RA-1137_7489_CA_MRP_20180105_2017SEMI2

102-A Woodwinds Industrial Court
Cary NC, 27511
919.467.3090 919.467.3515Phone:FAX:
ENCO Workorder(s): CA17338
Durham, NC 27703
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative. This report shall not be reproduced except in full, without
the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Enclosure(s)
Project Number: 7023, Project Name/Desc: Dixie - MWs
Attn: Justin Abreu
EMS Environmental (EM001)
117 South Hoover Road
Chuck Smith
Project Manager
Thursday, December 7, 2017
RE: Laboratory Results for
Dear Justin Abreu,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Monday, November 27, 2017.
Enclosure(s)
Page 1 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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SAMPLE SUMMARY/LABORATORY CHRONICLE
MW-4 CA17338-01 Sampled:11/27/17 12:29 Received:11/27/17 14:55Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
SM 6200B-1997 12/11/17 12/06/17 15:36 12/07/17 03:50
RW-2 CA17338-02 Sampled:11/27/17 12:17 Received:11/27/17 14:55Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
SM 6200B-1997 12/11/17 12/05/17 11:34 12/05/17 17:11
RW-3 CA17338-03 Sampled:11/27/17 12:23 Received:11/27/17 14:55Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
SM 6200B-1997 12/11/17 12/05/17 11:34 12/05/17 17:41
RW-4 CA17338-04 Sampled:11/27/17 12:08 Received:11/27/17 14:55Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
SM 6200B-1997 12/11/17 12/05/17 11:34 12/05/17 18:11
PW-15 CA17338-05 Sampled:11/27/17 13:10 Received:11/27/17 14:55Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
SM 6200B-1997 12/11/17 12/05/17 11:34 12/05/17 18:42
PW-17 INF CA17338-06 Sampled:11/27/17 13:02 Received:11/27/17 14:55Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
SM 6200B-1997 12/11/17 12/05/17 11:34 12/05/17 19:12
PW-17 EFF CA17338-07 Sampled:11/27/17 13:00 Received:11/27/17 14:55Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
SM 6200B-1997 12/11/17 12/05/17 11:34 12/05/17 19:42
PW-18 CA17338-08 Sampled:11/27/17 12:49 Received:11/27/17 14:55Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
SM 6200B-1997 12/11/17 12/05/17 11:34 12/05/17 20:12
PW-22 CA17338-09 Sampled:11/27/17 13:16 Received:11/27/17 14:55Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
SM 6200B-1997 12/11/17 12/05/17 11:34 12/05/17 20:42
PW-23 CA17338-10 Sampled:11/27/17 13:22 Received:11/27/17 14:55Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
SM 6200B-1997 12/11/17 12/05/17 11:34 12/05/17 21:12
Trip Blank CA17338-11 Sampled:11/27/17 12:08 Received:11/27/17 14:55Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
SM 6200B-1997 12/11/17 12/05/17 11:34 12/05/17 21:42
Page 2 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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SAMPLE DETECTION SUMMARY
Lab ID:Client ID:MW-4 CA17338-01
Analyte MethodUnitsPQLResultsFlag NotesMDL
3100 20 ug/L SM 6200B-1997D 1,2,4-Trimethylbenzene 1.3
860 20 ug/L SM 6200B-1997D 1,3,5-Trimethylbenzene 2.0
430 20 ug/L SM 6200B-1997D Benzene 1.0
830 20 ug/L SM 6200B-1997D Ethylbenzene 2.0
88 20 ug/L SM 6200B-1997D Isopropylbenzene 2.6
4400 40 ug/L SM 6200B-1997D m,p-Xylenes 3.6
460 20 ug/L SM 6200B-1997D Naphthalene 1.7
230 20 ug/L SM 6200B-1997D n-Butyl Benzene 1.5
250 20 ug/L SM 6200B-1997D n-Propyl Benzene 1.5
3000 20 ug/L SM 6200B-1997D o-Xylene 1.8
780 20 ug/L SM 6200B-1997D Toluene 1.1
7400 20 ug/L SM 6200B-1997D Xylenes (Total)4.4
Lab ID:Client ID:RW-2 CA17338-02
Analyte MethodUnitsPQLResultsFlag NotesMDL
200 50 ug/L SM 6200B-1997D 1,2,4-Trimethylbenzene 3.4
78 50 ug/L SM 6200B-1997D 1,3,5-Trimethylbenzene 5.0
1800 50 ug/L SM 6200B-1997D Benzene 2.5
300 50 ug/L SM 6200B-1997D Ethylbenzene 5.0
660 100 ug/L SM 6200B-1997D m,p-Xylenes 9.0
96 50 ug/L SM 6200B-1997D Naphthalene 4.3
450 50 ug/L SM 6200B-1997D o-Xylene 4.4
1200 50 ug/L SM 6200B-1997D Toluene 2.6
1100 50 ug/L SM 6200B-1997D Xylenes (Total)11
Lab ID:Client ID:RW-4 CA17338-04
Analyte MethodUnitsPQLResultsFlag NotesMDL
1800 50 ug/L SM 6200B-1997D 1,2,4-Trimethylbenzene 3.4
620 50 ug/L SM 6200B-1997D 1,3,5-Trimethylbenzene 5.0
3400 50 ug/L SM 6200B-1997D Benzene 2.5
810 50 ug/L SM 6200B-1997D Ethylbenzene 5.0
110 50 ug/L SM 6200B-1997D Isopropylbenzene 6.5
4400 100 ug/L SM 6200B-1997D m,p-Xylenes 9.0
180 50 ug/L SM 6200B-1997D Methyl-tert-Butyl Ether 6.0
330 50 ug/L SM 6200B-1997D Naphthalene 4.3
120 50 ug/L SM 6200B-1997D n-Butyl Benzene 3.7
190 50 ug/L SM 6200B-1997D n-Propyl Benzene 3.6
2800 50 ug/L SM 6200B-1997D o-Xylene 4.4
7400 50 ug/L SM 6200B-1997D Toluene 2.6
7200 50 ug/L SM 6200B-1997D Xylenes (Total)11
Lab ID:Client ID:PW-15 CA17338-05
Analyte MethodUnitsPQLResultsFlag NotesMDL
0.78 1.0 ug/L SM 6200B-1997J 1,2-Dichloroethane 0.082
9.8 1.0 ug/L SM 6200B-1997 Methyl-tert-Butyl Ether 0.12
Lab ID:Client ID:PW-17 INF CA17338-06
Analyte MethodUnitsPQLResultsFlag NotesMDL
3.3 1.0 ug/L SM 6200B-1997 1,2-Dichloroethane 0.082
56 1.0 ug/L SM 6200B-1997 Methyl-tert-Butyl Ether 0.12
Lab ID:Client ID:PW-18 CA17338-08
Analyte MethodUnitsPQLResultsFlag NotesMDL
1.2 1.0 ug/L SM 6200B-1997 Methyl-tert-Butyl Ether 0.12
Lab ID:Client ID:PW-22 CA17338-09
Analyte MethodUnitsPQLResultsFlag NotesMDL
0.56 1.0 ug/L SM 6200B-1997J Methyl-tert-Butyl Ether 0.12
Page 3 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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ANALYTICAL RESULTS
MW-4Description:Lab Sample ID:CA17338-01 11/27/17 14:55Received:
CA17338Work Order:11/27/17 12:29Sampled:Ground WaterMatrix:
Justin AbreuSampled By:Project:Dixie - MWs
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 12/07/17 03:501,1,1,2-Tetrachloroethane [630-20-6]^1.8 MRK7L06037201.8 UD 20
ug/L SM 6200B-1997 12/07/17 03:501,1,1-Trichloroethane [71-55-6]^3.0 MRK7L06037203.0 UD 20
ug/L SM 6200B-1997 12/07/17 03:501,1,2,2-Tetrachloroethane [79-34-5]^1.7 MRK7L06037201.7 UD 20
ug/L SM 6200B-1997 12/07/17 03:501,1,2-Trichloroethane [79-00-5]^1.4 MRK7L06037201.4 UD 20
ug/L SM 6200B-1997 12/07/17 03:501,1-Dichloroethane [75-34-3]^1.0 MRK7L06037201.0 UD 20
ug/L SM 6200B-1997 12/07/17 03:501,1-Dichloroethene [75-35-4]^3.0 MRK7L06037203.0 UD 20
ug/L SM 6200B-1997 12/07/17 03:501,1-Dichloropropene [563-58-6]^1.3 MRK7L06037201.3 UD 20
ug/L SM 6200B-1997 12/07/17 03:501,2,3-Trichlorobenzene [87-61-6]^5.0 MRK7L06037205.0 UD 20
ug/L SM 6200B-1997 12/07/17 03:501,2,3-Trichloropropane [96-18-4]^3.0 MRK7L06037203.0 UD 20
ug/L SM 6200B-1997 12/07/17 03:501,2,4-Trichlorobenzene [120-82-1]^1.9 MRK7L06037201.9 UD 20
ug/L SM 6200B-1997 12/07/17 03:501,2,4-Trimethylbenzene [95-63-6]^1.3 MRK7L06037203100D 20
ug/L SM 6200B-1997 12/07/17 03:501,2-Dibromo-3-chloropropane [96-12-8]^9.6 MRK7L06037209.6 UD 20
ug/L SM 6200B-1997 12/07/17 03:501,2-Dibromoethane [106-93-4]^8.4 MRK7L06037208.4 UD 20
ug/L SM 6200B-1997 12/07/17 03:501,2-Dichlorobenzene [95-50-1]^1.0 MRK7L06037201.0 UD 20
ug/L SM 6200B-1997 12/07/17 03:501,2-Dichloroethane [107-06-2]^1.6 MRK7L06037201.6 UD 20
ug/L SM 6200B-1997 12/07/17 03:501,2-Dichloropropane [78-87-5]^2.0 MRK7L06037202.0 UD 20
ug/L SM 6200B-1997 12/07/17 03:501,3,5-Trimethylbenzene [108-67-8]^2.0 MRK7L0603720860D 20
ug/L SM 6200B-1997 12/07/17 03:501,3-Dichlorobenzene [541-73-1]^1.8 MRK7L06037201.8 UD 20
ug/L SM 6200B-1997 12/07/17 03:501,3-Dichloropropane [142-28-9]^3.0 MRK7L06037203.0 UD 20
ug/L SM 6200B-1997 12/07/17 03:501,4-Dichlorobenzene [106-46-7]^2.0 MRK7L06037202.0 UD 20
ug/L SM 6200B-1997 12/07/17 03:502,2-Dichloropropane [594-20-7]^2.4 MRK7L06037202.4 UD 20
ug/L SM 6200B-1997 12/07/17 03:502-Chlorotoluene [95-49-8]^2.0 MRK7L06037202.0 UD 20
ug/L SM 6200B-1997 12/07/17 03:504-Chlorotoluene [106-43-4]^2.0 MRK7L06037202.0 UD 20
ug/L SM 6200B-1997 12/07/17 03:504-Isopropyltoluene [99-87-6]^1.3 MRK7L06037201.3 UD 20
ug/L SM 6200B-1997 12/07/17 03:50Benzene [71-43-2]^1.0 MRK7L0603720430D 20
ug/L SM 6200B-1997 12/07/17 03:50Bromobenzene [108-86-1]^2.6 MRK7L06037202.6 UD 20
ug/L SM 6200B-1997 12/07/17 03:50Bromochloromethane [74-97-5]^2.2 MRK7L06037202.2 UD 20
ug/L SM 6200B-1997 12/07/17 03:50Bromodichloromethane [75-27-4]^2.0 MRK7L06037202.0 UD 20
ug/L SM 6200B-1997 12/07/17 03:50Bromoform [75-25-2]^4.0 MRK7L06037204.0 UD 20
ug/L SM 6200B-1997 12/07/17 03:50Bromomethane [74-83-9]^5.6 MRK7L06037205.6 UD 20
ug/L SM 6200B-1997 12/07/17 03:50Carbon Tetrachloride [56-23-5]^1.6 MRK7L06037201.6 UD 20
ug/L SM 6200B-1997 12/07/17 03:50Chlorobenzene [108-90-7]^1.4 MRK7L06037201.4 UD 20
ug/L SM 6200B-1997 12/07/17 03:50Chloroethane [75-00-3]^3.6 MRK7L06037203.6 UD 20
ug/L SM 6200B-1997 12/07/17 03:50Chloroform [67-66-3]^1.7 MRK7L06037201.7 UD 20
ug/L SM 6200B-1997 12/07/17 03:50Chloromethane [74-87-3]^1.0 MRK7L06037201.0 UD 20
ug/L SM 6200B-1997 12/07/17 03:50cis-1,2-Dichloroethene [156-59-2]^1.5 MRK7L06037201.5 UD 20
ug/L SM 6200B-1997 12/07/17 03:50cis-1,3-Dichloropropene [10061-01-5]^1.5 MRK7L06037201.5 UD 20
ug/L SM 6200B-1997 12/07/17 03:50Dibromochloromethane [124-48-1]^1.3 MRK7L06037201.3 UD 20
ug/L SM 6200B-1997 12/07/17 03:50Dibromomethane [74-95-3]^2.6 MRK7L06037202.6 UD 20
ug/L SM 6200B-1997 12/07/17 03:50Dichlorodifluoromethane [75-71-8]^1.8 MRK7L06037201.8 UD 20
ug/L SM 6200B-1997 12/07/17 03:50Ethylbenzene [100-41-4]^2.0 MRK7L0603720830D 20
ug/L SM 6200B-1997 12/07/17 03:50Freon 113 [76-13-1]^7.0 MRK7L06037207.0 UD 20
ug/L SM 6200B-1997 12/07/17 03:50Hexachlorobutadiene [87-68-3]^3.0 MRK7L06037203.0 UD 20
ug/L SM 6200B-1997 12/07/17 03:50Isopropyl Ether [108-20-3]^4.2 MRK7L06037204.2 UD 20
ug/L SM 6200B-1997 12/07/17 03:50Isopropylbenzene [98-82-8]^2.6 MRK7L060372088D 20
ug/L SM 6200B-1997 12/07/17 03:50m,p-Xylenes [108-38-3/106-42-3]^3.6 MRK7L06037404400D 20
ug/L SM 6200B-1997 12/07/17 03:50Methylene Chloride [75-09-2]^1.4 MRK7L06037401.4 UD 20
Page 4 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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ANALYTICAL RESULTS
MW-4Description:Lab Sample ID:CA17338-01 11/27/17 14:55Received:
CA17338Work Order:11/27/17 12:29Sampled:Ground WaterMatrix:
Justin AbreuSampled By:Project:Dixie - MWs
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 12/07/17 03:50Methyl-tert-Butyl Ether [1634-04-4]^2.4 MRK7L06037202.4 UD 20
ug/L SM 6200B-1997 12/07/17 03:50Naphthalene [91-20-3]^1.7 MRK7L0603720460D 20
ug/L SM 6200B-1997 12/07/17 03:50n-Butyl Benzene [104-51-8]^1.5 MRK7L0603720230D 20
ug/L SM 6200B-1997 12/07/17 03:50n-Propyl Benzene [103-65-1]^1.5 MRK7L0603720250D 20
ug/L SM 6200B-1997 12/07/17 03:50o-Xylene [95-47-6]^1.8 MRK7L06037203000D 20
ug/L SM 6200B-1997 12/07/17 03:50sec-Butylbenzene [135-98-8]^1.1 MRK7L06037201.1 UD 20
ug/L SM 6200B-1997 12/07/17 03:50Styrene [100-42-5]^1.6 MRK7L06037201.6 UD 20
ug/L SM 6200B-1997 12/07/17 03:50tert-Butylbenzene [98-06-6]^1.9 MRK7L06037201.9 UD 20
ug/L SM 6200B-1997 12/07/17 03:50Tetrachloroethene [127-18-4]^2.0 MRK7L06037202.0 UD 20
ug/L SM 6200B-1997 12/07/17 03:50Toluene [108-88-3]^1.1 MRK7L0603720780D 20
ug/L SM 6200B-1997 12/07/17 03:50trans-1,2-Dichloroethene [156-60-5]^2.2 MRK7L06037202.2 UD 20
ug/L SM 6200B-1997 12/07/17 03:50trans-1,3-Dichloropropene [10061-02-6]^1.6 MRK7L06037201.6 UD 20
ug/L SM 6200B-1997 12/07/17 03:50Trichloroethene [79-01-6]^2.6 MRK7L06037202.6 UD 20
ug/L SM 6200B-1997 12/07/17 03:50Trichlorofluoromethane [75-69-4]^3.0 MRK7L06037203.0 UD 20
ug/L SM 6200B-1997 12/07/17 03:50Vinyl chloride [75-01-4]^1.7 MRK7L06037201.7 UD 20
ug/L SM 6200B-1997 12/07/17 03:50Xylenes (Total) [1330-20-7]^4.4 MRK7L06037207400D 20
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 70-13086 %MRKSM 6200B-1997 12/07/17 03:507L060374350.0 1
Dibromofluoromethane 70-13092 %MRKSM 6200B-1997 12/07/17 03:507L060374650.0 1
Toluene-d8 70-13092 %MRKSM 6200B-1997 12/07/17 03:507L060374650.0 1
Page 5 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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ANALYTICAL RESULTS
RW-2Description:Lab Sample ID:CA17338-02 11/27/17 14:55Received:
CA17338Work Order:11/27/17 12:17Sampled:Ground WaterMatrix:
Justin AbreuSampled By:Project:Dixie - MWs
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 12/05/17 17:111,1,1,2-Tetrachloroethane [630-20-6]^4.6 MRK7L05018504.6 UD 50
ug/L SM 6200B-1997 12/05/17 17:111,1,1-Trichloroethane [71-55-6]^7.5 MRK7L05018507.5 UD 50
ug/L SM 6200B-1997 12/05/17 17:111,1,2,2-Tetrachloroethane [79-34-5]^4.2 MRK7L05018504.2 UD 50
ug/L SM 6200B-1997 12/05/17 17:111,1,2-Trichloroethane [79-00-5]^3.4 MRK7L05018503.4 UD 50
ug/L SM 6200B-1997 12/05/17 17:111,1-Dichloroethane [75-34-3]^2.5 MRK7L05018502.5 UD 50
ug/L SM 6200B-1997 12/05/17 17:111,1-Dichloroethene [75-35-4]^7.5 MRK7L05018507.5 UD 50
ug/L SM 6200B-1997 12/05/17 17:111,1-Dichloropropene [563-58-6]^3.2 MRK7L05018503.2 UD 50
ug/L SM 6200B-1997 12/05/17 17:111,2,3-Trichlorobenzene [87-61-6]^12 MRK7L050185012UD 50
ug/L SM 6200B-1997 12/05/17 17:111,2,3-Trichloropropane [96-18-4]^7.5 MRK7L05018507.5 UD 50
ug/L SM 6200B-1997 12/05/17 17:111,2,4-Trichlorobenzene [120-82-1]^4.8 MRK7L05018504.8 UD 50
ug/L SM 6200B-1997 12/05/17 17:111,2,4-Trimethylbenzene [95-63-6]^3.4 MRK7L0501850200D 50
ug/L SM 6200B-1997 12/05/17 17:111,2-Dibromo-3-chloropropane [96-12-8]^24 MRK7L050185024UD 50
ug/L SM 6200B-1997 12/05/17 17:111,2-Dibromoethane [106-93-4]^21 MRK7L050185021UD 50
ug/L SM 6200B-1997 12/05/17 17:111,2-Dichlorobenzene [95-50-1]^2.6 MRK7L05018502.6 UD 50
ug/L SM 6200B-1997 12/05/17 17:111,2-Dichloroethane [107-06-2]^4.1 MRK7L05018504.1 UD 50
ug/L SM 6200B-1997 12/05/17 17:111,2-Dichloropropane [78-87-5]^4.9 MRK7L05018504.9 UD 50
ug/L SM 6200B-1997 12/05/17 17:111,3,5-Trimethylbenzene [108-67-8]^5.0 MRK7L050185078D 50
ug/L SM 6200B-1997 12/05/17 17:111,3-Dichlorobenzene [541-73-1]^4.6 MRK7L05018504.6 UD 50
ug/L SM 6200B-1997 12/05/17 17:111,3-Dichloropropane [142-28-9]^7.5 MRK7L05018507.5 UD 50
ug/L SM 6200B-1997 12/05/17 17:111,4-Dichlorobenzene [106-46-7]^5.0 MRK7L05018505.0 UD 50
ug/L SM 6200B-1997 12/05/17 17:112,2-Dichloropropane [594-20-7]^6.0 MRK7L05018506.0 UD 50
ug/L SM 6200B-1997 12/05/17 17:112-Chlorotoluene [95-49-8]^5.0 MRK7L05018505.0 UD 50
ug/L SM 6200B-1997 12/05/17 17:114-Chlorotoluene [106-43-4]^5.0 MRK7L05018505.0 UD 50
ug/L SM 6200B-1997 12/05/17 17:114-Isopropyltoluene [99-87-6]^3.3 MRK7L05018503.3 UD 50
ug/L SM 6200B-1997 12/05/17 17:11Benzene [71-43-2]^2.5 MRK7L05018501800D 50
ug/L SM 6200B-1997 12/05/17 17:11Bromobenzene [108-86-1]^6.5 MRK7L05018506.5 UD 50
ug/L SM 6200B-1997 12/05/17 17:11Bromochloromethane [74-97-5]^5.5 MRK7L05018505.5 UD 50
ug/L SM 6200B-1997 12/05/17 17:11Bromodichloromethane [75-27-4]^5.0 MRK7L05018505.0 UD 50
ug/L SM 6200B-1997 12/05/17 17:11Bromoform [75-25-2]^10 MRK7L050185010UD 50
ug/L SM 6200B-1997 12/05/17 17:11Bromomethane [74-83-9]^14 MRK7L050185014UD 50
ug/L SM 6200B-1997 12/05/17 17:11Carbon Tetrachloride [56-23-5]^4.1 MRK7L05018504.1 UD 50
ug/L SM 6200B-1997 12/05/17 17:11Chlorobenzene [108-90-7]^3.4 MRK7L05018503.4 UD 50
ug/L SM 6200B-1997 12/05/17 17:11Chloroethane [75-00-3]^9.0 MRK7L05018509.0 UD 50
ug/L SM 6200B-1997 12/05/17 17:11Chloroform [67-66-3]^4.2 MRK7L05018504.2 UD 50
ug/L SM 6200B-1997 12/05/17 17:11Chloromethane [74-87-3]^2.5 MRK7L05018502.5 UD 50
ug/L SM 6200B-1997 12/05/17 17:11cis-1,2-Dichloroethene [156-59-2]^3.8 MRK7L05018503.8 UD 50
ug/L SM 6200B-1997 12/05/17 17:11cis-1,3-Dichloropropene [10061-01-5]^3.6 MRK7L05018503.6 UD 50
ug/L SM 6200B-1997 12/05/17 17:11Dibromochloromethane [124-48-1]^3.4 MRK7L05018503.4 UD 50
ug/L SM 6200B-1997 12/05/17 17:11Dibromomethane [74-95-3]^6.5 MRK7L05018506.5 UD 50
ug/L SM 6200B-1997 12/05/17 17:11Dichlorodifluoromethane [75-71-8]^4.6 MRK7L05018504.6 UD 50
ug/L SM 6200B-1997 12/05/17 17:11Ethylbenzene [100-41-4]^5.0 MRK7L0501850300D 50
ug/L SM 6200B-1997 12/05/17 17:11Freon 113 [76-13-1]^18 MRK7L050185018UD 50
ug/L SM 6200B-1997 12/05/17 17:11Hexachlorobutadiene [87-68-3]^7.5 MRK7L05018507.5 UD 50
ug/L SM 6200B-1997 12/05/17 17:11Isopropyl Ether [108-20-3]^10 MRK7L050185010UD 50
ug/L SM 6200B-1997 12/05/17 17:11Isopropylbenzene [98-82-8]^6.5 MRK7L05018506.5 UD 50
ug/L SM 6200B-1997 12/05/17 17:11m,p-Xylenes [108-38-3/106-42-3]^9.0 MRK7L05018100660D 50
ug/L SM 6200B-1997 12/05/17 17:11Methylene Chloride [75-09-2]^3.5 MRK7L050181003.5 UD 50
Page 6 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
RW-2Description:Lab Sample ID:CA17338-02 11/27/17 14:55Received:
CA17338Work Order:11/27/17 12:17Sampled:Ground WaterMatrix:
Justin AbreuSampled By:Project:Dixie - MWs
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 12/05/17 17:11Methyl-tert-Butyl Ether [1634-04-4]^6.0 MRK7L05018506.0 UD 50
ug/L SM 6200B-1997 12/05/17 17:11Naphthalene [91-20-3]^4.3 MRK7L050185096D 50
ug/L SM 6200B-1997 12/05/17 17:11n-Butyl Benzene [104-51-8]^3.7 MRK7L05018503.7 UD 50
ug/L SM 6200B-1997 12/05/17 17:11n-Propyl Benzene [103-65-1]^3.6 MRK7L05018503.6 UD 50
ug/L SM 6200B-1997 12/05/17 17:11o-Xylene [95-47-6]^4.4 MRK7L0501850450D 50
ug/L SM 6200B-1997 12/05/17 17:11sec-Butylbenzene [135-98-8]^2.6 MRK7L05018502.6 UD 50
ug/L SM 6200B-1997 12/05/17 17:11Styrene [100-42-5]^4.1 MRK7L05018504.1 UD 50
ug/L SM 6200B-1997 12/05/17 17:11tert-Butylbenzene [98-06-6]^4.7 MRK7L05018504.7 UD 50
ug/L SM 6200B-1997 12/05/17 17:11Tetrachloroethene [127-18-4]^5.0 MRK7L05018505.0 UD 50
ug/L SM 6200B-1997 12/05/17 17:11Toluene [108-88-3]^2.6 MRK7L05018501200D 50
ug/L SM 6200B-1997 12/05/17 17:11trans-1,2-Dichloroethene [156-60-5]^5.5 MRK7L05018505.5 UD 50
ug/L SM 6200B-1997 12/05/17 17:11trans-1,3-Dichloropropene [10061-02-6]^4.0 MRK7L05018504.0 UD 50
ug/L SM 6200B-1997 12/05/17 17:11Trichloroethene [79-01-6]^6.5 MRK7L05018506.5 UD 50
ug/L SM 6200B-1997 12/05/17 17:11Trichlorofluoromethane [75-69-4]^7.5 MRK7L05018507.5 UD 50
ug/L SM 6200B-1997 12/05/17 17:11Vinyl chloride [75-01-4]^4.2 MRK7L05018504.2 UD 50
ug/L SM 6200B-1997 12/05/17 17:11Xylenes (Total) [1330-20-7]^11 MRK7L05018501100D 50
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 70-13082 %MRKSM 6200B-1997 12/05/17 17:117L050184150.0 1
Dibromofluoromethane 70-13090 %MRKSM 6200B-1997 12/05/17 17:117L050184550.0 1
Toluene-d8 70-13092 %MRKSM 6200B-1997 12/05/17 17:117L050184650.0 1
Page 7 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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ANALYTICAL RESULTS
RW-3Description:Lab Sample ID:CA17338-03 11/27/17 14:55Received:
CA17338Work Order:11/27/17 12:23Sampled:Ground WaterMatrix:
Justin AbreuSampled By:Project:Dixie - MWs
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 12/05/17 17:411,1,1,2-Tetrachloroethane [630-20-6]^0.091 MRK7L050181.00.091 U 1
ug/L SM 6200B-1997 12/05/17 17:411,1,1-Trichloroethane [71-55-6]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 17:411,1,2,2-Tetrachloroethane [79-34-5]^0.085 MRK7L050181.00.085 U 1
ug/L SM 6200B-1997 12/05/17 17:411,1,2-Trichloroethane [79-00-5]^0.068 MRK7L050181.00.068 U 1
ug/L SM 6200B-1997 12/05/17 17:411,1-Dichloroethane [75-34-3]^0.050 MRK7L050181.00.050 U 1
ug/L SM 6200B-1997 12/05/17 17:411,1-Dichloroethene [75-35-4]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 17:411,1-Dichloropropene [563-58-6]^0.063 MRK7L050181.00.063 U 1
ug/L SM 6200B-1997 12/05/17 17:411,2,3-Trichlorobenzene [87-61-6]^0.25 MRK7L050181.00.25 U 1
ug/L SM 6200B-1997 12/05/17 17:411,2,3-Trichloropropane [96-18-4]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 17:411,2,4-Trichlorobenzene [120-82-1]^0.097 MRK7L050181.00.097 U 1
ug/L SM 6200B-1997 12/05/17 17:411,2,4-Trimethylbenzene [95-63-6]^0.067 MRK7L050181.00.067 U 1
ug/L SM 6200B-1997 12/05/17 17:411,2-Dibromo-3-chloropropane [96-12-8]^0.48 MRK7L050181.00.48 U 1
ug/L SM 6200B-1997 12/05/17 17:411,2-Dibromoethane [106-93-4]^0.42 MRK7L050181.00.42 U 1
ug/L SM 6200B-1997 12/05/17 17:411,2-Dichlorobenzene [95-50-1]^0.052 MRK7L050181.00.052 U 1
ug/L SM 6200B-1997 12/05/17 17:411,2-Dichloroethane [107-06-2]^0.082 MRK7L050181.00.082 U 1
ug/L SM 6200B-1997 12/05/17 17:411,2-Dichloropropane [78-87-5]^0.098 MRK7L050181.00.098 U 1
ug/L SM 6200B-1997 12/05/17 17:411,3,5-Trimethylbenzene [108-67-8]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 17:411,3-Dichlorobenzene [541-73-1]^0.092 MRK7L050181.00.092 U 1
ug/L SM 6200B-1997 12/05/17 17:411,3-Dichloropropane [142-28-9]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 17:411,4-Dichlorobenzene [106-46-7]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 17:412,2-Dichloropropane [594-20-7]^0.12 MRK7L050181.00.12 U 1
ug/L SM 6200B-1997 12/05/17 17:412-Chlorotoluene [95-49-8]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 17:414-Chlorotoluene [106-43-4]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 17:414-Isopropyltoluene [99-87-6]^0.066 MRK7L050181.00.066 U 1
ug/L SM 6200B-1997 12/05/17 17:41Benzene [71-43-2]^0.050 MRK7L050181.00.050 U 1
ug/L SM 6200B-1997 12/05/17 17:41Bromobenzene [108-86-1]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 17:41Bromochloromethane [74-97-5]^0.11 MRK7L050181.00.11 U 1
ug/L SM 6200B-1997 12/05/17 17:41Bromodichloromethane [75-27-4]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 17:41Bromoform [75-25-2]^0.20 MRK7L050181.00.20 U 1
ug/L SM 6200B-1997 12/05/17 17:41Bromomethane [74-83-9]^0.28 MRK7L050181.00.28 U 1
ug/L SM 6200B-1997 12/05/17 17:41Carbon Tetrachloride [56-23-5]^0.082 MRK7L050181.00.082 U 1
ug/L SM 6200B-1997 12/05/17 17:41Chlorobenzene [108-90-7]^0.069 MRK7L050181.00.069 U 1
ug/L SM 6200B-1997 12/05/17 17:41Chloroethane [75-00-3]^0.18 MRK7L050181.00.18 U 1
ug/L SM 6200B-1997 12/05/17 17:41Chloroform [67-66-3]^0.083 MRK7L050181.00.083 U 1
ug/L SM 6200B-1997 12/05/17 17:41Chloromethane [74-87-3]^0.050 MRK7L050181.00.050 U 1
ug/L SM 6200B-1997 12/05/17 17:41cis-1,2-Dichloroethene [156-59-2]^0.075 MRK7L050181.00.075 U 1
ug/L SM 6200B-1997 12/05/17 17:41cis-1,3-Dichloropropene [10061-01-5]^0.073 MRK7L050181.00.073 U 1
ug/L SM 6200B-1997 12/05/17 17:41Dibromochloromethane [124-48-1]^0.067 MRK7L050181.00.067 U 1
ug/L SM 6200B-1997 12/05/17 17:41Dibromomethane [74-95-3]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 17:41Dichlorodifluoromethane [75-71-8]^0.091 MRK7L050181.00.091 U 1
ug/L SM 6200B-1997 12/05/17 17:41Ethylbenzene [100-41-4]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 17:41Freon 113 [76-13-1]^0.35 MRK7L050181.00.35 U 1
ug/L SM 6200B-1997 12/05/17 17:41Hexachlorobutadiene [87-68-3]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 17:41Isopropyl Ether [108-20-3]^0.21 MRK7L050181.00.21 U 1
ug/L SM 6200B-1997 12/05/17 17:41Isopropylbenzene [98-82-8]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 17:41m,p-Xylenes [108-38-3/106-42-3]^0.18 MRK7L050182.00.18 U 1
ug/L SM 6200B-1997 12/05/17 17:41Methylene Chloride [75-09-2]^0.070 MRK7L050182.00.070 U 1
Page 8 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
RW-3Description:Lab Sample ID:CA17338-03 11/27/17 14:55Received:
CA17338Work Order:11/27/17 12:23Sampled:Ground WaterMatrix:
Justin AbreuSampled By:Project:Dixie - MWs
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 12/05/17 17:41Methyl-tert-Butyl Ether [1634-04-4]^0.12 MRK7L050181.00.12 U 1
ug/L SM 6200B-1997 12/05/17 17:41Naphthalene [91-20-3]^0.086 MRK7L050181.00.086 U 1
ug/L SM 6200B-1997 12/05/17 17:41n-Butyl Benzene [104-51-8]^0.074 MRK7L050181.00.074 U 1
ug/L SM 6200B-1997 12/05/17 17:41n-Propyl Benzene [103-65-1]^0.073 MRK7L050181.00.073 U 1
ug/L SM 6200B-1997 12/05/17 17:41o-Xylene [95-47-6]^0.088 MRK7L050181.00.088 U 1
ug/L SM 6200B-1997 12/05/17 17:41sec-Butylbenzene [135-98-8]^0.053 MRK7L050181.00.053 U 1
ug/L SM 6200B-1997 12/05/17 17:41Styrene [100-42-5]^0.082 MRK7L050181.00.082 U 1
ug/L SM 6200B-1997 12/05/17 17:41tert-Butylbenzene [98-06-6]^0.094 MRK7L050181.00.094 U 1
ug/L SM 6200B-1997 12/05/17 17:41Tetrachloroethene [127-18-4]^0.099 MRK7L050181.00.099 U 1
ug/L SM 6200B-1997 12/05/17 17:41Toluene [108-88-3]^0.053 MRK7L050181.00.053 U 1
ug/L SM 6200B-1997 12/05/17 17:41trans-1,2-Dichloroethene [156-60-5]^0.11 MRK7L050181.00.11 U 1
ug/L SM 6200B-1997 12/05/17 17:41trans-1,3-Dichloropropene [10061-02-6]^0.080 MRK7L050181.00.080 U 1
ug/L SM 6200B-1997 12/05/17 17:41Trichloroethene [79-01-6]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 17:41Trichlorofluoromethane [75-69-4]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 17:41Vinyl chloride [75-01-4]^0.083 MRK7L050181.00.083 U 1
ug/L SM 6200B-1997 12/05/17 17:41Xylenes (Total) [1330-20-7]^0.22 MRK7L050181.00.22 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 70-13080 %MRKSM 6200B-1997 12/05/17 17:417L050184050.0 1
Dibromofluoromethane 70-13091 %MRKSM 6200B-1997 12/05/17 17:417L050184550.0 1
Toluene-d8 70-13090 %MRKSM 6200B-1997 12/05/17 17:417L050184550.0 1
Page 9 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
RW-4Description:Lab Sample ID:CA17338-04 11/27/17 14:55Received:
CA17338Work Order:11/27/17 12:08Sampled:Ground WaterMatrix:
Justin AbreuSampled By:Project:Dixie - MWs
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 12/05/17 18:111,1,1,2-Tetrachloroethane [630-20-6]^4.6 MRK7L05018504.6 UD 50
ug/L SM 6200B-1997 12/05/17 18:111,1,1-Trichloroethane [71-55-6]^7.5 MRK7L05018507.5 UD 50
ug/L SM 6200B-1997 12/05/17 18:111,1,2,2-Tetrachloroethane [79-34-5]^4.2 MRK7L05018504.2 UD 50
ug/L SM 6200B-1997 12/05/17 18:111,1,2-Trichloroethane [79-00-5]^3.4 MRK7L05018503.4 UD 50
ug/L SM 6200B-1997 12/05/17 18:111,1-Dichloroethane [75-34-3]^2.5 MRK7L05018502.5 UD 50
ug/L SM 6200B-1997 12/05/17 18:111,1-Dichloroethene [75-35-4]^7.5 MRK7L05018507.5 UD 50
ug/L SM 6200B-1997 12/05/17 18:111,1-Dichloropropene [563-58-6]^3.2 MRK7L05018503.2 UD 50
ug/L SM 6200B-1997 12/05/17 18:111,2,3-Trichlorobenzene [87-61-6]^12 MRK7L050185012UD 50
ug/L SM 6200B-1997 12/05/17 18:111,2,3-Trichloropropane [96-18-4]^7.5 MRK7L05018507.5 UD 50
ug/L SM 6200B-1997 12/05/17 18:111,2,4-Trichlorobenzene [120-82-1]^4.8 MRK7L05018504.8 UD 50
ug/L SM 6200B-1997 12/05/17 18:111,2,4-Trimethylbenzene [95-63-6]^3.4 MRK7L05018501800D 50
ug/L SM 6200B-1997 12/05/17 18:111,2-Dibromo-3-chloropropane [96-12-8]^24 MRK7L050185024UD 50
ug/L SM 6200B-1997 12/05/17 18:111,2-Dibromoethane [106-93-4]^21 MRK7L050185021UD 50
ug/L SM 6200B-1997 12/05/17 18:111,2-Dichlorobenzene [95-50-1]^2.6 MRK7L05018502.6 UD 50
ug/L SM 6200B-1997 12/05/17 18:111,2-Dichloroethane [107-06-2]^4.1 MRK7L05018504.1 UD 50
ug/L SM 6200B-1997 12/05/17 18:111,2-Dichloropropane [78-87-5]^4.9 MRK7L05018504.9 UD 50
ug/L SM 6200B-1997 12/05/17 18:111,3,5-Trimethylbenzene [108-67-8]^5.0 MRK7L0501850620D 50
ug/L SM 6200B-1997 12/05/17 18:111,3-Dichlorobenzene [541-73-1]^4.6 MRK7L05018504.6 UD 50
ug/L SM 6200B-1997 12/05/17 18:111,3-Dichloropropane [142-28-9]^7.5 MRK7L05018507.5 UD 50
ug/L SM 6200B-1997 12/05/17 18:111,4-Dichlorobenzene [106-46-7]^5.0 MRK7L05018505.0 UD 50
ug/L SM 6200B-1997 12/05/17 18:112,2-Dichloropropane [594-20-7]^6.0 MRK7L05018506.0 UD 50
ug/L SM 6200B-1997 12/05/17 18:112-Chlorotoluene [95-49-8]^5.0 MRK7L05018505.0 UD 50
ug/L SM 6200B-1997 12/05/17 18:114-Chlorotoluene [106-43-4]^5.0 MRK7L05018505.0 UD 50
ug/L SM 6200B-1997 12/05/17 18:114-Isopropyltoluene [99-87-6]^3.3 MRK7L05018503.3 UD 50
ug/L SM 6200B-1997 12/05/17 18:11Benzene [71-43-2]^2.5 MRK7L05018503400D 50
ug/L SM 6200B-1997 12/05/17 18:11Bromobenzene [108-86-1]^6.5 MRK7L05018506.5 UD 50
ug/L SM 6200B-1997 12/05/17 18:11Bromochloromethane [74-97-5]^5.5 MRK7L05018505.5 UD 50
ug/L SM 6200B-1997 12/05/17 18:11Bromodichloromethane [75-27-4]^5.0 MRK7L05018505.0 UD 50
ug/L SM 6200B-1997 12/05/17 18:11Bromoform [75-25-2]^10 MRK7L050185010UD 50
ug/L SM 6200B-1997 12/05/17 18:11Bromomethane [74-83-9]^14 MRK7L050185014UD 50
ug/L SM 6200B-1997 12/05/17 18:11Carbon Tetrachloride [56-23-5]^4.1 MRK7L05018504.1 UD 50
ug/L SM 6200B-1997 12/05/17 18:11Chlorobenzene [108-90-7]^3.4 MRK7L05018503.4 UD 50
ug/L SM 6200B-1997 12/05/17 18:11Chloroethane [75-00-3]^9.0 MRK7L05018509.0 UD 50
ug/L SM 6200B-1997 12/05/17 18:11Chloroform [67-66-3]^4.2 MRK7L05018504.2 UD 50
ug/L SM 6200B-1997 12/05/17 18:11Chloromethane [74-87-3]^2.5 MRK7L05018502.5 UD 50
ug/L SM 6200B-1997 12/05/17 18:11cis-1,2-Dichloroethene [156-59-2]^3.8 MRK7L05018503.8 UD 50
ug/L SM 6200B-1997 12/05/17 18:11cis-1,3-Dichloropropene [10061-01-5]^3.6 MRK7L05018503.6 UD 50
ug/L SM 6200B-1997 12/05/17 18:11Dibromochloromethane [124-48-1]^3.4 MRK7L05018503.4 UD 50
ug/L SM 6200B-1997 12/05/17 18:11Dibromomethane [74-95-3]^6.5 MRK7L05018506.5 UD 50
ug/L SM 6200B-1997 12/05/17 18:11Dichlorodifluoromethane [75-71-8]^4.6 MRK7L05018504.6 UD 50
ug/L SM 6200B-1997 12/05/17 18:11Ethylbenzene [100-41-4]^5.0 MRK7L0501850810D 50
ug/L SM 6200B-1997 12/05/17 18:11Freon 113 [76-13-1]^18 MRK7L050185018UD 50
ug/L SM 6200B-1997 12/05/17 18:11Hexachlorobutadiene [87-68-3]^7.5 MRK7L05018507.5 UD 50
ug/L SM 6200B-1997 12/05/17 18:11Isopropyl Ether [108-20-3]^10 MRK7L050185010UD 50
ug/L SM 6200B-1997 12/05/17 18:11Isopropylbenzene [98-82-8]^6.5 MRK7L0501850110D 50
ug/L SM 6200B-1997 12/05/17 18:11m,p-Xylenes [108-38-3/106-42-3]^9.0 MRK7L050181004400D 50
ug/L SM 6200B-1997 12/05/17 18:11Methylene Chloride [75-09-2]^3.5 MRK7L050181003.5 UD 50
Page 10 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
RW-4Description:Lab Sample ID:CA17338-04 11/27/17 14:55Received:
CA17338Work Order:11/27/17 12:08Sampled:Ground WaterMatrix:
Justin AbreuSampled By:Project:Dixie - MWs
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 12/05/17 18:11Methyl-tert-Butyl Ether [1634-04-4]^6.0 MRK7L0501850180D 50
ug/L SM 6200B-1997 12/05/17 18:11Naphthalene [91-20-3]^4.3 MRK7L0501850330D 50
ug/L SM 6200B-1997 12/05/17 18:11n-Butyl Benzene [104-51-8]^3.7 MRK7L0501850120D 50
ug/L SM 6200B-1997 12/05/17 18:11n-Propyl Benzene [103-65-1]^3.6 MRK7L0501850190D 50
ug/L SM 6200B-1997 12/05/17 18:11o-Xylene [95-47-6]^4.4 MRK7L05018502800D 50
ug/L SM 6200B-1997 12/05/17 18:11sec-Butylbenzene [135-98-8]^2.6 MRK7L05018502.6 UD 50
ug/L SM 6200B-1997 12/05/17 18:11Styrene [100-42-5]^4.1 MRK7L05018504.1 UD 50
ug/L SM 6200B-1997 12/05/17 18:11tert-Butylbenzene [98-06-6]^4.7 MRK7L05018504.7 UD 50
ug/L SM 6200B-1997 12/05/17 18:11Tetrachloroethene [127-18-4]^5.0 MRK7L05018505.0 UD 50
ug/L SM 6200B-1997 12/05/17 18:11Toluene [108-88-3]^2.6 MRK7L05018507400D 50
ug/L SM 6200B-1997 12/05/17 18:11trans-1,2-Dichloroethene [156-60-5]^5.5 MRK7L05018505.5 UD 50
ug/L SM 6200B-1997 12/05/17 18:11trans-1,3-Dichloropropene [10061-02-6]^4.0 MRK7L05018504.0 UD 50
ug/L SM 6200B-1997 12/05/17 18:11Trichloroethene [79-01-6]^6.5 MRK7L05018506.5 UD 50
ug/L SM 6200B-1997 12/05/17 18:11Trichlorofluoromethane [75-69-4]^7.5 MRK7L05018507.5 UD 50
ug/L SM 6200B-1997 12/05/17 18:11Vinyl chloride [75-01-4]^4.2 MRK7L05018504.2 UD 50
ug/L SM 6200B-1997 12/05/17 18:11Xylenes (Total) [1330-20-7]^11 MRK7L05018507200D 50
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 70-13084 %MRKSM 6200B-1997 12/05/17 18:117L050184250.0 1
Dibromofluoromethane 70-13089 %MRKSM 6200B-1997 12/05/17 18:117L050184550.0 1
Toluene-d8 70-13092 %MRKSM 6200B-1997 12/05/17 18:117L050184650.0 1
Page 11 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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ANALYTICAL RESULTS
PW-15Description:Lab Sample ID:CA17338-05 11/27/17 14:55Received:
CA17338Work Order:11/27/17 13:10Sampled:Ground WaterMatrix:
Justin AbreuSampled By:Project:Dixie - MWs
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 12/05/17 18:421,1,1,2-Tetrachloroethane [630-20-6]^0.091 MRK7L050181.00.091 U 1
ug/L SM 6200B-1997 12/05/17 18:421,1,1-Trichloroethane [71-55-6]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 18:421,1,2,2-Tetrachloroethane [79-34-5]^0.085 MRK7L050181.00.085 U 1
ug/L SM 6200B-1997 12/05/17 18:421,1,2-Trichloroethane [79-00-5]^0.068 MRK7L050181.00.068 U 1
ug/L SM 6200B-1997 12/05/17 18:421,1-Dichloroethane [75-34-3]^0.050 MRK7L050181.00.050 U 1
ug/L SM 6200B-1997 12/05/17 18:421,1-Dichloroethene [75-35-4]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 18:421,1-Dichloropropene [563-58-6]^0.063 MRK7L050181.00.063 U 1
ug/L SM 6200B-1997 12/05/17 18:421,2,3-Trichlorobenzene [87-61-6]^0.25 MRK7L050181.00.25 U 1
ug/L SM 6200B-1997 12/05/17 18:421,2,3-Trichloropropane [96-18-4]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 18:421,2,4-Trichlorobenzene [120-82-1]^0.097 MRK7L050181.00.097 U 1
ug/L SM 6200B-1997 12/05/17 18:421,2,4-Trimethylbenzene [95-63-6]^0.067 MRK7L050181.00.067 U 1
ug/L SM 6200B-1997 12/05/17 18:421,2-Dibromo-3-chloropropane [96-12-8]^0.48 MRK7L050181.00.48 U 1
ug/L SM 6200B-1997 12/05/17 18:421,2-Dibromoethane [106-93-4]^0.42 MRK7L050181.00.42 U 1
ug/L SM 6200B-1997 12/05/17 18:421,2-Dichlorobenzene [95-50-1]^0.052 MRK7L050181.00.052 U 1
ug/L SM 6200B-1997 12/05/17 18:421,2-Dichloroethane [107-06-2]^0.082 MRK7L050181.00.78 J 1
ug/L SM 6200B-1997 12/05/17 18:421,2-Dichloropropane [78-87-5]^0.098 MRK7L050181.00.098 U 1
ug/L SM 6200B-1997 12/05/17 18:421,3,5-Trimethylbenzene [108-67-8]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 18:421,3-Dichlorobenzene [541-73-1]^0.092 MRK7L050181.00.092 U 1
ug/L SM 6200B-1997 12/05/17 18:421,3-Dichloropropane [142-28-9]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 18:421,4-Dichlorobenzene [106-46-7]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 18:422,2-Dichloropropane [594-20-7]^0.12 MRK7L050181.00.12 U 1
ug/L SM 6200B-1997 12/05/17 18:422-Chlorotoluene [95-49-8]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 18:424-Chlorotoluene [106-43-4]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 18:424-Isopropyltoluene [99-87-6]^0.066 MRK7L050181.00.066 U 1
ug/L SM 6200B-1997 12/05/17 18:42Benzene [71-43-2]^0.050 MRK7L050181.00.050 U 1
ug/L SM 6200B-1997 12/05/17 18:42Bromobenzene [108-86-1]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 18:42Bromochloromethane [74-97-5]^0.11 MRK7L050181.00.11 U 1
ug/L SM 6200B-1997 12/05/17 18:42Bromodichloromethane [75-27-4]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 18:42Bromoform [75-25-2]^0.20 MRK7L050181.00.20 U 1
ug/L SM 6200B-1997 12/05/17 18:42Bromomethane [74-83-9]^0.28 MRK7L050181.00.28 U 1
ug/L SM 6200B-1997 12/05/17 18:42Carbon Tetrachloride [56-23-5]^0.082 MRK7L050181.00.082 U 1
ug/L SM 6200B-1997 12/05/17 18:42Chlorobenzene [108-90-7]^0.069 MRK7L050181.00.069 U 1
ug/L SM 6200B-1997 12/05/17 18:42Chloroethane [75-00-3]^0.18 MRK7L050181.00.18 U 1
ug/L SM 6200B-1997 12/05/17 18:42Chloroform [67-66-3]^0.083 MRK7L050181.00.083 U 1
ug/L SM 6200B-1997 12/05/17 18:42Chloromethane [74-87-3]^0.050 MRK7L050181.00.050 U 1
ug/L SM 6200B-1997 12/05/17 18:42cis-1,2-Dichloroethene [156-59-2]^0.075 MRK7L050181.00.075 U 1
ug/L SM 6200B-1997 12/05/17 18:42cis-1,3-Dichloropropene [10061-01-5]^0.073 MRK7L050181.00.073 U 1
ug/L SM 6200B-1997 12/05/17 18:42Dibromochloromethane [124-48-1]^0.067 MRK7L050181.00.067 U 1
ug/L SM 6200B-1997 12/05/17 18:42Dibromomethane [74-95-3]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 18:42Dichlorodifluoromethane [75-71-8]^0.091 MRK7L050181.00.091 U 1
ug/L SM 6200B-1997 12/05/17 18:42Ethylbenzene [100-41-4]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 18:42Freon 113 [76-13-1]^0.35 MRK7L050181.00.35 U 1
ug/L SM 6200B-1997 12/05/17 18:42Hexachlorobutadiene [87-68-3]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 18:42Isopropyl Ether [108-20-3]^0.21 MRK7L050181.00.21 U 1
ug/L SM 6200B-1997 12/05/17 18:42Isopropylbenzene [98-82-8]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 18:42m,p-Xylenes [108-38-3/106-42-3]^0.18 MRK7L050182.00.18 U 1
ug/L SM 6200B-1997 12/05/17 18:42Methylene Chloride [75-09-2]^0.070 MRK7L050182.00.070 U 1
Page 12 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
PW-15Description:Lab Sample ID:CA17338-05 11/27/17 14:55Received:
CA17338Work Order:11/27/17 13:10Sampled:Ground WaterMatrix:
Justin AbreuSampled By:Project:Dixie - MWs
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 12/05/17 18:42Methyl-tert-Butyl Ether [1634-04-4]^0.12 MRK7L050181.09.8 1
ug/L SM 6200B-1997 12/05/17 18:42Naphthalene [91-20-3]^0.086 MRK7L050181.00.086 U 1
ug/L SM 6200B-1997 12/05/17 18:42n-Butyl Benzene [104-51-8]^0.074 MRK7L050181.00.074 U 1
ug/L SM 6200B-1997 12/05/17 18:42n-Propyl Benzene [103-65-1]^0.073 MRK7L050181.00.073 U 1
ug/L SM 6200B-1997 12/05/17 18:42o-Xylene [95-47-6]^0.088 MRK7L050181.00.088 U 1
ug/L SM 6200B-1997 12/05/17 18:42sec-Butylbenzene [135-98-8]^0.053 MRK7L050181.00.053 U 1
ug/L SM 6200B-1997 12/05/17 18:42Styrene [100-42-5]^0.082 MRK7L050181.00.082 U 1
ug/L SM 6200B-1997 12/05/17 18:42tert-Butylbenzene [98-06-6]^0.094 MRK7L050181.00.094 U 1
ug/L SM 6200B-1997 12/05/17 18:42Tetrachloroethene [127-18-4]^0.099 MRK7L050181.00.099 U 1
ug/L SM 6200B-1997 12/05/17 18:42Toluene [108-88-3]^0.053 MRK7L050181.00.053 U 1
ug/L SM 6200B-1997 12/05/17 18:42trans-1,2-Dichloroethene [156-60-5]^0.11 MRK7L050181.00.11 U 1
ug/L SM 6200B-1997 12/05/17 18:42trans-1,3-Dichloropropene [10061-02-6]^0.080 MRK7L050181.00.080 U 1
ug/L SM 6200B-1997 12/05/17 18:42Trichloroethene [79-01-6]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 18:42Trichlorofluoromethane [75-69-4]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 18:42Vinyl chloride [75-01-4]^0.083 MRK7L050181.00.083 U 1
ug/L SM 6200B-1997 12/05/17 18:42Xylenes (Total) [1330-20-7]^0.22 MRK7L050181.00.22 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 70-13081 %MRKSM 6200B-1997 12/05/17 18:427L050184050.0 1
Dibromofluoromethane 70-13092 %MRKSM 6200B-1997 12/05/17 18:427L050184650.0 1
Toluene-d8 70-13093 %MRKSM 6200B-1997 12/05/17 18:427L050184650.0 1
Page 13 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
PW-17 INFDescription:Lab Sample ID:CA17338-06 11/27/17 14:55Received:
CA17338Work Order:11/27/17 13:02Sampled:Ground WaterMatrix:
Justin AbreuSampled By:Project:Dixie - MWs
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 12/05/17 19:121,1,1,2-Tetrachloroethane [630-20-6]^0.091 MRK7L050181.00.091 U 1
ug/L SM 6200B-1997 12/05/17 19:121,1,1-Trichloroethane [71-55-6]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 19:121,1,2,2-Tetrachloroethane [79-34-5]^0.085 MRK7L050181.00.085 U 1
ug/L SM 6200B-1997 12/05/17 19:121,1,2-Trichloroethane [79-00-5]^0.068 MRK7L050181.00.068 U 1
ug/L SM 6200B-1997 12/05/17 19:121,1-Dichloroethane [75-34-3]^0.050 MRK7L050181.00.050 U 1
ug/L SM 6200B-1997 12/05/17 19:121,1-Dichloroethene [75-35-4]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 19:121,1-Dichloropropene [563-58-6]^0.063 MRK7L050181.00.063 U 1
ug/L SM 6200B-1997 12/05/17 19:121,2,3-Trichlorobenzene [87-61-6]^0.25 MRK7L050181.00.25 U 1
ug/L SM 6200B-1997 12/05/17 19:121,2,3-Trichloropropane [96-18-4]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 19:121,2,4-Trichlorobenzene [120-82-1]^0.097 MRK7L050181.00.097 U 1
ug/L SM 6200B-1997 12/05/17 19:121,2,4-Trimethylbenzene [95-63-6]^0.067 MRK7L050181.00.067 U 1
ug/L SM 6200B-1997 12/05/17 19:121,2-Dibromo-3-chloropropane [96-12-8]^0.48 MRK7L050181.00.48 U 1
ug/L SM 6200B-1997 12/05/17 19:121,2-Dibromoethane [106-93-4]^0.42 MRK7L050181.00.42 U 1
ug/L SM 6200B-1997 12/05/17 19:121,2-Dichlorobenzene [95-50-1]^0.052 MRK7L050181.00.052 U 1
ug/L SM 6200B-1997 12/05/17 19:121,2-Dichloroethane [107-06-2]^0.082 MRK7L050181.03.3 1
ug/L SM 6200B-1997 12/05/17 19:121,2-Dichloropropane [78-87-5]^0.098 MRK7L050181.00.098 U 1
ug/L SM 6200B-1997 12/05/17 19:121,3,5-Trimethylbenzene [108-67-8]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 19:121,3-Dichlorobenzene [541-73-1]^0.092 MRK7L050181.00.092 U 1
ug/L SM 6200B-1997 12/05/17 19:121,3-Dichloropropane [142-28-9]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 19:121,4-Dichlorobenzene [106-46-7]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 19:122,2-Dichloropropane [594-20-7]^0.12 MRK7L050181.00.12 U 1
ug/L SM 6200B-1997 12/05/17 19:122-Chlorotoluene [95-49-8]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 19:124-Chlorotoluene [106-43-4]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 19:124-Isopropyltoluene [99-87-6]^0.066 MRK7L050181.00.066 U 1
ug/L SM 6200B-1997 12/05/17 19:12Benzene [71-43-2]^0.050 MRK7L050181.00.050 U 1
ug/L SM 6200B-1997 12/05/17 19:12Bromobenzene [108-86-1]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 19:12Bromochloromethane [74-97-5]^0.11 MRK7L050181.00.11 U 1
ug/L SM 6200B-1997 12/05/17 19:12Bromodichloromethane [75-27-4]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 19:12Bromoform [75-25-2]^0.20 MRK7L050181.00.20 U 1
ug/L SM 6200B-1997 12/05/17 19:12Bromomethane [74-83-9]^0.28 MRK7L050181.00.28 U 1
ug/L SM 6200B-1997 12/05/17 19:12Carbon Tetrachloride [56-23-5]^0.082 MRK7L050181.00.082 U 1
ug/L SM 6200B-1997 12/05/17 19:12Chlorobenzene [108-90-7]^0.069 MRK7L050181.00.069 U 1
ug/L SM 6200B-1997 12/05/17 19:12Chloroethane [75-00-3]^0.18 MRK7L050181.00.18 U 1
ug/L SM 6200B-1997 12/05/17 19:12Chloroform [67-66-3]^0.083 MRK7L050181.00.083 U 1
ug/L SM 6200B-1997 12/05/17 19:12Chloromethane [74-87-3]^0.050 MRK7L050181.00.050 U 1
ug/L SM 6200B-1997 12/05/17 19:12cis-1,2-Dichloroethene [156-59-2]^0.075 MRK7L050181.00.075 U 1
ug/L SM 6200B-1997 12/05/17 19:12cis-1,3-Dichloropropene [10061-01-5]^0.073 MRK7L050181.00.073 U 1
ug/L SM 6200B-1997 12/05/17 19:12Dibromochloromethane [124-48-1]^0.067 MRK7L050181.00.067 U 1
ug/L SM 6200B-1997 12/05/17 19:12Dibromomethane [74-95-3]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 19:12Dichlorodifluoromethane [75-71-8]^0.091 MRK7L050181.00.091 U 1
ug/L SM 6200B-1997 12/05/17 19:12Ethylbenzene [100-41-4]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 19:12Freon 113 [76-13-1]^0.35 MRK7L050181.00.35 U 1
ug/L SM 6200B-1997 12/05/17 19:12Hexachlorobutadiene [87-68-3]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 19:12Isopropyl Ether [108-20-3]^0.21 MRK7L050181.00.21 U 1
ug/L SM 6200B-1997 12/05/17 19:12Isopropylbenzene [98-82-8]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 19:12m,p-Xylenes [108-38-3/106-42-3]^0.18 MRK7L050182.00.18 U 1
ug/L SM 6200B-1997 12/05/17 19:12Methylene Chloride [75-09-2]^0.070 MRK7L050182.00.070 U 1
Page 14 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
PW-17 INFDescription:Lab Sample ID:CA17338-06 11/27/17 14:55Received:
CA17338Work Order:11/27/17 13:02Sampled:Ground WaterMatrix:
Justin AbreuSampled By:Project:Dixie - MWs
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 12/05/17 19:12Methyl-tert-Butyl Ether [1634-04-4]^0.12 MRK7L050181.056 1
ug/L SM 6200B-1997 12/05/17 19:12Naphthalene [91-20-3]^0.086 MRK7L050181.00.086 U 1
ug/L SM 6200B-1997 12/05/17 19:12n-Butyl Benzene [104-51-8]^0.074 MRK7L050181.00.074 U 1
ug/L SM 6200B-1997 12/05/17 19:12n-Propyl Benzene [103-65-1]^0.073 MRK7L050181.00.073 U 1
ug/L SM 6200B-1997 12/05/17 19:12o-Xylene [95-47-6]^0.088 MRK7L050181.00.088 U 1
ug/L SM 6200B-1997 12/05/17 19:12sec-Butylbenzene [135-98-8]^0.053 MRK7L050181.00.053 U 1
ug/L SM 6200B-1997 12/05/17 19:12Styrene [100-42-5]^0.082 MRK7L050181.00.082 U 1
ug/L SM 6200B-1997 12/05/17 19:12tert-Butylbenzene [98-06-6]^0.094 MRK7L050181.00.094 U 1
ug/L SM 6200B-1997 12/05/17 19:12Tetrachloroethene [127-18-4]^0.099 MRK7L050181.00.099 U 1
ug/L SM 6200B-1997 12/05/17 19:12Toluene [108-88-3]^0.053 MRK7L050181.00.053 U 1
ug/L SM 6200B-1997 12/05/17 19:12trans-1,2-Dichloroethene [156-60-5]^0.11 MRK7L050181.00.11 U 1
ug/L SM 6200B-1997 12/05/17 19:12trans-1,3-Dichloropropene [10061-02-6]^0.080 MRK7L050181.00.080 U 1
ug/L SM 6200B-1997 12/05/17 19:12Trichloroethene [79-01-6]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 19:12Trichlorofluoromethane [75-69-4]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 19:12Vinyl chloride [75-01-4]^0.083 MRK7L050181.00.083 U 1
ug/L SM 6200B-1997 12/05/17 19:12Xylenes (Total) [1330-20-7]^0.22 MRK7L050181.00.22 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 70-13079 %MRKSM 6200B-1997 12/05/17 19:127L050183950.0 1
Dibromofluoromethane 70-13093 %MRKSM 6200B-1997 12/05/17 19:127L050184750.0 1
Toluene-d8 70-13090 %MRKSM 6200B-1997 12/05/17 19:127L050184550.0 1
Page 15 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
PW-17 EFFDescription:Lab Sample ID:CA17338-07 11/27/17 14:55Received:
CA17338Work Order:11/27/17 13:00Sampled:Ground WaterMatrix:
Justin AbreuSampled By:Project:Dixie - MWs
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 12/05/17 19:421,1,1,2-Tetrachloroethane [630-20-6]^0.091 MRK7L050181.00.091 U 1
ug/L SM 6200B-1997 12/05/17 19:421,1,1-Trichloroethane [71-55-6]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 19:421,1,2,2-Tetrachloroethane [79-34-5]^0.085 MRK7L050181.00.085 U 1
ug/L SM 6200B-1997 12/05/17 19:421,1,2-Trichloroethane [79-00-5]^0.068 MRK7L050181.00.068 U 1
ug/L SM 6200B-1997 12/05/17 19:421,1-Dichloroethane [75-34-3]^0.050 MRK7L050181.00.050 U 1
ug/L SM 6200B-1997 12/05/17 19:421,1-Dichloroethene [75-35-4]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 19:421,1-Dichloropropene [563-58-6]^0.063 MRK7L050181.00.063 U 1
ug/L SM 6200B-1997 12/05/17 19:421,2,3-Trichlorobenzene [87-61-6]^0.25 MRK7L050181.00.25 U 1
ug/L SM 6200B-1997 12/05/17 19:421,2,3-Trichloropropane [96-18-4]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 19:421,2,4-Trichlorobenzene [120-82-1]^0.097 MRK7L050181.00.097 U 1
ug/L SM 6200B-1997 12/05/17 19:421,2,4-Trimethylbenzene [95-63-6]^0.067 MRK7L050181.00.067 U 1
ug/L SM 6200B-1997 12/05/17 19:421,2-Dibromo-3-chloropropane [96-12-8]^0.48 MRK7L050181.00.48 U 1
ug/L SM 6200B-1997 12/05/17 19:421,2-Dibromoethane [106-93-4]^0.42 MRK7L050181.00.42 U 1
ug/L SM 6200B-1997 12/05/17 19:421,2-Dichlorobenzene [95-50-1]^0.052 MRK7L050181.00.052 U 1
ug/L SM 6200B-1997 12/05/17 19:421,2-Dichloroethane [107-06-2]^0.082 MRK7L050181.00.082 U 1
ug/L SM 6200B-1997 12/05/17 19:421,2-Dichloropropane [78-87-5]^0.098 MRK7L050181.00.098 U 1
ug/L SM 6200B-1997 12/05/17 19:421,3,5-Trimethylbenzene [108-67-8]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 19:421,3-Dichlorobenzene [541-73-1]^0.092 MRK7L050181.00.092 U 1
ug/L SM 6200B-1997 12/05/17 19:421,3-Dichloropropane [142-28-9]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 19:421,4-Dichlorobenzene [106-46-7]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 19:422,2-Dichloropropane [594-20-7]^0.12 MRK7L050181.00.12 U 1
ug/L SM 6200B-1997 12/05/17 19:422-Chlorotoluene [95-49-8]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 19:424-Chlorotoluene [106-43-4]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 19:424-Isopropyltoluene [99-87-6]^0.066 MRK7L050181.00.066 U 1
ug/L SM 6200B-1997 12/05/17 19:42Benzene [71-43-2]^0.050 MRK7L050181.00.050 U 1
ug/L SM 6200B-1997 12/05/17 19:42Bromobenzene [108-86-1]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 19:42Bromochloromethane [74-97-5]^0.11 MRK7L050181.00.11 U 1
ug/L SM 6200B-1997 12/05/17 19:42Bromodichloromethane [75-27-4]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 19:42Bromoform [75-25-2]^0.20 MRK7L050181.00.20 U 1
ug/L SM 6200B-1997 12/05/17 19:42Bromomethane [74-83-9]^0.28 MRK7L050181.00.28 U 1
ug/L SM 6200B-1997 12/05/17 19:42Carbon Tetrachloride [56-23-5]^0.082 MRK7L050181.00.082 U 1
ug/L SM 6200B-1997 12/05/17 19:42Chlorobenzene [108-90-7]^0.069 MRK7L050181.00.069 U 1
ug/L SM 6200B-1997 12/05/17 19:42Chloroethane [75-00-3]^0.18 MRK7L050181.00.18 U 1
ug/L SM 6200B-1997 12/05/17 19:42Chloroform [67-66-3]^0.083 MRK7L050181.00.083 U 1
ug/L SM 6200B-1997 12/05/17 19:42Chloromethane [74-87-3]^0.050 MRK7L050181.00.050 U 1
ug/L SM 6200B-1997 12/05/17 19:42cis-1,2-Dichloroethene [156-59-2]^0.075 MRK7L050181.00.075 U 1
ug/L SM 6200B-1997 12/05/17 19:42cis-1,3-Dichloropropene [10061-01-5]^0.073 MRK7L050181.00.073 U 1
ug/L SM 6200B-1997 12/05/17 19:42Dibromochloromethane [124-48-1]^0.067 MRK7L050181.00.067 U 1
ug/L SM 6200B-1997 12/05/17 19:42Dibromomethane [74-95-3]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 19:42Dichlorodifluoromethane [75-71-8]^0.091 MRK7L050181.00.091 U 1
ug/L SM 6200B-1997 12/05/17 19:42Ethylbenzene [100-41-4]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 19:42Freon 113 [76-13-1]^0.35 MRK7L050181.00.35 U 1
ug/L SM 6200B-1997 12/05/17 19:42Hexachlorobutadiene [87-68-3]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 19:42Isopropyl Ether [108-20-3]^0.21 MRK7L050181.00.21 U 1
ug/L SM 6200B-1997 12/05/17 19:42Isopropylbenzene [98-82-8]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 19:42m,p-Xylenes [108-38-3/106-42-3]^0.18 MRK7L050182.00.18 U 1
ug/L SM 6200B-1997 12/05/17 19:42Methylene Chloride [75-09-2]^0.070 MRK7L050182.00.070 U 1
Page 16 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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ANALYTICAL RESULTS
PW-17 EFFDescription:Lab Sample ID:CA17338-07 11/27/17 14:55Received:
CA17338Work Order:11/27/17 13:00Sampled:Ground WaterMatrix:
Justin AbreuSampled By:Project:Dixie - MWs
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 12/05/17 19:42Methyl-tert-Butyl Ether [1634-04-4]^0.12 MRK7L050181.00.12 U 1
ug/L SM 6200B-1997 12/05/17 19:42Naphthalene [91-20-3]^0.086 MRK7L050181.00.086 U 1
ug/L SM 6200B-1997 12/05/17 19:42n-Butyl Benzene [104-51-8]^0.074 MRK7L050181.00.074 U 1
ug/L SM 6200B-1997 12/05/17 19:42n-Propyl Benzene [103-65-1]^0.073 MRK7L050181.00.073 U 1
ug/L SM 6200B-1997 12/05/17 19:42o-Xylene [95-47-6]^0.088 MRK7L050181.00.088 U 1
ug/L SM 6200B-1997 12/05/17 19:42sec-Butylbenzene [135-98-8]^0.053 MRK7L050181.00.053 U 1
ug/L SM 6200B-1997 12/05/17 19:42Styrene [100-42-5]^0.082 MRK7L050181.00.082 U 1
ug/L SM 6200B-1997 12/05/17 19:42tert-Butylbenzene [98-06-6]^0.094 MRK7L050181.00.094 U 1
ug/L SM 6200B-1997 12/05/17 19:42Tetrachloroethene [127-18-4]^0.099 MRK7L050181.00.099 U 1
ug/L SM 6200B-1997 12/05/17 19:42Toluene [108-88-3]^0.053 MRK7L050181.00.053 U 1
ug/L SM 6200B-1997 12/05/17 19:42trans-1,2-Dichloroethene [156-60-5]^0.11 MRK7L050181.00.11 U 1
ug/L SM 6200B-1997 12/05/17 19:42trans-1,3-Dichloropropene [10061-02-6]^0.080 MRK7L050181.00.080 U 1
ug/L SM 6200B-1997 12/05/17 19:42Trichloroethene [79-01-6]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 19:42Trichlorofluoromethane [75-69-4]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 19:42Vinyl chloride [75-01-4]^0.083 MRK7L050181.00.083 U 1
ug/L SM 6200B-1997 12/05/17 19:42Xylenes (Total) [1330-20-7]^0.22 MRK7L050181.00.22 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 70-13081 %MRKSM 6200B-1997 12/05/17 19:427L050184150.0 1
Dibromofluoromethane 70-13096 %MRKSM 6200B-1997 12/05/17 19:427L050184850.0 1
Toluene-d8 70-13094 %MRKSM 6200B-1997 12/05/17 19:427L050184750.0 1
Page 17 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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ANALYTICAL RESULTS
PW-18Description:Lab Sample ID:CA17338-08 11/27/17 14:55Received:
CA17338Work Order:11/27/17 12:49Sampled:Ground WaterMatrix:
Justin AbreuSampled By:Project:Dixie - MWs
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 12/05/17 20:121,1,1,2-Tetrachloroethane [630-20-6]^0.091 MRK7L050181.00.091 U 1
ug/L SM 6200B-1997 12/05/17 20:121,1,1-Trichloroethane [71-55-6]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 20:121,1,2,2-Tetrachloroethane [79-34-5]^0.085 MRK7L050181.00.085 U 1
ug/L SM 6200B-1997 12/05/17 20:121,1,2-Trichloroethane [79-00-5]^0.068 MRK7L050181.00.068 U 1
ug/L SM 6200B-1997 12/05/17 20:121,1-Dichloroethane [75-34-3]^0.050 MRK7L050181.00.050 U 1
ug/L SM 6200B-1997 12/05/17 20:121,1-Dichloroethene [75-35-4]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 20:121,1-Dichloropropene [563-58-6]^0.063 MRK7L050181.00.063 U 1
ug/L SM 6200B-1997 12/05/17 20:121,2,3-Trichlorobenzene [87-61-6]^0.25 MRK7L050181.00.25 U 1
ug/L SM 6200B-1997 12/05/17 20:121,2,3-Trichloropropane [96-18-4]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 20:121,2,4-Trichlorobenzene [120-82-1]^0.097 MRK7L050181.00.097 U 1
ug/L SM 6200B-1997 12/05/17 20:121,2,4-Trimethylbenzene [95-63-6]^0.067 MRK7L050181.00.067 U 1
ug/L SM 6200B-1997 12/05/17 20:121,2-Dibromo-3-chloropropane [96-12-8]^0.48 MRK7L050181.00.48 U 1
ug/L SM 6200B-1997 12/05/17 20:121,2-Dibromoethane [106-93-4]^0.42 MRK7L050181.00.42 U 1
ug/L SM 6200B-1997 12/05/17 20:121,2-Dichlorobenzene [95-50-1]^0.052 MRK7L050181.00.052 U 1
ug/L SM 6200B-1997 12/05/17 20:121,2-Dichloroethane [107-06-2]^0.082 MRK7L050181.00.082 U 1
ug/L SM 6200B-1997 12/05/17 20:121,2-Dichloropropane [78-87-5]^0.098 MRK7L050181.00.098 U 1
ug/L SM 6200B-1997 12/05/17 20:121,3,5-Trimethylbenzene [108-67-8]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 20:121,3-Dichlorobenzene [541-73-1]^0.092 MRK7L050181.00.092 U 1
ug/L SM 6200B-1997 12/05/17 20:121,3-Dichloropropane [142-28-9]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 20:121,4-Dichlorobenzene [106-46-7]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 20:122,2-Dichloropropane [594-20-7]^0.12 MRK7L050181.00.12 U 1
ug/L SM 6200B-1997 12/05/17 20:122-Chlorotoluene [95-49-8]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 20:124-Chlorotoluene [106-43-4]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 20:124-Isopropyltoluene [99-87-6]^0.066 MRK7L050181.00.066 U 1
ug/L SM 6200B-1997 12/05/17 20:12Benzene [71-43-2]^0.050 MRK7L050181.00.050 U 1
ug/L SM 6200B-1997 12/05/17 20:12Bromobenzene [108-86-1]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 20:12Bromochloromethane [74-97-5]^0.11 MRK7L050181.00.11 U 1
ug/L SM 6200B-1997 12/05/17 20:12Bromodichloromethane [75-27-4]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 20:12Bromoform [75-25-2]^0.20 MRK7L050181.00.20 U 1
ug/L SM 6200B-1997 12/05/17 20:12Bromomethane [74-83-9]^0.28 MRK7L050181.00.28 U 1
ug/L SM 6200B-1997 12/05/17 20:12Carbon Tetrachloride [56-23-5]^0.082 MRK7L050181.00.082 U 1
ug/L SM 6200B-1997 12/05/17 20:12Chlorobenzene [108-90-7]^0.069 MRK7L050181.00.069 U 1
ug/L SM 6200B-1997 12/05/17 20:12Chloroethane [75-00-3]^0.18 MRK7L050181.00.18 U 1
ug/L SM 6200B-1997 12/05/17 20:12Chloroform [67-66-3]^0.083 MRK7L050181.00.083 U 1
ug/L SM 6200B-1997 12/05/17 20:12Chloromethane [74-87-3]^0.050 MRK7L050181.00.050 U 1
ug/L SM 6200B-1997 12/05/17 20:12cis-1,2-Dichloroethene [156-59-2]^0.075 MRK7L050181.00.075 U 1
ug/L SM 6200B-1997 12/05/17 20:12cis-1,3-Dichloropropene [10061-01-5]^0.073 MRK7L050181.00.073 U 1
ug/L SM 6200B-1997 12/05/17 20:12Dibromochloromethane [124-48-1]^0.067 MRK7L050181.00.067 U 1
ug/L SM 6200B-1997 12/05/17 20:12Dibromomethane [74-95-3]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 20:12Dichlorodifluoromethane [75-71-8]^0.091 MRK7L050181.00.091 U 1
ug/L SM 6200B-1997 12/05/17 20:12Ethylbenzene [100-41-4]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 20:12Freon 113 [76-13-1]^0.35 MRK7L050181.00.35 U 1
ug/L SM 6200B-1997 12/05/17 20:12Hexachlorobutadiene [87-68-3]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 20:12Isopropyl Ether [108-20-3]^0.21 MRK7L050181.00.21 U 1
ug/L SM 6200B-1997 12/05/17 20:12Isopropylbenzene [98-82-8]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 20:12m,p-Xylenes [108-38-3/106-42-3]^0.18 MRK7L050182.00.18 U 1
ug/L SM 6200B-1997 12/05/17 20:12Methylene Chloride [75-09-2]^0.070 MRK7L050182.00.070 U 1
Page 18 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
PW-18Description:Lab Sample ID:CA17338-08 11/27/17 14:55Received:
CA17338Work Order:11/27/17 12:49Sampled:Ground WaterMatrix:
Justin AbreuSampled By:Project:Dixie - MWs
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 12/05/17 20:12Methyl-tert-Butyl Ether [1634-04-4]^0.12 MRK7L050181.01.2 1
ug/L SM 6200B-1997 12/05/17 20:12Naphthalene [91-20-3]^0.086 MRK7L050181.00.086 U 1
ug/L SM 6200B-1997 12/05/17 20:12n-Butyl Benzene [104-51-8]^0.074 MRK7L050181.00.074 U 1
ug/L SM 6200B-1997 12/05/17 20:12n-Propyl Benzene [103-65-1]^0.073 MRK7L050181.00.073 U 1
ug/L SM 6200B-1997 12/05/17 20:12o-Xylene [95-47-6]^0.088 MRK7L050181.00.088 U 1
ug/L SM 6200B-1997 12/05/17 20:12sec-Butylbenzene [135-98-8]^0.053 MRK7L050181.00.053 U 1
ug/L SM 6200B-1997 12/05/17 20:12Styrene [100-42-5]^0.082 MRK7L050181.00.082 U 1
ug/L SM 6200B-1997 12/05/17 20:12tert-Butylbenzene [98-06-6]^0.094 MRK7L050181.00.094 U 1
ug/L SM 6200B-1997 12/05/17 20:12Tetrachloroethene [127-18-4]^0.099 MRK7L050181.00.099 U 1
ug/L SM 6200B-1997 12/05/17 20:12Toluene [108-88-3]^0.053 MRK7L050181.00.053 U 1
ug/L SM 6200B-1997 12/05/17 20:12trans-1,2-Dichloroethene [156-60-5]^0.11 MRK7L050181.00.11 U 1
ug/L SM 6200B-1997 12/05/17 20:12trans-1,3-Dichloropropene [10061-02-6]^0.080 MRK7L050181.00.080 U 1
ug/L SM 6200B-1997 12/05/17 20:12Trichloroethene [79-01-6]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 20:12Trichlorofluoromethane [75-69-4]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 20:12Vinyl chloride [75-01-4]^0.083 MRK7L050181.00.083 U 1
ug/L SM 6200B-1997 12/05/17 20:12Xylenes (Total) [1330-20-7]^0.22 MRK7L050181.00.22 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 70-13081 %MRKSM 6200B-1997 12/05/17 20:127L050184050.0 1
Dibromofluoromethane 70-13092 %MRKSM 6200B-1997 12/05/17 20:127L050184650.0 1
Toluene-d8 70-13091 %MRKSM 6200B-1997 12/05/17 20:127L050184650.0 1
Page 19 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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ANALYTICAL RESULTS
PW-22Description:Lab Sample ID:CA17338-09 11/27/17 14:55Received:
CA17338Work Order:11/27/17 13:16Sampled:Ground WaterMatrix:
Justin AbreuSampled By:Project:Dixie - MWs
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 12/05/17 20:421,1,1,2-Tetrachloroethane [630-20-6]^0.091 MRK7L050181.00.091 U 1
ug/L SM 6200B-1997 12/05/17 20:421,1,1-Trichloroethane [71-55-6]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 20:421,1,2,2-Tetrachloroethane [79-34-5]^0.085 MRK7L050181.00.085 U 1
ug/L SM 6200B-1997 12/05/17 20:421,1,2-Trichloroethane [79-00-5]^0.068 MRK7L050181.00.068 U 1
ug/L SM 6200B-1997 12/05/17 20:421,1-Dichloroethane [75-34-3]^0.050 MRK7L050181.00.050 U 1
ug/L SM 6200B-1997 12/05/17 20:421,1-Dichloroethene [75-35-4]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 20:421,1-Dichloropropene [563-58-6]^0.063 MRK7L050181.00.063 U 1
ug/L SM 6200B-1997 12/05/17 20:421,2,3-Trichlorobenzene [87-61-6]^0.25 MRK7L050181.00.25 U 1
ug/L SM 6200B-1997 12/05/17 20:421,2,3-Trichloropropane [96-18-4]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 20:421,2,4-Trichlorobenzene [120-82-1]^0.097 MRK7L050181.00.097 U 1
ug/L SM 6200B-1997 12/05/17 20:421,2,4-Trimethylbenzene [95-63-6]^0.067 MRK7L050181.00.067 U 1
ug/L SM 6200B-1997 12/05/17 20:421,2-Dibromo-3-chloropropane [96-12-8]^0.48 MRK7L050181.00.48 U 1
ug/L SM 6200B-1997 12/05/17 20:421,2-Dibromoethane [106-93-4]^0.42 MRK7L050181.00.42 U 1
ug/L SM 6200B-1997 12/05/17 20:421,2-Dichlorobenzene [95-50-1]^0.052 MRK7L050181.00.052 U 1
ug/L SM 6200B-1997 12/05/17 20:421,2-Dichloroethane [107-06-2]^0.082 MRK7L050181.00.082 U 1
ug/L SM 6200B-1997 12/05/17 20:421,2-Dichloropropane [78-87-5]^0.098 MRK7L050181.00.098 U 1
ug/L SM 6200B-1997 12/05/17 20:421,3,5-Trimethylbenzene [108-67-8]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 20:421,3-Dichlorobenzene [541-73-1]^0.092 MRK7L050181.00.092 U 1
ug/L SM 6200B-1997 12/05/17 20:421,3-Dichloropropane [142-28-9]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 20:421,4-Dichlorobenzene [106-46-7]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 20:422,2-Dichloropropane [594-20-7]^0.12 MRK7L050181.00.12 U 1
ug/L SM 6200B-1997 12/05/17 20:422-Chlorotoluene [95-49-8]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 20:424-Chlorotoluene [106-43-4]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 20:424-Isopropyltoluene [99-87-6]^0.066 MRK7L050181.00.066 U 1
ug/L SM 6200B-1997 12/05/17 20:42Benzene [71-43-2]^0.050 MRK7L050181.00.050 U 1
ug/L SM 6200B-1997 12/05/17 20:42Bromobenzene [108-86-1]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 20:42Bromochloromethane [74-97-5]^0.11 MRK7L050181.00.11 U 1
ug/L SM 6200B-1997 12/05/17 20:42Bromodichloromethane [75-27-4]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 20:42Bromoform [75-25-2]^0.20 MRK7L050181.00.20 U 1
ug/L SM 6200B-1997 12/05/17 20:42Bromomethane [74-83-9]^0.28 MRK7L050181.00.28 U 1
ug/L SM 6200B-1997 12/05/17 20:42Carbon Tetrachloride [56-23-5]^0.082 MRK7L050181.00.082 U 1
ug/L SM 6200B-1997 12/05/17 20:42Chlorobenzene [108-90-7]^0.069 MRK7L050181.00.069 U 1
ug/L SM 6200B-1997 12/05/17 20:42Chloroethane [75-00-3]^0.18 MRK7L050181.00.18 U 1
ug/L SM 6200B-1997 12/05/17 20:42Chloroform [67-66-3]^0.083 MRK7L050181.00.083 U 1
ug/L SM 6200B-1997 12/05/17 20:42Chloromethane [74-87-3]^0.050 MRK7L050181.00.050 U 1
ug/L SM 6200B-1997 12/05/17 20:42cis-1,2-Dichloroethene [156-59-2]^0.075 MRK7L050181.00.075 U 1
ug/L SM 6200B-1997 12/05/17 20:42cis-1,3-Dichloropropene [10061-01-5]^0.073 MRK7L050181.00.073 U 1
ug/L SM 6200B-1997 12/05/17 20:42Dibromochloromethane [124-48-1]^0.067 MRK7L050181.00.067 U 1
ug/L SM 6200B-1997 12/05/17 20:42Dibromomethane [74-95-3]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 20:42Dichlorodifluoromethane [75-71-8]^0.091 MRK7L050181.00.091 U 1
ug/L SM 6200B-1997 12/05/17 20:42Ethylbenzene [100-41-4]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 20:42Freon 113 [76-13-1]^0.35 MRK7L050181.00.35 U 1
ug/L SM 6200B-1997 12/05/17 20:42Hexachlorobutadiene [87-68-3]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 20:42Isopropyl Ether [108-20-3]^0.21 MRK7L050181.00.21 U 1
ug/L SM 6200B-1997 12/05/17 20:42Isopropylbenzene [98-82-8]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 20:42m,p-Xylenes [108-38-3/106-42-3]^0.18 MRK7L050182.00.18 U 1
ug/L SM 6200B-1997 12/05/17 20:42Methylene Chloride [75-09-2]^0.070 MRK7L050182.00.070 U 1
Page 20 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
PW-22Description:Lab Sample ID:CA17338-09 11/27/17 14:55Received:
CA17338Work Order:11/27/17 13:16Sampled:Ground WaterMatrix:
Justin AbreuSampled By:Project:Dixie - MWs
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 12/05/17 20:42Methyl-tert-Butyl Ether [1634-04-4]^0.12 MRK7L050181.00.56 J 1
ug/L SM 6200B-1997 12/05/17 20:42Naphthalene [91-20-3]^0.086 MRK7L050181.00.086 U 1
ug/L SM 6200B-1997 12/05/17 20:42n-Butyl Benzene [104-51-8]^0.074 MRK7L050181.00.074 U 1
ug/L SM 6200B-1997 12/05/17 20:42n-Propyl Benzene [103-65-1]^0.073 MRK7L050181.00.073 U 1
ug/L SM 6200B-1997 12/05/17 20:42o-Xylene [95-47-6]^0.088 MRK7L050181.00.088 U 1
ug/L SM 6200B-1997 12/05/17 20:42sec-Butylbenzene [135-98-8]^0.053 MRK7L050181.00.053 U 1
ug/L SM 6200B-1997 12/05/17 20:42Styrene [100-42-5]^0.082 MRK7L050181.00.082 U 1
ug/L SM 6200B-1997 12/05/17 20:42tert-Butylbenzene [98-06-6]^0.094 MRK7L050181.00.094 U 1
ug/L SM 6200B-1997 12/05/17 20:42Tetrachloroethene [127-18-4]^0.099 MRK7L050181.00.099 U 1
ug/L SM 6200B-1997 12/05/17 20:42Toluene [108-88-3]^0.053 MRK7L050181.00.053 U 1
ug/L SM 6200B-1997 12/05/17 20:42trans-1,2-Dichloroethene [156-60-5]^0.11 MRK7L050181.00.11 U 1
ug/L SM 6200B-1997 12/05/17 20:42trans-1,3-Dichloropropene [10061-02-6]^0.080 MRK7L050181.00.080 U 1
ug/L SM 6200B-1997 12/05/17 20:42Trichloroethene [79-01-6]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 20:42Trichlorofluoromethane [75-69-4]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 20:42Vinyl chloride [75-01-4]^0.083 MRK7L050181.00.083 U 1
ug/L SM 6200B-1997 12/05/17 20:42Xylenes (Total) [1330-20-7]^0.22 MRK7L050181.00.22 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 70-13079 %MRKSM 6200B-1997 12/05/17 20:427L050184050.0 1
Dibromofluoromethane 70-13093 %MRKSM 6200B-1997 12/05/17 20:427L050184750.0 1
Toluene-d8 70-13093 %MRKSM 6200B-1997 12/05/17 20:427L050184650.0 1
Page 21 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
PW-23Description:Lab Sample ID:CA17338-10 11/27/17 14:55Received:
CA17338Work Order:11/27/17 13:22Sampled:Ground WaterMatrix:
Justin AbreuSampled By:Project:Dixie - MWs
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 12/05/17 21:121,1,1,2-Tetrachloroethane [630-20-6]^0.091 MRK7L050181.00.091 U 1
ug/L SM 6200B-1997 12/05/17 21:121,1,1-Trichloroethane [71-55-6]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 21:121,1,2,2-Tetrachloroethane [79-34-5]^0.085 MRK7L050181.00.085 U 1
ug/L SM 6200B-1997 12/05/17 21:121,1,2-Trichloroethane [79-00-5]^0.068 MRK7L050181.00.068 U 1
ug/L SM 6200B-1997 12/05/17 21:121,1-Dichloroethane [75-34-3]^0.050 MRK7L050181.00.050 U 1
ug/L SM 6200B-1997 12/05/17 21:121,1-Dichloroethene [75-35-4]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 21:121,1-Dichloropropene [563-58-6]^0.063 MRK7L050181.00.063 U 1
ug/L SM 6200B-1997 12/05/17 21:121,2,3-Trichlorobenzene [87-61-6]^0.25 MRK7L050181.00.25 U 1
ug/L SM 6200B-1997 12/05/17 21:121,2,3-Trichloropropane [96-18-4]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 21:121,2,4-Trichlorobenzene [120-82-1]^0.097 MRK7L050181.00.097 U 1
ug/L SM 6200B-1997 12/05/17 21:121,2,4-Trimethylbenzene [95-63-6]^0.067 MRK7L050181.00.067 U 1
ug/L SM 6200B-1997 12/05/17 21:121,2-Dibromo-3-chloropropane [96-12-8]^0.48 MRK7L050181.00.48 U 1
ug/L SM 6200B-1997 12/05/17 21:121,2-Dibromoethane [106-93-4]^0.42 MRK7L050181.00.42 U 1
ug/L SM 6200B-1997 12/05/17 21:121,2-Dichlorobenzene [95-50-1]^0.052 MRK7L050181.00.052 U 1
ug/L SM 6200B-1997 12/05/17 21:121,2-Dichloroethane [107-06-2]^0.082 MRK7L050181.00.082 U 1
ug/L SM 6200B-1997 12/05/17 21:121,2-Dichloropropane [78-87-5]^0.098 MRK7L050181.00.098 U 1
ug/L SM 6200B-1997 12/05/17 21:121,3,5-Trimethylbenzene [108-67-8]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 21:121,3-Dichlorobenzene [541-73-1]^0.092 MRK7L050181.00.092 U 1
ug/L SM 6200B-1997 12/05/17 21:121,3-Dichloropropane [142-28-9]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 21:121,4-Dichlorobenzene [106-46-7]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 21:122,2-Dichloropropane [594-20-7]^0.12 MRK7L050181.00.12 U 1
ug/L SM 6200B-1997 12/05/17 21:122-Chlorotoluene [95-49-8]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 21:124-Chlorotoluene [106-43-4]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 21:124-Isopropyltoluene [99-87-6]^0.066 MRK7L050181.00.066 U 1
ug/L SM 6200B-1997 12/05/17 21:12Benzene [71-43-2]^0.050 MRK7L050181.00.050 U 1
ug/L SM 6200B-1997 12/05/17 21:12Bromobenzene [108-86-1]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 21:12Bromochloromethane [74-97-5]^0.11 MRK7L050181.00.11 U 1
ug/L SM 6200B-1997 12/05/17 21:12Bromodichloromethane [75-27-4]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 21:12Bromoform [75-25-2]^0.20 MRK7L050181.00.20 U 1
ug/L SM 6200B-1997 12/05/17 21:12Bromomethane [74-83-9]^0.28 MRK7L050181.00.28 U 1
ug/L SM 6200B-1997 12/05/17 21:12Carbon Tetrachloride [56-23-5]^0.082 MRK7L050181.00.082 U 1
ug/L SM 6200B-1997 12/05/17 21:12Chlorobenzene [108-90-7]^0.069 MRK7L050181.00.069 U 1
ug/L SM 6200B-1997 12/05/17 21:12Chloroethane [75-00-3]^0.18 MRK7L050181.00.18 U 1
ug/L SM 6200B-1997 12/05/17 21:12Chloroform [67-66-3]^0.083 MRK7L050181.00.083 U 1
ug/L SM 6200B-1997 12/05/17 21:12Chloromethane [74-87-3]^0.050 MRK7L050181.00.050 U 1
ug/L SM 6200B-1997 12/05/17 21:12cis-1,2-Dichloroethene [156-59-2]^0.075 MRK7L050181.00.075 U 1
ug/L SM 6200B-1997 12/05/17 21:12cis-1,3-Dichloropropene [10061-01-5]^0.073 MRK7L050181.00.073 U 1
ug/L SM 6200B-1997 12/05/17 21:12Dibromochloromethane [124-48-1]^0.067 MRK7L050181.00.067 U 1
ug/L SM 6200B-1997 12/05/17 21:12Dibromomethane [74-95-3]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 21:12Dichlorodifluoromethane [75-71-8]^0.091 MRK7L050181.00.091 U 1
ug/L SM 6200B-1997 12/05/17 21:12Ethylbenzene [100-41-4]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 21:12Freon 113 [76-13-1]^0.35 MRK7L050181.00.35 U 1
ug/L SM 6200B-1997 12/05/17 21:12Hexachlorobutadiene [87-68-3]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 21:12Isopropyl Ether [108-20-3]^0.21 MRK7L050181.00.21 U 1
ug/L SM 6200B-1997 12/05/17 21:12Isopropylbenzene [98-82-8]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 21:12m,p-Xylenes [108-38-3/106-42-3]^0.18 MRK7L050182.00.18 U 1
ug/L SM 6200B-1997 12/05/17 21:12Methylene Chloride [75-09-2]^0.070 MRK7L050182.00.070 U 1
Page 22 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
PW-23Description:Lab Sample ID:CA17338-10 11/27/17 14:55Received:
CA17338Work Order:11/27/17 13:22Sampled:Ground WaterMatrix:
Justin AbreuSampled By:Project:Dixie - MWs
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 12/05/17 21:12Methyl-tert-Butyl Ether [1634-04-4]^0.12 MRK7L050181.00.12 U 1
ug/L SM 6200B-1997 12/05/17 21:12Naphthalene [91-20-3]^0.086 MRK7L050181.00.086 U 1
ug/L SM 6200B-1997 12/05/17 21:12n-Butyl Benzene [104-51-8]^0.074 MRK7L050181.00.074 U 1
ug/L SM 6200B-1997 12/05/17 21:12n-Propyl Benzene [103-65-1]^0.073 MRK7L050181.00.073 U 1
ug/L SM 6200B-1997 12/05/17 21:12o-Xylene [95-47-6]^0.088 MRK7L050181.00.088 U 1
ug/L SM 6200B-1997 12/05/17 21:12sec-Butylbenzene [135-98-8]^0.053 MRK7L050181.00.053 U 1
ug/L SM 6200B-1997 12/05/17 21:12Styrene [100-42-5]^0.082 MRK7L050181.00.082 U 1
ug/L SM 6200B-1997 12/05/17 21:12tert-Butylbenzene [98-06-6]^0.094 MRK7L050181.00.094 U 1
ug/L SM 6200B-1997 12/05/17 21:12Tetrachloroethene [127-18-4]^0.099 MRK7L050181.00.099 U 1
ug/L SM 6200B-1997 12/05/17 21:12Toluene [108-88-3]^0.053 MRK7L050181.00.053 U 1
ug/L SM 6200B-1997 12/05/17 21:12trans-1,2-Dichloroethene [156-60-5]^0.11 MRK7L050181.00.11 U 1
ug/L SM 6200B-1997 12/05/17 21:12trans-1,3-Dichloropropene [10061-02-6]^0.080 MRK7L050181.00.080 U 1
ug/L SM 6200B-1997 12/05/17 21:12Trichloroethene [79-01-6]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 21:12Trichlorofluoromethane [75-69-4]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 21:12Vinyl chloride [75-01-4]^0.083 MRK7L050181.00.083 U 1
ug/L SM 6200B-1997 12/05/17 21:12Xylenes (Total) [1330-20-7]^0.22 MRK7L050181.00.22 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 70-13081 %MRKSM 6200B-1997 12/05/17 21:127L050184150.0 1
Dibromofluoromethane 70-13096 %MRKSM 6200B-1997 12/05/17 21:127L050184850.0 1
Toluene-d8 70-13093 %MRKSM 6200B-1997 12/05/17 21:127L050184750.0 1
Page 23 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
Trip BlankDescription:Lab Sample ID:CA17338-11 11/27/17 14:55Received:
CA17338Work Order:11/27/17 12:08Sampled:WaterMatrix:
Justin AbreuSampled By:Project:Dixie - MWs
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 12/05/17 21:421,1,1,2-Tetrachloroethane [630-20-6]^0.091 MRK7L050181.00.091 U 1
ug/L SM 6200B-1997 12/05/17 21:421,1,1-Trichloroethane [71-55-6]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 21:421,1,2,2-Tetrachloroethane [79-34-5]^0.085 MRK7L050181.00.085 U 1
ug/L SM 6200B-1997 12/05/17 21:421,1,2-Trichloroethane [79-00-5]^0.068 MRK7L050181.00.068 U 1
ug/L SM 6200B-1997 12/05/17 21:421,1-Dichloroethane [75-34-3]^0.050 MRK7L050181.00.050 U 1
ug/L SM 6200B-1997 12/05/17 21:421,1-Dichloroethene [75-35-4]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 21:421,1-Dichloropropene [563-58-6]^0.063 MRK7L050181.00.063 U 1
ug/L SM 6200B-1997 12/05/17 21:421,2,3-Trichlorobenzene [87-61-6]^0.25 MRK7L050181.00.25 U 1
ug/L SM 6200B-1997 12/05/17 21:421,2,3-Trichloropropane [96-18-4]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 21:421,2,4-Trichlorobenzene [120-82-1]^0.097 MRK7L050181.00.097 U 1
ug/L SM 6200B-1997 12/05/17 21:421,2,4-Trimethylbenzene [95-63-6]^0.067 MRK7L050181.00.067 U 1
ug/L SM 6200B-1997 12/05/17 21:421,2-Dibromo-3-chloropropane [96-12-8]^0.48 MRK7L050181.00.48 U 1
ug/L SM 6200B-1997 12/05/17 21:421,2-Dibromoethane [106-93-4]^0.42 MRK7L050181.00.42 U 1
ug/L SM 6200B-1997 12/05/17 21:421,2-Dichlorobenzene [95-50-1]^0.052 MRK7L050181.00.052 U 1
ug/L SM 6200B-1997 12/05/17 21:421,2-Dichloroethane [107-06-2]^0.082 MRK7L050181.00.082 U 1
ug/L SM 6200B-1997 12/05/17 21:421,2-Dichloropropane [78-87-5]^0.098 MRK7L050181.00.098 U 1
ug/L SM 6200B-1997 12/05/17 21:421,3,5-Trimethylbenzene [108-67-8]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 21:421,3-Dichlorobenzene [541-73-1]^0.092 MRK7L050181.00.092 U 1
ug/L SM 6200B-1997 12/05/17 21:421,3-Dichloropropane [142-28-9]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 21:421,4-Dichlorobenzene [106-46-7]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 21:422,2-Dichloropropane [594-20-7]^0.12 MRK7L050181.00.12 U 1
ug/L SM 6200B-1997 12/05/17 21:422-Chlorotoluene [95-49-8]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 21:424-Chlorotoluene [106-43-4]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 21:424-Isopropyltoluene [99-87-6]^0.066 MRK7L050181.00.066 U 1
ug/L SM 6200B-1997 12/05/17 21:42Benzene [71-43-2]^0.050 MRK7L050181.00.050 U 1
ug/L SM 6200B-1997 12/05/17 21:42Bromobenzene [108-86-1]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 21:42Bromochloromethane [74-97-5]^0.11 MRK7L050181.00.11 U 1
ug/L SM 6200B-1997 12/05/17 21:42Bromodichloromethane [75-27-4]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 21:42Bromoform [75-25-2]^0.20 MRK7L050181.00.20 U 1
ug/L SM 6200B-1997 12/05/17 21:42Bromomethane [74-83-9]^0.28 MRK7L050181.00.28 U 1
ug/L SM 6200B-1997 12/05/17 21:42Carbon Tetrachloride [56-23-5]^0.082 MRK7L050181.00.082 U 1
ug/L SM 6200B-1997 12/05/17 21:42Chlorobenzene [108-90-7]^0.069 MRK7L050181.00.069 U 1
ug/L SM 6200B-1997 12/05/17 21:42Chloroethane [75-00-3]^0.18 MRK7L050181.00.18 U 1
ug/L SM 6200B-1997 12/05/17 21:42Chloroform [67-66-3]^0.083 MRK7L050181.00.083 U 1
ug/L SM 6200B-1997 12/05/17 21:42Chloromethane [74-87-3]^0.050 MRK7L050181.00.050 U 1
ug/L SM 6200B-1997 12/05/17 21:42cis-1,2-Dichloroethene [156-59-2]^0.075 MRK7L050181.00.075 U 1
ug/L SM 6200B-1997 12/05/17 21:42cis-1,3-Dichloropropene [10061-01-5]^0.073 MRK7L050181.00.073 U 1
ug/L SM 6200B-1997 12/05/17 21:42Dibromochloromethane [124-48-1]^0.067 MRK7L050181.00.067 U 1
ug/L SM 6200B-1997 12/05/17 21:42Dibromomethane [74-95-3]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 21:42Dichlorodifluoromethane [75-71-8]^0.091 MRK7L050181.00.091 U 1
ug/L SM 6200B-1997 12/05/17 21:42Ethylbenzene [100-41-4]^0.10 MRK7L050181.00.10 U 1
ug/L SM 6200B-1997 12/05/17 21:42Freon 113 [76-13-1]^0.35 MRK7L050181.00.35 U 1
ug/L SM 6200B-1997 12/05/17 21:42Hexachlorobutadiene [87-68-3]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 21:42Isopropyl Ether [108-20-3]^0.21 MRK7L050181.00.21 U 1
ug/L SM 6200B-1997 12/05/17 21:42Isopropylbenzene [98-82-8]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 21:42m,p-Xylenes [108-38-3/106-42-3]^0.18 MRK7L050182.00.18 U 1
ug/L SM 6200B-1997 12/05/17 21:42Methylene Chloride [75-09-2]^0.070 MRK7L050182.00.070 U 1
Page 24 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
Trip BlankDescription:Lab Sample ID:CA17338-11 11/27/17 14:55Received:
CA17338Work Order:11/27/17 12:08Sampled:WaterMatrix:
Justin AbreuSampled By:Project:Dixie - MWs
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 12/05/17 21:42Methyl-tert-Butyl Ether [1634-04-4]^0.12 MRK7L050181.00.12 U 1
ug/L SM 6200B-1997 12/05/17 21:42Naphthalene [91-20-3]^0.086 MRK7L050181.00.086 U 1
ug/L SM 6200B-1997 12/05/17 21:42n-Butyl Benzene [104-51-8]^0.074 MRK7L050181.00.074 U 1
ug/L SM 6200B-1997 12/05/17 21:42n-Propyl Benzene [103-65-1]^0.073 MRK7L050181.00.073 U 1
ug/L SM 6200B-1997 12/05/17 21:42o-Xylene [95-47-6]^0.088 MRK7L050181.00.088 U 1
ug/L SM 6200B-1997 12/05/17 21:42sec-Butylbenzene [135-98-8]^0.053 MRK7L050181.00.053 U 1
ug/L SM 6200B-1997 12/05/17 21:42Styrene [100-42-5]^0.082 MRK7L050181.00.082 U 1
ug/L SM 6200B-1997 12/05/17 21:42tert-Butylbenzene [98-06-6]^0.094 MRK7L050181.00.094 U 1
ug/L SM 6200B-1997 12/05/17 21:42Tetrachloroethene [127-18-4]^0.099 MRK7L050181.00.099 U 1
ug/L SM 6200B-1997 12/05/17 21:42Toluene [108-88-3]^0.053 MRK7L050181.00.053 U 1
ug/L SM 6200B-1997 12/05/17 21:42trans-1,2-Dichloroethene [156-60-5]^0.11 MRK7L050181.00.11 U 1
ug/L SM 6200B-1997 12/05/17 21:42trans-1,3-Dichloropropene [10061-02-6]^0.080 MRK7L050181.00.080 U 1
ug/L SM 6200B-1997 12/05/17 21:42Trichloroethene [79-01-6]^0.13 MRK7L050181.00.13 U 1
ug/L SM 6200B-1997 12/05/17 21:42Trichlorofluoromethane [75-69-4]^0.15 MRK7L050181.00.15 U 1
ug/L SM 6200B-1997 12/05/17 21:42Vinyl chloride [75-01-4]^0.083 MRK7L050181.00.083 U 1
ug/L SM 6200B-1997 12/05/17 21:42Xylenes (Total) [1330-20-7]^0.22 MRK7L050181.00.22 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 70-13079 %MRKSM 6200B-1997 12/05/17 21:427L050183950.0 1
Dibromofluoromethane 70-13093 %MRKSM 6200B-1997 12/05/17 21:427L050184750.0 1
Toluene-d8 70-13090 %MRKSM 6200B-1997 12/05/17 21:427L050184550.0 1
Page 25 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 7L05018 - EPA 5030B_MS
Prepared: 12/05/2017 00:34 Analyzed: 12/05/2017 12:41Blank (7L05018-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.00.091 U 1,1,1,2-Tetrachloroethane
ug/L1.00.15 U 1,1,1-Trichloroethane
ug/L1.00.085 U 1,1,2,2-Tetrachloroethane
ug/L1.00.068 U 1,1,2-Trichloroethane
ug/L1.00.050 U 1,1-Dichloroethane
ug/L1.00.15 U 1,1-Dichloroethene
ug/L1.00.063 U 1,1-Dichloropropene
ug/L1.00.25 U 1,2,3-Trichlorobenzene
ug/L1.00.15 U 1,2,3-Trichloropropane
ug/L1.00.097 U 1,2,4-Trichlorobenzene
ug/L1.00.067 U 1,2,4-Trimethylbenzene
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.42 U 1,2-Dibromoethane
ug/L1.00.052 U 1,2-Dichlorobenzene
ug/L1.00.082 U 1,2-Dichloroethane
ug/L1.00.098 U 1,2-Dichloropropane
ug/L1.00.10 U 1,3,5-Trimethylbenzene
ug/L1.00.092 U 1,3-Dichlorobenzene
ug/L1.00.15 U 1,3-Dichloropropane
ug/L1.00.10 U 1,4-Dichlorobenzene
ug/L1.00.12 U 2,2-Dichloropropane
ug/L1.00.10 U 2-Chlorotoluene
ug/L1.00.10 U 4-Chlorotoluene
ug/L1.00.066 U 4-Isopropyltoluene
ug/L1.00.050 U Benzene
ug/L1.00.13 U Bromobenzene
ug/L1.00.11 U Bromochloromethane
ug/L1.00.10 U Bromodichloromethane
ug/L1.00.20 U Bromoform
ug/L1.00.28 U Bromomethane
ug/L1.00.082 U Carbon Tetrachloride
ug/L1.00.069 U Chlorobenzene
ug/L1.00.18 U Chloroethane
ug/L1.00.083 U Chloroform
ug/L1.00.050 U Chloromethane
ug/L1.00.075 U cis-1,2-Dichloroethene
ug/L1.00.073 U cis-1,3-Dichloropropene
ug/L1.00.067 U Dibromochloromethane
ug/L1.00.13 U Dibromomethane
ug/L1.00.091 U Dichlorodifluoromethane
ug/L1.00.10 U Ethylbenzene
ug/L1.00.35 U Freon 113
ug/L1.00.15 U Hexachlorobutadiene
ug/L1.00.21 U Isopropyl Ether
ug/L1.00.13 U Isopropylbenzene
ug/L2.00.18 U m,p-Xylenes
ug/L2.00.070 U Methylene Chloride
ug/L1.00.12 U Methyl-tert-Butyl Ether
ug/L1.00.086 U Naphthalene
Page 26 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 7L05018 - EPA 5030B_MS - Continued
Prepared: 12/05/2017 00:34 Analyzed: 12/05/2017 12:41Blank (7L05018-BLK1) Continued
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.00.074 U n-Butyl Benzene
ug/L1.00.073 U n-Propyl Benzene
ug/L1.00.088 U o-Xylene
ug/L1.00.053 U sec-Butylbenzene
ug/L1.00.082 U Styrene
ug/L1.00.094 U tert-Butylbenzene
ug/L1.00.099 U Tetrachloroethene
ug/L1.00.053 U Toluene
ug/L1.00.11 U trans-1,2-Dichloroethene
ug/L1.00.080 U trans-1,3-Dichloropropene
ug/L1.00.13 U Trichloroethene
ug/L1.00.15 U Trichlorofluoromethane
ug/L1.00.083 U Vinyl chloride
ug/L1.00.22 U Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 8140
ug/L 50.0 70-130Dibromofluoromethane9145
ug/L 50.0 70-130Toluene-d8 9045
Prepared: 12/05/2017 00:34 Analyzed: 12/05/2017 10:40LCS (7L05018-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 70-13010421 1,1,1,2-Tetrachloroethane
ug/L1.0 20.0 70-13010321 1,1,1-Trichloroethane
ug/L1.0 20.0 70-13010321 1,1,2,2-Tetrachloroethane
ug/L1.0 20.0 70-13010020 1,1,2-Trichloroethane
ug/L1.0 20.0 70-13010721 1,1-Dichloroethane
ug/L1.0 20.0 70-1309820 1,1-Dichloroethene
ug/L1.0 20.0 70-13010421 1,1-Dichloropropene
ug/L1.0 20.0 70-13011222 1,2,3-Trichlorobenzene
ug/L1.0 20.0 70-1309619 1,2,3-Trichloropropane
ug/L1.0 20.0 70-13010020 1,2,4-Trichlorobenzene
ug/L1.0 20.0 70-13010220 1,2,4-Trimethylbenzene
ug/L1.0 20.0 70-1309519 1,2-Dibromo-3-chloropropane
ug/L1.0 20.0 70-13010020 1,2-Dibromoethane
ug/L1.0 20.0 70-13010321 1,2-Dichlorobenzene
ug/L1.0 20.0 70-13010120 1,2-Dichloroethane
ug/L1.0 20.0 70-13010521 1,2-Dichloropropane
ug/L1.0 20.0 70-13010220 1,3,5-Trimethylbenzene
ug/L1.0 20.0 70-13010321 1,3-Dichlorobenzene
ug/L1.0 20.0 70-1309319 1,3-Dichloropropane
ug/L1.0 20.0 70-13010621 1,4-Dichlorobenzene
ug/L1.0 20.0 70-13010120 2,2-Dichloropropane
ug/L1.0 20.0 70-13010521 2-Chlorotoluene
ug/L1.0 20.0 70-13010120 4-Chlorotoluene
ug/L1.0 20.0 70-13010321 4-Isopropyltoluene
ug/L1.0 20.0 70-13011022 Benzene
ug/L1.0 20.0 70-1309519 Bromobenzene
ug/L1.0 20.0 70-13011323 Bromochloromethane
ug/L1.0 20.0 70-13010922 Bromodichloromethane
Page 27 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 7L05018 - EPA 5030B_MS - Continued
Prepared: 12/05/2017 00:34 Analyzed: 12/05/2017 10:40LCS (7L05018-BS1) Continued
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 70-1309719 Bromoform
ug/L1.0 20.0 60-14011323 Bromomethane
ug/L1.0 20.0 70-13010321 Carbon Tetrachloride
ug/L1.0 20.0 70-13010822 Chlorobenzene
ug/L1.0 20.0 60-1409619 Chloroethane
ug/L1.0 20.0 70-13011423 Chloroform
ug/L1.0 20.0 60-14010822 Chloromethane
ug/L1.0 20.0 70-13010220 cis-1,2-Dichloroethene
ug/L1.0 20.0 70-1309920 cis-1,3-Dichloropropene
ug/L1.0 20.0 70-13010421 Dibromochloromethane
ug/L1.0 20.0 70-13010220 Dibromomethane
ug/L1.0 20.0 60-1409419 Dichlorodifluoromethane
ug/L1.0 20.0 70-13010120 Ethylbenzene
ug/L1.0 40.0 70-13010542 Freon 113
ug/L1.0 20.0 70-13010922 Hexachlorobutadiene
ug/L1.0 20.0 70-1309519 Isopropyl Ether
ug/L1.0 20.0 70-13010621 Isopropylbenzene
ug/L2.0 40.0 70-13010542 m,p-Xylenes
ug/L2.0 20.0 70-13010721 Methylene Chloride
ug/L1.0 20.0 70-1309319 Methyl-tert-Butyl Ether
ug/L1.0 20.0 70-1309018 Naphthalene
ug/L1.0 20.0 70-13011122 n-Butyl Benzene
ug/L1.0 20.0 70-13010220 n-Propyl Benzene
ug/L1.0 20.0 70-1309719 o-Xylene
ug/L1.0 20.0 70-13010521 sec-Butylbenzene
ug/L1.0 20.0 70-13010020 Styrene
ug/L1.0 20.0 70-13010220 tert-Butylbenzene
ug/L1.0 20.0 70-13010020 Tetrachloroethene
ug/L1.0 20.0 70-13010721 Toluene
ug/L1.0 20.0 70-13010020 trans-1,2-Dichloroethene
ug/L1.0 20.0 70-13010321 trans-1,3-Dichloropropene
ug/L1.0 20.0 70-13010321 Trichloroethene
ug/L1.0 20.0 60-14010120 Trichlorofluoromethane
ug/L1.0 20.0 60-1409719 Vinyl chloride
ug/L1.0 60.0 70-13010261 Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 8342
ug/L 50.0 70-130Dibromofluoromethane8945
ug/L 50.0 70-130Toluene-d8 9447
Prepared: 12/05/2017 00:34 Analyzed: 12/05/2017 11:10Matrix Spike (7L05018-MS1)
Source: CA18761-03
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 25.0 71-1171050.091 U26 1,1,1,2-Tetrachloroethane
ug/L1.0 25.0 72-1431070.15 U27 1,1,1-Trichloroethane
ug/L1.0 25.0 59-1331000.085 U25 1,1,2,2-Tetrachloroethane
ug/L1.0 25.0 67-118990.068 U25 1,1,2-Trichloroethane
ug/L1.0 25.0 79-1411080.050 U27 1,1-Dichloroethane
ug/L1.0 25.0 75-1331000.15 U25 1,1-Dichloroethene
ug/L1.0 25.0 70-1291070.063 U27 1,1-Dichloropropene
Page 28 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 7L05018 - EPA 5030B_MS - Continued
Prepared: 12/05/2017 00:34 Analyzed: 12/05/2017 11:10Matrix Spike (7L05018-MS1) Continued
Source: CA18761-03
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 25.0 62-1171070.25 U27 1,2,3-Trichlorobenzene
ug/L1.0 25.0 58-140960.15 U24 1,2,3-Trichloropropane
ug/L1.0 25.0 59-1221000.097 U25 1,2,4-Trichlorobenzene
ug/L1.0 25.0 74-1231020.067 U26 1,2,4-Trimethylbenzene
ug/L1.0 25.0 37-157900.48 U22 1,2-Dibromo-3-chloropropane
ug/L1.0 25.0 66-123980.42 U25 1,2-Dibromoethane
ug/L1.0 25.0 76-1161040.052 U26 1,2-Dichlorobenzene
ug/L1.0 25.0 72-151960.082 U24 1,2-Dichloroethane
ug/L1.0 25.0 78-1251040.098 U26 1,2-Dichloropropane
ug/L1.0 25.0 77-1291030.10 U26 1,3,5-Trimethylbenzene
ug/L1.0 25.0 76-1191060.092 U26 1,3-Dichlorobenzene
ug/L1.0 25.0 60-129930.15 U23 1,3-Dichloropropane
ug/L1.0 25.0 76-1221080.10 U27 1,4-Dichlorobenzene
ug/L1.0 25.0 21-1671080.12 U27 2,2-Dichloropropane
ug/L1.0 25.0 73-1351040.10 U26 2-Chlorotoluene
ug/L1.0 25.0 76-1341020.10 U26 4-Chlorotoluene
ug/L1.0 25.0 75-1271060.066 U26 4-Isopropyltoluene
ug/L1.0 25.0 81-1341110.050 U28 Benzene
ug/L1.0 25.0 72-115960.13 U24 Bromobenzene
ug/L1.0 25.0 74-1281100.11 U27 Bromochloromethane
ug/L1.0 25.0 72-1291080.10 U27 Bromodichloromethane
ug/L1.0 25.0 73-119940.20 U23 Bromoform
ug/L1.0 20.0 38-1891100.28 U22 Bromomethane
ug/L1.0 25.0 68-1421110.082 U28 Carbon Tetrachloride
ug/L1.0 25.0 83-1171130.069 U28 Chlorobenzene
ug/L1.0 20.0 45-213910.18 U18 Chloroethane
ug/L1.0 25.0 78-1381140.083 U28 Chloroform
ug/L1.0 20.0 56-1711070.050 U21 Chloromethane
ug/L1.0 25.0 69-1201040.075 U26 cis-1,2-Dichloroethene
ug/L1.0 25.0 63-1251020.073 U26 cis-1,3-Dichloropropene
ug/L1.0 25.0 73-1171010.067 U25 Dibromochloromethane
ug/L1.0 25.0 76-1241020.13 U25 Dibromomethane
ug/L1.0 20.0 25-161920.091 U18 Dichlorodifluoromethane
ug/L1.0 25.0 68-1241050.10 U26 Ethylbenzene
ug/L1.0 50.0 0-2001140.35 U57 Freon 113
ug/L1.0 25.0 63-1141080.15 U27 Hexachlorobutadiene
ug/L1.0 25.0 70-130970.21 U24 Isopropyl Ether
ug/L1.0 25.0 81-1361110.13 U28 Isopropylbenzene
ug/L2.0 50.0 79-1211100.18 U55 m,p-Xylenes
ug/L2.0 25.0 68-1281080.070 U27 Methylene Chloride
ug/L1.0 25.0 10-127920.12 U23 Methyl-tert-Butyl Ether
ug/L1.0 25.0 50-127850.086 U21 Naphthalene
ug/L1.0 25.0 68-1261160.074 U29 n-Butyl Benzene
ug/L1.0 25.0 76-1251080.073 U27 n-Propyl Benzene
ug/L1.0 25.0 71-1251010.088 U25 o-Xylene
ug/L1.0 25.0 75-1221080.053 U27 sec-Butylbenzene
ug/L1.0 25.0 73-1201030.082 U26 Styrene
ug/L1.0 25.0 70-1371040.094 U26 tert-Butylbenzene
ug/L1.0 25.0 40-1811060.099 U27 Tetrachloroethene
Page 29 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 7L05018 - EPA 5030B_MS - Continued
Prepared: 12/05/2017 00:34 Analyzed: 12/05/2017 11:10Matrix Spike (7L05018-MS1) Continued
Source: CA18761-03
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 25.0 71-1181090.053 U27 Toluene
ug/L1.0 25.0 75-1391020.11 U26 trans-1,2-Dichloroethene
ug/L1.0 25.0 62-1521050.080 U26 trans-1,3-Dichloropropene
ug/L1.0 25.0 75-1151050.13 U26 Trichloroethene
ug/L1.0 20.0 68-1831020.15 U20 Trichlorofluoromethane
ug/L1.0 20.0 49-150960.083 U19 Vinyl chloride
ug/L1.0 75.0 77-1211070.22 U80 Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 8442
ug/L 50.0 70-130Dibromofluoromethane8844
ug/L 50.0 70-130Toluene-d8 9246
Prepared: 12/05/2017 00:34 Analyzed: 12/05/2017 11:41Matrix Spike Dup (7L05018-MSD1)
Source: CA18761-03
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 25.0 1671-117108 30.091 U27 1,1,1,2-Tetrachloroethane
ug/L1.0 25.0 1872-143104 30.15 U26 1,1,1-Trichloroethane
ug/L1.0 25.0 1659-133105 50.085 U26 1,1,2,2-Tetrachloroethane
ug/L1.0 25.0 1867-118101 20.068 U25 1,1,2-Trichloroethane
ug/L1.0 25.0 1979-141106 20.050 U26 1,1-Dichloroethane
ug/L1.0 25.0 2075-13399 10.15 U25 1,1-Dichloroethene
ug/L1.0 25.0 1770-129105 20.063 U26 1,1-Dichloropropene
ug/L1.0 25.0 1762-117110 30.25 U27 1,2,3-Trichlorobenzene
ug/L1.0 25.0 1758-140102 60.15 U26 1,2,3-Trichloropropane
ug/L1.0 25.0 1759-12299 0.40.097 U25 1,2,4-Trichlorobenzene
ug/L1.0 25.0 1874-123103 0.50.067 U26 1,2,4-Trimethylbenzene
ug/L1.0 25.0 1837-15793 30.48 U23 1,2-Dibromo-3-chloropropane
ug/L1.0 25.0 1566-123100 20.42 U25 1,2-Dibromoethane
ug/L1.0 25.0 1676-116105 0.70.052 U26 1,2-Dichlorobenzene
ug/L1.0 25.0 1672-15197 10.082 U24 1,2-Dichloroethane
ug/L1.0 25.0 1978-125104 0.20.098 U26 1,2-Dichloropropane
ug/L1.0 25.0 1677-129102 10.10 U25 1,3,5-Trimethylbenzene
ug/L1.0 25.0 1776-119106 0.20.092 U26 1,3-Dichlorobenzene
ug/L1.0 25.0 1660-12995 20.15 U24 1,3-Dichloropropane
ug/L1.0 25.0 1676-122107 0.90.10 U27 1,4-Dichlorobenzene
ug/L1.0 25.0 2021-167106 30.12 U26 2,2-Dichloropropane
ug/L1.0 25.0 1673-135104 0.040.10 U26 2-Chlorotoluene
ug/L1.0 25.0 1676-134101 0.90.10 U25 4-Chlorotoluene
ug/L1.0 25.0 1775-127105 0.90.066 U26 4-Isopropyltoluene
ug/L1.0 25.0 1781-134110 20.050 U27 Benzene
ug/L1.0 25.0 1772-11599 20.13 U25 Bromobenzene
ug/L1.0 25.0 1874-128110 0.070.11 U27 Bromochloromethane
ug/L1.0 25.0 1672-129107 0.50.10 U27 Bromodichloromethane
ug/L1.0 25.0 4473-11996 20.20 U24 Bromoform
ug/L1.0 20.0 2738-189110 0.30.28 U22 Bromomethane
ug/L1.0 25.0 1768-142106 40.082 U27 Carbon Tetrachloride
ug/L1.0 25.0 1683-117112 10.069 U28 Chlorobenzene
ug/L1.0 20.0 2645-21391 00.18 U18 Chloroethane
ug/L1.0 25.0 1778-138113 0.50.083 U28 Chloroform
ug/L1.0 20.0 2856-171104 30.050 U21 Chloromethane
Page 30 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 7L05018 - EPA 5030B_MS - Continued
Prepared: 12/05/2017 00:34 Analyzed: 12/05/2017 11:41Matrix Spike Dup (7L05018-MSD1) Continued
Source: CA18761-03
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 25.0 1869-120103 10.075 U26 cis-1,2-Dichloroethene
ug/L1.0 25.0 1763-125100 20.073 U25 cis-1,3-Dichloropropene
ug/L1.0 25.0 1673-117103 20.067 U26 Dibromochloromethane
ug/L1.0 25.0 1576-124102 0.30.13 U26 Dibromomethane
ug/L1.0 20.0 4825-16187 50.091 U17 Dichlorodifluoromethane
ug/L1.0 25.0 1668-124104 0.60.10 U26 Ethylbenzene
ug/L1.0 50.0 250-200110 30.35 U55 Freon 113
ug/L1.0 25.0 1963-114109 10.15 U27 Hexachlorobutadiene
ug/L1.0 25.0 3070-13097 0.080.21 U24 Isopropyl Ether
ug/L1.0 25.0 1681-136110 0.80.13 U27 Isopropylbenzene
ug/L2.0 50.0 1679-121110 0.30.18 U55 m,p-Xylenes
ug/L2.0 25.0 1768-128106 20.070 U26 Methylene Chloride
ug/L1.0 25.0 2110-12795 40.12 U24 Methyl-tert-Butyl Ether
ug/L1.0 25.0 1950-12790 50.086 U22 Naphthalene
ug/L1.0 25.0 1568-126114 10.074 U29 n-Butyl Benzene
ug/L1.0 25.0 1676-125107 0.70.073 U27 n-Propyl Benzene
ug/L1.0 25.0 1571-125101 0.10.088 U25 o-Xylene
ug/L1.0 25.0 1775-122106 20.053 U27 sec-Butylbenzene
ug/L1.0 25.0 2373-120104 0.20.082 U26 Styrene
ug/L1.0 25.0 2270-137102 20.094 U25 tert-Butylbenzene
ug/L1.0 25.0 2640-181106 0.70.099 U26 Tetrachloroethene
ug/L1.0 25.0 1771-118109 0.30.053 U27 Toluene
ug/L1.0 25.0 1975-139102 0.40.11 U25 trans-1,2-Dichloroethene
ug/L1.0 25.0 1662-152107 20.080 U27 trans-1,3-Dichloropropene
ug/L1.0 25.0 1875-115103 20.13 U26 Trichloroethene
ug/L1.0 20.0 2268-18399 30.15 U20 Trichlorofluoromethane
ug/L1.0 20.0 2749-15095 20.083 U19 Vinyl chloride
ug/L1.0 75.0 1677-121107 0.10.22 U80 Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 8744
ug/L 50.0 70-130Dibromofluoromethane8944
ug/L 50.0 70-130Toluene-d8 9146
Batch 7L06037 - EPA 5030B_MS
Prepared: 12/06/2017 15:36 Analyzed: 12/07/2017 01:20Blank (7L06037-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.00.091 U 1,1,1,2-Tetrachloroethane
ug/L1.00.15 U 1,1,1-Trichloroethane
ug/L1.00.085 U 1,1,2,2-Tetrachloroethane
ug/L1.00.068 U 1,1,2-Trichloroethane
ug/L1.00.050 U 1,1-Dichloroethane
ug/L1.00.15 U 1,1-Dichloroethene
ug/L1.00.063 U 1,1-Dichloropropene
ug/L1.00.25 U 1,2,3-Trichlorobenzene
ug/L1.00.15 U 1,2,3-Trichloropropane
ug/L1.00.097 U 1,2,4-Trichlorobenzene
ug/L1.00.067 U 1,2,4-Trimethylbenzene
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
Page 31 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 7L06037 - EPA 5030B_MS - Continued
Prepared: 12/06/2017 15:36 Analyzed: 12/07/2017 01:20Blank (7L06037-BLK1) Continued
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.00.42 U 1,2-Dibromoethane
ug/L1.00.052 U 1,2-Dichlorobenzene
ug/L1.00.082 U 1,2-Dichloroethane
ug/L1.00.098 U 1,2-Dichloropropane
ug/L1.00.10 U 1,3,5-Trimethylbenzene
ug/L1.00.092 U 1,3-Dichlorobenzene
ug/L1.00.15 U 1,3-Dichloropropane
ug/L1.00.10 U 1,4-Dichlorobenzene
ug/L1.00.12 U 2,2-Dichloropropane
ug/L1.00.10 U 2-Chlorotoluene
ug/L1.00.10 U 4-Chlorotoluene
ug/L1.00.066 U 4-Isopropyltoluene
ug/L1.00.050 U Benzene
ug/L1.00.13 U Bromobenzene
ug/L1.00.11 U Bromochloromethane
ug/L1.00.10 U Bromodichloromethane
ug/L1.00.20 U Bromoform
ug/L1.00.28 U Bromomethane
ug/L1.00.082 U Carbon Tetrachloride
ug/L1.00.069 U Chlorobenzene
ug/L1.00.18 U Chloroethane
ug/L1.00.083 U Chloroform
ug/L1.00.050 U Chloromethane
ug/L1.00.075 U cis-1,2-Dichloroethene
ug/L1.00.073 U cis-1,3-Dichloropropene
ug/L1.00.067 U Dibromochloromethane
ug/L1.00.13 U Dibromomethane
ug/L1.00.091 U Dichlorodifluoromethane
ug/L1.00.10 U Ethylbenzene
ug/L1.00.35 U Freon 113
ug/L1.00.15 U Hexachlorobutadiene
ug/L1.00.21 U Isopropyl Ether
ug/L1.00.13 U Isopropylbenzene
ug/L2.00.18 U m,p-Xylenes
ug/L2.00.070 U Methylene Chloride
ug/L1.00.12 U Methyl-tert-Butyl Ether
ug/L1.00.086 U Naphthalene
ug/L1.00.074 U n-Butyl Benzene
ug/L1.00.073 U n-Propyl Benzene
ug/L1.00.088 U o-Xylene
ug/L1.00.053 U sec-Butylbenzene
ug/L1.00.082 U Styrene
ug/L1.00.094 U tert-Butylbenzene
ug/L1.00.099 U Tetrachloroethene
ug/L1.00.053 U Toluene
ug/L1.00.11 U trans-1,2-Dichloroethene
ug/L1.00.080 U trans-1,3-Dichloropropene
ug/L1.00.13 U Trichloroethene
ug/L1.00.15 U Trichlorofluoromethane
Page 32 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 7L06037 - EPA 5030B_MS - Continued
Prepared: 12/06/2017 15:36 Analyzed: 12/07/2017 01:20Blank (7L06037-BLK1) Continued
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.00.083 U Vinyl chloride
ug/L1.00.22 U Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 8141
ug/L 50.0 70-130Dibromofluoromethane9548
ug/L 50.0 70-130Toluene-d8 9145
Prepared: 12/06/2017 15:36 Analyzed: 12/06/2017 23:20LCS (7L06037-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 70-1309719 1,1,1,2-Tetrachloroethane
ug/L1.0 20.0 70-13010521 1,1,1-Trichloroethane
ug/L1.0 20.0 70-13010120 1,1,2,2-Tetrachloroethane
ug/L1.0 20.0 70-1309619 1,1,2-Trichloroethane
ug/L1.0 20.0 70-13011022 1,1-Dichloroethane
ug/L1.0 20.0 70-13010020 1,1-Dichloroethene
ug/L1.0 20.0 70-13010421 1,1-Dichloropropene
ug/L1.0 20.0 70-13010421 1,2,3-Trichlorobenzene
ug/L1.0 20.0 70-1309519 1,2,3-Trichloropropane
ug/L1.0 20.0 70-1309319 1,2,4-Trichlorobenzene
ug/L1.0 20.0 70-1309920 1,2,4-Trimethylbenzene
ug/L1.0 20.0 70-1309319 1,2-Dibromo-3-chloropropane
ug/L1.0 20.0 70-1309319 1,2-Dibromoethane
ug/L1.0 20.0 70-1309820 1,2-Dichlorobenzene
ug/L1.0 20.0 70-1309619 1,2-Dichloroethane
ug/L1.0 20.0 70-13010421 1,2-Dichloropropane
ug/L1.0 20.0 70-1309920 1,3,5-Trimethylbenzene
ug/L1.0 20.0 70-1309920 1,3-Dichlorobenzene
ug/L1.0 20.0 70-1309018 1,3-Dichloropropane
ug/L1.0 20.0 70-13010020 1,4-Dichlorobenzene
ug/L1.0 20.0 70-1309419 2,2-Dichloropropane
ug/L1.0 20.0 70-13010220 2-Chlorotoluene
ug/L1.0 20.0 70-1309820 4-Chlorotoluene
ug/L1.0 20.0 70-1309820 4-Isopropyltoluene
ug/L1.0 20.0 70-13010922 Benzene
ug/L1.0 20.0 70-1309218 Bromobenzene
ug/L1.0 20.0 70-13011022 Bromochloromethane
ug/L1.0 20.0 70-13010822 Bromodichloromethane
ug/L1.0 20.0 70-1309519 Bromoform
ug/L1.0 20.0 60-14011623 Bromomethane
ug/L1.0 20.0 70-13010120 Carbon Tetrachloride
ug/L1.0 20.0 70-13010421 Chlorobenzene
ug/L1.0 20.0 60-14010220 Chloroethane
ug/L1.0 20.0 70-13011022 Chloroform
ug/L1.0 20.0 60-14011824 Chloromethane
ug/L1.0 20.0 70-13010120 cis-1,2-Dichloroethene
ug/L1.0 20.0 70-1309619 cis-1,3-Dichloropropene
ug/L1.0 20.0 70-1309920 Dibromochloromethane
ug/L1.0 20.0 70-13010220 Dibromomethane
ug/L1.0 20.0 60-14010321 Dichlorodifluoromethane
Page 33 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 7L06037 - EPA 5030B_MS - Continued
Prepared: 12/06/2017 15:36 Analyzed: 12/06/2017 23:20LCS (7L06037-BS1) Continued
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 70-1309719 Ethylbenzene
ug/L1.0 20.0 70-13010621 Freon 113
ug/L1.0 20.0 70-13010120 Hexachlorobutadiene
ug/L1.0 20.0 70-1309820 Isopropyl Ether
ug/L1.0 20.0 70-13010120 Isopropylbenzene
ug/L2.0 40.0 70-13010341 m,p-Xylenes
ug/L2.0 20.0 70-13011323 Methylene Chloride
ug/L1.0 20.0 70-1309218 Methyl-tert-Butyl Ether
ug/L1.0 20.0 70-1308317 Naphthalene
ug/L1.0 20.0 70-13010621 n-Butyl Benzene
ug/L1.0 20.0 70-13010020 n-Propyl Benzene
ug/L1.0 20.0 70-1309419 o-Xylene
ug/L1.0 20.0 70-13010220 sec-Butylbenzene
ug/L1.0 20.0 70-1309619 Styrene
ug/L1.0 20.0 70-1309820 tert-Butylbenzene
ug/L1.0 20.0 70-1309118 Tetrachloroethene
ug/L1.0 20.0 70-13010220 Toluene
ug/L1.0 20.0 70-13010120 trans-1,2-Dichloroethene
ug/L1.0 20.0 70-1309920 trans-1,3-Dichloropropene
ug/L1.0 20.0 70-1309920 Trichloroethene
ug/L1.0 20.0 60-14010421 Trichlorofluoromethane
ug/L1.0 20.0 60-14010220 Vinyl chloride
ug/L1.0 60.0 70-13010060 Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 8543
ug/L 50.0 70-130Dibromofluoromethane9346
ug/L 50.0 70-130Toluene-d8 9447
Prepared: 12/06/2017 15:36 Analyzed: 12/06/2017 23:50Matrix Spike (7L06037-MS1)
Source: CA18761-06
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 71-1171020.091 U20 1,1,1,2-Tetrachloroethane
ug/L1.0 20.0 72-1431080.15 U22 1,1,1-Trichloroethane
ug/L1.0 20.0 59-1331040.085 U21 1,1,2,2-Tetrachloroethane
ug/L1.0 20.0 67-118970.068 U19 1,1,2-Trichloroethane
ug/L1.0 20.0 79-1411130.050 U23 1,1-Dichloroethane
ug/L1.0 20.0 75-1331000.15 U20 1,1-Dichloroethene
ug/L1.0 20.0 70-1291070.063 U21 1,1-Dichloropropene
ug/L1.0 20.0 62-1171000.25 U20 1,2,3-Trichlorobenzene
ug/L1.0 20.0 58-140970.15 U19 1,2,3-Trichloropropane
ug/L1.0 20.0 59-122920.097 U18 1,2,4-Trichlorobenzene
ug/L1.0 20.0 74-1231010.067 U20 1,2,4-Trimethylbenzene
ug/L1.0 20.0 37-157920.48 U18 1,2-Dibromo-3-chloropropane
ug/L1.0 20.0 66-123960.42 U19 1,2-Dibromoethane
ug/L1.0 20.0 76-116970.052 U19 1,2-Dichlorobenzene
ug/L1.0 20.0 72-151990.082 U20 1,2-Dichloroethane
ug/L1.0 20.0 78-1251080.098 U22 1,2-Dichloropropane
ug/L1.0 20.0 77-1291000.10 U20 1,3,5-Trimethylbenzene
ug/L1.0 20.0 76-1191010.092 U20 1,3-Dichlorobenzene
ug/L1.0 20.0 60-129920.15 U18 1,3-Dichloropropane
Page 34 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 7L06037 - EPA 5030B_MS - Continued
Prepared: 12/06/2017 15:36 Analyzed: 12/06/2017 23:50Matrix Spike (7L06037-MS1) Continued
Source: CA18761-06
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 76-1221020.10 U20 1,4-Dichlorobenzene
ug/L1.0 20.0 21-167970.12 U19 2,2-Dichloropropane
ug/L1.0 20.0 73-1351050.10 U21 2-Chlorotoluene
ug/L1.0 20.0 76-1341010.10 U20 4-Chlorotoluene
ug/L1.0 20.0 75-127990.066 U20 4-Isopropyltoluene
ug/L1.0 20.0 81-1341130.050 U23 Benzene
ug/L1.0 20.0 72-115920.13 U18 Bromobenzene
ug/L1.0 20.0 74-1281120.11 U22 Bromochloromethane
ug/L1.0 20.0 72-1291090.10 U22 Bromodichloromethane
ug/L1.0 20.0 73-119960.20 U19 Bromoform
ug/L1.0 20.0 38-1891200.28 U24 Bromomethane
ug/L1.0 20.0 68-1421050.082 U21 Carbon Tetrachloride
ug/L1.0 20.0 83-1171080.069 U22 Chlorobenzene
ug/L1.0 20.0 45-2131100.18 U22 Chloroethane
ug/L1.0 20.0 78-1381130.083 U23 Chloroform
ug/L1.0 20.0 56-1711270.050 U25 Chloromethane
ug/L1.0 20.0 69-1201030.075 U21 cis-1,2-Dichloroethene
ug/L1.0 20.0 63-1251000.073 U20 cis-1,3-Dichloropropene
ug/L1.0 20.0 73-1171010.067 U20 Dibromochloromethane
ug/L1.0 20.0 76-1241070.13 U21 Dibromomethane
ug/L1.0 20.0 25-1611060.091 U21 Dichlorodifluoromethane
ug/L1.0 20.0 68-124990.10 U20 Ethylbenzene
ug/L1.0 20.0 0-2001040.35 U21 Freon 113
ug/L1.0 20.0 63-114940.15 U19 Hexachlorobutadiene
ug/L1.0 20.0 70-130990.21 U20 Isopropyl Ether
ug/L1.0 20.0 81-1361030.13 U21 Isopropylbenzene
ug/L2.0 40.0 79-1211040.18 U42 m,p-Xylenes
ug/L2.0 20.0 68-1281180.070 U24 Methylene Chloride
ug/L1.0 20.0 10-127950.12 U19 Methyl-tert-Butyl Ether
ug/L1.0 20.0 50-127820.086 U16 Naphthalene
ug/L1.0 20.0 68-1261070.074 U21 n-Butyl Benzene
ug/L1.0 20.0 76-1251010.073 U20 n-Propyl Benzene
ug/L1.0 20.0 71-125960.088 U19 o-Xylene
ug/L1.0 20.0 75-1221040.053 U21 sec-Butylbenzene
ug/L1.0 20.0 73-120980.082 U20 Styrene
ug/L1.0 20.0 70-137990.094 U20 tert-Butylbenzene
ug/L1.0 20.0 40-181940.099 U19 Tetrachloroethene
ug/L1.0 20.0 71-1181050.053 U21 Toluene
ug/L1.0 20.0 75-1391050.11 U21 trans-1,2-Dichloroethene
ug/L1.0 20.0 62-1521000.080 U20 trans-1,3-Dichloropropene
ug/L1.0 20.0 75-1151020.13 U20 Trichloroethene
ug/L1.0 20.0 68-1831090.15 U22 Trichlorofluoromethane
ug/L1.0 20.0 49-1501100.083 U22 Vinyl chloride
ug/L1.0 60.0 77-1211020.22 U61 Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 8643
ug/L 50.0 70-130Dibromofluoromethane9145
ug/L 50.0 70-130Toluene-d8 9648
Page 35 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 7L06037 - EPA 5030B_MS - Continued
Prepared: 12/06/2017 15:36 Analyzed: 12/07/2017 00:20Matrix Spike Dup (7L06037-MSD1)
Source: CA18761-06
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 1671-11798 40.091 U20 1,1,1,2-Tetrachloroethane
ug/L1.0 20.0 1872-143102 50.15 U20 1,1,1-Trichloroethane
ug/L1.0 20.0 1659-133100 30.085 U20 1,1,2,2-Tetrachloroethane
ug/L1.0 20.0 1867-11895 30.068 U19 1,1,2-Trichloroethane
ug/L1.0 20.0 1979-141109 40.050 U22 1,1-Dichloroethane
ug/L1.0 20.0 2075-13396 40.15 U19 1,1-Dichloroethene
ug/L1.0 20.0 1770-129102 40.063 U20 1,1-Dichloropropene
ug/L1.0 20.0 1762-11797 30.25 U19 1,2,3-Trichlorobenzene
ug/L1.0 20.0 1758-14094 30.15 U19 1,2,3-Trichloropropane
ug/L1.0 20.0 1759-12287 50.097 U17 1,2,4-Trichlorobenzene
ug/L1.0 20.0 1874-12396 40.067 U19 1,2,4-Trimethylbenzene
ug/L1.0 20.0 1837-15790 30.48 U18 1,2-Dibromo-3-chloropropane
ug/L1.0 20.0 1566-12395 10.42 U19 1,2-Dibromoethane
ug/L1.0 20.0 1676-11696 10.052 U19 1,2-Dichlorobenzene
ug/L1.0 20.0 1672-15192 70.082 U18 1,2-Dichloroethane
ug/L1.0 20.0 1978-125102 60.098 U20 1,2-Dichloropropane
ug/L1.0 20.0 1677-12995 60.10 U19 1,3,5-Trimethylbenzene
ug/L1.0 20.0 1776-11995 60.092 U19 1,3-Dichlorobenzene
ug/L1.0 20.0 1660-12989 30.15 U18 1,3-Dichloropropane
ug/L1.0 20.0 1676-12297 50.10 U19 1,4-Dichlorobenzene
ug/L1.0 20.0 2021-16792 50.12 U18 2,2-Dichloropropane
ug/L1.0 20.0 1673-13598 60.10 U20 2-Chlorotoluene
ug/L1.0 20.0 1676-13496 60.10 U19 4-Chlorotoluene
ug/L1.0 20.0 1775-12795 40.066 U19 4-Isopropyltoluene
ug/L1.0 20.0 1781-134108 50.050 U22 Benzene
ug/L1.0 20.0 1772-11589 30.13 U18 Bromobenzene
ug/L1.0 20.0 1874-128107 50.11 U21 Bromochloromethane
ug/L1.0 20.0 1672-129106 30.10 U21 Bromodichloromethane
ug/L1.0 20.0 4473-11992 40.20 U18 Bromoform
ug/L1.0 20.0 2738-189114 60.28 U23 Bromomethane
ug/L1.0 20.0 1768-14298 60.082 U20 Carbon Tetrachloride
ug/L1.0 20.0 1683-117101 60.069 U20 Chlorobenzene
ug/L1.0 20.0 2645-213102 70.18 U20 Chloroethane
ug/L1.0 20.0 1778-138109 40.083 U22 Chloroform
ug/L1.0 20.0 2856-171115 100.050 U23 Chloromethane
ug/L1.0 20.0 1869-120103 0.10.075 U21 cis-1,2-Dichloroethene
ug/L1.0 20.0 1763-12594 60.073 U19 cis-1,3-Dichloropropene
ug/L1.0 20.0 1673-117100 0.80.067 U20 Dibromochloromethane
ug/L1.0 20.0 1576-124101 60.13 U20 Dibromomethane
ug/L1.0 20.0 4825-16199 70.091 U20 Dichlorodifluoromethane
ug/L1.0 20.0 1668-12494 50.10 U19 Ethylbenzene
ug/L1.0 20.0 250-20099 60.35 U20 Freon 113
ug/L1.0 20.0 1963-11491 30.15 U18 Hexachlorobutadiene
ug/L1.0 20.0 3070-13097 20.21 U19 Isopropyl Ether
ug/L1.0 20.0 1681-13698 60.13 U20 Isopropylbenzene
ug/L2.0 40.0 1679-121100 40.18 U40 m,p-Xylenes
ug/L2.0 20.0 1768-128113 40.070 U23 Methylene Chloride
ug/L1.0 20.0 2110-12793 10.12 U19 Methyl-tert-Butyl Ether
ug/L1.0 20.0 1950-12778 40.086 U16 Naphthalene
Page 36 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 7L06037 - EPA 5030B_MS - Continued
Prepared: 12/06/2017 15:36 Analyzed: 12/07/2017 00:20Matrix Spike Dup (7L06037-MSD1) Continued
Source: CA18761-06
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 1568-126101 50.074 U20 n-Butyl Benzene
ug/L1.0 20.0 1676-12597 40.073 U19 n-Propyl Benzene
ug/L1.0 20.0 1571-12592 50.088 U18 o-Xylene
ug/L1.0 20.0 1775-12298 60.053 U20 sec-Butylbenzene
ug/L1.0 20.0 2373-12095 30.082 U19 Styrene
ug/L1.0 20.0 2270-13794 50.094 U19 tert-Butylbenzene
ug/L1.0 20.0 2640-18191 30.099 U18 Tetrachloroethene
ug/L1.0 20.0 1771-118102 30.053 U20 Toluene
ug/L1.0 20.0 1975-139100 50.11 U20 trans-1,2-Dichloroethene
ug/L1.0 20.0 1662-15295 50.080 U19 trans-1,3-Dichloropropene
ug/L1.0 20.0 1875-11595 70.13 U19 Trichloroethene
ug/L1.0 20.0 2268-183103 60.15 U21 Trichlorofluoromethane
ug/L1.0 20.0 2749-150104 60.083 U21 Vinyl chloride
ug/L1.0 60.0 1677-12197 50.22 U58 Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 8543
ug/L 50.0 70-130Dibromofluoromethane9246
ug/L 50.0 70-130Toluene-d8 9447
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FLAGS/NOTES AND DEFINITIONS
The sample was analyzed at dilution.
The analyte was detected in the associated method blank.
The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
MRL
E
U
J
D
B
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
PQL: Practical Quantitation Limit.PQL
Page 38 of 39This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL