9214_HollySpringsCDLF_GWMR_20170714

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July 17, 2017

Mr. Ervin Lane
Compliance Hydrogeologist
NCDENR/Solid Waste Section
1646 Mail Service Center
Raleigh, NC 27699-1646

RE: First Semiannual Water Quality Monitoring Report of 2017
Holly Springs Closed C&D Landfill, Permit No. 92-14
Wake County, North Carolina

Dear Mr. Lane,

Republic Services of North Carolina, LLC is submitting the enclosed First Semiannual Water Quality Monitoring
Report of 2017 in electronic format, plus a hard copy of the original Environmental Monitoring Form. This
report covers the first semiannual compliance monitoring event of 2017 for the Holly Springs C&D Landfill,
Permit No. 92-14, as required by the North Carolina Division of Waste Management, Solid Waste Section.

If you have any questions, please contact Van Burbach with Joyce Engineering at [phone] or me at
[phone].

Sincerely,
Republic Services

Matt Einsmann, P.E.
Environmental Manager

Enclosure

cc: Van Burbach, Joyce Engineering

PREPARED FOR:
REPUBLIC SERVICES OF NORTH CAROLINA, LLC
4300 OLD HOLLY SPRINGS ROAD
APEX, NORTH CAROLINA 27539

CLOSED HOLLY SPRINGS C&D LANDFILL
PERMIT NO. 92-14

FIRST SEMIANNUAL WATER QUALITY
MONITORING REPORT OF 2017

JULY 2017

PREPARED BY:

2211 WEST MEADOWVIEW ROAD, SUITE 101
GREENSBORO, NORTH CAROLINA 27407
NC LICENSE NUMBER C-0782
PHONE: [phone]
FAX: [phone]
JOYCE ENGINEERING PROJECT NO. 00895.1701.12

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First Semiannual Water Quality Monitoring Report of 2017 Joyce Engineering
Closed Holly Springs C&D Landfill, Permit No. 92-14 July 2017

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EXECUTIVE SUMMARY

This report presents the results of the first semiannual water quality monitoring event of 2017
conducted at the closed Holly Springs C&D Landfill on May 31, 2017. Samples were collected
by representatives of Joyce Engineering from groundwater monitoring wells. The analytical
results from the May 31, 2017 monitoring event have been reported by Pace Analytical Services,
LLC. of Norcross, Georgia under NC laboratory certification number 381.

During the May 2017 water quality monitoring event, two inorganic constituents (arsenic and
barium) were reported at quantified concentrations above the Solid Waste Section Reporting
Limit (SWSL) in samples from one or more downgradient monitoring wells. No organic
constituents were detected at quantified concentrations above SWSLs in samples from
downgradient monitoring wells during the May 2017 event.

Arsenic was detected above the NC2L Standard in MW-12. The arsenic detected in MW-12 is
consistent with historical data and, as discussed in previous submittals, is most likely naturally
occurring. No other constituents were reported above their respective NC2L standards during
the May 2017 event.

Based on the results summarized herein, Republic Services of North Carolina, LLC, will
continue monitoring the uppermost aquifer beneath the closed Holly Springs C&D Landfill in
accordance with the requirements outlined in Title 15A NCAC 13B.0500.

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First Semiannual Water Quality Monitoring Report of 2017 Joyce Engineering
Closed Holly Springs C&D Landfill, Permit No. 92-14 July 2017

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First Semiannual Water Quality Monitoring Report of 2017
Closed Holly Springs C&D Landfill, Permit No. 94-14
Wake County, North Carolina

TABLE OF CONTENTS

1.0  INTRODUCTION..............................................................................................................1 
1.1  Site Description and Background ................................................................................ 1 
1.2 Sampling Network ........................................................................................................ 1 
1.3 Hydrogeologic Setting ................................................................................................... 1 
2.0 FIELD PROGRAM, MONITORING RESULTS, AND DISCUSSION ......................2 
2.1 Well Network and Groundwater Elevation Measurements...................................... 2 
2.2 May 2017 Monitoring Event ........................................................................................ 3 
2.3 Laboratory Analysis Program ..................................................................................... 3 
2.4 May 2017 Sampling Results ......................................................................................... 4 
3.0 LABORATORY AND FIELD QA/QC ............................................................................4 
4.0 DATA EVALUTION .........................................................................................................4 
4.1 Comparisons to Groundwater and Surface Water Standards ................................. 4 
4.2 Statistical Evaluations .................................................................................................. 5 
5.0 CONCLUSIONS ................................................................................................................5 
6.0 REFERENCES ...................................................................................................................6 

TABLES
Table 1 Historical Groundwater Elevations
Table 2 Hydraulic Gradients and Linear Groundwater Velocities
Table 3 Field Parameters by Location
Table 4 Quantified Detections by Monitoring Location
Table 5 Exceedances of Standards by Monitoring Location

DRAWING
Drawing 1 Groundwater Potentiometric Surface Map – May 31, 2017

APPENDICES
Appendix A Groundwater and Surface Water Field Data Logs
Appendix B May 2017 Laboratory Analytical Report
Appendix C Historical Groundwater Constituents in Groundwater
Appendix D Historical Surface Water Constituents in Surface Water
Appendix E Statistical Analyses Worksheets

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First Semiannual Water Quality Monitoring Report of 2017 Joyce Engineering
Closed Holly Springs C&D Landfill, Permit No. 92-14 July 2017

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1.0 INTRODUCTION
This report summarizes the monitoring results from the May 31, 2017, water quality monitoring
event at the closed Holly Springs Construction & Demolition (C&D) Landfill in Wake County,
North Carolina in accordance with Title 15A of the North Carolina Administrative Code
(NCAC) Subchapter 13B .0500. The closed Holly Springs C&D Landfill is maintained by
Republic Services of North Carolina, LLC (Republic) under Permit No. 92-14 issued by the
North Carolina Department of Environment and Natural Resources (DENR), now the
Department of Environmental Quality (NCDEQ)

1.1 Site Description and Background
The closed Holly Springs C&D Landfill is located within the town limits of Holly Springs, NC at
4300 Old Holly Springs Apex Road. The landfill is bounded to the north by Ivy Arbor Way, to
the east by Old Holly Springs Apex Road, to the south by heavily wooded properties, and to the
west by a golf course and wooded areas. The location of the facility is shown on the inlay on
Drawing 1. A power line easement runs through the southern portion of the landfill along an
east-northeast trending transect. Surrounding land use is primarily rural residential, silvicultural,
and commercial. Access to the facility is from Old Holly Springs Apex Road.

Topographic elevations at the facility range from approximately 280 to 420 feet above mean sea
level. Two small, unnamed perennial streams transect the site in a northwesterly direction
toward Little Branch, which is located northwest of the site. The first stream is located in the
southwest portion of the site and flows to the northwest, and the second flows from the
southeastern corner to the northwest corner of the site. The locations of the streams and surface
water sampling points are shown on Drawing 1.

1.2 Sampling Network
The facility’s current monitoring network is comprised of 12 monitoring wells (MW-1R, MW-2,
MW-3, MW-4, MW-5R, MW-6, MW-7, MW-9, MW-10, MW-11, MW-12, and MW-13), which
monitor the uppermost aquifer beneath the facility. Wells MW-1, MW-5, and MW-8 were
decommissioned due to construction activities at the landfill. Two surface water monitoring
points are monitored semiannually: upstream monitoring point SW-1 and downstream
monitoring point SW-2. Based on the results of the laboratory analyses, Republic Services of
North Carolina, LLC continues to maintain compliance with the detection monitoring
requirements under Title 15A Subchapter 13B.0500 rules at this facility.

1.3 Hydrogeologic Setting
Geologically, the facility is located in the Durham Sub-Basin within the Deep River Triassic
Basin in the Piedmont Physiographic Province, east of the Jonesboro Fault zone, where Triassic-
aged sediments are situated unconformably upon older igneous and metamorphic rocks of the
Carolina Slate Belt (NCGS, 1985). The underlying Triassic sedimentary rocks belong to the
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First Semiannual Water Quality Monitoring Report of 2017 Joyce Engineering
Closed Holly Springs C&D Landfill, Permit No. 92-14 July 2017

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Chatham Group, which are composed of conglomerate, arkosic sandstone, siltstone, claystone,
and mudstone (Horton and Zullo, 1991). Various dikes and sills are also found in this area.

The groundwater beneath the facility is present in a shallow, unconfined aquifer comprised of
unconsolidated sediment, partially weathered rock, and fractured sedimentary rocks.
Groundwater depths vary at the site ranging from approximately 6-29 feet below grade.
Groundwater elevations obtained during the May 2017 monitoring event, as well as historical
groundwater elevations, are summarized in Table 1. Based on the topography shown on
Drawing 1, regional groundwater flow in the uppermost aquifer beneath the site is expected to be
generally to the northwest toward Little Branch.

The hydraulic gradients in the uppermost aquifer underlying the site, as measured along the
conceptual flow paths shown on the May 31, 2017 potentiometric surface map (Drawing 1), were
calculated to be approximately 0.046 to 0.103 ft/ft (Table 2). The estimated rate of groundwater
flow for the uppermost aquifer beneath the facility was calculated using the following modified
Darcy equation:
Vgw = Ki/ne

Where Vgw = average linear groundwater velocity (feet per day), K = hydraulic conductivity (feet
per day), i = horizontal hydraulic gradient, and ne = effective porosity. Since we have no data on
hydraulic conductivity or effective porosity from this facility, we used estimated values based on
the average of values for these parameters reported for three other landfills located in Wake
County.

The average estimated linear groundwater flow velocity under the waste management unit is
approximately 0.3 to 0.7 ft/day (Table 2). Flow is generally toward the northwest (as expected),
although local flow directions vary (Drawing 1). The calculated linear velocity is based on the
simplifying assumptions of a homogenous and isotropic aquifer, and should be considered a
general estimate.

2.0 FIELD PROGRAM, MONITORING RESULTS, AND DISCUSSION
2.1 Well Network and Groundwater Elevation Measurements
The network of groundwater monitoring wells at the closed Holly Springs C&D Landfill consists
of 12 wells (MW-1R, MW-2, MW-3, MW-4, MW-5R, MW-6, MW-7, MW-9, MW-10, MW-11,
MW-12, and MW-13). Monitoring well locations are shown on Drawing 1. The network of
monitoring wells was constructed to target the preferential flow path for groundwater underlying
waste disposal areas. One upstream (SW-1) and one downstream (SW-2) surface water points
are also monitored.

Monitoring wells MW-1R and MW-10 are the facility’s background wells and are located
hydraulically upgradient of the waste disposal area in the southeast portion of the site. The other
monitoring wells are located downgradient or sidegradient of the waste disposal area.
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Closed Holly Springs C&D Landfill, Permit No. 92-14 July 2017

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2.2 May 2017 Monitoring Event
Personnel from Joyce Engineering visited the facility on May 31, 2017 to purge and sample
monitoring wells MW-1R, MW-2, MW-3, MW-4, MW-5R, MW-6, MW-7, MW-9, MW-10,
MW-11, MW-12, and MW-13. Surface water point SW-1 was dry (as observed during some
past events, as summarized in the historical table in Appendix D) and unable to be sampled
during the May 31, 2017 monitoring event; however, a sample was collected from SW-2. Depth-
to-water measurements were obtained from the network monitoring wells to the nearest 0.01 foot
using an electronic water level indicator prior to purging the wells. Monitoring well
groundwater elevations for this event are presented in Table 1. A groundwater potentiometric
surface map based on May 31, 2017 measurements, is shown on Drawing 1.

The monitoring wells were purged and sampled using dedicated pumps and micropurge
procedures; except for MW-9 and MW-12, which were sampled with a peristaltic pump and
micropurge procedures. MW-9 was sampled with a peristaltic pump to reduce the turbidity,
which has caused problems in previous events, and MW-12 was sampled with a peristaltic pump
because its dedicated pump was not working. The MW-12 pump will be repaired or replaced
before the next sampling event. For all of the monitoring wells, measurements of pH,
conductivity, dissolved oxygen, oxidation-reduction potential, temperature, and turbidity were
recorded on approximately 1 to 3-minute intervals during the purge, depending on the purge rate.
In general, the purge rate for each well was matched to the yield of the monitoring well, as
determined by continuously monitoring the depth to water, up to a maximum purge rate of 500
milliliters per minute. Purging was continued until stabilization was indicated by the field
parameters. In general, stabilization was deemed to be complete once the range in measured
values for each required field parameter was less than 10% over three monitoring intervals. The
field parameter data for each well/sample point prior to sampling are presented in Table 3, and
field sampling logs are included in Appendix A. Each log includes a description of the sampling
location, sampling equipment, sampling method, field observations, and field parameter
measurements.

The required groundwater samples were collected directly from the pump discharge tubing in the
laboratory-supplied, pre-preserved sample containers after purging was completed based on
stabilization of the field parameters. After collection, the samples were placed in a cooler on ice,
under chain-of-custody control.

2.3 Laboratory Analysis Program
The May 2017 groundwater and surface water samples were submitted to Pace Analytical
Services, LLC of Norcross, Georgia, under chain-of-custody control for analysis. The
groundwater samples, including the Field Blank, were analyzed for RCRA Metals and North
Carolina Appendix I VOCs plus tetrahydrofuran. The Trip Blank was analyzed for North
Carolina Appendix I VOCs plus tetrahydrofuran. The samples were received by the laboratory
on June 2, 2017, in good condition, and properly preserved, and within a time frame such that
analysis hold times were met for the event. The laboratory certificates-of-analysis and chains-of-
custody for the monitoring event are included in Appendix B.
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2.4 May 2017 Sampling Results
Constituents detected at quantified concentrations above the Solid Waste Section Reporting
Limits (SWSLs) during the May 2017 sampling event are presented in Table 4. Constituents
detected above applicable groundwater or surface water standards during the May 2017 sampling
event are presented in Table 5. Historical groundwater and surface water analytical data are
included in Appendices C and D, respectively.

Two RCRA metals (arsenic and barium) were detected in samples from monitoring wells at
quantified concentrations above their respective SWSLs. The detections are as follows: arsenic
in MW-12 and barium in MW-1R, MW-5R, MW-6, MW-7, MW-12, and MW-13. No organic
constituents were detected above their respective SWSLs during the May 2017 monitoring event.

Arsenic was detected above the NC2L Standard in MW-12 at 26.8 µg/L, which is consistent with
historical detections. Arsenic in MW-12 was not above the statistical background concentration
(see Section 4.2). No other constituents were detected above the applicable groundwater
protection standards (GPS).

3.0 LABORATORY AND FIELD QA/QC
The Field Blank was analyzed for 8 RCRA metals, NC Appendix I VOCs constituents plus
tetrahydrofuran and the Trip Blank for NC Appendix I VOCs plus tetrahydrofuran. There were
no detected constituents in either blank.

Upon receipt of the laboratory data package, the data were reviewed by Joyce Engineering
personnel for the following:

 General typographical errors;
 Correct analyses performed and within method specified hold times;
 Biased data results based on Surrogate Recoveries, Matrix Spike, Matrix Spike Duplicate,
and Laboratory Control Samples;
 Blank-qualified data (B-flags);
 Detections above the groundwater and surface water standards; and
 Detections that are above historical levels.

There were no errors or quality-control issues noted in the laboratory report or in the review by
Joyce.

4.0 DATA EVALUTION
4.1 Comparisons to Groundwater and Surface Water Standards
Arsenic was detected in exceedance of its NC2L standard in MW-12; however, this is consistent
with historical data from that well. Arsenic is naturally occurring in both upgradient and
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Closed Holly Springs C&D Landfill, Permit No. 92-14 July 2017

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downgradient wells, as discussed in past submittals. Wake County has been identified as an area
of North Carolina with a high probability of naturally occurring arsenic as presented in the
October 2003 DENR document “Distribution of Total Arsenic in Groundwater in the North
Carolina Piedmont”.

There was not enough running water to sample SW-1. There were no quantified detections
found in the SW-2 sample.

4.2 Statistical Evaluations
The data were evaluated through the use of the Shapiro-Wilk Test, Parametric Prediction Limits,
Parametric Tolerance Intervals, Aitchison’s Adjustment, Non-parametric Prediction Limits, and
Poisson Prediction Limits, as appropriate. Background data, tests for normality, outliers,
Aitchison’s adjustment, tolerance interval, or prediction limits are used, as appropriate based on
the background data. The statistical test by which downgradient data are compared to facility
background data is based upon the nature of the data and the number of data values that are less
than the laboratory limit of detection. Statistical tests are evaluated at the 0.01 level of
significance, 99% confidence level, and are conducted as one-tailed tests.

For interwell statistical evaluation, the results from downgradient wells are compared to the
statistical background based on the historical data from the facility’s upgradient background
well. Alternatively, intrawell statistical evaluation may be used to determine the background for
a specific monitoring well. For intrawell statistical evaluation, the data from the most recent six
sampling events are excluded and the earlier data are used for the background in the statistical
evaluation for comparison with the most recent result for a given constituent.

The arsenic results were evaluated using intrawell statistics in accordance with the procedures
outlined in 15A NCAC 13B.1632.(g) and (h) to determine if the quantified concentration
exceeded the background concentration. The statistical worksheets and summary table are
presented in Appendix E, and results are summarized below.

Constituent NC2L
Intrawell
Statistical
Background
Sample
Location
Sample
Result SSI
Arsenic 10 85.0 MW-12 26.8 No
Concentrations are in micrograms per liter (µg/L).
SSI = Statistically significant increase over background.

5.0 CONCLUSIONS
Based on the results summarized herein, Republic Services of North Carolina, LLC, will
continue monitoring the uppermost aquifer beneath the closed Holly Springs C&D Landfill in
accordance with the requirements for Detection Monitoring Program as outlined in Title 15A
NCAC 13B.0500.

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Closed Holly Springs C&D Landfill, Permit No. 92-14 July 2017

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6.0 REFERENCES
ESP Associates, P.A., 1997, Construction Quality Assurance (CQA) Submittal Holly Springs
Disposal, Inc. C&D Landfill Expansion-Cell 7, Phase A, July 30.

ESP Associates, P.A, 2003, Addendum to Permit 92-14 Holly Springs C&D Landfill Proposed
Cell 8 Expansion, February.

ESP Associates, P.A, 2003. Application for Permit to Operate a Construction & Demolition
Debris (C&D) Landfill-Holly Springs C&D Landfill Cell 8, Construction Quality Assurance
(CQA) Submittal BFI Waste Systems of North America, Inc., June.

Golder Associates NC, Inc., September 2011. Second Semi-Annual 2011 Sampling Event.
Prepared for Republic Services of North Carolina, LLC.

North Carolina Dept. Environment, Health, and Natural Resources (NCDEHNR), 1995, N.C.
Water Quality Monitoring Guidance Document for Solid Waste Facilities.

North Carolina Geologic Survey, 1985, Geologic Map of North Carolina; North Carolina
Department of Natural Resources and Community Development, Geological Survey Section;
scale 1:500,000.

Pippin, Charles G., Michele Butczynski, and Jonathan Clayton, 2003, Distribution of Total
Arsenic in Groundwater in the North Carolina Piedmont. Department of Environment and
Natural Resources Groundwater Section Resource Evaluation Program; Mooresville Regional
Office, October 3.

United States Environmental Protection Agency, 2003, Guidance for Developing Ecological Soil
Screening Levels. November.

TABLES

TABLE 1Historical Groundwater ElevationsLocation:MW-1R MW-2 MW-3 MW-4 MW-5R MW-6 MW-7 MW-9 MW-10 MW-11 MW-12 MW-13TOC Elevation:379.63 391.19 370.36 315.37 311.90 327.90 286.10 307.80 382.90 291.50 294.00 337.5722-Jul-09358.81 362.51 359.14 297.79 304.69 316.87 278.87 295.78 360.24 279.72 284.50 326.6726-Jan-10361.95 359.90 364.34 298.57 306.65 317.88 281.29 298.07 361.45 280.81 285.65 327.287-Jul-10356.32 363.41 358.61 298.30 304.19 316.57 278.63 296.23 361.12 278.76 284.32 325.155-Jan-11362.55 360.00 358.71 297.85 304.31 317.19 279.69 295.12 360.45 280.36 284.84 326.927-Jul-11356.89 358.69 358.73 297.96 305.01 317.45 279.23 296.61 360.66 280.15 284.63 326.8512-Jan-12357.72 357.73 359.54 298.76 305.02 317.61 280.32 296.15 360.68 280.48 284.93 327.2812-Jul-12357.79 357.54 359.17 297.60 304.29 317.08 278.89 295.78 360.35 279.35 284.44 326.326-Feb-13360.17 356.07 359.55 297.06 304.85 316.58 279.82 296.91 359.69 279.97 284.66 327.029-Jul-13355.78 357.38 359.45 297.56 304.29 316.99 280.29 297.89 363.05 279.25 284.79 327.5431-Jan-14357.62 356.10 359.52 296.97 304.81 316.60 279.79 296.89 359.64 280.00 284.60 326.9823-Jul-14357.53 360.29 358.91 298.27 305.15 317.70 279.40 295.34 361.22 280.26 284.48 327.0227-Jan-15361.30 354.74 364.44 298.43 307.23 318.90 280.70 297.29 363.98 281.50 285.55 327.7229-Jul-15358.58 362.29 358.46 298.39 305.00 317.66 279.26 297.01 361.90 280.23 284.34 326.8723-Jun-16361.38 363.70 360.06 299.02 305.09 318.30 279.73 297.28 362.60 280.45 284.48 326.372-Nov-16362.88 361.49 357.56 298.41 305.23 318.16 279.49 288.35* 362.60 280.87 284.51 326.7731-May-17 360.68 357.14 359.16 298.47 305.75 318.70 279.75 297.10 361.60 280.60 284.30 326.45MEAN:358.69 359.31 359.71 298.09 305.10 317.52 279.70 296.63 361.33 280.17 284.69 326.83MAXIMUM:362.55 363.70 364.44 299.02 307.23 318.90 281.29 298.07 363.98 281.50 285.65 327.72MINIMUM:355.78 27.49 5.92 16.35 4.67 9.00 4.81 9.73 18.92 10.00 8.35 9.85Notes:All measurements are given in feet AMSL (above mean sea level)TOC = Top of casing.The TOC elevation for MW-12 is approximate.-- = No data available.All data prior to 2012 taken from previous reports by Golder Associates NC, Inc. *MW-9 water level is lower than average as a result of slow recovery after well redevelopment performed on 11/1/2016. The initial depth to water was 10.45 feet on 11/1/16.Republic - Holly Springs LandfillPermit No. 92-14Joyce Engineering Inc.
TABLE 2Hydraulic Gradients and Linear Groundwater Velocities Groundwater Horizontal Hydraulic Effective LinearSegment Contours Gradient Conductivity Porosity VelocityLength(Beginning/End)iKneVgw( linear feet)(feet AMSL) (ft/ft) (ft/day)(ft/day)350290340310340310360320350310360320AVERAGE: 0.063 AVERAGE: 0.421Notes:Horizontal velocities based on the modified Darcy equation Vgw = Ki/neValues for K and ne were obtained by taking the averages of K and ne reported for three other landfills in Wake County, NC based on recent documents found on the DENR's CARA3Portal.Gradient segments are based on the May 2017 groundwater contours as shown on Drawing 1.0.056 1.0 0.15 0.375W 0.057 1.0 0.15 0.377535 N 0.056 1.0 0.15Gradient Calculation SegmentFlow Directioni11066N0.374i2530i4870NE0.0461.00.15i3390SW0.1031.00.150.684May 31, 20170.407i6656SW0.0611.00.150.307i5Republic- Holly Springs LandfillPermit No. 92-14Joyce Engineering Inc.
TABLE 3: Field Parameters
WELL ID PARAMETER RESULT UNITS COLLECT DATE
9214-MW1R Temperature 19.2 °C 5/31/2017
9214-MW1R Dissolved Oxygen 3.40 mg/l 5/31/2017
9214-MW1R Conductivity 319.3 µs/cm 5/31/2017
9214-MW1R pH 6.43 S.U. 5/31/2017
9214-MW1R Oxidation Reduction Potential 123.4 mV 5/31/2017
9214-MW1R Turbidity 4.06 NTU 5/31/2017
9214-MW1R Static Water Level 18.95 ft 5/31/2017
9214-MW1R Well Depth 54.60 ft 5/31/2017
9214-MW2 Temperature 17.2 °C 5/31/2017
9214-MW2 Dissolved Oxygen 1.28 mg/l 5/31/2017
9214-MW2 Conductivity 211.5 µs/cm 5/31/2017
9214-MW2 pH 6.52 S.U. 5/31/2017
9214-MW2 Oxidation Reduction Potential 16.8 mV 5/31/2017
9214-MW2 Turbidity 8.70 NTU 5/31/2017
9214-MW2 Static Water Level 34.05 ft 5/31/2017
9214-MW2 Well Depth 47.50 ft 5/31/2017
9214-MW3 Temperature 17.9 °C 5/31/2017
9214-MW3 Dissolved Oxygen 3.51 mg/l 5/31/2017
9214-MW3 Conductivity 69.2 µs/cm 5/31/2017
9214-MW3 pH 6.36 S.U. 5/31/2017
9214-MW3 Oxidation Reduction Potential 30.0 mV 5/31/2017
9214-MW3 Turbidity 4.21 NTU 5/31/2017
9214-MW3 Static Water Level 11.20 ft 5/31/2017
9214-MW3 Well Depth 35.39 ft 5/31/2017
9214-MW4 Temperature 16.8 °C 5/31/2017
9214-MW4 Dissolved Oxygen 2.25 mg/l 5/31/2017
9214-MW4 Conductivity 132.7 µs/cm 5/31/2017
9214-MW4 pH 5.54 S.U. 5/31/2017
9214-MW4 Oxidation Reduction Potential 99.2 mV 5/31/2017
9214-MW4 Turbidity 4.29 NTU 5/31/2017
9214-MW4 Static Water Level 16.9 ft 5/31/2017
9214-MW4 Well Depth 34.88 ft 5/31/2017
9214-MW5R Temperature 15.5 °C 5/31/2017
9214-MW5R Dissolved Oxygen 0.99 mg/l 5/31/2017
9214-MW5R Conductivity 653 µs/cm 5/31/2017
9214-MW5R pH 6.20 S.U. 5/31/2017
9214-MW5R Oxidation Reduction Potential 94.8 mV 5/31/2017
9214-MW5R Turbidity 5.86 NTU 5/31/2017
9214-MW5R Static Water Level 6.15 ft 5/31/2017
9214-MW5R Well Depth 24.21 ft 5/31/2017
Republic- Holly Springs Landfill
Permit No. 92-14 Page 1 of 3 Joyce Engineering
TABLE 3: Field Parameters
WELL ID PARAMETER RESULT UNITS COLLECT DATE
9214-MW6 Temperature 16.8 °C 5/31/2017
9214-MW6 Dissolved Oxygen 1.69 mg/l 5/31/2017
9214-MW6 Conductivity 294.2 µs/cm 5/31/2017
9214-MW6 pH 6.32 S.U. 5/31/2017
9214-MW6 Oxidation Reduction Potential 62.6 mV 5/31/2017
9214-MW6 Turbidity 8.87 NTU 5/31/2017
9214-MW6 Static Water Level 9.20 ft 5/31/2017
9214-MW6 Well Depth 21.4 ft 5/31/2017
9214-MW7 Temperature 15.8 °C 5/31/2017
9214-MW7 Dissolved Oxygen 1.03 mg/l 5/31/2017
9214-MW7 Conductivity 184.3 µs/cm 5/31/2017
9214-MW7 pH 5.44 S.U. 5/31/2017
9214-MW7 Oxidation Reduction Potential 106.5 mV 5/31/2017
9214-MW7 Turbidity 3.64 NTU 5/31/2017
9214-MW7 Static Water Level 6.35 ft 5/31/2017
9214-MW7 Well Depth 24.2 ft 5/31/2017
9214-MW9 Temperature 15.9 °C 5/31/2017
9214-MW9 Dissolved Oxygen 1.32 mg/l 5/31/2017
9214-MW9 Conductivity 607 µs/cm 5/31/2017
9214-MW9 pH 5.53 S.U. 5/31/2017
9214-MW9 Oxidation Reduction Potential 108.8 mV 5/31/2017
9214-MW9 Turbidity 15.1 NTU 5/31/2017
9214-MW9 Static Water Level 10.7 ft 5/31/2017
9214-MW9 Well Depth 23.80 ft 5/31/2017
9214-MW10 Temperature 17.6 °C 5/31/2017
9214-MW10 Dissolved Oxygen 6.11 mg/l 5/31/2017
9214-MW10 Conductivity 108.5 µs/cm 5/31/2017
9214-MW10 pH 6.40 S.U. 5/31/2017
9214-MW10 Oxidation Reduction Potential 83.1 mV 5/31/2017
9214-MW10 Turbidity 3.98 NTU 5/31/2017
9214-MW10 Static Water Level 21.30 ft 5/31/2017
9214-MW10 Well Depth 47.00 ft 5/31/2017
9214-MW11 Temperature 15.4 °C 5/31/2017
9214-MW11 Dissolved Oxygen 1.77 mg/l 5/31/2017
9214-MW11 Conductivity 622 µs/cm 5/31/2017
9214-MW11 pH 5.83 S.U. 5/31/2017
9214-MW11 Oxidation Reduction Potential 108.5 mV 5/31/2017
9214-MW11 Turbidity 5.29 NTU 5/31/2017
9214-MW11 Static Water Level 10.9 ft 5/31/2017
9214-MW11 Well Depth 25.75 ft 5/31/2017
Republic- Holly Springs Landfill
Permit No. 92-14 Page 2 of 3 Joyce Engineering
TABLE 3: Field Parameters
WELL ID PARAMETER RESULT UNITS COLLECT DATE
9214-MW12 Temperature 16.0 °C 5/31/2017
9214-MW12 Dissolved Oxygen 1.21 mg/l 5/31/2017
9214-MW12 Conductivity 692 µs/cm 5/31/2017
9214-MW12 pH 5.69 S.U. 5/31/2017
9214-MW12 Oxidation Reduction Potential 33.8 mV 5/31/2017
9214-MW12 Turbidity 15.17 NTU 5/31/2017
9214-MW12 Static Water Level 9.70 ft 5/31/2017
9214-MW12 Well Depth 25.19 ft 5/31/2017
9214-MW13 Temperature 15.7 °C 5/31/2017
9214-MW13 Dissolved Oxygen 2.09 mg/l 5/31/2017
9214-MW13 Conductivity 379.9 µs/cm 5/31/2017
9214-MW13 pH 5.93 S.U. 5/31/2017
9214-MW13 Oxidation Reduction Potential -49.1 mV 5/31/2017
9214-MW13 Turbidity 2.86 NTU 5/31/2017
9214-MW13 Static Water Level 11.12 ft 5/31/2017
9214-MW13 Well Depth 26.68 ft 5/31/2017
9214-SW-2 Temperature 20.0 °C 5/31/2017
9214-SW-2 Dissolved Oxygen 4.81 mg/l 5/31/2017
9214-SW-2 Conductivity 540 µs/cm 5/31/2017
9214-SW-2 pH 6.56 S.U. 5/31/2017
9214-SW-2 Oxidation Reduction Potential 67.1 mV 5/31/2017
9214-SW-2 Turbidity 15.0 NTU 5/31/2017
Notes:ºC= degrees Centigrade
mg/l - milligrams per liter
µs/cm = microsemens per centimeter
S.U.= Standard Units
mV = millivolts
ntu = Nephelometric Turbidity Units
ft = feet
Republic- Holly Springs Landfill
Permit No. 92-14 Page 3 of 3 Joyce Engineering
TABLE 4: Quantified Detections by Monitoring Location
WELL ID PARAMETER RESULT UNITS SWSL DATE
9214-MW1R Total Barium 408 µg/l 100 5/31/2017
9214-MW5R Total Barium 160 µg/l 100 5/31/2017
9214-MW6 Total Barium 298 µg/l 100 5/31/2017
9214-MW7 Total Barium 166 µg/l 100 5/31/2017
9214-MW12 Total Arsenic 26.8 µg/l 10 5/31/2017
9214-MW12 Total Barium 196 µg/l 100 5/31/2017
9214-MW13 Total Barium 238 µg/l 100 5/31/2017
Notes:µg/l = Micorgrams per liter.
SWSL = NC Soild Waste Section Reporting Limit.
Laboratory Reporting limit used when SWSL has not been established.
J = Estimated concentration below the SWSL.
Republic - Holly Springs Landfill
Permit No. 92-14
Joyce Engineering
TABLE 5: Exceedances of Standards by Monitiorng Location
WELL ID PARAMETER RESULT UNITS SWSL
NC2L/
*GWPS DATE
9214-MW12 Total Arsenic 26.8 µg/l 10 10 5/31/2017

Notes:µg/l = Micorgrams per liter
SWSL = NC Soild Waste Section Reporting Limit
Laboratory Reporting limit used when SWSL has not been established
NC2L = NC Groundwater Standard from 15A NCAC 2L.0202
GWPS = NC Solid Waste Section Groundwater Protection Standard (for constituents with no NC2L)
Republic - Holly Springs Landfill
Permit No. 92-14
Joyce Engineering

DRAWING

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LATERAL EXPANSION
CELL 7 NORTHWEST
EXPANSION
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CELL 4
CELL 8
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CELL 5
CELL 6
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357.14
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359.16
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298.47
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EXISTING 10' TOPOGRAPHIC CONTOUR
EXISTING 2' TOPOGRAPHIC CONTOUR
GROUNDWATER ELEVATION CONTOUR IN FEET ABOVE
MEAN SEA LEVEL BASED ON MAY 31, 2017 DATA.
GROUNDWATER FLOW DIRECTION
SEGMENT USED FOR GRADIENT CALCULATION
GROUNDWATER MONITORING WELL LOCATION AND
IDENTIFICATION WITH GROUNDWATER ELEVATION.
SURFACE MONITORING POINT LOCATION AND
IDENTIFICATION
1.TOPOGRAPHIC CONTOUR INTERVAL = 2 FEET
2.GROUNDWATER CONTOUR INTERVAL = 10 FEET
LEGEND
NOTES
i
i
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FLOW PATH LENGTH
1066 LF
530 LF
535 LF
i
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870 LF
390 LF
656 LF
PROJECT NO.APPROVEDCHECKEDDRAWNDESIGNEDDATEDATEREVISIONS AND RECORD OF ISSUEBYNO APPCK
SCALE All rights reserved.Ó Joyce Engineering, Inc.DRAWING NO.L:\Republic NC\Holly Springs\2017 May Holly Springs GW Map.dwg Layout=GW map2211 W. MEADOWVIEW ROADGREENSBORO, NC 27407PHONE: [phone]NC CORP LIC: C-0782895HOLLY SPRINGS CLOSED C&D LANDFILLWAKE COUNTY, NORTH CAROLINA20171
AS SHOWNGROUNDWATER POTENTIOMETRIC SURFACE MAPMAY 31, 2017PERMIT NO. 92-14GERHVBVB06/20/17VICINITY MAP
0
(FEET)
GRAPHIC SCALE
20010050
SOURCE: U.S.G.S. 7.5 MINUTE TOPO FOR APEX, NC

APPENDICES

Appendix A

Field Data Logs

Appendix B

Laboratory Analytical Reports

PACE ANALYTICAL SERVICES, LLC.Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]Republic Services of North Carolina, LLCProject: Holly Springs Closed C&D LandfillConover, NC 286131220 Commerce Street, SWMr. Matt EinsmannWe appreciate the opportunity to provide the analytical support for your project. The analytical results in this report are based upon information supplied by you, the client, and are for your exclusive use. If you have any questions regarding this data package, please do not hesitate to call. Pace Analytical Services, LLC. certifies that the following analytical results meet all requirements of the National Environmental Laboratory Accreditation Conference(NELAC).All test results relate only to the samples analyzed.Laboratory ReportProject #:[none]Prepared For:Attention:June 15, 2017Report Number:AAF0102Approved:This report may not be reproduced, except in full, without written approval from Pace Analytical Services, LLC.Page 1 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017Sample IDLaboratory IDMatrixDate SampledANALYTICAL REPORT FOR SAMPLESDate Received9214-MW1RAAF0102-0105/31/17 10:22 06/02/17 09:05Ground Water9214-MW2AAF0102-0205/31/17 11:5606/02/17 09:05Ground Water9214-MW3AAF0102-0305/31/17 11:1106/02/17 09:05Ground Water9214-MW4AAF0102-0405/31/17 12:1306/02/17 09:05Ground Water9214-MW5RAAF0102-0505/31/17 13:2506/02/17 09:05Ground Water9214-MW6AAF0102-0605/31/17 13:5406/02/17 09:05Ground Water9214-MW7AAF0102-0705/31/17 12:3206/02/17 09:05Ground Water9214-MW9AAF0102-0805/31/17 14:2406/02/17 09:05Ground Water9214-MW10AAF0102-0905/31/17 11:3706/02/17 09:05Ground Water9214-MW11AAF0102-1005/31/17 12:4906/02/17 09:05Ground Water9214-MW12AAF0102-1105/31/17 15:0406/02/17 09:05Ground Water9214-MW13AAF0102-1205/31/17 11:0006/02/17 09:05Ground Water9214-SW2AAF0102-1305/31/17 12:5506/02/17 09:05Surface Water9214-Field BlankAAF0102-1405/31/17 15:2106/02/17 09:05Water9214-Trip BlankAAF0102-1505/31/17 08:0006/02/17 09:05WaterPage 2 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW1RGround WaterAAF0102-01AAF010205/31/17 10:22Project:Holly Springs Closed C&D Landfill06/02/17 09:05Metals, TotalEPA 6020B2.21ug/L1Arsenic10.0J7060188EPA 3005A0.427440-38-206/10/17 20:2006/07/17 14:15EPA 6020B408ug/L1Barium1007060188EPA 3005A0.277440-39-306/10/17 20:2006/07/17 14:15NDEPA 6020Bug/L1Cadmium1.007060188EPA 3005A0.067440-43-906/10/17 20:2006/07/17 14:15EPA 6020B0.59ug/L1Chromium10.0J7060188EPA 3005A0.347440-47-306/10/17 20:2006/07/17 14:15NDEPA 6020Bug/L1Lead10.07060188EPA 3005A0.077439-92-106/10/17 20:2006/07/17 14:15NDEPA 6020Bug/L1Selenium10.07060188EPA 3005A1.417782-49-206/10/17 20:2006/07/17 14:15NDEPA 6020Bug/L1Silver10.07060188EPA 3005A0.327440-22-406/10/17 20:2006/07/17 14:15NDEPA 7470Aug/L1Mercury0.2007060107EPA 7470A0.0417439-97-606/06/17 13:5006/06/17 10:35Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L1Acetone1007060218EPA 5030B8.267-64-106/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L1Acrylonitrile2007060218EPA 5030B2.5107-13-106/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L1Benzene1.07060218EPA 5030B0.271-43-206/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L1Bromochloromethane3.07060218EPA 5030B0.574-97-506/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L1Bromodichloromethane1.07060218EPA 5030B0.475-27-406/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L1Bromoform3.07060218EPA 5030B0.675-25-206/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L1Bromomethane107060218EPA 5030B1.074-83-906/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L1Carbon Disulfide1007060218EPA 5030B0.875-15-006/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L1Carbon Tetrachloride1.07060218EPA 5030B0.456-23-506/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L1Chlorobenzene3.07060218EPA 5030B0.5108-90-706/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L1Chloroethane107060218EPA 5030B0.575-00-306/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L1Chloroform5.07060218EPA 5030B0.667-66-306/07/17 12:4406/07/17 10:00Page 3 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW1RGround WaterAAF0102-01AAF010205/31/17 10:22Project:Holly Springs Closed C&D Landfill06/02/17 09:05Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L1Chloromethane1.07060218EPA 5030B0.474-87-306/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L1Dibromochloromethane3.07060218EPA 5030B0.3124-48-106/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L11,2-Dibromo-3-chloropropane137060218EPA 5030B0.696-12-806/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L11,2-Dibromoethane1.07060218EPA 5030B0.3106-93-406/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L1Dibromomethane107060218EPA 5030B0.674-95-306/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L11,2-Dichlorobenzene5.07060218EPA 5030B0.595-50-106/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L11,4-Dichlorobenzene1.07060218EPA 5030B0.6106-46-706/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L1trans-1,4-Dichloro-2-butene1007060218EPA 5030B1.6110-57-606/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L11,1-Dichloroethane5.07060218EPA 5030B0.475-34-306/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L11,2-Dichloroethane1.07060218EPA 5030B0.7107-06-206/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L11,1-Dichloroethene5.07060218EPA 5030B0.775-35-406/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L1cis-1,2-Dichloroethene5.07060218EPA 5030B0.7156-59-206/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L1trans-1,2-Dichloroethene5.07060218EPA 5030B0.5156-60-506/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L11,2-Dichloropropane1.07060218EPA 5030B0.678-87-506/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L1cis-1,3-Dichloropropene1.07060218EPA 5030B0.210061-01-506/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L1trans-1,3-Dichloropropene1.07060218EPA 5030B0.310061-02-606/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L1Ethylbenzene1.07060218EPA 5030B0.4100-41-406/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L1Iodomethane107060218EPA 5030B3.174-88-406/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L1Methyl Butyl Ketone (2-Hexanone)507060218EPA 5030B0.9591-78-606/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L1Methylene Chloride1.07060218EPA 5030B0.575-09-206/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L1Methyl Ethyl Ketone (2-Butanone)1007060218EPA 5030B3.278-93-306/07/17 12:4406/07/17 10:00Page 4 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW1RGround WaterAAF0102-01AAF010205/31/17 10:22Project:Holly Springs Closed C&D Landfill06/02/17 09:05Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L14-Methyl-2-pentanone (MIBK)1007060218EPA 5030B0.9108-10-106/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L1Styrene1.07060218EPA 5030B0.5100-42-506/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L11,1,1,2-Tetrachloroethane5.07060218EPA 5030B0.3630-20-606/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L11,1,2,2-Tetrachloroethane3.07060218EPA 5030B0.579-34-506/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L1Tetrachloroethene1.07060218EPA 5030B0.8127-18-406/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L1Toluene1.07060218EPA 5030B0.3108-88-306/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L11,1,1-Trichloroethane1.07060218EPA 5030B0.471-55-606/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L11,1,2-Trichloroethane1.07060218EPA 5030B0.679-00-506/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L1Trichloroethene1.07060218EPA 5030B0.379-01-606/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L1Trichlorofluoromethane1.07060218EPA 5030B0.575-69-406/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L11,2,3-Trichloropropane1.07060218EPA 5030B0.596-18-406/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L1Vinyl Acetate507060218EPA 5030B0.4108-05-406/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L1Vinyl Chloride1.07060218EPA 5030B0.675-01-406/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L1Xylenes, total5.07060218EPA 5030B0.91330-20-706/07/17 12:4406/07/17 10:00NDEPA 8260Bug/L1Tetrahydrofuran107060218EPA 5030B1.3109-99-906/07/17 12:4406/07/17 10:00EPA 8260B92 %Surr: Dibromofluoromethane7060218EPA 5030B1868-53-706/07/17 12:4406/07/17 10:0080-120EPA 8260B98 %Surr: 1,2-Dichloroethane-d47060218EPA 5030B17060-07-006/07/17 12:4406/07/17 10:0078-120EPA 8260B99 %Surr: Toluene-d87060218EPA 5030B2037-26-506/07/17 12:4406/07/17 10:0080-120EPA 8260B98 %Surr: 4-Bromofluorobenzene7060218EPA 5030B460-00-406/07/17 12:4406/07/17 10:0080-120Page 5 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW2Ground WaterAAF0102-02AAF010205/31/17 11:56Project:Holly Springs Closed C&D Landfill06/02/17 09:05Metals, TotalEPA 6020B4.36ug/L1Arsenic10.0J7060188EPA 3005A0.427440-38-206/10/17 20:2506/07/17 14:15EPA 6020B74.0ug/L1Barium100J7060188EPA 3005A0.277440-39-306/10/17 20:2506/07/17 14:15NDEPA 6020Bug/L1Cadmium1.007060188EPA 3005A0.067440-43-906/10/17 20:2506/07/17 14:15EPA 6020B1.39ug/L1Chromium10.0J7060188EPA 3005A0.347440-47-306/10/17 20:2506/07/17 14:15EPA 6020B0.15ug/L1Lead10.0J7060188EPA 3005A0.077439-92-106/10/17 20:2506/07/17 14:15NDEPA 6020Bug/L1Selenium10.07060188EPA 3005A1.417782-49-206/10/17 20:2506/07/17 14:15NDEPA 6020Bug/L1Silver10.07060188EPA 3005A0.327440-22-406/10/17 20:2506/07/17 14:15NDEPA 7470Aug/L1Mercury0.2007060107EPA 7470A0.0417439-97-606/06/17 13:5206/06/17 10:35Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L1Acetone1007060218EPA 5030B8.267-64-106/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L1Acrylonitrile2007060218EPA 5030B2.5107-13-106/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L1Benzene1.07060218EPA 5030B0.271-43-206/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L1Bromochloromethane3.07060218EPA 5030B0.574-97-506/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L1Bromodichloromethane1.07060218EPA 5030B0.475-27-406/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L1Bromoform3.07060218EPA 5030B0.675-25-206/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L1Bromomethane107060218EPA 5030B1.074-83-906/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L1Carbon Disulfide1007060218EPA 5030B0.875-15-006/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L1Carbon Tetrachloride1.07060218EPA 5030B0.456-23-506/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L1Chlorobenzene3.07060218EPA 5030B0.5108-90-706/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L1Chloroethane107060218EPA 5030B0.575-00-306/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L1Chloroform5.07060218EPA 5030B0.667-66-306/07/17 13:1106/07/17 10:00Page 6 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW2Ground WaterAAF0102-02AAF010205/31/17 11:56Project:Holly Springs Closed C&D Landfill06/02/17 09:05Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L1Chloromethane1.07060218EPA 5030B0.474-87-306/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L1Dibromochloromethane3.07060218EPA 5030B0.3124-48-106/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L11,2-Dibromo-3-chloropropane137060218EPA 5030B0.696-12-806/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L11,2-Dibromoethane1.07060218EPA 5030B0.3106-93-406/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L1Dibromomethane107060218EPA 5030B0.674-95-306/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L11,2-Dichlorobenzene5.07060218EPA 5030B0.595-50-106/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L11,4-Dichlorobenzene1.07060218EPA 5030B0.6106-46-706/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L1trans-1,4-Dichloro-2-butene1007060218EPA 5030B1.6110-57-606/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L11,1-Dichloroethane5.07060218EPA 5030B0.475-34-306/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L11,2-Dichloroethane1.07060218EPA 5030B0.7107-06-206/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L11,1-Dichloroethene5.07060218EPA 5030B0.775-35-406/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L1cis-1,2-Dichloroethene5.07060218EPA 5030B0.7156-59-206/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L1trans-1,2-Dichloroethene5.07060218EPA 5030B0.5156-60-506/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L11,2-Dichloropropane1.07060218EPA 5030B0.678-87-506/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L1cis-1,3-Dichloropropene1.07060218EPA 5030B0.210061-01-506/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L1trans-1,3-Dichloropropene1.07060218EPA 5030B0.310061-02-606/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L1Ethylbenzene1.07060218EPA 5030B0.4100-41-406/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L1Iodomethane107060218EPA 5030B3.174-88-406/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L1Methyl Butyl Ketone (2-Hexanone)507060218EPA 5030B0.9591-78-606/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L1Methylene Chloride1.07060218EPA 5030B0.575-09-206/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L1Methyl Ethyl Ketone (2-Butanone)1007060218EPA 5030B3.278-93-306/07/17 13:1106/07/17 10:00Page 7 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW2Ground WaterAAF0102-02AAF010205/31/17 11:56Project:Holly Springs Closed C&D Landfill06/02/17 09:05Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L14-Methyl-2-pentanone (MIBK)1007060218EPA 5030B0.9108-10-106/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L1Styrene1.07060218EPA 5030B0.5100-42-506/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L11,1,1,2-Tetrachloroethane5.07060218EPA 5030B0.3630-20-606/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L11,1,2,2-Tetrachloroethane3.07060218EPA 5030B0.579-34-506/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L1Tetrachloroethene1.07060218EPA 5030B0.8127-18-406/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L1Toluene1.07060218EPA 5030B0.3108-88-306/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L11,1,1-Trichloroethane1.07060218EPA 5030B0.471-55-606/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L11,1,2-Trichloroethane1.07060218EPA 5030B0.679-00-506/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L1Trichloroethene1.07060218EPA 5030B0.379-01-606/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L1Trichlorofluoromethane1.07060218EPA 5030B0.575-69-406/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L11,2,3-Trichloropropane1.07060218EPA 5030B0.596-18-406/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L1Vinyl Acetate507060218EPA 5030B0.4108-05-406/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L1Vinyl Chloride1.07060218EPA 5030B0.675-01-406/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L1Xylenes, total5.07060218EPA 5030B0.91330-20-706/07/17 13:1106/07/17 10:00NDEPA 8260Bug/L1Tetrahydrofuran107060218EPA 5030B1.3109-99-906/07/17 13:1106/07/17 10:00EPA 8260B90 %Surr: Dibromofluoromethane7060218EPA 5030B1868-53-706/07/17 13:1106/07/17 10:0080-120EPA 8260B98 %Surr: 1,2-Dichloroethane-d47060218EPA 5030B17060-07-006/07/17 13:1106/07/17 10:0078-120EPA 8260B100 %Surr: Toluene-d87060218EPA 5030B2037-26-506/07/17 13:1106/07/17 10:0080-120EPA 8260B98 %Surr: 4-Bromofluorobenzene7060218EPA 5030B460-00-406/07/17 13:1106/07/17 10:0080-120Page 8 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW3Ground WaterAAF0102-03AAF010205/31/17 11:11Project:Holly Springs Closed C&D Landfill06/02/17 09:05Metals, TotalEPA 6020B3.25ug/L1Arsenic10.0J7060188EPA 3005A0.427440-38-206/10/17 20:3106/07/17 14:15EPA 6020B21.4ug/L1Barium100J7060188EPA 3005A0.277440-39-306/10/17 20:3106/07/17 14:15NDEPA 6020Bug/L1Cadmium1.007060188EPA 3005A0.067440-43-906/10/17 20:3106/07/17 14:15EPA 6020B0.34ug/L1Chromium10.0J7060188EPA 3005A0.347440-47-306/10/17 20:3106/07/17 14:15NDEPA 6020Bug/L1Lead10.07060188EPA 3005A0.077439-92-106/10/17 20:3106/07/17 14:15NDEPA 6020Bug/L1Selenium10.07060188EPA 3005A1.417782-49-206/10/17 20:3106/07/17 14:15NDEPA 6020Bug/L1Silver10.07060188EPA 3005A0.327440-22-406/10/17 20:3106/07/17 14:15NDEPA 7470Aug/L1Mercury0.2007060107EPA 7470A0.0417439-97-606/06/17 13:5506/06/17 10:35Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L1Acetone1007060218EPA 5030B8.267-64-106/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L1Acrylonitrile2007060218EPA 5030B2.5107-13-106/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L1Benzene1.07060218EPA 5030B0.271-43-206/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L1Bromochloromethane3.07060218EPA 5030B0.574-97-506/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L1Bromodichloromethane1.07060218EPA 5030B0.475-27-406/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L1Bromoform3.07060218EPA 5030B0.675-25-206/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L1Bromomethane107060218EPA 5030B1.074-83-906/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L1Carbon Disulfide1007060218EPA 5030B0.875-15-006/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L1Carbon Tetrachloride1.07060218EPA 5030B0.456-23-506/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L1Chlorobenzene3.07060218EPA 5030B0.5108-90-706/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L1Chloroethane107060218EPA 5030B0.575-00-306/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L1Chloroform5.07060218EPA 5030B0.667-66-306/07/17 13:3706/07/17 10:00Page 9 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW3Ground WaterAAF0102-03AAF010205/31/17 11:11Project:Holly Springs Closed C&D Landfill06/02/17 09:05Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L1Chloromethane1.07060218EPA 5030B0.474-87-306/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L1Dibromochloromethane3.07060218EPA 5030B0.3124-48-106/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L11,2-Dibromo-3-chloropropane137060218EPA 5030B0.696-12-806/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L11,2-Dibromoethane1.07060218EPA 5030B0.3106-93-406/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L1Dibromomethane107060218EPA 5030B0.674-95-306/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L11,2-Dichlorobenzene5.07060218EPA 5030B0.595-50-106/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L11,4-Dichlorobenzene1.07060218EPA 5030B0.6106-46-706/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L1trans-1,4-Dichloro-2-butene1007060218EPA 5030B1.6110-57-606/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L11,1-Dichloroethane5.07060218EPA 5030B0.475-34-306/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L11,2-Dichloroethane1.07060218EPA 5030B0.7107-06-206/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L11,1-Dichloroethene5.07060218EPA 5030B0.775-35-406/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L1cis-1,2-Dichloroethene5.07060218EPA 5030B0.7156-59-206/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L1trans-1,2-Dichloroethene5.07060218EPA 5030B0.5156-60-506/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L11,2-Dichloropropane1.07060218EPA 5030B0.678-87-506/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L1cis-1,3-Dichloropropene1.07060218EPA 5030B0.210061-01-506/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L1trans-1,3-Dichloropropene1.07060218EPA 5030B0.310061-02-606/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L1Ethylbenzene1.07060218EPA 5030B0.4100-41-406/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L1Iodomethane107060218EPA 5030B3.174-88-406/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L1Methyl Butyl Ketone (2-Hexanone)507060218EPA 5030B0.9591-78-606/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L1Methylene Chloride1.07060218EPA 5030B0.575-09-206/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L1Methyl Ethyl Ketone (2-Butanone)1007060218EPA 5030B3.278-93-306/07/17 13:3706/07/17 10:00Page 10 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW3Ground WaterAAF0102-03AAF010205/31/17 11:11Project:Holly Springs Closed C&D Landfill06/02/17 09:05Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L14-Methyl-2-pentanone (MIBK)1007060218EPA 5030B0.9108-10-106/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L1Styrene1.07060218EPA 5030B0.5100-42-506/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L11,1,1,2-Tetrachloroethane5.07060218EPA 5030B0.3630-20-606/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L11,1,2,2-Tetrachloroethane3.07060218EPA 5030B0.579-34-506/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L1Tetrachloroethene1.07060218EPA 5030B0.8127-18-406/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L1Toluene1.07060218EPA 5030B0.3108-88-306/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L11,1,1-Trichloroethane1.07060218EPA 5030B0.471-55-606/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L11,1,2-Trichloroethane1.07060218EPA 5030B0.679-00-506/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L1Trichloroethene1.07060218EPA 5030B0.379-01-606/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L1Trichlorofluoromethane1.07060218EPA 5030B0.575-69-406/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L11,2,3-Trichloropropane1.07060218EPA 5030B0.596-18-406/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L1Vinyl Acetate507060218EPA 5030B0.4108-05-406/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L1Vinyl Chloride1.07060218EPA 5030B0.675-01-406/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L1Xylenes, total5.07060218EPA 5030B0.91330-20-706/07/17 13:3706/07/17 10:00NDEPA 8260Bug/L1Tetrahydrofuran107060218EPA 5030B1.3109-99-906/07/17 13:3706/07/17 10:00EPA 8260B91 %Surr: Dibromofluoromethane7060218EPA 5030B1868-53-706/07/17 13:3706/07/17 10:0080-120EPA 8260B97 %Surr: 1,2-Dichloroethane-d47060218EPA 5030B17060-07-006/07/17 13:3706/07/17 10:0078-120EPA 8260B99 %Surr: Toluene-d87060218EPA 5030B2037-26-506/07/17 13:3706/07/17 10:0080-120EPA 8260B100 %Surr: 4-Bromofluorobenzene7060218EPA 5030B460-00-406/07/17 13:3706/07/17 10:0080-120Page 11 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW4Ground WaterAAF0102-04AAF010205/31/17 12:13Project:Holly Springs Closed C&D Landfill06/02/17 09:05Metals, TotalEPA 6020B2.95ug/L1Arsenic10.0J7060188EPA 3005A0.427440-38-206/10/17 20:3706/07/17 14:15EPA 6020B85.4ug/L1Barium100J7060188EPA 3005A0.277440-39-306/10/17 20:3706/07/17 14:15NDEPA 6020Bug/L1Cadmium1.007060188EPA 3005A0.067440-43-906/10/17 20:3706/07/17 14:15NDEPA 6020Bug/L1Chromium10.07060188EPA 3005A0.347440-47-306/10/17 20:3706/07/17 14:15NDEPA 6020Bug/L1Lead10.07060188EPA 3005A0.077439-92-106/10/17 20:3706/07/17 14:15NDEPA 6020Bug/L1Selenium10.07060188EPA 3005A1.417782-49-206/10/17 20:3706/07/17 14:15NDEPA 6020Bug/L1Silver10.07060188EPA 3005A0.327440-22-406/10/17 20:3706/07/17 14:15EPA 7470A0.043ug/L1Mercury0.200J7060107EPA 7470A0.0417439-97-606/06/17 13:5706/06/17 10:35Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L1Acetone1007060218EPA 5030B8.267-64-106/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L1Acrylonitrile2007060218EPA 5030B2.5107-13-106/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L1Benzene1.07060218EPA 5030B0.271-43-206/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L1Bromochloromethane3.07060218EPA 5030B0.574-97-506/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L1Bromodichloromethane1.07060218EPA 5030B0.475-27-406/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L1Bromoform3.07060218EPA 5030B0.675-25-206/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L1Bromomethane107060218EPA 5030B1.074-83-906/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L1Carbon Disulfide1007060218EPA 5030B0.875-15-006/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L1Carbon Tetrachloride1.07060218EPA 5030B0.456-23-506/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L1Chlorobenzene3.07060218EPA 5030B0.5108-90-706/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L1Chloroethane107060218EPA 5030B0.575-00-306/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L1Chloroform5.07060218EPA 5030B0.667-66-306/07/17 14:0406/07/17 10:00Page 12 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW4Ground WaterAAF0102-04AAF010205/31/17 12:13Project:Holly Springs Closed C&D Landfill06/02/17 09:05Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L1Chloromethane1.07060218EPA 5030B0.474-87-306/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L1Dibromochloromethane3.07060218EPA 5030B0.3124-48-106/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L11,2-Dibromo-3-chloropropane137060218EPA 5030B0.696-12-806/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L11,2-Dibromoethane1.07060218EPA 5030B0.3106-93-406/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L1Dibromomethane107060218EPA 5030B0.674-95-306/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L11,2-Dichlorobenzene5.07060218EPA 5030B0.595-50-106/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L11,4-Dichlorobenzene1.07060218EPA 5030B0.6106-46-706/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L1trans-1,4-Dichloro-2-butene1007060218EPA 5030B1.6110-57-606/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L11,1-Dichloroethane5.07060218EPA 5030B0.475-34-306/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L11,2-Dichloroethane1.07060218EPA 5030B0.7107-06-206/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L11,1-Dichloroethene5.07060218EPA 5030B0.775-35-406/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L1cis-1,2-Dichloroethene5.07060218EPA 5030B0.7156-59-206/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L1trans-1,2-Dichloroethene5.07060218EPA 5030B0.5156-60-506/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L11,2-Dichloropropane1.07060218EPA 5030B0.678-87-506/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L1cis-1,3-Dichloropropene1.07060218EPA 5030B0.210061-01-506/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L1trans-1,3-Dichloropropene1.07060218EPA 5030B0.310061-02-606/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L1Ethylbenzene1.07060218EPA 5030B0.4100-41-406/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L1Iodomethane107060218EPA 5030B3.174-88-406/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L1Methyl Butyl Ketone (2-Hexanone)507060218EPA 5030B0.9591-78-606/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L1Methylene Chloride1.07060218EPA 5030B0.575-09-206/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L1Methyl Ethyl Ketone (2-Butanone)1007060218EPA 5030B3.278-93-306/07/17 14:0406/07/17 10:00Page 13 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW4Ground WaterAAF0102-04AAF010205/31/17 12:13Project:Holly Springs Closed C&D Landfill06/02/17 09:05Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L14-Methyl-2-pentanone (MIBK)1007060218EPA 5030B0.9108-10-106/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L1Styrene1.07060218EPA 5030B0.5100-42-506/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L11,1,1,2-Tetrachloroethane5.07060218EPA 5030B0.3630-20-606/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L11,1,2,2-Tetrachloroethane3.07060218EPA 5030B0.579-34-506/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L1Tetrachloroethene1.07060218EPA 5030B0.8127-18-406/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L1Toluene1.07060218EPA 5030B0.3108-88-306/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L11,1,1-Trichloroethane1.07060218EPA 5030B0.471-55-606/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L11,1,2-Trichloroethane1.07060218EPA 5030B0.679-00-506/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L1Trichloroethene1.07060218EPA 5030B0.379-01-606/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L1Trichlorofluoromethane1.07060218EPA 5030B0.575-69-406/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L11,2,3-Trichloropropane1.07060218EPA 5030B0.596-18-406/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L1Vinyl Acetate507060218EPA 5030B0.4108-05-406/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L1Vinyl Chloride1.07060218EPA 5030B0.675-01-406/07/17 14:0406/07/17 10:00NDEPA 8260Bug/L1Xylenes, total5.07060218EPA 5030B0.91330-20-706/07/17 14:0406/07/17 10:00EPA 8260B1.9ug/L1Tetrahydrofuran10J7060218EPA 5030B1.3109-99-906/07/17 14:0406/07/17 10:00EPA 8260B91 %Surr: Dibromofluoromethane7060218EPA 5030B1868-53-706/07/17 14:0406/07/17 10:0080-120EPA 8260B96 %Surr: 1,2-Dichloroethane-d47060218EPA 5030B17060-07-006/07/17 14:0406/07/17 10:0078-120EPA 8260B99 %Surr: Toluene-d87060218EPA 5030B2037-26-506/07/17 14:0406/07/17 10:0080-120EPA 8260B99 %Surr: 4-Bromofluorobenzene7060218EPA 5030B460-00-406/07/17 14:0406/07/17 10:0080-120Page 14 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW5RGround WaterAAF0102-05AAF010205/31/17 13:25Project:Holly Springs Closed C&D Landfill06/02/17 09:05Metals, TotalEPA 6020B2.90ug/L1Arsenic10.0J7060188EPA 3005A0.427440-38-206/10/17 20:4206/07/17 14:15EPA 6020B160ug/L1Barium1007060188EPA 3005A0.277440-39-306/10/17 20:4206/07/17 14:15EPA 6020B0.10ug/L1Cadmium1.00J7060188EPA 3005A0.067440-43-906/10/17 20:4206/07/17 14:15EPA 6020B1.15ug/L1Chromium10.0J7060188EPA 3005A0.347440-47-306/10/17 20:4206/07/17 14:15EPA 6020B0.51ug/L1Lead10.0J7060188EPA 3005A0.077439-92-106/10/17 20:4206/07/17 14:15NDEPA 6020Bug/L1Selenium10.07060188EPA 3005A1.417782-49-206/10/17 20:4206/07/17 14:15NDEPA 6020Bug/L1Silver10.07060188EPA 3005A0.327440-22-406/10/17 20:4206/07/17 14:15NDEPA 7470Aug/L1Mercury0.2007060107EPA 7470A0.0417439-97-606/06/17 14:0406/06/17 10:35Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L1Acetone1007060218EPA 5030B8.267-64-106/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L1Acrylonitrile2007060218EPA 5030B2.5107-13-106/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L1Benzene1.07060218EPA 5030B0.271-43-206/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L1Bromochloromethane3.07060218EPA 5030B0.574-97-506/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L1Bromodichloromethane1.07060218EPA 5030B0.475-27-406/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L1Bromoform3.07060218EPA 5030B0.675-25-206/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L1Bromomethane107060218EPA 5030B1.074-83-906/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L1Carbon Disulfide1007060218EPA 5030B0.875-15-006/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L1Carbon Tetrachloride1.07060218EPA 5030B0.456-23-506/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L1Chlorobenzene3.07060218EPA 5030B0.5108-90-706/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L1Chloroethane107060218EPA 5030B0.575-00-306/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L1Chloroform5.07060218EPA 5030B0.667-66-306/07/17 14:3006/07/17 10:00Page 15 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW5RGround WaterAAF0102-05AAF010205/31/17 13:25Project:Holly Springs Closed C&D Landfill06/02/17 09:05Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L1Chloromethane1.07060218EPA 5030B0.474-87-306/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L1Dibromochloromethane3.07060218EPA 5030B0.3124-48-106/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L11,2-Dibromo-3-chloropropane137060218EPA 5030B0.696-12-806/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L11,2-Dibromoethane1.07060218EPA 5030B0.3106-93-406/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L1Dibromomethane107060218EPA 5030B0.674-95-306/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L11,2-Dichlorobenzene5.07060218EPA 5030B0.595-50-106/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L11,4-Dichlorobenzene1.07060218EPA 5030B0.6106-46-706/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L1trans-1,4-Dichloro-2-butene1007060218EPA 5030B1.6110-57-606/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L11,1-Dichloroethane5.07060218EPA 5030B0.475-34-306/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L11,2-Dichloroethane1.07060218EPA 5030B0.7107-06-206/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L11,1-Dichloroethene5.07060218EPA 5030B0.775-35-406/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L1cis-1,2-Dichloroethene5.07060218EPA 5030B0.7156-59-206/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L1trans-1,2-Dichloroethene5.07060218EPA 5030B0.5156-60-506/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L11,2-Dichloropropane1.07060218EPA 5030B0.678-87-506/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L1cis-1,3-Dichloropropene1.07060218EPA 5030B0.210061-01-506/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L1trans-1,3-Dichloropropene1.07060218EPA 5030B0.310061-02-606/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L1Ethylbenzene1.07060218EPA 5030B0.4100-41-406/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L1Iodomethane107060218EPA 5030B3.174-88-406/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L1Methyl Butyl Ketone (2-Hexanone)507060218EPA 5030B0.9591-78-606/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L1Methylene Chloride1.07060218EPA 5030B0.575-09-206/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L1Methyl Ethyl Ketone (2-Butanone)1007060218EPA 5030B3.278-93-306/07/17 14:3006/07/17 10:00Page 16 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW5RGround WaterAAF0102-05AAF010205/31/17 13:25Project:Holly Springs Closed C&D Landfill06/02/17 09:05Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L14-Methyl-2-pentanone (MIBK)1007060218EPA 5030B0.9108-10-106/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L1Styrene1.07060218EPA 5030B0.5100-42-506/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L11,1,1,2-Tetrachloroethane5.07060218EPA 5030B0.3630-20-606/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L11,1,2,2-Tetrachloroethane3.07060218EPA 5030B0.579-34-506/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L1Tetrachloroethene1.07060218EPA 5030B0.8127-18-406/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L1Toluene1.07060218EPA 5030B0.3108-88-306/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L11,1,1-Trichloroethane1.07060218EPA 5030B0.471-55-606/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L11,1,2-Trichloroethane1.07060218EPA 5030B0.679-00-506/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L1Trichloroethene1.07060218EPA 5030B0.379-01-606/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L1Trichlorofluoromethane1.07060218EPA 5030B0.575-69-406/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L11,2,3-Trichloropropane1.07060218EPA 5030B0.596-18-406/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L1Vinyl Acetate507060218EPA 5030B0.4108-05-406/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L1Vinyl Chloride1.07060218EPA 5030B0.675-01-406/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L1Xylenes, total5.07060218EPA 5030B0.91330-20-706/07/17 14:3006/07/17 10:00NDEPA 8260Bug/L1Tetrahydrofuran107060218EPA 5030B1.3109-99-906/07/17 14:3006/07/17 10:00EPA 8260B90 %Surr: Dibromofluoromethane7060218EPA 5030B1868-53-706/07/17 14:3006/07/17 10:0080-120EPA 8260B97 %Surr: 1,2-Dichloroethane-d47060218EPA 5030B17060-07-006/07/17 14:3006/07/17 10:0078-120EPA 8260B99 %Surr: Toluene-d87060218EPA 5030B2037-26-506/07/17 14:3006/07/17 10:0080-120EPA 8260B99 %Surr: 4-Bromofluorobenzene7060218EPA 5030B460-00-406/07/17 14:3006/07/17 10:0080-120Page 17 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW6Ground WaterAAF0102-06AAF010205/31/17 13:54Project:Holly Springs Closed C&D Landfill06/02/17 09:05Metals, TotalEPA 6020B2.10ug/L1Arsenic10.0J7060188EPA 3005A0.427440-38-206/10/17 21:0006/07/17 14:15EPA 6020B298ug/L1Barium1007060188EPA 3005A0.277440-39-306/10/17 21:0006/07/17 14:15NDEPA 6020Bug/L1Cadmium1.007060188EPA 3005A0.067440-43-906/10/17 21:0006/07/17 14:15EPA 6020B0.88ug/L1Chromium10.0J7060188EPA 3005A0.347440-47-306/10/17 21:0006/07/17 14:15NDEPA 6020Bug/L1Lead10.07060188EPA 3005A0.077439-92-106/10/17 21:0006/07/17 14:15NDEPA 6020Bug/L1Selenium10.07060188EPA 3005A1.417782-49-206/10/17 21:0006/07/17 14:15NDEPA 6020Bug/L1Silver10.07060188EPA 3005A0.327440-22-406/10/17 21:0006/07/17 14:15NDEPA 7470Aug/L1Mercury0.2007060107EPA 7470A0.0417439-97-606/06/17 14:0606/06/17 10:35Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L1Acetone1007060218EPA 5030B8.267-64-106/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L1Acrylonitrile2007060218EPA 5030B2.5107-13-106/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L1Benzene1.07060218EPA 5030B0.271-43-206/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L1Bromochloromethane3.07060218EPA 5030B0.574-97-506/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L1Bromodichloromethane1.07060218EPA 5030B0.475-27-406/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L1Bromoform3.07060218EPA 5030B0.675-25-206/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L1Bromomethane107060218EPA 5030B1.074-83-906/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L1Carbon Disulfide1007060218EPA 5030B0.875-15-006/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L1Carbon Tetrachloride1.07060218EPA 5030B0.456-23-506/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L1Chlorobenzene3.07060218EPA 5030B0.5108-90-706/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L1Chloroethane107060218EPA 5030B0.575-00-306/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L1Chloroform5.07060218EPA 5030B0.667-66-306/07/17 14:5606/07/17 10:00Page 18 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW6Ground WaterAAF0102-06AAF010205/31/17 13:54Project:Holly Springs Closed C&D Landfill06/02/17 09:05Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L1Chloromethane1.07060218EPA 5030B0.474-87-306/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L1Dibromochloromethane3.07060218EPA 5030B0.3124-48-106/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L11,2-Dibromo-3-chloropropane137060218EPA 5030B0.696-12-806/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L11,2-Dibromoethane1.07060218EPA 5030B0.3106-93-406/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L1Dibromomethane107060218EPA 5030B0.674-95-306/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L11,2-Dichlorobenzene5.07060218EPA 5030B0.595-50-106/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L11,4-Dichlorobenzene1.07060218EPA 5030B0.6106-46-706/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L1trans-1,4-Dichloro-2-butene1007060218EPA 5030B1.6110-57-606/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L11,1-Dichloroethane5.07060218EPA 5030B0.475-34-306/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L11,2-Dichloroethane1.07060218EPA 5030B0.7107-06-206/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L11,1-Dichloroethene5.07060218EPA 5030B0.775-35-406/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L1cis-1,2-Dichloroethene5.07060218EPA 5030B0.7156-59-206/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L1trans-1,2-Dichloroethene5.07060218EPA 5030B0.5156-60-506/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L11,2-Dichloropropane1.07060218EPA 5030B0.678-87-506/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L1cis-1,3-Dichloropropene1.07060218EPA 5030B0.210061-01-506/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L1trans-1,3-Dichloropropene1.07060218EPA 5030B0.310061-02-606/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L1Ethylbenzene1.07060218EPA 5030B0.4100-41-406/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L1Iodomethane107060218EPA 5030B3.174-88-406/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L1Methyl Butyl Ketone (2-Hexanone)507060218EPA 5030B0.9591-78-606/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L1Methylene Chloride1.07060218EPA 5030B0.575-09-206/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L1Methyl Ethyl Ketone (2-Butanone)1007060218EPA 5030B3.278-93-306/07/17 14:5606/07/17 10:00Page 19 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW6Ground WaterAAF0102-06AAF010205/31/17 13:54Project:Holly Springs Closed C&D Landfill06/02/17 09:05Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L14-Methyl-2-pentanone (MIBK)1007060218EPA 5030B0.9108-10-106/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L1Styrene1.07060218EPA 5030B0.5100-42-506/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L11,1,1,2-Tetrachloroethane5.07060218EPA 5030B0.3630-20-606/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L11,1,2,2-Tetrachloroethane3.07060218EPA 5030B0.579-34-506/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L1Tetrachloroethene1.07060218EPA 5030B0.8127-18-406/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L1Toluene1.07060218EPA 5030B0.3108-88-306/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L11,1,1-Trichloroethane1.07060218EPA 5030B0.471-55-606/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L11,1,2-Trichloroethane1.07060218EPA 5030B0.679-00-506/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L1Trichloroethene1.07060218EPA 5030B0.379-01-606/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L1Trichlorofluoromethane1.07060218EPA 5030B0.575-69-406/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L11,2,3-Trichloropropane1.07060218EPA 5030B0.596-18-406/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L1Vinyl Acetate507060218EPA 5030B0.4108-05-406/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L1Vinyl Chloride1.07060218EPA 5030B0.675-01-406/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L1Xylenes, total5.07060218EPA 5030B0.91330-20-706/07/17 14:5606/07/17 10:00NDEPA 8260Bug/L1Tetrahydrofuran107060218EPA 5030B1.3109-99-906/07/17 14:5606/07/17 10:00EPA 8260B92 %Surr: Dibromofluoromethane7060218EPA 5030B1868-53-706/07/17 14:5606/07/17 10:0080-120EPA 8260B99 %Surr: 1,2-Dichloroethane-d47060218EPA 5030B17060-07-006/07/17 14:5606/07/17 10:0078-120EPA 8260B100 %Surr: Toluene-d87060218EPA 5030B2037-26-506/07/17 14:5606/07/17 10:0080-120EPA 8260B98 %Surr: 4-Bromofluorobenzene7060218EPA 5030B460-00-406/07/17 14:5606/07/17 10:0080-120Page 20 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW7Ground WaterAAF0102-07AAF010205/31/17 12:32Project:Holly Springs Closed C&D Landfill06/02/17 09:05Metals, TotalEPA 6020B2.98ug/L1Arsenic10.0J7060188EPA 3005A0.427440-38-206/10/17 21:0506/07/17 14:15EPA 6020B166ug/L1Barium1007060188EPA 3005A0.277440-39-306/10/17 21:0506/07/17 14:15NDEPA 6020Bug/L1Cadmium1.007060188EPA 3005A0.067440-43-906/10/17 21:0506/07/17 14:15NDEPA 6020Bug/L1Chromium10.07060188EPA 3005A0.347440-47-306/10/17 21:0506/07/17 14:15NDEPA 6020Bug/L1Lead10.07060188EPA 3005A0.077439-92-106/10/17 21:0506/07/17 14:15NDEPA 6020Bug/L1Selenium10.07060188EPA 3005A1.417782-49-206/10/17 21:0506/07/17 14:15NDEPA 6020Bug/L1Silver10.07060188EPA 3005A0.327440-22-406/10/17 21:0506/07/17 14:15EPA 7470A0.146ug/L1Mercury0.200J7060107EPA 7470A0.0417439-97-606/06/17 14:0906/06/17 10:35Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L1Acetone1007060218EPA 5030B8.267-64-106/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L1Acrylonitrile2007060218EPA 5030B2.5107-13-106/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L1Benzene1.07060218EPA 5030B0.271-43-206/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L1Bromochloromethane3.07060218EPA 5030B0.574-97-506/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L1Bromodichloromethane1.07060218EPA 5030B0.475-27-406/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L1Bromoform3.07060218EPA 5030B0.675-25-206/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L1Bromomethane107060218EPA 5030B1.074-83-906/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L1Carbon Disulfide1007060218EPA 5030B0.875-15-006/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L1Carbon Tetrachloride1.07060218EPA 5030B0.456-23-506/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L1Chlorobenzene3.07060218EPA 5030B0.5108-90-706/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L1Chloroethane107060218EPA 5030B0.575-00-306/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L1Chloroform5.07060218EPA 5030B0.667-66-306/07/17 15:2306/07/17 10:00Page 21 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW7Ground WaterAAF0102-07AAF010205/31/17 12:32Project:Holly Springs Closed C&D Landfill06/02/17 09:05Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L1Chloromethane1.07060218EPA 5030B0.474-87-306/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L1Dibromochloromethane3.07060218EPA 5030B0.3124-48-106/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L11,2-Dibromo-3-chloropropane137060218EPA 5030B0.696-12-806/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L11,2-Dibromoethane1.07060218EPA 5030B0.3106-93-406/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L1Dibromomethane107060218EPA 5030B0.674-95-306/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L11,2-Dichlorobenzene5.07060218EPA 5030B0.595-50-106/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L11,4-Dichlorobenzene1.07060218EPA 5030B0.6106-46-706/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L1trans-1,4-Dichloro-2-butene1007060218EPA 5030B1.6110-57-606/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L11,1-Dichloroethane5.07060218EPA 5030B0.475-34-306/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L11,2-Dichloroethane1.07060218EPA 5030B0.7107-06-206/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L11,1-Dichloroethene5.07060218EPA 5030B0.775-35-406/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L1cis-1,2-Dichloroethene5.07060218EPA 5030B0.7156-59-206/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L1trans-1,2-Dichloroethene5.07060218EPA 5030B0.5156-60-506/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L11,2-Dichloropropane1.07060218EPA 5030B0.678-87-506/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L1cis-1,3-Dichloropropene1.07060218EPA 5030B0.210061-01-506/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L1trans-1,3-Dichloropropene1.07060218EPA 5030B0.310061-02-606/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L1Ethylbenzene1.07060218EPA 5030B0.4100-41-406/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L1Iodomethane107060218EPA 5030B3.174-88-406/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L1Methyl Butyl Ketone (2-Hexanone)507060218EPA 5030B0.9591-78-606/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L1Methylene Chloride1.07060218EPA 5030B0.575-09-206/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L1Methyl Ethyl Ketone (2-Butanone)1007060218EPA 5030B3.278-93-306/07/17 15:2306/07/17 10:00Page 22 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW7Ground WaterAAF0102-07AAF010205/31/17 12:32Project:Holly Springs Closed C&D Landfill06/02/17 09:05Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L14-Methyl-2-pentanone (MIBK)1007060218EPA 5030B0.9108-10-106/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L1Styrene1.07060218EPA 5030B0.5100-42-506/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L11,1,1,2-Tetrachloroethane5.07060218EPA 5030B0.3630-20-606/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L11,1,2,2-Tetrachloroethane3.07060218EPA 5030B0.579-34-506/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L1Tetrachloroethene1.07060218EPA 5030B0.8127-18-406/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L1Toluene1.07060218EPA 5030B0.3108-88-306/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L11,1,1-Trichloroethane1.07060218EPA 5030B0.471-55-606/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L11,1,2-Trichloroethane1.07060218EPA 5030B0.679-00-506/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L1Trichloroethene1.07060218EPA 5030B0.379-01-606/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L1Trichlorofluoromethane1.07060218EPA 5030B0.575-69-406/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L11,2,3-Trichloropropane1.07060218EPA 5030B0.596-18-406/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L1Vinyl Acetate507060218EPA 5030B0.4108-05-406/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L1Vinyl Chloride1.07060218EPA 5030B0.675-01-406/07/17 15:2306/07/17 10:00NDEPA 8260Bug/L1Xylenes, total5.07060218EPA 5030B0.91330-20-706/07/17 15:2306/07/17 10:00EPA 8260B1.6ug/L1Tetrahydrofuran10J7060218EPA 5030B1.3109-99-906/07/17 15:2306/07/17 10:00EPA 8260B88 %Surr: Dibromofluoromethane7060218EPA 5030B1868-53-706/07/17 15:2306/07/17 10:0080-120EPA 8260B97 %Surr: 1,2-Dichloroethane-d47060218EPA 5030B17060-07-006/07/17 15:2306/07/17 10:0078-120EPA 8260B99 %Surr: Toluene-d87060218EPA 5030B2037-26-506/07/17 15:2306/07/17 10:0080-120EPA 8260B97 %Surr: 4-Bromofluorobenzene7060218EPA 5030B460-00-406/07/17 15:2306/07/17 10:0080-120Page 23 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW9Ground WaterAAF0102-08AAF010205/31/17 14:24Project:Holly Springs Closed C&D Landfill06/02/17 09:05Metals, TotalEPA 6020B1.13ug/L1Arsenic10.0J7060188EPA 3005A0.427440-38-206/10/17 21:1106/07/17 14:15EPA 6020B77.6ug/L1Barium100J7060188EPA 3005A0.277440-39-306/10/17 21:1106/07/17 14:15EPA 6020B0.25ug/L1Cadmium1.00J7060188EPA 3005A0.067440-43-906/10/17 21:1106/07/17 14:15EPA 6020B1.05ug/L1Chromium10.0J7060188EPA 3005A0.347440-47-306/10/17 21:1106/07/17 14:15EPA 6020B1.12ug/L1Lead10.0J7060188EPA 3005A0.077439-92-106/10/17 21:1106/07/17 14:15NDEPA 6020Bug/L1Selenium10.07060188EPA 3005A1.417782-49-206/10/17 21:1106/07/17 14:15NDEPA 6020Bug/L1Silver10.07060188EPA 3005A0.327440-22-406/10/17 21:1106/07/17 14:15NDEPA 7470Aug/L1Mercury0.2007060107EPA 7470A0.0417439-97-606/06/17 14:1106/06/17 10:35Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L1Acetone1007060218EPA 5030B8.267-64-106/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L1Acrylonitrile2007060218EPA 5030B2.5107-13-106/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L1Benzene1.07060218EPA 5030B0.271-43-206/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L1Bromochloromethane3.07060218EPA 5030B0.574-97-506/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L1Bromodichloromethane1.07060218EPA 5030B0.475-27-406/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L1Bromoform3.07060218EPA 5030B0.675-25-206/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L1Bromomethane107060218EPA 5030B1.074-83-906/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L1Carbon Disulfide1007060218EPA 5030B0.875-15-006/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L1Carbon Tetrachloride1.07060218EPA 5030B0.456-23-506/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L1Chlorobenzene3.07060218EPA 5030B0.5108-90-706/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L1Chloroethane107060218EPA 5030B0.575-00-306/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L1Chloroform5.07060218EPA 5030B0.667-66-306/07/17 16:4206/07/17 10:00Page 24 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW9Ground WaterAAF0102-08AAF010205/31/17 14:24Project:Holly Springs Closed C&D Landfill06/02/17 09:05Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L1Chloromethane1.07060218EPA 5030B0.474-87-306/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L1Dibromochloromethane3.07060218EPA 5030B0.3124-48-106/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L11,2-Dibromo-3-chloropropane137060218EPA 5030B0.696-12-806/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L11,2-Dibromoethane1.07060218EPA 5030B0.3106-93-406/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L1Dibromomethane107060218EPA 5030B0.674-95-306/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L11,2-Dichlorobenzene5.07060218EPA 5030B0.595-50-106/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L11,4-Dichlorobenzene1.07060218EPA 5030B0.6106-46-706/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L1trans-1,4-Dichloro-2-butene1007060218EPA 5030B1.6110-57-606/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L11,1-Dichloroethane5.07060218EPA 5030B0.475-34-306/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L11,2-Dichloroethane1.07060218EPA 5030B0.7107-06-206/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L11,1-Dichloroethene5.07060218EPA 5030B0.775-35-406/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L1cis-1,2-Dichloroethene5.07060218EPA 5030B0.7156-59-206/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L1trans-1,2-Dichloroethene5.07060218EPA 5030B0.5156-60-506/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L11,2-Dichloropropane1.07060218EPA 5030B0.678-87-506/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L1cis-1,3-Dichloropropene1.07060218EPA 5030B0.210061-01-506/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L1trans-1,3-Dichloropropene1.07060218EPA 5030B0.310061-02-606/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L1Ethylbenzene1.07060218EPA 5030B0.4100-41-406/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L1Iodomethane107060218EPA 5030B3.174-88-406/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L1Methyl Butyl Ketone (2-Hexanone)507060218EPA 5030B0.9591-78-606/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L1Methylene Chloride1.07060218EPA 5030B0.575-09-206/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L1Methyl Ethyl Ketone (2-Butanone)1007060218EPA 5030B3.278-93-306/07/17 16:4206/07/17 10:00Page 25 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW9Ground WaterAAF0102-08AAF010205/31/17 14:24Project:Holly Springs Closed C&D Landfill06/02/17 09:05Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L14-Methyl-2-pentanone (MIBK)1007060218EPA 5030B0.9108-10-106/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L1Styrene1.07060218EPA 5030B0.5100-42-506/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L11,1,1,2-Tetrachloroethane5.07060218EPA 5030B0.3630-20-606/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L11,1,2,2-Tetrachloroethane3.07060218EPA 5030B0.579-34-506/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L1Tetrachloroethene1.07060218EPA 5030B0.8127-18-406/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L1Toluene1.07060218EPA 5030B0.3108-88-306/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L11,1,1-Trichloroethane1.07060218EPA 5030B0.471-55-606/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L11,1,2-Trichloroethane1.07060218EPA 5030B0.679-00-506/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L1Trichloroethene1.07060218EPA 5030B0.379-01-606/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L1Trichlorofluoromethane1.07060218EPA 5030B0.575-69-406/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L11,2,3-Trichloropropane1.07060218EPA 5030B0.596-18-406/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L1Vinyl Acetate507060218EPA 5030B0.4108-05-406/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L1Vinyl Chloride1.07060218EPA 5030B0.675-01-406/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L1Xylenes, total5.07060218EPA 5030B0.91330-20-706/07/17 16:4206/07/17 10:00NDEPA 8260Bug/L1Tetrahydrofuran107060218EPA 5030B1.3109-99-906/07/17 16:4206/07/17 10:00EPA 8260B93 %Surr: Dibromofluoromethane7060218EPA 5030B1868-53-706/07/17 16:4206/07/17 10:0080-120EPA 8260B99 %Surr: 1,2-Dichloroethane-d47060218EPA 5030B17060-07-006/07/17 16:4206/07/17 10:0078-120EPA 8260B98 %Surr: Toluene-d87060218EPA 5030B2037-26-506/07/17 16:4206/07/17 10:0080-120EPA 8260B100 %Surr: 4-Bromofluorobenzene7060218EPA 5030B460-00-406/07/17 16:4206/07/17 10:0080-120Page 26 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW10Ground WaterAAF0102-09AAF010205/31/17 11:37Project:Holly Springs Closed C&D Landfill06/02/17 09:05Metals, TotalEPA 6020B6.79ug/L1Arsenic10.0J7060188EPA 3005A0.427440-38-206/10/17 21:1706/07/17 14:15EPA 6020B20.7ug/L1Barium100J7060188EPA 3005A0.277440-39-306/10/17 21:1706/07/17 14:15NDEPA 6020Bug/L1Cadmium1.007060188EPA 3005A0.067440-43-906/10/17 21:1706/07/17 14:15EPA 6020B1.04ug/L1Chromium10.0J7060188EPA 3005A0.347440-47-306/10/17 21:1706/07/17 14:15NDEPA 6020Bug/L1Lead10.07060188EPA 3005A0.077439-92-106/10/17 21:1706/07/17 14:15NDEPA 6020Bug/L1Selenium10.07060188EPA 3005A1.417782-49-206/10/17 21:1706/07/17 14:15NDEPA 6020Bug/L1Silver10.07060188EPA 3005A0.327440-22-406/10/17 21:1706/07/17 14:15NDEPA 7470Aug/L1Mercury0.2007060107EPA 7470A0.0417439-97-606/06/17 14:1406/06/17 10:35Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L1Acetone1007060218EPA 5030B8.267-64-106/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L1Acrylonitrile2007060218EPA 5030B2.5107-13-106/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L1Benzene1.07060218EPA 5030B0.271-43-206/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L1Bromochloromethane3.07060218EPA 5030B0.574-97-506/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L1Bromodichloromethane1.07060218EPA 5030B0.475-27-406/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L1Bromoform3.07060218EPA 5030B0.675-25-206/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L1Bromomethane107060218EPA 5030B1.074-83-906/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L1Carbon Disulfide1007060218EPA 5030B0.875-15-006/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L1Carbon Tetrachloride1.07060218EPA 5030B0.456-23-506/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L1Chlorobenzene3.07060218EPA 5030B0.5108-90-706/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L1Chloroethane107060218EPA 5030B0.575-00-306/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L1Chloroform5.07060218EPA 5030B0.667-66-306/07/17 17:0906/07/17 10:00Page 27 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW10Ground WaterAAF0102-09AAF010205/31/17 11:37Project:Holly Springs Closed C&D Landfill06/02/17 09:05Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L1Chloromethane1.07060218EPA 5030B0.474-87-306/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L1Dibromochloromethane3.07060218EPA 5030B0.3124-48-106/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L11,2-Dibromo-3-chloropropane137060218EPA 5030B0.696-12-806/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L11,2-Dibromoethane1.07060218EPA 5030B0.3106-93-406/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L1Dibromomethane107060218EPA 5030B0.674-95-306/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L11,2-Dichlorobenzene5.07060218EPA 5030B0.595-50-106/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L11,4-Dichlorobenzene1.07060218EPA 5030B0.6106-46-706/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L1trans-1,4-Dichloro-2-butene1007060218EPA 5030B1.6110-57-606/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L11,1-Dichloroethane5.07060218EPA 5030B0.475-34-306/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L11,2-Dichloroethane1.07060218EPA 5030B0.7107-06-206/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L11,1-Dichloroethene5.07060218EPA 5030B0.775-35-406/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L1cis-1,2-Dichloroethene5.07060218EPA 5030B0.7156-59-206/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L1trans-1,2-Dichloroethene5.07060218EPA 5030B0.5156-60-506/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L11,2-Dichloropropane1.07060218EPA 5030B0.678-87-506/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L1cis-1,3-Dichloropropene1.07060218EPA 5030B0.210061-01-506/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L1trans-1,3-Dichloropropene1.07060218EPA 5030B0.310061-02-606/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L1Ethylbenzene1.07060218EPA 5030B0.4100-41-406/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L1Iodomethane107060218EPA 5030B3.174-88-406/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L1Methyl Butyl Ketone (2-Hexanone)507060218EPA 5030B0.9591-78-606/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L1Methylene Chloride1.07060218EPA 5030B0.575-09-206/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L1Methyl Ethyl Ketone (2-Butanone)1007060218EPA 5030B3.278-93-306/07/17 17:0906/07/17 10:00Page 28 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW10Ground WaterAAF0102-09AAF010205/31/17 11:37Project:Holly Springs Closed C&D Landfill06/02/17 09:05Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L14-Methyl-2-pentanone (MIBK)1007060218EPA 5030B0.9108-10-106/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L1Styrene1.07060218EPA 5030B0.5100-42-506/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L11,1,1,2-Tetrachloroethane5.07060218EPA 5030B0.3630-20-606/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L11,1,2,2-Tetrachloroethane3.07060218EPA 5030B0.579-34-506/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L1Tetrachloroethene1.07060218EPA 5030B0.8127-18-406/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L1Toluene1.07060218EPA 5030B0.3108-88-306/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L11,1,1-Trichloroethane1.07060218EPA 5030B0.471-55-606/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L11,1,2-Trichloroethane1.07060218EPA 5030B0.679-00-506/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L1Trichloroethene1.07060218EPA 5030B0.379-01-606/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L1Trichlorofluoromethane1.07060218EPA 5030B0.575-69-406/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L11,2,3-Trichloropropane1.07060218EPA 5030B0.596-18-406/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L1Vinyl Acetate507060218EPA 5030B0.4108-05-406/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L1Vinyl Chloride1.07060218EPA 5030B0.675-01-406/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L1Xylenes, total5.07060218EPA 5030B0.91330-20-706/07/17 17:0906/07/17 10:00NDEPA 8260Bug/L1Tetrahydrofuran107060218EPA 5030B1.3109-99-906/07/17 17:0906/07/17 10:00EPA 8260B91 %Surr: Dibromofluoromethane7060218EPA 5030B1868-53-706/07/17 17:0906/07/17 10:0080-120EPA 8260B99 %Surr: 1,2-Dichloroethane-d47060218EPA 5030B17060-07-006/07/17 17:0906/07/17 10:0078-120EPA 8260B100 %Surr: Toluene-d87060218EPA 5030B2037-26-506/07/17 17:0906/07/17 10:0080-120EPA 8260B101 %Surr: 4-Bromofluorobenzene7060218EPA 5030B460-00-406/07/17 17:0906/07/17 10:0080-120Page 29 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW11Ground WaterAAF0102-10AAF010205/31/17 12:49Project:Holly Springs Closed C&D Landfill06/02/17 09:05Metals, TotalEPA 6020B1.63ug/L1Arsenic10.0J7060188EPA 3005A0.427440-38-206/10/17 21:2206/07/17 14:15EPA 6020B53.2ug/L1Barium100J7060188EPA 3005A0.277440-39-306/10/17 21:2206/07/17 14:15NDEPA 6020Bug/L1Cadmium1.007060188EPA 3005A0.067440-43-906/10/17 21:2206/07/17 14:15EPA 6020B1.28ug/L1Chromium10.0J7060188EPA 3005A0.347440-47-306/10/17 21:2206/07/17 14:15NDEPA 6020Bug/L1Lead10.07060188EPA 3005A0.077439-92-106/10/17 21:2206/07/17 14:15NDEPA 6020Bug/L1Selenium10.07060188EPA 3005A1.417782-49-206/10/17 21:2206/07/17 14:15NDEPA 6020Bug/L1Silver10.07060188EPA 3005A0.327440-22-406/10/17 21:2206/07/17 14:15NDEPA 7470Aug/L1Mercury0.2007060107EPA 7470A0.0417439-97-606/06/17 14:1606/06/17 10:35Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L1Acetone1007060218EPA 5030B8.267-64-106/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L1Acrylonitrile2007060218EPA 5030B2.5107-13-106/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L1Benzene1.07060218EPA 5030B0.271-43-206/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L1Bromochloromethane3.07060218EPA 5030B0.574-97-506/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L1Bromodichloromethane1.07060218EPA 5030B0.475-27-406/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L1Bromoform3.07060218EPA 5030B0.675-25-206/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L1Bromomethane107060218EPA 5030B1.074-83-906/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L1Carbon Disulfide1007060218EPA 5030B0.875-15-006/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L1Carbon Tetrachloride1.07060218EPA 5030B0.456-23-506/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L1Chlorobenzene3.07060218EPA 5030B0.5108-90-706/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L1Chloroethane107060218EPA 5030B0.575-00-306/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L1Chloroform5.07060218EPA 5030B0.667-66-306/07/17 17:3606/07/17 10:00Page 30 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW11Ground WaterAAF0102-10AAF010205/31/17 12:49Project:Holly Springs Closed C&D Landfill06/02/17 09:05Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L1Chloromethane1.07060218EPA 5030B0.474-87-306/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L1Dibromochloromethane3.07060218EPA 5030B0.3124-48-106/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L11,2-Dibromo-3-chloropropane137060218EPA 5030B0.696-12-806/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L11,2-Dibromoethane1.07060218EPA 5030B0.3106-93-406/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L1Dibromomethane107060218EPA 5030B0.674-95-306/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L11,2-Dichlorobenzene5.07060218EPA 5030B0.595-50-106/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L11,4-Dichlorobenzene1.07060218EPA 5030B0.6106-46-706/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L1trans-1,4-Dichloro-2-butene1007060218EPA 5030B1.6110-57-606/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L11,1-Dichloroethane5.07060218EPA 5030B0.475-34-306/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L11,2-Dichloroethane1.07060218EPA 5030B0.7107-06-206/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L11,1-Dichloroethene5.07060218EPA 5030B0.775-35-406/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L1cis-1,2-Dichloroethene5.07060218EPA 5030B0.7156-59-206/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L1trans-1,2-Dichloroethene5.07060218EPA 5030B0.5156-60-506/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L11,2-Dichloropropane1.07060218EPA 5030B0.678-87-506/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L1cis-1,3-Dichloropropene1.07060218EPA 5030B0.210061-01-506/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L1trans-1,3-Dichloropropene1.07060218EPA 5030B0.310061-02-606/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L1Ethylbenzene1.07060218EPA 5030B0.4100-41-406/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L1Iodomethane107060218EPA 5030B3.174-88-406/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L1Methyl Butyl Ketone (2-Hexanone)507060218EPA 5030B0.9591-78-606/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L1Methylene Chloride1.07060218EPA 5030B0.575-09-206/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L1Methyl Ethyl Ketone (2-Butanone)1007060218EPA 5030B3.278-93-306/07/17 17:3606/07/17 10:00Page 31 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW11Ground WaterAAF0102-10AAF010205/31/17 12:49Project:Holly Springs Closed C&D Landfill06/02/17 09:05Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L14-Methyl-2-pentanone (MIBK)1007060218EPA 5030B0.9108-10-106/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L1Styrene1.07060218EPA 5030B0.5100-42-506/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L11,1,1,2-Tetrachloroethane5.07060218EPA 5030B0.3630-20-606/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L11,1,2,2-Tetrachloroethane3.07060218EPA 5030B0.579-34-506/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L1Tetrachloroethene1.07060218EPA 5030B0.8127-18-406/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L1Toluene1.07060218EPA 5030B0.3108-88-306/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L11,1,1-Trichloroethane1.07060218EPA 5030B0.471-55-606/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L11,1,2-Trichloroethane1.07060218EPA 5030B0.679-00-506/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L1Trichloroethene1.07060218EPA 5030B0.379-01-606/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L1Trichlorofluoromethane1.07060218EPA 5030B0.575-69-406/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L11,2,3-Trichloropropane1.07060218EPA 5030B0.596-18-406/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L1Vinyl Acetate507060218EPA 5030B0.4108-05-406/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L1Vinyl Chloride1.07060218EPA 5030B0.675-01-406/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L1Xylenes, total5.07060218EPA 5030B0.91330-20-706/07/17 17:3606/07/17 10:00NDEPA 8260Bug/L1Tetrahydrofuran107060218EPA 5030B1.3109-99-906/07/17 17:3606/07/17 10:00EPA 8260B92 %Surr: Dibromofluoromethane7060218EPA 5030B1868-53-706/07/17 17:3606/07/17 10:0080-120EPA 8260B99 %Surr: 1,2-Dichloroethane-d47060218EPA 5030B17060-07-006/07/17 17:3606/07/17 10:0078-120EPA 8260B100 %Surr: Toluene-d87060218EPA 5030B2037-26-506/07/17 17:3606/07/17 10:0080-120EPA 8260B98 %Surr: 4-Bromofluorobenzene7060218EPA 5030B460-00-406/07/17 17:3606/07/17 10:0080-120Page 32 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW12Ground WaterAAF0102-11AAF010205/31/17 15:04Project:Holly Springs Closed C&D Landfill06/02/17 09:05Metals, TotalEPA 6020B26.8ug/L1Arsenic10.07060188EPA 3005A0.427440-38-206/10/17 21:2806/07/17 14:15EPA 6020B196ug/L1Barium1007060188EPA 3005A0.277440-39-306/10/17 21:2806/07/17 14:15NDEPA 6020Bug/L1Cadmium1.007060188EPA 3005A0.067440-43-906/10/17 21:2806/07/17 14:15EPA 6020B0.73ug/L1Chromium10.0J7060188EPA 3005A0.347440-47-306/10/17 21:2806/07/17 14:15EPA 6020B0.14ug/L1Lead10.0J7060188EPA 3005A0.077439-92-106/10/17 21:2806/07/17 14:15EPA 6020B1.45ug/L1Selenium10.0J7060188EPA 3005A1.417782-49-206/10/17 21:2806/07/17 14:15NDEPA 6020Bug/L1Silver10.07060188EPA 3005A0.327440-22-406/10/17 21:2806/07/17 14:15NDEPA 7470Aug/L1Mercury0.2007060107EPA 7470A0.0417439-97-606/06/17 14:1806/06/17 10:35Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L1Acetone1007060218EPA 5030B8.267-64-106/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L1Acrylonitrile2007060218EPA 5030B2.5107-13-106/07/17 18:0206/07/17 10:00EPA 8260B0.6ug/L1Benzene1.0J7060218EPA 5030B0.271-43-206/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L1Bromochloromethane3.07060218EPA 5030B0.574-97-506/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L1Bromodichloromethane1.07060218EPA 5030B0.475-27-406/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L1Bromoform3.07060218EPA 5030B0.675-25-206/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L1Bromomethane107060218EPA 5030B1.074-83-906/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L1Carbon Disulfide1007060218EPA 5030B0.875-15-006/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L1Carbon Tetrachloride1.07060218EPA 5030B0.456-23-506/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L1Chlorobenzene3.07060218EPA 5030B0.5108-90-706/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L1Chloroethane107060218EPA 5030B0.575-00-306/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L1Chloroform5.07060218EPA 5030B0.667-66-306/07/17 18:0206/07/17 10:00Page 33 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW12Ground WaterAAF0102-11AAF010205/31/17 15:04Project:Holly Springs Closed C&D Landfill06/02/17 09:05Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L1Chloromethane1.07060218EPA 5030B0.474-87-306/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L1Dibromochloromethane3.07060218EPA 5030B0.3124-48-106/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L11,2-Dibromo-3-chloropropane137060218EPA 5030B0.696-12-806/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L11,2-Dibromoethane1.07060218EPA 5030B0.3106-93-406/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L1Dibromomethane107060218EPA 5030B0.674-95-306/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L11,2-Dichlorobenzene5.07060218EPA 5030B0.595-50-106/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L11,4-Dichlorobenzene1.07060218EPA 5030B0.6106-46-706/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L1trans-1,4-Dichloro-2-butene1007060218EPA 5030B1.6110-57-606/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L11,1-Dichloroethane5.07060218EPA 5030B0.475-34-306/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L11,2-Dichloroethane1.07060218EPA 5030B0.7107-06-206/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L11,1-Dichloroethene5.07060218EPA 5030B0.775-35-406/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L1cis-1,2-Dichloroethene5.07060218EPA 5030B0.7156-59-206/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L1trans-1,2-Dichloroethene5.07060218EPA 5030B0.5156-60-506/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L11,2-Dichloropropane1.07060218EPA 5030B0.678-87-506/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L1cis-1,3-Dichloropropene1.07060218EPA 5030B0.210061-01-506/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L1trans-1,3-Dichloropropene1.07060218EPA 5030B0.310061-02-606/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L1Ethylbenzene1.07060218EPA 5030B0.4100-41-406/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L1Iodomethane107060218EPA 5030B3.174-88-406/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L1Methyl Butyl Ketone (2-Hexanone)507060218EPA 5030B0.9591-78-606/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L1Methylene Chloride1.07060218EPA 5030B0.575-09-206/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L1Methyl Ethyl Ketone (2-Butanone)1007060218EPA 5030B3.278-93-306/07/17 18:0206/07/17 10:00Page 34 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW12Ground WaterAAF0102-11AAF010205/31/17 15:04Project:Holly Springs Closed C&D Landfill06/02/17 09:05Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L14-Methyl-2-pentanone (MIBK)1007060218EPA 5030B0.9108-10-106/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L1Styrene1.07060218EPA 5030B0.5100-42-506/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L11,1,1,2-Tetrachloroethane5.07060218EPA 5030B0.3630-20-606/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L11,1,2,2-Tetrachloroethane3.07060218EPA 5030B0.579-34-506/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L1Tetrachloroethene1.07060218EPA 5030B0.8127-18-406/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L1Toluene1.07060218EPA 5030B0.3108-88-306/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L11,1,1-Trichloroethane1.07060218EPA 5030B0.471-55-606/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L11,1,2-Trichloroethane1.07060218EPA 5030B0.679-00-506/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L1Trichloroethene1.07060218EPA 5030B0.379-01-606/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L1Trichlorofluoromethane1.07060218EPA 5030B0.575-69-406/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L11,2,3-Trichloropropane1.07060218EPA 5030B0.596-18-406/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L1Vinyl Acetate507060218EPA 5030B0.4108-05-406/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L1Vinyl Chloride1.07060218EPA 5030B0.675-01-406/07/17 18:0206/07/17 10:00NDEPA 8260Bug/L1Xylenes, total5.07060218EPA 5030B0.91330-20-706/07/17 18:0206/07/17 10:00EPA 8260B1.8ug/L1Tetrahydrofuran10J7060218EPA 5030B1.3109-99-906/07/17 18:0206/07/17 10:00EPA 8260B93 %Surr: Dibromofluoromethane7060218EPA 5030B1868-53-706/07/17 18:0206/07/17 10:0080-120EPA 8260B99 %Surr: 1,2-Dichloroethane-d47060218EPA 5030B17060-07-006/07/17 18:0206/07/17 10:0078-120EPA 8260B99 %Surr: Toluene-d87060218EPA 5030B2037-26-506/07/17 18:0206/07/17 10:0080-120EPA 8260B98 %Surr: 4-Bromofluorobenzene7060218EPA 5030B460-00-406/07/17 18:0206/07/17 10:0080-120Page 35 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW13Ground WaterAAF0102-12AAF010205/31/17 11:00Project:Holly Springs Closed C&D Landfill06/02/17 09:05Metals, TotalEPA 6020B7.09ug/L1Arsenic10.0J7060188EPA 3005A0.427440-38-206/10/17 21:3406/07/17 14:15EPA 6020B238ug/L1Barium1007060188EPA 3005A0.277440-39-306/10/17 21:3406/07/17 14:15EPA 6020B0.11ug/L1Cadmium1.00J7060188EPA 3005A0.067440-43-906/10/17 21:3406/07/17 14:15EPA 6020B0.36ug/L1Chromium10.0J7060188EPA 3005A0.347440-47-306/10/17 21:3406/07/17 14:15NDEPA 6020Bug/L1Lead10.07060188EPA 3005A0.077439-92-106/10/17 21:3406/07/17 14:15NDEPA 6020Bug/L1Selenium10.07060188EPA 3005A1.417782-49-206/10/17 21:3406/07/17 14:15NDEPA 6020Bug/L1Silver10.07060188EPA 3005A0.327440-22-406/10/17 21:3406/07/17 14:15NDEPA 7470Aug/L1Mercury0.2007060107EPA 7470A0.0417439-97-606/06/17 14:2106/06/17 10:35Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L1Acetone1007060218EPA 5030B8.267-64-106/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L1Acrylonitrile2007060218EPA 5030B2.5107-13-106/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L1Benzene1.07060218EPA 5030B0.271-43-206/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L1Bromochloromethane3.07060218EPA 5030B0.574-97-506/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L1Bromodichloromethane1.07060218EPA 5030B0.475-27-406/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L1Bromoform3.07060218EPA 5030B0.675-25-206/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L1Bromomethane107060218EPA 5030B1.074-83-906/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L1Carbon Disulfide1007060218EPA 5030B0.875-15-006/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L1Carbon Tetrachloride1.07060218EPA 5030B0.456-23-506/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L1Chlorobenzene3.07060218EPA 5030B0.5108-90-706/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L1Chloroethane107060218EPA 5030B0.575-00-306/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L1Chloroform5.07060218EPA 5030B0.667-66-306/07/17 18:2806/07/17 10:00Page 36 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW13Ground WaterAAF0102-12AAF010205/31/17 11:00Project:Holly Springs Closed C&D Landfill06/02/17 09:05Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L1Chloromethane1.07060218EPA 5030B0.474-87-306/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L1Dibromochloromethane3.07060218EPA 5030B0.3124-48-106/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L11,2-Dibromo-3-chloropropane137060218EPA 5030B0.696-12-806/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L11,2-Dibromoethane1.07060218EPA 5030B0.3106-93-406/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L1Dibromomethane107060218EPA 5030B0.674-95-306/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L11,2-Dichlorobenzene5.07060218EPA 5030B0.595-50-106/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L11,4-Dichlorobenzene1.07060218EPA 5030B0.6106-46-706/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L1trans-1,4-Dichloro-2-butene1007060218EPA 5030B1.6110-57-606/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L11,1-Dichloroethane5.07060218EPA 5030B0.475-34-306/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L11,2-Dichloroethane1.07060218EPA 5030B0.7107-06-206/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L11,1-Dichloroethene5.07060218EPA 5030B0.775-35-406/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L1cis-1,2-Dichloroethene5.07060218EPA 5030B0.7156-59-206/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L1trans-1,2-Dichloroethene5.07060218EPA 5030B0.5156-60-506/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L11,2-Dichloropropane1.07060218EPA 5030B0.678-87-506/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L1cis-1,3-Dichloropropene1.07060218EPA 5030B0.210061-01-506/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L1trans-1,3-Dichloropropene1.07060218EPA 5030B0.310061-02-606/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L1Ethylbenzene1.07060218EPA 5030B0.4100-41-406/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L1Iodomethane107060218EPA 5030B3.174-88-406/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L1Methyl Butyl Ketone (2-Hexanone)507060218EPA 5030B0.9591-78-606/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L1Methylene Chloride1.07060218EPA 5030B0.575-09-206/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L1Methyl Ethyl Ketone (2-Butanone)1007060218EPA 5030B3.278-93-306/07/17 18:2806/07/17 10:00Page 37 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-MW13Ground WaterAAF0102-12AAF010205/31/17 11:00Project:Holly Springs Closed C&D Landfill06/02/17 09:05Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L14-Methyl-2-pentanone (MIBK)1007060218EPA 5030B0.9108-10-106/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L1Styrene1.07060218EPA 5030B0.5100-42-506/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L11,1,1,2-Tetrachloroethane5.07060218EPA 5030B0.3630-20-606/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L11,1,2,2-Tetrachloroethane3.07060218EPA 5030B0.579-34-506/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L1Tetrachloroethene1.07060218EPA 5030B0.8127-18-406/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L1Toluene1.07060218EPA 5030B0.3108-88-306/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L11,1,1-Trichloroethane1.07060218EPA 5030B0.471-55-606/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L11,1,2-Trichloroethane1.07060218EPA 5030B0.679-00-506/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L1Trichloroethene1.07060218EPA 5030B0.379-01-606/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L1Trichlorofluoromethane1.07060218EPA 5030B0.575-69-406/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L11,2,3-Trichloropropane1.07060218EPA 5030B0.596-18-406/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L1Vinyl Acetate507060218EPA 5030B0.4108-05-406/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L1Vinyl Chloride1.07060218EPA 5030B0.675-01-406/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L1Xylenes, total5.07060218EPA 5030B0.91330-20-706/07/17 18:2806/07/17 10:00NDEPA 8260Bug/L1Tetrahydrofuran107060218EPA 5030B1.3109-99-906/07/17 18:2806/07/17 10:00EPA 8260B92 %Surr: Dibromofluoromethane7060218EPA 5030B1868-53-706/07/17 18:2806/07/17 10:0080-120EPA 8260B101 %Surr: 1,2-Dichloroethane-d47060218EPA 5030B17060-07-006/07/17 18:2806/07/17 10:0078-120EPA 8260B100 %Surr: Toluene-d87060218EPA 5030B2037-26-506/07/17 18:2806/07/17 10:0080-120EPA 8260B97 %Surr: 4-Bromofluorobenzene7060218EPA 5030B460-00-406/07/17 18:2806/07/17 10:0080-120Page 38 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-SW2Surface WaterAAF0102-13AAF010205/31/17 12:55Project:Holly Springs Closed C&D Landfill06/02/17 09:05Metals, TotalEPA 6020B2.28ug/L1Arsenic10.0J7060188EPA 3005A0.427440-38-206/10/17 21:4006/07/17 14:15EPA 6020B54.8ug/L1Barium100J7060188EPA 3005A0.277440-39-306/10/17 21:4006/07/17 14:15NDEPA 6020Bug/L1Cadmium1.007060188EPA 3005A0.067440-43-906/10/17 21:4006/07/17 14:15EPA 6020B1.12ug/L1Chromium10.0J7060188EPA 3005A0.347440-47-306/10/17 21:4006/07/17 14:15NDEPA 6020Bug/L1Lead10.07060188EPA 3005A0.077439-92-106/10/17 21:4006/07/17 14:15NDEPA 6020Bug/L1Selenium10.07060188EPA 3005A1.417782-49-206/10/17 21:4006/07/17 14:15NDEPA 6020Bug/L1Silver10.07060188EPA 3005A0.327440-22-406/10/17 21:4006/07/17 14:15NDEPA 7470Aug/L1Mercury0.2007060107EPA 7470A0.0417439-97-606/06/17 14:2306/06/17 10:35Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L1Acetone1007060218EPA 5030B8.267-64-106/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L1Acrylonitrile2007060218EPA 5030B2.5107-13-106/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L1Benzene1.07060218EPA 5030B0.271-43-206/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L1Bromochloromethane3.07060218EPA 5030B0.574-97-506/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L1Bromodichloromethane1.07060218EPA 5030B0.475-27-406/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L1Bromoform3.07060218EPA 5030B0.675-25-206/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L1Bromomethane107060218EPA 5030B1.074-83-906/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L1Carbon Disulfide1007060218EPA 5030B0.875-15-006/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L1Carbon Tetrachloride1.07060218EPA 5030B0.456-23-506/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L1Chlorobenzene3.07060218EPA 5030B0.5108-90-706/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L1Chloroethane107060218EPA 5030B0.575-00-306/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L1Chloroform5.07060218EPA 5030B0.667-66-306/07/17 18:5506/07/17 10:00Page 39 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-SW2Surface WaterAAF0102-13AAF010205/31/17 12:55Project:Holly Springs Closed C&D Landfill06/02/17 09:05Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L1Chloromethane1.07060218EPA 5030B0.474-87-306/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L1Dibromochloromethane3.07060218EPA 5030B0.3124-48-106/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L11,2-Dibromo-3-chloropropane137060218EPA 5030B0.696-12-806/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L11,2-Dibromoethane1.07060218EPA 5030B0.3106-93-406/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L1Dibromomethane107060218EPA 5030B0.674-95-306/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L11,2-Dichlorobenzene5.07060218EPA 5030B0.595-50-106/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L11,4-Dichlorobenzene1.07060218EPA 5030B0.6106-46-706/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L1trans-1,4-Dichloro-2-butene1007060218EPA 5030B1.6110-57-606/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L11,1-Dichloroethane5.07060218EPA 5030B0.475-34-306/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L11,2-Dichloroethane1.07060218EPA 5030B0.7107-06-206/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L11,1-Dichloroethene5.07060218EPA 5030B0.775-35-406/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L1cis-1,2-Dichloroethene5.07060218EPA 5030B0.7156-59-206/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L1trans-1,2-Dichloroethene5.07060218EPA 5030B0.5156-60-506/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L11,2-Dichloropropane1.07060218EPA 5030B0.678-87-506/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L1cis-1,3-Dichloropropene1.07060218EPA 5030B0.210061-01-506/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L1trans-1,3-Dichloropropene1.07060218EPA 5030B0.310061-02-606/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L1Ethylbenzene1.07060218EPA 5030B0.4100-41-406/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L1Iodomethane107060218EPA 5030B3.174-88-406/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L1Methyl Butyl Ketone (2-Hexanone)507060218EPA 5030B0.9591-78-606/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L1Methylene Chloride1.07060218EPA 5030B0.575-09-206/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L1Methyl Ethyl Ketone (2-Butanone)1007060218EPA 5030B3.278-93-306/07/17 18:5506/07/17 10:00Page 40 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-SW2Surface WaterAAF0102-13AAF010205/31/17 12:55Project:Holly Springs Closed C&D Landfill06/02/17 09:05Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L14-Methyl-2-pentanone (MIBK)1007060218EPA 5030B0.9108-10-106/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L1Styrene1.07060218EPA 5030B0.5100-42-506/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L11,1,1,2-Tetrachloroethane5.07060218EPA 5030B0.3630-20-606/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L11,1,2,2-Tetrachloroethane3.07060218EPA 5030B0.579-34-506/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L1Tetrachloroethene1.07060218EPA 5030B0.8127-18-406/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L1Toluene1.07060218EPA 5030B0.3108-88-306/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L11,1,1-Trichloroethane1.07060218EPA 5030B0.471-55-606/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L11,1,2-Trichloroethane1.07060218EPA 5030B0.679-00-506/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L1Trichloroethene1.07060218EPA 5030B0.379-01-606/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L1Trichlorofluoromethane1.07060218EPA 5030B0.575-69-406/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L11,2,3-Trichloropropane1.07060218EPA 5030B0.596-18-406/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L1Vinyl Acetate507060218EPA 5030B0.4108-05-406/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L1Vinyl Chloride1.07060218EPA 5030B0.675-01-406/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L1Xylenes, total5.07060218EPA 5030B0.91330-20-706/07/17 18:5506/07/17 10:00NDEPA 8260Bug/L1Tetrahydrofuran107060218EPA 5030B1.3109-99-906/07/17 18:5506/07/17 10:00EPA 8260B91 %Surr: Dibromofluoromethane7060218EPA 5030B1868-53-706/07/17 18:5506/07/17 10:0080-120EPA 8260B97 %Surr: 1,2-Dichloroethane-d47060218EPA 5030B17060-07-006/07/17 18:5506/07/17 10:0078-120EPA 8260B99 %Surr: Toluene-d87060218EPA 5030B2037-26-506/07/17 18:5506/07/17 10:0080-120EPA 8260B98 %Surr: 4-Bromofluorobenzene7060218EPA 5030B460-00-406/07/17 18:5506/07/17 10:0080-120Page 41 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-Field BlankWaterAAF0102-14AAF010205/31/17 15:21Project:Holly Springs Closed C&D Landfill06/02/17 09:05Metals, TotalNDEPA 6020Bug/L1Arsenic10.07060188EPA 3005A0.427440-38-206/10/17 21:4506/07/17 14:15NDEPA 6020Bug/L1Barium1007060188EPA 3005A0.277440-39-306/10/17 21:4506/07/17 14:15NDEPA 6020Bug/L1Cadmium1.007060188EPA 3005A0.067440-43-906/10/17 21:4506/07/17 14:15NDEPA 6020Bug/L1Chromium10.07060188EPA 3005A0.347440-47-306/10/17 21:4506/07/17 14:15NDEPA 6020Bug/L1Lead10.07060188EPA 3005A0.077439-92-106/10/17 21:4506/07/17 14:15NDEPA 6020Bug/L1Selenium10.07060188EPA 3005A1.417782-49-206/10/17 21:4506/07/17 14:15NDEPA 6020Bug/L1Silver10.07060188EPA 3005A0.327440-22-406/10/17 21:4506/07/17 14:15NDEPA 7470Aug/L1Mercury0.2007060107EPA 7470A0.0417439-97-606/06/17 14:2506/06/17 10:35Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L1Acetone1007060218EPA 5030B8.267-64-106/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L1Acrylonitrile2007060218EPA 5030B2.5107-13-106/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L1Benzene1.07060218EPA 5030B0.271-43-206/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L1Bromochloromethane3.07060218EPA 5030B0.574-97-506/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L1Bromodichloromethane1.07060218EPA 5030B0.475-27-406/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L1Bromoform3.07060218EPA 5030B0.675-25-206/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L1Bromomethane107060218EPA 5030B1.074-83-906/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L1Carbon Disulfide1007060218EPA 5030B0.875-15-006/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L1Carbon Tetrachloride1.07060218EPA 5030B0.456-23-506/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L1Chlorobenzene3.07060218EPA 5030B0.5108-90-706/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L1Chloroethane107060218EPA 5030B0.575-00-306/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L1Chloroform5.07060218EPA 5030B0.667-66-306/07/17 19:2106/07/17 10:00Page 42 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-Field BlankWaterAAF0102-14AAF010205/31/17 15:21Project:Holly Springs Closed C&D Landfill06/02/17 09:05Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L1Chloromethane1.07060218EPA 5030B0.474-87-306/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L1Dibromochloromethane3.07060218EPA 5030B0.3124-48-106/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L11,2-Dibromo-3-chloropropane137060218EPA 5030B0.696-12-806/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L11,2-Dibromoethane1.07060218EPA 5030B0.3106-93-406/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L1Dibromomethane107060218EPA 5030B0.674-95-306/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L11,2-Dichlorobenzene5.07060218EPA 5030B0.595-50-106/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L11,4-Dichlorobenzene1.07060218EPA 5030B0.6106-46-706/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L1trans-1,4-Dichloro-2-butene1007060218EPA 5030B1.6110-57-606/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L11,1-Dichloroethane5.07060218EPA 5030B0.475-34-306/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L11,2-Dichloroethane1.07060218EPA 5030B0.7107-06-206/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L11,1-Dichloroethene5.07060218EPA 5030B0.775-35-406/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L1cis-1,2-Dichloroethene5.07060218EPA 5030B0.7156-59-206/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L1trans-1,2-Dichloroethene5.07060218EPA 5030B0.5156-60-506/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L11,2-Dichloropropane1.07060218EPA 5030B0.678-87-506/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L1cis-1,3-Dichloropropene1.07060218EPA 5030B0.210061-01-506/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L1trans-1,3-Dichloropropene1.07060218EPA 5030B0.310061-02-606/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L1Ethylbenzene1.07060218EPA 5030B0.4100-41-406/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L1Iodomethane107060218EPA 5030B3.174-88-406/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L1Methyl Butyl Ketone (2-Hexanone)507060218EPA 5030B0.9591-78-606/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L1Methylene Chloride1.07060218EPA 5030B0.575-09-206/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L1Methyl Ethyl Ketone (2-Butanone)1007060218EPA 5030B3.278-93-306/07/17 19:2106/07/17 10:00Page 43 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-Field BlankWaterAAF0102-14AAF010205/31/17 15:21Project:Holly Springs Closed C&D Landfill06/02/17 09:05Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L14-Methyl-2-pentanone (MIBK)1007060218EPA 5030B0.9108-10-106/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L1Styrene1.07060218EPA 5030B0.5100-42-506/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L11,1,1,2-Tetrachloroethane5.07060218EPA 5030B0.3630-20-606/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L11,1,2,2-Tetrachloroethane3.07060218EPA 5030B0.579-34-506/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L1Tetrachloroethene1.07060218EPA 5030B0.8127-18-406/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L1Toluene1.07060218EPA 5030B0.3108-88-306/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L11,1,1-Trichloroethane1.07060218EPA 5030B0.471-55-606/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L11,1,2-Trichloroethane1.07060218EPA 5030B0.679-00-506/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L1Trichloroethene1.07060218EPA 5030B0.379-01-606/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L1Trichlorofluoromethane1.07060218EPA 5030B0.575-69-406/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L11,2,3-Trichloropropane1.07060218EPA 5030B0.596-18-406/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L1Vinyl Acetate507060218EPA 5030B0.4108-05-406/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L1Vinyl Chloride1.07060218EPA 5030B0.675-01-406/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L1Xylenes, total5.07060218EPA 5030B0.91330-20-706/07/17 19:2106/07/17 10:00NDEPA 8260Bug/L1Tetrahydrofuran107060218EPA 5030B1.3109-99-906/07/17 19:2106/07/17 10:00EPA 8260B90 %Surr: Dibromofluoromethane7060218EPA 5030B1868-53-706/07/17 19:2106/07/17 10:0080-120EPA 8260B100 %Surr: 1,2-Dichloroethane-d47060218EPA 5030B17060-07-006/07/17 19:2106/07/17 10:0078-120EPA 8260B99 %Surr: Toluene-d87060218EPA 5030B2037-26-506/07/17 19:2106/07/17 10:0080-120EPA 8260B100 %Surr: 4-Bromofluorobenzene7060218EPA 5030B460-00-406/07/17 19:2106/07/17 10:0080-120Page 44 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-Trip BlankWaterAAF0102-15AAF010205/31/17 08:00Project:Holly Springs Closed C&D Landfill06/02/17 09:05Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L1Acetone1007060218EPA 5030B8.267-64-106/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1Acrylonitrile2007060218EPA 5030B2.5107-13-106/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1Benzene1.07060218EPA 5030B0.271-43-206/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1Bromochloromethane3.07060218EPA 5030B0.574-97-506/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1Bromodichloromethane1.07060218EPA 5030B0.475-27-406/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1Bromoform3.07060218EPA 5030B0.675-25-206/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1Bromomethane107060218EPA 5030B1.074-83-906/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1Carbon Disulfide1007060218EPA 5030B0.875-15-006/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1Carbon Tetrachloride1.07060218EPA 5030B0.456-23-506/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1Chlorobenzene3.07060218EPA 5030B0.5108-90-706/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1Chloroethane107060218EPA 5030B0.575-00-306/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1Chloroform5.07060218EPA 5030B0.667-66-306/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1Chloromethane1.07060218EPA 5030B0.474-87-306/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1Dibromochloromethane3.07060218EPA 5030B0.3124-48-106/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L11,2-Dibromo-3-chloropropane137060218EPA 5030B0.696-12-806/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L11,2-Dibromoethane1.07060218EPA 5030B0.3106-93-406/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1Dibromomethane107060218EPA 5030B0.674-95-306/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L11,2-Dichlorobenzene5.07060218EPA 5030B0.595-50-106/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L11,4-Dichlorobenzene1.07060218EPA 5030B0.6106-46-706/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1trans-1,4-Dichloro-2-butene1007060218EPA 5030B1.6110-57-606/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L11,1-Dichloroethane5.07060218EPA 5030B0.475-34-306/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L11,2-Dichloroethane1.07060218EPA 5030B0.7107-06-206/07/17 19:4706/07/17 10:00Page 45 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-Trip BlankWaterAAF0102-15AAF010205/31/17 08:00Project:Holly Springs Closed C&D Landfill06/02/17 09:05Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L11,1-Dichloroethene5.07060218EPA 5030B0.775-35-406/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1cis-1,2-Dichloroethene5.07060218EPA 5030B0.7156-59-206/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1trans-1,2-Dichloroethene5.07060218EPA 5030B0.5156-60-506/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L11,2-Dichloropropane1.07060218EPA 5030B0.678-87-506/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1cis-1,3-Dichloropropene1.07060218EPA 5030B0.210061-01-506/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1trans-1,3-Dichloropropene1.07060218EPA 5030B0.310061-02-606/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1Ethylbenzene1.07060218EPA 5030B0.4100-41-406/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1Iodomethane107060218EPA 5030B3.174-88-406/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1Methyl Butyl Ketone (2-Hexanone)507060218EPA 5030B0.9591-78-606/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1Methylene Chloride1.07060218EPA 5030B0.575-09-206/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1Methyl Ethyl Ketone (2-Butanone)1007060218EPA 5030B3.278-93-306/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L14-Methyl-2-pentanone (MIBK)1007060218EPA 5030B0.9108-10-106/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1Styrene1.07060218EPA 5030B0.5100-42-506/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L11,1,1,2-Tetrachloroethane5.07060218EPA 5030B0.3630-20-606/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L11,1,2,2-Tetrachloroethane3.07060218EPA 5030B0.579-34-506/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1Tetrachloroethene1.07060218EPA 5030B0.8127-18-406/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1Toluene1.07060218EPA 5030B0.3108-88-306/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L11,1,1-Trichloroethane1.07060218EPA 5030B0.471-55-606/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L11,1,2-Trichloroethane1.07060218EPA 5030B0.679-00-506/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1Trichloroethene1.07060218EPA 5030B0.379-01-606/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1Trichlorofluoromethane1.07060218EPA 5030B0.575-69-406/07/17 19:4706/07/17 10:00Page 46 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultAnalyteSWSL/ RLPrepMethodQual DFUnitsBatchAnalyticalMethodMDLCAS #Prep Date/TimeAnalysis Date/TimeClient ID:Date/Time Sampled:Matrix:Report No.:Lab No:Date/Time Received:9214-Trip BlankWaterAAF0102-15AAF010205/31/17 08:00Project:Holly Springs Closed C&D Landfill06/02/17 09:05Volatile Organic Compounds by EPA 8260NDEPA 8260Bug/L11,2,3-Trichloropropane1.07060218EPA 5030B0.596-18-406/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1Vinyl Acetate507060218EPA 5030B0.4108-05-406/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1Vinyl Chloride1.07060218EPA 5030B0.675-01-406/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1Xylenes, total5.07060218EPA 5030B0.91330-20-706/07/17 19:4706/07/17 10:00NDEPA 8260Bug/L1Tetrahydrofuran107060218EPA 5030B1.3109-99-906/07/17 19:4706/07/17 10:00EPA 8260B91 %Surr: Dibromofluoromethane7060218EPA 5030B1868-53-706/07/17 19:4706/07/17 10:0080-120EPA 8260B103 %Surr: 1,2-Dichloroethane-d47060218EPA 5030B17060-07-006/07/17 19:4706/07/17 10:0078-120EPA 8260B98 %Surr: Toluene-d87060218EPA 5030B2037-26-506/07/17 19:4706/07/17 10:0080-120EPA 8260B99 %Surr: 4-Bromofluorobenzene7060218EPA 5030B460-00-406/07/17 19:4706/07/17 10:0080-120Page 47 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultLimitReportingUnitsLevelSpikeResultSource%REC%RECLimitsRPDRPDLimitQual AnalyteMetals, Total - Quality ControlBatch 7060107 - EPA 7470ABlank (7060107-BLK1)Prepared & Analyzed: 06/06/17 Mercuryug/LND0.200LCS (7060107-BS1)Prepared & Analyzed: 06/06/17 Mercuryug/L2.280.2002.500080-12091Matrix Spike (7060107-MS1)Prepared & Analyzed: 06/06/17 Source: AAF0102-07Mercuryug/L2.170.2002.50000.14675-12581Matrix Spike Dup (7060107-MSD1)Prepared & Analyzed: 06/06/17 Source: AAF0102-07Mercuryug/L2.220.2002.50000.1462075-125832Post Spike (7060107-PS1)Prepared & Analyzed: 06/06/17 Source: AAF0102-07Mercuryug/L1.641.66670.09880-12093Batch 7060188 - EPA 3005ABlank (7060188-BLK1)Prepared: 06/07/17 Analyzed: 06/10/17 Arsenicug/LND10.0Bariumug/LND100Cadmiumug/LND1.00Chromiumug/LND10.0Leadug/LND10.0Seleniumug/LND10.0Silverug/LND10.0LCS (7060188-BS1)Prepared: 06/07/17 Analyzed: 06/10/17 Arsenicug/L10210.0100.0080-120102Bariumug/L99.3100100.00J80-12099Cadmiumug/L1011.00100.0080-120101Page 48 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultLimitReportingUnitsLevelSpikeResultSource%REC%RECLimitsRPDRPDLimitQual AnalyteMetals, Total - Quality ControlBatch 7060188 - EPA 3005ALCS (7060188-BS1)Prepared: 06/07/17 Analyzed: 06/10/17 Chromiumug/L10010.0100.0080-120100Leadug/L10210.0100.0080-120102Seleniumug/L10210.0100.0080-120102Silverug/L10110.0100.0080-120101Matrix Spike (7060188-MS1)Prepared: 06/07/17 Analyzed: 06/10/17 Source: AAF0102-07Arsenicug/L10510.0100.002.9875-125102Bariumug/L263100100.0016675-12597Cadmiumug/L1021.00100.00ND75-125102Chromiumug/L10010.0100.00ND75-125100Leadug/L99.310.0100.00ND75-12599Seleniumug/L10510.0100.00ND75-125105Silverug/L98.810.0100.00ND75-12599Matrix Spike Dup (7060188-MSD1)Prepared: 06/07/17 Analyzed: 06/10/17 Source: AAF0102-07Arsenicug/L10310.0100.002.982075-1251002Bariumug/L267100100.001662075-1251022Cadmiumug/L1041.00100.00ND2075-1251043Chromiumug/L10110.0100.00ND2075-1251010.3Leadug/L98.810.0100.00ND2075-125990.6Seleniumug/L10310.0100.00ND2075-1251031Silverug/L10110.0100.00ND2075-1251012Post Spike (7060188-PS1)Prepared: 06/07/17 Analyzed: 06/10/17 Source: AAF0102-07Arsenicug/L101100.002.9880-12098Bariumug/L259100.0016680-12094Cadmiumug/L102100.000.0280-120102Chromiumug/L96.3100.000.3280-12096Page 49 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultLimitReportingUnitsLevelSpikeResultSource%REC%RECLimitsRPDRPDLimitQual AnalyteMetals, Total - Quality ControlBatch 7060188 - EPA 3005APost Spike (7060188-PS1)Prepared: 06/07/17 Analyzed: 06/10/17 Source: AAF0102-07Leadug/L97.3100.00-0.00780-12097Seleniumug/L100100.00-0.2580-120100Silverug/L98.8100.000.0280-12099Page 50 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultLimitReportingUnitsLevelSpikeResultSource%REC%RECLimitsRPDRPDLimitQual AnalyteVolatile Organic Compounds by EPA 8260 - Quality ControlBatch 7060218 - EPA 5030BBlank (7060218-BLK1)Prepared & Analyzed: 06/07/17 Acetoneug/LND100Acrylonitrileug/LND200Benzeneug/LND1.0Bromochloromethaneug/LND3.0Bromodichloromethaneug/LND1.0Bromoformug/LND3.0Bromomethaneug/LND10Carbon Disulfideug/LND100Carbon Tetrachlorideug/LND1.0Chlorobenzeneug/LND3.0Chloroethaneug/LND10Chloroformug/LND5.0Chloromethaneug/LND1.0Dibromochloromethaneug/LND3.01,2-Dibromo-3-chloropropaneug/LND131,2-Dibromoethaneug/LND1.0Dibromomethaneug/LND101,2-Dichlorobenzeneug/LND5.01,4-Dichlorobenzeneug/LND1.0trans-1,4-Dichloro-2-buteneug/LND1001,1-Dichloroethaneug/LND5.01,2-Dichloroethaneug/LND1.01,1-Dichloroetheneug/LND5.0cis-1,2-Dichloroetheneug/LND5.0trans-1,2-Dichloroetheneug/LND5.01,2-Dichloropropaneug/LND1.0cis-1,3-Dichloropropeneug/LND1.0Page 51 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultLimitReportingUnitsLevelSpikeResultSource%REC%RECLimitsRPDRPDLimitQual AnalyteVolatile Organic Compounds by EPA 8260 - Quality ControlBatch 7060218 - EPA 5030BBlank (7060218-BLK1)Prepared & Analyzed: 06/07/17 trans-1,3-Dichloropropeneug/LND1.0Ethylbenzeneug/LND1.0Iodomethaneug/LND10Methyl Butyl Ketone (2-Hexanone)ug/LND50Methylene Chlorideug/LND1.0Methyl Ethyl Ketone (2-Butanone)ug/LND1004-Methyl-2-pentanone (MIBK)ug/LND100Styreneug/LND1.01,1,1,2-Tetrachloroethaneug/LND5.01,1,2,2-Tetrachloroethaneug/LND3.0Tetrachloroetheneug/LND1.0Tolueneug/LND1.01,1,1-Trichloroethaneug/LND1.01,1,2-Trichloroethaneug/LND1.0Trichloroetheneug/LND1.0Trichlorofluoromethaneug/LND1.01,2,3-Trichloropropaneug/LND1.0Vinyl Acetateug/LND50Vinyl Chlorideug/LND1.0Xylenes, totalug/LND5.0Tetrahydrofuranug/LND10ug/L50.00080-120Surr: Dibromofluoromethane9447ug/L50.00078-120Surr: 1,2-Dichloroethane-d49748ug/L50.00080-120Surr: Toluene-d810050ug/L50.00080-120Surr: 4-Bromofluorobenzene9748LCS (7060218-BS1)Prepared & Analyzed: 06/07/17 Page 52 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultLimitReportingUnitsLevelSpikeResultSource%REC%RECLimitsRPDRPDLimitQual AnalyteVolatile Organic Compounds by EPA 8260 - Quality ControlBatch 7060218 - EPA 5030BLCS (7060218-BS1)Prepared & Analyzed: 06/07/17 Benzeneug/L5550.00067-134109Chlorobenzeneug/L5150.00069-1221031,1-Dichloroetheneug/L4950.00058-14299Tolueneug/L5250.00068-127104Trichloroetheneug/L4850.00072-13297ug/L50.00080-120Surr: Dibromofluoromethane9246ug/L50.00078-120Surr: 1,2-Dichloroethane-d49447ug/L50.00080-120Surr: Toluene-d89950ug/L50.00080-120Surr: 4-Bromofluorobenzene9949Matrix Spike (7060218-MS1)Prepared & Analyzed: 06/07/17 Source: AAF0102-07Benzeneug/L6050.0000.067-134119Chlorobenzeneug/L5550.0000.069-1221111,1-Dichloroetheneug/L6050.0000.058-142120Tolueneug/L5750.0000.068-127113Trichloroetheneug/L5350.0000.072-132107ug/L50.00080-120Surr: Dibromofluoromethane9045ug/L50.00078-120Surr: 1,2-Dichloroethane-d49648ug/L50.00080-120Surr: Toluene-d89949ug/L50.00080-120Surr: 4-Bromofluorobenzene9849Matrix Spike Dup (7060218-MSD1)Prepared & Analyzed: 06/07/17 Source: AAF0102-07Benzeneug/L5850.0000.0967-1341163Chlorobenzeneug/L5350.0000.01369-12210641,1-Dichloroetheneug/L5350.0000.09QR-0258-14210612Tolueneug/L5550.0000.0968-1271112Page 53 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017ResultLimitReportingUnitsLevelSpikeResultSource%REC%RECLimitsRPDRPDLimitQual AnalyteVolatile Organic Compounds by EPA 8260 - Quality ControlBatch 7060218 - EPA 5030BMatrix Spike Dup (7060218-MSD1)Prepared & Analyzed: 06/07/17 Source: AAF0102-07Trichloroetheneug/L5250.0000.01172-1321043ug/L50.00080-120Surr: Dibromofluoromethane9045ug/L50.00078-120Surr: 1,2-Dichloroethane-d49849ug/L50.00080-120Surr: Toluene-d89949ug/L50.00080-120Surr: 4-Bromofluorobenzene10050Page 54 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017Laboratory CertificationsCodeDescriptionNumberExpires812Georgia DW Inorganics Eff: 07/01/201606/30/2017GADW812Georgia DW Microbiology Eff: 07/01/201512/09/2019GADWM381North Carolina12/31/2017NCE87315FL DOH (Non-Pot. Water, Solids) Eff:: 07/01/201606/30/2017NELACE87315FL DOH NELAC (Drinking Water) Eff: 07/01/201606/30/2017NELDW98011001South Carolina06/30/2017SCT104704397-08-TXTexas03/31/2018TX460204Virginia12/14/2017VAPage 55 of 58
Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Peachtree Corners, GA 30092(770) 734-4200 FAX [phone]PACE ANALYTICAL SERVICES, LLC.Republic Services of North Carolina, LLC1220 Commerce Street, SWConover NC, 28613Attention: Mr. Matt EinsmannJune 15, 2017LegendDefination of Laboratory Terms - Not Detected at levels greater than or equal to SWSL/RLNDSWSL/RLMDL - NC DENR Solid Waste Section LImit/Reporting Limit (Adjusted for DF/Prep Factor) - Method Detection LimitQualifiers - Dilution FactorDFQR-02The RPD result exceeded the QC control limits; however, both percent recoveries were acceptable. Sample results for the QC batch were accepted based on percent recoveries.JEstimated value less than Reporting Limit (RL) but greater than Method Detection Limit(MDL) (CLP J-Flag).Note: Unless otherwise noted, all results are reported on an as received basis.Page 56 of 58
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LOG-IN CHECKLIST
Republic Services of North Carolina, LLC
Holly Springs Closed C&D LandfillProject:
Client:
Printed: 6/5/2017 11:44:08AM
Environmental Monitoring & Laboratory Analysis
[phone] FAX [phone]
110 Technology Parkway, Peachtree Corners, GA 30092
PACE ANALYTICAL SERVICES, LLC.
Date Received:06/02/17 09:05 Logged In By:Charles Hawks
Work Order:AAF0102
OBSERVATIONS
Attn: Mr. Matt Einsmann
#Samples: 15 #Containers: 64
3.0 3.0
YES
Minimum Temp(C):Maximum Temp(C):
CHECKLIST ITEMS
COC included with Samples
Sample Container(s) Intact
Chain of Custody Complete
Sample Container(s) Match COC
Custody seal Intact
Temperature in Compliance
Sufficient Sample Volume for Analysis
Zero Headspace Maintained for VOA Analyses
Samples labeled preserved (If Applicable)
Samples received within Allowable Hold Times
Samples Received on Ice
Preservation Confirmed
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
YES
Custody Seal(s) Used:Yes
Comments:
Page 1 of 1Page 58 of 58

Appendix C

Historical Groundwater Constituents

APPENDIX C
Historical Groundwater Constituents/Analytes
Analyte
Collection Date DL SWSL MW-1R MW-10 MW-2 MW-3 MW-4 MW-5R MW-6 MW-7 MW-9 MW-11 MW-12 MW-13 Blanks
Inorganic Compounds
Total Arsenic 07/22/09 2.8 10.0 3.84 J 7.37 J 6.86 J 5.85 J 6.60 J 6.26 J 7.04 J 4.87 J 4.26 J 7.19 J 21.4 9.63 J ND
NC2L = 10 µg/l 01/26/10 3.9 10.0 9.21 J 6.79 J 5.08 J 4.20 J 4.78 J ND ND 5.83 J ND ND 13.5 8.24 J ND
07/07/10 2.8 10.0 5.02 J 6.27 J ND 4.34 J 6.90 J ND 3.15 J ND ND ND 13.0 10.20 ND
01/05/11 2.8 10.0 ND 4.15 J 3.99 J ND ND ND ND ND ND ND 11.6 3.84 J ND
07/07/11 2.8 10.0 ND 5.06 J ND ND 5.31 J ND 3.15 J ND ND ND 14.0 8.09 J ND
01/12/12 2.8 10.0 1.82 J 2.81 J 2.81 J 4.32 J 2.89 J ND ND 1.52 J 14.2 ND 10.8 2.11 J ND
07/12/12 2.8 10.0 ND 1.40 J 3.57 J 1.33 J 1.85 J ND ND ND ND ND 14.6 6.86 J ND
02/06/13 2.8 10.0 ND 2.58 J 3.56 J 3.70 J 3.66 J ND ND 1.45 J ND 1.29 J 8.0 J 3.80 J ND
07/09/13 2.8 10.0 1.62 J 4.44 J 3.70 J 2.68 J 4.10 J ND 1.74 J ND ND ND 25.0 8.44 J ND
01/31/14 2.8 10.0 ND 5.77 J 2.72 J 2.31 J 3.47 J ND ND 0.89 J 5.72 J ND 21.3 1.47 J ND
07/23/14 1.13 10.0 1.14 J 4.39 J 2.40 J 3.42 J 1.67 J 1.19 J ND ND ND ND 22.1 20.2 ND
01/27/15 1.13 10.0 1.61 J 5.13 J 3.09 J 3.30 J 2.76 J ND 1.21 J 1.83 J 2.59 J ND 21.6 10.8 ND
07/29/15 0.75 10.0 ND 5.49 J 4.36 J 3.53 J 3.02 J ND 2.10 B 3.48 B 11.6 1.71 B 19.8 6.17 J 0.93 J
06/23/16 0.75 10.0 2.22 J 6.71 J 5.19 J 3.39 J 3.15 J 2.75 J 3.16 J 3.07 J 25.6 2.04 J 23.5 8.18 J ND
11/02/16 1.64 10.0 1.79 J 6.41 J 4.57 J 3.31 J 2.89 J 4.42 J 2.58 J 2.96 J 34.0 1.75 J 22.4 6.04 J ND
Dissolved Metals Analysis>11/02/16 1.64 10.0 --- --- --- --- --- --- --- ---ND --------- ---
05/31/17 0.42 10.0 2.21 J 6.79 J 4.36 J 3.25 J 2.95 J 2.90 J 2.10 J 2.98 J 1.13 J 1.63 J 26.8 7.09 J ND
Total Barium 07/22/09 4.2 100.0 258 48.1 J 72.6 J 30.6 J 54.4 J 162 266 122 112 84.3 J 209 386 ND
NC2L = 700 µg/l 01/26/10 0.25 100.00 327 49.9 J 77.8 J 36.2 J 45.3 J 144 275 105 138 45.2 J 220 540 0.66 J
07/07/10 1.0 100.0 219 24.8 J 61.0 J 27.5 J 43.4 J 131 209 126 113 44.3 J 149 385 ND
01/05/11 1.0 100.0 229 32.5 J 81.5 J 27.2 J 45.8 J 134 222 80.0 J 125 45.3 J 200 312 ND
07/07/11 1.0 100.0 266 27.5 J 80.4 J 31.7 J 53.6 J 130 272 141 196 56.8 J 217 354 ND
01/12/12 --- 100 260 42.6 J 82.0 J 46.2 J 48.4 J 130 261 97.6 J 387 40.8 J 243 300 0.09 J
07/12/12 --- 100 238 34.9 J 71.3 J 27.7 J 48.9 J 110 246 142 76.0 J 48.7 J 220 316 1.47 J
02/06/13 --- 100 250 43.6 J 67.6 J 26.8 J 48.2 J 113 248 70.6 J 106 59.3 J 118 263 1.05 J
07/09/13 --- 100 252 23.4 J 69.4 J 26.2 J 54.1 J 123 307 130 80.6 J 47.7 J 228 237 0.46 J
01/31/14 --- 100 258 22.0 J 74.4 J 29.5 J 54.2 J 109 245 116 129 35.3 J 163 259 ND
07/23/14 0.10 100 251 20.9 J 77.8 J 121 62.2 J 147 282 150 61.0 J 48.2 J 173 324 0.33 J
01/27/15 0.10 100 318 24.0 J 71.4 J 50.1 J 61.5 J 110 262 112 83.4 J 56.7 J 186 629 0.17 J
07/29/15 0.30 100 299 23.6 J 72.4 J 23.8 J 68.9 J 134 278 93.4 J 708 51.8 J 167 295 0.84 J
06/23/16 0.30 100 378 23.4 J 77.3 J 23.3 J 74.8 J 131 317 164 972 59.0 J 205 266 3.40 J
11/02/16 0.44 100 366 22.4 J 76.1 J 21.3 J 80.2 J 146 242 195 1240 62.3 J 178 262 0.49 J
Dissolved Metals Analysis>11/02/16 0.44 100 --- --- --- --- --- --- --- ---108 --------- ---
05/31/17 0.27 100 408 20.7 J 74.0 J 21.4 J 85.4 J 160 298 166 77.6 J 53.2 J 196 238 ND
Total Cadmium 07/22/09 0.1 1 0.31 J 0.14 J ND 0.16 J 0.194 J 0.37 J ND 0.232 J 0.49 J 0.17 J 0.39 J 0.17 J ND
NC2L = 2 µg/l 01/26/10 0.1 1 0.36 B 0.19 B ND 0.24 B 0.211 B 0.20 B 0.23 B 0.335 B 0.25 B 0.39 B ND 0.13 B 0.14 J
07/07/10 0.4 1 ND ND ND ND ND ND ND ND ND ND ND ND ND
01/05/11 0.4 1 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/07/11 0.4 1 ND ND ND ND ND ND ND ND ND ND ND ND ND
01/12/12 0.4 1 0.07 J ND ND ND ND ND ND ND 0.12 J ND ND ND ND
07/12/12 --- 1.00 0.11 J ND ND ND ND 0.06 J ND ND ND ND ND 0.10 J ND
02/06/13 --- 1.00 0.16 J ND ND ND ND ND ND ND 0.06 J 0.06 J 0.20 J 0.06 J ND
07/09/13 --- 1.00 ND ND ND ND ND ND ND ND 0.20 J ND 0.15 J ND ND
01/31/14 --- 1.00 ND ND ND ND ND ND ND ND 0.06 J ND 0.27 J ND ND
07/23/14 --- 1.00 ND ND ND 0.06 J ND ND ND ND 0.14 J 0.05 J 0.12 J ND ND
01/27/15 0.05 1.00 ND ND ND ND ND ND ND ND 0.08 J 0.07 J 0.09 J ND ND
07/29/15 0.10 1.00 ND ND ND ND ND ND ND ND 0.20 J ND ND ND ND
06/23/16 0.10 1.00 ND ND ND ND ND ND ND ND 0.16 J ND ND ND ND
11/02/16 0.07 1.00 ND ND ND ND ND ND ND ND ND R1 ND 0.13 J ND ND
05/31/17 0.06 1.00 ND ND ND ND ND 0.10 J ND ND 0.25 J ND ND 0.11 J ND
Total Chromium 07/22/09 0.7 10 ND 2.74 J 4.45 J 3.53 J ND 1.03 J 1.47 J 1.25 J 3.60 J 5.39 J 1.89 J ND ND
NC2L = 10 µg/l 01/26/10 1.7 10 2.91 J 2.03 J 6.80 J 4.05 J ND ND ND 2.38 J 5.17 J 4.39 J ND 1.72 J ND
07/07/10 1.0 10 1.50 J 1.59 J 3.16 J 2.46 J 1.93 J 1.70 J 1.10 J 1.06 J 3.85 J 2.94 J ND 2.68 J ND
01/05/11 1.0 10 ND 2.10 J 7.40 J 6.03 J ND 2.59 J 1.95 J 1.11 J 7.43 J 7.10 J ND ND ND
07/07/11 1.0 10 ND 2.41 J 4.75 J 2.01 J 1.06 J 1.80 J 1.28 J ND 22.50 3.54 J 1.82 J 1.62 J ND
01/12/12 1.0 10 ND 1.65 B 11.0 22.8 ND ND 0.84 B 1.38 B 17.90 3.19 B 1.07 B 1.47 B 0.82 J
07/12/12 --- 10.0 ND ND 1.23 J 3.01 J ND ND ND ND 3.00 J 1.02 J ND ND ND
02/06/13 --- 10.0 ND 0.86 B ND 3.40 B ND 1.18 B 15.70 ND 5.10 B ND 4.50 B 1.80 B 1.42 J
07/09/13 --- 10.0 2.56 B ND 0.60 B ND ND 2.16 B 7.47 B 1.39 B 4.15 B 3.11 B 3.24 B 2.39 B 3.51 J
01/31/14 --- 10.0 3.56 B 1.31 B 2.47 B 1.63 B ND 3.93 B 7.32 B 2.99 B 8.64 B 5.11 B 2.31 B 3.96 B 2.79 J
07/23/14 --- 10.0 1.99 J 1.43 J 2.86 J 7.72 J ND 1.75 J 2.81 J 1.58 J 3.57 J 2.65 J ND ND ND
01/27/15 0.73 10.0 1.53 J 3.08 J 1.74 J 1.52 J ND ND 1.05 J ND 2.69 J 4.37 J ND 3.37 J ND
07/29/15 0.43 10.0 2.44 J ND ND ND ND 0.76 J ND ND 17.0 1.56 J ND ND ND
06/23/16 0.43 10.0 0.61 J 0.93 J 1.22 J ND ND 0.74 J 0.82 J ND 28.8 1.27 J 1.07 J ND ND
11/02/16 0.94 10.0 ND 2.45 J 1.11 J ND ND ND ND ND 78.7 ND 4.91 J ND ND
Dissolved Metals Analysis>11/02/16 0.94 10.0 --- --- --- --- --- --- --- ---ND ------------
05/31/17 0.34 10.0 0.59 J 1.04 J 1.39 J 0.34 J ND 1.15 J 0.88 J ND 1.05 J 1.28 J 0.73 J 0.36 J ND

Total Lead 07/22/09 1.6 10 1.72 J ND ND ND ND ND ND ND 2.31 J 3.82 J 2.44 J ND ND
NC2L = 15 µg/l 01/26/10 1.1 10 3.05 J ND ND ND ND ND ND ND 4.9 J ND ND 2.24 J ND
07/07/10 1.9 10 ND ND ND ND ND ND ND ND 2.66 J ND ND ND ND
01/05/11 1.9 10 ND 2.40 J ND ND ND ND ND ND ND ND ND ND ND
07/07/11 1.9 10 ND ND ND ND ND ND ND ND 11.30 ND ND ND ND
01/12/12 1.9 10 ND ND 0.21 J 2.43 ND ND ND ND 19.60 0.59 J ND ND ND
07/12/12 --- 10.0 0.12 J ND ND 0.31 J ND ND ND ND 0.98 J 0.11 J ND 0.23 J ND
02/06/13 --- 10.0 0.26 J ND 0.11 J 0.68 J 0.09 J ND 0.68 J ND 5.48 J 0.22 J 1.63 J 0.13 J ND
07/09/13 --- 10.0 1.36 J ND 0.06 B 0.23 B 0.08 B ND 0.24 B ND 1.42 J ND 1.64 J 0.28 B 0.08 J
01/31/14 --- 10.0 0.08 J ND ND 0.85 J ND ND 0.24 J ND 10.4 0.08 J 0.32 J 0.13 J ND
07/23/14 --- 10.0 0.05 J ND 0.17 J 5.31 J ND ND ND ND 1.68 J 0.09 J 0.22 J 0.53 J ND
01/27/15 0.05 10.0 0.33 J ND ND 1.44 J ND ND ND ND 2.15 J 1.35 J 0.05 J 1.88 J ND
07/29/15 0.08 10.0 ND ND ND 0.11 J 0.32 J ND ND ND 32.8 0.15 J 0.20 J ND ND
06/23/16 0.08 10.0 ND ND ND ND ND 0.11 B ND ND 41.3 ND 0.46 B ND 0.26 J
11/02/16 0.12 10.0 ND ND ND ND ND ND ND ND 74.5 ND 0.50 J ND ND
Dissolved Metals Analysis>11/02/16 0.12 10.0 ------------------------ND ------------
05/31/17 0.07 10.0 ND ND 0.15 J ND ND 0.51 J ND ND 1.12 J ND 0.14 J ND ND
Holly Springs Closed C and D Landfill
Permit No. 92-14 Page 1 of 4 Joyce Engineering
APPENDIX C
Historical Groundwater Constituents/Analytes
Analyte
Collection Date DL SWSL MW-1R MW-10 MW-2 MW-3 MW-4 MW-5R MW-6 MW-7 MW-9 MW-11 MW-12 MW-13 Blanks
Total Mercury 07/22/09 0.1 0.2 ND ND ND ND ND ND ND 0.206 ND ND ND ND ND
NC2L = 1 µg/l 01/26/10 0.1 0.2 ND ND ND ND ND ND ND 0.115 J ND ND 0.070 J ND ND
07/07/10 0.2 0.2 ND ND ND ND ND ND ND ND ND ND ND ND ND
01/05/11 0.2 0.2 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/07/11 0.2 0.2 ND ND ND ND ND ND ND 0.194 J ND ND ND ND ND
01/12/12 0.2 0.2 ND ND ND ND ND ND ND 0.201 ND ND ND ND ND
07/12/12 --- 0.2 ND ND ND ND ND ND ND 0.197 J ND ND ND ND ND
02/06/13 --- 0.2 ND ND ND ND ND ND ND 0.066 J ND ND ND ND ND
07/09/13 --- 0.2 {0.088} B ND ND ND ND 0.067 J 0.074 J 0.259 ND ND 0.069 J 0.08 J ND {0.084} J
01/31/14 --- 0.2 ND ND 0.073 B ND ND ND 0.068 B 0.286 B ND ND 0.072 B ND 0.114 J
07/23/14 --- 0.2 0.069 J ND ND ND ND 0.126 J 0.065 J 0.193 J ND ND ND ND ND
01/27/15 0.064 0.2 ND ND 0.163 J ND ND ND ND 0.275 ND ND ND ND ND
07/29/15 0.070 0.2 ND ND ND ND ND ND ND 0.218 0.122 J ND ND ND ND
06/23/16 0.132 0.2 0.144 J ND ND ND ND ND ND 0.171 J ND ND ND ND ND
11/02/16 0.041 0.2 ND ND ND ND ND ND ND ND ND ND ND ND ND
05/31/17 0.041 0.2 ND ND ND ND 0.043 J ND ND 0.146 J ND ND ND ND ND
Total Selenium 07/22/09 3.4 10 ND ND ND ND ND ND ND ND ND ND ND ND ND
NC2L = 20 µg/l 01/26/10 0.8 10 ND ND ND ND ND 1.50 J 0.97 J 1.01 J 4.32 J 3.22 J 2.02 J 1.10 J ND
07/07/10 2.7 10 ND ND ND ND ND ND ND ND ND ND ND ND ND
01/05/11 2.7 10 ND ND ND ND ND ND ND ND ND ND 3.55 B ND 3.01 J
07/07/11 2.7 10 ND ND 6.34 (0.985) B ND ND ND ND ND 2.79 (6.37)B ND ND ND 3.21 J
01/12/12 2.7 10 ND ND ND 2.20 J ND ND ND ND 29.20 2.17 J 1.60 J ND ND
07/12/12 --- 10.0 ND ND ND ND ND ND ND 1.03 J 2.18 J 0.91 J 2.05 J 0.73 J ND
02/06/13 --- 10.0 ND ND ND ND ND 0.56 J ND ND 2.56 J 1.50 J ND ND ND
07/09/13 --- 10.0 ND ND ND ND ND ND ND 0.85 J 3.31 J 1.21 J 1.13 J ND ND
01/31/14 --- 10.0 ND ND ND ND ND ND ND 0.91 J 3.04 J 1.42 J 1.17 J ND ND
07/23/14 --- 10.0 ND ND ND ND ND 1.03 J 1.33 J 1.99 J 2.80 J 1.73 J 4.99 J 1.11 J ND
01/27/15 1.01 10.0 ND ND ND ND ND ND ND ND 3.62 J 1.66 J 2.41 J ND ND
07/29/15 0.85 10.0 ND ND ND ND ND 1.20 J ND 0.93 J 3.05 J 1.25 J 4.12 J 1.07 J ND
06/23/16 0.85 10.0 ND ND ND ND ND ND ND ND 16.7 1.20 J 2.33 J ND ND
11/02/16 1.00 10.0 ND ND ND ND ND ND ND ND 19.8 R1 J ND 2.21 J ND ND
05/31/17 1.41 10.0 ND ND ND ND ND ND ND ND ND ND 1.45 J ND ND
Total Silver 07/22/09 1.0 10 ND ND ND ND 1.28 J ND ND ND 1.04 J ND ND ND ND
NC2L = 20 µg/l 01/26/10 0.5 10 0.68 B 0.56 B 1.17 B ND 0.549 B 0.92 B 0.52 B 0.529 B 0.60 B 1.57 B 0.84 B 0.83 B 0.73 J
07/07/10 1.9 10 ND ND ND ND ND ND ND ND ND ND ND ND ND
01/05/11 1.9 10 ND ND ND ND ND ND ND ND ND ND 2.68 J ND ND
07/07/11 1.9 10 ND ND ND ND ND ND ND ND ND ND ND ND ND
01/12/12 1.9 10 ND ND 0.22 ND ND ND ND 0.58 J 0.20 J ND ND ND ND
07/12/12 --- 10.0 0.14 J ND 0.23 J ND ND ND ND ND ND ND 0.16 J 0.24 J ND
02/06/13 --- 10.0 ND ND ND ND ND ND ND ND ND ND 0.28 J ND ND
07/09/13 --- 10.0 0.85 J ND ND ND ND ND ND ND ND ND 0.51 J ND ND
01/31/14 --- 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/23/14 --- 10.0 ND ND ND ND ND ND ND ND ND ND ND 0.86 J ND
01/27/15 0.17 10.0 0.21 J 0.24 J 0.26 J 0.18 J ND ND ND ND ND 0.23 J ND 3.11 J ND
07/29/15 0.22 10.0 ND ND ND ND ND ND ND ND 0.28 J ND ND ND ND
06/23/16 0.22 10.0 ND ND ND ND ND ND ND ND 0.44 J ND ND ND ND
11/02/16 0.48 10.0 ND ND ND ND ND ND ND ND ND R1 ND ND 4.77 J ND
05/31/17 0.32 10.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
Organic Compounds
Acetone 07/22/09 1.5 100 ND ND ND ND ND ND ND ND ND ND 2.0 J ND ND
NC2L = 6000 µg/l 01/26/10 1.5 100 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/07/10 1.5 100 ND ND ND ND ND ND ND ND ND ND ND ND ND
01/05/11 1.5 100 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/07/11 1.2 100 ND ND ND ND ND ND ND ND ND ND 10.0 J ND ND
01/12/12 1.2 100 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/12/12 --- 100 ND ND ND ND ND ND ND ND ND ND ND ND ND
02/06/13 --- 100 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/09/13 --- 100 ND ND ND ND ND ND ND ND ND ND ND ND 2.4 J
01/31/14 --- 100 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/23/14 --- 100 ND ND ND 6.3 J ND ND ND ND ND ND 8.6 J ND ND
01/27/15 5.7 100 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/29/15 3.1 100 ND ND ND ND ND ND ND ND ND ND ND ND ND
06/23/16 4.9 100 ND ND ND ND ND ND ND ND ND ND ND ND ND
11/02/16 4.9 100 ND ND ND ND ND ND ND ND ND ND ND ND ND
05/31/17 8.2 100 ND ND ND ND ND ND ND ND ND ND ND ND ND
Benzene 07/22/09 0.2 1 ND ND ND ND ND ND ND ND ND ND ND ND ND
NC2L = 1 µg/l 01/26/10 0.1 1 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/07/10 0.2 1 ND ND ND ND ND ND ND ND ND ND 0.5 J ND ND
01/05/11 0.2 1 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/07/11 0.7 1 ND ND ND ND ND ND ND ND ND ND ND ND ND
01/12/12 --- 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/12/12 --- 1.0 ND ND ND ND ND ND ND ND ND ND 0.4 J ND ND
02/06/13 --- 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/09/13 --- 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
01/31/14 --- 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/23/14 --- 1.0 ND ND ND ND ND ND ND ND ND ND 0.6 J ND ND
01/27/15 0.2 1.0 ND ND ND ND ND ND ND ND ND ND 0.2 J ND ND
07/29/15 0.2 1.0 ND ND ND ND ND ND ND ND ND ND 0.5 J ND ND
06/23/16 0.2 1.0 ND ND ND ND ND ND ND ND ND ND 0.5 J ND ND
11/02/16 0.2 1.0 ND ND ND ND ND ND ND ND ND ND 0.5 J ND ND
05/31/17 0.2 1.0 ND ND ND ND ND ND ND ND ND ND 0.6 J ND ND
Chloroform 07/22/09 0.2 5 ND ND 0.6 J ND ND ND ND ND ND ND ND ND ND
NC2L = 70 µg/l 01/26/10 0.1 5 ND ND 0.7 J ND ND ND ND ND ND ND ND ND ND
07/07/10 0.2 5 ND ND 0.4 J ND ND ND ND ND ND ND ND ND ND
01/05/11 0.2 5 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/07/11 0.7 5 ND ND ND ND ND ND ND ND ND ND ND ND ND
01/12/12 --- 5.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/12/12 --- 5.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
02/06/13 --- 5.0 ND ND 0.5 J ND ND ND ND ND ND ND ND ND ND
07/09/13 --- 5.0 ND ND 0.4 B ND ND ND ND ND ND ND ND ND 0.50 J
01/31/14 --- 5.0 ND ND 0.3 J ND ND ND ND 0.3 J ND ND ND ND ND
07/23/14 --- 5.0 ND ND 0.3 J ND ND ND ND ND ND ND ND ND ND
01/27/15 0.2 5.0 ND ND ND ND ND ND ND 0.2 J ND ND ND ND ND
07/29/15 0.2 5.0 ND ND ND ND ND ND ND 0.2 J ND ND ND ND ND
06/23/16 0.3 5.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
11/02/16 0.3 5.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
05/31/17 0.6 5.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
Holly Springs Closed C and D Landfill
Permit No. 92-14 Page 2 of 4 Joyce Engineering
APPENDIX C
Historical Groundwater Constituents/Analytes
Analyte
Collection Date DL SWSL MW-1R MW-10 MW-2 MW-3 MW-4 MW-5R MW-6 MW-7 MW-9 MW-11 MW-12 MW-13 Blanks
Chloromethane 07/22/09 0.3 1 ND ND ND ND ND ND ND ND ND ND ND ND ND
NC2L = 3 µg/l 01/26/10 0.1 1 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/07/10 0.3 1 ND ND ND ND ND ND ND ND 0.45 J ND 0.43 J ND ND
01/05/11 0.3 1 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/07/11 0.6 1 ND ND ND ND ND ND ND ND ND ND ND ND ND
01/12/12 0.6 1 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/12/12 --- 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
02/06/13 --- 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/09/13 --- 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
01/31/14 --- 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/23/14 --- 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
01/27/15 0.2 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/29/15 0.4 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
06/23/16 0.4 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
11/02/16 0.4 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
05/31/17 0.4 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
Methyl Ethyl Ketone (2-Butanone) 07/23/14 --- 100 2.0 J ND 0.9 J ND ND ND ND ND ND ND ND ND ND
NC2L = 4,000 µg/l 01/27/15 0.8 100 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/29/15 0.9 100 ND ND ND ND ND ND ND ND ND ND ND ND ND
06/23/16 1.1 100 ND ND ND ND ND ND ND ND ND ND ND ND ND
11/02/16 1.1 100 ND ND ND ND ND ND ND ND ND ND ND ND ND
05/31/17 3.2 100 ND ND ND ND ND ND ND ND ND ND ND ND ND
Toluene 07/22/09 0.3 1 0.84 J ND ND ND ND ND ND ND ND ND ND ND ND
NC2L = 600 µg/l 01/26/10 0.1 1 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/07/10 0.3 1 ND ND ND ND ND ND ND ND ND ND ND ND ND
01/05/11 0.3 1 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/07/11 0.9 1 ND ND ND ND ND ND ND ND ND ND 1.80 ND ND
07/14/11 0.9 1 ND ND ND ND ND ND ND ND ND ND ND ND ND
01/12/12 0.6 1 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/12/12 --- 1.0 ND ND 0.20 J ND ND ND ND ND ND ND ND ND ND
02/06/13 --- 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/09/13 --- 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
01/31/14 --- 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/23/14 --- 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
01/27/15 0.2 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/29/15 0.2 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
06/23/16 0.3 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
11/02/16 0.3 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
05/31/17 0.3 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
Tetrachloroethene 07/29/15 0.3 1.0 ND 0.50 J 0.30 J ND ND 0.40 J 0.30 J ND ND ND ND ND ND
06/23/16 0.4 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
NC2L = 0.7 µg/l 11/02/16 0.4 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
05/31/17 0.8 1.0 ND ND ND ND ND ND ND ND ND ND ND ND ND
Tetrahydrofuran 01/05/11 0.8 10 ND ND ND ND ND ND ND ND ND ND ND ND ND
(No Standard)07/07/11 0.8 10 ND ND ND ND 1.7 ND ND 3.4 ND 2.80 1.20 ND ND
01/12/12 0.8 10 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/12/12 --- 10 ND ND ND ND ND ND ND ND ND ND ND ND ND
02/06/13 --- 10 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/09/13 --- 10 ND ND ND ND ND ND ND ND ND ND ND ND ND
01/31/14 --- 10 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/23/14 --- 10 ND ND ND ND ND ND ND ND ND ND ND ND ND
01/27/15 3.9 10 ND ND ND ND ND ND ND ND ND ND ND ND ND
07/29/15 0.7 10 ND ND ND ND ND 2.3 J ND 4.0 J ND 3.5 J 3.2 J ND ND
06/23/16 1.5 10 ND ND ND ND ND ND ND 2.9 J ND 1.8 J 3.1 J ND ND
11/02/16 1.5 10 ND ND ND ND ND 2.1 J ND ND ND 2.5 J ND ND ND
05/31/17 1.3 10 ND ND ND ND 1.9 J ND ND 1.6 J ND ND 1.8 J ND ND
Field Parameters
pH 07/22/09 -- -- 7.20 6.70 6.19 5.94 5.47 6.03 5.97 5.35 5.20 5.46 5.04 5.61 --
S.U.01/26/10 -- -- 6.80 6.46 6.04 6.18 5.38 5.76 5.90 5.14 5.07 5.39 5.38 5.50 --
07/07/10 -- -- 6.64 6.24 6.52 6.13 5.72 6.00 6.04 5.29 5.35 5.68 5.40 5.89 --
01/05/11 -- -- 6.79 6.12 6.18 5.99 5.54 5.92 5.88 5.6 5.39 5.69 5.45 5.84 --
07/07/11 -- -- 6.66 5.93 6.25 5.95 5.31 5.78 5.60 5.16 5.10 5.38 5.23 5.67 --
01/12/12 -- -- 7.06 6.41 6.39 6.14 5.78 7.73 7.81 6.24 5.40 6.35 5.66 5.99 --
07/12/12 -- -- 7.16 6.74 6.56 6.30 5.78 6.19 6.10 5.49 5.33 5.73 5.58 5.99 --
02/06/13 -- -- 6.80 6.49 6.25 6.13 5.64 6.19 6.09 5.95 5.33 5.70 5.38 5.86 --
07/09/13 -- -- 7.05 6.59 6.60 5.61 5.08 6.19 5.99 5.29 5.3 5.50 5.95 5.48 --
01/31/14 -- -- 7.06 6.96 6.87 6.29 6.71 6.45 6.75 6.02 6.13 6.10 6.29 7.19 --
07/23/14 --- --- 6.72 6.37 6.14 6.5 5.90 6.05 5.32 5.16 5.25 5.77 5.42 5.72 ---
01/27/15 FIELD FIELD 5.84 5.45 6.05 6.03 5.39 6.06 5.80 5.65 5.23 5.95 5.75 5.53 ---
07/29/15 FIELD FIELD 6.45 6.30 6.57 6.14 5.60 6.30 6.15 5.53 5.49 5.82 5.68 6.07 ---
06/23/16 FIELD FIELD 5.42 5.54 5.54 5.36 5.20 4.75 4.69 4.47 4.48 4.55 4.77 5.06 ---
11/02/16 FIELD FIELD 5.02 4.62 4.61 4.76 4.35 4.60 4.75 4.29 4.68 4.37 4.65 4.54 ---
05/31/17 FIELD FIELD 6.43 6.40 6.52 6.36 5.54 6.20 6.32 5.44 5.53 5.83 5.69 5.93 ---
Conductivity 07/22/09 -- -- 295 188 283 93.0 104 676 322 168 640 907 526 477 --
µS/cm 01/26/10 -- -- 296 186 283 99.0 100 673 376 151 791 934 503 444 --
07/07/10 -- -- 276 154 266 95.0 106 717 315 197 729 852 590 432 --
01/05/11 -- -- 272 143 294 111.0 114 757 337 162 889 966 629 471 --
07/07/11 -- -- 264 137 249 93.0 103 676 319 191 793 774 605 460 --
01/12/12 -- -- 218 166 254 87.0 95 558 271 137 709 709 621 424 --
07/12/12 -- -- 248 142.2 225.9 86.5 97.6 621 294 192.7 685 687 597 445.6 --
02/06/13 -- -- 257 157.8 215.2 79.4 100.6 517 278.9 114.7 692 683 201 406.3 --
07/09/13 -- -- 238 6.59 195.1 69.7 87.8 538 249.3 45.1 572 554 587 372 --
01/31/14 -- -- 220 14.0 220.7 77.9 100.6 589 282.6 158.4 631 752 429 368.2 --
07/23/14 --- --- 262 118.0 236.0 92.3 115.7 648 309.1 198 629 776 673 472.3 ---
01/27/15 FIELD FIELD 2361 114.3 199.8 65.2 109.6 573 283.2 146.7 676 596 532 363.3 ---
07/29/15 FIELD FIELD 265 124 211 68.0 113 630 286 141 636 649 641 433 ---
06/23/16 FIELD FIELD 315.1 122.9 222.7 73.4 126.8 679 313.5 197.2 761 649 752 391 ---
11/02/16 FIELD FIELD 298.2 127.3 216.1 69.4 131.6 740 300.5 238.3 1000 703 765 356.1 ---
05/31/17 FIELD FIELD 319.3 108.5 211.5 69.2 132.7 653 294.2 184.3 607 622 692 379.9 ---
Holly Springs Closed C and D Landfill
Permit No. 92-14 Page 3 of 4 Joyce Engineering
APPENDIX C
Historical Groundwater Constituents/Analytes
Analyte
Collection Date DL SWSL MW-1R MW-10 MW-2 MW-3 MW-4 MW-5R MW-6 MW-7 MW-9 MW-11 MW-12 MW-13 Blanks
Temperature 07/22/09 -- -- 22.31 17.98 19.84 20.64 18.96 17.43 18.57 18.84 18.23 17.03 19.23 28.29 --
°C 01/26/10 -- -- 16.22 15.72 12.89 10.09 15.73 13.39 13.26 12.3 13.23 14.52 14.32 12.67 --
07/07/10 -- -- 20.97 23.07 19.09 22.46 18.97 18.5 19.44 19.23 17.75 19.28 17.33 18.5 --
01/05/11 -- -- 15.19 13.16 13.22 16.14 15.76 12.97 15.94 13.68 13.98 14.46 14.09 14.64 --
07/07/11 -- -- 19 21.21 21.2 22.05 19.5 17.96 19.23 21.14 20.17 18.59 17.07 18.41 --
01/12/12 -- -- 13.33 14.55 16.48 17.55 17 14.24 15.27 14.76 15.56 15.88 14.97 14.78 --
07/12/12 -- -- 18.8 19.60 19.4 20.70 18.2 18.1 18.40 18.8 17.80 18.40 16.2 20.9 --
02/06/13 -- -- 13.9 17.40 17.2 16.90 16.5 14.8 16.20 14.9 14.90 15.60 14.5 14.6 --
07/09/13 -- -- 22.5 17.10 17.3 17.20 16.2 15.7 16.20 15.3 15.30 15.30 16 17 --
01/31/14 -- -- 12.7 16.70 15.6 14.50 15.7 14.5 15.00 14.1 14.40 14.70 14.1 14 --
07/23/14 --- --- 19.6 19.10 19.1 ---16.9 16.3 17.70 16.4 16.40 18.30 15.9 17.7 ---
01/27/15 FIELD FIELD 12.7 16.9 15.4 15.1 15.9 13.8 15.1 13.5 13.7 13.8 13.9 13.7 ---
07/29/15 FIELD FIELD 19.2 19.53 19.75 17.98 17.36 17.97 18.40 17.50 16.30 17.69 16.68 19.79 ---
06/23/16 FIELD FIELD 17.7 17.7 16.7 18.4 15.8 15.6 16.7 15.7 15.7 15.5 17.2 16.2 ---
11/02/16 FIELD FIELD 16.9 17.4 16.5 18.2 16.8 17.8 18.7 17.1 18.1 17.5 17.8 17.7 ---
05/31/17 FIELD FIELD 19.2 17.6 17.2 17.9 16.8 15.5 16.8 15.8 15.9 15.4 16.0 15.7 ---
Turbidity 07/22/09 -- -- 7.51 10.80 5.82 11.20 2.52 4.17 8.48 12 51.60 96.30 42.40 22.40 --
NTU 01/26/10 -- -- 135.0 1.95 1.6 5.51 1.19 0.7 2.89 1 64.60 1.82 43.90 78.60 --
07/07/10 -- -- 7.7 0.61 5.2 3.98 1.97 0.7 1.43 1.72 62.20 1.1 2.30 66.70 --
01/05/11 -- -- 0.3 0.97 1.6 2.70 1.7 0.4 0.44 0.41 66.70 0.92 5.89 17.50 --
07/07/11 -- -- 0.4 5.69 3.9 3.31 2.26 1.3 0.84 1.88 91.5 5.0 2.39 52.40 --
01/12/12 -- -- 8.8 0.73 1.2 8.43 6.81 6.2 6.23 11.11 30.10 19.30 4.45 9.55 --
07/12/12 -- -- 3.1 1.99 2.6 9.10 3.77 3.3 4.62 2.73 16.7 3.41 4.76 5.67 --
02/06/13 -- -- 16.5 12.60 4.7 16.70 2.5 --13.40 4.27 16.00 6.02 44.90 ----
07/09/13 -- -- 5.4 5.03 7.6 7.81 5.8 7.1 9.37 8.72 15.3 5.29 48.20 6.15 --
01/31/14 -- -- 4.1 5.81 4.9 4.02 3.99 4.2 5.89 5.32 8.4 5.11 4.40 4.02 --
07/23/14 --- --- 4.6 3.25 3.8 25.0 4.34 3.5 3.44 5.5 6.3 6.51 5.02 27.10 ---
01/27/15 FIELD FIELD 3.95 3.64 1.83 34.3 1.06 1.14 1.1 0.95 17.4 21.8 5.93 729 ---
07/29/15 FIELD FIELD 7.9 4.8 4.6 4.6 4.5 8 4.6 3.5 153 6.1 7.4 38.4 ---
06/23/16 FIELD FIELD 3.49 4.47 4.30 5.05 3.00 4.79 1.32 2.11 97.3 1.75 11.91 5.24 ---
11/02/16 FIELD FIELD 5.35 2.56 2.78 2.76 3.54 3.06 3.1 2.71 260 3.17 9.37 2.66 ---
05/31/17 FIELD FIELD 4.06 3.98 8.70 4.21 4.29 5.86 8.87 3.64 15.1 5.29 15.17 2.86 ---
Oxidation Reduction Potential 07/22/09 -- -- 75.4 92.10 44.1 56.70 108.1 95.4 104.10 128 127.4 118.30 67.30 -20.30 --
mV 01/26/10 -- -- -- 121.10 132.9 175.50 190.3 156.8 115.10 220.1 192.6 174.10 122.20 101.00 --
07/07/10 -- -- -71.7 -39.30 -3.1 -20.70 53.8 6.2 -31.40 65.9 -46.5 -47.20 -101.10 -116.00 --
01/05/11 -- -- 46.1 94.10 114.2 109.80 153.5 190.6 173.60 149.5 262.5 139.50 81.70 124.30 --
07/07/11 -- -- -0.7 104.70 17.0 104.50 77 69.7 79.60 67.2 104.0 18.00 -26.20 77.90 --
01/12/12 -- -- -39 249.20 83 150.60 61.3 174 -237.80 24.8 201.1 26.70 -18.20 -4.10 --
07/12/12 -- -- 77.8 67.60 25.7 71.50 125.2 138.4 123.70 137.1 110.2 145.90 4.10 -28.60 --
02/06/13 -- -- 139.1 131.30 89.3 98.00 179.6 63.2 278.90 182 137.4 211.30 80.20 55.10 --
07/09/13 -- -- 88.20 159.50 53.10 106.60 174.1 121.90 5.40 169.4 103.10 144.20 100.00 67.90 --
01/31/14 -- -- 10.80 60.20 65.10 97.60 92.3 51.30 71.00 124.2 100.60 60.20 95.00 48.90 --
07/23/14 --- --- 765.0 49.1 75.8 29.7 84.2 -567.0 29.2 94.2 98.2 57.5 792.0 80.0 ---
01/27/15 FIELD FIELD 1239.0 125.0 100.4 120.8 142.1 127.1 115.4 140.1 142.3 137.3 105.6 102.4 ---
07/29/15 FIELD FIELD 77.5 77.9 21.7 87.6 124.5 -80.6 20.1 146.6 79.5 61.9 -2.0 43.7 ---
06/23/16 FIELD FIELD 48.0 59.7 56.3 8.2 93.1 66.0 60.2 88.0 -19.9 89.1 15.7 -72.1 ---
11/02/16 FIELD FIELD 61.4 55.1 -9.6 42.8 76.7 -83.7 41.2 53.2 21.9 -27.0 -35.5 -95.6 ---
05/31/17 FIELD FIELD 123.4 83.1 16.8 30.0 99.2 94.8 62.6 106.5 108.8 108.5 33.8 -49.1 ---
Dissolved Oxygen 07/22/09 -- -- 3.50 4.16 3.31 3.80 1.58 0.53 1.53 0.67 0.42 0.40 0.67 0.78 --
mg/l 01/26/10 -- -- --7.70 4.64 8.96 4.01 3.43 5.18 6.51 1.76 7.60 1.27 1.89 --
07/07/10 -- -- 3.70 6.40 4.30 3.60 2.59 2.17 1.03 0.5 0.28 0.57 0.83 0.46 --
01/05/11 -- -- 1.32 4.36 2.16 4.04 2.72 3.92 2.19 4.66 2.46 4.63 0.73 1.26 --
07/07/11 -- -- 2.63 5.88 3.12 3.88 3.83 1.18 0.90 0.9 0.71 0.89 0.99 0.63 --
01/12/12 -- -- 0.69 3.03 2.04 5.50 2.19 2.51 1.00 4.07 2.87 6.18 3.01 0.70 --
07/12/12 -- -- 3.68 5.72 0.96 3.38 2.37 0.21 0.52 0.3 0.73 0.33 0.27 0.26 --
02/06/13 -- -- 1.67 2.50 1.48 5.29 4.11 2.99 2.97 5.41 0.86 2.96 0.28 0.88 --
07/09/13 -- -- 5.25 6.89 0.80 0.49 2.66 0.51 0.22 1.29 0.57 0.86 1.58 1.07 --
01/31/14 -- -- 2.94 3.98 0.43 5.79 2.2 2.88 1.24 2.8 1.04 7.65 2.38 1.61 --
07/23/14 --- --- 4.51 5.60 1.42 5.25 2.1 0.98 0.84 1.06 1.77 3.40 1.23 1.12 ---
01/27/15 FIELD FIELD 2.07 5.84 4.95 7.14 2.38 3.36 1.87 3.95 2.49 8.11 1.38 2.69 ---
07/29/15 FIELD FIELD 0.42 6.13 0.60 5.99 1.12 0.86 0.35 0.95 0.41 1.89 0.81 0.67 ---
06/23/16 FIELD FIELD 1.93 2.70 0.59 2.67 1.6 0.40 1.07 0.81 0.32 0.49 2.47 0.60 ---
11/02/16 FIELD FIELD 1.54 4.84 0.41 3.74 0.53 0.35 0.36 0.40 4.29 0.27 1.76 0.43 ---
05/31/17 FIELD FIELD 3.40 6.11 1.28 3.51 2.25 0.99 1.69 1.03 1.32 1.77 1.21 2.09 ---
Notes:
DL = Method Detection Limit.
SWSL = NC-DENR Solid Waste Section Limit.
NC2L = Groundwater Standard established in 15 A NCAC 2L.0202
GWPS = NC DENR Solid Waste Section Groundwater Protection Standard for constituents with no listed NC2L.
ND = Not detected above the DL.
J = Estimated concentration below the RL.
B = Blank qualified data.
dry = Insufficient water to sample.
--- = No data.
mg/l = milligrams per liter
µg/l = micrograms per liter
S.U. = Standard Units.
NTU = Nephelometric Turbidity Units.
µS/cm= microsiemens per centimeter.
mV = Millivolts.Bold = Concentrations above the NC2L or Groundwater Protection standards (GWPS) have been bolded.Blanks = field, trip and/or method blanks.
All data prior to 2012 taken from previous reports by Golder Associates NC, Inc.
Dissolved Metals Analysis - results for dissolved metals analysis for MW-9, collected 11/02/16 at time of sampling due to high sample turbidity. MW-9 metals exceedances were due to high sample turbidity.R1 = Lab flagged result with Qualifier "R-01: Elevated reporting limit due to matrix interference". The elevated reporting limits affect MW-9 Cadmium and Silver results that were below their respective detection limits, and Selenium that was below its quantitation limits due to the matrix interferrence.
Holly Springs Closed C and D Landfill
Permit No. 92-14 Page 4 of 4 Joyce Engineering

Appendix D

Historical Surface Water Constituents

APPENDIX D
Historical Surface Water Constituents/Analytes
Analyte
Sample
Collection Date DL RL SW-1 SW-2 Blanks
Inorganic Compounds
Total Arsenic 07/22/09 --- --- dry dry ---
NC2B = 50 µg/l 01/26/10 10 10.0 ND ND ND
07/07/10 10 10.0 dry dry ND
01/05/11 10 10.0 dry ND ND
07/07/11 10 10.0 dry ND ND
01/12/12 --- 10.0 ND ND ND
07/12/12 --- 10.0 dry ND ND
02/06/13 --- 10.0 dry ND ND
07/09/13 --- 10.0 ND 2.39 J ND
01/31/14 --- 10.0 dry ND ND
07/23/14 --- --- dry dry ---
01/27/15 1.13 10.0 ND ND ND
07/29/15 0.75 10.0 dry dry ---
NC2B = 10 µg/l 06/23/16 0.75 10.0 dry 2.10 J ND
11/02/16 1.64 10.0 dry 6.94 J ND
05/31/17 0.42 10.0 dry 2.28 J ND
Total Barium 07/22/09 --- --- dry dry ---
No NC2B Standard 01/26/10 10 100 45.2 J 52.3 J 0.66 J
07/07/10 10 100 dry dry ND
01/05/11 10 100 dry 39.1 J ND
07/07/11 10 100 dry 43.8 J ND
01/12/12 --- 100 74.2 J 48.1 J 0.90 J
07/12/12 --- 100 dry 35.1 J 1.47 J
02/06/13 --- 100 dry 59.8 J 1.05 J
07/09/13 --- 100 51.2 J 79.4 J 0.46 J
01/31/14 --- 100 dry 65.2 J ND
07/23/14 --- --- dry dry ---
01/27/15 0.10 100 37.1 J 75.9 J 0.17 J
07/29/15 0.30 100 dry dry ---
NC2B = 200,000 µg/l 06/23/16 0.30 100 dry 78.4 J 3.40 J
11/02/16 0.44 100 dry 143.0 0.49 J
05/31/17 0.27 100 dry 54.8 J ND
Total Cadmium 07/22/09 --- --- dry dry ---
NC2B = 2 µg/l 01/26/10 1 1.00 0.14 B ND 0.14 J
07/07/10 1 1.00 dry dry ND
01/05/11 1 1.00 dry ND ND
07/07/11 1 1.00 dry ND ND
01/12/12 --- 1.00 ND ND ND
07/12/12 --- 1.00 dry ND ND
02/06/13 --- 1.00 dry ND ND
07/09/13 --- 1.00 ND 0.07 J ND
01/31/14 --- 1.00 dry ND ND
07/23/14 --- --- dry dry ---
01/27/15 0.05 1.00 ND ND ND
07/29/15 0.10 1.00 dry dry ---
NC2B = 0.15 µg/l * 06/23/16 0.10 1.00 dry ND ND
11/02/16 0.07 1.00 dry ND ND
05/31/17 0.06 1.00 dry ND ND
Holly Springs Closed C and D Landfill
Permit No. 92-14 1 of 6 Joyce Engineering
APPENDIX D
Historical Surface Water Constituents/Analytes
Analyte
Sample
Collection Date DL RL SW-1 SW-2 Blanks
Total Chromium 07/22/09 --- --- dry dry ---
NC2B = 50 µg/l 01/26/10 10 10.0 ND ND ND
07/07/10 10 10.0 dry dry ND
01/05/11 10 10.0 dry ND ND
07/07/11 10 10.0 dry 1.85 J ND
01/12/12 --- 10.0 2.45 B 2.56 B 0.82 J
07/12/12 --- 10.0 dry ND ND
02/06/13 --- 10.0 dry 1.46 B 1.42 J
07/09/13 --- 10.0 3.12 B 3.03 B 3.51 J
01/31/14 --- 10.0 dry 0.97 B 2.79 J
07/23/14 --- --- dry dry ---
01/27/15 0.73 10.0 ND 3.31 J ND
07/29/15 0.43 10.0 dry dry ---
NC2B = 180 µg/l *06/23/16 0.43 10.0 dry 1.05 J ND
11/02/16 0.94 10.0 dry 2.78 J ND
05/31/17 0.34 10.0 dry 1.12 J ND
Total Lead 07/22/09 --- --- dry dry ---
NC2B = 25 µg/l 01/26/10 10 10.0 ND ND ND
07/07/10 10 10.0 dry dry ND
01/05/11 10 10.0 dry ND ND
07/07/11 10 10.0 dry ND ND
01/12/12 --- 10.0 1.52 J 0.35 J ND
07/12/12 --- 10.0 dry 0.17 J ND
02/06/13 --- 10.0 dry ND ND
07/09/13 --- 10.0 1.26 J 4.50 J 0.08 J
01/31/14 --- 10.0 dry 0.08 J ND
07/23/14 --- --- dry dry ---
01/27/15 0.05 10.0 0.59 J 0.31 J ND
07/29/15 0.08 10.00 dry dry ---
NC2B = 14 µg/l *06/23/16 0.08 10.0 dry 0.57 J 0.26 J
11/02/16 0.12 10.0 dry 0.14 J ND
05/31/17 0.07 10.0 dry ND ND
Total Mercury 07/22/09 --- --- dry dry ---
NC2B = 0.012 µg/l 01/26/10 0.2 0.200 0.06 J ND ND
07/07/10 0.2 0.200 dry dry ND
01/05/11 0.2 0.200 dry ND ND
07/07/11 0.2 0.200 dry ND ND
01/12/12 --- 0.200 ND ND ND
07/12/12 --- 0.200 dry ND ND
02/06/13 --- 0.200 dry ND ND
07/09/13 --- 0.200 0.08 J ND ND
01/31/14 --- 0.200 dry ND 0.114 J
07/23/14 --- --- dry dry ---
01/27/15 0.064 0.200 ND ND ND
07/29/15 0.07 0.20 dry dry ---
NC2B = 0.012 µg/l 06/23/16 0.132 0.200 dry ND ND
11/02/16 0.041 0.200 dry ND ND
05/31/17 0.041 0.200 dry ND ND
Holly Springs Closed C and D Landfill
Permit No. 92-14 2 of 6 Joyce Engineering
APPENDIX D
Historical Surface Water Constituents/Analytes
Analyte
Sample
Collection Date DL RL SW-1 SW-2 Blanks
Total Selenium 07/22/09 --- --- dry dry ---
NC2B = 5 µg/l 01/26/10 1 10.0 ND ND ND
07/07/10 10 10.0 dry dry ND
01/05/11 10 10.0 dry ND 3.01 J
07/07/11 10 10.0 dry ND 3.21 J
01/12/12 --- 10.0 ND 0.81 J ND
07/12/12 --- 10.0 dry 0.72 J ND
02/06/13 --- 10.0 dry 1.59 J ND
07/09/13 --- 10.0 ND 1.65 J ND
01/31/14 --- 10.0 dry 1.19 J ND
07/23/14 --- --- dry dry ---
01/27/15 1.01 10.0 ND ND ND
07/29/15 0.85 10.0 dry dry ---
NC2B = 5 µg/l 06/23/16 0.85 10.0 dry 1.06 J ND
11/02/16 1 10.0 dry 2.00 J ND
05/31/17 1.41 10.0 dry ND ND
Total Silver 07/22/09 --- --- dry dry ---
NC2B = 0.06 µg/l 01/26/10 10 10.0 ND ND 0.73 J
07/07/10 10 10.0 dry dry ND
01/05/11 10 10.0 dry ND ND
07/07/11 10 10.0 dry ND ND
01/12/12 --- 10.0 ND ND ND
07/12/12 --- 10.0 dry ND ND
02/06/13 --- 10.0 dry ND ND
07/09/13 --- 10.0 ND ND ND
01/31/14 --- 10.0 dry ND ND
07/23/14 --- --- dry dry ---
01/27/15 0.17 10.0 ND ND ND
07/29/15 0.22 10.0 dry dry ---
NC2B = 0.3 µg/l *06/23/16 0.22 10.0 dry ND ND
11/02/16 0.48 10.0 dry ND ND
05/31/17 0.32 10.0 dry ND ND
Holly Springs Closed C and D Landfill
Permit No. 92-14 3 of 6 Joyce Engineering
APPENDIX D
Historical Surface Water Constituents/Analytes
Analyte
Sample
Collection Date DL RL SW-1 SW-2 Blanks
Organic Compounds
Acetone 01/26/10 5 100 ND ND ND
No NC2B Standard 07/07/10 5 100 dry dry ND
01/05/11 5 100 dry ND ND
07/07/11 5 100 dry 4.4 J ND
01/12/12 --- 100 ND ND ND
07/12/12 --- 100 dry ND ND
02/06/13 --- 100 dry ND ND
07/09/13 --- 100 1.80 B 3.50 B 2.40 J
01/31/14 --- 100 dry ND ND
07/23/14 --- --- dry dry ---
01/27/15 5.7 100.0 ND ND ND
07/29/15 4.9 100 dry dry ---
NC2B = 2,000 µg/l 06/23/16 4.9 100 dry ND ND
11/02/16 4.9 100 dry ND ND
05/31/17 8.2 100 dry ND ND
Field Parameters
pH 07/22/09 --- --- dry dry ---
S.U. 01/26/10 --- --- 6.65 5.71 ---
07/07/10 --- --- dry dry ---
01/05/11 --- --- dry 6.43 ---
07/07/11 --- --- dry 6.87 ---
01/12/12 --- --- 5.83 6.92 ---
07/12/12 --- --- dry 7.25 ---
02/06/13 --- --- dry 6.63 ---
07/09/13 --- --- 6.33 6.29 ---
01/31/14 --- --- dry 6.76 ---
07/23/14 --- --- dry dry ---
01/27/15 FIELD FIELD 6.07 6.30 ---
07/29/15 FIELD FIELD dry dry ---
06/23/16 FIELD FIELD dry 5.09 ---
11/02/16 FIELD FIELD dry 4.97 ---
05/31/17 FIELD FIELD dry 6.56 ---
Holly Springs Closed C and D Landfill
Permit No. 92-14 4 of 6 Joyce Engineering
APPENDIX D
Historical Surface Water Constituents/Analytes
Analyte
Sample
Collection Date DL RL SW-1 SW-2 Blanks
Conductivity 07/22/09 --- --- dry dry ---
µS/cm 01/26/10 --- --- 49.00 191.0 ---
07/07/10 --- --- dry dry ---
01/05/11 --- --- dry 190.0 ---
07/07/11 --- --- dry 430.0 ---
01/12/12 --- --- 115.00 527.0 ---
07/12/12 --- --- dry 383.5 ---
02/06/13 --- --- dry 652.9 ---
07/09/13 --- --- 99.90 771.0 ---
01/31/14 --- --- dry 506.0 ---
07/23/14 --- --- dry dry ---
01/27/15 FIELD FIELD 260.9 397.2 ---
07/29/15 FIELD FIELD dry dry ---
06/23/16 FIELD FIELD dry 819.0 ---
11/02/16 FIELD FIELD dry 894.0 ---
05/31/17 FIELD FIELD dry 540.00 ---
Temperature 07/22/09 --- --- dry dry ---
°C 01/26/10 --- --- 6.71 9.16 ---
07/07/10 --- --- dry dry ---
01/05/11 --- --- dry 5.85 ---
07/07/11 --- --- dry 21.94 ---
01/12/12 --- --- 10.2 11.02 ---
07/12/12 --- --- dry 23.00 ---
02/06/13 --- --- dry 10.60 ---
07/09/13 --- --- 24.20 23.90 ---
01/31/14 --- --- dry 4.50 ---
07/23/14 --- --- dry dry ---
01/27/15 FIELD FIELD 7.0 6.5 ---
07/29/15 FIELD FIELD dry dry ---
06/23/16 FIELD FIELD dry 20.1 ---
11/02/16 FIELD FIELD dry 15.2 ---
05/31/17 FIELD FIELD dry 20.00 ---
Holly Springs Closed C and D Landfill
Permit No. 92-14 5 of 6 Joyce Engineering
APPENDIX D
Historical Surface Water Constituents/Analytes
Analyte
Sample
Collection Date DL RL SW-1 SW-2 Blanks
Turbidity 07/22/09 --- --- dry dry ---
NTU 01/26/10 --- --- 7.79 1.70 ---
07/07/10 --- --- dry dry ---
01/05/11 --- --- dry 5.33 ---
07/07/11 --- --- dry 22.30 ---
01/12/12 --- --- 25.50 13.87 ---
07/12/12 --- --- dry 45.00 ---
02/06/13 --- --- dry 4.60 ---
07/09/13 --- --- 21.20 6.29 ---
01/31/14 --- --- dry 3.30 ---
07/23/14 --- --- dry dry ---
01/27/15 FIELD FIELD 15.10 3.76 ---
07/29/15 FIELD FIELD dry dry ---
06/23/16 FIELD FIELD dry 9.17 ---
11/02/16 FIELD FIELD dry 23.5 ---
05/31/17 FIELD FIELD dry 15.00 ---
Oxidation Reduction Potential 07/22/09 --- --- dry dry ---
mV 01/26/10 --- --- 212.90 20.0 ---
07/07/10 --- --- dry dry ---
01/05/11 --- --- dry 117.8 ---
07/07/11 --- --- dry 19.2 ---
01/12/12 --- --- 16.30 100.8 ---
07/12/12 --- --- dry 95.0 ---
02/06/13 --- --- dry 37.0 ---
07/09/13 --- --- -0.90 80.4 ---
01/31/14 --- --- dry 86.0 ---
07/23/14 --- --- dry dry ---
01/27/15 FIELD FIELD 114.7 32.0 ---
07/29/15 FIELD FIELD dry dry ---
06/23/16 FIELD FIELD dry 87.6 ---
11/02/16 FIELD FIELD dry -43.3 ---
05/31/17 FIELD FIELD dry 67.10 ---
Dissolved Oxygen 07/22/09 --- --- dry dry ---
mg/l 01/26/10 --- --- 11.50 11.49 ---
07/07/10 --- --- dry dry ---
01/05/11 --- --- dry 10.22 ---
07/07/11 --- --- dry 6.05 ---
01/12/12 --- --- 7.94 7.87 ---
07/12/12 --- --- dry 2.15 ---
02/06/13 --- --- dry 9.12 ---
07/09/13 --- --- 5.0 6.50 ---
01/31/14 --- --- dry 13.98 ---
07/23/14 --- --- dry dry ---
01/27/15 FIELD FIELD 12.90 12.67 ---
07/29/15 FIELD FIELD dry dry ---
06/23/16 FIELD FIELD dry 1.95 ---
11/02/16 FIELD FIELD dry 1.60 ---
05/31/17 FIELD FIELD dry 4.81 ---
Notes:
DL = Method Detection Limit.
SWSL = NC-DENR Solid Waste Section Limit.
NC2B = Surface Water Standard established in 15A NCAC 2B (NC Freshwater Aquatic Life - Little Branch - Class C Waters)
* NC2B Standard is water hardness dependent, refer to Calculator in NC 15A NCAC 02B SW Standards & Protective Values doc.
ND = Not detected above the DL.
J = Estimated concentration below the SWSL.B = Blank qualified data.
dry = Insufficient water flow for sampling. --- = No data.
mg/l = milligrams per liter µg/l = micrograms per liter
S.U. = Standard Units.NTU = Nephelometric Turbidity Units.
µS/cm= microsiemens per centimeter.mV = Millivolts.
Bold = Concentrations above the NC2B Standards.
Blanks = field, trip and/or method blanks.
All data prior to 2012 taken from previous reports by Golder Associates NC, Inc.
Holly Springs Closed C and D Landfill
Permit No. 92-14 6 of 6 Joyce Engineering

Appendix E

Statistical Analyses Worksheets
& Summary Table

APPENDIX E:Statistical Background AnalysesArsenic 100% ND Log-NormalUpper Tolerance Limit - Intrawell (99% confidence level & 99% of population below tolerance limit)85.0 MW-12 26.8 NoNotes:Concentrations are in micrograms per liter (µg/l).NC2L = North Carolina 2L Groundwater Standard.GWPS = Solid Waste Section Groundwater Protect Standard.SSI = Statistically significant increase over background.%ND = Percentage of data that was non-detect (truncated).ConstituentData DistributionStatistical Method used to Establish BackgroundCalculated Background ConcentrationSample Location SSINC2LSample Result (µg/l)Republic Services - Holly Springs LandfillPermit No. 92-14Joyce Engineering
JOYCE Project: Republic Holly Springs
Project No: 895.1701.12
Date: July 10, 2017
Analyte: Arsenic (MW-12 Intrawell)
Quantitation
Concentration Limit
Sample No. Sample Date Location (µg/l) (µg/l)
1 7/22/2009 MW-12 21.4 10.0 8.0 25.0
2 1/26/2010 MW-12 13.5 10.0 10.8 21.4
3 7/7/2010 MW-12 13.0 10.0 11.6 21.3
4 1/5/2011 MW-12 11.6 10.0 13.0 14.6
5 7/7/2011 MW-12 14.0 10.0 13.5 14.0
6 1/12/2012 MW-12 10.8 10.0 14.0 13.5
7 7/12/2012 MW-12 14.6 10.0 14.6 13.0
8 2/6/2013 MW-12 8.0 10.0 21.3 11.6
9 7/9/2013 MW-12 25.0 10.0 21.4 10.8
10 1/31/2014 MW-12 21.3 10.0 25.0 8.0
Number of Data: 10
Number of Truncated Data: 0
Percentage of Truncated Data: 0%
Upper Tolerance Limit: 85.0 µg/l
Notes:
All concentrations in micrograms per liter (µg/l).
B = Blank qualified data - not used in statistical calculations.
ND = Not detected (truncated).
Sorted
Concentration (µg/l)
JEI Project:Republic Holly Springs
Project No: 895.1701.12
Date: July 10, 2017
Shapiro Wilk Test Statistic (W) for normality of total Arsenic (MW-12 Intrawell)
Complete the following table where
i = ordered value of sample, arranged from smallest to largest
X(i) = sample values arranged from smallest to largest
X(n-i+1) = sample values arranged from largest to smallest
A(n-i+1) = coefficient from table A-1, Statistical Analysis of Ground-Water
Data at RCRA Facilities
B(i) = summation of (X(n-i+1)-X(i))A(n-i+1)
i X(i) X(n-i+1) X(n-i+1) - X(i) A(n-i+1) B(i)
1 8.00 25.00 17 0.5739 9.76
2 10.80 21.40 10.6 0.3291 3.49
3 11.60 21.30 9.7 0.2141 2.08
4 13.00 14.60 1.6 0.1224 0.20
5 13.50 14.00 0.5 0.0399 0.02
6 14.00 13.50 -0.5
7 14.60 13.00 -1.6
8 21.30 11.60 -9.7
9 21.40 10.80 -10.6
10 25.00 8.00 -17
The test statistic W can be found using:
W = SQR[B/(SD x SQRT(n-1))]
where: B = summation of (X(n-i+1)-X(i))A(n-i+1) = 15.54
SD = standard deviation of the data group = 5.43
n = number of samples = 10
W = 0.910
Compare this value to the critical value in Table A-2 of Statistical Analysisof Ground-Water
Monitoring Data at RCRA Facilities, Addendum to Interim Final Guidance (Draft)
July, 1992, to determine if the data is normally distributed.
From Table A-2 with (n) samples and a 95% confidence level, the critical value is
W(crit) = 0.842
and the calculated W = 0.910
Therefore the data set is Normal
JEI Project:Republic Holly Springs
Project No: 895.1701.12
Date: July 10, 2017
Shapiro Wilk Test Statistic (W) for normality of total Arsenic (MW-12 Intrawell)
Complete the following table where
i = ordered value of sample, arranged from smallest to largest
X(i) = sample values arranged from smallest to largest
X(n-i+1) = sample values arranged from largest to smallest
A(n-i+1) = coefficient from table A-1, Statistical Analysis of Ground-Water
Data at RCRA Facilities
B(i) = summation of (X(n-i+1)-X(i))A(n-i+1)
i X(i) X(n-i+1) X(n-i+1) - X(i) A(n-i+1) B(i)
1 2.08 3.22 1.139434283 0.5739 0.65
2 2.38 3.06 0.683844788 0.3291 0.23
3 2.45 3.06 0.607701975 0.2141 0.13
4 2.56 2.68 0.116072171 0.1224 0.01
5 2.60 2.64 0.036367644 0.0399 0.00
6 2.64 2.60 -0.03636764
7 2.68 2.56 -0.11607217
8 3.06 2.45 -0.60770197
9 3.06 2.38 -0.68384479
10 3.22 2.08 -1.13943428
The test statistic W can be found using:
W = SQR[B/(SD x SQRT(n-1))]
where: B = summation of (X(n-i+1)-X(i))A(n-i+1) = 1.02
SD = standard deviation of the data group = 0.35
n = number of samples = 10
W = 0.951
Compare this value to the critical value in Table A-2 of Statistical Analysisof Ground-Water
Monitoring Data at RCRA Facilities, Addendum to Interim Final Guidance (Draft)
July, 1992, to determine if the data is normally distributed.
From Table A-2 with (n) samples and a 95% confidence level, the critical value is
W(crit) = 0.842
and the calculated W = 0.951
Therefore the data set is Log-Normal
JEI Project:Republic Holly Springs
Project No: 895.1701.12
Date: July 10, 2017
Probability Plots to determine the distribution of Arsenic (MW-12 Intrawell)
Complete the following table where
i = ordered value of sample, arranged from smallest to largest
X(i) = sample values arranged from smallest to largest
LN[X(i)] = Natural Log Value of sample concentrations arranged from
smallest to largest
[i/(n+1)] = Cumulative probability
n = number of samples = 10
X(i) LN[X(i)] i Rank [Rank/(n+1)]Quantiles
8 2.08 1 1 0.091 -1.34
10.8 2.38 2 2 0.182 -0.91
11.6 2.45 3 3 0.273 -0.60
13 2.56 4 4 0.364 -0.35
13.5 2.60 5 5 0.455 -0.11
14 2.64 6 6 0.545 0.11
14.6 2.68 7 7 0.636 0.35
21.3 3.06 8 8 0.727 0.60
21.4 3.06 9 9 0.818 0.91
25 3.22 10 10 0.909 1.34
Plot analysis indicates that the data more closely follow a normal distribution in the
log-transformed format.
JEI Project:Republic Holly Springs
Project No: 895.1701.12
Date: July 10, 2017
Probability Plots to determine the distribution of Arsenic (MW-12 Intrawell)
R² = 0.9134
-2.00
-1.50
-1.00
-0.50
0.00
0.50
1.00
1.50
2.00
0 5 10 15 20 25 30Quantile
Concentration (micrograms per liter)
Normal Probability Plot
Arsenic Concentrations
R² = 0.9292
-2.00
-1.50
-1.00
-0.50
0.00
0.50
1.00
1.50
0.00 0.50 1.00 1.50 2.00 2.50 3.00 3.50Quantile
Ln [Concentration (micrograms per liter)]
Log Normal Probability Plot
Arsenic Concentrations
JEI Project:Republic Holly Springs
Project No: 895.1701.12
Date: July 10, 2017
Determination of reported background value as an outlier
Analyte:Arsenic (MW-12 Intrawell)
Background Data Quantitation
ln(Concentration) Limit
Sample No. Sample Date Location (µg/l) (µg/l)
1 07/22/09 MW-12 3.063 10
2 01/26/10 MW-12 2.603 10
3 07/07/10 MW-12 2.565 10
4 01/05/11 MW-12 2.451 10
5 07/07/11 MW-12 2.639 10
6 01/12/12 MW-12 2.380 10
7 07/12/12 MW-12 2.681 10
8 02/06/13 MW-12 2.079 10
9 07/09/13 MW-12 3.219 10
10 01/31/14 MW-12 3.059 10
mean = 2.674
STD = 0.350
Note: All concentrations are micrograms per liter
Using the data listed above, form the statisitc Tn:
Tn = (Xn - mean) / STD
where: Xn = largest observed sample value
mean = mean of the background values
STD = standard deviation of the background values
For Xn = 3.219
mean = 2.674
STD = 0.350
Tn = 1.556
From Table 8 included in the Staistical Analysis of Groundwater Monitoring Data at
RCRA Facilities - Interim Final Guidance, the critical value for the given sample group is
Number of samples = 10
Tc = 2.176
Since Tc>Tn, the sample result is not considered to be an outlier
JEI Project:Republic Holly Springs
Project No: 895.1701.12
Date: July 10, 2017
Parametric Tolerance Interval for normally distributed data
Analyte:Arsenic (MW-12 Intrawell)
Background Data Nat Log Quantitation
Concentration Limit
Sample No. Sample Date Location (µg/l) (µg/l)
1 07/22/09 MW-12 3.06 10
2 01/26/10 MW-12 2.60 10
3 07/07/10 MW-12 2.56 10
4 01/05/11 MW-12 2.45 10
5 07/07/11 MW-12 2.64 10
6 01/12/12 MW-12 2.38 10
7 07/12/12 MW-12 2.68 10
8 02/06/13 MW-12 2.08 10
9 07/09/13 MW-12 3.22 10
10 01/31/14 MW-12 3.06 10
Note: All sample concentrations are micrograms per liter
Using the background data, the upper Tolerance Limit can be determined using:
Upper Tolerance Limit = (Mean Concentration) + K x (Standard Deviation Samples)
where: Mean Conc = mean concentration background samples
K = factor for constructing one sided normal tolerance limit
taken from table 4-2, page 87, Statistical Methods for Groundwater
Monitoring, Gibbons, 1994 99% Confidence Limit
& 99% below tolerance limit.
n = number of background samples
STDS = Standard Deviation Samples
For: n = 10
K = 5.047
Mean Conc = 2.67
STDS = 0.35
UTL = 85.0 µg/l