21031 Ideal Tool PhII LSA 20170519

LIMITED PHASE II
ENVIRONMENTAL SITE ASSESSMENT
REPORT

Ideal Tool & Die Property
3021 & 3029 Bank Street
Charlotte, North Carolina 28203

Prepared For:

LEH NC Bank, LLC
c/o: Mr. Nikolaus Matthias Lischerong
310 Arlington Ave Suite 402
Charlotte, North Carolina 28203

Prepared By:

HRP Associates, Inc.
1327 Miller Road, Suite D
Greenville, SC 29607

Consultant Project #: LIS2000.P2

Issued On: May 19, 2017

Limited Phase II Environmental Site Assessment
3021 & 3029 Bank St, Charlotte, NC
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TABLE OF CONTENTS
1.0 INTRODUCTION ........................................................................................................ 1
2.0 UTILITY MARKOUT AND GROUND PENETRATING RADAR SURVEY .......................... 2
2.1 Utility Markout ....................................................................................................... 2
2.2 Ground Penetrating Radar ...................................................................................... 2
3.0 MONITORING WELL PERMIT .................................................................................... 3
4.0 LIMITED SOIL AND GROUNDWATER INVESTIGATION ............................................. 4
4.1 Soil Boring Investigation ......................................................................................... 4
4.1.1 Subsurface Geology and Hydrogeology ......................................................... 5
4.1.2 Soil Boring Summary and Results ................................................................. 5
4.2 Groundwater Investigation ..................................................................................... 6
4.3 Boring Abandonment.............................................................................................. 6
4.4 Investigation Derived Wastes .................................................................................. 6
5.0 ANALYTICAL DATA .................................................................................................... 7
5.1 Soil Analytical Results ............................................................................................. 7
5.2 Groundwater Analytical Results ............................................................................... 7
5.3 Quality Assurance/Quality Control Samples .............................................................. 8
5.4 Equipment Decontamination ................................................................................... 8
6.0 CONCLUSIONS .......................................................................................................... 9
7.0 REFERENCES ........................................................................................................... 10
FIGURES

Figure 1 Site Location Figure 2 Site Plan
Tables
Table 1 Soil and Groundwater Investigative Summary
Table 2 Soil Analytical Data Summary
Table 3 Groundwater Analytical Data Summary APPENDICES

Appendix A: Subsurface Investigation Permit Appendix B: Soil Boring Logs
Appendix C: Field Data Sheets/Equipment Calibration Logs
Appendix D: Laboratory Analytical Report

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General Information

Project/Site Information: Consultant Information:
Ideal Tool & Die Property
3021 & 3029 Bank Street
Charlotte, NC 28203
HRP Associates, Inc.
1327 Miller Road, Suite D
Greenville, SC 29607 Phone: [phone]
Fax: [phone]
Site Access Contact: Mr. Nick Lischerong E-mail: [e-mail]

Project Number: LIS2000.P2
Client Information:
LEH NC Bank, LLC
c/o: Mr. Nikolaus Matthias Lischerong
310 Arlington Ave Suite 402
Charlotte, North Carolina 28203

Inspection Date: 05/02/2017
Report Date: 05/19/2017

Site Assessor and
Report Author: G. Storm Caldwell, GIT# 37
Project Geologist

Professional Daniel E McDonnell, PG# 2005 (NC) Geologist: Project Manager

Client Manager:
Robert “Ty” Hawkins
Project Manager

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1.0 INTRODUCTION
HRP Associates, Inc. (HRP) has completed a Limited Phase II Environmental Site Assessment (ESA) at
the Ideal Tool & Die property, located at 3021 and 3029 Bank Street in Charlotte, North Carolina
(herein referred to as the “Site”). A Site location map is included as Figure 1.

At the time of HRP’s May 2, 2017 field investigation, the Site consisted of two (2) contiguous parcels
of land identified by the Mecklenburg County Tax Assessor as parcels 14505205 and 14505206. Four (4) buildings totaling 13,624 square feet currently improve the Site, which were constructed in 1957.
Prior to 1957, the Site consisted of a portion of a baseball field (circa 1951) and undeveloped and/or
agricultural farmland (circa 1948). The Site buildings are constructed on a concrete slab, with brick
walls and pitched metal roofing. The Site has historically been occupied by Ideal Tool & Die, a tool
and die fabrication company, since 1974. The remainder of the Site consists of a loading dock,
fenced in front and rear areas, and a concrete parking area.

Please note that this Limited Phase II ESA was performed of the Site at your request as a “limited”
assessment in order to further assess current Site conditions. The work conducted by HRP was
performed as outlined in the HRP proposal dated April 6, 2017. HRP’s proposal provided guidelines
with respect to evaluation of certain areas of concern identified on the property along with a general
work plan, time frame, drilling program, investigatory techniques, and laboratory parameters. HRP
developed and implemented this scope of work based on the area of concern identified during HRP’s
Phase I ESA dated April 6, 2017 and information requested by the Client.

This report presents the following:

 Utility Mark-out and a Ground Penetrating Radar (GPR) Survey

 Monitoring Well Permit

 Limited Soil and Groundwater Investigation

 Analytical Data Summary
 Conclusions

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2.0 UTILITY MARKOUT AND GROUND PENETRATING RADAR SURVEY
2.1 Utility Markout
North Carolina 811 was contacted to identify public underground utilities at the Site prior to initiation
of the subsurface investigation.

2.2 Ground Penetrating Radar
A ground-penetrating radar (GPR) survey was performed at the Site prior to drilling activities to protect unidentified subsurface utility lines and other unforeseen subsurface obstructions. GPR
involves scanning the subsurface with a device that emits and records the return signals of
electromagnetic energy in the radar wavelength. HRP representatives established a survey grid of the
anticipated areas of investigation in an attempt to identify utility lines or other buried objects located
in the area prior to advancement of soil borings and/or temporary monitoring wells.

An approximate 20-foot radius around each of the soil borings was evaluated using GPR equipment. Unidentified subsurface objects, such as buried drums, USTs, or other discarded materials, were not
observed in the vicinity of the proposed borings during the GPR survey.

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3.0 MONITORING WELL PERMIT

HRP prepared and submitted a Subsurface Investigation Permit (SIP) to the Mecklenburg County
Health Department Groundwater & Wastewater Services Division prior to the installation of
temporary groundwater monitoring wells on the Site as required. Mecklenburg County approved
the installation of the proposed temporary groundwater monitoring wells (Permit #: 70002425). A
copy of the Subsurface Investigation Permit Approval letter is included as Appendix A.
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4.0 LIMITED SOIL AND GROUNDWATER INVESTIGATION
4.1 Soil Boring Investigation
On May 2, 2017, HRP advanced seven (7) soil borings on-Site to assess soil and groundwater
conditions. The location of each of the borings is summarized in the table below and depicted in
Figure 2. Additional information is provided in Table 1.

A Geoprobe® 6620DT mobile drill rig utilizing direct push technology was used to advance each boring. Five-foot soil macro-cores were collected continuously during boring advancement. Each
macro-core was screened for volatile organic compounds (VOCs) at one-foot intervals using a
calibrated MiniRae 3000 photo-ionization detector (PID). Soil boring logs are included in Appendix B.
The following table provides a brief description of each soil boring advanced at the Site.

Boring
ID Location of Boring
Total
Boring
Depth
(ft
bgs)
Depth to
Groundwater
(ft bgs)
Maximum
PID
Reading
(ppm)
Soil
Sample
Collected
Groundwater
Sample
Collected
SB-1 Northwestern area of the Site 34.5 30.42 133 Yes Yes
SB-2 Western area of the Site 18 NE 0.0 Not
Collected Not Collected
SB-3 Loading dock area 28 NE 760 Yes Not Collected
SB-4 Inside the Site building, adjacent to the machine press and sump 33 29.14 1.5 Yes Yes
SB-5 Southwest area of Site 2.5 NE NA Not
Collected Not Collected
SB-6 Southern property
boundary 23 NE 583 Yes Not Collected
SB-7 Southeastern property
boundary 29 22.43 4.5 Yes Yes

NE – Not encountered bgs- below ground surface TOC- top of casing

SB-1 This boring was advanced along the northwestern corner of the Site. This boring was
advanced to a total depth of approximately 34.5 feet below ground surface (bgs). A
maximum PID detection of 133 ppm was observed at a depth of approximately 17 feet bgs within this boring. A soil sample was collected from the depth interval of 17-18 feet bgs.
Groundwater was encountered at approximately 30.42 feet bgs in this boring.

SB-2 This boring was advanced along the western boundary of the Site. This boring was advanced to a total depth of approximately 18 feet bgs. PID detections were not observed in soils
screened within this boring. A soil sample was not collected from this boring. Groundwater
was not encountered in this boring.
SB-3 This boring was advanced within the fenced in loading dock area near the center of the Site.
This boring was advanced to a total depth of approximately 28 feet bgs. A maximum PID
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detection of 730 ppm was observed at a depth of approximately 14 feet bgs within this boring.
A soil sample was collected from the depth interval of 14-15 feet bgs. Groundwater was not
encountered in this boring.

SB-4 This boring was advanced within the interior of the Site building and adjacent to the former
machine press and sump. The boring was advanced to a total depth of approximately 33 feet
bgs. A maximum PID detection of 1.5 ppm was observed at a depth of approximately 5 feet bgs within this boring. A soil sample was collected from the depth interval of 5-6 feet bgs.
Groundwater was encountered at approximately 29.14 feet bgs in this boring.

SB-5 This boring was advanced along the southwestern corner of the Site. The boring was
advanced to a total depth of approximately 2.5 feet bgs. Soil was not screened for PID
detections within this boring due to a lack of soil recovery. A soil sample was not collected
from this boring. Groundwater was not encountered in this boring.

SB-6 This boring was advanced along the central southwestern Site boundary. The boring was
advanced to a total depth of approximately 23 feet below ground surface (bgs). A maximum
PID detection of 583 ppm was observed at a depth of approximately 12 feet bgs within this
boring. A soil sample was collected from the depth interval of 11-12 feet bgs. Groundwater
was not encountered in this boring.

SB-7 This boring was advanced along the southern corner of the Site. The boring was advanced to
a total depth of approximately 29 feet below ground surface (bgs). A maximum PID detection
of 4.5 ppm was observed at a depth of approximately 2 feet bgs within this boring. A soil
sample was collected from the depth interval of 3-5 feet bgs. Groundwater was encountered at approximately 22.43 feet bgs in this boring.

4.1.1 Subsurface Geology and Hydrogeology
Geology at the Site consists largely of a reddish-brown silt and clay with saprolitic transitions. Soil
boring logs are provided in Appendix B.

In general, groundwater flow is influenced by a variety of pedologic, topographic, hydrologic, geologic, and cultural factors. In unconfined, unconsolidated aquifers (like that presumed to be
present at shallow depths beneath the Site), groundwater flow generally mimics topography. Based
upon regional topography, and the location of surface water bodies, shallow groundwater at the Site
presumably flows towards the south-southwest.
4.1.2 Soil Boring Summary and Results
A total of five (5) soil samples were collected from the seven (7) borings advanced at the Site. One (1) soil sample was collected at the depth interval associated with the adjacent sub-grade sump
within the Site building and four (4) soil samples were collected at the depth interval associated with
elevated PID readings during advancement of the borings. Soil samples were collected at the
following depths:

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Sample
ID
Total Boring Depth
(feet bgs)
Soil Sample Depth
(feet bgs)
Observed PID
Reading
(ppm)
SB-1 34.5 17-18 133
SB-3 28 14-15 730
SB-4 33 5-6 1.5
SB-6 23 11-12 583
SB-7 29 3-5 4.5

4.2 Groundwater Investigation
Groundwater was observed within soil borings SB-1, SB-4, and SB-7, each of which was converted to
a temporary groundwater monitoring well (identified as TMW-1, TMW-4, and TMW-7 respectively). At SB-2, SB-3, SB-5, and SB-6, refusal was encountered at 18, 28, 2.5, and 23 feet bgs respectively;
groundwater was not observed in these borings.

Each temporary well was constructed of a 1-inch PVC riser with a 10-foot slotted-screen. Prior to sampling, each well was developed to remove sediment and to minimize turbidity within the well.
Development was considered complete when the well produced groundwater samples with stabilized
pH, conductivity, temperature, and relative turbidity stabilized. One (1) grab groundwater sample was
collected from each temporary monitoring well. Groundwater samples were collected on May 2, 2017
using a peristaltic pump and associated tubing. Water quality parameters were recorded prior to
sample collection, documented in the Field Data Sheets included in Appendix C.

4.3 Boring Abandonment
Each of the seven (7) borings were abandoned in accordance with NC DEQ Well Construction
Standards (15 NCAC 02C .0100) by a licensed well driller.

4.4 Investigation Derived Wastes
All soil cuttings and the purged groundwater generated during this assessment were temporarily
staged on-site in one (1) 55-gallon steel drum and positioned within the fenced in portion of the
loading dock area. A label was placed on the drum noting its content, along with HRP’s contact
information.
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5.0 ANALYTICAL DATA
HRP collected five (5) soil samples and three (3) groundwater samples from the borings and
temporary wells at the Site. All samples were submitted under Chain-of-Custody to a laboratory
certified in North Carolina.

A copy of the Laboratory Analytical Report is provided in Appendix D. The soil analytical results
were compared to the NC Industrial/Commercial Health Based Preliminary Soil Remediation Goal, NC Protection of Groundwater Preliminary Soil Remediation Goal, and NC Soils Average Concentrations
(2005-2007). Groundwater analytical results were compared to the NC 2L Groundwater Standards
and the NC Non-Residential Groundwater Screening Level.

5.1 Soil Analytical Results
Soil samples were collected from five (5) soil borings advanced at the Site (SB-1, SB-3, SB-4, SB-6,
and SB-7), and were analyzed for the following constituents:

 Volatile Organic Compounds (VOCs) (Full-list) – EPA Method 8260B
 Semi Volatile Organic Compounds (SVOCs) (Full-list) – EPA Method 8270D
 Priority Pollutant Metals via EPA 7470A
 PCBs via EPA 8082A

As shown in Table 2, the only organic compound detected was toluene, at a concentration of 7.8 mg/kg, which is slightly above the NC Protection of Groundwater Preliminary Soil Remediation Goal
standard of 5.5 mg/kg. SVOCs or PCBs were not detected above laboratory reporting limits in any of
the five (5) soil samples.
Priority Pollutant metals were not detected in exceedance of the NC Industrial/Commercial Health
Based Preliminary Soil Remediation Goal or the NC Protection of Groundwater Preliminary Soil
Remediation Goal (Table 2).

5.2 Groundwater Analytical Results
Groundwater samples were collected from three (3) temporary groundwater monitoring wells installed
at the Site (TMW-1, TMW-4, and TMW-7). Groundwater samples were analyzed for the following
constituents:

 Volatile Organic Compounds (VOCs) (Full-list) – EPA Method 8260B
 Semi Volatile Organic Compounds (SVOCs) (Full-list) – EPA Method 8270D
 Priority Pollutant Metals via EPA 7470A
 PCBs via EPA 8082A

Chromium was detected within TMW-4 in exceedance of the NC 2L Groundwater Standard (10 µg/L)
at a concentration of 12.8 µg/L. Iron was detected within TMW-1, TMW-4, and TMW-7 in exceedance
of the NC 2L Groundwater Standard (300 µg/L) with values of 2,840, 5,450, and 4,680 µg/L,
respectively. However, collected groundwater samples had high amounts of suspended solids, which
may contribute to elevated metal concentrations in preserved groundwater samples relative to Site
groundwater.
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Carbon tetrachloride was detected within TMW-7 in exceedance of the NC 2L Groundwater Standard
(0.3 µg/L) at a concentration of 12.0 µg/L. 1,2-Dichloropropane was detected within TMW-4 and
TMW-7 in exceedance of the NC 2L Groundwater Standard (0.6 µg/L) at concentrations of 1.0 and 1.3
µg/L, respectively. Tetrachloroethene was detected within TMW-1, TMW-4, and TMW-7 in exceedance
of the NC 2L Groundwater Standard (0.7 µg/L) at concentrations of 3.5, 5.3, and 8.5 µg/L,
respectively. Trichloroethene was detected within TMW-1, TMW-4, and TMW-7 in exceedance of the
NC 2L Groundwater Standard (3 µg/L) with values of 5.6, 13.0, and 9.3 µg/L, respectively.
SVOCs and PCBs were not detected above the laboratory reporting limit in any of the three (3)
groundwater samples.

5.3 Quality Assurance/Quality Control Samples
Samples were collected by HRP in accordance with the EPA Region IV SESD’s Field Branches Quality
System and Technical Procedures. All appropriate measures were taken to ensure the proper
collection and handling of samples in order to provide representative Site data.
Field instruments used as part of this assessment were calibrated in accordance with HRP’s internal
quality control procedures and laboratory certification requirements. A copy of the associated field
calibration log is provided in Appendix C.
Typical laboratory quality assurance/quality control (QA/QC) procedures were conducted and included
a laboratory blank, standard, duplicate, and spike samples. The results of the laboratory QA/QC
samples indicate that the laboratory data for the submitted soil samples are considered reliable, valid
and sufficient for the purpose of this assessment.
5.4 Equipment Decontamination
All reusable down-hole investigative equipment was decontaminated before first use and between
sampling locations. Field sampling equipment decontamination procedures were consistent with the EPA Region IV Equipment Cleaning and Decontamination Operating Procedure. Disposable macro-core
plastic liners were utilized to advance each boring. Samples were collected using disposable nitrile
gloves and all appropriate measures were taken to ensure the proper collection and handling of
samples in order to provide representative Site data.
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6.0 CONCLUSIONS
A Limited Phase II Environmental Site Assessment was performed at the Site for the purpose of
further assessing Site conditions.

HRP concludes the following based upon the May 2, 2017 Limited Phase II ESA:

 HRP advanced seven (7) soil borings at the Site to assess the potential impact from historical operations at the Site;

 Groundwater was encountered in three (3) of the seven (7) soil borings, and temporary groundwater monitoring wells were installed in these three (3) boring locations;

 Five (5) soil samples and three (3) groundwater samples were collected to evaluate Site conditions; and,
 Contaminants of concern (COC) were observed above applicable NCDEQ Remediation Goals
and 2L Groundwater Standards in one (1) of the five (5) soil samples and in each of the three (3) groundwater samples collected at the Site.

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7.0 REFERENCES
 American Society for Testing and Materials 2013. Standard Practice for Environmental Site
Assessments: Phase II Environmental Site Assessment Process: ASTM, Philadelphia, PA, ASTM E1903-11, 21 pp.

 U.S. Geological Survey. Groundwater Atlas of the United States.

 Soil Survey Staff, Natural Resources Conservation Service, United States Department of
Agriculture. Web Soil Survey.

 EPA Region IV SESD’s Field Branches Quality System and Technical Procedures.

 EPA Region IV Equipment Cleaning and Decontamination Operating Procedure (SESDPROC-205-R1, November 1, 2007).

 EPA Regional Screening Levels (May 2016)

 EPA Maximum Contaminant Levels (Taken from EPA RSL Summary Table- May 2016)

 NC Division of Waste Management Non-Residential Vapor Intrusion Screening Concentrations,
Groundwater Screening Level (GWSL), October 2016

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FIGURES

COMPILED: 5/5/2017
Figure 1 Site Location Ideal Tool & Die Property 3021 & 3029 Bank St Charlotte, NC HRP #: LIS2000.P2 Scale: 1” = 2,000’

North Revisions Date No.. Designed By: GSC Drawn By: GSC Reviewed RTH Issue Date: 03/13/2017 Project No: LIS2000.P2 Sheet Size: 11 x 17 Site Plan Ideal Tool & Die 3021 & 3029 Bank St Charlotte, NC
FIGURE NO.

2 50 ft
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TABLES
Boring Designation Approx. Sample Location Area of Concern Boring Depth
(ft bgs)
Max. Field
Screening Results
(ppm) / Depth (ft
bgs)
Soil Sample
Collected
Groundwater
Sample Collected
SB-1 Northwest area of the Site Adjacent to neighboring
property with known release 34.5 133 / 17 Yes TMW-1
SB-2 West area of the Site Western Site boundary 18 0.0 No No
SB-3 Loading dock area Drum storage area 28 760 / 15 Yes No
SB-4 Inside Site building, adjacent to
machine press
Staining on floor of Site
building 33 1.5 / 5 Yes TMW-4
SB-5 Southern property boundary Downgradient of Site activities 2.5 NA No No
SB-6 Southern property boundary Downgradient of Site activities 23 583 / 12 Yes No
SB-7 Southeastern property
boundary
Adjacent to former UST at
neighboring property 29 4.5 / 2 Yes TMW-7
NOTES:
1. SB = Soil boring
2. bgs = below ground surface
3. ppm = parts per million
4. NA = not applicable
TABLE 1
Ideal Tool and Die Property
Soil and Groundwater Investigative Summary
Sample(s) collected: 5/2/2017
3021 and 3029 Bank Street, Charlotte, NC
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Sample ID SB-1 (17-18)SB-3 (14-15)SB-4 (5-6)SB-6 (11-12)SB-7 (3-5)
NC
Industrial/Commercial
Health Based
Preliminary Soil
Remediation Goal
(mg/kg)
NC Protection of
Groundwater
Preliminary Soil
Remediation Goal
(mg/kg)
Field Screening results (ppm) / Depth of Sample
Collection (ft bgs)133 / 17-18 730 / 14-15 1.5 / 5-6 583 / 11-12 4.0 / 3-5 --
Approx. Boring Depth (bgs) Achieved 34.5 28 33 23 29 --
PCBs
Metals
Arsenic <0.47 1.2 4.6J 2.8J 1.4 3 5.8
Beryllium 0.32 1.1 0.69 0.42 0.41 460 63
Chromium 6.8 16.4 11.6 13.6 18.4 100,000 360,000
Copper 16.8 51.2 55.1 39.3 34.1 9400 700
Lead 2.0 2.4 9.4 7.6 16.9 800 270
Nickel 6.5 28.9 9.5 6.6 25 NE NE
Selenium 1.3 1.3 <2.6 2.3J 1.1 1160 2.1
Zinc 61.0 68.3 46.0 53.3 33.5 70,000 1200
Volatile Organic Compounds
Semi-Volatile Organic Compounds
Volatile Organic Compounds
Toluene 5.8J 5.3J 7.8 5.2J 4.7J 818 5.5
NOTES:1. Concentrations displayed are only those reported above the associated laboratory reporting limits.
2. Values indicated in bold exceed NC background levels3. Shaded values exceed a regulatory standard
4. bgs- below ground surface
5. J values are an estimated concentration in-between the laboratory detection and reporting limit.
6. Shaded values indicate exceedances of NC DEQ Remediation Goals
(mg/kg)
None detected above laboratory reporting limits
(mg/kg)
(mg/kg)
(mg/kg)
(mg/kg)
None detected above laboratory reporting limits
None detected above laboratory reporting limits
TABLE 2
3021 and 3029 Bank Street, Charlotte, NC
Ideal Tool and Die Property
Soil Analytical Data Summary
Sample(s) collected: 5/2/2017
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Sample ID TMW-1 TMW-4 TMW-7
NC 2L
Groundwater
Standards
(µg/L)
NC Non-Residential
Groundwater Screening
Level (µg/L) 4
Depth to Groundwater (ft bgs)30.42 29.14 22.43 --
Boring Depth Achieved (ft bgs)34.5 33 29 --
PCBs
Metals
Chromium <2.5 12.8 5.8 10 NA
Copper 8.3 13.8 28.6 1000 NA
Iron 2,840 5,450 4,680 300 NA
Nickel 2.5J 11.1 18.5 100 NA
Zinc 8.1J 9.8J 35.1 1000 NA
Semi-Volatile Organic Compounds (PAHs)
Volatile Organic Compounds
Carbon tetrachloride <0.25 <0.25 12.0 0.3 18.1
Chloroform 0.90J 3.6 4.9 70 35.5
1,1-Dichloroethane 1.1 2.1 3.0 6 334
1,1-Dichloroethene <0.56 0.75J 1.3 NE 164
cis-1,2-Dichloroethene 2.2 4.6 5.7 70 NE
1,2-Dichloropropane <0.27 1.0 1.3 0.6 30.4
Methyl-tert-butyl-ether <0.21 <0.21 2.0 20 19,700
Tetrachloroethene 3.5 5.3 8.5 0.7 48.4
Trichloroethene 5.6 13.0 9.3 3 4.35
NOTES:1. TCEQ's Protective Concentration Limits (PCLs), March 4, 20162. Concentrations displayed are only those reported above the associated laboratory reporting limits.
3. Shaded values indicate an exceedance of NC DEQ groundwater standards
4. NC Division of Waste Management Non-Residential Vapor Intrusion Screening Concentrations, Groundwater Screening Level (GWSL), October 2016
(µg/L or ppb)
(µg/L or ppb)
(µg/L or ppb)
(µg/L or ppb)
None Detected
None Detected
TABLE 3
Ideal Tool and Die Property
3021 and 3029 Bank Street, Charlotte, NC
Groundwater Analytical Data Summary
Sample(s) collected: 5/2/2017
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APPENDIX A
Subsurface Investigation Permit
SIP Form – revised 2/15/11
Mecklenburg County Health Department Groundwater & Wastewater Services 700 N. Tryon St., Suite 211 Charlotte, NC 28202
Phone: [phone] Fax: [phone] http://groundwater.charmeck.org
Permit Issuance Date: _______________
Permit Number: ____________________
SUBSURFACE INVESTIGATION PERMIT
I. Well Owner Information
Name: ___________________________________
Attn: _____________________________________
Phone #: _____________________
Address 1: ________________________________
Address 2: ________________________________
City: __________________________ State: _______ Zip: _____________
II. Agent Information (if applicable)

Name: ___________________________________
Attn: _____________________________________
Phone #: _____________________
Address 1: ________________________________
Address 2: ________________________________
City: __________________________ State: _______ Zip: _____________
III. Site Information

Site Name; ________________________________
Parcel ID Number: _____________________
Address: ________________________________
City: __________________________ State: _______ Zip: _____________

General Conditions of This Permit:
• This permit shall be VALID for a period not to exceed twelve (12) months from the date of issuance.
• This permit is VALID for the site specified aboveDQGmust be on-site during the course of the investigation
and made available to a Department representative upon request.
• A North Carolina Certified Well Contrator must perform any well contractor activities associated with this permit.
• All wells shall be constructed and abandoned to the standards of Chapter VI, Section V and Section VIof the Mecklenburg County Groundwater Well Regulations.
• All temporary wells, including those installed using Direct Push Technology, must be abandoned
to the standards of Chapter VI, Section VI of the Mecklenburg County Groundwater Well Regulations.
• Registration information for all wells must be submitted to the Department within thirty (30) days of well completion. If water samples are collected, it is recommended that the well NOT be registered until the
analytical results are received.

Agent
4/21/2017
70002425
LEH NC Bank, LLC
Nickolaus Matthias Lischerong
864-590-6478
310 Arlington Avenue
Suite 402
Charlotte NC 28203
HRP Associates, Inc.
Ty Hawkins
864-289-0311
1327 Miller Road
Sutie D
Greenville SC 29607
3021 & 3029 Bank Street
14505205
NC
Limited Phase II Environmental Site Assessment
3021 & 3029 Bank St, Charlotte, NC
H:\L\Lischerong Enterprises and Holdings\LIS2000.P2 - 3021 & 3029 Bank St., Charlotte P2\Report\Bank Street PII - Report.docx
APPENDIX B
SOIL BORING LOGS

Limited Phase II Environmental Site Assessment
3021 & 3029 Bank St, Charlotte, NC
H:\L\Lischerong Enterprises and Holdings\LIS2000.P2 - 3021 & 3029 Bank St., Charlotte P2\Report\Bank Street PII - Report.docx
APPENDIX C
FIELD DATA SHEETS/EQUIPMENT
CALIBRATION LOGS
Limited Phase II Environmental Site Assessment
3021 & 3029 Bank St, Charlotte, NC
H:\L\Lischerong Enterprises and Holdings\LIS2000.P2 - 3021 & 3029 Bank St., Charlotte P2\Report\Bank Street PII - Report.docx
APPENDIX D
LABORATORY ANALYTICAL REPORT
#=CL#
May 10, 2017
LIMS USE: FR - TY HAWKINS
LIMS OBJECT ID: 92339291
92339291
Project:
Pace Project No.:
RE:
Mr. Ty HawkinsHRP Associates, Inc.1327 Miller Rd. Suite DGreenville, SC 29607
BANK STREET
Dear Mr. Hawkins:
Enclosed are the analytical results for sample(s) received by the laboratory on May 03, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the mostcurrent, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager(704)875-9092
Enclosures
cc: EDD and Report, HRP Associates
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 86
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92339291
BANK STREET
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 86
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92339291
BANK STREET
Lab ID Sample ID Matrix Date Collected Date Received
92339291001 TMW-7 Water 05/02/17 15:40 05/03/17 10:45
92339291002 TMW-4 Water 05/02/17 15:25 05/03/17 10:45
92339291003 TMW-1 Water 05/02/17 13:59 05/03/17 10:45
92339291004 SB-1(17-18)Solid 05/02/17 09:50 05/03/17 10:45
92339291005 SB-3(14-15)Solid 05/02/17 10:55 05/03/17 10:45
92339291006 SB-4(5-6)Solid 05/02/17 11:50 05/03/17 10:45
92339291007 SB-6(14-15)Solid 05/02/17 12:30 05/03/17 10:45
92339291008 SB-7(3-5)Solid 05/02/17 13:15 05/03/17 10:45
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 86
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92339291
BANK STREET
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92339291001 TMW-7 EPA 8082 8 PASI-CHSK
EPA 6010 12 PASI-ASH1
EPA 7470 1 PASI-AKAL
EPA 8270 74 PASI-CRES
EPA 8260 63 PASI-CZDO
92339291002 TMW-4 EPA 8082 8 PASI-CHSK
EPA 6010 12 PASI-ASH1
EPA 7470 1 PASI-AKAL
EPA 8270 74 PASI-CRES
EPA 8260 63 PASI-CZDO
92339291003 TMW-1 EPA 8082 8 PASI-CHSK
EPA 6010 12 PASI-ASH1
EPA 7470 1 PASI-AKAL
EPA 8270 74 PASI-CRES
EPA 8260 63 PASI-CZDO
92339291004 SB-1(17-18)EPA 8082 8 PASI-CHSK
EPA 6010 12 PASI-ASH1
EPA 7471 1 PASI-AKAL
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CCLW
92339291005 SB-3(14-15)EPA 8082 8 PASI-CHSK
EPA 6010 12 PASI-ASH1
EPA 7471 1 PASI-AKAL
EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CCLW
92339291006 SB-4(5-6)EPA 8082 8 PASI-CHSK
EPA 6010 12 PASI-ASH1
EPA 7471 1 PASI-AKAL
EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CCLW
92339291007 SB-6(14-15)EPA 8082 8 PASI-CHSK
EPA 6010 12 PASI-ASH1
EPA 7471 1 PASI-AKAL
EPA 8270 74 PASI-CBPJ
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 86
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92339291
BANK STREET
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CCLW
92339291008 SB-7(3-5)EPA 8082 8 PASI-CHSK
EPA 6010 12 PASI-ASH1
EPA 7471 1 PASI-AKAL
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CCLW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 86
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339291
BANK STREET
Sample: TMW-7 Lab ID: 92339291001 Collected: 05/02/17 15:40 Received: 05/03/17 10:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 05/09/17 17:06 12674-11-205/09/17 09:000.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 05/09/17 17:06 11104-28-205/09/17 09:000.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 05/09/17 17:06 11141-16-505/09/17 09:000.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 05/09/17 17:06 53469-21-905/09/17 09:000.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 05/09/17 17:06 12672-29-605/09/17 09:000.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 05/09/17 17:06 11097-69-105/09/17 09:000.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 05/09/17 17:06 11096-82-505/09/17 09:000.50 0.50 1
Surrogates
Decachlorobiphenyl (S)60 %05/09/17 17:06 2051-24-305/09/17 09:0010-132 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 05/07/17 03:17 7440-36-005/04/17 14:405.0 3.9 1
Arsenic ND ug/L 05/07/17 03:17 7440-38-205/04/17 14:4010.0 5.0 1
Beryllium 0.63J ug/L 05/07/17 03:17 7440-41-705/04/17 14:401.0 0.50 1
Cadmium ND ug/L 05/07/17 03:17 7440-43-905/04/17 14:401.0 0.50 1
Chromium 5.8 ug/L 05/07/17 03:17 7440-47-305/04/17 14:405.0 2.5 1
Copper 28.6 ug/L 05/07/17 03:17 7440-50-805/04/17 14:405.0 2.5 1
Iron 4680 ug/L 05/07/17 03:17 7439-89-605/04/17 14:4050.0 25.0 1
Nickel 18.5 ug/L 05/07/17 03:17 7440-02-005/04/17 14:405.0 2.5 1
Selenium ND ug/L 05/07/17 03:17 7782-49-205/04/17 14:4010.0 5.0 1
Silver ND ug/L 05/07/17 03:17 7440-22-405/04/17 14:405.0 2.5 1
Thallium ND ug/L 05/07/17 03:17 7440-28-005/04/17 14:4010.0 5.0 1
Zinc 35.1 ug/L 05/07/17 03:17 7440-66-605/04/17 14:4010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 05/09/17 11:58 7439-97-605/05/17 02:350.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 05/10/17 09:31 83-32-905/09/17 14:0710.0 0.25 1
Acenaphthylene ND ug/L 05/10/17 09:31 208-96-805/09/17 14:0710.0 0.21 1
Aniline ND ug/L 05/10/17 09:31 62-53-305/09/17 14:0710.0 1.3 1
Anthracene ND ug/L 05/10/17 09:31 120-12-705/09/17 14:0710.0 0.14 1
Benzo(a)anthracene 0.86J ug/L 05/10/17 09:31 56-55-305/09/17 14:0710.0 0.33 1
Benzo(a)pyrene ND ug/L 05/10/17 09:31 50-32-805/09/17 14:0710.0 0.30 1
Benzo(b)fluoranthene ND ug/L 05/10/17 09:31 205-99-205/09/17 14:0710.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 05/10/17 09:31 191-24-205/09/17 14:0710.0 0.38 1
Benzo(k)fluoranthene ND ug/L 05/10/17 09:31 207-08-905/09/17 14:0710.0 0.43 1
Benzoic Acid ND ug/L 05/10/17 09:31 65-85-005/09/17 14:0750.0 11.1 1
Benzyl alcohol ND ug/L 05/10/17 09:31 100-51-605/09/17 14:0720.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 05/10/17 09:31 101-55-305/09/17 14:0710.0 1.3 1
Butylbenzylphthalate ND ug/L 05/10/17 09:31 85-68-705/09/17 14:0710.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 05/10/17 09:31 59-50-705/09/17 14:0720.0 4.2 1
4-Chloroaniline ND ug/L 05/10/17 09:31 106-47-805/09/17 14:0720.0 3.4 1
bis(2-Chloroethoxy)methane ND ug/L 05/10/17 09:31 111-91-105/09/17 14:0710.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 05/10/17 09:31 111-44-405/09/17 14:0710.0 1.5 1
2-Chloronaphthalene ND ug/L 05/10/17 09:31 91-58-705/09/17 14:0710.0 2.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 86
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339291
BANK STREET
Sample: TMW-7 Lab ID: 92339291001 Collected: 05/02/17 15:40 Received: 05/03/17 10:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Chlorophenol ND ug/L 05/10/17 09:31 95-57-805/09/17 14:0710.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 05/10/17 09:31 7005-72-305/09/17 14:0710.0 2.1 1
Chrysene 0.85J ug/L 05/10/17 09:31 218-01-905/09/17 14:0710.0 0.21 1
Dibenz(a,h)anthracene ND ug/L 05/10/17 09:31 53-70-305/09/17 14:0710.0 0.55 1
Dibenzofuran ND ug/L 05/10/17 09:31 132-64-905/09/17 14:0710.0 1.8 1
1,2-Dichlorobenzene ND ug/L 05/10/17 09:31 95-50-105/09/17 14:0710.0 1.2 1
1,3-Dichlorobenzene ND ug/L 05/10/17 09:31 541-73-105/09/17 14:0710.0 1.1 1
1,4-Dichlorobenzene ND ug/L 05/10/17 09:31 106-46-705/09/17 14:0710.0 1.2 1
3,3'-Dichlorobenzidine ND ug/L 05/10/17 09:31 91-94-105/09/17 14:0720.0 1.4 1
2,4-Dichlorophenol ND ug/L 05/10/17 09:31 120-83-205/09/17 14:0710.0 1.7 1
Diethylphthalate ND ug/L 05/10/17 09:31 84-66-205/09/17 14:0710.0 1.3 1
2,4-Dimethylphenol ND ug/L 05/10/17 09:31 105-67-905/09/17 14:0710.0 2.2 1
Dimethylphthalate ND ug/L 05/10/17 09:31 131-11-305/09/17 14:0710.0 1.5 1
Di-n-butylphthalate ND ug/L 05/10/17 09:31 84-74-205/09/17 14:0710.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 05/10/17 09:31 534-52-105/09/17 14:0720.0 1.7 1
2,4-Dinitrophenol ND ug/L 05/10/17 09:31 51-28-505/09/17 14:0750.0 6.5 1
2,4-Dinitrotoluene ND ug/L 05/10/17 09:31 121-14-205/09/17 14:0710.0 1.2 1
2,6-Dinitrotoluene ND ug/L 05/10/17 09:31 606-20-205/09/17 14:0710.0 1.7 1
Di-n-octylphthalate ND ug/L 05/10/17 09:31 117-84-005/09/17 14:0710.0 0.86 1
bis(2-Ethylhexyl)phthalate 1.1J ug/L 05/10/17 09:31 117-81-705/09/17 14:076.0 0.85 1
Fluoranthene ND ug/L 05/10/17 09:31 206-44-005/09/17 14:0710.0 0.21 1
Fluorene ND ug/L 05/10/17 09:31 86-73-705/09/17 14:0710.0 0.21 1
Hexachloro-1,3-butadiene ND ug/L 05/10/17 09:31 87-68-305/09/17 14:0710.0 1.8 1
Hexachlorobenzene ND ug/L 05/10/17 09:31 118-74-105/09/17 14:0710.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 05/10/17 09:31 77-47-405/09/17 14:0710.0 1.8 1
Hexachloroethane ND ug/L 05/10/17 09:31 67-72-105/09/17 14:0710.0 1.5 1
Indeno(1,2,3-cd)pyrene ND ug/L 05/10/17 09:31 193-39-505/09/17 14:0710.0 0.29 1
Isophorone ND ug/L 05/10/17 09:31 78-59-105/09/17 14:0710.0 1.8 1
1-Methylnaphthalene ND ug/L 05/10/17 09:31 90-12-005/09/17 14:0710.0 0.32 1
2-Methylnaphthalene ND ug/L 05/10/17 09:31 91-57-605/09/17 14:0710.0 0.28 1
2-Methylphenol(o-Cresol)ND ug/L 05/10/17 09:31 95-48-705/09/17 14:0710.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 05/10/17 09:31 15831-10-4 L105/09/17 14:0710.0 1.7 1
Naphthalene ND ug/L 05/10/17 09:31 91-20-305/09/17 14:0710.0 0.34 1
2-Nitroaniline ND ug/L 05/10/17 09:31 88-74-405/09/17 14:0750.0 2.8 1
3-Nitroaniline ND ug/L 05/10/17 09:31 99-09-205/09/17 14:0750.0 2.4 1
4-Nitroaniline ND ug/L 05/10/17 09:31 100-01-605/09/17 14:0720.0 2.5 1
Nitrobenzene ND ug/L 05/10/17 09:31 98-95-305/09/17 14:0710.0 1.7 1
2-Nitrophenol ND ug/L 05/10/17 09:31 88-75-505/09/17 14:0710.0 1.7 1
4-Nitrophenol ND ug/L 05/10/17 09:31 100-02-705/09/17 14:0750.0 5.8 1
N-Nitrosodimethylamine ND ug/L 05/10/17 09:31 62-75-905/09/17 14:0710.0 1.3 1
N-Nitroso-di-n-propylamine ND ug/L 05/10/17 09:31 621-64-705/09/17 14:0710.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 05/10/17 09:31 86-30-605/09/17 14:0710.0 1.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 05/10/17 09:31 108-60-105/09/17 14:0710.0 1.6 1
Pentachlorophenol ND ug/L 05/10/17 09:31 87-86-505/09/17 14:0725.0 2.3 1
Phenanthrene ND ug/L 05/10/17 09:31 85-01-805/09/17 14:0710.0 0.22 1
Phenol ND ug/L 05/10/17 09:31 108-95-205/09/17 14:0710.0 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 86
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339291
BANK STREET
Sample: TMW-7 Lab ID: 92339291001 Collected: 05/02/17 15:40 Received: 05/03/17 10:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Pyrene ND ug/L 05/10/17 09:31 129-00-005/09/17 14:0710.0 0.19 1
1,2,4-Trichlorobenzene ND ug/L 05/10/17 09:31 120-82-105/09/17 14:0710.0 1.9 1
2,4,5-Trichlorophenol ND ug/L 05/10/17 09:31 95-95-405/09/17 14:0710.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 05/10/17 09:31 88-06-205/09/17 14:0710.0 1.9 1
Surrogates
Nitrobenzene-d5 (S)50 %05/10/17 09:31 4165-60-005/09/17 14:0721-110 1
2-Fluorobiphenyl (S)53 %05/10/17 09:31 321-60-805/09/17 14:0727-110 1
Terphenyl-d14 (S)60 %05/10/17 09:31 1718-51-005/09/17 14:0731-107 1
Phenol-d6 (S)19 %05/10/17 09:31 13127-88-305/09/17 14:0710-110 1
2-Fluorophenol (S)26 %05/10/17 09:31 367-12-405/09/17 14:0712-110 1
2,4,6-Tribromophenol (S)65 %05/10/17 09:31 118-79-605/09/17 14:0727-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 05/06/17 09:27 67-64-125.0 10.0 1
Benzene ND ug/L 05/06/17 09:27 71-43-21.0 0.25 1
Bromobenzene ND ug/L 05/06/17 09:27 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 05/06/17 09:27 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 05/06/17 09:27 75-27-41.0 0.18 1
Bromoform ND ug/L 05/06/17 09:27 75-25-21.0 0.26 1
Bromomethane ND ug/L 05/06/17 09:27 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 05/06/17 09:27 78-93-35.0 0.96 1
Carbon tetrachloride 12.0 ug/L 05/06/17 09:27 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 05/06/17 09:27 108-90-71.0 0.23 1
Chloroethane ND ug/L 05/06/17 09:27 75-00-31.0 0.54 1
Chloroform 4.9 ug/L 05/06/17 09:27 67-66-31.0 0.14 1
Chloromethane ND ug/L 05/06/17 09:27 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 05/06/17 09:27 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 05/06/17 09:27 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 05/06/17 09:27 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 05/06/17 09:27 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/06/17 09:27 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/06/17 09:27 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/06/17 09:27 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 05/06/17 09:27 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 05/06/17 09:27 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 05/06/17 09:27 75-71-81.0 0.21 1
1,1-Dichloroethane 3.0 ug/L 05/06/17 09:27 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 05/06/17 09:27 107-06-21.0 0.24 1
1,1-Dichloroethene 1.3 ug/L 05/06/17 09:27 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 5.7 ug/L 05/06/17 09:27 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/06/17 09:27 156-60-51.0 0.49 1
1,2-Dichloropropane 1.3 ug/L 05/06/17 09:27 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 05/06/17 09:27 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 05/06/17 09:27 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 05/06/17 09:27 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 05/06/17 09:27 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 86
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339291
BANK STREET
Sample: TMW-7 Lab ID: 92339291001 Collected: 05/02/17 15:40 Received: 05/03/17 10:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
trans-1,3-Dichloropropene ND ug/L 05/06/17 09:27 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 05/06/17 09:27 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 05/06/17 09:27 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 05/06/17 09:27 87-68-31.0 0.71 1
2-Hexanone ND ug/L 05/06/17 09:27 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 05/06/17 09:27 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 05/06/17 09:27 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/06/17 09:27 108-10-15.0 0.33 1
Methyl-tert-butyl ether 2.0 ug/L 05/06/17 09:27 1634-04-41.0 0.21 1
Naphthalene ND ug/L 05/06/17 09:27 91-20-31.0 0.24 1
Styrene ND ug/L 05/06/17 09:27 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/06/17 09:27 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/06/17 09:27 79-34-51.0 0.40 1
Tetrachloroethene 8.5 ug/L 05/06/17 09:27 127-18-41.0 0.46 1
Toluene ND ug/L 05/06/17 09:27 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 05/06/17 09:27 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 05/06/17 09:27 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 05/06/17 09:27 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/06/17 09:27 79-00-51.0 0.29 1
Trichloroethene 9.3 ug/L 05/06/17 09:27 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/06/17 09:27 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/06/17 09:27 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/06/17 09:27 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 05/06/17 09:27 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/06/17 09:27 1330-20-71.0 0.66 1
m&p-Xylene ND ug/L 05/06/17 09:27 179601-23-12.0 0.66 1
o-Xylene ND ug/L 05/06/17 09:27 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)104 %05/06/17 09:27 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %05/06/17 09:27 17060-07-070-130 1
Toluene-d8 (S)107 %05/06/17 09:27 2037-26-570-130 1
Sample: TMW-4 Lab ID: 92339291002 Collected: 05/02/17 15:25 Received: 05/03/17 10:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 05/09/17 17:26 12674-11-205/09/17 09:000.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 05/09/17 17:26 11104-28-205/09/17 09:000.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 05/09/17 17:26 11141-16-505/09/17 09:000.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 05/09/17 17:26 53469-21-905/09/17 09:000.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 05/09/17 17:26 12672-29-605/09/17 09:000.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 05/09/17 17:26 11097-69-105/09/17 09:000.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 05/09/17 17:26 11096-82-505/09/17 09:000.50 0.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 86
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339291
BANK STREET
Sample: TMW-4 Lab ID: 92339291002 Collected: 05/02/17 15:25 Received: 05/03/17 10:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
Surrogates
Decachlorobiphenyl (S)29 %05/09/17 17:26 2051-24-305/09/17 09:0010-132 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 05/07/17 03:20 7440-36-005/04/17 14:405.0 3.9 1
Arsenic ND ug/L 05/07/17 03:20 7440-38-205/04/17 14:4010.0 5.0 1
Beryllium ND ug/L 05/07/17 03:20 7440-41-705/04/17 14:401.0 0.50 1
Cadmium ND ug/L 05/07/17 03:20 7440-43-905/04/17 14:401.0 0.50 1
Chromium 12.8 ug/L 05/07/17 03:20 7440-47-305/04/17 14:405.0 2.5 1
Copper 13.8 ug/L 05/07/17 03:20 7440-50-805/04/17 14:405.0 2.5 1
Iron 5450 ug/L 05/07/17 03:20 7439-89-605/04/17 14:4050.0 25.0 1
Nickel 11.1 ug/L 05/07/17 03:20 7440-02-005/04/17 14:405.0 2.5 1
Selenium ND ug/L 05/07/17 03:20 7782-49-205/04/17 14:4010.0 5.0 1
Silver ND ug/L 05/07/17 03:20 7440-22-405/04/17 14:405.0 2.5 1
Thallium ND ug/L 05/07/17 03:20 7440-28-005/04/17 14:4010.0 5.0 1
Zinc 9.8J ug/L 05/07/17 03:20 7440-66-605/04/17 14:4010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 05/09/17 12:00 7439-97-605/05/17 02:350.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 05/10/17 10:00 83-32-905/09/17 14:0710.0 0.25 1
Acenaphthylene ND ug/L 05/10/17 10:00 208-96-805/09/17 14:0710.0 0.21 1
Aniline ND ug/L 05/10/17 10:00 62-53-305/09/17 14:0710.0 1.3 1
Anthracene ND ug/L 05/10/17 10:00 120-12-705/09/17 14:0710.0 0.14 1
Benzo(a)anthracene ND ug/L 05/10/17 10:00 56-55-305/09/17 14:0710.0 0.33 1
Benzo(a)pyrene ND ug/L 05/10/17 10:00 50-32-805/09/17 14:0710.0 0.30 1
Benzo(b)fluoranthene ND ug/L 05/10/17 10:00 205-99-205/09/17 14:0710.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 05/10/17 10:00 191-24-205/09/17 14:0710.0 0.38 1
Benzo(k)fluoranthene ND ug/L 05/10/17 10:00 207-08-905/09/17 14:0710.0 0.43 1
Benzoic Acid ND ug/L 05/10/17 10:00 65-85-005/09/17 14:0750.0 11.1 1
Benzyl alcohol ND ug/L 05/10/17 10:00 100-51-605/09/17 14:0720.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 05/10/17 10:00 101-55-305/09/17 14:0710.0 1.3 1
Butylbenzylphthalate ND ug/L 05/10/17 10:00 85-68-705/09/17 14:0710.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 05/10/17 10:00 59-50-705/09/17 14:0720.0 4.2 1
4-Chloroaniline ND ug/L 05/10/17 10:00 106-47-805/09/17 14:0720.0 3.4 1
bis(2-Chloroethoxy)methane ND ug/L 05/10/17 10:00 111-91-105/09/17 14:0710.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 05/10/17 10:00 111-44-405/09/17 14:0710.0 1.5 1
2-Chloronaphthalene ND ug/L 05/10/17 10:00 91-58-705/09/17 14:0710.0 2.2 1
2-Chlorophenol ND ug/L 05/10/17 10:00 95-57-805/09/17 14:0710.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 05/10/17 10:00 7005-72-305/09/17 14:0710.0 2.1 1
Chrysene ND ug/L 05/10/17 10:00 218-01-905/09/17 14:0710.0 0.21 1
Dibenz(a,h)anthracene ND ug/L 05/10/17 10:00 53-70-305/09/17 14:0710.0 0.55 1
Dibenzofuran ND ug/L 05/10/17 10:00 132-64-905/09/17 14:0710.0 1.8 1
1,2-Dichlorobenzene ND ug/L 05/10/17 10:00 95-50-105/09/17 14:0710.0 1.2 1
1,3-Dichlorobenzene ND ug/L 05/10/17 10:00 541-73-105/09/17 14:0710.0 1.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 86
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339291
BANK STREET
Sample: TMW-4 Lab ID: 92339291002 Collected: 05/02/17 15:25 Received: 05/03/17 10:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
1,4-Dichlorobenzene ND ug/L 05/10/17 10:00 106-46-705/09/17 14:0710.0 1.2 1
3,3'-Dichlorobenzidine ND ug/L 05/10/17 10:00 91-94-105/09/17 14:0720.0 1.4 1
2,4-Dichlorophenol ND ug/L 05/10/17 10:00 120-83-205/09/17 14:0710.0 1.7 1
Diethylphthalate ND ug/L 05/10/17 10:00 84-66-205/09/17 14:0710.0 1.3 1
2,4-Dimethylphenol ND ug/L 05/10/17 10:00 105-67-905/09/17 14:0710.0 2.2 1
Dimethylphthalate ND ug/L 05/10/17 10:00 131-11-305/09/17 14:0710.0 1.5 1
Di-n-butylphthalate ND ug/L 05/10/17 10:00 84-74-205/09/17 14:0710.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 05/10/17 10:00 534-52-105/09/17 14:0720.0 1.7 1
2,4-Dinitrophenol ND ug/L 05/10/17 10:00 51-28-505/09/17 14:0750.0 6.5 1
2,4-Dinitrotoluene ND ug/L 05/10/17 10:00 121-14-205/09/17 14:0710.0 1.2 1
2,6-Dinitrotoluene ND ug/L 05/10/17 10:00 606-20-205/09/17 14:0710.0 1.7 1
Di-n-octylphthalate ND ug/L 05/10/17 10:00 117-84-005/09/17 14:0710.0 0.86 1
bis(2-Ethylhexyl)phthalate ND ug/L 05/10/17 10:00 117-81-705/09/17 14:076.0 0.85 1
Fluoranthene ND ug/L 05/10/17 10:00 206-44-005/09/17 14:0710.0 0.21 1
Fluorene ND ug/L 05/10/17 10:00 86-73-705/09/17 14:0710.0 0.21 1
Hexachloro-1,3-butadiene ND ug/L 05/10/17 10:00 87-68-305/09/17 14:0710.0 1.8 1
Hexachlorobenzene ND ug/L 05/10/17 10:00 118-74-105/09/17 14:0710.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 05/10/17 10:00 77-47-405/09/17 14:0710.0 1.8 1
Hexachloroethane ND ug/L 05/10/17 10:00 67-72-105/09/17 14:0710.0 1.5 1
Indeno(1,2,3-cd)pyrene ND ug/L 05/10/17 10:00 193-39-505/09/17 14:0710.0 0.29 1
Isophorone ND ug/L 05/10/17 10:00 78-59-105/09/17 14:0710.0 1.8 1
1-Methylnaphthalene ND ug/L 05/10/17 10:00 90-12-005/09/17 14:0710.0 0.32 1
2-Methylnaphthalene ND ug/L 05/10/17 10:00 91-57-605/09/17 14:0710.0 0.28 1
2-Methylphenol(o-Cresol)ND ug/L 05/10/17 10:00 95-48-705/09/17 14:0710.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 05/10/17 10:00 15831-10-4 L105/09/17 14:0710.0 1.7 1
Naphthalene ND ug/L 05/10/17 10:00 91-20-305/09/17 14:0710.0 0.34 1
2-Nitroaniline ND ug/L 05/10/17 10:00 88-74-405/09/17 14:0750.0 2.8 1
3-Nitroaniline ND ug/L 05/10/17 10:00 99-09-205/09/17 14:0750.0 2.4 1
4-Nitroaniline ND ug/L 05/10/17 10:00 100-01-605/09/17 14:0720.0 2.5 1
Nitrobenzene ND ug/L 05/10/17 10:00 98-95-305/09/17 14:0710.0 1.7 1
2-Nitrophenol ND ug/L 05/10/17 10:00 88-75-505/09/17 14:0710.0 1.7 1
4-Nitrophenol ND ug/L 05/10/17 10:00 100-02-705/09/17 14:0750.0 5.8 1
N-Nitrosodimethylamine ND ug/L 05/10/17 10:00 62-75-905/09/17 14:0710.0 1.3 1
N-Nitroso-di-n-propylamine ND ug/L 05/10/17 10:00 621-64-705/09/17 14:0710.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 05/10/17 10:00 86-30-605/09/17 14:0710.0 1.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 05/10/17 10:00 108-60-105/09/17 14:0710.0 1.6 1
Pentachlorophenol ND ug/L 05/10/17 10:00 87-86-505/09/17 14:0725.0 2.3 1
Phenanthrene ND ug/L 05/10/17 10:00 85-01-805/09/17 14:0710.0 0.22 1
Phenol ND ug/L 05/10/17 10:00 108-95-205/09/17 14:0710.0 1.7 1
Pyrene ND ug/L 05/10/17 10:00 129-00-005/09/17 14:0710.0 0.19 1
1,2,4-Trichlorobenzene ND ug/L 05/10/17 10:00 120-82-105/09/17 14:0710.0 1.9 1
2,4,5-Trichlorophenol ND ug/L 05/10/17 10:00 95-95-405/09/17 14:0710.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 05/10/17 10:00 88-06-205/09/17 14:0710.0 1.9 1
SurrogatesNitrobenzene-d5 (S)27 %05/10/17 10:00 4165-60-005/09/17 14:0721-110 1
2-Fluorobiphenyl (S)27 %05/10/17 10:00 321-60-805/09/17 14:0727-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 86
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339291
BANK STREET
Sample: TMW-4 Lab ID: 92339291002 Collected: 05/02/17 15:25 Received: 05/03/17 10:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Surrogates
Terphenyl-d14 (S)44 %05/10/17 10:00 1718-51-005/09/17 14:0731-107 1
Phenol-d6 (S)12 %05/10/17 10:00 13127-88-305/09/17 14:0710-110 1
2-Fluorophenol (S)17 %05/10/17 10:00 367-12-405/09/17 14:0712-110 1
2,4,6-Tribromophenol (S)44 %05/10/17 10:00 118-79-605/09/17 14:0727-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 05/07/17 06:11 67-64-125.0 10.0 1
Benzene ND ug/L 05/07/17 06:11 71-43-21.0 0.25 1
Bromobenzene ND ug/L 05/07/17 06:11 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 05/07/17 06:11 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 05/07/17 06:11 75-27-41.0 0.18 1
Bromoform ND ug/L 05/07/17 06:11 75-25-21.0 0.26 1
Bromomethane ND ug/L 05/07/17 06:11 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 05/07/17 06:11 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 05/07/17 06:11 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 05/07/17 06:11 108-90-71.0 0.23 1
Chloroethane ND ug/L 05/07/17 06:11 75-00-31.0 0.54 1
Chloroform 3.6 ug/L 05/07/17 06:11 67-66-31.0 0.14 1
Chloromethane ND ug/L 05/07/17 06:11 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 05/07/17 06:11 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 05/07/17 06:11 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 05/07/17 06:11 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 05/07/17 06:11 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/07/17 06:11 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/07/17 06:11 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/07/17 06:11 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 05/07/17 06:11 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 05/07/17 06:11 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 05/07/17 06:11 75-71-81.0 0.21 1
1,1-Dichloroethane 2.1 ug/L 05/07/17 06:11 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 05/07/17 06:11 107-06-21.0 0.24 1
1,1-Dichloroethene 0.75J ug/L 05/07/17 06:11 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 4.6 ug/L 05/07/17 06:11 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/07/17 06:11 156-60-51.0 0.49 1
1,2-Dichloropropane 1.0 ug/L 05/07/17 06:11 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 05/07/17 06:11 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 05/07/17 06:11 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 05/07/17 06:11 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 05/07/17 06:11 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/07/17 06:11 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 05/07/17 06:11 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 05/07/17 06:11 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 05/07/17 06:11 87-68-31.0 0.71 1
2-Hexanone ND ug/L 05/07/17 06:11 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 05/07/17 06:11 99-87-61.0 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 86
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339291
BANK STREET
Sample: TMW-4 Lab ID: 92339291002 Collected: 05/02/17 15:25 Received: 05/03/17 10:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
Methylene Chloride ND ug/L 05/07/17 06:11 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/07/17 06:11 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 05/07/17 06:11 1634-04-41.0 0.21 1
Naphthalene ND ug/L 05/07/17 06:11 91-20-31.0 0.24 1
Styrene ND ug/L 05/07/17 06:11 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/07/17 06:11 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/07/17 06:11 79-34-51.0 0.40 1
Tetrachloroethene 5.3 ug/L 05/07/17 06:11 127-18-41.0 0.46 1
Toluene ND ug/L 05/07/17 06:11 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 05/07/17 06:11 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 05/07/17 06:11 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 05/07/17 06:11 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/07/17 06:11 79-00-51.0 0.29 1
Trichloroethene 13.0 ug/L 05/07/17 06:11 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/07/17 06:11 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/07/17 06:11 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/07/17 06:11 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 05/07/17 06:11 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/07/17 06:11 1330-20-71.0 0.66 1
m&p-Xylene ND ug/L 05/07/17 06:11 179601-23-12.0 0.66 1
o-Xylene ND ug/L 05/07/17 06:11 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)102 %05/07/17 06:11 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %05/07/17 06:11 17060-07-070-130 1
Toluene-d8 (S)107 %05/07/17 06:11 2037-26-570-130 1
Sample: TMW-1 Lab ID: 92339291003 Collected: 05/02/17 13:59 Received: 05/03/17 10:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 05/09/17 17:46 12674-11-205/09/17 09:000.50 0.50 1
PCB-1221 (Aroclor 1221)ND ug/L 05/09/17 17:46 11104-28-205/09/17 09:000.50 0.50 1
PCB-1232 (Aroclor 1232)ND ug/L 05/09/17 17:46 11141-16-505/09/17 09:000.50 0.50 1
PCB-1242 (Aroclor 1242)ND ug/L 05/09/17 17:46 53469-21-905/09/17 09:000.50 0.50 1
PCB-1248 (Aroclor 1248)ND ug/L 05/09/17 17:46 12672-29-605/09/17 09:000.50 0.50 1
PCB-1254 (Aroclor 1254)ND ug/L 05/09/17 17:46 11097-69-105/09/17 09:000.50 0.50 1
PCB-1260 (Aroclor 1260)ND ug/L 05/09/17 17:46 11096-82-505/09/17 09:000.50 0.50 1
Surrogates
Decachlorobiphenyl (S)31 %05/09/17 17:46 2051-24-305/09/17 09:0010-132 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Antimony ND ug/L 05/09/17 14:39 7440-36-005/04/17 14:405.0 3.9 1
Arsenic ND ug/L 05/09/17 14:39 7440-38-205/04/17 14:4010.0 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 86
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339291
BANK STREET
Sample: TMW-1 Lab ID: 92339291003 Collected: 05/02/17 13:59 Received: 05/03/17 10:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 MET ICP
Beryllium ND ug/L 05/09/17 14:39 7440-41-705/04/17 14:401.0 0.50 1
Cadmium ND ug/L 05/09/17 14:39 7440-43-905/04/17 14:401.0 0.50 1
Chromium ND ug/L 05/09/17 14:39 7440-47-305/04/17 14:405.0 2.5 1
Copper 8.3 ug/L 05/09/17 14:39 7440-50-805/04/17 14:405.0 2.5 1
Iron 2840 ug/L 05/09/17 14:39 7439-89-605/04/17 14:4050.0 25.0 1
Nickel 2.5J ug/L 05/09/17 14:39 7440-02-005/04/17 14:405.0 2.5 1
Selenium ND ug/L 05/09/17 14:39 7782-49-205/04/17 14:4010.0 5.0 1
Silver ND ug/L 05/09/17 14:39 7440-22-405/04/17 14:405.0 2.5 1
Thallium ND ug/L 05/09/17 14:39 7440-28-005/04/17 14:4010.0 5.0 1
Zinc 8.1J ug/L 05/09/17 14:39 7440-66-605/04/17 14:4010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 05/05/17 11:58 7439-97-605/05/17 02:350.20 0.10 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 05/10/17 10:29 83-32-905/09/17 14:0710.0 0.25 1
Acenaphthylene ND ug/L 05/10/17 10:29 208-96-805/09/17 14:0710.0 0.21 1
Aniline ND ug/L 05/10/17 10:29 62-53-305/09/17 14:0710.0 1.3 1
Anthracene ND ug/L 05/10/17 10:29 120-12-705/09/17 14:0710.0 0.14 1
Benzo(a)anthracene ND ug/L 05/10/17 10:29 56-55-305/09/17 14:0710.0 0.33 1
Benzo(a)pyrene ND ug/L 05/10/17 10:29 50-32-805/09/17 14:0710.0 0.30 1
Benzo(b)fluoranthene ND ug/L 05/10/17 10:29 205-99-205/09/17 14:0710.0 0.28 1
Benzo(g,h,i)perylene ND ug/L 05/10/17 10:29 191-24-205/09/17 14:0710.0 0.38 1
Benzo(k)fluoranthene ND ug/L 05/10/17 10:29 207-08-905/09/17 14:0710.0 0.43 1
Benzoic Acid ND ug/L 05/10/17 10:29 65-85-005/09/17 14:0750.0 11.1 1
Benzyl alcohol ND ug/L 05/10/17 10:29 100-51-605/09/17 14:0720.0 3.4 1
4-Bromophenylphenyl ether ND ug/L 05/10/17 10:29 101-55-305/09/17 14:0710.0 1.3 1
Butylbenzylphthalate ND ug/L 05/10/17 10:29 85-68-705/09/17 14:0710.0 0.75 1
4-Chloro-3-methylphenol ND ug/L 05/10/17 10:29 59-50-705/09/17 14:0720.0 4.2 1
4-Chloroaniline ND ug/L 05/10/17 10:29 106-47-805/09/17 14:0720.0 3.4 1
bis(2-Chloroethoxy)methane ND ug/L 05/10/17 10:29 111-91-105/09/17 14:0710.0 1.7 1
bis(2-Chloroethyl) ether ND ug/L 05/10/17 10:29 111-44-405/09/17 14:0710.0 1.5 1
2-Chloronaphthalene ND ug/L 05/10/17 10:29 91-58-705/09/17 14:0710.0 2.2 1
2-Chlorophenol ND ug/L 05/10/17 10:29 95-57-805/09/17 14:0710.0 1.5 1
4-Chlorophenylphenyl ether ND ug/L 05/10/17 10:29 7005-72-305/09/17 14:0710.0 2.1 1
Chrysene ND ug/L 05/10/17 10:29 218-01-905/09/17 14:0710.0 0.21 1
Dibenz(a,h)anthracene ND ug/L 05/10/17 10:29 53-70-305/09/17 14:0710.0 0.55 1
Dibenzofuran ND ug/L 05/10/17 10:29 132-64-905/09/17 14:0710.0 1.8 1
1,2-Dichlorobenzene ND ug/L 05/10/17 10:29 95-50-105/09/17 14:0710.0 1.2 1
1,3-Dichlorobenzene ND ug/L 05/10/17 10:29 541-73-105/09/17 14:0710.0 1.1 1
1,4-Dichlorobenzene ND ug/L 05/10/17 10:29 106-46-705/09/17 14:0710.0 1.2 1
3,3'-Dichlorobenzidine ND ug/L 05/10/17 10:29 91-94-105/09/17 14:0720.0 1.4 1
2,4-Dichlorophenol ND ug/L 05/10/17 10:29 120-83-205/09/17 14:0710.0 1.7 1
Diethylphthalate 5.2J ug/L 05/10/17 10:29 84-66-205/09/17 14:0710.0 1.3 1
2,4-Dimethylphenol ND ug/L 05/10/17 10:29 105-67-905/09/17 14:0710.0 2.2 1
Dimethylphthalate ND ug/L 05/10/17 10:29 131-11-305/09/17 14:0710.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 86
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339291
BANK STREET
Sample: TMW-1 Lab ID: 92339291003 Collected: 05/02/17 13:59 Received: 05/03/17 10:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Di-n-butylphthalate ND ug/L 05/10/17 10:29 84-74-205/09/17 14:0710.0 1.1 1
4,6-Dinitro-2-methylphenol ND ug/L 05/10/17 10:29 534-52-105/09/17 14:0720.0 1.7 1
2,4-Dinitrophenol ND ug/L 05/10/17 10:29 51-28-505/09/17 14:0750.0 6.5 1
2,4-Dinitrotoluene ND ug/L 05/10/17 10:29 121-14-205/09/17 14:0710.0 1.2 1
2,6-Dinitrotoluene ND ug/L 05/10/17 10:29 606-20-205/09/17 14:0710.0 1.7 1
Di-n-octylphthalate ND ug/L 05/10/17 10:29 117-84-005/09/17 14:0710.0 0.86 1
bis(2-Ethylhexyl)phthalate ND ug/L 05/10/17 10:29 117-81-705/09/17 14:076.0 0.85 1
Fluoranthene ND ug/L 05/10/17 10:29 206-44-005/09/17 14:0710.0 0.21 1
Fluorene ND ug/L 05/10/17 10:29 86-73-705/09/17 14:0710.0 0.21 1
Hexachloro-1,3-butadiene ND ug/L 05/10/17 10:29 87-68-305/09/17 14:0710.0 1.8 1
Hexachlorobenzene ND ug/L 05/10/17 10:29 118-74-105/09/17 14:0710.0 1.1 1
Hexachlorocyclopentadiene ND ug/L 05/10/17 10:29 77-47-405/09/17 14:0710.0 1.8 1
Hexachloroethane ND ug/L 05/10/17 10:29 67-72-105/09/17 14:0710.0 1.5 1
Indeno(1,2,3-cd)pyrene ND ug/L 05/10/17 10:29 193-39-505/09/17 14:0710.0 0.29 1
Isophorone ND ug/L 05/10/17 10:29 78-59-105/09/17 14:0710.0 1.8 1
1-Methylnaphthalene ND ug/L 05/10/17 10:29 90-12-005/09/17 14:0710.0 0.32 1
2-Methylnaphthalene ND ug/L 05/10/17 10:29 91-57-605/09/17 14:0710.0 0.28 1
2-Methylphenol(o-Cresol)ND ug/L 05/10/17 10:29 95-48-705/09/17 14:0710.0 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 05/10/17 10:29 15831-10-4 L105/09/17 14:0710.0 1.7 1
Naphthalene ND ug/L 05/10/17 10:29 91-20-305/09/17 14:0710.0 0.34 1
2-Nitroaniline ND ug/L 05/10/17 10:29 88-74-405/09/17 14:0750.0 2.8 1
3-Nitroaniline ND ug/L 05/10/17 10:29 99-09-205/09/17 14:0750.0 2.4 1
4-Nitroaniline ND ug/L 05/10/17 10:29 100-01-605/09/17 14:0720.0 2.5 1
Nitrobenzene ND ug/L 05/10/17 10:29 98-95-305/09/17 14:0710.0 1.7 1
2-Nitrophenol ND ug/L 05/10/17 10:29 88-75-505/09/17 14:0710.0 1.7 1
4-Nitrophenol ND ug/L 05/10/17 10:29 100-02-705/09/17 14:0750.0 5.8 1
N-Nitrosodimethylamine ND ug/L 05/10/17 10:29 62-75-905/09/17 14:0710.0 1.3 1
N-Nitroso-di-n-propylamine ND ug/L 05/10/17 10:29 621-64-705/09/17 14:0710.0 2.1 1
N-Nitrosodiphenylamine ND ug/L 05/10/17 10:29 86-30-605/09/17 14:0710.0 1.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 05/10/17 10:29 108-60-105/09/17 14:0710.0 1.6 1
Pentachlorophenol ND ug/L 05/10/17 10:29 87-86-505/09/17 14:0725.0 2.3 1
Phenanthrene ND ug/L 05/10/17 10:29 85-01-805/09/17 14:0710.0 0.22 1
Phenol ND ug/L 05/10/17 10:29 108-95-205/09/17 14:0710.0 1.7 1
Pyrene ND ug/L 05/10/17 10:29 129-00-005/09/17 14:0710.0 0.19 1
1,2,4-Trichlorobenzene ND ug/L 05/10/17 10:29 120-82-105/09/17 14:0710.0 1.9 1
2,4,5-Trichlorophenol ND ug/L 05/10/17 10:29 95-95-405/09/17 14:0710.0 2.2 1
2,4,6-Trichlorophenol ND ug/L 05/10/17 10:29 88-06-205/09/17 14:0710.0 1.9 1
Surrogates
Nitrobenzene-d5 (S)44 %05/10/17 10:29 4165-60-005/09/17 14:0721-110 1
2-Fluorobiphenyl (S)47 %05/10/17 10:29 321-60-805/09/17 14:0727-110 1
Terphenyl-d14 (S)48 %05/10/17 10:29 1718-51-005/09/17 14:0731-107 1
Phenol-d6 (S)18 %05/10/17 10:29 13127-88-305/09/17 14:0710-110 1
2-Fluorophenol (S)25 %05/10/17 10:29 367-12-405/09/17 14:0712-110 1
2,4,6-Tribromophenol (S)74 %05/10/17 10:29 118-79-605/09/17 14:0727-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 86
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339291
BANK STREET
Sample: TMW-1 Lab ID: 92339291003 Collected: 05/02/17 13:59 Received: 05/03/17 10:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 05/07/17 06:29 67-64-125.0 10.0 1
Benzene ND ug/L 05/07/17 06:29 71-43-21.0 0.25 1
Bromobenzene ND ug/L 05/07/17 06:29 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 05/07/17 06:29 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 05/07/17 06:29 75-27-41.0 0.18 1
Bromoform ND ug/L 05/07/17 06:29 75-25-21.0 0.26 1
Bromomethane ND ug/L 05/07/17 06:29 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 05/07/17 06:29 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 05/07/17 06:29 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 05/07/17 06:29 108-90-71.0 0.23 1
Chloroethane ND ug/L 05/07/17 06:29 75-00-31.0 0.54 1
Chloroform 0.90J ug/L 05/07/17 06:29 67-66-31.0 0.14 1
Chloromethane ND ug/L 05/07/17 06:29 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 05/07/17 06:29 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 05/07/17 06:29 106-43-41.0 0.31 1
1,2-Dibromo-3-chloropropane ND ug/L 05/07/17 06:29 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 05/07/17 06:29 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 05/07/17 06:29 106-93-41.0 0.27 1
Dibromomethane ND ug/L 05/07/17 06:29 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 05/07/17 06:29 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 05/07/17 06:29 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 05/07/17 06:29 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 05/07/17 06:29 75-71-81.0 0.21 1
1,1-Dichloroethane 1.1 ug/L 05/07/17 06:29 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 05/07/17 06:29 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 05/07/17 06:29 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 2.2 ug/L 05/07/17 06:29 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 05/07/17 06:29 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 05/07/17 06:29 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 05/07/17 06:29 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 05/07/17 06:29 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 05/07/17 06:29 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 05/07/17 06:29 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 05/07/17 06:29 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 05/07/17 06:29 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 05/07/17 06:29 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 05/07/17 06:29 87-68-31.0 0.71 1
2-Hexanone ND ug/L 05/07/17 06:29 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 05/07/17 06:29 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 05/07/17 06:29 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/07/17 06:29 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 05/07/17 06:29 1634-04-41.0 0.21 1
Naphthalene ND ug/L 05/07/17 06:29 91-20-31.0 0.24 1
Styrene ND ug/L 05/07/17 06:29 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 05/07/17 06:29 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 05/07/17 06:29 79-34-51.0 0.40 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 86
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339291
BANK STREET
Sample: TMW-1 Lab ID: 92339291003 Collected: 05/02/17 13:59 Received: 05/03/17 10:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
Tetrachloroethene 3.5 ug/L 05/07/17 06:29 127-18-41.0 0.46 1
Toluene ND ug/L 05/07/17 06:29 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 05/07/17 06:29 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 05/07/17 06:29 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 05/07/17 06:29 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 05/07/17 06:29 79-00-51.0 0.29 1
Trichloroethene 5.6 ug/L 05/07/17 06:29 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 05/07/17 06:29 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 05/07/17 06:29 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 05/07/17 06:29 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 05/07/17 06:29 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 05/07/17 06:29 1330-20-71.0 0.66 1
m&p-Xylene ND ug/L 05/07/17 06:29 179601-23-12.0 0.66 1
o-Xylene ND ug/L 05/07/17 06:29 95-47-61.0 0.23 1
Surrogates
4-Bromofluorobenzene (S)103 %05/07/17 06:29 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %05/07/17 06:29 17060-07-070-130 1
Toluene-d8 (S)109 %05/07/17 06:29 2037-26-570-130 1
Sample: SB-1(17-18)Lab ID: 92339291004 Collected: 05/02/17 09:50 Received: 05/03/17 10:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8082 Preparation Method: EPA 35468082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/kg 05/05/17 00:38 12674-11-205/04/17 06:1838.5 17.5 1
PCB-1221 (Aroclor 1221)ND ug/kg 05/05/17 00:38 11104-28-205/04/17 06:1838.5 17.5 1
PCB-1232 (Aroclor 1232)ND ug/kg 05/05/17 00:38 11141-16-505/04/17 06:1838.5 17.5 1
PCB-1242 (Aroclor 1242)ND ug/kg 05/05/17 00:38 53469-21-905/04/17 06:1838.5 17.5 1
PCB-1248 (Aroclor 1248)ND ug/kg 05/05/17 00:38 12672-29-605/04/17 06:1838.5 17.5 1
PCB-1254 (Aroclor 1254)ND ug/kg 05/05/17 00:38 11097-69-105/04/17 06:1838.5 17.5 1
PCB-1260 (Aroclor 1260)ND ug/kg 05/05/17 00:38 11096-82-505/04/17 06:1838.5 17.5 1
Surrogates
Decachlorobiphenyl (S)67 %05/05/17 00:38 2051-24-305/04/17 06:1821-132 1
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Antimony ND mg/kg 05/09/17 21:32 7440-36-005/05/17 10:050.47 0.37 1
Arsenic ND mg/kg 05/09/17 21:32 7440-38-205/05/17 10:050.94 0.47 1
Beryllium 0.32 mg/kg 05/09/17 21:32 7440-41-705/05/17 10:050.094 0.047 1
Cadmium ND mg/kg 05/09/17 21:32 7440-43-905/05/17 10:050.094 0.047 1
Chromium 6.8 mg/kg 05/09/17 21:32 7440-47-305/05/17 10:050.47 0.24 1
Copper 16.8 mg/kg 05/09/17 21:32 7440-50-805/05/17 10:050.47 0.24 1
Lead 2.0 mg/kg 05/09/17 21:32 7439-92-105/05/17 10:050.47 0.24 1
Nickel 6.5 mg/kg 05/09/17 21:32 7440-02-005/05/17 10:050.47 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 86
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339291
BANK STREET
Sample: SB-1(17-18)Lab ID: 92339291004 Collected: 05/02/17 09:50 Received: 05/03/17 10:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Selenium 1.3 mg/kg 05/09/17 21:32 7782-49-205/05/17 10:050.94 0.47 1
Silver ND mg/kg 05/09/17 21:32 7440-22-405/05/17 10:050.47 0.24 1
Thallium ND mg/kg 05/09/17 21:32 7440-28-005/05/17 10:050.94 0.47 1
Zinc 61.0 mg/kg 05/09/17 21:32 7440-66-605/05/17 10:050.94 0.47 1
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury ND mg/kg 05/10/17 11:17 7439-97-605/10/17 04:000.0054 0.0027 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 05/05/17 15:47 83-32-905/04/17 22:23385 88.7 1
Acenaphthylene ND ug/kg 05/05/17 15:47 208-96-805/04/17 22:23385 91.0 1
Aniline ND ug/kg 05/05/17 15:47 62-53-305/04/17 22:23385 104 1
Anthracene ND ug/kg 05/05/17 15:47 120-12-705/04/17 22:23385 86.3 1
Benzo(a)anthracene ND ug/kg 05/05/17 15:47 56-55-305/04/17 22:23385 71.2 1
Benzo(a)pyrene ND ug/kg 05/05/17 15:47 50-32-805/04/17 22:23385 73.5 1
Benzo(b)fluoranthene ND ug/kg 05/05/17 15:47 205-99-205/04/17 22:23385 66.5 1
Benzo(g,h,i)perylene ND ug/kg 05/05/17 15:47 191-24-205/04/17 22:23385 98.0 1
Benzo(k)fluoranthene ND ug/kg 05/05/17 15:47 207-08-905/04/17 22:23385 75.8 1
Benzoic Acid ND ug/kg 05/05/17 15:47 65-85-005/04/17 22:231920 70.0 1
Benzyl alcohol ND ug/kg 05/05/17 15:47 100-51-605/04/17 22:23770 77.0 1
4-Bromophenylphenyl ether ND ug/kg 05/05/17 15:47 101-55-305/04/17 22:23385 70.0 1
Butylbenzylphthalate ND ug/kg 05/05/17 15:47 85-68-705/04/17 22:23385 81.7 1
4-Chloro-3-methylphenol ND ug/kg 05/05/17 15:47 59-50-705/04/17 22:23770 79.3 1
4-Chloroaniline ND ug/kg 05/05/17 15:47 106-47-805/04/17 22:231920 107 1
bis(2-Chloroethoxy)methane ND ug/kg 05/05/17 15:47 111-91-105/04/17 22:23385 89.8 1
bis(2-Chloroethyl) ether ND ug/kg 05/05/17 15:47 111-44-405/04/17 22:23385 98.0 1
2-Chloronaphthalene ND ug/kg 05/05/17 15:47 91-58-705/04/17 22:23385 75.8 1
2-Chlorophenol ND ug/kg 05/05/17 15:47 95-57-805/04/17 22:23385 105 1
4-Chlorophenylphenyl ether ND ug/kg 05/05/17 15:47 7005-72-305/04/17 22:23385 79.3 1
Chrysene ND ug/kg 05/05/17 15:47 218-01-905/04/17 22:23385 51.3 1
Dibenz(a,h)anthracene ND ug/kg 05/05/17 15:47 53-70-305/04/17 22:23385 81.7 1
Dibenzofuran ND ug/kg 05/05/17 15:47 132-64-905/04/17 22:23385 63.0 1
1,2-Dichlorobenzene ND ug/kg 05/05/17 15:47 95-50-105/04/17 22:23385 103 1
1,3-Dichlorobenzene ND ug/kg 05/05/17 15:47 541-73-1 L205/04/17 22:23385 87.5 1
1,4-Dichlorobenzene ND ug/kg 05/05/17 15:47 106-46-705/04/17 22:23385 108 1
3,3'-Dichlorobenzidine ND ug/kg 05/05/17 15:47 91-94-105/04/17 22:231920 84.0 1
2,4-Dichlorophenol ND ug/kg 05/05/17 15:47 120-83-205/04/17 22:23385 84.0 1
Diethylphthalate ND ug/kg 05/05/17 15:47 84-66-205/04/17 22:23385 59.5 1
2,4-Dimethylphenol ND ug/kg 05/05/17 15:47 105-67-905/04/17 22:23385 152 1
Dimethylphthalate ND ug/kg 05/05/17 15:47 131-11-305/04/17 22:23385 78.2 1
Di-n-butylphthalate ND ug/kg 05/05/17 15:47 84-74-205/04/17 22:23385 63.0 1
4,6-Dinitro-2-methylphenol ND ug/kg 05/05/17 15:47 534-52-105/04/17 22:23770 77.0 1
2,4-Dinitrophenol ND ug/kg 05/05/17 15:47 51-28-505/04/17 22:231920 63.0 1
2,4-Dinitrotoluene ND ug/kg 05/05/17 15:47 121-14-205/04/17 22:23385 72.3 1
2,6-Dinitrotoluene ND ug/kg 05/05/17 15:47 606-20-205/04/17 22:23385 80.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 86
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339291
BANK STREET
Sample: SB-1(17-18)Lab ID: 92339291004 Collected: 05/02/17 09:50 Received: 05/03/17 10:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Di-n-octylphthalate ND ug/kg 05/05/17 15:47 117-84-005/04/17 22:23385 80.5 1
bis(2-Ethylhexyl)phthalate ND ug/kg 05/05/17 15:47 117-81-705/04/17 22:23385 105 1
Fluoranthene ND ug/kg 05/05/17 15:47 206-44-005/04/17 22:23385 56.0 1
Fluorene ND ug/kg 05/05/17 15:47 86-73-705/04/17 22:23385 79.3 1
Hexachloro-1,3-butadiene ND ug/kg 05/05/17 15:47 87-68-305/04/17 22:23385 66.5 1
Hexachlorobenzene ND ug/kg 05/05/17 15:47 118-74-105/04/17 22:23385 49.0 1
Hexachlorocyclopentadiene ND ug/kg 05/05/17 15:47 77-47-405/04/17 22:23385 71.2 1
Hexachloroethane ND ug/kg 05/05/17 15:47 67-72-105/04/17 22:23385 101 1
Indeno(1,2,3-cd)pyrene ND ug/kg 05/05/17 15:47 193-39-505/04/17 22:23385 79.3 1
Isophorone ND ug/kg 05/05/17 15:47 78-59-105/04/17 22:23385 86.3 1
1-Methylnaphthalene ND ug/kg 05/05/17 15:47 90-12-005/04/17 22:23385 100 1
2-Methylnaphthalene ND ug/kg 05/05/17 15:47 91-57-605/04/17 22:23385 82.8 1
2-Methylphenol(o-Cresol)ND ug/kg 05/05/17 15:47 95-48-705/04/17 22:23385 117 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 05/05/17 15:47 15831-10-405/04/17 22:23385 152 1
Naphthalene ND ug/kg 05/05/17 15:47 91-20-305/04/17 22:23385 94.5 1
2-Nitroaniline ND ug/kg 05/05/17 15:47 88-74-405/04/17 22:231920 119 1
3-Nitroaniline ND ug/kg 05/05/17 15:47 99-09-205/04/17 22:231920 105 1
4-Nitroaniline ND ug/kg 05/05/17 15:47 100-01-605/04/17 22:23770 108 1
Nitrobenzene ND ug/kg 05/05/17 15:47 98-95-305/04/17 22:23385 105 1
2-Nitrophenol ND ug/kg 05/05/17 15:47 88-75-505/04/17 22:23385 93.3 1
4-Nitrophenol ND ug/kg 05/05/17 15:47 100-02-705/04/17 22:231920 68.8 1
N-Nitrosodimethylamine ND ug/kg 05/05/17 15:47 62-75-905/04/17 22:23385 125 1
N-Nitroso-di-n-propylamine ND ug/kg 05/05/17 15:47 621-64-705/04/17 22:23385 73.5 1
N-Nitrosodiphenylamine ND ug/kg 05/05/17 15:47 86-30-605/04/17 22:23385 114 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 05/05/17 15:47 108-60-105/04/17 22:23385 103 1
Pentachlorophenol ND ug/kg 05/05/17 15:47 87-86-505/04/17 22:231920 70.0 1
Phenanthrene ND ug/kg 05/05/17 15:47 85-01-805/04/17 22:23385 64.2 1
Phenol ND ug/kg 05/05/17 15:47 108-95-205/04/17 22:23385 115 1
Pyrene ND ug/kg 05/05/17 15:47 129-00-005/04/17 22:23385 65.3 1
1,2,4-Trichlorobenzene ND ug/kg 05/05/17 15:47 120-82-105/04/17 22:23385 74.7 1
2,4,5-Trichlorophenol ND ug/kg 05/05/17 15:47 95-95-405/04/17 22:23385 119 1
2,4,6-Trichlorophenol ND ug/kg 05/05/17 15:47 88-06-205/04/17 22:23385 85.2 1
Surrogates
Nitrobenzene-d5 (S)25 %05/05/17 15:47 4165-60-005/04/17 22:2323-110 1
2-Fluorobiphenyl (S)27 %05/05/17 15:47 321-60-8 S005/04/17 22:2330-110 1
Terphenyl-d14 (S)35 %05/05/17 15:47 1718-51-005/04/17 22:2328-110 1
Phenol-d6 (S)22 %05/05/17 15:47 13127-88-305/04/17 22:2322-110 1
2-Fluorophenol (S)21 %05/05/17 15:47 367-12-405/04/17 22:2313-110 1
2,4,6-Tribromophenol (S)28 %05/05/17 15:47 118-79-605/04/17 22:2327-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone 25.9J ug/kg 05/05/17 15:07 67-64-1125 12.5 1
Benzene ND ug/kg 05/05/17 15:07 71-43-26.3 2.0 1
Bromobenzene ND ug/kg 05/05/17 15:07 108-86-16.3 2.5 1
Bromochloromethane ND ug/kg 05/05/17 15:07 74-97-56.3 2.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 86
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339291
BANK STREET
Sample: SB-1(17-18)Lab ID: 92339291004 Collected: 05/02/17 09:50 Received: 05/03/17 10:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Bromodichloromethane ND ug/kg 05/05/17 15:07 75-27-46.3 2.4 1
Bromoform ND ug/kg 05/05/17 15:07 75-25-26.3 2.9 1
Bromomethane ND ug/kg 05/05/17 15:07 74-83-912.5 3.1 1
2-Butanone (MEK)ND ug/kg 05/05/17 15:07 78-93-3125 3.6 1
n-Butylbenzene ND ug/kg 05/05/17 15:07 104-51-86.3 2.3 1
sec-Butylbenzene ND ug/kg 05/05/17 15:07 135-98-86.3 2.0 1
tert-Butylbenzene ND ug/kg 05/05/17 15:07 98-06-66.3 2.5 1
Carbon tetrachloride ND ug/kg 05/05/17 15:07 56-23-56.3 3.3 1
Chlorobenzene ND ug/kg 05/05/17 15:07 108-90-76.3 2.4 1
Chloroethane ND ug/kg 05/05/17 15:07 75-00-312.5 3.0 1
Chloroform ND ug/kg 05/05/17 15:07 67-66-36.3 2.0 1
Chloromethane ND ug/kg 05/05/17 15:07 74-87-312.5 3.0 1
2-Chlorotoluene ND ug/kg 05/05/17 15:07 95-49-86.3 2.1 1
4-Chlorotoluene ND ug/kg 05/05/17 15:07 106-43-46.3 2.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 05/05/17 15:07 96-12-86.3 4.5 1
Dibromochloromethane ND ug/kg 05/05/17 15:07 124-48-16.3 2.3 1
1,2-Dibromoethane (EDB)ND ug/kg 05/05/17 15:07 106-93-46.3 2.3 1
Dibromomethane ND ug/kg 05/05/17 15:07 74-95-36.3 3.1 1
1,2-Dichlorobenzene ND ug/kg 05/05/17 15:07 95-50-16.3 2.4 1
1,3-Dichlorobenzene ND ug/kg 05/05/17 15:07 541-73-16.3 2.5 1
1,4-Dichlorobenzene ND ug/kg 05/05/17 15:07 106-46-76.3 2.1 1
Dichlorodifluoromethane ND ug/kg 05/05/17 15:07 75-71-812.5 4.5 1
1,1-Dichloroethane ND ug/kg 05/05/17 15:07 75-34-36.3 1.9 1
1,2-Dichloroethane ND ug/kg 05/05/17 15:07 107-06-26.3 2.8 1
1,1-Dichloroethene ND ug/kg 05/05/17 15:07 75-35-46.3 2.3 1
cis-1,2-Dichloroethene ND ug/kg 05/05/17 15:07 156-59-26.3 1.8 1
trans-1,2-Dichloroethene ND ug/kg 05/05/17 15:07 156-60-56.3 2.4 1
1,2-Dichloropropane ND ug/kg 05/05/17 15:07 78-87-56.3 2.1 1
1,3-Dichloropropane ND ug/kg 05/05/17 15:07 142-28-96.3 2.4 1
2,2-Dichloropropane ND ug/kg 05/05/17 15:07 594-20-76.3 2.1 1
1,1-Dichloropropene ND ug/kg 05/05/17 15:07 563-58-66.3 1.9 1
cis-1,3-Dichloropropene ND ug/kg 05/05/17 15:07 10061-01-56.3 2.3 1
trans-1,3-Dichloropropene ND ug/kg 05/05/17 15:07 10061-02-66.3 1.9 1
Diisopropyl ether ND ug/kg 05/05/17 15:07 108-20-36.3 2.1 1
Ethylbenzene ND ug/kg 05/05/17 15:07 100-41-46.3 2.3 1
Hexachloro-1,3-butadiene ND ug/kg 05/05/17 15:07 87-68-36.3 2.5 1
2-Hexanone ND ug/kg 05/05/17 15:07 591-78-662.7 4.9 1
Isopropylbenzene (Cumene)ND ug/kg 05/05/17 15:07 98-82-86.3 2.4 1
p-Isopropyltoluene ND ug/kg 05/05/17 15:07 99-87-66.3 2.1 1
Methylene Chloride 5.3J ug/kg 05/05/17 15:07 75-09-225.1 3.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 05/05/17 15:07 108-10-162.7 4.6 1
Methyl-tert-butyl ether ND ug/kg 05/05/17 15:07 1634-04-46.3 1.9 1
Naphthalene ND ug/kg 05/05/17 15:07 91-20-36.3 1.5 1
n-Propylbenzene ND ug/kg 05/05/17 15:07 103-65-16.3 2.1 1
Styrene ND ug/kg 05/05/17 15:07 100-42-56.3 2.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 86
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339291
BANK STREET
Sample: SB-1(17-18)Lab ID: 92339291004 Collected: 05/02/17 09:50 Received: 05/03/17 10:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
1,1,1,2-Tetrachloroethane ND ug/kg 05/05/17 15:07 630-20-66.3 2.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 05/05/17 15:07 79-34-56.3 2.4 1
Tetrachloroethene ND ug/kg 05/05/17 15:07 127-18-46.3 2.1 1
Toluene 5.8J ug/kg 05/05/17 15:07 108-88-36.3 2.3 1
1,2,3-Trichlorobenzene ND ug/kg 05/05/17 15:07 87-61-66.3 2.8 1
1,2,4-Trichlorobenzene ND ug/kg 05/05/17 15:07 120-82-16.3 2.0 1
1,1,1-Trichloroethane ND ug/kg 05/05/17 15:07 71-55-66.3 2.3 1
1,1,2-Trichloroethane ND ug/kg 05/05/17 15:07 79-00-56.3 2.6 1
Trichloroethene ND ug/kg 05/05/17 15:07 79-01-66.3 2.6 1
Trichlorofluoromethane ND ug/kg 05/05/17 15:07 75-69-46.3 2.8 1
1,2,3-Trichloropropane ND ug/kg 05/05/17 15:07 96-18-46.3 2.0 1
1,2,4-Trimethylbenzene ND ug/kg 05/05/17 15:07 95-63-66.3 2.5 1
1,3,5-Trimethylbenzene ND ug/kg 05/05/17 15:07 108-67-86.3 2.3 1
Vinyl acetate ND ug/kg 05/05/17 15:07 108-05-462.7 11.0 1
Vinyl chloride ND ug/kg 05/05/17 15:07 75-01-412.5 2.3 1
Xylene (Total)ND ug/kg 05/05/17 15:07 1330-20-712.5 4.5 1
m&p-Xylene ND ug/kg 05/05/17 15:07 179601-23-112.5 4.5 1
o-Xylene ND ug/kg 05/05/17 15:07 95-47-66.3 2.4 1
Surrogates
Toluene-d8 (S)101 %05/05/17 15:07 2037-26-570-130 1
4-Bromofluorobenzene (S)95 %05/05/17 15:07 460-00-470-130 1
1,2-Dichloroethane-d4 (S)118 %05/05/17 15:07 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 14.3 %05/04/17 17:400.10 0.10 1
Sample: SB-3(14-15)Lab ID: 92339291005 Collected: 05/02/17 10:55 Received: 05/03/17 10:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8082 Preparation Method: EPA 35468082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/kg 05/05/17 00:59 12674-11-205/04/17 06:1839.8 18.1 1
PCB-1221 (Aroclor 1221)ND ug/kg 05/05/17 00:59 11104-28-205/04/17 06:1839.8 18.1 1
PCB-1232 (Aroclor 1232)ND ug/kg 05/05/17 00:59 11141-16-505/04/17 06:1839.8 18.1 1
PCB-1242 (Aroclor 1242)ND ug/kg 05/05/17 00:59 53469-21-905/04/17 06:1839.8 18.1 1
PCB-1248 (Aroclor 1248)ND ug/kg 05/05/17 00:59 12672-29-605/04/17 06:1839.8 18.1 1
PCB-1254 (Aroclor 1254)ND ug/kg 05/05/17 00:59 11097-69-105/04/17 06:1839.8 18.1 1
PCB-1260 (Aroclor 1260)ND ug/kg 05/05/17 00:59 11096-82-505/04/17 06:1839.8 18.1 1
Surrogates
Decachlorobiphenyl (S)81 %05/05/17 00:59 2051-24-305/04/17 06:1821-132 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 86
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339291
BANK STREET
Sample: SB-3(14-15)Lab ID: 92339291005 Collected: 05/02/17 10:55 Received: 05/03/17 10:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Antimony ND mg/kg 05/09/17 21:35 7440-36-005/05/17 10:050.49 0.39 1
Arsenic 1.2 mg/kg 05/09/17 21:35 7440-38-205/05/17 10:050.99 0.49 1
Beryllium 1.1 mg/kg 05/09/17 21:35 7440-41-705/05/17 10:050.099 0.049 1
Cadmium ND mg/kg 05/09/17 21:35 7440-43-905/05/17 10:050.099 0.049 1
Chromium 16.4 mg/kg 05/09/17 21:35 7440-47-305/05/17 10:050.49 0.25 1
Copper 51.2 mg/kg 05/09/17 21:35 7440-50-805/05/17 10:050.49 0.25 1
Lead 2.4 mg/kg 05/09/17 21:35 7439-92-105/05/17 10:050.49 0.25 1
Nickel 28.9 mg/kg 05/09/17 21:35 7440-02-005/05/17 10:050.49 0.25 1
Selenium 1.3 mg/kg 05/09/17 21:35 7782-49-205/05/17 10:050.99 0.49 1
Silver ND mg/kg 05/09/17 21:35 7440-22-405/05/17 10:050.49 0.25 1
Thallium ND mg/kg 05/09/17 21:35 7440-28-005/05/17 10:050.99 0.49 1
Zinc 68.3 mg/kg 05/09/17 21:35 7440-66-605/05/17 10:050.99 0.49 1
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury 0.010 mg/kg 05/10/17 11:24 7439-97-605/10/17 04:000.0066 0.0033 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 05/10/17 11:27 83-32-905/09/17 15:41398 91.7 1
Acenaphthylene ND ug/kg 05/10/17 11:27 208-96-805/09/17 15:41398 94.1 1
Aniline ND ug/kg 05/10/17 11:27 62-53-305/09/17 15:41398 107 1
Anthracene ND ug/kg 05/10/17 11:27 120-12-705/09/17 15:41398 89.3 1
Benzo(a)anthracene ND ug/kg 05/10/17 11:27 56-55-305/09/17 15:41398 73.6 1
Benzo(a)pyrene ND ug/kg 05/10/17 11:27 50-32-805/09/17 15:41398 76.0 1
Benzo(b)fluoranthene ND ug/kg 05/10/17 11:27 205-99-205/09/17 15:41398 68.8 1
Benzo(g,h,i)perylene ND ug/kg 05/10/17 11:27 191-24-205/09/17 15:41398 101 1
Benzo(k)fluoranthene ND ug/kg 05/10/17 11:27 207-08-905/09/17 15:41398 78.5 1
Benzoic Acid ND ug/kg 05/10/17 11:27 65-85-005/09/17 15:411990 72.4 1
Benzyl alcohol ND ug/kg 05/10/17 11:27 100-51-605/09/17 15:41797 79.7 1
4-Bromophenylphenyl ether ND ug/kg 05/10/17 11:27 101-55-305/09/17 15:41398 72.4 1
Butylbenzylphthalate ND ug/kg 05/10/17 11:27 85-68-705/09/17 15:41398 84.5 1
4-Chloro-3-methylphenol ND ug/kg 05/10/17 11:27 59-50-705/09/17 15:41797 82.1 1
4-Chloroaniline ND ug/kg 05/10/17 11:27 106-47-805/09/17 15:411990 111 1
bis(2-Chloroethoxy)methane ND ug/kg 05/10/17 11:27 111-91-105/09/17 15:41398 92.9 1
bis(2-Chloroethyl) ether ND ug/kg 05/10/17 11:27 111-44-405/09/17 15:41398 101 1
2-Chloronaphthalene ND ug/kg 05/10/17 11:27 91-58-705/09/17 15:41398 78.5 1
2-Chlorophenol ND ug/kg 05/10/17 11:27 95-57-805/09/17 15:41398 109 1
4-Chlorophenylphenyl ether ND ug/kg 05/10/17 11:27 7005-72-305/09/17 15:41398 82.1 1
Chrysene ND ug/kg 05/10/17 11:27 218-01-905/09/17 15:41398 53.1 1
Dibenz(a,h)anthracene ND ug/kg 05/10/17 11:27 53-70-305/09/17 15:41398 84.5 1
Dibenzofuran ND ug/kg 05/10/17 11:27 132-64-905/09/17 15:41398 65.2 1
1,2-Dichlorobenzene ND ug/kg 05/10/17 11:27 95-50-105/09/17 15:41398 106 1
1,3-Dichlorobenzene ND ug/kg 05/10/17 11:27 541-73-1 L205/09/17 15:41398 90.5 1
1,4-Dichlorobenzene ND ug/kg 05/10/17 11:27 106-46-705/09/17 15:41398 112 1
3,3'-Dichlorobenzidine ND ug/kg 05/10/17 11:27 91-94-105/09/17 15:411990 86.9 1
2,4-Dichlorophenol ND ug/kg 05/10/17 11:27 120-83-205/09/17 15:41398 86.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 86
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339291
BANK STREET
Sample: SB-3(14-15)Lab ID: 92339291005 Collected: 05/02/17 10:55 Received: 05/03/17 10:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND ug/kg 05/10/17 11:27 84-66-205/09/17 15:41398 61.6 1
2,4-Dimethylphenol ND ug/kg 05/10/17 11:27 105-67-905/09/17 15:41398 157 1
Dimethylphthalate ND ug/kg 05/10/17 11:27 131-11-305/09/17 15:41398 80.9 1
Di-n-butylphthalate ND ug/kg 05/10/17 11:27 84-74-205/09/17 15:41398 65.2 1
4,6-Dinitro-2-methylphenol ND ug/kg 05/10/17 11:27 534-52-105/09/17 15:41797 79.7 1
2,4-Dinitrophenol ND ug/kg 05/10/17 11:27 51-28-505/09/17 15:411990 65.2 1
2,4-Dinitrotoluene ND ug/kg 05/10/17 11:27 121-14-205/09/17 15:41398 74.8 1
2,6-Dinitrotoluene ND ug/kg 05/10/17 11:27 606-20-205/09/17 15:41398 83.3 1
Di-n-octylphthalate ND ug/kg 05/10/17 11:27 117-84-005/09/17 15:41398 83.3 1
bis(2-Ethylhexyl)phthalate ND ug/kg 05/10/17 11:27 117-81-705/09/17 15:41398 109 1
Fluoranthene ND ug/kg 05/10/17 11:27 206-44-005/09/17 15:41398 57.9 1
Fluorene ND ug/kg 05/10/17 11:27 86-73-705/09/17 15:41398 82.1 1
Hexachloro-1,3-butadiene ND ug/kg 05/10/17 11:27 87-68-305/09/17 15:41398 68.8 1
Hexachlorobenzene ND ug/kg 05/10/17 11:27 118-74-105/09/17 15:41398 50.7 1
Hexachlorocyclopentadiene ND ug/kg 05/10/17 11:27 77-47-405/09/17 15:41398 73.6 1
Hexachloroethane ND ug/kg 05/10/17 11:27 67-72-105/09/17 15:41398 105 1
Indeno(1,2,3-cd)pyrene ND ug/kg 05/10/17 11:27 193-39-505/09/17 15:41398 82.1 1
Isophorone ND ug/kg 05/10/17 11:27 78-59-105/09/17 15:41398 89.3 1
1-Methylnaphthalene ND ug/kg 05/10/17 11:27 90-12-005/09/17 15:41398 104 1
2-Methylnaphthalene ND ug/kg 05/10/17 11:27 91-57-605/09/17 15:41398 85.7 1
2-Methylphenol(o-Cresol)ND ug/kg 05/10/17 11:27 95-48-705/09/17 15:41398 121 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 05/10/17 11:27 15831-10-405/09/17 15:41398 157 1
Naphthalene ND ug/kg 05/10/17 11:27 91-20-305/09/17 15:41398 97.8 1
2-Nitroaniline ND ug/kg 05/10/17 11:27 88-74-405/09/17 15:411990 123 1
3-Nitroaniline ND ug/kg 05/10/17 11:27 99-09-205/09/17 15:411990 109 1
4-Nitroaniline ND ug/kg 05/10/17 11:27 100-01-605/09/17 15:41797 112 1
Nitrobenzene ND ug/kg 05/10/17 11:27 98-95-305/09/17 15:41398 109 1
2-Nitrophenol ND ug/kg 05/10/17 11:27 88-75-505/09/17 15:41398 96.6 1
4-Nitrophenol ND ug/kg 05/10/17 11:27 100-02-705/09/17 15:411990 71.2 1
N-Nitrosodimethylamine ND ug/kg 05/10/17 11:27 62-75-905/09/17 15:41398 129 1
N-Nitroso-di-n-propylamine ND ug/kg 05/10/17 11:27 621-64-705/09/17 15:41398 76.0 1
N-Nitrosodiphenylamine ND ug/kg 05/10/17 11:27 86-30-605/09/17 15:41398 118 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 05/10/17 11:27 108-60-105/09/17 15:41398 106 1
Pentachlorophenol ND ug/kg 05/10/17 11:27 87-86-505/09/17 15:411990 72.4 1
Phenanthrene ND ug/kg 05/10/17 11:27 85-01-805/09/17 15:41398 66.4 1
Phenol ND ug/kg 05/10/17 11:27 108-95-205/09/17 15:41398 119 1
Pyrene ND ug/kg 05/10/17 11:27 129-00-005/09/17 15:41398 67.6 1
1,2,4-Trichlorobenzene ND ug/kg 05/10/17 11:27 120-82-105/09/17 15:41398 77.2 1
2,4,5-Trichlorophenol ND ug/kg 05/10/17 11:27 95-95-405/09/17 15:41398 123 1
2,4,6-Trichlorophenol ND ug/kg 05/10/17 11:27 88-06-205/09/17 15:41398 88.1 1
Surrogates
Nitrobenzene-d5 (S)27 %05/10/17 11:27 4165-60-005/09/17 15:4123-110 1
2-Fluorobiphenyl (S)27 %05/10/17 11:27 321-60-8 S005/09/17 15:4130-110 1
Terphenyl-d14 (S)39 %05/10/17 11:27 1718-51-005/09/17 15:4128-110 1
Phenol-d6 (S)28 %05/10/17 11:27 13127-88-305/09/17 15:4122-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 86
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339291
BANK STREET
Sample: SB-3(14-15)Lab ID: 92339291005 Collected: 05/02/17 10:55 Received: 05/03/17 10:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2-Fluorophenol (S)27 %05/10/17 11:27 367-12-405/09/17 15:4113-110 1
2,4,6-Tribromophenol (S)32 %05/10/17 11:27 118-79-605/09/17 15:4127-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone 33.7J ug/kg 05/05/17 15:27 67-64-1123 12.3 1
Benzene ND ug/kg 05/05/17 15:27 71-43-26.2 2.0 1
Bromobenzene ND ug/kg 05/05/17 15:27 108-86-16.2 2.5 1
Bromochloromethane ND ug/kg 05/05/17 15:27 74-97-56.2 2.1 1
Bromodichloromethane ND ug/kg 05/05/17 15:27 75-27-46.2 2.3 1
Bromoform ND ug/kg 05/05/17 15:27 75-25-26.2 2.8 1
Bromomethane ND ug/kg 05/05/17 15:27 74-83-912.3 3.1 1
2-Butanone (MEK)ND ug/kg 05/05/17 15:27 78-93-3123 3.6 1
n-Butylbenzene ND ug/kg 05/05/17 15:27 104-51-86.2 2.2 1
sec-Butylbenzene ND ug/kg 05/05/17 15:27 135-98-86.2 2.0 1
tert-Butylbenzene ND ug/kg 05/05/17 15:27 98-06-66.2 2.5 1
Carbon tetrachloride ND ug/kg 05/05/17 15:27 56-23-56.2 3.2 1
Chlorobenzene ND ug/kg 05/05/17 15:27 108-90-76.2 2.3 1
Chloroethane ND ug/kg 05/05/17 15:27 75-00-312.3 3.0 1
Chloroform ND ug/kg 05/05/17 15:27 67-66-36.2 2.0 1
Chloromethane ND ug/kg 05/05/17 15:27 74-87-312.3 3.0 1
2-Chlorotoluene ND ug/kg 05/05/17 15:27 95-49-86.2 2.1 1
4-Chlorotoluene ND ug/kg 05/05/17 15:27 106-43-46.2 2.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 05/05/17 15:27 96-12-86.2 4.4 1
Dibromochloromethane ND ug/kg 05/05/17 15:27 124-48-16.2 2.2 1
1,2-Dibromoethane (EDB)ND ug/kg 05/05/17 15:27 106-93-46.2 2.2 1
Dibromomethane ND ug/kg 05/05/17 15:27 74-95-36.2 3.1 1
1,2-Dichlorobenzene ND ug/kg 05/05/17 15:27 95-50-16.2 2.3 1
1,3-Dichlorobenzene ND ug/kg 05/05/17 15:27 541-73-16.2 2.5 1
1,4-Dichlorobenzene ND ug/kg 05/05/17 15:27 106-46-76.2 2.1 1
Dichlorodifluoromethane ND ug/kg 05/05/17 15:27 75-71-812.3 4.4 1
1,1-Dichloroethane ND ug/kg 05/05/17 15:27 75-34-36.2 1.9 1
1,2-Dichloroethane ND ug/kg 05/05/17 15:27 107-06-26.2 2.7 1
1,1-Dichloroethene ND ug/kg 05/05/17 15:27 75-35-46.2 2.2 1
cis-1,2-Dichloroethene ND ug/kg 05/05/17 15:27 156-59-26.2 1.7 1
trans-1,2-Dichloroethene ND ug/kg 05/05/17 15:27 156-60-56.2 2.3 1
1,2-Dichloropropane ND ug/kg 05/05/17 15:27 78-87-56.2 2.1 1
1,3-Dichloropropane ND ug/kg 05/05/17 15:27 142-28-96.2 2.3 1
2,2-Dichloropropane ND ug/kg 05/05/17 15:27 594-20-76.2 2.1 1
1,1-Dichloropropene ND ug/kg 05/05/17 15:27 563-58-66.2 1.9 1
cis-1,3-Dichloropropene ND ug/kg 05/05/17 15:27 10061-01-56.2 2.2 1
trans-1,3-Dichloropropene ND ug/kg 05/05/17 15:27 10061-02-66.2 1.9 1
Diisopropyl ether ND ug/kg 05/05/17 15:27 108-20-36.2 2.1 1
Ethylbenzene ND ug/kg 05/05/17 15:27 100-41-46.2 2.2 1
Hexachloro-1,3-butadiene ND ug/kg 05/05/17 15:27 87-68-36.2 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 86
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339291
BANK STREET
Sample: SB-3(14-15)Lab ID: 92339291005 Collected: 05/02/17 10:55 Received: 05/03/17 10:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
2-Hexanone ND ug/kg 05/05/17 15:27 591-78-661.7 4.8 1
Isopropylbenzene (Cumene)ND ug/kg 05/05/17 15:27 98-82-86.2 2.3 1
p-Isopropyltoluene ND ug/kg 05/05/17 15:27 99-87-66.2 2.1 1
Methylene Chloride ND ug/kg 05/05/17 15:27 75-09-224.7 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 05/05/17 15:27 108-10-161.7 4.6 1
Methyl-tert-butyl ether ND ug/kg 05/05/17 15:27 1634-04-46.2 1.9 1
Naphthalene ND ug/kg 05/05/17 15:27 91-20-36.2 1.5 1
n-Propylbenzene ND ug/kg 05/05/17 15:27 103-65-16.2 2.1 1
Styrene ND ug/kg 05/05/17 15:27 100-42-56.2 2.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 05/05/17 15:27 630-20-66.2 2.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 05/05/17 15:27 79-34-56.2 2.3 1
Tetrachloroethene ND ug/kg 05/05/17 15:27 127-18-46.2 2.1 1
Toluene 5.3J ug/kg 05/05/17 15:27 108-88-36.2 2.2 1
1,2,3-Trichlorobenzene ND ug/kg 05/05/17 15:27 87-61-66.2 2.7 1
1,2,4-Trichlorobenzene ND ug/kg 05/05/17 15:27 120-82-16.2 2.0 1
1,1,1-Trichloroethane ND ug/kg 05/05/17 15:27 71-55-66.2 2.2 1
1,1,2-Trichloroethane ND ug/kg 05/05/17 15:27 79-00-56.2 2.6 1
Trichloroethene ND ug/kg 05/05/17 15:27 79-01-66.2 2.6 1
Trichlorofluoromethane ND ug/kg 05/05/17 15:27 75-69-46.2 2.7 1
1,2,3-Trichloropropane ND ug/kg 05/05/17 15:27 96-18-46.2 2.0 1
1,2,4-Trimethylbenzene ND ug/kg 05/05/17 15:27 95-63-66.2 2.5 1
1,3,5-Trimethylbenzene ND ug/kg 05/05/17 15:27 108-67-86.2 2.2 1
Vinyl acetate ND ug/kg 05/05/17 15:27 108-05-461.7 10.9 1
Vinyl chloride ND ug/kg 05/05/17 15:27 75-01-412.3 2.2 1
Xylene (Total)ND ug/kg 05/05/17 15:27 1330-20-712.3 4.4 1
m&p-Xylene ND ug/kg 05/05/17 15:27 179601-23-112.3 4.4 1
o-Xylene ND ug/kg 05/05/17 15:27 95-47-66.2 2.3 1
Surrogates
Toluene-d8 (S)100 %05/05/17 15:27 2037-26-570-130 1
4-Bromofluorobenzene (S)96 %05/05/17 15:27 460-00-470-130 1
1,2-Dichloroethane-d4 (S)118 %05/05/17 15:27 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 17.1 %05/04/17 17:410.10 0.10 1
Sample: SB-4(5-6)Lab ID: 92339291006 Collected: 05/02/17 11:50 Received: 05/03/17 10:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8082 Preparation Method: EPA 35468082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/kg 05/05/17 01:20 12674-11-205/04/17 06:1841.2 18.7 1
PCB-1221 (Aroclor 1221)ND ug/kg 05/05/17 01:20 11104-28-205/04/17 06:1841.2 18.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 86
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339291
BANK STREET
Sample: SB-4(5-6)Lab ID: 92339291006 Collected: 05/02/17 11:50 Received: 05/03/17 10:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8082 Preparation Method: EPA 35468082 GCS PCB
PCB-1232 (Aroclor 1232)ND ug/kg 05/05/17 01:20 11141-16-505/04/17 06:1841.2 18.7 1
PCB-1242 (Aroclor 1242)ND ug/kg 05/05/17 01:20 53469-21-905/04/17 06:1841.2 18.7 1
PCB-1248 (Aroclor 1248)ND ug/kg 05/05/17 01:20 12672-29-605/04/17 06:1841.2 18.7 1
PCB-1254 (Aroclor 1254)ND ug/kg 05/05/17 01:20 11097-69-105/04/17 06:1841.2 18.7 1
PCB-1260 (Aroclor 1260)ND ug/kg 05/05/17 01:20 11096-82-505/04/17 06:1841.2 18.7 1
Surrogates
Decachlorobiphenyl (S)76 %05/05/17 01:20 2051-24-305/04/17 06:1821-132 1
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Antimony ND mg/kg 05/10/17 11:48 7440-36-0 D305/05/17 10:052.6 2.0 5
Arsenic 4.6J mg/kg 05/10/17 11:48 7440-38-2 D305/05/17 10:055.2 2.6 5
Beryllium 0.69 mg/kg 05/10/17 11:48 7440-41-705/05/17 10:050.52 0.26 5
Cadmium ND mg/kg 05/10/17 11:48 7440-43-9 D305/05/17 10:050.52 0.26 5
Chromium 11.6 mg/kg 05/10/17 11:48 7440-47-305/05/17 10:052.6 1.3 5
Copper 55.1 mg/kg 05/10/17 11:48 7440-50-805/05/17 10:052.6 1.3 5
Lead 9.4 mg/kg 05/10/17 11:48 7439-92-105/05/17 10:052.6 1.3 5
Nickel 9.5 mg/kg 05/10/17 11:48 7440-02-005/05/17 10:052.6 1.3 5
Selenium ND mg/kg 05/10/17 11:48 7782-49-2 D305/05/17 10:055.2 2.6 5
Silver ND mg/kg 05/10/17 11:48 7440-22-4 D305/05/17 10:052.6 1.3 5
Thallium ND mg/kg 05/10/17 11:48 7440-28-0 D305/05/17 10:055.2 2.6 5
Zinc 46.0 mg/kg 05/10/17 11:48 7440-66-605/05/17 10:055.2 2.6 5
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury 0.015 mg/kg 05/10/17 11:26 7439-97-605/10/17 04:000.0072 0.0036 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 05/10/17 11:56 83-32-905/09/17 15:41412 94.8 1
Acenaphthylene ND ug/kg 05/10/17 11:56 208-96-805/09/17 15:41412 97.3 1
Aniline ND ug/kg 05/10/17 11:56 62-53-305/09/17 15:41412 111 1
Anthracene ND ug/kg 05/10/17 11:56 120-12-705/09/17 15:41412 92.3 1
Benzo(a)anthracene ND ug/kg 05/10/17 11:56 56-55-305/09/17 15:41412 76.1 1
Benzo(a)pyrene ND ug/kg 05/10/17 11:56 50-32-805/09/17 15:41412 78.6 1
Benzo(b)fluoranthene ND ug/kg 05/10/17 11:56 205-99-205/09/17 15:41412 71.1 1
Benzo(g,h,i)perylene ND ug/kg 05/10/17 11:56 191-24-205/09/17 15:41412 105 1
Benzo(k)fluoranthene ND ug/kg 05/10/17 11:56 207-08-905/09/17 15:41412 81.1 1
Benzoic Acid ND ug/kg 05/10/17 11:56 65-85-005/09/17 15:412060 74.9 1
Benzyl alcohol ND ug/kg 05/10/17 11:56 100-51-605/09/17 15:41824 82.4 1
4-Bromophenylphenyl ether ND ug/kg 05/10/17 11:56 101-55-305/09/17 15:41412 74.9 1
Butylbenzylphthalate ND ug/kg 05/10/17 11:56 85-68-705/09/17 15:41412 87.3 1
4-Chloro-3-methylphenol ND ug/kg 05/10/17 11:56 59-50-705/09/17 15:41824 84.8 1
4-Chloroaniline ND ug/kg 05/10/17 11:56 106-47-805/09/17 15:412060 115 1
bis(2-Chloroethoxy)methane ND ug/kg 05/10/17 11:56 111-91-105/09/17 15:41412 96.1 1
bis(2-Chloroethyl) ether ND ug/kg 05/10/17 11:56 111-44-405/09/17 15:41412 105 1
2-Chloronaphthalene ND ug/kg 05/10/17 11:56 91-58-705/09/17 15:41412 81.1 1
2-Chlorophenol ND ug/kg 05/10/17 11:56 95-57-805/09/17 15:41412 112 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 86
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339291
BANK STREET
Sample: SB-4(5-6)Lab ID: 92339291006 Collected: 05/02/17 11:50 Received: 05/03/17 10:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
4-Chlorophenylphenyl ether ND ug/kg 05/10/17 11:56 7005-72-305/09/17 15:41412 84.8 1
Chrysene ND ug/kg 05/10/17 11:56 218-01-905/09/17 15:41412 54.9 1
Dibenz(a,h)anthracene ND ug/kg 05/10/17 11:56 53-70-305/09/17 15:41412 87.3 1
Dibenzofuran ND ug/kg 05/10/17 11:56 132-64-905/09/17 15:41412 67.4 1
1,2-Dichlorobenzene ND ug/kg 05/10/17 11:56 95-50-105/09/17 15:41412 110 1
1,3-Dichlorobenzene ND ug/kg 05/10/17 11:56 541-73-1 L205/09/17 15:41412 93.6 1
1,4-Dichlorobenzene ND ug/kg 05/10/17 11:56 106-46-705/09/17 15:41412 116 1
3,3'-Dichlorobenzidine ND ug/kg 05/10/17 11:56 91-94-105/09/17 15:412060 89.8 1
2,4-Dichlorophenol ND ug/kg 05/10/17 11:56 120-83-205/09/17 15:41412 89.8 1
Diethylphthalate ND ug/kg 05/10/17 11:56 84-66-205/09/17 15:41412 63.6 1
2,4-Dimethylphenol ND ug/kg 05/10/17 11:56 105-67-905/09/17 15:41412 162 1
Dimethylphthalate ND ug/kg 05/10/17 11:56 131-11-305/09/17 15:41412 83.6 1
Di-n-butylphthalate ND ug/kg 05/10/17 11:56 84-74-205/09/17 15:41412 67.4 1
4,6-Dinitro-2-methylphenol ND ug/kg 05/10/17 11:56 534-52-105/09/17 15:41824 82.4 1
2,4-Dinitrophenol ND ug/kg 05/10/17 11:56 51-28-505/09/17 15:412060 67.4 1
2,4-Dinitrotoluene ND ug/kg 05/10/17 11:56 121-14-205/09/17 15:41412 77.4 1
2,6-Dinitrotoluene ND ug/kg 05/10/17 11:56 606-20-205/09/17 15:41412 86.1 1
Di-n-octylphthalate ND ug/kg 05/10/17 11:56 117-84-005/09/17 15:41412 86.1 1
bis(2-Ethylhexyl)phthalate ND ug/kg 05/10/17 11:56 117-81-705/09/17 15:41412 112 1
Fluoranthene ND ug/kg 05/10/17 11:56 206-44-005/09/17 15:41412 59.9 1
Fluorene ND ug/kg 05/10/17 11:56 86-73-705/09/17 15:41412 84.8 1
Hexachloro-1,3-butadiene ND ug/kg 05/10/17 11:56 87-68-305/09/17 15:41412 71.1 1
Hexachlorobenzene ND ug/kg 05/10/17 11:56 118-74-105/09/17 15:41412 52.4 1
Hexachlorocyclopentadiene ND ug/kg 05/10/17 11:56 77-47-405/09/17 15:41412 76.1 1
Hexachloroethane ND ug/kg 05/10/17 11:56 67-72-105/09/17 15:41412 109 1
Indeno(1,2,3-cd)pyrene ND ug/kg 05/10/17 11:56 193-39-505/09/17 15:41412 84.8 1
Isophorone ND ug/kg 05/10/17 11:56 78-59-105/09/17 15:41412 92.3 1
1-Methylnaphthalene ND ug/kg 05/10/17 11:56 90-12-005/09/17 15:41412 107 1
2-Methylnaphthalene ND ug/kg 05/10/17 11:56 91-57-605/09/17 15:41412 88.6 1
2-Methylphenol(o-Cresol)ND ug/kg 05/10/17 11:56 95-48-705/09/17 15:41412 125 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 05/10/17 11:56 15831-10-405/09/17 15:41412 162 1
Naphthalene ND ug/kg 05/10/17 11:56 91-20-305/09/17 15:41412 101 1
2-Nitroaniline ND ug/kg 05/10/17 11:56 88-74-405/09/17 15:412060 127 1
3-Nitroaniline ND ug/kg 05/10/17 11:56 99-09-205/09/17 15:412060 112 1
4-Nitroaniline ND ug/kg 05/10/17 11:56 100-01-605/09/17 15:41824 116 1
Nitrobenzene ND ug/kg 05/10/17 11:56 98-95-305/09/17 15:41412 112 1
2-Nitrophenol ND ug/kg 05/10/17 11:56 88-75-505/09/17 15:41412 99.8 1
4-Nitrophenol ND ug/kg 05/10/17 11:56 100-02-705/09/17 15:412060 73.6 1
N-Nitrosodimethylamine ND ug/kg 05/10/17 11:56 62-75-905/09/17 15:41412 134 1
N-Nitroso-di-n-propylamine ND ug/kg 05/10/17 11:56 621-64-705/09/17 15:41412 78.6 1
N-Nitrosodiphenylamine ND ug/kg 05/10/17 11:56 86-30-605/09/17 15:41412 122 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 05/10/17 11:56 108-60-105/09/17 15:41412 110 1
Pentachlorophenol ND ug/kg 05/10/17 11:56 87-86-505/09/17 15:412060 74.9 1
Phenanthrene ND ug/kg 05/10/17 11:56 85-01-805/09/17 15:41412 68.6 1
Phenol ND ug/kg 05/10/17 11:56 108-95-205/09/17 15:41412 124 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 86
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339291
BANK STREET
Sample: SB-4(5-6)Lab ID: 92339291006 Collected: 05/02/17 11:50 Received: 05/03/17 10:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Pyrene ND ug/kg 05/10/17 11:56 129-00-005/09/17 15:41412 69.9 1
1,2,4-Trichlorobenzene ND ug/kg 05/10/17 11:56 120-82-105/09/17 15:41412 79.9 1
2,4,5-Trichlorophenol ND ug/kg 05/10/17 11:56 95-95-405/09/17 15:41412 127 1
2,4,6-Trichlorophenol ND ug/kg 05/10/17 11:56 88-06-205/09/17 15:41412 91.1 1
SurrogatesNitrobenzene-d5 (S)41 %05/10/17 11:56 4165-60-005/09/17 15:4123-110 1
2-Fluorobiphenyl (S)39 %05/10/17 11:56 321-60-805/09/17 15:4130-110 1
Terphenyl-d14 (S)50 %05/10/17 11:56 1718-51-005/09/17 15:4128-110 1
Phenol-d6 (S)31 %05/10/17 11:56 13127-88-305/09/17 15:4122-110 1
2-Fluorophenol (S)29 %05/10/17 11:56 367-12-405/09/17 15:4113-110 1
2,4,6-Tribromophenol (S)30 %05/10/17 11:56 118-79-605/09/17 15:4127-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone 40.9J ug/kg 05/05/17 15:46 67-64-1136 13.6 1
Benzene ND ug/kg 05/05/17 15:46 71-43-26.8 2.2 1
Bromobenzene ND ug/kg 05/05/17 15:46 108-86-16.8 2.7 1
Bromochloromethane ND ug/kg 05/05/17 15:46 74-97-56.8 2.3 1
Bromodichloromethane ND ug/kg 05/05/17 15:46 75-27-46.8 2.6 1
Bromoform ND ug/kg 05/05/17 15:46 75-25-26.8 3.1 1
Bromomethane ND ug/kg 05/05/17 15:46 74-83-913.6 3.4 1
2-Butanone (MEK)ND ug/kg 05/05/17 15:46 78-93-3136 4.0 1
n-Butylbenzene ND ug/kg 05/05/17 15:46 104-51-86.8 2.5 1
sec-Butylbenzene ND ug/kg 05/05/17 15:46 135-98-86.8 2.2 1
tert-Butylbenzene ND ug/kg 05/05/17 15:46 98-06-66.8 2.7 1
Carbon tetrachloride ND ug/kg 05/05/17 15:46 56-23-56.8 3.5 1
Chlorobenzene ND ug/kg 05/05/17 15:46 108-90-76.8 2.6 1
Chloroethane ND ug/kg 05/05/17 15:46 75-00-313.6 3.3 1
Chloroform ND ug/kg 05/05/17 15:46 67-66-36.8 2.2 1
Chloromethane ND ug/kg 05/05/17 15:46 74-87-313.6 3.3 1
2-Chlorotoluene ND ug/kg 05/05/17 15:46 95-49-86.8 2.3 1
4-Chlorotoluene ND ug/kg 05/05/17 15:46 106-43-46.8 2.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 05/05/17 15:46 96-12-86.8 4.9 1
Dibromochloromethane ND ug/kg 05/05/17 15:46 124-48-16.8 2.5 1
1,2-Dibromoethane (EDB)ND ug/kg 05/05/17 15:46 106-93-46.8 2.5 1
Dibromomethane ND ug/kg 05/05/17 15:46 74-95-36.8 3.4 1
1,2-Dichlorobenzene ND ug/kg 05/05/17 15:46 95-50-16.8 2.6 1
1,3-Dichlorobenzene ND ug/kg 05/05/17 15:46 541-73-16.8 2.7 1
1,4-Dichlorobenzene ND ug/kg 05/05/17 15:46 106-46-76.8 2.3 1
Dichlorodifluoromethane ND ug/kg 05/05/17 15:46 75-71-813.6 4.9 1
1,1-Dichloroethane ND ug/kg 05/05/17 15:46 75-34-36.8 2.0 1
1,2-Dichloroethane ND ug/kg 05/05/17 15:46 107-06-26.8 3.0 1
1,1-Dichloroethene ND ug/kg 05/05/17 15:46 75-35-46.8 2.5 1
cis-1,2-Dichloroethene ND ug/kg 05/05/17 15:46 156-59-26.8 1.9 1
trans-1,2-Dichloroethene ND ug/kg 05/05/17 15:46 156-60-56.8 2.6 1
1,2-Dichloropropane ND ug/kg 05/05/17 15:46 78-87-56.8 2.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 86
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339291
BANK STREET
Sample: SB-4(5-6)Lab ID: 92339291006 Collected: 05/02/17 11:50 Received: 05/03/17 10:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
1,3-Dichloropropane ND ug/kg 05/05/17 15:46 142-28-96.8 2.6 1
2,2-Dichloropropane ND ug/kg 05/05/17 15:46 594-20-76.8 2.3 1
1,1-Dichloropropene ND ug/kg 05/05/17 15:46 563-58-66.8 2.0 1
cis-1,3-Dichloropropene ND ug/kg 05/05/17 15:46 10061-01-56.8 2.5 1
trans-1,3-Dichloropropene ND ug/kg 05/05/17 15:46 10061-02-66.8 2.0 1
Diisopropyl ether ND ug/kg 05/05/17 15:46 108-20-36.8 2.3 1
Ethylbenzene ND ug/kg 05/05/17 15:46 100-41-46.8 2.5 1
Hexachloro-1,3-butadiene ND ug/kg 05/05/17 15:46 87-68-36.8 2.7 1
2-Hexanone ND ug/kg 05/05/17 15:46 591-78-668.1 5.3 1
Isopropylbenzene (Cumene)ND ug/kg 05/05/17 15:46 98-82-86.8 2.6 1
p-Isopropyltoluene ND ug/kg 05/05/17 15:46 99-87-66.8 2.3 1
Methylene Chloride 6.7J ug/kg 05/05/17 15:46 75-09-227.2 4.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 05/05/17 15:46 108-10-168.1 5.0 1
Methyl-tert-butyl ether ND ug/kg 05/05/17 15:46 1634-04-46.8 2.0 1
Naphthalene ND ug/kg 05/05/17 15:46 91-20-36.8 1.6 1
n-Propylbenzene ND ug/kg 05/05/17 15:46 103-65-16.8 2.3 1
Styrene ND ug/kg 05/05/17 15:46 100-42-56.8 2.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 05/05/17 15:46 630-20-66.8 2.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 05/05/17 15:46 79-34-56.8 2.6 1
Tetrachloroethene ND ug/kg 05/05/17 15:46 127-18-46.8 2.3 1
Toluene 7.8 ug/kg 05/05/17 15:46 108-88-36.8 2.5 1
1,2,3-Trichlorobenzene ND ug/kg 05/05/17 15:46 87-61-66.8 3.0 1
1,2,4-Trichlorobenzene ND ug/kg 05/05/17 15:46 120-82-16.8 2.2 1
1,1,1-Trichloroethane ND ug/kg 05/05/17 15:46 71-55-66.8 2.5 1
1,1,2-Trichloroethane ND ug/kg 05/05/17 15:46 79-00-56.8 2.9 1
Trichloroethene ND ug/kg 05/05/17 15:46 79-01-66.8 2.9 1
Trichlorofluoromethane ND ug/kg 05/05/17 15:46 75-69-46.8 3.0 1
1,2,3-Trichloropropane ND ug/kg 05/05/17 15:46 96-18-46.8 2.2 1
1,2,4-Trimethylbenzene ND ug/kg 05/05/17 15:46 95-63-66.8 2.7 1
1,3,5-Trimethylbenzene ND ug/kg 05/05/17 15:46 108-67-86.8 2.5 1
Vinyl acetate ND ug/kg 05/05/17 15:46 108-05-468.1 12.0 1
Vinyl chloride ND ug/kg 05/05/17 15:46 75-01-413.6 2.5 1
Xylene (Total)ND ug/kg 05/05/17 15:46 1330-20-713.6 4.9 1
m&p-Xylene ND ug/kg 05/05/17 15:46 179601-23-113.6 4.9 1
o-Xylene ND ug/kg 05/05/17 15:46 95-47-66.8 2.6 1
Surrogates
Toluene-d8 (S)101 %05/05/17 15:46 2037-26-570-130 1
4-Bromofluorobenzene (S)96 %05/05/17 15:46 460-00-470-130 1
1,2-Dichloroethane-d4 (S)122 %05/05/17 15:46 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 19.9 %05/04/17 17:410.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 86
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339291
BANK STREET
Sample: SB-6(14-15)Lab ID: 92339291007 Collected: 05/02/17 12:30 Received: 05/03/17 10:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8082 Preparation Method: EPA 35468082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/kg 05/04/17 18:02 12674-11-205/04/17 06:1840.8 18.5 1
PCB-1221 (Aroclor 1221)ND ug/kg 05/04/17 18:02 11104-28-205/04/17 06:1840.8 18.5 1
PCB-1232 (Aroclor 1232)ND ug/kg 05/04/17 18:02 11141-16-505/04/17 06:1840.8 18.5 1
PCB-1242 (Aroclor 1242)ND ug/kg 05/04/17 18:02 53469-21-905/04/17 06:1840.8 18.5 1
PCB-1248 (Aroclor 1248)ND ug/kg 05/04/17 18:02 12672-29-605/04/17 06:1840.8 18.5 1
PCB-1254 (Aroclor 1254)ND ug/kg 05/04/17 18:02 11097-69-105/04/17 06:1840.8 18.5 1
PCB-1260 (Aroclor 1260)ND ug/kg 05/04/17 18:02 11096-82-505/04/17 06:1840.8 18.5 1
Surrogates
Decachlorobiphenyl (S)58 %05/04/17 18:02 2051-24-305/04/17 06:1821-132 1
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Antimony ND mg/kg 05/10/17 11:51 7440-36-0 D305/05/17 10:052.1 1.6 5
Arsenic 2.8J mg/kg 05/10/17 11:51 7440-38-2 D305/05/17 10:054.2 2.1 5
Beryllium 0.42 mg/kg 05/10/17 11:51 7440-41-705/05/17 10:050.42 0.21 5
Cadmium ND mg/kg 05/10/17 11:51 7440-43-9 D305/05/17 10:050.42 0.21 5
Chromium 13.6 mg/kg 05/10/17 11:51 7440-47-305/05/17 10:052.1 1.0 5
Copper 39.3 mg/kg 05/10/17 11:51 7440-50-805/05/17 10:052.1 1.0 5
Lead 7.6 mg/kg 05/10/17 11:51 7439-92-105/05/17 10:052.1 1.0 5
Nickel 6.6 mg/kg 05/10/17 11:51 7440-02-005/05/17 10:052.1 1.0 5
Selenium 2.3J mg/kg 05/10/17 11:51 7782-49-2 D305/05/17 10:054.2 2.1 5
Silver ND mg/kg 05/10/17 11:51 7440-22-4 D305/05/17 10:052.1 1.0 5
Thallium ND mg/kg 05/10/17 11:51 7440-28-0 D305/05/17 10:054.2 2.1 5
Zinc 53.3 mg/kg 05/10/17 11:51 7440-66-605/05/17 10:054.2 2.1 5
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury ND mg/kg 05/10/17 11:28 7439-97-605/10/17 04:000.0044 0.0022 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 05/05/17 17:13 83-32-905/04/17 22:23408 94.0 1
Acenaphthylene ND ug/kg 05/05/17 17:13 208-96-805/04/17 22:23408 96.4 1
Aniline ND ug/kg 05/05/17 17:13 62-53-305/04/17 22:23408 110 1
Anthracene ND ug/kg 05/05/17 17:13 120-12-705/04/17 22:23408 91.5 1
Benzo(a)anthracene ND ug/kg 05/05/17 17:13 56-55-305/04/17 22:23408 75.4 1
Benzo(a)pyrene ND ug/kg 05/05/17 17:13 50-32-805/04/17 22:23408 77.9 1
Benzo(b)fluoranthene ND ug/kg 05/05/17 17:13 205-99-205/04/17 22:23408 70.5 1
Benzo(g,h,i)perylene ND ug/kg 05/05/17 17:13 191-24-205/04/17 22:23408 104 1
Benzo(k)fluoranthene ND ug/kg 05/05/17 17:13 207-08-905/04/17 22:23408 80.4 1
Benzoic Acid ND ug/kg 05/05/17 17:13 65-85-005/04/17 22:232040 74.2 1
Benzyl alcohol ND ug/kg 05/05/17 17:13 100-51-605/04/17 22:23816 81.6 1
4-Bromophenylphenyl ether ND ug/kg 05/05/17 17:13 101-55-305/04/17 22:23408 74.2 1
Butylbenzylphthalate ND ug/kg 05/05/17 17:13 85-68-705/04/17 22:23408 86.5 1
4-Chloro-3-methylphenol ND ug/kg 05/05/17 17:13 59-50-705/04/17 22:23816 84.1 1
4-Chloroaniline ND ug/kg 05/05/17 17:13 106-47-805/04/17 22:232040 114 1
bis(2-Chloroethoxy)methane ND ug/kg 05/05/17 17:13 111-91-105/04/17 22:23408 95.2 1
bis(2-Chloroethyl) ether ND ug/kg 05/05/17 17:13 111-44-405/04/17 22:23408 104 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 86
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339291
BANK STREET
Sample: SB-6(14-15)Lab ID: 92339291007 Collected: 05/02/17 12:30 Received: 05/03/17 10:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
2-Chloronaphthalene ND ug/kg 05/05/17 17:13 91-58-705/04/17 22:23408 80.4 1
2-Chlorophenol ND ug/kg 05/05/17 17:13 95-57-805/04/17 22:23408 111 1
4-Chlorophenylphenyl ether ND ug/kg 05/05/17 17:13 7005-72-305/04/17 22:23408 84.1 1
Chrysene ND ug/kg 05/05/17 17:13 218-01-905/04/17 22:23408 54.4 1
Dibenz(a,h)anthracene ND ug/kg 05/05/17 17:13 53-70-305/04/17 22:23408 86.5 1
Dibenzofuran ND ug/kg 05/05/17 17:13 132-64-905/04/17 22:23408 66.8 1
1,2-Dichlorobenzene ND ug/kg 05/05/17 17:13 95-50-105/04/17 22:23408 109 1
1,3-Dichlorobenzene ND ug/kg 05/05/17 17:13 541-73-1 L205/04/17 22:23408 92.7 1
1,4-Dichlorobenzene ND ug/kg 05/05/17 17:13 106-46-705/04/17 22:23408 115 1
3,3'-Dichlorobenzidine ND ug/kg 05/05/17 17:13 91-94-105/04/17 22:232040 89.0 1
2,4-Dichlorophenol ND ug/kg 05/05/17 17:13 120-83-205/04/17 22:23408 89.0 1
Diethylphthalate ND ug/kg 05/05/17 17:13 84-66-205/04/17 22:23408 63.1 1
2,4-Dimethylphenol ND ug/kg 05/05/17 17:13 105-67-905/04/17 22:23408 161 1
Dimethylphthalate ND ug/kg 05/05/17 17:13 131-11-305/04/17 22:23408 82.8 1
Di-n-butylphthalate ND ug/kg 05/05/17 17:13 84-74-205/04/17 22:23408 66.8 1
4,6-Dinitro-2-methylphenol ND ug/kg 05/05/17 17:13 534-52-105/04/17 22:23816 81.6 1
2,4-Dinitrophenol ND ug/kg 05/05/17 17:13 51-28-505/04/17 22:232040 66.8 1
2,4-Dinitrotoluene ND ug/kg 05/05/17 17:13 121-14-205/04/17 22:23408 76.7 1
2,6-Dinitrotoluene ND ug/kg 05/05/17 17:13 606-20-205/04/17 22:23408 85.3 1
Di-n-octylphthalate ND ug/kg 05/05/17 17:13 117-84-005/04/17 22:23408 85.3 1
bis(2-Ethylhexyl)phthalate ND ug/kg 05/05/17 17:13 117-81-705/04/17 22:23408 111 1
Fluoranthene ND ug/kg 05/05/17 17:13 206-44-005/04/17 22:23408 59.3 1
Fluorene ND ug/kg 05/05/17 17:13 86-73-705/04/17 22:23408 84.1 1
Hexachloro-1,3-butadiene ND ug/kg 05/05/17 17:13 87-68-305/04/17 22:23408 70.5 1
Hexachlorobenzene ND ug/kg 05/05/17 17:13 118-74-105/04/17 22:23408 51.9 1
Hexachlorocyclopentadiene ND ug/kg 05/05/17 17:13 77-47-405/04/17 22:23408 75.4 1
Hexachloroethane ND ug/kg 05/05/17 17:13 67-72-105/04/17 22:23408 108 1
Indeno(1,2,3-cd)pyrene ND ug/kg 05/05/17 17:13 193-39-505/04/17 22:23408 84.1 1
Isophorone ND ug/kg 05/05/17 17:13 78-59-105/04/17 22:23408 91.5 1
1-Methylnaphthalene ND ug/kg 05/05/17 17:13 90-12-005/04/17 22:23408 106 1
2-Methylnaphthalene ND ug/kg 05/05/17 17:13 91-57-605/04/17 22:23408 87.8 1
2-Methylphenol(o-Cresol)ND ug/kg 05/05/17 17:13 95-48-705/04/17 22:23408 124 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 05/05/17 17:13 15831-10-405/04/17 22:23408 161 1
Naphthalene ND ug/kg 05/05/17 17:13 91-20-305/04/17 22:23408 100 1
2-Nitroaniline ND ug/kg 05/05/17 17:13 88-74-405/04/17 22:232040 126 1
3-Nitroaniline ND ug/kg 05/05/17 17:13 99-09-205/04/17 22:232040 111 1
4-Nitroaniline ND ug/kg 05/05/17 17:13 100-01-605/04/17 22:23816 115 1
Nitrobenzene ND ug/kg 05/05/17 17:13 98-95-305/04/17 22:23408 111 1
2-Nitrophenol ND ug/kg 05/05/17 17:13 88-75-505/04/17 22:23408 98.9 1
4-Nitrophenol ND ug/kg 05/05/17 17:13 100-02-705/04/17 22:232040 72.9 1
N-Nitrosodimethylamine ND ug/kg 05/05/17 17:13 62-75-905/04/17 22:23408 132 1
N-Nitroso-di-n-propylamine ND ug/kg 05/05/17 17:13 621-64-705/04/17 22:23408 77.9 1
N-Nitrosodiphenylamine ND ug/kg 05/05/17 17:13 86-30-605/04/17 22:23408 121 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 05/05/17 17:13 108-60-105/04/17 22:23408 109 1
Pentachlorophenol ND ug/kg 05/05/17 17:13 87-86-505/04/17 22:232040 74.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 86
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339291
BANK STREET
Sample: SB-6(14-15)Lab ID: 92339291007 Collected: 05/02/17 12:30 Received: 05/03/17 10:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Phenanthrene ND ug/kg 05/05/17 17:13 85-01-805/04/17 22:23408 68.0 1
Phenol ND ug/kg 05/05/17 17:13 108-95-205/04/17 22:23408 122 1
Pyrene ND ug/kg 05/05/17 17:13 129-00-005/04/17 22:23408 69.2 1
1,2,4-Trichlorobenzene ND ug/kg 05/05/17 17:13 120-82-105/04/17 22:23408 79.1 1
2,4,5-Trichlorophenol ND ug/kg 05/05/17 17:13 95-95-405/04/17 22:23408 126 1
2,4,6-Trichlorophenol ND ug/kg 05/05/17 17:13 88-06-205/04/17 22:23408 90.2 1
Surrogates
Nitrobenzene-d5 (S)31 %05/05/17 17:13 4165-60-005/04/17 22:2323-110 1
2-Fluorobiphenyl (S)37 %05/05/17 17:13 321-60-805/04/17 22:2330-110 1
Terphenyl-d14 (S)47 %05/05/17 17:13 1718-51-005/04/17 22:2328-110 1
Phenol-d6 (S)33 %05/05/17 17:13 13127-88-305/04/17 22:2322-110 1
2-Fluorophenol (S)32 %05/05/17 17:13 367-12-405/04/17 22:2313-110 1
2,4,6-Tribromophenol (S)42 %05/05/17 17:13 118-79-605/04/17 22:2327-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone 39.8J ug/kg 05/05/17 16:06 67-64-1130 13.0 1
Benzene ND ug/kg 05/05/17 16:06 71-43-26.5 2.1 1
Bromobenzene ND ug/kg 05/05/17 16:06 108-86-16.5 2.6 1
Bromochloromethane ND ug/kg 05/05/17 16:06 74-97-56.5 2.2 1
Bromodichloromethane ND ug/kg 05/05/17 16:06 75-27-46.5 2.5 1
Bromoform ND ug/kg 05/05/17 16:06 75-25-26.5 3.0 1
Bromomethane ND ug/kg 05/05/17 16:06 74-83-913.0 3.3 1
2-Butanone (MEK)ND ug/kg 05/05/17 16:06 78-93-3130 3.8 1
n-Butylbenzene ND ug/kg 05/05/17 16:06 104-51-86.5 2.3 1
sec-Butylbenzene ND ug/kg 05/05/17 16:06 135-98-86.5 2.1 1
tert-Butylbenzene ND ug/kg 05/05/17 16:06 98-06-66.5 2.6 1
Carbon tetrachloride ND ug/kg 05/05/17 16:06 56-23-56.5 3.4 1
Chlorobenzene ND ug/kg 05/05/17 16:06 108-90-76.5 2.5 1
Chloroethane ND ug/kg 05/05/17 16:06 75-00-313.0 3.1 1
Chloroform ND ug/kg 05/05/17 16:06 67-66-36.5 2.1 1
Chloromethane ND ug/kg 05/05/17 16:06 74-87-313.0 3.1 1
2-Chlorotoluene ND ug/kg 05/05/17 16:06 95-49-86.5 2.2 1
4-Chlorotoluene ND ug/kg 05/05/17 16:06 106-43-46.5 2.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 05/05/17 16:06 96-12-86.5 4.7 1
Dibromochloromethane ND ug/kg 05/05/17 16:06 124-48-16.5 2.3 1
1,2-Dibromoethane (EDB)ND ug/kg 05/05/17 16:06 106-93-46.5 2.3 1
Dibromomethane ND ug/kg 05/05/17 16:06 74-95-36.5 3.3 1
1,2-Dichlorobenzene ND ug/kg 05/05/17 16:06 95-50-16.5 2.5 1
1,3-Dichlorobenzene ND ug/kg 05/05/17 16:06 541-73-16.5 2.6 1
1,4-Dichlorobenzene ND ug/kg 05/05/17 16:06 106-46-76.5 2.2 1
Dichlorodifluoromethane ND ug/kg 05/05/17 16:06 75-71-813.0 4.7 1
1,1-Dichloroethane ND ug/kg 05/05/17 16:06 75-34-36.5 2.0 1
1,2-Dichloroethane ND ug/kg 05/05/17 16:06 107-06-26.5 2.9 1
1,1-Dichloroethene ND ug/kg 05/05/17 16:06 75-35-46.5 2.3 1
cis-1,2-Dichloroethene ND ug/kg 05/05/17 16:06 156-59-26.5 1.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 86
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339291
BANK STREET
Sample: SB-6(14-15)Lab ID: 92339291007 Collected: 05/02/17 12:30 Received: 05/03/17 10:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
trans-1,2-Dichloroethene ND ug/kg 05/05/17 16:06 156-60-56.5 2.5 1
1,2-Dichloropropane ND ug/kg 05/05/17 16:06 78-87-56.5 2.2 1
1,3-Dichloropropane ND ug/kg 05/05/17 16:06 142-28-96.5 2.5 1
2,2-Dichloropropane ND ug/kg 05/05/17 16:06 594-20-76.5 2.2 1
1,1-Dichloropropene ND ug/kg 05/05/17 16:06 563-58-66.5 2.0 1
cis-1,3-Dichloropropene ND ug/kg 05/05/17 16:06 10061-01-56.5 2.3 1
trans-1,3-Dichloropropene ND ug/kg 05/05/17 16:06 10061-02-66.5 2.0 1
Diisopropyl ether ND ug/kg 05/05/17 16:06 108-20-36.5 2.2 1
Ethylbenzene ND ug/kg 05/05/17 16:06 100-41-46.5 2.3 1
Hexachloro-1,3-butadiene ND ug/kg 05/05/17 16:06 87-68-36.5 2.6 1
2-Hexanone ND ug/kg 05/05/17 16:06 591-78-665.1 5.1 1
Isopropylbenzene (Cumene)ND ug/kg 05/05/17 16:06 98-82-86.5 2.5 1
p-Isopropyltoluene ND ug/kg 05/05/17 16:06 99-87-66.5 2.2 1
Methylene Chloride ND ug/kg 05/05/17 16:06 75-09-226.0 3.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 05/05/17 16:06 108-10-165.1 4.8 1
Methyl-tert-butyl ether ND ug/kg 05/05/17 16:06 1634-04-46.5 2.0 1
Naphthalene ND ug/kg 05/05/17 16:06 91-20-36.5 1.6 1
n-Propylbenzene ND ug/kg 05/05/17 16:06 103-65-16.5 2.2 1
Styrene ND ug/kg 05/05/17 16:06 100-42-56.5 2.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 05/05/17 16:06 630-20-66.5 2.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 05/05/17 16:06 79-34-56.5 2.5 1
Tetrachloroethene ND ug/kg 05/05/17 16:06 127-18-46.5 2.2 1
Toluene 5.2J ug/kg 05/05/17 16:06 108-88-36.5 2.3 1
1,2,3-Trichlorobenzene ND ug/kg 05/05/17 16:06 87-61-66.5 2.9 1
1,2,4-Trichlorobenzene ND ug/kg 05/05/17 16:06 120-82-16.5 2.1 1
1,1,1-Trichloroethane ND ug/kg 05/05/17 16:06 71-55-66.5 2.3 1
1,1,2-Trichloroethane ND ug/kg 05/05/17 16:06 79-00-56.5 2.7 1
Trichloroethene ND ug/kg 05/05/17 16:06 79-01-66.5 2.7 1
Trichlorofluoromethane ND ug/kg 05/05/17 16:06 75-69-46.5 2.9 1
1,2,3-Trichloropropane ND ug/kg 05/05/17 16:06 96-18-46.5 2.1 1
1,2,4-Trimethylbenzene ND ug/kg 05/05/17 16:06 95-63-66.5 2.6 1
1,3,5-Trimethylbenzene ND ug/kg 05/05/17 16:06 108-67-86.5 2.3 1
Vinyl acetate ND ug/kg 05/05/17 16:06 108-05-465.1 11.5 1
Vinyl chloride ND ug/kg 05/05/17 16:06 75-01-413.0 2.3 1
Xylene (Total)ND ug/kg 05/05/17 16:06 1330-20-713.0 4.7 1
m&p-Xylene ND ug/kg 05/05/17 16:06 179601-23-113.0 4.7 1
o-Xylene ND ug/kg 05/05/17 16:06 95-47-66.5 2.5 1
Surrogates
Toluene-d8 (S)101 %05/05/17 16:06 2037-26-570-130 1
4-Bromofluorobenzene (S)99 %05/05/17 16:06 460-00-470-130 1
1,2-Dichloroethane-d4 (S)125 %05/05/17 16:06 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 19.1 %05/04/17 17:410.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 86
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339291
BANK STREET
Sample: SB-7(3-5)Lab ID: 92339291008 Collected: 05/02/17 13:15 Received: 05/03/17 10:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8082 Preparation Method: EPA 35468082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/kg 05/04/17 18:23 12674-11-205/04/17 06:1839.6 18.0 1
PCB-1221 (Aroclor 1221)ND ug/kg 05/04/17 18:23 11104-28-205/04/17 06:1839.6 18.0 1
PCB-1232 (Aroclor 1232)ND ug/kg 05/04/17 18:23 11141-16-505/04/17 06:1839.6 18.0 1
PCB-1242 (Aroclor 1242)ND ug/kg 05/04/17 18:23 53469-21-905/04/17 06:1839.6 18.0 1
PCB-1248 (Aroclor 1248)ND ug/kg 05/04/17 18:23 12672-29-605/04/17 06:1839.6 18.0 1
PCB-1254 (Aroclor 1254)ND ug/kg 05/04/17 18:23 11097-69-105/04/17 06:1839.6 18.0 1
PCB-1260 (Aroclor 1260)ND ug/kg 05/04/17 18:23 11096-82-505/04/17 06:1839.6 18.0 1
Surrogates
Decachlorobiphenyl (S)69 %05/04/17 18:23 2051-24-305/04/17 06:1821-132 1
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Antimony ND mg/kg 05/09/17 21:45 7440-36-005/05/17 10:050.43 0.33 1
Arsenic 1.4 mg/kg 05/09/17 21:45 7440-38-205/05/17 10:050.86 0.43 1
Beryllium 0.41 mg/kg 05/09/17 21:45 7440-41-705/05/17 10:050.086 0.043 1
Cadmium ND mg/kg 05/09/17 21:45 7440-43-905/05/17 10:050.086 0.043 1
Chromium 18.4 mg/kg 05/09/17 21:45 7440-47-305/05/17 10:050.43 0.21 1
Copper 34.1 mg/kg 05/09/17 21:45 7440-50-805/05/17 10:050.43 0.21 1
Lead 16.9 mg/kg 05/09/17 21:45 7439-92-105/05/17 10:050.43 0.21 1
Nickel 25.0 mg/kg 05/09/17 21:45 7440-02-005/05/17 10:050.43 0.21 1
Selenium 1.1 mg/kg 05/09/17 21:45 7782-49-205/05/17 10:050.86 0.43 1
Silver ND mg/kg 05/09/17 21:45 7440-22-405/05/17 10:050.43 0.21 1
Thallium ND mg/kg 05/09/17 21:45 7440-28-005/05/17 10:050.86 0.43 1
Zinc 33.5 mg/kg 05/09/17 21:45 7440-66-605/05/17 10:050.86 0.43 1
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury 0.0050J mg/kg 05/10/17 11:31 7439-97-605/10/17 04:000.0065 0.0033 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 05/05/17 17:42 83-32-905/04/17 22:23396 91.2 1
Acenaphthylene ND ug/kg 05/05/17 17:42 208-96-805/04/17 22:23396 93.6 1
Aniline ND ug/kg 05/05/17 17:42 62-53-305/04/17 22:23396 107 1
Anthracene ND ug/kg 05/05/17 17:42 120-12-705/04/17 22:23396 88.8 1
Benzo(a)anthracene ND ug/kg 05/05/17 17:42 56-55-305/04/17 22:23396 73.2 1
Benzo(a)pyrene ND ug/kg 05/05/17 17:42 50-32-805/04/17 22:23396 75.6 1
Benzo(b)fluoranthene ND ug/kg 05/05/17 17:42 205-99-205/04/17 22:23396 68.4 1
Benzo(g,h,i)perylene ND ug/kg 05/05/17 17:42 191-24-205/04/17 22:23396 101 1
Benzo(k)fluoranthene ND ug/kg 05/05/17 17:42 207-08-905/04/17 22:23396 78.0 1
Benzoic Acid ND ug/kg 05/05/17 17:42 65-85-005/04/17 22:231980 72.0 1
Benzyl alcohol ND ug/kg 05/05/17 17:42 100-51-605/04/17 22:23792 79.2 1
4-Bromophenylphenyl ether ND ug/kg 05/05/17 17:42 101-55-305/04/17 22:23396 72.0 1
Butylbenzylphthalate ND ug/kg 05/05/17 17:42 85-68-705/04/17 22:23396 84.0 1
4-Chloro-3-methylphenol ND ug/kg 05/05/17 17:42 59-50-705/04/17 22:23792 81.6 1
4-Chloroaniline ND ug/kg 05/05/17 17:42 106-47-805/04/17 22:231980 110 1
bis(2-Chloroethoxy)methane ND ug/kg 05/05/17 17:42 111-91-105/04/17 22:23396 92.4 1
bis(2-Chloroethyl) ether ND ug/kg 05/05/17 17:42 111-44-405/04/17 22:23396 101 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 86
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339291
BANK STREET
Sample: SB-7(3-5)Lab ID: 92339291008 Collected: 05/02/17 13:15 Received: 05/03/17 10:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
2-Chloronaphthalene ND ug/kg 05/05/17 17:42 91-58-705/04/17 22:23396 78.0 1
2-Chlorophenol ND ug/kg 05/05/17 17:42 95-57-805/04/17 22:23396 108 1
4-Chlorophenylphenyl ether ND ug/kg 05/05/17 17:42 7005-72-305/04/17 22:23396 81.6 1
Chrysene ND ug/kg 05/05/17 17:42 218-01-905/04/17 22:23396 52.8 1
Dibenz(a,h)anthracene ND ug/kg 05/05/17 17:42 53-70-305/04/17 22:23396 84.0 1
Dibenzofuran ND ug/kg 05/05/17 17:42 132-64-905/04/17 22:23396 64.8 1
1,2-Dichlorobenzene ND ug/kg 05/05/17 17:42 95-50-105/04/17 22:23396 106 1
1,3-Dichlorobenzene ND ug/kg 05/05/17 17:42 541-73-1 L205/04/17 22:23396 90.0 1
1,4-Dichlorobenzene ND ug/kg 05/05/17 17:42 106-46-705/04/17 22:23396 112 1
3,3'-Dichlorobenzidine ND ug/kg 05/05/17 17:42 91-94-105/04/17 22:231980 86.4 1
2,4-Dichlorophenol ND ug/kg 05/05/17 17:42 120-83-205/04/17 22:23396 86.4 1
Diethylphthalate ND ug/kg 05/05/17 17:42 84-66-205/04/17 22:23396 61.2 1
2,4-Dimethylphenol ND ug/kg 05/05/17 17:42 105-67-905/04/17 22:23396 156 1
Dimethylphthalate ND ug/kg 05/05/17 17:42 131-11-305/04/17 22:23396 80.4 1
Di-n-butylphthalate ND ug/kg 05/05/17 17:42 84-74-205/04/17 22:23396 64.8 1
4,6-Dinitro-2-methylphenol ND ug/kg 05/05/17 17:42 534-52-105/04/17 22:23792 79.2 1
2,4-Dinitrophenol ND ug/kg 05/05/17 17:42 51-28-505/04/17 22:231980 64.8 1
2,4-Dinitrotoluene ND ug/kg 05/05/17 17:42 121-14-205/04/17 22:23396 74.4 1
2,6-Dinitrotoluene ND ug/kg 05/05/17 17:42 606-20-205/04/17 22:23396 82.8 1
Di-n-octylphthalate ND ug/kg 05/05/17 17:42 117-84-005/04/17 22:23396 82.8 1
bis(2-Ethylhexyl)phthalate ND ug/kg 05/05/17 17:42 117-81-705/04/17 22:23396 108 1
Fluoranthene ND ug/kg 05/05/17 17:42 206-44-005/04/17 22:23396 57.6 1
Fluorene ND ug/kg 05/05/17 17:42 86-73-705/04/17 22:23396 81.6 1
Hexachloro-1,3-butadiene ND ug/kg 05/05/17 17:42 87-68-305/04/17 22:23396 68.4 1
Hexachlorobenzene ND ug/kg 05/05/17 17:42 118-74-105/04/17 22:23396 50.4 1
Hexachlorocyclopentadiene ND ug/kg 05/05/17 17:42 77-47-405/04/17 22:23396 73.2 1
Hexachloroethane ND ug/kg 05/05/17 17:42 67-72-105/04/17 22:23396 104 1
Indeno(1,2,3-cd)pyrene ND ug/kg 05/05/17 17:42 193-39-505/04/17 22:23396 81.6 1
Isophorone ND ug/kg 05/05/17 17:42 78-59-105/04/17 22:23396 88.8 1
1-Methylnaphthalene ND ug/kg 05/05/17 17:42 90-12-005/04/17 22:23396 103 1
2-Methylnaphthalene ND ug/kg 05/05/17 17:42 91-57-605/04/17 22:23396 85.2 1
2-Methylphenol(o-Cresol)ND ug/kg 05/05/17 17:42 95-48-705/04/17 22:23396 120 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 05/05/17 17:42 15831-10-405/04/17 22:23396 156 1
Naphthalene ND ug/kg 05/05/17 17:42 91-20-305/04/17 22:23396 97.2 1
2-Nitroaniline ND ug/kg 05/05/17 17:42 88-74-405/04/17 22:231980 122 1
3-Nitroaniline ND ug/kg 05/05/17 17:42 99-09-205/04/17 22:231980 108 1
4-Nitroaniline ND ug/kg 05/05/17 17:42 100-01-605/04/17 22:23792 112 1
Nitrobenzene ND ug/kg 05/05/17 17:42 98-95-305/04/17 22:23396 108 1
2-Nitrophenol ND ug/kg 05/05/17 17:42 88-75-505/04/17 22:23396 96.0 1
4-Nitrophenol ND ug/kg 05/05/17 17:42 100-02-705/04/17 22:231980 70.8 1
N-Nitrosodimethylamine ND ug/kg 05/05/17 17:42 62-75-905/04/17 22:23396 128 1
N-Nitroso-di-n-propylamine ND ug/kg 05/05/17 17:42 621-64-705/04/17 22:23396 75.6 1
N-Nitrosodiphenylamine ND ug/kg 05/05/17 17:42 86-30-605/04/17 22:23396 118 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 05/05/17 17:42 108-60-105/04/17 22:23396 106 1
Pentachlorophenol ND ug/kg 05/05/17 17:42 87-86-505/04/17 22:231980 72.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 86
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339291
BANK STREET
Sample: SB-7(3-5)Lab ID: 92339291008 Collected: 05/02/17 13:15 Received: 05/03/17 10:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Phenanthrene ND ug/kg 05/05/17 17:42 85-01-805/04/17 22:23396 66.0 1
Phenol ND ug/kg 05/05/17 17:42 108-95-205/04/17 22:23396 119 1
Pyrene ND ug/kg 05/05/17 17:42 129-00-005/04/17 22:23396 67.2 1
1,2,4-Trichlorobenzene ND ug/kg 05/05/17 17:42 120-82-105/04/17 22:23396 76.8 1
2,4,5-Trichlorophenol ND ug/kg 05/05/17 17:42 95-95-405/04/17 22:23396 122 1
2,4,6-Trichlorophenol ND ug/kg 05/05/17 17:42 88-06-205/04/17 22:23396 87.6 1
Surrogates
Nitrobenzene-d5 (S)35 %05/05/17 17:42 4165-60-005/04/17 22:2323-110 1
2-Fluorobiphenyl (S)35 %05/05/17 17:42 321-60-805/04/17 22:2330-110 1
Terphenyl-d14 (S)43 %05/05/17 17:42 1718-51-005/04/17 22:2328-110 1
Phenol-d6 (S)24 %05/05/17 17:42 13127-88-305/04/17 22:2322-110 1
2-Fluorophenol (S)22 %05/05/17 17:42 367-12-405/04/17 22:2313-110 1
2,4,6-Tribromophenol (S)27 %05/05/17 17:42 118-79-605/04/17 22:2327-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone 36.8J ug/kg 05/05/17 16:26 67-64-1127 12.7 1
Benzene ND ug/kg 05/05/17 16:26 71-43-26.3 2.0 1
Bromobenzene ND ug/kg 05/05/17 16:26 108-86-16.3 2.5 1
Bromochloromethane ND ug/kg 05/05/17 16:26 74-97-56.3 2.2 1
Bromodichloromethane ND ug/kg 05/05/17 16:26 75-27-46.3 2.4 1
Bromoform ND ug/kg 05/05/17 16:26 75-25-26.3 2.9 1
Bromomethane ND ug/kg 05/05/17 16:26 74-83-912.7 3.2 1
2-Butanone (MEK)ND ug/kg 05/05/17 16:26 78-93-3127 3.7 1
n-Butylbenzene ND ug/kg 05/05/17 16:26 104-51-86.3 2.3 1
sec-Butylbenzene ND ug/kg 05/05/17 16:26 135-98-86.3 2.0 1
tert-Butylbenzene ND ug/kg 05/05/17 16:26 98-06-66.3 2.5 1
Carbon tetrachloride ND ug/kg 05/05/17 16:26 56-23-56.3 3.3 1
Chlorobenzene ND ug/kg 05/05/17 16:26 108-90-76.3 2.4 1
Chloroethane ND ug/kg 05/05/17 16:26 75-00-312.7 3.0 1
Chloroform ND ug/kg 05/05/17 16:26 67-66-36.3 2.0 1
Chloromethane ND ug/kg 05/05/17 16:26 74-87-312.7 3.0 1
2-Chlorotoluene ND ug/kg 05/05/17 16:26 95-49-86.3 2.2 1
4-Chlorotoluene ND ug/kg 05/05/17 16:26 106-43-46.3 2.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 05/05/17 16:26 96-12-86.3 4.6 1
Dibromochloromethane ND ug/kg 05/05/17 16:26 124-48-16.3 2.3 1
1,2-Dibromoethane (EDB)ND ug/kg 05/05/17 16:26 106-93-46.3 2.3 1
Dibromomethane ND ug/kg 05/05/17 16:26 74-95-36.3 3.2 1
1,2-Dichlorobenzene ND ug/kg 05/05/17 16:26 95-50-16.3 2.4 1
1,3-Dichlorobenzene ND ug/kg 05/05/17 16:26 541-73-16.3 2.5 1
1,4-Dichlorobenzene ND ug/kg 05/05/17 16:26 106-46-76.3 2.2 1
Dichlorodifluoromethane ND ug/kg 05/05/17 16:26 75-71-812.7 4.6 1
1,1-Dichloroethane ND ug/kg 05/05/17 16:26 75-34-36.3 1.9 1
1,2-Dichloroethane ND ug/kg 05/05/17 16:26 107-06-26.3 2.8 1
1,1-Dichloroethene ND ug/kg 05/05/17 16:26 75-35-46.3 2.3 1
cis-1,2-Dichloroethene ND ug/kg 05/05/17 16:26 156-59-26.3 1.8 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
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Page 36 of 86
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339291
BANK STREET
Sample: SB-7(3-5)Lab ID: 92339291008 Collected: 05/02/17 13:15 Received: 05/03/17 10:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
trans-1,2-Dichloroethene ND ug/kg 05/05/17 16:26 156-60-56.3 2.4 1
1,2-Dichloropropane ND ug/kg 05/05/17 16:26 78-87-56.3 2.2 1
1,3-Dichloropropane ND ug/kg 05/05/17 16:26 142-28-96.3 2.4 1
2,2-Dichloropropane ND ug/kg 05/05/17 16:26 594-20-76.3 2.2 1
1,1-Dichloropropene ND ug/kg 05/05/17 16:26 563-58-66.3 1.9 1
cis-1,3-Dichloropropene ND ug/kg 05/05/17 16:26 10061-01-56.3 2.3 1
trans-1,3-Dichloropropene ND ug/kg 05/05/17 16:26 10061-02-66.3 1.9 1
Diisopropyl ether ND ug/kg 05/05/17 16:26 108-20-36.3 2.2 1
Ethylbenzene ND ug/kg 05/05/17 16:26 100-41-46.3 2.3 1
Hexachloro-1,3-butadiene ND ug/kg 05/05/17 16:26 87-68-36.3 2.5 1
2-Hexanone ND ug/kg 05/05/17 16:26 591-78-663.3 4.9 1
Isopropylbenzene (Cumene)ND ug/kg 05/05/17 16:26 98-82-86.3 2.4 1
p-Isopropyltoluene ND ug/kg 05/05/17 16:26 99-87-66.3 2.2 1
Methylene Chloride ND ug/kg 05/05/17 16:26 75-09-225.3 3.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 05/05/17 16:26 108-10-163.3 4.7 1
Methyl-tert-butyl ether ND ug/kg 05/05/17 16:26 1634-04-46.3 1.9 1
Naphthalene ND ug/kg 05/05/17 16:26 91-20-36.3 1.5 1
n-Propylbenzene ND ug/kg 05/05/17 16:26 103-65-16.3 2.2 1
Styrene ND ug/kg 05/05/17 16:26 100-42-56.3 2.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 05/05/17 16:26 630-20-66.3 2.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 05/05/17 16:26 79-34-56.3 2.4 1
Tetrachloroethene ND ug/kg 05/05/17 16:26 127-18-46.3 2.2 1
Toluene 4.7J ug/kg 05/05/17 16:26 108-88-36.3 2.3 1
1,2,3-Trichlorobenzene ND ug/kg 05/05/17 16:26 87-61-66.3 2.8 1
1,2,4-Trichlorobenzene ND ug/kg 05/05/17 16:26 120-82-16.3 2.0 1
1,1,1-Trichloroethane ND ug/kg 05/05/17 16:26 71-55-66.3 2.3 1
1,1,2-Trichloroethane ND ug/kg 05/05/17 16:26 79-00-56.3 2.7 1
Trichloroethene ND ug/kg 05/05/17 16:26 79-01-66.3 2.7 1
Trichlorofluoromethane ND ug/kg 05/05/17 16:26 75-69-46.3 2.8 1
1,2,3-Trichloropropane ND ug/kg 05/05/17 16:26 96-18-46.3 2.0 1
1,2,4-Trimethylbenzene ND ug/kg 05/05/17 16:26 95-63-66.3 2.5 1
1,3,5-Trimethylbenzene ND ug/kg 05/05/17 16:26 108-67-86.3 2.3 1
Vinyl acetate ND ug/kg 05/05/17 16:26 108-05-463.3 11.1 1
Vinyl chloride ND ug/kg 05/05/17 16:26 75-01-412.7 2.3 1
Xylene (Total)ND ug/kg 05/05/17 16:26 1330-20-712.7 4.6 1
m&p-Xylene ND ug/kg 05/05/17 16:26 179601-23-112.7 4.6 1
o-Xylene ND ug/kg 05/05/17 16:26 95-47-66.3 2.4 1
Surrogates
Toluene-d8 (S)102 %05/05/17 16:26 2037-26-570-130 1
4-Bromofluorobenzene (S)97 %05/05/17 16:26 460-00-470-130 1
1,2-Dichloroethane-d4 (S)117 %05/05/17 16:26 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 16.7 %05/04/17 17:410.10 0.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 37 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
359271
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples: 92339291001, 92339291002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1992679
Associated Lab Samples:92339291001, 92339291002
Matrix: Water
AnalyzedMDL
Mercury ug/L ND 0.20 05/09/17 10:570.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1992680LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.52.5 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1992681MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92339121007
1992682
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 79 75-12582 3 252.5ND 2.0 2.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
359272
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples: 92339291003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1992683
Associated Lab Samples:92339291003
Matrix: Water
AnalyzedMDL
Mercury ug/L ND 0.20 05/05/17 11:530.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1992684LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.42.5 97 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1992685MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92339291003
1992686
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 92 75-12590 2 252.5ND 2.3 2.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
359634
EPA 7471
EPA 7471
7471 Mercury
Associated Lab Samples: 92339291004, 92339291005, 92339291006, 92339291007, 92339291008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1994487
Associated Lab Samples:92339291004, 92339291005, 92339291006, 92339291007, 92339291008
Matrix: Solid
AnalyzedMDL
Mercury mg/kg ND 0.0060 05/10/17 10:550.0030
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1994488LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.080.083 96 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1994489MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92339249001
1994490
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg .052 96 75-12586 19 20.048ND 0.050 0.041
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
359181
EPA 3050
EPA 6010
6010 MET
Associated Lab Samples: 92339291004, 92339291005, 92339291006, 92339291007, 92339291008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1991978
Associated Lab Samples:92339291004, 92339291005, 92339291006, 92339291007, 92339291008
Matrix: Solid
AnalyzedMDL
Antimony mg/kg ND 0.50 05/09/17 20:550.39
Arsenic mg/kg ND 1.0 05/09/17 20:550.50
Beryllium mg/kg ND 0.10 05/09/17 20:550.050
Cadmium mg/kg ND 0.10 05/09/17 20:550.050
Chromium mg/kg ND 0.50 05/09/17 20:550.25
Copper mg/kg ND 0.50 05/09/17 20:550.25
Lead mg/kg ND 0.50 05/09/17 20:550.25
Nickel mg/kg ND 0.50 05/09/17 20:550.25
Selenium mg/kg ND 1.0 05/10/17 11:290.50
Silver mg/kg ND 0.50 05/09/17 20:550.25
Thallium mg/kg ND 1.0 05/09/17 20:550.50
Zinc mg/kg 0.64J 1.0 05/09/17 20:550.50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1991979LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony mg/kg 46.050 92 80-120
Arsenic mg/kg 45.850 92 80-120
Beryllium mg/kg 53.850 108 80-120
Cadmium mg/kg 48.850 98 80-120
Chromium mg/kg 52.350 105 80-120
Copper mg/kg 50.450 101 80-120
Lead mg/kg 47.750 95 80-120
Nickel mg/kg 48.750 97 80-120
Selenium mg/kg 51.450 103 80-120
Silver mg/kg 24.325 97 80-120
Thallium mg/kg 49.450 99 80-120
Zinc mg/kg 50.050 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1991980MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92339249001
1991981
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony mg/kg M140.3 69 75-12561 14 2039.7ND 28.0 24.4
Arsenic mg/kg M140.3 82 75-12572 14 2039.7ND 33.1 28.6
Beryllium mg/kg 40.3 93 75-12583 13 2039.7ND 37.6 33.1
Cadmium mg/kg 40.3 87 75-12579 12 2039.7ND 35.2 31.2
Chromium mg/kg 40.3 91 75-12580 14 2039.70.598 ug/g 37.3 32.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1991980MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92339249001
1991981
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Copper mg/kg 40.3 88 75-12579 12 2039.71.44 ug/g 37.1 32.7
Lead mg/kg 40.3 83 75-12576 10 2039.70.291 ug/g 33.8 30.6
Nickel mg/kg M140.3 81 75-12574 10 2039.70.902 ug/g 33.6 30.3
Selenium mg/kg 40.3 100 75-12596 6 2039.7ND 40.4 38.1
Silver mg/kg 20.2 90 75-12584 9 2019.8ND 18.3 16.7
Thallium mg/kg 40.3 86 75-12581 7 2039.7ND 34.5 32.3
Zinc mg/kg M140.3 -5 75-125-38 20 2039.773.8 ug/g 71.9 58.5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
359154
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples: 92339291001, 92339291002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1991818
Associated Lab Samples:92339291001, 92339291002
Matrix: Water
AnalyzedMDL
Antimony ug/L ND 5.0 05/07/17 01:493.9
Arsenic ug/L ND 10.0 05/07/17 01:495.0
Beryllium ug/L ND 1.0 05/07/17 01:490.50
Cadmium ug/L ND 1.0 05/07/17 01:490.50
Chromium ug/L ND 5.0 05/07/17 01:492.5
Copper ug/L ND 5.0 05/07/17 01:492.5
Iron ug/L ND 50.0 05/07/17 01:4925.0
Nickel ug/L ND 5.0 05/07/17 01:492.5
Selenium ug/L ND 10.0 05/07/17 01:495.0
Silver ug/L ND 5.0 05/07/17 01:492.5
Thallium ug/L ND 10.0 05/07/17 01:495.0
Zinc ug/L ND 10.0 05/07/17 01:495.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1991819LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 509500 102 80-120
Arsenic ug/L 515500 103 80-120
Beryllium ug/L 501500 100 80-120
Cadmium ug/L 506500 101 80-120
Chromium ug/L 478500 96 80-120
Copper ug/L 516500 103 80-120
Iron ug/L 49005000 98 80-120
Nickel ug/L 491500 98 80-120
Selenium ug/L 524500 105 80-120
Silver ug/L 248250 99 80-120
Thallium ug/L 492500 98 80-120
Zinc ug/L 519500 104 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1991820MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92339121007
1991821
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 99 75-125100 1 20500ND499 502
Arsenic ug/L 500 101 75-125102 1 20500ND503 510
Beryllium ug/L 500 100 75-125101 0 205000.75J 503 503
Cadmium ug/L 500 100 75-125100 0 20500ND498 500
Chromium ug/L 500 95 75-12595 0 20500ND476 475
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1991820MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92339121007
1991821
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Copper ug/L 500 102 75-125104 2 20500ND511 523
Iron ug/L 5000 93 75-12595 1 205000769012400 12400
Nickel ug/L 500 95 75-12595 0 205003.2J 480 480
Selenium ug/L 500 103 75-125103 0 20500ND514 513
Silver ug/L 250 98 75-12599 2 20250ND245 249
Thallium ug/L 500 96 75-12596 1 20500ND480 484
Zinc ug/L 500 101 75-125101 0 205006.1J 509 509
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
359157
EPA 3010A
EPA 6010
6010 MET
Associated Lab Samples: 92339291003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1991833
Associated Lab Samples:92339291003
Matrix: Water
AnalyzedMDL
Antimony ug/L ND 5.0 05/09/17 14:333.9
Arsenic ug/L ND 10.0 05/09/17 14:335.0
Beryllium ug/L ND 1.0 05/09/17 14:330.50
Cadmium ug/L ND 1.0 05/09/17 14:330.50
Chromium ug/L ND 5.0 05/09/17 14:332.5
Copper ug/L ND 5.0 05/09/17 14:332.5
Iron ug/L ND 50.0 05/09/17 14:3325.0
Nickel ug/L ND 5.0 05/09/17 14:332.5
Selenium ug/L ND 10.0 05/09/17 14:335.0
Silver ug/L ND 5.0 05/09/17 14:332.5
Thallium ug/L ND 10.0 05/09/17 14:335.0
Zinc ug/L ND 10.0 05/09/17 14:335.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1991834LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 462500 92 80-120
Arsenic ug/L 464500 93 80-120
Beryllium ug/L 508500 102 80-120
Cadmium ug/L 484500 97 80-120
Chromium ug/L 503500 101 80-120
Copper ug/L 495500 99 80-120
Iron ug/L 48705000 97 80-120
Nickel ug/L 479500 96 80-120
Selenium ug/L 482500 96 80-120
Silver ug/L 242250 97 80-120
Thallium ug/L 479500 96 80-120
Zinc ug/L 493500 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1991835MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92339291003
1991836
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 92 75-12593 1 20500ND464 467
Arsenic ug/L 500 93 75-12592 0 20500ND464 463
Beryllium ug/L 500 105 75-125105 0 20500ND524 523
Cadmium ug/L 500 98 75-12598 0 20500ND488 489
Chromium ug/L 500 102 75-125101 2 20500ND514 506
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1991835MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92339291003
1991836
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Copper ug/L 500 103 75-125103 1 205008.3 521 524
Iron ug/L 5000 106 75-125104 2 20500028408150 8020
Nickel ug/L 500 96 75-12595 1 205002.5J 482 480
Selenium ug/L 500 96 75-12598 1 20500ND482 488
Silver ug/L 250 98 75-12598 1 20250ND246 245
Thallium ug/L 500 99 75-12597 1 20500ND493 487
Zinc ug/L 500 99 75-12597 2 205008.1J 502 491
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
359430
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples: 92339291001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1993551
Associated Lab Samples:92339291001
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 05/06/17 01:570.33
1,1,1-Trichloroethane ug/L ND 1.0 05/06/17 01:570.48
1,1,2,2-Tetrachloroethane ug/L ND 1.0 05/06/17 01:570.40
1,1,2-Trichloroethane ug/L ND 1.0 05/06/17 01:570.29
1,1-Dichloroethane ug/L ND 1.0 05/06/17 01:570.32
1,1-Dichloroethene ug/L ND 1.0 05/06/17 01:570.56
1,1-Dichloropropene ug/L ND 1.0 05/06/17 01:570.49
1,2,3-Trichlorobenzene ug/L ND 1.0 05/06/17 01:570.33
1,2,3-Trichloropropane ug/L ND 1.0 05/06/17 01:570.41
1,2,4-Trichlorobenzene ug/L ND 1.0 05/06/17 01:570.35
1,2-Dibromo-3-chloropropane ug/L ND 2.0 05/06/17 01:572.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 05/06/17 01:570.27
1,2-Dichlorobenzene ug/L ND 1.0 05/06/17 01:570.30
1,2-Dichloroethane ug/L ND 1.0 05/06/17 01:570.24
1,2-Dichloropropane ug/L ND 1.0 05/06/17 01:570.27
1,3-Dichlorobenzene ug/L ND 1.0 05/06/17 01:570.24
1,3-Dichloropropane ug/L ND 1.0 05/06/17 01:570.28
1,4-Dichlorobenzene ug/L ND 1.0 05/06/17 01:570.33
2,2-Dichloropropane ug/L ND 1.0 05/06/17 01:570.13
2-Butanone (MEK)ug/L ND 5.0 05/06/17 01:570.96
2-Chlorotoluene ug/L ND 1.0 05/06/17 01:570.35
2-Hexanone ug/L ND 5.0 05/06/17 01:570.46
4-Chlorotoluene ug/L ND 1.0 05/06/17 01:570.31
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 05/06/17 01:570.33
Acetone ug/L ND 25.0 05/06/17 01:5710.0
Benzene ug/L ND 1.0 05/06/17 01:570.25
Bromobenzene ug/L ND 1.0 05/06/17 01:570.30
Bromochloromethane ug/L ND 1.0 05/06/17 01:570.17
Bromodichloromethane ug/L ND 1.0 05/06/17 01:570.18
Bromoform ug/L ND 1.0 05/06/17 01:570.26
Bromomethane ug/L ND 2.0 05/06/17 01:570.29
Carbon tetrachloride ug/L ND 1.0 05/06/17 01:570.25
Chlorobenzene ug/L ND 1.0 05/06/17 01:570.23
Chloroethane ug/L ND 1.0 05/06/17 01:570.54
Chloroform ug/L ND 1.0 05/06/17 01:570.14
Chloromethane ug/L ND 1.0 05/06/17 01:570.11
cis-1,2-Dichloroethene ug/L ND 1.0 05/06/17 01:570.19
cis-1,3-Dichloropropene ug/L ND 1.0 05/06/17 01:570.13
Dibromochloromethane ug/L ND 1.0 05/06/17 01:570.21
Dibromomethane ug/L ND 1.0 05/06/17 01:570.21
Dichlorodifluoromethane ug/L ND 1.0 05/06/17 01:570.21
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
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Page 47 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1993551
Associated Lab Samples:92339291001
Matrix: Water
AnalyzedMDL
Diisopropyl ether ug/L ND 1.0 05/06/17 01:570.12
Ethylbenzene ug/L ND 1.0 05/06/17 01:570.30
Hexachloro-1,3-butadiene ug/L ND 1.0 05/06/17 01:570.71
m&p-Xylene ug/L ND 2.0 05/06/17 01:570.66
Methyl-tert-butyl ether ug/L ND 1.0 05/06/17 01:570.21
Methylene Chloride ug/L ND 2.0 05/06/17 01:570.97
Naphthalene ug/L ND 1.0 05/06/17 01:570.24
o-Xylene ug/L ND 1.0 05/06/17 01:570.23
p-Isopropyltoluene ug/L ND 1.0 05/06/17 01:570.31
Styrene ug/L ND 1.0 05/06/17 01:570.26
Tetrachloroethene ug/L ND 1.0 05/06/17 01:570.46
Toluene ug/L ND 1.0 05/06/17 01:570.26
trans-1,2-Dichloroethene ug/L ND 1.0 05/06/17 01:570.49
trans-1,3-Dichloropropene ug/L ND 1.0 05/06/17 01:570.26
Trichloroethene ug/L ND 1.0 05/06/17 01:570.47
Trichlorofluoromethane ug/L ND 1.0 05/06/17 01:570.20
Vinyl acetate ug/L ND 2.0 05/06/17 01:570.35
Vinyl chloride ug/L ND 1.0 05/06/17 01:570.62
Xylene (Total)ug/L ND 1.0 05/06/17 01:570.66
1,2-Dichloroethane-d4 (S)%103 70-130 05/06/17 01:57
4-Bromofluorobenzene (S)%99 70-130 05/06/17 01:57
Toluene-d8 (S)%107 70-130 05/06/17 01:57
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1993552LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 53.850 108 70-130
1,1,1-Trichloroethane ug/L 49.050 98 70-130
1,1,2,2-Tetrachloroethane ug/L 49.950 100 70-130
1,1,2-Trichloroethane ug/L 48.850 98 70-130
1,1-Dichloroethane ug/L 48.250 96 70-130
1,1-Dichloroethene ug/L 47.150 94 70-132
1,1-Dichloropropene ug/L 52.550 105 70-130
1,2,3-Trichlorobenzene ug/L 52.450 105 70-135
1,2,3-Trichloropropane ug/L 51.250 102 70-130
1,2,4-Trichlorobenzene ug/L 50.650 101 70-134
1,2-Dibromo-3-chloropropane ug/L 50.150 100 70-130
1,2-Dibromoethane (EDB)ug/L 55.150 110 70-130
1,2-Dichlorobenzene ug/L 49.550 99 70-130
1,2-Dichloroethane ug/L 46.450 93 70-130
1,2-Dichloropropane ug/L 50.350 101 70-130
1,3-Dichlorobenzene ug/L 49.150 98 70-130
1,3-Dichloropropane ug/L 54.950 110 70-130
1,4-Dichlorobenzene ug/L 49.050 98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1993552LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 44.450 89 58-145
2-Butanone (MEK)ug/L 108100 108 70-145
2-Chlorotoluene ug/L 49.550 99 70-130
2-Hexanone ug/L 106100 106 70-144
4-Chlorotoluene ug/L 47.350 95 70-130
4-Methyl-2-pentanone (MIBK)ug/L 97.4100 97 70-140
Acetone ug/L 106100 106 50-175
Benzene ug/L 51.450 103 70-130
Bromobenzene ug/L 49.350 99 70-130
Bromochloromethane ug/L 50.250 100 70-130
Bromodichloromethane ug/L 49.050 98 70-130
Bromoform ug/L 43.050 86 70-130
Bromomethane ug/L 60.250 120 54-130
Carbon tetrachloride ug/L 50.550 101 70-132
Chlorobenzene ug/L 50.750 101 70-130
Chloroethane ug/L 46.550 93 64-134
Chloroform ug/L 47.950 96 70-130
Chloromethane ug/L 55.650 111 64-130
cis-1,2-Dichloroethene ug/L 47.550 95 70-131
cis-1,3-Dichloropropene ug/L 53.050 106 70-130
Dibromochloromethane ug/L 51.150 102 70-130
Dibromomethane ug/L 48.850 98 70-131
Dichlorodifluoromethane ug/L 58.850 118 56-130
Diisopropyl ether ug/L 52.050 104 70-130
Ethylbenzene ug/L 51.050 102 70-130
Hexachloro-1,3-butadiene ug/L 51.750 103 70-130
m&p-Xylene ug/L 99.6100 100 70-130
Methyl-tert-butyl ether ug/L 53.450 107 70-130
Methylene Chloride ug/L 52.450 105 63-130
Naphthalene ug/L 51.850 104 70-138
o-Xylene ug/L 49.650 99 70-130
p-Isopropyltoluene ug/L 50.250 100 70-130
Styrene ug/L 50.950 102 70-130
Tetrachloroethene ug/L 49.750 99 70-130
Toluene ug/L 48.550 97 70-130
trans-1,2-Dichloroethene ug/L 49.450 99 70-130
trans-1,3-Dichloropropene ug/L 51.450 103 70-132
Trichloroethene ug/L 51.550 103 70-130
Trichlorofluoromethane ug/L 48.650 97 62-133
Vinyl acetate ug/L 101100 101 66-157
Vinyl chloride ug/L 50.250 100 50-150
Xylene (Total)ug/L 149150 99 70-130
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%95 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1994184MATRIX SPIKE SAMPLE:
MSSpike
Result
92339289001
1,1,1,2-Tetrachloroethane ug/L 21.220 106 70-130ND
1,1,1-Trichloroethane ug/L 23.020 115 70-130ND
1,1,2,2-Tetrachloroethane ug/L 21.620 108 70-130ND
1,1,2-Trichloroethane ug/L 21.820 109 70-130ND
1,1-Dichloroethane ug/L 24.220 121 70-130ND
1,1-Dichloroethene ug/L 25.720 128 70-166ND
1,1-Dichloropropene ug/L 25.220 126 70-130ND
1,2,3-Trichlorobenzene ug/L 22.620 113 70-130ND
1,2,3-Trichloropropane ug/L 21.820 109 70-130ND
1,2,4-Trichlorobenzene ug/L 22.020 110 70-130ND
1,2-Dibromo-3-chloropropane ug/L 19.820 99 70-130ND
1,2-Dibromoethane (EDB)ug/L 22.120 111 70-130ND
1,2-Dichlorobenzene ug/L 22.020 110 70-130ND
1,2-Dichloroethane ug/L 22.220 111 70-130ND
1,2-Dichloropropane ug/L 24.420 122 70-130ND
1,3-Dichlorobenzene ug/L 21.720 108 70-130ND
1,3-Dichloropropane ug/L 23.720 119 70-130ND
1,4-Dichlorobenzene ug/L 20.620 103 70-130ND
2,2-Dichloropropane ug/L 25.120 125 70-130ND
2-Butanone (MEK)ug/L 45.940 115 70-130ND
2-Chlorotoluene ug/L 23.120 115 70-130ND
2-Hexanone ug/L 46.940 117 70-130ND
4-Chlorotoluene ug/L 21.720 109 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 43.140 108 70-130ND
Acetone ug/L 48.740 108 70-130ND
Benzene ug/L 24.520 122 70-148ND
Bromobenzene ug/L 22.720 114 70-130ND
Bromochloromethane ug/L 23.720 119 70-130ND
Bromodichloromethane ug/L 22.720 114 70-130ND
Bromoform ug/L 20.820 104 70-130ND
Bromomethane ug/L 30.2 M120151 70-130ND
Carbon tetrachloride ug/L 25.220 126 70-130ND
Chlorobenzene ug/L 22.120 110 70-146ND
Chloroethane ug/L 24.420 122 70-130ND
Chloroform ug/L 23.620 118 70-130ND
Chloromethane ug/L 30.1 M120150 70-130ND
cis-1,2-Dichloroethene ug/L 23.820 119 70-130ND
cis-1,3-Dichloropropene ug/L 23.620 118 70-130ND
Dibromochloromethane ug/L 21.820 109 70-130ND
Dibromomethane ug/L 23.420 117 70-130ND
Dichlorodifluoromethane ug/L 29.2 M120146 70-130ND
Diisopropyl ether ug/L 23.520 118 70-130ND
Ethylbenzene ug/L 23.620 118 70-130ND
Hexachloro-1,3-butadiene ug/L 24.420 122 70-130ND
m&p-Xylene ug/L 46.440 116 70-130ND
Methyl-tert-butyl ether ug/L 21.920 110 70-130ND
Methylene Chloride ug/L 24.520 122 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1994184MATRIX SPIKE SAMPLE:
MSSpike
Result
92339289001
Naphthalene ug/L 21.220 106 70-130ND
o-Xylene ug/L 22.620 113 70-130ND
p-Isopropyltoluene ug/L 22.120 110 70-130ND
Styrene ug/L 22.720 114 70-130ND
Tetrachloroethene ug/L 22.920 114 70-130ND
Toluene ug/L 23.220 116 70-155ND
trans-1,2-Dichloroethene ug/L 25.920 129 70-130ND
trans-1,3-Dichloropropene ug/L 21.720 109 70-130ND
Trichloroethene ug/L 23.520 117 69-151ND
Trichlorofluoromethane ug/L 26.7 M120134 70-130ND
Vinyl acetate ug/L 42.740 107 70-130ND
Vinyl chloride ug/L 27.1 M120136 70-130ND
1,2-Dichloroethane-d4 (S)%103 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92339289002
1994185SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Chlorotoluene ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Chlorotoluene ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Benzene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92339289002
1994185SAMPLE DUPLICATE:
Bromobenzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Diisopropyl ether ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
o-Xylene ug/L ND 30ND
p-Isopropyltoluene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%103 6110
4-Bromofluorobenzene (S)%101 1101
Toluene-d8 (S)%108 0107
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
359493
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples: 92339291002, 92339291003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1993794
Associated Lab Samples:92339291002, 92339291003
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 05/07/17 03:190.33
1,1,1-Trichloroethane ug/L ND 1.0 05/07/17 03:190.48
1,1,2,2-Tetrachloroethane ug/L ND 1.0 05/07/17 03:190.40
1,1,2-Trichloroethane ug/L ND 1.0 05/07/17 03:190.29
1,1-Dichloroethane ug/L ND 1.0 05/07/17 03:190.32
1,1-Dichloroethene ug/L ND 1.0 05/07/17 03:190.56
1,1-Dichloropropene ug/L ND 1.0 05/07/17 03:190.49
1,2,3-Trichlorobenzene ug/L ND 1.0 05/07/17 03:190.33
1,2,3-Trichloropropane ug/L ND 1.0 05/07/17 03:190.41
1,2,4-Trichlorobenzene ug/L ND 1.0 05/07/17 03:190.35
1,2-Dibromo-3-chloropropane ug/L ND 2.0 05/07/17 03:192.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 05/07/17 03:190.27
1,2-Dichlorobenzene ug/L ND 1.0 05/07/17 03:190.30
1,2-Dichloroethane ug/L ND 1.0 05/07/17 03:190.24
1,2-Dichloropropane ug/L ND 1.0 05/07/17 03:190.27
1,3-Dichlorobenzene ug/L ND 1.0 05/07/17 03:190.24
1,3-Dichloropropane ug/L ND 1.0 05/07/17 03:190.28
1,4-Dichlorobenzene ug/L ND 1.0 05/07/17 03:190.33
2,2-Dichloropropane ug/L ND 1.0 05/07/17 03:190.13
2-Butanone (MEK)ug/L ND 5.0 05/07/17 03:190.96
2-Chlorotoluene ug/L ND 1.0 05/07/17 03:190.35
2-Hexanone ug/L ND 5.0 05/07/17 03:190.46
4-Chlorotoluene ug/L ND 1.0 05/07/17 03:190.31
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 05/07/17 03:190.33
Acetone ug/L ND 25.0 05/07/17 03:1910.0
Benzene ug/L ND 1.0 05/07/17 03:190.25
Bromobenzene ug/L ND 1.0 05/07/17 03:190.30
Bromochloromethane ug/L ND 1.0 05/07/17 03:190.17
Bromodichloromethane ug/L ND 1.0 05/07/17 03:190.18
Bromoform ug/L ND 1.0 05/07/17 03:190.26
Bromomethane ug/L ND 2.0 05/07/17 03:190.29
Carbon tetrachloride ug/L ND 1.0 05/07/17 03:190.25
Chlorobenzene ug/L ND 1.0 05/07/17 03:190.23
Chloroethane ug/L ND 1.0 05/07/17 03:190.54
Chloroform ug/L ND 1.0 05/07/17 03:190.14
Chloromethane ug/L ND 1.0 05/07/17 03:190.11
cis-1,2-Dichloroethene ug/L ND 1.0 05/07/17 03:190.19
cis-1,3-Dichloropropene ug/L ND 1.0 05/07/17 03:190.13
Dibromochloromethane ug/L ND 1.0 05/07/17 03:190.21
Dibromomethane ug/L ND 1.0 05/07/17 03:190.21
Dichlorodifluoromethane ug/L ND 1.0 05/07/17 03:190.21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1993794
Associated Lab Samples:92339291002, 92339291003
Matrix: Water
AnalyzedMDL
Diisopropyl ether ug/L ND 1.0 05/07/17 03:190.12
Ethylbenzene ug/L ND 1.0 05/07/17 03:190.30
Hexachloro-1,3-butadiene ug/L ND 1.0 05/07/17 03:190.71
m&p-Xylene ug/L ND 2.0 05/07/17 03:190.66
Methyl-tert-butyl ether ug/L ND 1.0 05/07/17 03:190.21
Methylene Chloride ug/L ND 2.0 05/07/17 03:190.97
Naphthalene ug/L ND 1.0 05/07/17 03:190.24
o-Xylene ug/L ND 1.0 05/07/17 03:190.23
p-Isopropyltoluene ug/L ND 1.0 05/07/17 03:190.31
Styrene ug/L ND 1.0 05/07/17 03:190.26
Tetrachloroethene ug/L ND 1.0 05/07/17 03:190.46
Toluene ug/L ND 1.0 05/07/17 03:190.26
trans-1,2-Dichloroethene ug/L ND 1.0 05/07/17 03:190.49
trans-1,3-Dichloropropene ug/L ND 1.0 05/07/17 03:190.26
Trichloroethene ug/L ND 1.0 05/07/17 03:190.47
Trichlorofluoromethane ug/L ND 1.0 05/07/17 03:190.20
Vinyl acetate ug/L ND 2.0 05/07/17 03:190.35
Vinyl chloride ug/L ND 1.0 05/07/17 03:190.62
Xylene (Total)ug/L ND 1.0 05/07/17 03:190.66
1,2-Dichloroethane-d4 (S)%107 70-130 05/07/17 03:19
4-Bromofluorobenzene (S)%101 70-130 05/07/17 03:19
Toluene-d8 (S)%106 70-130 05/07/17 03:19
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1993795LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 48.750 97 70-130
1,1,1-Trichloroethane ug/L 44.950 90 70-130
1,1,2,2-Tetrachloroethane ug/L 48.350 97 70-130
1,1,2-Trichloroethane ug/L 49.450 99 70-130
1,1-Dichloroethane ug/L 46.050 92 70-130
1,1-Dichloroethene ug/L 49.750 99 70-132
1,1-Dichloropropene ug/L 49.750 99 70-130
1,2,3-Trichlorobenzene ug/L 50.350 101 70-135
1,2,3-Trichloropropane ug/L 46.550 93 70-130
1,2,4-Trichlorobenzene ug/L 47.850 96 70-134
1,2-Dibromo-3-chloropropane ug/L 48.650 97 70-130
1,2-Dibromoethane (EDB)ug/L 50.850 102 70-130
1,2-Dichlorobenzene ug/L 47.350 95 70-130
1,2-Dichloroethane ug/L 46.950 94 70-130
1,2-Dichloropropane ug/L 50.050 100 70-130
1,3-Dichlorobenzene ug/L 45.650 91 70-130
1,3-Dichloropropane ug/L 52.750 105 70-130
1,4-Dichlorobenzene ug/L 44.350 89 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
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Page 54 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1993795LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 42.950 86 58-145
2-Butanone (MEK)ug/L 100100 100 70-145
2-Chlorotoluene ug/L 45.550 91 70-130
2-Hexanone ug/L 99.4100 99 70-144
4-Chlorotoluene ug/L 44.650 89 70-130
4-Methyl-2-pentanone (MIBK)ug/L 94.4100 94 70-140
Acetone ug/L 103100 103 50-175
Benzene ug/L 50.550 101 70-130
Bromobenzene ug/L 46.050 92 70-130
Bromochloromethane ug/L 48.150 96 70-130
Bromodichloromethane ug/L 48.850 98 70-130
Bromoform ug/L 42.350 85 70-130
Bromomethane ug/L 48.250 96 54-130
Carbon tetrachloride ug/L 47.750 95 70-132
Chlorobenzene ug/L 47.450 95 70-130
Chloroethane ug/L 46.450 93 64-134
Chloroform ug/L 44.650 89 70-130
Chloromethane ug/L 48.150 96 64-130
cis-1,2-Dichloroethene ug/L 46.050 92 70-131
cis-1,3-Dichloropropene ug/L 51.550 103 70-130
Dibromochloromethane ug/L 48.350 97 70-130
Dibromomethane ug/L 48.650 97 70-131
Dichlorodifluoromethane ug/L 52.950 106 56-130
Diisopropyl ether ug/L 50.450 101 70-130
Ethylbenzene ug/L 47.550 95 70-130
Hexachloro-1,3-butadiene ug/L 47.650 95 70-130
m&p-Xylene ug/L 92.2100 92 70-130
Methyl-tert-butyl ether ug/L 49.750 99 70-130
Methylene Chloride ug/L 51.250 102 63-130
Naphthalene ug/L 48.550 97 70-138
o-Xylene ug/L 45.650 91 70-130
p-Isopropyltoluene ug/L 45.350 91 70-130
Styrene ug/L 46.950 94 70-130
Tetrachloroethene ug/L 46.350 93 70-130
Toluene ug/L 45.950 92 70-130
trans-1,2-Dichloroethene ug/L 45.250 90 70-130
trans-1,3-Dichloropropene ug/L 50.050 100 70-132
Trichloroethene ug/L 47.550 95 70-130
Trichlorofluoromethane ug/L 48.450 97 62-133
Vinyl acetate ug/L 100100 100 66-157
Vinyl chloride ug/L 48.350 97 50-150
Xylene (Total)ug/L 138150 92 70-130
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%96 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
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Page 55 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1993796MATRIX SPIKE SAMPLE:
MSSpike
Result
92339535007
1,1,1,2-Tetrachloroethane ug/L 19.620 98 70-130ND
1,1,1-Trichloroethane ug/L 21.420 107 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.320 102 70-130ND
1,1,2-Trichloroethane ug/L 19.320 96 70-130ND
1,1-Dichloroethane ug/L 21.420 107 70-130ND
1,1-Dichloroethene ug/L 23.420 117 70-166ND
1,1-Dichloropropene ug/L 23.120 115 70-130ND
1,2,3-Trichlorobenzene ug/L 20.820 104 70-130ND
1,2,3-Trichloropropane ug/L 19.820 99 70-130ND
1,2,4-Trichlorobenzene ug/L 20.120 101 70-130ND
1,2-Dibromo-3-chloropropane ug/L 19.020 95 70-130ND
1,2-Dibromoethane (EDB)ug/L 19.820 99 70-130ND
1,2-Dichlorobenzene ug/L 19.220 96 70-130ND
1,2-Dichloroethane ug/L 20.920 105 70-130ND
1,2-Dichloropropane ug/L 21.420 107 70-130ND
1,3-Dichlorobenzene ug/L 18.420 92 70-130ND
1,3-Dichloropropane ug/L 20.520 102 70-130ND
1,4-Dichlorobenzene ug/L 18.520 93 70-130ND
2,2-Dichloropropane ug/L 21.220 106 70-130ND
2-Butanone (MEK)ug/L 45.540 114 70-130ND
2-Chlorotoluene ug/L 20.120 101 70-130ND
2-Hexanone ug/L 45.040 112 70-130ND
4-Chlorotoluene ug/L 19.120 96 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 38.640 96 70-130ND
Acetone ug/L 67.1 M140134 70-13013.6J
Benzene ug/L 20.820 104 70-148ND
Bromobenzene ug/L 19.220 96 70-130ND
Bromochloromethane ug/L 22.220 111 70-130ND
Bromodichloromethane ug/L 20.020 100 70-130ND
Bromoform ug/L 18.820 94 70-130ND
Bromomethane ug/L 24.320 122 70-130ND
Carbon tetrachloride ug/L 21.220 106 70-130ND
Chlorobenzene ug/L 20.120 100 70-146ND
Chloroethane ug/L 22.820 114 70-130ND
Chloroform ug/L 21.120 105 70-130ND
Chloromethane ug/L 25.020 125 70-130ND
cis-1,2-Dichloroethene ug/L 21.820 109 70-130ND
cis-1,3-Dichloropropene ug/L 20.120 101 70-130ND
Dibromochloromethane ug/L 20.120 100 70-130ND
Dibromomethane ug/L 19.920 99 70-130ND
Dichlorodifluoromethane ug/L 26.3 M120131 70-130ND
Diisopropyl ether ug/L 22.120 110 70-130ND
Ethylbenzene ug/L 20.520 103 70-130ND
Hexachloro-1,3-butadiene ug/L 21.920 110 70-130ND
m&p-Xylene ug/L 40.640 101 70-130ND
Methyl-tert-butyl ether ug/L 21.320 107 70-130ND
Methylene Chloride ug/L 21.820 109 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
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Page 56 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1993796MATRIX SPIKE SAMPLE:
MSSpike
Result
92339535007
Naphthalene ug/L 21.020 105 70-130ND
o-Xylene ug/L 20.120 101 70-130ND
p-Isopropyltoluene ug/L 19.020 95 70-130ND
Styrene ug/L 19.820 99 70-130ND
Tetrachloroethene ug/L 19.420 97 70-130ND
Toluene ug/L 19.720 99 70-155ND
trans-1,2-Dichloroethene ug/L 22.920 114 70-130ND
trans-1,3-Dichloropropene ug/L 19.820 99 70-130ND
Trichloroethene ug/L 20.120 100 69-151ND
Trichlorofluoromethane ug/L 23.420 117 70-130ND
Vinyl acetate ug/L 36.940 92 70-130ND
Vinyl chloride ug/L 24.220 121 70-130ND
1,2-Dichloroethane-d4 (S)%111 70-130
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92339535016
1993797SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Chlorotoluene ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Chlorotoluene ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L 34.2 3012.4J
Benzene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92339535016
1993797SAMPLE DUPLICATE:
Bromobenzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Diisopropyl ether ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
o-Xylene ug/L ND 30ND
p-Isopropyltoluene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%108 6102
4-Bromofluorobenzene (S)%100 4105
Toluene-d8 (S)%108 4112
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
359368
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples: 92339291004, 92339291005, 92339291006, 92339291007, 92339291008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1993026
Associated Lab Samples:92339291004, 92339291005, 92339291006, 92339291007, 92339291008
Matrix: Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 6.7 05/05/17 11:302.8
1,1,1-Trichloroethane ug/kg ND 6.7 05/05/17 11:302.4
1,1,2,2-Tetrachloroethane ug/kg ND 6.7 05/05/17 11:302.5
1,1,2-Trichloroethane ug/kg ND 6.7 05/05/17 11:302.8
1,1-Dichloroethane ug/kg ND 6.7 05/05/17 11:302.0
1,1-Dichloroethene ug/kg ND 6.7 05/05/17 11:302.4
1,1-Dichloropropene ug/kg ND 6.7 05/05/17 11:302.0
1,2,3-Trichlorobenzene ug/kg ND 6.7 05/05/17 11:302.9
1,2,3-Trichloropropane ug/kg ND 6.7 05/05/17 11:302.1
1,2,4-Trichlorobenzene ug/kg ND 6.7 05/05/17 11:302.1
1,2,4-Trimethylbenzene ug/kg ND 6.7 05/05/17 11:302.7
1,2-Dibromo-3-chloropropane ug/kg ND 6.7 05/05/17 11:304.8
1,2-Dibromoethane (EDB)ug/kg ND 6.7 05/05/17 11:302.4
1,2-Dichlorobenzene ug/kg ND 6.7 05/05/17 11:302.5
1,2-Dichloroethane ug/kg ND 6.7 05/05/17 11:302.9
1,2-Dichloropropane ug/kg ND 6.7 05/05/17 11:302.3
1,3,5-Trimethylbenzene ug/kg ND 6.7 05/05/17 11:302.4
1,3-Dichlorobenzene ug/kg ND 6.7 05/05/17 11:302.7
1,3-Dichloropropane ug/kg ND 6.7 05/05/17 11:302.5
1,4-Dichlorobenzene ug/kg ND 6.7 05/05/17 11:302.3
2,2-Dichloropropane ug/kg ND 6.7 05/05/17 11:302.3
2-Butanone (MEK)ug/kg ND 133 05/05/17 11:303.9
2-Chlorotoluene ug/kg ND 6.7 05/05/17 11:302.3
2-Hexanone ug/kg ND 66.7 05/05/17 11:305.2
4-Chlorotoluene ug/kg ND 6.7 05/05/17 11:302.4
4-Methyl-2-pentanone (MIBK)ug/kg ND 66.7 05/05/17 11:304.9
Acetone ug/kg ND 133 05/05/17 11:3013.3
Benzene ug/kg ND 6.7 05/05/17 11:302.1
Bromobenzene ug/kg ND 6.7 05/05/17 11:302.7
Bromochloromethane ug/kg ND 6.7 05/05/17 11:302.3
Bromodichloromethane ug/kg ND 6.7 05/05/17 11:302.5
Bromoform ug/kg ND 6.7 05/05/17 11:303.1
Bromomethane ug/kg ND 13.3 05/05/17 11:303.3
Carbon tetrachloride ug/kg ND 6.7 05/05/17 11:303.5
Chlorobenzene ug/kg ND 6.7 05/05/17 11:302.5
Chloroethane ug/kg ND 13.3 05/05/17 11:303.2
Chloroform ug/kg ND 6.7 05/05/17 11:302.1
Chloromethane ug/kg ND 13.3 05/05/17 11:303.2
cis-1,2-Dichloroethene ug/kg ND 6.7 05/05/17 11:301.9
cis-1,3-Dichloropropene ug/kg ND 6.7 05/05/17 11:302.4
Dibromochloromethane ug/kg ND 6.7 05/05/17 11:302.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1993026
Associated Lab Samples:92339291004, 92339291005, 92339291006, 92339291007, 92339291008
Matrix: Solid
AnalyzedMDL
Dibromomethane ug/kg ND 6.7 05/05/17 11:303.3
Dichlorodifluoromethane ug/kg ND 13.3 05/05/17 11:304.8
Diisopropyl ether ug/kg ND 6.7 05/05/17 11:302.3
Ethylbenzene ug/kg ND 6.7 05/05/17 11:302.4
Hexachloro-1,3-butadiene ug/kg ND 6.7 05/05/17 11:302.7
Isopropylbenzene (Cumene)ug/kg ND 6.7 05/05/17 11:302.5
m&p-Xylene ug/kg ND 13.3 05/05/17 11:304.8
Methyl-tert-butyl ether ug/kg ND 6.7 05/05/17 11:302.0
Methylene Chloride ug/kg ND 26.7 05/05/17 11:304.0
n-Butylbenzene ug/kg ND 6.7 05/05/17 11:302.4
n-Propylbenzene ug/kg ND 6.7 05/05/17 11:302.3
Naphthalene ug/kg 2.8J 6.7 05/05/17 11:301.6
o-Xylene ug/kg ND 6.7 05/05/17 11:302.5
p-Isopropyltoluene ug/kg ND 6.7 05/05/17 11:302.3
sec-Butylbenzene ug/kg ND 6.7 05/05/17 11:302.1
Styrene ug/kg ND 6.7 05/05/17 11:302.4
tert-Butylbenzene ug/kg ND 6.7 05/05/17 11:302.7
Tetrachloroethene ug/kg ND 6.7 05/05/17 11:302.3
Toluene ug/kg ND 6.7 05/05/17 11:302.4
trans-1,2-Dichloroethene ug/kg ND 6.7 05/05/17 11:302.5
trans-1,3-Dichloropropene ug/kg ND 6.7 05/05/17 11:302.0
Trichloroethene ug/kg ND 6.7 05/05/17 11:302.8
Trichlorofluoromethane ug/kg ND 6.7 05/05/17 11:302.9
Vinyl acetate ug/kg ND 66.7 05/05/17 11:3011.7
Vinyl chloride ug/kg ND 13.3 05/05/17 11:302.4
Xylene (Total)ug/kg ND 13.3 05/05/17 11:304.8
1,2-Dichloroethane-d4 (S)%114 70-132 05/05/17 11:30
4-Bromofluorobenzene (S)%96 70-130 05/05/17 11:30
Toluene-d8 (S)%100 70-130 05/05/17 11:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1993027LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 51.552.9 97 74-137
1,1,1-Trichloroethane ug/kg 54.552.9 103 67-140
1,1,2,2-Tetrachloroethane ug/kg 49.652.9 94 72-141
1,1,2-Trichloroethane ug/kg 55.052.9 104 78-138
1,1-Dichloroethane ug/kg 57.052.9 108 69-134
1,1-Dichloroethene ug/kg 56.952.9 108 67-138
1,1-Dichloropropene ug/kg 57.152.9 108 69-139
1,2,3-Trichlorobenzene ug/kg 57.652.9 109 70-146
1,2,3-Trichloropropane ug/kg 54.252.9 103 69-144
1,2,4-Trichlorobenzene ug/kg 55.652.9 105 68-148
1,2,4-Trimethylbenzene ug/kg 53.652.9 101 74-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1993027LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 58.052.9 110 65-140
1,2-Dibromoethane (EDB)ug/kg 57.752.9 109 77-135
1,2-Dichlorobenzene ug/kg 55.452.9 105 77-141
1,2-Dichloroethane ug/kg 54.852.9 104 65-137
1,2-Dichloropropane ug/kg 55.452.9 105 72-136
1,3,5-Trimethylbenzene ug/kg 53.852.9 102 76-133
1,3-Dichlorobenzene ug/kg 53.252.9 101 74-138
1,3-Dichloropropane ug/kg 58.252.9 110 71-139
1,4-Dichlorobenzene ug/kg 53.352.9 101 76-138
2,2-Dichloropropane ug/kg 55.052.9 104 68-137
2-Butanone (MEK)ug/kg 126106 119 58-147
2-Chlorotoluene ug/kg 55.052.9 104 73-139
2-Hexanone ug/kg 102106 96 62-145
4-Chlorotoluene ug/kg 53.652.9 101 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 115106 109 64-149
Acetone ug/kg 131106 124 53-153
Benzene ug/kg 53.252.9 101 73-135
Bromobenzene ug/kg 55.952.9 106 75-133
Bromochloromethane ug/kg 54.352.9 103 73-134
Bromodichloromethane ug/kg 55.052.9 104 71-135
Bromoform ug/kg 52.552.9 99 66-141
Bromomethane ug/kg 41.352.9 78 53-160
Carbon tetrachloride ug/kg 51.552.9 97 60-145
Chlorobenzene ug/kg 54.252.9 103 78-130
Chloroethane ug/kg 56.952.9 108 64-149
Chloroform ug/kg 55.052.9 104 70-134
Chloromethane ug/kg 55.652.9 105 52-150
cis-1,2-Dichloroethene ug/kg 59.252.9 112 70-133
cis-1,3-Dichloropropene ug/kg 57.552.9 109 68-134
Dibromochloromethane ug/kg 55.352.9 105 71-138
Dibromomethane ug/kg 57.252.9 108 74-130
Dichlorodifluoromethane ug/kg 49.852.9 94 40-160
Diisopropyl ether ug/kg 57.952.9 109 69-141
Ethylbenzene ug/kg 52.152.9 99 75-133
Hexachloro-1,3-butadiene ug/kg 50.652.9 96 68-143
Isopropylbenzene (Cumene)ug/kg 51.252.9 97 76-143
m&p-Xylene ug/kg 103106 98 75-136
Methyl-tert-butyl ether ug/kg 59.152.9 112 68-144
Methylene Chloride ug/kg 55.552.9 105 45-154
n-Butylbenzene ug/kg 52.452.9 99 72-137
n-Propylbenzene ug/kg 52.352.9 99 76-136
Naphthalene ug/kg 63.552.9 120 68-151
o-Xylene ug/kg 53.552.9 101 76-141
p-Isopropyltoluene ug/kg 53.052.9 100 76-140
sec-Butylbenzene ug/kg 52.252.9 99 79-139
Styrene ug/kg 54.552.9 103 79-137
tert-Butylbenzene ug/kg 48.752.9 92 74-143
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1993027LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 42.752.9 81 71-138
Toluene ug/kg 53.952.9 102 74-131
trans-1,2-Dichloroethene ug/kg 57.452.9 109 67-135
trans-1,3-Dichloropropene ug/kg 57.752.9 109 65-146
Trichloroethene ug/kg 53.952.9 102 67-135
Trichlorofluoromethane ug/kg 56.952.9 108 59-144
Vinyl acetate ug/kg 62.8106 59 40-160
Vinyl chloride ug/kg 56.052.9 106 56-141
Xylene (Total)ug/kg 157159 99 76-137
1,2-Dichloroethane-d4 (S)%106 70-132
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1993815MATRIX SPIKE SAMPLE:
MSSpike
Result
92339174001
1,1,1,2-Tetrachloroethane ug/kg 13.815.5 89 70-130ND
1,1,1-Trichloroethane ug/kg 14.715.5 95 70-130ND
1,1,2,2-Tetrachloroethane ug/kg 15.115.5 97 70-130ND
1,1,2-Trichloroethane ug/kg 16.015.5 103 70-130ND
1,1-Dichloroethane ug/kg 16.715.5 108 70-130ND
1,1-Dichloroethene ug/kg 15.915.5 102 49-180ND
1,1-Dichloropropene ug/kg 16.015.5 103 70-130ND
1,2,3-Trichlorobenzene ug/kg 11.815.5 76 70-130ND
1,2,3-Trichloropropane ug/kg 14.815.5 96 70-130ND
1,2,4-Trichlorobenzene ug/kg 11.715.5 75 70-130ND
1,2,4-Trimethylbenzene ug/kg 14.315.5 92 70-130ND
1,2-Dibromo-3-chloropropane ug/kg 16.515.5 106 70-130ND
1,2-Dibromoethane (EDB)ug/kg 16.415.5 105 70-130ND
1,2-Dichlorobenzene ug/kg 14.315.5 92 70-130ND
1,2-Dichloroethane ug/kg 15.615.5 101 70-130ND
1,2-Dichloropropane ug/kg 16.215.5 104 70-130ND
1,3,5-Trimethylbenzene ug/kg 14.115.5 91 70-130ND
1,3-Dichlorobenzene ug/kg 13.915.5 89 70-130ND
1,3-Dichloropropane ug/kg 16.515.5 106 70-130ND
1,4-Dichlorobenzene ug/kg 13.915.5 89 70-130ND
2,2-Dichloropropane ug/kg 15.315.5 98 70-130ND
2-Butanone (MEK)ug/kg 36.8J31.1 119 70-130ND
2-Chlorotoluene ug/kg 14.615.5 94 70-130ND
2-Hexanone ug/kg 30.2J31.1 97 70-130ND
4-Chlorotoluene ug/kg 14.215.5 91 70-130ND
4-Methyl-2-pentanone (MIBK)ug/kg 33.2J31.1 107 70-130ND
Acetone ug/kg 61.6J M131.1 139 70-13018.4J
Benzene ug/kg 16.115.5 104 50-166ND
Bromobenzene ug/kg 15.115.5 97 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
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Huntersville, NC 28078
[phone]
Page 62 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1993815MATRIX SPIKE SAMPLE:
MSSpike
Result
92339174001
Bromochloromethane ug/kg 18.015.5 116 70-130ND
Bromodichloromethane ug/kg 15.315.5 99 70-130ND
Bromoform ug/kg 14.415.5 93 70-130ND
Bromomethane ug/kg 14.815.5 95 70-130ND
Carbon tetrachloride ug/kg 14.115.5 91 70-130ND
Chlorobenzene ug/kg 14.515.5 94 43-169ND
Chloroethane ug/kg 16.315.5 105 70-130ND
Chloroform ug/kg 15.715.5 101 70-130ND
Chloromethane ug/kg 15.315.5 99 70-130ND
cis-1,2-Dichloroethene ug/kg 16.715.5 108 70-130ND
cis-1,3-Dichloropropene ug/kg 16.415.5 105 70-130ND
Dibromochloromethane ug/kg 15.215.5 98 70-130ND
Dibromomethane ug/kg 16.015.5 103 70-130ND
Dichlorodifluoromethane ug/kg 13.615.5 87 70-130ND
Diisopropyl ether ug/kg 16.915.5 109 70-130ND
Ethylbenzene ug/kg 14.215.5 92 70-130ND
Hexachloro-1,3-butadiene ug/kg 8.4 M115.5 54 70-130ND
Isopropylbenzene (Cumene)ug/kg 13.315.5 86 70-130ND
m&p-Xylene ug/kg 27.531.1 89 70-130ND
Methyl-tert-butyl ether ug/kg 17.815.5 115 70-130ND
Methylene Chloride ug/kg 16.415.5 92 70-130ND
n-Butylbenzene ug/kg 12.615.5 81 70-130ND
n-Propylbenzene ug/kg 13.815.5 89 70-130ND
Naphthalene ug/kg 16.315.5 105 70-130ND
o-Xylene ug/kg 14.315.5 92 70-130ND
p-Isopropyltoluene ug/kg 13.215.5 85 70-130ND
sec-Butylbenzene ug/kg 12.815.5 83 70-130ND
Styrene ug/kg 14.315.5 92 70-130ND
tert-Butylbenzene ug/kg 12.215.5 78 70-130ND
Tetrachloroethene ug/kg 11.415.5 73 70-130ND
Toluene ug/kg 15.715.5 99 52-163ND
trans-1,2-Dichloroethene ug/kg 16.915.5 109 70-130ND
trans-1,3-Dichloropropene ug/kg 16.215.5 104 70-130ND
Trichloroethene ug/kg 15.315.5 98 49-167ND
Trichlorofluoromethane ug/kg 15.315.5 99 70-130ND
Vinyl acetate ug/kg 24.3J31.1 78 70-130ND
Vinyl chloride ug/kg 15.615.5 100 70-130ND
1,2-Dichloroethane-d4 (S)%108 70-132
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92339291004
1993814SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
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Page 63 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92339291004
1993814SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg 27.3J 3025.9J
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
m&p-Xylene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
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[phone]
Page 64 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92339291004
1993814SAMPLE DUPLICATE:
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg 6.0J 305.3J
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg 6.7 305.8J
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%111 3118
4-Bromofluorobenzene (S)%98 695
Toluene-d8 (S)%101 3101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
359091
EPA 3546
EPA 8082
8082 GCS PCB
Associated Lab Samples: 92339291004, 92339291005, 92339291006, 92339291007, 92339291008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1991636
Associated Lab Samples:92339291004, 92339291005, 92339291006, 92339291007, 92339291008
Matrix: Solid
AnalyzedMDL
PCB-1016 (Aroclor 1016)ug/kg ND 33.0 05/05/17 01:4115.0
PCB-1221 (Aroclor 1221)ug/kg ND 33.0 05/05/17 01:4115.0
PCB-1232 (Aroclor 1232)ug/kg ND 33.0 05/05/17 01:4115.0
PCB-1242 (Aroclor 1242)ug/kg ND 33.0 05/05/17 01:4115.0
PCB-1248 (Aroclor 1248)ug/kg ND 33.0 05/05/17 01:4115.0
PCB-1254 (Aroclor 1254)ug/kg ND 33.0 05/05/17 01:4115.0
PCB-1260 (Aroclor 1260)ug/kg ND 33.0 05/05/17 01:4115.0
Decachlorobiphenyl (S)%98 21-132 05/05/17 01:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1991637LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1991638
PCB-1016 (Aroclor 1016)ug/kg 123167 74 31-12071118 4 30
PCB-1260 (Aroclor 1260)ug/kg 146167 88 32-12088146 0 30
Decachlorobiphenyl (S)%95 21-13298
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
359665
EPA 3510
EPA 8082
8082 GCS PCB
Associated Lab Samples: 92339291001, 92339291002, 92339291003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1994579
Associated Lab Samples:92339291001, 92339291002, 92339291003
Matrix: Water
AnalyzedMDL
PCB-1016 (Aroclor 1016)ug/L ND 0.50 05/09/17 22:250.50
PCB-1221 (Aroclor 1221)ug/L ND 0.50 05/09/17 22:250.50
PCB-1232 (Aroclor 1232)ug/L ND 0.50 05/09/17 22:250.50
PCB-1242 (Aroclor 1242)ug/L ND 0.50 05/09/17 22:250.50
PCB-1248 (Aroclor 1248)ug/L ND 0.50 05/09/17 22:250.50
PCB-1254 (Aroclor 1254)ug/L ND 0.50 05/09/17 22:250.50
PCB-1260 (Aroclor 1260)ug/L ND 0.50 05/09/17 22:250.50
Decachlorobiphenyl (S)%82 10-132 05/09/17 22:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1994580LABORATORY CONTROL SAMPLE:
LCSSpike
PCB-1016 (Aroclor 1016)ug/L 3.85 76 50-150
PCB-1260 (Aroclor 1260)ug/L 4.05 79 50-150
Decachlorobiphenyl (S)%49 10-132
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1994581MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92339057011
1994582
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
PCB-1016 (Aroclor 1016) ug/L 10 91 50-15090 0 3010ND9.1 9.0
PCB-1260 (Aroclor 1260) ug/L 10 81 50-15078 4 3010ND8.1 7.8
Decachlorobiphenyl (S)%81 10-13271
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
359093
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples: 92339291004, 92339291007, 92339291008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1991642
Associated Lab Samples:92339291004, 92339291007, 92339291008
Matrix: Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 330 05/04/17 11:5164.0
1,2-Dichlorobenzene ug/kg ND 330 05/04/17 11:5188.0
1,3-Dichlorobenzene ug/kg ND 330 05/04/17 11:5175.0
1,4-Dichlorobenzene ug/kg ND 330 05/04/17 11:5193.0
1-Methylnaphthalene ug/kg ND 330 05/04/17 11:5186.0
2,2'-Oxybis(1-chloropropane)ug/kg ND 330 05/04/17 11:5188.0
2,4,5-Trichlorophenol ug/kg ND 330 05/04/17 11:51102
2,4,6-Trichlorophenol ug/kg ND 330 05/04/17 11:5173.0
2,4-Dichlorophenol ug/kg ND 330 05/04/17 11:5172.0
2,4-Dimethylphenol ug/kg ND 330 05/04/17 11:51130
2,4-Dinitrophenol ug/kg ND 1650 05/04/17 11:5154.0
2,4-Dinitrotoluene ug/kg ND 330 05/04/17 11:5162.0
2,6-Dinitrotoluene ug/kg ND 330 05/04/17 11:5169.0
2-Chloronaphthalene ug/kg ND 330 05/04/17 11:5165.0
2-Chlorophenol ug/kg ND 330 05/04/17 11:5190.0
2-Methylnaphthalene ug/kg ND 330 05/04/17 11:5171.0
2-Methylphenol(o-Cresol)ug/kg ND 330 05/04/17 11:51100
2-Nitroaniline ug/kg ND 1650 05/04/17 11:51102
2-Nitrophenol ug/kg ND 330 05/04/17 11:5180.0
3&4-Methylphenol(m&p Cresol)ug/kg ND 330 05/04/17 11:51130
3,3'-Dichlorobenzidine ug/kg ND 1650 05/04/17 11:5172.0
3-Nitroaniline ug/kg ND 1650 05/04/17 11:5190.0
4,6-Dinitro-2-methylphenol ug/kg ND 660 05/04/17 11:5166.0
4-Bromophenylphenyl ether ug/kg ND 330 05/04/17 11:5160.0
4-Chloro-3-methylphenol ug/kg ND 660 05/04/17 11:5168.0
4-Chloroaniline ug/kg ND 1650 05/04/17 11:5192.0
4-Chlorophenylphenyl ether ug/kg ND 330 05/04/17 11:5168.0
4-Nitroaniline ug/kg ND 660 05/04/17 11:5193.0
4-Nitrophenol ug/kg ND 1650 05/04/17 11:5159.0
Acenaphthene ug/kg ND 330 05/04/17 11:5176.0
Acenaphthylene ug/kg ND 330 05/04/17 11:5178.0
Aniline ug/kg ND 330 05/04/17 11:5189.0
Anthracene ug/kg ND 330 05/04/17 11:5174.0
Benzo(a)anthracene ug/kg ND 330 05/04/17 11:5161.0
Benzo(a)pyrene ug/kg ND 330 05/04/17 11:5163.0
Benzo(b)fluoranthene ug/kg ND 330 05/04/17 11:5157.0
Benzo(g,h,i)perylene ug/kg ND 330 05/04/17 11:5184.0
Benzo(k)fluoranthene ug/kg ND 330 05/04/17 11:5165.0
Benzoic Acid ug/kg ND 1650 05/04/17 11:5160.0
Benzyl alcohol ug/kg ND 660 05/04/17 11:5166.0
bis(2-Chloroethoxy)methane ug/kg ND 330 05/04/17 11:5177.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 68 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1991642
Associated Lab Samples:92339291004, 92339291007, 92339291008
Matrix: Solid
AnalyzedMDL
bis(2-Chloroethyl) ether ug/kg ND 330 05/04/17 11:5184.0
bis(2-Ethylhexyl)phthalate ug/kg ND 330 05/04/17 11:5190.0
Butylbenzylphthalate ug/kg ND 330 05/04/17 11:5170.0
Chrysene ug/kg ND 330 05/04/17 11:5144.0
Di-n-butylphthalate ug/kg ND 330 05/04/17 11:5154.0
Di-n-octylphthalate ug/kg ND 330 05/04/17 11:5169.0
Dibenz(a,h)anthracene ug/kg ND 330 05/04/17 11:5170.0
Dibenzofuran ug/kg ND 330 05/04/17 11:5154.0
Diethylphthalate ug/kg ND 330 05/04/17 11:5151.0
Dimethylphthalate ug/kg ND 330 05/04/17 11:5167.0
Fluoranthene ug/kg ND 330 05/04/17 11:5148.0
Fluorene ug/kg ND 330 05/04/17 11:5168.0
Hexachloro-1,3-butadiene ug/kg ND 330 05/04/17 11:5157.0
Hexachlorobenzene ug/kg ND 330 05/04/17 11:5142.0
Hexachlorocyclopentadiene ug/kg ND 330 05/04/17 11:5161.0
Hexachloroethane ug/kg ND 330 05/04/17 11:5187.0
Indeno(1,2,3-cd)pyrene ug/kg ND 330 05/04/17 11:5168.0
Isophorone ug/kg ND 330 05/04/17 11:5174.0
N-Nitroso-di-n-propylamine ug/kg ND 330 05/04/17 11:5163.0
N-Nitrosodimethylamine ug/kg ND 330 05/04/17 11:51107
N-Nitrosodiphenylamine ug/kg ND 330 05/04/17 11:5198.0
Naphthalene ug/kg ND 330 05/04/17 11:5181.0
Nitrobenzene ug/kg ND 330 05/04/17 11:5190.0
Pentachlorophenol ug/kg ND 1650 05/04/17 11:5160.0
Phenanthrene ug/kg ND 330 05/04/17 11:5155.0
Phenol ug/kg ND 330 05/04/17 11:5199.0
Pyrene ug/kg ND 330 05/04/17 11:5156.0
2,4,6-Tribromophenol (S)%75 27-110 05/04/17 11:51
2-Fluorobiphenyl (S)%73 30-110 05/04/17 11:51
2-Fluorophenol (S)%66 13-110 05/04/17 11:51
Nitrobenzene-d5 (S)%68 23-110 05/04/17 11:51
Phenol-d6 (S)%67 22-110 05/04/17 11:51
Terphenyl-d14 (S)%94 28-110 05/04/17 11:51
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1991643LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1991644
1,2,4-Trichlorobenzene ug/kg 914 R116705536-120751250 31 30
1,2-Dichlorobenzene ug/kg 874 R116705241-120721200 31 30
1,3-Dichlorobenzene ug/kg 882 L216705366-120711190 30 30
1,4-Dichlorobenzene ug/kg 8731670 52 42-120701170 29 30
1-Methylnaphthalene ug/kg 10301670 62 40-120751250 19 30
2,2'-Oxybis(1-chloropropane)ug/kg 8271670 50 17-120671110 29 30
2,4,5-Trichlorophenol ug/kg 10801670 65 37-120721210 11 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1991643LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1991644
2,4,6-Trichlorophenol ug/kg 11401670 68 40-120791320 15 30
2,4-Dichlorophenol ug/kg 10201670 61 33-120801340 27 30
2,4-Dimethylphenol ug/kg 10401670 63 36-120841390 29 30
2,4-Dinitrophenol ug/kg 60308330 72 22-121715920 2 30
2,4-Dinitrotoluene ug/kg 15501670 93 60-120931560 0 30
2,6-Dinitrotoluene ug/kg 15201670 91 54-120951580 4 30
2-Chloronaphthalene ug/kg 9931670 60 41-120761260 24 30
2-Chlorophenol ug/kg 920 R116705539-120761270 32 30
2-Methylnaphthalene ug/kg 10401670 62 26-120751260 19 30
2-Methylphenol(o-Cresol)ug/kg 9051670 54 41-120691150 24 30
2-Nitroaniline ug/kg 24703330 74 45-120792630 6 30
2-Nitrophenol ug/kg 9721670 58 35-120761260 26 30
3&4-Methylphenol(m&p Cresol)ug/kg 9181670 55 35-120691150 22 30
3,3'-Dichlorobenzidine ug/kg 22903330 69 16-125702340 2 30
3-Nitroaniline ug/kg 25903330 78 45-120812710 4 30
4,6-Dinitro-2-methylphenol ug/kg 26503330 79 46-120792630 1 30
4-Bromophenylphenyl ether ug/kg 12301670 74 36-120811340 9 30
4-Chloro-3-methylphenol ug/kg 26203330 79 37-120822730 4 30
4-Chloroaniline ug/kg 21303330 64 35-120752500 16 30
4-Chlorophenylphenyl ether ug/kg 11601670 70 30-120761270 9 30
4-Nitroaniline ug/kg 27903330 84 48-120832780 0 30
4-Nitrophenol ug/kg 62608330 75 43-120726040 3 30
Acenaphthene ug/kg 11001670 66 46-120761270 14 30
Acenaphthylene ug/kg 10601670 64 46-120741240 15 30
Aniline ug/kg 7301670 44 33-12058959 27 30
Anthracene ug/kg 12701670 76 63-120801330 4 30
Benzo(a)anthracene ug/kg 12401670 74 61-120791310 6 30
Benzo(a)pyrene ug/kg 12201670 73 59-120791310 8 30
Benzo(b)fluoranthene ug/kg 11801670 71 55-120761260 7 30
Benzo(g,h,i)perylene ug/kg 12901670 78 57-120811360 5 30
Benzo(k)fluoranthene ug/kg 11801670 71 56-120771280 8 30
Benzoic Acid ug/kg 48208330 58 13-120584820 0 30
Benzyl alcohol ug/kg 19203330 58 34-120732440 24 30
bis(2-Chloroethoxy)methane ug/kg 9321670 56 21-120721200 26 30
bis(2-Chloroethyl) ether ug/kg 9131670 55 25-120701170 25 30
bis(2-Ethylhexyl)phthalate ug/kg 14201670 85 56-123881460 3 30
Butylbenzylphthalate ug/kg 13801670 83 57-120851420 3 30
Chrysene ug/kg 12001670 72 64-120771280 7 30
Di-n-butylphthalate ug/kg 13801670 83 58-120841400 1 30
Di-n-octylphthalate ug/kg 13601670 82 47-121821360 0 30
Dibenz(a,h)anthracene ug/kg 13901670 84 56-120821360 2 30
Dibenzofuran ug/kg 11301670 68 43-120751250 10 30
Diethylphthalate ug/kg 13001670 78 55-120791310 1 30
Dimethylphthalate ug/kg 12701670 76 54-120781300 2 30
Fluoranthene ug/kg 13201670 79 61-120791320 0 30
Fluorene ug/kg 12001670 72 51-120781290 8 30
Hexachloro-1,3-butadiene ug/kg 871 R116705222-120761270 37 30
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1991643LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1991644
Hexachlorobenzene ug/kg 12301670 74 53-120801340 8 30
Hexachlorocyclopentadiene ug/kg 843 R116705118-150751250 39 30
Hexachloroethane ug/kg 8731670 52 39-120701170 29 30
Indeno(1,2,3-cd)pyrene ug/kg 13201670 79 58-120831390 5 30
Isophorone ug/kg 12901670 77 38-120871450 12 30
N-Nitroso-di-n-propylamine ug/kg 10301670 62 30-120731210 16 30
N-Nitrosodimethylamine ug/kg 874 R116705232-120751250 36 30
N-Nitrosodiphenylamine ug/kg 12201670 73 50-120801330 9 30
Naphthalene ug/kg 9141670 55 38-120731220 29 30
Nitrobenzene ug/kg 1010 R116706137-120821370 31 30
Pentachlorophenol ug/kg 24803330 74 10-120752490 0 30
Phenanthrene ug/kg 12301670 74 62-120771280 4 30
Phenol ug/kg 10101670 60 37-120801330 28 30
Pyrene ug/kg 11901670 72 63-120771280 7 30
2,4,6-Tribromophenol (S)%79 27-11084
2-Fluorobiphenyl (S)%57 30-11073
2-Fluorophenol (S)%52 13-11073
Nitrobenzene-d5 (S)%54 23-11073
Phenol-d6 (S)%55 22-11074
Terphenyl-d14 (S)%77 28-11083
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
359761
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples: 92339291005, 92339291006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1995248
Associated Lab Samples:92339291005, 92339291006
Matrix: Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 330 05/10/17 12:2564.0
1,2-Dichlorobenzene ug/kg ND 330 05/10/17 12:2588.0
1,3-Dichlorobenzene ug/kg ND 330 05/10/17 12:2575.0
1,4-Dichlorobenzene ug/kg ND 330 05/10/17 12:2593.0
1-Methylnaphthalene ug/kg ND 330 05/10/17 12:2586.0
2,2'-Oxybis(1-chloropropane)ug/kg ND 330 05/10/17 12:2588.0
2,4,5-Trichlorophenol ug/kg ND 330 05/10/17 12:25102
2,4,6-Trichlorophenol ug/kg ND 330 05/10/17 12:2573.0
2,4-Dichlorophenol ug/kg ND 330 05/10/17 12:2572.0
2,4-Dimethylphenol ug/kg ND 330 05/10/17 12:25130
2,4-Dinitrophenol ug/kg ND 1650 05/10/17 12:2554.0
2,4-Dinitrotoluene ug/kg ND 330 05/10/17 12:2562.0
2,6-Dinitrotoluene ug/kg ND 330 05/10/17 12:2569.0
2-Chloronaphthalene ug/kg ND 330 05/10/17 12:2565.0
2-Chlorophenol ug/kg ND 330 05/10/17 12:2590.0
2-Methylnaphthalene ug/kg ND 330 05/10/17 12:2571.0
2-Methylphenol(o-Cresol)ug/kg ND 330 05/10/17 12:25100
2-Nitroaniline ug/kg ND 1650 05/10/17 12:25102
2-Nitrophenol ug/kg ND 330 05/10/17 12:2580.0
3&4-Methylphenol(m&p Cresol)ug/kg ND 330 05/10/17 12:25130
3,3'-Dichlorobenzidine ug/kg ND 1650 05/10/17 12:2572.0
3-Nitroaniline ug/kg ND 1650 05/10/17 12:2590.0
4,6-Dinitro-2-methylphenol ug/kg ND 660 05/10/17 12:2566.0
4-Bromophenylphenyl ether ug/kg ND 330 05/10/17 12:2560.0
4-Chloro-3-methylphenol ug/kg ND 660 05/10/17 12:2568.0
4-Chloroaniline ug/kg ND 1650 05/10/17 12:2592.0
4-Chlorophenylphenyl ether ug/kg ND 330 05/10/17 12:2568.0
4-Nitroaniline ug/kg ND 660 05/10/17 12:2593.0
4-Nitrophenol ug/kg ND 1650 05/10/17 12:2559.0
Acenaphthene ug/kg ND 330 05/10/17 12:2576.0
Acenaphthylene ug/kg ND 330 05/10/17 12:2578.0
Aniline ug/kg ND 330 05/10/17 12:2589.0
Anthracene ug/kg ND 330 05/10/17 12:2574.0
Benzo(a)anthracene ug/kg ND 330 05/10/17 12:2561.0
Benzo(a)pyrene ug/kg ND 330 05/10/17 12:2563.0
Benzo(b)fluoranthene ug/kg ND 330 05/10/17 12:2557.0
Benzo(g,h,i)perylene ug/kg ND 330 05/10/17 12:2584.0
Benzo(k)fluoranthene ug/kg ND 330 05/10/17 12:2565.0
Benzoic Acid ug/kg ND 1650 05/10/17 12:2560.0
Benzyl alcohol ug/kg ND 660 05/10/17 12:2566.0
bis(2-Chloroethoxy)methane ug/kg ND 330 05/10/17 12:2577.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1995248
Associated Lab Samples:92339291005, 92339291006
Matrix: Solid
AnalyzedMDL
bis(2-Chloroethyl) ether ug/kg ND 330 05/10/17 12:2584.0
bis(2-Ethylhexyl)phthalate ug/kg ND 330 05/10/17 12:2590.0
Butylbenzylphthalate ug/kg ND 330 05/10/17 12:2570.0
Chrysene ug/kg ND 330 05/10/17 12:2544.0
Di-n-butylphthalate ug/kg ND 330 05/10/17 12:2554.0
Di-n-octylphthalate ug/kg ND 330 05/10/17 12:2569.0
Dibenz(a,h)anthracene ug/kg ND 330 05/10/17 12:2570.0
Dibenzofuran ug/kg ND 330 05/10/17 12:2554.0
Diethylphthalate ug/kg ND 330 05/10/17 12:2551.0
Dimethylphthalate ug/kg ND 330 05/10/17 12:2567.0
Fluoranthene ug/kg ND 330 05/10/17 12:2548.0
Fluorene ug/kg ND 330 05/10/17 12:2568.0
Hexachloro-1,3-butadiene ug/kg ND 330 05/10/17 12:2557.0
Hexachlorobenzene ug/kg ND 330 05/10/17 12:2542.0
Hexachlorocyclopentadiene ug/kg ND 330 05/10/17 12:2561.0
Hexachloroethane ug/kg ND 330 05/10/17 12:2587.0
Indeno(1,2,3-cd)pyrene ug/kg ND 330 05/10/17 12:2568.0
Isophorone ug/kg ND 330 05/10/17 12:2574.0
N-Nitroso-di-n-propylamine ug/kg ND 330 05/10/17 12:2563.0
N-Nitrosodimethylamine ug/kg ND 330 05/10/17 12:25107
N-Nitrosodiphenylamine ug/kg ND 330 05/10/17 12:2598.0
Naphthalene ug/kg ND 330 05/10/17 12:2581.0
Nitrobenzene ug/kg ND 330 05/10/17 12:2590.0
Pentachlorophenol ug/kg ND 1650 05/10/17 12:2560.0
Phenanthrene ug/kg ND 330 05/10/17 12:2555.0
Phenol ug/kg ND 330 05/10/17 12:2599.0
Pyrene ug/kg ND 330 05/10/17 12:2556.0
2,4,6-Tribromophenol (S)%78 27-110 05/10/17 12:25
2-Fluorobiphenyl (S)%69 30-110 05/10/17 12:25
2-Fluorophenol (S)%70 13-110 05/10/17 12:25
Nitrobenzene-d5 (S)%68 23-110 05/10/17 12:25
Phenol-d6 (S)%70 22-110 05/10/17 12:25
Terphenyl-d14 (S)%89 28-110 05/10/17 12:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1995249LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1995250
1,2,4-Trichlorobenzene ug/kg 9091670 55 36-120681130 22 30
1,2-Dichlorobenzene ug/kg 8041670 48 41-120641070 28 30
1,3-Dichlorobenzene ug/kg 786 L216704766-120641070 30 30
1,4-Dichlorobenzene ug/kg 763 R116704642-120631050 31 30
1-Methylnaphthalene ug/kg 9561670 57 40-120671120 16 30
2,2'-Oxybis(1-chloropropane)ug/kg 7981670 48 17-12059985 21 30
2,4,5-Trichlorophenol ug/kg 10201670 61 37-120671120 9 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 73 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1995249LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1995250
2,4,6-Trichlorophenol ug/kg 10801670 65 40-120761260 16 30
2,4-Dichlorophenol ug/kg 10301670 62 33-120741240 19 30
2,4-Dimethylphenol ug/kg 10501670 63 36-120761270 19 30
2,4-Dinitrophenol ug/kg 60608330 73 22-121705860 3 30
2,4-Dinitrotoluene ug/kg 15401670 92 60-120871450 6 30
2,6-Dinitrotoluene ug/kg 14901670 89 54-120901500 0 30
2-Chloronaphthalene ug/kg 9161670 55 41-120671120 20 30
2-Chlorophenol ug/kg 8941670 54 39-120671120 22 30
2-Methylnaphthalene ug/kg 9391670 56 26-120701160 21 30
2-Methylphenol(o-Cresol)ug/kg 8491670 51 41-12059990 15 30
2-Nitroaniline ug/kg 24403330 73 45-120752490 2 30
2-Nitrophenol ug/kg 9511670 57 35-120731220 25 30
3&4-Methylphenol(m&p Cresol)ug/kg 8511670 51 35-12059977 14 30
3,3'-Dichlorobenzidine ug/kg 23303330 70 16-125692300 1 30
3-Nitroaniline ug/kg 25403330 76 45-120762520 1 30
4,6-Dinitro-2-methylphenol ug/kg 25703330 77 46-120752510 3 30
4-Bromophenylphenyl ether ug/kg 12001670 72 36-120711190 1 30
4-Chloro-3-methylphenol ug/kg 23103330 69 37-120792620 13 30
4-Chloroaniline ug/kg 18603330 56 35-120712370 24 30
4-Chlorophenylphenyl ether ug/kg 10601670 64 30-120701160 9 30
4-Nitroaniline ug/kg 27803330 83 48-120782610 6 30
4-Nitrophenol ug/kg 62508330 75 43-120695720 9 30
Acenaphthene ug/kg 9961670 60 46-120681130 13 30
Acenaphthylene ug/kg 9781670 59 46-120681140 15 30
Aniline ug/kg 6971670 42 33-12052867 22 30
Anthracene ug/kg 12701670 76 63-120731210 5 30
Benzo(a)anthracene ug/kg 12101670 73 61-120731220 0 30
Benzo(a)pyrene ug/kg 11801670 71 59-120701160 2 30
Benzo(b)fluoranthene ug/kg 11801670 71 55-120681130 4 30
Benzo(g,h,i)perylene ug/kg 11901670 72 57-120731220 2 30
Benzo(k)fluoranthene ug/kg 11901670 71 56-120671120 6 30
Benzoic Acid ug/kg 51308330 62 13-120604980 3 30
Benzyl alcohol ug/kg 18603330 56 34-120662200 17 30
bis(2-Chloroethoxy)methane ug/kg 8791670 53 21-120671120 24 30
bis(2-Chloroethyl) ether ug/kg 7911670 47 25-120621030 27 30
bis(2-Ethylhexyl)phthalate ug/kg 15201670 91 56-123871440 5 30
Butylbenzylphthalate ug/kg 13901670 83 57-120851420 2 30
Chrysene ug/kg 11801670 71 64-120701170 0 30
Di-n-butylphthalate ug/kg 14101670 85 58-120781300 8 30
Di-n-octylphthalate ug/kg 13601670 82 47-121791320 3 30
Dibenz(a,h)anthracene ug/kg 12801670 77 56-120761270 0 30
Dibenzofuran ug/kg 10301670 62 43-120681130 9 30
Diethylphthalate ug/kg 13001670 78 55-120721210 7 30
Dimethylphthalate ug/kg 12201670 73 54-120731210 0 30
Fluoranthene ug/kg 13101670 79 61-120731210 8 30
Fluorene ug/kg 11201670 67 51-120721190 7 30
Hexachloro-1,3-butadiene ug/kg 8601670 52 22-120681140 28 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 74 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1995249LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1995250
Hexachlorobenzene ug/kg 12201670 73 53-120721200 2 30
Hexachlorocyclopentadiene ug/kg 826 R116705018-150681140 32 30
Hexachloroethane ug/kg 767 R116704639-120641070 33 30
Indeno(1,2,3-cd)pyrene ug/kg 12301670 74 58-120751260 2 30
Isophorone ug/kg 11401670 68 38-120831380 19 30
N-Nitroso-di-n-propylamine ug/kg 9121670 55 30-120641070 16 30
N-Nitrosodimethylamine ug/kg 824 R116704932-120691160 34 30
N-Nitrosodiphenylamine ug/kg 12101670 73 50-120701170 4 30
Naphthalene ug/kg 9021670 54 38-120661100 20 30
Nitrobenzene ug/kg 10201670 61 37-120761270 22 30
Pentachlorophenol ug/kg 27403330 82 10-120772570 6 30
Phenanthrene ug/kg 12301670 74 62-120691160 7 30
Phenol ug/kg 9921670 60 37-120711180 18 30
Pyrene ug/kg 12401670 74 63-120761270 2 30
2,4,6-Tribromophenol (S)%81 27-11078
2-Fluorobiphenyl (S)%55 30-11066
2-Fluorophenol (S)%50 13-11066
Nitrobenzene-d5 (S)%54 23-11069
Phenol-d6 (S)%55 22-11066
Terphenyl-d14 (S)%86 28-11086
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 75 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
359747
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples: 92339291001, 92339291002, 92339291003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1995040
Associated Lab Samples:92339291001, 92339291002, 92339291003
Matrix: Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 05/10/17 11:241.9
1,2-Dichlorobenzene ug/L ND 10.0 05/10/17 11:241.2
1,3-Dichlorobenzene ug/L ND 10.0 05/10/17 11:241.1
1,4-Dichlorobenzene ug/L ND 10.0 05/10/17 11:241.2
1-Methylnaphthalene ug/L ND 10.0 05/10/17 11:240.32
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 05/10/17 11:241.6
2,4,5-Trichlorophenol ug/L ND 10.0 05/10/17 11:242.2
2,4,6-Trichlorophenol ug/L ND 10.0 05/10/17 11:241.9
2,4-Dichlorophenol ug/L ND 10.0 05/10/17 11:241.7
2,4-Dimethylphenol ug/L ND 10.0 05/10/17 11:242.2
2,4-Dinitrophenol ug/L ND 50.0 05/10/17 11:246.5
2,4-Dinitrotoluene ug/L ND 10.0 05/10/17 11:241.2
2,6-Dinitrotoluene ug/L ND 10.0 05/10/17 11:241.7
2-Chloronaphthalene ug/L ND 10.0 05/10/17 11:242.2
2-Chlorophenol ug/L ND 10.0 05/10/17 11:241.5
2-Methylnaphthalene ug/L ND 10.0 05/10/17 11:240.28
2-Methylphenol(o-Cresol)ug/L ND 10.0 05/10/17 11:241.7
2-Nitroaniline ug/L ND 50.0 05/10/17 11:242.8
2-Nitrophenol ug/L ND 10.0 05/10/17 11:241.7
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 05/10/17 11:241.7
3,3'-Dichlorobenzidine ug/L 1.5J 20.0 05/10/17 11:241.4
3-Nitroaniline ug/L ND 50.0 05/10/17 11:242.4
4,6-Dinitro-2-methylphenol ug/L ND 20.0 05/10/17 11:241.7
4-Bromophenylphenyl ether ug/L ND 10.0 05/10/17 11:241.3
4-Chloro-3-methylphenol ug/L ND 20.0 05/10/17 11:244.2
4-Chloroaniline ug/L ND 20.0 05/10/17 11:243.4
4-Chlorophenylphenyl ether ug/L ND 10.0 05/10/17 11:242.1
4-Nitroaniline ug/L ND 20.0 05/10/17 11:242.5
4-Nitrophenol ug/L ND 50.0 05/10/17 11:245.8
Acenaphthene ug/L ND 10.0 05/10/17 11:240.25
Acenaphthylene ug/L ND 10.0 05/10/17 11:240.21
Aniline ug/L ND 10.0 05/10/17 11:241.3
Anthracene ug/L ND 10.0 05/10/17 11:240.14
Benzo(a)anthracene ug/L ND 10.0 05/10/17 11:240.33
Benzo(a)pyrene ug/L ND 10.0 05/10/17 11:240.30
Benzo(b)fluoranthene ug/L ND 10.0 05/10/17 11:240.28
Benzo(g,h,i)perylene ug/L ND 10.0 05/10/17 11:240.38
Benzo(k)fluoranthene ug/L ND 10.0 05/10/17 11:240.43
Benzoic Acid ug/L ND 50.0 05/10/17 11:2411.1
Benzyl alcohol ug/L ND 20.0 05/10/17 11:243.4
bis(2-Chloroethoxy)methane ug/L ND 10.0 05/10/17 11:241.7
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1995040
Associated Lab Samples:92339291001, 92339291002, 92339291003
Matrix: Water
AnalyzedMDL
bis(2-Chloroethyl) ether ug/L ND 10.0 05/10/17 11:241.5
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 05/10/17 11:240.85
Butylbenzylphthalate ug/L ND 10.0 05/10/17 11:240.75
Chrysene ug/L ND 10.0 05/10/17 11:240.21
Di-n-butylphthalate ug/L ND 10.0 05/10/17 11:241.1
Di-n-octylphthalate ug/L 1.3J 10.0 05/10/17 11:240.86
Dibenz(a,h)anthracene ug/L ND 10.0 05/10/17 11:240.55
Dibenzofuran ug/L ND 10.0 05/10/17 11:241.8
Diethylphthalate ug/L ND 10.0 05/10/17 11:241.3
Dimethylphthalate ug/L ND 10.0 05/10/17 11:241.5
Fluoranthene ug/L ND 10.0 05/10/17 11:240.21
Fluorene ug/L ND 10.0 05/10/17 11:240.21
Hexachloro-1,3-butadiene ug/L ND 10.0 05/10/17 11:241.8
Hexachlorobenzene ug/L ND 10.0 05/10/17 11:241.1
Hexachlorocyclopentadiene ug/L ND 10.0 05/10/17 11:241.8
Hexachloroethane ug/L ND 10.0 05/10/17 11:241.5
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 05/10/17 11:240.29
Isophorone ug/L ND 10.0 05/10/17 11:241.8
N-Nitroso-di-n-propylamine ug/L ND 10.0 05/10/17 11:242.1
N-Nitrosodimethylamine ug/L ND 10.0 05/10/17 11:241.3
N-Nitrosodiphenylamine ug/L ND 10.0 05/10/17 11:241.3
Naphthalene ug/L ND 10.0 05/10/17 11:240.34
Nitrobenzene ug/L ND 10.0 05/10/17 11:241.7
Pentachlorophenol ug/L ND 25.0 05/10/17 11:242.3
Phenanthrene ug/L ND 10.0 05/10/17 11:240.22
Phenol ug/L ND 10.0 05/10/17 11:241.7
Pyrene ug/L ND 10.0 05/10/17 11:240.19
2,4,6-Tribromophenol (S)%51 27-110 05/10/17 11:24
2-Fluorobiphenyl (S)%36 27-110 05/10/17 11:24
2-Fluorophenol (S)%19 12-110 05/10/17 11:24
Nitrobenzene-d5 (S)%36 21-110 05/10/17 11:24
Phenol-d6 (S)%14 10-110 05/10/17 11:24
Terphenyl-d14 (S)%73 31-107 05/10/17 11:24
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1995041LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 35.050 70 31-120
1,2-Dichlorobenzene ug/L 31.150 62 38-120
1,3-Dichlorobenzene ug/L 29.750 59 30-122
1,4-Dichlorobenzene ug/L 29.750 59 37-120
1-Methylnaphthalene ug/L 39.050 78 34-113
2,2'-Oxybis(1-chloropropane)ug/L 38.950 78 18-120
2,4,5-Trichlorophenol ug/L 38.650 77 43-113
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
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Huntersville, NC 28078
[phone]
Page 77 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1995041LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,6-Trichlorophenol ug/L 44.350 89 42-120
2,4-Dichlorophenol ug/L 40.850 82 30-120
2,4-Dimethylphenol ug/L 41.550 83 29-111
2,4-Dinitrophenol ug/L 206250 82 19-132
2,4-Dinitrotoluene ug/L 52.650 105 58-128
2,6-Dinitrotoluene ug/L 52.650 105 54-129
2-Chloronaphthalene ug/L 46.450 93 43-117
2-Chlorophenol ug/L 35.850 72 37-120
2-Methylnaphthalene ug/L 39.650 79 33-120
2-Methylphenol(o-Cresol)ug/L 30.450 61 31-120
2-Nitroaniline ug/L 80.5100 80 48-121
2-Nitrophenol ug/L 40.350 81 25-116
3&4-Methylphenol(m&p Cresol)ug/L 63.3 L150127 23-120
3,3'-Dichlorobenzidine ug/L 88.3100 88 10-154
3-Nitroaniline ug/L 89.0100 89 43-115
4,6-Dinitro-2-methylphenol ug/L 85.1100 85 44-124
4-Bromophenylphenyl ether ug/L 41.950 84 34-113
4-Chloro-3-methylphenol ug/L 83.6100 84 31-110
4-Chloroaniline ug/L 82.3100 82 20-120
4-Chlorophenylphenyl ether ug/L 41.550 83 34-116
4-Nitroaniline ug/L 93.0100 93 46-128
4-Nitrophenol ug/L 94.2250 38 11-120
Acenaphthene ug/L 43.150 86 48-114
Acenaphthylene ug/L 41.350 83 48-112
Aniline ug/L 27.050 54 26-120
Anthracene ug/L 43.350 87 57-118
Benzo(a)anthracene ug/L 44.450 89 56-121
Benzo(a)pyrene ug/L 42.850 86 55-127
Benzo(b)fluoranthene ug/L 44.750 89 53-128
Benzo(g,h,i)perylene ug/L 42.950 86 54-125
Benzo(k)fluoranthene ug/L 43.150 86 51-123
Benzoic Acid ug/L 76.1250 30 10-120
Benzyl alcohol ug/L 64.6100 65 27-120
bis(2-Chloroethoxy)methane ug/L 41.250 82 32-120
bis(2-Chloroethyl) ether ug/L 37.650 75 33-111
bis(2-Ethylhexyl)phthalate ug/L 53.450 107 50-145
Butylbenzylphthalate ug/L 54.150 108 54-138
Chrysene ug/L 43.750 87 58-127
Di-n-butylphthalate ug/L 47.150 94 56-125
Di-n-octylphthalate ug/L 52.450 105 50-134
Dibenz(a,h)anthracene ug/L 43.050 86 53-129
Dibenzofuran ug/L 41.950 84 45-120
Diethylphthalate ug/L 43.950 88 53-120
Dimethylphthalate ug/L 43.850 88 55-116
Fluoranthene ug/L 42.950 86 57-125
Fluorene ug/L 42.150 84 53-118
Hexachloro-1,3-butadiene ug/L 31.850 64 23-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
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[phone]
Page 78 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1995041LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/L 42.650 85 49-116
Hexachlorocyclopentadiene ug/L 30.350 61 26-158
Hexachloroethane ug/L 30.650 61 30-114
Indeno(1,2,3-cd)pyrene ug/L 43.450 87 55-128
Isophorone ug/L 49.550 99 31-118
N-Nitroso-di-n-propylamine ug/L 40.950 82 32-119
N-Nitrosodimethylamine ug/L 23.050 46 13-120
N-Nitrosodiphenylamine ug/L 42.950 86 43-120
Naphthalene ug/L 37.650 75 32-120
Nitrobenzene ug/L 44.250 88 33-110
Pentachlorophenol ug/L 85.5100 86 10-137
Phenanthrene ug/L 42.050 84 57-117
Phenol ug/L 17.750 35 10-120
Pyrene ug/L 46.950 94 55-122
2,4,6-Tribromophenol (S)%89 27-110
2-Fluorobiphenyl (S)%74 27-110
2-Fluorophenol (S)%42 12-110
Nitrobenzene-d5 (S)%77 21-110
Phenol-d6 (S)%30 10-110
Terphenyl-d14 (S)%106 31-107
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 79 of 86
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339291
BANK STREET
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
359136
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples: 92339291004, 92339291005, 92339291006, 92339291007, 92339291008
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92339291004
1991712SAMPLE DUPLICATE:
Percent Moisture %14.5 2 2514.3
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92339315015
1991713SAMPLE DUPLICATE:
Percent Moisture %20.5 2 2520.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
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Huntersville, NC 28078
[phone]
Page 80 of 86
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92339291
BANK STREET
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associatedsamples may be biased high.L1
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associatedsamples may be biased low.L2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 81 of 86
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92339291
BANK STREET
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92339291004 359091 359213SB-1(17-18)EPA 3546 EPA 8082
92339291005 359091 359213SB-3(14-15)EPA 3546 EPA 8082
92339291006 359091 359213SB-4(5-6)EPA 3546 EPA 8082
92339291007 359091 359213SB-6(14-15)EPA 3546 EPA 8082
92339291008 359091 359213SB-7(3-5)EPA 3546 EPA 8082
92339291001 359665 359851TMW-7 EPA 3510 EPA 8082
92339291002 359665 359851TMW-4 EPA 3510 EPA 8082
92339291003 359665 359851TMW-1 EPA 3510 EPA 8082
92339291004 359181 359382SB-1(17-18)EPA 3050 EPA 6010
92339291005 359181 359382SB-3(14-15)EPA 3050 EPA 6010
92339291006 359181 359382SB-4(5-6)EPA 3050 EPA 6010
92339291007 359181 359382SB-6(14-15)EPA 3050 EPA 6010
92339291008 359181 359382SB-7(3-5)EPA 3050 EPA 6010
92339291001 359154 359363TMW-7 EPA 3010A EPA 6010
92339291002 359154 359363TMW-4 EPA 3010A EPA 6010
92339291003 359157 359364TMW-1 EPA 3010A EPA 6010
92339291001 359271 359294TMW-7 EPA 7470 EPA 7470
92339291002 359271 359294TMW-4 EPA 7470 EPA 7470
92339291003 359272 359295TMW-1 EPA 7470 EPA 7470
92339291004 359634 359846SB-1(17-18)EPA 7471 EPA 7471
92339291005 359634 359846SB-3(14-15)EPA 7471 EPA 7471
92339291006 359634 359846SB-4(5-6)EPA 7471 EPA 7471
92339291007 359634 359846SB-6(14-15)EPA 7471 EPA 7471
92339291008 359634 359846SB-7(3-5)EPA 7471 EPA 7471
92339291004 359093 359186SB-1(17-18)EPA 3546 EPA 8270
92339291005 359761 359945SB-3(14-15)EPA 3546 EPA 8270
92339291006 359761 359945SB-4(5-6)EPA 3546 EPA 8270
92339291007 359093 359186SB-6(14-15)EPA 3546 EPA 8270
92339291008 359093 359186SB-7(3-5)EPA 3546 EPA 8270
92339291001 359747 359895TMW-7 EPA 3510 EPA 8270
92339291002 359747 359895TMW-4 EPA 3510 EPA 8270
92339291003 359747 359895TMW-1 EPA 3510 EPA 8270
92339291001 359430TMW-7 EPA 8260
92339291002 359493TMW-4 EPA 8260
92339291003 359493TMW-1 EPA 8260
92339291004 359368SB-1(17-18)EPA 8260
92339291005 359368SB-3(14-15)EPA 8260
92339291006 359368SB-4(5-6)EPA 8260
92339291007 359368SB-6(14-15)EPA 8260
92339291008 359368SB-7(3-5)EPA 8260
92339291004 359136SB-1(17-18)ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 82 of 86
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92339291
BANK STREET
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92339291005 359136SB-3(14-15)ASTM D2974-87
92339291006 359136SB-4(5-6)ASTM D2974-87
92339291007 359136SB-6(14-15)ASTM D2974-87
92339291008 359136SB-7(3-5)ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/10/2017 05:48 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 83 of 86
Page 84 of 86
Page 85 of 86
Page 86 of 86