10001_YanceyMitchellMSWLF_1987_GWMR_FID1086145

DElectronic Data -Email CD data loaded: Yes/ No Doc/Event#: Environmental Monitoring Reporting Form
Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are available for inspection and examination by any person upon request (NC General Statute 132-6}.
Instructions: Prepare one form for each Individually monitored unit.
Please type or print legibly. Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off-site source, pre-existing condition, etc.). ·
Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits. Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the facility (NCAC 13B .1629 (4)(a)(i}. Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste Section, 1646 Mail Service Center, Raleigh, NC 27699-1646.
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Anchor QEA of North Carolina, PLLC
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mall address:
Name: Brian Gant Phone: [phone]
E -ma ii: [e-mail]
Facility name: Facility Address:
Yancey-Mitchell Municipal Solid 555 Landfill Road Waste Landfill Burnsville, North Carolina 28714
Environmental Status: (Check all that apply) 0 Initial/Background Monitoring 18}Detection Monitoring
T e of data submitted: (Check all that apply) Groundwater monitoring data from monitoring wells Groundwater monitoring data from private water supply wells Leachate monitoring data
X Surface water monitorin data
Notification attached? 0 No. No groundwater or surface water standards were exceeded.
B D
-------------------------
NC Landfill Rule: Facility Permit# (.0500 or .1600} EJEJ Actual sampling dates (e.g:, October 20-24, 2006}
March 28 and 29, 2017
0 Assessment Monitoring 0 Corrective Action
Methane gas monitoring data Corrective action data (specify}
Other(specify}
[g] Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and preliminary analysis of the cause and significance of any concentration. 0 Yes, a notification of values exceeding an explosive methane gas limit is attached. II includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification To the best of my knowledge, the Information reported and statements made on this data submittal and attachments are true and correct. Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there are significant penalties for making any false statement, representation, or certification including the possibility of a fine and Imprisonment.
Alec Macbeth, P.G.
Facility Representative Name (Print) Alec MacBeth
Signature
· Project Geologist
Title Digitally signed by Alec MacBeth Date: 2017.06.30 16:08:15 -04'00'
231 Haywood Street Asheville, North Carolina 28805
Facility Representative Address
P-1649
NC PE Firm License Number (if applicable effective May 1, 2009)
Revised 6/2009
828-281-3350
(Area Code) Telephone Number
Affix NC Licensed/ Professional Geologist Seal
Date

June 2017
Yancey-Mitchell County Closed Municipal Solid Waste Landfill
Spring 2017 Semiannual Water Quality
Monitoring Report
Yancey County, North Carolina, Permit #100-01
Prepared for Yancey County, North Carolina, and Mitchell County, North Carolina

Project Number: C61485-01.01.02 A:\Projects\Yancey County\Solid Waste\Reports\2017\Spring\MSW LF\FINAL10001March2017 Water Quality Report mb.docx
June 2017
Yancey-Mitchell County Closed Municipal Solid Waste Landfill
Spring 2017 Semiannual Water Quality
Monitoring Report
Yancey County, North Carolina, Permit #100-01
Prepared for Yancey County, North Carolina
Mitchell County, North Carolina
Prepared by Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801

Alec Macbeth, P.G.
Project Geologist

Spring 2017 Semiannual
Water Quality Monitoring Report i June 2017
TABLE OF CONTENTS
1 Introduction .................................................................................................................... 1
2 Methods ......................................................................................................................... 2
2.1 Groundwater and Surface Water Sampling ......................................................................................... 2
2.1.1 Groundwater Purging and Sampling Methods .................................................................... 2
2.1.2 Surface Water Sampling Methods ........................................................................................... 4
2.2 Sample Handling, Documentation, and Analysis ............................................................................... 4
3 Findings .......................................................................................................................... 6
3.1 Analytical Results ......................................................................................................................................... 6
3.1.1 Groundwater Samples ................................................................................................................. 7
3.1.2 Surface Water Samples ............................................................................................................... 8
3.2 Hydrogeology ............................................................................................................................................... 9
4 Summary ....................................................................................................................... 10
4.1 Future Activities .......................................................................................................................................... 10
5 References ..................................................................................................................... 11

TABLES
Table 1 Monitoring Well Construction Summary
Table 2 Summary of Laboratory Analyses Performed on Samples
Table 3 Summary of Analytical Results
FIGURES
Figure 1 Site Location Map
Figure 2 Sample Location and Posted Data Map
Figure 3 Generalized Groundwater Flow Direction Map
APPENDICES
Appendix A Sampling Logs and Equipment Documentation & Instrument Calibration Data
Sheets
Appendix B Reports of Laboratory Analysis and Chain-of-Custody Documentation

Spring 2017 Semiannual
Water Quality Monitoring Report ii June 2017
ABBREVIATIONS
µg/L micrograms per liter
µS/cm microsiemens per centimeter
Anchor QEA Anchor QEA of North Carolina, PLLC
C&D Construction and Demolition Debris
CFR Code of Federal Regulations
DENR North Carolina Department of Environment and Natural Resources, which is
now the DEQ
DEQ North Carolina Department of Environmental Quality
DO dissolved oxygen
DWM Division of Waste Management
DWQ Division of Water Quality
EDD Electronic Data Deliverable
EPA U.S. Environmental Protection Agency
ft-bgs feet below ground surface
ft-TOC feet below the top of the well casing
GWPS Groundwater Protection Standard
IMAC interim maximum allowable concentrations
J-flag indicates analytical result is qualified by the laboratory as estimated and is
flagged with a “J” qualifier
MDL method detection limit
mg/L milligrams per liter
MRL method reporting limit
MSW Municipal Solid Waste
mV millivolt
NCAC North Carolina Administrative Code
NTU Nephelometric turbidity units
ORP oxidation reduction potential
PVC polyvinyl chloride
SC specific conductivity
SESD Science and Ecosystem Support Division
SU Standard Units
SWM Solid Waste Management
SWS Solid Waste Section
SWSL Solid Waste Section Limit
VOC volatile organic compound

Spring 2017 Semiannual
Water Quality Monitoring Report 1 June 2017
1 Introduction
This Spring 2017 Semiannual Water Quality Monitoring Report is presented by Anchor QEA of North
Carolina, PLLC (Anchor QEA).
The Yancey County Solid Waste Department operates a solid waste facility located on Landfill Road
near North Carolina (NC) Highway 80 in Burnsville, North Carolina (Figure 1). The facility accepts solid
waste from both Yancey County and Mitchell County and includes the following permitted
components:
• A closed municipal solid waste (MSW) landfill (Permit #100-01)
• A closed construction and demolition debris (C&D) landfill (Permit #100-02)
• An active transfer station (Permit #100-03T)
The approximate locations of the two landfill units within the solid waste facility are shown on
Figure 2.
This report addresses water quality associated with the MSW Landfill only. Water quality at the C&D
Landfill is addressed in a separate report, because the C&D Landfill is permitted separately under the
rules codified in Title 15A, Subchapter 13B, Section .0500 and .0601 (per June 25, 2010
Memorandum) of the North Carolina Administrative Code (15A NCAC 13B.0500 and 15A NCAC
13B.0601).
This report documents the first semiannual groundwater and surface water monitoring event for
2017 and is being submitted in accordance with requirements stipulated in the letter Closure of the
Yancey-Mitchell County Landfill Permit #100-01 issued by the North Carolina Department of
Environmental Quality (DEQ) Division of Waste Management (DWM) for the MSW Landfill on
December 21, 1995 and with regulations codified in the DEQ Solid Waste Management (SWM) Rules
15A NCAC 13B.0510. The December 21, 1995 letter requires semiannual monitoring of groundwater
and surface water quality. This report provides an evaluation of surface water and groundwater
quality for the MSW Landfill.
The water quality monitoring network for the MSW Landfill consists of four compliance monitoring
wells (MW 2, MW-3, MW-AR, and MW-B), one background monitoring well (MW-J), and two surface
water sampling locations (SW-1 and SW-2) located along the North Toe River (Figure 2).

Spring 2017 Semiannual
Water Quality Monitoring Report 2 June 2017
2 Methods
2.1 Groundwater and Surface Water Sampling
On March 28 and 29, 2017, groundwater and surface water samples were collected by Anchor QEA.
All sampling locations are shown on Figure 2. A monitoring well construction summary and a water
level measurement summary are presented in Table 1. This table includes both the closed MSW
Landfill wells and the closed C&D Landfill wells to provide a more comprehensive data set that can
be used to evaluate groundwater flow direction. Table 2 provides a list of all groundwater and
surface water samples collected that are applicable to the MSW Landfill and the analyses performed
on each sample.
2.1.1 Groundwater Purging and Sampling Methods
Groundwater purging and sampling was performed using either a disposable bailer or downhole
pumps as described in Sections 2.1.1.1 through 2.1.1.3. Prior to purging and sampling the monitoring
wells, the static water level was gauged with a decontaminated QED MP30 Water Level Meter. Field
parameters—pH, specific conductivity (SC), dissolved oxygen (DO), turbidity, oxidation reduction
potential (ORP), and temperature—were measured and recorded during purging with a YSI 556
Multiprobe Water Quality Meter. Well sampling logs with static water level measurements and the
field parameter data are included in Appendix A. Static water level measurements are also provided
in Table 1. Groundwater samples were collected after purging the monitoring wells and after field
parameters had stabilized. When monitoring wells were purged with a disposable bailer, a minimum
of three well volumes were purged from the monitoring well or, if the monitoring well recharged
slowly, the monitoring well was bailed dry and allowed to recharge prior to sampling.
Monitoring well total depth, the condition of the well casing, the groundwater recharge rate as
determined during purging, and the sample collection method(s) used at each monitoring well were
recorded on sampling logs provided in Appendix A. All groundwater purging and sampling was
performed by Anchor QEA personnel wearing new nitrile gloves and samples were collected in
laboratory-supplied sample containers. The specific purging methodologies used for the individual
monitoring wells are described in Sections 2.1.1.1 through 2.1.1.3, below. These methodologies are
consistent with historical practices.
2.1.1.1 Monitoring Well MW-2
Monitoring well MW-2 was purged and sampled on March 29, 2017. No well construction log or
drilling record is available for MW-2 (Table 1). The screened interval for monitoring well MW-2 is
assumed to be constructed in saprolite. The well’s total depth is 56.30 feet below the top of the well
casing (ft-TOC), as measured with the water level meter on the day of sampling. Although the well’s
surface completion is capped and secure, the casing is bent and likely cracked at approximately 10

Spring 2017 Semiannual
Water Quality Monitoring Report 3 June 2017
feet below ground surface (ft-bgs). This bend obstructed a downhole pump, so Anchor QEA
personnel used a more flexible, dedicated Teflon™ bailer (rather than a polyethylene bailer) to
bypass the bend in the casing, purged three well volumes, and subsequently collected a
groundwater sample. Field parameters were recorded for the initial groundwater withdrawal and
after each consecutive well volume was purged.
2.1.1.2 Monitoring Wells MW-AR, MW-B, and MW-3
A bladder pump and low-flow sampling techniques were used to purge and sample compliance
monitoring wells MW-3, MW-AR, and MW-B. No well construction log or drilling record is available
for monitoring wells MW-3 or MW-AR (Table 1). The screened interval for monitoring well MW-3 is
assumed to be constructed in saprolite. Monitoring well MW-3 has a total well depth of 38.0 ft-TOC,
as measured with a water level meter on the day of sampling. Monitoring well MW-AR has a total
depth of 71.4 ft-TOC, and its screened interval is assumed to be constructed in bedrock. The
screened interval for monitoring well MW-B is constructed in bedrock and has a total well depth of
70 ft-TOC. Total well depths for monitoring wells MW-AR and MW-B were measured with a water
level meter during prior sampling events. These three monitoring wells were purged using low-flow
sampling techniques in accordance with the procedures described in Low-Flow (Minimal Drawdown)
Ground-Water Sampling Procedures (Puls and Barcelona 1996).
During purging, the field parameters were measured and recorded approximately every 3 minutes.
Well purging continued until these parameters stabilized for three consecutive readings as outlined
in the United States Environmental Protection Agency (EPA) Region 4 Science and Ecosystem
Support Division (SESD) Operating Procedure: Groundwater Sampling (EPA 2013).
The required stabilization criteria were as follows:
• pH values within +/- 0.1 unit
• SC values within +/- 3 percent
• Temperature, DO, and turbidity values within +/- 10 percent
• ORP values within +/- 10 millivolts
Once the parameters stabilized, a groundwater sample was collected by an Anchor QEA technician
wearing a new pair of nitrile gloves.
2.1.1.3 Monitoring Well MW-J
Monitoring well MW-J, which has a total depth of 194.5 ft-bgs (Table 1), is located on a ridge in the
western part of the C&D Landfill. It is screened in bedrock and serves as a background well for the
water quality monitoring network. A bladder pump could not be used to purge and/or sample this
well due to the pressure head caused by the deep groundwater level in the well (146.01 ft-TOC).
Instead, Anchor QEA technicians used a GeoTech® Geosub® pump and performed low-flow

Spring 2017 Semiannual
Water Quality Monitoring Report 4 June 2017
sampling techniques to purge and sample the well on March 28, 2017. During purging, the field
parameters for groundwater were measured and recorded approximately every 3 minutes. Well
purging continued until these parameters stabilized for three consecutive readings. The stabilization
criteria were the same as for other wells (as described in Section 2.1.1.2). Once the parameters had
stabilized, groundwater samples were collected and placed into laboratory-supplied sample bottles
by a technician wearing a new pair of nitrile gloves.
2.1.2 Surface Water Sampling Methods
Surface water samples SW-1 and SW-2 were collected on March 28, 2017 at designated locations
from the North Toe River, which is located just east of the MSW Landfill. The SW-1 sample represents
surface water quality upstream of the MSW landfill, and the SW-2 sample represents surface water
quality downstream from the landfill. One round of field parameters—consisting of temperature, pH,
SC, DO, ORP, and turbidity—was measured and recorded at each surface water sampling location
prior to collecting the surface water sample. Each sample was collected into laboratory-supplied
sample containers by a technician wearing a new pair of nitrile gloves.
2.2 Sample Handling, Documentation, and Analysis
Field parameters and additional observations pertaining to the MSW Landfill sampling locations are
provided on sampling logs, which are included in Appendix A. Following collection, each
groundwater and surface water sample was immediately placed on ice in a sample cooler for
shipment to Prism Laboratories, a North Carolina-certified laboratory located in Charlotte, North
Carolina. The 1995 Closure Letter identified in Section 1.0 provides the sampling parameter list in its
Attachment 2 titled “Sampling and Analysis Requirements for Construction and Demolition Landfills
and Closed Sanitary Landfills” of the North Carolina Water Quality Monitoring Guidance Document for
Solid Waste Facilities (North Carolina Department of Environment and Natural Resources 1 [DENR]
1995). Table 2 provides details of analyses performed on all collected samples.
Proper chain-of-custody documentation procedures were followed during collection and
transportation of each sample to the laboratory. Documentation is included in Appendix B of this
report. A trip blank, provided by the laboratory, was placed in each sample cooler and analyzed for
Appendix I volatile organic compounds (VOCs) per Title 40 of the U.S. Code of Federal
Regulations (CFR), Part 258. The laboratory analytical reports are provided in Appendix B.
The Prism laboratory report of analysis, presented in Appendix B, contains results for selected
constituents that are not discussed in the text of this report. These constituents include eight
additional metals from the Appendix I constituent list, as well as tetrahydrofuran, chloride,
manganese, sulfate, iron, alkalinity, and total dissolved solids. The additional constituents were

1 The former DENR is now known as the DEQ.

Spring 2017 Semiannual
Water Quality Monitoring Report 5 June 2017
included in the laboratory analyses performed on three samples: the two surface water locations
(SW-1 and SW-2) and monitoring well MW-J. Samples were collected from these points to satisfy
monitoring requirements for both the MSW Landfill and the C&D Landfill. Samples collected from
the three referenced sampling points were analyzed for the additional constituents to meet
requirements of the 15A NCAC 13B.0500 and .0601 rules, pertaining to C&D landfills. A discussion of
the results for applicable constituents is included in the Spring 2017 Semiannual Water Quality
Monitoring Report, Yancey-Mitchell County Construction and Demolition Debris Landfill submitted in
June 2017 (Anchor QEA 2017).

Spring 2017 Semiannual
Water Quality Monitoring Report 6 June 2017
3 Findings
3.1 Analytical Results
The laboratory analytical results and field parameter data for the groundwater and surface water
samples collected at the landfill are included in Appendices A and B, as well as in the Electronic Data
Deliverable (EDD), which is provided separately to the DEQ DWM Solid Waste Section (SWS) per
applicable guidelines.
Non-detections were reported at the method detection limit (MDL), and all concentrations exceeding
the MDL were reported and appropriately qualified. The MDL is the minimum concentration of a
substance that can be measured and reported by a laboratory with 99 percent confidence that the
analyte concentration is greater than zero. All detections were compared to the analyte-specific Solid
Waste Section Limit (SWSL) established by the DEQ SWS. The SWSL is defined by the SWS as the
lowest concentration of an analyte in a sample that can be quantitatively determined with suitable
precision and accuracy. In this report, if the reported concentration is above the laboratory MDL and
below the method reporting limit (the analytical result is qualified by the laboratory as estimated and
is flagged with a “J” qualifier (J-flag). The MRL is the minimum concentration of a target analyte that
can be accurately determined by the referenced method. If the reported concentration is above the
laboratory MRL and below the SWSL, the analytical result is qualified as estimated and is flagged by
Anchor QEA with an italicized “J” qualifier (italicized J-flag). Concentrations detected below the
respective SWSLs are not discussed in the text of this report unless they exceed their contaminant-
specific water quality standard, as discussed below.
Detected concentrations of analytes in groundwater samples were compared to current groundwater
quality standards specified in 15A NCAC 2L.0202 and are referred to as “2L standards.” Detected
concentrations of analytes in groundwater with no established 2L standard were compared either to
the interim maximum allowable concentrations (IMACs) for Class GA and GSA groundwater (in
accordance with 15A NCAC 02L .0202 [c]) or Groundwater Protection Standards (GWPS), pursuant to
15A NCAC 13B.1634.
Detections of analytes in surface-water samples were compared to 15A NCAC 2B surface-water
quality standards (2B standards) established for Class B trout waters, as classified by the DEQ Division
of Water Quality (DWQ).
Table 3 presents the summary of detected constituents and outlines concentrations of analytes that
were above applicable SWSLs, as well as detected analytes that exceeded their respective 2L
standard, IMAC, or 2B standard.

Spring 2017 Semiannual
Water Quality Monitoring Report 7 June 2017
3.1.1 Groundwater Samples
The following sections summarize detections of field parameters, Appendix I VOCs, and metals in
groundwater.
3.1.1.1 Field Parameters
The pH readings measured from the samples collected from monitoring wells MW-2, MW-3, and
MW-AR were below the acceptable range of 6.5 to 8.5 Standard Units (SU) specified in the 2L
standards (Table 3). The pH readings recorded for this event are consistent with historical data.
Turbidity values at the time of sampling the monitoring wells ranged from 4.48 nephelometric
turbidity units (NTUs) in MW-J to 34.76 NTUs in MW-3 (Table 3). MW-2, which was purged and
sampled with a bailer, showed a turbidity value of 21.54 NTUs.
DO readings measured from the samples collected from the monitoring wells ranged between 2.08
milligrams per liter (mg/L) in MW-AR to 7.84 mg/L in MW-J. Specific conductivity measurements
ranged between 72 microsiemens per centimeter (µS/cm) in MW-AR to 1,551 µS/cm in MW-B. ORP
values measured in the samples collected from the monitoring wells ranged between -44.8
millivolts (mV) in MW-B to 309.2 mV in MW-AR. SWSLs and 2L standards are not established for DO,
specific conductivity, and ORP.
3.1.1.2 VOCs
Eleven VOCs were detected in the groundwater samples collected from one or more of the
monitoring wells (Table 3). Seven of the eleven VOCs (1,4-dichlorobenzene, benzene, chlorobenzene,
ethylbenzene, toluene, vinyl chloride, and total xylenes) were detected at concentrations above their
respective SWSLs in samples from one or more monitoring wells (Table 3). Only two compounds,
benzene and vinyl chloride, were detected at concentrations above their 2L standards. Both of these
exceedances occurred in the groundwater sample collected from MW-B at 3.8 micrograms per liter
(µg/L) and 2.6 µg/L, respectively (Table 3 and Figure 2). Historic data for monitoring well MW-B
shows consistent exceedances of these constituents during prior sampling events.
3.1.1.3 Metals
Seven metals were detected in the groundwater samples collected from one or more monitoring
wells (Table 3). Of the seven detected metals, only barium had detected concentration above its
SWSL in the sample collected from monitoring well MW-2 (Table 3). None of the detected metals
had concentrations that exceeded their respective 2L groundwater quality standards or IMACs.
Concentrations of the detected metals are consistent with historical data.

Spring 2017 Semiannual
Water Quality Monitoring Report 8 June 2017
3.1.2 Surface Water Samples
The following sections summarize detections of field parameters, VOCs, metals, and field parameters
in surface water. The location of sample point SW-1 in the North Toe River is upstream of the landfill
and is assumed to represent surface water quality upstream of the Yancey County MSW and C&D
landfills. The location of sample point SW-2 in the North Toe River is downstream of the landfill and
is assumed to represent surface water quality downstream of the landfills (Figure 2).
3.1.2.1 Field Parameters
The pH readings were obtained on March 28, 2017 for surface water samples. The pH readings
measured 6.25 and 6.45 SU for surface water samples SW-1 and SW-2, respectively. Both results are
within the 2B standard range for pH established at 6.0 to 9.0 SU (Table 3) and are consistent with
historical readings.
Turbidity was measured and recorded for SW-1 and SW-2 at 2.17 NTUs and 9.22 NTUs, respectively.
Both values are within the 2B standard of 10 NTUs (Table 3) and are consistent with historical
readings.
Dissolved oxygen was measured at 9.17 mg/L for SW-1 and 7.94 mg/L at SW-2, both values within
the established 2B standard for dissolved oxygen of 6.0 mg/L (the 2B standard indicates “equal to or
greater than 6.0 mg/L” for trout water) and are consistent with historical readings.
Specific conductivity measurements in surface water samples SW-1 and SW-2 were recorded at 70
µS/cm and 61 µS/cm, respectively. ORP measurements in SW-1 and SW-2 were recorded at 299.7 mV
and 300.1 mV, respectively. 2B standards do not exist for these field parameters. Detailed field
parameter results are provided in Appendix A and Table 3 of this report.
3.1.2.2 VOCs
No VOCs were detected in either of the surface water samples collected from the landfill.
3.1.2.3 Metals
Three metals (barium, chromium, and lead) were detected in both surface water samples (Table 3).
None of the detected metals exceeded their respective SWSLs or associated 2B standards. The
relationship of overall metals concentrations between the upstream and downstream surface water
samples does not show evidence of the landfill impacting surface water downstream of the landfill.
The detected metals in the downstream sample location were of similar concentration ranges as the
upstream sample location and supports the conclusion that the metal concentrations in the landfill
groundwater monitoring wells are not impacting the surface water.

Spring 2017 Semiannual
Water Quality Monitoring Report 9 June 2017
3.2 Hydrogeology
Groundwater elevations were calculated for the spring 2017 semiannual water quality monitoring
event using the measured depths to water and the associated top-of-casing elevations determined
from a survey performed for the monitoring wells in October 2009. Groundwater elevation data are
reported in Table 1. Figure 3 presents the generalized bedrock groundwater flow direction and
generalized saprolite groundwater flow direction. Generalized groundwater flow directions were
estimated using groundwater elevation data associated with a limited number of monitoring well
locations in an area of complex topographic and geologic conditions. The estimated groundwater
flow directions indicate that groundwater in the bedrock is flowing generally in a northeasterly
direction and that groundwater in the saprolite is generally mimicking topography. In the area where
data is available, groundwater flow in the saprolite is interpreted to be convergent toward a
topographic trough in a northerly direction. The apparent groundwater flow directions and the local
topography suggest that groundwater in both saprolite and bedrock is flowing toward the North Toe
River.

Spring 2017 Semiannual
Water Quality Monitoring Report 10 June 2017
4 Summary
Anchor QEA completed the first semiannual water quality monitoring event of 2017 at the Yancey-
Mitchell County MSW Landfill on March 28 and 29, 2017.
Table 3 of this report and the Prism Analytical Reports (Appendix B) provide detailed analytical
results and field data representing the groundwater and surface water quality at the MSW Landfill.
Generally, the groundwater and surface water analytical results show that constituent concentrations
are less than the respective SWSLs, 2B standards, and 2L standards, with the exception of benzene
and vinyl chloride in groundwater samples from compliance monitoring well MW-B. Benzene and
vinyl chloride have never been detected in the downstream surface water sample. The similarity in
concentrations of metals in both surface water samples supports the conclusion that groundwater
flow from the landfill toward the North Toe River is not impacting surface water.
4.1 Future Activities
Anchor QEA will continue to measure field parameters and collect water quality samples from
groundwater and surface water monitoring points associated with the MSW Landfill. Water quality
samples will be submitted to a North Carolina-certified laboratory for analysis of eight metals, as well
as Appendix I VOCs on a semiannual basis. The next sampling event is scheduled for September
2017.

Spring 2017 Semiannual
Water Quality Monitoring Report 11 June 2017
5 References
Anchor QEA (Anchor QEA of North Carolina, PLLC), 2017. Spring 2017 Semiannual Water Quality
Monitoring Report, Yancey-Mitchell County Construction and Demolition Debris Landfill. June
2017.
DENR (North Carolina Department of Environment and Natural Resources), 1995. North Carolina
Water Quality Monitoring Guidance Document for Solid Waste Facilities.
DENR DWM SWS (DENR Division of Waste Management Solid Waste Section), December 21, 1995.
Closure of the Yancey-Mitchell County Landfill Permit #100-01.
DENR DWM SWS, Revised April 2008. Solid Waste Section Guidelines for Groundwater, Soil, and
Surface Water Sampling.
EPA (United States Environmental Protection Agency), revised 2013. SESD Operating Procedure:
Groundwater Sampling. March 6, 2013.
Puls, R.W., and M. J. Barcelona, 1996. Low-Flow (Minimal Drawdown) Ground-Water Sampling
Procedures, U.S. Environmental Protection Agency, OSWER, EPA/540/S-95/504.

Tables
Table 1
Monitoring Well Construction Summary
Spring 2017 Semiannual Water Quality Monitoring Report
Yancey-Mitchell County Closed Construction and Demolition Debris Landfill
Page 1 of 1
June 2017
Northing Easting
Ground
Surface
Elevation
TOC
Elevation Stick Up
Total
Well
Depth
Depth To
Water
Groundwater
Elevation
Approximate
Depth to
Bedrock
Approximate
Bedrock
Elevation
Depth to Top
of Screened
Interval
Depth to
Bottom of
Screened
Interval
Top of Screen
Elevation
Elevation of
Bottom of
Screen
(NAD 83;
2007)(NAD 83; 2007)(feet NAVD
88)
(feet NAVD
88)
(feet above
ground
surface)
(feet
below
TOC)
(feet
below
TOC)
(feet NAVD 88)(feet bgs)(feet NAVD 88)(feet bgs)(feet bgs)(feet NAVD
88)
(feet NAVD
88)
C&D Landfill Monitoring Wells
100-02 MW-H 12/04/1996 809563.75 1058698.38 2,566.36 2,568.68 2.3 64.5 61.74 2,506.94 62 2,504 47.0 62.0 2,519.4 2,504.4
100-02 MW-I 12/02/1996 809923.04 1058531.91 2,596.57 2,598.77 2.0 83.0 76.81 2,521.96 ~85 2,512 64.0 79.0 2,532.6 2,517.6
100-02 MW-J 11/26/1996 808698.05 1057994.86 2,873.58 2,875.99 2.3 196.80 149.31 2,726.68 2 2,872 179.5 194.5 2,694.1 2,679.1 Bedrock
MSW Landfill Monitoring Wells
100-01 MW-2 No Well Record 809474.01 1059181.42 2,568.85 2,572.06 3.2 56.3 37.11 2,534.95
100-01 MW-3 No Well Record 809357.74 1058830.13 2,551.34 2,553.57 1.7 38.0 31.35 2,522.22
100-01 MW-AR No Well Record 808483.97 1059176.2 2,688.76 2,691.17 2.3 71.4 63.92 2,627.25 Assumed
Bedrock
100-01 MW-B 12/02/ 1996 809020.07 1059514.58 2,624.07 2,626.27 2.0 70.0 61.39 2,564.88 18 2,606 53.0 68.0 2,571.1 2,556.1 Bedrock
DENR Well
Construction/ Drilling
Log Record, dated
12/31/96
Notes:
Survey data showing the horizontal and vertical positions of the monitoring wells were presented in the Appendix A of "Fall 2009 Semiannual Water Quality Monitoring Report, Yancey-Mitchell County Construction and Demolition Debris Landfill" dated November 16, 2009.
No Well Record: Indicates that the well record, if it exists, was not readily obtainable.
NAD: North American Datum 1983
NAVD: North American Vertical Datum 1988
TOC: Top of casing
bgs: below ground surface
Depth to water: Measured on March 28 and 29, 2017
Saprolite DENR Well
Construction/Drilling
Log Record, dated
12/31/96
Assumed
Saprolite No Well
Construction/ Drilling
Record is Available
No Well Record No Well Record No Well
Record
No Well
Record
No Well
Record
No Well
Record
Source of Well
Construction
Information
Facility Permit Well ID Date Drilled
Geology of
Screened
Interval
Table 2
Summary of Laboratory Analyses Performed on Samples-March 2017
Spring 2017 Semiannual Water Quality Monitoring Report
Yancey-Mitchell County Closed Construction and Demolition Debris Landfill Page 1 of 1
June 2017
GROUNDWATER SAMPLES
VOCs Metals Sulfate Chloride TDS Alkalinity
EPA 8260B EPA 6020B
EPA 7470A
EPA
9056A
EPA
9056A SM 2540C SM 2320B
100-02 MW-H 03/29/2017 X X X X X X
100-02 MW-I 03/28/2017 X X X X X X
100-02 MW-J 03/28/2017 X X X X X X
SURFACE WATER SAMPLES
VOCs Metals Sulfate Chloride TDS Alkalinity
EPA 8260B EPA 6020B
EPA 7470A
EPA
9056A
EPA
9056A SM 2540C SM 2320B
100-02 SW-1 03/28/2017 X X X X X X
100-02 SW-2 03/28/2017 X X X X X X
QUALITY CONTROL SAMPLES
VOCs
EPA 8260B
100-02 TRIP BLANK (C&D)03/29/2017 X
100-02 TRIP BLANK (SW)03/28/2017 X
Notes:
VOCs Volatile organic compounds
FACILITY
PERMIT SAMPLE ID COLLECT DATE
VOCs and metals analysis include Appendix I constituents per 40 CFR Part 258. Metals include manganese, iron, and mercury in addition to Appendix I constituents.
Tetrahydrofuran analysis has been performed since the spring 2011 sampling event per the North Carolina Division of Waste Management, Solid Waste Section
requirement specified in the June 25, 2010 memorandum.
FACILITY
PERMIT WELL ID COLLECT DATE
FACILITY
PERMIT SAMPLE ID COLLECT DATE
Table 3
Summary of Analytical Results
Spring 2017 Semiannual Water Quality Monitoring Report
Yancey-Mitchell County Closed Construction and Demolition Debris Landfill
Page 1 of 2
June 2017
Metals (including Appendix I)
Lab Certification 40
Lab Methods EPA 6020B and EPA 7470A (Mercury)
Parameter Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Mercury Nickel Selenium Silver Thallium Vanadium Zinc
CAS Number 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-96-5 7439-97-6 7440-02-0 7782-49-2 7440-22-4 7440-28-0 7440-62-2 7440-66-6
SWS ID 14 15 23 34 51 53 54 340 131 342 132 152 183 184 194 209 213
Units µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L
Sample ID Collect Date Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result
Groundwater Samples
MW-H 03/29/2017 0.45 U 71 J 0.098 J 0.28 J 1.6 J, B 0.84 J 2.2 J 580 0.30 J 930 0.60 1.2 J 0.70 J 0.079 J 0.11 J 0.92 J 5.8 J
MW-I 03/28/2017 0.45 U 62 J 0.16 J 0.090 J 0.69 J, B 0.52 J 0.48 J 370 0.071 J 170 0.030 U 1.1 J 0.450 U 0.067 U 0.12 J 0.79 U 8.2 J
MW-J 03/28/2017 1.8 J 16 J 0.068 U 0.053 U 1.2 J, B 0.68 J 1.8 J 190 J 0.21 J 8.4 J 0.030 U 1.4 J 1.7 J 0.067 U 0.060 J 0.87 J 5.7 J
Surface Water Samples
SW-1 03/28/2017 0.45 U 18 J 0.068 U 0.053 U 0.42 J 0.10 J 0.93 J 240 J 0.14 J 31 J 0.030 U 0.25 J 0.450 U 0.067 U 0.34 J 0.79 U 2.6 J
SW-2 03/28/2017 0.45 U 16 J 0.068 U 0.053 U 0.48 J 0.12 J 1.1 J 250 J 0.15 J 25 J 0.030 U 0.34 J 0.450 U 0.067 U 0.23 J 0.79 U 5.1 J
Quality Control Samples
TRIP BLANK (C&D)03/29/2017 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
TRIP BLANK (SW)03/28/2017 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
MDL 0.450 0.120 0.068 0.053 0.320 0.056 0.410 20.0 0.061 0.760 0.030 0.082 0.450 0.067 0.018 0.79 1.30
MRL 1.0 5.0 1.0 1.0 2.0 1.0 5.0 100 1.0 5.0 0.20 2.0 5.0 5.0 1.0 1.0 10
SWSL 10 100 1 1 10 10 10 300 10 50 0.2 50 10 10 5.5 25 10
2L 10 700 NE 2 10 NE 1,000 300 15 50 1 100 20 20 NE NE 1,000
IMAC NE NE 4 NE NE 1 NE NE NE NE NE NE NE NE 0.2 0.3 NE
GWPS NE NE 4 NE NE 1 NE NE NE NE NE NE NE NE 0.28 0.3 NE
2B 10 200,000 6.5 0.15 35 4 2.7 NE 0.54 NE 0.012 16 5 0.06 0.47 NE 36
Notes:
Detections: Only detected constituents are listed on this table. Please refer to the Prism laboratory report of analyses for further details.
Appendix I: Indicates VOCs and metals per 40 CFR Part 258.
Lab Method: The analytical method used to analyze the constituents.
CAS Number: A unique number assigned by the Chemical Abstracts Service (CAS) to all identified parameters.
SWS ID: Solid Waste Section Identification Number.
Collect Date: The date on which the sample was collected in the field.
Result: Analytical data reported by the laboratory or field data collected by Anchor QEA.
U: A laboratory data qualifier used for parameters not detected at concentrations above MDL.
J: A laboratory data qualifier used for parameters detected at estimated concentrations above MDL but below MRL.
J: A qualifier assigned by Anchor QEA to reflect a detected concentration that is greater than MRL and MDL but less than the SWSL.
B: A laboratory data qualifier used to indicate an analyte that is found in the associated blank at a concentration greater than one-half of the report limit.
IMAC: Interim Maximum Allowable Concentration. The IMAC concentrations are listed in Appendix #1 of the 2L.
NE: Not Established
NA: Not Applicable
0.60: Bolded numbers indicate an SWSL exceedance
580: Shaded cells indicate the result is in exceedance of the 2L, IMAC, GWP, or 2B standard.
Units: Micrograms per liter (µg/L) and milligrams per liter (mg/L) for analytical results, Standard Units (SU) for pH, nephelometric turbidity units (NTU) for turbidity, microsiemens per centimeter (µS/cm) for specific conductivity,
degrees celcius (°C) for temperature, and millivolts (mV) for oxidation reduction potential.
2B: Indicates surface water standard per North Carolina Administrative Code, Title 15A: Department of Environmental Quality, Subchapter 2B - Surface Water and Wetland Standards (last amended in March 2016) or standard obtained from National Criteria per EPA table (current
as of May 15, 2013).
MDL: Method detection limit, which is the minimum concentration of a substance that can be measured and reported with 99% confidence that the analyte concentration is greater than zero.
MRL: Method reporting limit, which is the minimum concentration of a target analyte that can be accurately determined by the referenced method.
SWSL: The Solid Waste Section Limit. This limit (identified by DEQ) is the lowest amount of analyte in a sample that can be quantitatively determined with suitable precision and accuracy.
2L: Subchapter 2L - Groundwater Classifications and Standards, DEQ (Amended April 1, 2013). Groundwater standard from North Carolina Administrative Code, Title 15A: Department of Environmental Quality.
GWPS: The Groundwater Protection Standard pursuant to 15A NCAC 13B .1634, DEQ. Current standards were obtained from https://deq.nc.gov/about/divisions/waste-management/waste-management-permit-guidance/solid-waste-section/environmental-
monitoring/environmental-monitoring-list (last updated June, 2011). GWPS is used only if 2L or IMAC standards are not established for specific constituent.
Table 3
Summary of Analytical Results
Spring 2017 Semiannual Water Quality Monitoring Report
Yancey-Mitchell County Closed Construction and Demolition Debris Landfill
Page 2 of 2
June 2017
VOCs (Appendix I)Inorganics Field Parameters
Lab Certification 12
Lab Methods EPA 8260B EPA 9056A EPA 9056A SM2320 B SM2540 C 5445 (pH only)
Parameter
cis-1,2-
Dichloro-
ethene
Ethyl-
benzene
m & p
Xylene o-Xylene Tetra-
hydrofuran
Xylene
(Total)Chloride Sulfate
Total
Alkalinity to
pH 4.5
Total
Dissolved
Solids
pH Dissolved
Oxygen Turbidity Temperature Specific
Conductivity
Oxidation
Reduction
Potential
CAS Number 156-59-2 100-41-4 108-38-3 95-47-6 109-99-9 1330-20-7 16887-00-6 14808-79-8 NA NA SW320 7782-44-7 SW330 SW325 SW323 SW336
SWS ID 78 110 359 408 458 346 301 315 337 311 320 356 330 325 323 336
Units µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L SU mg/L NTU °C µS/cm mV
Sample ID Collect Date Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result Result
Groundwater Samples
MW-H 03/29/2017 0.69 J 0.061 U 0.12 U 0.044 U 39 0.15 U 39,000 76,000 J 100,000 330,000 5.73 3.40 29.24 13.47 362 293.5
MW-I 03/28/2017 0.056 U 0.061 U 0.12 U 0.044 U 42 0.15 U 15,000 570 J 23,000 76,000 5.29 3.22 8.78 12.35 99 249.0
MW-J 03/28/2017 0.056 U 0.90 J 3.7 2.0 0.16 U 5.6 1,800 100,000 J 59,000 250,000 6.95 7.84 4.48 13.80 310 281.6
Surface Water Samples
SW-1 03/28/2017 0.056 U 0.061 U 0.12 U 0.044 U 0.16 U 0.15 U 7,200 11,000 J 13,000 52,000 6.25 9.17 2.17 13.53 70 299.7
SW-2 03/28/2017 0.056 U 0.061 U 0.12 U 0.044 U 0.16 U 0.15 U 7,200 7,300 J 11,000 44,000 J 6.45 7.94 9.22 13.91 61 300.1
Quality Control Samples
TRIP BLANK (C&D)03/29/2017 0.056 U 0.061 U 0.12 U 0.044 U 0.16 U 0.15 U NA NA NA NA NA NA NA NA NA NA
TRIP BLANK (SW)03/28/2017 0.056 U 0.061 U 0.12 U 0.044 U 0.16 U 0.15 U NA NA NA NA NA NA NA NA NA NA
MDL 0.056 0.061 0.12 0.044 0.16 0.15 44 320 770 1,400 NA NA NA NA NA NA
MRL 0.50 0.50 1.0 0.50 10 3.0 1,000 1,000 5,000 50,000 NA NA NA NA NA NA
SWSL 5 1 NE NE NE 5 NE 250,000 NE NE NE NE NE NE NE NE
2L 70 600 500 500 NE 500 250,000 250,000 NE 500,000 6.5-8.5 NE NE NE NE NE
IMAC NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE
GWP NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE
2B 720 97 NE 600 NE 670 230,000 NE NE NE 6.0-9.0 >6.0 10 NE NE NE

Figures
[
0 2,0001,000
Feet
NOTE:Burnsville, NC is located approximately 7.0 milessouthwest of the landfill parcel boundary.
LEGEND:
Landfill Property Boundary
Publish Date: 2017/04/07, 3:10 PM | User: alesueurFilepath: P:\Yancey County\Solid Waste\Figures\GIS\MXD\2017\Spring\Figure 1 - Site Location Map AQ.mxd
Figure 1Site Location Map
Yancey-Mitchell Counties Closed Landfill Water Quality ReportYancey-Mitchell County Closed MSW (Permit #100-01) and Closed C&D (Permit #100-02) Landfills
SOURCES:Basemap: USGS 1:24,000 Scale Topo Maps, Micaville Quadrangle, 1987Site Property Boundary: Yancey County GIS
Anchor QEA of North Carolina, PLLC%7 miles to Burnsville, NC %NC Hwy-80
[
0 500 1,000250
Feet
NOTE(S):1. Posted data are constituents detected atconcentrations above their respective water qualitystandard (2L Standard, Interim Maximum AllowableConcentration [IMAC], or 2B Standard)2. Sample Dates: March 28 and 29, 20173. Surface water sample locations are approximate. Thedownstream surface water sample (SW-2) is shown onthe map inset.
LEGEND:
!U Bedrock Monitoring Well Location
!U Saprolite Monitoring Well Location
#*Surface Water Sample Location
Approximate Landfill Boundaries
Landfill Parcel Boundary
Streams
Publish Date: 2017/05/03, 1:37 PM | User: alesueurFilepath: P:\Yancey County\Solid Waste\Figures\GIS\MXD\2017\Spring\Figure 2 - C&D Sample Location Map AQ.mxd
Figure 2Sample Location and Posted Data Map
Yancey-Mitchell County Closed C&D Landfill Water Quality ReportYancey-Mitchell County Closed MSW (Permit #100-01) and Closed C&D (Permit #100-02) Landfills
SOURCE(S):Basemap: NC OneMap 2010Parcels and Streams: Yancey County GISMonitoring Wells: Survey data from Webb A. Morganand Associates, P.A. (2009)
Anchor QEA of North Carolina, PLLC
2L Groundwater Standards or IMACIron (300 µg/L)Manganese (50 µg/L)pH (6.5-8.5 Standard Units [SU])
#*!U
!U
!U
MW-I
Iron (370 µg/L)
Manganese (170 µg/L)
pH (5.29 SU)
MW-H
Iron (580 µg/L)Manganese (930 µg/L)
pH (5.73 SU)
MW-J (Background Well)
No Exceedances
Construction and Demolition Debris Landfill
Municipal SolidWaste Landfill
SW-1
No Exceedances%Flow DirectionREBELSREBELSCREEKCREEK
NORTH TOE RIVERNORTH TOE RI
VERWOLF BRANCHWOLF BRANCH#*
#*
SW-2
No Exceedances
0 6,0003,000
Feet
%%%%
!U
!U
!U
!U
!U
!U
!U %Flow Direction
Flow Direction
Generalized Bedrock Groundwater Flow
Generalized SaproliteGroundwater Flow
Construction
and DemolitionDebris Landfill
Municipal SolidWaste Landfill
MW-2
(2,534.95)MW-3
(2,522.22)
MW-AR
(2,627.25)
MW-B
(2,564.88)
MW-J
(2,726.68)
MW-H
(2,506.94)
MW-I
(2,521.96)25402580
2380
2520
2560
2460 2 5 6 0
26802440
2
4
80
2420
26602640
2420
2620
2540
24602520
24402480
2360
2600
2400
25002500
2
5
0
0
2700270026
00
24002700
24002500
2400
27002700
280025802560242028602480
2620278027202
7
4
0
2480
2
5
40
2
6
8
0 2520244028602720
24202520
2380
24402 4 2 0
2640
2840 244027202460
282026202460
2680
27802
6
6
0
2760 2480264027602680
2360REBELS CREEKREBELS CREEKWOLF BRANCHWOLF BRANCHNORTH TOE RIVERNORTH TOE RIVER
Publish Date: 2017/06/13, 1:42 PM | User: alesueurFilepath: P:\Yancey County\Solid Waste\Figures\GIS\MXD\2017\Spring\Fig3AQ.mxd
[
0 400200
Feet
NOTES:1. (2,521.96) = Calculatedgroundwater elevation2. Groundwater elevations arebased on depth to watermeasurements collected on March28 and 29, 2017.
Figure 3Generalized Groundwater Flow Direction Map
Yancey-Mitchell County Closed MSW and C&D Landfills Water Quality ReportsYancey-Mitchell County Closed MSW (Permit #100-01) and Closed C&D (Permit #100-02) Landfills
LEGEND:
!U Bedrock Monitoring Well
Location
!U Saprolite Monitoring WellLocation
Approximate Landfill Boundary
Elevation Contour (20ftInterval)
Landfill Parcel
SOURCE(S):Parcels: Yancey County GISMonitoring Wells: Survey data fromWebb A. Morgan and Associates,P.A. (2009)Elevation Contours: Yancey Countyand Mitchell County Lidar, 2007Roads: Yancey County and MitchellCounty GIS
Anchor QEA of North Carolina, PLLC

Appendix A
Sampling Logs and Equipment
Documentation & Instrument Calibration
Data Sheets

Appendix B
Reports of Laboratory Analysis and Chain-
of-Custody Documentation
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
04/18/2017
Anchor QEA of North Carolina, PLLC
Brian Gant
231 Haywood Street
Asheville, NC 28801
Project: Yancey-Mitchell MSW Landfill
Lab Submittal Date: 03/30/2017
Prism Work Order: 7030456
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
President/Project Manager
Reviewed ByRobbi A. Jones Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
MI Matrix spike outside of the control limits. Matrix interference suspected.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 21
Sample Receipt Summary
04/18/2017
Prism Work Order: 7030456
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
7030456-01 03/28/17MW-AR 03/30/17Water
7030456-02 03/29/17MW-B 03/30/17Water
7030456-03 03/29/17MW-2 03/30/17Water
7030456-04 03/28/17MW-3 03/30/17Water
7030456-05 03/29/17Trip Blank 03/30/17Water
Samples were received in good condition at 1.9 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 21
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 7030456
04/18/2017
Summary of Detections
0.51 J ug/L7030456-01 MW-AR Arsenic 6020B
22 ug/L7030456-01 MW-AR Barium 6020B
0.13 J ug/L7030456-01 MW-AR Cadmium 6020B
0.54 J ug/L7030456-01 MW-AR Chromium 6020B
0.11 J ug/L7030456-01 MW-AR Lead 6020B
0.099 J ug/L7030456-01 MW-AR Silver 6020B
4.6 ug/L7030456-02 MW-B Arsenic 6020B
71 ug/L7030456-02 MW-B Barium 6020B
0.63 J ug/L7030456-02 MW-B Chromium 6020B
0.36 J ug/L7030456-02 MW-B Lead 6020B
0.13 J ug/L7030456-02 MW-B Silver 6020B
5.6 ug/L7030456-02 MW-B 1,4-Dichlorobenzene 8260B
14 ug/L7030456-02 MW-B Acetone 8260B
3.8 ug/L7030456-02 MW-B Benzene 8260B
4.7 ug/L7030456-02 MW-B Chlorobenzene 8260B
1.9 ug/L7030456-02 MW-B Ethylbenzene 8260B
5.1 ug/L7030456-02 MW-B m,p-Xylenes 8260B
3.3 ug/L7030456-02 MW-B o-Xylene 8260B
180 ug/L7030456-02 MW-B Tetrahydrofuran 8260B
2.0 ug/L7030456-02 MW-B Toluene 8260B
2.6 ug/L7030456-02 MW-B Vinyl chloride 8260B
8.4 ug/L7030456-02 MW-B Xylenes, total 8260B
170 ug/L7030456-03 MW-2 Barium 6020B
0.20 J ug/L7030456-03 MW-2 Cadmium 6020B
0.33 J ug/L7030456-03 MW-2 Chromium 6020B
0.39 J ug/L7030456-03 MW-2 Lead 6020B
2.5 J ug/L7030456-03 MW-2 Selenium 6020B
0.071 J ug/L7030456-03 MW-2 Silver 6020B
3.4 ug/L7030456-03 MW-2 1,4-Dichlorobenzene 8260B
0.71 ug/L7030456-03 MW-2 Benzene 8260B
3.8 ug/L7030456-03 MW-2 Chlorobenzene 8260B
65 ug/L7030456-04 MW-3 Barium 6020B
0.082 J ug/L7030456-04 MW-3 Cadmium 6020B
0.79 J ug/L7030456-04 MW-3 Chromium 6020B
0.084 J ug/L7030456-04 MW-3 Lead 6020B
0.94 ug/L7030456-04 MW-3 1,4-Dichlorobenzene 8260B
5.1 ug/L7030456-04 MW-3 Acetone 8260B
1.6 ug/L7030456-04 MW-3 Chlorobenzene 8260B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 21
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street
Project: Yancey-Mitchell MSW LandfillAnchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030456-01
Prism Work Order: 7030456
Time Collected: 03/28/17 14:35
Time Submitted: 03/30/17 11:25
MW-AR
SWSL
Total Metals
7470A P7D016010.20 4/12/17 11:38 JABug/L 0.030Mercury0.2<0.030
6020B P7D006311.0 4/10/17 16:47 BGMJug/L 0.45Arsenic100.51
6020B P7D006315.0 4/10/17 16:47 BGMug/L 0.12Barium10022
6020B P7D006311.0 4/10/17 16:47 BGMJug/L 0.053Cadmium10.13
6020B P7D006311.0 4/10/17 16:47 BGMJug/L 0.32Chromium100.54
6020B P7D006311.0 4/10/17 16:47 BGMJug/L 0.061Lead100.11
6020B P7D006315.0 4/10/17 16:47 BGMug/L 0.45Selenium10<0.45
6020B P7D006315.0 4/10/17 16:47 BGMJug/L 0.067Silver100.099
Volatile Organic Compounds by GC/MS
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7C052011.0 4/1/17 0:02 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7C052012.0 4/1/17 0:02 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7C052015.0 4/1/17 0:02 KDMug/L 0.31Acetone100<0.31
8260B P7C05201204/1/17 0:02 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.048Benzene1<0.048
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7C052011.0 4/1/17 0:02 KDMug/L 0.040Bromoform3<0.040
8260B P7C052011.0 4/1/17 0:02 KDMug/L 0.18Bromomethane10<0.18
8260B P7C052015.0 4/1/17 0:02 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.062Chlorobenzene3<0.062
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.22Chloroethane10<0.22
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.076Chloroform5<0.076
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.079Chloromethane1<0.079
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 21
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street
Project: Yancey-Mitchell MSW LandfillAnchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030456-01
Prism Work Order: 7030456
Time Collected: 03/28/17 14:35
Time Submitted: 03/30/17 11:25
MW-AR
SWSL
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.065Dibromomethane10<0.065
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7C052011.0 4/1/17 0:02 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7C052015.0 4/1/17 0:02 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7C052015.0 4/1/17 0:02 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7C052015.0 4/1/17 0:02 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7C052015.0 4/1/17 0:02 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7C052011.0 4/1/17 0:02 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.044o-Xylene NE<0.044
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.047Styrene1<0.047
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7C05201104/1/17 0:02 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.044Toluene1<0.044
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7C05201104/1/17 0:02 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7C052012.0 4/1/17 0:02 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7C052010.50 4/1/17 0:02 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7C052013.0 4/1/17 0:02 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124112 %4-Bromofluorobenzene
75-129100 %Dibromofluoromethane
77-123100 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 21
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street
Project: Yancey-Mitchell MSW LandfillAnchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030456-02
Prism Work Order: 7030456
Time Collected: 03/29/17 11:48
Time Submitted: 03/30/17 11:25
MW-B
SWSL
Total Metals
7470A P7D016010.20 4/12/17 11:27 JABug/L 0.030Mercury0.2<0.030
6020B P7D006311.0 4/10/17 17:00 BGMug/L 0.45Arsenic104.6
6020B P7D006315.0 4/10/17 17:00 BGMug/L 0.12Barium10071
6020B P7D006311.0 4/10/17 17:00 BGMug/L 0.053Cadmium1<0.053
6020B P7D006311.0 4/10/17 17:00 BGMJug/L 0.32Chromium100.63
6020B P7D006311.0 4/10/17 17:00 BGMJug/L 0.061Lead100.36
6020B P7D006315.0 4/10/17 17:00 BGMug/L 0.45Selenium10<0.45
6020B P7D006315.0 4/10/17 17:00 BGMJug/L 0.067Silver100.13
Volatile Organic Compounds by GC/MS
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7C052011.0 4/1/17 3:29 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7C052012.0 4/1/17 3:29 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.0501,4-Dichlorobenzene 15.6
8260B P7C052015.0 4/1/17 3:29 KDMug/L 0.31Acetone10014
8260B P7C05201204/1/17 3:29 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.048Benzene13.8
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7C052011.0 4/1/17 3:29 KDMug/L 0.040Bromoform3<0.040
8260B P7C052011.0 4/1/17 3:29 KDMug/L 0.18Bromomethane10<0.18
8260B P7C052015.0 4/1/17 3:29 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.062Chlorobenzene34.7
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.22Chloroethane10<0.22
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.076Chloroform5<0.076
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.079Chloromethane1<0.079
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 21
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street
Project: Yancey-Mitchell MSW LandfillAnchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030456-02
Prism Work Order: 7030456
Time Collected: 03/29/17 11:48
Time Submitted: 03/30/17 11:25
MW-B
SWSL
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.065Dibromomethane10<0.065
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.061Ethylbenzene11.9
8260B P7C052011.0 4/1/17 3:29 KDMug/L 0.12m,p-Xylenes NE5.1
8260B P7C052015.0 4/1/17 3:29 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7C052015.0 4/1/17 3:29 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7C052015.0 4/1/17 3:29 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7C052015.0 4/1/17 3:29 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7C052011.0 4/1/17 3:29 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.044o-Xylene NE3.3
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.047Styrene1<0.047
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7C0520101004/1/17 3:55 KDMug/L 1.6TetrahydrofuranNE180
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.044Toluene12.0
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7C05201104/1/17 3:29 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7C052012.0 4/1/17 3:29 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7C052010.50 4/1/17 3:29 KDMug/L 0.097Vinyl chloride 12.6
8260B P7C052013.0 4/1/17 3:29 KDMug/L 0.15Xylenes, total 58.4
Surrogate Recovery Control Limits
80-124109 %4-Bromofluorobenzene
75-129103 %Dibromofluoromethane
77-123100 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 21
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street
Project: Yancey-Mitchell MSW LandfillAnchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030456-03
Prism Work Order: 7030456
Time Collected: 03/29/17 11:00
Time Submitted: 03/30/17 11:25
MW-2
SWSL
Total Metals
7470A P7D016010.20 4/12/17 11:42 JABug/L 0.030Mercury0.2<0.030
6020B P7D006311.0 4/10/17 17:04 BGMug/L 0.45Arsenic10<0.45
6020B P7D006315.0 4/10/17 17:04 BGMug/L 0.12Barium100170
6020B P7D006311.0 4/10/17 17:04 BGMJug/L 0.053Cadmium10.20
6020B P7D006311.0 4/10/17 17:04 BGMJug/L 0.32Chromium100.33
6020B P7D006311.0 4/10/17 17:04 BGMJug/L 0.061Lead100.39
6020B P7D006315.0 4/10/17 17:04 BGMJug/L 0.45Selenium102.5
6020B P7D006315.0 4/10/17 17:04 BGMJug/L 0.067Silver100.071
Volatile Organic Compounds by GC/MS
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7C052011.0 4/1/17 0:28 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7C052012.0 4/1/17 0:28 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.0501,4-Dichlorobenzene 13.4
8260B P7C052015.0 4/1/17 0:28 KDMug/L 0.31Acetone100<0.31
8260B P7C05201204/1/17 0:28 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.048Benzene10.71
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7C052011.0 4/1/17 0:28 KDMug/L 0.040Bromoform3<0.040
8260B P7C052011.0 4/1/17 0:28 KDMug/L 0.18Bromomethane10<0.18
8260B P7C052015.0 4/1/17 0:28 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.062Chlorobenzene33.8
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.22Chloroethane10<0.22
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.076Chloroform5<0.076
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.079Chloromethane1<0.079
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 21
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street
Project: Yancey-Mitchell MSW LandfillAnchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030456-03
Prism Work Order: 7030456
Time Collected: 03/29/17 11:00
Time Submitted: 03/30/17 11:25
MW-2
SWSL
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.065Dibromomethane10<0.065
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7C052011.0 4/1/17 0:28 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7C052015.0 4/1/17 0:28 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7C052015.0 4/1/17 0:28 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7C052015.0 4/1/17 0:28 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7C052015.0 4/1/17 0:28 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7C052011.0 4/1/17 0:28 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.044o-Xylene NE<0.044
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.047Styrene1<0.047
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7C05201104/1/17 0:28 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.044Toluene1<0.044
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7C05201104/1/17 0:28 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7C052012.0 4/1/17 0:28 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7C052010.50 4/1/17 0:28 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7C052013.0 4/1/17 0:28 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124113 %4-Bromofluorobenzene
75-129101 %Dibromofluoromethane
77-123102 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 21
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street
Project: Yancey-Mitchell MSW LandfillAnchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030456-04
Prism Work Order: 7030456
Time Collected: 03/28/17 11:28
Time Submitted: 03/30/17 11:25
MW-3
SWSL
Total Metals
7470A P7D016010.20 4/12/17 11:46 JABug/L 0.030Mercury0.2<0.030
6020B P7D006311.0 4/10/17 17:08 BGMug/L 0.45Arsenic10<0.45
6020B P7D006315.0 4/10/17 17:08 BGMug/L 0.12Barium10065
6020B P7D006311.0 4/10/17 17:08 BGMJug/L 0.053Cadmium10.082
6020B P7D006311.0 4/10/17 17:08 BGMJug/L 0.32Chromium100.79
6020B P7D006311.0 4/10/17 17:08 BGMJug/L 0.061Lead100.084
6020B P7D006315.0 4/10/17 17:08 BGMug/L 0.45Selenium10<0.45
6020B P7D006315.0 4/10/17 17:08 BGMug/L 0.067Silver10<0.067
Volatile Organic Compounds by GC/MS
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7C052011.0 4/1/17 0:54 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7C052012.0 4/1/17 0:54 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.0501,4-Dichlorobenzene 10.94
8260B P7C052015.0 4/1/17 0:54 KDMug/L 0.31Acetone1005.1
8260B P7C05201204/1/17 0:54 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.048Benzene1<0.048
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7C052011.0 4/1/17 0:54 KDMug/L 0.040Bromoform3<0.040
8260B P7C052011.0 4/1/17 0:54 KDMug/L 0.18Bromomethane10<0.18
8260B P7C052015.0 4/1/17 0:54 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.062Chlorobenzene31.6
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.22Chloroethane10<0.22
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.076Chloroform5<0.076
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.079Chloromethane1<0.079
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 21
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street
Project: Yancey-Mitchell MSW LandfillAnchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030456-04
Prism Work Order: 7030456
Time Collected: 03/28/17 11:28
Time Submitted: 03/30/17 11:25
MW-3
SWSL
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.065Dibromomethane10<0.065
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7C052011.0 4/1/17 0:54 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7C052015.0 4/1/17 0:54 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7C052015.0 4/1/17 0:54 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7C052015.0 4/1/17 0:54 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7C052015.0 4/1/17 0:54 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7C052011.0 4/1/17 0:54 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.044o-Xylene NE<0.044
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.047Styrene1<0.047
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7C05201104/1/17 0:54 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.044Toluene1<0.044
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7C05201104/1/17 0:54 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7C052012.0 4/1/17 0:54 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7C052010.50 4/1/17 0:54 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7C052013.0 4/1/17 0:54 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124112 %4-Bromofluorobenzene
75-129101 %Dibromofluoromethane
77-123101 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 21
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street
Project: Yancey-Mitchell MSW LandfillAnchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030456-05
Prism Work Order: 7030456
Time Collected: 03/29/17 00:00
Time Submitted: 03/30/17 11:25
Trip Blank
SWSL
Volatile Organic Compounds by GC/MS
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7C052011.0 3/31/17 20:34 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7C052012.0 3/31/17 20:34 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7C052015.0 3/31/17 20:34 KDMug/L 0.31Acetone100<0.31
8260B P7C05201203/31/17 20:34 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.048Benzene1<0.048
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7C052011.0 3/31/17 20:34 KDMug/L 0.040Bromoform3<0.040
8260B P7C052011.0 3/31/17 20:34 KDMug/L 0.18Bromomethane10<0.18
8260B P7C052015.0 3/31/17 20:34 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.062Chlorobenzene3<0.062
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.22Chloroethane10<0.22
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.076Chloroform5<0.076
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.079Chloromethane1<0.079
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.065Dibromomethane10<0.065
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7C052011.0 3/31/17 20:34 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7C052015.0 3/31/17 20:34 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7C052015.0 3/31/17 20:34 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7C052015.0 3/31/17 20:34 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7C052015.0 3/31/17 20:34 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 21
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street
Project: Yancey-Mitchell MSW LandfillAnchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030456-05
Prism Work Order: 7030456
Time Collected: 03/29/17 00:00
Time Submitted: 03/30/17 11:25
Trip Blank
SWSL
8260B P7C052011.0 3/31/17 20:34 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.044o-Xylene NE<0.044
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.047Styrene1<0.047
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7C05201103/31/17 20:34 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.044Toluene1<0.044
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7C05201103/31/17 20:34 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7C052012.0 3/31/17 20:34 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7C052010.50 3/31/17 20:34 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7C052013.0 3/31/17 20:34 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124114 %4-Bromofluorobenzene
75-129102 %Dibromofluoromethane
77-123104 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 21
4/18/17
Level II QC Report
231 Haywood Street
Project: Yancey-Mitchell MSW LandfillAnchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030456
Time Submitted: 3/30/2017 11:25:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7C0520 - 5030B
Blank (P7C0520-BLK1)Prepared & Analyzed: 03/31/17
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL1.0
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
Acetone ug/LBRL5.0
Acrylonitrile ug/LBRL20
Benzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL1.0
Bromomethane ug/LBRL1.0
Carbon disulfide ug/LBRL5.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Ethylbenzene ug/LBRL0.50
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL5.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Iodide ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL5.0
Methylene Chloride ug/LBRL1.0
o-Xylene ug/LBRL0.50
Styrene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Tetrahydrofuran ug/LBRL10
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
trans-1,4-Dichloro-2-butene ug/LBRL10
Trichloroethylene ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 21
4/18/17
Level II QC Report
231 Haywood Street
Project: Yancey-Mitchell MSW LandfillAnchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030456
Time Submitted: 3/30/2017 11:25:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7C0520 - 5030B
Blank (P7C0520-BLK1)Prepared & Analyzed: 03/31/17
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL2.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL3.0
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 11456.8
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10250.9
ug/L 50.00 77-123Surrogate: Toluene-d8 10250.9
LCS (P7C0520-BS1)Prepared & Analyzed: 03/31/17
1,1,1,2-Tetrachloroethane ug/L20.1 0.50 20.00 79-134101
1,1,1-Trichloroethane ug/L20.7 0.50 20.00 75-136104
1,1,2,2-Tetrachloroethane ug/L21.3 0.50 20.00 62-127106
1,1,2-Trichloroethane ug/L20.7 0.50 20.00 70-140104
1,1-Dichloroethane ug/L20.5 0.50 20.00 78-130102
1,1-Dichloroethylene ug/L19.4 0.50 20.00 70-15497
1,2,3-Trichloropropane ug/L21.2 1.0 20.00 71-127106
1,2-Dibromo-3-chloropropane ug/L19.8 2.0 20.00 63-13499
1,2-Dibromoethane ug/L22.5 0.50 20.00 77-135112
1,2-Dichlorobenzene ug/L20.7 0.50 20.00 78-128104
1,2-Dichloroethane ug/L20.8 0.50 20.00 68-131104
1,2-Dichloropropane ug/L21.2 0.50 20.00 77-130106
1,4-Dichlorobenzene ug/L20.5 0.50 20.00 75-126102
Acetone ug/L33.7 5.0 40.00 40-16684
Acrylonitrile ug/L38.8 20 40.00 81-12797
Benzene ug/L20.6 0.50 20.00 77-128103
Bromochloromethane ug/L20.2 0.50 20.00 78-135101
Bromodichloromethane ug/L20.7 0.50 20.00 76-138103
Bromoform ug/L17.8 1.0 20.00 71-13589
Bromomethane ug/L15.4 1.0 20.00 41-16877
Carbon disulfide ug/L20.6 5.0 20.00 59-135103
Carbon Tetrachloride ug/L21.6 0.50 20.00 72-142108
Chlorobenzene ug/L20.6 0.50 20.00 78-119103
Chloroethane ug/L16.2 0.50 20.00 57-14281
Chloroform ug/L20.7 0.50 20.00 77-130104
Chloromethane ug/L18.2 0.50 20.00 47-14591
cis-1,2-Dichloroethylene ug/L20.9 0.50 20.00 76-141105
cis-1,3-Dichloropropylene ug/L20.5 0.50 20.00 65-140103
Dibromochloromethane ug/L20.4 0.50 20.00 75-134102
Dibromomethane ug/L20.5 0.50 20.00 76-138102
Ethylbenzene ug/L21.2 0.50 20.00 80-127106
m,p-Xylenes ug/L44.1 1.0 40.00 77-133110
Methyl Butyl Ketone (2-Hexanone)ug/L20.1 5.0 20.00 64-137101
Methyl Ethyl Ketone (2-Butanone)ug/L20.8 5.0 20.00 71-134104
Methyl Iodide ug/L16.5 5.0 20.00 70-13082
Methyl Isobutyl Ketone ug/L18.9 5.0 20.00 69-13494
Methylene Chloride ug/L19.4 1.0 20.00 73-13197
o-Xylene ug/L21.7 0.50 20.00 78-128108
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 21
4/18/17
Level II QC Report
231 Haywood Street
Project: Yancey-Mitchell MSW LandfillAnchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030456
Time Submitted: 3/30/2017 11:25:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7C0520 - 5030B
LCS (P7C0520-BS1)Prepared & Analyzed: 03/31/17
Styrene ug/L19.2 0.50 20.00 78-12996
Tetrachloroethylene ug/L21.2 0.50 20.00 80-129106
Tetrahydrofuran ug/L19.8 10 20.00 70-13099
Toluene ug/L20.3 0.50 20.00 76-131101
trans-1,2-Dichloroethylene ug/L21.9 0.50 20.00 76-135109
trans-1,3-Dichloropropylene ug/L20.3 0.50 20.00 67-140101
trans-1,4-Dichloro-2-butene ug/L19.0 10 20.00 70-13095
Trichloroethylene ug/L20.2 0.50 20.00 77-133101
Trichlorofluoromethane ug/L17.4 0.50 20.00 62-14887
Vinyl acetate ug/L21.2 2.0 20.00 34-167106
Vinyl chloride ug/L21.3 0.50 20.00 57-141106
Xylenes, total ug/L65.8 3.0 60.00 77-133110
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10954.7
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10351.6
ug/L 50.00 77-123Surrogate: Toluene-d8 10451.8
LCS Dup (P7C0520-BSD1)Prepared & Analyzed: 03/31/17
1,1,1,2-Tetrachloroethane ug/L20.2 0.50 20.00 2079-134101 0.5
1,1,1-Trichloroethane ug/L20.6 0.50 20.00 2075-136103 0.3
1,1,2,2-Tetrachloroethane ug/L21.8 0.50 20.00 2062-127109 3
1,1,2-Trichloroethane ug/L20.9 0.50 20.00 2070-140104 0.7
1,1-Dichloroethane ug/L20.2 0.50 20.00 2078-130101 1
1,1-Dichloroethylene ug/L19.2 0.50 20.00 2070-15496 1
1,2,3-Trichloropropane ug/L22.4 1.0 20.00 2071-127112 6
1,2-Dibromo-3-chloropropane ug/L20.3 2.0 20.00 2063-134102 2
1,2-Dibromoethane ug/L22.3 0.50 20.00 2077-135111 0.9
1,2-Dichlorobenzene ug/L21.4 0.50 20.00 2078-128107 3
1,2-Dichloroethane ug/L20.9 0.50 20.00 2068-131105 0.4
1,2-Dichloropropane ug/L21.2 0.50 20.00 2077-130106 0.2
1,4-Dichlorobenzene ug/L20.7 0.50 20.00 2075-126104 1
Acetone ug/L35.3 5.0 40.00 2040-16688 5
Acrylonitrile ug/L40.8 20 40.00 2081-127102 5
Benzene ug/L20.4 0.50 20.00 2077-128102 0.9
Bromochloromethane ug/L20.7 0.50 20.00 2078-135104 2
Bromodichloromethane ug/L20.9 0.50 20.00 2076-138104 0.9
Bromoform ug/L18.2 1.0 20.00 2071-13591 2
Bromomethane ug/L15.7 1.0 20.00 2041-16879 2
Carbon disulfide ug/L20.3 5.0 20.00 2059-135102 1
Carbon Tetrachloride ug/L21.2 0.50 20.00 2072-142106 2
Chlorobenzene ug/L20.7 0.50 20.00 2078-119103 0.3
Chloroethane ug/L16.5 0.50 20.00 2057-14282 2
Chloroform ug/L20.7 0.50 20.00 2077-130104 0.05
Chloromethane ug/L17.6 0.50 20.00 2047-14588 3
cis-1,2-Dichloroethylene ug/L20.8 0.50 20.00 2076-141104 0.4
cis-1,3-Dichloropropylene ug/L20.7 0.50 20.00 2065-140103 0.6
Dibromochloromethane ug/L20.5 0.50 20.00 2075-134102 0.3
Dibromomethane ug/L21.2 0.50 20.00 2076-138106 3
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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4/18/17
Level II QC Report
231 Haywood Street
Project: Yancey-Mitchell MSW LandfillAnchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030456
Time Submitted: 3/30/2017 11:25:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7C0520 - 5030B
LCS Dup (P7C0520-BSD1)Prepared & Analyzed: 03/31/17
Ethylbenzene ug/L21.4 0.50 20.00 2080-127107 0.7
m,p-Xylenes ug/L44.1 1.0 40.00 2077-133110 0.05
Methyl Butyl Ketone (2-Hexanone)ug/L20.7 5.0 20.00 2064-137104 3
Methyl Ethyl Ketone (2-Butanone)ug/L22.3 5.0 20.00 2071-134111 7
Methyl Iodide ug/L18.6 5.0 20.00 2070-13093 12
Methyl Isobutyl Ketone ug/L19.6 5.0 20.00 2069-13498 4
Methylene Chloride ug/L19.4 1.0 20.00 2073-13197 0.05
o-Xylene ug/L21.8 0.50 20.00 2078-128109 0.6
Styrene ug/L19.2 0.50 20.00 2078-12996 0.1
Tetrachloroethylene ug/L21.2 0.50 20.00 2080-129106 0.2
Tetrahydrofuran ug/L20.7 10 20.00 2070-130103 4
Toluene ug/L20.4 0.50 20.00 2076-131102 0.6
trans-1,2-Dichloroethylene ug/L21.7 0.50 20.00 2076-135108 1
trans-1,3-Dichloropropylene ug/L20.5 0.50 20.00 2067-140102 1
trans-1,4-Dichloro-2-butene ug/L20.0 10 20.00 2070-130100 5
Trichloroethylene ug/L19.9 0.50 20.00 2077-13399 1
Trichlorofluoromethane ug/L17.3 0.50 20.00 2062-14886 0.8
Vinyl acetate ug/L21.7 2.0 20.00 2034-167108 2
Vinyl chloride ug/L21.5 0.50 20.00 2057-141108 1
Xylenes, total ug/L65.9 3.0 60.00 2077-133110 0.2
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 11155.3
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10150.4
ug/L 50.00 77-123Surrogate: Toluene-d8 10451.9
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 21
4/18/17
Level II QC Report
231 Haywood Street
Project: Yancey-Mitchell MSW LandfillAnchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030456
Time Submitted: 3/30/2017 11:25:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P7D0063 - 3005A
Blank (P7D0063-BLK1)Prepared: 04/06/17 Analyzed: 04/10/17
Arsenic ug/LBRL1.0
Barium ug/L0.467 5.0 J
Cadmium ug/LBRL1.0
Chromium ug/LBRL1.0
Lead ug/L0.110 1.0 J
Selenium ug/LBRL5.0
Silver ug/L0.139 5.0 J
LCS (P7D0063-BS1)Prepared: 04/06/17 Analyzed: 04/10/17
Arsenic ug/L1051.0 100.0 80-120105
Barium ug/L1065.0 100.0 80-120106
Cadmium ug/L1061.0 100.0 80-120106
Chromium ug/L1011.0 100.0 80-120101
Lead ug/L1071.0 100.0 80-120107
Selenium ug/L1015.0 100.0 80-120101
Silver ug/L1155.0 100.0 80-120115
Matrix Spike (P7D0063-MS1)Prepared: 04/06/17 Analyzed: 04/10/17 Source: 7030456-01
Arsenic ug/L1021.0 100.0 0.511 75-125102
Barium ug/L1245.0 100.0 21.8 75-125102
Cadmium ug/L1011.0 100.0 0.133 75-125101
Chromium ug/L99.3 1.0 100.0 0.535 75-12599
Lead ug/L1031.0 100.0 0.106 75-125103
Selenium ug/L98.7 5.0 100.0 BRL 75-12599
Silver ug/L1105.0 100.0 0.0990 75-125110
Matrix Spike Dup (P7D0063-MSD1)Prepared: 04/06/17 Analyzed: 04/10/17 Source: 7030456-01
Arsenic ug/L1011.0 100.0 0.511 2075-125100 1
Barium ug/L1205.0 100.0 21.8 2075-12598 3
Cadmium ug/L98.3 1.0 100.0 0.133 2075-12598 3
Chromium ug/L96.8 1.0 100.0 0.535 2075-12596 3
Lead ug/L1011.0 100.0 0.106 2075-125101 2
Selenium ug/L96.3 5.0 100.0 BRL 2075-12596 2
Silver ug/L1075.0 100.0 0.0990 2075-125107 2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 21
4/18/17
Level II QC Report
231 Haywood Street
Project: Yancey-Mitchell MSW LandfillAnchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030456
Time Submitted: 3/30/2017 11:25:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P7D0063 - 3005A
Post Spike (P7D0063-PS1)Prepared: 04/06/17 Analyzed: 04/07/17 Source: 7030456-01
Arsenic ug/L177 200.0 0.511 80-12088
Barium ug/L201 200.0 21.8 80-12089
Cadmium ug/L181 200.0 0.133 80-12090
Chromium ug/L179 200.0 0.535 80-12089
Lead ug/L195 200.0 0.106 80-12098
Selenium ug/L167 200.0 0.126 80-12083
Silver ug/L198 200.0 0.0990 80-12099
Batch P7D0160 - 7470A
Blank (P7D0160-BLK1)Prepared & Analyzed: 04/12/17
Mercury ug/LBRL0.20
LCS (P7D0160-BS1)Prepared & Analyzed: 04/12/17
Mercury ug/L8.74 0.20 9.375 80-12093
Matrix Spike (P7D0160-MS1)Prepared & Analyzed: 04/12/17 Source: 7030456-02
Mercury ug/L3.26 0.20 9.375 BRL MI80-12035
Matrix Spike Dup (P7D0160-MSD1)Prepared & Analyzed: 04/12/17 Source: 7030456-02
Mercury ug/L3.73 0.20 9.375 BRL 20 MI80-12040 14
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
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Sample Extraction Data
Prep Method: 3005A
Lab Number Batch Date/TimeInitialFinal
P7D00637030456-01 04/06/17 7:2550 50mL mL
P7D00637030456-02 04/06/17 7:2550 50mL mL
P7D00637030456-03 04/06/17 7:2550 50mL mL
P7D00637030456-04 04/06/17 7:2550 50mL mL
Prep Method: 7470A
Lab Number Batch Date/TimeInitialFinal
P7D01607030456-01 04/12/17 7:5020 30mL mL
P7D01607030456-02 04/12/17 7:5020 30mL mL
P7D01607030456-03 04/12/17 7:5020 30mL mL
P7D01607030456-04 04/12/17 7:5020 30mL mL
Prep Method: 5030B
Lab Number Batch Date/TimeInitialFinal
P7C05207030456-01 03/31/17 16:1010 10mL mL
P7C05207030456-02 03/31/17 16:1010 10mL mL
P7C05207030456-02 03/31/17 16:1010 10mL mL
P7C05207030456-03 03/31/17 16:1010 10mL mL
P7C05207030456-04 03/31/17 16:1010 10mL mL
P7C05207030456-05 03/31/17 16:1010 10mL mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 21
Page 21 of 21
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
04/17/2017
Anchor QEA of North Carolina, PLLC
Brian Gant
231 Haywood Street
Asheville, NC 28801
Project: Yancey-Mitchell Background Well
Lab Submittal Date: 03/30/2017
Prism Work Order: 7030457
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
President/Project Manager
Reviewed ByRobbi A. Jones Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
A Method Blank is less than 1/2 of the reporting limit of 2 ug/L which is reported on the samples in this analytical
batch.
B Analyte is found in the associated blank at a concentration >1/2 RL.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 15
Sample Receipt Summary
04/17/2017
Prism Work Order: 7030457
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
7030457-01 03/28/17MW-J 03/30/17Water
Samples were received in good condition at 2.1 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 15
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 7030457
04/17/2017
Summary of Detections
1800 ug/L7030457-01 MW-J Chloride 9056A
100000 ug/L7030457-01 MW-J Sulfate 9056A
59000 ug/L7030457-01 MW-J Total Alkalinity to pH 4.5 SM2320 B
250000 ug/L7030457-01 MW-J Total Dissolved Solids SM2540 C
1.8 ug/L7030457-01 MW-J Arsenic 6020B
16 ug/L7030457-01 MW-J Barium 6020B
1.2 J, B ug/L7030457-01 MW-J Chromium 6020B
0.68 J ug/L7030457-01 MW-J Cobalt 6020B
1.8 J ug/L7030457-01 MW-J Copper 6020B
190 ug/L7030457-01 MW-J Iron 6020B
0.21 J ug/L7030457-01 MW-J Lead 6020B
8.4 ug/L7030457-01 MW-J Manganese 6020B
1.4 J ug/L7030457-01 MW-J Nickel 6020B
1.7 J ug/L7030457-01 MW-J Selenium 6020B
0.060 J ug/L7030457-01 MW-J Thallium 6020B
0.87 J ug/L7030457-01 MW-J Vanadium 6020B
5.7 J ug/L7030457-01 MW-J Zinc 6020B
0.90 ug/L7030457-01 MW-J Ethylbenzene 8260B
3.7 ug/L7030457-01 MW-J m,p-Xylenes 8260B
2.0 ug/L7030457-01 MW-J o-Xylene 8260B
5.6 ug/L7030457-01 MW-J Xylenes, total 8260B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 15
Laboratory Report
04/17/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street
Project: Yancey-Mitchell Background
Well
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030457-01
Prism Work Order: 7030457
Time Collected: 03/28/17 12:47
Time Submitted: 03/30/17 11:25
MW-J
SWSL
Anions by Ion Chromatography
9056A P7D0014110003/30/17 12:28 EGCug/L 44ChlorideNE1800
9056A P7D0014110003/30/17 12:28 EGCug/L 320Sulfate250000100000
General Chemistry Parameters
SM2320 B P7C0513150003/31/17 10:30 EGCug/L 770Total Alkalinity to pH 4.5 NE59000
SM2540 C P7D00241500004/3/17 14:46 SLSug/L 1400Total Dissolved Solids NE250000
Total Metals
7470A P7D020210.20 4/13/17 13:01 JABug/L 0.030Mercury0.2<0.030
6020B P7D004611.0 4/5/17 20:55 bgmug/L 0.41Antimony6<0.41
6020B P7D004611.0 4/5/17 20:55 bgmug/L 0.45Arsenic101.8
6020B P7D004615.0 4/5/17 20:55 bgmug/L 0.12Barium10016
6020B P7D004611.0 4/5/17 20:55 bgmug/L 0.068Beryllium1<0.068
6020B P7D004611.0 4/5/17 20:55 bgmug/L 0.053Cadmium1<0.053
6020B P7D004612.0 4/5/17 20:55 bgmJ, B ug/L 0.32Chromium101.2
6020B P7D004611.0 4/5/17 20:55 bgmJug/L 0.056Cobalt100.68
6020B P7D004615.0 4/5/17 20:55 bgmJug/L 0.41Copper101.8
6020B P7D004611004/5/17 20:55 bgmug/L 20Iron300190
6020B P7D004611.0 4/5/17 20:55 bgmJug/L 0.061Lead100.21
6020B P7D004615.0 4/13/17 16:31 7800ug/L 0.76Manganese508.4
6020B P7D004612.0 4/5/17 20:55 bgmJug/L 0.082Nickel501.4
6020B P7D004615.0 4/5/17 20:55 bgmJug/L 0.45Selenium101.7
6020B P7D004615.0 4/5/17 20:55 bgmug/L 0.067Silver10<0.067
6020B P7D004611.0 4/5/17 20:55 bgmJug/L 0.018Thallium5.50.060
6020B P7D004611.0 4/5/17 20:55 bgmJug/L 0.79Vanadium250.87
6020B P7D00461104/5/17 20:55 bgmJug/L 1.3Zinc105.7
Volatile Organic Compounds by GC/MS
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7C052011.0 4/1/17 1:20 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7C052012.0 4/1/17 1:20 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.111,2-Dichloropropane 1<0.11
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 15
Laboratory Report
04/17/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street
Project: Yancey-Mitchell Background
Well
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030457-01
Prism Work Order: 7030457
Time Collected: 03/28/17 12:47
Time Submitted: 03/30/17 11:25
MW-J
SWSL
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7C052015.0 4/1/17 1:20 KDMug/L 0.31Acetone100<0.31
8260B P7C05201204/1/17 1:20 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.048Benzene1<0.048
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7C052011.0 4/1/17 1:20 KDMug/L 0.040Bromoform3<0.040
8260B P7C052011.0 4/1/17 1:20 KDMug/L 0.18Bromomethane10<0.18
8260B P7C052015.0 4/1/17 1:20 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.062Chlorobenzene3<0.062
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.22Chloroethane10<0.22
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.076Chloroform5<0.076
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.079Chloromethane1<0.079
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.065Dibromomethane10<0.065
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.061Ethylbenzene10.90
8260B P7C052011.0 4/1/17 1:20 KDMug/L 0.12m,p-Xylenes NE3.7
8260B P7C052015.0 4/1/17 1:20 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7C052015.0 4/1/17 1:20 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7C052015.0 4/1/17 1:20 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7C052015.0 4/1/17 1:20 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7C052011.0 4/1/17 1:20 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.044o-Xylene NE2.0
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.047Styrene1<0.047
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7C05201104/1/17 1:20 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.044Toluene1<0.044
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7C05201104/1/17 1:20 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7C052012.0 4/1/17 1:20 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7C052010.50 4/1/17 1:20 KDMug/L 0.097Vinyl chloride 1<0.097
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 15
Laboratory Report
04/17/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street
Project: Yancey-Mitchell Background
Well
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030457-01
Prism Work Order: 7030457
Time Collected: 03/28/17 12:47
Time Submitted: 03/30/17 11:25
MW-J
SWSL
8260B P7C052013.0 4/1/17 1:20 KDMug/L 0.15Xylenes, total 55.6
Surrogate Recovery Control Limits
80-124110 %4-Bromofluorobenzene
75-12999 %Dibromofluoromethane
77-123100 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 15
4/17/17
Level II QC Report
231 Haywood Street
Project: Yancey-Mitchell Background
Well
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030457
Time Submitted: 3/30/2017 11:25:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7C0520 - 5030B
Blank (P7C0520-BLK1)Prepared & Analyzed: 03/31/17
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL1.0
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
Acetone ug/LBRL5.0
Acrylonitrile ug/LBRL20
Benzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL1.0
Bromomethane ug/LBRL1.0
Carbon disulfide ug/LBRL5.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Ethylbenzene ug/LBRL0.50
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL5.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Iodide ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL5.0
Methylene Chloride ug/LBRL1.0
o-Xylene ug/LBRL0.50
Styrene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Tetrahydrofuran ug/LBRL10
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
trans-1,4-Dichloro-2-butene ug/LBRL10
Trichloroethylene ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 15
4/17/17
Level II QC Report
231 Haywood Street
Project: Yancey-Mitchell Background
Well
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030457
Time Submitted: 3/30/2017 11:25:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7C0520 - 5030B
Blank (P7C0520-BLK1)Prepared & Analyzed: 03/31/17
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL2.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL3.0
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 11456.8
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10250.9
ug/L 50.00 77-123Surrogate: Toluene-d8 10250.9
LCS (P7C0520-BS1)Prepared & Analyzed: 03/31/17
1,1,1,2-Tetrachloroethane ug/L20.1 0.50 20.00 79-134101
1,1,1-Trichloroethane ug/L20.7 0.50 20.00 75-136104
1,1,2,2-Tetrachloroethane ug/L21.3 0.50 20.00 62-127106
1,1,2-Trichloroethane ug/L20.7 0.50 20.00 70-140104
1,1-Dichloroethane ug/L20.5 0.50 20.00 78-130102
1,1-Dichloroethylene ug/L19.4 0.50 20.00 70-15497
1,2,3-Trichloropropane ug/L21.2 1.0 20.00 71-127106
1,2-Dibromo-3-chloropropane ug/L19.8 2.0 20.00 63-13499
1,2-Dibromoethane ug/L22.5 0.50 20.00 77-135112
1,2-Dichlorobenzene ug/L20.7 0.50 20.00 78-128104
1,2-Dichloroethane ug/L20.8 0.50 20.00 68-131104
1,2-Dichloropropane ug/L21.2 0.50 20.00 77-130106
1,4-Dichlorobenzene ug/L20.5 0.50 20.00 75-126102
Acetone ug/L33.7 5.0 40.00 40-16684
Acrylonitrile ug/L38.8 20 40.00 81-12797
Benzene ug/L20.6 0.50 20.00 77-128103
Bromochloromethane ug/L20.2 0.50 20.00 78-135101
Bromodichloromethane ug/L20.7 0.50 20.00 76-138103
Bromoform ug/L17.8 1.0 20.00 71-13589
Bromomethane ug/L15.4 1.0 20.00 41-16877
Carbon disulfide ug/L20.6 5.0 20.00 59-135103
Carbon Tetrachloride ug/L21.6 0.50 20.00 72-142108
Chlorobenzene ug/L20.6 0.50 20.00 78-119103
Chloroethane ug/L16.2 0.50 20.00 57-14281
Chloroform ug/L20.7 0.50 20.00 77-130104
Chloromethane ug/L18.2 0.50 20.00 47-14591
cis-1,2-Dichloroethylene ug/L20.9 0.50 20.00 76-141105
cis-1,3-Dichloropropylene ug/L20.5 0.50 20.00 65-140103
Dibromochloromethane ug/L20.4 0.50 20.00 75-134102
Dibromomethane ug/L20.5 0.50 20.00 76-138102
Ethylbenzene ug/L21.2 0.50 20.00 80-127106
m,p-Xylenes ug/L44.1 1.0 40.00 77-133110
Methyl Butyl Ketone (2-Hexanone)ug/L20.1 5.0 20.00 64-137101
Methyl Ethyl Ketone (2-Butanone)ug/L20.8 5.0 20.00 71-134104
Methyl Iodide ug/L16.5 5.0 20.00 70-13082
Methyl Isobutyl Ketone ug/L18.9 5.0 20.00 69-13494
Methylene Chloride ug/L19.4 1.0 20.00 73-13197
o-Xylene ug/L21.7 0.50 20.00 78-128108
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 15
4/17/17
Level II QC Report
231 Haywood Street
Project: Yancey-Mitchell Background
Well
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030457
Time Submitted: 3/30/2017 11:25:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7C0520 - 5030B
LCS (P7C0520-BS1)Prepared & Analyzed: 03/31/17
Styrene ug/L19.2 0.50 20.00 78-12996
Tetrachloroethylene ug/L21.2 0.50 20.00 80-129106
Tetrahydrofuran ug/L19.8 10 20.00 70-13099
Toluene ug/L20.3 0.50 20.00 76-131101
trans-1,2-Dichloroethylene ug/L21.9 0.50 20.00 76-135109
trans-1,3-Dichloropropylene ug/L20.3 0.50 20.00 67-140101
trans-1,4-Dichloro-2-butene ug/L19.0 10 20.00 70-13095
Trichloroethylene ug/L20.2 0.50 20.00 77-133101
Trichlorofluoromethane ug/L17.4 0.50 20.00 62-14887
Vinyl acetate ug/L21.2 2.0 20.00 34-167106
Vinyl chloride ug/L21.3 0.50 20.00 57-141106
Xylenes, total ug/L65.8 3.0 60.00 77-133110
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10954.7
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10351.6
ug/L 50.00 77-123Surrogate: Toluene-d8 10451.8
LCS Dup (P7C0520-BSD1)Prepared & Analyzed: 03/31/17
1,1,1,2-Tetrachloroethane ug/L20.2 0.50 20.00 2079-134101 0.5
1,1,1-Trichloroethane ug/L20.6 0.50 20.00 2075-136103 0.3
1,1,2,2-Tetrachloroethane ug/L21.8 0.50 20.00 2062-127109 3
1,1,2-Trichloroethane ug/L20.9 0.50 20.00 2070-140104 0.7
1,1-Dichloroethane ug/L20.2 0.50 20.00 2078-130101 1
1,1-Dichloroethylene ug/L19.2 0.50 20.00 2070-15496 1
1,2,3-Trichloropropane ug/L22.4 1.0 20.00 2071-127112 6
1,2-Dibromo-3-chloropropane ug/L20.3 2.0 20.00 2063-134102 2
1,2-Dibromoethane ug/L22.3 0.50 20.00 2077-135111 0.9
1,2-Dichlorobenzene ug/L21.4 0.50 20.00 2078-128107 3
1,2-Dichloroethane ug/L20.9 0.50 20.00 2068-131105 0.4
1,2-Dichloropropane ug/L21.2 0.50 20.00 2077-130106 0.2
1,4-Dichlorobenzene ug/L20.7 0.50 20.00 2075-126104 1
Acetone ug/L35.3 5.0 40.00 2040-16688 5
Acrylonitrile ug/L40.8 20 40.00 2081-127102 5
Benzene ug/L20.4 0.50 20.00 2077-128102 0.9
Bromochloromethane ug/L20.7 0.50 20.00 2078-135104 2
Bromodichloromethane ug/L20.9 0.50 20.00 2076-138104 0.9
Bromoform ug/L18.2 1.0 20.00 2071-13591 2
Bromomethane ug/L15.7 1.0 20.00 2041-16879 2
Carbon disulfide ug/L20.3 5.0 20.00 2059-135102 1
Carbon Tetrachloride ug/L21.2 0.50 20.00 2072-142106 2
Chlorobenzene ug/L20.7 0.50 20.00 2078-119103 0.3
Chloroethane ug/L16.5 0.50 20.00 2057-14282 2
Chloroform ug/L20.7 0.50 20.00 2077-130104 0.05
Chloromethane ug/L17.6 0.50 20.00 2047-14588 3
cis-1,2-Dichloroethylene ug/L20.8 0.50 20.00 2076-141104 0.4
cis-1,3-Dichloropropylene ug/L20.7 0.50 20.00 2065-140103 0.6
Dibromochloromethane ug/L20.5 0.50 20.00 2075-134102 0.3
Dibromomethane ug/L21.2 0.50 20.00 2076-138106 3
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 15
4/17/17
Level II QC Report
231 Haywood Street
Project: Yancey-Mitchell Background
Well
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030457
Time Submitted: 3/30/2017 11:25:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7C0520 - 5030B
LCS Dup (P7C0520-BSD1)Prepared & Analyzed: 03/31/17
Ethylbenzene ug/L21.4 0.50 20.00 2080-127107 0.7
m,p-Xylenes ug/L44.1 1.0 40.00 2077-133110 0.05
Methyl Butyl Ketone (2-Hexanone)ug/L20.7 5.0 20.00 2064-137104 3
Methyl Ethyl Ketone (2-Butanone)ug/L22.3 5.0 20.00 2071-134111 7
Methyl Iodide ug/L18.6 5.0 20.00 2070-13093 12
Methyl Isobutyl Ketone ug/L19.6 5.0 20.00 2069-13498 4
Methylene Chloride ug/L19.4 1.0 20.00 2073-13197 0.05
o-Xylene ug/L21.8 0.50 20.00 2078-128109 0.6
Styrene ug/L19.2 0.50 20.00 2078-12996 0.1
Tetrachloroethylene ug/L21.2 0.50 20.00 2080-129106 0.2
Tetrahydrofuran ug/L20.7 10 20.00 2070-130103 4
Toluene ug/L20.4 0.50 20.00 2076-131102 0.6
trans-1,2-Dichloroethylene ug/L21.7 0.50 20.00 2076-135108 1
trans-1,3-Dichloropropylene ug/L20.5 0.50 20.00 2067-140102 1
trans-1,4-Dichloro-2-butene ug/L20.0 10 20.00 2070-130100 5
Trichloroethylene ug/L19.9 0.50 20.00 2077-13399 1
Trichlorofluoromethane ug/L17.3 0.50 20.00 2062-14886 0.8
Vinyl acetate ug/L21.7 2.0 20.00 2034-167108 2
Vinyl chloride ug/L21.5 0.50 20.00 2057-141108 1
Xylenes, total ug/L65.9 3.0 60.00 2077-133110 0.2
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 11155.3
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10150.4
ug/L 50.00 77-123Surrogate: Toluene-d8 10451.9
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 15
4/17/17
Level II QC Report
231 Haywood Street
Project: Yancey-Mitchell Background
Well
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030457
Time Submitted: 3/30/2017 11:25:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P7D0046 - 3005A
Blank (P7D0046-BLK1)Prepared & Analyzed: 04/05/17
Antimony ug/LBRL1.0
Arsenic ug/LBRL1.0
Barium ug/LBRL5.0
Beryllium ug/LBRL1.0
Cadmium ug/LBRL1.0
Chromium ug/L0.593 1.0 A, J
Cobalt ug/LBRL1.0
Copper ug/LBRL5.0
Iron ug/LBRL100
Lead ug/LBRL1.0
Manganese ug/L0.831 5.0 J
Nickel ug/L0.395 2.0 J
Selenium ug/LBRL5.0
Silver ug/L0.113 5.0 J
Thallium ug/L0.177 1.0 J
Vanadium ug/LBRL1.0
Zinc ug/L1.93 10 J
LCS (P7D0046-BS1)Prepared & Analyzed: 04/05/17
Antimony ug/L91.2 1.0 100.0 80-12091
Arsenic ug/L96.0 1.0 100.0 80-12096
Barium ug/L93.6 5.0 100.0 80-12094
Beryllium ug/L95.4 1.0 100.0 80-12095
Cadmium ug/L1021.0 100.0 80-120102
Chromium ug/L92.2 1.0 100.0 B80-12092
Cobalt ug/L1061.0 100.0 80-120106
Copper ug/L1045.0 100.0 80-120104
Iron ug/L977 100 1000 80-12098
Lead ug/L1061.0 100.0 80-120106
Manganese ug/L1025.0 100.0 80-120102
Nickel ug/L1012.0 100.0 80-120101
Selenium ug/L88.3 5.0 100.0 80-12088
Silver ug/L1155.0 100.0 80-120115
Thallium ug/L94.3 1.0 100.0 80-12094
Vanadium ug/L86.7 1.0 100.0 80-12087
Zinc ug/L99.0 10 100.0 80-12099
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 15
4/17/17
Level II QC Report
231 Haywood Street
Project: Yancey-Mitchell Background
Well
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030457
Time Submitted: 3/30/2017 11:25:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P7D0202 - 7470A
Blank (P7D0202-BLK1)Prepared & Analyzed: 04/13/17
Mercury ug/LBRL0.20
LCS (P7D0202-BS1)Prepared & Analyzed: 04/13/17
Mercury ug/L9.41 0.20 9.375 80-120100
Matrix Spike (P7D0202-MS1)Prepared & Analyzed: 04/13/17 Source: 7030457-01
Mercury ug/L9.49 0.20 9.375 BRL 80-120101
Matrix Spike Dup (P7D0202-MSD1)Prepared & Analyzed: 04/13/17 Source: 7030457-01
Mercury ug/L9.29 0.20 9.375 BRL 2080-12099 2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 15
4/17/17
Level II QC Report
231 Haywood Street
Project: Yancey-Mitchell Background
Well
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030457
Time Submitted: 3/30/2017 11:25:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Anions by Ion Chromatography - Quality Control
Batch P7D0014 - NO PREP
Blank (P7D0014-BLK1)Prepared & Analyzed: 03/30/17
Chloride ug/LBRL1000
Sulfate ug/LBRL1000
LCS (P7D0014-BS1)Prepared & Analyzed: 03/30/17
Chloride ug/L397001000 40000 80-12099
Sulfate ug/L387001000 40000 80-12097
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 15
4/17/17
Level II QC Report
231 Haywood Street
Project: Yancey-Mitchell Background
Well
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030457
Time Submitted: 3/30/2017 11:25:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P7C0513 - NO PREP
Blank (P7C0513-BLK1)Prepared & Analyzed: 03/31/17
Total Alkalinity to pH 4.5 ug/LBRL5000
LCS (P7C0513-BS1)Prepared & Analyzed: 03/31/17
Total Alkalinity to pH 4.5 ug/L2540005000 250000 90-110102
Batch P7D0024 - NO PREP
Blank (P7D0024-BLK1)Prepared & Analyzed: 04/03/17
Total Dissolved Solids ug/LBRL50000
LCS (P7D0024-BS1)Prepared & Analyzed: 04/03/17
Total Dissolved Solids ug/L98800050000 1000000 90-11099
Sample Extraction Data
Prep Method: 3005A
Lab Number Batch Date/TimeInitialFinal
P7D00467030457-01 04/05/17 7:3550 50mL mL
P7D00467030457-01 04/05/17 7:3550 50mL mL
Prep Method: 7470A
Lab Number Batch Date/TimeInitialFinal
P7D02027030457-01 04/13/17 8:2020 30mL mL
Prep Method: 5030B
Lab Number Batch Date/TimeInitialFinal
P7C05207030457-01 03/31/17 16:1010 10mL mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Page 15 of 15
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
04/18/2017
Anchor QEA of North Carolina, PLLC
Brian Gant
231 Haywood Street
Asheville, NC 28801
Project: Yancey-Mitchell Surface Water Wells
Lab Submittal Date: 03/30/2017
Prism Work Order: 7030458
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
President/Project Manager
Reviewed ByRobbi A. Jones Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
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Sample Receipt Summary
04/18/2017
Prism Work Order: 7030458
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
7030458-01 03/28/17SW-1 03/30/17Water
7030458-02 03/28/17SW-2 03/30/17Water
7030458-03 03/28/17Trip Blank (SW)03/30/17Water
Samples were received in good condition at 2.1 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 7030458
04/18/2017
Summary of Detections
7200 ug/L7030458-01 SW-1 Chloride 9056A
11000 ug/L7030458-01 SW-1 Sulfate 9056A
13000 ug/L7030458-01 SW-1 Total Alkalinity to pH 4.5 SM2320 B
52000 ug/L7030458-01 SW-1 Total Dissolved Solids SM2540 C
18 ug/L7030458-01 SW-1 Barium 6020B
0.42 J ug/L7030458-01 SW-1 Chromium 6020B
0.10 J ug/L7030458-01 SW-1 Cobalt 6020B
0.93 J ug/L7030458-01 SW-1 Copper 6020B
240 ug/L7030458-01 SW-1 Iron 6020B
0.14 J ug/L7030458-01 SW-1 Lead 6020B
31 ug/L7030458-01 SW-1 Manganese 6020B
0.25 J ug/L7030458-01 SW-1 Nickel 6020B
0.34 J ug/L7030458-01 SW-1 Thallium 6020B
2.6 J ug/L7030458-01 SW-1 Zinc 6020B
7200 ug/L7030458-02 SW-2 Chloride 9056A
7300 ug/L7030458-02 SW-2 Sulfate 9056A
11000 ug/L7030458-02 SW-2 Total Alkalinity to pH 4.5 SM2320 B
44000 J ug/L7030458-02 SW-2 Total Dissolved Solids SM2540 C
16 ug/L7030458-02 SW-2 Barium 6020B
0.48 J ug/L7030458-02 SW-2 Chromium 6020B
0.12 J ug/L7030458-02 SW-2 Cobalt 6020B
1.1 J ug/L7030458-02 SW-2 Copper 6020B
250 ug/L7030458-02 SW-2 Iron 6020B
0.15 J ug/L7030458-02 SW-2 Lead 6020B
25 ug/L7030458-02 SW-2 Manganese 6020B
0.34 J ug/L7030458-02 SW-2 Nickel 6020B
0.23 J ug/L7030458-02 SW-2 Thallium 6020B
5.1 J ug/L7030458-02 SW-2 Zinc 6020B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 20
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street
Project: Yancey-Mitchell Surface
Water Wells
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030458-01
Prism Work Order: 7030458
Time Collected: 03/28/17 15:10
Time Submitted: 03/30/17 11:25
SW-1
SWSL
Anions by Ion Chromatography
9056A P7D0014110003/30/17 14:03 EGCug/L 44ChlorideNE7200
9056A P7D0014110003/30/17 14:03 EGCug/L 320Sulfate25000011000
General Chemistry Parameters
SM2320 B P7C0513150003/31/17 10:30 EGCug/L 770Total Alkalinity to pH 4.5 NE13000
SM2540 C P7D00241500004/3/17 14:46 SLSug/L 1400Total Dissolved Solids NE52000
Total Metals
7470A P7D020210.20 4/13/17 13:12 JABug/L 0.030Mercury0.2<0.030
6020B P7D006311.0 4/10/17 17:12 BGMug/L 0.41Antimony6<0.41
6020B P7D006311.0 4/10/17 17:12 BGMug/L 0.45Arsenic10<0.45
6020B P7D006315.0 4/10/17 17:12 BGMug/L 0.12Barium10018
6020B P7D006311.0 4/10/17 17:12 BGMug/L 0.068Beryllium1<0.068
6020B P7D006311.0 4/10/17 17:12 BGMug/L 0.053Cadmium1<0.053
6020B P7D006311.0 4/10/17 17:12 BGMJug/L 0.32Chromium100.42
6020B P7D006311.0 4/10/17 17:12 BGMJug/L 0.056Cobalt100.10
6020B P7D006315.0 4/10/17 17:12 BGMJug/L 0.41Copper100.93
6020B P7D006311004/10/17 17:12 bgmug/L 20Iron300240
6020B P7D006311.0 4/10/17 17:12 BGMJug/L 0.061Lead100.14
6020B P7D006315.0 4/10/17 17:12 bgmug/L 0.76Manganese5031
6020B P7D006312.0 4/10/17 17:12 BGMJug/L 0.082Nickel500.25
6020B P7D006315.0 4/10/17 17:12 BGMug/L 0.45Selenium10<0.45
6020B P7D006315.0 4/10/17 17:12 BGMug/L 0.067Silver10<0.067
6020B P7D006311.0 4/10/17 17:12 BGMJug/L 0.018Thallium5.50.34
6020B P7D006311.0 4/10/17 17:12 BGMug/L 0.79Vanadium25<0.79
6020B P7D00631104/10/17 17:12 BGMJug/L 1.3Zinc102.6
Volatile Organic Compounds by GC/MS
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7C052011.0 4/1/17 1:46 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7C052012.0 4/1/17 1:46 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.0661,2-Dichloroethane 1<0.066
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 20
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street
Project: Yancey-Mitchell Surface
Water Wells
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030458-01
Prism Work Order: 7030458
Time Collected: 03/28/17 15:10
Time Submitted: 03/30/17 11:25
SW-1
SWSL
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7C052015.0 4/1/17 1:46 KDMug/L 0.31Acetone100<0.31
8260B P7C05201204/1/17 1:46 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.048Benzene1<0.048
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7C052011.0 4/1/17 1:46 KDMug/L 0.040Bromoform3<0.040
8260B P7C052011.0 4/1/17 1:46 KDMug/L 0.18Bromomethane10<0.18
8260B P7C052015.0 4/1/17 1:46 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.062Chlorobenzene3<0.062
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.22Chloroethane10<0.22
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.076Chloroform5<0.076
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.079Chloromethane1<0.079
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.065Dibromomethane10<0.065
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7C052011.0 4/1/17 1:46 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7C052015.0 4/1/17 1:46 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7C052015.0 4/1/17 1:46 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7C052015.0 4/1/17 1:46 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7C052015.0 4/1/17 1:46 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7C052011.0 4/1/17 1:46 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.044o-Xylene NE<0.044
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.047Styrene1<0.047
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7C05201104/1/17 1:46 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.044Toluene1<0.044
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7C05201104/1/17 1:46 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7C052012.0 4/1/17 1:46 KDMug/L 0.060Vinyl acetate 50<0.060
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 20
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street
Project: Yancey-Mitchell Surface
Water Wells
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030458-01
Prism Work Order: 7030458
Time Collected: 03/28/17 15:10
Time Submitted: 03/30/17 11:25
SW-1
SWSL
8260B P7C052010.50 4/1/17 1:46 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7C052013.0 4/1/17 1:46 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124114 %4-Bromofluorobenzene
75-129102 %Dibromofluoromethane
77-123103 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 20
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street
Project: Yancey-Mitchell Surface
Water Wells
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030458-02
Prism Work Order: 7030458
Time Collected: 03/28/17 15:35
Time Submitted: 03/30/17 11:25
SW-2
SWSL
Anions by Ion Chromatography
9056A P7D0014110003/30/17 14:19 EGCug/L 44ChlorideNE7200
9056A P7D0014110003/30/17 14:19 EGCug/L 320Sulfate2500007300
General Chemistry Parameters
SM2320 B P7C0513150003/31/17 10:30 EGCug/L 770Total Alkalinity to pH 4.5 NE11000
SM2540 C P7D00241500004/3/17 14:46 SLSJug/L 1400Total Dissolved Solids NE44000
Total Metals
7470A P7D020210.20 4/13/17 13:16 JABug/L 0.030Mercury0.2<0.030
6020B P7D006311.0 4/10/17 17:17 BGMug/L 0.41Antimony6<0.41
6020B P7D006311.0 4/10/17 17:17 BGMug/L 0.45Arsenic10<0.45
6020B P7D006315.0 4/10/17 17:17 BGMug/L 0.12Barium10016
6020B P7D006311.0 4/10/17 17:17 BGMug/L 0.068Beryllium1<0.068
6020B P7D006311.0 4/10/17 17:17 BGMug/L 0.053Cadmium1<0.053
6020B P7D006311.0 4/10/17 17:17 BGMJug/L 0.32Chromium100.48
6020B P7D006311.0 4/10/17 17:17 BGMJug/L 0.056Cobalt100.12
6020B P7D006315.0 4/10/17 17:17 BGMJug/L 0.41Copper101.1
6020B P7D006311004/10/17 17:17 bgmug/L 20Iron300250
6020B P7D006311.0 4/10/17 17:17 BGMJug/L 0.061Lead100.15
6020B P7D006315.0 4/10/17 17:17 bgmug/L 0.76Manganese5025
6020B P7D006312.0 4/10/17 17:17 BGMJug/L 0.082Nickel500.34
6020B P7D006315.0 4/10/17 17:17 BGMug/L 0.45Selenium10<0.45
6020B P7D006315.0 4/10/17 17:17 BGMug/L 0.067Silver10<0.067
6020B P7D006311.0 4/10/17 17:17 BGMJug/L 0.018Thallium5.50.23
6020B P7D006311.0 4/10/17 17:17 BGMug/L 0.79Vanadium25<0.79
6020B P7D00631104/10/17 17:17 BGMJug/L 1.3Zinc105.1
Volatile Organic Compounds by GC/MS
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7C052011.0 4/1/17 2:11 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7C052012.0 4/1/17 2:11 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.111,2-Dichloropropane 1<0.11
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 20
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street
Project: Yancey-Mitchell Surface
Water Wells
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030458-02
Prism Work Order: 7030458
Time Collected: 03/28/17 15:35
Time Submitted: 03/30/17 11:25
SW-2
SWSL
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7C052015.0 4/1/17 2:11 KDMug/L 0.31Acetone100<0.31
8260B P7C05201204/1/17 2:11 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.048Benzene1<0.048
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7C052011.0 4/1/17 2:11 KDMug/L 0.040Bromoform3<0.040
8260B P7C052011.0 4/1/17 2:11 KDMug/L 0.18Bromomethane10<0.18
8260B P7C052015.0 4/1/17 2:11 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.062Chlorobenzene3<0.062
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.22Chloroethane10<0.22
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.076Chloroform5<0.076
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.079Chloromethane1<0.079
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.065Dibromomethane10<0.065
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7C052011.0 4/1/17 2:11 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7C052015.0 4/1/17 2:11 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7C052015.0 4/1/17 2:11 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7C052015.0 4/1/17 2:11 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7C052015.0 4/1/17 2:11 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
8260B P7C052011.0 4/1/17 2:11 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.044o-Xylene NE<0.044
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.047Styrene1<0.047
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7C05201104/1/17 2:11 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.044Toluene1<0.044
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7C05201104/1/17 2:11 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7C052012.0 4/1/17 2:11 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7C052010.50 4/1/17 2:11 KDMug/L 0.097Vinyl chloride 1<0.097
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 20
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street
Project: Yancey-Mitchell Surface
Water Wells
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030458-02
Prism Work Order: 7030458
Time Collected: 03/28/17 15:35
Time Submitted: 03/30/17 11:25
SW-2
SWSL
8260B P7C052013.0 4/1/17 2:11 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124112 %4-Bromofluorobenzene
75-129102 %Dibromofluoromethane
77-123103 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 20
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street
Project: Yancey-Mitchell Surface
Water Wells
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030458-03
Prism Work Order: 7030458
Time Collected: 03/28/17 00:00
Time Submitted: 03/30/17 11:25
Trip Blank (SW)
SWSL
Volatile Organic Compounds by GC/MS
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.111,1,1,2-Tetrachloroethane 5<0.11
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.0611,1,1-Trichloroethane 1<0.061
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.0361,1,2,2-Tetrachloroethane 3<0.036
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.0661,1,2-Trichloroethane 1<0.066
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.0831,1-Dichloroethane 5<0.083
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.0831,1-Dichloroethylene 5<0.083
8260B P7C052011.0 3/31/17 21:00 KDMug/L 0.141,2,3-Trichloropropane 1<0.14
8260B P7C052012.0 3/31/17 21:00 KDMug/L 0.171,2-Dibromo-3-chloropropane 13<0.17
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.0511,2-Dibromoethane 1<0.051
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.0761,2-Dichlorobenzene 5<0.076
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.0661,2-Dichloroethane 1<0.066
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.111,2-Dichloropropane 1<0.11
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.0501,4-Dichlorobenzene 1<0.050
8260B P7C052015.0 3/31/17 21:00 KDMug/L 0.31Acetone100<0.31
8260B P7C05201203/31/17 21:00 KDMug/L 0.20Acrylonitrile200<0.20
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.048Benzene1<0.048
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.14Bromochloromethane3<0.14
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.062Bromodichloromethane1<0.062
8260B P7C052011.0 3/31/17 21:00 KDMug/L 0.040Bromoform3<0.040
8260B P7C052011.0 3/31/17 21:00 KDMug/L 0.18Bromomethane10<0.18
8260B P7C052015.0 3/31/17 21:00 KDMug/L 0.075Carbon disulfide 100<0.075
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.11Carbon Tetrachloride 1<0.11
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.062Chlorobenzene3<0.062
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.22Chloroethane10<0.22
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.076Chloroform5<0.076
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.079Chloromethane1<0.079
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.056cis-1,2-Dichloroethylene 5<0.056
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.079cis-1,3-Dichloropropylene 1<0.079
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.081Dibromochloromethane3<0.081
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.065Dibromomethane10<0.065
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.061Ethylbenzene1<0.061
8260B P7C052011.0 3/31/17 21:00 KDMug/L 0.12m,p-Xylenes NE<0.12
8260B P7C052015.0 3/31/17 21:00 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)50<0.065
8260B P7C052015.0 3/31/17 21:00 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)100<0.24
8260B P7C052015.0 3/31/17 21:00 KDMug/L 0.33Methyl Iodide 10<0.33
8260B P7C052015.0 3/31/17 21:00 KDMug/L 0.078Methyl Isobutyl Ketone 100<0.078
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 20
Laboratory Report
04/18/2017
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
FactorUnitsMDL Analyst
231 Haywood Street
Project: Yancey-Mitchell Surface
Water Wells
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 7030458-03
Prism Work Order: 7030458
Time Collected: 03/28/17 00:00
Time Submitted: 03/30/17 11:25
Trip Blank (SW)
SWSL
8260B P7C052011.0 3/31/17 21:00 KDMug/L 0.083Methylene Chloride 1<0.083
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.044o-Xylene NE<0.044
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.047Styrene1<0.047
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.098Tetrachloroethylene1<0.098
8260B P7C05201103/31/17 21:00 KDMug/L 0.16TetrahydrofuranNE<0.16
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.044Toluene1<0.044
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.094trans-1,2-Dichloroethylene 5<0.094
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.070trans-1,3-Dichloropropylene 1<0.070
8260B P7C05201103/31/17 21:00 KDMug/L 0.12trans-1,4-Dichloro-2-butene 100<0.12
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.078Trichloroethylene1<0.078
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.062Trichlorofluoromethane1<0.062
8260B P7C052012.0 3/31/17 21:00 KDMug/L 0.060Vinyl acetate 50<0.060
8260B P7C052010.50 3/31/17 21:00 KDMug/L 0.097Vinyl chloride 1<0.097
8260B P7C052013.0 3/31/17 21:00 KDMug/L 0.15Xylenes, total 5<0.15
Surrogate Recovery Control Limits
80-124113 %4-Bromofluorobenzene
75-129103 %Dibromofluoromethane
77-123103 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 20
4/18/17
Level II QC Report
231 Haywood Street
Project: Yancey-Mitchell Surface Water
Wells
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030458
Time Submitted: 3/30/2017 11:25:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7C0520 - 5030B
Blank (P7C0520-BLK1)Prepared & Analyzed: 03/31/17
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL1.0
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
Acetone ug/LBRL5.0
Acrylonitrile ug/LBRL20
Benzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL1.0
Bromomethane ug/LBRL1.0
Carbon disulfide ug/LBRL5.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Ethylbenzene ug/LBRL0.50
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL5.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Iodide ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL5.0
Methylene Chloride ug/LBRL1.0
o-Xylene ug/LBRL0.50
Styrene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Tetrahydrofuran ug/LBRL10
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
trans-1,4-Dichloro-2-butene ug/LBRL10
Trichloroethylene ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 20
4/18/17
Level II QC Report
231 Haywood Street
Project: Yancey-Mitchell Surface Water
Wells
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030458
Time Submitted: 3/30/2017 11:25:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7C0520 - 5030B
Blank (P7C0520-BLK1)Prepared & Analyzed: 03/31/17
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL2.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL3.0
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 11456.8
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10250.9
ug/L 50.00 77-123Surrogate: Toluene-d8 10250.9
LCS (P7C0520-BS1)Prepared & Analyzed: 03/31/17
1,1,1,2-Tetrachloroethane ug/L20.1 0.50 20.00 79-134101
1,1,1-Trichloroethane ug/L20.7 0.50 20.00 75-136104
1,1,2,2-Tetrachloroethane ug/L21.3 0.50 20.00 62-127106
1,1,2-Trichloroethane ug/L20.7 0.50 20.00 70-140104
1,1-Dichloroethane ug/L20.5 0.50 20.00 78-130102
1,1-Dichloroethylene ug/L19.4 0.50 20.00 70-15497
1,2,3-Trichloropropane ug/L21.2 1.0 20.00 71-127106
1,2-Dibromo-3-chloropropane ug/L19.8 2.0 20.00 63-13499
1,2-Dibromoethane ug/L22.5 0.50 20.00 77-135112
1,2-Dichlorobenzene ug/L20.7 0.50 20.00 78-128104
1,2-Dichloroethane ug/L20.8 0.50 20.00 68-131104
1,2-Dichloropropane ug/L21.2 0.50 20.00 77-130106
1,4-Dichlorobenzene ug/L20.5 0.50 20.00 75-126102
Acetone ug/L33.7 5.0 40.00 40-16684
Acrylonitrile ug/L38.8 20 40.00 81-12797
Benzene ug/L20.6 0.50 20.00 77-128103
Bromochloromethane ug/L20.2 0.50 20.00 78-135101
Bromodichloromethane ug/L20.7 0.50 20.00 76-138103
Bromoform ug/L17.8 1.0 20.00 71-13589
Bromomethane ug/L15.4 1.0 20.00 41-16877
Carbon disulfide ug/L20.6 5.0 20.00 59-135103
Carbon Tetrachloride ug/L21.6 0.50 20.00 72-142108
Chlorobenzene ug/L20.6 0.50 20.00 78-119103
Chloroethane ug/L16.2 0.50 20.00 57-14281
Chloroform ug/L20.7 0.50 20.00 77-130104
Chloromethane ug/L18.2 0.50 20.00 47-14591
cis-1,2-Dichloroethylene ug/L20.9 0.50 20.00 76-141105
cis-1,3-Dichloropropylene ug/L20.5 0.50 20.00 65-140103
Dibromochloromethane ug/L20.4 0.50 20.00 75-134102
Dibromomethane ug/L20.5 0.50 20.00 76-138102
Ethylbenzene ug/L21.2 0.50 20.00 80-127106
m,p-Xylenes ug/L44.1 1.0 40.00 77-133110
Methyl Butyl Ketone (2-Hexanone)ug/L20.1 5.0 20.00 64-137101
Methyl Ethyl Ketone (2-Butanone)ug/L20.8 5.0 20.00 71-134104
Methyl Iodide ug/L16.5 5.0 20.00 70-13082
Methyl Isobutyl Ketone ug/L18.9 5.0 20.00 69-13494
Methylene Chloride ug/L19.4 1.0 20.00 73-13197
o-Xylene ug/L21.7 0.50 20.00 78-128108
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 20
4/18/17
Level II QC Report
231 Haywood Street
Project: Yancey-Mitchell Surface Water
Wells
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030458
Time Submitted: 3/30/2017 11:25:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7C0520 - 5030B
LCS (P7C0520-BS1)Prepared & Analyzed: 03/31/17
Styrene ug/L19.2 0.50 20.00 78-12996
Tetrachloroethylene ug/L21.2 0.50 20.00 80-129106
Tetrahydrofuran ug/L19.8 10 20.00 70-13099
Toluene ug/L20.3 0.50 20.00 76-131101
trans-1,2-Dichloroethylene ug/L21.9 0.50 20.00 76-135109
trans-1,3-Dichloropropylene ug/L20.3 0.50 20.00 67-140101
trans-1,4-Dichloro-2-butene ug/L19.0 10 20.00 70-13095
Trichloroethylene ug/L20.2 0.50 20.00 77-133101
Trichlorofluoromethane ug/L17.4 0.50 20.00 62-14887
Vinyl acetate ug/L21.2 2.0 20.00 34-167106
Vinyl chloride ug/L21.3 0.50 20.00 57-141106
Xylenes, total ug/L65.8 3.0 60.00 77-133110
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10954.7
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10351.6
ug/L 50.00 77-123Surrogate: Toluene-d8 10451.8
LCS Dup (P7C0520-BSD1)Prepared & Analyzed: 03/31/17
1,1,1,2-Tetrachloroethane ug/L20.2 0.50 20.00 2079-134101 0.5
1,1,1-Trichloroethane ug/L20.6 0.50 20.00 2075-136103 0.3
1,1,2,2-Tetrachloroethane ug/L21.8 0.50 20.00 2062-127109 3
1,1,2-Trichloroethane ug/L20.9 0.50 20.00 2070-140104 0.7
1,1-Dichloroethane ug/L20.2 0.50 20.00 2078-130101 1
1,1-Dichloroethylene ug/L19.2 0.50 20.00 2070-15496 1
1,2,3-Trichloropropane ug/L22.4 1.0 20.00 2071-127112 6
1,2-Dibromo-3-chloropropane ug/L20.3 2.0 20.00 2063-134102 2
1,2-Dibromoethane ug/L22.3 0.50 20.00 2077-135111 0.9
1,2-Dichlorobenzene ug/L21.4 0.50 20.00 2078-128107 3
1,2-Dichloroethane ug/L20.9 0.50 20.00 2068-131105 0.4
1,2-Dichloropropane ug/L21.2 0.50 20.00 2077-130106 0.2
1,4-Dichlorobenzene ug/L20.7 0.50 20.00 2075-126104 1
Acetone ug/L35.3 5.0 40.00 2040-16688 5
Acrylonitrile ug/L40.8 20 40.00 2081-127102 5
Benzene ug/L20.4 0.50 20.00 2077-128102 0.9
Bromochloromethane ug/L20.7 0.50 20.00 2078-135104 2
Bromodichloromethane ug/L20.9 0.50 20.00 2076-138104 0.9
Bromoform ug/L18.2 1.0 20.00 2071-13591 2
Bromomethane ug/L15.7 1.0 20.00 2041-16879 2
Carbon disulfide ug/L20.3 5.0 20.00 2059-135102 1
Carbon Tetrachloride ug/L21.2 0.50 20.00 2072-142106 2
Chlorobenzene ug/L20.7 0.50 20.00 2078-119103 0.3
Chloroethane ug/L16.5 0.50 20.00 2057-14282 2
Chloroform ug/L20.7 0.50 20.00 2077-130104 0.05
Chloromethane ug/L17.6 0.50 20.00 2047-14588 3
cis-1,2-Dichloroethylene ug/L20.8 0.50 20.00 2076-141104 0.4
cis-1,3-Dichloropropylene ug/L20.7 0.50 20.00 2065-140103 0.6
Dibromochloromethane ug/L20.5 0.50 20.00 2075-134102 0.3
Dibromomethane ug/L21.2 0.50 20.00 2076-138106 3
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 20
4/18/17
Level II QC Report
231 Haywood Street
Project: Yancey-Mitchell Surface Water
Wells
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030458
Time Submitted: 3/30/2017 11:25:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P7C0520 - 5030B
LCS Dup (P7C0520-BSD1)Prepared & Analyzed: 03/31/17
Ethylbenzene ug/L21.4 0.50 20.00 2080-127107 0.7
m,p-Xylenes ug/L44.1 1.0 40.00 2077-133110 0.05
Methyl Butyl Ketone (2-Hexanone)ug/L20.7 5.0 20.00 2064-137104 3
Methyl Ethyl Ketone (2-Butanone)ug/L22.3 5.0 20.00 2071-134111 7
Methyl Iodide ug/L18.6 5.0 20.00 2070-13093 12
Methyl Isobutyl Ketone ug/L19.6 5.0 20.00 2069-13498 4
Methylene Chloride ug/L19.4 1.0 20.00 2073-13197 0.05
o-Xylene ug/L21.8 0.50 20.00 2078-128109 0.6
Styrene ug/L19.2 0.50 20.00 2078-12996 0.1
Tetrachloroethylene ug/L21.2 0.50 20.00 2080-129106 0.2
Tetrahydrofuran ug/L20.7 10 20.00 2070-130103 4
Toluene ug/L20.4 0.50 20.00 2076-131102 0.6
trans-1,2-Dichloroethylene ug/L21.7 0.50 20.00 2076-135108 1
trans-1,3-Dichloropropylene ug/L20.5 0.50 20.00 2067-140102 1
trans-1,4-Dichloro-2-butene ug/L20.0 10 20.00 2070-130100 5
Trichloroethylene ug/L19.9 0.50 20.00 2077-13399 1
Trichlorofluoromethane ug/L17.3 0.50 20.00 2062-14886 0.8
Vinyl acetate ug/L21.7 2.0 20.00 2034-167108 2
Vinyl chloride ug/L21.5 0.50 20.00 2057-141108 1
Xylenes, total ug/L65.9 3.0 60.00 2077-133110 0.2
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 11155.3
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10150.4
ug/L 50.00 77-123Surrogate: Toluene-d8 10451.9
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 20
4/18/17
Level II QC Report
231 Haywood Street
Project: Yancey-Mitchell Surface Water
Wells
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030458
Time Submitted: 3/30/2017 11:25:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P7D0063 - 3005A
Blank (P7D0063-BLK1)Prepared: 04/06/17 Analyzed: 04/10/17
Antimony ug/LBRL1.0
Arsenic ug/LBRL1.0
Barium ug/L0.467 5.0 J
Beryllium ug/LBRL1.0
Cadmium ug/LBRL1.0
Chromium ug/LBRL1.0
Cobalt ug/LBRL1.0
Copper ug/LBRL5.0
Iron ug/LBRL100
Lead ug/L0.110 1.0 J
Manganese ug/LBRL5.0
Nickel ug/LBRL2.0
Selenium ug/LBRL5.0
Silver ug/L0.139 5.0 J
Thallium ug/L0.242 1.0 J
Vanadium ug/LBRL1.0
Zinc ug/L1.68 10 J
LCS (P7D0063-BS1)Prepared: 04/06/17 Analyzed: 04/10/17
Antimony ug/L1051.0 100.0 80-120105
Arsenic ug/L1051.0 100.0 80-120105
Barium ug/L1065.0 100.0 80-120106
Beryllium ug/L1041.0 100.0 80-120104
Cadmium ug/L1061.0 100.0 80-120106
Chromium ug/L1011.0 100.0 80-120101
Cobalt ug/L1091.0 100.0 80-120109
Copper ug/L1105.0 100.0 80-120110
Iron ug/L1100 100 1000 80-120110
Lead ug/L1071.0 100.0 80-120107
Manganese ug/L1025.0 100.0 80-120102
Nickel ug/L1072.0 100.0 80-120107
Selenium ug/L1015.0 100.0 80-120101
Silver ug/L1155.0 100.0 80-120115
Thallium ug/L95.0 1.0 100.0 80-12095
Vanadium ug/L99.3 1.0 100.0 80-12099
Zinc ug/L10710 100.0 80-120107
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 20
4/18/17
Level II QC Report
231 Haywood Street
Project: Yancey-Mitchell Surface Water
Wells
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030458
Time Submitted: 3/30/2017 11:25:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P7D0202 - 7470A
Blank (P7D0202-BLK1)Prepared & Analyzed: 04/13/17
Mercury ug/LBRL0.20
LCS (P7D0202-BS1)Prepared & Analyzed: 04/13/17
Mercury ug/L9.41 0.20 9.375 80-120100
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 20
4/18/17
Level II QC Report
231 Haywood Street
Project: Yancey-Mitchell Surface Water
Wells
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030458
Time Submitted: 3/30/2017 11:25:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Anions by Ion Chromatography - Quality Control
Batch P7D0014 - NO PREP
Blank (P7D0014-BLK1)Prepared & Analyzed: 03/30/17
Chloride ug/LBRL1000
Sulfate ug/LBRL1000
LCS (P7D0014-BS1)Prepared & Analyzed: 03/30/17
Chloride ug/L397001000 40000 80-12099
Sulfate ug/L387001000 40000 80-12097
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 20
4/18/17
Level II QC Report
231 Haywood Street
Project: Yancey-Mitchell Surface Water
Wells
Anchor QEA of North Carolina, PLLC
Asheville, NC 28801
Attn: Brian Gant
Prism Work Order: 7030458
Time Submitted: 3/30/2017 11:25:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P7C0513 - NO PREP
Blank (P7C0513-BLK1)Prepared & Analyzed: 03/31/17
Total Alkalinity to pH 4.5 ug/LBRL5000
LCS (P7C0513-BS1)Prepared & Analyzed: 03/31/17
Total Alkalinity to pH 4.5 ug/L2540005000 250000 90-110102
Batch P7D0024 - NO PREP
Blank (P7D0024-BLK1)Prepared & Analyzed: 04/03/17
Total Dissolved Solids ug/LBRL50000
LCS (P7D0024-BS1)Prepared & Analyzed: 04/03/17
Total Dissolved Solids ug/L98800050000 1000000 90-11099
Sample Extraction Data
Prep Method: 3005A
Lab Number Batch Date/TimeInitialFinal
P7D00637030458-01 04/06/17 7:2550 50mL mL
P7D00637030458-02 04/06/17 7:2550 50mL mL
Prep Method: 7470A
Lab Number Batch Date/TimeInitialFinal
P7D02027030458-01 04/13/17 8:2020 30mL mL
P7D02027030458-02 04/13/17 8:2020 30mL mL
Prep Method: 5030B
Lab Number Batch Date/TimeInitialFinal
P7C05207030458-01 03/31/17 16:1010 10mL mL
P7C05207030458-02 03/31/17 16:1010 10mL mL
P7C05207030458-03 03/31/17 16:1010 10mL mL
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