19054_ HD Supply Soil Dec Memo Pkg 20180218

State of North Carolina | Environmental Quality | Waste Management
1646 Mail Service Center | 217 West Jones Street | Raleigh, NC 27699-1646
919 707 8200 T

February 13, 2018

Sent Via E-mail

Matt Lucarelli
Beacon Partners
610 E Morehead St, Suite 250
Charlotte, NC 28202
[e-mail]

Subject: Brownfields Property Export Soil Review
HD Supply
1414 and 1422 South Tryon Street
Charlotte, Mecklenburg County
Brownfields Project No. 19054-15-060

Dear Mr. Lucarelli,

On February 8, 2018 the Department of Environmental Quality (DEQ) Solid Waste Section (SWS)
received data from the DEQ Brownfields Program for review to assist in evaluating what type of
facility could manage the proposed export soils. Based on our review of the data, DEQ SWS
agrees with DEQ Brownfield’s recommendations as follows:

• Shallow soil from Sections 1,3,4, and 6 can be exported to a Construction & Demolition
landfill (CDLF) or Municipal Solid Waste landfill (MSWLF) facility.
• Deep soil from Sections 1,2,3,4, and 6 can be exported to a CDLF facility.

If you have questions about this correspondence or require additional information, please feel free
to contact me by phone at 919-707-8288 or by email at [e-mail].

Sincerely,

Ervin Lane
Compliance Hydrogeologist
NC Department of Environmental Quality
Division of Waste Management - Solid Waste Section

cc: Carolyn Minnich (DEQ Brownfields)
1

DRAFT DECISION MEMORANDUM
DATE: February 8, 2018

FROM: Carolyn Minnich
TO: Ervin Lane, Solid Waste Section DEQ

RE: Soil Export
HD Supply Property
1414 & 1422 S Tryon Street Charlotte, Mecklenburg County
BF # 19054-15-060

Based on the following information, it has been determined that the above referenced site, may
export soil to a C&D landfill or Subtitle D Landfill or 1213 West Morehead Street Brownfields Project Number 18057 or another location as approved by DEQ. This decision is made upon
review of the following information in partnership with DEQ Brownfields (BF) and DEQ Soil
Waste Section (SWS).

The Brownfields Property is one parcel approximately 3.502 acres and located in an industrial area. The specific address is 1414 and 1422 South Tryon Street (PIN 07309204).
Redevelopment on the Brownfields Property will be two commercial office building, parking
garage, and limited residential apartments. See figure for layout. The developer is exporting
approximately 3500 cubic yards (cy) in the coming months. A soil characterization work plan
was submitted, reviewed and approved by BF Program. The property was divided into 7 quadrants to better assess and identify problem areas. The following is a summary of the work
plan:

General Methodology
• The soil characterization activities were conducted in accordance with the Soil
Characterization Work Plan dated October 23, 2017.
• The HD Supply site was divided into 7 sections (see attached Figure).
• Five soil borings were advanced in each of Sections 1 through 6 and one soil boring was advanced in Section 7.
• Two soil samples were collected in each section, one shallow sample (ground surface to 6
inches below ground surface [bgs]) and one deeper sample was collected from 6 inches
bgs to the bottom of the boring based on the depth of the soil cut in that area.
• Soil collected from the shallow interval from each of the five borings in a given section
was homogenized and submitted for laboratory analysis of SVOCs and RCRA metals.
• Soil collected from the deeper interval from each of the five borings in a given section
was homogenized and submitted for laboratory analysis of SVOCs and RCRA metals.
• One sample was collected from both the shallow and deeper interval from each section
for VOCs analysis based on field screening results. If field screening results did not
indicate the likely presence of impacts in a given section, then the sample for VOCs
2

analysis was collected from the central most boring in a given section. Samples submitted for VOC analysis were not homogenized.

Boring and Sample Nomenclature
• Each boring/sample begins with “SC-“ for Soil Characterization.
• Following the hyphen, the number depicts the section number (SC-1 was
advanced/collected in section 1)
• If an “S” follows the section number, the S indicates shallow sample (SC-1S). This sample was a composite of soil from each of the borings from the shallow interval in a given section for SVOC and RCRA metals analysis.
• If the letter following the section number was A, B, C, D, or E, this indicates a specific
boring location within a section where a sample was collected for VOC analysis (sample
was not homogenized). If a “S” follows the boring letter (A through E), that indicates the shallow sample was collected for VOC analysis (SC-1AS indicates Shallow sample collected from boring A in Section 1).
• If “DP” follows the section number, the “DP” indicates deep sample (SC-1DP). This
sample was a composite of soil from each of the borings from the deep interval in a given section for SVOC and RCRA metals analysis.
• If the letter following the section number was A, B, C, D, or E, this indicates a specific
boring location within a section where a sample was collected for VOC analysis (sample
was not homogenized). If “DP” follows the boring letter (A through E), that indicates the
deeper sample was collected for VOC analysis (SC-1EDP indicates Deeper sample collected from boring E in Section 1).

Results
• Analytical results did not indicate the presence of VOCs, SVOCs, or RCRA metals in the shallow or deep samples collected from Sections 1, 2, 3, or 4 at concentrations above
Residential PSRGs. Section 2 Shallow did have detections above Protection of
Groundwater for metals.
• The shallow soil sample collected from Section 5 indicated the presence of several SVOCs above laboratory reporting limits and benzo(a)pyrene, benzo(b)fluoranthene, and dibenzo(a,h)anthracene at concentrations above the Residential PSRGs, but below the
Commercial/Industrial PSRGs. Additionally, arsenic was detected above Residential and
Commercial/Residential PSRGs and above background levels at the Morehead Street BF
site.
• The deeper sample collected from Section 6 did not indicate the presence of VOCs or
SVOCs at concentrations above Residential or Commercial/Industrial PSRGs. Arsenic
was detected at 1.8 J mg/kg in the deeper sample from section 5 which is above the
Residential PSRG, but is below the Commercial/Industrial PSRG and below background arsenic concentrations at the Morehead Street BF Site (up to 3 mg/kg).
• The shallow soil sample collected from section 5 indicated the presence of PCE at a
concentration of 0.0024 mg/kg which is below Residential and Commercial/Industrial
PSRGs. Additionally, arsenic was detected at a concentration of 2.2 J mg/kg which is above the Residential PSRG, but below the Commercial/Industrial PSRG. No other VOCs, SVOCs, or RCRA metals were detected in the shallow or deeper soil samples
collected from section 6 at concentrations above Residential or Commercial PSRGs.
3

• Analytical results indicate the presence of PCE and TCE at low concentrations below the Residential and Commercial/Industrial PSRGs in the shallow and deeper samples
collected from section 7. No SVOCs or RCRA metals were detected above Residential
or Commercial PSRGs in the soil samples collected from section 7.
• Stockpile 1 sample was collected on January 17, 2018. The soils are from Section 2 deep and is approximately 1,000 cy. No VOCs, SVOCs were detected screening levels.
Arsenic was detected at 7.2 mg/kg and then re-analyzed with a result of 1.7 mg/kg. The
second result in consistent with background metal concentrations at HD Supply Property
and surrounding area.
• DEQ Risk Calculator dated October 2017 was used to compute the soil risk for resident,
non-residential worker, construction worker, and user defined in surface soil and
subsurface soil. No risk was detected and the Hazard Index was below 1 (more than an
order of magnitude below 1). See attached document for summary. Recommendations
• Shallow soil from Sections 1, 3, 4, and 6, can exported to C&D Landfill, Subtitle D
Landfill, or W Morehead Street BF site or another location approved by DEQ.
• Soil from Section 7 and shallow soil from Section 2, Section 5 and Section 6, should be used on site and marked on the revised plat map or transported to a Subtitle D Landfill.
• Deep soils from Section 1,2,3,4 and 6 can be exported to a C&D Landfill, if accepted by
the receiving facility.
On November 8, 2017, BF Program approved the export of soils to 1213 W. Morehead
Street, Brownfields Project Number 18057-14-060. Approximately ~4175 cu yds from Section 1
through 6 below 6 inches was exported to W Morehead Property and surficial soils from Section
1,3,and 4. The Developer has a remaining 3500 cu yds and has requested DEQ BF/SWS provide
a letter or email stating the export soils can be accepted a C&D landfill. To support this request, BF Program has reviewed and compared the analytical data to IHSB soil screening levels for
residential use and/or protection of groundwater.

4

Risk Calculator
Risk Calculator for Stockpile 1, 1000 cu yds from Section 2

5

2500 cu yds of soil to be cut and removed from the Brownfields Property below 6 inches across from Sections 1, 2, 3, 4 and 6. None from Section 7 or 5. The following is Risk
Calculator Output.

Table 1 - DRAFT
Summary of Soil Analytical Data
HD Supply Brownfields Site
1414 South Tryon Street
Charlotte, North Carolina
H&H Job No. BCP-064
Location
Sample ID SC-1CS SC-1S SC-1EDP SC-1DP SC-2BS SC-2S SC-2BDP SC-2DP SC-3BS SC-3S SC-3CDP SC-3DP SC-4BDP SC-4DP
Depth (ft bgs)0.0-0.5 0.0-0.5 0.5-2.4 0.5-2.41 0.0-0.5 0.0-0.5 0.5-2.4 0.5-2.41 0.0-0.5 0.0-0.5 0.5-2.4 0.5-2.41 0.0-0.5 0.0-0.5 0.0-0.5 0.0-0.5 0.5-2.4 0.5-2.41
Sample Date Protection of Groundwater Residential Industrial 10/26/17 10/26/17 10/26/17 10/26/17 10/26/17 10/26/17 10/26/17 10/26/17 10/25/17 10/25/17 10/25/17 10/25/17 10/25/17 10/25/17 10/25/17 10/25/17 10/25/17 10/25/17
Units (mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)
VOCs (8260B)------
Tetrachloroethylene 0.0063 1.7 8.2 <0.0016 NA <0.0018 NA <0.0013 NA <0.0014 NA <0.0012 NA <0.0015 NA <0.0013 <0.0012 NA NA <0.0015 NA
Trichloroethylene 0.0210 0.87 4.0 <0.0012 NA <0.0014 NA <0.00097 NA <0.0011 NA <0.00095 NA <0.0011 NA <0.0010 <0.00092 NA NA <0.0011 NA
SVOCs (8270C)
Anthracene 1,300 3,600 45,000 NA <0.060 NA <0.062 NA <0.063 NA <0.065 NA <0.052 NA <0.058 NA NA <0.063 <0.059 NA <0.062
Benzo(a)anthracene 0.35 1.1 21 NA <0.055 NA <0.057 NA <0.058 NA <0.059 NA <0.048 NA <0.053 NA NA <0.058 <0.054 NA <0.057
Benzo(a)pyrene 0.12 0.11 2.1 NA <0.065 NA <0.067 NA <0.068 NA <0.070 NA <0.056 NA <0.063 NA NA <0.068 <0.063 NA <0.067
Benzo(b)fluoranthene 1.2 1.1 21 NA <0.059 NA <0.061 NA 0.075 J NA <0.063 NA <0.051 NA <0.057 NA NA <0.062 <0.057 NA <0.061
Benzo(g,h,i)perylene 15,600 NS NS NA <0.092 NA <0.095 NA <0.097 NA <0.099 NA <0.079 NA <0.089 NA NA <0.097 <0.090 NA <0.095
Benzo(k)fluoranthene 1.2 11 210 NA <0.065 NA <0.067 NA <0.068 NA <0.070 NA <0.056 NA <0.063 NA NA <0.068 <0.063 NA <0.067
Bis(2-Ethylhexyl)phthalate 14 39 160 NA <0.16 NA <0.17 NA <0.17 NA <0.17 NA <0.14 NA <0.16 NA NA <0.17 <0.16 NA <0.17
Butylbenzylphthalate 290 290 1200 NA <0.099 NA <0.10 NA <0.10 NA <0.11 NA <0.086 NA <0.096 NA NA <0.10 <0.097 NA <0.10
Carbazole 0.74 NS NS NA <0.054 NA <0.056 NA <0.057 NA <0.058 NA <0.046 NA <0.052 NA NA <0.057 <0.053 NA <0.056
Chrysene 36 110 2100 NA <0.065 NA <0.067 NA <0.068 NA <0.070 NA <0.056 NA <0.063 NA NA <0.068 <0.063 NA <0.067
Dibenz(a,h)anthracene 0.38 0.11 2.1 NA <0.13 NA <0.13 NA <0.13 NA <0.14 NA <0.11 NA <0.12 NA NA <0.13 <0.12 NA <0.13
Fluoranthene 670 480 6000 NA <0.069 NA <0.071 NA 0.10 J NA <0.074 NA <0.059 NA <0.067 NA NA <0.072 <0.067 NA <0.071
Indeno(1,2,3-cd)pyrene 3.9 1.1 21 NA <0.15 NA <0.15 NA <0.16 NA <0.16 NA <0.13 NA <0.14 NA NA <0.16 <0.15 NA <0.16
Phenanthrene 134 NS NS NA <0.11 NA <0.11 NA <0.11 NA <0.12 NA <0.093 NA <0.10 NA NA <0.11 <0.11 NA <0.11
Pyrene 440 360 4500 NA <0.069 NA <0.071 NA 0.11 J NA <0.074 NA <0.059 NA <0.067 NA NA <0.072 <0.067 NA <0.071
RCRA Metals (6010/7174)
Arsenic 5.8 0.68 3.0 NA <1.6 NA <1.6 NA <1.6 NA <1.7 NA <1.3 NA <1.6 NA NA <1.6 <1.5 NA <1.5
Barium 580 3,100 47,000 NA 150 NA 61 NA 110 NA 75 NA 120 NA 27 NA NA 63 61 NA 70
Cadmium 3.0 7.5 110 NA 4.0 NA 4.1 NA 4.1 NA 3.3 NA 1.5 NA 3.0 NA NA 1.5 1.3 NA 2.7
Chromium*360,000 23,000 100,000 NA 130 NA 56 NA 61 NA 50 NA 16 NA 22 NA NA 21 16 NA 33
Lead 270 NS NS NA 53 NA 21 NA 45 NA 10 NA 4.9 NA <0.93 NA NA 22 41 NA 11
Mercury 1.0 2.3 3.1 NA 0.15 NA 0.080 NA 0.055 NA 0.050 NA 0.018 NA 0.045 NA NA 0.30 0.074 NA 0.055
Silver 3.4 78 1,200 NA 2.4 NA 2.6 NA 2.1 NA 2.2 NA 0.98 NA 2.0 NA NA <0.36 <0.36 NA 1.5
Notes:
1) Composite sample collected from multiple depth intervals based on proposed soil cut depths.
The maximum cut depth at each boring is depicted in the depth interval range
2) Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch Preliminary Soil Remedial Goals (October 2017)
VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; RCRA = Resource Conservation and Recovery Act
Samples for SVOCs and RCRA Metals collected as composite samples from five aliquots in each section
from shallow (S) and deep (DP) intervals
VOCs grab samples were collected from the boring in each section with the greatest potential for impacts based on field screening results
Only those compounds detected in at least one sample are shown above
Underline indicates concentration exceeds the Inactive Hazardous Sites Branch Protection of Residential Preliminary Soil Remedial Goal
Bold and Underline indicates concentration exceeds the Inactive Hazardous Sites Branch
Protection of Groundwater Preliminary Soil Remedial Goal
Method number follows parameter in parenthesis
NA = Not Analyzed; NS = Not Specified
BDL = Below detection limit
mg/kg = milligrams per kilogram
*Chromium III PSRG used for residential and industrial
DEQ Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation
Goals (PSRGs)2
Section 1 Section 2 Section 3 Section 4
SC-4ES/DUP-1 SC-4S/DUP1
\\hhfs01.harthickman.local\masterfiles\AAA-Master Projects\Beacon Partners- BEP or BCP\BCP-064 1414 and 1422 S. Tryon\brownfields\Soil Characterization\Tables\Soil Analytical Data for LF
1/25/2018
Table 1
Hart & Hickman, PC
Table 1 - DRAFT
Summary of Soil Analytical Data
HD Supply Brownfields Site
1414 South Tryon Street
Charlotte, North Carolina
H&H Job No. BCP-064
Location
Sample ID
Depth (ft bgs)
Sample Date Protection of Groundwater Residential Industrial
Units (mg/kg)(mg/kg)(mg/kg)
VOCs (8260B)------
Tetrachloroethylene 0.0063 1.7 8.2
Trichloroethylene 0.0210 0.87 4.0
SVOCs (8270C)
Anthracene 1,300 3,600 45,000
Benzo(a)anthracene 0.35 1.1 21
Benzo(a)pyrene 0.12 0.11 2.1
Benzo(b)fluoranthene 1.2 1.1 21
Benzo(g,h,i)perylene 15,600 NS NS
Benzo(k)fluoranthene 1.2 11 210
Bis(2-Ethylhexyl)phthalate 14 39 160
Butylbenzylphthalate 290 290 1200
Carbazole 0.74 NS NS
Chrysene 36 110 2100
Dibenz(a,h)anthracene 0.38 0.11 2.1
Fluoranthene 670 480 6000
Indeno(1,2,3-cd)pyrene 3.9 1.1 21
Phenanthrene 134 NS NS
Pyrene 440 360 4500
RCRA Metals (6010/7174)
Arsenic 5.8 0.68 3.0
Barium 580 3,100 47,000
Cadmium 3.0 7.5 110
Chromium*360,000 23,000 100,000
Lead 270 NS NS
Mercury 1.0 2.3 3.1
Silver 3.4 78 1,200
Notes:
1) Composite sample collected from multiple depth intervals based on proposed soil cut depths.
The maximum cut depth at each boring is depicted in the depth interval range
2) Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch Preliminary Soil Remedial Goals (October 2017)
VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; RCRA = Resource Conservation and Recovery Act
Samples for SVOCs and RCRA Metals collected as composite samples from five aliquots in each section
from shallow (S) and deep (DP) intervals
VOCs grab samples were collected from the boring in each section with the greatest potential for impacts based on field screening results
Only those compounds detected in at least one sample are shown above
Underline indicates concentration exceeds the Inactive Hazardous Sites Branch Protection of Residential Preliminary Soil Remedial Goal
Bold and Underline indicates concentration exceeds the Inactive Hazardous Sites Branch
Protection of Groundwater Preliminary Soil Remedial Goal
Method number follows parameter in parenthesis
NA = Not Analyzed; NS = Not Specified
BDL = Below detection limit
mg/kg = milligrams per kilogram
*Chromium III PSRG used for residential and industrial
DEQ Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation
Goals (PSRGs)2 SC-5CS SC-5S SC-5CDP SC-5DP SC-6CS SC-6S SC-6CDP SC-6DP SC-7S SC-7DP
0.0-0.5 0.0-0.5 0.5-1.4 0.5-1.81 0.0-0.5 0.0-0.5 0.5-1 0.5-1.31 0.0-0.5 0.5-1.51
10/25/17 10/25/17 10/25/17 10/25/17 10/25/17 10/25/17 10/25/17 10/25/17 10/25/17 10/25/17 1/17/18
(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)
<0.0014 NA <0.0013 NA 0.0024 NA <0.0014 NA 0.066 0.014 <0.005
<0.0011 NA <0.0010 NA <0.0012 NA <0.0011 NA 0.0036 0.0012 J <0.005
NA 0.078 J NA <0.066 NA <0.063 NA <0.063 <0.061 <0.064 <0.418
NA 0.75 NA <0.060 NA <0.058 NA <0.058 <0.056 <0.059 <0.418
NA 1.0 NA <0.071 NA <0.068 NA <0.068 <0.066 <0.069 <0.418
NA 1.6 NA <0.064 NA <0.062 NA <0.062 <0.060 <0.063 <0.418
NA 0.83 NA <0.10 NA <0.097 NA <0.096 <0.093 <0.098 <0.418
NA 0.54 NA <0.071 NA <0.068 NA <0.068 <0.066 <0.069 <0.418
NA 0.16 J NA <0.18 NA <0.17 NA <0.17 <0.16 <0.17 <0.418
NA 0.21 J NA <0.11 NA <0.10 NA <0.10 <0.10 <0.11 <0.418
NA 0.072 J NA <0.059 NA <0.057 NA <0.056 <0.055 <0.057 <0.418
NA 1.0 NA <0.071 NA <0.068 NA <0.068 <0.066 <0.069 <0.418
NA 0.17 NA <0.14 NA <0.13 NA <0.13 <0.13 <0.14 <0.418
NA 1.7 NA <0.075 NA <0.072 NA <0.072 <0.070 <0.073 <0.418
NA 0.86 NA <0.16 NA <0.16 NA <0.16 <0.15 <0.16 <0.418
NA 0.64 NA <0.12 NA <0.11 NA <0.11 <0.11 <0.11 <0.418
NA 1.7 NA <0.075 NA <0.072 NA <0.072 <0.070 <0.073 <0.418
NA 27 NA 1.8 J NA 2.2 J NA <1.7 <1.6 <1.7 7.2
NA 100 NA 83 NA 83 NA 92 48 43 56.8
NA 3.1 NA 2.3 NA 2.3 NA 2.8 3.6 4.5 0.15
NA 45 NA 42 NA 29 NA 63 70 92 24.2
NA 130 NA 38 NA 50 NA 0.66 J 1.4 <0.59 13.2
NA 0.11 NA 0.079 NA 0.084 NA 0.037 0.10 0.077 0.048
NA 0.95 NA 1.3 NA 1.3 NA 1.2 2.3 3 1
Stockpile-1
Section 5 Section 6 Section 7
\\hhfs01.harthickman.local\masterfiles\AAA-Master Projects\Beacon Partners- BEP or BCP\BCP-064 1414 and 1422 S. Tryon\brownfields\Soil Characterization\Tables\Soil Analytical Data for LF
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Table 1
Hart & Hickman, PC
SOUTH TRY
ON ST
RE
ET
WIN
O
N
A

S
T
R
E
E
T
WINNIF
RED ST
REET
B
L
A
N
D

S
T
R
E
E
T
SB-7
SB-1
SB-5
SB-3
SB-2
SB-4
SB-6
SB-8
SB-10
SB-9
SC-5B
SC-5A
SC-5E
SC-5D SC-5C
SC-6A
SC-6B
SC-6E
SC-6CSC-6D
SC-4B
SC-4A
SC-4B
SC-4E
SC-4D
SC-3B
SC-3E
SC-3D SC-3C
SC-3A
SC-1B
SC-1A
SC-1C
SC-1E
SC-1D
SC-2B
SC-2A
SC-2C
SC-2E
SC-2D
LEGEND
SITE PROPERTY BOUNDARY
DENOTES AREA TO BE CUT
DENOTES AREA TO BE FILLED
SECTION NUMBER
SURFACE SOIL ALIQUOT LOCATION
SURFACE & SUBSURFACE SOIL
ALIQUOT LOCATION
SOIL BORING LOCATION
AREA OF POTENTIAL SOIL
CONTAMINATION
REVISION NO. 0DATE: 11-3-17
JOB NO. BCP-064 FIGURE NO. 3
HD SUPPLY BROWNFIELDS SITE
1414 AND 1422 SOUTH TRYON STREET
CHARLOTTE, NORTH CAROLINA
CUT/FILL AND SAMPLE LOCATION MAP
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
C
F
1
1
3
6
2
4
7
5
S:\AAA-Master Projects\Beacon Partners- BEP or BCP\BCP-064 1414 and 1422 S. Tryon\brownfields\Figures\Cut Fill Map.dwg, FIG 3, 11/6/2017 11:50:28 AM, TDeSa
77665544332.52.5221.51.511J6.86.81' - 4" 2' - 8"46' - 4"21' - 8"18' - 8" 5' - 8" 10' - 0" 10' - 0"1' - 11"8' - 1"KLMM.8NN.8PP.4QQ.6SJ.9A1S500A3S500.A4S500.A6S500.25' - 0"25' - 0"25' - 0"25' - 0"25' - 0"24' - 8" 11' - 0"25' - 0" 5' - 4"14' - 8" 10' - 0" 4' - 4" 6' - 8"25' - 0"25' - 0"25' - 0"25' - 0"25' - 0"24' - 8" 11' - 0"5' - 4" 19' - 8"14' - 8" 10' - 0" 4' - 4" 6' - 8"26' - 10"19' - 6" 3' - 0" 18' - 8" 6' - 8" 12' - 0"F10x12F10F10F9F9F10F11F10F9F9F9F9F8MATCHLINE AREA "A"MATCHLINE AREA "B"S310D5.OPP. HANDF5F5( 747' - 0" )( 747' - 0" )( 747' - 0" )( 747' - 0" )( 746' - 6" )( 746' - 0" )( 747' - 6" )( 746' - 6" )D1S502W10X22{-0' - 8"}CJCJC3S301.C2S301.C4S301.F5AF5AF5AF5AF63' - 6"F7X10.33( 747' - 6" )F5AF15F15F15F15D1S301D1S301D1S301F42x14F5F5( 746' - 6" )( 746' - 6" )10' - 2"13' - 2"7' - 0" 7' - 0"1' - 4"1' - 4"7' - 8" 7' - 8"2' - 0"5 3/8"3' - 4"5 3/8"D2S402.D1S402.OPP. HANDOPP. HANDHSS8X8X1/4HSS8X8X1/4HSS8X8X1/4HSS8X8X1/4HSS8X8X1/4HSS8X8X1/4HSS8X8X1/4YP. FOR ELEV. UIDE RAIL UPPORTS
1010998877665544332.52.5221.51.511JJHHGGFFD.4D.4DC.2CCB.6B.6BBAAA.4EH.2H.86.86.8A2S500A5S500A6S50029' - 8"26' - 8"25' - 0"25' - 0"25' - 0"25' - 0"25' - 0"24' - 8" 4' - 4" 6' - 8"14' - 8" 10' - 0"10' - 0"64' - 0"10' - 0" 10' - 0" 5' - 8" 18' - 8"21' - 8"46' - 4"4' - 0"12' - 0" 6' - 8" 18' - 8" 3' - 0" 19' - 6"26' - 10" 2' - 8" 1' - 4"29' - 8"26' - 8"25' - 0"25' - 0"25' - 0"25' - 0"25' - 0"24' - 8" 4' - 4" 6' - 8"14' - 8" 10' - 0"1' - 11"8' - 1" 10' - 0"44' - 0"10' - 0"5' - 4" 19' - 8"5' - 4" 19' - 8"A3S500KKJ.9J.9A1S500A4S500F9F9F9F9F9F8F10F11F11F7F7F9F10F7X10.33F5F10F10F10F9AF11AF5F5F10AF10x12H.5H.5B5S501MATCHLINE AREA "A"MATCHLINE AREA "B"MATCHLINE AREA "A"MATCHLINE AREA "D"F11F12-5' - 6"A3S301S310D1.S310D5.A2S311F5F5.( 747' - 6" )C2S301C4S301CJCJCJCJCJCJCJCJCJCJCJCJS300C2D5S300C2S301.C3S301CJCJCJCJCJCJCJCJCJCJCJCJCJCJCJCJCJS300C2S300C2S300C2S300C2S300C2S300C2S300C2CJCJD1S502.{-0' - 8"}W16X26W12X22B4S300TYPA1S301CJF5AF5AF5AF5AF6F6F5AF5AF5AF5AF5A3' - 6"F5AF15F15F15F15D1S301D1S301D1S301F42x14F5F510' - 2"13' - 2"7' - 0" 7' - 0"D2S4021' - 4"1' - 4"7' - 8" 7' - 8"2' - 0"HSS8X8X1/4HSS8X8X1/4HSS8X8X1/4HSS8X8X1/4HSS8X8X1/4D1S4025 3/8"3' - 4"5 3/8"1' - 4"1' - 4"7' - 8" 7' - 8"2' - 0"5 3/8"D1S402.OPP. HANDOPP. HANDHSS8X8X1/4HSS8X8X1/4HSS8X8X1/4HSS8X8X1/4HSS8X8X1/4
HSS8X8X1/4HSS8X8X1/41' - 3 3/4"4' - 2"HSS12X4X1/2HSS8X6X3/8HSS8X6X3/8HSS8X6X3/8HSS8X6X3/8S400C5.TYP. FOR ELEV. GUIDE RAIL SUPPORTS6' - 0" 6' - 0"F-37' - 8"F-33' - 7 3/8"F-34' - 0"F-310' - 6"7' - 5 1/2"COORDINATE ELEVATOR LOCATION WITH PRECAST DRAWINGS.F-32' - 0"F-37' - 4 3/4" 1' - 6 1/2"F-3F-315' - 9 1/4"5' - 6 3/4"10"FOUNDATION PLAN 1. FINISHED FIRS ELEVATION OF 2. TOP OF FOOTIN ( ) REFEREN 3. INDICAT 4. SLABS-ON-GRA • GENE • OFFIC • PARK REFE 5. REFERENCE SH REFERENCE SH 6. REFERENCE S0 7. VERIFY DIMENS CONTRACTOR FXSTRUCTURAL STEEL COATING NOTE 1:THE COMPONENTS IDENTIFIED WITH THIS CALLOUT ON APPLICABLE DETAILS AND ELEVATIONS ARE TO BE EXPOSED AND WILL BE COVERED WITH AN INTUMESCENT PAINT. PAINT WITH COMPATIBLE PRIMER. COORDINATE PRIMER REQUIREMENTS WITH ARCHITECT.STRUCTURAL STEEL COATING NOTE 2:THE COMPONENTS IDENTIFIED WITH THIS CALLOUT ON APPLICABLE DETAILS AND ELEVATIONS ARE TO BE EXPOSED AND WILL BE COVERED WITH AN FINISHED COAT OF PAINT. COAT WITH A COMPATIBLE PRIMER. COORDINATE PRIMER REQUIREMENTS WITH ARCHITECT.COPYRIGHT 2017SCALE: 3/4" = 1'-0"S201.aPAINT NOTE 1N1NOTESCALE: 3/4" = 1'-0"S201.aPAINT NOTE 2N2NOTE1098765432.521.51J6.81' - 4" 2' - 8"46' - 4"21' - 8"18' - 8" 5' - 8" 10' - 0" 10' - 0"1' - 11"8' - 1"KLMM.8NN.8PP.4QQ.6SJ.9A1S500A5S500.A3S500.A4S500.A6S500.29' - 8"26' - 8"25' - 0"25' - 0"25' - 0"25' - 0"25' - 0"24' - 8" 11' - 0"5' - 4" 19' - 8"14' - 8" 10' - 0" 4' - 4" 6' - 8"26' - 10"19' - 6" 3' - 0" 18' - 8" 6' - 8" 12' - 0"F10AF10x12F10F10F10F9F9F10F11F12F11F11F10F9F9F9F9F8F7F7MATCHLINE AREA "A"MATCHLINE AREA "B"MATCHLINE AREA "B"MATCHLINE AREA "C"S310D5.S310D1.OPP. HANDOPP. HANDF5F5A3S301( 747' - 6" )( 747' - 6" )( 747' - 0" )( 747' - 0" )( 747' - 0" )( 747' - 0" )( 747' - 0" )( 746' - 6" )( 746' - 0" )( 747' - 6" )( 746' - 6" )D1S502CJCJCJCJCJCJD5S300W10X22{-0' - 8"}CJS300C2S300C2S300C2CJCJCJCJCJCJCJCJCJB4S300W12X22C3S301.C2S301.C4S301.F5AF5AF5AF5AF63' - 6"F7X10.33( 747' - 6" )F5AA1S301.CJF15F15F15F15D1S301D1S301D1S301F42x14F5F5( 746' - 6" )( 746' - 6" )10' - 2"13' - 2"7' - 0" 7' - 0"1' - 4"1' - 4"7' - 8" 7' - 8"2' - 0"5 3/8"3' - 4"5 3/8"D2S402.D1S402.OPP. HANDOPP. HANDHSS8X8X1/4HSS8X8X1/4HSS8X8X1/4HSS8X8X1/4HSS8X8X1/4HSS8X8X1/4
HSS8X8X1/44' - 2"1' - 3 3/4"3' - 6 3/4"HSS8X6X3/8HSS12X4X1/2HSS8X6X3/8HSS8X6X3/8HSS8X6X3/8S400C5.TYP. FOR ELEV. GUIDE RAIL SUPPORTS3' - 8"F-34' - 0"F-310' - 6"COORDINATE ELEVATOR LOCATION WITH PRECAST DRAWINGS.F-37' - 8"F-37' - 5 1/2"2' - 0"F-315' - 9 1/4"5' - 6 3/4"F-3F-37' - 4 3/4"EOS1' - 6 1/2"1112VpdMATCHLINE AREA "B"MATCHLINE AREA "C"MATCHLINE AREA "C"MATCHLINE AREA "D"S310D3.8' - 0"8' - 0" 8' - 0"8' - 0" 8' - 0"8' - 0" 8' - 0"8' - 0" 8' - 0"4' - 0" 4' - 0"8000 PSF MAX. BEARING PRESSUREWALL FOOTING 12'-0" WIDE X 4'-0" THICK WITH #7 @ 12" O.C. EACH WAY TOP AND BOTTOMADD #11 X 12'-0" TOP BARS AND #7 X 12'-0" BOTTOM BARS @ 12" O.C. STAGGERED WITH TYPICAL #7 BARS. CENTER ON GRID LINE.26' - 0"8000 PSF MAX. BEARING PRESSURE6000 PSF MAX. BEARING PRESSUREB2S311.B2S311.FOOTINGSTEP( 748' - 6" )FOOTINGSTEP( 745' - 6" )( 746' - 6" )( 746' - 6" )( 748' - 6" )FOOTINGSTEPB5S301S300C2S300C2CJCJCJCJCJCJCJCJCJCJCJCJCJCJCJCJCJCJCJCJCJCJREPRESENTS COLUMN FOR RESIDENTIAL STRUCTURE. COORDINATE COLUMN CONNECTION REQUIREMENTS WITH RESIDENTIAL STRUCTURE DRAWINGS (TYP.0D5S300D5S300CJUpdUpdXWpd( 748' - 6" )( 746' - 6" )( 746' - 6" )16' - 7" 18' - 6"25' - 11"F-214' - 6"F-24' - 0"4' - 0"CENTER FOOTING UNDER PRECAST WALL. REFERENCE PRECAST DRAWINGS FOR WALL DIMENSION.F-36' - 0"6' - 0"CENTER FOOTING UNDER PRECAST WALL. REFERENCE PRECAST DRAWINGS FOR WALL DIMENSION.F-34' - 0" 4' - 0"F-361' - 0"COORDINATE RESIDENTIAL ELEVATOR PIT DIMENSIONS WITH RESIDENTIAL DRAWINGS.F-31112RpdMATCHLINE AREA "A"MATCHLINE AREA "D"MATCHLINE AREA "C"MATCHLINE AREA "D"WALL FOOTING 12'-0" WIDE X 4'-0" THICK WITH #7 @ 12" O.C. EACH WAY TOP AND BOTTOMADD #11 X 12'-0" TOP BARS AND #7 X 12'-0" BOTTOM BARS @ 12" O.C. STAGGERED WITH TYPICAL #7 BARS. CENTER ON GRID LINE.26' - 0"8000 PSF MAX. BEARING PRESSURE6000 PSF MAX. BEARING PRESSUREWALL FOOTING 8'-0" WIDE X 2'-6" THICK WITH #6 @ 12" O.C. BOTH DIRECTIONS TOP AND BOTTOMCONTINUE SAME REINFORCING INTO FOOTING EXTENSIONS AT RESIDENTIAL COLUMNS.B2S3118000 PSF MAX. BEARING PRESSURE8' - 0"8' - 0"8' - 0"8' - 0"6000 PSF MAX. BEARING PRESSURE8' - 0" 8' - 0"8' - 0"8' - 0"C1S311.C1S311.C1S311.4' - 0" 4' - 0"B2S311.( 746' - 6" )( 745' - 6" )FOOTINGSTEP( 746' - 6" )( 748' - 6" )FOOTINGSTEPFOOTINGSTEPB5S301S300C2CJCJCJCJCJCJCJCJCJCJCJCJCJCJCJCJCJCJCJCJCJCJCJCJCJCJCJCJREPRESENTS COLUMN FOR RESIDENTIAL STRUCTURE. COORDINATE COLUMN CONNECTION REQUIREMENTS WITH RESIDENTIAL STRUCTURE DRAWINGS (TYP.0D5S300CJCJCJCJCJCJCJCJCJSpdTpdQpdFOOTINGSTEP( 748' - 6" )( 746' - 6" )4' - 0" 4' - 0"( 748' - 6" )( 746' - 6" )C1S31120' - 11 1/2"F-214' - 6"F-27' - 10 1/2"F-220' - 11 1/2"F-2F-26' - 0" 6' - 0"CENTER FOOTING UNDER PRECAST WALL. REFERENCE PRECAST DRAWINGS FOR WALL DIMENSION.F-34' - 0" 4' - 0"CENTER FOOTING UNDER PRECAST WALL. REFERENCE PRECAST DRAWINGS FOR WALL DIMENSION.F-34' - 0"5' - 4"6' - 2"F-3COORDINATE RESIDENTIAL ELEVATOR PIT DIMENSIONS WITH RESIDENTIAL DRAWINGS.F-3221,017 cu ft1,017 cu ft4,091 cu ft1,017 cu ft4,091 cu ft1,017 cu ft4,745 cu ft4,068 cu ft3,502 cu ft4,319 cu ft4,983 cu ft4,378 cu ft8,230 cu ft1,331 cu ft421 cu ft421 cu ft298 cu ft241 cu ft241 cu ft241 cu ft191 cu ft241 cu ft97 cu ft97 cu ft3,067 cu ft50 cu ft50 cu ft
#=CL#
January 29, 2018
LIMS USE: FR - NATHAN O'LEARY
LIMS OBJECT ID: 92371171
92371171
Project:
Pace Project No.:
RE:
Mr. Nathan O'Leary
Hart & Hickman
2923 S. Tryon St
Charlotte, NC 28203
BCP-064
Dear Mr. O'Leary:
Enclosed are the analytical results for sample(s) received by the laboratory on January 18, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 11
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92371171
BCP-064
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Certification: #346
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
Nevada Certification: FL NELAC Reciprocity
New Jersey Certification #: FL022
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
Wyoming Certification: FL NELAC Reciprocity
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 11
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92371171
BCP-064
Lab ID Sample ID Matrix Date Collected Date Received
92369939003 Stockpile-1 Arsenic re-run Solid 01/17/18 11:45 01/18/18 10:51
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 11
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92371171
BCP-064
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92369939003 Stockpile-1 Arsenic re-run EPA 6010 1 PASI-OMMT
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 11
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92371171
BCP-064
Sample:Stockpile-1 Arsenic re-run Lab ID:92369939003 Collected:01/17/18 11:45 Received:01/18/18 10:51 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Arsenic 1.7 mg/kg 01/27/18 21:45 7440-38-2 M1,R101/27/18 00:450.67 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 20.5 %01/18/18 15:450.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:52 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 11
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92371171
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
421625
EPA 3050
EPA 6010
6010 MET Solid
Associated Lab Samples:92369939003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2295905
Associated Lab Samples:92369939003
Matrix:Solid
Analyzed
Arsenic mg/kg ND 0.60 01/27/18 21:37
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2295906LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 13.814.6 95 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2295907MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92369939003
2295908
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg M1,R118.1 70 75-12562 24 2015.61.7 14.3 11.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:52 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 11
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92371171
BCP-064
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
Pace Analytical Services - Ormond BeachPASI-O
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:52 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 11
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92371171
BCP-064
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92369939003 421625 421633Stockpile-1 Arsenic re-run EPA 3050 EPA 6010
92369939003 395670Stockpile-1 Arsenic re-run ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:52 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 11
Page 9 of 11
Page 10 of 11
Page 11 of 11
#=CL#
January 29, 2018
LIMS USE: FR - NATHAN O'LEARY
LIMS OBJECT ID: 92369939
92369939
Project:
Pace Project No.:
RE:
Mr. Nathan O'Leary
Hart & Hickman
2923 S. Tryon St
Charlotte, NC 28203
BCP-064
Dear Mr. O'Leary:
Enclosed are the analytical results for sample(s) received by the laboratory on January 18, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 41
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92369939
BCP-064
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Certification: #346
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
Nevada Certification: FL NELAC Reciprocity
New Jersey Certification #: FL022
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
Wyoming Certification: FL NELAC Reciprocity
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 41
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92369939
BCP-064
Lab ID Sample ID Matrix Date Collected Date Received
92369939001 STOCKPILE-1 Solid 01/17/18 11:45 01/18/18 10:51
92369939002 STOCKPILE-2 Solid 01/17/18 12:00 01/18/18 10:51
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 41
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92369939
BCP-064
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92369939001 STOCKPILE-1 EPA 6010 7 PASI-OMMT
EPA 7471 1 PASI-OAMS
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92369939002 STOCKPILE-2 EPA 6010 7 PASI-OSC1
EPA 7471 1 PASI-OMLO
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92369939
BCP-064
Sample:STOCKPILE-1 Lab ID:92369939001 Collected:01/17/18 11:45 Received:01/18/18 10:51 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Arsenic 7.2 mg/kg 01/22/18 16:57 7440-38-201/22/18 07:301.4 1
Barium 56.8 mg/kg 01/22/18 16:57 7440-39-301/22/18 07:301.4 1
Cadmium 0.15 mg/kg 01/22/18 16:57 7440-43-901/22/18 07:300.14 1
Chromium 24.2 mg/kg 01/22/18 16:57 7440-47-301/22/18 07:300.71 1
Lead 13.2 mg/kg 01/22/18 16:57 7439-92-101/22/18 07:301.4 1
Selenium ND mg/kg 01/22/18 16:57 7782-49-201/22/18 07:302.1 1
Silver 1.0 mg/kg 01/22/18 16:57 7440-22-401/22/18 07:300.71 1
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury 0.048 mg/kg 01/22/18 12:22 7439-97-601/20/18 10:440.018 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 01/22/18 09:18 83-32-901/18/18 16:034181
Acenaphthylene ND ug/kg 01/22/18 09:18 208-96-801/18/18 16:034181
Aniline ND ug/kg 01/22/18 09:18 62-53-301/18/18 16:034181
Anthracene ND ug/kg 01/22/18 09:18 120-12-701/18/18 16:034181
Benzo(a)anthracene ND ug/kg 01/22/18 09:18 56-55-301/18/18 16:034181
Benzo(a)pyrene ND ug/kg 01/22/18 09:18 50-32-801/18/18 16:034181
Benzo(b)fluoranthene ND ug/kg 01/22/18 09:18 205-99-201/18/18 16:034181
Benzo(g,h,i)perylene ND ug/kg 01/22/18 09:18 191-24-201/18/18 16:034181
Benzo(k)fluoranthene ND ug/kg 01/22/18 09:18 207-08-901/18/18 16:034181
Benzoic Acid ND ug/kg 01/22/18 09:18 65-85-001/18/18 16:0320901
Benzyl alcohol ND ug/kg 01/22/18 09:18 100-51-601/18/18 16:038361
4-Bromophenylphenyl ether ND ug/kg 01/22/18 09:18 101-55-301/18/18 16:034181
Butylbenzylphthalate ND ug/kg 01/22/18 09:18 85-68-7 L101/18/18 16:034181
4-Chloro-3-methylphenol ND ug/kg 01/22/18 09:18 59-50-701/18/18 16:038361
4-Chloroaniline ND ug/kg 01/22/18 09:18 106-47-801/18/18 16:0320901
bis(2-Chloroethoxy)methane ND ug/kg 01/22/18 09:18 111-91-101/18/18 16:034181
bis(2-Chloroethyl) ether ND ug/kg 01/22/18 09:18 111-44-401/18/18 16:034181
2-Chloronaphthalene ND ug/kg 01/22/18 09:18 91-58-701/18/18 16:034181
2-Chlorophenol ND ug/kg 01/22/18 09:18 95-57-801/18/18 16:034181
4-Chlorophenylphenyl ether ND ug/kg 01/22/18 09:18 7005-72-301/18/18 16:034181
Chrysene ND ug/kg 01/22/18 09:18 218-01-901/18/18 16:034181
Dibenz(a,h)anthracene ND ug/kg 01/22/18 09:18 53-70-301/18/18 16:034181
Dibenzofuran ND ug/kg 01/22/18 09:18 132-64-901/18/18 16:034181
1,2-Dichlorobenzene ND ug/kg 01/22/18 09:18 95-50-101/18/18 16:034181
1,3-Dichlorobenzene ND ug/kg 01/22/18 09:18 541-73-101/18/18 16:034181
1,4-Dichlorobenzene ND ug/kg 01/22/18 09:18 106-46-701/18/18 16:034181
3,3'-Dichlorobenzidine ND ug/kg 01/22/18 09:18 91-94-101/18/18 16:0320901
2,4-Dichlorophenol ND ug/kg 01/22/18 09:18 120-83-201/18/18 16:034181
Diethylphthalate ND ug/kg 01/22/18 09:18 84-66-201/18/18 16:034181
2,4-Dimethylphenol ND ug/kg 01/22/18 09:18 105-67-901/18/18 16:034181
Dimethylphthalate ND ug/kg 01/22/18 09:18 131-11-301/18/18 16:034181
Di-n-butylphthalate ND ug/kg 01/22/18 09:18 84-74-201/18/18 16:034181
4,6-Dinitro-2-methylphenol ND ug/kg 01/22/18 09:18 534-52-101/18/18 16:038361
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92369939
BCP-064
Sample:STOCKPILE-1 Lab ID:92369939001 Collected:01/17/18 11:45 Received:01/18/18 10:51 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
2,4-Dinitrophenol ND ug/kg 01/22/18 09:18 51-28-501/18/18 16:0320901
2,4-Dinitrotoluene ND ug/kg 01/22/18 09:18 121-14-201/18/18 16:034181
2,6-Dinitrotoluene ND ug/kg 01/22/18 09:18 606-20-201/18/18 16:034181
Di-n-octylphthalate ND ug/kg 01/22/18 09:18 117-84-0 L101/18/18 16:034181
bis(2-Ethylhexyl)phthalate ND ug/kg 01/22/18 09:18 117-81-701/18/18 16:034181
Fluoranthene ND ug/kg 01/22/18 09:18 206-44-001/18/18 16:034181
Fluorene ND ug/kg 01/22/18 09:18 86-73-701/18/18 16:034181
Hexachloro-1,3-butadiene ND ug/kg 01/22/18 09:18 87-68-301/18/18 16:034181
Hexachlorobenzene ND ug/kg 01/22/18 09:18 118-74-101/18/18 16:034181
Hexachlorocyclopentadiene ND ug/kg 01/22/18 09:18 77-47-401/18/18 16:034181
Hexachloroethane ND ug/kg 01/22/18 09:18 67-72-101/18/18 16:034181
Indeno(1,2,3-cd)pyrene ND ug/kg 01/22/18 09:18 193-39-501/18/18 16:034181
Isophorone ND ug/kg 01/22/18 09:18 78-59-101/18/18 16:034181
1-Methylnaphthalene ND ug/kg 01/22/18 09:18 90-12-001/18/18 16:034181
2-Methylnaphthalene ND ug/kg 01/22/18 09:18 91-57-601/18/18 16:034181
2-Methylphenol(o-Cresol)ND ug/kg 01/22/18 09:18 95-48-701/18/18 16:034181
3&4-Methylphenol(m&p Cresol)ND ug/kg 01/22/18 09:18 15831-10-401/18/18 16:034181
Naphthalene ND ug/kg 01/22/18 09:18 91-20-301/18/18 16:034181
2-Nitroaniline ND ug/kg 01/22/18 09:18 88-74-401/18/18 16:0320901
3-Nitroaniline ND ug/kg 01/22/18 09:18 99-09-201/18/18 16:0320901
4-Nitroaniline ND ug/kg 01/22/18 09:18 100-01-601/18/18 16:038361
Nitrobenzene ND ug/kg 01/22/18 09:18 98-95-301/18/18 16:034181
2-Nitrophenol ND ug/kg 01/22/18 09:18 88-75-501/18/18 16:034181
4-Nitrophenol ND ug/kg 01/22/18 09:18 100-02-701/18/18 16:0320901
N-Nitrosodimethylamine ND ug/kg 01/22/18 09:18 62-75-901/18/18 16:034181
N-Nitroso-di-n-propylamine ND ug/kg 01/22/18 09:18 621-64-701/18/18 16:034181
N-Nitrosodiphenylamine ND ug/kg 01/22/18 09:18 86-30-601/18/18 16:034181
2,2'-Oxybis(1-chloropropane)ND ug/kg 01/22/18 09:18 108-60-101/18/18 16:034181
Pentachlorophenol ND ug/kg 01/22/18 09:18 87-86-501/18/18 16:0320901
Phenanthrene ND ug/kg 01/22/18 09:18 85-01-801/18/18 16:034181
Phenol ND ug/kg 01/22/18 09:18 108-95-201/18/18 16:034181
Pyrene ND ug/kg 01/22/18 09:18 129-00-001/18/18 16:034181
1,2,4-Trichlorobenzene ND ug/kg 01/22/18 09:18 120-82-101/18/18 16:034181
2,4,5-Trichlorophenol ND ug/kg 01/22/18 09:18 95-95-401/18/18 16:034181
2,4,6-Trichlorophenol ND ug/kg 01/22/18 09:18 88-06-201/18/18 16:034181
Surrogates
Nitrobenzene-d5 (S)80 %01/22/18 09:18 4165-60-001/18/18 16:0323-110 1
2-Fluorobiphenyl (S)82 %01/22/18 09:18 321-60-801/18/18 16:0330-110 1
Terphenyl-d14 (S)96 %01/22/18 09:18 1718-51-001/18/18 16:0328-110 1
Phenol-d6 (S)76 %01/22/18 09:18 13127-88-301/18/18 16:0322-110 1
2-Fluorophenol (S)79 %01/22/18 09:18 367-12-401/18/18 16:0313-110 1
2,4,6-Tribromophenol (S)87 %01/22/18 09:18 118-79-601/18/18 16:0327-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 01/18/18 16:30 67-64-11001
Benzene ND ug/kg 01/18/18 16:30 71-43-25.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92369939
BCP-064
Sample:STOCKPILE-1 Lab ID:92369939001 Collected:01/17/18 11:45 Received:01/18/18 10:51 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Bromobenzene ND ug/kg 01/18/18 16:30 108-86-15.0 1
Bromochloromethane ND ug/kg 01/18/18 16:30 74-97-55.0 1
Bromodichloromethane ND ug/kg 01/18/18 16:30 75-27-45.0 1
Bromoform ND ug/kg 01/18/18 16:30 75-25-25.0 1
Bromomethane ND ug/kg 01/18/18 16:30 74-83-910.0 1
2-Butanone (MEK)ND ug/kg 01/18/18 16:30 78-93-31001
n-Butylbenzene ND ug/kg 01/18/18 16:30 104-51-85.0 1
sec-Butylbenzene ND ug/kg 01/18/18 16:30 135-98-85.0 1
tert-Butylbenzene ND ug/kg 01/18/18 16:30 98-06-65.0 1
Carbon tetrachloride ND ug/kg 01/18/18 16:30 56-23-55.0 1
Chlorobenzene ND ug/kg 01/18/18 16:30 108-90-75.0 1
Chloroethane ND ug/kg 01/18/18 16:30 75-00-310.0 1
Chloroform ND ug/kg 01/18/18 16:30 67-66-35.0 1
Chloromethane ND ug/kg 01/18/18 16:30 74-87-310.0 1
2-Chlorotoluene ND ug/kg 01/18/18 16:30 95-49-85.0 1
4-Chlorotoluene ND ug/kg 01/18/18 16:30 106-43-45.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 01/18/18 16:30 96-12-85.0 1
Dibromochloromethane ND ug/kg 01/18/18 16:30 124-48-15.0 1
1,2-Dibromoethane (EDB)ND ug/kg 01/18/18 16:30 106-93-45.0 1
Dibromomethane ND ug/kg 01/18/18 16:30 74-95-35.0 1
1,2-Dichlorobenzene ND ug/kg 01/18/18 16:30 95-50-15.0 1
1,3-Dichlorobenzene ND ug/kg 01/18/18 16:30 541-73-15.0 1
1,4-Dichlorobenzene ND ug/kg 01/18/18 16:30 106-46-75.0 1
Dichlorodifluoromethane ND ug/kg 01/18/18 16:30 75-71-810.0 1
1,1-Dichloroethane ND ug/kg 01/18/18 16:30 75-34-35.0 1
1,2-Dichloroethane ND ug/kg 01/18/18 16:30 107-06-25.0 1
1,1-Dichloroethene ND ug/kg 01/18/18 16:30 75-35-45.0 1
cis-1,2-Dichloroethene ND ug/kg 01/18/18 16:30 156-59-25.0 1
trans-1,2-Dichloroethene ND ug/kg 01/18/18 16:30 156-60-55.0 1
1,2-Dichloropropane ND ug/kg 01/18/18 16:30 78-87-55.0 1
1,3-Dichloropropane ND ug/kg 01/18/18 16:30 142-28-95.0 1
2,2-Dichloropropane ND ug/kg 01/18/18 16:30 594-20-75.0 1
1,1-Dichloropropene ND ug/kg 01/18/18 16:30 563-58-65.0 1
cis-1,3-Dichloropropene ND ug/kg 01/18/18 16:30 10061-01-55.0 1
trans-1,3-Dichloropropene ND ug/kg 01/18/18 16:30 10061-02-65.0 1
Diisopropyl ether ND ug/kg 01/18/18 16:30 108-20-35.0 1
Ethylbenzene ND ug/kg 01/18/18 16:30 100-41-45.0 1
Hexachloro-1,3-butadiene ND ug/kg 01/18/18 16:30 87-68-35.0 1
2-Hexanone ND ug/kg 01/18/18 16:30 591-78-650.1 1
Isopropylbenzene (Cumene)ND ug/kg 01/18/18 16:30 98-82-85.0 1
p-Isopropyltoluene ND ug/kg 01/18/18 16:30 99-87-65.0 1
Methylene Chloride ND ug/kg 01/18/18 16:30 75-09-220.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 01/18/18 16:30 108-10-150.1 1
Methyl-tert-butyl ether ND ug/kg 01/18/18 16:30 1634-04-45.0 1
Naphthalene ND ug/kg 01/18/18 16:30 91-20-35.0 1
n-Propylbenzene ND ug/kg 01/18/18 16:30 103-65-15.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92369939
BCP-064
Sample:STOCKPILE-1 Lab ID:92369939001 Collected:01/17/18 11:45 Received:01/18/18 10:51 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Styrene ND ug/kg 01/18/18 16:30 100-42-55.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 01/18/18 16:30 630-20-65.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 01/18/18 16:30 79-34-55.0 1
Tetrachloroethene ND ug/kg 01/18/18 16:30 127-18-45.0 1
Toluene ND ug/kg 01/18/18 16:30 108-88-35.0 1
1,2,3-Trichlorobenzene ND ug/kg 01/18/18 16:30 87-61-65.0 1
1,2,4-Trichlorobenzene ND ug/kg 01/18/18 16:30 120-82-15.0 1
1,1,1-Trichloroethane ND ug/kg 01/18/18 16:30 71-55-65.0 1
1,1,2-Trichloroethane ND ug/kg 01/18/18 16:30 79-00-55.0 1
Trichloroethene ND ug/kg 01/18/18 16:30 79-01-65.0 1
Trichlorofluoromethane ND ug/kg 01/18/18 16:30 75-69-45.0 1
1,2,3-Trichloropropane ND ug/kg 01/18/18 16:30 96-18-45.0 1
1,2,4-Trimethylbenzene ND ug/kg 01/18/18 16:30 95-63-65.0 1
1,3,5-Trimethylbenzene ND ug/kg 01/18/18 16:30 108-67-85.0 1
Vinyl acetate ND ug/kg 01/18/18 16:30 108-05-450.1 1
Vinyl chloride ND ug/kg 01/18/18 16:30 75-01-410.0 1
Xylene (Total)ND ug/kg 01/18/18 16:30 1330-20-710.0 1
m&p-Xylene ND ug/kg 01/18/18 16:30 179601-23-110.0 1
o-Xylene ND ug/kg 01/18/18 16:30 95-47-65.0 1
Surrogates
Toluene-d8 (S)99 %01/18/18 16:30 2037-26-570-130 1
4-Bromofluorobenzene (S)98 %01/18/18 16:30 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %01/18/18 16:30 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 20.5 %01/19/18 12:380.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92369939
BCP-064
Sample:STOCKPILE-2 Lab ID:92369939002 Collected:01/17/18 12:00 Received:01/18/18 10:51 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Arsenic ND mg/kg 01/25/18 01:44 7440-38-201/24/18 01:503.6 5
Barium 37.2 mg/kg 01/24/18 10:05 7440-39-301/24/18 01:500.72 1
Cadmium ND mg/kg 01/25/18 01:44 7440-43-901/24/18 01:500.36 5
Chromium 20.7 mg/kg 01/24/18 10:05 7440-47-301/24/18 01:500.36 1
Lead 7.5 mg/kg 01/24/18 10:05 7439-92-101/24/18 01:500.72 1
Selenium ND mg/kg 01/25/18 01:44 7782-49-201/24/18 01:505.4 5
Silver ND mg/kg 01/24/18 10:05 7440-22-401/24/18 01:500.36 1
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury 0.019 mg/kg 01/25/18 11:50 7439-97-601/24/18 10:020.018 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 01/22/18 09:48 83-32-901/18/18 16:034271
Acenaphthylene ND ug/kg 01/22/18 09:48 208-96-801/18/18 16:034271
Aniline ND ug/kg 01/22/18 09:48 62-53-301/18/18 16:034271
Anthracene ND ug/kg 01/22/18 09:48 120-12-701/18/18 16:034271
Benzo(a)anthracene ND ug/kg 01/22/18 09:48 56-55-301/18/18 16:034271
Benzo(a)pyrene ND ug/kg 01/22/18 09:48 50-32-801/18/18 16:034271
Benzo(b)fluoranthene ND ug/kg 01/22/18 09:48 205-99-201/18/18 16:034271
Benzo(g,h,i)perylene ND ug/kg 01/22/18 09:48 191-24-201/18/18 16:034271
Benzo(k)fluoranthene ND ug/kg 01/22/18 09:48 207-08-901/18/18 16:034271
Benzoic Acid ND ug/kg 01/22/18 09:48 65-85-001/18/18 16:0321301
Benzyl alcohol ND ug/kg 01/22/18 09:48 100-51-601/18/18 16:038541
4-Bromophenylphenyl ether ND ug/kg 01/22/18 09:48 101-55-301/18/18 16:034271
Butylbenzylphthalate ND ug/kg 01/22/18 09:48 85-68-7 L101/18/18 16:034271
4-Chloro-3-methylphenol ND ug/kg 01/22/18 09:48 59-50-701/18/18 16:038541
4-Chloroaniline ND ug/kg 01/22/18 09:48 106-47-801/18/18 16:0321301
bis(2-Chloroethoxy)methane ND ug/kg 01/22/18 09:48 111-91-101/18/18 16:034271
bis(2-Chloroethyl) ether ND ug/kg 01/22/18 09:48 111-44-401/18/18 16:034271
2-Chloronaphthalene ND ug/kg 01/22/18 09:48 91-58-701/18/18 16:034271
2-Chlorophenol ND ug/kg 01/22/18 09:48 95-57-801/18/18 16:034271
4-Chlorophenylphenyl ether ND ug/kg 01/22/18 09:48 7005-72-301/18/18 16:034271
Chrysene ND ug/kg 01/22/18 09:48 218-01-901/18/18 16:034271
Dibenz(a,h)anthracene ND ug/kg 01/22/18 09:48 53-70-301/18/18 16:034271
Dibenzofuran ND ug/kg 01/22/18 09:48 132-64-901/18/18 16:034271
1,2-Dichlorobenzene ND ug/kg 01/22/18 09:48 95-50-101/18/18 16:034271
1,3-Dichlorobenzene ND ug/kg 01/22/18 09:48 541-73-101/18/18 16:034271
1,4-Dichlorobenzene ND ug/kg 01/22/18 09:48 106-46-701/18/18 16:034271
3,3'-Dichlorobenzidine ND ug/kg 01/22/18 09:48 91-94-101/18/18 16:0321301
2,4-Dichlorophenol ND ug/kg 01/22/18 09:48 120-83-201/18/18 16:034271
Diethylphthalate ND ug/kg 01/22/18 09:48 84-66-201/18/18 16:034271
2,4-Dimethylphenol ND ug/kg 01/22/18 09:48 105-67-901/18/18 16:034271
Dimethylphthalate ND ug/kg 01/22/18 09:48 131-11-301/18/18 16:034271
Di-n-butylphthalate ND ug/kg 01/22/18 09:48 84-74-201/18/18 16:034271
4,6-Dinitro-2-methylphenol ND ug/kg 01/22/18 09:48 534-52-101/18/18 16:038541
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92369939
BCP-064
Sample:STOCKPILE-2 Lab ID:92369939002 Collected:01/17/18 12:00 Received:01/18/18 10:51 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
2,4-Dinitrophenol ND ug/kg 01/22/18 09:48 51-28-501/18/18 16:0321301
2,4-Dinitrotoluene ND ug/kg 01/22/18 09:48 121-14-201/18/18 16:034271
2,6-Dinitrotoluene ND ug/kg 01/22/18 09:48 606-20-201/18/18 16:034271
Di-n-octylphthalate ND ug/kg 01/22/18 09:48 117-84-0 L101/18/18 16:034271
bis(2-Ethylhexyl)phthalate ND ug/kg 01/22/18 09:48 117-81-701/18/18 16:034271
Fluoranthene ND ug/kg 01/22/18 09:48 206-44-001/18/18 16:034271
Fluorene ND ug/kg 01/22/18 09:48 86-73-701/18/18 16:034271
Hexachloro-1,3-butadiene ND ug/kg 01/22/18 09:48 87-68-301/18/18 16:034271
Hexachlorobenzene ND ug/kg 01/22/18 09:48 118-74-101/18/18 16:034271
Hexachlorocyclopentadiene ND ug/kg 01/22/18 09:48 77-47-401/18/18 16:034271
Hexachloroethane ND ug/kg 01/22/18 09:48 67-72-101/18/18 16:034271
Indeno(1,2,3-cd)pyrene ND ug/kg 01/22/18 09:48 193-39-501/18/18 16:034271
Isophorone ND ug/kg 01/22/18 09:48 78-59-101/18/18 16:034271
1-Methylnaphthalene ND ug/kg 01/22/18 09:48 90-12-001/18/18 16:034271
2-Methylnaphthalene ND ug/kg 01/22/18 09:48 91-57-601/18/18 16:034271
2-Methylphenol(o-Cresol)ND ug/kg 01/22/18 09:48 95-48-701/18/18 16:034271
3&4-Methylphenol(m&p Cresol)ND ug/kg 01/22/18 09:48 15831-10-401/18/18 16:034271
Naphthalene ND ug/kg 01/22/18 09:48 91-20-301/18/18 16:034271
2-Nitroaniline ND ug/kg 01/22/18 09:48 88-74-401/18/18 16:0321301
3-Nitroaniline ND ug/kg 01/22/18 09:48 99-09-201/18/18 16:0321301
4-Nitroaniline ND ug/kg 01/22/18 09:48 100-01-601/18/18 16:038541
Nitrobenzene ND ug/kg 01/22/18 09:48 98-95-301/18/18 16:034271
2-Nitrophenol ND ug/kg 01/22/18 09:48 88-75-501/18/18 16:034271
4-Nitrophenol ND ug/kg 01/22/18 09:48 100-02-701/18/18 16:0321301
N-Nitrosodimethylamine ND ug/kg 01/22/18 09:48 62-75-901/18/18 16:034271
N-Nitroso-di-n-propylamine ND ug/kg 01/22/18 09:48 621-64-701/18/18 16:034271
N-Nitrosodiphenylamine ND ug/kg 01/22/18 09:48 86-30-601/18/18 16:034271
2,2'-Oxybis(1-chloropropane)ND ug/kg 01/22/18 09:48 108-60-101/18/18 16:034271
Pentachlorophenol ND ug/kg 01/22/18 09:48 87-86-501/18/18 16:0321301
Phenanthrene ND ug/kg 01/22/18 09:48 85-01-801/18/18 16:034271
Phenol ND ug/kg 01/22/18 09:48 108-95-201/18/18 16:034271
Pyrene ND ug/kg 01/22/18 09:48 129-00-001/18/18 16:034271
1,2,4-Trichlorobenzene ND ug/kg 01/22/18 09:48 120-82-101/18/18 16:034271
2,4,5-Trichlorophenol ND ug/kg 01/22/18 09:48 95-95-401/18/18 16:034271
2,4,6-Trichlorophenol ND ug/kg 01/22/18 09:48 88-06-201/18/18 16:034271
Surrogates
Nitrobenzene-d5 (S)84 %01/22/18 09:48 4165-60-001/18/18 16:0323-110 1
2-Fluorobiphenyl (S)80 %01/22/18 09:48 321-60-801/18/18 16:0330-110 1
Terphenyl-d14 (S)102 %01/22/18 09:48 1718-51-001/18/18 16:0328-110 1
Phenol-d6 (S)77 %01/22/18 09:48 13127-88-301/18/18 16:0322-110 1
2-Fluorophenol (S)81 %01/22/18 09:48 367-12-401/18/18 16:0313-110 1
2,4,6-Tribromophenol (S)83 %01/22/18 09:48 118-79-601/18/18 16:0327-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 01/22/18 16:20 67-64-11061
Benzene ND ug/kg 01/22/18 16:20 71-43-25.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92369939
BCP-064
Sample:STOCKPILE-2 Lab ID:92369939002 Collected:01/17/18 12:00 Received:01/18/18 10:51 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Bromobenzene ND ug/kg 01/22/18 16:20 108-86-15.3 1
Bromochloromethane ND ug/kg 01/22/18 16:20 74-97-55.3 1
Bromodichloromethane ND ug/kg 01/22/18 16:20 75-27-45.3 1
Bromoform ND ug/kg 01/22/18 16:20 75-25-25.3 1
Bromomethane ND ug/kg 01/22/18 16:20 74-83-910.6 1
2-Butanone (MEK)ND ug/kg 01/22/18 16:20 78-93-31061
n-Butylbenzene 29.1 ug/kg 01/22/18 16:20 104-51-85.3 1
sec-Butylbenzene 23.5 ug/kg 01/22/18 16:20 135-98-85.3 1
tert-Butylbenzene 7.8 ug/kg 01/22/18 16:20 98-06-65.3 1
Carbon tetrachloride ND ug/kg 01/22/18 16:20 56-23-55.3 1
Chlorobenzene ND ug/kg 01/22/18 16:20 108-90-75.3 1
Chloroethane ND ug/kg 01/22/18 16:20 75-00-310.6 1
Chloroform ND ug/kg 01/22/18 16:20 67-66-35.3 1
Chloromethane ND ug/kg 01/22/18 16:20 74-87-310.6 1
2-Chlorotoluene ND ug/kg 01/22/18 16:20 95-49-85.3 1
4-Chlorotoluene ND ug/kg 01/22/18 16:20 106-43-45.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 01/22/18 16:20 96-12-85.3 1
Dibromochloromethane ND ug/kg 01/22/18 16:20 124-48-15.3 1
1,2-Dibromoethane (EDB)ND ug/kg 01/22/18 16:20 106-93-45.3 1
Dibromomethane ND ug/kg 01/22/18 16:20 74-95-35.3 1
1,2-Dichlorobenzene ND ug/kg 01/22/18 16:20 95-50-15.3 1
1,3-Dichlorobenzene ND ug/kg 01/22/18 16:20 541-73-15.3 1
1,4-Dichlorobenzene ND ug/kg 01/22/18 16:20 106-46-75.3 1
Dichlorodifluoromethane ND ug/kg 01/22/18 16:20 75-71-810.6 1
1,1-Dichloroethane ND ug/kg 01/22/18 16:20 75-34-35.3 1
1,2-Dichloroethane ND ug/kg 01/22/18 16:20 107-06-25.3 1
1,1-Dichloroethene ND ug/kg 01/22/18 16:20 75-35-45.3 1
cis-1,2-Dichloroethene ND ug/kg 01/22/18 16:20 156-59-25.3 1
trans-1,2-Dichloroethene ND ug/kg 01/22/18 16:20 156-60-55.3 1
1,2-Dichloropropane ND ug/kg 01/22/18 16:20 78-87-55.3 1
1,3-Dichloropropane ND ug/kg 01/22/18 16:20 142-28-95.3 1
2,2-Dichloropropane ND ug/kg 01/22/18 16:20 594-20-75.3 1
1,1-Dichloropropene ND ug/kg 01/22/18 16:20 563-58-65.3 1
cis-1,3-Dichloropropene ND ug/kg 01/22/18 16:20 10061-01-55.3 1
trans-1,3-Dichloropropene ND ug/kg 01/22/18 16:20 10061-02-65.3 1
Diisopropyl ether ND ug/kg 01/22/18 16:20 108-20-35.3 1
Ethylbenzene ND ug/kg 01/22/18 16:20 100-41-45.3 1
Hexachloro-1,3-butadiene ND ug/kg 01/22/18 16:20 87-68-35.3 1
2-Hexanone ND ug/kg 01/22/18 16:20 591-78-653.2 1
Isopropylbenzene (Cumene)ND ug/kg 01/22/18 16:20 98-82-85.3 1
p-Isopropyltoluene 66.4 ug/kg 01/22/18 16:20 99-87-65.3 1
Methylene Chloride ND ug/kg 01/22/18 16:20 75-09-221.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 01/22/18 16:20 108-10-153.2 1
Methyl-tert-butyl ether ND ug/kg 01/22/18 16:20 1634-04-45.3 1
Naphthalene ND ug/kg 01/22/18 16:20 91-20-35.3 1
n-Propylbenzene 17.2 ug/kg 01/22/18 16:20 103-65-15.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92369939
BCP-064
Sample:STOCKPILE-2 Lab ID:92369939002 Collected:01/17/18 12:00 Received:01/18/18 10:51 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
Styrene ND ug/kg 01/22/18 16:20 100-42-55.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 01/22/18 16:20 630-20-65.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 01/22/18 16:20 79-34-55.3 1
Tetrachloroethene 1710 ug/kg 01/23/18 15:50 127-18-425450
Toluene ND ug/kg 01/22/18 16:20 108-88-35.3 1
1,2,3-Trichlorobenzene ND ug/kg 01/22/18 16:20 87-61-65.3 1
1,2,4-Trichlorobenzene ND ug/kg 01/22/18 16:20 120-82-15.3 1
1,1,1-Trichloroethane ND ug/kg 01/22/18 16:20 71-55-65.3 1
1,1,2-Trichloroethane ND ug/kg 01/22/18 16:20 79-00-55.3 1
Trichloroethene 9.7 ug/kg 01/22/18 16:20 79-01-65.3 1
Trichlorofluoromethane ND ug/kg 01/22/18 16:20 75-69-45.3 1
1,2,3-Trichloropropane ND ug/kg 01/22/18 16:20 96-18-45.3 1
1,2,4-Trimethylbenzene 907 ug/kg 01/23/18 15:50 95-63-625450
1,3,5-Trimethylbenzene 184 ug/kg 01/22/18 16:20 108-67-85.3 1
Vinyl acetate ND ug/kg 01/22/18 16:20 108-05-453.2 1
Vinyl chloride ND ug/kg 01/22/18 16:20 75-01-410.6 1
Xylene (Total)ND ug/kg 01/22/18 16:20 1330-20-710.6 1
m&p-Xylene ND ug/kg 01/22/18 16:20 179601-23-110.6 1
o-Xylene ND ug/kg 01/22/18 16:20 95-47-65.3 1
Surrogates
Toluene-d8 (S)99 %01/22/18 16:20 2037-26-570-130 1
4-Bromofluorobenzene (S)152 %01/22/18 16:20 460-00-4 S170-130 1
1,2-Dichloroethane-d4 (S)104 %01/22/18 16:20 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 22.5 %01/19/18 12:420.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92369939
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
420008
EPA 7471
EPA 7471
7471 Mercury
Associated Lab Samples:92369939001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2288032
Associated Lab Samples:92369939001
Matrix:Solid
Analyzed
Mercury mg/kg ND 0.0085 01/22/18 11:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2288033LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.10.096 105 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2288034MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35367767001
2288035
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg .077 91 80-12096 18 20.0890.0066J 0.077 0.092
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92369939
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
420717
EPA 7471
EPA 7471
7471 Mercury
Associated Lab Samples:92369939002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2291300
Associated Lab Samples:92369939002
Matrix:Solid
Analyzed
Mercury mg/kg ND 0.0070 01/25/18 10:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2291301LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.071.067 106 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2291302MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35367660004
2291303
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg M113.6 79 80-12090 15 2014.10.96J 11.7 13.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92369939
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
420120
EPA 3050
EPA 6010
6010 MET Solid
Associated Lab Samples:92369939001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2288487
Associated Lab Samples:92369939001
Matrix:Solid
Analyzed
Arsenic mg/kg ND 1.1 01/22/18 15:25
Barium mg/kg ND 1.1 01/22/18 15:25
Cadmium mg/kg ND 0.11 01/22/18 15:25
Chromium mg/kg ND 0.53 01/22/18 15:25
Lead mg/kg ND 1.1 01/22/18 15:25
Selenium mg/kg ND 1.6 01/22/18 15:25
Silver mg/kg ND 0.53 01/22/18 15:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2288488LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 14.414.6 98 80-120
Barium mg/kg 15.714.6 107 80-120
Cadmium mg/kg 1.51.5 104 80-120
Chromium mg/kg 15.414.6 106 80-120
Lead mg/kg 15.414.6 106 80-120
Selenium mg/kg 14.414.6 98 80-120
Silver mg/kg 1.51.5 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2288489MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35369222001
2288490
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 14.9 104 75-125101 4 2016.11.5 17.1 17.8
Barium mg/kg M114.9 158 75-125107 15 2016.119.7 43.2 37.0
Cadmium mg/kg 1.5 96 75-12598 9 201.60.18 1.6 1.8
Chromium mg/kg 14.9 113 75-125105 0 2016.18.1 24.9 25.0
Lead mg/kg 14.9 120 75-12590 7 2016.131.1 48.9 45.5
Selenium mg/kg 14.9 101 75-125101 8 2016.10.97U 15.4 16.7
Silver mg/kg M11.5 68 75-12571 7 201.60.71 1.7 1.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92369939
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
420652
EPA 3050
EPA 6010
6010 MET Solid
Associated Lab Samples:92369939002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2290870
Associated Lab Samples:92369939002
Matrix:Solid
Analyzed
Arsenic mg/kg ND 0.54 01/25/18 00:26
Barium mg/kg ND 0.54 01/25/18 00:26
Cadmium mg/kg ND 0.054 01/25/18 00:26
Chromium mg/kg ND 0.27 01/25/18 00:26
Lead mg/kg ND 0.54 01/25/18 00:26
Selenium mg/kg ND 0.82 01/25/18 00:26
Silver mg/kg ND 0.27 01/25/18 00:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2290871LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 13.313.6 98 80-120
Barium mg/kg 14.113.6 103 80-120
Cadmium mg/kg 1.41.4 100 80-120
Chromium mg/kg 14.313.6 105 80-120
Lead mg/kg 14.413.6 106 80-120
Selenium mg/kg 13.013.6 96 80-120
Silver mg/kg 1.41.4 101 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2290872MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35367958002
2290873
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 13.2 95 75-12595 10 2014.61.2 13.7 15.1
Barium mg/kg 13.2 98 75-125102 12 2014.61.5 14.5 16.4
Cadmium mg/kg 1.34 82 75-12583 11 201.450.061U 1.1 1.2
Chromium mg/kg M113.2 115 75-125129 11 2014.617.1 32.3 35.9
Lead mg/kg 13.2 91 75-12593 13 2014.60.63 12.6 14.3
Selenium mg/kg 13.2 76 75-12579 13 2014.60.92U 10.5 12.0
Silver mg/kg M11.34 135 75-125130 7 201.450.15U 1.8 1.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92369939
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
394662
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92369939001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2187737
Associated Lab Samples:92369939001
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.4 01/18/18 14:52
1,1,1-Trichloroethane ug/kg ND 5.4 01/18/18 14:52
1,1,2,2-Tetrachloroethane ug/kg ND 5.4 01/18/18 14:52
1,1,2-Trichloroethane ug/kg ND 5.4 01/18/18 14:52
1,1-Dichloroethane ug/kg ND 5.4 01/18/18 14:52
1,1-Dichloroethene ug/kg ND 5.4 01/18/18 14:52
1,1-Dichloropropene ug/kg ND 5.4 01/18/18 14:52
1,2,3-Trichlorobenzene ug/kg ND 5.4 01/18/18 14:52
1,2,3-Trichloropropane ug/kg ND 5.4 01/18/18 14:52
1,2,4-Trichlorobenzene ug/kg ND 5.4 01/18/18 14:52
1,2,4-Trimethylbenzene ug/kg ND 5.4 01/18/18 14:52
1,2-Dibromo-3-chloropropane ug/kg ND 5.4 01/18/18 14:52
1,2-Dibromoethane (EDB)ug/kg ND 5.4 01/18/18 14:52
1,2-Dichlorobenzene ug/kg ND 5.4 01/18/18 14:52
1,2-Dichloroethane ug/kg ND 5.4 01/18/18 14:52
1,2-Dichloropropane ug/kg ND 5.4 01/18/18 14:52
1,3,5-Trimethylbenzene ug/kg ND 5.4 01/18/18 14:52
1,3-Dichlorobenzene ug/kg ND 5.4 01/18/18 14:52
1,3-Dichloropropane ug/kg ND 5.4 01/18/18 14:52
1,4-Dichlorobenzene ug/kg ND 5.4 01/18/18 14:52
2,2-Dichloropropane ug/kg ND 5.4 01/18/18 14:52
2-Butanone (MEK)ug/kg ND 109 01/18/18 14:52
2-Chlorotoluene ug/kg ND 5.4 01/18/18 14:52
2-Hexanone ug/kg ND 54.5 01/18/18 14:52
4-Chlorotoluene ug/kg ND 5.4 01/18/18 14:52
4-Methyl-2-pentanone (MIBK)ug/kg ND 54.5 01/18/18 14:52
Acetone ug/kg ND 109 01/18/18 14:52
Benzene ug/kg ND 5.4 01/18/18 14:52
Bromobenzene ug/kg ND 5.4 01/18/18 14:52
Bromochloromethane ug/kg ND 5.4 01/18/18 14:52
Bromodichloromethane ug/kg ND 5.4 01/18/18 14:52
Bromoform ug/kg ND 5.4 01/18/18 14:52
Bromomethane ug/kg ND 10.9 01/18/18 14:52
Carbon tetrachloride ug/kg ND 5.4 01/18/18 14:52
Chlorobenzene ug/kg ND 5.4 01/18/18 14:52
Chloroethane ug/kg ND 10.9 01/18/18 14:52
Chloroform ug/kg ND 5.4 01/18/18 14:52
Chloromethane ug/kg ND 10.9 01/18/18 14:52
cis-1,2-Dichloroethene ug/kg ND 5.4 01/18/18 14:52
cis-1,3-Dichloropropene ug/kg ND 5.4 01/18/18 14:52
Dibromochloromethane ug/kg ND 5.4 01/18/18 14:52
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
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Page 17 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92369939
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2187737
Associated Lab Samples:92369939001
Matrix:Solid
Analyzed
Dibromomethane ug/kg ND 5.4 01/18/18 14:52
Dichlorodifluoromethane ug/kg ND 10.9 01/18/18 14:52
Diisopropyl ether ug/kg ND 5.4 01/18/18 14:52
Ethylbenzene ug/kg ND 5.4 01/18/18 14:52
Hexachloro-1,3-butadiene ug/kg ND 5.4 01/18/18 14:52
Isopropylbenzene (Cumene)ug/kg ND 5.4 01/18/18 14:52
m&p-Xylene ug/kg ND 10.9 01/18/18 14:52
Methyl-tert-butyl ether ug/kg ND 5.4 01/18/18 14:52
Methylene Chloride ug/kg ND 21.8 01/18/18 14:52
n-Butylbenzene ug/kg ND 5.4 01/18/18 14:52
n-Propylbenzene ug/kg ND 5.4 01/18/18 14:52
Naphthalene ug/kg ND 5.4 01/18/18 14:52
o-Xylene ug/kg ND 5.4 01/18/18 14:52
p-Isopropyltoluene ug/kg ND 5.4 01/18/18 14:52
sec-Butylbenzene ug/kg ND 5.4 01/18/18 14:52
Styrene ug/kg ND 5.4 01/18/18 14:52
tert-Butylbenzene ug/kg ND 5.4 01/18/18 14:52
Tetrachloroethene ug/kg ND 5.4 01/18/18 14:52
Toluene ug/kg ND 5.4 01/18/18 14:52
trans-1,2-Dichloroethene ug/kg ND 5.4 01/18/18 14:52
trans-1,3-Dichloropropene ug/kg ND 5.4 01/18/18 14:52
Trichloroethene ug/kg ND 5.4 01/18/18 14:52
Trichlorofluoromethane ug/kg ND 5.4 01/18/18 14:52
Vinyl acetate ug/kg ND 54.5 01/18/18 14:52
Vinyl chloride ug/kg ND 10.9 01/18/18 14:52
Xylene (Total)ug/kg ND 10.9 01/18/18 14:52
1,2-Dichloroethane-d4 (S)%99 70-132 01/18/18 14:52
4-Bromofluorobenzene (S)%97 70-130 01/18/18 14:52
Toluene-d8 (S)%98 70-130 01/18/18 14:52
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2187738LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 49.152.6 93 74-137
1,1,1-Trichloroethane ug/kg 43.952.6 83 67-140
1,1,2,2-Tetrachloroethane ug/kg 47.452.6 90 72-141
1,1,2-Trichloroethane ug/kg 47.652.6 90 78-138
1,1-Dichloroethane ug/kg 43.152.6 82 69-134
1,1-Dichloroethene ug/kg 45.152.6 86 67-138
1,1-Dichloropropene ug/kg 43.752.6 83 69-139
1,2,3-Trichlorobenzene ug/kg 50.652.6 96 70-146
1,2,3-Trichloropropane ug/kg 53.952.6 102 69-144
1,2,4-Trichlorobenzene ug/kg 52.152.6 99 68-148
1,2,4-Trimethylbenzene ug/kg 51.552.6 98 74-137
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
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Huntersville, NC 28078
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Page 18 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92369939
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2187738LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 50.152.6 95 65-140
1,2-Dibromoethane (EDB)ug/kg 51.552.6 98 77-135
1,2-Dichlorobenzene ug/kg 50.152.6 95 77-141
1,2-Dichloroethane ug/kg 44.352.6 84 65-137
1,2-Dichloropropane ug/kg 46.852.6 89 72-136
1,3,5-Trimethylbenzene ug/kg 50.752.6 96 76-133
1,3-Dichlorobenzene ug/kg 49.552.6 94 74-138
1,3-Dichloropropane ug/kg 51.452.6 98 71-139
1,4-Dichlorobenzene ug/kg 49.752.6 94 76-138
2,2-Dichloropropane ug/kg 43.652.6 83 68-137
2-Butanone (MEK)ug/kg 82.9J105 79 58-147
2-Chlorotoluene ug/kg 50.452.6 96 73-139
2-Hexanone ug/kg 105105 100 62-145
4-Chlorotoluene ug/kg 49.952.6 95 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 104105 99 64-149
Acetone ug/kg 98.4J105 93 53-153
Benzene ug/kg 46.252.6 88 73-135
Bromobenzene ug/kg 50.052.6 95 75-133
Bromochloromethane ug/kg 43.652.6 83 73-134
Bromodichloromethane ug/kg 46.952.6 89 71-135
Bromoform ug/kg 50.952.6 97 66-141
Bromomethane ug/kg 59.652.6 113 53-160
Carbon tetrachloride ug/kg 46.852.6 89 60-145
Chlorobenzene ug/kg 49.452.6 94 78-130
Chloroethane ug/kg 55.652.6 106 64-149
Chloroform ug/kg 42.652.6 81 70-134
Chloromethane ug/kg 40.352.6 77 52-150
cis-1,2-Dichloroethene ug/kg 42.852.6 81 70-133
cis-1,3-Dichloropropene ug/kg 48.552.6 92 68-134
Dibromochloromethane ug/kg 51.052.6 97 71-138
Dibromomethane ug/kg 46.052.6 87 74-130
Dichlorodifluoromethane ug/kg 43.452.6 82 40-160
Diisopropyl ether ug/kg 44.852.6 85 69-141
Ethylbenzene ug/kg 50.352.6 96 75-133
Hexachloro-1,3-butadiene ug/kg 49.052.6 93 68-143
Isopropylbenzene (Cumene)ug/kg 50.652.6 96 76-143
m&p-Xylene ug/kg 101105 96 75-136
Methyl-tert-butyl ether ug/kg 44.052.6 84 68-144
Methylene Chloride ug/kg 42.652.6 81 45-154
n-Butylbenzene ug/kg 50.852.6 97 72-137
n-Propylbenzene ug/kg 50.752.6 96 76-136
Naphthalene ug/kg 54.152.6 103 68-151
o-Xylene ug/kg 49.552.6 94 76-141
p-Isopropyltoluene ug/kg 50.852.6 97 76-140
sec-Butylbenzene ug/kg 49.752.6 94 79-139
Styrene ug/kg 49.852.6 95 79-137
tert-Butylbenzene ug/kg 45.852.6 87 74-143
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 19 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92369939
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2187738LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 46.452.6 88 71-138
Toluene ug/kg 46.652.6 89 74-131
trans-1,2-Dichloroethene ug/kg 44.452.6 84 67-135
trans-1,3-Dichloropropene ug/kg 48.452.6 92 65-146
Trichloroethene ug/kg 48.352.6 92 67-135
Trichlorofluoromethane ug/kg 46.152.6 88 59-144
Vinyl acetate ug/kg 101105 96 40-160
Vinyl chloride ug/kg 47.652.6 90 56-141
Xylene (Total)ug/kg 151158 95 76-137
1,2-Dichloroethane-d4 (S)%96 70-132
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2188211MATRIX SPIKE SAMPLE:
MSSpike
Result
92369843032
1,1,1,2-Tetrachloroethane ug/kg 36.835.2 105 70-130ND
1,1,1-Trichloroethane ug/kg 33.335.2 95 70-130ND
1,1,2,2-Tetrachloroethane ug/kg 38.135.2 108 70-130ND
1,1,2-Trichloroethane ug/kg 37.035.2 105 70-130ND
1,1-Dichloroethane ug/kg 33.535.2 95 70-130ND
1,1-Dichloroethene ug/kg 34.035.2 97 49-180ND
1,1-Dichloropropene ug/kg 33.235.2 94 70-130ND
1,2,3-Trichlorobenzene ug/kg 35.635.2 101 70-130ND
1,2,3-Trichloropropane ug/kg 40.235.2 114 70-130ND
1,2,4-Trichlorobenzene ug/kg 35.435.2 101 70-130ND
1,2,4-Trimethylbenzene ug/kg 38.435.2 109 70-130ND
1,2-Dibromo-3-chloropropane ug/kg 42.335.2 120 70-130ND
1,2-Dibromoethane (EDB)ug/kg 39.435.2 112 70-130ND
1,2-Dichlorobenzene ug/kg 37.335.2 106 70-130ND
1,2-Dichloroethane ug/kg 35.535.2 101 70-130ND
1,2-Dichloropropane ug/kg 35.635.2 101 70-130ND
1,3,5-Trimethylbenzene ug/kg 38.135.2 108 70-130ND
1,3-Dichlorobenzene ug/kg 36.435.2 103 70-130ND
1,3-Dichloropropane ug/kg 38.735.2 110 70-130ND
1,4-Dichlorobenzene ug/kg 37.135.2 106 70-130ND
2,2-Dichloropropane ug/kg 32.535.2 92 70-130ND
2-Butanone (MEK)ug/kg 72.9J70.3 104 70-130ND
2-Chlorotoluene ug/kg 38.535.2 109 70-130ND
2-Hexanone ug/kg 83.8J70.3 119 70-130ND
4-Chlorotoluene ug/kg 37.235.2 106 70-130ND
4-Methyl-2-pentanone (MIBK)ug/kg 82.2J70.3 117 70-130ND
Acetone ug/kg 405 M170.3 504 70-130ND
Benzene ug/kg 34.735.2 99 50-166ND
Bromobenzene ug/kg 37.035.2 105 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92369939
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2188211MATRIX SPIKE SAMPLE:
MSSpike
Result
92369843032
Bromochloromethane ug/kg 35.535.2 101 70-130ND
Bromodichloromethane ug/kg 35.235.2 100 70-130ND
Bromoform ug/kg 37.735.2 107 70-130ND
Bromomethane ug/kg 43.035.2 122 70-130ND
Carbon tetrachloride ug/kg 34.535.2 98 70-130ND
Chlorobenzene ug/kg 36.135.2 103 43-169ND
Chloroethane ug/kg 41.235.2 117 70-130ND
Chloroform ug/kg 33.135.2 94 70-130ND
Chloromethane ug/kg 30.235.2 86 70-130ND
cis-1,2-Dichloroethene ug/kg 32.535.2 92 70-130ND
cis-1,3-Dichloropropene ug/kg 36.035.2 102 70-130ND
Dibromochloromethane ug/kg 37.035.2 105 70-130ND
Dibromomethane ug/kg 36.235.2 103 70-130ND
Dichlorodifluoromethane ug/kg 32.435.2 92 70-130ND
Diisopropyl ether ug/kg 35.235.2 100 70-130ND
Ethylbenzene ug/kg 36.635.2 104 70-130ND
Hexachloro-1,3-butadiene ug/kg 35.735.2 102 70-130ND
Isopropylbenzene (Cumene)ug/kg 36.835.2 105 70-130ND
m&p-Xylene ug/kg 73.170.3 104 70-130ND
Methyl-tert-butyl ether ug/kg 35.935.2 102 70-130ND
Methylene Chloride ug/kg 102 M135.2 257 70-130ND
n-Butylbenzene ug/kg 37.535.2 107 70-130ND
n-Propylbenzene ug/kg 38.135.2 108 70-130ND
Naphthalene ug/kg 40.835.2 116 70-130ND
o-Xylene ug/kg 35.435.2 101 70-130ND
p-Isopropyltoluene ug/kg 37.635.2 107 70-130ND
sec-Butylbenzene ug/kg 37.935.2 108 70-130ND
Styrene ug/kg 35.435.2 101 70-130ND
tert-Butylbenzene ug/kg 34.835.2 99 70-130ND
Tetrachloroethene ug/kg 33.435.2 95 70-130ND
Toluene ug/kg 35.235.2 100 52-163ND
trans-1,2-Dichloroethene ug/kg 33.935.2 97 70-130ND
trans-1,3-Dichloropropene ug/kg 36.135.2 103 70-130ND
Trichloroethene ug/kg 34.835.2 99 49-167ND
Trichlorofluoromethane ug/kg 35.835.2 102 70-130ND
Vinyl acetate ug/kg 48.2J M170.3 68 70-130ND
Vinyl chloride ug/kg 36.335.2 103 70-130ND
Xylene (Total)ug/kg 109105 103 70-130ND
1,2-Dichloroethane-d4 (S)%101 70-132
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92369939
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92369843031
2188210SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg 130 6 30122
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92369939
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92369843031
2188210SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg 7.5J 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg 1.7J 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%100 8103
4-Bromofluorobenzene (S)%98 396
Toluene-d8 (S)%97 698
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 23 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92369939
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
394982
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92369939002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2189572
Associated Lab Samples:92369939002
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.3 01/22/18 12:03
1,1,1-Trichloroethane ug/kg ND 5.3 01/22/18 12:03
1,1,2,2-Tetrachloroethane ug/kg ND 5.3 01/22/18 12:03
1,1,2-Trichloroethane ug/kg ND 5.3 01/22/18 12:03
1,1-Dichloroethane ug/kg ND 5.3 01/22/18 12:03
1,1-Dichloroethene ug/kg ND 5.3 01/22/18 12:03
1,1-Dichloropropene ug/kg ND 5.3 01/22/18 12:03
1,2,3-Trichlorobenzene ug/kg ND 5.3 01/22/18 12:03
1,2,3-Trichloropropane ug/kg ND 5.3 01/22/18 12:03
1,2,4-Trichlorobenzene ug/kg ND 5.3 01/22/18 12:03
1,2,4-Trimethylbenzene ug/kg ND 5.3 01/22/18 12:03
1,2-Dibromo-3-chloropropane ug/kg ND 5.3 01/22/18 12:03
1,2-Dibromoethane (EDB)ug/kg ND 5.3 01/22/18 12:03
1,2-Dichlorobenzene ug/kg ND 5.3 01/22/18 12:03
1,2-Dichloroethane ug/kg ND 5.3 01/22/18 12:03
1,2-Dichloropropane ug/kg ND 5.3 01/22/18 12:03
1,3,5-Trimethylbenzene ug/kg ND 5.3 01/22/18 12:03
1,3-Dichlorobenzene ug/kg ND 5.3 01/22/18 12:03
1,3-Dichloropropane ug/kg ND 5.3 01/22/18 12:03
1,4-Dichlorobenzene ug/kg ND 5.3 01/22/18 12:03
2,2-Dichloropropane ug/kg ND 5.3 01/22/18 12:03
2-Butanone (MEK)ug/kg ND 105 01/22/18 12:03
2-Chlorotoluene ug/kg ND 5.3 01/22/18 12:03
2-Hexanone ug/kg ND 52.5 01/22/18 12:03
4-Chlorotoluene ug/kg ND 5.3 01/22/18 12:03
4-Methyl-2-pentanone (MIBK)ug/kg ND 52.5 01/22/18 12:03
Acetone ug/kg ND 105 01/22/18 12:03
Benzene ug/kg ND 5.3 01/22/18 12:03
Bromobenzene ug/kg ND 5.3 01/22/18 12:03
Bromochloromethane ug/kg ND 5.3 01/22/18 12:03
Bromodichloromethane ug/kg ND 5.3 01/22/18 12:03
Bromoform ug/kg ND 5.3 01/22/18 12:03
Bromomethane ug/kg ND 10.5 01/22/18 12:03
Carbon tetrachloride ug/kg ND 5.3 01/22/18 12:03
Chlorobenzene ug/kg ND 5.3 01/22/18 12:03
Chloroethane ug/kg ND 10.5 01/22/18 12:03
Chloroform ug/kg ND 5.3 01/22/18 12:03
Chloromethane ug/kg ND 10.5 01/22/18 12:03
cis-1,2-Dichloroethene ug/kg ND 5.3 01/22/18 12:03
cis-1,3-Dichloropropene ug/kg ND 5.3 01/22/18 12:03
Dibromochloromethane ug/kg ND 5.3 01/22/18 12:03
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 24 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92369939
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2189572
Associated Lab Samples:92369939002
Matrix:Solid
Analyzed
Dibromomethane ug/kg ND 5.3 01/22/18 12:03
Dichlorodifluoromethane ug/kg ND 10.5 01/22/18 12:03
Diisopropyl ether ug/kg ND 5.3 01/22/18 12:03
Ethylbenzene ug/kg ND 5.3 01/22/18 12:03
Hexachloro-1,3-butadiene ug/kg ND 5.3 01/22/18 12:03
Isopropylbenzene (Cumene)ug/kg ND 5.3 01/22/18 12:03
m&p-Xylene ug/kg ND 10.5 01/22/18 12:03
Methyl-tert-butyl ether ug/kg ND 5.3 01/22/18 12:03
Methylene Chloride ug/kg ND 21.0 01/22/18 12:03
n-Butylbenzene ug/kg ND 5.3 01/22/18 12:03
n-Propylbenzene ug/kg ND 5.3 01/22/18 12:03
Naphthalene ug/kg ND 5.3 01/22/18 12:03
o-Xylene ug/kg ND 5.3 01/22/18 12:03
p-Isopropyltoluene ug/kg ND 5.3 01/22/18 12:03
sec-Butylbenzene ug/kg ND 5.3 01/22/18 12:03
Styrene ug/kg ND 5.3 01/22/18 12:03
tert-Butylbenzene ug/kg ND 5.3 01/22/18 12:03
Tetrachloroethene ug/kg ND 5.3 01/22/18 12:03
Toluene ug/kg ND 5.3 01/22/18 12:03
trans-1,2-Dichloroethene ug/kg ND 5.3 01/22/18 12:03
trans-1,3-Dichloropropene ug/kg ND 5.3 01/22/18 12:03
Trichloroethene ug/kg ND 5.3 01/22/18 12:03
Trichlorofluoromethane ug/kg ND 5.3 01/22/18 12:03
Vinyl acetate ug/kg ND 52.5 01/22/18 12:03
Vinyl chloride ug/kg ND 10.5 01/22/18 12:03
Xylene (Total)ug/kg ND 10.5 01/22/18 12:03
1,2-Dichloroethane-d4 (S)%98 70-132 01/22/18 12:03
4-Bromofluorobenzene (S)%95 70-130 01/22/18 12:03
Toluene-d8 (S)%97 70-130 01/22/18 12:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2189573LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 52.851.8 102 74-137
1,1,1-Trichloroethane ug/kg 45.751.8 88 67-140
1,1,2,2-Tetrachloroethane ug/kg 46.351.8 90 72-141
1,1,2-Trichloroethane ug/kg 48.751.8 94 78-138
1,1-Dichloroethane ug/kg 45.351.8 87 69-134
1,1-Dichloroethene ug/kg 45.851.8 88 67-138
1,1-Dichloropropene ug/kg 45.051.8 87 69-139
1,2,3-Trichlorobenzene ug/kg 52.751.8 102 70-146
1,2,3-Trichloropropane ug/kg 53.551.8 103 69-144
1,2,4-Trichlorobenzene ug/kg 53.851.8 104 68-148
1,2,4-Trimethylbenzene ug/kg 54.551.8 105 74-137
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
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Page 25 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92369939
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2189573LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 51.151.8 99 65-140
1,2-Dibromoethane (EDB)ug/kg 53.251.8 103 77-135
1,2-Dichlorobenzene ug/kg 52.551.8 101 77-141
1,2-Dichloroethane ug/kg 45.051.8 87 65-137
1,2-Dichloropropane ug/kg 49.551.8 96 72-136
1,3,5-Trimethylbenzene ug/kg 54.451.8 105 76-133
1,3-Dichlorobenzene ug/kg 52.551.8 101 74-138
1,3-Dichloropropane ug/kg 53.251.8 103 71-139
1,4-Dichlorobenzene ug/kg 52.551.8 101 76-138
2,2-Dichloropropane ug/kg 45.951.8 89 68-137
2-Butanone (MEK)ug/kg 81.7J104 79 58-147
2-Chlorotoluene ug/kg 54.051.8 104 73-139
2-Hexanone ug/kg 106104 102 62-145
4-Chlorotoluene ug/kg 53.051.8 102 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 103104 99 64-149
Acetone ug/kg 101J104 98 53-153
Benzene ug/kg 48.551.8 94 73-135
Bromobenzene ug/kg 53.251.8 103 75-133
Bromochloromethane ug/kg 45.651.8 88 73-134
Bromodichloromethane ug/kg 48.651.8 94 71-135
Bromoform ug/kg 51.951.8 100 66-141
Bromomethane ug/kg 61.651.8 119 53-160
Carbon tetrachloride ug/kg 49.251.8 95 60-145
Chlorobenzene ug/kg 52.151.8 101 78-130
Chloroethane ug/kg 56.451.8 109 64-149
Chloroform ug/kg 44.851.8 86 70-134
Chloromethane ug/kg 41.751.8 81 52-150
cis-1,2-Dichloroethene ug/kg 44.451.8 86 70-133
cis-1,3-Dichloropropene ug/kg 50.551.8 98 68-134
Dibromochloromethane ug/kg 52.951.8 102 71-138
Dibromomethane ug/kg 49.051.8 95 74-130
Dichlorodifluoromethane ug/kg 42.051.8 81 40-160
Diisopropyl ether ug/kg 46.151.8 89 69-141
Ethylbenzene ug/kg 52.851.8 102 75-133
Hexachloro-1,3-butadiene ug/kg 52.351.8 101 68-143
Isopropylbenzene (Cumene)ug/kg 53.251.8 103 76-143
m&p-Xylene ug/kg 106104 102 75-136
Methyl-tert-butyl ether ug/kg 44.851.8 87 68-144
Methylene Chloride ug/kg 44.151.8 85 45-154
n-Butylbenzene ug/kg 53.251.8 103 72-137
n-Propylbenzene ug/kg 54.151.8 104 76-136
Naphthalene ug/kg 56.251.8 109 68-151
o-Xylene ug/kg 52.551.8 101 76-141
p-Isopropyltoluene ug/kg 53.951.8 104 76-140
sec-Butylbenzene ug/kg 53.351.8 103 79-139
Styrene ug/kg 52.651.8 102 79-137
tert-Butylbenzene ug/kg 48.551.8 94 74-143
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
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Huntersville, NC 28078
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Page 26 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92369939
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2189573LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 49.251.8 95 71-138
Toluene ug/kg 48.851.8 94 74-131
trans-1,2-Dichloroethene ug/kg 46.151.8 89 67-135
trans-1,3-Dichloropropene ug/kg 49.951.8 96 65-146
Trichloroethene ug/kg 51.751.8 100 67-135
Trichlorofluoromethane ug/kg 47.251.8 91 59-144
Vinyl acetate ug/kg 72.8104 70 40-160
Vinyl chloride ug/kg 49.351.8 95 56-141
Xylene (Total)ug/kg 159155 102 76-137
1,2-Dichloroethane-d4 (S)%91 70-132
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2190183MATRIX SPIKE SAMPLE:
MSSpike
Result
92370222001
1,1,1,2-Tetrachloroethane ug/kg 20.523.4 88 70-130ND
1,1,1-Trichloroethane ug/kg 22.223.4 95 70-130ND
1,1,2,2-Tetrachloroethane ug/kg 19.423.4 83 70-130ND
1,1,2-Trichloroethane ug/kg 20.423.4 87 70-130ND
1,1-Dichloroethane ug/kg 21.823.4 93 70-130ND
1,1-Dichloroethene ug/kg 22.323.4 95 49-180ND
1,1-Dichloropropene ug/kg 20.623.4 88 70-130ND
1,2,3-Trichlorobenzene ug/kg 9.3 M123.4 40 70-130ND
1,2,3-Trichloropropane ug/kg 20.923.4 89 70-130ND
1,2,4-Trichlorobenzene ug/kg 10.0 M123.4 43 70-130ND
1,2,4-Trimethylbenzene ug/kg 19.323.4 82 70-130ND
1,2-Dibromo-3-chloropropane ug/kg 18.923.4 80 70-130ND
1,2-Dibromoethane (EDB)ug/kg 20.323.4 86 70-130ND
1,2-Dichlorobenzene ug/kg 15.2 M123.4 65 70-130ND
1,2-Dichloroethane ug/kg 20.823.4 89 70-130ND
1,2-Dichloropropane ug/kg 21.623.4 92 70-130ND
1,3,5-Trimethylbenzene ug/kg 19.923.4 85 70-130ND
1,3-Dichlorobenzene ug/kg 15.1 M123.4 64 70-130ND
1,3-Dichloropropane ug/kg 21.823.4 93 70-130ND
1,4-Dichlorobenzene ug/kg 14.3 M123.4 61 70-130ND
2,2-Dichloropropane ug/kg 21.023.4 89 70-130ND
2-Butanone (MEK)ug/kg 42.2J46.9 90 70-130ND
2-Chlorotoluene ug/kg 18.423.4 79 70-130ND
2-Hexanone ug/kg 43.6J46.9 93 70-130ND
4-Chlorotoluene ug/kg 16.923.4 72 70-130ND
4-Methyl-2-pentanone (MIBK)ug/kg 44.7J46.9 95 70-130ND
Acetone ug/kg 45.6J46.9 97 70-130ND
Benzene ug/kg 22.223.4 95 50-166ND
Bromobenzene ug/kg 17.023.4 73 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
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Page 27 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92369939
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2190183MATRIX SPIKE SAMPLE:
MSSpike
Result
92370222001
Bromochloromethane ug/kg 21.023.4 90 70-130ND
Bromodichloromethane ug/kg 20.623.4 88 70-130ND
Bromoform ug/kg 18.923.4 81 70-130ND
Bromomethane ug/kg 19.523.4 83 70-130ND
Carbon tetrachloride ug/kg 21.923.4 93 70-130ND
Chlorobenzene ug/kg 18.123.4 77 43-169ND
Chloroethane ug/kg 26.323.4 112 70-130ND
Chloroform ug/kg 21.923.4 93 70-130ND
Chloromethane ug/kg 19.923.4 85 70-130ND
cis-1,2-Dichloroethene ug/kg 21.423.4 91 70-130ND
cis-1,3-Dichloropropene ug/kg 20.023.4 85 70-130ND
Dibromochloromethane ug/kg 20.423.4 87 70-130ND
Dibromomethane ug/kg 19.623.4 84 70-130ND
Dichlorodifluoromethane ug/kg 19.423.4 83 70-130ND
Diisopropyl ether ug/kg 22.523.4 96 70-130ND
Ethylbenzene ug/kg 21.323.4 91 70-130ND
Hexachloro-1,3-butadiene ug/kg 14.2 M123.4 60 70-130ND
Isopropylbenzene (Cumene)ug/kg 20.723.4 88 70-130ND
m&p-Xylene ug/kg 43.546.9 82 70-130ND
Methyl-tert-butyl ether ug/kg 21.923.4 93 70-130ND
Methylene Chloride ug/kg 20.2J M123.4 51 70-130ND
n-Butylbenzene ug/kg 17.723.4 76 70-130ND
n-Propylbenzene ug/kg 20.223.4 86 70-130ND
Naphthalene ug/kg 10.2 M123.4 43 70-130ND
o-Xylene ug/kg 20.023.4 85 70-130ND
p-Isopropyltoluene ug/kg 19.223.4 82 70-130ND
sec-Butylbenzene ug/kg 19.523.4 83 70-130ND
Styrene ug/kg 16.1 M123.4 69 70-130ND
tert-Butylbenzene ug/kg 18.623.4 79 70-130ND
Tetrachloroethene ug/kg 20.323.4 87 70-130ND
Toluene ug/kg 20.823.4 89 52-163ND
trans-1,2-Dichloroethene ug/kg 20.323.4 87 70-130ND
trans-1,3-Dichloropropene ug/kg 18.623.4 79 70-130ND
Trichloroethene ug/kg 20.723.4 88 49-167ND
Trichlorofluoromethane ug/kg 22.023.4 94 70-130ND
Vinyl acetate ug/kg 12.3J M146.9 26 70-130ND
Vinyl chloride ug/kg 22.323.4 95 70-130ND
Xylene (Total)ug/kg 63.570.3 90 70-130ND
1,2-Dichloroethane-d4 (S)%101 70-132
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
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9800 Kincey Ave. Suite 100
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Page 28 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92369939
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92370165003
2190182SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg 36.6J 3023.0J
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 29 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92369939
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92370165003
2190182SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg 4.5J 308.7J
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%101 13106
4-Bromofluorobenzene (S)%98 797
Toluene-d8 (S)%100 799
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
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Huntersville, NC 28078
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Page 30 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92369939
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
394683
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples:92369939001, 92369939002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2187858
Associated Lab Samples:92369939001, 92369939002
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 333 01/20/18 13:33
1,2-Dichlorobenzene ug/kg ND 333 01/20/18 13:33
1,3-Dichlorobenzene ug/kg ND 333 01/20/18 13:33
1,4-Dichlorobenzene ug/kg ND 333 01/20/18 13:33
1-Methylnaphthalene ug/kg ND 333 01/20/18 13:33
2,2'-Oxybis(1-chloropropane)ug/kg ND 333 01/20/18 13:33
2,4,5-Trichlorophenol ug/kg ND 333 01/20/18 13:33
2,4,6-Trichlorophenol ug/kg ND 333 01/20/18 13:33
2,4-Dichlorophenol ug/kg ND 333 01/20/18 13:33
2,4-Dimethylphenol ug/kg ND 333 01/20/18 13:33
2,4-Dinitrophenol ug/kg ND 1670 01/20/18 13:33
2,4-Dinitrotoluene ug/kg ND 333 01/20/18 13:33
2,6-Dinitrotoluene ug/kg ND 333 01/20/18 13:33
2-Chloronaphthalene ug/kg ND 333 01/20/18 13:33
2-Chlorophenol ug/kg ND 333 01/20/18 13:33
2-Methylnaphthalene ug/kg ND 333 01/20/18 13:33
2-Methylphenol(o-Cresol)ug/kg ND 333 01/20/18 13:33
2-Nitroaniline ug/kg ND 1670 01/20/18 13:33
2-Nitrophenol ug/kg ND 333 01/20/18 13:33
3&4-Methylphenol(m&p Cresol)ug/kg ND 333 01/20/18 13:33
3,3'-Dichlorobenzidine ug/kg ND 1670 01/20/18 13:33
3-Nitroaniline ug/kg ND 1670 01/20/18 13:33
4,6-Dinitro-2-methylphenol ug/kg ND 667 01/20/18 13:33
4-Bromophenylphenyl ether ug/kg ND 333 01/20/18 13:33
4-Chloro-3-methylphenol ug/kg ND 667 01/20/18 13:33
4-Chloroaniline ug/kg ND 1670 01/20/18 13:33
4-Chlorophenylphenyl ether ug/kg ND 333 01/20/18 13:33
4-Nitroaniline ug/kg ND 667 01/20/18 13:33
4-Nitrophenol ug/kg ND 1670 01/20/18 13:33
Acenaphthene ug/kg ND 333 01/20/18 13:33
Acenaphthylene ug/kg ND 333 01/20/18 13:33
Aniline ug/kg ND 333 01/20/18 13:33
Anthracene ug/kg ND 333 01/20/18 13:33
Benzo(a)anthracene ug/kg ND 333 01/20/18 13:33
Benzo(a)pyrene ug/kg ND 333 01/20/18 13:33
Benzo(b)fluoranthene ug/kg ND 333 01/20/18 13:33
Benzo(g,h,i)perylene ug/kg ND 333 01/20/18 13:33
Benzo(k)fluoranthene ug/kg ND 333 01/20/18 13:33
Benzoic Acid ug/kg ND 1670 01/20/18 13:33
Benzyl alcohol ug/kg ND 667 01/20/18 13:33
bis(2-Chloroethoxy)methane ug/kg ND 333 01/20/18 13:33
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
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9800 Kincey Ave. Suite 100
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Page 31 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92369939
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2187858
Associated Lab Samples:92369939001, 92369939002
Matrix:Solid
Analyzed
bis(2-Chloroethyl) ether ug/kg ND 333 01/20/18 13:33
bis(2-Ethylhexyl)phthalate ug/kg ND 333 01/20/18 13:33
Butylbenzylphthalate ug/kg ND 333 01/20/18 13:33
Chrysene ug/kg ND 333 01/20/18 13:33
Di-n-butylphthalate ug/kg ND 333 01/20/18 13:33
Di-n-octylphthalate ug/kg ND 333 01/20/18 13:33
Dibenz(a,h)anthracene ug/kg ND 333 01/20/18 13:33
Dibenzofuran ug/kg ND 333 01/20/18 13:33
Diethylphthalate ug/kg ND 333 01/20/18 13:33
Dimethylphthalate ug/kg ND 333 01/20/18 13:33
Fluoranthene ug/kg ND 333 01/20/18 13:33
Fluorene ug/kg ND 333 01/20/18 13:33
Hexachloro-1,3-butadiene ug/kg ND 333 01/20/18 13:33
Hexachlorobenzene ug/kg ND 333 01/20/18 13:33
Hexachlorocyclopentadiene ug/kg ND 333 01/20/18 13:33
Hexachloroethane ug/kg ND 333 01/20/18 13:33
Indeno(1,2,3-cd)pyrene ug/kg ND 333 01/20/18 13:33
Isophorone ug/kg ND 333 01/20/18 13:33
N-Nitroso-di-n-propylamine ug/kg ND 333 01/20/18 13:33
N-Nitrosodimethylamine ug/kg ND 333 01/20/18 13:33
N-Nitrosodiphenylamine ug/kg ND 333 01/20/18 13:33
Naphthalene ug/kg ND 333 01/20/18 13:33
Nitrobenzene ug/kg ND 333 01/20/18 13:33
Pentachlorophenol ug/kg ND 1670 01/20/18 13:33
Phenanthrene ug/kg ND 333 01/20/18 13:33
Phenol ug/kg ND 333 01/20/18 13:33
Pyrene ug/kg ND 333 01/20/18 13:33
2,4,6-Tribromophenol (S)%96 27-110 01/20/18 13:33
2-Fluorobiphenyl (S)%95 30-110 01/20/18 13:33
2-Fluorophenol (S)%87 13-110 01/20/18 13:33
Nitrobenzene-d5 (S)%87 23-110 01/20/18 13:33
Phenol-d6 (S)%86 22-110 01/20/18 13:33
Terphenyl-d14 (S)%114 28-110 S301/20/18 13:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2187859LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2187860
1,2,4-Trichlorobenzene ug/kg 751825 91 36-12087719 4 30
1,2-Dichlorobenzene ug/kg 735825 89 41-12083684 7 30
1,3-Dichlorobenzene ug/kg 733825 89 66-12082675 8 30
1,4-Dichlorobenzene ug/kg 727825 88 42-12082676 7 30
1-Methylnaphthalene ug/kg 867825 105 40-12089733 17 30
2,2'-Oxybis(1-chloropropane)ug/kg 599825 73 17-12069568 5 30
2,4,5-Trichlorophenol ug/kg 730825 88 37-12086708 3 30
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92369939
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2187859LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2187860
2,4,6-Trichlorophenol ug/kg 784825 95 40-12084695 12 30
2,4-Dichlorophenol ug/kg 712825 86 33-12081669 6 30
2,4-Dimethylphenol ug/kg 676825 82 36-12079654 3 30
2,4-Dinitrophenol ug/kg 33904130 82 22-121843460 2 30
2,4-Dinitrotoluene ug/kg 737825 89 60-12089734 0 30
2,6-Dinitrotoluene ug/kg 747825 91 54-12089737 1 30
2-Chloronaphthalene ug/kg 757825 92 41-12084693 9 30
2-Chlorophenol ug/kg 769825 93 39-12083684 12 30
2-Methylnaphthalene ug/kg 918825 111 26-12088732 23 30
2-Methylphenol(o-Cresol)ug/kg 776825 94 41-12086713 9 30
2-Nitroaniline ug/kg 1350J1650 82 45-120821360J 30
2-Nitrophenol ug/kg 722825 87 35-12081673 7 30
3&4-Methylphenol(m&p Cresol)ug/kg 660825 80 35-12075623 6 30
3,3'-Dichlorobenzidine ug/kg 1510J1650 92 16-125821350J 30
3-Nitroaniline ug/kg 1410J1650 85 45-120911500J 30
4,6-Dinitro-2-methylphenol ug/kg 17301650 105 46-120981620 7 30
4-Bromophenylphenyl ether ug/kg 758825 92 36-12083687 10 30
4-Chloro-3-methylphenol ug/kg 14801650 90 37-120891470 1 30
4-Chloroaniline ug/kg 1320J1650 80 35-120811340J 30
4-Chlorophenylphenyl ether ug/kg 689825 83 30-12080665 3 30
4-Nitroaniline ug/kg 14001650 85 48-120861430 2 30
4-Nitrophenol ug/kg 35704130 86 43-120873580 0 30
Acenaphthene ug/kg 750825 91 46-12086714 5 30
Acenaphthylene ug/kg 756825 92 46-12091753 0 30
Aniline ug/kg 867 R182510533-12075620 33 30
Anthracene ug/kg 777825 94 63-12087719 8 30
Benzo(a)anthracene ug/kg 811825 98 61-12094779 4 30
Benzo(a)pyrene ug/kg 792825 96 59-120102848 7 30
Benzo(b)fluoranthene ug/kg 782825 95 55-12094779 0 30
Benzo(g,h,i)perylene ug/kg 766825 93 57-12095789 3 30
Benzo(k)fluoranthene ug/kg 795825 96 56-12095787 1 30
Benzoic Acid ug/kg 23204130 56 13-120662730 16 30
Benzyl alcohol ug/kg 13501650 82 34-120771280 5 30
bis(2-Chloroethoxy)methane ug/kg 710825 86 21-12085700 1 30
bis(2-Chloroethyl) ether ug/kg 784825 95 25-12083690 13 30
bis(2-Ethylhexyl)phthalate ug/kg 927825 112 56-123107884 5 30
Butylbenzylphthalate ug/kg 1120 L182513557-120113933 18 30
Chrysene ug/kg 791825 96 64-12096799 1 30
Di-n-butylphthalate ug/kg 925825 112 58-12096792 15 30
Di-n-octylphthalate ug/kg 950 L182511547-1211221010 6 30
Dibenz(a,h)anthracene ug/kg 792825 96 56-12092765 4 30
Dibenzofuran ug/kg 730825 88 43-12083691 6 30
Diethylphthalate ug/kg 745825 90 55-12088731 2 30
Dimethylphthalate ug/kg 770825 93 54-12096791 3 30
Fluoranthene ug/kg 756825 92 61-12086709 6 30
Fluorene ug/kg 744825 90 51-12086711 5 30
Hexachloro-1,3-butadiene ug/kg 775825 94 22-12092758 2 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92369939
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2187859LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2187860
Hexachlorobenzene ug/kg 793825 96 53-12089739 7 30
Hexachlorocyclopentadiene ug/kg 830825 101 18-15078643 25 30
Hexachloroethane ug/kg 750825 91 39-12083687 9 30
Indeno(1,2,3-cd)pyrene ug/kg 772825 94 58-12092760 2 30
Isophorone ug/kg 679825 82 38-12080660 3 30
N-Nitroso-di-n-propylamine ug/kg 664825 80 30-12080660 1 30
N-Nitrosodimethylamine ug/kg 762825 92 32-12086715 6 30
N-Nitrosodiphenylamine ug/kg 769825 93 50-12086712 8 30
Naphthalene ug/kg 721825 87 38-12082679 6 30
Nitrobenzene ug/kg 715825 87 37-12084693 3 30
Pentachlorophenol ug/kg 1160J1650 71 10-120661090J 30
Phenanthrene ug/kg 759825 92 62-12089739 3 30
Phenol ug/kg 988 R182512037-12087720 31 30
Pyrene ug/kg 818825 99 63-12099817 0 30
2,4,6-Tribromophenol (S)%101 27-11086
2-Fluorobiphenyl (S)%90 30-11081
2-Fluorophenol (S)%89 13-11088
Nitrobenzene-d5 (S)%89 23-11081
Phenol-d6 (S)%S011622-11081
Terphenyl-d14 (S)%103 28-11099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92369939
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
394671
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92369939001
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92369077006
2187800SAMPLE DUPLICATE:
Percent Moisture %16.2 5 2515.3
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92369939001
2187801SAMPLE DUPLICATE:
Percent Moisture %20.5 0 2520.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92369939
BCP-064
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
394698
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92369939002
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92369884001
2187969SAMPLE DUPLICATE:
Percent Moisture %18.1 3 2517.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 41
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92369939
BCP-064
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
Pace Analytical Services - Ormond BeachPASI-O
ANALYTE QUALIFIERS
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
Surrogate recovery outside laboratory control limits (confirmed by re-analysis).S1
Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.S3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 41
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92369939
BCP-064
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92369939001 420120 420231STOCKPILE-1 EPA 3050 EPA 6010
92369939002 420652 420661STOCKPILE-2 EPA 3050 EPA 6010
92369939001 420008 420053STOCKPILE-1 EPA 7471 EPA 7471
92369939002 420717 420782STOCKPILE-2 EPA 7471 EPA 7471
92369939001 394683 394924STOCKPILE-1 EPA 3546 EPA 8270
92369939002 394683 394924STOCKPILE-2 EPA 3546 EPA 8270
92369939001 394662STOCKPILE-1 EPA 8260
92369939002 394982STOCKPILE-2 EPA 8260
92369939001 394671STOCKPILE-1 ASTM D2974-87
92369939002 394698STOCKPILE-2 ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/29/2018 02:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 41
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Table of Contents
Table of Contents
Sample Summary 4
Case Narrative 6
Sample Results 9
17J1417-01 9
17J1417-02 12
17J1417-03 16
17J1417-04 19
17J1417-05 23
17J1417-06 26
17J1417-07 30
17J1417-08 33
17J1417-09 37
17J1417-10 43
17J1417-11 49
17J1417-12 52
17J1417-13 56
17J1417-14 59
17J1417-15 63
17J1417-16 66
17J1417-17 72
17J1417-18 75
17J1417-19 79
Sample Preparation Information 85
QC Data 87
Volatile Organic Compounds by GC/MS 87
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B189634 87
Semivolatile Organic Compounds by GC/MS 92
B189567 92
B189653 96
B189841 101
Metals Analyses (Total) 107
B189826 107
B189827 108
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) 109
B189622 109
Flag/Qualifier Summary 110
Certifications 111
Chain of Custody/Sample Receipt 115
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Page 1 of 53
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Table of Contents
Sample Summary 3
Case Narrative 4
Sample Results 7
17J1448-01 7
17J1448-02 10
17J1448-03 14
17J1448-04 17
17J1448-05 21
17J1448-06 24
17J1448-07 28
17J1448-08 31
Sample Preparation Information 35
QC Data 36
Volatile Organic Compounds by GC/MS 36
B189790 36
Semivolatile Organic Compounds by GC/MS 41
B189696 41
Metals Analyses (Total) 46
B189826 46
B189827 46
Flag/Qualifier Summary 47
Certifications 48
Chain of Custody/Sample Receipt 52
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