RA-1137_7489_CA_RPTS_20180118_NPDES2017QTR4

102-A Woodwinds Industrial Court
Cary NC, 27511
919.467.3090 919.467.3515Phone:FAX:
ENCO Workorder(s): CA17337
Durham, NC 27703
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative. This report shall not be reproduced except in full, without
the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Enclosure(s)
Project Number: 7023, Project Name/Desc: Dixie
Attn: Justin Abreu
EMS Environmental (EM001)
117 South Hoover Road
Chuck Smith
Project Manager
Thursday, December 7, 2017
RE: Laboratory Results for
Dear Justin Abreu,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Monday, November 27, 2017.
Enclosure(s)
Page 1 of 23This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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SAMPLE SUMMARY/LABORATORY CHRONICLE
Influent 4th Qtr 2017 CA17337-01 Sampled:11/27/17 11:38 Received:11/27/17 14:55Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
SM 6200B-1997 12/11/17 12/05/17 11:34 12/05/17 16:11
Effluent 4th Qtr 2017 CA17337-02 Sampled:11/27/17 11:47 Received:11/27/17 14:55Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 1664B 12/25/17 11/28/17 11:26 11/29/17 15:47
EPA 420.1 12/25/17 12/06/17 08:45 12/07/17 10:05
EPA 6010D 11/30/17 11/29/17 15:01 11/30/17 12:3205/28/18
EPA 625 12/04/17 11/28/17 08:18 12/01/17 15:2901/07/18
SM 2540D-1997 12/04/17 12/04/17 14:25 12/04/17 14:25
SM 6200B-1997 12/11/17 12/05/17 11:34 12/05/17 16:41
SVE Effluent 4th Qtr 2017 CA17337-03 Sampled:11/27/17 11:36 Received:11/27/17 14:55Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
Method 18 Modified 11/30/17 11/29/17 16:09 11/29/17 20:54
SVE Effluent 4th Qtr 2017 CA17337-03RE1 Sampled:11/27/17 11:36 Received:11/27/17 14:55Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
Method 18 Modified 11/30/17 11/29/17 16:09 11/29/17 22:37
Trip Blank CA17337-04 Sampled:11/27/17 11:36 Received:11/27/17 14:55Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
SM 6200B-1997 12/11/17 12/05/17 11:34 12/05/17 15:41
Page 2 of 23This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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SAMPLE DETECTION SUMMARY
Lab ID:Client ID:Influent 4th Qtr 2017 CA17337-01
Analyte MethodUnitsPQLResultsFlag NotesMDL
200 5.0 ug/L SM 6200B-1997D 1,2,4-Trimethylbenzene 0.34
4.3 5.0 ug/L SM 6200B-1997JD 1,2-Dibromoethane 2.1
8.6 5.0 ug/L SM 6200B-1997D 1,2-Dichloroethane 0.41
62 5.0 ug/L SM 6200B-1997D 1,3,5-Trimethylbenzene 0.50
720 5.0 ug/L SM 6200B-1997D Benzene 0.25
97 5.0 ug/L SM 6200B-1997D Ethylbenzene 0.50
8.9 5.0 ug/L SM 6200B-1997D Isopropylbenzene 0.65
440 10 ug/L SM 6200B-1997D m,p-Xylenes 0.90
28 5.0 ug/L SM 6200B-1997D Methyl-tert-Butyl Ether 0.60
68 5.0 ug/L SM 6200B-1997D Naphthalene 0.43
16 5.0 ug/L SM 6200B-1997D n-Butyl Benzene 0.37
9.2 5.0 ug/L SM 6200B-1997D n-Propyl Benzene 0.36
300 5.0 ug/L SM 6200B-1997D o-Xylene 0.44
570 5.0 ug/L SM 6200B-1997D Toluene 0.26
740 5.0 ug/L SM 6200B-1997D Xylenes (Total)1.1
Lab ID:Client ID:SVE Effluent 4th Qtr 2017 CA17337-03
Analyte MethodUnitsPQLResultsFlag NotesMDL
0.26 0.032 mg/m‡ Air Method 18 Modified Benzene 0.0029
0.079 0.043 mg/m‡ Air Method 18 Modified Ethylbenzene 0.0040
33 3.7 mg/m‡ Air Method 18 Modified Total Light Petroleum Hydrocarbons 3.7
1.2 0.043 mg/m‡ Air Method 18 Modified Xylenes (Total)0.0078
Lab ID:Client ID:SVE Effluent 4th Qtr 2017 CA17337-03RE1
Analyte MethodUnitsPQLResultsFlag NotesMDL
1.7 0.38 mg/m‡ Air Method 18 Modified Toluene 0.030
Page 3 of 23This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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ANALYTICAL RESULTS
Influent 4th Qtr 2017Description:Lab Sample ID:CA17337-01 11/27/17 14:55Received:
CA17337Work Order:11/27/17 11:38Sampled:Waste WaterMatrix:
Justin AbreuSampled By:Project:Dixie
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 12/05/17 16:111,1,1,2-Tetrachloroethane [630-20-6]^0.46 MRK7L050185.00.46 UD 5
ug/L SM 6200B-1997 12/05/17 16:111,1,1-Trichloroethane [71-55-6]^0.75 MRK7L050185.00.75 UD 5
ug/L SM 6200B-1997 12/05/17 16:111,1,2,2-Tetrachloroethane [79-34-5]^0.42 MRK7L050185.00.42 UD 5
ug/L SM 6200B-1997 12/05/17 16:111,1,2-Trichloroethane [79-00-5]^0.34 MRK7L050185.00.34 UD 5
ug/L SM 6200B-1997 12/05/17 16:111,1-Dichloroethane [75-34-3]^0.25 MRK7L050185.00.25 UD 5
ug/L SM 6200B-1997 12/05/17 16:111,1-Dichloroethene [75-35-4]^0.75 MRK7L050185.00.75 UD 5
ug/L SM 6200B-1997 12/05/17 16:111,1-Dichloropropene [563-58-6]^0.32 MRK7L050185.00.32 UD 5
ug/L SM 6200B-1997 12/05/17 16:111,2,3-Trichlorobenzene [87-61-6]^1.2 MRK7L050185.01.2 UD 5
ug/L SM 6200B-1997 12/05/17 16:111,2,3-Trichloropropane [96-18-4]^0.75 MRK7L050185.00.75 UD 5
ug/L SM 6200B-1997 12/05/17 16:111,2,4-Trichlorobenzene [120-82-1]^0.48 MRK7L050185.00.48 UD 5
ug/L SM 6200B-1997 12/05/17 16:111,2,4-Trimethylbenzene [95-63-6]^0.34 MRK7L050185.0200D 5
ug/L SM 6200B-1997 12/05/17 16:111,2-Dibromo-3-chloropropane [96-12-8]^2.4 MRK7L050185.02.4 UD 5
ug/L SM 6200B-1997 12/05/17 16:111,2-Dibromoethane [106-93-4]^2.1 MRK7L050185.04.3 JD 5
ug/L SM 6200B-1997 12/05/17 16:111,2-Dichlorobenzene [95-50-1]^0.26 MRK7L050185.00.26 UD 5
ug/L SM 6200B-1997 12/05/17 16:111,2-Dichloroethane [107-06-2]^0.41 MRK7L050185.08.6 D 5
ug/L SM 6200B-1997 12/05/17 16:111,2-Dichloropropane [78-87-5]^0.49 MRK7L050185.00.49 UD 5
ug/L SM 6200B-1997 12/05/17 16:111,3,5-Trimethylbenzene [108-67-8]^0.50 MRK7L050185.062D 5
ug/L SM 6200B-1997 12/05/17 16:111,3-Dichlorobenzene [541-73-1]^0.46 MRK7L050185.00.46 UD 5
ug/L SM 6200B-1997 12/05/17 16:111,3-Dichloropropane [142-28-9]^0.75 MRK7L050185.00.75 UD 5
ug/L SM 6200B-1997 12/05/17 16:111,4-Dichlorobenzene [106-46-7]^0.50 MRK7L050185.00.50 UD 5
ug/L SM 6200B-1997 12/05/17 16:112,2-Dichloropropane [594-20-7]^0.60 MRK7L050185.00.60 UD 5
ug/L SM 6200B-1997 12/05/17 16:112-Chlorotoluene [95-49-8]^0.50 MRK7L050185.00.50 UD 5
ug/L SM 6200B-1997 12/05/17 16:114-Chlorotoluene [106-43-4]^0.50 MRK7L050185.00.50 UD 5
ug/L SM 6200B-1997 12/05/17 16:114-Isopropyltoluene [99-87-6]^0.33 MRK7L050185.00.33 UD 5
ug/L SM 6200B-1997 12/05/17 16:11Benzene [71-43-2]^0.25 MRK7L050185.0720D 5
ug/L SM 6200B-1997 12/05/17 16:11Bromobenzene [108-86-1]^0.65 MRK7L050185.00.65 UD 5
ug/L SM 6200B-1997 12/05/17 16:11Bromochloromethane [74-97-5]^0.55 MRK7L050185.00.55 UD 5
ug/L SM 6200B-1997 12/05/17 16:11Bromodichloromethane [75-27-4]^0.50 MRK7L050185.00.50 UD 5
ug/L SM 6200B-1997 12/05/17 16:11Bromoform [75-25-2]^1.0 MRK7L050185.01.0 UD 5
ug/L SM 6200B-1997 12/05/17 16:11Bromomethane [74-83-9]^1.4 MRK7L050185.01.4 UD 5
ug/L SM 6200B-1997 12/05/17 16:11Carbon Tetrachloride [56-23-5]^0.41 MRK7L050185.00.41 UD 5
ug/L SM 6200B-1997 12/05/17 16:11Chlorobenzene [108-90-7]^0.34 MRK7L050185.00.34 UD 5
ug/L SM 6200B-1997 12/05/17 16:11Chloroethane [75-00-3]^0.90 MRK7L050185.00.90 UD 5
ug/L SM 6200B-1997 12/05/17 16:11Chloroform [67-66-3]^0.42 MRK7L050185.00.42 UD 5
ug/L SM 6200B-1997 12/05/17 16:11Chloromethane [74-87-3]^0.25 MRK7L050185.00.25 UD 5
ug/L SM 6200B-1997 12/05/17 16:11cis-1,2-Dichloroethene [156-59-2]^0.38 MRK7L050185.00.38 UD 5
ug/L SM 6200B-1997 12/05/17 16:11cis-1,3-Dichloropropene [10061-01-5]^0.36 MRK7L050185.00.36 UD 5
ug/L SM 6200B-1997 12/05/17 16:11Dibromochloromethane [124-48-1]^0.34 MRK7L050185.00.34 UD 5
ug/L SM 6200B-1997 12/05/17 16:11Dibromomethane [74-95-3]^0.65 MRK7L050185.00.65 UD 5
ug/L SM 6200B-1997 12/05/17 16:11Dichlorodifluoromethane [75-71-8]^0.46 MRK7L050185.00.46 UD 5
ug/L SM 6200B-1997 12/05/17 16:11Ethylbenzene [100-41-4]^0.50 MRK7L050185.097D 5
ug/L SM 6200B-1997 12/05/17 16:11Freon 113 [76-13-1]^1.8 MRK7L050185.01.8 UD 5
ug/L SM 6200B-1997 12/05/17 16:11Hexachlorobutadiene [87-68-3]^0.75 MRK7L050185.00.75 UD 5
ug/L SM 6200B-1997 12/05/17 16:11Isopropyl Ether [108-20-3]^1.0 MRK7L050185.01.0 UD 5
ug/L SM 6200B-1997 12/05/17 16:11Isopropylbenzene [98-82-8]^0.65 MRK7L050185.08.9 D 5
ug/L SM 6200B-1997 12/05/17 16:11m,p-Xylenes [108-38-3/106-42-3]^0.90 MRK7L0501810440D 5
ug/L SM 6200B-1997 12/05/17 16:11Methylene Chloride [75-09-2]^0.35 MRK7L05018100.35 UD 5
Page 4 of 23This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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ANALYTICAL RESULTS
Influent 4th Qtr 2017Description:Lab Sample ID:CA17337-01 11/27/17 14:55Received:
CA17337Work Order:11/27/17 11:38Sampled:Waste WaterMatrix:
Justin AbreuSampled By:Project:Dixie
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 12/05/17 16:11Methyl-tert-Butyl Ether [1634-04-4]^0.60 MRK7L050185.028D 5
ug/L SM 6200B-1997 12/05/17 16:11Naphthalene [91-20-3]^0.43 MRK7L050185.068D 5
ug/L SM 6200B-1997 12/05/17 16:11n-Butyl Benzene [104-51-8]^0.37 MRK7L050185.016D 5
ug/L SM 6200B-1997 12/05/17 16:11n-Propyl Benzene [103-65-1]^0.36 MRK7L050185.09.2 D 5
ug/L SM 6200B-1997 12/05/17 16:11o-Xylene [95-47-6]^0.44 MRK7L050185.0300D 5
ug/L SM 6200B-1997 12/05/17 16:11sec-Butylbenzene [135-98-8]^0.26 MRK7L050185.00.26 UD 5
ug/L SM 6200B-1997 12/05/17 16:11Styrene [100-42-5]^0.41 MRK7L050185.00.41 UD 5
ug/L SM 6200B-1997 12/05/17 16:11tert-Butylbenzene [98-06-6]^0.47 MRK7L050185.00.47 UD 5
ug/L SM 6200B-1997 12/05/17 16:11Tetrachloroethene [127-18-4]^0.50 MRK7L050185.00.50 UD 5
ug/L SM 6200B-1997 12/05/17 16:11Toluene [108-88-3]^0.26 MRK7L050185.0570D 5
ug/L SM 6200B-1997 12/05/17 16:11trans-1,2-Dichloroethene [156-60-5]^0.55 MRK7L050185.00.55 UD 5
ug/L SM 6200B-1997 12/05/17 16:11trans-1,3-Dichloropropene [10061-02-6]^0.40 MRK7L050185.00.40 UD 5
ug/L SM 6200B-1997 12/05/17 16:11Trichloroethene [79-01-6]^0.65 MRK7L050185.00.65 UD 5
ug/L SM 6200B-1997 12/05/17 16:11Trichlorofluoromethane [75-69-4]^0.75 MRK7L050185.00.75 UD 5
ug/L SM 6200B-1997 12/05/17 16:11Vinyl chloride [75-01-4]^0.42 MRK7L050185.00.42 UD 5
ug/L SM 6200B-1997 12/05/17 16:11Xylenes (Total) [1330-20-7]^1.1 MRK7L050185.0740D 5
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 70-13083 %MRKSM 6200B-1997 12/05/17 16:117L050184150.0 1
Dibromofluoromethane 70-13087 %MRKSM 6200B-1997 12/05/17 16:117L050184350.0 1
Toluene-d8 70-13091 %MRKSM 6200B-1997 12/05/17 16:117L050184550.0 1
Page 5 of 23This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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ANALYTICAL RESULTS
Effluent 4th Qtr 2017Description:Lab Sample ID:CA17337-02 11/27/17 14:55Received:
CA17337Work Order:11/27/17 11:47Sampled:Waste WaterMatrix:
Justin AbreuSampled By:Project:Dixie
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 12/05/17 16:411,1,1,2-Tetrachloroethane [630-20-6]^0.091 MRK7L050181.00.091 U 1
ug/L SM 6200B-1997 12/05/17 16:411,1,1-Trichloroethane [71-55-6]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 16:411,1,2,2-Tetrachloroethane [79-34-5]^0.085 MRK7L050181.00.085 U 1
ug/L SM 6200B-1997 12/05/17 16:411,1,2-Trichloroethane [79-00-5]^0.068 MRK7L050181.00.068 U 1
ug/L SM 6200B-1997 12/05/17 16:411,1-Dichloroethane [75-34-3]^0.050 MRK7L050181.00.050 U 1
ug/L SM 6200B-1997 12/05/17 16:411,1-Dichloroethene [75-35-4]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 16:411,1-Dichloropropene [563-58-6]^0.063 MRK7L050181.00.063 U 1
ug/L SM 6200B-1997 12/05/17 16:411,2,3-Trichlorobenzene [87-61-6]^0.25 MRK7L050181.00.25 U 1
ug/L SM 6200B-1997 12/05/17 16:411,2,3-Trichloropropane [96-18-4]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 16:411,2,4-Trichlorobenzene [120-82-1]^0.097 MRK7L050181.00.097 U 1
ug/L SM 6200B-1997 12/05/17 16:411,2,4-Trimethylbenzene [95-63-6]^0.067 MRK7L050181.00.067 U 1
ug/L SM 6200B-1997 12/05/17 16:411,2-Dibromo-3-chloropropane [96-12-8]^0.48 MRK7L050181.00.48 U 1
ug/L SM 6200B-1997 12/05/17 16:411,2-Dibromoethane [106-93-4]^0.42 MRK7L050181.00.42 U 1
ug/L SM 6200B-1997 12/05/17 16:411,2-Dichlorobenzene [95-50-1]^0.052 MRK7L050181.00.052 U 1
ug/L SM 6200B-1997 12/05/17 16:411,2-Dichloroethane [107-06-2]^0.082 MRK7L050181.00.082 U 1
ug/L SM 6200B-1997 12/05/17 16:411,2-Dichloropropane [78-87-5]^0.098 MRK7L050181.00.098 U 1
ug/L SM 6200B-1997 12/05/17 16:411,3,5-Trimethylbenzene [108-67-8]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 16:411,3-Dichlorobenzene [541-73-1]^0.092 MRK7L050181.00.092 U 1
ug/L SM 6200B-1997 12/05/17 16:411,3-Dichloropropane [142-28-9]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 16:411,4-Dichlorobenzene [106-46-7]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 16:412,2-Dichloropropane [594-20-7]^0.12 MRK7L050181.00.12 U 1
ug/L SM 6200B-1997 12/05/17 16:412-Chlorotoluene [95-49-8]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 16:414-Chlorotoluene [106-43-4]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 16:414-Isopropyltoluene [99-87-6]^0.066 MRK7L050181.00.066 U 1
ug/L SM 6200B-1997 12/05/17 16:41Benzene [71-43-2]^0.050 MRK7L050181.00.050 U 1
ug/L SM 6200B-1997 12/05/17 16:41Bromobenzene [108-86-1]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 16:41Bromochloromethane [74-97-5]^0.11 MRK7L050181.00.11 U 1
ug/L SM 6200B-1997 12/05/17 16:41Bromodichloromethane [75-27-4]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 16:41Bromoform [75-25-2]^0.20 MRK7L050181.00.20 U 1
ug/L SM 6200B-1997 12/05/17 16:41Bromomethane [74-83-9]^0.28 MRK7L050181.00.28 U 1
ug/L SM 6200B-1997 12/05/17 16:41Carbon Tetrachloride [56-23-5]^0.082 MRK7L050181.00.082 U 1
ug/L SM 6200B-1997 12/05/17 16:41Chlorobenzene [108-90-7]^0.069 MRK7L050181.00.069 U 1
ug/L SM 6200B-1997 12/05/17 16:41Chloroethane [75-00-3]^0.18 MRK7L050181.00.18 U 1
ug/L SM 6200B-1997 12/05/17 16:41Chloroform [67-66-3]^0.083 MRK7L050181.00.083 U 1
ug/L SM 6200B-1997 12/05/17 16:41Chloromethane [74-87-3]^0.050 MRK7L050181.00.050 U 1
ug/L SM 6200B-1997 12/05/17 16:41cis-1,2-Dichloroethene [156-59-2]^0.075 MRK7L050181.00.075 U 1
ug/L SM 6200B-1997 12/05/17 16:41cis-1,3-Dichloropropene [10061-01-5]^0.073 MRK7L050181.00.073 U 1
ug/L SM 6200B-1997 12/05/17 16:41Dibromochloromethane [124-48-1]^0.067 MRK7L050181.00.067 U 1
ug/L SM 6200B-1997 12/05/17 16:41Dibromomethane [74-95-3]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 16:41Dichlorodifluoromethane [75-71-8]^0.091 MRK7L050181.00.091 U 1
ug/L SM 6200B-1997 12/05/17 16:41Ethylbenzene [100-41-4]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 16:41Freon 113 [76-13-1]^0.35 MRK7L050181.00.35 U 1
ug/L SM 6200B-1997 12/05/17 16:41Hexachlorobutadiene [87-68-3]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 16:41Isopropyl Ether [108-20-3]^0.21 MRK7L050181.00.21 U 1
ug/L SM 6200B-1997 12/05/17 16:41Isopropylbenzene [98-82-8]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 16:41m,p-Xylenes [108-38-3/106-42-3]^0.18 MRK7L050182.00.18 U 1
ug/L SM 6200B-1997 12/05/17 16:41Methylene Chloride [75-09-2]^0.070 MRK7L050182.00.070 U 1
Page 6 of 23This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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ANALYTICAL RESULTS
Effluent 4th Qtr 2017Description:Lab Sample ID:CA17337-02 11/27/17 14:55Received:
CA17337Work Order:11/27/17 11:47Sampled:Waste WaterMatrix:
Justin AbreuSampled By:Project:Dixie
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 12/05/17 16:41Methyl-tert-Butyl Ether [1634-04-4]^0.12 MRK7L050181.00.12 U 1
ug/L SM 6200B-1997 12/05/17 16:41Naphthalene [91-20-3]^0.086 MRK7L050181.00.086 U 1
ug/L SM 6200B-1997 12/05/17 16:41n-Butyl Benzene [104-51-8]^0.074 MRK7L050181.00.074 U 1
ug/L SM 6200B-1997 12/05/17 16:41n-Propyl Benzene [103-65-1]^0.073 MRK7L050181.00.073 U 1
ug/L SM 6200B-1997 12/05/17 16:41o-Xylene [95-47-6]^0.088 MRK7L050181.00.088 U 1
ug/L SM 6200B-1997 12/05/17 16:41sec-Butylbenzene [135-98-8]^0.053 MRK7L050181.00.053 U 1
ug/L SM 6200B-1997 12/05/17 16:41Styrene [100-42-5]^0.082 MRK7L050181.00.082 U 1
ug/L SM 6200B-1997 12/05/17 16:41tert-Butylbenzene [98-06-6]^0.094 MRK7L050181.00.094 U 1
ug/L SM 6200B-1997 12/05/17 16:41Tetrachloroethene [127-18-4]^0.099 MRK7L050181.00.099 U 1
ug/L SM 6200B-1997 12/05/17 16:41Toluene [108-88-3]^0.053 MRK7L050181.00.053 U 1
ug/L SM 6200B-1997 12/05/17 16:41trans-1,2-Dichloroethene [156-60-5]^0.11 MRK7L050181.00.11 U 1
ug/L SM 6200B-1997 12/05/17 16:41trans-1,3-Dichloropropene [10061-02-6]^0.080 MRK7L050181.00.080 U 1
ug/L SM 6200B-1997 12/05/17 16:41Trichloroethene [79-01-6]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 16:41Trichlorofluoromethane [75-69-4]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 16:41Vinyl chloride [75-01-4]^0.083 MRK7L050181.00.083 U 1
ug/L SM 6200B-1997 12/05/17 16:41Xylenes (Total) [1330-20-7]^0.22 MRK7L050181.00.22 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 70-13082 %MRKSM 6200B-1997 12/05/17 16:417L050184150.0 1
Dibromofluoromethane 70-13092 %MRKSM 6200B-1997 12/05/17 16:417L050184650.0 1
Toluene-d8 70-13092 %MRKSM 6200B-1997 12/05/17 16:417L050184650.0 1
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 625 12/01/17 15:292-Methylnaphthalene [91-57-6]^1.5 DFM7K28006101.5 U 1
ug/L EPA 625 12/01/17 15:29Acenaphthene [83-32-9]^1.4 DFM7K28006101.4 U 1
ug/L EPA 625 12/01/17 15:29Acenaphthylene [208-96-8]^1.2 DFM7K28006101.2 U 1
ug/L EPA 625 12/01/17 15:29Anthracene [120-12-7]^1.6 DFM7K28006101.6 U 1
ug/L EPA 625 12/01/17 15:29Benzo(a)anthracene [56-55-3]^1.3 DFM7K28006101.3 U 1
ug/L EPA 625 12/01/17 15:29Benzo(a)pyrene [50-32-8]^1.3 DFM7K28006101.3 U 1
ug/L EPA 625 12/01/17 15:29Benzo(b)fluoranthene [205-99-2]^1.0 DFM7K28006101.0 U 1
ug/L EPA 625 12/01/17 15:29Benzo(g,h,i)perylene [191-24-2]^2.4 DFM7K28006102.4 U 1
ug/L EPA 625 12/01/17 15:29Benzo(k)fluoranthene [207-08-9]^1.3 DFM7K28006101.3 U 1
ug/L EPA 625 12/01/17 15:29Chrysene [218-01-9]^2.0 DFM7K28006102.0 U 1
ug/L EPA 625 12/01/17 15:29Dibenzo(a,h)anthracene [53-70-3]^2.3 DFM7K28006102.3 U 1
ug/L EPA 625 12/01/17 15:29Fluoranthene [206-44-0]^2.1 DFM7K28006102.1 U 1
ug/L EPA 625 12/01/17 15:29Fluorene [86-73-7]^1.7 DFM7K28006101.7 U 1
ug/L EPA 625 12/01/17 15:29Indeno(1,2,3-cd)pyrene [193-39-5]^2.2 DFM7K28006102.2 U 1
ug/L EPA 625 12/01/17 15:29Naphthalene [91-20-3]^1.3 DFM7K28006101.3 U 1
ug/L EPA 625 12/01/17 15:29Phenanthrene [85-01-8]^1.4 DFM7K28006101.4 U 1
ug/L EPA 625 12/01/17 15:29Pyrene [129-00-0]^2.1 DFM7K28006102.1 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
2-Fluorobiphenyl 15-13982 %DFMEPA 625 12/01/17 15:297K280064150.0 1
Nitrobenzene-d5 16-14079 %DFMEPA 625 12/01/17 15:297K280063950.0 1
Terphenyl-d14 23-16455 %DFMEPA 625 12/01/17 15:297K280062750.0 1
Page 7 of 23This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
Effluent 4th Qtr 2017Description:Lab Sample ID:CA17337-02 11/27/17 14:55Received:
CA17337Work Order:11/27/17 11:47Sampled:Waste WaterMatrix:
Justin AbreuSampled By:Project:Dixie
Metals (acid extractable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 6010D 11/30/17 12:32Lead [7439-92-1]^3.10 JMV7K2903210.03.10 U 1
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/L SM 2540D-1997 12/04/17 14:25Total Suspended Solids^2.5 OMR7L040102.52.5 U 1
Classical Chemistry Parameters
^ - ENCO Orlando certified analyte [NC 424]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/L EPA 420.1 12/07/17 10:05Phenolics^0.034 CRG7L060060.0500.034 U 1
Classical Chemistry Parameters
^ - ENCO Jacksonville certified analyte [NC 442]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/L EPA 1664B 11/29/17 15:47Oil & Grease (HEM) [C-0007]^2.40 SMA7K280075.002.40 U 1
SVE Effluent 4th Qtr 2017Description:Lab Sample ID:CA17337-03 11/27/17 14:55Received:
CA17337Work Order:11/27/17 11:36Sampled:AirMatrix:
% Solids:Justin AbreuSampled By:Project:Dixie
Volatile Organic Compounds by GCMS
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/m‡ Air Method 18 Modified 11/29/17 20:54Benzene [71-43-2]0.0029 LTS7K290050.0320.26 4
mg/m‡ Air Method 18 Modified 11/29/17 20:54Ethylbenzene [100-41-4]0.0040 LTS7K290050.0430.079 4
mg/m‡ Air Method 18 Modified 11/29/17 20:54Methyl-tert-butyl ether [1634-04-4]0.0026 LTS7K290050.0360.0026 U QL-024
mg/m‡ Air Method 18 Modified 11/29/17 22:37Toluene [108-88-3]0.030 LTS7K290050.381.7 40
mg/m‡ Air Method 18 Modified 11/29/17 20:54Total Light Petroleum Hydrocarbons 3.7 LTS7K290053.733 4
mg/m‡ Air Method 18 Modified 11/29/17 20:54Xylenes (Total) [1330-20-7]0.0078 LTS7K290050.0431.2 4
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 64-130102 %LTSMethod 18 Modified 11/29/17 20:547K290053231.0 4
4-Bromofluorobenzene 64-13098 %LTSMethod 18 Modified 11/29/17 22:377K290053031.0 40
Page 8 of 23This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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ANALYTICAL RESULTS
Trip BlankDescription:Lab Sample ID:CA17337-04 11/27/17 14:55Received:
CA17337Work Order:11/27/17 11:36Sampled:WaterMatrix:
Justin AbreuSampled By:Project:Dixie
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 12/05/17 15:411,1,1,2-Tetrachloroethane [630-20-6]^0.091 MRK7L050181.00.091 U 1
ug/L SM 6200B-1997 12/05/17 15:411,1,1-Trichloroethane [71-55-6]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 15:411,1,2,2-Tetrachloroethane [79-34-5]^0.085 MRK7L050181.00.085 U 1
ug/L SM 6200B-1997 12/05/17 15:411,1,2-Trichloroethane [79-00-5]^0.068 MRK7L050181.00.068 U 1
ug/L SM 6200B-1997 12/05/17 15:411,1-Dichloroethane [75-34-3]^0.050 MRK7L050181.00.050 U 1
ug/L SM 6200B-1997 12/05/17 15:411,1-Dichloroethene [75-35-4]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 15:411,1-Dichloropropene [563-58-6]^0.063 MRK7L050181.00.063 U 1
ug/L SM 6200B-1997 12/05/17 15:411,2,3-Trichlorobenzene [87-61-6]^0.25 MRK7L050181.00.25 U 1
ug/L SM 6200B-1997 12/05/17 15:411,2,3-Trichloropropane [96-18-4]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 15:411,2,4-Trichlorobenzene [120-82-1]^0.097 MRK7L050181.00.097 U 1
ug/L SM 6200B-1997 12/05/17 15:411,2,4-Trimethylbenzene [95-63-6]^0.067 MRK7L050181.00.067 U 1
ug/L SM 6200B-1997 12/05/17 15:411,2-Dibromo-3-chloropropane [96-12-8]^0.48 MRK7L050181.00.48 U 1
ug/L SM 6200B-1997 12/05/17 15:411,2-Dibromoethane [106-93-4]^0.42 MRK7L050181.00.42 U 1
ug/L SM 6200B-1997 12/05/17 15:411,2-Dichlorobenzene [95-50-1]^0.052 MRK7L050181.00.052 U 1
ug/L SM 6200B-1997 12/05/17 15:411,2-Dichloroethane [107-06-2]^0.082 MRK7L050181.00.082 U 1
ug/L SM 6200B-1997 12/05/17 15:411,2-Dichloropropane [78-87-5]^0.098 MRK7L050181.00.098 U 1
ug/L SM 6200B-1997 12/05/17 15:411,3,5-Trimethylbenzene [108-67-8]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 15:411,3-Dichlorobenzene [541-73-1]^0.092 MRK7L050181.00.092 U 1
ug/L SM 6200B-1997 12/05/17 15:411,3-Dichloropropane [142-28-9]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 15:411,4-Dichlorobenzene [106-46-7]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 15:412,2-Dichloropropane [594-20-7]^0.12 MRK7L050181.00.12 U 1
ug/L SM 6200B-1997 12/05/17 15:412-Chlorotoluene [95-49-8]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 15:414-Chlorotoluene [106-43-4]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 15:414-Isopropyltoluene [99-87-6]^0.066 MRK7L050181.00.066 U 1
ug/L SM 6200B-1997 12/05/17 15:41Benzene [71-43-2]^0.050 MRK7L050181.00.050 U 1
ug/L SM 6200B-1997 12/05/17 15:41Bromobenzene [108-86-1]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 15:41Bromochloromethane [74-97-5]^0.11 MRK7L050181.00.11 U 1
ug/L SM 6200B-1997 12/05/17 15:41Bromodichloromethane [75-27-4]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 15:41Bromoform [75-25-2]^0.20 MRK7L050181.00.20 U 1
ug/L SM 6200B-1997 12/05/17 15:41Bromomethane [74-83-9]^0.28 MRK7L050181.00.28 U 1
ug/L SM 6200B-1997 12/05/17 15:41Carbon Tetrachloride [56-23-5]^0.082 MRK7L050181.00.082 U 1
ug/L SM 6200B-1997 12/05/17 15:41Chlorobenzene [108-90-7]^0.069 MRK7L050181.00.069 U 1
ug/L SM 6200B-1997 12/05/17 15:41Chloroethane [75-00-3]^0.18 MRK7L050181.00.18 U 1
ug/L SM 6200B-1997 12/05/17 15:41Chloroform [67-66-3]^0.083 MRK7L050181.00.083 U 1
ug/L SM 6200B-1997 12/05/17 15:41Chloromethane [74-87-3]^0.050 MRK7L050181.00.050 U 1
ug/L SM 6200B-1997 12/05/17 15:41cis-1,2-Dichloroethene [156-59-2]^0.075 MRK7L050181.00.075 U 1
ug/L SM 6200B-1997 12/05/17 15:41cis-1,3-Dichloropropene [10061-01-5]^0.073 MRK7L050181.00.073 U 1
ug/L SM 6200B-1997 12/05/17 15:41Dibromochloromethane [124-48-1]^0.067 MRK7L050181.00.067 U 1
ug/L SM 6200B-1997 12/05/17 15:41Dibromomethane [74-95-3]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 15:41Dichlorodifluoromethane [75-71-8]^0.091 MRK7L050181.00.091 U 1
ug/L SM 6200B-1997 12/05/17 15:41Ethylbenzene [100-41-4]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 15:41Freon 113 [76-13-1]^0.35 MRK7L050181.00.35 U 1
ug/L SM 6200B-1997 12/05/17 15:41Hexachlorobutadiene [87-68-3]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 15:41Isopropyl Ether [108-20-3]^0.21 MRK7L050181.00.21 U 1
ug/L SM 6200B-1997 12/05/17 15:41Isopropylbenzene [98-82-8]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 15:41m,p-Xylenes [108-38-3/106-42-3]^0.18 MRK7L050182.00.18 U 1
ug/L SM 6200B-1997 12/05/17 15:41Methylene Chloride [75-09-2]^0.070 MRK7L050182.00.070 U 1
Page 9 of 23This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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ANALYTICAL RESULTS
Trip BlankDescription:Lab Sample ID:CA17337-04 11/27/17 14:55Received:
CA17337Work Order:11/27/17 11:36Sampled:WaterMatrix:
Justin AbreuSampled By:Project:Dixie
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 12/05/17 15:41Methyl-tert-Butyl Ether [1634-04-4]^0.12 MRK7L050181.00.12 U 1
ug/L SM 6200B-1997 12/05/17 15:41Naphthalene [91-20-3]^0.086 MRK7L050181.00.086 U 1
ug/L SM 6200B-1997 12/05/17 15:41n-Butyl Benzene [104-51-8]^0.074 MRK7L050181.00.074 U 1
ug/L SM 6200B-1997 12/05/17 15:41n-Propyl Benzene [103-65-1]^0.073 MRK7L050181.00.073 U 1
ug/L SM 6200B-1997 12/05/17 15:41o-Xylene [95-47-6]^0.088 MRK7L050181.00.088 U 1
ug/L SM 6200B-1997 12/05/17 15:41sec-Butylbenzene [135-98-8]^0.053 MRK7L050181.00.053 U 1
ug/L SM 6200B-1997 12/05/17 15:41Styrene [100-42-5]^0.082 MRK7L050181.00.082 U 1
ug/L SM 6200B-1997 12/05/17 15:41tert-Butylbenzene [98-06-6]^0.094 MRK7L050181.00.094 U 1
ug/L SM 6200B-1997 12/05/17 15:41Tetrachloroethene [127-18-4]^0.099 MRK7L050181.00.099 U 1
ug/L SM 6200B-1997 12/05/17 15:41Toluene [108-88-3]^0.053 MRK7L050181.00.053 U 1
ug/L SM 6200B-1997 12/05/17 15:41trans-1,2-Dichloroethene [156-60-5]^0.11 MRK7L050181.00.11 U 1
ug/L SM 6200B-1997 12/05/17 15:41trans-1,3-Dichloropropene [10061-02-6]^0.080 MRK7L050181.00.080 U 1
ug/L SM 6200B-1997 12/05/17 15:41Trichloroethene [79-01-6]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 15:41Trichlorofluoromethane [75-69-4]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 15:41Vinyl chloride [75-01-4]^0.083 MRK7L050181.00.083 U 1
ug/L SM 6200B-1997 12/05/17 15:41Xylenes (Total) [1330-20-7]^0.22 MRK7L050181.00.22 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 70-13081 %MRKSM 6200B-1997 12/05/17 15:417L050184050.0 1
Dibromofluoromethane 70-13092 %MRKSM 6200B-1997 12/05/17 15:417L050184650.0 1
Toluene-d8 70-13090 %MRKSM 6200B-1997 12/05/17 15:417L050184550.0 1
Page 10 of 23This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 7L05018 - EPA 5030B_MS
Prepared: 12/05/2017 00:34 Analyzed: 12/05/2017 12:41Blank (7L05018-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.00.091 U 1,1,1,2-Tetrachloroethane
ug/L1.00.15 U 1,1,1-Trichloroethane
ug/L1.00.085 U 1,1,2,2-Tetrachloroethane
ug/L1.00.068 U 1,1,2-Trichloroethane
ug/L1.00.050 U 1,1-Dichloroethane
ug/L1.00.15 U 1,1-Dichloroethene
ug/L1.00.063 U 1,1-Dichloropropene
ug/L1.00.25 U 1,2,3-Trichlorobenzene
ug/L1.00.15 U 1,2,3-Trichloropropane
ug/L1.00.097 U 1,2,4-Trichlorobenzene
ug/L1.00.067 U 1,2,4-Trimethylbenzene
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.42 U 1,2-Dibromoethane
ug/L1.00.052 U 1,2-Dichlorobenzene
ug/L1.00.082 U 1,2-Dichloroethane
ug/L1.00.098 U 1,2-Dichloropropane
ug/L1.00.10 U 1,3,5-Trimethylbenzene
ug/L1.00.092 U 1,3-Dichlorobenzene
ug/L1.00.15 U 1,3-Dichloropropane
ug/L1.00.10 U 1,4-Dichlorobenzene
ug/L1.00.12 U 2,2-Dichloropropane
ug/L1.00.10 U 2-Chlorotoluene
ug/L1.00.10 U 4-Chlorotoluene
ug/L1.00.066 U 4-Isopropyltoluene
ug/L1.00.050 U Benzene
ug/L1.00.13 U Bromobenzene
ug/L1.00.11 U Bromochloromethane
ug/L1.00.10 U Bromodichloromethane
ug/L1.00.20 U Bromoform
ug/L1.00.28 U Bromomethane
ug/L1.00.082 U Carbon Tetrachloride
ug/L1.00.069 U Chlorobenzene
ug/L1.00.18 U Chloroethane
ug/L1.00.083 U Chloroform
ug/L1.00.050 U Chloromethane
ug/L1.00.075 U cis-1,2-Dichloroethene
ug/L1.00.073 U cis-1,3-Dichloropropene
ug/L1.00.067 U Dibromochloromethane
ug/L1.00.13 U Dibromomethane
ug/L1.00.091 U Dichlorodifluoromethane
ug/L1.00.10 U Ethylbenzene
ug/L1.00.35 U Freon 113
ug/L1.00.15 U Hexachlorobutadiene
ug/L1.00.21 U Isopropyl Ether
ug/L1.00.13 U Isopropylbenzene
ug/L2.00.18 U m,p-Xylenes
ug/L2.00.070 U Methylene Chloride
ug/L1.00.12 U Methyl-tert-Butyl Ether
ug/L1.00.086 U Naphthalene
Page 11 of 23This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 7L05018 - EPA 5030B_MS - Continued
Prepared: 12/05/2017 00:34 Analyzed: 12/05/2017 12:41Blank (7L05018-BLK1) Continued
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.00.074 U n-Butyl Benzene
ug/L1.00.073 U n-Propyl Benzene
ug/L1.00.088 U o-Xylene
ug/L1.00.053 U sec-Butylbenzene
ug/L1.00.082 U Styrene
ug/L1.00.094 U tert-Butylbenzene
ug/L1.00.099 U Tetrachloroethene
ug/L1.00.053 U Toluene
ug/L1.00.11 U trans-1,2-Dichloroethene
ug/L1.00.080 U trans-1,3-Dichloropropene
ug/L1.00.13 U Trichloroethene
ug/L1.00.15 U Trichlorofluoromethane
ug/L1.00.083 U Vinyl chloride
ug/L1.00.22 U Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 8140
ug/L 50.0 70-130Dibromofluoromethane9145
ug/L 50.0 70-130Toluene-d8 9045
Prepared: 12/05/2017 00:34 Analyzed: 12/05/2017 10:40LCS (7L05018-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 70-13010421 1,1,1,2-Tetrachloroethane
ug/L1.0 20.0 70-13010321 1,1,1-Trichloroethane
ug/L1.0 20.0 70-13010321 1,1,2,2-Tetrachloroethane
ug/L1.0 20.0 70-13010020 1,1,2-Trichloroethane
ug/L1.0 20.0 70-13010721 1,1-Dichloroethane
ug/L1.0 20.0 70-1309820 1,1-Dichloroethene
ug/L1.0 20.0 70-13010421 1,1-Dichloropropene
ug/L1.0 20.0 70-13011222 1,2,3-Trichlorobenzene
ug/L1.0 20.0 70-1309619 1,2,3-Trichloropropane
ug/L1.0 20.0 70-13010020 1,2,4-Trichlorobenzene
ug/L1.0 20.0 70-13010220 1,2,4-Trimethylbenzene
ug/L1.0 20.0 70-1309519 1,2-Dibromo-3-chloropropane
ug/L1.0 20.0 70-13010020 1,2-Dibromoethane
ug/L1.0 20.0 70-13010321 1,2-Dichlorobenzene
ug/L1.0 20.0 70-13010120 1,2-Dichloroethane
ug/L1.0 20.0 70-13010521 1,2-Dichloropropane
ug/L1.0 20.0 70-13010220 1,3,5-Trimethylbenzene
ug/L1.0 20.0 70-13010321 1,3-Dichlorobenzene
ug/L1.0 20.0 70-1309319 1,3-Dichloropropane
ug/L1.0 20.0 70-13010621 1,4-Dichlorobenzene
ug/L1.0 20.0 70-13010120 2,2-Dichloropropane
ug/L1.0 20.0 70-13010521 2-Chlorotoluene
ug/L1.0 20.0 70-13010120 4-Chlorotoluene
ug/L1.0 20.0 70-13010321 4-Isopropyltoluene
ug/L1.0 20.0 70-13011022 Benzene
ug/L1.0 20.0 70-1309519 Bromobenzene
ug/L1.0 20.0 70-13011323 Bromochloromethane
ug/L1.0 20.0 70-13010922 Bromodichloromethane
Page 12 of 23This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 7L05018 - EPA 5030B_MS - Continued
Prepared: 12/05/2017 00:34 Analyzed: 12/05/2017 10:40LCS (7L05018-BS1) Continued
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 70-1309719 Bromoform
ug/L1.0 20.0 60-14011323 Bromomethane
ug/L1.0 20.0 70-13010321 Carbon Tetrachloride
ug/L1.0 20.0 70-13010822 Chlorobenzene
ug/L1.0 20.0 60-1409619 Chloroethane
ug/L1.0 20.0 70-13011423 Chloroform
ug/L1.0 20.0 60-14010822 Chloromethane
ug/L1.0 20.0 70-13010220 cis-1,2-Dichloroethene
ug/L1.0 20.0 70-1309920 cis-1,3-Dichloropropene
ug/L1.0 20.0 70-13010421 Dibromochloromethane
ug/L1.0 20.0 70-13010220 Dibromomethane
ug/L1.0 20.0 60-1409419 Dichlorodifluoromethane
ug/L1.0 20.0 70-13010120 Ethylbenzene
ug/L1.0 40.0 70-13010542 Freon 113
ug/L1.0 20.0 70-13010922 Hexachlorobutadiene
ug/L1.0 20.0 70-1309519 Isopropyl Ether
ug/L1.0 20.0 70-13010621 Isopropylbenzene
ug/L2.0 40.0 70-13010542 m,p-Xylenes
ug/L2.0 20.0 70-13010721 Methylene Chloride
ug/L1.0 20.0 70-1309319 Methyl-tert-Butyl Ether
ug/L1.0 20.0 70-1309018 Naphthalene
ug/L1.0 20.0 70-13011122 n-Butyl Benzene
ug/L1.0 20.0 70-13010220 n-Propyl Benzene
ug/L1.0 20.0 70-1309719 o-Xylene
ug/L1.0 20.0 70-13010521 sec-Butylbenzene
ug/L1.0 20.0 70-13010020 Styrene
ug/L1.0 20.0 70-13010220 tert-Butylbenzene
ug/L1.0 20.0 70-13010020 Tetrachloroethene
ug/L1.0 20.0 70-13010721 Toluene
ug/L1.0 20.0 70-13010020 trans-1,2-Dichloroethene
ug/L1.0 20.0 70-13010321 trans-1,3-Dichloropropene
ug/L1.0 20.0 70-13010321 Trichloroethene
ug/L1.0 20.0 60-14010120 Trichlorofluoromethane
ug/L1.0 20.0 60-1409719 Vinyl chloride
ug/L1.0 60.0 70-13010261 Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 8342
ug/L 50.0 70-130Dibromofluoromethane8945
ug/L 50.0 70-130Toluene-d8 9447
Prepared: 12/05/2017 00:34 Analyzed: 12/05/2017 11:10Matrix Spike (7L05018-MS1)
Source: CA18761-03
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 25.0 71-1171050.091 U26 1,1,1,2-Tetrachloroethane
ug/L1.0 25.0 72-1431070.15 U27 1,1,1-Trichloroethane
ug/L1.0 25.0 59-1331000.085 U25 1,1,2,2-Tetrachloroethane
ug/L1.0 25.0 67-118990.068 U25 1,1,2-Trichloroethane
ug/L1.0 25.0 79-1411080.050 U27 1,1-Dichloroethane
ug/L1.0 25.0 75-1331000.15 U25 1,1-Dichloroethene
ug/L1.0 25.0 70-1291070.063 U27 1,1-Dichloropropene
Page 13 of 23This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 7L05018 - EPA 5030B_MS - Continued
Prepared: 12/05/2017 00:34 Analyzed: 12/05/2017 11:10Matrix Spike (7L05018-MS1) Continued
Source: CA18761-03
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 25.0 62-1171070.25 U27 1,2,3-Trichlorobenzene
ug/L1.0 25.0 58-140960.15 U24 1,2,3-Trichloropropane
ug/L1.0 25.0 59-1221000.097 U25 1,2,4-Trichlorobenzene
ug/L1.0 25.0 74-1231020.067 U26 1,2,4-Trimethylbenzene
ug/L1.0 25.0 37-157900.48 U22 1,2-Dibromo-3-chloropropane
ug/L1.0 25.0 66-123980.42 U25 1,2-Dibromoethane
ug/L1.0 25.0 76-1161040.052 U26 1,2-Dichlorobenzene
ug/L1.0 25.0 72-151960.082 U24 1,2-Dichloroethane
ug/L1.0 25.0 78-1251040.098 U26 1,2-Dichloropropane
ug/L1.0 25.0 77-1291030.10 U26 1,3,5-Trimethylbenzene
ug/L1.0 25.0 76-1191060.092 U26 1,3-Dichlorobenzene
ug/L1.0 25.0 60-129930.15 U23 1,3-Dichloropropane
ug/L1.0 25.0 76-1221080.10 U27 1,4-Dichlorobenzene
ug/L1.0 25.0 21-1671080.12 U27 2,2-Dichloropropane
ug/L1.0 25.0 73-1351040.10 U26 2-Chlorotoluene
ug/L1.0 25.0 76-1341020.10 U26 4-Chlorotoluene
ug/L1.0 25.0 75-1271060.066 U26 4-Isopropyltoluene
ug/L1.0 25.0 81-1341110.050 U28 Benzene
ug/L1.0 25.0 72-115960.13 U24 Bromobenzene
ug/L1.0 25.0 74-1281100.11 U27 Bromochloromethane
ug/L1.0 25.0 72-1291080.10 U27 Bromodichloromethane
ug/L1.0 25.0 73-119940.20 U23 Bromoform
ug/L1.0 20.0 38-1891100.28 U22 Bromomethane
ug/L1.0 25.0 68-1421110.082 U28 Carbon Tetrachloride
ug/L1.0 25.0 83-1171130.069 U28 Chlorobenzene
ug/L1.0 20.0 45-213910.18 U18 Chloroethane
ug/L1.0 25.0 78-1381140.083 U28 Chloroform
ug/L1.0 20.0 56-1711070.050 U21 Chloromethane
ug/L1.0 25.0 69-1201040.075 U26 cis-1,2-Dichloroethene
ug/L1.0 25.0 63-1251020.073 U26 cis-1,3-Dichloropropene
ug/L1.0 25.0 73-1171010.067 U25 Dibromochloromethane
ug/L1.0 25.0 76-1241020.13 U25 Dibromomethane
ug/L1.0 20.0 25-161920.091 U18 Dichlorodifluoromethane
ug/L1.0 25.0 68-1241050.10 U26 Ethylbenzene
ug/L1.0 50.0 0-2001140.35 U57 Freon 113
ug/L1.0 25.0 63-1141080.15 U27 Hexachlorobutadiene
ug/L1.0 25.0 70-130970.21 U24 Isopropyl Ether
ug/L1.0 25.0 81-1361110.13 U28 Isopropylbenzene
ug/L2.0 50.0 79-1211100.18 U55 m,p-Xylenes
ug/L2.0 25.0 68-1281080.070 U27 Methylene Chloride
ug/L1.0 25.0 10-127920.12 U23 Methyl-tert-Butyl Ether
ug/L1.0 25.0 50-127850.086 U21 Naphthalene
ug/L1.0 25.0 68-1261160.074 U29 n-Butyl Benzene
ug/L1.0 25.0 76-1251080.073 U27 n-Propyl Benzene
ug/L1.0 25.0 71-1251010.088 U25 o-Xylene
ug/L1.0 25.0 75-1221080.053 U27 sec-Butylbenzene
ug/L1.0 25.0 73-1201030.082 U26 Styrene
ug/L1.0 25.0 70-1371040.094 U26 tert-Butylbenzene
ug/L1.0 25.0 40-1811060.099 U27 Tetrachloroethene
Page 14 of 23This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 7L05018 - EPA 5030B_MS - Continued
Prepared: 12/05/2017 00:34 Analyzed: 12/05/2017 11:10Matrix Spike (7L05018-MS1) Continued
Source: CA18761-03
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 25.0 71-1181090.053 U27 Toluene
ug/L1.0 25.0 75-1391020.11 U26 trans-1,2-Dichloroethene
ug/L1.0 25.0 62-1521050.080 U26 trans-1,3-Dichloropropene
ug/L1.0 25.0 75-1151050.13 U26 Trichloroethene
ug/L1.0 20.0 68-1831020.15 U20 Trichlorofluoromethane
ug/L1.0 20.0 49-150960.083 U19 Vinyl chloride
ug/L1.0 75.0 77-1211070.22 U80 Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 8442
ug/L 50.0 70-130Dibromofluoromethane8844
ug/L 50.0 70-130Toluene-d8 9246
Prepared: 12/05/2017 00:34 Analyzed: 12/05/2017 11:41Matrix Spike Dup (7L05018-MSD1)
Source: CA18761-03
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 25.0 1671-117108 30.091 U27 1,1,1,2-Tetrachloroethane
ug/L1.0 25.0 1872-143104 30.15 U26 1,1,1-Trichloroethane
ug/L1.0 25.0 1659-133105 50.085 U26 1,1,2,2-Tetrachloroethane
ug/L1.0 25.0 1867-118101 20.068 U25 1,1,2-Trichloroethane
ug/L1.0 25.0 1979-141106 20.050 U26 1,1-Dichloroethane
ug/L1.0 25.0 2075-13399 10.15 U25 1,1-Dichloroethene
ug/L1.0 25.0 1770-129105 20.063 U26 1,1-Dichloropropene
ug/L1.0 25.0 1762-117110 30.25 U27 1,2,3-Trichlorobenzene
ug/L1.0 25.0 1758-140102 60.15 U26 1,2,3-Trichloropropane
ug/L1.0 25.0 1759-12299 0.40.097 U25 1,2,4-Trichlorobenzene
ug/L1.0 25.0 1874-123103 0.50.067 U26 1,2,4-Trimethylbenzene
ug/L1.0 25.0 1837-15793 30.48 U23 1,2-Dibromo-3-chloropropane
ug/L1.0 25.0 1566-123100 20.42 U25 1,2-Dibromoethane
ug/L1.0 25.0 1676-116105 0.70.052 U26 1,2-Dichlorobenzene
ug/L1.0 25.0 1672-15197 10.082 U24 1,2-Dichloroethane
ug/L1.0 25.0 1978-125104 0.20.098 U26 1,2-Dichloropropane
ug/L1.0 25.0 1677-129102 10.10 U25 1,3,5-Trimethylbenzene
ug/L1.0 25.0 1776-119106 0.20.092 U26 1,3-Dichlorobenzene
ug/L1.0 25.0 1660-12995 20.15 U24 1,3-Dichloropropane
ug/L1.0 25.0 1676-122107 0.90.10 U27 1,4-Dichlorobenzene
ug/L1.0 25.0 2021-167106 30.12 U26 2,2-Dichloropropane
ug/L1.0 25.0 1673-135104 0.040.10 U26 2-Chlorotoluene
ug/L1.0 25.0 1676-134101 0.90.10 U25 4-Chlorotoluene
ug/L1.0 25.0 1775-127105 0.90.066 U26 4-Isopropyltoluene
ug/L1.0 25.0 1781-134110 20.050 U27 Benzene
ug/L1.0 25.0 1772-11599 20.13 U25 Bromobenzene
ug/L1.0 25.0 1874-128110 0.070.11 U27 Bromochloromethane
ug/L1.0 25.0 1672-129107 0.50.10 U27 Bromodichloromethane
ug/L1.0 25.0 4473-11996 20.20 U24 Bromoform
ug/L1.0 20.0 2738-189110 0.30.28 U22 Bromomethane
ug/L1.0 25.0 1768-142106 40.082 U27 Carbon Tetrachloride
ug/L1.0 25.0 1683-117112 10.069 U28 Chlorobenzene
ug/L1.0 20.0 2645-21391 00.18 U18 Chloroethane
ug/L1.0 25.0 1778-138113 0.50.083 U28 Chloroform
ug/L1.0 20.0 2856-171104 30.050 U21 Chloromethane
Page 15 of 23This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 7L05018 - EPA 5030B_MS - Continued
Prepared: 12/05/2017 00:34 Analyzed: 12/05/2017 11:41Matrix Spike Dup (7L05018-MSD1) Continued
Source: CA18761-03
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 25.0 1869-120103 10.075 U26 cis-1,2-Dichloroethene
ug/L1.0 25.0 1763-125100 20.073 U25 cis-1,3-Dichloropropene
ug/L1.0 25.0 1673-117103 20.067 U26 Dibromochloromethane
ug/L1.0 25.0 1576-124102 0.30.13 U26 Dibromomethane
ug/L1.0 20.0 4825-16187 50.091 U17 Dichlorodifluoromethane
ug/L1.0 25.0 1668-124104 0.60.10 U26 Ethylbenzene
ug/L1.0 50.0 250-200110 30.35 U55 Freon 113
ug/L1.0 25.0 1963-114109 10.15 U27 Hexachlorobutadiene
ug/L1.0 25.0 3070-13097 0.080.21 U24 Isopropyl Ether
ug/L1.0 25.0 1681-136110 0.80.13 U27 Isopropylbenzene
ug/L2.0 50.0 1679-121110 0.30.18 U55 m,p-Xylenes
ug/L2.0 25.0 1768-128106 20.070 U26 Methylene Chloride
ug/L1.0 25.0 2110-12795 40.12 U24 Methyl-tert-Butyl Ether
ug/L1.0 25.0 1950-12790 50.086 U22 Naphthalene
ug/L1.0 25.0 1568-126114 10.074 U29 n-Butyl Benzene
ug/L1.0 25.0 1676-125107 0.70.073 U27 n-Propyl Benzene
ug/L1.0 25.0 1571-125101 0.10.088 U25 o-Xylene
ug/L1.0 25.0 1775-122106 20.053 U27 sec-Butylbenzene
ug/L1.0 25.0 2373-120104 0.20.082 U26 Styrene
ug/L1.0 25.0 2270-137102 20.094 U25 tert-Butylbenzene
ug/L1.0 25.0 2640-181106 0.70.099 U26 Tetrachloroethene
ug/L1.0 25.0 1771-118109 0.30.053 U27 Toluene
ug/L1.0 25.0 1975-139102 0.40.11 U25 trans-1,2-Dichloroethene
ug/L1.0 25.0 1662-152107 20.080 U27 trans-1,3-Dichloropropene
ug/L1.0 25.0 1875-115103 20.13 U26 Trichloroethene
ug/L1.0 20.0 2268-18399 30.15 U20 Trichlorofluoromethane
ug/L1.0 20.0 2749-15095 20.083 U19 Vinyl chloride
ug/L1.0 75.0 1677-121107 0.10.22 U80 Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 8744
ug/L 50.0 70-130Dibromofluoromethane8944
ug/L 50.0 70-130Toluene-d8 9146
Semivolatile Organic Compounds by GCMS - Quality Control
Batch 7K28006 - EPA 3510C_MS
Prepared: 11/28/2017 08:18 Analyzed: 12/01/2017 11:47Blank (7K28006-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L101.5 U 2-Methylnaphthalene
ug/L101.4 U Acenaphthene
ug/L101.2 U Acenaphthylene
ug/L101.6 U Anthracene
ug/L101.3 U Benzo(a)anthracene
ug/L101.3 U Benzo(a)pyrene
ug/L101.0 U Benzo(b)fluoranthene
ug/L102.4 U Benzo(g,h,i)perylene
ug/L101.3 U Benzo(k)fluoranthene
ug/L102.0 U Chrysene
Page 16 of 23This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch 7K28006 - EPA 3510C_MS - Continued
Prepared: 11/28/2017 08:18 Analyzed: 12/01/2017 11:47Blank (7K28006-BLK1) Continued
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L102.3 U Dibenzo(a,h)anthracene
ug/L102.1 U Fluoranthene
ug/L101.7 U Fluorene
ug/L102.2 U Indeno(1,2,3-cd)pyrene
ug/L101.3 U Naphthalene
ug/L101.4 U Phenanthrene
ug/L102.1 U Pyrene
ug/L 50.0 15-1392-Fluorobiphenyl 7939
ug/L 50.0 16-140Nitrobenzene-d5 7738
ug/L 50.0 23-164Terphenyl-d14 6934
Prepared: 11/28/2017 08:18 Analyzed: 12/01/2017 12:18LCS (7K28006-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L10 50.0 33-1119748 2-Methylnaphthalene
ug/L10 50.0 47-1459447 Acenaphthene
ug/L10 50.0 33-1459447 Acenaphthylene
ug/L10 50.0 27-1339547 Anthracene
ug/L10 50.0 33-1439648 Benzo(a)anthracene
ug/L10 50.0 17-1639949 Benzo(a)pyrene
ug/L10 50.0 24-1599547 Benzo(b)fluoranthene
ug/L10 50.0 10-21911055 Benzo(g,h,i)perylene
ug/L10 50.0 11-1629146 Benzo(k)fluoranthene
ug/L10 50.0 17-1689548 Chrysene
ug/L10 50.0 10-22711155 Dibenzo(a,h)anthracene
ug/L10 50.0 26-1378743 Fluoranthene
ug/L10 50.0 59-1219748 Fluorene
ug/L10 50.0 10-17111155 Indeno(1,2,3-cd)pyrene
ug/L10 50.0 21-1338945 Naphthalene
ug/L10 50.0 54-1209547 Phenanthrene
ug/L10 50.0 65-1348643 Pyrene
ug/L 50.0 15-1392-Fluorobiphenyl 9447
ug/L 50.0 16-140Nitrobenzene-d5 9045
ug/L 50.0 23-164Terphenyl-d14 8040
Prepared: 11/28/2017 08:18 Analyzed: 12/01/2017 12:50Matrix Spike (7K28006-MS1)
Source: CA17772-02
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L10 50.0 33-111921.5 U46 2-Methylnaphthalene
ug/L10 50.0 47-145911.4 U45 Acenaphthene
ug/L10 50.0 33-145901.2 U45 Acenaphthylene
ug/L10 50.0 27-133921.6 U46 Anthracene
ug/L10 50.0 33-143931.3 U47 Benzo(a)anthracene
ug/L10 50.0 17-163961.3 U48 Benzo(a)pyrene
ug/L10 50.0 24-159921.0 U46 Benzo(b)fluoranthene
ug/L10 50.0 10-2191072.4 U54 Benzo(g,h,i)perylene
ug/L10 50.0 11-162891.3 U44 Benzo(k)fluoranthene
ug/L10 50.0 17-168932.0 U47 Chrysene
Page 17 of 23This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch 7K28006 - EPA 3510C_MS - Continued
Prepared: 11/28/2017 08:18 Analyzed: 12/01/2017 12:50Matrix Spike (7K28006-MS1) Continued
Source: CA17772-02
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L10 50.0 10-2271102.3 U55 Dibenzo(a,h)anthracene
ug/L10 50.0 26-137832.1 U42 Fluoranthene
ug/L10 50.0 59-121921.7 U46 Fluorene
ug/L10 50.0 10-1711092.2 U55 Indeno(1,2,3-cd)pyrene
ug/L10 50.0 21-133841.3 U42 Naphthalene
ug/L10 50.0 54-120911.4 U46 Phenanthrene
ug/L10 50.0 52-115822.1 U41 Pyrene
ug/L 50.0 15-1392-Fluorobiphenyl 8643
ug/L 50.0 16-140Nitrobenzene-d5 8241
ug/L 50.0 23-164Terphenyl-d14 7537
Prepared: 11/28/2017 08:18 Analyzed: 12/01/2017 13:22Matrix Spike Dup (7K28006-MSD1)
Source: CA17772-02
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L10 50.0 2533-11188 51.5 U44 2-Methylnaphthalene
ug/L10 50.0 2547-14587 41.4 U44 Acenaphthene
ug/L10 50.0 2533-14587 41.2 U43 Acenaphthylene
ug/L10 50.0 2527-13390 21.6 U45 Anthracene
ug/L10 50.0 2533-14394 0.71.3 U47 Benzo(a)anthracene
ug/L10 50.0 2517-16398 21.3 U49 Benzo(a)pyrene
ug/L10 50.0 2524-15992 0.11.0 U46 Benzo(b)fluoranthene
ug/L10 50.0 2510-219107 0.42.4 U53 Benzo(g,h,i)perylene
ug/L10 50.0 2511-16291 21.3 U45 Benzo(k)fluoranthene
ug/L10 50.0 2517-16893 0.22.0 U47 Chrysene
ug/L10 50.0 2510-227110 0.42.3 U55 Dibenzo(a,h)anthracene
ug/L10 50.0 2526-13783 0.22.1 U42 Fluoranthene
ug/L10 50.0 2559-12191 21.7 U45 Fluorene
ug/L10 50.0 2510-171109 0.12.2 U54 Indeno(1,2,3-cd)pyrene
ug/L10 50.0 2521-13378 71.3 U39 Naphthalene
ug/L10 50.0 2554-12091 0.91.4 U45 Phenanthrene
ug/L10 50.0 2552-11583 12.1 U41 Pyrene
ug/L 50.0 15-1392-Fluorobiphenyl 8241
ug/L 50.0 16-140Nitrobenzene-d5 7638
ug/L 50.0 23-164Terphenyl-d14 7638
Metals (acid extractable) by EPA 6000/7000 Series Methods - Quality Control
Batch 7K29032 - SM18 3030C
Prepared: 11/29/2017 15:01 Analyzed: 11/30/2017 12:07Blank (7K29032-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L10.03.10 U Lead
Prepared: 11/29/2017 15:01 Analyzed: 11/30/2017 12:17LCS (7K29032-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L10.0 200 80-120107215 Lead
Page 18 of 23This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Metals (acid extractable) by EPA 6000/7000 Series Methods - Quality Control
Batch 7K29032 - SM18 3030C - Continued
Prepared: 11/29/2017 15:01 Analyzed: 11/30/2017 12:22Matrix Spike (7K29032-MS1)
Source: CA17339-13
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L10.0 200 75-1251073.10 U215 Lead
Prepared: 11/29/2017 15:01 Analyzed: 11/30/2017 12:24Matrix Spike Dup (7K29032-MSD1)
Source: CA17339-13
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L10.0 200 2075-125106 23.10 U211 Lead
Prepared: 11/29/2017 15:01 Analyzed: 11/30/2017 12:27Post Spike (7K29032-PS1)
Source: CA17339-13
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L0.00935 0.200 80-1201040.001280.209 Lead
Classical Chemistry Parameters - Quality Control
Batch 7L04010 - NO PREP
Prepared & Analyzed: 12/04/2017 14:25Blank (7L04010-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L2.52.5 U Total Suspended Solids
Prepared & Analyzed: 12/04/2017 14:25LCS (7L04010-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L2.5 100 80-1209696 Total Suspended Solids
Prepared & Analyzed: 12/04/2017 14:25Duplicate (7L04010-DUP1)
Source: CA14941-01
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L50 207270250 Total Suspended Solids
Prepared & Analyzed: 12/04/2017 14:25Duplicate (7L04010-DUP2)
Source: CA15470-01
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L50 203210220 Total Suspended Solids
Classical Chemistry Parameters - Quality Control
Batch 7L06006 - NO PREP
Prepared: 12/06/2017 08:45 Analyzed: 12/07/2017 10:05Blank (7L06006-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L0.0500.034 U Phenolics
Prepared: 12/06/2017 08:45 Analyzed: 12/07/2017 10:05LCS (7L06006-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
Page 19 of 23This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 7L06006 - NO PREP - Continued
Prepared: 12/06/2017 08:45 Analyzed: 12/07/2017 10:05LCS (7L06006-BS1) Continued
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L0.050 0.500 90-1101000.50 Phenolics
Prepared: 12/06/2017 08:45 Analyzed: 12/07/2017 10:05Matrix Spike (7L06006-MS1)
Source: AA08204-06
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L0.050 0.500 90-110950.0440.52 Phenolics
Prepared: 12/06/2017 08:45 Analyzed: 12/07/2017 10:05Matrix Spike Dup (7L06006-MSD1)
Source: AA08204-06
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L0.050 0.500 1090-11095 00.0440.52 Phenolics
Volatile Organic Compounds by GCMS - Quality Control
Batch 7K29005 - Same
Prepared & Analyzed: 11/29/2017 09:55Blank (7K29005-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/m‡ Air0.00800.00073 U Benzene
mg/m‡ Air0.0110.0010 U Ethylbenzene
mg/m‡ Air0.00900.00065 U Methyl-tert-butyl ether
mg/m‡ Air0.00940.00075 U Toluene
mg/m‡ Air0.920.92 U Total Light Petroleum Hydrocarbons
mg/m‡ Air0.0110.0020 U Xylenes (Total)
ppbv 31.0 64-1304-Bromofluorobenzene 8827
Prepared & Analyzed: 11/29/2017 16:07LCS (7K29005-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/m‡ Air0.0080 0.0320 68-1491050.033 Benzene
mg/m‡ Air0.011 0.0434 70-144920.040 Ethylbenzene
mg/m‡ Air0.0090 0.0361 70-1301350.049 Methyl-tert-butyl ether
mg/m‡ Air0.0094 0.0377 70-1441190.045 Toluene
ppbv 31.0 64-1304-Bromofluorobenzene 10332
Prepared & Analyzed: 11/29/2017 17:45LCS Dup (7K29005-BSD1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/m‡ Air0.0080 0.0320 2668-149106 20.034 Benzene
mg/m‡ Air0.011 0.0434 1070-14493 10.040 Ethylbenzene
mg/m‡ Air0.0090 0.0361 2070-130136 0.10.049 Methyl-tert-butyl ether
mg/m‡ Air0.0094 0.0377 2470-144119 0.30.045 Toluene
ppbv 31.0 64-1304-Bromofluorobenzene 10432
Classical Chemistry Parameters - Quality Control
Batch 7K28007 - EPA 1664B
Page 20 of 23This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 7K28007 - EPA 1664B - Continued
Prepared: 11/28/2017 11:26 Analyzed: 11/29/2017 15:47Blank (7K28007-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L5.002.40 U Oil & Grease (HEM)
Prepared: 11/28/2017 11:26 Analyzed: 11/29/2017 15:47LCS (7K28007-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L5.00 165 78-11487144 Oil & Grease (HEM)
Prepared: 11/28/2017 11:26 Analyzed: 11/29/2017 15:47LCS Dup (7K28007-BSD1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L5.00 196 1878-11486 15168 Oil & Grease (HEM)
Prepared: 11/28/2017 11:26 Analyzed: 11/29/2017 15:47Matrix Spike (7K28007-MS1)
Source: BA04914-01
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L5.00 148 78-114832.63126 Oil & Grease (HEM)
Page 21 of 23This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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FLAGS/NOTES AND DEFINITIONS
The sample was analyzed at dilution.
The analyte was detected in the associated method blank.
The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
MRL
E
U
J
D
B
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
PQL: Practical Quantitation Limit.PQL
The associated laboratory control sample exhibited high bias; since the result is ND, there is no
impact.
QL-02
Page 22 of 23This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL