prism Work Order: 7070173
Time Submitted: 7/12/2017 8:10:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7G0186 - 3510C MS
LCS (P7G0186-BS1)Prepared: 07/13/17 Analyzed: 07/14/17
4-Chloro-3-methylphenol ug/L40.5 10 50.00 52-11981
4-Chloroaniline ug/L41.1 10 50.00 33-11782
4-Chlorophenyl phenyl ether ug/L39.4 10 50.00 53-12179
4-Nitroaniline ug/L37.9 10 50.00 45-13576
4-Nitrophenol ug/L18.4 10 50.00 10-7737
Acenaphthene ug/L40.2 10 50.00 47-12280
Acenaphthylene ug/L41.3 10 50.00 41-13083
Acetophenone ug/L37.8 10 50.00 46-11876
Anthracene ug/L46.0 10 50.00 57-12392
Benzo(a)anthracene ug/L44.8 10 50.00 58-12590
Benzo(a)pyrene ug/L45.2 10 50.00 54-12890
Benzo(b)fluoranthene ug/L45.9 10 50.00 53-13192
Benzo(g,h,i)perylene ug/L39.8 10 50.00 50-13480
Benzo(k)fluoranthene ug/L43.3 10 50.00 57-12987
Benzyl alcohol ug/L35.0 10 50.00 31-11270
bis(2-Chloroethoxy)methane ug/L35.6 10 50.00 48-12071
Bis(2-Chloroethyl)ether ug/L33.0 10 50.00 43-11866
Bis(2-chloroisopropyl)ether ug/L33.0 10 50.00 37-13066
Bis(2-Ethylhexyl)phthalate ug/L44.3 10 50.00 55-13589
Butyl benzyl phthalate ug/L42.6 10 50.00 53-13485
Chrysene ug/L44.5 10 50.00 59-12389
Dibenzo(a,h)anthracene ug/L44.1 10 50.00 51-13488
Dibenzofuran ug/L42.6 10 50.00 53-11885
Diethyl phthalate ug/L44.6 10 50.00 56-12589
Dimethyl phthalate ug/L41.5 10 50.00 45-12783
Di-n-butyl phthalate ug/L45.8 10 50.00 59-12792
Di-n-octyl phthalate ug/L45.5 10 50.00 51-14091
Fluoranthene ug/L44.3 10 50.00 57-12889
Fluorene ug/L42.1 10 50.00 52-12484
Hexachlorobenzene ug/L43.1 10 50.00 53-12586
Hexachlorobutadiene ug/L31.8 10 50.00 22-12464
Hexachlorocyclopentadiene ug/L17.0 10 50.00 32-11734
Hexachloroethane ug/L28.0 10 50.00 21-11556
Indeno(1,2,3-cd)pyrene ug/L47.2 10 50.00 52-13494
Isophorone ug/L38.6 10 50.00 42-12477
Nitrobenzene ug/L35.4 10 50.00 45-12171
N-Nitrosodimethylamine ug/L25.9 10 50.00 10-11952
N-Nitroso-di-n-propylamine ug/L35.8 10 50.00 49-11972
N-Nitrosodiphenylamine ug/L54.1 10 50.00 51-123108
Pentachlorophenol ug/L52.6 10 50.00 35-138105
Phenanthrene ug/L45.6 10 50.00 59-12091
Phenol ug/L18.7 10 50.00 12-5837
Pyrene ug/L44.3 10 50.00 57-12689
ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 7537.7
ug/L 100.0 19-119Surrogate: 2-Fluorophenol 4746.9
ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 6733.7
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 16
7/25/17
Level II QC Report
68 Shipwash Drive
Project: Surry Lined MSWLFMunicipal Engineering Services Co., PA
Garner, NC 27529
Attn: Jonathan Pfohl
Prism Work Order: 7070173
Time Submitted: 7/12/2017 8:10:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7G0186 - 3510C MS
LCS (P7G0186-BS1)Prepared: 07/13/17 Analyzed: 07/14/17
ug/L 100.0 11-52Surrogate: Phenol-d5 3130.9
ug/L 50.00 50-134Surrogate: Terphenyl-d14 9748.7
LCS (P7G0186-BS2)Prepared: 07/13/17 Analyzed: 07/14/17
1,2,4,5-Tetrachlorobenzene ug/L30.8 10 50.00 35-12162
1,3,5-Trinitrobenzene ug/L45.3 20 50.00 41-13791
1,4-Naphthoquinone ug/L40.7 10 50.00 45-13581
1,4-Phenylenediamine ug/L47.6 10 50.00 45-13595
1-Naphthylamine ug/L42.1 10 50.00 24-12484
2,3,4,6-Tetrachlorophenol ug/L49.4 10 50.00 50-12899
2,6-Dichlorophenol ug/L41.1 10 50.00 50-11882
2-Acetylaminofluorene ug/L49.6 10 50.00 60-13899
2-Naphthylamine ug/L39.1 10 50.00 45-13578
3,3·-Dimethylbenzidine ug/L23.1 20 50.00 45-13546
3-Methylcholanthrene ug/L46.1 10 50.00 56-13392
4-Aminobiphenyl ug/L39.0 10 50.00 45-13578
5-Nitro-o-toluidine ug/L48.4 10 50.00 38-12697
7,12-Dimethylbenz(a)anthracene ug/L45.7 10 50.00 61-13391
Acetophenone ug/L38.0 10 50.00 46-11876
Chlorobenzilate ug/L48.9 10 50.00 58-15098
Diallate ug/L48.4 20 50.00 45-13597
Dimethoate ug/L49.8 10 50.00 45-135100
Diphenylamine ug/L44.9 10 50.00 55-11190
Disulfoton ug/L40.2 20 50.00 55-13080
Ethyl Methanesulfonate ug/L39.0 10 50.00 62-11878
Famphur ug/L74.1 20 50.00 LH45-135148
Hexachloropropene ug/L20.2 10 50.00 L45-13540
Isodrin ug/L45.8 10 50.00 68-12892
Isosafrole ug/L40.5 10 50.00 56-12681
Kepone ug/L60.8 20 50.00 45-135122
Methapyrilene ug/L16.0 100 50.00 L, J45-13532
Methyl Methanesulfonate ug/L29.6 20 50.00 33-10759
Methyl parathion ug/L51.1 20 50.00 45-159102
N-Nitrosodibutylamine ug/L40.6 10 50.00 60-12181
N-Nitrosodiethylamine ug/L41.6 10 50.00 43-12183
N-Nitrosomethylethylamine ug/L38.8 10 50.00 41-11778
N-Nitrosopiperidine ug/L38.5 10 50.00 56-12177
N-Nitrosopyrrolidine ug/L36.9 10 50.00 48-11374
O,O,O-Triethyl phosphorothioate ug/L39.1 10 50.00 60-11978
o-Toluidine ug/L35.4 10 50.00 30-11071
Parathion ug/L49.4 10 50.00 66-14099
p-Dimethylaminoazobenzene ug/L44.8 20 50.00 45-13590
Pentachlorobenzene ug/L37.8 10 50.00 59-12376
Pentachloronitrobenzene ug/L43.1 10 50.00 54-13586
Phenacetin ug/L48.8 20 50.00 71-12498
Phorate ug/L45.3 10 50.00 38-13991
Pronamide ug/L46.7 10 50.00 65-12993
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 16
7/25/17
Level II QC Report
68 Shipwash Drive
Project: Surry Lined MSWLFMunicipal Engineering Services Co., PA
Garner, NC 27529
Attn: Jonathan Pfohl
Prism Work Order: 7070173
Time Submitted: 7/12/2017 8:10:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7G0186 - 3510C MS
LCS (P7G0186-BS2)Prepared: 07/13/17 Analyzed: 07/14/17
Safrole ug/L42.4 10 50.00 61-11985
Thionazin ug/L47.8 10 50.00 72-13296
ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 7437.1
ug/L 100.0 19-119Surrogate: 2-Fluorophenol 5352.7
ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 6934.6
ug/L 100.0 11-52Surrogate: Phenol-d5 3434.4
ug/L 50.00 50-134Surrogate: Terphenyl-d14 9849.2
LCS Dup (P7G0186-BSD1)Prepared: 07/13/17 Analyzed: 07/14/17
1,2,4-Trichlorobenzene ug/L33.3 10 50.00 2029-12667 5
1,2-Dichlorobenzene ug/L33.9 10 50.00 2032-11168 9
1,3-Dichlorobenzene ug/L31.9 10 50.00 2028-11064 6
1,4-Dichlorobenzene ug/L32.8 10 50.00 2029-11266 9
2,4,5-Trichlorophenol ug/L41.3 10 50.00 2053-12383 2
2,4,6-Trichlorophenol ug/L41.7 10 50.00 2050-12583 2
2,4-Dichlorophenol ug/L38.8 10 50.00 2047-12178 6
2,4-Dimethylphenol ug/L44.1 10 50.00 2031-12488 3
2,4-Dinitrophenol ug/L43.0 10 50.00 2023-14386 0.6
2,4-Dinitrotoluene ug/L43.4 10 50.00 2057-12887 5
2,6-Dinitrotoluene ug/L43.2 10 50.00 2057-12486 5
2-Chloronaphthalene ug/L39.7 10 50.00 2040-11679 0.5
2-Chlorophenol ug/L40.0 10 50.00 2038-11780 8
2-Methylnaphthalene ug/L38.9 10 50.00 2040-12178 6
2-Methylphenol ug/L38.0 10 50.00 2030-11776 8
2-Nitroaniline ug/L38.0 10 50.00 2055-12776 6
2-Nitrophenol ug/L40.4 10 50.00 2047-12381 7
3,3’-Dichlorobenzidine ug/L43.7 10 50.00 2027-12987 4
3/4-Methylphenol ug/L30.5 10 50.00 2029-11061 6
3-Nitroaniline ug/L38.6 10 50.00 2041-12877 5
4,6-Dinitro-2-methylphenol ug/L43.1 10 50.00 2044-13786 0.6
4-Bromophenyl phenyl ether ug/L41.4 10 50.00 2055-12483 0.7
4-Chloro-3-methylphenol ug/L40.8 10 50.00 2052-11982 0.7
4-Chloroaniline ug/L42.1 10 50.00 2033-11784 2
4-Chlorophenyl phenyl ether ug/L38.2 10 50.00 2053-12176 3
4-Nitroaniline ug/L34.8 10 50.00 2045-13570 9
4-Nitrophenol ug/L17.0 10 50.00 2010-7734 8
Acenaphthene ug/L39.8 10 50.00 2047-12280 1
Acenaphthylene ug/L41.0 10 50.00 2041-13082 0.8
Acetophenone ug/L40.0 10 50.00 2046-11880 6
Anthracene ug/L45.7 10 50.00 2057-12391 0.6
Benzo(a)anthracene ug/L42.3 10 50.00 2058-12585 6
Benzo(a)pyrene ug/L43.6 10 50.00 2054-12887 4
Benzo(b)fluoranthene ug/L44.9 10 50.00 2053-13190 2
Benzo(g,h,i)perylene ug/L38.8 10 50.00 2050-13478 2
Benzo(k)fluoranthene ug/L42.3 10 50.00 2057-12985 2
Benzyl alcohol ug/L34.3 10 50.00 2031-11269 2
bis(2-Chloroethoxy)methane ug/L38.2 10 50.00 2048-12076 7
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 16
7/25/17
Level II QC Report
68 Shipwash Drive
Project: Surry Lined MSWLFMunicipal Engineering Services Co., PA
Garner, NC 27529
Attn: Jonathan Pfohl
Prism Work Order: 7070173
Time Submitted: 7/12/2017 8:10:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7G0186 - 3510C MS
LCS Dup (P7G0186-BSD1)Prepared: 07/13/17 Analyzed: 07/14/17
Bis(2-Chloroethyl)ether ug/L35.0 10 50.00 2043-11870 6
Bis(2-chloroisopropyl)ether ug/L35.2 10 50.00 2037-13070 6
Bis(2-Ethylhexyl)phthalate ug/L42.8 10 50.00 2055-13586 3
Butyl benzyl phthalate ug/L41.0 10 50.00 2053-13482 4
Chrysene ug/L43.3 10 50.00 2059-12387 3
Dibenzo(a,h)anthracene ug/L43.3 10 50.00 2051-13487 2
Dibenzofuran ug/L42.2 10 50.00 2053-11884 1
Diethyl phthalate ug/L41.8 10 50.00 2056-12584 6
Dimethyl phthalate ug/L40.1 10 50.00 2045-12780 3
Di-n-butyl phthalate ug/L45.1 10 50.00 2059-12790 1
Di-n-octyl phthalate ug/L44.4 10 50.00 2051-14089 2
Fluoranthene ug/L43.8 10 50.00 2057-12888 1
Fluorene ug/L41.1 10 50.00 2052-12482 2
Hexachlorobenzene ug/L43.8 10 50.00 2053-12588 1
Hexachlorobutadiene ug/L33.1 10 50.00 2022-12466 4
Hexachlorocyclopentadiene ug/L17.6 10 50.00 2032-11735 3
Hexachloroethane ug/L30.1 10 50.00 2021-11560 7
Indeno(1,2,3-cd)pyrene ug/L46.2 10 50.00 2052-13492 2
Isophorone ug/L40.0 10 50.00 2042-12480 4
Nitrobenzene ug/L38.0 10 50.00 2045-12176 7
N-Nitrosodimethylamine ug/L23.6 10 50.00 2010-11947 9
N-Nitroso-di-n-propylamine ug/L37.6 10 50.00 2049-11975 5
N-Nitrosodiphenylamine ug/L53.4 10 50.00 2051-123107 1
Pentachlorophenol ug/L52.9 10 50.00 2035-138106 0.5
Phenanthrene ug/L45.0 10 50.00 2059-12090 1
Phenol ug/L19.1 10 50.00 2012-5838 2
Pyrene ug/L43.2 10 50.00 2057-12686 3
ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 7738.6
ug/L 100.0 19-119Surrogate: 2-Fluorophenol 5251.5
ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 7235.8
ug/L 100.0 11-52Surrogate: Phenol-d5 3332.7
ug/L 50.00 50-134Surrogate: Terphenyl-d14 9447.1
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 16
7/25/17
Level II QC Report
68 Shipwash Drive
Project: Surry Lined MSWLFMunicipal Engineering Services Co., PA
Garner, NC 27529
Attn: Jonathan Pfohl
Prism Work Order: 7070173
Time Submitted: 7/12/2017 8:10:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7G0186 - 3510C MS
LCS Dup (P7G0186-BSD2)Prepared: 07/13/17 Analyzed: 07/14/17
1,2,4,5-Tetrachlorobenzene ug/L29.6 10 50.00 2035-12159 4
1,3,5-Trinitrobenzene ug/L44.4 20 50.00 2041-13789 2
1,4-Naphthoquinone ug/L40.1 10 50.00 2045-13580 1
1,4-Phenylenediamine ug/L46.4 10 50.00 2045-13593 3
1-Naphthylamine ug/L41.9 10 50.00 2024-12484 0.5
2,3,4,6-Tetrachlorophenol ug/L49.2 10 50.00 2050-12898 0.5
2,6-Dichlorophenol ug/L39.1 10 50.00 2050-11878 5
2-Acetylaminofluorene ug/L50.0 10 50.00 2060-138100 0.7
2-Naphthylamine ug/L38.2 10 50.00 2045-13576 2
3,3·-Dimethylbenzidine ug/L16.7 20 50.00 20 D, J45-13533 32
3-Methylcholanthrene ug/L46.5 10 50.00 2056-13393 0.8
4-Aminobiphenyl ug/L39.3 10 50.00 2045-13579 0.9
5-Nitro-o-toluidine ug/L48.5 10 50.00 2038-12697 0.2
7,12-Dimethylbenz(a)anthracene ug/L45.6 10 50.00 2061-13391 0.4
Acetophenone ug/L34.3 10 50.00 2046-11869 10
Chlorobenzilate ug/L47.4 10 50.00 2058-15095 3
Diallate ug/L50.5 20 50.00 2045-135101 4
Dimethoate ug/L49.2 10 50.00 2045-13598 1
Diphenylamine ug/L45.3 10 50.00 2055-11191 0.8
Disulfoton ug/L34.3 20 50.00 2055-13069 16
Ethyl Methanesulfonate ug/L35.6 10 50.00 2062-11871 9
Famphur ug/L72.7 20 50.00 20 LH45-135145 2
Hexachloropropene ug/L17.9 10 50.00 20 L45-13536 12
Isodrin ug/L45.4 10 50.00 2068-12891 0.9
Isosafrole ug/L38.6 10 50.00 2056-12677 5
Kepone ug/L56.9 20 50.00 2045-135114 7
Methapyrilene ug/L18.6 100 50.00 20 L, J45-13537 15
Methyl Methanesulfonate ug/L26.3 20 50.00 2033-10753 12
Methyl parathion ug/L51.0 20 50.00 2045-159102 0.3
N-Nitrosodibutylamine ug/L38.5 10 50.00 2060-12177 5
N-Nitrosodiethylamine ug/L36.8 10 50.00 2043-12174 12
N-Nitrosomethylethylamine ug/L34.5 10 50.00 2041-11769 12
N-Nitrosopiperidine ug/L35.7 10 50.00 2056-12171 7
N-Nitrosopyrrolidine ug/L34.3 10 50.00 2048-11369 7
O,O,O-Triethyl phosphorothioate ug/L35.8 10 50.00 2060-11972 9
o-Toluidine ug/L33.0 10 50.00 2030-11066 7
Parathion ug/L49.1 10 50.00 2066-14098 0.5
p-Dimethylaminoazobenzene ug/L44.7 20 50.00 2045-13589 0.4
Pentachlorobenzene ug/L38.1 10 50.00 2059-12376 0.6
Pentachloronitrobenzene ug/L43.9 10 50.00 2054-13588 2
Phenacetin ug/L48.0 20 50.00 2071-12496 1
Phorate ug/L44.4 10 50.00 2038-13989 2
Pronamide ug/L45.9 10 50.00 2065-12992 2
Safrole ug/L40.6 10 50.00 2061-11981 4
Thionazin ug/L47.5 10 50.00 2072-13295 0.7
ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 7235.8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 16
7/25/17
Level II QC Report
68 Shipwash Drive
Project: Surry Lined MSWLFMunicipal Engineering Services Co., PA
Garner, NC 27529
Attn: Jonathan Pfohl
Prism Work Order: 7070173
Time Submitted: 7/12/2017 8:10:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P7G0186 - 3510C MS
LCS Dup (P7G0186-BSD2)Prepared: 07/13/17 Analyzed: 07/14/17
ug/L 100.0 19-119Surrogate: 2-Fluorophenol 4746.7
ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 6231.1
ug/L 100.0 11-52Surrogate: Phenol-d5 3232.2
ug/L 50.00 50-134Surrogate: Terphenyl-d14 9748.5
Sample Extraction Data
Prep Method: 3510C MS
Lab Number Batch Date/TimeInitialFinal
P7G01867070173-01 07/13/17 11:3010001mLmL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 16
Page 16 of 16
#=CL#
June 16, 2017
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92342549
92342549
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
SURRY MSWLF SWS
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory between June 01, 2017
and June 02, 2017. The results relate only to the samples included in this report. Results reported
herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality
Assurance Manual, where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 44
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 44
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Lab ID Sample ID Matrix Date Collected Date Received
92342549001 SW-3 Water 05/31/17 00:00 06/01/17 07:55
92342730001 SW-1 Water 06/01/17 10:25 06/02/17 08:00
92342730002 SW-2 Water 06/01/17 16:00 06/02/17 08:00
92342730004 SW-4 Water 06/01/17 10:35 06/02/17 08:00
92342730005 SWN-1 Water 06/01/17 11:00 06/02/17 08:00
92342730006 SWN-2 Water 06/01/17 14:00 06/02/17 08:00
92342730007 SW-A Water 06/01/17 12:10 06/02/17 08:00
92342730008 SW-B Water 06/01/17 12:30 06/02/17 08:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 44
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92342549001 SW-3 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92342730001 SW-1 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92342730002 SW-2 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92342730004 SW-4 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92342730005 SWN-1 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92342730006 SWN-2 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92342730007 SW-A EPA 8260 50 PASI-CGAW
92342730008 SW-B EPA 8260 50 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Sample:SW-3 Lab ID:92342549001 Collected:05/31/17 00:00 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/09/17 21:51 7440-36-006/02/17 11:256.0 3.9 1
Arsenic ND ug/L 06/09/17 21:51 7440-38-206/02/17 11:2510.0 5.0 1
Barium 21.8J ug/L 06/09/17 21:51 7440-39-306/02/17 11:251002.5 1
Beryllium ND ug/L 06/09/17 21:51 7440-41-706/02/17 11:251.0 0.50 1
Cadmium ND ug/L 06/09/17 21:51 7440-43-906/02/17 11:251.0 0.50 1
Chromium ND ug/L 06/09/17 21:51 7440-47-306/02/17 11:2510.0 2.5 1
Cobalt 8.0J ug/L 06/09/17 21:51 7440-48-406/02/17 11:2510.0 2.5 1
Copper ND ug/L 06/09/17 21:51 7440-50-806/02/17 11:2510.0 2.5 1
Lead ND ug/L 06/09/17 21:51 7439-92-106/02/17 11:2510.0 2.5 1
Nickel ND ug/L 06/09/17 21:51 7440-02-006/02/17 11:2550.0 2.5 1
Selenium ND ug/L 06/09/17 21:51 7782-49-206/02/17 11:2510.0 5.0 1
Silver ND ug/L 06/09/17 21:51 7440-22-406/02/17 11:2510.0 2.5 1
Vanadium ND ug/L 06/09/17 21:51 7440-62-206/02/17 11:2525.0 2.5 1
Zinc 7.4J ug/L 06/09/17 21:51 7440-66-606/02/17 11:2510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/09/17 17:22 7440-28-006/06/17 02:455.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/04/17 08:10 67-64-110010.0 1
Acrylonitrile ND ug/L 06/04/17 08:10 107-13-12001.9 1
Benzene ND ug/L 06/04/17 08:10 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 08:10 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 08:10 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 08:10 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 08:10 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 08:10 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 08:10 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 08:10 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/17 08:10 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 08:10 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 08:10 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/17 08:10 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 08:10 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 08:10 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 08:10 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 08:10 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 08:10 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/04/17 08:10 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 08:10 110-57-6 L11001.0 1
1,1-Dichloroethane ND ug/L 06/04/17 08:10 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 08:10 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 08:10 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/17 08:10 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 08:10 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 08:10 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Sample:SW-3 Lab ID:92342549001 Collected:05/31/17 00:00 Received:06/01/17 07:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 06/04/17 08:10 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 08:10 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 08:10 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/04/17 08:10 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 08:10 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/04/17 08:10 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 08:10 108-10-11000.33 1
Styrene ND ug/L 06/04/17 08:10 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 08:10 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 08:10 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 08:10 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 08:10 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/04/17 08:10 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 08:10 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 08:10 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 08:10 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 08:10 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 08:10 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 08:10 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/17 08:10 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %06/04/17 08:10 460-00-470-130 1
1,2-Dichloroethane-d4 (S)90 %06/04/17 08:10 17060-07-070-130 1
Toluene-d8 (S)107 %06/04/17 08:10 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Sample:SW-1 Lab ID:92342730001 Collected:06/01/17 10:25 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/14/17 22:06 7440-36-006/04/17 16:406.0 3.9 1
Arsenic ND ug/L 06/14/17 22:06 7440-38-206/04/17 16:4010.0 5.0 1
Barium 26.8J ug/L 06/14/17 22:06 7440-39-306/04/17 16:401002.5 1
Beryllium ND ug/L 06/14/17 22:06 7440-41-706/04/17 16:401.0 0.50 1
Cadmium ND ug/L 06/14/17 22:06 7440-43-906/04/17 16:401.0 0.50 1
Chromium ND ug/L 06/14/17 22:06 7440-47-306/04/17 16:4010.0 2.5 1
Cobalt ND ug/L 06/14/17 22:06 7440-48-406/04/17 16:4010.0 2.5 1
Copper ND ug/L 06/14/17 22:06 7440-50-806/04/17 16:4010.0 2.5 1
Lead ND ug/L 06/14/17 22:06 7439-92-106/04/17 16:4010.0 2.5 1
Nickel ND ug/L 06/14/17 22:06 7440-02-006/04/17 16:4050.0 2.5 1
Selenium ND ug/L 06/14/17 22:06 7782-49-206/04/17 16:4010.0 5.0 1
Silver ND ug/L 06/14/17 22:06 7440-22-406/04/17 16:4010.0 2.5 1
Vanadium ND ug/L 06/14/17 22:06 7440-62-206/04/17 16:4025.0 2.5 1
Zinc ND ug/L 06/14/17 22:06 7440-66-606/04/17 16:4010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/09/17 17:51 7440-28-006/06/17 02:455.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/04/17 11:43 67-64-110010.0 1
Acrylonitrile ND ug/L 06/04/17 11:43 107-13-12001.9 1
Benzene ND ug/L 06/04/17 11:43 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 11:43 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 11:43 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 11:43 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 11:43 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 11:43 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 11:43 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 11:43 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/17 11:43 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 11:43 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 11:43 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/17 11:43 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 11:43 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 11:43 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 11:43 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 11:43 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 11:43 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/04/17 11:43 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 11:43 110-57-6 L11001.0 1
1,1-Dichloroethane ND ug/L 06/04/17 11:43 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 11:43 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 11:43 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/17 11:43 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 11:43 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 11:43 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Sample:SW-1 Lab ID:92342730001 Collected:06/01/17 10:25 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 06/04/17 11:43 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 11:43 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 11:43 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/04/17 11:43 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 11:43 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/04/17 11:43 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 11:43 108-10-11000.33 1
Styrene ND ug/L 06/04/17 11:43 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 11:43 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 11:43 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 11:43 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 11:43 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/04/17 11:43 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 11:43 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 11:43 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 11:43 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 11:43 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 11:43 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 11:43 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/17 11:43 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %06/04/17 11:43 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %06/04/17 11:43 17060-07-070-130 1
Toluene-d8 (S)108 %06/04/17 11:43 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Sample:SW-2 Lab ID:92342730002 Collected:06/01/17 16:00 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/14/17 22:09 7440-36-006/04/17 16:406.0 3.9 1
Arsenic ND ug/L 06/14/17 22:09 7440-38-206/04/17 16:4010.0 5.0 1
Barium 17.0J ug/L 06/14/17 22:09 7440-39-306/04/17 16:401002.5 1
Beryllium ND ug/L 06/14/17 22:09 7440-41-706/04/17 16:401.0 0.50 1
Cadmium ND ug/L 06/14/17 22:09 7440-43-906/04/17 16:401.0 0.50 1
Chromium ND ug/L 06/14/17 22:09 7440-47-306/04/17 16:4010.0 2.5 1
Cobalt 16.8 ug/L 06/14/17 22:09 7440-48-406/04/17 16:4010.0 2.5 1
Copper ND ug/L 06/14/17 22:09 7440-50-806/04/17 16:4010.0 2.5 1
Lead ND ug/L 06/14/17 22:09 7439-92-106/04/17 16:4010.0 2.5 1
Nickel ND ug/L 06/14/17 22:09 7440-02-006/04/17 16:4050.0 2.5 1
Selenium ND ug/L 06/14/17 22:09 7782-49-206/04/17 16:4010.0 5.0 1
Silver ND ug/L 06/14/17 22:09 7440-22-406/04/17 16:4010.0 2.5 1
Vanadium ND ug/L 06/14/17 22:09 7440-62-206/04/17 16:4025.0 2.5 1
Zinc ND ug/L 06/14/17 22:09 7440-66-606/04/17 16:4010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.048J ug/L 06/09/17 20:09 7440-28-006/06/17 02:455.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 13.3J ug/L 06/04/17 12:01 67-64-110010.0 1
Acrylonitrile ND ug/L 06/04/17 12:01 107-13-12001.9 1
Benzene ND ug/L 06/04/17 12:01 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 12:01 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 12:01 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 12:01 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 12:01 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 12:01 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 12:01 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 12:01 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/17 12:01 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 12:01 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 12:01 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/17 12:01 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 12:01 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 12:01 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 12:01 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 12:01 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 12:01 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/04/17 12:01 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 12:01 110-57-6 L11001.0 1
1,1-Dichloroethane ND ug/L 06/04/17 12:01 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 12:01 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 12:01 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 2.4J ug/L 06/04/17 12:01 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 12:01 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 12:01 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Sample:SW-2 Lab ID:92342730002 Collected:06/01/17 16:00 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 06/04/17 12:01 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 12:01 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 12:01 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/04/17 12:01 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 12:01 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/04/17 12:01 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 12:01 108-10-11000.33 1
Styrene ND ug/L 06/04/17 12:01 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 12:01 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 12:01 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 12:01 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 12:01 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/04/17 12:01 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 12:01 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 12:01 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 12:01 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 12:01 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 12:01 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 12:01 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/17 12:01 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)108 %06/04/17 12:01 460-00-470-130 1
1,2-Dichloroethane-d4 (S)90 %06/04/17 12:01 17060-07-070-130 1
Toluene-d8 (S)108 %06/04/17 12:01 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Sample:SW-4 Lab ID:92342730004 Collected:06/01/17 10:35 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/14/17 22:12 7440-36-006/04/17 16:406.0 3.9 1
Arsenic ND ug/L 06/14/17 22:12 7440-38-206/04/17 16:4010.0 5.0 1
Barium 22.0J ug/L 06/14/17 22:12 7440-39-306/04/17 16:401002.5 1
Beryllium ND ug/L 06/14/17 22:12 7440-41-706/04/17 16:401.0 0.50 1
Cadmium ND ug/L 06/14/17 22:12 7440-43-906/04/17 16:401.0 0.50 1
Chromium ND ug/L 06/14/17 22:12 7440-47-306/04/17 16:4010.0 2.5 1
Cobalt ND ug/L 06/14/17 22:12 7440-48-406/04/17 16:4010.0 2.5 1
Copper ND ug/L 06/14/17 22:12 7440-50-806/04/17 16:4010.0 2.5 1
Lead ND ug/L 06/14/17 22:12 7439-92-106/04/17 16:4010.0 2.5 1
Nickel ND ug/L 06/14/17 22:12 7440-02-006/04/17 16:4050.0 2.5 1
Selenium ND ug/L 06/14/17 22:12 7782-49-206/04/17 16:4010.0 5.0 1
Silver ND ug/L 06/14/17 22:12 7440-22-406/04/17 16:4010.0 2.5 1
Vanadium ND ug/L 06/14/17 22:12 7440-62-206/04/17 16:4025.0 2.5 1
Zinc 7.0J ug/L 06/14/17 22:12 7440-66-606/04/17 16:4010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.054J ug/L 06/09/17 20:14 7440-28-006/06/17 02:455.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 19.3J ug/L 06/04/17 12:19 67-64-110010.0 1
Acrylonitrile ND ug/L 06/04/17 12:19 107-13-12001.9 1
Benzene ND ug/L 06/04/17 12:19 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 12:19 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 12:19 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 12:19 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 12:19 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 12:19 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 12:19 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 12:19 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/17 12:19 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 12:19 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 12:19 67-66-35.0 0.14 1
Chloromethane 0.13J ug/L 06/04/17 12:19 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 12:19 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 12:19 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 12:19 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 12:19 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 12:19 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/04/17 12:19 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 12:19 110-57-6 L11001.0 1
1,1-Dichloroethane ND ug/L 06/04/17 12:19 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 12:19 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 12:19 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/17 12:19 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 12:19 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 12:19 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Sample:SW-4 Lab ID:92342730004 Collected:06/01/17 10:35 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 06/04/17 12:19 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 12:19 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 12:19 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/04/17 12:19 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 12:19 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/04/17 12:19 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 12:19 108-10-11000.33 1
Styrene ND ug/L 06/04/17 12:19 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 12:19 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 12:19 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 12:19 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 12:19 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/04/17 12:19 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 12:19 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 12:19 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 12:19 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 12:19 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 12:19 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 12:19 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/17 12:19 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)104 %06/04/17 12:19 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %06/04/17 12:19 17060-07-070-130 1
Toluene-d8 (S)108 %06/04/17 12:19 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Sample:SWN-1 Lab ID:92342730005 Collected:06/01/17 11:00 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/14/17 22:24 7440-36-006/04/17 16:406.0 3.9 1
Arsenic ND ug/L 06/14/17 22:24 7440-38-206/04/17 16:4010.0 5.0 1
Barium 21.3J ug/L 06/14/17 22:24 7440-39-306/04/17 16:401002.5 1
Beryllium ND ug/L 06/14/17 22:24 7440-41-706/04/17 16:401.0 0.50 1
Cadmium ND ug/L 06/14/17 22:24 7440-43-906/04/17 16:401.0 0.50 1
Chromium ND ug/L 06/14/17 22:24 7440-47-306/04/17 16:4010.0 2.5 1
Cobalt ND ug/L 06/14/17 22:24 7440-48-406/04/17 16:4010.0 2.5 1
Copper ND ug/L 06/14/17 22:24 7440-50-806/04/17 16:4010.0 2.5 1
Lead ND ug/L 06/14/17 22:24 7439-92-106/04/17 16:4010.0 2.5 1
Nickel ND ug/L 06/14/17 22:24 7440-02-006/04/17 16:4050.0 2.5 1
Selenium ND ug/L 06/14/17 22:24 7782-49-206/04/17 16:4010.0 5.0 1
Silver ND ug/L 06/14/17 22:24 7440-22-406/04/17 16:4010.0 2.5 1
Vanadium ND ug/L 06/14/17 22:24 7440-62-206/04/17 16:4025.0 2.5 1
Zinc 9.1J ug/L 06/14/17 22:24 7440-66-606/04/17 16:4010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/09/17 20:16 7440-28-006/06/17 02:455.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/04/17 12:37 67-64-110010.0 1
Acrylonitrile ND ug/L 06/04/17 12:37 107-13-12001.9 1
Benzene ND ug/L 06/04/17 12:37 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 12:37 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 12:37 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 12:37 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 12:37 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 12:37 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 12:37 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 12:37 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/17 12:37 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 12:37 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 12:37 67-66-35.0 0.14 1
Chloromethane 0.13J ug/L 06/04/17 12:37 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 12:37 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 12:37 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 12:37 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 12:37 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 12:37 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/04/17 12:37 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 12:37 110-57-6 L11001.0 1
1,1-Dichloroethane ND ug/L 06/04/17 12:37 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 12:37 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 12:37 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/17 12:37 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 12:37 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 12:37 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Sample:SWN-1 Lab ID:92342730005 Collected:06/01/17 11:00 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 06/04/17 12:37 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 12:37 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 12:37 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/04/17 12:37 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 12:37 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/04/17 12:37 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 12:37 108-10-11000.33 1
Styrene ND ug/L 06/04/17 12:37 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 12:37 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 12:37 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 12:37 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 12:37 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/04/17 12:37 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 12:37 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 12:37 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 12:37 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 12:37 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 12:37 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 12:37 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/17 12:37 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %06/04/17 12:37 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %06/04/17 12:37 17060-07-070-130 1
Toluene-d8 (S)109 %06/04/17 12:37 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Sample:SWN-2 Lab ID:92342730006 Collected:06/01/17 14:00 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/14/17 22:28 7440-36-006/04/17 16:406.0 3.9 1
Arsenic ND ug/L 06/14/17 22:28 7440-38-206/04/17 16:4010.0 5.0 1
Barium 20.4J ug/L 06/14/17 22:28 7440-39-306/04/17 16:401002.5 1
Beryllium ND ug/L 06/14/17 22:28 7440-41-706/04/17 16:401.0 0.50 1
Cadmium ND ug/L 06/14/17 22:28 7440-43-906/04/17 16:401.0 0.50 1
Chromium ND ug/L 06/14/17 22:28 7440-47-306/04/17 16:4010.0 2.5 1
Cobalt ND ug/L 06/14/17 22:28 7440-48-406/04/17 16:4010.0 2.5 1
Copper ND ug/L 06/14/17 22:28 7440-50-806/04/17 16:4010.0 2.5 1
Lead ND ug/L 06/14/17 22:28 7439-92-106/04/17 16:4010.0 2.5 1
Nickel ND ug/L 06/14/17 22:28 7440-02-006/04/17 16:4050.0 2.5 1
Selenium ND ug/L 06/14/17 22:28 7782-49-206/04/17 16:4010.0 5.0 1
Silver ND ug/L 06/14/17 22:28 7440-22-406/04/17 16:4010.0 2.5 1
Vanadium 2.8J ug/L 06/14/17 22:28 7440-62-206/04/17 16:4025.0 2.5 1
Zinc 5.4J ug/L 06/14/17 22:28 7440-66-606/04/17 16:4010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/09/17 20:18 7440-28-006/06/17 02:455.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 11.6J ug/L 06/04/17 12:55 67-64-110010.0 1
Acrylonitrile ND ug/L 06/04/17 12:55 107-13-12001.9 1
Benzene ND ug/L 06/04/17 12:55 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 12:55 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 12:55 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 12:55 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 12:55 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 12:55 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 12:55 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 12:55 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/17 12:55 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 12:55 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 12:55 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/17 12:55 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 12:55 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 12:55 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 12:55 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 12:55 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 12:55 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/04/17 12:55 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 12:55 110-57-6 L1,M01001.0 1
1,1-Dichloroethane ND ug/L 06/04/17 12:55 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 12:55 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 12:55 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/17 12:55 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 12:55 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 12:55 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Sample:SWN-2 Lab ID:92342730006 Collected:06/01/17 14:00 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 06/04/17 12:55 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 12:55 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 12:55 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/04/17 12:55 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 12:55 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/04/17 12:55 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 12:55 108-10-11000.33 1
Styrene ND ug/L 06/04/17 12:55 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 12:55 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 12:55 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 12:55 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 12:55 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/04/17 12:55 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 12:55 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 12:55 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 12:55 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 12:55 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 12:55 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 12:55 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/17 12:55 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)106 %06/04/17 12:55 460-00-470-130 1
1,2-Dichloroethane-d4 (S)88 %06/04/17 12:55 17060-07-070-130 1
Toluene-d8 (S)123 %06/04/17 12:55 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Sample:SW-A Lab ID:92342730007 Collected:06/01/17 12:10 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 12.2J ug/L 06/04/17 14:24 67-64-110010.0 1
Acrylonitrile ND ug/L 06/04/17 14:24 107-13-12001.9 1
Benzene ND ug/L 06/04/17 14:24 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 14:24 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 14:24 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 14:24 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 14:24 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 14:24 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 14:24 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 14:24 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/17 14:24 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 14:24 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 14:24 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/17 14:24 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 14:24 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 14:24 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 14:24 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 14:24 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 14:24 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/04/17 14:24 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 14:24 110-57-6 L11001.0 1
1,1-Dichloroethane ND ug/L 06/04/17 14:24 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 14:24 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 14:24 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/17 14:24 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 14:24 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 14:24 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 06/04/17 14:24 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 14:24 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 14:24 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/04/17 14:24 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 14:24 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/04/17 14:24 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 14:24 108-10-11000.33 1
Styrene ND ug/L 06/04/17 14:24 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 14:24 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 14:24 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 14:24 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 14:24 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/04/17 14:24 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 14:24 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 14:24 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 14:24 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 14:24 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 14:24 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 14:24 75-01-41.0 0.62 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Sample:SW-A Lab ID:92342730007 Collected:06/01/17 12:10 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Xylene (Total)ND ug/L 06/04/17 14:24 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)105 %06/04/17 14:24 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %06/04/17 14:24 17060-07-070-130 1
Toluene-d8 (S)104 %06/04/17 14:24 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Sample:SW-B Lab ID:92342730008 Collected:06/01/17 12:30 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/04/17 14:42 67-64-110010.0 1
Acrylonitrile ND ug/L 06/04/17 14:42 107-13-12001.9 1
Benzene ND ug/L 06/04/17 14:42 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 14:42 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 14:42 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 14:42 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 14:42 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 14:42 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 14:42 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 14:42 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/17 14:42 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 14:42 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 14:42 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/17 14:42 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 14:42 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 14:42 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 14:42 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 14:42 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 14:42 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 06/04/17 14:42 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 14:42 110-57-6 L11001.0 1
1,1-Dichloroethane ND ug/L 06/04/17 14:42 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 14:42 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 14:42 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/17 14:42 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 14:42 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 14:42 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 06/04/17 14:42 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 14:42 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 14:42 100-41-41.0 0.30 1
2-Hexanone ND ug/L 06/04/17 14:42 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 14:42 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 06/04/17 14:42 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 14:42 108-10-11000.33 1
Styrene ND ug/L 06/04/17 14:42 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 14:42 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 14:42 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 14:42 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 14:42 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 06/04/17 14:42 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 14:42 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 14:42 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 14:42 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 14:42 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 14:42 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 14:42 75-01-41.0 0.62 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
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Page 19 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Sample:SW-B Lab ID:92342730008 Collected:06/01/17 12:30 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Xylene (Total)ND ug/L 06/04/17 14:42 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %06/04/17 14:42 460-00-470-130 1
1,2-Dichloroethane-d4 (S)87 %06/04/17 14:42 17060-07-070-130 1
Toluene-d8 (S)108 %06/04/17 14:42 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363146
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92342549001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2013277
Associated Lab Samples:92342549001
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 5.0 06/09/17 20:333.9
Arsenic ug/L ND 10.0 06/09/17 20:335.0
Barium ug/L ND 5.0 06/09/17 20:332.5
Beryllium ug/L ND 1.0 06/09/17 20:330.50
Cadmium ug/L ND 1.0 06/09/17 20:330.50
Chromium ug/L ND 5.0 06/10/17 16:232.5
Cobalt ug/L ND 5.0 06/09/17 20:332.5
Copper ug/L ND 5.0 06/09/17 20:332.5
Lead ug/L ND 5.0 06/09/17 20:332.5
Nickel ug/L ND 5.0 06/10/17 16:232.5
Selenium ug/L ND 10.0 06/09/17 20:335.0
Silver ug/L ND 5.0 06/09/17 20:332.5
Vanadium ug/L ND 5.0 06/09/17 20:332.5
Zinc ug/L ND 10.0 06/09/17 20:335.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2013278LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 493500 99 80-120
Arsenic ug/L 474500 95 80-120
Barium ug/L 497500 99 80-120
Beryllium ug/L 497500 99 80-120
Cadmium ug/L 496500 99 80-120
Chromium ug/L 494500 99 80-120
Cobalt ug/L 494500 99 80-120
Copper ug/L 496500 99 80-120
Lead ug/L 489500 98 80-120
Nickel ug/L 485500 97 80-120
Selenium ug/L 495500 99 80-120
Silver ug/L 247250 99 80-120
Vanadium ug/L 484500 97 80-120
Zinc ug/L 496500 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2013279MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342472012
2013280
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 98 75-125101 2 20500ND491503
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2013279MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342472012
2013280
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L 500 94 75-12597 2 20500ND472483
Barium ug/L 500 98 75-125102 3 205000.091
mg/L 582 602
Beryllium ug/L 500 99 75-125102 3 20500ND494510
Cadmium ug/L 500 99 75-125101 2 20500ND495506
Chromium ug/L 500 99 75-125102 3 20500ND493508
Cobalt ug/L 500 98 75-125101 2 20500ND492503
Copper ug/L 500 99 75-125101 3 20500ND494508
Lead ug/L 500 97 75-12599 2 20500ND485496
Nickel ug/L 500 97 75-12599 2 205000.016
mg/L 500 510
Selenium ug/L 500 98 75-125101 3 20500ND490507
Silver ug/L 250 99 75-125101 2 20250ND247252
Vanadium ug/L 500 96 75-12599 3 20500ND482495
Zinc ug/L 500 98 75-125101 2 205000.066
mg/L 557 569
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363321
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92342730001, 92342730002, 92342730004, 92342730005, 92342730006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014222
Associated Lab Samples:92342730001, 92342730002, 92342730004, 92342730005, 92342730006
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 5.0 06/14/17 21:193.9
Arsenic ug/L ND 10.0 06/14/17 21:195.0
Barium ug/L ND 5.0 06/14/17 21:192.5
Beryllium ug/L ND 1.0 06/14/17 21:190.50
Cadmium ug/L ND 1.0 06/14/17 21:190.50
Chromium ug/L ND 5.0 06/14/17 21:192.5
Cobalt ug/L ND 5.0 06/14/17 21:192.5
Copper ug/L ND 5.0 06/14/17 21:192.5
Lead ug/L ND 5.0 06/14/17 21:192.5
Nickel ug/L ND 5.0 06/14/17 21:192.5
Selenium ug/L ND 10.0 06/14/17 21:195.0
Silver ug/L ND 5.0 06/14/17 21:192.5
Vanadium ug/L ND 5.0 06/14/17 21:192.5
Zinc ug/L ND 10.0 06/14/17 21:195.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014223LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 496500 99 80-120
Arsenic ug/L 475500 95 80-120
Barium ug/L 511500 102 80-120
Beryllium ug/L 457500 91 80-120
Cadmium ug/L 512500 102 80-120
Chromium ug/L 463500 93 80-120
Cobalt ug/L 498500 100 80-120
Copper ug/L 494500 99 80-120
Lead ug/L 486500 97 80-120
Nickel ug/L 463500 93 80-120
Selenium ug/L 501500 100 80-120
Silver ug/L 235250 94 80-120
Vanadium ug/L 456500 91 80-120
Zinc ug/L 472500 94 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014224MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342605016
2014225
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 103 75-125100 3 20500ND517501
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014224MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342605016
2014225
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L 500 100 75-12597 2 20500174672657
Barium ug/L 500 108 75-125104 3 205008.0 546 530
Beryllium ug/L 500 96 75-12594 2 205000.73J 481 471
Cadmium ug/L 500 108 75-125105 3 205001.7 540 524
Chromium ug/L 500 97 75-12594 3 20500ND486470
Cobalt ug/L 500 104 75-125100 3 2050075.0 594 577
Copper ug/L 500 104 75-125102 3 20500ND522509
Lead ug/L 500 100 75-12597 3 205004.4J 506 491
Nickel ug/L 500 96 75-12593 3 205003.2J 481 466
Selenium ug/L 500 102 75-125100 2 20500ND511501
Silver ug/L 250 99 75-12595 4 20250ND246238
Vanadium ug/L 500 96 75-12593 3 20500ND482466
Zinc ug/L 500 98 75-12595 3 205005.8J 495 479
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363478
EPA 3010A
EPA 6020B
6020 MET
Associated Lab Samples:92342549001, 92342730001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2015139
Associated Lab Samples:92342549001, 92342730001
Matrix:Water
AnalyzedMDL
Thallium ug/L ND 0.10 06/09/17 16:550.020
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2015140LABORATORY CONTROL SAMPLE:
LCSSpike
Thallium ug/L 90.8100 91 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015141MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342795001
2015142
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Thallium ug/L 100 92 75-12596 4 201000.090J 91.9 96.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363479
EPA 3010A
EPA 6020B
6020 MET
Associated Lab Samples:92342730002, 92342730004, 92342730005, 92342730006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2015143
Associated Lab Samples:92342730002, 92342730004, 92342730005, 92342730006
Matrix:Water
AnalyzedMDL
Thallium ug/L ND 0.10 06/09/17 20:050.020
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2015144LABORATORY CONTROL SAMPLE:
LCSSpike
Thallium ug/L 93.7100 94 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015145MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342730002
2015146
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Thallium ug/L 100 94 75-12595 0 201000.048J 94.4 94.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363307
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92342549001, 92342730001, 92342730002, 92342730004, 92342730005, 92342730006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014180
Associated Lab Samples:92342549001, 92342730001, 92342730002, 92342730004, 92342730005, 92342730006
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/04/17 06:410.33
1,1,1-Trichloroethane ug/L ND 1.0 06/04/17 06:410.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 06/04/17 06:410.40
1,1,2-Trichloroethane ug/L ND 1.0 06/04/17 06:410.29
1,1-Dichloroethane ug/L ND 5.0 06/04/17 06:410.32
1,1-Dichloroethene ug/L ND 5.0 06/04/17 06:410.56
1,2,3-Trichloropropane ug/L ND 1.0 06/04/17 06:410.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 06/04/17 06:412.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/04/17 06:410.27
1,2-Dichlorobenzene ug/L ND 5.0 06/04/17 06:410.30
1,2-Dichloroethane ug/L ND 1.0 06/04/17 06:410.24
1,2-Dichloropropane ug/L ND 1.0 06/04/17 06:410.27
1,4-Dichlorobenzene ug/L ND 1.0 06/04/17 06:410.33
2-Butanone (MEK)ug/L ND 100 06/04/17 06:410.96
2-Hexanone ug/L ND 50.0 06/04/17 06:410.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 06/04/17 06:410.33
Acetone ug/L ND 100 06/04/17 06:4110.0
Acrylonitrile ug/L ND 200 06/04/17 06:411.9
Benzene ug/L ND 1.0 06/04/17 06:410.25
Bromochloromethane ug/L ND 3.0 06/04/17 06:410.17
Bromodichloromethane ug/L ND 1.0 06/04/17 06:410.18
Bromoform ug/L ND 3.0 06/04/17 06:410.26
Bromomethane ug/L ND 10.0 06/04/17 06:410.29
Carbon disulfide ug/L ND 100 06/04/17 06:411.2
Carbon tetrachloride ug/L ND 1.0 06/04/17 06:410.25
Chlorobenzene ug/L ND 3.0 06/04/17 06:410.23
Chloroethane ug/L ND 10.0 06/04/17 06:410.54
Chloroform ug/L ND 5.0 06/04/17 06:410.14
Chloromethane ug/L ND 1.0 06/04/17 06:410.11
cis-1,2-Dichloroethene ug/L ND 5.0 06/04/17 06:410.19
cis-1,3-Dichloropropene ug/L ND 1.0 06/04/17 06:410.13
Dibromochloromethane ug/L ND 3.0 06/04/17 06:410.21
Dibromomethane ug/L ND 10.0 06/04/17 06:410.21
Ethylbenzene ug/L ND 1.0 06/04/17 06:410.30
Iodomethane ug/L ND 10.0 06/04/17 06:410.32
Methylene Chloride ug/L ND 1.0 06/04/17 06:410.97
Styrene ug/L ND 1.0 06/04/17 06:410.26
Tetrachloroethene ug/L ND 1.0 06/04/17 06:410.46
Toluene ug/L ND 1.0 06/04/17 06:410.26
trans-1,2-Dichloroethene ug/L ND 5.0 06/04/17 06:410.49
trans-1,3-Dichloropropene ug/L ND 1.0 06/04/17 06:410.26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014180
Associated Lab Samples:92342549001, 92342730001, 92342730002, 92342730004, 92342730005, 92342730006
Matrix:Water
AnalyzedMDL
trans-1,4-Dichloro-2-butene ug/L ND 100 06/04/17 06:411.0
Trichloroethene ug/L ND 1.0 06/04/17 06:410.47
Trichlorofluoromethane ug/L ND 1.0 06/04/17 06:410.20
Vinyl acetate ug/L ND 50.0 06/04/17 06:410.35
Vinyl chloride ug/L ND 1.0 06/04/17 06:410.62
Xylene (Total)ug/L ND 5.0 06/04/17 06:410.66
1,2-Dichloroethane-d4 (S)%89 70-130 06/04/17 06:41
4-Bromofluorobenzene (S)%113 70-130 06/04/17 06:41
Toluene-d8 (S)%106 70-130 06/04/17 06:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014181LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.150 100 80-125
1,1,1-Trichloroethane ug/L 48.850 98 71-129
1,1,2,2-Tetrachloroethane ug/L 57.050 114 79-124
1,1,2-Trichloroethane ug/L 51.150 102 85-125
1,1-Dichloroethane ug/L 49.950 100 73-126
1,1-Dichloroethene ug/L 44.750 89 66-135
1,2,3-Trichloropropane ug/L 47.350 95 75-130
1,2-Dibromo-3-chloropropane ug/L 48.750 97 71-133
1,2-Dibromoethane (EDB)ug/L 56.350 113 83-124
1,2-Dichlorobenzene ug/L 50.950 102 80-133
1,2-Dichloroethane ug/L 45.750 91 67-128
1,2-Dichloropropane ug/L 54.450 109 75-132
1,4-Dichlorobenzene ug/L 47.750 95 78-130
2-Butanone (MEK)ug/L 136100 136 61-144
2-Hexanone ug/L 110100 110 68-143
4-Methyl-2-pentanone (MIBK)ug/L 109100 109 72-135
Acetone ug/L 116100 116 48-146
Acrylonitrile ug/L 274250 110 40-160
Benzene ug/L 52.550 105 80-125
Bromochloromethane ug/L 47.850 96 71-125
Bromodichloromethane ug/L 49.350 99 78-124
Bromoform ug/L 48.150 96 71-128
Bromomethane ug/L 41.950 84 40-160
Carbon disulfide ug/L 50.8J50 102 50-160
Carbon tetrachloride ug/L 44.550 89 69-131
Chlorobenzene ug/L 51.450 103 81-122
Chloroethane ug/L 43.750 87 39-148
Chloroform ug/L 48.350 97 73-127
Chloromethane ug/L 53.850 108 44-146
cis-1,2-Dichloroethene ug/L 51.050 102 74-124
cis-1,3-Dichloropropene ug/L 53.850 108 72-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014181LABORATORY CONTROL SAMPLE:
LCSSpike
Dibromochloromethane ug/L 47.750 95 78-125
Dibromomethane ug/L 48.550 97 82-120
Ethylbenzene ug/L 50.350 101 79-121
Iodomethane ug/L 95.3100 95 39-154
Methylene Chloride ug/L 49.950 100 64-133
Styrene ug/L 49.750 99 84-126
Tetrachloroethene ug/L 45.950 92 78-122
Toluene ug/L 49.650 99 80-121
trans-1,2-Dichloroethene ug/L 51.450 103 71-127
trans-1,3-Dichloropropene ug/L 53.350 107 69-141
trans-1,4-Dichloro-2-butene ug/L 94.0J L15018840-160
Trichloroethene ug/L 50.650 101 78-122
Trichlorofluoromethane ug/L 45.050 90 53-137
Vinyl acetate ug/L 96.4100 96 40-160
Vinyl chloride ug/L 45.150 90 58-137
Xylene (Total)ug/L 141150 94 81-126
1,2-Dichloroethane-d4 (S)%90 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2014183MATRIX SPIKE SAMPLE:
MSSpike
Result
92342730006
1,1,1,2-Tetrachloroethane ug/L 19.120 96 70-130ND
1,1,1-Trichloroethane ug/L 22.520 112 70-130ND
1,1,2,2-Tetrachloroethane ug/L 22.020 110 70-130ND
1,1,2-Trichloroethane ug/L 20.120 100 70-130ND
1,1-Dichloroethane ug/L 22.320 112 70-130ND
1,1-Dichloroethene ug/L 23.020 115 70-166ND
1,2,3-Trichloropropane ug/L 18.120 90 70-130ND
1,2-Dibromo-3-chloropropane ug/L 18.920 94 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.120 106 70-130ND
1,2-Dichlorobenzene ug/L 21.220 106 70-130ND
1,2-Dichloroethane ug/L 20.320 101 70-130ND
1,2-Dichloropropane ug/L 22.920 115 70-130ND
1,4-Dichlorobenzene ug/L 20.220 101 70-130ND
2-Butanone (MEK)ug/L 46.6J40 116 70-130ND
2-Hexanone ug/L 44.9J40 112 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 42.0J40 105 70-130ND
Acetone ug/L 49.1J40 94 70-13011.6J
Acrylonitrile ug/L 113J100 113 70-130ND
Benzene ug/L 23.220 116 70-148ND
Bromochloromethane ug/L 20.920 105 70-130ND
Bromodichloromethane ug/L 21.320 106 70-130ND
Bromoform ug/L 17.320 86 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2014183MATRIX SPIKE SAMPLE:
MSSpike
Result
92342730006
Bromomethane ug/L 22.420 112 70-130ND
Carbon disulfide ug/L 23.6J20 118 70-130ND
Carbon tetrachloride ug/L 21.020 105 70-130ND
Chlorobenzene ug/L 22.020 110 70-146ND
Chloroethane ug/L 20.920 104 70-130ND
Chloroform ug/L 22.820 114 70-130ND
Chloromethane ug/L 24.620 123 70-130ND
cis-1,2-Dichloroethene ug/L 22.820 114 70-130ND
cis-1,3-Dichloropropene ug/L 22.420 112 70-130ND
Dibromochloromethane ug/L 19.520 98 70-130ND
Dibromomethane ug/L 21.820 109 70-130ND
Ethylbenzene ug/L 22.320 112 70-130ND
Iodomethane ug/L 41.240 103 70-130ND
Methylene Chloride ug/L 21.820 109 70-130ND
Styrene ug/L 20.920 104 70-130ND
Tetrachloroethene ug/L 20.820 104 70-130ND
Toluene ug/L 22.520 113 70-155ND
trans-1,2-Dichloroethene ug/L 23.920 119 70-130ND
trans-1,3-Dichloropropene ug/L 22.720 114 70-130ND
trans-1,4-Dichloro-2-butene ug/L 28.2J M02014170-130ND
Trichloroethene ug/L 22.520 112 69-151ND
Trichlorofluoromethane ug/L 21.720 109 70-130ND
Vinyl acetate ug/L 40.5J40 101 70-130ND
Vinyl chloride ug/L 21.220 106 70-130ND
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%104 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342730005
2014182SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342730005
2014182SAMPLE DUPLICATE:
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L 13.6J 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L 0.16J 300.13J
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%87 692
4-Bromofluorobenzene (S)%100 2102
Toluene-d8 (S)%108 1109
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363311
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92342730007, 92342730008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014186
Associated Lab Samples:92342730007, 92342730008
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/04/17 06:590.33
1,1,1-Trichloroethane ug/L ND 1.0 06/04/17 06:590.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 06/04/17 06:590.40
1,1,2-Trichloroethane ug/L ND 1.0 06/04/17 06:590.29
1,1-Dichloroethane ug/L ND 5.0 06/04/17 06:590.32
1,1-Dichloroethene ug/L ND 5.0 06/04/17 06:590.56
1,2,3-Trichloropropane ug/L ND 1.0 06/04/17 06:590.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 06/04/17 06:592.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/04/17 06:590.27
1,2-Dichlorobenzene ug/L ND 5.0 06/04/17 06:590.30
1,2-Dichloroethane ug/L ND 1.0 06/04/17 06:590.24
1,2-Dichloropropane ug/L ND 1.0 06/04/17 06:590.27
1,4-Dichlorobenzene ug/L ND 1.0 06/04/17 06:590.33
2-Butanone (MEK)ug/L ND 100 06/04/17 06:590.96
2-Hexanone ug/L ND 50.0 06/04/17 06:590.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 06/04/17 06:590.33
Acetone ug/L ND 100 06/04/17 06:5910.0
Acrylonitrile ug/L ND 200 06/04/17 06:591.9
Benzene ug/L ND 1.0 06/04/17 06:590.25
Bromochloromethane ug/L ND 3.0 06/04/17 06:590.17
Bromodichloromethane ug/L ND 1.0 06/04/17 06:590.18
Bromoform ug/L ND 3.0 06/04/17 06:590.26
Bromomethane ug/L ND 10.0 06/04/17 06:590.29
Carbon disulfide ug/L ND 100 06/04/17 06:591.2
Carbon tetrachloride ug/L ND 1.0 06/04/17 06:590.25
Chlorobenzene ug/L ND 3.0 06/04/17 06:590.23
Chloroethane ug/L ND 10.0 06/04/17 06:590.54
Chloroform ug/L ND 5.0 06/04/17 06:590.14
Chloromethane ug/L ND 1.0 06/04/17 06:590.11
cis-1,2-Dichloroethene ug/L ND 5.0 06/04/17 06:590.19
cis-1,3-Dichloropropene ug/L ND 1.0 06/04/17 06:590.13
Dibromochloromethane ug/L ND 3.0 06/04/17 06:590.21
Dibromomethane ug/L ND 10.0 06/04/17 06:590.21
Ethylbenzene ug/L ND 1.0 06/04/17 06:590.30
Iodomethane ug/L ND 10.0 06/04/17 06:590.32
Methylene Chloride ug/L ND 1.0 06/04/17 06:590.97
Styrene ug/L ND 1.0 06/04/17 06:590.26
Tetrachloroethene ug/L ND 1.0 06/04/17 06:590.46
Toluene ug/L ND 1.0 06/04/17 06:590.26
trans-1,2-Dichloroethene ug/L ND 5.0 06/04/17 06:590.49
trans-1,3-Dichloropropene ug/L ND 1.0 06/04/17 06:590.26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014186
Associated Lab Samples:92342730007, 92342730008
Matrix:Water
AnalyzedMDL
trans-1,4-Dichloro-2-butene ug/L ND 100 06/04/17 06:591.0
Trichloroethene ug/L ND 1.0 06/04/17 06:590.47
Trichlorofluoromethane ug/L ND 1.0 06/04/17 06:590.20
Vinyl acetate ug/L ND 50.0 06/04/17 06:590.35
Vinyl chloride ug/L ND 1.0 06/04/17 06:590.62
Xylene (Total)ug/L ND 5.0 06/04/17 06:590.66
1,2-Dichloroethane-d4 (S)%89 70-130 06/04/17 06:59
4-Bromofluorobenzene (S)%99 70-130 06/04/17 06:59
Toluene-d8 (S)%106 70-130 06/04/17 06:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014187LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.750 99 80-125
1,1,1-Trichloroethane ug/L 50.850 102 71-129
1,1,2,2-Tetrachloroethane ug/L 53.150 106 79-124
1,1,2-Trichloroethane ug/L 51.550 103 85-125
1,1-Dichloroethane ug/L 52.350 105 73-126
1,1-Dichloroethene ug/L 51.650 103 66-135
1,2,3-Trichloropropane ug/L 47.050 94 75-130
1,2-Dibromo-3-chloropropane ug/L 47.350 95 71-133
1,2-Dibromoethane (EDB)ug/L 54.150 108 83-124
1,2-Dichlorobenzene ug/L 48.250 96 80-133
1,2-Dichloroethane ug/L 48.450 97 67-128
1,2-Dichloropropane ug/L 52.750 105 75-132
1,4-Dichlorobenzene ug/L 45.650 91 78-130
2-Butanone (MEK)ug/L 138100 138 61-144
2-Hexanone ug/L 108100 108 68-143
4-Methyl-2-pentanone (MIBK)ug/L 107100 107 72-135
Acetone ug/L 123100 123 48-146
Acrylonitrile ug/L 286250 114 40-160
Benzene ug/L 52.550 105 80-125
Bromochloromethane ug/L 48.350 97 71-125
Bromodichloromethane ug/L 48.550 97 78-124
Bromoform ug/L 48.550 97 71-128
Bromomethane ug/L 44.850 90 40-160
Carbon disulfide ug/L 52.8J50 106 50-160
Carbon tetrachloride ug/L 44.250 88 69-131
Chlorobenzene ug/L 49.950 100 81-122
Chloroethane ug/L 43.650 87 39-148
Chloroform ug/L 52.250 104 73-127
Chloromethane ug/L 58.150 116 44-146
cis-1,2-Dichloroethene ug/L 54.050 108 74-124
cis-1,3-Dichloropropene ug/L 52.450 105 72-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014187LABORATORY CONTROL SAMPLE:
LCSSpike
Dibromochloromethane ug/L 48.750 97 78-125
Dibromomethane ug/L 46.050 92 82-120
Ethylbenzene ug/L 48.050 96 79-121
Iodomethane ug/L 95.1100 95 39-154
Methylene Chloride ug/L 53.350 107 64-133
Styrene ug/L 48.350 97 84-126
Tetrachloroethene ug/L 47.950 96 78-122
Toluene ug/L 48.350 97 80-121
trans-1,2-Dichloroethene ug/L 53.850 108 71-127
trans-1,3-Dichloropropene ug/L 51.450 103 69-141
trans-1,4-Dichloro-2-butene ug/L 99.7J L15019940-160
Trichloroethene ug/L 49.550 99 78-122
Trichlorofluoromethane ug/L 46.550 93 53-137
Vinyl acetate ug/L 103100 103 40-160
Vinyl chloride ug/L 46.950 94 58-137
Xylene (Total)ug/L 141150 94 81-126
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%95 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2014189MATRIX SPIKE SAMPLE:
MSSpike
Result
92342784004
1,1,1,2-Tetrachloroethane ug/L 19.220 96 70-130ND
1,1,1-Trichloroethane ug/L 22.820 114 70-130ND
1,1,2,2-Tetrachloroethane ug/L 21.320 106 70-130ND
1,1,2-Trichloroethane ug/L 21.120 105 70-130ND
1,1-Dichloroethane ug/L 24.120 120 70-130ND
1,1-Dichloroethene ug/L 24.120 120 70-166ND
1,2,3-Trichloropropane ug/L 20.320 102 70-130ND
1,2-Dibromo-3-chloropropane ug/L 19.720 99 70-130ND
1,2-Dibromoethane (EDB)ug/L 20.620 103 70-130ND
1,2-Dichlorobenzene ug/L 22.020 110 70-130ND
1,2-Dichloroethane ug/L 20.720 104 70-130ND
1,2-Dichloropropane ug/L 22.820 114 70-130ND
1,4-Dichlorobenzene ug/L 21.820 109 70-130ND
2-Butanone (MEK)ug/L 46.8J40 117 70-130ND
2-Hexanone ug/L 41.2J40 103 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 42.3J40 106 70-130ND
Acetone ug/L 49.1J40 90 70-13012.9J
Acrylonitrile ug/L 111J100 111 70-130ND
Benzene ug/L 23.720 119 70-148ND
Bromochloromethane ug/L 21.920 109 70-130ND
Bromodichloromethane ug/L 22.420 112 70-130ND
Bromoform ug/L 17.720 88 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2014189MATRIX SPIKE SAMPLE:
MSSpike
Result
92342784004
Bromomethane ug/L 23.220 116 70-130ND
Carbon disulfide ug/L 24.5J20 123 70-130ND
Carbon tetrachloride ug/L 21.220 106 70-130ND
Chlorobenzene ug/L 22.520 112 70-146ND
Chloroethane ug/L 18.920 94 70-130ND
Chloroform ug/L 22.320 111 70-130ND
Chloromethane ug/L 24.420 121 70-1300.14J
cis-1,2-Dichloroethene ug/L 24.820 123 70-1300.22J
cis-1,3-Dichloropropene ug/L 22.520 113 70-130ND
Dibromochloromethane ug/L 19.220 96 70-130ND
Dibromomethane ug/L 21.320 107 70-130ND
Ethylbenzene ug/L 22.220 111 70-130ND
Iodomethane ug/L 44.240 110 70-130ND
Methylene Chloride ug/L 22.620 113 70-130ND
Styrene ug/L 21.320 107 70-130ND
Tetrachloroethene ug/L 20.720 103 70-130ND
Toluene ug/L 22.220 111 70-155ND
trans-1,2-Dichloroethene ug/L 23.720 118 70-130ND
trans-1,3-Dichloropropene ug/L 22.020 110 70-130ND
trans-1,4-Dichloro-2-butene ug/L 24.7J20 124 70-130ND
Trichloroethene ug/L 23.520 117 69-151ND
Trichlorofluoromethane ug/L 22.520 112 70-130ND
Vinyl acetate ug/L 38.6J40 96 70-130ND
Vinyl chloride ug/L 21.520 107 70-130ND
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%94 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342784003
2014188SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 0.35J 300.37J
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L 0.86J 30ND
1,4-Dichlorobenzene ug/L 2.4 5 302.5
2-Butanone (MEK)ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342784003
2014188SAMPLE DUPLICATE:
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L 13.9J 3021.4J
Acrylonitrile ug/L ND 30ND
Benzene ug/L 0.52J 300.62J
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L 0.97J 300.87J
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L 0.11J 30ND
cis-1,2-Dichloroethene ug/L 1.0J 3 301.0J
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L 0.91J 300.88J
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%90 090
4-Bromofluorobenzene (S)%98 299
Toluene-d8 (S)%105 3108
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 36 of 44
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 37 of 44
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92342549
SURRY MSWLF SWS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92342549001 363146 364135SW-3 EPA 3010A EPA 6010
92342730001 363321 364621SW-1 EPA 3010A EPA 6010
92342730002 363321 364621SW-2 EPA 3010A EPA 6010
92342730004 363321 364621SW-4 EPA 3010A EPA 6010
92342730005 363321 364621SWN-1 EPA 3010A EPA 6010
92342730006 363321 364621SWN-2 EPA 3010A EPA 6010
92342549001 363478 363771SW-3 EPA 3010A EPA 6020B
92342730001 363478 363771SW-1 EPA 3010A EPA 6020B
92342730002 363479 363773SW-2 EPA 3010A EPA 6020B
92342730004 363479 363773SW-4 EPA 3010A EPA 6020B
92342730005 363479 363773SWN-1 EPA 3010A EPA 6020B
92342730006 363479 363773SWN-2 EPA 3010A EPA 6020B
92342549001 363307SW-3 EPA 8260
92342730001 363307SW-1 EPA 8260
92342730002 363307SW-2 EPA 8260
92342730004 363307SW-4 EPA 8260
92342730005 363307SWN-1 EPA 8260
92342730006 363307SWN-2 EPA 8260
92342730007 363311SW-A EPA 8260
92342730008 363311SW-B EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/16/2017 01:32 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 38 of 44
Page 39 of 44
Page 40 of 44
Page 41 of 44
Page 42 of 44
Page 43 of 44
Page 44 of 44
#=CL#
June 15, 2017
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92342727
92342727
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
SURRY BANKS
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on June 02, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 28
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92342727
SURRY BANKS
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 28
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92342727
SURRY BANKS
Lab ID Sample ID Matrix Date Collected Date Received
92342727001 EB Water 06/01/17 18:00 06/02/17 08:00
92342727002 FB Water 06/01/17 17:55 06/02/17 08:00
92342727003 TB Water 06/01/17 00:00 06/02/17 08:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 28
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92342727
SURRY BANKS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92342727001 EB EPA 6010 15 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AWAB
EPA 8260 67 PASI-CGAW
SM 4500-CN-E 1 PASI-AAES2
92342727002 FB EPA 6010 15 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 7470 1 PASI-AWAB
EPA 8260 67 PASI-CGAW
92342727003 TB EPA 8260 67 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 4 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342727
SURRY BANKS
Sample:EB Lab ID:92342727001 Collected:06/01/17 18:00 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/14/17 21:59 7440-36-006/04/17 16:406.0 3.9 1
Arsenic ND ug/L 06/14/17 21:59 7440-38-206/04/17 16:4010.0 5.0 1
Barium ND ug/L 06/14/17 21:59 7440-39-306/04/17 16:401002.5 1
Beryllium ND ug/L 06/14/17 21:59 7440-41-706/04/17 16:401.0 0.50 1
Cadmium ND ug/L 06/14/17 21:59 7440-43-906/04/17 16:401.0 0.50 1
Chromium ND ug/L 06/14/17 21:59 7440-47-306/04/17 16:4010.0 2.5 1
Cobalt ND ug/L 06/14/17 21:59 7440-48-406/04/17 16:4010.0 2.5 1
Copper ND ug/L 06/14/17 21:59 7440-50-806/04/17 16:4010.0 2.5 1
Lead ND ug/L 06/14/17 21:59 7439-92-106/04/17 16:4010.0 2.5 1
Nickel ND ug/L 06/14/17 21:59 7440-02-006/04/17 16:4050.0 2.5 1
Selenium ND ug/L 06/14/17 21:59 7782-49-206/04/17 16:4010.0 5.0 1
Silver ND ug/L 06/14/17 21:59 7440-22-406/04/17 16:4010.0 2.5 1
Tin ND ug/L 06/14/17 21:59 7440-31-506/04/17 16:401002.5 1
Vanadium ND ug/L 06/14/17 21:59 7440-62-206/04/17 16:4025.0 2.5 1
Zinc ND ug/L 06/14/17 21:59 7440-66-606/04/17 16:4010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/09/17 17:47 7440-28-006/06/17 02:455.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/06/17 09:42 7439-97-606/05/17 20:000.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 14.4J ug/L 06/04/17 21:12 67-64-110010.0 1
Acetonitrile ND ug/L 06/04/17 21:12 75-05-855.0 2.2 1
Acrolein ND ug/L 06/04/17 21:12 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 06/04/17 21:12 107-13-12001.9 1
Allyl chloride ND ug/L 06/04/17 21:12 107-05-110.0 1.5 1
Benzene ND ug/L 06/04/17 21:12 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 21:12 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 21:12 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 21:12 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 21:12 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 21:12 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 21:12 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 21:12 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/17 21:12 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 21:12 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 21:12 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/17 21:12 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/04/17 21:12 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 21:12 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 21:12 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 21:12 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 21:12 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 21:12 95-50-15.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
Pace Analytical Services, LLC
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Page 5 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342727
SURRY BANKS
Sample:EB Lab ID:92342727001 Collected:06/01/17 18:00 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,3-Dichlorobenzene ND ug/L 06/04/17 21:12 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/04/17 21:12 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 21:12 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/04/17 21:12 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/04/17 21:12 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 21:12 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 21:12 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/17 21:12 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 21:12 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 21:12 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/04/17 21:12 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/04/17 21:12 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/04/17 21:12 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/04/17 21:12 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 21:12 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 21:12 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/04/17 21:12 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/04/17 21:12 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/04/17 21:12 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 21:12 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/04/17 21:12 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/04/17 21:12 126-98-71000.93 1
Methylene Chloride ND ug/L 06/04/17 21:12 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/04/17 21:12 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 21:12 108-10-11000.33 1
Naphthalene ND ug/L 06/04/17 21:12 91-20-310.0 0.24 1
Propionitrile ND ug/L 06/04/17 21:12 107-12-01503.6 1
Styrene ND ug/L 06/04/17 21:12 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 21:12 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 21:12 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 21:12 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 21:12 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/04/17 21:12 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/04/17 21:12 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 21:12 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 21:12 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 21:12 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 21:12 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 21:12 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 21:12 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/17 21:12 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)109 %06/04/17 21:12 460-00-470-130 1
1,2-Dichloroethane-d4 (S)87 %06/04/17 21:12 17060-07-070-130 1
Toluene-d8 (S)106 %06/04/17 21:12 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
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Page 6 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342727
SURRY BANKS
Sample:EB Lab ID:92342727001 Collected:06/01/17 18:00 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 4500-CN-E4500CNE Cyanide, Total
Cyanide ND ug/L 06/07/17 13:50 57-12-510.0 4.0 1
REPORT OF LABORATORY ANALYSIS
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Page 7 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342727
SURRY BANKS
Sample:FB Lab ID:92342727002 Collected:06/01/17 17:55 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 06/14/17 22:03 7440-36-006/04/17 16:406.0 3.9 1
Arsenic ND ug/L 06/14/17 22:03 7440-38-206/04/17 16:4010.0 5.0 1
Barium ND ug/L 06/14/17 22:03 7440-39-306/04/17 16:401002.5 1
Beryllium ND ug/L 06/14/17 22:03 7440-41-706/04/17 16:401.0 0.50 1
Cadmium ND ug/L 06/14/17 22:03 7440-43-906/04/17 16:401.0 0.50 1
Chromium ND ug/L 06/14/17 22:03 7440-47-306/04/17 16:4010.0 2.5 1
Cobalt ND ug/L 06/14/17 22:03 7440-48-406/04/17 16:4010.0 2.5 1
Copper ND ug/L 06/14/17 22:03 7440-50-806/04/17 16:4010.0 2.5 1
Lead ND ug/L 06/14/17 22:03 7439-92-106/04/17 16:4010.0 2.5 1
Nickel ND ug/L 06/14/17 22:03 7440-02-006/04/17 16:4050.0 2.5 1
Selenium ND ug/L 06/14/17 22:03 7782-49-206/04/17 16:4010.0 5.0 1
Silver ND ug/L 06/14/17 22:03 7440-22-406/04/17 16:4010.0 2.5 1
Tin ND ug/L 06/14/17 22:03 7440-31-506/04/17 16:401002.5 1
Vanadium ND ug/L 06/14/17 22:03 7440-62-206/04/17 16:4025.0 2.5 1
Zinc ND ug/L 06/14/17 22:03 7440-66-606/04/17 16:4010.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 06/09/17 17:49 7440-28-006/06/17 02:455.5 0.020 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 06/06/17 09:45 7439-97-606/05/17 20:000.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 10.2J ug/L 06/04/17 21:30 67-64-110010.0 1
Acetonitrile ND ug/L 06/04/17 21:30 75-05-855.0 2.2 1
Acrolein ND ug/L 06/04/17 21:30 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 06/04/17 21:30 107-13-12001.9 1
Allyl chloride ND ug/L 06/04/17 21:30 107-05-110.0 1.5 1
Benzene ND ug/L 06/04/17 21:30 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 21:30 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 21:30 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 21:30 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 21:30 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 21:30 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 21:30 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 21:30 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/17 21:30 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 21:30 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 21:30 67-66-35.0 0.14 1
Chloromethane ND ug/L 06/04/17 21:30 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/04/17 21:30 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 21:30 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 21:30 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 21:30 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 21:30 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 21:30 95-50-15.0 0.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
Pace Analytical Services, LLC
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Page 8 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342727
SURRY BANKS
Sample:FB Lab ID:92342727002 Collected:06/01/17 17:55 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,3-Dichlorobenzene ND ug/L 06/04/17 21:30 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/04/17 21:30 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 21:30 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/04/17 21:30 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/04/17 21:30 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 21:30 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 21:30 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/17 21:30 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 21:30 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 21:30 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/04/17 21:30 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/04/17 21:30 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/04/17 21:30 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/04/17 21:30 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 21:30 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 21:30 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/04/17 21:30 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/04/17 21:30 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/04/17 21:30 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 21:30 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/04/17 21:30 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/04/17 21:30 126-98-71000.93 1
Methylene Chloride ND ug/L 06/04/17 21:30 75-09-21.0 0.97 1
Methyl methacrylate ND ug/L 06/04/17 21:30 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 21:30 108-10-11000.33 1
Naphthalene ND ug/L 06/04/17 21:30 91-20-310.0 0.24 1
Propionitrile ND ug/L 06/04/17 21:30 107-12-01503.6 1
Styrene ND ug/L 06/04/17 21:30 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 21:30 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 21:30 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 21:30 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 21:30 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/04/17 21:30 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/04/17 21:30 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 21:30 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 21:30 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 21:30 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 21:30 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 21:30 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 21:30 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/17 21:30 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %06/04/17 21:30 460-00-470-130 1
1,2-Dichloroethane-d4 (S)89 %06/04/17 21:30 17060-07-070-130 1
Toluene-d8 (S)106 %06/04/17 21:30 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 9 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342727
SURRY BANKS
Sample:TB Lab ID:92342727003 Collected:06/01/17 00:00 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 06/04/17 21:48 67-64-110010.0 1
Acetonitrile ND ug/L 06/04/17 21:48 75-05-855.0 2.2 1
Acrolein ND ug/L 06/04/17 21:48 107-02-853.0 1.6 1
Acrylonitrile ND ug/L 06/04/17 21:48 107-13-12001.9 1
Allyl chloride ND ug/L 06/04/17 21:48 107-05-110.0 1.5 1
Benzene ND ug/L 06/04/17 21:48 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 06/04/17 21:48 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 06/04/17 21:48 75-27-41.0 0.18 1
Bromoform ND ug/L 06/04/17 21:48 75-25-23.0 0.26 1
Bromomethane ND ug/L 06/04/17 21:48 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 06/04/17 21:48 78-93-31000.96 1
Carbon disulfide ND ug/L 06/04/17 21:48 75-15-01001.2 1
Carbon tetrachloride ND ug/L 06/04/17 21:48 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 06/04/17 21:48 108-90-73.0 0.23 1
Chloroethane ND ug/L 06/04/17 21:48 75-00-310.0 0.54 1
Chloroform ND ug/L 06/04/17 21:48 67-66-35.0 0.14 1
Chloromethane 0.14J ug/L 06/04/17 21:48 74-87-31.0 0.11 1
Chloroprene ND ug/L 06/04/17 21:48 126-99-820.0 0.27 1
1,2-Dibromo-3-chloropropane ND ug/L 06/04/17 21:48 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 06/04/17 21:48 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 06/04/17 21:48 106-93-41.0 0.27 1
Dibromomethane ND ug/L 06/04/17 21:48 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 06/04/17 21:48 95-50-15.0 0.30 1
1,3-Dichlorobenzene ND ug/L 06/04/17 21:48 541-73-15.0 0.24 1
1,4-Dichlorobenzene ND ug/L 06/04/17 21:48 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 06/04/17 21:48 110-57-61001.0 1
Dichlorodifluoromethane ND ug/L 06/04/17 21:48 75-71-85.0 0.21 1
1,1-Dichloroethane ND ug/L 06/04/17 21:48 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 06/04/17 21:48 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 06/04/17 21:48 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 06/04/17 21:48 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 06/04/17 21:48 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 06/04/17 21:48 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 06/04/17 21:48 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 06/04/17 21:48 594-20-715.0 0.13 1
1,1-Dichloropropene ND ug/L 06/04/17 21:48 563-58-65.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 06/04/17 21:48 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 06/04/17 21:48 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 06/04/17 21:48 100-41-41.0 0.30 1
Ethyl methacrylate ND ug/L 06/04/17 21:48 97-63-210.0 0.20 1
Hexachloro-1,3-butadiene ND ug/L 06/04/17 21:48 87-68-310.0 0.71 1
2-Hexanone ND ug/L 06/04/17 21:48 591-78-650.0 0.46 1
Iodomethane ND ug/L 06/04/17 21:48 74-88-410.0 0.32 1
Isobutanol ND ug/L 06/04/17 21:48 78-83-110035.0 1
Methacrylonitrile ND ug/L 06/04/17 21:48 126-98-71000.93 1
Methylene Chloride ND ug/L 06/04/17 21:48 75-09-21.0 0.97 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92342727
SURRY BANKS
Sample:TB Lab ID:92342727003 Collected:06/01/17 00:00 Received:06/02/17 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Methyl methacrylate ND ug/L 06/04/17 21:48 80-62-630.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/04/17 21:48 108-10-11000.33 1
Naphthalene ND ug/L 06/04/17 21:48 91-20-310.0 0.24 1
Propionitrile ND ug/L 06/04/17 21:48 107-12-01503.6 1
Styrene ND ug/L 06/04/17 21:48 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 06/04/17 21:48 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 06/04/17 21:48 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 06/04/17 21:48 127-18-41.0 0.46 1
Toluene ND ug/L 06/04/17 21:48 108-88-31.0 0.26 1
1,2,4-Trichlorobenzene ND ug/L 06/04/17 21:48 120-82-110.0 0.35 1
1,1,1-Trichloroethane ND ug/L 06/04/17 21:48 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 06/04/17 21:48 79-00-51.0 0.29 1
Trichloroethene ND ug/L 06/04/17 21:48 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 06/04/17 21:48 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 06/04/17 21:48 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 06/04/17 21:48 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 06/04/17 21:48 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 06/04/17 21:48 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %06/04/17 21:48 460-00-470-130 1
1,2-Dichloroethane-d4 (S)89 %06/04/17 21:48 17060-07-070-130 1
Toluene-d8 (S)107 %06/04/17 21:48 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342727
SURRY BANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363459
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92342727001, 92342727002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2015066
Associated Lab Samples:92342727001, 92342727002
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 06/06/17 09:310.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2015067LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.42.5 95 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015068MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342658001
2015069
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L M1,R12.5 93 75-12562 40 252.5ND 2.4 1.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342727
SURRY BANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363321
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92342727001, 92342727002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014222
Associated Lab Samples:92342727001, 92342727002
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 5.0 06/14/17 21:193.9
Arsenic ug/L ND 10.0 06/14/17 21:195.0
Barium ug/L ND 5.0 06/14/17 21:192.5
Beryllium ug/L ND 1.0 06/14/17 21:190.50
Cadmium ug/L ND 1.0 06/14/17 21:190.50
Chromium ug/L ND 5.0 06/14/17 21:192.5
Cobalt ug/L ND 5.0 06/14/17 21:192.5
Copper ug/L ND 5.0 06/14/17 21:192.5
Lead ug/L ND 5.0 06/14/17 21:192.5
Nickel ug/L ND 5.0 06/14/17 21:192.5
Selenium ug/L ND 10.0 06/14/17 21:195.0
Silver ug/L ND 5.0 06/14/17 21:192.5
Tin ug/L ND 5.0 06/14/17 21:192.5
Vanadium ug/L ND 5.0 06/14/17 21:192.5
Zinc ug/L ND 10.0 06/14/17 21:195.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014223LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 496500 99 80-120
Arsenic ug/L 475500 95 80-120
Barium ug/L 511500 102 80-120
Beryllium ug/L 457500 91 80-120
Cadmium ug/L 512500 102 80-120
Chromium ug/L 463500 93 80-120
Cobalt ug/L 498500 100 80-120
Copper ug/L 494500 99 80-120
Lead ug/L 486500 97 80-120
Nickel ug/L 463500 93 80-120
Selenium ug/L 501500 100 80-120
Silver ug/L 235250 94 80-120
Tin ug/L 485500 97 80-120
Vanadium ug/L 456500 91 80-120
Zinc ug/L 472500 94 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342727
SURRY BANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2014224MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342605016
2014225
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 103 75-125100 3 20500ND517501
Arsenic ug/L 500 100 75-12597 2 20500174672657
Barium ug/L 500 108 75-125104 3 205008.0 546 530
Beryllium ug/L 500 96 75-12594 2 205000.73J 481 471
Cadmium ug/L 500 108 75-125105 3 205001.7 540 524
Chromium ug/L 500 97 75-12594 3 20500ND486470
Cobalt ug/L 500 104 75-125100 3 2050075.0 594 577
Copper ug/L 500 104 75-125102 3 20500ND522509
Lead ug/L 500 100 75-12597 3 205004.4J 506 491
Nickel ug/L 500 96 75-12593 3 205003.2J 481 466
Selenium ug/L 500 102 75-125100 2 20500ND511501
Silver ug/L 250 99 75-12595 4 20250ND246238
Tin ug/L 500 101 75-12597 4 20500ND503484
Vanadium ug/L 500 96 75-12593 3 20500ND482466
Zinc ug/L 500 98 75-12595 3 205005.8J 495 479
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342727
SURRY BANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363478
EPA 3010A
EPA 6020B
6020 MET
Associated Lab Samples:92342727001, 92342727002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2015139
Associated Lab Samples:92342727001, 92342727002
Matrix:Water
AnalyzedMDL
Thallium ug/L ND 0.10 06/09/17 16:550.020
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2015140LABORATORY CONTROL SAMPLE:
LCSSpike
Thallium ug/L 90.8100 91 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015141MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342795001
2015142
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Thallium ug/L 100 92 75-12596 4 201000.090J 91.9 96.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342727
SURRY BANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363328
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92342727001, 92342727002, 92342727003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014255
Associated Lab Samples:92342727001, 92342727002, 92342727003
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 06/04/17 20:010.33
1,1,1-Trichloroethane ug/L ND 1.0 06/04/17 20:010.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 06/04/17 20:010.40
1,1,2-Trichloroethane ug/L ND 1.0 06/04/17 20:010.29
1,1-Dichloroethane ug/L ND 5.0 06/04/17 20:010.32
1,1-Dichloroethene ug/L ND 5.0 06/04/17 20:010.56
1,1-Dichloropropene ug/L ND 5.0 06/04/17 20:010.49
1,2,3-Trichloropropane ug/L ND 1.0 06/04/17 20:010.41
1,2,4-Trichlorobenzene ug/L ND 10.0 06/04/17 20:010.35
1,2-Dibromo-3-chloropropane ug/L ND 13.0 06/04/17 20:012.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/04/17 20:010.27
1,2-Dichlorobenzene ug/L ND 5.0 06/04/17 20:010.30
1,2-Dichloroethane ug/L ND 1.0 06/04/17 20:010.24
1,2-Dichloropropane ug/L ND 1.0 06/04/17 20:010.27
1,3-Dichlorobenzene ug/L ND 5.0 06/04/17 20:010.24
1,3-Dichloropropane ug/L ND 1.0 06/04/17 20:010.28
1,4-Dichlorobenzene ug/L ND 1.0 06/04/17 20:010.33
2,2-Dichloropropane ug/L ND 15.0 06/04/17 20:010.13
2-Butanone (MEK)ug/L ND 100 06/04/17 20:010.96
2-Hexanone ug/L ND 50.0 06/04/17 20:010.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 06/04/17 20:010.33
Acetone ug/L ND 100 06/04/17 20:0110.0
Acetonitrile ug/L ND 55.0 06/04/17 20:012.2
Acrolein ug/L ND 53.0 06/04/17 20:011.6
Acrylonitrile ug/L ND 200 06/04/17 20:011.9
Allyl chloride ug/L ND 10.0 06/04/17 20:011.5
Benzene ug/L ND 1.0 06/04/17 20:010.25
Bromochloromethane ug/L ND 3.0 06/04/17 20:010.17
Bromodichloromethane ug/L ND 1.0 06/04/17 20:010.18
Bromoform ug/L ND 3.0 06/04/17 20:010.26
Bromomethane ug/L ND 10.0 06/04/17 20:010.29
Carbon disulfide ug/L ND 100 06/04/17 20:011.2
Carbon tetrachloride ug/L ND 1.0 06/04/17 20:010.25
Chlorobenzene ug/L ND 3.0 06/04/17 20:010.23
Chloroethane ug/L ND 10.0 06/04/17 20:010.54
Chloroform ug/L ND 5.0 06/04/17 20:010.14
Chloromethane ug/L ND 1.0 06/04/17 20:010.11
Chloroprene ug/L ND 20.0 06/04/17 20:010.27
cis-1,2-Dichloroethene ug/L ND 5.0 06/04/17 20:010.19
cis-1,3-Dichloropropene ug/L ND 1.0 06/04/17 20:010.13
Dibromochloromethane ug/L ND 3.0 06/04/17 20:010.21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342727
SURRY BANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2014255
Associated Lab Samples:92342727001, 92342727002, 92342727003
Matrix:Water
AnalyzedMDL
Dibromomethane ug/L ND 10.0 06/04/17 20:010.21
Dichlorodifluoromethane ug/L ND 5.0 06/04/17 20:010.21
Ethyl methacrylate ug/L ND 10.0 06/04/17 20:010.20
Ethylbenzene ug/L ND 1.0 06/04/17 20:010.30
Hexachloro-1,3-butadiene ug/L ND 10.0 06/04/17 20:010.71
Iodomethane ug/L ND 10.0 06/04/17 20:010.32
Isobutanol ug/L ND 100 06/04/17 20:0135.0
Methacrylonitrile ug/L ND 100 06/04/17 20:010.93
Methyl methacrylate ug/L ND 30.0 06/04/17 20:012.0
Methylene Chloride ug/L ND 1.0 06/04/17 20:010.97
Naphthalene ug/L ND 10.0 06/04/17 20:010.24
Propionitrile ug/L ND 150 06/04/17 20:013.6
Styrene ug/L ND 1.0 06/04/17 20:010.26
Tetrachloroethene ug/L ND 1.0 06/04/17 20:010.46
Toluene ug/L ND 1.0 06/04/17 20:010.26
trans-1,2-Dichloroethene ug/L ND 5.0 06/04/17 20:010.49
trans-1,3-Dichloropropene ug/L ND 1.0 06/04/17 20:010.26
trans-1,4-Dichloro-2-butene ug/L ND 100 06/04/17 20:011.0
Trichloroethene ug/L ND 1.0 06/04/17 20:010.47
Trichlorofluoromethane ug/L ND 1.0 06/04/17 20:010.20
Vinyl acetate ug/L ND 50.0 06/04/17 20:010.35
Vinyl chloride ug/L ND 1.0 06/04/17 20:010.62
Xylene (Total)ug/L ND 5.0 06/04/17 20:010.66
1,2-Dichloroethane-d4 (S)%85 70-130 06/04/17 20:01
4-Bromofluorobenzene (S)%100 70-130 06/04/17 20:01
Toluene-d8 (S)%115 70-130 06/04/17 20:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014256LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 46.650 93 80-125
1,1,1-Trichloroethane ug/L 50.750 101 71-129
1,1,2,2-Tetrachloroethane ug/L 49.850 100 79-124
1,1,2-Trichloroethane ug/L 48.950 98 85-125
1,1-Dichloroethane ug/L 49.650 99 73-126
1,1-Dichloroethene ug/L 46.950 94 66-135
1,1-Dichloropropene ug/L 51.950 104 74-135
1,2,3-Trichloropropane ug/L 46.550 93 75-130
1,2,4-Trichlorobenzene ug/L 46.550 93 75-134
1,2-Dibromo-3-chloropropane ug/L 46.750 93 71-133
1,2-Dibromoethane (EDB)ug/L 54.550 109 83-124
1,2-Dichlorobenzene ug/L 47.550 95 80-133
1,2-Dichloroethane ug/L 47.050 94 67-128
1,2-Dichloropropane ug/L 53.450 107 75-132
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
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Page 17 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342727
SURRY BANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014256LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 48.150 96 77-130
1,3-Dichloropropane ug/L 54.150 108 76-131
1,4-Dichlorobenzene ug/L 47.950 96 78-130
2,2-Dichloropropane ug/L 50.750 101 40-160
2-Butanone (MEK)ug/L 126100 126 61-144
2-Hexanone ug/L 101100 101 68-143
4-Methyl-2-pentanone (MIBK)ug/L 94.9J100 95 72-135
Acetone ug/L 115100 115 48-146
Acetonitrile ug/L 525500 105 62-150
Acrolein ug/L 320250 128 24-160
Acrylonitrile ug/L 268250 107 40-160
Allyl chloride ug/L 47.650 95 66-137
Benzene ug/L 52.150 104 80-125
Bromochloromethane ug/L 48.950 98 71-125
Bromodichloromethane ug/L 48.550 97 78-124
Bromoform ug/L 43.150 86 71-128
Bromomethane ug/L 42.150 84 40-160
Carbon disulfide ug/L 49.3J50 99 50-160
Carbon tetrachloride ug/L 45.150 90 69-131
Chlorobenzene ug/L 48.850 98 81-122
Chloroethane ug/L 40.850 82 39-148
Chloroform ug/L 50.950 102 73-127
Chloromethane ug/L 49.950 100 44-146
Chloroprene ug/L 49.350 99 75-145
cis-1,2-Dichloroethene ug/L 52.550 105 74-124
cis-1,3-Dichloropropene ug/L 54.150 108 72-132
Dibromochloromethane ug/L 47.550 95 78-125
Dibromomethane ug/L 44.250 88 82-120
Dichlorodifluoromethane ug/L 41.150 82 34-157
Ethyl methacrylate ug/L 45.750 91 82-121
Ethylbenzene ug/L 50.150 100 79-121
Hexachloro-1,3-butadiene ug/L 43.550 87 72-131
Iodomethane ug/L 91.7100 92 39-154
Isobutanol ug/L 11301000 113 34-160
Methacrylonitrile ug/L 563500 113 74-134
Methyl methacrylate ug/L 43.550 87 84-124
Methylene Chloride ug/L 53.650 107 64-133
Naphthalene ug/L 48.650 97 73-133
Propionitrile ug/L 562500 112 73-140
Styrene ug/L 51.050 102 84-126
Tetrachloroethene ug/L 44.850 90 78-122
Toluene ug/L 46.450 93 80-121
trans-1,2-Dichloroethene ug/L 52.350 105 71-127
trans-1,3-Dichloropropene ug/L 52.450 105 69-141
trans-1,4-Dichloro-2-butene ug/L 68.3J50 137 40-160
Trichloroethene ug/L 50.450 101 78-122
Trichlorofluoromethane ug/L 45.450 91 53-137
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
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Huntersville, NC 28078
[phone]
Page 18 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342727
SURRY BANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2014256LABORATORY CONTROL SAMPLE:
LCSSpike
Vinyl acetate ug/L 99.2100 99 40-160
Vinyl chloride ug/L 41.950 84 58-137
Xylene (Total)ug/L 149150 99 81-126
1,2-Dichloroethane-d4 (S)%103 70-130
4-Bromofluorobenzene (S)%107 70-130
Toluene-d8 (S)%96 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2014258MATRIX SPIKE SAMPLE:
MSSpike
Result
92342478011
1,1,1,2-Tetrachloroethane ug/L 20.020 100 70-130ND
1,1,1-Trichloroethane ug/L 23.020 115 70-130ND
1,1,2,2-Tetrachloroethane ug/L 22.120 110 70-130ND
1,1,2-Trichloroethane ug/L 22.220 111 70-130ND
1,1-Dichloroethane ug/L 23.120 116 70-130ND
1,1-Dichloroethene ug/L 23.020 115 70-166ND
1,1-Dichloropropene ug/L 23.320 116 70-130ND
1,2,3-Trichloropropane ug/L 19.520 98 70-130ND
1,2,4-Trichlorobenzene ug/L 19.320 97 70-130ND
1,2-Dibromo-3-chloropropane ug/L 18.220 91 70-130ND
1,2-Dibromoethane (EDB)ug/L 19.720 99 70-130ND
1,2-Dichlorobenzene ug/L 20.920 105 70-130ND
1,2-Dichloroethane ug/L 21.320 106 70-130ND
1,2-Dichloropropane ug/L 24.120 120 70-130ND
1,3-Dichlorobenzene ug/L 21.720 108 70-130ND
1,3-Dichloropropane ug/L 20.420 102 70-130ND
1,4-Dichlorobenzene ug/L 21.120 105 70-130ND
2,2-Dichloropropane ug/L 21.220 106 70-130ND
2-Butanone (MEK)ug/L 47.7J40 119 70-130ND
2-Hexanone ug/L 40.9J40 102 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 43.2J40 108 70-130ND
Acetone ug/L 93.5J M14019870-13014.4J
Acetonitrile ug/L 219200 110 70-130ND
Acrolein ug/L 117100 117 70-130ND
Acrylonitrile ug/L 114J100 114 70-130ND
Allyl chloride ug/L 26.8 M12013470-130ND
Benzene ug/L 23.420 117 70-148ND
Bromochloromethane ug/L 21.420 107 70-130ND
Bromodichloromethane ug/L 22.420 112 70-130ND
Bromoform ug/L 16.520 83 70-130ND
Bromomethane ug/L 19.820 99 70-130ND
Carbon disulfide ug/L 23.4J20 117 70-130ND
Carbon tetrachloride ug/L 22.420 112 70-130ND
Chlorobenzene ug/L 22.120 110 70-146ND
Chloroethane ug/L 21.720 108 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
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Huntersville, NC 28078
[phone]
Page 19 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342727
SURRY BANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2014258MATRIX SPIKE SAMPLE:
MSSpike
Result
92342478011
Chloroform ug/L 23.220 116 70-130ND
Chloromethane ug/L 25.820 129 70-130ND
Chloroprene ug/L 22.820 114 70-130ND
cis-1,2-Dichloroethene ug/L 24.520 119 70-1300.64J
cis-1,3-Dichloropropene ug/L 23.420 117 70-130ND
Dibromochloromethane ug/L 18.420 92 70-130ND
Dibromomethane ug/L 21.720 108 70-130ND
Dichlorodifluoromethane ug/L 19.220 96 70-130ND
Ethyl methacrylate ug/L 19.420 97 70-130ND
Ethylbenzene ug/L 23.020 115 70-130ND
Hexachloro-1,3-butadiene ug/L 19.320 96 70-130ND
Iodomethane ug/L 41.640 104 70-130ND
Isobutanol ug/L 419400 105 70-130ND
Methacrylonitrile ug/L 230200 115 70-130ND
Methyl methacrylate ug/L 19.7J20 98 70-130ND
Methylene Chloride ug/L 23.220 116 70-130ND
Naphthalene ug/L 21.620 108 70-130ND
Propionitrile ug/L 243200 121 70-130ND
Styrene ug/L 22.320 112 70-130ND
Tetrachloroethene ug/L 19.420 97 70-130ND
Toluene ug/L 22.720 113 70-155ND
trans-1,2-Dichloroethene ug/L 25.020 125 70-130ND
trans-1,3-Dichloropropene ug/L 21.820 109 70-130ND
trans-1,4-Dichloro-2-butene ug/L 21.3J20 106 70-130ND
Trichloroethene ug/L 23.820 119 69-151ND
Trichlorofluoromethane ug/L 22.120 111 70-130ND
Vinyl acetate ug/L 37.6J40 94 70-130ND
Vinyl chloride ug/L 21.820 109 70-130ND
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%109 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342478010
2014257SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 0.50J 300.36J
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342727
SURRY BANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342478010
2014257SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acetonitrile ug/L ND 30ND
Acrolein ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Allyl chloride ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L 0.29J 30ND
Chloroprene ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 0.88J 300.65J
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Ethyl methacrylate ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Isobutanol ug/L ND 30ND
Methacrylonitrile ug/L ND 30ND
Methyl methacrylate ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
Propionitrile ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
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Huntersville, NC 28078
[phone]
Page 21 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342727
SURRY BANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92342478010
2014257SAMPLE DUPLICATE:
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%92 092
4-Bromofluorobenzene (S)%105 2103
Toluene-d8 (S)%108 2109
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92342727
SURRY BANKS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
363513
SM 4500-CN-E
SM 4500-CN-E
4500CNE Cyanide, Total
Associated Lab Samples:92342727001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2015224
Associated Lab Samples:92342727001
Matrix:Water
AnalyzedMDL
Cyanide ug/L ND 10.0 06/07/17 13:524.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2015225LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide ug/L 101100 101 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015226MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342317015
2015227
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L 100 94 80-12091 2 10100ND97.6 95.4
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2015228MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92342712006
2015229
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide ug/L M1,R11002980-12019 27 101000.013
mg/L 41.2 31.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 28
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92342727
SURRY BANKS
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 28
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92342727
SURRY BANKS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92342727001 363321 364621EBEPA 3010A EPA 6010
92342727002 363321 364621FBEPA 3010A EPA 6010
92342727001 363478 363771EBEPA 3010A EPA 6020B
92342727002 363478 363771FBEPA 3010A EPA 6020B
92342727001 363459 363485EBEPA 7470 EPA 7470
92342727002 363459 363485FBEPA 7470 EPA 7470
92342727001 363328EBEPA 8260
92342727002 363328FBEPA 8260
92342727003 363328TBEPA 8260
92342727001 363513EBSM 4500-CN-E
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/15/2017 04:16 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 28
Page 26 of 28
Page 27 of 28
Page 28 of 28
Appendix B
Field Sampling Parameter Data Sheet(s)