08022_Reeves_Monitoring Rpt 20120831

ANNUAL MONITORING REPORT (2012) FORMER REEVES SITE BROWNFIELDS SITE NO. 08022-04-60 8900 RESEARCH DRIVE CHARLOTTE, MECKLENBURG CO, NC S&ME PROJECT 1354-11-006A

Prepared for:

Polymers Center of Excellence
8900 Research Drive
Charlotte, North Carolina 28104-6015

Prepared by:

S&ME, Inc.
9711 Southern Pine Boulevard
Charlotte, North Carolina 28273-5560

February 8, 2012
2012 Annual Monitoring Report S&ME Project No. 1354-11-006A
Reeves Site, Brownfields Site No. 08022-04-60, Charlotte, NC February 8, 2012

with the Notice of Brownfields Property. The April 25, 2006 letter indicated that four
monitoring wells (MW-5B, MW-5C, MW-6, and MW-7) and the adjacent stream are to
be sampled annually and analyzed for volatile organic compounds (VOCs) by
Environmental Protection Agency (EPA) Method 8260 or equivalent. The monitor wells
and stream sample locations are illustrated on Figure 3.

2. SCOPE OF SERVICES
2.1 Surface Water and Groundwater Sampling
On January 6, 2012, S&ME collected one upstream sample (SW-U) and one downstream
(SW-D) surface water sample at the approximate locations shown on Figure 3. The SW-
U sample was collected from the bridge, using a disposable bailer. The SW-D sample
was collected by directly dipping the sample container into the stream with care not to
allow sediment to enter the sample containers and not to allow overfilling to prevent the
loss of any preservatives, if present. Sample containers with appropriate preservatives
were provided by the laboratory.

On January 6, 2012, S&ME also collected groundwater samples from the following
monitor wells: MW-5B, MW-5C, MW-6, and MW-7. Prior to sampling, the depth to
water in each well was measured from the top of the well casing (TOC) and the monitor
wells were purged of three to five well volumes (or until dry) using a disposable bailer.
The samples were submitted to Pace Analytical Laboratories, Inc. (Pace) in Huntersville,
North Carolina, a North Carolina-certified laboratory, for the analysis of VOCs by EPA
Method 8260. In addition to the four monitor well samples, one duplicate sample of
MW-5B (identified as Duplicate) was additionally analyzed for quality control purposes.
Copies of the field sampling forms are included in Appendix II.

The purge water was contained in a 55-gallon drum for off-site disposal. The purge
water will be disposed off-site at a permitted facility as appropriate for hazardous or non-
hazardous waste. Documentation of disposal, (i.e., waste manifest and invoice), will be
provided to Polymers Center of Excellence upon receipt by the disposal company.
S&ME will also provide a copy of that documentation to the NCDENR, if requested by
the NCDENR.

3. RESULTS
3.1 Groundwater Flow
The depth to water in the surficial aquifer ranged from 9.73 feet below the top of casing
(flush mount well) in monitor well MW-6, to 29.18 feet below the top of casing (~2.5
feet stickup) in the monitor well MW-5B. The January 2012 groundwater levels ranged
from approximately 0.3 to 2.3 feet higher than the January 2011 groundwater levels.
Based on the top of casing elevations and the depth to water (Table 1), the groundwater
2
2012 Annual Monitoring Report S&ME Project No. 1354-11-006A
Reeves Site, Brownfields Site No. 08022-04-60, Charlotte, NC February 8, 2012

flow is generally toward the east-southeast in the general direction of Doby Creek under
a hydraulic gradient of approximately 0.028 ft/ft between monitoring wells MW-5B and
MW-6, and approximately 0.007 ft/ft between monitoring wells MW-6 and MW-7
(Figure 3).

The local vertical hydraulic gradient calculated using water levels measured in nested
monitoring wells MW-5B and MW-5C is approximately 0.004 ft/ft in the downward
direction.
3.2 Surface Water Quality
VOCs were not detected in the two surface water samples (SW-U and SW-D). The
results are summarized in Table 2, and a copy of the laboratory report is included in
Appendix I.
3.3 Groundwater Quality
No VOCs were detected in the groundwater samples from the deep monitor well MW-5C
or from the downgradient monitor well MW-7. Tetrachloroethene was detected in
monitoring well MW-5B [16.1 micrograms per liter (µg/L)] and the duplicate of MW-5B
(14.6 µg/L) as well as monitor well MW-6 (21.1 µg/L) compared to the 15A NCAC 2L
.0202 groundwater quality standard (2L Standard) of 0.7 µg/L. No other VOCs were
detected in monitoring wells MW-5B or MW-6. The results are summarized in Table 2,
and a copy of the laboratory report and the Chain-of-Custody form are included in
Appendix I.

The 2012 concentrations of tetrachloroethene were lower than those detected in 2011 by
approximately 6% in MW-5B and approximately 41% in MW-6.

The relative percent difference between sample MW-5B and its duplicate is 9.8%. No
VOCs were detected in the trip blank. All of the laboratory internal quality controls were
within acceptable limits, with the exception of one analyte (hexachloro-1,3-butadiene)
detected in the Method Blank. However, this analyte was not detected in any of the site
samples or other laboratory control samples.

3

TABLES

Table 1
Summary of Field Parameters (January 6, 2012)
Former Reeves Property (Brownfields Project No. 08022-04-60)
8900 Research Drive
Charlotte, Mecklenburg Co., North Carolina
S&ME Project No. 1354-11-006A
Monitoring Well ID
MW-5B MW-5C MW-6 MW-7
Depth to Water ft below TOC 29.18 29.17 9.73 6.81
TOC Elevation ft above MSL 632.17 632.06 609.54 605.74
BOS Elevation ft above MSL 599.85 571.77 591.04 589.54
Total Depth ft below TOC 32.35 59.80 18.85 16.23
Water Column feet 3.17 30.63 9.12 9.42
Water Level Elevation ft above MSL 602.99 602.89 599.81 598.93
Mid Point-Sampling Interval feet 601.42 575.27 NA NA
Change in Water Level
Elevation feet -0.1 NA NA
Vertical Gradient feet/feet -0.004 NA NA
Temperature °C 16.2 14.6 15.3 16.1
pH Standard Units 6.8 7.3 7.0 7.6
Conductivity µS/cm 191 136 154 88
Notes:
ft : feet
TOC : Top of Casing of the well
MSL : Mean Sea Level
°C : Degrees Celcius
µS/cm: micro siemens per centimeter
NA - Not Applicable
Parameter Unit
S:\1354\PROJECT\2011\11-001 - 11-050\11-006A Reeves Site\11-006A Tables.xls, Field Parameters
Table 2
Summary of Water Sampling Results
Former Reeves Property (Brownfields Project No. 08022-04-60)
8900 Research Drive
Charlotte, Mecklenburg Co., North Carolina
S&ME Project No. 1354-11-006A
Well / Surface Water Sample ID 2L
MW-5B DUPLICATE MW-5C MW-6 MW-7 SW-U SW-D Standard
05/04/04 150 150 2.7 24 5.4 --- ---
05/08/06 50 71 1.2 15 <0.16 <0.16 <0.16
08/09/07 42.8 38.9 1 38.3 <1.0 <1.0 <1.0
03/11/08 92 <1.0 (7) <1.0 38 <1.0 <1.0 <1.0
01/29/09 31.6 31.9 <1.0 27.8 <1.0 <1.0 <1.0
02/24/10 13.2 11.9 <1.0 25.9 <1.0 <1.0 <1.0
01/20/11 17.1 <1.0 (5C)1.1 35.9 <1.0 <1.0 <1.0
01/06/12 16.1 14.6 <1.0 21.1 <1.0 <1.0 <1.0
05/08/06 <0.26 <0.26 <0.26 2.7 <0.26 <0.26 <0.26
08/09/07 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
03/11/08 <1.0 <1.0 (7) <1.0 <1.0 <1.0 <1.0 <1.0
01/29/09 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
02/24/10 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
01/20/11 <1.0 <1.0 (5C) <1.0 <1.0 <1.0 <1.0 <1.0
01/06/12 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
05/08/06 13 17 <0.35 <0.35 <0.35 <0.35 <0.35
08/09/07 5.5 4.9 <1.0 <1.0 <1.0 <1.0 <1.0
03/11/08 6.9 <1.0 (7) <1.0 <1.0 <1.0 <1.0 <1.0
01/29/09 2.3 2.3 <1.0 <1.0 <1.0 <1.0 <1.0
02/24/10 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
01/20/11 <1.0 <1.0 (5C) <1.0 <1.0 <1.0 <1.0 <1.0
01/06/12 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
05/08/06 <0.33 <0.33 <0.33 1.2 <0.33 <0.33 <0.33
08/09/07 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
03/11/08 <1.0 <1.0 (7) <1.0 <1.0 <1.0 <1.0 <1.0
01/29/09 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
02/24/10 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
01/20/11 <1.0 <1.0 (5C) <1.0 <1.0 <1.0 <1.0 <1.0
01/06/12 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
05/08/06 1.4 1.9 <0.39 <0.39 <0.39 <0.39 <0.39
08/09/07 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
03/11/08 1.3 <1.0 (7) <1.0 <1.0 <1.0 <1.0 <1.0
01/29/09 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
02/24/10 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
01/20/11 <1.0 <1.0 (5C) <1.0 <1.0 <1.0 <1.0 <1.0
01/06/12 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
1,1-Dichloro-
ethene µg/L 7
0.7
Trichloro-
ethene µg/L
cis-1,2-Dichloro-
ethene
Tetrachloro-
ethene
µg/L
3
200
70
DateCompound Unit
1,1,1-Trichloro-
ethane µg/L
µg/L
Page 1 of 2
Table 2
Summary of Water Sampling Results
Former Reeves Property (Brownfields Project No. 08022-04-60)
8900 Research Drive
Charlotte, Mecklenburg Co., North Carolina
S&ME Project No. 1354-11-006A
Well / Surface Water Sample ID 2L
MW-5B DUPLICATE MW-5C MW-6 MW-7 SW-U SW-D StandardDateCompound Unit
05/04/04 --- --- 1.1 --- --- --- ---
05/08/06 <0.29 <0.29 1.1 <0.29 <0.29 <0.29 <0.29
08/09/07 <1.0 <1.0 1.1 <1.0 <1.0 <1.0 <1.0
03/11/08 <1.0 <1.0 (7)1.0 <1.0 <1.0 <1.0 <1.0
01/29/09 <1.0 <1.0 1.0 <1.0 <1.0 <1.0 <1.0
02/24/10 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
01/20/11 <1.0 1.0 (5C)1.1 <1.0 <1.0 <1.0 <1.0
01/06/12 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
Notes:
The May 4, 2004 data obtained from the Notice of Brownfields Property
Sample ID "Duplicate" is a duplicate of MW-5B, unless noted otherwise with the well # in parentheses (7) = (MW-7)
µg/L : micrograms per liter
2L Standard : 15A NCAC 2L .0202 Groundwater Quality Standard
Highlighted and underlined values exceed 2L Standards
Chloroform µg/L 70
Page 2 of 2

FIGURES

.

Circles are ~1000 ft, 1500 ft, and 1 mile radii centered near
monitor wells MW-5A, MW-5B and MW-5C
Scale: As Shown
Checked by: BLD
Drawn by: WAQ
Date: 02-08-2012
SITE LOCATION MAP
Former Reeves Property
8900 Research Drive
Charlotte, North Carolina

Figure

1
S&ME Job No.: 1354-11-006A

Source: USGS Topographic Map obtained from http://terraserver-usa.com

1,500 Feet

Scale: As Shown
Checked by: BLD
Drawn by: WAQ
Date: 02-08-2012
SITE AERIAL MAP
Reeves Site (BF# 08022-04-60)
8900 Research Drive
Charlotte, North Carolina

Figure

2
S&ME Job No.: 1354-11-006A

Source: Mecklenburg County POLARIS website250 Feet
SITE

APPENDIX I

Laboratory Report and Chain of Custody

January 10, 2012
LIMS USE: FR - AL QUARLES
LIMS OBJECT ID: 92109776
92109776
Project:
Pace Project No.:
RE:
Mr. Al Quarles
S&ME, Inc.
9751 Southern Pine Blvd.
Charlotte, NC 28273
FORMER REEVES SITE
Dear Mr. Quarles:
Enclosed are the analytical results for sample(s) received by the laboratory on January 06, 2012.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Herring
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
CERTIFICATIONS
Pace Project No.:
Project:
92109776
FORMER REEVES SITE
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001South Carolina Drinking Water Cert. #: 99006003Virginia Drinking Water Certification #: 00213
Connecticut Certification #: PH-0104Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84Louisiana DHH Drinking Water # LA 100031West Virginia Certification #: 357Virginia/VELAP Certification #: 460144
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92109776
FORMER REEVES SITE
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92109776001 SW-D EPA 8260 63 PASI-CMCK
92109776002 SW-U EPA 8260 63 PASI-CMCK
92109776003 MW-5B EPA 8260 63 PASI-CMCK
92109776004 MW-5C EPA 8260 63 PASI-CMCK
92109776005 MW-6 EPA 8260 63 PASI-CMCK
92109776006 MW-7 EPA 8260 63 PASI-CMCK
92109776007 DUP EPA 8260 63 PASI-CMCK
92109776008 TRIP BLANK EPA 8260 63 PASI-CMCK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
HITS ONLY
Pace Project No.:
Project:
92109776
FORMER REEVES SITE
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92109776003 MW-5B
Tetrachloroethene 16.1 ug/L 01/09/12 12:591.0EPA 8260
92109776004 MW-5C
Chloroform <1.0 ug/L 01/09/12 13:241.0EPA 8260
92109776005 MW-6
Tetrachloroethene 21.1 ug/L 01/09/12 13:481.0EPA 8260
Trichlorofluoromethane <1.0 ug/L 01/09/12 13:481.0EPA 8260
92109776007 DUP
Tetrachloroethene 14.6 ug/L 01/09/12 14:361.0EPA 8260
92109776008 TRIP BLANK
Acetone <25.0 ug/L 01/09/12 11:4625.0EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
PROJECT NARRATIVE
Pace Project No.:
Project:
92109776
FORMER REEVES SITE
Method:
Client:S&ME, Inc.
EPA 8260
Date:January 10, 2012
Description:8260 MSV Low Level
General Information:
8 samples were analyzed for EPA 8260. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank with any exceptions noted below.
QC Batch: MSV/17864
B-: Analyte detected in method blank but was not detected in the associated samples.
• BLANK (Lab ID: 707960)
• Hexachloro-1,3-butadiene
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92109776
FORMER REEVES SITE
Sample:SW-D Lab ID:92109776001 Collected:01/06/12 11:05 Received:01/06/12 15:42 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone <25.0 ug/L 1 01/09/12 12:11 67-64-125.0
Benzene <1.0 ug/L 1 01/09/12 12:11 71-43-21.0
Bromobenzene <1.0 ug/L 1 01/09/12 12:11 108-86-11.0
Bromochloromethane <1.0 ug/L 1 01/09/12 12:11 74-97-51.0
Bromodichloromethane <1.0 ug/L 1 01/09/12 12:11 75-27-41.0
Bromoform <1.0 ug/L 1 01/09/12 12:11 75-25-21.0
Bromomethane <2.0 ug/L 1 01/09/12 12:11 74-83-92.0
2-Butanone (MEK)<5.0 ug/L 1 01/09/12 12:11 78-93-35.0
Carbon tetrachloride <1.0 ug/L 1 01/09/12 12:11 56-23-51.0
Chlorobenzene <1.0 ug/L 1 01/09/12 12:11 108-90-71.0
Chloroethane <1.0 ug/L 1 01/09/12 12:11 75-00-31.0
Chloroform <1.0 ug/L 1 01/09/12 12:11 67-66-31.0
Chloromethane <1.0 ug/L 1 01/09/12 12:11 74-87-31.0
2-Chlorotoluene <1.0 ug/L 1 01/09/12 12:11 95-49-81.0
4-Chlorotoluene <1.0 ug/L 1 01/09/12 12:11 106-43-41.0
1,2-Dibromo-3-chloropropane <5.0 ug/L 1 01/09/12 12:11 96-12-85.0
Dibromochloromethane <1.0 ug/L 1 01/09/12 12:11 124-48-11.0
1,2-Dibromoethane (EDB)<1.0 ug/L 1 01/09/12 12:11 106-93-41.0
Dibromomethane <1.0 ug/L 1 01/09/12 12:11 74-95-31.0
1,2-Dichlorobenzene <1.0 ug/L 1 01/09/12 12:11 95-50-11.0
1,3-Dichlorobenzene <1.0 ug/L 1 01/09/12 12:11 541-73-11.0
1,4-Dichlorobenzene <1.0 ug/L 1 01/09/12 12:11 106-46-71.0
Dichlorodifluoromethane <1.0 ug/L 1 01/09/12 12:11 75-71-81.0
1,1-Dichloroethane <1.0 ug/L 1 01/09/12 12:11 75-34-31.0
1,2-Dichloroethane <1.0 ug/L 1 01/09/12 12:11 107-06-21.0
1,1-Dichloroethene <1.0 ug/L 1 01/09/12 12:11 75-35-41.0
cis-1,2-Dichloroethene <1.0 ug/L 1 01/09/12 12:11 156-59-21.0
trans-1,2-Dichloroethene <1.0 ug/L 1 01/09/12 12:11 156-60-51.0
1,2-Dichloropropane <1.0 ug/L 1 01/09/12 12:11 78-87-51.0
1,3-Dichloropropane <1.0 ug/L 1 01/09/12 12:11 142-28-91.0
2,2-Dichloropropane <1.0 ug/L 1 01/09/12 12:11 594-20-71.0
1,1-Dichloropropene <1.0 ug/L 1 01/09/12 12:11 563-58-61.0
cis-1,3-Dichloropropene <1.0 ug/L 1 01/09/12 12:11 10061-01-51.0
trans-1,3-Dichloropropene <1.0 ug/L 1 01/09/12 12:11 10061-02-61.0
Diisopropyl ether <1.0 ug/L 1 01/09/12 12:11 108-20-31.0
Ethylbenzene <1.0 ug/L 1 01/09/12 12:11 100-41-41.0
Hexachloro-1,3-butadiene <1.0 ug/L 1 01/09/12 12:11 87-68-31.0
2-Hexanone <5.0 ug/L 1 01/09/12 12:11 591-78-65.0
p-Isopropyltoluene <1.0 ug/L 1 01/09/12 12:11 99-87-61.0
Methylene Chloride <2.0 ug/L 1 01/09/12 12:11 75-09-22.0
4-Methyl-2-pentanone (MIBK)<5.0 ug/L 1 01/09/12 12:11 108-10-15.0
Methyl-tert-butyl ether <1.0 ug/L 1 01/09/12 12:11 1634-04-41.0
Naphthalene <1.0 ug/L 1 01/09/12 12:11 91-20-31.0
Styrene <1.0 ug/L 1 01/09/12 12:11 100-42-51.0
1,1,1,2-Tetrachloroethane <1.0 ug/L 1 01/09/12 12:11 630-20-61.0
1,1,2,2-Tetrachloroethane <1.0 ug/L 1 01/09/12 12:11 79-34-51.0
Tetrachloroethene <1.0 ug/L 1 01/09/12 12:11 127-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/10/2012 02:58 PM Page 6 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92109776
FORMER REEVES SITE
Sample:SW-D Lab ID:92109776001 Collected:01/06/12 11:05 Received:01/06/12 15:42 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene <1.0 ug/L 1 01/09/12 12:11 108-88-31.0
1,2,3-Trichlorobenzene <1.0 ug/L 1 01/09/12 12:11 87-61-61.0
1,2,4-Trichlorobenzene <1.0 ug/L 1 01/09/12 12:11 120-82-11.0
1,1,1-Trichloroethane <1.0 ug/L 1 01/09/12 12:11 71-55-61.0
1,1,2-Trichloroethane <1.0 ug/L 1 01/09/12 12:11 79-00-51.0
Trichloroethene <1.0 ug/L 1 01/09/12 12:11 79-01-61.0
Trichlorofluoromethane <1.0 ug/L 1 01/09/12 12:11 75-69-41.0
1,2,3-Trichloropropane <1.0 ug/L 1 01/09/12 12:11 96-18-41.0
Vinyl acetate <2.0 ug/L 1 01/09/12 12:11 108-05-42.0
Vinyl chloride <1.0 ug/L 1 01/09/12 12:11 75-01-41.0
m&p-Xylene <2.0 ug/L 1 01/09/12 12:11 179601-23-12.0
o-Xylene <1.0 ug/L 1 01/09/12 12:11 95-47-61.0
Surrogates
4-Bromofluorobenzene (S)96 %1 01/09/12 12:11 460-00-470-130
Dibromofluoromethane (S)105 %1 01/09/12 12:11 1868-53-770-130
1,2-Dichloroethane-d4 (S)102 %1 01/09/12 12:11 17060-07-070-130
Toluene-d8 (S)100 %1 01/09/12 12:11 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/10/2012 02:58 PM Page 7 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92109776
FORMER REEVES SITE
Sample:SW-U Lab ID:92109776002 Collected:01/06/12 11:30 Received:01/06/12 15:42 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone <25.0 ug/L 1 01/09/12 12:35 67-64-125.0
Benzene <1.0 ug/L 1 01/09/12 12:35 71-43-21.0
Bromobenzene <1.0 ug/L 1 01/09/12 12:35 108-86-11.0
Bromochloromethane <1.0 ug/L 1 01/09/12 12:35 74-97-51.0
Bromodichloromethane <1.0 ug/L 1 01/09/12 12:35 75-27-41.0
Bromoform <1.0 ug/L 1 01/09/12 12:35 75-25-21.0
Bromomethane <2.0 ug/L 1 01/09/12 12:35 74-83-92.0
2-Butanone (MEK)<5.0 ug/L 1 01/09/12 12:35 78-93-35.0
Carbon tetrachloride <1.0 ug/L 1 01/09/12 12:35 56-23-51.0
Chlorobenzene <1.0 ug/L 1 01/09/12 12:35 108-90-71.0
Chloroethane <1.0 ug/L 1 01/09/12 12:35 75-00-31.0
Chloroform <1.0 ug/L 1 01/09/12 12:35 67-66-31.0
Chloromethane <1.0 ug/L 1 01/09/12 12:35 74-87-31.0
2-Chlorotoluene <1.0 ug/L 1 01/09/12 12:35 95-49-81.0
4-Chlorotoluene <1.0 ug/L 1 01/09/12 12:35 106-43-41.0
1,2-Dibromo-3-chloropropane <5.0 ug/L 1 01/09/12 12:35 96-12-85.0
Dibromochloromethane <1.0 ug/L 1 01/09/12 12:35 124-48-11.0
1,2-Dibromoethane (EDB)<1.0 ug/L 1 01/09/12 12:35 106-93-41.0
Dibromomethane <1.0 ug/L 1 01/09/12 12:35 74-95-31.0
1,2-Dichlorobenzene <1.0 ug/L 1 01/09/12 12:35 95-50-11.0
1,3-Dichlorobenzene <1.0 ug/L 1 01/09/12 12:35 541-73-11.0
1,4-Dichlorobenzene <1.0 ug/L 1 01/09/12 12:35 106-46-71.0
Dichlorodifluoromethane <1.0 ug/L 1 01/09/12 12:35 75-71-81.0
1,1-Dichloroethane <1.0 ug/L 1 01/09/12 12:35 75-34-31.0
1,2-Dichloroethane <1.0 ug/L 1 01/09/12 12:35 107-06-21.0
1,1-Dichloroethene <1.0 ug/L 1 01/09/12 12:35 75-35-41.0
cis-1,2-Dichloroethene <1.0 ug/L 1 01/09/12 12:35 156-59-21.0
trans-1,2-Dichloroethene <1.0 ug/L 1 01/09/12 12:35 156-60-51.0
1,2-Dichloropropane <1.0 ug/L 1 01/09/12 12:35 78-87-51.0
1,3-Dichloropropane <1.0 ug/L 1 01/09/12 12:35 142-28-91.0
2,2-Dichloropropane <1.0 ug/L 1 01/09/12 12:35 594-20-71.0
1,1-Dichloropropene <1.0 ug/L 1 01/09/12 12:35 563-58-61.0
cis-1,3-Dichloropropene <1.0 ug/L 1 01/09/12 12:35 10061-01-51.0
trans-1,3-Dichloropropene <1.0 ug/L 1 01/09/12 12:35 10061-02-61.0
Diisopropyl ether <1.0 ug/L 1 01/09/12 12:35 108-20-31.0
Ethylbenzene <1.0 ug/L 1 01/09/12 12:35 100-41-41.0
Hexachloro-1,3-butadiene <1.0 ug/L 1 01/09/12 12:35 87-68-31.0
2-Hexanone <5.0 ug/L 1 01/09/12 12:35 591-78-65.0
p-Isopropyltoluene <1.0 ug/L 1 01/09/12 12:35 99-87-61.0
Methylene Chloride <2.0 ug/L 1 01/09/12 12:35 75-09-22.0
4-Methyl-2-pentanone (MIBK)<5.0 ug/L 1 01/09/12 12:35 108-10-15.0
Methyl-tert-butyl ether <1.0 ug/L 1 01/09/12 12:35 1634-04-41.0
Naphthalene <1.0 ug/L 1 01/09/12 12:35 91-20-31.0
Styrene <1.0 ug/L 1 01/09/12 12:35 100-42-51.0
1,1,1,2-Tetrachloroethane <1.0 ug/L 1 01/09/12 12:35 630-20-61.0
1,1,2,2-Tetrachloroethane <1.0 ug/L 1 01/09/12 12:35 79-34-51.0
Tetrachloroethene <1.0 ug/L 1 01/09/12 12:35 127-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/10/2012 02:58 PM Page 8 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92109776
FORMER REEVES SITE
Sample:SW-U Lab ID:92109776002 Collected:01/06/12 11:30 Received:01/06/12 15:42 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene <1.0 ug/L 1 01/09/12 12:35 108-88-31.0
1,2,3-Trichlorobenzene <1.0 ug/L 1 01/09/12 12:35 87-61-61.0
1,2,4-Trichlorobenzene <1.0 ug/L 1 01/09/12 12:35 120-82-11.0
1,1,1-Trichloroethane <1.0 ug/L 1 01/09/12 12:35 71-55-61.0
1,1,2-Trichloroethane <1.0 ug/L 1 01/09/12 12:35 79-00-51.0
Trichloroethene <1.0 ug/L 1 01/09/12 12:35 79-01-61.0
Trichlorofluoromethane <1.0 ug/L 1 01/09/12 12:35 75-69-41.0
1,2,3-Trichloropropane <1.0 ug/L 1 01/09/12 12:35 96-18-41.0
Vinyl acetate <2.0 ug/L 1 01/09/12 12:35 108-05-42.0
Vinyl chloride <1.0 ug/L 1 01/09/12 12:35 75-01-41.0
m&p-Xylene <2.0 ug/L 1 01/09/12 12:35 179601-23-12.0
o-Xylene <1.0 ug/L 1 01/09/12 12:35 95-47-61.0
Surrogates
4-Bromofluorobenzene (S)95 %1 01/09/12 12:35 460-00-470-130
Dibromofluoromethane (S)106 %1 01/09/12 12:35 1868-53-770-130
1,2-Dichloroethane-d4 (S)101 %1 01/09/12 12:35 17060-07-070-130
Toluene-d8 (S)100 %1 01/09/12 12:35 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/10/2012 02:58 PM Page 9 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92109776
FORMER REEVES SITE
Sample:MW-5B Lab ID:92109776003 Collected:01/06/12 14:15 Received:01/06/12 15:42 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone <25.0 ug/L 1 01/09/12 12:59 67-64-125.0
Benzene <1.0 ug/L 1 01/09/12 12:59 71-43-21.0
Bromobenzene <1.0 ug/L 1 01/09/12 12:59 108-86-11.0
Bromochloromethane <1.0 ug/L 1 01/09/12 12:59 74-97-51.0
Bromodichloromethane <1.0 ug/L 1 01/09/12 12:59 75-27-41.0
Bromoform <1.0 ug/L 1 01/09/12 12:59 75-25-21.0
Bromomethane <2.0 ug/L 1 01/09/12 12:59 74-83-92.0
2-Butanone (MEK)<5.0 ug/L 1 01/09/12 12:59 78-93-35.0
Carbon tetrachloride <1.0 ug/L 1 01/09/12 12:59 56-23-51.0
Chlorobenzene <1.0 ug/L 1 01/09/12 12:59 108-90-71.0
Chloroethane <1.0 ug/L 1 01/09/12 12:59 75-00-31.0
Chloroform <1.0 ug/L 1 01/09/12 12:59 67-66-31.0
Chloromethane <1.0 ug/L 1 01/09/12 12:59 74-87-31.0
2-Chlorotoluene <1.0 ug/L 1 01/09/12 12:59 95-49-81.0
4-Chlorotoluene <1.0 ug/L 1 01/09/12 12:59 106-43-41.0
1,2-Dibromo-3-chloropropane <5.0 ug/L 1 01/09/12 12:59 96-12-85.0
Dibromochloromethane <1.0 ug/L 1 01/09/12 12:59 124-48-11.0
1,2-Dibromoethane (EDB)<1.0 ug/L 1 01/09/12 12:59 106-93-41.0
Dibromomethane <1.0 ug/L 1 01/09/12 12:59 74-95-31.0
1,2-Dichlorobenzene <1.0 ug/L 1 01/09/12 12:59 95-50-11.0
1,3-Dichlorobenzene <1.0 ug/L 1 01/09/12 12:59 541-73-11.0
1,4-Dichlorobenzene <1.0 ug/L 1 01/09/12 12:59 106-46-71.0
Dichlorodifluoromethane <1.0 ug/L 1 01/09/12 12:59 75-71-81.0
1,1-Dichloroethane <1.0 ug/L 1 01/09/12 12:59 75-34-31.0
1,2-Dichloroethane <1.0 ug/L 1 01/09/12 12:59 107-06-21.0
1,1-Dichloroethene <1.0 ug/L 1 01/09/12 12:59 75-35-41.0
cis-1,2-Dichloroethene <1.0 ug/L 1 01/09/12 12:59 156-59-21.0
trans-1,2-Dichloroethene <1.0 ug/L 1 01/09/12 12:59 156-60-51.0
1,2-Dichloropropane <1.0 ug/L 1 01/09/12 12:59 78-87-51.0
1,3-Dichloropropane <1.0 ug/L 1 01/09/12 12:59 142-28-91.0
2,2-Dichloropropane <1.0 ug/L 1 01/09/12 12:59 594-20-71.0
1,1-Dichloropropene <1.0 ug/L 1 01/09/12 12:59 563-58-61.0
cis-1,3-Dichloropropene <1.0 ug/L 1 01/09/12 12:59 10061-01-51.0
trans-1,3-Dichloropropene <1.0 ug/L 1 01/09/12 12:59 10061-02-61.0
Diisopropyl ether <1.0 ug/L 1 01/09/12 12:59 108-20-31.0
Ethylbenzene <1.0 ug/L 1 01/09/12 12:59 100-41-41.0
Hexachloro-1,3-butadiene <1.0 ug/L 1 01/09/12 12:59 87-68-31.0
2-Hexanone <5.0 ug/L 1 01/09/12 12:59 591-78-65.0
p-Isopropyltoluene <1.0 ug/L 1 01/09/12 12:59 99-87-61.0
Methylene Chloride <2.0 ug/L 1 01/09/12 12:59 75-09-22.0
4-Methyl-2-pentanone (MIBK)<5.0 ug/L 1 01/09/12 12:59 108-10-15.0
Methyl-tert-butyl ether <1.0 ug/L 1 01/09/12 12:59 1634-04-41.0
Naphthalene <1.0 ug/L 1 01/09/12 12:59 91-20-31.0
Styrene <1.0 ug/L 1 01/09/12 12:59 100-42-51.0
1,1,1,2-Tetrachloroethane <1.0 ug/L 1 01/09/12 12:59 630-20-61.0
1,1,2,2-Tetrachloroethane <1.0 ug/L 1 01/09/12 12:59 79-34-51.0
Tetrachloroethene 16.1 ug/L 1 01/09/12 12:59 127-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/10/2012 02:58 PM Page 10 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92109776
FORMER REEVES SITE
Sample:MW-5B Lab ID:92109776003 Collected:01/06/12 14:15 Received:01/06/12 15:42 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene <1.0 ug/L 1 01/09/12 12:59 108-88-31.0
1,2,3-Trichlorobenzene <1.0 ug/L 1 01/09/12 12:59 87-61-61.0
1,2,4-Trichlorobenzene <1.0 ug/L 1 01/09/12 12:59 120-82-11.0
1,1,1-Trichloroethane <1.0 ug/L 1 01/09/12 12:59 71-55-61.0
1,1,2-Trichloroethane <1.0 ug/L 1 01/09/12 12:59 79-00-51.0
Trichloroethene <1.0 ug/L 1 01/09/12 12:59 79-01-61.0
Trichlorofluoromethane <1.0 ug/L 1 01/09/12 12:59 75-69-41.0
1,2,3-Trichloropropane <1.0 ug/L 1 01/09/12 12:59 96-18-41.0
Vinyl acetate <2.0 ug/L 1 01/09/12 12:59 108-05-42.0
Vinyl chloride <1.0 ug/L 1 01/09/12 12:59 75-01-41.0
m&p-Xylene <2.0 ug/L 1 01/09/12 12:59 179601-23-12.0
o-Xylene <1.0 ug/L 1 01/09/12 12:59 95-47-61.0
Surrogates
4-Bromofluorobenzene (S)99 %1 01/09/12 12:59 460-00-470-130
Dibromofluoromethane (S)104 %1 01/09/12 12:59 1868-53-770-130
1,2-Dichloroethane-d4 (S)103 %1 01/09/12 12:59 17060-07-070-130
Toluene-d8 (S)101 %1 01/09/12 12:59 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/10/2012 02:58 PM Page 11 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92109776
FORMER REEVES SITE
Sample:MW-5C Lab ID:92109776004 Collected:01/06/12 13:10 Received:01/06/12 15:42 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone <25.0 ug/L 1 01/09/12 13:24 67-64-125.0
Benzene <1.0 ug/L 1 01/09/12 13:24 71-43-21.0
Bromobenzene <1.0 ug/L 1 01/09/12 13:24 108-86-11.0
Bromochloromethane <1.0 ug/L 1 01/09/12 13:24 74-97-51.0
Bromodichloromethane <1.0 ug/L 1 01/09/12 13:24 75-27-41.0
Bromoform <1.0 ug/L 1 01/09/12 13:24 75-25-21.0
Bromomethane <2.0 ug/L 1 01/09/12 13:24 74-83-92.0
2-Butanone (MEK)<5.0 ug/L 1 01/09/12 13:24 78-93-35.0
Carbon tetrachloride <1.0 ug/L 1 01/09/12 13:24 56-23-51.0
Chlorobenzene <1.0 ug/L 1 01/09/12 13:24 108-90-71.0
Chloroethane <1.0 ug/L 1 01/09/12 13:24 75-00-31.0
Chloroform <1.0 ug/L 1 01/09/12 13:24 67-66-31.0
Chloromethane <1.0 ug/L 1 01/09/12 13:24 74-87-31.0
2-Chlorotoluene <1.0 ug/L 1 01/09/12 13:24 95-49-81.0
4-Chlorotoluene <1.0 ug/L 1 01/09/12 13:24 106-43-41.0
1,2-Dibromo-3-chloropropane <5.0 ug/L 1 01/09/12 13:24 96-12-85.0
Dibromochloromethane <1.0 ug/L 1 01/09/12 13:24 124-48-11.0
1,2-Dibromoethane (EDB)<1.0 ug/L 1 01/09/12 13:24 106-93-41.0
Dibromomethane <1.0 ug/L 1 01/09/12 13:24 74-95-31.0
1,2-Dichlorobenzene <1.0 ug/L 1 01/09/12 13:24 95-50-11.0
1,3-Dichlorobenzene <1.0 ug/L 1 01/09/12 13:24 541-73-11.0
1,4-Dichlorobenzene <1.0 ug/L 1 01/09/12 13:24 106-46-71.0
Dichlorodifluoromethane <1.0 ug/L 1 01/09/12 13:24 75-71-81.0
1,1-Dichloroethane <1.0 ug/L 1 01/09/12 13:24 75-34-31.0
1,2-Dichloroethane <1.0 ug/L 1 01/09/12 13:24 107-06-21.0
1,1-Dichloroethene <1.0 ug/L 1 01/09/12 13:24 75-35-41.0
cis-1,2-Dichloroethene <1.0 ug/L 1 01/09/12 13:24 156-59-21.0
trans-1,2-Dichloroethene <1.0 ug/L 1 01/09/12 13:24 156-60-51.0
1,2-Dichloropropane <1.0 ug/L 1 01/09/12 13:24 78-87-51.0
1,3-Dichloropropane <1.0 ug/L 1 01/09/12 13:24 142-28-91.0
2,2-Dichloropropane <1.0 ug/L 1 01/09/12 13:24 594-20-71.0
1,1-Dichloropropene <1.0 ug/L 1 01/09/12 13:24 563-58-61.0
cis-1,3-Dichloropropene <1.0 ug/L 1 01/09/12 13:24 10061-01-51.0
trans-1,3-Dichloropropene <1.0 ug/L 1 01/09/12 13:24 10061-02-61.0
Diisopropyl ether <1.0 ug/L 1 01/09/12 13:24 108-20-31.0
Ethylbenzene <1.0 ug/L 1 01/09/12 13:24 100-41-41.0
Hexachloro-1,3-butadiene <1.0 ug/L 1 01/09/12 13:24 87-68-31.0
2-Hexanone <5.0 ug/L 1 01/09/12 13:24 591-78-65.0
p-Isopropyltoluene <1.0 ug/L 1 01/09/12 13:24 99-87-61.0
Methylene Chloride <2.0 ug/L 1 01/09/12 13:24 75-09-22.0
4-Methyl-2-pentanone (MIBK)<5.0 ug/L 1 01/09/12 13:24 108-10-15.0
Methyl-tert-butyl ether <1.0 ug/L 1 01/09/12 13:24 1634-04-41.0
Naphthalene <1.0 ug/L 1 01/09/12 13:24 91-20-31.0
Styrene <1.0 ug/L 1 01/09/12 13:24 100-42-51.0
1,1,1,2-Tetrachloroethane <1.0 ug/L 1 01/09/12 13:24 630-20-61.0
1,1,2,2-Tetrachloroethane <1.0 ug/L 1 01/09/12 13:24 79-34-51.0
Tetrachloroethene <1.0 ug/L 1 01/09/12 13:24 127-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/10/2012 02:58 PM Page 12 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92109776
FORMER REEVES SITE
Sample:MW-5C Lab ID:92109776004 Collected:01/06/12 13:10 Received:01/06/12 15:42 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene <1.0 ug/L 1 01/09/12 13:24 108-88-31.0
1,2,3-Trichlorobenzene <1.0 ug/L 1 01/09/12 13:24 87-61-61.0
1,2,4-Trichlorobenzene <1.0 ug/L 1 01/09/12 13:24 120-82-11.0
1,1,1-Trichloroethane <1.0 ug/L 1 01/09/12 13:24 71-55-61.0
1,1,2-Trichloroethane <1.0 ug/L 1 01/09/12 13:24 79-00-51.0
Trichloroethene <1.0 ug/L 1 01/09/12 13:24 79-01-61.0
Trichlorofluoromethane <1.0 ug/L 1 01/09/12 13:24 75-69-41.0
1,2,3-Trichloropropane <1.0 ug/L 1 01/09/12 13:24 96-18-41.0
Vinyl acetate <2.0 ug/L 1 01/09/12 13:24 108-05-42.0
Vinyl chloride <1.0 ug/L 1 01/09/12 13:24 75-01-41.0
m&p-Xylene <2.0 ug/L 1 01/09/12 13:24 179601-23-12.0
o-Xylene <1.0 ug/L 1 01/09/12 13:24 95-47-61.0
Surrogates
4-Bromofluorobenzene (S)93 %1 01/09/12 13:24 460-00-470-130
Dibromofluoromethane (S)103 %1 01/09/12 13:24 1868-53-770-130
1,2-Dichloroethane-d4 (S)105 %1 01/09/12 13:24 17060-07-070-130
Toluene-d8 (S)103 %1 01/09/12 13:24 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/10/2012 02:58 PM Page 13 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92109776
FORMER REEVES SITE
Sample:MW-6 Lab ID:92109776005 Collected:01/06/12 14:30 Received:01/06/12 15:42 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone <25.0 ug/L 1 01/09/12 13:48 67-64-125.0
Benzene <1.0 ug/L 1 01/09/12 13:48 71-43-21.0
Bromobenzene <1.0 ug/L 1 01/09/12 13:48 108-86-11.0
Bromochloromethane <1.0 ug/L 1 01/09/12 13:48 74-97-51.0
Bromodichloromethane <1.0 ug/L 1 01/09/12 13:48 75-27-41.0
Bromoform <1.0 ug/L 1 01/09/12 13:48 75-25-21.0
Bromomethane <2.0 ug/L 1 01/09/12 13:48 74-83-92.0
2-Butanone (MEK)<5.0 ug/L 1 01/09/12 13:48 78-93-35.0
Carbon tetrachloride <1.0 ug/L 1 01/09/12 13:48 56-23-51.0
Chlorobenzene <1.0 ug/L 1 01/09/12 13:48 108-90-71.0
Chloroethane <1.0 ug/L 1 01/09/12 13:48 75-00-31.0
Chloroform <1.0 ug/L 1 01/09/12 13:48 67-66-31.0
Chloromethane <1.0 ug/L 1 01/09/12 13:48 74-87-31.0
2-Chlorotoluene <1.0 ug/L 1 01/09/12 13:48 95-49-81.0
4-Chlorotoluene <1.0 ug/L 1 01/09/12 13:48 106-43-41.0
1,2-Dibromo-3-chloropropane <5.0 ug/L 1 01/09/12 13:48 96-12-85.0
Dibromochloromethane <1.0 ug/L 1 01/09/12 13:48 124-48-11.0
1,2-Dibromoethane (EDB)<1.0 ug/L 1 01/09/12 13:48 106-93-41.0
Dibromomethane <1.0 ug/L 1 01/09/12 13:48 74-95-31.0
1,2-Dichlorobenzene <1.0 ug/L 1 01/09/12 13:48 95-50-11.0
1,3-Dichlorobenzene <1.0 ug/L 1 01/09/12 13:48 541-73-11.0
1,4-Dichlorobenzene <1.0 ug/L 1 01/09/12 13:48 106-46-71.0
Dichlorodifluoromethane <1.0 ug/L 1 01/09/12 13:48 75-71-81.0
1,1-Dichloroethane <1.0 ug/L 1 01/09/12 13:48 75-34-31.0
1,2-Dichloroethane <1.0 ug/L 1 01/09/12 13:48 107-06-21.0
1,1-Dichloroethene <1.0 ug/L 1 01/09/12 13:48 75-35-41.0
cis-1,2-Dichloroethene <1.0 ug/L 1 01/09/12 13:48 156-59-21.0
trans-1,2-Dichloroethene <1.0 ug/L 1 01/09/12 13:48 156-60-51.0
1,2-Dichloropropane <1.0 ug/L 1 01/09/12 13:48 78-87-51.0
1,3-Dichloropropane <1.0 ug/L 1 01/09/12 13:48 142-28-91.0
2,2-Dichloropropane <1.0 ug/L 1 01/09/12 13:48 594-20-71.0
1,1-Dichloropropene <1.0 ug/L 1 01/09/12 13:48 563-58-61.0
cis-1,3-Dichloropropene <1.0 ug/L 1 01/09/12 13:48 10061-01-51.0
trans-1,3-Dichloropropene <1.0 ug/L 1 01/09/12 13:48 10061-02-61.0
Diisopropyl ether <1.0 ug/L 1 01/09/12 13:48 108-20-31.0
Ethylbenzene <1.0 ug/L 1 01/09/12 13:48 100-41-41.0
Hexachloro-1,3-butadiene <1.0 ug/L 1 01/09/12 13:48 87-68-31.0
2-Hexanone <5.0 ug/L 1 01/09/12 13:48 591-78-65.0
p-Isopropyltoluene <1.0 ug/L 1 01/09/12 13:48 99-87-61.0
Methylene Chloride <2.0 ug/L 1 01/09/12 13:48 75-09-22.0
4-Methyl-2-pentanone (MIBK)<5.0 ug/L 1 01/09/12 13:48 108-10-15.0
Methyl-tert-butyl ether <1.0 ug/L 1 01/09/12 13:48 1634-04-41.0
Naphthalene <1.0 ug/L 1 01/09/12 13:48 91-20-31.0
Styrene <1.0 ug/L 1 01/09/12 13:48 100-42-51.0
1,1,1,2-Tetrachloroethane <1.0 ug/L 1 01/09/12 13:48 630-20-61.0
1,1,2,2-Tetrachloroethane <1.0 ug/L 1 01/09/12 13:48 79-34-51.0
Tetrachloroethene 21.1 ug/L 1 01/09/12 13:48 127-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/10/2012 02:58 PM Page 14 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92109776
FORMER REEVES SITE
Sample:MW-6 Lab ID:92109776005 Collected:01/06/12 14:30 Received:01/06/12 15:42 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene <1.0 ug/L 1 01/09/12 13:48 108-88-31.0
1,2,3-Trichlorobenzene <1.0 ug/L 1 01/09/12 13:48 87-61-61.0
1,2,4-Trichlorobenzene <1.0 ug/L 1 01/09/12 13:48 120-82-11.0
1,1,1-Trichloroethane <1.0 ug/L 1 01/09/12 13:48 71-55-61.0
1,1,2-Trichloroethane <1.0 ug/L 1 01/09/12 13:48 79-00-51.0
Trichloroethene <1.0 ug/L 1 01/09/12 13:48 79-01-61.0
Trichlorofluoromethane <1.0 ug/L 1 01/09/12 13:48 75-69-41.0
1,2,3-Trichloropropane <1.0 ug/L 1 01/09/12 13:48 96-18-41.0
Vinyl acetate <2.0 ug/L 1 01/09/12 13:48 108-05-42.0
Vinyl chloride <1.0 ug/L 1 01/09/12 13:48 75-01-41.0
m&p-Xylene <2.0 ug/L 1 01/09/12 13:48 179601-23-12.0
o-Xylene <1.0 ug/L 1 01/09/12 13:48 95-47-61.0
Surrogates
4-Bromofluorobenzene (S)99 %1 01/09/12 13:48 460-00-470-130
Dibromofluoromethane (S)107 %1 01/09/12 13:48 1868-53-770-130
1,2-Dichloroethane-d4 (S)105 %1 01/09/12 13:48 17060-07-070-130
Toluene-d8 (S)100 %1 01/09/12 13:48 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/10/2012 02:58 PM Page 15 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92109776
FORMER REEVES SITE
Sample:MW-7 Lab ID:92109776006 Collected:01/06/12 11:15 Received:01/06/12 15:42 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone <25.0 ug/L 1 01/09/12 14:12 67-64-125.0
Benzene <1.0 ug/L 1 01/09/12 14:12 71-43-21.0
Bromobenzene <1.0 ug/L 1 01/09/12 14:12 108-86-11.0
Bromochloromethane <1.0 ug/L 1 01/09/12 14:12 74-97-51.0
Bromodichloromethane <1.0 ug/L 1 01/09/12 14:12 75-27-41.0
Bromoform <1.0 ug/L 1 01/09/12 14:12 75-25-21.0
Bromomethane <2.0 ug/L 1 01/09/12 14:12 74-83-92.0
2-Butanone (MEK)<5.0 ug/L 1 01/09/12 14:12 78-93-35.0
Carbon tetrachloride <1.0 ug/L 1 01/09/12 14:12 56-23-51.0
Chlorobenzene <1.0 ug/L 1 01/09/12 14:12 108-90-71.0
Chloroethane <1.0 ug/L 1 01/09/12 14:12 75-00-31.0
Chloroform <1.0 ug/L 1 01/09/12 14:12 67-66-31.0
Chloromethane <1.0 ug/L 1 01/09/12 14:12 74-87-31.0
2-Chlorotoluene <1.0 ug/L 1 01/09/12 14:12 95-49-81.0
4-Chlorotoluene <1.0 ug/L 1 01/09/12 14:12 106-43-41.0
1,2-Dibromo-3-chloropropane <5.0 ug/L 1 01/09/12 14:12 96-12-85.0
Dibromochloromethane <1.0 ug/L 1 01/09/12 14:12 124-48-11.0
1,2-Dibromoethane (EDB)<1.0 ug/L 1 01/09/12 14:12 106-93-41.0
Dibromomethane <1.0 ug/L 1 01/09/12 14:12 74-95-31.0
1,2-Dichlorobenzene <1.0 ug/L 1 01/09/12 14:12 95-50-11.0
1,3-Dichlorobenzene <1.0 ug/L 1 01/09/12 14:12 541-73-11.0
1,4-Dichlorobenzene <1.0 ug/L 1 01/09/12 14:12 106-46-71.0
Dichlorodifluoromethane <1.0 ug/L 1 01/09/12 14:12 75-71-81.0
1,1-Dichloroethane <1.0 ug/L 1 01/09/12 14:12 75-34-31.0
1,2-Dichloroethane <1.0 ug/L 1 01/09/12 14:12 107-06-21.0
1,1-Dichloroethene <1.0 ug/L 1 01/09/12 14:12 75-35-41.0
cis-1,2-Dichloroethene <1.0 ug/L 1 01/09/12 14:12 156-59-21.0
trans-1,2-Dichloroethene <1.0 ug/L 1 01/09/12 14:12 156-60-51.0
1,2-Dichloropropane <1.0 ug/L 1 01/09/12 14:12 78-87-51.0
1,3-Dichloropropane <1.0 ug/L 1 01/09/12 14:12 142-28-91.0
2,2-Dichloropropane <1.0 ug/L 1 01/09/12 14:12 594-20-71.0
1,1-Dichloropropene <1.0 ug/L 1 01/09/12 14:12 563-58-61.0
cis-1,3-Dichloropropene <1.0 ug/L 1 01/09/12 14:12 10061-01-51.0
trans-1,3-Dichloropropene <1.0 ug/L 1 01/09/12 14:12 10061-02-61.0
Diisopropyl ether <1.0 ug/L 1 01/09/12 14:12 108-20-31.0
Ethylbenzene <1.0 ug/L 1 01/09/12 14:12 100-41-41.0
Hexachloro-1,3-butadiene <1.0 ug/L 1 01/09/12 14:12 87-68-31.0
2-Hexanone <5.0 ug/L 1 01/09/12 14:12 591-78-65.0
p-Isopropyltoluene <1.0 ug/L 1 01/09/12 14:12 99-87-61.0
Methylene Chloride <2.0 ug/L 1 01/09/12 14:12 75-09-22.0
4-Methyl-2-pentanone (MIBK)<5.0 ug/L 1 01/09/12 14:12 108-10-15.0
Methyl-tert-butyl ether <1.0 ug/L 1 01/09/12 14:12 1634-04-41.0
Naphthalene <1.0 ug/L 1 01/09/12 14:12 91-20-31.0
Styrene <1.0 ug/L 1 01/09/12 14:12 100-42-51.0
1,1,1,2-Tetrachloroethane <1.0 ug/L 1 01/09/12 14:12 630-20-61.0
1,1,2,2-Tetrachloroethane <1.0 ug/L 1 01/09/12 14:12 79-34-51.0
Tetrachloroethene <1.0 ug/L 1 01/09/12 14:12 127-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/10/2012 02:58 PM Page 16 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92109776
FORMER REEVES SITE
Sample:MW-7 Lab ID:92109776006 Collected:01/06/12 11:15 Received:01/06/12 15:42 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene <1.0 ug/L 1 01/09/12 14:12 108-88-31.0
1,2,3-Trichlorobenzene <1.0 ug/L 1 01/09/12 14:12 87-61-61.0
1,2,4-Trichlorobenzene <1.0 ug/L 1 01/09/12 14:12 120-82-11.0
1,1,1-Trichloroethane <1.0 ug/L 1 01/09/12 14:12 71-55-61.0
1,1,2-Trichloroethane <1.0 ug/L 1 01/09/12 14:12 79-00-51.0
Trichloroethene <1.0 ug/L 1 01/09/12 14:12 79-01-61.0
Trichlorofluoromethane <1.0 ug/L 1 01/09/12 14:12 75-69-41.0
1,2,3-Trichloropropane <1.0 ug/L 1 01/09/12 14:12 96-18-41.0
Vinyl acetate <2.0 ug/L 1 01/09/12 14:12 108-05-42.0
Vinyl chloride <1.0 ug/L 1 01/09/12 14:12 75-01-41.0
m&p-Xylene <2.0 ug/L 1 01/09/12 14:12 179601-23-12.0
o-Xylene <1.0 ug/L 1 01/09/12 14:12 95-47-61.0
Surrogates
4-Bromofluorobenzene (S)93 %1 01/09/12 14:12 460-00-470-130
Dibromofluoromethane (S)109 %1 01/09/12 14:12 1868-53-770-130
1,2-Dichloroethane-d4 (S)104 %1 01/09/12 14:12 17060-07-070-130
Toluene-d8 (S)100 %1 01/09/12 14:12 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/10/2012 02:58 PM Page 17 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92109776
FORMER REEVES SITE
Sample:DUP Lab ID:92109776007 Collected:01/06/12 14:16 Received:01/06/12 15:42 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone <25.0 ug/L 1 01/09/12 14:36 67-64-125.0
Benzene <1.0 ug/L 1 01/09/12 14:36 71-43-21.0
Bromobenzene <1.0 ug/L 1 01/09/12 14:36 108-86-11.0
Bromochloromethane <1.0 ug/L 1 01/09/12 14:36 74-97-51.0
Bromodichloromethane <1.0 ug/L 1 01/09/12 14:36 75-27-41.0
Bromoform <1.0 ug/L 1 01/09/12 14:36 75-25-21.0
Bromomethane <2.0 ug/L 1 01/09/12 14:36 74-83-92.0
2-Butanone (MEK)<5.0 ug/L 1 01/09/12 14:36 78-93-35.0
Carbon tetrachloride <1.0 ug/L 1 01/09/12 14:36 56-23-51.0
Chlorobenzene <1.0 ug/L 1 01/09/12 14:36 108-90-71.0
Chloroethane <1.0 ug/L 1 01/09/12 14:36 75-00-31.0
Chloroform <1.0 ug/L 1 01/09/12 14:36 67-66-31.0
Chloromethane <1.0 ug/L 1 01/09/12 14:36 74-87-31.0
2-Chlorotoluene <1.0 ug/L 1 01/09/12 14:36 95-49-81.0
4-Chlorotoluene <1.0 ug/L 1 01/09/12 14:36 106-43-41.0
1,2-Dibromo-3-chloropropane <5.0 ug/L 1 01/09/12 14:36 96-12-85.0
Dibromochloromethane <1.0 ug/L 1 01/09/12 14:36 124-48-11.0
1,2-Dibromoethane (EDB)<1.0 ug/L 1 01/09/12 14:36 106-93-41.0
Dibromomethane <1.0 ug/L 1 01/09/12 14:36 74-95-31.0
1,2-Dichlorobenzene <1.0 ug/L 1 01/09/12 14:36 95-50-11.0
1,3-Dichlorobenzene <1.0 ug/L 1 01/09/12 14:36 541-73-11.0
1,4-Dichlorobenzene <1.0 ug/L 1 01/09/12 14:36 106-46-71.0
Dichlorodifluoromethane <1.0 ug/L 1 01/09/12 14:36 75-71-81.0
1,1-Dichloroethane <1.0 ug/L 1 01/09/12 14:36 75-34-31.0
1,2-Dichloroethane <1.0 ug/L 1 01/09/12 14:36 107-06-21.0
1,1-Dichloroethene <1.0 ug/L 1 01/09/12 14:36 75-35-41.0
cis-1,2-Dichloroethene <1.0 ug/L 1 01/09/12 14:36 156-59-21.0
trans-1,2-Dichloroethene <1.0 ug/L 1 01/09/12 14:36 156-60-51.0
1,2-Dichloropropane <1.0 ug/L 1 01/09/12 14:36 78-87-51.0
1,3-Dichloropropane <1.0 ug/L 1 01/09/12 14:36 142-28-91.0
2,2-Dichloropropane <1.0 ug/L 1 01/09/12 14:36 594-20-71.0
1,1-Dichloropropene <1.0 ug/L 1 01/09/12 14:36 563-58-61.0
cis-1,3-Dichloropropene <1.0 ug/L 1 01/09/12 14:36 10061-01-51.0
trans-1,3-Dichloropropene <1.0 ug/L 1 01/09/12 14:36 10061-02-61.0
Diisopropyl ether <1.0 ug/L 1 01/09/12 14:36 108-20-31.0
Ethylbenzene <1.0 ug/L 1 01/09/12 14:36 100-41-41.0
Hexachloro-1,3-butadiene <1.0 ug/L 1 01/09/12 14:36 87-68-31.0
2-Hexanone <5.0 ug/L 1 01/09/12 14:36 591-78-65.0
p-Isopropyltoluene <1.0 ug/L 1 01/09/12 14:36 99-87-61.0
Methylene Chloride <2.0 ug/L 1 01/09/12 14:36 75-09-22.0
4-Methyl-2-pentanone (MIBK)<5.0 ug/L 1 01/09/12 14:36 108-10-15.0
Methyl-tert-butyl ether <1.0 ug/L 1 01/09/12 14:36 1634-04-41.0
Naphthalene <1.0 ug/L 1 01/09/12 14:36 91-20-31.0
Styrene <1.0 ug/L 1 01/09/12 14:36 100-42-51.0
1,1,1,2-Tetrachloroethane <1.0 ug/L 1 01/09/12 14:36 630-20-61.0
1,1,2,2-Tetrachloroethane <1.0 ug/L 1 01/09/12 14:36 79-34-51.0
Tetrachloroethene 14.6 ug/L 1 01/09/12 14:36 127-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/10/2012 02:58 PM Page 18 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92109776
FORMER REEVES SITE
Sample:DUP Lab ID:92109776007 Collected:01/06/12 14:16 Received:01/06/12 15:42 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene <1.0 ug/L 1 01/09/12 14:36 108-88-31.0
1,2,3-Trichlorobenzene <1.0 ug/L 1 01/09/12 14:36 87-61-61.0
1,2,4-Trichlorobenzene <1.0 ug/L 1 01/09/12 14:36 120-82-11.0
1,1,1-Trichloroethane <1.0 ug/L 1 01/09/12 14:36 71-55-61.0
1,1,2-Trichloroethane <1.0 ug/L 1 01/09/12 14:36 79-00-51.0
Trichloroethene <1.0 ug/L 1 01/09/12 14:36 79-01-61.0
Trichlorofluoromethane <1.0 ug/L 1 01/09/12 14:36 75-69-41.0
1,2,3-Trichloropropane <1.0 ug/L 1 01/09/12 14:36 96-18-41.0
Vinyl acetate <2.0 ug/L 1 01/09/12 14:36 108-05-42.0
Vinyl chloride <1.0 ug/L 1 01/09/12 14:36 75-01-41.0
m&p-Xylene <2.0 ug/L 1 01/09/12 14:36 179601-23-12.0
o-Xylene <1.0 ug/L 1 01/09/12 14:36 95-47-61.0
Surrogates
4-Bromofluorobenzene (S)96 %1 01/09/12 14:36 460-00-470-130
Dibromofluoromethane (S)102 %1 01/09/12 14:36 1868-53-770-130
1,2-Dichloroethane-d4 (S)101 %1 01/09/12 14:36 17060-07-070-130
Toluene-d8 (S)100 %1 01/09/12 14:36 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/10/2012 02:58 PM Page 19 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92109776
FORMER REEVES SITE
Sample:TRIP BLANK Lab ID:92109776008 Collected:01/06/12 00:00 Received:01/06/12 15:42 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone <25.0 ug/L 1 01/09/12 11:46 67-64-125.0
Benzene <1.0 ug/L 1 01/09/12 11:46 71-43-21.0
Bromobenzene <1.0 ug/L 1 01/09/12 11:46 108-86-11.0
Bromochloromethane <1.0 ug/L 1 01/09/12 11:46 74-97-51.0
Bromodichloromethane <1.0 ug/L 1 01/09/12 11:46 75-27-41.0
Bromoform <1.0 ug/L 1 01/09/12 11:46 75-25-21.0
Bromomethane <2.0 ug/L 1 01/09/12 11:46 74-83-92.0
2-Butanone (MEK)<5.0 ug/L 1 01/09/12 11:46 78-93-35.0
Carbon tetrachloride <1.0 ug/L 1 01/09/12 11:46 56-23-51.0
Chlorobenzene <1.0 ug/L 1 01/09/12 11:46 108-90-71.0
Chloroethane <1.0 ug/L 1 01/09/12 11:46 75-00-31.0
Chloroform <1.0 ug/L 1 01/09/12 11:46 67-66-31.0
Chloromethane <1.0 ug/L 1 01/09/12 11:46 74-87-31.0
2-Chlorotoluene <1.0 ug/L 1 01/09/12 11:46 95-49-81.0
4-Chlorotoluene <1.0 ug/L 1 01/09/12 11:46 106-43-41.0
1,2-Dibromo-3-chloropropane <5.0 ug/L 1 01/09/12 11:46 96-12-85.0
Dibromochloromethane <1.0 ug/L 1 01/09/12 11:46 124-48-11.0
1,2-Dibromoethane (EDB)<1.0 ug/L 1 01/09/12 11:46 106-93-41.0
Dibromomethane <1.0 ug/L 1 01/09/12 11:46 74-95-31.0
1,2-Dichlorobenzene <1.0 ug/L 1 01/09/12 11:46 95-50-11.0
1,3-Dichlorobenzene <1.0 ug/L 1 01/09/12 11:46 541-73-11.0
1,4-Dichlorobenzene <1.0 ug/L 1 01/09/12 11:46 106-46-71.0
Dichlorodifluoromethane <1.0 ug/L 1 01/09/12 11:46 75-71-81.0
1,1-Dichloroethane <1.0 ug/L 1 01/09/12 11:46 75-34-31.0
1,2-Dichloroethane <1.0 ug/L 1 01/09/12 11:46 107-06-21.0
1,1-Dichloroethene <1.0 ug/L 1 01/09/12 11:46 75-35-41.0
cis-1,2-Dichloroethene <1.0 ug/L 1 01/09/12 11:46 156-59-21.0
trans-1,2-Dichloroethene <1.0 ug/L 1 01/09/12 11:46 156-60-51.0
1,2-Dichloropropane <1.0 ug/L 1 01/09/12 11:46 78-87-51.0
1,3-Dichloropropane <1.0 ug/L 1 01/09/12 11:46 142-28-91.0
2,2-Dichloropropane <1.0 ug/L 1 01/09/12 11:46 594-20-71.0
1,1-Dichloropropene <1.0 ug/L 1 01/09/12 11:46 563-58-61.0
cis-1,3-Dichloropropene <1.0 ug/L 1 01/09/12 11:46 10061-01-51.0
trans-1,3-Dichloropropene <1.0 ug/L 1 01/09/12 11:46 10061-02-61.0
Diisopropyl ether <1.0 ug/L 1 01/09/12 11:46 108-20-31.0
Ethylbenzene <1.0 ug/L 1 01/09/12 11:46 100-41-41.0
Hexachloro-1,3-butadiene <1.0 ug/L 1 01/09/12 11:46 87-68-31.0
2-Hexanone <5.0 ug/L 1 01/09/12 11:46 591-78-65.0
p-Isopropyltoluene <1.0 ug/L 1 01/09/12 11:46 99-87-61.0
Methylene Chloride <2.0 ug/L 1 01/09/12 11:46 75-09-22.0
4-Methyl-2-pentanone (MIBK)<5.0 ug/L 1 01/09/12 11:46 108-10-15.0
Methyl-tert-butyl ether <1.0 ug/L 1 01/09/12 11:46 1634-04-41.0
Naphthalene <1.0 ug/L 1 01/09/12 11:46 91-20-31.0
Styrene <1.0 ug/L 1 01/09/12 11:46 100-42-51.0
1,1,1,2-Tetrachloroethane <1.0 ug/L 1 01/09/12 11:46 630-20-61.0
1,1,2,2-Tetrachloroethane <1.0 ug/L 1 01/09/12 11:46 79-34-51.0
Tetrachloroethene <1.0 ug/L 1 01/09/12 11:46 127-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/10/2012 02:58 PM Page 20 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
92109776
FORMER REEVES SITE
Sample:TRIP BLANK Lab ID:92109776008 Collected:01/06/12 00:00 Received:01/06/12 15:42 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene <1.0 ug/L 1 01/09/12 11:46 108-88-31.0
1,2,3-Trichlorobenzene <1.0 ug/L 1 01/09/12 11:46 87-61-61.0
1,2,4-Trichlorobenzene <1.0 ug/L 1 01/09/12 11:46 120-82-11.0
1,1,1-Trichloroethane <1.0 ug/L 1 01/09/12 11:46 71-55-61.0
1,1,2-Trichloroethane <1.0 ug/L 1 01/09/12 11:46 79-00-51.0
Trichloroethene <1.0 ug/L 1 01/09/12 11:46 79-01-61.0
Trichlorofluoromethane <1.0 ug/L 1 01/09/12 11:46 75-69-41.0
1,2,3-Trichloropropane <1.0 ug/L 1 01/09/12 11:46 96-18-41.0
Vinyl acetate <2.0 ug/L 1 01/09/12 11:46 108-05-42.0
Vinyl chloride <1.0 ug/L 1 01/09/12 11:46 75-01-41.0
m&p-Xylene <2.0 ug/L 1 01/09/12 11:46 179601-23-12.0
o-Xylene <1.0 ug/L 1 01/09/12 11:46 95-47-61.0
Surrogates
4-Bromofluorobenzene (S)96 %1 01/09/12 11:46 460-00-470-130
Dibromofluoromethane (S)104 %1 01/09/12 11:46 1868-53-770-130
1,2-Dichloroethane-d4 (S)103 %1 01/09/12 11:46 17060-07-070-130
Toluene-d8 (S)100 %1 01/09/12 11:46 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/10/2012 02:58 PM Page 21 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92109776
FORMER REEVES SITE
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/17864
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:92109776001, 92109776002, 92109776003, 92109776004, 92109776005, 92109776006, 92109776007,
92109776008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:707960
Associated Lab Samples:92109776001, 92109776002, 92109776003, 92109776004, 92109776005, 92109776006, 92109776007,
92109776008
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L <1.0 1.0 01/09/12 10:58
1,1,1-Trichloroethane ug/L <1.0 1.0 01/09/12 10:58
1,1,2,2-Tetrachloroethane ug/L <1.0 1.0 01/09/12 10:58
1,1,2-Trichloroethane ug/L <1.0 1.0 01/09/12 10:58
1,1-Dichloroethane ug/L <1.0 1.0 01/09/12 10:58
1,1-Dichloroethene ug/L <1.0 1.0 01/09/12 10:58
1,1-Dichloropropene ug/L <1.0 1.0 01/09/12 10:58
1,2,3-Trichlorobenzene ug/L <1.0 1.0 01/09/12 10:58
1,2,3-Trichloropropane ug/L <1.0 1.0 01/09/12 10:58
1,2,4-Trichlorobenzene ug/L <1.0 1.0 01/09/12 10:58
1,2-Dibromo-3-chloropropane ug/L <5.0 5.0 01/09/12 10:58
1,2-Dibromoethane (EDB)ug/L <1.0 1.0 01/09/12 10:58
1,2-Dichlorobenzene ug/L <1.0 1.0 01/09/12 10:58
1,2-Dichloroethane ug/L <1.0 1.0 01/09/12 10:58
1,2-Dichloropropane ug/L <1.0 1.0 01/09/12 10:58
1,3-Dichlorobenzene ug/L <1.0 1.0 01/09/12 10:58
1,3-Dichloropropane ug/L <1.0 1.0 01/09/12 10:58
1,4-Dichlorobenzene ug/L <1.0 1.0 01/09/12 10:58
2,2-Dichloropropane ug/L <1.0 1.0 01/09/12 10:58
2-Butanone (MEK)ug/L <5.0 5.0 01/09/12 10:58
2-Chlorotoluene ug/L <1.0 1.0 01/09/12 10:58
2-Hexanone ug/L <5.0 5.0 01/09/12 10:58
4-Chlorotoluene ug/L <1.0 1.0 01/09/12 10:58
4-Methyl-2-pentanone (MIBK)ug/L <5.0 5.0 01/09/12 10:58
Acetone ug/L <25.0 25.0 01/09/12 10:58
Benzene ug/L <1.0 1.0 01/09/12 10:58
Bromobenzene ug/L <1.0 1.0 01/09/12 10:58
Bromochloromethane ug/L <1.0 1.0 01/09/12 10:58
Bromodichloromethane ug/L <1.0 1.0 01/09/12 10:58
Bromoform ug/L <1.0 1.0 01/09/12 10:58
Bromomethane ug/L <2.0 2.0 01/09/12 10:58
Carbon tetrachloride ug/L <1.0 1.0 01/09/12 10:58
Chlorobenzene ug/L <1.0 1.0 01/09/12 10:58
Chloroethane ug/L <1.0 1.0 01/09/12 10:58
Chloroform ug/L <1.0 1.0 01/09/12 10:58
Chloromethane ug/L <1.0 1.0 01/09/12 10:58
cis-1,2-Dichloroethene ug/L <1.0 1.0 01/09/12 10:58
cis-1,3-Dichloropropene ug/L <1.0 1.0 01/09/12 10:58
Dibromochloromethane ug/L <1.0 1.0 01/09/12 10:58
Dibromomethane ug/L <1.0 1.0 01/09/12 10:58
Dichlorodifluoromethane ug/L <1.0 1.0 01/09/12 10:58
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/10/2012 02:58 PM Page 22 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92109776
FORMER REEVES SITE
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:707960
Associated Lab Samples:92109776001, 92109776002, 92109776003, 92109776004, 92109776005, 92109776006, 92109776007,
92109776008
Matrix:Water
Analyzed
Diisopropyl ether ug/L <1.0 1.0 01/09/12 10:58
Ethylbenzene ug/L <1.0 1.0 01/09/12 10:58
Hexachloro-1,3-butadiene ug/L 1.6 1.0 B-01/09/12 10:58
m&p-Xylene ug/L <2.0 2.0 01/09/12 10:58
Methyl-tert-butyl ether ug/L <1.0 1.0 01/09/12 10:58
Methylene Chloride ug/L <2.0 2.0 01/09/12 10:58
Naphthalene ug/L <1.0 1.0 01/09/12 10:58
o-Xylene ug/L <1.0 1.0 01/09/12 10:58
p-Isopropyltoluene ug/L <1.0 1.0 01/09/12 10:58
Styrene ug/L <1.0 1.0 01/09/12 10:58
Tetrachloroethene ug/L <1.0 1.0 01/09/12 10:58
Toluene ug/L <1.0 1.0 01/09/12 10:58
trans-1,2-Dichloroethene ug/L <1.0 1.0 01/09/12 10:58
trans-1,3-Dichloropropene ug/L <1.0 1.0 01/09/12 10:58
Trichloroethene ug/L <1.0 1.0 01/09/12 10:58
Trichlorofluoromethane ug/L <1.0 1.0 01/09/12 10:58
Vinyl acetate ug/L <2.0 2.0 01/09/12 10:58
Vinyl chloride ug/L <1.0 1.0 01/09/12 10:58
1,2-Dichloroethane-d4 (S)%104 70-130 01/09/12 10:58
4-Bromofluorobenzene (S)%104 70-130 01/09/12 10:58
Dibromofluoromethane (S)%104 70-130 01/09/12 10:58
Toluene-d8 (S)%98 70-130 01/09/12 10:58
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
707961LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.250 98 70-130
1,1,1-Trichloroethane ug/L 47.050 94 70-130
1,1,2,2-Tetrachloroethane ug/L 45.350 91 70-130
1,1,2-Trichloroethane ug/L 55.250 110 70-130
1,1-Dichloroethane ug/L 44.250 88 70-130
1,1-Dichloroethene ug/L 54.650 109 70-132
1,1-Dichloropropene ug/L 51.450 103 70-130
1,2,3-Trichlorobenzene ug/L 44.450 89 70-135
1,2,3-Trichloropropane ug/L 43.750 87 70-130
1,2,4-Trichlorobenzene ug/L 49.550 99 70-134
1,2-Dibromo-3-chloropropane ug/L 45.550 91 70-130
1,2-Dibromoethane (EDB)ug/L 51.350 103 70-130
1,2-Dichlorobenzene ug/L 51.450 103 70-130
1,2-Dichloroethane ug/L 48.150 96 70-130
1,2-Dichloropropane ug/L 50.050 100 70-130
1,3-Dichlorobenzene ug/L 52.050 104 70-130
1,3-Dichloropropane ug/L 47.750 95 70-130
1,4-Dichlorobenzene ug/L 49.850 100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/10/2012 02:58 PM Page 23 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92109776
FORMER REEVES SITE
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
707961LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 48.350 97 58-145
2-Butanone (MEK)ug/L 95.9100 96 70-145
2-Chlorotoluene ug/L 52.450 105 70-130
2-Hexanone ug/L 100100 100 70-144
4-Chlorotoluene ug/L 51.950 104 70-130
4-Methyl-2-pentanone (MIBK)ug/L 103100 103 70-140
Acetone ug/L 96.0100 96 50-175
Benzene ug/L 56.750 113 70-130
Bromobenzene ug/L 50.450 101 70-130
Bromochloromethane ug/L 50.350 101 70-130
Bromodichloromethane ug/L 47.450 95 70-130
Bromoform ug/L 49.150 98 70-130
Bromomethane ug/L 43.450 87 54-130
Carbon tetrachloride ug/L 54.150 108 70-132
Chlorobenzene ug/L 50.850 102 70-130
Chloroethane ug/L 52.350 105 64-134
Chloroform ug/L 48.950 98 70-130
Chloromethane ug/L 50.450 101 64-130
cis-1,2-Dichloroethene ug/L 50.050 100 70-131
cis-1,3-Dichloropropene ug/L 52.050 104 70-130
Dibromochloromethane ug/L 46.850 94 70-130
Dibromomethane ug/L 51.850 104 70-131
Dichlorodifluoromethane ug/L 48.550 97 56-130
Diisopropyl ether ug/L 51.850 104 70-130
Ethylbenzene ug/L 51.450 103 70-130
Hexachloro-1,3-butadiene ug/L 50.750 101 70-130
m&p-Xylene ug/L 101100 101 70-130
Methyl-tert-butyl ether ug/L 52.350 105 70-130
Methylene Chloride ug/L 49.550 99 63-130
Naphthalene ug/L 43.450 87 70-138
o-Xylene ug/L 50.350 101 70-130
p-Isopropyltoluene ug/L 55.450 111 70-130
Styrene ug/L 53.450 107 70-130
Tetrachloroethene ug/L 49.750 99 70-130
Toluene ug/L 54.050 108 70-130
trans-1,2-Dichloroethene ug/L 49.650 99 70-130
trans-1,3-Dichloropropene ug/L 52.350 105 70-132
Trichloroethene ug/L 54.250 108 70-130
Trichlorofluoromethane ug/L 50.550 101 62-133
Vinyl acetate ug/L 73.3100 73 66-157
Vinyl chloride ug/L 54.250 108 69-130
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%99 70-130
Dibromofluoromethane (S)%96 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/10/2012 02:58 PM Page 24 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
92109776
FORMER REEVES SITE
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
707962MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92109416001
707963
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1-Dichloroethene ug/L 50 111 70-166119 750ND55.5 59.4
Benzene ug/L 50 98 70-148107 950ND49.0 53.7
Chlorobenzene ug/L 50 119 70-146130 950ND59.6 65.1
Toluene ug/L 50 115 70-155126 950ND57.3 62.8
Trichloroethene ug/L 50 116 69-151128 950ND58.2 63.8
1,2-Dichloroethane-d4 (S)%103 70-130100
4-Bromofluorobenzene (S)%94 70-13098
Dibromofluoromethane (S)%99 70-130102
Toluene-d8 (S)%95 70-13097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/10/2012 02:58 PM Page 25 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Project No.:
Project:
92109776
FORMER REEVES SITE
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte detected in method blank but was not detected in the associated samples.B-
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/10/2012 02:58 PM Page 26 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92109776
FORMER REEVES SITE
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92109776001 MSV/17864SW-D EPA 8260
92109776002 MSV/17864SW-U EPA 8260
92109776003 MSV/17864MW-5B EPA 8260
92109776004 MSV/17864MW-5C EPA 8260
92109776005 MSV/17864MW-6 EPA 8260
92109776006 MSV/17864MW-7 EPA 8260
92109776007 MSV/17864DUPEPA 8260
92109776008 MSV/17864TRIP BLANK EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/10/2012 02:58 PM Page 27 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]

APPENDIX II

Field Sampling Logs

APPENDIX III

Exhibit B of the Filed Notice of Brownfields Property