16041 Fleming Labs BF Redevelopment Summary Rpt 20140924

Via 2nd Day FedEx
September 24, 2014
NC DENR Brownfields Section
Division of Waste Management
1646 Mail Service Center
Raleigh, NC 27699-1646
Attention: Mr. Tony Duque
Brownfields Project Manager

Re: Brownfields Redevelopment Report
Fleming Laboratories Charlotte, North Carolina
Brownfields Project #16041-12-060
H&H Project No. FMG-003
Dear Tony:

On behalf of Fleming Laboratories (Fleming), Hart & Hickman, PC is providing the attached
Brownfields Redevelopment Report in accordance with the Environmental Action Plan for the
Fleming Ready for Re-Use project in Charlotte, Mecklenburg County, North Carolina. This report is provided as a PDF on CD and as a hard copy. Should you have any questions or need additional
information, please do not hesitate to contact me at [phone].

Sincerely,
Hart & Hickman, PC
Matt Bramblett, PE
Principal
Attachment
cc: Mr. George Fleming, Fleming Labs (via email; CD and 2 copies via US Mail)
Ms. Amanda Short, HMW (via email)
Mr. Benne Hutson, HMW (via email)
Brownfields Redevelopment Report
Fleming Laboratories
BF Project No. 16041-12-060

2205, 2009, and 2215 Thrift Road
Charlotte, North Carolina

H&H Job No. FMG-003
September 24, 2014

Brownfields Redevelopment Report Fleming Laboratories
2205, 2209, and 2215 Thrift Road
Charlotte, North Carolina H&H Job No. FMG-003 Table of Contents

Section Page
1.0 Introduction .............................................................................................................................1
2.0 Building Demolition ................................................................................................................2
2.1 Asbestos Abatement..............................................................................................................2
2.2 Hazardous Building Materials ..............................................................................................3
2.3 C&D Debris ..........................................................................................................................4
2.4 UST Abandonment ...............................................................................................................4
3.0 Hazardous Soil Management .................................................................................................5
4.0 Site Restoration .......................................................................................................................7
4.1 Phase I Grading .....................................................................................................................7
4.2 Phase II Grading ...................................................................................................................7
5.0 Summary ..................................................................................................................................9

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List of Tables

Table 1 Hazardous Material Disposal Summary
Table 2 Post-Excavation Soil Sample Results
Table 3 Borrow Pit Soil Sample Results

List of Figures

Figure 1 Site Location Map
Figure 2 Site Map
Figure 3 Identified Regulated Building Materials
Figure 4 Characteristically Hazardous Soil Map
Figure 5 Shallow Soil Arsenic Concentration Map

List of Appendices

Appendix A Regulated Material Disposal Manifests
Appendix B UST Abandonment Documentation
Appendix C Laboratory Analytical Data
Appendix D Site Redevelopment Plans

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Brownfields Redevelopment Report Fleming Laboratories
2205, 2209, and 2215 Thrift Road
Charlotte, North Carolina H&H Job No. FMG-003
1.0 Introduction

On behalf of Fleming Laboratories Inc. (Fleming), Hart & Hickman, PC (H&H) has prepared
this Brownfields redevelopment report to document redevelopment activities at the Fleming
properties located at 2205, 2209, and 2215 Thrift Road in Charlotte, North Carolina (Figure 1).
The redevelopment activities were conducted under the North Carolina Department of
Environment and Natural Resources (DENR) Ready for Reuse Brownfields Program
(Project Number 16041-12-060). The redevelopment activities were conducted in accordance
with the DENR-approved Environment Action Plan (EAP) which was prepared by H&H and
submitted to DENR on October 23, 2013.

Four of the five site buildings were demolished with a gravel parking lot constructed in their
place. The following sections describe the building demolition, management of impacted soils
and regulated building materials, soil grading activities, and sampling activities. Redevelopment
activities began in March 2014 and were completed in June 2014. With the exception of the
stormwater piping installation, the building demolition and parking lot construction work were
conducted by Contaminant Control, Inc. (CCI).

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2.0 Building Demolition
Buildings identified for demolition as part of the redevelopment activities included Building B,
Building C, Building D, and Building E. Building A remains in place and continues to be used
by Fleming. A Site map is included as Figure 2. Previous assessment activities of building
materials identified leachable levels of arsenic above characteristic hazardous waste levels in
certain areas. These materials were identified in the Refined Building Floor Assessment report
dated December 18, 2012. In addition, asbestos containing material (ACM) found in these
buildings were reported in the Asbestos Survey dated January 19, 2012 and the Asbestos Survey
Report-Supplemental dated December 3, 2013. These characteristically hazardous building
materials and ACMs were managed separately from the general construction and demolition
(C&D) debris generated during demolition. The management of each of these materials is
discussed in greater detail in the following sections. A summary of the hazardous waste disposal
amounts is included in Table 1.

2.1 Asbestos Abatement

Prior to building demolition, an asbestos abatement was performed by CCI, a licensed asbestos
removal contractor. The onsite materials classified as ACM are identified on Figure 3. In
general, the ACM on the site consisted of non-friable roofing, flashing, and coated stickups of
Buildings B, C, D, and E, and the rear windows of Building B. In addition, a boiler and 1ft of
piping thermal system insulation (TSI) located in the basement of Building C were determined to
be friable ACM.

The non-friable roofing, flashing, and coated stickups of Buildings B, C, D, and E, were
removed using hand tools and containerized in lined and covered roll off dumpsters. The
windows of Building B were sprayed with an adhesive and double wrapped in 6 mil
polyethylene sheeting. Once wrapped the windows were placed in the roll off dumpsters along
with the roofing, flashing, and stickups.

Prior to disposal of the boiler and 1 ft of pipe in the basement of Building C, the friable TSI was
removed using hand tools enclosed in a negative pressure chamber attached to a three stage
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decontamination trailer. The TSI from the boiler and piping was bagged and transported to
CCI’s Salisbury, NC office. The piping was sprayed with adhesive and double wrapped in 6 mil
polyethylene sheeting and also sent to CCI’s Salisbury office. The boiler was double wrapped in
6 mil polyethylene sheeting and placed in the roll off dumpsters along with the roofing, flashing,
and coated stickups.

The roll off dumpsters were transported to Greenway Waste Solutions in Huntersville,
North Carolina for disposal as non-friable ACM. A total of 53.84 tons of non-friable ACM was
removed from the site. Waste Shipment Records for the non-friable ACM disposal are included
in Appendix A

The TSI was sent to CCI’s Salisbury facility for bulking and then transported to HAM Sanitary
Landfill in Peterstown, West Virginia. A total of 18 bags (approximately 120 sq ft) of friable
material and 1 linear foot of friable piping was disposed. The Waste Shipment Manifest for the
friable ACM disposal is also included in Appendix A.

Prior to building demolition, H&H and CCI personnel performed a final asbestos review and
confirmed that the identified ACMs had been removed from the site buildings to be demolished.

2.2 Hazardous Building Materials
As mentioned above, previous building material assessment activities identified certain floors in
the buildings as containing leachable concentrations of arsenic above characteristically
hazardous waste levels. These areas included a portion of the concrete floor in Building C and a
portion of the wood floor in Building D (Figure 3). Prior to building demolition, these materials
were removed and placed into lined and covered roll off containers. The wood material from
Building D was removed using hand tools and cut into sections no greater than 3 ft in length
prior to placement in the roll off container. The concrete floor in Building C was separated from
the rest of the building utilizing a skid steer with a breaker attachment. Once the concrete was
separated from the rest of the structure, it was placed in roll off containers. A total of 22.13 tons
of wood and a total of 52.34 tons of concrete were removed from the site for disposal as
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hazardous waste (Table 1). Hazardous waste manifests for the wood and concrete materials are
provided in Appendix A.

2.3 C&D Debris
Material not identified as hazardous waste or as an ACM was demolished using a track mounted
excavator with a breaker and hand tools. C&D debris was separated by type (wood, metal, or
concrete) as demolition activities progressed. Materials were then loaded onto trucks for offsite
disposal. Wood material and concrete floors identified as non-hazardous were disposed at
Greenway Waste Solutions (GWS) of Harrisburg in Concord, North Carolina. Concrete
materials from the walls and ceiling of the facility were sent for recycling at C&M Recycling in
Charlotte, North Carolina. Metal materials were recycled at A-1 recycling in Gastonia, North
Carolina. Approximately 1,840 tons of C&D material were disposed of offsite.

2.4 UST Abandonment

As part of redevelopment activities, an approximate 900-gallon heating oil underground storage
tank (UST) located on the eastern side of the property was abandoned in place. The tank was
uncovered during demolition activities and observed to contain residual fuel and water. No
impacts from the UST were observed on the surface near the UST. CCI utilized a vacuum truck
to remove fluids from the tank. Following fluid removal, CCI thoroughly rinsed the tank with a
power washer and vacuumed out the wash water. Once the tank was cleaned, it was filled with
flowable cement and covered with soil. Abandonment documentation for UST is included in
Appendix B.

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3.0 Hazardous Soil Management
Soils containing leachable concentrations of arsenic were identified during site assessment
activities as described in the Arsenic Assessment report dated July 10, 2012. In order to
complete planned grading activities for site redevelopment, hazardous soil above the grade line
needed to be excavated and transported to a permitted hazardous waste disposal facility. These
areas are identified on Figure 4. Following soil excavation, composite samples were collected
from the sidewalls of the excavation to confirm that the hazardous soil had been adequately
removed. The hazardous soil excavation, sampling, and analytical results are described in the
following section.

Soil containing arsenic above the characteristically hazardous waste threshold was cut from two
areas of the site near the northwest corner of Building B and under the southwest corner of
Building B. Soil was direct loaded onto transport trucks using a Uniform Hazardous Waste
Manifest for disposal at a permitted hazardous waste disposal facility.

A wedge of impacted soil was removed near the northwest corner of Building B to allow for
placement of the clean soil cap where the original grade was relatively high. Because the cut
soil tapered away to the west and abutted existing hardscape to the north, only one composite
sidewall sample (SW-3) was collected to confirm that hazardous waste soil was adequately
removed (Figure 4). The soil sample was analyzed for TCLP arsenic and the lab report is
provided in Appendix C. The detected concentration of arsenic (0.10 mg/L) was below the
characteristically hazardous waste level of 5.0 mg/L (Table 2).

After demolition of Building B, a rectangular block of impacted soil was removed from under
the southwest corner of Building B because soil impacts exceeded the characteristically
hazardous waste level for arsenic and also were being cut to meet the proposed grade. The
reason that soils were cut in this area is that the built up concrete slab for Building B was on soil
that was higher than surrounding grades. Because the cut soil abutted the exterior wall to the
west (where the soil grade was approximately 4 ft lower) and the basement of Building C to the
south, only two composite sidewall samples (SW-1 and SW-2) were collected to confirm that
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hazardous waste soil was adequately removed (Figure 4). A composite base sample (B-1) was
also collected at a depth of four ft within the block of soil.

TCLP arsenic exceeded the characteristically hazardous waste level in sample B-1 and SW-1
(Table 2 and Appendix C), and additional soil was removed. For this additional excavation,
approximately 1 to 2 ft were cut below sample B-1 to get to 1 ft below the proposed final grade
(to allow for capping with clean soil). Because the remaining soil below B-1 would not be
disturbed by grading, it was left in place and a second base sample was not collected. In
addition, approximately 10 ft were cut to the north of sample SW-1. Composite sidewall sample
SW-1B was then collected. TCLP arsenic was not detected in sample SW-1B (Table 2 and
Appendix C).

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4.0 Site Restoration
Site restoration and grading plans were developed by Isaacs Group, LLC based on design
specifications outlined in the EAP. Plans provided by Isaacs Group are included in Appendix D.
Site restoration included grading of site soils, installation of geofabric, storm water piping
installation, import of clean fill and gravel, and hydro-seeding. Site restoration procedures are
discussed in greater detail in the following section.

4.1 Phase I Grading

As discussed in the July 2012 Arsenic Assessment Report, shallow soil at the site contains levels
of arsenic above the DENR Inactive Hazardous Sites Branch (IHSB) Non-Residential
Preliminary Soil Remediation Goal (PSRG) (Figure 5). In accordance with the EAP, grading
activities were tracked in order to record replacement of impacted soil onsite. The approximate
extent of cut and fill areas are depicted on Figure 5. In general, soils cut from the western
portion of the site were used as fill in the former basement of Building C, while soils cut from
the eastern portion of the site were used as fill in the southeastern portion of the site as part of the
Phase I Grading Plan.

Following completion of the Phase I grading plan, CCI began the installation of geofabric across
the site. The geofabric was unrolled on the soil and overlapped the adjacent section of geofabric
by a minimum of 18 inches. Concurrent with the installation of the geofabric, the stormwater
piping shown on Isaacs Group’s plans in the southern portion of the site was installed by Harvest
Environmental. Soil removed from this area to allow for the installation of the pipe was used as
fill in the southwest portion of this site as shown on Figure 5.

4.2 Phase II Grading
Following Phase I grading activities and installation of geofabric, Phase II grading activities
began. In accordance with the EAP, to protect future workers and occupants from impacted site
soil and clean fill material was imported and placed to cover the geofabric a minimum of 1 ft.
The perimeter of the site consisted of 1 ft of clean soil. The central area of the site consisted of
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6-inches of clean soil overlain by 6-inches of gravel as shown on the Phase II Grading Plan in
Appendix C. In accordance with the EAP, two composite samples were collected from a
reputable borrow source (Berryhill) for analysis of VOCs, SVOCs, and HSL Metals. No VOCs
or SVOCs were detected, and HSL metals were consistent with naturally occurring
concentrations in the area (Table 3). The laboratory report along with the chain of custody form
are included in Appendix C.

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5.0 Summary

Site redevelopment activities have been completed at the Fleming Laboratories site as part of the
Brownfields Program Ready for Reuse program (Brownfields Project No 16041-12-060). Site
redevelopment activities were completed in accordance with the DENR-approved EAP
submitted on October 23, 2013. The redevelopment activities included the segregation and
disposal of ACM; characteristically hazardous building materials and soil and placement;
demolition of Building B, C, D, and E; site grading, geofabric barrier installation; and import of
clean cap materials.

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Table 1
Hazardous Material Disposal Summary
Fleming Laboratories
Charlotte, North Carolina
H&H Job No. FMG.003
S:\AAA-Master Projects\Fleming Labs (FMG)\FMG-003 Demo Phase\Post Development Report\Tables
Table 1 (Page 1 of 1)
Hart & Hickman, PC
Manifest ID Material Type Facility Disposal Date Estimated Tonnage(1)Final Tonnage(2)
012056614JJK Arsenic Wood 4/21/2014 12 17.37
012056613JJK Arsenic Wood 4/23/2014 12 4.76
22.13
012056595JJK Arsenic Concrete 4/25/2014 18 10.79
012056594JJK Arsenic Concrete 4/25/2014 18 12.06
012056596JJK Arsenic Concrete 4/28/2014 19 15.96
012056593JJK Arsenic Concrete 4/28/2014 19 13.53
52.34
012056605JJK Arsenic Soil 5/7/2014 22 24.7
012056607JJK Arsenic Soil 5/7/2014 22 28.3
012056606JJK Arsenic Soil 5/7/2014 22 23.74
012056609JJK Arsenic Soil 5/15/2014 23
012056611JJK Arsenic Soil 5/15/2014 24
012056610JJK Arsenic Soil 5/15/2014 24 28.66
156.44
Notes:
1. Estimated tonnage based on transport drivers reading of truck pressure gauges
2. Final tonnage recorded on scales at disposal facility
Total Hazardous Soil Disposal
51.04
Total Hazardous Concrete Disposal
Total Hazardous Wood Disposal
Table 2
Post-Excavation Soil Sample Results
Fleming Laboratories
Charlotte, North Carolina
H&H Job No. FMG.003
S:\AAA-Master Projects\Fleming Labs (FMG)\FMG-003 Demo Phase\Post Development Report\Tables
Table 2 (Page 1 of 1)Hart & Hickman, PC
Screening Criteria
Sample ID SW-1 B-1 SW-1B SW-2 SW-3
Depth from Original Grade (ft)2 to 3 4 2 to 3 2 to 3 1
Sample Date 5/6/2014 5/6/2014 5/14/2014 5/6/2014 5/6/2014
TCLP Metals (6010)
Arsenic 42 35 <0.050 <0.050 0.10 5
Notes:
Units reported in mg/kg
1. Resource Recovery Conservation Act Characteristic Hazardous Waste Level
EPA Method follows parameter in parenthesis
RCRA Characteristic
Hazardous Level1
Table 3
Borrow Pit Soil Sample Results
Fleming Laboratories
Charlotte, North Carolina
H&H Job No. FMG.003
S:\AAA-Master Projects\Fleming Labs (FMG)\FMG-003 Demo Phase\Post Development Report\Tables
Table 3 (Page 1 of 1)
Hart & Hickman, PC
Sample ID Berryhill Borrow Berryhill Borrow-2
Sample Type Composite Composite
Sample Date 5/14/2014 5/21/2014
VOCs (8260)BRL BRL --
SVOCs (8270)BRL BRL --
HSL Metals (6010/7471/7196) Range Mean
Arsenic 1.3 <0.68 2.4 1.0 - 18 4.8
Beryllium 1.5 0.47 400 nd - 2.0 0.11
Chromium 77 8.8 100,000 7.0 - 300 65
Copper 130 44.2 8,200 3.0 - 100 34
Lead 13 4.8 800 nd - 50 16
Manganese 930 466 4,600 8.0 - 3,394*594*
Nickel 34 8.7 4,000 nd - 150 23
Selenium 1.5 0.68 1,000 <0.1 - 0.8 0.42
Thallium 1.0 <0.68 2.0 NE NE
Zinc 97 44.8 62,000 25 - 140 56
Mercury <0.026 0.0045 3.1 0.03 - 0.52 0.121
Notes:
Units reported in mg/kg
1. NC DENR Inactive Hazardous Sites Branch (IHSB) Industrial Health Based Soil Remediation Goals (SRGs) - Janurary 2014
2. NC Background Metals in Soil values from Elements in North American Soils by Dragun and Chekiri, 2005
* Values for Southeastern USA soils used because North Carolina soils not specified
Only constituents with at least one detection shown
EPA Method follows parameter in parenthesis
BRL = Below Reporitng Limits; -- = Not Applicable; NE = Not Established
VOCs = Volatile Organic Compounds; SVOCs = Semi-VOCs; HSL = Hazardous Substance List
Background Metals in Soil2
Screening Criteria
Industrial SRG1
SITE
0 2000 4000
APPROXIMATE
SCALE IN FEET
N
U.S.G.S. QUADRANGLE MAPS
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
TITLE
PROJECT
SITE LOCATION MAP
FLEMING LABORATORIESCHARLOTTE, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE:
7-30-14 0
1FMG-003
Charlotte East, North Carolina, 1988

Appendix A
Regulated Material Disposal Manifests

Appendix B
UST Abandonment Documentation

Appendix C
Laboratory Analytical Data

#=CL#
May 27, 2014
LIMS USE: FR - JOHN LOPEZ
LIMS OBJECT ID: 92202395
92202395
Project:
Pace Project No.:
RE:
John Lopez
Hart & Hickman
2923 S. Tryon St
Suite 100
Charlotte, NC 28203
FLEMING LABS
Dear John Lopez:
Enclosed are the analytical results for sample(s) received by the laboratory on May 21, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 22
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92202395
FLEMING LABS
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92202395
FLEMING LABS
Sample:BERRHILL BORROW - 2 Lab ID:92202395001 Collected:05/21/14 12:00 Received:05/21/14 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Antimony ND mg/kg 05/23/14 05:46 7440-36-005/22/14 14:400.34 1
Arsenic ND mg/kg 05/23/14 05:46 7440-38-205/22/14 14:400.68 1
Beryllium 0.47 mg/kg 05/23/14 05:46 7440-41-705/22/14 14:400.068 1
Cadmium ND mg/kg 05/23/14 05:46 7440-43-905/22/14 14:400.068 1
Chromium 8.9 mg/kg 05/23/14 05:46 7440-47-305/22/14 14:400.34 1
Copper 44.2 mg/kg 05/23/14 05:46 7440-50-805/22/14 14:400.34 1
Lead 4.8 mg/kg 05/23/14 05:46 7439-92-105/22/14 14:400.34 1
Manganese 466 mg/kg 05/23/14 05:46 7439-96-505/22/14 14:400.34 1
Nickel 8.7 mg/kg 05/23/14 05:46 7440-02-005/22/14 14:400.34 1
Selenium ND mg/kg 05/23/14 05:46 7782-49-205/22/14 14:400.68 1
Silver ND mg/kg 05/23/14 05:46 7440-22-405/22/14 14:400.34 1
Thallium ND mg/kg 05/23/14 05:46 7440-28-005/22/14 14:400.68 1
Zinc 44.8 mg/kg 05/23/14 05:46 7440-66-605/22/14 14:400.68 1
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.0045 mg/kg 05/23/14 16:36 7439-97-605/22/14 20:450.0038 1
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 05/27/14 10:50 83-32-905/23/14 14:363891
Acenaphthylene ND ug/kg 05/27/14 10:50 208-96-805/23/14 14:363891
Aniline ND ug/kg 05/27/14 10:50 62-53-305/23/14 14:363891
Anthracene ND ug/kg 05/27/14 10:50 120-12-705/23/14 14:363891
Benzo(a)anthracene ND ug/kg 05/27/14 10:50 56-55-305/23/14 14:363891
Benzo(a)pyrene ND ug/kg 05/27/14 10:50 50-32-805/23/14 14:363891
Benzo(b)fluoranthene ND ug/kg 05/27/14 10:50 205-99-205/23/14 14:363891
Benzo(g,h,i)perylene ND ug/kg 05/27/14 10:50 191-24-205/23/14 14:363891
Benzo(k)fluoranthene ND ug/kg 05/27/14 10:50 207-08-905/23/14 14:363891
Benzoic Acid ND ug/kg 05/27/14 10:50 65-85-005/23/14 14:3619401
Benzyl alcohol ND ug/kg 05/27/14 10:50 100-51-605/23/14 14:367771
4-Bromophenylphenyl ether ND ug/kg 05/27/14 10:50 101-55-305/23/14 14:363891
Butylbenzylphthalate ND ug/kg 05/27/14 10:50 85-68-705/23/14 14:363891
4-Chloro-3-methylphenol ND ug/kg 05/27/14 10:50 59-50-705/23/14 14:367771
4-Chloroaniline ND ug/kg 05/27/14 10:50 106-47-805/23/14 14:3619401
bis(2-Chloroethoxy)methane ND ug/kg 05/27/14 10:50 111-91-105/23/14 14:363891
bis(2-Chloroethyl) ether ND ug/kg 05/27/14 10:50 111-44-405/23/14 14:363891
bis(2-Chloroisopropyl) ether ND ug/kg 05/27/14 10:50 108-60-105/23/14 14:363891
2-Chloronaphthalene ND ug/kg 05/27/14 10:50 91-58-705/23/14 14:363891
2-Chlorophenol ND ug/kg 05/27/14 10:50 95-57-805/23/14 14:363891
4-Chlorophenylphenyl ether ND ug/kg 05/27/14 10:50 7005-72-305/23/14 14:363891
Chrysene ND ug/kg 05/27/14 10:50 218-01-905/23/14 14:363891
Dibenz(a,h)anthracene ND ug/kg 05/27/14 10:50 53-70-305/23/14 14:363891
Dibenzofuran ND ug/kg 05/27/14 10:50 132-64-905/23/14 14:363891
1,2-Dichlorobenzene ND ug/kg 05/27/14 10:50 95-50-105/23/14 14:363891
1,3-Dichlorobenzene ND ug/kg 05/27/14 10:50 541-73-105/23/14 14:363891
1,4-Dichlorobenzene ND ug/kg 05/27/14 10:50 106-46-705/23/14 14:363891
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/27/2014 11:29 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92202395
FLEMING LABS
Sample:BERRHILL BORROW - 2 Lab ID:92202395001 Collected:05/21/14 12:00 Received:05/21/14 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
3,3'-Dichlorobenzidine ND ug/kg 05/27/14 10:50 91-94-105/23/14 14:3619401
2,4-Dichlorophenol ND ug/kg 05/27/14 10:50 120-83-205/23/14 14:363891
Diethylphthalate ND ug/kg 05/27/14 10:50 84-66-205/23/14 14:363891
2,4-Dimethylphenol ND ug/kg 05/27/14 10:50 105-67-905/23/14 14:363891
Dimethylphthalate ND ug/kg 05/27/14 10:50 131-11-305/23/14 14:363891
Di-n-butylphthalate ND ug/kg 05/27/14 10:50 84-74-205/23/14 14:363891
4,6-Dinitro-2-methylphenol ND ug/kg 05/27/14 10:50 534-52-105/23/14 14:367771
2,4-Dinitrophenol ND ug/kg 05/27/14 10:50 51-28-505/23/14 14:3619401
2,4-Dinitrotoluene ND ug/kg 05/27/14 10:50 121-14-205/23/14 14:363891
2,6-Dinitrotoluene ND ug/kg 05/27/14 10:50 606-20-205/23/14 14:363891
Di-n-octylphthalate ND ug/kg 05/27/14 10:50 117-84-005/23/14 14:363891
bis(2-Ethylhexyl)phthalate ND ug/kg 05/27/14 10:50 117-81-705/23/14 14:363891
Fluoranthene ND ug/kg 05/27/14 10:50 206-44-005/23/14 14:363891
Fluorene ND ug/kg 05/27/14 10:50 86-73-705/23/14 14:363891
Hexachloro-1,3-butadiene ND ug/kg 05/27/14 10:50 87-68-305/23/14 14:363891
Hexachlorobenzene ND ug/kg 05/27/14 10:50 118-74-105/23/14 14:363891
Hexachlorocyclopentadiene ND ug/kg 05/27/14 10:50 77-47-405/23/14 14:363891
Hexachloroethane ND ug/kg 05/27/14 10:50 67-72-105/23/14 14:363891
Indeno(1,2,3-cd)pyrene ND ug/kg 05/27/14 10:50 193-39-505/23/14 14:363891
Isophorone ND ug/kg 05/27/14 10:50 78-59-105/23/14 14:363891
1-Methylnaphthalene ND ug/kg 05/27/14 10:50 90-12-005/23/14 14:363891
2-Methylnaphthalene ND ug/kg 05/27/14 10:50 91-57-605/23/14 14:363891
2-Methylphenol(o-Cresol)ND ug/kg 05/27/14 10:50 95-48-705/23/14 14:363891
3&4-Methylphenol(m&p Cresol)ND ug/kg 05/27/14 10:5005/23/14 14:363891
Naphthalene ND ug/kg 05/27/14 10:50 91-20-305/23/14 14:363891
2-Nitroaniline ND ug/kg 05/27/14 10:50 88-74-405/23/14 14:3619401
3-Nitroaniline ND ug/kg 05/27/14 10:50 99-09-205/23/14 14:3619401
4-Nitroaniline ND ug/kg 05/27/14 10:50 100-01-605/23/14 14:367771
Nitrobenzene ND ug/kg 05/27/14 10:50 98-95-305/23/14 14:363891
2-Nitrophenol ND ug/kg 05/27/14 10:50 88-75-505/23/14 14:363891
4-Nitrophenol ND ug/kg 05/27/14 10:50 100-02-705/23/14 14:3619401
N-Nitrosodimethylamine ND ug/kg 05/27/14 10:50 62-75-905/23/14 14:363891
N-Nitroso-di-n-propylamine ND ug/kg 05/27/14 10:50 621-64-705/23/14 14:363891
N-Nitrosodiphenylamine ND ug/kg 05/27/14 10:50 86-30-605/23/14 14:363891
Pentachlorophenol ND ug/kg 05/27/14 10:50 87-86-505/23/14 14:3619401
Phenanthrene ND ug/kg 05/27/14 10:50 85-01-805/23/14 14:363891
Phenol ND ug/kg 05/27/14 10:50 108-95-205/23/14 14:363891
Pyrene ND ug/kg 05/27/14 10:50 129-00-005/23/14 14:363891
1,2,4-Trichlorobenzene ND ug/kg 05/27/14 10:50 120-82-105/23/14 14:363891
2,4,5-Trichlorophenol ND ug/kg 05/27/14 10:50 95-95-405/23/14 14:363891
2,4,6-Trichlorophenol ND ug/kg 05/27/14 10:50 88-06-205/23/14 14:363891
Surrogates
Nitrobenzene-d5 (S)81 %05/27/14 10:50 4165-60-005/23/14 14:3623-110 1
2-Fluorobiphenyl (S)64 %05/27/14 10:50 321-60-805/23/14 14:3630-110 1
Terphenyl-d14 (S)79 %05/27/14 10:50 1718-51-005/23/14 14:3628-110 1
Phenol-d6 (S)52 %05/27/14 10:50 13127-88-305/23/14 14:3622-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/27/2014 11:29 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92202395
FLEMING LABS
Sample:BERRHILL BORROW - 2 Lab ID:92202395001 Collected:05/21/14 12:00 Received:05/21/14 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Surrogates
2-Fluorophenol (S)55 %05/27/14 10:50 367-12-405/23/14 14:3613-110 1
2,4,6-Tribromophenol (S)61 %05/27/14 10:50 118-79-605/23/14 14:3627-110 1
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 05/22/14 22:52 67-64-185.3 1
Benzene ND ug/kg 05/22/14 22:52 71-43-24.3 1
Bromobenzene ND ug/kg 05/22/14 22:52 108-86-14.3 1
Bromochloromethane ND ug/kg 05/22/14 22:52 74-97-54.3 1
Bromodichloromethane ND ug/kg 05/22/14 22:52 75-27-44.3 1
Bromoform ND ug/kg 05/22/14 22:52 75-25-24.3 1
Bromomethane ND ug/kg 05/22/14 22:52 74-83-98.5 1
2-Butanone (MEK)ND ug/kg 05/22/14 22:52 78-93-385.3 1
n-Butylbenzene ND ug/kg 05/22/14 22:52 104-51-84.3 1
sec-Butylbenzene ND ug/kg 05/22/14 22:52 135-98-84.3 1
tert-Butylbenzene ND ug/kg 05/22/14 22:52 98-06-64.3 1
Carbon tetrachloride ND ug/kg 05/22/14 22:52 56-23-54.3 1
Chlorobenzene ND ug/kg 05/22/14 22:52 108-90-74.3 1
Chloroethane ND ug/kg 05/22/14 22:52 75-00-38.5 1
Chloroform ND ug/kg 05/22/14 22:52 67-66-34.3 1
Chloromethane ND ug/kg 05/22/14 22:52 74-87-38.5 1
2-Chlorotoluene ND ug/kg 05/22/14 22:52 95-49-84.3 1
4-Chlorotoluene ND ug/kg 05/22/14 22:52 106-43-44.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 05/22/14 22:52 96-12-84.3 1
Dibromochloromethane ND ug/kg 05/22/14 22:52 124-48-14.3 1
1,2-Dibromoethane (EDB)ND ug/kg 05/22/14 22:52 106-93-44.3 1
Dibromomethane ND ug/kg 05/22/14 22:52 74-95-34.3 1
1,2-Dichlorobenzene ND ug/kg 05/22/14 22:52 95-50-14.3 1
1,3-Dichlorobenzene ND ug/kg 05/22/14 22:52 541-73-14.3 1
1,4-Dichlorobenzene ND ug/kg 05/22/14 22:52 106-46-74.3 1
Dichlorodifluoromethane ND ug/kg 05/22/14 22:52 75-71-88.5 1
1,1-Dichloroethane ND ug/kg 05/22/14 22:52 75-34-34.3 1
1,2-Dichloroethane ND ug/kg 05/22/14 22:52 107-06-24.3 1
1,1-Dichloroethene ND ug/kg 05/22/14 22:52 75-35-44.3 1
cis-1,2-Dichloroethene ND ug/kg 05/22/14 22:52 156-59-24.3 1
trans-1,2-Dichloroethene ND ug/kg 05/22/14 22:52 156-60-54.3 1
1,2-Dichloropropane ND ug/kg 05/22/14 22:52 78-87-54.3 1
1,3-Dichloropropane ND ug/kg 05/22/14 22:52 142-28-94.3 1
2,2-Dichloropropane ND ug/kg 05/22/14 22:52 594-20-74.3 1
1,1-Dichloropropene ND ug/kg 05/22/14 22:52 563-58-64.3 1
cis-1,3-Dichloropropene ND ug/kg 05/22/14 22:52 10061-01-54.3 1
trans-1,3-Dichloropropene ND ug/kg 05/22/14 22:52 10061-02-64.3 1
Diisopropyl ether ND ug/kg 05/22/14 22:52 108-20-34.3 1
Ethylbenzene ND ug/kg 05/22/14 22:52 100-41-44.3 1
Hexachloro-1,3-butadiene ND ug/kg 05/22/14 22:52 87-68-34.3 1
2-Hexanone ND ug/kg 05/22/14 22:52 591-78-642.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/27/2014 11:29 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92202395
FLEMING LABS
Sample:BERRHILL BORROW - 2 Lab ID:92202395001 Collected:05/21/14 12:00 Received:05/21/14 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Isopropylbenzene (Cumene)ND ug/kg 05/22/14 22:52 98-82-84.3 1
p-Isopropyltoluene ND ug/kg 05/22/14 22:52 99-87-64.3 1
Methylene Chloride ND ug/kg 05/22/14 22:52 75-09-217.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 05/22/14 22:52 108-10-142.7 1
Methyl-tert-butyl ether ND ug/kg 05/22/14 22:52 1634-04-44.3 1
Naphthalene ND ug/kg 05/22/14 22:52 91-20-34.3 1
n-Propylbenzene ND ug/kg 05/22/14 22:52 103-65-14.3 1
Styrene ND ug/kg 05/22/14 22:52 100-42-54.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 05/22/14 22:52 630-20-64.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 05/22/14 22:52 79-34-54.3 1
Tetrachloroethene ND ug/kg 05/22/14 22:52 127-18-44.3 1
Toluene ND ug/kg 05/22/14 22:52 108-88-34.3 1
1,2,3-Trichlorobenzene ND ug/kg 05/22/14 22:52 87-61-64.3 1
1,2,4-Trichlorobenzene ND ug/kg 05/22/14 22:52 120-82-14.3 1
1,1,1-Trichloroethane ND ug/kg 05/22/14 22:52 71-55-64.3 1
1,1,2-Trichloroethane ND ug/kg 05/22/14 22:52 79-00-54.3 1
Trichloroethene ND ug/kg 05/22/14 22:52 79-01-64.3 1
Trichlorofluoromethane ND ug/kg 05/22/14 22:52 75-69-44.3 1
1,2,3-Trichloropropane ND ug/kg 05/22/14 22:52 96-18-44.3 1
1,2,4-Trimethylbenzene ND ug/kg 05/22/14 22:52 95-63-64.3 1
1,3,5-Trimethylbenzene ND ug/kg 05/22/14 22:52 108-67-84.3 1
Vinyl acetate ND ug/kg 05/22/14 22:52 108-05-442.7 1
Vinyl chloride ND ug/kg 05/22/14 22:52 75-01-48.5 1
Xylene (Total)ND ug/kg 05/22/14 22:52 1330-20-78.5 1
m&p-Xylene ND ug/kg 05/22/14 22:52 179601-23-18.5 1
o-Xylene ND ug/kg 05/22/14 22:52 95-47-64.3 1
Surrogates
Toluene-d8 (S)100 %05/22/14 22:52 2037-26-570-130 1
4-Bromofluorobenzene (S)100 %05/22/14 22:52 460-00-470-130 1
1,2-Dichloroethane-d4 (S)127 %05/22/14 22:52 17060-07-070-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 15.1 %05/23/14 16:240.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/27/2014 11:29 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92202395
FLEMING LABS
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/6649
EPA 7471
EPA 7471
7471 Mercury
Associated Lab Samples:92202395001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1205410
Associated Lab Samples:92202395001
Matrix:Solid
Analyzed
Mercury mg/kg ND 0.0050 05/23/14 16:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1205411LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.074.067 110 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1205412MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92202329001
1205413
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury mg/kg R1.066 79 75-125107 43.0940.033 0.086 0.13
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/27/2014 11:29 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92202395
FLEMING LABS
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/16020
EPA 3050
EPA 6010
6010 MET
Associated Lab Samples:92202395001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1204845
Associated Lab Samples:92202395001
Matrix:Solid
Analyzed
Antimony mg/kg ND 0.50 05/23/14 05:22
Arsenic mg/kg ND 1.0 05/23/14 05:22
Beryllium mg/kg ND 0.10 05/23/14 05:22
Cadmium mg/kg ND 0.10 05/23/14 05:22
Chromium mg/kg ND 0.50 05/23/14 05:22
Copper mg/kg ND 0.50 05/23/14 05:22
Lead mg/kg ND 0.50 05/23/14 05:22
Manganese mg/kg ND 0.50 05/23/14 05:22
Nickel mg/kg ND 0.50 05/23/14 05:22
Selenium mg/kg ND 1.0 05/23/14 05:22
Silver mg/kg ND 0.50 05/23/14 05:22
Thallium mg/kg ND 1.0 05/23/14 05:22
Zinc mg/kg ND 1.0 05/23/14 05:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1204846LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony mg/kg 47.750 95 80-120
Arsenic mg/kg 46.350 93 80-120
Beryllium mg/kg 46.650 93 80-120
Cadmium mg/kg 46.250 92 80-120
Chromium mg/kg 46.450 93 80-120
Copper mg/kg 46.850 94 80-120
Lead mg/kg 46.950 94 80-120
Manganese mg/kg 46.250 92 80-120
Nickel mg/kg 46.750 93 80-120
Selenium mg/kg 47.050 94 80-120
Silver mg/kg 23.425 94 80-120
Thallium mg/kg 45.050 90 80-120
Zinc mg/kg 46.850 94 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1204847MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92202329001
1204848
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Antimony mg/kg M148.8 45 75-12547 348.2ND 21.9 22.6
Arsenic mg/kg M148.8 67 75-12568 148.2ND 32.7 33.1
Beryllium mg/kg 48.8 80 75-12582 248.20.98 39.9 40.5
Cadmium mg/kg 48.8 77 75-12579 148.21.2 39.0 39.3
Chromium mg/kg 48.8 78 75-12581 148.263.3 101 102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/27/2014 11:29 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92202395
FLEMING LABS
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1204847MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92202329001
1204848
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Copper mg/kg 48.8 84 75-12586 048.216.4 57.7 57.9
Lead mg/kg M1,R148.8 68 75-125116 2348.256.2 89.3 112
Manganese mg/kg M148.8 -23 75-125-19 148.2237 226 228
Nickel mg/kg M148.8 74 75-12578 348.214.9 50.9 52.4
Selenium mg/kg M148.8 57 75-12557 148.2ND 27.9 27.7
Silver mg/kg 24.4 82 75-12584 124.1ND 20.2 20.5
Thallium mg/kg M148.8 64 75-12567 448.2ND 31.2 32.4
Zinc mg/kg M1,R148.8 115 75-125225 4048.247.5 104 156
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/27/2014 11:29 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92202395
FLEMING LABS
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/26916
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92202395001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1204924
Associated Lab Samples:92202395001
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 4.5 05/22/14 14:56
1,1,1-Trichloroethane ug/kg ND 4.5 05/22/14 14:56
1,1,2,2-Tetrachloroethane ug/kg ND 4.5 05/22/14 14:56
1,1,2-Trichloroethane ug/kg ND 4.5 05/22/14 14:56
1,1-Dichloroethane ug/kg ND 4.5 05/22/14 14:56
1,1-Dichloroethene ug/kg ND 4.5 05/22/14 14:56
1,1-Dichloropropene ug/kg ND 4.5 05/22/14 14:56
1,2,3-Trichlorobenzene ug/kg ND 4.5 05/22/14 14:56
1,2,3-Trichloropropane ug/kg ND 4.5 05/22/14 14:56
1,2,4-Trichlorobenzene ug/kg ND 4.5 05/22/14 14:56
1,2,4-Trimethylbenzene ug/kg ND 4.5 05/22/14 14:56
1,2-Dibromo-3-chloropropane ug/kg ND 4.5 05/22/14 14:56
1,2-Dibromoethane (EDB)ug/kg ND 4.5 05/22/14 14:56
1,2-Dichlorobenzene ug/kg ND 4.5 05/22/14 14:56
1,2-Dichloroethane ug/kg ND 4.5 05/22/14 14:56
1,2-Dichloropropane ug/kg ND 4.5 05/22/14 14:56
1,3,5-Trimethylbenzene ug/kg ND 4.5 05/22/14 14:56
1,3-Dichlorobenzene ug/kg ND 4.5 05/22/14 14:56
1,3-Dichloropropane ug/kg ND 4.5 05/22/14 14:56
1,4-Dichlorobenzene ug/kg ND 4.5 05/22/14 14:56
2,2-Dichloropropane ug/kg ND 4.5 05/22/14 14:56
2-Butanone (MEK)ug/kg ND 90.7 05/22/14 14:56
2-Chlorotoluene ug/kg ND 4.5 05/22/14 14:56
2-Hexanone ug/kg ND 45.4 05/22/14 14:56
4-Chlorotoluene ug/kg ND 4.5 05/22/14 14:56
4-Methyl-2-pentanone (MIBK)ug/kg ND 45.4 05/22/14 14:56
Acetone ug/kg ND 90.7 05/22/14 14:56
Benzene ug/kg ND 4.5 05/22/14 14:56
Bromobenzene ug/kg ND 4.5 05/22/14 14:56
Bromochloromethane ug/kg ND 4.5 05/22/14 14:56
Bromodichloromethane ug/kg ND 4.5 05/22/14 14:56
Bromoform ug/kg ND 4.5 05/22/14 14:56
Bromomethane ug/kg ND 9.1 05/22/14 14:56
Carbon tetrachloride ug/kg ND 4.5 05/22/14 14:56
Chlorobenzene ug/kg ND 4.5 05/22/14 14:56
Chloroethane ug/kg ND 9.1 05/22/14 14:56
Chloroform ug/kg ND 4.5 05/22/14 14:56
Chloromethane ug/kg ND 9.1 05/22/14 14:56
cis-1,2-Dichloroethene ug/kg ND 4.5 05/22/14 14:56
cis-1,3-Dichloropropene ug/kg ND 4.5 05/22/14 14:56
Dibromochloromethane ug/kg ND 4.5 05/22/14 14:56
Dibromomethane ug/kg ND 4.5 05/22/14 14:56
Dichlorodifluoromethane ug/kg ND 9.1 05/22/14 14:56
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/27/2014 11:29 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92202395
FLEMING LABS
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1204924
Associated Lab Samples:92202395001
Matrix:Solid
Analyzed
Diisopropyl ether ug/kg ND 4.5 05/22/14 14:56
Ethylbenzene ug/kg ND 4.5 05/22/14 14:56
Hexachloro-1,3-butadiene ug/kg ND 4.5 05/22/14 14:56
Isopropylbenzene (Cumene)ug/kg ND 4.5 05/22/14 14:56
m&p-Xylene ug/kg ND 9.1 05/22/14 14:56
Methyl-tert-butyl ether ug/kg ND 4.5 05/22/14 14:56
Methylene Chloride ug/kg ND 18.1 05/22/14 14:56
n-Butylbenzene ug/kg ND 4.5 05/22/14 14:56
n-Propylbenzene ug/kg ND 4.5 05/22/14 14:56
Naphthalene ug/kg ND 4.5 05/22/14 14:56
o-Xylene ug/kg ND 4.5 05/22/14 14:56
p-Isopropyltoluene ug/kg ND 4.5 05/22/14 14:56
sec-Butylbenzene ug/kg ND 4.5 05/22/14 14:56
Styrene ug/kg ND 4.5 05/22/14 14:56
tert-Butylbenzene ug/kg ND 4.5 05/22/14 14:56
Tetrachloroethene ug/kg ND 4.5 05/22/14 14:56
Toluene ug/kg ND 4.5 05/22/14 14:56
trans-1,2-Dichloroethene ug/kg ND 4.5 05/22/14 14:56
trans-1,3-Dichloropropene ug/kg ND 4.5 05/22/14 14:56
Trichloroethene ug/kg ND 4.5 05/22/14 14:56
Trichlorofluoromethane ug/kg ND 4.5 05/22/14 14:56
Vinyl acetate ug/kg ND 45.4 05/22/14 14:56
Vinyl chloride ug/kg ND 9.1 05/22/14 14:56
Xylene (Total)ug/kg ND 9.1 05/22/14 14:56
1,2-Dichloroethane-d4 (S)%106 70-132 05/22/14 14:56
4-Bromofluorobenzene (S)%104 70-130 05/22/14 14:56
Toluene-d8 (S)%101 70-130 05/22/14 14:56
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1204925LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 43.143.9 98 70-131
1,1,1-Trichloroethane ug/kg 37.943.9 86 70-141
1,1,2,2-Tetrachloroethane ug/kg 42.143.9 96 70-130
1,1,2-Trichloroethane ug/kg 38.343.9 87 70-132
1,1-Dichloroethane ug/kg 37.043.9 84 70-143
1,1-Dichloroethene ug/kg 39.143.9 89 70-137
1,1-Dichloropropene ug/kg 41.043.9 93 70-135
1,2,3-Trichlorobenzene ug/kg 38.843.9 88 69-153
1,2,3-Trichloropropane ug/kg 41.943.9 95 70-130
1,2,4-Trichlorobenzene ug/kg 40.843.9 93 55-171
1,2,4-Trimethylbenzene ug/kg 45.543.9 103 70-149
1,2-Dibromo-3-chloropropane ug/kg 41.943.9 95 68-141
1,2-Dibromoethane (EDB)ug/kg 40.843.9 93 70-130
1,2-Dichlorobenzene ug/kg 42.443.9 97 70-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/27/2014 11:29 AM
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Page 11 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92202395
FLEMING LABS
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1204925LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloroethane ug/kg 38.843.9 88 70-137
1,2-Dichloropropane ug/kg 37.743.9 86 70-133
1,3,5-Trimethylbenzene ug/kg 44.743.9 102 70-143
1,3-Dichlorobenzene ug/kg 40.843.9 93 70-144
1,3-Dichloropropane ug/kg 40.843.9 93 70-132
1,4-Dichlorobenzene ug/kg 43.143.9 98 70-142
2,2-Dichloropropane ug/kg 38.643.9 88 68-152
2-Butanone (MEK)ug/kg 77.5J87.9 88 70-149
2-Chlorotoluene ug/kg 41.343.9 94 70-141
2-Hexanone ug/kg 91.387.9 104 70-149
4-Chlorotoluene ug/kg 42.943.9 98 70-149
4-Methyl-2-pentanone (MIBK)ug/kg 81.287.9 92 70-153
Acetone ug/kg 77.5J87.9 88 70-157
Benzene ug/kg 38.443.9 87 70-130
Bromobenzene ug/kg 43.943.9 100 70-141
Bromochloromethane ug/kg 41.043.9 93 70-149
Bromodichloromethane ug/kg 42.043.9 96 70-130
Bromoform ug/kg 43.143.9 98 70-131
Bromomethane ug/kg 38.143.9 87 64-136
Carbon tetrachloride ug/kg 40.043.9 91 70-154
Chlorobenzene ug/kg 40.243.9 92 70-135
Chloroethane ug/kg 36.543.9 83 68-151
Chloroform ug/kg 42.743.9 97 70-130
Chloromethane ug/kg 35.743.9 81 70-132
cis-1,2-Dichloroethene ug/kg 39.343.9 89 70-140
cis-1,3-Dichloropropene ug/kg 40.143.9 91 70-137
Dibromochloromethane ug/kg 45.743.9 104 70-130
Dibromomethane ug/kg 38.643.9 88 70-136
Dichlorodifluoromethane ug/kg 40.543.9 92 36-148
Diisopropyl ether ug/kg 40.143.9 91 70-139
Ethylbenzene ug/kg 43.343.9 98 70-137
Hexachloro-1,3-butadiene ug/kg 40.943.9 93 70-145
Isopropylbenzene (Cumene)ug/kg 43.443.9 99 70-141
m&p-Xylene ug/kg 84.887.9 96 70-140
Methyl-tert-butyl ether ug/kg 39.543.9 90 45-150
Methylene Chloride ug/kg 36.243.9 82 70-133
n-Butylbenzene ug/kg 46.543.9 106 65-155
n-Propylbenzene ug/kg 44.043.9 100 70-148
Naphthalene ug/kg 39.543.9 90 70-148
o-Xylene ug/kg 42.343.9 96 70-141
p-Isopropyltoluene ug/kg 44.343.9 101 70-148
sec-Butylbenzene ug/kg 42.743.9 97 70-145
Styrene ug/kg 42.843.9 97 70-138
tert-Butylbenzene ug/kg 42.743.9 97 70-143
Tetrachloroethene ug/kg 43.643.9 99 70-140
Toluene ug/kg 39.843.9 91 70-130
trans-1,2-Dichloroethene ug/kg 39.243.9 89 70-136
trans-1,3-Dichloropropene ug/kg 39.443.9 90 70-138
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92202395
FLEMING LABS
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1204925LABORATORY CONTROL SAMPLE:
LCSSpike
Trichloroethene ug/kg 38.243.9 87 70-132
Trichlorofluoromethane ug/kg 40.543.9 92 69-134
Vinyl acetate ug/kg 76.2 F387.9 87 24-161
Vinyl chloride ug/kg 42.243.9 96 55-140
Xylene (Total)ug/kg 127132 96 70-141
1,2-Dichloroethane-d4 (S)%103 70-132
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%97 70-130
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92202395
FLEMING LABS
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/27888
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples:92202395001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1206172
Associated Lab Samples:92202395001
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 330 05/27/14 09:52
1,2-Dichlorobenzene ug/kg ND 330 05/27/14 09:52
1,3-Dichlorobenzene ug/kg ND 330 05/27/14 09:52
1,4-Dichlorobenzene ug/kg ND 330 05/27/14 09:52
1-Methylnaphthalene ug/kg ND 330 05/27/14 09:52
2,4,5-Trichlorophenol ug/kg ND 330 05/27/14 09:52
2,4,6-Trichlorophenol ug/kg ND 330 05/27/14 09:52
2,4-Dichlorophenol ug/kg ND 330 05/27/14 09:52
2,4-Dimethylphenol ug/kg ND 330 05/27/14 09:52
2,4-Dinitrophenol ug/kg ND 1650 05/27/14 09:52
2,4-Dinitrotoluene ug/kg ND 330 05/27/14 09:52
2,6-Dinitrotoluene ug/kg ND 330 05/27/14 09:52
2-Chloronaphthalene ug/kg ND 330 05/27/14 09:52
2-Chlorophenol ug/kg ND 330 05/27/14 09:52
2-Methylnaphthalene ug/kg ND 330 05/27/14 09:52
2-Methylphenol(o-Cresol)ug/kg ND 330 05/27/14 09:52
2-Nitroaniline ug/kg ND 1650 05/27/14 09:52
2-Nitrophenol ug/kg ND 330 05/27/14 09:52
3&4-Methylphenol(m&p Cresol)ug/kg ND 330 05/27/14 09:52
3,3'-Dichlorobenzidine ug/kg ND 1650 05/27/14 09:52
3-Nitroaniline ug/kg ND 1650 05/27/14 09:52
4,6-Dinitro-2-methylphenol ug/kg ND 660 05/27/14 09:52
4-Bromophenylphenyl ether ug/kg ND 330 05/27/14 09:52
4-Chloro-3-methylphenol ug/kg ND 660 05/27/14 09:52
4-Chloroaniline ug/kg ND 1650 05/27/14 09:52
4-Chlorophenylphenyl ether ug/kg ND 330 05/27/14 09:52
4-Nitroaniline ug/kg ND 660 05/27/14 09:52
4-Nitrophenol ug/kg ND 1650 05/27/14 09:52
Acenaphthene ug/kg ND 330 05/27/14 09:52
Acenaphthylene ug/kg ND 330 05/27/14 09:52
Aniline ug/kg ND 330 05/27/14 09:52
Anthracene ug/kg ND 330 05/27/14 09:52
Benzo(a)anthracene ug/kg ND 330 05/27/14 09:52
Benzo(a)pyrene ug/kg ND 330 05/27/14 09:52
Benzo(b)fluoranthene ug/kg ND 330 05/27/14 09:52
Benzo(g,h,i)perylene ug/kg ND 330 05/27/14 09:52
Benzo(k)fluoranthene ug/kg ND 330 05/27/14 09:52
Benzoic Acid ug/kg ND 1650 05/27/14 09:52
Benzyl alcohol ug/kg ND 660 05/27/14 09:52
bis(2-Chloroethoxy)methane ug/kg ND 330 05/27/14 09:52
bis(2-Chloroethyl) ether ug/kg ND 330 05/27/14 09:52
bis(2-Chloroisopropyl) ether ug/kg ND 330 05/27/14 09:52
bis(2-Ethylhexyl)phthalate ug/kg ND 330 05/27/14 09:52
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Page 14 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92202395
FLEMING LABS
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1206172
Associated Lab Samples:92202395001
Matrix:Solid
Analyzed
Butylbenzylphthalate ug/kg ND 330 05/27/14 09:52
Chrysene ug/kg ND 330 05/27/14 09:52
Di-n-butylphthalate ug/kg ND 330 05/27/14 09:52
Di-n-octylphthalate ug/kg ND 330 05/27/14 09:52
Dibenz(a,h)anthracene ug/kg ND 330 05/27/14 09:52
Dibenzofuran ug/kg ND 330 05/27/14 09:52
Diethylphthalate ug/kg ND 330 05/27/14 09:52
Dimethylphthalate ug/kg ND 330 05/27/14 09:52
Fluoranthene ug/kg ND 330 05/27/14 09:52
Fluorene ug/kg ND 330 05/27/14 09:52
Hexachloro-1,3-butadiene ug/kg ND 330 05/27/14 09:52
Hexachlorobenzene ug/kg ND 330 05/27/14 09:52
Hexachlorocyclopentadiene ug/kg ND 330 05/27/14 09:52
Hexachloroethane ug/kg ND 330 05/27/14 09:52
Indeno(1,2,3-cd)pyrene ug/kg ND 330 05/27/14 09:52
Isophorone ug/kg ND 330 05/27/14 09:52
N-Nitroso-di-n-propylamine ug/kg ND 330 05/27/14 09:52
N-Nitrosodimethylamine ug/kg ND 330 05/27/14 09:52
N-Nitrosodiphenylamine ug/kg ND 330 05/27/14 09:52
Naphthalene ug/kg ND 330 05/27/14 09:52
Nitrobenzene ug/kg ND 330 05/27/14 09:52
Pentachlorophenol ug/kg ND 1650 05/27/14 09:52
Phenanthrene ug/kg ND 330 05/27/14 09:52
Phenol ug/kg ND 330 05/27/14 09:52
Pyrene ug/kg ND 330 05/27/14 09:52
2,4,6-Tribromophenol (S)%59 27-110 05/27/14 09:52
2-Fluorobiphenyl (S)%70 30-110 05/27/14 09:52
2-Fluorophenol (S)%61 13-110 05/27/14 09:52
Nitrobenzene-d5 (S)%86 23-110 05/27/14 09:52
Phenol-d6 (S)%60 22-110 05/27/14 09:52
Terphenyl-d14 (S)%92 28-110 05/27/14 09:52
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1206173LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 14201670 85 39-101
1,2-Dichlorobenzene ug/kg 13201670 79 36-110
1,3-Dichlorobenzene ug/kg 13101670 78 35-110
1,4-Dichlorobenzene ug/kg 13401670 80 35-110
1-Methylnaphthalene ug/kg 12501670 75 45-105
2,4,5-Trichlorophenol ug/kg 14501670 87 48-109
2,4,6-Trichlorophenol ug/kg 14101670 85 45-111
2,4-Dichlorophenol ug/kg 14301670 86 51-116
2,4-Dimethylphenol ug/kg 13501670 81 42-103
2,4-Dinitrophenol ug/kg 74508330 89 28-103
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 05/27/2014 11:29 AM
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[phone]
Page 15 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92202395
FLEMING LABS
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1206173LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dinitrotoluene ug/kg 17301670 104 46-114
2,6-Dinitrotoluene ug/kg 17501670 105 48-112
2-Chloronaphthalene ug/kg 13301670 80 44-105
2-Chlorophenol ug/kg 13601670 82 36-110
2-Methylnaphthalene ug/kg 13101670 78 39-112
2-Methylphenol(o-Cresol)ug/kg 14001670 84 39-101
2-Nitroaniline ug/kg 36203330 109 44-111
2-Nitrophenol ug/kg 16701670 100 41-100
3&4-Methylphenol(m&p Cresol)ug/kg 13901670 83 43-103
3,3'-Dichlorobenzidine ug/kg 25203330 75 10-150
3-Nitroaniline ug/kg 29803330 89 35-110
4,6-Dinitro-2-methylphenol ug/kg 31903330 96 38-118
4-Bromophenylphenyl ether ug/kg 13501670 81 47-115
4-Chloro-3-methylphenol ug/kg 28803330 86 43-127
4-Chloroaniline ug/kg 27803330 83 34-109
4-Chlorophenylphenyl ether ug/kg 13701670 82 44-115
4-Nitroaniline ug/kg 31103330 93 37-111
4-Nitrophenol ug/kg 86508330 104 21-152
Acenaphthene ug/kg 12501670 75 38-117
Acenaphthylene ug/kg 12701670 76 46-107
Aniline ug/kg 13601670 81 29-110
Anthracene ug/kg 13701670 82 50-110
Benzo(a)anthracene ug/kg 13101670 78 47-116
Benzo(a)pyrene ug/kg 14201670 85 47-106
Benzo(b)fluoranthene ug/kg 13801670 83 47-109
Benzo(g,h,i)perylene ug/kg 10801670 65 39-115
Benzo(k)fluoranthene ug/kg 13101670 79 45-117
Benzoic Acid ug/kg 50408330 60 16-110
Benzyl alcohol ug/kg 29603330 89 38-105
bis(2-Chloroethoxy)methane ug/kg 14101670 85 39-110
bis(2-Chloroethyl) ether ug/kg 13601670 82 19-119
bis(2-Chloroisopropyl) ether ug/kg 13901670 83 21-110
bis(2-Ethylhexyl)phthalate ug/kg 13801670 83 35-116
Butylbenzylphthalate ug/kg 14101670 84 38-110
Chrysene ug/kg 13101670 79 49-110
Di-n-butylphthalate ug/kg 12601670 76 43-109
Di-n-octylphthalate ug/kg 13901670 83 37-109
Dibenz(a,h)anthracene ug/kg 11201670 67 43-116
Dibenzofuran ug/kg 14001670 84 45-106
Diethylphthalate ug/kg 12301670 74 41-114
Dimethylphthalate ug/kg 13401670 80 43-110
Fluoranthene ug/kg 14201670 85 50-114
Fluorene ug/kg 13701670 82 46-114
Hexachloro-1,3-butadiene ug/kg 14601670 88 28-111
Hexachlorobenzene ug/kg 13301670 80 46-120
Hexachlorocyclopentadiene ug/kg 15601670 94 18-119
Hexachloroethane ug/kg 14601670 87 33-110
Indeno(1,2,3-cd)pyrene ug/kg 8951670 54 42-115
REPORT OF LABORATORY ANALYSIS
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Page 16 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92202395
FLEMING LABS
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1206173LABORATORY CONTROL SAMPLE:
LCSSpike
Isophorone ug/kg 16801670 101 44-109
N-Nitroso-di-n-propylamine ug/kg 14001670 84 43-104
N-Nitrosodimethylamine ug/kg 10301670 62 29-110
N-Nitrosodiphenylamine ug/kg 11001670 66 48-113
Naphthalene ug/kg 12601670 76 41-110
Nitrobenzene ug/kg 1840 L3167011138-110
Pentachlorophenol ug/kg 25703330 77 32-128
Phenanthrene ug/kg 13401670 80 50-110
Phenol ug/kg 15001670 90 28-106
Pyrene ug/kg 13501670 81 45-114
2,4,6-Tribromophenol (S)%91 27-110
2-Fluorobiphenyl (S)%80 30-110
2-Fluorophenol (S)%78 13-110
Nitrobenzene-d5 (S)%100 23-110
Phenol-d6 (S)%85 22-110
Terphenyl-d14 (S)%86 28-110
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 17 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92202395
FLEMING LABS
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/6603
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92202395001
Parameter Units
Dup
Result QualifiersRPDResult
92201832003
1205512SAMPLE DUPLICATE:
Percent Moisture %16.7 016.8
Parameter Units
Dup
Result QualifiersRPDResult
92200734001
1205655SAMPLE DUPLICATE:
Percent Moisture %20.8 421.6
REPORT OF LABORATORY ANALYSIS
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Page 18 of 22
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92202395
FLEMING LABS
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside the
laboratory's control limits. The result is estimated.F3
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.L3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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Page 19 of 22
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92202395
FLEMING LABS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92202395001 MPRP/16020 ICP/14486BERRHILL BORROW - 2 EPA 3050 EPA 6010
92202395001 MERP/6649 MERC/6404BERRHILL BORROW - 2 EPA 7471 EPA 7471
92202395001 OEXT/27888 MSSV/9155BERRHILL BORROW - 2 EPA 3546 EPA 8270
92202395001 MSV/26916BERRHILL BORROW - 2 EPA 8260
92202395001 PMST/6603BERRHILL BORROW - 2 ASTM D2974-87
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Appendix D
Site Redevelopment Plans