RA-5451_26996_CA_SAR_20160815

2512 Independence Blvd., Suite 200-34
Wilmington, North Carolina 28412
Telephone [phone] Fax [phone] www.atcassociates.com

August 15, 2016
Mr. Sean Patrick
North Carolina Department of Environmental Quality Division of Waste Management, UST Section
Raleigh Regional Office 1628 Mail Service Center Raleigh, North Carolina 27699-1628
Re: Soil Sampling Results - Revised
Former Pantry #3187
804 Durham Road Roxboro, Person County, North Carolina Risk Classification: I170D
NCDEQ Incident No. 26996
Dear Mr. Patrick:
On behalf of Circle K Stores, Inc. (Pantry), ATC Associates of North Carolina, P.C. (ATC) has prepared
this letter report to provide a summary of the laboratory analytical results from the recent soil sampling
event (as approved in TA-7).

Soil Sampling
On June 7, 2016, soil sampling was performed by ATC to determine the presence or absence of free product
at the referenced site. On this date, monitoring well MW-1 was gauged for the presence of free product
and depth to water. ATC did not measure free product within well MW-1 and the depth to water was
measured at approximately 16.10 feet below ground surface (bgs).

ATC collected soil samples for laboratory analyses using direct push technology. Two soil samples were
collected from each borehole at depths ranging from either five to seven feet bgs or seven to ten feet bgs
and ten to twelve feet bgs, above the saturated zone. Upon collection, the soil samples were placed in
laboratory-supplied containers, labeled (ASB-1A, ASB-1B, ASB-2A, ASB-2B, ASB-3A, ASB-3B,
ASB-4A, ASB-4B, ASB-5A, ASB-5B, ASB-6A, and ASB-6B), placed in ice, and delivered under
chain-of-custody to Con-test Analytical Laboratory (Con-test), in East Longmeadow, Massachusetts, for
analyses. The soil samples were analyzed for volatile organic compounds (VOCs) via EPA Method 8260B
including methyl tertiary-butyl ether (MTBE) and isopropyl ether (IPE) and semi-volatile VOCs via EPA
Method 8270D. Additionally, the soil samples were analyzed by Massachusetts Department of
Environmental Protection (MADEP) Methods for volatile petroleum hydrocarbon fractions (VPH) and
extractable petroleum hydrocarbon fractions (EPH). Boring logs are provided in Attachment I. The soil
sample locations are depicted in Figure 1.

TABLES

TABLE 1
SOIL ANALYTICAL DATA
FORMER PANTRY #3187
804 DURHAM ROAD
ROXBORO, PERSON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO. 26996
Sample Depth
(feet)
PID
Reading
(ppm)
Date
Sampled
BenzeneTolueneEthylbenzeneTotal XylenesMTBENaphthaleneIsopropylbenzenep-Isopropyltoluenen-Butylbenzenesec-Butylbenzenen-PropylbenzeneStyrene1,2,4-Trimethybenzene1,3,5-Trimethylbenzene1-Methylnaphthalene2-MethylnaphthaleneNaphthaleneC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsASB-1A 5-7 1.5 06/07/16 <0.0024 0.0022J <0.0024 0.0041J <0.0048 <0.0048 <0.0024 <0.0024 <0.0024 <0.0024 <0.0024 <0.0024 0.0010J <0.0024 <0.22 <0.22 <0.22 <15 <28 <13 <28
ASB-1B 10-12 35.0 06/07/16 0.0012J 0.0054 0.0045 0.0154 <0.0048 0.0032J <0.0024 <0.0024 <0.0024 <0.0024 <0.0024 <0.0024 0.0065 0.0014J <0.23 <0.23 <0.23 <17 <30 <13 <30
ASB-2A 5-7 1,481 06/07/16 <0.40 3.3 5.9 29.5 <0.40 4.1 0.80 0.30J 1.4 0.28J 2.9 0.080J 19 6.0 2.9 6.7 5.3 1,000 89 <27 1,349
ASB-2B 10-12 442 06/07/16 <0.072 0.091 0.26 1.15 <0.072 0.34 0.055J 0.024J 0.13 0.030J 0.22 <0.072 1.4 0.48 2.5 6.5 6.2 <17 65 40 56
ASB-3A 7-10 33.2 06/07/16 0.011 0.057 0.014 0.084 <0.0050 0.011 <0.0025 <0.0025 0.0012J <0.0025 0.0025 <0.0025 0.029 0.0077 <0.22 <0.22 <0.22 <16 <29 <13 <29
ASB-3B 10-12 122 06/07/16 <0.0021 0.0020J 0.0012J 0.0066J <0.0041 0.0047 <0.0021 <0.0021 0.00075J <0.0021 <0.0021 <0.0021 0.004 0.0010J <0.22 <0.22 <0.22 <15 <28 <13 <28
ASB-4A 7-10 3.1 06/07/16 <0.0023 <0.0023 <0.0023 <0.0069 <0.0046 <0.0046 <0.0023 <0.0023 <0.0023 <0.0023 <0.0023 <0.0023 <0.0023 <0.0023 <0.22 <0.22 <0.22 <13 <26 <13 <26
ASB-4B 10-12 2.3 06/07/16 <0.0021 0.0012J <0.0021 0.00083J <0.0041 <0.0041 <0.0021 <0.0021 <0.0021 <0.0021 <0.0021 <0.0021 <0.0021 <0.0021 <0.22 <0.22 <0.22 <15 <28 <13 <28
ASB-5A 5-7 1.0 06/07/16 <0.0021 0.0017J <0.0021 0.00309J <0.0043 <0.0043 <0.0021 <0.0021 <0.0021 <0.0021 <0.0021 <0.0021 <0.0021 <0.0021 <0.22 <0.22 <0.22 <14 <27 <13 <27
ASB-5B 10-12 23.2 06/07/16 <0.0020 0.0016J 0.00084J 0.0035J <0.0041 <0.0041 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.0020 <0.22 <0.22 <0.22 <15 <28 <13 <28
ASB-6A 5-7 23.7 06/07/16 <0.0024 0.0011J <0.0024 <0.0072 <0.0048 <0.0048 <0.0024 <0.0024 <0.0024 <0.0024 <0.0024 <0.0024 0.0015J <0.0024 <0.21 <0.21 <0.21 <14 <26 <12 19
ASB-6B 10-12 30.3 06/07/16 0.0023J 0.0018J 0.0056 0.0091J <0.0053 0.0085 <0.0027 <0.0027 <0.0027 <0.0027 0.0019J <0.0027 0.012 0.0033 <0.22 <0.22 <0.22 <16 <13 <29 15
0.0056 4.3 4.9 0.0019 0.091 0.16 1.7 0.12 4.3 3.3 1.7 1.5 8.5 8.3 0.004 3.6 0.16 68 540 #31
18 1,200 1,560 3,129 350 313 1,564 100 626 626 626 3,128 782 782 20 63 313 939 1,500 31,000 469
164 32,000 40,000 81,760 3,100 8,176 40,880 4,000 16,350 16,350 16,350 81,760 20,440 20,440 100 1,635 8,176 24,528 40,000 810,000 12,264
Notes:
1. MSCC denotes maximum soil contaminant concentration.
2. Concentrations reported in milligrams per kilogram (mg/kg).
3. "<" = not detected at or above the laboratory detection limit.
4. Bold indicates concentration equals or exceeds Residential MSCC.
5. Final C9-C18 Aliphatics values are calculated by adding C9-C12 Aliphatics to C9-C18 Aliphatics as reported in the laboratory report.
6. Final C9-C22 Aromatics are calculated by adding C9-C10 Aromatics with C11-C22 Aromatics as reported in the laboratory analytical report.
7. # Considered immobile.
8. J denotes concentration estimated by laboratory.
MADEP Methods for VPH and EPH
Industrial/Commerical MSCC
EPA Method 8270DEPA Method 8260B
Soil-to-Groundwater MSCC
Residential MSCC
Analytical Method
TABLE 2
SOIL ANALYTICAL DATA - CSA
PANTRY #3187804 DURHAM ROAD
ROXBORO, PERSON COUNTY, NORTH CAROLINANCDEQ INCIDENT NO. 26996
Soil BoringDepth (feet)Date SampledIncident PhaseDROGROBenzeneTolueneEthylbenzeneTotal XylenesMTBENaphthalene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzene2-HexanoneAcetoneChloroformIsopropyl etherIsopropylbenzenen-Butylbenzenen-Propylbenzenesec-ButylbenzeneC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 Aromatics5 2/6/2006 LSA ----8.19 87 32.6 177 <1.2 17.1 <1.2 <1.2 <6.2 <15 <1.2 <1.2 2.73 6.46 12.7 1.5 694 644.9 <8.7 377.2102/6/2006 LSA ----105 587 170 923 12.5 85.9 <2.7 <2.7 <14 <34 <2.7 5.66 14.9 28.3 62.9 6.05 882 437 <17 787.6152/6/2006 LSA ----98.6 434 136 691 <7.4 74.6 <7.4 <19 <37 <93 <7.4 <7.4 <7.4 22.2 47.7 <7.4 2,230 1,141 <37 1,98952/6/2006 LSA ----<0.0030 0.0117 <0.0030 0.0063 <0.0030 <0.0030 <0.0030 <0.0030 <0.015 <0.038 0.283 <0.0030 <0.0030 <0.0030 <0.0030 <0.0030 4.73 3.74 <8.6 ND102/6/2006 LSA ----0.0063 0.0177 0.0026 0.0133 <0.0022 <0.0022 <0.0022 <0.0022 <0.011 0.054 0.977 <0.0022 <0.0022 <0.0022 <0.0022 <0.0022 <2.3 ND <8.7 ND152/6/2006 LSA ----0.189 0.37 0.0764 0.591 1.34 0.0314 <0.0023 <0.0023 0.1 0.0589 0.797 0.0643 0.0063 0.0078 0.017 <0.0023 3.41 1.3 <8.2 1.52
5 2/6/2006 LSA ----<0.0033 0.0052 <0.0033 0.0253 <0.0033 <0.0033 <0.0033 <0.0033 <0.017 <0.042 <0.0033 <0.0033 <0.0033 <0.0033 <0.0033 <0.0033 <3.4 ND <8.7 ND102/6/2006 LSA ----<0.0024 0.0114 <0.0024 <0.0054 <0.0024 <0.0024 <0.0024 <0.0024 <0.012 <0.030 <0.0024 <0.0024 <0.0024 <0.0024 <0.0024 <0.0024 <2.5 ND <9 ND
15 2/6/2006 LSA ----<0.0023 0.0041 <0.0023 <0.0052 <0.0023 <0.0023 <0.0023 <0.0023 <0.012 <0.029 <0.0023 <0.0023 <0.0023 <0.0023 <0.0023 <0.0023 <2.6 ND <9.1 ND0-5 5/1/2012 CSA <13 <8.8 <0.005 <0.005 0.0065 <0.005 0.010 <0.005 <0.005 <0.005 <0.0099 0.16 <0.005 --<0.005 <0.005 0.0069 <0.005 --------
5-10 5/1/2012 CSA <13 <7.2 0.026 0.034 0.034 0.067 0.046 0.012 0.042 0.011 <0.014 0.18 <0.007 --<0.007 <0.007 <0.007 <0.007 <4.3 ND <20 ND10-14 5/1/2012 CSA <14 <13 0.011 0.0079 0.017 0.018 0.034 <0.0059 0.023 0.006 <0.012 0.29 <0.0059 --<0.0059 <0.0059 <0.0059 <0.0059 --------
0-5 5/1/2012 CSA <13 <6.8 <0.0076 <0.0076 <0.0076 <0.0076 <0.0076 <0.0076 <0.0076 <0.0076 <0.015 <0.15 <0.0076 --<0.0076 <0.0076 <0.0076 <0.0076 --------5-10 5/1/2012 CSA <13 <6.3 <0.0058 <0.0058 <0.0058 <0.00583 <0.0058 <0.0058 <0.0058 <0.0058 <0.012 <0.12 <0.0058 --<0.0058 <0.0058 <0.0058 <0.0058 <3.8 ND <19 ND
10-15 5/1/2012 CSA <14 <7.3 <0.0068 <0.0068 <0.0068 <0.0068 <0.0068 <0.0068 <0.0068 <0.0068 <0.014 <0.14 <0.0068 --<0.0068 <0.0068 <0.0068 <0.0068 --------0-5 5/1/2012 CSA <12 <7.7 <0.0072 <0.0072 <0.0072 <0.0072 <0.0072 <0.0072 <0.0072 <0.0072 <0.014 <0.14 <0.0072 --<0.0072 <0.0072 <0.0072 <0.0072 <4.6 ND <18 ND
5-10 5/1/2012 CSA <13 <6.5 <0.0067 <0.0067 <0.0067 <0.0067 <0.0067 <0.0067 <0.0067 <0.0067 <0.013 <0.13 <0.0067 --<0.0067 <0.0067 <0.0067 <0.0067 --------10-14 5/1/2012 CSA <13 <6.4 <0.0055 <0.0055 <0.0055 <0.0055 <0.0055 <0.0055 <0.0055 <0.0055 <0.011 <0.11 <0.0055 --<0.0055 <0.0055 <0.0055 <0.0055 --------
0-5 5/1/2012 CSA <12 <6.2 <0.0062 <0.0062 <0.0062 <0.0062 <0.0062 <0.0062 <0.0062 <0.0062 <0.012 <0.12 <0.0062 --<0.0062 <0.0062 <0.0062 <0.0062 --------
5-10 5/1/2012 CSA <12 <6.5 <0.0065 <0.0065 <0.0065 <0.0065 <0.0065 <0.0065 <0.0065 <0.0065 <0.013 <0.13 <0.0065 --<0.0065 <0.0065 <0.0065 <0.0065 --------
10-14 5/1/2012 CSA <13 <7.4 <0.0065 <0.0065 <0.0065 <0.0065 <0.0065 <0.0065 <0.0065 <0.0065 <0.013 <0.13 <0.0065 --<0.0065 <0.0065 <0.0065 <0.0065 <4.4 ND <20 ND
0-5 5/1/2012 CSA <12 <7.9 <0.0066 <0.0066 <0.0066 <0.0066 <0.0066 <0.0066 <0.0066 <0.0066 <0.013 <0.13 <0.0066 --<0.0066 <0.0066 <0.0066 <0.0066 --------5-9 5/1/2012 CSA <12 <5.7 <0.0084 <0.0084 <0.0084 <0.0084 <0.0084 <0.0084 <0.0084 <0.0084 <0.017 <0.17 <0.0084 --<0.0084 <0.0084 <0.0084 <0.0084 <3.4 ND <19 ND0-5 5/1/2012 CSA <12 <5.4 <0.0064 <0.0064 <0.0064 <0.0064 <0.0064 <0.0064 <0.0064 <0.0064 <0.013 <0.13 <0.0064 --<0.0064 <0.0064 <0.0064 <0.0064 <3.2 ND <19 ND5-10 5/1/2012 CSA <14 <6.8 <0.0051 <0.0051 <0.0051 <0.0051 <0.0051 <0.0051 <0.0051 <0.0051 <0.010 <0.1 <0.0051 --<0.0051 <0.0051 <0.0051 <0.0051 --------
10-11 5/1/2012 CSA <13 <5.9 <0.0078 <0.0078 <0.0078 <0.0078 <0.0078 <0.0078 <0.0078 <0.0078 <0.016 <0.16 <0.0078 --<0.0078 <0.0078 <0.0078 <0.0078 --------0-5 5/1/2012 CSA <13 <7.6 <0.0072 <0.0072 <0.0072 <0.0072 <0.0072 <0.0072 <0.0072 <0.0072 <0.014 <0.14 <0.0072 --<0.0072 <0.0072 <0.0072 <0.0072 --------
5-10 5/1/2012 CSA <13 <6.6 <0.0069 <0.0069 <0.0069 <0.0069 <0.0069 <0.0069 <0.0069 <0.0069 <0.014 <0.14 <0.0069 --<0.0069 <0.0069 <0.0069 <0.0069 --------
10-14 5/1/2012 CSA <13 6.1 0.009 <0.0057 <0.0057 <0.0057 0.0071 <0.0057 <0.0057 <0.0057 <0.011 <0.11 <0.0057 --<0.0057 <0.0057 <0.0057 <0.0057 <3 ND <19 ND
10 10 --------------------------------------------0.0056 4.3 4.9 4.6 0.091 0.16 8.5 8.3 0.1 24 0.37 0.37 1.7 4.3 1.7 3.3 68 540 NE 31
----18 1,200 1,560 3,129 350 313 782 782 70 14,000 20 156 1,564 626 626 626 939 1,500 31,000 469
----164 32,000 40,000 81,760 3,100 8,176 20,440 20,440 2,000 360,000 180 4,088 40,880 16,350 16,350 16,350 24,528 40,000 810,000 12,264
Notes:
1. "<" or ND = Not detected at or above the laboratory detection limit.
2. Concentrations are reported in milligrams per kilogram (mg/kg) = parts per million.
3. Concentrations in bold print equal or exceed the Residential MSCCs.
5. NCDEQ = North Carolina Department of Environmental Quality.
6. NE = Not Established.
7. MTBE = Methyl Tertiary Butyl Ether.
8. Maximum Soil Contaminant Coincentrations (MSCCs) are referenced in the "Groundwater Section
Guidelines for the Investigation and Remediation of Soil and Groundwater", July 2008.
SB-3
MW-1
MW-2
MW-3
SB-1
SB-2
Residential MSCC
Industrial/Commercial MSCC
SB-4
SB-5
SB-6
SB-8
NCDEQ State Action Level
Soil-to-Groundwater MSCC

FIGURE

ATTACHMENT I

Roxboro, North Carolina804 Durham Road
Pantry #3187
Client: The Pantry, Inc.
Refusal at 17.5 feet bgs.

BORING LOG: ASB-1
(Page 1 of 1)
Date(s) Drilled : 6/6/16
Drilling Conractor : GEX
Drilling Method : Direct Push
Boring Diameter : 2 Inches
Sampling Method : Macrocore
Sampling Interval : Continuous
Logged By : Chris Hanley
Depth in Feet0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
Surf.
Elev.USCSAR
CL
CL
CL GRAPHICDESCRIPTION
Concrete
Silty CLAY, light brown, dry, low plasticity.
Silty CLAY, dark brown/orange/light gray, moist, med plasticity.
Silty CLAY, dark brown/brown with lenses of light gray clay, very moist, med-high plasticity.
Refusal on rock.
PID ppm
(Sample ID)
4.6
1.5 (SB-1A)
3.3
35.0 (SB-1B)
227
Roxboro, North Carolina804 Durham Road
Pantry #3187
Client: The Pantry, Inc.

BORING LOG: ASB-2
(Page 1 of 1)
Date(s) Drilled : 6/6/16
Drilling Conractor : GEX
Drilling Method : Direct Push
Boring Diameter : 2 Inches
Sampling Method : Macrocore
Sampling Interval : Continuous
Logged By : Chris Hanley
Depth in Feet0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Surf.
Elev.USCSAR
SM
CL
CL
CL
SC GRAPHICDESCRIPTION
Concrete
Silty SAND, dark gray, non-uniform, dry.
Silty CLAY, light brown, dry, med-low plasticity.
Silty CLAY, dark brown/brown/light gray, moist, med plasticity.
Silty CLAY, light gray/light tan, very moist, low plasticity.
Clayey SAND with some silt, dark gray with light gray bands, wet, no plasticity.
Bottom of boring.
PID ppm
(Sample ID)
4.4
575
1,481 (SB-2A)
136
442 (SB-2B)
336
Roxboro, North Carolina804 Durham Road
Pantry #3187
Client: The Pantry, Inc.

BORING LOG: ASB-3
(Page 1 of 1)
Date(s) Drilled : 6/6/16
Drilling Conractor : GEX
Drilling Method : Direct Push
Boring Diameter : 2 Inches
Sampling Method : Macrocore
Sampling Interval : Continuous
Logged By : Chris Hanley
Depth in Feet0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Surf.
Elev.USCSAR
CL
CL GRAPHICDESCRIPTION
Concrete
Silty CLAY, dark brown, dry, low plasticity.
Silty CLAY, dark brown with red mottling and thin lenses of light gray clay, moist, med platicity.
Bottom of boring.
PID ppm
(Sample ID)
16.2
9.5
1.2
33.2 (SB-3A)
122 (SB-3B)
116
Roxboro, North Carolina804 Durham Road
Pantry #3187
Client: The Pantry, Inc.

BORING LOG: ASB-4
(Page 1 of 1)
Date(s) Drilled : 6/6/16
Drilling Conractor : GEX
Drilling Method : Direct Push
Boring Diameter : 2 Inches
Sampling Method : Macrocore
Sampling Interval : Continuous
Logged By : Chris Hanley
Depth in Feet0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Surf.
Elev.USCSAR
CL
CL GRAPHICDESCRIPTION
Concrete
Silty CLAY, light brown, dry, med-low plasticity.
Silty CLAY, light brown/light gray/dark brown, med plasticity, moist.
Bottom of boring.
PID ppm
(Sample ID)
6.3
2.7
2.5
3.1 (SB-4A)
2.3 (SB-4B)
1.2
Roxboro, North Carolina804 Durham Road
Pantry #3187
Client: The Pantry, Inc.

BORING LOG: ASB-5
(Page 1 of 1)
Date(s) Drilled : 6/6/16
Drilling Conractor : GEX
Drilling Method : Direct Push
Boring Diameter : 2 Inches
Sampling Method : Macrocore
Sampling Interval : Continuous
Logged By : Chris Hanley
Depth in Feet0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Surf.
Elev.USCSAR
CL
CL
CL GRAPHICDESCRIPTION
Asphalt
Silty CLAY, light brown, dry, med-low plasticity.
Silty CLAY, dark brown with thin lenses of bluish gray clay, med plasticity, moist.
Silty CLAY, light gray/tan, wet, med plasticity.
Bottom of boring.
PID ppm
(Sample ID)
0.7
0.7
1.0 (SB-5A)
21.2
23.2 (SB-5B)
89.1
Roxboro, North Carolina804 Durham Road
Pantry #3187
Client: The Pantry, Inc.

BORING LOG: ASB-6
(Page 1 of 1)
Date(s) Drilled : 6/6/16
Drilling Conractor : GEX
Drilling Method : Direct Push
Boring Diameter : 2 Inches
Sampling Method : Macrocore
Sampling Interval : Continuous
Logged By : Chris Hanley
Depth in Feet0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Surf.
Elev.USCSAR
CL
CL
CL
SC GRAPHICDESCRIPTION
Asphalt
Silty CLAY, dark brown/brown/light gray, dry, low platicity.
Silty CLAY, light brown/light gray, moist, med plasticity.
Silty CLAY, light brown with lenses of light gray clay, very moist, med plasticity.
Clayey SAND, tan/light gray, coarse, wet.
Bottom of boring.
PID ppm
(Sample ID)
0.9
6.6
23.7 (SB-5A)
28.3
30.3 (SB-5B)
18.2
16.2
84.7

ATTACHMENT II
Page 1 of 133
Table of Contents
Table of Contents
Sample Summary 4
Hits Only Report 6
Case Narrative 9
Sample Results 13
16F0430-01 13
16F0430-02 20
16F0430-03 27
16F0430-04 34
16F0430-05 41
16F0430-06 48
16F0430-07 55
16F0430-08 62
16F0430-09 69
16F0430-10 76
16F0430-11 83
16F0430-12 90
Sample Preparation Information 97
QC Data 99
Volatile Organic Compounds by GC/MS 99
B151035 99
B151093 103
Semivolatile Organic Compounds by GC/MS 109
B151004 109
Petroleum Hydrocarbons Analyses - EPH 117
B151027 117
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Table of Contents (continued)
Petroleum Hydrocarbons Analyses - VPH 121
B151058 121
Flag/Qualifier Summary 123
Certifications 124
Chain of Custody/Sample Receipt 130
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