3412_Forsyth_OldSalisburyRoad_CDLF_GWSupplement_FID1087987_20171218

ASSESSMENT
MONITORING
REPORT

Supplement to the December 2017
Groundwater Sampling Event
Old Salisbury Road Landfill
NCDEQ Permit NO. 34-12
HDR Project No. 10066253
Forsyth County, North Carolina
January 2018

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Winston-Salem City/County Utilities | Supplement to the Assessment Monitoring Report Table of Contents
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Table of Contents
Table of Contents ........................................................................................................................... i
List of Tables .......................................................................................................................... i
List of Figures ......................................................................................................................... i
Appendices ............................................................................................................................ ii
List of Acronyms .................................................................................................................... ii
1.0 Purpose .............................................................................................................................. 1
2.0 General .............................................................................................................................. 1
2.1. Facility Background ........................................................................................................ 1
2.2. Regulatory Authority ....................................................................................................... 1
2.3. Assessment Monitoring .................................................................................................. 1
3.0 Monitoring Plan .................................................................................................................. 3
4.0 Data Collection ................................................................................................................... 5
5.0 Results ............................................................................................................................... 5
5.1. Detected Groundwater Constituents .............................................................................. 5
6.0 Summary & Recommendations ......................................................................................... 6

List of Tables
Table 1 - Existing Groundwater Monitoring Well Details ............................................................... 3
Table 2 - Sampling Schedule ........................................................................................................ 4
Table 3 - Parameters Tested by Method - December 2017 .......................................................... 4
Table 4 - Event Summary – December 2017 ................................................................................ 7

List of Figures
Figure 1 - Groundwater Contours and Sample Locations – November 2017 ............................... 2
Figure 2 - Selected Groundwater Detections in MW-2R ............................................................... 5

Winston-Salem City/County Utilities | Supplement to the Assessment Monitoring Report Table of Contents
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Appendices
Appendix A – Summary of Groundwater Monitoring Results
Appendix B – Laboratory Groundwater Report
Appendix C – Field Data
Appendix D – Electronic Files

List of Acronyms
2L 15A NCAC Subchapter 02L - Groundwater Classification and Standards
µg/L micrograms per liter
EPA United States Environmental Protection Agency
MCL Maximum Contaminant Level
MDL method detction limit
NC DENR North Carolina Department of Environment and Natural Resources1
NCDEQ North Carolina Department of Environmental Quality1
ND not detected in sample
NE standard not established
NS not sampled
NTU Nephelometric turbidity units
PCB polychlorinated biphenyl
PCE tetrachloroethene
PRL practical reporting limit
PVC polyvinyl chloride
SWSL solid waste section limits
SVOC semi-volatile organic compound
VOC volatile organic compound
USGS U.S. Geological Survey
1Prior to September 18, 2015, the NCDEQ was referred to as the NC DENR. Both naming conventions are used in this report, as appropriate.

Winston-Salem City/County Utilities | Supplement to the Assessment Monitoring Report Purpose
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1.0 Purpose
This document supplements the Assessment Monitoring Report dated January 4, 2018 with the
additional data acquired from the December 2017 monitoring event. The current assessment
plan requires all wells to be tested for the complete set of Appendix II parameters every two
years. The wells were sampled for semiannual subset of Appendix II constituents during the
November event. The December event provides the balance of the Appendix II constituents and
repeated some of the Appendix I constituents. This document reports the results of the
December Appendix II testing.
2.0 General
HDR Engineering, Inc. of the Carolinas (HDR), on behalf of the Winston-Salem City/County
Utility Commission (the City), is hereby submitting assessment monitoring results for
groundwater at the Old Salisbury Road C&D Landfill (OSR) located in Forsyth County, North
Carolina. These results supplement those presented in the Assessment Monitoring Report
dated January 4, 2018.
2.1. Facility Background
The OSR landfill covers approximately 56 acres and is situated within a 140-acre tract north of
Friedberg Church Road and west of Old Salisbury Road in Forsyth County, North Carolina. The
site is accessed via Old Salisbury Road (State Road 3011). The Forsyth/Davidson County line
borders the site to the south. Figure 1 illustrates the location of the OSR landfill. The facility was
originally issued a permit to operate on July 3, 1996 and opened in August of the same year.
2.2. Regulatory Authority
The site is currently operated under NC DENR facility permit number 34-12 dated April 6, 2015
(DIN 23258). The groundwater monitoring and reporting requirements are addressed in items
36 to 45 of the permit. NC Solid Waste Management Rules 15A NCAC 13B .0544(b) and
.0544(c) define the requirements for the site’s groundwater and surface water monitoring plans,
respectively. The current Groundwater Monitoring Plan was approved as noted, by NC DENR
on March 5, 2015 (DIN 23910).
2.3. Assessment Monitoring
The site is currently in assessment monitoring. Assessment monitoring is being conducted to
address the detection of benzene and tetrachloroethene (PCE) above the groundwater
monitoring standards in groundwater monitoring well MW-2R that were initially detected during
the May 2011 and June 2011 events. The approved Assessment Monitoring Plan for MW-2R
can be summarized as follows.
• Groundwater monitoring wells MW-1R, MW-2R, MW-4R and MW-15 will be sampled
semiannually for the previously detected Appendix II constituents, in addition to
Appendix I constituents; and
FORSYTH COUNTY
DAVIDSON COUNTY FORSYTH COUNTY
DAVIDSON COUNTY
V
IV
VI
III
II
I
SHEET TITLE
PROJECT TITLE
PROJECT MANAGER
DATE
PROJECT NUMBER
REFERENCE DOCUMENT
EXHIBIT NUMBER
REFERENCE SHEET
SHEET TITLE
PROJECT TITLE
GROUNDWATER CONTOURS
AND SAMPLE LOCATIONS
FALL 2017
Winston-Salem City/County Utilities | Supplement to the Assessment Monitoring Report Monitoring Plan
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• All groundwater monitoring wells will be sampled during every other Fall event (odd
years) for the entire Appendix II constituent list.
• Additional Appendix II constituents detected will be added to the sampling program for
subsequent semiannual events.
3.0 Monitoring Plan
Sampling occurs semiannually for the site monitoring wells and four surface water monitoring
locations. The groundwater monitoring locations are depicted on Figure 1. Table 1 provides
location and construction details for the existing monitoring wells.
Groundwater monitoring well MW-1R is located hydraulically upgradient of the landfill and is
considered as the background well for the site. Upstream surface water (SW-1) and
downstream surface water (SW-2) samples are obtained from the adjacent stream to the east.
Surface water samples (SW-3 and SW-4) are obtained from the drainage channel in the vicinity
of MW-2R. SW-3 is located south of the entrance road near MW-2R; SW-4 is located on the
north side of the entrance road, downstream of SW-3.
Table 1 - Existing Groundwater Monitoring Well Details

The monitoring program consists of collection and analysis of groundwater samples from 14
wells. The sampling event occurred over two days (December 28-29, 2017). Pace Analytical
Laboratories, Inc. (Pace) of Huntersville, North Carolina (NC Cert. # 5342), on behalf of HDR,
sampled the groundwater monitoring wells for this report. Synoptic groundwater elevations were
not measured for this event.
The sampled locations were evaluated by the methods and for the analytical parameters listed
in Table 2 for the Appendix II parameters not sampled for at all wells during the November 2017
event. The wells were resampled for the missing parameters on December 28 & 29, 2017. This
report presents the results of the December sampling. See Table 3.

OSR LF
WELL Installed
NC Sate
Plane
Northing
NC Sate
Plane
Easting
Well
Diameter
(inches)
Well
Depth
(below
ground)
Depth:
Ground to
Top of
Screen
Screened
Interval
(ft)
Screened Interval
Geology
Top Of
Casing
Elevation
(ft MSL)
Ground
Elevation
(ft MSL)
MW-1R 12/27/1995 820,411 1,622,983 2 60.0 45 15 Granitic saprolite 836.42 833.40MW-2R 12/29/1995 820,974 1,622,722 2 23.0 8 15 Granitic saprolite 785.22 781.81MW-3R 7/7/1999 821,237 1,621,463 2 27.0 12 15 Granitic saprolite 776.60 772.90MW-4R 12/28/1995 820,435 1,621,428 2 20.0 5 15 Granitic saprolite 767.96 765.70MW-5R 12/29/1995 820,137 1,622,130 2 32.0 17 15 Granitic saprolite 784.36 782.30MW-7 12/28/1995 820,886 1,621,424 2 48.0 33 15 Granitic saprolite 803.66 802.10MW-8 7/7/1999 821,930 1,621,485 2 27.0 12 15 Granitic saprolite 762.50 759.80MW-9 8/11/2004 822,311 1,621,986 2 60.0 45 15 Sand 790.28 788.04
MW-10 8/10/2004 822,626 1,622,699 2 21.0 6 15 Sand 738.21 735.70MW-11 8/10/2004 822,307 1,622,838 2 20.0 5 15 Sand 732.59 730.35MW-12 8/9/2004 821,844 1,622,955 2 16.0 6 10 Silt 739.07 736.41
MW-13 8/9/2004 821,500 1,622,915 2 20.0 5 15 Sand 751.23 749.19MW-14 8/11/2004 822,420 1,622,260 2 60.0 45 15 Sand 783.88 781.44MW-15 4/6/2012 821,083 1,622,884 2 48.2 33.2 15 Bedrock 802.85 800.58
Winston-Salem City/County Utilities | Supplement to the Assessment Monitoring Report Monitoring Plan
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Table 2 - Sampling Schedule
Method Parameter(s) Frequency Monitoring Wells Surface Water
EPA 300.0 Sulfate 2x/year All All
EPA 6010 Trace Metals 2x/year All All
EPA 7470 Mercury 2x/year All All
EPA 8081
Pesticides Fall of odd years (2017) All None
4,4'-DDD, 4,4'-DDT, Aldrin, alpha-BHC, delta-BHC, Endosulfan I, Endosulfan II, Endrin, Endrin aldehyde, Heptachlor, Heptachlor epoxide & Methoxychlor
(Pesticides previously detected)
2x/year MW-1R, MW-2R, MW-4, MW-7, MW-10 & MW-15 None
EPA 8082 PCB’s Fall of odd years (2017) All None
EPA 8151
Herbicides Fall of odd years (2017) All None
2,4,5-TP (Silvex), 2,4-D
(Herbicides previously detected) 2x/year MW-1R, MW-2R, MW-4R & MW-15 None
EPA 8260
App I VOCs + Tetrahydrofuran 2x/year All All
Appendix II VOCs Fall of odd years (2017) All None
Dichlorodifluoromethane
(Appendix II VOC
previously detected)
2x/year All None
EPA 8270
SVOCs Fall of odd years (2017) All None
Benzo(a)anthracene, Bis(2-ethylhexyl)phthalate, Chrysene Dibenz(a,h)anthracene &
Indeno(1,2,3-cd)pyrene
(SVOCs previously detected)
2x/year MW-1R, MW-2R, MW-4R , MW-3R & MW-15 SW-2
SM 2320B Alkalinity 2x/year All All
SM 2540C Total Dissolved Solids 2x/year All All
SM 4500 Chloride, Cyanide, Sulfide 2x/year All All
Field Temperature, Specific conductance, Dissolved Oxygen, Redox, Turbidity, pH 2x/year All All
Field Total well depth and static water level 2x/year All NA

Table 3 - Parameters Tested by Method - December 2017

Method
MW-1R MW-2R MW-3R MW-4R MW-5R MW-7 MW-8 MW-9
MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-2
Equipment Blank Trip Blank
EPA 8081 19 19 19 19 19 19 19 19 19 19 19 19 19 19 19EPA 8082 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7
EPA 8151A 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4
EPA 8260 67 67 67 67 67 67 67 67 67 67 67 67 67 67 67 67 67EPA 8270 105 105 105 105 105 105 105 105 105 105 105 105 105 105 105 105
Field 8 8 8 8 8 8 8 8 8 8 8 8 8 8 6
Winston-Salem City/County Utilities | Supplement to the Assessment Monitoring Report Data Collection
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4.0 Data Collection
Samples were collected from each of the landfill groundwater wells using the dedicated QEDTM
MicroPurge ® pumps that were installed in August 2004, except at MW-15, which is sampled
with a bailer.
A variable speed micro-purge pump (or bailer in the case of MW-15) was used to purge
groundwater from each well until stabilization of measured field parameters (pH, conductivity,
redox, temperature, turbidity, and dissolved oxygen) occurred. Following completion of purging
activities, the wells were sampled using the same pump and field parameters (pH, specific
conductance, redox, turbidity, dissolved oxygen, and temperature) were recorded on field
sampling logs. Copies of these logs are provided in Appendix C.
5.0 Results
No Appendix II constituents were detected above the PRL.
5.1. Detected Groundwater Constituents
Detections of benzene and PCE above the groundwater standards triggered assessment
monitoring for well MW-2R. The trends of selected containments detected in MW-2R above the
SWSL are shown on Figure 2.
Figure 2 - Selected Groundwater Detections in MW-2R
0.1
1
10
100
1000
10000
100000
1000000
1-Jan-09 1-Jan-10 1-Jan-11 1-Jan-12 1-Jan-13 1-Jan-14 1-Jan-15 1-Jan-16 1-Jan-17 1-Jan-18 1-Jan-19Detected Concentration (ug/L)Date Sample Collected
MW-2R Groundwater DetectionsOSR Construction & Demolition Landfill Permit 34-12
Total Dissolved Solids
Sulfate
Chloride
Manganese
Iron
Barium
Selenium
Lead
Chromium
Benzene
Tetrachloroethene
Vinyl chloride
Methylene Chloride
bis(2-Ethylhexyl)phthalate
Heptachlor
delta-BHC
Chloromethane
alpha-BHC
4,4'-DDT
Winston-Salem City/County Utilities | Supplement to the Assessment Monitoring Report Summary & Recommendations
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A summary of the constituents detected during this period, along with the NCDEQ solid waste
section limits (SWSL) and applicable North Carolina state maximum concentration levels, are
provided in Table 4. There were thirteen detections above the PRL; they were all Appendix I
constituents. Four were above the 2L standard, five were above the NC SWSL but below the 2L
standard, and four were detected on constituents without standards.
Appendix A contains historical summaries of Appendix II detections by parameter. The complete
laboratory analyses are provided in Appendix B. A Microsoft Excel file containing the analysis
data in NCDEQ electronic data deliverable format is include as part of Appendix D.
The constituents detected above 2L groundwater standards for this event are as follows.
• Appendix I constituents
o Benzene in MW-2R
o Tetrachloroethene in MW-2R
o Vinyl Chloride in MW-2R
o Methylene Chloride in MW-7
• All SVOCs, herbicides and pesticides were non detect or below the PRL during this
sampling event.
6.0 Summary & Recommendations
The results of the analysis reported in this supplement are not significantly different than the
results reported for the November 2017 data. No Appendix II constituents were detected above
the PRL.
The full round of Appendix II parameters were not sampled for at all wells during the November
2017 event. The wells were resampled for the missing parameters on December 28 & 29, 2017.
The results of the December sampling indicate no new Appendix II constituents need to be
added to the semiannual sampling events.
The level of detections from this event are generally consistent with previous events. No
Appendix II constituents have been detected above the 2L standard since the November 2016
event. The two herbicides detected in November, were below the SWSL. No pesticides or semi-
volatile organic compounds were detected in 2017. The pesticides, heptachlor and heptachlor
epoxide that were last detected during the November 2016 sampling event, and were not
detected in the December 2017 event.
Table 4 depicts a summary of exceedances and field parameters for the December 2017
Sampling Event.

Winston-Salem City/County Utilities | Supplement to the Assessment Monitoring Report Summary & Recommendations

Table 4 - Event Summary – December 2017

Note - To distinguish non detections (ND) from not sampled (NS), refer to complete laboratory analysis. This table represents both ND and NS as blanks.

Standard Max
SWSL 2L units MW-1R MW-2R MW-3R MW-4R MW-5R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-2
EPA 8260
µg/L
1 1 µg/L Benzene 2.5
1 5 µg/L Methylene Chloride 1.1 5.7
NE NE µg/L o-Xylene 1.1
1 0.7 µg/L Tetrachloroethene 1.5
NE NE µg/L Tetrahydrofuran 59.1 135 61.3
1 3 µg/L Trichloroethene 1.3
1 2000 µg/L Trichlorofluoromethane 1.6 1.4 1.4
1 0.03 µg/L Vinyl chloride 1.4
Field
°C
Field Temperature 11.7 5.7 7.7 11.8 11.4 9.9 6.7 11 11.7 12.5 11.2 11.2 9.9 8.2 3.2
µmhos/cm
Field Specific Conductance 214.6 1320 383.6 1140 175.1 236.6 75.2 148.6 1873 329.2 308.6 111.4 169.2 832 783.6
mg/L
Oxygen, Dissolved 3.3 0.4 0.5 0.6 5.1 1 4.5 6.2 0.1 0.1 0.3 1.3 2.9 2.3 2.4
mV
REDOX 112.4 -38.8 -37.4 100.2 106.5 78.2 169.8 132.7 -50.6 -43.9 163.2 216.5 150.5 105.1 -68.9
NTU
Turbidity 2.8 2.4 9.4 9.6 4.2 3.5 9.7 9.6 7.8 9.8 9.7 9.7 7.4 2.7 554.5
Std. Units
Field pH 5.6 6.4 6.4 6.1 6.1 5.6 5.7 5.7 6.4 6.1 6 5.8 5.6 6.1 6.8
feet
Static Water Level 35.1 8.3 21.15 9.44 11.5 37 18.55 52.94 12.18 4.14 5.46 9.09 52.09 39.58
Total Well Depth 60 21 27 20 50 48 27 60 21 20 15.7 20 60 48
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Winston-Salem City/County Utilities | Supplement to the Assessment Monitoring Report
Appendix A – Summary of Groundwater Monitoring Results

A
Appendix A – Summary of
Groundwater Monitoring Results

A-1 Appendix II Detections (9 pages)

Winston-Salem City/County Utilities | Supplement to the Assessment Monitoring Report Appendix A – Summary of Groundwater Monitoring Results

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A1Facility Permit 34-12Old Salisbury Road Landfill (C&D)OSR Concern (Multiple ItemSelected groundwater detections of concern within the last 6 yearsQualifier (Multiple ItemHighlighted cells are at or above the current standardValueColumn LabelsSWSL2L Row LabelsDec-17Nov-17Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12Apr-12Mar-12Dec-11Nov-11Jun-11Herbicides2 50 µg/L 2,4,5-TP (Silvex)2 50 µg/L MW-2R 0.072 0.14 0.232 70 µg/L 2,4-D2 70 µg/L MW-2R 0.43 1.12 70 µg/L MW-15 0.2725 0.3 µg/L Pentachlorophenol25 0.3 µg/L Equipment Blank 0.018Pesticides0.1 0.1 µg/L 4,4'-DDD0.1 0.1 µg/L MW-70.130.1 0.1 µg/L MW-150.0620.1 0.1 µg/L SW-30.0790.1 0.1 µg/L SW-40.110.060.1 0.1 µg/L 4,4'-DDT0.1 0.1 µg/L MW-2R0.540.1 0.1 µg/L MW-4R0.140.1 0.1 µg/L MW-110.050.1 0.1 µg/L SW-30.090.1 0.1 µg/L SW-40.050.05 2 µg/L Aldrin0.05 2 µg/L MW-2R0.120.05 0.006 µg/L alpha-BHC0.05 0.006 µg/L MW-2R0.120.05 0.019 µg/L beta-BHC0.05 0.019 µg/L MW-70.10.05 0.019 µg/L delta-BHC0.05 0.019 µg/L MW-2R0.180.05 0.019 µg/L MW-4R0.070.002 0.002 µg/L Dieldrin0.002 0.002 µg/L MW-70.11 0.08MCLc:\pwworking\tpa\d0269489\W-S GW Revised.xlsb1 of 9
A1Facility Permit 34-12Old Salisbury Road Landfill (C&D)OSR Concern (Multiple ItemSelected groundwater detections of concern within the last 6 yearsQualifier (Multiple ItemHighlighted cells are at or above the current standardValueColumn LabelsSWSL2L Row LabelsDec-17Nov-17Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12Apr-12Mar-12Dec-11Nov-11Jun-11MCL0.1 40 µg/L Endosulfan I0.1 40 µg/L MW-7 0.150.1 40 µg/L MW-10 0.170.1 42 µg/L Endosulfan II0.1 42 µg/L MW-4R0.120.1 42 µg/L SW-30.071 0.090.1 42 µg/L SW-40.070.1 2 µg/L Endrin0.1 2 µg/L MW-2R0.270.1 2 µg/L SW-10.080.1 2 µg/L Endrin aldehyde0.1 2 µg/L MW-2R0.23 0.280.1 2 µg/L SW-40.060.05 0.008 µg/L Heptachlor0.05 0.008 µg/L MW-2R0.480.05 0.008 µg/L MW-100.21 0.120.075 0.004 µg/L Heptachlor epoxide0.075 0.004 µg/L MW-70.12 0.070.075 0.004 µg/L MW-100.17 0.0931 40 µg/L Methoxychlor1 40 µg/L MW-2R0.83SemiVOCs10 NE µg/L 2,4-Dinitrotoluene10 NE µg/L MW-2R 5.910 NE µg/L 2,6-Dinitrotoluene10 NE µg/L MW-2R 8.110 40 µg/L 3&4-Methylphenol(m&p Cresol)10 40 µg/L SW-33.620 NE µg/L 3,3'-Dichlorobenzidine20 NE µg/L SW-23.610 NE µg/L 3-Methylcholanthrene10 NE µg/L SW-22.9c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb2 of 9
A1Facility Permit 34-12Old Salisbury Road Landfill (C&D)OSR Concern (Multiple ItemSelected groundwater detections of concern within the last 6 yearsQualifier (Multiple ItemHighlighted cells are at or above the current standardValueColumn LabelsSWSL2L Row LabelsDec-17Nov-17Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12Apr-12Mar-12Dec-11Nov-11Jun-11MCL10 0.05 µg/L Benzo(a)anthracene10 0.05 µg/L MW-1R1.410 0.05 µg/L SW-21.110 0.005 µg/L Benzo(a)pyrene10 0.005 µg/L MW-131.110 0.005 µg/L SW-22.510 0.05 µg/L Benzo(b)fluoranthene10 0.05 µg/L MW-13110 0.05 µg/L SW-22.810 200 µg/L Benzo(g,h,i)perylene10 200 µg/L MW-3R 110 200 µg/L MW-111.310 200 µg/L MW-121.210 200 µg/L MW-131.510 200 µg/L SW-21.810 0.5 µg/L Benzo(k)fluoranthene10 0.5 µg/L SW-22.515 3 µg/L bis(2-Ethylhexyl)phthalate15 3 µg/L MW-1R2.415 3 µg/L MW-2R1.115 3 µg/L MW-3R5.515 3 µg/L MW-5R115 3 µg/L MW-91315 3 µg/L MW-149.815 3 µg/L SW-21.1#N/A #N/A #N/A Butylbenzylphthalate#N/A #N/A #N/A MW-4R 1.710 5 µg/L Chrysene10 5 µg/L MW-1R1.510 5 µg/L SW-21.1c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb3 of 9
A1Facility Permit 34-12Old Salisbury Road Landfill (C&D)OSR Concern (Multiple ItemSelected groundwater detections of concern within the last 6 yearsQualifier (Multiple ItemHighlighted cells are at or above the current standardValueColumn LabelsSWSL2L Row LabelsDec-17Nov-17Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12Apr-12Mar-12Dec-11Nov-11Jun-11MCL10 0.005 µg/L Dibenz(a,h)anthracene10 0.005 µg/L MW-3R110 0.005 µg/L MW-131.210 0.005 µg/L SW-22.110 100 µg/L Di-n-octylphthalate10 100 µg/L MW-8 5.610 100 µg/L MW-12 5.610 0.05 µg/L Indeno(1,2,3-cd)pyrene10 0.05 µg/L MW-3R1.110 0.05 µg/L MW-121.210 0.05 µg/L MW-131.510 0.05 µg/L SW-22.2VOCs1 200 µg/L 1,1,1-Trichloroethane1 200 µg/L MW-75 6 µg/L 1,1-Dichloroethane5 6 µg/L MW-2R 0.54 0.48 0.48 0.53 0.49 1.1 0.83 1.3 1.2 1.2 1.1 1.25 6 µg/L MW-7 1.6 1.4 1.3 1.5 1.2 0.91 1.1 1.3 0.81 0.9 0.84 1.2 1.2 1.95 350 µg/L 1,1-Dichloroethene5 350 µg/L MW-2R36.6 395 350 µg/L MW-135 350 µg/L MW-153.15 350 µg/L SW-40.581 0.4 µg/L 1,2-Dichloroethane1 0.4 µg/L MW-2R 0.241 6 µg/L 1,4-Dichlorobenzene1 6 µg/L MW-2R 0.37 0.46 0.39 0.38 0.4100 4000 µg/L 2-Butanone (MEK)100 4000 µg/L Equipment Blank100 4000 µg/L MW-2Rc:\pwworking\tpa\d0269489\W-S GW Revised.xlsb4 of 9
A1Facility Permit 34-12Old Salisbury Road Landfill (C&D)OSR Concern (Multiple ItemSelected groundwater detections of concern within the last 6 yearsQualifier (Multiple ItemHighlighted cells are at or above the current standardValueColumn LabelsSWSL2L Row LabelsDec-17Nov-17Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12Apr-12Mar-12Dec-11Nov-11Jun-11MCL50 NE µg/L 2-Hexanone50 NE µg/L MW-2R0.4850 NE µg/L MW-10 0.69 0.9650 NE µg/L SW-2 1.850 NE µg/L SW-4 3.1100 NE µg/L 4-Methyl-2-pentanone (MIBK)100 NE µg/L MW-10 1.1 2.8 2.5 2.6 5.6 2.2100 6000 µg/L Acetone100 6000 µg/L Equipment Blank 18.35.5100 6000 µg/L GP-B-1 (12-16)3.6100 6000 µg/L MW-2R 10.3 20.3 3.7100 6000 µg/L MW-3R 21.4100 6000 µg/L MW-4R 11100 6000 µg/L MW-5R 18.4100 6000 µg/L MW-7 15.7100 6000 µg/L MW-8 15.8100 6000 µg/L MW-10 13.7 12.1 22.5 14.1 11.8100 6000 µg/L MW-11 21.1100 6000 µg/L MW-12 12.1100 6000 µg/L MW-13 17.3100 6000 µg/L MW-14 14.7100 6000 µg/L MW-15 13.2100 6000 µg/L SW-1 11.22.2100 6000 µg/L SW-2 12.94100 6000 µg/L SW-3 16.2100 6000 µg/L SW-4 161 1 µg/L Benzene1 1 µg/L MW-2R2.5 2.6 2.1 2.2 1.7 1.5 1.7 2.5 1.8 1.9 1.4 1.3 1.5 2 1.61 1 µg/L MW-4R 0.38 0.42 0.28 0.271 1 µg/L MW-7 0.39 0.38 0.43 0.42 0.26 0.291 1 µg/L MW-10 0.57 0.52 0.83 0.46 0.441 1 µg/L SW-3 0.42 0.54 0.32 0.88 0.34 0.25c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb5 of 9
A1Facility Permit 34-12Old Salisbury Road Landfill (C&D)OSR Concern (Multiple ItemSelected groundwater detections of concern within the last 6 yearsQualifier (Multiple ItemHighlighted cells are at or above the current standardValueColumn LabelsSWSL2L Row LabelsDec-17Nov-17Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12Apr-12Mar-12Dec-11Nov-11Jun-11MCL100 700 µg/L Carbon Disulfide100 700 µg/L MW-1R100 700 µg/L MW-3R100 700 µg/L MW-5R100 700 µg/L MW-7100 700 µg/L MW-10 2.1 2 5.210 3000 µg/L Chloroethane10 3000 µg/L MW-2R 2.110 3000 µg/L MW-71.35 70 µg/L Chloroform5 70 µg/L GP-B-1 (12-16)0.985 70 µg/L MW-2R0.16 0.35 70 µg/L MW-15 0.44 0.44 0.4 0.44 0.7 0.44 0.26 0.49 0.77 0.63 0.49 1.45 70 µg/L SW-40.971 3 µg/L Chloromethane1 3 µg/L MW-2R 0.251 3 µg/L MW-4R1 3 µg/L MW-5R1 3 µg/L MW-7 0.131 3 µg/L MW-11 0.231 3 µg/L MW-121 3 µg/L MW-141 3 µg/L SW-2 0.125 70 µg/L cis-1,2-Dichloroethene5 70 µg/L MW-1R 0.76 0.62 0.38 0.25 70 µg/L MW-2R 0.66 0.6 0.51 0.47 0.26 0.5 0.38 0.41 0.26 0.25 0.33 0.55 70 µg/L MW-7 1.1 1.1 1.1 1.1 0.77 0.8 0.73 0.73 0.37 0.54 0.72 0.62 0.5 0.75 70 µg/L MW-10 0.27 0.23 0.2 0.33 0.355 70 µg/L MW-12 0.235 70 µg/L SW-2 0.335 70 µg/L SW-3 0.26c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb6 of 9
A1Facility Permit 34-12Old Salisbury Road Landfill (C&D)OSR Concern (Multiple ItemSelected groundwater detections of concern within the last 6 yearsQualifier (Multiple ItemHighlighted cells are at or above the current standardValueColumn LabelsSWSL2L Row LabelsDec-17Nov-17Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12Apr-12Mar-12Dec-11Nov-11Jun-11MCL5 1000 µg/L Dichlorodifluoromethane5 1000 µg/L MW-2R 0.265 1000 µg/L MW-7 0.62 15 1000 µg/L MW-9 1.7 1.2 1.5 0.88 0.76 0.28 0.285 1000 µg/L MW-12 0.235 1000 µg/L MW-14 3.6 3.9 3.6 2.3 3.6 2.11 600 µg/L Ethylbenzene1 600 µg/L MW-1R 0.381 600 µg/L MW-10 0.41 0.53 0.55 0.4 1 0.735 500 µg/L m&p-Xylene5 500 µg/L MW-2R0.75 500 µg/L MW-7 1.6 1.4 1.2 2.2 1.8 0.84 1.5 1.1 0.965 500 µg/L MW-10 1.3 1.1 1.2 2.1 0.68 1.2 1.11 5 µg/L Methylene Chloride1 5 µg/L Equipment Blank61.1 1.8 3.21 5 µg/L MW-1R 2.31 5 µg/L MW-2R 1.1 4.4 1.3 2.3 3.7 3.7 3 4.2 4.5 3.2 3.51 5 µg/L MW-3R 3.4 2.31 5 µg/L MW-4R 2.91 5 µg/L MW-5R 3.21 5 µg/L MW-75.74.6 3.1 4.2 3.79.53.9 2.1 2.91 5 µg/L MW-8 1.11 5 µg/L MW-10 2.8 1.21 5 µg/L MW-11 1.41 5 µg/L MW-12 2 21 5 µg/L MW-14 1.61 5 µg/L MW-15 2.41 5 µg/L SW-1 21 5 µg/L SW-2 3.11 5 µg/L SW-3 11 5 µg/L SW-4 1.210 6 µg/L Naphthalene10 6 µg/L MW-2R0.86 1.3 1.6 1.9c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb7 of 9
A1Facility Permit 34-12Old Salisbury Road Landfill (C&D)OSR Concern (Multiple ItemSelected groundwater detections of concern within the last 6 yearsQualifier (Multiple ItemHighlighted cells are at or above the current standardValueColumn LabelsSWSL2L Row LabelsDec-17Nov-17Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12Apr-12Mar-12Dec-11Nov-11Jun-11MCLNE NE µg/L o-XyleneNE NE µg/L MW-2R 0.33 0.31 0.54 0.54 0.63 1 1.2NE NE µg/L MW-7 0.62 0.68 0.46 0.63 0.47 0.27 0.4 0.36 0.27NE NE µg/L MW-10 1.1 0.97 1 2.1 0.43 0.85 0.651 0.7 µg/L Tetrachloroethene1 0.7 µg/L MW-2R1.5 1.8 1.8 1.3 0.95 1.2 2 1.8 2.2 1.5 1.8 1.7 1.8 1.61 0.7 µg/L MW-7 0.481 0.7 µg/L MW-14 0.61NE NE µg/L TetrahydrofuranNE NE µg/L Equipment Blank3.2NE NE µg/L MW-2R 59.1 28 36.3 39.1 49.6 35.8 34.6 79.2 72.6 99.6 111 93.2 152197 274NE NE µg/L MW-4R9.3 13.6 3.5 7 5.8 15.9 11.8 11.7 8.5 13.5 8.8NE NE µg/L MW-720.132 21.7 13.5 17.7 14.1 8.8 5.2 13.7 24.2 26 18.9NE NE µg/L MW-10 135 131 182 237 6.1 120 145 106 18.6 5NE NE µg/L MW-114.54.4NE NE µg/L MW-1211.4 26.8 12.4NE NE µg/L MW-13NE NE µg/L MW-1512 16.8 27.3 19.8 16.9 15.5 21.4 14.7 7.4 6.3NE NE µg/L SW-2 61.318.4NE NE µg/L SW-36.33.3 10.2 9.7 18.9 5.1 4.8 4.5NE NE µg/L SW-43.5 3.64.1 4.41 600 µg/L Toluene1 600 µg/L MW-1R1 600 µg/L MW-2R0.271 600 µg/L MW-10 0.35 0.270.631 600 µg/L SW-20.521 3 µg/L Trichloroethene1 3 µg/L MW-1R 0.651 3 µg/L MW-2R 1.3 0.93 1 1.2 0.71 0.66 0.79 0.85 0.71 0.89 0.68 0.77 0.820.91 3 µg/L MW-7 0.58c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb8 of 9
A1Facility Permit 34-12Old Salisbury Road Landfill (C&D)OSR Concern (Multiple ItemSelected groundwater detections of concern within the last 6 yearsQualifier (Multiple ItemHighlighted cells are at or above the current standardValueColumn LabelsSWSL2L Row LabelsDec-17Nov-17Jun-17May-17Nov-16Jun-16May-16Nov-15May-15Nov-14May-14Nov-13May-13Nov-12Apr-12Mar-12Dec-11Nov-11Jun-11MCL1 2000 µg/L Trichlorofluoromethane1 2000 µg/L GP-A-7 (20.5-24.5)0.251 2000 µg/L MW-2R 1.5 0.71 1 1.5 2.4 3.7 12 12.1 16.9 20.9 201 2000 µg/L MW-7 1.6 1.6 0.91 1.5 0.92 1.4 0.79 1.2 0.62 0.47 0.25 0.29 0.31 2000 µg/L MW-9 1.4 1.2 1.4 1 1.3 1.1 0.98 0.96 0.47 0.69 0.36 0.49 0.41 2000 µg/L MW-100.2 0.33 0.38 0.49 0.71 2000 µg/L MW-12 1.4 0.52 1 2.8 1.4 0.82 0.22 0.321 2000 µg/L MW-131 2000 µg/L MW-14 0.8 0.87 0.75 0.58 1.1 0.54 0.59 0.57 0.341 2000 µg/L MW-15 0.22 0.71 2.1 4.4 5.1 4.8 4.4 3.9 5.3 7.6 4.3 8.1 7.31 2000 µg/L SW-4 0.32 0.27 0.25 1.41 0.03 µg/L Vinyl chloride1 0.03 µg/L MW-2R1.4 1.4 1 0.72 0.75 0.7 1.2 0.955 500 µg/L Xylenes (Total)5 500 µg/L MW-2R0.98 1.65 500 µg/L MW-71.2 0.795 500 µg/L MW-10 1.1c:\pwworking\tpa\d0269489\W-S GW Revised.xlsb9 of 9
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Winston-Salem City/County Utilities | Supplement to the Assessment Monitoring Report Appendix B – Laboratory Groundwater Report

B
Appendix B – Laboratory Groundwater Report

Winston-Salem City/County Utilities | Supplement to the Assessment Monitoring Report Appendix B – Laboratory Groundwater Report

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#=CL#
January 11, 2018
LIMS USE: FR - SEAN QUARRY
LIMS OBJECT ID: 92368450
92368450
Project:
Pace Project No.:
RE:
Sean QuarryHDR Engineering440 South Church StreetSuite 1000Charlotte, NC 28202
OSR 305065
Dear Sean Quarry:
Enclosed are the analytical results for sample(s) received by the laboratory on December 29, 2017.
The results relate only to the samples included in this report. Results reported herein conform to themost current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Herring
[e-mail]
HORIZON Database Administrator1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 176
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92368450
OSR 305065
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 176
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92368450
OSR 305065
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92368450001 TRIP BLANK EPA 8260 70 PASI-CSWB
92368450002 EQUIPMENT BLANK EPA 8081 21 PASI-CPKS
EPA 8082 8 PASI-CPKS
EPA 8270 111 PASI-CBPJ
EPA 8260 70 PASI-CSWB
92368450003 MW-1R EPA 8081 21 PASI-CPKS
EPA 8082 8 PASI-CPKS
EPA 8270 111 PASI-CBPJ
EPA 8260 70 PASI-CSWB
92368450004 MW-2R EPA 8081 21 PASI-CPKS
EPA 8082 8 PASI-CPKS
EPA 8270 111 PASI-CBPJ
EPA 8260 70 PASI-CSWB
92368450005 MW-3R EPA 8081 21 PASI-CPKS
EPA 8082 8 PASI-CPKS
EPA 8270 111 PASI-CBPJ
EPA 8260 70 PASI-CSWB
92368450006 MW-5R EPA 8081 21 PASI-CPKS
EPA 8082 8 PASI-CPKS
EPA 8270 111 PASI-CBPJ
EPA 8260 70 PASI-CSWB
92368450007 MW-7 EPA 8081 21 PASI-CPKS
EPA 8082 8 PASI-CPKS
EPA 8270 111 PASI-CBPJ
EPA 8260 70 PASI-CSWB
92368450008 MW-9 EPA 8081 21 PASI-CPKS
EPA 8082 8 PASI-CPKS
EPA 8270 111 PASI-CBPJ
EPA 8260 70 PASI-CSWB
92368450009 MW-10 EPA 8081 21 PASI-CPKS
EPA 8082 8 PASI-CPKS
EPA 8270 111 PASI-CBPJ
EPA 8260 70 PASI-CSWB
92368450010 MW-13 EPA 8081 21 PASI-CPKS
EPA 8082 8 PASI-CPKS
EPA 8270 111 PASI-CBPJ
EPA 8260 70 PASI-CSWB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 176
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92368450
OSR 305065
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92368450011 MW-14 EPA 8081 21 PASI-CPKS
EPA 8082 8 PASI-CPKS
EPA 8270 111 PASI-CBPJ
EPA 8260 70 PASI-CSWB
92368450012 SW-2 EPA 8270 111 PASI-CBPJ
EPA 8260 70 PASI-CSWB
92368450013 MW-4R EPA 8081 21 PASI-CPKS
EPA 8082 8 PASI-CPKS
EPA 8270 111 PASI-CBPJ
EPA 8260 70 PASI-CSWB
92368450014 MW-8 EPA 8081 21 PASI-CPKS
EPA 8082 8 PASI-CPKS
EPA 8270 111 PASI-CBPJ
EPA 8260 70 PASI-CSWB
92368450015 MW-11 EPA 8081 21 PASI-CPKS
EPA 8082 8 PASI-CPKS
EPA 8270 111 PASI-CBPJ
EPA 8260 70 PASI-CSWB
92368450016 MW-12 EPA 8081 21 PASI-CPKS
EPA 8082 8 PASI-CPKS
EPA 8270 111 PASI-CBPJ
EPA 8260 70 PASI-CSWB
92368450017 MW-15 EPA 8081 21 PASI-CPKS
EPA 8082 8 PASI-CPKS
EPA 8270 111 PASI-CBPJ
EPA 8260 70 PASI-CSWB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:TRIP BLANK Lab ID:92368450001 Collected:12/28/17 00:00 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/18 01:07 67-64-125.0 1
Acetonitrile ND ug/L 01/03/18 01:07 75-05-850.0 1
Acrolein ND ug/L 01/03/18 01:07 107-02-810.0 1
Acrylonitrile ND ug/L 01/03/18 01:07 107-13-110.0 1
Allyl chloride ND ug/L 01/03/18 01:07 107-05-12.0 1
Benzene ND ug/L 01/03/18 01:07 71-43-21.0 1
Bromochloromethane ND ug/L 01/03/18 01:07 74-97-51.0 1
Bromodichloromethane ND ug/L 01/03/18 01:07 75-27-41.0 1
Bromoform ND ug/L 01/03/18 01:07 75-25-21.0 1
Bromomethane ND ug/L 01/03/18 01:07 74-83-92.0 1
2-Butanone (MEK)ND ug/L 01/03/18 01:07 78-93-35.0 1
Carbon disulfide ND ug/L 01/03/18 01:07 75-15-02.0 1
Carbon tetrachloride ND ug/L 01/03/18 01:07 56-23-51.0 1
Chlorobenzene ND ug/L 01/03/18 01:07 108-90-71.0 1
Chloroethane ND ug/L 01/03/18 01:07 75-00-31.0 1
Chloroform ND ug/L 01/03/18 01:07 67-66-31.0 1
Chloromethane ND ug/L 01/03/18 01:07 74-87-31.0 1
Chloroprene ND ug/L 01/03/18 01:07 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/18 01:07 96-12-8 L22.0 1
Dibromochloromethane ND ug/L 01/03/18 01:07 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/18 01:07 106-93-41.0 1
Dibromomethane ND ug/L 01/03/18 01:07 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 01/03/18 01:07 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 01/03/18 01:07 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 01/03/18 01:07 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/18 01:07 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 01/03/18 01:07 75-71-81.0 1
1,1-Dichloroethane ND ug/L 01/03/18 01:07 75-34-31.0 1
1,2-Dichloroethane ND ug/L 01/03/18 01:07 107-06-21.0 1
1,1-Dichloroethene ND ug/L 01/03/18 01:07 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 01/03/18 01:07 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 01/03/18 01:07 156-60-51.0 1
1,2-Dichloropropane ND ug/L 01/03/18 01:07 78-87-51.0 1
1,3-Dichloropropane ND ug/L 01/03/18 01:07 142-28-91.0 1
2,2-Dichloropropane ND ug/L 01/03/18 01:07 594-20-71.0 1
1,1-Dichloropropene ND ug/L 01/03/18 01:07 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 01/03/18 01:07 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 01/03/18 01:07 10061-02-61.0 1
Ethylbenzene ND ug/L 01/03/18 01:07 100-41-41.0 1
Ethyl methacrylate ND ug/L 01/03/18 01:07 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 01/03/18 01:07 87-68-31.0 1
2-Hexanone ND ug/L 01/03/18 01:07 591-78-65.0 1
Iodomethane ND ug/L 01/03/18 01:07 74-88-45.0 1
Isobutanol ND ug/L 01/03/18 01:07 78-83-11001
Methacrylonitrile ND ug/L 01/03/18 01:07 126-98-710.0 1
Methylene Chloride ND ug/L 01/03/18 01:07 75-09-21.0 1
Methyl methacrylate ND ug/L 01/03/18 01:07 80-62-6 L22.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:TRIP BLANK Lab ID:92368450001 Collected:12/28/17 00:00 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/18 01:07 108-10-15.0 1
Naphthalene ND ug/L 01/03/18 01:07 91-20-31.0 1
Propionitrile ND ug/L 01/03/18 01:07 107-12-020.0 1
Styrene ND ug/L 01/03/18 01:07 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/18 01:07 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/18 01:07 79-34-51.0 1
Tetrachloroethene ND ug/L 01/03/18 01:07 127-18-41.0 1
Tetrahydrofuran ND ug/L 01/03/18 01:07 109-99-910.0 1
Toluene ND ug/L 01/03/18 01:07 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 01/03/18 01:07 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 01/03/18 01:07 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 01/03/18 01:07 79-00-51.0 1
Trichloroethene ND ug/L 01/03/18 01:07 79-01-61.0 1
Trichlorofluoromethane ND ug/L 01/03/18 01:07 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 01/03/18 01:07 96-18-41.0 1
Vinyl acetate ND ug/L 01/03/18 01:07 108-05-42.0 1
Vinyl chloride ND ug/L 01/03/18 01:07 75-01-41.0 1
Xylene (Total)ND ug/L 01/03/18 01:07 1330-20-71.0 1
m&p-Xylene ND ug/L 01/03/18 01:07 179601-23-12.0 1
o-Xylene ND ug/L 01/03/18 01:07 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)101 %01/03/18 01:07 460-00-470-130 1
1,2-Dichloroethane-d4 (S)94 %01/03/18 01:07 17060-07-070-130 1
Toluene-d8 (S)109 %01/03/18 01:07 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:EQUIPMENT BLANK Lab ID:92368450002 Collected:12/28/17 16:30 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 01/02/18 15:43 309-00-212/29/17 10:130.050 1
alpha-BHC ND ug/L 01/02/18 15:43 319-84-612/29/17 10:130.050 1
beta-BHC ND ug/L 01/02/18 15:43 319-85-712/29/17 10:130.050 1
delta-BHC ND ug/L 01/02/18 15:43 319-86-812/29/17 10:130.050 1
gamma-BHC (Lindane)ND ug/L 01/02/18 15:43 58-89-912/29/17 10:130.050 1
Chlordane (Technical)ND ug/L 01/02/18 15:43 57-74-912/29/17 10:130.20 1
4,4'-DDD ND ug/L 01/02/18 15:43 72-54-812/29/17 10:130.050 1
4,4'-DDE ND ug/L 01/02/18 15:43 72-55-912/29/17 10:130.050 1
4,4'-DDT ND ug/L 01/02/18 15:43 50-29-312/29/17 10:130.050 1
Dieldrin ND ug/L 01/02/18 15:43 60-57-112/29/17 10:130.050 1
Endosulfan I ND ug/L 01/02/18 15:43 959-98-812/29/17 10:130.050 1
Endosulfan II ND ug/L 01/02/18 15:43 33213-65-912/29/17 10:130.050 1
Endosulfan sulfate ND ug/L 01/02/18 15:43 1031-07-812/29/17 10:130.050 1
Endrin ND ug/L 01/02/18 15:43 72-20-812/29/17 10:130.050 1
Endrin aldehyde ND ug/L 01/02/18 15:43 7421-93-412/29/17 10:130.050 1
Heptachlor ND ug/L 01/02/18 15:43 76-44-812/29/17 10:130.050 1
Heptachlor epoxide ND ug/L 01/02/18 15:43 1024-57-312/29/17 10:130.050 1
Methoxychlor ND ug/L 01/02/18 15:43 72-43-512/29/17 10:130.15 1
Toxaphene ND ug/L 01/02/18 15:43 8001-35-212/29/17 10:130.20 1
Surrogates
Tetrachloro-m-xylene (S)86 %01/02/18 15:43 877-09-812/29/17 10:1320-130 1
Decachlorobiphenyl (S)60 %01/02/18 15:43 2051-24-312/29/17 10:1320-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 01/02/18 13:28 12674-11-212/29/17 10:130.50 1
PCB-1221 (Aroclor 1221)ND ug/L 01/02/18 13:28 11104-28-212/29/17 10:130.50 1
PCB-1232 (Aroclor 1232)ND ug/L 01/02/18 13:28 11141-16-512/29/17 10:130.50 1
PCB-1242 (Aroclor 1242)ND ug/L 01/02/18 13:28 53469-21-912/29/17 10:130.50 1
PCB-1248 (Aroclor 1248)ND ug/L 01/02/18 13:28 12672-29-612/29/17 10:130.50 1
PCB-1254 (Aroclor 1254)ND ug/L 01/02/18 13:28 11097-69-112/29/17 10:130.50 1
PCB-1260 (Aroclor 1260)ND ug/L 01/02/18 13:28 11096-82-512/29/17 10:130.50 1
Surrogates
Decachlorobiphenyl (S)65 %01/02/18 13:28 2051-24-312/29/17 10:1310-132 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 01/05/18 15:08 83-32-901/04/18 12:1810.0 1
Acenaphthylene ND ug/L 01/05/18 15:08 208-96-801/04/18 12:1810.0 1
Acetophenone ND ug/L 01/05/18 15:08 98-86-201/04/18 12:1810.0 1
2-Acetylaminofluorene ND ug/L 01/05/18 15:08 53-96-301/04/18 12:1820.0 1
4-Aminobiphenyl ND ug/L 01/05/18 15:08 92-67-101/04/18 12:1810.0 1
Anthracene ND ug/L 01/05/18 15:08 120-12-701/04/18 12:1810.0 1
Benzo(a)anthracene ND ug/L 01/05/18 15:08 56-55-301/04/18 12:1810.0 1
Benzo(a)pyrene ND ug/L 01/05/18 15:08 50-32-801/04/18 12:1810.0 1
Benzo(b)fluoranthene ND ug/L 01/05/18 15:08 205-99-201/04/18 12:1810.0 1
Benzo(g,h,i)perylene ND ug/L 01/05/18 15:08 191-24-201/04/18 12:1810.0 1
Benzo(k)fluoranthene ND ug/L 01/05/18 15:08 207-08-901/04/18 12:1810.0 1
Benzyl alcohol ND ug/L 01/05/18 15:08 100-51-601/04/18 12:1820.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 7 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:EQUIPMENT BLANK Lab ID:92368450002 Collected:12/28/17 16:30 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
4-Bromophenylphenyl ether ND ug/L 01/05/18 15:08 101-55-301/04/18 12:1810.0 1
Butylbenzylphthalate ND ug/L 01/05/18 15:08 85-68-701/04/18 12:1810.0 1
4-Chloro-3-methylphenol ND ug/L 01/05/18 15:08 59-50-701/04/18 12:1820.0 1
4-Chloroaniline ND ug/L 01/05/18 15:08 106-47-801/04/18 12:1820.0 1
Chlorobenzilate ND ug/L 01/05/18 15:08 510-15-601/04/18 12:1810.0 1
bis(2-Chloroethoxy)methane ND ug/L 01/05/18 15:08 111-91-101/04/18 12:1810.0 1
bis(2-Chloroethyl) ether ND ug/L 01/05/18 15:08 111-44-401/04/18 12:1810.0 1
2-Chloronaphthalene ND ug/L 01/05/18 15:08 91-58-701/04/18 12:1810.0 1
2-Chlorophenol ND ug/L 01/05/18 15:08 95-57-801/04/18 12:1810.0 1
4-Chlorophenylphenyl ether ND ug/L 01/05/18 15:08 7005-72-301/04/18 12:1810.0 1
Chrysene ND ug/L 01/05/18 15:08 218-01-901/04/18 12:1810.0 1
Diallate ND ug/L 01/05/18 15:08 2303-16-401/04/18 12:1810.0 1
Dibenz(a,h)anthracene ND ug/L 01/05/18 15:08 53-70-301/04/18 12:1810.0 1
Dibenzofuran ND ug/L 01/05/18 15:08 132-64-901/04/18 12:1810.0 1
3,3'-Dichlorobenzidine ND ug/L 01/05/18 15:08 91-94-101/04/18 12:1820.0 1
2,4-Dichlorophenol ND ug/L 01/05/18 15:08 120-83-201/04/18 12:1810.0 1
2,6-Dichlorophenol ND ug/L 01/05/18 15:08 87-65-0 L201/04/18 12:1810.0 1
Diethylphthalate ND ug/L 01/05/18 15:08 84-66-201/04/18 12:1810.0 1
Dimethoate ND ug/L 01/05/18 15:08 60-51-501/04/18 12:1810.0 1
P-Dimethylaminoazobenzene ND ug/L 01/05/18 15:08 60-11-701/04/18 12:185.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 01/05/18 15:08 57-97-601/04/18 12:1810.0 1
3,3'-Dimethylbenzidine ND ug/L 01/05/18 15:08 119-93-701/04/18 12:1810.0 1
2,4-Dimethylphenol ND ug/L 01/05/18 15:08 105-67-901/04/18 12:1810.0 1
Dimethylphthalate ND ug/L 01/05/18 15:08 131-11-301/04/18 12:1810.0 1
Di-n-butylphthalate ND ug/L 01/05/18 15:08 84-74-201/04/18 12:1810.0 1
4,6-Dinitro-2-methylphenol ND ug/L 01/05/18 15:08 534-52-1 L201/04/18 12:1820.0 1
1,3-Dinitrobenzene ND ug/L 01/05/18 15:08 99-65-001/04/18 12:1820.0 1
2,4-Dinitrophenol ND ug/L 01/05/18 15:08 51-28-501/04/18 12:1850.0 1
2,4-Dinitrotoluene ND ug/L 01/05/18 15:08 121-14-201/04/18 12:1810.0 1
2,6-Dinitrotoluene ND ug/L 01/05/18 15:08 606-20-201/04/18 12:1810.0 1
Di-n-octylphthalate ND ug/L 01/05/18 15:08 117-84-0 L101/04/18 12:1810.0 1
Diphenylamine ND ug/L 01/05/18 15:08 122-39-401/04/18 12:1810.0 1
Disulfoton ND ug/L 01/05/18 15:08 298-04-401/04/18 12:1810.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 01/05/18 15:08 117-81-701/04/18 12:186.0 1
Ethyl methanesulfonate ND ug/L 01/05/18 15:08 62-50-001/04/18 12:1820.0 1
Famphur ND ug/L 01/05/18 15:08 52-85-701/04/18 12:1810.0 1
Fluoranthene ND ug/L 01/05/18 15:08 206-44-001/04/18 12:1810.0 1
Fluorene ND ug/L 01/05/18 15:08 86-73-701/04/18 12:1810.0 1
Hexachlorobenzene ND ug/L 01/05/18 15:08 118-74-101/04/18 12:1810.0 1
Hexachlorocyclopentadiene ND ug/L 01/05/18 15:08 77-47-401/04/18 12:1810.0 1
Hexachloroethane ND ug/L 01/05/18 15:08 67-72-101/04/18 12:1810.0 1
Hexachlorophene ND ug/L 01/05/18 15:08 70-30-401/04/18 12:181001
Indeno(1,2,3-cd)pyrene ND ug/L 01/05/18 15:08 193-39-501/04/18 12:1810.0 1
Isodrin ND ug/L 01/05/18 15:08 465-73-601/04/18 12:1820.0 1
Isophorone ND ug/L 01/05/18 15:08 78-59-101/04/18 12:1810.0 1
Isosafrole ND ug/L 01/05/18 15:08 120-58-101/04/18 12:1810.0 1
Kepone ND ug/L 01/05/18 15:08 143-50-0 L101/04/18 12:1810.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:EQUIPMENT BLANK Lab ID:92368450002 Collected:12/28/17 16:30 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Methapyrilene ND ug/L 01/05/18 15:08 91-80-501/04/18 12:1850.0 1
3-Methylcholanthrene ND ug/L 01/05/18 15:08 56-49-501/04/18 12:1810.0 1
Methyl methanesulfonate ND ug/L 01/05/18 15:08 66-27-3 L101/04/18 12:185.0 1
2-Methylnaphthalene ND ug/L 01/05/18 15:08 91-57-601/04/18 12:1810.0 1
Methyl parathion ND ug/L 01/05/18 15:08 298-00-001/04/18 12:1810.0 1
2-Methylphenol(o-Cresol)ND ug/L 01/05/18 15:08 95-48-701/04/18 12:1810.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 01/05/18 15:08 15831-10-401/04/18 12:1810.0 1
1-Naphthalenamine ND ug/L 01/05/18 15:08 134-32-701/04/18 12:185.0 1
2-Naphthalenamine ND ug/L 01/05/18 15:08 91-59-801/04/18 12:185.0 1
1,4-Naphthoquinone ND ug/L 01/05/18 15:08 130-15-401/04/18 12:185.0 1
2-Nitroaniline ND ug/L 01/05/18 15:08 88-74-401/04/18 12:1850.0 1
3-Nitroaniline ND ug/L 01/05/18 15:08 99-09-201/04/18 12:1850.0 1
4-Nitroaniline ND ug/L 01/05/18 15:08 100-01-601/04/18 12:1820.0 1
Nitrobenzene ND ug/L 01/05/18 15:08 98-95-301/04/18 12:1810.0 1
2-Nitrophenol ND ug/L 01/05/18 15:08 88-75-501/04/18 12:1810.0 1
4-Nitrophenol ND ug/L 01/05/18 15:08 100-02-701/04/18 12:1850.0 1
5-Nitro-o-toluidine ND ug/L 01/05/18 15:08 99-55-801/04/18 12:1810.0 1
N-Nitrosodiethylamine ND ug/L 01/05/18 15:08 55-18-501/04/18 12:1820.0 1
N-Nitrosodimethylamine ND ug/L 01/05/18 15:08 62-75-901/04/18 12:1810.0 1
N-Nitroso-di-n-butylamine ND ug/L 01/05/18 15:08 924-16-301/04/18 12:1810.0 1
N-Nitroso-di-n-propylamine ND ug/L 01/05/18 15:08 621-64-701/04/18 12:1810.0 1
N-Nitrosodiphenylamine ND ug/L 01/05/18 15:08 86-30-601/04/18 12:1810.0 1
N-Nitrosomethylethylamine ND ug/L 01/05/18 15:08 10595-95-601/04/18 12:1810.0 1
N-Nitrosopiperidine ND ug/L 01/05/18 15:08 100-75-401/04/18 12:1820.0 1
N-Nitrosopyrrolidine ND ug/L 01/05/18 15:08 930-55-201/04/18 12:1810.0 1
O,O,O-Triethylphosphorothioate ND ug/L 01/05/18 15:08 126-68-101/04/18 12:1810.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 01/05/18 15:08 108-60-101/04/18 12:1810.0 1
Parathion (Ethyl parathion)ND ug/L 01/05/18 15:08 56-38-201/04/18 12:1810.0 1
Pentachlorobenzene ND ug/L 01/05/18 15:08 608-93-501/04/18 12:1810.0 1
Pentachloronitrobenzene ND ug/L 01/05/18 15:08 82-68-801/04/18 12:1820.0 1
Pentachlorophenol ND ug/L 01/05/18 15:08 87-86-501/04/18 12:1825.0 1
Phenacetin ND ug/L 01/05/18 15:08 62-44-201/04/18 12:1820.0 1
Phenanthrene ND ug/L 01/05/18 15:08 85-01-801/04/18 12:1810.0 1
Phenol ND ug/L 01/05/18 15:08 108-95-201/04/18 12:1810.0 1
p-Phenylenediamine ND ug/L 01/05/18 15:08 106-50-301/04/18 12:1810.0 1
Phorate ND ug/L 01/05/18 15:08 298-02-201/04/18 12:1810.0 1
Pronamide ND ug/L 01/05/18 15:08 23950-58-501/04/18 12:1810.0 1
Pyrene ND ug/L 01/05/18 15:08 129-00-001/04/18 12:1810.0 1
Safrole ND ug/L 01/05/18 15:08 94-59-701/04/18 12:1810.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 01/05/18 15:08 95-94-301/04/18 12:1810.0 1
2,3,4,6-Tetrachlorophenol ND ug/L 01/05/18 15:08 58-90-201/04/18 12:1810.0 1
Thionazin ND ug/L 01/05/18 15:08 297-97-201/04/18 12:1820.0 1
O-Toluidine ND ug/L 01/05/18 15:08 95-53-401/04/18 12:1810.0 1
2,4,5-Trichlorophenol ND ug/L 01/05/18 15:08 95-95-401/04/18 12:1810.0 1
2,4,6-Trichlorophenol ND ug/L 01/05/18 15:08 88-06-2 L201/04/18 12:1810.0 1
1,3,5-Trinitrobenzene ND ug/L 01/05/18 15:08 99-35-4 L201/04/18 12:1810.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:EQUIPMENT BLANK Lab ID:92368450002 Collected:12/28/17 16:30 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Surrogates
Nitrobenzene-d5 (S)86 %01/05/18 15:08 4165-60-001/04/18 12:1821-110 1
2-Fluorobiphenyl (S)87 %01/05/18 15:08 321-60-801/04/18 12:1827-110 1
Terphenyl-d14 (S)88 %01/05/18 15:08 1718-51-001/04/18 12:1831-107 1
Phenol-d6 (S)10 %01/05/18 15:08 13127-88-301/04/18 12:1810-110 1
2-Fluorophenol (S)10 %01/05/18 15:08 367-12-4 S201/04/18 12:1812-110 1
2,4,6-Tribromophenol (S)26 %01/05/18 15:08 118-79-6 S201/04/18 12:1827-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/18 01:24 67-64-125.0 1
Acetonitrile ND ug/L 01/03/18 01:24 75-05-850.0 1
Acrolein ND ug/L 01/03/18 01:24 107-02-810.0 1
Acrylonitrile ND ug/L 01/03/18 01:24 107-13-110.0 1
Allyl chloride ND ug/L 01/03/18 01:24 107-05-12.0 1
Benzene ND ug/L 01/03/18 01:24 71-43-21.0 1
Bromochloromethane ND ug/L 01/03/18 01:24 74-97-51.0 1
Bromodichloromethane ND ug/L 01/03/18 01:24 75-27-41.0 1
Bromoform ND ug/L 01/03/18 01:24 75-25-21.0 1
Bromomethane ND ug/L 01/03/18 01:24 74-83-92.0 1
2-Butanone (MEK)ND ug/L 01/03/18 01:24 78-93-35.0 1
Carbon disulfide ND ug/L 01/03/18 01:24 75-15-02.0 1
Carbon tetrachloride ND ug/L 01/03/18 01:24 56-23-51.0 1
Chlorobenzene ND ug/L 01/03/18 01:24 108-90-71.0 1
Chloroethane ND ug/L 01/03/18 01:24 75-00-31.0 1
Chloroform ND ug/L 01/03/18 01:24 67-66-31.0 1
Chloromethane ND ug/L 01/03/18 01:24 74-87-31.0 1
Chloroprene ND ug/L 01/03/18 01:24 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/18 01:24 96-12-8 L22.0 1
Dibromochloromethane ND ug/L 01/03/18 01:24 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/18 01:24 106-93-41.0 1
Dibromomethane ND ug/L 01/03/18 01:24 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 01/03/18 01:24 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 01/03/18 01:24 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 01/03/18 01:24 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/18 01:24 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 01/03/18 01:24 75-71-81.0 1
1,1-Dichloroethane ND ug/L 01/03/18 01:24 75-34-31.0 1
1,2-Dichloroethane ND ug/L 01/03/18 01:24 107-06-21.0 1
1,1-Dichloroethene ND ug/L 01/03/18 01:24 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 01/03/18 01:24 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 01/03/18 01:24 156-60-51.0 1
1,2-Dichloropropane ND ug/L 01/03/18 01:24 78-87-51.0 1
1,3-Dichloropropane ND ug/L 01/03/18 01:24 142-28-91.0 1
2,2-Dichloropropane ND ug/L 01/03/18 01:24 594-20-71.0 1
1,1-Dichloropropene ND ug/L 01/03/18 01:24 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 01/03/18 01:24 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 01/03/18 01:24 10061-02-61.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:EQUIPMENT BLANK Lab ID:92368450002 Collected:12/28/17 16:30 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/03/18 01:24 100-41-41.0 1
Ethyl methacrylate ND ug/L 01/03/18 01:24 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 01/03/18 01:24 87-68-31.0 1
2-Hexanone ND ug/L 01/03/18 01:24 591-78-65.0 1
Iodomethane ND ug/L 01/03/18 01:24 74-88-45.0 1
Isobutanol ND ug/L 01/03/18 01:24 78-83-11001
Methacrylonitrile ND ug/L 01/03/18 01:24 126-98-710.0 1
Methylene Chloride ND ug/L 01/03/18 01:24 75-09-21.0 1
Methyl methacrylate ND ug/L 01/03/18 01:24 80-62-6 L22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/18 01:24 108-10-15.0 1
Naphthalene ND ug/L 01/03/18 01:24 91-20-31.0 1
Propionitrile ND ug/L 01/03/18 01:24 107-12-020.0 1
Styrene ND ug/L 01/03/18 01:24 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/18 01:24 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/18 01:24 79-34-51.0 1
Tetrachloroethene ND ug/L 01/03/18 01:24 127-18-41.0 1
Tetrahydrofuran ND ug/L 01/03/18 01:24 109-99-910.0 1
Toluene ND ug/L 01/03/18 01:24 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 01/03/18 01:24 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 01/03/18 01:24 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 01/03/18 01:24 79-00-51.0 1
Trichloroethene ND ug/L 01/03/18 01:24 79-01-61.0 1
Trichlorofluoromethane ND ug/L 01/03/18 01:24 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 01/03/18 01:24 96-18-41.0 1
Vinyl acetate ND ug/L 01/03/18 01:24 108-05-42.0 1
Vinyl chloride ND ug/L 01/03/18 01:24 75-01-41.0 1
Xylene (Total)ND ug/L 01/03/18 01:24 1330-20-71.0 1
m&p-Xylene ND ug/L 01/03/18 01:24 179601-23-12.0 1
o-Xylene ND ug/L 01/03/18 01:24 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)103 %01/03/18 01:24 460-00-470-130 1
1,2-Dichloroethane-d4 (S)94 %01/03/18 01:24 17060-07-070-130 1
Toluene-d8 (S)111 %01/03/18 01:24 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 11 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-1R Lab ID:92368450003 Collected:12/28/17 14:40 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By GLG 01/05/18 11:281
Collected Date 12/28/17 01/05/18 11:281
Collected Time 14:40 01/05/18 11:281
pH 5.6 Std. Units 01/05/18 11:280.10 1
Temperature 11.7 deg C 01/05/18 11:280.50 1
Static Water Level 35.1 feet 01/05/18 11:281
Specific Conductance 214.6 umhos/cm 01/05/18 11:281.0 1
Oxygen, Dissolved 3.3 mg/L 01/05/18 11:28 7782-44-71
Total Well Depth 60.0 feet 01/05/18 11:281
REDOX 112.4 mV 01/05/18 11:281
Turbidity 2.8 NTU 01/05/18 11:281.0 1
Odor NONE 01/05/18 11:281
Appearance CLEAR 01/05/18 11:281
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 01/02/18 16:00 309-00-212/29/17 10:130.050 1
alpha-BHC ND ug/L 01/02/18 16:00 319-84-612/29/17 10:130.050 1
beta-BHC ND ug/L 01/02/18 16:00 319-85-712/29/17 10:130.050 1
delta-BHC ND ug/L 01/02/18 16:00 319-86-812/29/17 10:130.050 1
gamma-BHC (Lindane)ND ug/L 01/02/18 16:00 58-89-912/29/17 10:130.050 1
Chlordane (Technical)ND ug/L 01/02/18 16:00 57-74-912/29/17 10:130.20 1
4,4'-DDD ND ug/L 01/02/18 16:00 72-54-812/29/17 10:130.050 1
4,4'-DDE ND ug/L 01/02/18 16:00 72-55-912/29/17 10:130.050 1
4,4'-DDT ND ug/L 01/02/18 16:00 50-29-312/29/17 10:130.050 1
Dieldrin ND ug/L 01/02/18 16:00 60-57-112/29/17 10:130.050 1
Endosulfan I ND ug/L 01/02/18 16:00 959-98-812/29/17 10:130.050 1
Endosulfan II ND ug/L 01/02/18 16:00 33213-65-912/29/17 10:130.050 1
Endosulfan sulfate ND ug/L 01/02/18 16:00 1031-07-812/29/17 10:130.050 1
Endrin ND ug/L 01/02/18 16:00 72-20-812/29/17 10:130.050 1
Endrin aldehyde ND ug/L 01/02/18 16:00 7421-93-412/29/17 10:130.050 1
Heptachlor ND ug/L 01/02/18 16:00 76-44-812/29/17 10:130.050 1
Heptachlor epoxide ND ug/L 01/02/18 16:00 1024-57-312/29/17 10:130.050 1
Methoxychlor ND ug/L 01/02/18 16:00 72-43-512/29/17 10:130.15 1
Toxaphene ND ug/L 01/02/18 16:00 8001-35-212/29/17 10:130.20 1
Surrogates
Tetrachloro-m-xylene (S)101 %01/02/18 16:00 877-09-812/29/17 10:1320-130 1
Decachlorobiphenyl (S)58 %01/02/18 16:00 2051-24-312/29/17 10:1320-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 01/02/18 13:49 12674-11-212/29/17 10:130.50 1
PCB-1221 (Aroclor 1221)ND ug/L 01/02/18 13:49 11104-28-212/29/17 10:130.50 1
PCB-1232 (Aroclor 1232)ND ug/L 01/02/18 13:49 11141-16-512/29/17 10:130.50 1
PCB-1242 (Aroclor 1242)ND ug/L 01/02/18 13:49 53469-21-912/29/17 10:130.50 1
PCB-1248 (Aroclor 1248)ND ug/L 01/02/18 13:49 12672-29-612/29/17 10:130.50 1
PCB-1254 (Aroclor 1254)ND ug/L 01/02/18 13:49 11097-69-112/29/17 10:130.50 1
PCB-1260 (Aroclor 1260)ND ug/L 01/02/18 13:49 11096-82-512/29/17 10:130.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 12 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-1R Lab ID:92368450003 Collected:12/28/17 14:40 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
Surrogates
Decachlorobiphenyl (S)60 %01/02/18 13:49 2051-24-312/29/17 10:1310-132 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 01/02/18 15:11 83-32-912/29/17 10:1510.0 1
Acenaphthylene ND ug/L 01/02/18 15:11 208-96-812/29/17 10:1510.0 1
Acetophenone ND ug/L 01/02/18 15:11 98-86-212/29/17 10:1510.0 1
2-Acetylaminofluorene ND ug/L 01/02/18 15:11 53-96-3 L212/29/17 10:1520.0 1
4-Aminobiphenyl ND ug/L 01/02/18 15:11 92-67-112/29/17 10:1510.0 1
Anthracene ND ug/L 01/02/18 15:11 120-12-712/29/17 10:1510.0 1
Benzo(a)anthracene ND ug/L 01/02/18 15:11 56-55-312/29/17 10:1510.0 1
Benzo(a)pyrene ND ug/L 01/02/18 15:11 50-32-812/29/17 10:1510.0 1
Benzo(b)fluoranthene ND ug/L 01/02/18 15:11 205-99-212/29/17 10:1510.0 1
Benzo(g,h,i)perylene ND ug/L 01/02/18 15:11 191-24-212/29/17 10:1510.0 1
Benzo(k)fluoranthene ND ug/L 01/02/18 15:11 207-08-912/29/17 10:1510.0 1
Benzyl alcohol ND ug/L 01/02/18 15:11 100-51-612/29/17 10:1520.0 1
4-Bromophenylphenyl ether ND ug/L 01/02/18 15:11 101-55-312/29/17 10:1510.0 1
Butylbenzylphthalate ND ug/L 01/02/18 15:11 85-68-712/29/17 10:1510.0 1
4-Chloro-3-methylphenol ND ug/L 01/02/18 15:11 59-50-712/29/17 10:1520.0 1
4-Chloroaniline ND ug/L 01/02/18 15:11 106-47-812/29/17 10:1520.0 1
Chlorobenzilate ND ug/L 01/02/18 15:11 510-15-612/29/17 10:1510.0 1
bis(2-Chloroethoxy)methane ND ug/L 01/02/18 15:11 111-91-112/29/17 10:1510.0 1
bis(2-Chloroethyl) ether ND ug/L 01/02/18 15:11 111-44-412/29/17 10:1510.0 1
2-Chloronaphthalene ND ug/L 01/02/18 15:11 91-58-712/29/17 10:1510.0 1
2-Chlorophenol ND ug/L 01/02/18 15:11 95-57-812/29/17 10:1510.0 1
4-Chlorophenylphenyl ether ND ug/L 01/02/18 15:11 7005-72-312/29/17 10:1510.0 1
Chrysene ND ug/L 01/02/18 15:11 218-01-912/29/17 10:1510.0 1
Diallate ND ug/L 01/02/18 15:11 2303-16-412/29/17 10:1510.0 1
Dibenz(a,h)anthracene ND ug/L 01/02/18 15:11 53-70-312/29/17 10:1510.0 1
Dibenzofuran ND ug/L 01/02/18 15:11 132-64-912/29/17 10:1510.0 1
3,3'-Dichlorobenzidine ND ug/L 01/02/18 15:11 91-94-112/29/17 10:1520.0 1
2,4-Dichlorophenol ND ug/L 01/02/18 15:11 120-83-212/29/17 10:1510.0 1
2,6-Dichlorophenol ND ug/L 01/02/18 15:11 87-65-012/29/17 10:1510.0 1
Diethylphthalate ND ug/L 01/02/18 15:11 84-66-212/29/17 10:1510.0 1
Dimethoate ND ug/L 01/02/18 15:11 60-51-512/29/17 10:1510.0 1
P-Dimethylaminoazobenzene ND ug/L 01/02/18 15:11 60-11-712/29/17 10:155.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 01/02/18 15:11 57-97-612/29/17 10:1510.0 1
3,3'-Dimethylbenzidine ND ug/L 01/02/18 15:11 119-93-712/29/17 10:1510.0 1
2,4-Dimethylphenol ND ug/L 01/02/18 15:11 105-67-912/29/17 10:1510.0 1
Dimethylphthalate ND ug/L 01/02/18 15:11 131-11-312/29/17 10:1510.0 1
Di-n-butylphthalate ND ug/L 01/02/18 15:11 84-74-212/29/17 10:1510.0 1
4,6-Dinitro-2-methylphenol ND ug/L 01/02/18 15:11 534-52-112/29/17 10:1520.0 1
1,3-Dinitrobenzene ND ug/L 01/02/18 15:11 99-65-012/29/17 10:1520.0 1
2,4-Dinitrophenol ND ug/L 01/02/18 15:11 51-28-512/29/17 10:1550.0 1
2,4-Dinitrotoluene ND ug/L 01/02/18 15:11 121-14-212/29/17 10:1510.0 1
2,6-Dinitrotoluene ND ug/L 01/02/18 15:11 606-20-212/29/17 10:1510.0 1
Di-n-octylphthalate ND ug/L 01/02/18 15:11 117-84-012/29/17 10:1510.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 13 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-1R Lab ID:92368450003 Collected:12/28/17 14:40 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Diphenylamine ND ug/L 01/02/18 15:11 122-39-412/29/17 10:1510.0 1
Disulfoton ND ug/L 01/02/18 15:11 298-04-412/29/17 10:1510.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 01/02/18 15:11 117-81-712/29/17 10:156.0 1
Ethyl methanesulfonate ND ug/L 01/02/18 15:11 62-50-012/29/17 10:1520.0 1
Famphur ND ug/L 01/02/18 15:11 52-85-712/29/17 10:1510.0 1
Fluoranthene ND ug/L 01/02/18 15:11 206-44-012/29/17 10:1510.0 1
Fluorene ND ug/L 01/02/18 15:11 86-73-712/29/17 10:1510.0 1
Hexachlorobenzene ND ug/L 01/02/18 15:11 118-74-112/29/17 10:1510.0 1
Hexachlorocyclopentadiene ND ug/L 01/02/18 15:11 77-47-412/29/17 10:1510.0 1
Hexachloroethane ND ug/L 01/02/18 15:11 67-72-112/29/17 10:1510.0 1
Hexachlorophene ND ug/L 01/02/18 15:11 70-30-412/29/17 10:151001
Indeno(1,2,3-cd)pyrene ND ug/L 01/02/18 15:11 193-39-512/29/17 10:1510.0 1
Isodrin ND ug/L 01/02/18 15:11 465-73-612/29/17 10:1520.0 1
Isophorone ND ug/L 01/02/18 15:11 78-59-112/29/17 10:1510.0 1
Isosafrole ND ug/L 01/02/18 15:11 120-58-112/29/17 10:1510.0 1
Kepone ND ug/L 01/02/18 15:11 143-50-012/29/17 10:1510.0 1
Methapyrilene ND ug/L 01/02/18 15:11 91-80-5 L212/29/17 10:1550.0 1
3-Methylcholanthrene ND ug/L 01/02/18 15:11 56-49-512/29/17 10:1510.0 1
Methyl methanesulfonate ND ug/L 01/02/18 15:11 66-27-3 L112/29/17 10:155.0 1
2-Methylnaphthalene ND ug/L 01/02/18 15:11 91-57-612/29/17 10:1510.0 1
Methyl parathion ND ug/L 01/02/18 15:11 298-00-012/29/17 10:1510.0 1
2-Methylphenol(o-Cresol)ND ug/L 01/02/18 15:11 95-48-712/29/17 10:1510.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 01/02/18 15:11 15831-10-412/29/17 10:1510.0 1
1-Naphthalenamine ND ug/L 01/02/18 15:11 134-32-712/29/17 10:155.0 1
2-Naphthalenamine ND ug/L 01/02/18 15:11 91-59-812/29/17 10:155.0 1
1,4-Naphthoquinone ND ug/L 01/02/18 15:11 130-15-412/29/17 10:155.0 1
2-Nitroaniline ND ug/L 01/02/18 15:11 88-74-412/29/17 10:1550.0 1
3-Nitroaniline ND ug/L 01/02/18 15:11 99-09-212/29/17 10:1550.0 1
4-Nitroaniline ND ug/L 01/02/18 15:11 100-01-612/29/17 10:1520.0 1
Nitrobenzene ND ug/L 01/02/18 15:11 98-95-312/29/17 10:1510.0 1
2-Nitrophenol ND ug/L 01/02/18 15:11 88-75-512/29/17 10:1510.0 1
4-Nitrophenol ND ug/L 01/02/18 15:11 100-02-712/29/17 10:1550.0 1
5-Nitro-o-toluidine ND ug/L 01/02/18 15:11 99-55-812/29/17 10:1510.0 1
N-Nitrosodiethylamine ND ug/L 01/02/18 15:11 55-18-512/29/17 10:1520.0 1
N-Nitrosodimethylamine ND ug/L 01/02/18 15:11 62-75-912/29/17 10:1510.0 1
N-Nitroso-di-n-butylamine ND ug/L 01/02/18 15:11 924-16-312/29/17 10:1510.0 1
N-Nitroso-di-n-propylamine ND ug/L 01/02/18 15:11 621-64-712/29/17 10:1510.0 1
N-Nitrosodiphenylamine ND ug/L 01/02/18 15:11 86-30-612/29/17 10:1510.0 1
N-Nitrosomethylethylamine ND ug/L 01/02/18 15:11 10595-95-612/29/17 10:1510.0 1
N-Nitrosopiperidine ND ug/L 01/02/18 15:11 100-75-412/29/17 10:1520.0 1
N-Nitrosopyrrolidine ND ug/L 01/02/18 15:11 930-55-212/29/17 10:1510.0 1
O,O,O-Triethylphosphorothioate ND ug/L 01/02/18 15:11 126-68-1 L212/29/17 10:1510.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 01/02/18 15:11 108-60-112/29/17 10:1510.0 1
Parathion (Ethyl parathion)ND ug/L 01/02/18 15:11 56-38-212/29/17 10:1510.0 1
Pentachlorobenzene ND ug/L 01/02/18 15:11 608-93-512/29/17 10:1510.0 1
Pentachloronitrobenzene ND ug/L 01/02/18 15:11 82-68-812/29/17 10:1520.0 1
Pentachlorophenol ND ug/L 01/02/18 15:11 87-86-512/29/17 10:1525.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-1R Lab ID:92368450003 Collected:12/28/17 14:40 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Phenacetin ND ug/L 01/02/18 15:11 62-44-212/29/17 10:1520.0 1
Phenanthrene ND ug/L 01/02/18 15:11 85-01-812/29/17 10:1510.0 1
Phenol ND ug/L 01/02/18 15:11 108-95-212/29/17 10:1510.0 1
p-Phenylenediamine ND ug/L 01/02/18 15:11 106-50-312/29/17 10:1510.0 1
Phorate ND ug/L 01/02/18 15:11 298-02-212/29/17 10:1510.0 1
Pronamide ND ug/L 01/02/18 15:11 23950-58-512/29/17 10:1510.0 1
Pyrene ND ug/L 01/02/18 15:11 129-00-012/29/17 10:1510.0 1
Safrole ND ug/L 01/02/18 15:11 94-59-712/29/17 10:1510.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 01/02/18 15:11 95-94-312/29/17 10:1510.0 1
2,3,4,6-Tetrachlorophenol ND ug/L 01/02/18 15:11 58-90-212/29/17 10:1510.0 1
Thionazin ND ug/L 01/02/18 15:11 297-97-212/29/17 10:1520.0 1
O-Toluidine ND ug/L 01/02/18 15:11 95-53-412/29/17 10:1510.0 1
2,4,5-Trichlorophenol ND ug/L 01/02/18 15:11 95-95-412/29/17 10:1510.0 1
2,4,6-Trichlorophenol ND ug/L 01/02/18 15:11 88-06-212/29/17 10:1510.0 1
1,3,5-Trinitrobenzene ND ug/L 01/02/18 15:11 99-35-4 L212/29/17 10:1510.0 1
Surrogates
Nitrobenzene-d5 (S)72 %01/02/18 15:11 4165-60-012/29/17 10:1521-110 1
2-Fluorobiphenyl (S)65 %01/02/18 15:11 321-60-812/29/17 10:1527-110 1
Terphenyl-d14 (S)55 %01/02/18 15:11 1718-51-012/29/17 10:1531-107 1
Phenol-d6 (S)18 %01/02/18 15:11 13127-88-312/29/17 10:1510-110 1
2-Fluorophenol (S)29 %01/02/18 15:11 367-12-412/29/17 10:1512-110 1
2,4,6-Tribromophenol (S)74 %01/02/18 15:11 118-79-612/29/17 10:1527-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/18 01:41 67-64-125.0 1
Acetonitrile ND ug/L 01/03/18 01:41 75-05-850.0 1
Acrolein ND ug/L 01/03/18 01:41 107-02-810.0 1
Acrylonitrile ND ug/L 01/03/18 01:41 107-13-110.0 1
Allyl chloride ND ug/L 01/03/18 01:41 107-05-12.0 1
Benzene ND ug/L 01/03/18 01:41 71-43-21.0 1
Bromochloromethane ND ug/L 01/03/18 01:41 74-97-51.0 1
Bromodichloromethane ND ug/L 01/03/18 01:41 75-27-41.0 1
Bromoform ND ug/L 01/03/18 01:41 75-25-21.0 1
Bromomethane ND ug/L 01/03/18 01:41 74-83-92.0 1
2-Butanone (MEK)ND ug/L 01/03/18 01:41 78-93-35.0 1
Carbon disulfide ND ug/L 01/03/18 01:41 75-15-02.0 1
Carbon tetrachloride ND ug/L 01/03/18 01:41 56-23-51.0 1
Chlorobenzene ND ug/L 01/03/18 01:41 108-90-71.0 1
Chloroethane ND ug/L 01/03/18 01:41 75-00-31.0 1
Chloroform ND ug/L 01/03/18 01:41 67-66-31.0 1
Chloromethane ND ug/L 01/03/18 01:41 74-87-31.0 1
Chloroprene ND ug/L 01/03/18 01:41 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/18 01:41 96-12-8 L22.0 1
Dibromochloromethane ND ug/L 01/03/18 01:41 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/18 01:41 106-93-41.0 1
Dibromomethane ND ug/L 01/03/18 01:41 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 01/03/18 01:41 95-50-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-1R Lab ID:92368450003 Collected:12/28/17 14:40 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,3-Dichlorobenzene ND ug/L 01/03/18 01:41 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 01/03/18 01:41 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/18 01:41 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 01/03/18 01:41 75-71-81.0 1
1,1-Dichloroethane ND ug/L 01/03/18 01:41 75-34-31.0 1
1,2-Dichloroethane ND ug/L 01/03/18 01:41 107-06-21.0 1
1,1-Dichloroethene ND ug/L 01/03/18 01:41 75-35-41.0 1
cis-1,2-Dichloroethene 0.76J ug/L 01/03/18 01:41 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 01/03/18 01:41 156-60-51.0 1
1,2-Dichloropropane ND ug/L 01/03/18 01:41 78-87-51.0 1
1,3-Dichloropropane ND ug/L 01/03/18 01:41 142-28-91.0 1
2,2-Dichloropropane ND ug/L 01/03/18 01:41 594-20-71.0 1
1,1-Dichloropropene ND ug/L 01/03/18 01:41 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 01/03/18 01:41 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 01/03/18 01:41 10061-02-61.0 1
Ethylbenzene ND ug/L 01/03/18 01:41 100-41-41.0 1
Ethyl methacrylate ND ug/L 01/03/18 01:41 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 01/03/18 01:41 87-68-31.0 1
2-Hexanone ND ug/L 01/03/18 01:41 591-78-65.0 1
Iodomethane ND ug/L 01/03/18 01:41 74-88-45.0 1
Isobutanol ND ug/L 01/03/18 01:41 78-83-11001
Methacrylonitrile ND ug/L 01/03/18 01:41 126-98-710.0 1
Methylene Chloride ND ug/L 01/03/18 01:41 75-09-21.0 1
Methyl methacrylate ND ug/L 01/03/18 01:41 80-62-6 L22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/18 01:41 108-10-15.0 1
Naphthalene ND ug/L 01/03/18 01:41 91-20-31.0 1
Propionitrile ND ug/L 01/03/18 01:41 107-12-020.0 1
Styrene ND ug/L 01/03/18 01:41 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/18 01:41 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/18 01:41 79-34-51.0 1
Tetrachloroethene ND ug/L 01/03/18 01:41 127-18-41.0 1
Tetrahydrofuran ND ug/L 01/03/18 01:41 109-99-910.0 1
Toluene ND ug/L 01/03/18 01:41 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 01/03/18 01:41 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 01/03/18 01:41 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 01/03/18 01:41 79-00-51.0 1
Trichloroethene 0.65J ug/L 01/03/18 01:41 79-01-61.0 1
Trichlorofluoromethane ND ug/L 01/03/18 01:41 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 01/03/18 01:41 96-18-41.0 1
Vinyl acetate ND ug/L 01/03/18 01:41 108-05-42.0 1
Vinyl chloride ND ug/L 01/03/18 01:41 75-01-41.0 1
Xylene (Total)ND ug/L 01/03/18 01:41 1330-20-71.0 1
m&p-Xylene ND ug/L 01/03/18 01:41 179601-23-12.0 1
o-Xylene ND ug/L 01/03/18 01:41 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)102 %01/03/18 01:41 460-00-470-130 1
1,2-Dichloroethane-d4 (S)91 %01/03/18 01:41 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 16 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-1R Lab ID:92368450003 Collected:12/28/17 14:40 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Surrogates
Toluene-d8 (S)109 %01/03/18 01:41 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 17 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-2R Lab ID:92368450004 Collected:12/28/17 15:25 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By STV 01/05/18 11:291
Collected Date 12/28/17 01/05/18 11:291
Collected Time 15:25 01/05/18 11:291
pH 6.4 Std. Units 01/05/18 11:290.10 1
Temperature 5.7 deg C 01/05/18 11:290.50 1
Static Water Level 8.30 feet 01/05/18 11:291
Specific Conductance 1320 umhos/cm 01/05/18 11:291.0 1
Oxygen, Dissolved 0.4 mg/L 01/05/18 11:29 7782-44-71
Total Well Depth 21 feet 01/05/18 11:291
REDOX -38.8 mV 01/05/18 11:291
Turbidity 2.4 NTU 01/05/18 11:291.0 1
Odor SULFURIC 01/05/18 11:291
Appearance CLEAR 01/05/18 11:291
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 01/02/18 16:18 309-00-212/29/17 10:130.050 1
alpha-BHC ND ug/L 01/02/18 16:18 319-84-612/29/17 10:130.050 1
beta-BHC ND ug/L 01/02/18 16:18 319-85-712/29/17 10:130.050 1
delta-BHC ND ug/L 01/02/18 16:18 319-86-812/29/17 10:130.050 1
gamma-BHC (Lindane)ND ug/L 01/02/18 16:18 58-89-912/29/17 10:130.050 1
Chlordane (Technical)ND ug/L 01/02/18 16:18 57-74-912/29/17 10:130.20 1
4,4'-DDD ND ug/L 01/02/18 16:18 72-54-812/29/17 10:130.050 1
4,4'-DDE ND ug/L 01/02/18 16:18 72-55-912/29/17 10:130.050 1
4,4'-DDT ND ug/L 01/02/18 16:18 50-29-312/29/17 10:130.050 1
Dieldrin ND ug/L 01/02/18 16:18 60-57-112/29/17 10:130.050 1
Endosulfan I ND ug/L 01/02/18 16:18 959-98-812/29/17 10:130.050 1
Endosulfan II ND ug/L 01/02/18 16:18 33213-65-912/29/17 10:130.050 1
Endosulfan sulfate ND ug/L 01/02/18 16:18 1031-07-812/29/17 10:130.050 1
Endrin ND ug/L 01/02/18 16:18 72-20-812/29/17 10:130.050 1
Endrin aldehyde ND ug/L 01/02/18 16:18 7421-93-412/29/17 10:130.050 1
Heptachlor ND ug/L 01/02/18 16:18 76-44-812/29/17 10:130.050 1
Heptachlor epoxide ND ug/L 01/02/18 16:18 1024-57-312/29/17 10:130.050 1
Methoxychlor ND ug/L 01/02/18 16:18 72-43-512/29/17 10:130.15 1
Toxaphene ND ug/L 01/02/18 16:18 8001-35-212/29/17 10:130.20 1
Surrogates
Tetrachloro-m-xylene (S)57 %01/02/18 16:18 877-09-812/29/17 10:1320-130 1
Decachlorobiphenyl (S)56 %01/02/18 16:18 2051-24-312/29/17 10:1320-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 01/02/18 14:10 12674-11-212/29/17 10:130.50 1
PCB-1221 (Aroclor 1221)ND ug/L 01/02/18 14:10 11104-28-212/29/17 10:130.50 1
PCB-1232 (Aroclor 1232)ND ug/L 01/02/18 14:10 11141-16-512/29/17 10:130.50 1
PCB-1242 (Aroclor 1242)ND ug/L 01/02/18 14:10 53469-21-912/29/17 10:130.50 1
PCB-1248 (Aroclor 1248)ND ug/L 01/02/18 14:10 12672-29-612/29/17 10:130.50 1
PCB-1254 (Aroclor 1254)ND ug/L 01/02/18 14:10 11097-69-112/29/17 10:130.50 1
PCB-1260 (Aroclor 1260)ND ug/L 01/02/18 14:10 11096-82-512/29/17 10:130.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 18 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-2R Lab ID:92368450004 Collected:12/28/17 15:25 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
Surrogates
Decachlorobiphenyl (S)58 %01/02/18 14:10 2051-24-312/29/17 10:1310-132 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 01/04/18 11:28 83-32-912/29/17 10:1510.0 1
Acenaphthylene ND ug/L 01/04/18 11:28 208-96-812/29/17 10:1510.0 1
Acetophenone ND ug/L 01/04/18 11:28 98-86-212/29/17 10:1510.0 1
2-Acetylaminofluorene ND ug/L 01/04/18 11:28 53-96-3 L212/29/17 10:1520.0 1
4-Aminobiphenyl ND ug/L 01/04/18 11:28 92-67-112/29/17 10:1510.0 1
Anthracene ND ug/L 01/04/18 11:28 120-12-712/29/17 10:1510.0 1
Benzo(a)anthracene ND ug/L 01/04/18 11:28 56-55-312/29/17 10:1510.0 1
Benzo(a)pyrene ND ug/L 01/04/18 11:28 50-32-812/29/17 10:1510.0 1
Benzo(b)fluoranthene ND ug/L 01/04/18 11:28 205-99-212/29/17 10:1510.0 1
Benzo(g,h,i)perylene ND ug/L 01/04/18 11:28 191-24-212/29/17 10:1510.0 1
Benzo(k)fluoranthene ND ug/L 01/04/18 11:28 207-08-912/29/17 10:1510.0 1
Benzyl alcohol ND ug/L 01/04/18 11:28 100-51-612/29/17 10:1520.0 1
4-Bromophenylphenyl ether ND ug/L 01/04/18 11:28 101-55-312/29/17 10:1510.0 1
Butylbenzylphthalate ND ug/L 01/04/18 11:28 85-68-712/29/17 10:1510.0 1
4-Chloro-3-methylphenol ND ug/L 01/04/18 11:28 59-50-712/29/17 10:1520.0 1
4-Chloroaniline ND ug/L 01/04/18 11:28 106-47-812/29/17 10:1520.0 1
Chlorobenzilate ND ug/L 01/04/18 11:28 510-15-612/29/17 10:1510.0 1
bis(2-Chloroethoxy)methane ND ug/L 01/04/18 11:28 111-91-112/29/17 10:1510.0 1
bis(2-Chloroethyl) ether ND ug/L 01/04/18 11:28 111-44-412/29/17 10:1510.0 1
2-Chloronaphthalene ND ug/L 01/04/18 11:28 91-58-712/29/17 10:1510.0 1
2-Chlorophenol ND ug/L 01/04/18 11:28 95-57-812/29/17 10:1510.0 1
4-Chlorophenylphenyl ether ND ug/L 01/04/18 11:28 7005-72-312/29/17 10:1510.0 1
Chrysene ND ug/L 01/04/18 11:28 218-01-912/29/17 10:1510.0 1
Diallate ND ug/L 01/04/18 11:28 2303-16-412/29/17 10:1510.0 1
Dibenz(a,h)anthracene ND ug/L 01/04/18 11:28 53-70-312/29/17 10:1510.0 1
Dibenzofuran ND ug/L 01/04/18 11:28 132-64-912/29/17 10:1510.0 1
3,3'-Dichlorobenzidine ND ug/L 01/04/18 11:28 91-94-112/29/17 10:1520.0 1
2,4-Dichlorophenol ND ug/L 01/04/18 11:28 120-83-212/29/17 10:1510.0 1
2,6-Dichlorophenol ND ug/L 01/04/18 11:28 87-65-012/29/17 10:1510.0 1
Diethylphthalate ND ug/L 01/04/18 11:28 84-66-212/29/17 10:1510.0 1
Dimethoate ND ug/L 01/04/18 11:28 60-51-512/29/17 10:1510.0 1
P-Dimethylaminoazobenzene ND ug/L 01/04/18 11:28 60-11-712/29/17 10:155.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 01/04/18 11:28 57-97-612/29/17 10:1510.0 1
3,3'-Dimethylbenzidine ND ug/L 01/04/18 11:28 119-93-712/29/17 10:1510.0 1
2,4-Dimethylphenol ND ug/L 01/04/18 11:28 105-67-912/29/17 10:1510.0 1
Dimethylphthalate ND ug/L 01/04/18 11:28 131-11-312/29/17 10:1510.0 1
Di-n-butylphthalate ND ug/L 01/04/18 11:28 84-74-212/29/17 10:1510.0 1
4,6-Dinitro-2-methylphenol ND ug/L 01/04/18 11:28 534-52-112/29/17 10:1520.0 1
1,3-Dinitrobenzene ND ug/L 01/04/18 11:28 99-65-012/29/17 10:1520.0 1
2,4-Dinitrophenol ND ug/L 01/04/18 11:28 51-28-512/29/17 10:1550.0 1
2,4-Dinitrotoluene ND ug/L 01/04/18 11:28 121-14-212/29/17 10:1510.0 1
2,6-Dinitrotoluene ND ug/L 01/04/18 11:28 606-20-212/29/17 10:1510.0 1
Di-n-octylphthalate ND ug/L 01/04/18 11:28 117-84-012/29/17 10:1510.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-2R Lab ID:92368450004 Collected:12/28/17 15:25 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Diphenylamine ND ug/L 01/04/18 11:28 122-39-412/29/17 10:1510.0 1
Disulfoton ND ug/L 01/04/18 11:28 298-04-412/29/17 10:1510.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 01/04/18 11:28 117-81-712/29/17 10:156.0 1
Ethyl methanesulfonate ND ug/L 01/04/18 11:28 62-50-012/29/17 10:1520.0 1
Famphur ND ug/L 01/04/18 11:28 52-85-712/29/17 10:1510.0 1
Fluoranthene ND ug/L 01/04/18 11:28 206-44-012/29/17 10:1510.0 1
Fluorene ND ug/L 01/04/18 11:28 86-73-712/29/17 10:1510.0 1
Hexachlorobenzene ND ug/L 01/04/18 11:28 118-74-112/29/17 10:1510.0 1
Hexachlorocyclopentadiene ND ug/L 01/04/18 11:28 77-47-412/29/17 10:1510.0 1
Hexachloroethane ND ug/L 01/04/18 11:28 67-72-112/29/17 10:1510.0 1
Hexachlorophene ND ug/L 01/04/18 11:28 70-30-412/29/17 10:151001
Indeno(1,2,3-cd)pyrene ND ug/L 01/04/18 11:28 193-39-512/29/17 10:1510.0 1
Isodrin ND ug/L 01/04/18 11:28 465-73-612/29/17 10:1520.0 1
Isophorone ND ug/L 01/04/18 11:28 78-59-112/29/17 10:1510.0 1
Isosafrole ND ug/L 01/04/18 11:28 120-58-112/29/17 10:1510.0 1
Kepone ND ug/L 01/04/18 11:28 143-50-012/29/17 10:1510.0 1
Methapyrilene ND ug/L 01/04/18 11:28 91-80-5 L212/29/17 10:1550.0 1
3-Methylcholanthrene ND ug/L 01/04/18 11:28 56-49-512/29/17 10:1510.0 1
Methyl methanesulfonate ND ug/L 01/04/18 11:28 66-27-3 L112/29/17 10:155.0 1
2-Methylnaphthalene ND ug/L 01/04/18 11:28 91-57-612/29/17 10:1510.0 1
Methyl parathion ND ug/L 01/04/18 11:28 298-00-012/29/17 10:1510.0 1
2-Methylphenol(o-Cresol)ND ug/L 01/04/18 11:28 95-48-712/29/17 10:1510.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 01/04/18 11:28 15831-10-412/29/17 10:1510.0 1
1-Naphthalenamine ND ug/L 01/04/18 11:28 134-32-712/29/17 10:155.0 1
2-Naphthalenamine ND ug/L 01/04/18 11:28 91-59-812/29/17 10:155.0 1
1,4-Naphthoquinone ND ug/L 01/04/18 11:28 130-15-412/29/17 10:155.0 1
2-Nitroaniline ND ug/L 01/04/18 11:28 88-74-412/29/17 10:1550.0 1
3-Nitroaniline ND ug/L 01/04/18 11:28 99-09-212/29/17 10:1550.0 1
4-Nitroaniline ND ug/L 01/04/18 11:28 100-01-612/29/17 10:1520.0 1
Nitrobenzene ND ug/L 01/04/18 11:28 98-95-312/29/17 10:1510.0 1
2-Nitrophenol ND ug/L 01/04/18 11:28 88-75-512/29/17 10:1510.0 1
4-Nitrophenol ND ug/L 01/04/18 11:28 100-02-712/29/17 10:1550.0 1
5-Nitro-o-toluidine ND ug/L 01/04/18 11:28 99-55-812/29/17 10:1510.0 1
N-Nitrosodiethylamine ND ug/L 01/04/18 11:28 55-18-512/29/17 10:1520.0 1
N-Nitrosodimethylamine ND ug/L 01/04/18 11:28 62-75-912/29/17 10:1510.0 1
N-Nitroso-di-n-butylamine ND ug/L 01/04/18 11:28 924-16-312/29/17 10:1510.0 1
N-Nitroso-di-n-propylamine ND ug/L 01/04/18 11:28 621-64-712/29/17 10:1510.0 1
N-Nitrosodiphenylamine ND ug/L 01/04/18 11:28 86-30-612/29/17 10:1510.0 1
N-Nitrosomethylethylamine ND ug/L 01/04/18 11:28 10595-95-612/29/17 10:1510.0 1
N-Nitrosopiperidine ND ug/L 01/04/18 11:28 100-75-412/29/17 10:1520.0 1
N-Nitrosopyrrolidine ND ug/L 01/04/18 11:28 930-55-212/29/17 10:1510.0 1
O,O,O-Triethylphosphorothioate ND ug/L 01/04/18 11:28 126-68-1 L212/29/17 10:1510.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 01/04/18 11:28 108-60-112/29/17 10:1510.0 1
Parathion (Ethyl parathion)ND ug/L 01/04/18 11:28 56-38-212/29/17 10:1510.0 1
Pentachlorobenzene ND ug/L 01/04/18 11:28 608-93-512/29/17 10:1510.0 1
Pentachloronitrobenzene ND ug/L 01/04/18 11:28 82-68-812/29/17 10:1520.0 1
Pentachlorophenol ND ug/L 01/04/18 11:28 87-86-512/29/17 10:1525.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-2R Lab ID:92368450004 Collected:12/28/17 15:25 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Phenacetin ND ug/L 01/04/18 11:28 62-44-212/29/17 10:1520.0 1
Phenanthrene ND ug/L 01/04/18 11:28 85-01-812/29/17 10:1510.0 1
Phenol ND ug/L 01/04/18 11:28 108-95-212/29/17 10:1510.0 1
p-Phenylenediamine ND ug/L 01/04/18 11:28 106-50-312/29/17 10:1510.0 1
Phorate ND ug/L 01/04/18 11:28 298-02-212/29/17 10:1510.0 1
Pronamide ND ug/L 01/04/18 11:28 23950-58-512/29/17 10:1510.0 1
Pyrene ND ug/L 01/04/18 11:28 129-00-012/29/17 10:1510.0 1
Safrole ND ug/L 01/04/18 11:28 94-59-712/29/17 10:1510.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 01/04/18 11:28 95-94-312/29/17 10:1510.0 1
2,3,4,6-Tetrachlorophenol ND ug/L 01/04/18 11:28 58-90-212/29/17 10:1510.0 1
Thionazin ND ug/L 01/04/18 11:28 297-97-212/29/17 10:1520.0 1
O-Toluidine ND ug/L 01/04/18 11:28 95-53-412/29/17 10:1510.0 1
2,4,5-Trichlorophenol ND ug/L 01/04/18 11:28 95-95-412/29/17 10:1510.0 1
2,4,6-Trichlorophenol ND ug/L 01/04/18 11:28 88-06-212/29/17 10:1510.0 1
1,3,5-Trinitrobenzene ND ug/L 01/04/18 11:28 99-35-4 L212/29/17 10:1510.0 1
Surrogates
Nitrobenzene-d5 (S)43 %01/04/18 11:28 4165-60-012/29/17 10:1521-110 1
2-Fluorobiphenyl (S)57 %01/04/18 11:28 321-60-812/29/17 10:1527-110 1
Terphenyl-d14 (S)53 %01/04/18 11:28 1718-51-012/29/17 10:1531-107 1
Phenol-d6 (S)13 %01/04/18 11:28 13127-88-312/29/17 10:1510-110 1
2-Fluorophenol (S)19 %01/04/18 11:28 367-12-412/29/17 10:1512-110 1
2,4,6-Tribromophenol (S)75 %01/04/18 11:28 118-79-612/29/17 10:1527-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/18 01:59 67-64-125.0 1
Acetonitrile ND ug/L 01/03/18 01:59 75-05-850.0 1
Acrolein ND ug/L 01/03/18 01:59 107-02-810.0 1
Acrylonitrile ND ug/L 01/03/18 01:59 107-13-110.0 1
Allyl chloride ND ug/L 01/03/18 01:59 107-05-12.0 1
Benzene 2.5 ug/L 01/03/18 01:59 71-43-21.0 1
Bromochloromethane ND ug/L 01/03/18 01:59 74-97-51.0 1
Bromodichloromethane ND ug/L 01/03/18 01:59 75-27-41.0 1
Bromoform ND ug/L 01/03/18 01:59 75-25-21.0 1
Bromomethane ND ug/L 01/03/18 01:59 74-83-92.0 1
2-Butanone (MEK)ND ug/L 01/03/18 01:59 78-93-35.0 1
Carbon disulfide ND ug/L 01/03/18 01:59 75-15-02.0 1
Carbon tetrachloride ND ug/L 01/03/18 01:59 56-23-51.0 1
Chlorobenzene ND ug/L 01/03/18 01:59 108-90-71.0 1
Chloroethane ND ug/L 01/03/18 01:59 75-00-3 M11.0 1
Chloroform ND ug/L 01/03/18 01:59 67-66-31.0 1
Chloromethane ND ug/L 01/03/18 01:59 74-87-31.0 1
Chloroprene ND ug/L 01/03/18 01:59 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/18 01:59 96-12-8 L22.0 1
Dibromochloromethane ND ug/L 01/03/18 01:59 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/18 01:59 106-93-41.0 1
Dibromomethane ND ug/L 01/03/18 01:59 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 01/03/18 01:59 95-50-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-2R Lab ID:92368450004 Collected:12/28/17 15:25 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,3-Dichlorobenzene ND ug/L 01/03/18 01:59 541-73-11.0 1
1,4-Dichlorobenzene 0.37J ug/L 01/03/18 01:59 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/18 01:59 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 01/03/18 01:59 75-71-8 M11.0 1
1,1-Dichloroethane 0.54J ug/L 01/03/18 01:59 75-34-31.0 1
1,2-Dichloroethane ND ug/L 01/03/18 01:59 107-06-21.0 1
1,1-Dichloroethene ND ug/L 01/03/18 01:59 75-35-41.0 1
cis-1,2-Dichloroethene 0.66J ug/L 01/03/18 01:59 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 01/03/18 01:59 156-60-51.0 1
1,2-Dichloropropane ND ug/L 01/03/18 01:59 78-87-51.0 1
1,3-Dichloropropane ND ug/L 01/03/18 01:59 142-28-91.0 1
2,2-Dichloropropane ND ug/L 01/03/18 01:59 594-20-71.0 1
1,1-Dichloropropene ND ug/L 01/03/18 01:59 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 01/03/18 01:59 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 01/03/18 01:59 10061-02-61.0 1
Ethylbenzene ND ug/L 01/03/18 01:59 100-41-41.0 1
Ethyl methacrylate ND ug/L 01/03/18 01:59 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 01/03/18 01:59 87-68-31.0 1
2-Hexanone ND ug/L 01/03/18 01:59 591-78-65.0 1
Iodomethane ND ug/L 01/03/18 01:59 74-88-45.0 1
Isobutanol ND ug/L 01/03/18 01:59 78-83-11001
Methacrylonitrile ND ug/L 01/03/18 01:59 126-98-710.0 1
Methylene Chloride 1.1 ug/L 01/03/18 01:59 75-09-2 C91.0 1
Methyl methacrylate ND ug/L 01/03/18 01:59 80-62-6 L22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/18 01:59 108-10-15.0 1
Naphthalene ND ug/L 01/03/18 01:59 91-20-31.0 1
Propionitrile ND ug/L 01/03/18 01:59 107-12-020.0 1
Styrene ND ug/L 01/03/18 01:59 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/18 01:59 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/18 01:59 79-34-51.0 1
Tetrachloroethene 1.5 ug/L 01/03/18 01:59 127-18-41.0 1
Tetrahydrofuran 59.1 ug/L 01/03/18 01:59 109-99-9 M110.0 1
Toluene ND ug/L 01/03/18 01:59 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 01/03/18 01:59 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 01/03/18 01:59 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 01/03/18 01:59 79-00-51.0 1
Trichloroethene 1.3 ug/L 01/03/18 01:59 79-01-61.0 1
Trichlorofluoromethane ND ug/L 01/03/18 01:59 75-69-4 M11.0 1
1,2,3-Trichloropropane ND ug/L 01/03/18 01:59 96-18-41.0 1
Vinyl acetate ND ug/L 01/03/18 01:59 108-05-42.0 1
Vinyl chloride 1.4 ug/L 01/03/18 01:59 75-01-4 M11.0 1
Xylene (Total)ND ug/L 01/03/18 01:59 1330-20-71.0 1
m&p-Xylene ND ug/L 01/03/18 01:59 179601-23-12.0 1
o-Xylene ND ug/L 01/03/18 01:59 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)101 %01/03/18 01:59 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %01/03/18 01:59 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
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Page 22 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-2R Lab ID:92368450004 Collected:12/28/17 15:25 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Surrogates
Toluene-d8 (S)108 %01/03/18 01:59 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 23 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-3R Lab ID:92368450005 Collected:12/28/17 11:40 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By GLG 01/05/18 11:361
Collected Date 12/28/17 01/05/18 11:361
Collected Time 11:40 01/05/18 11:361
pH 6.4 Std. Units 01/05/18 11:360.10 1
Temperature 7.7 deg C 01/05/18 11:360.50 1
Static Water Level 21.15 feet 01/05/18 11:361
Specific Conductance 383.6 umhos/cm 01/05/18 11:361.0 1
Oxygen, Dissolved 0.5 mg/L 01/05/18 11:36 7782-44-71
Total Well Depth 27.0 feet 01/05/18 11:361
REDOX -37.4 mV 01/05/18 11:361
Turbidity 9.4 NTU 01/05/18 11:361.0 1
Odor NONE 01/05/18 11:361
Appearance CLEAR 01/05/18 11:361
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 01/02/18 16:35 309-00-212/29/17 10:130.050 1
alpha-BHC ND ug/L 01/02/18 16:35 319-84-612/29/17 10:130.050 1
beta-BHC ND ug/L 01/02/18 16:35 319-85-712/29/17 10:130.050 1
delta-BHC ND ug/L 01/02/18 16:35 319-86-812/29/17 10:130.050 1
gamma-BHC (Lindane)ND ug/L 01/02/18 16:35 58-89-912/29/17 10:130.050 1
Chlordane (Technical)ND ug/L 01/02/18 16:35 57-74-912/29/17 10:130.20 1
4,4'-DDD ND ug/L 01/02/18 16:35 72-54-812/29/17 10:130.050 1
4,4'-DDE ND ug/L 01/02/18 16:35 72-55-912/29/17 10:130.050 1
4,4'-DDT ND ug/L 01/02/18 16:35 50-29-312/29/17 10:130.050 1
Dieldrin ND ug/L 01/02/18 16:35 60-57-112/29/17 10:130.050 1
Endosulfan I ND ug/L 01/02/18 16:35 959-98-812/29/17 10:130.050 1
Endosulfan II ND ug/L 01/02/18 16:35 33213-65-912/29/17 10:130.050 1
Endosulfan sulfate ND ug/L 01/02/18 16:35 1031-07-812/29/17 10:130.050 1
Endrin ND ug/L 01/02/18 16:35 72-20-812/29/17 10:130.050 1
Endrin aldehyde ND ug/L 01/02/18 16:35 7421-93-412/29/17 10:130.050 1
Heptachlor ND ug/L 01/02/18 16:35 76-44-812/29/17 10:130.050 1
Heptachlor epoxide ND ug/L 01/02/18 16:35 1024-57-312/29/17 10:130.050 1
Methoxychlor ND ug/L 01/02/18 16:35 72-43-512/29/17 10:130.15 1
Toxaphene ND ug/L 01/02/18 16:35 8001-35-212/29/17 10:130.20 1
Surrogates
Tetrachloro-m-xylene (S)63 %01/02/18 16:35 877-09-812/29/17 10:1320-130 1
Decachlorobiphenyl (S)70 %01/02/18 16:35 2051-24-312/29/17 10:1320-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 01/02/18 14:31 12674-11-212/29/17 10:130.50 1
PCB-1221 (Aroclor 1221)ND ug/L 01/02/18 14:31 11104-28-212/29/17 10:130.50 1
PCB-1232 (Aroclor 1232)ND ug/L 01/02/18 14:31 11141-16-512/29/17 10:130.50 1
PCB-1242 (Aroclor 1242)ND ug/L 01/02/18 14:31 53469-21-912/29/17 10:130.50 1
PCB-1248 (Aroclor 1248)ND ug/L 01/02/18 14:31 12672-29-612/29/17 10:130.50 1
PCB-1254 (Aroclor 1254)ND ug/L 01/02/18 14:31 11097-69-112/29/17 10:130.50 1
PCB-1260 (Aroclor 1260)ND ug/L 01/02/18 14:31 11096-82-512/29/17 10:130.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 24 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-3R Lab ID:92368450005 Collected:12/28/17 11:40 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
Surrogates
Decachlorobiphenyl (S)72 %01/02/18 14:31 2051-24-312/29/17 10:1310-132 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 01/02/18 16:10 83-32-912/29/17 10:1510.0 1
Acenaphthylene ND ug/L 01/02/18 16:10 208-96-812/29/17 10:1510.0 1
Acetophenone ND ug/L 01/02/18 16:10 98-86-212/29/17 10:1510.0 1
2-Acetylaminofluorene ND ug/L 01/02/18 16:10 53-96-3 L212/29/17 10:1520.0 1
4-Aminobiphenyl ND ug/L 01/02/18 16:10 92-67-112/29/17 10:1510.0 1
Anthracene ND ug/L 01/02/18 16:10 120-12-712/29/17 10:1510.0 1
Benzo(a)anthracene ND ug/L 01/02/18 16:10 56-55-312/29/17 10:1510.0 1
Benzo(a)pyrene ND ug/L 01/02/18 16:10 50-32-812/29/17 10:1510.0 1
Benzo(b)fluoranthene ND ug/L 01/02/18 16:10 205-99-212/29/17 10:1510.0 1
Benzo(g,h,i)perylene ND ug/L 01/02/18 16:10 191-24-212/29/17 10:1510.0 1
Benzo(k)fluoranthene ND ug/L 01/02/18 16:10 207-08-912/29/17 10:1510.0 1
Benzyl alcohol ND ug/L 01/02/18 16:10 100-51-612/29/17 10:1520.0 1
4-Bromophenylphenyl ether ND ug/L 01/02/18 16:10 101-55-312/29/17 10:1510.0 1
Butylbenzylphthalate ND ug/L 01/02/18 16:10 85-68-712/29/17 10:1510.0 1
4-Chloro-3-methylphenol ND ug/L 01/02/18 16:10 59-50-712/29/17 10:1520.0 1
4-Chloroaniline ND ug/L 01/02/18 16:10 106-47-812/29/17 10:1520.0 1
Chlorobenzilate ND ug/L 01/02/18 16:10 510-15-612/29/17 10:1510.0 1
bis(2-Chloroethoxy)methane ND ug/L 01/02/18 16:10 111-91-112/29/17 10:1510.0 1
bis(2-Chloroethyl) ether ND ug/L 01/02/18 16:10 111-44-412/29/17 10:1510.0 1
2-Chloronaphthalene ND ug/L 01/02/18 16:10 91-58-712/29/17 10:1510.0 1
2-Chlorophenol ND ug/L 01/02/18 16:10 95-57-812/29/17 10:1510.0 1
4-Chlorophenylphenyl ether ND ug/L 01/02/18 16:10 7005-72-312/29/17 10:1510.0 1
Chrysene ND ug/L 01/02/18 16:10 218-01-912/29/17 10:1510.0 1
Diallate ND ug/L 01/02/18 16:10 2303-16-412/29/17 10:1510.0 1
Dibenz(a,h)anthracene ND ug/L 01/02/18 16:10 53-70-312/29/17 10:1510.0 1
Dibenzofuran ND ug/L 01/02/18 16:10 132-64-912/29/17 10:1510.0 1
3,3'-Dichlorobenzidine ND ug/L 01/02/18 16:10 91-94-112/29/17 10:1520.0 1
2,4-Dichlorophenol ND ug/L 01/02/18 16:10 120-83-212/29/17 10:1510.0 1
2,6-Dichlorophenol ND ug/L 01/02/18 16:10 87-65-012/29/17 10:1510.0 1
Diethylphthalate ND ug/L 01/02/18 16:10 84-66-212/29/17 10:1510.0 1
Dimethoate ND ug/L 01/02/18 16:10 60-51-512/29/17 10:1510.0 1
P-Dimethylaminoazobenzene ND ug/L 01/02/18 16:10 60-11-712/29/17 10:155.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 01/02/18 16:10 57-97-612/29/17 10:1510.0 1
3,3'-Dimethylbenzidine ND ug/L 01/02/18 16:10 119-93-712/29/17 10:1510.0 1
2,4-Dimethylphenol ND ug/L 01/02/18 16:10 105-67-912/29/17 10:1510.0 1
Dimethylphthalate ND ug/L 01/02/18 16:10 131-11-312/29/17 10:1510.0 1
Di-n-butylphthalate ND ug/L 01/02/18 16:10 84-74-212/29/17 10:1510.0 1
4,6-Dinitro-2-methylphenol ND ug/L 01/02/18 16:10 534-52-112/29/17 10:1520.0 1
1,3-Dinitrobenzene ND ug/L 01/02/18 16:10 99-65-012/29/17 10:1520.0 1
2,4-Dinitrophenol ND ug/L 01/02/18 16:10 51-28-512/29/17 10:1550.0 1
2,4-Dinitrotoluene ND ug/L 01/02/18 16:10 121-14-212/29/17 10:1510.0 1
2,6-Dinitrotoluene ND ug/L 01/02/18 16:10 606-20-212/29/17 10:1510.0 1
Di-n-octylphthalate ND ug/L 01/02/18 16:10 117-84-012/29/17 10:1510.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 25 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-3R Lab ID:92368450005 Collected:12/28/17 11:40 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Diphenylamine ND ug/L 01/02/18 16:10 122-39-412/29/17 10:1510.0 1
Disulfoton ND ug/L 01/02/18 16:10 298-04-412/29/17 10:1510.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 01/02/18 16:10 117-81-712/29/17 10:156.0 1
Ethyl methanesulfonate ND ug/L 01/02/18 16:10 62-50-012/29/17 10:1520.0 1
Famphur ND ug/L 01/02/18 16:10 52-85-712/29/17 10:1510.0 1
Fluoranthene ND ug/L 01/02/18 16:10 206-44-012/29/17 10:1510.0 1
Fluorene ND ug/L 01/02/18 16:10 86-73-712/29/17 10:1510.0 1
Hexachlorobenzene ND ug/L 01/02/18 16:10 118-74-112/29/17 10:1510.0 1
Hexachlorocyclopentadiene ND ug/L 01/02/18 16:10 77-47-412/29/17 10:1510.0 1
Hexachloroethane ND ug/L 01/02/18 16:10 67-72-112/29/17 10:1510.0 1
Hexachlorophene ND ug/L 01/02/18 16:10 70-30-412/29/17 10:151001
Indeno(1,2,3-cd)pyrene ND ug/L 01/02/18 16:10 193-39-512/29/17 10:1510.0 1
Isodrin ND ug/L 01/02/18 16:10 465-73-612/29/17 10:1520.0 1
Isophorone ND ug/L 01/02/18 16:10 78-59-112/29/17 10:1510.0 1
Isosafrole ND ug/L 01/02/18 16:10 120-58-112/29/17 10:1510.0 1
Kepone ND ug/L 01/02/18 16:10 143-50-012/29/17 10:1510.0 1
Methapyrilene ND ug/L 01/02/18 16:10 91-80-5 L212/29/17 10:1550.0 1
3-Methylcholanthrene ND ug/L 01/02/18 16:10 56-49-512/29/17 10:1510.0 1
Methyl methanesulfonate ND ug/L 01/02/18 16:10 66-27-3 L112/29/17 10:155.0 1
2-Methylnaphthalene ND ug/L 01/02/18 16:10 91-57-612/29/17 10:1510.0 1
Methyl parathion ND ug/L 01/02/18 16:10 298-00-012/29/17 10:1510.0 1
2-Methylphenol(o-Cresol)ND ug/L 01/02/18 16:10 95-48-712/29/17 10:1510.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 01/02/18 16:10 15831-10-412/29/17 10:1510.0 1
1-Naphthalenamine ND ug/L 01/02/18 16:10 134-32-712/29/17 10:155.0 1
2-Naphthalenamine ND ug/L 01/02/18 16:10 91-59-812/29/17 10:155.0 1
1,4-Naphthoquinone ND ug/L 01/02/18 16:10 130-15-412/29/17 10:155.0 1
2-Nitroaniline ND ug/L 01/02/18 16:10 88-74-412/29/17 10:1550.0 1
3-Nitroaniline ND ug/L 01/02/18 16:10 99-09-212/29/17 10:1550.0 1
4-Nitroaniline ND ug/L 01/02/18 16:10 100-01-612/29/17 10:1520.0 1
Nitrobenzene ND ug/L 01/02/18 16:10 98-95-312/29/17 10:1510.0 1
2-Nitrophenol ND ug/L 01/02/18 16:10 88-75-512/29/17 10:1510.0 1
4-Nitrophenol ND ug/L 01/02/18 16:10 100-02-712/29/17 10:1550.0 1
5-Nitro-o-toluidine ND ug/L 01/02/18 16:10 99-55-812/29/17 10:1510.0 1
N-Nitrosodiethylamine ND ug/L 01/02/18 16:10 55-18-512/29/17 10:1520.0 1
N-Nitrosodimethylamine ND ug/L 01/02/18 16:10 62-75-912/29/17 10:1510.0 1
N-Nitroso-di-n-butylamine ND ug/L 01/02/18 16:10 924-16-312/29/17 10:1510.0 1
N-Nitroso-di-n-propylamine ND ug/L 01/02/18 16:10 621-64-712/29/17 10:1510.0 1
N-Nitrosodiphenylamine ND ug/L 01/02/18 16:10 86-30-612/29/17 10:1510.0 1
N-Nitrosomethylethylamine ND ug/L 01/02/18 16:10 10595-95-612/29/17 10:1510.0 1
N-Nitrosopiperidine ND ug/L 01/02/18 16:10 100-75-412/29/17 10:1520.0 1
N-Nitrosopyrrolidine ND ug/L 01/02/18 16:10 930-55-212/29/17 10:1510.0 1
O,O,O-Triethylphosphorothioate ND ug/L 01/02/18 16:10 126-68-1 L212/29/17 10:1510.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 01/02/18 16:10 108-60-112/29/17 10:1510.0 1
Parathion (Ethyl parathion)ND ug/L 01/02/18 16:10 56-38-212/29/17 10:1510.0 1
Pentachlorobenzene ND ug/L 01/02/18 16:10 608-93-512/29/17 10:1510.0 1
Pentachloronitrobenzene ND ug/L 01/02/18 16:10 82-68-812/29/17 10:1520.0 1
Pentachlorophenol ND ug/L 01/02/18 16:10 87-86-512/29/17 10:1525.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-3R Lab ID:92368450005 Collected:12/28/17 11:40 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Phenacetin ND ug/L 01/02/18 16:10 62-44-212/29/17 10:1520.0 1
Phenanthrene ND ug/L 01/02/18 16:10 85-01-812/29/17 10:1510.0 1
Phenol ND ug/L 01/02/18 16:10 108-95-212/29/17 10:1510.0 1
p-Phenylenediamine ND ug/L 01/02/18 16:10 106-50-312/29/17 10:1510.0 1
Phorate ND ug/L 01/02/18 16:10 298-02-212/29/17 10:1510.0 1
Pronamide ND ug/L 01/02/18 16:10 23950-58-512/29/17 10:1510.0 1
Pyrene ND ug/L 01/02/18 16:10 129-00-012/29/17 10:1510.0 1
Safrole ND ug/L 01/02/18 16:10 94-59-712/29/17 10:1510.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 01/02/18 16:10 95-94-312/29/17 10:1510.0 1
2,3,4,6-Tetrachlorophenol ND ug/L 01/02/18 16:10 58-90-212/29/17 10:1510.0 1
Thionazin ND ug/L 01/02/18 16:10 297-97-212/29/17 10:1520.0 1
O-Toluidine ND ug/L 01/02/18 16:10 95-53-412/29/17 10:1510.0 1
2,4,5-Trichlorophenol ND ug/L 01/02/18 16:10 95-95-412/29/17 10:1510.0 1
2,4,6-Trichlorophenol ND ug/L 01/02/18 16:10 88-06-212/29/17 10:1510.0 1
1,3,5-Trinitrobenzene ND ug/L 01/02/18 16:10 99-35-4 L212/29/17 10:1510.0 1
Surrogates
Nitrobenzene-d5 (S)47 %01/02/18 16:10 4165-60-012/29/17 10:1521-110 1
2-Fluorobiphenyl (S)45 %01/02/18 16:10 321-60-812/29/17 10:1527-110 1
Terphenyl-d14 (S)50 %01/02/18 16:10 1718-51-012/29/17 10:1531-107 1
Phenol-d6 (S)12 %01/02/18 16:10 13127-88-312/29/17 10:1510-110 1
2-Fluorophenol (S)22 %01/02/18 16:10 367-12-412/29/17 10:1512-110 1
2,4,6-Tribromophenol (S)61 %01/02/18 16:10 118-79-612/29/17 10:1527-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/18 02:16 67-64-125.0 1
Acetonitrile ND ug/L 01/03/18 02:16 75-05-850.0 1
Acrolein ND ug/L 01/03/18 02:16 107-02-810.0 1
Acrylonitrile ND ug/L 01/03/18 02:16 107-13-110.0 1
Allyl chloride ND ug/L 01/03/18 02:16 107-05-12.0 1
Benzene ND ug/L 01/03/18 02:16 71-43-21.0 1
Bromochloromethane ND ug/L 01/03/18 02:16 74-97-51.0 1
Bromodichloromethane ND ug/L 01/03/18 02:16 75-27-41.0 1
Bromoform ND ug/L 01/03/18 02:16 75-25-21.0 1
Bromomethane ND ug/L 01/03/18 02:16 74-83-92.0 1
2-Butanone (MEK)ND ug/L 01/03/18 02:16 78-93-35.0 1
Carbon disulfide ND ug/L 01/03/18 02:16 75-15-02.0 1
Carbon tetrachloride ND ug/L 01/03/18 02:16 56-23-51.0 1
Chlorobenzene ND ug/L 01/03/18 02:16 108-90-71.0 1
Chloroethane ND ug/L 01/03/18 02:16 75-00-31.0 1
Chloroform ND ug/L 01/03/18 02:16 67-66-31.0 1
Chloromethane ND ug/L 01/03/18 02:16 74-87-31.0 1
Chloroprene ND ug/L 01/03/18 02:16 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/18 02:16 96-12-8 L22.0 1
Dibromochloromethane ND ug/L 01/03/18 02:16 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/18 02:16 106-93-41.0 1
Dibromomethane ND ug/L 01/03/18 02:16 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 01/03/18 02:16 95-50-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
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Page 27 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-3R Lab ID:92368450005 Collected:12/28/17 11:40 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,3-Dichlorobenzene ND ug/L 01/03/18 02:16 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 01/03/18 02:16 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/18 02:16 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 01/03/18 02:16 75-71-81.0 1
1,1-Dichloroethane ND ug/L 01/03/18 02:16 75-34-31.0 1
1,2-Dichloroethane ND ug/L 01/03/18 02:16 107-06-21.0 1
1,1-Dichloroethene ND ug/L 01/03/18 02:16 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 01/03/18 02:16 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 01/03/18 02:16 156-60-51.0 1
1,2-Dichloropropane ND ug/L 01/03/18 02:16 78-87-51.0 1
1,3-Dichloropropane ND ug/L 01/03/18 02:16 142-28-91.0 1
2,2-Dichloropropane ND ug/L 01/03/18 02:16 594-20-71.0 1
1,1-Dichloropropene ND ug/L 01/03/18 02:16 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 01/03/18 02:16 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 01/03/18 02:16 10061-02-61.0 1
Ethylbenzene ND ug/L 01/03/18 02:16 100-41-41.0 1
Ethyl methacrylate ND ug/L 01/03/18 02:16 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 01/03/18 02:16 87-68-31.0 1
2-Hexanone ND ug/L 01/03/18 02:16 591-78-65.0 1
Iodomethane ND ug/L 01/03/18 02:16 74-88-45.0 1
Isobutanol ND ug/L 01/03/18 02:16 78-83-11001
Methacrylonitrile ND ug/L 01/03/18 02:16 126-98-710.0 1
Methylene Chloride ND ug/L 01/03/18 02:16 75-09-21.0 1
Methyl methacrylate ND ug/L 01/03/18 02:16 80-62-6 L22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/18 02:16 108-10-15.0 1
Naphthalene ND ug/L 01/03/18 02:16 91-20-31.0 1
Propionitrile ND ug/L 01/03/18 02:16 107-12-020.0 1
Styrene ND ug/L 01/03/18 02:16 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/18 02:16 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/18 02:16 79-34-51.0 1
Tetrachloroethene ND ug/L 01/03/18 02:16 127-18-41.0 1
Tetrahydrofuran ND ug/L 01/03/18 02:16 109-99-910.0 1
Toluene ND ug/L 01/03/18 02:16 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 01/03/18 02:16 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 01/03/18 02:16 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 01/03/18 02:16 79-00-51.0 1
Trichloroethene ND ug/L 01/03/18 02:16 79-01-61.0 1
Trichlorofluoromethane ND ug/L 01/03/18 02:16 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 01/03/18 02:16 96-18-41.0 1
Vinyl acetate ND ug/L 01/03/18 02:16 108-05-42.0 1
Vinyl chloride ND ug/L 01/03/18 02:16 75-01-41.0 1
Xylene (Total)ND ug/L 01/03/18 02:16 1330-20-71.0 1
m&p-Xylene ND ug/L 01/03/18 02:16 179601-23-12.0 1
o-Xylene ND ug/L 01/03/18 02:16 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)100 %01/03/18 02:16 460-00-470-130 1
1,2-Dichloroethane-d4 (S)87 %01/03/18 02:16 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-3R Lab ID:92368450005 Collected:12/28/17 11:40 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Surrogates
Toluene-d8 (S)111 %01/03/18 02:16 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 29 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-5R Lab ID:92368450006 Collected:12/28/17 15:30 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By GLG 01/05/18 11:391
Collected Date 12/28/17 01/05/18 11:391
Collected Time 15:30 01/05/18 11:391
pH 6.1 Std. Units 01/05/18 11:390.10 1
Temperature 11.4 deg C 01/05/18 11:390.50 1
Static Water Level 11.5 feet 01/05/18 11:391
Specific Conductance 175.1 umhos/cm 01/05/18 11:391.0 1
Oxygen, Dissolved 5.1 mg/L 01/05/18 11:39 7782-44-71
Total Well Depth 50.0 feet 01/05/18 11:391
REDOX 106.5 mV 01/05/18 11:391
Turbidity 4.2 NTU 01/05/18 11:391.0 1
Odor NONE 01/05/18 11:391
Appearance CLEAR 01/05/18 11:391
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 01/02/18 16:53 309-00-212/29/17 10:130.050 1
alpha-BHC ND ug/L 01/02/18 16:53 319-84-612/29/17 10:130.050 1
beta-BHC ND ug/L 01/02/18 16:53 319-85-712/29/17 10:130.050 1
delta-BHC ND ug/L 01/02/18 16:53 319-86-812/29/17 10:130.050 1
gamma-BHC (Lindane)ND ug/L 01/02/18 16:53 58-89-912/29/17 10:130.050 1
Chlordane (Technical)ND ug/L 01/02/18 16:53 57-74-912/29/17 10:130.20 1
4,4'-DDD ND ug/L 01/02/18 16:53 72-54-812/29/17 10:130.050 1
4,4'-DDE ND ug/L 01/02/18 16:53 72-55-912/29/17 10:130.050 1
4,4'-DDT ND ug/L 01/02/18 16:53 50-29-312/29/17 10:130.050 1
Dieldrin ND ug/L 01/02/18 16:53 60-57-112/29/17 10:130.050 1
Endosulfan I ND ug/L 01/02/18 16:53 959-98-812/29/17 10:130.050 1
Endosulfan II ND ug/L 01/02/18 16:53 33213-65-912/29/17 10:130.050 1
Endosulfan sulfate ND ug/L 01/02/18 16:53 1031-07-812/29/17 10:130.050 1
Endrin ND ug/L 01/02/18 16:53 72-20-812/29/17 10:130.050 1
Endrin aldehyde ND ug/L 01/02/18 16:53 7421-93-412/29/17 10:130.050 1
Heptachlor ND ug/L 01/02/18 16:53 76-44-812/29/17 10:130.050 1
Heptachlor epoxide ND ug/L 01/02/18 16:53 1024-57-312/29/17 10:130.050 1
Methoxychlor ND ug/L 01/02/18 16:53 72-43-512/29/17 10:130.15 1
Toxaphene ND ug/L 01/02/18 16:53 8001-35-212/29/17 10:130.20 1
Surrogates
Tetrachloro-m-xylene (S)63 %01/02/18 16:53 877-09-812/29/17 10:1320-130 1
Decachlorobiphenyl (S)56 %01/02/18 16:53 2051-24-312/29/17 10:1320-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 01/02/18 14:52 12674-11-212/29/17 10:130.50 1
PCB-1221 (Aroclor 1221)ND ug/L 01/02/18 14:52 11104-28-212/29/17 10:130.50 1
PCB-1232 (Aroclor 1232)ND ug/L 01/02/18 14:52 11141-16-512/29/17 10:130.50 1
PCB-1242 (Aroclor 1242)ND ug/L 01/02/18 14:52 53469-21-912/29/17 10:130.50 1
PCB-1248 (Aroclor 1248)ND ug/L 01/02/18 14:52 12672-29-612/29/17 10:130.50 1
PCB-1254 (Aroclor 1254)ND ug/L 01/02/18 14:52 11097-69-112/29/17 10:130.50 1
PCB-1260 (Aroclor 1260)ND ug/L 01/02/18 14:52 11096-82-512/29/17 10:130.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-5R Lab ID:92368450006 Collected:12/28/17 15:30 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
Surrogates
Decachlorobiphenyl (S)58 %01/02/18 14:52 2051-24-312/29/17 10:1310-132 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 01/04/18 12:03 83-32-912/29/17 10:1510.0 1
Acenaphthylene ND ug/L 01/04/18 12:03 208-96-812/29/17 10:1510.0 1
Acetophenone ND ug/L 01/04/18 12:03 98-86-212/29/17 10:1510.0 1
2-Acetylaminofluorene ND ug/L 01/04/18 12:03 53-96-3 L212/29/17 10:1520.0 1
4-Aminobiphenyl ND ug/L 01/04/18 12:03 92-67-112/29/17 10:1510.0 1
Anthracene ND ug/L 01/04/18 12:03 120-12-712/29/17 10:1510.0 1
Benzo(a)anthracene ND ug/L 01/04/18 12:03 56-55-312/29/17 10:1510.0 1
Benzo(a)pyrene ND ug/L 01/04/18 12:03 50-32-812/29/17 10:1510.0 1
Benzo(b)fluoranthene ND ug/L 01/04/18 12:03 205-99-212/29/17 10:1510.0 1
Benzo(g,h,i)perylene ND ug/L 01/04/18 12:03 191-24-212/29/17 10:1510.0 1
Benzo(k)fluoranthene ND ug/L 01/04/18 12:03 207-08-912/29/17 10:1510.0 1
Benzyl alcohol ND ug/L 01/04/18 12:03 100-51-612/29/17 10:1520.0 1
4-Bromophenylphenyl ether ND ug/L 01/04/18 12:03 101-55-312/29/17 10:1510.0 1
Butylbenzylphthalate ND ug/L 01/04/18 12:03 85-68-712/29/17 10:1510.0 1
4-Chloro-3-methylphenol ND ug/L 01/04/18 12:03 59-50-712/29/17 10:1520.0 1
4-Chloroaniline ND ug/L 01/04/18 12:03 106-47-812/29/17 10:1520.0 1
Chlorobenzilate ND ug/L 01/04/18 12:03 510-15-612/29/17 10:1510.0 1
bis(2-Chloroethoxy)methane ND ug/L 01/04/18 12:03 111-91-112/29/17 10:1510.0 1
bis(2-Chloroethyl) ether ND ug/L 01/04/18 12:03 111-44-412/29/17 10:1510.0 1
2-Chloronaphthalene ND ug/L 01/04/18 12:03 91-58-712/29/17 10:1510.0 1
2-Chlorophenol ND ug/L 01/04/18 12:03 95-57-812/29/17 10:1510.0 1
4-Chlorophenylphenyl ether ND ug/L 01/04/18 12:03 7005-72-312/29/17 10:1510.0 1
Chrysene ND ug/L 01/04/18 12:03 218-01-912/29/17 10:1510.0 1
Diallate ND ug/L 01/04/18 12:03 2303-16-412/29/17 10:1510.0 1
Dibenz(a,h)anthracene ND ug/L 01/04/18 12:03 53-70-312/29/17 10:1510.0 1
Dibenzofuran ND ug/L 01/04/18 12:03 132-64-912/29/17 10:1510.0 1
3,3'-Dichlorobenzidine ND ug/L 01/04/18 12:03 91-94-112/29/17 10:1520.0 1
2,4-Dichlorophenol ND ug/L 01/04/18 12:03 120-83-212/29/17 10:1510.0 1
2,6-Dichlorophenol ND ug/L 01/04/18 12:03 87-65-012/29/17 10:1510.0 1
Diethylphthalate ND ug/L 01/04/18 12:03 84-66-212/29/17 10:1510.0 1
Dimethoate ND ug/L 01/04/18 12:03 60-51-512/29/17 10:1510.0 1
P-Dimethylaminoazobenzene ND ug/L 01/04/18 12:03 60-11-712/29/17 10:155.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 01/04/18 12:03 57-97-612/29/17 10:1510.0 1
3,3'-Dimethylbenzidine ND ug/L 01/04/18 12:03 119-93-712/29/17 10:1510.0 1
2,4-Dimethylphenol ND ug/L 01/04/18 12:03 105-67-912/29/17 10:1510.0 1
Dimethylphthalate ND ug/L 01/04/18 12:03 131-11-312/29/17 10:1510.0 1
Di-n-butylphthalate ND ug/L 01/04/18 12:03 84-74-212/29/17 10:1510.0 1
4,6-Dinitro-2-methylphenol ND ug/L 01/04/18 12:03 534-52-112/29/17 10:1520.0 1
1,3-Dinitrobenzene ND ug/L 01/04/18 12:03 99-65-012/29/17 10:1520.0 1
2,4-Dinitrophenol ND ug/L 01/04/18 12:03 51-28-512/29/17 10:1550.0 1
2,4-Dinitrotoluene ND ug/L 01/04/18 12:03 121-14-212/29/17 10:1510.0 1
2,6-Dinitrotoluene ND ug/L 01/04/18 12:03 606-20-212/29/17 10:1510.0 1
Di-n-octylphthalate ND ug/L 01/04/18 12:03 117-84-012/29/17 10:1510.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-5R Lab ID:92368450006 Collected:12/28/17 15:30 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Diphenylamine ND ug/L 01/04/18 12:03 122-39-412/29/17 10:1510.0 1
Disulfoton ND ug/L 01/04/18 12:03 298-04-412/29/17 10:1510.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 01/04/18 12:03 117-81-712/29/17 10:156.0 1
Ethyl methanesulfonate ND ug/L 01/04/18 12:03 62-50-012/29/17 10:1520.0 1
Famphur ND ug/L 01/04/18 12:03 52-85-712/29/17 10:1510.0 1
Fluoranthene ND ug/L 01/04/18 12:03 206-44-012/29/17 10:1510.0 1
Fluorene ND ug/L 01/04/18 12:03 86-73-712/29/17 10:1510.0 1
Hexachlorobenzene ND ug/L 01/04/18 12:03 118-74-112/29/17 10:1510.0 1
Hexachlorocyclopentadiene ND ug/L 01/04/18 12:03 77-47-412/29/17 10:1510.0 1
Hexachloroethane ND ug/L 01/04/18 12:03 67-72-112/29/17 10:1510.0 1
Hexachlorophene ND ug/L 01/04/18 12:03 70-30-412/29/17 10:151001
Indeno(1,2,3-cd)pyrene ND ug/L 01/04/18 12:03 193-39-512/29/17 10:1510.0 1
Isodrin ND ug/L 01/04/18 12:03 465-73-612/29/17 10:1520.0 1
Isophorone ND ug/L 01/04/18 12:03 78-59-112/29/17 10:1510.0 1
Isosafrole ND ug/L 01/04/18 12:03 120-58-112/29/17 10:1510.0 1
Kepone ND ug/L 01/04/18 12:03 143-50-012/29/17 10:1510.0 1
Methapyrilene ND ug/L 01/04/18 12:03 91-80-5 L212/29/17 10:1550.0 1
3-Methylcholanthrene ND ug/L 01/04/18 12:03 56-49-512/29/17 10:1510.0 1
Methyl methanesulfonate ND ug/L 01/04/18 12:03 66-27-3 L112/29/17 10:155.0 1
2-Methylnaphthalene ND ug/L 01/04/18 12:03 91-57-612/29/17 10:1510.0 1
Methyl parathion ND ug/L 01/04/18 12:03 298-00-012/29/17 10:1510.0 1
2-Methylphenol(o-Cresol)ND ug/L 01/04/18 12:03 95-48-712/29/17 10:1510.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 01/04/18 12:03 15831-10-412/29/17 10:1510.0 1
1-Naphthalenamine ND ug/L 01/04/18 12:03 134-32-712/29/17 10:155.0 1
2-Naphthalenamine ND ug/L 01/04/18 12:03 91-59-812/29/17 10:155.0 1
1,4-Naphthoquinone ND ug/L 01/04/18 12:03 130-15-412/29/17 10:155.0 1
2-Nitroaniline ND ug/L 01/04/18 12:03 88-74-412/29/17 10:1550.0 1
3-Nitroaniline ND ug/L 01/04/18 12:03 99-09-212/29/17 10:1550.0 1
4-Nitroaniline ND ug/L 01/04/18 12:03 100-01-612/29/17 10:1520.0 1
Nitrobenzene ND ug/L 01/04/18 12:03 98-95-312/29/17 10:1510.0 1
2-Nitrophenol ND ug/L 01/04/18 12:03 88-75-512/29/17 10:1510.0 1
4-Nitrophenol ND ug/L 01/04/18 12:03 100-02-712/29/17 10:1550.0 1
5-Nitro-o-toluidine ND ug/L 01/04/18 12:03 99-55-812/29/17 10:1510.0 1
N-Nitrosodiethylamine ND ug/L 01/04/18 12:03 55-18-512/29/17 10:1520.0 1
N-Nitrosodimethylamine ND ug/L 01/04/18 12:03 62-75-912/29/17 10:1510.0 1
N-Nitroso-di-n-butylamine ND ug/L 01/04/18 12:03 924-16-312/29/17 10:1510.0 1
N-Nitroso-di-n-propylamine ND ug/L 01/04/18 12:03 621-64-712/29/17 10:1510.0 1
N-Nitrosodiphenylamine ND ug/L 01/04/18 12:03 86-30-612/29/17 10:1510.0 1
N-Nitrosomethylethylamine ND ug/L 01/04/18 12:03 10595-95-612/29/17 10:1510.0 1
N-Nitrosopiperidine ND ug/L 01/04/18 12:03 100-75-412/29/17 10:1520.0 1
N-Nitrosopyrrolidine ND ug/L 01/04/18 12:03 930-55-212/29/17 10:1510.0 1
O,O,O-Triethylphosphorothioate ND ug/L 01/04/18 12:03 126-68-1 L212/29/17 10:1510.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 01/04/18 12:03 108-60-112/29/17 10:1510.0 1
Parathion (Ethyl parathion)ND ug/L 01/04/18 12:03 56-38-212/29/17 10:1510.0 1
Pentachlorobenzene ND ug/L 01/04/18 12:03 608-93-512/29/17 10:1510.0 1
Pentachloronitrobenzene ND ug/L 01/04/18 12:03 82-68-812/29/17 10:1520.0 1
Pentachlorophenol ND ug/L 01/04/18 12:03 87-86-512/29/17 10:1525.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-5R Lab ID:92368450006 Collected:12/28/17 15:30 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Phenacetin ND ug/L 01/04/18 12:03 62-44-212/29/17 10:1520.0 1
Phenanthrene ND ug/L 01/04/18 12:03 85-01-812/29/17 10:1510.0 1
Phenol ND ug/L 01/04/18 12:03 108-95-212/29/17 10:1510.0 1
p-Phenylenediamine ND ug/L 01/04/18 12:03 106-50-312/29/17 10:1510.0 1
Phorate ND ug/L 01/04/18 12:03 298-02-212/29/17 10:1510.0 1
Pronamide ND ug/L 01/04/18 12:03 23950-58-512/29/17 10:1510.0 1
Pyrene ND ug/L 01/04/18 12:03 129-00-012/29/17 10:1510.0 1
Safrole ND ug/L 01/04/18 12:03 94-59-712/29/17 10:1510.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 01/04/18 12:03 95-94-312/29/17 10:1510.0 1
2,3,4,6-Tetrachlorophenol ND ug/L 01/04/18 12:03 58-90-212/29/17 10:1510.0 1
Thionazin ND ug/L 01/04/18 12:03 297-97-212/29/17 10:1520.0 1
O-Toluidine ND ug/L 01/04/18 12:03 95-53-412/29/17 10:1510.0 1
2,4,5-Trichlorophenol ND ug/L 01/04/18 12:03 95-95-412/29/17 10:1510.0 1
2,4,6-Trichlorophenol ND ug/L 01/04/18 12:03 88-06-212/29/17 10:1510.0 1
1,3,5-Trinitrobenzene ND ug/L 01/04/18 12:03 99-35-4 L212/29/17 10:1510.0 1
Surrogates
Nitrobenzene-d5 (S)70 %01/04/18 12:03 4165-60-012/29/17 10:1521-110 1
2-Fluorobiphenyl (S)64 %01/04/18 12:03 321-60-812/29/17 10:1527-110 1
Terphenyl-d14 (S)63 %01/04/18 12:03 1718-51-012/29/17 10:1531-107 1
Phenol-d6 (S)18 %01/04/18 12:03 13127-88-312/29/17 10:1510-110 1
2-Fluorophenol (S)32 %01/04/18 12:03 367-12-412/29/17 10:1512-110 1
2,4,6-Tribromophenol (S)73 %01/04/18 12:03 118-79-612/29/17 10:1527-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/18 02:33 67-64-125.0 1
Acetonitrile ND ug/L 01/03/18 02:33 75-05-850.0 1
Acrolein ND ug/L 01/03/18 02:33 107-02-810.0 1
Acrylonitrile ND ug/L 01/03/18 02:33 107-13-110.0 1
Allyl chloride ND ug/L 01/03/18 02:33 107-05-12.0 1
Benzene ND ug/L 01/03/18 02:33 71-43-21.0 1
Bromochloromethane ND ug/L 01/03/18 02:33 74-97-51.0 1
Bromodichloromethane ND ug/L 01/03/18 02:33 75-27-41.0 1
Bromoform ND ug/L 01/03/18 02:33 75-25-21.0 1
Bromomethane ND ug/L 01/03/18 02:33 74-83-92.0 1
2-Butanone (MEK)ND ug/L 01/03/18 02:33 78-93-35.0 1
Carbon disulfide ND ug/L 01/03/18 02:33 75-15-02.0 1
Carbon tetrachloride ND ug/L 01/03/18 02:33 56-23-51.0 1
Chlorobenzene ND ug/L 01/03/18 02:33 108-90-71.0 1
Chloroethane ND ug/L 01/03/18 02:33 75-00-31.0 1
Chloroform ND ug/L 01/03/18 02:33 67-66-31.0 1
Chloromethane ND ug/L 01/03/18 02:33 74-87-31.0 1
Chloroprene ND ug/L 01/03/18 02:33 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/18 02:33 96-12-8 L22.0 1
Dibromochloromethane ND ug/L 01/03/18 02:33 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/18 02:33 106-93-41.0 1
Dibromomethane ND ug/L 01/03/18 02:33 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 01/03/18 02:33 95-50-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 33 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-5R Lab ID:92368450006 Collected:12/28/17 15:30 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,3-Dichlorobenzene ND ug/L 01/03/18 02:33 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 01/03/18 02:33 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/18 02:33 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 01/03/18 02:33 75-71-81.0 1
1,1-Dichloroethane ND ug/L 01/03/18 02:33 75-34-31.0 1
1,2-Dichloroethane ND ug/L 01/03/18 02:33 107-06-21.0 1
1,1-Dichloroethene ND ug/L 01/03/18 02:33 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 01/03/18 02:33 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 01/03/18 02:33 156-60-51.0 1
1,2-Dichloropropane ND ug/L 01/03/18 02:33 78-87-51.0 1
1,3-Dichloropropane ND ug/L 01/03/18 02:33 142-28-91.0 1
2,2-Dichloropropane ND ug/L 01/03/18 02:33 594-20-71.0 1
1,1-Dichloropropene ND ug/L 01/03/18 02:33 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 01/03/18 02:33 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 01/03/18 02:33 10061-02-61.0 1
Ethylbenzene ND ug/L 01/03/18 02:33 100-41-41.0 1
Ethyl methacrylate ND ug/L 01/03/18 02:33 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 01/03/18 02:33 87-68-31.0 1
2-Hexanone ND ug/L 01/03/18 02:33 591-78-65.0 1
Iodomethane ND ug/L 01/03/18 02:33 74-88-45.0 1
Isobutanol ND ug/L 01/03/18 02:33 78-83-11001
Methacrylonitrile ND ug/L 01/03/18 02:33 126-98-710.0 1
Methylene Chloride ND ug/L 01/03/18 02:33 75-09-21.0 1
Methyl methacrylate ND ug/L 01/03/18 02:33 80-62-6 L22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/18 02:33 108-10-15.0 1
Naphthalene ND ug/L 01/03/18 02:33 91-20-31.0 1
Propionitrile ND ug/L 01/03/18 02:33 107-12-020.0 1
Styrene ND ug/L 01/03/18 02:33 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/18 02:33 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/18 02:33 79-34-51.0 1
Tetrachloroethene ND ug/L 01/03/18 02:33 127-18-41.0 1
Tetrahydrofuran ND ug/L 01/03/18 02:33 109-99-910.0 1
Toluene ND ug/L 01/03/18 02:33 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 01/03/18 02:33 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 01/03/18 02:33 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 01/03/18 02:33 79-00-51.0 1
Trichloroethene ND ug/L 01/03/18 02:33 79-01-61.0 1
Trichlorofluoromethane ND ug/L 01/03/18 02:33 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 01/03/18 02:33 96-18-41.0 1
Vinyl acetate ND ug/L 01/03/18 02:33 108-05-42.0 1
Vinyl chloride ND ug/L 01/03/18 02:33 75-01-41.0 1
Xylene (Total)ND ug/L 01/03/18 02:33 1330-20-71.0 1
m&p-Xylene ND ug/L 01/03/18 02:33 179601-23-12.0 1
o-Xylene ND ug/L 01/03/18 02:33 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)99 %01/03/18 02:33 460-00-470-130 1
1,2-Dichloroethane-d4 (S)90 %01/03/18 02:33 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-5R Lab ID:92368450006 Collected:12/28/17 15:30 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Surrogates
Toluene-d8 (S)105 %01/03/18 02:33 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-7 Lab ID:92368450007 Collected:12/28/17 12:50 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By GLG 01/05/18 11:401
Collected Date 12/28/17 01/05/18 11:401
Collected Time 12:50 01/05/18 11:401
pH 5.6 Std. Units 01/05/18 11:400.10 1
Temperature 9.9 deg C 01/05/18 11:400.50 1
Static Water Level 37.0 feet 01/05/18 11:401
Specific Conductance 236.6 umhos/cm 01/05/18 11:401.0 1
Oxygen, Dissolved 1.0 mg/L 01/05/18 11:40 7782-44-71
Total Well Depth 48.0 feet 01/05/18 11:401
REDOX 78.2 mV 01/05/18 11:401
Turbidity 3.5 NTU 01/05/18 11:401.0 1
Odor NONE 01/05/18 11:401
Appearance CLEAR 01/05/18 11:401
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 01/02/18 17:10 309-00-212/29/17 10:130.050 1
alpha-BHC ND ug/L 01/02/18 17:10 319-84-612/29/17 10:130.050 1
beta-BHC ND ug/L 01/02/18 17:10 319-85-712/29/17 10:130.050 1
delta-BHC ND ug/L 01/02/18 17:10 319-86-812/29/17 10:130.050 1
gamma-BHC (Lindane)ND ug/L 01/02/18 17:10 58-89-912/29/17 10:130.050 1
Chlordane (Technical)ND ug/L 01/02/18 17:10 57-74-912/29/17 10:130.20 1
4,4'-DDD ND ug/L 01/02/18 17:10 72-54-812/29/17 10:130.050 1
4,4'-DDE ND ug/L 01/02/18 17:10 72-55-912/29/17 10:130.050 1
4,4'-DDT ND ug/L 01/02/18 17:10 50-29-312/29/17 10:130.050 1
Dieldrin ND ug/L 01/02/18 17:10 60-57-112/29/17 10:130.050 1
Endosulfan I ND ug/L 01/02/18 17:10 959-98-812/29/17 10:130.050 1
Endosulfan II ND ug/L 01/02/18 17:10 33213-65-912/29/17 10:130.050 1
Endosulfan sulfate ND ug/L 01/02/18 17:10 1031-07-812/29/17 10:130.050 1
Endrin ND ug/L 01/02/18 17:10 72-20-812/29/17 10:130.050 1
Endrin aldehyde ND ug/L 01/02/18 17:10 7421-93-412/29/17 10:130.050 1
Heptachlor ND ug/L 01/02/18 17:10 76-44-812/29/17 10:130.050 1
Heptachlor epoxide ND ug/L 01/02/18 17:10 1024-57-312/29/17 10:130.050 1
Methoxychlor ND ug/L 01/02/18 17:10 72-43-512/29/17 10:130.15 1
Toxaphene ND ug/L 01/02/18 17:10 8001-35-212/29/17 10:130.20 1
Surrogates
Tetrachloro-m-xylene (S)75 %01/02/18 17:10 877-09-812/29/17 10:1320-130 1
Decachlorobiphenyl (S)71 %01/02/18 17:10 2051-24-312/29/17 10:1320-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 01/02/18 15:13 12674-11-212/29/17 10:130.50 1
PCB-1221 (Aroclor 1221)ND ug/L 01/02/18 15:13 11104-28-212/29/17 10:130.50 1
PCB-1232 (Aroclor 1232)ND ug/L 01/02/18 15:13 11141-16-512/29/17 10:130.50 1
PCB-1242 (Aroclor 1242)ND ug/L 01/02/18 15:13 53469-21-912/29/17 10:130.50 1
PCB-1248 (Aroclor 1248)ND ug/L 01/02/18 15:13 12672-29-612/29/17 10:130.50 1
PCB-1254 (Aroclor 1254)ND ug/L 01/02/18 15:13 11097-69-112/29/17 10:130.50 1
PCB-1260 (Aroclor 1260)ND ug/L 01/02/18 15:13 11096-82-512/29/17 10:130.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-7 Lab ID:92368450007 Collected:12/28/17 12:50 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
Surrogates
Decachlorobiphenyl (S)70 %01/02/18 15:13 2051-24-312/29/17 10:1310-132 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 01/02/18 17:08 83-32-912/29/17 10:1510.0 1
Acenaphthylene ND ug/L 01/02/18 17:08 208-96-812/29/17 10:1510.0 1
Acetophenone ND ug/L 01/02/18 17:08 98-86-212/29/17 10:1510.0 1
2-Acetylaminofluorene ND ug/L 01/02/18 17:08 53-96-3 L212/29/17 10:1520.0 1
4-Aminobiphenyl ND ug/L 01/02/18 17:08 92-67-112/29/17 10:1510.0 1
Anthracene ND ug/L 01/02/18 17:08 120-12-712/29/17 10:1510.0 1
Benzo(a)anthracene ND ug/L 01/02/18 17:08 56-55-312/29/17 10:1510.0 1
Benzo(a)pyrene ND ug/L 01/02/18 17:08 50-32-812/29/17 10:1510.0 1
Benzo(b)fluoranthene ND ug/L 01/02/18 17:08 205-99-212/29/17 10:1510.0 1
Benzo(g,h,i)perylene ND ug/L 01/02/18 17:08 191-24-212/29/17 10:1510.0 1
Benzo(k)fluoranthene ND ug/L 01/02/18 17:08 207-08-912/29/17 10:1510.0 1
Benzyl alcohol ND ug/L 01/02/18 17:08 100-51-612/29/17 10:1520.0 1
4-Bromophenylphenyl ether ND ug/L 01/02/18 17:08 101-55-312/29/17 10:1510.0 1
Butylbenzylphthalate ND ug/L 01/02/18 17:08 85-68-712/29/17 10:1510.0 1
4-Chloro-3-methylphenol ND ug/L 01/02/18 17:08 59-50-712/29/17 10:1520.0 1
4-Chloroaniline ND ug/L 01/02/18 17:08 106-47-812/29/17 10:1520.0 1
Chlorobenzilate ND ug/L 01/02/18 17:08 510-15-612/29/17 10:1510.0 1
bis(2-Chloroethoxy)methane ND ug/L 01/02/18 17:08 111-91-112/29/17 10:1510.0 1
bis(2-Chloroethyl) ether ND ug/L 01/02/18 17:08 111-44-412/29/17 10:1510.0 1
2-Chloronaphthalene ND ug/L 01/02/18 17:08 91-58-712/29/17 10:1510.0 1
2-Chlorophenol ND ug/L 01/02/18 17:08 95-57-812/29/17 10:1510.0 1
4-Chlorophenylphenyl ether ND ug/L 01/02/18 17:08 7005-72-312/29/17 10:1510.0 1
Chrysene ND ug/L 01/02/18 17:08 218-01-912/29/17 10:1510.0 1
Diallate ND ug/L 01/02/18 17:08 2303-16-412/29/17 10:1510.0 1
Dibenz(a,h)anthracene ND ug/L 01/02/18 17:08 53-70-312/29/17 10:1510.0 1
Dibenzofuran ND ug/L 01/02/18 17:08 132-64-912/29/17 10:1510.0 1
3,3'-Dichlorobenzidine ND ug/L 01/02/18 17:08 91-94-112/29/17 10:1520.0 1
2,4-Dichlorophenol ND ug/L 01/02/18 17:08 120-83-212/29/17 10:1510.0 1
2,6-Dichlorophenol ND ug/L 01/02/18 17:08 87-65-012/29/17 10:1510.0 1
Diethylphthalate ND ug/L 01/02/18 17:08 84-66-212/29/17 10:1510.0 1
Dimethoate ND ug/L 01/02/18 17:08 60-51-512/29/17 10:1510.0 1
P-Dimethylaminoazobenzene ND ug/L 01/02/18 17:08 60-11-712/29/17 10:155.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 01/02/18 17:08 57-97-612/29/17 10:1510.0 1
3,3'-Dimethylbenzidine ND ug/L 01/02/18 17:08 119-93-712/29/17 10:1510.0 1
2,4-Dimethylphenol ND ug/L 01/02/18 17:08 105-67-912/29/17 10:1510.0 1
Dimethylphthalate ND ug/L 01/02/18 17:08 131-11-312/29/17 10:1510.0 1
Di-n-butylphthalate ND ug/L 01/02/18 17:08 84-74-212/29/17 10:1510.0 1
4,6-Dinitro-2-methylphenol ND ug/L 01/02/18 17:08 534-52-112/29/17 10:1520.0 1
1,3-Dinitrobenzene ND ug/L 01/02/18 17:08 99-65-012/29/17 10:1520.0 1
2,4-Dinitrophenol ND ug/L 01/02/18 17:08 51-28-512/29/17 10:1550.0 1
2,4-Dinitrotoluene ND ug/L 01/02/18 17:08 121-14-212/29/17 10:1510.0 1
2,6-Dinitrotoluene ND ug/L 01/02/18 17:08 606-20-212/29/17 10:1510.0 1
Di-n-octylphthalate ND ug/L 01/02/18 17:08 117-84-012/29/17 10:1510.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-7 Lab ID:92368450007 Collected:12/28/17 12:50 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Diphenylamine ND ug/L 01/02/18 17:08 122-39-412/29/17 10:1510.0 1
Disulfoton ND ug/L 01/02/18 17:08 298-04-412/29/17 10:1510.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 01/02/18 17:08 117-81-712/29/17 10:156.0 1
Ethyl methanesulfonate ND ug/L 01/02/18 17:08 62-50-012/29/17 10:1520.0 1
Famphur ND ug/L 01/02/18 17:08 52-85-712/29/17 10:1510.0 1
Fluoranthene ND ug/L 01/02/18 17:08 206-44-012/29/17 10:1510.0 1
Fluorene ND ug/L 01/02/18 17:08 86-73-712/29/17 10:1510.0 1
Hexachlorobenzene ND ug/L 01/02/18 17:08 118-74-112/29/17 10:1510.0 1
Hexachlorocyclopentadiene ND ug/L 01/02/18 17:08 77-47-412/29/17 10:1510.0 1
Hexachloroethane ND ug/L 01/02/18 17:08 67-72-112/29/17 10:1510.0 1
Hexachlorophene ND ug/L 01/02/18 17:08 70-30-412/29/17 10:151001
Indeno(1,2,3-cd)pyrene ND ug/L 01/02/18 17:08 193-39-512/29/17 10:1510.0 1
Isodrin ND ug/L 01/02/18 17:08 465-73-612/29/17 10:1520.0 1
Isophorone ND ug/L 01/02/18 17:08 78-59-112/29/17 10:1510.0 1
Isosafrole ND ug/L 01/02/18 17:08 120-58-112/29/17 10:1510.0 1
Kepone ND ug/L 01/02/18 17:08 143-50-012/29/17 10:1510.0 1
Methapyrilene ND ug/L 01/02/18 17:08 91-80-5 L212/29/17 10:1550.0 1
3-Methylcholanthrene ND ug/L 01/02/18 17:08 56-49-512/29/17 10:1510.0 1
Methyl methanesulfonate ND ug/L 01/02/18 17:08 66-27-3 L112/29/17 10:155.0 1
2-Methylnaphthalene ND ug/L 01/02/18 17:08 91-57-612/29/17 10:1510.0 1
Methyl parathion ND ug/L 01/02/18 17:08 298-00-012/29/17 10:1510.0 1
2-Methylphenol(o-Cresol)ND ug/L 01/02/18 17:08 95-48-712/29/17 10:1510.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 01/02/18 17:08 15831-10-412/29/17 10:1510.0 1
1-Naphthalenamine ND ug/L 01/02/18 17:08 134-32-712/29/17 10:155.0 1
2-Naphthalenamine ND ug/L 01/02/18 17:08 91-59-812/29/17 10:155.0 1
1,4-Naphthoquinone ND ug/L 01/02/18 17:08 130-15-412/29/17 10:155.0 1
2-Nitroaniline ND ug/L 01/02/18 17:08 88-74-412/29/17 10:1550.0 1
3-Nitroaniline ND ug/L 01/02/18 17:08 99-09-212/29/17 10:1550.0 1
4-Nitroaniline ND ug/L 01/02/18 17:08 100-01-612/29/17 10:1520.0 1
Nitrobenzene ND ug/L 01/02/18 17:08 98-95-312/29/17 10:1510.0 1
2-Nitrophenol ND ug/L 01/02/18 17:08 88-75-512/29/17 10:1510.0 1
4-Nitrophenol ND ug/L 01/02/18 17:08 100-02-712/29/17 10:1550.0 1
5-Nitro-o-toluidine ND ug/L 01/02/18 17:08 99-55-812/29/17 10:1510.0 1
N-Nitrosodiethylamine ND ug/L 01/02/18 17:08 55-18-512/29/17 10:1520.0 1
N-Nitrosodimethylamine ND ug/L 01/02/18 17:08 62-75-912/29/17 10:1510.0 1
N-Nitroso-di-n-butylamine ND ug/L 01/02/18 17:08 924-16-312/29/17 10:1510.0 1
N-Nitroso-di-n-propylamine ND ug/L 01/02/18 17:08 621-64-712/29/17 10:1510.0 1
N-Nitrosodiphenylamine ND ug/L 01/02/18 17:08 86-30-612/29/17 10:1510.0 1
N-Nitrosomethylethylamine ND ug/L 01/02/18 17:08 10595-95-612/29/17 10:1510.0 1
N-Nitrosopiperidine ND ug/L 01/02/18 17:08 100-75-412/29/17 10:1520.0 1
N-Nitrosopyrrolidine ND ug/L 01/02/18 17:08 930-55-212/29/17 10:1510.0 1
O,O,O-Triethylphosphorothioate ND ug/L 01/02/18 17:08 126-68-1 L212/29/17 10:1510.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 01/02/18 17:08 108-60-112/29/17 10:1510.0 1
Parathion (Ethyl parathion)ND ug/L 01/02/18 17:08 56-38-212/29/17 10:1510.0 1
Pentachlorobenzene ND ug/L 01/02/18 17:08 608-93-512/29/17 10:1510.0 1
Pentachloronitrobenzene ND ug/L 01/02/18 17:08 82-68-812/29/17 10:1520.0 1
Pentachlorophenol ND ug/L 01/02/18 17:08 87-86-512/29/17 10:1525.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 38 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-7 Lab ID:92368450007 Collected:12/28/17 12:50 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Phenacetin ND ug/L 01/02/18 17:08 62-44-212/29/17 10:1520.0 1
Phenanthrene ND ug/L 01/02/18 17:08 85-01-812/29/17 10:1510.0 1
Phenol ND ug/L 01/02/18 17:08 108-95-212/29/17 10:1510.0 1
p-Phenylenediamine ND ug/L 01/02/18 17:08 106-50-312/29/17 10:1510.0 1
Phorate ND ug/L 01/02/18 17:08 298-02-212/29/17 10:1510.0 1
Pronamide ND ug/L 01/02/18 17:08 23950-58-512/29/17 10:1510.0 1
Pyrene ND ug/L 01/02/18 17:08 129-00-012/29/17 10:1510.0 1
Safrole ND ug/L 01/02/18 17:08 94-59-712/29/17 10:1510.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 01/02/18 17:08 95-94-312/29/17 10:1510.0 1
2,3,4,6-Tetrachlorophenol ND ug/L 01/02/18 17:08 58-90-212/29/17 10:1510.0 1
Thionazin ND ug/L 01/02/18 17:08 297-97-212/29/17 10:1520.0 1
O-Toluidine ND ug/L 01/02/18 17:08 95-53-412/29/17 10:1510.0 1
2,4,5-Trichlorophenol ND ug/L 01/02/18 17:08 95-95-412/29/17 10:1510.0 1
2,4,6-Trichlorophenol ND ug/L 01/02/18 17:08 88-06-212/29/17 10:1510.0 1
1,3,5-Trinitrobenzene ND ug/L 01/02/18 17:08 99-35-4 L212/29/17 10:1510.0 1
Surrogates
Nitrobenzene-d5 (S)76 %01/02/18 17:08 4165-60-012/29/17 10:1521-110 1
2-Fluorobiphenyl (S)72 %01/02/18 17:08 321-60-812/29/17 10:1527-110 1
Terphenyl-d14 (S)72 %01/02/18 17:08 1718-51-012/29/17 10:1531-107 1
Phenol-d6 (S)21 %01/02/18 17:08 13127-88-312/29/17 10:1510-110 1
2-Fluorophenol (S)35 %01/02/18 17:08 367-12-412/29/17 10:1512-110 1
2,4,6-Tribromophenol (S)84 %01/02/18 17:08 118-79-612/29/17 10:1527-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/18 02:50 67-64-125.0 1
Acetonitrile ND ug/L 01/03/18 02:50 75-05-850.0 1
Acrolein ND ug/L 01/03/18 02:50 107-02-810.0 1
Acrylonitrile ND ug/L 01/03/18 02:50 107-13-110.0 1
Allyl chloride ND ug/L 01/03/18 02:50 107-05-12.0 1
Benzene 0.39J ug/L 01/03/18 02:50 71-43-21.0 1
Bromochloromethane ND ug/L 01/03/18 02:50 74-97-51.0 1
Bromodichloromethane ND ug/L 01/03/18 02:50 75-27-41.0 1
Bromoform ND ug/L 01/03/18 02:50 75-25-21.0 1
Bromomethane ND ug/L 01/03/18 02:50 74-83-92.0 1
2-Butanone (MEK)ND ug/L 01/03/18 02:50 78-93-35.0 1
Carbon disulfide ND ug/L 01/03/18 02:50 75-15-02.0 1
Carbon tetrachloride ND ug/L 01/03/18 02:50 56-23-51.0 1
Chlorobenzene ND ug/L 01/03/18 02:50 108-90-71.0 1
Chloroethane ND ug/L 01/03/18 02:50 75-00-31.0 1
Chloroform ND ug/L 01/03/18 02:50 67-66-31.0 1
Chloromethane ND ug/L 01/03/18 02:50 74-87-31.0 1
Chloroprene ND ug/L 01/03/18 02:50 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/18 02:50 96-12-8 L22.0 1
Dibromochloromethane ND ug/L 01/03/18 02:50 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/18 02:50 106-93-41.0 1
Dibromomethane ND ug/L 01/03/18 02:50 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 01/03/18 02:50 95-50-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-7 Lab ID:92368450007 Collected:12/28/17 12:50 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,3-Dichlorobenzene ND ug/L 01/03/18 02:50 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 01/03/18 02:50 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/18 02:50 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 01/03/18 02:50 75-71-81.0 1
1,1-Dichloroethane 1.6 ug/L 01/03/18 02:50 75-34-31.0 1
1,2-Dichloroethane ND ug/L 01/03/18 02:50 107-06-21.0 1
1,1-Dichloroethene ND ug/L 01/03/18 02:50 75-35-41.0 1
cis-1,2-Dichloroethene 1.1 ug/L 01/03/18 02:50 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 01/03/18 02:50 156-60-51.0 1
1,2-Dichloropropane ND ug/L 01/03/18 02:50 78-87-51.0 1
1,3-Dichloropropane ND ug/L 01/03/18 02:50 142-28-91.0 1
2,2-Dichloropropane ND ug/L 01/03/18 02:50 594-20-71.0 1
1,1-Dichloropropene ND ug/L 01/03/18 02:50 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 01/03/18 02:50 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 01/03/18 02:50 10061-02-61.0 1
Ethylbenzene ND ug/L 01/03/18 02:50 100-41-41.0 1
Ethyl methacrylate ND ug/L 01/03/18 02:50 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 01/03/18 02:50 87-68-31.0 1
2-Hexanone ND ug/L 01/03/18 02:50 591-78-65.0 1
Iodomethane ND ug/L 01/03/18 02:50 74-88-45.0 1
Isobutanol ND ug/L 01/03/18 02:50 78-83-11001
Methacrylonitrile ND ug/L 01/03/18 02:50 126-98-710.0 1
Methylene Chloride 5.7 ug/L 01/03/18 02:50 75-09-21.0 1
Methyl methacrylate ND ug/L 01/03/18 02:50 80-62-6 L22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/18 02:50 108-10-15.0 1
Naphthalene ND ug/L 01/03/18 02:50 91-20-31.0 1
Propionitrile ND ug/L 01/03/18 02:50 107-12-020.0 1
Styrene ND ug/L 01/03/18 02:50 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/18 02:50 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/18 02:50 79-34-51.0 1
Tetrachloroethene ND ug/L 01/03/18 02:50 127-18-41.0 1
Tetrahydrofuran ND ug/L 01/03/18 02:50 109-99-910.0 1
Toluene ND ug/L 01/03/18 02:50 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 01/03/18 02:50 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 01/03/18 02:50 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 01/03/18 02:50 79-00-51.0 1
Trichloroethene 0.58J ug/L 01/03/18 02:50 79-01-61.0 1
Trichlorofluoromethane 1.6 ug/L 01/03/18 02:50 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 01/03/18 02:50 96-18-41.0 1
Vinyl acetate ND ug/L 01/03/18 02:50 108-05-42.0 1
Vinyl chloride ND ug/L 01/03/18 02:50 75-01-41.0 1
Xylene (Total)ND ug/L 01/03/18 02:50 1330-20-71.0 1
m&p-Xylene 1.6J ug/L 01/03/18 02:50 179601-23-12.0 1
o-Xylene 0.62J ug/L 01/03/18 02:50 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)102 %01/03/18 02:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)88 %01/03/18 02:50 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-7 Lab ID:92368450007 Collected:12/28/17 12:50 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Surrogates
Toluene-d8 (S)110 %01/03/18 02:50 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-9 Lab ID:92368450008 Collected:12/28/17 11:30 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By STV 01/05/18 11:451
Collected Date 12/28/17 01/05/18 11:451
Collected Time 11:30 01/05/18 11:451
pH 5.7 Std. Units 01/05/18 11:450.10 1
Temperature 11.0 deg C 01/05/18 11:450.50 1
Static Water Level 52.94 feet 01/05/18 11:451
Specific Conductance 148.6 umhos/cm 01/05/18 11:451.0 1
Oxygen, Dissolved 6.2 mg/L 01/05/18 11:45 7782-44-71
Total Well Depth 60 feet 01/05/18 11:451
REDOX 132.7 mV 01/05/18 11:451
Turbidity 9.6 NTU 01/05/18 11:451.0 1
Odor NONE 01/05/18 11:451
Appearance CLEAR 01/05/18 11:451
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 01/02/18 17:28 309-00-212/29/17 10:130.050 1
alpha-BHC ND ug/L 01/02/18 17:28 319-84-612/29/17 10:130.050 1
beta-BHC ND ug/L 01/02/18 17:28 319-85-712/29/17 10:130.050 1
delta-BHC ND ug/L 01/02/18 17:28 319-86-812/29/17 10:130.050 1
gamma-BHC (Lindane)ND ug/L 01/02/18 17:28 58-89-912/29/17 10:130.050 1
Chlordane (Technical)ND ug/L 01/02/18 17:28 57-74-912/29/17 10:130.20 1
4,4'-DDD ND ug/L 01/02/18 17:28 72-54-812/29/17 10:130.050 1
4,4'-DDE ND ug/L 01/02/18 17:28 72-55-912/29/17 10:130.050 1
4,4'-DDT ND ug/L 01/02/18 17:28 50-29-312/29/17 10:130.050 1
Dieldrin ND ug/L 01/02/18 17:28 60-57-112/29/17 10:130.050 1
Endosulfan I ND ug/L 01/02/18 17:28 959-98-812/29/17 10:130.050 1
Endosulfan II ND ug/L 01/02/18 17:28 33213-65-912/29/17 10:130.050 1
Endosulfan sulfate ND ug/L 01/02/18 17:28 1031-07-812/29/17 10:130.050 1
Endrin ND ug/L 01/02/18 17:28 72-20-812/29/17 10:130.050 1
Endrin aldehyde ND ug/L 01/02/18 17:28 7421-93-412/29/17 10:130.050 1
Heptachlor ND ug/L 01/02/18 17:28 76-44-812/29/17 10:130.050 1
Heptachlor epoxide ND ug/L 01/02/18 17:28 1024-57-312/29/17 10:130.050 1
Methoxychlor ND ug/L 01/02/18 17:28 72-43-512/29/17 10:130.15 1
Toxaphene ND ug/L 01/02/18 17:28 8001-35-212/29/17 10:130.20 1
Surrogates
Tetrachloro-m-xylene (S)60 %01/02/18 17:28 877-09-812/29/17 10:1320-130 1
Decachlorobiphenyl (S)49 %01/02/18 17:28 2051-24-312/29/17 10:1320-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 01/02/18 15:33 12674-11-212/29/17 10:130.50 1
PCB-1221 (Aroclor 1221)ND ug/L 01/02/18 15:33 11104-28-212/29/17 10:130.50 1
PCB-1232 (Aroclor 1232)ND ug/L 01/02/18 15:33 11141-16-512/29/17 10:130.50 1
PCB-1242 (Aroclor 1242)ND ug/L 01/02/18 15:33 53469-21-912/29/17 10:130.50 1
PCB-1248 (Aroclor 1248)ND ug/L 01/02/18 15:33 12672-29-612/29/17 10:130.50 1
PCB-1254 (Aroclor 1254)ND ug/L 01/02/18 15:33 11097-69-112/29/17 10:130.50 1
PCB-1260 (Aroclor 1260)ND ug/L 01/02/18 15:33 11096-82-512/29/17 10:130.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-9 Lab ID:92368450008 Collected:12/28/17 11:30 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
Surrogates
Decachlorobiphenyl (S)49 %01/02/18 15:33 2051-24-312/29/17 10:1310-132 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 01/03/18 14:52 83-32-912/29/17 10:1510.0 1
Acenaphthylene ND ug/L 01/03/18 14:52 208-96-812/29/17 10:1510.0 1
Acetophenone ND ug/L 01/03/18 14:52 98-86-212/29/17 10:1510.0 1
2-Acetylaminofluorene ND ug/L 01/03/18 14:52 53-96-3 L212/29/17 10:1520.0 1
4-Aminobiphenyl ND ug/L 01/03/18 14:52 92-67-112/29/17 10:1510.0 1
Anthracene ND ug/L 01/03/18 14:52 120-12-712/29/17 10:1510.0 1
Benzo(a)anthracene ND ug/L 01/03/18 14:52 56-55-312/29/17 10:1510.0 1
Benzo(a)pyrene ND ug/L 01/03/18 14:52 50-32-812/29/17 10:1510.0 1
Benzo(b)fluoranthene ND ug/L 01/03/18 14:52 205-99-212/29/17 10:1510.0 1
Benzo(g,h,i)perylene ND ug/L 01/03/18 14:52 191-24-212/29/17 10:1510.0 1
Benzo(k)fluoranthene ND ug/L 01/03/18 14:52 207-08-912/29/17 10:1510.0 1
Benzyl alcohol ND ug/L 01/03/18 14:52 100-51-612/29/17 10:1520.0 1
4-Bromophenylphenyl ether ND ug/L 01/03/18 14:52 101-55-312/29/17 10:1510.0 1
Butylbenzylphthalate ND ug/L 01/03/18 14:52 85-68-712/29/17 10:1510.0 1
4-Chloro-3-methylphenol ND ug/L 01/03/18 14:52 59-50-712/29/17 10:1520.0 1
4-Chloroaniline ND ug/L 01/03/18 14:52 106-47-812/29/17 10:1520.0 1
Chlorobenzilate ND ug/L 01/03/18 14:52 510-15-612/29/17 10:1510.0 1
bis(2-Chloroethoxy)methane ND ug/L 01/03/18 14:52 111-91-112/29/17 10:1510.0 1
bis(2-Chloroethyl) ether ND ug/L 01/03/18 14:52 111-44-412/29/17 10:1510.0 1
2-Chloronaphthalene ND ug/L 01/03/18 14:52 91-58-712/29/17 10:1510.0 1
2-Chlorophenol ND ug/L 01/03/18 14:52 95-57-812/29/17 10:1510.0 1
4-Chlorophenylphenyl ether ND ug/L 01/03/18 14:52 7005-72-312/29/17 10:1510.0 1
Chrysene ND ug/L 01/03/18 14:52 218-01-912/29/17 10:1510.0 1
Diallate ND ug/L 01/03/18 14:52 2303-16-412/29/17 10:1510.0 1
Dibenz(a,h)anthracene ND ug/L 01/03/18 14:52 53-70-312/29/17 10:1510.0 1
Dibenzofuran ND ug/L 01/03/18 14:52 132-64-912/29/17 10:1510.0 1
3,3'-Dichlorobenzidine ND ug/L 01/03/18 14:52 91-94-112/29/17 10:1520.0 1
2,4-Dichlorophenol ND ug/L 01/03/18 14:52 120-83-212/29/17 10:1510.0 1
2,6-Dichlorophenol ND ug/L 01/03/18 14:52 87-65-012/29/17 10:1510.0 1
Diethylphthalate ND ug/L 01/03/18 14:52 84-66-212/29/17 10:1510.0 1
Dimethoate ND ug/L 01/03/18 14:52 60-51-512/29/17 10:1510.0 1
P-Dimethylaminoazobenzene ND ug/L 01/03/18 14:52 60-11-712/29/17 10:155.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 01/03/18 14:52 57-97-612/29/17 10:1510.0 1
3,3'-Dimethylbenzidine ND ug/L 01/03/18 14:52 119-93-712/29/17 10:1510.0 1
2,4-Dimethylphenol ND ug/L 01/03/18 14:52 105-67-912/29/17 10:1510.0 1
Dimethylphthalate ND ug/L 01/03/18 14:52 131-11-312/29/17 10:1510.0 1
Di-n-butylphthalate ND ug/L 01/03/18 14:52 84-74-212/29/17 10:1510.0 1
4,6-Dinitro-2-methylphenol ND ug/L 01/03/18 14:52 534-52-112/29/17 10:1520.0 1
1,3-Dinitrobenzene ND ug/L 01/03/18 14:52 99-65-012/29/17 10:1520.0 1
2,4-Dinitrophenol ND ug/L 01/03/18 14:52 51-28-512/29/17 10:1550.0 1
2,4-Dinitrotoluene ND ug/L 01/03/18 14:52 121-14-212/29/17 10:1510.0 1
2,6-Dinitrotoluene ND ug/L 01/03/18 14:52 606-20-212/29/17 10:1510.0 1
Di-n-octylphthalate ND ug/L 01/03/18 14:52 117-84-012/29/17 10:1510.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-9 Lab ID:92368450008 Collected:12/28/17 11:30 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Diphenylamine ND ug/L 01/03/18 14:52 122-39-412/29/17 10:1510.0 1
Disulfoton ND ug/L 01/03/18 14:52 298-04-412/29/17 10:1510.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 01/03/18 14:52 117-81-712/29/17 10:156.0 1
Ethyl methanesulfonate ND ug/L 01/03/18 14:52 62-50-012/29/17 10:1520.0 1
Famphur ND ug/L 01/03/18 14:52 52-85-712/29/17 10:1510.0 1
Fluoranthene ND ug/L 01/03/18 14:52 206-44-012/29/17 10:1510.0 1
Fluorene ND ug/L 01/03/18 14:52 86-73-712/29/17 10:1510.0 1
Hexachlorobenzene ND ug/L 01/03/18 14:52 118-74-112/29/17 10:1510.0 1
Hexachlorocyclopentadiene ND ug/L 01/03/18 14:52 77-47-412/29/17 10:1510.0 1
Hexachloroethane ND ug/L 01/03/18 14:52 67-72-112/29/17 10:1510.0 1
Hexachlorophene ND ug/L 01/03/18 14:52 70-30-412/29/17 10:151001
Indeno(1,2,3-cd)pyrene ND ug/L 01/03/18 14:52 193-39-512/29/17 10:1510.0 1
Isodrin ND ug/L 01/03/18 14:52 465-73-612/29/17 10:1520.0 1
Isophorone ND ug/L 01/03/18 14:52 78-59-112/29/17 10:1510.0 1
Isosafrole ND ug/L 01/03/18 14:52 120-58-112/29/17 10:1510.0 1
Kepone ND ug/L 01/03/18 14:52 143-50-012/29/17 10:1510.0 1
Methapyrilene ND ug/L 01/03/18 14:52 91-80-5 L212/29/17 10:1550.0 1
3-Methylcholanthrene ND ug/L 01/03/18 14:52 56-49-512/29/17 10:1510.0 1
Methyl methanesulfonate ND ug/L 01/03/18 14:52 66-27-3 L112/29/17 10:155.0 1
2-Methylnaphthalene ND ug/L 01/03/18 14:52 91-57-612/29/17 10:1510.0 1
Methyl parathion ND ug/L 01/03/18 14:52 298-00-012/29/17 10:1510.0 1
2-Methylphenol(o-Cresol)ND ug/L 01/03/18 14:52 95-48-712/29/17 10:1510.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 01/03/18 14:52 15831-10-412/29/17 10:1510.0 1
1-Naphthalenamine ND ug/L 01/03/18 14:52 134-32-712/29/17 10:155.0 1
2-Naphthalenamine ND ug/L 01/03/18 14:52 91-59-812/29/17 10:155.0 1
1,4-Naphthoquinone ND ug/L 01/03/18 14:52 130-15-412/29/17 10:155.0 1
2-Nitroaniline ND ug/L 01/03/18 14:52 88-74-412/29/17 10:1550.0 1
3-Nitroaniline ND ug/L 01/03/18 14:52 99-09-212/29/17 10:1550.0 1
4-Nitroaniline ND ug/L 01/03/18 14:52 100-01-612/29/17 10:1520.0 1
Nitrobenzene ND ug/L 01/03/18 14:52 98-95-312/29/17 10:1510.0 1
2-Nitrophenol ND ug/L 01/03/18 14:52 88-75-512/29/17 10:1510.0 1
4-Nitrophenol ND ug/L 01/03/18 14:52 100-02-712/29/17 10:1550.0 1
5-Nitro-o-toluidine ND ug/L 01/03/18 14:52 99-55-812/29/17 10:1510.0 1
N-Nitrosodiethylamine ND ug/L 01/03/18 14:52 55-18-512/29/17 10:1520.0 1
N-Nitrosodimethylamine ND ug/L 01/03/18 14:52 62-75-912/29/17 10:1510.0 1
N-Nitroso-di-n-butylamine ND ug/L 01/03/18 14:52 924-16-312/29/17 10:1510.0 1
N-Nitroso-di-n-propylamine ND ug/L 01/03/18 14:52 621-64-712/29/17 10:1510.0 1
N-Nitrosodiphenylamine ND ug/L 01/03/18 14:52 86-30-612/29/17 10:1510.0 1
N-Nitrosomethylethylamine ND ug/L 01/03/18 14:52 10595-95-612/29/17 10:1510.0 1
N-Nitrosopiperidine ND ug/L 01/03/18 14:52 100-75-412/29/17 10:1520.0 1
N-Nitrosopyrrolidine ND ug/L 01/03/18 14:52 930-55-212/29/17 10:1510.0 1
O,O,O-Triethylphosphorothioate ND ug/L 01/03/18 14:52 126-68-1 L212/29/17 10:1510.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 01/03/18 14:52 108-60-112/29/17 10:1510.0 1
Parathion (Ethyl parathion)ND ug/L 01/03/18 14:52 56-38-212/29/17 10:1510.0 1
Pentachlorobenzene ND ug/L 01/03/18 14:52 608-93-512/29/17 10:1510.0 1
Pentachloronitrobenzene ND ug/L 01/03/18 14:52 82-68-812/29/17 10:1520.0 1
Pentachlorophenol ND ug/L 01/03/18 14:52 87-86-512/29/17 10:1525.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 44 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-9 Lab ID:92368450008 Collected:12/28/17 11:30 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Phenacetin ND ug/L 01/03/18 14:52 62-44-212/29/17 10:1520.0 1
Phenanthrene ND ug/L 01/03/18 14:52 85-01-812/29/17 10:1510.0 1
Phenol ND ug/L 01/03/18 14:52 108-95-212/29/17 10:1510.0 1
p-Phenylenediamine ND ug/L 01/03/18 14:52 106-50-312/29/17 10:1510.0 1
Phorate ND ug/L 01/03/18 14:52 298-02-212/29/17 10:1510.0 1
Pronamide ND ug/L 01/03/18 14:52 23950-58-512/29/17 10:1510.0 1
Pyrene ND ug/L 01/03/18 14:52 129-00-012/29/17 10:1510.0 1
Safrole ND ug/L 01/03/18 14:52 94-59-712/29/17 10:1510.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 01/03/18 14:52 95-94-312/29/17 10:1510.0 1
2,3,4,6-Tetrachlorophenol ND ug/L 01/03/18 14:52 58-90-212/29/17 10:1510.0 1
Thionazin ND ug/L 01/03/18 14:52 297-97-212/29/17 10:1520.0 1
O-Toluidine ND ug/L 01/03/18 14:52 95-53-412/29/17 10:1510.0 1
2,4,5-Trichlorophenol ND ug/L 01/03/18 14:52 95-95-412/29/17 10:1510.0 1
2,4,6-Trichlorophenol ND ug/L 01/03/18 14:52 88-06-212/29/17 10:1510.0 1
1,3,5-Trinitrobenzene ND ug/L 01/03/18 14:52 99-35-4 L212/29/17 10:1510.0 1
Surrogates
Nitrobenzene-d5 (S)38 %01/03/18 14:52 4165-60-012/29/17 10:1521-110 1
2-Fluorobiphenyl (S)37 %01/03/18 14:52 321-60-812/29/17 10:1527-110 1
Terphenyl-d14 (S)81 %01/03/18 14:52 1718-51-012/29/17 10:1531-107 1
Phenol-d6 (S)16 %01/03/18 14:52 13127-88-312/29/17 10:1510-110 1
2-Fluorophenol (S)21 %01/03/18 14:52 367-12-412/29/17 10:1512-110 1
2,4,6-Tribromophenol (S)75 %01/03/18 14:52 118-79-612/29/17 10:1527-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/18 03:08 67-64-125.0 1
Acetonitrile ND ug/L 01/03/18 03:08 75-05-850.0 1
Acrolein ND ug/L 01/03/18 03:08 107-02-810.0 1
Acrylonitrile ND ug/L 01/03/18 03:08 107-13-110.0 1
Allyl chloride ND ug/L 01/03/18 03:08 107-05-12.0 1
Benzene ND ug/L 01/03/18 03:08 71-43-21.0 1
Bromochloromethane ND ug/L 01/03/18 03:08 74-97-51.0 1
Bromodichloromethane ND ug/L 01/03/18 03:08 75-27-41.0 1
Bromoform ND ug/L 01/03/18 03:08 75-25-21.0 1
Bromomethane ND ug/L 01/03/18 03:08 74-83-92.0 1
2-Butanone (MEK)ND ug/L 01/03/18 03:08 78-93-35.0 1
Carbon disulfide ND ug/L 01/03/18 03:08 75-15-02.0 1
Carbon tetrachloride ND ug/L 01/03/18 03:08 56-23-51.0 1
Chlorobenzene ND ug/L 01/03/18 03:08 108-90-71.0 1
Chloroethane ND ug/L 01/03/18 03:08 75-00-31.0 1
Chloroform ND ug/L 01/03/18 03:08 67-66-31.0 1
Chloromethane ND ug/L 01/03/18 03:08 74-87-31.0 1
Chloroprene ND ug/L 01/03/18 03:08 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/18 03:08 96-12-8 L22.0 1
Dibromochloromethane ND ug/L 01/03/18 03:08 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/18 03:08 106-93-41.0 1
Dibromomethane ND ug/L 01/03/18 03:08 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 01/03/18 03:08 95-50-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-9 Lab ID:92368450008 Collected:12/28/17 11:30 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,3-Dichlorobenzene ND ug/L 01/03/18 03:08 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 01/03/18 03:08 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/18 03:08 110-57-61.0 1
Dichlorodifluoromethane 1.7 ug/L 01/03/18 03:08 75-71-81.0 1
1,1-Dichloroethane ND ug/L 01/03/18 03:08 75-34-31.0 1
1,2-Dichloroethane ND ug/L 01/03/18 03:08 107-06-21.0 1
1,1-Dichloroethene ND ug/L 01/03/18 03:08 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 01/03/18 03:08 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 01/03/18 03:08 156-60-51.0 1
1,2-Dichloropropane ND ug/L 01/03/18 03:08 78-87-51.0 1
1,3-Dichloropropane ND ug/L 01/03/18 03:08 142-28-91.0 1
2,2-Dichloropropane ND ug/L 01/03/18 03:08 594-20-71.0 1
1,1-Dichloropropene ND ug/L 01/03/18 03:08 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 01/03/18 03:08 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 01/03/18 03:08 10061-02-61.0 1
Ethylbenzene ND ug/L 01/03/18 03:08 100-41-41.0 1
Ethyl methacrylate ND ug/L 01/03/18 03:08 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 01/03/18 03:08 87-68-31.0 1
2-Hexanone ND ug/L 01/03/18 03:08 591-78-65.0 1
Iodomethane ND ug/L 01/03/18 03:08 74-88-45.0 1
Isobutanol ND ug/L 01/03/18 03:08 78-83-11001
Methacrylonitrile ND ug/L 01/03/18 03:08 126-98-710.0 1
Methylene Chloride ND ug/L 01/03/18 03:08 75-09-21.0 1
Methyl methacrylate ND ug/L 01/03/18 03:08 80-62-6 L22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/18 03:08 108-10-15.0 1
Naphthalene ND ug/L 01/03/18 03:08 91-20-31.0 1
Propionitrile ND ug/L 01/03/18 03:08 107-12-020.0 1
Styrene ND ug/L 01/03/18 03:08 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/18 03:08 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/18 03:08 79-34-51.0 1
Tetrachloroethene ND ug/L 01/03/18 03:08 127-18-41.0 1
Tetrahydrofuran ND ug/L 01/03/18 03:08 109-99-910.0 1
Toluene ND ug/L 01/03/18 03:08 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 01/03/18 03:08 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 01/03/18 03:08 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 01/03/18 03:08 79-00-51.0 1
Trichloroethene ND ug/L 01/03/18 03:08 79-01-61.0 1
Trichlorofluoromethane 1.4 ug/L 01/03/18 03:08 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 01/03/18 03:08 96-18-41.0 1
Vinyl acetate ND ug/L 01/03/18 03:08 108-05-42.0 1
Vinyl chloride ND ug/L 01/03/18 03:08 75-01-41.0 1
Xylene (Total)ND ug/L 01/03/18 03:08 1330-20-71.0 1
m&p-Xylene ND ug/L 01/03/18 03:08 179601-23-12.0 1
o-Xylene ND ug/L 01/03/18 03:08 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)100 %01/03/18 03:08 460-00-470-130 1
1,2-Dichloroethane-d4 (S)84 %01/03/18 03:08 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-9 Lab ID:92368450008 Collected:12/28/17 11:30 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Surrogates
Toluene-d8 (S)112 %01/03/18 03:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-10 Lab ID:92368450009 Collected:12/28/17 14:40 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JSH 01/05/18 11:461
Collected Date 12/28/17 01/05/18 11:461
Collected Time 14:40 01/05/18 11:461
pH 6.4 Std. Units 01/05/18 11:460.10 1
Temperature 11.7 deg C 01/05/18 11:460.50 1
Static Water Level 12.18 feet 01/05/18 11:461
Specific Conductance 1873 umhos/cm 01/05/18 11:461.0 1
Oxygen, Dissolved 0.1 mg/L 01/05/18 11:46 7782-44-71
Total Well Depth 21.0 feet 01/05/18 11:461
REDOX -50.6 mV 01/05/18 11:461
Turbidity 7.8 NTU 01/05/18 11:461.0 1
Odor SULFUR 01/05/18 11:461
Appearance SOAPY 01/05/18 11:461
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 01/02/18 17:46 309-00-212/29/17 10:130.050 1
alpha-BHC ND ug/L 01/02/18 17:46 319-84-612/29/17 10:130.050 1
beta-BHC ND ug/L 01/02/18 17:46 319-85-712/29/17 10:130.050 1
delta-BHC ND ug/L 01/02/18 17:46 319-86-812/29/17 10:130.050 1
gamma-BHC (Lindane)ND ug/L 01/02/18 17:46 58-89-912/29/17 10:130.050 1
Chlordane (Technical)ND ug/L 01/02/18 17:46 57-74-912/29/17 10:130.20 1
4,4'-DDD ND ug/L 01/02/18 17:46 72-54-812/29/17 10:130.050 1
4,4'-DDE ND ug/L 01/02/18 17:46 72-55-912/29/17 10:130.050 1
4,4'-DDT ND ug/L 01/02/18 17:46 50-29-312/29/17 10:130.050 1
Dieldrin ND ug/L 01/02/18 17:46 60-57-112/29/17 10:130.050 1
Endosulfan I ND ug/L 01/02/18 17:46 959-98-812/29/17 10:130.050 1
Endosulfan II ND ug/L 01/02/18 17:46 33213-65-912/29/17 10:130.050 1
Endosulfan sulfate ND ug/L 01/02/18 17:46 1031-07-812/29/17 10:130.050 1
Endrin ND ug/L 01/02/18 17:46 72-20-812/29/17 10:130.050 1
Endrin aldehyde ND ug/L 01/02/18 17:46 7421-93-412/29/17 10:130.050 1
Heptachlor ND ug/L 01/02/18 17:46 76-44-812/29/17 10:130.050 1
Heptachlor epoxide ND ug/L 01/02/18 17:46 1024-57-312/29/17 10:130.050 1
Methoxychlor ND ug/L 01/02/18 17:46 72-43-512/29/17 10:130.15 1
Toxaphene ND ug/L 01/02/18 17:46 8001-35-212/29/17 10:130.20 1
Surrogates
Tetrachloro-m-xylene (S)201 %01/02/18 17:46 877-09-8 S312/29/17 10:1320-130 1
Decachlorobiphenyl (S)59 %01/02/18 17:46 2051-24-312/29/17 10:1320-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 01/02/18 15:54 12674-11-212/29/17 10:130.50 1
PCB-1221 (Aroclor 1221)ND ug/L 01/02/18 15:54 11104-28-212/29/17 10:130.50 1
PCB-1232 (Aroclor 1232)ND ug/L 01/02/18 15:54 11141-16-512/29/17 10:130.50 1
PCB-1242 (Aroclor 1242)ND ug/L 01/02/18 15:54 53469-21-912/29/17 10:130.50 1
PCB-1248 (Aroclor 1248)ND ug/L 01/02/18 15:54 12672-29-612/29/17 10:130.50 1
PCB-1254 (Aroclor 1254)ND ug/L 01/02/18 15:54 11097-69-112/29/17 10:130.50 1
PCB-1260 (Aroclor 1260)ND ug/L 01/02/18 15:54 11096-82-512/29/17 10:130.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-10 Lab ID:92368450009 Collected:12/28/17 14:40 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
Surrogates
Decachlorobiphenyl (S)46 %01/02/18 15:54 2051-24-312/29/17 10:1310-132 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 01/03/18 15:22 83-32-912/29/17 10:1510.0 1
Acenaphthylene ND ug/L 01/03/18 15:22 208-96-812/29/17 10:1510.0 1
Acetophenone ND ug/L 01/03/18 15:22 98-86-212/29/17 10:1510.0 1
2-Acetylaminofluorene ND ug/L 01/03/18 15:22 53-96-3 L212/29/17 10:1520.0 1
4-Aminobiphenyl ND ug/L 01/03/18 15:22 92-67-112/29/17 10:1510.0 1
Anthracene ND ug/L 01/03/18 15:22 120-12-712/29/17 10:1510.0 1
Benzo(a)anthracene ND ug/L 01/03/18 15:22 56-55-312/29/17 10:1510.0 1
Benzo(a)pyrene ND ug/L 01/03/18 15:22 50-32-812/29/17 10:1510.0 1
Benzo(b)fluoranthene ND ug/L 01/03/18 15:22 205-99-212/29/17 10:1510.0 1
Benzo(g,h,i)perylene ND ug/L 01/03/18 15:22 191-24-212/29/17 10:1510.0 1
Benzo(k)fluoranthene ND ug/L 01/03/18 15:22 207-08-912/29/17 10:1510.0 1
Benzyl alcohol ND ug/L 01/03/18 15:22 100-51-612/29/17 10:1520.0 1
4-Bromophenylphenyl ether ND ug/L 01/03/18 15:22 101-55-312/29/17 10:1510.0 1
Butylbenzylphthalate ND ug/L 01/03/18 15:22 85-68-712/29/17 10:1510.0 1
4-Chloro-3-methylphenol ND ug/L 01/03/18 15:22 59-50-712/29/17 10:1520.0 1
4-Chloroaniline ND ug/L 01/03/18 15:22 106-47-812/29/17 10:1520.0 1
Chlorobenzilate ND ug/L 01/03/18 15:22 510-15-612/29/17 10:1510.0 1
bis(2-Chloroethoxy)methane ND ug/L 01/03/18 15:22 111-91-112/29/17 10:1510.0 1
bis(2-Chloroethyl) ether ND ug/L 01/03/18 15:22 111-44-412/29/17 10:1510.0 1
2-Chloronaphthalene ND ug/L 01/03/18 15:22 91-58-712/29/17 10:1510.0 1
2-Chlorophenol ND ug/L 01/03/18 15:22 95-57-812/29/17 10:1510.0 1
4-Chlorophenylphenyl ether ND ug/L 01/03/18 15:22 7005-72-312/29/17 10:1510.0 1
Chrysene ND ug/L 01/03/18 15:22 218-01-912/29/17 10:1510.0 1
Diallate ND ug/L 01/03/18 15:22 2303-16-412/29/17 10:1510.0 1
Dibenz(a,h)anthracene ND ug/L 01/03/18 15:22 53-70-312/29/17 10:1510.0 1
Dibenzofuran ND ug/L 01/03/18 15:22 132-64-912/29/17 10:1510.0 1
3,3'-Dichlorobenzidine ND ug/L 01/03/18 15:22 91-94-112/29/17 10:1520.0 1
2,4-Dichlorophenol ND ug/L 01/03/18 15:22 120-83-212/29/17 10:1510.0 1
2,6-Dichlorophenol ND ug/L 01/03/18 15:22 87-65-012/29/17 10:1510.0 1
Diethylphthalate ND ug/L 01/03/18 15:22 84-66-212/29/17 10:1510.0 1
Dimethoate ND ug/L 01/03/18 15:22 60-51-512/29/17 10:1510.0 1
P-Dimethylaminoazobenzene ND ug/L 01/03/18 15:22 60-11-712/29/17 10:155.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 01/03/18 15:22 57-97-612/29/17 10:1510.0 1
3,3'-Dimethylbenzidine ND ug/L 01/03/18 15:22 119-93-712/29/17 10:1510.0 1
2,4-Dimethylphenol ND ug/L 01/03/18 15:22 105-67-912/29/17 10:1510.0 1
Dimethylphthalate ND ug/L 01/03/18 15:22 131-11-312/29/17 10:1510.0 1
Di-n-butylphthalate ND ug/L 01/03/18 15:22 84-74-212/29/17 10:1510.0 1
4,6-Dinitro-2-methylphenol ND ug/L 01/03/18 15:22 534-52-112/29/17 10:1520.0 1
1,3-Dinitrobenzene ND ug/L 01/03/18 15:22 99-65-012/29/17 10:1520.0 1
2,4-Dinitrophenol ND ug/L 01/03/18 15:22 51-28-512/29/17 10:1550.0 1
2,4-Dinitrotoluene ND ug/L 01/03/18 15:22 121-14-212/29/17 10:1510.0 1
2,6-Dinitrotoluene ND ug/L 01/03/18 15:22 606-20-212/29/17 10:1510.0 1
Di-n-octylphthalate ND ug/L 01/03/18 15:22 117-84-012/29/17 10:1510.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-10 Lab ID:92368450009 Collected:12/28/17 14:40 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Diphenylamine ND ug/L 01/03/18 15:22 122-39-412/29/17 10:1510.0 1
Disulfoton ND ug/L 01/03/18 15:22 298-04-412/29/17 10:1510.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 01/03/18 15:22 117-81-712/29/17 10:156.0 1
Ethyl methanesulfonate ND ug/L 01/03/18 15:22 62-50-012/29/17 10:1520.0 1
Famphur ND ug/L 01/03/18 15:22 52-85-712/29/17 10:1510.0 1
Fluoranthene ND ug/L 01/03/18 15:22 206-44-012/29/17 10:1510.0 1
Fluorene ND ug/L 01/03/18 15:22 86-73-712/29/17 10:1510.0 1
Hexachlorobenzene ND ug/L 01/03/18 15:22 118-74-112/29/17 10:1510.0 1
Hexachlorocyclopentadiene ND ug/L 01/03/18 15:22 77-47-412/29/17 10:1510.0 1
Hexachloroethane ND ug/L 01/03/18 15:22 67-72-112/29/17 10:1510.0 1
Hexachlorophene ND ug/L 01/03/18 15:22 70-30-412/29/17 10:151001
Indeno(1,2,3-cd)pyrene ND ug/L 01/03/18 15:22 193-39-512/29/17 10:1510.0 1
Isodrin ND ug/L 01/03/18 15:22 465-73-612/29/17 10:1520.0 1
Isophorone ND ug/L 01/03/18 15:22 78-59-112/29/17 10:1510.0 1
Isosafrole ND ug/L 01/03/18 15:22 120-58-112/29/17 10:1510.0 1
Kepone ND ug/L 01/03/18 15:22 143-50-012/29/17 10:1510.0 1
Methapyrilene ND ug/L 01/03/18 15:22 91-80-5 L212/29/17 10:1550.0 1
3-Methylcholanthrene ND ug/L 01/03/18 15:22 56-49-512/29/17 10:1510.0 1
Methyl methanesulfonate ND ug/L 01/03/18 15:22 66-27-3 L112/29/17 10:155.0 1
2-Methylnaphthalene ND ug/L 01/03/18 15:22 91-57-612/29/17 10:1510.0 1
Methyl parathion ND ug/L 01/03/18 15:22 298-00-012/29/17 10:1510.0 1
2-Methylphenol(o-Cresol)ND ug/L 01/03/18 15:22 95-48-712/29/17 10:1510.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 01/03/18 15:22 15831-10-412/29/17 10:1510.0 1
1-Naphthalenamine ND ug/L 01/03/18 15:22 134-32-712/29/17 10:155.0 1
2-Naphthalenamine ND ug/L 01/03/18 15:22 91-59-812/29/17 10:155.0 1
1,4-Naphthoquinone ND ug/L 01/03/18 15:22 130-15-412/29/17 10:155.0 1
2-Nitroaniline ND ug/L 01/03/18 15:22 88-74-412/29/17 10:1550.0 1
3-Nitroaniline ND ug/L 01/03/18 15:22 99-09-212/29/17 10:1550.0 1
4-Nitroaniline ND ug/L 01/03/18 15:22 100-01-612/29/17 10:1520.0 1
Nitrobenzene ND ug/L 01/03/18 15:22 98-95-312/29/17 10:1510.0 1
2-Nitrophenol ND ug/L 01/03/18 15:22 88-75-512/29/17 10:1510.0 1
4-Nitrophenol ND ug/L 01/03/18 15:22 100-02-712/29/17 10:1550.0 1
5-Nitro-o-toluidine ND ug/L 01/03/18 15:22 99-55-812/29/17 10:1510.0 1
N-Nitrosodiethylamine ND ug/L 01/03/18 15:22 55-18-512/29/17 10:1520.0 1
N-Nitrosodimethylamine ND ug/L 01/03/18 15:22 62-75-912/29/17 10:1510.0 1
N-Nitroso-di-n-butylamine ND ug/L 01/03/18 15:22 924-16-312/29/17 10:1510.0 1
N-Nitroso-di-n-propylamine ND ug/L 01/03/18 15:22 621-64-712/29/17 10:1510.0 1
N-Nitrosodiphenylamine ND ug/L 01/03/18 15:22 86-30-612/29/17 10:1510.0 1
N-Nitrosomethylethylamine ND ug/L 01/03/18 15:22 10595-95-612/29/17 10:1510.0 1
N-Nitrosopiperidine ND ug/L 01/03/18 15:22 100-75-412/29/17 10:1520.0 1
N-Nitrosopyrrolidine ND ug/L 01/03/18 15:22 930-55-212/29/17 10:1510.0 1
O,O,O-Triethylphosphorothioate ND ug/L 01/03/18 15:22 126-68-1 L212/29/17 10:1510.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 01/03/18 15:22 108-60-112/29/17 10:1510.0 1
Parathion (Ethyl parathion)ND ug/L 01/03/18 15:22 56-38-212/29/17 10:1510.0 1
Pentachlorobenzene ND ug/L 01/03/18 15:22 608-93-512/29/17 10:1510.0 1
Pentachloronitrobenzene ND ug/L 01/03/18 15:22 82-68-812/29/17 10:1520.0 1
Pentachlorophenol ND ug/L 01/03/18 15:22 87-86-512/29/17 10:1525.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 50 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-10 Lab ID:92368450009 Collected:12/28/17 14:40 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Phenacetin ND ug/L 01/03/18 15:22 62-44-212/29/17 10:1520.0 1
Phenanthrene ND ug/L 01/03/18 15:22 85-01-812/29/17 10:1510.0 1
Phenol ND ug/L 01/03/18 15:22 108-95-212/29/17 10:1510.0 1
p-Phenylenediamine ND ug/L 01/03/18 15:22 106-50-312/29/17 10:1510.0 1
Phorate ND ug/L 01/03/18 15:22 298-02-212/29/17 10:1510.0 1
Pronamide ND ug/L 01/03/18 15:22 23950-58-512/29/17 10:1510.0 1
Pyrene ND ug/L 01/03/18 15:22 129-00-012/29/17 10:1510.0 1
Safrole ND ug/L 01/03/18 15:22 94-59-712/29/17 10:1510.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 01/03/18 15:22 95-94-312/29/17 10:1510.0 1
2,3,4,6-Tetrachlorophenol ND ug/L 01/03/18 15:22 58-90-212/29/17 10:1510.0 1
Thionazin ND ug/L 01/03/18 15:22 297-97-212/29/17 10:1520.0 1
O-Toluidine ND ug/L 01/03/18 15:22 95-53-412/29/17 10:1510.0 1
2,4,5-Trichlorophenol ND ug/L 01/03/18 15:22 95-95-412/29/17 10:1510.0 1
2,4,6-Trichlorophenol ND ug/L 01/03/18 15:22 88-06-212/29/17 10:1510.0 1
1,3,5-Trinitrobenzene ND ug/L 01/03/18 15:22 99-35-4 L212/29/17 10:1510.0 1
Surrogates
Nitrobenzene-d5 (S)72 %01/03/18 15:22 4165-60-012/29/17 10:1521-110 1
2-Fluorobiphenyl (S)62 %01/03/18 15:22 321-60-812/29/17 10:1527-110 1
Terphenyl-d14 (S)39 %01/03/18 15:22 1718-51-012/29/17 10:1531-107 1
Phenol-d6 (S)21 %01/03/18 15:22 13127-88-312/29/17 10:1510-110 1
2-Fluorophenol (S)30 %01/03/18 15:22 367-12-412/29/17 10:1512-110 1
2,4,6-Tribromophenol (S)78 %01/03/18 15:22 118-79-612/29/17 10:1527-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 13.7J ug/L 01/03/18 03:25 67-64-125.0 1
Acetonitrile ND ug/L 01/03/18 03:25 75-05-850.0 1
Acrolein ND ug/L 01/03/18 03:25 107-02-810.0 1
Acrylonitrile ND ug/L 01/03/18 03:25 107-13-110.0 1
Allyl chloride ND ug/L 01/03/18 03:25 107-05-12.0 1
Benzene 0.57J ug/L 01/03/18 03:25 71-43-21.0 1
Bromochloromethane ND ug/L 01/03/18 03:25 74-97-51.0 1
Bromodichloromethane ND ug/L 01/03/18 03:25 75-27-41.0 1
Bromoform ND ug/L 01/03/18 03:25 75-25-21.0 1
Bromomethane ND ug/L 01/03/18 03:25 74-83-92.0 1
2-Butanone (MEK)ND ug/L 01/03/18 03:25 78-93-35.0 1
Carbon disulfide 2.1 ug/L 01/03/18 03:25 75-15-02.0 1
Carbon tetrachloride ND ug/L 01/03/18 03:25 56-23-51.0 1
Chlorobenzene ND ug/L 01/03/18 03:25 108-90-71.0 1
Chloroethane ND ug/L 01/03/18 03:25 75-00-31.0 1
Chloroform ND ug/L 01/03/18 03:25 67-66-31.0 1
Chloromethane ND ug/L 01/03/18 03:25 74-87-31.0 1
Chloroprene ND ug/L 01/03/18 03:25 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/18 03:25 96-12-8 L22.0 1
Dibromochloromethane ND ug/L 01/03/18 03:25 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/18 03:25 106-93-41.0 1
Dibromomethane ND ug/L 01/03/18 03:25 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 01/03/18 03:25 95-50-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-10 Lab ID:92368450009 Collected:12/28/17 14:40 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,3-Dichlorobenzene ND ug/L 01/03/18 03:25 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 01/03/18 03:25 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/18 03:25 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 01/03/18 03:25 75-71-81.0 1
1,1-Dichloroethane ND ug/L 01/03/18 03:25 75-34-31.0 1
1,2-Dichloroethane ND ug/L 01/03/18 03:25 107-06-21.0 1
1,1-Dichloroethene ND ug/L 01/03/18 03:25 75-35-41.0 1
cis-1,2-Dichloroethene 0.27J ug/L 01/03/18 03:25 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 01/03/18 03:25 156-60-51.0 1
1,2-Dichloropropane ND ug/L 01/03/18 03:25 78-87-51.0 1
1,3-Dichloropropane ND ug/L 01/03/18 03:25 142-28-91.0 1
2,2-Dichloropropane ND ug/L 01/03/18 03:25 594-20-71.0 1
1,1-Dichloropropene ND ug/L 01/03/18 03:25 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 01/03/18 03:25 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 01/03/18 03:25 10061-02-61.0 1
Ethylbenzene 0.41J ug/L 01/03/18 03:25 100-41-41.0 1
Ethyl methacrylate ND ug/L 01/03/18 03:25 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 01/03/18 03:25 87-68-31.0 1
2-Hexanone ND ug/L 01/03/18 03:25 591-78-65.0 1
Iodomethane ND ug/L 01/03/18 03:25 74-88-45.0 1
Isobutanol ND ug/L 01/03/18 03:25 78-83-11001
Methacrylonitrile ND ug/L 01/03/18 03:25 126-98-710.0 1
Methylene Chloride ND ug/L 01/03/18 03:25 75-09-21.0 1
Methyl methacrylate ND ug/L 01/03/18 03:25 80-62-6 L22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/18 03:25 108-10-15.0 1
Naphthalene ND ug/L 01/03/18 03:25 91-20-31.0 1
Propionitrile ND ug/L 01/03/18 03:25 107-12-020.0 1
Styrene ND ug/L 01/03/18 03:25 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/18 03:25 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/18 03:25 79-34-51.0 1
Tetrachloroethene ND ug/L 01/03/18 03:25 127-18-41.0 1
Tetrahydrofuran 135 ug/L 01/03/18 03:25 109-99-910.0 1
Toluene 0.35J ug/L 01/03/18 03:25 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 01/03/18 03:25 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 01/03/18 03:25 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 01/03/18 03:25 79-00-51.0 1
Trichloroethene ND ug/L 01/03/18 03:25 79-01-61.0 1
Trichlorofluoromethane ND ug/L 01/03/18 03:25 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 01/03/18 03:25 96-18-41.0 1
Vinyl acetate ND ug/L 01/03/18 03:25 108-05-42.0 1
Vinyl chloride ND ug/L 01/03/18 03:25 75-01-41.0 1
Xylene (Total)1.1 ug/L 01/03/18 03:25 1330-20-71.0 1
m&p-Xylene 1.3J ug/L 01/03/18 03:25 179601-23-12.0 1
o-Xylene 1.1 ug/L 01/03/18 03:25 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)100 %01/03/18 03:25 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %01/03/18 03:25 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-10 Lab ID:92368450009 Collected:12/28/17 14:40 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Surrogates
Toluene-d8 (S)110 %01/03/18 03:25 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-13 Lab ID:92368450010 Collected:12/28/17 12:26 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JSH 01/05/18 11:501
Collected Date 12/28/17 01/05/18 11:501
Collected Time 12:26 01/05/18 11:501
pH 5.8 Std. Units 01/05/18 11:500.10 1
Temperature 11.2 deg C 01/05/18 11:500.50 1
Static Water Level 9.09 feet 01/05/18 11:501
Specific Conductance 111.4 umhos/cm 01/05/18 11:501.0 1
Oxygen, Dissolved 1.3 mg/L 01/05/18 11:50 7782-44-71
Total Well Depth 20.0 feet 01/05/18 11:501
REDOX 216.5 mV 01/05/18 11:501
Turbidity 9.7 NTU 01/05/18 11:501.0 1
Odor NONE 01/05/18 11:501
Appearance CLEAR 01/05/18 11:501
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 01/02/18 18:03 309-00-212/29/17 10:130.050 1
alpha-BHC ND ug/L 01/02/18 18:03 319-84-612/29/17 10:130.050 1
beta-BHC ND ug/L 01/02/18 18:03 319-85-712/29/17 10:130.050 1
delta-BHC ND ug/L 01/02/18 18:03 319-86-812/29/17 10:130.050 1
gamma-BHC (Lindane)ND ug/L 01/02/18 18:03 58-89-912/29/17 10:130.050 1
Chlordane (Technical)ND ug/L 01/02/18 18:03 57-74-912/29/17 10:130.20 1
4,4'-DDD ND ug/L 01/02/18 18:03 72-54-812/29/17 10:130.050 1
4,4'-DDE ND ug/L 01/02/18 18:03 72-55-912/29/17 10:130.050 1
4,4'-DDT ND ug/L 01/02/18 18:03 50-29-312/29/17 10:130.050 1
Dieldrin ND ug/L 01/02/18 18:03 60-57-112/29/17 10:130.050 1
Endosulfan I ND ug/L 01/02/18 18:03 959-98-812/29/17 10:130.050 1
Endosulfan II ND ug/L 01/02/18 18:03 33213-65-912/29/17 10:130.050 1
Endosulfan sulfate ND ug/L 01/02/18 18:03 1031-07-812/29/17 10:130.050 1
Endrin ND ug/L 01/02/18 18:03 72-20-812/29/17 10:130.050 1
Endrin aldehyde ND ug/L 01/02/18 18:03 7421-93-412/29/17 10:130.050 1
Heptachlor ND ug/L 01/02/18 18:03 76-44-812/29/17 10:130.050 1
Heptachlor epoxide ND ug/L 01/02/18 18:03 1024-57-312/29/17 10:130.050 1
Methoxychlor ND ug/L 01/02/18 18:03 72-43-512/29/17 10:130.15 1
Toxaphene ND ug/L 01/02/18 18:03 8001-35-212/29/17 10:130.20 1
Surrogates
Tetrachloro-m-xylene (S)49 %01/02/18 18:03 877-09-812/29/17 10:1320-130 1
Decachlorobiphenyl (S)51 %01/02/18 18:03 2051-24-312/29/17 10:1320-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 01/02/18 16:15 12674-11-212/29/17 10:130.50 1
PCB-1221 (Aroclor 1221)ND ug/L 01/02/18 16:15 11104-28-212/29/17 10:130.50 1
PCB-1232 (Aroclor 1232)ND ug/L 01/02/18 16:15 11141-16-512/29/17 10:130.50 1
PCB-1242 (Aroclor 1242)ND ug/L 01/02/18 16:15 53469-21-912/29/17 10:130.50 1
PCB-1248 (Aroclor 1248)ND ug/L 01/02/18 16:15 12672-29-612/29/17 10:130.50 1
PCB-1254 (Aroclor 1254)ND ug/L 01/02/18 16:15 11097-69-112/29/17 10:130.50 1
PCB-1260 (Aroclor 1260)ND ug/L 01/02/18 16:15 11096-82-512/29/17 10:130.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-13 Lab ID:92368450010 Collected:12/28/17 12:26 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
Surrogates
Decachlorobiphenyl (S)52 %01/02/18 16:15 2051-24-312/29/17 10:1310-132 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 01/02/18 18:35 83-32-912/29/17 10:1510.0 1
Acenaphthylene ND ug/L 01/02/18 18:35 208-96-812/29/17 10:1510.0 1
Acetophenone ND ug/L 01/02/18 18:35 98-86-212/29/17 10:1510.0 1
2-Acetylaminofluorene ND ug/L 01/02/18 18:35 53-96-3 L212/29/17 10:1520.0 1
4-Aminobiphenyl ND ug/L 01/02/18 18:35 92-67-112/29/17 10:1510.0 1
Anthracene ND ug/L 01/02/18 18:35 120-12-712/29/17 10:1510.0 1
Benzo(a)anthracene ND ug/L 01/02/18 18:35 56-55-312/29/17 10:1510.0 1
Benzo(a)pyrene ND ug/L 01/02/18 18:35 50-32-812/29/17 10:1510.0 1
Benzo(b)fluoranthene ND ug/L 01/02/18 18:35 205-99-212/29/17 10:1510.0 1
Benzo(g,h,i)perylene ND ug/L 01/02/18 18:35 191-24-212/29/17 10:1510.0 1
Benzo(k)fluoranthene ND ug/L 01/02/18 18:35 207-08-912/29/17 10:1510.0 1
Benzyl alcohol ND ug/L 01/02/18 18:35 100-51-612/29/17 10:1520.0 1
4-Bromophenylphenyl ether ND ug/L 01/02/18 18:35 101-55-312/29/17 10:1510.0 1
Butylbenzylphthalate ND ug/L 01/02/18 18:35 85-68-712/29/17 10:1510.0 1
4-Chloro-3-methylphenol ND ug/L 01/02/18 18:35 59-50-712/29/17 10:1520.0 1
4-Chloroaniline ND ug/L 01/02/18 18:35 106-47-812/29/17 10:1520.0 1
Chlorobenzilate ND ug/L 01/02/18 18:35 510-15-612/29/17 10:1510.0 1
bis(2-Chloroethoxy)methane ND ug/L 01/02/18 18:35 111-91-112/29/17 10:1510.0 1
bis(2-Chloroethyl) ether ND ug/L 01/02/18 18:35 111-44-412/29/17 10:1510.0 1
2-Chloronaphthalene ND ug/L 01/02/18 18:35 91-58-712/29/17 10:1510.0 1
2-Chlorophenol ND ug/L 01/02/18 18:35 95-57-812/29/17 10:1510.0 1
4-Chlorophenylphenyl ether ND ug/L 01/02/18 18:35 7005-72-312/29/17 10:1510.0 1
Chrysene ND ug/L 01/02/18 18:35 218-01-912/29/17 10:1510.0 1
Diallate ND ug/L 01/02/18 18:35 2303-16-412/29/17 10:1510.0 1
Dibenz(a,h)anthracene ND ug/L 01/02/18 18:35 53-70-312/29/17 10:1510.0 1
Dibenzofuran ND ug/L 01/02/18 18:35 132-64-912/29/17 10:1510.0 1
3,3'-Dichlorobenzidine ND ug/L 01/02/18 18:35 91-94-112/29/17 10:1520.0 1
2,4-Dichlorophenol ND ug/L 01/02/18 18:35 120-83-212/29/17 10:1510.0 1
2,6-Dichlorophenol ND ug/L 01/02/18 18:35 87-65-012/29/17 10:1510.0 1
Diethylphthalate ND ug/L 01/02/18 18:35 84-66-212/29/17 10:1510.0 1
Dimethoate ND ug/L 01/02/18 18:35 60-51-512/29/17 10:1510.0 1
P-Dimethylaminoazobenzene ND ug/L 01/02/18 18:35 60-11-712/29/17 10:155.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 01/02/18 18:35 57-97-612/29/17 10:1510.0 1
3,3'-Dimethylbenzidine ND ug/L 01/02/18 18:35 119-93-712/29/17 10:1510.0 1
2,4-Dimethylphenol ND ug/L 01/02/18 18:35 105-67-912/29/17 10:1510.0 1
Dimethylphthalate ND ug/L 01/02/18 18:35 131-11-312/29/17 10:1510.0 1
Di-n-butylphthalate ND ug/L 01/02/18 18:35 84-74-212/29/17 10:1510.0 1
4,6-Dinitro-2-methylphenol ND ug/L 01/02/18 18:35 534-52-112/29/17 10:1520.0 1
1,3-Dinitrobenzene ND ug/L 01/02/18 18:35 99-65-012/29/17 10:1520.0 1
2,4-Dinitrophenol ND ug/L 01/02/18 18:35 51-28-512/29/17 10:1550.0 1
2,4-Dinitrotoluene ND ug/L 01/02/18 18:35 121-14-212/29/17 10:1510.0 1
2,6-Dinitrotoluene ND ug/L 01/02/18 18:35 606-20-212/29/17 10:1510.0 1
Di-n-octylphthalate ND ug/L 01/02/18 18:35 117-84-012/29/17 10:1510.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
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Page 55 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-13 Lab ID:92368450010 Collected:12/28/17 12:26 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Diphenylamine ND ug/L 01/02/18 18:35 122-39-412/29/17 10:1510.0 1
Disulfoton ND ug/L 01/02/18 18:35 298-04-412/29/17 10:1510.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 01/02/18 18:35 117-81-712/29/17 10:156.0 1
Ethyl methanesulfonate ND ug/L 01/02/18 18:35 62-50-012/29/17 10:1520.0 1
Famphur ND ug/L 01/02/18 18:35 52-85-712/29/17 10:1510.0 1
Fluoranthene ND ug/L 01/02/18 18:35 206-44-012/29/17 10:1510.0 1
Fluorene ND ug/L 01/02/18 18:35 86-73-712/29/17 10:1510.0 1
Hexachlorobenzene ND ug/L 01/02/18 18:35 118-74-112/29/17 10:1510.0 1
Hexachlorocyclopentadiene ND ug/L 01/02/18 18:35 77-47-412/29/17 10:1510.0 1
Hexachloroethane ND ug/L 01/02/18 18:35 67-72-112/29/17 10:1510.0 1
Hexachlorophene ND ug/L 01/02/18 18:35 70-30-412/29/17 10:151001
Indeno(1,2,3-cd)pyrene ND ug/L 01/02/18 18:35 193-39-512/29/17 10:1510.0 1
Isodrin ND ug/L 01/02/18 18:35 465-73-612/29/17 10:1520.0 1
Isophorone ND ug/L 01/02/18 18:35 78-59-112/29/17 10:1510.0 1
Isosafrole ND ug/L 01/02/18 18:35 120-58-112/29/17 10:1510.0 1
Kepone ND ug/L 01/02/18 18:35 143-50-012/29/17 10:1510.0 1
Methapyrilene ND ug/L 01/02/18 18:35 91-80-5 L212/29/17 10:1550.0 1
3-Methylcholanthrene ND ug/L 01/02/18 18:35 56-49-512/29/17 10:1510.0 1
Methyl methanesulfonate ND ug/L 01/02/18 18:35 66-27-3 L112/29/17 10:155.0 1
2-Methylnaphthalene ND ug/L 01/02/18 18:35 91-57-612/29/17 10:1510.0 1
Methyl parathion ND ug/L 01/02/18 18:35 298-00-012/29/17 10:1510.0 1
2-Methylphenol(o-Cresol)ND ug/L 01/02/18 18:35 95-48-712/29/17 10:1510.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 01/02/18 18:35 15831-10-412/29/17 10:1510.0 1
1-Naphthalenamine ND ug/L 01/02/18 18:35 134-32-712/29/17 10:155.0 1
2-Naphthalenamine ND ug/L 01/02/18 18:35 91-59-812/29/17 10:155.0 1
1,4-Naphthoquinone ND ug/L 01/02/18 18:35 130-15-412/29/17 10:155.0 1
2-Nitroaniline ND ug/L 01/02/18 18:35 88-74-412/29/17 10:1550.0 1
3-Nitroaniline ND ug/L 01/02/18 18:35 99-09-212/29/17 10:1550.0 1
4-Nitroaniline ND ug/L 01/02/18 18:35 100-01-612/29/17 10:1520.0 1
Nitrobenzene ND ug/L 01/02/18 18:35 98-95-312/29/17 10:1510.0 1
2-Nitrophenol ND ug/L 01/02/18 18:35 88-75-512/29/17 10:1510.0 1
4-Nitrophenol ND ug/L 01/02/18 18:35 100-02-712/29/17 10:1550.0 1
5-Nitro-o-toluidine ND ug/L 01/02/18 18:35 99-55-812/29/17 10:1510.0 1
N-Nitrosodiethylamine ND ug/L 01/02/18 18:35 55-18-512/29/17 10:1520.0 1
N-Nitrosodimethylamine ND ug/L 01/02/18 18:35 62-75-912/29/17 10:1510.0 1
N-Nitroso-di-n-butylamine ND ug/L 01/02/18 18:35 924-16-312/29/17 10:1510.0 1
N-Nitroso-di-n-propylamine ND ug/L 01/02/18 18:35 621-64-712/29/17 10:1510.0 1
N-Nitrosodiphenylamine ND ug/L 01/02/18 18:35 86-30-612/29/17 10:1510.0 1
N-Nitrosomethylethylamine ND ug/L 01/02/18 18:35 10595-95-612/29/17 10:1510.0 1
N-Nitrosopiperidine ND ug/L 01/02/18 18:35 100-75-412/29/17 10:1520.0 1
N-Nitrosopyrrolidine ND ug/L 01/02/18 18:35 930-55-212/29/17 10:1510.0 1
O,O,O-Triethylphosphorothioate ND ug/L 01/02/18 18:35 126-68-1 L212/29/17 10:1510.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 01/02/18 18:35 108-60-112/29/17 10:1510.0 1
Parathion (Ethyl parathion)ND ug/L 01/02/18 18:35 56-38-212/29/17 10:1510.0 1
Pentachlorobenzene ND ug/L 01/02/18 18:35 608-93-512/29/17 10:1510.0 1
Pentachloronitrobenzene ND ug/L 01/02/18 18:35 82-68-812/29/17 10:1520.0 1
Pentachlorophenol ND ug/L 01/02/18 18:35 87-86-512/29/17 10:1525.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-13 Lab ID:92368450010 Collected:12/28/17 12:26 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Phenacetin ND ug/L 01/02/18 18:35 62-44-212/29/17 10:1520.0 1
Phenanthrene ND ug/L 01/02/18 18:35 85-01-812/29/17 10:1510.0 1
Phenol ND ug/L 01/02/18 18:35 108-95-212/29/17 10:1510.0 1
p-Phenylenediamine ND ug/L 01/02/18 18:35 106-50-312/29/17 10:1510.0 1
Phorate ND ug/L 01/02/18 18:35 298-02-212/29/17 10:1510.0 1
Pronamide ND ug/L 01/02/18 18:35 23950-58-512/29/17 10:1510.0 1
Pyrene ND ug/L 01/02/18 18:35 129-00-012/29/17 10:1510.0 1
Safrole ND ug/L 01/02/18 18:35 94-59-712/29/17 10:1510.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 01/02/18 18:35 95-94-312/29/17 10:1510.0 1
2,3,4,6-Tetrachlorophenol ND ug/L 01/02/18 18:35 58-90-212/29/17 10:1510.0 1
Thionazin ND ug/L 01/02/18 18:35 297-97-212/29/17 10:1520.0 1
O-Toluidine ND ug/L 01/02/18 18:35 95-53-412/29/17 10:1510.0 1
2,4,5-Trichlorophenol ND ug/L 01/02/18 18:35 95-95-412/29/17 10:1510.0 1
2,4,6-Trichlorophenol ND ug/L 01/02/18 18:35 88-06-212/29/17 10:1510.0 1
1,3,5-Trinitrobenzene ND ug/L 01/02/18 18:35 99-35-4 L212/29/17 10:1510.0 1
Surrogates
Nitrobenzene-d5 (S)56 %01/02/18 18:35 4165-60-012/29/17 10:1521-110 1
2-Fluorobiphenyl (S)55 %01/02/18 18:35 321-60-812/29/17 10:1527-110 1
Terphenyl-d14 (S)61 %01/02/18 18:35 1718-51-012/29/17 10:1531-107 1
Phenol-d6 (S)14 %01/02/18 18:35 13127-88-312/29/17 10:1510-110 1
2-Fluorophenol (S)26 %01/02/18 18:35 367-12-412/29/17 10:1512-110 1
2,4,6-Tribromophenol (S)67 %01/02/18 18:35 118-79-612/29/17 10:1527-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/18 03:42 67-64-125.0 1
Acetonitrile ND ug/L 01/03/18 03:42 75-05-850.0 1
Acrolein ND ug/L 01/03/18 03:42 107-02-810.0 1
Acrylonitrile ND ug/L 01/03/18 03:42 107-13-110.0 1
Allyl chloride ND ug/L 01/03/18 03:42 107-05-12.0 1
Benzene ND ug/L 01/03/18 03:42 71-43-21.0 1
Bromochloromethane ND ug/L 01/03/18 03:42 74-97-51.0 1
Bromodichloromethane ND ug/L 01/03/18 03:42 75-27-41.0 1
Bromoform ND ug/L 01/03/18 03:42 75-25-21.0 1
Bromomethane ND ug/L 01/03/18 03:42 74-83-92.0 1
2-Butanone (MEK)ND ug/L 01/03/18 03:42 78-93-35.0 1
Carbon disulfide ND ug/L 01/03/18 03:42 75-15-02.0 1
Carbon tetrachloride ND ug/L 01/03/18 03:42 56-23-51.0 1
Chlorobenzene ND ug/L 01/03/18 03:42 108-90-71.0 1
Chloroethane ND ug/L 01/03/18 03:42 75-00-31.0 1
Chloroform ND ug/L 01/03/18 03:42 67-66-31.0 1
Chloromethane ND ug/L 01/03/18 03:42 74-87-31.0 1
Chloroprene ND ug/L 01/03/18 03:42 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/18 03:42 96-12-8 L22.0 1
Dibromochloromethane ND ug/L 01/03/18 03:42 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/18 03:42 106-93-41.0 1
Dibromomethane ND ug/L 01/03/18 03:42 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 01/03/18 03:42 95-50-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-13 Lab ID:92368450010 Collected:12/28/17 12:26 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,3-Dichlorobenzene ND ug/L 01/03/18 03:42 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 01/03/18 03:42 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/18 03:42 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 01/03/18 03:42 75-71-81.0 1
1,1-Dichloroethane ND ug/L 01/03/18 03:42 75-34-31.0 1
1,2-Dichloroethane ND ug/L 01/03/18 03:42 107-06-21.0 1
1,1-Dichloroethene ND ug/L 01/03/18 03:42 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 01/03/18 03:42 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 01/03/18 03:42 156-60-51.0 1
1,2-Dichloropropane ND ug/L 01/03/18 03:42 78-87-51.0 1
1,3-Dichloropropane ND ug/L 01/03/18 03:42 142-28-91.0 1
2,2-Dichloropropane ND ug/L 01/03/18 03:42 594-20-71.0 1
1,1-Dichloropropene ND ug/L 01/03/18 03:42 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 01/03/18 03:42 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 01/03/18 03:42 10061-02-61.0 1
Ethylbenzene ND ug/L 01/03/18 03:42 100-41-41.0 1
Ethyl methacrylate ND ug/L 01/03/18 03:42 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 01/03/18 03:42 87-68-31.0 1
2-Hexanone ND ug/L 01/03/18 03:42 591-78-65.0 1
Iodomethane ND ug/L 01/03/18 03:42 74-88-45.0 1
Isobutanol ND ug/L 01/03/18 03:42 78-83-11001
Methacrylonitrile ND ug/L 01/03/18 03:42 126-98-710.0 1
Methylene Chloride ND ug/L 01/03/18 03:42 75-09-21.0 1
Methyl methacrylate ND ug/L 01/03/18 03:42 80-62-6 L22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/18 03:42 108-10-15.0 1
Naphthalene ND ug/L 01/03/18 03:42 91-20-31.0 1
Propionitrile ND ug/L 01/03/18 03:42 107-12-020.0 1
Styrene ND ug/L 01/03/18 03:42 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/18 03:42 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/18 03:42 79-34-51.0 1
Tetrachloroethene ND ug/L 01/03/18 03:42 127-18-41.0 1
Tetrahydrofuran ND ug/L 01/03/18 03:42 109-99-910.0 1
Toluene ND ug/L 01/03/18 03:42 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 01/03/18 03:42 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 01/03/18 03:42 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 01/03/18 03:42 79-00-51.0 1
Trichloroethene ND ug/L 01/03/18 03:42 79-01-61.0 1
Trichlorofluoromethane ND ug/L 01/03/18 03:42 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 01/03/18 03:42 96-18-41.0 1
Vinyl acetate ND ug/L 01/03/18 03:42 108-05-42.0 1
Vinyl chloride ND ug/L 01/03/18 03:42 75-01-41.0 1
Xylene (Total)ND ug/L 01/03/18 03:42 1330-20-71.0 1
m&p-Xylene ND ug/L 01/03/18 03:42 179601-23-12.0 1
o-Xylene ND ug/L 01/03/18 03:42 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)104 %01/03/18 03:42 460-00-470-130 1
1,2-Dichloroethane-d4 (S)88 %01/03/18 03:42 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-13 Lab ID:92368450010 Collected:12/28/17 12:26 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Surrogates
Toluene-d8 (S)108 %01/03/18 03:42 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-14 Lab ID:92368450011 Collected:12/28/17 13:35 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By STV 01/05/18 11:511
Collected Date 12/28/17 01/05/18 11:511
Collected Time 13:35 01/05/18 11:511
pH 5.6 Std. Units 01/05/18 11:510.10 1
Temperature 9.9 deg C 01/05/18 11:510.50 1
Static Water Level 52.09 feet 01/05/18 11:511
Specific Conductance 169.2 umhos/cm 01/05/18 11:511.0 1
Oxygen, Dissolved 2.9 mg/L 01/05/18 11:51 7782-44-71
Total Well Depth 60 feet 01/05/18 11:511
REDOX 150.5 mV 01/05/18 11:511
Turbidity 7.4 NTU 01/05/18 11:511.0 1
Odor NONE 01/05/18 11:511
Appearance CLEAR 01/05/18 11:511
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 01/02/18 18:21 309-00-212/29/17 10:130.050 1
alpha-BHC ND ug/L 01/02/18 18:21 319-84-612/29/17 10:130.050 1
beta-BHC ND ug/L 01/02/18 18:21 319-85-712/29/17 10:130.050 1
delta-BHC ND ug/L 01/02/18 18:21 319-86-812/29/17 10:130.050 1
gamma-BHC (Lindane)ND ug/L 01/02/18 18:21 58-89-912/29/17 10:130.050 1
Chlordane (Technical)ND ug/L 01/02/18 18:21 57-74-912/29/17 10:130.20 1
4,4'-DDD ND ug/L 01/02/18 18:21 72-54-812/29/17 10:130.050 1
4,4'-DDE ND ug/L 01/02/18 18:21 72-55-912/29/17 10:130.050 1
4,4'-DDT ND ug/L 01/02/18 18:21 50-29-312/29/17 10:130.050 1
Dieldrin ND ug/L 01/02/18 18:21 60-57-112/29/17 10:130.050 1
Endosulfan I ND ug/L 01/02/18 18:21 959-98-812/29/17 10:130.050 1
Endosulfan II ND ug/L 01/02/18 18:21 33213-65-912/29/17 10:130.050 1
Endosulfan sulfate ND ug/L 01/02/18 18:21 1031-07-812/29/17 10:130.050 1
Endrin ND ug/L 01/02/18 18:21 72-20-812/29/17 10:130.050 1
Endrin aldehyde ND ug/L 01/02/18 18:21 7421-93-412/29/17 10:130.050 1
Heptachlor ND ug/L 01/02/18 18:21 76-44-812/29/17 10:130.050 1
Heptachlor epoxide ND ug/L 01/02/18 18:21 1024-57-312/29/17 10:130.050 1
Methoxychlor ND ug/L 01/02/18 18:21 72-43-512/29/17 10:130.15 1
Toxaphene ND ug/L 01/02/18 18:21 8001-35-212/29/17 10:130.20 1
Surrogates
Tetrachloro-m-xylene (S)68 %01/02/18 18:21 877-09-812/29/17 10:1320-130 1
Decachlorobiphenyl (S)66 %01/02/18 18:21 2051-24-312/29/17 10:1320-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 01/02/18 16:36 12674-11-212/29/17 10:130.50 1
PCB-1221 (Aroclor 1221)ND ug/L 01/02/18 16:36 11104-28-212/29/17 10:130.50 1
PCB-1232 (Aroclor 1232)ND ug/L 01/02/18 16:36 11141-16-512/29/17 10:130.50 1
PCB-1242 (Aroclor 1242)ND ug/L 01/02/18 16:36 53469-21-912/29/17 10:130.50 1
PCB-1248 (Aroclor 1248)ND ug/L 01/02/18 16:36 12672-29-612/29/17 10:130.50 1
PCB-1254 (Aroclor 1254)ND ug/L 01/02/18 16:36 11097-69-112/29/17 10:130.50 1
PCB-1260 (Aroclor 1260)ND ug/L 01/02/18 16:36 11096-82-512/29/17 10:130.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-14 Lab ID:92368450011 Collected:12/28/17 13:35 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
Surrogates
Decachlorobiphenyl (S)64 %01/02/18 16:36 2051-24-312/29/17 10:1310-132 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 01/02/18 19:05 83-32-912/29/17 10:1510.0 1
Acenaphthylene ND ug/L 01/02/18 19:05 208-96-812/29/17 10:1510.0 1
Acetophenone ND ug/L 01/02/18 19:05 98-86-212/29/17 10:1510.0 1
2-Acetylaminofluorene ND ug/L 01/02/18 19:05 53-96-3 L212/29/17 10:1520.0 1
4-Aminobiphenyl ND ug/L 01/02/18 19:05 92-67-112/29/17 10:1510.0 1
Anthracene ND ug/L 01/02/18 19:05 120-12-712/29/17 10:1510.0 1
Benzo(a)anthracene ND ug/L 01/02/18 19:05 56-55-312/29/17 10:1510.0 1
Benzo(a)pyrene ND ug/L 01/02/18 19:05 50-32-812/29/17 10:1510.0 1
Benzo(b)fluoranthene ND ug/L 01/02/18 19:05 205-99-212/29/17 10:1510.0 1
Benzo(g,h,i)perylene ND ug/L 01/02/18 19:05 191-24-212/29/17 10:1510.0 1
Benzo(k)fluoranthene ND ug/L 01/02/18 19:05 207-08-912/29/17 10:1510.0 1
Benzyl alcohol ND ug/L 01/02/18 19:05 100-51-612/29/17 10:1520.0 1
4-Bromophenylphenyl ether ND ug/L 01/02/18 19:05 101-55-312/29/17 10:1510.0 1
Butylbenzylphthalate ND ug/L 01/02/18 19:05 85-68-712/29/17 10:1510.0 1
4-Chloro-3-methylphenol ND ug/L 01/02/18 19:05 59-50-712/29/17 10:1520.0 1
4-Chloroaniline ND ug/L 01/02/18 19:05 106-47-812/29/17 10:1520.0 1
Chlorobenzilate ND ug/L 01/02/18 19:05 510-15-612/29/17 10:1510.0 1
bis(2-Chloroethoxy)methane ND ug/L 01/02/18 19:05 111-91-112/29/17 10:1510.0 1
bis(2-Chloroethyl) ether ND ug/L 01/02/18 19:05 111-44-412/29/17 10:1510.0 1
2-Chloronaphthalene ND ug/L 01/02/18 19:05 91-58-712/29/17 10:1510.0 1
2-Chlorophenol ND ug/L 01/02/18 19:05 95-57-812/29/17 10:1510.0 1
4-Chlorophenylphenyl ether ND ug/L 01/02/18 19:05 7005-72-312/29/17 10:1510.0 1
Chrysene ND ug/L 01/02/18 19:05 218-01-912/29/17 10:1510.0 1
Diallate ND ug/L 01/02/18 19:05 2303-16-412/29/17 10:1510.0 1
Dibenz(a,h)anthracene ND ug/L 01/02/18 19:05 53-70-312/29/17 10:1510.0 1
Dibenzofuran ND ug/L 01/02/18 19:05 132-64-912/29/17 10:1510.0 1
3,3'-Dichlorobenzidine ND ug/L 01/02/18 19:05 91-94-112/29/17 10:1520.0 1
2,4-Dichlorophenol ND ug/L 01/02/18 19:05 120-83-212/29/17 10:1510.0 1
2,6-Dichlorophenol ND ug/L 01/02/18 19:05 87-65-012/29/17 10:1510.0 1
Diethylphthalate ND ug/L 01/02/18 19:05 84-66-212/29/17 10:1510.0 1
Dimethoate ND ug/L 01/02/18 19:05 60-51-512/29/17 10:1510.0 1
P-Dimethylaminoazobenzene ND ug/L 01/02/18 19:05 60-11-712/29/17 10:155.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 01/02/18 19:05 57-97-612/29/17 10:1510.0 1
3,3'-Dimethylbenzidine ND ug/L 01/02/18 19:05 119-93-712/29/17 10:1510.0 1
2,4-Dimethylphenol ND ug/L 01/02/18 19:05 105-67-912/29/17 10:1510.0 1
Dimethylphthalate ND ug/L 01/02/18 19:05 131-11-312/29/17 10:1510.0 1
Di-n-butylphthalate ND ug/L 01/02/18 19:05 84-74-212/29/17 10:1510.0 1
4,6-Dinitro-2-methylphenol ND ug/L 01/02/18 19:05 534-52-112/29/17 10:1520.0 1
1,3-Dinitrobenzene ND ug/L 01/02/18 19:05 99-65-012/29/17 10:1520.0 1
2,4-Dinitrophenol ND ug/L 01/02/18 19:05 51-28-512/29/17 10:1550.0 1
2,4-Dinitrotoluene ND ug/L 01/02/18 19:05 121-14-212/29/17 10:1510.0 1
2,6-Dinitrotoluene ND ug/L 01/02/18 19:05 606-20-212/29/17 10:1510.0 1
Di-n-octylphthalate ND ug/L 01/02/18 19:05 117-84-012/29/17 10:1510.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
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Page 61 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-14 Lab ID:92368450011 Collected:12/28/17 13:35 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Diphenylamine ND ug/L 01/02/18 19:05 122-39-412/29/17 10:1510.0 1
Disulfoton ND ug/L 01/02/18 19:05 298-04-412/29/17 10:1510.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 01/02/18 19:05 117-81-712/29/17 10:156.0 1
Ethyl methanesulfonate ND ug/L 01/02/18 19:05 62-50-012/29/17 10:1520.0 1
Famphur ND ug/L 01/02/18 19:05 52-85-712/29/17 10:1510.0 1
Fluoranthene ND ug/L 01/02/18 19:05 206-44-012/29/17 10:1510.0 1
Fluorene ND ug/L 01/02/18 19:05 86-73-712/29/17 10:1510.0 1
Hexachlorobenzene ND ug/L 01/02/18 19:05 118-74-112/29/17 10:1510.0 1
Hexachlorocyclopentadiene ND ug/L 01/02/18 19:05 77-47-412/29/17 10:1510.0 1
Hexachloroethane ND ug/L 01/02/18 19:05 67-72-112/29/17 10:1510.0 1
Hexachlorophene ND ug/L 01/02/18 19:05 70-30-412/29/17 10:151001
Indeno(1,2,3-cd)pyrene ND ug/L 01/02/18 19:05 193-39-512/29/17 10:1510.0 1
Isodrin ND ug/L 01/02/18 19:05 465-73-612/29/17 10:1520.0 1
Isophorone ND ug/L 01/02/18 19:05 78-59-112/29/17 10:1510.0 1
Isosafrole ND ug/L 01/02/18 19:05 120-58-112/29/17 10:1510.0 1
Kepone ND ug/L 01/02/18 19:05 143-50-012/29/17 10:1510.0 1
Methapyrilene ND ug/L 01/02/18 19:05 91-80-5 L212/29/17 10:1550.0 1
3-Methylcholanthrene ND ug/L 01/02/18 19:05 56-49-512/29/17 10:1510.0 1
Methyl methanesulfonate ND ug/L 01/02/18 19:05 66-27-3 L112/29/17 10:155.0 1
2-Methylnaphthalene ND ug/L 01/02/18 19:05 91-57-612/29/17 10:1510.0 1
Methyl parathion ND ug/L 01/02/18 19:05 298-00-012/29/17 10:1510.0 1
2-Methylphenol(o-Cresol)ND ug/L 01/02/18 19:05 95-48-712/29/17 10:1510.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 01/02/18 19:05 15831-10-412/29/17 10:1510.0 1
1-Naphthalenamine ND ug/L 01/02/18 19:05 134-32-712/29/17 10:155.0 1
2-Naphthalenamine ND ug/L 01/02/18 19:05 91-59-812/29/17 10:155.0 1
1,4-Naphthoquinone ND ug/L 01/02/18 19:05 130-15-412/29/17 10:155.0 1
2-Nitroaniline ND ug/L 01/02/18 19:05 88-74-412/29/17 10:1550.0 1
3-Nitroaniline ND ug/L 01/02/18 19:05 99-09-212/29/17 10:1550.0 1
4-Nitroaniline ND ug/L 01/02/18 19:05 100-01-612/29/17 10:1520.0 1
Nitrobenzene ND ug/L 01/02/18 19:05 98-95-312/29/17 10:1510.0 1
2-Nitrophenol ND ug/L 01/02/18 19:05 88-75-512/29/17 10:1510.0 1
4-Nitrophenol ND ug/L 01/02/18 19:05 100-02-712/29/17 10:1550.0 1
5-Nitro-o-toluidine ND ug/L 01/02/18 19:05 99-55-812/29/17 10:1510.0 1
N-Nitrosodiethylamine ND ug/L 01/02/18 19:05 55-18-512/29/17 10:1520.0 1
N-Nitrosodimethylamine ND ug/L 01/02/18 19:05 62-75-912/29/17 10:1510.0 1
N-Nitroso-di-n-butylamine ND ug/L 01/02/18 19:05 924-16-312/29/17 10:1510.0 1
N-Nitroso-di-n-propylamine ND ug/L 01/02/18 19:05 621-64-712/29/17 10:1510.0 1
N-Nitrosodiphenylamine ND ug/L 01/02/18 19:05 86-30-612/29/17 10:1510.0 1
N-Nitrosomethylethylamine ND ug/L 01/02/18 19:05 10595-95-612/29/17 10:1510.0 1
N-Nitrosopiperidine ND ug/L 01/02/18 19:05 100-75-412/29/17 10:1520.0 1
N-Nitrosopyrrolidine ND ug/L 01/02/18 19:05 930-55-212/29/17 10:1510.0 1
O,O,O-Triethylphosphorothioate ND ug/L 01/02/18 19:05 126-68-1 L212/29/17 10:1510.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 01/02/18 19:05 108-60-112/29/17 10:1510.0 1
Parathion (Ethyl parathion)ND ug/L 01/02/18 19:05 56-38-212/29/17 10:1510.0 1
Pentachlorobenzene ND ug/L 01/02/18 19:05 608-93-512/29/17 10:1510.0 1
Pentachloronitrobenzene ND ug/L 01/02/18 19:05 82-68-812/29/17 10:1520.0 1
Pentachlorophenol ND ug/L 01/02/18 19:05 87-86-512/29/17 10:1525.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-14 Lab ID:92368450011 Collected:12/28/17 13:35 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Phenacetin ND ug/L 01/02/18 19:05 62-44-212/29/17 10:1520.0 1
Phenanthrene ND ug/L 01/02/18 19:05 85-01-812/29/17 10:1510.0 1
Phenol ND ug/L 01/02/18 19:05 108-95-212/29/17 10:1510.0 1
p-Phenylenediamine ND ug/L 01/02/18 19:05 106-50-312/29/17 10:1510.0 1
Phorate ND ug/L 01/02/18 19:05 298-02-212/29/17 10:1510.0 1
Pronamide ND ug/L 01/02/18 19:05 23950-58-512/29/17 10:1510.0 1
Pyrene ND ug/L 01/02/18 19:05 129-00-012/29/17 10:1510.0 1
Safrole ND ug/L 01/02/18 19:05 94-59-712/29/17 10:1510.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 01/02/18 19:05 95-94-312/29/17 10:1510.0 1
2,3,4,6-Tetrachlorophenol ND ug/L 01/02/18 19:05 58-90-212/29/17 10:1510.0 1
Thionazin ND ug/L 01/02/18 19:05 297-97-212/29/17 10:1520.0 1
O-Toluidine ND ug/L 01/02/18 19:05 95-53-412/29/17 10:1510.0 1
2,4,5-Trichlorophenol ND ug/L 01/02/18 19:05 95-95-412/29/17 10:1510.0 1
2,4,6-Trichlorophenol ND ug/L 01/02/18 19:05 88-06-212/29/17 10:1510.0 1
1,3,5-Trinitrobenzene ND ug/L 01/02/18 19:05 99-35-4 L212/29/17 10:1510.0 1
Surrogates
Nitrobenzene-d5 (S)71 %01/02/18 19:05 4165-60-012/29/17 10:1521-110 1
2-Fluorobiphenyl (S)67 %01/02/18 19:05 321-60-812/29/17 10:1527-110 1
Terphenyl-d14 (S)87 %01/02/18 19:05 1718-51-012/29/17 10:1531-107 1
Phenol-d6 (S)19 %01/02/18 19:05 13127-88-312/29/17 10:1510-110 1
2-Fluorophenol (S)32 %01/02/18 19:05 367-12-412/29/17 10:1512-110 1
2,4,6-Tribromophenol (S)80 %01/02/18 19:05 118-79-612/29/17 10:1527-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/18 04:00 67-64-125.0 1
Acetonitrile ND ug/L 01/03/18 04:00 75-05-850.0 1
Acrolein ND ug/L 01/03/18 04:00 107-02-810.0 1
Acrylonitrile ND ug/L 01/03/18 04:00 107-13-110.0 1
Allyl chloride ND ug/L 01/03/18 04:00 107-05-12.0 1
Benzene ND ug/L 01/03/18 04:00 71-43-21.0 1
Bromochloromethane ND ug/L 01/03/18 04:00 74-97-51.0 1
Bromodichloromethane ND ug/L 01/03/18 04:00 75-27-41.0 1
Bromoform ND ug/L 01/03/18 04:00 75-25-21.0 1
Bromomethane ND ug/L 01/03/18 04:00 74-83-92.0 1
2-Butanone (MEK)ND ug/L 01/03/18 04:00 78-93-35.0 1
Carbon disulfide ND ug/L 01/03/18 04:00 75-15-02.0 1
Carbon tetrachloride ND ug/L 01/03/18 04:00 56-23-51.0 1
Chlorobenzene ND ug/L 01/03/18 04:00 108-90-71.0 1
Chloroethane ND ug/L 01/03/18 04:00 75-00-31.0 1
Chloroform ND ug/L 01/03/18 04:00 67-66-31.0 1
Chloromethane ND ug/L 01/03/18 04:00 74-87-31.0 1
Chloroprene ND ug/L 01/03/18 04:00 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/18 04:00 96-12-8 L22.0 1
Dibromochloromethane ND ug/L 01/03/18 04:00 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/18 04:00 106-93-41.0 1
Dibromomethane ND ug/L 01/03/18 04:00 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 01/03/18 04:00 95-50-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-14 Lab ID:92368450011 Collected:12/28/17 13:35 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,3-Dichlorobenzene ND ug/L 01/03/18 04:00 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 01/03/18 04:00 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/18 04:00 110-57-61.0 1
Dichlorodifluoromethane 3.6 ug/L 01/03/18 04:00 75-71-81.0 1
1,1-Dichloroethane ND ug/L 01/03/18 04:00 75-34-31.0 1
1,2-Dichloroethane ND ug/L 01/03/18 04:00 107-06-21.0 1
1,1-Dichloroethene ND ug/L 01/03/18 04:00 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 01/03/18 04:00 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 01/03/18 04:00 156-60-51.0 1
1,2-Dichloropropane ND ug/L 01/03/18 04:00 78-87-51.0 1
1,3-Dichloropropane ND ug/L 01/03/18 04:00 142-28-91.0 1
2,2-Dichloropropane ND ug/L 01/03/18 04:00 594-20-71.0 1
1,1-Dichloropropene ND ug/L 01/03/18 04:00 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 01/03/18 04:00 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 01/03/18 04:00 10061-02-61.0 1
Ethylbenzene ND ug/L 01/03/18 04:00 100-41-41.0 1
Ethyl methacrylate ND ug/L 01/03/18 04:00 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 01/03/18 04:00 87-68-31.0 1
2-Hexanone ND ug/L 01/03/18 04:00 591-78-65.0 1
Iodomethane ND ug/L 01/03/18 04:00 74-88-45.0 1
Isobutanol ND ug/L 01/03/18 04:00 78-83-11001
Methacrylonitrile ND ug/L 01/03/18 04:00 126-98-710.0 1
Methylene Chloride ND ug/L 01/03/18 04:00 75-09-21.0 1
Methyl methacrylate ND ug/L 01/03/18 04:00 80-62-6 L22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/18 04:00 108-10-15.0 1
Naphthalene ND ug/L 01/03/18 04:00 91-20-31.0 1
Propionitrile ND ug/L 01/03/18 04:00 107-12-020.0 1
Styrene ND ug/L 01/03/18 04:00 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/18 04:00 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/18 04:00 79-34-51.0 1
Tetrachloroethene ND ug/L 01/03/18 04:00 127-18-41.0 1
Tetrahydrofuran ND ug/L 01/03/18 04:00 109-99-910.0 1
Toluene ND ug/L 01/03/18 04:00 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 01/03/18 04:00 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 01/03/18 04:00 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 01/03/18 04:00 79-00-51.0 1
Trichloroethene ND ug/L 01/03/18 04:00 79-01-61.0 1
Trichlorofluoromethane 0.80J ug/L 01/03/18 04:00 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 01/03/18 04:00 96-18-41.0 1
Vinyl acetate ND ug/L 01/03/18 04:00 108-05-42.0 1
Vinyl chloride ND ug/L 01/03/18 04:00 75-01-41.0 1
Xylene (Total)ND ug/L 01/03/18 04:00 1330-20-71.0 1
m&p-Xylene ND ug/L 01/03/18 04:00 179601-23-12.0 1
o-Xylene ND ug/L 01/03/18 04:00 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)99 %01/03/18 04:00 460-00-470-130 1
1,2-Dichloroethane-d4 (S)85 %01/03/18 04:00 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-14 Lab ID:92368450011 Collected:12/28/17 13:35 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Surrogates
Toluene-d8 (S)112 %01/03/18 04:00 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:SW-2 Lab ID:92368450012 Collected:12/28/17 14:50 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By STV 01/05/18 11:271
Collected Date 12/28/17 01/05/18 11:271
Collected Time 14:30 01/05/18 11:271
pH 6.8 Std. Units 01/05/18 11:270.10 1
Temperature 3.2 deg C 01/05/18 11:270.50 1
Specific Conductance 783.6 umhos/cm 01/05/18 11:271.0 1
Oxygen, Dissolved 2.4 mg/L 01/05/18 11:27 7782-44-71
REDOX -68.9 mV 01/05/18 11:271
Turbidity 554.5 NTU 01/05/18 11:271.0 1
Odor SULFURIC 01/05/18 11:271
Appearance MUDDY 01/05/18 11:271
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 01/03/18 15:51 83-32-912/29/17 10:151001
Acenaphthylene ND ug/L 01/03/18 15:51 208-96-812/29/17 10:151001
Acetophenone ND ug/L 01/03/18 15:51 98-86-212/29/17 10:151001
2-Acetylaminofluorene ND ug/L 01/03/18 15:51 53-96-3 L212/29/17 10:152001
4-Aminobiphenyl ND ug/L 01/03/18 15:51 92-67-112/29/17 10:151001
Anthracene ND ug/L 01/03/18 15:51 120-12-712/29/17 10:151001
Benzo(a)anthracene ND ug/L 01/03/18 15:51 56-55-312/29/17 10:151001
Benzo(a)pyrene ND ug/L 01/03/18 15:51 50-32-812/29/17 10:151001
Benzo(b)fluoranthene ND ug/L 01/03/18 15:51 205-99-212/29/17 10:151001
Benzo(g,h,i)perylene ND ug/L 01/03/18 15:51 191-24-212/29/17 10:151001
Benzo(k)fluoranthene ND ug/L 01/03/18 15:51 207-08-912/29/17 10:151001
Benzyl alcohol ND ug/L 01/03/18 15:51 100-51-612/29/17 10:152001
4-Bromophenylphenyl ether ND ug/L 01/03/18 15:51 101-55-312/29/17 10:151001
Butylbenzylphthalate ND ug/L 01/03/18 15:51 85-68-712/29/17 10:151001
4-Chloro-3-methylphenol ND ug/L 01/03/18 15:51 59-50-712/29/17 10:152001
4-Chloroaniline ND ug/L 01/03/18 15:51 106-47-812/29/17 10:152001
Chlorobenzilate ND ug/L 01/03/18 15:51 510-15-612/29/17 10:151001
bis(2-Chloroethoxy)methane ND ug/L 01/03/18 15:51 111-91-112/29/17 10:151001
bis(2-Chloroethyl) ether ND ug/L 01/03/18 15:51 111-44-412/29/17 10:151001
2-Chloronaphthalene ND ug/L 01/03/18 15:51 91-58-712/29/17 10:151001
2-Chlorophenol ND ug/L 01/03/18 15:51 95-57-812/29/17 10:151001
4-Chlorophenylphenyl ether ND ug/L 01/03/18 15:51 7005-72-312/29/17 10:151001
Chrysene ND ug/L 01/03/18 15:51 218-01-912/29/17 10:151001
Diallate ND ug/L 01/03/18 15:51 2303-16-412/29/17 10:151001
Dibenz(a,h)anthracene ND ug/L 01/03/18 15:51 53-70-312/29/17 10:151001
Dibenzofuran ND ug/L 01/03/18 15:51 132-64-912/29/17 10:151001
3,3'-Dichlorobenzidine ND ug/L 01/03/18 15:51 91-94-112/29/17 10:152001
2,4-Dichlorophenol ND ug/L 01/03/18 15:51 120-83-212/29/17 10:151001
2,6-Dichlorophenol ND ug/L 01/03/18 15:51 87-65-012/29/17 10:151001
Diethylphthalate ND ug/L 01/03/18 15:51 84-66-212/29/17 10:151001
Dimethoate ND ug/L 01/03/18 15:51 60-51-512/29/17 10:151001
P-Dimethylaminoazobenzene ND ug/L 01/03/18 15:51 60-11-712/29/17 10:1550.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 01/03/18 15:51 57-97-612/29/17 10:151001
3,3'-Dimethylbenzidine ND ug/L 01/03/18 15:51 119-93-712/29/17 10:151001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 66 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:SW-2 Lab ID:92368450012 Collected:12/28/17 14:50 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2,4-Dimethylphenol ND ug/L 01/03/18 15:51 105-67-912/29/17 10:151001
Dimethylphthalate ND ug/L 01/03/18 15:51 131-11-312/29/17 10:151001
Di-n-butylphthalate ND ug/L 01/03/18 15:51 84-74-212/29/17 10:151001
4,6-Dinitro-2-methylphenol ND ug/L 01/03/18 15:51 534-52-112/29/17 10:152001
1,3-Dinitrobenzene ND ug/L 01/03/18 15:51 99-65-012/29/17 10:152001
2,4-Dinitrophenol ND ug/L 01/03/18 15:51 51-28-512/29/17 10:155001
2,4-Dinitrotoluene ND ug/L 01/03/18 15:51 121-14-212/29/17 10:151001
2,6-Dinitrotoluene ND ug/L 01/03/18 15:51 606-20-212/29/17 10:151001
Di-n-octylphthalate ND ug/L 01/03/18 15:51 117-84-012/29/17 10:151001
Diphenylamine ND ug/L 01/03/18 15:51 122-39-412/29/17 10:151001
Disulfoton ND ug/L 01/03/18 15:51 298-04-412/29/17 10:151001
bis(2-Ethylhexyl)phthalate ND ug/L 01/03/18 15:51 117-81-712/29/17 10:1560.0 1
Ethyl methanesulfonate ND ug/L 01/03/18 15:51 62-50-012/29/17 10:152001
Famphur ND ug/L 01/03/18 15:51 52-85-712/29/17 10:151001
Fluoranthene ND ug/L 01/03/18 15:51 206-44-012/29/17 10:151001
Fluorene ND ug/L 01/03/18 15:51 86-73-712/29/17 10:151001
Hexachlorobenzene ND ug/L 01/03/18 15:51 118-74-112/29/17 10:151001
Hexachlorocyclopentadiene ND ug/L 01/03/18 15:51 77-47-412/29/17 10:151001
Hexachloroethane ND ug/L 01/03/18 15:51 67-72-112/29/17 10:151001
Hexachlorophene ND ug/L 01/03/18 15:51 70-30-412/29/17 10:1510001
Indeno(1,2,3-cd)pyrene ND ug/L 01/03/18 15:51 193-39-512/29/17 10:151001
Isodrin ND ug/L 01/03/18 15:51 465-73-612/29/17 10:152001
Isophorone ND ug/L 01/03/18 15:51 78-59-112/29/17 10:151001
Isosafrole ND ug/L 01/03/18 15:51 120-58-112/29/17 10:151001
Kepone ND ug/L 01/03/18 15:51 143-50-012/29/17 10:151001
Methapyrilene ND ug/L 01/03/18 15:51 91-80-5 L212/29/17 10:155001
3-Methylcholanthrene ND ug/L 01/03/18 15:51 56-49-512/29/17 10:151001
Methyl methanesulfonate ND ug/L 01/03/18 15:51 66-27-3 L112/29/17 10:1550.0 1
2-Methylnaphthalene ND ug/L 01/03/18 15:51 91-57-612/29/17 10:151001
Methyl parathion ND ug/L 01/03/18 15:51 298-00-012/29/17 10:151001
2-Methylphenol(o-Cresol)ND ug/L 01/03/18 15:51 95-48-712/29/17 10:151001
3&4-Methylphenol(m&p Cresol)ND ug/L 01/03/18 15:51 15831-10-412/29/17 10:151001
1-Naphthalenamine ND ug/L 01/03/18 15:51 134-32-712/29/17 10:1550.0 1
2-Naphthalenamine ND ug/L 01/03/18 15:51 91-59-812/29/17 10:1550.0 1
1,4-Naphthoquinone ND ug/L 01/03/18 15:51 130-15-412/29/17 10:1550.0 1
2-Nitroaniline ND ug/L 01/03/18 15:51 88-74-412/29/17 10:155001
3-Nitroaniline ND ug/L 01/03/18 15:51 99-09-212/29/17 10:155001
4-Nitroaniline ND ug/L 01/03/18 15:51 100-01-612/29/17 10:152001
Nitrobenzene ND ug/L 01/03/18 15:51 98-95-312/29/17 10:151001
2-Nitrophenol ND ug/L 01/03/18 15:51 88-75-512/29/17 10:151001
4-Nitrophenol ND ug/L 01/03/18 15:51 100-02-712/29/17 10:155001
5-Nitro-o-toluidine ND ug/L 01/03/18 15:51 99-55-812/29/17 10:151001
N-Nitrosodiethylamine ND ug/L 01/03/18 15:51 55-18-512/29/17 10:152001
N-Nitrosodimethylamine ND ug/L 01/03/18 15:51 62-75-912/29/17 10:151001
N-Nitroso-di-n-butylamine ND ug/L 01/03/18 15:51 924-16-312/29/17 10:151001
N-Nitroso-di-n-propylamine ND ug/L 01/03/18 15:51 621-64-712/29/17 10:151001
N-Nitrosodiphenylamine ND ug/L 01/03/18 15:51 86-30-612/29/17 10:151001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 67 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:SW-2 Lab ID:92368450012 Collected:12/28/17 14:50 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
N-Nitrosomethylethylamine ND ug/L 01/03/18 15:51 10595-95-612/29/17 10:151001
N-Nitrosopiperidine ND ug/L 01/03/18 15:51 100-75-412/29/17 10:152001
N-Nitrosopyrrolidine ND ug/L 01/03/18 15:51 930-55-212/29/17 10:151001
O,O,O-Triethylphosphorothioate ND ug/L 01/03/18 15:51 126-68-1 L212/29/17 10:151001
2,2'-Oxybis(1-chloropropane)ND ug/L 01/03/18 15:51 108-60-112/29/17 10:151001
Parathion (Ethyl parathion)ND ug/L 01/03/18 15:51 56-38-212/29/17 10:151001
Pentachlorobenzene ND ug/L 01/03/18 15:51 608-93-512/29/17 10:151001
Pentachloronitrobenzene ND ug/L 01/03/18 15:51 82-68-812/29/17 10:152001
Pentachlorophenol ND ug/L 01/03/18 15:51 87-86-512/29/17 10:152501
Phenacetin ND ug/L 01/03/18 15:51 62-44-212/29/17 10:152001
Phenanthrene ND ug/L 01/03/18 15:51 85-01-812/29/17 10:151001
Phenol ND ug/L 01/03/18 15:51 108-95-212/29/17 10:151001
p-Phenylenediamine ND ug/L 01/03/18 15:51 106-50-312/29/17 10:151001
Phorate ND ug/L 01/03/18 15:51 298-02-212/29/17 10:151001
Pronamide ND ug/L 01/03/18 15:51 23950-58-512/29/17 10:151001
Pyrene ND ug/L 01/03/18 15:51 129-00-012/29/17 10:151001
Safrole ND ug/L 01/03/18 15:51 94-59-712/29/17 10:151001
1,2,4,5-Tetrachlorobenzene ND ug/L 01/03/18 15:51 95-94-312/29/17 10:151001
2,3,4,6-Tetrachlorophenol ND ug/L 01/03/18 15:51 58-90-212/29/17 10:151001
Thionazin ND ug/L 01/03/18 15:51 297-97-212/29/17 10:152001
O-Toluidine ND ug/L 01/03/18 15:51 95-53-412/29/17 10:151001
2,4,5-Trichlorophenol ND ug/L 01/03/18 15:51 95-95-412/29/17 10:151001
2,4,6-Trichlorophenol ND ug/L 01/03/18 15:51 88-06-212/29/17 10:151001
1,3,5-Trinitrobenzene ND ug/L 01/03/18 15:51 99-35-4 L212/29/17 10:151001
Surrogates
Nitrobenzene-d5 (S)70 %01/03/18 15:51 4165-60-012/29/17 10:1521-110 1
2-Fluorobiphenyl (S)70 %01/03/18 15:51 321-60-812/29/17 10:1527-110 1
Terphenyl-d14 (S)66 %01/03/18 15:51 1718-51-012/29/17 10:1531-107 1
Phenol-d6 (S)56 %01/03/18 15:51 13127-88-312/29/17 10:1510-110 1
2-Fluorophenol (S)56 %01/03/18 15:51 367-12-412/29/17 10:1512-110 1
2,4,6-Tribromophenol (S)88 %01/03/18 15:51 118-79-612/29/17 10:1527-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 12.9J ug/L 01/03/18 04:17 67-64-125.0 1
Acetonitrile ND ug/L 01/03/18 04:17 75-05-850.0 1
Acrolein ND ug/L 01/03/18 04:17 107-02-810.0 1
Acrylonitrile ND ug/L 01/03/18 04:17 107-13-110.0 1
Allyl chloride ND ug/L 01/03/18 04:17 107-05-12.0 1
Benzene ND ug/L 01/03/18 04:17 71-43-21.0 1
Bromochloromethane ND ug/L 01/03/18 04:17 74-97-51.0 1
Bromodichloromethane ND ug/L 01/03/18 04:17 75-27-41.0 1
Bromoform ND ug/L 01/03/18 04:17 75-25-21.0 1
Bromomethane ND ug/L 01/03/18 04:17 74-83-92.0 1
2-Butanone (MEK)ND ug/L 01/03/18 04:17 78-93-35.0 1
Carbon disulfide ND ug/L 01/03/18 04:17 75-15-02.0 1
Carbon tetrachloride ND ug/L 01/03/18 04:17 56-23-51.0 1
Chlorobenzene ND ug/L 01/03/18 04:17 108-90-71.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:SW-2 Lab ID:92368450012 Collected:12/28/17 14:50 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Chloroethane ND ug/L 01/03/18 04:17 75-00-31.0 1
Chloroform ND ug/L 01/03/18 04:17 67-66-31.0 1
Chloromethane ND ug/L 01/03/18 04:17 74-87-31.0 1
Chloroprene ND ug/L 01/03/18 04:17 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/18 04:17 96-12-8 L22.0 1
Dibromochloromethane ND ug/L 01/03/18 04:17 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/18 04:17 106-93-41.0 1
Dibromomethane ND ug/L 01/03/18 04:17 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 01/03/18 04:17 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 01/03/18 04:17 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 01/03/18 04:17 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/18 04:17 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 01/03/18 04:17 75-71-81.0 1
1,1-Dichloroethane ND ug/L 01/03/18 04:17 75-34-31.0 1
1,2-Dichloroethane ND ug/L 01/03/18 04:17 107-06-21.0 1
1,1-Dichloroethene ND ug/L 01/03/18 04:17 75-35-41.0 1
cis-1,2-Dichloroethene 0.33J ug/L 01/03/18 04:17 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 01/03/18 04:17 156-60-51.0 1
1,2-Dichloropropane ND ug/L 01/03/18 04:17 78-87-51.0 1
1,3-Dichloropropane ND ug/L 01/03/18 04:17 142-28-91.0 1
2,2-Dichloropropane ND ug/L 01/03/18 04:17 594-20-71.0 1
1,1-Dichloropropene ND ug/L 01/03/18 04:17 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 01/03/18 04:17 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 01/03/18 04:17 10061-02-61.0 1
Ethylbenzene ND ug/L 01/03/18 04:17 100-41-41.0 1
Ethyl methacrylate ND ug/L 01/03/18 04:17 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 01/03/18 04:17 87-68-31.0 1
2-Hexanone ND ug/L 01/03/18 04:17 591-78-65.0 1
Iodomethane ND ug/L 01/03/18 04:17 74-88-45.0 1
Isobutanol ND ug/L 01/03/18 04:17 78-83-11001
Methacrylonitrile ND ug/L 01/03/18 04:17 126-98-710.0 1
Methylene Chloride ND ug/L 01/03/18 04:17 75-09-21.0 1
Methyl methacrylate ND ug/L 01/03/18 04:17 80-62-6 L22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/18 04:17 108-10-15.0 1
Naphthalene ND ug/L 01/03/18 04:17 91-20-31.0 1
Propionitrile ND ug/L 01/03/18 04:17 107-12-020.0 1
Styrene ND ug/L 01/03/18 04:17 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/18 04:17 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/18 04:17 79-34-51.0 1
Tetrachloroethene ND ug/L 01/03/18 04:17 127-18-41.0 1
Tetrahydrofuran 61.3 ug/L 01/03/18 04:17 109-99-910.0 1
Toluene ND ug/L 01/03/18 04:17 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 01/03/18 04:17 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 01/03/18 04:17 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 01/03/18 04:17 79-00-51.0 1
Trichloroethene ND ug/L 01/03/18 04:17 79-01-61.0 1
Trichlorofluoromethane ND ug/L 01/03/18 04:17 75-69-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:SW-2 Lab ID:92368450012 Collected:12/28/17 14:50 Received:12/29/17 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2,3-Trichloropropane ND ug/L 01/03/18 04:17 96-18-41.0 1
Vinyl acetate ND ug/L 01/03/18 04:17 108-05-42.0 1
Vinyl chloride ND ug/L 01/03/18 04:17 75-01-41.0 1
Xylene (Total)ND ug/L 01/03/18 04:17 1330-20-71.0 1
m&p-Xylene ND ug/L 01/03/18 04:17 179601-23-12.0 1
o-Xylene ND ug/L 01/03/18 04:17 95-47-61.0 1
Surrogates4-Bromofluorobenzene (S)101 %01/03/18 04:17 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %01/03/18 04:17 17060-07-070-130 1
Toluene-d8 (S)113 %01/03/18 04:17 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-4R Lab ID:92368450013 Collected:12/29/17 10:20 Received:12/29/17 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By GLG 01/05/18 11:371
Collected Date 12/29/17 01/05/18 11:371
Collected Time 10:20 01/05/18 11:371
pH 6.1 Std. Units 01/05/18 11:370.10 1
Temperature 11.8 deg C 01/05/18 11:370.50 1
Static Water Level 9.44 feet 01/05/18 11:371
Specific Conductance 1140 umhos/cm 01/05/18 11:371.0 1
Oxygen, Dissolved 0.6 mg/L 01/05/18 11:37 7782-44-71
Total Well Depth 20.0 feet 01/05/18 11:371
REDOX 100.2 mV 01/05/18 11:371
Turbidity 9.6 NTU 01/05/18 11:371.0 1
Odor NONE 01/05/18 11:371
Appearance CLEAR 01/05/18 11:371
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 01/02/18 21:33 309-00-201/02/18 07:110.050 1
alpha-BHC ND ug/L 01/02/18 21:33 319-84-601/02/18 07:110.050 1
beta-BHC ND ug/L 01/02/18 21:33 319-85-701/02/18 07:110.050 1
delta-BHC ND ug/L 01/02/18 21:33 319-86-801/02/18 07:110.050 1
gamma-BHC (Lindane)ND ug/L 01/02/18 21:33 58-89-901/02/18 07:110.050 1
Chlordane (Technical)ND ug/L 01/02/18 21:33 57-74-901/02/18 07:110.20 1
4,4'-DDD ND ug/L 01/02/18 21:33 72-54-801/02/18 07:110.050 1
4,4'-DDE ND ug/L 01/02/18 21:33 72-55-901/02/18 07:110.050 1
4,4'-DDT ND ug/L 01/02/18 21:33 50-29-301/02/18 07:110.050 1
Dieldrin ND ug/L 01/02/18 21:33 60-57-101/02/18 07:110.050 1
Endosulfan I ND ug/L 01/02/18 21:33 959-98-801/02/18 07:110.050 1
Endosulfan II ND ug/L 01/02/18 21:33 33213-65-901/02/18 07:110.050 1
Endosulfan sulfate ND ug/L 01/02/18 21:33 1031-07-801/02/18 07:110.050 1
Endrin ND ug/L 01/02/18 21:33 72-20-801/02/18 07:110.050 1
Endrin aldehyde ND ug/L 01/02/18 21:33 7421-93-401/02/18 07:110.050 1
Heptachlor ND ug/L 01/02/18 21:33 76-44-801/02/18 07:110.050 1
Heptachlor epoxide ND ug/L 01/02/18 21:33 1024-57-301/02/18 07:110.050 1
Methoxychlor ND ug/L 01/02/18 21:33 72-43-501/02/18 07:110.15 1
Toxaphene ND ug/L 01/02/18 21:33 8001-35-201/02/18 07:110.20 1
Surrogates
Tetrachloro-m-xylene (S)69 %01/02/18 21:33 877-09-801/02/18 07:1120-130 1
Decachlorobiphenyl (S)60 %01/02/18 21:33 2051-24-301/02/18 07:1120-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 01/02/18 19:23 12674-11-201/02/18 07:110.50 1
PCB-1221 (Aroclor 1221)ND ug/L 01/02/18 19:23 11104-28-201/02/18 07:110.50 1
PCB-1232 (Aroclor 1232)ND ug/L 01/02/18 19:23 11141-16-501/02/18 07:110.50 1
PCB-1242 (Aroclor 1242)ND ug/L 01/02/18 19:23 53469-21-901/02/18 07:110.50 1
PCB-1248 (Aroclor 1248)ND ug/L 01/02/18 19:23 12672-29-601/02/18 07:110.50 1
PCB-1254 (Aroclor 1254)ND ug/L 01/02/18 19:23 11097-69-101/02/18 07:110.50 1
PCB-1260 (Aroclor 1260)ND ug/L 01/02/18 19:23 11096-82-501/02/18 07:110.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-4R Lab ID:92368450013 Collected:12/29/17 10:20 Received:12/29/17 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
Surrogates
Decachlorobiphenyl (S)61 %01/02/18 19:23 2051-24-301/02/18 07:1110-132 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 01/03/18 17:49 83-32-901/02/18 08:2210.0 1
Acenaphthylene ND ug/L 01/03/18 17:49 208-96-801/02/18 08:2210.0 1
Acetophenone ND ug/L 01/03/18 17:49 98-86-201/02/18 08:2210.0 1
2-Acetylaminofluorene ND ug/L 01/03/18 17:49 53-96-3 L201/02/18 08:2220.0 1
4-Aminobiphenyl ND ug/L 01/03/18 17:49 92-67-101/02/18 08:2210.0 1
Anthracene ND ug/L 01/03/18 17:49 120-12-701/02/18 08:2210.0 1
Benzo(a)anthracene ND ug/L 01/03/18 17:49 56-55-301/02/18 08:2210.0 1
Benzo(a)pyrene ND ug/L 01/03/18 17:49 50-32-801/02/18 08:2210.0 1
Benzo(b)fluoranthene ND ug/L 01/03/18 17:49 205-99-201/02/18 08:2210.0 1
Benzo(g,h,i)perylene ND ug/L 01/03/18 17:49 191-24-201/02/18 08:2210.0 1
Benzo(k)fluoranthene ND ug/L 01/03/18 17:49 207-08-901/02/18 08:2210.0 1
Benzyl alcohol ND ug/L 01/03/18 17:49 100-51-601/02/18 08:2220.0 1
4-Bromophenylphenyl ether ND ug/L 01/03/18 17:49 101-55-301/02/18 08:2210.0 1
Butylbenzylphthalate ND ug/L 01/03/18 17:49 85-68-701/02/18 08:2210.0 1
4-Chloro-3-methylphenol ND ug/L 01/03/18 17:49 59-50-701/02/18 08:2220.0 1
4-Chloroaniline ND ug/L 01/03/18 17:49 106-47-801/02/18 08:2220.0 1
Chlorobenzilate ND ug/L 01/03/18 17:49 510-15-601/02/18 08:2210.0 1
bis(2-Chloroethoxy)methane ND ug/L 01/03/18 17:49 111-91-101/02/18 08:2210.0 1
bis(2-Chloroethyl) ether ND ug/L 01/03/18 17:49 111-44-401/02/18 08:2210.0 1
2-Chloronaphthalene ND ug/L 01/03/18 17:49 91-58-701/02/18 08:2210.0 1
2-Chlorophenol ND ug/L 01/03/18 17:49 95-57-801/02/18 08:2210.0 1
4-Chlorophenylphenyl ether ND ug/L 01/03/18 17:49 7005-72-301/02/18 08:2210.0 1
Chrysene ND ug/L 01/03/18 17:49 218-01-901/02/18 08:2210.0 1
Diallate ND ug/L 01/03/18 17:49 2303-16-401/02/18 08:2210.0 1
Dibenz(a,h)anthracene ND ug/L 01/03/18 17:49 53-70-301/02/18 08:2210.0 1
Dibenzofuran ND ug/L 01/03/18 17:49 132-64-901/02/18 08:2210.0 1
3,3'-Dichlorobenzidine ND ug/L 01/03/18 17:49 91-94-101/02/18 08:2220.0 1
2,4-Dichlorophenol ND ug/L 01/03/18 17:49 120-83-201/02/18 08:2210.0 1
2,6-Dichlorophenol ND ug/L 01/03/18 17:49 87-65-001/02/18 08:2210.0 1
Diethylphthalate ND ug/L 01/03/18 17:49 84-66-201/02/18 08:2210.0 1
Dimethoate ND ug/L 01/03/18 17:49 60-51-501/02/18 08:2210.0 1
P-Dimethylaminoazobenzene ND ug/L 01/03/18 17:49 60-11-701/02/18 08:225.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 01/03/18 17:49 57-97-601/02/18 08:2210.0 1
3,3'-Dimethylbenzidine ND ug/L 01/03/18 17:49 119-93-701/02/18 08:2210.0 1
2,4-Dimethylphenol ND ug/L 01/03/18 17:49 105-67-901/02/18 08:2210.0 1
Dimethylphthalate ND ug/L 01/03/18 17:49 131-11-301/02/18 08:2210.0 1
Di-n-butylphthalate ND ug/L 01/03/18 17:49 84-74-201/02/18 08:2210.0 1
4,6-Dinitro-2-methylphenol ND ug/L 01/03/18 17:49 534-52-101/02/18 08:2220.0 1
1,3-Dinitrobenzene ND ug/L 01/03/18 17:49 99-65-001/02/18 08:2220.0 1
2,4-Dinitrophenol ND ug/L 01/03/18 17:49 51-28-501/02/18 08:2250.0 1
2,4-Dinitrotoluene ND ug/L 01/03/18 17:49 121-14-201/02/18 08:2210.0 1
2,6-Dinitrotoluene ND ug/L 01/03/18 17:49 606-20-201/02/18 08:2210.0 1
Di-n-octylphthalate ND ug/L 01/03/18 17:49 117-84-001/02/18 08:2210.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
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Page 72 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-4R Lab ID:92368450013 Collected:12/29/17 10:20 Received:12/29/17 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Diphenylamine ND ug/L 01/03/18 17:49 122-39-401/02/18 08:2210.0 1
Disulfoton ND ug/L 01/03/18 17:49 298-04-401/02/18 08:2210.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 01/03/18 17:49 117-81-701/02/18 08:226.0 1
Ethyl methanesulfonate ND ug/L 01/03/18 17:49 62-50-001/02/18 08:2220.0 1
Famphur ND ug/L 01/03/18 17:49 52-85-701/02/18 08:2210.0 1
Fluoranthene ND ug/L 01/03/18 17:49 206-44-001/02/18 08:2210.0 1
Fluorene ND ug/L 01/03/18 17:49 86-73-701/02/18 08:2210.0 1
Hexachlorobenzene ND ug/L 01/03/18 17:49 118-74-101/02/18 08:2210.0 1
Hexachlorocyclopentadiene ND ug/L 01/03/18 17:49 77-47-401/02/18 08:2210.0 1
Hexachloroethane ND ug/L 01/03/18 17:49 67-72-101/02/18 08:2210.0 1
Hexachlorophene ND ug/L 01/03/18 17:49 70-30-401/02/18 08:221001
Indeno(1,2,3-cd)pyrene ND ug/L 01/03/18 17:49 193-39-501/02/18 08:2210.0 1
Isodrin ND ug/L 01/03/18 17:49 465-73-601/02/18 08:2220.0 1
Isophorone ND ug/L 01/03/18 17:49 78-59-101/02/18 08:2210.0 1
Isosafrole ND ug/L 01/03/18 17:49 120-58-101/02/18 08:2210.0 1
Kepone ND ug/L 01/03/18 17:49 143-50-001/02/18 08:2210.0 1
Methapyrilene ND ug/L 01/03/18 17:49 91-80-501/02/18 08:2250.0 1
3-Methylcholanthrene ND ug/L 01/03/18 17:49 56-49-501/02/18 08:2210.0 1
Methyl methanesulfonate ND ug/L 01/03/18 17:49 66-27-3 L101/02/18 08:225.0 1
2-Methylnaphthalene ND ug/L 01/03/18 17:49 91-57-601/02/18 08:2210.0 1
Methyl parathion ND ug/L 01/03/18 17:49 298-00-001/02/18 08:2210.0 1
2-Methylphenol(o-Cresol)ND ug/L 01/03/18 17:49 95-48-701/02/18 08:2210.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 01/03/18 17:49 15831-10-401/02/18 08:2210.0 1
1-Naphthalenamine ND ug/L 01/03/18 17:49 134-32-701/02/18 08:225.0 1
2-Naphthalenamine ND ug/L 01/03/18 17:49 91-59-801/02/18 08:225.0 1
1,4-Naphthoquinone ND ug/L 01/03/18 17:49 130-15-401/02/18 08:225.0 1
2-Nitroaniline ND ug/L 01/03/18 17:49 88-74-401/02/18 08:2250.0 1
3-Nitroaniline ND ug/L 01/03/18 17:49 99-09-201/02/18 08:2250.0 1
4-Nitroaniline ND ug/L 01/03/18 17:49 100-01-601/02/18 08:2220.0 1
Nitrobenzene ND ug/L 01/03/18 17:49 98-95-301/02/18 08:2210.0 1
2-Nitrophenol ND ug/L 01/03/18 17:49 88-75-501/02/18 08:2210.0 1
4-Nitrophenol ND ug/L 01/03/18 17:49 100-02-701/02/18 08:2250.0 1
5-Nitro-o-toluidine ND ug/L 01/03/18 17:49 99-55-8 L201/02/18 08:2210.0 1
N-Nitrosodiethylamine ND ug/L 01/03/18 17:49 55-18-501/02/18 08:2220.0 1
N-Nitrosodimethylamine ND ug/L 01/03/18 17:49 62-75-901/02/18 08:2210.0 1
N-Nitroso-di-n-butylamine ND ug/L 01/03/18 17:49 924-16-301/02/18 08:2210.0 1
N-Nitroso-di-n-propylamine ND ug/L 01/03/18 17:49 621-64-701/02/18 08:2210.0 1
N-Nitrosodiphenylamine ND ug/L 01/03/18 17:49 86-30-601/02/18 08:2210.0 1
N-Nitrosomethylethylamine ND ug/L 01/03/18 17:49 10595-95-601/02/18 08:2210.0 1
N-Nitrosopiperidine ND ug/L 01/03/18 17:49 100-75-401/02/18 08:2220.0 1
N-Nitrosopyrrolidine ND ug/L 01/03/18 17:49 930-55-201/02/18 08:2210.0 1
O,O,O-Triethylphosphorothioate ND ug/L 01/03/18 17:49 126-68-101/02/18 08:2210.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 01/03/18 17:49 108-60-101/02/18 08:2210.0 1
Parathion (Ethyl parathion)ND ug/L 01/03/18 17:49 56-38-201/02/18 08:2210.0 1
Pentachlorobenzene ND ug/L 01/03/18 17:49 608-93-501/02/18 08:2210.0 1
Pentachloronitrobenzene ND ug/L 01/03/18 17:49 82-68-801/02/18 08:2220.0 1
Pentachlorophenol ND ug/L 01/03/18 17:49 87-86-501/02/18 08:2225.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 73 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-4R Lab ID:92368450013 Collected:12/29/17 10:20 Received:12/29/17 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Phenacetin ND ug/L 01/03/18 17:49 62-44-201/02/18 08:2220.0 1
Phenanthrene ND ug/L 01/03/18 17:49 85-01-801/02/18 08:2210.0 1
Phenol ND ug/L 01/03/18 17:49 108-95-201/02/18 08:2210.0 1
p-Phenylenediamine ND ug/L 01/03/18 17:49 106-50-3 L201/02/18 08:2210.0 1
Phorate ND ug/L 01/03/18 17:49 298-02-201/02/18 08:2210.0 1
Pronamide ND ug/L 01/03/18 17:49 23950-58-501/02/18 08:2210.0 1
Pyrene ND ug/L 01/03/18 17:49 129-00-001/02/18 08:2210.0 1
Safrole ND ug/L 01/03/18 17:49 94-59-701/02/18 08:2210.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 01/03/18 17:49 95-94-301/02/18 08:2210.0 1
2,3,4,6-Tetrachlorophenol ND ug/L 01/03/18 17:49 58-90-201/02/18 08:2210.0 1
Thionazin ND ug/L 01/03/18 17:49 297-97-201/02/18 08:2220.0 1
O-Toluidine ND ug/L 01/03/18 17:49 95-53-401/02/18 08:2210.0 1
2,4,5-Trichlorophenol ND ug/L 01/03/18 17:49 95-95-401/02/18 08:2210.0 1
2,4,6-Trichlorophenol ND ug/L 01/03/18 17:49 88-06-201/02/18 08:2210.0 1
1,3,5-Trinitrobenzene ND ug/L 01/03/18 17:49 99-35-4 L201/02/18 08:2210.0 1
Surrogates
Nitrobenzene-d5 (S)71 %01/03/18 17:49 4165-60-001/02/18 08:2221-110 1
2-Fluorobiphenyl (S)68 %01/03/18 17:49 321-60-801/02/18 08:2227-110 1
Terphenyl-d14 (S)44 %01/03/18 17:49 1718-51-001/02/18 08:2231-107 1
Phenol-d6 (S)18 %01/03/18 17:49 13127-88-301/02/18 08:2210-110 1
2-Fluorophenol (S)30 %01/03/18 17:49 367-12-401/02/18 08:2212-110 1
2,4,6-Tribromophenol (S)77 %01/03/18 17:49 118-79-601/02/18 08:2227-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/18 16:11 67-64-125.0 1
Acetonitrile ND ug/L 01/03/18 16:11 75-05-850.0 1
Acrolein ND ug/L 01/03/18 16:11 107-02-810.0 1
Acrylonitrile ND ug/L 01/03/18 16:11 107-13-110.0 1
Allyl chloride ND ug/L 01/03/18 16:11 107-05-12.0 1
Benzene ND ug/L 01/03/18 16:11 71-43-21.0 1
Bromochloromethane ND ug/L 01/03/18 16:11 74-97-51.0 1
Bromodichloromethane ND ug/L 01/03/18 16:11 75-27-41.0 1
Bromoform ND ug/L 01/03/18 16:11 75-25-21.0 1
Bromomethane ND ug/L 01/03/18 16:11 74-83-92.0 1
2-Butanone (MEK)ND ug/L 01/03/18 16:11 78-93-35.0 1
Carbon disulfide ND ug/L 01/03/18 16:11 75-15-02.0 1
Carbon tetrachloride ND ug/L 01/03/18 16:11 56-23-51.0 1
Chlorobenzene ND ug/L 01/03/18 16:11 108-90-71.0 1
Chloroethane ND ug/L 01/03/18 16:11 75-00-31.0 1
Chloroform ND ug/L 01/03/18 16:11 67-66-31.0 1
Chloromethane ND ug/L 01/03/18 16:11 74-87-31.0 1
Chloroprene ND ug/L 01/03/18 16:11 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/18 16:11 96-12-82.0 1
Dibromochloromethane ND ug/L 01/03/18 16:11 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/18 16:11 106-93-41.0 1
Dibromomethane ND ug/L 01/03/18 16:11 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 01/03/18 16:11 95-50-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 74 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-4R Lab ID:92368450013 Collected:12/29/17 10:20 Received:12/29/17 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,3-Dichlorobenzene ND ug/L 01/03/18 16:11 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 01/03/18 16:11 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/18 16:11 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 01/03/18 16:11 75-71-81.0 1
1,1-Dichloroethane ND ug/L 01/03/18 16:11 75-34-31.0 1
1,2-Dichloroethane ND ug/L 01/03/18 16:11 107-06-21.0 1
1,1-Dichloroethene ND ug/L 01/03/18 16:11 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 01/03/18 16:11 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 01/03/18 16:11 156-60-51.0 1
1,2-Dichloropropane ND ug/L 01/03/18 16:11 78-87-51.0 1
1,3-Dichloropropane ND ug/L 01/03/18 16:11 142-28-91.0 1
2,2-Dichloropropane ND ug/L 01/03/18 16:11 594-20-71.0 1
1,1-Dichloropropene ND ug/L 01/03/18 16:11 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 01/03/18 16:11 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 01/03/18 16:11 10061-02-61.0 1
Ethylbenzene ND ug/L 01/03/18 16:11 100-41-41.0 1
Ethyl methacrylate ND ug/L 01/03/18 16:11 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 01/03/18 16:11 87-68-31.0 1
2-Hexanone ND ug/L 01/03/18 16:11 591-78-65.0 1
Iodomethane ND ug/L 01/03/18 16:11 74-88-45.0 1
Isobutanol ND ug/L 01/03/18 16:11 78-83-11001
Methacrylonitrile ND ug/L 01/03/18 16:11 126-98-710.0 1
Methylene Chloride ND ug/L 01/03/18 16:11 75-09-21.0 1
Methyl methacrylate ND ug/L 01/03/18 16:11 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/18 16:11 108-10-15.0 1
Naphthalene ND ug/L 01/03/18 16:11 91-20-31.0 1
Propionitrile ND ug/L 01/03/18 16:11 107-12-020.0 1
Styrene ND ug/L 01/03/18 16:11 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/18 16:11 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/18 16:11 79-34-51.0 1
Tetrachloroethene ND ug/L 01/03/18 16:11 127-18-41.0 1
Tetrahydrofuran ND ug/L 01/03/18 16:11 109-99-910.0 1
Toluene ND ug/L 01/03/18 16:11 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 01/03/18 16:11 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 01/03/18 16:11 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 01/03/18 16:11 79-00-51.0 1
Trichloroethene ND ug/L 01/03/18 16:11 79-01-61.0 1
Trichlorofluoromethane ND ug/L 01/03/18 16:11 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 01/03/18 16:11 96-18-41.0 1
Vinyl acetate ND ug/L 01/03/18 16:11 108-05-42.0 1
Vinyl chloride ND ug/L 01/03/18 16:11 75-01-41.0 1
Xylene (Total)ND ug/L 01/03/18 16:11 1330-20-71.0 1
m&p-Xylene ND ug/L 01/03/18 16:11 179601-23-12.0 1
o-Xylene ND ug/L 01/03/18 16:11 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)98 %01/03/18 16:11 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %01/03/18 16:11 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 75 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-4R Lab ID:92368450013 Collected:12/29/17 10:20 Received:12/29/17 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Surrogates
Toluene-d8 (S)111 %01/03/18 16:11 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 76 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-8 Lab ID:92368450014 Collected:12/29/17 10:40 Received:12/29/17 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By STV 01/05/18 11:431
Collected Date 12/29/17 01/05/18 11:431
Collected Time 10:40 01/05/18 11:431
pH 5.7 Std. Units 01/05/18 11:430.10 1
Temperature 6.7 deg C 01/05/18 11:430.50 1
Static Water Level 18.55 feet 01/05/18 11:431
Specific Conductance 75.2 umhos/cm 01/05/18 11:431.0 1
Oxygen, Dissolved 4.5 mg/L 01/05/18 11:43 7782-44-71
Total Well Depth 27 feet 01/05/18 11:431
REDOX 169.8 mV 01/05/18 11:431
Turbidity 9.7 NTU 01/05/18 11:431.0 1
Odor NONE 01/05/18 11:431
Appearance CLEAR 01/05/18 11:431
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 01/02/18 21:51 309-00-201/02/18 07:110.050 1
alpha-BHC ND ug/L 01/02/18 21:51 319-84-601/02/18 07:110.050 1
beta-BHC ND ug/L 01/02/18 21:51 319-85-701/02/18 07:110.050 1
delta-BHC ND ug/L 01/02/18 21:51 319-86-801/02/18 07:110.050 1
gamma-BHC (Lindane)ND ug/L 01/02/18 21:51 58-89-901/02/18 07:110.050 1
Chlordane (Technical)ND ug/L 01/02/18 21:51 57-74-901/02/18 07:110.20 1
4,4'-DDD ND ug/L 01/02/18 21:51 72-54-801/02/18 07:110.050 1
4,4'-DDE ND ug/L 01/02/18 21:51 72-55-901/02/18 07:110.050 1
4,4'-DDT ND ug/L 01/02/18 21:51 50-29-301/02/18 07:110.050 1
Dieldrin ND ug/L 01/02/18 21:51 60-57-101/02/18 07:110.050 1
Endosulfan I ND ug/L 01/02/18 21:51 959-98-801/02/18 07:110.050 1
Endosulfan II ND ug/L 01/02/18 21:51 33213-65-901/02/18 07:110.050 1
Endosulfan sulfate ND ug/L 01/02/18 21:51 1031-07-801/02/18 07:110.050 1
Endrin ND ug/L 01/02/18 21:51 72-20-801/02/18 07:110.050 1
Endrin aldehyde ND ug/L 01/02/18 21:51 7421-93-401/02/18 07:110.050 1
Heptachlor ND ug/L 01/02/18 21:51 76-44-801/02/18 07:110.050 1
Heptachlor epoxide ND ug/L 01/02/18 21:51 1024-57-301/02/18 07:110.050 1
Methoxychlor ND ug/L 01/02/18 21:51 72-43-501/02/18 07:110.15 1
Toxaphene ND ug/L 01/02/18 21:51 8001-35-201/02/18 07:110.20 1
Surrogates
Tetrachloro-m-xylene (S)65 %01/02/18 21:51 877-09-801/02/18 07:1120-130 1
Decachlorobiphenyl (S)47 %01/02/18 21:51 2051-24-301/02/18 07:1120-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 01/02/18 19:44 12674-11-201/02/18 07:110.50 1
PCB-1221 (Aroclor 1221)ND ug/L 01/02/18 19:44 11104-28-201/02/18 07:110.50 1
PCB-1232 (Aroclor 1232)ND ug/L 01/02/18 19:44 11141-16-501/02/18 07:110.50 1
PCB-1242 (Aroclor 1242)ND ug/L 01/02/18 19:44 53469-21-901/02/18 07:110.50 1
PCB-1248 (Aroclor 1248)ND ug/L 01/02/18 19:44 12672-29-601/02/18 07:110.50 1
PCB-1254 (Aroclor 1254)ND ug/L 01/02/18 19:44 11097-69-101/02/18 07:110.50 1
PCB-1260 (Aroclor 1260)ND ug/L 01/02/18 19:44 11096-82-501/02/18 07:110.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 77 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-8 Lab ID:92368450014 Collected:12/29/17 10:40 Received:12/29/17 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
Surrogates
Decachlorobiphenyl (S)47 %01/02/18 19:44 2051-24-301/02/18 07:1110-132 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 01/03/18 18:19 83-32-901/02/18 08:2210.0 1
Acenaphthylene ND ug/L 01/03/18 18:19 208-96-801/02/18 08:2210.0 1
Acetophenone ND ug/L 01/03/18 18:19 98-86-201/02/18 08:2210.0 1
2-Acetylaminofluorene ND ug/L 01/03/18 18:19 53-96-3 L201/02/18 08:2220.0 1
4-Aminobiphenyl ND ug/L 01/03/18 18:19 92-67-101/02/18 08:2210.0 1
Anthracene ND ug/L 01/03/18 18:19 120-12-701/02/18 08:2210.0 1
Benzo(a)anthracene ND ug/L 01/03/18 18:19 56-55-301/02/18 08:2210.0 1
Benzo(a)pyrene ND ug/L 01/03/18 18:19 50-32-801/02/18 08:2210.0 1
Benzo(b)fluoranthene ND ug/L 01/03/18 18:19 205-99-201/02/18 08:2210.0 1
Benzo(g,h,i)perylene ND ug/L 01/03/18 18:19 191-24-201/02/18 08:2210.0 1
Benzo(k)fluoranthene ND ug/L 01/03/18 18:19 207-08-901/02/18 08:2210.0 1
Benzyl alcohol ND ug/L 01/03/18 18:19 100-51-601/02/18 08:2220.0 1
4-Bromophenylphenyl ether ND ug/L 01/03/18 18:19 101-55-301/02/18 08:2210.0 1
Butylbenzylphthalate ND ug/L 01/03/18 18:19 85-68-701/02/18 08:2210.0 1
4-Chloro-3-methylphenol ND ug/L 01/03/18 18:19 59-50-701/02/18 08:2220.0 1
4-Chloroaniline ND ug/L 01/03/18 18:19 106-47-801/02/18 08:2220.0 1
Chlorobenzilate ND ug/L 01/03/18 18:19 510-15-601/02/18 08:2210.0 1
bis(2-Chloroethoxy)methane ND ug/L 01/03/18 18:19 111-91-101/02/18 08:2210.0 1
bis(2-Chloroethyl) ether ND ug/L 01/03/18 18:19 111-44-401/02/18 08:2210.0 1
2-Chloronaphthalene ND ug/L 01/03/18 18:19 91-58-701/02/18 08:2210.0 1
2-Chlorophenol ND ug/L 01/03/18 18:19 95-57-801/02/18 08:2210.0 1
4-Chlorophenylphenyl ether ND ug/L 01/03/18 18:19 7005-72-301/02/18 08:2210.0 1
Chrysene ND ug/L 01/03/18 18:19 218-01-901/02/18 08:2210.0 1
Diallate ND ug/L 01/03/18 18:19 2303-16-401/02/18 08:2210.0 1
Dibenz(a,h)anthracene ND ug/L 01/03/18 18:19 53-70-301/02/18 08:2210.0 1
Dibenzofuran ND ug/L 01/03/18 18:19 132-64-901/02/18 08:2210.0 1
3,3'-Dichlorobenzidine ND ug/L 01/03/18 18:19 91-94-101/02/18 08:2220.0 1
2,4-Dichlorophenol ND ug/L 01/03/18 18:19 120-83-201/02/18 08:2210.0 1
2,6-Dichlorophenol ND ug/L 01/03/18 18:19 87-65-001/02/18 08:2210.0 1
Diethylphthalate ND ug/L 01/03/18 18:19 84-66-201/02/18 08:2210.0 1
Dimethoate ND ug/L 01/03/18 18:19 60-51-501/02/18 08:2210.0 1
P-Dimethylaminoazobenzene ND ug/L 01/03/18 18:19 60-11-701/02/18 08:225.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 01/03/18 18:19 57-97-601/02/18 08:2210.0 1
3,3'-Dimethylbenzidine ND ug/L 01/03/18 18:19 119-93-701/02/18 08:2210.0 1
2,4-Dimethylphenol ND ug/L 01/03/18 18:19 105-67-901/02/18 08:2210.0 1
Dimethylphthalate ND ug/L 01/03/18 18:19 131-11-301/02/18 08:2210.0 1
Di-n-butylphthalate ND ug/L 01/03/18 18:19 84-74-201/02/18 08:2210.0 1
4,6-Dinitro-2-methylphenol ND ug/L 01/03/18 18:19 534-52-101/02/18 08:2220.0 1
1,3-Dinitrobenzene ND ug/L 01/03/18 18:19 99-65-001/02/18 08:2220.0 1
2,4-Dinitrophenol ND ug/L 01/03/18 18:19 51-28-501/02/18 08:2250.0 1
2,4-Dinitrotoluene ND ug/L 01/03/18 18:19 121-14-201/02/18 08:2210.0 1
2,6-Dinitrotoluene ND ug/L 01/03/18 18:19 606-20-201/02/18 08:2210.0 1
Di-n-octylphthalate ND ug/L 01/03/18 18:19 117-84-001/02/18 08:2210.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 78 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-8 Lab ID:92368450014 Collected:12/29/17 10:40 Received:12/29/17 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Diphenylamine ND ug/L 01/03/18 18:19 122-39-401/02/18 08:2210.0 1
Disulfoton ND ug/L 01/03/18 18:19 298-04-401/02/18 08:2210.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 01/03/18 18:19 117-81-701/02/18 08:226.0 1
Ethyl methanesulfonate ND ug/L 01/03/18 18:19 62-50-001/02/18 08:2220.0 1
Famphur ND ug/L 01/03/18 18:19 52-85-701/02/18 08:2210.0 1
Fluoranthene ND ug/L 01/03/18 18:19 206-44-001/02/18 08:2210.0 1
Fluorene ND ug/L 01/03/18 18:19 86-73-701/02/18 08:2210.0 1
Hexachlorobenzene ND ug/L 01/03/18 18:19 118-74-101/02/18 08:2210.0 1
Hexachlorocyclopentadiene ND ug/L 01/03/18 18:19 77-47-401/02/18 08:2210.0 1
Hexachloroethane ND ug/L 01/03/18 18:19 67-72-101/02/18 08:2210.0 1
Hexachlorophene ND ug/L 01/03/18 18:19 70-30-401/02/18 08:221001
Indeno(1,2,3-cd)pyrene ND ug/L 01/03/18 18:19 193-39-501/02/18 08:2210.0 1
Isodrin ND ug/L 01/03/18 18:19 465-73-601/02/18 08:2220.0 1
Isophorone ND ug/L 01/03/18 18:19 78-59-101/02/18 08:2210.0 1
Isosafrole ND ug/L 01/03/18 18:19 120-58-101/02/18 08:2210.0 1
Kepone ND ug/L 01/03/18 18:19 143-50-001/02/18 08:2210.0 1
Methapyrilene ND ug/L 01/03/18 18:19 91-80-501/02/18 08:2250.0 1
3-Methylcholanthrene ND ug/L 01/03/18 18:19 56-49-501/02/18 08:2210.0 1
Methyl methanesulfonate ND ug/L 01/03/18 18:19 66-27-3 L101/02/18 08:225.0 1
2-Methylnaphthalene ND ug/L 01/03/18 18:19 91-57-601/02/18 08:2210.0 1
Methyl parathion ND ug/L 01/03/18 18:19 298-00-001/02/18 08:2210.0 1
2-Methylphenol(o-Cresol)ND ug/L 01/03/18 18:19 95-48-701/02/18 08:2210.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 01/03/18 18:19 15831-10-401/02/18 08:2210.0 1
1-Naphthalenamine ND ug/L 01/03/18 18:19 134-32-701/02/18 08:225.0 1
2-Naphthalenamine ND ug/L 01/03/18 18:19 91-59-801/02/18 08:225.0 1
1,4-Naphthoquinone ND ug/L 01/03/18 18:19 130-15-401/02/18 08:225.0 1
2-Nitroaniline ND ug/L 01/03/18 18:19 88-74-401/02/18 08:2250.0 1
3-Nitroaniline ND ug/L 01/03/18 18:19 99-09-201/02/18 08:2250.0 1
4-Nitroaniline ND ug/L 01/03/18 18:19 100-01-601/02/18 08:2220.0 1
Nitrobenzene ND ug/L 01/03/18 18:19 98-95-301/02/18 08:2210.0 1
2-Nitrophenol ND ug/L 01/03/18 18:19 88-75-501/02/18 08:2210.0 1
4-Nitrophenol ND ug/L 01/03/18 18:19 100-02-701/02/18 08:2250.0 1
5-Nitro-o-toluidine ND ug/L 01/03/18 18:19 99-55-8 L201/02/18 08:2210.0 1
N-Nitrosodiethylamine ND ug/L 01/03/18 18:19 55-18-501/02/18 08:2220.0 1
N-Nitrosodimethylamine ND ug/L 01/03/18 18:19 62-75-901/02/18 08:2210.0 1
N-Nitroso-di-n-butylamine ND ug/L 01/03/18 18:19 924-16-301/02/18 08:2210.0 1
N-Nitroso-di-n-propylamine ND ug/L 01/03/18 18:19 621-64-701/02/18 08:2210.0 1
N-Nitrosodiphenylamine ND ug/L 01/03/18 18:19 86-30-601/02/18 08:2210.0 1
N-Nitrosomethylethylamine ND ug/L 01/03/18 18:19 10595-95-601/02/18 08:2210.0 1
N-Nitrosopiperidine ND ug/L 01/03/18 18:19 100-75-401/02/18 08:2220.0 1
N-Nitrosopyrrolidine ND ug/L 01/03/18 18:19 930-55-201/02/18 08:2210.0 1
O,O,O-Triethylphosphorothioate ND ug/L 01/03/18 18:19 126-68-101/02/18 08:2210.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 01/03/18 18:19 108-60-101/02/18 08:2210.0 1
Parathion (Ethyl parathion)ND ug/L 01/03/18 18:19 56-38-201/02/18 08:2210.0 1
Pentachlorobenzene ND ug/L 01/03/18 18:19 608-93-501/02/18 08:2210.0 1
Pentachloronitrobenzene ND ug/L 01/03/18 18:19 82-68-801/02/18 08:2220.0 1
Pentachlorophenol ND ug/L 01/03/18 18:19 87-86-501/02/18 08:2225.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 79 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-8 Lab ID:92368450014 Collected:12/29/17 10:40 Received:12/29/17 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Phenacetin ND ug/L 01/03/18 18:19 62-44-201/02/18 08:2220.0 1
Phenanthrene ND ug/L 01/03/18 18:19 85-01-801/02/18 08:2210.0 1
Phenol ND ug/L 01/03/18 18:19 108-95-201/02/18 08:2210.0 1
p-Phenylenediamine ND ug/L 01/03/18 18:19 106-50-3 L201/02/18 08:2210.0 1
Phorate ND ug/L 01/03/18 18:19 298-02-201/02/18 08:2210.0 1
Pronamide ND ug/L 01/03/18 18:19 23950-58-501/02/18 08:2210.0 1
Pyrene ND ug/L 01/03/18 18:19 129-00-001/02/18 08:2210.0 1
Safrole ND ug/L 01/03/18 18:19 94-59-701/02/18 08:2210.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 01/03/18 18:19 95-94-301/02/18 08:2210.0 1
2,3,4,6-Tetrachlorophenol ND ug/L 01/03/18 18:19 58-90-201/02/18 08:2210.0 1
Thionazin ND ug/L 01/03/18 18:19 297-97-201/02/18 08:2220.0 1
O-Toluidine ND ug/L 01/03/18 18:19 95-53-401/02/18 08:2210.0 1
2,4,5-Trichlorophenol ND ug/L 01/03/18 18:19 95-95-401/02/18 08:2210.0 1
2,4,6-Trichlorophenol ND ug/L 01/03/18 18:19 88-06-201/02/18 08:2210.0 1
1,3,5-Trinitrobenzene ND ug/L 01/03/18 18:19 99-35-4 L201/02/18 08:2210.0 1
Surrogates
Nitrobenzene-d5 (S)37 %01/03/18 18:19 4165-60-001/02/18 08:2221-110 1
2-Fluorobiphenyl (S)35 %01/03/18 18:19 321-60-801/02/18 08:2227-110 1
Terphenyl-d14 (S)46 %01/03/18 18:19 1718-51-001/02/18 08:2231-107 1
Phenol-d6 (S)13 %01/03/18 18:19 13127-88-301/02/18 08:2210-110 1
2-Fluorophenol (S)19 %01/03/18 18:19 367-12-401/02/18 08:2212-110 1
2,4,6-Tribromophenol (S)42 %01/03/18 18:19 118-79-601/02/18 08:2227-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/18 16:28 67-64-125.0 1
Acetonitrile ND ug/L 01/03/18 16:28 75-05-850.0 1
Acrolein ND ug/L 01/03/18 16:28 107-02-810.0 1
Acrylonitrile ND ug/L 01/03/18 16:28 107-13-110.0 1
Allyl chloride ND ug/L 01/03/18 16:28 107-05-12.0 1
Benzene ND ug/L 01/03/18 16:28 71-43-21.0 1
Bromochloromethane ND ug/L 01/03/18 16:28 74-97-51.0 1
Bromodichloromethane ND ug/L 01/03/18 16:28 75-27-41.0 1
Bromoform ND ug/L 01/03/18 16:28 75-25-21.0 1
Bromomethane ND ug/L 01/03/18 16:28 74-83-92.0 1
2-Butanone (MEK)ND ug/L 01/03/18 16:28 78-93-35.0 1
Carbon disulfide ND ug/L 01/03/18 16:28 75-15-02.0 1
Carbon tetrachloride ND ug/L 01/03/18 16:28 56-23-51.0 1
Chlorobenzene ND ug/L 01/03/18 16:28 108-90-71.0 1
Chloroethane ND ug/L 01/03/18 16:28 75-00-31.0 1
Chloroform ND ug/L 01/03/18 16:28 67-66-31.0 1
Chloromethane ND ug/L 01/03/18 16:28 74-87-31.0 1
Chloroprene ND ug/L 01/03/18 16:28 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/18 16:28 96-12-82.0 1
Dibromochloromethane ND ug/L 01/03/18 16:28 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/18 16:28 106-93-41.0 1
Dibromomethane ND ug/L 01/03/18 16:28 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 01/03/18 16:28 95-50-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 80 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-8 Lab ID:92368450014 Collected:12/29/17 10:40 Received:12/29/17 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,3-Dichlorobenzene ND ug/L 01/03/18 16:28 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 01/03/18 16:28 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/18 16:28 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 01/03/18 16:28 75-71-81.0 1
1,1-Dichloroethane ND ug/L 01/03/18 16:28 75-34-31.0 1
1,2-Dichloroethane ND ug/L 01/03/18 16:28 107-06-21.0 1
1,1-Dichloroethene ND ug/L 01/03/18 16:28 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 01/03/18 16:28 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 01/03/18 16:28 156-60-51.0 1
1,2-Dichloropropane ND ug/L 01/03/18 16:28 78-87-51.0 1
1,3-Dichloropropane ND ug/L 01/03/18 16:28 142-28-91.0 1
2,2-Dichloropropane ND ug/L 01/03/18 16:28 594-20-71.0 1
1,1-Dichloropropene ND ug/L 01/03/18 16:28 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 01/03/18 16:28 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 01/03/18 16:28 10061-02-61.0 1
Ethylbenzene ND ug/L 01/03/18 16:28 100-41-41.0 1
Ethyl methacrylate ND ug/L 01/03/18 16:28 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 01/03/18 16:28 87-68-31.0 1
2-Hexanone ND ug/L 01/03/18 16:28 591-78-65.0 1
Iodomethane ND ug/L 01/03/18 16:28 74-88-45.0 1
Isobutanol ND ug/L 01/03/18 16:28 78-83-11001
Methacrylonitrile ND ug/L 01/03/18 16:28 126-98-710.0 1
Methylene Chloride ND ug/L 01/03/18 16:28 75-09-21.0 1
Methyl methacrylate ND ug/L 01/03/18 16:28 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/18 16:28 108-10-15.0 1
Naphthalene ND ug/L 01/03/18 16:28 91-20-31.0 1
Propionitrile ND ug/L 01/03/18 16:28 107-12-020.0 1
Styrene ND ug/L 01/03/18 16:28 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/18 16:28 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/18 16:28 79-34-51.0 1
Tetrachloroethene ND ug/L 01/03/18 16:28 127-18-41.0 1
Tetrahydrofuran ND ug/L 01/03/18 16:28 109-99-910.0 1
Toluene ND ug/L 01/03/18 16:28 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 01/03/18 16:28 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 01/03/18 16:28 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 01/03/18 16:28 79-00-51.0 1
Trichloroethene ND ug/L 01/03/18 16:28 79-01-61.0 1
Trichlorofluoromethane ND ug/L 01/03/18 16:28 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 01/03/18 16:28 96-18-41.0 1
Vinyl acetate ND ug/L 01/03/18 16:28 108-05-42.0 1
Vinyl chloride ND ug/L 01/03/18 16:28 75-01-41.0 1
Xylene (Total)ND ug/L 01/03/18 16:28 1330-20-71.0 1
m&p-Xylene ND ug/L 01/03/18 16:28 179601-23-12.0 1
o-Xylene ND ug/L 01/03/18 16:28 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)102 %01/03/18 16:28 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %01/03/18 16:28 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 81 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-8 Lab ID:92368450014 Collected:12/29/17 10:40 Received:12/29/17 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Surrogates
Toluene-d8 (S)111 %01/03/18 16:28 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 82 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-11 Lab ID:92368450015 Collected:12/29/17 11:55 Received:12/29/17 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By JSH 01/05/18 11:471
Collected Date 12/29/17 01/05/18 11:471
Collected Time 11:55 01/05/18 11:471
pH 6.1 Std. Units 01/05/18 11:470.10 1
Temperature 12.5 deg C 01/05/18 11:470.50 1
Static Water Level 4.14 feet 01/05/18 11:471
Specific Conductance 329.2 umhos/cm 01/05/18 11:471.0 1
Oxygen, Dissolved 0.1 mg/L 01/05/18 11:47 7782-44-71
Total Well Depth 20.0 feet 01/05/18 11:471
REDOX -43.9 mV 01/05/18 11:471
Turbidity 9.8 NTU 01/05/18 11:471.0 1
Odor SULFUR 01/05/18 11:471
Appearance CLEAR 01/05/18 11:471
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 01/02/18 22:09 309-00-201/02/18 07:110.050 1
alpha-BHC ND ug/L 01/02/18 22:09 319-84-601/02/18 07:110.050 1
beta-BHC ND ug/L 01/02/18 22:09 319-85-701/02/18 07:110.050 1
delta-BHC ND ug/L 01/02/18 22:09 319-86-801/02/18 07:110.050 1
gamma-BHC (Lindane)ND ug/L 01/02/18 22:09 58-89-901/02/18 07:110.050 1
Chlordane (Technical)ND ug/L 01/02/18 22:09 57-74-901/02/18 07:110.20 1
4,4'-DDD ND ug/L 01/02/18 22:09 72-54-801/02/18 07:110.050 1
4,4'-DDE ND ug/L 01/02/18 22:09 72-55-901/02/18 07:110.050 1
4,4'-DDT ND ug/L 01/02/18 22:09 50-29-301/02/18 07:110.050 1
Dieldrin ND ug/L 01/02/18 22:09 60-57-101/02/18 07:110.050 1
Endosulfan I ND ug/L 01/02/18 22:09 959-98-801/02/18 07:110.050 1
Endosulfan II ND ug/L 01/02/18 22:09 33213-65-901/02/18 07:110.050 1
Endosulfan sulfate ND ug/L 01/02/18 22:09 1031-07-801/02/18 07:110.050 1
Endrin ND ug/L 01/02/18 22:09 72-20-801/02/18 07:110.050 1
Endrin aldehyde ND ug/L 01/02/18 22:09 7421-93-401/02/18 07:110.050 1
Heptachlor ND ug/L 01/02/18 22:09 76-44-801/02/18 07:110.050 1
Heptachlor epoxide ND ug/L 01/02/18 22:09 1024-57-301/02/18 07:110.050 1
Methoxychlor ND ug/L 01/02/18 22:09 72-43-501/02/18 07:110.15 1
Toxaphene ND ug/L 01/02/18 22:09 8001-35-201/02/18 07:110.20 1
Surrogates
Tetrachloro-m-xylene (S)60 %01/02/18 22:09 877-09-801/02/18 07:1120-130 1
Decachlorobiphenyl (S)61 %01/02/18 22:09 2051-24-301/02/18 07:1120-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 01/02/18 20:05 12674-11-201/02/18 07:110.50 1
PCB-1221 (Aroclor 1221)ND ug/L 01/02/18 20:05 11104-28-201/02/18 07:110.50 1
PCB-1232 (Aroclor 1232)ND ug/L 01/02/18 20:05 11141-16-501/02/18 07:110.50 1
PCB-1242 (Aroclor 1242)ND ug/L 01/02/18 20:05 53469-21-901/02/18 07:110.50 1
PCB-1248 (Aroclor 1248)ND ug/L 01/02/18 20:05 12672-29-601/02/18 07:110.50 1
PCB-1254 (Aroclor 1254)ND ug/L 01/02/18 20:05 11097-69-101/02/18 07:110.50 1
PCB-1260 (Aroclor 1260)ND ug/L 01/02/18 20:05 11096-82-501/02/18 07:110.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 83 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-11 Lab ID:92368450015 Collected:12/29/17 11:55 Received:12/29/17 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
Surrogates
Decachlorobiphenyl (S)60 %01/02/18 20:05 2051-24-301/02/18 07:1110-132 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 01/03/18 18:48 83-32-901/02/18 08:2210.0 1
Acenaphthylene ND ug/L 01/03/18 18:48 208-96-801/02/18 08:2210.0 1
Acetophenone ND ug/L 01/03/18 18:48 98-86-201/02/18 08:2210.0 1
2-Acetylaminofluorene ND ug/L 01/03/18 18:48 53-96-3 L201/02/18 08:2220.0 1
4-Aminobiphenyl ND ug/L 01/03/18 18:48 92-67-101/02/18 08:2210.0 1
Anthracene ND ug/L 01/03/18 18:48 120-12-701/02/18 08:2210.0 1
Benzo(a)anthracene ND ug/L 01/03/18 18:48 56-55-301/02/18 08:2210.0 1
Benzo(a)pyrene ND ug/L 01/03/18 18:48 50-32-801/02/18 08:2210.0 1
Benzo(b)fluoranthene ND ug/L 01/03/18 18:48 205-99-201/02/18 08:2210.0 1
Benzo(g,h,i)perylene ND ug/L 01/03/18 18:48 191-24-201/02/18 08:2210.0 1
Benzo(k)fluoranthene ND ug/L 01/03/18 18:48 207-08-901/02/18 08:2210.0 1
Benzyl alcohol ND ug/L 01/03/18 18:48 100-51-601/02/18 08:2220.0 1
4-Bromophenylphenyl ether ND ug/L 01/03/18 18:48 101-55-301/02/18 08:2210.0 1
Butylbenzylphthalate ND ug/L 01/03/18 18:48 85-68-701/02/18 08:2210.0 1
4-Chloro-3-methylphenol ND ug/L 01/03/18 18:48 59-50-701/02/18 08:2220.0 1
4-Chloroaniline ND ug/L 01/03/18 18:48 106-47-801/02/18 08:2220.0 1
Chlorobenzilate ND ug/L 01/03/18 18:48 510-15-601/02/18 08:2210.0 1
bis(2-Chloroethoxy)methane ND ug/L 01/03/18 18:48 111-91-101/02/18 08:2210.0 1
bis(2-Chloroethyl) ether ND ug/L 01/03/18 18:48 111-44-401/02/18 08:2210.0 1
2-Chloronaphthalene ND ug/L 01/03/18 18:48 91-58-701/02/18 08:2210.0 1
2-Chlorophenol ND ug/L 01/03/18 18:48 95-57-801/02/18 08:2210.0 1
4-Chlorophenylphenyl ether ND ug/L 01/03/18 18:48 7005-72-301/02/18 08:2210.0 1
Chrysene ND ug/L 01/03/18 18:48 218-01-901/02/18 08:2210.0 1
Diallate ND ug/L 01/03/18 18:48 2303-16-401/02/18 08:2210.0 1
Dibenz(a,h)anthracene ND ug/L 01/03/18 18:48 53-70-301/02/18 08:2210.0 1
Dibenzofuran ND ug/L 01/03/18 18:48 132-64-901/02/18 08:2210.0 1
3,3'-Dichlorobenzidine ND ug/L 01/03/18 18:48 91-94-101/02/18 08:2220.0 1
2,4-Dichlorophenol ND ug/L 01/03/18 18:48 120-83-201/02/18 08:2210.0 1
2,6-Dichlorophenol ND ug/L 01/03/18 18:48 87-65-001/02/18 08:2210.0 1
Diethylphthalate ND ug/L 01/03/18 18:48 84-66-201/02/18 08:2210.0 1
Dimethoate ND ug/L 01/03/18 18:48 60-51-501/02/18 08:2210.0 1
P-Dimethylaminoazobenzene ND ug/L 01/03/18 18:48 60-11-701/02/18 08:225.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 01/03/18 18:48 57-97-601/02/18 08:2210.0 1
3,3'-Dimethylbenzidine ND ug/L 01/03/18 18:48 119-93-701/02/18 08:2210.0 1
2,4-Dimethylphenol ND ug/L 01/03/18 18:48 105-67-901/02/18 08:2210.0 1
Dimethylphthalate ND ug/L 01/03/18 18:48 131-11-301/02/18 08:2210.0 1
Di-n-butylphthalate ND ug/L 01/03/18 18:48 84-74-201/02/18 08:2210.0 1
4,6-Dinitro-2-methylphenol ND ug/L 01/03/18 18:48 534-52-101/02/18 08:2220.0 1
1,3-Dinitrobenzene ND ug/L 01/03/18 18:48 99-65-001/02/18 08:2220.0 1
2,4-Dinitrophenol ND ug/L 01/03/18 18:48 51-28-501/02/18 08:2250.0 1
2,4-Dinitrotoluene ND ug/L 01/03/18 18:48 121-14-201/02/18 08:2210.0 1
2,6-Dinitrotoluene ND ug/L 01/03/18 18:48 606-20-201/02/18 08:2210.0 1
Di-n-octylphthalate ND ug/L 01/03/18 18:48 117-84-001/02/18 08:2210.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 84 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-11 Lab ID:92368450015 Collected:12/29/17 11:55 Received:12/29/17 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Diphenylamine ND ug/L 01/03/18 18:48 122-39-401/02/18 08:2210.0 1
Disulfoton ND ug/L 01/03/18 18:48 298-04-401/02/18 08:2210.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 01/03/18 18:48 117-81-701/02/18 08:226.0 1
Ethyl methanesulfonate ND ug/L 01/03/18 18:48 62-50-001/02/18 08:2220.0 1
Famphur ND ug/L 01/03/18 18:48 52-85-701/02/18 08:2210.0 1
Fluoranthene ND ug/L 01/03/18 18:48 206-44-001/02/18 08:2210.0 1
Fluorene ND ug/L 01/03/18 18:48 86-73-701/02/18 08:2210.0 1
Hexachlorobenzene ND ug/L 01/03/18 18:48 118-74-101/02/18 08:2210.0 1
Hexachlorocyclopentadiene ND ug/L 01/03/18 18:48 77-47-401/02/18 08:2210.0 1
Hexachloroethane ND ug/L 01/03/18 18:48 67-72-101/02/18 08:2210.0 1
Hexachlorophene ND ug/L 01/03/18 18:48 70-30-401/02/18 08:221001
Indeno(1,2,3-cd)pyrene ND ug/L 01/03/18 18:48 193-39-501/02/18 08:2210.0 1
Isodrin ND ug/L 01/03/18 18:48 465-73-601/02/18 08:2220.0 1
Isophorone ND ug/L 01/03/18 18:48 78-59-101/02/18 08:2210.0 1
Isosafrole ND ug/L 01/03/18 18:48 120-58-101/02/18 08:2210.0 1
Kepone ND ug/L 01/03/18 18:48 143-50-001/02/18 08:2210.0 1
Methapyrilene ND ug/L 01/03/18 18:48 91-80-501/02/18 08:2250.0 1
3-Methylcholanthrene ND ug/L 01/03/18 18:48 56-49-501/02/18 08:2210.0 1
Methyl methanesulfonate ND ug/L 01/03/18 18:48 66-27-3 L101/02/18 08:225.0 1
2-Methylnaphthalene ND ug/L 01/03/18 18:48 91-57-601/02/18 08:2210.0 1
Methyl parathion ND ug/L 01/03/18 18:48 298-00-001/02/18 08:2210.0 1
2-Methylphenol(o-Cresol)ND ug/L 01/03/18 18:48 95-48-701/02/18 08:2210.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 01/03/18 18:48 15831-10-401/02/18 08:2210.0 1
1-Naphthalenamine ND ug/L 01/03/18 18:48 134-32-701/02/18 08:225.0 1
2-Naphthalenamine ND ug/L 01/03/18 18:48 91-59-801/02/18 08:225.0 1
1,4-Naphthoquinone ND ug/L 01/03/18 18:48 130-15-401/02/18 08:225.0 1
2-Nitroaniline ND ug/L 01/03/18 18:48 88-74-401/02/18 08:2250.0 1
3-Nitroaniline ND ug/L 01/03/18 18:48 99-09-201/02/18 08:2250.0 1
4-Nitroaniline ND ug/L 01/03/18 18:48 100-01-601/02/18 08:2220.0 1
Nitrobenzene ND ug/L 01/03/18 18:48 98-95-301/02/18 08:2210.0 1
2-Nitrophenol ND ug/L 01/03/18 18:48 88-75-501/02/18 08:2210.0 1
4-Nitrophenol ND ug/L 01/03/18 18:48 100-02-701/02/18 08:2250.0 1
5-Nitro-o-toluidine ND ug/L 01/03/18 18:48 99-55-8 L201/02/18 08:2210.0 1
N-Nitrosodiethylamine ND ug/L 01/03/18 18:48 55-18-501/02/18 08:2220.0 1
N-Nitrosodimethylamine ND ug/L 01/03/18 18:48 62-75-901/02/18 08:2210.0 1
N-Nitroso-di-n-butylamine ND ug/L 01/03/18 18:48 924-16-301/02/18 08:2210.0 1
N-Nitroso-di-n-propylamine ND ug/L 01/03/18 18:48 621-64-701/02/18 08:2210.0 1
N-Nitrosodiphenylamine ND ug/L 01/03/18 18:48 86-30-601/02/18 08:2210.0 1
N-Nitrosomethylethylamine ND ug/L 01/03/18 18:48 10595-95-601/02/18 08:2210.0 1
N-Nitrosopiperidine ND ug/L 01/03/18 18:48 100-75-401/02/18 08:2220.0 1
N-Nitrosopyrrolidine ND ug/L 01/03/18 18:48 930-55-201/02/18 08:2210.0 1
O,O,O-Triethylphosphorothioate ND ug/L 01/03/18 18:48 126-68-101/02/18 08:2210.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 01/03/18 18:48 108-60-101/02/18 08:2210.0 1
Parathion (Ethyl parathion)ND ug/L 01/03/18 18:48 56-38-201/02/18 08:2210.0 1
Pentachlorobenzene ND ug/L 01/03/18 18:48 608-93-501/02/18 08:2210.0 1
Pentachloronitrobenzene ND ug/L 01/03/18 18:48 82-68-801/02/18 08:2220.0 1
Pentachlorophenol ND ug/L 01/03/18 18:48 87-86-501/02/18 08:2225.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 85 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-11 Lab ID:92368450015 Collected:12/29/17 11:55 Received:12/29/17 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Phenacetin ND ug/L 01/03/18 18:48 62-44-201/02/18 08:2220.0 1
Phenanthrene ND ug/L 01/03/18 18:48 85-01-801/02/18 08:2210.0 1
Phenol ND ug/L 01/03/18 18:48 108-95-201/02/18 08:2210.0 1
p-Phenylenediamine ND ug/L 01/03/18 18:48 106-50-3 L201/02/18 08:2210.0 1
Phorate ND ug/L 01/03/18 18:48 298-02-201/02/18 08:2210.0 1
Pronamide ND ug/L 01/03/18 18:48 23950-58-501/02/18 08:2210.0 1
Pyrene ND ug/L 01/03/18 18:48 129-00-001/02/18 08:2210.0 1
Safrole ND ug/L 01/03/18 18:48 94-59-701/02/18 08:2210.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 01/03/18 18:48 95-94-301/02/18 08:2210.0 1
2,3,4,6-Tetrachlorophenol ND ug/L 01/03/18 18:48 58-90-201/02/18 08:2210.0 1
Thionazin ND ug/L 01/03/18 18:48 297-97-201/02/18 08:2220.0 1
O-Toluidine ND ug/L 01/03/18 18:48 95-53-401/02/18 08:2210.0 1
2,4,5-Trichlorophenol ND ug/L 01/03/18 18:48 95-95-401/02/18 08:2210.0 1
2,4,6-Trichlorophenol ND ug/L 01/03/18 18:48 88-06-201/02/18 08:2210.0 1
1,3,5-Trinitrobenzene ND ug/L 01/03/18 18:48 99-35-4 L201/02/18 08:2210.0 1
Surrogates
Nitrobenzene-d5 (S)73 %01/03/18 18:48 4165-60-001/02/18 08:2221-110 1
2-Fluorobiphenyl (S)69 %01/03/18 18:48 321-60-801/02/18 08:2227-110 1
Terphenyl-d14 (S)67 %01/03/18 18:48 1718-51-001/02/18 08:2231-107 1
Phenol-d6 (S)18 %01/03/18 18:48 13127-88-301/02/18 08:2210-110 1
2-Fluorophenol (S)30 %01/03/18 18:48 367-12-401/02/18 08:2212-110 1
2,4,6-Tribromophenol (S)77 %01/03/18 18:48 118-79-601/02/18 08:2227-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/18 16:45 67-64-125.0 1
Acetonitrile ND ug/L 01/03/18 16:45 75-05-850.0 1
Acrolein ND ug/L 01/03/18 16:45 107-02-810.0 1
Acrylonitrile ND ug/L 01/03/18 16:45 107-13-110.0 1
Allyl chloride ND ug/L 01/03/18 16:45 107-05-12.0 1
Benzene ND ug/L 01/03/18 16:45 71-43-21.0 1
Bromochloromethane ND ug/L 01/03/18 16:45 74-97-51.0 1
Bromodichloromethane ND ug/L 01/03/18 16:45 75-27-41.0 1
Bromoform ND ug/L 01/03/18 16:45 75-25-21.0 1
Bromomethane ND ug/L 01/03/18 16:45 74-83-92.0 1
2-Butanone (MEK)ND ug/L 01/03/18 16:45 78-93-35.0 1
Carbon disulfide ND ug/L 01/03/18 16:45 75-15-02.0 1
Carbon tetrachloride ND ug/L 01/03/18 16:45 56-23-51.0 1
Chlorobenzene ND ug/L 01/03/18 16:45 108-90-71.0 1
Chloroethane ND ug/L 01/03/18 16:45 75-00-31.0 1
Chloroform ND ug/L 01/03/18 16:45 67-66-31.0 1
Chloromethane ND ug/L 01/03/18 16:45 74-87-31.0 1
Chloroprene ND ug/L 01/03/18 16:45 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/18 16:45 96-12-82.0 1
Dibromochloromethane ND ug/L 01/03/18 16:45 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/18 16:45 106-93-41.0 1
Dibromomethane ND ug/L 01/03/18 16:45 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 01/03/18 16:45 95-50-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 86 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-11 Lab ID:92368450015 Collected:12/29/17 11:55 Received:12/29/17 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,3-Dichlorobenzene ND ug/L 01/03/18 16:45 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 01/03/18 16:45 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/18 16:45 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 01/03/18 16:45 75-71-81.0 1
1,1-Dichloroethane ND ug/L 01/03/18 16:45 75-34-31.0 1
1,2-Dichloroethane ND ug/L 01/03/18 16:45 107-06-21.0 1
1,1-Dichloroethene ND ug/L 01/03/18 16:45 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 01/03/18 16:45 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 01/03/18 16:45 156-60-51.0 1
1,2-Dichloropropane ND ug/L 01/03/18 16:45 78-87-51.0 1
1,3-Dichloropropane ND ug/L 01/03/18 16:45 142-28-91.0 1
2,2-Dichloropropane ND ug/L 01/03/18 16:45 594-20-71.0 1
1,1-Dichloropropene ND ug/L 01/03/18 16:45 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 01/03/18 16:45 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 01/03/18 16:45 10061-02-61.0 1
Ethylbenzene ND ug/L 01/03/18 16:45 100-41-41.0 1
Ethyl methacrylate ND ug/L 01/03/18 16:45 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 01/03/18 16:45 87-68-31.0 1
2-Hexanone ND ug/L 01/03/18 16:45 591-78-65.0 1
Iodomethane ND ug/L 01/03/18 16:45 74-88-45.0 1
Isobutanol ND ug/L 01/03/18 16:45 78-83-11001
Methacrylonitrile ND ug/L 01/03/18 16:45 126-98-710.0 1
Methylene Chloride ND ug/L 01/03/18 16:45 75-09-21.0 1
Methyl methacrylate ND ug/L 01/03/18 16:45 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/18 16:45 108-10-15.0 1
Naphthalene ND ug/L 01/03/18 16:45 91-20-31.0 1
Propionitrile ND ug/L 01/03/18 16:45 107-12-020.0 1
Styrene ND ug/L 01/03/18 16:45 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/18 16:45 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/18 16:45 79-34-51.0 1
Tetrachloroethene ND ug/L 01/03/18 16:45 127-18-41.0 1
Tetrahydrofuran ND ug/L 01/03/18 16:45 109-99-910.0 1
Toluene ND ug/L 01/03/18 16:45 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 01/03/18 16:45 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 01/03/18 16:45 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 01/03/18 16:45 79-00-51.0 1
Trichloroethene ND ug/L 01/03/18 16:45 79-01-61.0 1
Trichlorofluoromethane ND ug/L 01/03/18 16:45 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 01/03/18 16:45 96-18-41.0 1
Vinyl acetate ND ug/L 01/03/18 16:45 108-05-42.0 1
Vinyl chloride ND ug/L 01/03/18 16:45 75-01-41.0 1
Xylene (Total)ND ug/L 01/03/18 16:45 1330-20-71.0 1
m&p-Xylene ND ug/L 01/03/18 16:45 179601-23-12.0 1
o-Xylene ND ug/L 01/03/18 16:45 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)100 %01/03/18 16:45 460-00-470-130 1
1,2-Dichloroethane-d4 (S)90 %01/03/18 16:45 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 87 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-11 Lab ID:92368450015 Collected:12/29/17 11:55 Received:12/29/17 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Surrogates
Toluene-d8 (S)111 %01/03/18 16:45 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 88 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-12 Lab ID:92368450016 Collected:12/29/17 12:55 Received:12/29/17 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By STV 01/05/18 11:491
Collected Date 12/29/17 01/05/18 11:491
Collected Time 12:55 01/05/18 11:491
pH 6.0 Std. Units 01/05/18 11:490.10 1
Temperature 11.2 deg C 01/05/18 11:490.50 1
Static Water Level 5.46 feet 01/05/18 11:491
Specific Conductance 308.6 umhos/cm 01/05/18 11:491.0 1
Oxygen, Dissolved 0.3 mg/L 01/05/18 11:49 7782-44-71
Total Well Depth 15.7 feet 01/05/18 11:491
REDOX 163.2 mV 01/05/18 11:491
Turbidity 9.7 NTU 01/05/18 11:491.0 1
Odor NONE 01/05/18 11:491
Appearance CLEAR 01/05/18 11:491
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 01/02/18 22:26 309-00-201/02/18 07:110.050 1
alpha-BHC ND ug/L 01/02/18 22:26 319-84-601/02/18 07:110.050 1
beta-BHC ND ug/L 01/02/18 22:26 319-85-701/02/18 07:110.050 1
delta-BHC ND ug/L 01/02/18 22:26 319-86-801/02/18 07:110.050 1
gamma-BHC (Lindane)ND ug/L 01/02/18 22:26 58-89-901/02/18 07:110.050 1
Chlordane (Technical)ND ug/L 01/02/18 22:26 57-74-901/02/18 07:110.20 1
4,4'-DDD ND ug/L 01/02/18 22:26 72-54-801/02/18 07:110.050 1
4,4'-DDE ND ug/L 01/02/18 22:26 72-55-901/02/18 07:110.050 1
4,4'-DDT ND ug/L 01/02/18 22:26 50-29-301/02/18 07:110.050 1
Dieldrin ND ug/L 01/02/18 22:26 60-57-101/02/18 07:110.050 1
Endosulfan I ND ug/L 01/02/18 22:26 959-98-801/02/18 07:110.050 1
Endosulfan II ND ug/L 01/02/18 22:26 33213-65-901/02/18 07:110.050 1
Endosulfan sulfate ND ug/L 01/02/18 22:26 1031-07-801/02/18 07:110.050 1
Endrin ND ug/L 01/02/18 22:26 72-20-801/02/18 07:110.050 1
Endrin aldehyde ND ug/L 01/02/18 22:26 7421-93-401/02/18 07:110.050 1
Heptachlor ND ug/L 01/02/18 22:26 76-44-801/02/18 07:110.050 1
Heptachlor epoxide ND ug/L 01/02/18 22:26 1024-57-301/02/18 07:110.050 1
Methoxychlor ND ug/L 01/02/18 22:26 72-43-501/02/18 07:110.15 1
Toxaphene ND ug/L 01/02/18 22:26 8001-35-201/02/18 07:110.20 1
Surrogates
Tetrachloro-m-xylene (S)77 %01/02/18 22:26 877-09-801/02/18 07:1120-130 1
Decachlorobiphenyl (S)76 %01/02/18 22:26 2051-24-301/02/18 07:1120-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 01/02/18 20:26 12674-11-201/02/18 07:110.50 1
PCB-1221 (Aroclor 1221)ND ug/L 01/02/18 20:26 11104-28-201/02/18 07:110.50 1
PCB-1232 (Aroclor 1232)ND ug/L 01/02/18 20:26 11141-16-501/02/18 07:110.50 1
PCB-1242 (Aroclor 1242)ND ug/L 01/02/18 20:26 53469-21-901/02/18 07:110.50 1
PCB-1248 (Aroclor 1248)ND ug/L 01/02/18 20:26 12672-29-601/02/18 07:110.50 1
PCB-1254 (Aroclor 1254)ND ug/L 01/02/18 20:26 11097-69-101/02/18 07:110.50 1
PCB-1260 (Aroclor 1260)ND ug/L 01/02/18 20:26 11096-82-501/02/18 07:110.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 89 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-12 Lab ID:92368450016 Collected:12/29/17 12:55 Received:12/29/17 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
Surrogates
Decachlorobiphenyl (S)77 %01/02/18 20:26 2051-24-301/02/18 07:1110-132 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 01/03/18 19:17 83-32-901/02/18 08:2210.0 1
Acenaphthylene ND ug/L 01/03/18 19:17 208-96-801/02/18 08:2210.0 1
Acetophenone ND ug/L 01/03/18 19:17 98-86-201/02/18 08:2210.0 1
2-Acetylaminofluorene ND ug/L 01/03/18 19:17 53-96-3 L201/02/18 08:2220.0 1
4-Aminobiphenyl ND ug/L 01/03/18 19:17 92-67-101/02/18 08:2210.0 1
Anthracene ND ug/L 01/03/18 19:17 120-12-701/02/18 08:2210.0 1
Benzo(a)anthracene ND ug/L 01/03/18 19:17 56-55-301/02/18 08:2210.0 1
Benzo(a)pyrene ND ug/L 01/03/18 19:17 50-32-801/02/18 08:2210.0 1
Benzo(b)fluoranthene ND ug/L 01/03/18 19:17 205-99-201/02/18 08:2210.0 1
Benzo(g,h,i)perylene ND ug/L 01/03/18 19:17 191-24-201/02/18 08:2210.0 1
Benzo(k)fluoranthene ND ug/L 01/03/18 19:17 207-08-901/02/18 08:2210.0 1
Benzyl alcohol ND ug/L 01/03/18 19:17 100-51-601/02/18 08:2220.0 1
4-Bromophenylphenyl ether ND ug/L 01/03/18 19:17 101-55-301/02/18 08:2210.0 1
Butylbenzylphthalate ND ug/L 01/03/18 19:17 85-68-701/02/18 08:2210.0 1
4-Chloro-3-methylphenol ND ug/L 01/03/18 19:17 59-50-701/02/18 08:2220.0 1
4-Chloroaniline ND ug/L 01/03/18 19:17 106-47-801/02/18 08:2220.0 1
Chlorobenzilate ND ug/L 01/03/18 19:17 510-15-601/02/18 08:2210.0 1
bis(2-Chloroethoxy)methane ND ug/L 01/03/18 19:17 111-91-101/02/18 08:2210.0 1
bis(2-Chloroethyl) ether ND ug/L 01/03/18 19:17 111-44-401/02/18 08:2210.0 1
2-Chloronaphthalene ND ug/L 01/03/18 19:17 91-58-701/02/18 08:2210.0 1
2-Chlorophenol ND ug/L 01/03/18 19:17 95-57-801/02/18 08:2210.0 1
4-Chlorophenylphenyl ether ND ug/L 01/03/18 19:17 7005-72-301/02/18 08:2210.0 1
Chrysene ND ug/L 01/03/18 19:17 218-01-901/02/18 08:2210.0 1
Diallate ND ug/L 01/03/18 19:17 2303-16-401/02/18 08:2210.0 1
Dibenz(a,h)anthracene ND ug/L 01/03/18 19:17 53-70-301/02/18 08:2210.0 1
Dibenzofuran ND ug/L 01/03/18 19:17 132-64-901/02/18 08:2210.0 1
3,3'-Dichlorobenzidine ND ug/L 01/03/18 19:17 91-94-101/02/18 08:2220.0 1
2,4-Dichlorophenol ND ug/L 01/03/18 19:17 120-83-201/02/18 08:2210.0 1
2,6-Dichlorophenol ND ug/L 01/03/18 19:17 87-65-001/02/18 08:2210.0 1
Diethylphthalate ND ug/L 01/03/18 19:17 84-66-201/02/18 08:2210.0 1
Dimethoate ND ug/L 01/03/18 19:17 60-51-501/02/18 08:2210.0 1
P-Dimethylaminoazobenzene ND ug/L 01/03/18 19:17 60-11-701/02/18 08:225.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 01/03/18 19:17 57-97-601/02/18 08:2210.0 1
3,3'-Dimethylbenzidine ND ug/L 01/03/18 19:17 119-93-701/02/18 08:2210.0 1
2,4-Dimethylphenol ND ug/L 01/03/18 19:17 105-67-901/02/18 08:2210.0 1
Dimethylphthalate ND ug/L 01/03/18 19:17 131-11-301/02/18 08:2210.0 1
Di-n-butylphthalate ND ug/L 01/03/18 19:17 84-74-201/02/18 08:2210.0 1
4,6-Dinitro-2-methylphenol ND ug/L 01/03/18 19:17 534-52-101/02/18 08:2220.0 1
1,3-Dinitrobenzene ND ug/L 01/03/18 19:17 99-65-001/02/18 08:2220.0 1
2,4-Dinitrophenol ND ug/L 01/03/18 19:17 51-28-501/02/18 08:2250.0 1
2,4-Dinitrotoluene ND ug/L 01/03/18 19:17 121-14-201/02/18 08:2210.0 1
2,6-Dinitrotoluene ND ug/L 01/03/18 19:17 606-20-201/02/18 08:2210.0 1
Di-n-octylphthalate ND ug/L 01/03/18 19:17 117-84-001/02/18 08:2210.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 90 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-12 Lab ID:92368450016 Collected:12/29/17 12:55 Received:12/29/17 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Diphenylamine ND ug/L 01/03/18 19:17 122-39-401/02/18 08:2210.0 1
Disulfoton ND ug/L 01/03/18 19:17 298-04-401/02/18 08:2210.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 01/03/18 19:17 117-81-701/02/18 08:226.0 1
Ethyl methanesulfonate ND ug/L 01/03/18 19:17 62-50-001/02/18 08:2220.0 1
Famphur ND ug/L 01/03/18 19:17 52-85-701/02/18 08:2210.0 1
Fluoranthene ND ug/L 01/03/18 19:17 206-44-001/02/18 08:2210.0 1
Fluorene ND ug/L 01/03/18 19:17 86-73-701/02/18 08:2210.0 1
Hexachlorobenzene ND ug/L 01/03/18 19:17 118-74-101/02/18 08:2210.0 1
Hexachlorocyclopentadiene ND ug/L 01/03/18 19:17 77-47-401/02/18 08:2210.0 1
Hexachloroethane ND ug/L 01/03/18 19:17 67-72-101/02/18 08:2210.0 1
Hexachlorophene ND ug/L 01/03/18 19:17 70-30-401/02/18 08:221001
Indeno(1,2,3-cd)pyrene ND ug/L 01/03/18 19:17 193-39-501/02/18 08:2210.0 1
Isodrin ND ug/L 01/03/18 19:17 465-73-601/02/18 08:2220.0 1
Isophorone ND ug/L 01/03/18 19:17 78-59-101/02/18 08:2210.0 1
Isosafrole ND ug/L 01/03/18 19:17 120-58-101/02/18 08:2210.0 1
Kepone ND ug/L 01/03/18 19:17 143-50-001/02/18 08:2210.0 1
Methapyrilene ND ug/L 01/03/18 19:17 91-80-501/02/18 08:2250.0 1
3-Methylcholanthrene ND ug/L 01/03/18 19:17 56-49-501/02/18 08:2210.0 1
Methyl methanesulfonate ND ug/L 01/03/18 19:17 66-27-3 L101/02/18 08:225.0 1
2-Methylnaphthalene ND ug/L 01/03/18 19:17 91-57-601/02/18 08:2210.0 1
Methyl parathion ND ug/L 01/03/18 19:17 298-00-001/02/18 08:2210.0 1
2-Methylphenol(o-Cresol)ND ug/L 01/03/18 19:17 95-48-701/02/18 08:2210.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 01/03/18 19:17 15831-10-401/02/18 08:2210.0 1
1-Naphthalenamine ND ug/L 01/03/18 19:17 134-32-701/02/18 08:225.0 1
2-Naphthalenamine ND ug/L 01/03/18 19:17 91-59-801/02/18 08:225.0 1
1,4-Naphthoquinone ND ug/L 01/03/18 19:17 130-15-401/02/18 08:225.0 1
2-Nitroaniline ND ug/L 01/03/18 19:17 88-74-401/02/18 08:2250.0 1
3-Nitroaniline ND ug/L 01/03/18 19:17 99-09-201/02/18 08:2250.0 1
4-Nitroaniline ND ug/L 01/03/18 19:17 100-01-601/02/18 08:2220.0 1
Nitrobenzene ND ug/L 01/03/18 19:17 98-95-301/02/18 08:2210.0 1
2-Nitrophenol ND ug/L 01/03/18 19:17 88-75-501/02/18 08:2210.0 1
4-Nitrophenol ND ug/L 01/03/18 19:17 100-02-701/02/18 08:2250.0 1
5-Nitro-o-toluidine ND ug/L 01/03/18 19:17 99-55-8 L201/02/18 08:2210.0 1
N-Nitrosodiethylamine ND ug/L 01/03/18 19:17 55-18-501/02/18 08:2220.0 1
N-Nitrosodimethylamine ND ug/L 01/03/18 19:17 62-75-901/02/18 08:2210.0 1
N-Nitroso-di-n-butylamine ND ug/L 01/03/18 19:17 924-16-301/02/18 08:2210.0 1
N-Nitroso-di-n-propylamine ND ug/L 01/03/18 19:17 621-64-701/02/18 08:2210.0 1
N-Nitrosodiphenylamine ND ug/L 01/03/18 19:17 86-30-601/02/18 08:2210.0 1
N-Nitrosomethylethylamine ND ug/L 01/03/18 19:17 10595-95-601/02/18 08:2210.0 1
N-Nitrosopiperidine ND ug/L 01/03/18 19:17 100-75-401/02/18 08:2220.0 1
N-Nitrosopyrrolidine ND ug/L 01/03/18 19:17 930-55-201/02/18 08:2210.0 1
O,O,O-Triethylphosphorothioate ND ug/L 01/03/18 19:17 126-68-101/02/18 08:2210.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 01/03/18 19:17 108-60-101/02/18 08:2210.0 1
Parathion (Ethyl parathion)ND ug/L 01/03/18 19:17 56-38-201/02/18 08:2210.0 1
Pentachlorobenzene ND ug/L 01/03/18 19:17 608-93-501/02/18 08:2210.0 1
Pentachloronitrobenzene ND ug/L 01/03/18 19:17 82-68-801/02/18 08:2220.0 1
Pentachlorophenol ND ug/L 01/03/18 19:17 87-86-501/02/18 08:2225.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 91 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-12 Lab ID:92368450016 Collected:12/29/17 12:55 Received:12/29/17 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Phenacetin ND ug/L 01/03/18 19:17 62-44-201/02/18 08:2220.0 1
Phenanthrene ND ug/L 01/03/18 19:17 85-01-801/02/18 08:2210.0 1
Phenol ND ug/L 01/03/18 19:17 108-95-201/02/18 08:2210.0 1
p-Phenylenediamine ND ug/L 01/03/18 19:17 106-50-3 L201/02/18 08:2210.0 1
Phorate ND ug/L 01/03/18 19:17 298-02-201/02/18 08:2210.0 1
Pronamide ND ug/L 01/03/18 19:17 23950-58-501/02/18 08:2210.0 1
Pyrene ND ug/L 01/03/18 19:17 129-00-001/02/18 08:2210.0 1
Safrole ND ug/L 01/03/18 19:17 94-59-701/02/18 08:2210.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 01/03/18 19:17 95-94-301/02/18 08:2210.0 1
2,3,4,6-Tetrachlorophenol ND ug/L 01/03/18 19:17 58-90-201/02/18 08:2210.0 1
Thionazin ND ug/L 01/03/18 19:17 297-97-201/02/18 08:2220.0 1
O-Toluidine ND ug/L 01/03/18 19:17 95-53-401/02/18 08:2210.0 1
2,4,5-Trichlorophenol ND ug/L 01/03/18 19:17 95-95-401/02/18 08:2210.0 1
2,4,6-Trichlorophenol ND ug/L 01/03/18 19:17 88-06-201/02/18 08:2210.0 1
1,3,5-Trinitrobenzene ND ug/L 01/03/18 19:17 99-35-4 L201/02/18 08:2210.0 1
Surrogates
Nitrobenzene-d5 (S)68 %01/03/18 19:17 4165-60-001/02/18 08:2221-110 1
2-Fluorobiphenyl (S)64 %01/03/18 19:17 321-60-801/02/18 08:2227-110 1
Terphenyl-d14 (S)52 %01/03/18 19:17 1718-51-001/02/18 08:2231-107 1
Phenol-d6 (S)21 %01/03/18 19:17 13127-88-301/02/18 08:2210-110 1
2-Fluorophenol (S)31 %01/03/18 19:17 367-12-401/02/18 08:2212-110 1
2,4,6-Tribromophenol (S)71 %01/03/18 19:17 118-79-601/02/18 08:2227-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/18 17:02 67-64-125.0 1
Acetonitrile ND ug/L 01/03/18 17:02 75-05-850.0 1
Acrolein ND ug/L 01/03/18 17:02 107-02-810.0 1
Acrylonitrile ND ug/L 01/03/18 17:02 107-13-110.0 1
Allyl chloride ND ug/L 01/03/18 17:02 107-05-12.0 1
Benzene ND ug/L 01/03/18 17:02 71-43-21.0 1
Bromochloromethane ND ug/L 01/03/18 17:02 74-97-51.0 1
Bromodichloromethane ND ug/L 01/03/18 17:02 75-27-41.0 1
Bromoform ND ug/L 01/03/18 17:02 75-25-21.0 1
Bromomethane ND ug/L 01/03/18 17:02 74-83-92.0 1
2-Butanone (MEK)ND ug/L 01/03/18 17:02 78-93-35.0 1
Carbon disulfide ND ug/L 01/03/18 17:02 75-15-02.0 1
Carbon tetrachloride ND ug/L 01/03/18 17:02 56-23-51.0 1
Chlorobenzene ND ug/L 01/03/18 17:02 108-90-71.0 1
Chloroethane ND ug/L 01/03/18 17:02 75-00-31.0 1
Chloroform ND ug/L 01/03/18 17:02 67-66-31.0 1
Chloromethane ND ug/L 01/03/18 17:02 74-87-31.0 1
Chloroprene ND ug/L 01/03/18 17:02 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/18 17:02 96-12-82.0 1
Dibromochloromethane ND ug/L 01/03/18 17:02 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/18 17:02 106-93-41.0 1
Dibromomethane ND ug/L 01/03/18 17:02 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 01/03/18 17:02 95-50-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 92 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-12 Lab ID:92368450016 Collected:12/29/17 12:55 Received:12/29/17 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,3-Dichlorobenzene ND ug/L 01/03/18 17:02 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 01/03/18 17:02 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/18 17:02 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 01/03/18 17:02 75-71-81.0 1
1,1-Dichloroethane ND ug/L 01/03/18 17:02 75-34-31.0 1
1,2-Dichloroethane ND ug/L 01/03/18 17:02 107-06-21.0 1
1,1-Dichloroethene ND ug/L 01/03/18 17:02 75-35-41.0 1
cis-1,2-Dichloroethene 0.23J ug/L 01/03/18 17:02 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 01/03/18 17:02 156-60-51.0 1
1,2-Dichloropropane ND ug/L 01/03/18 17:02 78-87-51.0 1
1,3-Dichloropropane ND ug/L 01/03/18 17:02 142-28-91.0 1
2,2-Dichloropropane ND ug/L 01/03/18 17:02 594-20-71.0 1
1,1-Dichloropropene ND ug/L 01/03/18 17:02 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 01/03/18 17:02 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 01/03/18 17:02 10061-02-61.0 1
Ethylbenzene ND ug/L 01/03/18 17:02 100-41-41.0 1
Ethyl methacrylate ND ug/L 01/03/18 17:02 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 01/03/18 17:02 87-68-31.0 1
2-Hexanone ND ug/L 01/03/18 17:02 591-78-65.0 1
Iodomethane ND ug/L 01/03/18 17:02 74-88-45.0 1
Isobutanol ND ug/L 01/03/18 17:02 78-83-11001
Methacrylonitrile ND ug/L 01/03/18 17:02 126-98-710.0 1
Methylene Chloride ND ug/L 01/03/18 17:02 75-09-21.0 1
Methyl methacrylate ND ug/L 01/03/18 17:02 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/18 17:02 108-10-15.0 1
Naphthalene ND ug/L 01/03/18 17:02 91-20-31.0 1
Propionitrile ND ug/L 01/03/18 17:02 107-12-020.0 1
Styrene ND ug/L 01/03/18 17:02 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/18 17:02 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/18 17:02 79-34-51.0 1
Tetrachloroethene ND ug/L 01/03/18 17:02 127-18-41.0 1
Tetrahydrofuran ND ug/L 01/03/18 17:02 109-99-910.0 1
Toluene ND ug/L 01/03/18 17:02 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 01/03/18 17:02 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 01/03/18 17:02 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 01/03/18 17:02 79-00-51.0 1
Trichloroethene ND ug/L 01/03/18 17:02 79-01-61.0 1
Trichlorofluoromethane 1.4 ug/L 01/03/18 17:02 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 01/03/18 17:02 96-18-41.0 1
Vinyl acetate ND ug/L 01/03/18 17:02 108-05-42.0 1
Vinyl chloride ND ug/L 01/03/18 17:02 75-01-41.0 1
Xylene (Total)ND ug/L 01/03/18 17:02 1330-20-71.0 1
m&p-Xylene ND ug/L 01/03/18 17:02 179601-23-12.0 1
o-Xylene ND ug/L 01/03/18 17:02 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)98 %01/03/18 17:02 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %01/03/18 17:02 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 93 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-12 Lab ID:92368450016 Collected:12/29/17 12:55 Received:12/29/17 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Surrogates
Toluene-d8 (S)110 %01/03/18 17:02 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 94 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-15 Lab ID:92368450017 Collected:12/29/17 11:30 Received:12/29/17 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method:Monitoring Well Data
Collected By GLG 01/05/18 11:521
Collected Date 12/29/17 01/05/18 11:521
Collected Time 11:30 01/05/18 11:521
pH 6.1 Std. Units 01/05/18 11:520.10 1
Temperature 8.2 deg C 01/05/18 11:520.50 1
Static Water Level 39.58 feet 01/05/18 11:521
Specific Conductance 832 umhos/cm 01/05/18 11:521.0 1
Oxygen, Dissolved 2.3 mg/L 01/05/18 11:52 7782-44-71
Total Well Depth 48.0 feet 01/05/18 11:521
REDOX 105.1 mV 01/05/18 11:521
Turbidity 2.7 NTU 01/05/18 11:521.0 1
Odor NONE 01/05/18 11:521
Appearance CLEAR 01/05/18 11:521
Analytical Method: EPA 8081 Preparation Method: EPA 35108081 Organochlorine Pesticides
Aldrin ND ug/L 01/02/18 22:44 309-00-201/02/18 07:110.050 1
alpha-BHC ND ug/L 01/02/18 22:44 319-84-601/02/18 07:110.050 1
beta-BHC ND ug/L 01/02/18 22:44 319-85-701/02/18 07:110.050 1
delta-BHC ND ug/L 01/02/18 22:44 319-86-801/02/18 07:110.050 1
gamma-BHC (Lindane)ND ug/L 01/02/18 22:44 58-89-901/02/18 07:110.050 1
Chlordane (Technical)ND ug/L 01/02/18 22:44 57-74-901/02/18 07:110.20 1
4,4'-DDD ND ug/L 01/02/18 22:44 72-54-801/02/18 07:110.050 1
4,4'-DDE ND ug/L 01/02/18 22:44 72-55-901/02/18 07:110.050 1
4,4'-DDT ND ug/L 01/02/18 22:44 50-29-301/02/18 07:110.050 1
Dieldrin ND ug/L 01/02/18 22:44 60-57-101/02/18 07:110.050 1
Endosulfan I ND ug/L 01/02/18 22:44 959-98-801/02/18 07:110.050 1
Endosulfan II ND ug/L 01/02/18 22:44 33213-65-901/02/18 07:110.050 1
Endosulfan sulfate ND ug/L 01/02/18 22:44 1031-07-801/02/18 07:110.050 1
Endrin ND ug/L 01/02/18 22:44 72-20-801/02/18 07:110.050 1
Endrin aldehyde ND ug/L 01/02/18 22:44 7421-93-401/02/18 07:110.050 1
Heptachlor ND ug/L 01/02/18 22:44 76-44-801/02/18 07:110.050 1
Heptachlor epoxide ND ug/L 01/02/18 22:44 1024-57-301/02/18 07:110.050 1
Methoxychlor ND ug/L 01/02/18 22:44 72-43-501/02/18 07:110.15 1
Toxaphene ND ug/L 01/02/18 22:44 8001-35-201/02/18 07:110.20 1
Surrogates
Tetrachloro-m-xylene (S)68 %01/02/18 22:44 877-09-801/02/18 07:1120-130 1
Decachlorobiphenyl (S)70 %01/02/18 22:44 2051-24-301/02/18 07:1120-130 1
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/L 01/02/18 20:47 12674-11-201/02/18 07:110.50 1
PCB-1221 (Aroclor 1221)ND ug/L 01/02/18 20:47 11104-28-201/02/18 07:110.50 1
PCB-1232 (Aroclor 1232)ND ug/L 01/02/18 20:47 11141-16-501/02/18 07:110.50 1
PCB-1242 (Aroclor 1242)ND ug/L 01/02/18 20:47 53469-21-901/02/18 07:110.50 1
PCB-1248 (Aroclor 1248)ND ug/L 01/02/18 20:47 12672-29-601/02/18 07:110.50 1
PCB-1254 (Aroclor 1254)ND ug/L 01/02/18 20:47 11097-69-101/02/18 07:110.50 1
PCB-1260 (Aroclor 1260)ND ug/L 01/02/18 20:47 11096-82-501/02/18 07:110.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 95 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-15 Lab ID:92368450017 Collected:12/29/17 11:30 Received:12/29/17 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8082 Preparation Method: EPA 35108082 GCS PCB
Surrogates
Decachlorobiphenyl (S)67 %01/02/18 20:47 2051-24-301/02/18 07:1110-132 1
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 01/04/18 12:33 83-32-901/02/18 08:2210.0 1
Acenaphthylene ND ug/L 01/04/18 12:33 208-96-801/02/18 08:2210.0 1
Acetophenone ND ug/L 01/04/18 12:33 98-86-201/02/18 08:2210.0 1
2-Acetylaminofluorene ND ug/L 01/04/18 12:33 53-96-3 L201/02/18 08:2220.0 1
4-Aminobiphenyl ND ug/L 01/04/18 12:33 92-67-101/02/18 08:2210.0 1
Anthracene ND ug/L 01/04/18 12:33 120-12-701/02/18 08:2210.0 1
Benzo(a)anthracene ND ug/L 01/04/18 12:33 56-55-301/02/18 08:2210.0 1
Benzo(a)pyrene ND ug/L 01/04/18 12:33 50-32-801/02/18 08:2210.0 1
Benzo(b)fluoranthene ND ug/L 01/04/18 12:33 205-99-201/02/18 08:2210.0 1
Benzo(g,h,i)perylene ND ug/L 01/04/18 12:33 191-24-201/02/18 08:2210.0 1
Benzo(k)fluoranthene ND ug/L 01/04/18 12:33 207-08-901/02/18 08:2210.0 1
Benzyl alcohol ND ug/L 01/04/18 12:33 100-51-601/02/18 08:2220.0 1
4-Bromophenylphenyl ether ND ug/L 01/04/18 12:33 101-55-301/02/18 08:2210.0 1
Butylbenzylphthalate ND ug/L 01/04/18 12:33 85-68-701/02/18 08:2210.0 1
4-Chloro-3-methylphenol ND ug/L 01/04/18 12:33 59-50-701/02/18 08:2220.0 1
4-Chloroaniline ND ug/L 01/04/18 12:33 106-47-801/02/18 08:2220.0 1
Chlorobenzilate ND ug/L 01/04/18 12:33 510-15-601/02/18 08:2210.0 1
bis(2-Chloroethoxy)methane ND ug/L 01/04/18 12:33 111-91-101/02/18 08:2210.0 1
bis(2-Chloroethyl) ether ND ug/L 01/04/18 12:33 111-44-401/02/18 08:2210.0 1
2-Chloronaphthalene ND ug/L 01/04/18 12:33 91-58-701/02/18 08:2210.0 1
2-Chlorophenol ND ug/L 01/04/18 12:33 95-57-801/02/18 08:2210.0 1
4-Chlorophenylphenyl ether ND ug/L 01/04/18 12:33 7005-72-301/02/18 08:2210.0 1
Chrysene ND ug/L 01/04/18 12:33 218-01-901/02/18 08:2210.0 1
Diallate ND ug/L 01/04/18 12:33 2303-16-401/02/18 08:2210.0 1
Dibenz(a,h)anthracene ND ug/L 01/04/18 12:33 53-70-301/02/18 08:2210.0 1
Dibenzofuran ND ug/L 01/04/18 12:33 132-64-901/02/18 08:2210.0 1
3,3'-Dichlorobenzidine ND ug/L 01/04/18 12:33 91-94-101/02/18 08:2220.0 1
2,4-Dichlorophenol ND ug/L 01/04/18 12:33 120-83-201/02/18 08:2210.0 1
2,6-Dichlorophenol ND ug/L 01/04/18 12:33 87-65-001/02/18 08:2210.0 1
Diethylphthalate ND ug/L 01/04/18 12:33 84-66-201/02/18 08:2210.0 1
Dimethoate ND ug/L 01/04/18 12:33 60-51-501/02/18 08:2210.0 1
P-Dimethylaminoazobenzene ND ug/L 01/04/18 12:33 60-11-701/02/18 08:225.0 1
7,12-Dimethylbenz(a)anthracene ND ug/L 01/04/18 12:33 57-97-601/02/18 08:2210.0 1
3,3'-Dimethylbenzidine ND ug/L 01/04/18 12:33 119-93-701/02/18 08:2210.0 1
2,4-Dimethylphenol ND ug/L 01/04/18 12:33 105-67-901/02/18 08:2210.0 1
Dimethylphthalate ND ug/L 01/04/18 12:33 131-11-301/02/18 08:2210.0 1
Di-n-butylphthalate ND ug/L 01/04/18 12:33 84-74-201/02/18 08:2210.0 1
4,6-Dinitro-2-methylphenol ND ug/L 01/04/18 12:33 534-52-101/02/18 08:2220.0 1
1,3-Dinitrobenzene ND ug/L 01/04/18 12:33 99-65-001/02/18 08:2220.0 1
2,4-Dinitrophenol ND ug/L 01/04/18 12:33 51-28-501/02/18 08:2250.0 1
2,4-Dinitrotoluene ND ug/L 01/04/18 12:33 121-14-201/02/18 08:2210.0 1
2,6-Dinitrotoluene ND ug/L 01/04/18 12:33 606-20-201/02/18 08:2210.0 1
Di-n-octylphthalate ND ug/L 01/04/18 12:33 117-84-001/02/18 08:2210.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 96 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-15 Lab ID:92368450017 Collected:12/29/17 11:30 Received:12/29/17 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Diphenylamine ND ug/L 01/04/18 12:33 122-39-401/02/18 08:2210.0 1
Disulfoton ND ug/L 01/04/18 12:33 298-04-401/02/18 08:2210.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 01/04/18 12:33 117-81-701/02/18 08:226.0 1
Ethyl methanesulfonate ND ug/L 01/04/18 12:33 62-50-001/02/18 08:2220.0 1
Famphur ND ug/L 01/04/18 12:33 52-85-701/02/18 08:2210.0 1
Fluoranthene ND ug/L 01/04/18 12:33 206-44-001/02/18 08:2210.0 1
Fluorene ND ug/L 01/04/18 12:33 86-73-701/02/18 08:2210.0 1
Hexachlorobenzene ND ug/L 01/04/18 12:33 118-74-101/02/18 08:2210.0 1
Hexachlorocyclopentadiene ND ug/L 01/04/18 12:33 77-47-401/02/18 08:2210.0 1
Hexachloroethane ND ug/L 01/04/18 12:33 67-72-101/02/18 08:2210.0 1
Hexachlorophene ND ug/L 01/04/18 12:33 70-30-401/02/18 08:221001
Indeno(1,2,3-cd)pyrene ND ug/L 01/04/18 12:33 193-39-501/02/18 08:2210.0 1
Isodrin ND ug/L 01/04/18 12:33 465-73-601/02/18 08:2220.0 1
Isophorone ND ug/L 01/04/18 12:33 78-59-101/02/18 08:2210.0 1
Isosafrole ND ug/L 01/04/18 12:33 120-58-101/02/18 08:2210.0 1
Kepone ND ug/L 01/04/18 12:33 143-50-001/02/18 08:2210.0 1
Methapyrilene ND ug/L 01/04/18 12:33 91-80-501/02/18 08:2250.0 1
3-Methylcholanthrene ND ug/L 01/04/18 12:33 56-49-501/02/18 08:2210.0 1
Methyl methanesulfonate ND ug/L 01/04/18 12:33 66-27-3 L101/02/18 08:225.0 1
2-Methylnaphthalene ND ug/L 01/04/18 12:33 91-57-601/02/18 08:2210.0 1
Methyl parathion ND ug/L 01/04/18 12:33 298-00-001/02/18 08:2210.0 1
2-Methylphenol(o-Cresol)ND ug/L 01/04/18 12:33 95-48-701/02/18 08:2210.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 01/04/18 12:33 15831-10-401/02/18 08:2210.0 1
1-Naphthalenamine ND ug/L 01/04/18 12:33 134-32-701/02/18 08:225.0 1
2-Naphthalenamine ND ug/L 01/04/18 12:33 91-59-801/02/18 08:225.0 1
1,4-Naphthoquinone ND ug/L 01/04/18 12:33 130-15-401/02/18 08:225.0 1
2-Nitroaniline ND ug/L 01/04/18 12:33 88-74-401/02/18 08:2250.0 1
3-Nitroaniline ND ug/L 01/04/18 12:33 99-09-201/02/18 08:2250.0 1
4-Nitroaniline ND ug/L 01/04/18 12:33 100-01-601/02/18 08:2220.0 1
Nitrobenzene ND ug/L 01/04/18 12:33 98-95-301/02/18 08:2210.0 1
2-Nitrophenol ND ug/L 01/04/18 12:33 88-75-501/02/18 08:2210.0 1
4-Nitrophenol ND ug/L 01/04/18 12:33 100-02-701/02/18 08:2250.0 1
5-Nitro-o-toluidine ND ug/L 01/04/18 12:33 99-55-8 L201/02/18 08:2210.0 1
N-Nitrosodiethylamine ND ug/L 01/04/18 12:33 55-18-501/02/18 08:2220.0 1
N-Nitrosodimethylamine ND ug/L 01/04/18 12:33 62-75-901/02/18 08:2210.0 1
N-Nitroso-di-n-butylamine ND ug/L 01/04/18 12:33 924-16-301/02/18 08:2210.0 1
N-Nitroso-di-n-propylamine ND ug/L 01/04/18 12:33 621-64-701/02/18 08:2210.0 1
N-Nitrosodiphenylamine ND ug/L 01/04/18 12:33 86-30-601/02/18 08:2210.0 1
N-Nitrosomethylethylamine ND ug/L 01/04/18 12:33 10595-95-601/02/18 08:2210.0 1
N-Nitrosopiperidine ND ug/L 01/04/18 12:33 100-75-401/02/18 08:2220.0 1
N-Nitrosopyrrolidine ND ug/L 01/04/18 12:33 930-55-201/02/18 08:2210.0 1
O,O,O-Triethylphosphorothioate ND ug/L 01/04/18 12:33 126-68-101/02/18 08:2210.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 01/04/18 12:33 108-60-101/02/18 08:2210.0 1
Parathion (Ethyl parathion)ND ug/L 01/04/18 12:33 56-38-201/02/18 08:2210.0 1
Pentachlorobenzene ND ug/L 01/04/18 12:33 608-93-501/02/18 08:2210.0 1
Pentachloronitrobenzene ND ug/L 01/04/18 12:33 82-68-801/02/18 08:2220.0 1
Pentachlorophenol ND ug/L 01/04/18 12:33 87-86-501/02/18 08:2225.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 97 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-15 Lab ID:92368450017 Collected:12/29/17 11:30 Received:12/29/17 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Phenacetin ND ug/L 01/04/18 12:33 62-44-201/02/18 08:2220.0 1
Phenanthrene ND ug/L 01/04/18 12:33 85-01-801/02/18 08:2210.0 1
Phenol ND ug/L 01/04/18 12:33 108-95-201/02/18 08:2210.0 1
p-Phenylenediamine ND ug/L 01/04/18 12:33 106-50-3 L201/02/18 08:2210.0 1
Phorate ND ug/L 01/04/18 12:33 298-02-201/02/18 08:2210.0 1
Pronamide ND ug/L 01/04/18 12:33 23950-58-501/02/18 08:2210.0 1
Pyrene ND ug/L 01/04/18 12:33 129-00-001/02/18 08:2210.0 1
Safrole ND ug/L 01/04/18 12:33 94-59-701/02/18 08:2210.0 1
1,2,4,5-Tetrachlorobenzene ND ug/L 01/04/18 12:33 95-94-301/02/18 08:2210.0 1
2,3,4,6-Tetrachlorophenol ND ug/L 01/04/18 12:33 58-90-201/02/18 08:2210.0 1
Thionazin ND ug/L 01/04/18 12:33 297-97-201/02/18 08:2220.0 1
O-Toluidine ND ug/L 01/04/18 12:33 95-53-401/02/18 08:2210.0 1
2,4,5-Trichlorophenol ND ug/L 01/04/18 12:33 95-95-401/02/18 08:2210.0 1
2,4,6-Trichlorophenol ND ug/L 01/04/18 12:33 88-06-201/02/18 08:2210.0 1
1,3,5-Trinitrobenzene ND ug/L 01/04/18 12:33 99-35-4 L201/02/18 08:2210.0 1
Surrogates
Nitrobenzene-d5 (S)65 %01/04/18 12:33 4165-60-001/02/18 08:2221-110 1
2-Fluorobiphenyl (S)62 %01/04/18 12:33 321-60-801/02/18 08:2227-110 1
Terphenyl-d14 (S)55 %01/04/18 12:33 1718-51-001/02/18 08:2231-107 1
Phenol-d6 (S)15 %01/04/18 12:33 13127-88-301/02/18 08:2210-110 1
2-Fluorophenol (S)28 %01/04/18 12:33 367-12-401/02/18 08:2212-110 1
2,4,6-Tribromophenol (S)71 %01/04/18 12:33 118-79-601/02/18 08:2227-110 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/18 17:20 67-64-125.0 1
Acetonitrile ND ug/L 01/03/18 17:20 75-05-850.0 1
Acrolein ND ug/L 01/03/18 17:20 107-02-810.0 1
Acrylonitrile ND ug/L 01/03/18 17:20 107-13-110.0 1
Allyl chloride ND ug/L 01/03/18 17:20 107-05-12.0 1
Benzene ND ug/L 01/03/18 17:20 71-43-21.0 1
Bromochloromethane ND ug/L 01/03/18 17:20 74-97-51.0 1
Bromodichloromethane ND ug/L 01/03/18 17:20 75-27-41.0 1
Bromoform ND ug/L 01/03/18 17:20 75-25-21.0 1
Bromomethane ND ug/L 01/03/18 17:20 74-83-92.0 1
2-Butanone (MEK)ND ug/L 01/03/18 17:20 78-93-35.0 1
Carbon disulfide ND ug/L 01/03/18 17:20 75-15-02.0 1
Carbon tetrachloride ND ug/L 01/03/18 17:20 56-23-51.0 1
Chlorobenzene ND ug/L 01/03/18 17:20 108-90-71.0 1
Chloroethane ND ug/L 01/03/18 17:20 75-00-31.0 1
Chloroform 0.44J ug/L 01/03/18 17:20 67-66-31.0 1
Chloromethane ND ug/L 01/03/18 17:20 74-87-31.0 1
Chloroprene ND ug/L 01/03/18 17:20 126-99-85.0 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/18 17:20 96-12-82.0 1
Dibromochloromethane ND ug/L 01/03/18 17:20 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/18 17:20 106-93-41.0 1
Dibromomethane ND ug/L 01/03/18 17:20 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 01/03/18 17:20 95-50-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 98 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-15 Lab ID:92368450017 Collected:12/29/17 11:30 Received:12/29/17 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,3-Dichlorobenzene ND ug/L 01/03/18 17:20 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 01/03/18 17:20 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/18 17:20 110-57-61.0 1
Dichlorodifluoromethane ND ug/L 01/03/18 17:20 75-71-81.0 1
1,1-Dichloroethane ND ug/L 01/03/18 17:20 75-34-31.0 1
1,2-Dichloroethane ND ug/L 01/03/18 17:20 107-06-21.0 1
1,1-Dichloroethene ND ug/L 01/03/18 17:20 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 01/03/18 17:20 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 01/03/18 17:20 156-60-51.0 1
1,2-Dichloropropane ND ug/L 01/03/18 17:20 78-87-51.0 1
1,3-Dichloropropane ND ug/L 01/03/18 17:20 142-28-91.0 1
2,2-Dichloropropane ND ug/L 01/03/18 17:20 594-20-71.0 1
1,1-Dichloropropene ND ug/L 01/03/18 17:20 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 01/03/18 17:20 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 01/03/18 17:20 10061-02-61.0 1
Ethylbenzene ND ug/L 01/03/18 17:20 100-41-41.0 1
Ethyl methacrylate ND ug/L 01/03/18 17:20 97-63-21.0 1
Hexachloro-1,3-butadiene ND ug/L 01/03/18 17:20 87-68-31.0 1
2-Hexanone ND ug/L 01/03/18 17:20 591-78-65.0 1
Iodomethane ND ug/L 01/03/18 17:20 74-88-45.0 1
Isobutanol ND ug/L 01/03/18 17:20 78-83-11001
Methacrylonitrile ND ug/L 01/03/18 17:20 126-98-710.0 1
Methylene Chloride ND ug/L 01/03/18 17:20 75-09-21.0 1
Methyl methacrylate ND ug/L 01/03/18 17:20 80-62-62.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/18 17:20 108-10-15.0 1
Naphthalene ND ug/L 01/03/18 17:20 91-20-31.0 1
Propionitrile ND ug/L 01/03/18 17:20 107-12-020.0 1
Styrene ND ug/L 01/03/18 17:20 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/18 17:20 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/18 17:20 79-34-51.0 1
Tetrachloroethene ND ug/L 01/03/18 17:20 127-18-41.0 1
Tetrahydrofuran ND ug/L 01/03/18 17:20 109-99-910.0 1
Toluene ND ug/L 01/03/18 17:20 108-88-31.0 1
1,2,4-Trichlorobenzene ND ug/L 01/03/18 17:20 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 01/03/18 17:20 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 01/03/18 17:20 79-00-51.0 1
Trichloroethene ND ug/L 01/03/18 17:20 79-01-61.0 1
Trichlorofluoromethane 0.22J ug/L 01/03/18 17:20 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 01/03/18 17:20 96-18-41.0 1
Vinyl acetate ND ug/L 01/03/18 17:20 108-05-42.0 1
Vinyl chloride ND ug/L 01/03/18 17:20 75-01-41.0 1
Xylene (Total)ND ug/L 01/03/18 17:20 1330-20-71.0 1
m&p-Xylene ND ug/L 01/03/18 17:20 179601-23-12.0 1
o-Xylene ND ug/L 01/03/18 17:20 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)100 %01/03/18 17:20 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %01/03/18 17:20 17060-07-070-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
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Page 99 of 176
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92368450
OSR 305065
Sample:MW-15 Lab ID:92368450017 Collected:12/29/17 11:30 Received:12/29/17 16:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Surrogates
Toluene-d8 (S)109 %01/03/18 17:20 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
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Page 100 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
392950
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92368450001, 92368450002, 92368450003, 92368450004, 92368450005, 92368450006, 92368450007,92368450008, 92368450009, 92368450010, 92368450011, 92368450012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2179164
Associated Lab Samples:92368450001, 92368450002, 92368450003, 92368450004, 92368450005, 92368450006, 92368450007,92368450008, 92368450009, 92368450010, 92368450011, 92368450012
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 01/03/18 00:32
1,1,1-Trichloroethane ug/L ND 1.0 01/03/18 00:32
1,1,2,2-Tetrachloroethane ug/L ND 1.0 01/03/18 00:32
1,1,2-Trichloroethane ug/L ND 1.0 01/03/18 00:32
1,1-Dichloroethane ug/L ND 1.0 01/03/18 00:32
1,1-Dichloroethene ug/L ND 1.0 01/03/18 00:32
1,1-Dichloropropene ug/L ND 1.0 01/03/18 00:32
1,2,3-Trichloropropane ug/L ND 1.0 01/03/18 00:32
1,2,4-Trichlorobenzene ug/L ND 1.0 01/03/18 00:32
1,2-Dibromo-3-chloropropane ug/L ND 2.0 01/03/18 00:32
1,2-Dibromoethane (EDB)ug/L ND 1.0 01/03/18 00:32
1,2-Dichlorobenzene ug/L ND 1.0 01/03/18 00:32
1,2-Dichloroethane ug/L ND 1.0 01/03/18 00:32
1,2-Dichloropropane ug/L ND 1.0 01/03/18 00:32
1,3-Dichlorobenzene ug/L ND 1.0 01/03/18 00:32
1,3-Dichloropropane ug/L ND 1.0 01/03/18 00:32
1,4-Dichlorobenzene ug/L ND 1.0 01/03/18 00:32
2,2-Dichloropropane ug/L ND 1.0 01/03/18 00:32
2-Butanone (MEK)ug/L ND 5.0 01/03/18 00:32
2-Hexanone ug/L ND 5.0 01/03/18 00:32
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 01/03/18 00:32
Acetone ug/L ND 25.0 01/03/18 00:32
Acetonitrile ug/L ND 50.0 01/03/18 00:32
Acrolein ug/L ND 10.0 01/03/18 00:32
Acrylonitrile ug/L ND 10.0 01/03/18 00:32
Allyl chloride ug/L ND 2.0 01/03/18 00:32
Benzene ug/L ND 1.0 01/03/18 00:32
Bromochloromethane ug/L ND 1.0 01/03/18 00:32
Bromodichloromethane ug/L ND 1.0 01/03/18 00:32
Bromoform ug/L ND 1.0 01/03/18 00:32
Bromomethane ug/L ND 2.0 01/03/18 00:32
Carbon disulfide ug/L ND 2.0 01/03/18 00:32
Carbon tetrachloride ug/L ND 1.0 01/03/18 00:32
Chlorobenzene ug/L ND 1.0 01/03/18 00:32
Chloroethane ug/L ND 1.0 01/03/18 00:32
Chloroform ug/L ND 1.0 01/03/18 00:32
Chloromethane ug/L ND 1.0 01/03/18 00:32
Chloroprene ug/L ND 5.0 01/03/18 00:32
cis-1,2-Dichloroethene ug/L ND 1.0 01/03/18 00:32
cis-1,3-Dichloropropene ug/L ND 1.0 01/03/18 00:32
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
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Page 101 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2179164
Associated Lab Samples:92368450001, 92368450002, 92368450003, 92368450004, 92368450005, 92368450006, 92368450007,92368450008, 92368450009, 92368450010, 92368450011, 92368450012
Matrix:Water
Analyzed
Dibromochloromethane ug/L ND 1.0 01/03/18 00:32
Dibromomethane ug/L ND 1.0 01/03/18 00:32
Dichlorodifluoromethane ug/L ND 1.0 01/03/18 00:32
Ethyl methacrylate ug/L ND 1.0 01/03/18 00:32
Ethylbenzene ug/L ND 1.0 01/03/18 00:32
Hexachloro-1,3-butadiene ug/L ND 1.0 01/03/18 00:32
Iodomethane ug/L ND 5.0 01/03/18 00:32
Isobutanol ug/L ND 100 01/03/18 00:32
m&p-Xylene ug/L ND 2.0 01/03/18 00:32
Methacrylonitrile ug/L ND 10.0 01/03/18 00:32
Methyl methacrylate ug/L ND 2.0 01/03/18 00:32
Methylene Chloride ug/L ND 1.0 01/03/18 00:32
Naphthalene ug/L ND 1.0 01/03/18 00:32
o-Xylene ug/L ND 1.0 01/03/18 00:32
Propionitrile ug/L ND 20.0 01/03/18 00:32
Styrene ug/L ND 1.0 01/03/18 00:32
Tetrachloroethene ug/L ND 1.0 01/03/18 00:32
Tetrahydrofuran ug/L ND 10.0 01/03/18 00:32
Toluene ug/L ND 1.0 01/03/18 00:32
trans-1,2-Dichloroethene ug/L ND 1.0 01/03/18 00:32
trans-1,3-Dichloropropene ug/L ND 1.0 01/03/18 00:32
trans-1,4-Dichloro-2-butene ug/L ND 1.0 01/03/18 00:32
Trichloroethene ug/L ND 1.0 01/03/18 00:32
Trichlorofluoromethane ug/L ND 1.0 01/03/18 00:32
Vinyl acetate ug/L ND 2.0 01/03/18 00:32
Vinyl chloride ug/L ND 1.0 01/03/18 00:32
Xylene (Total)ug/L ND 1.0 01/03/18 00:32
1,2-Dichloroethane-d4 (S)%98 70-130 01/03/18 00:32
4-Bromofluorobenzene (S)%102 70-130 01/03/18 00:32
Toluene-d8 (S)%109 70-130 01/03/18 00:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2179165LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 44.950 90 80-125
1,1,1-Trichloroethane ug/L 52.850 106 71-129
1,1,2,2-Tetrachloroethane ug/L 41.250 82 79-124
1,1,2-Trichloroethane ug/L 47.150 94 85-125
1,1-Dichloroethane ug/L 47.850 96 73-126
1,1-Dichloroethene ug/L 49.850 100 66-135
1,1-Dichloropropene ug/L 49.550 99 74-135
1,2,3-Trichloropropane ug/L 42.650 85 75-130
1,2,4-Trichlorobenzene ug/L 50.150 100 75-134
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 102 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2179165LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 35.0 L2507071-133
1,2-Dibromoethane (EDB)ug/L 43.350 87 83-124
1,2-Dichlorobenzene ug/L 49.250 98 80-133
1,2-Dichloroethane ug/L 47.250 94 67-128
1,2-Dichloropropane ug/L 54.050 108 75-132
1,3-Dichlorobenzene ug/L 49.950 100 77-130
1,3-Dichloropropane ug/L 51.150 102 76-131
1,4-Dichlorobenzene ug/L 49.650 99 78-130
2,2-Dichloropropane ug/L 42.950 86 40-160
2-Butanone (MEK)ug/L 72.5100 73 61-144
2-Hexanone ug/L 71.2100 71 68-143
4-Methyl-2-pentanone (MIBK)ug/L 76.9100 77 72-135
Acetone ug/L 90.3100 90 48-146
Acetonitrile ug/L 430500 86 62-150
Acrolein ug/L 221250 88 24-160
Acrylonitrile ug/L 203250 81 40-160
Allyl chloride ug/L 52.050 104 66-137
Benzene ug/L 52.050 104 80-125
Bromochloromethane ug/L 47.250 94 71-125
Bromodichloromethane ug/L 51.650 103 78-124
Bromoform ug/L 39.950 80 71-128
Bromomethane ug/L 32.450 65 40-160
Carbon disulfide ug/L 48.150 96 50-160
Carbon tetrachloride ug/L 55.150 110 69-131
Chlorobenzene ug/L 49.650 99 81-122
Chloroethane ug/L 49.050 98 39-148
Chloroform ug/L 46.950 94 73-127
Chloromethane ug/L 43.350 87 44-146
Chloroprene ug/L 51.350 103 75-145
cis-1,2-Dichloroethene ug/L 51.650 103 74-124
cis-1,3-Dichloropropene ug/L 48.250 96 72-132
Dibromochloromethane ug/L 50.950 102 78-125
Dibromomethane ug/L 45.750 91 82-120
Dichlorodifluoromethane ug/L 39.650 79 34-157
Ethyl methacrylate ug/L 44.050 88 82-121
Ethylbenzene ug/L 50.350 101 79-121
Hexachloro-1,3-butadiene ug/L 52.350 105 72-131
Iodomethane ug/L 76.6100 77 39-154
Isobutanol ug/L 7561000 76 34-160
m&p-Xylene ug/L 98.6100 99 81-124
Methacrylonitrile ug/L 401500 80 74-134
Methyl methacrylate ug/L 40.8 L2508284-124
Methylene Chloride ug/L 49.350 99 64-133
Naphthalene ug/L 46.950 94 73-133
o-Xylene ug/L 49.350 99 79-131
Propionitrile ug/L 390500 78 73-140
Styrene ug/L 49.250 98 84-126
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 103 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2179165LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/L 50.650 101 78-122
Tetrahydrofuran ug/L 360500 72 69-148
Toluene ug/L 49.150 98 80-121
trans-1,2-Dichloroethene ug/L 50.150 100 71-127
trans-1,3-Dichloropropene ug/L 44.750 89 69-141
trans-1,4-Dichloro-2-butene ug/L 41.050 82 40-160
Trichloroethene ug/L 56.050 112 78-122
Trichlorofluoromethane ug/L 45.350 91 53-137
Vinyl acetate ug/L 84.1100 84 40-160
Vinyl chloride ug/L 51.250 102 58-137
Xylene (Total)ug/L 148150 99 81-126
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2179846MATRIX SPIKE SAMPLE:
MSSpike
Result
92368450004
1,1,1,2-Tetrachloroethane ug/L 18.620 93 70-130ND
1,1,1-Trichloroethane ug/L 23.920 119 70-130ND
1,1,2,2-Tetrachloroethane ug/L 16.220 81 70-130ND
1,1,2-Trichloroethane ug/L 18.520 92 70-130ND
1,1-Dichloroethane ug/L 23.220 113 70-1300.54J
1,1-Dichloroethene ug/L 25.820 129 70-166ND
1,1-Dichloropropene ug/L 21.820 109 70-130ND
1,2,3-Trichloropropane ug/L 16.420 82 70-130ND
1,2,4-Trichlorobenzene ug/L 21.820 109 70-130ND
1,2-Dibromo-3-chloropropane ug/L 14.920 74 70-130ND
1,2-Dibromoethane (EDB)ug/L 17.020 85 70-130ND
1,2-Dichlorobenzene ug/L 21.320 107 70-130ND
1,2-Dichloroethane ug/L 20.420 102 70-130ND
1,2-Dichloropropane ug/L 21.720 108 70-130ND
1,3-Dichlorobenzene ug/L 22.220 111 70-130ND
1,3-Dichloropropane ug/L 18.320 92 70-130ND
1,4-Dichlorobenzene ug/L 22.720 112 70-1300.37J
2,2-Dichloropropane ug/L 19.020 95 70-130ND
2-Butanone (MEK)ug/L 29.940 75 70-130ND
2-Hexanone ug/L 29.440 74 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 32.540 81 70-130ND
Acetone ug/L 36.540 91 70-130ND
Acetonitrile ug/L 193200 96 70-130ND
Acrolein ug/L 96.3100 96 70-130ND
Acrylonitrile ug/L 86.9100 87 70-130ND
Allyl chloride ug/L 25.320 126 70-130ND
Benzene ug/L 25.120 113 70-1482.5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
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Page 104 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2179846MATRIX SPIKE SAMPLE:
MSSpike
Result
92368450004
Bromochloromethane ug/L 21.120 105 70-130ND
Bromodichloromethane ug/L 21.220 106 70-130ND
Bromoform ug/L 16.520 82 70-130ND
Bromomethane ug/L 19.020 95 70-130ND
Carbon disulfide ug/L 24.120 121 70-130ND
Carbon tetrachloride ug/L 24.220 121 70-130ND
Chlorobenzene ug/L 22.320 111 70-146ND
Chloroethane ug/L 28.0 M12014070-130ND
Chloroform ug/L 22.520 113 70-130ND
Chloromethane ug/L 22.720 114 70-130ND
Chloroprene ug/L 21.620 108 70-130ND
cis-1,2-Dichloroethene ug/L 24.620 120 70-1300.66J
cis-1,3-Dichloropropene ug/L 18.320 91 70-130ND
Dibromochloromethane ug/L 17.620 88 70-130ND
Dibromomethane ug/L 19.320 96 70-130ND
Dichlorodifluoromethane ug/L 26.6 M12013370-130ND
Ethyl methacrylate ug/L 18.220 91 70-130ND
Ethylbenzene ug/L 22.420 112 70-130ND
Hexachloro-1,3-butadiene ug/L 23.820 119 70-130ND
Iodomethane ug/L 44.940 112 70-130ND
Isobutanol ug/L 374400 94 70-130ND
m&p-Xylene ug/L 45.140 113 70-130ND
Methacrylonitrile ug/L 156200 78 70-130ND
Methyl methacrylate ug/L 17.420 87 70-130ND
Methylene Chloride ug/L 26.820 128 70-1301.1
Naphthalene ug/L 19.220 96 70-130ND
o-Xylene ug/L 21.820 109 70-130ND
Propionitrile ug/L 169200 84 70-130ND
Styrene ug/L 21.120 106 70-130ND
Tetrachloroethene ug/L 24.020 113 70-1301.5
Tetrahydrofuran ug/L 175 M12005870-13059.1
Toluene ug/L 23.520 117 70-155ND
trans-1,2-Dichloroethene ug/L 25.020 125 70-130ND
trans-1,3-Dichloropropene ug/L 16.920 85 70-130ND
trans-1,4-Dichloro-2-butene ug/L 14.720 74 70-130ND
Trichloroethene ug/L 24.120 114 69-1511.3
Trichlorofluoromethane ug/L 27.8 M12013970-130ND
Vinyl acetate ug/L 29.840 75 70-130ND
Vinyl chloride ug/L 30.0 M12014370-1301.4
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%96 70-130
Toluene-d8 (S)%102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
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Page 105 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92368450001
2179167SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1-Dichloroethane ug/L NDND
1,1-Dichloroethene ug/L NDND
1,1-Dichloropropene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2,4-Trichlorobenzene ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,3-Dichlorobenzene ug/L NDND
1,3-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2,2-Dichloropropane ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Hexanone ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
Acetonitrile ug/L NDND
Acrolein ug/L NDND
Acrylonitrile ug/L NDND
Allyl chloride ug/L NDND
Benzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon disulfide ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
Chloroprene ug/L NDND
cis-1,2-Dichloroethene ug/L 0.73JND
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Dichlorodifluoromethane ug/L NDND
Ethyl methacrylate ug/L NDND
Ethylbenzene ug/L NDND
Hexachloro-1,3-butadiene ug/L NDND
Iodomethane ug/L NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
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Page 106 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92368450001
2179167SAMPLE DUPLICATE:
Isobutanol ug/L NDND
m&p-Xylene ug/L NDND
Methacrylonitrile ug/L NDND
Methyl methacrylate ug/L NDND
Methylene Chloride ug/L NDND
Naphthalene ug/L NDND
o-Xylene ug/L NDND
Propionitrile ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Tetrahydrofuran ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
trans-1,4-Dichloro-2-butene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl acetate ug/L NDND
Vinyl chloride ug/L NDND
Xylene (Total)ug/L NDND
1,2-Dichloroethane-d4 (S)%91 394
4-Bromofluorobenzene (S)%100 1101
Toluene-d8 (S)%108 1109
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 107 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
393369
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92368450013, 92368450014, 92368450015, 92368450016, 92368450017
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2181055
Associated Lab Samples:92368450013, 92368450014, 92368450015, 92368450016, 92368450017
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 01/03/18 15:53
1,1,1-Trichloroethane ug/L ND 1.0 01/03/18 15:53
1,1,2,2-Tetrachloroethane ug/L ND 1.0 01/03/18 15:53
1,1,2-Trichloroethane ug/L ND 1.0 01/03/18 15:53
1,1-Dichloroethane ug/L ND 1.0 01/03/18 15:53
1,1-Dichloroethene ug/L ND 1.0 01/03/18 15:53
1,1-Dichloropropene ug/L ND 1.0 01/03/18 15:53
1,2,3-Trichloropropane ug/L ND 1.0 01/03/18 15:53
1,2,4-Trichlorobenzene ug/L ND 1.0 01/03/18 15:53
1,2-Dibromo-3-chloropropane ug/L ND 2.0 01/03/18 15:53
1,2-Dibromoethane (EDB)ug/L ND 1.0 01/03/18 15:53
1,2-Dichlorobenzene ug/L ND 1.0 01/03/18 15:53
1,2-Dichloroethane ug/L ND 1.0 01/03/18 15:53
1,2-Dichloropropane ug/L ND 1.0 01/03/18 15:53
1,3-Dichlorobenzene ug/L ND 1.0 01/03/18 15:53
1,3-Dichloropropane ug/L ND 1.0 01/03/18 15:53
1,4-Dichlorobenzene ug/L ND 1.0 01/03/18 15:53
2,2-Dichloropropane ug/L ND 1.0 01/03/18 15:53
2-Butanone (MEK)ug/L ND 5.0 01/03/18 15:53
2-Hexanone ug/L ND 5.0 01/03/18 15:53
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 01/03/18 15:53
Acetone ug/L ND 25.0 01/03/18 15:53
Acetonitrile ug/L ND 50.0 01/03/18 15:53
Acrolein ug/L ND 10.0 01/03/18 15:53
Acrylonitrile ug/L ND 10.0 01/03/18 15:53
Allyl chloride ug/L ND 2.0 01/03/18 15:53
Benzene ug/L ND 1.0 01/03/18 15:53
Bromochloromethane ug/L ND 1.0 01/03/18 15:53
Bromodichloromethane ug/L ND 1.0 01/03/18 15:53
Bromoform ug/L ND 1.0 01/03/18 15:53
Bromomethane ug/L ND 2.0 01/03/18 15:53
Carbon disulfide ug/L ND 2.0 01/03/18 15:53
Carbon tetrachloride ug/L ND 1.0 01/03/18 15:53
Chlorobenzene ug/L ND 1.0 01/03/18 15:53
Chloroethane ug/L ND 1.0 01/03/18 15:53
Chloroform ug/L ND 1.0 01/03/18 15:53
Chloromethane ug/L ND 1.0 01/03/18 15:53
Chloroprene ug/L ND 5.0 01/03/18 15:53
cis-1,2-Dichloroethene ug/L ND 1.0 01/03/18 15:53
cis-1,3-Dichloropropene ug/L ND 1.0 01/03/18 15:53
Dibromochloromethane ug/L ND 1.0 01/03/18 15:53
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 108 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2181055
Associated Lab Samples:92368450013, 92368450014, 92368450015, 92368450016, 92368450017
Matrix:Water
Analyzed
Dibromomethane ug/L ND 1.0 01/03/18 15:53
Dichlorodifluoromethane ug/L ND 1.0 01/03/18 15:53
Ethyl methacrylate ug/L ND 1.0 01/03/18 15:53
Ethylbenzene ug/L ND 1.0 01/03/18 15:53
Hexachloro-1,3-butadiene ug/L ND 1.0 01/03/18 15:53
Iodomethane ug/L ND 5.0 01/03/18 15:53
Isobutanol ug/L ND 100 01/03/18 15:53
m&p-Xylene ug/L ND 2.0 01/03/18 15:53
Methacrylonitrile ug/L ND 10.0 01/03/18 15:53
Methyl methacrylate ug/L ND 2.0 01/03/18 15:53
Methylene Chloride ug/L ND 1.0 01/03/18 15:53
Naphthalene ug/L ND 1.0 01/03/18 15:53
o-Xylene ug/L ND 1.0 01/03/18 15:53
Propionitrile ug/L ND 20.0 01/03/18 15:53
Styrene ug/L ND 1.0 01/03/18 15:53
Tetrachloroethene ug/L ND 1.0 01/03/18 15:53
Tetrahydrofuran ug/L ND 10.0 01/03/18 15:53
Toluene ug/L ND 1.0 01/03/18 15:53
trans-1,2-Dichloroethene ug/L ND 1.0 01/03/18 15:53
trans-1,3-Dichloropropene ug/L ND 1.0 01/03/18 15:53
trans-1,4-Dichloro-2-butene ug/L ND 1.0 01/03/18 15:53
Trichloroethene ug/L ND 1.0 01/03/18 15:53
Trichlorofluoromethane ug/L ND 1.0 01/03/18 15:53
Vinyl acetate ug/L ND 2.0 01/03/18 15:53
Vinyl chloride ug/L ND 1.0 01/03/18 15:53
Xylene (Total)ug/L ND 1.0 01/03/18 15:53
1,2-Dichloroethane-d4 (S)%96 70-130 01/03/18 15:53
4-Bromofluorobenzene (S)%100 70-130 01/03/18 15:53
Toluene-d8 (S)%110 70-130 01/03/18 15:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2181056LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 45.250 90 80-125
1,1,1-Trichloroethane ug/L 50.550 101 71-129
1,1,2,2-Tetrachloroethane ug/L 43.750 87 79-124
1,1,2-Trichloroethane ug/L 48.650 97 85-125
1,1-Dichloroethane ug/L 47.550 95 73-126
1,1-Dichloroethene ug/L 47.950 96 66-135
1,1-Dichloropropene ug/L 46.150 92 74-135
1,2,3-Trichloropropane ug/L 45.450 91 75-130
1,2,4-Trichlorobenzene ug/L 51.850 104 75-134
1,2-Dibromo-3-chloropropane ug/L 38.250 76 71-133
1,2-Dibromoethane (EDB)ug/L 44.950 90 83-124
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
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Huntersville, NC 28078
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Page 109 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2181056LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichlorobenzene ug/L 49.050 98 80-133
1,2-Dichloroethane ug/L 46.650 93 67-128
1,2-Dichloropropane ug/L 51.950 104 75-132
1,3-Dichlorobenzene ug/L 49.450 99 77-130
1,3-Dichloropropane ug/L 52.250 104 76-131
1,4-Dichlorobenzene ug/L 48.850 98 78-130
2,2-Dichloropropane ug/L 44.450 89 40-160
2-Butanone (MEK)ug/L 79.8100 80 61-144
2-Hexanone ug/L 82.4100 82 68-143
4-Methyl-2-pentanone (MIBK)ug/L 84.2100 84 72-135
Acetone ug/L 101100 101 48-146
Acetonitrile ug/L 421500 84 62-150
Acrolein ug/L 238250 95 24-160
Acrylonitrile ug/L 211250 84 40-160
Allyl chloride ug/L 46.750 93 66-137
Benzene ug/L 49.650 99 80-125
Bromochloromethane ug/L 45.550 91 71-125
Bromodichloromethane ug/L 49.950 100 78-124
Bromoform ug/L 42.150 84 71-128
Bromomethane ug/L 37.650 75 40-160
Carbon disulfide ug/L 47.350 95 50-160
Carbon tetrachloride ug/L 51.650 103 69-131
Chlorobenzene ug/L 48.950 98 81-122
Chloroethane ug/L 49.350 99 39-148
Chloroform ug/L 45.250 90 73-127
Chloromethane ug/L 46.050 92 44-146
Chloroprene ug/L 47.950 96 75-145
cis-1,2-Dichloroethene ug/L 48.850 98 74-124
cis-1,3-Dichloropropene ug/L 46.950 94 72-132
Dibromochloromethane ug/L 50.850 102 78-125
Dibromomethane ug/L 45.750 91 82-120
Dichlorodifluoromethane ug/L 46.450 93 34-157
Ethyl methacrylate ug/L 46.750 93 82-121
Ethylbenzene ug/L 49.750 99 79-121
Hexachloro-1,3-butadiene ug/L 50.650 101 72-131
Iodomethane ug/L 79.6100 80 39-154
Isobutanol ug/L 7691000 77 34-160
m&p-Xylene ug/L 97.7100 98 81-124
Methacrylonitrile ug/L 414500 83 74-134
Methyl methacrylate ug/L 43.250 86 84-124
Methylene Chloride ug/L 49.150 98 64-133
Naphthalene ug/L 49.850 100 73-133
o-Xylene ug/L 48.950 98 79-131
Propionitrile ug/L 393500 79 73-140
Styrene ug/L 49.750 99 84-126
Tetrachloroethene ug/L 49.950 100 78-122
Tetrahydrofuran ug/L 394500 79 69-148
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 110 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2181056LABORATORY CONTROL SAMPLE:
LCSSpike
Toluene ug/L 47.250 94 80-121
trans-1,2-Dichloroethene ug/L 47.550 95 71-127
trans-1,3-Dichloropropene ug/L 44.450 89 69-141
trans-1,4-Dichloro-2-butene ug/L 42.750 85 40-160
Trichloroethene ug/L 52.250 104 78-122
Trichlorofluoromethane ug/L 45.850 92 53-137
Vinyl acetate ug/L 87.2100 87 40-160
Vinyl chloride ug/L 51.950 104 58-137
Xylene (Total)ug/L 147150 98 81-126
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2181058MATRIX SPIKE SAMPLE:
MSSpike
Result
92368450014
1,1,1,2-Tetrachloroethane ug/L 18.420 92 70-130ND
1,1,1-Trichloroethane ug/L 22.220 111 70-130ND
1,1,2,2-Tetrachloroethane ug/L 18.620 93 70-130ND
1,1,2-Trichloroethane ug/L 20.120 101 70-130ND
1,1-Dichloroethane ug/L 21.220 106 70-130ND
1,1-Dichloroethene ug/L 22.920 114 70-166ND
1,1-Dichloropropene ug/L 20.820 104 70-130ND
1,2,3-Trichloropropane ug/L 19.620 98 70-130ND
1,2,4-Trichlorobenzene ug/L 21.520 108 70-130ND
1,2-Dibromo-3-chloropropane ug/L 16.920 84 70-130ND
1,2-Dibromoethane (EDB)ug/L 18.820 94 70-130ND
1,2-Dichlorobenzene ug/L 20.220 101 70-130ND
1,2-Dichloroethane ug/L 20.420 102 70-130ND
1,2-Dichloropropane ug/L 21.920 109 70-130ND
1,3-Dichlorobenzene ug/L 20.820 104 70-130ND
1,3-Dichloropropane ug/L 20.620 103 70-130ND
1,4-Dichlorobenzene ug/L 20.620 103 70-130ND
2,2-Dichloropropane ug/L 18.220 91 70-130ND
2-Butanone (MEK)ug/L 34.240 86 70-130ND
2-Hexanone ug/L 36.140 90 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 38.740 97 70-130ND
Acetone ug/L 43.740 109 70-130ND
Acetonitrile ug/L 227200 113 70-130ND
Acrolein ug/L 109100 109 70-130ND
Acrylonitrile ug/L 103100 103 70-130ND
Allyl chloride ug/L 21.420 107 70-130ND
Benzene ug/L 21.720 109 70-148ND
Bromochloromethane ug/L 20.520 102 70-130ND
Bromodichloromethane ug/L 21.220 106 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 111 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2181058MATRIX SPIKE SAMPLE:
MSSpike
Result
92368450014
Bromoform ug/L 17.320 86 70-130ND
Bromomethane ug/L 18.520 92 70-130ND
Carbon disulfide ug/L 22.220 111 70-130ND
Carbon tetrachloride ug/L 23.020 115 70-130ND
Chlorobenzene ug/L 21.220 106 70-146ND
Chloroethane ug/L 23.520 117 70-130ND
Chloroform ug/L 21.720 108 70-130ND
Chloromethane ug/L 20.620 103 70-130ND
Chloroprene ug/L 21.120 105 70-130ND
cis-1,2-Dichloroethene ug/L 21.920 110 70-130ND
cis-1,3-Dichloropropene ug/L 18.120 91 70-130ND
Dibromochloromethane ug/L 18.620 93 70-130ND
Dibromomethane ug/L 20.220 101 70-130ND
Dichlorodifluoromethane ug/L 23.620 118 70-130ND
Ethyl methacrylate ug/L 20.520 102 70-130ND
Ethylbenzene ug/L 21.720 108 70-130ND
Hexachloro-1,3-butadiene ug/L 21.220 106 70-130ND
Iodomethane ug/L 38.640 97 70-130ND
Isobutanol ug/L 420400 105 70-130ND
m&p-Xylene ug/L 42.440 106 70-130ND
Methacrylonitrile ug/L 178200 89 70-130ND
Methyl methacrylate ug/L 19.520 98 70-130ND
Methylene Chloride ug/L 21.320 107 70-130ND
Naphthalene ug/L 20.220 101 70-130ND
o-Xylene ug/L 20.920 104 70-130ND
Propionitrile ug/L 197200 98 70-130ND
Styrene ug/L 19.920 99 70-130ND
Tetrachloroethene ug/L 20.820 104 70-130ND
Tetrahydrofuran ug/L 184200 92 70-130ND
Toluene ug/L 21.520 108 70-155ND
trans-1,2-Dichloroethene ug/L 22.720 113 70-130ND
trans-1,3-Dichloropropene ug/L 17.520 88 70-130ND
trans-1,4-Dichloro-2-butene ug/L 18.020 90 70-130ND
Trichloroethene ug/L 22.820 114 69-151ND
Trichlorofluoromethane ug/L 21.820 109 70-130ND
Vinyl acetate ug/L 31.740 79 70-130ND
Vinyl chloride ug/L 25.620 128 70-130ND
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92368450013
2181057SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
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Page 112 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92368450013
2181057SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1-Dichloroethane ug/L NDND
1,1-Dichloroethene ug/L NDND
1,1-Dichloropropene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2,4-Trichlorobenzene ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,3-Dichlorobenzene ug/L NDND
1,3-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2,2-Dichloropropane ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Hexanone ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
Acetonitrile ug/L NDND
Acrolein ug/L NDND
Acrylonitrile ug/L NDND
Allyl chloride ug/L NDND
Benzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon disulfide ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
Chloroprene ug/L NDND
cis-1,2-Dichloroethene ug/L NDND
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Dichlorodifluoromethane ug/L NDND
Ethyl methacrylate ug/L NDND
Ethylbenzene ug/L NDND
Hexachloro-1,3-butadiene ug/L NDND
Iodomethane ug/L NDND
Isobutanol ug/L NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
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9800 Kincey Ave. Suite 100
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Page 113 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92368450013
2181057SAMPLE DUPLICATE:
m&p-Xylene ug/L NDND
Methacrylonitrile ug/L NDND
Methyl methacrylate ug/L NDND
Methylene Chloride ug/L NDND
Naphthalene ug/L NDND
o-Xylene ug/L NDND
Propionitrile ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Tetrahydrofuran ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
trans-1,4-Dichloro-2-butene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl acetate ug/L NDND
Vinyl chloride ug/L NDND
Xylene (Total)ug/L NDND
1,2-Dichloroethane-d4 (S)%93 295
4-Bromofluorobenzene (S)%101 398
Toluene-d8 (S)%111 0111
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 114 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
392784
EPA 3510
EPA 8081
8081A GCS Pesticides
Associated Lab Samples:92368450002, 92368450003, 92368450004, 92368450005, 92368450006, 92368450007, 92368450008,92368450009, 92368450010, 92368450011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2178400
Associated Lab Samples:92368450002, 92368450003, 92368450004, 92368450005, 92368450006, 92368450007, 92368450008,92368450009, 92368450010, 92368450011
Matrix:Water
Analyzed
4,4'-DDD ug/L ND 0.050 01/02/18 18:38
4,4'-DDE ug/L ND 0.050 01/02/18 18:38
4,4'-DDT ug/L ND 0.050 01/02/18 18:38
Aldrin ug/L ND 0.050 01/02/18 18:38
alpha-BHC ug/L ND 0.050 01/02/18 18:38
beta-BHC ug/L ND 0.050 01/02/18 18:38
Chlordane (Technical)ug/L ND 0.20 01/02/18 18:38
delta-BHC ug/L ND 0.050 01/02/18 18:38
Dieldrin ug/L ND 0.050 01/02/18 18:38
Endosulfan I ug/L ND 0.050 01/02/18 18:38
Endosulfan II ug/L ND 0.050 01/02/18 18:38
Endosulfan sulfate ug/L ND 0.050 01/02/18 18:38
Endrin ug/L ND 0.050 01/02/18 18:38
Endrin aldehyde ug/L ND 0.050 01/02/18 18:38
gamma-BHC (Lindane)ug/L ND 0.050 01/02/18 18:38
Heptachlor ug/L ND 0.050 01/02/18 18:38
Heptachlor epoxide ug/L ND 0.050 01/02/18 18:38
Methoxychlor ug/L ND 0.15 01/02/18 18:38
Toxaphene ug/L ND 0.20 01/02/18 18:38
Decachlorobiphenyl (S)%93 20-130 01/02/18 18:38
Tetrachloro-m-xylene (S)%86 20-130 01/02/18 18:38
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2178401LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2178402
4,4'-DDD ug/L 0.22.25 88 20-150900.22 2 30
4,4'-DDE ug/L 0.21.25 87 20-150880.22 1 30
4,4'-DDT ug/L 0.22.25 87 20-150880.22 2 30
Aldrin ug/L 0.20.25 82 20-150610.15 29 30
alpha-BHC ug/L 0.20 R1.25 80 20-150520.13 42 30
beta-BHC ug/L 0.18.25 72 20-150720.18 0 30
delta-BHC ug/L 0.22.25 89 20-150860.21 3 30
Dieldrin ug/L 0.21.25 85 20-150850.21 1 30
Endosulfan I ug/L 0.21.25 86 20-150830.21 4 30
Endosulfan II ug/L 0.22.25 89 20-150910.23 2 30
Endosulfan sulfate ug/L 0.23.25 91 20-150930.23 2 30
Endrin ug/L 0.22.25 89 20-150890.22 0 30
Endrin aldehyde ug/L 0.19.25 76 20-150700.17 8 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 115 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2178401LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2178402
gamma-BHC (Lindane)ug/L 0.20.25 81 20-150630.16 25 30
Heptachlor ug/L 0.19 R1.25 75 20-150540.13 33 30
Heptachlor epoxide ug/L 0.22.25 87 20-150790.20 10 30
Methoxychlor ug/L 0.65.74 88 20-150900.67 2 30
Decachlorobiphenyl (S)%89 20-13089
Tetrachloro-m-xylene (S)%88 20-13044
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 116 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
392886
EPA 3510
EPA 8081
8081A GCS Pesticides
Associated Lab Samples:92368450013, 92368450014, 92368450015, 92368450016, 92368450017
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2178894
Associated Lab Samples:92368450013, 92368450014, 92368450015, 92368450016, 92368450017
Matrix:Water
Analyzed
4,4'-DDD ug/L ND 0.050 01/02/18 23:01
4,4'-DDE ug/L ND 0.050 01/02/18 23:01
4,4'-DDT ug/L ND 0.050 01/02/18 23:01
Aldrin ug/L ND 0.050 01/02/18 23:01
alpha-BHC ug/L ND 0.050 01/02/18 23:01
beta-BHC ug/L ND 0.050 01/02/18 23:01
Chlordane (Technical)ug/L ND 0.20 01/02/18 23:01
delta-BHC ug/L ND 0.050 01/02/18 23:01
Dieldrin ug/L ND 0.050 01/02/18 23:01
Endosulfan I ug/L ND 0.050 01/02/18 23:01
Endosulfan II ug/L ND 0.050 01/02/18 23:01
Endosulfan sulfate ug/L ND 0.050 01/02/18 23:01
Endrin ug/L ND 0.050 01/02/18 23:01
Endrin aldehyde ug/L ND 0.050 01/02/18 23:01
gamma-BHC (Lindane)ug/L ND 0.050 01/02/18 23:01
Heptachlor ug/L ND 0.050 01/02/18 23:01
Heptachlor epoxide ug/L ND 0.050 01/02/18 23:01
Methoxychlor ug/L ND 0.15 01/02/18 23:01
Toxaphene ug/L ND 0.20 01/02/18 23:01
Decachlorobiphenyl (S)%88 20-130 01/02/18 23:01
Tetrachloro-m-xylene (S)%98 20-130 01/02/18 23:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2178895LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2178896
4,4'-DDD ug/L 0.23.25 92 20-1501010.25 9 30
4,4'-DDE ug/L 0.22.25 89 20-150980.24 10 30
4,4'-DDT ug/L 0.23.25 92 20-1501000.25 9 30
Aldrin ug/L 0.21.25 84 20-150920.23 9 30
alpha-BHC ug/L 0.21.25 83 20-150920.23 10 30
beta-BHC ug/L 0.18.25 73 20-150770.19 6 30
delta-BHC ug/L 0.23.25 92 20-150960.24 5 30
Dieldrin ug/L 0.22.25 90 20-150990.25 9 30
Endosulfan I ug/L 0.22.25 88 20-150970.24 9 30
Endosulfan II ug/L 0.23.25 93 20-1501020.25 9 30
Endosulfan sulfate ug/L 0.24.25 95 20-1501030.26 8 30
Endrin ug/L 0.23.25 92 20-1501010.25 10 30
Endrin aldehyde ug/L 0.21.25 85 20-150910.23 8 30
gamma-BHC (Lindane)ug/L 0.21.25 84 20-150930.23 10 30
Heptachlor ug/L 0.20.25 79 20-150870.22 9 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 117 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2178895LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2178896
Heptachlor epoxide ug/L 0.22.25 87 20-150960.24 9 30
Methoxychlor ug/L 0.70.74 94 20-1501020.76 8 30
Decachlorobiphenyl (S)%98 20-130104
Tetrachloro-m-xylene (S)%88 20-13096
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 118 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
392785
EPA 3510
EPA 8082
8082 GCS PCB
Associated Lab Samples:92368450002, 92368450003, 92368450004, 92368450005, 92368450006, 92368450007, 92368450008,92368450009, 92368450010, 92368450011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2178404
Associated Lab Samples:92368450002, 92368450003, 92368450004, 92368450005, 92368450006, 92368450007, 92368450008,92368450009, 92368450010, 92368450011
Matrix:Water
Analyzed
PCB-1016 (Aroclor 1016)ug/L ND 0.50 01/02/18 16:57
PCB-1221 (Aroclor 1221)ug/L ND 0.50 01/02/18 16:57
PCB-1232 (Aroclor 1232)ug/L ND 0.50 01/02/18 16:57
PCB-1242 (Aroclor 1242)ug/L ND 0.50 01/02/18 16:57
PCB-1248 (Aroclor 1248)ug/L ND 0.50 01/02/18 16:57
PCB-1254 (Aroclor 1254)ug/L ND 0.50 01/02/18 16:57
PCB-1260 (Aroclor 1260)ug/L ND 0.50 01/02/18 16:57
Decachlorobiphenyl (S)%85 10-132 01/02/18 16:57
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2178405LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2178406
PCB-1016 (Aroclor 1016)ug/L 4.25 84 50-150834.1 2 30
PCB-1260 (Aroclor 1260)ug/L 4.35 85 50-150864.3 1 30
Decachlorobiphenyl (S)%119 10-132116
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 119 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
392887
EPA 3510
EPA 8082
8082 GCS PCB
Associated Lab Samples:92368450013, 92368450014, 92368450015, 92368450016, 92368450017
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2178897
Associated Lab Samples:92368450013, 92368450014, 92368450015, 92368450016, 92368450017
Matrix:Water
Analyzed
PCB-1016 (Aroclor 1016)ug/L ND 0.50 01/02/18 18:00
PCB-1221 (Aroclor 1221)ug/L ND 0.50 01/02/18 18:00
PCB-1232 (Aroclor 1232)ug/L ND 0.50 01/02/18 18:00
PCB-1242 (Aroclor 1242)ug/L ND 0.50 01/02/18 18:00
PCB-1248 (Aroclor 1248)ug/L ND 0.50 01/02/18 18:00
PCB-1254 (Aroclor 1254)ug/L ND 0.50 01/02/18 18:00
PCB-1260 (Aroclor 1260)ug/L ND 0.50 01/02/18 18:00
Decachlorobiphenyl (S)%85 10-132 01/02/18 18:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2178898LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2178899
PCB-1016 (Aroclor 1016)ug/L 4.65 93 50-150834.1 12 30
PCB-1260 (Aroclor 1260)ug/L 4.65 93 50-150854.2 9 30
Decachlorobiphenyl (S)%125 10-132114
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 120 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
392786
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92368450003, 92368450004, 92368450005, 92368450006, 92368450007, 92368450008, 92368450009,92368450010, 92368450011, 92368450012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2178407
Associated Lab Samples:92368450003, 92368450004, 92368450005, 92368450006, 92368450007, 92368450008, 92368450009,92368450010, 92368450011, 92368450012
Matrix:Water
Analyzed
1,2,4,5-Tetrachlorobenzene ug/L ND 10.0 01/02/18 13:14
1,3,5-Trinitrobenzene ug/L ND 10.0 01/02/18 13:14
1,3-Dinitrobenzene ug/L ND 20.0 01/02/18 13:14
1,4-Naphthoquinone ug/L ND 5.0 01/02/18 13:14
1-Naphthalenamine ug/L ND 5.0 01/02/18 13:14
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 01/02/18 13:14
2,3,4,6-Tetrachlorophenol ug/L ND 10.0 01/02/18 13:14
2,4,5-Trichlorophenol ug/L ND 10.0 01/02/18 13:14
2,4,6-Trichlorophenol ug/L ND 10.0 01/02/18 13:14
2,4-Dichlorophenol ug/L ND 10.0 01/02/18 13:14
2,4-Dimethylphenol ug/L ND 10.0 01/02/18 13:14
2,4-Dinitrophenol ug/L ND 50.0 01/02/18 13:14
2,4-Dinitrotoluene ug/L ND 10.0 01/02/18 13:14
2,6-Dichlorophenol ug/L ND 10.0 01/02/18 13:14
2,6-Dinitrotoluene ug/L ND 10.0 01/02/18 13:14
2-Acetylaminofluorene ug/L ND 20.0 01/02/18 13:14
2-Chloronaphthalene ug/L ND 10.0 01/02/18 13:14
2-Chlorophenol ug/L ND 10.0 01/02/18 13:14
2-Methylnaphthalene ug/L ND 10.0 01/02/18 13:14
2-Methylphenol(o-Cresol)ug/L ND 10.0 01/02/18 13:14
2-Naphthalenamine ug/L ND 5.0 01/02/18 13:14
2-Nitroaniline ug/L ND 50.0 01/02/18 13:14
2-Nitrophenol ug/L ND 10.0 01/02/18 13:14
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 01/02/18 13:14
3,3'-Dichlorobenzidine ug/L ND 20.0 01/02/18 13:14
3,3'-Dimethylbenzidine ug/L ND 10.0 01/02/18 13:14
3-Methylcholanthrene ug/L ND 10.0 01/02/18 13:14
3-Nitroaniline ug/L ND 50.0 01/02/18 13:14
4,6-Dinitro-2-methylphenol ug/L ND 20.0 01/02/18 13:14
4-Aminobiphenyl ug/L ND 10.0 01/02/18 13:14
4-Bromophenylphenyl ether ug/L ND 10.0 01/02/18 13:14
4-Chloro-3-methylphenol ug/L ND 20.0 01/02/18 13:14
4-Chloroaniline ug/L ND 20.0 01/02/18 13:14
4-Chlorophenylphenyl ether ug/L ND 10.0 01/02/18 13:14
4-Nitroaniline ug/L ND 20.0 01/02/18 13:14
4-Nitrophenol ug/L ND 50.0 01/02/18 13:14
5-Nitro-o-toluidine ug/L ND 10.0 01/02/18 13:14
7,12-Dimethylbenz(a)anthracene ug/L ND 10.0 01/02/18 13:14
Acenaphthene ug/L ND 10.0 01/02/18 13:14
Acenaphthylene ug/L ND 10.0 01/02/18 13:14
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 121 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2178407
Associated Lab Samples:92368450003, 92368450004, 92368450005, 92368450006, 92368450007, 92368450008, 92368450009,92368450010, 92368450011, 92368450012
Matrix:Water
Analyzed
Acetophenone ug/L ND 10.0 01/02/18 13:14
Anthracene ug/L ND 10.0 01/02/18 13:14
Benzo(a)anthracene ug/L ND 10.0 01/02/18 13:14
Benzo(a)pyrene ug/L ND 10.0 01/02/18 13:14
Benzo(b)fluoranthene ug/L ND 10.0 01/02/18 13:14
Benzo(g,h,i)perylene ug/L ND 10.0 01/02/18 13:14
Benzo(k)fluoranthene ug/L ND 10.0 01/02/18 13:14
Benzyl alcohol ug/L ND 20.0 01/02/18 13:14
bis(2-Chloroethoxy)methane ug/L ND 10.0 01/02/18 13:14
bis(2-Chloroethyl) ether ug/L ND 10.0 01/02/18 13:14
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 01/02/18 13:14
Butylbenzylphthalate ug/L ND 10.0 01/02/18 13:14
Chlorobenzilate ug/L ND 10.0 01/02/18 13:14
Chrysene ug/L ND 10.0 01/02/18 13:14
Di-n-butylphthalate ug/L ND 10.0 01/02/18 13:14
Di-n-octylphthalate ug/L ND 10.0 01/02/18 13:14
Diallate ug/L ND 10.0 01/02/18 13:14
Dibenz(a,h)anthracene ug/L ND 10.0 01/02/18 13:14
Dibenzofuran ug/L ND 10.0 01/02/18 13:14
Diethylphthalate ug/L ND 10.0 01/02/18 13:14
Dimethoate ug/L ND 10.0 01/02/18 13:14
Dimethylphthalate ug/L ND 10.0 01/02/18 13:14
Diphenylamine ug/L ND 10.0 01/02/18 13:14
Disulfoton ug/L ND 10.0 01/02/18 13:14
Ethyl methanesulfonate ug/L ND 20.0 01/02/18 13:14
Famphur ug/L ND 10.0 01/02/18 13:14
Fluoranthene ug/L ND 10.0 01/02/18 13:14
Fluorene ug/L ND 10.0 01/02/18 13:14
Hexachlorobenzene ug/L ND 10.0 01/02/18 13:14
Hexachlorocyclopentadiene ug/L ND 10.0 01/02/18 13:14
Hexachloroethane ug/L ND 10.0 01/02/18 13:14
Hexachlorophene ug/L ND 100 01/02/18 13:14
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 01/02/18 13:14
Isodrin ug/L ND 20.0 01/02/18 13:14
Isophorone ug/L ND 10.0 01/02/18 13:14
Isosafrole ug/L ND 10.0 01/02/18 13:14
Kepone ug/L ND 10.0 01/02/18 13:14
Methapyrilene ug/L ND 50.0 01/02/18 13:14
Methyl methanesulfonate ug/L ND 5.0 01/02/18 13:14
Methyl parathion ug/L ND 10.0 01/02/18 13:14
N-Nitroso-di-n-butylamine ug/L ND 10.0 01/02/18 13:14
N-Nitroso-di-n-propylamine ug/L ND 10.0 01/02/18 13:14
N-Nitrosodiethylamine ug/L ND 20.0 01/02/18 13:14
N-Nitrosodimethylamine ug/L ND 10.0 01/02/18 13:14
N-Nitrosodiphenylamine ug/L ND 10.0 01/02/18 13:14
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 122 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2178407
Associated Lab Samples:92368450003, 92368450004, 92368450005, 92368450006, 92368450007, 92368450008, 92368450009,92368450010, 92368450011, 92368450012
Matrix:Water
Analyzed
N-Nitrosomethylethylamine ug/L ND 10.0 01/02/18 13:14
N-Nitrosopiperidine ug/L ND 20.0 01/02/18 13:14
N-Nitrosopyrrolidine ug/L ND 10.0 01/02/18 13:14
Nitrobenzene ug/L ND 10.0 01/02/18 13:14
O,O,O-Triethylphosphorothioate ug/L ND 10.0 01/02/18 13:14
O-Toluidine ug/L ND 10.0 01/02/18 13:14
P-Dimethylaminoazobenzene ug/L ND 5.0 01/02/18 13:14
p-Phenylenediamine ug/L ND 10.0 01/02/18 13:14
Parathion (Ethyl parathion)ug/L ND 10.0 01/02/18 13:14
Pentachlorobenzene ug/L ND 10.0 01/02/18 13:14
Pentachloronitrobenzene ug/L ND 20.0 01/02/18 13:14
Pentachlorophenol ug/L ND 25.0 01/02/18 13:14
Phenacetin ug/L ND 20.0 01/02/18 13:14
Phenanthrene ug/L ND 10.0 01/02/18 13:14
Phenol ug/L ND 10.0 01/02/18 13:14
Phorate ug/L ND 10.0 01/02/18 13:14
Pronamide ug/L ND 10.0 01/02/18 13:14
Pyrene ug/L ND 10.0 01/02/18 13:14
Safrole ug/L ND 10.0 01/02/18 13:14
Thionazin ug/L ND 20.0 01/02/18 13:14
2,4,6-Tribromophenol (S)%16 27-110 S001/02/18 13:14
2-Fluorobiphenyl (S)%57 27-110 01/02/18 13:14
2-Fluorophenol (S)%9 12-110 S001/02/18 13:14
Nitrobenzene-d5 (S)%59 21-110 01/02/18 13:14
Phenol-d6 (S)%12 10-110 01/02/18 13:14
Terphenyl-d14 (S)%73 31-107 01/02/18 13:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2178408LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2178409
1,2,4,5-Tetrachlorobenzene ug/L 34.0 R1506816-1294924.4 33 30
1,3,5-Trinitrobenzene ug/L 26.7 L2505355-1255929.7 11 30
1,3-Dinitrobenzene ug/L 41.050 82 30-1228441.8 2 30
1,4-Naphthoquinone ug/L 38.350 77 31-1207838.8 1 30
1-Naphthalenamine ug/L 26.750 53 37-1265828.9 8 30
2,2'-Oxybis(1-chloropropane)ug/L 31.6 R1506318-1203818.8 51 30
2,3,4,6-Tetrachlorophenol ug/L 90.250 180 54-27618089.9 0 30
2,4,5-Trichlorophenol ug/L 37.450 75 43-1137236.0 4 30
2,4,6-Trichlorophenol ug/L 37.950 76 42-1207035.0 8 30
2,4-Dichlorophenol ug/L 37.150 74 30-1205527.4 30 30
2,4-Dimethylphenol ug/L 35.5 R1507129-1115024.9 35 30
2,4-Dinitrophenol ug/L 215250 86 19-13291228 6 30
2,4-Dinitrotoluene ug/L 42.650 85 58-1288944.5 4 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 123 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2178408LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2178409
2,6-Dichlorophenol ug/L 42.4 R1508554-1286130.3 33 30
2,6-Dinitrotoluene ug/L 45.250 90 54-1298944.6 1 30
2-Acetylaminofluorene ug/L 38.1 L2507681-1608040.2 6 30
2-Chloronaphthalene ug/L 41.450 83 43-1176633.1 22 30
2-Chlorophenol ug/L 34.9 R1507037-1204120.5 52 30
2-Methylnaphthalene ug/L 36.150 72 33-1205326.6 30 30
2-Methylphenol(o-Cresol)ug/L 32.6 R1506531-1203517.3 61 30
2-Naphthalenamine ug/L 33.250 66 41-1367034.8 5 30
2-Nitroaniline ug/L 79.0100 79 48-1217979.4 0 30
2-Nitrophenol ug/L 38.4 R1507725-1165125.5 40 30
3&4-Methylphenol(m&p Cresol)ug/L 24.2 R1504823-1203417.0 35 30
3,3'-Dichlorobenzidine ug/L 83.8250 34 10-1543690.1 7 30
3,3'-Dimethylbenzidine ug/L 37.0 R11003710-1576060.3 48 30
3-Methylcholanthrene ug/L 42.450 85 65-1309246.0 8 30
3-Nitroaniline ug/L 82.4100 82 43-1158685.6 4 30
4,6-Dinitro-2-methylphenol ug/L 93.7100 94 44-12410099.5 6 30
4-Aminobiphenyl ug/L 27.450 55 21-1256532.4 17 30
4-Bromophenylphenyl ether ug/L 39.350 79 34-1138140.7 3 30
4-Chloro-3-methylphenol ug/L 76.4100 76 31-1107171.1 7 30
4-Chloroaniline ug/L 69.9100 70 20-1205454.5 25 30
4-Chlorophenylphenyl ether ug/L 37.750 75 34-1167336.3 4 30
4-Nitroaniline ug/L 87.9100 88 46-1288786.8 1 30
4-Nitrophenol ug/L 82.5250 33 11-1203793.0 12 30
5-Nitro-o-toluidine ug/L 45.150 90 78-1609145.7 1 30
7,12-Dimethylbenz(a)anthracene ug/L 41.650 83 47-1249346.6 11 30
Acenaphthene ug/L 38.350 77 48-1146934.3 11 30
Acenaphthylene ug/L 39.950 80 48-1127034.8 14 30
Acetophenone ug/L 39.5 R1507924-1204924.7 46 30
Anthracene ug/L 41.850 84 57-1188442.0 0 30
Benzo(a)anthracene ug/L 41.350 83 56-1218642.8 4 30
Benzo(a)pyrene ug/L 42.650 85 55-1279547.7 11 30
Benzo(b)fluoranthene ug/L 46.450 93 53-1289949.3 6 30
Benzo(g,h,i)perylene ug/L 44.250 88 54-1259346.3 5 30
Benzo(k)fluoranthene ug/L 42.750 85 51-1239245.8 7 30
Benzyl alcohol ug/L 62.3 R11006227-1203837.9 49 30
bis(2-Chloroethoxy)methane ug/L 37.9 R1507632-1205125.7 38 30
bis(2-Chloroethyl) ether ug/L 37.9 R1507633-1114622.8 50 30
bis(2-Ethylhexyl)phthalate ug/L 44.150 88 50-1459648.0 9 30
Butylbenzylphthalate ug/L 48.250 96 54-13810552.5 9 30
Chlorobenzilate ug/L 37.450 75 65-1328341.5 10 30
Chrysene ug/L 42.150 84 58-1278743.7 4 30
Di-n-butylphthalate ug/L 42.650 85 56-1258944.4 4 30
Di-n-octylphthalate ug/L 47.150 94 50-13411356.3 18 30
Diallate ug/L 41.450 83 47-1238442.2 2 30
Dibenz(a,h)anthracene ug/L 44.250 88 53-1298944.3 0 30
Dibenzofuran ug/L 38.750 77 45-1207336.3 6 30
Diethylphthalate ug/L 40.950 82 53-1208743.4 6 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
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Page 124 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2178408LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2178409
Dimethoate ug/L 43.050 86 57-1399346.7 8 30
Dimethylphthalate ug/L 42.150 84 55-1168542.3 0 30
Diphenylamine ug/L 39.950 80 42-1208040.1 1 30
Disulfoton ug/L 38.050 76 49-1568040.1 5 30
Ethyl methanesulfonate ug/L 40.9 R1508243-1204924.6 50 30
Famphur ug/L 90.9100 91 40-1609090.3 1 30
Fluoranthene ug/L 42.350 85 57-1258743.5 3 30
Fluorene ug/L 42.050 84 53-1187939.3 7 30
Hexachlorobenzene ug/L 42.550 85 49-1168442.1 1 30
Hexachlorocyclopentadiene ug/L 33.4 R1506726-1584220.8 46 30
Hexachloroethane ug/L 26.5 R1505330-1143417.1 43 30
Hexachlorophene ug/L 127 R15002510-13043215 51 30
Indeno(1,2,3-cd)pyrene ug/L 44.350 89 55-1289145.3 2 30
Isodrin ug/L 43.450 87 68-1298743.7 1 30
Isophorone ug/L 37.350 75 31-1185627.8 29 30
Isosafrole ug/L 39.750 79 48-1076633.0 19 30
Kepone ug/L 74.5 R11007410-124113113 41 30
Methapyrilene ug/L 16.0J L2503240-1605125.7J 30
Methyl methanesulfonate ug/L 89.9 L1,R15018025-11411356.4 46 30
Methyl parathion ug/L 48.450 97 58-13710250.9 5 30
N-Nitroso-di-n-butylamine ug/L 33.650 67 36-1155125.5 27 30
N-Nitroso-di-n-propylamine ug/L 40.2 R1508032-1195225.8 44 30
N-Nitrosodiethylamine ug/L 39.1 R1507847-1154723.4 50 30
N-Nitrosodimethylamine ug/L 24.7 R1504913-1202814.0 55 30
N-Nitrosodiphenylamine ug/L 39.950 80 43-1208040.1 1 30
N-Nitrosomethylethylamine ug/L 37.0 R1507439-1204522.5 49 30
N-Nitrosopiperidine ug/L 40.6 R1508143-1135829.2 33 30
N-Nitrosopyrrolidine ug/L 38.9 R1507832-1105225.8 40 30
Nitrobenzene ug/L 38.2 R1507633-1105025.1 41 30
O,O,O-Triethylphosphorothioate ug/L 37.6 L2,R1507551-1275024.8 41 30
O-Toluidine ug/L 34.6 R1506927-1204522.4 43 30
P-Dimethylaminoazobenzene ug/L 18.6100 19 10-1202120.6 10 30
p-Phenylenediamine ug/L 44.250 88 72-1439547.5 7 30
Parathion (Ethyl parathion)ug/L 40.750 81 56-1408642.8 5 30
Pentachlorobenzene ug/L 37.050 74 30-1377035.0 5 30
Pentachloronitrobenzene ug/L 51.250 102 70-12410452.0 2 30
Pentachlorophenol ug/L 80.0250 32 10-1373485.3 6 30
Phenacetin ug/L 45.150 90 60-1309447.2 4 30
Phenanthrene ug/L 41.150 82 57-1178341.3 1 30
Phenol ug/L 17.6 R1503510-1202110.3 52 30
Phorate ug/L 42.550 85 55-1268843.8 3 30
Pronamide ug/L 47.550 95 75-12410050.1 5 30
Pyrene ug/L 45.550 91 55-1229547.3 4 30
Safrole ug/L 36.2 R1507241-1205225.8 34 30
Thionazin ug/L 41.050 82 63-1378542.4 4 30
2,4,6-Tribromophenol (S)%85 27-11086
2-Fluorobiphenyl (S)%75 27-11057
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 125 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2178408LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2178409
2-Fluorophenol (S)%42 12-11023
Nitrobenzene-d5 (S)%78 21-11050
Phenol-d6 (S)%28 10-11016
Terphenyl-d14 (S)%83 31-10783
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 126 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
392890
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92368450013, 92368450014, 92368450015, 92368450016, 92368450017
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2178907
Associated Lab Samples:92368450013, 92368450014, 92368450015, 92368450016, 92368450017
Matrix:Water
Analyzed
1,2,4,5-Tetrachlorobenzene ug/L ND 10.0 01/03/18 16:21
1,3,5-Trinitrobenzene ug/L ND 10.0 01/03/18 16:21
1,3-Dinitrobenzene ug/L ND 20.0 01/03/18 16:21
1,4-Naphthoquinone ug/L ND 5.0 01/03/18 16:21
1-Naphthalenamine ug/L ND 5.0 01/03/18 16:21
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 01/03/18 16:21
2,3,4,6-Tetrachlorophenol ug/L ND 10.0 01/03/18 16:21
2,4,5-Trichlorophenol ug/L ND 10.0 01/03/18 16:21
2,4,6-Trichlorophenol ug/L ND 10.0 01/03/18 16:21
2,4-Dichlorophenol ug/L ND 10.0 01/03/18 16:21
2,4-Dimethylphenol ug/L ND 10.0 01/03/18 16:21
2,4-Dinitrophenol ug/L ND 50.0 01/03/18 16:21
2,4-Dinitrotoluene ug/L ND 10.0 01/03/18 16:21
2,6-Dichlorophenol ug/L ND 10.0 01/03/18 16:21
2,6-Dinitrotoluene ug/L ND 10.0 01/03/18 16:21
2-Acetylaminofluorene ug/L ND 20.0 01/03/18 16:21
2-Chloronaphthalene ug/L ND 10.0 01/03/18 16:21
2-Chlorophenol ug/L ND 10.0 01/03/18 16:21
2-Methylnaphthalene ug/L ND 10.0 01/03/18 16:21
2-Methylphenol(o-Cresol)ug/L ND 10.0 01/03/18 16:21
2-Naphthalenamine ug/L ND 5.0 01/03/18 16:21
2-Nitroaniline ug/L ND 50.0 01/03/18 16:21
2-Nitrophenol ug/L ND 10.0 01/03/18 16:21
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 01/03/18 16:21
3,3'-Dichlorobenzidine ug/L ND 20.0 01/03/18 16:21
3,3'-Dimethylbenzidine ug/L ND 10.0 01/03/18 16:21
3-Methylcholanthrene ug/L ND 10.0 01/03/18 16:21
3-Nitroaniline ug/L ND 50.0 01/03/18 16:21
4,6-Dinitro-2-methylphenol ug/L ND 20.0 01/03/18 16:21
4-Aminobiphenyl ug/L ND 10.0 01/03/18 16:21
4-Bromophenylphenyl ether ug/L ND 10.0 01/03/18 16:21
4-Chloro-3-methylphenol ug/L ND 20.0 01/03/18 16:21
4-Chloroaniline ug/L ND 20.0 01/03/18 16:21
4-Chlorophenylphenyl ether ug/L ND 10.0 01/03/18 16:21
4-Nitroaniline ug/L ND 20.0 01/03/18 16:21
4-Nitrophenol ug/L ND 50.0 01/03/18 16:21
5-Nitro-o-toluidine ug/L ND 10.0 01/03/18 16:21
7,12-Dimethylbenz(a)anthracene ug/L ND 10.0 01/03/18 16:21
Acenaphthene ug/L ND 10.0 01/03/18 16:21
Acenaphthylene ug/L ND 10.0 01/03/18 16:21
Acetophenone ug/L ND 10.0 01/03/18 16:21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 127 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2178907
Associated Lab Samples:92368450013, 92368450014, 92368450015, 92368450016, 92368450017
Matrix:Water
Analyzed
Anthracene ug/L ND 10.0 01/03/18 16:21
Benzo(a)anthracene ug/L ND 10.0 01/03/18 16:21
Benzo(a)pyrene ug/L ND 10.0 01/03/18 16:21
Benzo(b)fluoranthene ug/L ND 10.0 01/03/18 16:21
Benzo(g,h,i)perylene ug/L ND 10.0 01/03/18 16:21
Benzo(k)fluoranthene ug/L ND 10.0 01/03/18 16:21
Benzyl alcohol ug/L ND 20.0 01/03/18 16:21
bis(2-Chloroethoxy)methane ug/L ND 10.0 01/03/18 16:21
bis(2-Chloroethyl) ether ug/L ND 10.0 01/03/18 16:21
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 01/03/18 16:21
Butylbenzylphthalate ug/L ND 10.0 01/03/18 16:21
Chlorobenzilate ug/L ND 10.0 01/03/18 16:21
Chrysene ug/L ND 10.0 01/03/18 16:21
Di-n-butylphthalate ug/L ND 10.0 01/03/18 16:21
Di-n-octylphthalate ug/L ND 10.0 01/03/18 16:21
Diallate ug/L ND 10.0 01/03/18 16:21
Dibenz(a,h)anthracene ug/L ND 10.0 01/03/18 16:21
Dibenzofuran ug/L ND 10.0 01/03/18 16:21
Diethylphthalate ug/L ND 10.0 01/03/18 16:21
Dimethoate ug/L ND 10.0 01/03/18 16:21
Dimethylphthalate ug/L ND 10.0 01/03/18 16:21
Diphenylamine ug/L ND 10.0 01/03/18 16:21
Disulfoton ug/L ND 10.0 01/03/18 16:21
Ethyl methanesulfonate ug/L ND 20.0 01/03/18 16:21
Famphur ug/L ND 10.0 01/03/18 16:21
Fluoranthene ug/L ND 10.0 01/03/18 16:21
Fluorene ug/L ND 10.0 01/03/18 16:21
Hexachlorobenzene ug/L ND 10.0 01/03/18 16:21
Hexachlorocyclopentadiene ug/L ND 10.0 01/03/18 16:21
Hexachloroethane ug/L ND 10.0 01/03/18 16:21
Hexachlorophene ug/L ND 100 01/03/18 16:21
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 01/03/18 16:21
Isodrin ug/L ND 20.0 01/03/18 16:21
Isophorone ug/L ND 10.0 01/03/18 16:21
Isosafrole ug/L ND 10.0 01/03/18 16:21
Kepone ug/L ND 10.0 01/03/18 16:21
Methapyrilene ug/L ND 50.0 01/03/18 16:21
Methyl methanesulfonate ug/L ND 5.0 01/03/18 16:21
Methyl parathion ug/L ND 10.0 01/03/18 16:21
N-Nitroso-di-n-butylamine ug/L ND 10.0 01/03/18 16:21
N-Nitroso-di-n-propylamine ug/L ND 10.0 01/03/18 16:21
N-Nitrosodiethylamine ug/L ND 20.0 01/03/18 16:21
N-Nitrosodimethylamine ug/L ND 10.0 01/03/18 16:21
N-Nitrosodiphenylamine ug/L ND 10.0 01/03/18 16:21
N-Nitrosomethylethylamine ug/L ND 10.0 01/03/18 16:21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 128 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2178907
Associated Lab Samples:92368450013, 92368450014, 92368450015, 92368450016, 92368450017
Matrix:Water
Analyzed
N-Nitrosopiperidine ug/L ND 20.0 01/03/18 16:21
N-Nitrosopyrrolidine ug/L ND 10.0 01/03/18 16:21
Nitrobenzene ug/L ND 10.0 01/03/18 16:21
O,O,O-Triethylphosphorothioate ug/L ND 10.0 01/03/18 16:21
O-Toluidine ug/L ND 10.0 01/03/18 16:21
P-Dimethylaminoazobenzene ug/L ND 5.0 01/03/18 16:21
p-Phenylenediamine ug/L ND 10.0 01/03/18 16:21
Parathion (Ethyl parathion)ug/L ND 10.0 01/03/18 16:21
Pentachlorobenzene ug/L ND 10.0 01/03/18 16:21
Pentachloronitrobenzene ug/L ND 20.0 01/03/18 16:21
Pentachlorophenol ug/L ND 25.0 01/03/18 16:21
Phenacetin ug/L ND 20.0 01/03/18 16:21
Phenanthrene ug/L ND 10.0 01/03/18 16:21
Phenol ug/L ND 10.0 01/03/18 16:21
Phorate ug/L ND 10.0 01/03/18 16:21
Pronamide ug/L ND 10.0 01/03/18 16:21
Pyrene ug/L ND 10.0 01/03/18 16:21
Safrole ug/L ND 10.0 01/03/18 16:21
Thionazin ug/L ND 20.0 01/03/18 16:21
2,4,6-Tribromophenol (S)%79 27-110 01/03/18 16:21
2-Fluorobiphenyl (S)%65 27-110 01/03/18 16:21
2-Fluorophenol (S)%36 12-110 01/03/18 16:21
Nitrobenzene-d5 (S)%68 21-110 01/03/18 16:21
Phenol-d6 (S)%23 10-110 01/03/18 16:21
Terphenyl-d14 (S)%86 31-107 01/03/18 16:21
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2178908LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2178909
1,2,4,5-Tetrachlorobenzene ug/L 29.950 60 16-1297437.1 21 30
1,3,5-Trinitrobenzene ug/L 27.9 L2505655-1254421.9 24 30
1,3-Dinitrobenzene ug/L 34.850 70 30-1226733.4 4 30
1,4-Naphthoquinone ug/L 37.750 75 31-1207135.7 5 30
1-Naphthalenamine ug/L 22.050 44 37-1264120.5 7 30
2,2'-Oxybis(1-chloropropane)ug/L 24.050 48 18-1205527.4 13 30
2,3,4,6-Tetrachlorophenol ug/L 73.150 146 54-27611858.8 22 30
2,4,5-Trichlorophenol ug/L 36.150 72 43-1136029.8 19 30
2,4,6-Trichlorophenol ug/L 34.550 69 42-1206834.0 2 30
2,4-Dichlorophenol ug/L 32.650 65 30-1205929.7 9 30
2,4-Dimethylphenol ug/L 30.850 62 29-1115829.1 6 30
2,4-Dinitrophenol ug/L 146 R12505919-13243107 31 30
2,4-Dinitrotoluene ug/L 37.150 74 58-1286532.7 12 30
2,6-Dichlorophenol ug/L 35.950 72 54-1286934.7 3 30
2,6-Dinitrotoluene ug/L 40.450 81 54-1297738.3 6 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 129 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2178908LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2178909
2-Acetylaminofluorene ug/L 40.7 L2508181-1608039.8 2 30
2-Chloronaphthalene ug/L 37.950 76 43-1178442.0 10 30
2-Chlorophenol ug/L 30.950 62 37-1205828.8 7 30
2-Methylnaphthalene ug/L 33.650 67 33-1206331.6 6 30
2-Methylphenol(o-Cresol)ug/L 29.850 60 31-1205125.7 15 30
2-Naphthalenamine ug/L 23.750 47 41-1364823.8 0 30
2-Nitroaniline ug/L 67.9100 68 48-1216363.2 7 30
2-Nitrophenol ug/L 33.150 66 25-1166934.7 5 30
3&4-Methylphenol(m&p Cresol)ug/L 21.150 42 23-1203316.5 25 30
3,3'-Dichlorobenzidine ug/L 82.2250 33 10-1543381.9 0 30
3,3'-Dimethylbenzidine ug/L 47.0100 47 10-1574948.9 4 30
3-Methylcholanthrene ug/L 43.650 87 65-1309145.4 4 30
3-Nitroaniline ug/L 68.4100 68 43-1156059.9 13 30
4,6-Dinitro-2-methylphenol ug/L 81.9100 82 44-1247272.4 12 30
4-Aminobiphenyl ug/L 28.450 57 21-1255929.3 3 30
4-Bromophenylphenyl ether ug/L 42.650 85 34-1138642.8 1 30
4-Chloro-3-methylphenol ug/L 71.9 R11007231-1105251.5 33 30
4-Chloroaniline ug/L 58.7100 59 20-1205150.6 15 30
4-Chlorophenylphenyl ether ug/L 36.850 74 34-1166633.2 10 30
4-Nitroaniline ug/L 71.7100 72 46-1285656.3 24 30
4-Nitrophenol ug/L 65.5250 26 11-1201846.1J 30
5-Nitro-o-toluidine ug/L 35.8 L2507278-1606431.9 12 30
7,12-Dimethylbenz(a)anthracene ug/L 42.150 84 47-1249246.2 9 30
Acenaphthene ug/L 36.650 73 48-1147135.7 2 30
Acenaphthylene ug/L 36.350 73 48-1127336.4 0 30
Acetophenone ug/L 35.050 70 24-1206130.5 14 30
Anthracene ug/L 40.650 81 57-1188040.1 1 30
Benzo(a)anthracene ug/L 40.250 80 56-1218542.3 5 30
Benzo(a)pyrene ug/L 39.650 79 55-1278642.9 8 30
Benzo(b)fluoranthene ug/L 43.650 87 53-1289145.5 4 30
Benzo(g,h,i)perylene ug/L 44.450 89 54-1258944.3 0 30
Benzo(k)fluoranthene ug/L 42.150 84 51-1239044.9 6 30
Benzyl alcohol ug/L 53.8100 54 27-1204949.3 9 30
bis(2-Chloroethoxy)methane ug/L 35.150 70 32-1207034.9 1 30
bis(2-Chloroethyl) ether ug/L 31.850 64 33-1116331.5 1 30
bis(2-Ethylhexyl)phthalate ug/L 45.250 90 50-1459447.0 4 30
Butylbenzylphthalate ug/L 48.050 96 54-1389949.3 3 30
Chlorobenzilate ug/L 37.450 75 65-1328241.2 10 30
Chrysene ug/L 40.850 82 58-1278442.2 3 30
Di-n-butylphthalate ug/L 42.050 84 56-1258341.3 2 30
Di-n-octylphthalate ug/L 51.150 102 50-13411658.2 13 30
Diallate ug/L 45.150 90 47-1239246.2 3 30
Dibenz(a,h)anthracene ug/L 44.250 88 53-1298944.6 1 30
Dibenzofuran ug/L 35.850 72 45-1207135.6 1 30
Diethylphthalate ug/L 37.750 75 53-1206934.5 9 30
Dimethoate ug/L 40.450 81 57-1397336.7 10 30
Dimethylphthalate ug/L 38.950 78 55-1167436.8 5 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
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Page 130 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2178908LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2178909
Diphenylamine ug/L 40.550 81 42-1208140.6 0 30
Disulfoton ug/L 40.050 80 49-1568140.4 1 30
Ethyl methanesulfonate ug/L 35.050 70 43-1206633.0 6 30
Famphur ug/L 70.8100 71 40-1608180.8 13 30
Fluoranthene ug/L 40.350 81 57-1257236.0 11 30
Fluorene ug/L 38.850 78 53-1187135.4 9 30
Hexachlorobenzene ug/L 42.850 86 49-1168743.5 2 30
Hexachlorocyclopentadiene ug/L 30.150 60 26-1587437.1 21 30
Hexachloroethane ug/L 26.750 53 30-1145025.0 7 30
Hexachlorophene ug/L 153500 31 10-13026129 17 30
Indeno(1,2,3-cd)pyrene ug/L 43.550 87 55-1288944.4 2 30
Isodrin ug/L 43.750 87 68-1298442.1 4 30
Isophorone ug/L 33.350 67 31-1186633.2 0 30
Isosafrole ug/L 37.150 74 48-1078240.8 9 30
Kepone ug/L 106100 106 10-124112112 5 30
Methapyrilene ug/L 22.1J50 44 40-1604422.2J 30
Methyl methanesulfonate ug/L 79.5 L15015925-11415677.8 2 30
Methyl parathion ug/L 46.850 94 58-1378843.8 7 30
N-Nitroso-di-n-butylamine ug/L 29.050 58 36-1155426.8 8 30
N-Nitroso-di-n-propylamine ug/L 36.250 72 32-1196030.1 18 30
N-Nitrosodiethylamine ug/L 34.550 69 47-1156733.4 3 30
N-Nitrosodimethylamine ug/L 19.150 38 13-1204723.6 21 30
N-Nitrosodiphenylamine ug/L 40.550 81 43-1208140.6 0 30
N-Nitrosomethylethylamine ug/L 32.150 64 39-1206231.1 3 30
N-Nitrosopiperidine ug/L 36.550 73 43-1137135.4 3 30
N-Nitrosopyrrolidine ug/L 37.5 R1507532-1105226.2 36 30
Nitrobenzene ug/L 31.550 63 33-1107035.1 11 30
O,O,O-Triethylphosphorothioate ug/L 34.750 69 51-1277838.8 11 30
O-Toluidine ug/L 28.950 58 27-1204924.4 17 30
P-Dimethylaminoazobenzene ug/L 18.2100 18 10-1202121.0 14 30
p-Phenylenediamine ug/L 37.6 L2,R1507572-1434924.4 43 30
Parathion (Ethyl parathion)ug/L 40.250 80 56-1407537.5 7 30
Pentachlorobenzene ug/L 34.550 69 30-1376934.7 0 30
Pentachloronitrobenzene ug/L 49.750 99 70-1249748.4 3 30
Pentachlorophenol ug/L 68.9250 28 10-1372356.5 20 30
Phenacetin ug/L 42.850 86 60-1308140.3 6 30
Phenanthrene ug/L 39.850 80 57-1178039.9 0 30
Phenol ug/L 14.250 28 10-1202512.4 13 30
Phorate ug/L 47.050 94 55-1269447.1 0 30
Pronamide ug/L 47.650 95 75-1248944.5 7 30
Pyrene ug/L 41.550 83 55-1229145.7 10 30
Safrole ug/L 33.350 67 41-1206532.7 2 30
Thionazin ug/L 38.250 76 63-1376934.5 10 30
2,4,6-Tribromophenol (S)%84 27-11082
2-Fluorobiphenyl (S)%67 27-11078
2-Fluorophenol (S)%32 12-11033
Nitrobenzene-d5 (S)%67 21-11073
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
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Huntersville, NC 28078
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Page 131 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2178908LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2178909
Phenol-d6 (S)%25 10-11021
Terphenyl-d14 (S)%73 31-10786
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 132 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
393210
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92368450002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2180512
Associated Lab Samples:92368450002
Matrix:Water
Analyzed
1,2,4,5-Tetrachlorobenzene ug/L ND 10.0 01/05/18 13:40
1,3,5-Trinitrobenzene ug/L ND 10.0 01/05/18 13:40
1,3-Dinitrobenzene ug/L ND 20.0 01/05/18 13:40
1,4-Naphthoquinone ug/L ND 5.0 01/05/18 13:40
1-Naphthalenamine ug/L ND 5.0 01/05/18 13:40
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 01/05/18 13:40
2,3,4,6-Tetrachlorophenol ug/L ND 10.0 01/05/18 13:40
2,4,5-Trichlorophenol ug/L ND 10.0 01/05/18 13:40
2,4,6-Trichlorophenol ug/L ND 10.0 01/05/18 13:40
2,4-Dichlorophenol ug/L ND 10.0 01/05/18 13:40
2,4-Dimethylphenol ug/L ND 10.0 01/05/18 13:40
2,4-Dinitrophenol ug/L ND 50.0 01/05/18 13:40
2,4-Dinitrotoluene ug/L ND 10.0 01/05/18 13:40
2,6-Dichlorophenol ug/L ND 10.0 01/05/18 13:40
2,6-Dinitrotoluene ug/L ND 10.0 01/05/18 13:40
2-Acetylaminofluorene ug/L ND 20.0 01/05/18 13:40
2-Chloronaphthalene ug/L ND 10.0 01/05/18 13:40
2-Chlorophenol ug/L ND 10.0 01/05/18 13:40
2-Methylnaphthalene ug/L ND 10.0 01/05/18 13:40
2-Methylphenol(o-Cresol)ug/L ND 10.0 01/05/18 13:40
2-Naphthalenamine ug/L ND 5.0 01/05/18 13:40
2-Nitroaniline ug/L ND 50.0 01/05/18 13:40
2-Nitrophenol ug/L ND 10.0 01/05/18 13:40
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 01/05/18 13:40
3,3'-Dichlorobenzidine ug/L ND 20.0 01/05/18 13:40
3,3'-Dimethylbenzidine ug/L ND 10.0 01/05/18 13:40
3-Methylcholanthrene ug/L ND 10.0 01/05/18 13:40
3-Nitroaniline ug/L ND 50.0 01/05/18 13:40
4,6-Dinitro-2-methylphenol ug/L ND 20.0 01/05/18 13:40
4-Aminobiphenyl ug/L ND 10.0 01/05/18 13:40
4-Bromophenylphenyl ether ug/L ND 10.0 01/05/18 13:40
4-Chloro-3-methylphenol ug/L ND 20.0 01/05/18 13:40
4-Chloroaniline ug/L ND 20.0 01/05/18 13:40
4-Chlorophenylphenyl ether ug/L ND 10.0 01/05/18 13:40
4-Nitroaniline ug/L ND 20.0 01/05/18 13:40
4-Nitrophenol ug/L ND 50.0 01/05/18 13:40
5-Nitro-o-toluidine ug/L ND 10.0 01/05/18 13:40
7,12-Dimethylbenz(a)anthracene ug/L ND 10.0 01/05/18 13:40
Acenaphthene ug/L ND 10.0 01/05/18 13:40
Acenaphthylene ug/L ND 10.0 01/05/18 13:40
Acetophenone ug/L ND 10.0 01/05/18 13:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 133 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2180512
Associated Lab Samples:92368450002
Matrix:Water
Analyzed
Anthracene ug/L ND 10.0 01/05/18 13:40
Benzo(a)anthracene ug/L ND 10.0 01/05/18 13:40
Benzo(a)pyrene ug/L ND 10.0 01/05/18 13:40
Benzo(b)fluoranthene ug/L ND 10.0 01/05/18 13:40
Benzo(g,h,i)perylene ug/L ND 10.0 01/05/18 13:40
Benzo(k)fluoranthene ug/L ND 10.0 01/05/18 13:40
Benzyl alcohol ug/L ND 20.0 01/05/18 13:40
bis(2-Chloroethoxy)methane ug/L ND 10.0 01/05/18 13:40
bis(2-Chloroethyl) ether ug/L ND 10.0 01/05/18 13:40
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 01/05/18 13:40
Butylbenzylphthalate ug/L ND 10.0 01/05/18 13:40
Chlorobenzilate ug/L ND 10.0 01/05/18 13:40
Chrysene ug/L ND 10.0 01/05/18 13:40
Di-n-butylphthalate ug/L ND 10.0 01/05/18 13:40
Di-n-octylphthalate ug/L ND 10.0 01/05/18 13:40
Diallate ug/L ND 10.0 01/05/18 13:40
Dibenz(a,h)anthracene ug/L ND 10.0 01/05/18 13:40
Dibenzofuran ug/L ND 10.0 01/05/18 13:40
Diethylphthalate ug/L ND 10.0 01/05/18 13:40
Dimethoate ug/L ND 10.0 01/05/18 13:40
Dimethylphthalate ug/L ND 10.0 01/05/18 13:40
Diphenylamine ug/L ND 10.0 01/05/18 13:40
Disulfoton ug/L ND 10.0 01/05/18 13:40
Ethyl methanesulfonate ug/L ND 20.0 01/05/18 13:40
Famphur ug/L ND 10.0 01/05/18 13:40
Fluoranthene ug/L ND 10.0 01/05/18 13:40
Fluorene ug/L ND 10.0 01/05/18 13:40
Hexachlorobenzene ug/L ND 10.0 01/05/18 13:40
Hexachlorocyclopentadiene ug/L ND 10.0 01/05/18 13:40
Hexachloroethane ug/L ND 10.0 01/05/18 13:40
Hexachlorophene ug/L ND 100 01/05/18 13:40
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 01/05/18 13:40
Isodrin ug/L ND 20.0 01/05/18 13:40
Isophorone ug/L ND 10.0 01/05/18 13:40
Isosafrole ug/L ND 10.0 01/05/18 13:40
Kepone ug/L ND 10.0 01/05/18 13:40
Methapyrilene ug/L ND 50.0 01/05/18 13:40
Methyl methanesulfonate ug/L ND 5.0 01/05/18 13:40
Methyl parathion ug/L ND 10.0 01/05/18 13:40
N-Nitroso-di-n-butylamine ug/L ND 10.0 01/05/18 13:40
N-Nitroso-di-n-propylamine ug/L ND 10.0 01/05/18 13:40
N-Nitrosodiethylamine ug/L ND 20.0 01/05/18 13:40
N-Nitrosodimethylamine ug/L ND 10.0 01/05/18 13:40
N-Nitrosodiphenylamine ug/L ND 10.0 01/05/18 13:40
N-Nitrosomethylethylamine ug/L ND 10.0 01/05/18 13:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 134 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2180512
Associated Lab Samples:92368450002
Matrix:Water
Analyzed
N-Nitrosopiperidine ug/L ND 20.0 01/05/18 13:40
N-Nitrosopyrrolidine ug/L ND 10.0 01/05/18 13:40
Nitrobenzene ug/L ND 10.0 01/05/18 13:40
O,O,O-Triethylphosphorothioate ug/L ND 10.0 01/05/18 13:40
O-Toluidine ug/L ND 10.0 01/05/18 13:40
P-Dimethylaminoazobenzene ug/L ND 5.0 01/05/18 13:40
p-Phenylenediamine ug/L ND 10.0 01/05/18 13:40
Parathion (Ethyl parathion)ug/L ND 10.0 01/05/18 13:40
Pentachlorobenzene ug/L ND 10.0 01/05/18 13:40
Pentachloronitrobenzene ug/L ND 20.0 01/05/18 13:40
Pentachlorophenol ug/L ND 25.0 01/05/18 13:40
Phenacetin ug/L ND 20.0 01/05/18 13:40
Phenanthrene ug/L ND 10.0 01/05/18 13:40
Phenol ug/L ND 10.0 01/05/18 13:40
Phorate ug/L ND 10.0 01/05/18 13:40
Pronamide ug/L ND 10.0 01/05/18 13:40
Pyrene ug/L ND 10.0 01/05/18 13:40
Safrole ug/L ND 10.0 01/05/18 13:40
Thionazin ug/L ND 20.0 01/05/18 13:40
2,4,6-Tribromophenol (S)%46 27-110 01/05/18 13:40
2-Fluorobiphenyl (S)%74 27-110 01/05/18 13:40
2-Fluorophenol (S)%23 12-110 01/05/18 13:40
Nitrobenzene-d5 (S)%77 21-110 01/05/18 13:40
Phenol-d6 (S)%19 10-110 01/05/18 13:40
Terphenyl-d14 (S)%86 31-107 01/05/18 13:40
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2180514LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2180515
1,2,4,5-Tetrachlorobenzene ug/L 37.350 75 16-1298542.3 12 30
1,3,5-Trinitrobenzene ug/L 24.8 L2505055-1256331.6 24 30
1,3-Dinitrobenzene ug/L 45.850 92 30-1229748.4 6 30
1,4-Naphthoquinone ug/L 41.950 84 31-1209547.4 12 30
1-Naphthalenamine ug/L 33.050 66 37-1267236.1 9 30
2,2'-Oxybis(1-chloropropane)ug/L 31.150 62 18-1207135.4 13 30
2,3,4,6-Tetrachlorophenol ug/L 51.450 103 54-2768341.7 21 30
2,4,5-Trichlorophenol ug/L 30.1 R1506043-1134321.3 34 30
2,4,6-Trichlorophenol ug/L 23.6 L2504742-1203617.9 27 30
2,4-Dichlorophenol ug/L 30.750 61 30-1205326.7 14 30
2,4-Dimethylphenol ug/L 35.550 71 29-1118442.0 17 30
2,4-Dinitrophenol ug/L 47.5J250 19 19-1321947.0J 30
2,4-Dinitrotoluene ug/L 47.750 95 58-12810050.0 5 30
2,6-Dichlorophenol ug/L 27.3 L2505554-1284020.2 30 30
2,6-Dinitrotoluene ug/L 50.150 100 54-12910753.3 6 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 135 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2180514LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2180515
2-Acetylaminofluorene ug/L 47.250 94 81-16010251.0 8 30
2-Chloronaphthalene ug/L 44.150 88 43-1179748.4 9 30
2-Chlorophenol ug/L 31.450 63 37-1205527.3 14 30
2-Methylnaphthalene ug/L 32.750 65 33-1207738.5 16 30
2-Methylphenol(o-Cresol)ug/L 31.550 63 31-1207437.1 16 30
2-Naphthalenamine ug/L 37.850 76 41-1368040.1 6 30
2-Nitroaniline ug/L 86.6100 87 48-1219493.5 8 30
2-Nitrophenol ug/L 29.550 59 25-1164723.5 23 30
3&4-Methylphenol(m&p Cresol)ug/L 22.150 44 23-1205426.9 20 30
3,3'-Dichlorobenzidine ug/L 101250 40 10-15443107 6 30
3,3'-Dimethylbenzidine ug/L 78.2100 78 10-1578484.5 8 30
3-Methylcholanthrene ug/L 54.050 108 65-13011054.8 2 30
3-Nitroaniline ug/L 88.5100 89 43-1159797.4 10 30
4,6-Dinitro-2-methylphenol ug/L 35.2 L21003544-1243332.9 7 30
4-Aminobiphenyl ug/L 39.650 79 21-1258442.2 6 30
4-Bromophenylphenyl ether ug/L 48.650 97 34-1139849.2 1 30
4-Chloro-3-methylphenol ug/L 76.6100 77 31-1108786.7 12 30
4-Chloroaniline ug/L 71.0100 71 20-1208483.6 16 30
4-Chlorophenylphenyl ether ug/L 43.650 87 34-1169145.5 4 30
4-Nitroaniline ug/L 92.7100 93 46-128102102 9 30
4-Nitrophenol ug/L 34.2J250 14 11-1201333.4J 30
5-Nitro-o-toluidine ug/L 45.350 91 78-16010150.5 11 30
7,12-Dimethylbenz(a)anthracene ug/L 52.450 105 47-12410351.7 1 30
Acenaphthene ug/L 42.750 85 48-1149246.1 8 30
Acenaphthylene ug/L 42.450 85 48-1129145.5 7 30
Acetophenone ug/L 36.950 74 24-1208843.8 17 30
Anthracene ug/L 49.050 98 57-11810049.8 2 30
Benzo(a)anthracene ug/L 49.250 98 56-12110150.6 3 30
Benzo(a)pyrene ug/L 51.350 103 55-12710050.1 2 30
Benzo(b)fluoranthene ug/L 53.550 107 53-12810753.4 0 30
Benzo(g,h,i)perylene ug/L 50.250 100 54-12510351.5 2 30
Benzo(k)fluoranthene ug/L 51.250 102 51-1239849.0 4 30
Benzyl alcohol ug/L 59.1100 59 27-1207271.6 19 30
bis(2-Chloroethoxy)methane ug/L 38.950 78 32-1209547.3 20 30
bis(2-Chloroethyl) ether ug/L 36.450 73 33-1118542.7 16 30
bis(2-Ethylhexyl)phthalate ug/L 56.150 112 50-14511658.0 3 30
Butylbenzylphthalate ug/L 59.650 119 54-13812361.3 3 30
Chlorobenzilate ug/L 48.050 96 65-1329647.8 1 30
Chrysene ug/L 48.850 98 58-1279949.6 2 30
Di-n-butylphthalate ug/L 51.050 102 56-12510552.6 3 30
Di-n-octylphthalate ug/L 64.1 L15012850-13414471.9 11 30
Diallate ug/L 49.150 98 47-12310451.9 5 30
Dibenz(a,h)anthracene ug/L 52.650 105 53-12910552.4 0 30
Dibenzofuran ug/L 44.650 89 45-1209246.2 4 30
Diethylphthalate ug/L 47.950 96 53-1209748.6 2 30
Dimethoate ug/L 49.750 99 57-13910351.5 4 30
Dimethylphthalate ug/L 47.050 94 55-1169949.5 5 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 136 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2180514LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2180515
Diphenylamine ug/L 47.350 95 42-1209647.8 1 30
Disulfoton ug/L 48.550 97 49-1569547.7 2 30
Ethyl methanesulfonate ug/L 37.750 75 43-1209245.8 19 30
Famphur ug/L 98.0 R11009840-1607171.0 32 30
Fluoranthene ug/L 47.050 94 57-12510150.5 7 30
Fluorene ug/L 47.350 95 53-1189849.0 4 30
Hexachlorobenzene ug/L 49.550 99 49-11610050.0 1 30
Hexachlorocyclopentadiene ug/L 23.750 47 26-1585728.5 19 30
Hexachloroethane ug/L 20.950 42 30-1144321.3 2 30
Hexachlorophene ug/L 156500 31 10-13028141 10 30
Indeno(1,2,3-cd)pyrene ug/L 50.750 101 55-12810251.0 1 30
Isodrin ug/L 50.350 101 68-12910452.0 3 30
Isophorone ug/L 37.950 76 31-1189145.5 18 30
Isosafrole ug/L 43.550 87 48-1079748.4 11 30
Kepone ug/L 129 L110012910-124120120 8 30
Methapyrilene ug/L 36.1J50 72 40-1607336.3J 30
Methyl methanesulfonate ug/L 86.5 L15017325-114203102 16 30
Methyl parathion ug/L 56.850 114 58-13711859.0 4 30
N-Nitroso-di-n-butylamine ug/L 35.950 72 36-1158643.1 18 30
N-Nitroso-di-n-propylamine ug/L 37.250 74 32-1199145.6 20 30
N-Nitrosodiethylamine ug/L 40.450 81 47-1159245.8 13 30
N-Nitrosodimethylamine ug/L 24.250 48 13-1205326.5 9 30
N-Nitrosodiphenylamine ug/L 47.350 95 43-1209647.8 1 30
N-Nitrosomethylethylamine ug/L 36.250 72 39-1207939.7 9 30
N-Nitrosopiperidine ug/L 40.850 82 43-1139849.0 18 30
N-Nitrosopyrrolidine ug/L 34.150 68 32-1109145.4 28 30
Nitrobenzene ug/L 39.050 78 33-1108844.1 12 30
O,O,O-Triethylphosphorothioate ug/L 40.950 82 51-1279547.7 16 30
O-Toluidine ug/L 32.050 64 27-1207638.0 17 30
P-Dimethylaminoazobenzene ug/L 23.7100 24 10-1202424.3 2 30
p-Phenylenediamine ug/L 45.150 90 72-14311054.8 19 30
Parathion (Ethyl parathion)ug/L 48.650 97 56-14010351.5 6 30
Pentachlorobenzene ug/L 43.550 87 30-1379145.4 4 30
Pentachloronitrobenzene ug/L 51.050 102 70-12411054.8 7 30
Pentachlorophenol ug/L 37.8250 15 10-1371333.0 14 30
Phenacetin ug/L 51.850 104 60-13011457.1 10 30
Phenanthrene ug/L 47.050 94 57-1179848.9 4 30
Phenol ug/L 16.050 32 10-1203517.5 9 30
Phorate ug/L 53.250 106 55-12611456.9 7 30
Pronamide ug/L 53.550 107 75-12411859.0 10 30
Pyrene ug/L 52.850 106 55-12210653.1 1 30
Safrole ug/L 37.850 76 41-1208944.3 16 30
Thionazin ug/L 47.650 95 63-1379949.6 4 30
2,4,6-Tribromophenol (S)%66 27-11049
2-Fluorobiphenyl (S)%85 27-11092
2-Fluorophenol (S)%31 12-11023
Nitrobenzene-d5 (S)%79 21-11093
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 137 of 176
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92368450
OSR 305065
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2180514LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2180515
Phenol-d6 (S)%25 10-11029
Terphenyl-d14 (S)%100 31-107100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 138 of 176
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92368450
OSR 305065
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Common Laboratory Contaminant.C9
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associatedsamples may be biased high.L1
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associatedsamples may be biased low.L2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from samplere-analysis).S2
Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.S3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 139 of 176
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92368450
OSR 305065
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92368450003 MW-1R
92368450004 MW-2R
92368450005 MW-3R
92368450006 MW-5R
92368450007 MW-7
92368450008 MW-9
92368450009 MW-10
92368450010 MW-13
92368450011 MW-14
92368450012 SW-2
92368450013 MW-4R
92368450014 MW-8
92368450015 MW-11
92368450016 MW-12
92368450017 MW-15
92368450002 392784 392919EQUIPMENT BLANK EPA 3510 EPA 8081
92368450003 392784 392919MW-1R EPA 3510 EPA 8081
92368450004 392784 392919MW-2R EPA 3510 EPA 8081
92368450005 392784 392919MW-3R EPA 3510 EPA 8081
92368450006 392784 392919MW-5R EPA 3510 EPA 8081
92368450007 392784 392919MW-7 EPA 3510 EPA 8081
92368450008 392784 392919MW-9 EPA 3510 EPA 8081
92368450009 392784 392919MW-10 EPA 3510 EPA 8081
92368450010 392784 392919MW-13 EPA 3510 EPA 8081
92368450011 392784 392919MW-14 EPA 3510 EPA 8081
92368450013 392886 392923MW-4R EPA 3510 EPA 8081
92368450014 392886 392923MW-8 EPA 3510 EPA 8081
92368450015 392886 392923MW-11 EPA 3510 EPA 8081
92368450016 392886 392923MW-12 EPA 3510 EPA 8081
92368450017 392886 392923MW-15 EPA 3510 EPA 8081
92368450002 392785 392920EQUIPMENT BLANK EPA 3510 EPA 8082
92368450003 392785 392920MW-1R EPA 3510 EPA 8082
92368450004 392785 392920MW-2R EPA 3510 EPA 8082
92368450005 392785 392920MW-3R EPA 3510 EPA 8082
92368450006 392785 392920MW-5R EPA 3510 EPA 8082
92368450007 392785 392920MW-7 EPA 3510 EPA 8082
92368450008 392785 392920MW-9 EPA 3510 EPA 8082
92368450009 392785 392920MW-10 EPA 3510 EPA 8082
92368450010 392785 392920MW-13 EPA 3510 EPA 8082
92368450011 392785 392920MW-14 EPA 3510 EPA 8082
92368450013 392887 392924MW-4R EPA 3510 EPA 8082
92368450014 392887 392924MW-8 EPA 3510 EPA 8082
92368450015 392887 392924MW-11 EPA 3510 EPA 8082
92368450016 392887 392924MW-12 EPA 3510 EPA 8082
92368450017 392887 392924MW-15 EPA 3510 EPA 8082
92368450002 393210 393391EQUIPMENT BLANK EPA 3510 EPA 8270
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 140 of 176
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92368450
OSR 305065
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92368450003 392786 392901MW-1R EPA 3510 EPA 8270
92368450004 392786 392901MW-2R EPA 3510 EPA 8270
92368450005 392786 392901MW-3R EPA 3510 EPA 8270
92368450006 392786 392901MW-5R EPA 3510 EPA 8270
92368450007 392786 392901MW-7 EPA 3510 EPA 8270
92368450008 392786 392901MW-9 EPA 3510 EPA 8270
92368450009 392786 392901MW-10 EPA 3510 EPA 8270
92368450010 392786 392901MW-13 EPA 3510 EPA 8270
92368450011 392786 392901MW-14 EPA 3510 EPA 8270
92368450012 392786 392901SW-2 EPA 3510 EPA 8270
92368450013 392890 393037MW-4R EPA 3510 EPA 8270
92368450014 392890 393037MW-8 EPA 3510 EPA 8270
92368450015 392890 393037MW-11 EPA 3510 EPA 8270
92368450016 392890 393037MW-12 EPA 3510 EPA 8270
92368450017 392890 393037MW-15 EPA 3510 EPA 8270
92368450001 392950TRIP BLANK EPA 8260
92368450002 392950EQUIPMENT BLANK EPA 8260
92368450003 392950MW-1R EPA 8260
92368450004 392950MW-2R EPA 8260
92368450005 392950MW-3R EPA 8260
92368450006 392950MW-5R EPA 8260
92368450007 392950MW-7 EPA 8260
92368450008 392950MW-9 EPA 8260
92368450009 392950MW-10 EPA 8260
92368450010 392950MW-13 EPA 8260
92368450011 392950MW-14 EPA 8260
92368450012 392950SW-2 EPA 8260
92368450013 393369MW-4R EPA 8260
92368450014 393369MW-8 EPA 8260
92368450015 393369MW-11 EPA 8260
92368450016 393369MW-12 EPA 8260
92368450017 393369MW-15 EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/11/2018 10:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 141 of 176
Page 142 of 176
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PACE ANALYTICAL SERVICES, LLC.
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
Pace Analytical Services Inc. - Huntersville
Project: OSR 305065
Huntersville, NC 28078
9800 Kincey Avenue Suite 100
Mr. Kevin Herring
We appreciate the opportunity to provide the analytical support for your project. The analytical results in this report are based
upon information supplied by you, the client, and are for your exclusive use. If you have any questions regarding this data
package, please do not hesitate to call.
Laboratory Report
Project #:92368450
Prepared For:
Attention:
January 10, 2018
Report Number:AAL1010
Approved:
This report may not be reproduced, except in full, without written approval from Pace Analytical Services, LLC.
Pace Analytical Services, LLC. certifies that the following analytical results meet all requirements of the National
Environmental Laboratory Accreditation Conference(NELAC).
All test results relate only to the samples analyzed.
Page 1 of 26
Page 151 of 176
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, LLC.
Pace Analytical Services Inc. - Huntersville
9800 Kincey Avenue Suite 100
Huntersville NC, 28078
Attention: Mr. Kevin Herring
January 10, 2018
Sample ID Laboratory ID Matrix Date Sampled
ANALYTICAL REPORT FOR SAMPLES
Date Received
Equipment Blank/92368450002 AAL1010-01 12/28/17 16:30 12/30/17 10:05Water
MW-1R/92368450003 AAL1010-02 12/28/17 14:40 12/30/17 10:05Water
MW-2R/92368450004 AAL1010-03 12/28/17 15:25 12/30/17 10:05Water
MW-3R/92368450005 AAL1010-04 12/28/17 11:40 12/30/17 10:05Water
MW-5R/92368450006 AAL1010-05 12/28/17 15:30 12/30/17 10:05Water
MW-7/92368450007 AAL1010-06 12/28/17 12:50 12/30/17 10:05Water
MW-9/92368450008 AAL1010-07 12/28/17 11:30 12/30/17 10:05Water
MW-10/92368450009 AAL1010-08 12/28/17 14:40 12/30/17 10:05Water
MW-13/92368450010 AAL1010-09 12/28/17 12:26 12/30/17 10:05Water
MW-14/92368450011 AAL1010-10 12/28/17 13:35 12/30/17 10:05Water
MW-4R/92368450013 AAL1010-11 12/29/17 10:20 12/30/17 10:05Water
MW-8/92368450014 AAL1010-12 12/29/17 10:40 12/30/17 10:05Water
MW-11/92368450015 AAL1010-13 12/29/17 11:55 12/30/17 10:05Water
MW-12/92368450016 AAL1010-14 12/29/17 12:55 12/30/17 10:05Water
MW-15/92368450017 AAL1010-15 12/29/17 11:30 12/30/17 10:05Water
Page 2 of 26
Page 152 of 176
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, LLC.
Pace Analytical Services Inc. - Huntersville
9800 Kincey Avenue Suite 100
Huntersville NC, 28078
Attention: Mr. Kevin Herring
January 10, 2018
ResultAnalyte RL
Preparation
Date
Analytical
DateMethodQual. DFUnits Init.Batch
Report No.: AAL1010
Client ID: Equipment Blank/92368450002
Date/Time Sampled: 12/28/2017 4:30:00PM
Matrix: Water
Lab Number ID: AAL1010-01
Date/Time Received: 12/30/2017 10:05:00AM
Project:OSR 305065
Chlorinated Herbicides by EPA 8151
ND EPA 8151Aug/L 15.0 1/02/18 11:15 1/05/18 13:27 ACM2,4-D 8010043
ND EPA 8151Aug/L 15.0 1/02/18 11:15 1/05/18 13:27 ACM2,4-DB 8010043
ND EPA 8151Aug/L 15.0 1/02/18 11:15 1/05/18 13:27 ACM2,4,5-T 8010043
ND EPA 8151Aug/L 110 1/02/18 11:15 1/05/18 13:27 ACM2,4,5-TP (Silvex)8010043
ND EPA 8151Aug/L 110 1/02/18 11:15 1/05/18 13:27 ACMDalapon8010043
ND EPA 8151Aug/L 15.0 1/02/18 11:15 1/05/18 13:27 ACMDicamba8010043
ND EPA 8151Aug/L 15.0 1/02/18 11:15 1/05/18 13:27 ACMDichloroprop8010043
ND EPA 8151Aug/L 15.0 1/02/18 11:15 1/05/18 13:27 ACMDinoseb8010043
ND EPA 8151Aug/L 11000 1/02/18 11:15 1/05/18 13:27 ACMMCPA8010043
ND EPA 8151Aug/L 11000 1/02/18 11:15 1/05/18 13:27 ACMMCPP8010043
EPA 8151A10-155124 %Surrogate: DCAA 1/02/18 11:15 1/5/18 13:27 8010043
Page 3 of 26
Page 153 of 176
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, LLC.
Pace Analytical Services Inc. - Huntersville
9800 Kincey Avenue Suite 100
Huntersville NC, 28078
Attention: Mr. Kevin Herring
January 10, 2018
ResultAnalyte RL
Preparation
Date
Analytical
DateMethodQual. DFUnits Init.Batch
Report No.: AAL1010
Client ID: MW-1R/92368450003
Date/Time Sampled: 12/28/2017 2:40:00PM
Matrix: Water
Lab Number ID: AAL1010-02
Date/Time Received: 12/30/2017 10:05:00AM
Project:OSR 305065
Chlorinated Herbicides by EPA 8151
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 15:20 ACM2,4-D 8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 15:20 ACM2,4-DB 8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 15:20 ACM2,4,5-T 8010043
ND EPA 8151Aug/L 110 1/03/18 8:30 1/05/18 15:20 ACM2,4,5-TP (Silvex)8010043
ND EPA 8151Aug/L 110 1/03/18 8:30 1/05/18 15:20 ACMDalapon8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 15:20 ACMDicamba8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 15:20 ACMDichloroprop8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 15:20 ACMDinoseb8010043
ND EPA 8151Aug/L 11000 1/03/18 8:30 1/05/18 15:20 ACMMCPA8010043
ND EPA 8151Aug/L 11000 1/03/18 8:30 1/05/18 15:20 ACMMCPP8010043
EPA 8151A10-155153 %Surrogate: DCAA 1/03/18 8:30 1/5/18 15:20 8010043
Page 4 of 26
Page 154 of 176
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, LLC.
Pace Analytical Services Inc. - Huntersville
9800 Kincey Avenue Suite 100
Huntersville NC, 28078
Attention: Mr. Kevin Herring
January 10, 2018
ResultAnalyte RL
Preparation
Date
Analytical
DateMethodQual. DFUnits Init.Batch
Report No.: AAL1010
Client ID: MW-2R/92368450004
Date/Time Sampled: 12/28/2017 3:25:00PM
Matrix: Water
Lab Number ID: AAL1010-03
Date/Time Received: 12/30/2017 10:05:00AM
Project:OSR 305065
Chlorinated Herbicides by EPA 8151
ND EPA 8151Aug/L 210R-01 1/03/18 8:30 1/08/18 14:57 ACM2,4-D 8010043
ND EPA 8151Aug/L 210R-01 1/03/18 8:30 1/08/18 14:57 ACM2,4-DB 8010043
ND EPA 8151Aug/L 210R-01 1/03/18 8:30 1/08/18 14:57 ACM2,4,5-T 8010043
ND EPA 8151Aug/L 220R-01 1/03/18 8:30 1/08/18 14:57 ACM2,4,5-TP (Silvex)8010043
ND EPA 8151Aug/L 220R-01 1/03/18 8:30 1/08/18 14:57 ACMDalapon8010043
ND EPA 8151Aug/L 210R-01 1/03/18 8:30 1/08/18 14:57 ACMDicamba8010043
ND EPA 8151Aug/L 210R-01 1/03/18 8:30 1/08/18 14:57 ACMDichloroprop8010043
ND EPA 8151Aug/L 210R-01 1/03/18 8:30 1/08/18 14:57 ACMDinoseb8010043
ND EPA 8151Aug/L 22000R-01 1/03/18 8:30 1/08/18 14:57 ACMMCPA8010043
ND EPA 8151Aug/L 22000R-01 1/03/18 8:30 1/08/18 14:57 ACMMCPP8010043
EPA 8151A S-0410-155218 %Surrogate: DCAA 1/03/18 8:30 1/8/18 14:57 8010043
Page 5 of 26
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Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, LLC.
Pace Analytical Services Inc. - Huntersville
9800 Kincey Avenue Suite 100
Huntersville NC, 28078
Attention: Mr. Kevin Herring
January 10, 2018
ResultAnalyte RL
Preparation
Date
Analytical
DateMethodQual. DFUnits Init.Batch
Report No.: AAL1010
Client ID: MW-3R/92368450005
Date/Time Sampled: 12/28/2017 11:40:00AM
Matrix: Water
Lab Number ID: AAL1010-04
Date/Time Received: 12/30/2017 10:05:00AM
Project:OSR 305065
Chlorinated Herbicides by EPA 8151
ND EPA 8151Aug/L 210R-01 1/03/18 8:30 1/08/18 15:18 ACM2,4-D 8010043
ND EPA 8151Aug/L 210R-01 1/03/18 8:30 1/08/18 15:18 ACM2,4-DB 8010043
ND EPA 8151Aug/L 210R-01 1/03/18 8:30 1/08/18 15:18 ACM2,4,5-T 8010043
ND EPA 8151Aug/L 220R-01 1/03/18 8:30 1/08/18 15:18 ACM2,4,5-TP (Silvex)8010043
ND EPA 8151Aug/L 220R-01 1/03/18 8:30 1/08/18 15:18 ACMDalapon8010043
ND EPA 8151Aug/L 210R-01 1/03/18 8:30 1/08/18 15:18 ACMDicamba8010043
ND EPA 8151Aug/L 210R-01 1/03/18 8:30 1/08/18 15:18 ACMDichloroprop8010043
ND EPA 8151Aug/L 210R-01 1/03/18 8:30 1/08/18 15:18 ACMDinoseb8010043
ND EPA 8151Aug/L 22000R-01 1/03/18 8:30 1/08/18 15:18 ACMMCPA8010043
ND EPA 8151Aug/L 22000R-01 1/03/18 8:30 1/08/18 15:18 ACMMCPP8010043
EPA 8151A S-0410-155226 %Surrogate: DCAA 1/03/18 8:30 1/8/18 15:18 8010043
Page 6 of 26
Page 156 of 176
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, LLC.
Pace Analytical Services Inc. - Huntersville
9800 Kincey Avenue Suite 100
Huntersville NC, 28078
Attention: Mr. Kevin Herring
January 10, 2018
ResultAnalyte RL
Preparation
Date
Analytical
DateMethodQual. DFUnits Init.Batch
Report No.: AAL1010
Client ID: MW-5R/92368450006
Date/Time Sampled: 12/28/2017 3:30:00PM
Matrix: Water
Lab Number ID: AAL1010-05
Date/Time Received: 12/30/2017 10:05:00AM
Project:OSR 305065
Chlorinated Herbicides by EPA 8151
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 16:23 ACM2,4-D 8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 16:23 ACM2,4-DB 8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 16:23 ACM2,4,5-T 8010043
ND EPA 8151Aug/L 110 1/03/18 8:30 1/05/18 16:23 ACM2,4,5-TP (Silvex)8010043
ND EPA 8151Aug/L 110 1/03/18 8:30 1/05/18 16:23 ACMDalapon8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 16:23 ACMDicamba8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 16:23 ACMDichloroprop8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 16:23 ACMDinoseb8010043
ND EPA 8151Aug/L 11000 1/03/18 8:30 1/05/18 16:23 ACMMCPA8010043
ND EPA 8151Aug/L 11000 1/03/18 8:30 1/05/18 16:23 ACMMCPP8010043
EPA 8151A S-0410-155193 %Surrogate: DCAA 1/03/18 8:30 1/5/18 16:23 8010043
Page 7 of 26
Page 157 of 176
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, LLC.
Pace Analytical Services Inc. - Huntersville
9800 Kincey Avenue Suite 100
Huntersville NC, 28078
Attention: Mr. Kevin Herring
January 10, 2018
ResultAnalyte RL
Preparation
Date
Analytical
DateMethodQual. DFUnits Init.Batch
Report No.: AAL1010
Client ID: MW-7/92368450007
Date/Time Sampled: 12/28/2017 12:50:00PM
Matrix: Water
Lab Number ID: AAL1010-06
Date/Time Received: 12/30/2017 10:05:00AM
Project:OSR 305065
Chlorinated Herbicides by EPA 8151
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 16:44 ACM2,4-D 8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 16:44 ACM2,4-DB 8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 16:44 ACM2,4,5-T 8010043
ND EPA 8151Aug/L 110 1/03/18 8:30 1/05/18 16:44 ACM2,4,5-TP (Silvex)8010043
ND EPA 8151Aug/L 110 1/03/18 8:30 1/05/18 16:44 ACMDalapon8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 16:44 ACMDicamba8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 16:44 ACMDichloroprop8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 16:44 ACMDinoseb8010043
ND EPA 8151Aug/L 11000 1/03/18 8:30 1/05/18 16:44 ACMMCPA8010043
ND EPA 8151Aug/L 11000 1/03/18 8:30 1/05/18 16:44 ACMMCPP8010043
EPA 8151A S-0410-155189 %Surrogate: DCAA 1/03/18 8:30 1/5/18 16:44 8010043
Page 8 of 26
Page 158 of 176
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, LLC.
Pace Analytical Services Inc. - Huntersville
9800 Kincey Avenue Suite 100
Huntersville NC, 28078
Attention: Mr. Kevin Herring
January 10, 2018
ResultAnalyte RL
Preparation
Date
Analytical
DateMethodQual. DFUnits Init.Batch
Report No.: AAL1010
Client ID: MW-9/92368450008
Date/Time Sampled: 12/28/2017 11:30:00AM
Matrix: Water
Lab Number ID: AAL1010-07
Date/Time Received: 12/30/2017 10:05:00AM
Project:OSR 305065
Chlorinated Herbicides by EPA 8151
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 17:05 ACM2,4-D 8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 17:05 ACM2,4-DB 8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 17:05 ACM2,4,5-T 8010043
ND EPA 8151Aug/L 110 1/03/18 8:30 1/05/18 17:05 ACM2,4,5-TP (Silvex)8010043
ND EPA 8151Aug/L 110 1/03/18 8:30 1/05/18 17:05 ACMDalapon8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 17:05 ACMDicamba8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 17:05 ACMDichloroprop8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 17:05 ACMDinoseb8010043
ND EPA 8151Aug/L 11000 1/03/18 8:30 1/05/18 17:05 ACMMCPA8010043
ND EPA 8151Aug/L 11000 1/03/18 8:30 1/05/18 17:05 ACMMCPP8010043
EPA 8151A10-15590 %Surrogate: DCAA 1/03/18 8:30 1/5/18 17:05 8010043
Page 9 of 26
Page 159 of 176
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, LLC.
Pace Analytical Services Inc. - Huntersville
9800 Kincey Avenue Suite 100
Huntersville NC, 28078
Attention: Mr. Kevin Herring
January 10, 2018
ResultAnalyte RL
Preparation
Date
Analytical
DateMethodQual. DFUnits Init.Batch
Report No.: AAL1010
Client ID: MW-10/92368450009
Date/Time Sampled: 12/28/2017 2:40:00PM
Matrix: Water
Lab Number ID: AAL1010-08
Date/Time Received: 12/30/2017 10:05:00AM
Project:OSR 305065
Chlorinated Herbicides by EPA 8151
ND EPA 8151Aug/L 1050R-01 1/03/18 8:30 1/08/18 15:39 ACM2,4-D 8010043
ND EPA 8151Aug/L 1050R-01 1/03/18 8:30 1/08/18 15:39 ACM2,4-DB 8010043
ND EPA 8151Aug/L 1050R-01 1/03/18 8:30 1/08/18 15:39 ACM2,4,5-T 8010043
ND EPA 8151Aug/L 10100R-01 1/03/18 8:30 1/08/18 15:39 ACM2,4,5-TP (Silvex)8010043
ND EPA 8151Aug/L 10100R-01 1/03/18 8:30 1/08/18 15:39 ACMDalapon8010043
ND EPA 8151Aug/L 1050R-01 1/03/18 8:30 1/08/18 15:39 ACMDicamba8010043
ND EPA 8151Aug/L 1050R-01 1/03/18 8:30 1/08/18 15:39 ACMDichloroprop8010043
ND EPA 8151Aug/L 1050R-01 1/03/18 8:30 1/08/18 15:39 ACMDinoseb8010043
ND EPA 8151Aug/L 1010000R-01 1/03/18 8:30 1/08/18 15:39 ACMMCPA8010043
ND EPA 8151Aug/L 1010000R-01 1/03/18 8:30 1/08/18 15:39 ACMMCPP8010043
EPA 8151A S-0410-155592 %Surrogate: DCAA 1/03/18 8:30 1/8/18 15:39 8010043
Page 10 of 26
Page 160 of 176
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, LLC.
Pace Analytical Services Inc. - Huntersville
9800 Kincey Avenue Suite 100
Huntersville NC, 28078
Attention: Mr. Kevin Herring
January 10, 2018
ResultAnalyte RL
Preparation
Date
Analytical
DateMethodQual. DFUnits Init.Batch
Report No.: AAL1010
Client ID: MW-13/92368450010
Date/Time Sampled: 12/28/2017 12:26:00PM
Matrix: Water
Lab Number ID: AAL1010-09
Date/Time Received: 12/30/2017 10:05:00AM
Project:OSR 305065
Chlorinated Herbicides by EPA 8151
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 18:17 ACM2,4-D 8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 18:17 ACM2,4-DB 8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 18:17 ACM2,4,5-T 8010043
ND EPA 8151Aug/L 110 1/03/18 8:30 1/05/18 18:17 ACM2,4,5-TP (Silvex)8010043
ND EPA 8151Aug/L 110 1/03/18 8:30 1/05/18 18:17 ACMDalapon8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 18:17 ACMDicamba8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 18:17 ACMDichloroprop8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 18:17 ACMDinoseb8010043
ND EPA 8151Aug/L 11000 1/03/18 8:30 1/05/18 18:17 ACMMCPA8010043
ND EPA 8151Aug/L 11000 1/03/18 8:30 1/05/18 18:17 ACMMCPP8010043
EPA 8151A10-155112 %Surrogate: DCAA 1/03/18 8:30 1/5/18 18:17 8010043
Page 11 of 26
Page 161 of 176
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, LLC.
Pace Analytical Services Inc. - Huntersville
9800 Kincey Avenue Suite 100
Huntersville NC, 28078
Attention: Mr. Kevin Herring
January 10, 2018
ResultAnalyte RL
Preparation
Date
Analytical
DateMethodQual. DFUnits Init.Batch
Report No.: AAL1010
Client ID: MW-14/92368450011
Date/Time Sampled: 12/28/2017 1:35:00PM
Matrix: Water
Lab Number ID: AAL1010-10
Date/Time Received: 12/30/2017 10:05:00AM
Project:OSR 305065
Chlorinated Herbicides by EPA 8151
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 18:38 ACM2,4-D 8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 18:38 ACM2,4-DB 8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 18:38 ACM2,4,5-T 8010043
ND EPA 8151Aug/L 110 1/03/18 8:30 1/05/18 18:38 ACM2,4,5-TP (Silvex)8010043
ND EPA 8151Aug/L 110 1/03/18 8:30 1/05/18 18:38 ACMDalapon8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 18:38 ACMDicamba8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 18:38 ACMDichloroprop8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 18:38 ACMDinoseb8010043
ND EPA 8151Aug/L 11000 1/03/18 8:30 1/05/18 18:38 ACMMCPA8010043
ND EPA 8151Aug/L 11000 1/03/18 8:30 1/05/18 18:38 ACMMCPP8010043
EPA 8151A S-0410-155159 %Surrogate: DCAA 1/03/18 8:30 1/5/18 18:38 8010043
Page 12 of 26
Page 162 of 176
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, LLC.
Pace Analytical Services Inc. - Huntersville
9800 Kincey Avenue Suite 100
Huntersville NC, 28078
Attention: Mr. Kevin Herring
January 10, 2018
ResultAnalyte RL
Preparation
Date
Analytical
DateMethodQual. DFUnits Init.Batch
Report No.: AAL1010
Client ID: MW-4R/92368450013
Date/Time Sampled: 12/29/2017 10:20:00AM
Matrix: Water
Lab Number ID: AAL1010-11
Date/Time Received: 12/30/2017 10:05:00AM
Project:OSR 305065
Chlorinated Herbicides by EPA 8151
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 18:59 ACM2,4-D 8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 18:59 ACM2,4-DB 8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 18:59 ACM2,4,5-T 8010043
ND EPA 8151Aug/L 110 1/03/18 8:30 1/05/18 18:59 ACM2,4,5-TP (Silvex)8010043
ND EPA 8151Aug/L 110 1/03/18 8:30 1/05/18 18:59 ACMDalapon8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 18:59 ACMDicamba8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 18:59 ACMDichloroprop8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 18:59 ACMDinoseb8010043
ND EPA 8151Aug/L 11000 1/03/18 8:30 1/05/18 18:59 ACMMCPA8010043
ND EPA 8151Aug/L 11000 1/03/18 8:30 1/05/18 18:59 ACMMCPP8010043
EPA 8151A S-0410-155184 %Surrogate: DCAA 1/03/18 8:30 1/5/18 18:59 8010043
Page 13 of 26
Page 163 of 176
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, LLC.
Pace Analytical Services Inc. - Huntersville
9800 Kincey Avenue Suite 100
Huntersville NC, 28078
Attention: Mr. Kevin Herring
January 10, 2018
ResultAnalyte RL
Preparation
Date
Analytical
DateMethodQual. DFUnits Init.Batch
Report No.: AAL1010
Client ID: MW-8/92368450014
Date/Time Sampled: 12/29/2017 10:40:00AM
Matrix: Water
Lab Number ID: AAL1010-12
Date/Time Received: 12/30/2017 10:05:00AM
Project:OSR 305065
Chlorinated Herbicides by EPA 8151
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 19:20 ACM2,4-D 8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 19:20 ACM2,4-DB 8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 19:20 ACM2,4,5-T 8010043
ND EPA 8151Aug/L 110 1/03/18 8:30 1/05/18 19:20 ACM2,4,5-TP (Silvex)8010043
ND EPA 8151Aug/L 110 1/03/18 8:30 1/05/18 19:20 ACMDalapon8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 19:20 ACMDicamba8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 19:20 ACMDichloroprop8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 19:20 ACMDinoseb8010043
ND EPA 8151Aug/L 11000 1/03/18 8:30 1/05/18 19:20 ACMMCPA8010043
ND EPA 8151Aug/L 11000 1/03/18 8:30 1/05/18 19:20 ACMMCPP8010043
EPA 8151A10-155147 %Surrogate: DCAA 1/03/18 8:30 1/5/18 19:20 8010043
Page 14 of 26
Page 164 of 176
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, LLC.
Pace Analytical Services Inc. - Huntersville
9800 Kincey Avenue Suite 100
Huntersville NC, 28078
Attention: Mr. Kevin Herring
January 10, 2018
ResultAnalyte RL
Preparation
Date
Analytical
DateMethodQual. DFUnits Init.Batch
Report No.: AAL1010
Client ID: MW-11/92368450015
Date/Time Sampled: 12/29/2017 11:55:00AM
Matrix: Water
Lab Number ID: AAL1010-13
Date/Time Received: 12/30/2017 10:05:00AM
Project:OSR 305065
Chlorinated Herbicides by EPA 8151
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 19:41 ACM2,4-D 8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 19:41 ACM2,4-DB 8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 19:41 ACM2,4,5-T 8010043
ND EPA 8151Aug/L 110 1/03/18 8:30 1/05/18 19:41 ACM2,4,5-TP (Silvex)8010043
ND EPA 8151Aug/L 110 1/03/18 8:30 1/05/18 19:41 ACMDalapon8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 19:41 ACMDicamba8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 19:41 ACMDichloroprop8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 19:41 ACMDinoseb8010043
ND EPA 8151Aug/L 11000 1/03/18 8:30 1/05/18 19:41 ACMMCPA8010043
ND EPA 8151Aug/L 11000 1/03/18 8:30 1/05/18 19:41 ACMMCPP8010043
EPA 8151A10-155121 %Surrogate: DCAA 1/03/18 8:30 1/5/18 19:41 8010043
Page 15 of 26
Page 165 of 176
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, LLC.
Pace Analytical Services Inc. - Huntersville
9800 Kincey Avenue Suite 100
Huntersville NC, 28078
Attention: Mr. Kevin Herring
January 10, 2018
ResultAnalyte RL
Preparation
Date
Analytical
DateMethodQual. DFUnits Init.Batch
Report No.: AAL1010
Client ID: MW-12/92368450016
Date/Time Sampled: 12/29/2017 12:55:00PM
Matrix: Water
Lab Number ID: AAL1010-14
Date/Time Received: 12/30/2017 10:05:00AM
Project:OSR 305065
Chlorinated Herbicides by EPA 8151
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 20:01 ACM2,4-D 8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 20:01 ACM2,4-DB 8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 20:01 ACM2,4,5-T 8010043
ND EPA 8151Aug/L 110 1/03/18 8:30 1/05/18 20:01 ACM2,4,5-TP (Silvex)8010043
ND EPA 8151Aug/L 110 1/03/18 8:30 1/05/18 20:01 ACMDalapon8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 20:01 ACMDicamba8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 20:01 ACMDichloroprop8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 20:01 ACMDinoseb8010043
ND EPA 8151Aug/L 11000 1/03/18 8:30 1/05/18 20:01 ACMMCPA8010043
ND EPA 8151Aug/L 11000 1/03/18 8:30 1/05/18 20:01 ACMMCPP8010043
EPA 8151A10-155116 %Surrogate: DCAA 1/03/18 8:30 1/5/18 20:01 8010043
Page 16 of 26
Page 166 of 176
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, LLC.
Pace Analytical Services Inc. - Huntersville
9800 Kincey Avenue Suite 100
Huntersville NC, 28078
Attention: Mr. Kevin Herring
January 10, 2018
ResultAnalyte RL
Preparation
Date
Analytical
DateMethodQual. DFUnits Init.Batch
Report No.: AAL1010
Client ID: MW-15/92368450017
Date/Time Sampled: 12/29/2017 11:30:00AM
Matrix: Water
Lab Number ID: AAL1010-15
Date/Time Received: 12/30/2017 10:05:00AM
Project:OSR 305065
Chlorinated Herbicides by EPA 8151
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 20:22 ACM2,4-D 8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 20:22 ACM2,4-DB 8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 20:22 ACM2,4,5-T 8010043
ND EPA 8151Aug/L 110 1/03/18 8:30 1/05/18 20:22 ACM2,4,5-TP (Silvex)8010043
ND EPA 8151Aug/L 110 1/03/18 8:30 1/05/18 20:22 ACMDalapon8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 20:22 ACMDicamba8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 20:22 ACMDichloroprop8010043
ND EPA 8151Aug/L 15.0 1/03/18 8:30 1/05/18 20:22 ACMDinoseb8010043
ND EPA 8151Aug/L 11000 1/03/18 8:30 1/05/18 20:22 ACMMCPA8010043
ND EPA 8151Aug/L 11000 1/03/18 8:30 1/05/18 20:22 ACMMCPP8010043
EPA 8151A S-0410-155163 %Surrogate: DCAA 1/03/18 8:30 1/5/18 20:22 8010043
Page 17 of 26
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Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, LLC.
Pace Analytical Services Inc. - Huntersville
9800 Kincey Avenue Suite 100
Huntersville NC, 28078
Attention: Mr. Kevin Herring
January 10, 2018
Report No.: AAL1010
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Chlorinated Herbicides by EPA 8151 - Quality Control
Batch 8010043 - EPA 8151A
Blank (8010043-BLK1)Prepared: 01/02/18 Analyzed: 01/05/18
2,4-D ug/LND5.0
2,4-DB ug/LND5.0
2,4,5-T ug/LND5.0
2,4,5-TP (Silvex)ug/LND10
Dalapon ug/LND10
Dicamba ug/LND5.0
Dichloroprop ug/LND5.0
Dinoseb ug/LND5.0
MCPA ug/LND1000
MCPP ug/LND1000
ug/L 10.000 S-0910-155Surrogate: DCAA 17017.0
Blank (8010043-BLK2)Prepared: 01/03/18 Analyzed: 01/05/18
2,4-D ug/LND5.0
2,4-DB ug/LND5.0
2,4,5-T ug/LND5.0
2,4,5-TP (Silvex)ug/LND10
Dalapon ug/LND10
Dicamba ug/LND5.0
Dichloroprop ug/LND5.0
Dinoseb ug/LND5.0
MCPA ug/LND1000
MCPP ug/LND1000
ug/L 10.000 10-155Surrogate: DCAA 12912.9
LCS (8010043-BS1)Prepared: 01/02/18 Analyzed: 01/05/18
2,4-D ug/L9.04 5.0 10.000 29-14590
2,4-DB ug/L22.8 5.0 10.000 QL-0324-145228
2,4,5-T ug/L9.42 5.0 10.000 31-15094
2,4,5-TP (Silvex)ug/L9.05 10 10.000 35-13890
Dalapon ug/L7.73 10 10.000 31-12077
Dicamba ug/L9.79 5.0 10.000 45-13998
Dichloroprop ug/L11.7 5.0 10.000 54-139117
Dinoseb ug/L2.61 5.0 10.000 10-18226
MCPA ug/L15701000 1000.0 QL-0325-147157
MCPP ug/L11301000 1000.0 10-169113
ug/L 10.000 10-155Surrogate: DCAA 14514.5
Page 18 of 26
Page 168 of 176
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, LLC.
Pace Analytical Services Inc. - Huntersville
9800 Kincey Avenue Suite 100
Huntersville NC, 28078
Attention: Mr. Kevin Herring
January 10, 2018
Report No.: AAL1010
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Chlorinated Herbicides by EPA 8151 - Quality Control
Batch 8010043 - EPA 8151A
LCS (8010043-BS2)Prepared: 01/03/18 Analyzed: 01/08/18
2,4-D ug/L11.3 5.0 10.000 29-145113
2,4-DB ug/L22.9 5.0 10.000 QL-0324-145229
2,4,5-T ug/L12.2 5.0 10.000 31-150122
2,4,5-TP (Silvex)ug/L12.5 10 10.000 35-138125
Dalapon ug/L10.2 10 10.000 31-120102
Dicamba ug/L13.5 5.0 10.000 45-139135
Dichloroprop ug/L14.8 5.0 10.000 QL-0354-139148
Dinoseb ug/L2.15 5.0 10.000 10-18222
MCPA ug/L13901000 1000.0 25-147139
MCPP ug/L12101000 1000.0 10-169121
ug/L 10.000 S-0910-155Surrogate: DCAA 17517.5
Matrix Spike (8010043-MS1)Prepared: 01/02/18 Analyzed: 01/05/18 Source: AAL1010-01
2,4-D ug/L11.0 5.0 10.000 ND 10-156110
2,4-DB ug/L17.5 5.0 10.000 ND QM-0924-145175
2,4,5-T ug/L11.2 5.0 10.000 ND 10-158112
2,4,5-TP (Silvex)ug/L11.5 10 10.000 ND 10-156115
Dalapon ug/L8.66 10 10.000 ND 31-12087
Dicamba ug/L12.1 5.0 10.000 ND 45-139121
Dichloroprop ug/L13.7 5.0 10.000 ND 54-139137
Dinoseb ug/L1.68 5.0 10.000 ND 10-17417
MCPA ug/LND1000 1000.0 ND QM-0925-1470
MCPP ug/L20601000 1000.0 ND QM-0510-169206
ug/L 10.000 S-0410-155Surrogate: DCAA 17517.5
Matrix Spike Dup (8010043-MSD1)Prepared: 01/02/18 Analyzed: 01/05/18 Source: AAL1010-01
2,4-D ug/L9.04 5.0 10.000 ND 4910-15690 19
2,4-DB ug/L17.3 5.0 10.000 ND 50 QM-0924-145173 1
2,4,5-T ug/L8.77 5.0 10.000 ND 4810-15888 25
2,4,5-TP (Silvex)ug/L8.84 10 10.000 ND 4610-15688 26
Dalapon ug/L6.56 10 10.000 ND 5031-12066 27
Dicamba ug/L9.34 5.0 10.000 ND 5045-13993 26
Dichloroprop ug/L11.6 5.0 10.000 ND 5054-139116 17
Dinoseb ug/L2.12 5.0 10.000 ND 5610-17421 23
MCPA ug/L16201000 1000.0 ND 50 QM-0925-147162
MCPP ug/L12301000 1000.0 ND 50 QM-0510-169123 51
ug/L 10.000 10-155Surrogate: DCAA 15015.0
Page 19 of 26
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Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, LLC.
Pace Analytical Services Inc. - Huntersville
9800 Kincey Avenue Suite 100
Huntersville NC, 28078
Attention: Mr. Kevin Herring
January 10, 2018
Laboratory Certifications
Code Description Number Expires
812Georgia DW Inorganics Eff: 07/01/2016 06/30/2018GADW
812Georgia DW Microbiology Eff: 07/01/2015 12/09/2019GADWM
381North Carolina 12/31/2018NC
E87315FL DOH (Non-Pot. Water, Solids) Eff:: 07/01/2016 06/30/2018NELAC
E87315FL DOH NELAC (Drinking Water) Eff: 07/01/2016 06/30/2018NELDW
98011001South Carolina 06/30/2018SC
T104704397-08-TXTexas 03/31/2018TX
460204Virginia 12/14/2018VA
Page 20 of 26
Page 170 of 176
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Peachtree Corners, GA 30092
[phone] FAX [phone]
PACE ANALYTICAL SERVICES, LLC.
Pace Analytical Services Inc. - Huntersville
9800 Kincey Avenue Suite 100
Huntersville NC, 28078
Attention: Mr. Kevin Herring
January 10, 2018
Legend
Definition of Laboratory Terms
ND
TIC
CFU
SOP
RL
- None Detected at the Reporting Limit
- Tentatively Identified Compound
- Colony Forming Units
- Method run per Pace Standard Operating Procedure
- Reporting Limit
Definition of Qualifiers
Sample Information
N-Nitrosodiphenylamine breaks down to diphenylamine in the GCMS; both analytes are reported as
N-Nitrososdiphenylamine. Pace is not NELAC certified for diphenylamine.
Phthalic acid and phthalic anhydride are reported as dimethyl phthalate
Maleic acid and maleic anhydride are reported as dimethyl malate
1,2-Diphenylhydrazine breaks down to azobenzene in the GCMS; both analytes are reported as azobenzene
DF - Dilution Factor
* - Analyte not included in the NELAC list of certified analytes.
Drinking Water Records will be available for at least 5 years and are subject to disposal after the 5 years have
elapsed.
S-09 Surrogate recovery was outside control limits biased high. Associated target analytes were not detected at levels
at or above the Method Detection Limit and the data was not affected.
S-04 The surrogate recovery for this sample is outside of established control limits due to a suspected sample matrix
effect.
R-01 Elevated reporting limit due to matrix interference.
QM-09 MS and/or MSD and/or RPD and/or PDS recoveries were outside acceptance limits biased high. Target analyte
was not detected at levels at or above reporting limit and data was not affected.
QM-05 The spike recovery was outside acceptance limits for the MS and/or MSD and/or PDS due to suspected matrix
interference. Sample results for the QC batch were accepted based on acceptable LCS recoveries.
QL-03 Lab Control recoveries were outside of control limits biased high. Target analyte was not detected at levels at or
above reporting limit and data was not affected.
Note: Unless otherwise noted, all results are reported on an as received basis.
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LOG-IN CHECKLIST
Pace Analytical Services Inc. - Huntersville
OSR 305065Project:
Client:
Printed: 1/4/2018 3:29:50PM
Environmental Monitoring & Laboratory Analysis
[phone] FAX [phone]
110 Technology Parkway, Peachtree Corners, GA 30092
PACE ANALYTICAL SERVICES, LLC.
Date Received:12/30/17 10:05 Logged In By:Mohammad M. Rahman
Work Order:AAL1010
OBSERVATIONS
Attn: Mr. Kevin Herring
#Samples: 15 #Containers: 30
0.2 0.2
YES
Minimum Temp(C):Maximum Temp(C):
CHECKLIST ITEMS
COC included with Samples
Sample Container(s) Intact
Chain of Custody Complete
Sample Container(s) Match COC
Custody seal Intact
Temperature in Compliance
Sufficient Sample Volume for Analysis
Zero Headspace Maintained for VOA Analyses
Samples labeled preserved (If Applicable)
Samples received within Allowable Hold Times
Samples Received on Ice
Preservation Confirmed
YES
YES
YES
N/A
YES
YES
YES
YES
YES
YES
YES
Custody Seal(s) Used:No
Comments:
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Winston-Salem City/County Utilities | Supplement to the Assessment Monitoring Report Appendix C – Field Data

C
Appendix C – Field Data

Winston-Salem City/County Utilities | Supplement to the Assessment Monitoring Report Appendix C – Field Data

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Winston-Salem City/County Utilities | Supplement to the Assessment Monitoring Report Appendix D – Electronic Files

D
Appendix D – Electronic Files
Portable Document Format (PDF) of this Report
Electronic Data Deliverable (EDD) of Groundwater
Results

Winston-Salem City/County Utilities | Supplement to the Assessment Monitoring Report Appendix D – Electronic Files

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