9701_WilkesCounty_MSWLF_WQMR_20170419

2211 W. Meadowview Road, Suite 101 Greensboro, NC 27407
tel: [phone] fax: [phone] www.JoyceEngineering.com February 20, 2018
Ms. Christine Ritter Compliance Hydrogeologist Division of Waste Management/Solid Waste Section 1646 Mail Service Center Raleigh, NC 27699-1646

RE: Second Semiannual Water Quality Monitoring Reports of 2017 Wilkes County Landfills: Germantown Landfill, Permit No. 97-01 Project No. 2180180, Task No. 05
Dear Christine: On behalf of Wilkes County, Joyce Engineering is submitting the Second Semiannual Water Quality Monitoring Report of 2017 for the Wilkes County Germantown Landfill, Permit No. 97-01. The attached report contains electronic versions of the complete report and all appendices for the
October 2017 sampling event. Also attached is the North Carolina Environmental Monitoring Reporting Form for the October 2017 monitoring event. If you wish to have a hard copy of the report, drawings, or appendices, we will be happy to provide it upon your request. Please feel free to contact me or Rochelle Mesubed at [phone] if you
have any questions regarding this report.
Sincerely, JOYCE ENGINEERING
Hannu Kemppinen P.G. Senior Project Consultant Enclosures
C: Kent Brandon - Wilkes County, Solid Waste Director (2 copies)

PREPARED FOR:
WILKES COUNTY DEPARTMENT OF SOLID WASTE
9219 ELKIN HIGHWAY ROARING RIVER, NORTH CAROLINA 27298
GERMANTOWN LANDFILL PERMIT NO. 97-01
SECOND SEMIANNUAL
WATER QUALITY MONITORING REPORT OF 2017

FEBRUARY 2018
PREPARED BY:

2211 WEST MEADOWVIEW ROAD, SUITE 101 GREENSBORO, NORTH CAROLINA 27407 NC LICENSE NUMBER C-0782 PHONE: [phone] FAX: [phone] PROJECT NO. 2180180.05

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Second Semiannual Water Quality Monitoring Report of 2017 Joyce Engineering Germantown Landfill, Permit No. 97-01 February 2018
i

Second Semiannual Water Quality Monitoring Report of 2017 Germantown Landfill
Wilkes County, North Carolina
TABLE OF CONTENTS
1.0 INTRODUCTION.................................................................................................................1
1.1 Site Information ......................................................................................................................1
1.2 Site Geology............................................................................................................................1
1.3 Regulatory Status ....................................................................................................................1
2.0 FACILITY MONITORING PROGRAM ..........................................................................1
2.1 Groundwater Monitoring Program .........................................................................................1
2.2 Surface Water Monitoring Program ........................................................................................2
3.0 SECOND SEMIANNUAL SAMPLING EVENT OF 2017 ...............................................2
3.1 Field Work and Visual Inspection ..........................................................................................2
3.2 Laboratory Analysis and JOYCE Quality Control .................................................................3
4.0 HYDROGEOLOGIC CONDITIONS.................................................................................4
5.0 DATA ANALYSIS ................................................................................................................4
5.1 Groundwater Data Analysis and Comparisons to Standards ..................................................4
5.2 Surface Water Data Analysis and Comparisons to Standards ................................................5
6.0 CONCLUSION .....................................................................................................................5
7.0 REFERENCES ......................................................................................................................6

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Second Semiannual Water Quality Monitoring Report of 2017 Joyce Engineering Germantown Landfill, Permit No. 97-01 February 2018
ii

Second Semiannual Water Quality Monitoring Report of 2017 Germantown Landfill
Wilkes County, North Carolina
TABLE OF CONTENTS CONTINUED
Tables
Table 1 Summary of Groundwater Elevations
Table 2 Summary of New Detections and Exceedances
Table 3 Summary of Field Parameters
Table 4 Horizontal Groundwater Flow Velocities
Figure
Figure 1 Site Location Map
Drawing
Drawing 1 Groundwater Surface Map
Appendices
Appendix 1 Laboratory Analytical Reports and Field Data Logs
Appendix 2 Historical Groundwater Elevations
Appendix 3 Historically Detected Constituents

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Second Semiannual Water Quality Monitoring Report of 2017 Joyce Engineering Germantown Landfill, Permit No. 97-01 February 2018 1
1.0 INTRODUCTION
1.1 Site Information
The Germantown Landfill is a closed, unlined municipal solid waste (MSW) landfill owned by Wilkes County. The landfill property is located near the town of Wilkesboro, North Carolina. The property boundary is indicated on an excerpt from the 7.5 minutes USGS topographic map
for Moravian Falls, North Carolina (Figure 1).
The closed landfill currently houses the Wilkes County Fire Marshal and training grounds. The area surrounding the landfill is primarily residential/agricultural and contains open fields and woodlands.
1.2 Site Geology
The Germantown Landfill is located at the boundary of the Inner Piedmont Belt and Blue Ridge
Belt in the Brevard Fault Zone. In the vicinity of the site, the Brevard Zone is a five-mile wide, east-northeast trending fault zone with a complex structural and metamorphic history. Finely interlayered gneiss and schist within the zone are amphibolite facies, with peak metamorphism as high as the kyanite zone for pelitic assemblages.
1.3 Regulatory Status
Wilkes County is currently monitoring groundwater at the Germantown Landfill in accordance with criteria set forth in Rule .0500 of the North Carolina Solid Waste Management Rules (NCSWMR) for municipal solid waste landfills (MSWLF) closed prior to October 9, 1993.
2.0 FACILITY MONITORING PROGRAM
2.1 Groundwater Monitoring Program
The current groundwater compliance monitoring network includes five monitoring wells, including one upgradient well and four downgradient wells. These wells are summarized below, along with their current monitoring program status.

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Second Semiannual Water Quality Monitoring Report of 2017 Joyce Engineering Germantown Landfill, Permit No. 97-01 February 2018 2
TOC = Top of casing.
The approximate locations for the wells are shown in Drawing 1. Groundwater samples are
collected semiannually during the second and fourth quarters. Samples are analyzed for all constituents listed in the NCSWMR Appendix I (NC Appendix I) during the first and second semiannual events.
2.2 Surface Water Monitoring Program
Surface water at the Germantown Landfill is monitored semiannually in accordance with
NCSWMR §0602 and in conjunction with the groundwater sampling events. Samples are collected from three surface water monitoring points (Upstream, Downstream and Outfall #1).
Surface water samples are collected and analyzed for the NC Appendix I list of constituents during both semiannual monitoring events. The results are compared to the 15A NCAC 2B (NC
2B) Surface Water Standards in a value-to-value comparison. These surface water monitoring
points are summarized below, along with their current monitoring program status.
Surface Point Classification Monitoring Program
Upstream Up Stream/Compliance Surface Water
Downstream Compliance Surface Water
Outfall #1 Compliance Surface Water
3.0 SECOND SEMIANNUAL SAMPLING EVENT OF 2017
3.1 Field Work and Visual Inspection
On October 19, 2017, Joyce Engineering (JOYCE) personnel purged and sampled facility monitoring wells MW-1, MW-2, MW-3, MW-4 and MW-5. Prior to purging, the depth to static water level was measured for all monitoring wells with an electronic water level indicator, accurate to 0.01 foot. Surface monitoring points (Upstream, Downstream and Outfall #1) were
also sampled during the October 2017 monitoring event. The approximate locations for the monitoring wells and surface points are shown in Drawing 1.
During sampling, the monitoring wells were purged and sampled using either disposable bailers or a 12 volt plastic pump. Measurements of temperature, pH, specific conductivity, and turbidity were recorded in the site specific log book prior to purging, after each purge volume, and during
Monitoring Well Classification Monitoring Program Total Depth from TOC (ft)
MW-1 Background Detection (.0500) 89.69 MW-2 Compliance Detection (.0500) 81.54 MW-3 Compliance Detection (.0500) 64.00 MW-4 Compliance Detection (.0500) 28.21 MW-5 Compliance Detection (.0500) 23.47

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Second Semiannual Water Quality Monitoring Report of 2017 Joyce Engineering Germantown Landfill, Permit No. 97-01 February 2018 3
sampling (Appendix 1). Prior to sampling, laboratory-supplied containers were prepared with
the following information:
• Monitoring well number (completed by field personnel),
• Date and time of sample collection (completed by field personnel),
• Initials of sampling personnel (completed by field personnel),
• Project name and number (completed by the laboratory),
• Chemical preservative (completed by the laboratory); and
• Requested chemical analysis (completed by the laboratory).
Groundwater samples from each monitoring well were collected directly from the disposable bailers or 12 volt pump in the provided laboratory containers within 24 hours of the final purge volume. Immediately after collection, the samples were placed in a laboratory provided cooler
and chilled on ice.
Surface water samples were collected directly from stream flow by lowering the prepared sample containers into the stream flow with the opening facing into the current. There was no running water from Outfall #1 therefore; Outfall #1 was not sampled. Care was taken not to overfill the sample containers (which could lead to preservative loss) and to avoid sampling-induced
turbidity. At the time of sampling, surface water was also measured for temperature, pH, specific conductivity, and turbidity. After sample collection, the samples were placed in a laboratory provided cooler and chilled on ice. Field data logs are provided in the Appendix 1.
A visual inspection program has been implemented at the Germantown Landfill in order to detect potential releases of leachate and/or landfill gas migration in a timely manner. This inspection
program involves field personnel making the following observations:
• Observation of stress induced on the biological community (i.e., dead or dying vegetation),
• Indications of leachate impact (i.e., seeps, impacted surface water),
• Observations of erosion; and
• Negative changes around the waste facility.
3.2 Laboratory Analysis and JOYCE Quality Control
The October 2017 groundwater and surface water samples were submitted to Pace Analytical Laboratories, Inc. of Huntersville, North Carolina under chain-of-custody control for analysis. As presented earlier, the groundwater and surface water samples were analyzed for the NC Appendix I constituents. JOYCE requested a Level II data report for the final laboratory report. The samples were received by the laboratory on October 20, 2017, in good condition, properly
preserved temperature, and within analysis hold times.

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Second Semiannual Water Quality Monitoring Report of 2017 Joyce Engineering Germantown Landfill, Permit No. 97-01 February 2018 4
In addition to samples collected for compliance monitoring at the Germantown Landfill, a Field
Blank was collected by JOYCE personnel to be analyzed for NC Appendix I constituents. Also, a Trip Blank was prepared by the laboratory to accompany the volatile sampling containers during shipment to and from the laboratory. The October 2017 Field Blank was analyzed for the NC Appendix I volatile organics only.
Upon receipt of the laboratory data package, the data was reviewed by JOYCE personnel for the
following:
• General typographical errors,
• Correct analyses performed and within method specified hold times,
• Biased data results based on Surrogate Recoveries, Matrix Spike, Matrix Spike Duplicate, and Laboratory Control Samples,
• Blank qualified data (B-flags),
• Detections above the groundwater and surface water standards; and
• Detections that are above historical levels.
4.0 HYDROGEOLOGICAL CONDITIONS
Depth to groundwater was measured in the compliance monitoring wells at the site prior to
sampling. The groundwater elevations were calculated relative to the surveyed measuring point (top of casing) for each monitoring well. The groundwater elevations are summarized in Table 1.
The potentiometric surface contours shown in Drawing 1 are based on data from the October 2017 sampling event. Estimated horizontal groundwater gradients from the October 2017
groundwater elevations are presented in Table 4. The horizontal gradients calculated for the facility from these data ranged from 0.0332 to 0.1354 ft/ft.
Linear groundwater flow velocities for wells screened in saprolite were computed using the following modified Darcy equation:
V = Ki/n
where
V = average linear velocity (feet per day – ft/day),
K = hydraulic conductivity (ft/day), i = horizontal hydraulic gradient, and ne = effective porosity.
A hydraulic conductivity (K) of 5.50 E -01 ft/day based on results from slug testing and an
estimated effective porosity of 16% based on soils typical of this region were used to estimate average linear groundwater flow velocities for the site. The calculated flow velocities are

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Second Semiannual Water Quality Monitoring Report of 2017 Joyce Engineering Germantown Landfill, Permit No. 97-01 February 2018 5
summarized in Table 4. The estimated linear groundwater flow velocity under the waste
management unit ranges from 0.114 ft/day to 0.465 ft/day.
The linear velocity equation and resulting rates make the simplified assumptions of a homogeneous and isotropic aquifer; however, soils common in this terrain are characteristically heterogeneous. Site boring logs record that soils sampled at the site commonly exhibits relict
foliation. These structures can result in locally anisotropic groundwater flow.
5.0 DATA ANALYSIS
The results from the October 2017 sampling event were received on November 8, 2017 from Pace Analytical Laboratories, Inc. (Appendix 1).
5.1 Groundwater Data Analysis and Comparisons to Standards
The following inorganic and organic constituents were detected at quantified concentrations in
groundwater during the October 2017 sampling event. All concentrations are reported in micrograms per liter (µg/L). Concentrations with a “J” are considered to be estimated. Concentrations with a “B” are attributed to lab or field contamination.
Constituent NC2L/ (GWPS)
SWSL Background Downgradient Blanks MW-1 MW-2 MW-3 MW-4 MW-5
Barium 700 100 115 10.9 J 10.2 J 93.5 J 442 ND
Cobalt (1) 10 ND ND ND 13.5 14.1 ND
Vanadium 0.3 25 ND ND ND 4.1 J 4.4 J ND
Zinc 1000 10 5.7 J 13.2 ND ND 7.4 J ND Benzene 1 1 ND ND ND ND 1.0 ND Chlorobenzene 50 3 0.3 J ND ND 5.1 9.6 ND 1,4-Dichlorobenzene 6 1 0.4 J ND ND 2.4 4.0 ND
ND= Not Detected
In general, the organic and inorganic results are consistent with historical data. Historical
groundwater data can be found in Appendix 1.
5.2 Surface Water Data Analysis and Comparisons to Standards
No inorganic and organic constituents were detected at quantified concentrations in surface water during the October 2017 sampling event. In general, the results are consistent with historical data. Historical surface water data can be found in Appendix I.

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Second Semiannual Water Quality Monitoring Report of 2017 Joyce Engineering Germantown Landfill, Permit No. 97-01 February 2018 6
6.0 CONCLUSION
Based on historical data, inorganic and organic constituents detected above the NC SWSL in groundwater and surface water samples collected during the October 2017 sampling event are generally consistent with previous events. The Germantown Landfill will remain in Detection Monitoring under Rule .0500 of the NCSWMR and the next semiannual sampling event is
tentatively scheduled for the April 2018.
7.0 REFERENCES
Brown, Philip M., Chief Geologist, 1985, Geologic Map of North Carolina, The North Carolina Geologic Survey, scale 1:500,000.
Fetter, C.W., 2001, Applied Hydrogeology, Fourth Edition: Prentice-Hall, Inc..
Johnson, A.I., 1967, Specific Yield - Compilation of Specific Yields For Various Materials: U.S.
Geological Survey Water Supply Paper 1662-D.
North Carolina Department of Environment and Natural Resources, 1990-2011, Solid Waste Management Regulations.
USEPA, 1986, RCRA Ground Water Monitoring Technical Enforcement Guidance Document
(TEGD).
USEPA, 1992, Statistical Analysis of Groundwater Monitoring Data at RCRA Facilities,
Addendum to Interim Final Guidance, Chapter 2, July.

Tables
Table 1 Summary of Groundwater Elevations
Table 2 Summary of New Detections and Exceedances
Table 3 Summary of Field Parameters
Table 4 Horizontal Groundwater Flow Velocities

Table 1
Summary of Groundwater Elevations
TABLE 1: Groundwater Elevations
from to
MW-1 1233.00 58.05 --89.69 1174.95
MW-2 1177.85 48.20 --81.54 1129.65
MW-3 1059.00 44.40 --64.00 1014.60
MW-4 1018.00 14.20 --28.21 1003.80
MW-5 1045.75 9.55 --23.47 1036.20
Notes
ft = feet
Groundwater
Elevation
ftmsl
ftmsl = feet mean sea level
Location
TOC
Elevation
ftmsl
Depth to
Groundwater ft
SCREENED INTERVAL
DEPTH B.G.S.
WELL
DEPTH
ft

Table 2
Summary of New Detections and Exceedances
TABLE 2: Summary of Detections
Wilkes Co. Germantown Landfill
Permit 97-01 Joyce Engineering
WELL ID PARAMETER RESULT UNITS NC SWSL NC 2L GWPS DATE
9701-MW1 Barium 115.0 µg/L 100 700 -10/19/2017
9701-MW2 Zinc 13.2 µg/L 10 1000 -10/19/2017
9701-MW4 Cobalt 13.5 µg/L 10 -1 10/19/2017
9701-MW4 Vanadium 4.1 µg/L 25 -0.3 10/19/2017
9701-MW4 1,4-Dichlorobenzene 2.4 µg/L 1 6 -10/19/2017
9701-MW4 Chlorobenzene 5.1 µg/L 3 50 -10/19/2017
9701-MW5 Barium 442 µg/L 100 700 -10/19/2017
9701-MW5 Cobalt 14.1 µg/L 10 -1 10/19/2017
9701-MW5 Vanadium 4.4 µg/L 25 -0.3 10/19/2017
9701-MW5 Benzene 1.0 µg/L 1 1 -10/19/2017
9701-MW5 1,4-Dichlorobenzene 4.0 µg/L 1 6 -10/19/2017
9701-MW5 Chlorobenzene 9.6 µg/L 3 50 -10/19/2017
NOTES:All Results in micorgrams per liter (µg/L)
SWSL = NC Soild Waste Section Reporting Limit
BOLD = Exceedance
TABLE 2: Summary of Exceedances
Wilkes Co. Germantown Landfill
Permit No. 97-01 Joyce Engineering
WELL ID PARAMETER RESULT UNITS SWSL C2L/*GWPS/(NC2 GPS DATE
9701-MW4 Cobalt 13.5 µg/L 10 1*1 10/19/2017
9701-MW5 Cobalt 14.1 µg/L 10 1*1 10/19/2017
9701-MW5 Benzene 1.0 µg/L 1 1 1 10/19/2017
NOTES:All Results in micorgrams per liter (µg/L)
SWSL = NC Soild Waste Section Reporting Limit
NC2L = NC Groundwater Standard from 15A NCAC 2L.0202
*GWPS = NC Solid Waste Section Groundwater Protection Standard (for constituents with no NC2L)
GPS = Groundwater Protection Standard as defined by 15A NCAC 13B.1634(g)

Table 3
Summary of Field Parameters
TABLE 3
Summary of Field Parameters
Wilkes Co. Germantown Landfill
Permit No. 97-01 Joyce Engineering
WELL ID PARAMETER RESULT UNITS COLLECT DATE
9701-MW1 pH 5.80 S.U.10/19/2017
9701-MW1 Temperature 17.1 C˚10/19/2017
9701-MW1 Conductivity 142 µS/cm 10/19/2017
9701-MW1 Turbidity 4.77 NTU 10/19/2017
9701-MW1 Static Water Level 58.05 ft 10/19/2017
9701-MW1 Well Depth 89.69 ft 10/19/2017
9701-MW2 pH 7.04 S.U.10/19/2017
9701-MW2 Temperature 15.9 C˚10/19/2017
9701-MW2 Conductivity 190 µS/cm 10/19/2017
9701-MW2 Turbidity 5.04 NTU 10/19/2017
9701-MW2 Static Water Level 48.20 ft 10/19/2017
9701-MW2 Well Depth 81.54 ft 10/19/2017
9701-MW3 pH 5.71 S.U.10/19/2017
9701-MW3 Temperature 16.0 C˚10/19/2017
9701-MW3 Conductivity 56 µS/cm 10/19/2017
9701-MW3 Turbidity 6.45 NTU 10/19/2017
9701-MW3 Static Water Level 44.40 ft 10/19/2017
9701-MW3 Well Depth 64.00 ft 10/19/2017
TABLE 3
Summary of Field Parameters
Wilkes Co. Germantown Landfill
Permit No. 97-01 Joyce Engineering
WELL ID PARAMETER RESULT UNITS COLLECT DATE
9701-MW4 pH 6.28 S.U.10/19/2017
9701-MW4 Temperature 15.4 C˚10/19/2017
9701-MW4 Conductivity 639 µS/cm 10/19/2017
9701-MW4 Turbidity 10.0 NTU 10/19/2017
9701-MW4 Static Water Level 14.2 ft 10/19/2017
9701-MW4 Well Depth 28.21 ft 10/19/2017
9701-MW5 pH 6.32 S.U.10/19/2017
9701-MW5 Temperature 17.0 C˚10/19/2017
9701-MW5 Conductivity 1510 µS/cm 10/19/2017
9701-MW5 Turbidity 12.17 NTU 10/19/2017
9701-MW5 Static Water Level 9.55 ft 10/19/2017
9701-MW5 Well Depth 23.47 ft 10/19/2017
9701-Upstream pH 7.4 S.U.10/19/2017
9701-Upstream Temperature 15.7 C˚10/19/2017
9701-Upstream Conductivity 76 µS/cm 10/19/2017
9701-Upstream Turbidity 9.9 NTU 10/19/2017
9701-Downstream pH 7.46 S.U.10/19/2017
9701-Downstream Temperature 15.6 C˚10/19/2017
9701-Downstream Conductivity 75 µS/cm 10/19/2017
9701-Downstream Turbidity 6.51 NTU 10/19/2017
NOTES:C˚= degrees Centigrade
S.U.= Standard Units
µS/cm = microsemens per centimeter
NTU = Nephelometric Turbidity Units
ft =Feet

Table 4
Horizontal Groundwater Flow Velocities
TABLE 4: Horizontal Groundwater Flow Velocities
Wilkes County Germantown Landfill
Permit # 97-01 Joyce Engineering
Date of Water Table Measurements: October 17, 2017
SEGMENT HORIZ.HYDRAULIC EFFECTIVE LINEAR
FLOW BEGIN & END GRADIENT CONDUCTIVITY POROSITY VELOCITY
DIRECTION GW ELEVATION i K n e V
(feet-AMSL)(ft/ft) (ft/day)(ft/year)
1,160
1,140
1,140
1,010
1,160
1,010
Average 0.0893 Average 0.307
Notes:
Linear flow velocity: V = Ki/n e (modified Darcy equation).
Hydraulic conductivity (K ) is based on slug test from Wilkes County Roaring River Landfill.
Effective porosity (n e ) is based on data for the Wilkes County Roaring River Landfill.
Refer to Drawing 1 for flow line segments.
0.16
i 2 1309 E 0.0993 0.165.50E-01
0.1145.50E-01
0.4655.50E-01
FLOW LINE
SEGMENT
SEGMENT
LENGTH
(feet)
i 3 1108 E 0.1354
0.341
i 1 602 S 0.0332 0.16

Figure 1
Site Location Map

Drawing 1
Groundwater Surface Map
1
2
2
01210
120
0
1200
1190
118
0
1190
1180
1170
1160
1050125012201
2
3
0
12
4
012101200
11601170118011901160
1150
1140
1130
1120
1110
108010901100111011201130114011501100 1090 1080
1070
1060
1050
1040
1030
1020
1070
1060
105010401030101
0
1010
101
0 114011501
1
4
0
1
1
4
0
115011201140 1
130
1
1
2
010801070
1060
1130
10601070108010901100111011201120113010301
0
4
0
1
0
5
010601
0
7
0
1
0
8
0
10
9
0
1
1
0
011101
1
2
0
11
3
0
1
1
4
01110
1010
10
1
0 1150CLOSED
LANDFILL
EXIST. GAS VENT (TYP.)
GV
GV
GV GV
GV
GV
EXISTING
FIREFIGHTER
TRAINING
FACILITY
APPROX. LOCATION OF
EDGE OF CAP
EMERGENCY/
DISASTER
DEBRIS
PROCESSING
AREA (2 ACRES)
(NOT MONITORED)
GP-2
GP-1
EXISTING
POLE BARN
EXISTING
GARAGE
EXISTING
OFFICES
APPROXIMATE LOCATION OF
PROPERTY LINE
MORAVIAN CREEK
MORAVIAN CREEK
GP-4
GW-2
GW-4
GW-3
GW-1
GREENHOUSE
SEDIMENT BASIN
LEGEND
EDGE OF LINER
PAVED ROAD
EXISTING 2 FT CONTOUR
EXISTING 10 FT CONTOUR
GRAVEL ROAD
GROUNDWATER MONITORING WELL LOCATION,
IDENTIFICATION, AND GROUNDWATER ELEVATION
POINT IN TIME GROUNDWATER CONTOUR
(APPROXIMATE) 1 FT. CONTOUR INTERVAL
GROUNDWATER FLOW PATHWAY USED TO
CALCULATE HYDRAULIC GRADIENT
i 1SEGMENT USED FOR GRADIENT CALCULATION
MW-3
1014.60
1.STATIC WATER LEVELS MEASURED ON OCTOBER 17, 2017.
2.GROUNDWATER CONTOURS BASED ON LINEAR INTERPOLATION BETWEEN AND EXTRAPOLATION FROM KNOWN DATA,
TOPOGRAPHIC CONTOURS, AND KNOWN FIELD CONDITIONS. THEREFORE, GROUNDWATER CONTOURS MUST BE ASSUMED TO
BE APPROXIMATE.
3.GROUNDWATER ELEVATIONS ARE MEASURED IN FEET AND REFERENCED TO MEAN SEA LEVEL.
1140
NOT MONITORED NM
SEGMENT LENGTH
i1
i2
= 602 LF
= 1,309 LF
= 1,108 LF 119011801
1
7
0
116
0
MW-1
1174.95
MW-2
1129.65
MW-3
1014.60
MW-4
1003.80
MW-5
1036.20
1040
1060
1080
1100
1140
1160
1160
1060i1
i2
i 3
i3
PROPERTY LINE
STREAM
1120
11
4
0
1020
1010
101
010201040 114011
2
01140
1100
108
0
PROJECT NO.APPROVEDCHECKEDDRAWNDESIGNEDDATEDATEREVISIONS AND RECORD OF ISSUEBYNOAPPCKSCALE All rights reserved.Ó Joyce Engineering, Inc.DRAWING NO.L:\Wilkes\GERMANTOWN\dwg\GW MAPS\GW MAP OCTOBER 2017.dwg Layout=Layout12211 W. MEADOWVIEW ROADGREENSBORO, NC 27407PHONE: [phone]NC CORP LIC: C-0782356GERMANTOWN LANDFILLWILKES COUNTY, NORTH CAROLINA20171
AS SHOWNGROUNDWATER CONTOUR MAPOCTOBER 17. 2017RMRWHRMVB11/6/170
(FEET)
GRAPHIC SCALE
20010050

Appendices
Appendix 1 Laboratory Analytical Reports and Field Data Logs
Appendix 2 Historical Groundwater Elevations
Appendix 3 Historical Detected Constituents

Appendix 1
Laboratory Analytical Reports and Field Data Logs
#=CL#
November 08, 2017
LIMS USE: FR - VAN BURBACH
LIMS OBJECT ID: 92360016
92360016
Project:
Pace Project No.:
RE:
Mr. Van Burbach
Joyce Engineering-NC
2211 W. Meadowview Road
Suite 101
Greensboro, NC 27407
WILKES-GERMANTOWN 356180112
Dear Mr. Burbach:
Enclosed are the analytical results for sample(s) received by the laboratory on October 20, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
[phone]
Enclosures
cc:Gretta Eller, Joyce Engineering
Mr. Daniel Girdner, Joyce Engineering-Greensboro
Haley Seaton, Joyce Engineering
Miguel Vazquez, Joyce Engineering
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 42
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 42
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Lab ID Sample ID Matrix Date Collected Date Received
92360016001 9701-TRIP BLANK Water 10/19/17 08:00 10/20/17 10:41
92360016002 9701-DOWNSTREAM Water 10/19/17 15:40 10/20/17 10:41
92360016003 9701-FIELD BLANK Water 10/19/17 17:00 10/20/17 10:41
92360016004 9701-MW1 Water 10/19/17 13:58 10/20/17 10:41
92360016005 9701-MW2 Water 10/19/17 16:42 10/20/17 10:41
92360016006 9701-MW3 Water 10/19/17 15:24 10/20/17 10:41
92360016007 9701-MW4 Water 10/19/17 15:50 10/20/17 10:41
92360016008 9701-MW5 Water 10/19/17 16:55 10/20/17 10:41
92360016009 9701-UPSTREAM Water 10/19/17 15:50 10/20/17 10:41
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
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[phone]
Page 3 of 42
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92360016001 9701-TRIP BLANK EPA 8260 50 PASI-CGAW
92360016002 9701-DOWNSTREAM EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92360016003 9701-FIELD BLANK EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92360016004 9701-MW1 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92360016005 9701-MW2 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92360016006 9701-MW3 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92360016007 9701-MW4 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92360016008 9701-MW5 EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
92360016009 9701-UPSTREAM EPA 6010 14 PASI-ASH1
EPA 6020B 1 PASI-ACDF
EPA 8260 50 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 42
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92360016002 9701-DOWNSTREAM
Barium 22.7J ug/L 10/31/17 15:53100EPA 6010
92360016003 9701-FIELD BLANK
Selenium 5.5J ug/L 10/31/17 15:5610.0EPA 6010
92360016004 9701-MW1
Barium 115 ug/L 10/31/17 15:59100EPA 6010
Zinc 5.7J ug/L 10/31/17 15:5910.0EPA 6010
Chlorobenzene 0.30J ug/L 10/22/17 21:213.0EPA 8260
Chloromethane 0.27J ug/L 10/22/17 21:211.0EPA 8260
1,4-Dichlorobenzene 0.40J ug/L 10/22/17 21:211.0EPA 8260
92360016005 9701-MW2
Barium 10.9J ug/L 10/31/17 16:03100EPA 6010
Selenium 9.7J ug/L 10/31/17 16:0310.0EPA 6010
Zinc 13.2 ug/L 10/31/17 16:0310.0EPA 6010
Thallium 0.071J ug/L 11/08/17 00:075.5EPA 6020B
Chloromethane 0.29J ug/L 10/22/17 21:381.0EPA 8260
92360016006 9701-MW3
Barium 10.2J ug/L 10/31/17 16:06100EPA 6010
92360016007 9701-MW4
Barium 93.5J ug/L 10/31/17 16:09100EPA 6010
Cobalt 13.5 ug/L 10/31/17 16:0910.0EPA 6010
Copper 9.6J ug/L 10/31/17 16:0910.0EPA 6010
Lead 2.6J ug/L 10/31/17 16:0910.0EPA 6010
Nickel 4.6J ug/L 10/31/17 16:0950.0EPA 6010
Vanadium 4.1J ug/L 10/31/17 16:0925.0EPA 6010
Thallium 0.025J ug/L 11/08/17 00:125.5EPA 6020B
Chlorobenzene 5.1 ug/L 10/22/17 22:133.0EPA 8260
Chloromethane 0.25J ug/L 10/22/17 22:131.0EPA 8260
1,4-Dichlorobenzene 2.4 ug/L 10/22/17 22:131.0EPA 8260
92360016008 9701-MW5
Barium 442 ug/L 10/31/17 16:12100EPA 6010
Cobalt 14.1 ug/L 10/31/17 16:1210.0EPA 6010
Copper 3.3J ug/L 10/31/17 16:1210.0EPA 6010
Lead 4.8J ug/L 10/31/17 16:1210.0EPA 6010
Nickel 9.9J ug/L 10/31/17 16:1250.0EPA 6010
Vanadium 4.4J ug/L 10/31/17 16:1225.0EPA 6010
Zinc 7.4J ug/L 10/31/17 16:1210.0EPA 6010
Thallium 0.040J ug/L 11/08/17 00:195.5EPA 6020B
Benzene 1.0 ug/L 10/22/17 22:301.0EPA 8260
Chlorobenzene 9.6 ug/L 10/22/17 22:303.0EPA 8260
Chloromethane 0.20J ug/L 10/22/17 22:301.0EPA 8260
1,4-Dichlorobenzene 4.0 ug/L 10/22/17 22:301.0EPA 8260
92360016009 9701-UPSTREAM
Barium 22.7J ug/L 10/31/17 16:15100EPA 6010
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 42
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92360016009 9701-UPSTREAM
Selenium 7.9J ug/L 10/31/17 16:1510.0EPA 6010
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Sample:9701-TRIP BLANK Lab ID:92360016001 Collected:10/19/17 08:00 Received:10/20/17 10:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/22/17 19:02 67-64-110010.0 1
Acrylonitrile ND ug/L 10/22/17 19:02 107-13-12001.9 1
Benzene ND ug/L 10/22/17 19:02 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/22/17 19:02 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/22/17 19:02 75-27-41.0 0.18 1
Bromoform ND ug/L 10/22/17 19:02 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/22/17 19:02 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/22/17 19:02 78-93-31000.96 1
Carbon disulfide ND ug/L 10/22/17 19:02 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/22/17 19:02 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/22/17 19:02 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/22/17 19:02 75-00-310.0 0.54 1
Chloroform ND ug/L 10/22/17 19:02 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/22/17 19:02 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/22/17 19:02 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/22/17 19:02 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/22/17 19:02 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/22/17 19:02 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/22/17 19:02 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/22/17 19:02 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/22/17 19:02 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/22/17 19:02 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/22/17 19:02 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/22/17 19:02 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/22/17 19:02 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/22/17 19:02 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/22/17 19:02 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 10/22/17 19:02 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/22/17 19:02 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 10/22/17 19:02 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/22/17 19:02 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/22/17 19:02 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/22/17 19:02 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/22/17 19:02 108-10-11000.33 1
Styrene ND ug/L 10/22/17 19:02 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/22/17 19:02 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/22/17 19:02 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/22/17 19:02 127-18-41.0 0.46 1
Toluene ND ug/L 10/22/17 19:02 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/22/17 19:02 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/22/17 19:02 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/22/17 19:02 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/22/17 19:02 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/22/17 19:02 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/22/17 19:02 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/22/17 19:02 75-01-41.0 0.62 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2017 10:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 7 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Sample:9701-TRIP BLANK Lab ID:92360016001 Collected:10/19/17 08:00 Received:10/20/17 10:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Xylene (Total)ND ug/L 10/22/17 19:02 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %10/22/17 19:02 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %10/22/17 19:02 17060-07-070-130 1
Toluene-d8 (S)101 %10/22/17 19:02 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2017 10:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Sample:9701-DOWNSTREAM Lab ID:92360016002 Collected:10/19/17 15:40 Received:10/20/17 10:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 10/31/17 15:53 7440-36-010/28/17 16:156.0 3.9 1
Arsenic ND ug/L 10/31/17 15:53 7440-38-210/28/17 16:1510.0 5.0 1
Barium 22.7J ug/L 10/31/17 15:53 7440-39-310/28/17 16:151002.5 1
Beryllium ND ug/L 10/31/17 15:53 7440-41-710/28/17 16:151.0 0.50 1
Cadmium ND ug/L 10/31/17 15:53 7440-43-910/28/17 16:151.0 0.50 1
Chromium ND ug/L 10/31/17 15:53 7440-47-310/28/17 16:1510.0 2.5 1
Cobalt ND ug/L 10/31/17 15:53 7440-48-410/28/17 16:1510.0 2.5 1
Copper ND ug/L 10/31/17 15:53 7440-50-810/28/17 16:1510.0 2.5 1
Lead ND ug/L 10/31/17 15:53 7439-92-110/28/17 16:1510.0 2.5 1
Nickel ND ug/L 10/31/17 15:53 7440-02-010/28/17 16:1550.0 2.5 1
Selenium ND ug/L 10/31/17 15:53 7782-49-210/28/17 16:1510.0 5.0 1
Silver ND ug/L 10/31/17 15:53 7440-22-410/28/17 16:1510.0 2.5 1
Vanadium ND ug/L 10/31/17 15:53 7440-62-210/28/17 16:1525.0 2.5 1
Zinc ND ug/L 10/31/17 15:53 7440-66-610/28/17 16:1510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 11/07/17 23:53 7440-28-0 1g10/31/17 09:355.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/22/17 21:04 67-64-110010.0 1
Acrylonitrile ND ug/L 10/22/17 21:04 107-13-12001.9 1
Benzene ND ug/L 10/22/17 21:04 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/22/17 21:04 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/22/17 21:04 75-27-41.0 0.18 1
Bromoform ND ug/L 10/22/17 21:04 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/22/17 21:04 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/22/17 21:04 78-93-31000.96 1
Carbon disulfide ND ug/L 10/22/17 21:04 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/22/17 21:04 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/22/17 21:04 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/22/17 21:04 75-00-310.0 0.54 1
Chloroform ND ug/L 10/22/17 21:04 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/22/17 21:04 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/22/17 21:04 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/22/17 21:04 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/22/17 21:04 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/22/17 21:04 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/22/17 21:04 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/22/17 21:04 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/22/17 21:04 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/22/17 21:04 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/22/17 21:04 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/22/17 21:04 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/22/17 21:04 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/22/17 21:04 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/22/17 21:04 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2017 10:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Sample:9701-DOWNSTREAM Lab ID:92360016002 Collected:10/19/17 15:40 Received:10/20/17 10:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 10/22/17 21:04 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/22/17 21:04 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 10/22/17 21:04 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/22/17 21:04 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/22/17 21:04 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/22/17 21:04 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/22/17 21:04 108-10-11000.33 1
Styrene ND ug/L 10/22/17 21:04 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/22/17 21:04 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/22/17 21:04 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/22/17 21:04 127-18-41.0 0.46 1
Toluene ND ug/L 10/22/17 21:04 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/22/17 21:04 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/22/17 21:04 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/22/17 21:04 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/22/17 21:04 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/22/17 21:04 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/22/17 21:04 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/22/17 21:04 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/22/17 21:04 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %10/22/17 21:04 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %10/22/17 21:04 17060-07-070-130 1
Toluene-d8 (S)104 %10/22/17 21:04 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2017 10:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Sample:9701-FIELD BLANK Lab ID:92360016003 Collected:10/19/17 17:00 Received:10/20/17 10:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 10/31/17 15:56 7440-36-010/28/17 16:156.0 3.9 1
Arsenic ND ug/L 10/31/17 15:56 7440-38-210/28/17 16:1510.0 5.0 1
Barium ND ug/L 10/31/17 15:56 7440-39-310/28/17 16:151002.5 1
Beryllium ND ug/L 10/31/17 15:56 7440-41-710/28/17 16:151.0 0.50 1
Cadmium ND ug/L 10/31/17 15:56 7440-43-910/28/17 16:151.0 0.50 1
Chromium ND ug/L 10/31/17 15:56 7440-47-310/28/17 16:1510.0 2.5 1
Cobalt ND ug/L 10/31/17 15:56 7440-48-410/28/17 16:1510.0 2.5 1
Copper ND ug/L 10/31/17 15:56 7440-50-810/28/17 16:1510.0 2.5 1
Lead ND ug/L 10/31/17 15:56 7439-92-110/28/17 16:1510.0 2.5 1
Nickel ND ug/L 10/31/17 15:56 7440-02-010/28/17 16:1550.0 2.5 1
Selenium 5.5J ug/L 10/31/17 15:56 7782-49-210/28/17 16:1510.0 5.0 1
Silver ND ug/L 10/31/17 15:56 7440-22-410/28/17 16:1510.0 2.5 1
Vanadium ND ug/L 10/31/17 15:56 7440-62-210/28/17 16:1525.0 2.5 1
Zinc ND ug/L 10/31/17 15:56 7440-66-610/28/17 16:1510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 11/07/17 23:56 7440-28-0 1g10/31/17 09:355.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/29/17 05:22 67-64-110010.0 1
Acrylonitrile ND ug/L 10/29/17 05:22 107-13-12001.9 1
Benzene ND ug/L 10/29/17 05:22 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/29/17 05:22 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/29/17 05:22 75-27-41.0 0.18 1
Bromoform ND ug/L 10/29/17 05:22 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/29/17 05:22 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/29/17 05:22 78-93-31000.96 1
Carbon disulfide ND ug/L 10/29/17 05:22 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/29/17 05:22 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/29/17 05:22 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/29/17 05:22 75-00-310.0 0.54 1
Chloroform ND ug/L 10/29/17 05:22 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/29/17 05:22 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/29/17 05:22 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/29/17 05:22 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/29/17 05:22 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/29/17 05:22 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/29/17 05:22 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/29/17 05:22 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/29/17 05:22 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/29/17 05:22 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/29/17 05:22 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/29/17 05:22 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/29/17 05:22 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/29/17 05:22 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/29/17 05:22 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2017 10:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 11 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Sample:9701-FIELD BLANK Lab ID:92360016003 Collected:10/19/17 17:00 Received:10/20/17 10:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 10/29/17 05:22 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/29/17 05:22 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 10/29/17 05:22 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/29/17 05:22 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/29/17 05:22 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/29/17 05:22 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/29/17 05:22 108-10-11000.33 1
Styrene ND ug/L 10/29/17 05:22 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/29/17 05:22 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/29/17 05:22 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/29/17 05:22 127-18-41.0 0.46 1
Toluene ND ug/L 10/29/17 05:22 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/29/17 05:22 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/29/17 05:22 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/29/17 05:22 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/29/17 05:22 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/29/17 05:22 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/29/17 05:22 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/29/17 05:22 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/29/17 05:22 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %10/29/17 05:22 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %10/29/17 05:22 17060-07-070-130 1
Toluene-d8 (S)101 %10/29/17 05:22 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2017 10:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Sample:9701-MW1 Lab ID:92360016004 Collected:10/19/17 13:58 Received:10/20/17 10:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 10/31/17 15:59 7440-36-010/28/17 16:156.0 3.9 1
Arsenic ND ug/L 10/31/17 15:59 7440-38-210/28/17 16:1510.0 5.0 1
Barium 115 ug/L 10/31/17 15:59 7440-39-310/28/17 16:151002.5 1
Beryllium ND ug/L 10/31/17 15:59 7440-41-710/28/17 16:151.0 0.50 1
Cadmium ND ug/L 10/31/17 15:59 7440-43-910/28/17 16:151.0 0.50 1
Chromium ND ug/L 10/31/17 15:59 7440-47-310/28/17 16:1510.0 2.5 1
Cobalt ND ug/L 10/31/17 15:59 7440-48-410/28/17 16:1510.0 2.5 1
Copper ND ug/L 10/31/17 15:59 7440-50-810/28/17 16:1510.0 2.5 1
Lead ND ug/L 10/31/17 15:59 7439-92-110/28/17 16:1510.0 2.5 1
Nickel ND ug/L 10/31/17 15:59 7440-02-010/28/17 16:1550.0 2.5 1
Selenium ND ug/L 10/31/17 15:59 7782-49-210/28/17 16:1510.0 5.0 1
Silver ND ug/L 10/31/17 15:59 7440-22-410/28/17 16:1510.0 2.5 1
Vanadium ND ug/L 10/31/17 15:59 7440-62-210/28/17 16:1525.0 2.5 1
Zinc 5.7J ug/L 10/31/17 15:59 7440-66-610/28/17 16:1510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 11/07/17 23:58 7440-28-0 1g10/31/17 09:355.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/22/17 21:21 67-64-110010.0 1
Acrylonitrile ND ug/L 10/22/17 21:21 107-13-12001.9 1
Benzene ND ug/L 10/22/17 21:21 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/22/17 21:21 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/22/17 21:21 75-27-41.0 0.18 1
Bromoform ND ug/L 10/22/17 21:21 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/22/17 21:21 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/22/17 21:21 78-93-31000.96 1
Carbon disulfide ND ug/L 10/22/17 21:21 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/22/17 21:21 56-23-51.0 0.25 1
Chlorobenzene 0.30J ug/L 10/22/17 21:21 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/22/17 21:21 75-00-310.0 0.54 1
Chloroform ND ug/L 10/22/17 21:21 67-66-35.0 0.14 1
Chloromethane 0.27J ug/L 10/22/17 21:21 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/22/17 21:21 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/22/17 21:21 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/22/17 21:21 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/22/17 21:21 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/22/17 21:21 95-50-15.0 0.30 1
1,4-Dichlorobenzene 0.40J ug/L 10/22/17 21:21 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/22/17 21:21 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/22/17 21:21 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/22/17 21:21 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/22/17 21:21 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/22/17 21:21 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/22/17 21:21 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/22/17 21:21 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2017 10:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Sample:9701-MW1 Lab ID:92360016004 Collected:10/19/17 13:58 Received:10/20/17 10:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 10/22/17 21:21 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/22/17 21:21 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 10/22/17 21:21 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/22/17 21:21 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/22/17 21:21 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/22/17 21:21 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/22/17 21:21 108-10-11000.33 1
Styrene ND ug/L 10/22/17 21:21 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/22/17 21:21 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/22/17 21:21 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/22/17 21:21 127-18-41.0 0.46 1
Toluene ND ug/L 10/22/17 21:21 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/22/17 21:21 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/22/17 21:21 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/22/17 21:21 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/22/17 21:21 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/22/17 21:21 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/22/17 21:21 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/22/17 21:21 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/22/17 21:21 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %10/22/17 21:21 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %10/22/17 21:21 17060-07-070-130 1
Toluene-d8 (S)105 %10/22/17 21:21 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2017 10:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Sample:9701-MW2 Lab ID:92360016005 Collected:10/19/17 16:42 Received:10/20/17 10:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 10/31/17 16:03 7440-36-010/28/17 16:156.0 3.9 1
Arsenic ND ug/L 10/31/17 16:03 7440-38-210/28/17 16:1510.0 5.0 1
Barium 10.9J ug/L 10/31/17 16:03 7440-39-310/28/17 16:151002.5 1
Beryllium ND ug/L 10/31/17 16:03 7440-41-710/28/17 16:151.0 0.50 1
Cadmium ND ug/L 10/31/17 16:03 7440-43-910/28/17 16:151.0 0.50 1
Chromium ND ug/L 10/31/17 16:03 7440-47-310/28/17 16:1510.0 2.5 1
Cobalt ND ug/L 10/31/17 16:03 7440-48-410/28/17 16:1510.0 2.5 1
Copper ND ug/L 10/31/17 16:03 7440-50-810/28/17 16:1510.0 2.5 1
Lead ND ug/L 10/31/17 16:03 7439-92-110/28/17 16:1510.0 2.5 1
Nickel ND ug/L 10/31/17 16:03 7440-02-010/28/17 16:1550.0 2.5 1
Selenium 9.7J ug/L 10/31/17 16:03 7782-49-210/28/17 16:1510.0 5.0 1
Silver ND ug/L 10/31/17 16:03 7440-22-410/28/17 16:1510.0 2.5 1
Vanadium ND ug/L 10/31/17 16:03 7440-62-210/28/17 16:1525.0 2.5 1
Zinc 13.2 ug/L 10/31/17 16:03 7440-66-610/28/17 16:1510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.071J ug/L 11/08/17 00:07 7440-28-010/31/17 09:355.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/22/17 21:38 67-64-110010.0 1
Acrylonitrile ND ug/L 10/22/17 21:38 107-13-12001.9 1
Benzene ND ug/L 10/22/17 21:38 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/22/17 21:38 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/22/17 21:38 75-27-41.0 0.18 1
Bromoform ND ug/L 10/22/17 21:38 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/22/17 21:38 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/22/17 21:38 78-93-31000.96 1
Carbon disulfide ND ug/L 10/22/17 21:38 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/22/17 21:38 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/22/17 21:38 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/22/17 21:38 75-00-310.0 0.54 1
Chloroform ND ug/L 10/22/17 21:38 67-66-35.0 0.14 1
Chloromethane 0.29J ug/L 10/22/17 21:38 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/22/17 21:38 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/22/17 21:38 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/22/17 21:38 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/22/17 21:38 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/22/17 21:38 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/22/17 21:38 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/22/17 21:38 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/22/17 21:38 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/22/17 21:38 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/22/17 21:38 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/22/17 21:38 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/22/17 21:38 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/22/17 21:38 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2017 10:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Sample:9701-MW2 Lab ID:92360016005 Collected:10/19/17 16:42 Received:10/20/17 10:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 10/22/17 21:38 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/22/17 21:38 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 10/22/17 21:38 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/22/17 21:38 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/22/17 21:38 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/22/17 21:38 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/22/17 21:38 108-10-11000.33 1
Styrene ND ug/L 10/22/17 21:38 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/22/17 21:38 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/22/17 21:38 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/22/17 21:38 127-18-41.0 0.46 1
Toluene ND ug/L 10/22/17 21:38 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/22/17 21:38 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/22/17 21:38 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/22/17 21:38 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/22/17 21:38 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/22/17 21:38 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/22/17 21:38 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/22/17 21:38 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/22/17 21:38 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %10/22/17 21:38 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %10/22/17 21:38 17060-07-070-130 1
Toluene-d8 (S)105 %10/22/17 21:38 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2017 10:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Sample:9701-MW3 Lab ID:92360016006 Collected:10/19/17 15:24 Received:10/20/17 10:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 10/31/17 16:06 7440-36-010/28/17 16:156.0 3.9 1
Arsenic ND ug/L 10/31/17 16:06 7440-38-210/28/17 16:1510.0 5.0 1
Barium 10.2J ug/L 10/31/17 16:06 7440-39-310/28/17 16:151002.5 1
Beryllium ND ug/L 10/31/17 16:06 7440-41-710/28/17 16:151.0 0.50 1
Cadmium ND ug/L 10/31/17 16:06 7440-43-910/28/17 16:151.0 0.50 1
Chromium ND ug/L 10/31/17 16:06 7440-47-310/28/17 16:1510.0 2.5 1
Cobalt ND ug/L 10/31/17 16:06 7440-48-410/28/17 16:1510.0 2.5 1
Copper ND ug/L 10/31/17 16:06 7440-50-810/28/17 16:1510.0 2.5 1
Lead ND ug/L 10/31/17 16:06 7439-92-110/28/17 16:1510.0 2.5 1
Nickel ND ug/L 10/31/17 16:06 7440-02-010/28/17 16:1550.0 2.5 1
Selenium ND ug/L 10/31/17 16:06 7782-49-210/28/17 16:1510.0 5.0 1
Silver ND ug/L 10/31/17 16:06 7440-22-410/28/17 16:1510.0 2.5 1
Vanadium ND ug/L 10/31/17 16:06 7440-62-210/28/17 16:1525.0 2.5 1
Zinc ND ug/L 10/31/17 16:06 7440-66-610/28/17 16:1510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 11/08/17 00:10 7440-28-010/31/17 09:355.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/22/17 21:55 67-64-110010.0 1
Acrylonitrile ND ug/L 10/22/17 21:55 107-13-12001.9 1
Benzene ND ug/L 10/22/17 21:55 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/22/17 21:55 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/22/17 21:55 75-27-41.0 0.18 1
Bromoform ND ug/L 10/22/17 21:55 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/22/17 21:55 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/22/17 21:55 78-93-31000.96 1
Carbon disulfide ND ug/L 10/22/17 21:55 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/22/17 21:55 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/22/17 21:55 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/22/17 21:55 75-00-310.0 0.54 1
Chloroform ND ug/L 10/22/17 21:55 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/22/17 21:55 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/22/17 21:55 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/22/17 21:55 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/22/17 21:55 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/22/17 21:55 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/22/17 21:55 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/22/17 21:55 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/22/17 21:55 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/22/17 21:55 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/22/17 21:55 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/22/17 21:55 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/22/17 21:55 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/22/17 21:55 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/22/17 21:55 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2017 10:03 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
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Page 17 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Sample:9701-MW3 Lab ID:92360016006 Collected:10/19/17 15:24 Received:10/20/17 10:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 10/22/17 21:55 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/22/17 21:55 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 10/22/17 21:55 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/22/17 21:55 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/22/17 21:55 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/22/17 21:55 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/22/17 21:55 108-10-11000.33 1
Styrene ND ug/L 10/22/17 21:55 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/22/17 21:55 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/22/17 21:55 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/22/17 21:55 127-18-41.0 0.46 1
Toluene ND ug/L 10/22/17 21:55 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/22/17 21:55 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/22/17 21:55 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/22/17 21:55 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/22/17 21:55 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/22/17 21:55 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/22/17 21:55 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/22/17 21:55 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/22/17 21:55 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %10/22/17 21:55 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %10/22/17 21:55 17060-07-070-130 1
Toluene-d8 (S)105 %10/22/17 21:55 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2017 10:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Sample:9701-MW4 Lab ID:92360016007 Collected:10/19/17 15:50 Received:10/20/17 10:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 10/31/17 16:09 7440-36-010/28/17 16:156.0 3.9 1
Arsenic ND ug/L 10/31/17 16:09 7440-38-210/28/17 16:1510.0 5.0 1
Barium 93.5J ug/L 10/31/17 16:09 7440-39-310/28/17 16:151002.5 1
Beryllium ND ug/L 10/31/17 16:09 7440-41-710/28/17 16:151.0 0.50 1
Cadmium ND ug/L 10/31/17 16:09 7440-43-910/28/17 16:151.0 0.50 1
Chromium ND ug/L 10/31/17 16:09 7440-47-310/28/17 16:1510.0 2.5 1
Cobalt 13.5 ug/L 10/31/17 16:09 7440-48-410/28/17 16:1510.0 2.5 1
Copper 9.6J ug/L 10/31/17 16:09 7440-50-810/28/17 16:1510.0 2.5 1
Lead 2.6J ug/L 10/31/17 16:09 7439-92-110/28/17 16:1510.0 2.5 1
Nickel 4.6J ug/L 10/31/17 16:09 7440-02-010/28/17 16:1550.0 2.5 1
Selenium ND ug/L 10/31/17 16:09 7782-49-210/28/17 16:1510.0 5.0 1
Silver ND ug/L 10/31/17 16:09 7440-22-410/28/17 16:1510.0 2.5 1
Vanadium 4.1J ug/L 10/31/17 16:09 7440-62-210/28/17 16:1525.0 2.5 1
Zinc ND ug/L 10/31/17 16:09 7440-66-610/28/17 16:1510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.025J ug/L 11/08/17 00:12 7440-28-010/31/17 09:355.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/22/17 22:13 67-64-110010.0 1
Acrylonitrile ND ug/L 10/22/17 22:13 107-13-12001.9 1
Benzene ND ug/L 10/22/17 22:13 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/22/17 22:13 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/22/17 22:13 75-27-41.0 0.18 1
Bromoform ND ug/L 10/22/17 22:13 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/22/17 22:13 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/22/17 22:13 78-93-31000.96 1
Carbon disulfide ND ug/L 10/22/17 22:13 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/22/17 22:13 56-23-51.0 0.25 1
Chlorobenzene 5.1 ug/L 10/22/17 22:13 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/22/17 22:13 75-00-310.0 0.54 1
Chloroform ND ug/L 10/22/17 22:13 67-66-35.0 0.14 1
Chloromethane 0.25J ug/L 10/22/17 22:13 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/22/17 22:13 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/22/17 22:13 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/22/17 22:13 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/22/17 22:13 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/22/17 22:13 95-50-15.0 0.30 1
1,4-Dichlorobenzene 2.4 ug/L 10/22/17 22:13 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/22/17 22:13 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/22/17 22:13 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/22/17 22:13 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/22/17 22:13 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/22/17 22:13 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/22/17 22:13 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/22/17 22:13 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2017 10:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 19 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Sample:9701-MW4 Lab ID:92360016007 Collected:10/19/17 15:50 Received:10/20/17 10:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 10/22/17 22:13 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/22/17 22:13 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 10/22/17 22:13 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/22/17 22:13 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/22/17 22:13 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/22/17 22:13 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/22/17 22:13 108-10-11000.33 1
Styrene ND ug/L 10/22/17 22:13 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/22/17 22:13 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/22/17 22:13 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/22/17 22:13 127-18-41.0 0.46 1
Toluene ND ug/L 10/22/17 22:13 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/22/17 22:13 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/22/17 22:13 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/22/17 22:13 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/22/17 22:13 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/22/17 22:13 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/22/17 22:13 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/22/17 22:13 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/22/17 22:13 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %10/22/17 22:13 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %10/22/17 22:13 17060-07-070-130 1
Toluene-d8 (S)106 %10/22/17 22:13 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2017 10:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Sample:9701-MW5 Lab ID:92360016008 Collected:10/19/17 16:55 Received:10/20/17 10:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 10/31/17 16:12 7440-36-010/28/17 16:156.0 3.9 1
Arsenic ND ug/L 10/31/17 16:12 7440-38-210/28/17 16:1510.0 5.0 1
Barium 442 ug/L 10/31/17 16:12 7440-39-310/28/17 16:151002.5 1
Beryllium ND ug/L 10/31/17 16:12 7440-41-710/28/17 16:151.0 0.50 1
Cadmium ND ug/L 10/31/17 16:12 7440-43-910/28/17 16:151.0 0.50 1
Chromium ND ug/L 10/31/17 16:12 7440-47-310/28/17 16:1510.0 2.5 1
Cobalt 14.1 ug/L 10/31/17 16:12 7440-48-410/28/17 16:1510.0 2.5 1
Copper 3.3J ug/L 10/31/17 16:12 7440-50-810/28/17 16:1510.0 2.5 1
Lead 4.8J ug/L 10/31/17 16:12 7439-92-110/28/17 16:1510.0 2.5 1
Nickel 9.9J ug/L 10/31/17 16:12 7440-02-010/28/17 16:1550.0 2.5 1
Selenium ND ug/L 10/31/17 16:12 7782-49-210/28/17 16:1510.0 5.0 1
Silver ND ug/L 10/31/17 16:12 7440-22-410/28/17 16:1510.0 2.5 1
Vanadium 4.4J ug/L 10/31/17 16:12 7440-62-210/28/17 16:1525.0 2.5 1
Zinc 7.4J ug/L 10/31/17 16:12 7440-66-610/28/17 16:1510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium 0.040J ug/L 11/08/17 00:19 7440-28-010/31/17 09:355.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/22/17 22:30 67-64-110010.0 1
Acrylonitrile ND ug/L 10/22/17 22:30 107-13-12001.9 1
Benzene 1.0 ug/L 10/22/17 22:30 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/22/17 22:30 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/22/17 22:30 75-27-41.0 0.18 1
Bromoform ND ug/L 10/22/17 22:30 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/22/17 22:30 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/22/17 22:30 78-93-31000.96 1
Carbon disulfide ND ug/L 10/22/17 22:30 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/22/17 22:30 56-23-51.0 0.25 1
Chlorobenzene 9.6 ug/L 10/22/17 22:30 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/22/17 22:30 75-00-310.0 0.54 1
Chloroform ND ug/L 10/22/17 22:30 67-66-35.0 0.14 1
Chloromethane 0.20J ug/L 10/22/17 22:30 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/22/17 22:30 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/22/17 22:30 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/22/17 22:30 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/22/17 22:30 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/22/17 22:30 95-50-15.0 0.30 1
1,4-Dichlorobenzene 4.0 ug/L 10/22/17 22:30 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/22/17 22:30 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/22/17 22:30 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/22/17 22:30 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/22/17 22:30 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/22/17 22:30 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/22/17 22:30 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/22/17 22:30 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2017 10:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Sample:9701-MW5 Lab ID:92360016008 Collected:10/19/17 16:55 Received:10/20/17 10:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 10/22/17 22:30 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/22/17 22:30 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 10/22/17 22:30 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/22/17 22:30 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/22/17 22:30 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/22/17 22:30 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/22/17 22:30 108-10-11000.33 1
Styrene ND ug/L 10/22/17 22:30 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/22/17 22:30 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/22/17 22:30 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/22/17 22:30 127-18-41.0 0.46 1
Toluene ND ug/L 10/22/17 22:30 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/22/17 22:30 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/22/17 22:30 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/22/17 22:30 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/22/17 22:30 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/22/17 22:30 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/22/17 22:30 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/22/17 22:30 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/22/17 22:30 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %10/22/17 22:30 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %10/22/17 22:30 17060-07-070-130 1
Toluene-d8 (S)104 %10/22/17 22:30 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2017 10:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Sample:9701-UPSTREAM Lab ID:92360016009 Collected:10/19/17 15:50 Received:10/20/17 10:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 10/31/17 16:15 7440-36-010/28/17 16:156.0 3.9 1
Arsenic ND ug/L 10/31/17 16:15 7440-38-210/28/17 16:1510.0 5.0 1
Barium 22.7J ug/L 10/31/17 16:15 7440-39-310/28/17 16:151002.5 1
Beryllium ND ug/L 10/31/17 16:15 7440-41-710/28/17 16:151.0 0.50 1
Cadmium ND ug/L 10/31/17 16:15 7440-43-910/28/17 16:151.0 0.50 1
Chromium ND ug/L 10/31/17 16:15 7440-47-310/28/17 16:1510.0 2.5 1
Cobalt ND ug/L 10/31/17 16:15 7440-48-410/28/17 16:1510.0 2.5 1
Copper ND ug/L 10/31/17 16:15 7440-50-810/28/17 16:1510.0 2.5 1
Lead ND ug/L 10/31/17 16:15 7439-92-110/28/17 16:1510.0 2.5 1
Nickel ND ug/L 10/31/17 16:15 7440-02-010/28/17 16:1550.0 2.5 1
Selenium 7.9J ug/L 10/31/17 16:15 7782-49-210/28/17 16:1510.0 5.0 1
Silver ND ug/L 10/31/17 16:15 7440-22-410/28/17 16:1510.0 2.5 1
Vanadium ND ug/L 10/31/17 16:15 7440-62-210/28/17 16:1525.0 2.5 1
Zinc ND ug/L 10/31/17 16:15 7440-66-610/28/17 16:1510.0 5.0 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Thallium ND ug/L 11/08/17 00:22 7440-28-010/31/17 09:355.5 0.020 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/22/17 22:47 67-64-110010.0 1
Acrylonitrile ND ug/L 10/22/17 22:47 107-13-12001.9 1
Benzene ND ug/L 10/22/17 22:47 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 10/22/17 22:47 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 10/22/17 22:47 75-27-41.0 0.18 1
Bromoform ND ug/L 10/22/17 22:47 75-25-23.0 0.26 1
Bromomethane ND ug/L 10/22/17 22:47 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 10/22/17 22:47 78-93-31000.96 1
Carbon disulfide ND ug/L 10/22/17 22:47 75-15-01001.2 1
Carbon tetrachloride ND ug/L 10/22/17 22:47 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 10/22/17 22:47 108-90-73.0 0.23 1
Chloroethane ND ug/L 10/22/17 22:47 75-00-310.0 0.54 1
Chloroform ND ug/L 10/22/17 22:47 67-66-35.0 0.14 1
Chloromethane ND ug/L 10/22/17 22:47 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 10/22/17 22:47 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 10/22/17 22:47 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 10/22/17 22:47 106-93-41.0 0.27 1
Dibromomethane ND ug/L 10/22/17 22:47 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 10/22/17 22:47 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 10/22/17 22:47 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 10/22/17 22:47 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 10/22/17 22:47 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 10/22/17 22:47 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 10/22/17 22:47 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 10/22/17 22:47 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 10/22/17 22:47 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 10/22/17 22:47 78-87-51.0 0.27 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/08/2017 10:03 AM
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Page 23 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Sample:9701-UPSTREAM Lab ID:92360016009 Collected:10/19/17 15:50 Received:10/20/17 10:41 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
cis-1,3-Dichloropropene ND ug/L 10/22/17 22:47 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 10/22/17 22:47 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 10/22/17 22:47 100-41-41.0 0.30 1
2-Hexanone ND ug/L 10/22/17 22:47 591-78-650.0 0.46 1
Iodomethane ND ug/L 10/22/17 22:47 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 10/22/17 22:47 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/22/17 22:47 108-10-11000.33 1
Styrene ND ug/L 10/22/17 22:47 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 10/22/17 22:47 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 10/22/17 22:47 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 10/22/17 22:47 127-18-41.0 0.46 1
Toluene ND ug/L 10/22/17 22:47 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 10/22/17 22:47 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 10/22/17 22:47 79-00-51.0 0.29 1
Trichloroethene ND ug/L 10/22/17 22:47 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 10/22/17 22:47 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 10/22/17 22:47 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 10/22/17 22:47 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 10/22/17 22:47 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 10/22/17 22:47 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %10/22/17 22:47 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %10/22/17 22:47 17060-07-070-130 1
Toluene-d8 (S)103 %10/22/17 22:47 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/08/2017 10:03 AM
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[phone]
Page 24 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
384390
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples:92360016002, 92360016003, 92360016004, 92360016005, 92360016006, 92360016007, 92360016008,
92360016009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2130719
Associated Lab Samples:92360016002, 92360016003, 92360016004, 92360016005, 92360016006, 92360016007, 92360016008,
92360016009
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 10/31/17 15:283.9
Arsenic ug/L ND 10.0 10/31/17 15:285.0
Barium ug/L ND 100 10/31/17 15:282.5
Beryllium ug/L ND 1.0 10/31/17 15:280.50
Cadmium ug/L ND 1.0 10/31/17 15:280.50
Chromium ug/L ND 10.0 10/31/17 15:282.5
Cobalt ug/L ND 10.0 10/31/17 15:282.5
Copper ug/L ND 10.0 10/31/17 15:282.5
Lead ug/L ND 10.0 10/31/17 15:282.5
Nickel ug/L ND 50.0 10/31/17 15:282.5
Selenium ug/L ND 10.0 10/31/17 15:285.0
Silver ug/L ND 10.0 10/31/17 15:282.5
Vanadium ug/L ND 25.0 10/31/17 15:282.5
Zinc ug/L ND 10.0 10/31/17 15:285.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2130720LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 492500 98 80-120
Arsenic ug/L 481500 96 80-120
Barium ug/L 501500 100 80-120
Beryllium ug/L 503500 101 80-120
Cadmium ug/L 488500 98 80-120
Chromium ug/L 470500 94 80-120
Cobalt ug/L 491500 98 80-120
Copper ug/L 488500 98 80-120
Lead ug/L 483500 97 80-120
Nickel ug/L 473500 95 80-120
Selenium ug/L 492500 98 80-120
Silver ug/L 244250 98 80-120
Vanadium ug/L 481500 96 80-120
Zinc ug/L 489500 98 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/08/2017 10:03 AM
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Huntersville, NC 28078
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Page 25 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2130721MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92360013005
2130722
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 102 75-125101 1 20500ND512504
Arsenic ug/L 500 100 75-125100 0 20500ND501501
Barium ug/L 500 106 75-125105 1 2050063.4J 592 588
Beryllium ug/L 500 106 75-125106 0 20500ND530529
Cadmium ug/L 500 102 75-125101 1 205005.1 514 509
Chromium ug/L 500 98 75-12598 1 20500ND492488
Cobalt ug/L 500 103 75-125101 1 20500ND514507
Copper ug/L 500 103 75-125103 0 20500ND516514
Lead ug/L 500 101 75-12599 2 20500ND506494
Nickel ug/L 500 99 75-12598 1 2050010.7J 505 499
Selenium ug/L 500 102 75-125102 0 20500ND509509
Silver ug/L 250 101 75-125100 1 20250ND253252
Vanadium ug/L 500 101 75-12599 2 20500ND505497
Zinc ug/L 500 102 75-125100 2 2050016.4 528 519
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/08/2017 10:03 AM
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Page 26 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
384619
EPA 3010A
EPA 6020B
6020 MET
Associated Lab Samples:92360016002, 92360016003, 92360016004, 92360016005, 92360016006, 92360016007, 92360016008,
92360016009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2131748
Associated Lab Samples:92360016002, 92360016003, 92360016004, 92360016005, 92360016006, 92360016007, 92360016008,
92360016009
Matrix:Water
AnalyzedMDL
Thallium ug/L ND 5.5 1g11/07/17 23:250.020
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2131749LABORATORY CONTROL SAMPLE:
LCSSpike
Thallium ug/L 103100 103 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2131750MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92360013002
2131751
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Thallium ug/L 100 97 75-12595 2 20100ND97.1 95.3
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2131752MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92360013003
2131753
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Thallium ug/L 100 97 75-12595 2 201000.029J 97.2 95.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2017 10:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
383479
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92360016001, 92360016002, 92360016004, 92360016005, 92360016006, 92360016007, 92360016008,
92360016009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2125383
Associated Lab Samples:92360016001, 92360016002, 92360016004, 92360016005, 92360016006, 92360016007, 92360016008,
92360016009
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 10/22/17 14:440.33
1,1,1-Trichloroethane ug/L ND 1.0 10/22/17 14:440.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 10/22/17 14:440.40
1,1,2-Trichloroethane ug/L ND 1.0 10/22/17 14:440.29
1,1-Dichloroethane ug/L ND 5.0 10/22/17 14:440.32
1,1-Dichloroethene ug/L ND 5.0 10/22/17 14:440.56
1,2,3-Trichloropropane ug/L ND 1.0 10/22/17 14:440.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 10/22/17 14:442.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 10/22/17 14:440.27
1,2-Dichlorobenzene ug/L ND 5.0 10/22/17 14:440.30
1,2-Dichloroethane ug/L ND 1.0 10/22/17 14:440.24
1,2-Dichloropropane ug/L ND 1.0 10/22/17 14:440.27
1,4-Dichlorobenzene ug/L ND 1.0 10/22/17 14:440.33
2-Butanone (MEK)ug/L ND 100 10/22/17 14:440.96
2-Hexanone ug/L ND 50.0 10/22/17 14:440.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 10/22/17 14:440.33
Acetone ug/L ND 100 10/22/17 14:4410.0
Acrylonitrile ug/L ND 200 10/22/17 14:441.9
Benzene ug/L ND 1.0 10/22/17 14:440.25
Bromochloromethane ug/L ND 3.0 10/22/17 14:440.17
Bromodichloromethane ug/L ND 1.0 10/22/17 14:440.18
Bromoform ug/L ND 3.0 10/22/17 14:440.26
Bromomethane ug/L ND 10.0 10/22/17 14:440.29
Carbon disulfide ug/L ND 100 10/22/17 14:441.2
Carbon tetrachloride ug/L ND 1.0 10/22/17 14:440.25
Chlorobenzene ug/L ND 3.0 10/22/17 14:440.23
Chloroethane ug/L ND 10.0 10/22/17 14:440.54
Chloroform ug/L 0.34J 5.0 10/22/17 14:440.14
Chloromethane ug/L ND 1.0 10/22/17 14:440.11
cis-1,2-Dichloroethene ug/L ND 5.0 10/22/17 14:440.19
cis-1,3-Dichloropropene ug/L ND 1.0 10/22/17 14:440.13
Dibromochloromethane ug/L ND 3.0 10/22/17 14:440.21
Dibromomethane ug/L ND 10.0 10/22/17 14:440.21
Ethylbenzene ug/L ND 1.0 10/22/17 14:440.30
Iodomethane ug/L ND 10.0 10/22/17 14:440.32
Methylene Chloride ug/L ND 1.0 10/22/17 14:440.97
Styrene ug/L ND 1.0 10/22/17 14:440.26
Tetrachloroethene ug/L ND 1.0 10/22/17 14:440.46
Toluene ug/L ND 1.0 10/22/17 14:440.26
trans-1,2-Dichloroethene ug/L ND 5.0 10/22/17 14:440.49
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/08/2017 10:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2125383
Associated Lab Samples:92360016001, 92360016002, 92360016004, 92360016005, 92360016006, 92360016007, 92360016008,
92360016009
Matrix:Water
AnalyzedMDL
trans-1,3-Dichloropropene ug/L ND 1.0 10/22/17 14:440.26
trans-1,4-Dichloro-2-butene ug/L ND 100 10/22/17 14:441.0
Trichloroethene ug/L ND 1.0 10/22/17 14:440.47
Trichlorofluoromethane ug/L ND 1.0 10/22/17 14:440.20
Vinyl acetate ug/L ND 50.0 10/22/17 14:440.35
Vinyl chloride ug/L ND 1.0 10/22/17 14:440.62
Xylene (Total)ug/L ND 5.0 10/22/17 14:440.66
1,2-Dichloroethane-d4 (S)%94 70-130 10/22/17 14:44
4-Bromofluorobenzene (S)%97 70-130 10/22/17 14:44
Toluene-d8 (S)%102 70-130 10/22/17 14:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2125384LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 59.250 118 80-125
1,1,1-Trichloroethane ug/L 51.850 104 71-129
1,1,2,2-Tetrachloroethane ug/L 55.250 110 79-124
1,1,2-Trichloroethane ug/L 54.950 110 85-125
1,1-Dichloroethane ug/L 48.750 97 73-126
1,1-Dichloroethene ug/L 48.850 98 66-135
1,2,3-Trichloropropane ug/L 57.550 115 75-130
1,2-Dibromo-3-chloropropane ug/L 63.050 126 71-133
1,2-Dibromoethane (EDB)ug/L 59.850 120 83-124
1,2-Dichlorobenzene ug/L 58.050 116 80-133
1,2-Dichloroethane ug/L 49.550 99 67-128
1,2-Dichloropropane ug/L 54.550 109 75-132
1,4-Dichlorobenzene ug/L 57.850 116 78-130
2-Butanone (MEK)ug/L 108100 108 61-144
2-Hexanone ug/L 110100 110 68-143
4-Methyl-2-pentanone (MIBK)ug/L 102100 102 72-135
Acetone ug/L 104100 104 48-146
Acrylonitrile ug/L 257250 103 40-160
Benzene ug/L 53.450 107 80-125
Bromochloromethane ug/L 51.350 103 71-125
Bromodichloromethane ug/L 53.150 106 78-124
Bromoform ug/L 63.050 126 71-128
Bromomethane ug/L 45.650 91 40-160
Carbon disulfide ug/L 52.4J50 105 50-160
Carbon tetrachloride ug/L 49.650 99 69-131
Chlorobenzene ug/L 54.850 110 81-122
Chloroethane ug/L 48.350 97 39-148
Chloroform ug/L 46.050 92 73-127
Chloromethane ug/L 51.550 103 44-146
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/08/2017 10:03 AM
Pace Analytical Services, LLC
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Page 29 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2125384LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 50.950 102 74-124
cis-1,3-Dichloropropene ug/L 58.650 117 72-132
Dibromochloromethane ug/L 55.650 111 78-125
Dibromomethane ug/L 50.650 101 82-120
Ethylbenzene ug/L 55.750 111 79-121
Iodomethane ug/L 102100 102 39-154
Methylene Chloride ug/L 48.550 97 64-133
Styrene ug/L 56.650 113 84-126
Tetrachloroethene ug/L 57.150 114 78-122
Toluene ug/L 50.650 101 80-121
trans-1,2-Dichloroethene ug/L 50.650 101 71-127
trans-1,3-Dichloropropene ug/L 58.450 117 69-141
trans-1,4-Dichloro-2-butene ug/L 56.7J50 113 40-160
Trichloroethene ug/L 55.150 110 78-122
Trichlorofluoromethane ug/L 48.250 96 53-137
Vinyl acetate ug/L 102100 102 40-160
Vinyl chloride ug/L 53.050 106 58-137
Xylene (Total)ug/L 168150 112 81-126
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%95 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2125388MATRIX SPIKE SAMPLE:
MSSpike
Result
92360013007
1,1,1,2-Tetrachloroethane ug/L 21.820 109 70-130ND
1,1,1-Trichloroethane ug/L 21.620 108 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.020 100 70-130ND
1,1,2-Trichloroethane ug/L 20.420 102 70-130ND
1,1-Dichloroethane ug/L 20.420 102 70-130ND
1,1-Dichloroethene ug/L 22.020 110 70-166ND
1,2,3-Trichloropropane ug/L 21.720 109 70-130ND
1,2-Dibromo-3-chloropropane ug/L 19.820 99 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.920 109 70-130ND
1,2-Dichlorobenzene ug/L 22.020 110 70-130ND
1,2-Dichloroethane ug/L 20.220 101 70-130ND
1,2-Dichloropropane ug/L 21.520 107 70-130ND
1,4-Dichlorobenzene ug/L 21.720 109 70-130ND
2-Butanone (MEK)ug/L 41.4J40 104 70-130ND
2-Hexanone ug/L 38.7J40 97 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 38.3J40 96 70-130ND
Acetone ug/L 38.4J40 96 70-130ND
Acrylonitrile ug/L 102J100 102 70-130ND
Benzene ug/L 20.920 105 70-148ND
Bromochloromethane ug/L 20.520 103 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/08/2017 10:03 AM
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Page 30 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2125388MATRIX SPIKE SAMPLE:
MSSpike
Result
92360013007
Bromodichloromethane ug/L 20.620 103 70-130ND
Bromoform ug/L 20.720 104 70-130ND
Bromomethane ug/L 16.720 84 70-130ND
Carbon disulfide ug/L 21.9J20 109 70-130ND
Carbon tetrachloride ug/L 21.320 107 70-130ND
Chlorobenzene ug/L 22.020 110 70-146ND
Chloroethane ug/L 21.220 106 70-130ND
Chloroform ug/L 18.920 95 70-130ND
Chloromethane ug/L 22.320 110 70-1300.20J
cis-1,2-Dichloroethene ug/L 21.520 107 70-130ND
cis-1,3-Dichloropropene ug/L 20.420 102 70-130ND
Dibromochloromethane ug/L 20.620 103 70-130ND
Dibromomethane ug/L 20.620 103 70-130ND
Ethylbenzene ug/L 22.420 112 70-130ND
Iodomethane ug/L 38.540 96 70-130ND
Methylene Chloride ug/L 17.320 87 70-130ND
Styrene ug/L 20.720 103 70-130ND
Tetrachloroethene ug/L 22.120 110 70-130ND
Toluene ug/L 20.620 103 70-155ND
trans-1,2-Dichloroethene ug/L 21.020 105 70-130ND
trans-1,3-Dichloropropene ug/L 20.120 100 70-130ND
trans-1,4-Dichloro-2-butene ug/L 17.8J20 89 70-130ND
Trichloroethene ug/L 22.020 110 69-151ND
Trichlorofluoromethane ug/L 21.420 107 70-130ND
Vinyl acetate ug/L 33.5J40 84 70-130ND
Vinyl chloride ug/L 23.420 117 70-130ND
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%95 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92360013006
2125387SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/08/2017 10:03 AM
Pace Analytical Services, LLC
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[phone]
Page 31 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92360013006
2125387SAMPLE DUPLICATE:
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 300.23J
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%97 298
4-Bromofluorobenzene (S)%96 398
Toluene-d8 (S)%107 4102
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
384397
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92360016003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2130739
Associated Lab Samples:92360016003
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 10/29/17 01:510.33
1,1,1-Trichloroethane ug/L ND 1.0 10/29/17 01:510.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 10/29/17 01:510.40
1,1,2-Trichloroethane ug/L ND 1.0 10/29/17 01:510.29
1,1-Dichloroethane ug/L ND 5.0 10/29/17 01:510.32
1,1-Dichloroethene ug/L ND 5.0 10/29/17 01:510.56
1,2,3-Trichloropropane ug/L ND 1.0 10/29/17 01:510.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 10/29/17 01:512.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 10/29/17 01:510.27
1,2-Dichlorobenzene ug/L ND 5.0 10/29/17 01:510.30
1,2-Dichloroethane ug/L ND 1.0 10/29/17 01:510.24
1,2-Dichloropropane ug/L ND 1.0 10/29/17 01:510.27
1,4-Dichlorobenzene ug/L ND 1.0 10/29/17 01:510.33
2-Butanone (MEK)ug/L ND 100 10/29/17 01:510.96
2-Hexanone ug/L ND 50.0 10/29/17 01:510.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 10/29/17 01:510.33
Acetone ug/L ND 100 10/29/17 01:5110.0
Acrylonitrile ug/L ND 200 10/29/17 01:511.9
Benzene ug/L ND 1.0 10/29/17 01:510.25
Bromochloromethane ug/L ND 3.0 10/29/17 01:510.17
Bromodichloromethane ug/L ND 1.0 10/29/17 01:510.18
Bromoform ug/L ND 3.0 10/29/17 01:510.26
Bromomethane ug/L ND 10.0 10/29/17 01:510.29
Carbon disulfide ug/L ND 100 10/29/17 01:511.2
Carbon tetrachloride ug/L ND 1.0 10/29/17 01:510.25
Chlorobenzene ug/L ND 3.0 10/29/17 01:510.23
Chloroethane ug/L ND 10.0 10/29/17 01:510.54
Chloroform ug/L 0.19J 5.0 10/29/17 01:510.14
Chloromethane ug/L ND 1.0 10/29/17 01:510.11
cis-1,2-Dichloroethene ug/L ND 5.0 10/29/17 01:510.19
cis-1,3-Dichloropropene ug/L ND 1.0 10/29/17 01:510.13
Dibromochloromethane ug/L ND 3.0 10/29/17 01:510.21
Dibromomethane ug/L ND 10.0 10/29/17 01:510.21
Ethylbenzene ug/L ND 1.0 10/29/17 01:510.30
Iodomethane ug/L ND 10.0 10/29/17 01:510.32
Methylene Chloride ug/L ND 1.0 10/29/17 01:510.97
Styrene ug/L ND 1.0 10/29/17 01:510.26
Tetrachloroethene ug/L ND 1.0 10/29/17 01:510.46
Toluene ug/L ND 1.0 10/29/17 01:510.26
trans-1,2-Dichloroethene ug/L ND 5.0 10/29/17 01:510.49
trans-1,3-Dichloropropene ug/L ND 1.0 10/29/17 01:510.26
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2130739
Associated Lab Samples:92360016003
Matrix:Water
AnalyzedMDL
trans-1,4-Dichloro-2-butene ug/L ND 100 10/29/17 01:511.0
Trichloroethene ug/L ND 1.0 10/29/17 01:510.47
Trichlorofluoromethane ug/L ND 1.0 10/29/17 01:510.20
Vinyl acetate ug/L ND 50.0 10/29/17 01:510.35
Vinyl chloride ug/L ND 1.0 10/29/17 01:510.62
Xylene (Total)ug/L ND 5.0 10/29/17 01:510.66
1,2-Dichloroethane-d4 (S)%100 70-130 10/29/17 01:51
4-Bromofluorobenzene (S)%98 70-130 10/29/17 01:51
Toluene-d8 (S)%100 70-130 10/29/17 01:51
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2130740LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.050 104 80-125
1,1,1-Trichloroethane ug/L 46.450 93 71-129
1,1,2,2-Tetrachloroethane ug/L 46.550 93 79-124
1,1,2-Trichloroethane ug/L 48.550 97 85-125
1,1-Dichloroethane ug/L 44.850 90 73-126
1,1-Dichloroethene ug/L 48.050 96 66-135
1,2,3-Trichloropropane ug/L 52.350 105 75-130
1,2-Dibromo-3-chloropropane ug/L 46.850 94 71-133
1,2-Dibromoethane (EDB)ug/L 53.950 108 83-124
1,2-Dichlorobenzene ug/L 48.950 98 80-133
1,2-Dichloroethane ug/L 48.850 98 67-128
1,2-Dichloropropane ug/L 48.450 97 75-132
1,4-Dichlorobenzene ug/L 47.950 96 78-130
2-Butanone (MEK)ug/L 99.7J100 100 61-144
2-Hexanone ug/L 98.3100 98 68-143
4-Methyl-2-pentanone (MIBK)ug/L 101100 101 72-135
Acetone ug/L 101100 101 48-146
Acrylonitrile ug/L 242250 97 40-160
Benzene ug/L 46.550 93 80-125
Bromochloromethane ug/L 47.650 95 71-125
Bromodichloromethane ug/L 46.150 92 78-124
Bromoform ug/L 51.050 102 71-128
Bromomethane ug/L 62.350 125 40-160
Carbon disulfide ug/L 47.3J50 95 50-160
Carbon tetrachloride ug/L 45.150 90 69-131
Chlorobenzene ug/L 47.950 96 81-122
Chloroethane ug/L 52.850 106 39-148
Chloroform ug/L 42.550 85 73-127
Chloromethane ug/L 50.150 100 44-146
cis-1,2-Dichloroethene ug/L 47.050 94 74-124
cis-1,3-Dichloropropene ug/L 49.950 100 72-132
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2130740LABORATORY CONTROL SAMPLE:
LCSSpike
Dibromochloromethane ug/L 51.750 103 78-125
Dibromomethane ug/L 48.550 97 82-120
Ethylbenzene ug/L 46.350 93 79-121
Iodomethane ug/L 92.0100 92 39-154
Methylene Chloride ug/L 47.850 96 64-133
Styrene ug/L 45.850 92 84-126
Tetrachloroethene ug/L 50.650 101 78-122
Toluene ug/L 45.450 91 80-121
trans-1,2-Dichloroethene ug/L 44.450 89 71-127
trans-1,3-Dichloropropene ug/L 49.950 100 69-141
trans-1,4-Dichloro-2-butene ug/L 45.9J50 92 40-160
Trichloroethene ug/L 50.250 100 78-122
Trichlorofluoromethane ug/L 48.050 96 53-137
Vinyl acetate ug/L 94.5100 94 40-160
Vinyl chloride ug/L 46.350 93 58-137
Xylene (Total)ug/L 137150 91 81-126
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%93 70-130
Toluene-d8 (S)%92 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2130741MATRIX SPIKE SAMPLE:
MSSpike
Result
92360777008
1,1,1,2-Tetrachloroethane ug/L 22.320 112 70-130<0.33
1,1,1-Trichloroethane ug/L 21.320 106 70-130<0.48
1,1,2,2-Tetrachloroethane ug/L 20.520 102 70-130<0.40
1,1,2-Trichloroethane ug/L 21.420 107 70-130<0.29
1,1-Dichloroethane ug/L 85.420 71 70-13071.3
1,1-Dichloroethene ug/L 28.820 108 70-1667.2
1,2,3-Trichloropropane ug/L 22.120 111 70-130<0.41
1,2-Dibromo-3-chloropropane ug/L 18.820 94 70-130<2.0
1,2-Dibromoethane (EDB)ug/L 22.320 111 70-130<0.27
1,2-Dichlorobenzene ug/L 20.420 102 70-130<0.30
1,2-Dichloroethane ug/L 20.520 101 70-1300.34J
1,2-Dichloropropane ug/L 21.120 105 70-130<0.27
1,4-Dichlorobenzene ug/L 20.320 101 70-130<0.33
2-Butanone (MEK)ug/L 37.8J40 95 70-130<0.96
2-Hexanone ug/L 40.6J40 102 70-130<0.46
4-Methyl-2-pentanone (MIBK)ug/L 44.0J40 110 70-130<0.33
Acetone ug/L 45.2J40 113 70-130<10.0
Acrylonitrile ug/L 98.8J100 99 70-130<1.9
Benzene ug/L 20.720 103 70-148<0.25
Bromochloromethane ug/L 20.020 100 70-130<0.17
Bromodichloromethane ug/L 19.820 99 70-130<0.18
Bromoform ug/L 20.820 104 70-130<0.26
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 35 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2130741MATRIX SPIKE SAMPLE:
MSSpike
Result
92360777008
Bromomethane ug/L 17.520 87 70-130<0.29
Carbon disulfide ug/L 22.1J20 110 70-130<1.2
Carbon tetrachloride ug/L 20.720 104 70-130<0.25
Chlorobenzene ug/L 21.520 108 70-146<0.23
Chloroethane ug/L 29.020 117 70-1305.5
Chloroform ug/L 19.820 99 70-130<0.14
Chloromethane ug/L 20.320 102 70-130<0.11
cis-1,2-Dichloroethene ug/L 80.8 M1206570-13067.8
cis-1,3-Dichloropropene ug/L 21.120 106 70-130<0.13
Dibromochloromethane ug/L 21.020 105 70-130<0.21
Dibromomethane ug/L 20.220 101 70-130<0.21
Ethylbenzene ug/L 20.520 103 70-130<0.30
Iodomethane ug/L 25.4 M1406470-130<0.32
Methylene Chloride ug/L 18.920 94 70-130<0.97
Styrene ug/L 19.720 99 70-130<0.26
Tetrachloroethene ug/L 22.620 113 70-130<0.46
Toluene ug/L 20.820 104 70-155<0.26
trans-1,2-Dichloroethene ug/L 20.520 102 70-130<0.49
trans-1,3-Dichloropropene ug/L 20.620 103 70-130<0.26
trans-1,4-Dichloro-2-butene ug/L 13.7J M1206870-130<1.0
Trichloroethene ug/L 23.820 109 69-1512.0
Trichlorofluoromethane ug/L 24.120 121 70-130<0.20
Vinyl acetate ug/L 35.5J40 89 70-130<0.35
Vinyl chloride ug/L 24.220 109 70-1302.3
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%95 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92360777009
2130742SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30<0.33
1,1,1-Trichloroethane ug/L ND 30<0.48
1,1,2,2-Tetrachloroethane ug/L ND 30<0.40
1,1,2-Trichloroethane ug/L ND 30<0.29
1,1-Dichloroethane ug/L ND 30<0.32
1,1-Dichloroethene ug/L ND 30<0.56
1,2,3-Trichloropropane ug/L ND 30<0.41
1,2-Dibromo-3-chloropropane ug/L ND 30<2.0
1,2-Dibromoethane (EDB)ug/L ND 30<0.27
1,2-Dichlorobenzene ug/L ND 30<0.30
1,2-Dichloroethane ug/L ND 30<0.24
1,2-Dichloropropane ug/L ND 30<0.27
1,4-Dichlorobenzene ug/L ND 30<0.33
2-Butanone (MEK)ug/L 17.0J 3 3016.4
REPORT OF LABORATORY ANALYSIS
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Page 36 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92360777009
2130742SAMPLE DUPLICATE:
2-Hexanone ug/L 3.7J 303.3J
4-Methyl-2-pentanone (MIBK)ug/L ND 30<0.33
Acetone ug/L 68.2J 1 3067.7
Acrylonitrile ug/L ND 30<1.9
Benzene ug/L ND 30<0.25
Bromochloromethane ug/L ND 30<0.17
Bromodichloromethane ug/L ND 30<0.18
Bromoform ug/L ND 30<0.26
Bromomethane ug/L ND 30<0.29
Carbon disulfide ug/L ND 30<1.2
Carbon tetrachloride ug/L ND 30<0.25
Chlorobenzene ug/L ND 30<0.23
Chloroethane ug/L ND 30<0.54
Chloroform ug/L ND 30<0.14
Chloromethane ug/L ND 30<0.11
cis-1,2-Dichloroethene ug/L ND 30<0.19
cis-1,3-Dichloropropene ug/L ND 30<0.13
Dibromochloromethane ug/L ND 30<0.21
Dibromomethane ug/L ND 30<0.21
Ethylbenzene ug/L ND 30<0.30
Iodomethane ug/L ND 30<0.32
Methylene Chloride ug/L ND 30<0.97
Styrene ug/L ND 30<0.26
Tetrachloroethene ug/L ND 30<0.46
Toluene ug/L ND 30<0.26
trans-1,2-Dichloroethene ug/L ND 30<0.49
trans-1,3-Dichloropropene ug/L ND 30<0.26
trans-1,4-Dichloro-2-butene ug/L ND 30<1.0
Trichloroethene ug/L ND 30<0.47
Trichlorofluoromethane ug/L ND 30<0.20
Vinyl acetate ug/L ND 30<0.35
Vinyl chloride ug/L ND 30<0.62
Xylene (Total)ug/L ND 30<0.66
1,2-Dichloroethane-d4 (S)%102 2100
4-Bromofluorobenzene (S)%100 298
Toluene-d8 (S)%100 2102
REPORT OF LABORATORY ANALYSIS
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The concentration in the Blank QC is less than the reporting limit but greater than 1/2 the reporting limit.1g
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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Page 38 of 42
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92360016
WILKES-GERMANTOWN 356180112
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92360016002 384390 3844329701-DOWNSTREAM EPA 3010A EPA 6010
92360016003 384390 3844329701-FIELD BLANK EPA 3010A EPA 6010
92360016004 384390 3844329701-MW1 EPA 3010A EPA 6010
92360016005 384390 3844329701-MW2 EPA 3010A EPA 6010
92360016006 384390 3844329701-MW3 EPA 3010A EPA 6010
92360016007 384390 3844329701-MW4 EPA 3010A EPA 6010
92360016008 384390 3844329701-MW5 EPA 3010A EPA 6010
92360016009 384390 3844329701-UPSTREAM EPA 3010A EPA 6010
92360016002 384619 3846899701-DOWNSTREAM EPA 3010A EPA 6020B
92360016003 384619 3846899701-FIELD BLANK EPA 3010A EPA 6020B
92360016004 384619 3846899701-MW1 EPA 3010A EPA 6020B
92360016005 384619 3846899701-MW2 EPA 3010A EPA 6020B
92360016006 384619 3846899701-MW3 EPA 3010A EPA 6020B
92360016007 384619 3846899701-MW4 EPA 3010A EPA 6020B
92360016008 384619 3846899701-MW5 EPA 3010A EPA 6020B
92360016009 384619 3846899701-UPSTREAM EPA 3010A EPA 6020B
92360016001 3834799701-TRIP BLANK EPA 8260
92360016002 3834799701-DOWNSTREAM EPA 8260
92360016003 3843979701-FIELD BLANK EPA 8260
92360016004 3834799701-MW1 EPA 8260
92360016005 3834799701-MW2 EPA 8260
92360016006 3834799701-MW3 EPA 8260
92360016007 3834799701-MW4 EPA 8260
92360016008 3834799701-MW5 EPA 8260
92360016009 3834799701-UPSTREAM EPA 8260
REPORT OF LABORATORY ANALYSIS
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Page 39 of 42
Page 40 of 42
Page 41 of 42
Page 42 of 42

Appendix 2
Historical Groundwater Elevations
APPENDIX 2
Summary of Historical Groundwater Elevations
Wilkes County
Germantown Landfill
Permit No. 97-01 Joyce Engineering
MW-1 MW-2 MW-3 MW-4 MW-5
TOC Elevation 1233.00 1177.85 1059.00 1018.00 1045.75
Well Depth 89.69 81.54 64.00 28.21 23.47
Apr-13 1178.75 1131.92 1015.73 1006.25 1036.85
Oct-13 1182.76 1130.85 1016.00 1005.30 1036.17
Apr-14 1182.86 1131.85 1016.20 1006.75 1037.05
Oct-14 1180.81 1129.79 1015.49 1004.49 1036.40
Apr-15 1178.96 1130.81 1015.51 1005.07 1036.59
Oct-15 1177.15 1131.00 1013.10 1004.15 1035.80
Apr-16 1187.15 1132.85 1016.79 1006.45 1036.34
Oct-16 1180.12 1129.75 1015.20 1003.50 1034.97
Apr-17 1175.28 1129.20 1014.50 1002.86 1034.94
Oct-17 1174.95 1129.65 1014.60 1003.80 1036.20
Notes:
TOC = Top of Casing
Location

Appendix 3
Historically Detected Constituents
APPENDIX 3
Summary of Historically Detected Constituents
Wilkes County Germantown Landfill
Permit No. 97-01 page 1 of 13 Joyce Engineering
Analyte DL QL MW-1 MW-2 MW-3 MW-4 MW-5 Upstream Downstream Outfall #1 Outfall #2 Blanks
INORGANICS
Antimony 28-Nov-07 1.2 6.0 ND ND 3.1 J ND (2.8 J)ND ND ND 1.7 J ---ND
GWPS = 1.4 µg/L (10/23/07)21-Apr-08 1.2 6.0 1.2 B ND 1.2 B ND (ND)ND 4.1 B ND 1.9 B ---1.3 J
NC 2B = NE (05/01/07)22-Dec-08 1.2 6.0 ND 1.3 J 3.7 (ND)J ND ND ND 1.5 J ND ---ND
23-Jun-09 1.2 6.0 5.9 J 2.3 (5.3 J)J ND ND ND 2.5 J 2.9 J 3.6 J ---ND
15-Dec-09 1.2 6.0 ND 2.3 B 3.9 B ND (3.4 B)1.8 B 2.2 B ND 4.6 B ---3.5 J
28-Jun-10 1.2 6.0 ND 2.0 B 2.5 B ND 1.2 (ND) B 6.6 B ND ND ---2.2 J
GWPS = 1 µg/L (8/1/10)02-Nov-10 1.2 6.0 ND ND 2.4 (ND)J 3.5 J 3.1 J ND 2.5 J ND ---ND
12-Apr-11 2.6 6.0 ND ND ND ND ND ND ND ND ---ND
18-Oct-11 5.0 6.0 ND ND ND ND ND ND ND ------ND
10-Apr-12 5.0 6.0 ND ND ND ND ND ND ND ------ND
15-Oct-12 5.0 6.0 ND ND ND ND ND ND ND ------ND
16-Apr-13 5.0 6.0 ND ND ND ND ND ND ND ND ---ND
08-Oct-13 5.0 6.0 ND ND ND ND ND ND ND ------ND
29-Apr-14 5.0 6.0 ND ND ND ND ND ND ND ------ND
14-Oct-14 5.0 6.0 ND ND ND ND ND ND ND ------ND
09-Apr-15 3.8 6.0 ND ND ND ND ND ND ND ------ND
27-Oct-15 3.8 6.0 ND ND ND 4.2 J ND ND ND ND ---ND
21-Apr-16 0.069 6.0 ND 0.23 J 0.61 J 0.31 J 0.25 J 0.12 J 0.10 J ------ND
11-Oct-16 3.8 6.0 ND ND ND ND ND ND ND ------ND
18-Apr-17 3.9 6.0 ND ND ND ND ND ND ND ------ND
19-Oct-17 3.9 6.0 ND ND ND ND ND ND ND ------ND
Arsenic 19-Jun-07 5.5 10.0 ND ND 8.2 J ND ND (ND)7.7 J ND ND ---ND
NC 2L = 50 µg/L (10/23/07)28-Nov-07 5.5 10.0 ND ND ND ND (ND)ND ND ND ND ---ND
NC 2B = 50 µg/L (05/01/07)21-Apr-08 5.5 10.0 ND ND ND ND (ND)ND ND ND ND ---ND
22-Dec-08 5.5 10.0 ND ND ND (ND)ND ND ND ND ND ---ND
23-Jun-09 5.5 10.0 ND 6.3 (ND)J ND ND ND ND ND ND ---ND
15-Dec-09 5.5 10.0 ND ND ND ND (ND)ND ND ND ND ---ND
NC 2L = 10 µg/L (01/01/10)28-Jun-10 5.5 10.0 ND 6.1 J ND ND ND (ND)ND ND ND ---ND
02-Nov-10 5.5 10.0 ND ND ND (ND)ND ND ND ND ND ---ND
12-Apr-11 2.7 10.0 ND ND ND ND 6.9 J ND ND ND ---ND
18-Oct-11 5.0 10.0 ND ND ND ND ND ND ND ------ND
10-Apr-12 5.0 10.0 ND ND ND ND ND ND ND ------ND
15-Oct-12 5.0 10.0 ND ND ND ND ND ND ND ------ND
16-Apr-13 5.0 10.0 ND ND ND ND 7.8 J ND ND ND ---ND
08-Oct-13 5.0 10.0 ND ND ND 5.3 J ND ND ND ------ND
29-Apr-14 5.0 10.0 ND ND ND ND ND ND ND ------ND
14-Oct-14 5.0 10.0 ND ND ND ND ND ND ND ------ND
09-Apr-15 2.5 10.0 ND ND ND ND ND ND ND ------ND
27-Oct-15 2.5 10.0 ND ND ND ND 4.3 J ND ND 2.8 J ---ND
21-Apr-16 0.29 10.0 0.76 J ND ND 0.62 J 2.5 J ND ND ------ND
11-Oct-16 2.5 10.0 ND ND ND 3.5 J 3.8 J ND ND ------ND
18-Apr-17 5.0 10.0 ND ND ND ND ND ND ND ------ND
19-Oct-17 5.0 10.0 ND ND ND ND ND ND ND ------ND
Barium Apr-93 ---10 177 220 159 ND 121 ND 166 5600 799 ---
Sep-93 ---250 ND 1940 ND ND ND ND ND ---------
Apr-94 ---250 ND ND ND ND ND ND ND ND ND ---
Oct-94 ---500 ND ND ND ND ND ND ND ND 567 ---
Apr-95 ---500 ND ND ND ND ND ND ND ND ------
Nov-95 ---500 ND ND ND ND ND ND ND ND ------
May-96 ---500 ND ND ND ND ND ND ND ND ------
Nov-96 ---500 ND ND ND ND 1040 ND ND ND ---ND
Mar-97 ---500 ND ND ND ND 531 ND ND ND ---ND
Sep-97 ---500 ND ND ND ND ND ND ND ND ---ND
Mar-98 ---500 ND ND ND ND 520 ND ND ND ---ND
Sep-98 ---500 ND ND ND ND ND ND ND ND ---ND
Mar-99 ---500 ND ND ND ND ND ND ND ND ---ND
Sep-99 ---500 ND ND ND ND 549 ND ND ND ---ND
May-00 ---500 ND ND ND ND ND ND ND ND ---ND
Oct-00 ---500 ND ND ND ND 507 ND ND ND ---ND
Mar-01 ---500 ND ND ND ND ND ND ND ND ---ND
Oct-01 ---500 ND ND ND ND 566 ND ND ND ---ND
Apr-02 ---500 ND ND ND ND ND ND ND ND ---ND
Nov-02 ---500 ND ND ND ND 500 ND ND ND ---ND
May-03 ---500 ND ND ND ND ND ND ND ND ---ND
Nov-03 ---500 ND ND ND ND ND(517)ND ND ND ---ND
Apr-04 ---500 ND ND ND ND ND ND ND ND ---ND
Oct-04 ---500 ND ND ND ND ND ND ND ND ---ND
May-05 ---500 ND ND ND ND ND ND ND ND ---ND
Oct-05 ---500 ND ND ND ND ND ND ND ND ---ND
23-May-06 ---500 ND ND ND ND ND ND ND ND ---ND
09-Nov-06 ---500 ND ND ND ND ND ND ND ND ---ND
19-Jun-07 1.1 100 94.9 J 13.3 B 12.2 B 82.3 J 520 (462)23.6 B 23.1 B 364 ---13.5 J
NC 2L = 2,000 µg/L (10/23/07)28-Nov-07 1.1 100 380 43.5 J 10.9 B 128 (109)458 19.7 J 34.7 J 151 ---2.51 J
NC 2B = NE (05/01/07)21-Apr-08 1.1 100 101 20.4 B 12.1 B 90.0 (98 J)J 417 19.5 B 27.9 B 177 ---9.7 J
22-Dec-08 1.1 100 95.0 J 9.1 J 8.5 (16.6 J)J 77.6 J 414 20.0 J 21.3 J 132 ---1.6 J
23-Jun-09 1.1 100 168 4.8 (6.1 B)B 13.1 B 65.4 B 440 19.8 B 19.5 B 294 ---8.5 J
15-Dec-09 1.1 100 168 7.6 B 18.1 B 68.6 (64.6 B)B 400 22.2 B 19.7 B 138 ---18.2 J
NC 2L = 700 µg/L (01/01/10)28-Jun-10 1.1 100 81.1 J 4.6 B 7.5 B 45.6 J 325 (362)18.1 19.6 234 ---2.0 J
02-Nov-10 1.1 100 157 6.2 B 9.1 (9.2 B)B 51.0 B 318 17.7 B 23.8 B 170 ---10.9 J
12-Apr-11 0.20 100 106 9.6 B 16.2 B 79.4 J 433 19.3 B 18.2 B 39.8 B ---13.2 J
18-Oct-11 5.0 100 133 11.5 J 9.4 J 113 517 19.6 J 20.4 J ------ND
10-Apr-12 5.0 100 122 9.1 B 8.7 B 94.1 J 328 17.6 B 17.2 B ------15.8 J
15-Oct-12 5.0 100 123 5.3 J 8.8 J 72.9 J 359 25.4 J 19.9 J ------ND
16-Apr-13 5.0 100 168 6.6 J 8.0 J 51.9 372 17.6 J 17.6 J 306 ---ND
08-Oct-13 5.0 100 122 5.8 J 8.2 J 71.6 J 393 21.8 J 23.0 J ------ND
29-Apr-14 5.0 100 92.0 J 5.3 J 7.7 J 60.1 J 415 25.4 J 27.3 J ------ND
14-Oct-14 5.0 100 111 6.9 J 8.6 J 82.0 J 377 20.4 J 19.9 J ------ND
09-Apr-15 2.5 100 128 8.0 J 8.6 J 70.6 J 327 18.3 J 54.7 J ------ND
27-Oct-15 2.5 100 116 11.3 J 8.2 J 84.8 J 325 25.3 J 30.0 J 132 ---ND
21-Apr-16 0.041 100 97 J 7.5 J 8.2 J 67 J 360 16 J 18 J ------0.65 J
11-Oct-16 2.5 100 90.1 J 13.5 J 8.6 J 154 395 18.6 J 18.8 J ------ND
18-Apr-17 2.5 100 101 9.9 J 9.2 J 85.4 J 412 18.8 J 17.7 J ------ND
19-Oct-17 2.5 100 115 10.9 J 10.2 J 93.5 J 442 22.7 J 22.7 J ------ND
Sample Collection
Date
APPENDIX 3
Summary of Historically Detected Constituents
Wilkes County Germantown Landfill
Permit No. 97-01 page 2 of 13 Joyce Engineering
Analyte DL QL MW-1 MW-2 MW-3 MW-4 MW-5 Upstream Downstream Outfall #1 Outfall #2 Blanks
Sample Collection
Date
Beryllium May-96 ---2 3 6 4 4 4 4 4 5 ------
Nov-96 ---2 ND ND ND ND 6 ND ND ND ---ND
Mar-97 ---2 ND ND ND 2 4 ND ND ND ---ND
Sep-97 ---2 ND ND ND ND ND ND ND ND ---ND
Mar-98 ---2 ND ND 6 ND 13 ND ND ND ---ND
Sep-98 ---2 ND ND ND 2 8 ND ND 7 ---ND
Mar-99 ---2 ND ND ND 3 9 ND ND ND ---ND
Sep-99 ---2 ND ND ND ND ND ND ND ND ---ND
May-00 ---2 ND ND ND ND ND ND ND ND ---ND
Oct-00 ---2 ND ND ND ND ND ND ND ND ---ND
Mar-01 ---2 ND ND ND ND ND ND ND ND ---ND
Oct-01 ---2 ND ND ND ND ND ND ND ND ---ND
Apr-02 ---2 ND ND ND ND ND ND ND ND ---ND
Nov-02 ---2 ND ND ND ND ND ND ND ND ---ND
May-03 ---2 ND ND ND ND ND ND ND ND ---ND
Nov-03 ---2 ND ND ND ND ND ND ND ND ---ND
Apr-04 ---2 ND ND ND ND ND ND ND ND ---ND
Oct-04 ---2 ND ND ND ND ND ND ND ND ---ND
May-05 ---2 ND ND ND ND ND ND ND ND ---ND
Oct-05 ---2 ND ND ND ND ND ND ND ND ---ND
23-May-06 ---2 ND ND ND ND ND ND ND ND ---ND
09-Nov-06 ---2 ND ND ND ND ND ND ND ND ---ND
19-Jun-07 0.2 1.0 ND ND ND ND ND (ND)ND ND ND ---ND
GWPS = 4 µg/L (10/23/07)28-Nov-07 0.2 1.0 ND ND 0.6 B ND (0.21 B)ND ND ND ND ---0.2 J
NC 2B = 6.5 µg/L (05/01/07)21-Apr-08 0.2 1.0 0.3 J ND 0.2 J 0.4 (ND)J 0.2 J ND ND ND ---ND
22-Dec-08 0.2 1.0 ND 0.8 J ND (ND)ND ND ND ND ND ---ND
23-Jun-09 0.2 1.0 ND ND (ND)ND ND ND ND ND ND ---ND
15-Dec-09 0.2 1.0 ND ND ND ND (ND)ND ND ND ND ---ND
28-Jun-10 0.2 1.0 ND ND ND ND ND (ND)ND ND ND ---ND
02-Nov-10 0.2 1.0 0.2 J 0.3 J ND (ND)0.4 J 0.3 J 0.2 J 1.8 0.2 J ---ND
12-Apr-11 0.10 1.0 ND ND ND ND 0.48 B ND ND 0.64 B ---0.28 J
18-Oct-11 1.0 1.0 ND ND ND ND ND ND ND ------ND
10-Apr-12 1.0 1.0 ND ND ND ND ND ND ND ------ND
15-Oct-12 1.0 1.0 ND ND ND ND ND ND ND ------ND
16-Apr-13 1.0 1.0 ND ND ND ND ND ND ND ND ---ND
08-Oct-13 1.0 1.0 ND ND ND ND ND ND ND ------ND
29-Apr-14 1.0 1.0 ND ND ND ND 1.3 ND ND ------ND
14-Oct-14 1.0 1.0 ND ND ND ND ND ND ND ------ND
09-Apr-15 0.5 1.0 ND ND ND ND ND ND ND ------ND
27-Oct-15 0.5 1.0 ND ND ND ND ND ND ND ND ---ND
21-Apr-16 0.047 1.0 ND ND ND 0.087 J 0.18 J ND ND ------ND
11-Oct-16 0.5 1.0 ND ND ND 0.57 J ND ND ND ------ND
18-Apr-17 0.5 1.0 ND ND ND ND ND ND ND ------ND
19-Oct-17 0.5 1.0 ND ND ND ND ND ND ND ------ND
Cadmium Apr-93 ---2 ND 6 2.1 2 5 2 2 2.3 2.8 ---
Sep-93 ---2 ND 2.1 ND ND ND ND ND ---------
Apr-94 ---2 ND ND ND ND ND ND ND ND ND ---
Apr-95 ---1 ND ND ND ND ND ND ND ND ------
Nov-95 ---1 ND ND ND 1 ND ND ND ND ------
May-96 ---1 1 10 ND ND ND 1 ND 4 ------
Nov-96 ---1 ND 4 1 1 23 ND ND ND ---ND
Mar-97 ---1 ND ND 1 3 18 ND ND ND ---ND
Sep-97 ---1 1 2 4 15 ND ND ND ---ND
Mar-98 ---1 ND ND 2 ND 5 ND ND ND ---ND
Oct-94 ---1 ND ND 1 ND ND ND ND ND ND ---
Sep-98 ---1 ND ND ND (ND)1 4 ND ND 3 ---ND
Mar-99 ---1 ND ND ND (ND)ND 2 ND ND ND ---ND
Sep-99 ---1 ND ND ND ND ND ND ND ND ---ND
May-00 ---1 ND ND ND (ND)ND ND ND ND ND ---ND
Oct-00 ---1 1 ND ND 2(1)6 1 ND 1 ---ND
Mar-01 ---1 ND ND (ND)ND 1 4 ND ND ND ---ND
Oct-01 ---1 ND ND ND ND (ND)ND ND ND ND ---ND
Apr-02 ---1 ND 2 ND ND (ND)1 ND ND ND ---ND
Nov-02 ---1 ND ND ND (ND)1 ND ND ND ND ---ND
May-03 ---1 ND ND ND ND (ND)ND ND ND ND ---ND
Nov-03 ---1 ND ND ND ND ND (ND)ND ND ND ---ND
Apr-04 ---1 ND 1 ND (ND)ND ND ND ND ND ---ND
Oct-04 ---1 ND ND (ND)ND ND ND ND ND ND ---ND
May-05 ---1 ND ND (ND)ND ND ND ND ND ND ---ND
Oct-05 ---1 ND ND ND ND ND (ND)ND ND ND ---ND
23-May-06 ---1 ND ND (ND)ND 1 6 ND 1 2 ---ND
09-Nov-06 ---1 ND ND ND ND (ND)ND ND ND ND ---ND
19-Jun-07 0.2 1.0 1.6 B 1.8 B 1.0 B 2.4 B 10.2 (8.1)1.3 B 0.9 B 5.9 ---0.7 J
NC 2L = 1.75 µg/L (10/23/07)28-Nov-07 0.2 1.0 0.25 J 0.4 J 0.5 J 0.65 (6.0)3.1 J ND ND 0.86 J ---ND
NC 2B = 2 µg/L (05/01/07)21-Apr-08 0.2 1.0 0.5 J 0.3 J 0.4 J ND (ND)ND ND ND ND ---ND
22-Dec-08 0.2 1.0 0.96 B 1.0 B ND (ND)ND ND ND ND ND ---0.8 J
23-Jun-09 0.2 1.0 0.6 J 0.5 (ND)J ND ND 0.3 J ND ND ND ---ND
15-Dec-09 0.2 1.0 ND 0.8 J ND ND (ND)ND 0.5 J ND ND ---ND
NC 2L = 2 µg/L (01/01/10)28-Jun-10 0.2 1.0 0.4 J 0.2 J 0.3 J 0.6 J 4.5 (4.8)0.3 J ND 2.6 ---ND
02-Nov-10 0.2 1.0 0.5 J 0.4 J ND (1.2)1.0 8.8 0.4 J 0.3 J 0.9 J ---ND
12-Apr-11 0.50 1.0 ND ND ND ND ND ND ND 0.59 J ---ND
18-Oct-11 1.0 1.0 ND ND ND ND ND ND ND ------ND
10-Apr-12 1.0 1.0 ND ND ND ND ND ND ND ------ND
15-Oct-12 1.0 1.0 ND ND ND ND ND ND ND ------ND
16-Apr-13 1.0 1.0 ND ND ND ND 1.7 ND ND ND ---ND
08-Oct-13 1.0 1.0 ND ND ND ND ND ND ND ------ND
29-Apr-14 1.0 1.0 ND ND ND ND 1.3 ND ND ------ND
14-Oct-14 1.0 1.0 ND ND ND ND ND ND ND ------ND
09-Apr-15 0.5 1.0 ND ND ND ND ND ND ND ------ND
27-Oct-15 0.5 1.0 ND 2.4 ND ND 0.75 J ND ND ND ---ND
21-Apr-16 0.019 1.0 0.24 B 0.26 B 0.14 B 0.23 B 0.17 B 0.11 B 0.084 B ------0.068 J
11-Oct-16 0.5 1.0 ND ND ND ND ND ND ND ------ND
18-Apr-17 0.5 1.0 ND ND ND ND ND ND ND ------ND
19-Oct-17 0.5 1.0 ND ND ND ND ND ND ND ------ND
APPENDIX 3
Summary of Historically Detected Constituents
Wilkes County Germantown Landfill
Permit No. 97-01 page 3 of 13 Joyce Engineering
Analyte DL QL MW-1 MW-2 MW-3 MW-4 MW-5 Upstream Downstream Outfall #1 Outfall #2 Blanks
Sample Collection
Date
Chromium Apr-93 ---40 ND 140 ND ND ND ND ND ND ND ---
Sep-93 ---20 ND 673 ND ND ND ND ND ND ------
Apr-94 ---20 ND 31 ND ND ND ND ND ND ND ---
Oct-94 ---10 ND ND ND ND ND ND ND ND 16 ---
Apr-95 ---10 ND ND ND ND ND ND ND ND ------
Nov-95 ---10 ND ND ND ND ND ND ND ND ------
May-96 ---10 ND 118 11 ND ND ND ND ND ------
Nov-96 ---10 ND 48 12 ND 154 ND ND ND ---ND
Mar-97 ---10 ND ND 10 ND 38 ND ND ND ---ND
Sep-97 ---10 ND 17 26 ND 11 ND ND ND ---ND
Mar-98 ---10 ND ND 25 ND 16 ND ND ND ---ND
Sep-98 ---10 ND ND ND 12 17 ND ND ND ---ND
Mar-99 ---10 ND ND ND ND ND ND ND ND ---ND
Sep-99 ---10 ND ND ND ND 36 ND ND ND ND ND
May-00 ---10 ND ND ND ND ND ND ND ND ---ND
Oct-00 ---10 ND ND ND ND 11 ND ND ND ---ND
Mar-01 ---10 ND ND ND ND ND ND ND ND ---ND
Oct-01 ---10 ND ND ND ND 27 ND ND ND ---ND
Apr-02 ---10 ND ND ND ND ND ND ND ND ---ND
Nov-02 ---10 ND ND ND ND ND ND ND ND ---ND
May-03 ---10 ND ND ND ND ND ND ND ND ---ND
Nov-03 ---10 ND ND ND ND 12(14)ND ND ND ---ND
Apr-04 ---10 ND ND ND ND ND ND ND ND ---ND
Oct-04 ---10 ND ND ND ND ND ND ND ND ---ND
May-05 ---10 ND ND ND ND ND ND ND ND ---ND
Oct-05 ---10 ND ND ND ND ND ND ND ND ---ND
23-May-06 ---10 ND ND ND ND 12 ND ND ND ---ND
09-Nov-06 ---10 ND ND ND ND ND ND ND ND ---ND
19-Jun-07 0.7 10.0 2.4 B 1.0 B 1.4 B 5.3 B 17.9 B (6.2 B)3.8 B 4.9 B ND ---6.1 J
NC 2L = 50 µg/L (10/23/07)28-Nov-07 0.7 10.0 1.8 J 3.3 J 1.3 J 9.0 (19.7)J 4.3 J ND 0.76 J 10.8 ---ND
NC 2B = 50 µg/L (05/01/07)21-Apr-08 0.7 10.0 2.1 J ND ND 5.6 (ND)J ND ND ND ND ---ND
22-Dec-08 0.7 10.0 1.1 J 2.2 J ND (1.2 J)7.6 J 7.2 J ND ND 1.9 J ---ND
23-Jun-09 0.7 10.0 2.5 J 1.4 (ND)J 1.1 J 2.0 J 5.6 J 1.0 J 0.8 J 1.0 J ---ND
15-Dec-09 0.7 10.0 2.4 J 4.7 J 0.8 J 2.2 (1.9 J)J 8.0 J 3.6 J ND 1.7 J ---ND
NC 2L = 10 µg/L (01/01/10)28-Jun-10 0.7 10.0 ND 1.4 J ND ND ND (ND)ND ND ND ---ND
02-Nov-10 0.7 10.0 1.6 J ND ND (ND)2.3 J ND ND ND 1.4 J ---ND
12-Apr-11 0.40 10.0 ND 4.1 J 1.1 J 1.7 J 12.2 0.60 J 0.80 J 1.6 J ---ND
18-Oct-11 5.0 10.0 ND 5.4 J ND 9.4 J 19.5 ND ND ------ND
10-Apr-12 5.0 10.0 ND ND ND 6.4 J ND ND ND ------ND
15-Oct-12 5.0 10.0 ND ND ND ND ND ND ND ------ND
16-Apr-13 5.0 10.0 ND ND ND ND ND ND ND 5.6 J ---ND
08-Oct-13 5.0 10.0 ND ND 8.6 J ND ND ND ND ------ND
29-Apr-14 5.0 10.0 ND ND ND ND 16.3 ND ND ------ND
14-Oct-14 5.0 10.0 ND ND ND ND ND 10.7 5.4 J ------ND
09-Apr-15 2.5 10.0 ND ND ND 4.0 J 2.7 J ND 5.7 J ------ND
27-Oct-15 2.5 10.0 ND ND ND ND 9.3 J ND ND 4.5 J ---ND
21-Apr-16 0.51 10.0 ND ND ND 0.52 J 3.1 J ND ND ------ND
11-Oct-16 2.5 10.0 ND ND ND 16.4 8.9 J ND ND ------ND
18-Apr-17 2.5 10.0 ND ND ND ND 5.1 J ND ND ------ND
19-Oct-17 2.5 10.0 ND ND ND ND ND ND ND ------ND
APPENDIX 3
Summary of Historically Detected Constituents
Wilkes County Germantown Landfill
Permit No. 97-01 page 4 of 13 Joyce Engineering
Analyte DL QL MW-1 MW-2 MW-3 MW-4 MW-5 Upstream Downstream Outfall #1 Outfall #2 Blanks
Sample Collection
Date
Cobalt Oct-94 ---10 ND ND ND 18 ND ND ND ND 24 ---
Apr-95 ---10 ND ND ND ND ND ND ND 10 ------
Nov-95 ---10 ND ND ND ND ND ND ND ND ------
May-96 ---10 ND 34 ND 21 ND ND ND 13 ------
Nov-96 ---10 ND 11 ND 18 86 ND ND ND ---ND
Mar-97 ---10 ND ND ND 20 44 ND ND ND ---ND
Sep-97 ---10 ND ND 0.014 31 27 ND ND ND ---ND
Mar-98 ---10 ND ND 34 18 37 ND ND ND ---ND
Sep-98 ---10 ND ND ND 26 30 ND ND 12 ---ND
Mar-99 ---10 ND ND ND 16 25 ND ND ND ---ND
Sep-99 ---10 ND ND ND 17 33 ND ND ND ---ND
May-00 ---10 ND ND ND 18 32 ND ND ND ---ND
Oct-00 ---10 ND ND ND 23(22)32 ND ND ND ---ND
Mar-01 ---10 ND ND ND 18 24 ND ND ND ---ND
Oct-01 ---10 ND ND 20 20(20)35 ND ND ND ---ND
Apr-02 ---10 ND ND ND 11(12)25 ND ND ND ---ND
Nov-02 ---10 ND ND ND 20 28 ND ND ND ---ND
May-03 ---10 ND ND ND 19(19)22 ND ND ND ---ND
Nov-03 ---10 ND ND ND 16 28(29)ND ND ND ---ND
Apr-04 ---10 ND ND ND 13 23 ND ND 12 ---ND
Oct-04 ---10 ND ND ND 14 19 ND ND ND ---ND
May-05 ---10 ND ND ND 11 23 ND ND 11 ---ND
Oct-05 ---10 ND ND ND 19 19(20)ND ND ND ---ND
23-May-06 ---10 ND ND ND 15 24 ND ND 10 ---ND
09-Nov-06 ---10 ND ND ND 16(15)19 ND ND ND ---ND
19-Jun-07 0.7 10.0 ND ND ND 14.8 28.2 (23.8)ND ND 10.6 ---ND
GWPS = 70 µg/L (10/23/07)28-Nov-07 0.7 10.0 ND 0.8 J ND 19.4 (15.3)18.8 ND ND ND ---ND
NC 2B = NE (05/01/07)21-Apr-08 0.7 10.0 1.5 1.0 J 0.8 J 13.8 (12.6)21.7 ND ND 6.1 J ---ND
22-Dec-08 0.7 10.0 ND 1.9 J ND (ND)12.7 20.8 ND ND 4.1 J ---ND
23-Jun-09 0.7 10.0 4.0 J ND (ND)ND 8.7 J 20.1 ND ND 9.9 J ---ND
15-Dec-09 0.7 10.0 3.2 J 1.7 J ND 12.0 (11.6)18.8 ND ND 4.7 J ---ND
28-Jun-10 0.7 10.0 ND ND ND 5.8 J 15.6 (16.4)ND ND 8.5 J ---ND
GWPS = 1 µg/L (10/1/10)02-Nov-10 0.7 10.0 3.5 J ND ND (ND)13.9 13.9 ND ND 5.6 J ---ND
12-Apr-11 0.60 10.0 1.5 B 1.9 B 2.2 B 12.4 8.8 J 2.5 B ND 1.4 B ---1.1 J
18-Oct-11 5.0 10.0 ND ND ND 25.0 64.5 ND ND ------ND
10-Apr-12 5.0 10.0 ND ND ND 13.1 23.2 ND ND ------ND
15-Oct-12 5.0 10.0 ND ND ND 9.5 J ND ND ND ------ND
16-Apr-13 5.0 10.0 13.0 ND ND 7.8 J 95.1 ND ND 14.1 ---ND
08-Oct-13 5.0 10.0 8.4 J ND ND 17.7 102 ND ND ------ND
29-Apr-14 5.0 10.0 ND ND ND 6.8 J ND ND ND ------ND
14-Oct-14 5.0 10.0 ND ND ND 11.4 11.5 ND ND ------ND
09-Apr-15 2.5 10.0 ND ND ND 9.8 J 13.7 ND ND ------ND
27-Oct-15 2.5 10.0 2.8 J ND ND 12.1 11.7 ND ND 5.8 J ---ND
21-Apr-16 0.013 10.0 4.3 J 0.10 J 0.065 J 11 17 0.13 J 0.20 J ------ND
11-Oct-16 2.5 10.0 ND ND ND 23.6 18.0 ND ND ------ND
18-Apr-17 2.5 10.0 ND ND ND 13.3 15.4 ND ND ------ND
19-Oct-17 2.5 10.0 ND ND ND 13.5 14.1 ND ND ------ND
APPENDIX 3
Summary of Historically Detected Constituents
Wilkes County Germantown Landfill
Permit No. 97-01 page 5 of 13 Joyce Engineering
Analyte DL QL MW-1 MW-2 MW-3 MW-4 MW-5 Upstream Downstream Outfall #1 Outfall #2 Blanks
Sample Collection
Date
Copper Apr-93 ---20 ND ND ND ND ND ND ND 263 ND ---
Sep-93 ---10 ND 138 ND ND ND ND ND ---------
Apr-94 ---10 ND ND ND ND ND ND ND ND ND ---
Oct-94 ---200 ND ND ND ND ND ND ND ND ND ---
Apr-95 ---200 ND ND ND ND ND ND ND ND ------
Nov-95 ---200 ND ND ND ND ND ND ND ND ------
May-96 ---200 ND ND ND ND ND ND ND ND ------
Nov-96 ---200 ND ND ND ND 114 ND ND ND ---ND
Mar-97 ---200 ND ND ND ND ND ND ND ND ---ND
Sep-97 ---200 ND ND ND ND ND ND ND ND ---ND
Mar-98 ---200 ND ND ND ND ND ND ND ND ---ND
Sep-98 ---10 ND ND ND ND ND ND ND ND ---ND
Mar-99 ---10 ND ND ND ND ND ND ND ND ---ND
Sep-99 ---200 ND ND ND ND ND ND ND ND ---ND
May-00 ---200 ND ND ND ND ND ND ND ND ---ND
Oct-00 ---200 ND ND ND ND ND ND ND ND ---ND
Mar-01 ---200 ND ND ND ND ND ND ND ND ---ND
Oct-01 ---200 ND ND ND ND ND ND ND ND ---ND
Apr-02 ---200 ND ND ND ND ND ND ND ND ---ND
Nov-02 ---200 ND ND ND ND ND ND ND ND ---ND
May-03 ---200 ND ND ND ND ND ND ND ND ---ND
Nov-03 ---200 ND ND ND ND ND ND ND ND ---ND
Apr-04 ---200 ND ND ND ND ND ND ND ND ---ND
Oct-04 ---200 ND ND ND ND ND ND ND ND ---ND
May-05 ---200 ND ND ND ND ND ND ND ND ---ND
Oct-05 ---200 ND ND ND ND ND ND ND ND ---ND
23-May-06 ---200 ND ND ND ND ND ND ND ND ---ND
09-Nov-06 ---200 ND ND ND ND ND ND ND ND ---ND
19-Jun-07 2.0 10.0 2.6 B 2.8 B 2.8 B 15.5 B 15.6 (10.9 B)B 8.6 B 4.0 B ND ---5.1
NC 2L = 1,000 µg/L (10/23/07)28-Nov-07 2.0 10.0 ND 5.7 B 3.2 B 30.5 (24.4)ND 3.7 B 2.8 B 3.3 B ---2.5 J
NC 2B = 7 µg/L (05/01/07)21-Apr-08 2.0 10.0 2.3 B ND ND 20.6 (22.0 B)B 7.4 B ND ND 6.6 B ---7.0 J
22-Dec-08 2.0 10.0 ND 2.4 J 3.8 (ND)J 2.7 J ND ND ND ND ---ND
23-Jun-09 2.0 10.0 ND ND (ND)ND 5.5 J 4.4 J 1.3 J ND ND ---ND
15-Dec-09 2.0 10.0 ND 2.4 B ND 5.9 (3.8 B)B 2.9 B ND ND ND ---2.7 J
NC 2L = 1,000 µg/L (01/01/10)28-Jun-10 2.0 10.0 ND ND ND 2.0 J 1.3 (2.3 J)J ND ND ND ---ND
02-Nov-10 2.0 10.0 ND ND ND (7.4 J)ND ND ND ND ND ---ND
12-Apr-11 0.30 10.0 0.52 B 4.8 J 3.4 B 5.0 J 10.3 1.0 B 0.94 B 2.5 B ---0.92 J
18-Oct-11 5.0 10.0 ND ND ND 36.5 14.2 ND ND ------ND
10-Apr-12 5.0 10.0 ND ND ND 26.0 ND ND ND ------ND
15-Oct-12 5.0 10.0 ND ND ND ND ND ND ND ------ND
16-Apr-13 5.0 10.0 ND ND ND 5.6 J ND ND ND 11.3 ---ND
08-Oct-13 5.0 10.0 ND ND ND ND ND ND ND ------ND
29-Apr-14 5.0 10.0 ND ND ND 11.2 ND ND ND ------ND
14-Oct-14 5.0 10.0 ND ND ND 10.6 5.3 J ND ND ------ND
09-Apr-15 2.5 10.0 ND 4.0 J ND 17.6 6.0 J ND 4.6 J ------3.2 J
27-Oct-15 2.5 10.0 ND ND ND ND 14.8 ND 2.5 J 12.4 ---ND
21-Apr-16 0.44 10.0 0.48 J 6.8 J 1.4 J 4.9 J 2.9 J 0.58 J 0.65 J ------ND
11-Oct-16 2.5 10.0 ND 3.0 J ND 58.7 6.0 J ND ND ------ND
18-Apr-17 2.5 10.0 ND ND ND ND ND ND ND ------ND
19-Oct-17 2.5 10.0 ND ND ND 9.6 J 3.3 J ND ND ------ND
APPENDIX 3
Summary of Historically Detected Constituents
Wilkes County Germantown Landfill
Permit No. 97-01 page 6 of 13 Joyce Engineering
Analyte DL QL MW-1 MW-2 MW-3 MW-4 MW-5 Upstream Downstream Outfall #1 Outfall #2 Blanks
Sample Collection
Date
Lead Apr-93 ---5 ND 497 22 ND 18.1 ND ND 163 ND ---
Sep-93 ---5 ND 224 16 5 ND ND ND ---------
Apr-94 ---5 ND 14.2 6 13 6 ND ND ND ND ND
Oct-94 ---10 ND ND ND ND ND ND ND ND ND ---
Apr-95 ---10 ND ND 11 ND ND ND ND ND ------
Nov-95 ---10 ND ND 13 ND ND ND ND ND ------
May-96 ---10 ND 41 21 11 ND ND ND ND ------
Nov-96 ---10 ND 20 22 ND 96 ND ND ND ---ND
Mar-97 ---10 ND ND 19 ND 37 ND ND ND ---ND
Sep-97 ---10 ND 12 51 ND 12 ND 19 ND ---ND
Mar-98 ---10 ND ND 130 ND 30 ND ND ND ---ND
Sep-98 ---10 ND ND ND 11 14 ND ND ND ---ND
Mar-99 ---10 ND ND ND ND 8 ND ND ND ---ND
Sep-99 ---10 ND ND ND ND ND ND ND ND ---ND
May-00 ---10 ND ND ND ND ND ND ND ND ---ND
Oct-00 ---10 ND ND ND 18(10)15 ND ND ND ---ND
Mar-01 ---10 ND ND ND ND ND ND ND ND ---ND
Oct-01 ---10 ND ND ND ND 19 ND ND ND ---ND
Apr-02 ---10 ND ND ND ND ND ND ND ND ---ND
Nov-02 ---10 ND ND ND ND 16 ND ND ND ---ND
May-03 ---10 ND ND ND ND ND ND ND ND ---ND
Nov-03 ---10 ND ND ND ND 16(20)ND ND ND ---ND
Apr-04 ---10 ND ND ND ND ND ND ND ND ---ND
Oct-04 ---10 ND ND ND ND ND ND ND 13 ---ND
May-05 ---10 ND ND ND ND ND ND ND ND ---ND
Oct-05 ---10 ND ND ND ND ND ND ND ND ---ND
23-May-06 ---10 ND ND ND ND 12 ND ND ND ---ND
09-Nov-06 ---10 ND ND ND ND ND ND ND ND ---ND
19-Jun-07 2.0 10.0 12.9 ND ND 2.6 J 13.3 (5.1 J)ND ND ND ---ND
NC 2L = 15 µg/L (10/23/07)28-Nov-07 2.0 10.0 ND ND ND 6.6 (20.9)B 5.6 B ND ND 6.5 B ---2.1 J
NC 2B = 25 µg/L (05/01/07)21-Apr-08 2.0 10.0 ND 3.8 J 2.0 J 5.2 (4.2 J)J 14.5 ND ND 3.1 J ---ND
22-Dec-08 2.0 10.0 3.2 B 5.2 B ND (2.6 B)3.7 B 9.8 B 3.0 B ND ND ---3.1 J
23-Jun-09 2.0 10.0 2.8 J 3.2 (ND)J 3.1 J 3.2 J 11.5 3.2 J ND 4.6 J ---ND
15-Dec-09 2.0 10.0 ND 3.8 J ND 5.6 (ND)J 7.5 J ND ND ND ---ND
28-Jun-10 2.0 10.0 4.8 J 2.9 J 4.7 J ND 5.8 (3.6 J)J 3.4 J 2.1 J 2.7 J ---ND
02-Nov-10 2.0 10.0 2.6 J ND ND (ND)3.0 J 7.5 J ND ND ND ---ND
12-Apr-11 4.0 10.0 ND ND ND ND ND ND ND ND ---ND
18-Oct-11 5.0 10.0 ND ND ND 7.0 J 7.4 J ND ND ------ND
10-Apr-12 5.0 10.0 ND ND ND ND ND ND ND ------ND
15-Oct-12 5.0 10.0 ND ND ND ND ND ND ND ------ND
16-Apr-13 5.0 10.0 ND ND ND ND ND ND ND ND ---ND
08-Oct-13 5.0 10.0 ND ND ND ND ND ND ND ------ND
29-Apr-14 5.0 10.0 ND ND ND ND 6.0 J ND ND ------ND
14-Oct-14 5.0 10.0 ND ND ND ND ND ND ND ------ND
09-Apr-15 2.5 10.0 ND ND ND 4.6 J 4.4 J ND ND ------ND
27-Oct-15 2.5 10.0 ND ND ND ND 8.7 J ND ND 6.2 J ---ND
21-Apr-16 0.02 10.0 0.12 B 0.39 J 0.37 J 0.58 J 2.4 J 0.17 B 0.27 J ------0.043 J
11-Oct-16 2.5 10.0 ND ND ND 10.4 6.1 J ND ND ------ND
18-Apr-17 2.5 10.0 ND ND ND ND 5.3 J ND ND ------ND
19-Oct-17 2.5 10.0 ND ND ND 2.6 J 4.8 J ND ND ------ND
APPENDIX 3
Summary of Historically Detected Constituents
Wilkes County Germantown Landfill
Permit No. 97-01 page 7 of 13 Joyce Engineering
Analyte DL QL MW-1 MW-2 MW-3 MW-4 MW-5 Upstream Downstream Outfall #1 Outfall #2 Blanks
Sample Collection
Date
Nickel Nov-96 ---50 ND ND ND ND 76 ND ND ND ---ND
Mar-97 ---50 ND ND ND ND ND ND ND ND ---ND
Sep-97 ---50 ND ND ND ND ND ND ND ND ---ND
Mar-98 ---50 ND ND ND ND ND ND ND ND ---ND
Sep-98 ---50 ND ND ND ND ND ND ND ND ---ND
Mar-99 ---50 ND ND ND ND ND ND ND ND ---ND
Sep-99 ---50 ND ND ND ND ND ND ND ND ---ND
May-00 ---50 ND ND ND ND ND ND ND ND ---ND
Oct-00 ---50 ND ND ND ND ND ND ND ND ---ND
Mar-01 ---50 ND ND ND ND ND ND ND ND ---ND
Oct-01 ---50 ND ND ND ND ND ND ND ND ---ND
Apr-02 ---50 ND ND ND ND ND ND ND ND ---ND
Nov-02 ---50 ND ND ND ND ND ND ND ND ---ND
May-03 ---50 ND ND ND ND ND ND ND ND ---ND
Nov-03 ---50 ND ND ND ND ND ND ND ND ---ND
Apr-04 ---50 ND ND ND ND ND ND ND ND ---ND
Oct-04 ---50 ND ND ND ND ND ND ND ND ---ND
May-05 ---50 ND ND ND ND ND ND ND ND ---ND
Oct-05 ---50 ND ND ND ND ND ND ND ND ---ND
23-May-06 ---50 ND ND ND ND ND ND ND ND ---ND
09-Nov-06 ---50 ND ND ND ND ND ND ND ND ---ND
19-Jun-07 0.6 50.0 ND ND 1.4 B 9.0 B 16.8 B (11.4 B)11.2 B 4.0 B 12.8 B ---9.6 J
NC 2L = 100 µg/L (10/23/07)28-Nov-07 0.6 50.0 1.4 B ND 1.6 B 5.2 (13.6 J)B 7.9 J 1.9 B 1.1 B 12.2 J ---1.4 J
NC 2B = 88 µg/L (05/01/07)21-Apr-08 0.6 50.0 2.0 B ND ND 2.6 (3.9 B)B 9.1 B ND ND 9.5 B ---3.3 J
22-Dec-08 0.6 50.0 ND 5.7 J ND (ND)7.5 J 13.2 J ND ND 7.8 J ---ND
23-Jun-09 0.6 50.0 1.5 B ND (ND)ND 2.4 B 9.9 B ND ND 9.0 B ---2.8 J
15-Dec-09 0.6 50.0 ND 2.1 J ND 1.3 (1.1 J)J 8.2 J ND ND 5.4 J ---ND
28-Jun-10 0.6 10.0 ND ND ND ND 5.7 (5.7 J)J ND ND 8.5 J ---ND
02-Nov-10 0.6 50.0 2.8 B 1.3 B 1.3 (ND)B 5.2 B 7.1 J 1.1 B 0.7 B 9.5 J ---1.3 J
12-Apr-11 1.7 50.0 ND ND ND 2.2 B 11.2 B ND ND ND ---4.4 J
18-Oct-11 5.0 50.0 ND ND ND ND 12.4 J ND ND ------ND
10-Apr-12 5.0 50.0 ND ND ND ND 6.8 J ND ND ------ND
15-Oct-12 5.0 50.0 ND ND ND ND ND ND ND ------ND
16-Apr-13 5.0 50.0 ND ND ND ND 8.1 J ND ND 19.6 J ---ND
08-Oct-13 5.0 50.0 ND ND ND ND 6.7 J ND ND ------ND
29-Apr-14 5.0 50.0 ND ND ND ND 10.0 J ND ND ------ND
14-Oct-14 5.0 50.0 ND ND ND ND 9.3 J ND ND ------ND
09-Apr-15 2.5 50.0 ND ND ND 3.6 J 8.4 J ND ND ------ND
27-Oct-15 2.5 50.0 ND 3.0 J ND 4.0 J 9.7 J ND ND 6.7 J ---ND
21-Apr-16 0.053 50.0 1.1 B 0.49 B 0.52 B 3.4 B 9.9 J 0.30 B 0.33 B ------1.1 J
11-Oct-16 2.5 50.0 ND ND ND 8.8 J 13.7 J ND ND ------ND
18-Apr-17 2.5 50.0 ND ND ND 4.1 J 10.8 J ND ND ------ND
19-Oct-17 2.5 50.0 ND ND ND 4.6 J 9.9 J ND ND ------ND
Selenium Apr-93 ---5 ND ND ND ND ND ND ND ND ND ---
Sep-93 ---5 ND 25 ND 5 ND ND ND ---------
Apr-94 ---5 ND ND ND ND ND ND ND ND ND ---
Oct-94 ---20 ND ND ND ND ND ND ND ND ND ---
Apr-95 ---20 ND ND ND ND ND ND ND ND ------
Nov-95 ---20 ND ND ND ND ND ND ND ND ------
May-96 ---20 ND ND ND ND ND ND ND ND ------
Nov-96 ---20 ND ND ND ND ND ND ND ND ---ND
Mar-97 ---20 ND ND ND ND ND ND ND ND ---ND
Sep-97 ---20 ND ND ND ND ND ND ND ND ---ND
Mar-98 ---20 ND ND ND ND ND ND ND ND ---ND
Sep-98 ---20 ND ND ND ND ND ND ND ND ---ND
Mar-99 ---20 ND ND ND ND ND ND ND ND ---ND
Sep-99 ---20 ND ND ND ND ND ND ND ND ---ND
May-00 ---20 ND ND ND ND ND ND ND ND ---ND
Oct-00 ---20 ND ND ND ND ND ND ND ND ---ND
Mar-01 ---20 ND ND ND ND ND ND ND ND ---ND
Oct-01 ---20 ND ND ND ND ND ND ND ND ---ND
Apr-02 ---20 ND ND ND ND ND ND ND ND ---ND
Nov-02 ---20 ND ND ND ND ND ND ND ND ---ND
May-03 ---20 ND ND ND ND ND ND ND ND ---ND
Nov-03 ---20 ND ND ND ND ND ND ND ND ---ND
Apr-04 ---20 ND ND ND ND ND ND ND ND ---ND
Oct-04 ---20 ND ND ND ND ND ND ND ND ---ND
May-05 ---20 ND ND ND ND ND ND ND ND ---ND
Oct-05 ---20 ND ND ND ND ND ND ND ND ---ND
23-May-06 ---20 ND ND ND ND ND ND ND ND ---ND
09-Nov-06 ---20 ND ND ND ND ND ND ND ND ---ND
19-Jun-07 6.3 10.0 ND ND ND ND ND (ND)ND ND ND ---ND
NC 2L = 50 µg/L (10/23/07)28-Nov-07 6.3 10.0 ND ND ND ND (ND)ND 7.6 B ND ND ---7.8 J
NC 2B = 5 µg/L (05/01/07)21-Apr-08 6.3 10.0 ND ND ND ND (4.7 J)ND ND ND ND ---ND
22-Dec-08 6.3 10.0 ND ND ND (ND)ND ND ND ND ND ---ND
23-Jun-09 6.3 10.0 ND ND (ND)ND ND ND ND ND ND ---ND
15-Dec-09 6.3 10.0 ND ND ND ND (ND)ND ND ND ND ---ND
NC 2L = 20 µg/L (01/01/10)28-Jun-10 6.3 10.0 ND ND ND ND ND (ND)ND ND ND ---ND
02-Nov-10 6.3 10.0 ND ND ND (ND)ND ND ND ND ND ---ND
12-Apr-11 3.8 10.0 ND ND ND ND ND ND ND ND ---ND
18-Oct-11 10.0 10.0 ND ND ND ND ND ND ND ------ND
10-Apr-12 10.0 10.0 ND ND ND ND ND ND ND ------ND
15-Oct-12 10.0 10.0 ND ND ND ND ND ND ND ------ND
16-Apr-13 10.0 10.0 ND ND ND ND ND ND ND ND ---ND
08-Oct-13 10.0 10.0 ND ND ND ND ND ND ND ------ND
29-Apr-14 10.0 10.0 ND ND ND ND 15.7 ND ND ------ND
14-Oct-14 10.0 10.0 ND ND ND ND ND ND ND ------ND
09-Apr-15 5.0 10.0 ND ND ND ND ND ND ND ------ND
27-Oct-15 5.0 10.0 ND ND ND ND ND ND ND ND ---ND
21-Apr-16 0.35 10.0 ND 0.71 J ND ND 1.8 J ND 0.36 J ------ND
11-Oct-16 5.0 10.0 ND ND ND ND ND ND ND ------ND
18-Apr-17 5.0 10.0 ND ND ND ND ND ND ND ------ND
19-Oct-17 5.0 10.0 ND 9.7 J ND ND ND 7.9 J ND ------5.5 J
APPENDIX 3
Summary of Historically Detected Constituents
Wilkes County Germantown Landfill
Permit No. 97-01 page 8 of 13 Joyce Engineering
Analyte DL QL MW-1 MW-2 MW-3 MW-4 MW-5 Upstream Downstream Outfall #1 Outfall #2 Blanks
Sample Collection
Date
Silver 28-Nov-07 1.1 10.0 ND ND 1.5 J ND (ND)ND ND ND ND ---ND
NC 2L = 17.5 µg/L (10/23/07)21-Apr-08 1.1 10.0 ND ND ND ND (ND)ND ND ND ND ---ND
NC 2B = 0.06 µg/L (05/01/07)22-Dec-08 1.1 10.0 ND ND ND (ND)ND ND ND ND ND ---ND
23-Jun-09 1.1 10.0 ND 1.1 (ND)B ND ND ND ND ND ND ---9.3 J
15-Dec-09 1.1 10.0 ND ND ND 2.3 (ND)B ND 1.4 B 2.2 B ND ---1.6 J
NC 2L = 20 µg/L (01/01/10)28-Jun-10 1.1 10.0 1.2 J 1.4 J 1.4 J ND ND (ND)ND ND ND ---ND
02-Nov-10 1.1 10.0 ND ND ND (ND)ND ND ND ND ND ---ND
12-Apr-11 0.10 10.0 ND ND ND ND ND ND ND 0.12 B ---0.21 J
18-Oct-11 5.0 10.0 ND ND ND ND ND ND ND ------ND
10-Apr-12 5.0 10.0 ND ND ND ND ND ND ND ------ND
15-Oct-12 5.0 10.0 ND ND ND ND ND ND ND ------ND
16-Apr-13 5.0 10.0 ND ND ND ND ND ND ND ND ---ND
08-Oct-13 5.0 10.0 ND ND ND ND ND ND ND ------ND
29-Apr-14 5.0 10.0 ND ND ND ND ND ND ND ------ND
14-Oct-14 5.0 10.0 ND ND ND ND ND ND ND ------ND
09-Apr-15 2.5 10.0 ND ND ND ND ND ND ND ------ND
27-Oct-15 2.5 10.0 ND ND ND ND ND ND ND ND ---ND
21-Apr-16 0.011 10.0 0.056 B 0.029 B 0.18 J 0.11 J 0.023 B 0.024 B 0.014 B ------0.012 J
11-Oct-16 2.5 10.0 ND ND ND ND ND ND ND ------ND
18-Apr-17 2.5 10.0 ND ND ND ND ND ND ND ------ND
19-Oct-17 2.5 10.0 ND ND ND ND ND ND ND ------ND
Thallium 19-Jun-07 2.7 5.5 ND ND 4.3 J ND ND (ND)ND ND ND ---ND
GWPS = 0.28 µg/L (10/23/07)28-Nov-07 2.7 5.5 ND ND ND ND ND ND ND ND ---ND
NC 2B = NE (05/01/07)21-Apr-08 2.7 5.5 ND ND 2.9 B ND (ND)ND ND ND ND ---3.3 J
22-Dec-08 2.7 5.5 ND ND ND (ND)ND ND ND ND ND ---4.0 J
23-Jun-09 2.7 5.5 ND 4.0 (ND)J ND ND ND ND ND ND ---ND
15-Dec-09 2.7 5.5 ND ND ND ND (ND)ND ND ND ND ---ND
28-Jun-10 2.7 5.5 ND 3.0 J ND ND ND (ND)ND ND ND ---ND
GWPS = 0.2 µg/L (10/1/10)02-Nov-10 2.7 5.5 ND ND ND (ND)ND ND ND 4.7 B 4.5 B ---3.9 J
12-Apr-11 3.0 5.5 ND ND ND ND 3.0 J ND ND ND ---ND
18-Oct-11 5.4 5.5 ND ND ND 5.8 ND ND ND ------ND
10-Apr-12 5.4 5.5 ND ND ND ND ND ND ND ------ND
15-Oct-12 5.4 5.5 ND ND ND ND ND ND ND ------ND
16-Apr-13 5.4 5.5 ND ND ND ND ND ND ND ND ---ND
08-Oct-13 5.4 5.5 ND ND ND ND ND ND ND ------ND
29-Apr-14 5.4 5.5 ND ND ND ND ND ND ND ------ND
14-Oct-14 5.4 5.5 ND ND ND ND ND ND ND ------ND
09-Apr-15 5.0 5.5 ND ND ND ND ND ND ND ------ND
27-Oct-15 5.0 5.5 ND ND ND ND ND ND ND ND ---ND
21-Apr-16 0.0093 5 0.064 J 0.07 J 0.021 J 0.078 J 0.048 J ND ND ------ND
11-Oct-16 5.0 5.5 ND ND ND ND ND ND ND ------ND
18-Apr-17 0.0 5.5 ND 0.09 J ND ND 0.025 J ND ND ------ND
19-Oct-17 0.0 5.5 ND 0.07 J ND 0.025 J 0.040 J ND ND ------ND
Vanadium Oct-94 ---40 ND ND ND 174 62 ND ND 127 256 ---
Apr-95 ---40 ND ND ND ND ND ND ND ND ------
Nov-95 ---40 ND ND ND ND ND ND ND ND ------
May-96 ---40 ND 152 ND ND ND ND ND ND ------
Nov-96 ---40 ND 59 ND ND 203 ND ND ND ---ND
Mar-97 ---40 ND ND ND ND 66 ND ND ND ---ND
Sep-97 ---40 ND ND 55 ND ND ND ND ND ---ND
Mar-98 ---40 ND ND 87 ND 48 ND ND ND ---ND
Sep-98 ---40 ND ND ND ND ND ND ND ND ---ND
Mar-99 ---40 ND ND ND ND ND ND ND ND ---ND
Sep-99 ---40 ND ND ND ND 92 ND ND ND ND ND
May-00 ---40 ND ND ND ND ND ND ND ND ---ND
Oct-00 ---40 ND ND ND ND ND ND ND ND ---ND
Mar-01 ---40 ND ND ND ND ND ND ND ND ---ND
Oct-01 ---40 ND ND ND ND 57 ND ND ND ---ND
Apr-02 ---40 ND ND ND ND ND ND ND ND ---ND
Nov-02 ---40 ND ND ND ND ND ND ND ND ---ND
May-03 ---40 ND ND ND ND ND ND ND ND ---ND
Nov-03 ---40 ND ND ND ND 41(47)ND ND ND ---ND
Apr-04 ---40 ND ND ND ND ND ND ND ND ---ND
Oct-04 ---40 ND ND ND ND ND ND ND ND ---ND
May-05 ---40 ND ND ND ND ND ND ND ND ---ND
Oct-05 ---40 ND ND ND ND ND ND ND ND ---ND
23-May-06 ---40 ND ND ND ND ND ND ND ND ---ND
09-Nov-06 ---40 ND ND ND ND ND ND ND ND ---ND
19-Jun-07 0.4 25.0 ND ND ND 6.9 J 30.0 (14.0 J)ND ND ND ---ND
GWPS = 3.5 µg/L (10/23/07)28-Nov-07 0.4 25.0 ND 3.0 J ND 11.3 (7.4 J)J ND ND ND ND ---ND
NC 2B = NE (05/01/07)21-Apr-08 0.4 25.0 ND 4.0 J ND 4.3 (4.6 J)J 22.4 J ND ND ND ---ND
22-Dec-08 0.4 25.0 2.2 J 1.9 J ND (ND)1.5 J 16.7 J ND ND ND ---ND
23-Jun-09 0.4 25.0 ND ND (ND)ND 2.5 J 16.8 J ND ND 3.6 J ---ND
15-Dec-09 0.4 25.0 ND 5.6 B 1.9 B 2.3 (2.3 B)B 16.6 B ND ND 0.6 B ---5.2 J
28-Jun-10 0.4 25.0 3.4 J ND ND ND 3.3 (7.1 J)J ND 1.3 J ND ---ND
GWPS = 0.3 µg/L (10/1/10)02-Nov-10 0.4 25.0 ND ND 0.9 (1.3 J)J 1.4 J 8.9 J 1.1 J 0.6 J 2.0 J ---ND
12-Apr-11 0.20 25.0 ND 5.3 J 1.7 J ND 23.2 J 0.64 B 0.72 B 1.9 J ---0.27 J
18-Oct-11 5.0 25.0 ND 6.6 J ND 19.1 J 31.8 ND ND ------ND
10-Apr-12 5.0 25.0 ND ND ND 12.1 J ND ND ND ------ND
15-Oct-12 5.0 25.0 ND ND ND ND ND ND ND ------ND
16-Apr-13 5.0 25.0 ND ND ND ND 5.4 J ND ND ND ---ND
08-Oct-13 5.0 25.0 ND ND ND ND ND ND ND ------ND
29-Apr-14 5.0 25.0 ND ND ND ND 20.7 J ND ND ------ND
14-Oct-14 5.0 25.0 ND ND ND ND ND ND ND ------ND
09-Apr-15 2.5 25.0 2.8 J ND ND 11.2 J 8.9 J ND 5.3 J ------ND
27-Oct-15 2.5 25.0 2.7 J ND ND 3.8 J 17.6 J ND ND 9.7 J ---ND
21-Apr-16 2.5 25.0 ND ND ND ND 5.6 J ND ND ------ND
11-Oct-16 2.5 25.0 ND ND ND 41.3 13.1 J ND ND ------ND
18-Apr-17 2.5 25.0 ND ND ND 7.6 J 16.5 J ND ND ------ND
19-Oct-17 2.5 25.0 ND ND ND 4.1 J 4.4 J ND ND ------ND
APPENDIX 3
Summary of Historically Detected Constituents
Wilkes County Germantown Landfill
Permit No. 97-01 page 9 of 13 Joyce Engineering
Analyte DL QL MW-1 MW-2 MW-3 MW-4 MW-5 Upstream Downstream Outfall #1 Outfall #2 Blanks
Sample Collection
Date
Zinc Apr-93 ---20 49 312 78 44 59 ND 34 4290 83 ---
Sep-93 ---20 ND 1640 ND ND ND ND ND ---------
Apr-94 ---20 25 88 ND ND ND 26 26 54 60 ---
Oct-94 ---50 ND 68 ND ND ND ND ND ND ND ---
Apr-95 ---50 ND ND 98 ND ND ND ND ND ------
Nov-95 ---50 ND ND ND ND 81 ND 50 84 ------
May-96 ---50 97 327 159 68 70 71 ND 91 ------
Nov-96 ---50 90 159 84 ND 418 50 86 ND ---ND
Mar-97 ---50 ND 99 88 56 130 ND ND ND ---ND
Sep-97 ---50 70 560 200 72 171 118 200 ND ---ND
Mar-98 ---50 ND 168 197 ND 94 ND ND ND ---ND
Sep-98 ---50 ND ND ND ND ND 159 ND 123 ---ND
Mar-99 ---50 ND ND ND ND ND ND ND ND ---ND
Sep-99 ---50 ND ND ND ND 61 ND ND ND ---ND
May-00 ---50 ND ND ND ND ND ND ND ND ------
Oct-00 ---50 ND 63 ND ND ND ND ND ND ---ND
Mar-01 ---50 ND ND ND ND ND ND ND ND ---ND
Oct-01 ---50 ND ND ND ND ND ND ND ND ---ND
Apr-02 ---50 ND ND ND ND ND ND ND ND ---ND
Nov-02 ---50 52 70 57(ND)50 69 ND ND ND ---ND
May-03 ---50 ND 77 ND ND ND 50 ND 61 ---ND
Nov-03 ---50 ND ND ND 78 52(89)ND 51 135 ---ND
Apr-04 ---50 ND ND ND ND ND ND ND ND ---ND
Oct-04 ---50 ND ND ND ND ND ND ND 138 ---ND
May-05 ---50 ND ND ND ND ND ND ND ND ---ND
Oct-05 ---50 137 ND ND ND ND ND ND 79 ---ND
23-May-06 ---50 ND ND ND ND ND ND ND ND ---ND
09-Nov-06 ---50 ND ND ND ND ND ND ND ND ---74
19-Jun-07 2.7 10.0 53.4 103 39.6 49.4 110 (95.8)89.9 73.2 144 ---3.0 J
NC 2L = 1,050 µg/L (10/23/07)28-Nov-07 2.7 10.0 13.2 B 33.4 B 8.3 B 11.2 (70.6)B 26.8 B 7.6 B 5.8 B 28.9 B ---7.1 J
NC 2B = 50 µg/L (05/01/07)21-Apr-08 2.7 10.0 ND ND ND ND (ND)17.9 B ND ND 21.3 B ---6.0 J
22-Dec-08 2.7 10.0 ND 10.3 B ND (ND)ND 11.4 B ND ND ND ---11.1 J
23-Jun-09 2.7 10.0 83.7 B ND (ND)76.1 B 27.1 B 108 B 36.8 B 41.3 B 79.7 B ---51.8 B
15-Dec-09 2.7 10.0 ND 20.5 B 8.8 B 7.4 (ND)B 29.4 B 30.8 B 11.2 B ND ---26.5
NC 2L = 1,000 µg/L (01/01/10)28-Jun-10 2.7 10.0 20.0 B 9.6 B 14.9 B 18.2 B 15.9 (18.5 B)B 8.5 B 24.6 B 25.9 B ---9.0 J
02-Nov-10 2.7 10.0 11.4 B 17.4 B 11.9 (7.2 B)B 14.6 B 22.8 B 11.3 B 14.3 B 16.5 B ---13.3
12-Apr-11 0.40 10.0 7.4 B 14.8 B 7.0 B 5.0 B 28.9 B 3.6 B 4.2 B 9.7 B ---22.5
18-Oct-11 10.0 10.0 ND 14.0 ND 14.5 57.6 ND ND ------ND
10-Apr-12 10.0 10.0 ND ND ND ND ND ND ND ------ND
15-Oct-12 10.0 10.0 ND ND ND ND ND ND ND ------ND
16-Apr-13 10.0 10.0 ND 12.3 ND ND 11.3 ND ND 17.3 ---ND
08-Oct-13 10.0 10.0 ND ND ND ND 14.5 ND ND ------ND
29-Apr-14 10.0 10.0 ND ND ND ND 27.3 ND ND ------ND
14-Oct-14 10.0 10.0 ND ND ND ND ND ND ND ------ND
09-Apr-15 5.0 10.0 5.9 J 7.4 J ND 6.1 J 5.5 J ND 16.9 ------ND
27-Oct-15 5.0 10.0 6.1 B 9.7 J 6.4 B ND 41 B 8.0 B 10.1 16.6 ---8.6 J
21-Apr-16 0.98 10.0 5.9 B 17 B 9.2 B 6.4 B 10 B 2.8 B 3.8 B ------3.5 J
11-Oct-16 5.0 10.0 ND 15.8 6.5 J 18.2 23.4 ND ND ------ND
18-Apr-17 5.0 10.0 ND 5.6 J ND ND 14.7 ND ND ------ND
19-Oct-17 5.0 10.0 5.7 J 13.2 ND ND 7.4 J ND ND ------ND
Organic Compounds
Acetone 19-Jun-07 1.2 100 ND ND ND 5.3 J ND (ND)ND ND 7.0 J ---ND
NC 2L = 700 µg/L (10/23/07)28-Nov-07 1.2 100 ND 2.40 J 1.85 J 2.0 (2.8 J)J ND 1.8 J 2.7 J 2.3 J ---ND
NC 2B = NE (05/01/07)21-Apr-08 1.2 100 8.69 J 7.17 J ND ND (ND)ND ND 6.1 J ND ---ND
22-Dec-08 1.2 100 3.1 J ND ND (ND)3.6 J ND 2.1 J ND ND ---ND
23-Jun-09 1.2 100 ND ND (ND)ND ND ND ND ND ND ---ND
15-Dec-09 1.2 100 ND ND ND ND (ND)ND ND ND ND ---ND
NC 2L = 6,000 µg/L (01/01/10)28-Jun-10 1.2 100 ND ND ND ND ND (ND)ND ND ND ---ND
02-Nov-10 1.2 100 ND ND ND (ND)ND 20.2 J ND ND ND ---ND
12-Apr-11 2.2 100 ND ND ND ND ND ND ND 2.7 J ---ND
18-Oct-11 2.2 100 ND ND ND 2.3 B 3.2 B 2.8 B 2.5 B ------2.2 J
10-Apr-12 2.2 100 ND ND ND ND ND ND ND ------6.0 J
15-Oct-12 10.0 100 ND ND ND ND 15.1 J ND ND ------ND
16-Apr-13 10.0 100 ND 10.6 B ND 10.0 B ND ND 10.7 B 22.5 B ---48.9 J
08-Oct-13 10.0 100 ND ND ND ND ND ND ND ------ND
29-Apr-14 10.0 100 ND ND ND ND ND ND ND ------ND
14-Oct-14 10.0 100 ND ND ND ND ND ND ND ------ND
09-Apr-15 10.0 100 ND ND ND ND ND ND ND ------ND
27-Oct-15 10.0 100 ND ND ND ND 19.1 J ND ND 10.2 J ---ND
21-Apr-16 0.31 100 ND ND ND 4.2 J ND ND ND ------ND
11-Oct-16 10.0 100 ND ND ND ND ND ND ND ------ND
18-Apr-17 10.0 100 ND ND ND ND ND ND ND ------ND
19-Oct-17 10.0 100 ND ND ND ND ND ND ND ------ND
APPENDIX 3
Summary of Historically Detected Constituents
Wilkes County Germantown Landfill
Permit No. 97-01 page 10 of 13 Joyce Engineering
Analyte DL QL MW-1 MW-2 MW-3 MW-4 MW-5 Upstream Downstream Outfall #1 Outfall #2 Blanks
Sample Collection
Date
Benzene 19-Jun-07 0.1 1.0 ND ND ND ND 1.4 (1.4)ND ND ND ---ND
NC 2L = 1 µg/L (10/23/07)28-Nov-07 0.1 1.0 ND ND ND ND (ND)ND ND ND ND ---ND
NC 2B = NE (05/01/07)21-Apr-08 0.1 1.0 ND ND ND ND (ND)1.34 ND ND ND ---ND
22-Dec-08 0.1 1.0 ND ND ND (ND)ND 1.1 ND ND ND ---ND
23-Jun-09 0.1 1.0 ND ND (ND)ND ND 1.0 J ND ND 0.5 J ---ND
15-Dec-09 0.1 1.0 ND ND ND 0.2 (0.2 J)J 1.2 ND ND 0.4 J ---ND
28-Jun-10 0.1 1.0 ND ND ND ND 0.8 (0.8 J)J ND ND 0.3 J ---ND
02-Nov-10 0.1 1.0 ND ND ND (ND)ND 1.1 ND ND ND ---ND
12-Apr-11 0.25 1.0 ND ND ND ND 1.1 ND ND ND ---ND
18-Oct-11 0.25 1.0 ND ND ND ND 1.3 ND ND ------ND
10-Apr-12 0.25 1.0 ND ND ND ND 1.1 ND ND ------ND
15-Oct-12 0.25 1.0 ND ND ND ND 0.96 J ND ND ------ND
16-Apr-13 0.25 1.0 0.69 J ND ND ND 1.2 ND ND ND ---ND
08-Oct-13 0.25 1.0 ND ND ND ND 1.3 ND ND ------ND
29-Apr-14 0.25 1.0 ND ND ND ND 1.2 ND ND ------ND
14-Oct-14 0.25 1.0 ND ND ND ND 1.1 ND ND ------ND
09-Apr-15 0.25 1.0 ND ND ND ND 0.66 J ND ND ------ND
27-Oct-15 0.25 1.0 ND ND ND ND 0.99 J ND ND ND ---ND
21-Apr-16 0.048 1.0 ND ND ND ND 1.2 ND ND ------ND
11-Oct-16 0.25 1.0 ND ND ND 0.33 J 1.0 ND ND ------ND
18-Apr-17 0.25 1.0 ND ND ND 0.35 J 1.1 ND ND ------ND
19-Oct-17 0.25 1.0 ND ND ND ND 1.0 ND ND ------ND
Bromomethane 16-Apr-13 0.29 10.0 0.54 J ND ND ND ND ND ND ND ---ND
NC 2L = NE (01/01/10)08-Oct-13 0.29 10.0 ND ND ND ND ND ND ND ------ND
NC 2B = NE (05/01/07)29-Apr-14 0.29 10.0 ND ND ND ND ND ND ND ------ND
14-Oct-14 0.29 10.0 ND ND ND ND ND ND ND ------0.63 J
09-Apr-15 0.29 10.0 ND ND ND ND ND ND ND ------ND
27-Oct-15 0.29 10.0 ND ND ND ND ND ND ND ND ---ND
21-Apr-16 0.18 10.0 ND ND ND ND ND ND ND ------ND
11-Oct-16 0.29 10.0 ND ND ND ND ND ND ND ------ND
18-Apr-17 0.29 10.0 ND ND ND ND ND ND ND ------ND
19-Oct-17 0.29 10.0 ND ND ND ND ND ND ND ------ND
Carbon Disulfide 28-Nov-07 0.5 100 1.02 J 11.0 J 2.95 J 1.4 (0.6 J)J ND ND ND ND ---ND
NC 2L = 700 µg/L (10/23/07)21-Apr-08 0.5 100 ND ND ND ND (ND)2.9 J ND ND ND ---ND
NC 2B = NE (05/01/07)22-Dec-08 0.5 100 ND ND ND 1.0 J 0.9 J ND ND ND ---ND
23-Jun-09 0.5 100 ND ND (ND)ND ND ND ND ND ND ---ND
15-Dec-09 0.5 100 ND ND ND ND (ND)ND ND ND ND ---ND
28-Jun-10 0.5 100 ND ND ND ND ND (ND)ND ND ND ---ND
02-Nov-10 0.5 100 ND ND ND (ND)ND ND ND ND ND ---ND
12-Apr-11 1.2 100 ND ND ND ND ND ND ND ND ---ND
18-Oct-11 1.2 100 ND ND ND ND ND ND ND ------ND
10-Apr-12 1.2 100 ND ND ND ND ND ND ND ------ND
15-Oct-12 1.2 100 ND ND ND ND ND ND ND ------ND
16-Apr-13 1.2 100 ND ND ND ND ND ND ND ND ---ND
08-Oct-13 1.2 100 ND ND ND ND ND ND ND ------ND
29-Apr-14 1.2 100 ND ND ND ND ND ND ND ------ND
14-Oct-14 1.2 100 ND ND ND ND ND ND ND ------ND
09-Apr-15 1.2 100 ND ND ND ND ND ND ND ------ND
27-Oct-15 1.2 100 ND ND ND ND ND ND ND ND ---ND
21-Apr-16 0.075 100 ND ND ND ND ND ND ND ------ND
11-Oct-16 1.2 100 ND ND ND ND ND ND ND ------ND
18-Apr-17 1.2 100 ND ND ND ND ND ND ND ------ND
19-Oct-17 1.2 100 ND ND ND ND ND ND ND ------ND
Chlorobenzene Sep-98 ---5 ND ND ND ND 9 ND ND ND ---ND
Mar-99 ---5 ND ND ND ND 8 ND ND ND ---ND
Oct-99 ---5 ND ND ND ND 5.9 ND ND ND ---ND
May-00 ---5 ND ND ND 5.6 9.6 ND ND ND ---ND
Oct-00 ---5 ND ND ND ND 8.7 ND ND ND ---ND
Mar-01 ---5 ND ND ND ND 8.8 ND ND ND ---ND
Oct-01 ---5 ND ND ND ND 11 ND ND ND ---ND
Apr-02 ---5 ND ND ND ND 11 ND ND ND ---ND
Nov-02 ---5 ND ND ND ND 8.1 ND ND ND ---ND
May-03 ---5 ND ND ND ND 9.1 ND ND ND ---ND
Nov-03 ---5 ND ND ND ND 8.9(9.7)ND ND ND ---ND
Apr-04 ---5 ND ND ND ND 9.3 ND ND ND ---ND
Oct-04 ---5 ND ND ND ND 12 ND ND ND ---ND
May-05 ---5 ND ND ND ND 6.6 ND ND ND ---ND
Oct-05 ---5 ND ND ND ND 8.1(7.8)ND ND ND ---ND
23-May-06 ---5 ND ND ND ND 6.3 ND ND ND ---ND
09-Nov-06 ---5 ND ND ND ND 10 ND ND ND ---ND
19-Jun-07 0.1 3.0 ND ND ND 1.9 J 10.6 (10.6)ND ND 0.8 J ---ND
NC 2L = 50 µg/L (10/23/07)28-Nov-07 0.1 3.0 ND ND ND 1.9 (2.3 J)J 7.4 ND ND ND ---ND
NC 2B = NE (05/01/07)21-Apr-08 0.1 3.0 ND ND ND 4.8 (4.6)9.9 ND ND 1.6 J ---ND
22-Dec-08 0.1 3.0 ND ND ND (ND)1.6 J 8.0 ND ND 0.7 J ---ND
23-Jun-09 0.1 3.0 ND ND (ND)ND 1.0 J 8.0 ND ND 2.0 J ---ND
15-Dec-09 0.1 3.0 0.7 J ND ND 2.1 (1.9 J)J 9.6 ND ND 2.6 J ---ND
28-Jun-10 0.1 3.0 ND ND ND ND 7.7 (7.2)ND ND 1.5 J ---ND
02-Nov-10 0.1 3.0 0.8 J ND ND (ND)1.3 J 6.7 ND ND 0.5 J ---ND
12-Apr-11 0.23 3.0 0.34 J ND ND 3.2 9.9 ND ND ND ---ND
18-Oct-11 0.23 3.0 0.42 J ND ND 1.9 J 10 ND ND ------ND
10-Apr-12 0.23 3.0 0.30 B ND ND 3.5 8.8 ND ND ------0.32 J
15-Oct-12 0.23 3.0 0.25 J ND ND 1.7 J 7.0 ND ND ------ND
16-Apr-13 0.23 3.0 1.2 J ND 1.3 J ND 9.4 ND ND ND ---ND
08-Oct-13 0.23 3.0 1.1 J ND ND 2.3 J 10.0 ND ND ------ND
29-Apr-14 0.23 3.0 0.67 J ND ND 1.3 J 10.5 ND ND ------ND
14-Oct-14 0.23 3.0 0.56 J ND ND 4.3 8.7 ND ND ------ND
09-Apr-15 0.23 3.0 0.72 J ND ND 1.9 J 6.7 ND ND ------ND
27-Oct-15 0.23 3.0 0.77 J ND ND 4.8 8.1 ND ND ND ---ND
21-Apr-16 0.062 3.0 0.67 J ND ND 3.0 11 ND ND ------ND
11-Oct-16 0.23 3.0 0.54 J ND ND 6.8 8.9 ND ND ------ND
18-Apr-17 0.23 3.0 ND ND ND 4.9 9.9 ND ND ------ND
19-Oct-17 0.23 3.0 0.30 J ND ND 5.1 9.6 ND ND ------ND
APPENDIX 3
Summary of Historically Detected Constituents
Wilkes County Germantown Landfill
Permit No. 97-01 page 11 of 13 Joyce Engineering
Analyte DL QL MW-1 MW-2 MW-3 MW-4 MW-5 Upstream Downstream Outfall #1 Outfall #2 Blanks
Sample Collection
Date
Chloromethane 22-Dec-08 0.1 1.0 ND ND ND ND ND ND ND 0.2 J ---ND
NC 2L = 2.6 µg/L (10/23/07)23-Jun-09 0.1 1.0 ND ND (ND)ND ND ND ND ND ND ---ND
NC 2B = NE (05/01/07)15-Dec-09 0.1 1.0 ND ND ND ND (ND)ND ND ND ND ---ND
NC 2L = 3 µg/L (01/01/10)28-Jun-10 0.1 1.0 ND ND ND ND ND (ND)ND ND ND ---ND
02-Nov-10 0.1 1.0 ND ND ND (ND)ND ND ND ND ND ---ND
12-Apr-11 0.11 1.0 ND ND 0.19 J ND ND ND ND ND ---ND
18-Oct-11 0.11 1.0 0.14 J ND ND ND ND 0.16 J 0.13 J ------ND
10-Apr-12 0.11 1.0 ND ND ND ND ND ND ND ------ND
15-Oct-12 0.11 1.0 ND ND ND ND ND ND ND ------ND
16-Apr-13 0.11 1.0 0.43 J ND ND ND ND ND ND ND ---ND
08-Oct-13 0.11 1.0 ND ND ND ND ND ND ND ------ND
29-Apr-14 0.11 1.0 ND ND ND ND ND ND ND ------ND
14-Oct-14 0.11 1.0 ND ND ND ND ND ND ND ------ND
09-Apr-15 0.11 1.0 ND ND ND ND ND ND ND ------ND
27-Oct-15 0.11 1.0 ND ND ND ND ND ND ND ND ---ND
21-Apr-16 0.079 1.0 ND ND ND ND ND ND ND ------ND
11-Oct-16 0.11 1.0 ND ND ND ND ND ND ND ------ND
18-Apr-17 0.11 1.0 ND ND ND ND ND ND ND ------ND
19-Oct-17 0.11 1.0 0.27 J 0.29 J ND 0.25 J 0.2 J ND ND ------ND
cis-1,2-Dichloroethene Oct-94 ---5 8 ND ND ND 11 ND ND ND ND ND
Apr-95 ---5 ND ND ND ND ND ND ND ND ------
Nov-95 ---5 ND ND ND ND 8 ND ND ND ------
May-96 ---5 ND ND ND ND ND ND ND ND ------
Nov-96 ---5 ND ND ND ND ND ND ND ND ---ND
Mar-97 ---5 ND ND ND ND ND ND ND ND ---ND
Sep-97 ---5 ND ND ND ND ND ND ND ND ---ND
Mar-98 ---5 ND ND ND ND ND ND ND ND ---ND
Sep-98 ---5 ND ND ND ND ND ND ND ND ---ND
Mar-99 ---5 ND ND ND ND ND ND ND ND ---ND
Sep-99 ---5 ND ND ND ND ND ND ND ND ---ND
May-00 ---5 ND ND ND ND ND ND ND ND ---ND
Oct-00 ---5 ND ND ND ND ND ND ND ND ---ND
Mar-01 ---5 ND ND ND ND ND ND ND ND ---ND
Oct-01 ---5 ND ND ND ND ND ND ND ND ---ND
Apr-02 ---5 ND ND ND ND ND ND ND ND ---ND
Nov-02 ---5 ND ND ND ND ND ND ND ND ---ND
May-03 ---5 ND ND ND ND ND ND ND ND ---ND
Nov-03 ---5 ND ND ND ND ND ND ND ND ---ND
Apr-04 ---5 ND ND ND ND ND ND ND ND ---ND
Oct-04 ------ND ND ND ND ND ND ND ND ---ND
May-05 ---5 ND ND ND ND ND ND ND ND ---ND
Oct-05 ---5 ND ND ND ND ND ND ND ND ---ND
23-May-06 ---5 ND ND ND ND ND ND ND ND ---ND
09-Nov-06 ---5 ND ND ND ND ND ND ND ND ---ND
19-Jun-07 0.1 5.0 ND ND ND ND ND (ND)ND ND ND ---ND
NC 2L = 70 µg/L (10/23/07)28-Nov-07 0.1 5.0 ND ND ND ND (ND)ND ND ND ND ---ND
NC 2B = NE (05/01/07)21-Apr-08 0.1 5.0 ND ND ND ND (ND)ND ND ND ND ---ND
22-Dec-08 0.1 5.0 ND ND ND (ND)ND ND ND ND ND ---ND
23-Jun-09 0.1 5.0 ND ND (ND)ND ND ND ND ND ND ---ND
15-Dec-09 0.1 5.0 ND ND ND ND (ND)ND ND ND ND ---ND
28-Jun-10 0.1 5.0 ND ND ND ND ND (ND)ND ND ND ---ND
02-Nov-10 0.1 5.0 ND ND ND (ND)ND ND ND ND ND ---ND
12-Apr-11 0.19 5.0 ND ND ND ND ND ND ND ND ---ND
18-Oct-11 0.19 5.0 ND ND ND 0.25 J ND ND ND ------ND
10-Apr-12 0.19 5.0 ND ND ND ND ND ND ND ------ND
15-Oct-12 0.19 5.0 ND ND ND ND ND ND ND ------ND
16-Apr-13 0.19 5.0 ND ND ND ND ND ND ND ND ---ND
08-Oct-13 0.19 5.0 ND ND ND ND ND ND ND ------ND
29-Apr-14 0.19 5.0 ND ND ND ND ND ND ND ------ND
14-Oct-14 0.19 5.0 ND ND ND ND ND ND ND ------ND
09-Apr-15 0.19 5.0 ND ND ND ND ND ND ND ------ND
27-Oct-15 0.19 5.0 ND ND ND ND ND ND ND ND ---ND
21-Apr-16 0.19 5.0 ND ND ND ND ND ND ND ND ---ND
11-Oct-16 0.19 5.0 ND ND ND ND ND ND ND ------ND
18-Apr-17 0.19 5.0 ND ND ND ND ND ND ND ------ND
19-Oct-17 0.19 5.0 ND ND ND ND ND ND ND ------ND
APPENDIX 3
Summary of Historically Detected Constituents
Wilkes County Germantown Landfill
Permit No. 97-01 page 12 of 13 Joyce Engineering
Analyte DL QL MW-1 MW-2 MW-3 MW-4 MW-5 Upstream Downstream Outfall #1 Outfall #2 Blanks
Sample Collection
Date
1,2-Dichlorobenzene Apr-02 ---5 ND ND ND ND 5.4 ND ND ND ---ND
Nov-02 ---5 ND ND ND ND 5.2 ND ND ND ---ND
May-03 ---5 ND ND ND ND ND ND ND ND ---ND
Nov-03 ---5 ND ND ND ND ND ND ND ND ---ND
Apr-04 ---5 ND ND ND ND ND ND ND ND ---ND
Oct-04 ---5 ND ND ND ND 6.7 ND ND ND ---ND
May-05 ---5 ND ND ND ND ND ND ND ND ---ND
Oct-05 ---5 ND ND ND ND ND ND ND ND ---ND
23-May-06 ---5 ND ND ND ND ND ND ND ND ---ND
09-Nov-06 ---5 ND ND ND ND ND ND ND ND ---ND
19-Jun-07 0.1 5.0 ND ND ND ND ND (ND)ND ND ND ---ND
NC 2L = 24 µg/L (10/23/07)28-Nov-07 0.1 5.0 ND ND ND ND (ND)ND ND ND ND ---ND
NC 2B = NE (05/01/07)21-Apr-08 0.1 5.0 ND ND ND ND (ND)0.4 J ND ND ND ---ND
22-Dec-08 0.1 5.0 ND ND ND (ND)ND 0.3 J ND ND ND ---ND
23-Jun-09 0.1 5.0 ND ND (ND)ND ND 0.4 J ND ND ND ---ND
15-Dec-09 0.1 5.0 ND ND ND ND (ND)0.4 J ND ND ND ---ND
NC 2L = 20 µg/L (01/01/10)28-Jun-10 0.1 5.0 ND ND ND ND 0.2 (0.2 J)J ND ND ND ---ND
02-Nov-10 0.1 5.0 ND ND ND (ND)ND ND ND ND ND ---ND
12-Apr-11 0.30 5.0 ND ND ND ND 0.34 J ND ND ND ---ND
18-Oct-11 0.30 5.0 ND ND ND ND 0.32 J ND ND ------ND
10-Apr-12 0.30 5.0 ND ND ND ND 0.32 J ND ND ------ND
15-Oct-12 0.30 5.0 ND ND ND ND ND ND ND ------ND
16-Apr-13 0.30 5.0 0.81 J ND ND ND 0.38 J ND ND ND ---ND
08-Oct-13 0.30 5.0 ND ND ND ND 0.37 J ND ND ------ND
29-Apr-14 0.30 5.0 ND ND ND ND 0.45 J ND ND ------ND
14-Oct-14 0.30 5.0 ND ND ND ND 0.33 J ND ND ------ND
09-Apr-15 0.30 5.0 ND ND ND 1.2 J ND ND ND ------ND
27-Oct-15 0.30 5.0 ND ND ND ND 0.32 J ND ND ND ---ND
21-Apr-16 0.076 5.0 ND ND ND ND ND ND ND ------ND
11-Oct-16 0.30 5.0 ND ND ND ND 0.33 J ND ND ------ND
18-Apr-17 0.30 5.0 ND ND ND ND 0.34 J ND ND ------ND
19-Oct-17 0.30 5.0 ND ND ND ND ND ND ND ------ND
1,4-Dichlorobenzene Mar-98 ---5 ND ND ND 6 7 ND ND ND ---ND
Sep-98 ---5 ND ND ND 5 5 ND ND ND ---ND
Mar-99 ---5 ND ND ND ND 5 ND ND ND ---ND
Sep-99 ---5 ND ND ND 7.8 ND ND ND ND ---ND
May-00 ---5 ND ND ND 6.9 6 ND ND ND ---ND
Oct-00 ---5 ND ND ND 6.1(5.7)5 ND ND ND ---ND
Mar-01 ---5 ND ND ND ND 5.5 ND ND ND ---ND
Oct-01 ---5 ND ND ND ND 5.3 ND ND ND ---ND
Apr-02 ---5 ND ND ND ND ND ND ND ND ---ND
Nov-02 ---5 ND ND ND ND ND ND ND ND ---ND
May-03 ---5 ND ND ND 5.0(5.1)5.8 ND ND ND ---ND
Nov-03 ---5 ND ND ND ND 5.5(5.0)ND ND ND ---ND
Apr-04 ---5 ND ND ND ND 6.0 ND ND ND ---ND
Oct-04 ------ND ND ND ND 5.3 ND ND ND ---ND
May-05 ---5 ND ND ND ND ND ND ND ND ---ND
Oct-05 ---5 ND ND ND ND ND ND ND ND ---ND
23-May-06 ---5 ND ND ND ND ND ND ND ND ---ND
09-Nov-06 ---5 ND ND ND ND ND ND ND ND ---ND
19-Jun-07 0.1 1.0 ND ND ND 2.2 4.8 (5.0)ND ND 2.8 ---ND
NC 2L = 1.4 µg/L (10/23/07)28-Nov-07 0.1 1.0 ND ND ND 2.8 (3.2)3.2 ND ND 1.4 ---ND
NC 2B = NE (05/01/07)21-Apr-08 0.1 1.0 ND ND ND 3.3 (3.3)4.5 ND ND 1.6 ---ND
22-Dec-08 0.1 1.0 ND ND ND (ND)2.1 4.4 ND ND 1.2 ---ND
23-Jun-09 0.1 1.0 ND ND (3.3)ND 1.6 4.1 ND ND 2.3 ---ND
15-Dec-09 0.1 1.0 ND ND ND 2.2 (2.0)4.8 ND ND 1.8 ---ND
NC 2L = 6 µg/L (01/01/10)28-Jun-10 0.1 1.0 0.1 J ND ND 1.0 3.4 (3.4)ND ND 1.8 ---ND
02-Nov-10 0.1 1.0 ND ND ND (ND)1.6 2.9 ND ND 1.3 ---ND
12-Apr-11 0.33 1.0 ND ND ND ND 4.6 ND ND ND ---ND
18-Oct-11 0.33 1.0 0.53 J ND ND 2.6 4.2 ND ND ------ND
10-Apr-12 0.33 1.0 0.38 J ND ND 2.0 4.2 ND ND ------ND
15-Oct-12 0.33 1.0 0.41 J ND ND 1.9 3.3 ND ND ------ND
16-Apr-13 0.33 1.0 ND ND 1.2 ND 4.6 ND ND ND ---ND
08-Oct-13 0.33 1.0 0.50 J ND ND 2.1 4.4 ND ND ------ND
29-Apr-14 0.33 1.0 ND ND ND 1.6 5.1 ND ND ------ND
14-Oct-14 0.33 1.0 ND ND ND 2.4 3.7 ND ND ------ND
09-Apr-15 0.33 1.0 0.36 J ND ND 1.1 3.0 ND ND ------ND
27-Oct-15 0.33 1.0 0.45 J ND ND 2.2 3.4 ND ND ND ---ND
21-Apr-16 0.05 1.0 ND ND ND 2.6 4.6 ND ND ------ND
11-Oct-16 0.33 1.0 ND ND ND 3.5 3.7 ND ND ------ND
18-Apr-17 0.33 1.0 0.35 J ND ND 2.2 3.9 ND ND ------ND
19-Oct-17 0.33 1.0 0.40 J ND ND 2.4 4.0 ND ND ------ND
APPENDIX 3
Summary of Historically Detected Constituents
Wilkes County Germantown Landfill
Permit No. 97-01 page 13 of 13 Joyce Engineering
Analyte DL QL MW-1 MW-2 MW-3 MW-4 MW-5 Upstream Downstream Outfall #1 Outfall #2 Blanks
Sample Collection
Date
Methylene Chloride 16-Apr-13 0.97 1.0 2.4 B 2.7 B 2.6 B 2.7 B 2.4 B 2.5 B 2.5 B 2.5 B ---3.2
NC 2L = 5µg/L (01/01/10)08-Oct-13 0.97 1.0 ND ND ND ND ND ND ND ------1.2
NC 2B = NE (05/01/07)29-Apr-14 0.97 1.0 ND ND ND ND ND ND ND ------ND
14-Oct-14 0.97 1.0 ND ND ND ND ND ND ND ------ND
09-Apr-15 0.97 1.0 ND ND ND ND ND ND ND ------1.3
27-Oct-15 0.97 1.0 ND ND ND ND ND ND ND ND ---ND
21-Apr-16 0.083 1.0 ND ND ND ND ND ND ND ------ND
11-Oct-16 0.97 1.0 ND ND ND ND ND ND ND ------ND
18-Apr-17 0.97 1.0 ND ND ND ND ND ND ND ------1.2 C9
19-Oct-17 0.97 1.0 ND ND ND ND ND ND ND ------ND
Styrene 16-Apr-13 0.26 1.0 0.78 J ND ND ND ND ND ND ND ND ND
NC 2L = 70µg/L (01/01/10)08-Oct-13 0.26 1.0 ND ND ND ND ND ND ND ------ND
NC 2B = NE (05/01/07)29-Apr-14 0.26 1.0 ND ND ND ND ND ND ND ------ND
14-Oct-14 0.26 1.0 ND ND ND ND ND ND ND ------ND
09-Apr-15 0.26 1.0 ND ND ND ND ND ND ND ------ND
27-Oct-15 0.26 1.0 ND ND ND ND ND ND ND ND ---ND
21-Apr-16 0.047 1.0 ND ND ND ND ND ND ND ------ND
11-Oct-16 0.26 1.0 ND ND ND ND ND ND ND ------ND
18-Apr-17 0.26 1.0 ND ND ND ND ND ND ND ------ND
19-Oct-17 0.26 1.0 ND ND ND ND ND ND ND ------ND
Toluene 16-Apr-13 0.26 1.0 0.37 J ND ND ND ND ND ND ND ND ND
NC 2L = 600µg/L (01/01/10)08-Oct-13 0.26 1.0 ND ND ND ND ND ND ND ------ND
NC 2B = 11 (05/01/07)29-Apr-14 0.26 1.0 ND ND ND ND ND ND ND ------ND
14-Oct-14 0.26 1.0 ND ND ND ND ND ND ND ------ND
09-Apr-15 0.26 1.0 ND ND ND ND ND ND ND ------ND
27-Oct-15 0.26 1.0 ND ND ND ND ND ND ND ND ---ND
21-Apr-16 0.044 1.0 ND ND ND ND ND ND ND ------ND
11-Oct-16 0.26 1.0 ND ND ND ND ND ND ND ------ND
18-Apr-17 0.26 1.0 ND ND ND ND ND ND ND ------ND
19-Oct-17 0.26 1.0 ND ND ND ND ND ND ND ------ND
Xylene (Total)Apr-02 ---5 ND 9.3 ND ND ND ND ND ND ---ND
Nov-02 ---5 ND ND ND ND ND ND ND ND ---ND
May-03 ---5 ND ND ND ND ND ND ND ND ---ND
Nov-03 ---5 ND ND ND ND ND ND ND ND ---ND
Apr-04 ---5 ND ND ND ND ND ND ND ND ---ND
Oct-04 ------ND ND ND ND ND ND ND ND ---ND
May-05 ---5 ND ND ND ND ND ND ND ND ---ND
Oct-05 ---5 ND ND ND ND ND ND ND ND ---ND
23-May-06 ---5 ND ND ND ND ND ND ND ND ---ND
09-Nov-06 ---5 ND ND ND ND ND ND ND ND ---ND
19-Jun-07 0.3 4.0 ND ND ND ND ND (ND)ND ND ND ---ND
NC 2L = 530 µg/L (10/23/07)28-Nov-07 0.3 4.0 ND ND ND ND (ND)ND ND ND ND ---ND
NC 2B = NE (05/01/07)21-Apr-08 0.3 4.0 ND ND ND ND (ND)0.4 J ND ND 1.3 J ---ND
22-Dec-08 0.3 4.0 ND ND ND (ND)ND ND ND ND ND ---ND
23-Jun-09 0.3 4.0 ND ND (ND)ND ND ND ND ND 1.2 J ---ND
15-Dec-09 0.3 5.0 ND ND ND ND (ND)ND ND ND 1.2 J ---ND
NC 2L = 5,000 µg/L (01/01/10)28-Jun-10 0.3 5.0 ND ND ND ND ND (ND)ND ND ND ---ND
02-Nov-10 0.3 5.0 ND ND ND (ND)ND ND ND ND ND ---ND
12-Apr-11 0.66 2.0 ND ND ND ND ND ND ND ND ---ND
18-Oct-11 0.66 2.0 ND ND ND ND ND ND ND ------ND
10-Apr-12 0.66 2.0 ND ND ND ND ND ND ND ------ND
15-Oct-12 0.66 5.0 ND ND ND ND ND ND ND ------ND
16-Apr-13 0.66 5.0 ND ND ND ND ND ND ND ND ---ND
08-Oct-13 0.66 5.0 ND ND ND ND ND ND ND ------ND
29-Apr-14 0.66 5.0 ND ND ND ND ND ND ND ------ND
14-Oct-14 0.66 5.0 ND ND ND ND ND ND ND ------ND
09-Apr-15 0.66 5.0 ND ND ND ND ND ND ND ------ND
27-Oct-15 0.66 5.0 ND ND ND ND ND ND ND ND ---ND
21-Apr-16 0.15 5.0 ND ND ND ND 0.52 J ND ND ------ND
11-Oct-16 0.66 5.0 ND ND ND ND ND ND ND ------ND
18-Apr-17 0.66 5.0 ND ND ND ND ND ND ND ------ND
19-Oct-17 0.66 5.0 ND ND ND ND ND ND ND ------ND
Notes:
All concentrations are reported in micrograms per liter (mg/L).
Values shown in parentheses are from duplicate samples.
MW = Groundwater monitoring well.
DL = Laboratory detection limit.
QL = Laboratory reporting limit ( NC SWSL {or lower} From June 2007 to present).
B = Reported detect considered to represent blank contamination.
--- = Not sampled and/or not reported
NC 2L = North Carolina's groundwater quality Standard established under 15A NCAC 2L, .0202.
J = Estimate concetrations.
GWPS = Groundwater Protection Standards.
NC 2B = North Carolina Surface Water Standard.
Bold = values above the NC 2L, GWPS and/or NC 2B.