6013_GreenwayNorthMeckCDLF_20171010_GWMonReport_DIN28781

-i- Fall 2017 Water Quality Monitoring Report January 2018
TABLE OF CONTENTS

1.0 PURPOSE ...........................................................................................................................1
2.0 SITE DESCRIPTION AND BACKGROUND ................................................................2
3.0 RECENT MODIFICATIONS TO THE MONITORING SYSTEM ............................4
4.0 INTERIM ABATEMENT MEASURES .........................................................................5 4.1 Alternative Public Water Supply For Neighboring Residences ............................. 5 4.2 Mitigation of Landfill Gas – A Potential Source of Site Groundwater Impacts .................................................................................................................... 5
5.0 DESCRIPTION OF FIELD SAMPLING ACTIVITIES ...............................................6
5.1 Well Water Level Gauging ..................................................................................... 6 5.2 Well Purging ........................................................................................................... 6 5.3 Groundwater Sample Collection ............................................................................. 7
6.0 GROUNDWATER FLOW EVALUATION ...................................................................8
7.0 WATER SAMPLE ANALYTICAL PARAMETERS ....................................................9
8.0 SAMPLE ANALYTICAL DATA EVALUATION.......................................................10 8.1 Organic Analytes Detected at Concentrations Exceeding the 2L Standards ........ 10 8.2 Metal Analytes Detected at Concentrations Exceeding the 2L Standards ............ 11
8.3 Inorganic Leachate Indicator Parameters .............................................................. 11
8.4 Vinyl Chloride and Background Metals Demonstration Letters .......................... 12
9.0 CONCLUSIONS AND RECOMMENDATIONS .........................................................13 9.1 Conclusions ........................................................................................................... 13 10.2 Recommendations ................................................................................................. 14

LIST OF FIGURES Figure 1 – Site Location Map
Figure 2 – Site Map
Figure 3 – Groundwater Potentiometric Map Figure 4 – Landfill Gas Extract System LIST OF TABLES Table 1 – History of Water Level Gauging Data and Well Construction Details Table 2 – Summary of Recent Site Groundwater Analytical Detections Table 3 – History of Site Groundwater Analytical Detections Table 4 - Summary of Vertical Hydraulic Gradients

-ii- Fall 2017 Water Quality Monitoring Report January 2018
Table of Contents (continued)
Page ii
LIST OF APPENDICES Appendix A – Groundwater Sampling Field Logs
Appendix B - Laboratory Analytical Data Reports

-1- Fall 2017 Water Quality Monitoring Report January 2018

1.0 PURPOSE

On behalf of Greenway Waste Solutions at North Meck, LLC, Civil & Environmental Consultants,
Inc. (CEC) has prepared this Fall 2017 Semi-Annual Water Quality Monitoring Report for the
Closed Phase I Area at the subject landfill facility. This report describes the well gauging and field
sampling activities, and provides a summary of the site groundwater conditions and acquired
groundwater sample data.

-2- Fall 2017 Water Quality Monitoring Report January 2018

2.0 SITE DESCRIPTION AND BACKGROUND

Greenway Waste Solutions at North Meck, LLC (GWS) operates the subject landfill under Solid
Waste Facility Permit Number 60-13. The facility address is 15300 Holbrooks Road, Huntersville,
North Carolina. The Closed Phase I C&D disposal area (Closed Phase I Area) is located in the
southern portion of the site and is bounded by an unnamed tributary of Cane Creek to the north
with other landfill disposal areas further to the north, private property to the west, and land owned
by Mecklenburg County to the east. Adjacent land parcels to the south and southeast of the Closed
Phase I Area are developed with single-family residences. Some adjacent parcels to the south and
southeast have been recently purchased by GWS. Cane Creek lies south and southeast of the
adjacent private properties on the south side of the closed landfill. The Closed Phase I Area
comprises approximately 23.3 acres. Waste placement in this disposal area generally occurred
during the years 1993 to 2002. It has been reported that the eastern and southern margins of this
disposal area contain buried land-clearing debris approximately 30-40 feet wide and 20-30 feet
deep. A Site Map is attached as Figure 1.

Routine semi-annual groundwater monitoring has been conducted at the landfill since June 1996.
The approximate locations of monitoring wells are shown on Figure 2. During the October 2012
monitoring event, VOCs were reported at concentrations exceeding the groundwater quality
standards as defined by Title 15A North Carolina Administrative Code Subchapter 02L
Groundwater Classifications and Standards (2L Standards) in MW-5. On a more consistent basis
and concurrent with a change in the laboratory services provider (from Pace Analytical Services,
Inc. to Shealy Environmental Services, Inc.) as of the April 2013 and for subsequent semi-annual
monitoring events, VOCs (particularly vinyl chloride) were being reported in several detection
well samples at concentrations exceeding the 2L Standards. As a consequence, the North Carolina
Department of Environmental Quality (NCDEQ) – Solid Waste Section (SWS) required the
permittee to implement a program of groundwater assessment monitoring and to perform a
contaminant delineation investigation.

Due to the proximity of a few private residential water supply wells (now inactive) downgradient
of the landfill area, samples were collected from these wells. VOCs reported in the landfill

-3- Fall 2017 Water Quality Monitoring Report January 2018

monitoring wells were also reported in the former Gilkerson residence well. The Gilkerson and
other neighboring water supply wells were made inactive and these residences connected to a
public water supply. GWS has purchased the former Gilkerson and Wright parcels.

-4- Fall 2017 Water Quality Monitoring Report January 2018

3.0 RECENT MODIFICATIONS TO THE MONITORING SYSTEM

The SWS requested that the facility owner perform a characterization of the nature and extent of
the groundwater contamination in the Closed Phase I Area. The SWS’s request was made in
response to the reports of vinyl chloride (VC) at concentrations above the 2L Standards in several
detection monitoring wells at the subject landfill as reported in July 2013.

The facility owner has been conducting an on-going contaminant delineation since September
2013, which has included the following activities:

1) Installation of 12 additional assessment monitoring wells (MW-4A, MW-4D, MW-5D,
MW-6D, MW-7A, MW-7D, MW-8D, MW-10D, MW-11A, MW-11B, MW-11D-1,
and MW-11D-2) in September 2013 to further delineate the vertical extent of impacted groundwater; 2) Installation of two additional deep bedrock monitoring wells (MW-4D-1 and MW-6D-
1) in May 2014 to delineate the vertical extent of impacted groundwater at the southern
and southeastern perimeter of the Closed Phase I Area; 3) Groundwater assessment monitoring wells installed after 2013 and three off-site inactive private water supply wells have been routinely monitored and sampled along
with the originally permitted groundwater detection monitoring wells for the Appendix
I parameter list; 4) Installation of four landfill gas probes and subsequent gas sampling to evaluate the potential for landfill gas to impact site groundwater; and

5) Analytical leachate/landfill gas ‟indicator” parameters including alkalinity, chloride, iron, manganese, sulfate, and total dissolved solids are being evaluated to characterize the source of the groundwater impacts.

-5- Fall 2017 Water Quality Monitoring Report January 2018

4.0 INTERIM ABATEMENT MEASURES

4.1 ALTERNATIVE PUBLIC WATER SUPPLY FOR NEIGHBORING RESIDENCES

Private residential supply wells located hydraulically down-gradient of the Closed Phase I Area
have been made inactive (see Figure 2). These residences have been connected to a public water
system. Moreover, the landfill owner has recently purchased the former Gilkerson and Wright
parcels situated in this area.

4.2 MITIGATION OF LANDFILL GAS – A POTENTIAL SOURCE OF SITE
GROUNDWATER IMPACTS

GWS engaged CEC to design, construct, and implement a landfill (LFG) extraction well system
to mitigate LFG migration at the Closed Phase I Area. The system consists of 15 perimeter LFG
extraction wells, three LFG extraction wells placed in the waste mass, a blower and LFG collection
piping and appurtenances. The approximate locations of LFG extraction wells are depicted on Figure
3. This system was made operational on April 2, 2015, and has been operated continually since
except for brief down-time due to electrical outages. Initially, the extraction wells exhibited positive
pressure buildup in all extraction wells, which can cause LFG migration. Since system startup, the
positive pressure in the extraction wells has been reduced and all wells are now performing at a
negative pressure (vacuum) at each well. Methane concentrations have not been detected during
recent perimeter LFG well monitoring at the Closed Phase I Area. Further, non-methane VOCs (i.e.,
VC) in the gas phase are also being removed by the LFG extraction system, which should ultimately
reduce a significant VOC source of groundwater impacts at the subject landfill.

-6- Fall 2017 Water Quality Monitoring Report January 2018

5.0 DESCRIPTION OF FIELD SAMPLING ACTIVITIES

Field activities associated with the Fall 2017 semi-annual groundwater monitoring were conducted
by CEC personnel from October 10 – October 13, 2017. Project oversight was provided by an
NC-licensed geologist. Well water levels were gauged, static well water was purged, and
groundwater samples were collected from 23 monitoring wells including shallow wells MW-1,
MW-4, MW-4A, MW-5, MW-6, MW-7A, MW-8, MW-9, MW-10, MW-11A, and MW-11B, and
deeper wells MW-4D, MW-4D-1, MW-5D, MW-6D, MW-6D-1, MW-7, MW-7D, MW-8D, MW-
10D, MW-11, MW-11D-1, and MW-11D-2. Also, groundwater samples were collected from three
off-site inactive private water supply wells (former Gilkerson, Hammill, and Tinsley residential
wells) situated adjacent to the southern perimeter of the Closed Phase I Area. The approximate
locations of these monitoring points are shown on Figure 2.

5.1 WELL WATER LEVEL GAUGING

Prior to well purging/sampling, the water level in each monitoring well was gauged using an
electronic water level meter. The depth-to-groundwater as measured from a reference point on the
top-of-casing was recorded to the nearest 0.01-inch on the well sampling field log (see Appendix
A). The water level probe was decontaminated between well measurements.

5.2 WELL PURGING

Where the water table was shallow a peristaltic pump was utilized to purge the well at a low-flow
rate until targeted analytical parameters were found to stabilize. During the well purge, specific
conductance, pH, dissolved oxygen, and oxidation-reduction potential were frequently measured
with a YSI 556 Water Quality Meter in a flow-through cell to observe and document the chemical
stability of the formation water entering the monitoring well. When parameter values indicated
stable water chemistry as defined by USEPA Groundwater Sampling Guidelines for Superfund
and RCRA Project Managers (EPA 542-S-02-001, May 2002), the well purge was considered
complete and groundwater samples were then collected. Well purge data were recorded on the
well sampling field logs provided in Appendix A.

-7- Fall 2017 Water Quality Monitoring Report January 2018

Where the water table was too deep to effectively use a low-flow peristaltic pump, a clean
Monsoon submersible pump was employed to purge wells MW-4, MW-4A, MW-4D, MW-4D-1,
MW-6, MW-6D, MW-6D-1, MW-7, MW-7A, MW-7D, MW-8, MW-8D, MW-10D, and MW-11
until targeted analytical parameters stabilized. The submersible pump intake was maintained
above each well screen provided that the well was adequately recharged during the well purge.
The pump was cleaned and new tubing was attached between wells.

5.3 GROUNDWATER SAMPLE COLLECTION

Following the above-described well purging procedures, groundwater samples were collected
from each well employing either the same low-flow pumping protocols for the shallow wells or
utilizing a submersible pump. Groundwater samples were collected in laboratory-supplied sample
containers that were labeled and packed on ice in insulated coolers, which were then shipped
overnight by FedEx to the selected analytical laboratory under chain-of-custody protocol.

-8- Fall 2017 Water Quality Monitoring Report January 2018

6.0 GROUNDWATER FLOW EVALUATION

A depth-to-water level measurement was performed relative to the top-of-well casing in each
groundwater monitoring well prior to well purging. A water level elevation was calculated by
subtracting the depth-to-water from the respective surveyed top-of-well casing elevation datum.
Monitoring well gauging data are summarized in Table 1.

Calculated water table elevations were used to prepare the Fall 2017 groundwater potentiometric
map presented in Figure 3. Shallow groundwater movement across the Closed Phase I Area is
radial; northward toward the tributary creek situated to the north and eastward or southward toward
Cane Creek situated to the south. The "V″-shaped potentiometric contours in the vicinity of the
tributary creek are indicative of shallow groundwater discharge from the Closed Phase I Area as
well as from the adjacent Infill Area situated on the north side of the tributary creek. An upward
vertical gradient of 0.026 feet/foot was calculated for well cluster MW-5/5D located south of the
tributary creek indicating groundwater recharge to the tributary in this site area. Also, upward
vertical hydraulic gradients were calculated for well clusters MW-4A/4D, MW-11A/11D-1, and
MW-11B/MW-11D-2 that are located in the southern half of the Closed Phase I Area in the vicinity
of Cane Creek. These data indicate local groundwater recharge to Cane Creek. A downward
vertical gradient was determined for MW-6/6D located at the southeastern perimeter of the landfill
and approximately 300 feet from Cane Creek. A summary table for vertical hydraulic gradients is
presented in Table 4.

-9- Fall 2017 Water Quality Monitoring Report January 2018

7.0 WATER SAMPLE ANALYTICAL PARAMETERS

For the routine Fall 2017 semi-annual monitoring event, groundwater samples were collected from
23 monitoring wells and three water supply wells that were submitted to TestAmerica laboratory
for analytical testing for the following parameters:

Appendix I Volatile Organic Compounds (VOCs) plus Tetrahydrofuran (THF) [EPA 8260B]
Appendix I Metals [EPA 200.8]

Monitoring well samples were also tested for leachate indicator parameters including the following
list:

Alkalinity [SM2320B]
Manganese [EPA 200.8]
Mercury [EPA 245.1]
Sulfate [EPA 9056A]
Calcium [EPA 200.8]
Chloride [9056A]
Iron [EPA 200.8]
Total Dissolved Solids (TDS) [SM2540C]

A quality control trip blank was analyzed for Appendix I VOCs plus tetrahydrofuran.

In addition to routine semi-annual sample collection at the Closed Phase I Area, CEC personnel
collected a split sample from well MW-5D that was submitted to Pace for VOC analyses.

-10- Fall 2017 Water Quality Monitoring Report January 2018

8.0 SAMPLE ANALYTICAL DATA EVALUATION

Laboratory analytical data reports for the Fall 2017 semi-annual monitoring event are provided in
Appendix B. Summaries of Appendix I VOCs, Appendix I metals, and inorganic analytes detected
in the collected water samples at concentrations above their respective laboratory reporting limits
are provided in Table 2. A historical summary of analytes detected in groundwater samples at
concentrations above their respective laboratory reporting limits are provided in Table 3.

8.1 ORGANIC ANALYTES DETECTED AT CONCENTRATIONS EXCEEDING THE 2L STANDARDS
For the October 2017 monitoring event, VC was detected at 1.8 µg/L in interior well MW-1 and
at 1.3 and 1.8 µg/L in interior well cluster MW-5/MW-5D, respectively. The 2L Standard for VC
is 0.03 µg/L. Benzene was observed at 1.1 µg/L at perimeter well MW-4, at 1.4 µg/L at perimeter
well MW-6D-1, and at 3.2 µg/L in interior well MW-10D. The 2L Standard for benzene is 1.0
µg/L.

The sampled inactive water supply wells are located off-site to the south and southeast of the
Closed Phase I Area. Trihalomethanes including bromodichloromethane and
dibromochloromethane were detected in both the inactive Gilkerson and Tinsley supply wells at
concentrations exceeding their 2L Standards. These compounds are commonly formed at relative
low concentrations as a by-product of treating water with chlorine-based disinfectants and
subsequent interaction with natural organics present in the water. Trihalomethanes have not been
typically detected in the on-site groundwater samples.

Tetrahydrofuran (THF) was detected at 230 µg/L in the Hammill well sample. Although the North
Carolina Occupational and Environmental Epidemiology Branch previously established a health-
based standard for THF of 700 µg/L, there is currently no 2L Standard due to the lack of historical
toxicological data necessary to promulgate regulatory standards. THF was previously detected at
26 µg/L in the Hammill well sample in April 2016.

-11- Fall 2017 Water Quality Monitoring Report January 2018

8.2 METAL ANALYTES DETECTED AT CONCENTRATIONS EXCEEDING THE 2L STANDARDS

As highlighted in Table 2, the laboratory test results for the monitoring event show that iron and
manganese exceed the 2L Standards in the majority of the landfill monitoring well samples. Iron
and manganese are naturally occurring metals in the local formation and can occur at elevated
levels in reduced groundwater conditions such as those encountered at the subject landfill.
Chromium, cobalt and vanadium were detected in several wells at concentrations exceeding their
respective 2L Standards; however, the detected range of these analyte concentrations appears to
be well within their naturally occurring levels. Copper was detected at 1.8 mg/L in MW-10D and
nickel was detected at 0.47 mg/L in MW-8; both analyte concentrations were elevated and
exceeded their respective 2L Standards. Elevated copper and nickel were reported for these
respective wells once before; however, these trends are not persistent.

8.3 INORGANIC LEACHATE INDICATOR PARAMETERS

The detections of inorganic parameters are summarized in Table 2. The levels of total dissolved
solids (TDS) exceeded its 2L Standard of 500 mg/L in wells MW-1, MW-5, MW-5D, MW-6,
MW-6D, MW-6D-1, MW-7, MW-8D, MW-10, MW-10D, MW-11 and the Hammill WSW.
Alkalinity and chloride appear to be elevated in wells MW-5, MW-5D, MW-6, MW-6D, MW-6D-
1, MW-7, MW-8D, MW-10D, and MW-11. Sulfate exceeds the 2L standard of 250 mg/L in the
Hammill WSW.

It is important to note that elevated TDS was observed in upgradient background wells MW-1 and
MW-10 and cross-gradient well MW-2. Also, elevated chloride was observed in upgradient
background well MW-1. Accordingly, CEC is currently evaluating available monitoring data for
the closed Mecklenburg County Holbrooks Road Landfill facility, which lies adjacent and north
of the subject landfill, to assess the potential for leachate migration beneath the subject landfill
from this adjacent off-site MSW landfill.

-12- Fall 2017 Water Quality Monitoring Report January 2018

8.4 VINYL CHLORIDE AND BACKGROUND METALS DEMONSTRATION LETTERS

In Spring 2017, per 15A NCAC 13B .0544 (b) (1) (I), on behalf of Greenway Waste Solutions at
North Meck, LLC, CEC prepared and submitted letters under separate cover to the NCDEQ-SWS
Compliance Unit presenting historical data and recent technical findings regarding the laboratory
detections of VC and on the presence of background metals in the groundwater underlying the landfill.
Both letters present and discuss data on laboratory error in falsely reporting VC due to the Freon
conversion and on the presence of naturally occurring metals in geology and hydrogeology at the
landfill.

Regarding the SWS Compliance Unit’s review of the Demonstration Letter on Laboratory Analyses
for Vinyl Chloride, they issued a letter (DIN 28701) dated December 19, 2017 noting that prior to Fall
2016 laboratory error may have resulting in the false inflation or detection of VC in several landfill
monitoring wells; however, maintaining that the laboratory data still indicate exceedances of vinyl
chloride above the 2L Standard in violation of NC groundwater rules. The SWS Compliance Unit
did not acknowledge that more recent and more accurate laboratory data for VC indicate that
significantly fewer facility monitoring wells are non-compliant with regard to VC levels and that
several non-compliant wells occur in the interior areas of the landfill facility. Further, the SWS
Compliance Unit stated that the proposed updated Water Quality Monitoring Plan (DIN 28684),
which proposes to unify the groundwater monitoring approach for the entire landfill facility utilizing
designated point of compliance groundwater monitoring wells, is currently under Section review.

Regarding the SWS Compliance Unit’s review of the Demonstration Letter on Background Metals
in Groundwater, they issued a letter (DIN 28645) dated December 19, 2017 requesting that additional
information be submitted in an Alternate Source Demonstration Addendum. In response, CEC will
prepare the requested addendum study on behalf of GWS and will submit the addendum within 120
days of receipt of the aforementioned letter.

-13- Fall 2017 Water Quality Monitoring Report January 2018

9.0 CONCLUSIONS AND RECOMMENDATIONS

9.1 CONCLUSIONS

Routine field activities associated with the Fall 2017 semi-annual groundwater monitoring were
conducted by CEC personnel from October 10 – October 13, 2017. Well water levels were gauged,
static well water was purged, and groundwater samples were collected from 23 monitoring wells
including shallow wells MW-1, MW-4, MW-4A, MW-5, MW-6, MW-7A, MW-8, MW-9, MW-
10, MW-11A, and MW-11B, and deeper wells MW-4D, MW-4D-1, MW-5D, MW-6D, MW-6D-
1, MW-7, MW-7D, MW-8D, MW-10D, MW-11, MW-11D-1, and MW-11D-2.

Also, groundwater samples were collected from three off-site inactive private water supply wells
(former Gilkerson, Hammill, and Tinsley residential wells) situated adjacent to the southern
perimeter of the Closed Phase I Area.

Vinyl chloride was detected at 1.8 µg/L in interior well MW-1 and at 1.3 and 1.8 µg/L in interior
well pair cluster MW-5/MW-5D, respectively. The 2L Standard for vinyl chloride is 0.03 µg/L.
Benzene was observed at 1.1 µg/L at perimeter well MW-4, at 1.4 µg/L at perimeter well MW-
6D-1, and at 3.2 µg/L in interior well MW-10D. The 2L Standard for benzene is 1.0 µg/L.

Trihalomethanes including bromodichloromethane and dibromochloromethane were detected in
both the inactive Gilkerson and Tinsley supply wells at concentrations exceeding their 2L
Standards. These compounds are commonly formed at relative low concentrations as a by-product
of treating water with chlorine-based disinfectants and subsequent interaction with natural organics
present in the water. Trihalomethanes have not been typically detected in the on-site groundwater
samples.

Iron and manganese exceed the 2L Standards in the majority of the landfill monitoring well
samples. Iron and manganese are naturally occurring metals in the local formation and can occur
at elevated levels in reduced groundwater conditions such as those encountered at the subject
landfill. Chromium, cobalt and vanadium were detected in several wells at concentrations

-14- Fall 2017 Water Quality Monitoring Report January 2018

exceeding their respective 2L Standards; however, the detected range of these analyte
concentrations appears to be well within their naturally occurring levels. Copper was detected at
1.8 mg/L in MW-10D and nickel was detected at 0.47 mg/L in MW-8; both analyte concentrations
were elevated and exceeded their respective 2L Standards. Elevated copper and nickel were
reported for these respective wells once before; however, these trends are not persistent.

The 2L Standard for total dissolved solids (TDS) was exceeded in well samples MW-1, MW-5,
MW-5D, MW-6, MW-6D, MW-6D-1, MW-7, MW-8D, MW-10, MW-10D, MW-11, and the
Hammill WSW. Alkalinity and chloride appear to be elevated in wells MW-5, MW-5D, MW-6,
MW-6D, MW-6D-1, MW-7, MW-8D, MW-10D, and MW-11. Sulfate exceeds the 2L standard of
250 mg/L in the Hammill WSW. It is important to note that elevated TDS was observed in
upgradient background wells MW-1 and MW-10 and cross-gradient well MW-2. Also, elevated
chloride was observed in upgradient background well MW-1.

10.2 RECOMMENDATIONS

The presence and/or persistence of elevated copper in MW-10D and elevated nickel in MW-8
should be confirmed or dismissed by subsequent sample collection before further consideration.

To minimize sampling artifacts and validate certain metals and inorganic parameter data, CEC will
carefully monitor turbidity in the site monitoring wells during the well purge process. CEC will
make an effort to minimize turbidity prior to collecting well samples.

FIGURES

REFERENCE
DATE:DWG SCALE:
DRAWN BY:CHECKED BY:APPROVED BY:
PROJECT NO:
FIGURE NO.:
SITE LOCATION MAP
111-370.0011"=1000'AUGUST 2017
PNP EHS EHS 1
NORTH MECKLENBURG C&D LANDFILL
GREENWAY WASTE SOLUTIONS OF
NORTH MECK, LLC
www.cecinc.com
1900 Center Park Drive - Suite A - Charlotte, NC 28217
Ph: 980.237.0373 · Fax: [phone]
NORTH
DATE:DWG SCALE:
DRAWN BY:CHECKED BY:APPROVED BY:
PROJECT NO:
FIGURE NO.:
SITE MAP

111-370.0011" = 400'DECEMBER 2017
JKS PNP EHS 2
GREENWAY WASTE SOLUTIONS OF
NORTH MECK, LCC
NORTH MECKLENBURG LANDFILL
HUNTERSVILLE, NORTH CAROLINA
REFERENCE www.cecinc.com
1900 Center Park Drive - Suite A - Charlotte, NC 28217
Ph: 980.237.0373 · Fax: [phone]
NORTH
LEGEND
8
A
B
34567 12
C
D
E
F
G
H
8 34567 12
A
B
C
D
E
F
G
H
DESCRIPTIONDATENOREVISION RECORD333 Baldwin Road · Pittsburgh, PA 15205412-429-2324 · 800-365-2324www.cecinc.comDATE:DWG SCALE:DRAWN BY:CHECKED BY:APPROVED BY:PROJECT NO:FIGURE NO.2017 FALLGROUNDWATER POTENTIOMETRIC MAP111-370.0011" = 200'OCTOBER 2017CTHEHSSLB3GREENWAY WASTE SOLUTIONSAT NORTH MECK, LLCNORTH MECK LANDFILLHUNTERSVILLE, NCNORTH LEGEND
8AB3456712CDEFGH83456712ABCDEFGHDESCRIPTIONDATENO
REVISION RECORD
www.cecinc.com
1900 Center Park Drive - Suite A - Charlotte, NC 28217
Ph: 980.237.0373 · Fax: [phone]
DATE:
DWG SCALE:
DRAWN BY:
CHECKED BY:
APPROVED BY:
PROJECT NO:DRAWING NO.:LANDFILL GAS
EXTRACTION SYSTEM
111-370.001
1"=200'
MARCH 2017 CTH
NTB
SLB
GREENWAY WASTE SOLUTIONS
OF NORTH MECK, LLC
NORTH MECKLENBURG LANDFILL
HUNTERSVILLE, NC NORTHNORTH CAROLINABOARD OF EXAMINERSFOR ENGINEERS ANDSURVEYORS LICENSENO. C-3035REFERENCE4

TABLES

Table 1
History of Water Level Gauging Data and Well Construction Details
Fall 2017 Semi-Annual Groundwater Monitoring
North Meck Closed Phase I Area Landfill
CEC Project No. 111-370.001
Depth to
Water2
WT Elev.
(ft)
Depth to
Water2
WT Elev.
(ft)
Depth to
Water2
WT Elev.
(ft)
Depth to
Water2
WT Elev.
(ft)
MW-1 25 15-25 685.31 14.03 671.28 13.67 671.64 NM NM 13.89 671.42
MW-4 42 32-42 717.55 34.97 682.58 36 681.55 35.45 682.1 35.42 682.13
MW-4A 44 34-44 711.63 33.04 678.59 33.61 678.02 32.62 679.01 33.01 678.62
MW-4D 100 85-100 711.30 32.43 678.87 32.93 678.37 32.03 679.27 32.55 678.75
MW-4D-1 135 120-135 NM 32.90 NM 33.1 NM 32.41 NM 33.05 NM
MW-5 29 19-29 682.99 20.43 662.56 19.4 663.59 19.92 663.07 20.49 662.5
MW-5D 55 45-55 681.84 18.42 663.42 17.4 664.44 18.4 663.44 18.61 663.23
MW-6 67 57-67 738.25 59.22 679.03 57.64 680.61 56.76 681.49 58.44 679.81
MW-6D 95 80-95 737.90 58.51 679.39 58.29 679.61 57.88 680.02 58.71 679.19
MW-6D-1 160 145-160 NM 61.07 NM 58.88 NM 58.18 NM 58.82 NM
MW-7 85 70-85 738.27 53.98 684.29 59.8 678.47 53.48 684.79 52.89 685.38
MW-7A 60 50-60 727.52 43.00 684.52 44.02 683.5 43.65 683.87 43.1 684.42
MW-7D 110 95-110 727.36 45.39 681.97 45.34 682.02 45.7 681.66 44.9 682.46
MW-8 80 70-80 764.39 67.02 697.37 68.72 695.67 68.59 695.8 68.41 695.98
MW-8D 122 107-122 768.20 71.51 696.69 72.5 695.7 72.35 695.85 72 696.2
MW-9 25 15-25 706.30 19.17 687.13 16.84 689.46 NM NM 17.03 689.27
MW-10 25 15-25 696.81 18.25 678.56 17.08 679.73 17.5 679.31 17.88 678.93
MW-10D 65 55-65 726.77 43.56 683.21 41.71 685.06 41.66 685.11 42.83 683.94
MW-11 73 63-73 731.90 48.12 683.78 42.28 689.62 41.44 690.46 46.34 685.56
MW-11A 30 20-30 675.74 18.26 657.48 12.54 663.2 NM NM 16.23 659.51
MW-11B 27 17-27 673.24 15.87 657.37 4.52 668.72 NM NM 13.68 659.56
MW-11D-1 60 50-60 674.44 15.20 659.24 11.52 662.92 NM NM 14.91 659.53
MW-11D-2 40 30-40 673.92 15.42 658.50 10.61 663.31 NM NM 14.31 659.61
MW= Monitoring Well TOC= Top of Casing WT= Water Table (1) Measured in Ft Below Ground Surface
NM= Not Measured (2) Depth relative to TOC elevation
6/15/2017 10/9/2017
Well ID Well
Depth1
Screen
Interval1
TOC
Elev.
(ft)10/27/2016 4/28/2017
Table 2
Summary of Recent Site Groundwater and Private Wells Analytical Detections
Fall 2017 Semi-Annual Groundwater Monitoring
North Meck Closed Phase I Area Landfill
CEC Project No. 111-370.001
Constituent
NCDEQ
Standard
(mg/L) *
MW-1 MW-4 MW-4A MW-4D MW-4D-1 MW-5 MW-5D MW-5D (Dup.) MW-5D PACE MW-6 MW-6D MW-6D-1
10.10.17 10.10.17 10.10.17 10.10.17 10.10.17 10.10.17 10.10.17 10.10.17 10.10.17 10.10.17 10.10.17 10.10.17Acetone6<0.005 0.0057 <0.005 <0.005 <0.005 <0.005 0.0053 <0.005 <0.005 <0.005 <0.005 <0.005Arsenic0.01 0.001 0.0006 0.00030 0.00048 0.0036 <0.001 0.00049 <0.001 <0.001 0.0038 0.00035 0.0027
Barium 0.7 0.37 0.41 0.17 0.047 0.068 0.24 0.24 NA NA 0.22 0.27 0.38
Benzene 0.001 <0.0005 0.0011 <0.0005 <0.0005 <0.0005 0.00076 0.0007 0.00098 <0.0005 <0.0005 0.00066 0.0014
Beryllium**0.004 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 NA NA <0.001 <0.001 <0.001
Bromoform 0.004 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001
Bromodichloromethane 0.0006 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.0012-Butanone (MEK)4 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005Cadmium0.002 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 NA NA <0.0005 <0.0005 <0.0005Chloroform0.07 <0.002 <0.002 <0.002 <0.002 <0.002 <0.002 <0.002 <0.002 <0.002 <0.002 <0.002 <0.002
Chloroethane 3 <0.001 <0.001 <0.001 <0.001 <0.001 0.0017 0.0016 0.0021 0.0017 <0.001 <0.001 <0.001
Chromium 0.01 <0.005 0.0026 0.01 <0.005 0.0043 <0.005 <0.005 NA NA <0.005 0.0032 <0.005
Cobalt**0.001 0.0072 0.0049 0.0054 <0.001 <0.001 0.0016 0.0009 NA NA 0.0027 0.0033 0.0009
Copper 1 0.0068 0.0016 0.102 <0.002 0.0095 0.0012 0.0240 NA NA 0.0032 0.0035 0.0009
Carbon Disulfide 0.7 <0.002 <0.002 <0.002 <0.002 <0.002 <0.002 <0.002 NA NA <0.002 <0.002 <0.0021,1-Dichloroethane 0.006 <0.001 <0.001 0.00075 <0.001 0.00076 0.00098 0.0016 NA 0.0016 <0.001 <0.001 <0.0011,1-Dichloroethene 0.35 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 NA <0.001 <0.001 <0.001 <0.0011,4-Dichlorobenzene 0.006 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 NA <0.001 <0.001 <0.001 <0.001
cis-1,2-Dichloroethene 0.07 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 0.0018 0.0026 0.0025 <0.001 <0.001 <0.001
Dibromochloromethane 0.0004 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001
Ethylbenzene 0.6 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 NA <0.0005 <0.0005 <0.0005 <0.0005
Toluene 0.6 <0.0005 <0.0005 <0.0005 <0.0005 0.00038 <0.0005 <0.0005 NA <0.0005 <0.0005 <0.0005 <0.0005
Xylenes 0.5 <0.001 <0.001 <0.001 <0.001 0.00041 <0.001 <0.001 NA <0.001 <0.001 <0.001 <0.001Lead0.015 0.0029 0.0039 0.00017 <0.0005 <0.0005 <0.0005 <0.0005 NA <0.0005 0.0023 0.0002 <0.0005Manganese0.05 18 0.76 0.26 0.21 0.25 0.37 0.74 NA NA 1.5 6.9 0.355Mercury0.001 <0.0002 <0.0002 0.00043 <0.0002 <0.0002 <0.0002 <0.0002 NA NA <0.0002 <0.0002 <0.0002
Methylene Chloride 0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 NA <0.005 <0.005 <0.005 <0.005
Nickel 0.1 <0.002 0.0038 0.0065 <0.002 0.0023 0.0012 0.0085 NA NA 0.0023 0.0130 0.0121
Selenium 0.02 <0.0025 <0.0025 <0.0025 <0.0025 <0.0025 <0.0025 <0.0025 NA NA 0.0015 0.0012 <0.0025
Tetrahydrofuran NS <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 0.0150 NA 0.0234 <0.010 0.0480 0.0112
Thallium**0.0002 <0.002 <0.002 <0.002 <0.002 <0.002 <0.002 <0.002 NA NA <0.002 <0.002 <0.002
Vanadium**0.0003 <0.005 <0.005 0.0035 <0.005 0.0028 <0.005 0.0032 NA NA 0.0027 0.0033 0.0073Vinyl Chloride 0.00003 0.0018 <0.0005 <0.0005 <0.0005 <0.0005 0.0013 0.0018 0.0024 0.0024 <0.0005 <0.0005 <0.0005Zinc10.12 0.051 0.016 0.011 <0.02 <0.02 <0.02 NA NA 0.0160 0.0083 <0.02AlkalinityNS230300210140210450790NANA750780650
Iron 0.3 81 1.7 1.3 0.32 0.53 0.21 0.1600 NA NA 2.4 0.48 3.3
Total Dissolved Solids 500 280 400 330 180 250 690 1300 NA NA 910 960 700
Sulfate 250 34 10 12 7.8 1.3 100 190 NA NA 38 28 13
Chloride 250 3.1 19.0 11.0 5.9 8.9 42.0 91.0 NA NA 36.0 27.0 25.0
* NCDEQ Standard = 15A NCAC 02L .0202 Groundwater
Standards (Eff. April 1, 2013) ** Interim Maximum Allowable Concentration (IMAC) Bold/Yellow values exceed the NCDEQ Standard or IMAC
NS = Not Specified NA= Not Analyzed < "Reporting Limit" = Value is less that the Reporting Limit
Table 2 (cont.)
Summary of Recent Site Groundwater and Private Wells Analytical Detections
Fall 2017 Semi-Annual Groundwater Monitoring
North Meck Closed Phase I Area Landfill
CEC Project No. 111-370.001
Constituent
NCDEQ
Standard
(mg/L) *
Acetone 6Arsenic0.01
Barium 0.7
Benzene 0.001
Beryllium**0.004
Bromoform 0.004
Bromodichloromethane 0.00062-Butanone (MEK)4Cadmium0.002Chloroform0.07
Chloroethane 3
Chromium 0.01
Cobalt**0.001
Copper 1
Carbon Disulfide 0.71,1-Dichloroethane 0.0061,1-Dichloroethene 0.351,4-Dichlorobenzene 0.006
cis-1,2-Dichloroethene 0.07
Dibromochloromethane 0.0004
Ethylbenzene 0.6
Toluene 0.6
Xylenes 0.5Lead0.015Manganese0.05Mercury0.001
Methylene Chloride 0.005
Nickel 0.1
Selenium 0.02
Tetrahydrofuran NS
Thallium**0.0002Vanadium**0.0003Vinyl Chloride 0.00003Zinc1
Alkalinity NS
Iron 0.3
Total Dissolved Solids 500
Sulfate 250
Chloride 250
* NCDEQ Standard = 15A NCAC 02L .0202 Groundwater
Standards (Eff. April 1, 2013) ** Interim Maximum Allowable Concentration (IMAC) Bold/Yellow values exceed the NCDEQ Standard or IMAC
NS = Not Specified NA= Not Analyzed < "Reporting Limit" = Value is less that the Reporting Limit
MW-7 MW-7A MW-7D MW-8 MW-8D MW-9 MW-10 MW-10D MW-11 MW-11A MW-11B
10.10.17 10.10.17 10.10.17 10.11.17 10.11.17 10.10.17 10.10.17 10.11.17 10.11.17 10.10.17 10.10.17<0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005<0.001 0.00086 <0.001 0.0015 0.00015 <0.001 0.0013 0.0016 0.00052 <0.001 <0.001
0.33 0.34 0.22 0.14 0.11 0.054 0.24 0.21 0.27 0.039 0.085
<0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 0.0032 0.0009 <0.0005 <0.0005
<0.001 <0.001 <0.001 0.00064 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001
<0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001
<0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001<0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005<0.0005 <0.0005 <0.0005 0.00052 <0.0005 <0.0005 <0.0005 0.0031 0.00045 <0.0005 <0.0005<0.002 <0.002 <0.002 <0.002 <0.002 <0.002 <0.002 <0.002 <0.002 <0.002 <0.002
<0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001
0.0024 0.018 <0.005 0.013 0.013 <0.005 <0.005 0.0066 0.051 <0.005 <0.005
0.0007 0.00340 <0.001 0.0033 0.0033 <0.001 0.005 0.049 0.0031 <0.001 <0.001
0.002 0.00960 <0.002 0.11 0.0079 <0.002 <0.002 1.8 0.036 0.00071 0.0038
<0.002 <0.002 <0.002 <0.002 <0.002 <0.002 <0.002 <0.002 <0.002 <0.002 <0.002<0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001<0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001<0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 0.0018 <0.001 <0.001 <0.001
<0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001
<0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001
<0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005
<0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005
<0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001
<0.0005 0.00081 <0.0005 0.013 0.00074 <0.0005 <0.0005 0.0029 0.00076 <0.0005 <0.00050.31 0.12 0.0480 4.3 0.26 0.0019 4.1 17 2.5 0.0036 0.013<0.0002 0.00094 <0.0002 <0.0002 <0.0002 <0.0002 <0.0002 <0.0002 <0.0002 <0.0002 <0.0002<0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 0.0075 <0.005 <0.005 <0.005
0.0020 0.0110 <0.002 0.47 0.012 <0.002 <0.002 0.06 0.053 <0.002 <0.002
0.0013 0.0015 <0.0025 0.0023 <0.0025 <0.0025 <0.0025 0.0012 <0.0025 <0.0025 <0.0025
0.01000 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 0.081 0.017 <0.010 <0.010
<0.002 <0.002 <0.002 <0.002 <0.002 <0.002 <0.002 <0.002 <0.002 <0.002 <0.002
<0.005 0.015 <0.005 0.072 0.011 0.0022 <0.005 0.02 0.007 <0.005 <0.005<0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005<0.02 0.0190 <0.02 0.079 0.016 <0.02 <0.02 0.045 0.051 <0.02 <0.0244028034029040052380170011003850
0.16000 4.8 0.62 29 4.3 <0.1 60 2.7 0.75 <0.1 <0.1
560 410 480 420 570 180 510 2500 1400 120 110
35 22 26 46 15 15 0.78 140 96 11 16
25.0 38.0 40.0 12.0 82.0 24.0 25.0 200.0 51.0 3.4 3.6
Table 2 (cont.)
Summary of Recent Site Groundwater and Private Wells Analytical Detections
Fall 2017 Semi-Annual Groundwater Monitoring
North Meck Closed Phase I Area Landfill
CEC Project No. 111-370.001
Constituent
NCDEQ
Standard
(mg/L) *
Acetone 6Arsenic0.01
Barium 0.7
Benzene 0.001
Beryllium**0.004
Bromoform 0.004
Bromodichloromethane 0.00062-Butanone (MEK)4Cadmium0.002Chloroform0.07
Chloroethane 3
Chromium 0.01
Cobalt**0.001
Copper 1
Carbon Disulfide 0.71,1-Dichloroethane 0.0061,1-Dichloroethene 0.351,4-Dichlorobenzene 0.006
cis-1,2-Dichloroethene 0.07
Dibromochloromethane 0.0004
Ethylbenzene 0.6
Toluene 0.6
Xylenes 0.5Lead0.015Manganese0.05Mercury0.001
Methylene Chloride 0.005
Nickel 0.1
Selenium 0.02
Tetrahydrofuran NS
Thallium**0.0002Vanadium**0.0003Vinyl Chloride 0.00003Zinc1
Alkalinity NS
Iron 0.3
Total Dissolved Solids 500
Sulfate 250
Chloride 250
* NCDEQ Standard = 15A NCAC 02L .0202 Groundwater
Standards (Eff. April 1, 2013) ** Interim Maximum Allowable Concentration (IMAC) Bold/Yellow values exceed the NCDEQ Standard or IMAC
NS = Not Specified NA= Not Analyzed < "Reporting Limit" = Value is less that the Reporting Limit
MW-11D-1 MW-11D-2 Gilkerson WSW Hammill WSW Tinsley WSW
10.10.17 10.10.17 10.31.17 10.31.17 10.31.17<0.005 <0.005 <0.005 0.0065 <0.0050.00037 <0.001 0.00015 0.00047 0.00019
0.094 0.14 0.012 0.041 0.01
<0.0005 <0.0005 <0.0005 <0.0005 <0.0005
<0.001 <0.001 <0.001 <0.001 <0.001
<0.001 <0.001 <0.001 <0.001 0.00078
<0.001 <0.001 0.014 <0.001 0.014<0.005 <0.005 <0.005 0.022 <0.005<0.0005 <0.0005 <0.0005 <0.0005 <0.0005<0.002 <0.002 0.041 <0.002 0.042
<0.001 <0.001 <0.001 <0.001 <0.001
<0.005 <0.005 <0.005 <0.005 <0.005
<0.001 0.00032 <0.001 <0.001 <0.001
0.0097 0.005 0.0018 0.0043 0.0041
<0.002 <0.002 <0.002 <0.002 <0.002<0.001 <0.001 <0.001 <0.001 <0.001<0.001 <0.001 <0.001 <0.001 <0.001<0.001 <0.001 <0.001 <0.001 <0.001
<0.001 <0.001 <0.001 <0.001 <0.001
<0.001 <0.001 0.0076 <0.001 0.0069
<0.0005 <0.0005 <0.0005 <0.0005 <0.0005
<0.0005 <0.0005 <0.0005 <0.0005 <0.0005
<0.001 <0.001 <0.001 <0.001 <0.0010.00016 <0.0005 0.005 0.00028 <0.00050.0072 0.073 0.016 0.06 0.0016<0.0002 <0.0002 0.00029 <0.0002 <0.0002<0.005 <0.005 <0.005 <0.005 <0.005
<0.002 0.001 <0.002 0.00095 <0.002
<0.0025 <0.0025 <0.0025 <0.0025 <0.0025
<0.010 <0.010 <0.010 0.23 <0.010
<0.002 <0.002 <0.002 <0.002 <0.002
0.0025 <0.005 <0.005 <0.005 <0.005<0.0005 <0.0005 <0.0005 <0.0005 <0.00050.02 0.0092 0.032 0.49 <0.0229048219523
<0.1 <0.1 0.66 0.29 <0.1
400 100 62 600 66
34 10 8.9 320 31
18.0 3.2 9.5 5.6 35
Table 3History of Site Groundwater and Private Wells Analytical DetectionsFall 2017 Semi-Annual Groundwater Monitoring
North Meck Closed Phase I Area Landfill
CEC Project No. 111-370.001
Constituent NCDEQ Standard (mg/L) *
Sample Date -3.20.98 4.13.99 3.9.00 3.23.01 3.16.02 10.31.02 3.26.03 9.13.03 3.26.04 12.2.04 4.23.05 10.25.05 3.28.06 9.27.06 3.31.07 4.10.08
Acetone 6
Arsenic 0.01 0.0180
Barium 0.7 0.1 0.059 0.053 0.051 0.045 0.055 0.045 0.059 0.043 0.046 0.053 0.043Benzene0.001
Beryllium**NEBromodichloromethane0.0006
Bromoform 0.004
2-Butanone (MEK)4Cadmium0.002
Calcium NEChloroethane3
Chloroform 0.07
Chromium 0.01
Cobalt**0.001
Copper 1Carbon Disulfide 0.7
Dibromochloromethane 0.0004
1,1-Dichloroethane 0.006
1,1-Dichloroethene 0.35
1,4-Dichlorobenzene 0.006cis-1,2-Dichloroethene 0.07
bis (2-Ethylhexyl) phthalate 0.003
Ethylbenzene 0.6
Toluene 0.6
Xylenes 0.5Heptachlor0.000008
beta-BHC NE
Lead 0.015
Manganese 0.05
Mercury 0.001Methylene Chloride 0.005
Nickel 0.1
Selenium 0.02 0.031 0.0072
Sulfide NE
Tetrahydrofuran NEThallium**0.0002
Vanadium**0.0003
Vinyl Chloride 0.00003
Zinc 1
Alkalinity NEAmmonia-N 1.5
Iron 0.3
Total Dissolved Solids 500
Sulfate 250
Carbon Dioxide NE
Chloride 250
MW-1
* NCDEQ Standard = 15A NCAC 02L .0202 Groundwater Standards (Eff. April 1, 2013) ** Interim Maximum Allowable Concentration Bold /yellowvalues exceed the NCDEQ Standard N/E= Not Established = POC Wells
Table 3 (cont.)History of Site Groundwater and Private Wells Analytical DetectionsFall 2017 Semi-Annual Groundwater Monitoring
North Meck Closed Phase I Area Landfill
CEC Project No. 111-370.001
Constituent NCDEQ Standard (mg/L) *
Sample Date -
Acetone 6
Arsenic 0.01Barium0.7Benzene0.001
Beryllium**NEBromodichloromethane0.0006
Bromoform 0.004
2-Butanone (MEK)4Cadmium0.002
Calcium NEChloroethane3
Chloroform 0.07
Chromium 0.01
Cobalt**0.001
Copper 1Carbon Disulfide 0.7
Dibromochloromethane 0.0004
1,1-Dichloroethane 0.006
1,1-Dichloroethene 0.35
1,4-Dichlorobenzene 0.006cis-1,2-Dichloroethene 0.07
bis (2-Ethylhexyl) phthalate 0.003
Ethylbenzene 0.6
Toluene 0.6
Xylenes 0.5Heptachlor0.000008
beta-BHC NE
Lead 0.015
Manganese 0.05
Mercury 0.001Methylene Chloride 0.005
Nickel 0.1
Selenium 0.02
Sulfide NE
Tetrahydrofuran NEThallium**0.0002
Vanadium**0.0003
Vinyl Chloride 0.00003
Zinc 1
Alkalinity NEAmmonia-N 1.5
Iron 0.3
Total Dissolved Solids 500
Sulfate 250
Carbon Dioxide NE
Chloride 250
5.13.09 10.18.11 4.12.12 10.24.12 4.25.13 10.3.13 4.10.14 10.23.14 4.24.15 10.21.15 4.22.16 10.27.16 4.28.17 10.10.17 3.20.98 4.13.99
0.0026
0.0036 0.0131 0.012 0.01 0.0026 0.0013 0.001
0.0402 0.0252 0.193 0.12 0.071 0.065 0.11 0.077 0.46 0.081 0.0664 0.067 0.37
0.0016
0.00064
110 100 98.5
0.0086
0.0017 0.0072
0.0314 0.0073 0.067 0.0051 0.0068
0.0011
0.0013
0.016 0.00021 0.0029
4.5 3.2 2.96 21 18
0.0001
0.0067
0.0534 0.071 0.007
0.0015 0.00180.0457 0.02 0.043 0.031 0.2 0.011 0.12
348 289 330 370 370 396 290 2300.9 0.7 0.72
13.8 15 81
353 371 380 460 400 432 410 280
14.6 14.4 31 34.2 46 34
440 500
3.04 3.6 3.3 3.0 3.3 6 3.1
MW-1 cont.MW-4
* NCDEQ Standard = 15A NCAC 02L .0202 Groundwater Standards (Eff. April 1, 2013) ** Interim Maximum Allowable Concentration Bold /yellow values exceed the NCDEQ Standard N/E= Not Established = POC Wells
Table 3 (cont.)History of Site Groundwater and Private Wells Analytical DetectionsFall 2017 Semi-Annual Groundwater Monitoring
North Meck Closed Phase I Area Landfill
CEC Project No. 111-370.001
Constituent NCDEQ Standard (mg/L) *
Sample Date -
Acetone 6
Arsenic 0.01Barium0.7Benzene0.001
Beryllium**NEBromodichloromethane0.0006
Bromoform 0.004
2-Butanone (MEK)4Cadmium0.002
Calcium NEChloroethane3
Chloroform 0.07
Chromium 0.01
Cobalt**0.001
Copper 1Carbon Disulfide 0.7
Dibromochloromethane 0.0004
1,1-Dichloroethane 0.006
1,1-Dichloroethene 0.35
1,4-Dichlorobenzene 0.006cis-1,2-Dichloroethene 0.07
bis (2-Ethylhexyl) phthalate 0.003
Ethylbenzene 0.6
Toluene 0.6
Xylenes 0.5Heptachlor0.000008
beta-BHC NE
Lead 0.015
Manganese 0.05
Mercury 0.001Methylene Chloride 0.005
Nickel 0.1
Selenium 0.02
Sulfide NE
Tetrahydrofuran NEThallium**0.0002
Vanadium**0.0003
Vinyl Chloride 0.00003
Zinc 1
Alkalinity NEAmmonia-N 1.5
Iron 0.3
Total Dissolved Solids 500
Sulfate 250
Carbon Dioxide NE
Chloride 250
3.9.00 3.23.01 3.16.02 10.31.02 3.26.03 9.13.03 3.26.04 12.2.04 4.23.05 10.25.05 3.28.06 9.27.06 3.31.07 4.10.08 5.13.09 10.18.11 4.12.12
0.005
0.014 0.0032 0.0076
0.14 0.082 0.1 0.12 0.19 0.22 0.22 0.24 0.26 0.28 0.32 0.343 0.557
0.0004
0.0102
332
427
6.23
MW-4 cont.
* NCDEQ Standard = 15A NCAC 02L .0202 Groundwater Standards (Eff. April 1, 2013) ** Interim Maximum Allowable Concentration Bold /yellow values exceed the NCDEQ Standard N/E= Not Established = POC Wells
Table 3 (cont.)History of Site Groundwater and Private Wells Analytical DetectionsFall 2017 Semi-Annual Groundwater Monitoring
North Meck Closed Phase I Area Landfill
CEC Project No. 111-370.001
Constituent NCDEQ Standard (mg/L) *
Sample Date -
Acetone 6
Arsenic 0.01Barium0.7Benzene0.001
Beryllium**NEBromodichloromethane0.0006
Bromoform 0.004
2-Butanone (MEK)4Cadmium0.002
Calcium NEChloroethane3
Chloroform 0.07
Chromium 0.01
Cobalt**0.001
Copper 1Carbon Disulfide 0.7
Dibromochloromethane 0.0004
1,1-Dichloroethane 0.006
1,1-Dichloroethene 0.35
1,4-Dichlorobenzene 0.006cis-1,2-Dichloroethene 0.07
bis (2-Ethylhexyl) phthalate 0.003
Ethylbenzene 0.6
Toluene 0.6
Xylenes 0.5Heptachlor0.000008
beta-BHC NE
Lead 0.015
Manganese 0.05
Mercury 0.001Methylene Chloride 0.005
Nickel 0.1
Selenium 0.02
Sulfide NE
Tetrahydrofuran NEThallium**0.0002
Vanadium**0.0003
Vinyl Chloride 0.00003
Zinc 1
Alkalinity NEAmmonia-N 1.5
Iron 0.3
Total Dissolved Solids 500
Sulfate 250
Carbon Dioxide NE
Chloride 250
10.24.12 4.25.13 10.3.13 4.10.14 10.23.14 4.24.15 10.21.15 4.22.16 10.27.16 5.1.17 6.15.17 10.10.17 10.3.13 4.10.14 10.23.14
0.028 0.0058 0.0057
0.0019 0.0056 0.00062 0.00056
0.527 0.62 0.62 0.65 0.61 0.65 0.55 0.66 0.241 0.44 0.41 0.27 0.12 0.083
0.0011 0.00032 0.0011
0.00012
55 71 34.7
0.0061 0.008 0.0026 0.027
0.0117 0.018 0.019 0.006 0.0049
0.0059 0.019 0.02 0.0038 0.0016 0.0860.0017
0.00120.0017 0.0024
0.0027 0.0059 0.011 0.0039 0.026
3.3 3.5 1.39 0.82 0.76
0.00032
0.008 0.015 0.0093 0.0038
0.02 0.0025 0.068
0.0035 0.0071 0.0068 0.0070 0.0027 0.0012 0.014 0.0034 0.0034 0.0034
0.027 0.14 0.3 0.096 0.051 0.013 0.32 0.015
306 390 320 390 253 310 3001110.14
3.59 2.5 1.7
357 420 440 440 344 480 400
8 11.9 20 10
660 900
5.74 4.7 8.1 7.3 16 21 19.0
MW-4AMW-4 cont.
* NCDEQ Standard = 15A NCAC 02L .0202 Groundwater Standards (Eff. April 1, 2013) ** Interim Maximum Allowable Concentration Bold /yellowvalues exceed the NCDEQ Standard N/E= Not Established = POC Wells
Table 3 (cont.)History of Site Groundwater and Private Wells Analytical DetectionsFall 2017 Semi-Annual Groundwater Monitoring
North Meck Closed Phase I Area Landfill
CEC Project No. 111-370.001
Constituent NCDEQ Standard (mg/L) *
Sample Date -
Acetone 6
Arsenic 0.01Barium0.7Benzene0.001
Beryllium**NEBromodichloromethane0.0006
Bromoform 0.004
2-Butanone (MEK)4Cadmium0.002
Calcium NEChloroethane3
Chloroform 0.07
Chromium 0.01
Cobalt**0.001
Copper 1Carbon Disulfide 0.7
Dibromochloromethane 0.0004
1,1-Dichloroethane 0.006
1,1-Dichloroethene 0.35
1,4-Dichlorobenzene 0.006cis-1,2-Dichloroethene 0.07
bis (2-Ethylhexyl) phthalate 0.003
Ethylbenzene 0.6
Toluene 0.6
Xylenes 0.5Heptachlor0.000008
beta-BHC NE
Lead 0.015
Manganese 0.05
Mercury 0.001Methylene Chloride 0.005
Nickel 0.1
Selenium 0.02
Sulfide NE
Tetrahydrofuran NEThallium**0.0002
Vanadium**0.0003
Vinyl Chloride 0.00003
Zinc 1
Alkalinity NEAmmonia-N 1.5
Iron 0.3
Total Dissolved Solids 500
Sulfate 250
Carbon Dioxide NE
Chloride 250
4.24.15 10.21.15 4.22.16 10.27.16 5.1.17 6.15.17 10.10.17 10.3.13 4.10.14 10.23.14 4.24.15 10.21.15 4.22.16 10.27.16
0.00043 0.0003 0.0015 0.0012
0.11 0.11 0.068 0.246 0.16 0.17 0.086 0.089 0.14 0.11 0.14 0.11 0.05620.00035
0.00012
34 14 42.4 84 70 35.9
0.0099 0.0023 0.01 0.008
0.0054 0.00095 0.0054
0.0053 0.0037 0.102 0.0063 0.102 0.016 0.0013
0.00064 0.00054 0.00075 0.0024 0.0028 0.0028 0.0025 0.00130.0018 0.0014 0.0011 0.0026 0.0037 0.0014 0.0011
0.00150.003 0.0074
0.0039 0.0081 0.0011
0.0274 0.0015 0.000170.026 0.021 0.285 0.039 0.26 0.46 0.41 0.21
0.00025 0.0001 0.00043 0.0003 0.00048
0.0186 0.0036 0.0065 0.0066
0.0554 0.005 0.0035
0.0012 0.002 0.0037 0.0047 0.006 0.0069 0.0017 0.00065 0.00085
0.29 0.89 1.2 0.257 0.039 0.016 0.045 0.043 0.044 0.072
170 190 201 210 190 180 1320.17 0.82
21.3 1.7 1.3 0.285
280 280 273 320 330 270 230 18210.8 11 12 8.1
380 620 210 210
8.2 8.4 10 10 11.0 8.4 7.2 5.7
MW-4A (cont.)MW-4D
* NCDEQ Standard = 15A NCAC 02L .0202 Groundwater Standards (Eff. April 1, 2013) ** Interim Maximum Allowable Concentration Bold /yellowvalues exceed the NCDEQ Standard N/E= Not Established = POC Wells
Table 3 (cont.)History of Site Groundwater and Private Wells Analytical DetectionsFall 2017 Semi-Annual Groundwater Monitoring
North Meck Closed Phase I Area Landfill
CEC Project No. 111-370.001
Constituent NCDEQ Standard (mg/L) *
Sample Date -
Acetone 6
Arsenic 0.01Barium0.7Benzene0.001
Beryllium**NEBromodichloromethane0.0006
Bromoform 0.004
2-Butanone (MEK)4Cadmium0.002
Calcium NEChloroethane3
Chloroform 0.07
Chromium 0.01
Cobalt**0.001
Copper 1Carbon Disulfide 0.7
Dibromochloromethane 0.0004
1,1-Dichloroethane 0.006
1,1-Dichloroethene 0.35
1,4-Dichlorobenzene 0.006cis-1,2-Dichloroethene 0.07
bis (2-Ethylhexyl) phthalate 0.003
Ethylbenzene 0.6
Toluene 0.6
Xylenes 0.5Heptachlor0.000008
beta-BHC NE
Lead 0.015
Manganese 0.05
Mercury 0.001Methylene Chloride 0.005
Nickel 0.1
Selenium 0.02
Sulfide NE
Tetrahydrofuran NEThallium**0.0002
Vanadium**0.0003
Vinyl Chloride 0.00003
Zinc 1
Alkalinity NEAmmonia-N 1.5
Iron 0.3
Total Dissolved Solids 500
Sulfate 250
Carbon Dioxide NE
Chloride 250
5.1.17 6.15.17 10.10.17 10.23.14 4.24.15 10.21.15 4.22.16 10.27.16 5.1.17 6.15.17 10.10.17 3.20.98 4.13.99 3.9.00 3.23.01 3.16.02
0.00064 0.00048 0.0015 0.0017 0.0033 0.0036 0.024
0.05 0.047 0.03 0.031 0.032 0.045 0.0498 0.062 0.068 0.28 0.17 0.140.00046
0.014
37 44 42.4
0.0058 0.0043 0.006
0.0022
0.0013 0.00950.0096 0.0021
0.00055 0.0018 0.001 0.00072 0.00071 0.000760.0012 0.0015 0.0011
0.00038
0.0012 0.0012 0.00041
0.0012
0.28 0.21 0.03 0.18 0.194 0.21 0.25
0.0036 0.0023
0.0028
0.0011 0.0012 0.00076 0.0021
0.0087 0.011 0.011 0.016
140 140 150 190 187 200 2100.074
0.33 0.32 0.362 0.49 0.53
210 180 210 240 239 240 250
8.5 7.8 5.3 3 1.3
140 190
5.5 5.9 13 12 12 13 8.9
MW-5MW-4D cont.MW-4D-1
* NCDEQ Standard = 15A NCAC 02L .0202 Groundwater Standards (Eff. April 1, 2013) ** Interim Maximum Allowable Concentration Bold /yellowvalues exceed the NCDEQ Standard N/E= Not Established = POC Wells
Table 3 (cont.)History of Site Groundwater and Private Wells Analytical DetectionsFall 2017 Semi-Annual Groundwater Monitoring
North Meck Closed Phase I Area Landfill
CEC Project No. 111-370.001
Constituent NCDEQ Standard (mg/L) *
Sample Date -
Acetone 6
Arsenic 0.01Barium0.7Benzene0.001
Beryllium**NEBromodichloromethane0.0006
Bromoform 0.004
2-Butanone (MEK)4Cadmium0.002
Calcium NEChloroethane3
Chloroform 0.07
Chromium 0.01
Cobalt**0.001
Copper 1Carbon Disulfide 0.7
Dibromochloromethane 0.0004
1,1-Dichloroethane 0.006
1,1-Dichloroethene 0.35
1,4-Dichlorobenzene 0.006cis-1,2-Dichloroethene 0.07
bis (2-Ethylhexyl) phthalate 0.003
Ethylbenzene 0.6
Toluene 0.6
Xylenes 0.5Heptachlor0.000008
beta-BHC NE
Lead 0.015
Manganese 0.05
Mercury 0.001Methylene Chloride 0.005
Nickel 0.1
Selenium 0.02
Sulfide NE
Tetrahydrofuran NEThallium**0.0002
Vanadium**0.0003
Vinyl Chloride 0.00003
Zinc 1
Alkalinity NEAmmonia-N 1.5
Iron 0.3
Total Dissolved Solids 500
Sulfate 250
Carbon Dioxide NE
Chloride 250
10.31.02 3.26.03 9.13.03 3.26.04 12.2.04 4.23.05 10.25.05 3.28.06 9.27.06 3.31.07 4.10.08 5.13.09 10.18.11 4.12.12 10.24.12 4.25.13
0.0038
0.12 0.15 0.14 0.13 0.4 0.37 0.28 0.28 0.22 0.239 0.247 1.32 0.460.00053 0.00053
0.001
0.0319 0.0053
0.0338
0.0273 1.13 0.16
0.0035 0.00073
0.00039 0.0019 0.0021
0.0137
0.00012
0.0243
0.0052 0.0088
0.0063 0.324 0.051
0.00064 0.00095 0.0046
0.0279 0.327 0.049
343 232 230
344 433 470
14.6 114 100
26.8 25
MW-5 cont.
* NCDEQ Standard = 15A NCAC 02L .0202 Groundwater Standards (Eff. April 1, 2013) ** Interim Maximum Allowable Concentration Bold /yellow values exceed the NCDEQ Standard N/E= Not Established = POC Wells
Table 3 (cont.)History of Site Groundwater and Private Wells Analytical DetectionsFall 2017 Semi-Annual Groundwater Monitoring
North Meck Closed Phase I Area Landfill
CEC Project No. 111-370.001
Constituent NCDEQ Standard (mg/L) *
Sample Date -
Acetone 6
Arsenic 0.01Barium0.7Benzene0.001
Beryllium**NEBromodichloromethane0.0006
Bromoform 0.004
2-Butanone (MEK)4Cadmium0.002
Calcium NEChloroethane3
Chloroform 0.07
Chromium 0.01
Cobalt**0.001
Copper 1Carbon Disulfide 0.7
Dibromochloromethane 0.0004
1,1-Dichloroethane 0.006
1,1-Dichloroethene 0.35
1,4-Dichlorobenzene 0.006cis-1,2-Dichloroethene 0.07
bis (2-Ethylhexyl) phthalate 0.003
Ethylbenzene 0.6
Toluene 0.6
Xylenes 0.5Heptachlor0.000008
beta-BHC NE
Lead 0.015
Manganese 0.05
Mercury 0.001Methylene Chloride 0.005
Nickel 0.1
Selenium 0.02
Sulfide NE
Tetrahydrofuran NEThallium**0.0002
Vanadium**0.0003
Vinyl Chloride 0.00003
Zinc 1
Alkalinity NEAmmonia-N 1.5
Iron 0.3
Total Dissolved Solids 500
Sulfate 250
Carbon Dioxide NE
Chloride 250
10.3.13 4.10.14 10.23.14 4.24.15 10.21.15 4.22.16 10.27.16 4.27.17 6.15.17 10.10.17 10.3.13 4.10.14 10.23.14 4.24.15
0.00015
0.41 0.37 0.46 0.28 0.28 0.31 0.254 0.23 0.24 0.28 0.32 0.32 0.320.00074 0.00076 0.00076 0.0011 0.0012
0.11
99 120 128 0.0015 0.0017 0.0022
0.0055 0.013
0.0027 0.0016
0.11 0.063 0.14 0.011 0.021 0.049 0.0344 0.0054 0.0012 0.028 0.019 0.0072 0.0058
0.0033 0.00083 0.00091 0.00098 0.0036 0.0033 0.0019 0.0029
0.0021 0.0018 0.0019 0.0019 0.0019 0.0014 0.0021 0.0019 0.002 0.0065 0.0054 0.0031 0.0043
0.0011 0.0015
0.00022
0.29 0.31 0.416 0.49 0.37
0.0024 0.0012
0.0014
0.036 0.037 0.033 0.03
0.0072 0.014 0.0076
0.0075 0.0064 0.0086 0.003 0.0021 0.0033 0.0079 0.0016 0.0013 0.012 0.013 0.003 0.00620.031 0.026 0.055 0.085 0.012
310 310 398 420 4500.096
2.8 0.55 0.21
590 450 612 730 69080.7 92 100
870 1300
28 23 34 37 42.0
MW-5 cont.MW-5D
* NCDEQ Standard = 15A NCAC 02L .0202 Groundwater Standards (Eff. April 1, 2013) ** Interim Maximum Allowable Concentration Bold /yellowvalues exceed the NCDEQ Standard N/E= Not Established = POC Wells
Table 3 (cont.)History of Site Groundwater and Private Wells Analytical DetectionsFall 2017 Semi-Annual Groundwater Monitoring
North Meck Closed Phase I Area Landfill
CEC Project No. 111-370.001
Constituent NCDEQ Standard (mg/L) *
Sample Date -
Acetone 6
Arsenic 0.01Barium0.7Benzene0.001
Beryllium**NEBromodichloromethane0.0006
Bromoform 0.004
2-Butanone (MEK)4Cadmium0.002
Calcium NEChloroethane3
Chloroform 0.07
Chromium 0.01
Cobalt**0.001
Copper 1Carbon Disulfide 0.7
Dibromochloromethane 0.0004
1,1-Dichloroethane 0.006
1,1-Dichloroethene 0.35
1,4-Dichlorobenzene 0.006cis-1,2-Dichloroethene 0.07
bis (2-Ethylhexyl) phthalate 0.003
Ethylbenzene 0.6
Toluene 0.6
Xylenes 0.5Heptachlor0.000008
beta-BHC NE
Lead 0.015
Manganese 0.05
Mercury 0.001Methylene Chloride 0.005
Nickel 0.1
Selenium 0.02
Sulfide NE
Tetrahydrofuran NEThallium**0.0002
Vanadium**0.0003
Vinyl Chloride 0.00003
Zinc 1
Alkalinity NEAmmonia-N 1.5
Iron 0.3
Total Dissolved Solids 500
Sulfate 250
Carbon Dioxide NE
Chloride 250
10.21.15 4.22.16 10.27.16 4.27.17 4.27.17 6.15.17 10.10.17 10.10.17 P 3.20.98 4.13.99 3.9.00 3.23.01 3.16.02 10.31.02 3.26.03
(Pace limited)0.0053
0.001 0.0023 0.00027 0.00049 0.017
0.29 0.75 0.26 0.23 0.24 0.13 0.058 0.082 0.084
0.0013 0.0013 0.00097 0.0007
0.00031
250 220 2510.0021 0.0014 0.0016 0.0011 0.0018 0.0016 0.0017
0.0097
0.0076 0.00071 0.00089
0.0052 0.29 0.0011 0.024
0.0028 0.002 0.0019 0.0021 0.0017 0.002 0.0016 0.0017
0.0038 0.0025 0.0028 0.0032 0.0024 0.0023 0.0018 0.0025
0.0048 0.00026
0.8 1.2 0.62 0.67 0.74
0.00016
0.0096 0.015 0.0074 0.0091 0.0085
0.0041 0.0059
0.024 0.024 0.0297 0.026 0.024 0.015 0.0234
0.007 0.11 0.0061 0.0055 0.0032
0.0066 0.0055 0.0021 0.0024 0.0072 0.0025 0.0018 0.0024
0.078 0.032
620 700 703 750 7900.085 0.72
0.161 0.11 0.16
1200 1100 1080 1300 1300
145 170 190
1400 2100
84 79 92 85 91.0
MW-5D (cont.)MW-6
* NCDEQ Standard = 15A NCAC 02L .0202 Groundwater Standards (Eff. April 1, 2013) ** Interim Maximum Allowable Concentration Bold /yellowvalues exceed the NCDEQ Standard N/E= Not Established = POC Wells
Table 3 (cont.)History of Site Groundwater and Private Wells Analytical DetectionsFall 2017 Semi-Annual Groundwater Monitoring
North Meck Closed Phase I Area Landfill
CEC Project No. 111-370.001
Constituent NCDEQ Standard (mg/L) *
Sample Date -
Acetone 6
Arsenic 0.01Barium0.7Benzene0.001
Beryllium**NEBromodichloromethane0.0006
Bromoform 0.004
2-Butanone (MEK)4Cadmium0.002
Calcium NEChloroethane3
Chloroform 0.07
Chromium 0.01
Cobalt**0.001
Copper 1Carbon Disulfide 0.7
Dibromochloromethane 0.0004
1,1-Dichloroethane 0.006
1,1-Dichloroethene 0.35
1,4-Dichlorobenzene 0.006cis-1,2-Dichloroethene 0.07
bis (2-Ethylhexyl) phthalate 0.003
Ethylbenzene 0.6
Toluene 0.6
Xylenes 0.5Heptachlor0.000008
beta-BHC NE
Lead 0.015
Manganese 0.05
Mercury 0.001Methylene Chloride 0.005
Nickel 0.1
Selenium 0.02
Sulfide NE
Tetrahydrofuran NEThallium**0.0002
Vanadium**0.0003
Vinyl Chloride 0.00003
Zinc 1
Alkalinity NEAmmonia-N 1.5
Iron 0.3
Total Dissolved Solids 500
Sulfate 250
Carbon Dioxide NE
Chloride 250
9.13.03 3.26.04 12.2.04 4.23.05 10.25.05 3.28.06 9.27.06 3.31.07 4.10.08 5.13.09 10.18.11 4.12.12 10.24.12 4.25.13 10.3.13 4.10.14 10.23.14
0.0027
0.0027
0.04 0.096 0.11 0.12 0.17 0.18 0.19 0.2 0.255 0.288 0.31 0.32 0.3 0.32
0.0067
0.0096 0.01 0.011 0.02
0.00017
0.0117 0.0131
0.0029 0.00160.026 0.028 0.021 0.13 0.04 0.06
675 662 670
692 773 70026.1 31.3 17
27 30 30
MW-6 cont.
* NCDEQ Standard = 15A NCAC 02L .0202 Groundwater Standards (Eff. April 1, 2013) ** Interim Maximum Allowable Concentration Bold /yellow values exceed the NCDEQ Standard N/E= Not Established = POC Wells
Table 3 (cont.)History of Site Groundwater and Private Wells Analytical DetectionsFall 2017 Semi-Annual Groundwater Monitoring
North Meck Closed Phase I Area Landfill
CEC Project No. 111-370.001
Constituent NCDEQ Standard (mg/L) *
Sample Date -
Acetone 6
Arsenic 0.01Barium0.7Benzene0.001
Beryllium**NEBromodichloromethane0.0006
Bromoform 0.004
2-Butanone (MEK)4Cadmium0.002
Calcium NEChloroethane3
Chloroform 0.07
Chromium 0.01
Cobalt**0.001
Copper 1Carbon Disulfide 0.7
Dibromochloromethane 0.0004
1,1-Dichloroethane 0.006
1,1-Dichloroethene 0.35
1,4-Dichlorobenzene 0.006cis-1,2-Dichloroethene 0.07
bis (2-Ethylhexyl) phthalate 0.003
Ethylbenzene 0.6
Toluene 0.6
Xylenes 0.5Heptachlor0.000008
beta-BHC NE
Lead 0.015
Manganese 0.05
Mercury 0.001Methylene Chloride 0.005
Nickel 0.1
Selenium 0.02
Sulfide NE
Tetrahydrofuran NEThallium**0.0002
Vanadium**0.0003
Vinyl Chloride 0.00003
Zinc 1
Alkalinity NEAmmonia-N 1.5
Iron 0.3
Total Dissolved Solids 500
Sulfate 250
Carbon Dioxide NE
Chloride 250
4.24.15 10.21.15 4.22.16 10.27.16 4.27.17 6.15.17 10.10.17 10.3.13 4.10.14 10.23.14 4.24.15 10.21.15 4.22.16 10.27.16 4.28.17
0.0012 0.00077 0.0038 0.0013 0.00041
0.3 0.29 0.27 0.265 0.19 0.22 0.21 0.22 0.24 0.25 0.22 0.12 0.244 0.270.00094
0.00015 0.00027 0.00025
140 130 154 190 180 188
0.00390.00086 0.0027 0.005
0.0065 0.0059 0.006 0.0085 0.0032 0.011 0.0013 0.0075 0.017
0.0013
0.0014
0.0051 0.00065 0.0023 0.013 0.0017
0.15 0.025 3.51 0.17 1.5 1.6 1.3 3.56 7.2
0.012 0.015 0.017 0.0023 0.0058 0.0086 0.013
0.0017 0.0015
0.0348 0.018 0.025 0.027 0.0029 0.0072 0.0294 0.06
0.0038 0.0027 0.0057 0.0041
0.0007 0.0047 0.0057 0.0014 0.0015 0.0027 0.0047
0.02 0.081 0.023 0.02 0.016 0.02 0.025 0.056 0.0303
660 420 791 530 750 730 850 953 8300.063 0.087
2.38 0.99 2.4 2.32 0.72
870 490 942 720 910 910 920 1040 100043.7 30 38 27
900 500 990 1600
37 34 32 31 36.0 21 20 25 25
MW-6 cont. MW-6D
* NCDEQ Standard = 15A NCAC 02L .0202 Groundwater Standards (Eff. April 1, 2013) ** Interim Maximum Allowable Concentration Bold /yellow values exceed the NCDEQ Standard N/E= Not Established = POC Wells
Table 3 (cont.)History of Site Groundwater and Private Wells Analytical DetectionsFall 2017 Semi-Annual Groundwater Monitoring
North Meck Closed Phase I Area Landfill
CEC Project No. 111-370.001
Constituent NCDEQ Standard (mg/L) *
Sample Date -
Acetone 6
Arsenic 0.01Barium0.7Benzene0.001
Beryllium**NEBromodichloromethane0.0006
Bromoform 0.004
2-Butanone (MEK)4Cadmium0.002
Calcium NEChloroethane3
Chloroform 0.07
Chromium 0.01
Cobalt**0.001
Copper 1Carbon Disulfide 0.7
Dibromochloromethane 0.0004
1,1-Dichloroethane 0.006
1,1-Dichloroethene 0.35
1,4-Dichlorobenzene 0.006cis-1,2-Dichloroethene 0.07
bis (2-Ethylhexyl) phthalate 0.003
Ethylbenzene 0.6
Toluene 0.6
Xylenes 0.5Heptachlor0.000008
beta-BHC NE
Lead 0.015
Manganese 0.05
Mercury 0.001Methylene Chloride 0.005
Nickel 0.1
Selenium 0.02
Sulfide NE
Tetrahydrofuran NEThallium**0.0002
Vanadium**0.0003
Vinyl Chloride 0.00003
Zinc 1
Alkalinity NEAmmonia-N 1.5
Iron 0.3
Total Dissolved Solids 500
Sulfate 250
Carbon Dioxide NE
Chloride 250
6.15.17 10.10.17 10.23.14 4.24.15 10.21.15 4.22.16 10.27.16 4.28.17 6.15.17 10.10.17 10.3.13 4.10.14 10.23.14 4.24.15
0.00035 0.0017 0.0027 0.002 0.0027
0.27 0.25 0.23 0.29 0.29 0.372 0.36 0.38 0.26 0.25 0.24 0.310.00071 0.00066 0.0026 0.0017 0.0014
0.00013
150 140 160
0.0032 0.0173 0.0042
0.0033 0.0065 0.00085
0.0035 0.0196 0.0022 0.00094 0.0063 0.00450.0028
0.0013 0.0023
0.0011
0.0011 0.0015
0.00019 0.013
6.9 0.37 0.48 0.355 0.37 0.355
0.013 0.0121 0.005 0.0121
0.0012 0.0012
0.067 0.048 0.12 0.11 0.11 0.007 0.0112 0.013 0.011 0.0112
0.0033 0.0073 0.0073
0.0038 0.0016 0.0037 0.0014 0.0014 0.0033 0.0011
0.0083 0.073 0.048 0.032
780 500 570 637 6370.068 0.14 0.14
0.48 5.33 2.1 3.3
960 600 620 666 750 666
28 11
490 590
27.0 25 25 30 24 29.6
MW-6D-1MW-6D (cont.)MW-7
* NCDEQ Standard = 15A NCAC 02L .0202 Groundwater Standards (Eff. April 1, 2013) ** Interim Maximum Allowable Concentration Bold /yellowvalues exceed the NCDEQ Standard N/E= Not Established = POC Wells
Table 3 (cont.)History of Site Groundwater and Private Wells Analytical DetectionsFall 2017 Semi-Annual Groundwater Monitoring
North Meck Closed Phase I Area Landfill
CEC Project No. 111-370.001
Constituent NCDEQ Standard (mg/L) *
Sample Date -
Acetone 6
Arsenic 0.01Barium0.7Benzene0.001
Beryllium**NEBromodichloromethane0.0006
Bromoform 0.004
2-Butanone (MEK)4Cadmium0.002
Calcium NEChloroethane3
Chloroform 0.07
Chromium 0.01
Cobalt**0.001
Copper 1Carbon Disulfide 0.7
Dibromochloromethane 0.0004
1,1-Dichloroethane 0.006
1,1-Dichloroethene 0.35
1,4-Dichlorobenzene 0.006cis-1,2-Dichloroethene 0.07
bis (2-Ethylhexyl) phthalate 0.003
Ethylbenzene 0.6
Toluene 0.6
Xylenes 0.5Heptachlor0.000008
beta-BHC NE
Lead 0.015
Manganese 0.05
Mercury 0.001Methylene Chloride 0.005
Nickel 0.1
Selenium 0.02
Sulfide NE
Tetrahydrofuran NEThallium**0.0002
Vanadium**0.0003
Vinyl Chloride 0.00003
Zinc 1
Alkalinity NEAmmonia-N 1.5
Iron 0.3
Total Dissolved Solids 500
Sulfate 250
Carbon Dioxide NE
Chloride 250
10.21.15 4.22.16 10.27.16 5.1.17 6.15.17 10.10.17 10.3.13 4.10.14 10.23.14 4.24.15 10.21.15 4.22.16 10.27.16 5.1.17 6.15.17 10.10.17
0.00043 0.00028 0.00086
0.26 0.29 0.284 0.33 0.33 0.22 0.3 0.26 0.3 0.28 0.27 0.276 0.27 0.340.00035
86 91 89.2 61 63 58.2
0.018 0.0024 0.0024 0.018
0.026 0.0007 0.0023 0.0034
0.0048 0.0089 0.002 0.0078 0.0016 0.0014 0.0013 0.0096
0.00220.0026 0.0024 0.0028 0.0011 0.0014 0.0019
0.0016
0.0011 0.0024 0.00021 0.00081
0.19 0.2 0.0889 0.16 0.31 0.2 0.065 0.0644 0.047 0.12
0.0002 0.00012 0.00094
0.012 0.002 0.0021 0.011
0.0016 0.0013 0.0014 0.0015
0.01
0.0057 0.013 0.0075 0.0052 <0.0005 0.015
0.0016 0.0022 0.0093 0.0032
0.073 0.016 0.018 0.0074 0.019
310 390 376 400 650 230 270 242 260 2800.19 0.053
0.18 3.9 0.16 1.54 0.8 4.8
470 490 485 550 700 350 370 376 420 410
33.2 25 13 21.1 20 22
370 540 350 460
44 44 56 51 25.0 30 32 38 36 38.0
MW-7AMW-7 (cont.)
* NCDEQ Standard = 15A NCAC 02L .0202 Groundwater Standards (Eff. April 1, 2013) ** Interim Maximum Allowable Concentration Bold /yellowvalues exceed the NCDEQ Standard N/E= Not Established = POC Wells
Table 3 (cont.)History of Site Groundwater and Private Wells Analytical DetectionsFall 2017 Semi-Annual Groundwater Monitoring
North Meck Closed Phase I Area Landfill
CEC Project No. 111-370.001
Constituent NCDEQ Standard (mg/L) *
Sample Date -
Acetone 6
Arsenic 0.01Barium0.7Benzene0.001
Beryllium**NEBromodichloromethane0.0006
Bromoform 0.004
2-Butanone (MEK)4Cadmium0.002
Calcium NEChloroethane3
Chloroform 0.07
Chromium 0.01
Cobalt**0.001
Copper 1Carbon Disulfide 0.7
Dibromochloromethane 0.0004
1,1-Dichloroethane 0.006
1,1-Dichloroethene 0.35
1,4-Dichlorobenzene 0.006cis-1,2-Dichloroethene 0.07
bis (2-Ethylhexyl) phthalate 0.003
Ethylbenzene 0.6
Toluene 0.6
Xylenes 0.5Heptachlor0.000008
beta-BHC NE
Lead 0.015
Manganese 0.05
Mercury 0.001Methylene Chloride 0.005
Nickel 0.1
Selenium 0.02
Sulfide NE
Tetrahydrofuran NEThallium**0.0002
Vanadium**0.0003
Vinyl Chloride 0.00003
Zinc 1
Alkalinity NEAmmonia-N 1.5
Iron 0.3
Total Dissolved Solids 500
Sulfate 250
Carbon Dioxide NE
Chloride 250
10.3.13 4.10.14 10.23.14 4.24.15 10.21.15 4.22.16 10.28.16 5.1.17 6.15.17 10.10.17 10.3.13 4.10.14 10.23.14 4.24.15 10.21.15
0.02 0.36 0.027
0.19 0.22 0.21 0.18 0.019 0.2 0.2 0.21 0.22 0.23 0.2 0.057 0.045 0.15
82 84 84.6 57
0.0066 0.029 0.0057 0.027 0.045
0.0014 0.035 0.12 0.015 0.06
0.0018 0.0026
0.0011 0.0015 0.0019 0.002
0.0011
0.0014
0.00022 0.015 0.027 0.015
0.17 0.083 0.0907 0.05 0.048 4.4
0.026
0.0052
0.082 0.12 0.059
0.0013 0.0016 0.0011 0.004 0.00110.05 0.071 0.18 0.028 0.13
270 310 323 320 340 250
0.073 0.46
0.332 0.61 0.62
390 410 433 480 480 22023.1 27 26
310 400 290
35 35 49 42 40.0 7.9
MW-7D MW-8
* NCDEQ Standard = 15A NCAC 02L .0202 Groundwater Standards (Eff. April 1, 2013) ** Interim Maximum Allowable Concentration Bold /yellowvalues exceed the NCDEQ Standard N/E= Not Established = POC Wells
Table 3 (cont.)History of Site Groundwater and Private Wells Analytical DetectionsFall 2017 Semi-Annual Groundwater Monitoring
North Meck Closed Phase I Area Landfill
CEC Project No. 111-370.001
Constituent NCDEQ Standard (mg/L) *
Sample Date -
Acetone 6
Arsenic 0.01Barium0.7Benzene0.001
Beryllium**NEBromodichloromethane0.0006
Bromoform 0.004
2-Butanone (MEK)4Cadmium0.002
Calcium NEChloroethane3
Chloroform 0.07
Chromium 0.01
Cobalt**0.001
Copper 1Carbon Disulfide 0.7
Dibromochloromethane 0.0004
1,1-Dichloroethane 0.006
1,1-Dichloroethene 0.35
1,4-Dichlorobenzene 0.006cis-1,2-Dichloroethene 0.07
bis (2-Ethylhexyl) phthalate 0.003
Ethylbenzene 0.6
Toluene 0.6
Xylenes 0.5Heptachlor0.000008
beta-BHC NE
Lead 0.015
Manganese 0.05
Mercury 0.001Methylene Chloride 0.005
Nickel 0.1
Selenium 0.02
Sulfide NE
Tetrahydrofuran NEThallium**0.0002
Vanadium**0.0003
Vinyl Chloride 0.00003
Zinc 1
Alkalinity NEAmmonia-N 1.5
Iron 0.3
Total Dissolved Solids 500
Sulfate 250
Carbon Dioxide NE
Chloride 250
4.22.16 10.28.16 4.28.17 6.15.17 10.11.17 10.3.13 4.10.14 10.23.14 4.24.15 10.21.15 4.22.16 10.28.16 4.28.17 6.15.17
0.032
0.0029 0.0015 0.002
0.037 0.13 0.14 0.14 0.14 0.09 0.091 0.034 0.072 0.055 0.115 0.35
0.00091 0.00064
0.00037 0.00052 0.00023
43 47.8 85 85 119
0.0171 0.062 0.013 0.14
0.0064 0.0484 0.038 0.0033 0.0079 0.047
0.0021 0.0471 0.1 0.11 0.038 0.03 0.0065 0.0045 0.0162 0.078
0.0042 0.00081
0.0074 0.013
2.4 4.28 3.1 4.3 0.081 0.13 0.254 0.67
0.00012
0.228 0.046 0.47 0.0099 0.11
0.0023 0.0017 0.0016
0.0028
0.0061 0.006
0.511 0.077 0.072 0.028 0.076
0.00045 0.0016 0.0017 0.0021 0.00066 0.0032
0.537 0.088 0.079 0.97 0.033 0.0016 0.0178 0.069
260 280 290 250 280 3551.8 0.27
16.6 23 29 9.51 31
300 332 430 420 430 410 509 560
50.2 41 46 14.7 17
440 240 280
6 9 10 12.0 55 53 77 71
MW-8DMW-8 (cont.)
* NCDEQ Standard = 15A NCAC 02L .0202 Groundwater Standards (Eff. April 1, 2013) ** Interim Maximum Allowable Concentration Bold /yellowvalues exceed the NCDEQ Standard N/E= Not Established = POC Wells
Table 3 (cont.)History of Site Groundwater and Private Wells Analytical DetectionsFall 2017 Semi-Annual Groundwater Monitoring
North Meck Closed Phase I Area Landfill
CEC Project No. 111-370.001
Constituent NCDEQ Standard (mg/L) *
Sample Date -
Acetone 6
Arsenic 0.01Barium0.7Benzene0.001
Beryllium**NEBromodichloromethane0.0006
Bromoform 0.004
2-Butanone (MEK)4Cadmium0.002
Calcium NEChloroethane3
Chloroform 0.07
Chromium 0.01
Cobalt**0.001
Copper 1Carbon Disulfide 0.7
Dibromochloromethane 0.0004
1,1-Dichloroethane 0.006
1,1-Dichloroethene 0.35
1,4-Dichlorobenzene 0.006cis-1,2-Dichloroethene 0.07
bis (2-Ethylhexyl) phthalate 0.003
Ethylbenzene 0.6
Toluene 0.6
Xylenes 0.5Heptachlor0.000008
beta-BHC NE
Lead 0.015
Manganese 0.05
Mercury 0.001Methylene Chloride 0.005
Nickel 0.1
Selenium 0.02
Sulfide NE
Tetrahydrofuran NEThallium**0.0002
Vanadium**0.0003
Vinyl Chloride 0.00003
Zinc 1
Alkalinity NEAmmonia-N 1.5
Iron 0.3
Total Dissolved Solids 500
Sulfate 250
Carbon Dioxide NE
Chloride 250
MW-8D
(cont.)
10.11.17 10.3.13 4.10.14 10.23.14 4.24.15 10.21.15 4.22.16 10.27.16 4.28.17 10.10.17 3.20.98 4.13.99 3.9.00 3.23.01 3.16.02 10.31.02 3.26.03
0.00015 0.017
0.11 0.25 0.11 0.21 0.21 0.07 0.065 0.0497 0.042 0.054 0.097 0.046
0.006
13 14 12.2
0.013 0.016 0.012 0.015
0.0033 0.00041
0.0079 0.043 0.013 0.029 0.031 0.0049 0.0026 0.00092
0.00074
0.26 0.06 0.034 0.0062 0.03 0.0019
0.012 0.001
0.011 0.058 0.05 0.063 0.0032 0.0022
0.016 0.081 0.094 0.083 0.08 0.026
400 40 53 50.2 520.3
4.3 0.167 0.38
570 250 220 161 160 1801518.5 18 15
100 320
82.0 14 30 19 9 24.0
MW-9 MW-10
* NCDEQ Standard = 15A NCAC 02L .0202 Groundwater Standards (Eff. April 1, 2013) ** Interim Maximum Allowable Concentration Bold /yellow values exceed the NCDEQ Standard N/E= Not Established = POC Wells
Table 3 (cont.)History of Site Groundwater and Private Wells Analytical DetectionsFall 2017 Semi-Annual Groundwater Monitoring
North Meck Closed Phase I Area Landfill
CEC Project No. 111-370.001
Constituent NCDEQ Standard (mg/L) *
Sample Date -
Acetone 6
Arsenic 0.01Barium0.7Benzene0.001
Beryllium**NEBromodichloromethane0.0006
Bromoform 0.004
2-Butanone (MEK)4Cadmium0.002
Calcium NEChloroethane3
Chloroform 0.07
Chromium 0.01
Cobalt**0.001
Copper 1Carbon Disulfide 0.7
Dibromochloromethane 0.0004
1,1-Dichloroethane 0.006
1,1-Dichloroethene 0.35
1,4-Dichlorobenzene 0.006cis-1,2-Dichloroethene 0.07
bis (2-Ethylhexyl) phthalate 0.003
Ethylbenzene 0.6
Toluene 0.6
Xylenes 0.5Heptachlor0.000008
beta-BHC NE
Lead 0.015
Manganese 0.05
Mercury 0.001Methylene Chloride 0.005
Nickel 0.1
Selenium 0.02
Sulfide NE
Tetrahydrofuran NEThallium**0.0002
Vanadium**0.0003
Vinyl Chloride 0.00003
Zinc 1
Alkalinity NEAmmonia-N 1.5
Iron 0.3
Total Dissolved Solids 500
Sulfate 250
Carbon Dioxide NE
Chloride 250
9.13.03 3.26.04 12.2.04 4.23.05 10.25.05 3.28.06 9.27.06 3.31.07 4.10.08 5.13.09 10.18.11 4.12.12 10.24.12 4.25.13 10.3.13 4.10.14
0.0026
0.0027 0.0096 0.012 0.013
0.1 0.08 0.091 0.096 0.13 0.048 0.11 0.0739 0.11 0.426 0.22 0.17 0.54
0.0015
0.033
0.0064 0.018
0.0655 0.011
0.0311
0.00012
0.017
0.0054 0.015 0.0042
0.0071 0.162
0.0022 0.0053 0.0072
0.0146 0.107
188 175 220
244 212 130
2.72
11.3 12.3 13
MW-10 cont.
* NCDEQ Standard = 15A NCAC 02L .0202 Groundwater Standards (Eff. April 1, 2013) ** Interim Maximum Allowable Concentration Bold /yellow values exceed the NCDEQ Standard N/E= Not Established = POC Wells
Table 3 (cont.)History of Site Groundwater and Private Wells Analytical DetectionsFall 2017 Semi-Annual Groundwater Monitoring
North Meck Closed Phase I Area Landfill
CEC Project No. 111-370.001
Constituent NCDEQ Standard (mg/L) *
Sample Date -
Acetone 6
Arsenic 0.01Barium0.7Benzene0.001
Beryllium**NEBromodichloromethane0.0006
Bromoform 0.004
2-Butanone (MEK)4Cadmium0.002
Calcium NEChloroethane3
Chloroform 0.07
Chromium 0.01
Cobalt**0.001
Copper 1Carbon Disulfide 0.7
Dibromochloromethane 0.0004
1,1-Dichloroethane 0.006
1,1-Dichloroethene 0.35
1,4-Dichlorobenzene 0.006cis-1,2-Dichloroethene 0.07
bis (2-Ethylhexyl) phthalate 0.003
Ethylbenzene 0.6
Toluene 0.6
Xylenes 0.5Heptachlor0.000008
beta-BHC NE
Lead 0.015
Manganese 0.05
Mercury 0.001Methylene Chloride 0.005
Nickel 0.1
Selenium 0.02
Sulfide NE
Tetrahydrofuran NEThallium**0.0002
Vanadium**0.0003
Vinyl Chloride 0.00003
Zinc 1
Alkalinity NEAmmonia-N 1.5
Iron 0.3
Total Dissolved Solids 500
Sulfate 250
Carbon Dioxide NE
Chloride 250
10.23.14 4.24.15 10.21.15 4.22.16 10.27.16 5.1.17 6.15.17 10.10.17 10.3.13 4.10.14 10.23.14 4.24.15 10.21.15 4.22.16
0.0051 0.0012 0.0013 0.0023
0.25 0.52 0.27 0.39 0.249 0.29 0.24 0.29 0.19 0.2 0.2 0.19 0.150.00041 0.0031 0.0027 0.0029 0.0025 0.0013 0.0025
50 100 61.6 380 420
0.0069 0.0049 0.005 0.033 0.026 0.026 0.024 0.025
0.0051 0.0014 0.068 0.011 0.015 0.007 0.0076 0.015
0.003 0.0029 0.0024 0.0016
0.003
0.004
0.0019
2.9 3.7 3.48 4 4.1 13 17
0.00013
0.051 0.043 0.04 0.042 0.046
0.0089
0.0074 0.12 0.11 0.091 0.085 0.061 0.054
0.012 0.0053 0.005
0.0067 0.0031 0.0061 0.025 0.027 0.029 0.0081 0.0024 0.011
0.076 0.037 0.053 0.015
220 580 360 500 380 1600 15001.5 1.5 1.5 0.51 0.19
67.7 60 60
340 670 430 610 510 2300 2300
0.0007 0.78
320 1300 2000 2100
16 30 24 32 25.0 130 140
MW-10DMW-10 cont.
* NCDEQ Standard = 15A NCAC 02L .0202 Groundwater Standards (Eff. April 1, 2013) ** Interim Maximum Allowable Concentration Bold /yellow values exceed the NCDEQ Standard N/E= Not Established = POC Wells
Table 3 (cont.)History of Site Groundwater and Private Wells Analytical DetectionsFall 2017 Semi-Annual Groundwater Monitoring
North Meck Closed Phase I Area Landfill
CEC Project No. 111-370.001
Constituent NCDEQ Standard (mg/L) *
Sample Date -
Acetone 6
Arsenic 0.01Barium0.7Benzene0.001
Beryllium**NEBromodichloromethane0.0006
Bromoform 0.004
2-Butanone (MEK)4Cadmium0.002
Calcium NEChloroethane3
Chloroform 0.07
Chromium 0.01
Cobalt**0.001
Copper 1Carbon Disulfide 0.7
Dibromochloromethane 0.0004
1,1-Dichloroethane 0.006
1,1-Dichloroethene 0.35
1,4-Dichlorobenzene 0.006cis-1,2-Dichloroethene 0.07
bis (2-Ethylhexyl) phthalate 0.003
Ethylbenzene 0.6
Toluene 0.6
Xylenes 0.5Heptachlor0.000008
beta-BHC NE
Lead 0.015
Manganese 0.05
Mercury 0.001Methylene Chloride 0.005
Nickel 0.1
Selenium 0.02
Sulfide NE
Tetrahydrofuran NEThallium**0.0002
Vanadium**0.0003
Vinyl Chloride 0.00003
Zinc 1
Alkalinity NEAmmonia-N 1.5
Iron 0.3
Total Dissolved Solids 500
Sulfate 250
Carbon Dioxide NE
Chloride 250
MW-10D (cont.)
10.27.16 5.1.17 6.15.17 10.11.17 3.20.98 4.13.99 3.9.00 3.23.01 3.16.02 10.31.02 3.26.03 9.13.03 3.26.04 12.2.04 4.23.05 10.25.05
0.0014 0.0016 0.015
0.244 0.2 0.21 0.14 0.18 0.16 0.18 0.17 0.21 0.25 0.3 0.3
0.0029 0.0032 0.0033 0.0032
0.00054 0.0031
392
0.0099 0.006 0.0066
0.0364 0.038 0.049
1.44 0.46 1.8
0.0019 0.00019 0.0022 0.0018
0.0012 0.0029
17 17 17
0.0002 0.00074 0.00016 0.00082 0.001 0.000480.0075
0.0509 0.048 0.06
0.0012
0.081 0.076 0.077 0.0810.0059
0.0528 0.015 0.02
0.018
0.0227 0.0096 0.045
1610 1700 1700
9.44 2.3 2.7
2260 2500 2500
216 190 140
179 190 200.0
MW-11
* NCDEQ Standard = 15A NCAC 02L .0202 Groundwater Standards (Eff. April 1, 2013) ** Interim Maximum Allowable Concentration Bold /yellow values exceed the NCDEQ Standard N/E= Not Established = POC Wells
Table 3 (cont.)History of Site Groundwater and Private Wells Analytical DetectionsFall 2017 Semi-Annual Groundwater Monitoring
North Meck Closed Phase I Area Landfill
CEC Project No. 111-370.001
Constituent NCDEQ Standard (mg/L) *
Sample Date -
Acetone 6
Arsenic 0.01Barium0.7Benzene0.001
Beryllium**NEBromodichloromethane0.0006
Bromoform 0.004
2-Butanone (MEK)4Cadmium0.002
Calcium NEChloroethane3
Chloroform 0.07
Chromium 0.01
Cobalt**0.001
Copper 1Carbon Disulfide 0.7
Dibromochloromethane 0.0004
1,1-Dichloroethane 0.006
1,1-Dichloroethene 0.35
1,4-Dichlorobenzene 0.006cis-1,2-Dichloroethene 0.07
bis (2-Ethylhexyl) phthalate 0.003
Ethylbenzene 0.6
Toluene 0.6
Xylenes 0.5Heptachlor0.000008
beta-BHC NE
Lead 0.015
Manganese 0.05
Mercury 0.001Methylene Chloride 0.005
Nickel 0.1
Selenium 0.02
Sulfide NE
Tetrahydrofuran NEThallium**0.0002
Vanadium**0.0003
Vinyl Chloride 0.00003
Zinc 1
Alkalinity NEAmmonia-N 1.5
Iron 0.3
Total Dissolved Solids 500
Sulfate 250
Carbon Dioxide NE
Chloride 250
3.28.06 9.27.06 3.31.07 4.10.08 5.13.09 10.18.11 4.12.12 10.24.12 4.25.13 10.3.13 4.10.14 10.23.14 4.24.15 10.21.15 4.22.16
0.0032
0.0086 0.014 0.0012
0.22 0.16 0.15 0.174 0.343 0.244 0.14 0.27 0.1 0.28 0.24 0.26 0.210.00087 0.001 0.0012 0.00062
0.0008
270 160
0.00085
0.01 0.0065 0.014 0.032 0.042 0.014 0.045
1.8 0.73
0.0007 0.002 0.00027
0.0181 0.0164 0.023 0.012
0.0027
0.0284 0.028 0.052 0.023 0.028 0.03 0.022 0.0094
0.0054 0.019
0.0027 0.0086 0.0092 0.012 0.002 0.00190.068 0.031
331 227 990 990 8300.16
382 1160 1200 1400 1100
156 100
1400 1100
6.18 59.7 49 45 36
MW-11 cont.
* NCDEQ Standard = 15A NCAC 02L .0202 Groundwater Standards (Eff. April 1, 2013) ** Interim Maximum Allowable Concentration Bold /yellow values exceed the NCDEQ Standard N/E= Not Established = POC Wells
Table 3 (cont.)History of Site Groundwater and Private Wells Analytical DetectionsFall 2017 Semi-Annual Groundwater Monitoring
North Meck Closed Phase I Area Landfill
CEC Project No. 111-370.001
Constituent NCDEQ Standard (mg/L) *
Sample Date -
Acetone 6
Arsenic 0.01Barium0.7Benzene0.001
Beryllium**NEBromodichloromethane0.0006
Bromoform 0.004
2-Butanone (MEK)4Cadmium0.002
Calcium NEChloroethane3
Chloroform 0.07
Chromium 0.01
Cobalt**0.001
Copper 1Carbon Disulfide 0.7
Dibromochloromethane 0.0004
1,1-Dichloroethane 0.006
1,1-Dichloroethene 0.35
1,4-Dichlorobenzene 0.006cis-1,2-Dichloroethene 0.07
bis (2-Ethylhexyl) phthalate 0.003
Ethylbenzene 0.6
Toluene 0.6
Xylenes 0.5Heptachlor0.000008
beta-BHC NE
Lead 0.015
Manganese 0.05
Mercury 0.001Methylene Chloride 0.005
Nickel 0.1
Selenium 0.02
Sulfide NE
Tetrahydrofuran NEThallium**0.0002
Vanadium**0.0003
Vinyl Chloride 0.00003
Zinc 1
Alkalinity NEAmmonia-N 1.5
Iron 0.3
Total Dissolved Solids 500
Sulfate 250
Carbon Dioxide NE
Chloride 250
MW-11 cont.
10.28.16 4.28.17 6.15.17 10.11.17 10.3.13 4.10.14 10.23.14 4.24.15 10.21.15 4.22.16 10.27.16 4.28.17 10.10.17 10.3.13 4.10.14 10.21.15
0.00083 0.00052
0.448 0.31 0.27 0.047 0.047 0.05 0.04 0.054 0.036 0.329 0.035 0.039 0.2
0.0011 0.0007 0.0009
0.00051 0.00045
290 13 8.3 138 15
0.022 0.017 0.051
0.0089 0.0062 0.0031
0.203 0.089 0.036 0.00082 0.013 0.00071 0.043
0.0011
0.0153 0.0026 0.00076 0.0024
1.73 2.2 2.5 0.015 0.012 0.0608 0.0061 0.0036 0.11
0.0204 0.031 0.053
0.0289 0.02 0.016 0.017
0.0655 0.034 0.007 0.017
0.0069 0.00370.0867 0.025 0.051 0.016 0.016 0.058
1150 1100 1100 88 33 502 37 38 650.12 ND 0.087
33 5.6 0.75 0.164
1100 1500 1400 240 110 657 140 120 670112959642.6 14 11
150 110 130
55 46 51.0 9.1 3.5 32.8 3.5 3.4 4.6
MW-11A MW-11B
* NCDEQ Standard = 15A NCAC 02L .0202 Groundwater Standards (Eff. April 1, 2013) ** Interim Maximum Allowable Concentration Bold /yellowvalues exceed the NCDEQ Standard N/E= Not Established = POC Wells
Table 3 (cont.)History of Site Groundwater and Private Wells Analytical DetectionsFall 2017 Semi-Annual Groundwater Monitoring
North Meck Closed Phase I Area Landfill
CEC Project No. 111-370.001
Constituent NCDEQ Standard (mg/L) *
Sample Date -
Acetone 6
Arsenic 0.01Barium0.7Benzene0.001
Beryllium**NEBromodichloromethane0.0006
Bromoform 0.004
2-Butanone (MEK)4Cadmium0.002
Calcium NEChloroethane3
Chloroform 0.07
Chromium 0.01
Cobalt**0.001
Copper 1Carbon Disulfide 0.7
Dibromochloromethane 0.0004
1,1-Dichloroethane 0.006
1,1-Dichloroethene 0.35
1,4-Dichlorobenzene 0.006cis-1,2-Dichloroethene 0.07
bis (2-Ethylhexyl) phthalate 0.003
Ethylbenzene 0.6
Toluene 0.6
Xylenes 0.5Heptachlor0.000008
beta-BHC NE
Lead 0.015
Manganese 0.05
Mercury 0.001Methylene Chloride 0.005
Nickel 0.1
Selenium 0.02
Sulfide NE
Tetrahydrofuran NEThallium**0.0002
Vanadium**0.0003
Vinyl Chloride 0.00003
Zinc 1
Alkalinity NEAmmonia-N 1.5
Iron 0.3
Total Dissolved Solids 500
Sulfate 250
Carbon Dioxide NE
Chloride 250
4.24.15 4.22.16 10.27.16 4.28.17 10.10.17 10.3.13 4.10.14 10.23.14 4.24.15 10.21.15 4.22.16 10.27.16 4.28.17 10.10.17 10.3.13 4.10.14
0.00043 0.00037
0.088 0.0844 0.07 0.085 0.13 0.13 0.13 0.1 0.074 0.11 0.0852 0.092 0.094 0.12 0.15
11.5
9.5 57 13 70.6
0.0076 0.0076
0.0085 0.0034 0.0038 0.0059 0.02 0.02 0.01 0.027 0.0043 0.0081 0.0096 0.0097 0.0078
0.00024 0.00016
0.034 0.025 0.0053 0.013 0.014 0.22 0.0101 0.01 0.0072
0.00014
0.001
0.0084
0.0022 0.0025
0.0045 0.002 0.0014
0.026 0.019 0.02
39 46.9 48 50 280 280 268 280 2900.15
0.0974
110 131 140 110 400 360 386 410 400
13.4 17 16 33.2 32 34
150 290 310
4.4 4.8 3.8 3.6 19 15 18 17 18.0
MW-11D-1MW-11B (cont.)MW-11D-2
* NCDEQ Standard = 15A NCAC 02L .0202 Groundwater Standards (Eff. April 1, 2013) ** Interim Maximum Allowable Concentration Bold /yellowvalues exceed the NCDEQ Standard N/E= Not Established = POC Wells
Table 3 (cont.)History of Site Groundwater and Private Wells Analytical DetectionsFall 2017 Semi-Annual Groundwater Monitoring
North Meck Closed Phase I Area Landfill
CEC Project No. 111-370.001
Constituent NCDEQ Standard (mg/L) *
Sample Date -
Acetone 6
Arsenic 0.01Barium0.7Benzene0.001
Beryllium**NEBromodichloromethane0.0006
Bromoform 0.004
2-Butanone (MEK)4Cadmium0.002
Calcium NEChloroethane3
Chloroform 0.07
Chromium 0.01
Cobalt**0.001
Copper 1Carbon Disulfide 0.7
Dibromochloromethane 0.0004
1,1-Dichloroethane 0.006
1,1-Dichloroethene 0.35
1,4-Dichlorobenzene 0.006cis-1,2-Dichloroethene 0.07
bis (2-Ethylhexyl) phthalate 0.003
Ethylbenzene 0.6
Toluene 0.6
Xylenes 0.5Heptachlor0.000008
beta-BHC NE
Lead 0.015
Manganese 0.05
Mercury 0.001Methylene Chloride 0.005
Nickel 0.1
Selenium 0.02
Sulfide NE
Tetrahydrofuran NEThallium**0.0002
Vanadium**0.0003
Vinyl Chloride 0.00003
Zinc 1
Alkalinity NEAmmonia-N 1.5
Iron 0.3
Total Dissolved Solids 500
Sulfate 250
Carbon Dioxide NE
Chloride 250
10.23.14 4.24.15 10.21.15 4.22.16 10.27.16 4.28.17 10.10.17 10.23.14 4.24.15 10.21.15 4.22.16 10.27.16 4.28.17 6.15.17 10.10.17
0.0017 0.0027 0.002 0.0027
0.056 0.13 0.083 0.11 0.0979 0.12 0.14 0.25 0.23 0.29 0.29 0.372 0.36 0.38
0.0026 0.0017 0.0014
0.00013
14 13 12.6 12.6 150 140 160
0.0173 0.0042
0.0012 0.00032 0.0065 0.00085
0.0015 0.0047 0.0085 0.005 0.0196 0.0022 0.000940.0028
0.0014 0.0011
0.098 0.29 0.0394 0.099 0.073 0.37 0.48 0.355 0.37 0.355
0.001 0.0121 0.005 0.0121
0.0012
0.12 0.11 0.11 0.007 0.0112 0.013 0.011 0.0112
0.0073 0.0073
0.0038 0.0016 0.00370.022 0.0092 0.073
75 69 62.8 50 48 500 570 637 637ND0.068 0.14 0.14
0.0714 0.05 5.33 2.1 3.3
190 170 145 130 100 600 620 666 750 666
11.8 15 10 11
140 160 490 590
4.4 5.5 4.1 4.1 3.2 25 25 30 24 29.6
MW-6D-1MW-11D-2 (cont.)
* NCDEQ Standard = 15A NCAC 02L .0202 Groundwater Standards (Eff. April 1, 2013) ** Interim Maximum Allowable Concentration Bold /yellowvalues exceed the NCDEQ Standard N/E= Not Established = POC Wells
Table 3 (cont.)History of Site Groundwater and Private Wells Analytical DetectionsFall 2017 Semi-Annual Groundwater Monitoring
North Meck Closed Phase I Area Landfill
CEC Project No. 111-370.001
Constituent NCDEQ Standard (mg/L) *
Sample Date -
Acetone 6
Arsenic 0.01Barium0.7Benzene0.001
Beryllium**NEBromodichloromethane0.0006
Bromoform 0.004
2-Butanone (MEK)4Cadmium0.002
Calcium NEChloroethane3
Chloroform 0.07
Chromium 0.01
Cobalt**0.001
Copper 1Carbon Disulfide 0.7
Dibromochloromethane 0.0004
1,1-Dichloroethane 0.006
1,1-Dichloroethene 0.35
1,4-Dichlorobenzene 0.006cis-1,2-Dichloroethene 0.07
bis (2-Ethylhexyl) phthalate 0.003
Ethylbenzene 0.6
Toluene 0.6
Xylenes 0.5Heptachlor0.000008
beta-BHC NE
Lead 0.015
Manganese 0.05
Mercury 0.001Methylene Chloride 0.005
Nickel 0.1
Selenium 0.02
Sulfide NE
Tetrahydrofuran NEThallium**0.0002
Vanadium**0.0003
Vinyl Chloride 0.00003
Zinc 1
Alkalinity NEAmmonia-N 1.5
Iron 0.3
Total Dissolved Solids 500
Sulfate 250
Carbon Dioxide NE
Chloride 250
4.24.15 10.21.15 4.22.16 10.28.16 6.15.17 10.31.17 4.24.15 10.21.15 4.22.16 10.28.16 5.1.17 10.31.17 4.24.15 10.21.15 4.22.16 10.28.16 5.1.17 10.31.17
0.0074 0.0065
0.00054 0.00019 0.00018 0.00015 0.0053 0.004 0.0028 0.00047
0.1 0.095 0.084 0.033 0.093 0.01 0.031 0.048 0.032 0.0441 0.051 0.012 0.044 0.049 0.037 0.0795 0.035 0.041
0.014 0.014
0.00078
0.022
63 62 98.1 22 23 21.2 110 110 55.3
0.042 0.041
0.0022
0.0041 0.202 0.0011 0.0041 0.0076 0.013 0.018 0.0047 0.008 0.0328 0.0044 0.0043
0.0069 0.0076
0.0886 0.00054 0.005 0.006 0.0006 0.00028
0.12 0.025 0.0543 0.04 0.0016 0.12 0.0214 0.016 0.062 0.058 0.053 0.072 0.06
0.00012 0.00029
0.0015 0.00095
0.026 0.23
0.0077 0.01
0.00093 0.000860.024 0.033 0.366 0.0093 0.02 0.015 0.032 0.053 0.025 0.014 0.027 0.033 0.49
150 160 95.6 160 23 82 98 93.1 85 21 99 159 94 95ND0.074
0.311 0.2 0.477 3 0.66 0.324 0.79 0.29
320 320 550 380 66 140 170 155 160 62 570 308 600 600
310 83 31 6.7 5.2 8.9 72.3 310 320
130 160 100 170 96
17 17 5 17 35 7.7 7.1 11 8 9.5 5 19 5.4 5.6
Hammill WSWGilkerson WSWTinsley WSW (cont.)
* NCDEQ Standard = 15A NCAC 02L .0202 Groundwater Standards (Eff. April 1, 2013) ** Interim Maximum Allowable Concentration Bold /yellowvalues exceed the NCDEQ Standard N/E= Not Established = POC Wells
Table 4
Summary of Vertical Hydraulic Gradients
Fall 2017 Semi-Annual Groundwater Monitoring
North Meck Closed Phase I Area Landfill
CEC Project No. 111-370.001
Well ID Depth1
Ground
Elev.
(ft)
TOC
Elev.
(ft)
TOS
Depth1
BOS
Depth1
TOS
Elev.
(ft)
BOS
Elev.
(ft)
Screen
Midpoint
Elev.
(ft)
April
W.L.2
April
W.L.
Elev.
(ft)
October
W.L.2
October
W.L.
Elev.
(ft)
Vertical
Gradient
Direction
of
Gradient
MW-4A 44 711.93 711.63 34 44 677.93 667.93 672.93 33.61 678.02 33.01 678.62
MW-4D 100 711.72 711.30 85 100 626.72 611.72 619.22 32.93 678.37 32.55 678.75
MW-5 29 NM 682.99 19 29 663.99 653.99 658.99 19.40 663.59 20.49 662.50
MW-5D 55 679.22 681.84 45 55 634.22 626.84 630.53 17.40 664.44 18.61 663.23
MW-6 67 NM 738.25 57 67 681.25 671.25 676.25 57.64 680.61 58.44 679.81
MW-6D 95 735.05 737.90 80 95 655.05 642.9 648.975 58.29 679.61 58.71 679.19
MW-7A 60 724.81 727.52 50 60 674.81 664.81 669.81 44.02 683.50 43.10 684.42
MW-7D 110 724.85 727.36 95 110 629.85 614.85 622.35 45.34 682.02 44.90 682.46
MW-8 80 NM 764.39 70 80 694.39 684.39 689.39 68.72 695.67 68.41 695.98
MW-8D 122 766.2 768.20 107 122 661.20 646.20 653.7 72.50 695.70 72.00 696.20
MW-11A 30 672.87 675.74 20 30 652.87 642.87 647.87 12.54 663.20 16.23 659.51
MW-11D-1 60 672.52 674.44 50 60 622.52 612.52 617.52 11.52 662.92 13.68 659.56
MW-11B 27 670.77 673.24 17 27 653.77 643.77 648.77 4.52 668.72 14.91 659.53
MW-11D-2 40 671.04 673.92 30 40 641.04 631.04 636.04 10.61 663.31 14.31 659.61
Notes:
TOC = Top-of-PVC Casing
NM = Not Measured
TOS = Top-of-Screen
BOS = Bottom-of-Screen
W.L. = Water Level
(1) measured in feet below ground surface
(2) depth relative to TOC elevation
0.002
0.006
0.002
0.026
0.023
0.041
0.0062
UP
UP
UP
UP
DOWN
DOWN
UP
𝑉𝑉𝑉𝑉𝑉𝑉𝑉𝑉𝑉𝑉𝑉𝑉𝑉𝑉𝑉𝑉𝐺𝐺𝑉𝑉𝑉𝑉𝐺𝐺𝑉𝑉𝑉𝑉𝐺𝐺𝑉𝑉=−𝑆𝑆𝑆𝑉𝑉𝑉𝑉𝑉𝑉𝑆𝑆𝑆𝑆𝑊𝑊𝑉𝑉𝑉𝑉𝑉𝑉𝑊𝑊𝑉𝑉𝑉𝑉𝑉𝑉𝑉𝑉𝐿𝐿𝑉𝑉𝐿𝐿𝑉𝑉𝑉𝑉𝐸𝐸𝑉𝑉𝑉𝑉𝐿𝐿.−𝐷𝐷𝑉𝑉𝑉𝑉𝐷𝐷𝑊𝑊𝑉𝑉𝑉𝑉𝑉𝑉𝑊𝑊𝑉𝑉𝑉𝑉𝑉𝑉𝑉𝑉𝐿𝐿𝑉𝑉𝐿𝐿𝑉𝑉𝑉𝑉𝐸𝐸𝑉𝑉𝑉𝑉𝐿𝐿.𝑆𝑆𝑆𝑉𝑉𝑉𝑉𝑉𝑉𝑆𝑆𝑆𝑆𝑊𝑊𝑉𝑉𝑉𝑉𝑉𝑉𝑆𝑆𝑉𝑉𝑉𝑉𝑉𝑉𝑉𝑉𝐺𝐺𝑀𝑀𝑉𝑉𝐺𝐺𝐷𝐷𝑆𝑆𝑉𝑉𝐺𝐺𝑉𝑉−𝐷𝐷𝑉𝑉𝑉𝑉𝐷𝐷𝑊𝑊𝑉𝑉𝑉𝑉𝑉𝑉𝑆𝑆𝑉𝑉𝑉𝑉𝑉𝑉𝑉𝑉𝐺𝐺𝑀𝑀𝑉𝑉𝐺𝐺𝐷𝐷𝑆𝑆𝑉𝑉𝐺𝐺𝑉𝑉

APPENDIX A

APPENDIX B

ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Chicago
2417 Bond Street
University Park, IL 60484
Tel: [phone]
TestAmerica Job ID: 500-135435-1
Client Project/Site: NC North Mecklenburg Landfill
For:
Civil & Environmental Consultants Inc
1900 Center Park Drive
Suite A
Charlotte, North Carolina 28217
Attn: Phillip Pressley
Authorized for release by:
10/29/2017 6:34:07 PM
Robin Kintz, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
TestAmerica Job ID: 500-135435-1
Page 2 of 99 TestAmerica Chicago10/29/2017
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .63
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .64
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .71
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .72
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .86
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .95
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .96
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .99
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Case Narrative
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-135435-1
Project/Site: NC North Mecklenburg Landfill
Job ID: 500-135435-1
Laboratory: TestAmerica Chicago
Narrative
Job Narrative
500-135435-1
Comments
No additional comments.
Receipt
The samples were received on 10/11/2017 10:15 AM; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperatures of the 2 coolers at receipt time were 0.4º C and 0.7º C.
GC/MS VOA
Method(s) 8260B: The laboratory control sample (LCS) for 406058 recovered outside control limits for the following analytes:
Bromomethane and Carbon disulfide. These analytes were biased high in the LCS and were not detected in the associated samples;
therefore, the data have been reported.
Method(s) 8260B: The method blanks for batches 405768 and 406058 were non-detect for all target analytes. Samples associated with
the method blanks detected Acetone just above the reporting limit. Acetone is a known lab contaminant; therefore all low level detects for
this compound should be considered lab contamination. The results have been flagged with a "CN" to denote the probable
contamination.
MW-5D NMLF (500-135435-1), MW-4 NMLF (500-135435-6), SW-4 (500-135435-15), SW-Eff (500-135435-16) and Trip Blank
(500-135435-25)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
Method(s) 200.8: The continuing calibration verification (CCV) associated with batch 500-405644 recovered above the upper control limit
for Selenium. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported.
Method(s) 200.8: The continuing calibration verification (CCV) at line 59, was outside the control limits for Selenium bracketing the method
blank (MB) and laboratory control sample (LCS). The MB and LCS were within the method control limits. The associated samples were
bracketed by CCV that were within control limits. Therefore, the data have been reported
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
General Chemistry
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
TestAmerica ChicagoPage 3 of 99 10/29/2017
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Detection Summary
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Client Sample ID: MW-5D NMLF Lab Sample ID: 500-135435-1
1,1-Dichloroethane
RL
1.0 ug/L
MDL
0.41
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA11.6 8260B
Acetone 5.0 ug/L1.7 Total/NA15.3 cn 8260B
Benzene 0.50 ug/L0.15 Total/NA10.70 8260B
Chloroethane 1.0 ug/L0.51 Total/NA11.6 8260B
cis-1,2-Dichloroethene 1.0 ug/L0.41 Total/NA11.8 8260B
Tetrahydrofuran 10 ug/L1.9 Total/NA1158260B
Vinyl chloride 0.50 ug/L0.20 Total/NA11.8 8260B
Arsenic 1.0 ug/L0.15 Total/NA10.49 J 200.8
Barium 2.5 ug/L0.37 Total/NA1240200.8
Cobalt 1.0 ug/L0.27 Total/NA10.89 J 200.8
Copper 2.0 ug/L0.63 Total/NA12.4 200.8
Iron 100 ug/L38 Total/NA1160200.8
Manganese 2.5 ug/L1.1 Total/NA1740200.8
Nickel 2.0 ug/L0.92 Total/NA18.5 200.8
Vanadium 5.0 ug/L2.0 Total/NA13.2 J 200.8
Chloride 5.0 mg/L4.3 Total/NA25919056A
Sulfate 5.0 mg/L2.4 Total/NA251909056A
Alkalinity 5.0 mg/L3.7 Total/NA1790SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA11300SM 2540C
Client Sample ID: MW-1 NMLF Lab Sample ID: 500-135435-2
Arsenic
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA11.0 200.8
Barium 2.5 ug/L0.37 Total/NA137200.8
Cobalt 1.0 ug/L0.27 Total/NA10.72 J 200.8
Copper 2.0 ug/L0.63 Total/NA10.68 J 200.8
Iron 100 ug/L38 Total/NA18100200.8
Lead 0.50 ug/L0.16 Total/NA10.29 J B 200.8
Manganese 2.5 ug/L1.1 Total/NA11800200.8
Zinc 20 ug/L8.1 Total/NA112J200.8
Chloride 0.20 mg/L0.17 Total/NA13.1 9056A
Sulfate 4.0 mg/L1.9 Total/NA20349056A
Alkalinity 5.0 mg/L3.7 Total/NA1230SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1280SM 2540C
Client Sample ID: MW-5 NMLF Lab Sample ID: 500-135435-3
1,1-Dichloroethane
RL
1.0 ug/L
MDL
0.41
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.98 8260B
Benzene 0.50 ug/L0.15 Total/NA10.76 8260B
Chloroethane 1.0 ug/L0.51 Total/NA11.7 8260B
Vinyl chloride 0.50 ug/L0.20 Total/NA11.3 8260B
Barium 2.5 ug/L0.37 Total/NA1240200.8
Cobalt 1.0 ug/L0.27 Total/NA11.6 200.8
Copper 2.0 ug/L0.63 Total/NA11.2 J 200.8
Iron 100 ug/L38 Total/NA1210200.8
Manganese 2.5 ug/L1.1 Total/NA1370200.8
Nickel 2.0 ug/L0.92 Total/NA11.2 J 200.8
Chloride 5.0 mg/L4.3 Total/NA25429056A
TestAmerica Chicago
This Detection Summary does not include radiochemical test results.
Page 4 of 99 10/29/2017
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Detection Summary
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Client Sample ID: MW-5 NMLF (Continued)Lab Sample ID: 500-135435-3
Sulfate
RL
5.0 mg/L
MDL
2.4
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA251009056A
Alkalinity 5.0 mg/L3.7 Total/NA1450SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1690SM 2540C
Client Sample ID: MW-10 NMLF Lab Sample ID: 500-135435-4
Arsenic
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA11.3 200.8
Barium 2.5 ug/L0.37 Total/NA1240200.8
Cobalt 1.0 ug/L0.27 Total/NA15.0 200.8
Copper 2.0 ug/L0.63 Total/NA11.3 J 200.8
Iron 100 ug/L38 Total/NA160000200.8
Manganese 2.5 ug/L1.1 Total/NA14100200.8
Chloride 4.0 mg/L3.4 Total/NA20259056A
Sulfate 0.20 mg/L0.095 Total/NA10.78 9056A
Alkalinity 5.0 mg/L3.7 Total/NA1380SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1510SM 2540C
Client Sample ID: MW-7 NMLF Lab Sample ID: 500-135435-5
Barium
RL
2.5 ug/L
MDL
0.37
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1330200.8
Chromium 5.0 ug/L2.3 Total/NA12.4 J 200.8
Cobalt 1.0 ug/L0.27 Total/NA10.70 J 200.8
Copper 2.0 ug/L0.63 Total/NA12.0 200.8
Iron 100 ug/L38 Total/NA1160200.8
Lead 0.50 ug/L0.16 Total/NA10.20 J B 200.8
Manganese 2.5 ug/L1.1 Total/NA1130200.8
Chloride 4.0 mg/L3.4 Total/NA20479056A
Sulfate 1.0 mg/L0.48 Total/NA5359056A
Alkalinity 5.0 mg/L3.7 Total/NA1440SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1560SM 2540C
Client Sample ID: MW-4 NMLF Lab Sample ID: 500-135435-6
Acetone
RL
5.0 ug/L
MDL
1.7
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1cn5.7 8260B
Benzene 0.50 ug/L0.15 Total/NA11.1 8260B
Arsenic 1.0 ug/L0.15 Total/NA10.56 J 200.8
Barium 2.5 ug/L0.37 Total/NA1410200.8
Chromium 5.0 ug/L2.3 Total/NA12.6 J 200.8
Cobalt 1.0 ug/L0.27 Total/NA14.9 200.8
Copper 2.0 ug/L0.63 Total/NA11.6 J 200.8
Iron 100 ug/L38 Total/NA11700200.8
Lead 0.50 ug/L0.16 Total/NA13.9 B 200.8
Manganese 2.5 ug/L1.1 Total/NA1760200.8
Nickel 2.0 ug/L0.92 Total/NA13.8 200.8
Zinc 20 ug/L8.1 Total/NA151200.8
Chloride 2.0 mg/L1.7 Total/NA10199056A
Sulfate 0.40 mg/L0.19 Total/NA2109056A
TestAmerica Chicago
This Detection Summary does not include radiochemical test results.
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Detection Summary
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Client Sample ID: MW-4 NMLF (Continued)Lab Sample ID: 500-135435-6
Alkalinity
RL
5.0 mg/L
MDL
3.7
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1300SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1400SM 2540C
Client Sample ID: MW-4A NMLF Lab Sample ID: 500-135435-7
1,1-Dichloroethane
RL
1.0 ug/L
MDL
0.41
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.75 8260B
Arsenic 1.0 ug/L0.15 Total/NA10.30 J 200.8
Barium 2.5 ug/L0.37 Total/NA1170200.8
Chromium 5.0 ug/L2.3 Total/NA110200.8
Cobalt 1.0 ug/L0.27 Total/NA10.94 J 200.8
Copper 2.0 ug/L0.63 Total/NA16.4 200.8
Iron 100 ug/L38 Total/NA11300200.8
Lead 0.50 ug/L0.16 Total/NA11.2 B 200.8
Manganese 2.5 ug/L1.1 Total/NA134200.8
Nickel 2.0 ug/L0.92 Total/NA16.5 200.8
Vanadium 5.0 ug/L2.0 Total/NA13.5 J 200.8
Zinc 20 ug/L8.1 Total/NA116J200.8
Mercury 0.20 ug/L0.091 Total/NA10.43 245.1
Chloride 0.40 mg/L0.34 Total/NA2119056A
Sulfate 0.40 mg/L0.19 Total/NA2129056A
Alkalinity 5.0 mg/L3.7 Total/NA1210SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1330SM 2540C
Client Sample ID: MW-4D NMLF Lab Sample ID: 500-135435-8
Arsenic
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.48 200.8
Barium 2.5 ug/L0.37 Total/NA147200.8
Iron 100 ug/L38 Total/NA1320200.8
Lead 0.50 ug/L0.16 Total/NA10.17 J B 200.8
Manganese 2.5 ug/L1.1 Total/NA1260200.8
Zinc 20 ug/L8.1 Total/NA111J200.8
Chloride 0.40 mg/L0.34 Total/NA25.9 9056A
Sulfate 0.40 mg/L0.19 Total/NA27.8 9056A
Alkalinity 5.0 mg/L3.7 Total/NA1140SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1180SM 2540C
Client Sample ID: MW-6 NMLF Lab Sample ID: 500-135435-9
Arsenic
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA13.8 200.8
Barium 2.5 ug/L0.37 Total/NA1220B200.8
Cobalt 1.0 ug/L0.27 Total/NA12.7 200.8
Copper 2.0 ug/L0.63 Total/NA13.2 200.8
Iron 100 ug/L38 Total/NA12400200.8
Lead 0.50 ug/L0.16 Total/NA12.3 B 200.8
Manganese 2.5 ug/L1.1 Total/NA11500200.8
Nickel 2.0 ug/L0.92 Total/NA12.3 200.8
Selenium 2.5 ug/L1.1 Total/NA11.5 J B ^200.8
TestAmerica Chicago
This Detection Summary does not include radiochemical test results.
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Detection Summary
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Client Sample ID: MW-6 NMLF (Continued)Lab Sample ID: 500-135435-9
Vanadium
RL
5.0 ug/L
MDL
2.0
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J2.7 200.8
Zinc 20 ug/L8.1 Total/NA116J B 200.8
Chloride 2.0 mg/L1.7 Total/NA10369056A
Sulfate 2.0 mg/L0.95 Total/NA10389056A
Alkalinity 5.0 mg/L3.7 Total/NA1750SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1910SM 2540C
Client Sample ID: MW-6D-1 NMLF Lab Sample ID: 500-135435-10
Benzene
RL
0.50 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA11.4 8260B
Tetrahydrofuran 10 ug/L1.9 Total/NA1108260B
Arsenic 1.0 ug/L0.15 Total/NA12.7 200.8
Barium 2.5 ug/L0.37 Total/NA1380B200.8
Cobalt 1.0 ug/L0.27 Total/NA10.85 J 200.8
Copper 2.0 ug/L0.63 Total/NA10.94 J 200.8
Iron 100 ug/L38 Total/NA13300200.8
Manganese 2.5 ug/L1.1 Total/NA1310200.8
Nickel 2.0 ug/L0.92 Total/NA12.0 200.8
Selenium 2.5 ug/L1.1 Total/NA11.3 J B ^200.8
Chloride 2.0 mg/L1.7 Total/NA10259056A
Sulfate 2.0 mg/L0.95 Total/NA10139056A
Alkalinity 5.0 mg/L3.7 Total/NA1650SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1700SM 2540C
Client Sample ID: MW-6D NMLF Lab Sample ID: 500-135435-11
Benzene
RL
0.50 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA10.66 8260B
Tetrahydrofuran 10 ug/L1.9 Total/NA1488260B
Arsenic 1.0 ug/L0.15 Total/NA10.35 J 200.8
Barium 2.5 ug/L0.37 Total/NA1270B200.8
Chromium 5.0 ug/L2.3 Total/NA13.2 J 200.8
Cobalt 1.0 ug/L0.27 Total/NA13.3 200.8
Copper 2.0 ug/L0.63 Total/NA13.5 200.8
Iron 100 ug/L38 Total/NA1480200.8
Lead 0.50 ug/L0.16 Total/NA10.19 J B 200.8
Manganese 25 ug/L11 Total/NA106900200.8
Nickel 2.0 ug/L0.92 Total/NA113200.8
Selenium 2.5 ug/L1.1 Total/NA11.2 J B ^200.8
Vanadium 5.0 ug/L2.0 Total/NA13.3 J 200.8
Zinc 20 ug/L8.1 Total/NA18.3 J B 200.8
Chloride 1.0 mg/L0.85 Total/NA5279056A
Sulfate 1.0 mg/L0.48 Total/NA5289056A
Alkalinity 5.0 mg/L3.7 Total/NA1780SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1960SM 2540C
Client Sample ID: MW-7A NMLF Lab Sample ID: 500-135435-12
TestAmerica Chicago
This Detection Summary does not include radiochemical test results.
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Detection Summary
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Client Sample ID: MW-7A NMLF (Continued)Lab Sample ID: 500-135435-12
Arsenic
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.86 200.8
Barium 2.5 ug/L0.37 Total/NA1340B200.8
Chromium 5.0 ug/L2.3 Total/NA118200.8
Cobalt 1.0 ug/L0.27 Total/NA13.4 200.8
Copper 2.0 ug/L0.63 Total/NA19.6 200.8
Iron 100 ug/L38 Total/NA14800200.8
Lead 0.50 ug/L0.16 Total/NA10.81 B 200.8
Manganese 2.5 ug/L1.1 Total/NA1120200.8
Nickel 2.0 ug/L0.92 Total/NA111200.8
Selenium 2.5 ug/L1.1 Total/NA11.5 J B ^200.8
Vanadium 5.0 ug/L2.0 Total/NA115200.8
Zinc 20 ug/L8.1 Total/NA119J B 200.8
Mercury 0.20 ug/L0.091 Total/NA10.94 245.1
Chloride 2.0 mg/L1.7 Total/NA10389056A
Sulfate 2.0 mg/L0.95 Total/NA10229056A
Alkalinity 5.0 mg/L3.7 Total/NA1280SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1410SM 2540C
Client Sample ID: MW-7D NMLF Lab Sample ID: 500-135435-13
Barium
RL
2.5 ug/L
MDL
0.37
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1B220200.8
Iron 100 ug/L38 Total/NA1620200.8
Manganese 2.5 ug/L1.1 Total/NA148200.8
Chloride 2.0 mg/L1.7 Total/NA10409056A
Sulfate 2.0 mg/L0.95 Total/NA10269056A
Alkalinity 5.0 mg/L3.7 Total/NA1340SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1480SM 2540C
Client Sample ID: MW-9 NMLF Lab Sample ID: 500-135435-14
Barium
RL
2.5 ug/L
MDL
0.37
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1B54200.8
Manganese 2.5 ug/L1.1 Total/NA11.9 J 200.8
Vanadium 5.0 ug/L2.0 Total/NA12.2 J 200.8
Chloride 2.0 mg/L1.7 Total/NA10249056A
Sulfate 0.40 mg/L0.19 Total/NA2159056A
Alkalinity 5.0 mg/L3.7 Total/NA152SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1180SM 2540C
Client Sample ID: SW-4 Lab Sample ID: 500-135435-15
Acetone
RL
5.0 ug/L
MDL
1.7
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1cn6.8 8260B
Client Sample ID: SW-Eff Lab Sample ID: 500-135435-16
Acetone
RL
5.0 ug/L
MDL
1.7
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1cn7.4 8260B
TestAmerica Chicago
This Detection Summary does not include radiochemical test results.
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Detection Summary
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Client Sample ID: SW-3 Lab Sample ID: 500-135435-17
No Detections.
Client Sample ID: SW-2 Lab Sample ID: 500-135435-18
No Detections.
Client Sample ID: MW-4D-1 NMLF Lab Sample ID: 500-135435-19
1,1-Dichloroethane
RL
1.0 ug/L
MDL
0.41
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.76 8260B
Toluene 0.50 ug/L0.15 Total/NA10.38 J 8260B
Xylenes, Total 1.0 ug/L0.22 Total/NA10.41 J 8260B
Arsenic 1.0 ug/L0.15 Total/NA13.6 200.8
Barium 2.5 ug/L0.37 Total/NA168B200.8
Chromium 5.0 ug/L2.3 Total/NA14.3 J 200.8
Copper 2.0 ug/L0.63 Total/NA19.5 200.8
Iron 100 ug/L38 Total/NA1530200.8
Manganese 2.5 ug/L1.1 Total/NA1250200.8
Nickel 2.0 ug/L0.92 Total/NA12.3 200.8
Vanadium 5.0 ug/L2.0 Total/NA12.8 J 200.8
Chloride 1.0 mg/L0.85 Total/NA58.9 9056A
Sulfate 0.20 mg/L0.095 Total/NA11.3 9056A
Alkalinity 5.0 mg/L3.7 Total/NA1210SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1250SM 2540C
Client Sample ID: MW-11D-1 NMLF Lab Sample ID: 500-135435-20
Arsenic
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.37 200.8
Barium 2.5 ug/L0.37 Total/NA194B200.8
Copper 2.0 ug/L0.63 Total/NA19.7 200.8
Lead 0.50 ug/L0.16 Total/NA10.16 J B 200.8
Manganese 2.5 ug/L1.1 Total/NA17.2 200.8
Vanadium 5.0 ug/L2.0 Total/NA12.5 J 200.8
Zinc 20 ug/L8.1 Total/NA120B200.8
Chloride 2.0 mg/L1.7 Total/NA1018F1 F2 9056A
Sulfate 2.0 mg/L0.95 Total/NA1034F1 F2 9056A
Alkalinity 5.0 mg/L3.7 Total/NA1290SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1400SM 2540C
Client Sample ID: MW-11D-2 NMLF Lab Sample ID: 500-135435-21
Barium
RL
2.5 ug/L
MDL
0.37
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1B140200.8
Cobalt 1.0 ug/L0.27 Total/NA10.32 J 200.8
Copper 2.0 ug/L0.63 Total/NA15.0 200.8
Manganese 2.5 ug/L1.1 Total/NA173200.8
Nickel 2.0 ug/L0.92 Total/NA11.0 J 200.8
Zinc 20 ug/L8.1 Total/NA19.2 J B 200.8
Chloride 0.40 mg/L0.34 Total/NA23.2 9056A
Sulfate 0.40 mg/L0.19 Total/NA2109056A
Alkalinity 5.0 mg/L3.7 Total/NA148SM 2320B
TestAmerica Chicago
This Detection Summary does not include radiochemical test results.
Page 9 of 99 10/29/2017
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Detection Summary
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Client Sample ID: MW-11D-2 NMLF (Continued)Lab Sample ID: 500-135435-21
Total Dissolved Solids
RL
10 mg/L
MDL
4.3
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1100SM 2540C
Client Sample ID: MW-11A NMLF Lab Sample ID: 500-135435-22
Barium
RL
2.5 ug/L
MDL
0.37
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1B39200.8
Copper 2.0 ug/L0.63 Total/NA10.71 J 200.8
Manganese 2.5 ug/L1.1 Total/NA13.6 200.8
Chloride 0.40 mg/L0.34 Total/NA23.4 9056A
Sulfate 0.40 mg/L0.19 Total/NA2119056A
Alkalinity 5.0 mg/L3.7 Total/NA138SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1120SM 2540C
Client Sample ID: MW-11B NMLF Lab Sample ID: 500-135435-23
Barium
RL
2.5 ug/L
MDL
0.37
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1B85200.8
Copper 2.0 ug/L0.63 Total/NA13.8 200.8
Iron 100 ug/L38 Total/NA157J200.8
Manganese 2.5 ug/L1.1 Total/NA113200.8
Chloride 0.20 mg/L0.17 Total/NA13.6 9056A
Sulfate 1.0 mg/L0.48 Total/NA5169056A
Alkalinity 5.0 mg/L3.7 Total/NA150SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1110SM 2540C
Client Sample ID: duplicate Lab Sample ID: 500-135435-24
Benzene
RL
0.50 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA10.98 8260B
Chloroethane 1.0 ug/L0.51 Total/NA12.1 8260B
cis-1,2-Dichloroethene 1.0 ug/L0.41 Total/NA12.6 8260B
Vinyl chloride 0.50 ug/L0.20 Total/NA12.4 8260B
Client Sample ID: Trip Blank Lab Sample ID: 500-135435-25
Acetone
RL
5.0 ug/L
MDL
1.7
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1cn9.3 8260B
TestAmerica Chicago
This Detection Summary does not include radiochemical test results.
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Method Summary
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL CHI
EPA200.8 Metals (ICP/MS)TAL CHI
EPA245.1 Mercury (CVAA)TAL CHI
SW8469056AAnions, Ion Chromatography TAL CHI
SMSM 2320B Alkalinity TAL CHI
SMSM 2540C Solids, Total Dissolved (TDS)TAL CHI
Protocol References:
EPA = US Environmental Protection Agency
SM = "Standard Methods For The Examination Of Water And Wastewater",
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL [phone]
TestAmerica Chicago
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Sample Summary
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
500-135435-1 MW-5D NMLF Water 10/10/17 10:50 10/11/17 10:15
500-135435-2 MW-1 NMLF Water 10/10/17 09:50 10/11/17 10:15
500-135435-3 MW-5 NMLF Water 10/10/17 10:30 10/11/17 10:15
500-135435-4 MW-10 NMLF Water 10/10/17 11:45 10/11/17 10:15
500-135435-5 MW-7 NMLF Water 10/10/17 16:15 10/11/17 10:15
500-135435-6 MW-4 NMLF Water 10/10/17 11:45 10/11/17 10:15
500-135435-7 MW-4A NMLF Water 10/10/17 10:35 10/11/17 10:15
500-135435-8 MW-4D NMLF Water 10/10/17 11:05 10/11/17 10:15
500-135435-9 MW-6 NMLF Water 10/10/17 14:30 10/11/17 10:15
500-135435-10 MW-6D-1 NMLF Water 10/10/17 14:00 10/11/17 10:15
500-135435-11 MW-6D NMLF Water 10/10/17 13:30 10/11/17 10:15
500-135435-12 MW-7A NMLF Water 10/10/17 15:15 10/11/17 10:15
500-135435-13 MW-7D NMLF Water 10/10/17 15:45 10/11/17 10:15
500-135435-14 MW-9 NMLF Water 10/10/17 13:15 10/11/17 10:15
500-135435-15 SW-4 Water 10/10/17 15:30 10/11/17 10:15
500-135435-16 SW-Eff Water 10/10/17 15:45 10/11/17 10:15
500-135435-17 SW-3 Water 10/10/17 16:00 10/11/17 10:15
500-135435-18 SW-2 Water 10/10/17 16:15 10/11/17 10:15
500-135435-19 MW-4D-1 NMLF Water 10/10/17 08:55 10/11/17 10:15
500-135435-20 MW-11D-1 NMLF Water 10/10/17 13:55 10/11/17 10:15
500-135435-21 MW-11D-2 NMLF Water 10/10/17 14:50 10/11/17 10:15
500-135435-22 MW-11A NMLF Water 10/10/17 14:15 10/11/17 10:15
500-135435-23 MW-11B NMLF Water 10/10/17 15:15 10/11/17 10:15
500-135435-24 duplicate Water 10/10/17 10:50 10/11/17 10:15
500-135435-25 Trip Blank Water 10/10/17 00:00 10/11/17 10:15
TestAmerica Chicago
Page 12 of 99 10/29/2017
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-1Client Sample ID: MW-5D NMLF
Matrix: WaterDate Collected: 10/10/17 10:50
Date Received: 10/11/17 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 10:30 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/18/17 10:30 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/18/17 10:30 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/18/17 10:30 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/18/17 10:30 11,1-Dichloroethane 1.6
1.0 0.39 ug/L 10/18/17 10:30 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 10/18/17 10:30 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 10/18/17 10:30 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/18/17 10:30 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/18/17 10:30 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/18/17 10:30 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/18/17 10:30 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 10/18/17 10:30 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 10/18/17 10:30 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 10/18/17 10:30 12-Hexanone <5.0
5.0 2.2 ug/L 10/18/17 10:30 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/18/17 10:30 1Acetone5.3 cn
20 4.5 ug/L 10/18/17 10:30 1Acrylonitrile<20
0.50 0.15 ug/L 10/18/17 10:30 1Benzene0.70
1.0 0.43 ug/L 10/18/17 10:30 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/18/17 10:30 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/18/17 10:30 1Bromoform<1.0
2.0 0.80 ug/L 10/18/17 10:30 1Bromomethane<2.0
2.0 0.45 ug/L 10/18/17 10:30 1Carbon disulfide <2.0
1.0 0.38 ug/L 10/18/17 10:30 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/18/17 10:30 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/18/17 10:30 1Chloroethane1.6
2.0 0.37 ug/L 10/18/17 10:30 1Chloroform<2.0
1.0 0.32 ug/L 10/18/17 10:30 1Chloromethane<1.0
1.0 0.41 ug/L 10/18/17 10:30 1cis-1,2-Dichloroethene 1.8
1.0 0.42 ug/L 10/18/17 10:30 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/18/17 10:30 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/18/17 10:30 1Dibromomethane<1.0
0.50 0.18 ug/L 10/18/17 10:30 1Ethylbenzene<0.50
2.5 0.66 ug/L 10/18/17 10:30 1Iodomethane<2.5
5.0 1.6 ug/L 10/18/17 10:30 1Methylene Chloride <5.0
1.0 0.39 ug/L 10/18/17 10:30 1Styrene<1.0
1.0 0.37 ug/L 10/18/17 10:30 1Tetrachloroethene<1.0
10 1.9 ug/L 10/18/17 10:30 1Tetrahydrofuran15
0.50 0.15 ug/L 10/18/17 10:30 1Toluene<0.50
1.0 0.35 ug/L 10/18/17 10:30 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/18/17 10:30 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/18/17 10:30 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/18/17 10:30 1Trichloroethene<0.50
1.0 0.43 ug/L 10/18/17 10:30 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/18/17 10:30 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/18/17 10:30 1Vinyl chloride 1.8
1.0 0.22 ug/L 10/18/17 10:30 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-1Client Sample ID: MW-5D NMLF
Matrix: WaterDate Collected: 10/10/17 10:50
Date Received: 10/11/17 10:15
1,2-Dichloroethane-d4 (Surr)88 75-126 10/18/17 10:30 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)92 10/18/17 10:30 172-124
Dibromofluoromethane 98 10/18/17 10:30 175-120
Toluene-d8 (Surr)96 10/18/17 10:30 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 10/12/17 10:35 10/12/17 15:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 10/12/17 10:35 10/12/17 15:47 1Arsenic0.49 J
2.5 0.37 ug/L 10/12/17 10:35 10/12/17 15:47 1Barium240
1.0 0.43 ug/L 10/12/17 10:35 10/12/17 15:47 1Beryllium<1.0
0.50 0.15 ug/L 10/12/17 10:35 10/12/17 15:47 1Cadmium<0.50
5.0 2.3 ug/L 10/12/17 10:35 10/12/17 15:47 1Chromium<5.0
1.0 0.27 ug/L 10/12/17 10:35 10/12/17 15:47 1Cobalt0.89 J
2.0 0.63 ug/L 10/16/17 11:25 10/17/17 16:28 1Copper2.4
100 38 ug/L 10/12/17 10:35 10/12/17 15:47 1Iron160
0.50 0.16 ug/L 10/12/17 10:35 10/12/17 15:47 1Lead<0.50
2.5 1.1 ug/L 10/12/17 10:35 10/12/17 15:47 1Manganese740
2.0 0.92 ug/L 10/12/17 10:35 10/12/17 15:47 1Nickel8.5
2.5 1.1 ug/L 10/12/17 10:35 10/12/17 15:47 1Selenium<2.5
0.50 0.078 ug/L 10/12/17 10:35 10/12/17 15:47 1Silver<0.50
2.0 0.65 ug/L 10/12/17 10:35 10/12/17 15:47 1Thallium<2.0
5.0 2.0 ug/L 10/12/17 10:35 10/12/17 15:47 1Vanadium3.2 J
20 8.1 ug/L 10/12/17 10:35 10/12/17 15:47 1Zinc<20
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 10/18/17 15:35 10/19/17 09:57 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chloride 91 5.0 4.3 mg/L 10/26/17 22:30 25
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.0 2.4 mg/L 10/26/17 06:00 25Sulfate190
5.0 3.7 mg/L 10/18/17 16:00 1Alkalinity790
10 4.3 mg/L 10/13/17 03:16 1Total Dissolved Solids 1300
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-2Client Sample ID: MW-1 NMLF
Matrix: WaterDate Collected: 10/10/17 09:50
Date Received: 10/11/17 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 10:57 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/18/17 10:57 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/18/17 10:57 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/18/17 10:57 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/18/17 10:57 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/18/17 10:57 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 10/18/17 10:57 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 10/18/17 10:57 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/18/17 10:57 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/18/17 10:57 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/18/17 10:57 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/18/17 10:57 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 10/18/17 10:57 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 10/18/17 10:57 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 10/18/17 10:57 12-Hexanone <5.0
5.0 2.2 ug/L 10/18/17 10:57 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/18/17 10:57 1Acetone<5.0
20 4.5 ug/L 10/18/17 10:57 1Acrylonitrile<20
0.50 0.15 ug/L 10/18/17 10:57 1Benzene<0.50
1.0 0.43 ug/L 10/18/17 10:57 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/18/17 10:57 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/18/17 10:57 1Bromoform<1.0
2.0 0.80 ug/L 10/18/17 10:57 1Bromomethane<2.0
2.0 0.45 ug/L 10/18/17 10:57 1Carbon disulfide <2.0
1.0 0.38 ug/L 10/18/17 10:57 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/18/17 10:57 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/18/17 10:57 1Chloroethane<1.0
2.0 0.37 ug/L 10/18/17 10:57 1Chloroform<2.0
1.0 0.32 ug/L 10/18/17 10:57 1Chloromethane<1.0
1.0 0.41 ug/L 10/18/17 10:57 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/18/17 10:57 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/18/17 10:57 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/18/17 10:57 1Dibromomethane<1.0
0.50 0.18 ug/L 10/18/17 10:57 1Ethylbenzene<0.50
2.5 0.66 ug/L 10/18/17 10:57 1Iodomethane<2.5
5.0 1.6 ug/L 10/18/17 10:57 1Methylene Chloride <5.0
1.0 0.39 ug/L 10/18/17 10:57 1Styrene<1.0
1.0 0.37 ug/L 10/18/17 10:57 1Tetrachloroethene<1.0
10 1.9 ug/L 10/18/17 10:57 1Tetrahydrofuran<10
0.50 0.15 ug/L 10/18/17 10:57 1Toluene<0.50
1.0 0.35 ug/L 10/18/17 10:57 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/18/17 10:57 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/18/17 10:57 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/18/17 10:57 1Trichloroethene<0.50
1.0 0.43 ug/L 10/18/17 10:57 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/18/17 10:57 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/18/17 10:57 1Vinyl chloride <0.50
1.0 0.22 ug/L 10/18/17 10:57 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-2Client Sample ID: MW-1 NMLF
Matrix: WaterDate Collected: 10/10/17 09:50
Date Received: 10/11/17 10:15
1,2-Dichloroethane-d4 (Surr)90 75-126 10/18/17 10:57 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)93 10/18/17 10:57 172-124
Dibromofluoromethane 101 10/18/17 10:57 175-120
Toluene-d8 (Surr)95 10/18/17 10:57 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 10/12/17 10:35 10/12/17 16:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 10/12/17 10:35 10/12/17 16:02 1Arsenic1.0
2.5 0.37 ug/L 10/12/17 10:35 10/12/17 16:02 1Barium37
1.0 0.43 ug/L 10/12/17 10:35 10/12/17 16:02 1Beryllium<1.0
0.50 0.15 ug/L 10/12/17 10:35 10/12/17 16:02 1Cadmium<0.50
5.0 2.3 ug/L 10/12/17 10:35 10/12/17 16:02 1Chromium<5.0
1.0 0.27 ug/L 10/12/17 10:35 10/12/17 16:02 1Cobalt0.72 J
2.0 0.63 ug/L 10/16/17 11:25 10/17/17 16:33 1Copper0.68 J
100 38 ug/L 10/12/17 10:35 10/12/17 16:02 1Iron8100
0.50 0.16 ug/L 10/12/17 10:35 10/12/17 16:02 1Lead0.29 J B
2.5 1.1 ug/L 10/12/17 10:35 10/12/17 16:02 1Manganese1800
2.0 0.92 ug/L 10/12/17 10:35 10/12/17 16:02 1Nickel<2.0
2.5 1.1 ug/L 10/12/17 10:35 10/12/17 16:02 1Selenium<2.5
0.50 0.078 ug/L 10/12/17 10:35 10/12/17 16:02 1Silver<0.50
2.0 0.65 ug/L 10/12/17 10:35 10/12/17 16:02 1Thallium<2.0
5.0 2.0 ug/L 10/12/17 10:35 10/12/17 16:02 1Vanadium<5.0
20 8.1 ug/L 10/12/17 10:35 10/12/17 16:02 1Zinc12J
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 10/18/17 15:35 10/19/17 09:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chloride 3.1 0.20 0.17 mg/L 10/26/17 22:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4.0 1.9 mg/L 10/26/17 06:37 20Sulfate34
5.0 3.7 mg/L 10/18/17 16:20 1Alkalinity230
10 4.3 mg/L 10/13/17 03:23 1Total Dissolved Solids 280
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-3Client Sample ID: MW-5 NMLF
Matrix: WaterDate Collected: 10/10/17 10:30
Date Received: 10/11/17 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 11:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/18/17 11:24 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/18/17 11:24 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/18/17 11:24 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/18/17 11:24 11,1-Dichloroethane 0.98 J
1.0 0.39 ug/L 10/18/17 11:24 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 10/18/17 11:24 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 10/18/17 11:24 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/18/17 11:24 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/18/17 11:24 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/18/17 11:24 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/18/17 11:24 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 10/18/17 11:24 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 10/18/17 11:24 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 10/18/17 11:24 12-Hexanone <5.0
5.0 2.2 ug/L 10/18/17 11:24 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/18/17 11:24 1Acetone<5.0
20 4.5 ug/L 10/18/17 11:24 1Acrylonitrile<20
0.50 0.15 ug/L 10/18/17 11:24 1Benzene0.76
1.0 0.43 ug/L 10/18/17 11:24 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/18/17 11:24 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/18/17 11:24 1Bromoform<1.0
2.0 0.80 ug/L 10/18/17 11:24 1Bromomethane<2.0
2.0 0.45 ug/L 10/18/17 11:24 1Carbon disulfide <2.0
1.0 0.38 ug/L 10/18/17 11:24 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/18/17 11:24 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/18/17 11:24 1Chloroethane1.7
2.0 0.37 ug/L 10/18/17 11:24 1Chloroform<2.0
1.0 0.32 ug/L 10/18/17 11:24 1Chloromethane<1.0
1.0 0.41 ug/L 10/18/17 11:24 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/18/17 11:24 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/18/17 11:24 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/18/17 11:24 1Dibromomethane<1.0
0.50 0.18 ug/L 10/18/17 11:24 1Ethylbenzene<0.50
2.5 0.66 ug/L 10/18/17 11:24 1Iodomethane<2.5
5.0 1.6 ug/L 10/18/17 11:24 1Methylene Chloride <5.0
1.0 0.39 ug/L 10/18/17 11:24 1Styrene<1.0
1.0 0.37 ug/L 10/18/17 11:24 1Tetrachloroethene<1.0
10 1.9 ug/L 10/18/17 11:24 1Tetrahydrofuran<10
0.50 0.15 ug/L 10/18/17 11:24 1Toluene<0.50
1.0 0.35 ug/L 10/18/17 11:24 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/18/17 11:24 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/18/17 11:24 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/18/17 11:24 1Trichloroethene<0.50
1.0 0.43 ug/L 10/18/17 11:24 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/18/17 11:24 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/18/17 11:24 1Vinyl chloride 1.3
1.0 0.22 ug/L 10/18/17 11:24 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-3Client Sample ID: MW-5 NMLF
Matrix: WaterDate Collected: 10/10/17 10:30
Date Received: 10/11/17 10:15
1,2-Dichloroethane-d4 (Surr)95 75-126 10/18/17 11:24 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)92 10/18/17 11:24 172-124
Dibromofluoromethane 105 10/18/17 11:24 175-120
Toluene-d8 (Surr)91 10/18/17 11:24 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 10/12/17 10:35 10/12/17 16:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 10/12/17 10:35 10/12/17 16:06 1Arsenic<1.0
2.5 0.37 ug/L 10/12/17 10:35 10/12/17 16:06 1Barium240
1.0 0.43 ug/L 10/12/17 10:35 10/12/17 16:06 1Beryllium<1.0
0.50 0.15 ug/L 10/12/17 10:35 10/12/17 16:06 1Cadmium<0.50
5.0 2.3 ug/L 10/12/17 10:35 10/12/17 16:06 1Chromium<5.0
1.0 0.27 ug/L 10/12/17 10:35 10/12/17 16:06 1Cobalt1.6
2.0 0.63 ug/L 10/16/17 11:25 10/17/17 16:37 1Copper1.2 J
100 38 ug/L 10/12/17 10:35 10/12/17 16:06 1Iron210
0.50 0.16 ug/L 10/12/17 10:35 10/12/17 16:06 1Lead<0.50
2.5 1.1 ug/L 10/12/17 10:35 10/12/17 16:06 1Manganese370
2.0 0.92 ug/L 10/12/17 10:35 10/12/17 16:06 1Nickel1.2 J
2.5 1.1 ug/L 10/12/17 10:35 10/12/17 16:06 1Selenium<2.5
0.50 0.078 ug/L 10/12/17 10:35 10/12/17 16:06 1Silver<0.50
2.0 0.65 ug/L 10/12/17 10:35 10/12/17 16:06 1Thallium<2.0
5.0 2.0 ug/L 10/12/17 10:35 10/12/17 16:06 1Vanadium<5.0
20 8.1 ug/L 10/12/17 10:35 10/12/17 16:06 1Zinc<20
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 10/18/17 15:35 10/19/17 10:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chloride 42 5.0 4.3 mg/L 10/26/17 22:55 25
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.0 2.4 mg/L 10/26/17 06:49 25Sulfate100
5.0 3.7 mg/L 10/18/17 16:29 1Alkalinity450
10 4.3 mg/L 10/13/17 03:29 1Total Dissolved Solids 690
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-4Client Sample ID: MW-10 NMLF
Matrix: WaterDate Collected: 10/10/17 11:45
Date Received: 10/11/17 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 11:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/18/17 11:51 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/18/17 11:51 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/18/17 11:51 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/18/17 11:51 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/18/17 11:51 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 10/18/17 11:51 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 10/18/17 11:51 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/18/17 11:51 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/18/17 11:51 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/18/17 11:51 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/18/17 11:51 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 10/18/17 11:51 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 10/18/17 11:51 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 10/18/17 11:51 12-Hexanone <5.0
5.0 2.2 ug/L 10/18/17 11:51 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/18/17 11:51 1Acetone<5.0
20 4.5 ug/L 10/18/17 11:51 1Acrylonitrile<20
0.50 0.15 ug/L 10/18/17 11:51 1Benzene<0.50
1.0 0.43 ug/L 10/18/17 11:51 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/18/17 11:51 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/18/17 11:51 1Bromoform<1.0
2.0 0.80 ug/L 10/18/17 11:51 1Bromomethane<2.0
2.0 0.45 ug/L 10/18/17 11:51 1Carbon disulfide <2.0
1.0 0.38 ug/L 10/18/17 11:51 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/18/17 11:51 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/18/17 11:51 1Chloroethane<1.0
2.0 0.37 ug/L 10/18/17 11:51 1Chloroform<2.0
1.0 0.32 ug/L 10/18/17 11:51 1Chloromethane<1.0
1.0 0.41 ug/L 10/18/17 11:51 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/18/17 11:51 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/18/17 11:51 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/18/17 11:51 1Dibromomethane<1.0
0.50 0.18 ug/L 10/18/17 11:51 1Ethylbenzene<0.50
2.5 0.66 ug/L 10/18/17 11:51 1Iodomethane<2.5
5.0 1.6 ug/L 10/18/17 11:51 1Methylene Chloride <5.0
1.0 0.39 ug/L 10/18/17 11:51 1Styrene<1.0
1.0 0.37 ug/L 10/18/17 11:51 1Tetrachloroethene<1.0
10 1.9 ug/L 10/18/17 11:51 1Tetrahydrofuran<10
0.50 0.15 ug/L 10/18/17 11:51 1Toluene<0.50
1.0 0.35 ug/L 10/18/17 11:51 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/18/17 11:51 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/18/17 11:51 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/18/17 11:51 1Trichloroethene<0.50
1.0 0.43 ug/L 10/18/17 11:51 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/18/17 11:51 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/18/17 11:51 1Vinyl chloride <0.50
1.0 0.22 ug/L 10/18/17 11:51 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-4Client Sample ID: MW-10 NMLF
Matrix: WaterDate Collected: 10/10/17 11:45
Date Received: 10/11/17 10:15
1,2-Dichloroethane-d4 (Surr)93 75-126 10/18/17 11:51 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)93 10/18/17 11:51 172-124
Dibromofluoromethane 103 10/18/17 11:51 175-120
Toluene-d8 (Surr)92 10/18/17 11:51 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 10/12/17 10:35 10/12/17 16:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 10/12/17 10:35 10/12/17 16:10 1Arsenic1.3
2.5 0.37 ug/L 10/12/17 10:35 10/12/17 16:10 1Barium240
1.0 0.43 ug/L 10/12/17 10:35 10/12/17 16:10 1Beryllium<1.0
0.50 0.15 ug/L 10/12/17 10:35 10/12/17 16:10 1Cadmium<0.50
5.0 2.3 ug/L 10/12/17 10:35 10/12/17 16:10 1Chromium<5.0
1.0 0.27 ug/L 10/12/17 10:35 10/12/17 16:10 1Cobalt5.0
2.0 0.63 ug/L 10/16/17 11:25 10/17/17 16:41 1Copper1.3 J
100 38 ug/L 10/12/17 10:35 10/12/17 16:10 1Iron60000
0.50 0.16 ug/L 10/12/17 10:35 10/12/17 16:10 1Lead<0.50
2.5 1.1 ug/L 10/12/17 10:35 10/12/17 16:10 1Manganese4100
2.0 0.92 ug/L 10/12/17 10:35 10/12/17 16:10 1Nickel<2.0
2.5 1.1 ug/L 10/12/17 10:35 10/12/17 16:10 1Selenium<2.5
0.50 0.078 ug/L 10/12/17 10:35 10/12/17 16:10 1Silver<0.50
2.0 0.65 ug/L 10/12/17 10:35 10/12/17 16:10 1Thallium<2.0
5.0 2.0 ug/L 10/12/17 10:35 10/12/17 16:10 1Vanadium<5.0
20 8.1 ug/L 10/12/17 10:35 10/12/17 16:10 1Zinc<20
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 10/18/17 15:35 10/19/17 10:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chloride 25 4.0 3.4 mg/L 10/26/17 23:19 20
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.20 0.095 mg/L 10/26/17 23:07 1Sulfate0.78
5.0 3.7 mg/L 10/18/17 11:14 1Alkalinity380
10 4.3 mg/L 10/13/17 03:31 1Total Dissolved Solids 510
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-5Client Sample ID: MW-7 NMLF
Matrix: WaterDate Collected: 10/10/17 16:15
Date Received: 10/11/17 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 12:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/18/17 12:19 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/18/17 12:19 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/18/17 12:19 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/18/17 12:19 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/18/17 12:19 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 10/18/17 12:19 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 10/18/17 12:19 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/18/17 12:19 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/18/17 12:19 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/18/17 12:19 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/18/17 12:19 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 10/18/17 12:19 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 10/18/17 12:19 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 10/18/17 12:19 12-Hexanone <5.0
5.0 2.2 ug/L 10/18/17 12:19 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/18/17 12:19 1Acetone<5.0
20 4.5 ug/L 10/18/17 12:19 1Acrylonitrile<20
0.50 0.15 ug/L 10/18/17 12:19 1Benzene<0.50
1.0 0.43 ug/L 10/18/17 12:19 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/18/17 12:19 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/18/17 12:19 1Bromoform<1.0
2.0 0.80 ug/L 10/18/17 12:19 1Bromomethane<2.0
2.0 0.45 ug/L 10/18/17 12:19 1Carbon disulfide <2.0
1.0 0.38 ug/L 10/18/17 12:19 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/18/17 12:19 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/18/17 12:19 1Chloroethane<1.0
2.0 0.37 ug/L 10/18/17 12:19 1Chloroform<2.0
1.0 0.32 ug/L 10/18/17 12:19 1Chloromethane<1.0
1.0 0.41 ug/L 10/18/17 12:19 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/18/17 12:19 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/18/17 12:19 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/18/17 12:19 1Dibromomethane<1.0
0.50 0.18 ug/L 10/18/17 12:19 1Ethylbenzene<0.50
2.5 0.66 ug/L 10/18/17 12:19 1Iodomethane<2.5
5.0 1.6 ug/L 10/18/17 12:19 1Methylene Chloride <5.0
1.0 0.39 ug/L 10/18/17 12:19 1Styrene<1.0
1.0 0.37 ug/L 10/18/17 12:19 1Tetrachloroethene<1.0
10 1.9 ug/L 10/18/17 12:19 1Tetrahydrofuran<10
0.50 0.15 ug/L 10/18/17 12:19 1Toluene<0.50
1.0 0.35 ug/L 10/18/17 12:19 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/18/17 12:19 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/18/17 12:19 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/18/17 12:19 1Trichloroethene<0.50
1.0 0.43 ug/L 10/18/17 12:19 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/18/17 12:19 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/18/17 12:19 1Vinyl chloride <0.50
1.0 0.22 ug/L 10/18/17 12:19 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-5Client Sample ID: MW-7 NMLF
Matrix: WaterDate Collected: 10/10/17 16:15
Date Received: 10/11/17 10:15
1,2-Dichloroethane-d4 (Surr)93 75-126 10/18/17 12:19 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)93 10/18/17 12:19 172-124
Dibromofluoromethane 102 10/18/17 12:19 175-120
Toluene-d8 (Surr)93 10/18/17 12:19 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 10/12/17 10:35 10/12/17 16:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 10/12/17 10:35 10/12/17 16:21 1Arsenic<1.0
2.5 0.37 ug/L 10/12/17 10:35 10/12/17 16:21 1Barium330
1.0 0.43 ug/L 10/12/17 10:35 10/12/17 16:21 1Beryllium<1.0
0.50 0.15 ug/L 10/12/17 10:35 10/12/17 16:21 1Cadmium<0.50
5.0 2.3 ug/L 10/12/17 10:35 10/12/17 16:21 1Chromium2.4 J
1.0 0.27 ug/L 10/12/17 10:35 10/12/17 16:21 1Cobalt0.70 J
2.0 0.63 ug/L 10/16/17 11:25 10/17/17 16:45 1Copper2.0
100 38 ug/L 10/12/17 10:35 10/12/17 16:21 1Iron160
0.50 0.16 ug/L 10/12/17 10:35 10/12/17 16:21 1Lead0.20 J B
2.5 1.1 ug/L 10/12/17 10:35 10/12/17 16:21 1Manganese130
2.0 0.92 ug/L 10/12/17 10:35 10/12/17 16:21 1Nickel<2.0
2.5 1.1 ug/L 10/12/17 10:35 10/12/17 16:21 1Selenium<2.5
0.50 0.078 ug/L 10/12/17 10:35 10/12/17 16:21 1Silver<0.50
2.0 0.65 ug/L 10/12/17 10:35 10/12/17 16:21 1Thallium<2.0
5.0 2.0 ug/L 10/12/17 10:35 10/12/17 16:21 1Vanadium<5.0
20 8.1 ug/L 10/12/17 10:35 10/12/17 16:21 1Zinc<20
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 10/18/17 15:35 10/19/17 10:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chloride 47 4.0 3.4 mg/L 10/26/17 23:44 20
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.48 mg/L 10/26/17 23:32 5Sulfate35
5.0 3.7 mg/L 10/19/17 11:37 1Alkalinity440
10 4.3 mg/L 10/13/17 03:34 1Total Dissolved Solids 560
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-6Client Sample ID: MW-4 NMLF
Matrix: WaterDate Collected: 10/10/17 11:45
Date Received: 10/11/17 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 12:46 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/18/17 12:46 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/18/17 12:46 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/18/17 12:46 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/18/17 12:46 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/18/17 12:46 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 10/18/17 12:46 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 10/18/17 12:46 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/18/17 12:46 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/18/17 12:46 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/18/17 12:46 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/18/17 12:46 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 10/18/17 12:46 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 10/18/17 12:46 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 10/18/17 12:46 12-Hexanone <5.0
5.0 2.2 ug/L 10/18/17 12:46 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/18/17 12:46 1Acetone5.7 cn
20 4.5 ug/L 10/18/17 12:46 1Acrylonitrile<20
0.50 0.15 ug/L 10/18/17 12:46 1Benzene1.1
1.0 0.43 ug/L 10/18/17 12:46 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/18/17 12:46 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/18/17 12:46 1Bromoform<1.0
2.0 0.80 ug/L 10/18/17 12:46 1Bromomethane<2.0
2.0 0.45 ug/L 10/18/17 12:46 1Carbon disulfide <2.0
1.0 0.38 ug/L 10/18/17 12:46 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/18/17 12:46 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/18/17 12:46 1Chloroethane<1.0
2.0 0.37 ug/L 10/18/17 12:46 1Chloroform<2.0
1.0 0.32 ug/L 10/18/17 12:46 1Chloromethane<1.0
1.0 0.41 ug/L 10/18/17 12:46 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/18/17 12:46 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/18/17 12:46 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/18/17 12:46 1Dibromomethane<1.0
0.50 0.18 ug/L 10/18/17 12:46 1Ethylbenzene<0.50
2.5 0.66 ug/L 10/18/17 12:46 1Iodomethane<2.5
5.0 1.6 ug/L 10/18/17 12:46 1Methylene Chloride <5.0
1.0 0.39 ug/L 10/18/17 12:46 1Styrene<1.0
1.0 0.37 ug/L 10/18/17 12:46 1Tetrachloroethene<1.0
10 1.9 ug/L 10/18/17 12:46 1Tetrahydrofuran<10
0.50 0.15 ug/L 10/18/17 12:46 1Toluene<0.50
1.0 0.35 ug/L 10/18/17 12:46 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/18/17 12:46 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/18/17 12:46 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/18/17 12:46 1Trichloroethene<0.50
1.0 0.43 ug/L 10/18/17 12:46 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/18/17 12:46 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/18/17 12:46 1Vinyl chloride <0.50
1.0 0.22 ug/L 10/18/17 12:46 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-6Client Sample ID: MW-4 NMLF
Matrix: WaterDate Collected: 10/10/17 11:45
Date Received: 10/11/17 10:15
1,2-Dichloroethane-d4 (Surr)93 75-126 10/18/17 12:46 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)93 10/18/17 12:46 172-124
Dibromofluoromethane 103 10/18/17 12:46 175-120
Toluene-d8 (Surr)95 10/18/17 12:46 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 10/12/17 10:35 10/12/17 16:36 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 10/12/17 10:35 10/12/17 16:36 1Arsenic0.56 J
2.5 0.37 ug/L 10/12/17 10:35 10/12/17 16:36 1Barium410
1.0 0.43 ug/L 10/12/17 10:35 10/12/17 16:36 1Beryllium<1.0
0.50 0.15 ug/L 10/12/17 10:35 10/12/17 16:36 1Cadmium<0.50
5.0 2.3 ug/L 10/12/17 10:35 10/12/17 16:36 1Chromium2.6 J
1.0 0.27 ug/L 10/12/17 10:35 10/12/17 16:36 1Cobalt4.9
2.0 0.63 ug/L 10/16/17 11:25 10/17/17 16:48 1Copper1.6 J
100 38 ug/L 10/12/17 10:35 10/12/17 16:36 1Iron1700
0.50 0.16 ug/L 10/12/17 10:35 10/12/17 16:36 1Lead3.9 B
2.5 1.1 ug/L 10/12/17 10:35 10/12/17 16:36 1Manganese760
2.0 0.92 ug/L 10/12/17 10:35 10/12/17 16:36 1Nickel3.8
2.5 1.1 ug/L 10/12/17 10:35 10/12/17 16:36 1Selenium<2.5
0.50 0.078 ug/L 10/12/17 10:35 10/12/17 16:36 1Silver<0.50
2.0 0.65 ug/L 10/12/17 10:35 10/12/17 16:36 1Thallium<2.0
5.0 2.0 ug/L 10/12/17 10:35 10/12/17 16:36 1Vanadium<5.0
20 8.1 ug/L 10/12/17 10:35 10/12/17 16:36 1Zinc51
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 10/18/17 15:35 10/19/17 10:04 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chloride 19 2.0 1.7 mg/L 10/27/17 00:33 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.40 0.19 mg/L 10/26/17 23:56 2Sulfate10
5.0 3.7 mg/L 10/19/17 11:53 1Alkalinity300
10 4.3 mg/L 10/13/17 03:36 1Total Dissolved Solids 400
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-7Client Sample ID: MW-4A NMLF
Matrix: WaterDate Collected: 10/10/17 10:35
Date Received: 10/11/17 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 13:13 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/18/17 13:13 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/18/17 13:13 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/18/17 13:13 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/18/17 13:13 11,1-Dichloroethane 0.75 J
1.0 0.39 ug/L 10/18/17 13:13 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 10/18/17 13:13 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 10/18/17 13:13 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/18/17 13:13 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/18/17 13:13 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/18/17 13:13 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/18/17 13:13 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 10/18/17 13:13 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 10/18/17 13:13 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 10/18/17 13:13 12-Hexanone <5.0
5.0 2.2 ug/L 10/18/17 13:13 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/18/17 13:13 1Acetone<5.0
20 4.5 ug/L 10/18/17 13:13 1Acrylonitrile<20
0.50 0.15 ug/L 10/18/17 13:13 1Benzene<0.50
1.0 0.43 ug/L 10/18/17 13:13 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/18/17 13:13 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/18/17 13:13 1Bromoform<1.0
2.0 0.80 ug/L 10/18/17 13:13 1Bromomethane<2.0
2.0 0.45 ug/L 10/18/17 13:13 1Carbon disulfide <2.0
1.0 0.38 ug/L 10/18/17 13:13 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/18/17 13:13 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/18/17 13:13 1Chloroethane<1.0
2.0 0.37 ug/L 10/18/17 13:13 1Chloroform<2.0
1.0 0.32 ug/L 10/18/17 13:13 1Chloromethane<1.0
1.0 0.41 ug/L 10/18/17 13:13 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/18/17 13:13 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/18/17 13:13 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/18/17 13:13 1Dibromomethane<1.0
0.50 0.18 ug/L 10/18/17 13:13 1Ethylbenzene<0.50
2.5 0.66 ug/L 10/18/17 13:13 1Iodomethane<2.5
5.0 1.6 ug/L 10/18/17 13:13 1Methylene Chloride <5.0
1.0 0.39 ug/L 10/18/17 13:13 1Styrene<1.0
1.0 0.37 ug/L 10/18/17 13:13 1Tetrachloroethene<1.0
10 1.9 ug/L 10/18/17 13:13 1Tetrahydrofuran<10
0.50 0.15 ug/L 10/18/17 13:13 1Toluene<0.50
1.0 0.35 ug/L 10/18/17 13:13 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/18/17 13:13 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/18/17 13:13 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/18/17 13:13 1Trichloroethene<0.50
1.0 0.43 ug/L 10/18/17 13:13 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/18/17 13:13 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/18/17 13:13 1Vinyl chloride <0.50
1.0 0.22 ug/L 10/18/17 13:13 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-7Client Sample ID: MW-4A NMLF
Matrix: WaterDate Collected: 10/10/17 10:35
Date Received: 10/11/17 10:15
1,2-Dichloroethane-d4 (Surr)94 75-126 10/18/17 13:13 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)92 10/18/17 13:13 172-124
Dibromofluoromethane 105 10/18/17 13:13 175-120
Toluene-d8 (Surr)94 10/18/17 13:13 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 10/12/17 10:35 10/12/17 16:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 10/12/17 10:35 10/12/17 16:40 1Arsenic0.30 J
2.5 0.37 ug/L 10/12/17 10:35 10/12/17 16:40 1Barium170
1.0 0.43 ug/L 10/12/17 10:35 10/12/17 16:40 1Beryllium<1.0
0.50 0.15 ug/L 10/12/17 10:35 10/12/17 16:40 1Cadmium<0.50
5.0 2.3 ug/L 10/12/17 10:35 10/12/17 16:40 1Chromium10
1.0 0.27 ug/L 10/12/17 10:35 10/12/17 16:40 1Cobalt0.94 J
2.0 0.63 ug/L 10/16/17 11:25 10/17/17 16:52 1Copper6.4
100 38 ug/L 10/12/17 10:35 10/12/17 16:40 1Iron1300
0.50 0.16 ug/L 10/12/17 10:35 10/12/17 16:40 1Lead1.2 B
2.5 1.1 ug/L 10/12/17 10:35 10/12/17 16:40 1Manganese34
2.0 0.92 ug/L 10/12/17 10:35 10/12/17 16:40 1Nickel6.5
2.5 1.1 ug/L 10/12/17 10:35 10/12/17 16:40 1Selenium<2.5
0.50 0.078 ug/L 10/12/17 10:35 10/12/17 16:40 1Silver<0.50
2.0 0.65 ug/L 10/12/17 10:35 10/12/17 16:40 1Thallium<2.0
5.0 2.0 ug/L 10/12/17 10:35 10/12/17 16:40 1Vanadium3.5 J
20 8.1 ug/L 10/12/17 10:35 10/12/17 16:40 1Zinc16J
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury 0.43 0.20 0.091 ug/L 10/18/17 15:35 10/19/17 10:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chloride 11 0.40 0.34 mg/L 10/27/17 00:46 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.40 0.19 mg/L 10/27/17 00:46 2Sulfate12
5.0 3.7 mg/L 10/19/17 11:59 1Alkalinity210
10 4.3 mg/L 10/13/17 03:39 1Total Dissolved Solids 330
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-8Client Sample ID: MW-4D NMLF
Matrix: WaterDate Collected: 10/10/17 11:05
Date Received: 10/11/17 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 13:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/18/17 13:40 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/18/17 13:40 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/18/17 13:40 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/18/17 13:40 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/18/17 13:40 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 10/18/17 13:40 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 10/18/17 13:40 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/18/17 13:40 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/18/17 13:40 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/18/17 13:40 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/18/17 13:40 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 10/18/17 13:40 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 10/18/17 13:40 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 10/18/17 13:40 12-Hexanone <5.0
5.0 2.2 ug/L 10/18/17 13:40 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/18/17 13:40 1Acetone<5.0
20 4.5 ug/L 10/18/17 13:40 1Acrylonitrile<20
0.50 0.15 ug/L 10/18/17 13:40 1Benzene<0.50
1.0 0.43 ug/L 10/18/17 13:40 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/18/17 13:40 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/18/17 13:40 1Bromoform<1.0
2.0 0.80 ug/L 10/18/17 13:40 1Bromomethane<2.0
2.0 0.45 ug/L 10/18/17 13:40 1Carbon disulfide <2.0
1.0 0.38 ug/L 10/18/17 13:40 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/18/17 13:40 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/18/17 13:40 1Chloroethane<1.0
2.0 0.37 ug/L 10/18/17 13:40 1Chloroform<2.0
1.0 0.32 ug/L 10/18/17 13:40 1Chloromethane<1.0
1.0 0.41 ug/L 10/18/17 13:40 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/18/17 13:40 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/18/17 13:40 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/18/17 13:40 1Dibromomethane<1.0
0.50 0.18 ug/L 10/18/17 13:40 1Ethylbenzene<0.50
2.5 0.66 ug/L 10/18/17 13:40 1Iodomethane<2.5
5.0 1.6 ug/L 10/18/17 13:40 1Methylene Chloride <5.0
1.0 0.39 ug/L 10/18/17 13:40 1Styrene<1.0
1.0 0.37 ug/L 10/18/17 13:40 1Tetrachloroethene<1.0
10 1.9 ug/L 10/18/17 13:40 1Tetrahydrofuran<10
0.50 0.15 ug/L 10/18/17 13:40 1Toluene<0.50
1.0 0.35 ug/L 10/18/17 13:40 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/18/17 13:40 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/18/17 13:40 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/18/17 13:40 1Trichloroethene<0.50
1.0 0.43 ug/L 10/18/17 13:40 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/18/17 13:40 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/18/17 13:40 1Vinyl chloride <0.50
1.0 0.22 ug/L 10/18/17 13:40 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-8Client Sample ID: MW-4D NMLF
Matrix: WaterDate Collected: 10/10/17 11:05
Date Received: 10/11/17 10:15
1,2-Dichloroethane-d4 (Surr)94 75-126 10/18/17 13:40 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)93 10/18/17 13:40 172-124
Dibromofluoromethane 105 10/18/17 13:40 175-120
Toluene-d8 (Surr)93 10/18/17 13:40 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 10/12/17 10:35 10/12/17 16:44 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 10/12/17 10:35 10/12/17 16:44 1Arsenic0.48 J
2.5 0.37 ug/L 10/12/17 10:35 10/12/17 16:44 1Barium47
1.0 0.43 ug/L 10/12/17 10:35 10/12/17 16:44 1Beryllium<1.0
0.50 0.15 ug/L 10/12/17 10:35 10/12/17 16:44 1Cadmium<0.50
5.0 2.3 ug/L 10/12/17 10:35 10/12/17 16:44 1Chromium<5.0
1.0 0.27 ug/L 10/12/17 10:35 10/12/17 16:44 1Cobalt<1.0
2.0 0.63 ug/L 10/16/17 11:25 10/17/17 16:56 1Copper<2.0
100 38 ug/L 10/12/17 10:35 10/12/17 16:44 1Iron320
0.50 0.16 ug/L 10/12/17 10:35 10/12/17 16:44 1Lead0.17 J B
2.5 1.1 ug/L 10/12/17 10:35 10/12/17 16:44 1Manganese260
2.0 0.92 ug/L 10/12/17 10:35 10/12/17 16:44 1Nickel<2.0
2.5 1.1 ug/L 10/12/17 10:35 10/12/17 16:44 1Selenium<2.5
0.50 0.078 ug/L 10/12/17 10:35 10/12/17 16:44 1Silver<0.50
2.0 0.65 ug/L 10/12/17 10:35 10/12/17 16:44 1Thallium<2.0
5.0 2.0 ug/L 10/12/17 10:35 10/12/17 16:44 1Vanadium<5.0
20 8.1 ug/L 10/12/17 10:35 10/12/17 16:44 1Zinc11J
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 10/18/17 15:35 10/19/17 10:07 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chloride 5.9 0.40 0.34 mg/L 10/27/17 01:11 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.40 0.19 mg/L 10/27/17 01:11 2Sulfate7.8
5.0 3.7 mg/L 10/19/17 12:09 1Alkalinity140
10 4.3 mg/L 10/13/17 03:42 1Total Dissolved Solids 180
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-9Client Sample ID: MW-6 NMLF
Matrix: WaterDate Collected: 10/10/17 14:30
Date Received: 10/11/17 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 14:07 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/18/17 14:07 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/18/17 14:07 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/18/17 14:07 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/18/17 14:07 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/18/17 14:07 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 10/18/17 14:07 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 10/18/17 14:07 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/18/17 14:07 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/18/17 14:07 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/18/17 14:07 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/18/17 14:07 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 10/18/17 14:07 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 10/18/17 14:07 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 10/18/17 14:07 12-Hexanone <5.0
5.0 2.2 ug/L 10/18/17 14:07 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/18/17 14:07 1Acetone<5.0
20 4.5 ug/L 10/18/17 14:07 1Acrylonitrile<20
0.50 0.15 ug/L 10/18/17 14:07 1Benzene<0.50
1.0 0.43 ug/L 10/18/17 14:07 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/18/17 14:07 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/18/17 14:07 1Bromoform<1.0
2.0 0.80 ug/L 10/18/17 14:07 1Bromomethane<2.0
2.0 0.45 ug/L 10/18/17 14:07 1Carbon disulfide <2.0
1.0 0.38 ug/L 10/18/17 14:07 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/18/17 14:07 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/18/17 14:07 1Chloroethane<1.0
2.0 0.37 ug/L 10/18/17 14:07 1Chloroform<2.0
1.0 0.32 ug/L 10/18/17 14:07 1Chloromethane<1.0
1.0 0.41 ug/L 10/18/17 14:07 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/18/17 14:07 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/18/17 14:07 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/18/17 14:07 1Dibromomethane<1.0
0.50 0.18 ug/L 10/18/17 14:07 1Ethylbenzene<0.50
2.5 0.66 ug/L 10/18/17 14:07 1Iodomethane<2.5
5.0 1.6 ug/L 10/18/17 14:07 1Methylene Chloride <5.0
1.0 0.39 ug/L 10/18/17 14:07 1Styrene<1.0
1.0 0.37 ug/L 10/18/17 14:07 1Tetrachloroethene<1.0
10 1.9 ug/L 10/18/17 14:07 1Tetrahydrofuran<10
0.50 0.15 ug/L 10/18/17 14:07 1Toluene<0.50
1.0 0.35 ug/L 10/18/17 14:07 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/18/17 14:07 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/18/17 14:07 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/18/17 14:07 1Trichloroethene<0.50
1.0 0.43 ug/L 10/18/17 14:07 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/18/17 14:07 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/18/17 14:07 1Vinyl chloride <0.50
1.0 0.22 ug/L 10/18/17 14:07 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-9Client Sample ID: MW-6 NMLF
Matrix: WaterDate Collected: 10/10/17 14:30
Date Received: 10/11/17 10:15
1,2-Dichloroethane-d4 (Surr)93 75-126 10/18/17 14:07 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)92 10/18/17 14:07 172-124
Dibromofluoromethane 105 10/18/17 14:07 175-120
Toluene-d8 (Surr)93 10/18/17 14:07 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 10/13/17 08:45 10/16/17 19:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 10/13/17 08:45 10/16/17 19:15 1Arsenic3.8
2.5 0.37 ug/L 10/13/17 08:45 10/16/17 19:15 1Barium220B
1.0 0.43 ug/L 10/13/17 08:45 10/16/17 19:15 1Beryllium<1.0
0.50 0.15 ug/L 10/13/17 08:45 10/16/17 19:15 1Cadmium<0.50
5.0 2.3 ug/L 10/13/17 08:45 10/16/17 19:15 1Chromium<5.0
1.0 0.27 ug/L 10/13/17 08:45 10/16/17 19:15 1Cobalt2.7
2.0 0.63 ug/L 10/13/17 08:45 10/17/17 13:49 1Copper3.2
100 38 ug/L 10/13/17 08:45 10/16/17 19:15 1Iron2400
0.50 0.16 ug/L 10/13/17 08:45 10/16/17 19:15 1Lead2.3 B
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 19:15 1Manganese1500
2.0 0.92 ug/L 10/13/17 08:45 10/16/17 19:15 1Nickel2.3
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 19:15 1Selenium1.5 J B ^
0.50 0.078 ug/L 10/13/17 08:45 10/16/17 19:15 1Silver<0.50
2.0 0.65 ug/L 10/13/17 08:45 10/16/17 19:15 1Thallium<2.0
5.0 2.0 ug/L 10/13/17 08:45 10/17/17 13:49 1Vanadium2.7 J
20 8.1 ug/L 10/13/17 08:45 10/16/17 19:15 1Zinc16J B
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 10/18/17 15:35 10/19/17 10:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chloride 36 2.0 1.7 mg/L 10/27/17 01:35 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.0 0.95 mg/L 10/27/17 01:35 10Sulfate38
5.0 3.7 mg/L 10/19/17 12:19 1Alkalinity750
10 4.3 mg/L 10/13/17 03:44 1Total Dissolved Solids 910
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-10Client Sample ID: MW-6D-1 NMLF
Matrix: WaterDate Collected: 10/10/17 14:00
Date Received: 10/11/17 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 14:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/18/17 14:34 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/18/17 14:34 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/18/17 14:34 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/18/17 14:34 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/18/17 14:34 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 10/18/17 14:34 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 10/18/17 14:34 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/18/17 14:34 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/18/17 14:34 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/18/17 14:34 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/18/17 14:34 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 10/18/17 14:34 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 10/18/17 14:34 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 10/18/17 14:34 12-Hexanone <5.0
5.0 2.2 ug/L 10/18/17 14:34 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/18/17 14:34 1Acetone<5.0
20 4.5 ug/L 10/18/17 14:34 1Acrylonitrile<20
0.50 0.15 ug/L 10/18/17 14:34 1Benzene1.4
1.0 0.43 ug/L 10/18/17 14:34 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/18/17 14:34 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/18/17 14:34 1Bromoform<1.0
2.0 0.80 ug/L 10/18/17 14:34 1Bromomethane<2.0
2.0 0.45 ug/L 10/18/17 14:34 1Carbon disulfide <2.0
1.0 0.38 ug/L 10/18/17 14:34 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/18/17 14:34 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/18/17 14:34 1Chloroethane<1.0
2.0 0.37 ug/L 10/18/17 14:34 1Chloroform<2.0
1.0 0.32 ug/L 10/18/17 14:34 1Chloromethane<1.0
1.0 0.41 ug/L 10/18/17 14:34 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/18/17 14:34 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/18/17 14:34 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/18/17 14:34 1Dibromomethane<1.0
0.50 0.18 ug/L 10/18/17 14:34 1Ethylbenzene<0.50
2.5 0.66 ug/L 10/18/17 14:34 1Iodomethane<2.5
5.0 1.6 ug/L 10/18/17 14:34 1Methylene Chloride <5.0
1.0 0.39 ug/L 10/18/17 14:34 1Styrene<1.0
1.0 0.37 ug/L 10/18/17 14:34 1Tetrachloroethene<1.0
10 1.9 ug/L 10/18/17 14:34 1Tetrahydrofuran10
0.50 0.15 ug/L 10/18/17 14:34 1Toluene<0.50
1.0 0.35 ug/L 10/18/17 14:34 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/18/17 14:34 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/18/17 14:34 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/18/17 14:34 1Trichloroethene<0.50
1.0 0.43 ug/L 10/18/17 14:34 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/18/17 14:34 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/18/17 14:34 1Vinyl chloride <0.50
1.0 0.22 ug/L 10/18/17 14:34 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-10Client Sample ID: MW-6D-1 NMLF
Matrix: WaterDate Collected: 10/10/17 14:00
Date Received: 10/11/17 10:15
1,2-Dichloroethane-d4 (Surr)93 75-126 10/18/17 14:34 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)93 10/18/17 14:34 172-124
Dibromofluoromethane 103 10/18/17 14:34 175-120
Toluene-d8 (Surr)91 10/18/17 14:34 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 10/13/17 08:45 10/16/17 19:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 10/13/17 08:45 10/16/17 19:19 1Arsenic2.7
2.5 0.37 ug/L 10/13/17 08:45 10/16/17 19:19 1Barium380B
1.0 0.43 ug/L 10/13/17 08:45 10/16/17 19:19 1Beryllium<1.0
0.50 0.15 ug/L 10/13/17 08:45 10/16/17 19:19 1Cadmium<0.50
5.0 2.3 ug/L 10/13/17 08:45 10/16/17 19:19 1Chromium<5.0
1.0 0.27 ug/L 10/13/17 08:45 10/16/17 19:19 1Cobalt0.85 J
2.0 0.63 ug/L 10/13/17 08:45 10/17/17 13:54 1Copper0.94 J
100 38 ug/L 10/13/17 08:45 10/16/17 19:19 1Iron3300
0.50 0.16 ug/L 10/13/17 08:45 10/16/17 19:19 1Lead<0.50
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 19:19 1Manganese310
2.0 0.92 ug/L 10/13/17 08:45 10/16/17 19:19 1Nickel2.0
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 19:19 1Selenium1.3 J B ^
0.50 0.078 ug/L 10/13/17 08:45 10/16/17 19:19 1Silver<0.50
2.0 0.65 ug/L 10/13/17 08:45 10/16/17 19:19 1Thallium<2.0
5.0 2.0 ug/L 10/13/17 08:45 10/17/17 13:54 1Vanadium<5.0
20 8.1 ug/L 10/13/17 08:45 10/16/17 19:19 1Zinc<20
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 10/18/17 15:35 10/19/17 10:13 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chloride 25 2.0 1.7 mg/L 10/27/17 02:00 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.0 0.95 mg/L 10/27/17 02:00 10Sulfate13
5.0 3.7 mg/L 10/19/17 12:29 1Alkalinity650
10 4.3 mg/L 10/13/17 03:47 1Total Dissolved Solids 700
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-11Client Sample ID: MW-6D NMLF
Matrix: WaterDate Collected: 10/10/17 13:30
Date Received: 10/11/17 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 15:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/18/17 15:01 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/18/17 15:01 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/18/17 15:01 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/18/17 15:01 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/18/17 15:01 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 10/18/17 15:01 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 10/18/17 15:01 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/18/17 15:01 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/18/17 15:01 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/18/17 15:01 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/18/17 15:01 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 10/18/17 15:01 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 10/18/17 15:01 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 10/18/17 15:01 12-Hexanone <5.0
5.0 2.2 ug/L 10/18/17 15:01 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/18/17 15:01 1Acetone<5.0
20 4.5 ug/L 10/18/17 15:01 1Acrylonitrile<20
0.50 0.15 ug/L 10/18/17 15:01 1Benzene0.66
1.0 0.43 ug/L 10/18/17 15:01 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/18/17 15:01 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/18/17 15:01 1Bromoform<1.0
2.0 0.80 ug/L 10/18/17 15:01 1Bromomethane<2.0
2.0 0.45 ug/L 10/18/17 15:01 1Carbon disulfide <2.0
1.0 0.38 ug/L 10/18/17 15:01 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/18/17 15:01 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/18/17 15:01 1Chloroethane<1.0
2.0 0.37 ug/L 10/18/17 15:01 1Chloroform<2.0
1.0 0.32 ug/L 10/18/17 15:01 1Chloromethane<1.0
1.0 0.41 ug/L 10/18/17 15:01 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/18/17 15:01 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/18/17 15:01 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/18/17 15:01 1Dibromomethane<1.0
0.50 0.18 ug/L 10/18/17 15:01 1Ethylbenzene<0.50
2.5 0.66 ug/L 10/18/17 15:01 1Iodomethane<2.5
5.0 1.6 ug/L 10/18/17 15:01 1Methylene Chloride <5.0
1.0 0.39 ug/L 10/18/17 15:01 1Styrene<1.0
1.0 0.37 ug/L 10/18/17 15:01 1Tetrachloroethene<1.0
10 1.9 ug/L 10/18/17 15:01 1Tetrahydrofuran48
0.50 0.15 ug/L 10/18/17 15:01 1Toluene<0.50
1.0 0.35 ug/L 10/18/17 15:01 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/18/17 15:01 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/18/17 15:01 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/18/17 15:01 1Trichloroethene<0.50
1.0 0.43 ug/L 10/18/17 15:01 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/18/17 15:01 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/18/17 15:01 1Vinyl chloride <0.50
1.0 0.22 ug/L 10/18/17 15:01 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-11Client Sample ID: MW-6D NMLF
Matrix: WaterDate Collected: 10/10/17 13:30
Date Received: 10/11/17 10:15
1,2-Dichloroethane-d4 (Surr)95 75-126 10/18/17 15:01 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)94 10/18/17 15:01 172-124
Dibromofluoromethane 104 10/18/17 15:01 175-120
Toluene-d8 (Surr)92 10/18/17 15:01 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 10/13/17 08:45 10/16/17 19:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 10/13/17 08:45 10/16/17 19:35 1Arsenic0.35 J
2.5 0.37 ug/L 10/13/17 08:45 10/16/17 19:35 1Barium270B
1.0 0.43 ug/L 10/13/17 08:45 10/16/17 19:35 1Beryllium<1.0
0.50 0.15 ug/L 10/13/17 08:45 10/16/17 19:35 1Cadmium<0.50
5.0 2.3 ug/L 10/13/17 08:45 10/16/17 19:35 1Chromium3.2 J
1.0 0.27 ug/L 10/13/17 08:45 10/16/17 19:35 1Cobalt3.3
2.0 0.63 ug/L 10/13/17 08:45 10/17/17 14:13 1Copper3.5
100 38 ug/L 10/13/17 08:45 10/16/17 19:35 1Iron480
0.50 0.16 ug/L 10/13/17 08:45 10/16/17 19:35 1Lead0.19 J B
25 11 ug/L 10/13/17 08:45 10/17/17 14:17 10Manganese6900
2.0 0.92 ug/L 10/13/17 08:45 10/16/17 19:35 1Nickel13
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 19:35 1Selenium1.2 J B ^
0.50 0.078 ug/L 10/13/17 08:45 10/16/17 19:35 1Silver<0.50
2.0 0.65 ug/L 10/13/17 08:45 10/16/17 19:35 1Thallium<2.0
5.0 2.0 ug/L 10/13/17 08:45 10/17/17 14:13 1Vanadium3.3 J
20 8.1 ug/L 10/13/17 08:45 10/16/17 19:35 1Zinc8.3 J B
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 10/18/17 15:35 10/19/17 10:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chloride 27 1.0 0.85 mg/L 10/27/17 03:02 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.48 mg/L 10/27/17 03:02 5Sulfate28
5.0 3.7 mg/L 10/19/17 12:40 1Alkalinity780
10 4.3 mg/L 10/13/17 03:49 1Total Dissolved Solids 960
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-12Client Sample ID: MW-7A NMLF
Matrix: WaterDate Collected: 10/10/17 15:15
Date Received: 10/11/17 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 15:29 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/18/17 15:29 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/18/17 15:29 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/18/17 15:29 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/18/17 15:29 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/18/17 15:29 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 10/18/17 15:29 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 10/18/17 15:29 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/18/17 15:29 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/18/17 15:29 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/18/17 15:29 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/18/17 15:29 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 10/18/17 15:29 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 10/18/17 15:29 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 10/18/17 15:29 12-Hexanone <5.0
5.0 2.2 ug/L 10/18/17 15:29 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/18/17 15:29 1Acetone<5.0
20 4.5 ug/L 10/18/17 15:29 1Acrylonitrile<20
0.50 0.15 ug/L 10/18/17 15:29 1Benzene<0.50
1.0 0.43 ug/L 10/18/17 15:29 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/18/17 15:29 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/18/17 15:29 1Bromoform<1.0
2.0 0.80 ug/L 10/18/17 15:29 1Bromomethane<2.0
2.0 0.45 ug/L 10/18/17 15:29 1Carbon disulfide <2.0
1.0 0.38 ug/L 10/18/17 15:29 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/18/17 15:29 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/18/17 15:29 1Chloroethane<1.0
2.0 0.37 ug/L 10/18/17 15:29 1Chloroform<2.0
1.0 0.32 ug/L 10/18/17 15:29 1Chloromethane<1.0
1.0 0.41 ug/L 10/18/17 15:29 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/18/17 15:29 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/18/17 15:29 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/18/17 15:29 1Dibromomethane<1.0
0.50 0.18 ug/L 10/18/17 15:29 1Ethylbenzene<0.50
2.5 0.66 ug/L 10/18/17 15:29 1Iodomethane<2.5
5.0 1.6 ug/L 10/18/17 15:29 1Methylene Chloride <5.0
1.0 0.39 ug/L 10/18/17 15:29 1Styrene<1.0
1.0 0.37 ug/L 10/18/17 15:29 1Tetrachloroethene<1.0
10 1.9 ug/L 10/18/17 15:29 1Tetrahydrofuran<10
0.50 0.15 ug/L 10/18/17 15:29 1Toluene<0.50
1.0 0.35 ug/L 10/18/17 15:29 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/18/17 15:29 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/18/17 15:29 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/18/17 15:29 1Trichloroethene<0.50
1.0 0.43 ug/L 10/18/17 15:29 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/18/17 15:29 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/18/17 15:29 1Vinyl chloride <0.50
1.0 0.22 ug/L 10/18/17 15:29 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-12Client Sample ID: MW-7A NMLF
Matrix: WaterDate Collected: 10/10/17 15:15
Date Received: 10/11/17 10:15
1,2-Dichloroethane-d4 (Surr)95 75-126 10/18/17 15:29 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)91 10/18/17 15:29 172-124
Dibromofluoromethane 105 10/18/17 15:29 175-120
Toluene-d8 (Surr)90 10/18/17 15:29 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 10/13/17 08:45 10/16/17 19:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 10/13/17 08:45 10/16/17 19:39 1Arsenic0.86 J
2.5 0.37 ug/L 10/13/17 08:45 10/16/17 19:39 1Barium340B
1.0 0.43 ug/L 10/13/17 08:45 10/16/17 19:39 1Beryllium<1.0
0.50 0.15 ug/L 10/13/17 08:45 10/16/17 19:39 1Cadmium<0.50
5.0 2.3 ug/L 10/13/17 08:45 10/16/17 19:39 1Chromium18
1.0 0.27 ug/L 10/13/17 08:45 10/16/17 19:39 1Cobalt3.4
2.0 0.63 ug/L 10/13/17 08:45 10/17/17 14:22 1Copper9.6
100 38 ug/L 10/13/17 08:45 10/16/17 19:39 1Iron4800
0.50 0.16 ug/L 10/13/17 08:45 10/16/17 19:39 1Lead0.81 B
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 19:39 1Manganese120
2.0 0.92 ug/L 10/13/17 08:45 10/16/17 19:39 1Nickel11
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 19:39 1Selenium1.5 J B ^
0.50 0.078 ug/L 10/13/17 08:45 10/16/17 19:39 1Silver<0.50
2.0 0.65 ug/L 10/13/17 08:45 10/16/17 19:39 1Thallium<2.0
5.0 2.0 ug/L 10/13/17 08:45 10/17/17 14:22 1Vanadium15
20 8.1 ug/L 10/13/17 08:45 10/16/17 19:39 1Zinc19J B
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury 0.94 0.20 0.091 ug/L 10/18/17 15:35 10/19/17 10:16 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chloride 38 2.0 1.7 mg/L 10/27/17 03:39 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.0 0.95 mg/L 10/27/17 03:39 10Sulfate22
5.0 3.7 mg/L 10/19/17 12:47 1Alkalinity280
10 4.3 mg/L 10/13/17 03:52 1Total Dissolved Solids 410
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-13Client Sample ID: MW-7D NMLF
Matrix: WaterDate Collected: 10/10/17 15:45
Date Received: 10/11/17 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 15:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/18/17 15:56 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/18/17 15:56 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/18/17 15:56 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/18/17 15:56 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/18/17 15:56 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 10/18/17 15:56 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 10/18/17 15:56 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/18/17 15:56 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/18/17 15:56 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/18/17 15:56 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/18/17 15:56 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 10/18/17 15:56 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 10/18/17 15:56 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 10/18/17 15:56 12-Hexanone <5.0
5.0 2.2 ug/L 10/18/17 15:56 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/18/17 15:56 1Acetone<5.0
20 4.5 ug/L 10/18/17 15:56 1Acrylonitrile<20
0.50 0.15 ug/L 10/18/17 15:56 1Benzene<0.50
1.0 0.43 ug/L 10/18/17 15:56 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/18/17 15:56 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/18/17 15:56 1Bromoform<1.0
2.0 0.80 ug/L 10/18/17 15:56 1Bromomethane<2.0
2.0 0.45 ug/L 10/18/17 15:56 1Carbon disulfide <2.0
1.0 0.38 ug/L 10/18/17 15:56 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/18/17 15:56 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/18/17 15:56 1Chloroethane<1.0
2.0 0.37 ug/L 10/18/17 15:56 1Chloroform<2.0
1.0 0.32 ug/L 10/18/17 15:56 1Chloromethane<1.0
1.0 0.41 ug/L 10/18/17 15:56 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/18/17 15:56 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/18/17 15:56 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/18/17 15:56 1Dibromomethane<1.0
0.50 0.18 ug/L 10/18/17 15:56 1Ethylbenzene<0.50
2.5 0.66 ug/L 10/18/17 15:56 1Iodomethane<2.5
5.0 1.6 ug/L 10/18/17 15:56 1Methylene Chloride <5.0
1.0 0.39 ug/L 10/18/17 15:56 1Styrene<1.0
1.0 0.37 ug/L 10/18/17 15:56 1Tetrachloroethene<1.0
10 1.9 ug/L 10/18/17 15:56 1Tetrahydrofuran<10
0.50 0.15 ug/L 10/18/17 15:56 1Toluene<0.50
1.0 0.35 ug/L 10/18/17 15:56 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/18/17 15:56 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/18/17 15:56 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/18/17 15:56 1Trichloroethene<0.50
1.0 0.43 ug/L 10/18/17 15:56 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/18/17 15:56 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/18/17 15:56 1Vinyl chloride <0.50
1.0 0.22 ug/L 10/18/17 15:56 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-13Client Sample ID: MW-7D NMLF
Matrix: WaterDate Collected: 10/10/17 15:45
Date Received: 10/11/17 10:15
1,2-Dichloroethane-d4 (Surr)93 75-126 10/18/17 15:56 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)92 10/18/17 15:56 172-124
Dibromofluoromethane 105 10/18/17 15:56 175-120
Toluene-d8 (Surr)96 10/18/17 15:56 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 10/13/17 08:45 10/16/17 19:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 10/13/17 08:45 10/16/17 19:51 1Arsenic<1.0
2.5 0.37 ug/L 10/13/17 08:45 10/16/17 19:51 1Barium220B
1.0 0.43 ug/L 10/13/17 08:45 10/16/17 19:51 1Beryllium<1.0
0.50 0.15 ug/L 10/13/17 08:45 10/16/17 19:51 1Cadmium<0.50
5.0 2.3 ug/L 10/13/17 08:45 10/16/17 19:51 1Chromium<5.0
1.0 0.27 ug/L 10/13/17 08:45 10/16/17 19:51 1Cobalt<1.0
2.0 0.63 ug/L 10/13/17 08:45 10/17/17 14:36 1Copper<2.0
100 38 ug/L 10/13/17 08:45 10/16/17 19:51 1Iron620
0.50 0.16 ug/L 10/13/17 08:45 10/16/17 19:51 1Lead<0.50
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 19:51 1Manganese48
2.0 0.92 ug/L 10/13/17 08:45 10/16/17 19:51 1Nickel<2.0
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 19:51 1Selenium<2.5
0.50 0.078 ug/L 10/13/17 08:45 10/16/17 19:51 1Silver<0.50
2.0 0.65 ug/L 10/13/17 08:45 10/16/17 19:51 1Thallium<2.0
5.0 2.0 ug/L 10/13/17 08:45 10/17/17 14:36 1Vanadium<5.0
20 8.1 ug/L 10/13/17 08:45 10/16/17 19:51 1Zinc<20
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 10/18/17 15:35 10/19/17 10:18 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chloride 40 2.0 1.7 mg/L 10/27/17 03:51 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.0 0.95 mg/L 10/27/17 03:51 10Sulfate26
5.0 3.7 mg/L 10/19/17 12:54 1Alkalinity340
10 4.3 mg/L 10/13/17 03:54 1Total Dissolved Solids 480
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-14Client Sample ID: MW-9 NMLF
Matrix: WaterDate Collected: 10/10/17 13:15
Date Received: 10/11/17 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 16:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/18/17 16:23 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/18/17 16:23 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/18/17 16:23 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/18/17 16:23 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/18/17 16:23 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 10/18/17 16:23 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 10/18/17 16:23 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/18/17 16:23 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/18/17 16:23 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/18/17 16:23 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/18/17 16:23 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 10/18/17 16:23 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 10/18/17 16:23 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 10/18/17 16:23 12-Hexanone <5.0
5.0 2.2 ug/L 10/18/17 16:23 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/18/17 16:23 1Acetone<5.0
20 4.5 ug/L 10/18/17 16:23 1Acrylonitrile<20
0.50 0.15 ug/L 10/18/17 16:23 1Benzene<0.50
1.0 0.43 ug/L 10/18/17 16:23 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/18/17 16:23 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/18/17 16:23 1Bromoform<1.0
2.0 0.80 ug/L 10/18/17 16:23 1Bromomethane<2.0
2.0 0.45 ug/L 10/18/17 16:23 1Carbon disulfide <2.0
1.0 0.38 ug/L 10/18/17 16:23 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/18/17 16:23 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/18/17 16:23 1Chloroethane<1.0
2.0 0.37 ug/L 10/18/17 16:23 1Chloroform<2.0
1.0 0.32 ug/L 10/18/17 16:23 1Chloromethane<1.0
1.0 0.41 ug/L 10/18/17 16:23 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/18/17 16:23 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/18/17 16:23 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/18/17 16:23 1Dibromomethane<1.0
0.50 0.18 ug/L 10/18/17 16:23 1Ethylbenzene<0.50
2.5 0.66 ug/L 10/18/17 16:23 1Iodomethane<2.5
5.0 1.6 ug/L 10/18/17 16:23 1Methylene Chloride <5.0
1.0 0.39 ug/L 10/18/17 16:23 1Styrene<1.0
1.0 0.37 ug/L 10/18/17 16:23 1Tetrachloroethene<1.0
10 1.9 ug/L 10/18/17 16:23 1Tetrahydrofuran<10
0.50 0.15 ug/L 10/18/17 16:23 1Toluene<0.50
1.0 0.35 ug/L 10/18/17 16:23 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/18/17 16:23 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/18/17 16:23 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/18/17 16:23 1Trichloroethene<0.50
1.0 0.43 ug/L 10/18/17 16:23 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/18/17 16:23 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/18/17 16:23 1Vinyl chloride <0.50
1.0 0.22 ug/L 10/18/17 16:23 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-14Client Sample ID: MW-9 NMLF
Matrix: WaterDate Collected: 10/10/17 13:15
Date Received: 10/11/17 10:15
1,2-Dichloroethane-d4 (Surr)94 75-126 10/18/17 16:23 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)94 10/18/17 16:23 172-124
Dibromofluoromethane 103 10/18/17 16:23 175-120
Toluene-d8 (Surr)96 10/18/17 16:23 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 10/13/17 08:45 10/16/17 19:55 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 10/13/17 08:45 10/16/17 19:55 1Arsenic<1.0
2.5 0.37 ug/L 10/13/17 08:45 10/16/17 19:55 1Barium54B
1.0 0.43 ug/L 10/13/17 08:45 10/16/17 19:55 1Beryllium<1.0
0.50 0.15 ug/L 10/13/17 08:45 10/16/17 19:55 1Cadmium<0.50
5.0 2.3 ug/L 10/13/17 08:45 10/16/17 19:55 1Chromium<5.0
1.0 0.27 ug/L 10/13/17 08:45 10/16/17 19:55 1Cobalt<1.0
2.0 0.63 ug/L 10/13/17 08:45 10/17/17 14:41 1Copper<2.0
100 38 ug/L 10/13/17 08:45 10/16/17 19:55 1Iron<100
0.50 0.16 ug/L 10/13/17 08:45 10/16/17 19:55 1Lead<0.50
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 19:55 1Manganese1.9 J
2.0 0.92 ug/L 10/13/17 08:45 10/16/17 19:55 1Nickel<2.0
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 19:55 1Selenium<2.5
0.50 0.078 ug/L 10/13/17 08:45 10/16/17 19:55 1Silver<0.50
2.0 0.65 ug/L 10/13/17 08:45 10/16/17 19:55 1Thallium<2.0
5.0 2.0 ug/L 10/13/17 08:45 10/17/17 14:41 1Vanadium2.2 J
20 8.1 ug/L 10/13/17 08:45 10/16/17 19:55 1Zinc<20
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 10/18/17 15:35 10/19/17 10:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chloride 24 2.0 1.7 mg/L 10/27/17 04:28 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.40 0.19 mg/L 10/27/17 04:16 2Sulfate15
5.0 3.7 mg/L 10/19/17 13:00 1Alkalinity52
10 4.3 mg/L 10/13/17 03:57 1Total Dissolved Solids 180
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-15Client Sample ID: SW-4
Matrix: WaterDate Collected: 10/10/17 15:30
Date Received: 10/11/17 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 16:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/18/17 16:50 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/18/17 16:50 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/18/17 16:50 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/18/17 16:50 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/18/17 16:50 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 10/18/17 16:50 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 10/18/17 16:50 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/18/17 16:50 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/18/17 16:50 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/18/17 16:50 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/18/17 16:50 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 10/18/17 16:50 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 10/18/17 16:50 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 10/18/17 16:50 12-Hexanone <5.0
5.0 2.2 ug/L 10/18/17 16:50 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/18/17 16:50 1Acetone6.8 cn
20 4.5 ug/L 10/18/17 16:50 1Acrylonitrile<20
0.50 0.15 ug/L 10/18/17 16:50 1Benzene<0.50
1.0 0.43 ug/L 10/18/17 16:50 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/18/17 16:50 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/18/17 16:50 1Bromoform<1.0
2.0 0.80 ug/L 10/18/17 16:50 1Bromomethane<2.0
2.0 0.45 ug/L 10/18/17 16:50 1Carbon disulfide <2.0
1.0 0.38 ug/L 10/18/17 16:50 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/18/17 16:50 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/18/17 16:50 1Chloroethane<1.0
2.0 0.37 ug/L 10/18/17 16:50 1Chloroform<2.0
1.0 0.32 ug/L 10/18/17 16:50 1Chloromethane<1.0
1.0 0.41 ug/L 10/18/17 16:50 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/18/17 16:50 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/18/17 16:50 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/18/17 16:50 1Dibromomethane<1.0
0.50 0.18 ug/L 10/18/17 16:50 1Ethylbenzene<0.50
2.5 0.66 ug/L 10/18/17 16:50 1Iodomethane<2.5
5.0 1.6 ug/L 10/18/17 16:50 1Methylene Chloride <5.0
1.0 0.39 ug/L 10/18/17 16:50 1Styrene<1.0
1.0 0.37 ug/L 10/18/17 16:50 1Tetrachloroethene<1.0
10 1.9 ug/L 10/18/17 16:50 1Tetrahydrofuran<10
0.50 0.15 ug/L 10/18/17 16:50 1Toluene<0.50
1.0 0.35 ug/L 10/18/17 16:50 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/18/17 16:50 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/18/17 16:50 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/18/17 16:50 1Trichloroethene<0.50
1.0 0.43 ug/L 10/18/17 16:50 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/18/17 16:50 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/18/17 16:50 1Vinyl chloride <0.50
1.0 0.22 ug/L 10/18/17 16:50 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-15Client Sample ID: SW-4
Matrix: WaterDate Collected: 10/10/17 15:30
Date Received: 10/11/17 10:15
1,2-Dichloroethane-d4 (Surr)97 75-126 10/18/17 16:50 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)93 10/18/17 16:50 172-124
Dibromofluoromethane 106 10/18/17 16:50 175-120
Toluene-d8 (Surr)93 10/18/17 16:50 175-120
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-16Client Sample ID: SW-Eff
Matrix: WaterDate Collected: 10/10/17 15:45
Date Received: 10/11/17 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 17:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/18/17 17:17 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/18/17 17:17 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/18/17 17:17 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/18/17 17:17 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/18/17 17:17 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 10/18/17 17:17 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 10/18/17 17:17 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/18/17 17:17 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/18/17 17:17 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/18/17 17:17 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/18/17 17:17 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 10/18/17 17:17 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 10/18/17 17:17 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 10/18/17 17:17 12-Hexanone <5.0
5.0 2.2 ug/L 10/18/17 17:17 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/18/17 17:17 1Acetone7.4 cn
20 4.5 ug/L 10/18/17 17:17 1Acrylonitrile<20
0.50 0.15 ug/L 10/18/17 17:17 1Benzene<0.50
1.0 0.43 ug/L 10/18/17 17:17 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/18/17 17:17 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/18/17 17:17 1Bromoform<1.0
2.0 0.80 ug/L 10/18/17 17:17 1Bromomethane<2.0
2.0 0.45 ug/L 10/18/17 17:17 1Carbon disulfide <2.0
1.0 0.38 ug/L 10/18/17 17:17 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/18/17 17:17 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/18/17 17:17 1Chloroethane<1.0
2.0 0.37 ug/L 10/18/17 17:17 1Chloroform<2.0
1.0 0.32 ug/L 10/18/17 17:17 1Chloromethane<1.0
1.0 0.41 ug/L 10/18/17 17:17 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/18/17 17:17 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/18/17 17:17 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/18/17 17:17 1Dibromomethane<1.0
0.50 0.18 ug/L 10/18/17 17:17 1Ethylbenzene<0.50
2.5 0.66 ug/L 10/18/17 17:17 1Iodomethane<2.5
5.0 1.6 ug/L 10/18/17 17:17 1Methylene Chloride <5.0
1.0 0.39 ug/L 10/18/17 17:17 1Styrene<1.0
1.0 0.37 ug/L 10/18/17 17:17 1Tetrachloroethene<1.0
10 1.9 ug/L 10/18/17 17:17 1Tetrahydrofuran<10
0.50 0.15 ug/L 10/18/17 17:17 1Toluene<0.50
1.0 0.35 ug/L 10/18/17 17:17 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/18/17 17:17 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/18/17 17:17 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/18/17 17:17 1Trichloroethene<0.50
1.0 0.43 ug/L 10/18/17 17:17 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/18/17 17:17 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/18/17 17:17 1Vinyl chloride <0.50
1.0 0.22 ug/L 10/18/17 17:17 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-16Client Sample ID: SW-Eff
Matrix: WaterDate Collected: 10/10/17 15:45
Date Received: 10/11/17 10:15
1,2-Dichloroethane-d4 (Surr)94 75-126 10/18/17 17:17 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)92 10/18/17 17:17 172-124
Dibromofluoromethane 104 10/18/17 17:17 175-120
Toluene-d8 (Surr)94 10/18/17 17:17 175-120
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-17Client Sample ID: SW-3
Matrix: WaterDate Collected: 10/10/17 16:00
Date Received: 10/11/17 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 17:44 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/18/17 17:44 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/18/17 17:44 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/18/17 17:44 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/18/17 17:44 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/18/17 17:44 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 10/18/17 17:44 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 10/18/17 17:44 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/18/17 17:44 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/18/17 17:44 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/18/17 17:44 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/18/17 17:44 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 10/18/17 17:44 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 10/18/17 17:44 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 10/18/17 17:44 12-Hexanone <5.0
5.0 2.2 ug/L 10/18/17 17:44 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/18/17 17:44 1Acetone<5.0
20 4.5 ug/L 10/18/17 17:44 1Acrylonitrile<20
0.50 0.15 ug/L 10/18/17 17:44 1Benzene<0.50
1.0 0.43 ug/L 10/18/17 17:44 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/18/17 17:44 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/18/17 17:44 1Bromoform<1.0
2.0 0.80 ug/L 10/18/17 17:44 1Bromomethane<2.0
2.0 0.45 ug/L 10/18/17 17:44 1Carbon disulfide <2.0
1.0 0.38 ug/L 10/18/17 17:44 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/18/17 17:44 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/18/17 17:44 1Chloroethane<1.0
2.0 0.37 ug/L 10/18/17 17:44 1Chloroform<2.0
1.0 0.32 ug/L 10/18/17 17:44 1Chloromethane<1.0
1.0 0.41 ug/L 10/18/17 17:44 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/18/17 17:44 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/18/17 17:44 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/18/17 17:44 1Dibromomethane<1.0
0.50 0.18 ug/L 10/18/17 17:44 1Ethylbenzene<0.50
2.5 0.66 ug/L 10/18/17 17:44 1Iodomethane<2.5
5.0 1.6 ug/L 10/18/17 17:44 1Methylene Chloride <5.0
1.0 0.39 ug/L 10/18/17 17:44 1Styrene<1.0
1.0 0.37 ug/L 10/18/17 17:44 1Tetrachloroethene<1.0
10 1.9 ug/L 10/18/17 17:44 1Tetrahydrofuran<10
0.50 0.15 ug/L 10/18/17 17:44 1Toluene<0.50
1.0 0.35 ug/L 10/18/17 17:44 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/18/17 17:44 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/18/17 17:44 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/18/17 17:44 1Trichloroethene<0.50
1.0 0.43 ug/L 10/18/17 17:44 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/18/17 17:44 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/18/17 17:44 1Vinyl chloride <0.50
1.0 0.22 ug/L 10/18/17 17:44 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-17Client Sample ID: SW-3
Matrix: WaterDate Collected: 10/10/17 16:00
Date Received: 10/11/17 10:15
1,2-Dichloroethane-d4 (Surr)95 75-126 10/18/17 17:44 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)92 10/18/17 17:44 172-124
Dibromofluoromethane 106 10/18/17 17:44 175-120
Toluene-d8 (Surr)94 10/18/17 17:44 175-120
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-18Client Sample ID: SW-2
Matrix: WaterDate Collected: 10/10/17 16:15
Date Received: 10/11/17 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 18:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/18/17 18:11 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/18/17 18:11 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/18/17 18:11 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/18/17 18:11 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/18/17 18:11 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 10/18/17 18:11 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 10/18/17 18:11 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/18/17 18:11 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/18/17 18:11 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/18/17 18:11 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/18/17 18:11 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 10/18/17 18:11 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 10/18/17 18:11 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 10/18/17 18:11 12-Hexanone <5.0
5.0 2.2 ug/L 10/18/17 18:11 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/18/17 18:11 1Acetone<5.0
20 4.5 ug/L 10/18/17 18:11 1Acrylonitrile<20
0.50 0.15 ug/L 10/18/17 18:11 1Benzene<0.50
1.0 0.43 ug/L 10/18/17 18:11 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/18/17 18:11 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/18/17 18:11 1Bromoform<1.0
2.0 0.80 ug/L 10/18/17 18:11 1Bromomethane<2.0
2.0 0.45 ug/L 10/18/17 18:11 1Carbon disulfide <2.0
1.0 0.38 ug/L 10/18/17 18:11 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/18/17 18:11 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/18/17 18:11 1Chloroethane<1.0
2.0 0.37 ug/L 10/18/17 18:11 1Chloroform<2.0
1.0 0.32 ug/L 10/18/17 18:11 1Chloromethane<1.0
1.0 0.41 ug/L 10/18/17 18:11 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/18/17 18:11 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/18/17 18:11 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/18/17 18:11 1Dibromomethane<1.0
0.50 0.18 ug/L 10/18/17 18:11 1Ethylbenzene<0.50
2.5 0.66 ug/L 10/18/17 18:11 1Iodomethane<2.5
5.0 1.6 ug/L 10/18/17 18:11 1Methylene Chloride <5.0
1.0 0.39 ug/L 10/18/17 18:11 1Styrene<1.0
1.0 0.37 ug/L 10/18/17 18:11 1Tetrachloroethene<1.0
10 1.9 ug/L 10/18/17 18:11 1Tetrahydrofuran<10
0.50 0.15 ug/L 10/18/17 18:11 1Toluene<0.50
1.0 0.35 ug/L 10/18/17 18:11 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/18/17 18:11 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/18/17 18:11 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/18/17 18:11 1Trichloroethene<0.50
1.0 0.43 ug/L 10/18/17 18:11 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/18/17 18:11 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/18/17 18:11 1Vinyl chloride <0.50
1.0 0.22 ug/L 10/18/17 18:11 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-18Client Sample ID: SW-2
Matrix: WaterDate Collected: 10/10/17 16:15
Date Received: 10/11/17 10:15
1,2-Dichloroethane-d4 (Surr)95 75-126 10/18/17 18:11 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)90 10/18/17 18:11 172-124
Dibromofluoromethane 105 10/18/17 18:11 175-120
Toluene-d8 (Surr)94 10/18/17 18:11 175-120
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-19Client Sample ID: MW-4D-1 NMLF
Matrix: WaterDate Collected: 10/10/17 08:55
Date Received: 10/11/17 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/19/17 22:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/19/17 22:41 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/19/17 22:41 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/19/17 22:41 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/19/17 22:41 11,1-Dichloroethane 0.76 J
1.0 0.39 ug/L 10/19/17 22:41 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 10/19/17 22:41 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 10/19/17 22:41 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/19/17 22:41 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/19/17 22:41 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/19/17 22:41 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/19/17 22:41 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 10/19/17 22:41 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 10/19/17 22:41 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 10/19/17 22:41 12-Hexanone <5.0
5.0 2.2 ug/L 10/19/17 22:41 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/19/17 22:41 1Acetone<5.0
20 4.5 ug/L 10/19/17 22:41 1Acrylonitrile<20
0.50 0.15 ug/L 10/19/17 22:41 1Benzene<0.50
1.0 0.43 ug/L 10/19/17 22:41 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/19/17 22:41 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/19/17 22:41 1Bromoform<1.0
2.0 0.80 ug/L 10/19/17 22:41 1Bromomethane<2.0 *
2.0 0.45 ug/L 10/19/17 22:41 1Carbon disulfide <2.0 *
1.0 0.38 ug/L 10/19/17 22:41 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/19/17 22:41 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/19/17 22:41 1Chloroethane<1.0
2.0 0.37 ug/L 10/19/17 22:41 1Chloroform<2.0
1.0 0.32 ug/L 10/19/17 22:41 1Chloromethane<1.0
1.0 0.41 ug/L 10/19/17 22:41 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/19/17 22:41 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/19/17 22:41 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/19/17 22:41 1Dibromomethane<1.0
0.50 0.18 ug/L 10/19/17 22:41 1Ethylbenzene<0.50
2.5 0.66 ug/L 10/19/17 22:41 1Iodomethane<2.5
5.0 1.6 ug/L 10/19/17 22:41 1Methylene Chloride <5.0
1.0 0.39 ug/L 10/19/17 22:41 1Styrene<1.0
1.0 0.37 ug/L 10/19/17 22:41 1Tetrachloroethene<1.0
10 1.9 ug/L 10/19/17 22:41 1Tetrahydrofuran<10
0.50 0.15 ug/L 10/19/17 22:41 1Toluene0.38 J
1.0 0.35 ug/L 10/19/17 22:41 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/19/17 22:41 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/19/17 22:41 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/19/17 22:41 1Trichloroethene<0.50
1.0 0.43 ug/L 10/19/17 22:41 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/19/17 22:41 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/19/17 22:41 1Vinyl chloride <0.50
1.0 0.22 ug/L 10/19/17 22:41 1Xylenes, Total 0.41 J
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-19Client Sample ID: MW-4D-1 NMLF
Matrix: WaterDate Collected: 10/10/17 08:55
Date Received: 10/11/17 10:15
1,2-Dichloroethane-d4 (Surr)94 75-126 10/19/17 22:41 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)93 10/19/17 22:41 172-124
Dibromofluoromethane 107 10/19/17 22:41 175-120
Toluene-d8 (Surr)93 10/19/17 22:41 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 10/13/17 08:45 10/16/17 19:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 10/13/17 08:45 10/16/17 19:59 1Arsenic3.6
2.5 0.37 ug/L 10/13/17 08:45 10/16/17 19:59 1Barium68B
1.0 0.43 ug/L 10/13/17 08:45 10/16/17 19:59 1Beryllium<1.0
0.50 0.15 ug/L 10/13/17 08:45 10/16/17 19:59 1Cadmium<0.50
5.0 2.3 ug/L 10/13/17 08:45 10/16/17 19:59 1Chromium4.3 J
1.0 0.27 ug/L 10/13/17 08:45 10/16/17 19:59 1Cobalt<1.0
2.0 0.63 ug/L 10/13/17 08:45 10/17/17 14:45 1Copper9.5
100 38 ug/L 10/13/17 08:45 10/16/17 19:59 1Iron530
0.50 0.16 ug/L 10/13/17 08:45 10/16/17 19:59 1Lead<0.50
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 19:59 1Manganese250
2.0 0.92 ug/L 10/13/17 08:45 10/16/17 19:59 1Nickel2.3
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 19:59 1Selenium<2.5
0.50 0.078 ug/L 10/13/17 08:45 10/16/17 19:59 1Silver<0.50
2.0 0.65 ug/L 10/13/17 08:45 10/16/17 19:59 1Thallium<2.0
5.0 2.0 ug/L 10/13/17 08:45 10/17/17 14:45 1Vanadium2.8 J
20 8.1 ug/L 10/13/17 08:45 10/16/17 19:59 1Zinc<20
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 10/18/17 15:35 10/19/17 10:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chloride 8.9 1.0 0.85 mg/L 10/27/17 04:53 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.20 0.095 mg/L 10/27/17 04:41 1Sulfate1.3
5.0 3.7 mg/L 10/19/17 13:07 1Alkalinity210
10 4.3 mg/L 10/13/17 04:00 1Total Dissolved Solids 250
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-20Client Sample ID: MW-11D-1 NMLF
Matrix: WaterDate Collected: 10/10/17 13:55
Date Received: 10/11/17 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/19/17 23:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/19/17 23:08 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/19/17 23:08 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/19/17 23:08 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/19/17 23:08 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/19/17 23:08 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 10/19/17 23:08 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 10/19/17 23:08 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/19/17 23:08 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/19/17 23:08 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/19/17 23:08 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/19/17 23:08 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 10/19/17 23:08 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 10/19/17 23:08 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 10/19/17 23:08 12-Hexanone <5.0
5.0 2.2 ug/L 10/19/17 23:08 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/19/17 23:08 1Acetone<5.0
20 4.5 ug/L 10/19/17 23:08 1Acrylonitrile<20
0.50 0.15 ug/L 10/19/17 23:08 1Benzene<0.50
1.0 0.43 ug/L 10/19/17 23:08 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/19/17 23:08 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/19/17 23:08 1Bromoform<1.0
2.0 0.80 ug/L 10/19/17 23:08 1Bromomethane<2.0 *
2.0 0.45 ug/L 10/19/17 23:08 1Carbon disulfide <2.0 *
1.0 0.38 ug/L 10/19/17 23:08 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/19/17 23:08 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/19/17 23:08 1Chloroethane<1.0
2.0 0.37 ug/L 10/19/17 23:08 1Chloroform<2.0
1.0 0.32 ug/L 10/19/17 23:08 1Chloromethane<1.0
1.0 0.41 ug/L 10/19/17 23:08 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/19/17 23:08 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/19/17 23:08 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/19/17 23:08 1Dibromomethane<1.0
0.50 0.18 ug/L 10/19/17 23:08 1Ethylbenzene<0.50
2.5 0.66 ug/L 10/19/17 23:08 1Iodomethane<2.5
5.0 1.6 ug/L 10/19/17 23:08 1Methylene Chloride <5.0
1.0 0.39 ug/L 10/19/17 23:08 1Styrene<1.0
1.0 0.37 ug/L 10/19/17 23:08 1Tetrachloroethene<1.0
10 1.9 ug/L 10/19/17 23:08 1Tetrahydrofuran<10
0.50 0.15 ug/L 10/19/17 23:08 1Toluene<0.50
1.0 0.35 ug/L 10/19/17 23:08 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/19/17 23:08 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/19/17 23:08 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/19/17 23:08 1Trichloroethene<0.50
1.0 0.43 ug/L 10/19/17 23:08 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/19/17 23:08 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/19/17 23:08 1Vinyl chloride <0.50
1.0 0.22 ug/L 10/19/17 23:08 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-20Client Sample ID: MW-11D-1 NMLF
Matrix: WaterDate Collected: 10/10/17 13:55
Date Received: 10/11/17 10:15
1,2-Dichloroethane-d4 (Surr)99 75-126 10/19/17 23:08 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)92 10/19/17 23:08 172-124
Dibromofluoromethane 109 10/19/17 23:08 175-120
Toluene-d8 (Surr)93 10/19/17 23:08 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 10/13/17 08:45 10/16/17 20:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 10/13/17 08:45 10/16/17 20:03 1Arsenic0.37 J
2.5 0.37 ug/L 10/13/17 08:45 10/16/17 20:03 1Barium94B
1.0 0.43 ug/L 10/13/17 08:45 10/16/17 20:03 1Beryllium<1.0
0.50 0.15 ug/L 10/13/17 08:45 10/16/17 20:03 1Cadmium<0.50
5.0 2.3 ug/L 10/13/17 08:45 10/16/17 20:03 1Chromium<5.0
1.0 0.27 ug/L 10/13/17 08:45 10/16/17 20:03 1Cobalt<1.0
2.0 0.63 ug/L 10/13/17 08:45 10/17/17 14:50 1Copper9.7
100 38 ug/L 10/13/17 08:45 10/16/17 20:03 1Iron<100
0.50 0.16 ug/L 10/13/17 08:45 10/16/17 20:03 1Lead0.16 J B
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 20:03 1Manganese7.2
2.0 0.92 ug/L 10/13/17 08:45 10/16/17 20:03 1Nickel<2.0
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 20:03 1Selenium<2.5
0.50 0.078 ug/L 10/13/17 08:45 10/16/17 20:03 1Silver<0.50
2.0 0.65 ug/L 10/13/17 08:45 10/16/17 20:03 1Thallium<2.0
5.0 2.0 ug/L 10/13/17 08:45 10/17/17 14:50 1Vanadium2.5 J
20 8.1 ug/L 10/13/17 08:45 10/16/17 20:03 1Zinc20B
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 10/18/17 15:35 10/19/17 10:25 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chloride 18 F1 F2 2.0 1.7 mg/L 10/27/17 05:30 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.0 0.95 mg/L 10/27/17 05:30 10Sulfate34F1 F2
5.0 3.7 mg/L 10/19/17 13:14 1Alkalinity290
10 4.3 mg/L 10/13/17 04:02 1Total Dissolved Solids 400
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-21Client Sample ID: MW-11D-2 NMLF
Matrix: WaterDate Collected: 10/10/17 14:50
Date Received: 10/11/17 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/19/17 23:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/19/17 23:35 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/19/17 23:35 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/19/17 23:35 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/19/17 23:35 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/19/17 23:35 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 10/19/17 23:35 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 10/19/17 23:35 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/19/17 23:35 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/19/17 23:35 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/19/17 23:35 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/19/17 23:35 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 10/19/17 23:35 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 10/19/17 23:35 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 10/19/17 23:35 12-Hexanone <5.0
5.0 2.2 ug/L 10/19/17 23:35 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/19/17 23:35 1Acetone<5.0
20 4.5 ug/L 10/19/17 23:35 1Acrylonitrile<20
0.50 0.15 ug/L 10/19/17 23:35 1Benzene<0.50
1.0 0.43 ug/L 10/19/17 23:35 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/19/17 23:35 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/19/17 23:35 1Bromoform<1.0
2.0 0.80 ug/L 10/19/17 23:35 1Bromomethane<2.0 *
2.0 0.45 ug/L 10/19/17 23:35 1Carbon disulfide <2.0 *
1.0 0.38 ug/L 10/19/17 23:35 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/19/17 23:35 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/19/17 23:35 1Chloroethane<1.0
2.0 0.37 ug/L 10/19/17 23:35 1Chloroform<2.0
1.0 0.32 ug/L 10/19/17 23:35 1Chloromethane<1.0
1.0 0.41 ug/L 10/19/17 23:35 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/19/17 23:35 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/19/17 23:35 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/19/17 23:35 1Dibromomethane<1.0
0.50 0.18 ug/L 10/19/17 23:35 1Ethylbenzene<0.50
2.5 0.66 ug/L 10/19/17 23:35 1Iodomethane<2.5
5.0 1.6 ug/L 10/19/17 23:35 1Methylene Chloride <5.0
1.0 0.39 ug/L 10/19/17 23:35 1Styrene<1.0
1.0 0.37 ug/L 10/19/17 23:35 1Tetrachloroethene<1.0
10 1.9 ug/L 10/19/17 23:35 1Tetrahydrofuran<10
0.50 0.15 ug/L 10/19/17 23:35 1Toluene<0.50
1.0 0.35 ug/L 10/19/17 23:35 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/19/17 23:35 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/19/17 23:35 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/19/17 23:35 1Trichloroethene<0.50
1.0 0.43 ug/L 10/19/17 23:35 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/19/17 23:35 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/19/17 23:35 1Vinyl chloride <0.50
1.0 0.22 ug/L 10/19/17 23:35 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-21Client Sample ID: MW-11D-2 NMLF
Matrix: WaterDate Collected: 10/10/17 14:50
Date Received: 10/11/17 10:15
1,2-Dichloroethane-d4 (Surr)95 75-126 10/19/17 23:35 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)93 10/19/17 23:35 172-124
Dibromofluoromethane 108 10/19/17 23:35 175-120
Toluene-d8 (Surr)92 10/19/17 23:35 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 10/13/17 08:45 10/16/17 20:07 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 10/13/17 08:45 10/16/17 20:07 1Arsenic<1.0
2.5 0.37 ug/L 10/13/17 08:45 10/16/17 20:07 1Barium140B
1.0 0.43 ug/L 10/13/17 08:45 10/16/17 20:07 1Beryllium<1.0
0.50 0.15 ug/L 10/13/17 08:45 10/16/17 20:07 1Cadmium<0.50
5.0 2.3 ug/L 10/13/17 08:45 10/16/17 20:07 1Chromium<5.0
1.0 0.27 ug/L 10/13/17 08:45 10/16/17 20:07 1Cobalt0.32 J
2.0 0.63 ug/L 10/13/17 08:45 10/17/17 14:54 1Copper5.0
100 38 ug/L 10/13/17 08:45 10/16/17 20:07 1Iron<100
0.50 0.16 ug/L 10/13/17 08:45 10/16/17 20:07 1Lead<0.50
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 20:07 1Manganese73
2.0 0.92 ug/L 10/13/17 08:45 10/16/17 20:07 1Nickel1.0 J
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 20:07 1Selenium<2.5
0.50 0.078 ug/L 10/13/17 08:45 10/16/17 20:07 1Silver<0.50
2.0 0.65 ug/L 10/13/17 08:45 10/16/17 20:07 1Thallium<2.0
5.0 2.0 ug/L 10/13/17 08:45 10/17/17 14:54 1Vanadium<5.0
20 8.1 ug/L 10/13/17 08:45 10/16/17 20:07 1Zinc9.2 J B
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 10/18/17 15:35 10/19/17 10:26 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chloride 3.2 0.40 0.34 mg/L 10/27/17 06:07 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.40 0.19 mg/L 10/27/17 06:07 2Sulfate10
5.0 3.7 mg/L 10/19/17 13:19 1Alkalinity48
10 4.3 mg/L 10/13/17 04:05 1Total Dissolved Solids 100
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-22Client Sample ID: MW-11A NMLF
Matrix: WaterDate Collected: 10/10/17 14:15
Date Received: 10/11/17 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/20/17 00:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/20/17 00:02 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/20/17 00:02 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/20/17 00:02 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/20/17 00:02 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/20/17 00:02 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 10/20/17 00:02 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 10/20/17 00:02 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/20/17 00:02 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/20/17 00:02 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/20/17 00:02 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/20/17 00:02 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 10/20/17 00:02 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 10/20/17 00:02 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 10/20/17 00:02 12-Hexanone <5.0
5.0 2.2 ug/L 10/20/17 00:02 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/20/17 00:02 1Acetone<5.0
20 4.5 ug/L 10/20/17 00:02 1Acrylonitrile<20
0.50 0.15 ug/L 10/20/17 00:02 1Benzene<0.50
1.0 0.43 ug/L 10/20/17 00:02 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/20/17 00:02 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/20/17 00:02 1Bromoform<1.0
2.0 0.80 ug/L 10/20/17 00:02 1Bromomethane<2.0 *
2.0 0.45 ug/L 10/20/17 00:02 1Carbon disulfide <2.0 *
1.0 0.38 ug/L 10/20/17 00:02 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/20/17 00:02 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/20/17 00:02 1Chloroethane<1.0
2.0 0.37 ug/L 10/20/17 00:02 1Chloroform<2.0
1.0 0.32 ug/L 10/20/17 00:02 1Chloromethane<1.0
1.0 0.41 ug/L 10/20/17 00:02 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/20/17 00:02 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/20/17 00:02 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/20/17 00:02 1Dibromomethane<1.0
0.50 0.18 ug/L 10/20/17 00:02 1Ethylbenzene<0.50
2.5 0.66 ug/L 10/20/17 00:02 1Iodomethane<2.5
5.0 1.6 ug/L 10/20/17 00:02 1Methylene Chloride <5.0
1.0 0.39 ug/L 10/20/17 00:02 1Styrene<1.0
1.0 0.37 ug/L 10/20/17 00:02 1Tetrachloroethene<1.0
10 1.9 ug/L 10/20/17 00:02 1Tetrahydrofuran<10
0.50 0.15 ug/L 10/20/17 00:02 1Toluene<0.50
1.0 0.35 ug/L 10/20/17 00:02 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/20/17 00:02 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/20/17 00:02 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/20/17 00:02 1Trichloroethene<0.50
1.0 0.43 ug/L 10/20/17 00:02 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/20/17 00:02 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/20/17 00:02 1Vinyl chloride <0.50
1.0 0.22 ug/L 10/20/17 00:02 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-22Client Sample ID: MW-11A NMLF
Matrix: WaterDate Collected: 10/10/17 14:15
Date Received: 10/11/17 10:15
1,2-Dichloroethane-d4 (Surr)98 75-126 10/20/17 00:02 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)94 10/20/17 00:02 172-124
Dibromofluoromethane 108 10/20/17 00:02 175-120
Toluene-d8 (Surr)94 10/20/17 00:02 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 10/13/17 08:45 10/16/17 20:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 10/13/17 08:45 10/16/17 20:10 1Arsenic<1.0
2.5 0.37 ug/L 10/13/17 08:45 10/16/17 20:10 1Barium39B
1.0 0.43 ug/L 10/13/17 08:45 10/16/17 20:10 1Beryllium<1.0
0.50 0.15 ug/L 10/13/17 08:45 10/16/17 20:10 1Cadmium<0.50
5.0 2.3 ug/L 10/13/17 08:45 10/16/17 20:10 1Chromium<5.0
1.0 0.27 ug/L 10/13/17 08:45 10/16/17 20:10 1Cobalt<1.0
2.0 0.63 ug/L 10/13/17 08:45 10/17/17 14:59 1Copper0.71 J
100 38 ug/L 10/13/17 08:45 10/16/17 20:10 1Iron<100
0.50 0.16 ug/L 10/13/17 08:45 10/16/17 20:10 1Lead<0.50
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 20:10 1Manganese3.6
2.0 0.92 ug/L 10/13/17 08:45 10/16/17 20:10 1Nickel<2.0
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 20:10 1Selenium<2.5
0.50 0.078 ug/L 10/13/17 08:45 10/16/17 20:10 1Silver<0.50
2.0 0.65 ug/L 10/13/17 08:45 10/16/17 20:10 1Thallium<2.0
5.0 2.0 ug/L 10/13/17 08:45 10/17/17 14:59 1Vanadium<5.0
20 8.1 ug/L 10/13/17 08:45 10/16/17 20:10 1Zinc<20
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 10/18/17 15:35 10/19/17 10:31 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chloride 3.4 0.40 0.34 mg/L 10/27/17 06:32 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.40 0.19 mg/L 10/27/17 06:32 2Sulfate11
5.0 3.7 mg/L 10/19/17 13:28 1Alkalinity38
10 4.3 mg/L 10/13/17 04:07 1Total Dissolved Solids 120
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-23Client Sample ID: MW-11B NMLF
Matrix: WaterDate Collected: 10/10/17 15:15
Date Received: 10/11/17 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/20/17 00:29 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/20/17 00:29 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/20/17 00:29 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/20/17 00:29 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/20/17 00:29 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/20/17 00:29 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 10/20/17 00:29 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 10/20/17 00:29 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/20/17 00:29 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/20/17 00:29 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/20/17 00:29 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/20/17 00:29 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 10/20/17 00:29 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 10/20/17 00:29 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 10/20/17 00:29 12-Hexanone <5.0
5.0 2.2 ug/L 10/20/17 00:29 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/20/17 00:29 1Acetone<5.0
20 4.5 ug/L 10/20/17 00:29 1Acrylonitrile<20
0.50 0.15 ug/L 10/20/17 00:29 1Benzene<0.50
1.0 0.43 ug/L 10/20/17 00:29 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/20/17 00:29 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/20/17 00:29 1Bromoform<1.0
2.0 0.80 ug/L 10/20/17 00:29 1Bromomethane<2.0 *
2.0 0.45 ug/L 10/20/17 00:29 1Carbon disulfide <2.0 *
1.0 0.38 ug/L 10/20/17 00:29 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/20/17 00:29 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/20/17 00:29 1Chloroethane<1.0
2.0 0.37 ug/L 10/20/17 00:29 1Chloroform<2.0
1.0 0.32 ug/L 10/20/17 00:29 1Chloromethane<1.0
1.0 0.41 ug/L 10/20/17 00:29 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/20/17 00:29 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/20/17 00:29 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/20/17 00:29 1Dibromomethane<1.0
0.50 0.18 ug/L 10/20/17 00:29 1Ethylbenzene<0.50
2.5 0.66 ug/L 10/20/17 00:29 1Iodomethane<2.5
5.0 1.6 ug/L 10/20/17 00:29 1Methylene Chloride <5.0
1.0 0.39 ug/L 10/20/17 00:29 1Styrene<1.0
1.0 0.37 ug/L 10/20/17 00:29 1Tetrachloroethene<1.0
10 1.9 ug/L 10/20/17 00:29 1Tetrahydrofuran<10
0.50 0.15 ug/L 10/20/17 00:29 1Toluene<0.50
1.0 0.35 ug/L 10/20/17 00:29 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/20/17 00:29 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/20/17 00:29 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/20/17 00:29 1Trichloroethene<0.50
1.0 0.43 ug/L 10/20/17 00:29 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/20/17 00:29 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/20/17 00:29 1Vinyl chloride <0.50
1.0 0.22 ug/L 10/20/17 00:29 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-23Client Sample ID: MW-11B NMLF
Matrix: WaterDate Collected: 10/10/17 15:15
Date Received: 10/11/17 10:15
1,2-Dichloroethane-d4 (Surr)96 75-126 10/20/17 00:29 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)94 10/20/17 00:29 172-124
Dibromofluoromethane 110 10/20/17 00:29 175-120
Toluene-d8 (Surr)92 10/20/17 00:29 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 10/13/17 08:45 10/16/17 20:14 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 10/13/17 08:45 10/16/17 20:14 1Arsenic<1.0
2.5 0.37 ug/L 10/13/17 08:45 10/16/17 20:14 1Barium85B
1.0 0.43 ug/L 10/13/17 08:45 10/16/17 20:14 1Beryllium<1.0
0.50 0.15 ug/L 10/13/17 08:45 10/16/17 20:14 1Cadmium<0.50
5.0 2.3 ug/L 10/13/17 08:45 10/16/17 20:14 1Chromium<5.0
1.0 0.27 ug/L 10/13/17 08:45 10/16/17 20:14 1Cobalt<1.0
2.0 0.63 ug/L 10/13/17 08:45 10/17/17 15:04 1Copper3.8
100 38 ug/L 10/13/17 08:45 10/16/17 20:14 1Iron57J
0.50 0.16 ug/L 10/13/17 08:45 10/16/17 20:14 1Lead<0.50
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 20:14 1Manganese13
2.0 0.92 ug/L 10/13/17 08:45 10/16/17 20:14 1Nickel<2.0
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 20:14 1Selenium<2.5
0.50 0.078 ug/L 10/13/17 08:45 10/16/17 20:14 1Silver<0.50
2.0 0.65 ug/L 10/13/17 08:45 10/16/17 20:14 1Thallium<2.0
5.0 2.0 ug/L 10/13/17 08:45 10/17/17 15:04 1Vanadium<5.0
20 8.1 ug/L 10/13/17 08:45 10/16/17 20:14 1Zinc<20
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 10/18/17 15:35 10/19/17 10:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chloride 3.6 0.20 0.17 mg/L 10/27/17 06:44 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.48 mg/L 10/27/17 06:56 5Sulfate16
5.0 3.7 mg/L 10/19/17 13:33 1Alkalinity50
10 4.3 mg/L 10/13/17 04:10 1Total Dissolved Solids 110
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-24Client Sample ID: duplicate
Matrix: WaterDate Collected: 10/10/17 10:50
Date Received: 10/11/17 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/20/17 00:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/20/17 00:56 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/20/17 00:56 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/20/17 00:56 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/20/17 00:56 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/20/17 00:56 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 10/20/17 00:56 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 10/20/17 00:56 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/20/17 00:56 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/20/17 00:56 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/20/17 00:56 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/20/17 00:56 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 10/20/17 00:56 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 10/20/17 00:56 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 10/20/17 00:56 12-Hexanone <5.0
5.0 2.2 ug/L 10/20/17 00:56 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/20/17 00:56 1Acetone<5.0
20 4.5 ug/L 10/20/17 00:56 1Acrylonitrile<20
0.50 0.15 ug/L 10/20/17 00:56 1Benzene0.98
1.0 0.43 ug/L 10/20/17 00:56 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/20/17 00:56 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/20/17 00:56 1Bromoform<1.0
2.0 0.80 ug/L 10/20/17 00:56 1Bromomethane<2.0 *
2.0 0.45 ug/L 10/20/17 00:56 1Carbon disulfide <2.0 *
1.0 0.38 ug/L 10/20/17 00:56 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/20/17 00:56 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/20/17 00:56 1Chloroethane2.1
2.0 0.37 ug/L 10/20/17 00:56 1Chloroform<2.0
1.0 0.32 ug/L 10/20/17 00:56 1Chloromethane<1.0
1.0 0.41 ug/L 10/20/17 00:56 1cis-1,2-Dichloroethene 2.6
1.0 0.42 ug/L 10/20/17 00:56 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/20/17 00:56 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/20/17 00:56 1Dibromomethane<1.0
0.50 0.18 ug/L 10/20/17 00:56 1Ethylbenzene<0.50
2.5 0.66 ug/L 10/20/17 00:56 1Iodomethane<2.5
5.0 1.6 ug/L 10/20/17 00:56 1Methylene Chloride <5.0
1.0 0.39 ug/L 10/20/17 00:56 1Styrene<1.0
1.0 0.37 ug/L 10/20/17 00:56 1Tetrachloroethene<1.0
10 1.9 ug/L 10/20/17 00:56 1Tetrahydrofuran<10
0.50 0.15 ug/L 10/20/17 00:56 1Toluene<0.50
1.0 0.35 ug/L 10/20/17 00:56 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/20/17 00:56 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/20/17 00:56 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/20/17 00:56 1Trichloroethene<0.50
1.0 0.43 ug/L 10/20/17 00:56 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/20/17 00:56 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/20/17 00:56 1Vinyl chloride 2.4
1.0 0.22 ug/L 10/20/17 00:56 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-24Client Sample ID: duplicate
Matrix: WaterDate Collected: 10/10/17 10:50
Date Received: 10/11/17 10:15
1,2-Dichloroethane-d4 (Surr)95 75-126 10/20/17 00:56 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)96 10/20/17 00:56 172-124
Dibromofluoromethane 107 10/20/17 00:56 175-120
Toluene-d8 (Surr)94 10/20/17 00:56 175-120
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-25Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 10/10/17 00:00
Date Received: 10/11/17 10:15
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/20/17 01:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/20/17 01:23 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/20/17 01:23 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/20/17 01:23 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/20/17 01:23 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/20/17 01:23 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 10/20/17 01:23 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 10/20/17 01:23 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/20/17 01:23 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/20/17 01:23 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/20/17 01:23 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/20/17 01:23 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 10/20/17 01:23 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 10/20/17 01:23 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 10/20/17 01:23 12-Hexanone <5.0
5.0 2.2 ug/L 10/20/17 01:23 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/20/17 01:23 1Acetone9.3 cn
20 4.5 ug/L 10/20/17 01:23 1Acrylonitrile<20
0.50 0.15 ug/L 10/20/17 01:23 1Benzene<0.50
1.0 0.43 ug/L 10/20/17 01:23 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/20/17 01:23 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/20/17 01:23 1Bromoform<1.0
2.0 0.80 ug/L 10/20/17 01:23 1Bromomethane<2.0 *
2.0 0.45 ug/L 10/20/17 01:23 1Carbon disulfide <2.0 *
1.0 0.38 ug/L 10/20/17 01:23 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/20/17 01:23 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/20/17 01:23 1Chloroethane<1.0
2.0 0.37 ug/L 10/20/17 01:23 1Chloroform<2.0
1.0 0.32 ug/L 10/20/17 01:23 1Chloromethane<1.0
1.0 0.41 ug/L 10/20/17 01:23 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/20/17 01:23 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/20/17 01:23 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/20/17 01:23 1Dibromomethane<1.0
0.50 0.18 ug/L 10/20/17 01:23 1Ethylbenzene<0.50
2.5 0.66 ug/L 10/20/17 01:23 1Iodomethane<2.5
5.0 1.6 ug/L 10/20/17 01:23 1Methylene Chloride <5.0
1.0 0.39 ug/L 10/20/17 01:23 1Styrene<1.0
1.0 0.37 ug/L 10/20/17 01:23 1Tetrachloroethene<1.0
10 1.9 ug/L 10/20/17 01:23 1Tetrahydrofuran<10
0.50 0.15 ug/L 10/20/17 01:23 1Toluene<0.50
1.0 0.35 ug/L 10/20/17 01:23 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/20/17 01:23 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/20/17 01:23 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/20/17 01:23 1Trichloroethene<0.50
1.0 0.43 ug/L 10/20/17 01:23 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/20/17 01:23 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/20/17 01:23 1Vinyl chloride <0.50
1.0 0.22 ug/L 10/20/17 01:23 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135435-25Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 10/10/17 00:00
Date Received: 10/11/17 10:15
1,2-Dichloroethane-d4 (Surr)97 75-126 10/20/17 01:23 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)93 10/20/17 01:23 172-124
Dibromofluoromethane 111 10/20/17 01:23 175-120
Toluene-d8 (Surr)91 10/20/17 01:23 175-120
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Definitions/Glossary
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Qualifiers
GC/MS VOA
Qualifier Description
cn Refer to Case Narrative for further detail
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
*LCS or LCSD is outside acceptance limits.
Metals
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
B Compound was found in the blank and sample.
^ICV,CCV,ICB,CCB, ISA, ISB, CRI, CRA, DLCK or MRL standard: Instrument related QC is outside acceptance limits.
General Chemistry
Qualifier Description
4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not
applicable.
Qualifier
F1 MS and/or MSD Recovery is outside acceptance limits.
F2 MS/MSD RPD exceeds control limits
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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QC Association Summary
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
GC/MS VOA
Analysis Batch: 405768
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B500-135435-1 MW-5D NMLF Total/NA
Water 8260B500-135435-2 MW-1 NMLF Total/NA
Water 8260B500-135435-3 MW-5 NMLF Total/NA
Water 8260B500-135435-4 MW-10 NMLF Total/NA
Water 8260B500-135435-5 MW-7 NMLF Total/NA
Water 8260B500-135435-6 MW-4 NMLF Total/NA
Water 8260B500-135435-7 MW-4A NMLF Total/NA
Water 8260B500-135435-8 MW-4D NMLF Total/NA
Water 8260B500-135435-9 MW-6 NMLF Total/NA
Water 8260B500-135435-10 MW-6D-1 NMLF Total/NA
Water 8260B500-135435-11 MW-6D NMLF Total/NA
Water 8260B500-135435-12 MW-7A NMLF Total/NA
Water 8260B500-135435-13 MW-7D NMLF Total/NA
Water 8260B500-135435-14 MW-9 NMLF Total/NA
Water 8260B500-135435-15 SW-4 Total/NA
Water 8260B500-135435-16 SW-Eff Total/NA
Water 8260B500-135435-17 SW-3 Total/NA
Water 8260B500-135435-18 SW-2 Total/NA
Water 8260BMB 500-405768/5 Method Blank Total/NA
Water 8260BLCS 500-405768/4 Lab Control Sample Total/NA
Analysis Batch: 406058
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B500-135435-19 MW-4D-1 NMLF Total/NA
Water 8260B500-135435-20 MW-11D-1 NMLF Total/NA
Water 8260B500-135435-21 MW-11D-2 NMLF Total/NA
Water 8260B500-135435-22 MW-11A NMLF Total/NA
Water 8260B500-135435-23 MW-11B NMLF Total/NA
Water 8260B500-135435-24 duplicate Total/NA
Water 8260B500-135435-25 Trip Blank Total/NA
Water 8260BMB 500-406058/6 Method Blank Total/NA
Water 8260BLCS 500-406058/5 Lab Control Sample Total/NA
Metals
Prep Batch: 405077
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 200.8500-135435-1 MW-5D NMLF Total/NA
Water 200.8500-135435-2 MW-1 NMLF Total/NA
Water 200.8500-135435-3 MW-5 NMLF Total/NA
Water 200.8500-135435-4 MW-10 NMLF Total/NA
Water 200.8500-135435-5 MW-7 NMLF Total/NA
Water 200.8500-135435-6 MW-4 NMLF Total/NA
Water 200.8500-135435-7 MW-4A NMLF Total/NA
Water 200.8500-135435-8 MW-4D NMLF Total/NA
Water 200.8MB 500-405077/1-A Method Blank Total/NA
Water 200.8LCS 500-405077/2-A Lab Control Sample Total/NA
Water 200.8500-135435-1 MS MW-5D NMLF Total/NA
Water 200.8500-135435-5 MS MW-7 NMLF Total/NA
Water 200.8500-135435-1 DU MW-5D NMLF Total/NA
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QC Association Summary
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Metals (Continued)
Prep Batch: 405077 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 200.8500-135435-5 DU MW-7 NMLF Total/NA
Prep Batch: 405222
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 200.8500-135435-9 MW-6 NMLF Total/NA
Water 200.8500-135435-10 MW-6D-1 NMLF Total/NA
Water 200.8500-135435-11 MW-6D NMLF Total/NA
Water 200.8500-135435-12 MW-7A NMLF Total/NA
Water 200.8500-135435-13 MW-7D NMLF Total/NA
Water 200.8500-135435-14 MW-9 NMLF Total/NA
Water 200.8500-135435-19 MW-4D-1 NMLF Total/NA
Water 200.8500-135435-20 MW-11D-1 NMLF Total/NA
Water 200.8500-135435-21 MW-11D-2 NMLF Total/NA
Water 200.8500-135435-22 MW-11A NMLF Total/NA
Water 200.8500-135435-23 MW-11B NMLF Total/NA
Water 200.8MB 500-405222/1-A Method Blank Total/NA
Water 200.8LCS 500-405222/2-A Lab Control Sample Total/NA
Water 200.8500-135435-10 MS MW-6D-1 NMLF Total/NA
Water 200.8500-135435-10 DU MW-6D-1 NMLF Total/NA
Analysis Batch: 405231
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 200.8 405077500-135435-1 MW-5D NMLF Total/NA
Water 200.8 405077500-135435-2 MW-1 NMLF Total/NA
Water 200.8 405077500-135435-3 MW-5 NMLF Total/NA
Water 200.8 405077500-135435-4 MW-10 NMLF Total/NA
Water 200.8 405077500-135435-5 MW-7 NMLF Total/NA
Water 200.8 405077500-135435-6 MW-4 NMLF Total/NA
Water 200.8 405077500-135435-7 MW-4A NMLF Total/NA
Water 200.8 405077500-135435-8 MW-4D NMLF Total/NA
Water 200.8 405077MB 500-405077/1-A Method Blank Total/NA
Water 200.8 405077LCS 500-405077/2-A Lab Control Sample Total/NA
Water 200.8 405077500-135435-1 MS MW-5D NMLF Total/NA
Water 200.8 405077500-135435-5 MS MW-7 NMLF Total/NA
Water 200.8 405077500-135435-1 DU MW-5D NMLF Total/NA
Water 200.8 405077500-135435-5 DU MW-7 NMLF Total/NA
Prep Batch: 405526
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 200.8500-135435-1 MW-5D NMLF Total/NA
Water 200.8500-135435-2 MW-1 NMLF Total/NA
Water 200.8500-135435-3 MW-5 NMLF Total/NA
Water 200.8500-135435-4 MW-10 NMLF Total/NA
Water 200.8500-135435-5 MW-7 NMLF Total/NA
Water 200.8500-135435-6 MW-4 NMLF Total/NA
Water 200.8500-135435-7 MW-4A NMLF Total/NA
Water 200.8500-135435-8 MW-4D NMLF Total/NA
Water 200.8MB 500-405526/1-A Method Blank Total/NA
Water 200.8LCS 500-405526/2-A Lab Control Sample Total/NA
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QC Association Summary
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Metals (Continued)
Analysis Batch: 405644
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 200.8 405222500-135435-9 MW-6 NMLF Total/NA
Water 200.8 405222500-135435-10 MW-6D-1 NMLF Total/NA
Water 200.8 405222500-135435-11 MW-6D NMLF Total/NA
Water 200.8 405222500-135435-12 MW-7A NMLF Total/NA
Water 200.8 405222500-135435-13 MW-7D NMLF Total/NA
Water 200.8 405222500-135435-14 MW-9 NMLF Total/NA
Water 200.8 405222500-135435-19 MW-4D-1 NMLF Total/NA
Water 200.8 405222500-135435-20 MW-11D-1 NMLF Total/NA
Water 200.8 405222500-135435-21 MW-11D-2 NMLF Total/NA
Water 200.8 405222500-135435-22 MW-11A NMLF Total/NA
Water 200.8 405222500-135435-23 MW-11B NMLF Total/NA
Water 200.8 405222MB 500-405222/1-A Method Blank Total/NA
Water 200.8 405222LCS 500-405222/2-A Lab Control Sample Total/NA
Water 200.8 405222500-135435-10 MS MW-6D-1 NMLF Total/NA
Water 200.8 405222500-135435-10 DU MW-6D-1 NMLF Total/NA
Analysis Batch: 405834
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 200.8 405222500-135435-9 MW-6 NMLF Total/NA
Water 200.8 405222500-135435-10 MW-6D-1 NMLF Total/NA
Water 200.8 405222500-135435-11 MW-6D NMLF Total/NA
Water 200.8 405222500-135435-11 MW-6D NMLF Total/NA
Water 200.8 405222500-135435-12 MW-7A NMLF Total/NA
Water 200.8 405222500-135435-13 MW-7D NMLF Total/NA
Water 200.8 405222500-135435-14 MW-9 NMLF Total/NA
Water 200.8 405222500-135435-19 MW-4D-1 NMLF Total/NA
Water 200.8 405222500-135435-20 MW-11D-1 NMLF Total/NA
Water 200.8 405222500-135435-21 MW-11D-2 NMLF Total/NA
Water 200.8 405222500-135435-22 MW-11A NMLF Total/NA
Water 200.8 405222500-135435-23 MW-11B NMLF Total/NA
Water 200.8 405222MB 500-405222/1-A Method Blank Total/NA
Water 200.8 405222LCS 500-405222/2-A Lab Control Sample Total/NA
Water 200.8 405222500-135435-10 MS MW-6D-1 NMLF Total/NA
Water 200.8 405222500-135435-10 DU MW-6D-1 NMLF Total/NA
Analysis Batch: 405836
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 200.8 405526500-135435-1 MW-5D NMLF Total/NA
Water 200.8 405526500-135435-2 MW-1 NMLF Total/NA
Water 200.8 405526500-135435-3 MW-5 NMLF Total/NA
Water 200.8 405526500-135435-4 MW-10 NMLF Total/NA
Water 200.8 405526500-135435-5 MW-7 NMLF Total/NA
Water 200.8 405526500-135435-6 MW-4 NMLF Total/NA
Water 200.8 405526500-135435-7 MW-4A NMLF Total/NA
Water 200.8 405526500-135435-8 MW-4D NMLF Total/NA
Water 200.8 405526MB 500-405526/1-A Method Blank Total/NA
Water 200.8 405526LCS 500-405526/2-A Lab Control Sample Total/NA
Prep Batch: 405903
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 245.1500-135435-1 MW-5D NMLF Total/NA
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QC Association Summary
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Metals (Continued)
Prep Batch: 405903 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 245.1500-135435-2 MW-1 NMLF Total/NA
Water 245.1500-135435-3 MW-5 NMLF Total/NA
Water 245.1500-135435-4 MW-10 NMLF Total/NA
Water 245.1500-135435-5 MW-7 NMLF Total/NA
Water 245.1500-135435-6 MW-4 NMLF Total/NA
Water 245.1500-135435-7 MW-4A NMLF Total/NA
Water 245.1500-135435-8 MW-4D NMLF Total/NA
Water 245.1500-135435-9 MW-6 NMLF Total/NA
Water 245.1500-135435-10 MW-6D-1 NMLF Total/NA
Water 245.1500-135435-11 MW-6D NMLF Total/NA
Water 245.1500-135435-12 MW-7A NMLF Total/NA
Water 245.1500-135435-13 MW-7D NMLF Total/NA
Water 245.1500-135435-14 MW-9 NMLF Total/NA
Water 245.1500-135435-19 MW-4D-1 NMLF Total/NA
Water 245.1500-135435-20 MW-11D-1 NMLF Total/NA
Water 245.1500-135435-21 MW-11D-2 NMLF Total/NA
Water 245.1500-135435-22 MW-11A NMLF Total/NA
Water 245.1500-135435-23 MW-11B NMLF Total/NA
Water 245.1MB 500-405903/12-A Method Blank Total/NA
Water 245.1LCS 500-405903/13-A Lab Control Sample Total/NA
Water 245.1500-135435-14 MS MW-9 NMLF Total/NA
Water 245.1500-135435-23 MS MW-11B NMLF Total/NA
Water 245.1500-135435-14 DU MW-9 NMLF Total/NA
Water 245.1500-135435-23 DU MW-11B NMLF Total/NA
Analysis Batch: 406044
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 245.1 405903500-135435-1 MW-5D NMLF Total/NA
Water 245.1 405903500-135435-2 MW-1 NMLF Total/NA
Water 245.1 405903500-135435-3 MW-5 NMLF Total/NA
Water 245.1 405903500-135435-4 MW-10 NMLF Total/NA
Water 245.1 405903500-135435-5 MW-7 NMLF Total/NA
Water 245.1 405903500-135435-6 MW-4 NMLF Total/NA
Water 245.1 405903500-135435-7 MW-4A NMLF Total/NA
Water 245.1 405903500-135435-8 MW-4D NMLF Total/NA
Water 245.1 405903500-135435-9 MW-6 NMLF Total/NA
Water 245.1 405903500-135435-10 MW-6D-1 NMLF Total/NA
Water 245.1 405903500-135435-11 MW-6D NMLF Total/NA
Water 245.1 405903500-135435-12 MW-7A NMLF Total/NA
Water 245.1 405903500-135435-13 MW-7D NMLF Total/NA
Water 245.1 405903500-135435-14 MW-9 NMLF Total/NA
Water 245.1 405903500-135435-19 MW-4D-1 NMLF Total/NA
Water 245.1 405903500-135435-20 MW-11D-1 NMLF Total/NA
Water 245.1 405903500-135435-21 MW-11D-2 NMLF Total/NA
Water 245.1 405903500-135435-22 MW-11A NMLF Total/NA
Water 245.1 405903500-135435-23 MW-11B NMLF Total/NA
Water 245.1 405903MB 500-405903/12-A Method Blank Total/NA
Water 245.1 405903LCS 500-405903/13-A Lab Control Sample Total/NA
Water 245.1 405903500-135435-14 MS MW-9 NMLF Total/NA
Water 245.1 405903500-135435-23 MS MW-11B NMLF Total/NA
Water 245.1 405903500-135435-14 DU MW-9 NMLF Total/NA
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QC Association Summary
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Metals (Continued)
Analysis Batch: 406044 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 245.1 405903500-135435-23 DU MW-11B NMLF Total/NA
General Chemistry
Analysis Batch: 405176
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 2540C500-135435-1 MW-5D NMLF Total/NA
Water SM 2540C500-135435-2 MW-1 NMLF Total/NA
Water SM 2540C500-135435-3 MW-5 NMLF Total/NA
Water SM 2540C500-135435-4 MW-10 NMLF Total/NA
Water SM 2540C500-135435-5 MW-7 NMLF Total/NA
Water SM 2540C500-135435-6 MW-4 NMLF Total/NA
Water SM 2540C500-135435-7 MW-4A NMLF Total/NA
Water SM 2540C500-135435-8 MW-4D NMLF Total/NA
Water SM 2540C500-135435-9 MW-6 NMLF Total/NA
Water SM 2540C500-135435-10 MW-6D-1 NMLF Total/NA
Water SM 2540C500-135435-11 MW-6D NMLF Total/NA
Water SM 2540C500-135435-12 MW-7A NMLF Total/NA
Water SM 2540C500-135435-13 MW-7D NMLF Total/NA
Water SM 2540C500-135435-14 MW-9 NMLF Total/NA
Water SM 2540C500-135435-19 MW-4D-1 NMLF Total/NA
Water SM 2540C500-135435-20 MW-11D-1 NMLF Total/NA
Water SM 2540C500-135435-21 MW-11D-2 NMLF Total/NA
Water SM 2540C500-135435-22 MW-11A NMLF Total/NA
Water SM 2540C500-135435-23 MW-11B NMLF Total/NA
Water SM 2540CMB 500-405176/1 Method Blank Total/NA
Water SM 2540CLCS 500-405176/2 Lab Control Sample Total/NA
Water SM 2540C500-135435-1 MS MW-5D NMLF Total/NA
Water SM 2540C500-135435-1 DU MW-5D NMLF Total/NA
Water SM 2540C500-135435-2 DU MW-1 NMLF Total/NA
Analysis Batch: 405996
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 2320B500-135435-1 MW-5D NMLF Total/NA
Water SM 2320B500-135435-2 MW-1 NMLF Total/NA
Water SM 2320B500-135435-3 MW-5 NMLF Total/NA
Water SM 2320B500-135435-4 MW-10 NMLF Total/NA
Water SM 2320BMB 500-405996/28 Method Blank Total/NA
Water SM 2320BMB 500-405996/3 Method Blank Total/NA
Water SM 2320BLCS 500-405996/29 Lab Control Sample Total/NA
Water SM 2320BLCS 500-405996/4 Lab Control Sample Total/NA
Water SM 2320B500-135435-3 DU MW-5 NMLF Total/NA
Analysis Batch: 406172
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 2320B500-135435-5 MW-7 NMLF Total/NA
Water SM 2320B500-135435-6 MW-4 NMLF Total/NA
Water SM 2320B500-135435-7 MW-4A NMLF Total/NA
Water SM 2320B500-135435-8 MW-4D NMLF Total/NA
Water SM 2320B500-135435-9 MW-6 NMLF Total/NA
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QC Association Summary
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
General Chemistry (Continued)
Analysis Batch: 406172 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 2320B500-135435-10 MW-6D-1 NMLF Total/NA
Water SM 2320B500-135435-11 MW-6D NMLF Total/NA
Water SM 2320B500-135435-12 MW-7A NMLF Total/NA
Water SM 2320B500-135435-13 MW-7D NMLF Total/NA
Water SM 2320B500-135435-14 MW-9 NMLF Total/NA
Water SM 2320B500-135435-19 MW-4D-1 NMLF Total/NA
Water SM 2320B500-135435-20 MW-11D-1 NMLF Total/NA
Water SM 2320B500-135435-21 MW-11D-2 NMLF Total/NA
Water SM 2320B500-135435-22 MW-11A NMLF Total/NA
Water SM 2320B500-135435-23 MW-11B NMLF Total/NA
Water SM 2320BMB 500-406172/3 Method Blank Total/NA
Water SM 2320BLCS 500-406172/4 Lab Control Sample Total/NA
Water SM 2320B500-135435-5 DU MW-7 NMLF Total/NA
Analysis Batch: 407075
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 9056A500-135435-1 MW-5D NMLF Total/NA
Water 9056A500-135435-2 MW-1 NMLF Total/NA
Water 9056A500-135435-3 MW-5 NMLF Total/NA
Water 9056AMB 500-407075/14 Method Blank Total/NA
Water 9056ALCS 500-407075/15 Lab Control Sample Total/NA
Analysis Batch: 407282
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 9056A500-135435-1 MW-5D NMLF Total/NA
Water 9056A500-135435-2 MW-1 NMLF Total/NA
Water 9056A500-135435-3 MW-5 NMLF Total/NA
Water 9056A500-135435-4 MW-10 NMLF Total/NA
Water 9056A500-135435-4 MW-10 NMLF Total/NA
Water 9056A500-135435-5 MW-7 NMLF Total/NA
Water 9056A500-135435-5 MW-7 NMLF Total/NA
Water 9056A500-135435-6 MW-4 NMLF Total/NA
Water 9056A500-135435-6 MW-4 NMLF Total/NA
Water 9056A500-135435-7 MW-4A NMLF Total/NA
Water 9056A500-135435-8 MW-4D NMLF Total/NA
Water 9056A500-135435-9 MW-6 NMLF Total/NA
Water 9056A500-135435-10 MW-6D-1 NMLF Total/NA
Water 9056A500-135435-11 MW-6D NMLF Total/NA
Water 9056A500-135435-12 MW-7A NMLF Total/NA
Water 9056A500-135435-13 MW-7D NMLF Total/NA
Water 9056A500-135435-14 MW-9 NMLF Total/NA
Water 9056A500-135435-14 MW-9 NMLF Total/NA
Water 9056A500-135435-19 MW-4D-1 NMLF Total/NA
Water 9056A500-135435-19 MW-4D-1 NMLF Total/NA
Water 9056A500-135435-20 MW-11D-1 NMLF Total/NA
Water 9056A500-135435-21 MW-11D-2 NMLF Total/NA
Water 9056A500-135435-22 MW-11A NMLF Total/NA
Water 9056A500-135435-23 MW-11B NMLF Total/NA
Water 9056A500-135435-23 MW-11B NMLF Total/NA
Water 9056AMB 500-407282/3 Method Blank Total/NA
Water 9056ALCS 500-407282/4 Lab Control Sample Total/NA
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QC Association Summary
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
General Chemistry (Continued)
Analysis Batch: 407282 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 9056A500-135435-10 MS MW-6D-1 NMLF Total/NA
Water 9056A500-135435-10 MSD MW-6D-1 NMLF Total/NA
Water 9056A500-135435-20 MS MW-11D-1 NMLF Total/NA
Water 9056A500-135435-20 MSD MW-11D-1 NMLF Total/NA
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Surrogate Summary
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (75-126)(72-124)(75-120)(75-120)
12DCE BFB DBFM TOL
88 92 98 96500-135435-1
Percent Surrogate Recovery (Acceptance Limits)
MW-5D NMLF
90 93 101 95500-135435-2 MW-1 NMLF
95 92 105 91500-135435-3 MW-5 NMLF
93 93 103 92500-135435-4 MW-10 NMLF
93 93 102 93500-135435-5 MW-7 NMLF
93 93 103 95500-135435-6 MW-4 NMLF
94 92 105 94500-135435-7 MW-4A NMLF
94 93 105 93500-135435-8 MW-4D NMLF
93 92 105 93500-135435-9 MW-6 NMLF
93 93 103 91500-135435-10 MW-6D-1 NMLF
95 94 104 92500-135435-11 MW-6D NMLF
95 91 105 90500-135435-12 MW-7A NMLF
93 92 105 96500-135435-13 MW-7D NMLF
94 94 103 96500-135435-14 MW-9 NMLF
97 93 106 93500-135435-15 SW-4
94 92 104 94500-135435-16 SW-Eff
95 92 106 94500-135435-17 SW-3
95 90 105 94500-135435-18 SW-2
94 93 107 93500-135435-19 MW-4D-1 NMLF
99 92 109 93500-135435-20 MW-11D-1 NMLF
95 93 108 92500-135435-21 MW-11D-2 NMLF
98 94 108 94500-135435-22 MW-11A NMLF
96 94 110 92500-135435-23 MW-11B NMLF
95 96 107 94500-135435-24 duplicate
97 93 111 91500-135435-25 Trip Blank
85 85 96 94LCS 500-405768/4 Lab Control Sample
88 86 100 93LCS 500-406058/5 Lab Control Sample
87 94 100 94MB 500-405768/5 Method Blank
92 95 103 95MB 500-406058/6 Method Blank
Surrogate Legend
12DCE = 1,2-Dichloroethane-d4 (Surr)
BFB = 4-Bromofluorobenzene (Surr)
DBFM = Dibromofluoromethane
TOL = Toluene-d8 (Surr)
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QC Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 500-405768/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405768
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 09:35 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<1.0 0.381.0 ug/L 10/18/17 09:35 11,1,1-Trichloroethane
<1.0 0.401.0 ug/L 10/18/17 09:35 11,1,2,2-Tetrachloroethane
<1.0 0.351.0 ug/L 10/18/17 09:35 11,1,2-Trichloroethane
<1.0 0.411.0 ug/L 10/18/17 09:35 11,1-Dichloroethane
<1.0 0.391.0 ug/L 10/18/17 09:35 11,1-Dichloroethene
<1.0 0.411.0 ug/L 10/18/17 09:35 11,2,3-Trichloropropane
<5.0 2.05.0 ug/L 10/18/17 09:35 11,2-Dibromo-3-Chloropropane
<1.0 0.391.0 ug/L 10/18/17 09:35 11,2-Dibromoethane
<1.0 0.331.0 ug/L 10/18/17 09:35 11,2-Dichlorobenzene
<1.0 0.391.0 ug/L 10/18/17 09:35 11,2-Dichloroethane
<1.0 0.431.0 ug/L 10/18/17 09:35 11,2-Dichloropropane
<1.0 0.361.0 ug/L 10/18/17 09:35 11,4-Dichlorobenzene
<5.0 2.15.0 ug/L 10/18/17 09:35 12-Butanone (MEK)
<5.0 1.65.0 ug/L 10/18/17 09:35 12-Hexanone
<5.0 2.25.0 ug/L 10/18/17 09:35 14-Methyl-2-pentanone (MIBK)
<5.0 1.75.0 ug/L 10/18/17 09:35 1Acetone
<20 4.520 ug/L 10/18/17 09:35 1Acrylonitrile
<0.50 0.150.50 ug/L 10/18/17 09:35 1Benzene
<1.0 0.431.0 ug/L 10/18/17 09:35 1Bromochloromethane
<1.0 0.371.0 ug/L 10/18/17 09:35 1Bromodichloromethane
<1.0 0.481.0 ug/L 10/18/17 09:35 1Bromoform
<2.0 0.802.0 ug/L 10/18/17 09:35 1Bromomethane
<2.0 0.452.0 ug/L 10/18/17 09:35 1Carbon disulfide
<1.0 0.381.0 ug/L 10/18/17 09:35 1Carbon tetrachloride
<1.0 0.391.0 ug/L 10/18/17 09:35 1Chlorobenzene
<1.0 0.511.0 ug/L 10/18/17 09:35 1Chloroethane
<2.0 0.372.0 ug/L 10/18/17 09:35 1Chloroform
<1.0 0.321.0 ug/L 10/18/17 09:35 1Chloromethane
<1.0 0.411.0 ug/L 10/18/17 09:35 1cis-1,2-Dichloroethene
<1.0 0.421.0 ug/L 10/18/17 09:35 1cis-1,3-Dichloropropene
<1.0 0.491.0 ug/L 10/18/17 09:35 1Dibromochloromethane
<1.0 0.271.0 ug/L 10/18/17 09:35 1Dibromomethane
<0.50 0.180.50 ug/L 10/18/17 09:35 1Ethylbenzene
<2.5 0.662.5 ug/L 10/18/17 09:35 1Iodomethane
<5.0 1.65.0 ug/L 10/18/17 09:35 1Methylene Chloride
<1.0 0.391.0 ug/L 10/18/17 09:35 1Styrene
<1.0 0.371.0 ug/L 10/18/17 09:35 1Tetrachloroethene
<10 1.910 ug/L 10/18/17 09:35 1Tetrahydrofuran
<0.50 0.150.50 ug/L 10/18/17 09:35 1Toluene
<1.0 0.351.0 ug/L 10/18/17 09:35 1trans-1,2-Dichloroethene
<1.0 0.361.0 ug/L 10/18/17 09:35 1trans-1,3-Dichloropropene
<5.0 1.25.0 ug/L 10/18/17 09:35 1trans-1,4-Dichloro-2-butene
<0.50 0.160.50 ug/L 10/18/17 09:35 1Trichloroethene
<1.0 0.431.0 ug/L 10/18/17 09:35 1Trichlorofluoromethane
<2.0 0.912.0 ug/L 10/18/17 09:35 1Vinyl acetate
<0.50 0.200.50 ug/L 10/18/17 09:35 1Vinyl chloride
<1.0 0.221.0 ug/L 10/18/17 09:35 1Xylenes, Total
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TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
1,2-Dichloroethane-d4 (Surr)87 75-126 10/18/17 09:35 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
94 10/18/17 09:35 14-Bromofluorobenzene (Surr)72-124
100 10/18/17 09:35 1Dibromofluoromethane75-120
94 10/18/17 09:35 1Toluene-d8 (Surr)75-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-405768/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405768
1,1,1,2-Tetrachloroethane 50.0 43.5 ug/L 87 70-125
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,1,1-Trichloroethane 50.0 49.4 ug/L 99 70-125
1,1,2,2-Tetrachloroethane 50.0 40.9 ug/L 82 67-127
1,1,2-Trichloroethane 50.0 39.5 ug/L 79 70-122
1,1-Dichloroethane 50.0 45.5 ug/L 91 70-125
1,1-Dichloroethene 50.0 41.6 ug/L 83 67-122
1,2,3-Trichloropropane 50.0 35.2 ug/L 70 50-133
1,2-Dibromo-3-Chloropropane 50.0 35.7 ug/L 71 56-123
1,2-Dibromoethane 50.0 38.8 ug/L 78 70-125
1,2-Dichlorobenzene 50.0 43.7 ug/L 87 70-125
1,2-Dichloroethane 50.0 40.4 ug/L 81 68-127
1,2-Dichloropropane 50.0 40.3 ug/L 81 67-130
1,4-Dichlorobenzene 50.0 44.2 ug/L 88 70-120
2-Butanone (MEK)50.0 28.4 ug/L 57 53-141
2-Hexanone 50.0 29.4 ug/L 59 56-135
4-Methyl-2-pentanone (MIBK)50.0 29.2 ug/L 58 56-133
Acetone 50.0 35.1 ug/L 70 40-143
Acrylonitrile 500 402 ug/L 80 67-140
Benzene 50.0 45.3 ug/L 91 70-120
Bromochloromethane 50.0 42.9 ug/L 86 65-122
Bromodichloromethane 50.0 43.1 ug/L 86 69-120
Bromoform 50.0 40.6 ug/L 81 56-132
Bromomethane 50.0 62.3 ug/L 125 40-130
Carbon disulfide 50.0 36.0 ug/L 72 66-120
Carbon tetrachloride 50.0 51.1 ug/L 102 65-122
Chlorobenzene 50.0 46.9 ug/L 94 70-120
Chloroethane 50.0 49.7 ug/L 99 45-127
Chloroform 50.0 47.0 ug/L 94 70-120
Chloromethane 50.0 41.0 ug/L 82 54-147
cis-1,2-Dichloroethene 50.0 46.0 ug/L 92 70-125
cis-1,3-Dichloropropene 50.0 36.8 ug/L 74 64-127
Dibromochloromethane 50.0 41.0 ug/L 82 68-125
Dibromomethane 50.0 40.2 ug/L 80 70-120
Ethylbenzene 50.0 47.5 ug/L 95 70-120
Iodomethane 50.0 38.6 ug/L 77 61-136
Methylene Chloride 50.0 45.1 ug/L 90 69-125
Styrene 50.0 48.2 ug/L 96 70-120
Tetrachloroethene 50.0 47.0 ug/L 94 70-128
Tetrahydrofuran 100 63.4 ug/L 63 59-139
Toluene 50.0 46.3 ug/L 93 70-125
trans-1,2-Dichloroethene 50.0 48.8 ug/L 98 70-125
trans-1,3-Dichloropropene 50.0 37.4 ug/L 75 62-128
trans-1,4-Dichloro-2-butene 50.0 34.7 ug/L 69 60-130
Trichloroethene 50.0 44.9 ug/L 90 70-125
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QC Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-405768/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405768
Trichlorofluoromethane 50.0 51.2 ug/L 102 70-126
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Vinyl acetate 50.0 34.0 ug/L 68 43-133
Vinyl chloride 50.0 43.0 ug/L 86 64-126
Xylenes, Total 100 96.3 ug/L 96 70-125
1,2-Dichloroethane-d4 (Surr)75 -126
Surrogate
85
LCS LCS
Qualifier Limits%Recovery
854-Bromofluorobenzene (Surr)72 -124
96Dibromofluoromethane 75 -120
94Toluene-d8 (Surr)75 -120
Client Sample ID: Method BlankLab Sample ID: MB 500-406058/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 406058
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/19/17 22:14 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<1.0 0.381.0 ug/L 10/19/17 22:14 11,1,1-Trichloroethane
<1.0 0.401.0 ug/L 10/19/17 22:14 11,1,2,2-Tetrachloroethane
<1.0 0.351.0 ug/L 10/19/17 22:14 11,1,2-Trichloroethane
<1.0 0.411.0 ug/L 10/19/17 22:14 11,1-Dichloroethane
<1.0 0.391.0 ug/L 10/19/17 22:14 11,1-Dichloroethene
<1.0 0.411.0 ug/L 10/19/17 22:14 11,2,3-Trichloropropane
<5.0 2.05.0 ug/L 10/19/17 22:14 11,2-Dibromo-3-Chloropropane
<1.0 0.391.0 ug/L 10/19/17 22:14 11,2-Dibromoethane
<1.0 0.331.0 ug/L 10/19/17 22:14 11,2-Dichlorobenzene
<1.0 0.391.0 ug/L 10/19/17 22:14 11,2-Dichloroethane
<1.0 0.431.0 ug/L 10/19/17 22:14 11,2-Dichloropropane
<1.0 0.361.0 ug/L 10/19/17 22:14 11,4-Dichlorobenzene
<5.0 2.15.0 ug/L 10/19/17 22:14 12-Butanone (MEK)
<5.0 1.65.0 ug/L 10/19/17 22:14 12-Hexanone
<5.0 2.25.0 ug/L 10/19/17 22:14 14-Methyl-2-pentanone (MIBK)
<5.0 1.75.0 ug/L 10/19/17 22:14 1Acetone
<20 4.520 ug/L 10/19/17 22:14 1Acrylonitrile
<0.50 0.150.50 ug/L 10/19/17 22:14 1Benzene
<1.0 0.431.0 ug/L 10/19/17 22:14 1Bromochloromethane
<1.0 0.371.0 ug/L 10/19/17 22:14 1Bromodichloromethane
<1.0 0.481.0 ug/L 10/19/17 22:14 1Bromoform
<2.0 0.802.0 ug/L 10/19/17 22:14 1Bromomethane
<2.0 0.452.0 ug/L 10/19/17 22:14 1Carbon disulfide
<1.0 0.381.0 ug/L 10/19/17 22:14 1Carbon tetrachloride
<1.0 0.391.0 ug/L 10/19/17 22:14 1Chlorobenzene
<1.0 0.511.0 ug/L 10/19/17 22:14 1Chloroethane
<2.0 0.372.0 ug/L 10/19/17 22:14 1Chloroform
<1.0 0.321.0 ug/L 10/19/17 22:14 1Chloromethane
<1.0 0.411.0 ug/L 10/19/17 22:14 1cis-1,2-Dichloroethene
<1.0 0.421.0 ug/L 10/19/17 22:14 1cis-1,3-Dichloropropene
<1.0 0.491.0 ug/L 10/19/17 22:14 1Dibromochloromethane
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QC Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 500-406058/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 406058
RL MDL
Dibromomethane <1.0 1.0 0.27 ug/L 10/19/17 22:14 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.50 0.180.50 ug/L 10/19/17 22:14 1Ethylbenzene
<2.5 0.662.5 ug/L 10/19/17 22:14 1Iodomethane
<5.0 1.65.0 ug/L 10/19/17 22:14 1Methylene Chloride
<1.0 0.391.0 ug/L 10/19/17 22:14 1Styrene
<1.0 0.371.0 ug/L 10/19/17 22:14 1Tetrachloroethene
<10 1.910 ug/L 10/19/17 22:14 1Tetrahydrofuran
<0.50 0.150.50 ug/L 10/19/17 22:14 1Toluene
<1.0 0.351.0 ug/L 10/19/17 22:14 1trans-1,2-Dichloroethene
<1.0 0.361.0 ug/L 10/19/17 22:14 1trans-1,3-Dichloropropene
<5.0 1.25.0 ug/L 10/19/17 22:14 1trans-1,4-Dichloro-2-butene
<0.50 0.160.50 ug/L 10/19/17 22:14 1Trichloroethene
<1.0 0.431.0 ug/L 10/19/17 22:14 1Trichlorofluoromethane
<2.0 0.912.0 ug/L 10/19/17 22:14 1Vinyl acetate
<0.50 0.200.50 ug/L 10/19/17 22:14 1Vinyl chloride
<1.0 0.221.0 ug/L 10/19/17 22:14 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)92 75-126 10/19/17 22:14 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
95 10/19/17 22:14 14-Bromofluorobenzene (Surr)72-124
103 10/19/17 22:14 1Dibromofluoromethane75-120
95 10/19/17 22:14 1Toluene-d8 (Surr)75-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-406058/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 406058
1,1,1,2-Tetrachloroethane 50.0 44.9 ug/L 90 70-125
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,1,1-Trichloroethane 50.0 55.5 ug/L 111 70-125
1,1,2,2-Tetrachloroethane 50.0 45.9 ug/L 92 67-127
1,1,2-Trichloroethane 50.0 42.4 ug/L 85 70-122
1,1-Dichloroethane 50.0 54.2 ug/L 108 70-125
1,1-Dichloroethene 50.0 57.6 ug/L 115 67-122
1,2,3-Trichloropropane 50.0 37.8 ug/L 76 50-133
1,2-Dibromo-3-Chloropropane 50.0 37.3 ug/L 75 56-123
1,2-Dibromoethane 50.0 41.6 ug/L 83 70-125
1,2-Dichlorobenzene 50.0 46.2 ug/L 92 70-125
1,2-Dichloroethane 50.0 46.1 ug/L 92 68-127
1,2-Dichloropropane 50.0 45.2 ug/L 90 67-130
1,4-Dichlorobenzene 50.0 46.4 ug/L 93 70-120
2-Butanone (MEK)50.0 36.5 ug/L 73 53-141
2-Hexanone 50.0 33.5 ug/L 67 56-135
4-Methyl-2-pentanone (MIBK)50.0 32.4 ug/L 65 56-133
Acetone 50.0 45.0 ug/L 90 40-143
Acrylonitrile 500 470 ug/L 94 67-140
Benzene 50.0 51.2 ug/L 102 70-120
Bromochloromethane 50.0 49.1 ug/L 98 65-122
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QC Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-406058/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 406058
Bromodichloromethane 50.0 47.3 ug/L 95 69-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Bromoform 50.0 41.9 ug/L 84 56-132
Bromomethane 50.0 81.2 *ug/L 162 40-130
Carbon disulfide 50.0 60.5 *ug/L 121 66-120
Carbon tetrachloride 50.0 56.4 ug/L 113 65-122
Chlorobenzene 50.0 49.2 ug/L 98 70-120
Chloroethane 50.0 62.7 ug/L 125 45-127
Chloroform 50.0 52.5 ug/L 105 70-120
Chloromethane 50.0 55.7 ug/L 111 54-147
cis-1,2-Dichloroethene 50.0 52.8 ug/L 106 70-125
cis-1,3-Dichloropropene 50.0 39.1 ug/L 78 64-127
Dibromochloromethane 50.0 42.6 ug/L 85 68-125
Dibromomethane 50.0 45.4 ug/L 91 70-120
Ethylbenzene 50.0 49.6 ug/L 99 70-120
Iodomethane 50.0 55.0 ug/L 110 61-136
Methylene Chloride 50.0 55.7 ug/L 111 69-125
Styrene 50.0 50.3 ug/L 101 70-120
Tetrachloroethene 50.0 47.4 ug/L 95 70-128
Tetrahydrofuran 100 71.6 ug/L 72 59-139
Toluene 50.0 49.7 ug/L 99 70-125
trans-1,2-Dichloroethene 50.0 57.8 ug/L 116 70-125
trans-1,3-Dichloropropene 50.0 40.2 ug/L 80 62-128
trans-1,4-Dichloro-2-butene 50.0 35.9 ug/L 72 60-130
Trichloroethene 50.0 46.9 ug/L 94 70-125
Trichlorofluoromethane 50.0 58.5 ug/L 117 70-126
Vinyl acetate 50.0 34.0 ug/L 68 43-133
Vinyl chloride 50.0 54.7 ug/L 109 64-126
Xylenes, Total 100 100 ug/L 100 70-125
1,2-Dichloroethane-d4 (Surr)75 -126
Surrogate
88
LCS LCS
Qualifier Limits%Recovery
864-Bromofluorobenzene (Surr)72 -124
100Dibromofluoromethane 75 -120
93Toluene-d8 (Surr)75 -120
Method: 200.8 - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 500-405077/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405231 Prep Batch: 405077
RL MDL
Antimony <3.0 3.0 1.3 ug/L 10/12/17 10:35 10/12/17 15:27 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<1.0 0.151.0 ug/L 10/12/17 10:35 10/12/17 15:27 1Arsenic
<2.5 0.372.5 ug/L 10/12/17 10:35 10/12/17 15:27 1Barium
<1.0 0.431.0 ug/L 10/12/17 10:35 10/12/17 15:27 1Beryllium
<0.50 0.150.50 ug/L 10/12/17 10:35 10/12/17 15:27 1Cadmium
<5.0 2.35.0 ug/L 10/12/17 10:35 10/12/17 15:27 1Chromium
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QC Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 200.8 - Metals (ICP/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 500-405077/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405231 Prep Batch: 405077
RL MDL
Cobalt <1.0 1.0 0.27 ug/L 10/12/17 10:35 10/12/17 15:27 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<100 38100 ug/L 10/12/17 10:35 10/12/17 15:27 1Iron
0.169 J 0.160.50 ug/L 10/12/17 10:35 10/12/17 15:27 1Lead
<2.5 1.12.5 ug/L 10/12/17 10:35 10/12/17 15:27 1Manganese
<2.0 0.922.0 ug/L 10/12/17 10:35 10/12/17 15:27 1Nickel
<2.5 1.12.5 ug/L 10/12/17 10:35 10/12/17 15:27 1Selenium
<0.50 0.0780.50 ug/L 10/12/17 10:35 10/12/17 15:27 1Silver
<2.0 0.652.0 ug/L 10/12/17 10:35 10/12/17 15:27 1Thallium
<5.0 2.05.0 ug/L 10/12/17 10:35 10/12/17 15:27 1Vanadium
<20 8.120 ug/L 10/12/17 10:35 10/12/17 15:27 1Zinc
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-405077/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405231 Prep Batch: 405077
Antimony 500 472 ug/L 94 85-115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Arsenic 100 95.3 ug/L 95 85-115
Barium 500 502 ug/L 100 85-115
Beryllium 50.0 47.8 ug/L 96 85-115
Cadmium 50.0 48.6 ug/L 97 85-115
Chromium 200 201 ug/L 100 85-115
Cobalt 500 506 ug/L 101 85-115
Iron 1000 1040 ug/L 104 85-115
Lead 100 98.5 ug/L 98 85-115
Manganese 500 498 ug/L 100 85-115
Nickel 500 509 ug/L 102 85-115
Selenium 100 94.5 ug/L 95 85-115
Silver 50.0 49.5 ug/L 99 85-115
Thallium 100 99.5 ug/L 99 85-115
Vanadium 500 492 ug/L 98 85-115
Zinc 500 498 ug/L 100 85-115
Client Sample ID: MW-5D NMLFLab Sample ID: 500-135435-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405231 Prep Batch: 405077
Antimony <3.0 500 474 ug/L 95 70-130
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Arsenic 0.49 J 100 94.4 ug/L 94 70-130
Barium 240 500 706 ug/L 93 70-130
Beryllium <1.0 50.0 45.1 ug/L 90 70-130
Cadmium <0.50 50.0 47.0 ug/L 94 70-130
Chromium <5.0 200 184 ug/L 92 70-130
Cobalt 0.89 J 500 457 ug/L 91 70-130
Iron 160 1000 1090 ug/L 93 70-130
Lead <0.50 100 99.6 ug/L 100 70-130
Manganese 740 500 1130 ug/L 78 70-130
Nickel 8.5 500 455 ug/L 89 70-130
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QC Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 200.8 - Metals (ICP/MS) (Continued)
Client Sample ID: MW-5D NMLFLab Sample ID: 500-135435-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405231 Prep Batch: 405077
Selenium <2.5 100 93.6 ug/L 94 70-130
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Silver <0.50 50.0 47.4 ug/L 95 70-130
Thallium <2.0 100 101 ug/L 101 70-130
Vanadium 3.2 J 500 459 ug/L 91 70-130
Zinc <20 500 464 ug/L 93 70-130
Client Sample ID: MW-7 NMLFLab Sample ID: 500-135435-5 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405231 Prep Batch: 405077
Antimony <3.0 500 487 ug/L 97 70-130
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Arsenic <1.0 100 97.0 ug/L 97 70-130
Barium 330 500 818 ug/L 98 70-130
Beryllium <1.0 50.0 45.7 ug/L 91 70-130
Cadmium <0.50 50.0 48.8 ug/L 98 70-130
Chromium 2.4 J 200 189 ug/L 93 70-130
Cobalt 0.70 J 500 463 ug/L 93 70-130
Iron 160 1000 1140 ug/L 97 70-130
Lead 0.20 J B 100 100 ug/L 100 70-130
Manganese 130 500 579 ug/L 90 70-130
Nickel <2.0 500 457 ug/L 91 70-130
Selenium <2.5 100 95.7 ug/L 96 70-130
Silver <0.50 50.0 50.1 ug/L 100 70-130
Thallium <2.0 100 102 ug/L 102 70-130
Vanadium <5.0 500 462 ug/L 92 70-130
Zinc <20 500 487 ug/L 97 70-130
Client Sample ID: MW-5D NMLFLab Sample ID: 500-135435-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405231 Prep Batch: 405077
Antimony <3.0 <3.0 ug/L NC 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Arsenic 0.49 J 0.469 J ug/L 4 20
Barium 240 217 ug/L 10 20
Beryllium <1.0 <1.0 ug/L NC 20
Cadmium <0.50 <0.50 ug/L NC 20
Chromium <5.0 <5.0 ug/L NC 20
Cobalt 0.89 J 0.804 J ug/L 11 20
Iron 160 149 ug/L 5 20
Lead <0.50 <0.50 ug/L NC 20
Manganese 740 684 ug/L 8 20
Nickel 8.5 7.75 ug/L 9 20
Selenium <2.5 <2.5 ug/L NC 20
Silver <0.50 <0.50 ug/L NC 20
Thallium <2.0 <2.0 ug/L NC 20
Vanadium 3.2 J 3.25 J ug/L 2 20
Zinc <20 <20 ug/L NC 20
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QC Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Client Sample ID: MW-7 NMLFLab Sample ID: 500-135435-5 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405231 Prep Batch: 405077
Antimony <3.0 <3.0 ug/L NC 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Arsenic <1.0 <1.0 ug/L NC 20
Barium 330 323 ug/L 1 20
Beryllium <1.0 <1.0 ug/L NC 20
Cadmium <0.50 <0.50 ug/L NC 20
Chromium 2.4 J 2.87 J ug/L 17 20
Cobalt 0.70 J 0.679 J ug/L 3 20
Iron 160 168 ug/L 3 20
Lead 0.20 J B 0.195 J ug/L 4 20
Manganese 130 127 ug/L 1 20
Nickel <2.0 <2.0 ug/L NC 20
Selenium <2.5 <2.5 ug/L NC 20
Silver <0.50 <0.50 ug/L NC 20
Thallium <2.0 <2.0 ug/L NC 20
Vanadium <5.0 <5.0 ug/L NC 20
Zinc <20 <20 ug/L NC 20
Client Sample ID: Method BlankLab Sample ID: MB 500-405222/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405644 Prep Batch: 405222
RL MDL
Antimony <3.0 3.0 1.3 ug/L 10/13/17 08:45 10/16/17 19:08 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<1.0 0.151.0 ug/L 10/13/17 08:45 10/16/17 19:08 1Arsenic
0.531 J 0.372.5 ug/L 10/13/17 08:45 10/16/17 19:08 1Barium
<1.0 0.431.0 ug/L 10/13/17 08:45 10/16/17 19:08 1Beryllium
<0.50 0.150.50 ug/L 10/13/17 08:45 10/16/17 19:08 1Cadmium
<5.0 2.35.0 ug/L 10/13/17 08:45 10/16/17 19:08 1Chromium
<1.0 0.271.0 ug/L 10/13/17 08:45 10/16/17 19:08 1Cobalt
<100 38100 ug/L 10/13/17 08:45 10/16/17 19:08 1Iron
0.311 J 0.160.50 ug/L 10/13/17 08:45 10/16/17 19:08 1Lead
<2.5 1.12.5 ug/L 10/13/17 08:45 10/16/17 19:08 1Manganese
<2.0 0.922.0 ug/L 10/13/17 08:45 10/16/17 19:08 1Nickel
1.55 J ^1.12.5 ug/L 10/13/17 08:45 10/16/17 19:08 1Selenium
<0.50 0.0780.50 ug/L 10/13/17 08:45 10/16/17 19:08 1Silver
<2.0 0.652.0 ug/L 10/13/17 08:45 10/16/17 19:08 1Thallium
14.1 J 8.120 ug/L 10/13/17 08:45 10/16/17 19:08 1Zinc
Client Sample ID: Method BlankLab Sample ID: MB 500-405222/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405834 Prep Batch: 405222
RL MDL
Copper <2.0 2.0 0.63 ug/L 10/13/17 08:45 10/17/17 13:40 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<5.0 2.05.0 ug/L 10/13/17 08:45 10/17/17 13:40 1Vanadium
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QC Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 200.8 - Metals (ICP/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-405222/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405644 Prep Batch: 405222
Antimony 500 530 ug/L 106 85-115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Arsenic 100 109 ug/L 109 85-115
Barium 500 551 ug/L 110 85-115
Beryllium 50.0 47.7 ug/L 95 85-115
Cadmium 50.0 53.2 ug/L 106 85-115
Chromium 200 203 ug/L 102 85-115
Cobalt 500 496 ug/L 99 85-115
Iron 1000 1130 ug/L 113 85-115
Lead 100 105 ug/L 105 85-115
Manganese 500 518 ug/L 104 85-115
Nickel 500 497 ug/L 99 85-115
Selenium 100 110 ^ug/L 110 85-115
Silver 50.0 53.0 ug/L 106 85-115
Thallium 100 107 ug/L 107 85-115
Zinc 500 555 ug/L 111 85-115
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-405222/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405834 Prep Batch: 405222
Copper 250 267 ug/L 107 85-115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Vanadium 500 507 ug/L 101 85-115
Client Sample ID: MW-6D-1 NMLFLab Sample ID: 500-135435-10 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405644 Prep Batch: 405222
Antimony <3.0 500 525 ug/L 105 70-130
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Arsenic 2.7 100 108 ug/L 105 70-130
Barium 380 B 500 911 ug/L 107 70-130
Beryllium <1.0 50.0 42.3 ug/L 85 70-130
Cadmium <0.50 50.0 51.5 ug/L 103 70-130
Chromium <5.0 200 192 ug/L 96 70-130
Cobalt 0.85 J 500 459 ug/L 92 70-130
Iron 3300 1000 4240 ug/L 97 70-130
Lead <0.50 100 104 ug/L 104 70-130
Manganese 310 500 791 ug/L 97 70-130
Nickel 2.0 500 455 ug/L 91 70-130
Selenium 1.3 J B ^100 104 ^ug/L 103 70-130
Silver <0.50 50.0 51.0 ug/L 102 70-130
Thallium <2.0 100 108 ug/L 108 70-130
Zinc <20 500 522 ug/L 104 70-130
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QC Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 200.8 - Metals (ICP/MS) (Continued)
Client Sample ID: MW-6D-1 NMLFLab Sample ID: 500-135435-10 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405834 Prep Batch: 405222
Copper 0.94 J 250 261 ug/L 104 70-130
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Vanadium <5.0 500 502 ug/L 100 70-130
Client Sample ID: MW-6D-1 NMLFLab Sample ID: 500-135435-10 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405644 Prep Batch: 405222
Antimony <3.0 <3.0 ug/L NC 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Arsenic 2.7 2.72 ug/L 0.8 20
Barium 380 B 376 ug/L 0.5 20
Beryllium <1.0 <1.0 ug/L NC 20
Cadmium <0.50 <0.50 ug/L NC 20
Chromium <5.0 <5.0 ug/L NC 20
Cobalt 0.85 J 0.913 J ug/L 8 20
Iron 3300 3350 ug/L 3 20
Lead <0.50 0.191 J ug/L NC 20
Manganese 310 314 ug/L 2 20
Nickel 2.0 1.85 J ug/L 9 20
Selenium 1.3 J B ^1.43 J ^ug/L 8 20
Silver <0.50 <0.50 ug/L NC 20
Thallium <2.0 <2.0 ug/L NC 20
Zinc <20 <20 ug/L NC 20
Client Sample ID: MW-6D-1 NMLFLab Sample ID: 500-135435-10 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405834 Prep Batch: 405222
Copper 0.94 J 0.913 J ug/L 3 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Vanadium <5.0 <5.0 ug/L NC 20
Client Sample ID: Method BlankLab Sample ID: MB 500-405526/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405836 Prep Batch: 405526
RL MDL
Copper <2.0 2.0 0.63 ug/L 10/16/17 11:25 10/17/17 16:21 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-405526/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405836 Prep Batch: 405526
Copper 250 261 ug/L 104 85-115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
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QC Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 245.1 - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 500-405903/12-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 406044 Prep Batch: 405903
RL MDL
Mercury <0.20 0.20 0.091 ug/L 10/18/17 15:35 10/19/17 09:46 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-405903/13-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 406044 Prep Batch: 405903
Mercury 2.00 1.89 ug/L 94 85-115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: MW-9 NMLFLab Sample ID: 500-135435-14 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 406044 Prep Batch: 405903
Mercury <0.20 1.00 1.02 ug/L 102 70-130
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: MW-11B NMLFLab Sample ID: 500-135435-23 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 406044 Prep Batch: 405903
Mercury <0.20 1.00 0.931 ug/L 93 70-130
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: MW-9 NMLFLab Sample ID: 500-135435-14 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 406044 Prep Batch: 405903
Mercury <0.20 <0.20 ug/L NC 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Client Sample ID: MW-11B NMLFLab Sample ID: 500-135435-23 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 406044 Prep Batch: 405903
Mercury <0.20 <0.20 ug/L NC 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Method: 9056A - Anions, Ion Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 500-407075/14
Matrix: Water Prep Type: Total/NA
Analysis Batch: 407075
RL MDL
Sulfate <0.20 0.20 0.095 mg/L 10/25/17 22:23 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
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QC Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 9056A - Anions, Ion Chromatography (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-407075/15
Matrix: Water Prep Type: Total/NA
Analysis Batch: 407075
Sulfate 5.00 5.36 mg/L 107 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Method BlankLab Sample ID: MB 500-407282/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 407282
RL MDL
Chloride <0.20 0.20 0.17 mg/L 10/26/17 22:05 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.20 0.0950.20 mg/L 10/26/17 22:05 1Sulfate
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-407282/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 407282
Chloride 3.00 2.97 mg/L 99 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Sulfate 5.00 5.05 mg/L 101 80-120
Client Sample ID: MW-6D-1 NMLFLab Sample ID: 500-135435-10 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 407282
Chloride 25 10.0 36.0 mg/L 106 80-120
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Sulfate 13 25.0 41.2 mg/L 113 80-120
Client Sample ID: MW-6D-1 NMLFLab Sample ID: 500-135435-10 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 407282
Chloride 25 10.0 36.2 mg/L 108 80-120 1 15
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Sulfate 13 25.0 41.8 mg/L 115 80-120 1 15
Client Sample ID: MW-11D-1 NMLFLab Sample ID: 500-135435-20 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 407282
Chloride 18 F1 F2 10.0 31.8 F1 mg/L 135 80-120
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Sulfate 34 F1 F2 25.0 70.4 F1 mg/L 146 80-120
Client Sample ID: MW-11D-1 NMLFLab Sample ID: 500-135435-20 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 407282
Chloride 18 F1 F2 10.0 23.8 F1 F2 mg/L 56 80-120 29 15
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Sulfate 34 F1 F2 25.0 48.6 F1 F2 mg/L 58 80-120 37 15
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QC Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: SM 2320B - Alkalinity
Client Sample ID: Method BlankLab Sample ID: MB 500-405996/28
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405996
RL MDL
Alkalinity <5.0 5.0 3.7 mg/L 10/18/17 16:07 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Method BlankLab Sample ID: MB 500-405996/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405996
RL MDL
Alkalinity <5.0 5.0 3.7 mg/L 10/18/17 11:00 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-405996/29
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405996
Alkalinity 100 108 mg/L 108 85-115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-405996/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405996
Alkalinity 100 106 mg/L 106 85-115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: MW-5 NMLFLab Sample ID: 500-135435-3 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405996
Alkalinity 450 446 mg/L 0.7 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Client Sample ID: Method BlankLab Sample ID: MB 500-406172/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 406172
RL MDL
Alkalinity <5.0 5.0 3.7 mg/L 10/19/17 10:58 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-406172/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 406172
Alkalinity 100 107 mg/L 107 85-115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: MW-7 NMLFLab Sample ID: 500-135435-5 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 406172
Alkalinity 440 447 mg/L 0.4 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
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QC Sample Results
TestAmerica Job ID: 500-135435-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: SM 2540C - Solids, Total Dissolved (TDS)
Client Sample ID: Method BlankLab Sample ID: MB 500-405176/1
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405176
RL MDL
Total Dissolved Solids <10 10 4.3 mg/L 10/13/17 03:11 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-405176/2
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405176
Total Dissolved Solids 250 256 mg/L 102 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: MW-5D NMLFLab Sample ID: 500-135435-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405176
Total Dissolved Solids 1300 250 1550 4 mg/L 120 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: MW-5D NMLFLab Sample ID: 500-135435-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405176
Total Dissolved Solids 1300 1250 mg/L 0.2 5
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Client Sample ID: MW-1 NMLFLab Sample ID: 500-135435-2 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405176
Total Dissolved Solids 280 296 mg/L 4 5
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
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Lab Chronicle
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-135435-1
Project/Site: NC North Mecklenburg Landfill
Client Sample ID: MW-5D NMLF Lab Sample ID: 500-135435-1
Matrix: WaterDate Collected: 10/10/17 10:50
Date Received: 10/11/17 10:15
Analysis 8260B 10/18/17 10:30 JJH1405768 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 405077 10/12/17 10:35 LWN TAL CHITotal/NA
Analysis 200.8 1 405231 10/12/17 15:47 FXG TAL CHITotal/NA
Prep 200.8 405526 10/16/17 11:25 LWN TAL CHITotal/NA
Analysis 200.8 1 405836 10/17/17 16:28 FXG TAL CHITotal/NA
Prep 245.1 405903 10/18/17 15:35 EEN TAL CHITotal/NA
Analysis 245.1 1 406044 10/19/17 09:57 EEN TAL CHITotal/NA
Analysis 9056A 25 407075 10/26/17 06:00 EAT TAL CHITotal/NA
Analysis 9056A 25 407282 10/26/17 22:30 EAT TAL CHITotal/NA
Analysis SM 2320B 1 405996 10/18/17 16:00 SMO TAL CHITotal/NA
Analysis SM 2540C 1 405176 10/13/17 03:16 CLB TAL CHITotal/NA
Client Sample ID: MW-1 NMLF Lab Sample ID: 500-135435-2
Matrix: WaterDate Collected: 10/10/17 09:50
Date Received: 10/11/17 10:15
Analysis 8260B 10/18/17 10:57 JJH1405768 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 405077 10/12/17 10:35 LWN TAL CHITotal/NA
Analysis 200.8 1 405231 10/12/17 16:02 FXG TAL CHITotal/NA
Prep 200.8 405526 10/16/17 11:25 LWN TAL CHITotal/NA
Analysis 200.8 1 405836 10/17/17 16:33 FXG TAL CHITotal/NA
Prep 245.1 405903 10/18/17 15:35 EEN TAL CHITotal/NA
Analysis 245.1 1 406044 10/19/17 09:59 EEN TAL CHITotal/NA
Analysis 9056A 20 407075 10/26/17 06:37 EAT TAL CHITotal/NA
Analysis 9056A 1 407282 10/26/17 22:42 EAT TAL CHITotal/NA
Analysis SM 2320B 1 405996 10/18/17 16:20 SMO TAL CHITotal/NA
Analysis SM 2540C 1 405176 10/13/17 03:23 CLB TAL CHITotal/NA
Client Sample ID: MW-5 NMLF Lab Sample ID: 500-135435-3
Matrix: WaterDate Collected: 10/10/17 10:30
Date Received: 10/11/17 10:15
Analysis 8260B 10/18/17 11:24 JJH1405768 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 405077 10/12/17 10:35 LWN TAL CHITotal/NA
Analysis 200.8 1 405231 10/12/17 16:06 FXG TAL CHITotal/NA
Prep 200.8 405526 10/16/17 11:25 LWN TAL CHITotal/NA
Analysis 200.8 1 405836 10/17/17 16:37 FXG TAL CHITotal/NA
Prep 245.1 405903 10/18/17 15:35 EEN TAL CHITotal/NA
Analysis 245.1 1 406044 10/19/17 10:00 EEN TAL CHITotal/NA
Analysis 9056A 25 407075 10/26/17 06:49 EAT TAL CHITotal/NA
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Lab Chronicle
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-135435-1
Project/Site: NC North Mecklenburg Landfill
Client Sample ID: MW-5 NMLF Lab Sample ID: 500-135435-3
Matrix: WaterDate Collected: 10/10/17 10:30
Date Received: 10/11/17 10:15
Analysis 9056A 10/26/17 22:55 EAT25407282 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis SM 2320B 1 405996 10/18/17 16:29 SMO TAL CHITotal/NA
Analysis SM 2540C 1 405176 10/13/17 03:29 CLB TAL CHITotal/NA
Client Sample ID: MW-10 NMLF Lab Sample ID: 500-135435-4
Matrix: WaterDate Collected: 10/10/17 11:45
Date Received: 10/11/17 10:15
Analysis 8260B 10/18/17 11:51 JJH1405768 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 405077 10/12/17 10:35 LWN TAL CHITotal/NA
Analysis 200.8 1 405231 10/12/17 16:10 FXG TAL CHITotal/NA
Prep 200.8 405526 10/16/17 11:25 LWN TAL CHITotal/NA
Analysis 200.8 1 405836 10/17/17 16:41 FXG TAL CHITotal/NA
Prep 245.1 405903 10/18/17 15:35 EEN TAL CHITotal/NA
Analysis 245.1 1 406044 10/19/17 10:02 EEN TAL CHITotal/NA
Analysis 9056A 1 407282 10/26/17 23:07 EAT TAL CHITotal/NA
Analysis 9056A 20 407282 10/26/17 23:19 EAT TAL CHITotal/NA
Analysis SM 2320B 1 405996 10/18/17 11:14 SMO TAL CHITotal/NA
Analysis SM 2540C 1 405176 10/13/17 03:31 CLB TAL CHITotal/NA
Client Sample ID: MW-7 NMLF Lab Sample ID: 500-135435-5
Matrix: WaterDate Collected: 10/10/17 16:15
Date Received: 10/11/17 10:15
Analysis 8260B 10/18/17 12:19 JJH1405768 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 405077 10/12/17 10:35 LWN TAL CHITotal/NA
Analysis 200.8 1 405231 10/12/17 16:21 FXG TAL CHITotal/NA
Prep 200.8 405526 10/16/17 11:25 LWN TAL CHITotal/NA
Analysis 200.8 1 405836 10/17/17 16:45 FXG TAL CHITotal/NA
Prep 245.1 405903 10/18/17 15:35 EEN TAL CHITotal/NA
Analysis 245.1 1 406044 10/19/17 10:03 EEN TAL CHITotal/NA
Analysis 9056A 5 407282 10/26/17 23:32 EAT TAL CHITotal/NA
Analysis 9056A 20 407282 10/26/17 23:44 EAT TAL CHITotal/NA
Analysis SM 2320B 1 406172 10/19/17 11:37 SMO TAL CHITotal/NA
Analysis SM 2540C 1 405176 10/13/17 03:34 CLB TAL CHITotal/NA
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Lab Chronicle
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-135435-1
Project/Site: NC North Mecklenburg Landfill
Client Sample ID: MW-4 NMLF Lab Sample ID: 500-135435-6
Matrix: WaterDate Collected: 10/10/17 11:45
Date Received: 10/11/17 10:15
Analysis 8260B 10/18/17 12:46 JJH1405768 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 405077 10/12/17 10:35 LWN TAL CHITotal/NA
Analysis 200.8 1 405231 10/12/17 16:36 FXG TAL CHITotal/NA
Prep 200.8 405526 10/16/17 11:25 LWN TAL CHITotal/NA
Analysis 200.8 1 405836 10/17/17 16:48 FXG TAL CHITotal/NA
Prep 245.1 405903 10/18/17 15:35 EEN TAL CHITotal/NA
Analysis 245.1 1 406044 10/19/17 10:04 EEN TAL CHITotal/NA
Analysis 9056A 2 407282 10/26/17 23:56 EAT TAL CHITotal/NA
Analysis 9056A 10 407282 10/27/17 00:33 EAT TAL CHITotal/NA
Analysis SM 2320B 1 406172 10/19/17 11:53 SMO TAL CHITotal/NA
Analysis SM 2540C 1 405176 10/13/17 03:36 CLB TAL CHITotal/NA
Client Sample ID: MW-4A NMLF Lab Sample ID: 500-135435-7
Matrix: WaterDate Collected: 10/10/17 10:35
Date Received: 10/11/17 10:15
Analysis 8260B 10/18/17 13:13 JJH1405768 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 405077 10/12/17 10:35 LWN TAL CHITotal/NA
Analysis 200.8 1 405231 10/12/17 16:40 FXG TAL CHITotal/NA
Prep 200.8 405526 10/16/17 11:25 LWN TAL CHITotal/NA
Analysis 200.8 1 405836 10/17/17 16:52 FXG TAL CHITotal/NA
Prep 245.1 405903 10/18/17 15:35 EEN TAL CHITotal/NA
Analysis 245.1 1 406044 10/19/17 10:06 EEN TAL CHITotal/NA
Analysis 9056A 2 407282 10/27/17 00:46 EAT TAL CHITotal/NA
Analysis SM 2320B 1 406172 10/19/17 11:59 SMO TAL CHITotal/NA
Analysis SM 2540C 1 405176 10/13/17 03:39 CLB TAL CHITotal/NA
Client Sample ID: MW-4D NMLF Lab Sample ID: 500-135435-8
Matrix: WaterDate Collected: 10/10/17 11:05
Date Received: 10/11/17 10:15
Analysis 8260B 10/18/17 13:40 JJH1405768 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 405077 10/12/17 10:35 LWN TAL CHITotal/NA
Analysis 200.8 1 405231 10/12/17 16:44 FXG TAL CHITotal/NA
Prep 200.8 405526 10/16/17 11:25 LWN TAL CHITotal/NA
Analysis 200.8 1 405836 10/17/17 16:56 FXG TAL CHITotal/NA
Prep 245.1 405903 10/18/17 15:35 EEN TAL CHITotal/NA
Analysis 245.1 1 406044 10/19/17 10:07 EEN TAL CHITotal/NA
Analysis 9056A 2 407282 10/27/17 01:11 EAT TAL CHITotal/NA
Analysis SM 2320B 1 406172 10/19/17 12:09 SMO TAL CHITotal/NA
TestAmerica Chicago
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Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-135435-1
Project/Site: NC North Mecklenburg Landfill
Client Sample ID: MW-4D NMLF Lab Sample ID: 500-135435-8
Matrix: WaterDate Collected: 10/10/17 11:05
Date Received: 10/11/17 10:15
Analysis SM 2540C 10/13/17 03:42 CLB1405176 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: MW-6 NMLF Lab Sample ID: 500-135435-9
Matrix: WaterDate Collected: 10/10/17 14:30
Date Received: 10/11/17 10:15
Analysis 8260B 10/18/17 14:07 JJH1405768 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405834 10/17/17 13:49 FXG TAL CHITotal/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405644 10/16/17 19:15 FXG TAL CHITotal/NA
Prep 245.1 405903 10/18/17 15:35 EEN TAL CHITotal/NA
Analysis 245.1 1 406044 10/19/17 10:09 EEN TAL CHITotal/NA
Analysis 9056A 10 407282 10/27/17 01:35 EAT TAL CHITotal/NA
Analysis SM 2320B 1 406172 10/19/17 12:19 SMO TAL CHITotal/NA
Analysis SM 2540C 1 405176 10/13/17 03:44 CLB TAL CHITotal/NA
Client Sample ID: MW-6D-1 NMLF Lab Sample ID: 500-135435-10
Matrix: WaterDate Collected: 10/10/17 14:00
Date Received: 10/11/17 10:15
Analysis 8260B 10/18/17 14:34 JJH1405768 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405834 10/17/17 13:54 FXG TAL CHITotal/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405644 10/16/17 19:19 FXG TAL CHITotal/NA
Prep 245.1 405903 10/18/17 15:35 EEN TAL CHITotal/NA
Analysis 245.1 1 406044 10/19/17 10:13 EEN TAL CHITotal/NA
Analysis 9056A 10 407282 10/27/17 02:00 EAT TAL CHITotal/NA
Analysis SM 2320B 1 406172 10/19/17 12:29 SMO TAL CHITotal/NA
Analysis SM 2540C 1 405176 10/13/17 03:47 CLB TAL CHITotal/NA
Client Sample ID: MW-6D NMLF Lab Sample ID: 500-135435-11
Matrix: WaterDate Collected: 10/10/17 13:30
Date Received: 10/11/17 10:15
Analysis 8260B 10/18/17 15:01 JJH1405768 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405834 10/17/17 14:13 FXG TAL CHITotal/NA
TestAmerica Chicago
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Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-135435-1
Project/Site: NC North Mecklenburg Landfill
Client Sample ID: MW-6D NMLF Lab Sample ID: 500-135435-11
Matrix: WaterDate Collected: 10/10/17 13:30
Date Received: 10/11/17 10:15
Prep 200.8 10/13/17 08:45 LWN405222 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 200.8 10 405834 10/17/17 14:17 FXG TAL CHITotal/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405644 10/16/17 19:35 FXG TAL CHITotal/NA
Prep 245.1 405903 10/18/17 15:35 EEN TAL CHITotal/NA
Analysis 245.1 1 406044 10/19/17 10:15 EEN TAL CHITotal/NA
Analysis 9056A 5 407282 10/27/17 03:02 EAT TAL CHITotal/NA
Analysis SM 2320B 1 406172 10/19/17 12:40 SMO TAL CHITotal/NA
Analysis SM 2540C 1 405176 10/13/17 03:49 CLB TAL CHITotal/NA
Client Sample ID: MW-7A NMLF Lab Sample ID: 500-135435-12
Matrix: WaterDate Collected: 10/10/17 15:15
Date Received: 10/11/17 10:15
Analysis 8260B 10/18/17 15:29 JJH1405768 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405834 10/17/17 14:22 FXG TAL CHITotal/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405644 10/16/17 19:39 FXG TAL CHITotal/NA
Prep 245.1 405903 10/18/17 15:35 EEN TAL CHITotal/NA
Analysis 245.1 1 406044 10/19/17 10:16 EEN TAL CHITotal/NA
Analysis 9056A 10 407282 10/27/17 03:39 EAT TAL CHITotal/NA
Analysis SM 2320B 1 406172 10/19/17 12:47 SMO TAL CHITotal/NA
Analysis SM 2540C 1 405176 10/13/17 03:52 CLB TAL CHITotal/NA
Client Sample ID: MW-7D NMLF Lab Sample ID: 500-135435-13
Matrix: WaterDate Collected: 10/10/17 15:45
Date Received: 10/11/17 10:15
Analysis 8260B 10/18/17 15:56 JJH1405768 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405834 10/17/17 14:36 FXG TAL CHITotal/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405644 10/16/17 19:51 FXG TAL CHITotal/NA
Prep 245.1 405903 10/18/17 15:35 EEN TAL CHITotal/NA
Analysis 245.1 1 406044 10/19/17 10:18 EEN TAL CHITotal/NA
Analysis 9056A 10 407282 10/27/17 03:51 EAT TAL CHITotal/NA
Analysis SM 2320B 1 406172 10/19/17 12:54 SMO TAL CHITotal/NA
Analysis SM 2540C 1 405176 10/13/17 03:54 CLB TAL CHITotal/NA
TestAmerica Chicago
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Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-135435-1
Project/Site: NC North Mecklenburg Landfill
Client Sample ID: MW-9 NMLF Lab Sample ID: 500-135435-14
Matrix: WaterDate Collected: 10/10/17 13:15
Date Received: 10/11/17 10:15
Analysis 8260B 10/18/17 16:23 JJH1405768 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405834 10/17/17 14:41 FXG TAL CHITotal/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405644 10/16/17 19:55 FXG TAL CHITotal/NA
Prep 245.1 405903 10/18/17 15:35 EEN TAL CHITotal/NA
Analysis 245.1 1 406044 10/19/17 10:19 EEN TAL CHITotal/NA
Analysis 9056A 2 407282 10/27/17 04:16 EAT TAL CHITotal/NA
Analysis 9056A 10 407282 10/27/17 04:28 EAT TAL CHITotal/NA
Analysis SM 2320B 1 406172 10/19/17 13:00 SMO TAL CHITotal/NA
Analysis SM 2540C 1 405176 10/13/17 03:57 CLB TAL CHITotal/NA
Client Sample ID: SW-4 Lab Sample ID: 500-135435-15
Matrix: WaterDate Collected: 10/10/17 15:30
Date Received: 10/11/17 10:15
Analysis 8260B 10/18/17 16:50 JJH1405768 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: SW-Eff Lab Sample ID: 500-135435-16
Matrix: WaterDate Collected: 10/10/17 15:45
Date Received: 10/11/17 10:15
Analysis 8260B 10/18/17 17:17 JJH1405768 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: SW-3 Lab Sample ID: 500-135435-17
Matrix: WaterDate Collected: 10/10/17 16:00
Date Received: 10/11/17 10:15
Analysis 8260B 10/18/17 17:44 JJH1405768 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: SW-2 Lab Sample ID: 500-135435-18
Matrix: WaterDate Collected: 10/10/17 16:15
Date Received: 10/11/17 10:15
Analysis 8260B 10/18/17 18:11 JJH1405768 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
TestAmerica Chicago
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Lab Chronicle
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-135435-1
Project/Site: NC North Mecklenburg Landfill
Client Sample ID: MW-4D-1 NMLF Lab Sample ID: 500-135435-19
Matrix: WaterDate Collected: 10/10/17 08:55
Date Received: 10/11/17 10:15
Analysis 8260B 10/19/17 22:41 EMA1406058 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405834 10/17/17 14:45 FXG TAL CHITotal/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405644 10/16/17 19:59 FXG TAL CHITotal/NA
Prep 245.1 405903 10/18/17 15:35 EEN TAL CHITotal/NA
Analysis 245.1 1 406044 10/19/17 10:23 EEN TAL CHITotal/NA
Analysis 9056A 1 407282 10/27/17 04:41 EAT TAL CHITotal/NA
Analysis 9056A 5 407282 10/27/17 04:53 EAT TAL CHITotal/NA
Analysis SM 2320B 1 406172 10/19/17 13:07 SMO TAL CHITotal/NA
Analysis SM 2540C 1 405176 10/13/17 04:00 CLB TAL CHITotal/NA
Client Sample ID: MW-11D-1 NMLF Lab Sample ID: 500-135435-20
Matrix: WaterDate Collected: 10/10/17 13:55
Date Received: 10/11/17 10:15
Analysis 8260B 10/19/17 23:08 EMA1406058 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405834 10/17/17 14:50 FXG TAL CHITotal/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405644 10/16/17 20:03 FXG TAL CHITotal/NA
Prep 245.1 405903 10/18/17 15:35 EEN TAL CHITotal/NA
Analysis 245.1 1 406044 10/19/17 10:25 EEN TAL CHITotal/NA
Analysis 9056A 10 407282 10/27/17 05:30 EAT TAL CHITotal/NA
Analysis SM 2320B 1 406172 10/19/17 13:14 SMO TAL CHITotal/NA
Analysis SM 2540C 1 405176 10/13/17 04:02 CLB TAL CHITotal/NA
Client Sample ID: MW-11D-2 NMLF Lab Sample ID: 500-135435-21
Matrix: WaterDate Collected: 10/10/17 14:50
Date Received: 10/11/17 10:15
Analysis 8260B 10/19/17 23:35 EMA1406058 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405834 10/17/17 14:54 FXG TAL CHITotal/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405644 10/16/17 20:07 FXG TAL CHITotal/NA
Prep 245.1 405903 10/18/17 15:35 EEN TAL CHITotal/NA
Analysis 245.1 1 406044 10/19/17 10:26 EEN TAL CHITotal/NA
Analysis 9056A 2 407282 10/27/17 06:07 EAT TAL CHITotal/NA
Analysis SM 2320B 1 406172 10/19/17 13:19 SMO TAL CHITotal/NA
TestAmerica Chicago
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Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-135435-1
Project/Site: NC North Mecklenburg Landfill
Client Sample ID: MW-11D-2 NMLF Lab Sample ID: 500-135435-21
Matrix: WaterDate Collected: 10/10/17 14:50
Date Received: 10/11/17 10:15
Analysis SM 2540C 10/13/17 04:05 CLB1405176 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: MW-11A NMLF Lab Sample ID: 500-135435-22
Matrix: WaterDate Collected: 10/10/17 14:15
Date Received: 10/11/17 10:15
Analysis 8260B 10/20/17 00:02 EMA1406058 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405834 10/17/17 14:59 FXG TAL CHITotal/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405644 10/16/17 20:10 FXG TAL CHITotal/NA
Prep 245.1 405903 10/18/17 15:35 EEN TAL CHITotal/NA
Analysis 245.1 1 406044 10/19/17 10:31 EEN TAL CHITotal/NA
Analysis 9056A 2 407282 10/27/17 06:32 EAT TAL CHITotal/NA
Analysis SM 2320B 1 406172 10/19/17 13:28 SMO TAL CHITotal/NA
Analysis SM 2540C 1 405176 10/13/17 04:07 CLB TAL CHITotal/NA
Client Sample ID: MW-11B NMLF Lab Sample ID: 500-135435-23
Matrix: WaterDate Collected: 10/10/17 15:15
Date Received: 10/11/17 10:15
Analysis 8260B 10/20/17 00:29 EMA1406058 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405834 10/17/17 15:04 FXG TAL CHITotal/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405644 10/16/17 20:14 FXG TAL CHITotal/NA
Prep 245.1 405903 10/18/17 15:35 EEN TAL CHITotal/NA
Analysis 245.1 1 406044 10/19/17 10:32 EEN TAL CHITotal/NA
Analysis 9056A 1 407282 10/27/17 06:44 EAT TAL CHITotal/NA
Analysis 9056A 5 407282 10/27/17 06:56 EAT TAL CHITotal/NA
Analysis SM 2320B 1 406172 10/19/17 13:33 SMO TAL CHITotal/NA
Analysis SM 2540C 1 405176 10/13/17 04:10 CLB TAL CHITotal/NA
Client Sample ID: duplicate Lab Sample ID: 500-135435-24
Matrix: WaterDate Collected: 10/10/17 10:50
Date Received: 10/11/17 10:15
Analysis 8260B 10/20/17 00:56 EMA1406058 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
TestAmerica Chicago
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Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-135435-1
Project/Site: NC North Mecklenburg Landfill
Client Sample ID: Trip Blank Lab Sample ID: 500-135435-25
Matrix: WaterDate Collected: 10/10/17 00:00
Date Received: 10/11/17 10:15
Analysis 8260B 10/20/17 01:23 EMA1406058 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Laboratory References:
TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL [phone]
TestAmerica Chicago
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Accreditation/Certification Summary
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-135435-1
Project/Site: NC North Mecklenburg Landfill
Laboratory: TestAmerica Chicago
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program EPA Region Identification Number Expiration Date
North Carolina (WW/SW)2914State Program 12-31-17 *
Analysis Method Prep Method Matrix Analyte
The following analytes are included in this report, but accreditation/certification is not offered by the governing authority:
8260B Water trans-1,4-Dichloro-2-butene
TestAmerica Chicago
* Accreditation/Certification renewal pending - accreditation/certification considered valid.
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Login Sample Receipt Checklist
Client: Civil & Environmental Consultants Inc Job Number: 500-135435-1
Login Number: 135435
Question Answer Comment
Creator: Kelsey, Shawn M
List Source: TestAmerica Chicago
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.(0.7)(0.4)c
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
TrueResidual Chlorine Checked.
TestAmerica Chicago
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ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Chicago
2417 Bond Street
University Park, IL 60484
Tel: [phone]
TestAmerica Job ID: 500-135505-1
Client Project/Site: NC North Mecklenburg Landfill
For:
Civil & Environmental Consultants Inc
1900 Center Park Drive
Suite A
Charlotte, North Carolina 28217
Attn: Bruce D. Reilly
Authorized for release by:
10/30/2017 3:25:57 PM
Robin Kintz, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
TestAmerica Job ID: 500-135505-1
Page 2 of 112 TestAmerica Chicago10/30/2017
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .64
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .65
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .72
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .75
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .101
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .107
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .108
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .112
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Case Narrative
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-135505-1
Project/Site: NC North Mecklenburg Landfill
Job ID: 500-135505-1
Laboratory: TestAmerica Chicago
Narrative
Job Narrative
500-135505-1
Comments
No additional comments.
Receipt
The samples were received on 10/12/2017 10:00 AM; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperatures of the 4 coolers at receipt time were 0.5º C, 1.8º C, 5.8º C and 5.9º C.
Receipt Exceptions
Received sample 14 not on the chain of custody (COC), added to COC and logged in. Sample 10 was listed twice on COC. MW-8 NMLF
(500-135505-10) and MW-10 Infill (500-135505-14)
GC/MS VOA
Method(s) 8260B: The method blank for batch 405855 was non-detect for all target analytes. Samples associated with this method blank
detected Acetone just above the reporting limit. Acetone is a known lab contaminant; therefore all low level detects for this compound
should be considered lab contamination. The results have been flagged with a "CN" to denote the probable contamination. MW-10 Infill
(500-135505-14)
Method(s) 8260B: The method blanks for batches 405855 and 405489 were non-detect for all target analytes. Samples associated with
the method blanks detected Methylene Chloride just above the reporting limit. Methylene Chloride is a known lab contaminant; therefore all
low level detects for this compound should be considered lab contamination. The results have been flagged with a "CN" to denote the
probable contamination. Duplicate 2 (500-135505-3),
MW-12 Infill (500-135505-4), MW-12D Infill (500-135505-5), Infill Duplicate 1 (500-135505-6) and MW-10D NMLF (500-135505-12)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC/MS Semi VOA
Method(s) 8270D: The following sample contained one acid surrogate outside acceptance limits: MW-1 Infill (500-135505-8). The
laboratory's SOP allows one acid and one base surrogate to be outside acceptance limits; therefore, re-extraction was not performed.
These results have been reported and qualified.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC Semi VOA
Method(s) 8151A: The continuing calibration verification (CCV) associated with batch 500-405510 recovered above the upper control limit
for 2,4-D, 2,4,5-T and Pentachlorophenol. The samples associated with this CCV were non-detects for the affected analytes; therefore, the
data haS been reported. The following samples are impacted: MW-14 Infill (500-135505-1), MW-8 Infill (500-135505-2), MW-12 Infill
(500-135505-4), MW-12D Infill (500-135505-5) and MW-7D Infill (500-135505-7).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
Method(s) 200.8: The continuing calibration verification (CCV) at line 59, was outside the control limits for Selenium bracketing the method
blank (MB) and laboratory control sample (LCS). The MB and LCS were within the method control limits. The associated samples were
bracketed by CCV that were within control limits. Therefore, the data have been reported
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
General Chemistry
Method(s) 9056A: Manual integration was performed on the following IC 8 samples due to the software identifying the baseline incorrectly:
(500-135505-L-8 MS) and (500-135505-L-8 MSD).
TestAmerica ChicagoPage 3 of 112 10/30/2017
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Case Narrative
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-135505-1
Project/Site: NC North Mecklenburg Landfill
Job ID: 500-135505-1 (Continued)
Laboratory: TestAmerica Chicago (Continued)
Method(s) 9056A: Manual integration was performed on the following ion chromatography samples: (500-135505-I-1 MS) and
(500-135505-I-1 MSD).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
TestAmerica ChicagoPage 4 of 112 10/30/2017
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Detection Summary
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Client Sample ID: MW-14 Infill Lab Sample ID: 500-135505-1
Arsenic
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.34 200.8
Barium 2.5 ug/L0.37 Total/NA129B200.8
Cobalt 1.0 ug/L0.27 Total/NA10.33 J 200.8
Copper 2.0 ug/L0.63 Total/NA10.66 J 200.8
Iron 100 ug/L38 Total/NA1340200.8
Lead 0.50 ug/L0.16 Total/NA10.25 J B 200.8
Manganese 2.5 ug/L1.1 Total/NA194200.8
Chloride 0.20 mg/L0.17 Total/NA16.7 9056A
Sulfate 0.40 mg/L0.19 Total/NA29.9 9056A
Alkalinity 5.0 mg/L3.7 Total/NA165SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1140SM 2540C
Client Sample ID: MW-8 Infill Lab Sample ID: 500-135505-2
Di-n-butyl phthalate
RL
3.8 ug/L
MDL
0.56
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.61 8270D
PCB-1260 0.40 ug/L0.071 Total/NA10.37 J 8082A
Barium 2.5 ug/L0.37 Total/NA141B200.8
Cobalt 1.0 ug/L0.27 Total/NA11.4 200.8
Copper 2.0 ug/L0.63 Total/NA11.1 J 200.8
Iron 100 ug/L38 Total/NA1440200.8
Lead 0.50 ug/L0.16 Total/NA10.16 J B 200.8
Manganese 2.5 ug/L1.1 Total/NA1110200.8
Nickel 2.0 ug/L0.92 Total/NA11.4 J 200.8
Vanadium 5.0 ug/L2.0 Total/NA15.1 200.8
Chloride 5.0 mg/L4.3 Total/NA25929056A
Sulfate 0.20 mg/L0.095 Total/NA18.4 9056A
Alkalinity 5.0 mg/L3.7 Total/NA1150SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1390SM 2540C
Client Sample ID: Duplicate 2 Lab Sample ID: 500-135505-3
Benzene
RL
0.50 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA10.61 8260B
cis-1,2-Dichloroethene 1.0 ug/L0.41 Total/NA11.7 8260B
Methylene Chloride 5.0 ug/L1.6 Total/NA15.4 cn 8260B
Vinyl chloride 0.50 ug/L0.20 Total/NA12.3 8260B
Client Sample ID: MW-12 Infill Lab Sample ID: 500-135505-4
Benzene
RL
0.50 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA10.66 8260B
Methylene Chloride 5.0 ug/L1.6 Total/NA15.8 cn 8260B
Vinyl chloride 0.50 ug/L0.20 Total/NA12.7 8260B
Arsenic 1.0 ug/L0.15 Total/NA10.19 J 200.8
Barium 2.5 ug/L0.37 Total/NA1240B200.8
Chromium 5.0 ug/L2.3 Total/NA13.3 J 200.8
Cobalt 1.0 ug/L0.27 Total/NA18.7 200.8
Copper 2.0 ug/L0.63 Total/NA14.7 200.8
Iron 100 ug/L38 Total/NA1930200.8
TestAmerica Chicago
This Detection Summary does not include radiochemical test results.
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Detection Summary
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Client Sample ID: MW-12 Infill (Continued)Lab Sample ID: 500-135505-4
Lead
RL
0.50 ug/L
MDL
0.16
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1B0.85 200.8
Manganese 2.5 ug/L1.1 Total/NA1340V200.8
Nickel 2.0 ug/L0.92 Total/NA111200.8
Vanadium 5.0 ug/L2.0 Total/NA12.3 J 200.8
Zinc 20 ug/L8.1 Total/NA126B200.8
Chloride 2.0 mg/L1.7 Total/NA10369056A
Sulfate 2.0 mg/L0.95 Total/NA10759056A
Alkalinity 5.0 mg/L3.7 Total/NA1480SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1700SM 2540C
Client Sample ID: MW-12D Infill Lab Sample ID: 500-135505-5
Benzene
RL
0.50 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA10.50 8260B
Methylene Chloride 5.0 ug/L1.6 Total/NA14.8 J cn 8260B
Tetrahydrofuran 10 ug/L1.9 Total/NA14.1 J 8260B
Vinyl chloride 0.50 ug/L0.20 Total/NA11.7 8260B
Benzo[a]anthracene 0.15 ug/L0.042 Total/NA10.16 8270D
Benzo[a]pyrene 0.15 ug/L0.073 Total/NA10.18 8270D
Benzo[b]fluoranthene 0.15 ug/L0.060 Total/NA10.26 8270D
Benzo[k]fluoranthene 0.15 ug/L0.047 Total/NA10.093 J 8270D
Chrysene 0.15 ug/L0.050 Total/NA10.18 8270D
Di-n-butyl phthalate 3.7 ug/L0.54 Total/NA10.73 J 8270D
Indeno[1,2,3-cd]pyrene 0.15 ug/L0.055 Total/NA10.13 J 8270D
Arsenic 1.0 ug/L0.15 Total/NA13.1 200.8
Barium 2.5 ug/L0.37 Total/NA1210B200.8
Cobalt 1.0 ug/L0.27 Total/NA12.3 200.8
Copper 2.0 ug/L0.63 Total/NA12.5 200.8
Iron 100 ug/L38 Total/NA17000200.8
Lead 0.50 ug/L0.16 Total/NA10.65 B 200.8
Manganese 2.5 ug/L1.1 Total/NA1480200.8
Nickel 2.0 ug/L0.92 Total/NA14.1 200.8
Zinc 20 ug/L8.1 Total/NA127B200.8
Chloride 2.0 mg/L1.7 Total/NA10349056A
Sulfate 2.0 mg/L0.95 Total/NA10529056A
Alkalinity 5.0 mg/L3.7 Total/NA1580SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1780SM 2540C
Client Sample ID: Infill Duplicate 1 Lab Sample ID: 500-135505-6
Benzene
RL
0.50 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA10.54 8260B
Methylene Chloride 5.0 ug/L1.6 Total/NA15.2 cn 8260B
Vinyl chloride 0.50 ug/L0.20 Total/NA11.7 8260B
Client Sample ID: MW-7D Infill Lab Sample ID: 500-135505-7
Benzene
RL
0.50 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA10.78 8260B
Tetrahydrofuran 10 ug/L1.9 Total/NA1118260B
TestAmerica Chicago
This Detection Summary does not include radiochemical test results.
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Detection Summary
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Client Sample ID: MW-7D Infill (Continued)Lab Sample ID: 500-135505-7
Antimony
RL
3.0 ug/L
MDL
1.3
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J1.8 200.8
Arsenic 1.0 ug/L0.15 Total/NA11.1 200.8
Barium 2.5 ug/L0.37 Total/NA1270B200.8
Chromium 5.0 ug/L2.3 Total/NA16.2 200.8
Cobalt 1.0 ug/L0.27 Total/NA12.4 200.8
Copper 2.0 ug/L0.63 Total/NA12.6 200.8
Iron 100 ug/L38 Total/NA13000200.8
Lead 0.50 ug/L0.16 Total/NA10.44 J B 200.8
Manganese 2.5 ug/L1.1 Total/NA11200200.8
Nickel 2.0 ug/L0.92 Total/NA114200.8
Vanadium 5.0 ug/L2.0 Total/NA12.1 J 200.8
Zinc 20 ug/L8.1 Total/NA113J B 200.8
Chloride 5.0 mg/L4.3 Total/NA25899056A
Sulfate 5.0 mg/L2.4 Total/NA251309056A
Alkalinity 5.0 mg/L3.7 Total/NA1730SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA11200SM 2540C
Client Sample ID: MW-1 Infill Lab Sample ID: 500-135505-8
Bis(2-ethylhexyl) phthalate
RL
7.6 ug/L
MDL
1.3
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J1.6 8270D
Arsenic 1.0 ug/L0.15 Total/NA12.6 200.8
Barium 2.5 ug/L0.37 Total/NA1250B200.8
Beryllium 1.0 ug/L0.43 Total/NA10.94 J 200.8
Cadmium 0.50 ug/L0.15 Total/NA10.23 J 200.8
Chromium 5.0 ug/L2.3 Total/NA1140200.8
Cobalt 1.0 ug/L0.27 Total/NA122200.8
Copper 2.0 ug/L0.63 Total/NA167B200.8
Iron 100 ug/L38 Total/NA140000B200.8
Lead 0.50 ug/L0.16 Total/NA111B200.8
Manganese 2.5 ug/L1.1 Total/NA11200200.8
Nickel 2.0 ug/L0.92 Total/NA188200.8
Selenium 2.5 ug/L1.1 Total/NA11.6 J B 200.8
Vanadium 5.0 ug/L2.0 Total/NA171200.8
Zinc 20 ug/L8.1 Total/NA1120B200.8
Chloride 1.0 mg/L0.85 Total/NA5219056A
Sulfate 1.0 mg/L0.48 Total/NA5139056A
Alkalinity 5.0 mg/L3.7 Total/NA1210SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1320SM 2540C
Client Sample ID: TB Lab Sample ID: 500-135505-9
No Detections.
Client Sample ID: MW-8 NMLF Lab Sample ID: 500-135505-10
Arsenic
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA11.5 200.8
Barium 2.5 ug/L0.37 Total/NA1140B200.8
Beryllium 1.0 ug/L0.43 Total/NA10.64 J 200.8
Cadmium 0.50 ug/L0.15 Total/NA10.52 200.8
TestAmerica Chicago
This Detection Summary does not include radiochemical test results.
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Detection Summary
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Client Sample ID: MW-8 NMLF (Continued)Lab Sample ID: 500-135505-10
Chromium
RL
5.0 ug/L
MDL
2.3
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1870200.8
Cobalt 1.0 ug/L0.27 Total/NA137200.8
Copper 2.0 ug/L0.63 Total/NA1110B200.8
Iron 100 ug/L38 Total/NA129000B200.8
Lead 0.50 ug/L0.16 Total/NA113B200.8
Manganese 2.5 ug/L1.1 Total/NA14300200.8
Nickel 2.0 ug/L0.92 Total/NA1470200.8
Selenium 2.5 ug/L1.1 Total/NA12.3 J B 200.8
Vanadium 5.0 ug/L2.0 Total/NA172200.8
Zinc 20 ug/L8.1 Total/NA179B200.8
Chloride 1.0 mg/L0.85 Total/NA5129056A
Sulfate 1.0 mg/L0.48 Total/NA5469056A
Alkalinity 5.0 mg/L3.7 Total/NA1290SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1420SM 2540C
Client Sample ID: MW-8D NMLF Lab Sample ID: 500-135505-11
Arsenic
RL
1.0 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.15 200.8
Barium 2.5 ug/L0.37 Total/NA1110200.8
Chromium 5.0 ug/L2.3 Total/NA113200.8
Cobalt 1.0 ug/L0.27 Total/NA13.3 200.8
Copper 2.0 ug/L0.63 Total/NA17.9 200.8
Iron 100 ug/L38 Total/NA14300200.8
Lead 0.50 ug/L0.16 Total/NA10.74 200.8
Manganese 2.5 ug/L1.1 Total/NA1260200.8
Nickel 2.0 ug/L0.92 Total/NA112200.8
Vanadium 5.0 ug/L2.0 Total/NA111200.8
Zinc 20 ug/L8.1 Total/NA116J200.8
Chloride 5.0 mg/L4.3 Total/NA25829056A
Sulfate 0.40 mg/L0.19 Total/NA2159056A
Alkalinity 5.0 mg/L3.7 Total/NA1400SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1570SM 2540C
Client Sample ID: MW-10D NMLF Lab Sample ID: 500-135505-12
1,4-Dichlorobenzene
RL
1.0 ug/L
MDL
0.36
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA11.8 8260B
Benzene 0.50 ug/L0.15 Total/NA13.2 8260B
Methylene Chloride 5.0 ug/L1.6 Total/NA17.5 cn 8260B
Tetrahydrofuran 10 ug/L1.9 Total/NA1798260B
Arsenic 1.0 ug/L0.15 Total/NA11.6 200.8
Barium 2.5 ug/L0.37 Total/NA1210200.8
Cadmium 0.50 ug/L0.15 Total/NA13.1 200.8
Chromium 5.0 ug/L2.3 Total/NA16.6 200.8
Cobalt 1.0 ug/L0.27 Total/NA149200.8
Copper 2.0 ug/L0.63 Total/NA11800200.8
Iron 100 ug/L38 Total/NA12700200.8
Lead 0.50 ug/L0.16 Total/NA12.9 200.8
Manganese 50 ug/L22 Total/NA2017000200.8
TestAmerica Chicago
This Detection Summary does not include radiochemical test results.
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Detection Summary
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Client Sample ID: MW-10D NMLF (Continued)Lab Sample ID: 500-135505-12
Nickel
RL
2.0 ug/L
MDL
0.92
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA160200.8
Selenium 2.5 ug/L1.1 Total/NA11.2 J 200.8
Silver 0.50 ug/L0.078 Total/NA10.12 J 200.8
Vanadium 5.0 ug/L2.0 Total/NA120200.8
Zinc 20 ug/L8.1 Total/NA145200.8
Mercury 0.20 ug/L0.091 Total/NA10.16 J 245.1
Chloride 10 mg/L8.5 Total/NA502009056A
Sulfate 10 mg/L4.8 Total/NA501409056A
Alkalinity 5.0 mg/L3.7 Total/NA11700SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA12500SM 2540C
Client Sample ID: MW-11 NMLF Lab Sample ID: 500-135505-13
Benzene
RL
0.50 ug/L
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA10.90 8260B
Tetrahydrofuran 10 ug/L1.9 Total/NA1178260B
Arsenic 1.0 ug/L0.15 Total/NA10.52 J 200.8
Barium 2.5 ug/L0.37 Total/NA1270200.8
Cadmium 0.50 ug/L0.15 Total/NA10.45 J 200.8
Chromium 5.0 ug/L2.3 Total/NA151200.8
Cobalt 1.0 ug/L0.27 Total/NA13.1 200.8
Copper 2.0 ug/L0.63 Total/NA136200.8
Iron 100 ug/L38 Total/NA1750200.8
Lead 0.50 ug/L0.16 Total/NA10.76 200.8
Manganese 2.5 ug/L1.1 Total/NA12500200.8
Nickel 2.0 ug/L0.92 Total/NA153200.8
Vanadium 5.0 ug/L2.0 Total/NA17.0 200.8
Zinc 20 ug/L8.1 Total/NA151200.8
Chloride 2.0 mg/L1.7 Total/NA10519056A
Sulfate 5.0 mg/L2.4 Total/NA25969056A
Alkalinity 5.0 mg/L3.7 Total/NA11100SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA11400SM 2540C
Client Sample ID: MW-10 Infill Lab Sample ID: 500-135505-14
Acetone
RL
5.0 ug/L
MDL
1.7
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1cn158260B
Tetrahydrofuran 10 ug/L1.9 Total/NA15.2 J 8260B
TestAmerica Chicago
This Detection Summary does not include radiochemical test results.
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Method Summary
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL CHI
SW8468270DSemivolatile Organic Compounds (GC/MS)TAL CHI
SW8468081BOrganochlorine Pesticides (GC)TAL CHI
SW8468082APolychlorinated Biphenyls (PCBs) by Gas Chromatography TAL CHI
SW8468151AHerbicides (GC)TAL CHI
EPA200.8 Metals (ICP/MS)TAL CHI
EPA245.1 Mercury (CVAA)TAL CHI
SW8469014Cyanide TAL CHI
SW8469056AAnions, Ion Chromatography TAL CHI
SMSM 2320B Alkalinity TAL CHI
SMSM 2540C Solids, Total Dissolved (TDS)TAL CHI
Protocol References:
EPA = US Environmental Protection Agency
SM = "Standard Methods For The Examination Of Water And Wastewater",
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL [phone]
TestAmerica Chicago
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Sample Summary
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
500-135505-1 MW-14 Infill Water 10/11/17 16:10 10/12/17 10:00
500-135505-2 MW-8 Infill Water 10/11/17 15:00 10/12/17 10:00
500-135505-3 Duplicate 2 Water 10/11/17 13:15 10/12/17 10:00
500-135505-4 MW-12 Infill Water 10/11/17 13:15 10/12/17 10:00
500-135505-5 MW-12D Infill Water 10/11/17 12:30 10/12/17 10:00
500-135505-6 Infill Duplicate 1 Water 10/11/17 12:30 10/12/17 10:00
500-135505-7 MW-7D Infill Water 10/11/17 14:40 10/12/17 10:00
500-135505-8 MW-1 Infill Water 10/11/17 15:40 10/12/17 10:00
500-135505-9 TB Water 10/11/17 00:00 10/12/17 10:00
500-135505-10 MW-8 NMLF Water 10/11/17 10:40 10/12/17 10:00
500-135505-11 MW-8D NMLF Water 10/11/17 10:10 10/12/17 10:00
500-135505-12 MW-10D NMLF Water 10/11/17 11:25 10/12/17 10:00
500-135505-13 MW-11 NMLF Water 10/11/17 12:25 10/12/17 10:00
500-135505-14 MW-10 Infill Water 10/11/17 13:45 10/12/17 10:00
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-1Client Sample ID: MW-14 Infill
Matrix: WaterDate Collected: 10/11/17 16:10
Date Received: 10/12/17 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 16:22 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/18/17 16:22 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/18/17 16:22 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/18/17 16:22 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/18/17 16:22 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/18/17 16:22 11,1-Dichloroethene <1.0
1.0 0.30 ug/L 10/18/17 16:22 11,1-Dichloropropene <1.0
1.0 0.41 ug/L 10/18/17 16:22 11,2,3-Trichloropropane <1.0
1.0 0.34 ug/L 10/18/17 16:22 11,2,4-Trichlorobenzene <1.0
5.0 2.0 ug/L 10/18/17 16:22 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/18/17 16:22 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/18/17 16:22 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/18/17 16:22 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/18/17 16:22 11,2-Dichloropropane <1.0
1.0 0.40 ug/L 10/18/17 16:22 11,3-Dichlorobenzene <1.0
1.0 0.36 ug/L 10/18/17 16:22 11,3-Dichloropropane <1.0
1.0 0.36 ug/L 10/18/17 16:22 11,4-Dichlorobenzene <1.0
1.0 0.44 ug/L 10/18/17 16:22 12,2-Dichloropropane <1.0
5.0 2.1 ug/L 10/18/17 16:22 12-Butanone (MEK)<5.0
1.0 0.23 ug/L 10/18/17 16:22 12-Chloro-1,3-butadiene <1.0
5.0 1.6 ug/L 10/18/17 16:22 12-Hexanone <5.0
2.5 0.86 ug/L 10/18/17 16:22 13-Chloropropene <2.5
5.0 2.2 ug/L 10/18/17 16:22 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/18/17 16:22 1Acetone<5.0
10 4.2 ug/L 10/18/17 16:22 1Acetonitrile<10
100 23 ug/L 10/18/17 16:22 1Acrolein<100
20 4.5 ug/L 10/18/17 16:22 1Acrylonitrile<20
0.50 0.15 ug/L 10/18/17 16:22 1Benzene<0.50
1.0 0.43 ug/L 10/18/17 16:22 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/18/17 16:22 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/18/17 16:22 1Bromoform<1.0
2.0 0.80 ug/L 10/18/17 16:22 1Bromomethane<2.0
2.0 0.45 ug/L 10/18/17 16:22 1Carbon disulfide <2.0
1.0 0.38 ug/L 10/18/17 16:22 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/18/17 16:22 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/18/17 16:22 1Chloroethane<1.0
2.0 0.37 ug/L 10/18/17 16:22 1Chloroform<2.0
1.0 0.32 ug/L 10/18/17 16:22 1Chloromethane<1.0
1.0 0.41 ug/L 10/18/17 16:22 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/18/17 16:22 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/18/17 16:22 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/18/17 16:22 1Dibromomethane<1.0
2.0 0.67 ug/L 10/18/17 16:22 1Dichlorodifluoromethane<2.0
2.5 0.53 ug/L 10/18/17 16:22 1Ethyl methacrylate <2.5
0.50 0.18 ug/L 10/18/17 16:22 1Ethylbenzene<0.50
1.0 0.45 ug/L 10/18/17 16:22 1Hexachlorobutadiene<1.0
2.5 0.66 ug/L 10/18/17 16:22 1Iodomethane<2.5
100 36 ug/L 10/18/17 16:22 1Isobutyl alcohol <100
10 2.5 ug/L 10/18/17 16:22 1Methacrylonitrile<10
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-1Client Sample ID: MW-14 Infill
Matrix: WaterDate Collected: 10/11/17 16:10
Date Received: 10/12/17 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Methyl methacrylate <2.5 2.5 0.55 ug/L 10/18/17 16:22 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.0 1.6 ug/L 10/18/17 16:22 1Methylene Chloride <5.0
10 4.8 ug/L 10/18/17 16:22 1Propionitrile<10
1.0 0.39 ug/L 10/18/17 16:22 1Styrene<1.0
1.0 0.37 ug/L 10/18/17 16:22 1Tetrachloroethene<1.0
10 1.9 ug/L 10/18/17 16:22 1Tetrahydrofuran<10
0.50 0.15 ug/L 10/18/17 16:22 1Toluene<0.50
1.0 0.35 ug/L 10/18/17 16:22 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/18/17 16:22 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/18/17 16:22 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/18/17 16:22 1Trichloroethene<0.50
1.0 0.43 ug/L 10/18/17 16:22 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/18/17 16:22 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/18/17 16:22 1Vinyl chloride <0.50
1.0 0.22 ug/L 10/18/17 16:22 1Xylenes, Total <1.0
1,2-Dichloroethane-d4 (Surr)107 75-126 10/18/17 16:22 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)96 10/18/17 16:22 172-124
Dibromofluoromethane 99 10/18/17 16:22 175-120
Toluene-d8 (Surr)94 10/18/17 16:22 175-120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.85 0.85 0.26 ug/L 10/16/17 07:32 10/18/17 22:37 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.85 0.23 ug/L 10/16/17 07:32 10/18/17 22:37 1Acenaphthylene<0.85
4.3 0.57 ug/L 10/16/17 07:32 10/18/17 22:37 1Acetophenone<4.3
8.5 1.8 ug/L 10/16/17 07:32 10/18/17 22:37 12-Acetylaminofluorene <8.5
8.5 3.2 ug/L 10/16/17 07:32 10/18/17 22:37 14-Aminobiphenyl <8.5
0.85 0.29 ug/L 10/16/17 07:32 10/18/17 22:37 1Anthracene<0.85
0.17 0.048 ug/L 10/16/17 07:32 10/18/17 22:37 1Benzo[a]anthracene <0.17
0.17 0.084 ug/L 10/16/17 07:32 10/18/17 22:37 1Benzo[a]pyrene <0.17
0.17 0.069 ug/L 10/16/17 07:32 10/18/17 22:37 1Benzo[b]fluoranthene <0.17
0.85 0.32 ug/L 10/16/17 07:32 10/18/17 22:37 1Benzo[g,h,i]perylene <0.85
0.17 0.055 ug/L 10/16/17 07:32 10/18/17 22:37 1Benzo[k]fluoranthene <0.17
17 5.2 ug/L 10/16/17 07:32 10/18/17 22:37 1Benzyl alcohol <17
1.7 0.24 ug/L 10/16/17 07:32 10/18/17 22:37 1Bis(2-chloroethoxy)methane <1.7
1.7 0.25 ug/L 10/16/17 07:32 10/18/17 22:37 1Bis(2-chloroethyl)ether <1.7
8.5 1.5 ug/L 10/16/17 07:32 10/18/17 22:37 1Bis(2-ethylhexyl) phthalate <8.5
4.3 0.46 ug/L 10/16/17 07:32 10/18/17 22:37 14-Bromophenyl phenyl ether <4.3
1.7 0.41 ug/L 10/16/17 07:32 10/18/17 22:37 1Butyl benzyl phthalate <1.7
8.5 1.7 ug/L 10/16/17 07:32 10/18/17 22:37 14-Chloroaniline <8.5
8.5 2.9 ug/L 10/16/17 07:32 10/18/17 22:37 1Chlorobenzilate<8.5
8.5 2.0 ug/L 10/16/17 07:32 10/18/17 22:37 14-Chloro-3-methylphenol <8.5
1.7 0.20 ug/L 10/16/17 07:32 10/18/17 22:37 12-Chloronaphthalene <1.7
4.3 0.48 ug/L 10/16/17 07:32 10/18/17 22:37 12-Chlorophenol <4.3
4.3 0.54 ug/L 10/16/17 07:32 10/18/17 22:37 14-Chlorophenyl phenyl ether <4.3
0.17 0.058 ug/L 10/16/17 07:32 10/18/17 22:37 1Chrysene<0.17
8.5 4.7 ug/L 10/16/17 07:32 10/18/17 22:37 1Diallate<8.5
0.26 0.043 ug/L 10/16/17 07:32 10/18/17 22:37 1Dibenz(a,h)anthracene <0.26
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-1Client Sample ID: MW-14 Infill
Matrix: WaterDate Collected: 10/11/17 16:10
Date Received: 10/12/17 10:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
Dibenzofuran <1.7 1.7 0.22 ug/L 10/16/17 07:32 10/18/17 22:37 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4.3 1.5 ug/L 10/16/17 07:32 10/18/17 22:37 13,3'-Dichlorobenzidine <4.3
8.5 2.2 ug/L 10/16/17 07:32 10/18/17 22:37 12,4-Dichlorophenol <8.5
8.5 3.0 ug/L 10/16/17 07:32 10/18/17 22:37 12,6-Dichlorophenol <8.5
4.3 0.31 ug/L 10/16/17 07:32 10/18/17 22:37 1Diethyl phthalate <4.3
8.5 1.6 ug/L 10/16/17 07:32 10/18/17 22:37 1Dimethoate<8.5
34 2.6 ug/L 10/16/17 07:32 10/18/17 22:37 17,12-Dimethylbenz(a)anthracene <34
34 15 ug/L 10/16/17 07:32 10/18/17 22:37 13,3'-Dimethylbenzidine <34
8.5 1.5 ug/L 10/16/17 07:32 10/18/17 22:37 12,4-Dimethylphenol <8.5
4.3 0.27 ug/L 10/16/17 07:32 10/18/17 22:37 1Dimethyl phthalate <4.3
4.3 0.62 ug/L 10/16/17 07:32 10/18/17 22:37 1Di-n-butyl phthalate <4.3
17 5.0 ug/L 10/16/17 07:32 10/18/17 22:37 14,6-Dinitro-2-methylphenol <17
17 7.3 ug/L 10/16/17 07:32 10/18/17 22:37 12,4-Dinitrophenol <17
0.85 0.21 ug/L 10/16/17 07:32 10/18/17 22:37 12,4-Dinitrotoluene <0.85
0.85 0.063 ug/L 10/16/17 07:32 10/18/17 22:37 12,6-Dinitrotoluene <0.85
8.5 0.90 ug/L 10/16/17 07:32 10/18/17 22:37 1Di-n-octyl phthalate <8.5
8.5 2.2 ug/L 10/16/17 07:32 10/18/17 22:37 1Diphenylamine<8.5
8.5 1.6 ug/L 10/16/17 07:32 10/18/17 22:37 1Disulfoton<8.5
17 3.2 ug/L 10/16/17 07:32 10/18/17 22:37 1Ethyl methanesulfonate <17
8.5 1.8 ug/L 10/16/17 07:32 10/18/17 22:37 1Ethyl Parathion <8.5
34 26 ug/L 10/16/17 07:32 10/18/17 22:37 1Famphur<34
0.85 0.39 ug/L 10/16/17 07:32 10/18/17 22:37 1Fluoranthene<0.85
0.85 0.21 ug/L 10/16/17 07:32 10/18/17 22:37 1Fluorene<0.85
0.43 0.068 ug/L 10/16/17 07:32 10/18/17 22:37 1Hexachlorobenzene<0.43
17 5.4 ug/L 10/16/17 07:32 10/18/17 22:37 1Hexachlorocyclopentadiene<17
4.3 0.51 ug/L 10/16/17 07:32 10/18/17 22:37 1Hexachloroethane<4.3
17 4.0 ug/L 10/16/17 07:32 10/18/17 22:37 1Hexachloropropene<17
0.17 0.064 ug/L 10/16/17 07:32 10/18/17 22:37 1Indeno[1,2,3-cd]pyrene <0.17
17 5.9 ug/L 10/16/17 07:32 10/18/17 22:37 1Isodrin<17
1.7 0.32 ug/L 10/16/17 07:32 10/18/17 22:37 1Isophorone<1.7
8.5 3.3 ug/L 10/16/17 07:32 10/18/17 22:37 1Isosafrole<8.5
8.5 1.4 ug/L 10/16/17 07:32 10/18/17 22:37 1Kepone<8.5
4.3 1.1 ug/L 10/16/17 07:32 10/18/17 22:37 1m-Dinitrobenzene <4.3
34 8.7 ug/L 10/16/17 07:32 10/18/17 22:37 1Methapyrilene<34
8.5 1.9 ug/L 10/16/17 07:32 10/18/17 22:37 13-Methylcholanthrene <8.5
34 5.1 ug/L 10/16/17 07:32 10/18/17 22:37 1Methyl methanesulfonate <34
1.7 0.056 ug/L 10/16/17 07:32 10/18/17 22:37 12-Methylnaphthalene <1.7
8.5 2.0 ug/L 10/16/17 07:32 10/18/17 22:37 1Methyl parathion <8.5
1.7 0.26 ug/L 10/16/17 07:32 10/18/17 22:37 12-Methylphenol <1.7
1.7 0.38 ug/L 10/16/17 07:32 10/18/17 22:37 13 & 4 Methylphenol <1.7
0.85 0.26 ug/L 10/16/17 07:32 10/18/17 22:37 1Naphthalene<0.85
34 33 ug/L 10/16/17 07:32 10/18/17 22:37 11,4-Naphthoquinone <34
17 5.1 ug/L 10/16/17 07:32 10/18/17 22:37 11-Naphthylamine <17
17 7.8 ug/L 10/16/17 07:32 10/18/17 22:37 12-Naphthylamine <17
4.3 1.1 ug/L 10/16/17 07:32 10/18/17 22:37 12-Nitroaniline <4.3
8.5 1.5 ug/L 10/16/17 07:32 10/18/17 22:37 13-Nitroaniline <8.5
8.5 1.4 ug/L 10/16/17 07:32 10/18/17 22:37 14-Nitroaniline <8.5
0.85 0.38 ug/L 10/16/17 07:32 10/18/17 22:37 1Nitrobenzene<0.85
8.5 2.6 ug/L 10/16/17 07:32 10/18/17 22:37 15-Nitro-o-toluidine <8.5
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-1Client Sample ID: MW-14 Infill
Matrix: WaterDate Collected: 10/11/17 16:10
Date Received: 10/12/17 10:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
2-Nitrophenol <8.5 8.5 2.1 ug/L 10/16/17 07:32 10/18/17 22:37 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
17 6.3 ug/L 10/16/17 07:32 10/18/17 22:37 14-Nitrophenol <17
17 7.3 ug/L 10/16/17 07:32 10/18/17 22:37 1N-Nitrosodiethylamine <17
8.5 4.1 ug/L 10/16/17 07:32 10/18/17 22:37 1N-Nitrosodimethylamine <8.5
8.5 3.6 ug/L 10/16/17 07:32 10/18/17 22:37 1N-Nitrosodi-n-butylamine <8.5
0.43 0.13 ug/L 10/16/17 07:32 10/18/17 22:37 1N-Nitrosodi-n-propylamine <0.43
1.7 0.32 ug/L 10/16/17 07:32 10/18/17 22:37 1N-Nitrosodiphenylamine <1.7
17 6.4 ug/L 10/16/17 07:32 10/18/17 22:37 1N-Nitrosomethylethylamine <17
8.5 3.0 ug/L 10/16/17 07:32 10/18/17 22:37 1N-Nitrosopiperidine <8.5
8.5 2.9 ug/L 10/16/17 07:32 10/18/17 22:37 1N-Nitrosopyrrolidine <8.5
17 4.7 ug/L 10/16/17 07:32 10/18/17 22:37 1o,o',o''-Triethylphosphorothioate <17
34 6.8 ug/L 10/16/17 07:32 10/18/17 22:37 1o-Toluidine <34
1.7 0.32 ug/L 10/16/17 07:32 10/18/17 22:37 12,2'-oxybis[1-chloropropane]<1.7
8.5 2.6 ug/L 10/16/17 07:32 10/18/17 22:37 1p-Dimethylamino azobenzene <8.5
8.5 2.4 ug/L 10/16/17 07:32 10/18/17 22:37 1Pentachlorobenzene<8.5
8.5 3.0 ug/L 10/16/17 07:32 10/18/17 22:37 1Pentachloronitrobenzene<8.5
8.5 1.9 ug/L 10/16/17 07:32 10/18/17 22:37 1Phenacetin<8.5
0.85 0.26 ug/L 10/16/17 07:32 10/18/17 22:37 1Phenanthrene<0.85
4.3 0.57 ug/L 10/16/17 07:32 10/18/17 22:37 1Phenol<4.3
8.5 1.8 ug/L 10/16/17 07:32 10/18/17 22:37 1Phorate<8.5
68 14 ug/L 10/16/17 07:32 10/18/17 22:37 1p-Phenylene diamine <68
8.5 1.8 ug/L 10/16/17 07:32 10/18/17 22:37 1Pronamide<8.5
0.85 0.36 ug/L 10/16/17 07:32 10/18/17 22:37 1Pyrene<0.85
8.5 3.4 ug/L 10/16/17 07:32 10/18/17 22:37 1Safrole<8.5
8.5 1.6 ug/L 10/16/17 07:32 10/18/17 22:37 1sym-Trinitrobenzene <8.5
8.5 8.5 ug/L 10/16/17 07:32 10/18/17 22:37 12,3,7,8-TCDD (Screen)<8.5
4.3 0.49 ug/L 10/16/17 07:32 10/18/17 22:37 11,2,4,5-Tetrachlorobenzene <4.3
4.3 0.64 ug/L 10/16/17 07:32 10/18/17 22:37 12,3,4,6-Tetrachlorophenol <4.3
8.5 2.2 ug/L 10/16/17 07:32 10/18/17 22:37 1Thionazin<8.5
8.5 2.2 ug/L 10/16/17 07:32 10/18/17 22:37 12,4,5-Trichlorophenol <8.5
4.3 0.61 ug/L 10/16/17 07:32 10/18/17 22:37 12,4,6-Trichlorophenol <4.3
2-Fluorobiphenyl 79 34-110 10/16/17 07:32 10/18/17 22:37 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol 57 10/16/17 07:32 10/18/17 22:37 127-110
Nitrobenzene-d5 77 10/16/17 07:32 10/18/17 22:37 136-120
Phenol-d5 35 10/16/17 07:32 10/18/17 22:37 120-100
Terphenyl-d14 96 10/16/17 07:32 10/18/17 22:37 140-145
2,4,6-Tribromophenol 114 10/16/17 07:32 10/18/17 22:37 140-145
Method: 8081B - Organochlorine Pesticides (GC)
RL MDL
alpha-BHC <0.037 0.037 0.0024 ug/L 10/13/17 09:13 10/16/17 16:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.037 0.0095 ug/L 10/13/17 09:13 10/16/17 16:01 1beta-BHC <0.037
0.037 0.0096 ug/L 10/13/17 09:13 10/16/17 16:01 1delta-BHC <0.037
0.037 0.0052 ug/L 10/13/17 09:13 10/16/17 16:01 1gamma-BHC (Lindane)<0.037
0.037 0.013 ug/L 10/13/17 09:13 10/16/17 16:01 1Heptachlor<0.037
0.037 0.0050 ug/L 10/13/17 09:13 10/16/17 16:01 1Aldrin<0.037
0.037 0.013 ug/L 10/13/17 09:13 10/16/17 16:01 1Heptachlor epoxide <0.037
0.037 0.0038 ug/L 10/13/17 09:13 10/16/17 16:01 1Endosulfan I <0.037
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-1Client Sample ID: MW-14 Infill
Matrix: WaterDate Collected: 10/11/17 16:10
Date Received: 10/12/17 10:00
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
RL MDL
Dieldrin <0.037 0.037 0.012 ug/L 10/13/17 09:13 10/16/17 16:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.037 0.0036 ug/L 10/13/17 09:13 10/16/17 16:01 14,4'-DDE <0.037
0.037 0.013 ug/L 10/13/17 09:13 10/16/17 16:01 1Endrin<0.037
0.037 0.0026 ug/L 10/13/17 09:13 10/16/17 16:01 1Endosulfan II <0.037
0.037 0.012 ug/L 10/13/17 09:13 10/16/17 16:01 14,4'-DDD <0.037
0.037 0.011 ug/L 10/13/17 09:13 10/16/17 16:01 1Endosulfan sulfate <0.037
0.037 0.0030 ug/L 10/13/17 09:13 10/16/17 16:01 14,4'-DDT <0.037
0.075 0.022 ug/L 10/13/17 09:13 10/16/17 16:01 1Methoxychlor<0.075
0.37 0.19 ug/L 10/13/17 09:13 10/16/17 16:01 1Toxaphene<0.37
0.037 0.0077 ug/L 10/13/17 09:13 10/16/17 16:01 1Endrin aldehyde <0.037
0.075 0.037 ug/L 10/13/17 09:13 10/16/17 16:01 1Chlordane (technical)<0.075
DCB Decachlorobiphenyl 58 30-130 10/13/17 09:13 10/16/17 16:01 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 67 10/13/17 09:13 10/16/17 16:01 130-120
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
RL MDL
PCB-1016 <0.37 0.37 0.063 ug/L 10/13/17 09:13 10/20/17 13:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.37 0.19 ug/L 10/13/17 09:13 10/20/17 13:09 1PCB-1221 <0.37
0.37 0.19 ug/L 10/13/17 09:13 10/20/17 13:09 1PCB-1232 <0.37
0.37 0.19 ug/L 10/13/17 09:13 10/20/17 13:09 1PCB-1242 <0.37
0.37 0.19 ug/L 10/13/17 09:13 10/20/17 13:09 1PCB-1248 <0.37
0.37 0.19 ug/L 10/13/17 09:13 10/20/17 13:09 1PCB-1254 <0.37
0.37 0.066 ug/L 10/13/17 09:13 10/20/17 13:09 1PCB-1260 <0.37
Tetrachloro-m-xylene 65 30-120 10/13/17 09:13 10/20/17 13:09 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
DCB Decachlorobiphenyl 69 10/13/17 09:13 10/20/17 13:09 130-140
Method: 8151A - Herbicides (GC)
RL MDL
2,4-D <0.96 0.96 0.45 ug/L 10/12/17 11:45 10/16/17 18:30 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.9 0.16 ug/L 10/12/17 11:45 10/16/17 18:30 1Dinoseb<1.9
0.48 0.087 ug/L 10/12/17 11:45 10/16/17 18:30 1Pentachlorophenol<0.48
0.96 0.28 ug/L 10/12/17 11:45 10/16/17 18:30 1Silvex (2,4,5-TP)<0.96
0.96 0.42 ug/L 10/12/17 11:45 10/16/17 18:30 12,4,5-T <0.96
DCAA 57 25-130 10/12/17 11:45 10/16/17 18:30 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 10/13/17 08:45 10/16/17 20:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 10/13/17 08:45 10/16/17 20:38 1Arsenic0.34 J
2.5 0.37 ug/L 10/13/17 08:45 10/16/17 20:38 1Barium29B
1.0 0.43 ug/L 10/13/17 08:45 10/16/17 20:38 1Beryllium<1.0
0.50 0.15 ug/L 10/13/17 08:45 10/16/17 20:38 1Cadmium<0.50
5.0 2.3 ug/L 10/13/17 08:45 10/16/17 20:38 1Chromium<5.0
1.0 0.27 ug/L 10/13/17 08:45 10/16/17 20:38 1Cobalt0.33 J
2.0 0.63 ug/L 10/13/17 08:45 10/17/17 15:13 1Copper0.66 J
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-1Client Sample ID: MW-14 Infill
Matrix: WaterDate Collected: 10/11/17 16:10
Date Received: 10/12/17 10:00
Method: 200.8 - Metals (ICP/MS) (Continued)
RL MDL
Iron 340 100 38 ug/L 10/13/17 08:45 10/16/17 20:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.50 0.16 ug/L 10/13/17 08:45 10/16/17 20:38 1Lead0.25 J B
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 20:38 1Manganese94
2.0 0.92 ug/L 10/13/17 08:45 10/16/17 20:38 1Nickel<2.0
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 20:38 1Selenium<2.5
0.50 0.078 ug/L 10/13/17 08:45 10/16/17 20:38 1Silver<0.50
2.0 0.65 ug/L 10/13/17 08:45 10/16/17 20:38 1Thallium<2.0
10 4.2 ug/L 10/13/17 08:45 10/16/17 20:38 1Tin<10
5.0 2.0 ug/L 10/13/17 08:45 10/17/17 15:13 1Vanadium<5.0
20 8.1 ug/L 10/13/17 08:45 10/16/17 20:38 1Zinc<20
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 10/18/17 15:35 10/19/17 10:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Cyanide, Total <0.010 0.010 0.0035 mg/L 10/19/17 18:27 10/20/17 16:46 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.20 0.17 mg/L 10/28/17 13:20 1Chloride6.7
0.40 0.19 mg/L 10/30/17 04:43 2Sulfate9.9
5.0 3.7 mg/L 10/19/17 15:35 1Alkalinity65
10 4.3 mg/L 10/13/17 05:56 1Total Dissolved Solids 140
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-2Client Sample ID: MW-8 Infill
Matrix: WaterDate Collected: 10/11/17 15:00
Date Received: 10/12/17 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 16:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/18/17 16:48 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/18/17 16:48 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/18/17 16:48 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/18/17 16:48 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/18/17 16:48 11,1-Dichloroethene <1.0
1.0 0.30 ug/L 10/18/17 16:48 11,1-Dichloropropene <1.0
1.0 0.41 ug/L 10/18/17 16:48 11,2,3-Trichloropropane <1.0
1.0 0.34 ug/L 10/18/17 16:48 11,2,4-Trichlorobenzene <1.0
5.0 2.0 ug/L 10/18/17 16:48 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/18/17 16:48 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/18/17 16:48 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/18/17 16:48 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/18/17 16:48 11,2-Dichloropropane <1.0
1.0 0.40 ug/L 10/18/17 16:48 11,3-Dichlorobenzene <1.0
1.0 0.36 ug/L 10/18/17 16:48 11,3-Dichloropropane <1.0
1.0 0.36 ug/L 10/18/17 16:48 11,4-Dichlorobenzene <1.0
1.0 0.44 ug/L 10/18/17 16:48 12,2-Dichloropropane <1.0
5.0 2.1 ug/L 10/18/17 16:48 12-Butanone (MEK)<5.0
1.0 0.23 ug/L 10/18/17 16:48 12-Chloro-1,3-butadiene <1.0
5.0 1.6 ug/L 10/18/17 16:48 12-Hexanone <5.0
2.5 0.86 ug/L 10/18/17 16:48 13-Chloropropene <2.5
5.0 2.2 ug/L 10/18/17 16:48 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/18/17 16:48 1Acetone<5.0
10 4.2 ug/L 10/18/17 16:48 1Acetonitrile<10
100 23 ug/L 10/18/17 16:48 1Acrolein<100
20 4.5 ug/L 10/18/17 16:48 1Acrylonitrile<20
0.50 0.15 ug/L 10/18/17 16:48 1Benzene<0.50
1.0 0.43 ug/L 10/18/17 16:48 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/18/17 16:48 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/18/17 16:48 1Bromoform<1.0
2.0 0.80 ug/L 10/18/17 16:48 1Bromomethane<2.0
2.0 0.45 ug/L 10/18/17 16:48 1Carbon disulfide <2.0
1.0 0.38 ug/L 10/18/17 16:48 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/18/17 16:48 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/18/17 16:48 1Chloroethane<1.0
2.0 0.37 ug/L 10/18/17 16:48 1Chloroform<2.0
1.0 0.32 ug/L 10/18/17 16:48 1Chloromethane<1.0
1.0 0.41 ug/L 10/18/17 16:48 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/18/17 16:48 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/18/17 16:48 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/18/17 16:48 1Dibromomethane<1.0
2.0 0.67 ug/L 10/18/17 16:48 1Dichlorodifluoromethane<2.0
2.5 0.53 ug/L 10/18/17 16:48 1Ethyl methacrylate <2.5
0.50 0.18 ug/L 10/18/17 16:48 1Ethylbenzene<0.50
1.0 0.45 ug/L 10/18/17 16:48 1Hexachlorobutadiene<1.0
2.5 0.66 ug/L 10/18/17 16:48 1Iodomethane<2.5
100 36 ug/L 10/18/17 16:48 1Isobutyl alcohol <100
10 2.5 ug/L 10/18/17 16:48 1Methacrylonitrile<10
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-2Client Sample ID: MW-8 Infill
Matrix: WaterDate Collected: 10/11/17 15:00
Date Received: 10/12/17 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Methyl methacrylate <2.5 2.5 0.55 ug/L 10/18/17 16:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.0 1.6 ug/L 10/18/17 16:48 1Methylene Chloride <5.0
10 4.8 ug/L 10/18/17 16:48 1Propionitrile<10
1.0 0.39 ug/L 10/18/17 16:48 1Styrene<1.0
1.0 0.37 ug/L 10/18/17 16:48 1Tetrachloroethene<1.0
10 1.9 ug/L 10/18/17 16:48 1Tetrahydrofuran<10
0.50 0.15 ug/L 10/18/17 16:48 1Toluene<0.50
1.0 0.35 ug/L 10/18/17 16:48 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/18/17 16:48 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/18/17 16:48 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/18/17 16:48 1Trichloroethene<0.50
1.0 0.43 ug/L 10/18/17 16:48 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/18/17 16:48 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/18/17 16:48 1Vinyl chloride <0.50
1.0 0.22 ug/L 10/18/17 16:48 1Xylenes, Total <1.0
1,2-Dichloroethane-d4 (Surr)106 75-126 10/18/17 16:48 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)98 10/18/17 16:48 172-124
Dibromofluoromethane 95 10/18/17 16:48 175-120
Toluene-d8 (Surr)96 10/18/17 16:48 175-120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.76 0.76 0.24 ug/L 10/16/17 07:32 10/18/17 23:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.76 0.20 ug/L 10/16/17 07:32 10/18/17 23:06 1Acenaphthylene<0.76
3.8 0.51 ug/L 10/16/17 07:32 10/18/17 23:06 1Acetophenone<3.8
7.6 1.6 ug/L 10/16/17 07:32 10/18/17 23:06 12-Acetylaminofluorene <7.6
7.6 2.9 ug/L 10/16/17 07:32 10/18/17 23:06 14-Aminobiphenyl <7.6
0.76 0.25 ug/L 10/16/17 07:32 10/18/17 23:06 1Anthracene<0.76
0.15 0.043 ug/L 10/16/17 07:32 10/18/17 23:06 1Benzo[a]anthracene <0.15
0.15 0.075 ug/L 10/16/17 07:32 10/18/17 23:06 1Benzo[a]pyrene <0.15
0.15 0.061 ug/L 10/16/17 07:32 10/18/17 23:06 1Benzo[b]fluoranthene <0.15
0.76 0.29 ug/L 10/16/17 07:32 10/18/17 23:06 1Benzo[g,h,i]perylene <0.76
0.15 0.049 ug/L 10/16/17 07:32 10/18/17 23:06 1Benzo[k]fluoranthene <0.15
15 4.6 ug/L 10/16/17 07:32 10/18/17 23:06 1Benzyl alcohol <15
1.5 0.22 ug/L 10/16/17 07:32 10/18/17 23:06 1Bis(2-chloroethoxy)methane <1.5
1.5 0.22 ug/L 10/16/17 07:32 10/18/17 23:06 1Bis(2-chloroethyl)ether <1.5
7.6 1.3 ug/L 10/16/17 07:32 10/18/17 23:06 1Bis(2-ethylhexyl) phthalate <7.6
3.8 0.41 ug/L 10/16/17 07:32 10/18/17 23:06 14-Bromophenyl phenyl ether <3.8
1.5 0.37 ug/L 10/16/17 07:32 10/18/17 23:06 1Butyl benzyl phthalate <1.5
7.6 1.5 ug/L 10/16/17 07:32 10/18/17 23:06 14-Chloroaniline <7.6
7.6 2.6 ug/L 10/16/17 07:32 10/18/17 23:06 1Chlorobenzilate<7.6
7.6 1.8 ug/L 10/16/17 07:32 10/18/17 23:06 14-Chloro-3-methylphenol <7.6
1.5 0.18 ug/L 10/16/17 07:32 10/18/17 23:06 12-Chloronaphthalene <1.5
3.8 0.43 ug/L 10/16/17 07:32 10/18/17 23:06 12-Chlorophenol <3.8
3.8 0.48 ug/L 10/16/17 07:32 10/18/17 23:06 14-Chlorophenyl phenyl ether <3.8
0.15 0.052 ug/L 10/16/17 07:32 10/18/17 23:06 1Chrysene<0.15
7.6 4.2 ug/L 10/16/17 07:32 10/18/17 23:06 1Diallate<7.6
0.23 0.039 ug/L 10/16/17 07:32 10/18/17 23:06 1Dibenz(a,h)anthracene <0.23
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-2Client Sample ID: MW-8 Infill
Matrix: WaterDate Collected: 10/11/17 15:00
Date Received: 10/12/17 10:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
Dibenzofuran <1.5 1.5 0.20 ug/L 10/16/17 07:32 10/18/17 23:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
3.8 1.3 ug/L 10/16/17 07:32 10/18/17 23:06 13,3'-Dichlorobenzidine <3.8
7.6 2.0 ug/L 10/16/17 07:32 10/18/17 23:06 12,4-Dichlorophenol <7.6
7.6 2.7 ug/L 10/16/17 07:32 10/18/17 23:06 12,6-Dichlorophenol <7.6
3.8 0.28 ug/L 10/16/17 07:32 10/18/17 23:06 1Diethyl phthalate <3.8
7.6 1.4 ug/L 10/16/17 07:32 10/18/17 23:06 1Dimethoate<7.6
30 2.3 ug/L 10/16/17 07:32 10/18/17 23:06 17,12-Dimethylbenz(a)anthracene <30
30 14 ug/L 10/16/17 07:32 10/18/17 23:06 13,3'-Dimethylbenzidine <30
7.6 1.4 ug/L 10/16/17 07:32 10/18/17 23:06 12,4-Dimethylphenol <7.6
3.8 0.24 ug/L 10/16/17 07:32 10/18/17 23:06 1Dimethyl phthalate <3.8
3.8 0.56 ug/L 10/16/17 07:32 10/18/17 23:06 1Di-n-butyl phthalate 0.61 J
15 4.5 ug/L 10/16/17 07:32 10/18/17 23:06 14,6-Dinitro-2-methylphenol <15
15 6.5 ug/L 10/16/17 07:32 10/18/17 23:06 12,4-Dinitrophenol <15
0.76 0.19 ug/L 10/16/17 07:32 10/18/17 23:06 12,4-Dinitrotoluene <0.76
0.76 0.056 ug/L 10/16/17 07:32 10/18/17 23:06 12,6-Dinitrotoluene <0.76
7.6 0.80 ug/L 10/16/17 07:32 10/18/17 23:06 1Di-n-octyl phthalate <7.6
7.6 1.9 ug/L 10/16/17 07:32 10/18/17 23:06 1Diphenylamine<7.6
7.6 1.5 ug/L 10/16/17 07:32 10/18/17 23:06 1Disulfoton<7.6
15 2.9 ug/L 10/16/17 07:32 10/18/17 23:06 1Ethyl methanesulfonate <15
7.6 1.6 ug/L 10/16/17 07:32 10/18/17 23:06 1Ethyl Parathion <7.6
30 23 ug/L 10/16/17 07:32 10/18/17 23:06 1Famphur<30
0.76 0.35 ug/L 10/16/17 07:32 10/18/17 23:06 1Fluoranthene<0.76
0.76 0.19 ug/L 10/16/17 07:32 10/18/17 23:06 1Fluorene<0.76
0.38 0.060 ug/L 10/16/17 07:32 10/18/17 23:06 1Hexachlorobenzene<0.38
15 4.9 ug/L 10/16/17 07:32 10/18/17 23:06 1Hexachlorocyclopentadiene<15
3.8 0.46 ug/L 10/16/17 07:32 10/18/17 23:06 1Hexachloroethane<3.8
15 3.6 ug/L 10/16/17 07:32 10/18/17 23:06 1Hexachloropropene<15
0.15 0.057 ug/L 10/16/17 07:32 10/18/17 23:06 1Indeno[1,2,3-cd]pyrene <0.15
15 5.3 ug/L 10/16/17 07:32 10/18/17 23:06 1Isodrin<15
1.5 0.29 ug/L 10/16/17 07:32 10/18/17 23:06 1Isophorone<1.5
7.6 3.0 ug/L 10/16/17 07:32 10/18/17 23:06 1Isosafrole<7.6
7.6 1.3 ug/L 10/16/17 07:32 10/18/17 23:06 1Kepone<7.6
3.8 1.0 ug/L 10/16/17 07:32 10/18/17 23:06 1m-Dinitrobenzene <3.8
30 7.7 ug/L 10/16/17 07:32 10/18/17 23:06 1Methapyrilene<30
7.6 1.7 ug/L 10/16/17 07:32 10/18/17 23:06 13-Methylcholanthrene <7.6
30 4.5 ug/L 10/16/17 07:32 10/18/17 23:06 1Methyl methanesulfonate <30
1.5 0.050 ug/L 10/16/17 07:32 10/18/17 23:06 12-Methylnaphthalene <1.5
7.6 1.8 ug/L 10/16/17 07:32 10/18/17 23:06 1Methyl parathion <7.6
1.5 0.23 ug/L 10/16/17 07:32 10/18/17 23:06 12-Methylphenol <1.5
1.5 0.34 ug/L 10/16/17 07:32 10/18/17 23:06 13 & 4 Methylphenol <1.5
0.76 0.24 ug/L 10/16/17 07:32 10/18/17 23:06 1Naphthalene<0.76
30 30 ug/L 10/16/17 07:32 10/18/17 23:06 11,4-Naphthoquinone <30
15 4.5 ug/L 10/16/17 07:32 10/18/17 23:06 11-Naphthylamine <15
15 7.0 ug/L 10/16/17 07:32 10/18/17 23:06 12-Naphthylamine <15
3.8 0.98 ug/L 10/16/17 07:32 10/18/17 23:06 12-Nitroaniline <3.8
7.6 1.4 ug/L 10/16/17 07:32 10/18/17 23:06 13-Nitroaniline <7.6
7.6 1.3 ug/L 10/16/17 07:32 10/18/17 23:06 14-Nitroaniline <7.6
0.76 0.34 ug/L 10/16/17 07:32 10/18/17 23:06 1Nitrobenzene<0.76
7.6 2.4 ug/L 10/16/17 07:32 10/18/17 23:06 15-Nitro-o-toluidine <7.6
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-2Client Sample ID: MW-8 Infill
Matrix: WaterDate Collected: 10/11/17 15:00
Date Received: 10/12/17 10:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
2-Nitrophenol <7.6 7.6 1.9 ug/L 10/16/17 07:32 10/18/17 23:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
15 5.7 ug/L 10/16/17 07:32 10/18/17 23:06 14-Nitrophenol <15
15 6.5 ug/L 10/16/17 07:32 10/18/17 23:06 1N-Nitrosodiethylamine <15
7.6 3.6 ug/L 10/16/17 07:32 10/18/17 23:06 1N-Nitrosodimethylamine <7.6
7.6 3.2 ug/L 10/16/17 07:32 10/18/17 23:06 1N-Nitrosodi-n-butylamine <7.6
0.38 0.12 ug/L 10/16/17 07:32 10/18/17 23:06 1N-Nitrosodi-n-propylamine <0.38
1.5 0.28 ug/L 10/16/17 07:32 10/18/17 23:06 1N-Nitrosodiphenylamine <1.5
15 5.7 ug/L 10/16/17 07:32 10/18/17 23:06 1N-Nitrosomethylethylamine <15
7.6 2.7 ug/L 10/16/17 07:32 10/18/17 23:06 1N-Nitrosopiperidine <7.6
7.6 2.6 ug/L 10/16/17 07:32 10/18/17 23:06 1N-Nitrosopyrrolidine <7.6
15 4.2 ug/L 10/16/17 07:32 10/18/17 23:06 1o,o',o''-Triethylphosphorothioate <15
30 6.0 ug/L 10/16/17 07:32 10/18/17 23:06 1o-Toluidine <30
1.5 0.29 ug/L 10/16/17 07:32 10/18/17 23:06 12,2'-oxybis[1-chloropropane]<1.5
7.6 2.3 ug/L 10/16/17 07:32 10/18/17 23:06 1p-Dimethylamino azobenzene <7.6
7.6 2.1 ug/L 10/16/17 07:32 10/18/17 23:06 1Pentachlorobenzene<7.6
7.6 2.7 ug/L 10/16/17 07:32 10/18/17 23:06 1Pentachloronitrobenzene<7.6
7.6 1.7 ug/L 10/16/17 07:32 10/18/17 23:06 1Phenacetin<7.6
0.76 0.23 ug/L 10/16/17 07:32 10/18/17 23:06 1Phenanthrene<0.76
3.8 0.51 ug/L 10/16/17 07:32 10/18/17 23:06 1Phenol<3.8
7.6 1.6 ug/L 10/16/17 07:32 10/18/17 23:06 1Phorate<7.6
61 12 ug/L 10/16/17 07:32 10/18/17 23:06 1p-Phenylene diamine <61
7.6 1.6 ug/L 10/16/17 07:32 10/18/17 23:06 1Pronamide<7.6
0.76 0.32 ug/L 10/16/17 07:32 10/18/17 23:06 1Pyrene<0.76
7.6 3.0 ug/L 10/16/17 07:32 10/18/17 23:06 1Safrole<7.6
7.6 1.4 ug/L 10/16/17 07:32 10/18/17 23:06 1sym-Trinitrobenzene <7.6
7.6 7.6 ug/L 10/16/17 07:32 10/18/17 23:06 12,3,7,8-TCDD (Screen)<7.6
3.8 0.44 ug/L 10/16/17 07:32 10/18/17 23:06 11,2,4,5-Tetrachlorobenzene <3.8
3.8 0.57 ug/L 10/16/17 07:32 10/18/17 23:06 12,3,4,6-Tetrachlorophenol <3.8
7.6 2.0 ug/L 10/16/17 07:32 10/18/17 23:06 1Thionazin<7.6
7.6 2.0 ug/L 10/16/17 07:32 10/18/17 23:06 12,4,5-Trichlorophenol <7.6
3.8 0.55 ug/L 10/16/17 07:32 10/18/17 23:06 12,4,6-Trichlorophenol <3.8
2-Fluorobiphenyl 60 34-110 10/16/17 07:32 10/18/17 23:06 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol 42 10/16/17 07:32 10/18/17 23:06 127-110
Nitrobenzene-d5 56 10/16/17 07:32 10/18/17 23:06 136-120
Phenol-d5 24 10/16/17 07:32 10/18/17 23:06 120-100
Terphenyl-d14 93 10/16/17 07:32 10/18/17 23:06 140-145
2,4,6-Tribromophenol 102 10/16/17 07:32 10/18/17 23:06 140-145
Method: 8081B - Organochlorine Pesticides (GC)
RL MDL
alpha-BHC <0.040 0.040 0.0026 ug/L 10/13/17 09:13 10/16/17 16:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.040 0.010 ug/L 10/13/17 09:13 10/16/17 16:20 1beta-BHC <0.040
0.040 0.010 ug/L 10/13/17 09:13 10/16/17 16:20 1delta-BHC <0.040
0.040 0.0057 ug/L 10/13/17 09:13 10/16/17 16:20 1gamma-BHC (Lindane)<0.040
0.040 0.014 ug/L 10/13/17 09:13 10/16/17 16:20 1Heptachlor<0.040
0.040 0.0054 ug/L 10/13/17 09:13 10/16/17 16:20 1Aldrin<0.040
0.040 0.014 ug/L 10/13/17 09:13 10/16/17 16:20 1Heptachlor epoxide <0.040
0.040 0.0041 ug/L 10/13/17 09:13 10/16/17 16:20 1Endosulfan I <0.040
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-2Client Sample ID: MW-8 Infill
Matrix: WaterDate Collected: 10/11/17 15:00
Date Received: 10/12/17 10:00
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
RL MDL
Dieldrin <0.040 0.040 0.013 ug/L 10/13/17 09:13 10/16/17 16:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.040 0.0038 ug/L 10/13/17 09:13 10/16/17 16:20 14,4'-DDE <0.040
0.040 0.014 ug/L 10/13/17 09:13 10/16/17 16:20 1Endrin<0.040
0.040 0.0028 ug/L 10/13/17 09:13 10/16/17 16:20 1Endosulfan II <0.040
0.040 0.013 ug/L 10/13/17 09:13 10/16/17 16:20 14,4'-DDD <0.040
0.040 0.012 ug/L 10/13/17 09:13 10/16/17 16:20 1Endosulfan sulfate <0.040
0.040 0.0032 ug/L 10/13/17 09:13 10/16/17 16:20 14,4'-DDT <0.040
0.081 0.023 ug/L 10/13/17 09:13 10/16/17 16:20 1Methoxychlor<0.081
0.40 0.20 ug/L 10/13/17 09:13 10/16/17 16:20 1Toxaphene<0.40
0.040 0.0083 ug/L 10/13/17 09:13 10/16/17 16:20 1Endrin aldehyde <0.040
0.081 0.040 ug/L 10/13/17 09:13 10/16/17 16:20 1Chlordane (technical)<0.081
DCB Decachlorobiphenyl 76 30-130 10/13/17 09:13 10/16/17 16:20 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 76 10/13/17 09:13 10/16/17 16:20 130-120
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
RL MDL
PCB-1016 <0.40 0.40 0.068 ug/L 10/13/17 09:13 10/20/17 13:25 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.40 0.20 ug/L 10/13/17 09:13 10/20/17 13:25 1PCB-1221 <0.40
0.40 0.20 ug/L 10/13/17 09:13 10/20/17 13:25 1PCB-1232 <0.40
0.40 0.20 ug/L 10/13/17 09:13 10/20/17 13:25 1PCB-1242 <0.40
0.40 0.20 ug/L 10/13/17 09:13 10/20/17 13:25 1PCB-1248 <0.40
0.40 0.20 ug/L 10/13/17 09:13 10/20/17 13:25 1PCB-1254 <0.40
0.40 0.071 ug/L 10/13/17 09:13 10/20/17 13:25 1PCB-1260 0.37 J
Tetrachloro-m-xylene 82 30-120 10/13/17 09:13 10/20/17 13:25 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
DCB Decachlorobiphenyl 98 10/13/17 09:13 10/20/17 13:25 130-140
Method: 8151A - Herbicides (GC)
RL MDL
2,4-D <0.97 0.97 0.45 ug/L 10/12/17 11:45 10/16/17 18:55 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.9 0.16 ug/L 10/12/17 11:45 10/16/17 18:55 1Dinoseb<1.9
0.48 0.087 ug/L 10/12/17 11:45 10/16/17 18:55 1Pentachlorophenol<0.48
0.97 0.28 ug/L 10/12/17 11:45 10/16/17 18:55 1Silvex (2,4,5-TP)<0.97
0.97 0.42 ug/L 10/12/17 11:45 10/16/17 18:55 12,4,5-T <0.97
DCAA 61 25-130 10/12/17 11:45 10/16/17 18:55 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 10/13/17 08:45 10/16/17 20:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 10/13/17 08:45 10/16/17 20:42 1Arsenic<1.0
2.5 0.37 ug/L 10/13/17 08:45 10/16/17 20:42 1Barium41B
1.0 0.43 ug/L 10/13/17 08:45 10/16/17 20:42 1Beryllium<1.0
0.50 0.15 ug/L 10/13/17 08:45 10/16/17 20:42 1Cadmium<0.50
5.0 2.3 ug/L 10/13/17 08:45 10/16/17 20:42 1Chromium<5.0
1.0 0.27 ug/L 10/13/17 08:45 10/16/17 20:42 1Cobalt1.4
2.0 0.63 ug/L 10/13/17 08:45 10/17/17 15:18 1Copper1.1 J
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-2Client Sample ID: MW-8 Infill
Matrix: WaterDate Collected: 10/11/17 15:00
Date Received: 10/12/17 10:00
Method: 200.8 - Metals (ICP/MS) (Continued)
RL MDL
Iron 440 100 38 ug/L 10/13/17 08:45 10/16/17 20:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.50 0.16 ug/L 10/13/17 08:45 10/16/17 20:42 1Lead0.16 J B
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 20:42 1Manganese110
2.0 0.92 ug/L 10/13/17 08:45 10/16/17 20:42 1Nickel1.4 J
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 20:42 1Selenium<2.5
0.50 0.078 ug/L 10/13/17 08:45 10/16/17 20:42 1Silver<0.50
2.0 0.65 ug/L 10/13/17 08:45 10/16/17 20:42 1Thallium<2.0
10 4.2 ug/L 10/13/17 08:45 10/16/17 20:42 1Tin<10
5.0 2.0 ug/L 10/13/17 08:45 10/17/17 15:18 1Vanadium5.1
20 8.1 ug/L 10/13/17 08:45 10/16/17 20:42 1Zinc<20
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 10/18/17 15:35 10/19/17 10:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Cyanide, Total <0.010 0.010 0.0035 mg/L 10/24/17 12:00 10/24/17 15:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.0 4.3 mg/L 10/28/17 13:45 25Chloride92
0.20 0.095 mg/L 10/28/17 13:32 1Sulfate8.4
5.0 3.7 mg/L 10/19/17 15:50 1Alkalinity150
10 4.3 mg/L 10/13/17 05:58 1Total Dissolved Solids 390
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-3Client Sample ID: Duplicate 2
Matrix: WaterDate Collected: 10/11/17 13:15
Date Received: 10/12/17 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 17:14 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/18/17 17:14 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/18/17 17:14 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/18/17 17:14 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/18/17 17:14 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/18/17 17:14 11,1-Dichloroethene <1.0
1.0 0.30 ug/L 10/18/17 17:14 11,1-Dichloropropene <1.0
1.0 0.41 ug/L 10/18/17 17:14 11,2,3-Trichloropropane <1.0
1.0 0.34 ug/L 10/18/17 17:14 11,2,4-Trichlorobenzene <1.0
5.0 2.0 ug/L 10/18/17 17:14 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/18/17 17:14 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/18/17 17:14 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/18/17 17:14 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/18/17 17:14 11,2-Dichloropropane <1.0
1.0 0.40 ug/L 10/18/17 17:14 11,3-Dichlorobenzene <1.0
1.0 0.36 ug/L 10/18/17 17:14 11,3-Dichloropropane <1.0
1.0 0.36 ug/L 10/18/17 17:14 11,4-Dichlorobenzene <1.0
1.0 0.44 ug/L 10/18/17 17:14 12,2-Dichloropropane <1.0
5.0 2.1 ug/L 10/18/17 17:14 12-Butanone (MEK)<5.0
1.0 0.23 ug/L 10/18/17 17:14 12-Chloro-1,3-butadiene <1.0
5.0 1.6 ug/L 10/18/17 17:14 12-Hexanone <5.0
2.5 0.86 ug/L 10/18/17 17:14 13-Chloropropene <2.5
5.0 2.2 ug/L 10/18/17 17:14 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/18/17 17:14 1Acetone<5.0
10 4.2 ug/L 10/18/17 17:14 1Acetonitrile<10
100 23 ug/L 10/18/17 17:14 1Acrolein<100
20 4.5 ug/L 10/18/17 17:14 1Acrylonitrile<20
0.50 0.15 ug/L 10/18/17 17:14 1Benzene0.61
1.0 0.43 ug/L 10/18/17 17:14 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/18/17 17:14 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/18/17 17:14 1Bromoform<1.0
2.0 0.80 ug/L 10/18/17 17:14 1Bromomethane<2.0
2.0 0.45 ug/L 10/18/17 17:14 1Carbon disulfide <2.0
1.0 0.38 ug/L 10/18/17 17:14 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/18/17 17:14 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/18/17 17:14 1Chloroethane<1.0
2.0 0.37 ug/L 10/18/17 17:14 1Chloroform<2.0
1.0 0.32 ug/L 10/18/17 17:14 1Chloromethane<1.0
1.0 0.41 ug/L 10/18/17 17:14 1cis-1,2-Dichloroethene 1.7
1.0 0.42 ug/L 10/18/17 17:14 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/18/17 17:14 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/18/17 17:14 1Dibromomethane<1.0
2.0 0.67 ug/L 10/18/17 17:14 1Dichlorodifluoromethane<2.0
2.5 0.53 ug/L 10/18/17 17:14 1Ethyl methacrylate <2.5
0.50 0.18 ug/L 10/18/17 17:14 1Ethylbenzene<0.50
1.0 0.45 ug/L 10/18/17 17:14 1Hexachlorobutadiene<1.0
2.5 0.66 ug/L 10/18/17 17:14 1Iodomethane<2.5
100 36 ug/L 10/18/17 17:14 1Isobutyl alcohol <100
10 2.5 ug/L 10/18/17 17:14 1Methacrylonitrile<10
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-3Client Sample ID: Duplicate 2
Matrix: WaterDate Collected: 10/11/17 13:15
Date Received: 10/12/17 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Methyl methacrylate <2.5 2.5 0.55 ug/L 10/18/17 17:14 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.0 1.6 ug/L 10/18/17 17:14 1Methylene Chloride 5.4 cn
10 4.8 ug/L 10/18/17 17:14 1Propionitrile<10
1.0 0.39 ug/L 10/18/17 17:14 1Styrene<1.0
1.0 0.37 ug/L 10/18/17 17:14 1Tetrachloroethene<1.0
10 1.9 ug/L 10/18/17 17:14 1Tetrahydrofuran<10
0.50 0.15 ug/L 10/18/17 17:14 1Toluene<0.50
1.0 0.35 ug/L 10/18/17 17:14 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/18/17 17:14 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/18/17 17:14 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/18/17 17:14 1Trichloroethene<0.50
1.0 0.43 ug/L 10/18/17 17:14 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/18/17 17:14 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/18/17 17:14 1Vinyl chloride 2.3
1.0 0.22 ug/L 10/18/17 17:14 1Xylenes, Total <1.0
1,2-Dichloroethane-d4 (Surr)107 75-126 10/18/17 17:14 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)98 10/18/17 17:14 172-124
Dibromofluoromethane 100 10/18/17 17:14 175-120
Toluene-d8 (Surr)94 10/18/17 17:14 175-120
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-4Client Sample ID: MW-12 Infill
Matrix: WaterDate Collected: 10/11/17 13:15
Date Received: 10/12/17 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 17:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/18/17 17:40 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/18/17 17:40 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/18/17 17:40 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/18/17 17:40 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/18/17 17:40 11,1-Dichloroethene <1.0
1.0 0.30 ug/L 10/18/17 17:40 11,1-Dichloropropene <1.0
1.0 0.41 ug/L 10/18/17 17:40 11,2,3-Trichloropropane <1.0
1.0 0.34 ug/L 10/18/17 17:40 11,2,4-Trichlorobenzene <1.0
5.0 2.0 ug/L 10/18/17 17:40 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/18/17 17:40 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/18/17 17:40 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/18/17 17:40 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/18/17 17:40 11,2-Dichloropropane <1.0
1.0 0.40 ug/L 10/18/17 17:40 11,3-Dichlorobenzene <1.0
1.0 0.36 ug/L 10/18/17 17:40 11,3-Dichloropropane <1.0
1.0 0.36 ug/L 10/18/17 17:40 11,4-Dichlorobenzene <1.0
1.0 0.44 ug/L 10/18/17 17:40 12,2-Dichloropropane <1.0
5.0 2.1 ug/L 10/18/17 17:40 12-Butanone (MEK)<5.0
1.0 0.23 ug/L 10/18/17 17:40 12-Chloro-1,3-butadiene <1.0
5.0 1.6 ug/L 10/18/17 17:40 12-Hexanone <5.0
2.5 0.86 ug/L 10/18/17 17:40 13-Chloropropene <2.5
5.0 2.2 ug/L 10/18/17 17:40 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/18/17 17:40 1Acetone<5.0
10 4.2 ug/L 10/18/17 17:40 1Acetonitrile<10
100 23 ug/L 10/18/17 17:40 1Acrolein<100
20 4.5 ug/L 10/18/17 17:40 1Acrylonitrile<20
0.50 0.15 ug/L 10/18/17 17:40 1Benzene0.66
1.0 0.43 ug/L 10/18/17 17:40 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/18/17 17:40 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/18/17 17:40 1Bromoform<1.0
2.0 0.80 ug/L 10/18/17 17:40 1Bromomethane<2.0
2.0 0.45 ug/L 10/18/17 17:40 1Carbon disulfide <2.0
1.0 0.38 ug/L 10/18/17 17:40 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/18/17 17:40 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/18/17 17:40 1Chloroethane<1.0
2.0 0.37 ug/L 10/18/17 17:40 1Chloroform<2.0
1.0 0.32 ug/L 10/18/17 17:40 1Chloromethane<1.0
1.0 0.41 ug/L 10/18/17 17:40 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/18/17 17:40 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/18/17 17:40 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/18/17 17:40 1Dibromomethane<1.0
2.0 0.67 ug/L 10/18/17 17:40 1Dichlorodifluoromethane<2.0
2.5 0.53 ug/L 10/18/17 17:40 1Ethyl methacrylate <2.5
0.50 0.18 ug/L 10/18/17 17:40 1Ethylbenzene<0.50
1.0 0.45 ug/L 10/18/17 17:40 1Hexachlorobutadiene<1.0
2.5 0.66 ug/L 10/18/17 17:40 1Iodomethane<2.5
100 36 ug/L 10/18/17 17:40 1Isobutyl alcohol <100
10 2.5 ug/L 10/18/17 17:40 1Methacrylonitrile<10
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-4Client Sample ID: MW-12 Infill
Matrix: WaterDate Collected: 10/11/17 13:15
Date Received: 10/12/17 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Methyl methacrylate <2.5 2.5 0.55 ug/L 10/18/17 17:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.0 1.6 ug/L 10/18/17 17:40 1Methylene Chloride 5.8 cn
10 4.8 ug/L 10/18/17 17:40 1Propionitrile<10
1.0 0.39 ug/L 10/18/17 17:40 1Styrene<1.0
1.0 0.37 ug/L 10/18/17 17:40 1Tetrachloroethene<1.0
10 1.9 ug/L 10/18/17 17:40 1Tetrahydrofuran<10
0.50 0.15 ug/L 10/18/17 17:40 1Toluene<0.50
1.0 0.35 ug/L 10/18/17 17:40 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/18/17 17:40 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/18/17 17:40 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/18/17 17:40 1Trichloroethene<0.50
1.0 0.43 ug/L 10/18/17 17:40 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/18/17 17:40 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/18/17 17:40 1Vinyl chloride 2.7
1.0 0.22 ug/L 10/18/17 17:40 1Xylenes, Total <1.0
1,2-Dichloroethane-d4 (Surr)106 75-126 10/18/17 17:40 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)97 10/18/17 17:40 172-124
Dibromofluoromethane 99 10/18/17 17:40 175-120
Toluene-d8 (Surr)93 10/18/17 17:40 175-120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.75 0.75 0.23 ug/L 10/16/17 07:32 10/18/17 23:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.75 0.20 ug/L 10/16/17 07:32 10/18/17 23:35 1Acenaphthylene<0.75
3.8 0.50 ug/L 10/16/17 07:32 10/18/17 23:35 1Acetophenone<3.8
7.5 1.6 ug/L 10/16/17 07:32 10/18/17 23:35 12-Acetylaminofluorene <7.5
7.5 2.8 ug/L 10/16/17 07:32 10/18/17 23:35 14-Aminobiphenyl <7.5
0.75 0.25 ug/L 10/16/17 07:32 10/18/17 23:35 1Anthracene<0.75
0.15 0.043 ug/L 10/16/17 07:32 10/18/17 23:35 1Benzo[a]anthracene <0.15
0.15 0.075 ug/L 10/16/17 07:32 10/18/17 23:35 1Benzo[a]pyrene <0.15
0.15 0.061 ug/L 10/16/17 07:32 10/18/17 23:35 1Benzo[b]fluoranthene <0.15
0.75 0.28 ug/L 10/16/17 07:32 10/18/17 23:35 1Benzo[g,h,i]perylene <0.75
0.15 0.048 ug/L 10/16/17 07:32 10/18/17 23:35 1Benzo[k]fluoranthene <0.15
15 4.6 ug/L 10/16/17 07:32 10/18/17 23:35 1Benzyl alcohol <15
1.5 0.21 ug/L 10/16/17 07:32 10/18/17 23:35 1Bis(2-chloroethoxy)methane <1.5
1.5 0.22 ug/L 10/16/17 07:32 10/18/17 23:35 1Bis(2-chloroethyl)ether <1.5
7.5 1.3 ug/L 10/16/17 07:32 10/18/17 23:35 1Bis(2-ethylhexyl) phthalate <7.5
3.8 0.41 ug/L 10/16/17 07:32 10/18/17 23:35 14-Bromophenyl phenyl ether <3.8
1.5 0.36 ug/L 10/16/17 07:32 10/18/17 23:35 1Butyl benzyl phthalate <1.5
7.5 1.5 ug/L 10/16/17 07:32 10/18/17 23:35 14-Chloroaniline <7.5
7.5 2.6 ug/L 10/16/17 07:32 10/18/17 23:35 1Chlorobenzilate<7.5
7.5 1.7 ug/L 10/16/17 07:32 10/18/17 23:35 14-Chloro-3-methylphenol <7.5
1.5 0.18 ug/L 10/16/17 07:32 10/18/17 23:35 12-Chloronaphthalene <1.5
3.8 0.42 ug/L 10/16/17 07:32 10/18/17 23:35 12-Chlorophenol <3.8
3.8 0.48 ug/L 10/16/17 07:32 10/18/17 23:35 14-Chlorophenyl phenyl ether <3.8
0.15 0.051 ug/L 10/16/17 07:32 10/18/17 23:35 1Chrysene<0.15
7.5 4.2 ug/L 10/16/17 07:32 10/18/17 23:35 1Diallate<7.5
0.23 0.038 ug/L 10/16/17 07:32 10/18/17 23:35 1Dibenz(a,h)anthracene <0.23
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-4Client Sample ID: MW-12 Infill
Matrix: WaterDate Collected: 10/11/17 13:15
Date Received: 10/12/17 10:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
Dibenzofuran <1.5 1.5 0.20 ug/L 10/16/17 07:32 10/18/17 23:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
3.8 1.3 ug/L 10/16/17 07:32 10/18/17 23:35 13,3'-Dichlorobenzidine <3.8
7.5 2.0 ug/L 10/16/17 07:32 10/18/17 23:35 12,4-Dichlorophenol <7.5
7.5 2.6 ug/L 10/16/17 07:32 10/18/17 23:35 12,6-Dichlorophenol <7.5
3.8 0.27 ug/L 10/16/17 07:32 10/18/17 23:35 1Diethyl phthalate <3.8
7.5 1.4 ug/L 10/16/17 07:32 10/18/17 23:35 1Dimethoate<7.5
30 2.3 ug/L 10/16/17 07:32 10/18/17 23:35 17,12-Dimethylbenz(a)anthracene <30
30 13 ug/L 10/16/17 07:32 10/18/17 23:35 13,3'-Dimethylbenzidine <30
7.5 1.4 ug/L 10/16/17 07:32 10/18/17 23:35 12,4-Dimethylphenol <7.5
3.8 0.24 ug/L 10/16/17 07:32 10/18/17 23:35 1Dimethyl phthalate <3.8
3.8 0.55 ug/L 10/16/17 07:32 10/18/17 23:35 1Di-n-butyl phthalate <3.8
15 4.4 ug/L 10/16/17 07:32 10/18/17 23:35 14,6-Dinitro-2-methylphenol <15
15 6.5 ug/L 10/16/17 07:32 10/18/17 23:35 12,4-Dinitrophenol <15
0.75 0.18 ug/L 10/16/17 07:32 10/18/17 23:35 12,4-Dinitrotoluene <0.75
0.75 0.056 ug/L 10/16/17 07:32 10/18/17 23:35 12,6-Dinitrotoluene <0.75
7.5 0.79 ug/L 10/16/17 07:32 10/18/17 23:35 1Di-n-octyl phthalate <7.5
7.5 1.9 ug/L 10/16/17 07:32 10/18/17 23:35 1Diphenylamine<7.5
7.5 1.4 ug/L 10/16/17 07:32 10/18/17 23:35 1Disulfoton<7.5
15 2.9 ug/L 10/16/17 07:32 10/18/17 23:35 1Ethyl methanesulfonate <15
7.5 1.6 ug/L 10/16/17 07:32 10/18/17 23:35 1Ethyl Parathion <7.5
30 23 ug/L 10/16/17 07:32 10/18/17 23:35 1Famphur<30
0.75 0.34 ug/L 10/16/17 07:32 10/18/17 23:35 1Fluoranthene<0.75
0.75 0.18 ug/L 10/16/17 07:32 10/18/17 23:35 1Fluorene<0.75
0.38 0.060 ug/L 10/16/17 07:32 10/18/17 23:35 1Hexachlorobenzene<0.38
15 4.8 ug/L 10/16/17 07:32 10/18/17 23:35 1Hexachlorocyclopentadiene<15
3.8 0.45 ug/L 10/16/17 07:32 10/18/17 23:35 1Hexachloroethane<3.8
15 3.5 ug/L 10/16/17 07:32 10/18/17 23:35 1Hexachloropropene<15
0.15 0.056 ug/L 10/16/17 07:32 10/18/17 23:35 1Indeno[1,2,3-cd]pyrene <0.15
15 5.2 ug/L 10/16/17 07:32 10/18/17 23:35 1Isodrin<15
1.5 0.28 ug/L 10/16/17 07:32 10/18/17 23:35 1Isophorone<1.5
7.5 2.9 ug/L 10/16/17 07:32 10/18/17 23:35 1Isosafrole<7.5
7.5 1.2 ug/L 10/16/17 07:32 10/18/17 23:35 1Kepone<7.5
3.8 1.0 ug/L 10/16/17 07:32 10/18/17 23:35 1m-Dinitrobenzene <3.8
30 7.6 ug/L 10/16/17 07:32 10/18/17 23:35 1Methapyrilene<30
7.5 1.7 ug/L 10/16/17 07:32 10/18/17 23:35 13-Methylcholanthrene <7.5
30 4.5 ug/L 10/16/17 07:32 10/18/17 23:35 1Methyl methanesulfonate <30
1.5 0.049 ug/L 10/16/17 07:32 10/18/17 23:35 12-Methylnaphthalene <1.5
7.5 1.8 ug/L 10/16/17 07:32 10/18/17 23:35 1Methyl parathion <7.5
1.5 0.23 ug/L 10/16/17 07:32 10/18/17 23:35 12-Methylphenol <1.5
1.5 0.34 ug/L 10/16/17 07:32 10/18/17 23:35 13 & 4 Methylphenol <1.5
0.75 0.23 ug/L 10/16/17 07:32 10/18/17 23:35 1Naphthalene<0.75
30 29 ug/L 10/16/17 07:32 10/18/17 23:35 11,4-Naphthoquinone <30
15 4.5 ug/L 10/16/17 07:32 10/18/17 23:35 11-Naphthylamine <15
15 6.9 ug/L 10/16/17 07:32 10/18/17 23:35 12-Naphthylamine <15
3.8 0.97 ug/L 10/16/17 07:32 10/18/17 23:35 12-Nitroaniline <3.8
7.5 1.3 ug/L 10/16/17 07:32 10/18/17 23:35 13-Nitroaniline <7.5
7.5 1.3 ug/L 10/16/17 07:32 10/18/17 23:35 14-Nitroaniline <7.5
0.75 0.34 ug/L 10/16/17 07:32 10/18/17 23:35 1Nitrobenzene<0.75
7.5 2.3 ug/L 10/16/17 07:32 10/18/17 23:35 15-Nitro-o-toluidine <7.5
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-4Client Sample ID: MW-12 Infill
Matrix: WaterDate Collected: 10/11/17 13:15
Date Received: 10/12/17 10:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
2-Nitrophenol <7.5 7.5 1.9 ug/L 10/16/17 07:32 10/18/17 23:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
15 5.6 ug/L 10/16/17 07:32 10/18/17 23:35 14-Nitrophenol <15
15 6.5 ug/L 10/16/17 07:32 10/18/17 23:35 1N-Nitrosodiethylamine <15
7.5 3.6 ug/L 10/16/17 07:32 10/18/17 23:35 1N-Nitrosodimethylamine <7.5
7.5 3.2 ug/L 10/16/17 07:32 10/18/17 23:35 1N-Nitrosodi-n-butylamine <7.5
0.38 0.12 ug/L 10/16/17 07:32 10/18/17 23:35 1N-Nitrosodi-n-propylamine <0.38
1.5 0.28 ug/L 10/16/17 07:32 10/18/17 23:35 1N-Nitrosodiphenylamine <1.5
15 5.6 ug/L 10/16/17 07:32 10/18/17 23:35 1N-Nitrosomethylethylamine <15
7.5 2.6 ug/L 10/16/17 07:32 10/18/17 23:35 1N-Nitrosopiperidine <7.5
7.5 2.5 ug/L 10/16/17 07:32 10/18/17 23:35 1N-Nitrosopyrrolidine <7.5
15 4.2 ug/L 10/16/17 07:32 10/18/17 23:35 1o,o',o''-Triethylphosphorothioate <15
30 6.0 ug/L 10/16/17 07:32 10/18/17 23:35 1o-Toluidine <30
1.5 0.29 ug/L 10/16/17 07:32 10/18/17 23:35 12,2'-oxybis[1-chloropropane]<1.5
7.5 2.3 ug/L 10/16/17 07:32 10/18/17 23:35 1p-Dimethylamino azobenzene <7.5
7.5 2.1 ug/L 10/16/17 07:32 10/18/17 23:35 1Pentachlorobenzene<7.5
7.5 2.7 ug/L 10/16/17 07:32 10/18/17 23:35 1Pentachloronitrobenzene<7.5
7.5 1.7 ug/L 10/16/17 07:32 10/18/17 23:35 1Phenacetin<7.5
0.75 0.23 ug/L 10/16/17 07:32 10/18/17 23:35 1Phenanthrene<0.75
3.8 0.51 ug/L 10/16/17 07:32 10/18/17 23:35 1Phenol<3.8
7.5 1.6 ug/L 10/16/17 07:32 10/18/17 23:35 1Phorate<7.5
60 12 ug/L 10/16/17 07:32 10/18/17 23:35 1p-Phenylene diamine <60
7.5 1.6 ug/L 10/16/17 07:32 10/18/17 23:35 1Pronamide<7.5
0.75 0.32 ug/L 10/16/17 07:32 10/18/17 23:35 1Pyrene<0.75
7.5 3.0 ug/L 10/16/17 07:32 10/18/17 23:35 1Safrole<7.5
7.5 1.4 ug/L 10/16/17 07:32 10/18/17 23:35 1sym-Trinitrobenzene <7.5
7.5 7.5 ug/L 10/16/17 07:32 10/18/17 23:35 12,3,7,8-TCDD (Screen)<7.5
3.8 0.43 ug/L 10/16/17 07:32 10/18/17 23:35 11,2,4,5-Tetrachlorobenzene <3.8
3.8 0.56 ug/L 10/16/17 07:32 10/18/17 23:35 12,3,4,6-Tetrachlorophenol <3.8
7.5 2.0 ug/L 10/16/17 07:32 10/18/17 23:35 1Thionazin<7.5
7.5 1.9 ug/L 10/16/17 07:32 10/18/17 23:35 12,4,5-Trichlorophenol <7.5
3.8 0.54 ug/L 10/16/17 07:32 10/18/17 23:35 12,4,6-Trichlorophenol <3.8
2-Fluorobiphenyl 72 34-110 10/16/17 07:32 10/18/17 23:35 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol 48 10/16/17 07:32 10/18/17 23:35 127-110
Nitrobenzene-d5 68 10/16/17 07:32 10/18/17 23:35 136-120
Phenol-d5 33 10/16/17 07:32 10/18/17 23:35 120-100
Terphenyl-d14 93 10/16/17 07:32 10/18/17 23:35 140-145
2,4,6-Tribromophenol 114 10/16/17 07:32 10/18/17 23:35 140-145
Method: 8081B - Organochlorine Pesticides (GC)
RL MDL
alpha-BHC <0.037 0.037 0.0024 ug/L 10/13/17 09:13 10/16/17 16:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.037 0.0094 ug/L 10/13/17 09:13 10/16/17 16:39 1beta-BHC <0.037
0.037 0.0095 ug/L 10/13/17 09:13 10/16/17 16:39 1delta-BHC <0.037
0.037 0.0052 ug/L 10/13/17 09:13 10/16/17 16:39 1gamma-BHC (Lindane)<0.037
0.037 0.012 ug/L 10/13/17 09:13 10/16/17 16:39 1Heptachlor<0.037
0.037 0.0049 ug/L 10/13/17 09:13 10/16/17 16:39 1Aldrin<0.037
0.037 0.013 ug/L 10/13/17 09:13 10/16/17 16:39 1Heptachlor epoxide <0.037
0.037 0.0038 ug/L 10/13/17 09:13 10/16/17 16:39 1Endosulfan I <0.037
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-4Client Sample ID: MW-12 Infill
Matrix: WaterDate Collected: 10/11/17 13:15
Date Received: 10/12/17 10:00
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
RL MDL
Dieldrin <0.037 0.037 0.012 ug/L 10/13/17 09:13 10/16/17 16:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.037 0.0035 ug/L 10/13/17 09:13 10/16/17 16:39 14,4'-DDE <0.037
0.037 0.013 ug/L 10/13/17 09:13 10/16/17 16:39 1Endrin<0.037
0.037 0.0026 ug/L 10/13/17 09:13 10/16/17 16:39 1Endosulfan II <0.037
0.037 0.012 ug/L 10/13/17 09:13 10/16/17 16:39 14,4'-DDD <0.037
0.037 0.011 ug/L 10/13/17 09:13 10/16/17 16:39 1Endosulfan sulfate <0.037
0.037 0.0030 ug/L 10/13/17 09:13 10/16/17 16:39 14,4'-DDT <0.037
0.074 0.021 ug/L 10/13/17 09:13 10/16/17 16:39 1Methoxychlor<0.074
0.37 0.19 ug/L 10/13/17 09:13 10/16/17 16:39 1Toxaphene<0.37
0.037 0.0076 ug/L 10/13/17 09:13 10/16/17 16:39 1Endrin aldehyde <0.037
0.074 0.037 ug/L 10/13/17 09:13 10/16/17 16:39 1Chlordane (technical)<0.074
DCB Decachlorobiphenyl 93 30-130 10/13/17 09:13 10/16/17 16:39 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 119 10/13/17 09:13 10/16/17 16:39 130-120
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
RL MDL
PCB-1016 <0.37 0.37 0.062 ug/L 10/13/17 09:13 10/20/17 13:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.37 0.19 ug/L 10/13/17 09:13 10/20/17 13:42 1PCB-1221 <0.37
0.37 0.19 ug/L 10/13/17 09:13 10/20/17 13:42 1PCB-1232 <0.37
0.37 0.19 ug/L 10/13/17 09:13 10/20/17 13:42 1PCB-1242 <0.37
0.37 0.19 ug/L 10/13/17 09:13 10/20/17 13:42 1PCB-1248 <0.37
0.37 0.19 ug/L 10/13/17 09:13 10/20/17 13:42 1PCB-1254 <0.37
0.37 0.065 ug/L 10/13/17 09:13 10/20/17 13:42 1PCB-1260 <0.37
Tetrachloro-m-xylene 70 30-120 10/13/17 09:13 10/20/17 13:42 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
DCB Decachlorobiphenyl 97 10/13/17 09:13 10/20/17 13:42 130-140
Method: 8151A - Herbicides (GC)
RL MDL
2,4-D <1.0 1.0 0.47 ug/L 10/12/17 11:45 10/16/17 19:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.0 0.17 ug/L 10/12/17 11:45 10/16/17 19:19 1Dinoseb<2.0
0.51 0.091 ug/L 10/12/17 11:45 10/16/17 19:19 1Pentachlorophenol<0.51
1.0 0.29 ug/L 10/12/17 11:45 10/16/17 19:19 1Silvex (2,4,5-TP)<1.0
1.0 0.44 ug/L 10/12/17 11:45 10/16/17 19:19 12,4,5-T <1.0
DCAA 61 25-130 10/12/17 11:45 10/16/17 19:19 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 10/13/17 08:45 10/16/17 20:46 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 10/13/17 08:45 10/16/17 20:46 1Arsenic0.19 J
2.5 0.37 ug/L 10/13/17 08:45 10/16/17 20:46 1Barium240B
1.0 0.43 ug/L 10/13/17 08:45 10/16/17 20:46 1Beryllium<1.0
0.50 0.15 ug/L 10/13/17 08:45 10/16/17 20:46 1Cadmium<0.50
5.0 2.3 ug/L 10/13/17 08:45 10/16/17 20:46 1Chromium3.3 J
1.0 0.27 ug/L 10/13/17 08:45 10/16/17 20:46 1Cobalt8.7
2.0 0.63 ug/L 10/13/17 08:45 10/17/17 15:32 1Copper4.7
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-4Client Sample ID: MW-12 Infill
Matrix: WaterDate Collected: 10/11/17 13:15
Date Received: 10/12/17 10:00
Method: 200.8 - Metals (ICP/MS) (Continued)
RL MDL
Iron 930 100 38 ug/L 10/13/17 08:45 10/16/17 20:46 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.50 0.16 ug/L 10/13/17 08:45 10/16/17 20:46 1Lead0.85 B
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 20:46 1Manganese340V
2.0 0.92 ug/L 10/13/17 08:45 10/16/17 20:46 1Nickel11
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 20:46 1Selenium<2.5
0.50 0.078 ug/L 10/13/17 08:45 10/16/17 20:46 1Silver<0.50
2.0 0.65 ug/L 10/13/17 08:45 10/16/17 20:46 1Thallium<2.0
10 4.2 ug/L 10/13/17 08:45 10/16/17 20:46 1Tin<10
5.0 2.0 ug/L 10/13/17 08:45 10/17/17 15:32 1Vanadium2.3 J
20 8.1 ug/L 10/13/17 08:45 10/16/17 20:46 1Zinc26B
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 10/18/17 15:35 10/19/17 10:57 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Cyanide, Total <0.010 0.010 0.0035 mg/L 10/24/17 12:00 10/24/17 15:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.0 1.7 mg/L 10/28/17 13:58 10Chloride36
2.0 0.95 mg/L 10/28/17 13:58 10Sulfate75
5.0 3.7 mg/L 10/19/17 15:59 1Alkalinity480
10 4.3 mg/L 10/13/17 06:01 1Total Dissolved Solids 700
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-5Client Sample ID: MW-12D Infill
Matrix: WaterDate Collected: 10/11/17 12:30
Date Received: 10/12/17 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 18:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/18/17 18:06 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/18/17 18:06 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/18/17 18:06 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/18/17 18:06 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/18/17 18:06 11,1-Dichloroethene <1.0
1.0 0.30 ug/L 10/18/17 18:06 11,1-Dichloropropene <1.0
1.0 0.41 ug/L 10/18/17 18:06 11,2,3-Trichloropropane <1.0
1.0 0.34 ug/L 10/18/17 18:06 11,2,4-Trichlorobenzene <1.0
5.0 2.0 ug/L 10/18/17 18:06 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/18/17 18:06 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/18/17 18:06 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/18/17 18:06 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/18/17 18:06 11,2-Dichloropropane <1.0
1.0 0.40 ug/L 10/18/17 18:06 11,3-Dichlorobenzene <1.0
1.0 0.36 ug/L 10/18/17 18:06 11,3-Dichloropropane <1.0
1.0 0.36 ug/L 10/18/17 18:06 11,4-Dichlorobenzene <1.0
1.0 0.44 ug/L 10/18/17 18:06 12,2-Dichloropropane <1.0
5.0 2.1 ug/L 10/18/17 18:06 12-Butanone (MEK)<5.0
1.0 0.23 ug/L 10/18/17 18:06 12-Chloro-1,3-butadiene <1.0
5.0 1.6 ug/L 10/18/17 18:06 12-Hexanone <5.0
2.5 0.86 ug/L 10/18/17 18:06 13-Chloropropene <2.5
5.0 2.2 ug/L 10/18/17 18:06 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/18/17 18:06 1Acetone<5.0
10 4.2 ug/L 10/18/17 18:06 1Acetonitrile<10
100 23 ug/L 10/18/17 18:06 1Acrolein<100
20 4.5 ug/L 10/18/17 18:06 1Acrylonitrile<20
0.50 0.15 ug/L 10/18/17 18:06 1Benzene0.50
1.0 0.43 ug/L 10/18/17 18:06 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/18/17 18:06 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/18/17 18:06 1Bromoform<1.0
2.0 0.80 ug/L 10/18/17 18:06 1Bromomethane<2.0
2.0 0.45 ug/L 10/18/17 18:06 1Carbon disulfide <2.0
1.0 0.38 ug/L 10/18/17 18:06 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/18/17 18:06 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/18/17 18:06 1Chloroethane<1.0
2.0 0.37 ug/L 10/18/17 18:06 1Chloroform<2.0
1.0 0.32 ug/L 10/18/17 18:06 1Chloromethane<1.0
1.0 0.41 ug/L 10/18/17 18:06 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/18/17 18:06 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/18/17 18:06 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/18/17 18:06 1Dibromomethane<1.0
2.0 0.67 ug/L 10/18/17 18:06 1Dichlorodifluoromethane<2.0
2.5 0.53 ug/L 10/18/17 18:06 1Ethyl methacrylate <2.5
0.50 0.18 ug/L 10/18/17 18:06 1Ethylbenzene<0.50
1.0 0.45 ug/L 10/18/17 18:06 1Hexachlorobutadiene<1.0
2.5 0.66 ug/L 10/18/17 18:06 1Iodomethane<2.5
100 36 ug/L 10/18/17 18:06 1Isobutyl alcohol <100
10 2.5 ug/L 10/18/17 18:06 1Methacrylonitrile<10
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-5Client Sample ID: MW-12D Infill
Matrix: WaterDate Collected: 10/11/17 12:30
Date Received: 10/12/17 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Methyl methacrylate <2.5 2.5 0.55 ug/L 10/18/17 18:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.0 1.6 ug/L 10/18/17 18:06 1Methylene Chloride 4.8 J cn
10 4.8 ug/L 10/18/17 18:06 1Propionitrile<10
1.0 0.39 ug/L 10/18/17 18:06 1Styrene<1.0
1.0 0.37 ug/L 10/18/17 18:06 1Tetrachloroethene<1.0
10 1.9 ug/L 10/18/17 18:06 1Tetrahydrofuran4.1 J
0.50 0.15 ug/L 10/18/17 18:06 1Toluene<0.50
1.0 0.35 ug/L 10/18/17 18:06 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/18/17 18:06 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/18/17 18:06 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/18/17 18:06 1Trichloroethene<0.50
1.0 0.43 ug/L 10/18/17 18:06 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/18/17 18:06 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/18/17 18:06 1Vinyl chloride 1.7
1.0 0.22 ug/L 10/18/17 18:06 1Xylenes, Total <1.0
1,2-Dichloroethane-d4 (Surr)106 75-126 10/18/17 18:06 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)98 10/18/17 18:06 172-124
Dibromofluoromethane 96 10/18/17 18:06 175-120
Toluene-d8 (Surr)97 10/18/17 18:06 175-120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.74 0.74 0.23 ug/L 10/16/17 07:32 10/19/17 00:04 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.74 0.20 ug/L 10/16/17 07:32 10/19/17 00:04 1Acenaphthylene<0.74
3.7 0.49 ug/L 10/16/17 07:32 10/19/17 00:04 1Acetophenone<3.7
7.4 1.6 ug/L 10/16/17 07:32 10/19/17 00:04 12-Acetylaminofluorene <7.4
7.4 2.8 ug/L 10/16/17 07:32 10/19/17 00:04 14-Aminobiphenyl <7.4
0.74 0.25 ug/L 10/16/17 07:32 10/19/17 00:04 1Anthracene<0.74
0.15 0.042 ug/L 10/16/17 07:32 10/19/17 00:04 1Benzo[a]anthracene 0.16
0.15 0.073 ug/L 10/16/17 07:32 10/19/17 00:04 1Benzo[a]pyrene 0.18
0.15 0.060 ug/L 10/16/17 07:32 10/19/17 00:04 1Benzo[b]fluoranthene 0.26
0.74 0.28 ug/L 10/16/17 07:32 10/19/17 00:04 1Benzo[g,h,i]perylene <0.74
0.15 0.047 ug/L 10/16/17 07:32 10/19/17 00:04 1Benzo[k]fluoranthene 0.093 J
15 4.5 ug/L 10/16/17 07:32 10/19/17 00:04 1Benzyl alcohol <15
1.5 0.21 ug/L 10/16/17 07:32 10/19/17 00:04 1Bis(2-chloroethoxy)methane <1.5
1.5 0.22 ug/L 10/16/17 07:32 10/19/17 00:04 1Bis(2-chloroethyl)ether <1.5
7.4 1.3 ug/L 10/16/17 07:32 10/19/17 00:04 1Bis(2-ethylhexyl) phthalate <7.4
3.7 0.40 ug/L 10/16/17 07:32 10/19/17 00:04 14-Bromophenyl phenyl ether <3.7
1.5 0.35 ug/L 10/16/17 07:32 10/19/17 00:04 1Butyl benzyl phthalate <1.5
7.4 1.5 ug/L 10/16/17 07:32 10/19/17 00:04 14-Chloroaniline <7.4
7.4 2.5 ug/L 10/16/17 07:32 10/19/17 00:04 1Chlorobenzilate<7.4
7.4 1.7 ug/L 10/16/17 07:32 10/19/17 00:04 14-Chloro-3-methylphenol <7.4
1.5 0.17 ug/L 10/16/17 07:32 10/19/17 00:04 12-Chloronaphthalene <1.5
3.7 0.41 ug/L 10/16/17 07:32 10/19/17 00:04 12-Chlorophenol <3.7
3.7 0.47 ug/L 10/16/17 07:32 10/19/17 00:04 14-Chlorophenyl phenyl ether <3.7
0.15 0.050 ug/L 10/16/17 07:32 10/19/17 00:04 1Chrysene0.18
7.4 4.1 ug/L 10/16/17 07:32 10/19/17 00:04 1Diallate<7.4
0.22 0.038 ug/L 10/16/17 07:32 10/19/17 00:04 1Dibenz(a,h)anthracene <0.22
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-5Client Sample ID: MW-12D Infill
Matrix: WaterDate Collected: 10/11/17 12:30
Date Received: 10/12/17 10:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
Dibenzofuran <1.5 1.5 0.19 ug/L 10/16/17 07:32 10/19/17 00:04 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
3.7 1.3 ug/L 10/16/17 07:32 10/19/17 00:04 13,3'-Dichlorobenzidine <3.7
7.4 1.9 ug/L 10/16/17 07:32 10/19/17 00:04 12,4-Dichlorophenol <7.4
7.4 2.6 ug/L 10/16/17 07:32 10/19/17 00:04 12,6-Dichlorophenol <7.4
3.7 0.27 ug/L 10/16/17 07:32 10/19/17 00:04 1Diethyl phthalate <3.7
7.4 1.4 ug/L 10/16/17 07:32 10/19/17 00:04 1Dimethoate<7.4
30 2.2 ug/L 10/16/17 07:32 10/19/17 00:04 17,12-Dimethylbenz(a)anthracene <30
30 13 ug/L 10/16/17 07:32 10/19/17 00:04 13,3'-Dimethylbenzidine <30
7.4 1.3 ug/L 10/16/17 07:32 10/19/17 00:04 12,4-Dimethylphenol <7.4
3.7 0.23 ug/L 10/16/17 07:32 10/19/17 00:04 1Dimethyl phthalate <3.7
3.7 0.54 ug/L 10/16/17 07:32 10/19/17 00:04 1Di-n-butyl phthalate 0.73 J
15 4.4 ug/L 10/16/17 07:32 10/19/17 00:04 14,6-Dinitro-2-methylphenol <15
15 6.3 ug/L 10/16/17 07:32 10/19/17 00:04 12,4-Dinitrophenol <15
0.74 0.18 ug/L 10/16/17 07:32 10/19/17 00:04 12,4-Dinitrotoluene <0.74
0.74 0.055 ug/L 10/16/17 07:32 10/19/17 00:04 12,6-Dinitrotoluene <0.74
7.4 0.78 ug/L 10/16/17 07:32 10/19/17 00:04 1Di-n-octyl phthalate <7.4
7.4 1.9 ug/L 10/16/17 07:32 10/19/17 00:04 1Diphenylamine<7.4
7.4 1.4 ug/L 10/16/17 07:32 10/19/17 00:04 1Disulfoton<7.4
15 2.8 ug/L 10/16/17 07:32 10/19/17 00:04 1Ethyl methanesulfonate <15
7.4 1.5 ug/L 10/16/17 07:32 10/19/17 00:04 1Ethyl Parathion <7.4
30 22 ug/L 10/16/17 07:32 10/19/17 00:04 1Famphur<30
0.74 0.34 ug/L 10/16/17 07:32 10/19/17 00:04 1Fluoranthene<0.74
0.74 0.18 ug/L 10/16/17 07:32 10/19/17 00:04 1Fluorene<0.74
0.37 0.059 ug/L 10/16/17 07:32 10/19/17 00:04 1Hexachlorobenzene<0.37
15 4.7 ug/L 10/16/17 07:32 10/19/17 00:04 1Hexachlorocyclopentadiene<15
3.7 0.44 ug/L 10/16/17 07:32 10/19/17 00:04 1Hexachloroethane<3.7
15 3.5 ug/L 10/16/17 07:32 10/19/17 00:04 1Hexachloropropene<15
0.15 0.055 ug/L 10/16/17 07:32 10/19/17 00:04 1Indeno[1,2,3-cd]pyrene 0.13 J
15 5.1 ug/L 10/16/17 07:32 10/19/17 00:04 1Isodrin<15
1.5 0.28 ug/L 10/16/17 07:32 10/19/17 00:04 1Isophorone<1.5
7.4 2.9 ug/L 10/16/17 07:32 10/19/17 00:04 1Isosafrole<7.4
7.4 1.2 ug/L 10/16/17 07:32 10/19/17 00:04 1Kepone<7.4
3.7 0.98 ug/L 10/16/17 07:32 10/19/17 00:04 1m-Dinitrobenzene <3.7
30 7.5 ug/L 10/16/17 07:32 10/19/17 00:04 1Methapyrilene<30
7.4 1.7 ug/L 10/16/17 07:32 10/19/17 00:04 13-Methylcholanthrene <7.4
30 4.4 ug/L 10/16/17 07:32 10/19/17 00:04 1Methyl methanesulfonate <30
1.5 0.048 ug/L 10/16/17 07:32 10/19/17 00:04 12-Methylnaphthalene <1.5
7.4 1.7 ug/L 10/16/17 07:32 10/19/17 00:04 1Methyl parathion <7.4
1.5 0.23 ug/L 10/16/17 07:32 10/19/17 00:04 12-Methylphenol <1.5
1.5 0.33 ug/L 10/16/17 07:32 10/19/17 00:04 13 & 4 Methylphenol <1.5
0.74 0.23 ug/L 10/16/17 07:32 10/19/17 00:04 1Naphthalene<0.74
30 29 ug/L 10/16/17 07:32 10/19/17 00:04 11,4-Naphthoquinone <30
15 4.4 ug/L 10/16/17 07:32 10/19/17 00:04 11-Naphthylamine <15
15 6.7 ug/L 10/16/17 07:32 10/19/17 00:04 12-Naphthylamine <15
3.7 0.95 ug/L 10/16/17 07:32 10/19/17 00:04 12-Nitroaniline <3.7
7.4 1.3 ug/L 10/16/17 07:32 10/19/17 00:04 13-Nitroaniline <7.4
7.4 1.2 ug/L 10/16/17 07:32 10/19/17 00:04 14-Nitroaniline <7.4
0.74 0.33 ug/L 10/16/17 07:32 10/19/17 00:04 1Nitrobenzene<0.74
7.4 2.3 ug/L 10/16/17 07:32 10/19/17 00:04 15-Nitro-o-toluidine <7.4
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-5Client Sample ID: MW-12D Infill
Matrix: WaterDate Collected: 10/11/17 12:30
Date Received: 10/12/17 10:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
2-Nitrophenol <7.4 7.4 1.8 ug/L 10/16/17 07:32 10/19/17 00:04 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
15 5.5 ug/L 10/16/17 07:32 10/19/17 00:04 14-Nitrophenol <15
15 6.3 ug/L 10/16/17 07:32 10/19/17 00:04 1N-Nitrosodiethylamine <15
7.4 3.5 ug/L 10/16/17 07:32 10/19/17 00:04 1N-Nitrosodimethylamine <7.4
7.4 3.1 ug/L 10/16/17 07:32 10/19/17 00:04 1N-Nitrosodi-n-butylamine <7.4
0.37 0.11 ug/L 10/16/17 07:32 10/19/17 00:04 1N-Nitrosodi-n-propylamine <0.37
1.5 0.27 ug/L 10/16/17 07:32 10/19/17 00:04 1N-Nitrosodiphenylamine <1.5
15 5.5 ug/L 10/16/17 07:32 10/19/17 00:04 1N-Nitrosomethylethylamine <15
7.4 2.6 ug/L 10/16/17 07:32 10/19/17 00:04 1N-Nitrosopiperidine <7.4
7.4 2.5 ug/L 10/16/17 07:32 10/19/17 00:04 1N-Nitrosopyrrolidine <7.4
15 4.1 ug/L 10/16/17 07:32 10/19/17 00:04 1o,o',o''-Triethylphosphorothioate <15
30 5.9 ug/L 10/16/17 07:32 10/19/17 00:04 1o-Toluidine <30
1.5 0.28 ug/L 10/16/17 07:32 10/19/17 00:04 12,2'-oxybis[1-chloropropane]<1.5
7.4 2.2 ug/L 10/16/17 07:32 10/19/17 00:04 1p-Dimethylamino azobenzene <7.4
7.4 2.1 ug/L 10/16/17 07:32 10/19/17 00:04 1Pentachlorobenzene<7.4
7.4 2.6 ug/L 10/16/17 07:32 10/19/17 00:04 1Pentachloronitrobenzene<7.4
7.4 1.7 ug/L 10/16/17 07:32 10/19/17 00:04 1Phenacetin<7.4
0.74 0.22 ug/L 10/16/17 07:32 10/19/17 00:04 1Phenanthrene<0.74
3.7 0.50 ug/L 10/16/17 07:32 10/19/17 00:04 1Phenol<3.7
7.4 1.6 ug/L 10/16/17 07:32 10/19/17 00:04 1Phorate<7.4
59 12 ug/L 10/16/17 07:32 10/19/17 00:04 1p-Phenylene diamine <59
7.4 1.6 ug/L 10/16/17 07:32 10/19/17 00:04 1Pronamide<7.4
0.74 0.32 ug/L 10/16/17 07:32 10/19/17 00:04 1Pyrene<0.74
7.4 3.0 ug/L 10/16/17 07:32 10/19/17 00:04 1Safrole<7.4
7.4 1.4 ug/L 10/16/17 07:32 10/19/17 00:04 1sym-Trinitrobenzene <7.4
7.4 7.4 ug/L 10/16/17 07:32 10/19/17 00:04 12,3,7,8-TCDD (Screen)<7.4
3.7 0.42 ug/L 10/16/17 07:32 10/19/17 00:04 11,2,4,5-Tetrachlorobenzene <3.7
3.7 0.55 ug/L 10/16/17 07:32 10/19/17 00:04 12,3,4,6-Tetrachlorophenol <3.7
7.4 1.9 ug/L 10/16/17 07:32 10/19/17 00:04 1Thionazin<7.4
7.4 1.9 ug/L 10/16/17 07:32 10/19/17 00:04 12,4,5-Trichlorophenol <7.4
3.7 0.53 ug/L 10/16/17 07:32 10/19/17 00:04 12,4,6-Trichlorophenol <3.7
2-Fluorobiphenyl 80 34-110 10/16/17 07:32 10/19/17 00:04 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol 44 10/16/17 07:32 10/19/17 00:04 127-110
Nitrobenzene-d5 78 10/16/17 07:32 10/19/17 00:04 136-120
Phenol-d5 40 10/16/17 07:32 10/19/17 00:04 120-100
Terphenyl-d14 106 10/16/17 07:32 10/19/17 00:04 140-145
2,4,6-Tribromophenol 110 10/16/17 07:32 10/19/17 00:04 140-145
Method: 8081B - Organochlorine Pesticides (GC)
RL MDL
alpha-BHC <0.037 0.037 0.0024 ug/L 10/13/17 09:13 10/16/17 16:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.037 0.0094 ug/L 10/13/17 09:13 10/16/17 16:58 1beta-BHC <0.037
0.037 0.0095 ug/L 10/13/17 09:13 10/16/17 16:58 1delta-BHC <0.037
0.037 0.0052 ug/L 10/13/17 09:13 10/16/17 16:58 1gamma-BHC (Lindane)<0.037
0.037 0.013 ug/L 10/13/17 09:13 10/16/17 16:58 1Heptachlor<0.037
0.037 0.0049 ug/L 10/13/17 09:13 10/16/17 16:58 1Aldrin<0.037
0.037 0.013 ug/L 10/13/17 09:13 10/16/17 16:58 1Heptachlor epoxide <0.037
0.037 0.0038 ug/L 10/13/17 09:13 10/16/17 16:58 1Endosulfan I <0.037
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-5Client Sample ID: MW-12D Infill
Matrix: WaterDate Collected: 10/11/17 12:30
Date Received: 10/12/17 10:00
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
RL MDL
Dieldrin <0.037 0.037 0.012 ug/L 10/13/17 09:13 10/16/17 16:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.037 0.0035 ug/L 10/13/17 09:13 10/16/17 16:58 14,4'-DDE <0.037
0.037 0.013 ug/L 10/13/17 09:13 10/16/17 16:58 1Endrin<0.037
0.037 0.0026 ug/L 10/13/17 09:13 10/16/17 16:58 1Endosulfan II <0.037
0.037 0.012 ug/L 10/13/17 09:13 10/16/17 16:58 14,4'-DDD <0.037
0.037 0.011 ug/L 10/13/17 09:13 10/16/17 16:58 1Endosulfan sulfate <0.037
0.037 0.0030 ug/L 10/13/17 09:13 10/16/17 16:58 14,4'-DDT <0.037
0.074 0.021 ug/L 10/13/17 09:13 10/16/17 16:58 1Methoxychlor<0.074
0.37 0.19 ug/L 10/13/17 09:13 10/16/17 16:58 1Toxaphene<0.37
0.037 0.0076 ug/L 10/13/17 09:13 10/16/17 16:58 1Endrin aldehyde <0.037
0.074 0.037 ug/L 10/13/17 09:13 10/16/17 16:58 1Chlordane (technical)<0.074
DCB Decachlorobiphenyl 97 30-130 10/13/17 09:13 10/16/17 16:58 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 86 10/13/17 09:13 10/16/17 16:58 130-120
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
RL MDL
PCB-1016 <0.37 0.37 0.062 ug/L 10/13/17 09:13 10/20/17 13:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.37 0.19 ug/L 10/13/17 09:13 10/20/17 13:58 1PCB-1221 <0.37
0.37 0.19 ug/L 10/13/17 09:13 10/20/17 13:58 1PCB-1232 <0.37
0.37 0.19 ug/L 10/13/17 09:13 10/20/17 13:58 1PCB-1242 <0.37
0.37 0.19 ug/L 10/13/17 09:13 10/20/17 13:58 1PCB-1248 <0.37
0.37 0.19 ug/L 10/13/17 09:13 10/20/17 13:58 1PCB-1254 <0.37
0.37 0.065 ug/L 10/13/17 09:13 10/20/17 13:58 1PCB-1260 <0.37
Tetrachloro-m-xylene 85 30-120 10/13/17 09:13 10/20/17 13:58 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
DCB Decachlorobiphenyl 95 10/13/17 09:13 10/20/17 13:58 130-140
Method: 8151A - Herbicides (GC)
RL MDL
2,4-D <0.95 0.95 0.44 ug/L 10/12/17 11:45 10/16/17 19:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.9 0.16 ug/L 10/12/17 11:45 10/16/17 19:43 1Dinoseb<1.9
0.48 0.085 ug/L 10/12/17 11:45 10/16/17 19:43 1Pentachlorophenol<0.48
0.95 0.27 ug/L 10/12/17 11:45 10/16/17 19:43 1Silvex (2,4,5-TP)<0.95
0.95 0.41 ug/L 10/12/17 11:45 10/16/17 19:43 12,4,5-T <0.95
DCAA 63 25-130 10/12/17 11:45 10/16/17 19:43 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 10/13/17 08:45 10/16/17 21:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 10/13/17 08:45 10/16/17 21:01 1Arsenic3.1
2.5 0.37 ug/L 10/13/17 08:45 10/16/17 21:01 1Barium210B
1.0 0.43 ug/L 10/13/17 08:45 10/16/17 21:01 1Beryllium<1.0
0.50 0.15 ug/L 10/13/17 08:45 10/16/17 21:01 1Cadmium<0.50
5.0 2.3 ug/L 10/13/17 08:45 10/16/17 21:01 1Chromium<5.0
1.0 0.27 ug/L 10/13/17 08:45 10/16/17 21:01 1Cobalt2.3
2.0 0.63 ug/L 10/13/17 08:45 10/17/17 15:51 1Copper2.5
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-5Client Sample ID: MW-12D Infill
Matrix: WaterDate Collected: 10/11/17 12:30
Date Received: 10/12/17 10:00
Method: 200.8 - Metals (ICP/MS) (Continued)
RL MDL
Iron 7000 100 38 ug/L 10/13/17 08:45 10/16/17 21:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.50 0.16 ug/L 10/13/17 08:45 10/16/17 21:01 1Lead0.65 B
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 21:01 1Manganese480
2.0 0.92 ug/L 10/13/17 08:45 10/16/17 21:01 1Nickel4.1
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 21:01 1Selenium<2.5
0.50 0.078 ug/L 10/13/17 08:45 10/16/17 21:01 1Silver<0.50
2.0 0.65 ug/L 10/13/17 08:45 10/16/17 21:01 1Thallium<2.0
10 4.2 ug/L 10/13/17 08:45 10/16/17 21:01 1Tin<10
5.0 2.0 ug/L 10/13/17 08:45 10/17/17 15:51 1Vanadium<5.0
20 8.1 ug/L 10/13/17 08:45 10/16/17 21:01 1Zinc27B
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 10/18/17 15:35 10/19/17 10:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Cyanide, Total <0.010 0.010 0.0035 mg/L 10/24/17 12:00 10/24/17 15:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.0 1.7 mg/L 10/28/17 14:10 10Chloride34
2.0 0.95 mg/L 10/28/17 14:10 10Sulfate52
5.0 3.7 mg/L 10/19/17 16:08 1Alkalinity580
10 4.3 mg/L 10/13/17 06:03 1Total Dissolved Solids 780
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-6Client Sample ID: Infill Duplicate 1
Matrix: WaterDate Collected: 10/11/17 12:30
Date Received: 10/12/17 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 18:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/18/17 18:33 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/18/17 18:33 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/18/17 18:33 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/18/17 18:33 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/18/17 18:33 11,1-Dichloroethene <1.0
1.0 0.30 ug/L 10/18/17 18:33 11,1-Dichloropropene <1.0
1.0 0.41 ug/L 10/18/17 18:33 11,2,3-Trichloropropane <1.0
1.0 0.34 ug/L 10/18/17 18:33 11,2,4-Trichlorobenzene <1.0
5.0 2.0 ug/L 10/18/17 18:33 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/18/17 18:33 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/18/17 18:33 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/18/17 18:33 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/18/17 18:33 11,2-Dichloropropane <1.0
1.0 0.40 ug/L 10/18/17 18:33 11,3-Dichlorobenzene <1.0
1.0 0.36 ug/L 10/18/17 18:33 11,3-Dichloropropane <1.0
1.0 0.36 ug/L 10/18/17 18:33 11,4-Dichlorobenzene <1.0
1.0 0.44 ug/L 10/18/17 18:33 12,2-Dichloropropane <1.0
5.0 2.1 ug/L 10/18/17 18:33 12-Butanone (MEK)<5.0
1.0 0.23 ug/L 10/18/17 18:33 12-Chloro-1,3-butadiene <1.0
5.0 1.6 ug/L 10/18/17 18:33 12-Hexanone <5.0
2.5 0.86 ug/L 10/18/17 18:33 13-Chloropropene <2.5
5.0 2.2 ug/L 10/18/17 18:33 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/18/17 18:33 1Acetone<5.0
10 4.2 ug/L 10/18/17 18:33 1Acetonitrile<10
100 23 ug/L 10/18/17 18:33 1Acrolein<100
20 4.5 ug/L 10/18/17 18:33 1Acrylonitrile<20
0.50 0.15 ug/L 10/18/17 18:33 1Benzene0.54
1.0 0.43 ug/L 10/18/17 18:33 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/18/17 18:33 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/18/17 18:33 1Bromoform<1.0
2.0 0.80 ug/L 10/18/17 18:33 1Bromomethane<2.0
2.0 0.45 ug/L 10/18/17 18:33 1Carbon disulfide <2.0
1.0 0.38 ug/L 10/18/17 18:33 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/18/17 18:33 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/18/17 18:33 1Chloroethane<1.0
2.0 0.37 ug/L 10/18/17 18:33 1Chloroform<2.0
1.0 0.32 ug/L 10/18/17 18:33 1Chloromethane<1.0
1.0 0.41 ug/L 10/18/17 18:33 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/18/17 18:33 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/18/17 18:33 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/18/17 18:33 1Dibromomethane<1.0
2.0 0.67 ug/L 10/18/17 18:33 1Dichlorodifluoromethane<2.0
2.5 0.53 ug/L 10/18/17 18:33 1Ethyl methacrylate <2.5
0.50 0.18 ug/L 10/18/17 18:33 1Ethylbenzene<0.50
1.0 0.45 ug/L 10/18/17 18:33 1Hexachlorobutadiene<1.0
2.5 0.66 ug/L 10/18/17 18:33 1Iodomethane<2.5
100 36 ug/L 10/18/17 18:33 1Isobutyl alcohol <100
10 2.5 ug/L 10/18/17 18:33 1Methacrylonitrile<10
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-6Client Sample ID: Infill Duplicate 1
Matrix: WaterDate Collected: 10/11/17 12:30
Date Received: 10/12/17 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Methyl methacrylate <2.5 2.5 0.55 ug/L 10/18/17 18:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.0 1.6 ug/L 10/18/17 18:33 1Methylene Chloride 5.2 cn
10 4.8 ug/L 10/18/17 18:33 1Propionitrile<10
1.0 0.39 ug/L 10/18/17 18:33 1Styrene<1.0
1.0 0.37 ug/L 10/18/17 18:33 1Tetrachloroethene<1.0
10 1.9 ug/L 10/18/17 18:33 1Tetrahydrofuran<10
0.50 0.15 ug/L 10/18/17 18:33 1Toluene<0.50
1.0 0.35 ug/L 10/18/17 18:33 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/18/17 18:33 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/18/17 18:33 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/18/17 18:33 1Trichloroethene<0.50
1.0 0.43 ug/L 10/18/17 18:33 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/18/17 18:33 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/18/17 18:33 1Vinyl chloride 1.7
1.0 0.22 ug/L 10/18/17 18:33 1Xylenes, Total <1.0
1,2-Dichloroethane-d4 (Surr)107 75-126 10/18/17 18:33 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)96 10/18/17 18:33 172-124
Dibromofluoromethane 100 10/18/17 18:33 175-120
Toluene-d8 (Surr)94 10/18/17 18:33 175-120
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-7Client Sample ID: MW-7D Infill
Matrix: WaterDate Collected: 10/11/17 14:40
Date Received: 10/12/17 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 19:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/18/17 19:00 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/18/17 19:00 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/18/17 19:00 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/18/17 19:00 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/18/17 19:00 11,1-Dichloroethene <1.0
1.0 0.30 ug/L 10/18/17 19:00 11,1-Dichloropropene <1.0
1.0 0.41 ug/L 10/18/17 19:00 11,2,3-Trichloropropane <1.0
1.0 0.34 ug/L 10/18/17 19:00 11,2,4-Trichlorobenzene <1.0
5.0 2.0 ug/L 10/18/17 19:00 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/18/17 19:00 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/18/17 19:00 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/18/17 19:00 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/18/17 19:00 11,2-Dichloropropane <1.0
1.0 0.40 ug/L 10/18/17 19:00 11,3-Dichlorobenzene <1.0
1.0 0.36 ug/L 10/18/17 19:00 11,3-Dichloropropane <1.0
1.0 0.36 ug/L 10/18/17 19:00 11,4-Dichlorobenzene <1.0
1.0 0.44 ug/L 10/18/17 19:00 12,2-Dichloropropane <1.0
5.0 2.1 ug/L 10/18/17 19:00 12-Butanone (MEK)<5.0
1.0 0.23 ug/L 10/18/17 19:00 12-Chloro-1,3-butadiene <1.0
5.0 1.6 ug/L 10/18/17 19:00 12-Hexanone <5.0
2.5 0.86 ug/L 10/18/17 19:00 13-Chloropropene <2.5
5.0 2.2 ug/L 10/18/17 19:00 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/18/17 19:00 1Acetone<5.0
10 4.2 ug/L 10/18/17 19:00 1Acetonitrile<10
100 23 ug/L 10/18/17 19:00 1Acrolein<100
20 4.5 ug/L 10/18/17 19:00 1Acrylonitrile<20
0.50 0.15 ug/L 10/18/17 19:00 1Benzene0.78
1.0 0.43 ug/L 10/18/17 19:00 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/18/17 19:00 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/18/17 19:00 1Bromoform<1.0
2.0 0.80 ug/L 10/18/17 19:00 1Bromomethane<2.0
2.0 0.45 ug/L 10/18/17 19:00 1Carbon disulfide <2.0
1.0 0.38 ug/L 10/18/17 19:00 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/18/17 19:00 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/18/17 19:00 1Chloroethane<1.0
2.0 0.37 ug/L 10/18/17 19:00 1Chloroform<2.0
1.0 0.32 ug/L 10/18/17 19:00 1Chloromethane<1.0
1.0 0.41 ug/L 10/18/17 19:00 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/18/17 19:00 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/18/17 19:00 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/18/17 19:00 1Dibromomethane<1.0
2.0 0.67 ug/L 10/18/17 19:00 1Dichlorodifluoromethane<2.0
2.5 0.53 ug/L 10/18/17 19:00 1Ethyl methacrylate <2.5
0.50 0.18 ug/L 10/18/17 19:00 1Ethylbenzene<0.50
1.0 0.45 ug/L 10/18/17 19:00 1Hexachlorobutadiene<1.0
2.5 0.66 ug/L 10/18/17 19:00 1Iodomethane<2.5
100 36 ug/L 10/18/17 19:00 1Isobutyl alcohol <100
10 2.5 ug/L 10/18/17 19:00 1Methacrylonitrile<10
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-7Client Sample ID: MW-7D Infill
Matrix: WaterDate Collected: 10/11/17 14:40
Date Received: 10/12/17 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Methyl methacrylate <2.5 2.5 0.55 ug/L 10/18/17 19:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.0 1.6 ug/L 10/18/17 19:00 1Methylene Chloride <5.0
10 4.8 ug/L 10/18/17 19:00 1Propionitrile<10
1.0 0.39 ug/L 10/18/17 19:00 1Styrene<1.0
1.0 0.37 ug/L 10/18/17 19:00 1Tetrachloroethene<1.0
10 1.9 ug/L 10/18/17 19:00 1Tetrahydrofuran11
0.50 0.15 ug/L 10/18/17 19:00 1Toluene<0.50
1.0 0.35 ug/L 10/18/17 19:00 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/18/17 19:00 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/18/17 19:00 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/18/17 19:00 1Trichloroethene<0.50
1.0 0.43 ug/L 10/18/17 19:00 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/18/17 19:00 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/18/17 19:00 1Vinyl chloride <0.50
1.0 0.22 ug/L 10/18/17 19:00 1Xylenes, Total <1.0
1,2-Dichloroethane-d4 (Surr)106 75-126 10/18/17 19:00 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)97 10/18/17 19:00 172-124
Dibromofluoromethane 97 10/18/17 19:00 175-120
Toluene-d8 (Surr)95 10/18/17 19:00 175-120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.78 0.78 0.24 ug/L 10/16/17 07:32 10/19/17 00:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.78 0.21 ug/L 10/16/17 07:32 10/19/17 00:33 1Acenaphthylene<0.78
3.9 0.51 ug/L 10/16/17 07:32 10/19/17 00:33 1Acetophenone<3.9
7.8 1.6 ug/L 10/16/17 07:32 10/19/17 00:33 12-Acetylaminofluorene <7.8
7.8 2.9 ug/L 10/16/17 07:32 10/19/17 00:33 14-Aminobiphenyl <7.8
0.78 0.26 ug/L 10/16/17 07:32 10/19/17 00:33 1Anthracene<0.78
0.16 0.044 ug/L 10/16/17 07:32 10/19/17 00:33 1Benzo[a]anthracene <0.16
0.16 0.077 ug/L 10/16/17 07:32 10/19/17 00:33 1Benzo[a]pyrene <0.16
0.16 0.063 ug/L 10/16/17 07:32 10/19/17 00:33 1Benzo[b]fluoranthene <0.16
0.78 0.29 ug/L 10/16/17 07:32 10/19/17 00:33 1Benzo[g,h,i]perylene <0.78
0.16 0.050 ug/L 10/16/17 07:32 10/19/17 00:33 1Benzo[k]fluoranthene <0.16
16 4.7 ug/L 10/16/17 07:32 10/19/17 00:33 1Benzyl alcohol <16
1.6 0.22 ug/L 10/16/17 07:32 10/19/17 00:33 1Bis(2-chloroethoxy)methane <1.6
1.6 0.23 ug/L 10/16/17 07:32 10/19/17 00:33 1Bis(2-chloroethyl)ether <1.6
7.8 1.3 ug/L 10/16/17 07:32 10/19/17 00:33 1Bis(2-ethylhexyl) phthalate <7.8
3.9 0.42 ug/L 10/16/17 07:32 10/19/17 00:33 14-Bromophenyl phenyl ether <3.9
1.6 0.37 ug/L 10/16/17 07:32 10/19/17 00:33 1Butyl benzyl phthalate <1.6
7.8 1.6 ug/L 10/16/17 07:32 10/19/17 00:33 14-Chloroaniline <7.8
7.8 2.6 ug/L 10/16/17 07:32 10/19/17 00:33 1Chlorobenzilate<7.8
7.8 1.8 ug/L 10/16/17 07:32 10/19/17 00:33 14-Chloro-3-methylphenol <7.8
1.6 0.18 ug/L 10/16/17 07:32 10/19/17 00:33 12-Chloronaphthalene <1.6
3.9 0.43 ug/L 10/16/17 07:32 10/19/17 00:33 12-Chlorophenol <3.9
3.9 0.49 ug/L 10/16/17 07:32 10/19/17 00:33 14-Chlorophenyl phenyl ether <3.9
0.16 0.053 ug/L 10/16/17 07:32 10/19/17 00:33 1Chrysene<0.16
7.8 4.3 ug/L 10/16/17 07:32 10/19/17 00:33 1Diallate<7.8
0.23 0.039 ug/L 10/16/17 07:32 10/19/17 00:33 1Dibenz(a,h)anthracene <0.23
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-7Client Sample ID: MW-7D Infill
Matrix: WaterDate Collected: 10/11/17 14:40
Date Received: 10/12/17 10:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
Dibenzofuran <1.6 1.6 0.20 ug/L 10/16/17 07:32 10/19/17 00:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
3.9 1.3 ug/L 10/16/17 07:32 10/19/17 00:33 13,3'-Dichlorobenzidine <3.9
7.8 2.0 ug/L 10/16/17 07:32 10/19/17 00:33 12,4-Dichlorophenol <7.8
7.8 2.7 ug/L 10/16/17 07:32 10/19/17 00:33 12,6-Dichlorophenol <7.8
3.9 0.28 ug/L 10/16/17 07:32 10/19/17 00:33 1Diethyl phthalate <3.9
7.8 1.4 ug/L 10/16/17 07:32 10/19/17 00:33 1Dimethoate<7.8
31 2.3 ug/L 10/16/17 07:32 10/19/17 00:33 17,12-Dimethylbenz(a)anthracene <31
31 14 ug/L 10/16/17 07:32 10/19/17 00:33 13,3'-Dimethylbenzidine <31
7.8 1.4 ug/L 10/16/17 07:32 10/19/17 00:33 12,4-Dimethylphenol <7.8
3.9 0.24 ug/L 10/16/17 07:32 10/19/17 00:33 1Dimethyl phthalate <3.9
3.9 0.57 ug/L 10/16/17 07:32 10/19/17 00:33 1Di-n-butyl phthalate <3.9
16 4.6 ug/L 10/16/17 07:32 10/19/17 00:33 14,6-Dinitro-2-methylphenol <16
16 6.7 ug/L 10/16/17 07:32 10/19/17 00:33 12,4-Dinitrophenol <16
0.78 0.19 ug/L 10/16/17 07:32 10/19/17 00:33 12,4-Dinitrotoluene <0.78
0.78 0.057 ug/L 10/16/17 07:32 10/19/17 00:33 12,6-Dinitrotoluene <0.78
7.8 0.81 ug/L 10/16/17 07:32 10/19/17 00:33 1Di-n-octyl phthalate <7.8
7.8 2.0 ug/L 10/16/17 07:32 10/19/17 00:33 1Diphenylamine<7.8
7.8 1.5 ug/L 10/16/17 07:32 10/19/17 00:33 1Disulfoton<7.8
16 2.9 ug/L 10/16/17 07:32 10/19/17 00:33 1Ethyl methanesulfonate <16
7.8 1.6 ug/L 10/16/17 07:32 10/19/17 00:33 1Ethyl Parathion <7.8
31 23 ug/L 10/16/17 07:32 10/19/17 00:33 1Famphur<31
0.78 0.35 ug/L 10/16/17 07:32 10/19/17 00:33 1Fluoranthene<0.78
0.78 0.19 ug/L 10/16/17 07:32 10/19/17 00:33 1Fluorene<0.78
0.39 0.062 ug/L 10/16/17 07:32 10/19/17 00:33 1Hexachlorobenzene<0.39
16 4.9 ug/L 10/16/17 07:32 10/19/17 00:33 1Hexachlorocyclopentadiene<16
3.9 0.46 ug/L 10/16/17 07:32 10/19/17 00:33 1Hexachloroethane<3.9
16 3.6 ug/L 10/16/17 07:32 10/19/17 00:33 1Hexachloropropene<16
0.16 0.058 ug/L 10/16/17 07:32 10/19/17 00:33 1Indeno[1,2,3-cd]pyrene <0.16
16 5.4 ug/L 10/16/17 07:32 10/19/17 00:33 1Isodrin<16
1.6 0.29 ug/L 10/16/17 07:32 10/19/17 00:33 1Isophorone<1.6
7.8 3.0 ug/L 10/16/17 07:32 10/19/17 00:33 1Isosafrole<7.8
7.8 1.3 ug/L 10/16/17 07:32 10/19/17 00:33 1Kepone<7.8
3.9 1.0 ug/L 10/16/17 07:32 10/19/17 00:33 1m-Dinitrobenzene <3.9
31 7.9 ug/L 10/16/17 07:32 10/19/17 00:33 1Methapyrilene<31
7.8 1.8 ug/L 10/16/17 07:32 10/19/17 00:33 13-Methylcholanthrene <7.8
31 4.6 ug/L 10/16/17 07:32 10/19/17 00:33 1Methyl methanesulfonate <31
1.6 0.051 ug/L 10/16/17 07:32 10/19/17 00:33 12-Methylnaphthalene <1.6
7.8 1.8 ug/L 10/16/17 07:32 10/19/17 00:33 1Methyl parathion <7.8
1.6 0.24 ug/L 10/16/17 07:32 10/19/17 00:33 12-Methylphenol <1.6
1.6 0.35 ug/L 10/16/17 07:32 10/19/17 00:33 13 & 4 Methylphenol <1.6
0.78 0.24 ug/L 10/16/17 07:32 10/19/17 00:33 1Naphthalene<0.78
31 30 ug/L 10/16/17 07:32 10/19/17 00:33 11,4-Naphthoquinone <31
16 4.6 ug/L 10/16/17 07:32 10/19/17 00:33 11-Naphthylamine <16
16 7.1 ug/L 10/16/17 07:32 10/19/17 00:33 12-Naphthylamine <16
3.9 1.0 ug/L 10/16/17 07:32 10/19/17 00:33 12-Nitroaniline <3.9
7.8 1.4 ug/L 10/16/17 07:32 10/19/17 00:33 13-Nitroaniline <7.8
7.8 1.3 ug/L 10/16/17 07:32 10/19/17 00:33 14-Nitroaniline <7.8
0.78 0.35 ug/L 10/16/17 07:32 10/19/17 00:33 1Nitrobenzene<0.78
7.8 2.4 ug/L 10/16/17 07:32 10/19/17 00:33 15-Nitro-o-toluidine <7.8
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-7Client Sample ID: MW-7D Infill
Matrix: WaterDate Collected: 10/11/17 14:40
Date Received: 10/12/17 10:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
2-Nitrophenol <7.8 7.8 1.9 ug/L 10/16/17 07:32 10/19/17 00:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
16 5.8 ug/L 10/16/17 07:32 10/19/17 00:33 14-Nitrophenol <16
16 6.7 ug/L 10/16/17 07:32 10/19/17 00:33 1N-Nitrosodiethylamine <16
7.8 3.7 ug/L 10/16/17 07:32 10/19/17 00:33 1N-Nitrosodimethylamine <7.8
7.8 3.2 ug/L 10/16/17 07:32 10/19/17 00:33 1N-Nitrosodi-n-butylamine <7.8
0.39 0.12 ug/L 10/16/17 07:32 10/19/17 00:33 1N-Nitrosodi-n-propylamine <0.39
1.6 0.29 ug/L 10/16/17 07:32 10/19/17 00:33 1N-Nitrosodiphenylamine <1.6
16 5.8 ug/L 10/16/17 07:32 10/19/17 00:33 1N-Nitrosomethylethylamine <16
7.8 2.7 ug/L 10/16/17 07:32 10/19/17 00:33 1N-Nitrosopiperidine <7.8
7.8 2.6 ug/L 10/16/17 07:32 10/19/17 00:33 1N-Nitrosopyrrolidine <7.8
16 4.3 ug/L 10/16/17 07:32 10/19/17 00:33 1o,o',o''-Triethylphosphorothioate <16
31 6.1 ug/L 10/16/17 07:32 10/19/17 00:33 1o-Toluidine <31
1.6 0.29 ug/L 10/16/17 07:32 10/19/17 00:33 12,2'-oxybis[1-chloropropane]<1.6
7.8 2.3 ug/L 10/16/17 07:32 10/19/17 00:33 1p-Dimethylamino azobenzene <7.8
7.8 2.2 ug/L 10/16/17 07:32 10/19/17 00:33 1Pentachlorobenzene<7.8
7.8 2.8 ug/L 10/16/17 07:32 10/19/17 00:33 1Pentachloronitrobenzene<7.8
7.8 1.8 ug/L 10/16/17 07:32 10/19/17 00:33 1Phenacetin<7.8
0.78 0.23 ug/L 10/16/17 07:32 10/19/17 00:33 1Phenanthrene<0.78
3.9 0.52 ug/L 10/16/17 07:32 10/19/17 00:33 1Phenol<3.9
7.8 1.7 ug/L 10/16/17 07:32 10/19/17 00:33 1Phorate<7.8
62 13 ug/L 10/16/17 07:32 10/19/17 00:33 1p-Phenylene diamine <62
7.8 1.7 ug/L 10/16/17 07:32 10/19/17 00:33 1Pronamide<7.8
0.78 0.33 ug/L 10/16/17 07:32 10/19/17 00:33 1Pyrene<0.78
7.8 3.1 ug/L 10/16/17 07:32 10/19/17 00:33 1Safrole<7.8
7.8 1.4 ug/L 10/16/17 07:32 10/19/17 00:33 1sym-Trinitrobenzene <7.8
7.8 7.8 ug/L 10/16/17 07:32 10/19/17 00:33 12,3,7,8-TCDD (Screen)<7.8
3.9 0.44 ug/L 10/16/17 07:32 10/19/17 00:33 11,2,4,5-Tetrachlorobenzene <3.9
3.9 0.58 ug/L 10/16/17 07:32 10/19/17 00:33 12,3,4,6-Tetrachlorophenol <3.9
7.8 2.0 ug/L 10/16/17 07:32 10/19/17 00:33 1Thionazin<7.8
7.8 2.0 ug/L 10/16/17 07:32 10/19/17 00:33 12,4,5-Trichlorophenol <7.8
3.9 0.56 ug/L 10/16/17 07:32 10/19/17 00:33 12,4,6-Trichlorophenol <3.9
2-Fluorobiphenyl 85 34-110 10/16/17 07:32 10/19/17 00:33 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol 56 10/16/17 07:32 10/19/17 00:33 127-110
Nitrobenzene-d5 82 10/16/17 07:32 10/19/17 00:33 136-120
Phenol-d5 48 10/16/17 07:32 10/19/17 00:33 120-100
Terphenyl-d14 92 10/16/17 07:32 10/19/17 00:33 140-145
2,4,6-Tribromophenol 121 10/16/17 07:32 10/19/17 00:33 140-145
Method: 8081B - Organochlorine Pesticides (GC)
RL MDL
alpha-BHC <0.038 0.038 0.0024 ug/L 10/13/17 09:13 10/17/17 13:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.038 0.0096 ug/L 10/13/17 09:13 10/17/17 13:47 1beta-BHC <0.038
0.038 0.0097 ug/L 10/13/17 09:13 10/17/17 13:47 1delta-BHC <0.038
0.038 0.0053 ug/L 10/13/17 09:13 10/17/17 13:47 1gamma-BHC (Lindane)<0.038
0.038 0.013 ug/L 10/13/17 09:13 10/17/17 13:47 1Heptachlor<0.038
0.038 0.0050 ug/L 10/13/17 09:13 10/17/17 13:47 1Aldrin<0.038
0.038 0.013 ug/L 10/13/17 09:13 10/17/17 13:47 1Heptachlor epoxide <0.038
0.038 0.0038 ug/L 10/13/17 09:13 10/17/17 13:47 1Endosulfan I <0.038
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-7Client Sample ID: MW-7D Infill
Matrix: WaterDate Collected: 10/11/17 14:40
Date Received: 10/12/17 10:00
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
RL MDL
Dieldrin <0.038 0.038 0.012 ug/L 10/13/17 09:13 10/17/17 13:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.038 0.0036 ug/L 10/13/17 09:13 10/17/17 13:47 14,4'-DDE <0.038
0.038 0.013 ug/L 10/13/17 09:13 10/17/17 13:47 1Endrin<0.038
0.038 0.0026 ug/L 10/13/17 09:13 10/17/17 13:47 1Endosulfan II <0.038
0.038 0.012 ug/L 10/13/17 09:13 10/17/17 13:47 14,4'-DDD <0.038
0.038 0.011 ug/L 10/13/17 09:13 10/17/17 13:47 1Endosulfan sulfate <0.038
0.038 0.0030 ug/L 10/13/17 09:13 10/17/17 13:47 14,4'-DDT <0.038
0.075 0.022 ug/L 10/13/17 09:13 10/17/17 13:47 1Methoxychlor<0.075
0.38 0.19 ug/L 10/13/17 09:13 10/17/17 13:47 1Toxaphene<0.38
0.038 0.0077 ug/L 10/13/17 09:13 10/17/17 13:47 1Endrin aldehyde <0.038
0.075 0.038 ug/L 10/13/17 09:13 10/17/17 13:47 1Chlordane (technical)<0.075
DCB Decachlorobiphenyl 96 30-130 10/13/17 09:13 10/17/17 13:47 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 82 10/13/17 09:13 10/17/17 13:47 130-120
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
RL MDL
PCB-1016 <0.38 0.38 0.063 ug/L 10/13/17 09:13 10/20/17 14:14 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.38 0.19 ug/L 10/13/17 09:13 10/20/17 14:14 1PCB-1221 <0.38
0.38 0.19 ug/L 10/13/17 09:13 10/20/17 14:14 1PCB-1232 <0.38
0.38 0.19 ug/L 10/13/17 09:13 10/20/17 14:14 1PCB-1242 <0.38
0.38 0.19 ug/L 10/13/17 09:13 10/20/17 14:14 1PCB-1248 <0.38
0.38 0.19 ug/L 10/13/17 09:13 10/20/17 14:14 1PCB-1254 <0.38
0.38 0.066 ug/L 10/13/17 09:13 10/20/17 14:14 1PCB-1260 <0.38
Tetrachloro-m-xylene 92 30-120 10/13/17 09:13 10/20/17 14:14 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
DCB Decachlorobiphenyl 97 10/13/17 09:13 10/20/17 14:14 130-140
Method: 8151A - Herbicides (GC)
RL MDL
2,4-D <0.96 0.96 0.45 ug/L 10/12/17 11:45 10/16/17 20:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.9 0.16 ug/L 10/12/17 11:45 10/16/17 20:08 1Dinoseb<1.9
0.48 0.086 ug/L 10/12/17 11:45 10/16/17 20:08 1Pentachlorophenol<0.48
0.96 0.28 ug/L 10/12/17 11:45 10/16/17 20:08 1Silvex (2,4,5-TP)<0.96
0.96 0.42 ug/L 10/12/17 11:45 10/16/17 20:08 12,4,5-T <0.96
DCAA 59 25-130 10/12/17 11:45 10/16/17 20:08 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony 1.8 J 3.0 1.3 ug/L 10/13/17 08:45 10/16/17 21:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 10/13/17 08:45 10/16/17 21:05 1Arsenic1.1
2.5 0.37 ug/L 10/13/17 08:45 10/16/17 21:05 1Barium270B
1.0 0.43 ug/L 10/13/17 08:45 10/16/17 21:05 1Beryllium<1.0
0.50 0.15 ug/L 10/13/17 08:45 10/16/17 21:05 1Cadmium<0.50
5.0 2.3 ug/L 10/13/17 08:45 10/16/17 21:05 1Chromium6.2
1.0 0.27 ug/L 10/13/17 08:45 10/16/17 21:05 1Cobalt2.4
2.0 0.63 ug/L 10/13/17 08:45 10/17/17 15:55 1Copper2.6
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-7Client Sample ID: MW-7D Infill
Matrix: WaterDate Collected: 10/11/17 14:40
Date Received: 10/12/17 10:00
Method: 200.8 - Metals (ICP/MS) (Continued)
RL MDL
Iron 3000 100 38 ug/L 10/13/17 08:45 10/16/17 21:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.50 0.16 ug/L 10/13/17 08:45 10/16/17 21:05 1Lead0.44 J B
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 21:05 1Manganese1200
2.0 0.92 ug/L 10/13/17 08:45 10/16/17 21:05 1Nickel14
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 21:05 1Selenium<2.5
0.50 0.078 ug/L 10/13/17 08:45 10/16/17 21:05 1Silver<0.50
2.0 0.65 ug/L 10/13/17 08:45 10/16/17 21:05 1Thallium<2.0
10 4.2 ug/L 10/13/17 08:45 10/16/17 21:05 1Tin<10
5.0 2.0 ug/L 10/13/17 08:45 10/17/17 15:55 1Vanadium2.1 J
20 8.1 ug/L 10/13/17 08:45 10/16/17 21:05 1Zinc13J B
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 10/18/17 15:35 10/19/17 11:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Cyanide, Total <0.010 0.010 0.0035 mg/L 10/24/17 12:00 10/24/17 15:03 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.0 4.3 mg/L 10/28/17 14:48 25Chloride89
5.0 2.4 mg/L 10/28/17 14:48 25Sulfate130
5.0 3.7 mg/L 10/19/17 16:19 1Alkalinity730
10 4.3 mg/L 10/13/17 06:06 1Total Dissolved Solids 1200
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-8Client Sample ID: MW-1 Infill
Matrix: WaterDate Collected: 10/11/17 15:40
Date Received: 10/12/17 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 19:25 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/18/17 19:25 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/18/17 19:25 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/18/17 19:25 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/18/17 19:25 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/18/17 19:25 11,1-Dichloroethene <1.0
1.0 0.30 ug/L 10/18/17 19:25 11,1-Dichloropropene <1.0
1.0 0.41 ug/L 10/18/17 19:25 11,2,3-Trichloropropane <1.0
1.0 0.34 ug/L 10/18/17 19:25 11,2,4-Trichlorobenzene <1.0
5.0 2.0 ug/L 10/18/17 19:25 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/18/17 19:25 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/18/17 19:25 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/18/17 19:25 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/18/17 19:25 11,2-Dichloropropane <1.0
1.0 0.40 ug/L 10/18/17 19:25 11,3-Dichlorobenzene <1.0
1.0 0.36 ug/L 10/18/17 19:25 11,3-Dichloropropane <1.0
1.0 0.36 ug/L 10/18/17 19:25 11,4-Dichlorobenzene <1.0
1.0 0.44 ug/L 10/18/17 19:25 12,2-Dichloropropane <1.0
5.0 2.1 ug/L 10/18/17 19:25 12-Butanone (MEK)<5.0
1.0 0.23 ug/L 10/18/17 19:25 12-Chloro-1,3-butadiene <1.0
5.0 1.6 ug/L 10/18/17 19:25 12-Hexanone <5.0
2.5 0.86 ug/L 10/18/17 19:25 13-Chloropropene <2.5
5.0 2.2 ug/L 10/18/17 19:25 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/18/17 19:25 1Acetone<5.0
10 4.2 ug/L 10/18/17 19:25 1Acetonitrile<10
100 23 ug/L 10/18/17 19:25 1Acrolein<100
20 4.5 ug/L 10/18/17 19:25 1Acrylonitrile<20
0.50 0.15 ug/L 10/18/17 19:25 1Benzene<0.50
1.0 0.43 ug/L 10/18/17 19:25 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/18/17 19:25 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/18/17 19:25 1Bromoform<1.0
2.0 0.80 ug/L 10/18/17 19:25 1Bromomethane<2.0
2.0 0.45 ug/L 10/18/17 19:25 1Carbon disulfide <2.0
1.0 0.38 ug/L 10/18/17 19:25 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/18/17 19:25 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/18/17 19:25 1Chloroethane<1.0
2.0 0.37 ug/L 10/18/17 19:25 1Chloroform<2.0
1.0 0.32 ug/L 10/18/17 19:25 1Chloromethane<1.0
1.0 0.41 ug/L 10/18/17 19:25 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/18/17 19:25 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/18/17 19:25 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/18/17 19:25 1Dibromomethane<1.0
2.0 0.67 ug/L 10/18/17 19:25 1Dichlorodifluoromethane<2.0
2.5 0.53 ug/L 10/18/17 19:25 1Ethyl methacrylate <2.5
0.50 0.18 ug/L 10/18/17 19:25 1Ethylbenzene<0.50
1.0 0.45 ug/L 10/18/17 19:25 1Hexachlorobutadiene<1.0
2.5 0.66 ug/L 10/18/17 19:25 1Iodomethane<2.5
100 36 ug/L 10/18/17 19:25 1Isobutyl alcohol <100
10 2.5 ug/L 10/18/17 19:25 1Methacrylonitrile<10
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-8Client Sample ID: MW-1 Infill
Matrix: WaterDate Collected: 10/11/17 15:40
Date Received: 10/12/17 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Methyl methacrylate <2.5 2.5 0.55 ug/L 10/18/17 19:25 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.0 1.6 ug/L 10/18/17 19:25 1Methylene Chloride <5.0
10 4.8 ug/L 10/18/17 19:25 1Propionitrile<10
1.0 0.39 ug/L 10/18/17 19:25 1Styrene<1.0
1.0 0.37 ug/L 10/18/17 19:25 1Tetrachloroethene<1.0
10 1.9 ug/L 10/18/17 19:25 1Tetrahydrofuran<10
0.50 0.15 ug/L 10/18/17 19:25 1Toluene<0.50
1.0 0.35 ug/L 10/18/17 19:25 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/18/17 19:25 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/18/17 19:25 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/18/17 19:25 1Trichloroethene<0.50
1.0 0.43 ug/L 10/18/17 19:25 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/18/17 19:25 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/18/17 19:25 1Vinyl chloride <0.50
1.0 0.22 ug/L 10/18/17 19:25 1Xylenes, Total <1.0
1,2-Dichloroethane-d4 (Surr)106 75-126 10/18/17 19:25 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)97 10/18/17 19:25 172-124
Dibromofluoromethane 98 10/18/17 19:25 175-120
Toluene-d8 (Surr)95 10/18/17 19:25 175-120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene <0.76 0.76 0.24 ug/L 10/16/17 07:32 10/20/17 19:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.76 0.20 ug/L 10/16/17 07:32 10/20/17 19:40 1Acenaphthylene<0.76
3.8 0.51 ug/L 10/16/17 07:32 10/20/17 19:40 1Acetophenone<3.8
7.6 1.6 ug/L 10/16/17 07:32 10/20/17 19:40 12-Acetylaminofluorene <7.6
7.6 2.9 ug/L 10/16/17 07:32 10/20/17 19:40 14-Aminobiphenyl <7.6
0.76 0.25 ug/L 10/16/17 07:32 10/20/17 19:40 1Anthracene<0.76
0.15 0.043 ug/L 10/16/17 07:32 10/20/17 19:40 1Benzo[a]anthracene <0.15
0.15 0.075 ug/L 10/16/17 07:32 10/20/17 19:40 1Benzo[a]pyrene <0.15
0.15 0.061 ug/L 10/16/17 07:32 10/20/17 19:40 1Benzo[b]fluoranthene <0.15
0.76 0.29 ug/L 10/16/17 07:32 10/20/17 19:40 1Benzo[g,h,i]perylene <0.76
0.15 0.049 ug/L 10/16/17 07:32 10/20/17 19:40 1Benzo[k]fluoranthene <0.15
15 4.6 ug/L 10/16/17 07:32 10/20/17 19:40 1Benzyl alcohol <15
1.5 0.22 ug/L 10/16/17 07:32 10/20/17 19:40 1Bis(2-chloroethoxy)methane <1.5
1.5 0.22 ug/L 10/16/17 07:32 10/20/17 19:40 1Bis(2-chloroethyl)ether <1.5
7.6 1.3 ug/L 10/16/17 07:32 10/20/17 19:40 1Bis(2-ethylhexyl) phthalate 1.6 J
3.8 0.41 ug/L 10/16/17 07:32 10/20/17 19:40 14-Bromophenyl phenyl ether <3.8
1.5 0.37 ug/L 10/16/17 07:32 10/20/17 19:40 1Butyl benzyl phthalate <1.5
7.6 1.5 ug/L 10/16/17 07:32 10/20/17 19:40 14-Chloroaniline <7.6
7.6 2.6 ug/L 10/16/17 07:32 10/20/17 19:40 1Chlorobenzilate<7.6
7.6 1.8 ug/L 10/16/17 07:32 10/20/17 19:40 14-Chloro-3-methylphenol <7.6
1.5 0.18 ug/L 10/16/17 07:32 10/20/17 19:40 12-Chloronaphthalene <1.5
3.8 0.43 ug/L 10/16/17 07:32 10/20/17 19:40 12-Chlorophenol <3.8
3.8 0.48 ug/L 10/16/17 07:32 10/20/17 19:40 14-Chlorophenyl phenyl ether <3.8
0.15 0.052 ug/L 10/16/17 07:32 10/20/17 19:40 1Chrysene<0.15
7.6 4.2 ug/L 10/16/17 07:32 10/20/17 19:40 1Diallate<7.6
0.23 0.039 ug/L 10/16/17 07:32 10/20/17 19:40 1Dibenz(a,h)anthracene <0.23
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TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-8Client Sample ID: MW-1 Infill
Matrix: WaterDate Collected: 10/11/17 15:40
Date Received: 10/12/17 10:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
Dibenzofuran <1.5 1.5 0.20 ug/L 10/16/17 07:32 10/20/17 19:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
3.8 1.3 ug/L 10/16/17 07:32 10/20/17 19:40 13,3'-Dichlorobenzidine <3.8
7.6 2.0 ug/L 10/16/17 07:32 10/20/17 19:40 12,4-Dichlorophenol <7.6
7.6 2.7 ug/L 10/16/17 07:32 10/20/17 19:40 12,6-Dichlorophenol <7.6
3.8 0.28 ug/L 10/16/17 07:32 10/20/17 19:40 1Diethyl phthalate <3.8
7.6 1.4 ug/L 10/16/17 07:32 10/20/17 19:40 1Dimethoate<7.6
31 2.3 ug/L 10/16/17 07:32 10/20/17 19:40 17,12-Dimethylbenz(a)anthracene <31
31 14 ug/L 10/16/17 07:32 10/20/17 19:40 13,3'-Dimethylbenzidine <31
7.6 1.4 ug/L 10/16/17 07:32 10/20/17 19:40 12,4-Dimethylphenol <7.6
3.8 0.24 ug/L 10/16/17 07:32 10/20/17 19:40 1Dimethyl phthalate <3.8
3.8 0.56 ug/L 10/16/17 07:32 10/20/17 19:40 1Di-n-butyl phthalate <3.8
15 4.5 ug/L 10/16/17 07:32 10/20/17 19:40 14,6-Dinitro-2-methylphenol <15
15 6.6 ug/L 10/16/17 07:32 10/20/17 19:40 12,4-Dinitrophenol <15
0.76 0.19 ug/L 10/16/17 07:32 10/20/17 19:40 12,4-Dinitrotoluene <0.76
0.76 0.056 ug/L 10/16/17 07:32 10/20/17 19:40 12,6-Dinitrotoluene <0.76
7.6 0.80 ug/L 10/16/17 07:32 10/20/17 19:40 1Di-n-octyl phthalate <7.6
7.6 1.9 ug/L 10/16/17 07:32 10/20/17 19:40 1Diphenylamine<7.6
7.6 1.5 ug/L 10/16/17 07:32 10/20/17 19:40 1Disulfoton<7.6
15 2.9 ug/L 10/16/17 07:32 10/20/17 19:40 1Ethyl methanesulfonate <15
7.6 1.6 ug/L 10/16/17 07:32 10/20/17 19:40 1Ethyl Parathion <7.6
31 23 ug/L 10/16/17 07:32 10/20/17 19:40 1Famphur<31
0.76 0.35 ug/L 10/16/17 07:32 10/20/17 19:40 1Fluoranthene<0.76
0.76 0.19 ug/L 10/16/17 07:32 10/20/17 19:40 1Fluorene<0.76
0.38 0.061 ug/L 10/16/17 07:32 10/20/17 19:40 1Hexachlorobenzene<0.38
15 4.9 ug/L 10/16/17 07:32 10/20/17 19:40 1Hexachlorocyclopentadiene<15
3.8 0.46 ug/L 10/16/17 07:32 10/20/17 19:40 1Hexachloroethane<3.8
15 3.6 ug/L 10/16/17 07:32 10/20/17 19:40 1Hexachloropropene<15
0.15 0.057 ug/L 10/16/17 07:32 10/20/17 19:40 1Indeno[1,2,3-cd]pyrene <0.15
15 5.3 ug/L 10/16/17 07:32 10/20/17 19:40 1Isodrin<15
1.5 0.29 ug/L 10/16/17 07:32 10/20/17 19:40 1Isophorone<1.5
7.6 3.0 ug/L 10/16/17 07:32 10/20/17 19:40 1Isosafrole<7.6
7.6 1.3 ug/L 10/16/17 07:32 10/20/17 19:40 1Kepone<7.6
3.8 1.0 ug/L 10/16/17 07:32 10/20/17 19:40 1m-Dinitrobenzene <3.8
31 7.7 ug/L 10/16/17 07:32 10/20/17 19:40 1Methapyrilene<31
7.6 1.7 ug/L 10/16/17 07:32 10/20/17 19:40 13-Methylcholanthrene <7.6
31 4.5 ug/L 10/16/17 07:32 10/20/17 19:40 1Methyl methanesulfonate <31
1.5 0.050 ug/L 10/16/17 07:32 10/20/17 19:40 12-Methylnaphthalene <1.5
7.6 1.8 ug/L 10/16/17 07:32 10/20/17 19:40 1Methyl parathion <7.6
1.5 0.23 ug/L 10/16/17 07:32 10/20/17 19:40 12-Methylphenol <1.5
1.5 0.34 ug/L 10/16/17 07:32 10/20/17 19:40 13 & 4 Methylphenol <1.5
0.76 0.24 ug/L 10/16/17 07:32 10/20/17 19:40 1Naphthalene<0.76
31 30 ug/L 10/16/17 07:32 10/20/17 19:40 11,4-Naphthoquinone <31
15 4.5 ug/L 10/16/17 07:32 10/20/17 19:40 11-Naphthylamine <15
15 7.0 ug/L 10/16/17 07:32 10/20/17 19:40 12-Naphthylamine <15
3.8 0.98 ug/L 10/16/17 07:32 10/20/17 19:40 12-Nitroaniline <3.8
7.6 1.4 ug/L 10/16/17 07:32 10/20/17 19:40 13-Nitroaniline <7.6
7.6 1.3 ug/L 10/16/17 07:32 10/20/17 19:40 14-Nitroaniline <7.6
0.76 0.34 ug/L 10/16/17 07:32 10/20/17 19:40 1Nitrobenzene<0.76
7.6 2.4 ug/L 10/16/17 07:32 10/20/17 19:40 15-Nitro-o-toluidine <7.6
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-8Client Sample ID: MW-1 Infill
Matrix: WaterDate Collected: 10/11/17 15:40
Date Received: 10/12/17 10:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
2-Nitrophenol <7.6 7.6 1.9 ug/L 10/16/17 07:32 10/20/17 19:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
15 5.7 ug/L 10/16/17 07:32 10/20/17 19:40 14-Nitrophenol <15
15 6.6 ug/L 10/16/17 07:32 10/20/17 19:40 1N-Nitrosodiethylamine <15
7.6 3.6 ug/L 10/16/17 07:32 10/20/17 19:40 1N-Nitrosodimethylamine <7.6
7.6 3.2 ug/L 10/16/17 07:32 10/20/17 19:40 1N-Nitrosodi-n-butylamine <7.6
0.38 0.12 ug/L 10/16/17 07:32 10/20/17 19:40 1N-Nitrosodi-n-propylamine <0.38
1.5 0.28 ug/L 10/16/17 07:32 10/20/17 19:40 1N-Nitrosodiphenylamine <1.5
15 5.7 ug/L 10/16/17 07:32 10/20/17 19:40 1N-Nitrosomethylethylamine <15
7.6 2.7 ug/L 10/16/17 07:32 10/20/17 19:40 1N-Nitrosopiperidine <7.6
7.6 2.6 ug/L 10/16/17 07:32 10/20/17 19:40 1N-Nitrosopyrrolidine <7.6
15 4.2 ug/L 10/16/17 07:32 10/20/17 19:40 1o,o',o''-Triethylphosphorothioate <15
31 6.0 ug/L 10/16/17 07:32 10/20/17 19:40 1o-Toluidine <31
1.5 0.29 ug/L 10/16/17 07:32 10/20/17 19:40 12,2'-oxybis[1-chloropropane]<1.5
7.6 2.3 ug/L 10/16/17 07:32 10/20/17 19:40 1p-Dimethylamino azobenzene <7.6
7.6 2.1 ug/L 10/16/17 07:32 10/20/17 19:40 1Pentachlorobenzene<7.6
7.6 2.7 ug/L 10/16/17 07:32 10/20/17 19:40 1Pentachloronitrobenzene<7.6
7.6 1.7 ug/L 10/16/17 07:32 10/20/17 19:40 1Phenacetin<7.6
0.76 0.23 ug/L 10/16/17 07:32 10/20/17 19:40 1Phenanthrene<0.76
3.8 0.51 ug/L 10/16/17 07:32 10/20/17 19:40 1Phenol<3.8
7.6 1.6 ug/L 10/16/17 07:32 10/20/17 19:40 1Phorate<7.6
61 12 ug/L 10/16/17 07:32 10/20/17 19:40 1p-Phenylene diamine <61
7.6 1.6 ug/L 10/16/17 07:32 10/20/17 19:40 1Pronamide<7.6
0.76 0.33 ug/L 10/16/17 07:32 10/20/17 19:40 1Pyrene<0.76
7.6 3.1 ug/L 10/16/17 07:32 10/20/17 19:40 1Safrole<7.6
7.6 1.4 ug/L 10/16/17 07:32 10/20/17 19:40 1sym-Trinitrobenzene <7.6
7.6 7.6 ug/L 10/16/17 07:32 10/20/17 19:40 12,3,7,8-TCDD (Screen)<7.6
3.8 0.44 ug/L 10/16/17 07:32 10/20/17 19:40 11,2,4,5-Tetrachlorobenzene <3.8
3.8 0.57 ug/L 10/16/17 07:32 10/20/17 19:40 12,3,4,6-Tetrachlorophenol <3.8
7.6 2.0 ug/L 10/16/17 07:32 10/20/17 19:40 1Thionazin<7.6
7.6 2.0 ug/L 10/16/17 07:32 10/20/17 19:40 12,4,5-Trichlorophenol <7.6
3.8 0.55 ug/L 10/16/17 07:32 10/20/17 19:40 12,4,6-Trichlorophenol <3.8
2-Fluorobiphenyl 77 34-110 10/16/17 07:32 10/20/17 19:40 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol 27 10/16/17 07:32 10/20/17 19:40 127-110
Nitrobenzene-d5 96 10/16/17 07:32 10/20/17 19:40 136-120
Phenol-d5 26 10/16/17 07:32 10/20/17 19:40 120-100
Terphenyl-d14 96 10/16/17 07:32 10/20/17 19:40 140-145
2,4,6-Tribromophenol 39 X 10/16/17 07:32 10/20/17 19:40 140-145
Method: 8081B - Organochlorine Pesticides (GC)
RL MDL
alpha-BHC <0.037 0.037 0.0024 ug/L 10/13/17 09:13 10/17/17 14:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.037 0.0094 ug/L 10/13/17 09:13 10/17/17 14:06 1beta-BHC <0.037
0.037 0.0095 ug/L 10/13/17 09:13 10/17/17 14:06 1delta-BHC <0.037
0.037 0.0051 ug/L 10/13/17 09:13 10/17/17 14:06 1gamma-BHC (Lindane)<0.037
0.037 0.012 ug/L 10/13/17 09:13 10/17/17 14:06 1Heptachlor<0.037
0.037 0.0049 ug/L 10/13/17 09:13 10/17/17 14:06 1Aldrin<0.037
0.037 0.013 ug/L 10/13/17 09:13 10/17/17 14:06 1Heptachlor epoxide <0.037
0.037 0.0038 ug/L 10/13/17 09:13 10/17/17 14:06 1Endosulfan I <0.037
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-8Client Sample ID: MW-1 Infill
Matrix: WaterDate Collected: 10/11/17 15:40
Date Received: 10/12/17 10:00
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
RL MDL
Dieldrin <0.037 0.037 0.012 ug/L 10/13/17 09:13 10/17/17 14:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.037 0.0035 ug/L 10/13/17 09:13 10/17/17 14:06 14,4'-DDE <0.037
0.037 0.013 ug/L 10/13/17 09:13 10/17/17 14:06 1Endrin<0.037
0.037 0.0026 ug/L 10/13/17 09:13 10/17/17 14:06 1Endosulfan II <0.037
0.037 0.012 ug/L 10/13/17 09:13 10/17/17 14:06 14,4'-DDD <0.037
0.037 0.011 ug/L 10/13/17 09:13 10/17/17 14:06 1Endosulfan sulfate <0.037
0.037 0.0029 ug/L 10/13/17 09:13 10/17/17 14:06 14,4'-DDT <0.037
0.073 0.021 ug/L 10/13/17 09:13 10/17/17 14:06 1Methoxychlor<0.073
0.37 0.18 ug/L 10/13/17 09:13 10/17/17 14:06 1Toxaphene<0.37
0.037 0.0075 ug/L 10/13/17 09:13 10/17/17 14:06 1Endrin aldehyde <0.037
0.073 0.037 ug/L 10/13/17 09:13 10/17/17 14:06 1Chlordane (technical)<0.073
DCB Decachlorobiphenyl 45 30-130 10/13/17 09:13 10/17/17 14:06 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Tetrachloro-m-xylene 69 10/13/17 09:13 10/17/17 14:06 130-120
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
RL MDL
PCB-1016 <0.37 0.37 0.061 ug/L 10/13/17 09:13 10/20/17 14:30 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.37 0.18 ug/L 10/13/17 09:13 10/20/17 14:30 1PCB-1221 <0.37
0.37 0.18 ug/L 10/13/17 09:13 10/20/17 14:30 1PCB-1232 <0.37
0.37 0.18 ug/L 10/13/17 09:13 10/20/17 14:30 1PCB-1242 <0.37
0.37 0.18 ug/L 10/13/17 09:13 10/20/17 14:30 1PCB-1248 <0.37
0.37 0.18 ug/L 10/13/17 09:13 10/20/17 14:30 1PCB-1254 <0.37
0.37 0.064 ug/L 10/13/17 09:13 10/20/17 14:30 1PCB-1260 <0.37
Tetrachloro-m-xylene 73 30-120 10/13/17 09:13 10/20/17 14:30 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
DCB Decachlorobiphenyl 53 10/13/17 09:13 10/20/17 14:30 130-140
Method: 8151A - Herbicides (GC)
RL MDL
2,4-D <0.96 0.96 0.44 ug/L 10/12/17 11:45 10/18/17 01:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.9 0.16 ug/L 10/12/17 11:45 10/18/17 01:28 1Dinoseb<1.9
0.48 0.086 ug/L 10/12/17 11:45 10/18/17 01:28 1Pentachlorophenol<0.48
0.96 0.28 ug/L 10/12/17 11:45 10/18/17 01:28 1Silvex (2,4,5-TP)<0.96
0.96 0.41 ug/L 10/12/17 11:45 10/18/17 01:28 12,4,5-T <0.96
DCAA 94 25-130 10/12/17 11:45 10/18/17 01:28 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 10/13/17 08:45 10/16/17 21:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 10/13/17 08:45 10/16/17 21:09 1Arsenic2.6
2.5 0.37 ug/L 10/13/17 08:45 10/16/17 21:09 1Barium250B
1.0 0.43 ug/L 10/13/17 08:45 10/17/17 16:00 1Beryllium0.94 J
0.50 0.15 ug/L 10/13/17 08:45 10/16/17 21:09 1Cadmium0.23 J
5.0 2.3 ug/L 10/13/17 08:45 10/17/17 16:00 1Chromium140
1.0 0.27 ug/L 10/13/17 08:45 10/17/17 16:00 1Cobalt22
2.0 0.63 ug/L 10/13/17 08:45 10/16/17 21:09 1Copper67B
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-8Client Sample ID: MW-1 Infill
Matrix: WaterDate Collected: 10/11/17 15:40
Date Received: 10/12/17 10:00
Method: 200.8 - Metals (ICP/MS) (Continued)
RL MDL
Iron 40000 B 100 38 ug/L 10/13/17 08:45 10/17/17 16:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.50 0.16 ug/L 10/13/17 08:45 10/16/17 21:09 1Lead11B
2.5 1.1 ug/L 10/13/17 08:45 10/17/17 16:00 1Manganese1200
2.0 0.92 ug/L 10/13/17 08:45 10/17/17 16:00 1Nickel88
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 21:09 1Selenium1.6 J B
0.50 0.078 ug/L 10/13/17 08:45 10/16/17 21:09 1Silver<0.50
2.0 0.65 ug/L 10/13/17 08:45 10/16/17 21:09 1Thallium<2.0
10 4.2 ug/L 10/13/17 08:45 10/16/17 21:09 1Tin<10
5.0 2.0 ug/L 10/13/17 08:45 10/17/17 16:00 1Vanadium71
20 8.1 ug/L 10/13/17 08:45 10/16/17 21:09 1Zinc120B
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 10/18/17 15:35 10/19/17 11:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Cyanide, Total <0.010 0.010 0.0035 mg/L 10/24/17 12:00 10/24/17 15:04 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.85 mg/L 10/28/17 15:14 5Chloride21
1.0 0.48 mg/L 10/28/17 15:14 5Sulfate13
5.0 3.7 mg/L 10/19/17 16:25 1Alkalinity210
10 4.3 mg/L 10/13/17 06:08 1Total Dissolved Solids 320
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-9Client Sample ID: TB
Matrix: WaterDate Collected: 10/11/17 00:00
Date Received: 10/12/17 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 19:52 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/18/17 19:52 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/18/17 19:52 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/18/17 19:52 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/18/17 19:52 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/18/17 19:52 11,1-Dichloroethene <1.0
1.0 0.30 ug/L 10/18/17 19:52 11,1-Dichloropropene <1.0
1.0 0.41 ug/L 10/18/17 19:52 11,2,3-Trichloropropane <1.0
1.0 0.34 ug/L 10/18/17 19:52 11,2,4-Trichlorobenzene <1.0
5.0 2.0 ug/L 10/18/17 19:52 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/18/17 19:52 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/18/17 19:52 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/18/17 19:52 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/18/17 19:52 11,2-Dichloropropane <1.0
1.0 0.40 ug/L 10/18/17 19:52 11,3-Dichlorobenzene <1.0
1.0 0.36 ug/L 10/18/17 19:52 11,3-Dichloropropane <1.0
1.0 0.36 ug/L 10/18/17 19:52 11,4-Dichlorobenzene <1.0
1.0 0.44 ug/L 10/18/17 19:52 12,2-Dichloropropane <1.0
5.0 2.1 ug/L 10/18/17 19:52 12-Butanone (MEK)<5.0
1.0 0.23 ug/L 10/18/17 19:52 12-Chloro-1,3-butadiene <1.0
5.0 1.6 ug/L 10/18/17 19:52 12-Hexanone <5.0
2.5 0.86 ug/L 10/18/17 19:52 13-Chloropropene <2.5
5.0 2.2 ug/L 10/18/17 19:52 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/18/17 19:52 1Acetone<5.0
10 4.2 ug/L 10/18/17 19:52 1Acetonitrile<10
100 23 ug/L 10/18/17 19:52 1Acrolein<100
20 4.5 ug/L 10/18/17 19:52 1Acrylonitrile<20
0.50 0.15 ug/L 10/18/17 19:52 1Benzene<0.50
1.0 0.43 ug/L 10/18/17 19:52 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/18/17 19:52 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/18/17 19:52 1Bromoform<1.0
2.0 0.80 ug/L 10/18/17 19:52 1Bromomethane<2.0
2.0 0.45 ug/L 10/18/17 19:52 1Carbon disulfide <2.0
1.0 0.38 ug/L 10/18/17 19:52 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/18/17 19:52 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/18/17 19:52 1Chloroethane<1.0
2.0 0.37 ug/L 10/18/17 19:52 1Chloroform<2.0
1.0 0.32 ug/L 10/18/17 19:52 1Chloromethane<1.0
1.0 0.41 ug/L 10/18/17 19:52 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/18/17 19:52 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/18/17 19:52 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/18/17 19:52 1Dibromomethane<1.0
2.0 0.67 ug/L 10/18/17 19:52 1Dichlorodifluoromethane<2.0
2.5 0.53 ug/L 10/18/17 19:52 1Ethyl methacrylate <2.5
0.50 0.18 ug/L 10/18/17 19:52 1Ethylbenzene<0.50
1.0 0.45 ug/L 10/18/17 19:52 1Hexachlorobutadiene<1.0
2.5 0.66 ug/L 10/18/17 19:52 1Iodomethane<2.5
100 36 ug/L 10/18/17 19:52 1Isobutyl alcohol <100
10 2.5 ug/L 10/18/17 19:52 1Methacrylonitrile<10
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-9Client Sample ID: TB
Matrix: WaterDate Collected: 10/11/17 00:00
Date Received: 10/12/17 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Methyl methacrylate <2.5 2.5 0.55 ug/L 10/18/17 19:52 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.0 1.6 ug/L 10/18/17 19:52 1Methylene Chloride <5.0
10 4.8 ug/L 10/18/17 19:52 1Propionitrile<10
1.0 0.39 ug/L 10/18/17 19:52 1Styrene<1.0
1.0 0.37 ug/L 10/18/17 19:52 1Tetrachloroethene<1.0
10 1.9 ug/L 10/18/17 19:52 1Tetrahydrofuran<10
0.50 0.15 ug/L 10/18/17 19:52 1Toluene<0.50
1.0 0.35 ug/L 10/18/17 19:52 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/18/17 19:52 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/18/17 19:52 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/18/17 19:52 1Trichloroethene<0.50
1.0 0.43 ug/L 10/18/17 19:52 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/18/17 19:52 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/18/17 19:52 1Vinyl chloride <0.50
1.0 0.22 ug/L 10/18/17 19:52 1Xylenes, Total <1.0
1,2-Dichloroethane-d4 (Surr)109 75-126 10/18/17 19:52 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)99 10/18/17 19:52 172-124
Dibromofluoromethane 101 10/18/17 19:52 175-120
Toluene-d8 (Surr)94 10/18/17 19:52 175-120
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-10Client Sample ID: MW-8 NMLF
Matrix: WaterDate Collected: 10/11/17 10:40
Date Received: 10/12/17 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 20:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/18/17 20:19 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/18/17 20:19 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/18/17 20:19 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/18/17 20:19 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/18/17 20:19 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 10/18/17 20:19 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 10/18/17 20:19 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/18/17 20:19 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/18/17 20:19 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/18/17 20:19 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/18/17 20:19 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 10/18/17 20:19 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 10/18/17 20:19 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 10/18/17 20:19 12-Hexanone <5.0
5.0 2.2 ug/L 10/18/17 20:19 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/18/17 20:19 1Acetone<5.0
20 4.5 ug/L 10/18/17 20:19 1Acrylonitrile<20
0.50 0.15 ug/L 10/18/17 20:19 1Benzene<0.50
1.0 0.43 ug/L 10/18/17 20:19 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/18/17 20:19 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/18/17 20:19 1Bromoform<1.0
2.0 0.80 ug/L 10/18/17 20:19 1Bromomethane<2.0
2.0 0.45 ug/L 10/18/17 20:19 1Carbon disulfide <2.0
1.0 0.38 ug/L 10/18/17 20:19 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/18/17 20:19 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/18/17 20:19 1Chloroethane<1.0
2.0 0.37 ug/L 10/18/17 20:19 1Chloroform<2.0
1.0 0.32 ug/L 10/18/17 20:19 1Chloromethane<1.0
1.0 0.41 ug/L 10/18/17 20:19 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/18/17 20:19 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/18/17 20:19 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/18/17 20:19 1Dibromomethane<1.0
0.50 0.18 ug/L 10/18/17 20:19 1Ethylbenzene<0.50
2.5 0.66 ug/L 10/18/17 20:19 1Iodomethane<2.5
5.0 1.6 ug/L 10/18/17 20:19 1Methylene Chloride <5.0
1.0 0.39 ug/L 10/18/17 20:19 1Styrene<1.0
1.0 0.37 ug/L 10/18/17 20:19 1Tetrachloroethene<1.0
10 1.9 ug/L 10/18/17 20:19 1Tetrahydrofuran<10
0.50 0.15 ug/L 10/18/17 20:19 1Toluene<0.50
1.0 0.35 ug/L 10/18/17 20:19 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/18/17 20:19 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/18/17 20:19 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/18/17 20:19 1Trichloroethene<0.50
1.0 0.43 ug/L 10/18/17 20:19 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/18/17 20:19 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/18/17 20:19 1Vinyl chloride <0.50
1.0 0.22 ug/L 10/18/17 20:19 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-10Client Sample ID: MW-8 NMLF
Matrix: WaterDate Collected: 10/11/17 10:40
Date Received: 10/12/17 10:00
1,2-Dichloroethane-d4 (Surr)107 75-126 10/18/17 20:19 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)100 10/18/17 20:19 172-124
Dibromofluoromethane 99 10/18/17 20:19 175-120
Toluene-d8 (Surr)94 10/18/17 20:19 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 10/13/17 08:45 10/16/17 21:13 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 10/13/17 08:45 10/16/17 21:13 1Arsenic1.5
2.5 0.37 ug/L 10/13/17 08:45 10/16/17 21:13 1Barium140B
1.0 0.43 ug/L 10/13/17 08:45 10/17/17 16:04 1Beryllium0.64 J
0.50 0.15 ug/L 10/13/17 08:45 10/16/17 21:13 1Cadmium0.52
5.0 2.3 ug/L 10/13/17 08:45 10/17/17 16:04 1Chromium870
1.0 0.27 ug/L 10/13/17 08:45 10/17/17 16:04 1Cobalt37
2.0 0.63 ug/L 10/13/17 08:45 10/16/17 21:13 1Copper110B
100 38 ug/L 10/13/17 08:45 10/17/17 16:04 1Iron29000B
0.50 0.16 ug/L 10/13/17 08:45 10/16/17 21:13 1Lead13B
2.5 1.1 ug/L 10/13/17 08:45 10/17/17 16:04 1Manganese4300
2.0 0.92 ug/L 10/13/17 08:45 10/17/17 16:04 1Nickel470
2.5 1.1 ug/L 10/13/17 08:45 10/16/17 21:13 1Selenium2.3 J B
0.50 0.078 ug/L 10/13/17 08:45 10/16/17 21:13 1Silver<0.50
2.0 0.65 ug/L 10/13/17 08:45 10/16/17 21:13 1Thallium<2.0
5.0 2.0 ug/L 10/13/17 08:45 10/17/17 16:04 1Vanadium72
20 8.1 ug/L 10/13/17 08:45 10/16/17 21:13 1Zinc79B
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 10/18/17 15:35 10/19/17 11:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chloride 12 1.0 0.85 mg/L 10/28/17 15:52 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.48 mg/L 10/28/17 15:52 5Sulfate46
5.0 3.7 mg/L 10/19/17 16:32 1Alkalinity290
10 4.3 mg/L 10/13/17 06:11 1Total Dissolved Solids 420
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-11Client Sample ID: MW-8D NMLF
Matrix: WaterDate Collected: 10/11/17 10:10
Date Received: 10/12/17 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 20:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/18/17 20:45 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/18/17 20:45 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/18/17 20:45 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/18/17 20:45 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/18/17 20:45 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 10/18/17 20:45 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 10/18/17 20:45 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/18/17 20:45 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/18/17 20:45 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/18/17 20:45 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/18/17 20:45 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 10/18/17 20:45 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 10/18/17 20:45 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 10/18/17 20:45 12-Hexanone <5.0
5.0 2.2 ug/L 10/18/17 20:45 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/18/17 20:45 1Acetone<5.0
20 4.5 ug/L 10/18/17 20:45 1Acrylonitrile<20
0.50 0.15 ug/L 10/18/17 20:45 1Benzene<0.50
1.0 0.43 ug/L 10/18/17 20:45 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/18/17 20:45 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/18/17 20:45 1Bromoform<1.0
2.0 0.80 ug/L 10/18/17 20:45 1Bromomethane<2.0
2.0 0.45 ug/L 10/18/17 20:45 1Carbon disulfide <2.0
1.0 0.38 ug/L 10/18/17 20:45 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/18/17 20:45 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/18/17 20:45 1Chloroethane<1.0
2.0 0.37 ug/L 10/18/17 20:45 1Chloroform<2.0
1.0 0.32 ug/L 10/18/17 20:45 1Chloromethane<1.0
1.0 0.41 ug/L 10/18/17 20:45 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/18/17 20:45 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/18/17 20:45 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/18/17 20:45 1Dibromomethane<1.0
0.50 0.18 ug/L 10/18/17 20:45 1Ethylbenzene<0.50
2.5 0.66 ug/L 10/18/17 20:45 1Iodomethane<2.5
5.0 1.6 ug/L 10/18/17 20:45 1Methylene Chloride <5.0
1.0 0.39 ug/L 10/18/17 20:45 1Styrene<1.0
1.0 0.37 ug/L 10/18/17 20:45 1Tetrachloroethene<1.0
10 1.9 ug/L 10/18/17 20:45 1Tetrahydrofuran<10
0.50 0.15 ug/L 10/18/17 20:45 1Toluene<0.50
1.0 0.35 ug/L 10/18/17 20:45 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/18/17 20:45 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/18/17 20:45 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/18/17 20:45 1Trichloroethene<0.50
1.0 0.43 ug/L 10/18/17 20:45 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/18/17 20:45 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/18/17 20:45 1Vinyl chloride <0.50
1.0 0.22 ug/L 10/18/17 20:45 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-11Client Sample ID: MW-8D NMLF
Matrix: WaterDate Collected: 10/11/17 10:10
Date Received: 10/12/17 10:00
1,2-Dichloroethane-d4 (Surr)108 75-126 10/18/17 20:45 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)100 10/18/17 20:45 172-124
Dibromofluoromethane 101 10/18/17 20:45 175-120
Toluene-d8 (Surr)93 10/18/17 20:45 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 10/13/17 11:30 10/16/17 12:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 10/13/17 11:30 10/16/17 12:11 1Arsenic0.15 J
2.5 0.37 ug/L 10/13/17 11:30 10/16/17 12:11 1Barium110
1.0 0.43 ug/L 10/13/17 11:30 10/16/17 23:23 1Beryllium<1.0
0.50 0.15 ug/L 10/13/17 11:30 10/16/17 12:11 1Cadmium<0.50
5.0 2.3 ug/L 10/13/17 11:30 10/16/17 12:11 1Chromium13
1.0 0.27 ug/L 10/13/17 11:30 10/16/17 23:23 1Cobalt3.3
2.0 0.63 ug/L 10/13/17 11:30 10/16/17 12:11 1Copper7.9
100 38 ug/L 10/13/17 11:30 10/16/17 23:23 1Iron4300
0.50 0.16 ug/L 10/13/17 11:30 10/16/17 12:11 1Lead0.74
2.5 1.1 ug/L 10/13/17 11:30 10/16/17 23:23 1Manganese260
2.0 0.92 ug/L 10/13/17 11:30 10/16/17 23:23 1Nickel12
2.5 1.1 ug/L 10/13/17 11:30 10/16/17 12:11 1Selenium<2.5
0.50 0.078 ug/L 10/13/17 11:30 10/16/17 12:11 1Silver<0.50
2.0 0.65 ug/L 10/13/17 11:30 10/16/17 12:11 1Thallium<2.0
5.0 2.0 ug/L 10/13/17 11:30 10/16/17 23:23 1Vanadium11
20 8.1 ug/L 10/13/17 11:30 10/16/17 12:11 1Zinc16J
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 10/18/17 15:35 10/19/17 11:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chloride 82 5.0 4.3 mg/L 10/28/17 16:30 25
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.40 0.19 mg/L 10/28/17 16:17 2Sulfate15
5.0 3.7 mg/L 10/24/17 16:17 1Alkalinity400
10 4.3 mg/L 10/16/17 04:25 1Total Dissolved Solids 570
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-12Client Sample ID: MW-10D NMLF
Matrix: WaterDate Collected: 10/11/17 11:25
Date Received: 10/12/17 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/16/17 22:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/16/17 22:51 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/16/17 22:51 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/16/17 22:51 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/16/17 22:51 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/16/17 22:51 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 10/16/17 22:51 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 10/16/17 22:51 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/16/17 22:51 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/16/17 22:51 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/16/17 22:51 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/16/17 22:51 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 10/16/17 22:51 11,4-Dichlorobenzene 1.8
5.0 2.1 ug/L 10/16/17 22:51 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 10/16/17 22:51 12-Hexanone <5.0
5.0 2.2 ug/L 10/16/17 22:51 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/16/17 22:51 1Acetone<5.0
20 4.5 ug/L 10/16/17 22:51 1Acrylonitrile<20
0.50 0.15 ug/L 10/16/17 22:51 1Benzene3.2
1.0 0.43 ug/L 10/16/17 22:51 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/16/17 22:51 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/16/17 22:51 1Bromoform<1.0
2.0 0.80 ug/L 10/16/17 22:51 1Bromomethane<2.0
2.0 0.45 ug/L 10/16/17 22:51 1Carbon disulfide <2.0
1.0 0.38 ug/L 10/16/17 22:51 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/16/17 22:51 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/16/17 22:51 1Chloroethane<1.0
2.0 0.37 ug/L 10/16/17 22:51 1Chloroform<2.0
1.0 0.32 ug/L 10/16/17 22:51 1Chloromethane<1.0
1.0 0.41 ug/L 10/16/17 22:51 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/16/17 22:51 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/16/17 22:51 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/16/17 22:51 1Dibromomethane<1.0
0.50 0.18 ug/L 10/16/17 22:51 1Ethylbenzene<0.50
2.5 0.66 ug/L 10/16/17 22:51 1Iodomethane<2.5
5.0 1.6 ug/L 10/16/17 22:51 1Methylene Chloride 7.5 cn
1.0 0.39 ug/L 10/16/17 22:51 1Styrene<1.0
1.0 0.37 ug/L 10/16/17 22:51 1Tetrachloroethene<1.0
10 1.9 ug/L 10/16/17 22:51 1Tetrahydrofuran79
0.50 0.15 ug/L 10/16/17 22:51 1Toluene<0.50
1.0 0.35 ug/L 10/16/17 22:51 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/16/17 22:51 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/16/17 22:51 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/16/17 22:51 1Trichloroethene<0.50
1.0 0.43 ug/L 10/16/17 22:51 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/16/17 22:51 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/16/17 22:51 1Vinyl chloride <0.50
1.0 0.22 ug/L 10/16/17 22:51 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-12Client Sample ID: MW-10D NMLF
Matrix: WaterDate Collected: 10/11/17 11:25
Date Received: 10/12/17 10:00
1,2-Dichloroethane-d4 (Surr)103 75-126 10/16/17 22:51 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)95 10/16/17 22:51 172-124
Dibromofluoromethane 96 10/16/17 22:51 175-120
Toluene-d8 (Surr)95 10/16/17 22:51 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 10/13/17 11:30 10/16/17 12:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 10/13/17 11:30 10/16/17 12:15 1Arsenic1.6
2.5 0.37 ug/L 10/13/17 11:30 10/16/17 12:15 1Barium210
1.0 0.43 ug/L 10/13/17 11:30 10/16/17 23:28 1Beryllium<1.0
0.50 0.15 ug/L 10/13/17 11:30 10/16/17 12:15 1Cadmium3.1
5.0 2.3 ug/L 10/13/17 11:30 10/16/17 12:15 1Chromium6.6
1.0 0.27 ug/L 10/13/17 11:30 10/16/17 23:28 1Cobalt49
2.0 0.63 ug/L 10/13/17 11:30 10/16/17 12:15 1Copper1800
100 38 ug/L 10/13/17 11:30 10/16/17 23:28 1Iron2700
0.50 0.16 ug/L 10/13/17 11:30 10/16/17 12:15 1Lead2.9
50 22 ug/L 10/13/17 11:30 10/17/17 13:21 20Manganese17000
2.0 0.92 ug/L 10/13/17 11:30 10/16/17 23:28 1Nickel60
2.5 1.1 ug/L 10/13/17 11:30 10/16/17 12:15 1Selenium1.2 J
0.50 0.078 ug/L 10/13/17 11:30 10/16/17 12:15 1Silver0.12 J
2.0 0.65 ug/L 10/13/17 11:30 10/16/17 12:15 1Thallium<2.0
5.0 2.0 ug/L 10/13/17 11:30 10/16/17 23:28 1Vanadium20
20 8.1 ug/L 10/13/17 11:30 10/16/17 12:15 1Zinc45
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury 0.16 J 0.20 0.091 ug/L 10/18/17 15:35 10/19/17 11:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chloride 200 10 8.5 mg/L 10/28/17 16:42 50
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10 4.8 mg/L 10/28/17 16:42 50Sulfate140
5.0 3.7 mg/L 10/24/17 13:50 1Alkalinity1700
10 4.3 mg/L 10/16/17 04:31 1Total Dissolved Solids 2500
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-13Client Sample ID: MW-11 NMLF
Matrix: WaterDate Collected: 10/11/17 12:25
Date Received: 10/12/17 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 21:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/18/17 21:11 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/18/17 21:11 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/18/17 21:11 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/18/17 21:11 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/18/17 21:11 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 10/18/17 21:11 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 10/18/17 21:11 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/18/17 21:11 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/18/17 21:11 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/18/17 21:11 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/18/17 21:11 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 10/18/17 21:11 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 10/18/17 21:11 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 10/18/17 21:11 12-Hexanone <5.0
5.0 2.2 ug/L 10/18/17 21:11 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/18/17 21:11 1Acetone<5.0
20 4.5 ug/L 10/18/17 21:11 1Acrylonitrile<20
0.50 0.15 ug/L 10/18/17 21:11 1Benzene0.90
1.0 0.43 ug/L 10/18/17 21:11 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/18/17 21:11 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/18/17 21:11 1Bromoform<1.0
2.0 0.80 ug/L 10/18/17 21:11 1Bromomethane<2.0
2.0 0.45 ug/L 10/18/17 21:11 1Carbon disulfide <2.0
1.0 0.38 ug/L 10/18/17 21:11 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/18/17 21:11 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/18/17 21:11 1Chloroethane<1.0
2.0 0.37 ug/L 10/18/17 21:11 1Chloroform<2.0
1.0 0.32 ug/L 10/18/17 21:11 1Chloromethane<1.0
1.0 0.41 ug/L 10/18/17 21:11 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/18/17 21:11 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/18/17 21:11 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/18/17 21:11 1Dibromomethane<1.0
0.50 0.18 ug/L 10/18/17 21:11 1Ethylbenzene<0.50
2.5 0.66 ug/L 10/18/17 21:11 1Iodomethane<2.5
5.0 1.6 ug/L 10/18/17 21:11 1Methylene Chloride <5.0
1.0 0.39 ug/L 10/18/17 21:11 1Styrene<1.0
1.0 0.37 ug/L 10/18/17 21:11 1Tetrachloroethene<1.0
10 1.9 ug/L 10/18/17 21:11 1Tetrahydrofuran17
0.50 0.15 ug/L 10/18/17 21:11 1Toluene<0.50
1.0 0.35 ug/L 10/18/17 21:11 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/18/17 21:11 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/18/17 21:11 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/18/17 21:11 1Trichloroethene<0.50
1.0 0.43 ug/L 10/18/17 21:11 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/18/17 21:11 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/18/17 21:11 1Vinyl chloride <0.50
1.0 0.22 ug/L 10/18/17 21:11 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-13Client Sample ID: MW-11 NMLF
Matrix: WaterDate Collected: 10/11/17 12:25
Date Received: 10/12/17 10:00
1,2-Dichloroethane-d4 (Surr)105 75-126 10/18/17 21:11 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)100 10/18/17 21:11 172-124
Dibromofluoromethane 96 10/18/17 21:11 175-120
Toluene-d8 (Surr)97 10/18/17 21:11 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 10/13/17 11:30 10/16/17 12:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 10/13/17 11:30 10/16/17 12:19 1Arsenic0.52 J
2.5 0.37 ug/L 10/13/17 11:30 10/16/17 12:19 1Barium270
1.0 0.43 ug/L 10/13/17 11:30 10/16/17 23:32 1Beryllium<1.0
0.50 0.15 ug/L 10/13/17 11:30 10/16/17 12:19 1Cadmium0.45 J
5.0 2.3 ug/L 10/13/17 11:30 10/16/17 12:19 1Chromium51
1.0 0.27 ug/L 10/13/17 11:30 10/16/17 23:32 1Cobalt3.1
2.0 0.63 ug/L 10/13/17 11:30 10/16/17 12:19 1Copper36
100 38 ug/L 10/13/17 11:30 10/16/17 23:32 1Iron750
0.50 0.16 ug/L 10/13/17 11:30 10/16/17 12:19 1Lead0.76
2.5 1.1 ug/L 10/13/17 11:30 10/16/17 23:32 1Manganese2500
2.0 0.92 ug/L 10/13/17 11:30 10/16/17 23:32 1Nickel53
2.5 1.1 ug/L 10/13/17 11:30 10/16/17 12:19 1Selenium<2.5
0.50 0.078 ug/L 10/13/17 11:30 10/16/17 12:19 1Silver<0.50
2.0 0.65 ug/L 10/13/17 11:30 10/16/17 12:19 1Thallium<2.0
5.0 2.0 ug/L 10/13/17 11:30 10/16/17 23:32 1Vanadium7.0
20 8.1 ug/L 10/13/17 11:30 10/16/17 12:19 1Zinc51
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 10/18/17 15:35 10/19/17 11:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chloride 51 2.0 1.7 mg/L 10/28/17 17:21 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.0 2.4 mg/L 10/28/17 17:33 25Sulfate96
5.0 3.7 mg/L 10/24/17 16:30 1Alkalinity1100
10 4.3 mg/L 10/16/17 04:33 1Total Dissolved Solids 1400
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-14Client Sample ID: MW-10 Infill
Matrix: WaterDate Collected: 10/11/17 13:45
Date Received: 10/12/17 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 21:37 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 10/18/17 21:37 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 10/18/17 21:37 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 10/18/17 21:37 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 10/18/17 21:37 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 10/18/17 21:37 11,1-Dichloroethene <1.0
1.0 0.30 ug/L 10/18/17 21:37 11,1-Dichloropropene <1.0
1.0 0.41 ug/L 10/18/17 21:37 11,2,3-Trichloropropane <1.0
1.0 0.34 ug/L 10/18/17 21:37 11,2,4-Trichlorobenzene <1.0
5.0 2.0 ug/L 10/18/17 21:37 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 10/18/17 21:37 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 10/18/17 21:37 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 10/18/17 21:37 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 10/18/17 21:37 11,2-Dichloropropane <1.0
1.0 0.40 ug/L 10/18/17 21:37 11,3-Dichlorobenzene <1.0
1.0 0.36 ug/L 10/18/17 21:37 11,3-Dichloropropane <1.0
1.0 0.36 ug/L 10/18/17 21:37 11,4-Dichlorobenzene <1.0
1.0 0.44 ug/L 10/18/17 21:37 12,2-Dichloropropane <1.0
5.0 2.1 ug/L 10/18/17 21:37 12-Butanone (MEK)<5.0
1.0 0.23 ug/L 10/18/17 21:37 12-Chloro-1,3-butadiene <1.0
5.0 1.6 ug/L 10/18/17 21:37 12-Hexanone <5.0
2.5 0.86 ug/L 10/18/17 21:37 13-Chloropropene <2.5
5.0 2.2 ug/L 10/18/17 21:37 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 10/18/17 21:37 1Acetone15cn
10 4.2 ug/L 10/18/17 21:37 1Acetonitrile<10
100 23 ug/L 10/18/17 21:37 1Acrolein<100
20 4.5 ug/L 10/18/17 21:37 1Acrylonitrile<20
0.50 0.15 ug/L 10/18/17 21:37 1Benzene<0.50
1.0 0.43 ug/L 10/18/17 21:37 1Bromochloromethane<1.0
1.0 0.37 ug/L 10/18/17 21:37 1Bromodichloromethane<1.0
1.0 0.48 ug/L 10/18/17 21:37 1Bromoform<1.0
2.0 0.80 ug/L 10/18/17 21:37 1Bromomethane<2.0
2.0 0.45 ug/L 10/18/17 21:37 1Carbon disulfide <2.0
1.0 0.38 ug/L 10/18/17 21:37 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 10/18/17 21:37 1Chlorobenzene<1.0
1.0 0.51 ug/L 10/18/17 21:37 1Chloroethane<1.0
2.0 0.37 ug/L 10/18/17 21:37 1Chloroform<2.0
1.0 0.32 ug/L 10/18/17 21:37 1Chloromethane<1.0
1.0 0.41 ug/L 10/18/17 21:37 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 10/18/17 21:37 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 10/18/17 21:37 1Dibromochloromethane<1.0
1.0 0.27 ug/L 10/18/17 21:37 1Dibromomethane<1.0
2.0 0.67 ug/L 10/18/17 21:37 1Dichlorodifluoromethane<2.0
2.5 0.53 ug/L 10/18/17 21:37 1Ethyl methacrylate <2.5
0.50 0.18 ug/L 10/18/17 21:37 1Ethylbenzene<0.50
1.0 0.45 ug/L 10/18/17 21:37 1Hexachlorobutadiene<1.0
2.5 0.66 ug/L 10/18/17 21:37 1Iodomethane<2.5
100 36 ug/L 10/18/17 21:37 1Isobutyl alcohol <100
10 2.5 ug/L 10/18/17 21:37 1Methacrylonitrile<10
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Client Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Lab Sample ID: 500-135505-14Client Sample ID: MW-10 Infill
Matrix: WaterDate Collected: 10/11/17 13:45
Date Received: 10/12/17 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
Methyl methacrylate <2.5 2.5 0.55 ug/L 10/18/17 21:37 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.0 1.6 ug/L 10/18/17 21:37 1Methylene Chloride <5.0
10 4.8 ug/L 10/18/17 21:37 1Propionitrile<10
1.0 0.39 ug/L 10/18/17 21:37 1Styrene<1.0
1.0 0.37 ug/L 10/18/17 21:37 1Tetrachloroethene<1.0
10 1.9 ug/L 10/18/17 21:37 1Tetrahydrofuran5.2 J
0.50 0.15 ug/L 10/18/17 21:37 1Toluene<0.50
1.0 0.35 ug/L 10/18/17 21:37 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 10/18/17 21:37 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 10/18/17 21:37 1trans-1,4-Dichloro-2-butene <5.0
0.50 0.16 ug/L 10/18/17 21:37 1Trichloroethene<0.50
1.0 0.43 ug/L 10/18/17 21:37 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 10/18/17 21:37 1Vinyl acetate <2.0
0.50 0.20 ug/L 10/18/17 21:37 1Vinyl chloride <0.50
1.0 0.22 ug/L 10/18/17 21:37 1Xylenes, Total <1.0
1,2-Dichloroethane-d4 (Surr)107 75-126 10/18/17 21:37 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)99 10/18/17 21:37 172-124
Dibromofluoromethane 98 10/18/17 21:37 175-120
Toluene-d8 (Surr)96 10/18/17 21:37 175-120
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Definitions/Glossary
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Qualifiers
GC/MS VOA
Qualifier Description
cn Refer to Case Narrative for further detail
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
GC/MS Semi VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
X Surrogate is outside control limits
GC Semi VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
Metals
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
B Compound was found in the blank and sample.
V Serial Dilution exceeds the control limits
F5 Duplicate RPD exceeds limit, and one or both sample results are less than 5 times RL. The data are considered valid because the
absolute difference is less than the RL.
^ICV,CCV,ICB,CCB, ISA, ISB, CRI, CRA, DLCK or MRL standard: Instrument related QC is outside acceptance limits.
General Chemistry
Qualifier Description
4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not
applicable.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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QC Association Summary
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
GC/MS VOA
Analysis Batch: 405489
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B500-135505-12 MW-10D NMLF Total/NA
Water 8260BMB 500-405489/7 Method Blank Total/NA
Water 8260BLCS 500-405489/5 Lab Control Sample Total/NA
Analysis Batch: 405855
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B500-135505-1 MW-14 Infill Total/NA
Water 8260B500-135505-2 MW-8 Infill Total/NA
Water 8260B500-135505-3 Duplicate 2 Total/NA
Water 8260B500-135505-4 MW-12 Infill Total/NA
Water 8260B500-135505-5 MW-12D Infill Total/NA
Water 8260B500-135505-6 Infill Duplicate 1 Total/NA
Water 8260B500-135505-7 MW-7D Infill Total/NA
Water 8260B500-135505-8 MW-1 Infill Total/NA
Water 8260B500-135505-9 TB Total/NA
Water 8260B500-135505-10 MW-8 NMLF Total/NA
Water 8260B500-135505-11 MW-8D NMLF Total/NA
Water 8260B500-135505-13 MW-11 NMLF Total/NA
Water 8260B500-135505-14 MW-10 Infill Total/NA
Water 8260BMB 500-405855/7 Method Blank Total/NA
Water 8260BLCS 500-405855/5 Lab Control Sample Total/NA
Water 8260B500-135505-14 MS MW-10 Infill Total/NA
Water 8260B500-135505-14 MSD MW-10 Infill Total/NA
GC/MS Semi VOA
Prep Batch: 405441
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510C500-135505-1 MW-14 Infill Total/NA
Water 3510C500-135505-2 MW-8 Infill Total/NA
Water 3510C500-135505-4 MW-12 Infill Total/NA
Water 3510C500-135505-5 MW-12D Infill Total/NA
Water 3510C500-135505-7 MW-7D Infill Total/NA
Water 3510C500-135505-8 MW-1 Infill Total/NA
Water 3510CMB 500-405441/1-A Method Blank Total/NA
Water 3510CLCS 500-405441/2-A Lab Control Sample Total/NA
Water 3510CLCSD 500-405441/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 405562
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8270D 405441MB 500-405441/1-A Method Blank Total/NA
Water 8270D 405441LCS 500-405441/2-A Lab Control Sample Total/NA
Water 8270D 405441LCSD 500-405441/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 405883
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8270D 405441500-135505-1 MW-14 Infill Total/NA
Water 8270D 405441500-135505-2 MW-8 Infill Total/NA
Water 8270D 405441500-135505-4 MW-12 Infill Total/NA
Water 8270D 405441500-135505-5 MW-12D Infill Total/NA
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QC Association Summary
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
GC/MS Semi VOA (Continued)
Analysis Batch: 405883 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8270D 405441500-135505-7 MW-7D Infill Total/NA
Analysis Batch: 406153
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8270D 405441500-135505-8 MW-1 Infill Total/NA
GC Semi VOA
Prep Batch: 405080
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8151A500-135505-1 MW-14 Infill Total/NA
Water 8151A500-135505-2 MW-8 Infill Total/NA
Water 8151A500-135505-4 MW-12 Infill Total/NA
Water 8151A500-135505-5 MW-12D Infill Total/NA
Water 8151A500-135505-7 MW-7D Infill Total/NA
Water 8151A500-135505-8 MW-1 Infill Total/NA
Water 8151AMB 500-405080/1-A Method Blank Total/NA
Water 8151ALCS 500-405080/2-A Lab Control Sample Total/NA
Water 8151ALCSD 500-405080/3-A Lab Control Sample Dup Total/NA
Prep Batch: 405223
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510C500-135505-1 MW-14 Infill Total/NA
Water 3510C500-135505-2 MW-8 Infill Total/NA
Water 3510C500-135505-4 MW-12 Infill Total/NA
Water 3510C500-135505-5 MW-12D Infill Total/NA
Water 3510C500-135505-7 MW-7D Infill Total/NA
Water 3510C500-135505-8 MW-1 Infill Total/NA
Water 3510CMB 500-405223/1-A Method Blank Total/NA
Water 3510CLCS 500-405223/2-A Lab Control Sample Total/NA
Water 3510CLCS 500-405223/4-A Lab Control Sample Total/NA
Water 3510CLCSD 500-405223/3-A Lab Control Sample Dup Total/NA
Water 3510CLCSD 500-405223/5-A Lab Control Sample Dup Total/NA
Analysis Batch: 405510
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8151A 405080500-135505-1 MW-14 Infill Total/NA
Water 8151A 405080500-135505-2 MW-8 Infill Total/NA
Water 8151A 405080500-135505-4 MW-12 Infill Total/NA
Water 8151A 405080500-135505-5 MW-12D Infill Total/NA
Water 8151A 405080500-135505-7 MW-7D Infill Total/NA
Water 8151A 405080MB 500-405080/1-A Method Blank Total/NA
Water 8151A 405080LCS 500-405080/2-A Lab Control Sample Total/NA
Water 8151A 405080LCSD 500-405080/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 405522
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8081B 405223500-135505-1 MW-14 Infill Total/NA
Water 8081B 405223500-135505-2 MW-8 Infill Total/NA
Water 8081B 405223500-135505-4 MW-12 Infill Total/NA
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QC Association Summary
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
GC Semi VOA (Continued)
Analysis Batch: 405522 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8081B 405223500-135505-5 MW-12D Infill Total/NA
Water 8081B 405223MB 500-405223/1-A Method Blank Total/NA
Water 8081B 405223LCS 500-405223/2-A Lab Control Sample Total/NA
Water 8081B 405223LCSD 500-405223/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 405636
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8151A 405080500-135505-8 MW-1 Infill Total/NA
Analysis Batch: 405675
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8081B 405223500-135505-7 MW-7D Infill Total/NA
Water 8081B 405223500-135505-8 MW-1 Infill Total/NA
Analysis Batch: 406209
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8082A 405223500-135505-1 MW-14 Infill Total/NA
Water 8082A 405223500-135505-2 MW-8 Infill Total/NA
Water 8082A 405223500-135505-4 MW-12 Infill Total/NA
Water 8082A 405223500-135505-5 MW-12D Infill Total/NA
Water 8082A 405223500-135505-7 MW-7D Infill Total/NA
Water 8082A 405223500-135505-8 MW-1 Infill Total/NA
Water 8082A 405223MB 500-405223/1-A Method Blank Total/NA
Water 8082A 405223LCS 500-405223/4-A Lab Control Sample Total/NA
Water 8082A 405223LCSD 500-405223/5-A Lab Control Sample Dup Total/NA
Metals
Prep Batch: 405222
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 200.8500-135505-1 MW-14 Infill Total/NA
Water 200.8500-135505-2 MW-8 Infill Total/NA
Water 200.8500-135505-4 MW-12 Infill Total/NA
Water 200.8500-135505-5 MW-12D Infill Total/NA
Water 200.8500-135505-7 MW-7D Infill Total/NA
Water 200.8500-135505-8 MW-1 Infill Total/NA
Water 200.8500-135505-10 MW-8 NMLF Total/NA
Water 200.8MB 500-405222/1-A Method Blank Total/NA
Water 200.8LCS 500-405222/2-A Lab Control Sample Total/NA
Water 200.8500-135505-4 MS MW-12 Infill Total/NA
Water 200.8500-135505-4 DU MW-12 Infill Total/NA
Prep Batch: 405247
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 200.8500-135505-11 MW-8D NMLF Total/NA
Water 200.8500-135505-12 MW-10D NMLF Total/NA
Water 200.8500-135505-13 MW-11 NMLF Total/NA
Water 200.8MB 500-405247/1-A Method Blank Total/NA
Water 200.8LCS 500-405247/2-A Lab Control Sample Total/NA
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QC Association Summary
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Metals (Continued)
Analysis Batch: 405553
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 200.8 405247500-135505-11 MW-8D NMLF Total/NA
Water 200.8 405247500-135505-12 MW-10D NMLF Total/NA
Water 200.8 405247500-135505-13 MW-11 NMLF Total/NA
Water 200.8 405247MB 500-405247/1-A Method Blank Total/NA
Water 200.8 405247LCS 500-405247/2-A Lab Control Sample Total/NA
Analysis Batch: 405643
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 200.8 405247500-135505-11 MW-8D NMLF Total/NA
Water 200.8 405247500-135505-12 MW-10D NMLF Total/NA
Water 200.8 405247500-135505-13 MW-11 NMLF Total/NA
Water 200.8 405247MB 500-405247/1-A Method Blank Total/NA
Water 200.8 405247LCS 500-405247/2-A Lab Control Sample Total/NA
Analysis Batch: 405644
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 200.8 405222500-135505-1 MW-14 Infill Total/NA
Water 200.8 405222500-135505-2 MW-8 Infill Total/NA
Water 200.8 405222500-135505-4 MW-12 Infill Total/NA
Water 200.8 405222500-135505-5 MW-12D Infill Total/NA
Water 200.8 405222500-135505-7 MW-7D Infill Total/NA
Water 200.8 405222500-135505-8 MW-1 Infill Total/NA
Water 200.8 405222500-135505-10 MW-8 NMLF Total/NA
Water 200.8 405222MB 500-405222/1-A Method Blank Total/NA
Water 200.8 405222LCS 500-405222/2-A Lab Control Sample Total/NA
Water 200.8 405222500-135505-4 MS MW-12 Infill Total/NA
Water 200.8 405222500-135505-4 DU MW-12 Infill Total/NA
Analysis Batch: 405834
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 200.8 405222500-135505-1 MW-14 Infill Total/NA
Water 200.8 405222500-135505-2 MW-8 Infill Total/NA
Water 200.8 405222500-135505-4 MW-12 Infill Total/NA
Water 200.8 405222500-135505-5 MW-12D Infill Total/NA
Water 200.8 405222500-135505-7 MW-7D Infill Total/NA
Water 200.8 405222500-135505-8 MW-1 Infill Total/NA
Water 200.8 405222500-135505-10 MW-8 NMLF Total/NA
Water 200.8 405247500-135505-12 MW-10D NMLF Total/NA
Water 200.8 405222MB 500-405222/1-A Method Blank Total/NA
Water 200.8 405222LCS 500-405222/2-A Lab Control Sample Total/NA
Water 200.8 405222500-135505-4 MS MW-12 Infill Total/NA
Water 200.8 405222500-135505-4 DU MW-12 Infill Total/NA
Prep Batch: 405904
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 245.1500-135505-1 MW-14 Infill Total/NA
Water 245.1500-135505-2 MW-8 Infill Total/NA
Water 245.1500-135505-4 MW-12 Infill Total/NA
Water 245.1500-135505-5 MW-12D Infill Total/NA
Water 245.1500-135505-7 MW-7D Infill Total/NA
Water 245.1500-135505-8 MW-1 Infill Total/NA
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QC Association Summary
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Metals (Continued)
Prep Batch: 405904 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 245.1500-135505-10 MW-8 NMLF Total/NA
Water 245.1500-135505-11 MW-8D NMLF Total/NA
Water 245.1500-135505-12 MW-10D NMLF Total/NA
Water 245.1500-135505-13 MW-11 NMLF Total/NA
Water 245.1MB 500-405904/12-A Method Blank Total/NA
Water 245.1LCS 500-405904/13-A Lab Control Sample Total/NA
Water 245.1500-135505-1 MS MW-14 Infill Total/NA
Water 245.1500-135505-1 DU MW-14 Infill Total/NA
Analysis Batch: 406044
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 245.1 405904500-135505-1 MW-14 Infill Total/NA
Water 245.1 405904500-135505-2 MW-8 Infill Total/NA
Water 245.1 405904500-135505-4 MW-12 Infill Total/NA
Water 245.1 405904500-135505-5 MW-12D Infill Total/NA
Water 245.1 405904500-135505-7 MW-7D Infill Total/NA
Water 245.1 405904500-135505-8 MW-1 Infill Total/NA
Water 245.1 405904500-135505-10 MW-8 NMLF Total/NA
Water 245.1 405904500-135505-11 MW-8D NMLF Total/NA
Water 245.1 405904500-135505-12 MW-10D NMLF Total/NA
Water 245.1 405904500-135505-13 MW-11 NMLF Total/NA
Water 245.1 405904MB 500-405904/12-A Method Blank Total/NA
Water 245.1 405904LCS 500-405904/13-A Lab Control Sample Total/NA
Water 245.1 405904500-135505-1 MS MW-14 Infill Total/NA
Water 245.1 405904500-135505-1 DU MW-14 Infill Total/NA
General Chemistry
Analysis Batch: 405177
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 2540C500-135505-1 MW-14 Infill Total/NA
Water SM 2540C500-135505-2 MW-8 Infill Total/NA
Water SM 2540C500-135505-4 MW-12 Infill Total/NA
Water SM 2540C500-135505-5 MW-12D Infill Total/NA
Water SM 2540C500-135505-7 MW-7D Infill Total/NA
Water SM 2540C500-135505-8 MW-1 Infill Total/NA
Water SM 2540C500-135505-10 MW-8 NMLF Total/NA
Water SM 2540CMB 500-405177/1 Method Blank Total/NA
Water SM 2540CLCS 500-405177/2 Lab Control Sample Total/NA
Analysis Batch: 405423
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 2540C500-135505-11 MW-8D NMLF Total/NA
Water SM 2540C500-135505-12 MW-10D NMLF Total/NA
Water SM 2540C500-135505-13 MW-11 NMLF Total/NA
Water SM 2540CMB 500-405423/1 Method Blank Total/NA
Water SM 2540CLCS 500-405423/2 Lab Control Sample Total/NA
Water SM 2540C500-135505-11 DU MW-8D NMLF Total/NA
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QC Association Summary
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
General Chemistry (Continued)
Prep Batch: 406103
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 9010B500-135505-1 MW-14 Infill Total/NA
Water 9010BMB 500-406103/1-A Method Blank Total/NA
Water 9010BLCS 500-406103/2-A Lab Control Sample Total/NA
Analysis Batch: 406172
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 2320B500-135505-1 MW-14 Infill Total/NA
Water SM 2320B500-135505-2 MW-8 Infill Total/NA
Water SM 2320B500-135505-4 MW-12 Infill Total/NA
Water SM 2320B500-135505-5 MW-12D Infill Total/NA
Water SM 2320B500-135505-7 MW-7D Infill Total/NA
Water SM 2320B500-135505-8 MW-1 Infill Total/NA
Water SM 2320B500-135505-10 MW-8 NMLF Total/NA
Water SM 2320BMB 500-406172/28 Method Blank Total/NA
Water SM 2320BLCS 500-406172/29 Lab Control Sample Total/NA
Water SM 2320B500-135505-1 DU MW-14 Infill Total/NA
Analysis Batch: 406574
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 9014 406103500-135505-1 MW-14 Infill Total/NA
Water 9014 406103MB 500-406103/1-A Method Blank Total/NA
Water 9014 406103LCS 500-406103/2-A Lab Control Sample Total/NA
Prep Batch: 406665
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 9010B500-135505-2 MW-8 Infill Total/NA
Water 9010B500-135505-4 MW-12 Infill Total/NA
Water 9010B500-135505-5 MW-12D Infill Total/NA
Water 9010B500-135505-7 MW-7D Infill Total/NA
Water 9010B500-135505-8 MW-1 Infill Total/NA
Water 9010BMB 500-406665/1-A Method Blank Total/NA
Water 9010BLCS 500-406665/2-A Lab Control Sample Total/NA
Analysis Batch: 406763
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 9014 406665500-135505-2 MW-8 Infill Total/NA
Water 9014 406665500-135505-4 MW-12 Infill Total/NA
Water 9014 406665500-135505-5 MW-12D Infill Total/NA
Water 9014 406665500-135505-7 MW-7D Infill Total/NA
Water 9014 406665500-135505-8 MW-1 Infill Total/NA
Water 9014 406665MB 500-406665/1-A Method Blank Total/NA
Water 9014 406665LCS 500-406665/2-A Lab Control Sample Total/NA
Analysis Batch: 406877
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 2320B500-135505-11 MW-8D NMLF Total/NA
Water SM 2320B500-135505-12 MW-10D NMLF Total/NA
Water SM 2320B500-135505-13 MW-11 NMLF Total/NA
Water SM 2320BMB 500-406877/28 Method Blank Total/NA
Water SM 2320BMB 500-406877/3 Method Blank Total/NA
Water SM 2320BLCS 500-406877/29 Lab Control Sample Total/NA
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QC Association Summary
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
General Chemistry (Continued)
Analysis Batch: 406877 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 2320BLCS 500-406877/4 Lab Control Sample Total/NA
Analysis Batch: 407493
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 9056A500-135505-1 MW-14 Infill Total/NA
Water 9056A500-135505-2 MW-8 Infill Total/NA
Water 9056A500-135505-2 MW-8 Infill Total/NA
Water 9056A500-135505-4 MW-12 Infill Total/NA
Water 9056A500-135505-5 MW-12D Infill Total/NA
Water 9056A500-135505-7 MW-7D Infill Total/NA
Water 9056A500-135505-8 MW-1 Infill Total/NA
Water 9056A500-135505-10 MW-8 NMLF Total/NA
Water 9056A500-135505-11 MW-8D NMLF Total/NA
Water 9056A500-135505-11 MW-8D NMLF Total/NA
Water 9056A500-135505-12 MW-10D NMLF Total/NA
Water 9056A500-135505-13 MW-11 NMLF Total/NA
Water 9056A500-135505-13 MW-11 NMLF Total/NA
Water 9056AMB 500-407493/23 Method Blank Total/NA
Water 9056ALCS 500-407493/34 Lab Control Sample Total/NA
Water 9056A500-135505-8 MS MW-1 Infill Total/NA
Water 9056A500-135505-8 MSD MW-1 Infill Total/NA
Analysis Batch: 407616
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 9056A500-135505-1 MW-14 Infill Total/NA
Water 9056AMB 500-407616/23 Method Blank Total/NA
Water 9056ALCS 500-407616/29 Lab Control Sample Total/NA
Water 9056A500-135505-1 MS MW-14 Infill Total/NA
Water 9056A500-135505-1 MSD MW-14 Infill Total/NA
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Surrogate Summary
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (75-126)(72-124)(75-120)(75-120)
12DCE BFB DBFM TOL
107 96 99 94500-135505-1
Percent Surrogate Recovery (Acceptance Limits)
MW-14 Infill
106 98 95 96500-135505-2 MW-8 Infill
107 98 100 94500-135505-3 Duplicate 2
106 97 99 93500-135505-4 MW-12 Infill
106 98 96 97500-135505-5 MW-12D Infill
107 96 100 94500-135505-6 Infill Duplicate 1
106 97 97 95500-135505-7 MW-7D Infill
106 97 98 95500-135505-8 MW-1 Infill
109 99 101 94500-135505-9 TB
107 100 99 94500-135505-10 MW-8 NMLF
108 100 101 93500-135505-11 MW-8D NMLF
103 95 96 95500-135505-12 MW-10D NMLF
105 100 96 97500-135505-13 MW-11 NMLF
107 99 98 96500-135505-14 MW-10 Infill
103 88 95 95500-135505-14 MS MW-10 Infill
104 91 96 96500-135505-14 MSD MW-10 Infill
102 85 99 93LCS 500-405489/5 Lab Control Sample
102 86 97 96LCS 500-405855/5 Lab Control Sample
98 97 95 98MB 500-405489/7 Method Blank
105 98 96 95MB 500-405855/7 Method Blank
Surrogate Legend
12DCE = 1,2-Dichloroethane-d4 (Surr)
BFB = 4-Bromofluorobenzene (Surr)
DBFM = Dibromofluoromethane
TOL = Toluene-d8 (Surr)
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (34-110)(27-110)(36-120)(20-100)(40-145)(40-145)
FBP 2FP NBZ PHL TPH TBP
79 57 77 35 96 114500-135505-1
Percent Surrogate Recovery (Acceptance Limits)
MW-14 Infill
60 42 56 9324 102500-135505-2 MW-8 Infill
72 48 68 9333 114500-135505-4 MW-12 Infill
80 44 78 10640 110500-135505-5 MW-12D Infill
85 56 82 9248 121500-135505-7 MW-7D Infill
77 27 96 9626 39 X500-135505-8 MW-1 Infill
73 60 75 9646 105LCS 500-405441/2-A Lab Control Sample
73 62 76 9748 108LCSD 500-405441/3-A Lab Control Sample Dup
74 61 75 9935 103MB 500-405441/1-A Method Blank
Surrogate Legend
FBP = 2-Fluorobiphenyl
2FP = 2-Fluorophenol
NBZ = Nitrobenzene-d5
PHL = Phenol-d5
TPH = Terphenyl-d14
TBP = 2,4,6-Tribromophenol
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Surrogate Summary
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 8081B - Organochlorine Pesticides (GC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-130)(30-120)
DCB2 TCX2
58 67500-135505-1
Percent Surrogate Recovery (Acceptance Limits)
MW-14 Infill
76 76500-135505-2 MW-8 Infill
93 119500-135505-4 MW-12 Infill
97 86500-135505-5 MW-12D Infill
96 82500-135505-7 MW-7D Infill
45 69500-135505-8 MW-1 Infill
87 84LCS 500-405223/2-A Lab Control Sample
82 83LCSD 500-405223/3-A Lab Control Sample Dup
81 81MB 500-405223/1-A Method Blank
Surrogate Legend
DCB = DCB Decachlorobiphenyl
TCX = Tetrachloro-m-xylene
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (30-120)(30-140)
TCX1 DCB1
65 69500-135505-1
Percent Surrogate Recovery (Acceptance Limits)
MW-14 Infill
82 98500-135505-2 MW-8 Infill
70 97500-135505-4 MW-12 Infill
85 95500-135505-5 MW-12D Infill
92 97500-135505-7 MW-7D Infill
73 53500-135505-8 MW-1 Infill
78 100LCS 500-405223/4-A Lab Control Sample
72 97LCSD 500-405223/5-A Lab Control Sample Dup
80 104MB 500-405223/1-A Method Blank
Surrogate Legend
TCX = Tetrachloro-m-xylene
DCB = DCB Decachlorobiphenyl
Method: 8151A - Herbicides (GC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (25-130)
DCPA2
57500-135505-1
Percent Surrogate Recovery (Acceptance Limits)
MW-14 Infill
61500-135505-2 MW-8 Infill
61500-135505-4 MW-12 Infill
63500-135505-5 MW-12D Infill
59500-135505-7 MW-7D Infill
94500-135505-8 MW-1 Infill
49LCS 500-405080/2-A Lab Control Sample
56LCSD 500-405080/3-A Lab Control Sample Dup
45MB 500-405080/1-A Method Blank
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Surrogate Summary
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Surrogate Legend
DCPA = DCAA
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QC Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 500-405489/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405489
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/16/17 14:02 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<1.0 0.381.0 ug/L 10/16/17 14:02 11,1,1-Trichloroethane
<1.0 0.401.0 ug/L 10/16/17 14:02 11,1,2,2-Tetrachloroethane
<1.0 0.351.0 ug/L 10/16/17 14:02 11,1,2-Trichloroethane
<1.0 0.411.0 ug/L 10/16/17 14:02 11,1-Dichloroethane
<1.0 0.391.0 ug/L 10/16/17 14:02 11,1-Dichloroethene
<1.0 0.411.0 ug/L 10/16/17 14:02 11,2,3-Trichloropropane
<5.0 2.05.0 ug/L 10/16/17 14:02 11,2-Dibromo-3-Chloropropane
<1.0 0.391.0 ug/L 10/16/17 14:02 11,2-Dibromoethane
<1.0 0.331.0 ug/L 10/16/17 14:02 11,2-Dichlorobenzene
<1.0 0.391.0 ug/L 10/16/17 14:02 11,2-Dichloroethane
<1.0 0.431.0 ug/L 10/16/17 14:02 11,2-Dichloropropane
<1.0 0.361.0 ug/L 10/16/17 14:02 11,4-Dichlorobenzene
<5.0 2.15.0 ug/L 10/16/17 14:02 12-Butanone (MEK)
<5.0 1.65.0 ug/L 10/16/17 14:02 12-Hexanone
<5.0 2.25.0 ug/L 10/16/17 14:02 14-Methyl-2-pentanone (MIBK)
<5.0 1.75.0 ug/L 10/16/17 14:02 1Acetone
<20 4.520 ug/L 10/16/17 14:02 1Acrylonitrile
<0.50 0.150.50 ug/L 10/16/17 14:02 1Benzene
<1.0 0.431.0 ug/L 10/16/17 14:02 1Bromochloromethane
<1.0 0.371.0 ug/L 10/16/17 14:02 1Bromodichloromethane
<1.0 0.481.0 ug/L 10/16/17 14:02 1Bromoform
<2.0 0.802.0 ug/L 10/16/17 14:02 1Bromomethane
<2.0 0.452.0 ug/L 10/16/17 14:02 1Carbon disulfide
<1.0 0.381.0 ug/L 10/16/17 14:02 1Carbon tetrachloride
<1.0 0.391.0 ug/L 10/16/17 14:02 1Chlorobenzene
<1.0 0.511.0 ug/L 10/16/17 14:02 1Chloroethane
<2.0 0.372.0 ug/L 10/16/17 14:02 1Chloroform
<1.0 0.321.0 ug/L 10/16/17 14:02 1Chloromethane
<1.0 0.411.0 ug/L 10/16/17 14:02 1cis-1,2-Dichloroethene
<1.0 0.421.0 ug/L 10/16/17 14:02 1cis-1,3-Dichloropropene
<1.0 0.491.0 ug/L 10/16/17 14:02 1Dibromochloromethane
<1.0 0.271.0 ug/L 10/16/17 14:02 1Dibromomethane
<0.50 0.180.50 ug/L 10/16/17 14:02 1Ethylbenzene
<2.5 0.662.5 ug/L 10/16/17 14:02 1Iodomethane
<5.0 1.65.0 ug/L 10/16/17 14:02 1Methylene Chloride
<1.0 0.391.0 ug/L 10/16/17 14:02 1Styrene
<1.0 0.371.0 ug/L 10/16/17 14:02 1Tetrachloroethene
<10 1.910 ug/L 10/16/17 14:02 1Tetrahydrofuran
<0.50 0.150.50 ug/L 10/16/17 14:02 1Toluene
<1.0 0.351.0 ug/L 10/16/17 14:02 1trans-1,2-Dichloroethene
<1.0 0.361.0 ug/L 10/16/17 14:02 1trans-1,3-Dichloropropene
<5.0 1.25.0 ug/L 10/16/17 14:02 1trans-1,4-Dichloro-2-butene
<0.50 0.160.50 ug/L 10/16/17 14:02 1Trichloroethene
<1.0 0.431.0 ug/L 10/16/17 14:02 1Trichlorofluoromethane
<2.0 0.912.0 ug/L 10/16/17 14:02 1Vinyl acetate
<0.50 0.200.50 ug/L 10/16/17 14:02 1Vinyl chloride
<1.0 0.221.0 ug/L 10/16/17 14:02 1Xylenes, Total
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QC Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
1,2-Dichloroethane-d4 (Surr)98 75-126 10/16/17 14:02 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
97 10/16/17 14:02 14-Bromofluorobenzene (Surr)72-124
95 10/16/17 14:02 1Dibromofluoromethane75-120
98 10/16/17 14:02 1Toluene-d8 (Surr)75-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-405489/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405489
1,1,1,2-Tetrachloroethane 50.0 51.1 ug/L 102 70-125
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,1,1-Trichloroethane 50.0 56.4 ug/L 113 70-125
1,1,2,2-Tetrachloroethane 50.0 39.9 ug/L 80 67-127
1,1,2-Trichloroethane 50.0 44.2 ug/L 88 70-122
1,1-Dichloroethane 50.0 54.0 ug/L 108 70-125
1,1-Dichloroethene 50.0 51.5 ug/L 103 67-122
1,2,3-Trichloropropane 50.0 40.9 ug/L 82 50-133
1,2-Dibromo-3-Chloropropane 50.0 42.7 ug/L 85 56-123
1,2-Dibromoethane 50.0 44.9 ug/L 90 70-125
1,2-Dichlorobenzene 50.0 46.8 ug/L 94 70-125
1,2-Dichloroethane 50.0 55.0 ug/L 110 68-127
1,2-Dichloropropane 50.0 47.1 ug/L 94 67-130
1,4-Dichlorobenzene 50.0 47.2 ug/L 94 70-120
2-Butanone (MEK)50.0 43.5 ug/L 87 53-141
2-Hexanone 50.0 45.7 ug/L 91 56-135
4-Methyl-2-pentanone (MIBK)50.0 46.6 ug/L 93 56-133
Acetone 50.0 46.0 ug/L 92 40-143
Acrylonitrile 500 510 ug/L 102 67-140
Benzene 50.0 48.7 ug/L 97 70-120
Bromochloromethane 50.0 49.9 ug/L 100 65-122
Bromodichloromethane 50.0 50.0 ug/L 100 69-120
Bromoform 50.0 50.3 ug/L 101 56-132
Bromomethane 50.0 52.6 ug/L 105 40-130
Carbon disulfide 50.0 53.4 ug/L 107 66-120
Carbon tetrachloride 50.0 57.3 ug/L 115 65-122
Chlorobenzene 50.0 48.7 ug/L 97 70-120
Chloroethane 50.0 52.5 ug/L 105 45-127
Chloroform 50.0 51.3 ug/L 103 70-120
Chloromethane 50.0 44.1 ug/L 88 54-147
cis-1,2-Dichloroethene 50.0 50.5 ug/L 101 70-125
cis-1,3-Dichloropropene 50.0 46.2 ug/L 92 64-127
Dibromochloromethane 50.0 48.5 ug/L 97 68-125
Dibromomethane 50.0 49.7 ug/L 99 70-120
Ethylbenzene 50.0 49.6 ug/L 99 70-120
Iodomethane 50.0 52.6 ug/L 105 61-136
Methylene Chloride 50.0 51.1 ug/L 102 69-125
Styrene 50.0 51.5 ug/L 103 70-120
Tetrachloroethene 50.0 50.7 ug/L 101 70-128
Tetrahydrofuran 100 91.9 ug/L 92 59-139
Toluene 50.0 49.7 ug/L 99 70-125
trans-1,2-Dichloroethene 50.0 51.8 ug/L 104 70-125
trans-1,3-Dichloropropene 50.0 46.2 ug/L 92 62-128
trans-1,4-Dichloro-2-butene 50.0 47.6 ug/L 95 60-130
Trichloroethene 50.0 49.4 ug/L 99 70-125
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QC Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-405489/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405489
Trichlorofluoromethane 50.0 53.3 ug/L 107 70-126
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Vinyl acetate 50.0 46.6 ug/L 93 43-133
Vinyl chloride 50.0 50.4 ug/L 101 64-126
Xylenes, Total 100 103 ug/L 103 70-125
1,2-Dichloroethane-d4 (Surr)75 -126
Surrogate
102
LCS LCS
Qualifier Limits%Recovery
854-Bromofluorobenzene (Surr)72 -124
99Dibromofluoromethane 75 -120
93Toluene-d8 (Surr)75 -120
Client Sample ID: Method BlankLab Sample ID: MB 500-405855/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405855
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 10/18/17 15:03 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<1.0 0.381.0 ug/L 10/18/17 15:03 11,1,1-Trichloroethane
<1.0 0.401.0 ug/L 10/18/17 15:03 11,1,2,2-Tetrachloroethane
<1.0 0.351.0 ug/L 10/18/17 15:03 11,1,2-Trichloroethane
<1.0 0.411.0 ug/L 10/18/17 15:03 11,1-Dichloroethane
<1.0 0.391.0 ug/L 10/18/17 15:03 11,1-Dichloroethene
<1.0 0.301.0 ug/L 10/18/17 15:03 11,1-Dichloropropene
<1.0 0.411.0 ug/L 10/18/17 15:03 11,2,3-Trichloropropane
<1.0 0.341.0 ug/L 10/18/17 15:03 11,2,4-Trichlorobenzene
<5.0 2.05.0 ug/L 10/18/17 15:03 11,2-Dibromo-3-Chloropropane
<1.0 0.391.0 ug/L 10/18/17 15:03 11,2-Dibromoethane
<1.0 0.331.0 ug/L 10/18/17 15:03 11,2-Dichlorobenzene
<1.0 0.391.0 ug/L 10/18/17 15:03 11,2-Dichloroethane
<1.0 0.431.0 ug/L 10/18/17 15:03 11,2-Dichloropropane
<1.0 0.401.0 ug/L 10/18/17 15:03 11,3-Dichlorobenzene
<1.0 0.361.0 ug/L 10/18/17 15:03 11,3-Dichloropropane
<1.0 0.361.0 ug/L 10/18/17 15:03 11,4-Dichlorobenzene
<1.0 0.441.0 ug/L 10/18/17 15:03 12,2-Dichloropropane
<5.0 2.15.0 ug/L 10/18/17 15:03 12-Butanone (MEK)
<1.0 0.231.0 ug/L 10/18/17 15:03 12-Chloro-1,3-butadiene
<5.0 1.65.0 ug/L 10/18/17 15:03 12-Hexanone
<2.5 0.862.5 ug/L 10/18/17 15:03 13-Chloropropene
<5.0 2.25.0 ug/L 10/18/17 15:03 14-Methyl-2-pentanone (MIBK)
<5.0 1.75.0 ug/L 10/18/17 15:03 1Acetone
<10 4.210 ug/L 10/18/17 15:03 1Acetonitrile
<100 23100 ug/L 10/18/17 15:03 1Acrolein
<20 4.520 ug/L 10/18/17 15:03 1Acrylonitrile
<0.50 0.150.50 ug/L 10/18/17 15:03 1Benzene
<1.0 0.431.0 ug/L 10/18/17 15:03 1Bromochloromethane
<1.0 0.371.0 ug/L 10/18/17 15:03 1Bromodichloromethane
<1.0 0.481.0 ug/L 10/18/17 15:03 1Bromoform
<2.0 0.802.0 ug/L 10/18/17 15:03 1Bromomethane
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QC Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 500-405855/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405855
RL MDL
Carbon disulfide <2.0 2.0 0.45 ug/L 10/18/17 15:03 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<1.0 0.381.0 ug/L 10/18/17 15:03 1Carbon tetrachloride
<1.0 0.391.0 ug/L 10/18/17 15:03 1Chlorobenzene
<1.0 0.511.0 ug/L 10/18/17 15:03 1Chloroethane
<2.0 0.372.0 ug/L 10/18/17 15:03 1Chloroform
<1.0 0.321.0 ug/L 10/18/17 15:03 1Chloromethane
<1.0 0.411.0 ug/L 10/18/17 15:03 1cis-1,2-Dichloroethene
<1.0 0.421.0 ug/L 10/18/17 15:03 1cis-1,3-Dichloropropene
<1.0 0.491.0 ug/L 10/18/17 15:03 1Dibromochloromethane
<1.0 0.271.0 ug/L 10/18/17 15:03 1Dibromomethane
<2.0 0.672.0 ug/L 10/18/17 15:03 1Dichlorodifluoromethane
<2.5 0.532.5 ug/L 10/18/17 15:03 1Ethyl methacrylate
<0.50 0.180.50 ug/L 10/18/17 15:03 1Ethylbenzene
<1.0 0.451.0 ug/L 10/18/17 15:03 1Hexachlorobutadiene
<2.5 0.662.5 ug/L 10/18/17 15:03 1Iodomethane
<100 36100 ug/L 10/18/17 15:03 1Isobutyl alcohol
<10 2.510 ug/L 10/18/17 15:03 1Methacrylonitrile
<2.5 0.552.5 ug/L 10/18/17 15:03 1Methyl methacrylate
<5.0 1.65.0 ug/L 10/18/17 15:03 1Methylene Chloride
<10 4.810 ug/L 10/18/17 15:03 1Propionitrile
<1.0 0.391.0 ug/L 10/18/17 15:03 1Styrene
<1.0 0.371.0 ug/L 10/18/17 15:03 1Tetrachloroethene
<10 1.910 ug/L 10/18/17 15:03 1Tetrahydrofuran
<0.50 0.150.50 ug/L 10/18/17 15:03 1Toluene
<1.0 0.351.0 ug/L 10/18/17 15:03 1trans-1,2-Dichloroethene
<1.0 0.361.0 ug/L 10/18/17 15:03 1trans-1,3-Dichloropropene
<5.0 1.25.0 ug/L 10/18/17 15:03 1trans-1,4-Dichloro-2-butene
<0.50 0.160.50 ug/L 10/18/17 15:03 1Trichloroethene
<1.0 0.431.0 ug/L 10/18/17 15:03 1Trichlorofluoromethane
<2.0 0.912.0 ug/L 10/18/17 15:03 1Vinyl acetate
<0.50 0.200.50 ug/L 10/18/17 15:03 1Vinyl chloride
<1.0 0.221.0 ug/L 10/18/17 15:03 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)105 75-126 10/18/17 15:03 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
98 10/18/17 15:03 14-Bromofluorobenzene (Surr)72-124
96 10/18/17 15:03 1Dibromofluoromethane75-120
95 10/18/17 15:03 1Toluene-d8 (Surr)75-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-405855/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405855
1,1,1,2-Tetrachloroethane 50.0 54.8 ug/L 110 70-125
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,1,1-Trichloroethane 50.0 57.7 ug/L 115 70-125
1,1,2,2-Tetrachloroethane 50.0 42.6 ug/L 85 67-127
1,1,2-Trichloroethane 50.0 47.9 ug/L 96 70-122
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QC Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-405855/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405855
1,1-Dichloroethane 50.0 55.4 ug/L 111 70-125
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,1-Dichloroethene 50.0 53.9 ug/L 108 67-122
1,1-Dichloropropene 50.0 53.6 ug/L 107 70-121
1,2,3-Trichloropropane 50.0 44.1 ug/L 88 50-133
1,2,4-Trichlorobenzene 50.0 50.3 ug/L 101 66-127
1,2-Dibromo-3-Chloropropane 50.0 49.5 ug/L 99 56-123
1,2-Dibromoethane 50.0 48.5 ug/L 97 70-125
1,2-Dichlorobenzene 50.0 50.1 ug/L 100 70-125
1,2-Dichloroethane 50.0 58.2 ug/L 116 68-127
1,2-Dichloropropane 50.0 48.6 ug/L 97 67-130
1,3-Dichlorobenzene 50.0 49.5 ug/L 99 70-125
1,3-Dichloropropane 50.0 48.0 ug/L 96 62-136
1,4-Dichlorobenzene 50.0 49.9 ug/L 100 70-120
2,2-Dichloropropane 50.0 60.8 ug/L 122 58-129
2-Butanone (MEK)50.0 41.3 ug/L 83 53-141
2-Hexanone 50.0 47.5 ug/L 95 56-135
4-Methyl-2-pentanone (MIBK)50.0 47.6 ug/L 95 56-133
Acetone 50.0 47.4 ug/L 95 40-143
Acrylonitrile 500 556 ug/L 111 67-140
Benzene 50.0 50.5 ug/L 101 70-120
Bromochloromethane 50.0 50.7 ug/L 101 65-122
Bromodichloromethane 50.0 51.9 ug/L 104 69-120
Bromoform 50.0 55.7 ug/L 111 56-132
Bromomethane 50.0 45.2 ug/L 90 40-130
Carbon disulfide 50.0 55.3 ug/L 111 66-120
Carbon tetrachloride 50.0 59.0 ug/L 118 65-122
Chlorobenzene 50.0 52.9 ug/L 106 70-120
Chloroethane 50.0 43.4 ug/L 87 45-127
Chloroform 50.0 52.5 ug/L 105 70-120
Chloromethane 50.0 36.0 ug/L 72 54-147
cis-1,2-Dichloroethene 50.0 50.8 ug/L 102 70-125
cis-1,3-Dichloropropene 50.0 49.4 ug/L 99 64-127
Dibromochloromethane 50.0 51.8 ug/L 104 68-125
Dibromomethane 50.0 50.8 ug/L 102 70-120
Dichlorodifluoromethane 50.0 35.8 ug/L 72 40-150
Ethylbenzene 50.0 53.9 ug/L 108 70-120
Hexachlorobutadiene 50.0 54.5 ug/L 109 51-150
Iodomethane 50.0 53.6 ug/L 107 61-136
m&p-Xylene 50.0 54.4 ug/L 109 70-125
Methylene Chloride 50.0 51.5 ug/L 103 69-125
o-Xylene 50.0 55.9 ug/L 112 70-120
Styrene 50.0 55.5 ug/L 111 70-120
Tetrachloroethene 50.0 55.2 ug/L 110 70-128
Tetrahydrofuran 100 92.1 ug/L 92 59-139
Toluene 50.0 54.0 ug/L 108 70-125
trans-1,2-Dichloroethene 50.0 52.3 ug/L 105 70-125
trans-1,3-Dichloropropene 50.0 50.9 ug/L 102 62-128
trans-1,4-Dichloro-2-butene 50.0 56.7 ug/L 113 60-130
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QC Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-405855/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405855
Trichloroethene 50.0 50.6 ug/L 101 70-125
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Trichlorofluoromethane 50.0 47.5 ug/L 95 70-126
Vinyl acetate 50.0 53.0 ug/L 106 43-133
Vinyl chloride 50.0 44.5 ug/L 89 64-126
Xylenes, Total 100 110 ug/L 110 70-125
1,2-Dichloroethane-d4 (Surr)75 -126
Surrogate
102
LCS LCS
Qualifier Limits%Recovery
864-Bromofluorobenzene (Surr)72 -124
97Dibromofluoromethane 75 -120
96Toluene-d8 (Surr)75 -120
Client Sample ID: MW-10 InfillLab Sample ID: 500-135505-14 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405855
1,1,1,2-Tetrachloroethane <1.0 50.0 51.0 ug/L 102 70-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
1,1,1-Trichloroethane <1.0 50.0 53.6 ug/L 107 70-125
1,1,2,2-Tetrachloroethane <1.0 50.0 42.5 ug/L 85 67-127
1,1,2-Trichloroethane <1.0 50.0 47.8 ug/L 96 70-122
1,1-Dichloroethane <1.0 50.0 51.7 ug/L 103 70-125
1,1-Dichloroethene <1.0 50.0 48.4 ug/L 97 67-122
1,1-Dichloropropene <1.0 50.0 50.4 ug/L 101 70-121
1,2,3-Trichloropropane <1.0 50.0 41.8 ug/L 84 50-133
1,2,4-Trichlorobenzene <1.0 50.0 44.8 ug/L 90 66-127
1,2-Dibromo-3-Chloropropane <5.0 50.0 43.9 ug/L 88 56-123
1,2-Dibromoethane <1.0 50.0 46.5 ug/L 93 70-125
1,2-Dichlorobenzene <1.0 50.0 47.5 ug/L 95 70-125
1,2-Dichloroethane <1.0 50.0 56.8 ug/L 114 68-127
1,2-Dichloropropane <1.0 50.0 50.2 ug/L 100 67-130
1,3-Dichlorobenzene <1.0 50.0 46.9 ug/L 94 70-125
1,3-Dichloropropane <1.0 50.0 47.5 ug/L 95 62-136
1,4-Dichlorobenzene <1.0 50.0 46.7 ug/L 93 70-120
2,2-Dichloropropane <1.0 50.0 54.2 ug/L 108 58-129
2-Butanone (MEK)<5.0 50.0 43.6 ug/L 87 53-141
2-Hexanone <5.0 50.0 47.4 ug/L 95 56-135
4-Methyl-2-pentanone (MIBK)<5.0 50.0 47.4 ug/L 95 56-133
Acetone 15 cn 50.0 58.6 ug/L 88 40-143
Acrylonitrile <20 500 521 ug/L 104 67-140
Benzene <0.50 50.0 48.4 ug/L 97 70-120
Bromochloromethane <1.0 50.0 47.3 ug/L 95 65-122
Bromodichloromethane <1.0 50.0 51.2 ug/L 102 69-120
Bromoform <1.0 50.0 51.5 ug/L 103 56-132
Bromomethane <2.0 50.0 42.2 ug/L 84 40-130
Carbon disulfide <2.0 50.0 50.9 ug/L 102 66-120
Carbon tetrachloride <1.0 50.0 55.0 ug/L 110 65-122
Chlorobenzene <1.0 50.0 50.4 ug/L 101 70-120
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QC Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: MW-10 InfillLab Sample ID: 500-135505-14 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405855
Chloroethane <1.0 50.0 46.5 ug/L 93 45-127
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Chloroform <2.0 50.0 48.6 ug/L 97 70-120
Chloromethane <1.0 50.0 37.5 ug/L 75 54-147
cis-1,2-Dichloroethene <1.0 50.0 47.6 ug/L 95 70-125
cis-1,3-Dichloropropene <1.0 50.0 48.6 ug/L 97 64-127
Dibromochloromethane <1.0 50.0 50.6 ug/L 101 68-125
Dibromomethane <1.0 50.0 48.9 ug/L 98 70-120
Dichlorodifluoromethane <2.0 50.0 33.7 ug/L 67 40-150
Ethylbenzene <0.50 50.0 50.0 ug/L 100 70-120
Hexachlorobutadiene <1.0 50.0 48.8 ug/L 98 51-150
Iodomethane <2.5 50.0 49.8 ug/L 100 61-136
m&p-Xylene <1.0 50.0 51.5 ug/L 103 70-125
Methylene Chloride <5.0 50.0 48.2 ug/L 96 69-125
o-Xylene <0.50 50.0 52.0 ug/L 104 70-120
Styrene <1.0 50.0 51.7 ug/L 103 70-120
Tetrachloroethene <1.0 50.0 51.4 ug/L 103 70-128
Tetrahydrofuran 5.2 J 100 97.2 ug/L 92 59-139
Toluene <0.50 50.0 52.0 ug/L 104 70-125
trans-1,2-Dichloroethene <1.0 50.0 49.0 ug/L 98 70-125
trans-1,3-Dichloropropene <1.0 50.0 48.9 ug/L 98 62-128
trans-1,4-Dichloro-2-butene <5.0 50.0 50.0 ug/L 100 60-130
Trichloroethene <0.50 50.0 48.5 ug/L 97 70-125
Trichlorofluoromethane <1.0 50.0 46.5 ug/L 93 70-126
Vinyl acetate <2.0 50.0 50.1 ug/L 100 43-133
Vinyl chloride <0.50 50.0 44.5 ug/L 89 64-126
Xylenes, Total <1.0 100 104 ug/L 104 70-125
1,2-Dichloroethane-d4 (Surr)75 -126
Surrogate
103
MS MS
Qualifier Limits%Recovery
884-Bromofluorobenzene (Surr)72 -124
95Dibromofluoromethane 75 -120
95Toluene-d8 (Surr)75 -120
Client Sample ID: MW-10 InfillLab Sample ID: 500-135505-14 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405855
1,1,1,2-Tetrachloroethane <1.0 50.0 52.1 ug/L 104 70-125 2 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
1,1,1-Trichloroethane <1.0 50.0 54.2 ug/L 108 70-125 1 20
1,1,2,2-Tetrachloroethane <1.0 50.0 43.9 ug/L 88 67-127 3 20
1,1,2-Trichloroethane <1.0 50.0 50.0 ug/L 100 70-122 4 20
1,1-Dichloroethane <1.0 50.0 52.0 ug/L 104 70-125 1 20
1,1-Dichloroethene <1.0 50.0 48.5 ug/L 97 67-122 0 20
1,1-Dichloropropene <1.0 50.0 51.2 ug/L 102 70-121 2 20
1,2,3-Trichloropropane <1.0 50.0 43.5 ug/L 87 50-133 4 20
1,2,4-Trichlorobenzene <1.0 50.0 46.0 ug/L 92 66-127 2 20
1,2-Dibromo-3-Chloropropane <5.0 50.0 48.9 ug/L 98 56-123 11 20
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QC Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: MW-10 InfillLab Sample ID: 500-135505-14 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405855
1,2-Dibromoethane <1.0 50.0 47.9 ug/L 96 70-125 3 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
1,2-Dichlorobenzene <1.0 50.0 49.1 ug/L 98 70-125 3 20
1,2-Dichloroethane <1.0 50.0 57.6 ug/L 115 68-127 1 20
1,2-Dichloropropane <1.0 50.0 50.4 ug/L 101 67-130 1 20
1,3-Dichlorobenzene <1.0 50.0 48.4 ug/L 97 70-125 3 20
1,3-Dichloropropane <1.0 50.0 49.1 ug/L 98 62-136 3 20
1,4-Dichlorobenzene <1.0 50.0 48.9 ug/L 98 70-120 5 20
2,2-Dichloropropane <1.0 50.0 54.4 ug/L 109 58-129 0 20
2-Butanone (MEK)<5.0 50.0 47.9 ug/L 96 53-141 10 20
2-Hexanone <5.0 50.0 47.8 ug/L 96 56-135 1 20
4-Methyl-2-pentanone (MIBK)<5.0 50.0 47.5 ug/L 95 56-133 0 20
Acetone 15 cn 50.0 65.1 ug/L 101 40-143 10 20
Acrylonitrile <20 500 521 ug/L 104 67-140 0 20
Benzene <0.50 50.0 49.4 ug/L 99 70-120 2 20
Bromochloromethane <1.0 50.0 46.9 ug/L 94 65-122 1 20
Bromodichloromethane <1.0 50.0 52.4 ug/L 105 69-120 2 20
Bromoform <1.0 50.0 52.0 ug/L 104 56-132 1 20
Bromomethane <2.0 50.0 43.5 ug/L 87 40-130 3 20
Carbon disulfide <2.0 50.0 51.1 ug/L 102 66-120 0 20
Carbon tetrachloride <1.0 50.0 54.9 ug/L 110 65-122 0 20
Chlorobenzene <1.0 50.0 51.6 ug/L 103 70-120 2 20
Chloroethane <1.0 50.0 44.8 ug/L 90 45-127 4 20
Chloroform <2.0 50.0 49.3 ug/L 99 70-120 1 20
Chloromethane <1.0 50.0 36.6 ug/L 73 54-147 2 20
cis-1,2-Dichloroethene <1.0 50.0 48.0 ug/L 96 70-125 1 20
cis-1,3-Dichloropropene <1.0 50.0 49.3 ug/L 99 64-127 1 20
Dibromochloromethane <1.0 50.0 51.8 ug/L 104 68-125 2 20
Dibromomethane <1.0 50.0 49.8 ug/L 100 70-120 2 20
Dichlorodifluoromethane <2.0 50.0 32.6 ug/L 65 40-150 3 20
Ethylbenzene <0.50 50.0 50.7 ug/L 101 70-120 1 20
Hexachlorobutadiene <1.0 50.0 50.6 ug/L 101 51-150 4 20
Iodomethane <2.5 50.0 49.9 ug/L 100 61-136 0 20
m&p-Xylene <1.0 50.0 52.2 ug/L 104 70-125 1 20
Methylene Chloride <5.0 50.0 48.1 ug/L 96 69-125 0 20
o-Xylene <0.50 50.0 52.1 ug/L 104 70-120 0 20
Styrene <1.0 50.0 52.3 ug/L 105 70-120 1 20
Tetrachloroethene <1.0 50.0 51.5 ug/L 103 70-128 0 20
Tetrahydrofuran 5.2 J 100 96.5 ug/L 91 59-139 1 20
Toluene <0.50 50.0 52.7 ug/L 105 70-125 1 20
trans-1,2-Dichloroethene <1.0 50.0 49.0 ug/L 98 70-125 0 20
trans-1,3-Dichloropropene <1.0 50.0 50.1 ug/L 100 62-128 3 20
trans-1,4-Dichloro-2-butene <5.0 50.0 53.9 ug/L 108 60-130 8 20
Trichloroethene <0.50 50.0 48.8 ug/L 98 70-125 1 20
Trichlorofluoromethane <1.0 50.0 46.4 ug/L 93 70-126 0 20
Vinyl acetate <2.0 50.0 50.1 ug/L 100 43-133 0 20
Vinyl chloride <0.50 50.0 43.5 ug/L 87 64-126 2 20
Xylenes, Total <1.0 100 104 ug/L 104 70-125 1 20
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QC Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: MW-10 InfillLab Sample ID: 500-135505-14 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405855
1,2-Dichloroethane-d4 (Surr)75 -126
Surrogate
104
MSD MSD
Qualifier Limits%Recovery
914-Bromofluorobenzene (Surr)72 -124
96Dibromofluoromethane 75 -120
96Toluene-d8 (Surr)75 -120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 500-405441/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405562 Prep Batch: 405441
RL MDL
Acenaphthene <0.80 0.80 0.25 ug/L 10/16/17 07:32 10/16/17 22:17 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.80 0.210.80 ug/L 10/16/17 07:32 10/16/17 22:17 1Acenaphthylene
<4.0 0.534.0 ug/L 10/16/17 07:32 10/16/17 22:17 1Acetophenone
<8.0 1.78.0 ug/L 10/16/17 07:32 10/16/17 22:17 12-Acetylaminofluorene
<8.0 3.08.0 ug/L 10/16/17 07:32 10/16/17 22:17 14-Aminobiphenyl
<0.80 0.270.80 ug/L 10/16/17 07:32 10/16/17 22:17 1Anthracene
<0.16 0.0450.16 ug/L 10/16/17 07:32 10/16/17 22:17 1Benzo[a]anthracene
<0.16 0.0790.16 ug/L 10/16/17 07:32 10/16/17 22:17 1Benzo[a]pyrene
<0.16 0.0650.16 ug/L 10/16/17 07:32 10/16/17 22:17 1Benzo[b]fluoranthene
<0.80 0.300.80 ug/L 10/16/17 07:32 10/16/17 22:17 1Benzo[g,h,i]perylene
<0.16 0.0510.16 ug/L 10/16/17 07:32 10/16/17 22:17 1Benzo[k]fluoranthene
<16 4.816 ug/L 10/16/17 07:32 10/16/17 22:17 1Benzyl alcohol
<1.6 0.231.6 ug/L 10/16/17 07:32 10/16/17 22:17 1Bis(2-chloroethoxy)methane
<1.6 0.231.6 ug/L 10/16/17 07:32 10/16/17 22:17 1Bis(2-chloroethyl)ether
<8.0 1.48.0 ug/L 10/16/17 07:32 10/16/17 22:17 1Bis(2-ethylhexyl) phthalate
<4.0 0.434.0 ug/L 10/16/17 07:32 10/16/17 22:17 14-Bromophenyl phenyl ether
<1.6 0.381.6 ug/L 10/16/17 07:32 10/16/17 22:17 1Butyl benzyl phthalate
<8.0 1.68.0 ug/L 10/16/17 07:32 10/16/17 22:17 14-Chloroaniline
<8.0 2.78.0 ug/L 10/16/17 07:32 10/16/17 22:17 1Chlorobenzilate
<8.0 1.88.0 ug/L 10/16/17 07:32 10/16/17 22:17 14-Chloro-3-methylphenol
<1.6 0.191.6 ug/L 10/16/17 07:32 10/16/17 22:17 12-Chloronaphthalene
<4.0 0.454.0 ug/L 10/16/17 07:32 10/16/17 22:17 12-Chlorophenol
<4.0 0.514.0 ug/L 10/16/17 07:32 10/16/17 22:17 14-Chlorophenyl phenyl ether
<0.16 0.0550.16 ug/L 10/16/17 07:32 10/16/17 22:17 1Chrysene
<8.0 4.48.0 ug/L 10/16/17 07:32 10/16/17 22:17 1Diallate
<0.24 0.0410.24 ug/L 10/16/17 07:32 10/16/17 22:17 1Dibenz(a,h)anthracene
<1.6 0.211.6 ug/L 10/16/17 07:32 10/16/17 22:17 1Dibenzofuran
<4.0 1.44.0 ug/L 10/16/17 07:32 10/16/17 22:17 13,3'-Dichlorobenzidine
<8.0 2.18.0 ug/L 10/16/17 07:32 10/16/17 22:17 12,4-Dichlorophenol
<8.0 2.88.0 ug/L 10/16/17 07:32 10/16/17 22:17 12,6-Dichlorophenol
<4.0 0.294.0 ug/L 10/16/17 07:32 10/16/17 22:17 1Diethyl phthalate
<8.0 1.58.0 ug/L 10/16/17 07:32 10/16/17 22:17 1Dimethoate
<32 2.432 ug/L 10/16/17 07:32 10/16/17 22:17 17,12-Dimethylbenz(a)anthracene
<32 1432 ug/L 10/16/17 07:32 10/16/17 22:17 13,3'-Dimethylbenzidine
<8.0 1.48.0 ug/L 10/16/17 07:32 10/16/17 22:17 12,4-Dimethylphenol
<4.0 0.254.0 ug/L 10/16/17 07:32 10/16/17 22:17 1Dimethyl phthalate
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QC Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 500-405441/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405562 Prep Batch: 405441
RL MDL
Di-n-butyl phthalate <4.0 4.0 0.58 ug/L 10/16/17 07:32 10/16/17 22:17 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<16 4.716 ug/L 10/16/17 07:32 10/16/17 22:17 14,6-Dinitro-2-methylphenol
<16 6.916 ug/L 10/16/17 07:32 10/16/17 22:17 12,4-Dinitrophenol
<0.80 0.200.80 ug/L 10/16/17 07:32 10/16/17 22:17 12,4-Dinitrotoluene
<0.80 0.0590.80 ug/L 10/16/17 07:32 10/16/17 22:17 12,6-Dinitrotoluene
<8.0 0.848.0 ug/L 10/16/17 07:32 10/16/17 22:17 1Di-n-octyl phthalate
<8.0 2.08.0 ug/L 10/16/17 07:32 10/16/17 22:17 1Diphenylamine
<8.0 1.58.0 ug/L 10/16/17 07:32 10/16/17 22:17 1Disulfoton
<16 3.016 ug/L 10/16/17 07:32 10/16/17 22:17 1Ethyl methanesulfonate
<8.0 1.78.0 ug/L 10/16/17 07:32 10/16/17 22:17 1Ethyl Parathion
<32 2432 ug/L 10/16/17 07:32 10/16/17 22:17 1Famphur
<0.80 0.360.80 ug/L 10/16/17 07:32 10/16/17 22:17 1Fluoranthene
<0.80 0.200.80 ug/L 10/16/17 07:32 10/16/17 22:17 1Fluorene
<0.40 0.0640.40 ug/L 10/16/17 07:32 10/16/17 22:17 1Hexachlorobenzene
<16 5.116 ug/L 10/16/17 07:32 10/16/17 22:17 1Hexachlorocyclopentadiene
<4.0 0.484.0 ug/L 10/16/17 07:32 10/16/17 22:17 1Hexachloroethane
<16 3.816 ug/L 10/16/17 07:32 10/16/17 22:17 1Hexachloropropene
<0.16 0.0600.16 ug/L 10/16/17 07:32 10/16/17 22:17 1Indeno[1,2,3-cd]pyrene
<16 5.516 ug/L 10/16/17 07:32 10/16/17 22:17 1Isodrin
<1.6 0.301.6 ug/L 10/16/17 07:32 10/16/17 22:17 1Isophorone
<8.0 3.18.0 ug/L 10/16/17 07:32 10/16/17 22:17 1Isosafrole
<8.0 1.38.0 ug/L 10/16/17 07:32 10/16/17 22:17 1Kepone
<4.0 1.14.0 ug/L 10/16/17 07:32 10/16/17 22:17 1m-Dinitrobenzene
<32 8.132 ug/L 10/16/17 07:32 10/16/17 22:17 1Methapyrilene
<8.0 1.88.0 ug/L 10/16/17 07:32 10/16/17 22:17 13-Methylcholanthrene
<32 4.832 ug/L 10/16/17 07:32 10/16/17 22:17 1Methyl methanesulfonate
<1.6 0.0521.6 ug/L 10/16/17 07:32 10/16/17 22:17 12-Methylnaphthalene
<8.0 1.98.0 ug/L 10/16/17 07:32 10/16/17 22:17 1Methyl parathion
<1.6 0.241.6 ug/L 10/16/17 07:32 10/16/17 22:17 12-Methylphenol
<1.6 0.361.6 ug/L 10/16/17 07:32 10/16/17 22:17 13 & 4 Methylphenol
<0.80 0.250.80 ug/L 10/16/17 07:32 10/16/17 22:17 1Naphthalene
<32 3132 ug/L 10/16/17 07:32 10/16/17 22:17 11,4-Naphthoquinone
<16 4.716 ug/L 10/16/17 07:32 10/16/17 22:17 11-Naphthylamine
<16 7.316 ug/L 10/16/17 07:32 10/16/17 22:17 12-Naphthylamine
<4.0 1.04.0 ug/L 10/16/17 07:32 10/16/17 22:17 12-Nitroaniline
<8.0 1.48.0 ug/L 10/16/17 07:32 10/16/17 22:17 13-Nitroaniline
<8.0 1.38.0 ug/L 10/16/17 07:32 10/16/17 22:17 14-Nitroaniline
<0.80 0.360.80 ug/L 10/16/17 07:32 10/16/17 22:17 1Nitrobenzene
<8.0 2.58.0 ug/L 10/16/17 07:32 10/16/17 22:17 15-Nitro-o-toluidine
<8.0 2.08.0 ug/L 10/16/17 07:32 10/16/17 22:17 12-Nitrophenol
<16 5.916 ug/L 10/16/17 07:32 10/16/17 22:17 14-Nitrophenol
<16 6.916 ug/L 10/16/17 07:32 10/16/17 22:17 1N-Nitrosodiethylamine
<8.0 3.88.0 ug/L 10/16/17 07:32 10/16/17 22:17 1N-Nitrosodimethylamine
<8.0 3.48.0 ug/L 10/16/17 07:32 10/16/17 22:17 1N-Nitrosodi-n-butylamine
<0.40 0.120.40 ug/L 10/16/17 07:32 10/16/17 22:17 1N-Nitrosodi-n-propylamine
<1.6 0.301.6 ug/L 10/16/17 07:32 10/16/17 22:17 1N-Nitrosodiphenylamine
<16 6.016 ug/L 10/16/17 07:32 10/16/17 22:17 1N-Nitrosomethylethylamine
<8.0 2.88.0 ug/L 10/16/17 07:32 10/16/17 22:17 1N-Nitrosopiperidine
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QC Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 500-405441/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405562 Prep Batch: 405441
RL MDL
N-Nitrosopyrrolidine <8.0 8.0 2.7 ug/L 10/16/17 07:32 10/16/17 22:17 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<16 4.416 ug/L 10/16/17 07:32 10/16/17 22:17 1o,o',o''-Triethylphosphorothioate
<32 6.332 ug/L 10/16/17 07:32 10/16/17 22:17 1o-Toluidine
<1.6 0.301.6 ug/L 10/16/17 07:32 10/16/17 22:17 12,2'-oxybis[1-chloropropane]
<8.0 2.48.0 ug/L 10/16/17 07:32 10/16/17 22:17 1p-Dimethylamino azobenzene
<8.0 2.28.0 ug/L 10/16/17 07:32 10/16/17 22:17 1Pentachlorobenzene
<8.0 2.98.0 ug/L 10/16/17 07:32 10/16/17 22:17 1Pentachloronitrobenzene
<8.0 1.88.0 ug/L 10/16/17 07:32 10/16/17 22:17 1Phenacetin
<0.80 0.240.80 ug/L 10/16/17 07:32 10/16/17 22:17 1Phenanthrene
<4.0 0.544.0 ug/L 10/16/17 07:32 10/16/17 22:17 1Phenol
<8.0 1.78.0 ug/L 10/16/17 07:32 10/16/17 22:17 1Phorate
<64 1364 ug/L 10/16/17 07:32 10/16/17 22:17 1p-Phenylene diamine
<8.0 1.78.0 ug/L 10/16/17 07:32 10/16/17 22:17 1Pronamide
<0.80 0.340.80 ug/L 10/16/17 07:32 10/16/17 22:17 1Pyrene
<8.0 3.28.0 ug/L 10/16/17 07:32 10/16/17 22:17 1Safrole
<8.0 1.58.0 ug/L 10/16/17 07:32 10/16/17 22:17 1sym-Trinitrobenzene
<8.0 8.08.0 ug/L 10/16/17 07:32 10/16/17 22:17 12,3,7,8-TCDD (Screen)
<4.0 0.464.0 ug/L 10/16/17 07:32 10/16/17 22:17 11,2,4,5-Tetrachlorobenzene
<4.0 0.604.0 ug/L 10/16/17 07:32 10/16/17 22:17 12,3,4,6-Tetrachlorophenol
<8.0 2.18.0 ug/L 10/16/17 07:32 10/16/17 22:17 1Thionazin
<8.0 2.18.0 ug/L 10/16/17 07:32 10/16/17 22:17 12,4,5-Trichlorophenol
<4.0 0.574.0 ug/L 10/16/17 07:32 10/16/17 22:17 12,4,6-Trichlorophenol
2-Fluorobiphenyl 74 34-110 10/16/17 22:17 1
MB MB
Surrogate
10/16/17 07:32
Dil FacPreparedAnalyzedQualifierLimits%Recovery
61 10/16/17 07:32 10/16/17 22:17 12-Fluorophenol 27-110
75 10/16/17 07:32 10/16/17 22:17 1Nitrobenzene-d5 36-120
35 10/16/17 07:32 10/16/17 22:17 1Phenol-d5 20-100
99 10/16/17 07:32 10/16/17 22:17 1Terphenyl-d14 40-145
103 10/16/17 07:32 10/16/17 22:17 12,4,6-Tribromophenol 40-145
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-405441/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405562 Prep Batch: 405441
Acenaphthene 32.0 25.4 ug/L 79 46-110
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Acenaphthylene 32.0 22.9 ug/L 71 47-110
Acetophenone 32.0 21.6 ug/L 68 60-110
Anthracene 32.0 27.7 ug/L 87 67-110
Benzo[a]anthracene 32.0 28.8 ug/L 90 70-120
Benzo[a]pyrene 32.0 32.8 ug/L 103 70-120
Benzo[b]fluoranthene 32.0 32.3 ug/L 101 69-123
Benzo[g,h,i]perylene 32.0 34.6 ug/L 108 70-120
Benzo[k]fluoranthene 32.0 31.4 ug/L 98 70-120
Benzyl alcohol 32.0 21.3 ug/L 67 33-127
Bis(2-chloroethoxy)methane 32.0 24.7 ug/L 77 60-110
Bis(2-chloroethyl)ether 32.0 20.4 ug/L 64 49-110
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QC Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-405441/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405562 Prep Batch: 405441
Bis(2-ethylhexyl) phthalate 32.0 28.8 ug/L 90 69-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
4-Bromophenyl phenyl ether 32.0 26.7 ug/L 83 58-120
Butyl benzyl phthalate 32.0 29.2 ug/L 91 68-120
4-Chloroaniline 32.0 22.4 ug/L 70 35-128
4-Chloro-3-methylphenol 32.0 27.9 ug/L 87 64-120
2-Chloronaphthalene 32.0 21.7 ug/L 68 39-110
2-Chlorophenol 32.0 23.0 ug/L 72 59-110
4-Chlorophenyl phenyl ether 32.0 24.4 ug/L 76 47-112
Chrysene 32.0 29.1 ug/L 91 68-120
Dibenz(a,h)anthracene 32.0 34.9 ug/L 109 70-127
Dibenzofuran 32.0 24.2 ug/L 75 51-110
3,3'-Dichlorobenzidine 32.0 30.9 ug/L 97 60-132
2,4-Dichlorophenol 32.0 26.9 ug/L 84 62-110
2,6-Dichlorophenol 32.0 25.7 ug/L 80 60-110
Diethyl phthalate 32.0 29.5 ug/L 92 62-120
2,4-Dimethylphenol 32.0 25.6 ug/L 80 51-110
Dimethyl phthalate 32.0 27.8 ug/L 87 63-120
Di-n-butyl phthalate 32.0 28.6 ug/L 89 70-120
4,6-Dinitro-2-methylphenol 64.0 51.8 ug/L 81 50-117
2,4-Dinitrophenol 64.0 56.7 ug/L 89 37-130
2,4-Dinitrotoluene 32.0 31.4 ug/L 98 63-122
2,6-Dinitrotoluene 32.0 30.0 ug/L 94 63-119
Di-n-octyl phthalate 32.0 30.7 ug/L 96 70-122
Fluoranthene 32.0 29.8 ug/L 93 68-120
Fluorene 32.0 25.2 ug/L 79 53-120
Hexachlorobenzene 32.0 28.3 ug/L 88 61-120
Hexachlorocyclopentadiene 32.0 14.5 J ug/L 45 10-100
Hexachloroethane 32.0 14.5 ug/L 45 20-100
Indeno[1,2,3-cd]pyrene 32.0 34.4 ug/L 108 65-133
Isophorone 32.0 23.9 ug/L 75 57-110
2-Methylnaphthalene 32.0 19.9 ug/L 62 34-110
2-Methylphenol 32.0 22.6 ug/L 71 53-110
3 & 4 Methylphenol 32.0 21.5 ug/L 67 53-110
Naphthalene 32.0 20.2 ug/L 63 36-110
2-Nitroaniline 32.0 28.3 ug/L 89 59-122
3-Nitroaniline 32.0 26.9 ug/L 84 47-123
4-Nitroaniline 32.0 24.7 ug/L 77 52-147
Nitrobenzene 32.0 26.0 ug/L 81 53-110
2-Nitrophenol 32.0 24.5 ug/L 77 58-110
4-Nitrophenol 64.0 40.8 ug/L 64 20-110
N-Nitrosodimethylamine 32.0 16.0 ug/L 50 41-110
N-Nitrosodi-n-propylamine 32.0 23.2 ug/L 72 58-110
N-Nitrosodiphenylamine 32.0 27.6 ug/L 86 66-110
2,2'-oxybis[1-chloropropane]32.0 13.3 ug/L 42 38-110
Phenanthrene 32.0 27.0 ug/L 85 65-120
Phenol 32.0 15.5 ug/L 49 33-100
Pyrene 32.0 29.1 ug/L 91 70-110
1,2,4,5-Tetrachlorobenzene 32.0 20.2 ug/L 63 30-110
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QC Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-405441/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405562 Prep Batch: 405441
2,3,4,6-Tetrachlorophenol 32.0 28.3 ug/L 88 44-118
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
2,4,5-Trichlorophenol 32.0 28.2 ug/L 88 63-120
2,4,6-Trichlorophenol 32.0 27.1 ug/L 85 62-110
2-Fluorobiphenyl 34 -110
Surrogate
73
LCS LCS
Qualifier Limits%Recovery
602-Fluorophenol 27 -110
75Nitrobenzene-d5 36 -120
46Phenol-d5 20 -100
96Terphenyl-d14 40 -145
1052,4,6-Tribromophenol 40 -145
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 500-405441/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405562 Prep Batch: 405441
Acenaphthene 32.0 26.1 ug/L 82 46-110 3 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acenaphthylene 32.0 23.6 ug/L 74 47-110 3 20
Acetophenone 32.0 22.1 ug/L 69 60-110 2 20
Anthracene 32.0 28.3 ug/L 88 67-110 2 20
Benzo[a]anthracene 32.0 29.2 ug/L 91 70-120 1 20
Benzo[a]pyrene 32.0 33.0 ug/L 103 70-120 1 20
Benzo[b]fluoranthene 32.0 32.4 ug/L 101 69-123 0 20
Benzo[g,h,i]perylene 32.0 34.5 ug/L 108 70-120 0 20
Benzo[k]fluoranthene 32.0 31.9 ug/L 100 70-120 2 20
Benzyl alcohol 32.0 21.8 ug/L 68 33-127 3 20
Bis(2-chloroethoxy)methane 32.0 24.9 ug/L 78 60-110 1 20
Bis(2-chloroethyl)ether 32.0 20.5 ug/L 64 49-110 0 20
Bis(2-ethylhexyl) phthalate 32.0 29.1 ug/L 91 69-120 1 20
4-Bromophenyl phenyl ether 32.0 27.3 ug/L 85 58-120 3 20
Butyl benzyl phthalate 32.0 29.5 ug/L 92 68-120 1 20
4-Chloroaniline 32.0 24.2 ug/L 76 35-128 8 20
4-Chloro-3-methylphenol 32.0 28.0 ug/L 88 64-120 1 20
2-Chloronaphthalene 32.0 21.6 ug/L 68 39-110 0 20
2-Chlorophenol 32.0 23.3 ug/L 73 59-110 1 20
4-Chlorophenyl phenyl ether 32.0 25.1 ug/L 78 47-112 3 20
Chrysene 32.0 29.2 ug/L 91 68-120 0 20
Dibenz(a,h)anthracene 32.0 35.3 ug/L 110 70-127 1 20
Dibenzofuran 32.0 25.3 ug/L 79 51-110 5 20
3,3'-Dichlorobenzidine 32.0 32.0 ug/L 100 60-132 4 20
2,4-Dichlorophenol 32.0 27.1 ug/L 85 62-110 1 20
2,6-Dichlorophenol 32.0 26.2 ug/L 82 60-110 2 20
Diethyl phthalate 32.0 30.4 ug/L 95 62-120 3 20
2,4-Dimethylphenol 32.0 25.8 ug/L 81 51-110 1 20
Dimethyl phthalate 32.0 28.5 ug/L 89 63-120 3 20
Di-n-butyl phthalate 32.0 28.8 ug/L 90 70-120 1 20
4,6-Dinitro-2-methylphenol 64.0 52.1 ug/L 81 50-117 1 20
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QC Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 500-405441/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405562 Prep Batch: 405441
2,4-Dinitrophenol 64.0 58.7 ug/L 92 37-130 3 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
2,4-Dinitrotoluene 32.0 32.5 ug/L 102 63-122 3 20
2,6-Dinitrotoluene 32.0 30.7 ug/L 96 63-119 2 20
Di-n-octyl phthalate 32.0 30.9 ug/L 97 70-122 1 20
Fluoranthene 32.0 30.2 ug/L 94 68-120 1 20
Fluorene 32.0 26.0 ug/L 81 53-120 3 20
Hexachlorobenzene 32.0 28.9 ug/L 90 61-120 2 20
Hexachlorocyclopentadiene 32.0 14.0 J ug/L 44 10-100 4 20
Hexachloroethane 32.0 13.8 ug/L 43 20-100 5 20
Indeno[1,2,3-cd]pyrene 32.0 34.7 ug/L 108 65-133 1 20
Isophorone 32.0 24.5 ug/L 76 57-110 2 20
2-Methylnaphthalene 32.0 20.3 ug/L 63 34-110 2 20
2-Methylphenol 32.0 22.9 ug/L 72 53-110 1 20
3 & 4 Methylphenol 32.0 22.3 ug/L 70 53-110 4 20
Naphthalene 32.0 20.8 ug/L 65 36-110 3 20
2-Nitroaniline 32.0 29.7 ug/L 93 59-122 5 20
3-Nitroaniline 32.0 29.4 ug/L 92 47-123 9 20
4-Nitroaniline 32.0 25.8 ug/L 81 52-147 5 20
Nitrobenzene 32.0 26.7 ug/L 83 53-110 3 20
2-Nitrophenol 32.0 24.9 ug/L 78 58-110 2 20
4-Nitrophenol 64.0 45.0 ug/L 70 20-110 10 20
N-Nitrosodimethylamine 32.0 16.2 ug/L 51 41-110 2 20
N-Nitrosodi-n-propylamine 32.0 23.6 ug/L 74 58-110 2 20
N-Nitrosodiphenylamine 32.0 28.0 ug/L 88 66-110 1 20
2,2'-oxybis[1-chloropropane]32.0 13.7 ug/L 43 38-110 2 20
Phenanthrene 32.0 27.6 ug/L 86 65-120 2 20
Phenol 32.0 16.5 ug/L 52 33-100 6 20
Pyrene 32.0 29.4 ug/L 92 70-110 1 20
1,2,4,5-Tetrachlorobenzene 32.0 19.6 ug/L 61 30-110 3 20
2,3,4,6-Tetrachlorophenol 32.0 29.8 ug/L 93 44-118 5 20
2,4,5-Trichlorophenol 32.0 29.0 ug/L 91 63-120 3 20
2,4,6-Trichlorophenol 32.0 27.8 ug/L 87 62-110 3 20
2-Fluorobiphenyl 34 -110
Surrogate
73
LCSD LCSD
Qualifier Limits%Recovery
622-Fluorophenol 27 -110
76Nitrobenzene-d5 36 -120
48Phenol-d5 20 -100
97Terphenyl-d14 40 -145
1082,4,6-Tribromophenol 40 -145
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QC Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 8081B - Organochlorine Pesticides (GC)
Client Sample ID: Method BlankLab Sample ID: MB 500-405223/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405522 Prep Batch: 405223
RL MDL
alpha-BHC <0.040 0.040 0.0026 ug/L 10/13/17 09:13 10/16/17 14:25 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.040 0.0100.040 ug/L 10/13/17 09:13 10/16/17 14:25 1beta-BHC
<0.040 0.0100.040 ug/L 10/13/17 09:13 10/16/17 14:25 1delta-BHC
<0.040 0.00560.040 ug/L 10/13/17 09:13 10/16/17 14:25 1gamma-BHC (Lindane)
<0.040 0.0140.040 ug/L 10/13/17 09:13 10/16/17 14:25 1Heptachlor
<0.040 0.00530.040 ug/L 10/13/17 09:13 10/16/17 14:25 1Aldrin
<0.040 0.0140.040 ug/L 10/13/17 09:13 10/16/17 14:25 1Heptachlor epoxide
<0.040 0.00410.040 ug/L 10/13/17 09:13 10/16/17 14:25 1Endosulfan I
<0.040 0.0130.040 ug/L 10/13/17 09:13 10/16/17 14:25 1Dieldrin
<0.040 0.00380.040 ug/L 10/13/17 09:13 10/16/17 14:25 14,4'-DDE
<0.040 0.0140.040 ug/L 10/13/17 09:13 10/16/17 14:25 1Endrin
<0.040 0.00280.040 ug/L 10/13/17 09:13 10/16/17 14:25 1Endosulfan II
<0.040 0.0130.040 ug/L 10/13/17 09:13 10/16/17 14:25 14,4'-DDD
<0.040 0.0120.040 ug/L 10/13/17 09:13 10/16/17 14:25 1Endosulfan sulfate
<0.040 0.00320.040 ug/L 10/13/17 09:13 10/16/17 14:25 14,4'-DDT
<0.080 0.0230.080 ug/L 10/13/17 09:13 10/16/17 14:25 1Methoxychlor
<0.40 0.200.40 ug/L 10/13/17 09:13 10/16/17 14:25 1Toxaphene
<0.040 0.00820.040 ug/L 10/13/17 09:13 10/16/17 14:25 1Endrin aldehyde
<0.080 0.0400.080 ug/L 10/13/17 09:13 10/16/17 14:25 1Chlordane (technical)
DCB Decachlorobiphenyl 81 30-130 10/16/17 14:25 1
MB MB
Surrogate
10/13/17 09:13
Dil FacPreparedAnalyzedQualifierLimits%Recovery
81 10/13/17 09:13 10/16/17 14:25 1Tetrachloro-m-xylene 30-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-405223/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405522 Prep Batch: 405223
alpha-BHC 0.320 0.341 ug/L 107 65-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
beta-BHC 0.320 0.331 ug/L 103 65-120
delta-BHC 0.320 0.312 ug/L 98 70-122
gamma-BHC (Lindane)0.320 0.334 ug/L 104 68-120
Heptachlor 0.320 0.300 ug/L 94 40-120
Aldrin 0.320 0.272 ug/L 85 34-120
Heptachlor epoxide 0.320 0.296 ug/L 92 64-120
Endosulfan I 0.320 0.235 ug/L 74 35-110
Dieldrin 0.320 0.310 ug/L 97 68-120
4,4'-DDE 0.320 0.302 ug/L 94 58-122
Endrin 0.320 0.312 ug/L 98 60-132
Endosulfan II 0.320 0.260 ug/L 81 53-110
4,4'-DDD 0.320 0.323 ug/L 101 69-124
Endosulfan sulfate 0.320 0.299 ug/L 93 70-133
4,4'-DDT 0.320 0.282 ug/L 88 62-127
Methoxychlor 0.320 0.293 ug/L 91 63-135
Endrin aldehyde 0.320 0.285 ug/L 89 66-120
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QC Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-405223/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405522 Prep Batch: 405223
DCB Decachlorobiphenyl 30 -130
Surrogate
87
LCS LCS
Qualifier Limits%Recovery
84Tetrachloro-m-xylene 30 -120
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 500-405223/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405522 Prep Batch: 405223
alpha-BHC 0.320 0.332 ug/L 104 65-120 3 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
beta-BHC 0.320 0.320 ug/L 100 65-120 3 20
delta-BHC 0.320 0.319 ug/L 100 70-122 2 20
gamma-BHC (Lindane)0.320 0.328 ug/L 102 68-120 2 20
Heptachlor 0.320 0.305 ug/L 95 40-120 2 20
Aldrin 0.320 0.290 ug/L 91 34-120 6 20
Heptachlor epoxide 0.320 0.309 ug/L 97 64-120 4 20
Endosulfan I 0.320 0.261 ug/L 82 35-110 11 20
Dieldrin 0.320 0.321 ug/L 100 68-120 4 20
4,4'-DDE 0.320 0.303 ug/L 95 58-122 0 20
Endrin 0.320 0.317 ug/L 99 60-132 2 20
Endosulfan II 0.320 0.291 ug/L 91 53-110 11 20
4,4'-DDD 0.320 0.331 ug/L 104 69-124 2 20
Endosulfan sulfate 0.320 0.312 ug/L 98 70-133 4 20
4,4'-DDT 0.320 0.340 ug/L 106 62-127 19 20
Methoxychlor 0.320 0.300 ug/L 94 63-135 2 20
Endrin aldehyde 0.320 0.337 ug/L 105 66-120 17 20
DCB Decachlorobiphenyl 30 -130
Surrogate
82
LCSD LCSD
Qualifier Limits%Recovery
83Tetrachloro-m-xylene 30 -120
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 500-405223/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 406209 Prep Batch: 405223
RL MDL
PCB-1016 <0.40 0.40 0.067 ug/L 10/13/17 09:13 10/20/17 11:48 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.40 0.200.40 ug/L 10/13/17 09:13 10/20/17 11:48 1PCB-1221
<0.40 0.200.40 ug/L 10/13/17 09:13 10/20/17 11:48 1PCB-1232
<0.40 0.200.40 ug/L 10/13/17 09:13 10/20/17 11:48 1PCB-1242
<0.40 0.200.40 ug/L 10/13/17 09:13 10/20/17 11:48 1PCB-1248
<0.40 0.200.40 ug/L 10/13/17 09:13 10/20/17 11:48 1PCB-1254
<0.40 0.0700.40 ug/L 10/13/17 09:13 10/20/17 11:48 1PCB-1260
Tetrachloro-m-xylene 80 30-120 10/20/17 11:48 1
MB MB
Surrogate
10/13/17 09:13
Dil FacPreparedAnalyzedQualifierLimits%Recovery
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QC Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 500-405223/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 406209 Prep Batch: 405223
DCB Decachlorobiphenyl 104 30-140 10/20/17 11:48 1
MB MB
Surrogate
10/13/17 09:13
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-405223/4-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 406209 Prep Batch: 405223
PCB-1016 4.00 3.46 ug/L 86 56-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
PCB-1260 4.00 3.63 ug/L 91 53-137
Tetrachloro-m-xylene 30 -120
Surrogate
78
LCS LCS
Qualifier Limits%Recovery
100DCB Decachlorobiphenyl 30 -140
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 500-405223/5-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 406209 Prep Batch: 405223
PCB-1016 4.00 3.21 ug/L 80 56-120 8 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
PCB-1260 4.00 3.35 ug/L 84 53-137 8 20
Tetrachloro-m-xylene 30 -120
Surrogate
72
LCSD LCSD
Qualifier Limits%Recovery
97DCB Decachlorobiphenyl 30 -140
Method: 8151A - Herbicides (GC)
Client Sample ID: Method BlankLab Sample ID: MB 500-405080/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405510 Prep Batch: 405080
RL MDL
2,4-D <1.0 1.0 0.47 ug/L 10/12/17 11:12 10/16/17 16:53 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<2.0 0.162.0 ug/L 10/12/17 11:12 10/16/17 16:53 1Dinoseb
<0.50 0.0900.50 ug/L 10/12/17 11:12 10/16/17 16:53 1Pentachlorophenol
<1.0 0.291.0 ug/L 10/12/17 11:12 10/16/17 16:53 1Silvex (2,4,5-TP)
<1.0 0.431.0 ug/L 10/12/17 11:12 10/16/17 16:53 12,4,5-T
DCAA 45 25-130 10/16/17 16:53 1
MB MB
Surrogate
10/12/17 11:12
Dil FacPreparedAnalyzedQualifierLimits%Recovery
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QC Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 8151A - Herbicides (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-405080/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405510 Prep Batch: 405080
2,4-D 10.1 4.71 ug/L 47 30-115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Dinoseb 10.1 3.35 ug/L 33 30-110
Pentachlorophenol 2.53 1.01 ug/L 40 40-122
Silvex (2,4,5-TP)2.51 1.20 ug/L 48 32-115
2,4,5-T 2.53 1.21 ug/L 48 30-115
DCAA 25 -130
Surrogate
49
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 500-405080/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405510 Prep Batch: 405080
2,4-D 10.1 5.30 ug/L 53 30-115 12 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Dinoseb 10.1 3.89 ug/L 39 30-110 15 20
Pentachlorophenol 2.53 1.09 ug/L 43 40-122 8 20
Silvex (2,4,5-TP)2.51 1.37 ug/L 54 32-115 13 20
2,4,5-T 2.53 1.41 ug/L 56 30-115 15 20
DCAA 25 -130
Surrogate
56
LCSD LCSD
Qualifier Limits%Recovery
Method: 200.8 - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 500-405222/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405644 Prep Batch: 405222
RL MDL
Antimony <3.0 3.0 1.3 ug/L 10/13/17 08:45 10/16/17 19:08 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<1.0 0.151.0 ug/L 10/13/17 08:45 10/16/17 19:08 1Arsenic
0.531 J 0.372.5 ug/L 10/13/17 08:45 10/16/17 19:08 1Barium
<1.0 0.431.0 ug/L 10/13/17 08:45 10/16/17 19:08 1Beryllium
<0.50 0.150.50 ug/L 10/13/17 08:45 10/16/17 19:08 1Cadmium
<5.0 2.35.0 ug/L 10/13/17 08:45 10/16/17 19:08 1Chromium
<1.0 0.271.0 ug/L 10/13/17 08:45 10/16/17 19:08 1Cobalt
<100 38100 ug/L 10/13/17 08:45 10/16/17 19:08 1Iron
0.311 J 0.160.50 ug/L 10/13/17 08:45 10/16/17 19:08 1Lead
<2.5 1.12.5 ug/L 10/13/17 08:45 10/16/17 19:08 1Manganese
<2.0 0.922.0 ug/L 10/13/17 08:45 10/16/17 19:08 1Nickel
1.55 J ^1.12.5 ug/L 10/13/17 08:45 10/16/17 19:08 1Selenium
<0.50 0.0780.50 ug/L 10/13/17 08:45 10/16/17 19:08 1Silver
<2.0 0.652.0 ug/L 10/13/17 08:45 10/16/17 19:08 1Thallium
<10 4.210 ug/L 10/13/17 08:45 10/16/17 19:08 1Tin
14.1 J 8.120 ug/L 10/13/17 08:45 10/16/17 19:08 1Zinc
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QC Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 200.8 - Metals (ICP/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 500-405222/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405834 Prep Batch: 405222
RL MDL
Copper <2.0 2.0 0.63 ug/L 10/13/17 08:45 10/17/17 13:40 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<5.0 2.05.0 ug/L 10/13/17 08:45 10/17/17 13:40 1Vanadium
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-405222/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405644 Prep Batch: 405222
Antimony 500 530 ug/L 106 85-115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Arsenic 100 109 ug/L 109 85-115
Barium 500 551 ug/L 110 85-115
Beryllium 50.0 47.7 ug/L 95 85-115
Cadmium 50.0 53.2 ug/L 106 85-115
Chromium 200 203 ug/L 102 85-115
Cobalt 500 496 ug/L 99 85-115
Iron 1000 1130 ug/L 113 85-115
Lead 100 105 ug/L 105 85-115
Manganese 500 518 ug/L 104 85-115
Nickel 500 497 ug/L 99 85-115
Selenium 100 110 ^ug/L 110 85-115
Silver 50.0 53.0 ug/L 106 85-115
Thallium 100 107 ug/L 107 85-115
Tin 1000 1050 ug/L 105 85-115
Zinc 500 555 ug/L 111 85-115
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-405222/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405834 Prep Batch: 405222
Copper 250 267 ug/L 107 85-115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Vanadium 500 507 ug/L 101 85-115
Client Sample ID: MW-12 InfillLab Sample ID: 500-135505-4 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405644 Prep Batch: 405222
Antimony <3.0 500 529 ug/L 106 70-130
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Arsenic 0.19 J 100 106 ug/L 106 70-130
Barium 240 B 500 776 ug/L 107 70-130
Beryllium <1.0 50.0 45.1 ug/L 90 70-130
Cadmium <0.50 50.0 52.1 ug/L 104 70-130
Chromium 3.3 J 200 197 ug/L 97 70-130
Cobalt 8.7 500 475 ug/L 93 70-130
Iron 930 1000 1990 ug/L 106 70-130
Lead 0.85 B 100 105 ug/L 104 70-130
Manganese 340 V 500 833 ug/L 98 70-130
Nickel 11 500 471 ug/L 92 70-130
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QC Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 200.8 - Metals (ICP/MS) (Continued)
Client Sample ID: MW-12 InfillLab Sample ID: 500-135505-4 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405644 Prep Batch: 405222
Selenium <2.5 100 105 ug/L 105 70-130
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Silver <0.50 50.0 52.1 ug/L 104 70-130
Thallium <2.0 100 109 ug/L 109 70-130
Tin <10 1000 1050 ug/L 105 70-130
Zinc 26 B 500 527 ug/L 100 70-130
Client Sample ID: MW-12 InfillLab Sample ID: 500-135505-4 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405834 Prep Batch: 405222
Copper 4.7 250 263 ug/L 103 70-130
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Vanadium 2.3 J 500 500 ug/L 100 70-130
Client Sample ID: MW-12 InfillLab Sample ID: 500-135505-4 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405644 Prep Batch: 405222
Antimony <3.0 <3.0 ug/L NC 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Arsenic 0.19 J 0.200 J ug/L 6 20
Barium 240 B 239 ug/L 1 20
Beryllium <1.0 <1.0 ug/L NC 20
Cadmium <0.50 <0.50 ug/L NC 20
Chromium 3.3 J 2.55 J F5 ug/L 26 20
Cobalt 8.7 8.52 ug/L 2 20
Iron 930 854 ug/L 8 20
Lead 0.85 B 0.380 J F5 ug/L 76 20
Manganese 340 V 340 ug/L 0.4 20
Nickel 11 10.7 ug/L 6 20
Selenium <2.5 <2.5 ug/L NC 20
Silver <0.50 <0.50 ug/L NC 20
Thallium <2.0 <2.0 ug/L NC 20
Tin <10 <10 ug/L NC 20
Zinc 26 B <20 ug/L NC 20
Client Sample ID: MW-12 InfillLab Sample ID: 500-135505-4 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405834 Prep Batch: 405222
Copper 4.7 4.13 ug/L 14 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Vanadium 2.3 J 2.24 J ug/L 0.9 20
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QC Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 200.8 - Metals (ICP/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 500-405247/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405553 Prep Batch: 405247
RL MDL
Antimony <3.0 3.0 1.3 ug/L 10/13/17 11:30 10/16/17 11:47 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<1.0 0.151.0 ug/L 10/13/17 11:30 10/16/17 11:47 1Arsenic
<2.5 0.372.5 ug/L 10/13/17 11:30 10/16/17 11:47 1Barium
<0.50 0.150.50 ug/L 10/13/17 11:30 10/16/17 11:47 1Cadmium
<5.0 2.35.0 ug/L 10/13/17 11:30 10/16/17 11:47 1Chromium
<2.0 0.632.0 ug/L 10/13/17 11:30 10/16/17 11:47 1Copper
<0.50 0.160.50 ug/L 10/13/17 11:30 10/16/17 11:47 1Lead
<2.5 1.12.5 ug/L 10/13/17 11:30 10/16/17 11:47 1Selenium
<0.50 0.0780.50 ug/L 10/13/17 11:30 10/16/17 11:47 1Silver
<2.0 0.652.0 ug/L 10/13/17 11:30 10/16/17 11:47 1Thallium
<20 8.120 ug/L 10/13/17 11:30 10/16/17 11:47 1Zinc
Client Sample ID: Method BlankLab Sample ID: MB 500-405247/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405643 Prep Batch: 405247
RL MDL
Beryllium <1.0 1.0 0.43 ug/L 10/13/17 11:30 10/16/17 23:14 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<1.0 0.271.0 ug/L 10/13/17 11:30 10/16/17 23:14 1Cobalt
<100 38100 ug/L 10/13/17 11:30 10/16/17 23:14 1Iron
<2.5 1.12.5 ug/L 10/13/17 11:30 10/16/17 23:14 1Manganese
<2.0 0.922.0 ug/L 10/13/17 11:30 10/16/17 23:14 1Nickel
<5.0 2.05.0 ug/L 10/13/17 11:30 10/16/17 23:14 1Vanadium
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-405247/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405553 Prep Batch: 405247
Antimony 500 507 ug/L 101 85-115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Arsenic 100 105 ug/L 105 85-115
Barium 500 552 ug/L 110 85-115
Cadmium 50.0 52.4 ug/L 105 85-115
Chromium 200 212 ug/L 106 85-115
Copper 250 281 ug/L 112 85-115
Lead 100 106 ug/L 106 85-115
Selenium 100 104 ug/L 104 85-115
Silver 50.0 53.1 ug/L 106 85-115
Thallium 100 107 ug/L 107 85-115
Zinc 500 569 ug/L 114 85-115
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-405247/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405643 Prep Batch: 405247
Beryllium 50.0 50.6 ug/L 101 85-115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Cobalt 500 517 ug/L 103 85-115
Iron 1000 1070 ug/L 107 85-115
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QC Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 200.8 - Metals (ICP/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-405247/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405643 Prep Batch: 405247
Manganese 500 525 ug/L 105 85-115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Nickel 500 529 ug/L 106 85-115
Vanadium 500 506 ug/L 101 85-115
Method: 245.1 - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 500-405904/12-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 406044 Prep Batch: 405904
RL MDL
Mercury <0.20 0.20 0.091 ug/L 10/18/17 15:35 10/19/17 10:37 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-405904/13-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 406044 Prep Batch: 405904
Mercury 2.00 1.90 ug/L 95 85-115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: MW-14 InfillLab Sample ID: 500-135505-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 406044 Prep Batch: 405904
Mercury <0.20 1.00 0.962 ug/L 96 70-130
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: MW-14 InfillLab Sample ID: 500-135505-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 406044 Prep Batch: 405904
Mercury <0.20 <0.20 ug/L NC 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Method: 9014 - Cyanide
Client Sample ID: Method BlankLab Sample ID: MB 500-406103/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 406574 Prep Batch: 406103
RL MDL
Cyanide, Total <0.010 0.010 0.0035 mg/L 10/19/17 18:27 10/20/17 16:40 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-406103/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 406574 Prep Batch: 406103
Cyanide, Total 0.100 0.0927 mg/L 93 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
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QC Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 9014 - Cyanide (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 500-406665/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 406763 Prep Batch: 406665
RL MDL
Cyanide, Total <0.010 0.010 0.0035 mg/L 10/24/17 12:00 10/24/17 15:00 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-406665/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 406763 Prep Batch: 406665
Cyanide, Total 0.100 0.0895 mg/L 90 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Method: 9056A - Anions, Ion Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 500-407493/23
Matrix: Water Prep Type: Total/NA
Analysis Batch: 407493
RL MDL
Chloride <0.20 0.20 0.17 mg/L 10/28/17 12:16 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.20 0.0950.20 mg/L 10/28/17 12:16 1Sulfate
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-407493/34
Matrix: Water Prep Type: Total/NA
Analysis Batch: 407493
Chloride 3.00 3.00 mg/L 100 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Sulfate 5.00 5.00 mg/L 100 80-120
Client Sample ID: MW-1 InfillLab Sample ID: 500-135505-8 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 407493
Chloride 21 5.00 24.4 4 mg/L 64 80-120
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Sulfate 13 12.5 26.8 mg/L 108 80-120
Client Sample ID: MW-1 InfillLab Sample ID: 500-135505-8 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 407493
Chloride 21 5.00 24.5 4 mg/L 65 80-120 0 15
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Sulfate 13 12.5 27.1 mg/L 110 80-120 1 15
Client Sample ID: Method BlankLab Sample ID: MB 500-407616/23
Matrix: Water Prep Type: Total/NA
Analysis Batch: 407616
RL MDL
Chloride <0.20 0.20 0.17 mg/L 10/30/17 00:17 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
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QC Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: 9056A - Anions, Ion Chromatography (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 500-407616/23
Matrix: Water Prep Type: Total/NA
Analysis Batch: 407616
RL MDL
Sulfate <0.20 0.20 0.095 mg/L 10/30/17 00:17 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-407616/29
Matrix: Water Prep Type: Total/NA
Analysis Batch: 407616
Chloride 3.00 2.95 mg/L 98 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Sulfate 5.00 4.96 mg/L 99 80-120
Client Sample ID: MW-14 InfillLab Sample ID: 500-135505-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 407616
Sulfate 9.9 5.00 15.7 mg/L 117 80-120
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: MW-14 InfillLab Sample ID: 500-135505-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 407616
Sulfate 9.9 5.00 15.7 mg/L 117 80-120 0 15
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Method: SM 2320B - Alkalinity
Client Sample ID: Method BlankLab Sample ID: MB 500-406172/28
Matrix: Water Prep Type: Total/NA
Analysis Batch: 406172
RL MDL
Alkalinity <5.0 5.0 3.7 mg/L 10/19/17 13:46 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-406172/29
Matrix: Water Prep Type: Total/NA
Analysis Batch: 406172
Alkalinity 100 105 mg/L 105 85-115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: MW-14 InfillLab Sample ID: 500-135505-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 406172
Alkalinity 65 63.6 mg/L 3 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
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QC Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: SM 2320B - Alkalinity (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 500-406877/28
Matrix: Water Prep Type: Total/NA
Analysis Batch: 406877
RL MDL
Alkalinity <5.0 5.0 3.7 mg/L 10/24/17 14:55 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Method BlankLab Sample ID: MB 500-406877/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 406877
RL MDL
Alkalinity <5.0 5.0 3.7 mg/L 10/24/17 11:38 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-406877/29
Matrix: Water Prep Type: Total/NA
Analysis Batch: 406877
Alkalinity 100 107 mg/L 107 85-115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-406877/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 406877
Alkalinity 100 104 mg/L 104 85-115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Method: SM 2540C - Solids, Total Dissolved (TDS)
Client Sample ID: Method BlankLab Sample ID: MB 500-405177/1
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405177
RL MDL
Total Dissolved Solids <10 10 4.3 mg/L 10/13/17 05:25 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-405177/2
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405177
Total Dissolved Solids 250 260 mg/L 104 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Method BlankLab Sample ID: MB 500-405423/1
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405423
RL MDL
Total Dissolved Solids <10 10 4.3 mg/L 10/16/17 04:13 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
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QC Sample Results
TestAmerica Job ID: 500-135505-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill
Method: SM 2540C - Solids, Total Dissolved (TDS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-405423/2
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405423
Total Dissolved Solids 250 262 mg/L 105 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: MW-8D NMLFLab Sample ID: 500-135505-11 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 405423
Total Dissolved Solids 570 570 mg/L 0.4 5
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
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Lab Chronicle
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-135505-1
Project/Site: NC North Mecklenburg Landfill
Client Sample ID: MW-14 Infill Lab Sample ID: 500-135505-1
Matrix: WaterDate Collected: 10/11/17 16:10
Date Received: 10/12/17 10:00
Analysis 8260B 10/18/17 16:22 EMA1405855 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3510C 405441 10/16/17 07:32 BSO TAL CHITotal/NA
Analysis 8270D 1 405883 10/18/17 22:37 GES TAL CHITotal/NA
Prep 3510C 405223 10/13/17 09:13 BSO TAL CHITotal/NA
Analysis 8081B 1 405522 10/16/17 16:01 PJG TAL CHITotal/NA
Prep 3510C 405223 10/13/17 09:13 BSO TAL CHITotal/NA
Analysis 8082A 1 406209 10/20/17 13:09 BJH TAL CHITotal/NA
Prep 8151A 405080 10/12/17 11:45 BSO TAL CHITotal/NA
Analysis 8151A 1 405510 10/16/17 18:30 JBJ TAL CHITotal/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405834 10/17/17 15:13 FXG TAL CHITotal/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405644 10/16/17 20:38 FXG TAL CHITotal/NA
Prep 245.1 405904 10/18/17 15:35 EEN TAL CHITotal/NA
Analysis 245.1 1 406044 10/19/17 10:51 EEN TAL CHITotal/NA
Prep 9010B 406103 10/19/17 18:27 MAN TAL CHITotal/NA
Analysis 9014 1 406574 MAN TAL CHITotal/NA
10/20/17 16:46
10/20/17 16:47
(Start)
(End)
Analysis 9056A 1 407493 10/28/17 13:20 EAT TAL CHITotal/NA
Analysis 9056A 2 407616 10/30/17 04:43 PMF TAL CHITotal/NA
Analysis SM 2320B 1 406172 10/19/17 15:35 SMO TAL CHITotal/NA
Analysis SM 2540C 1 405177 10/13/17 05:56 CLB TAL CHITotal/NA
Client Sample ID: MW-8 Infill Lab Sample ID: 500-135505-2
Matrix: WaterDate Collected: 10/11/17 15:00
Date Received: 10/12/17 10:00
Analysis 8260B 10/18/17 16:48 EMA1405855 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3510C 405441 10/16/17 07:32 BSO TAL CHITotal/NA
Analysis 8270D 1 405883 10/18/17 23:06 GES TAL CHITotal/NA
Prep 3510C 405223 10/13/17 09:13 BSO TAL CHITotal/NA
Analysis 8081B 1 405522 10/16/17 16:20 PJG TAL CHITotal/NA
Prep 3510C 405223 10/13/17 09:13 BSO TAL CHITotal/NA
Analysis 8082A 1 406209 10/20/17 13:25 BJH TAL CHITotal/NA
Prep 8151A 405080 10/12/17 11:45 BSO TAL CHITotal/NA
Analysis 8151A 1 405510 10/16/17 18:55 JBJ TAL CHITotal/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405834 10/17/17 15:18 FXG TAL CHITotal/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405644 10/16/17 20:42 FXG TAL CHITotal/NA
Prep 245.1 405904 10/18/17 15:35 EEN TAL CHITotal/NA
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Lab Chronicle
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-135505-1
Project/Site: NC North Mecklenburg Landfill
Client Sample ID: MW-8 Infill Lab Sample ID: 500-135505-2
Matrix: WaterDate Collected: 10/11/17 15:00
Date Received: 10/12/17 10:00
Analysis 245.1 10/19/17 10:56 EEN1406044 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 9010B 406665 10/24/17 12:00 MAN TAL CHITotal/NA
Analysis 9014 1 406763 MAN TAL CHITotal/NA
10/24/17 15:02
10/24/17 15:02
(Start)
(End)
Analysis 9056A 1 407493 10/28/17 13:32 EAT TAL CHITotal/NA
Analysis 9056A 25 407493 10/28/17 13:45 EAT TAL CHITotal/NA
Analysis SM 2320B 1 406172 10/19/17 15:50 SMO TAL CHITotal/NA
Analysis SM 2540C 1 405177 10/13/17 05:58 CLB TAL CHITotal/NA
Client Sample ID: Duplicate 2 Lab Sample ID: 500-135505-3
Matrix: WaterDate Collected: 10/11/17 13:15
Date Received: 10/12/17 10:00
Analysis 8260B 10/18/17 17:14 EMA1405855 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: MW-12 Infill Lab Sample ID: 500-135505-4
Matrix: WaterDate Collected: 10/11/17 13:15
Date Received: 10/12/17 10:00
Analysis 8260B 10/18/17 17:40 EMA1405855 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3510C 405441 10/16/17 07:32 BSO TAL CHITotal/NA
Analysis 8270D 1 405883 10/18/17 23:35 GES TAL CHITotal/NA
Prep 3510C 405223 10/13/17 09:13 BSO TAL CHITotal/NA
Analysis 8081B 1 405522 10/16/17 16:39 PJG TAL CHITotal/NA
Prep 3510C 405223 10/13/17 09:13 BSO TAL CHITotal/NA
Analysis 8082A 1 406209 10/20/17 13:42 BJH TAL CHITotal/NA
Prep 8151A 405080 10/12/17 11:45 BSO TAL CHITotal/NA
Analysis 8151A 1 405510 10/16/17 19:19 JBJ TAL CHITotal/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405834 10/17/17 15:32 FXG TAL CHITotal/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405644 10/16/17 20:46 FXG TAL CHITotal/NA
Prep 245.1 405904 10/18/17 15:35 EEN TAL CHITotal/NA
Analysis 245.1 1 406044 10/19/17 10:57 EEN TAL CHITotal/NA
Prep 9010B 406665 10/24/17 12:00 MAN TAL CHITotal/NA
Analysis 9014 1 406763 MAN TAL CHITotal/NA
10/24/17 15:02
10/24/17 15:03
(Start)
(End)
Analysis 9056A 10 407493 10/28/17 13:58 EAT TAL CHITotal/NA
Analysis SM 2320B 1 406172 10/19/17 15:59 SMO TAL CHITotal/NA
TestAmerica Chicago
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Lab Chronicle
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-135505-1
Project/Site: NC North Mecklenburg Landfill
Client Sample ID: MW-12 Infill Lab Sample ID: 500-135505-4
Matrix: WaterDate Collected: 10/11/17 13:15
Date Received: 10/12/17 10:00
Analysis SM 2540C 10/13/17 06:01 CLB1405177 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: MW-12D Infill Lab Sample ID: 500-135505-5
Matrix: WaterDate Collected: 10/11/17 12:30
Date Received: 10/12/17 10:00
Analysis 8260B 10/18/17 18:06 EMA1405855 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3510C 405441 10/16/17 07:32 BSO TAL CHITotal/NA
Analysis 8270D 1 405883 10/19/17 00:04 GES TAL CHITotal/NA
Prep 3510C 405223 10/13/17 09:13 BSO TAL CHITotal/NA
Analysis 8081B 1 405522 10/16/17 16:58 PJG TAL CHITotal/NA
Prep 3510C 405223 10/13/17 09:13 BSO TAL CHITotal/NA
Analysis 8082A 1 406209 10/20/17 13:58 BJH TAL CHITotal/NA
Prep 8151A 405080 10/12/17 11:45 BSO TAL CHITotal/NA
Analysis 8151A 1 405510 10/16/17 19:43 JBJ TAL CHITotal/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405834 10/17/17 15:51 FXG TAL CHITotal/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405644 10/16/17 21:01 FXG TAL CHITotal/NA
Prep 245.1 405904 10/18/17 15:35 EEN TAL CHITotal/NA
Analysis 245.1 1 406044 10/19/17 10:59 EEN TAL CHITotal/NA
Prep 9010B 406665 10/24/17 12:00 MAN TAL CHITotal/NA
Analysis 9014 1 406763 MAN TAL CHITotal/NA
10/24/17 15:03
10/24/17 15:03
(Start)
(End)
Analysis 9056A 10 407493 10/28/17 14:10 EAT TAL CHITotal/NA
Analysis SM 2320B 1 406172 10/19/17 16:08 SMO TAL CHITotal/NA
Analysis SM 2540C 1 405177 10/13/17 06:03 CLB TAL CHITotal/NA
Client Sample ID: Infill Duplicate 1 Lab Sample ID: 500-135505-6
Matrix: WaterDate Collected: 10/11/17 12:30
Date Received: 10/12/17 10:00
Analysis 8260B 10/18/17 18:33 EMA1405855 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: MW-7D Infill Lab Sample ID: 500-135505-7
Matrix: WaterDate Collected: 10/11/17 14:40
Date Received: 10/12/17 10:00
Analysis 8260B 10/18/17 19:00 EMA1405855 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
TestAmerica Chicago
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Lab Chronicle
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-135505-1
Project/Site: NC North Mecklenburg Landfill
Prep 3510C 10/16/17 07:32 BSO405441 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270D 1 405883 10/19/17 00:33 GES TAL CHITotal/NA
Prep 3510C 405223 10/13/17 09:13 BSO TAL CHITotal/NA
Analysis 8081B 1 405675 10/17/17 13:47 PJG TAL CHITotal/NA
Prep 3510C 405223 10/13/17 09:13 BSO TAL CHITotal/NA
Analysis 8082A 1 406209 10/20/17 14:14 BJH TAL CHITotal/NA
Prep 8151A 405080 10/12/17 11:45 BSO TAL CHITotal/NA
Analysis 8151A 1 405510 10/16/17 20:08 JBJ TAL CHITotal/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405834 10/17/17 15:55 FXG TAL CHITotal/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405644 10/16/17 21:05 FXG TAL CHITotal/NA
Prep 245.1 405904 10/18/17 15:35 EEN TAL CHITotal/NA
Analysis 245.1 1 406044 10/19/17 11:00 EEN TAL CHITotal/NA
Prep 9010B 406665 10/24/17 12:00 MAN TAL CHITotal/NA
Analysis 9014 1 406763 MAN TAL CHITotal/NA
10/24/17 15:03
10/24/17 15:03
(Start)
(End)
Analysis 9056A 25 407493 10/28/17 14:48 EAT TAL CHITotal/NA
Analysis SM 2320B 1 406172 10/19/17 16:19 SMO TAL CHITotal/NA
Analysis SM 2540C 1 405177 10/13/17 06:06 CLB TAL CHITotal/NA
Client Sample ID: MW-1 Infill Lab Sample ID: 500-135505-8
Matrix: WaterDate Collected: 10/11/17 15:40
Date Received: 10/12/17 10:00
Analysis 8260B 10/18/17 19:25 EMA1405855 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3510C 405441 10/16/17 07:32 BSO TAL CHITotal/NA
Analysis 8270D 1 406153 10/20/17 19:40 WDS TAL CHITotal/NA
Prep 3510C 405223 10/13/17 09:13 BSO TAL CHITotal/NA
Analysis 8081B 1 405675 10/17/17 14:06 PJG TAL CHITotal/NA
Prep 3510C 405223 10/13/17 09:13 BSO TAL CHITotal/NA
Analysis 8082A 1 406209 10/20/17 14:30 BJH TAL CHITotal/NA
Prep 8151A 405080 10/12/17 11:45 BSO TAL CHITotal/NA
Analysis 8151A 1 405636 10/18/17 01:28 JBJ TAL CHITotal/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405834 10/17/17 16:00 FXG TAL CHITotal/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405644 10/16/17 21:09 FXG TAL CHITotal/NA
Prep 245.1 405904 10/18/17 15:35 EEN TAL CHITotal/NA
Analysis 245.1 1 406044 10/19/17 11:02 EEN TAL CHITotal/NA
Prep 9010B 406665 10/24/17 12:00 MAN TAL CHITotal/NA
Analysis 9014 1 406763 MAN TAL CHITotal/NA
10/24/17 15:04
10/24/17 15:04
(Start)
(End)
Analysis 9056A 5 407493 10/28/17 15:14 EAT TAL CHITotal/NA
Analysis SM 2320B 1 406172 10/19/17 16:25 SMO TAL CHITotal/NA
TestAmerica Chicago
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Lab Chronicle
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-135505-1
Project/Site: NC North Mecklenburg Landfill
Analysis SM 2540C 10/13/17 06:08 CLB1405177 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: TB Lab Sample ID: 500-135505-9
Matrix: WaterDate Collected: 10/11/17 00:00
Date Received: 10/12/17 10:00
Analysis 8260B 10/18/17 19:52 EMA1405855 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: MW-8 NMLF Lab Sample ID: 500-135505-10
Matrix: WaterDate Collected: 10/11/17 10:40
Date Received: 10/12/17 10:00
Analysis 8260B 10/18/17 20:19 EMA1405855 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405834 10/17/17 16:04 FXG TAL CHITotal/NA
Prep 200.8 405222 10/13/17 08:45 LWN TAL CHITotal/NA
Analysis 200.8 1 405644 10/16/17 21:13 FXG TAL CHITotal/NA
Prep 245.1 405904 10/18/17 15:35 EEN TAL CHITotal/NA
Analysis 245.1 1 406044 10/19/17 11:06 EEN TAL CHITotal/NA
Analysis 9056A 5 407493 10/28/17 15:52 EAT TAL CHITotal/NA
Analysis SM 2320B 1 406172 10/19/17 16:32 SMO TAL CHITotal/NA
Analysis SM 2540C 1 405177 10/13/17 06:11 CLB TAL CHITotal/NA
Client Sample ID: MW-8D NMLF Lab Sample ID: 500-135505-11
Matrix: WaterDate Collected: 10/11/17 10:10
Date Received: 10/12/17 10:00
Analysis 8260B 10/18/17 20:45 EMA1405855 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 405247 10/13/17 11:30 LWN TAL CHITotal/NA
Analysis 200.8 1 405643 10/16/17 23:23 FXG TAL CHITotal/NA
Prep 200.8 405247 10/13/17 11:30 LWN TAL CHITotal/NA
Analysis 200.8 1 405553 10/16/17 12:11 FXG TAL CHITotal/NA
Prep 245.1 405904 10/18/17 15:35 EEN TAL CHITotal/NA
Analysis 245.1 1 406044 10/19/17 11:08 EEN TAL CHITotal/NA
Analysis 9056A 2 407493 10/28/17 16:17 EAT TAL CHITotal/NA
Analysis 9056A 25 407493 10/28/17 16:30 EAT TAL CHITotal/NA
Analysis SM 2320B 1 406877 10/24/17 16:17 SMO TAL CHITotal/NA
Analysis SM 2540C 1 405423 10/16/17 04:25 CLB TAL CHITotal/NA
TestAmerica Chicago
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Lab Chronicle
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-135505-1
Project/Site: NC North Mecklenburg Landfill
Client Sample ID: MW-10D NMLF Lab Sample ID: 500-135505-12
Matrix: WaterDate Collected: 10/11/17 11:25
Date Received: 10/12/17 10:00
Analysis 8260B 10/16/17 22:51 DJD1405489 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 405247 10/13/17 11:30 LWN TAL CHITotal/NA
Analysis 200.8 1 405643 10/16/17 23:28 FXG TAL CHITotal/NA
Prep 200.8 405247 10/13/17 11:30 LWN TAL CHITotal/NA
Analysis 200.8 20 405834 10/17/17 13:21 FXG TAL CHITotal/NA
Prep 200.8 405247 10/13/17 11:30 LWN TAL CHITotal/NA
Analysis 200.8 1 405553 10/16/17 12:15 FXG TAL CHITotal/NA
Prep 245.1 405904 10/18/17 15:35 EEN TAL CHITotal/NA
Analysis 245.1 1 406044 10/19/17 11:09 EEN TAL CHITotal/NA
Analysis 9056A 50 407493 10/28/17 16:42 EAT TAL CHITotal/NA
Analysis SM 2320B 1 406877 10/24/17 13:50 SMO TAL CHITotal/NA
Analysis SM 2540C 1 405423 10/16/17 04:31 CLB TAL CHITotal/NA
Client Sample ID: MW-11 NMLF Lab Sample ID: 500-135505-13
Matrix: WaterDate Collected: 10/11/17 12:25
Date Received: 10/12/17 10:00
Analysis 8260B 10/18/17 21:11 EMA1405855 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 405247 10/13/17 11:30 LWN TAL CHITotal/NA
Analysis 200.8 1 405643 10/16/17 23:32 FXG TAL CHITotal/NA
Prep 200.8 405247 10/13/17 11:30 LWN TAL CHITotal/NA
Analysis 200.8 1 405553 10/16/17 12:19 FXG TAL CHITotal/NA
Prep 245.1 405904 10/18/17 15:35 EEN TAL CHITotal/NA
Analysis 245.1 1 406044 10/19/17 11:10 EEN TAL CHITotal/NA
Analysis 9056A 10 407493 10/28/17 17:21 EAT TAL CHITotal/NA
Analysis 9056A 25 407493 10/28/17 17:33 EAT TAL CHITotal/NA
Analysis SM 2320B 1 406877 10/24/17 16:30 SMO TAL CHITotal/NA
Analysis SM 2540C 1 405423 10/16/17 04:33 CLB TAL CHITotal/NA
Client Sample ID: MW-10 Infill Lab Sample ID: 500-135505-14
Matrix: WaterDate Collected: 10/11/17 13:45
Date Received: 10/12/17 10:00
Analysis 8260B 10/18/17 21:37 EMA1405855 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Laboratory References:
TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL [phone]
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Accreditation/Certification Summary
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-135505-1
Project/Site: NC North Mecklenburg Landfill
Laboratory: TestAmerica Chicago
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program EPA Region Identification Number Expiration Date
North Carolina (WW/SW)2914State Program 12-31-17 *
Analysis Method Prep Method Matrix Analyte
The following analytes are included in this report, but accreditation/certification is not offered by the governing authority:
8260B Water trans-1,4-Dichloro-2-butene
8270D 3510C Water 2,3,7,8-TCDD (Screen)
TestAmerica Chicago
* Accreditation/Certification renewal pending - accreditation/certification considered valid.
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Login Sample Receipt Checklist
Client: Civil & Environmental Consultants Inc Job Number: 500-135505-1
Login Number: 135505
Question Answer Comment
Creator: Scott, Sherri L
List Source: TestAmerica Chicago
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.5.9.5.8,0.5,1.8
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
FalseThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Chicago
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ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Chicago
2417 Bond Street
University Park, IL 60484
Tel: [phone]
TestAmerica Job ID: 500-136658-1
Client Project/Site: NC North Mecklenburg Landfill (Closed)
For:
Civil & Environmental Consultants Inc
1900 Center Park Drive
Suite A
Charlotte, North Carolina 28217
Attn: Mr. Ed Stephens
Authorized for release by:
11/16/2017 12:05:45 PM
Robin Kintz, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill (Closed)
TestAmerica Job ID: 500-136658-1
Page 2 of 28 TestAmerica Chicago11/16/2017
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .14
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .16
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .17
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .24
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .26
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .27
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .28
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Case Narrative
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-136658-1
Project/Site: NC North Mecklenburg Landfill (Closed)
Job ID: 500-136658-1
Laboratory: TestAmerica Chicago
Narrative
Job Narrative
500-136658-1
Comments
No additional comments.
Receipt
The samples were received on 11/2/2017 9:00 AM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was -0.9º C.
GC/MS VOA
Method(s) 8260B: The method blank for preparation batch 409675 contained Methylene Chloride above the reporting limit (RL). None of
the samples associated with this method blank contained the target compound; therefore, re-analysis of samples were not performed.
Method(s) 8260B: The following analytes recovered outside control limits for the LCS associated with batch 409675: Methylene Chloride
and trans-1,4-Dichloro-2-butene. This is not indicative of a systematic control problem because these were random marginal
exceedances. Qualified results have been reported.
Method(s) 8260B: The following sample detected Acetone above the reporting limit: Hammill Well (500-136658-3). The method blank
409675 associated with the sample did not detect Acetone. Since Acetone is a known lab contaminant and the results are just above the
reporting limit; the results have been flagged with a "cn" flag to denote the suspected lab contamination.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
General Chemistry
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
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Detection Summary
TestAmerica Job ID: 500-136658-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill (Closed)
Client Sample ID: Tinsley Well Lab Sample ID: 500-136658-1
Bromodichloromethane
RL
1.0 ug/L
MDL
0.37
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1148260B
Bromoform 1.0 ug/L0.48 Total/NA10.78 J 8260B
Chloroform 2.0 ug/L0.37 Total/NA1428260B
Dibromochloromethane 1.0 ug/L0.49 Total/NA16.9 8260B
Arsenic 1.0 ug/L0.15 Total/NA10.19 J 200.8
Barium 2.5 ug/L0.37 Total/NA110200.8
Copper 2.0 ug/L0.63 Total/NA14.1 200.8
Manganese 2.5 ug/L1.1 Total/NA11.6 J 200.8
Chloride 2.0 mg/L1.7 Total/NA1035F19056A
Sulfate 2.0 mg/L0.95 Total/NA1031F19056A
Alkalinity 5.0 mg/L3.7 Total/NA123SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA166SM 2540C
Client Sample ID: Gilkerson Well Lab Sample ID: 500-136658-2
Bromodichloromethane
RL
1.0 ug/L
MDL
0.37
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1148260B
Chloroform 2.0 ug/L0.37 Total/NA1418260B
Dibromochloromethane 1.0 ug/L0.49 Total/NA17.6 8260B
Arsenic 1.0 ug/L0.15 Total/NA10.15 J 200.8
Barium 2.5 ug/L0.37 Total/NA112200.8
Copper 2.0 ug/L0.63 Total/NA118200.8
Iron 100 ug/L38 Total/NA1660200.8
Lead 0.50 ug/L0.16 Total/NA15.0 200.8
Manganese 2.5 ug/L1.1 Total/NA116200.8
Zinc 20 ug/L8.1 Total/NA132200.8
Mercury 0.20 ug/L0.091 Total/NA10.29 245.1
Chloride 0.40 mg/L0.34 Total/NA29.5 9056A
Sulfate 0.40 mg/L0.19 Total/NA28.9 9056A
Alkalinity 5.0 mg/L3.7 Total/NA121SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA162SM 2540C
Client Sample ID: Hammill Well Lab Sample ID: 500-136658-3
2-Butanone (MEK)
RL
5.0 ug/L
MDL
2.1
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1228260B
Acetone 5.0 ug/L1.7 Total/NA16.5 cn 8260B
Tetrahydrofuran 10 ug/L1.9 Total/NA12308260B
Arsenic 1.0 ug/L0.15 Total/NA10.47 J 200.8
Barium 2.5 ug/L0.37 Total/NA141200.8
Copper 2.0 ug/L0.63 Total/NA14.3 200.8
Iron 100 ug/L38 Total/NA1290200.8
Lead 0.50 ug/L0.16 Total/NA10.28 J 200.8
Manganese 2.5 ug/L1.1 Total/NA160200.8
Nickel 2.0 ug/L0.92 Total/NA10.95 J 200.8
Zinc 20 ug/L8.1 Total/NA1490200.8
Chloride 0.40 mg/L0.34 Total/NA25.6 9056A
Sulfate 10 mg/L4.8 Total/NA503209056A
Alkalinity 5.0 mg/L3.7 Total/NA195SM 2320B
Total Dissolved Solids 10 mg/L4.3 Total/NA1600SM 2540C
TestAmerica Chicago
This Detection Summary does not include radiochemical test results.
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Method Summary
TestAmerica Job ID: 500-136658-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill (Closed)
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL CHI
EPA200.8 Metals (ICP/MS)TAL CHI
EPA245.1 Mercury (CVAA)TAL CHI
SW8469056AAnions, Ion Chromatography TAL CHI
SMSM 2320B Alkalinity TAL CHI
SMSM 2540C Solids, Total Dissolved (TDS)TAL CHI
Protocol References:
EPA = US Environmental Protection Agency
SM = "Standard Methods For The Examination Of Water And Wastewater",
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL [phone]
TestAmerica Chicago
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Sample Summary
TestAmerica Job ID: 500-136658-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill (Closed)
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
500-136658-1 Tinsley Well Water 10/31/17 13:45 11/02/17 09:00
500-136658-2 Gilkerson Well Water 10/31/17 14:00 11/02/17 09:00
500-136658-3 Hammill Well Water 10/31/17 14:15 11/02/17 09:00
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Client Sample Results
TestAmerica Job ID: 500-136658-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill (Closed)
Lab Sample ID: 500-136658-1Client Sample ID: Tinsley Well
Matrix: WaterDate Collected: 10/31/17 13:45
Date Received: 11/02/17 09:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 11/13/17 14:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 11/13/17 14:32 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 11/13/17 14:32 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 11/13/17 14:32 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 11/13/17 14:32 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 11/13/17 14:32 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 11/13/17 14:32 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 11/13/17 14:32 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 11/13/17 14:32 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 11/13/17 14:32 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 11/13/17 14:32 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 11/13/17 14:32 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 11/13/17 14:32 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 11/13/17 14:32 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 11/13/17 14:32 12-Hexanone <5.0
5.0 2.2 ug/L 11/13/17 14:32 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 11/13/17 14:32 1Acetone<5.0
20 4.5 ug/L 11/13/17 14:32 1Acrylonitrile<20
0.50 0.15 ug/L 11/13/17 14:32 1Benzene<0.50
1.0 0.43 ug/L 11/13/17 14:32 1Bromochloromethane<1.0
1.0 0.37 ug/L 11/13/17 14:32 1Bromodichloromethane14
1.0 0.48 ug/L 11/13/17 14:32 1Bromoform0.78 J
2.0 0.80 ug/L 11/13/17 14:32 1Bromomethane<2.0
2.0 0.45 ug/L 11/13/17 14:32 1Carbon disulfide <2.0
1.0 0.38 ug/L 11/13/17 14:32 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 11/13/17 14:32 1Chlorobenzene<1.0
1.0 0.51 ug/L 11/13/17 14:32 1Chloroethane<1.0
2.0 0.37 ug/L 11/13/17 14:32 1Chloroform42
1.0 0.32 ug/L 11/13/17 14:32 1Chloromethane<1.0
1.0 0.41 ug/L 11/13/17 14:32 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 11/13/17 14:32 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 11/13/17 14:32 1Dibromochloromethane6.9
1.0 0.27 ug/L 11/13/17 14:32 1Dibromomethane<1.0
0.50 0.18 ug/L 11/13/17 14:32 1Ethylbenzene<0.50
2.5 0.66 ug/L 11/13/17 14:32 1Iodomethane<2.5
5.0 1.6 ug/L 11/13/17 14:32 1Methylene Chloride <5.0 *
1.0 0.39 ug/L 11/13/17 14:32 1Styrene<1.0
1.0 0.37 ug/L 11/13/17 14:32 1Tetrachloroethene<1.0
10 1.9 ug/L 11/13/17 14:32 1Tetrahydrofuran<10
0.50 0.15 ug/L 11/13/17 14:32 1Toluene<0.50
1.0 0.35 ug/L 11/13/17 14:32 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 11/13/17 14:32 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 11/13/17 14:32 1trans-1,4-Dichloro-2-butene <5.0 *
0.50 0.16 ug/L 11/13/17 14:32 1Trichloroethene<0.50
1.0 0.43 ug/L 11/13/17 14:32 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 11/13/17 14:32 1Vinyl acetate <2.0
0.50 0.20 ug/L 11/13/17 14:32 1Vinyl chloride <0.50
1.0 0.22 ug/L 11/13/17 14:32 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-136658-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill (Closed)
Lab Sample ID: 500-136658-1Client Sample ID: Tinsley Well
Matrix: WaterDate Collected: 10/31/17 13:45
Date Received: 11/02/17 09:00
1,2-Dichloroethane-d4 (Surr)86 75-126 11/13/17 14:32 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)85 11/13/17 14:32 172-124
Dibromofluoromethane 92 11/13/17 14:32 175-120
Toluene-d8 (Surr)102 11/13/17 14:32 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 11/03/17 10:50 11/03/17 17:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 11/03/17 10:50 11/03/17 17:48 1Arsenic0.19 J
2.5 0.37 ug/L 11/03/17 10:50 11/03/17 17:48 1Barium10
1.0 0.43 ug/L 11/03/17 10:50 11/06/17 12:48 1Beryllium<1.0
0.50 0.15 ug/L 11/03/17 10:50 11/03/17 17:48 1Cadmium<0.50
5.0 2.3 ug/L 11/03/17 10:50 11/06/17 12:48 1Chromium<5.0
1.0 0.27 ug/L 11/03/17 10:50 11/06/17 12:48 1Cobalt<1.0
2.0 0.63 ug/L 11/03/17 10:50 11/03/17 17:48 1Copper4.1
100 38 ug/L 11/03/17 10:50 11/06/17 12:48 1Iron<100
0.50 0.16 ug/L 11/03/17 10:50 11/03/17 17:48 1Lead<0.50
2.5 1.1 ug/L 11/03/17 10:50 11/06/17 12:48 1Manganese1.6 J
2.0 0.92 ug/L 11/03/17 10:50 11/06/17 12:48 1Nickel<2.0
2.5 1.1 ug/L 11/03/17 10:50 11/03/17 17:48 1Selenium<2.5
0.50 0.078 ug/L 11/03/17 10:50 11/03/17 17:48 1Silver<0.50
2.0 0.65 ug/L 11/03/17 10:50 11/03/17 17:48 1Thallium<2.0
5.0 2.0 ug/L 11/03/17 10:50 11/06/17 12:48 1Vanadium<5.0
20 8.1 ug/L 11/03/17 10:50 11/03/17 17:48 1Zinc<20
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 11/03/17 12:20 11/06/17 11:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chloride 35 F1 2.0 1.7 mg/L 11/15/17 03:36 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.0 0.95 mg/L 11/15/17 03:36 10Sulfate31F1
5.0 3.7 mg/L 11/08/17 17:21 1Alkalinity23
10 4.3 mg/L 11/06/17 02:20 1Total Dissolved Solids 66
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Client Sample Results
TestAmerica Job ID: 500-136658-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill (Closed)
Lab Sample ID: 500-136658-2Client Sample ID: Gilkerson Well
Matrix: WaterDate Collected: 10/31/17 14:00
Date Received: 11/02/17 09:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 11/13/17 15:29 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 11/13/17 15:29 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 11/13/17 15:29 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 11/13/17 15:29 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 11/13/17 15:29 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 11/13/17 15:29 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 11/13/17 15:29 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 11/13/17 15:29 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 11/13/17 15:29 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 11/13/17 15:29 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 11/13/17 15:29 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 11/13/17 15:29 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 11/13/17 15:29 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 11/13/17 15:29 12-Butanone (MEK)<5.0
5.0 1.6 ug/L 11/13/17 15:29 12-Hexanone <5.0
5.0 2.2 ug/L 11/13/17 15:29 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 11/13/17 15:29 1Acetone<5.0
20 4.5 ug/L 11/13/17 15:29 1Acrylonitrile<20
0.50 0.15 ug/L 11/13/17 15:29 1Benzene<0.50
1.0 0.43 ug/L 11/13/17 15:29 1Bromochloromethane<1.0
1.0 0.37 ug/L 11/13/17 15:29 1Bromodichloromethane14
1.0 0.48 ug/L 11/13/17 15:29 1Bromoform<1.0
2.0 0.80 ug/L 11/13/17 15:29 1Bromomethane<2.0
2.0 0.45 ug/L 11/13/17 15:29 1Carbon disulfide <2.0
1.0 0.38 ug/L 11/13/17 15:29 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 11/13/17 15:29 1Chlorobenzene<1.0
1.0 0.51 ug/L 11/13/17 15:29 1Chloroethane<1.0
2.0 0.37 ug/L 11/13/17 15:29 1Chloroform41
1.0 0.32 ug/L 11/13/17 15:29 1Chloromethane<1.0
1.0 0.41 ug/L 11/13/17 15:29 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 11/13/17 15:29 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 11/13/17 15:29 1Dibromochloromethane7.6
1.0 0.27 ug/L 11/13/17 15:29 1Dibromomethane<1.0
0.50 0.18 ug/L 11/13/17 15:29 1Ethylbenzene<0.50
2.5 0.66 ug/L 11/13/17 15:29 1Iodomethane<2.5
5.0 1.6 ug/L 11/13/17 15:29 1Methylene Chloride <5.0 *
1.0 0.39 ug/L 11/13/17 15:29 1Styrene<1.0
1.0 0.37 ug/L 11/13/17 15:29 1Tetrachloroethene<1.0
10 1.9 ug/L 11/13/17 15:29 1Tetrahydrofuran<10
0.50 0.15 ug/L 11/13/17 15:29 1Toluene<0.50
1.0 0.35 ug/L 11/13/17 15:29 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 11/13/17 15:29 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 11/13/17 15:29 1trans-1,4-Dichloro-2-butene <5.0 *
0.50 0.16 ug/L 11/13/17 15:29 1Trichloroethene<0.50
1.0 0.43 ug/L 11/13/17 15:29 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 11/13/17 15:29 1Vinyl acetate <2.0
0.50 0.20 ug/L 11/13/17 15:29 1Vinyl chloride <0.50
1.0 0.22 ug/L 11/13/17 15:29 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-136658-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill (Closed)
Lab Sample ID: 500-136658-2Client Sample ID: Gilkerson Well
Matrix: WaterDate Collected: 10/31/17 14:00
Date Received: 11/02/17 09:00
1,2-Dichloroethane-d4 (Surr)86 75-126 11/13/17 15:29 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)86 11/13/17 15:29 172-124
Dibromofluoromethane 92 11/13/17 15:29 175-120
Toluene-d8 (Surr)103 11/13/17 15:29 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 11/03/17 10:50 11/03/17 18:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 11/03/17 10:50 11/03/17 18:11 1Arsenic0.15 J
2.5 0.37 ug/L 11/03/17 10:50 11/03/17 18:11 1Barium12
1.0 0.43 ug/L 11/03/17 10:50 11/03/17 18:11 1Beryllium<1.0
0.50 0.15 ug/L 11/03/17 10:50 11/03/17 18:11 1Cadmium<0.50
5.0 2.3 ug/L 11/03/17 10:50 11/03/17 18:11 1Chromium<5.0
1.0 0.27 ug/L 11/03/17 10:50 11/03/17 18:11 1Cobalt<1.0
2.0 0.63 ug/L 11/03/17 10:50 11/03/17 18:11 1Copper18
100 38 ug/L 11/03/17 10:50 11/03/17 18:11 1Iron660
0.50 0.16 ug/L 11/03/17 10:50 11/03/17 18:11 1Lead5.0
2.5 1.1 ug/L 11/03/17 10:50 11/06/17 13:07 1Manganese16
2.0 0.92 ug/L 11/03/17 10:50 11/03/17 18:11 1Nickel<2.0
2.5 1.1 ug/L 11/03/17 10:50 11/03/17 18:11 1Selenium<2.5
0.50 0.078 ug/L 11/03/17 10:50 11/03/17 18:11 1Silver<0.50
2.0 0.65 ug/L 11/03/17 10:50 11/03/17 18:11 1Thallium<2.0
5.0 2.0 ug/L 11/03/17 10:50 11/03/17 18:11 1Vanadium<5.0
20 8.1 ug/L 11/03/17 10:50 11/03/17 18:11 1Zinc32
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury 0.29 0.20 0.091 ug/L 11/03/17 12:20 11/06/17 11:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chloride 9.5 0.40 0.34 mg/L 11/15/17 04:13 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.40 0.19 mg/L 11/15/17 04:13 2Sulfate8.9
5.0 3.7 mg/L 11/09/17 15:43 1Alkalinity21
10 4.3 mg/L 11/06/17 02:25 1Total Dissolved Solids 62
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Client Sample Results
TestAmerica Job ID: 500-136658-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill (Closed)
Lab Sample ID: 500-136658-3Client Sample ID: Hammill Well
Matrix: WaterDate Collected: 10/31/17 14:15
Date Received: 11/02/17 09:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 11/13/17 15:55 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.38 ug/L 11/13/17 15:55 11,1,1-Trichloroethane <1.0
1.0 0.40 ug/L 11/13/17 15:55 11,1,2,2-Tetrachloroethane <1.0
1.0 0.35 ug/L 11/13/17 15:55 11,1,2-Trichloroethane <1.0
1.0 0.41 ug/L 11/13/17 15:55 11,1-Dichloroethane <1.0
1.0 0.39 ug/L 11/13/17 15:55 11,1-Dichloroethene <1.0
1.0 0.41 ug/L 11/13/17 15:55 11,2,3-Trichloropropane <1.0
5.0 2.0 ug/L 11/13/17 15:55 11,2-Dibromo-3-Chloropropane <5.0
1.0 0.39 ug/L 11/13/17 15:55 11,2-Dibromoethane <1.0
1.0 0.33 ug/L 11/13/17 15:55 11,2-Dichlorobenzene <1.0
1.0 0.39 ug/L 11/13/17 15:55 11,2-Dichloroethane <1.0
1.0 0.43 ug/L 11/13/17 15:55 11,2-Dichloropropane <1.0
1.0 0.36 ug/L 11/13/17 15:55 11,4-Dichlorobenzene <1.0
5.0 2.1 ug/L 11/13/17 15:55 12-Butanone (MEK)22
5.0 1.6 ug/L 11/13/17 15:55 12-Hexanone <5.0
5.0 2.2 ug/L 11/13/17 15:55 14-Methyl-2-pentanone (MIBK)<5.0
5.0 1.7 ug/L 11/13/17 15:55 1Acetone6.5 cn
20 4.5 ug/L 11/13/17 15:55 1Acrylonitrile<20
0.50 0.15 ug/L 11/13/17 15:55 1Benzene<0.50
1.0 0.43 ug/L 11/13/17 15:55 1Bromochloromethane<1.0
1.0 0.37 ug/L 11/13/17 15:55 1Bromodichloromethane<1.0
1.0 0.48 ug/L 11/13/17 15:55 1Bromoform<1.0
2.0 0.80 ug/L 11/13/17 15:55 1Bromomethane<2.0
2.0 0.45 ug/L 11/13/17 15:55 1Carbon disulfide <2.0
1.0 0.38 ug/L 11/13/17 15:55 1Carbon tetrachloride <1.0
1.0 0.39 ug/L 11/13/17 15:55 1Chlorobenzene<1.0
1.0 0.51 ug/L 11/13/17 15:55 1Chloroethane<1.0
2.0 0.37 ug/L 11/13/17 15:55 1Chloroform<2.0
1.0 0.32 ug/L 11/13/17 15:55 1Chloromethane<1.0
1.0 0.41 ug/L 11/13/17 15:55 1cis-1,2-Dichloroethene <1.0
1.0 0.42 ug/L 11/13/17 15:55 1cis-1,3-Dichloropropene <1.0
1.0 0.49 ug/L 11/13/17 15:55 1Dibromochloromethane<1.0
1.0 0.27 ug/L 11/13/17 15:55 1Dibromomethane<1.0
0.50 0.18 ug/L 11/13/17 15:55 1Ethylbenzene<0.50
2.5 0.66 ug/L 11/13/17 15:55 1Iodomethane<2.5
5.0 1.6 ug/L 11/13/17 15:55 1Methylene Chloride <5.0 *
1.0 0.39 ug/L 11/13/17 15:55 1Styrene<1.0
1.0 0.37 ug/L 11/13/17 15:55 1Tetrachloroethene<1.0
10 1.9 ug/L 11/13/17 15:55 1Tetrahydrofuran230
0.50 0.15 ug/L 11/13/17 15:55 1Toluene<0.50
1.0 0.35 ug/L 11/13/17 15:55 1trans-1,2-Dichloroethene <1.0
1.0 0.36 ug/L 11/13/17 15:55 1trans-1,3-Dichloropropene <1.0
5.0 1.2 ug/L 11/13/17 15:55 1trans-1,4-Dichloro-2-butene <5.0 *
0.50 0.16 ug/L 11/13/17 15:55 1Trichloroethene<0.50
1.0 0.43 ug/L 11/13/17 15:55 1Trichlorofluoromethane<1.0
2.0 0.91 ug/L 11/13/17 15:55 1Vinyl acetate <2.0
0.50 0.20 ug/L 11/13/17 15:55 1Vinyl chloride <0.50
1.0 0.22 ug/L 11/13/17 15:55 1Xylenes, Total <1.0
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Client Sample Results
TestAmerica Job ID: 500-136658-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill (Closed)
Lab Sample ID: 500-136658-3Client Sample ID: Hammill Well
Matrix: WaterDate Collected: 10/31/17 14:15
Date Received: 11/02/17 09:00
1,2-Dichloroethane-d4 (Surr)87 75-126 11/13/17 15:55 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)85 11/13/17 15:55 172-124
Dibromofluoromethane 92 11/13/17 15:55 175-120
Toluene-d8 (Surr)104 11/13/17 15:55 175-120
Method: 200.8 - Metals (ICP/MS)
RL MDL
Antimony <3.0 3.0 1.3 ug/L 11/03/17 10:50 11/03/17 18:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 0.15 ug/L 11/03/17 10:50 11/03/17 18:15 1Arsenic0.47 J
2.5 0.37 ug/L 11/03/17 10:50 11/03/17 18:15 1Barium41
1.0 0.43 ug/L 11/03/17 10:50 11/03/17 18:15 1Beryllium<1.0
0.50 0.15 ug/L 11/03/17 10:50 11/03/17 18:15 1Cadmium<0.50
5.0 2.3 ug/L 11/03/17 10:50 11/03/17 18:15 1Chromium<5.0
1.0 0.27 ug/L 11/03/17 10:50 11/03/17 18:15 1Cobalt<1.0
2.0 0.63 ug/L 11/03/17 10:50 11/03/17 18:15 1Copper4.3
100 38 ug/L 11/03/17 10:50 11/03/17 18:15 1Iron290
0.50 0.16 ug/L 11/03/17 10:50 11/03/17 18:15 1Lead0.28 J
2.5 1.1 ug/L 11/03/17 10:50 11/06/17 13:12 1Manganese60
2.0 0.92 ug/L 11/03/17 10:50 11/03/17 18:15 1Nickel0.95 J
2.5 1.1 ug/L 11/03/17 10:50 11/03/17 18:15 1Selenium<2.5
0.50 0.078 ug/L 11/03/17 10:50 11/03/17 18:15 1Silver<0.50
2.0 0.65 ug/L 11/03/17 10:50 11/03/17 18:15 1Thallium<2.0
5.0 2.0 ug/L 11/03/17 10:50 11/03/17 18:15 1Vanadium<5.0
20 8.1 ug/L 11/03/17 10:50 11/03/17 18:15 1Zinc490
Method: 245.1 - Mercury (CVAA)
RL MDL
Mercury <0.20 0.20 0.091 ug/L 11/03/17 12:20 11/06/17 11:13 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Chloride 5.6 0.40 0.34 mg/L 11/15/17 04:25 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10 4.8 mg/L 11/15/17 07:26 50Sulfate320
5.0 3.7 mg/L 11/09/17 15:49 1Alkalinity95
10 4.3 mg/L 11/06/17 02:28 1Total Dissolved Solids 600
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Definitions/Glossary
TestAmerica Job ID: 500-136658-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill (Closed)
Qualifiers
GC/MS VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
*LCS or LCSD is outside acceptance limits.
cn Refer to Case Narrative for further detail
Metals
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
General Chemistry
Qualifier Description
F1 MS and/or MSD Recovery is outside acceptance limits.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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QC Association Summary
TestAmerica Job ID: 500-136658-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill (Closed)
GC/MS VOA
Analysis Batch: 409675
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B500-136658-1 Tinsley Well Total/NA
Water 8260B500-136658-2 Gilkerson Well Total/NA
Water 8260B500-136658-3 Hammill Well Total/NA
Water 8260BMB 500-409675/7 Method Blank Total/NA
Water 8260BLCS 500-409675/5 Lab Control Sample Total/NA
Metals
Prep Batch: 408352
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 245.1500-136658-1 Tinsley Well Total/NA
Water 245.1500-136658-2 Gilkerson Well Total/NA
Water 245.1500-136658-3 Hammill Well Total/NA
Water 245.1MB 500-408352/12-A Method Blank Total/NA
Water 245.1LCS 500-408352/13-A Lab Control Sample Total/NA
Prep Batch: 408362
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 200.8500-136658-1 Tinsley Well Total/NA
Water 200.8500-136658-2 Gilkerson Well Total/NA
Water 200.8500-136658-3 Hammill Well Total/NA
Water 200.8MB 500-408362/1-A Method Blank Total/NA
Water 200.8LCS 500-408362/2-A Lab Control Sample Total/NA
Water 200.8500-136658-1 MS Tinsley Well Total/NA
Water 200.8500-136658-1 DU Tinsley Well Total/NA
Analysis Batch: 408572
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 200.8 408362500-136658-1 Tinsley Well Total/NA
Water 200.8 408362500-136658-2 Gilkerson Well Total/NA
Water 200.8 408362500-136658-3 Hammill Well Total/NA
Water 200.8 408362MB 500-408362/1-A Method Blank Total/NA
Water 200.8 408362LCS 500-408362/2-A Lab Control Sample Total/NA
Water 200.8 408362500-136658-1 MS Tinsley Well Total/NA
Water 200.8 408362500-136658-1 DU Tinsley Well Total/NA
Analysis Batch: 408624
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 245.1 408352500-136658-1 Tinsley Well Total/NA
Water 245.1 408352500-136658-2 Gilkerson Well Total/NA
Water 245.1 408352500-136658-3 Hammill Well Total/NA
Water 245.1 408352MB 500-408352/12-A Method Blank Total/NA
Water 245.1 408352LCS 500-408352/13-A Lab Control Sample Total/NA
Analysis Batch: 408632
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 200.8 408362500-136658-1 Tinsley Well Total/NA
Water 200.8 408362500-136658-2 Gilkerson Well Total/NA
Water 200.8 408362500-136658-3 Hammill Well Total/NA
Water 200.8 408362MB 500-408362/1-A Method Blank Total/NA
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QC Association Summary
TestAmerica Job ID: 500-136658-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill (Closed)
Metals (Continued)
Analysis Batch: 408632 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 200.8 408362LCS 500-408362/2-A Lab Control Sample Total/NA
Water 200.8 408362500-136658-1 MS Tinsley Well Total/NA
Water 200.8 408362500-136658-1 DU Tinsley Well Total/NA
General Chemistry
Analysis Batch: 408533
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 2540C500-136658-1 Tinsley Well Total/NA
Water SM 2540C500-136658-2 Gilkerson Well Total/NA
Water SM 2540C500-136658-3 Hammill Well Total/NA
Water SM 2540CMB 500-408533/1 Method Blank Total/NA
Water SM 2540CLCS 500-408533/2 Lab Control Sample Total/NA
Water SM 2540C500-136658-1 DU Tinsley Well Total/NA
Analysis Batch: 409180
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 2320B500-136658-1 Tinsley Well Total/NA
Water SM 2320BMB 500-409180/28 Method Blank Total/NA
Water SM 2320BLCS 500-409180/29 Lab Control Sample Total/NA
Water SM 2320B500-136658-1 DU Tinsley Well Total/NA
Analysis Batch: 409367
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 2320B500-136658-2 Gilkerson Well Total/NA
Water SM 2320B500-136658-3 Hammill Well Total/NA
Water SM 2320BMB 500-409367/3 Method Blank Total/NA
Water SM 2320BLCS 500-409367/4 Lab Control Sample Total/NA
Analysis Batch: 410022
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 9056A500-136658-1 Tinsley Well Total/NA
Water 9056A500-136658-2 Gilkerson Well Total/NA
Water 9056A500-136658-3 Hammill Well Total/NA
Water 9056A500-136658-3 Hammill Well Total/NA
Water 9056AMB 500-410022/3 Method Blank Total/NA
Water 9056ALCS 500-410022/4 Lab Control Sample Total/NA
Water 9056A500-136658-1 MS Tinsley Well Total/NA
Water 9056A500-136658-1 MSD Tinsley Well Total/NA
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Surrogate Summary
TestAmerica Job ID: 500-136658-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill (Closed)
Method: 8260B - Volatile Organic Compounds (GC/MS)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (75-126)(72-124)(75-120)(75-120)
12DCE BFB DBFM TOL
86 85 92 102500-136658-1
Percent Surrogate Recovery (Acceptance Limits)
Tinsley Well
86 86 92 103500-136658-2 Gilkerson Well
87 85 92 104500-136658-3 Hammill Well
83 82 90 100LCS 500-409675/5 Lab Control Sample
85 87 89 101MB 500-409675/7 Method Blank
Surrogate Legend
12DCE = 1,2-Dichloroethane-d4 (Surr)
BFB = 4-Bromofluorobenzene (Surr)
DBFM = Dibromofluoromethane
TOL = Toluene-d8 (Surr)
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QC Sample Results
TestAmerica Job ID: 500-136658-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill (Closed)
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 500-409675/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 409675
RL MDL
1,1,1,2-Tetrachloroethane <1.0 1.0 0.46 ug/L 11/13/17 13:38 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<1.0 0.381.0 ug/L 11/13/17 13:38 11,1,1-Trichloroethane
<1.0 0.401.0 ug/L 11/13/17 13:38 11,1,2,2-Tetrachloroethane
<1.0 0.351.0 ug/L 11/13/17 13:38 11,1,2-Trichloroethane
<1.0 0.411.0 ug/L 11/13/17 13:38 11,1-Dichloroethane
<1.0 0.391.0 ug/L 11/13/17 13:38 11,1-Dichloroethene
<1.0 0.411.0 ug/L 11/13/17 13:38 11,2,3-Trichloropropane
<5.0 2.05.0 ug/L 11/13/17 13:38 11,2-Dibromo-3-Chloropropane
<1.0 0.391.0 ug/L 11/13/17 13:38 11,2-Dibromoethane
<1.0 0.331.0 ug/L 11/13/17 13:38 11,2-Dichlorobenzene
<1.0 0.391.0 ug/L 11/13/17 13:38 11,2-Dichloroethane
<1.0 0.431.0 ug/L 11/13/17 13:38 11,2-Dichloropropane
<1.0 0.361.0 ug/L 11/13/17 13:38 11,4-Dichlorobenzene
<5.0 2.15.0 ug/L 11/13/17 13:38 12-Butanone (MEK)
<5.0 1.65.0 ug/L 11/13/17 13:38 12-Hexanone
<5.0 2.25.0 ug/L 11/13/17 13:38 14-Methyl-2-pentanone (MIBK)
<5.0 1.75.0 ug/L 11/13/17 13:38 1Acetone
<20 4.520 ug/L 11/13/17 13:38 1Acrylonitrile
<0.50 0.150.50 ug/L 11/13/17 13:38 1Benzene
<1.0 0.431.0 ug/L 11/13/17 13:38 1Bromochloromethane
<1.0 0.371.0 ug/L 11/13/17 13:38 1Bromodichloromethane
<1.0 0.481.0 ug/L 11/13/17 13:38 1Bromoform
<2.0 0.802.0 ug/L 11/13/17 13:38 1Bromomethane
<2.0 0.452.0 ug/L 11/13/17 13:38 1Carbon disulfide
<1.0 0.381.0 ug/L 11/13/17 13:38 1Carbon tetrachloride
<1.0 0.391.0 ug/L 11/13/17 13:38 1Chlorobenzene
<1.0 0.511.0 ug/L 11/13/17 13:38 1Chloroethane
<2.0 0.372.0 ug/L 11/13/17 13:38 1Chloroform
<1.0 0.321.0 ug/L 11/13/17 13:38 1Chloromethane
<1.0 0.411.0 ug/L 11/13/17 13:38 1cis-1,2-Dichloroethene
<1.0 0.421.0 ug/L 11/13/17 13:38 1cis-1,3-Dichloropropene
<1.0 0.491.0 ug/L 11/13/17 13:38 1Dibromochloromethane
<1.0 0.271.0 ug/L 11/13/17 13:38 1Dibromomethane
<0.50 0.180.50 ug/L 11/13/17 13:38 1Ethylbenzene
<2.5 0.662.5 ug/L 11/13/17 13:38 1Iodomethane
5.17 1.65.0 ug/L 11/13/17 13:38 1Methylene Chloride
<1.0 0.391.0 ug/L 11/13/17 13:38 1Styrene
<1.0 0.371.0 ug/L 11/13/17 13:38 1Tetrachloroethene
<10 1.910 ug/L 11/13/17 13:38 1Tetrahydrofuran
<0.50 0.150.50 ug/L 11/13/17 13:38 1Toluene
<1.0 0.351.0 ug/L 11/13/17 13:38 1trans-1,2-Dichloroethene
<1.0 0.361.0 ug/L 11/13/17 13:38 1trans-1,3-Dichloropropene
<5.0 1.25.0 ug/L 11/13/17 13:38 1trans-1,4-Dichloro-2-butene
<0.50 0.160.50 ug/L 11/13/17 13:38 1Trichloroethene
<1.0 0.431.0 ug/L 11/13/17 13:38 1Trichlorofluoromethane
<2.0 0.912.0 ug/L 11/13/17 13:38 1Vinyl acetate
<0.50 0.200.50 ug/L 11/13/17 13:38 1Vinyl chloride
<1.0 0.221.0 ug/L 11/13/17 13:38 1Xylenes, Total
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QC Sample Results
TestAmerica Job ID: 500-136658-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill (Closed)
1,2-Dichloroethane-d4 (Surr)85 75-126 11/13/17 13:38 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
87 11/13/17 13:38 14-Bromofluorobenzene (Surr)72-124
89 11/13/17 13:38 1Dibromofluoromethane75-120
101 11/13/17 13:38 1Toluene-d8 (Surr)75-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-409675/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 409675
1,1,1,2-Tetrachloroethane 50.0 45.4 ug/L 91 70-125
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,1,1-Trichloroethane 50.0 45.2 ug/L 90 70-125
1,1,2,2-Tetrachloroethane 50.0 41.9 ug/L 84 67-127
1,1,2-Trichloroethane 50.0 48.8 ug/L 98 70-122
1,1-Dichloroethane 50.0 52.4 ug/L 105 70-125
1,1-Dichloroethene 50.0 51.9 ug/L 104 67-122
1,2,3-Trichloropropane 50.0 37.3 ug/L 75 50-133
1,2-Dibromo-3-Chloropropane 50.0 34.9 ug/L 70 56-123
1,2-Dibromoethane 50.0 47.1 ug/L 94 70-125
1,2-Dichlorobenzene 50.0 46.5 ug/L 93 70-125
1,2-Dichloroethane 50.0 42.5 ug/L 85 68-127
1,2-Dichloropropane 50.0 53.9 ug/L 108 67-130
1,4-Dichlorobenzene 50.0 44.4 ug/L 89 70-120
2-Butanone (MEK)50.0 48.0 ug/L 96 53-141
2-Hexanone 50.0 44.0 ug/L 88 56-135
4-Methyl-2-pentanone (MIBK)50.0 44.1 ug/L 88 56-133
Acetone 50.0 44.5 ug/L 89 40-143
Acrylonitrile 500 498 ug/L 100 67-140
Benzene 50.0 49.9 ug/L 100 70-120
Bromochloromethane 50.0 48.6 ug/L 97 65-122
Bromodichloromethane 50.0 43.7 ug/L 87 69-120
Bromoform 50.0 39.1 ug/L 78 56-132
Bromomethane 50.0 45.0 ug/L 90 40-130
Carbon disulfide 50.0 52.9 ug/L 106 66-120
Carbon tetrachloride 50.0 43.8 ug/L 88 65-122
Chlorobenzene 50.0 48.7 ug/L 97 70-120
Chloroethane 50.0 46.0 ug/L 92 45-127
Chloroform 50.0 46.7 ug/L 93 70-120
Chloromethane 50.0 43.9 ug/L 88 54-147
cis-1,2-Dichloroethene 50.0 49.1 ug/L 98 70-125
cis-1,3-Dichloropropene 50.0 47.2 ug/L 94 64-127
Dibromochloromethane 50.0 41.4 ug/L 83 68-125
Dibromomethane 50.0 45.3 ug/L 91 70-120
Ethylbenzene 50.0 49.6 ug/L 99 70-120
Iodomethane 50.0 53.0 ug/L 106 61-136
Methylene Chloride 50.0 68.5 *ug/L 137 69-125
Styrene 50.0 49.3 ug/L 99 70-120
Tetrachloroethene 50.0 53.2 ug/L 106 70-128
Tetrahydrofuran 100 93.5 ug/L 93 59-139
Toluene 50.0 48.2 ug/L 96 70-125
trans-1,2-Dichloroethene 50.0 51.1 ug/L 102 70-125
trans-1,3-Dichloropropene 50.0 44.1 ug/L 88 62-128
trans-1,4-Dichloro-2-butene 50.0 25.7 *ug/L 51 60-130
Trichloroethene 50.0 52.7 ug/L 105 70-125
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QC Sample Results
TestAmerica Job ID: 500-136658-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill (Closed)
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-409675/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 409675
Trichlorofluoromethane 50.0 40.0 ug/L 80 70-126
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Vinyl acetate 50.0 34.6 ug/L 69 43-133
Vinyl chloride 50.0 53.9 ug/L 108 64-126
Xylenes, Total 100 93.0 ug/L 93 70-125
1,2-Dichloroethane-d4 (Surr)75 -126
Surrogate
83
LCS LCS
Qualifier Limits%Recovery
824-Bromofluorobenzene (Surr)72 -124
90Dibromofluoromethane 75 -120
100Toluene-d8 (Surr)75 -120
Method: 200.8 - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 500-408362/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 408572 Prep Batch: 408362
RL MDL
Antimony <3.0 3.0 1.3 ug/L 11/03/17 10:50 11/03/17 16:51 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<1.0 0.151.0 ug/L 11/03/17 10:50 11/03/17 16:51 1Arsenic
<2.5 0.372.5 ug/L 11/03/17 10:50 11/03/17 16:51 1Barium
<0.50 0.150.50 ug/L 11/03/17 10:50 11/03/17 16:51 1Cadmium
<2.0 0.632.0 ug/L 11/03/17 10:50 11/03/17 16:51 1Copper
<0.50 0.160.50 ug/L 11/03/17 10:50 11/03/17 16:51 1Lead
<2.5 1.12.5 ug/L 11/03/17 10:50 11/03/17 16:51 1Selenium
<0.50 0.0780.50 ug/L 11/03/17 10:50 11/03/17 16:51 1Silver
<2.0 0.652.0 ug/L 11/03/17 10:50 11/03/17 16:51 1Thallium
<20 8.120 ug/L 11/03/17 10:50 11/03/17 16:51 1Zinc
Client Sample ID: Method BlankLab Sample ID: MB 500-408362/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 408632 Prep Batch: 408362
RL MDL
Beryllium <1.0 1.0 0.43 ug/L 11/03/17 10:50 11/06/17 11:38 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<5.0 2.35.0 ug/L 11/03/17 10:50 11/06/17 11:38 1Chromium
<1.0 0.271.0 ug/L 11/03/17 10:50 11/06/17 11:38 1Cobalt
<100 38100 ug/L 11/03/17 10:50 11/06/17 11:38 1Iron
<2.5 1.12.5 ug/L 11/03/17 10:50 11/06/17 11:38 1Manganese
<2.0 0.922.0 ug/L 11/03/17 10:50 11/06/17 11:38 1Nickel
<5.0 2.05.0 ug/L 11/03/17 10:50 11/06/17 11:38 1Vanadium
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-408362/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 408572 Prep Batch: 408362
Antimony 500 481 ug/L 96 85-115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
TestAmerica Chicago
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QC Sample Results
TestAmerica Job ID: 500-136658-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill (Closed)
Method: 200.8 - Metals (ICP/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-408362/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 408572 Prep Batch: 408362
Arsenic 100 97.7 ug/L 98 85-115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Barium 500 513 ug/L 103 85-115
Cadmium 50.0 49.6 ug/L 99 85-115
Copper 250 256 ug/L 102 85-115
Lead 100 95.4 ug/L 95 85-115
Selenium 100 95.9 ug/L 96 85-115
Silver 50.0 51.9 ug/L 104 85-115
Thallium 100 95.3 ug/L 95 85-115
Zinc 500 513 ug/L 103 85-115
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-408362/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 408632 Prep Batch: 408362
Beryllium 50.0 50.2 ug/L 100 85-115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Chromium 200 201 ug/L 100 85-115
Cobalt 500 504 ug/L 101 85-115
Iron 1000 1000 ug/L 100 85-115
Manganese 500 510 ug/L 102 85-115
Nickel 500 514 ug/L 103 85-115
Vanadium 500 499 ug/L 100 85-115
Client Sample ID: Tinsley WellLab Sample ID: 500-136658-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 408572 Prep Batch: 408362
Antimony <3.0 500 498 ug/L 100 70-130
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Arsenic 0.19 J 100 98.8 ug/L 99 70-130
Barium 10 500 534 ug/L 105 70-130
Cadmium <0.50 50.0 49.9 ug/L 100 70-130
Copper 4.1 250 256 ug/L 101 70-130
Lead <0.50 100 98.3 ug/L 98 70-130
Selenium <2.5 100 97.5 ug/L 97 70-130
Silver <0.50 50.0 52.0 ug/L 104 70-130
Thallium <2.0 100 97.8 ug/L 98 70-130
Zinc <20 500 508 ug/L 102 70-130
Client Sample ID: Tinsley WellLab Sample ID: 500-136658-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 408632 Prep Batch: 408362
Beryllium <1.0 50.0 49.3 ug/L 99 70-130
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Chromium <5.0 200 201 ug/L 101 70-130
Cobalt <1.0 500 508 ug/L 102 70-130
Iron <100 1000 1000 ug/L 100 70-130
Manganese 1.6 J 500 507 ug/L 101 70-130
TestAmerica Chicago
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QC Sample Results
TestAmerica Job ID: 500-136658-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill (Closed)
Method: 200.8 - Metals (ICP/MS) (Continued)
Client Sample ID: Tinsley WellLab Sample ID: 500-136658-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 408632 Prep Batch: 408362
Nickel <2.0 500 520 ug/L 104 70-130
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Vanadium <5.0 500 503 ug/L 101 70-130
Client Sample ID: Tinsley WellLab Sample ID: 500-136658-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 408572 Prep Batch: 408362
Antimony <3.0 <3.0 ug/L NC 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Arsenic 0.19 J 0.204 J ug/L 6 20
Barium 10 10.8 ug/L 5 20
Cadmium <0.50 <0.50 ug/L NC 20
Copper 4.1 4.24 ug/L 3 20
Lead <0.50 <0.50 ug/L NC 20
Selenium <2.5 <2.5 ug/L NC 20
Silver <0.50 <0.50 ug/L NC 20
Thallium <2.0 <2.0 ug/L NC 20
Zinc <20 <20 ug/L NC 20
Client Sample ID: Tinsley WellLab Sample ID: 500-136658-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 408632 Prep Batch: 408362
Beryllium <1.0 <1.0 ug/L NC 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Chromium <5.0 <5.0 ug/L NC 20
Cobalt <1.0 <1.0 ug/L NC 20
Iron <100 <100 ug/L NC 20
Manganese 1.6 J 1.71 J ug/L 6 20
Nickel <2.0 1.47 J ug/L NC 20
Vanadium <5.0 <5.0 ug/L NC 20
Method: 245.1 - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 500-408352/12-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 408624 Prep Batch: 408352
RL MDL
Mercury <0.20 0.20 0.091 ug/L 11/03/17 12:20 11/06/17 10:48 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-408352/13-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 408624 Prep Batch: 408352
Mercury 2.00 1.81 ug/L 91 85-115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
TestAmerica Chicago
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QC Sample Results
TestAmerica Job ID: 500-136658-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill (Closed)
Method: 9056A - Anions, Ion Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 500-410022/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 410022
RL MDL
Chloride <0.20 0.20 0.17 mg/L 11/14/17 21:49 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.20 0.0950.20 mg/L 11/14/17 21:49 1Sulfate
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-410022/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 410022
Chloride 3.00 3.03 mg/L 101 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Sulfate 5.00 5.21 mg/L 104 80-120
Client Sample ID: Tinsley WellLab Sample ID: 500-136658-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 410022
Chloride 35 F1 10.0 41.7 F1 mg/L 71 80-120
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Sulfate 31 F1 25.0 48.9 F1 mg/L 73 80-120
Client Sample ID: Tinsley WellLab Sample ID: 500-136658-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 410022
Chloride 35 F1 10.0 42.9 mg/L 83 80-120 3 15
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Sulfate 31 F1 25.0 49.6 F1 mg/L 75 80-120 1 15
Method: SM 2320B - Alkalinity
Client Sample ID: Method BlankLab Sample ID: MB 500-409180/28
Matrix: Water Prep Type: Total/NA
Analysis Batch: 409180
RL MDL
Alkalinity <5.0 5.0 3.7 mg/L 11/08/17 14:34 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-409180/29
Matrix: Water Prep Type: Total/NA
Analysis Batch: 409180
Alkalinity 100 107 mg/L 107 85-115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Tinsley WellLab Sample ID: 500-136658-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 409180
Alkalinity 23 22.5 mg/L 2 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
TestAmerica Chicago
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QC Sample Results
TestAmerica Job ID: 500-136658-1Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill (Closed)
Method: SM 2320B - Alkalinity (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 500-409367/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 409367
RL MDL
Alkalinity <5.0 5.0 3.7 mg/L 11/09/17 12:40 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-409367/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 409367
Alkalinity 100 107 mg/L 107 85-115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Method: SM 2540C - Solids, Total Dissolved (TDS)
Client Sample ID: Method BlankLab Sample ID: MB 500-408533/1
Matrix: Water Prep Type: Total/NA
Analysis Batch: 408533
RL MDL
Total Dissolved Solids <10 10 4.3 mg/L 11/06/17 02:05 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-408533/2
Matrix: Water Prep Type: Total/NA
Analysis Batch: 408533
Total Dissolved Solids 250 250 mg/L 100 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Tinsley WellLab Sample ID: 500-136658-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 408533
Total Dissolved Solids 66 68.0 mg/L 3 5
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
TestAmerica Chicago
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Lab Chronicle
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-136658-1
Project/Site: NC North Mecklenburg Landfill (Closed)
Client Sample ID: Tinsley Well Lab Sample ID: 500-136658-1
Matrix: WaterDate Collected: 10/31/17 13:45
Date Received: 11/02/17 09:00
Analysis 8260B 11/13/17 14:32 EMA1409675 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 408362 11/03/17 10:50 LWN TAL CHITotal/NA
Analysis 200.8 1 408632 11/06/17 12:48 FXG TAL CHITotal/NA
Prep 200.8 408362 11/03/17 10:50 LWN TAL CHITotal/NA
Analysis 200.8 1 408572 11/03/17 17:48 FXG TAL CHITotal/NA
Prep 245.1 408352 11/03/17 12:20 EEN TAL CHITotal/NA
Analysis 245.1 1 408624 11/06/17 11:10 EEN TAL CHITotal/NA
Analysis 9056A 10 410022 11/15/17 03:36 EAT TAL CHITotal/NA
Analysis SM 2320B 1 409180 11/08/17 17:21 SMO TAL CHITotal/NA
Analysis SM 2540C 1 408533 11/06/17 02:20 CLB TAL CHITotal/NA
Client Sample ID: Gilkerson Well Lab Sample ID: 500-136658-2
Matrix: WaterDate Collected: 10/31/17 14:00
Date Received: 11/02/17 09:00
Analysis 8260B 11/13/17 15:29 EMA1409675 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 408362 11/03/17 10:50 LWN TAL CHITotal/NA
Analysis 200.8 1 408632 11/06/17 13:07 FXG TAL CHITotal/NA
Prep 200.8 408362 11/03/17 10:50 LWN TAL CHITotal/NA
Analysis 200.8 1 408572 11/03/17 18:11 FXG TAL CHITotal/NA
Prep 245.1 408352 11/03/17 12:20 EEN TAL CHITotal/NA
Analysis 245.1 1 408624 11/06/17 11:11 EEN TAL CHITotal/NA
Analysis 9056A 2 410022 11/15/17 04:13 EAT TAL CHITotal/NA
Analysis SM 2320B 1 409367 11/09/17 15:43 SMO TAL CHITotal/NA
Analysis SM 2540C 1 408533 11/06/17 02:25 CLB TAL CHITotal/NA
Client Sample ID: Hammill Well Lab Sample ID: 500-136658-3
Matrix: WaterDate Collected: 10/31/17 14:15
Date Received: 11/02/17 09:00
Analysis 8260B 11/13/17 15:55 EMA1409675 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 200.8 408362 11/03/17 10:50 LWN TAL CHITotal/NA
Analysis 200.8 1 408632 11/06/17 13:12 FXG TAL CHITotal/NA
Prep 200.8 408362 11/03/17 10:50 LWN TAL CHITotal/NA
Analysis 200.8 1 408572 11/03/17 18:15 FXG TAL CHITotal/NA
Prep 245.1 408352 11/03/17 12:20 EEN TAL CHITotal/NA
Analysis 245.1 1 408624 11/06/17 11:13 EEN TAL CHITotal/NA
Analysis 9056A 2 410022 11/15/17 04:25 EAT TAL CHITotal/NA
Analysis 9056A 50 410022 11/15/17 07:26 EAT TAL CHITotal/NA
Analysis SM 2320B 1 409367 11/09/17 15:49 SMO TAL CHITotal/NA
TestAmerica Chicago
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Lab Chronicle
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-136658-1
Project/Site: NC North Mecklenburg Landfill (Closed)
Client Sample ID: Hammill Well Lab Sample ID: 500-136658-3
Matrix: WaterDate Collected: 10/31/17 14:15
Date Received: 11/02/17 09:00
Analysis SM 2540C 11/06/17 02:28 CLB1408533 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Laboratory References:
TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL [phone]
TestAmerica Chicago
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Accreditation/Certification Summary
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-136658-1
Project/Site: NC North Mecklenburg Landfill (Closed)
Laboratory: TestAmerica Chicago
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program EPA Region Identification Number Expiration Date
North Carolina (WW/SW)2914State Program 12-31-17 *
Analysis Method Prep Method Matrix Analyte
The following analytes are included in this report, but accreditation/certification is not offered by the governing authority:
8260B Water trans-1,4-Dichloro-2-butene
TestAmerica Chicago
* Accreditation/Certification renewal pending - accreditation/certification considered valid.
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Login Sample Receipt Checklist
Client: Civil & Environmental Consultants Inc Job Number: 500-136658-1
Login Number: 136658
Question Answer Comment
Creator: Kelsey, Shawn M
List Source: TestAmerica Chicago
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.-0.9c
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Chicago
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#=CL#
October 20, 2017
LIMS USE: FR - ED STEPHENS
LIMS OBJECT ID: 92359172
92359172
Project:
Pace Project No.:
RE:
Ed Stephens
Civil & Environmental Consultants
1900 Center Park Drive
Charlotte, NC 28217
North Meck Landfill
Dear Ed Stephens:
Enclosed are the analytical results for sample(s) received by the laboratory on October 13, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 22
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92359172
North Meck Landfill
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 22
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92359172
North Meck Landfill
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92359172001 MW-5D NMLF EPA 8260 51 PASI-CGAW
92359172002 MW-12D Infill EPA 8260 51 PASI-CGAW
92359172003 MW-12 Infill EPA 8260 51 PASI-CGAW
92359172004 MW-9 Infill EPA 8260 51 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 22
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92359172
North Meck Landfill
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92359172001 MW-5D NMLF
Chloroethane 1.7 ug/L 10/19/17 00:551.0EPA 8260
1,1-Dichloroethane 1.7 ug/L 10/19/17 00:551.0EPA 8260
cis-1,2-Dichloroethene 2.5 ug/L 10/19/17 00:551.0EPA 8260
Tetrahydrofuran 23.4 ug/L 10/19/17 00:5510.0EPA 8260
Vinyl chloride 2.4 ug/L 10/19/17 00:551.0EPA 8260
92359172002 MW-12D Infill
cis-1,2-Dichloroethene 1.8 ug/L 10/19/17 01:111.0EPA 8260
Vinyl chloride 1.7 ug/L 10/19/17 01:111.0EPA 8260
92359172003 MW-12 Infill
cis-1,2-Dichloroethene 2.1 ug/L 10/19/17 01:271.0EPA 8260
Vinyl chloride 2.4 ug/L 10/19/17 01:271.0EPA 8260
92359172004 MW-9 Infill
Benzene 1.3 ug/L 10/19/17 01:431.0EPA 8260
cis-1,2-Dichloroethene 2.2 ug/L 10/19/17 01:431.0EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92359172
North Meck Landfill
Sample:MW-5D NMLF Lab ID:92359172001 Collected:10/10/17 10:50 Received:10/13/17 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/19/17 00:55 67-64-125.0 1
Acrylonitrile ND ug/L 10/19/17 00:55 107-13-110.0 1
Benzene ND ug/L 10/19/17 00:55 71-43-21.0 1
Bromochloromethane ND ug/L 10/19/17 00:55 74-97-51.0 1
Bromodichloromethane ND ug/L 10/19/17 00:55 75-27-41.0 1
Bromoform ND ug/L 10/19/17 00:55 75-25-21.0 1
Bromomethane ND ug/L 10/19/17 00:55 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/19/17 00:55 78-93-35.0 1
Carbon disulfide ND ug/L 10/19/17 00:55 75-15-02.0 1
Carbon tetrachloride ND ug/L 10/19/17 00:55 56-23-51.0 1
Chlorobenzene ND ug/L 10/19/17 00:55 108-90-71.0 1
Chloroethane 1.7 ug/L 10/19/17 00:55 75-00-31.0 1
Chloroform ND ug/L 10/19/17 00:55 67-66-31.0 1
Chloromethane ND ug/L 10/19/17 00:55 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/19/17 00:55 96-12-82.0 1
Dibromochloromethane ND ug/L 10/19/17 00:55 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/19/17 00:55 106-93-41.0 1
Dibromomethane ND ug/L 10/19/17 00:55 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/19/17 00:55 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 10/19/17 00:55 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 10/19/17 00:55 110-57-61.0 1
1,1-Dichloroethane 1.7 ug/L 10/19/17 00:55 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/19/17 00:55 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/19/17 00:55 75-35-41.0 1
cis-1,2-Dichloroethene 2.5 ug/L 10/19/17 00:55 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/19/17 00:55 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/19/17 00:55 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 10/19/17 00:55 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/19/17 00:55 10061-02-61.0 1
Ethylbenzene ND ug/L 10/19/17 00:55 100-41-41.0 1
2-Hexanone ND ug/L 10/19/17 00:55 591-78-65.0 1
Iodomethane ND ug/L 10/19/17 00:55 74-88-45.0 1
Methylene Chloride ND ug/L 10/19/17 00:55 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/19/17 00:55 108-10-15.0 1
Styrene ND ug/L 10/19/17 00:55 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/19/17 00:55 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/19/17 00:55 79-34-5 L21.0 1
Tetrachloroethene ND ug/L 10/19/17 00:55 127-18-41.0 1
Tetrahydrofuran 23.4 ug/L 10/19/17 00:55 109-99-910.0 1
Toluene ND ug/L 10/19/17 00:55 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 10/19/17 00:55 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/19/17 00:55 79-00-51.0 1
Trichloroethene ND ug/L 10/19/17 00:55 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/19/17 00:55 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/19/17 00:55 96-18-41.0 1
Vinyl acetate ND ug/L 10/19/17 00:55 108-05-42.0 1
Vinyl chloride 2.4 ug/L 10/19/17 00:55 75-01-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2017 02:31 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 5 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92359172
North Meck Landfill
Sample:MW-5D NMLF Lab ID:92359172001 Collected:10/10/17 10:50 Received:10/13/17 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Xylene (Total)ND ug/L 10/19/17 00:55 1330-20-71.0 1
Surrogates
4-Bromofluorobenzene (S)102 %10/19/17 00:55 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %10/19/17 00:55 17060-07-070-130 1
Toluene-d8 (S)100 %10/19/17 00:55 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2017 02:31 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92359172
North Meck Landfill
Sample:MW-12D Infill Lab ID:92359172002 Collected:10/11/17 12:30 Received:10/13/17 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/19/17 01:11 67-64-125.0 1
Acrylonitrile ND ug/L 10/19/17 01:11 107-13-110.0 1
Benzene ND ug/L 10/19/17 01:11 71-43-21.0 1
Bromochloromethane ND ug/L 10/19/17 01:11 74-97-51.0 1
Bromodichloromethane ND ug/L 10/19/17 01:11 75-27-41.0 1
Bromoform ND ug/L 10/19/17 01:11 75-25-21.0 1
Bromomethane ND ug/L 10/19/17 01:11 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/19/17 01:11 78-93-35.0 1
Carbon disulfide ND ug/L 10/19/17 01:11 75-15-02.0 1
Carbon tetrachloride ND ug/L 10/19/17 01:11 56-23-51.0 1
Chlorobenzene ND ug/L 10/19/17 01:11 108-90-71.0 1
Chloroethane ND ug/L 10/19/17 01:11 75-00-31.0 1
Chloroform ND ug/L 10/19/17 01:11 67-66-31.0 1
Chloromethane ND ug/L 10/19/17 01:11 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/19/17 01:11 96-12-82.0 1
Dibromochloromethane ND ug/L 10/19/17 01:11 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/19/17 01:11 106-93-41.0 1
Dibromomethane ND ug/L 10/19/17 01:11 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/19/17 01:11 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 10/19/17 01:11 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 10/19/17 01:11 110-57-61.0 1
1,1-Dichloroethane ND ug/L 10/19/17 01:11 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/19/17 01:11 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/19/17 01:11 75-35-41.0 1
cis-1,2-Dichloroethene 1.8 ug/L 10/19/17 01:11 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/19/17 01:11 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/19/17 01:11 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 10/19/17 01:11 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/19/17 01:11 10061-02-61.0 1
Ethylbenzene ND ug/L 10/19/17 01:11 100-41-41.0 1
2-Hexanone ND ug/L 10/19/17 01:11 591-78-65.0 1
Iodomethane ND ug/L 10/19/17 01:11 74-88-45.0 1
Methylene Chloride ND ug/L 10/19/17 01:11 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/19/17 01:11 108-10-15.0 1
Styrene ND ug/L 10/19/17 01:11 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/19/17 01:11 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/19/17 01:11 79-34-5 L21.0 1
Tetrachloroethene ND ug/L 10/19/17 01:11 127-18-41.0 1
Tetrahydrofuran ND ug/L 10/19/17 01:11 109-99-910.0 1
Toluene ND ug/L 10/19/17 01:11 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 10/19/17 01:11 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/19/17 01:11 79-00-51.0 1
Trichloroethene ND ug/L 10/19/17 01:11 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/19/17 01:11 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/19/17 01:11 96-18-41.0 1
Vinyl acetate ND ug/L 10/19/17 01:11 108-05-42.0 1
Vinyl chloride 1.7 ug/L 10/19/17 01:11 75-01-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2017 02:31 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92359172
North Meck Landfill
Sample:MW-12D Infill Lab ID:92359172002 Collected:10/11/17 12:30 Received:10/13/17 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Xylene (Total)ND ug/L 10/19/17 01:11 1330-20-71.0 1
Surrogates
4-Bromofluorobenzene (S)103 %10/19/17 01:11 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %10/19/17 01:11 17060-07-070-130 1
Toluene-d8 (S)100 %10/19/17 01:11 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2017 02:31 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92359172
North Meck Landfill
Sample:MW-12 Infill Lab ID:92359172003 Collected:10/11/17 13:15 Received:10/13/17 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/19/17 01:27 67-64-125.0 1
Acrylonitrile ND ug/L 10/19/17 01:27 107-13-110.0 1
Benzene ND ug/L 10/19/17 01:27 71-43-21.0 1
Bromochloromethane ND ug/L 10/19/17 01:27 74-97-51.0 1
Bromodichloromethane ND ug/L 10/19/17 01:27 75-27-41.0 1
Bromoform ND ug/L 10/19/17 01:27 75-25-21.0 1
Bromomethane ND ug/L 10/19/17 01:27 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/19/17 01:27 78-93-35.0 1
Carbon disulfide ND ug/L 10/19/17 01:27 75-15-02.0 1
Carbon tetrachloride ND ug/L 10/19/17 01:27 56-23-51.0 1
Chlorobenzene ND ug/L 10/19/17 01:27 108-90-71.0 1
Chloroethane ND ug/L 10/19/17 01:27 75-00-31.0 1
Chloroform ND ug/L 10/19/17 01:27 67-66-31.0 1
Chloromethane ND ug/L 10/19/17 01:27 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/19/17 01:27 96-12-82.0 1
Dibromochloromethane ND ug/L 10/19/17 01:27 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/19/17 01:27 106-93-41.0 1
Dibromomethane ND ug/L 10/19/17 01:27 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/19/17 01:27 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 10/19/17 01:27 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 10/19/17 01:27 110-57-61.0 1
1,1-Dichloroethane ND ug/L 10/19/17 01:27 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/19/17 01:27 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/19/17 01:27 75-35-41.0 1
cis-1,2-Dichloroethene 2.1 ug/L 10/19/17 01:27 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/19/17 01:27 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/19/17 01:27 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 10/19/17 01:27 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/19/17 01:27 10061-02-61.0 1
Ethylbenzene ND ug/L 10/19/17 01:27 100-41-41.0 1
2-Hexanone ND ug/L 10/19/17 01:27 591-78-65.0 1
Iodomethane ND ug/L 10/19/17 01:27 74-88-45.0 1
Methylene Chloride ND ug/L 10/19/17 01:27 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/19/17 01:27 108-10-15.0 1
Styrene ND ug/L 10/19/17 01:27 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/19/17 01:27 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/19/17 01:27 79-34-5 L21.0 1
Tetrachloroethene ND ug/L 10/19/17 01:27 127-18-41.0 1
Tetrahydrofuran ND ug/L 10/19/17 01:27 109-99-910.0 1
Toluene ND ug/L 10/19/17 01:27 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 10/19/17 01:27 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/19/17 01:27 79-00-51.0 1
Trichloroethene ND ug/L 10/19/17 01:27 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/19/17 01:27 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/19/17 01:27 96-18-41.0 1
Vinyl acetate ND ug/L 10/19/17 01:27 108-05-42.0 1
Vinyl chloride 2.4 ug/L 10/19/17 01:27 75-01-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2017 02:31 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92359172
North Meck Landfill
Sample:MW-12 Infill Lab ID:92359172003 Collected:10/11/17 13:15 Received:10/13/17 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Xylene (Total)ND ug/L 10/19/17 01:27 1330-20-71.0 1
Surrogates
4-Bromofluorobenzene (S)101 %10/19/17 01:27 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %10/19/17 01:27 17060-07-070-130 1
Toluene-d8 (S)101 %10/19/17 01:27 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2017 02:31 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92359172
North Meck Landfill
Sample:MW-9 Infill Lab ID:92359172004 Collected:10/12/17 10:00 Received:10/13/17 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 10/19/17 01:43 67-64-125.0 1
Acrylonitrile ND ug/L 10/19/17 01:43 107-13-110.0 1
Benzene 1.3 ug/L 10/19/17 01:43 71-43-21.0 1
Bromochloromethane ND ug/L 10/19/17 01:43 74-97-51.0 1
Bromodichloromethane ND ug/L 10/19/17 01:43 75-27-41.0 1
Bromoform ND ug/L 10/19/17 01:43 75-25-21.0 1
Bromomethane ND ug/L 10/19/17 01:43 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/19/17 01:43 78-93-35.0 1
Carbon disulfide ND ug/L 10/19/17 01:43 75-15-02.0 1
Carbon tetrachloride ND ug/L 10/19/17 01:43 56-23-51.0 1
Chlorobenzene ND ug/L 10/19/17 01:43 108-90-71.0 1
Chloroethane ND ug/L 10/19/17 01:43 75-00-31.0 1
Chloroform ND ug/L 10/19/17 01:43 67-66-31.0 1
Chloromethane ND ug/L 10/19/17 01:43 74-87-31.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/19/17 01:43 96-12-82.0 1
Dibromochloromethane ND ug/L 10/19/17 01:43 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/19/17 01:43 106-93-41.0 1
Dibromomethane ND ug/L 10/19/17 01:43 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/19/17 01:43 95-50-11.0 1
1,4-Dichlorobenzene ND ug/L 10/19/17 01:43 106-46-71.0 1
trans-1,4-Dichloro-2-butene ND ug/L 10/19/17 01:43 110-57-61.0 1
1,1-Dichloroethane ND ug/L 10/19/17 01:43 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/19/17 01:43 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/19/17 01:43 75-35-41.0 1
cis-1,2-Dichloroethene 2.2 ug/L 10/19/17 01:43 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/19/17 01:43 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/19/17 01:43 78-87-51.0 1
cis-1,3-Dichloropropene ND ug/L 10/19/17 01:43 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/19/17 01:43 10061-02-61.0 1
Ethylbenzene ND ug/L 10/19/17 01:43 100-41-41.0 1
2-Hexanone ND ug/L 10/19/17 01:43 591-78-65.0 1
Iodomethane ND ug/L 10/19/17 01:43 74-88-45.0 1
Methylene Chloride ND ug/L 10/19/17 01:43 75-09-21.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/19/17 01:43 108-10-15.0 1
Styrene ND ug/L 10/19/17 01:43 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/19/17 01:43 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/19/17 01:43 79-34-5 L21.0 1
Tetrachloroethene ND ug/L 10/19/17 01:43 127-18-41.0 1
Tetrahydrofuran ND ug/L 10/19/17 01:43 109-99-910.0 1
Toluene ND ug/L 10/19/17 01:43 108-88-31.0 1
1,1,1-Trichloroethane ND ug/L 10/19/17 01:43 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/19/17 01:43 79-00-51.0 1
Trichloroethene ND ug/L 10/19/17 01:43 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/19/17 01:43 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/19/17 01:43 96-18-41.0 1
Vinyl acetate ND ug/L 10/19/17 01:43 108-05-42.0 1
Vinyl chloride ND ug/L 10/19/17 01:43 75-01-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2017 02:31 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92359172
North Meck Landfill
Sample:MW-9 Infill Lab ID:92359172004 Collected:10/12/17 10:00 Received:10/13/17 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level Landfill
Xylene (Total)ND ug/L 10/19/17 01:43 1330-20-71.0 1
Surrogates
4-Bromofluorobenzene (S)100 %10/19/17 01:43 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %10/19/17 01:43 17060-07-070-130 1
Toluene-d8 (S)101 %10/19/17 01:43 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2017 02:31 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92359172
North Meck Landfill
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
382978
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92359172001, 92359172002, 92359172003, 92359172004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2122612
Associated Lab Samples:92359172001, 92359172002, 92359172003, 92359172004
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 10/18/17 23:51
1,1,1-Trichloroethane ug/L ND 1.0 10/18/17 23:51
1,1,2,2-Tetrachloroethane ug/L ND 1.0 10/18/17 23:51
1,1,2-Trichloroethane ug/L ND 1.0 10/18/17 23:51
1,1-Dichloroethane ug/L ND 1.0 10/18/17 23:51
1,1-Dichloroethene ug/L ND 1.0 10/18/17 23:51
1,2,3-Trichloropropane ug/L ND 1.0 10/18/17 23:51
1,2-Dibromo-3-chloropropane ug/L ND 2.0 10/18/17 23:51
1,2-Dibromoethane (EDB)ug/L ND 1.0 10/18/17 23:51
1,2-Dichlorobenzene ug/L ND 1.0 10/18/17 23:51
1,2-Dichloroethane ug/L ND 1.0 10/18/17 23:51
1,2-Dichloropropane ug/L ND 1.0 10/18/17 23:51
1,4-Dichlorobenzene ug/L ND 1.0 10/18/17 23:51
2-Butanone (MEK)ug/L ND 5.0 10/18/17 23:51
2-Hexanone ug/L ND 5.0 10/18/17 23:51
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 10/18/17 23:51
Acetone ug/L ND 25.0 10/18/17 23:51
Acrylonitrile ug/L ND 10.0 10/18/17 23:51
Benzene ug/L ND 1.0 10/18/17 23:51
Bromochloromethane ug/L ND 1.0 10/18/17 23:51
Bromodichloromethane ug/L ND 1.0 10/18/17 23:51
Bromoform ug/L ND 1.0 10/18/17 23:51
Bromomethane ug/L ND 2.0 10/18/17 23:51
Carbon disulfide ug/L ND 2.0 10/18/17 23:51
Carbon tetrachloride ug/L ND 1.0 10/18/17 23:51
Chlorobenzene ug/L ND 1.0 10/18/17 23:51
Chloroethane ug/L ND 1.0 10/18/17 23:51
Chloroform ug/L ND 1.0 10/18/17 23:51
Chloromethane ug/L ND 1.0 10/18/17 23:51
cis-1,2-Dichloroethene ug/L ND 1.0 10/18/17 23:51
cis-1,3-Dichloropropene ug/L ND 1.0 10/18/17 23:51
Dibromochloromethane ug/L ND 1.0 10/18/17 23:51
Dibromomethane ug/L ND 1.0 10/18/17 23:51
Ethylbenzene ug/L ND 1.0 10/18/17 23:51
Iodomethane ug/L ND 5.0 10/18/17 23:51
Methylene Chloride ug/L ND 1.0 10/18/17 23:51
Styrene ug/L ND 1.0 10/18/17 23:51
Tetrachloroethene ug/L ND 1.0 10/18/17 23:51
Tetrahydrofuran ug/L ND 10.0 10/18/17 23:51
Toluene ug/L ND 1.0 10/18/17 23:51
trans-1,2-Dichloroethene ug/L ND 1.0 10/18/17 23:51
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2017 02:31 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92359172
North Meck Landfill
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2122612
Associated Lab Samples:92359172001, 92359172002, 92359172003, 92359172004
Matrix:Water
Analyzed
trans-1,3-Dichloropropene ug/L ND 1.0 10/18/17 23:51
trans-1,4-Dichloro-2-butene ug/L ND 1.0 10/18/17 23:51
Trichloroethene ug/L ND 1.0 10/18/17 23:51
Trichlorofluoromethane ug/L ND 1.0 10/18/17 23:51
Vinyl acetate ug/L ND 2.0 10/18/17 23:51
Vinyl chloride ug/L ND 1.0 10/18/17 23:51
Xylene (Total)ug/L ND 1.0 10/18/17 23:51
1,2-Dichloroethane-d4 (S)%99 70-130 10/18/17 23:51
4-Bromofluorobenzene (S)%104 70-130 10/18/17 23:51
Toluene-d8 (S)%101 70-130 10/18/17 23:51
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2122613LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 44.650 89 80-125
1,1,1-Trichloroethane ug/L 51.050 102 71-129
1,1,2,2-Tetrachloroethane ug/L 38.8 L2507879-124
1,1,2-Trichloroethane ug/L 47.850 96 85-125
1,1-Dichloroethane ug/L 50.150 100 73-126
1,1-Dichloroethene ug/L 55.250 110 66-135
1,2,3-Trichloropropane ug/L 39.450 79 75-130
1,2-Dibromo-3-chloropropane ug/L 35.450 71 71-133
1,2-Dibromoethane (EDB)ug/L 43.150 86 83-124
1,2-Dichlorobenzene ug/L 43.750 87 80-133
1,2-Dichloroethane ug/L 48.150 96 67-128
1,2-Dichloropropane ug/L 49.850 100 75-132
1,4-Dichlorobenzene ug/L 43.850 88 78-130
2-Butanone (MEK)ug/L 71.4100 71 61-144
2-Hexanone ug/L 69.2100 69 68-143
4-Methyl-2-pentanone (MIBK)ug/L 84.4100 84 72-135
Acetone ug/L 75.4100 75 48-146
Acrylonitrile ug/L 199250 79 40-160
Benzene ug/L 48.250 96 80-125
Bromochloromethane ug/L 50.150 100 71-125
Bromodichloromethane ug/L 49.150 98 78-124
Bromoform ug/L 41.050 82 71-128
Bromomethane ug/L 51.250 102 40-160
Carbon disulfide ug/L 55.950 112 50-160
Carbon tetrachloride ug/L 52.850 106 69-131
Chlorobenzene ug/L 44.450 89 81-122
Chloroethane ug/L 52.550 105 39-148
Chloroform ug/L 48.050 96 73-127
Chloromethane ug/L 46.350 93 44-146
cis-1,2-Dichloroethene ug/L 50.450 101 74-124
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2017 02:31 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92359172
North Meck Landfill
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2122613LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,3-Dichloropropene ug/L 49.250 98 72-132
Dibromochloromethane ug/L 44.550 89 78-125
Dibromomethane ug/L 48.550 97 82-120
Ethylbenzene ug/L 44.650 89 79-121
Iodomethane ug/L 98.6100 99 39-154
Methylene Chloride ug/L 53.350 107 64-133
Styrene ug/L 45.150 90 84-126
Tetrachloroethene ug/L 45.750 91 78-122
Tetrahydrofuran ug/L 378500 76 69-148
Toluene ug/L 49.350 99 80-121
trans-1,2-Dichloroethene ug/L 51.850 104 71-127
trans-1,3-Dichloropropene ug/L 47.150 94 69-141
trans-1,4-Dichloro-2-butene ug/L 26.450 53 40-160
Trichloroethene ug/L 51.350 103 78-122
Trichlorofluoromethane ug/L 50.250 100 53-137
Vinyl acetate ug/L 92.3100 92 40-160
Vinyl chloride ug/L 55.250 110 58-137
Xylene (Total)ug/L 133150 89 81-126
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2122615MATRIX SPIKE SAMPLE:
MSSpike
Result
92359468008
1,1,1,2-Tetrachloroethane ug/L 19.720 98 70-130ND
1,1,1-Trichloroethane ug/L 22.620 113 70-130ND
1,1,2,2-Tetrachloroethane ug/L 18.420 92 70-130ND
1,1,2-Trichloroethane ug/L 21.120 105 70-130ND
1,1-Dichloroethane ug/L 22.520 112 70-130ND
1,1-Dichloroethene ug/L 24.220 121 70-166ND
1,2,3-Trichloropropane ug/L 18.920 95 70-130ND
1,2-Dibromo-3-chloropropane ug/L 16.120 81 70-130ND
1,2-Dibromoethane (EDB)ug/L 19.920 100 70-130ND
1,2-Dichlorobenzene ug/L 18.820 94 70-130ND
1,2-Dichloroethane ug/L 21.020 105 70-130ND
1,2-Dichloropropane ug/L 21.920 109 70-130ND
1,4-Dichlorobenzene ug/L 19.320 97 70-130ND
2-Butanone (MEK)ug/L 38.740 97 70-130ND
2-Hexanone ug/L 35.140 88 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 39.640 99 70-130ND
Acetone ug/L 37.540 94 70-130ND
Acrylonitrile ug/L 98.5100 99 70-130ND
Benzene ug/L 21.820 109 70-148ND
Bromochloromethane ug/L 22.320 111 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2017 02:31 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92359172
North Meck Landfill
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2122615MATRIX SPIKE SAMPLE:
MSSpike
Result
92359468008
Bromodichloromethane ug/L 20.620 103 70-130ND
Bromoform ug/L 18.020 90 70-130ND
Bromomethane ug/L 19.720 98 70-130ND
Carbon disulfide ug/L 24.420 122 70-130ND
Carbon tetrachloride ug/L 22.720 113 70-130ND
Chlorobenzene ug/L 20.020 100 70-146ND
Chloroethane ug/L 23.120 116 70-130ND
Chloroform ug/L 20.820 104 70-130ND
Chloromethane ug/L 19.320 97 70-130ND
cis-1,2-Dichloroethene ug/L 22.620 113 70-130ND
cis-1,3-Dichloropropene ug/L 20.620 103 70-130ND
Dibromochloromethane ug/L 19.120 96 70-130ND
Dibromomethane ug/L 20.920 104 70-130ND
Ethylbenzene ug/L 20.120 101 70-130ND
Iodomethane ug/L 22.4 M1405670-130ND
Methylene Chloride ug/L 15.620 78 70-130ND
Styrene ug/L 20.020 100 70-130ND
Tetrachloroethene ug/L 20.720 103 70-130ND
Tetrahydrofuran ug/L 192200 96 70-130ND
Toluene ug/L 21.520 108 70-155ND
trans-1,2-Dichloroethene ug/L 22.820 114 70-130ND
trans-1,3-Dichloropropene ug/L 20.120 100 70-130ND
trans-1,4-Dichloro-2-butene ug/L 9.8 M1204970-130ND
Trichloroethene ug/L 22.220 111 69-151ND
Trichlorofluoromethane ug/L 22.520 112 70-130ND
Vinyl acetate ug/L 41.440 103 70-130ND
Vinyl chloride ug/L 23.420 117 70-130ND
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92359468007
2122614SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1-Dichloroethane ug/L NDND
1,1-Dichloroethene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2017 02:31 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92359172
North Meck Landfill
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92359468007
2122614SAMPLE DUPLICATE:
1,2-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Hexanone ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
Acrylonitrile ug/L NDND
Benzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon disulfide ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L NDND
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Ethylbenzene ug/L NDND
Iodomethane ug/L NDND
Methylene Chloride ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Tetrahydrofuran ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
trans-1,4-Dichloro-2-butene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L .49JND
Vinyl acetate ug/L NDND
Vinyl chloride ug/L NDND
Xylene (Total)ug/L NDND
1,2-Dichloroethane-d4 (S)%101 1100
4-Bromofluorobenzene (S)%103 2101
Toluene-d8 (S)%100 0100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2017 02:31 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 22
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92359172
North Meck Landfill
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2017 02:31 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 22
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92359172
North Meck Landfill
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92359172001 382978MW-5D NMLF EPA 8260
92359172002 382978MW-12D Infill EPA 8260
92359172003 382978MW-12 Infill EPA 8260
92359172004 382978MW-9 Infill EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/20/2017 02:31 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 22
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