9801_WilsonCounty_MSWLF_GWMR

May 31, 2017

Mr. Ervin Lane, Hydrogeologist
NC Division of Waste Management
Solid Waste Section
Mail Service Center 1646
Raleigh, NC 27699-1646

Re: 2017 First Semi-Annual Water Quality Monitoring Results
Closed Wilson County Landfill
Wilson, North Carolina
Permit #98-01

Dear Ervin:

Babb & Associates, P.A. has completed the 2017 first semi-annual sampling event at the closed Wilson
County Landfill. On May 10, 2017, nine groundwater monitoring wells and five surface water monitoring
stations were sampled and analyzed for volatile organic compounds (VOCs) by EPA Method 8260 and
Appendix I inorganic compounds.

A site map is provided with this report which shows the groundwater and surface water sample locations
and shallow potentiometric surface. Additional attachments to this report include tables summarizing the
groundwater and surface water analytical results (Tables 1 & 2), field parameters collected during the
monitoring event (Table 3), well construction information (Table 4), and groundwater flow rates (Table 5).
The laboratory analytical report, in pdf and EDD formats, is included as Appendix A.

If there are any questions regarding the attached information, please contact me at [phone].

Respectfully,

Babb & Associates, P.A.

Gary D. Babb, P.G.
President

Enclosures

cc: Mr. Andy Davis, Director
Wilson County Solid Waste

Water Quality Monitoring Report

Wilson County Municipal Solid Waste Landfill
2400 Highway 42 East
Wilson, North Carolina
Permit No. 98-01

Prepared for:

Wilson County Solid Waste
P.O. Box 1728
Wilson, North Carolina 27894

Prepared by:

Babb & Associates, P.A.
P.O. Box 37697
Raleigh, North Carolina 27627

May 2017

___________________________________
Gary D. Babb, Licensed Geologist

Table of Contents

1.0 Introduction 1
1.1 Site Information
1.2 Site Geology
1.3 Site Hydrogeology

2.0 Water Quality Monitoring Program 5
2.1 Groundwater Monitoring Network
2.2 Surface Water Monitoring Network

3.0 Water Quality Sample Collection 7
3.1 Field Sample Procedures
3.2 Field Quality Assurance
3.3 Sample Delivery/Chain-of-Custody

4.0 Laboratory Analysis 9

5.0 Hydrogeological Conditions 10

6.0 Laboratory Analytical Results 11
6.1 Groundwater Analytical Results
6.2 Surface Water Analytical Results
6.3 Quality Control Sample

7.0 Conclusions 14

Figure 1 Water Quality Monitoring Sample Locations/Potentiometric Map

Table 1 Groundwater Analytical Results
Table 2 Surface Water Analytical Results
Table 3 Field Parameter Measurements
Table 4 Well Construction Information/Elevations
Table 5 Groundwater Flow Rates

Appendix A ENCO Laboratory Analytical Report

Wilson County Closed Landfill Water Quality Monitoring Report
May 2017 Page 1

1.0 Introduction

1.1 Site Information

The closed Wilson County Landfill is located approximately 3.5 miles east of downtown
Wilson, NC at the intersection of NC 42 and Tucker Court. Originally, the site of the
closed Wilson County Landfill facility was dominated by a hill (approximately 108 feet
above msl) located in the central portion of the present site. Several residential/farm
houses were located in the northeast portion of the site. An intermittent stream
originating in the northern portion of the site flowed southeastward eventually flowing
into an unnamed stream southeast of the site. This unnamed stream flowed westward
becoming part of the southern site boundary and traversed the southwestern most portion
of the site and emptied into the Toisnot Swamp Canal. The remainder of the site
contained drainage features that radiated outward from the dominant hill and discharged
into these streams or with other drainage features located to the northwest of the site.
Wetland areas were associated with streams and the Toisnot Swamp. Prior to
construction of the landfill facility, agriculture was the primary land use in this area of
Wilson County.

Surrounding properties within 1,500 feet of the site are currently being used for farming,
residential, or solid waste management purposes. Land south of the site is mostly
farmland with a mobile home park located approximately 1,200 feet to the south. Land
immediately west of the site is owned by Wilson County and used for construction and
demolition debris disposal, recycling/reclaimation, and other solid waste management
activities. Land north of the site is mostly used for farmland with wooded areas. Land
east of the site is mostly farmland with wooded areas and light residential use.

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May 2017 Page 2

1.2 Site Geology

The closed Wilson County Landfill is located in the western portion of the Carolina
Coastal Plain near the Fall Line. The Fall Line is the province boundary between the
Piedmont and the Coastal Plain provinces. It represents a significant change in lithology,
which in turn reflects a change in stream gradients. Lithology of the Piedmont province
is primarily igneous and metamorphic while the Coastal Plain province is primarily
sedimentary. In general, rivers and streams in the Piedmont Province have higher flow
rates with well defined channels while Coastal Plain rivers and streams are meandering
with lesser defined channels resulting in swamps and bays. These streams, swamps, and
bays are the major discharge point of the uppermost aquifer.

The Carolina Coastal Plain is underlain by flat-lying to very gently eastward dipping
sedimentary strata which overlay a foundation of crystalline rocks. These sediments
were deposited during repeated marine transgressive and regressive cycles due to
fluctuations in sea level caused by expansion and recession of glacial ice caps during the
Pliocene and early Pleistocene epochs (approximately 2 to 5 million years ago).

Sediments in the area of the closed Wilson County Landfill facility are classified as being
in the Yorktown Formation. Information gathered from the Geologic Map of North
Carolina, 1985 and The Geology of the Carolina, 1991, cites that sediments of the
Yorktown Formation are fossiliferous clay with varying amounts of fine-grained sand,
silty sand, sandy silt, silty clay, and bluish gray shell material. These types of deposits
are found mainly north of the Neuse River and are commonly concentrated in lenses and
vary in vertical and horizontal dimensions. The topography of the Coastal Plain is
characterized by flat to gently undulating relief.

The local geology is characterized by relatively thin layers (0.5 - 7.0 feet) of clays, silts,
and sands in varying textures and colors that overlie a gray/black silty clay/sand that is
found throughout the area. The drainage canals located on the northwest and southeast
Wilson County Closed Landfill Water Quality Monitoring Report
May 2017 Page 3

property boundaries expose these silty clay and sand layers. The original soils at the site
were excavated to create capacity for waste disposal.

1.3 Site Hydrogeology

The major groundwater discharge features influencing groundwater flow direction at the
site are the Toisnot Swamp and drainage ditches located to the southeast and northwest of
the site. Groundwater level measurements collected on May 10, 2017 indicate that the
general groundwater flow direction on the facility is to the south-southeast towards the
Toisnot Swamp Canal. However, the presence of drainage ditches have an impact on
localized groundwater flow. Groundwater flow near the southeastern drainage ditch
tends to be in a more southerly direction towards the drainage ditch. A Potentiometric
Map indicating groundwater flow directions is provided as Figure 1.

Aquifer hydraulic conductivity testing was performed in June 1997 on five of the site
monitoring wells and consisted of rising and falling head tests (slug tests). The results of
the slug test data was analyzed using the Bouwer and Rice method and are summarized
on the table below:

WELL ID HYDRAULIC
CONDUCTIVITY
(centimeters/second)
TYPE OF TEST FORMATION
MW-3A 3.80 x 10-5 Falling Yorktown
P-3 1.27 x 10-4 Rising Alluvium/Yorktown
MW-4 1.01 x 10-4 Rising Alluvium
MW-4 5.89 x 10-4 Falling Alluvium
MW-5 8.50 x 10-5 Rising Alluvium
MW-5 2.06 x 10-4 Falling Alluvium
MW-6 1.85 x 10-4 Rising Yorktown
MW-6 6.53 x 10-4 Falling Yorktown
MW-7 1.66 x 10-4 Rising Alluvium
MW-7 1.95 x 10-4 Falling Alluvium

Wilson County Closed Landfill Water Quality Monitoring Report
May 2017 Page 4

The geometric average of the shallow water table aquifer hydraulic conductivity is 2.56 x
10-4 cm/sec (0.73 feet per day). This value may be considered a reasonable estimate of
the hydraulic conductivity of the shallow water table aquifer at the closed Wilson County
Landfill site.

Wilson County Closed Landfill Water Quality Monitoring Report
May 2017 Page 5

2.0 Water Quality Monitoring Program

The water quality monitoring network at the closed Wilson County Landfill is evaluated on a
semi-annual basis. The location of the groundwater and surface water samples collected during
the semi-annual monitoring events is shown on the attached Figure 1.

2.1 Groundwater Monitoring Network

There are nine groundwater monitoring wells located at the facility that comprise the
existing groundwater monitoring system (Figure 1). Monitoring well MW-1A is located
to the northwest of the landfill area and serves as the sidegradient groundwater
monitoring well. This well is situated on the northwest edge of the drainage ditch that
separates former fill and borrow areas. Monitoring well MW-2 is located at the entrance
to the landfill at Landfill Road (SR 1503) and serves as the upgradient groundwater
monitoring well providing background water quality. Monitoring well MW-3 is located
on the landfill side of the drainage ditch on the southeast property boundary of the
landfill. Monitoring well MW-3A, added in 2004, is also located on the southeastern side
of the landfill but on the opposite side of the drainage ditch. Monitoring wells MW-4 and
MW-5 are both located to the southwest and downgradient of the landfill but
hydraulically upgradient of the Toisnot Swamp Canal. Monitoring wells MW-6 and
MW-7 are located on the southeast border of the landfill. Monitoring well MW-8 is
considered a side-gradient monitoring well to the west of the former landfill area.

Table 4 provides monitoring well construction information including installation date,
well depth/screened interval, survey elevations, and lat/long for each well location. Table
5 provides the estimated hydraulic conductivity values for select monitoring wells based
on falling/rising head slug tests.

Wilson County Closed Landfill Water Quality Monitoring Report
May 2017 Page 6

2.2 Surface Water Monitoring Network

There are presently five surface water monitoring stations associated with the closed
Wilson County Landfill. Surface water monitoring stations SW-1 and SW-2 are both
located on the Toisnot Swamp Canal. The upstream sampling location (SW-1) is located
approximately 400 feet northwest of the landfill property boundary. The downstream
sampling location (SW-2) is located approximately 1,100 feet southeast of the landfill
property boundary. The drainage canal located along the southeastern boundary of the
landfill is monitored with surface water stations SW-3 and SW-4. The drainage canal
located on the northwestern boundary of the landfill is monitoring with surface water
station SW-5. These surface water monitoring locations are shown on Figure 1.

Wilson County Closed Landfill Water Quality Monitoring Report
May 2017 Page 7

3.0 Water Quality Sample Collection

Samples of groundwater and surface water were collected in accordance with the approved
Wilson County 1996 Water Quality Monitoring Plan and the 2008 NC Solid Waste Section
Guidelines for Groundwater, Soil, and Surface Water Sampling Guidance Document. A brief
description of the sample collection procedure is provided below.

3.1 Field Sample Procedures

Prior to groundwater sampling, water levels were obtained from each well using an
electric water level meter capable of measuring the depth to water to the nearest 0.01 feet.
This information was later used to determine the elevation of the water table in each
monitoring well relative to surveyed datum (Table 3). The depth to water in each well
was also used to determine the volume of standing water in the well casing. This
information allowed for the purging of a minimum of three casing volumes from each
well prior to sample collection to assure a fresh groundwater sample was collected. New
disposable laboratory gloves were worn by sampling personnel and each well was purged
and sampled with a new disposable bailer which was discarded after use.

After the monitoring wells had been allowed to recover from purging, samples were
collected in the following order:

 Volatile organic compounds
 Inorganic compounds
 Field Parameters (pH, Conductivity, Temperature)

The samples are collected directly in the laboratory-supplied containers which are pre-
filled with the appropriate preservative. No filtering of the samples is performed prior to
collection. After collection, the samples are placed in a cooler on ice for overnight
shipment to the analytical laboratory.

Wilson County Closed Landfill Water Quality Monitoring Report
May 2017 Page 8

Surface water samples are collected directly into the laboratory-supplied containers as
grab samples. Sampling personnel wear new disposable laboratory gloves for each
surface water sample collected. As with the groundwater samples, these samples are
stored in a cooler on ice prior to overnight delivery to the analytical laboratory.

3.2 Field Quality Assurance

One trip blank sample was prepared by the analytical laboratory and accompanied the
sample shipment until receipt back at the laboratory. The trip blank sample was analyzed
for volatile organic compounds. Temperature blanks are also provided with the sample
shipments to assure the proper temperature is maintained until delivery to the analytical
laboratory.

3.3 Sample Delivery/Chain of Custody

All groundwater and surface water samples are stored in coolers on ice immediately after
collection. Individual sample containers for each well or surface water sample are placed
in zip lock plastic bags to reduce the potential for cross contamination. Chain-of-Custody
control documents are prepared and shipped with each cooler. Custody seals are also
used for each cooler to maintain sample integrity until delivery to the analytical
laboratory. The sample coolers are shipped via Federal Express for next morning
delivery to the analytical laboratory.

Wilson County Closed Landfill Water Quality Monitoring Report
May 2017 Page 9

4.0 Laboratory Analysis

The samples were analyzed for parameters specified by the Solid Waste Section for Detection
Monitoring at permitted solid waste facilities. The standard Detection Monitoring Program for
groundwater and surface water samples consists of the Appendix I parameters. The Appendix I
analysis consists of volatile organic compounds by EPA Method 8260B and inorganic
compounds by EPA Methods 6010C/6020A.

The laboratory performing the water quality analysis is Environmental Conservation
Laboratories, Inc. (ENCO) of Cary, North Carolina, which is a NC Certified Laboratory.
Internal quality control samples, including matrix spikes/matrix spike duplicates, are performed
by ENCO for each set of samples. The ENCO laboratory report, including internal quality
control samples, is provided with this report in Appendix A.

Wilson County Closed Landfill Water Quality Monitoring Report
May 2017 Page 10

5.0 Hydrogeological Conditions

The depth to groundwater was measured in the nine compliance monitoring wells during the
May 10, 2017 monitoring event. The groundwater elevations were calculated relative to the
surveyed measuring point (top of casing) for each monitoring well. The groundwater elevations
are summarized on Table 3 and the potentiometric surface of the shallow water table is shown on
Figure 1.

The general direction of groundwater flow, based on the water level information collected during
this monitoring event, is also shown on Figure 1. Groundwater flow direction is generally to the
south-southwest, toward the Toisnot Swamp Canal.

Based on the results of prior hydrologic tests conducted at the site, groundwater flow rate in the
shallow saprolite ranges from 0.108 ft/day to 1.85 ft/day. The average hydraulic conductivity
and transmissivity values for the site are provided on Table 5.

Wilson County Closed Landfill Water Quality Monitoring Report
May 2017 Page 11

6.0 Laboratory Analytical Results

Final laboratory analytical results for the samples collected on May 10, 2017 were received from
the analytical laboratory on May 24, 2017. A summary of the analytical results are provided on
Table 1 (groundwater), Table 2 (surface water), and Table 3 (field parameters).

6.1 Groundwater Analytical Results

During this monitoring event, only one volatile organic compound (VOC) was reported
above the laboratory reporting limits. Monitoring well MW-7 reported the compound
cis-1,2-dichloroethene at a concentration of 17 ug/l which is well below the established
NC 2L Groundwater Standard of 70 ug/l. No other VOCs were detected at
concentrations exceeding the laboratory reporting limits, Solid Waste Section Limits
(SWSLs), or the NC 2L Groundwater Standards in any of the remaining eight
groundwater monitoring wells.

No inorganic compounds were detected at a concentration that exceeded the NC 2L
Groundwater Standards in any of the nine groundwater monitoring wells sampled during
this monitoring event. The inorganic compound barium was reported above the
laboratory detection limit and SWSL in monitoring wells MW-1A, MW-2, MW-3, MW-
3A, MW-4, MW-5, and MW-7; however, the reported concentrations did not exceed the
established NC 2L Groundwater Standard. The inorganic compound beryllium was
reported above the laboratory detection limit and SWSL in monitoring wells MW-3 and
MW-6; however, the reported concentrations did not exceed the established NC 2L
Groundwater Standard. Monitoring well MW-6 also reported a detectable concentration
of cobalt, which does not have an established NC 2L Groundwater Standard. Monitoring
wells MW-1A, MW-3, MW-5, MW-6, and MW-8 reported detectable concentrations of
zinc, although the concentrations were well below the established NC 2L Groundwater
Standard. A summary of the groundwater laboratory analytical results and the
corresponding NC 2L Groundwater Standard is provided on Table 1.

Wilson County Closed Landfill Water Quality Monitoring Report
May 2017 Page 12

6.2 Surface Water Analytical Results

During sampling of the five surface water monitoring stations, the compound toluene was
reported above the laboratory reporting limit in surface water samples SW-3 (3.4 ug/l)
and SW-5 (12.0 ug/l). The reported concentration of toluene at SW-5 is slightly above
the established NC 2B Surface Water Standard of 11.0 ug/l. No other VOCs were
reported in any of the surface water samples above the SWSLs, laboratory detection
limits, or 2B Surface Water Standards.

The inorganic compound zinc was reported above the laboratory detection limit in four of
the five surface water samples with the reported concentration in SW-3 (113 ug/l)
exceeding the 2B Surface Water Standard of 50 ug/l. The inorganic compound arsenic
was also reported in surface water sample SW-3 at a concentration of 10.1 ug/l which
slightly exceeds the 2B Surface Water Standard of 10 ug/l. The surface water sample
SW-3 also reported concentrations of cobalt (11.2 ug/l) and lead (27.6 ug/l) which
slightly exceed the established 2B Surface Water Standards of 3 ug/l and 25 ug/l,
respectively.

The inorganic compound barium was reported above the laboratory detection limit in
SW-1, SW-2, SW-3, SW-4, and SW-5; however, the reported concentrations were well
below the established 2B Surface Water Standard for barium. The inorganic compound
beryllium was reported in surface water sample SW-3 above the SWSLs but below the
2B Surface Water Standard. The inorganic compound vanadium was reported in surface
water sample SW-3 above the SWSLs, however there is no 2B Surface Water Standard
for vanadium. No other inorganic compounds were reported above the laboratory
detection limits or NC 2B Surface Water Standards in the samples collected from the five
surface water monitoring stations. A summary of the surface water analytical results and
corresponding NC 2B Surface Water Standard for the five surface water samples is
provided on Table 2.

Wilson County Closed Landfill Water Quality Monitoring Report
May 2017 Page 13

6.3 Quality Control Sample

One trip blank was submitted and analyzed for quality assurance purposes. No VOCs
were detected at a concentration equaling or exceeding laboratory quantitation limits in
the trip blank.

Wilson County Closed Landfill Water Quality Monitoring Report
May 2017 Page 14

7.0 Conclusions

The results of this monitoring event report only minor variants from the established NC 2L
Groundwater Standards and NC 2B Surface Water Standards. Based on the results of this water
quality monitoring event, the closed Wilson County Landfill will remain in Detection
Monitoring in accordance with Title 15A NACA 13B .0601. The 2017 fall semi-annual water
quality monitoring event is tentatively scheduled for October 2017.

Attachments to this report include tables summarizing the groundwater and surface water
analytical results (Tables 1 & 2), field parameters collected during the monitoring event (Table
3), well construction information (Table 4), and hydrologic test results (Table 5). A copy of the
laboratory analytical report in pdf and EDD formats is included with this report in Appendix A.

SITE MAP

TABLES

TABLE 12017 First Semi-Annual Groundwater Laboratory Analytical ResultsWilson County MSWLFWilson, North CarolinaPermit #98-01Parameter MW-1A MW-2 MW-3 MW-3A MW-4 MW-5 MW-6 MW-7 MW-8 2L Std.Metals (ug/l) Barium 208 66 103 298 581 644 46.6 J 112 61.2 J 700Beryllium 0.659 J BQL 1.45 BQL BQL BQL 2.63 0.174 J 0.324 J NECadmium BQL BQL BQL BQL BQL BQL 0.773 J BQL BQL 2Chromium 1.41 J BQL BQL BQL BQL 3.43 J BQL BQL BQL 10Cobalt 7.26 J BQL 3.48 J BQL BQL 2.37 J 25.2 BQL 4.88 J NECopper 1.82 J BQL BQL BQL BQL BQL BQL BQL BQL 1000Nickel 10.1 J BQL 7.37 J BQL BQL 4.95 J 40.3 J BQL 2.44 J 100Selenium BQL BQL BQL BQL BQL BQL 1.04 J BQL BQL 20Silver 2.19 J BQL BQL 2.17 J BQL BQL BQL BQL BQL 20Vanadium 1.67 J BQL BQL BQL BQL 3.80 J 8.35 J 2.93 J BQL NEZinc 16.2 BQL 18.7 BQL BQL 12.3 52.6 9.41 J 11.8 1000Method 8260B (ug/l) 1,1-Dichloroethane BQL BQL BQL BQL BQL BQL BQL 1.6 J BQL 6cis-1,2-Dichloroethene BQL BQL BQL BQL BQL BQL BQL 17.0 BQL 70Notes:Samples collected on May 10, 2017BQL - Below laboratory quantitation limit.Bold concentrations equal or exceed established or interim standards.NE - Not established.J - Between MDL and RL
TABLE 22017 First Semi-Annual Surface Water Laboratory Analytical ResultsWilson County MSWLFWilson, North CarolinaPermit #98-01Parameter SW-1 SW-2 SW-3 SW-4 SW-5 2B Std.Metals (ug/l) Arsenic BQL BQL10.1BQL 7.68 J 10Barium 153 69.8 J 237 78.5 229 1000Beryllium BQL BQL 2.09 BQL 0.287 J 6.5Cadmium BQL BQL 0.528 J BQL BQL 2Chromium BQL BQL 8.18 J BQL 2.46 J 50Cobalt 1.96 J 1.95 J11.22.39 J 4.88 J 3Copper BQL BQL 9.62 J 1.85 J BQL 7Lead BQL BQL27.6BQL BQL 25Nickel BQL BQL 19.6 J BQL 3.42 J 88Silver BQL BQL BQL BQL 1.94 J 0.06Vanadium 1.54 J BQL 34.5 1.41 J 3.08 J NEZinc 15.4 9.97 J11314.0 13.8 50Method 8260B (ug/l)4-Methyl-2-pentanone BQL BQL BQL BQL 1.1 J 26cis-1,2-Dichloroethene BQL 1.2 J BQL 1.2 J BQL 330Toluene 0.50 J BQL 3.4 BQL12.011Notes:Samples collected on May 10, 2017BQL - Below laboratory quantitation limit.Bold concentrations equal or exceed established or interim standards.NE - Not established.J - Between MDL and RL
TABLE 32017 First Semi-Annual Field ParametersWilson County MSWLFWilson, North CarolinaPermit #98-01Monitoring WellSample Date Sample Time Depth to GW GW Elevation Conductivity Temperature - C pHMW-1A 5/10/2017 1157 15.25 94.14 492 20.4 7.1MW-2 5/10/2017 1418 4.75 115.29 111 17.1 5.0MW-3 5/10/2017 1347 16.53 91.61 137 18.5 6.0MW-3A 5/10/2017 1353 19.29 96.14 349 19.1 7.5MW-4 5/10/2017 1229 2.71 82.11 1205 17.7 6.6MW-5 5/10/2017 1304 4.42 82.72 1269 17.7 6.6MW-6 5/10/2017 1353 21.61 87.85 249 17.8 4.4MW-7 5/10/2017 1330 7.19 83.41 194 18.0 6.6MW-8 5/10/2017 1206 8.22 84.04 127 20.6 5.4SW-1 5/10/2017 1254 NA NA 408 20.1 7.4SW-2 5/10/2017 1245 NA NA 138 18.9 7.3SW-3 5/10/2017 1357 NA NA 289 16.3 4.1SW-4 5/10/2017 1236 NA NA 135 18.5 7.8SW-5 5/10/2017 1310 NA NA 742 18.7 7.5
TABLE 4Groundwater Monitoring Well ConstructionWilson County MSW LandfillWilson, North CaroliinaPermit #98-01Well IDDate DrilledWell DiameterTotal DepthTOS DepthScreened IntervalGround ElevationTOC ElevationGroundwater DepthGroundwater ElevationLat/Long GeologyMW-1A 6/3/04 2" 30.0' 15.0' 15' - 30' 107.10 109.39 15.25 94.14717305.1 N 2340146.21 Esilty sandy CLAYMW-2 4/26/89 2" 14.0' 4.0' 4' - 14' 118.02 120.04 4.75 115.29717575.76 N 2342716.01 Esilty sandy CLAYMW-3 6/3/04 2" 25.0' 10.0' 10' - 25' 105.86 108.14 16.53 91.61716665.86 N 2341686.99 Efine SANDMW-3A 5/15/97 2" 34.0' 24.0' 24' - 34' 113.74 115.43 19.29 96.14716681.30 N 2341690.92 Emed. grey SILTMW-4 4/26/89 2" 13.0' 3.0' 3' - 13' 82.88 84.82 2.71 82.11715502.17 N 2339430.85 Esilty sandy CLAYMW-5 4/26/89 2" 13.0' 3.0' 3' - 13' 85.48 87.14 4.42 82.72715895.82 N 2339078.98 Esilty sandy CLAYMW-6 5/15/97 2" 28.0' 18.0' 18' - 28' 106.06 109.46 21.61 87.85716169.90 N 2341285.55 Ef. to coarse SANDMW-7 5/15/97 2" 15.0' 10.0' 10' - 15' 86.08 90.60 7.19 83.41715883.59 N 2340278.91 Esilty sandy CLAYMW-8 6/3/04 2" 20.0' 5.0' 5' - 20' 89.86 92.26 8.22 84.04716707.97 N 2339545.89 Ecoarse SANDTOS - Top of ScreenTOC - Top of CasingGroundwater depths collected on 5/10/2017
TABLE 5Groundwater Flow Rates 1Wilson County MSW LandfillWilson, North CarolinaPermit #98-01Test Piezometer Test Type 2Hydraulic Conductivity (centimeters/second)Hydraulic Conductivity (feet/day)Geologic MaterialMW-3A Falling Head 3.80 x 10-50.108 med. grey SILTMW-4 Rising Head 1.01 x 10-40.227 silty sandy CLAYMW-4 Falling Head 5.89 x 10-41.67 silty sandy CLAYMW-5 Rising Head 8.50 x 10-50.24 silty sandy CLAYMW-5 Falling Head 2.06 x 10-40.585 silty sandy CLAYMW-6 Rising Head 1.85 x 10-40.524 f. to coarse SANDMW-6 Falling Head 6.53 x 10-41.85 f. to coarse SANDMW-7 Rising Head 1.66 x 10-40.471 silty sandy CLAYMW-7 Falling Head 1.95 x 10-40.553 silty sandy CLAY1 Data from June 2003 Groundwater and Surface Water Assessment Report2 Aquifer Testing by falling/rising head slug tests, analyzed using Bouwer and Rice method

LAB REPORT

102-A Woodwinds Industrial Court
Cary NC, 27511
919.467.3090 919.467.3515Phone:FAX:www.encolabs.com
Environmental Conservation Laboratories, Inc.
ENCO Workorder(s): CA05959
Raleigh, NC 27606
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative. This report shall not be reproduced except in full, without
the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Enclosure(s)
Project Number: [none], Project Name/Desc: Wilson County MSWLF
Attn: Gary Babb
Babb & Associates (BA024)
3605 Country Cove Lane
Bill Scott
Project Manager
Wednesday, May 24, 2017
RE: Laboratory Results for
Dear Gary Babb,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Thursday, May 11, 2017.
The total number of pages in this report, including this page is 62.
Page 1 of 65
www.encolabs.com
SAMPLE SUMMARY/LABORATORY CHRONICLE
9801-MW1A CA05959-01 Sampled:05/10/17 11:57 Received:05/11/17 10:10Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 11/06/17 05/17/17 11:36 5/19/2017 10:24
EPA 6020B 11/06/17 05/18/17 10:27 5/23/2017 16:04
EPA 8260B 05/24/17 05/19/17 16:24 5/19/2017 19:58
9801-MW2 CA05959-02 Sampled:05/10/17 14:18 Received:05/11/17 10:10Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 11/06/17 05/17/17 11:36 5/19/2017 10:36
EPA 6020B 11/06/17 05/18/17 10:27 5/23/2017 16:07
EPA 8260B 05/24/17 05/18/17 00:08 5/18/2017 10:04
9801-MW3 CA05959-03 Sampled:05/10/17 13:47 Received:05/11/17 10:10Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 11/06/17 05/17/17 11:36 5/19/2017 10:39
EPA 6020B 11/06/17 05/18/17 10:27 5/23/2017 16:11
EPA 8260B 05/24/17 05/18/17 00:08 5/18/2017 10:34
9801-MW3A CA05959-04 Sampled:05/10/17 13:53 Received:05/11/17 10:10Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 11/06/17 05/17/17 11:36 5/19/2017 10:49
EPA 6020B 11/06/17 05/18/17 10:27 5/23/2017 16:15
EPA 8260B 05/24/17 05/18/17 00:08 5/18/2017 11:03
9801-MW4 CA05959-05 Sampled:05/10/17 12:29 Received:05/11/17 10:10Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 11/06/17 05/17/17 11:36 5/19/2017 10:51
EPA 6020B 11/06/17 05/18/17 10:27 5/23/2017 16:18
EPA 8260B 05/24/17 05/18/17 00:08 5/18/2017 11:33
9801-MW5 CA05959-06 Sampled:05/10/17 13:04 Received:05/11/17 10:10Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 11/06/17 05/17/17 11:36 5/19/2017 10:54
EPA 6020B 11/06/17 05/18/17 10:27 5/23/2017 16:22
EPA 8260B 05/24/17 05/18/17 00:08 5/18/2017 12:03
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9801-MW6 CA05959-07 Sampled:05/10/17 13:53 Received:05/11/17 10:10Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 11/06/17 05/17/17 11:36 5/19/2017 10:56
EPA 6020B 11/06/17 05/18/17 10:27 5/23/2017 16:25
EPA 8260B 05/24/17 05/18/17 00:08 5/18/2017 12:34
9801-MW7 CA05959-08 Sampled:05/10/17 13:30 Received:05/11/17 10:10Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 11/06/17 05/17/17 11:36 5/19/2017 10:59
EPA 6020B 11/06/17 05/18/17 10:27 5/23/2017 16:29
EPA 8260B 05/24/17 05/18/17 00:08 5/18/2017 13:04
9801-MW8 CA05959-09 Sampled:05/10/17 12:06 Received:05/11/17 10:10Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 11/06/17 05/17/17 11:36 5/19/2017 11:02
EPA 6020B 11/06/17 05/18/17 10:27 5/23/2017 16:33
EPA 8260B 05/24/17 05/18/17 00:08 5/18/2017 13:35
9801-SW1 CA05959-10 Sampled:05/10/17 12:54 Received:05/11/17 10:10Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 11/06/17 05/17/17 11:36 5/19/2017 11:04
EPA 6020B 11/06/17 05/18/17 10:27 5/23/2017 16:36
EPA 8260B 05/24/17 05/18/17 00:08 5/18/2017 14:06
9801-SW2 CA05959-11 Sampled:05/10/17 12:45 Received:05/11/17 10:10Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 11/06/17 05/17/17 11:36 5/19/2017 11:07
EPA 6020B 11/06/17 05/18/17 10:27 5/23/2017 16:48
EPA 8260B 05/24/17 05/18/17 00:08 5/18/2017 14:36
9801-SW3 CA05959-12 Sampled:05/10/17 13:57 Received:05/11/17 10:10Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 11/06/17 05/17/17 11:36 5/19/2017 11:09
EPA 6020B 11/06/17 05/18/17 10:27 5/23/2017 16:51
EPA 8260B 05/24/17 05/17/17 11:43 5/18/2017 20:06
9801-SW4 CA05959-13 Sampled:05/10/17 12:36 Received:05/11/17 10:10Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 11/06/17 05/17/17 11:36 5/19/2017 11:12
EPA 6020B 11/06/17 05/18/17 10:27 5/23/2017 16:55
EPA 8260B 05/24/17 05/17/17 11:43 5/18/2017 20:36
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9801-SW5 CA05959-14 Sampled:05/10/17 13:10 Received:05/11/17 10:10Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 11/06/17 05/17/17 11:36 5/19/2017 11:22
EPA 6020B 11/06/17 05/18/17 10:27 5/23/2017 16:59
EPA 8260B 05/24/17 05/17/17 11:43 5/18/2017 21:07
9801-Tripblank CA05959-15 Sampled:05/10/17 11:57 Received:05/11/17 10:10Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 8260B 05/24/17 05/17/17 11:43 5/18/2017 13:34
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NORTH CAROLINA SWS SAMPLE DETECTION SUMMARY
Analyte MethodUnitsResults
Lab ID:Client ID:9801-MW1A CA05959-01
Flag NotesMDLNC SWSLMRLDF
208 ug/L EPA 6010D 10010.01.001Barium - Total
0.659 ug/L EPA 6010DJ 11.000.1301Beryllium - Total
1.41 ug/L EPA 6010DJ 1010.01.401Chromium - Total
7.26 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
1.82 ug/L EPA 6010DJ 1010.01.601Copper - Total
10.1 ug/L EPA 6010DJ 5010.02.201Nickel - Total
2.19 ug/L EPA 6010DJ 1010.01.901Silver - Total
1.67 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
16.2 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-MW2 CA05959-02
Flag NotesMDLNC SWSLMRLDF
66.0 ug/L EPA 6010DJ 10010.01.001Barium - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-MW3 CA05959-03
Flag NotesMDLNC SWSLMRLDF
103 ug/L EPA 6010D 10010.01.001Barium - Total
1.45 ug/L EPA 6010D 11.000.1301Beryllium - Total
3.48 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
7.37 ug/L EPA 6010DJ 5010.02.201Nickel - Total
18.7 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-MW3A CA05959-04
Flag NotesMDLNC SWSLMRLDF
298 ug/L EPA 6010D 10010.01.001Barium - Total
2.17 ug/L EPA 6010DJ 1010.01.901Silver - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-MW4 CA05959-05
Flag NotesMDLNC SWSLMRLDF
581 ug/L EPA 6010D 10010.01.001Barium - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-MW5 CA05959-06
Flag NotesMDLNC SWSLMRLDF
644 ug/L EPA 6010D 10010.01.001Barium - Total
3.43 ug/L EPA 6010DJ 1010.01.401Chromium - Total
2.37 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
4.95 ug/L EPA 6010DJ 5010.02.201Nickel - Total
3.80 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
12.3 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-MW6 CA05959-07
Flag NotesMDLNC SWSLMRLDF
46.6 ug/L EPA 6010DJ 10010.01.001Barium - Total
2.63 ug/L EPA 6010D 11.000.1301Beryllium - Total
0.773 ug/L EPA 6010DJ 11.000.3601Cadmium - Total
25.2 ug/L EPA 6010D 1010.01.101Cobalt - Total
40.3 ug/L EPA 6010DJ 5010.02.201Nickel - Total
1.04 ug/L EPA 6020BJ 103.000.9101Selenium - Total
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Analyte MethodUnitsResults
Lab ID:Client ID:9801-MW6 CA05959-07
Flag NotesMDLNC SWSLMRLDF
8.35 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
52.6 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-MW7 CA05959-08
Flag NotesMDLNC SWSLMRLDF
1.6 ug/L EPA 8260BJ 51.00.1311,1-Dichloroethane
112 ug/L EPA 6010D 10010.01.001Barium - Total
0.174 ug/L EPA 6010DJ 11.000.1301Beryllium - Total
17 ug/L EPA 8260B 51.00.151cis-1,2-Dichloroethene
2.93 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
9.41 ug/L EPA 6010DJ 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-MW8 CA05959-09
Flag NotesMDLNC SWSLMRLDF
61.2 ug/L EPA 6010DJ 10010.01.001Barium - Total
0.324 ug/L EPA 6010DJ 11.000.1301Beryllium - Total
4.88 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
2.44 ug/L EPA 6010DJ 5010.02.201Nickel - Total
11.8 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-SW1 CA05959-10
Flag NotesMDLNC SWSLMRLDF
153 ug/L EPA 6010D 10010.01.001Barium - Total
1.96 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
0.50 ug/L EPA 8260BJ 11.00.141Toluene
1.54 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
15.4 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-SW2 CA05959-11
Flag NotesMDLNC SWSLMRLDF
69.8 ug/L EPA 6010DJ 10010.01.001Barium - Total
1.2 ug/L EPA 8260BJ 51.00.151cis-1,2-Dichloroethene
1.95 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
9.97 ug/L EPA 6010DJ 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-SW3 CA05959-12
Flag NotesMDLNC SWSLMRLDF
10.1 ug/L EPA 6010D 1010.06.801Arsenic - Total
237 ug/L EPA 6010D 10010.01.001Barium - Total
2.09 ug/L EPA 6010D 11.000.1301Beryllium - Total
0.528 ug/L EPA 6010DJ 11.000.3601Cadmium - Total
8.18 ug/L EPA 6010DJ 1010.01.401Chromium - Total
11.2 ug/L EPA 6010D 1010.01.101Cobalt - Total
9.62 ug/L EPA 6010DJ 1010.01.601Copper - Total
27.6 ug/L EPA 6010D 1010.03.101Lead - Total
19.6 ug/L EPA 6010DJ 5010.02.201Nickel - Total
3.4 ug/L EPA 8260B 11.00.141Toluene
34.5 ug/L EPA 6010D 2510.01.401Vanadium - Total
113 ug/L EPA 6010D 1010.04.401Zinc - Total
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Analyte MethodUnitsResults
Lab ID:Client ID:9801-SW4 CA05959-13
Flag NotesMDLNC SWSLMRLDF
78.5 ug/L EPA 6010DJ 10010.01.001Barium - Total
1.2 ug/L EPA 8260BJ 51.00.151cis-1,2-Dichloroethene
2.39 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
1.85 ug/L EPA 6010DJ 1010.01.601Copper - Total
1.41 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
14.0 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:9801-SW5 CA05959-14
Flag NotesMDLNC SWSLMRLDF
1.1 ug/L EPA 8260BJ 1005.01.114-Methyl-2-pentanone
7.68 ug/L EPA 6010DJ 1010.06.801Arsenic - Total
229 ug/L EPA 6010D 10010.01.001Barium - Total
0.287 ug/L EPA 6010DJ 11.000.1301Beryllium - Total
2.46 ug/L EPA 6010DJ 1010.01.401Chromium - Total
4.88 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
3.42 ug/L EPA 6010DJ 5010.02.201Nickel - Total
1.94 ug/L EPA 6010DJ 1010.01.901Silver - Total
12 ug/L EPA 8260B 11.00.141Toluene
3.08 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
13.8 ug/L EPA 6010D 1010.04.401Zinc - Total
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ANALYTICAL RESULTS
9801-MW1ADescription:Lab Sample ID:CA05959-01 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 11:57 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/19/17 19:581,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/19/17 19:581,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/19/17 19:581,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/19/17 19:581,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/19/17 19:581,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/19/17 19:581,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/19/17 19:581,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/19/17 19:581,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/19/17 19:581,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/19/17 19:581,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/19/17 19:581,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/19/17 19:581,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/19/17 19:581,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/19/17 19:582-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/19/17 19:582-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/19/17 19:584-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/19/17 19:58Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/19/17 19:58Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/19/17 19:58Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/19/17 19:58Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/19/17 19:58Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/19/17 19:58Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/19/17 19:58Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/19/17 19:58Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/19/17 19:58Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/19/17 19:58Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/19/17 19:58Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/19/17 19:58Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/19/17 19:58Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/19/17 19:58cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/19/17 19:58cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/19/17 19:58Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/19/17 19:58Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/19/17 19:58Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/19/17 19:58Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/19/17 19:58m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/19/17 19:58Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/19/17 19:58o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/19/17 19:58Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/19/17 19:58Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/19/17 19:58Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/19/17 19:58trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/19/17 19:58trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/19/17 19:58trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/19/17 19:58Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/19/17 19:58Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/19/17 19:58Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/19/17 19:58Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
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9801-MW1ADescription:Lab Sample ID:CA05959-01 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 11:57 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/19/17 19:58Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136102 %MRKEPA 8260B 05/19/17 19:587E190285150.0 1
Dibromofluoromethane 67-129109 %MRKEPA 8260B 05/19/17 19:587E190285450.0 1
Toluene-d8 59-134103 %MRKEPA 8260B 05/19/17 19:587E190285150.0 1
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9801-MW1ADescription:Lab Sample ID:CA05959-01 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 11:57 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/23/17 16:04Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/19/17 10:24Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/19/17 10:24Barium [7440-39-3] ^1.00 JMV10.0208 1001
ug/L EPA 6010D 05/19/17 10:24Beryllium [7440-41-7] ^0.130 JMV1.000.659 J 11
ug/L EPA 6010D 05/19/17 10:24Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/19/17 10:24Chromium [7440-47-3] ^1.40 JMV10.01.41 J 101
ug/L EPA 6010D 05/19/17 10:24Cobalt [7440-48-4] ^1.10 JMV10.07.26 J 101
ug/L EPA 6010D 05/19/17 10:24Copper [7440-50-8] ^1.60 JMV10.01.82 J 101
ug/L EPA 6010D 05/19/17 10:24Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/19/17 10:24Nickel [7440-02-0] ^2.20 JMV10.010.1 J 501
ug/L EPA 6020B 05/23/17 16:04Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/19/17 10:24Silver [7440-22-4] ^1.90 JMV10.02.19 J 101
ug/L EPA 6020B 05/23/17 16:04Thallium [7440-28-0] ^0.110 JDH1.000.110 U 5.51
ug/L EPA 6010D 05/19/17 10:24Vanadium [7440-62-2] ^1.40 JMV10.01.67 J 251
ug/L EPA 6010D 05/19/17 10:24Zinc [7440-66-6] ^4.40 JMV10.016.2 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-MW2Description:Lab Sample ID:CA05959-02 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 14:18 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/18/17 10:041,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/18/17 10:041,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/18/17 10:041,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/18/17 10:041,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/18/17 10:041,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/18/17 10:041,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/18/17 10:041,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/18/17 10:041,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/18/17 10:041,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/18/17 10:041,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/18/17 10:041,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/18/17 10:041,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/18/17 10:041,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/18/17 10:042-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/18/17 10:042-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/18/17 10:044-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/18/17 10:04Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/18/17 10:04Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/18/17 10:04Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 10:04Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/18/17 10:04Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 10:04Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/18/17 10:04Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/18/17 10:04Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/18/17 10:04Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 10:04Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/18/17 10:04Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/18/17 10:04Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/18/17 10:04Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/18/17 10:04cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/18/17 10:04cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/18/17 10:04Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/18/17 10:04Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/18/17 10:04Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/18/17 10:04Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/18/17 10:04m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/18/17 10:04Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/18/17 10:04o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/18/17 10:04Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/18/17 10:04Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 10:04Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/18/17 10:04trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/18/17 10:04trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 10:04trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/18/17 10:04Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 10:04Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/18/17 10:04Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/18/17 10:04Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/18/17 10:04Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-MW2Description:Lab Sample ID:CA05959-02 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 14:18 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13699 %MRKEPA 8260B 05/18/17 10:047E170254950.0 1
Dibromofluoromethane 67-129109 %MRKEPA 8260B 05/18/17 10:047E170255450.0 1
Toluene-d8 59-134112 %MRKEPA 8260B 05/18/17 10:047E170255650.0 1
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9801-MW2Description:Lab Sample ID:CA05959-02 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 14:18 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/23/17 16:07Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/19/17 10:36Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/19/17 10:36Barium [7440-39-3] ^1.00 JMV10.066.0 J 1001
ug/L EPA 6010D 05/19/17 10:36Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/19/17 10:36Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/19/17 10:36Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 05/19/17 10:36Cobalt [7440-48-4] ^1.10 JMV10.01.10 U 101
ug/L EPA 6010D 05/19/17 10:36Copper [7440-50-8] ^1.60 JMV10.01.60 U 101
ug/L EPA 6010D 05/19/17 10:36Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/19/17 10:36Nickel [7440-02-0] ^2.20 JMV10.02.20 U 501
ug/L EPA 6020B 05/23/17 16:07Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/19/17 10:36Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/23/17 16:07Thallium [7440-28-0] ^0.110 JDH1.000.110 U 5.51
ug/L EPA 6010D 05/19/17 10:36Vanadium [7440-62-2] ^1.40 JMV10.01.40 U 251
ug/L EPA 6010D 05/19/17 10:36Zinc [7440-66-6] ^4.40 JMV10.04.40 U 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-MW3Description:Lab Sample ID:CA05959-03 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 13:47 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/18/17 10:341,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/18/17 10:341,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/18/17 10:341,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/18/17 10:341,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/18/17 10:341,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/18/17 10:341,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/18/17 10:341,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/18/17 10:341,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/18/17 10:341,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/18/17 10:341,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/18/17 10:341,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/18/17 10:341,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/18/17 10:341,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/18/17 10:342-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/18/17 10:342-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/18/17 10:344-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/18/17 10:34Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/18/17 10:34Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/18/17 10:34Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 10:34Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/18/17 10:34Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 10:34Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/18/17 10:34Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/18/17 10:34Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/18/17 10:34Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 10:34Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/18/17 10:34Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/18/17 10:34Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/18/17 10:34Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/18/17 10:34cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/18/17 10:34cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/18/17 10:34Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/18/17 10:34Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/18/17 10:34Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/18/17 10:34Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/18/17 10:34m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/18/17 10:34Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/18/17 10:34o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/18/17 10:34Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/18/17 10:34Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 10:34Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/18/17 10:34trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/18/17 10:34trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 10:34trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/18/17 10:34Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 10:34Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/18/17 10:34Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/18/17 10:34Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/18/17 10:34Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-MW3Description:Lab Sample ID:CA05959-03 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 13:47 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136101 %MRKEPA 8260B 05/18/17 10:347E170255050.0 1
Dibromofluoromethane 67-129111 %MRKEPA 8260B 05/18/17 10:347E170255650.0 1
Toluene-d8 59-134107 %MRKEPA 8260B 05/18/17 10:347E170255350.0 1
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9801-MW3Description:Lab Sample ID:CA05959-03 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 13:47 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/23/17 16:11Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/19/17 10:39Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/19/17 10:39Barium [7440-39-3] ^1.00 JMV10.0103 1001
ug/L EPA 6010D 05/19/17 10:39Beryllium [7440-41-7] ^0.130 JMV1.001.45 11
ug/L EPA 6010D 05/19/17 10:39Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/19/17 10:39Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 05/19/17 10:39Cobalt [7440-48-4] ^1.10 JMV10.03.48 J 101
ug/L EPA 6010D 05/19/17 10:39Copper [7440-50-8] ^1.60 JMV10.01.60 U 101
ug/L EPA 6010D 05/19/17 10:39Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/19/17 10:39Nickel [7440-02-0] ^2.20 JMV10.07.37 J 501
ug/L EPA 6020B 05/23/17 16:11Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/19/17 10:39Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/23/17 16:11Thallium [7440-28-0] ^0.110 JDH1.000.110 U 5.51
ug/L EPA 6010D 05/19/17 10:39Vanadium [7440-62-2] ^1.40 JMV10.01.40 U 251
ug/L EPA 6010D 05/19/17 10:39Zinc [7440-66-6] ^4.40 JMV10.018.7 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-MW3ADescription:Lab Sample ID:CA05959-04 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 13:53 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/18/17 11:031,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/18/17 11:031,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/18/17 11:031,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/18/17 11:031,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/18/17 11:031,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/18/17 11:031,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/18/17 11:031,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/18/17 11:031,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/18/17 11:031,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/18/17 11:031,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/18/17 11:031,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/18/17 11:031,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/18/17 11:031,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/18/17 11:032-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/18/17 11:032-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/18/17 11:034-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/18/17 11:03Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/18/17 11:03Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/18/17 11:03Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 11:03Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/18/17 11:03Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 11:03Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/18/17 11:03Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/18/17 11:03Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/18/17 11:03Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 11:03Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/18/17 11:03Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/18/17 11:03Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/18/17 11:03Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/18/17 11:03cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/18/17 11:03cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/18/17 11:03Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/18/17 11:03Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/18/17 11:03Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/18/17 11:03Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/18/17 11:03m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/18/17 11:03Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/18/17 11:03o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/18/17 11:03Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/18/17 11:03Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 11:03Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/18/17 11:03trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/18/17 11:03trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 11:03trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/18/17 11:03Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 11:03Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/18/17 11:03Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/18/17 11:03Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/18/17 11:03Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-MW3ADescription:Lab Sample ID:CA05959-04 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 13:53 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136100 %MRKEPA 8260B 05/18/17 11:037E170255050.0 1
Dibromofluoromethane 67-129110 %MRKEPA 8260B 05/18/17 11:037E170255550.0 1
Toluene-d8 59-134111 %MRKEPA 8260B 05/18/17 11:037E170255550.0 1
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9801-MW3ADescription:Lab Sample ID:CA05959-04 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 13:53 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/23/17 16:15Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/19/17 10:49Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/19/17 10:49Barium [7440-39-3] ^1.00 JMV10.0298 1001
ug/L EPA 6010D 05/19/17 10:49Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/19/17 10:49Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/19/17 10:49Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 05/19/17 10:49Cobalt [7440-48-4] ^1.10 JMV10.01.10 U 101
ug/L EPA 6010D 05/19/17 10:49Copper [7440-50-8] ^1.60 JMV10.01.60 U 101
ug/L EPA 6010D 05/19/17 10:49Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/19/17 10:49Nickel [7440-02-0] ^2.20 JMV10.02.20 U 501
ug/L EPA 6020B 05/23/17 16:15Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/19/17 10:49Silver [7440-22-4] ^1.90 JMV10.02.17 J 101
ug/L EPA 6020B 05/23/17 16:15Thallium [7440-28-0] ^0.110 JDH1.000.110 U 5.51
ug/L EPA 6010D 05/19/17 10:49Vanadium [7440-62-2] ^1.40 JMV10.01.40 U 251
ug/L EPA 6010D 05/19/17 10:49Zinc [7440-66-6] ^4.40 JMV10.04.40 U 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-MW4Description:Lab Sample ID:CA05959-05 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 12:29 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/18/17 11:331,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/18/17 11:331,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/18/17 11:331,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/18/17 11:331,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/18/17 11:331,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/18/17 11:331,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/18/17 11:331,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/18/17 11:331,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/18/17 11:331,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/18/17 11:331,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/18/17 11:331,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/18/17 11:331,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/18/17 11:331,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/18/17 11:332-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/18/17 11:332-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/18/17 11:334-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/18/17 11:33Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/18/17 11:33Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/18/17 11:33Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 11:33Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/18/17 11:33Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 11:33Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/18/17 11:33Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/18/17 11:33Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/18/17 11:33Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 11:33Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/18/17 11:33Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/18/17 11:33Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/18/17 11:33Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/18/17 11:33cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/18/17 11:33cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/18/17 11:33Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/18/17 11:33Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/18/17 11:33Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/18/17 11:33Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/18/17 11:33m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/18/17 11:33Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/18/17 11:33o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/18/17 11:33Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/18/17 11:33Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 11:33Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/18/17 11:33trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/18/17 11:33trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 11:33trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/18/17 11:33Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 11:33Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/18/17 11:33Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/18/17 11:33Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/18/17 11:33Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-MW4Description:Lab Sample ID:CA05959-05 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 12:29 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136100 %MRKEPA 8260B 05/18/17 11:337E170255050.0 1
Dibromofluoromethane 67-129112 %MRKEPA 8260B 05/18/17 11:337E170255650.0 1
Toluene-d8 59-134110 %MRKEPA 8260B 05/18/17 11:337E170255550.0 1
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9801-MW4Description:Lab Sample ID:CA05959-05 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 12:29 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/23/17 16:18Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/19/17 10:51Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/19/17 10:51Barium [7440-39-3] ^1.00 JMV10.0581 1001
ug/L EPA 6010D 05/19/17 10:51Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/19/17 10:51Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/19/17 10:51Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 05/19/17 10:51Cobalt [7440-48-4] ^1.10 JMV10.01.10 U 101
ug/L EPA 6010D 05/19/17 10:51Copper [7440-50-8] ^1.60 JMV10.01.60 U 101
ug/L EPA 6010D 05/19/17 10:51Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/19/17 10:51Nickel [7440-02-0] ^2.20 JMV10.02.20 U 501
ug/L EPA 6020B 05/23/17 16:18Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/19/17 10:51Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/23/17 16:18Thallium [7440-28-0] ^0.110 JDH1.000.110 U 5.51
ug/L EPA 6010D 05/19/17 10:51Vanadium [7440-62-2] ^1.40 JMV10.01.40 U 251
ug/L EPA 6010D 05/19/17 10:51Zinc [7440-66-6] ^4.40 JMV10.04.40 U 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-MW5Description:Lab Sample ID:CA05959-06 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 13:04 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/18/17 12:031,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/18/17 12:031,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/18/17 12:031,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/18/17 12:031,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/18/17 12:031,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/18/17 12:031,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/18/17 12:031,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/18/17 12:031,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/18/17 12:031,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/18/17 12:031,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/18/17 12:031,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/18/17 12:031,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/18/17 12:031,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/18/17 12:032-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/18/17 12:032-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/18/17 12:034-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/18/17 12:03Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/18/17 12:03Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/18/17 12:03Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 12:03Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/18/17 12:03Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 12:03Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/18/17 12:03Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/18/17 12:03Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/18/17 12:03Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 12:03Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/18/17 12:03Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/18/17 12:03Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/18/17 12:03Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/18/17 12:03cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/18/17 12:03cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/18/17 12:03Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/18/17 12:03Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/18/17 12:03Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/18/17 12:03Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/18/17 12:03m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/18/17 12:03Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/18/17 12:03o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/18/17 12:03Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/18/17 12:03Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 12:03Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/18/17 12:03trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/18/17 12:03trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 12:03trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/18/17 12:03Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 12:03Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/18/17 12:03Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/18/17 12:03Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/18/17 12:03Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-MW5Description:Lab Sample ID:CA05959-06 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 13:04 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13699 %MRKEPA 8260B 05/18/17 12:037E170255050.0 1
Dibromofluoromethane 67-129111 %MRKEPA 8260B 05/18/17 12:037E170255650.0 1
Toluene-d8 59-134108 %MRKEPA 8260B 05/18/17 12:037E170255450.0 1
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9801-MW5Description:Lab Sample ID:CA05959-06 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 13:04 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/23/17 16:22Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/19/17 10:54Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/19/17 10:54Barium [7440-39-3] ^1.00 JMV10.0644 1001
ug/L EPA 6010D 05/19/17 10:54Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/19/17 10:54Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/19/17 10:54Chromium [7440-47-3] ^1.40 JMV10.03.43 J 101
ug/L EPA 6010D 05/19/17 10:54Cobalt [7440-48-4] ^1.10 JMV10.02.37 J 101
ug/L EPA 6010D 05/19/17 10:54Copper [7440-50-8] ^1.60 JMV10.01.60 U 101
ug/L EPA 6010D 05/19/17 10:54Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/19/17 10:54Nickel [7440-02-0] ^2.20 JMV10.04.95 J 501
ug/L EPA 6020B 05/23/17 16:22Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/19/17 10:54Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/23/17 16:22Thallium [7440-28-0] ^0.110 JDH1.000.110 U 5.51
ug/L EPA 6010D 05/19/17 10:54Vanadium [7440-62-2] ^1.40 JMV10.03.80 J 251
ug/L EPA 6010D 05/19/17 10:54Zinc [7440-66-6] ^4.40 JMV10.012.3 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-MW6Description:Lab Sample ID:CA05959-07 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 13:53 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/18/17 12:341,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/18/17 12:341,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/18/17 12:341,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/18/17 12:341,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/18/17 12:341,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/18/17 12:341,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/18/17 12:341,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/18/17 12:341,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/18/17 12:341,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/18/17 12:341,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/18/17 12:341,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/18/17 12:341,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/18/17 12:341,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/18/17 12:342-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/18/17 12:342-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/18/17 12:344-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/18/17 12:34Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/18/17 12:34Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/18/17 12:34Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 12:34Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/18/17 12:34Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 12:34Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/18/17 12:34Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/18/17 12:34Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/18/17 12:34Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 12:34Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/18/17 12:34Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/18/17 12:34Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/18/17 12:34Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/18/17 12:34cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/18/17 12:34cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/18/17 12:34Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/18/17 12:34Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/18/17 12:34Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/18/17 12:34Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/18/17 12:34m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/18/17 12:34Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/18/17 12:34o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/18/17 12:34Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/18/17 12:34Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 12:34Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/18/17 12:34trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/18/17 12:34trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 12:34trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/18/17 12:34Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 12:34Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/18/17 12:34Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/18/17 12:34Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/18/17 12:34Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-MW6Description:Lab Sample ID:CA05959-07 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 13:53 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13697 %MRKEPA 8260B 05/18/17 12:347E170254850.0 1
Dibromofluoromethane 67-129103 %MRKEPA 8260B 05/18/17 12:347E170255250.0 1
Toluene-d8 59-134111 %MRKEPA 8260B 05/18/17 12:347E170255550.0 1
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9801-MW6Description:Lab Sample ID:CA05959-07 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 13:53 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/23/17 16:25Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/19/17 10:56Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/19/17 10:56Barium [7440-39-3] ^1.00 JMV10.046.6 J 1001
ug/L EPA 6010D 05/19/17 10:56Beryllium [7440-41-7] ^0.130 JMV1.002.63 11
ug/L EPA 6010D 05/19/17 10:56Cadmium [7440-43-9] ^0.360 JMV1.000.773 J 11
ug/L EPA 6010D 05/19/17 10:56Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 05/19/17 10:56Cobalt [7440-48-4] ^1.10 JMV10.025.2 101
ug/L EPA 6010D 05/19/17 10:56Copper [7440-50-8] ^1.60 JMV10.01.60 U 101
ug/L EPA 6010D 05/19/17 10:56Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/19/17 10:56Nickel [7440-02-0] ^2.20 JMV10.040.3 J 501
ug/L EPA 6020B 05/23/17 16:25Selenium [7782-49-2] ^0.910 JDH3.001.04 J 101
ug/L EPA 6010D 05/19/17 10:56Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/23/17 16:25Thallium [7440-28-0] ^0.110 JDH1.000.110 U 5.51
ug/L EPA 6010D 05/19/17 10:56Vanadium [7440-62-2] ^1.40 JMV10.08.35 J 251
ug/L EPA 6010D 05/19/17 10:56Zinc [7440-66-6] ^4.40 JMV10.052.6 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-MW7Description:Lab Sample ID:CA05959-08 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 13:30 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/18/17 13:041,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/18/17 13:041,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/18/17 13:041,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/18/17 13:041,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/18/17 13:041,1-Dichloroethane [75-34-3] ^0.13 MRK1.01.6 J 51
ug/L EPA 8260B 05/18/17 13:041,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/18/17 13:041,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/18/17 13:041,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/18/17 13:041,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/18/17 13:041,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/18/17 13:041,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/18/17 13:041,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/18/17 13:041,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/18/17 13:042-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/18/17 13:042-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/18/17 13:044-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/18/17 13:04Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/18/17 13:04Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/18/17 13:04Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 13:04Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/18/17 13:04Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 13:04Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/18/17 13:04Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/18/17 13:04Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/18/17 13:04Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 13:04Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/18/17 13:04Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/18/17 13:04Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/18/17 13:04Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/18/17 13:04cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.017 51
ug/L EPA 8260B 05/18/17 13:04cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/18/17 13:04Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/18/17 13:04Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/18/17 13:04Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/18/17 13:04Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/18/17 13:04m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/18/17 13:04Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/18/17 13:04o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/18/17 13:04Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/18/17 13:04Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 13:04Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/18/17 13:04trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/18/17 13:04trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 13:04trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/18/17 13:04Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 13:04Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/18/17 13:04Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/18/17 13:04Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/18/17 13:04Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-MW7Description:Lab Sample ID:CA05959-08 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 13:30 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13698 %MRKEPA 8260B 05/18/17 13:047E170254950.0 1
Dibromofluoromethane 67-129111 %MRKEPA 8260B 05/18/17 13:047E170255550.0 1
Toluene-d8 59-134112 %MRKEPA 8260B 05/18/17 13:047E170255650.0 1
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9801-MW7Description:Lab Sample ID:CA05959-08 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 13:30 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/23/17 16:29Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/19/17 10:59Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/19/17 10:59Barium [7440-39-3] ^1.00 JMV10.0112 1001
ug/L EPA 6010D 05/19/17 10:59Beryllium [7440-41-7] ^0.130 JMV1.000.174 J 11
ug/L EPA 6010D 05/19/17 10:59Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/19/17 10:59Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 05/19/17 10:59Cobalt [7440-48-4] ^1.10 JMV10.01.10 U 101
ug/L EPA 6010D 05/19/17 10:59Copper [7440-50-8] ^1.60 JMV10.01.60 U 101
ug/L EPA 6010D 05/19/17 10:59Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/19/17 10:59Nickel [7440-02-0] ^2.20 JMV10.02.20 U 501
ug/L EPA 6020B 05/23/17 16:29Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/19/17 10:59Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/23/17 16:29Thallium [7440-28-0] ^0.110 JDH1.000.110 U 5.51
ug/L EPA 6010D 05/19/17 10:59Vanadium [7440-62-2] ^1.40 JMV10.02.93 J 251
ug/L EPA 6010D 05/19/17 10:59Zinc [7440-66-6] ^4.40 JMV10.09.41 J 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-MW8Description:Lab Sample ID:CA05959-09 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 12:06 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/18/17 13:351,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/18/17 13:351,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/18/17 13:351,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/18/17 13:351,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/18/17 13:351,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/18/17 13:351,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/18/17 13:351,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/18/17 13:351,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/18/17 13:351,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/18/17 13:351,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/18/17 13:351,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/18/17 13:351,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/18/17 13:351,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/18/17 13:352-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/18/17 13:352-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/18/17 13:354-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/18/17 13:35Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/18/17 13:35Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/18/17 13:35Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 13:35Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/18/17 13:35Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 13:35Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/18/17 13:35Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/18/17 13:35Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/18/17 13:35Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 13:35Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/18/17 13:35Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/18/17 13:35Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/18/17 13:35Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/18/17 13:35cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/18/17 13:35cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/18/17 13:35Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/18/17 13:35Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/18/17 13:35Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/18/17 13:35Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/18/17 13:35m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/18/17 13:35Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/18/17 13:35o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/18/17 13:35Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/18/17 13:35Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 13:35Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/18/17 13:35trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/18/17 13:35trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 13:35trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/18/17 13:35Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 13:35Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/18/17 13:35Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/18/17 13:35Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/18/17 13:35Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-MW8Description:Lab Sample ID:CA05959-09 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 12:06 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136100 %MRKEPA 8260B 05/18/17 13:357E170255050.0 1
Dibromofluoromethane 67-129112 %MRKEPA 8260B 05/18/17 13:357E170255650.0 1
Toluene-d8 59-134111 %MRKEPA 8260B 05/18/17 13:357E170255650.0 1
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www.encolabs.com
9801-MW8Description:Lab Sample ID:CA05959-09 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 12:06 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/23/17 16:33Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/19/17 11:02Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/19/17 11:02Barium [7440-39-3] ^1.00 JMV10.061.2 J 1001
ug/L EPA 6010D 05/19/17 11:02Beryllium [7440-41-7] ^0.130 JMV1.000.324 J 11
ug/L EPA 6010D 05/19/17 11:02Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/19/17 11:02Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 05/19/17 11:02Cobalt [7440-48-4] ^1.10 JMV10.04.88 J 101
ug/L EPA 6010D 05/19/17 11:02Copper [7440-50-8] ^1.60 JMV10.01.60 U 101
ug/L EPA 6010D 05/19/17 11:02Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/19/17 11:02Nickel [7440-02-0] ^2.20 JMV10.02.44 J 501
ug/L EPA 6020B 05/23/17 16:33Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/19/17 11:02Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/23/17 16:33Thallium [7440-28-0] ^0.110 JDH1.000.110 U 5.51
ug/L EPA 6010D 05/19/17 11:02Vanadium [7440-62-2] ^1.40 JMV10.01.40 U 251
ug/L EPA 6010D 05/19/17 11:02Zinc [7440-66-6] ^4.40 JMV10.011.8 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-SW1Description:Lab Sample ID:CA05959-10 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 12:54 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/18/17 14:061,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/18/17 14:061,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/18/17 14:061,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/18/17 14:061,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/18/17 14:061,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/18/17 14:061,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/18/17 14:061,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/18/17 14:061,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/18/17 14:061,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/18/17 14:061,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/18/17 14:061,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/18/17 14:061,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/18/17 14:061,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/18/17 14:062-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/18/17 14:062-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/18/17 14:064-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/18/17 14:06Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/18/17 14:06Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/18/17 14:06Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 14:06Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/18/17 14:06Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 14:06Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/18/17 14:06Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/18/17 14:06Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/18/17 14:06Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 14:06Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/18/17 14:06Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/18/17 14:06Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/18/17 14:06Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/18/17 14:06cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/18/17 14:06cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/18/17 14:06Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/18/17 14:06Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/18/17 14:06Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/18/17 14:06Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/18/17 14:06m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/18/17 14:06Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/18/17 14:06o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/18/17 14:06Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/18/17 14:06Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 14:06Toluene [108-88-3] ^0.14 MRK1.00.50 J 11
ug/L EPA 8260B 05/18/17 14:06trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/18/17 14:06trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 14:06trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/18/17 14:06Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 14:06Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/18/17 14:06Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/18/17 14:06Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/18/17 14:06Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-SW1Description:Lab Sample ID:CA05959-10 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 12:54 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13699 %MRKEPA 8260B 05/18/17 14:067E170254950.0 1
Dibromofluoromethane 67-129113 %MRKEPA 8260B 05/18/17 14:067E170255750.0 1
Toluene-d8 59-134110 %MRKEPA 8260B 05/18/17 14:067E170255550.0 1
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9801-SW1Description:Lab Sample ID:CA05959-10 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 12:54 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/23/17 16:36Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/19/17 11:04Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/19/17 11:04Barium [7440-39-3] ^1.00 JMV10.0153 1001
ug/L EPA 6010D 05/19/17 11:04Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/19/17 11:04Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/19/17 11:04Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 05/19/17 11:04Cobalt [7440-48-4] ^1.10 JMV10.01.96 J 101
ug/L EPA 6010D 05/19/17 11:04Copper [7440-50-8] ^1.60 JMV10.01.60 U 101
ug/L EPA 6010D 05/19/17 11:04Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/19/17 11:04Nickel [7440-02-0] ^2.20 JMV10.02.20 U 501
ug/L EPA 6020B 05/23/17 16:36Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/19/17 11:04Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/23/17 16:36Thallium [7440-28-0] ^0.110 JDH1.000.110 U 5.51
ug/L EPA 6010D 05/19/17 11:04Vanadium [7440-62-2] ^1.40 JMV10.01.54 J 251
ug/L EPA 6010D 05/19/17 11:04Zinc [7440-66-6] ^4.40 JMV10.015.4 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-SW2Description:Lab Sample ID:CA05959-11 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 12:45 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/18/17 14:361,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/18/17 14:361,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/18/17 14:361,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/18/17 14:361,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/18/17 14:361,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/18/17 14:361,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/18/17 14:361,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/18/17 14:361,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/18/17 14:361,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/18/17 14:361,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/18/17 14:361,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/18/17 14:361,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/18/17 14:361,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/18/17 14:362-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/18/17 14:362-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/18/17 14:364-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/18/17 14:36Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/18/17 14:36Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/18/17 14:36Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 14:36Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/18/17 14:36Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 14:36Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/18/17 14:36Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/18/17 14:36Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/18/17 14:36Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 14:36Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/18/17 14:36Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/18/17 14:36Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/18/17 14:36Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/18/17 14:36cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.01.2 J 51
ug/L EPA 8260B 05/18/17 14:36cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/18/17 14:36Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/18/17 14:36Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/18/17 14:36Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/18/17 14:36Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/18/17 14:36m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/18/17 14:36Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/18/17 14:36o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/18/17 14:36Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/18/17 14:36Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 14:36Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/18/17 14:36trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/18/17 14:36trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 14:36trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/18/17 14:36Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 14:36Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/18/17 14:36Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/18/17 14:36Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/18/17 14:36Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-SW2Description:Lab Sample ID:CA05959-11 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 12:45 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13698 %MRKEPA 8260B 05/18/17 14:367E170254950.0 1
Dibromofluoromethane 67-129104 %MRKEPA 8260B 05/18/17 14:367E170255250.0 1
Toluene-d8 59-134110 %MRKEPA 8260B 05/18/17 14:367E170255550.0 1
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9801-SW2Description:Lab Sample ID:CA05959-11 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 12:45 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/23/17 16:48Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/19/17 11:07Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/19/17 11:07Barium [7440-39-3] ^1.00 JMV10.069.8 J 1001
ug/L EPA 6010D 05/19/17 11:07Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/19/17 11:07Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/19/17 11:07Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 05/19/17 11:07Cobalt [7440-48-4] ^1.10 JMV10.01.95 J 101
ug/L EPA 6010D 05/19/17 11:07Copper [7440-50-8] ^1.60 JMV10.01.60 U 101
ug/L EPA 6010D 05/19/17 11:07Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/19/17 11:07Nickel [7440-02-0] ^2.20 JMV10.02.20 U 501
ug/L EPA 6020B 05/23/17 16:48Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/19/17 11:07Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/23/17 16:48Thallium [7440-28-0] ^0.110 JDH1.000.110 U 5.51
ug/L EPA 6010D 05/19/17 11:07Vanadium [7440-62-2] ^1.40 JMV10.01.40 U 251
ug/L EPA 6010D 05/19/17 11:07Zinc [7440-66-6] ^4.40 JMV10.09.97 J 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-SW3Description:Lab Sample ID:CA05959-12 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 13:57 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/18/17 20:061,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/18/17 20:061,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/18/17 20:061,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/18/17 20:061,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/18/17 20:061,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/18/17 20:061,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/18/17 20:061,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/18/17 20:061,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/18/17 20:061,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/18/17 20:061,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/18/17 20:061,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/18/17 20:061,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/18/17 20:061,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/18/17 20:062-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/18/17 20:062-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/18/17 20:064-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/18/17 20:06Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/18/17 20:06Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/18/17 20:06Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 20:06Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/18/17 20:06Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 20:06Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/18/17 20:06Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/18/17 20:06Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/18/17 20:06Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 20:06Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/18/17 20:06Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/18/17 20:06Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/18/17 20:06Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/18/17 20:06cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/18/17 20:06cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/18/17 20:06Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/18/17 20:06Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/18/17 20:06Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/18/17 20:06Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/18/17 20:06m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/18/17 20:06Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/18/17 20:06o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/18/17 20:06Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/18/17 20:06Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 20:06Toluene [108-88-3] ^0.14 MRK1.03.4 11
ug/L EPA 8260B 05/18/17 20:06trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/18/17 20:06trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 20:06trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/18/17 20:06Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 20:06Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/18/17 20:06Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/18/17 20:06Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/18/17 20:06Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-SW3Description:Lab Sample ID:CA05959-12 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 13:57 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13687 %MRKEPA 8260B 05/18/17 20:067E170144450.0 1
Dibromofluoromethane 67-129101 %MRKEPA 8260B 05/18/17 20:067E170145150.0 1
Toluene-d8 59-13495 %MRKEPA 8260B 05/18/17 20:067E170144850.0 1
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9801-SW3Description:Lab Sample ID:CA05959-12 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 13:57 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/23/17 16:51Antimony [7440-36-0] ^3.70 JDH20.03.70 UD R-01610
ug/L EPA 6010D 05/19/17 11:09Arsenic [7440-38-2] ^6.80 JMV10.010.1 101
ug/L EPA 6010D 05/19/17 11:09Barium [7440-39-3] ^1.00 JMV10.0237 1001
ug/L EPA 6010D 05/19/17 11:09Beryllium [7440-41-7] ^0.130 JMV1.002.09 11
ug/L EPA 6010D 05/19/17 11:09Cadmium [7440-43-9] ^0.360 JMV1.000.528 J 11
ug/L EPA 6010D 05/19/17 11:09Chromium [7440-47-3] ^1.40 JMV10.08.18 J 101
ug/L EPA 6010D 05/19/17 11:09Cobalt [7440-48-4] ^1.10 JMV10.011.2 101
ug/L EPA 6010D 05/19/17 11:09Copper [7440-50-8] ^1.60 JMV10.09.62 J 101
ug/L EPA 6010D 05/19/17 11:09Lead [7439-92-1] ^3.10 JMV10.027.6 101
ug/L EPA 6010D 05/19/17 11:09Nickel [7440-02-0] ^2.20 JMV10.019.6 J 501
ug/L EPA 6020B 05/23/17 16:51Selenium [7782-49-2] ^9.10 JDH30.09.10 UD R-011010
ug/L EPA 6010D 05/19/17 11:09Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/23/17 16:51Thallium [7440-28-0] ^1.10 JDH10.01.10 UD R-015.510
ug/L EPA 6010D 05/19/17 11:09Vanadium [7440-62-2] ^1.40 JMV10.034.5 251
ug/L EPA 6010D 05/19/17 11:09Zinc [7440-66-6] ^4.40 JMV10.0113 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-SW4Description:Lab Sample ID:CA05959-13 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 12:36 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/18/17 20:361,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/18/17 20:361,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/18/17 20:361,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/18/17 20:361,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/18/17 20:361,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/18/17 20:361,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/18/17 20:361,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/18/17 20:361,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/18/17 20:361,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/18/17 20:361,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/18/17 20:361,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/18/17 20:361,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/18/17 20:361,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/18/17 20:362-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/18/17 20:362-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/18/17 20:364-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/18/17 20:36Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/18/17 20:36Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/18/17 20:36Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 20:36Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/18/17 20:36Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 20:36Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/18/17 20:36Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/18/17 20:36Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/18/17 20:36Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 20:36Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/18/17 20:36Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/18/17 20:36Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/18/17 20:36Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/18/17 20:36cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.01.2 J 51
ug/L EPA 8260B 05/18/17 20:36cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/18/17 20:36Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/18/17 20:36Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/18/17 20:36Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/18/17 20:36Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/18/17 20:36m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/18/17 20:36Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/18/17 20:36o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/18/17 20:36Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/18/17 20:36Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 20:36Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/18/17 20:36trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/18/17 20:36trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 20:36trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/18/17 20:36Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 20:36Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/18/17 20:36Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/18/17 20:36Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/18/17 20:36Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-SW4Description:Lab Sample ID:CA05959-13 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 12:36 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13688 %MRKEPA 8260B 05/18/17 20:367E170144450.0 1
Dibromofluoromethane 67-129100 %MRKEPA 8260B 05/18/17 20:367E170145050.0 1
Toluene-d8 59-13495 %MRKEPA 8260B 05/18/17 20:367E170144850.0 1
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9801-SW4Description:Lab Sample ID:CA05959-13 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 12:36 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/23/17 16:55Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/19/17 11:12Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/19/17 11:12Barium [7440-39-3] ^1.00 JMV10.078.5 J 1001
ug/L EPA 6010D 05/19/17 11:12Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/19/17 11:12Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/19/17 11:12Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 05/19/17 11:12Cobalt [7440-48-4] ^1.10 JMV10.02.39 J 101
ug/L EPA 6010D 05/19/17 11:12Copper [7440-50-8] ^1.60 JMV10.01.85 J 101
ug/L EPA 6010D 05/19/17 11:12Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/19/17 11:12Nickel [7440-02-0] ^2.20 JMV10.02.20 U 501
ug/L EPA 6020B 05/23/17 16:55Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/19/17 11:12Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/23/17 16:55Thallium [7440-28-0] ^0.110 JDH1.000.110 U 5.51
ug/L EPA 6010D 05/19/17 11:12Vanadium [7440-62-2] ^1.40 JMV10.01.41 J 251
ug/L EPA 6010D 05/19/17 11:12Zinc [7440-66-6] ^4.40 JMV10.014.0 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-SW5Description:Lab Sample ID:CA05959-14 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 13:10 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/18/17 21:071,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/18/17 21:071,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/18/17 21:071,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/18/17 21:071,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/18/17 21:071,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/18/17 21:071,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/18/17 21:071,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/18/17 21:071,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/18/17 21:071,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/18/17 21:071,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/18/17 21:071,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/18/17 21:071,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/18/17 21:071,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/18/17 21:072-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/18/17 21:072-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/18/17 21:074-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 J 1001
ug/L EPA 8260B 05/18/17 21:07Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/18/17 21:07Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/18/17 21:07Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 21:07Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/18/17 21:07Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 21:07Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/18/17 21:07Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/18/17 21:07Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/18/17 21:07Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 21:07Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/18/17 21:07Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/18/17 21:07Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/18/17 21:07Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/18/17 21:07cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/18/17 21:07cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/18/17 21:07Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/18/17 21:07Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/18/17 21:07Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/18/17 21:07Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/18/17 21:07m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/18/17 21:07Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/18/17 21:07o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/18/17 21:07Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/18/17 21:07Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 21:07Toluene [108-88-3] ^0.14 MRK1.012 11
ug/L EPA 8260B 05/18/17 21:07trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/18/17 21:07trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 21:07trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/18/17 21:07Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 21:07Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/18/17 21:07Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/18/17 21:07Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/18/17 21:07Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-SW5Description:Lab Sample ID:CA05959-14 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 13:10 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13688 %MRKEPA 8260B 05/18/17 21:077E170144450.0 1
Dibromofluoromethane 67-129102 %MRKEPA 8260B 05/18/17 21:077E170145150.0 1
Toluene-d8 59-13495 %MRKEPA 8260B 05/18/17 21:077E170144850.0 1
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9801-SW5Description:Lab Sample ID:CA05959-14 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 13:10 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/23/17 16:59Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/19/17 11:22Arsenic [7440-38-2] ^6.80 JMV10.07.68 J 101
ug/L EPA 6010D 05/19/17 11:22Barium [7440-39-3] ^1.00 JMV10.0229 1001
ug/L EPA 6010D 05/19/17 11:22Beryllium [7440-41-7] ^0.130 JMV1.000.287 J 11
ug/L EPA 6010D 05/19/17 11:22Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/19/17 11:22Chromium [7440-47-3] ^1.40 JMV10.02.46 J 101
ug/L EPA 6010D 05/19/17 11:22Cobalt [7440-48-4] ^1.10 JMV10.04.88 J 101
ug/L EPA 6010D 05/19/17 11:22Copper [7440-50-8] ^1.60 JMV10.01.60 U 101
ug/L EPA 6010D 05/19/17 11:22Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/19/17 11:22Nickel [7440-02-0] ^2.20 JMV10.03.42 J 501
ug/L EPA 6020B 05/23/17 16:59Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/19/17 11:22Silver [7440-22-4] ^1.90 JMV10.01.94 J 101
ug/L EPA 6020B 05/23/17 16:59Thallium [7440-28-0] ^0.110 JDH1.000.110 U 5.51
ug/L EPA 6010D 05/19/17 11:22Vanadium [7440-62-2] ^1.40 JMV10.03.08 J 251
ug/L EPA 6010D 05/19/17 11:22Zinc [7440-66-6] ^4.40 JMV10.013.8 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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9801-TripblankDescription:Lab Sample ID:CA05959-15 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 11:57 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/18/17 13:341,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/18/17 13:341,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/18/17 13:341,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/18/17 13:341,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/18/17 13:341,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/18/17 13:341,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/18/17 13:341,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/18/17 13:341,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/18/17 13:341,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/18/17 13:341,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/18/17 13:341,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/18/17 13:341,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/18/17 13:341,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/18/17 13:342-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/18/17 13:342-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/18/17 13:344-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/18/17 13:34Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/18/17 13:34Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/18/17 13:34Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 13:34Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/18/17 13:34Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 13:34Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/18/17 13:34Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/18/17 13:34Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/18/17 13:34Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 13:34Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/18/17 13:34Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/18/17 13:34Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/18/17 13:34Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/18/17 13:34cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/18/17 13:34cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/18/17 13:34Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/18/17 13:34Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/18/17 13:34Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/18/17 13:34Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/18/17 13:34m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/18/17 13:34Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/18/17 13:34o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/18/17 13:34Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/18/17 13:34Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/18/17 13:34Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/18/17 13:34trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/18/17 13:34trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 13:34trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/18/17 13:34Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/18/17 13:34Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/18/17 13:34Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/18/17 13:34Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/18/17 13:34Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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9801-TripblankDescription:Lab Sample ID:CA05959-15 05/11/17 10:10Received:
Matrix:Water Sampled:05/10/17 11:57 Work Order:CA05959
Wilson County MSWLFProject:Sampled By:ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13690 %MRKEPA 8260B 05/18/17 13:347E170144550.0 1
Dibromofluoromethane 67-12996 %MRKEPA 8260B 05/18/17 13:347E170144850.0 1
Toluene-d8 59-13492 %MRKEPA 8260B 05/18/17 13:347E170144650.0 1
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 7E17014 - EPA 5030B_MS
Prepared: 05/17/2017 11:43 Analyzed: 05/18/2017 13:03Blank (7E17014-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.17 U 1,1,1,2-Tetrachloroethane
ug/L1.00.12 U 1,1,1-Trichloroethane
ug/L1.00.28 U 1,1,2,2-Tetrachloroethane
ug/L1.00.14 U 1,1,2-Trichloroethane
ug/L1.00.13 U 1,1-Dichloroethane
ug/L1.00.21 U 1,1-Dichloroethene
ug/L1.00.23 U 1,2,3-Trichloropropane
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.66 U 1,2-Dibromoethane
ug/L1.00.19 U 1,2-Dichlorobenzene
ug/L1.00.21 U 1,2-Dichloroethane
ug/L1.00.10 U 1,2-Dichloropropane
ug/L1.00.19 U 1,4-Dichlorobenzene
ug/L5.01.3 U 2-Butanone
ug/L5.00.88 U 2-Hexanone
ug/L5.01.1 U 4-Methyl-2-pentanone
ug/L2010U Acetone
ug/L103.5 U Acrylonitrile
ug/L1.00.15 U Benzene
ug/L1.00.48 U Bromochloromethane
ug/L1.00.17 U Bromodichloromethane
ug/L1.00.22 U Bromoform
ug/L1.00.14 U Bromomethane
ug/L5.01.5 U Carbon disulfide
ug/L1.00.17 U Carbon tetrachloride
ug/L1.00.17 U Chlorobenzene
ug/L1.00.23 U Chloroethane
ug/L1.00.18 U Chloroform
ug/L1.00.13 U Chloromethane
ug/L1.00.15 U cis-1,2-Dichloroethene
ug/L1.00.20 U cis-1,3-Dichloropropene
ug/L1.00.17 U Dibromochloromethane
ug/L1.00.27 U Dibromomethane
ug/L1.00.13 U Ethylbenzene
ug/L5.01.7 U Iodomethane
ug/L2.00.17 U m,p-Xylenes
ug/L1.00.23 U Methylene chloride
ug/L1.00.065 U o-Xylene
ug/L1.00.11 U Styrene
ug/L1.00.17 U Tetrachloroethene
ug/L1.00.14 U Toluene
ug/L1.00.21 U trans-1,2-Dichloroethene
ug/L1.00.15 U trans-1,3-Dichloropropene
ug/L1.00.70 U trans-1,4-Dichloro-2-butene
ug/L1.00.15 U Trichloroethene
ug/L1.00.24 U Trichlorofluoromethane
ug/L5.00.95 U Vinyl acetate
ug/L1.00.32 U Vinyl chloride
ug/L3.00.45 U Xylenes (Total)
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 7E17014 - EPA 5030B_MS
Prepared: 05/17/2017 11:43 Analyzed: 05/18/2017 13:03Blank (7E17014-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 8945
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 9648
ug/L 50.0 59-134Surrogate: Toluene-d8 9447
Prepared: 05/17/2017 11:43 Analyzed: 05/18/2017 10:32LCS (7E17014-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-13310020 1,1-Dichloroethene
ug/L1.0 20.0 81-13411323 Benzene
ug/L1.0 20.0 83-1179619 Chlorobenzene
ug/L1.0 20.0 71-11810822 Toluene
ug/L1.0 20.0 74-11910120 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 8743
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 9447
ug/L 50.0 59-134Surrogate: Toluene-d8 9648
Prepared: 05/17/2017 11:43 Analyzed: 05/18/2017 11:33Matrix Spike (7E17014-MS1)
Source: CA07481-10
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-1331040.21 U21 1,1-Dichloroethene
ug/L1.0 20.0 81-1341130.15 U23 Benzene
ug/L1.0 20.0 83-117970.17 U19 Chlorobenzene
ug/L1.0 20.0 71-1181110.14 U22 Toluene
ug/L1.0 20.0 74-1191000.15 U20 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 8643
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 9246
ug/L 50.0 59-134Surrogate: Toluene-d8 9547
Prepared: 05/17/2017 11:43 Analyzed: 05/18/2017 12:03Matrix Spike Dup (7E17014-MSD1)
Source: CA07481-10
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 2075-133102 10.21 U20 1,1-Dichloroethene
ug/L1.0 20.0 1781-134109 40.15 U22 Benzene
ug/L1.0 20.0 1683-11799 20.17 U20 Chlorobenzene
ug/L1.0 20.0 1771-118113 20.14 U23 Toluene
ug/L1.0 20.0 2274-11994 60.15 U19 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9246
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 9447
ug/L 50.0 59-134Surrogate: Toluene-d8 9547
Batch 7E17025 - EPA 5030B_MS
Prepared: 05/17/2017 15:08 Analyzed: 05/18/2017 06:37Blank (7E17025-BLK1)
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 7E17025 - EPA 5030B_MS
Prepared: 05/17/2017 15:08 Analyzed: 05/18/2017 06:37Blank (7E17025-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.17 U 1,1,1,2-Tetrachloroethane
ug/L1.00.12 U 1,1,1-Trichloroethane
ug/L1.00.28 U 1,1,2,2-Tetrachloroethane
ug/L1.00.14 U 1,1,2-Trichloroethane
ug/L1.00.13 U 1,1-Dichloroethane
ug/L1.00.21 U 1,1-Dichloroethene
ug/L1.00.23 U 1,2,3-Trichloropropane
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.66 U 1,2-Dibromoethane
ug/L1.00.19 U 1,2-Dichlorobenzene
ug/L1.00.21 U 1,2-Dichloroethane
ug/L1.00.10 U 1,2-Dichloropropane
ug/L1.00.19 U 1,4-Dichlorobenzene
ug/L5.01.3 U 2-Butanone
ug/L5.00.88 U 2-Hexanone
ug/L5.01.1 U 4-Methyl-2-pentanone
ug/L2010U Acetone
ug/L103.5 U Acrylonitrile
ug/L1.00.15 U Benzene
ug/L1.00.48 U Bromochloromethane
ug/L1.00.17 U Bromodichloromethane
ug/L1.00.22 U Bromoform
ug/L1.00.14 U Bromomethane
ug/L5.01.5 U Carbon disulfide
ug/L1.00.17 U Carbon tetrachloride
ug/L1.00.17 U Chlorobenzene
ug/L1.00.23 U Chloroethane
ug/L1.00.18 U Chloroform
ug/L1.00.13 U Chloromethane
ug/L1.00.15 U cis-1,2-Dichloroethene
ug/L1.00.20 U cis-1,3-Dichloropropene
ug/L1.00.17 U Dibromochloromethane
ug/L1.00.27 U Dibromomethane
ug/L1.00.13 U Ethylbenzene
ug/L5.01.7 U Iodomethane
ug/L2.00.17 U m,p-Xylenes
ug/L1.00.23 U Methylene chloride
ug/L1.00.065 U o-Xylene
ug/L1.00.11 U Styrene
ug/L1.00.17 U Tetrachloroethene
ug/L1.00.14 U Toluene
ug/L1.00.21 U trans-1,2-Dichloroethene
ug/L1.00.15 U trans-1,3-Dichloropropene
ug/L1.00.70 U trans-1,4-Dichloro-2-butene
ug/L1.00.15 U Trichloroethene
ug/L1.00.24 U Trichlorofluoromethane
ug/L5.00.95 U Vinyl acetate
ug/L1.00.32 U Vinyl chloride
ug/L3.00.45 U Xylenes (Total)
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 7E17025 - EPA 5030B_MS
Prepared: 05/17/2017 15:08 Analyzed: 05/18/2017 06:37Blank (7E17025-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9950
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 10955
ug/L 50.0 59-134Surrogate: Toluene-d8 11256
Prepared: 05/17/2017 15:08 Analyzed: 05/18/2017 04:39LCS (7E17025-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-13311022 1,1-Dichloroethene
ug/L1.0 20.0 81-13412525 Benzene
ug/L1.0 20.0 83-1179519 Chlorobenzene
ug/L1.0 20.0 71-11810220 Toluene
ug/L1.0 20.0 74-11910120 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 10351
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 11557
ug/L 50.0 59-134Surrogate: Toluene-d8 11557
Prepared: 05/17/2017 15:08 Analyzed: 05/18/2017 05:08Matrix Spike (7E17025-MS1)
Source: CA07481-06
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-133800.21 U16 1,1-Dichloroethene
ug/L1.0 20.0 81-1341030.15 U21 Benzene
ug/L1.0 20.0 83-117880.17 U18 Chlorobenzene
ug/L1.0 20.0 71-1181010.14 U20 Toluene
ug/L1.0 20.0 74-119890.15 U18 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 10954
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 11357
ug/L 50.0 59-134Surrogate: Toluene-d8 10754
Prepared: 05/17/2017 15:08 Analyzed: 05/18/2017 05:38Matrix Spike Dup (7E17025-MSD1)
Source: CA07481-06
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 2075-13373 100.21 U15 QM-071,1-Dichloroethene
ug/L1.0 20.0 1781-13499 40.15 U20 Benzene
ug/L1.0 20.0 1683-11776 140.17 U15 QM-07Chlorobenzene
ug/L1.0 20.0 1771-11882 200.14 U16 QR-02Toluene
ug/L1.0 20.0 2274-11983 70.15 U17 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9548
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 10954
ug/L 50.0 59-134Surrogate: Toluene-d8 10955
Batch 7E19028 - EPA 5030B_MS
Prepared: 05/19/2017 16:24 Analyzed: 05/19/2017 19:29Blank (7E19028-BLK1)
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 7E19028 - EPA 5030B_MS
Prepared: 05/19/2017 16:24 Analyzed: 05/19/2017 19:29Blank (7E19028-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.17 U 1,1,1,2-Tetrachloroethane
ug/L1.00.12 U 1,1,1-Trichloroethane
ug/L1.00.28 U 1,1,2,2-Tetrachloroethane
ug/L1.00.14 U 1,1,2-Trichloroethane
ug/L1.00.13 U 1,1-Dichloroethane
ug/L1.00.21 U 1,1-Dichloroethene
ug/L1.00.23 U 1,2,3-Trichloropropane
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.66 U 1,2-Dibromoethane
ug/L1.00.19 U 1,2-Dichlorobenzene
ug/L1.00.21 U 1,2-Dichloroethane
ug/L1.00.10 U 1,2-Dichloropropane
ug/L1.00.19 U 1,4-Dichlorobenzene
ug/L5.01.3 U 2-Butanone
ug/L5.00.88 U 2-Hexanone
ug/L5.01.1 U 4-Methyl-2-pentanone
ug/L2010U Acetone
ug/L103.5 U Acrylonitrile
ug/L1.00.15 U Benzene
ug/L1.00.48 U Bromochloromethane
ug/L1.00.17 U Bromodichloromethane
ug/L1.00.22 U Bromoform
ug/L1.00.14 U Bromomethane
ug/L5.01.5 U Carbon disulfide
ug/L1.00.17 U Carbon tetrachloride
ug/L1.00.17 U Chlorobenzene
ug/L1.00.23 U Chloroethane
ug/L1.00.18 U Chloroform
ug/L1.00.13 U Chloromethane
ug/L1.00.15 U cis-1,2-Dichloroethene
ug/L1.00.20 U cis-1,3-Dichloropropene
ug/L1.00.17 U Dibromochloromethane
ug/L1.00.27 U Dibromomethane
ug/L1.00.13 U Ethylbenzene
ug/L5.01.7 U Iodomethane
ug/L2.00.17 U m,p-Xylenes
ug/L1.00.23 U Methylene chloride
ug/L1.00.065 U o-Xylene
ug/L1.00.11 U Styrene
ug/L1.00.17 U Tetrachloroethene
ug/L1.00.14 U Toluene
ug/L1.00.21 U trans-1,2-Dichloroethene
ug/L1.00.15 U trans-1,3-Dichloropropene
ug/L1.00.70 U trans-1,4-Dichloro-2-butene
ug/L1.00.15 U Trichloroethene
ug/L1.00.24 U Trichlorofluoromethane
ug/L5.00.95 U Vinyl acetate
ug/L1.00.32 U Vinyl chloride
ug/L3.00.45 U Xylenes (Total)
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 7E19028 - EPA 5030B_MS
Prepared: 05/19/2017 16:24 Analyzed: 05/19/2017 19:29Blank (7E19028-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 10351
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 10753
ug/L 50.0 59-134Surrogate: Toluene-d8 10352
Prepared: 05/19/2017 16:24 Analyzed: 05/19/2017 17:31LCS (7E19028-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-1339820 1,1-Dichloroethene
ug/L1.0 20.0 81-13410721 Benzene
ug/L1.0 20.0 83-1179719 Chlorobenzene
ug/L1.0 20.0 71-11810421 Toluene
ug/L1.0 20.0 74-11910120 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 10251
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 11055
ug/L 50.0 59-134Surrogate: Toluene-d8 10452
Prepared: 05/19/2017 16:24 Analyzed: 05/19/2017 18:00Matrix Spike (7E19028-MS1)
Source: CA07933-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-1331080.21 U22 1,1-Dichloroethene
ug/L1.0 20.0 81-1341180.15 U24 Benzene
ug/L1.0 20.0 83-1171040.17 U21 Chlorobenzene
ug/L1.0 20.0 71-1181110.14 U22 Toluene
ug/L1.0 20.0 74-1191110.15 U22 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 10251
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 10653
ug/L 50.0 59-134Surrogate: Toluene-d8 10251
Prepared: 05/19/2017 16:24 Analyzed: 05/19/2017 18:30Matrix Spike Dup (7E19028-MSD1)
Source: CA07933-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 2075-133104 40.21 U21 1,1-Dichloroethene
ug/L1.0 20.0 1781-134112 50.15 U22 Benzene
ug/L1.0 20.0 1683-11790 140.17 U18 Chlorobenzene
ug/L1.0 20.0 1771-11899 110.14 U20 Toluene
ug/L1.0 20.0 2274-119108 30.15 U22 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9347
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 10552
ug/L 50.0 59-134Surrogate: Toluene-d8 10452
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 7E17013 - EPA 3005A
Prepared: 05/17/2017 11:36 Analyzed: 05/19/2017 10:13Blank (7E17013-BLK1)
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 7E17013 - EPA 3005A
Prepared: 05/17/2017 11:36 Analyzed: 05/19/2017 10:13Blank (7E17013-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.06.80 U Arsenic
ug/L10.01.00 U Barium
ug/L1.000.130 U Beryllium
ug/L1.000.360 U Cadmium
ug/L10.01.40 U Chromium
ug/L10.01.10 U Cobalt
ug/L10.01.60 U Copper
ug/L10.03.10 U Lead
ug/L10.02.20 U Nickel
ug/L10.01.90 U Silver
ug/L10.01.40 U Vanadium
ug/L10.04.40 U Zinc
Prepared: 05/17/2017 11:36 Analyzed: 05/19/2017 10:21LCS (7E17013-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 80-12094189 Arsenic
ug/L10.0 200 80-120100200 Barium
ug/L1.00 20.0 80-1209819.7 Beryllium
ug/L1.00 20.0 80-12010020.0 Cadmium
ug/L10.0 200 80-12097195 Chromium
ug/L10.0 200 80-12099197 Cobalt
ug/L10.0 200 80-12097193 Copper
ug/L10.0 200 80-12099199 Lead
ug/L10.0 200 80-12097194 Nickel
ug/L10.0 200 80-12097194 Silver
ug/L10.0 200 80-12095190 Vanadium
ug/L10.0 200 80-12099198 Zinc
Prepared: 05/17/2017 11:36 Analyzed: 05/19/2017 10:26Matrix Spike (7E17013-MS1)
Source: CA05959-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 75-125946.80 U189 Arsenic
ug/L10.0 200 75-12595208399 Barium
ug/L1.00 20.0 75-125980.65920.3 Beryllium
ug/L1.00 20.0 75-125950.360 U19.0 Cadmium
ug/L10.0 200 75-125951.41192 Chromium
ug/L10.0 200 75-125957.26197 Cobalt
ug/L10.0 200 75-125951.82191 Copper
ug/L10.0 200 75-125933.10 U186 Lead
ug/L10.0 200 75-1259510.1200 Nickel
ug/L10.0 200 75-125942.19190 Silver
ug/L10.0 200 75-125951.67191 Vanadium
ug/L10.0 200 75-1259516.2206 Zinc
Prepared: 05/17/2017 11:36 Analyzed: 05/19/2017 10:29Matrix Spike Dup (7E17013-MSD1)
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 7E17013 - EPA 3005A
Prepared: 05/17/2017 11:36 Analyzed: 05/19/2017 10:29Matrix Spike Dup (7E17013-MSD1) Continued
Source: CA05959-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 2075-12594 0.26.80 U188 Arsenic
ug/L10.0 200 2075-12595 0.2208398 Barium
ug/L1.00 20.0 2075-12598 0.20.65920.3 Beryllium
ug/L1.00 20.0 2075-12595 0.30.360 U19.0 Cadmium
ug/L10.0 200 2075-12595 0.031.41192 Chromium
ug/L10.0 200 2075-12594 0.77.26195 Cobalt
ug/L10.0 200 2075-12594 0.21.82191 Copper
ug/L10.0 200 2075-12593 0.43.10 U185 Lead
ug/L10.0 200 2075-12595 0.110.1200 Nickel
ug/L10.0 200 2075-12594 0.12.19190 Silver
ug/L10.0 200 2075-12595 0.11.67191 Vanadium
ug/L10.0 200 2075-12595 0.0716.2206 Zinc
Prepared: 05/17/2017 11:36 Analyzed: 05/19/2017 10:31Post Spike (7E17013-PS1)
Source: CA05959-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L0.0100 0.200 80-120900.003610.184 Arsenic
mg/L0.0100 0.200 80-120950.2080.398 Barium
mg/L0.00100 0.0200 80-120980.0006590.0203 Beryllium
mg/L0.00100 0.0200 80-120955.72E-50.0190 Cadmium
mg/L0.0100 0.200 80-120950.001410.191 Chromium
mg/L0.0100 0.200 80-120940.007260.195 Cobalt
mg/L0.0100 0.200 80-120950.001820.192 Copper
mg/L0.0100 0.200 80-12093-0.001830.187 Lead
mg/L0.0100 0.200 80-120950.01010.200 Nickel
mg/L0.0100 0.200 80-120930.002190.188 Silver
mg/L0.0100 0.200 80-120940.001670.190 Vanadium
mg/L0.0100 0.200 80-120950.01620.207 Zinc
Batch 7E18016 - EPA 3005A
Prepared: 05/18/2017 10:27 Analyzed: 05/23/2017 15:04Blank (7E18016-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.000.370 U Antimony
ug/L3.000.910 U Selenium
ug/L1.000.110 U Thallium
Prepared: 05/18/2017 10:27 Analyzed: 05/23/2017 15:08Blank (7E18016-BLK2)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.000.370 U Antimony
ug/L3.000.910 U Selenium
ug/L1.000.110 U Thallium
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 7E18016 - EPA 3005A
Prepared: 05/18/2017 10:27 Analyzed: 05/23/2017 15:23LCS (7E18016-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 80-120101202 Antimony
ug/L3.00 200 80-120105211 Selenium
ug/L1.00 200 80-12099199 Thallium
Prepared: 05/18/2017 10:27 Analyzed: 05/23/2017 15:27Matrix Spike (7E18016-MS1)
Source: CA06786-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 75-125900.370 U180 Antimony
ug/L3.00 200 75-1251020.910 U203 Selenium
ug/L1.00 200 75-125920.110 U184 Thallium
Prepared: 05/18/2017 10:27 Analyzed: 05/23/2017 15:31Matrix Spike Dup (7E18016-MSD1)
Source: CA06786-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 2075-12589 10.370 U177 Antimony
ug/L3.00 200 2075-125103 10.910 U206 Selenium
ug/L1.00 200 2075-12593 10.110 U186 Thallium
Prepared: 05/18/2017 10:27 Analyzed: 05/23/2017 15:34Post Spike (7E18016-PS1)
Source: CA06786-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 80-120990.0479197 Antimony
ug/L3.00 200 80-12098-1.02197 Selenium
ug/L1.00 200 75-125890.0357179 Thallium
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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was
accepted based on acceptable LCS recovery.
QM-07
The RPD result exceeded the QC control limits; however, both percent recoveries were
acceptable. Sample results for the QC batch were accepted based on percent recoveries and
completeness of QC data.
QR-02
The Reporting Limit for this analyte has been raised to account for matrix interference.R-01
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