HomeMy WebLinkAbout12033 N Tryon Griffin Vapor Intrusion Evaluation 20130205
Vapor Intrusion Evaluation
Former Ira Griffin & Sons Property
2205 and 2215 North Tryon Street
Charlotte, North Carolina
H&H Job No. CLT-300
February 5, 2013
Via Email
February 5, 2013
NC DENR Brownfields Section
1314 Mallard Ridge Rd
Tega Cay, SC 29708 Attn: Carolyn F. Minnich
Re: Former Ira Griffin & Sons Property
Vapor Intrusion Evaluation 2205 and 2215 North Tryon Street Charlotte, North Carolina
H&H Job No. CLT-300
Dear Carolyn:
This vapor intrusion evaluation was conducted to facilitate Brownfield planning. The 2.86-acre
property consists of two buildings previously utilized as office and warehouse space. The
buildings are currently vacant. Ira Griffin and Sons occupied the subject facility between 1983
and 2008 where they fabricated, assembled, and shipped textile manufacturing equipment. Prior
to Ira Griffin & Sons, the property was utilized by Crawford Sprinkler System a trailer
manufacturer, and a neon sign manufacturer.
Step 1: Groundwater Screening
Groundwater data collected in 2008 at the Former Ira Griffin & Sons Property and the adjacent
Latimer property consisted of collecting six samples from temporary wells installed to a depth of
approximately 30 ft below ground surface (bgs). Each well was constructed of a 1-inch diameter
Schedule 40 PVC riser and a 15-ft length of 0.01-inch slot screen installed to bracket the water
table. Groundwater was encountered at depths ranging between 17 and 19 ft bgs. Following
depth-to-water measurement, each well was purged a minimum of one well volume using a
peristaltic pump and dedicated tubing, and the water quality parameters (pH, conductivity, and
temperature) were measured. After stabilization of the water quality parameters, ground water
Carolyn F. Minnich
February 5, 2013
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samples were collected. All groundwater samples were analyzed for volatile organic compounds
(VOCs) by EPA Method 6230D and polycyclic aromatic hydrocarbons (PAHs) by EPA Method
8270C. The three groundwater samples collected August 2008 were also analyzed for metals by
EPA Method 6010B and 7470A/7471A. Following sampling, the temporary monitoring wells were
properly abandoned.
H&H compared the 2008 data with the current July 2012 IHSB Residential and
Industrial/Commercial Vapor Intrusion Screening Criteria. The 2008 groundwater data and
applicable screening criteria are shown on Table 1. A site map and sample location map are
included as Figures 1 and 2, respectively. The groundwater samples collected from TMW-3
(179 µg/L), TMW-5 (55.3 µg/L), and TW-4 (43.9 µg/L) contained 1,1-DCE at concentrations
exceeding the IHSB residential screening criteria. In addition, the concentration of 1,1-DCE
from TMW-3 exceeded the IHSB industrial/commercial screening criteria.
Step 2: Soil Vapor Assessment/Screening
In the April 15, 2009 letter, DENR requested submittal of a work plan and collection of soil gas
samples or subslab samples on the former Ira Griffin & Sons property and the adjacent Latimer
property to determine if soil vapor poses a potential unacceptable risk to current or future site
structures. H&H submitted a work plan for the soil vapor assessment on June 1, 2009.
The work plan was subsequently approved with comments by DENR on June 22, 2009, which
were incorporated into the sampling event. Two subsurface vapor points (VPs) labeled VP-3 and
VP-5 and one subslab VP labeled VP-4 were installed on July 16, 2009 on the former Ira Griffin
& Sons property. Sampling locations are depicted on Figure 2 and were installed on July 16,
2009 on the former Ira Griffin & Sons property. These locations corresponded with the
previously discussed groundwater sample points.
For the installation of VP-3 and VP-5, a hand auger was utilized to install a 3-inch diameter
boring through the underlying soil to a depth of 5 feet below land surface (bls). A rotary
Carolyn F. Minnich
February 5, 2013
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hammer drill was utilized to bore through the concrete slab at the VP-4 location. The building
slab was observed to be approximately 6 inches thick at the VP-4 location and underlain by a
gravel layer.
A stainless steel AMS dedicated soil gas vapor point fitted with ¼-inch diameter Teflon tubing
was installed into each borehole. With the exception of VP-4, the tip installed at this subsurface
VP location was advanced to 5.5 feet bls. The tip installed at the VP-4 location was set
approximately 1 to 2 inches beneath the slab using an AMS Gas Vapor Probe Kit and slide
hammer. Filter sand was then poured through each borehole around the vapor point to
approximately 4 to 6 inches above each subsurface point and approximately 5 inches below the
top surface of the concrete slab at the VP-4 location. Each borehole was subsequently completed
by installing hydrated bentonite from the top of the sand to the surface of the borehole.
After allowing the bentonite to set for at least 24-hours in each borehole, H&H personnel
collected vapor samples from VP-3 through VP-5 on July 17, 2009 using 6-liter Summa
canisters. Prior to mobilizing to the site, the initial vacuum in each Summa canister was
measured and recorded using a vacuum gauge provided by the lab. In the field, the following
procedures were used to sample each VP. The VP was purged using a 60 mL syringe with a
three-way valve to evacuate air in the probe annular space and tubing. After purging the VP, the
Summa canister was connected to a flow regulator (set by the lab to limit the vapor intake rate to
approximately 6-liters per hour) and the sample train was checked for leaks. Subsequently, the
flow regulator was connected to the VP tubing using a ferrule to form an air-tight seal. The
canister’s air intake valve was then opened to begin collection of the vapor sample.
As approved by DENR in the June 2009 Work Plan, the samples were collected and analyzed for
1,2-DCA, cis-1,2-DCE, PCE, TCE, and vinyl chloride. However, the soil gas samples were not
required to be analyzed for 1,1-DCE at that time. Subsequently, H&H requested the lab reissue
the lab report to include 1,1-DCE. The lab report was revised and is included as Appendix A.
The available analytical results, compared against the IHSB Residential and
Carolyn F. Minnich
February 5, 2013
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Industrial/Commercial Vapor Intrusion screening criteria are provided on Table 2. PCE was
detected in the samples from VP-4 and VP-5 at concentrations up to 50 µg/m3, which is below
both the residential and industrial screening criteria for PCE. In addition, 1,1-DCE was detected
in all three soil gas samples at concentrations up to 120 µg/mg3, which is below both the
residential and industrial screening criteria for 1,1-DCE.
Step 3: Indoor Air Sampling
This step was not completed as available soil gas concentrations were not detected above
applicable screening criteria.
Step 4: Recommendations
Based on the soil vapor results H&H does not recommend additional vapor intrusion assessment
or mitigation at the Ira Griffin & Sons Property.
Should you have any questions or require any additional information concerning this submittal,
please feel free to contact me at (704) 586-0007.
Sincerely,
Hart & Hickman, PC
Bruce Hickman Principal Engineer
Attachments
cc: David Wolfe, City of Charlotte (Electronic Copy)
Cindy Nolan, US EPA (Hard Copy)
Geoffrey Curme, Mount Vernon Asset Management, LLC (Hard and Electronic Copy)
Peter McGrath, Moore & VanAllen (Electronic Copy)
S:\AAA-Master Projects\City of Charlotte - CLT\CLT-300 Brownfield Grant Activities\North Tryon Vapor Intrusion Evaluations\Griffin Vapor Intrusion Evaluation\
2008 Griffin Soil and GW Data
1/28/2013
Table 1
Hart & Hickman, PC
Table 1
Summary of Groundwater Analytical Data
Ira Griffin & Sons Property
Charlotte, North Carolina
H&H Project No. CLT-300
Sample ID TMW-3 TMW-4 TMW-5 TW-2 TW-3 TW-4
Date 6/25/08 6/25/08 6/25/08 8/8/08 8/8/08 8/8/08
1,1-Dichloroethane 2.94 <0.5 <0.5 <0.500 <0.500 1.50 65 330
1,2-Dichloroethane 1.37 <0.5 <0.5 <0.500 <0.500 <0.500 20 98
1,1-Dichloroethene (1,1-DCE)179 <0.5 55.3 1.21 1.19 43.9 38 160
cis-1,2-Dichloroethene <0.5 <0.5 <0.5 <0.500 <0.500 <0.500 NS NS
Tetrachloroethene (PCE)<0.5 <0.5 0.790 <0.500 <0.500 <0.500 12 49
1,1,1-Trichloroethane 0.830 <0.5 0.720 <0.500 <0.500 <0.500 1,500 6,300
Trichloroethene (TCE)<0.5 <0.5 <0.5 <0.500 <0.500 <0.500 1.1 4.4
All Target Compounds ND ND ND ND ND ND ----
Barium NA NA NA 0.0844 0.566 0.475 NS NS
Cadmium NA NA NA <0.00100 0.00160 0.00120 NS NS
Chromium NA NA NA 0.00510 0.758 0.209 NS NS
Notes:
1) NC DENR Inactive Hazardous Sites Branch (IHSB) Residential Vapor Intrusion Screening Levels (July 2012)
2) NC DENR IHSB Industrial/Commercial Vapor Intrusion Screening Levels (July 2012)
3) Has both carcinogenic and non-carcinogenic properties
Only those compounds detected in at least one sample shown in above table.
Bold indicates that concentration exceeds the residential screening levels.
Bold and underlined indicates that concentration exceeds the industrial/commercial screening levels.
VOCs=volatile organic compounds, PAHs = polycyclic aromatic hydrocarbons
NA = Not Analyzed
NS = Not Specified
ND = Not Detected
Total Metals (EPA Method 6010B and 7470A/7471A) mg/L
IHSB Industrial/
Commercial
Acceptable
Groundwater
Concentration 2
IHSB Residential
Acceptable
Groundwater
Concentration 1
VOCs (EPA Method 8260B) µg/L
PAHs (EPA Method 8270C) µg/L
Table 2
Summary of Vapor Analytical Detections
IRA Griffin Sons Property
Charlotte, North Carolina
Hart & Hickman Project No. CLT-300
S:\AAA-Master Projects\City of Charlotte - CLT\CLT-300 Brownfield Grant Activities\North Tryon Vapor Intrusion Evaluations\Griffin Vapor Intrusion Evaluation\
Soil Vapor Analytical DCE 10 30 2012
1/28/2013
Table 2
Hart & Hickman, PC1,1-Dichloroethene1,2-Dichloroethanecis-1,2-DichloroetheneTetrachloroetheneTrichloroetheneVinyl ChlorideVP-3 07/17/09 TO-15 120 <3.1 <3.0 <5.2 <4.1 <1.9
VP-4 07/17/09 TO-15 11 <3.0 <3.0 11 <4.0 <1.9
VP-5 07/17/09 TO-15 50 <3.2 <3.2 50 <4.3 <2.0
VP-5 (Dup)07/17/09 TO-15 32 <3.0 <3.0 32 <4.0 <1.9
1,760 47 NE 350 17.6 280
420 9.4 NE 83.4 4.2 16
TimeTemperature (oC)Initial 1130 29.2
Midpoint 1200 30.0Final124530.3
Notes:
1. NC DENR Inactive Hazardous Sites Branch Industrial/Commercial Vapor Intrusion Screening Table (July 2012)
2. NC DENR Inactive Hazardous Sites Branch Residential Vapor Intrusion Screening Table (July 2012)Bold value exceeds IHSB Residential Soil Gas Screening Level.Bold Underlined value exceeds IHSB Residential and Industrial/Commercial Soil Gas Screening Level.
NE = Value not established
µg/m3
IHSB Residential Vapor Intrusion Soil Gas
Screening Level 2
Stage of SamplingVP-4
Ambient Air Temperature Meaurements
Near Indoor VPs During Sample CollectionAnalytical MethodIHSB Industrial/Commercial Vapor Intrusion
Soil Gas Screening Level 1Sample IDSampling Date (mm/dd/yy)
0 2000 4000
APPROXIMATE
SCALE IN FEET
N
U.S.G.S. QUADRANGLE MAP
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
TITLE
PROJECT
SITE LOCATION MAP
IRA GRIFFIN & SONS PROPERTY
2205 -2221 NORTH TRYON STREET CHARLOTTE, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE:
10-30-12 0
1 CLT-300
CHARLOTTE EAST, NC 1967 REVISED/INSPECTED 1988
DERITA, NC 1993
SITE
APP
LABORA
PENDIX A
ATORY REPPORT
10/23/2012
Mr. Matt Ingalls
Hart & Hickman
2923 South Tryon Street
Suite 100
Charlotte NC 28203
Project Name: N. Tryon Hills Assemblege
Project #: MVT-002
Dear Mr. Matt Ingalls
The following report includes the data for the above referenced project for sample(s)
received on 7/28/2009 at Air Toxics Ltd.
The data and associated QC analyzed by Modified TO-15 are compliant with the
project requirements or laboratory criteria with the exception of the deviations noted in
the attached case narrative.
Thank you for choosing Air Toxics Ltd. for your air analysis needs. Air Toxics Ltd. is
committed to providing accurate data of the highest quality. Please feel free to contact
the Project Manager: Ausha Scott at 916-985-1000 if you have any questions regarding
the data in this report.
Regards,
Ausha Scott
Project Manager
Workorder #: 0907610R1
Page 1 of 13
Mr. Matt Ingalls
Hart & Hickman
2923 South Tryon Street
Suite 100
Charlotte, NC 28203
WORK ORDER #:0907610R1
CLIENT:BILL TO:
PHONE:
Accounts Payable
Hart & Hickman
2923 South Tryon Street
Suite 100
Charlotte, NC 28203
704-887-4617
704-586-0373
07/28/2009
DATE COMPLETED:08/12/2009
P.O. #MVT-002
PROJECT #MVT-002 N. Tryon Hills Assemblege
Work Order Summary
FAX:
DATE RECEIVED:
DATE REISSUED:10/23/2012
CONTACT:Ausha Scott
NAMEFRACTION #TEST VAC./PRES.
RECEIPT
PRESSURE
FINAL
01A VP-3 Modified TO-15 3.5 "Hg 5 psi
02A VP-4 Modified TO-15 3.0 "Hg 5 psi
02AA VP-4 Lab Duplicate Modified TO-15 3.0 "Hg 5 psi
03A VP-5 Modified TO-15 5.0 "Hg 5 psi
04A VP-5 (DUP)Modified TO-15 3.0 "Hg 5 psi
05A Lab Blank Modified TO-15 NA NA
06A CCV Modified TO-15 NA NA
07A LCS Modified TO-15 NA NA
CERTIFIED BY:
Technical Director
DATE:
Name of Accrediting Agency: NELAP/ORELAP (Oregon Environmental Laboratory Accreditation Program)
Accreditation number: CA300005, Effective date: 10/18/2011, Expiration date: 10/17/2012.
180 BLUE RAVINE ROAD, SUITE B FOLSOM, CA - 9563
(916) 985-1000 . (800) 985-5955 . FAX (916) 985-1020
10/23/12
Page 2 of 13
This report shall not be reproduced, except in full, without the written approval of Eurofins Air Toxics, Inc.
Eurofins Air Toxics Ltd. certifies that the test results contained in this report meet all requirements of the NELAC standards
Certfication numbers: AZ Licensure AZ0775, CA NELAP - 12282CA, NY NELAP - 11291,
TX NELAP - T104704434-12-5, UT NELAP CA009332012-3, WA NELAP - C935
LABORATORY NARRATIVEModified TO-15Hart & HickmanWorkorder# 0907610R1
Four 6 Liter Summa Canister samples were received on July 28, 2009. The laboratory performed
analysis via modified EPA Method TO-15 using GC/MS in the full scan mode.
This workorder was independently validated prior to submittal using 'USEPA National Functional
Guidelines' as generally applied to the analysis of volatile organic compounds in air. A rules-based,
logic driven, independent validation engine was employed to assess completeness, evaluate pass/fail of
relevant project quality control requirements and verification of all quantified amounts.
Method modifications taken to run these samples are summarized in the table below. Specific project
requirements may over-ride the ATL modifications.
Requirement ATL ModificationsTO-15
Daily CCV </= 30% Difference </= 30% Difference; Compounds exceeding this criterion
and associated data are flagged and narrated.
Sample collection media Summa canister ATL recommends use of summa canisters to insure data
defensibility, but will report results from Tedlar bags at
client request
Method Detection Limit Follow 40CFR Pt.136
App. B
The MDL met all relevant requirements in Method
TO-15 (statistical MDL less than the LOQ). The
concentration of the spiked replicate may have exceeded
10X the calculated MDL in some cases
Receiving Notes
Sample collection date was incomplete on the Chain of Custody (COC) for samples VP-4, VP-5 and
VP-5 (DUP). The sampling date was taken from the tags.
Tetrachloroethene in samples VP-5 and VP-5 (DUP) was outside of the 25% RPD crtieria for
duplicate samples. These samples appear to be field duplcaies accroding to the COC.
THE WORKORDER WAS REISSUED ON OCTOBER 23, 2012 TO REPORT
1,1-DICHLOROETHENE PER CLIENT'S REQUEST.
Analytical Notes
Eight qualifiers may have been used on the data analysis sheets and indicates as follows:
B - Compound present in laboratory blank greater than reporting limit (background subtraction not
performed).
J - Estimated value.
E - Exceeds instrument calibration range.
Definition of Data Qualifying Flags
Page 3 of 13
S - Saturated peak.
Q - Exceeds quality control limits.
U - Compound analyzed for but not detected above the reporting limit.
UJ- Non-detected compound associated with low bias in the CCV and/or LCS.
N - The identification is based on presumptive evidence.
File extensions may have been used on the data analysis sheets and indicates
as follows:
a-File was requantified
b-File was quantified by a second column and detector
r1-File was requantified for the purpose of reissue
Page 4 of 13
EPA METHOD TO-15 GC/MS FULL SCAN
Summary of Detected Compounds
Client Sample ID: VP-3
Lab ID#: 0907610R1-01A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.76 31 3.0 1201,1-Dichloroethene
Client Sample ID: VP-4
Lab ID#: 0907610R1-02A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.74 1.7 5.0 11Tetrachloroethene
Client Sample ID: VP-4 Lab Duplicate
Lab ID#: 0907610R1-02AA
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.74 1.7 5.0 11Tetrachloroethene
Client Sample ID: VP-5
Lab ID#: 0907610R1-03A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.80 7.3 5.5 50Tetrachloroethene
Client Sample ID: VP-5 (DUP)
Lab ID#: 0907610R1-04A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.74 4.6 5.0 32Tetrachloroethene
Page 5 of 13
Client Sample ID: VP-3
Lab ID#: 0907610R1-01A
EPA METHOD TO-15 GC/MS FULL SCAN
e080408r1File Name:
Dil. Factor:1.52
Date of Collection: 7/17/09 12:30:00 PM
Date of Analysis: 8/4/09 02:24 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.76 Not Detected 1.9 Not DetectedVinyl Chloride
0.76 31 3.0 1201,1-Dichloroethene
0.76 Not Detected 3.0 Not Detectedcis-1,2-Dichloroethene
0.76 Not Detected 3.1 Not Detected1,2-Dichloroethane
0.76 Not Detected 4.1 Not DetectedTrichloroethene
0.76 Not Detected 5.2 Not DetectedTetrachloroethene
Container Type: 6 Liter Summa Canister
Limits%RecoverySurrogates
Method
100 70-1301,2-Dichloroethane-d4
100 70-130Toluene-d8
102 70-1304-Bromofluorobenzene
Page 6 of 13
Client Sample ID: VP-4
Lab ID#: 0907610R1-02A
EPA METHOD TO-15 GC/MS FULL SCAN
e080409r1File Name:
Dil. Factor:1.49
Date of Collection: 7/17/09 12:45:00 PM
Date of Analysis: 8/4/09 03:14 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.74 Not Detected 1.9 Not DetectedVinyl Chloride
0.74 Not Detected 3.0 Not Detected1,1-Dichloroethene
0.74 Not Detected 3.0 Not Detectedcis-1,2-Dichloroethene
0.74 Not Detected 3.0 Not Detected1,2-Dichloroethane
0.74 Not Detected 4.0 Not DetectedTrichloroethene
0.74 1.7 5.0 11Tetrachloroethene
Container Type: 6 Liter Summa Canister
Limits%RecoverySurrogates
Method
99 70-1301,2-Dichloroethane-d4
99 70-130Toluene-d8
101 70-1304-Bromofluorobenzene
Page 7 of 13
Client Sample ID: VP-4 Lab Duplicate
Lab ID#: 0907610R1-02AA
EPA METHOD TO-15 GC/MS FULL SCAN
e080425r1File Name:
Dil. Factor:1.49
Date of Collection: 7/17/09 12:45:00 PM
Date of Analysis: 8/5/09 07:43 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.74 Not Detected 1.9 Not DetectedVinyl Chloride
0.74 Not Detected 3.0 Not Detected1,1-Dichloroethene
0.74 Not Detected 3.0 Not Detectedcis-1,2-Dichloroethene
0.74 Not Detected 3.0 Not Detected1,2-Dichloroethane
0.74 Not Detected 4.0 Not DetectedTrichloroethene
0.74 1.7 5.0 11Tetrachloroethene
Container Type: 6 Liter Summa Canister
Limits%RecoverySurrogates
Method
96 70-1301,2-Dichloroethane-d4
99 70-130Toluene-d8
101 70-1304-Bromofluorobenzene
Page 8 of 13
Client Sample ID: VP-5
Lab ID#: 0907610R1-03A
EPA METHOD TO-15 GC/MS FULL SCAN
e080410r1File Name:
Dil. Factor:1.61
Date of Collection: 7/17/09 12:20:00 PM
Date of Analysis: 8/4/09 04:04 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.80 Not Detected 2.0 Not DetectedVinyl Chloride
0.80 Not Detected 3.2 Not Detected1,1-Dichloroethene
0.80 Not Detected 3.2 Not Detectedcis-1,2-Dichloroethene
0.80 Not Detected 3.2 Not Detected1,2-Dichloroethane
0.80 Not Detected 4.3 Not DetectedTrichloroethene
0.80 7.3 5.5 50Tetrachloroethene
Container Type: 6 Liter Summa Canister
Limits%RecoverySurrogates
Method
92 70-1301,2-Dichloroethane-d4
101 70-130Toluene-d8
94 70-1304-Bromofluorobenzene
Page 9 of 13
Client Sample ID: VP-5 (DUP)
Lab ID#: 0907610R1-04A
EPA METHOD TO-15 GC/MS FULL SCAN
e080423r1File Name:
Dil. Factor:1.49
Date of Collection: 7/17/09 12:20:00 PM
Date of Analysis: 8/5/09 06:16 AM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.74 Not Detected 1.9 Not DetectedVinyl Chloride
0.74 Not Detected 3.0 Not Detected1,1-Dichloroethene
0.74 Not Detected 3.0 Not Detectedcis-1,2-Dichloroethene
0.74 Not Detected 3.0 Not Detected1,2-Dichloroethane
0.74 Not Detected 4.0 Not DetectedTrichloroethene
0.74 4.6 5.0 32Tetrachloroethene
Container Type: 6 Liter Summa Canister
Limits%RecoverySurrogates
Method
93 70-1301,2-Dichloroethane-d4
100 70-130Toluene-d8
97 70-1304-Bromofluorobenzene
Page 10 of 13
Client Sample ID: Lab Blank
Lab ID#: 0907610R1-05A
EPA METHOD TO-15 GC/MS FULL SCAN
e080405File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 8/4/09 12:08 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.50 Not Detected 1.3 Not DetectedVinyl Chloride
0.50 Not Detected 2.0 Not Detected1,1-Dichloroethene
0.50 Not Detected 2.0 Not Detectedcis-1,2-Dichloroethene
0.50 Not Detected 2.0 Not Detected1,2-Dichloroethane
0.50 Not Detected 2.7 Not DetectedTrichloroethene
0.50 Not Detected 3.4 Not DetectedTetrachloroethene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
97 70-1301,2-Dichloroethane-d4
98 70-130Toluene-d8
102 70-1304-Bromofluorobenzene
Page 11 of 13
Client Sample ID: CCV
Lab ID#: 0907610R1-06A
EPA METHOD TO-15 GC/MS FULL SCAN
e080403File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 8/4/09 10:44 AM
%RecoveryCompound
84Vinyl Chloride
861,1-Dichloroethene
87cis-1,2-Dichloroethene
861,2-Dichloroethane
87Trichloroethene
84Tetrachloroethene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
98 70-1301,2-Dichloroethane-d4
101 70-130Toluene-d8
101 70-1304-Bromofluorobenzene
Page 12 of 13
Client Sample ID: LCS
Lab ID#: 0907610R1-07A
EPA METHOD TO-15 GC/MS FULL SCAN
e080404File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 8/4/09 11:25 AM
%RecoveryCompound
97Vinyl Chloride
1131,1-Dichloroethene
103cis-1,2-Dichloroethene
1001,2-Dichloroethane
101Trichloroethene
101Tetrachloroethene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
98 70-1301,2-Dichloroethane-d4
99 70-130Toluene-d8
100 70-1304-Bromofluorobenzene
Page 13 of 13