RA-2651_16593_CA_MRP_20180222_2017-2

102-A Woodwinds Industrial Court
Cary NC, 27511
919.467.3090 919.467.3515Phone:FAX:
ENCO Workorder(s): CA19202
Durham, NC 27703
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative. This report shall not be reproduced except in full, without
the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Enclosure(s)
Project Number: 7193, Project Name/Desc: Kuik Stop
Attn: Justin Abreu
EMS Environmental (EM001)
117 South Hoover Road
Chuck Smith
Project Manager
Tuesday, January 16, 2018
RE: Laboratory Results for
Dear Justin Abreu,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, January 9, 2018.
Enclosure(s)
Page 1 of 27This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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SAMPLE SUMMARY/LABORATORY CHRONICLE
MW-2 CA19202-01 Sampled:01/09/18 12:36 Received:01/09/18 15:41Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 300.0 02/06/18 01/11/18 14:37 01/11/18 17:07
EPA 6010D 01/12/18 01/10/18 09:12 01/15/18 13:1107/09/18
EPA 6010D 07/08/18 01/10/18 08:20 01/15/18 11:38
SM 6200B-1997 01/23/18 01/10/18 10:02 01/10/18 17:55
MW-3 CA19202-02 Sampled:01/09/18 11:57 Received:01/09/18 15:41Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 01/12/18 01/10/18 09:12 01/15/18 13:2407/09/18
EPA 6010D 07/08/18 01/10/18 08:20 01/15/18 11:40
SM 6200B-1997 01/23/18 01/10/18 10:02 01/10/18 18:26
MW-8 CA19202-03 Sampled:01/09/18 12:08 Received:01/09/18 15:41Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 300.0 02/06/18 01/11/18 14:37 01/11/18 17:21
EPA 6010D 01/12/18 01/10/18 09:12 01/15/18 13:2607/09/18
SM 6200B-1997 01/23/18 01/10/18 10:02 01/10/18 18:56
MW-8 CA19202-03RE1 Sampled:01/09/18 12:08 Received:01/09/18 15:41Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 07/08/18 01/10/18 08:20 01/15/18 12:20
MW-12 CA19202-04 Sampled:01/09/18 12:29 Received:01/09/18 15:41Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 01/12/18 01/10/18 09:12 01/15/18 13:2907/09/18
SM 6200B-1997 01/23/18 01/10/18 10:02 01/10/18 19:26
MW-12 CA19202-04RE1 Sampled:01/09/18 12:29 Received:01/09/18 15:41Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 300.0 02/06/18 01/11/18 14:37 01/12/18 10:15
EPA 6010D 07/08/18 01/10/18 08:20 01/15/18 12:22
MW-13 CA19202-05 Sampled:01/09/18 12:15 Received:01/09/18 15:41Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 300.0 02/06/18 01/11/18 14:37 01/11/18 17:50
EPA 6010D 01/12/18 01/10/18 09:12 01/15/18 13:3207/09/18
EPA 6010D 07/08/18 01/10/18 08:20 01/15/18 11:47
SM 6200B-1997 01/23/18 01/10/18 10:02 01/10/18 19:57
Brown SW CA19202-06 Sampled:01/09/18 12:49 Received:01/09/18 15:41Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 01/12/18 01/10/18 09:12 01/15/18 13:3507/09/18
SM 6200B-1997 01/23/18 01/10/18 10:02 01/10/18 20:27
Trip Blank CA19202-07 Sampled:01/09/18 11:57 Received:01/09/18 15:41Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
SM 6200B-1997 01/23/18 01/10/18 10:02 01/10/18 20:57
Page 2 of 27This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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SAMPLE DETECTION SUMMARY
Lab ID:Client ID:MW-2 CA19202-01
Analyte MethodUnitsPQLResultsFlag NotesMDL
15400 50.0 ug/L EPA 6010D Iron - Total 22.0
23.0 10.0 ug/L EPA 6010D Lead - Total 3.10
24 5.0 mg/L EPA 300.0 Sulfate as SO4 2.9
Lab ID:Client ID:MW-3 CA19202-02
Analyte MethodUnitsPQLResultsFlag NotesMDL
740 10 ug/L SM 6200B-1997D 1,2,4-Trimethylbenzene 0.67
360 10 ug/L SM 6200B-1997D 1,3,5-Trimethylbenzene 1.0
8.1 10 ug/L SM 6200B-1997JD 4-Isopropyltoluene 0.66
46 10 ug/L SM 6200B-1997D Benzene 0.50
340 10 ug/L SM 6200B-1997D Ethylbenzene 1.0
13100 50.0 ug/L EPA 6010D Iron - Total 22.0
19 10 ug/L SM 6200B-1997D Isopropyl Ether 2.1
41 10 ug/L SM 6200B-1997D Isopropylbenzene 1.3
18.3 10.0 ug/L EPA 6010D Lead - Total 3.10
880 20 ug/L SM 6200B-1997D m,p-Xylenes 1.8
45 10 ug/L SM 6200B-1997D Methyl-tert-Butyl Ether 1.2
230 10 ug/L SM 6200B-1997D Naphthalene 0.86
55 10 ug/L SM 6200B-1997D n-Butyl Benzene 0.74
110 10 ug/L SM 6200B-1997D n-Propyl Benzene 0.73
140 10 ug/L SM 6200B-1997D o-Xylene 0.88
1000 10 ug/L SM 6200B-1997D Xylenes (Total)2.2
Lab ID:Client ID:MW-8 CA19202-03
Analyte MethodUnitsPQLResultsFlag NotesMDL
174 10.0 ug/L EPA 6010D Lead - Total 3.10
12 1.0 ug/L SM 6200B-1997 Methyl-tert-Butyl Ether 0.12
3.5 5.0 mg/L EPA 300.0J Sulfate as SO4 2.9
Lab ID:Client ID:MW-8 CA19202-03RE1
Analyte MethodUnitsPQLResultsFlag NotesMDL
327000 250 ug/L EPA 6010DD Iron - Total 110
Lab ID:Client ID:MW-12 CA19202-04
Analyte MethodUnitsPQLResultsFlag NotesMDL
10 1.0 ug/L SM 6200B-1997 1,2,4-Trimethylbenzene 0.067
1.8 1.0 ug/L SM 6200B-1997 1,3,5-Trimethylbenzene 0.10
0.91 1.0 ug/L SM 6200B-1997J 4-Isopropyltoluene 0.066
0.51 1.0 ug/L SM 6200B-1997J Benzene 0.050
5.1 1.0 ug/L SM 6200B-1997 Ethylbenzene 0.10
4.5 1.0 ug/L SM 6200B-1997 Isopropylbenzene 0.13
397 10.0 ug/L EPA 6010D Lead - Total 3.10
1.3 1.0 ug/L SM 6200B-1997 Naphthalene 0.086
2.9 1.0 ug/L SM 6200B-1997 n-Butyl Benzene 0.074
10 1.0 ug/L SM 6200B-1997 n-Propyl Benzene 0.073
1.6 1.0 ug/L SM 6200B-1997 sec-Butylbenzene 0.053
Lab ID:Client ID:MW-12 CA19202-04RE1
Analyte MethodUnitsPQLResultsFlag NotesMDL
396000 250 ug/L EPA 6010DD Iron - Total 110
37 10 mg/L EPA 300.0D R-01Sulfate as SO4 5.8
Lab ID:Client ID:MW-13 CA19202-05
Analyte MethodUnitsPQLResultsFlag NotesMDL
6960 50.0 ug/L EPA 6010D Iron - Total 22.0
64 10 ug/L SM 6200B-1997D Isopropyl Ether 2.1
3.21 10.0 ug/L EPA 6010DJ Lead - Total 3.10
1000 10 ug/L SM 6200B-1997D Methyl-tert-Butyl Ether 1.2
4.7 5.0 mg/L EPA 300.0J Sulfate as SO4 2.9
Page 3 of 27This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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ANALYTICAL RESULTS
MW-2Description:Lab Sample ID:CA19202-01 01/09/18 15:41Received:
CA19202Work Order:01/09/18 12:36Sampled:Ground WaterMatrix:
Justin AbreuSampled By:Project:Kuik Stop
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 01/10/18 17:551,1,1,2-Tetrachloroethane [630-20-6]^0.091 MRK8A100111.00.091 U 1
ug/L SM 6200B-1997 01/10/18 17:551,1,1-Trichloroethane [71-55-6]^0.15 MRK8A100111.00.15 U 1
ug/L SM 6200B-1997 01/10/18 17:551,1,2,2-Tetrachloroethane [79-34-5]^0.085 MRK8A100111.00.085 U 1
ug/L SM 6200B-1997 01/10/18 17:551,1,2-Trichloroethane [79-00-5]^0.068 MRK8A100111.00.068 U 1
ug/L SM 6200B-1997 01/10/18 17:551,1-Dichloroethane [75-34-3]^0.050 MRK8A100111.00.050 U 1
ug/L SM 6200B-1997 01/10/18 17:551,1-Dichloroethene [75-35-4]^0.15 MRK8A100111.00.15 U 1
ug/L SM 6200B-1997 01/10/18 17:551,1-Dichloropropene [563-58-6]^0.063 MRK8A100111.00.063 U 1
ug/L SM 6200B-1997 01/10/18 17:551,2,3-Trichlorobenzene [87-61-6]^0.25 MRK8A100111.00.25 U 1
ug/L SM 6200B-1997 01/10/18 17:551,2,3-Trichloropropane [96-18-4]^0.15 MRK8A100111.00.15 U 1
ug/L SM 6200B-1997 01/10/18 17:551,2,4-Trichlorobenzene [120-82-1]^0.097 MRK8A100111.00.097 U 1
ug/L SM 6200B-1997 01/10/18 17:551,2,4-Trimethylbenzene [95-63-6]^0.067 MRK8A100111.00.067 U 1
ug/L SM 6200B-1997 01/10/18 17:551,2-Dibromo-3-chloropropane [96-12-8]^0.48 MRK8A100111.00.48 U 1
ug/L SM 6200B-1997 01/10/18 17:551,2-Dibromoethane [106-93-4]^0.42 MRK8A100111.00.42 U 1
ug/L SM 6200B-1997 01/10/18 17:551,2-Dichlorobenzene [95-50-1]^0.052 MRK8A100111.00.052 U 1
ug/L SM 6200B-1997 01/10/18 17:551,2-Dichloroethane [107-06-2]^0.082 MRK8A100111.00.082 U 1
ug/L SM 6200B-1997 01/10/18 17:551,2-Dichloropropane [78-87-5]^0.098 MRK8A100111.00.098 U 1
ug/L SM 6200B-1997 01/10/18 17:551,3,5-Trimethylbenzene [108-67-8]^0.10 MRK8A100111.00.10 U 1
ug/L SM 6200B-1997 01/10/18 17:551,3-Dichlorobenzene [541-73-1]^0.092 MRK8A100111.00.092 U 1
ug/L SM 6200B-1997 01/10/18 17:551,3-Dichloropropane [142-28-9]^0.15 MRK8A100111.00.15 U 1
ug/L SM 6200B-1997 01/10/18 17:551,4-Dichlorobenzene [106-46-7]^0.10 MRK8A100111.00.10 U 1
ug/L SM 6200B-1997 01/10/18 17:552,2-Dichloropropane [594-20-7]^0.12 MRK8A100111.00.12 U 1
ug/L SM 6200B-1997 01/10/18 17:552-Chlorotoluene [95-49-8]^0.10 MRK8A100111.00.10 U 1
ug/L SM 6200B-1997 01/10/18 17:554-Chlorotoluene [106-43-4]^0.10 MRK8A100111.00.10 U 1
ug/L SM 6200B-1997 01/10/18 17:554-Isopropyltoluene [99-87-6]^0.066 MRK8A100111.00.066 U 1
ug/L SM 6200B-1997 01/10/18 17:55Benzene [71-43-2]^0.050 MRK8A100111.00.050 U 1
ug/L SM 6200B-1997 01/10/18 17:55Bromobenzene [108-86-1]^0.13 MRK8A100111.00.13 U 1
ug/L SM 6200B-1997 01/10/18 17:55Bromochloromethane [74-97-5]^0.11 MRK8A100111.00.11 U 1
ug/L SM 6200B-1997 01/10/18 17:55Bromodichloromethane [75-27-4]^0.10 MRK8A100111.00.10 U 1
ug/L SM 6200B-1997 01/10/18 17:55Bromoform [75-25-2]^0.20 MRK8A100111.00.20 U 1
ug/L SM 6200B-1997 01/10/18 17:55Bromomethane [74-83-9]^0.28 MRK8A100111.00.28 U 1
ug/L SM 6200B-1997 01/10/18 17:55Carbon Tetrachloride [56-23-5]^0.082 MRK8A100111.00.082 U 1
ug/L SM 6200B-1997 01/10/18 17:55Chlorobenzene [108-90-7]^0.069 MRK8A100111.00.069 U 1
ug/L SM 6200B-1997 01/10/18 17:55Chloroethane [75-00-3]^0.18 MRK8A100111.00.18 U 1
ug/L SM 6200B-1997 01/10/18 17:55Chloroform [67-66-3]^0.083 MRK8A100111.00.083 U 1
ug/L SM 6200B-1997 01/10/18 17:55Chloromethane [74-87-3]^0.050 MRK8A100111.00.050 U 1
ug/L SM 6200B-1997 01/10/18 17:55cis-1,2-Dichloroethene [156-59-2]^0.075 MRK8A100111.00.075 U 1
ug/L SM 6200B-1997 01/10/18 17:55cis-1,3-Dichloropropene [10061-01-5]^0.073 MRK8A100111.00.073 U 1
ug/L SM 6200B-1997 01/10/18 17:55Dibromochloromethane [124-48-1]^0.067 MRK8A100111.00.067 U 1
ug/L SM 6200B-1997 01/10/18 17:55Dibromomethane [74-95-3]^0.13 MRK8A100111.00.13 U 1
ug/L SM 6200B-1997 01/10/18 17:55Dichlorodifluoromethane [75-71-8]^0.091 MRK8A100111.00.091 U 1
ug/L SM 6200B-1997 01/10/18 17:55Ethylbenzene [100-41-4]^0.10 MRK8A100111.00.10 U 1
ug/L SM 6200B-1997 01/10/18 17:55Freon 113 [76-13-1]^0.35 MRK8A100111.00.35 U 1
ug/L SM 6200B-1997 01/10/18 17:55Hexachlorobutadiene [87-68-3]^0.15 MRK8A100111.00.15 U 1
ug/L SM 6200B-1997 01/10/18 17:55Isopropyl Ether [108-20-3]^0.21 MRK8A100111.00.21 U 1
ug/L SM 6200B-1997 01/10/18 17:55Isopropylbenzene [98-82-8]^0.13 MRK8A100111.00.13 U 1
ug/L SM 6200B-1997 01/10/18 17:55m,p-Xylenes [108-38-3/106-42-3]^0.18 MRK8A100112.00.18 U 1
ug/L SM 6200B-1997 01/10/18 17:55Methylene Chloride [75-09-2]^0.070 MRK8A100112.00.070 U 1
Page 4 of 27This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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ANALYTICAL RESULTS
MW-2Description:Lab Sample ID:CA19202-01 01/09/18 15:41Received:
CA19202Work Order:01/09/18 12:36Sampled:Ground WaterMatrix:
Justin AbreuSampled By:Project:Kuik Stop
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 01/10/18 17:55Methyl-tert-Butyl Ether [1634-04-4]^0.12 MRK8A100111.00.12 U 1
ug/L SM 6200B-1997 01/10/18 17:55Naphthalene [91-20-3]^0.086 MRK8A100111.00.086 U 1
ug/L SM 6200B-1997 01/10/18 17:55n-Butyl Benzene [104-51-8]^0.074 MRK8A100111.00.074 U 1
ug/L SM 6200B-1997 01/10/18 17:55n-Propyl Benzene [103-65-1]^0.073 MRK8A100111.00.073 U 1
ug/L SM 6200B-1997 01/10/18 17:55o-Xylene [95-47-6]^0.088 MRK8A100111.00.088 U 1
ug/L SM 6200B-1997 01/10/18 17:55sec-Butylbenzene [135-98-8]^0.053 MRK8A100111.00.053 U 1
ug/L SM 6200B-1997 01/10/18 17:55Styrene [100-42-5]^0.082 MRK8A100111.00.082 U 1
ug/L SM 6200B-1997 01/10/18 17:55tert-Butylbenzene [98-06-6]^0.094 MRK8A100111.00.094 U 1
ug/L SM 6200B-1997 01/10/18 17:55Tetrachloroethene [127-18-4]^0.099 MRK8A100111.00.099 U 1
ug/L SM 6200B-1997 01/10/18 17:55Toluene [108-88-3]^0.053 MRK8A100111.00.053 U 1
ug/L SM 6200B-1997 01/10/18 17:55trans-1,2-Dichloroethene [156-60-5]^0.11 MRK8A100111.00.11 U 1
ug/L SM 6200B-1997 01/10/18 17:55trans-1,3-Dichloropropene [10061-02-6]^0.080 MRK8A100111.00.080 U 1
ug/L SM 6200B-1997 01/10/18 17:55Trichloroethene [79-01-6]^0.13 MRK8A100111.00.13 U 1
ug/L SM 6200B-1997 01/10/18 17:55Trichlorofluoromethane [75-69-4]^0.15 MRK8A100111.00.15 U 1
ug/L SM 6200B-1997 01/10/18 17:55Vinyl chloride [75-01-4]^0.083 MRK8A100111.00.083 U 1
ug/L SM 6200B-1997 01/10/18 17:55Xylenes (Total) [1330-20-7]^0.22 MRK8A100111.00.22 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 70-130102 %MRKSM 6200B-1997 01/10/18 17:558A100115150.0 1
Dibromofluoromethane 70-130105 %MRKSM 6200B-1997 01/10/18 17:558A100115350.0 1
Toluene-d8 70-13099 %MRKSM 6200B-1997 01/10/18 17:558A100115050.0 1
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 6010D 01/15/18 11:38Iron [7439-89-6]^22.0 JDH8A1000450.015400 1
Metals (acid extractable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 6010D 01/15/18 13:11Lead [7439-92-1]^3.10 JDH8A1000710.023.0 1
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/L EPA 300.0 01/11/18 17:07Sulfate as SO4 [14808-79-8]^2.9 MKS8A110335.024 1
Page 5 of 27This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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ANALYTICAL RESULTS
MW-3Description:Lab Sample ID:CA19202-02 01/09/18 15:41Received:
CA19202Work Order:01/09/18 11:57Sampled:Ground WaterMatrix:
Justin AbreuSampled By:Project:Kuik Stop
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 01/10/18 18:261,1,1,2-Tetrachloroethane [630-20-6]^0.91 MRK8A10011100.91 UD 10
ug/L SM 6200B-1997 01/10/18 18:261,1,1-Trichloroethane [71-55-6]^1.5 MRK8A10011101.5 UD 10
ug/L SM 6200B-1997 01/10/18 18:261,1,2,2-Tetrachloroethane [79-34-5]^0.85 MRK8A10011100.85 UD 10
ug/L SM 6200B-1997 01/10/18 18:261,1,2-Trichloroethane [79-00-5]^0.68 MRK8A10011100.68 UD 10
ug/L SM 6200B-1997 01/10/18 18:261,1-Dichloroethane [75-34-3]^0.50 MRK8A10011100.50 UD 10
ug/L SM 6200B-1997 01/10/18 18:261,1-Dichloroethene [75-35-4]^1.5 MRK8A10011101.5 UD 10
ug/L SM 6200B-1997 01/10/18 18:261,1-Dichloropropene [563-58-6]^0.63 MRK8A10011100.63 UD 10
ug/L SM 6200B-1997 01/10/18 18:261,2,3-Trichlorobenzene [87-61-6]^2.5 MRK8A10011102.5 UD 10
ug/L SM 6200B-1997 01/10/18 18:261,2,3-Trichloropropane [96-18-4]^1.5 MRK8A10011101.5 UD 10
ug/L SM 6200B-1997 01/10/18 18:261,2,4-Trichlorobenzene [120-82-1]^0.97 MRK8A10011100.97 UD 10
ug/L SM 6200B-1997 01/10/18 18:261,2,4-Trimethylbenzene [95-63-6]^0.67 MRK8A1001110740D 10
ug/L SM 6200B-1997 01/10/18 18:261,2-Dibromo-3-chloropropane [96-12-8]^4.8 MRK8A10011104.8 UD 10
ug/L SM 6200B-1997 01/10/18 18:261,2-Dibromoethane [106-93-4]^4.2 MRK8A10011104.2 UD 10
ug/L SM 6200B-1997 01/10/18 18:261,2-Dichlorobenzene [95-50-1]^0.52 MRK8A10011100.52 UD 10
ug/L SM 6200B-1997 01/10/18 18:261,2-Dichloroethane [107-06-2]^0.82 MRK8A10011100.82 UD 10
ug/L SM 6200B-1997 01/10/18 18:261,2-Dichloropropane [78-87-5]^0.98 MRK8A10011100.98 UD 10
ug/L SM 6200B-1997 01/10/18 18:261,3,5-Trimethylbenzene [108-67-8]^1.0 MRK8A1001110360D 10
ug/L SM 6200B-1997 01/10/18 18:261,3-Dichlorobenzene [541-73-1]^0.92 MRK8A10011100.92 UD 10
ug/L SM 6200B-1997 01/10/18 18:261,3-Dichloropropane [142-28-9]^1.5 MRK8A10011101.5 UD 10
ug/L SM 6200B-1997 01/10/18 18:261,4-Dichlorobenzene [106-46-7]^1.0 MRK8A10011101.0 UD 10
ug/L SM 6200B-1997 01/10/18 18:262,2-Dichloropropane [594-20-7]^1.2 MRK8A10011101.2 UD 10
ug/L SM 6200B-1997 01/10/18 18:262-Chlorotoluene [95-49-8]^1.0 MRK8A10011101.0 UD 10
ug/L SM 6200B-1997 01/10/18 18:264-Chlorotoluene [106-43-4]^1.0 MRK8A10011101.0 UD 10
ug/L SM 6200B-1997 01/10/18 18:264-Isopropyltoluene [99-87-6]^0.66 MRK8A10011108.1 JD 10
ug/L SM 6200B-1997 01/10/18 18:26Benzene [71-43-2]^0.50 MRK8A100111046D 10
ug/L SM 6200B-1997 01/10/18 18:26Bromobenzene [108-86-1]^1.3 MRK8A10011101.3 UD 10
ug/L SM 6200B-1997 01/10/18 18:26Bromochloromethane [74-97-5]^1.1 MRK8A10011101.1 UD 10
ug/L SM 6200B-1997 01/10/18 18:26Bromodichloromethane [75-27-4]^1.0 MRK8A10011101.0 UD 10
ug/L SM 6200B-1997 01/10/18 18:26Bromoform [75-25-2]^2.0 MRK8A10011102.0 UD 10
ug/L SM 6200B-1997 01/10/18 18:26Bromomethane [74-83-9]^2.8 MRK8A10011102.8 UD 10
ug/L SM 6200B-1997 01/10/18 18:26Carbon Tetrachloride [56-23-5]^0.82 MRK8A10011100.82 UD 10
ug/L SM 6200B-1997 01/10/18 18:26Chlorobenzene [108-90-7]^0.69 MRK8A10011100.69 UD 10
ug/L SM 6200B-1997 01/10/18 18:26Chloroethane [75-00-3]^1.8 MRK8A10011101.8 UD 10
ug/L SM 6200B-1997 01/10/18 18:26Chloroform [67-66-3]^0.83 MRK8A10011100.83 UD 10
ug/L SM 6200B-1997 01/10/18 18:26Chloromethane [74-87-3]^0.50 MRK8A10011100.50 UD 10
ug/L SM 6200B-1997 01/10/18 18:26cis-1,2-Dichloroethene [156-59-2]^0.75 MRK8A10011100.75 UD 10
ug/L SM 6200B-1997 01/10/18 18:26cis-1,3-Dichloropropene [10061-01-5]^0.73 MRK8A10011100.73 UD 10
ug/L SM 6200B-1997 01/10/18 18:26Dibromochloromethane [124-48-1]^0.67 MRK8A10011100.67 UD 10
ug/L SM 6200B-1997 01/10/18 18:26Dibromomethane [74-95-3]^1.3 MRK8A10011101.3 UD 10
ug/L SM 6200B-1997 01/10/18 18:26Dichlorodifluoromethane [75-71-8]^0.91 MRK8A10011100.91 UD 10
ug/L SM 6200B-1997 01/10/18 18:26Ethylbenzene [100-41-4]^1.0 MRK8A1001110340D 10
ug/L SM 6200B-1997 01/10/18 18:26Freon 113 [76-13-1]^3.5 MRK8A10011103.5 UD 10
ug/L SM 6200B-1997 01/10/18 18:26Hexachlorobutadiene [87-68-3]^1.5 MRK8A10011101.5 UD 10
ug/L SM 6200B-1997 01/10/18 18:26Isopropyl Ether [108-20-3]^2.1 MRK8A100111019D 10
ug/L SM 6200B-1997 01/10/18 18:26Isopropylbenzene [98-82-8]^1.3 MRK8A100111041D 10
ug/L SM 6200B-1997 01/10/18 18:26m,p-Xylenes [108-38-3/106-42-3]^1.8 MRK8A1001120880D 10
ug/L SM 6200B-1997 01/10/18 18:26Methylene Chloride [75-09-2]^0.70 MRK8A10011200.70 UD 10
Page 6 of 27This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
MW-3Description:Lab Sample ID:CA19202-02 01/09/18 15:41Received:
CA19202Work Order:01/09/18 11:57Sampled:Ground WaterMatrix:
Justin AbreuSampled By:Project:Kuik Stop
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 01/10/18 18:26Methyl-tert-Butyl Ether [1634-04-4]^1.2 MRK8A100111045D 10
ug/L SM 6200B-1997 01/10/18 18:26Naphthalene [91-20-3]^0.86 MRK8A1001110230D 10
ug/L SM 6200B-1997 01/10/18 18:26n-Butyl Benzene [104-51-8]^0.74 MRK8A100111055D 10
ug/L SM 6200B-1997 01/10/18 18:26n-Propyl Benzene [103-65-1]^0.73 MRK8A1001110110D 10
ug/L SM 6200B-1997 01/10/18 18:26o-Xylene [95-47-6]^0.88 MRK8A1001110140D 10
ug/L SM 6200B-1997 01/10/18 18:26sec-Butylbenzene [135-98-8]^0.53 MRK8A10011100.53 UD 10
ug/L SM 6200B-1997 01/10/18 18:26Styrene [100-42-5]^0.82 MRK8A10011100.82 UD 10
ug/L SM 6200B-1997 01/10/18 18:26tert-Butylbenzene [98-06-6]^0.94 MRK8A10011100.94 UD 10
ug/L SM 6200B-1997 01/10/18 18:26Tetrachloroethene [127-18-4]^0.99 MRK8A10011100.99 UD 10
ug/L SM 6200B-1997 01/10/18 18:26Toluene [108-88-3]^0.53 MRK8A10011100.53 UD 10
ug/L SM 6200B-1997 01/10/18 18:26trans-1,2-Dichloroethene [156-60-5]^1.1 MRK8A10011101.1 UD 10
ug/L SM 6200B-1997 01/10/18 18:26trans-1,3-Dichloropropene [10061-02-6]^0.80 MRK8A10011100.80 UD 10
ug/L SM 6200B-1997 01/10/18 18:26Trichloroethene [79-01-6]^1.3 MRK8A10011101.3 UD 10
ug/L SM 6200B-1997 01/10/18 18:26Trichlorofluoromethane [75-69-4]^1.5 MRK8A10011101.5 UD 10
ug/L SM 6200B-1997 01/10/18 18:26Vinyl chloride [75-01-4]^0.83 MRK8A10011100.83 UD 10
ug/L SM 6200B-1997 01/10/18 18:26Xylenes (Total) [1330-20-7]^2.2 MRK8A10011101000D 10
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 70-130114 %MRKSM 6200B-1997 01/10/18 18:268A100115750.0 1
Dibromofluoromethane 70-130105 %MRKSM 6200B-1997 01/10/18 18:268A100115250.0 1
Toluene-d8 70-130100 %MRKSM 6200B-1997 01/10/18 18:268A100115050.0 1
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 6010D 01/15/18 11:40Iron [7439-89-6]^22.0 JDH8A1000450.013100 1
Metals (acid extractable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 6010D 01/15/18 13:24Lead [7439-92-1]^3.10 JDH8A1000710.018.3 1
Page 7 of 27This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
MW-8Description:Lab Sample ID:CA19202-03 01/09/18 15:41Received:
CA19202Work Order:01/09/18 12:08Sampled:Ground WaterMatrix:
Justin AbreuSampled By:Project:Kuik Stop
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 01/10/18 18:561,1,1,2-Tetrachloroethane [630-20-6]^0.091 MRK8A100111.00.091 U 1
ug/L SM 6200B-1997 01/10/18 18:561,1,1-Trichloroethane [71-55-6]^0.15 MRK8A100111.00.15 U 1
ug/L SM 6200B-1997 01/10/18 18:561,1,2,2-Tetrachloroethane [79-34-5]^0.085 MRK8A100111.00.085 U 1
ug/L SM 6200B-1997 01/10/18 18:561,1,2-Trichloroethane [79-00-5]^0.068 MRK8A100111.00.068 U 1
ug/L SM 6200B-1997 01/10/18 18:561,1-Dichloroethane [75-34-3]^0.050 MRK8A100111.00.050 U 1
ug/L SM 6200B-1997 01/10/18 18:561,1-Dichloroethene [75-35-4]^0.15 MRK8A100111.00.15 U 1
ug/L SM 6200B-1997 01/10/18 18:561,1-Dichloropropene [563-58-6]^0.063 MRK8A100111.00.063 U 1
ug/L SM 6200B-1997 01/10/18 18:561,2,3-Trichlorobenzene [87-61-6]^0.25 MRK8A100111.00.25 U 1
ug/L SM 6200B-1997 01/10/18 18:561,2,3-Trichloropropane [96-18-4]^0.15 MRK8A100111.00.15 U 1
ug/L SM 6200B-1997 01/10/18 18:561,2,4-Trichlorobenzene [120-82-1]^0.097 MRK8A100111.00.097 U 1
ug/L SM 6200B-1997 01/10/18 18:561,2,4-Trimethylbenzene [95-63-6]^0.067 MRK8A100111.00.067 U 1
ug/L SM 6200B-1997 01/10/18 18:561,2-Dibromo-3-chloropropane [96-12-8]^0.48 MRK8A100111.00.48 U 1
ug/L SM 6200B-1997 01/10/18 18:561,2-Dibromoethane [106-93-4]^0.42 MRK8A100111.00.42 U 1
ug/L SM 6200B-1997 01/10/18 18:561,2-Dichlorobenzene [95-50-1]^0.052 MRK8A100111.00.052 U 1
ug/L SM 6200B-1997 01/10/18 18:561,2-Dichloroethane [107-06-2]^0.082 MRK8A100111.00.082 U 1
ug/L SM 6200B-1997 01/10/18 18:561,2-Dichloropropane [78-87-5]^0.098 MRK8A100111.00.098 U 1
ug/L SM 6200B-1997 01/10/18 18:561,3,5-Trimethylbenzene [108-67-8]^0.10 MRK8A100111.00.10 U 1
ug/L SM 6200B-1997 01/10/18 18:561,3-Dichlorobenzene [541-73-1]^0.092 MRK8A100111.00.092 U 1
ug/L SM 6200B-1997 01/10/18 18:561,3-Dichloropropane [142-28-9]^0.15 MRK8A100111.00.15 U 1
ug/L SM 6200B-1997 01/10/18 18:561,4-Dichlorobenzene [106-46-7]^0.10 MRK8A100111.00.10 U 1
ug/L SM 6200B-1997 01/10/18 18:562,2-Dichloropropane [594-20-7]^0.12 MRK8A100111.00.12 U 1
ug/L SM 6200B-1997 01/10/18 18:562-Chlorotoluene [95-49-8]^0.10 MRK8A100111.00.10 U 1
ug/L SM 6200B-1997 01/10/18 18:564-Chlorotoluene [106-43-4]^0.10 MRK8A100111.00.10 U 1
ug/L SM 6200B-1997 01/10/18 18:564-Isopropyltoluene [99-87-6]^0.066 MRK8A100111.00.066 U 1
ug/L SM 6200B-1997 01/10/18 18:56Benzene [71-43-2]^0.050 MRK8A100111.00.050 U 1
ug/L SM 6200B-1997 01/10/18 18:56Bromobenzene [108-86-1]^0.13 MRK8A100111.00.13 U 1
ug/L SM 6200B-1997 01/10/18 18:56Bromochloromethane [74-97-5]^0.11 MRK8A100111.00.11 U 1
ug/L SM 6200B-1997 01/10/18 18:56Bromodichloromethane [75-27-4]^0.10 MRK8A100111.00.10 U 1
ug/L SM 6200B-1997 01/10/18 18:56Bromoform [75-25-2]^0.20 MRK8A100111.00.20 U 1
ug/L SM 6200B-1997 01/10/18 18:56Bromomethane [74-83-9]^0.28 MRK8A100111.00.28 U 1
ug/L SM 6200B-1997 01/10/18 18:56Carbon Tetrachloride [56-23-5]^0.082 MRK8A100111.00.082 U 1
ug/L SM 6200B-1997 01/10/18 18:56Chlorobenzene [108-90-7]^0.069 MRK8A100111.00.069 U 1
ug/L SM 6200B-1997 01/10/18 18:56Chloroethane [75-00-3]^0.18 MRK8A100111.00.18 U 1
ug/L SM 6200B-1997 01/10/18 18:56Chloroform [67-66-3]^0.083 MRK8A100111.00.083 U 1
ug/L SM 6200B-1997 01/10/18 18:56Chloromethane [74-87-3]^0.050 MRK8A100111.00.050 U 1
ug/L SM 6200B-1997 01/10/18 18:56cis-1,2-Dichloroethene [156-59-2]^0.075 MRK8A100111.00.075 U 1
ug/L SM 6200B-1997 01/10/18 18:56cis-1,3-Dichloropropene [10061-01-5]^0.073 MRK8A100111.00.073 U 1
ug/L SM 6200B-1997 01/10/18 18:56Dibromochloromethane [124-48-1]^0.067 MRK8A100111.00.067 U 1
ug/L SM 6200B-1997 01/10/18 18:56Dibromomethane [74-95-3]^0.13 MRK8A100111.00.13 U 1
ug/L SM 6200B-1997 01/10/18 18:56Dichlorodifluoromethane [75-71-8]^0.091 MRK8A100111.00.091 U 1
ug/L SM 6200B-1997 01/10/18 18:56Ethylbenzene [100-41-4]^0.10 MRK8A100111.00.10 U 1
ug/L SM 6200B-1997 01/10/18 18:56Freon 113 [76-13-1]^0.35 MRK8A100111.00.35 U 1
ug/L SM 6200B-1997 01/10/18 18:56Hexachlorobutadiene [87-68-3]^0.15 MRK8A100111.00.15 U 1
ug/L SM 6200B-1997 01/10/18 18:56Isopropyl Ether [108-20-3]^0.21 MRK8A100111.00.21 U 1
ug/L SM 6200B-1997 01/10/18 18:56Isopropylbenzene [98-82-8]^0.13 MRK8A100111.00.13 U 1
ug/L SM 6200B-1997 01/10/18 18:56m,p-Xylenes [108-38-3/106-42-3]^0.18 MRK8A100112.00.18 U 1
ug/L SM 6200B-1997 01/10/18 18:56Methylene Chloride [75-09-2]^0.070 MRK8A100112.00.070 U 1
Page 8 of 27This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
MW-8Description:Lab Sample ID:CA19202-03 01/09/18 15:41Received:
CA19202Work Order:01/09/18 12:08Sampled:Ground WaterMatrix:
Justin AbreuSampled By:Project:Kuik Stop
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 01/10/18 18:56Methyl-tert-Butyl Ether [1634-04-4]^0.12 MRK8A100111.012 1
ug/L SM 6200B-1997 01/10/18 18:56Naphthalene [91-20-3]^0.086 MRK8A100111.00.086 U 1
ug/L SM 6200B-1997 01/10/18 18:56n-Butyl Benzene [104-51-8]^0.074 MRK8A100111.00.074 U 1
ug/L SM 6200B-1997 01/10/18 18:56n-Propyl Benzene [103-65-1]^0.073 MRK8A100111.00.073 U 1
ug/L SM 6200B-1997 01/10/18 18:56o-Xylene [95-47-6]^0.088 MRK8A100111.00.088 U 1
ug/L SM 6200B-1997 01/10/18 18:56sec-Butylbenzene [135-98-8]^0.053 MRK8A100111.00.053 U 1
ug/L SM 6200B-1997 01/10/18 18:56Styrene [100-42-5]^0.082 MRK8A100111.00.082 U 1
ug/L SM 6200B-1997 01/10/18 18:56tert-Butylbenzene [98-06-6]^0.094 MRK8A100111.00.094 U 1
ug/L SM 6200B-1997 01/10/18 18:56Tetrachloroethene [127-18-4]^0.099 MRK8A100111.00.099 U 1
ug/L SM 6200B-1997 01/10/18 18:56Toluene [108-88-3]^0.053 MRK8A100111.00.053 U 1
ug/L SM 6200B-1997 01/10/18 18:56trans-1,2-Dichloroethene [156-60-5]^0.11 MRK8A100111.00.11 U 1
ug/L SM 6200B-1997 01/10/18 18:56trans-1,3-Dichloropropene [10061-02-6]^0.080 MRK8A100111.00.080 U 1
ug/L SM 6200B-1997 01/10/18 18:56Trichloroethene [79-01-6]^0.13 MRK8A100111.00.13 U 1
ug/L SM 6200B-1997 01/10/18 18:56Trichlorofluoromethane [75-69-4]^0.15 MRK8A100111.00.15 U 1
ug/L SM 6200B-1997 01/10/18 18:56Vinyl chloride [75-01-4]^0.083 MRK8A100111.00.083 U 1
ug/L SM 6200B-1997 01/10/18 18:56Xylenes (Total) [1330-20-7]^0.22 MRK8A100111.00.22 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 70-130103 %MRKSM 6200B-1997 01/10/18 18:568A100115150.0 1
Dibromofluoromethane 70-130104 %MRKSM 6200B-1997 01/10/18 18:568A100115250.0 1
Toluene-d8 70-13098 %MRKSM 6200B-1997 01/10/18 18:568A100114950.0 1
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 6010D 01/15/18 12:20Iron [7439-89-6]^110 JDH8A10004250327000D 5
Metals (acid extractable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 6010D 01/15/18 13:26Lead [7439-92-1]^3.10 JDH8A1000710.0174 1
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/L EPA 300.0 01/11/18 17:21Sulfate as SO4 [14808-79-8]^2.9 MKS8A110335.03.5 J 1
Page 9 of 27This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
MW-12Description:Lab Sample ID:CA19202-04 01/09/18 15:41Received:
CA19202Work Order:01/09/18 12:29Sampled:Ground WaterMatrix:
Justin AbreuSampled By:Project:Kuik Stop
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 01/10/18 19:261,1,1,2-Tetrachloroethane [630-20-6]^0.091 MRK8A100111.00.091 U 1
ug/L SM 6200B-1997 01/10/18 19:261,1,1-Trichloroethane [71-55-6]^0.15 MRK8A100111.00.15 U 1
ug/L SM 6200B-1997 01/10/18 19:261,1,2,2-Tetrachloroethane [79-34-5]^0.085 MRK8A100111.00.085 U 1
ug/L SM 6200B-1997 01/10/18 19:261,1,2-Trichloroethane [79-00-5]^0.068 MRK8A100111.00.068 U 1
ug/L SM 6200B-1997 01/10/18 19:261,1-Dichloroethane [75-34-3]^0.050 MRK8A100111.00.050 U 1
ug/L SM 6200B-1997 01/10/18 19:261,1-Dichloroethene [75-35-4]^0.15 MRK8A100111.00.15 U 1
ug/L SM 6200B-1997 01/10/18 19:261,1-Dichloropropene [563-58-6]^0.063 MRK8A100111.00.063 U 1
ug/L SM 6200B-1997 01/10/18 19:261,2,3-Trichlorobenzene [87-61-6]^0.25 MRK8A100111.00.25 U 1
ug/L SM 6200B-1997 01/10/18 19:261,2,3-Trichloropropane [96-18-4]^0.15 MRK8A100111.00.15 U 1
ug/L SM 6200B-1997 01/10/18 19:261,2,4-Trichlorobenzene [120-82-1]^0.097 MRK8A100111.00.097 U 1
ug/L SM 6200B-1997 01/10/18 19:261,2,4-Trimethylbenzene [95-63-6]^0.067 MRK8A100111.010 1
ug/L SM 6200B-1997 01/10/18 19:261,2-Dibromo-3-chloropropane [96-12-8]^0.48 MRK8A100111.00.48 U 1
ug/L SM 6200B-1997 01/10/18 19:261,2-Dibromoethane [106-93-4]^0.42 MRK8A100111.00.42 U 1
ug/L SM 6200B-1997 01/10/18 19:261,2-Dichlorobenzene [95-50-1]^0.052 MRK8A100111.00.052 U 1
ug/L SM 6200B-1997 01/10/18 19:261,2-Dichloroethane [107-06-2]^0.082 MRK8A100111.00.082 U 1
ug/L SM 6200B-1997 01/10/18 19:261,2-Dichloropropane [78-87-5]^0.098 MRK8A100111.00.098 U 1
ug/L SM 6200B-1997 01/10/18 19:261,3,5-Trimethylbenzene [108-67-8]^0.10 MRK8A100111.01.8 1
ug/L SM 6200B-1997 01/10/18 19:261,3-Dichlorobenzene [541-73-1]^0.092 MRK8A100111.00.092 U 1
ug/L SM 6200B-1997 01/10/18 19:261,3-Dichloropropane [142-28-9]^0.15 MRK8A100111.00.15 U 1
ug/L SM 6200B-1997 01/10/18 19:261,4-Dichlorobenzene [106-46-7]^0.10 MRK8A100111.00.10 U 1
ug/L SM 6200B-1997 01/10/18 19:262,2-Dichloropropane [594-20-7]^0.12 MRK8A100111.00.12 U 1
ug/L SM 6200B-1997 01/10/18 19:262-Chlorotoluene [95-49-8]^0.10 MRK8A100111.00.10 U 1
ug/L SM 6200B-1997 01/10/18 19:264-Chlorotoluene [106-43-4]^0.10 MRK8A100111.00.10 U 1
ug/L SM 6200B-1997 01/10/18 19:264-Isopropyltoluene [99-87-6]^0.066 MRK8A100111.00.91 J 1
ug/L SM 6200B-1997 01/10/18 19:26Benzene [71-43-2]^0.050 MRK8A100111.00.51 J 1
ug/L SM 6200B-1997 01/10/18 19:26Bromobenzene [108-86-1]^0.13 MRK8A100111.00.13 U 1
ug/L SM 6200B-1997 01/10/18 19:26Bromochloromethane [74-97-5]^0.11 MRK8A100111.00.11 U 1
ug/L SM 6200B-1997 01/10/18 19:26Bromodichloromethane [75-27-4]^0.10 MRK8A100111.00.10 U 1
ug/L SM 6200B-1997 01/10/18 19:26Bromoform [75-25-2]^0.20 MRK8A100111.00.20 U 1
ug/L SM 6200B-1997 01/10/18 19:26Bromomethane [74-83-9]^0.28 MRK8A100111.00.28 U 1
ug/L SM 6200B-1997 01/10/18 19:26Carbon Tetrachloride [56-23-5]^0.082 MRK8A100111.00.082 U 1
ug/L SM 6200B-1997 01/10/18 19:26Chlorobenzene [108-90-7]^0.069 MRK8A100111.00.069 U 1
ug/L SM 6200B-1997 01/10/18 19:26Chloroethane [75-00-3]^0.18 MRK8A100111.00.18 U 1
ug/L SM 6200B-1997 01/10/18 19:26Chloroform [67-66-3]^0.083 MRK8A100111.00.083 U 1
ug/L SM 6200B-1997 01/10/18 19:26Chloromethane [74-87-3]^0.050 MRK8A100111.00.050 U 1
ug/L SM 6200B-1997 01/10/18 19:26cis-1,2-Dichloroethene [156-59-2]^0.075 MRK8A100111.00.075 U 1
ug/L SM 6200B-1997 01/10/18 19:26cis-1,3-Dichloropropene [10061-01-5]^0.073 MRK8A100111.00.073 U 1
ug/L SM 6200B-1997 01/10/18 19:26Dibromochloromethane [124-48-1]^0.067 MRK8A100111.00.067 U 1
ug/L SM 6200B-1997 01/10/18 19:26Dibromomethane [74-95-3]^0.13 MRK8A100111.00.13 U 1
ug/L SM 6200B-1997 01/10/18 19:26Dichlorodifluoromethane [75-71-8]^0.091 MRK8A100111.00.091 U 1
ug/L SM 6200B-1997 01/10/18 19:26Ethylbenzene [100-41-4]^0.10 MRK8A100111.05.1 1
ug/L SM 6200B-1997 01/10/18 19:26Freon 113 [76-13-1]^0.35 MRK8A100111.00.35 U 1
ug/L SM 6200B-1997 01/10/18 19:26Hexachlorobutadiene [87-68-3]^0.15 MRK8A100111.00.15 U 1
ug/L SM 6200B-1997 01/10/18 19:26Isopropyl Ether [108-20-3]^0.21 MRK8A100111.00.21 U 1
ug/L SM 6200B-1997 01/10/18 19:26Isopropylbenzene [98-82-8]^0.13 MRK8A100111.04.5 1
ug/L SM 6200B-1997 01/10/18 19:26m,p-Xylenes [108-38-3/106-42-3]^0.18 MRK8A100112.00.18 U 1
ug/L SM 6200B-1997 01/10/18 19:26Methylene Chloride [75-09-2]^0.070 MRK8A100112.00.070 U 1
Page 10 of 27This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
MW-12Description:Lab Sample ID:CA19202-04 01/09/18 15:41Received:
CA19202Work Order:01/09/18 12:29Sampled:Ground WaterMatrix:
Justin AbreuSampled By:Project:Kuik Stop
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 01/10/18 19:26Methyl-tert-Butyl Ether [1634-04-4]^0.12 MRK8A100111.00.12 U 1
ug/L SM 6200B-1997 01/10/18 19:26Naphthalene [91-20-3]^0.086 MRK8A100111.01.3 1
ug/L SM 6200B-1997 01/10/18 19:26n-Butyl Benzene [104-51-8]^0.074 MRK8A100111.02.9 1
ug/L SM 6200B-1997 01/10/18 19:26n-Propyl Benzene [103-65-1]^0.073 MRK8A100111.010 1
ug/L SM 6200B-1997 01/10/18 19:26o-Xylene [95-47-6]^0.088 MRK8A100111.00.088 U 1
ug/L SM 6200B-1997 01/10/18 19:26sec-Butylbenzene [135-98-8]^0.053 MRK8A100111.01.6 1
ug/L SM 6200B-1997 01/10/18 19:26Styrene [100-42-5]^0.082 MRK8A100111.00.082 U 1
ug/L SM 6200B-1997 01/10/18 19:26tert-Butylbenzene [98-06-6]^0.094 MRK8A100111.00.094 U 1
ug/L SM 6200B-1997 01/10/18 19:26Tetrachloroethene [127-18-4]^0.099 MRK8A100111.00.099 U 1
ug/L SM 6200B-1997 01/10/18 19:26Toluene [108-88-3]^0.053 MRK8A100111.00.053 U 1
ug/L SM 6200B-1997 01/10/18 19:26trans-1,2-Dichloroethene [156-60-5]^0.11 MRK8A100111.00.11 U 1
ug/L SM 6200B-1997 01/10/18 19:26trans-1,3-Dichloropropene [10061-02-6]^0.080 MRK8A100111.00.080 U 1
ug/L SM 6200B-1997 01/10/18 19:26Trichloroethene [79-01-6]^0.13 MRK8A100111.00.13 U 1
ug/L SM 6200B-1997 01/10/18 19:26Trichlorofluoromethane [75-69-4]^0.15 MRK8A100111.00.15 U 1
ug/L SM 6200B-1997 01/10/18 19:26Vinyl chloride [75-01-4]^0.083 MRK8A100111.00.083 U 1
ug/L SM 6200B-1997 01/10/18 19:26Xylenes (Total) [1330-20-7]^0.22 MRK8A100111.00.22 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 70-130104 %MRKSM 6200B-1997 01/10/18 19:268A100115250.0 1
Dibromofluoromethane 70-130104 %MRKSM 6200B-1997 01/10/18 19:268A100115250.0 1
Toluene-d8 70-13096 %MRKSM 6200B-1997 01/10/18 19:268A100114850.0 1
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 6010D 01/15/18 12:22Iron [7439-89-6]^110 JDH8A10004250396000D 5
Metals (acid extractable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 6010D 01/15/18 13:29Lead [7439-92-1]^3.10 JDH8A1000710.0397 1
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/L EPA 300.0 01/12/18 10:15Sulfate as SO4 [14808-79-8]^5.8 MKS8A110331037D R-012
Page 11 of 27This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
MW-13Description:Lab Sample ID:CA19202-05 01/09/18 15:41Received:
CA19202Work Order:01/09/18 12:15Sampled:Ground WaterMatrix:
Justin AbreuSampled By:Project:Kuik Stop
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 01/10/18 19:571,1,1,2-Tetrachloroethane [630-20-6]^0.91 MRK8A10011100.91 UD 10
ug/L SM 6200B-1997 01/10/18 19:571,1,1-Trichloroethane [71-55-6]^1.5 MRK8A10011101.5 UD 10
ug/L SM 6200B-1997 01/10/18 19:571,1,2,2-Tetrachloroethane [79-34-5]^0.85 MRK8A10011100.85 UD 10
ug/L SM 6200B-1997 01/10/18 19:571,1,2-Trichloroethane [79-00-5]^0.68 MRK8A10011100.68 UD 10
ug/L SM 6200B-1997 01/10/18 19:571,1-Dichloroethane [75-34-3]^0.50 MRK8A10011100.50 UD 10
ug/L SM 6200B-1997 01/10/18 19:571,1-Dichloroethene [75-35-4]^1.5 MRK8A10011101.5 UD 10
ug/L SM 6200B-1997 01/10/18 19:571,1-Dichloropropene [563-58-6]^0.63 MRK8A10011100.63 UD 10
ug/L SM 6200B-1997 01/10/18 19:571,2,3-Trichlorobenzene [87-61-6]^2.5 MRK8A10011102.5 UD 10
ug/L SM 6200B-1997 01/10/18 19:571,2,3-Trichloropropane [96-18-4]^1.5 MRK8A10011101.5 UD 10
ug/L SM 6200B-1997 01/10/18 19:571,2,4-Trichlorobenzene [120-82-1]^0.97 MRK8A10011100.97 UD 10
ug/L SM 6200B-1997 01/10/18 19:571,2,4-Trimethylbenzene [95-63-6]^0.67 MRK8A10011100.67 UD 10
ug/L SM 6200B-1997 01/10/18 19:571,2-Dibromo-3-chloropropane [96-12-8]^4.8 MRK8A10011104.8 UD 10
ug/L SM 6200B-1997 01/10/18 19:571,2-Dibromoethane [106-93-4]^4.2 MRK8A10011104.2 UD 10
ug/L SM 6200B-1997 01/10/18 19:571,2-Dichlorobenzene [95-50-1]^0.52 MRK8A10011100.52 UD 10
ug/L SM 6200B-1997 01/10/18 19:571,2-Dichloroethane [107-06-2]^0.82 MRK8A10011100.82 UD 10
ug/L SM 6200B-1997 01/10/18 19:571,2-Dichloropropane [78-87-5]^0.98 MRK8A10011100.98 UD 10
ug/L SM 6200B-1997 01/10/18 19:571,3,5-Trimethylbenzene [108-67-8]^1.0 MRK8A10011101.0 UD 10
ug/L SM 6200B-1997 01/10/18 19:571,3-Dichlorobenzene [541-73-1]^0.92 MRK8A10011100.92 UD 10
ug/L SM 6200B-1997 01/10/18 19:571,3-Dichloropropane [142-28-9]^1.5 MRK8A10011101.5 UD 10
ug/L SM 6200B-1997 01/10/18 19:571,4-Dichlorobenzene [106-46-7]^1.0 MRK8A10011101.0 UD 10
ug/L SM 6200B-1997 01/10/18 19:572,2-Dichloropropane [594-20-7]^1.2 MRK8A10011101.2 UD 10
ug/L SM 6200B-1997 01/10/18 19:572-Chlorotoluene [95-49-8]^1.0 MRK8A10011101.0 UD 10
ug/L SM 6200B-1997 01/10/18 19:574-Chlorotoluene [106-43-4]^1.0 MRK8A10011101.0 UD 10
ug/L SM 6200B-1997 01/10/18 19:574-Isopropyltoluene [99-87-6]^0.66 MRK8A10011100.66 UD 10
ug/L SM 6200B-1997 01/10/18 19:57Benzene [71-43-2]^0.50 MRK8A10011100.50 UD 10
ug/L SM 6200B-1997 01/10/18 19:57Bromobenzene [108-86-1]^1.3 MRK8A10011101.3 UD 10
ug/L SM 6200B-1997 01/10/18 19:57Bromochloromethane [74-97-5]^1.1 MRK8A10011101.1 UD 10
ug/L SM 6200B-1997 01/10/18 19:57Bromodichloromethane [75-27-4]^1.0 MRK8A10011101.0 UD 10
ug/L SM 6200B-1997 01/10/18 19:57Bromoform [75-25-2]^2.0 MRK8A10011102.0 UD 10
ug/L SM 6200B-1997 01/10/18 19:57Bromomethane [74-83-9]^2.8 MRK8A10011102.8 UD 10
ug/L SM 6200B-1997 01/10/18 19:57Carbon Tetrachloride [56-23-5]^0.82 MRK8A10011100.82 UD 10
ug/L SM 6200B-1997 01/10/18 19:57Chlorobenzene [108-90-7]^0.69 MRK8A10011100.69 UD 10
ug/L SM 6200B-1997 01/10/18 19:57Chloroethane [75-00-3]^1.8 MRK8A10011101.8 UD 10
ug/L SM 6200B-1997 01/10/18 19:57Chloroform [67-66-3]^0.83 MRK8A10011100.83 UD 10
ug/L SM 6200B-1997 01/10/18 19:57Chloromethane [74-87-3]^0.50 MRK8A10011100.50 UD 10
ug/L SM 6200B-1997 01/10/18 19:57cis-1,2-Dichloroethene [156-59-2]^0.75 MRK8A10011100.75 UD 10
ug/L SM 6200B-1997 01/10/18 19:57cis-1,3-Dichloropropene [10061-01-5]^0.73 MRK8A10011100.73 UD 10
ug/L SM 6200B-1997 01/10/18 19:57Dibromochloromethane [124-48-1]^0.67 MRK8A10011100.67 UD 10
ug/L SM 6200B-1997 01/10/18 19:57Dibromomethane [74-95-3]^1.3 MRK8A10011101.3 UD 10
ug/L SM 6200B-1997 01/10/18 19:57Dichlorodifluoromethane [75-71-8]^0.91 MRK8A10011100.91 UD 10
ug/L SM 6200B-1997 01/10/18 19:57Ethylbenzene [100-41-4]^1.0 MRK8A10011101.0 UD 10
ug/L SM 6200B-1997 01/10/18 19:57Freon 113 [76-13-1]^3.5 MRK8A10011103.5 UD 10
ug/L SM 6200B-1997 01/10/18 19:57Hexachlorobutadiene [87-68-3]^1.5 MRK8A10011101.5 UD 10
ug/L SM 6200B-1997 01/10/18 19:57Isopropyl Ether [108-20-3]^2.1 MRK8A100111064D 10
ug/L SM 6200B-1997 01/10/18 19:57Isopropylbenzene [98-82-8]^1.3 MRK8A10011101.3 UD 10
ug/L SM 6200B-1997 01/10/18 19:57m,p-Xylenes [108-38-3/106-42-3]^1.8 MRK8A10011201.8 UD 10
ug/L SM 6200B-1997 01/10/18 19:57Methylene Chloride [75-09-2]^0.70 MRK8A10011200.70 UD 10
Page 12 of 27This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
MW-13Description:Lab Sample ID:CA19202-05 01/09/18 15:41Received:
CA19202Work Order:01/09/18 12:15Sampled:Ground WaterMatrix:
Justin AbreuSampled By:Project:Kuik Stop
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 01/10/18 19:57Methyl-tert-Butyl Ether [1634-04-4]^1.2 MRK8A10011101000D 10
ug/L SM 6200B-1997 01/10/18 19:57Naphthalene [91-20-3]^0.86 MRK8A10011100.86 UD 10
ug/L SM 6200B-1997 01/10/18 19:57n-Butyl Benzene [104-51-8]^0.74 MRK8A10011100.74 UD 10
ug/L SM 6200B-1997 01/10/18 19:57n-Propyl Benzene [103-65-1]^0.73 MRK8A10011100.73 UD 10
ug/L SM 6200B-1997 01/10/18 19:57o-Xylene [95-47-6]^0.88 MRK8A10011100.88 UD 10
ug/L SM 6200B-1997 01/10/18 19:57sec-Butylbenzene [135-98-8]^0.53 MRK8A10011100.53 UD 10
ug/L SM 6200B-1997 01/10/18 19:57Styrene [100-42-5]^0.82 MRK8A10011100.82 UD 10
ug/L SM 6200B-1997 01/10/18 19:57tert-Butylbenzene [98-06-6]^0.94 MRK8A10011100.94 UD 10
ug/L SM 6200B-1997 01/10/18 19:57Tetrachloroethene [127-18-4]^0.99 MRK8A10011100.99 UD 10
ug/L SM 6200B-1997 01/10/18 19:57Toluene [108-88-3]^0.53 MRK8A10011100.53 UD 10
ug/L SM 6200B-1997 01/10/18 19:57trans-1,2-Dichloroethene [156-60-5]^1.1 MRK8A10011101.1 UD 10
ug/L SM 6200B-1997 01/10/18 19:57trans-1,3-Dichloropropene [10061-02-6]^0.80 MRK8A10011100.80 UD 10
ug/L SM 6200B-1997 01/10/18 19:57Trichloroethene [79-01-6]^1.3 MRK8A10011101.3 UD 10
ug/L SM 6200B-1997 01/10/18 19:57Trichlorofluoromethane [75-69-4]^1.5 MRK8A10011101.5 UD 10
ug/L SM 6200B-1997 01/10/18 19:57Vinyl chloride [75-01-4]^0.83 MRK8A10011100.83 UD 10
ug/L SM 6200B-1997 01/10/18 19:57Xylenes (Total) [1330-20-7]^2.2 MRK8A10011102.2 UD 10
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 70-130106 %MRKSM 6200B-1997 01/10/18 19:578A100115350.0 1
Dibromofluoromethane 70-130105 %MRKSM 6200B-1997 01/10/18 19:578A100115250.0 1
Toluene-d8 70-13098 %MRKSM 6200B-1997 01/10/18 19:578A100114950.0 1
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 6010D 01/15/18 11:47Iron [7439-89-6]^22.0 JDH8A1000450.06960 1
Metals (acid extractable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 6010D 01/15/18 13:32Lead [7439-92-1]^3.10 JDH8A1000710.03.21 J 1
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
mg/L EPA 300.0 01/11/18 17:50Sulfate as SO4 [14808-79-8]^2.9 MKS8A110335.04.7 J 1
Page 13 of 27This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
Brown SWDescription:Lab Sample ID:CA19202-06 01/09/18 15:41Received:
CA19202Work Order:01/09/18 12:49Sampled:Ground WaterMatrix:
Justin AbreuSampled By:Project:Kuik Stop
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 01/10/18 20:271,1,1,2-Tetrachloroethane [630-20-6]^0.091 MRK8A100111.00.091 U 1
ug/L SM 6200B-1997 01/10/18 20:271,1,1-Trichloroethane [71-55-6]^0.15 MRK8A100111.00.15 U 1
ug/L SM 6200B-1997 01/10/18 20:271,1,2,2-Tetrachloroethane [79-34-5]^0.085 MRK8A100111.00.085 U 1
ug/L SM 6200B-1997 01/10/18 20:271,1,2-Trichloroethane [79-00-5]^0.068 MRK8A100111.00.068 U 1
ug/L SM 6200B-1997 01/10/18 20:271,1-Dichloroethane [75-34-3]^0.050 MRK8A100111.00.050 U 1
ug/L SM 6200B-1997 01/10/18 20:271,1-Dichloroethene [75-35-4]^0.15 MRK8A100111.00.15 U 1
ug/L SM 6200B-1997 01/10/18 20:271,1-Dichloropropene [563-58-6]^0.063 MRK8A100111.00.063 U 1
ug/L SM 6200B-1997 01/10/18 20:271,2,3-Trichlorobenzene [87-61-6]^0.25 MRK8A100111.00.25 U 1
ug/L SM 6200B-1997 01/10/18 20:271,2,3-Trichloropropane [96-18-4]^0.15 MRK8A100111.00.15 U 1
ug/L SM 6200B-1997 01/10/18 20:271,2,4-Trichlorobenzene [120-82-1]^0.097 MRK8A100111.00.097 U 1
ug/L SM 6200B-1997 01/10/18 20:271,2,4-Trimethylbenzene [95-63-6]^0.067 MRK8A100111.00.067 U 1
ug/L SM 6200B-1997 01/10/18 20:271,2-Dibromo-3-chloropropane [96-12-8]^0.48 MRK8A100111.00.48 U 1
ug/L SM 6200B-1997 01/10/18 20:271,2-Dibromoethane [106-93-4]^0.42 MRK8A100111.00.42 U 1
ug/L SM 6200B-1997 01/10/18 20:271,2-Dichlorobenzene [95-50-1]^0.052 MRK8A100111.00.052 U 1
ug/L SM 6200B-1997 01/10/18 20:271,2-Dichloroethane [107-06-2]^0.082 MRK8A100111.00.082 U 1
ug/L SM 6200B-1997 01/10/18 20:271,2-Dichloropropane [78-87-5]^0.098 MRK8A100111.00.098 U 1
ug/L SM 6200B-1997 01/10/18 20:271,3,5-Trimethylbenzene [108-67-8]^0.10 MRK8A100111.00.10 U 1
ug/L SM 6200B-1997 01/10/18 20:271,3-Dichlorobenzene [541-73-1]^0.092 MRK8A100111.00.092 U 1
ug/L SM 6200B-1997 01/10/18 20:271,3-Dichloropropane [142-28-9]^0.15 MRK8A100111.00.15 U 1
ug/L SM 6200B-1997 01/10/18 20:271,4-Dichlorobenzene [106-46-7]^0.10 MRK8A100111.00.10 U 1
ug/L SM 6200B-1997 01/10/18 20:272,2-Dichloropropane [594-20-7]^0.12 MRK8A100111.00.12 U 1
ug/L SM 6200B-1997 01/10/18 20:272-Chlorotoluene [95-49-8]^0.10 MRK8A100111.00.10 U 1
ug/L SM 6200B-1997 01/10/18 20:274-Chlorotoluene [106-43-4]^0.10 MRK8A100111.00.10 U 1
ug/L SM 6200B-1997 01/10/18 20:274-Isopropyltoluene [99-87-6]^0.066 MRK8A100111.00.066 U 1
ug/L SM 6200B-1997 01/10/18 20:27Benzene [71-43-2]^0.050 MRK8A100111.00.050 U 1
ug/L SM 6200B-1997 01/10/18 20:27Bromobenzene [108-86-1]^0.13 MRK8A100111.00.13 U 1
ug/L SM 6200B-1997 01/10/18 20:27Bromochloromethane [74-97-5]^0.11 MRK8A100111.00.11 U 1
ug/L SM 6200B-1997 01/10/18 20:27Bromodichloromethane [75-27-4]^0.10 MRK8A100111.00.10 U 1
ug/L SM 6200B-1997 01/10/18 20:27Bromoform [75-25-2]^0.20 MRK8A100111.00.20 U 1
ug/L SM 6200B-1997 01/10/18 20:27Bromomethane [74-83-9]^0.28 MRK8A100111.00.28 U 1
ug/L SM 6200B-1997 01/10/18 20:27Carbon Tetrachloride [56-23-5]^0.082 MRK8A100111.00.082 U 1
ug/L SM 6200B-1997 01/10/18 20:27Chlorobenzene [108-90-7]^0.069 MRK8A100111.00.069 U 1
ug/L SM 6200B-1997 01/10/18 20:27Chloroethane [75-00-3]^0.18 MRK8A100111.00.18 U 1
ug/L SM 6200B-1997 01/10/18 20:27Chloroform [67-66-3]^0.083 MRK8A100111.00.083 U 1
ug/L SM 6200B-1997 01/10/18 20:27Chloromethane [74-87-3]^0.050 MRK8A100111.00.050 U 1
ug/L SM 6200B-1997 01/10/18 20:27cis-1,2-Dichloroethene [156-59-2]^0.075 MRK8A100111.00.075 U 1
ug/L SM 6200B-1997 01/10/18 20:27cis-1,3-Dichloropropene [10061-01-5]^0.073 MRK8A100111.00.073 U 1
ug/L SM 6200B-1997 01/10/18 20:27Dibromochloromethane [124-48-1]^0.067 MRK8A100111.00.067 U 1
ug/L SM 6200B-1997 01/10/18 20:27Dibromomethane [74-95-3]^0.13 MRK8A100111.00.13 U 1
ug/L SM 6200B-1997 01/10/18 20:27Dichlorodifluoromethane [75-71-8]^0.091 MRK8A100111.00.091 U 1
ug/L SM 6200B-1997 01/10/18 20:27Ethylbenzene [100-41-4]^0.10 MRK8A100111.00.10 U 1
ug/L SM 6200B-1997 01/10/18 20:27Freon 113 [76-13-1]^0.35 MRK8A100111.00.35 U 1
ug/L SM 6200B-1997 01/10/18 20:27Hexachlorobutadiene [87-68-3]^0.15 MRK8A100111.00.15 U 1
ug/L SM 6200B-1997 01/10/18 20:27Isopropyl Ether [108-20-3]^0.21 MRK8A100111.00.21 U 1
ug/L SM 6200B-1997 01/10/18 20:27Isopropylbenzene [98-82-8]^0.13 MRK8A100111.00.13 U 1
ug/L SM 6200B-1997 01/10/18 20:27m,p-Xylenes [108-38-3/106-42-3]^0.18 MRK8A100112.00.18 U 1
ug/L SM 6200B-1997 01/10/18 20:27Methylene Chloride [75-09-2]^0.070 MRK8A100112.00.070 U 1
Page 14 of 27This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
www.encolabs.com
ANALYTICAL RESULTS
Brown SWDescription:Lab Sample ID:CA19202-06 01/09/18 15:41Received:
CA19202Work Order:01/09/18 12:49Sampled:Ground WaterMatrix:
Justin AbreuSampled By:Project:Kuik Stop
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 01/10/18 20:27Methyl-tert-Butyl Ether [1634-04-4]^0.12 MRK8A100111.00.12 U 1
ug/L SM 6200B-1997 01/10/18 20:27Naphthalene [91-20-3]^0.086 MRK8A100111.00.086 U 1
ug/L SM 6200B-1997 01/10/18 20:27n-Butyl Benzene [104-51-8]^0.074 MRK8A100111.00.074 U 1
ug/L SM 6200B-1997 01/10/18 20:27n-Propyl Benzene [103-65-1]^0.073 MRK8A100111.00.073 U 1
ug/L SM 6200B-1997 01/10/18 20:27o-Xylene [95-47-6]^0.088 MRK8A100111.00.088 U 1
ug/L SM 6200B-1997 01/10/18 20:27sec-Butylbenzene [135-98-8]^0.053 MRK8A100111.00.053 U 1
ug/L SM 6200B-1997 01/10/18 20:27Styrene [100-42-5]^0.082 MRK8A100111.00.082 U 1
ug/L SM 6200B-1997 01/10/18 20:27tert-Butylbenzene [98-06-6]^0.094 MRK8A100111.00.094 U 1
ug/L SM 6200B-1997 01/10/18 20:27Tetrachloroethene [127-18-4]^0.099 MRK8A100111.00.099 U 1
ug/L SM 6200B-1997 01/10/18 20:27Toluene [108-88-3]^0.053 MRK8A100111.00.053 U 1
ug/L SM 6200B-1997 01/10/18 20:27trans-1,2-Dichloroethene [156-60-5]^0.11 MRK8A100111.00.11 U 1
ug/L SM 6200B-1997 01/10/18 20:27trans-1,3-Dichloropropene [10061-02-6]^0.080 MRK8A100111.00.080 U 1
ug/L SM 6200B-1997 01/10/18 20:27Trichloroethene [79-01-6]^0.13 MRK8A100111.00.13 U 1
ug/L SM 6200B-1997 01/10/18 20:27Trichlorofluoromethane [75-69-4]^0.15 MRK8A100111.00.15 U 1
ug/L SM 6200B-1997 01/10/18 20:27Vinyl chloride [75-01-4]^0.083 MRK8A100111.00.083 U 1
ug/L SM 6200B-1997 01/10/18 20:27Xylenes (Total) [1330-20-7]^0.22 MRK8A100111.00.22 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 70-130110 %MRKSM 6200B-1997 01/10/18 20:278A100115550.0 1
Dibromofluoromethane 70-130104 %MRKSM 6200B-1997 01/10/18 20:278A100115250.0 1
Toluene-d8 70-13098 %MRKSM 6200B-1997 01/10/18 20:278A100114950.0 1
Metals (acid extractable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L EPA 6010D 01/15/18 13:35Lead [7439-92-1]^3.10 JDH8A1000710.03.10 U 1
Page 15 of 27This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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ANALYTICAL RESULTS
Trip BlankDescription:Lab Sample ID:CA19202-07 01/09/18 15:41Received:
CA19202Work Order:01/09/18 11:57Sampled:WaterMatrix:
ENCOSampled By:Project:Kuik Stop
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 01/10/18 20:571,1,1,2-Tetrachloroethane [630-20-6]^0.091 MRK8A100111.00.091 U 1
ug/L SM 6200B-1997 01/10/18 20:571,1,1-Trichloroethane [71-55-6]^0.15 MRK8A100111.00.15 U 1
ug/L SM 6200B-1997 01/10/18 20:571,1,2,2-Tetrachloroethane [79-34-5]^0.085 MRK8A100111.00.085 U 1
ug/L SM 6200B-1997 01/10/18 20:571,1,2-Trichloroethane [79-00-5]^0.068 MRK8A100111.00.068 U 1
ug/L SM 6200B-1997 01/10/18 20:571,1-Dichloroethane [75-34-3]^0.050 MRK8A100111.00.050 U 1
ug/L SM 6200B-1997 01/10/18 20:571,1-Dichloroethene [75-35-4]^0.15 MRK8A100111.00.15 U 1
ug/L SM 6200B-1997 01/10/18 20:571,1-Dichloropropene [563-58-6]^0.063 MRK8A100111.00.063 U 1
ug/L SM 6200B-1997 01/10/18 20:571,2,3-Trichlorobenzene [87-61-6]^0.25 MRK8A100111.00.25 U 1
ug/L SM 6200B-1997 01/10/18 20:571,2,3-Trichloropropane [96-18-4]^0.15 MRK8A100111.00.15 U 1
ug/L SM 6200B-1997 01/10/18 20:571,2,4-Trichlorobenzene [120-82-1]^0.097 MRK8A100111.00.097 U 1
ug/L SM 6200B-1997 01/10/18 20:571,2,4-Trimethylbenzene [95-63-6]^0.067 MRK8A100111.00.067 U 1
ug/L SM 6200B-1997 01/10/18 20:571,2-Dibromo-3-chloropropane [96-12-8]^0.48 MRK8A100111.00.48 U 1
ug/L SM 6200B-1997 01/10/18 20:571,2-Dibromoethane [106-93-4]^0.42 MRK8A100111.00.42 U 1
ug/L SM 6200B-1997 01/10/18 20:571,2-Dichlorobenzene [95-50-1]^0.052 MRK8A100111.00.052 U 1
ug/L SM 6200B-1997 01/10/18 20:571,2-Dichloroethane [107-06-2]^0.082 MRK8A100111.00.082 U 1
ug/L SM 6200B-1997 01/10/18 20:571,2-Dichloropropane [78-87-5]^0.098 MRK8A100111.00.098 U 1
ug/L SM 6200B-1997 01/10/18 20:571,3,5-Trimethylbenzene [108-67-8]^0.10 MRK8A100111.00.10 U 1
ug/L SM 6200B-1997 01/10/18 20:571,3-Dichlorobenzene [541-73-1]^0.092 MRK8A100111.00.092 U 1
ug/L SM 6200B-1997 01/10/18 20:571,3-Dichloropropane [142-28-9]^0.15 MRK8A100111.00.15 U 1
ug/L SM 6200B-1997 01/10/18 20:571,4-Dichlorobenzene [106-46-7]^0.10 MRK8A100111.00.10 U 1
ug/L SM 6200B-1997 01/10/18 20:572,2-Dichloropropane [594-20-7]^0.12 MRK8A100111.00.12 U 1
ug/L SM 6200B-1997 01/10/18 20:572-Chlorotoluene [95-49-8]^0.10 MRK8A100111.00.10 U 1
ug/L SM 6200B-1997 01/10/18 20:574-Chlorotoluene [106-43-4]^0.10 MRK8A100111.00.10 U 1
ug/L SM 6200B-1997 01/10/18 20:574-Isopropyltoluene [99-87-6]^0.066 MRK8A100111.00.066 U 1
ug/L SM 6200B-1997 01/10/18 20:57Benzene [71-43-2]^0.050 MRK8A100111.00.050 U 1
ug/L SM 6200B-1997 01/10/18 20:57Bromobenzene [108-86-1]^0.13 MRK8A100111.00.13 U 1
ug/L SM 6200B-1997 01/10/18 20:57Bromochloromethane [74-97-5]^0.11 MRK8A100111.00.11 U 1
ug/L SM 6200B-1997 01/10/18 20:57Bromodichloromethane [75-27-4]^0.10 MRK8A100111.00.10 U 1
ug/L SM 6200B-1997 01/10/18 20:57Bromoform [75-25-2]^0.20 MRK8A100111.00.20 U 1
ug/L SM 6200B-1997 01/10/18 20:57Bromomethane [74-83-9]^0.28 MRK8A100111.00.28 U 1
ug/L SM 6200B-1997 01/10/18 20:57Carbon Tetrachloride [56-23-5]^0.082 MRK8A100111.00.082 U 1
ug/L SM 6200B-1997 01/10/18 20:57Chlorobenzene [108-90-7]^0.069 MRK8A100111.00.069 U 1
ug/L SM 6200B-1997 01/10/18 20:57Chloroethane [75-00-3]^0.18 MRK8A100111.00.18 U 1
ug/L SM 6200B-1997 01/10/18 20:57Chloroform [67-66-3]^0.083 MRK8A100111.00.083 U 1
ug/L SM 6200B-1997 01/10/18 20:57Chloromethane [74-87-3]^0.050 MRK8A100111.00.050 U 1
ug/L SM 6200B-1997 01/10/18 20:57cis-1,2-Dichloroethene [156-59-2]^0.075 MRK8A100111.00.075 U 1
ug/L SM 6200B-1997 01/10/18 20:57cis-1,3-Dichloropropene [10061-01-5]^0.073 MRK8A100111.00.073 U 1
ug/L SM 6200B-1997 01/10/18 20:57Dibromochloromethane [124-48-1]^0.067 MRK8A100111.00.067 U 1
ug/L SM 6200B-1997 01/10/18 20:57Dibromomethane [74-95-3]^0.13 MRK8A100111.00.13 U 1
ug/L SM 6200B-1997 01/10/18 20:57Dichlorodifluoromethane [75-71-8]^0.091 MRK8A100111.00.091 U 1
ug/L SM 6200B-1997 01/10/18 20:57Ethylbenzene [100-41-4]^0.10 MRK8A100111.00.10 U 1
ug/L SM 6200B-1997 01/10/18 20:57Freon 113 [76-13-1]^0.35 MRK8A100111.00.35 U 1
ug/L SM 6200B-1997 01/10/18 20:57Hexachlorobutadiene [87-68-3]^0.15 MRK8A100111.00.15 U 1
ug/L SM 6200B-1997 01/10/18 20:57Isopropyl Ether [108-20-3]^0.21 MRK8A100111.00.21 U 1
ug/L SM 6200B-1997 01/10/18 20:57Isopropylbenzene [98-82-8]^0.13 MRK8A100111.00.13 U 1
ug/L SM 6200B-1997 01/10/18 20:57m,p-Xylenes [108-38-3/106-42-3]^0.18 MRK8A100112.00.18 U 1
ug/L SM 6200B-1997 01/10/18 20:57Methylene Chloride [75-09-2]^0.070 MRK8A100112.00.070 U 1
Page 16 of 27This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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ANALYTICAL RESULTS
Trip BlankDescription:Lab Sample ID:CA19202-07 01/09/18 15:41Received:
CA19202Work Order:01/09/18 11:57Sampled:WaterMatrix:
ENCOSampled By:Project:Kuik Stop
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-1997 01/10/18 20:57Methyl-tert-Butyl Ether [1634-04-4]^0.12 MRK8A100111.00.12 U 1
ug/L SM 6200B-1997 01/10/18 20:57Naphthalene [91-20-3]^0.086 MRK8A100111.00.086 U 1
ug/L SM 6200B-1997 01/10/18 20:57n-Butyl Benzene [104-51-8]^0.074 MRK8A100111.00.074 U 1
ug/L SM 6200B-1997 01/10/18 20:57n-Propyl Benzene [103-65-1]^0.073 MRK8A100111.00.073 U 1
ug/L SM 6200B-1997 01/10/18 20:57o-Xylene [95-47-6]^0.088 MRK8A100111.00.088 U 1
ug/L SM 6200B-1997 01/10/18 20:57sec-Butylbenzene [135-98-8]^0.053 MRK8A100111.00.053 U 1
ug/L SM 6200B-1997 01/10/18 20:57Styrene [100-42-5]^0.082 MRK8A100111.00.082 U 1
ug/L SM 6200B-1997 01/10/18 20:57tert-Butylbenzene [98-06-6]^0.094 MRK8A100111.00.094 U 1
ug/L SM 6200B-1997 01/10/18 20:57Tetrachloroethene [127-18-4]^0.099 MRK8A100111.00.099 U 1
ug/L SM 6200B-1997 01/10/18 20:57Toluene [108-88-3]^0.053 MRK8A100111.00.053 U 1
ug/L SM 6200B-1997 01/10/18 20:57trans-1,2-Dichloroethene [156-60-5]^0.11 MRK8A100111.00.11 U 1
ug/L SM 6200B-1997 01/10/18 20:57trans-1,3-Dichloropropene [10061-02-6]^0.080 MRK8A100111.00.080 U 1
ug/L SM 6200B-1997 01/10/18 20:57Trichloroethene [79-01-6]^0.13 MRK8A100111.00.13 U 1
ug/L SM 6200B-1997 01/10/18 20:57Trichlorofluoromethane [75-69-4]^0.15 MRK8A100111.00.15 U 1
ug/L SM 6200B-1997 01/10/18 20:57Vinyl chloride [75-01-4]^0.083 MRK8A100111.00.083 U 1
ug/L SM 6200B-1997 01/10/18 20:57Xylenes (Total) [1330-20-7]^0.22 MRK8A100111.00.22 U 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 70-130105 %MRKSM 6200B-1997 01/10/18 20:578A100115250.0 1
Dibromofluoromethane 70-130102 %MRKSM 6200B-1997 01/10/18 20:578A100115150.0 1
Toluene-d8 70-130100 %MRKSM 6200B-1997 01/10/18 20:578A100115050.0 1
Page 17 of 27This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 8A10011 - EPA 5030B_MS
Prepared: 01/10/2018 10:02 Analyzed: 01/10/2018 17:25Blank (8A10011-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.00.091 U 1,1,1,2-Tetrachloroethane
ug/L1.00.15 U 1,1,1-Trichloroethane
ug/L1.00.085 U 1,1,2,2-Tetrachloroethane
ug/L1.00.068 U 1,1,2-Trichloroethane
ug/L1.00.050 U 1,1-Dichloroethane
ug/L1.00.15 U 1,1-Dichloroethene
ug/L1.00.063 U 1,1-Dichloropropene
ug/L1.00.25 U 1,2,3-Trichlorobenzene
ug/L1.00.15 U 1,2,3-Trichloropropane
ug/L1.00.097 U 1,2,4-Trichlorobenzene
ug/L1.00.067 U 1,2,4-Trimethylbenzene
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.42 U 1,2-Dibromoethane
ug/L1.00.052 U 1,2-Dichlorobenzene
ug/L1.00.082 U 1,2-Dichloroethane
ug/L1.00.098 U 1,2-Dichloropropane
ug/L1.00.10 U 1,3,5-Trimethylbenzene
ug/L1.00.092 U 1,3-Dichlorobenzene
ug/L1.00.15 U 1,3-Dichloropropane
ug/L1.00.10 U 1,4-Dichlorobenzene
ug/L1.00.12 U 2,2-Dichloropropane
ug/L1.00.10 U 2-Chlorotoluene
ug/L1.00.10 U 4-Chlorotoluene
ug/L1.00.066 U 4-Isopropyltoluene
ug/L1.00.050 U Benzene
ug/L1.00.13 U Bromobenzene
ug/L1.00.11 U Bromochloromethane
ug/L1.00.10 U Bromodichloromethane
ug/L1.00.20 U Bromoform
ug/L1.00.28 U Bromomethane
ug/L1.00.082 U Carbon Tetrachloride
ug/L1.00.069 U Chlorobenzene
ug/L1.00.18 U Chloroethane
ug/L1.00.083 U Chloroform
ug/L1.00.050 U Chloromethane
ug/L1.00.075 U cis-1,2-Dichloroethene
ug/L1.00.073 U cis-1,3-Dichloropropene
ug/L1.00.067 U Dibromochloromethane
ug/L1.00.13 U Dibromomethane
ug/L1.00.091 U Dichlorodifluoromethane
ug/L1.00.10 U Ethylbenzene
ug/L1.00.35 U Freon 113
ug/L1.00.15 U Hexachlorobutadiene
ug/L1.00.21 U Isopropyl Ether
ug/L1.00.13 U Isopropylbenzene
ug/L2.00.18 U m,p-Xylenes
ug/L2.00.070 U Methylene Chloride
ug/L1.00.12 U Methyl-tert-Butyl Ether
ug/L1.00.086 U Naphthalene
Page 18 of 27This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 8A10011 - EPA 5030B_MS - Continued
Prepared: 01/10/2018 10:02 Analyzed: 01/10/2018 17:25Blank (8A10011-BLK1) Continued
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.00.074 U n-Butyl Benzene
ug/L1.00.073 U n-Propyl Benzene
ug/L1.00.088 U o-Xylene
ug/L1.00.053 U sec-Butylbenzene
ug/L1.00.082 U Styrene
ug/L1.00.094 U tert-Butylbenzene
ug/L1.00.099 U Tetrachloroethene
ug/L1.00.053 U Toluene
ug/L1.00.11 U trans-1,2-Dichloroethene
ug/L1.00.080 U trans-1,3-Dichloropropene
ug/L1.00.13 U Trichloroethene
ug/L1.00.15 U Trichlorofluoromethane
ug/L1.00.083 U Vinyl chloride
ug/L1.00.22 U Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 10553
ug/L 50.0 70-130Dibromofluoromethane10553
ug/L 50.0 70-130Toluene-d8 9949
Prepared: 01/10/2018 10:02 Analyzed: 01/10/2018 16:24LCS (8A10011-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 70-1309619 1,1,1,2-Tetrachloroethane
ug/L1.0 20.0 70-1309920 1,1,1-Trichloroethane
ug/L1.0 20.0 70-1309218 1,1,2,2-Tetrachloroethane
ug/L1.0 20.0 70-1308517 1,1,2-Trichloroethane
ug/L1.0 20.0 70-13010521 1,1-Dichloroethane
ug/L1.0 20.0 70-13010521 1,1-Dichloroethene
ug/L1.0 20.0 70-1309619 1,1-Dichloropropene
ug/L1.0 20.0 70-13010421 1,2,3-Trichlorobenzene
ug/L1.0 20.0 70-1308216 1,2,3-Trichloropropane
ug/L1.0 20.0 70-13010621 1,2,4-Trichlorobenzene
ug/L1.0 20.0 70-1308717 1,2,4-Trimethylbenzene
ug/L1.0 20.0 70-13010020 1,2-Dibromo-3-chloropropane
ug/L1.0 20.0 70-1309018 1,2-Dibromoethane
ug/L1.0 20.0 70-1309018 1,2-Dichlorobenzene
ug/L1.0 20.0 70-13011323 1,2-Dichloroethane
ug/L1.0 20.0 70-1309719 1,2-Dichloropropane
ug/L1.0 20.0 70-1308818 1,3,5-Trimethylbenzene
ug/L1.0 20.0 70-1309319 1,3-Dichlorobenzene
ug/L1.0 20.0 70-1308717 1,3-Dichloropropane
ug/L1.0 20.0 70-1308717 1,4-Dichlorobenzene
ug/L1.0 20.0 70-13011022 2,2-Dichloropropane
ug/L1.0 20.0 70-1308517 2-Chlorotoluene
ug/L1.0 20.0 70-13010220 4-Chlorotoluene
ug/L1.0 20.0 70-1308517 4-Isopropyltoluene
ug/L1.0 20.0 70-1309619 Benzene
ug/L1.0 20.0 70-1309419 Bromobenzene
ug/L1.0 20.0 70-13011423 Bromochloromethane
ug/L1.0 20.0 70-13010321 Bromodichloromethane
Page 19 of 27This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 8A10011 - EPA 5030B_MS - Continued
Prepared: 01/10/2018 10:02 Analyzed: 01/10/2018 16:24LCS (8A10011-BS1) Continued
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 70-1308417 Bromoform
ug/L1.0 20.0 60-1407515 Bromomethane
ug/L1.0 20.0 70-1309820 Carbon Tetrachloride
ug/L1.0 20.0 70-1308717 Chlorobenzene
ug/L1.0 20.0 60-14011824 Chloroethane
ug/L1.0 20.0 70-1309619 Chloroform
ug/L1.0 20.0 60-14010020 Chloromethane
ug/L1.0 20.0 70-1309619 cis-1,2-Dichloroethene
ug/L1.0 20.0 70-1309519 cis-1,3-Dichloropropene
ug/L1.0 20.0 70-1309118 Dibromochloromethane
ug/L1.0 20.0 70-1309519 Dibromomethane
ug/L1.0 20.0 60-14010120 Dichlorodifluoromethane
ug/L1.0 20.0 70-1308617 Ethylbenzene
ug/L1.0 20.0 70-1308517 Freon 113
ug/L1.0 20.0 70-13011022 Hexachlorobutadiene
ug/L1.0 20.0 70-1309018 Isopropyl Ether
ug/L1.0 20.0 70-1309719 Isopropylbenzene
ug/L2.0 40.0 70-1309739 m,p-Xylenes
ug/L2.0 20.0 70-1309719 Methylene Chloride
ug/L1.0 20.0 70-1309419 Methyl-tert-Butyl Ether
ug/L1.0 20.0 70-1309519 Naphthalene
ug/L1.0 20.0 70-1308717 n-Butyl Benzene
ug/L1.0 20.0 70-1308918 n-Propyl Benzene
ug/L1.0 20.0 70-1308717 o-Xylene
ug/L1.0 20.0 70-1308317 sec-Butylbenzene
ug/L1.0 20.0 70-1308617 Styrene
ug/L1.0 20.0 70-1308417 tert-Butylbenzene
ug/L1.0 20.0 70-13010321 Tetrachloroethene
ug/L1.0 20.0 70-1308717 Toluene
ug/L1.0 20.0 70-1309920 trans-1,2-Dichloroethene
ug/L1.0 20.0 70-1309619 trans-1,3-Dichloropropene
ug/L1.0 20.0 70-1309218 Trichloroethene
ug/L1.0 20.0 60-14011423 Trichlorofluoromethane
ug/L1.0 20.0 60-14010421 Vinyl chloride
ug/L1.0 60.0 70-1309456 Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 10854
ug/L 50.0 70-130Dibromofluoromethane10452
ug/L 50.0 70-130Toluene-d8 9849
Prepared: 01/10/2018 10:02 Analyzed: 01/10/2018 14:44Matrix Spike (8A10011-MS1)
Source: CB00257-10
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 71-1171010.091 U20 1,1,1,2-Tetrachloroethane
ug/L1.0 20.0 72-1431030.15 U21 1,1,1-Trichloroethane
ug/L1.0 20.0 59-133940.085 U19 1,1,2,2-Tetrachloroethane
ug/L1.0 20.0 67-118920.068 U18 1,1,2-Trichloroethane
ug/L1.0 20.0 79-1411060.050 U21 1,1-Dichloroethane
ug/L1.0 20.0 75-1331130.15 U23 1,1-Dichloroethene
ug/L1.0 20.0 70-1291030.063 U21 1,1-Dichloropropene
Page 20 of 27This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 8A10011 - EPA 5030B_MS - Continued
Prepared: 01/10/2018 10:02 Analyzed: 01/10/2018 14:44Matrix Spike (8A10011-MS1) Continued
Source: CB00257-10
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 62-117961.220 1,2,3-Trichlorobenzene
ug/L1.0 20.0 58-140920.15 U18 1,2,3-Trichloropropane
ug/L1.0 20.0 59-1221080.4822 1,2,4-Trichlorobenzene
ug/L1.0 20.0 74-123910.067 U18 1,2,4-Trimethylbenzene
ug/L1.0 20.0 37-157970.48 U19 1,2-Dibromo-3-chloropropane
ug/L1.0 20.0 66-123930.42 U19 1,2-Dibromoethane
ug/L1.0 20.0 76-116970.052 U19 1,2-Dichlorobenzene
ug/L1.0 20.0 72-1511220.082 U24 1,2-Dichloroethane
ug/L1.0 20.0 78-125930.098 U19 1,2-Dichloropropane
ug/L1.0 20.0 77-129970.10 U19 1,3,5-Trimethylbenzene
ug/L1.0 20.0 76-119980.092 U20 1,3-Dichlorobenzene
ug/L1.0 20.0 60-129970.15 U19 1,3-Dichloropropane
ug/L1.0 20.0 76-122890.10 U18 1,4-Dichlorobenzene
ug/L1.0 20.0 21-1671220.12 U24 2,2-Dichloropropane
ug/L1.0 20.0 73-135950.10 U19 2-Chlorotoluene
ug/L1.0 20.0 76-134960.10 U19 4-Chlorotoluene
ug/L1.0 20.0 75-127930.066 U19 4-Isopropyltoluene
ug/L1.0 20.0 81-134940.050 U19 Benzene
ug/L1.0 20.0 72-115990.13 U20 Bromobenzene
ug/L1.0 20.0 74-1281160.11 U23 Bromochloromethane
ug/L1.0 20.0 72-1291100.10 U22 Bromodichloromethane
ug/L1.0 20.0 73-119950.20 U19 Bromoform
ug/L1.0 20.0 38-189890.28 U18 Bromomethane
ug/L1.0 20.0 68-1421090.082 U22 Carbon Tetrachloride
ug/L1.0 20.0 83-117940.069 U19 Chlorobenzene
ug/L1.0 20.0 45-213600.18 U12 Chloroethane
ug/L1.0 20.0 78-1381040.083 U21 Chloroform
ug/L1.0 20.0 56-1711080.050 U22 Chloromethane
ug/L1.0 20.0 69-120950.075 U19 cis-1,2-Dichloroethene
ug/L1.0 20.0 63-1251030.073 U21 cis-1,3-Dichloropropene
ug/L1.0 20.0 73-1171000.067 U20 Dibromochloromethane
ug/L1.0 20.0 76-124950.13 U19 Dibromomethane
ug/L1.0 20.0 25-1611190.091 U24 Dichlorodifluoromethane
ug/L1.0 20.0 68-124950.10 U19 Ethylbenzene
ug/L1.0 20.0 0-200940.35 U19 Freon 113
ug/L1.0 20.0 63-1141201.526 QM-07Hexachlorobutadiene
ug/L1.0 20.0 70-130980.21 U20 Isopropyl Ether
ug/L1.0 20.0 81-1361070.13 U21 Isopropylbenzene
ug/L2.0 40.0 79-1211050.18 U42 m,p-Xylenes
ug/L2.0 20.0 68-128980.070 U20 Methylene Chloride
ug/L1.0 20.0 10-127940.12 U19 Methyl-tert-Butyl Ether
ug/L1.0 20.0 50-127960.4620 Naphthalene
ug/L1.0 20.0 68-126960.074 U19 n-Butyl Benzene
ug/L1.0 20.0 76-125990.073 U20 n-Propyl Benzene
ug/L1.0 20.0 71-125980.088 U20 o-Xylene
ug/L1.0 20.0 75-122900.053 U18 sec-Butylbenzene
ug/L1.0 20.0 73-120950.082 U19 Styrene
ug/L1.0 20.0 70-137940.094 U19 tert-Butylbenzene
ug/L1.0 20.0 40-1811100.099 U22 Tetrachloroethene
Page 21 of 27This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 8A10011 - EPA 5030B_MS - Continued
Prepared: 01/10/2018 10:02 Analyzed: 01/10/2018 14:44Matrix Spike (8A10011-MS1) Continued
Source: CB00257-10
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 71-118970.053 U19 Toluene
ug/L1.0 20.0 75-1391010.11 U20 trans-1,2-Dichloroethene
ug/L1.0 20.0 62-152990.080 U20 trans-1,3-Dichloropropene
ug/L1.0 20.0 75-1151010.13 U20 Trichloroethene
ug/L1.0 20.0 68-1831330.15 U27 Trichlorofluoromethane
ug/L1.0 20.0 49-1501080.083 U22 Vinyl chloride
ug/L1.0 60.0 77-1211020.22 U61 Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 11055
ug/L 50.0 70-130Dibromofluoromethane10251
ug/L 50.0 70-130Toluene-d8 10351
Prepared: 01/10/2018 10:02 Analyzed: 01/10/2018 16:55Matrix Spike Dup (8A10011-MSD1)
Source: CB00257-10
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 1671-11797 40.091 U19 1,1,1,2-Tetrachloroethane
ug/L1.0 20.0 1872-14394 90.15 U19 1,1,1-Trichloroethane
ug/L1.0 20.0 1659-13393 0.90.085 U19 1,1,2,2-Tetrachloroethane
ug/L1.0 20.0 1867-11885 90.068 U17 1,1,2-Trichloroethane
ug/L1.0 20.0 1979-141102 40.050 U20 1,1-Dichloroethane
ug/L1.0 20.0 2075-133108 40.15 U22 1,1-Dichloroethene
ug/L1.0 20.0 1770-12998 50.063 U20 1,1-Dichloropropene
ug/L1.0 20.0 1762-11795 11.220 1,2,3-Trichlorobenzene
ug/L1.0 20.0 1758-14091 0.70.15 U18 1,2,3-Trichloropropane
ug/L1.0 20.0 1759-122105 20.4821 1,2,4-Trichlorobenzene
ug/L1.0 20.0 1874-12388 30.067 U18 1,2,4-Trimethylbenzene
ug/L1.0 20.0 1837-157101 40.48 U20 1,2-Dibromo-3-chloropropane
ug/L1.0 20.0 1566-12391 20.42 U18 1,2-Dibromoethane
ug/L1.0 20.0 1676-11693 40.052 U19 1,2-Dichlorobenzene
ug/L1.0 20.0 1672-151120 10.082 U24 1,2-Dichloroethane
ug/L1.0 20.0 1978-12599 60.098 U20 1,2-Dichloropropane
ug/L1.0 20.0 1677-12992 60.10 U18 1,3,5-Trimethylbenzene
ug/L1.0 20.0 1776-11987 120.092 U17 1,3-Dichlorobenzene
ug/L1.0 20.0 1660-12986 120.15 U17 1,3-Dichloropropane
ug/L1.0 20.0 1676-12283 60.10 U17 1,4-Dichlorobenzene
ug/L1.0 20.0 2021-167112 90.12 U22 2,2-Dichloropropane
ug/L1.0 20.0 1673-13585 110.10 U17 2-Chlorotoluene
ug/L1.0 20.0 1676-13491 50.10 U18 4-Chlorotoluene
ug/L1.0 20.0 1775-12790 30.066 U18 4-Isopropyltoluene
ug/L1.0 20.0 1781-13492 10.050 U18 Benzene
ug/L1.0 20.0 1772-115101 20.13 U20 Bromobenzene
ug/L1.0 20.0 1874-128110 50.11 U22 Bromochloromethane
ug/L1.0 20.0 1672-129103 60.10 U21 Bromodichloromethane
ug/L1.0 20.0 4473-11991 50.20 U18 Bromoform
ug/L1.0 20.0 2738-18974 180.28 U15 Bromomethane
ug/L1.0 20.0 1768-14298 110.082 U20 Carbon Tetrachloride
ug/L1.0 20.0 1683-11790 40.069 U18 Chlorobenzene
ug/L1.0 20.0 2645-213112 600.18 U22 QM-07Chloroethane
ug/L1.0 20.0 1778-13894 100.083 U19 Chloroform
ug/L1.0 20.0 2856-171111 30.050 U22 Chloromethane
Page 22 of 27This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 8A10011 - EPA 5030B_MS - Continued
Prepared: 01/10/2018 10:02 Analyzed: 01/10/2018 16:55Matrix Spike Dup (8A10011-MSD1) Continued
Source: CB00257-10
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 1869-12097 20.075 U19 cis-1,2-Dichloroethene
ug/L1.0 20.0 1763-12592 120.073 U18 cis-1,3-Dichloropropene
ug/L1.0 20.0 1673-11792 80.067 U18 Dibromochloromethane
ug/L1.0 20.0 1576-12499 40.13 U20 Dibromomethane
ug/L1.0 20.0 4825-161113 50.091 U23 Dichlorodifluoromethane
ug/L1.0 20.0 1668-12490 50.10 U18 Ethylbenzene
ug/L1.0 20.0 250-20092 20.35 U18 Freon 113
ug/L1.0 20.0 1963-114102 161.522 Hexachlorobutadiene
ug/L1.0 20.0 3070-13088 100.21 U18 Isopropyl Ether
ug/L1.0 20.0 1681-136101 60.13 U20 Isopropylbenzene
ug/L2.0 40.0 1679-121100 50.18 U40 m,p-Xylenes
ug/L2.0 20.0 1768-12899 10.070 U20 Methylene Chloride
ug/L1.0 20.0 2110-12792 30.12 U18 Methyl-tert-Butyl Ether
ug/L1.0 20.0 1950-12786 100.4618 Naphthalene
ug/L1.0 20.0 1568-12690 70.074 U18 n-Butyl Benzene
ug/L1.0 20.0 1676-12591 90.073 U18 n-Propyl Benzene
ug/L1.0 20.0 1571-12589 100.088 U18 o-Xylene
ug/L1.0 20.0 1775-12287 30.053 U17 sec-Butylbenzene
ug/L1.0 20.0 2373-12085 110.082 U17 Styrene
ug/L1.0 20.0 2270-13791 30.094 U18 tert-Butylbenzene
ug/L1.0 20.0 2640-181102 70.099 U20 Tetrachloroethene
ug/L1.0 20.0 1771-11890 70.053 U18 Toluene
ug/L1.0 20.0 1975-139101 0.60.11 U20 trans-1,2-Dichloroethene
ug/L1.0 20.0 1662-15298 10.080 U20 trans-1,3-Dichloropropene
ug/L1.0 20.0 1875-11595 60.13 U19 Trichloroethene
ug/L1.0 20.0 2268-183115 140.15 U23 Trichlorofluoromethane
ug/L1.0 20.0 2749-150104 40.083 U21 Vinyl chloride
ug/L1.0 60.0 1677-12196 60.22 U58 Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 10653
ug/L 50.0 70-130Dibromofluoromethane9950
ug/L 50.0 70-130Toluene-d8 10251
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 8A10004 - EPA 3005A
Prepared: 01/10/2018 08:20 Analyzed: 01/15/2018 10:14Blank (8A10004-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L50.022.0 U Iron
Prepared: 01/10/2018 08:20 Analyzed: 01/15/2018 10:17Blank (8A10004-BLK2)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L50.022.0 U Iron
Prepared: 01/10/2018 08:20 Analyzed: 01/15/2018 10:20LCS (8A10004-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
Page 23 of 27This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 8A10004 - EPA 3005A - Continued
Prepared: 01/10/2018 08:20 Analyzed: 01/15/2018 10:20LCS (8A10004-BS1) Continued
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L50.0 1000 80-1201021020 Iron
Prepared: 01/10/2018 08:20 Analyzed: 01/15/2018 10:26Matrix Spike (8A10004-MS1)
Source: CA16482-01
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L50.0 1000 75-1251045921630 Iron
Prepared: 01/10/2018 08:20 Analyzed: 01/15/2018 10:39Matrix Spike Dup (8A10004-MSD1)
Source: CA16482-01
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L50.0 1000 2075-12595 55921550 Iron
Prepared: 01/10/2018 08:20 Analyzed: 01/15/2018 10:41Post Spike (8A10004-PS1)
Source: CA16482-01
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L0.0500 1.00 80-1201130.5921.72 Iron
Metals (acid extractable) by EPA 6000/7000 Series Methods - Quality Control
Batch 8A10007 - SM18 3030C
Prepared: 01/10/2018 09:12 Analyzed: 01/15/2018 12:58Blank (8A10007-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L10.03.10 U Lead
Prepared: 01/10/2018 09:12 Analyzed: 01/15/2018 13:01LCS (8A10007-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L10.0 200 80-120111222 Lead
Prepared: 01/10/2018 09:12 Analyzed: 01/15/2018 13:14Matrix Spike (8A10007-MS1)
Source: CA19202-01
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L10.0 200 75-12510623.0236 Lead
Prepared: 01/10/2018 09:12 Analyzed: 01/15/2018 13:16Matrix Spike Dup (8A10007-MSD1)
Source: CA19202-01
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L10.0 200 2075-125110 323.0243 Lead
Prepared: 01/10/2018 09:12 Analyzed: 01/15/2018 13:18Post Spike (8A10007-PS1)
Source: CA19202-01
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L0.00935 0.200 80-1201000.02300.223 Lead
Classical Chemistry Parameters - Quality Control
Page 24 of 27This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 8A11033 - NO PREP
Prepared: 01/11/2018 14:37 Analyzed: 01/11/2018 15:41Blank (8A11033-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L5.02.9 U Sulfate as SO4
Prepared: 01/11/2018 14:37 Analyzed: 01/11/2018 15:55LCS (8A11033-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L5.0 50.0 90-1109548 Sulfate as SO4
Prepared: 01/11/2018 14:37 Analyzed: 01/12/2018 09:47Matrix Spike (8A11033-MS1)
Source: CB00238-02RE2
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L20 80.0 90-110922195 Sulfate as SO4
Prepared: 01/11/2018 14:37 Analyzed: 01/11/2018 16:38Matrix Spike (8A11033-MS2)
Source: CA18745-01
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L5.0 20.0 90-110951432 Sulfate as SO4
Prepared: 01/11/2018 14:37 Analyzed: 01/12/2018 10:01Matrix Spike Dup (8A11033-MSD1)
Source: CB00238-02RE2
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
mg/L20 80.0 1090-11092 0.72194 Sulfate as SO4
Page 25 of 27This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL
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FLAGS/NOTES AND DEFINITIONS
The sample was analyzed at dilution.
The analyte was detected in the associated method blank.
The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
MRL
E
U
J
D
B
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
PQL: Practical Quantitation Limit.PQL
The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was
accepted based on acceptable LCS recovery.
QM-07
The associated continuing calibration verification standard exhibited high bias; since the result is
ND, there is no impact.
QV-01
The Reporting Limit for this analyte has been raised to account for matrix interference.R-01
Page 26 of 27This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL