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HomeMy WebLinkAbout1302_CabarrusCountyCDLF_GWMR_DIN28216_20161101C a b a r r u s C o u n t y C & D L a n d f i l l S e m i - A n n u a l S a m p l i n g R e p o r t F a c i l i t y P e r m i t # 1 3 0 2 - C D L F - 2 0 0 6 ( N o v e m b e r 2 0 1 6 S a m p l i n g E v e n t ) P r e p a r e d F e b r u a r y 2 0 1 7 5400 Glenwood Avenue, Suite 400 Raleigh, North Carolina 27612 tel: 919 325-3500 fax: 919 781-5730 February 9, 2017 Ms. Jaclynne Drummond North Carolina Department of Environmental Quality Division of Waste Management Solid Waste Section 2090 U.S. 70 Highway Swannanoa, North Carolina 28778 Subject: November 2016 Semi-Annual Sampling Report Cabarrus County C&D Landfill Facility Permit No. 1302-CDLF-2006 Dear Ms. Drummond: CDM Smith Inc., on behalf of Cabarrus County, is submitting an electronic copy of the November 2016 semi-annual sampling event report for the Cabarrus County C&D Landfill. This letter report presents the results of the recently completed sampling at the C&D Landfill and constitutes the second semi-annual sampling event for 2016. The approved monitoring well network for the C&D Landfill consists of background wells CD-1s and -1d; compliance wells CD-2, -3, -4 Rep, -7, and -8; and surface water sample location SW-3. CD-4 Rep was installed in January 2009 as part of the proposed Phase 1 C&D Landfill expansion. Monitoring wells CD-7 and -8, formerly piezometers B-7 and -19 respectively, were added to the monitoring program in July 2014 as part of the Phase 2 C&D Landfill expansion. Field activities and sampling results for the groundwater and surface water samples are discussed below. Field Activities Groundwater samples from the Cabarrus County C&D Landfill were collected on November 1-2, 2016. Groundwater samples were collected from the monitoring wells by use of disposable, laboratory decontaminated Teflon™ bailers or a QED bladder pump system using low-flow sampling techniques. Monitoring well locations and the surface water location for the C&D Landfill are provided on Figure 1. Groundwater elevations were measured at each well prior to sampling and are presented in Table 1. Well construction details for each monitoring well are also provided in Table 1. These groundwater elevations were used to construct potentiometric contours for this sampling event and are presented on Figure 1. After depth to groundwater was measured, each well was purged prior to sampling to provide fresh formation water within the well water column. Each purge volume was measured for pH, conductivity, turbidity, temperature, dissolved oxygen, and oxidation-reduction potential using a YSI-556 Ms. Jaclynne Drummond February 9, 2017 Page 2 multi-parameter water quality meter and Oakton T100 or Lamotte 2020 turbidity meters. The water quality parameters at the time of sampling are presented in Table 2. The headspace of each monitoring well was screened for methane gas using a RKI Eagle multi-gas monitor. Screening results are provided in Appendix A. Sampling Results Pace Analytical Services, Inc., located in Peachtree Corners, Georgia, analyzed the groundwater samples for North Carolina Appendix I volatile organic compounds (VOCs) plus tetrahydrofuran, North Carolina Appendix I metals plus iron, mercury, and manganese, alkalinity, total dissolved solids, chloride, and sulfate with the exception of CD-4 Rep. Samples collected from CD-4 Rep were analyzed for North Carolina Appendix I VOCs and metals. In accordance with the North Carolina Department of Environmental Quality’s Solid Waste Section (SWS) guidelines the analytical results were reported to the laboratory specific method detection limit (MDL) and are quantifiable at or below SWS Limits (SWSLs). All monitoring wells for the C&D Landfill had detections of analytes above the MDL but below the SWSL. These detections were qualified as estimated or “J” flags. The following list indicates the analytes detected above the laboratory specific MDL at each sampling location. No “J” flag or general chemistry detections are provided. Underlined analytes exceeded the 15A NCAC 02L .0202 (NC 2L) Groundwater Quality Standard, Groundwater Protection Standard, or the 15A NCAC 02B Surface Water Quality Standard for Class C Waters. CD-1s (Background) Metals: Iron, Manganese Volatile Organic Compounds: None Detected CD-1d (Background) Metals: Iron Volatile Organic Compounds: None Detected CD-2 Metals: Iron, Manganese, Zinc Volatile Organic Compounds: None Detected CD-3 Metals: Barium, Iron, Manganese Volatile Organic Compounds: None Detected Ms. Jaclynne Drummond February 9, 2017 Page 3 CD-4 Rep Metals: None Detected Volatile Organic Compounds: None Detected CD-7 Metals: Iron, Manganese Volatile Organic Compounds: None Detected CD-8 Metals: Copper, Iron, Manganese, Zinc Volatile Organic Compounds: None Detected SW-3 Metals: Dry Volatile Organic Compounds: Dry “J” flags were not included in the previous list, but several locations had “J” flag detections that exceeded the standards. These constituents along with their location are listed below. Cobalt: CD-1s, -2, -3, -4 Rep, and -8 Vanadium: CD-2, -4 Rep, and -8 A duplicate sample, identified as Dup, was collected from CD-8 and had similar analyte concentrations as those detected in CD-8. An equipment blank was not collected due to an oversight by the sampling team. Similar sampling equipment and supplies were used for the November 2016 sampling event compared to historical events. Historical analytical data has never shown impacts from sampling equipment or supplies. No analytes were detected above laboratory MDLs in the trip blank. Metals detected above the standards are likely natural occurring based on concentrations in the background monitoring wells or are from elevated turbidity at the time of sample collection. No VOCs were detected above the NC 2L Standards. General chemistry results were below the NC 2L Standards with the exception of total dissolved solids (TDS). TDS were detected above the NC 2L Standard in CD-2 and -8. A complete summary of all detected constituents from the November 2016 sampling event is presented in Table 3. The laboratory analytical report is provided in Appendix A. The next semi-annual sampling event will be completed in the spring of 2017. In accordance with recent changes to the SWS reporting requirements, a 14-Day Notification will be submitted with the Spring 2017 sampling report, if constituents exceed their respective limits. In addition, CDM Smith will prepare an Alternate Source Demonstration (ASD) for Inorganic Compounds at the C&D Landfill. There is an approved ASD for volatile organic compounds already on file for this site. Ms. Jaclynne Drummond February 9, 2017 Page 4 If you have any questions or require further explanation, do not hesitate to call me at (919) 325-3500 or by email at colonemf@cdmsmith.com. Very truly yours, Mathew F. Colone, P.G. CDM Smith Inc. cc: Kevin Grant, Cabarrus County Ta b l e 1 Mo n i t o r i n g W e l l C o n s t r u c t i o n S u m m a r y a n d G r o u n d w a t e r E l e v a t i o n s No v e m b e r 2 0 1 6 S e m i - A n n u a l S a m p l i n g E v e n t Ca b a r r u s C o u n t y C & D L a n d f i l l Fa c i l i t y P e r m i t N u m b e r 1 3 0 2 - C D L F - 2 0 0 6 Sc r e e n In t e r v a l Fi l t e r In t e r v a l Se a l In t e r v a l TO C El e v a t i o n Depth to Groundwater (feet BTOC)Groundwater Elevation 13 0 2 - C D L F - 2 0 0 6 CD - 1 s (b a c k g r o u n d w e l l ) 8/ 7 / 2 0 0 6 3 5 . 4 7 7 8 8 8 0 . 5 2 3 3 4 S a p r o l i t e 2 9 . 5 3 1 8 . 0 - 2 8 . 0 1 6 . 0 - 2 8 . 0 1 4 . 0 - 1 6 . 0 2 . 0 7 5 5 . 0 0 2 5 . 2 3 7 2 9 . 7 7 13 0 2 - C D L F - 2 0 0 6 CD - 1 d (b a c k g r o u n d w e l l ) 7/ 2 1 / 2 0 0 4 3 5 . 4 7 7 8 8 8 0 . 5 2 3 4 0 P W R 5 2 . 1 5 4 0 . 0 - 5 0 . 0 3 8 . 0 - 5 0 . 0 3 6 . 0 - 3 8 . 0 2 . 0 7 5 7 . 4 0 2 7 . 8 3 7 2 9 . 5 7 13 0 2 - C D L F - 2 0 0 6 C D - 2 9 / 1 2 / 2 0 0 6 3 5 . 4 7 6 9 8 8 0 . 5 2 4 9 4 S a p r o l i t e 2 5 . 6 9 9 . 0 - 2 4 . 0 7 . 0 - 2 4 . 0 5 . 0 - 7 . 0 2 . 0 7 3 3 . 0 0 1 5 . 6 0 7 1 7 . 4 0 13 0 2 - C D L F - 2 0 0 6 C D - 3 7 / 1 / 2 0 1 4 3 5 . 4 7 5 8 0 8 0 . 5 2 5 0 2 S a p r o l i t e / P W R 5 3 . 5 0 3 5 . 0 - 5 0 . 0 3 2 . 0 - 5 0 . 0 3 0 . 0 - 3 2 . 0 2 . 0 7 4 4 . 4 8 3 8 . 9 1 7 0 5 . 5 7 13 0 2 - C D L F - 2 0 0 6 C D - 4 R e p 1 / 1 5 / 2 0 0 9 3 5 . 4 7 6 5 6 8 0 . 5 2 2 1 0 S a p r o l i t e 1 9 . 4 1 6 . 0 - 1 6 . 0 4 . 0 - 1 6 . 0 2 . 0 - 4 . 0 2 . 0 7 3 9 . 1 5 1 0 . 2 5 7 2 8 . 9 0 13 0 2 - C D L F - 2 0 0 6 C D - 7 1 1 / 2 5 / 2 0 0 2 3 5 . 4 7 5 6 7 8 0 . 5 2 5 5 1 B e d r o c k 4 6 . 3 1 3 4 . 0 - 4 4 . 0 3 2 . 0 - 4 4 . 0 3 0 . 0 - 3 2 . 0 2 . 0 7 4 4 . 8 1 4 0 . 2 7 7 0 4 . 5 4 13 0 2 - C D L F - 2 0 0 6 C D - 8 7 / 1 / 2 0 1 4 3 5 . 4 7 5 1 8 8 0 . 5 2 4 9 7 P W R 4 3 . 4 0 3 3 . 0 - 4 3 . 0 3 1 . 0 - 4 3 . 0 2 9 . 0 - 3 1 . 0 2 . 0 7 3 8 . 3 9 3 2 . 7 4 7 0 5 . 6 5 No t e s : 1. B T O C - B e l o w T o p o f C a s i n g 2. b g s - B e l o w G r o u n d S u r f a c e 3. P W R - P a r t i a l l y W e a t h e r e d R o c k Fa c i l i t y P e r m i t Nu m b e r Gr o u n d w a t e r E l e v a t i o n s - M e a s u r e d 1 0 / 3 1 / 2 0 1 6 De p t h ( f e e t b g s ) To t a l D e p t h (f e e t B T O C ) Mo n i t o r i n g W e l l Dia m e t e r (in c h e s ) Mo n i t o r i n g W e l l Co d e Ge o l o g y o f Sc r e e n e d I n t e r v a l In s t a l l a t i o n Da t e La t i t u d e L o n g i t u d e Pa g e 1 o f 1 January 2017 Table 2 Water Quality Measurements November 2016 Semi-Annual Sampling Event Cabarrus County C&D Landfill Facility Permit Number 1302-CDLF-2006 pH (S.U.) Conductivity (µS/cm) Temperature (degrees Celsius) Dissolved Oxygen (mg/L) ORP (mVs) Turbidity (NTUs) CD-1s (background well)5.05 113 16.1 4.49 360.2 6 CD-1d (background well)5.34 124 15.9 3.10 330.0 8 CD-2 4.59 103 17.0 2.48 183.8 48 CD-3*5.33 484 16.5 1.24 63.6 13 CD-4 Rep 5.28 209 17.0 1.35 79.3 3 CD-7 5.36 417 15.8 1.88 118.1 7 CD-8 5.76 246 17.0 1.37 29.0 48 Surface Water Sample Location SW-3 Notes: 1. CD-4 Rep was installed as part of the proposed Phase 1 C&D Landfill expansion in November 2010. 2. * CD-3 was relocated on July 1, 2014, as part of the Phase 2 C&D Landfill Expansion. 3. µS/cm - Microsiemens per centimeter 4. mg/L - Milligrams per liter 5. ORP - Oxidation-Reduction Potential 6. NTUs - Nephelometric Turbidity Units 7. mVs - Millivolts 8. S.U. - Standard Unit Water Quality Measurements Monitoring Well Code DRY Page 1 of 1 January 2017 Table 3a Detected Groundwater Constituents - General Chemistry and Metals November 2016 Semi-Annual Sampling Event Cabarrus County C&D Landfill Facility Permit Number 1302-CDLF-2006 Al k a l i n i t y Ch e m i c a l O x y g e n D e m a n d Ch l o r i d e Fe r r o u s I r o n Nit r a t e Su l f a t e To t a l D i s s o l v e d S o l i d s An t i m o n y Ar s e n i c Ba r i u m Be r y l l i u m Ca d m i u m Ch r o m i u m Co b a l t Co p p e r Le a d Ir o n Ma n g a n e s e Me r c u r y Ni c k e l Se l e n i u m Sil v e r Th a l l i u m Va n a d i u m Zin c NE NE 250,000 NE 10,000 250,000 500,000 1*10 700 4*2 10 1*1,000 15 300 50 1 100 20 20 0.2*0.3*1,000 NE NE NE NE 10,000 250,000 NE 6 10 100 1 1 10 10 10 10 300 50 0.2 50 10 10 5.5 25 10 CD-1s 3-May-11 47,000 3,600 1,200J 146,000 81.4J 0.19J 5.45JB 4.23J 16.0 2.32J 7,770 190 5.93J 0.14J 20.6J 26.5 CD-1s 8-Nov-11 40,000 4,000 1,100J 65,000 59.7J 0.25JB 4.46J 2.67J 12.4 1.9J 5,350 127 4.41J 0.08J 11.2J 18.2 CD-1s 7-May-12 46,000 3,900 158,000 45.5J 3.30J 1.19J 8.75J 1.12J 3,120 63.4 3.01J 12.7J 12.6B CD-1s 28-Nov-12 39,000 4,100 0 110,000 63.8J 0.11J 5.65J 3.05J 11.6 1.43J 5,210 139 4.66J 17.1J 16.9 CD-1s 7-May-13 42,000 4,000 220 120,000 0.94J 2.4JB 35.6J 0.88J 0.67J 4.04J 0.39J 1,340 37.7 1.78J 0.13J 6.06J 5.08J CD-1s 5-Nov-13 30,000 3,800 2,420 80,500 46.8J 0.12J 3.59J 1.63J 10.2 1.35J 4,200 82.2 3.50J 18.4JB 15.4B CD-1s 6-May-14 42,000 3,800 0 111,000 28.8J 4.14JB 1.48J 0.11J 347B 10.1B 1.03J 0.31J 3.40J 2.98JB CD-1s 4-Nov-14 41,000 3,900 0 102,000 28.7J 0.13J 1.31J 0.06J 118 6.6J 1.04J 0.11J 2.57JB 1.58J CD-1s 5-May-15 38,000 3,800 0 <5,000 113,000 1.63J 29.5JB 1.33J 0.15J 371 13.8 0.103JB 1.17J 2.40J 2.75JB CD-1s 27-Oct-15 43,000 30,600 3,800 0 130J 110,000 1.00J 28.4J 0.80J 0.39J 0.75J 0.12J 234 35.9 1.21J 4.19CN,J 0.15J 4.10J 3.36B-01,J CD-1s 17-May-16 43,000 <10,000 3,700 0 79J 1,000J 130,000 23.9J 0.94J 0.99J 0.12J 446 17.0J 1.01J 4.70J 1.93J CD-1s 1-Nov-16 46,000 26,500 4,200 0 67J,H-02 <5,000 71,000 30.5J 1.23J 1.32J 1.36J 0.28J 647 70.8 1.35J 4.30J CD-1d 3-May-11 57,000 2,600 3,000J 206,000 2.44J 231 2.03 16.7 18.6 112 14.0 49,400 659 22.3J 0.11J 101 103 CD-1d 8-Nov-11 30,000 2,900 3,000J 98,000 74.5J 0.51J 4.08J 4.27J 27 2.84J 9,190 144 5.68J 24.6J 26.3 CD-1d 7-May-12 50,000 2,800 150,000 72.4J 0.58J 3.91J 4.67J 25 2.81J 9,380 170 5.58J 26 27.9B CD-1d 28-Nov-12 46,000 3,000 0 128,000 0.33J 37.7J 0.07J 2.38J 0.94J 12.6 1.14J 1,900 41.4 2.50J 8.90J 13 CD-1d 7-May-13 52,000 3,000 560 125,000 0.88J 1.02JB 31.2J 0.07J 0.78J 4.5J 0.49J 1,080 25.5 1.92J 6.18J 13.1 CD-1d 5-Nov-13 42,000 3,000 700 104,000 35.0J 0.86J 4.34J 1.13J 1.90J 812 46.2 17.1JB 10.8B CD-1d 6-May-14 46,000 2,900 119,000 1.14J 37.8J 0.07J 0.05J 3.22JB 1.16J 7.34J 0.81J 1,610B 49.6B 2.74J 0.12J 6.16J 9.41JB CD-1d 4-Nov-14 43,000 3,100 0 101,000 43.1J 0.16J 0.11J 2.25J 9.09J 0.87J 3,400 88.5 2.88J 10.2JB 10.7 CD-1d 5-May-15 44,000 2,900 0 <5000 115,000 34.5JB 0.84J 3.63J 0.39J 1,320 32.5 1.42J 5.18J 3.68JB CD-1d 27-Oct-15 46,000 2,900 0 120,000 0.42J 42.3J 0.13J 1.87J 2.15J 8.18J 0.97J 3,170 87.4 2.49J 4.37CN,J 0.06J 10.9J 14.0B-01 CD-1d 17-May-16 96,000 18,000 0 <50 14,000J 202,000 81.3J 0.46J 4.86J 7.42J 26.0 3.13J 12,000 287 7.11J 2.11J 0.07J 29.3 29.7 CD-1d 1-Nov-16 52,000 3,400 0 <5,000 99,000 32.6J 1.19J 0.77J 2.82J 0.33J 1,200 31.3J 1.24J 7.96J 4.29J CD-2 3-May-11 2,850 6,800 1,300J 209,000 1.78J 55.9J 0.23J 3.04JB 3.62J 7.91J 2.75J 5,560 92.2 0.031J 3.60J 22.2J 12B CD-2 8-Nov-11 9,000 7,500 1,400J 41,500 22.1J 0.21JB 1.41J 2.15J 3.53J 1.07J 1,660 47.4 1.9J 4.99J CD-2 7-May-12 21,000 7,200 104,000 36.4J 0.19J 2.71J 3.38J 5.03J 1.94J 2,760 74.1 2.95J 9.8J 16.5B CD-2 28-Nov-12 25,000 6,700 (1)39.5J 0.13J 2.89J 2.95J 4.40J 1.42J 2,720 67.2 2.72J 10.1J 7.92J CD-2 7-May-13 20,000 7,200 80,000 0.34J 1.25JB 39.4J 0.23J 1.32J 2.8J 4.44J 1.34J 2,450 57.8 2.59J 0.08J 9.02J 8.79J CD-2 5-Nov-13 28,000 6,600 55,000 45.1J 0.20J 0.64J 3.31J 4.01J 1.60J 1,600 68.8 0.087J 2.38J 14J 7.77JB CD-2 7-May-14 16,000 8,200 135,000 37.5J 0.10J 1.98JB 2.48J 2.26J 0.78JB 1,130B 49.3 0.105J 2.00J 5.00J CD-2 5-Nov-14 25,000 7,500 330,000 0.07J 46.0J 2.21JB 2.69J 3.59J 1.10J 2,000B 59.6 (1)2.47J 7.23J 6.92JB CD-2 6-May-15 16,000 8,100 136,000 52.0JB 0.18J 2.10JB 2.90J 5.91J 1.37J 2240 57.6 0.158JB 3.74J 6.97J 8.02JB CD-2 27-Oct-15 7,750 7,300 5,900J 178,000 0.83J 60.0J 0.42J 3.94B-01,J 3.71J 8.71J 2.67J 5,150 83.8 0.073J 5.50J 4.05CN,J 0.08J 16.3J 13.3 CD-2 18-May-16 20,000 7,900 <5,000 147,000 49.8J 0.22J 2.32J 3.41J 3.56J 1.20J 2,350 71.7 0.189J 2.68J 8.34J 7.62J CD-2 1-Nov-16 20,000 8,100 <5,000 850,000H-02 64.5J 0.26J 3.10J 4.15J 5.48J 2.55J 4,010 99.5 0.056J 3.11J 15.3J 13.9 1302-CDLF-2006 1302-CDLF-2006 1302-CDLF-2006 North Carolina 2L or Groundwater Protection Standard Solid Waste Section Limit MetalsGeneral Chemistry Sa m p l e D a t e Mo n i t o r i n g W e l l C o d e Fa c i l i t y P e r m i t N u m b e r Page 1 of 6 January 2017 Table 3a Detected Groundwater Constituents - General Chemistry and Metals November 2016 Semi-Annual Sampling Event Cabarrus County C&D Landfill Facility Permit Number 1302-CDLF-2006 Al k a l i n i t y Ch e m i c a l O x y g e n D e m a n d Ch l o r i d e Fe r r o u s I r o n Nit r a t e Su l f a t e To t a l D i s s o l v e d S o l i d s An t i m o n y Ar s e n i c Ba r i u m Be r y l l i u m Ca d m i u m Ch r o m i u m Co b a l t Co p p e r Le a d Ir o n Ma n g a n e s e Me r c u r y Ni c k e l Se l e n i u m Sil v e r Th a l l i u m Va n a d i u m Zin c NE NE 250,000 NE 10,000 250,000 500,000 1*10 700 4*2 10 1*1,000 15 300 50 1 100 20 20 0.2*0.3*1,000 NE NE NE NE 10,000 250,000 NE 6 10 100 1 1 10 10 10 10 300 50 0.2 50 10 10 5.5 25 10 1302-CDLF-2006 North Carolina 2L or Groundwater Protection Standard Solid Waste Section Limit MetalsGeneral Chemistry Sa m p l e D a t e Mo n i t o r i n g W e l l C o d e Fa c i l i t y P e r m i t N u m b e r CD-3 3-May-11 105,000 4,300 3,200J 404,000 48.9J 0.11J 2.36J 7.57J 1.30J 3,580 93.6 2.48J 12.2J 8.64JB CD-3 8-Nov-11 85,000 5,400 3,900J 144,000 25.5J 0.65J 1.01J 178 24.9 1.48J 5.16J CD-3 7-May-12 75,000 4,500 177,000 41.7J 0.84J 1.27J 3.84J 0.54J 1,170 32.6 3.37J 6.18J 6.81J,B CD-3 28-Nov-12 104,000 5,100 (1)46.7J 1.41J 1.90J 4.35J 0.82J 1,740 68.9 1.86J 9.52J 6.93J CD-3 7-May-13 122,000 4,800 181,000 33.8J 1.20J 2.35J 0.42J 880 56.3 1.41J 5.86J 2.89J CD-3 5-Nov-13 59,000 4,500 121,000 64J 0.21J 0.74J 3.47J 10.6 2.06J 5,170 139 3.25J 21.2J 12.2B CD-3 7-May-14 61,600 4,200 127,000 28.7J 1.66JB 0.72J 83.2B 4.4J 1.14J 2.42J CD-3 5-Nov-14 82,000 13,000 13,000J 425,000 162 0.14J 1.85JB 3.00J 6.22J 1.21J 3,770B 1,030 (1)8.65J 12.9J 9.94JB CD-3 6-May-15 89,000 13,000 22,000J 280,000 1.38J 159 0.11J 1.26J 2.84J 0.42J 1,230B 1,090 0.102JB 7.25J 5.29J 5.93J CD-3 27-Oct-15 95,000 13,000 23,000J 255,000 155 0.10J 1.02B-01,J 1.82J 3.91J 0.68J 2,010 936 7.72J 2.60CN,J 6.03J 6.81J CD-3 18-May-16 100,000 14,000 26,000J 311,000 194 0.12J 1.60J 1.35J 0.24J 607 1,010 7.88J 1.19J 4.02J 3.73J CD-3 1-Nov-16 95,000 14,000 27,000J 162,000 158 0.13J 2.07J 2.77J 0.49J 1,400 922 6.81J 6.82J CD-4 Rep 3-May-11 124,000 9,700 `206 0.9JB 17.6 0.62J 8.39J 2.72JB CD-4 Rep (dup)3-May-11 0.21J 206 17.9 0.68J 8.98J 0.17J 2.85J CD-4 Rep 8-Nov-11 0.14J 191 0.93J 18.2 1.00J 8.86J 9.44J CD-4 Rep 9-May-12 184 1.69J 18.1 1.70J 0.17J 11.3J 3.03J 16.1B CD-4 Rep 29-Nov-12 172 13.7 0.62J 7.03J 2.84J 2.14JB CD-4 Rep 10-May-13 75.5J 0.5J 2.71J 7.87J 1.94J 0.88J 11.2J 11.1J 10.3 CD-4 Rep 7-Nov-13 1.36J 60.4J 0.35J 0.07J 0.77J 5.31J 1.83J 0.57J 5.11J 0.13J 32 4.40JB CD-4 Rep 7-May-14 62.4J 0.31J 0.05J 3.25JB 5.02J 1.70J 0.32J 6.52J 22.2J 2.97JB CD-4 Rep 5-Nov-14 70.0J 0.31J 2.59J 1.46J 0.72J 4.29J 14.8JB 6.85J CD-4 Rep 6-May-15 58.4J 0.39J 1.13J 5.94J 1.90J 0.53J 4.72J 14.0J 2.99J CD-4 Rep 27-Oct-15 0.79J 57.9J 0.32J 2.18J 5.86J 8.95J 1.26J 10.7J 4.14CN,J 13.9J 8.34B-01,J CD-4 Rep 18-May-16 1.09J 56.2J 0.46J 1.24J 7.31J 1.02J 0.66J 5.43J 18.0J 3.70J CD-4 Rep 2-Nov-16 46.3J 0.27J 1.35J 1.59J 1.18J 0.90J 4.18J 1.11J 18.1J 8.81J CD-7 1-Jul-14 66,000 7,600 15,000J 420,000 53.1J 0.131J 669 8.74J 4.11J 4.06J CD-7 5-Nov-14 77,000 8,500 18,000J 1,170,000 1.32J 118 3.74 15.1B 3.71J 40.0 13.6 21,100B 341 (1)8.91J 0.24J 75.8 19.4B CD-7 6-May-15 86,000 9,800 25,000J 660,000 1.71J 66.8J 0.28J 0.45J 4.36J 0.86J 1,630B 43.4 3.36J 4.14J 3.33J CD-7 27-Oct-15 81,000 11,000 28,000J 291,000 87.2J 1.12 5.33B-01,J 1.52J 16.6 4.69J 6,560 145 0.138J 6.61J 3.81CN,J 23.4J 11.3 CD-7 18-May-16 90,000 10,000 29,000J 282,000 74.8J 0.43J 2.18J 0.36J 4.74J 1.20J 2,160 59.4 0.164J 4.90J 10.2J 4.03J CD-7 1-Nov-16 100,000 13,000 34,000 413,000 82.6J 0.28J 1.21J 3.45J 1.06J 1,200 170 5.58J 4.98J 1302-CDLF-2006 1302-CDLF-2006 1302-CDLF-2006 Page 2 of 6 January 2017 Table 3a Detected Groundwater Constituents - General Chemistry and Metals November 2016 Semi-Annual Sampling Event Cabarrus County C&D Landfill Facility Permit Number 1302-CDLF-2006 Al k a l i n i t y Ch e m i c a l O x y g e n D e m a n d Ch l o r i d e Fe r r o u s I r o n Nit r a t e Su l f a t e To t a l D i s s o l v e d S o l i d s An t i m o n y Ar s e n i c Ba r i u m Be r y l l i u m Ca d m i u m Ch r o m i u m Co b a l t Co p p e r Le a d Ir o n Ma n g a n e s e Me r c u r y Ni c k e l Se l e n i u m Sil v e r Th a l l i u m Va n a d i u m Zin c NE NE 250,000 NE 10,000 250,000 500,000 1*10 700 4*2 10 1*1,000 15 300 50 1 100 20 20 0.2*0.3*1,000 NE NE NE NE 10,000 250,000 NE 6 10 100 1 1 10 10 10 10 300 50 0.2 50 10 10 5.5 25 10 1302-CDLF-2006 North Carolina 2L or Groundwater Protection Standard Solid Waste Section Limit MetalsGeneral Chemistry Sa m p l e D a t e Mo n i t o r i n g W e l l C o d e Fa c i l i t y P e r m i t N u m b e r CD-8 1-Jul-14 75,000 3,900 3,700J 120,000 0.256J 421 0.191J 14.4 12.6 78 6.55J 26,600 1,360 13.8J 0.238J 93.3 79.6 CD-8 5-Nov-14 86,000 3,500 253,000 83.4J 1.64JB 1.20J 7.15J 0.59J 2,360B 131 (1)3.34J 8.18J 11.0B CD-8 6-May-15 57,000 3,300 <5000 138,000 0.36J 53.8JB 0.48J 4.13J 0.27J 1,030 58.5 0.095JB 2.43J 4.03J 9.73JB CD-8 27-Oct-15 72,000 3,600 1,100J 132,000 0.75J 1.79J 162 0.32J 0.21J 5.88B-01,J 1.90J 38.6 2.29J 2,960 95.2 9.53J 3.65CN,J 11.2J 1,430 CD-8 (dup)27-Oct-15 70,000 3,500 130,000 0.40J 1.72J 160 0.33J 0.21J 5.54B-01,J 1.80J 36.3 2.12J 2,630 82.4 8.69J 4.20CN,J 10.6J 1,310 CD-8 19-May-16 115,000 2,000 <5,000 205,000 0.49J 1.52J 133 0.20J 3.54J 1.40J 28.1 1.28J 2,320 123 8.72J 13.2J 1,250 CD-8 (dup)19-May-16 110,000 2,000 <5,000 215,000 1.27J 1.55J 136 0.23J 0.10J 4.41J 1.63J 31.2 1.87J 3,230 129 9.76J 14.8J 1,600 CD-8 1-Nov-16 90,000 3,400 <5,000 517,000H-02 94.6J 0.17J 2.27J 2.52J 15.6 1.06J 3,350 433 3.96J 18.1J 244 CD-8 (dup)1-Nov-16 80,000 3,500 2,100J 428,000H-02 96.7J 0.21J 3.11J 2.47J 18.8 1.18J 4,640 412 4.09J 22.2J 247 Notes: 1. All units are in micrograms per liter (parts per billion). 2. * - Groundwater Protection Standard 3. NE - Standard Not Established; dup - Duplicate Sample 4. J - Indicates the analytical result is an estimated concentration between the method detection limit and the Solid Waste Section Reporting Limit. 6. CN - Detected silver concentrations were determined to be the result of contamination from the preservative acid used. 7. H-02 - Analysis was completed outside of hold time. 8. CD-4 Rep was installed as part of the proposed Phase 1 C&D Landfill expansion in January 2009. Beginning November 2011 samples collected from CD-4 Rep are only analyzed for Appendix I metals. 9. Alkalinity, chloride, ferrous iron, sulfate, and total dissolved solids were added to the sampling program in May 2010. 10. (1) - Not analyzed due to laboratory oversight. 11. CD-3 was relocated on July 1, 2014, as part of the Phase 2 C&D Landfill expansion. 12. CD-7 and -8 (formerly piezometers B-7 and -19) were added to the monitoring program in July 2014 as part of the Phase 2 C&D Landfill expansion. 13. Ferrous iron results for CD-1s and -1d are based on field testing and results for CD-4 Rep are laboratory derived. - Concentration exceeds the 15A NCAC 02L .0202 or Groundwater Protection Standard - Indicates the result is below the detection limit or not analyzed. 1302-CDLF-2006 5. B, B-01 - The analyte concentration detected in the method blank was greater than the method detection limit. Page 3 of 6 January 2017 Table 3b Detected Groundwater Constituents - Volatile Organic Compounds November 2016 Semi-Annual Sampling Event Cabarrus County C&D Landfill Facility Permit Number 1302-CDLF-2006 Fa c i l i t y P e r m i t N u m b e r Mo n i t o r i n g W e l l C o d e Sa m p l e D a t e 2- B u t a n o n e Ch l o r o b e n z e n e 1, 4 - D i c h l o r o b e n z e n e 1, 1 - D i c h l o r o e t h a n e 1, 1 - D i c h l o r o e t h e n e ci s - 1 , 2 - D i c h l o r o e t h e n e Me t h y l e n e C h l o r i d e To l u e n e Tr i c h l o r o f l u o r o m e t h a n e Ch l o r o m e t h a n e Te t r a c h l o r o e t h e n e Tr i c h l o r o e t h e n e Te t r a h y d r o f u r a n 4,000 50 6 6 7 70 5 600 2,000 3 0.7 3 NE 100 3 1 5 5 5 1 1 1 1 1 1 NE CD-1s 3-May-11 CD-1s 8-Nov-11 CD-1s 7-May-12 CD-1s 27-Nov-12 0.4J 0.2J CD-1s 7-May-13 CD-1s 5-Nov-13 CD-1s 6-May-14 CD-1s 4-Nov-14 CD-1s 5-May-15 CD-1s 27-Oct-15 CD-1s 17-May-16 CD-1s 1-Nov-16 CD-1d 3-May-11 CD-1d 8-Nov-11 CD-1d 7-May-12 CD-1d 27-Nov-12 CD-1d 7-May-13 CD-1d 5-Nov-13 CD-1d 6-May-14 CD-1d 4-Nov-14 CD-1d 5-May-15 CD-1d 27-Oct-15 CD-1d 17-May-16 CD-1d 1-Nov-16 CD-2 3-May-11 CD-2 8-Nov-11 CD-2 7-May-12 CD-2 27-Nov-12 0.4J CD-2 7-May-13 CD-2 5-Nov-13 CD-2 6-May-14 CD-2 4-Nov-14 CD-2 7-May-15 CD-2 27-Oct-15 CD-2 17-May-16 CD-2 1-Nov-16 CD-3 3-May-11 CD-3 8-Nov-11 16J CD-3 7-May-12 CD-3 27-Nov-12 0.4J CD-3 7-May-13 CD-3 5-Nov-13 CD-3 6-May-14 CD-3 4-Nov-14 CD-3 6-May-15 2.4 CD-3 27-Oct-15 1.6 CD-3 17-May-16 0.6J 2.1 CD-3 1-Nov-16 0.6J 5.9 1302-CDLF-2006 North Carolina 2L Standard Solid Waste Section Limit 1302-CDLF-2006 1302-CDLF-2006 1302-CDLF-2006 Page 4 of 6 January 2017 Table 3b Detected Groundwater Constituents - Volatile Organic Compounds November 2016 Semi-Annual Sampling Event Cabarrus County C&D Landfill Facility Permit Number 1302-CDLF-2006 Fa c i l i t y P e r m i t N u m b e r Mo n i t o r i n g W e l l C o d e Sa m p l e D a t e 2- B u t a n o n e Ch l o r o b e n z e n e 1, 4 - D i c h l o r o b e n z e n e 1, 1 - D i c h l o r o e t h a n e 1, 1 - D i c h l o r o e t h e n e ci s - 1 , 2 - D i c h l o r o e t h e n e Me t h y l e n e C h l o r i d e To l u e n e Tr i c h l o r o f l u o r o m e t h a n e Ch l o r o m e t h a n e Te t r a c h l o r o e t h e n e Tr i c h l o r o e t h e n e Te t r a h y d r o f u r a n 4,000 50 6 6 7 70 5 600 2,000 3 0.7 3 NE 100 3 1 5 5 5 1 1 1 1 1 1 NE 1302-CDLF-2006 North Carolina 2L Standard Solid Waste Section Limit CD-4 Rep 3-May-11 CD-4 Rep (dup)3-May-11 CD-4 Rep 8-Nov-11 CD-4 Rep 8-May-12 CD-4 Rep 28-Nov-12 0.3J CD-4 Rep 9-May-13 CD-4 Rep 7-Nov-13 0.6J CD-4 Rep 6-May-14 CD-4 Rep 4-Nov-14 CD-4 Rep 6-May-15 CD-4 Rep 27-Oct-15 CD-4 Rep 17-May-16 CD-4 Rep 2-Nov-16 CD-7 (B-7)22-Mar-12 CD-7 (B-7)3-May-12 0.65J 0.67J CD-7 1-Jul-14 CD-7 4-Nov-14 CD-7 6-May-15 0.4J CD-7 27-Oct-15 0.4J 0.5J CD-7 17-May-16 0.7J 1.0J 1.9 CD-7 1-Nov-16 1.2J 1.7J 5.8 CD-8 (B-19)22-Jan-09 0.22J 3.34J 2.84J 0.89J 1.21 2.2 1.21 CD-8 (B-19)22-Mar-12 1.13 2.24 1.03 CD-8 (B-19)3-May-12 0.18J 0.80J 1.51 0.90J CD-8 1-Jul-14 3.2J 0.57J 1.5 0.45J CD-8 4-Nov-14 0.8J CD-8 6-May-15 0.5J CD-8 27-Oct-15 0.6J CD-8 (dup)27-Oct-15 0.5J CD-8 18-May-16 CD-8 (dup)18-May-16 CD-8 1-Nov-16 CD-8 (dup)1-Nov-16 Notes: 1. All units are in micrograms per liter (parts per billion). 2. dup - Duplicate Sample 3. J - Indicates the analytical result is an estimated concentration between the method detection limit and the Solid Waste Section Reporting Limit. 5. NE - Standard Not Established 7. CD-3 was relocated on July 1, 2014, as part of the Phase 2 C&D Landfill expansion. 8. CD-7 and -8 (formerly piezometers B-7 and -19) were added to the monitoring program in July 2014 as part of the Phase 2 C&D Landfill expansion. - Concentration exceeds the 15A NCAC 02L .0202 or Groundwater Protection Standard - Indicates the result is below the detection limit. 1302-CDLF-2006 1302-CDLF-2006 6. CD-4 Rep was installed as part of the proposed Phase 1 C&D Landfill expansion in January 4. B - The analyte concentration detected in the method blank was greater than the method 1302-CDLF-2006 Page 5 of 6 January 2017 Table 3c Detected Surface Water Constituents - Metals, Volatile Organic Compounds, and General Chemistry November 2016 Semi-Annual Sampling Event Cabarrus County C&D Landfill Facility Permit Number 1302-CDLF-2006 An t i m o n y Ar s e n i c Ba r i u m Be r y l l i u m Ca d m i u m Ch r o m i u m Co b a l t Co p p e r Ir o n Le a d Ma n g a n e s e Me r c u r y Ni c k e l Se l e n i u m Si l v e r Th a l l i u m Va n a d i u m Zi n c Ac e t o n e Be n z e n e Ch l o r o b e n z e n e 1, 4 - D i c h l o r o b e n z e n e Te t r a h y d r o f u r a n Al k a l i n i t y Ch l o r i d e Su l f a t e To t a l D i s s o l v e d S o l i d s 640*10*200,000*6.5**0.15**24**4*2.7**NS 0.54**NS 0.012**16**5**0.06**0.47*NS 36**2,000**51*140**100**NS NS 230**NS NS 6 10 100 1 1 10 10 10 300 10 50 0.2 50 10 10 5.5 25 10 100 1 3 1 NE 1 NE 250 NE SW-3 9-Nov-11 SW-3 9-May-12 SW-3 29-Nov-12 SW-3 10-May-13 0.27J 152 2.23J 3.07J 4.30J 996 0.49J 887B 4.68J 0.10J 3.01J 33.4 60 20 240J 482 SW-3 5-Nov-13 SW-3 6-May-14 7.70J 301 2.41 0.22J 30.1B 58.3 39.9 67,600B 21.4B 9,250 29.4J 3.71J 0.23J 101 354 22J 8.5J 530 71 440 1,430 SW-3 4-Nov-14 SW-3 5-May-15 SW-3 27-Oct-15 SW-3 19-May-16 11.1 200 5.95 38.1 17.1 22.4 59,700 48.1 576 15.5J 18.0 0.31J 180 85.3 5.6J 25 3.2 47J 908H-02 SW-3 3-Nov-16 Notes: 1. Metal and volatile organic compound concentrations are in micrograms per liter (parts per billion). 2. General chemistry concentrations are in milligrams per liter (parts per million). 3. Standards obtained from section 15A NCAC 02B .0211 (North Carolina 2B) Surface Water Standards for Class C Waters (June 2016). 4. * - Human Health Standard 5. ** - Freshwater Aquatic Life 6. NS - No Standard; NE - Not Established 7. J - Indicates the analytical result is an estimated concentration between the method detection limit and the Solid Waste Section Reporting Limit. - Concentration exceeds the North Carolina 2B Human Health or Freshwater Aquatic Life Standard for Class C Waters. - Indicates the result is below the detection limit. 9. H-02 - Total dissolved solids analysis was analyzed outside of hold time for SW-3. DRY 1302-CDLF-2006 DRY DRY DRY DRY DRY 8. B - The analyte concentration detected in the method blank was greater than the method detection limit. DRY Solid Waste Section Limit DRY DRY DRYDRY DRY General ChemistryMetalsVolatile Organic Compounds DRYDRY DRY DRY DRY DRY Facility Permit Number Surface Water Code Sample Date DRY North Carolina 2B Human Health or Freshwater Aquatic Life Standard DRY DRY DRY DRY DRY Page 6 of 6 January 2017         Appendix A  P AC E AN A L YT I C A L S E R VI C E S , I N C . En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h Pr o j e c t : C a b a r r u s C o - C & D Ra l e i g h , N C 2 7 6 1 2 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 M r . M a t C o l o n e W e a p p r e c i a t e t h e o p p o r t u n i t y t o p r o v i d e t h e a n a l y t i c a l s u p p o r t f o r y o u r p r o j e c t . T h e a n a l y t i c a l r e s u l t s i n t h i s r e p o r t a r e b a s e d u p o n i n f o r m a t i o n s u p p l i e d b y y o u , t h e cl i e n t , a n d a r e f o r y o u r e x c l u s i v e u s e . I f y o u h a v e a n y q u e s t i o n s r e g a r d i n g t h i s d a t a p a c k a g e , p l e a s e d o n o t h e s i t a t e t o c a l l . Pa c e An a l y t i c a l S e r v i c e s , Inc. certifies that th e f o l l o w i n g a n a l y t i c a l r e s u l t s m e e t a l l r e q u i r e m e n t s o f t h e N a t i o n a l E n v i r o n m e n t a l L a b o r a t o r y Ac c r e d i t a t i o n C o n f e r e n c e (N E L A C ) . A l l t e s t r e s u l t s r e l a t e o n l y t o t h e sa m p l e s a n a l y z e d . La b o r a t o r y R e p o r t Pr o j e c t # : [ n o n e ] Pr e p a r e d F o r : At t e n t i o n : No v e m b e r 3 0 , 2 0 1 6 Re p o r t N u m b e r : AZ K 0 1 2 0 Ap p r o v e d : Th i s r e p o r t m a y n o t b e r e p r o d u c e d , e x c e p t i n f u l l , wi t h o u t w r i t t e n a p p r o v a l f r o m P a c e An a l y t i c a l S e r v i c e s , I n c . Page 1 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Sa m p l e I D La b o r a t o r y I D Ma t r i x Da t e S a m p l e d AN A L YT I C A L R E P O R T F O R S A M P L E S Date Received 13 0 2 - C D 1 S AZ K 0 1 2 0 - 0 1 1 1/ 0 1 / 1 6 0 9 : 1 3 1 1/03/16 09:35 Gr o u n d W at e r 13 0 2 - C D 1 D AZ K 0 1 2 0 - 0 2 1 1/ 0 1 / 1 6 1 0 : 0 3 1 1/03/16 09:35 Gr o u n d W at e r 13 0 2 - C D 2 AZ K 0 1 2 0 - 0 3 1 1/ 0 1 / 1 6 0 8 : 4 9 1 1/03/16 09:35 Gr o u n d W at e r 13 0 2 - C D 2 AZ K 0 1 2 0 - 0 4 1 1/ 0 2 / 1 6 0 8 : 1 5 1 1/03/16 09:35 Gr o u n d W at e r 13 0 2 - C D 3 AZ K 0 1 2 0 - 0 5 1 1/ 0 1 / 1 6 0 9 : 4 5 1 1/03/16 09:35 Gr o u n d W at e r 13 0 2 - C D 3 AZ K 0 1 2 0 - 0 6 1 1/ 0 2 / 1 6 0 8 : 4 5 1 1/03/16 09:35 Gr o u n d W at e r 13 0 2 - C D 7 AZ K 0 1 2 0 - 0 7 1 1/ 0 1 / 1 6 1 0 : 2 2 1 1/03/16 09:35 Gr o u n d W at e r 13 0 2 - C D 7 AZ K 0 1 2 0 - 0 8 1 1/ 0 2 / 1 6 0 9 : 0 0 1 1/03/16 09:35 Gr o u n d W at e r 13 0 2 - C D 8 AZ K 0 1 2 0 - 0 9 1 1/ 0 1 / 1 6 1 0 : 5 2 1 1/03/16 09:35 Gr o u n d W at e r 13 0 2 - C D 8 AZ K 0 1 2 0 - 1 0 1 1/ 0 2 / 1 6 0 9 : 3 0 1 1/03/16 09:35 Gr o u n d W at e r 13 0 2 - D u p l i c a t e AZ K 0 1 2 0 - 11 1 1/ 0 1 / 1 6 0 0 : 0 0 1 1/03/16 09:35 Gr o u n d W at e r 13 0 2 - D u p l i c a t e AZ K 0 1 2 0 - 1 2 1 1/ 0 2 / 1 6 0 0 : 0 0 1 1/03/16 09:35 Gr o u n d W at e r 13 0 2 - T rip B l a n k AZ K 0 1 2 0 - 1 3 1 1/ 0 1 / 1 6 0 0 : 0 0 1 1/03/16 17:30 W at e r 13 0 2 - C D 1 S AZ K 0 1 2 0 - 1 4 1 1/ 0 3 / 1 6 1 3 : 0 7 1 1/03/16 09:35 Gr o u n d W at e r Page 2 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Io n C h r o m a t o g r a p h An a l y s i s v i a E P A 90 5 6 A (H - 0 2 Q u a l i f i e r ) : Or i g i n a l a n a l y s i s f o r s a m p l e AZ K 01 2 0 - 0 1 ( C D - 1 S ) f o r N i t r a t e w a s p r e p a r e d w i t h i n t h e 4 8 - h o u r m e t h o d - s p e c i f i e d h o l d i n g t i m e . H o w e v e r , t h e a n a l y t i c a l in s t r u m e n t m a l f u n c t i o n e d , a n d a n a l y s i s c o u l d n o t b e c o m p l e t e d w i t h i n t h e h o l d i n g t i m e . T ot a l D i s s o l v e d S o l i d s An a l y s i s v i a S M 25 4 0 C ( H - 0 2 Q u a l i f i e r ) : Or i g i n a l a n a l y s i s f o r s a m p l e s AZ K 01 2 0 - 0 3 ( C D - 2 ) , A Z K 0 1 2 0 - 0 9 ( C D - 8 ) , an d AZ K 01 2 0 - 1 1 (D u p l i c a t e ) f o r T D S w a s p r e p a r e d w i t h i n t h e 7 - d a y me t h o d - s p e c i f i e d h o l d i n g t i m e . H o w e v e r , r e a n a l y s i s w a s r e q u i r e d , a n d t h e r e a n a l y s i s c o u l d n o t b e c o m p l e t e d w i t h i n t h e h o l d i n g t i m e . Ca s e N a r r a t i v e Page 3 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 1 S Gr o u n d W at e r AZ K 0 1 2 0 - 0 1 AZK0120 1 1/ 0 1 / 1 6 0 9 : 1 3 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 On S i t e EP A 9 0 5 0 A 11 3 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/01/16 09:13 1 1/ 0 1 / 1 6 0 9 : 1 3 SM 4 5 0 0 - O G 44 9 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/01/16 09:13 1 1/ 0 1 / 1 6 0 9 : 1 3 ND NA ug / L 1 Fi e l d - F e r r o u s I r o n 20 0 61 10187 NA 20 0 FE 2 1 1/01/16 09:13 1 1/ 0 1 / 1 6 0 9 : 1 3 EP A 9 0 4 0 C 5. 0 5 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/01/16 09:13 1 1/ 0 1 / 1 6 0 9 : 1 3 NA 36 0 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/01/16 09:13 1 1/ 0 1 / 1 6 0 9 : 1 3 SM 2 5 5 0 B 16 . 1 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/01/16 09:13 1 1/ 0 1 / 1 6 0 9 : 1 3 EP A 1 8 0 . 1 5. 7 2 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/01/16 09:13 1 1/ 0 1 / 1 6 0 9 : 1 3 NA 25 . 2 3 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/01/16 09:13 1 1/ 0 1 / 1 6 0 9 : 1 3 Ge n e r a l C h e m i s t r y SM 2 3 2 0 B 46 0 0 0 ug / L 1 Alk a l i n i t y a s C a C O 3 10 0 0 61 10164 SM 2 3 2 0 B 10 0 0 AL K 1 1/07/16 10:00 1 1/ 0 7 / 1 6 1 0 : 0 0 SM 5 2 2 0 D 26 5 0 0 ug / L 1 Ch e m i c a l O x y g e n D e m a n d 10 0 0 0 61 10153 EP A 4 1 0 . 4 10 0 0 0 E- 1 0 11 7 1 1/05/16 14:30 1 1/ 0 5 / 1 6 1 2 : 1 5 ND SM 4 5 0 0 - S D ug / L 1 T ot a l S u l f i d e 20 0 61 10191 SM 4 5 0 0 - S D 20 0 18 4 9 6 - 2 5 - 8 1 1/08/16 10:00 1 1/ 0 8 / 1 6 1 0 : 0 0 SM 2 5 4 0 C 71 0 0 0 ug / L 1 T ot a l D i s s o l v e d S o l i d s 10 0 0 0 61 10128 SM 2 5 4 0 C 10 0 0 0 E- 1 0 1 7 3 1 1/04/16 18:35 1 1/ 0 4 / 1 6 1 8 : 3 5 ND EP A 9 0 6 0 A ug / L 1 T ot a l O r g a n i c C a r b o n 10 0 0 61 10154 EP A 9 0 6 0 A 10 0 0 E- 1 0 1 9 5 1 1/08/16 17:56 1 1/ 0 8 / 1 6 1 3 : 0 0 In o r g a n i c An i o n s EP A 9 0 5 6 A 42 0 0 ug / L 1 Ch l o r i d e 10 0 0 61 10305 EP A 9 0 5 6 A 10 0 0 16 8 8 7 - 0 0 - 6 1 1/07/16 14:40 1 1/ 0 7 / 1 6 1 4 : 4 0 EP A 9 0 5 6 A 67 ug / L 1 Ni t r a t e a s N 50 H- 0 2 61 10305 EP A 9 0 5 6 A 50 14 7 9 7 - 5 5 - 8 1 1/07/16 14:40 1 1/ 0 7 / 1 6 1 4 : 4 0 ND EP A 9 0 5 6 A ug / L 1 Su l f a t e 50 0 0 61 10305 EP A 9 0 5 6 A 50 0 0 14 8 0 8 - 7 9 - 8 1 1/07/16 14:40 1 1/ 0 7 / 1 6 1 4 : 4 0 Me t a l s , T ot a l Page 4 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 1 S Gr o u n d W at e r AZ K 0 1 2 0 - 0 1 AZK0120 1 1/ 0 1 / 1 6 0 9 : 1 3 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10182 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 61 10182 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 30 . 5 ug / L 1 Ba r i u m 10 0 J 61 10182 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Be r y l l i u m 1. 0 0 61 10182 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 61 10182 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 2 3 ug / L 1 Ch r o m i u m 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 3 2 ug / L 1 Co b a l t 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 3 6 ug / L 1 Co p p e r 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 2 8 ug / L 1 Le a d 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 3 5 ug / L 1 Ni c k e l 50 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 61 10182 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10182 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10182 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 61 10182 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 4. 3 0 ug / L 1 Zi n c 10 . 0 J 61 10182 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 A 64 7 ug / L 1 Ir o n 40 . 0 61 10182 EP A 3 0 0 5 A 9. 5 74 3 9 - 8 9 - 6 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 A 70 . 8 ug / L 1 Ma n g a n e s e 10 . 0 61 10182 EP A 3 0 0 5 A 1. 0 74 3 9 - 9 6 - 5 1 1/16/16 18:48 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 7 4 7 0 A ug / L 1 Me r c u r y 0. 2 0 0 61 10101 EP A 7 4 7 0 A 0. 0 4 1 74 3 9 - 9 7 - 6 1 1/04/16 13:21 1 1/ 0 4 / 1 6 0 8 : 4 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 10166 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 5 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 1 S Gr o u n d W at e r AZ K 0 1 2 0 - 0 1 AZK0120 1 1/ 0 1 / 1 6 0 9 : 1 3 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 10166 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 10166 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 10166 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 10166 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 10166 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 10166 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 6 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 1 S Gr o u n d W at e r AZ K 0 1 2 0 - 0 1 AZK0120 1 1/ 0 1 / 1 6 0 9 : 1 3 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 10166 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 10166 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 10166 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 10166 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 7 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 1 S Gr o u n d W at e r AZ K 0 1 2 0 - 0 1 AZK0120 1 1/ 0 1 / 1 6 0 9 : 1 3 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a h y d r o f u r a n 10 61 10166 EP A 5 0 3 0 B 1. 5 10 9 - 9 9 - 9 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 99 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 10166 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 0 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 10166 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 91 % Su r r : T ol u e n e - d 8 61 10166 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 96 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 10166 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/07/16 10:16 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 Page 8 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 1 D Gr o u n d W at e r AZ K 0 1 2 0 - 0 2 AZK0120 1 1/ 0 1 / 1 6 1 0 : 0 3 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 On S i t e EP A 9 0 5 0 A 12 4 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/01/16 10:03 1 1/ 0 1 / 1 6 1 0 : 0 3 SM 4 5 0 0 - O G 31 0 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/01/16 10:03 1 1/ 0 1 / 1 6 1 0 : 0 3 EP A 9 0 4 0 C 5. 3 4 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/01/16 10:03 1 1/ 0 1 / 1 6 1 0 : 0 3 NA 33 0 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/01/16 10:03 1 1/ 0 1 / 1 6 1 0 : 0 3 SM 2 5 5 0 B 15 . 9 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/01/16 10:03 1 1/ 0 1 / 1 6 1 0 : 0 3 EP A 1 8 0 . 1 8. 2 7 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/01/16 10:03 1 1/ 0 1 / 1 6 1 0 : 0 3 NA 27 . 8 3 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/01/16 10:03 1 1/ 0 1 / 1 6 1 0 : 0 3 Ge n e r a l C h e m i s t r y SM 2 3 2 0 B 52 0 0 0 ug / L 1 Alk a l i n i t y a s C a C O 3 10 0 0 61 10164 SM 2 3 2 0 B 10 0 0 AL K 1 1/07/16 10:00 1 1/ 0 7 / 1 6 1 0 : 0 0 SM 2 5 4 0 C 99 0 0 0 ug / L 1 T ot a l D i s s o l v e d S o l i d s 10 0 0 0 61 10128 SM 2 5 4 0 C 10 0 0 0 E- 1 0 1 7 3 1 1/04/16 18:35 1 1/ 0 4 / 1 6 1 8 : 3 5 In o r g a n i c An i o n s EP A 9 0 5 6 A 34 0 0 ug / L 1 Ch l o r i d e 10 0 0 61 10305 EP A 9 0 5 6 A 10 0 0 16 8 8 7 - 0 0 - 6 1 1/07/16 15:00 1 1/ 0 7 / 1 6 1 5 : 0 0 ND EP A 9 0 5 6 A ug / L 1 Su l f a t e 50 0 0 61 10305 EP A 9 0 5 6 A 50 0 0 14 8 0 8 - 7 9 - 8 1 1/07/16 15:00 1 1/ 0 7 / 1 6 1 5 : 0 0 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10182 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 61 10182 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 32 . 6 ug / L 1 Ba r i u m 10 0 J 61 10182 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Be r y l l i u m 1. 0 0 61 10182 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 61 10182 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 Page 9 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 1 D Gr o u n d W at e r AZ K 0 1 2 0 - 0 2 AZK0120 1 1/ 0 1 / 1 6 1 0 : 0 3 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 Me t a l s , T ot a l EP A 6 0 2 0 B 1. 1 9 ug / L 1 Ch r o m i u m 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 7 7 ug / L 1 Co b a l t 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 2. 8 2 ug / L 1 Co p p e r 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 3 3 ug / L 1 Le a d 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 2 4 ug / L 1 Ni c k e l 50 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 61 10182 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10182 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10182 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 7. 9 6 ug / L 1 V an a d i u m 25 . 0 J 61 10182 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 4. 2 9 ug / L 1 Zi n c 10 . 0 J 61 10182 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 A 12 0 0 ug / L 1 Ir o n 40 . 0 61 10182 EP A 3 0 0 5 A 9. 5 74 3 9 - 8 9 - 6 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 A 31 . 3 ug / L 1 Ma n g a n e s e 10 . 0 61 10182 EP A 3 0 0 5 A 1. 0 74 3 9 - 9 6 - 5 1 1/16/16 18:54 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 7 4 7 0 A ug / L 1 Me r c u r y 0. 2 0 0 61 10101 EP A 7 4 7 0 A 0. 0 4 1 74 3 9 - 9 7 - 6 1 1/04/16 13:24 1 1/ 0 4 / 1 6 0 8 : 4 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 10166 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 10166 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 10166 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 10166 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 10 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 1 D Gr o u n d W at e r AZ K 0 1 2 0 - 0 2 AZK0120 1 1/ 0 1 / 1 6 1 0 : 0 3 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 10166 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 10166 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 10166 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 10166 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 11 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 1 D Gr o u n d W at e r AZ K 0 1 2 0 - 0 2 AZK0120 1 1/ 0 1 / 1 6 1 0 : 0 3 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 10166 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 10166 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 10166 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 10166 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a h y d r o f u r a n 10 61 10166 EP A 5 0 3 0 B 1. 5 10 9 - 9 9 - 9 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 98 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 10166 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 0 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 10166 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 78 - 1 2 0 Page 12 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 1 D Gr o u n d W at e r AZ K 0 1 2 0 - 0 2 AZK0120 1 1/ 0 1 / 1 6 1 0 : 0 3 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 EP A 8 2 6 0 B 91 % Su r r : T ol u e n e - d 8 61 10166 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 94 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 10166 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/07/16 10:43 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 Page 13 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 2 Gr o u n d W at e r AZ K 0 1 2 0 - 0 3 AZK0120 1 1/ 0 1 / 1 6 0 8 : 4 9 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 On S i t e EP A 9 0 5 0 A 10 3 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/01/16 08:49 1 1/ 0 1 / 1 6 0 8 : 4 9 SM 4 5 0 0 - O G 24 8 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/01/16 08:49 1 1/ 0 1 / 1 6 0 8 : 4 9 EP A 9 0 4 0 C 4. 5 9 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/01/16 08:49 1 1/ 0 1 / 1 6 0 8 : 4 9 NA 18 4 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/01/16 08:49 1 1/ 0 1 / 1 6 0 8 : 4 9 SM 2 5 5 0 B 17 . 0 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/01/16 08:49 1 1/ 0 1 / 1 6 0 8 : 4 9 EP A 1 8 0 . 1 80 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 > 61 10187 NA 0. 1 0 TU R B 1 1/01/16 08:49 1 1/ 0 1 / 1 6 0 8 : 4 9 NA 15 . 6 0 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/01/16 08:49 1 1/ 0 1 / 1 6 0 8 : 4 9 Ge n e r a l C h e m i s t r y SM 2 3 2 0 B 20 0 0 0 ug / L 1 Alk a l i n i t y a s C a C O 3 10 0 0 61 10164 SM 2 3 2 0 B 10 0 0 AL K 1 1/07/16 10:00 1 1/ 0 7 / 1 6 1 0 : 0 0 SM 2 5 4 0 C 85 0 0 0 0 ug / L 1 T ot a l D i s s o l v e d S o l i d s 10 0 0 0 0 H- 0 2 61 10327 SM 2 5 4 0 C 10 0 0 0 0 E- 1 0 1 7 3 1 1/1 1/16 14:10 1 1/ 1 1/16 14:10 In o r g a n i c An i o n s EP A 9 0 5 6 A 81 0 0 ug / L 1 Ch l o r i d e 10 0 0 61 10305 EP A 9 0 5 6 A 10 0 0 16 8 8 7 - 0 0 - 6 1 1/10/16 18:54 1 1/ 1 0 / 1 6 1 5 : 5 0 ND EP A 9 0 5 6 A ug / L 1 Su l f a t e 50 0 0 61 10305 EP A 9 0 5 6 A 50 0 0 14 8 0 8 - 7 9 - 8 1 1/10/16 18:54 1 1/ 1 0 / 1 6 1 5 : 5 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 10166 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 10166 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 10166 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 14 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 2 Gr o u n d W at e r AZ K 0 1 2 0 - 0 3 AZK0120 1 1/ 0 1 / 1 6 0 8 : 4 9 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 10166 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 10166 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 10166 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 10166 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 10166 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 15 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 2 Gr o u n d W at e r AZ K 0 1 2 0 - 0 3 AZK0120 1 1/ 0 1 / 1 6 0 8 : 4 9 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 10166 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 10166 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 10166 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 10166 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a h y d r o f u r a n 10 61 10166 EP A 5 0 3 0 B 1. 5 10 9 - 9 9 - 9 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 16 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 2 Gr o u n d W at e r AZ K 0 1 2 0 - 0 3 AZK0120 1 1/ 0 1 / 1 6 0 8 : 4 9 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 EP A 8 2 6 0 B 98 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 10166 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 1 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 10166 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 91 % Su r r : T ol u e n e - d 8 61 10166 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 94 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 10166 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/07/16 16:41 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 Page 17 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 2 Gr o u n d W at e r AZ K 0 1 2 0 - 0 4 AZK0120 1 1/ 0 2 / 1 6 0 8 : 1 5 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 On S i t e EP A 1 8 0 . 1 48 . 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/02/16 08:15 1 1/ 0 2 / 1 6 0 8 : 1 5 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10222 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/16/16 23:29 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 61 10222 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/16/16 23:29 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 64 . 5 ug / L 1 Ba r i u m 10 0 J 61 10222 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/16/16 23:29 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 0. 2 6 ug / L 1 Be r y l l i u m 1. 0 0 J 61 10222 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/18/16 18:28 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 61 10222 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/16/16 23:29 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 3. 1 0 ug / L 1 Ch r o m i u m 10 . 0 J 61 10222 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/16/16 23:29 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 4. 1 5 ug / L 1 Co b a l t 10 . 0 J 61 10222 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/16/16 23:29 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 5. 4 8 ug / L 1 Co p p e r 10 . 0 J 61 10222 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/16/16 23:29 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 2. 5 5 ug / L 1 Le a d 10 . 0 J 61 10222 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/16/16 23:29 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 3. 11 ug / L 1 Ni c k e l 50 . 0 J 61 10222 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/16/16 23:29 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 61 10222 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/16/16 23:29 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10222 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/16/16 23:29 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10222 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/16/16 23:29 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 15 . 3 ug / L 1 V an a d i u m 25 . 0 J 61 10222 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/16/16 23:29 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 13 . 9 ug / L 1 Zi n c 10 . 0 61 10222 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/16/16 23:29 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 A 40 1 0 ug / L 1 Ir o n 40 . 0 61 10222 EP A 3 0 0 5 A 9. 5 74 3 9 - 8 9 - 6 1 1/16/16 23:29 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 A 99 . 5 ug / L 1 Ma n g a n e s e 10 . 0 61 10222 EP A 3 0 0 5 A 1. 0 74 3 9 - 9 6 - 5 1 1/16/16 23:29 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 7 4 7 0 A 0. 0 5 6 ug / L 1 Me r c u r y 0. 2 0 0 J 61 10101 EP A 7 4 7 0 A 0. 0 4 1 74 3 9 - 9 7 - 6 1 1/04/16 14:56 1 1/ 0 4 / 1 6 0 8 : 4 0 Page 18 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 3 Gr o u n d W at e r AZ K 0 1 2 0 - 0 5 AZK0120 1 1/ 0 1 / 1 6 0 9 : 4 5 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 On S i t e EP A 9 0 5 0 A 48 4 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/01/16 09:45 1 1/ 0 1 / 1 6 0 9 : 4 5 SM 4 5 0 0 - O G 12 4 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/01/16 09:45 1 1/ 0 1 / 1 6 0 9 : 4 5 EP A 9 0 4 0 C 5. 3 3 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/01/16 09:45 1 1/ 0 1 / 1 6 0 9 : 4 5 NA 64 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/01/16 09:45 1 1/ 0 1 / 1 6 0 9 : 4 5 SM 2 5 5 0 B 16 . 5 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/01/16 09:45 1 1/ 0 1 / 1 6 0 9 : 4 5 EP A 1 8 0 . 1 80 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 > 61 10187 NA 0. 1 0 TU R B 1 1/01/16 09:45 1 1/ 0 1 / 1 6 0 9 : 4 5 NA 38 . 9 1 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/01/16 09:45 1 1/ 0 1 / 1 6 0 9 : 4 5 Ge n e r a l C h e m i s t r y SM 2 3 2 0 B 95 0 0 0 ug / L 1 Alk a l i n i t y a s C a C O 3 10 0 0 61 10164 SM 2 3 2 0 B 10 0 0 AL K 1 1/07/16 10:00 1 1/ 0 7 / 1 6 1 0 : 0 0 SM 2 5 4 0 C 16 2 0 0 0 ug / L 1 T ot a l D i s s o l v e d S o l i d s 20 0 0 0 61 10128 SM 2 5 4 0 C 20 0 0 0 E- 1 0 1 7 3 1 1/04/16 18:35 1 1/ 0 4 / 1 6 1 8 : 3 5 In o r g a n i c An i o n s EP A 9 0 5 6 A 14 0 0 0 ug / L 1 Ch l o r i d e 10 0 0 61 10305 EP A 9 0 5 6 A 10 0 0 16 8 8 7 - 0 0 - 6 1 1/10/16 19:15 1 1/ 1 0 / 1 6 1 5 : 5 0 EP A 9 0 5 6 A 27 0 0 0 ug / L 1 Su l f a t e 50 0 0 61 10305 EP A 9 0 5 6 A 50 0 0 14 8 0 8 - 7 9 - 8 1 1/10/16 19:15 1 1/ 1 0 / 1 6 1 5 : 5 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 10166 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 10166 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 10166 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 19 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 3 Gr o u n d W at e r AZ K 0 1 2 0 - 0 5 AZK0120 1 1/ 0 1 / 1 6 0 9 : 4 5 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 10166 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 10166 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 10166 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 10166 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 10166 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 20 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 3 Gr o u n d W at e r AZ K 0 1 2 0 - 0 5 AZK0120 1 1/ 0 1 / 1 6 0 9 : 4 5 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 10166 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 10166 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 10166 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 0. 6 ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 J 61 10166 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 10166 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 5. 9 ug / L 1 T et r a h y d r o f u r a n 10 J 61 10166 EP A 5 0 3 0 B 1. 5 10 9 - 9 9 - 9 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 21 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 3 Gr o u n d W at e r AZ K 0 1 2 0 - 0 5 AZK0120 1 1/ 0 1 / 1 6 0 9 : 4 5 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 EP A 8 2 6 0 B 98 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 10166 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 1 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 10166 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 91 % Su r r : T ol u e n e - d 8 61 10166 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 94 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 10166 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/07/16 18:04 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 Page 22 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 3 Gr o u n d W at e r AZ K 0 1 2 0 - 0 6 AZK0120 1 1/ 0 2 / 1 6 0 8 : 4 5 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 On S i t e EP A 1 8 0 . 1 13 . 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/02/16 08:45 1 1/ 0 2 / 1 6 0 8 : 4 5 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10222 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/16/16 23:34 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 61 10222 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/16/16 23:34 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 15 8 ug / L 1 Ba r i u m 10 0 61 10222 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/16/16 23:34 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 0. 1 3 ug / L 1 Be r y l l i u m 1. 0 0 J 61 10222 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/18/16 18:36 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 61 10222 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/16/16 23:34 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 6 0 2 0 B ug / L 1 Ch r o m i u m 10 . 0 61 10222 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/16/16 23:34 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 2. 0 7 ug / L 1 Co b a l t 10 . 0 J 61 10222 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/16/16 23:34 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 2. 7 7 ug / L 1 Co p p e r 10 . 0 J 61 10222 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/16/16 23:34 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 0. 4 9 ug / L 1 Le a d 10 . 0 J 61 10222 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/16/16 23:34 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 6. 8 1 ug / L 1 Ni c k e l 50 . 0 J 61 10222 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/16/16 23:34 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 61 10222 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/16/16 23:34 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10222 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/16/16 23:34 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10222 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/16/16 23:34 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 61 10222 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/16/16 23:34 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 6. 8 2 ug / L 1 Zi n c 10 . 0 J 61 10222 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/16/16 23:34 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 A 14 0 0 ug / L 1 Ir o n 40 . 0 61 10222 EP A 3 0 0 5 A 9. 5 74 3 9 - 8 9 - 6 1 1/16/16 23:34 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 A 92 2 ug / L 1 Ma n g a n e s e 10 . 0 61 10222 EP A 3 0 0 5 A 1. 0 74 3 9 - 9 6 - 5 1 1/16/16 23:34 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 7 4 7 0 A ug / L 1 Me r c u r y 0. 2 0 0 61 10101 EP A 7 4 7 0 A 0. 0 4 1 74 3 9 - 9 7 - 6 1 1/04/16 14:59 1 1/ 0 4 / 1 6 0 8 : 4 0 Page 23 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 7 Gr o u n d W at e r AZ K 0 1 2 0 - 0 7 AZK0120 1 1/ 0 1 / 1 6 1 0 : 2 2 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 On S i t e EP A 9 0 5 0 A 41 7 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/01/16 10:22 1 1/ 0 1 / 1 6 1 0 : 2 2 SM 4 5 0 0 - O G 18 8 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/01/16 10:22 1 1/ 0 1 / 1 6 1 0 : 2 2 EP A 9 0 4 0 C 5. 3 6 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/01/16 10:22 1 1/ 0 1 / 1 6 1 0 : 2 2 NA 11 8 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/01/16 10:22 1 1/ 0 1 / 1 6 1 0 : 2 2 SM 2 5 5 0 B 15 . 8 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/01/16 10:22 1 1/ 0 1 / 1 6 1 0 : 2 2 EP A 1 8 0 . 1 80 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 > 61 10187 NA 0. 1 0 TU R B 1 1/01/16 10:22 1 1/ 0 1 / 1 6 1 0 : 2 2 NA 40 . 2 7 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/01/16 10:22 1 1/ 0 1 / 1 6 1 0 : 2 2 Ge n e r a l C h e m i s t r y SM 2 3 2 0 B 10 0 0 0 0 ug / L 1 Alk a l i n i t y a s C a C O 3 10 0 0 61 10164 SM 2 3 2 0 B 10 0 0 AL K 1 1/07/16 10:00 1 1/ 0 7 / 1 6 1 0 : 0 0 SM 2 5 4 0 C 41 3 0 0 0 ug / L 1 T ot a l D i s s o l v e d S o l i d s 66 7 0 0 61 10128 SM 2 5 4 0 C 66 7 0 0 E- 1 0 1 7 3 1 1/04/16 18:35 1 1/ 0 4 / 1 6 1 8 : 3 5 In o r g a n i c An i o n s EP A 9 0 5 6 A 13 0 0 0 ug / L 1 Ch l o r i d e 10 0 0 61 10305 EP A 9 0 5 6 A 10 0 0 16 8 8 7 - 0 0 - 6 1 1/10/16 19:37 1 1/ 1 0 / 1 6 1 5 : 5 0 EP A 9 0 5 6 A 34 0 0 0 ug / L 1 Su l f a t e 50 0 0 61 10305 EP A 9 0 5 6 A 50 0 0 14 8 0 8 - 7 9 - 8 1 1/10/16 19:37 1 1/ 1 0 / 1 6 1 5 : 5 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 10166 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 10166 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 10166 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 24 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 7 Gr o u n d W at e r AZ K 0 1 2 0 - 0 7 AZK0120 1 1/ 0 1 / 1 6 1 0 : 2 2 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 10166 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 10166 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 10166 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 10166 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 10166 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 1. 2 ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 J 61 10166 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 1. 7 ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 J 61 10166 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 25 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 7 Gr o u n d W at e r AZ K 0 1 2 0 - 0 7 AZK0120 1 1/ 0 1 / 1 6 1 0 : 2 2 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 10166 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 10166 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 10166 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 10166 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 5. 8 ug / L 1 T et r a h y d r o f u r a n 10 J 61 10166 EP A 5 0 3 0 B 1. 5 10 9 - 9 9 - 9 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 26 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 7 Gr o u n d W at e r AZ K 0 1 2 0 - 0 7 AZK0120 1 1/ 0 1 / 1 6 1 0 : 2 2 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 EP A 8 2 6 0 B 98 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 10166 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 1 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 10166 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 92 % Su r r : T ol u e n e - d 8 61 10166 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 93 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 10166 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/07/16 18:31 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 Page 27 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 7 Gr o u n d W at e r AZ K 0 1 2 0 - 0 8 AZK0120 1 1/ 0 2 / 1 6 0 9 : 0 0 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 On S i t e EP A 1 8 0 . 1 7. 2 1 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/02/16 09:00 1 1/ 0 2 / 1 6 0 9 : 0 0 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10222 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/16/16 23:40 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 61 10222 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/16/16 23:40 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 82 . 6 ug / L 1 Ba r i u m 10 0 J 61 10222 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/16/16 23:40 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 0. 2 8 ug / L 1 Be r y l l i u m 1. 0 0 J 61 10222 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/18/16 19:03 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 61 10222 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/16/16 23:40 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 1. 2 1 ug / L 1 Ch r o m i u m 10 . 0 J 61 10222 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/16/16 23:40 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 6 0 2 0 B ug / L 1 Co b a l t 10 . 0 61 10222 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/16/16 23:40 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 3. 4 5 ug / L 1 Co p p e r 10 . 0 J 61 10222 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/16/16 23:40 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 1. 0 6 ug / L 1 Le a d 10 . 0 J 61 10222 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/16/16 23:40 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 5. 5 8 ug / L 1 Ni c k e l 50 . 0 J 61 10222 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/16/16 23:40 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 61 10222 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/16/16 23:40 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10222 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/16/16 23:40 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10222 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/16/16 23:40 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 6 0 2 0 B ug / L 1 V an a d i u m 25 . 0 61 10222 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/16/16 23:40 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 4. 9 8 ug / L 1 Zi n c 10 . 0 J 61 10222 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/16/16 23:40 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 A 12 0 0 ug / L 1 Ir o n 40 . 0 61 10222 EP A 3 0 0 5 A 9. 5 74 3 9 - 8 9 - 6 1 1/16/16 23:40 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 A 17 0 ug / L 1 Ma n g a n e s e 10 . 0 61 10222 EP A 3 0 0 5 A 1. 0 74 3 9 - 9 6 - 5 1 1/16/16 23:40 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 7 4 7 0 A ug / L 1 Me r c u r y 0. 2 0 0 61 10101 EP A 7 4 7 0 A 0. 0 4 1 74 3 9 - 9 7 - 6 1 1/04/16 15:01 1 1/ 0 4 / 1 6 0 8 : 4 0 Page 28 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 8 Gr o u n d W at e r AZ K 0 1 2 0 - 0 9 AZK0120 1 1/ 0 1 / 1 6 1 0 : 5 2 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 On S i t e EP A 9 0 5 0 A 24 6 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/01/16 10:52 1 1/ 0 1 / 1 6 1 0 : 5 2 SM 4 5 0 0 - O G 13 7 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/01/16 10:52 1 1/ 0 1 / 1 6 1 0 : 5 2 EP A 9 0 4 0 C 5. 7 6 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/01/16 10:52 1 1/ 0 1 / 1 6 1 0 : 5 2 NA 29 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/01/16 10:52 1 1/ 0 1 / 1 6 1 0 : 5 2 SM 2 5 5 0 B 17 . 0 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/01/16 10:52 1 1/ 0 1 / 1 6 1 0 : 5 2 EP A 1 8 0 . 1 80 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 > 61 10187 NA 0. 1 0 TU R B 1 1/01/16 10:52 1 1/ 0 1 / 1 6 1 0 : 5 2 NA 32 . 7 4 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/01/16 10:52 1 1/ 0 1 / 1 6 1 0 : 5 2 Ge n e r a l C h e m i s t r y SM 2 3 2 0 B 90 0 0 0 ug / L 1 Alk a l i n i t y a s C a C O 3 10 0 0 61 10164 SM 2 3 2 0 B 10 0 0 AL K 1 1/07/16 10:00 1 1/ 0 7 / 1 6 1 0 : 0 0 SM 2 5 4 0 C 51 7 0 0 0 ug / L 1 T ot a l D i s s o l v e d S o l i d s 33 3 0 0 H- 0 2 61 10327 SM 2 5 4 0 C 33 3 0 0 E- 1 0 1 7 3 1 1/1 1/16 14:10 1 1/ 1 1/16 14:10 In o r g a n i c An i o n s EP A 9 0 5 6 A 34 0 0 ug / L 1 Ch l o r i d e 10 0 0 61 10305 EP A 9 0 5 6 A 10 0 0 16 8 8 7 - 0 0 - 6 1 1/10/16 19:58 1 1/ 1 0 / 1 6 1 5 : 5 0 ND EP A 9 0 5 6 A ug / L 1 Su l f a t e 50 0 0 61 10305 EP A 9 0 5 6 A 50 0 0 14 8 0 8 - 7 9 - 8 1 1/10/16 19:58 1 1/ 1 0 / 1 6 1 5 : 5 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 10166 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 10166 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 10166 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 29 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 8 Gr o u n d W at e r AZ K 0 1 2 0 - 0 9 AZK0120 1 1/ 0 1 / 1 6 1 0 : 5 2 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 10166 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 10166 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 10166 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 10166 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 10166 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 30 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 8 Gr o u n d W at e r AZ K 0 1 2 0 - 0 9 AZK0120 1 1/ 0 1 / 1 6 1 0 : 5 2 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 10166 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 10166 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 10166 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 10166 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a h y d r o f u r a n 10 61 10166 EP A 5 0 3 0 B 1. 5 10 9 - 9 9 - 9 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 31 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 8 Gr o u n d W at e r AZ K 0 1 2 0 - 0 9 AZK0120 1 1/ 0 1 / 1 6 1 0 : 5 2 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 EP A 8 2 6 0 B 99 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 10166 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 1 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 10166 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 92 % Su r r : T ol u e n e - d 8 61 10166 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 94 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 10166 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/07/16 18:59 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 Page 32 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 8 Gr o u n d W at e r AZ K 0 1 2 0 - 1 0 AZK0120 1 1/ 0 2 / 1 6 0 9 : 3 0 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 On S i t e EP A 1 8 0 . 1 48 . 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/02/16 09:30 1 1/ 0 2 / 1 6 0 9 : 3 0 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10222 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/16/16 23:46 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 61 10222 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/16/16 23:46 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 94 . 6 ug / L 1 Ba r i u m 10 0 J 61 10222 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/16/16 23:46 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 0. 1 7 ug / L 1 Be r y l l i u m 1. 0 0 J 61 10222 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/18/16 19:10 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 61 10222 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/16/16 23:46 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 2. 2 7 ug / L 1 Ch r o m i u m 10 . 0 J 61 10222 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/16/16 23:46 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 2. 5 2 ug / L 1 Co b a l t 10 . 0 J 61 10222 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/16/16 23:46 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 15 . 6 ug / L 1 Co p p e r 10 . 0 61 10222 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/16/16 23:46 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 1. 0 6 ug / L 1 Le a d 10 . 0 J 61 10222 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/16/16 23:46 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 3. 9 6 ug / L 1 Ni c k e l 50 . 0 J 61 10222 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/16/16 23:46 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 61 10222 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/16/16 23:46 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10222 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/16/16 23:46 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10222 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/16/16 23:46 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 18 . 1 ug / L 1 V an a d i u m 25 . 0 J 61 10222 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/16/16 23:46 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 24 4 ug / L 1 Zi n c 10 . 0 61 10222 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/16/16 23:46 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 A 33 5 0 ug / L 1 Ir o n 40 . 0 61 10222 EP A 3 0 0 5 A 9. 5 74 3 9 - 8 9 - 6 1 1/16/16 23:46 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 A 43 3 ug / L 1 Ma n g a n e s e 10 . 0 61 10222 EP A 3 0 0 5 A 1. 0 74 3 9 - 9 6 - 5 1 1/16/16 23:46 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 7 4 7 0 A ug / L 1 Me r c u r y 0. 2 0 0 61 10101 EP A 7 4 7 0 A 0. 0 4 1 74 3 9 - 9 7 - 6 1 1/04/16 15:03 1 1/ 0 4 / 1 6 0 8 : 4 0 Page 33 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - D u p l i c a t e Gr o u n d W at e r AZ K 0 1 2 0 - 11 AZK0120 1 1/ 0 1 / 1 6 0 0 : 0 0 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 Ge n e r a l C h e m i s t r y SM 2 3 2 0 B 80 0 0 0 ug / L 1 Alk a l i n i t y a s C a C O 3 10 0 0 61 10164 SM 2 3 2 0 B 10 0 0 AL K 1 1/07/16 10:00 1 1/ 0 7 / 1 6 1 0 : 0 0 SM 2 5 4 0 C 42 8 0 0 0 ug / L 1 T ot a l D i s s o l v e d S o l i d s 40 0 0 0 H- 0 2 61 10327 SM 2 5 4 0 C 40 0 0 0 E- 1 0 1 7 3 1 1/1 1/16 14:10 1 1/ 1 1/16 14:10 In o r g a n i c An i o n s EP A 9 0 5 6 A 35 0 0 ug / L 1 Ch l o r i d e 10 0 0 61 10305 EP A 9 0 5 6 A 10 0 0 16 8 8 7 - 0 0 - 6 1 1/10/16 20:19 1 1/ 1 0 / 1 6 1 5 : 5 0 EP A 9 0 5 6 A 21 0 0 ug / L 1 Su l f a t e 50 0 0 J 61 10305 EP A 9 0 5 6 A 51 14 8 0 8 - 7 9 - 8 1 1/10/16 20:19 1 1/ 1 0 / 1 6 1 5 : 5 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 10166 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 10166 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 10166 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 10166 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 10166 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 10166 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 34 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - D u p l i c a t e Gr o u n d W at e r AZ K 0 1 2 0 - 11 AZK0120 1 1/ 0 1 / 1 6 0 0 : 0 0 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 10166 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 10166 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 10166 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 10166 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 10166 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 35 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - D u p l i c a t e Gr o u n d W at e r AZ K 0 1 2 0 - 11 AZK0120 1 1/ 0 1 / 1 6 0 0 : 0 0 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 10166 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a h y d r o f u r a n 10 61 10166 EP A 5 0 3 0 B 1. 5 10 9 - 9 9 - 9 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 98 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 10166 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 1 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 10166 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 93 % Su r r : T ol u e n e - d 8 61 10166 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 94 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 10166 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/07/16 19:26 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 Page 36 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - D u p l i c a t e Gr o u n d W at e r AZ K 0 1 2 0 - 1 2 AZK0120 1 1/ 0 2 / 1 6 0 0 : 0 0 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10222 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/16/16 23:52 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 61 10222 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/16/16 23:52 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 96 . 7 ug / L 1 Ba r i u m 10 0 J 61 10222 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/16/16 23:52 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 0. 2 1 ug / L 1 Be r y l l i u m 1. 0 0 J 61 10222 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/18/16 19:18 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 61 10222 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/16/16 23:52 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 3. 11 ug / L 1 Ch r o m i u m 10 . 0 J 61 10222 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/16/16 23:52 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 2. 4 7 ug / L 1 Co b a l t 10 . 0 J 61 10222 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/16/16 23:52 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 18 . 8 ug / L 1 Co p p e r 10 . 0 61 10222 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/16/16 23:52 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 1. 1 8 ug / L 1 Le a d 10 . 0 J 61 10222 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/16/16 23:52 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 4. 0 9 ug / L 1 Ni c k e l 50 . 0 J 61 10222 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/16/16 23:52 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 6 0 2 0 B ug / L 1 Se l e n i u m 10 . 0 61 10222 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/16/16 23:52 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10222 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/16/16 23:52 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10222 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/16/16 23:52 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 22 . 2 ug / L 1 V an a d i u m 25 . 0 J 61 10222 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/16/16 23:52 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 B 24 7 ug / L 1 Zi n c 10 . 0 61 10222 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/16/16 23:52 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 A 46 4 0 ug / L 1 Ir o n 40 . 0 61 10222 EP A 3 0 0 5 A 9. 5 74 3 9 - 8 9 - 6 1 1/16/16 23:52 1 1/ 0 9 / 1 6 1 0 : 5 0 EP A 6 0 2 0 A 41 2 ug / L 1 Ma n g a n e s e 10 . 0 61 10222 EP A 3 0 0 5 A 1. 0 74 3 9 - 9 6 - 5 1 1/16/16 23:52 1 1/ 0 9 / 1 6 1 0 : 5 0 ND EP A 7 4 7 0 A ug / L 1 Me r c u r y 0. 2 0 0 61 10101 EP A 7 4 7 0 A 0. 0 4 1 74 3 9 - 9 7 - 6 1 1/04/16 15:06 1 1/ 0 4 / 1 6 0 8 : 4 0 Page 37 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 4 R e p Gr o u n d W at e r AZ K 0 0 4 4 - 11 AZK0044 1 1/ 0 1 / 1 6 0 8 : 1 7 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 On S i t e EP A 9 0 5 0 A 20 9 um h o s / c m 1 Fi e l d - S p e c i f i c C o n d u c t a n c e 1 61 10187 NA 1 CO N D 1 1/01/16 08:17 1 1/ 0 1 / 1 6 0 8 : 1 7 SM 4 5 0 0 - O G 13 5 0 ug / L 1 Di s s o l v e d O x y g e n 0. 0 61 10187 NA 0. 0 NA 1 1/01/16 08:17 1 1/ 0 1 / 1 6 0 8 : 1 7 EP A 9 0 4 0 C 5. 2 8 pH U n i t s 1 Fi e l d - p H 61 10187 NA PH 1 1/01/16 08:17 1 1/ 0 1 / 1 6 0 8 : 1 7 NA 79 mV 1 Fi e l d - R e d o x 61 10187 NA RE D O X 1 1/01/16 08:17 1 1/ 0 1 / 1 6 0 8 : 1 7 SM 2 5 5 0 B 17 . 0 °C 1 Fi e l d - T em p e r a t u r e 61 10187 NA TE M P 1 1/01/16 08:17 1 1/ 0 1 / 1 6 0 8 : 1 7 EP A 1 8 0 . 1 80 0 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 > 61 10187 NA 0. 1 0 TU R B 1 1/01/16 08:17 1 1/ 0 1 / 1 6 0 8 : 1 7 NA 10 . 2 5 fe e t 1 Fi e l d - W at e r L e v e l 61 10187 NA WL 1 1/01/16 08:17 1 1/ 0 1 / 1 6 0 8 : 1 7 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 102 11 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 102 11 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 102 11 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 102 11 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 56 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 4 R e p Gr o u n d W at e r AZ K 0 0 4 4 - 11 AZK0044 1 1/ 0 1 / 1 6 0 8 : 1 7 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 102 11 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 102 11 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 102 11 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 102 11 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 102 11 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 Page 57 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 4 R e p Gr o u n d W at e r AZ K 0 0 4 4 - 11 AZK0044 1 1/ 0 1 / 1 6 0 8 : 1 7 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 102 11 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 102 11 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 102 11 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 102 11 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 EP A 8 2 6 0 B 98 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 102 11 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 1 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 102 11 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 93 % Su r r : T ol u e n e - d 8 61 102 11 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 93 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 102 11 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/08/16 20:47 1 1/ 0 8 / 1 6 1 0 : 0 0 80 - 1 2 0 Page 58 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 4 R e p Gr o u n d W at e r AZ K 0 0 4 4 - 1 2 AZK0044 1 1/ 0 2 / 1 6 0 8 : 1 0 Pr o j e c t : Ca b a r r u s C o - 2 & 3 1 1/ 0 3 / 1 6 0 9 : 3 5 On S i t e EP A 1 8 0 . 1 3. 2 1 NT U 1 Fi e l d - T ur b i d i t y 0. 1 0 61 10187 NA 0. 1 0 TU R B 1 1/02/16 08:10 1 1/ 0 2 / 1 6 0 8 : 1 0 Me t a l s , T ot a l ND EP A 6 0 2 0 B ug / L 1 An t i m o n y 6. 0 0 61 10182 EP A 3 0 0 5 A 0. 8 5 74 4 0 - 3 6 - 0 1 1/16/16 20:43 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ar s e n i c 10 . 0 61 10182 EP A 3 0 0 5 A 1. 6 4 74 4 0 - 3 8 - 2 1 1/29/16 13:33 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 46 . 3 ug / L 1 Ba r i u m 10 0 J 61 10182 EP A 3 0 0 5 A 0. 4 4 74 4 0 - 3 9 - 3 1 1/16/16 20:43 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 2 7 ug / L 1 Be r y l l i u m 1. 0 0 J 61 10182 EP A 3 0 0 5 A 0. 0 8 74 4 0 - 4 1 - 7 1 1/16/16 20:43 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Ca d m i u m 1. 0 0 61 10182 EP A 3 0 0 5 A 0. 0 7 74 4 0 - 4 3 - 9 1 1/16/16 20:43 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 3 5 ug / L 1 Ch r o m i u m 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 9 4 74 4 0 - 4 7 - 3 1 1/29/16 13:33 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 5 9 ug / L 1 Co b a l t 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 2 74 4 0 - 4 8 - 4 1 1/29/16 13:33 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 1 8 ug / L 1 Co p p e r 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 4 74 4 0 - 5 0 - 8 1 1/29/16 13:33 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 0. 9 0 ug / L 1 Le a d 10 . 0 J 61 10182 EP A 3 0 0 5 A 0. 1 2 74 3 9 - 9 2 - 1 1 1/16/16 20:43 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 4. 1 8 ug / L 1 Ni c k e l 50 . 0 J 61 10182 EP A 3 0 0 5 A 0. 5 5 74 4 0 - 0 2 - 0 1 1/29/16 13:33 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 1. 11 ug / L 1 Se l e n i u m 10 . 0 J 61 10182 EP A 3 0 0 5 A 1. 0 0 77 8 2 - 4 9 - 2 1 1/29/16 13:33 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Sil v e r 10 . 0 61 10182 EP A 3 0 0 5 A 0. 4 8 74 4 0 - 2 2 - 4 1 1/16/16 20:43 1 1/ 0 8 / 1 6 1 4 : 4 5 ND EP A 6 0 2 0 B ug / L 1 Th a l l i u m 5. 5 0 61 10182 EP A 3 0 0 5 A 0. 2 1 74 4 0 - 2 8 - 0 1 1/16/16 20:43 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 18 . 1 ug / L 1 V an a d i u m 25 . 0 J 61 10182 EP A 3 0 0 5 A 7. 1 4 74 4 0 - 6 2 - 2 1 1/29/16 13:33 1 1/ 0 8 / 1 6 1 4 : 4 5 EP A 6 0 2 0 B 8. 8 1 ug / L 1 Zi n c 10 . 0 J 61 10182 EP A 3 0 0 5 A 2. 1 0 74 4 0 - 6 6 - 6 1 1/29/16 13:33 1 1/ 0 8 / 1 6 1 4 : 4 5 Page 59 of 155 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - T ri p B l a n k W at e r AZ K 0 1 2 0 - 1 3 AZK0120 1 1/ 0 1 / 1 6 0 0 : 0 0 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 1 7 : 3 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 Ac e t o n e 10 0 61 10166 EP A 5 0 3 0 B 4. 9 67 - 6 4 - 1 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ac r y l o n i t r i l e 20 0 61 10166 EP A 5 0 3 0 B 1. 8 10 7 - 1 3 - 1 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Be n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 2 71 - 4 3 - 2 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o c h l o r o m e t h a n e 3. 0 61 10166 EP A 5 0 3 0 B 0. 7 74 - 9 7 - 5 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o d i c h l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 6 75 - 2 7 - 4 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o f o r m 3. 0 61 10166 EP A 5 0 3 0 B 0. 7 75 - 2 5 - 2 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Br o m o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 8 74 - 8 3 - 9 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n D i s u l f i d e 10 0 61 10166 EP A 5 0 3 0 B 0. 6 75 - 1 5 - 0 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ca r b o n T et r a c h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 6 56 - 2 3 - 5 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o b e n z e n e 3. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 8 - 9 0 - 7 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 4 75 - 0 0 - 3 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o f o r m 5. 0 61 10166 EP A 5 0 3 0 B 0. 3 67 - 6 6 - 3 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Ch l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 74 - 8 7 - 3 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o c h l o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 12 4 - 4 8 - 1 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e 13 61 10166 EP A 5 0 3 0 B 2. 0 96 - 1 2 - 8 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i b r o m o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 10 6 - 9 3 - 4 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Di b r o m o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 7 74 - 9 5 - 3 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o b e n z e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 95 - 5 0 - 1 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 4 - D i c h l o r o b e n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 6 - 4 6 - 7 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e 10 0 61 10166 EP A 5 0 3 0 B 1. 5 1 10 - 5 7 - 6 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h a n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 75 - 3 4 - 3 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 7 - 0 6 - 2 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 38 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - T ri p B l a n k W at e r AZ K 0 1 2 0 - 1 3 AZK0120 1 1/ 0 1 / 1 6 0 0 : 0 0 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 1 7 : 3 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 3 5 - 4 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 5 15 6 - 5 9 - 2 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 2 - D i c h l o r o e t h e n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 15 6 - 6 0 - 5 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 - D i c h l o r o p r o p a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 78 - 8 7 - 5 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 cis - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 1 - 5 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 6 1 - 0 2 - 6 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Et h y l b e n z e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 2 10 0 - 4 1 - 4 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Io d o m e t h a n e 10 61 10166 EP A 5 0 3 0 B 0. 6 74 - 8 8 - 4 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l B u t y l K e t o n e (2 - H e x a n o n e ) 50 61 10166 EP A 5 0 3 0 B 0. 9 59 1 - 7 8 - 6 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l e n e C h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 0 9 - 2 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Me t h y l E t h y l K e t o n e (2 - B u t a n o n e ) 10 0 61 10166 EP A 5 0 3 0 B 1. 1 78 - 9 3 - 3 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) 10 0 61 10166 EP A 5 0 3 0 B 1. 7 10 8 - 1 0 - 1 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 St y r e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 10 0 - 4 2 - 5 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e 5. 0 61 10166 EP A 5 0 3 0 B 0. 6 63 0 - 2 0 - 6 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 79 - 3 4 - 5 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a c h l o r o e t h e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 12 7 - 1 8 - 4 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T olu e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 3 10 8 - 8 8 - 3 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 1 - T ric h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 71 - 5 5 - 6 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 1, 1 , 2 - T ric h l o r o e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 8 79 - 0 0 - 5 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o e t h e n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 4 79 - 0 1 - 6 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T ric h l o r o f l u o r o m e t h a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 5 75 - 6 9 - 4 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 Page 39 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - T ri p B l a n k W at e r AZ K 0 1 2 0 - 1 3 AZK0120 1 1/ 0 1 / 1 6 0 0 : 0 0 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 1 7 : 3 0 V ol a t i l e O r g a n i c C o m p o u n d s b y E PA 8 2 6 0 ND EP A 8 2 6 0 B ug / L 1 1, 2 , 3 - T ric h l o r o p r o p a n e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 96 - 1 8 - 4 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l Ac e t a t e 50 61 10166 EP A 5 0 3 0 B 0. 8 10 8 - 0 5 - 4 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 V in y l C h l o r i d e 1. 0 61 10166 EP A 5 0 3 0 B 0. 7 75 - 0 1 - 4 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 Xy l e n e s , t o t a l 5. 0 61 10166 EP A 5 0 3 0 B 0. 4 13 3 0 - 2 0 - 7 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 ND EP A 8 2 6 0 B ug / L 1 T et r a h y d r o f u r a n 10 61 10166 EP A 5 0 3 0 B 1. 5 10 9 - 9 9 - 9 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 EP A 8 2 6 0 B 98 % Su r r : D i b r o m o f l u o r o m e t h a n e 61 10166 EP A 5 0 3 0 B 18 6 8 - 5 3 - 7 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 10 0 % Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 61 10166 EP A 5 0 3 0 B 17 0 6 0 - 0 7 - 0 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 78 - 1 2 0 EP A 8 2 6 0 B 91 % Su r r : T ol u e n e - d 8 61 10166 EP A 5 0 3 0 B 20 3 7 - 2 6 - 5 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 EP A 8 2 6 0 B 93 % Su r r : 4 - B r o m o f l u o r o b e n z e n e 61 10166 EP A 5 0 3 0 B 46 0 - 0 0 - 4 1 1/07/16 16:13 1 1/ 0 7 / 1 6 0 9 : 0 0 80 - 1 2 0 Page 40 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t An a l y t e SW S L / RL Pr e p Me t h o d Qu a l DF Un i t s Batch An a l y t i c a l Me t h o d MD L CA S # Pr e p D a t e / T imeAnalysis Date/T ime Cl i e n t I D : Da t e / T im e S a m p l e d : Ma t r i x : Report No.: La b N o : Da t e / T im e R e c e i v e d : 13 0 2 - C D 1 S Gr o u n d W at e r AZ K 0 1 2 0 - 1 4 AZK0120 1 1/ 0 3 / 1 6 1 3 : 0 7 Pr o j e c t : Ca b a r r u s C o - C & D 1 1/ 0 3 / 1 6 0 9 : 3 5 Ge n e r a l C h e m i s t r y ND SM 5 2 1 0 B ug / L 1 Bio c h e m i c a l O x y g e n D e m a n d 20 0 0 6110115 SM 5 2 1 0 B 20 0 0 E- 1 0 1 0 6 1 1/09/16 07:52 1 1/ 0 4 / 1 6 0 8 : 5 6 Page 41 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e Ge n e r a l C h e m i s t r y - Q u a l i t y C o n t r o l Ba t c h 6 11 0 1 15 - S M 5 2 1 0 B Bl a n k ( 6 11 0 1 15 - B L K 1 ) Pr e p a r e d : 1 1/ 0 4 / 1 6 An a l y z e d : 1 1/09/16 Bi o c h e m i c a l O x y g e n D e m a n d ug / L ND 20 0 0 LC S ( 6 11 0 1 15 - B S 1 ) Pr e p a r e d : 1 1/ 0 4 / 1 6 An a l y z e d : 1 1/09/16 Bi o c h e m i c a l O x y g e n D e m a n d ug / L 22 4 0 0 0 20 0 0 19 8 0 0 0 85 - 11 5 11 3 Du p l i c a t e ( 6 11 0 1 15 - D U P 1 ) Pr e p a r e d : 1 1/ 0 4 / 1 6 An a l y z e d : 1 1/09/16 So u r ce : AZ K 0 1 4 3 - 0 1 Bi o c h e m i c a l O x y g e n D e m a n d ug / L 19 6 0 0 0 20 0 0 ND 20 Ba t c h 6 1 10 1 2 8 - S M 2 5 4 0 C Bl a n k ( 6 1 10 1 2 8 - B L K 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 4 / 1 6 T ot a l D i s s o l v e d S o l i d s ug / L ND 10 0 0 0 LC S ( 6 1 10 1 2 8 - B S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 4 / 1 6 T ot a l D i s s o l v e d S o l i d s ug / L 33 8 0 0 0 10 0 0 0 40 0 0 0 0 84 - 1 0 8 84 Du p l i c a t e ( 6 1 10 1 2 8 - D U P 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 4 / 1 6 So u r ce : AZ K 0 0 4 4 - 0 6 T ot a l D i s s o l v e d S o l i d s ug / L 42 3 0 0 0 10 0 0 0 47 5 0 0 0 10 QR-03 12 Du p l i c a t e ( 6 1 10 1 2 8 - D U P 2 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 4 / 1 6 So u r ce : AZ K 0 1 2 0 - 0 7 T ot a l D i s s o l v e d S o l i d s ug / L 36 7 0 0 0 66 7 0 0 41 3 0 0 0 10 QR-03 12 Ba t c h 6 1 10 1 5 3 - E P A 4 1 0 . 4 Bl a n k ( 6 1 10 1 5 3 - B L K 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 5 / 1 6 Ch e m i c a l O x y g e n D e m a n d ug / L ND 10 0 0 0 Page 42 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e Ge n e r a l C h e m i s t r y - Q u a l i t y C o n t r o l Ba t c h 6 1 10 1 5 3 - E P A 4 1 0 . 4 LC S ( 6 1 10 1 5 3 - B S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 5 / 1 6 Ch e m i c a l O x y g e n D e m a n d ug / L 20 4 0 0 0 10 0 0 0 20 0 0 0 0 90 - 11 0 10 2 Du p l i c a t e ( 6 1 10 1 5 3 - D U P 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 5 / 1 6 So u r ce : AZ K 0 0 8 1 - 0 1 Ch e m i c a l O x y g e n D e m a n d ug / L 32 6 0 0 0 40 0 0 0 31 7 0 0 0 10 3 Ma t r i x S p i k e ( 6 1 10 1 5 3 - M S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 5 / 1 6 So u r ce : AZ K 0 0 4 2 - 0 1 Ch e m i c a l O x y g e n D e m a n d ug / L 23 6 0 0 0 10 0 0 0 20 0 0 0 0 26 5 0 0 90 - 11 0 10 5 Ma t r i x S p i k e ( 6 1 10 1 5 3 - M S 2 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 5 / 1 6 So u r ce : AZ K 0 0 4 4 - 0 3 Ch e m i c a l O x y g e n D e m a n d ug / L 22 7 0 0 0 10 0 0 0 20 0 0 0 0 25 8 0 0 90 - 11 0 10 1 Ma t r i x S p i k e D u p ( 6 1 10 1 5 3 - M S D 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 5 / 1 6 So u r ce : AZ K 0 0 4 2 - 0 1 Ch e m i c a l O x y g e n D e m a n d ug / L 22 7 0 0 0 10 0 0 0 20 0 0 0 0 26 5 0 0 10 90 - 11 0 10 0 4 Ba t c h 6 1 10 1 5 4 - E P A 9 0 6 0 A Bl a n k ( 6 1 10 1 5 4 - B L K 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 8 / 1 6 T ot a l O r g a n i c C a r b o n ug / L ND 10 0 0 LC S ( 6 1 10 1 5 4 - B S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 8 / 1 6 T ot a l O r g a n i c C a r b o n ug / L 19 6 0 0 10 0 0 20 0 0 0 88 - 11 2 98 Ma t r i x S p i k e ( 6 1 10 1 5 4 - M S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 8 / 1 6 So u r ce : AZ J 0 8 4 1 - 0 1 T ot a l O r g a n i c C a r b o n ug / L 19 4 0 0 10 0 0 20 0 0 0 ND 67 - 1 4 1 97 Ma t r i x S p i k e D u p ( 6 1 10 1 5 4 - M S D 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 8 / 1 6 So u r ce : AZ J 0 8 4 1 - 0 1 T ot a l O r g a n i c C a r b o n ug / L 19 2 0 0 10 0 0 20 0 0 0 ND 16 67 - 1 4 1 96 0. 9 Page 43 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e Ge n e r a l C h e m i s t r y - Q u a l i t y C o n t r o l Ba t c h 6 1 10 1 6 4 - S M 2 3 2 0 B Bl a n k ( 6 1 10 1 6 4 - B L K 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 7 / 1 6 Al k a l i n i t y a s C a C O 3 ug / L ND 10 0 0 LC S ( 6 1 10 1 6 4 - B S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 7 / 1 6 Al k a l i n i t y a s C a C O 3 ug / L 10 0 0 0 0 10 0 0 10 0 0 0 0 85 - 11 5 10 0 Du p l i c a t e ( 6 1 10 1 6 4 - D U P 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 7 / 1 6 So u r ce : AZ K 0 0 4 2 - 0 1 Al k a l i n i t y a s C a C O 3 ug / L 45 0 0 0 10 0 0 46 0 0 0 10 2 Ba t c h 6 1 10 1 9 1 - S M 4 5 0 0 - S D Bl a n k ( 6 1 10 1 9 1 - B L K 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 8 / 1 6 T ot a l S u l f i d e ug / L ND 20 0 LC S ( 6 1 10 1 9 1 - B S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 8 / 1 6 T ot a l S u l f i d e ug / L 54 4 20 0 50 1 . 0 0 80 - 1 2 0 10 9 Ma t r i x S p i k e ( 6 1 10 1 9 1 - M S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 8 / 1 6 So u r ce : AZ K 0 1 5 1 - 0 1 T ot a l S u l f i d e ug / L 78 1 20 0 50 1 . 0 0 ND QM-05 30 - 1 2 9 15 6 Ma t r i x S p i k e D u p ( 6 1 10 1 9 1 - M S D 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 8 / 1 6 So u r ce : AZ K 0 1 5 1 - 0 1 T ot a l S u l f i d e ug / L 76 3 20 0 50 1 . 0 0 ND 10 QM-05 30 - 1 2 9 15 2 2. 3 3 Ba t c h 6 1 10 3 2 7 - S M 2 5 4 0 C Bl a n k ( 6 1 10 3 2 7 - B L K 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 1 1/ 1 6 T ot a l D i s s o l v e d S o l i d s ug / L ND 10 0 0 0 Page 44 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e Ge n e r a l C h e m i s t r y - Q u a l i t y C o n t r o l Ba t c h 6 1 10 3 2 7 - S M 2 5 4 0 C LC S ( 6 1 10 3 2 7 - B S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 1 1/ 1 6 T ot a l D i s s o l v e d S o l i d s ug / L 39 8 0 0 0 10 0 0 0 40 0 0 0 0 84 - 1 0 8 10 0 Du p l i c a t e ( 6 1 10 3 2 7 - D U P 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 1 1/ 1 6 So u r ce : AZ K 0 1 2 0 - 0 3 R E 1 T ot a l D i s s o l v e d S o l i d s ug / L 88 0 0 0 0 10 0 0 0 0 85 0 0 0 0 10 3 Du p l i c a t e ( 6 1 10 3 2 7 - D U P 2 ) Pr e p a r e d & An a l y z e d : 1 1/ 1 1/ 1 6 So u r ce : AZ K 0 1 2 0 - 0 9 R E 1 T ot a l D i s s o l v e d S o l i d s ug / L 53 7 0 0 0 33 3 0 0 51 7 0 0 0 10 4 Du p l i c a t e ( 6 1 10 3 2 7 - D U P 3 ) Pr e p a r e d & An a l y z e d : 1 1/ 1 1/ 1 6 So u r ce : AZ K 0 1 2 0 - 1 1R E 1 T ot a l D i s s o l v e d S o l i d s ug / L 40 8 0 0 0 40 0 0 0 42 8 0 0 0 10 5 Page 45 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e In o r g a n i c An i o n s - Q u a l i t y C o n t r o l Ba t c h 6 1 10 3 0 5 - E P A 9 0 5 6 A Bl a n k ( 6 1 10 3 0 5 - B L K 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 1 0 / 1 6 Ch l o r i d e ug / L ND 10 0 0 Ni t r a t e a s N ug / L ND 50 Su l f a t e ug / L ND 50 0 0 LC S ( 6 1 10 3 0 5 - B S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 1 0 / 1 6 Ch l o r i d e ug / L 99 6 0 10 0 0 10 0 1 0 90 - 11 0 99 Ni t r a t e a s N ug / L 10 0 0 0 50 10 0 2 0 90 - 11 0 10 0 Su l f a t e ug / L 10 2 0 0 50 0 0 10 0 2 0 90 - 11 0 10 2 Ma t r i x S p i k e ( 6 1 10 3 0 5 - M S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 1 0 / 1 6 So u r ce : AZ K 0 3 6 7 - 0 2 Ch l o r i d e ug / L 59 2 0 0 10 0 0 10 0 1 0 54 1 0 0 QM-02 90 - 11 0 50 Ni t r a t e a s N ug / L 32 5 0 0 50 10 0 2 0 24 3 0 0 QM-02 90 - 11 0 82 Su l f a t e ug / L 1 13 0 0 0 50 0 0 10 0 2 0 1 15 0 0 0 QM-02 90 - 11 0 0 Ma t r i x S p i k e ( 6 1 10 3 0 5 - M S 2 ) Pr e p a r e d & An a l y z e d : 1 1/ 1 0 / 1 6 So u r ce : AZ K 0 1 2 0 - 11 Ch l o r i d e ug / L 13 5 0 0 10 0 0 10 0 1 0 35 2 0 90 - 11 0 10 0 Ni t r a t e a s N ug / L 10 1 0 0 50 10 0 2 0 94 . 0 90 - 11 0 10 0 Su l f a t e ug / L 12 2 0 0 50 0 0 10 0 2 0 ND QM-05 90 - 11 0 12 1 Ma t r i x S p i k e D u p ( 6 1 10 3 0 5 - M S D 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 1 0 / 1 6 So u r ce : AZ K 0 3 6 7 - 0 2 Ch l o r i d e ug / L 59 1 0 0 10 0 0 10 0 1 0 54 1 0 0 15 QM-02 90 - 11 0 50 0. 0 9 Ni t r a t e a s N ug / L 32 4 0 0 50 10 0 2 0 24 3 0 0 15 QM-02 90 - 11 0 82 0. 0 8 Su l f a t e ug / L 1 13 0 0 0 50 0 0 10 0 2 0 1 15 0 0 0 15 QM-02 90 - 11 0 0 0. 0 9 Page 46 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e Me t a l s , T ot a l - Q u a l i t y C o n t r o l Ba t c h 6 1 10 1 0 1 - E P A 7 4 7 0 A Bl a n k ( 6 1 10 1 0 1 - B L K 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 4 / 1 6 Me r c u r y ug / L ND 0. 2 0 0 LC S ( 6 1 10 1 0 1 - B S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 4 / 1 6 Me r c u r y ug / L 2. 5 2 0. 2 0 0 2. 5 0 0 0 80 - 1 2 0 10 1 Ma t r i x S p i k e ( 6 1 10 1 0 1 - M S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 4 / 1 6 So u r ce : AZ K 0 1 0 9 - 0 7 Me r c u r y ug / L 1. 9 5 0. 2 0 0 2. 5 0 0 0 ND 75 - 1 2 5 78 Ma t r i x S p i k e D u p ( 6 1 10 1 0 1 - M S D 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 4 / 1 6 So u r ce : AZ K 0 1 0 9 - 0 7 Me r c u r y ug / L 1. 9 4 0. 2 0 0 2. 5 0 0 0 ND 20 75 - 1 2 5 78 0. 3 Po s t S p i k e ( 6 1 10 1 0 1 - P S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 4 / 1 6 So u r ce : AZ K 0 1 0 9 - 0 7 Me r c u r y ug / L 1. 3 5 1. 6 6 6 7 0. 0 0 7 80 - 1 2 0 80 Ba t c h 6 1 10 1 8 2 - E P A 3 0 0 5 A Bl a n k ( 6 1 10 1 8 2 - B L K 1 ) Pr e p a r e d : 1 1/ 0 8 / 1 6 An a l y z e d : 1 1/16/16 An t i m o n y ug / L ND 6. 0 0 Ar s e n i c ug / L ND 10 . 0 Ba r i u m ug / L ND 10 0 Be r y l l i u m ug / L ND 1. 0 0 Ca d m i u m ug / L ND 1. 0 0 Ch r o m i u m ug / L ND 10 . 0 Co b a l t ug / L ND 10 . 0 Co p p e r ug / L ND 10 . 0 Ir o n ug / L ND 40 . 0 Le a d ug / L ND 10 . 0 Ma n g a n e s e ug / L ND 10 . 0 Ni c k e l ug / L ND 50 . 0 Page 47 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e Me t a l s , T ot a l - Q u a l i t y C o n t r o l Ba t c h 6 1 10 1 8 2 - E P A 3 0 0 5 A Bl a n k ( 6 1 10 1 8 2 - B L K 1 ) Pr e p a r e d : 1 1/ 0 8 / 1 6 An a l y z e d : 1 1/16/16 Se l e n i u m ug / L ND 10 . 0 Si l v e r ug / L ND 10 . 0 Th a l l i u m ug / L ND 5. 5 0 V an a d i u m ug / L ND 25 . 0 Zi n c ug / L ND 10 . 0 LC S ( 6 1 10 1 8 2 - B S 1 ) Pr e p a r e d : 1 1/ 0 8 / 1 6 An a l y z e d : 1 1/16/16 An t i m o n y ug / L 10 2 6. 0 0 10 0 . 0 0 80 - 1 2 0 10 2 Ar s e n i c ug / L 97 . 5 10 . 0 10 0 . 0 0 80 - 1 2 0 97 Ba r i u m ug / L 94 . 5 10 0 10 0 . 0 0 J 80 - 1 2 0 95 Be r y l l i u m ug / L 95 . 1 1. 0 0 10 0 . 0 0 80 - 1 2 0 95 Ca d m i u m ug / L 95 . 2 1. 0 0 10 0 . 0 0 80 - 1 2 0 95 Ch r o m i u m ug / L 99 . 6 10 . 0 10 0 . 0 0 80 - 1 2 0 10 0 Co b a l t ug / L 10 1 10 . 0 10 0 . 0 0 80 - 1 2 0 10 1 Co p p e r ug / L 98 . 0 10 . 0 10 0 . 0 0 80 - 1 2 0 98 Ir o n ug / L 10 6 0 40 . 0 10 0 0 . 0 80 - 1 2 0 10 6 Le a d ug / L 96 . 7 10 . 0 10 0 . 0 0 80 - 1 2 0 97 Ma n g a n e s e ug / L 10 2 10 . 0 10 0 . 0 0 80 - 1 2 0 10 2 Ni c k e l ug / L 10 2 50 . 0 10 0 . 0 0 80 - 1 2 0 10 2 Se l e n i u m ug / L 99 . 5 10 . 0 10 0 . 0 0 80 - 1 2 0 99 Si l v e r ug / L 97 . 2 10 . 0 10 0 . 0 0 80 - 1 2 0 97 Th a l l i u m ug / L 96 . 4 5. 5 0 10 0 . 0 0 80 - 1 2 0 96 V an a d i u m ug / L 98 . 9 25 . 0 10 0 . 0 0 80 - 1 2 0 99 Zi n c ug / L 10 3 10 . 0 10 0 . 0 0 80 - 1 2 0 10 3 Ma t r i x S p i k e ( 6 1 10 1 8 2 - M S 1 ) Pr e p a r e d : 1 1/ 0 8 / 1 6 An a l y z e d : 1 1/16/16 So u r ce : AZ K 0 0 4 2 - 0 8 An t i m o n y ug / L 10 3 6. 0 0 10 0 . 0 0 ND 75 - 1 2 5 10 3 Ar s e n i c ug / L 10 2 10 . 0 10 0 . 0 0 ND 75 - 1 2 5 10 2 Page 48 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e Me t a l s , T ot a l - Q u a l i t y C o n t r o l Ba t c h 6 1 10 1 8 2 - E P A 3 0 0 5 A Ma t r i x S p i k e ( 6 1 10 1 8 2 - M S 1 ) Pr e p a r e d : 1 1/ 0 8 / 1 6 An a l y z e d : 1 1/16/16 So u r ce : AZ K 0 0 4 2 - 0 8 Ba r i u m ug / L 15 7 10 0 10 0 . 0 0 61 . 8 75 - 1 2 5 95 Be r y l l i u m ug / L 84 . 7 1. 0 0 10 0 . 0 0 ND 75 - 1 2 5 85 Ca d m i u m ug / L 95 . 7 1. 0 0 10 0 . 0 0 0. 1 4 75 - 1 2 5 96 Ch r o m i u m ug / L 10 7 10 . 0 10 0 . 0 0 ND 75 - 1 2 5 10 7 Co b a l t ug / L 11 9 10 . 0 10 0 . 0 0 18 . 7 75 - 1 2 5 10 0 Co p p e r ug / L 10 2 10 . 0 10 0 . 0 0 4. 4 0 75 - 1 2 5 98 Ir o n ug / L 22 3 0 40 . 0 10 0 0 . 0 1 17 0 75 - 1 2 5 10 6 Le a d ug / L 94 . 0 10 . 0 10 0 . 0 0 0. 1 8 75 - 1 2 5 94 Ma n g a n e s e ug / L 51 0 0 10 . 0 10 0 . 0 0 50 3 0 QM-02 75 - 1 2 5 71 Ni c k e l ug / L 12 8 50 . 0 10 0 . 0 0 27 . 9 75 - 1 2 5 10 0 Se l e n i u m ug / L 10 4 10 . 0 10 0 . 0 0 ND 75 - 1 2 5 10 4 Si l v e r ug / L 96 . 4 10 . 0 10 0 . 0 0 ND 75 - 1 2 5 96 Th a l l i u m ug / L 96 . 9 5. 5 0 10 0 . 0 0 ND 75 - 1 2 5 97 V an a d i u m ug / L 10 7 25 . 0 10 0 . 0 0 ND 75 - 1 2 5 10 7 Zi n c ug / L 23 0 10 . 0 10 0 . 0 0 11 9 75 - 1 2 5 11 1 Ma t r i x S p i k e D u p ( 6 1 10 1 8 2 - M S D 1 ) Pr e p a r e d : 1 1/ 0 8 / 1 6 An a l y z e d : 1 1/16/16 So u r ce : AZ K 0 0 4 2 - 0 8 An t i m o n y ug / L 10 3 6. 0 0 10 0 . 0 0 ND 20 75 - 1 2 5 10 3 0. 0 3 Ar s e n i c ug / L 10 1 10 . 0 10 0 . 0 0 ND 20 75 - 1 2 5 10 1 0. 2 Ba r i u m ug / L 15 3 10 0 10 0 . 0 0 61 . 8 20 75 - 1 2 5 91 3 Be r y l l i u m ug / L 84 . 6 1. 0 0 10 0 . 0 0 ND 20 75 - 1 2 5 85 0. 1 Ca d m i u m ug / L 98 . 7 1. 0 0 10 0 . 0 0 0. 1 4 20 75 - 1 2 5 99 3 Ch r o m i u m ug / L 10 0 10 . 0 10 0 . 0 0 ND 20 75 - 1 2 5 10 0 6 Co b a l t ug / L 11 7 10 . 0 10 0 . 0 0 18 . 7 20 75 - 1 2 5 99 1 Co p p e r ug / L 10 5 10 . 0 10 0 . 0 0 4. 4 0 20 75 - 1 2 5 10 0 2 Ir o n ug / L 21 8 0 40 . 0 10 0 0 . 0 1 17 0 20 75 - 1 2 5 10 1 2 Le a d ug / L 94 . 2 10 . 0 10 0 . 0 0 0. 1 8 20 75 - 1 2 5 94 0. 2 Ma n g a n e s e ug / L 50 1 0 10 . 0 10 0 . 0 0 50 3 0 20 QM-02 75 - 1 2 5 0 2 Page 49 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e Me t a l s , T ot a l - Q u a l i t y C o n t r o l Ba t c h 6 1 10 1 8 2 - E P A 3 0 0 5 A Ma t r i x S p i k e D u p ( 6 1 10 1 8 2 - M S D 1 ) Pr e p a r e d : 1 1/ 0 8 / 1 6 An a l y z e d : 1 1/16/16 So u r ce : AZ K 0 0 4 2 - 0 8 Ni c k e l ug / L 12 6 50 . 0 10 0 . 0 0 27 . 9 20 75 - 1 2 5 98 2 Se l e n i u m ug / L 10 4 10 . 0 10 0 . 0 0 ND 20 75 - 1 2 5 10 4 0. 3 Si l v e r ug / L 95 . 0 10 . 0 10 0 . 0 0 ND 20 75 - 1 2 5 95 1 Th a l l i u m ug / L 94 . 9 5. 5 0 10 0 . 0 0 ND 20 75 - 1 2 5 95 2 V an a d i u m ug / L 10 2 25 . 0 10 0 . 0 0 ND 20 75 - 1 2 5 10 2 5 Zi n c ug / L 22 0 10 . 0 10 0 . 0 0 11 9 20 75 - 1 2 5 10 0 5 Po s t S p i k e ( 6 1 10 1 8 2 - P S 1 ) Pr e p a r e d : 1 1/ 0 8 / 1 6 An a l y z e d : 1 1/16/16 So u r ce : AZ K 0 0 4 2 - 0 8 An t i m o n y ug / L 10 2 10 0 . 0 0 0. 2 0 80 - 1 2 0 10 2 Ar s e n i c ug / L 10 4 10 0 . 0 0 0. 3 0 80 - 1 2 0 10 3 Ba r i u m ug / L 16 0 10 0 . 0 0 61 . 8 80 - 1 2 0 98 Be r y l l i u m ug / L 87 . 2 10 0 . 0 0 0. 0 2 80 - 1 2 0 87 Ca d m i u m ug / L 99 . 0 10 0 . 0 0 0. 1 4 80 - 1 2 0 99 Ch r o m i u m ug / L 99 . 7 10 0 . 0 0 0. 4 0 80 - 1 2 0 99 Co b a l t ug / L 11 9 10 0 . 0 0 18 . 7 80 - 1 2 0 10 0 Co p p e r ug / L 10 2 10 0 . 0 0 4. 4 0 80 - 1 2 0 98 Ir o n ug / L 21 8 0 10 0 0 . 0 1 17 0 80 - 1 2 0 10 1 Le a d ug / L 93 . 4 10 0 . 0 0 0. 1 8 80 - 1 2 0 93 Ma n g a n e s e ug / L 51 0 0 10 0 . 0 0 50 3 0 QM-02 80 - 1 2 0 66 Ni c k e l ug / L 12 6 10 0 . 0 0 27 . 9 80 - 1 2 0 98 Se l e n i u m ug / L 10 7 10 0 . 0 0 -0 . 2 2 80 - 1 2 0 10 7 Si l v e r ug / L 97 . 8 10 0 . 0 0 0. 0 2 80 - 1 2 0 98 Th a l l i u m ug / L 95 . 9 10 0 . 0 0 0. 0 3 80 - 1 2 0 96 V an a d i u m ug / L 10 5 10 0 . 0 0 0. 4 2 80 - 1 2 0 10 5 Zi n c ug / L 22 2 10 0 . 0 0 11 9 80 - 1 2 0 10 3 Ba t c h 6 1 10 2 2 2 - E P A 3 0 0 5 A Page 50 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e Me t a l s , T ot a l - Q u a l i t y C o n t r o l Ba t c h 6 1 10 2 2 2 - E P A 3 0 0 5 A Bl a n k ( 6 1 10 2 2 2 - B L K 1 ) Pr e p a r e d : 1 1/ 0 9 / 1 6 An a l y z e d : 1 1/16/16 An t i m o n y ug / L ND 6. 0 0 Ar s e n i c ug / L ND 10 . 0 Ba r i u m ug / L ND 10 0 Be r y l l i u m ug / L ND 1. 0 0 Ca d m i u m ug / L ND 1. 0 0 Ch r o m i u m ug / L ND 10 . 0 Co b a l t ug / L ND 10 . 0 Co p p e r ug / L ND 10 . 0 Ir o n ug / L ND 40 . 0 Le a d ug / L ND 10 . 0 Ma n g a n e s e ug / L ND 10 . 0 Ni c k e l ug / L ND 50 . 0 Se l e n i u m ug / L ND 10 . 0 Si l v e r ug / L ND 10 . 0 Th a l l i u m ug / L ND 5. 5 0 V an a d i u m ug / L ND 25 . 0 Zi n c ug / L ND 10 . 0 LC S ( 6 1 10 2 2 2 - B S 1 ) Pr e p a r e d : 1 1/ 0 9 / 1 6 An a l y z e d : 1 1/16/16 An t i m o n y ug / L 10 3 6. 0 0 10 0 . 0 0 80 - 1 2 0 10 3 Ar s e n i c ug / L 98 . 3 10 . 0 10 0 . 0 0 80 - 1 2 0 98 Ba r i u m ug / L 95 . 7 10 0 10 0 . 0 0 J 80 - 1 2 0 96 Be r y l l i u m ug / L 98 . 3 1. 0 0 10 0 . 0 0 80 - 1 2 0 98 Ca d m i u m ug / L 96 . 3 1. 0 0 10 0 . 0 0 80 - 1 2 0 96 Ch r o m i u m ug / L 98 . 2 10 . 0 10 0 . 0 0 80 - 1 2 0 98 Co b a l t ug / L 95 . 6 10 . 0 10 0 . 0 0 80 - 1 2 0 96 Co p p e r ug / L 96 . 2 10 . 0 10 0 . 0 0 80 - 1 2 0 96 Ir o n ug / L 95 1 40 . 0 10 0 0 . 0 80 - 1 2 0 95 Page 51 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e Me t a l s , T ot a l - Q u a l i t y C o n t r o l Ba t c h 6 1 10 2 2 2 - E P A 3 0 0 5 A LC S ( 6 1 10 2 2 2 - B S 1 ) Pr e p a r e d : 1 1/ 0 9 / 1 6 An a l y z e d : 1 1/16/16 Le a d ug / L 98 . 3 10 . 0 10 0 . 0 0 80 - 1 2 0 98 Ma n g a n e s e ug / L 97 . 9 10 . 0 10 0 . 0 0 80 - 1 2 0 98 Ni c k e l ug / L 95 . 5 50 . 0 10 0 . 0 0 80 - 1 2 0 95 Se l e n i u m ug / L 10 2 10 . 0 10 0 . 0 0 80 - 1 2 0 10 2 Si l v e r ug / L 10 1 10 . 0 10 0 . 0 0 80 - 1 2 0 10 1 Th a l l i u m ug / L 99 . 1 5. 5 0 10 0 . 0 0 80 - 1 2 0 99 V an a d i u m ug / L 97 . 9 25 . 0 10 0 . 0 0 80 - 1 2 0 98 Zi n c ug / L 10 0 10 . 0 10 0 . 0 0 80 - 1 2 0 10 0 Ma t r i x S p i k e ( 6 1 10 2 2 2 - M S 1 ) Pr e p a r e d : 1 1/ 0 9 / 1 6 An a l y z e d : 1 1/16/16 So u r ce : AZ K 0 1 0 9 - 0 7 An t i m o n y ug / L 10 5 6. 0 0 10 0 . 0 0 ND 75 - 1 2 5 10 5 Ar s e n i c ug / L 10 3 10 . 0 10 0 . 0 0 2. 9 6 75 - 1 2 5 10 0 Ba r i u m ug / L 28 3 10 0 10 0 . 0 0 19 5 75 - 1 2 5 88 Be r y l l i u m ug / L 95 . 4 1. 0 0 10 0 . 0 0 ND 75 - 1 2 5 95 Ca d m i u m ug / L 97 . 4 1. 0 0 10 0 . 0 0 ND 75 - 1 2 5 97 Ch r o m i u m ug / L 93 . 5 10 . 0 10 0 . 0 0 ND 75 - 1 2 5 94 Co b a l t ug / L 98 . 3 10 . 0 10 0 . 0 0 1. 9 0 75 - 1 2 5 96 Co p p e r ug / L 93 . 5 10 . 0 10 0 . 0 0 1. 1 7 75 - 1 2 5 92 Ir o n ug / L 15 8 0 40 . 0 10 0 0 . 0 61 9 75 - 1 2 5 96 Le a d ug / L 98 . 4 10 . 0 10 0 . 0 0 ND 75 - 1 2 5 98 Ma n g a n e s e ug / L 38 4 10 . 0 10 0 . 0 0 29 3 75 - 1 2 5 92 Ni c k e l ug / L 97 . 3 50 . 0 10 0 . 0 0 4. 9 0 75 - 1 2 5 92 Se l e n i u m ug / L 10 4 10 . 0 10 0 . 0 0 ND 75 - 1 2 5 10 4 Si l v e r ug / L 97 . 2 10 . 0 10 0 . 0 0 ND 75 - 1 2 5 97 Th a l l i u m ug / L 99 . 2 5. 5 0 10 0 . 0 0 ND 75 - 1 2 5 99 V an a d i u m ug / L 97 . 5 25 . 0 10 0 . 0 0 ND 75 - 1 2 5 98 Zi n c ug / L 99 . 6 10 . 0 10 0 . 0 0 3. 4 6 75 - 1 2 5 96 Page 52 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e Me t a l s , T ot a l - Q u a l i t y C o n t r o l Ba t c h 6 1 10 2 2 2 - E P A 3 0 0 5 A Ma t r i x S p i k e D u p ( 6 1 10 2 2 2 - M S D 1 ) Pr e p a r e d : 1 1/ 0 9 / 1 6 An a l y z e d : 1 1/16/16 So u r ce : AZ K 0 1 0 9 - 0 7 An t i m o n y ug / L 10 5 6. 0 0 10 0 . 0 0 ND 20 75 - 1 2 5 10 5 0. 4 Ar s e n i c ug / L 10 2 10 . 0 10 0 . 0 0 2. 9 6 20 75 - 1 2 5 99 1 Ba r i u m ug / L 28 4 10 0 10 0 . 0 0 19 5 20 75 - 1 2 5 89 0. 4 Be r y l l i u m ug / L 97 . 6 1. 0 0 10 0 . 0 0 ND 20 75 - 1 2 5 98 2 Ca d m i u m ug / L 96 . 3 1. 0 0 10 0 . 0 0 ND 20 75 - 1 2 5 96 1 Ch r o m i u m ug / L 10 0 10 . 0 10 0 . 0 0 ND 20 75 - 1 2 5 10 0 7 Co b a l t ug / L 10 2 10 . 0 10 0 . 0 0 1. 9 0 20 75 - 1 2 5 10 0 4 Co p p e r ug / L 98 . 2 10 . 0 10 0 . 0 0 1. 1 7 20 75 - 1 2 5 97 5 Ir o n ug / L 16 2 0 40 . 0 10 0 0 . 0 61 9 20 75 - 1 2 5 10 0 2 Le a d ug / L 97 . 4 10 . 0 10 0 . 0 0 ND 20 75 - 1 2 5 97 1 Ma n g a n e s e ug / L 39 2 10 . 0 10 0 . 0 0 29 3 20 75 - 1 2 5 10 0 2 Ni c k e l ug / L 10 2 50 . 0 10 0 . 0 0 4. 9 0 20 75 - 1 2 5 97 5 Se l e n i u m ug / L 10 1 10 . 0 10 0 . 0 0 ND 20 75 - 1 2 5 10 1 3 Si l v e r ug / L 10 0 10 . 0 10 0 . 0 0 ND 20 75 - 1 2 5 10 0 3 Th a l l i u m ug / L 99 . 3 5. 5 0 10 0 . 0 0 ND 20 75 - 1 2 5 99 0. 1 V an a d i u m ug / L 10 6 25 . 0 10 0 . 0 0 ND 20 75 - 1 2 5 10 6 8 Zi n c ug / L 10 2 10 . 0 10 0 . 0 0 3. 4 6 20 75 - 1 2 5 99 3 Po s t S p i k e ( 6 1 10 2 2 2 - P S 1 ) Pr e p a r e d : 1 1/ 0 9 / 1 6 An a l y z e d : 1 1/16/16 So u r ce : AZ K 0 1 0 9 - 0 7 An t i m o n y ug / L 10 6 10 0 . 0 0 -0 . 0 1 80 - 1 2 0 10 6 Ar s e n i c ug / L 10 6 10 0 . 0 0 2. 9 6 80 - 1 2 0 10 4 Ba r i u m ug / L 29 5 10 0 . 0 0 19 5 80 - 1 2 0 10 0 Be r y l l i u m ug / L 98 . 8 10 0 . 0 0 0. 0 3 80 - 1 2 0 99 Ca d m i u m ug / L 99 . 1 10 0 . 0 0 -0 . 0 0 0 9 80 - 1 2 0 99 Ch r o m i u m ug / L 99 . 2 10 0 . 0 0 0. 2 2 80 - 1 2 0 99 Co b a l t ug / L 10 2 10 0 . 0 0 1. 9 0 80 - 1 2 0 10 0 Co p p e r ug / L 10 1 10 0 . 0 0 1. 1 7 80 - 1 2 0 10 0 Ir o n ug / L 16 3 0 10 0 0 . 0 61 9 80 - 1 2 0 10 1 Page 53 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e Me t a l s , T ot a l - Q u a l i t y C o n t r o l Ba t c h 6 1 10 2 2 2 - E P A 3 0 0 5 A Po s t S p i k e ( 6 1 10 2 2 2 - P S 1 ) Pr e p a r e d : 1 1/ 0 9 / 1 6 An a l y z e d : 1 1/16/16 So u r ce : AZ K 0 1 0 9 - 0 7 Le a d ug / L 10 1 10 0 . 0 0 0. 0 2 80 - 1 2 0 10 1 Ma n g a n e s e ug / L 41 4 10 0 . 0 0 29 3 QM-02 80 - 1 2 0 12 1 Ni c k e l ug / L 10 7 10 0 . 0 0 4. 9 0 80 - 1 2 0 10 2 Se l e n i u m ug / L 10 9 10 0 . 0 0 0. 0 2 80 - 1 2 0 10 9 Si l v e r ug / L 99 . 1 10 0 . 0 0 0. 0 3 80 - 1 2 0 99 Th a l l i u m ug / L 10 2 10 0 . 0 0 0. 0 2 80 - 1 2 0 10 2 V an a d i u m ug / L 10 5 10 0 . 0 0 1. 5 1 80 - 1 2 0 10 4 Zi n c ug / L 11 2 10 0 . 0 0 3. 4 6 80 - 1 2 0 10 9 Page 54 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e V ol a t i l e O r g a n i c C o m p o u n d s b y E P A 8 2 6 0 - Q u a l i t y C o n t r o l Ba t c h 6 1 10 1 6 6 - E P A 5 0 3 0 B Bl a n k ( 6 1 10 1 6 6 - B L K 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 7 / 1 6 Ac e t o n e ug / L ND 10 0 Ac r y l o n i t r i l e ug / L ND 20 0 Be n z e n e ug / L ND 1. 0 Br o m o c h l o r o m e t h a n e ug / L ND 3. 0 Br o m o d i c h l o r o m e t h a n e ug / L ND 1. 0 Br o m o f o r m ug / L ND 3. 0 Br o m o m e t h a n e ug / L ND 10 Ca r b o n D i s u l f i d e ug / L ND 10 0 Ca r b o n T et r a c h l o r i d e ug / L ND 1. 0 Ch l o r o b e n z e n e ug / L ND 3. 0 Ch l o r o e t h a n e ug / L ND 10 Ch l o r o f o r m ug / L ND 5. 0 Ch l o r o m e t h a n e ug / L ND 1. 0 Di b r o m o c h l o r o m e t h a n e ug / L ND 1. 0 1, 2 - D i b r o m o - 3 - c h l o r o p r o p a n e ug / L ND 13 1, 2 - D i b r o m o e t h a n e ug / L ND 1. 0 Di b r o m o m e t h a n e ug / L ND 10 1, 2 - D i c h l o r o b e n z e n e ug / L ND 5. 0 1, 4 - D i c h l o r o b e n z e n e ug / L ND 1. 0 tr a n s - 1 , 4 - D i c h l o r o - 2 - b u t e n e ug / L ND 10 0 1, 1 - D i c h l o r o e t h a n e ug / L ND 5. 0 1, 2 - D i c h l o r o e t h a n e ug / L ND 1. 0 1, 1 - D i c h l o r o e t h e n e ug / L ND 5. 0 ci s - 1 , 2 - D i c h l o r o e t h e n e ug / L ND 5. 0 tr a n s - 1 , 2 - D i c h l o r o e t h e n e ug / L ND 5. 0 1, 2 - D i c h l o r o p r o p a n e ug / L ND 1. 0 ci s - 1 , 3 - D i c h l o r o p r o p e n e ug / L ND 1. 0 Page 55 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e V ol a t i l e O r g a n i c C o m p o u n d s b y E P A 8 2 6 0 - Q u a l i t y C o n t r o l Ba t c h 6 1 10 1 6 6 - E P A 5 0 3 0 B Bl a n k ( 6 1 10 1 6 6 - B L K 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 7 / 1 6 tr a n s - 1 , 3 - D i c h l o r o p r o p e n e ug / L ND 1. 0 Et h y l b e n z e n e ug / L ND 1. 0 Io d o m e t h a n e ug / L ND 10 Me t h y l B u t y l K e t o n e ( 2 - H e x a n o n e ) ug / L ND 50 Me t h y l e n e C h l o r i d e ug / L ND 1. 0 Me t h y l E t h y l K e t o n e ( 2 - B u t a n o n e ) ug / L ND 10 0 4- M e t h y l - 2 - p e n t a n o n e ( M I B K ) ug / L ND 10 0 St y r e n e ug / L ND 1. 0 1, 1 , 1 , 2 - T et r a c h l o r o e t h a n e ug / L ND 5. 0 1, 1 , 2 , 2 - T et r a c h l o r o e t h a n e ug / L ND 1. 0 T et r a c h l o r o e t h e n e ug / L ND 1. 0 T olu e n e ug / L ND 1. 0 1, 1 , 1 - T ri c h l o r o e t h a n e ug / L ND 1. 0 1, 1 , 2 - T ri c h l o r o e t h a n e ug / L ND 1. 0 T ri c h l o r o e t h e n e ug / L ND 1. 0 T ri c h l o r o f l u o r o m e t h a n e ug / L ND 1. 0 1, 2 , 3 - T ri c h l o r o p r o p a n e ug / L ND 1. 0 V in y l Ac e t a t e ug / L ND 50 V in y l C h l o r i d e ug / L ND 1. 0 Xy l e n e s , t o t a l ug / L ND 5. 0 T et r a h y d r o f u r a n ug / L ND 10 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : D i b r o m o f l u o r o m e t h a n e 98 49 ug / L 50 . 0 0 0 78 - 1 2 0 Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 99 50 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : T olu e n e - d 8 92 46 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : 4 - B r o m o f l u o r o b e n z e n e 94 47 LC S ( 6 1 10 1 6 6 - B S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 7 / 1 6 Page 56 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e V ol a t i l e O r g a n i c C o m p o u n d s b y E P A 8 2 6 0 - Q u a l i t y C o n t r o l Ba t c h 6 1 10 1 6 6 - E P A 5 0 3 0 B LC S ( 6 1 10 1 6 6 - B S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 7 / 1 6 Be n z e n e ug / L 59 50 . 0 0 0 67 - 1 3 4 11 9 Ch l o r o b e n z e n e ug / L 59 50 . 0 0 0 69 - 1 2 2 11 8 1, 1 - D i c h l o r o e t h e n e ug / L 65 50 . 0 0 0 58 - 1 4 2 13 0 T olu e n e ug / L 54 50 . 0 0 0 68 - 1 2 7 10 9 T ri c h l o r o e t h e n e ug / L 51 50 . 0 0 0 72 - 1 3 2 10 3 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : D i b r o m o f l u o r o m e t h a n e 10 1 50 ug / L 50 . 0 0 0 78 - 1 2 0 Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 10 1 50 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : T olu e n e - d 8 91 46 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : 4 - B r o m o f l u o r o b e n z e n e 91 46 Ma t r i x S p i k e ( 6 1 10 1 6 6 - M S 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 7 / 1 6 So u r ce : AZ K 0 0 4 2 - 0 7 Be n z e n e ug / L 62 50 . 0 0 0 0. 0 67 - 1 3 4 12 5 Ch l o r o b e n z e n e ug / L 61 50 . 0 0 0 0. 0 QM-05 69 - 1 2 2 12 3 1, 1 - D i c h l o r o e t h e n e ug / L 85 50 . 0 0 0 0. 0 QM-05 58 - 1 4 2 16 9 T olu e n e ug / L 58 50 . 0 0 0 0. 0 68 - 1 2 7 11 6 T ri c h l o r o e t h e n e ug / L 56 50 . 0 0 0 0. 0 72 - 1 3 2 11 3 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : D i b r o m o f l u o r o m e t h a n e 98 49 ug / L 50 . 0 0 0 78 - 1 2 0 Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 10 3 51 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : T olu e n e - d 8 91 45 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : 4 - B r o m o f l u o r o b e n z e n e 94 47 Ma t r i x S p i k e D u p ( 6 1 10 1 6 6 - M S D 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 7 / 1 6 So u r ce : AZ K 0 0 4 2 - 0 7 Be n z e n e ug / L 58 50 . 0 0 0 0. 0 9 67 - 1 3 4 11 6 7 Ch l o r o b e n z e n e ug / L 56 50 . 0 0 0 0. 0 13 69 - 1 2 2 11 3 8 1, 1 - D i c h l o r o e t h e n e ug / L 78 50 . 0 0 0 0. 0 9 QM-05 58 - 1 4 2 15 6 8 T olu e n e ug / L 54 50 . 0 0 0 0. 0 9 68 - 1 2 7 10 8 7 Page 57 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Re s u l t Li m i t Re p o r t i n g Un i t s Le v e l Sp i k e Re s u l t So u r c e %R E C %R E C Li m i t s RP D RPD Limit Qual An a l y t e V ol a t i l e O r g a n i c C o m p o u n d s b y E P A 8 2 6 0 - Q u a l i t y C o n t r o l Ba t c h 6 1 10 1 6 6 - E P A 5 0 3 0 B Ma t r i x S p i k e D u p ( 6 1 10 1 6 6 - M S D 1 ) Pr e p a r e d & An a l y z e d : 1 1/ 0 7 / 1 6 So u r ce : AZ K 0 0 4 2 - 0 7 T ri c h l o r o e t h e n e ug / L 53 50 . 0 0 0 0. 0 11 72 - 1 3 2 10 6 6 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : D i b r o m o f l u o r o m e t h a n e 98 49 ug / L 50 . 0 0 0 78 - 1 2 0 Su r r : 1 , 2 - D i c h l o r o e t h a n e - d 4 10 3 52 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : T olu e n e - d 8 90 45 ug / L 50 . 0 0 0 80 - 1 2 0 Su r r : 4 - B r o m o f l u o r o b e n z e n e 93 46 Page 58 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 La b o r a t o r y C e r t i f i c a t i o n s Co d e De s c r i p t i o n Nu m b e r Expires 81 2 Ge o r g i a D W I n o r g a n i c s E f f: 0 7 / 0 1 / 2 0 1 6 06/30/2017 GA D W 81 2 Ge o r g i a D W M i c r o b i o l o g y E f f: 0 7 / 0 1 / 2 0 1 5 12/09/2016 GA D W M 38 1 No r t h C a r o l i n a 12/31/2016 NC E8 7 3 1 5 F L D O H ( N o n - P o t . W at e r , S o l i d s ) E f f: : 0 7 / 0 1 / 2 0 1 6 06/30/2017 NE L A C E8 7 3 1 5 F L D O H N E L A C ( D r i n k i n g W at e r ) E f f: 0 7 / 0 1 / 2 0 1 6 06/30/2017 NE L D W 98 0 11 0 0 1 So u t h C a r o l i n a 06/30/2017 SC T1 0 4 7 0 4 3 9 7 - 0 8 - T X T ex a s 03/31/2017 TX 13 4 0 V ir g i n i a 12/14/2016 VA Page 59 of 61 En v i r o n m e n t a l M o n i t o r i n g & La b o r a t o r y An a l y s i s 1 10 T ec h n o l o g y P a r k w a y , P e a c h t r e e C o r n e r s , G A 30 0 9 2 (7 7 0 ) 7 3 4 - 4 2 0 0 F AX (7 7 0 ) 7 3 4 - 4 2 0 1 P AC E AN A L YT I C A L S E R VI C E S , I N C . Ca m p D r e s s e r & M c K e e I n c . - R a l e i g h 54 0 0 G l e n w o o d A ve . , S u i t e 3 0 0 Ra l e i g h N C , 2 7 6 1 2 At t e n t i o n : M r . M a t C o l o n e November 30, 2016 Le g e n d De f i n a t i o n o f L a b o r a t o r y T er m s - N o t D e t e c t e d a t l e v e l s g r e a t e r t h a n o r e q u a l t o S W S L / R L ND SW S L / R L MD L - NC D E N R S o l i d W as t e S e c t i o n L I m i t /R e p o r t i n g L i m i t ( A d j u s t e d f o r D F / P r e p F a c t o r ) - M e t h o d D e t e c t i o n L i m i t Qu a l i f i e r s - D i l u t i o n F a c t o r DF QR - 0 3 Th e R P D v a l u e f o r t h e s a m p l e d u p l i c a t e o r M S / M S D w a s o u t s i d e o f Q C a c c e p t a n c e l i m i t s d u e t o s u s p e c t e d m a t r i x i n t e r f e r e n c e a n d / o r n o n - h o m o g e n e o u s s a m p l e ma t r i x . QM - 0 5 Th e s p i k e r e c o v e r y w a s o u t s i d e a c c e p t a n c e l i m i t s f o r t h e M S a n d / o r M S D a n d / o r P D S d u e t o s u s p e c t e d m a t r i x i n t e r f e r e n c e . S a m p l e r e s u l t s f o r t h e Q C b a t c h we r e a c c e p t e d b a s e d o n a c c e p t a b l e L C S r e c o v e r i e s . QM - 0 2 Th e s p i k e r e c o v e r y i s o u t s i d e a c c e p t a n c e l i m i t s d u e t o i n s i g n i f i c a n t s p i k e a m o u n t a s c o m p a r e d t o s a m p l e c o n c e n t r a t i o n . J Es t i m a t e d v a l u e l e s s t h a n R e p o r t i n g L i m i t ( R L ) b u t g r e a t e r t h a n M e t h o d D e t e c t i o n L i m i t ( M D L ) ( C L P J - F l a g ) . H- 0 2 Sa m p l e w a s p r e p a r e d a n d / o r a n a l y z e d o u t s i d e o f t h e E PA r e c o m m e n d e d h o l d i n g t i m e . S e e C a s e N a r r a t i v e . > Gr e a t e r t h a n t h e r e s u l t v a l u e r e p o r t e d . No t e : U n l e s s o t h e r w i s e n o t e d , a l l r e s u l t s a r e r e p o r t e d o n a n a s r e c e i v e d b a s i s . Page 60 of 61 cdmsmith.com