0201_AlexanderCDLFoverMSWLF_WQMR1068003

Alexander County Active C&D and Closed MSWLF
Taylorsville, North Carolina
December 2016
MESCO Project Number: G17003.0
Semi-Annual Water Quality Monitoring Report
with Corrective Action Update
Prepared for
Municipal Engineering Services Company, P.A.Garner and Boone, North Carolina
Permit Number: 02-01
P.O. Box 97
Garner, NC 27529
P.E. License No. C-0281

TABLE OF CONTENTS
SECTION
Introduction Page 1
Background Page 1
Sampling Procedures Page 2
Field Parameter Data Page 2
Laboratory Results Page 3
Quality Control Samples Page 3
Groundwater Samples Page 3
Surface Water Samples Page 4
Groundwater and Surface Water Characterization Page 4
Corrective Action Update Page 5
MNA Analysis (AOCs MW-16, MW-24, MW-26) Page 5
Phytoremediation (AOC MW-24) Page 5
Enhanced Bioremediation via Substrate Injection (AOC MW-26) Page 5
Landfill Gas Extraction (AOC MW-1B) Page 6
Findings Page 6
Closing Page 7
FIGURES
VOC 2L Exceedance Comparison Histograms Figure 1
Phytoremediation Summary Figure 2
Total VOCs and Benzene Concentrations Pre/Post Injection Comparison in AOC MW-26 Figure 3
Dissolved Methane Concentrations Histograms Figure 4
Total VOC Concentrations Histograms Figure 5
SHEETS
Topographic Map with Site Location Sheet 1
Potentiometric Map of Uppermost Aquifer w/ VOCs Detected Above 2L Standards Sheet 2
TABLES
Groundwater Monitoring Well Construction Table Table 1
Field Observations of Monitoring Locations Table 2
Field Parameter Data Summary Table 3
Sampling and Analysis Summary Table 4
Groundwater & QC Detections Table 5
Surface Water Detections Table 6
Hydrologic Properties at Monitoring Well Locations Table 7
MNA Parameter Data Summary Table 8
APPENDICIES
Laboratory Analysis Report and Chains of Custody Appendix A
Field Sampling Parameter Data Sheet(s) Appendix B
Sheets
Topographic Map with Site Location
SHEET 1
QUADRANGLE LEGEND
Alexander County Active C&D and Closed MSWLF
1/20 1 MILE
LANDFILL PROPERTY
N
2500 Paynes Dairy Road
Taylorsville, NC 28681
Lat:35-15-18.7246
Long:-81-08-51.51.32
Northing:767009.09
Easting:1363506.43
IW-1MW-24
MW-25
MW-26
MW-27
MW-21
MW-23
MW-20
MW-22
MW-5
Benzene 2.5 ug/l
MW-1
Benzene - 1.1 ug/l
MW-16
Benzene - 2.3 ug/l
1,1-Dichloroethane - 8.0 ug/l1,2-Dichloropropane - 0.83(j)
MW-31,4-Dichlorobenzene - 10.4 ug/lBenzene - 5.3 ug/l
MW-11Benzene - 2.8 ug/l1,4-Dichlorobenzene - 8.4 ug/l
MW-12
1,4-Dichlorobenzene - 8.7 ug/l
MW-7
Benzene - 3.2 ug/l
1,2-Dichloroethane - 0.47(j)
MW-6Benzene - 1.1 ug/
December 29-31, 2016
WELL #
15A NCAC 2L Groundwater Quality Standard 1.0 6.0 6.0 0.6 0.4
MW-1B
MW-1 1080.54 35.96 1044.58 1.1MW-1A 1085.32 >47.34 <1037.98
MW-1B 1082.56 44.77 1037.79
MW-18 1084.33 52.85 1031.48MW-19 1071.48 52.33 1019.15
MW-16
MW-5 1051.26 43.03 1008.23 2.5
MW-10 1040.80 36.21 1004.59
MW-16 1037.56 31.80 1005.76 2.3 8.0 0.83 (j)
MW-32 1025.26 32.55 992.71
MW-33 1007.40 14.25 993.15
MW-34 1014.60 9.14 1005.46
MW-24
MW-7 1009.24 40.60 968.64 3.2 0.42 (j)
MW-12 1007.35 55.79 951.56 8.7
MW-12D*1008.46 64.00 944.46
MW-24 974.04 33.62 940.42
MW-25 981.93 34.15 947.78
MW-26
MW-3 1024.73 25.72 999.01 5.3 10.4
MW-11 1011.96 43.11 968.85 2.8 8.4
MW-26 990.69 34.18 956.51 2.1 8.2MW-27 992.19 26.79 965.40
MW-31 985.42 30.21 955.21
MW-2 1004.48 >30.45 <974.03MW-4R 1012.64 16.91 995.73 1.3
MW-6 1010.79 35.35 975.44 1.1
MW-9 996.27 12.22 984.05
MW-13 1004.56 47.27 957.29
MW-14 997.44 41.81 955.63
MW-15 1023.44 25.70 997.74 2.6
MW-17 991.16 20.90 970.26
MW-20 1046.92 40.92 1006.00
MW-21 990.00 36.25 953.75
MW-22 958.97 16.35 942.62
MW-23 950.48 19.61 930.87
* = Deep well(s) not used for groundwater contouring
M ³M´4XDOLILHGFRQFHQWUDWLRQ6:6/FRQVLGHUHGDQHVWLPDWH
Groundwater Levels & VOCs Detected Above 2L Standards
AREA OF CONCERN
per CAP
TOP OF CASING
ELEVATION (FT AMSL)
DEPTH TO WATER (FT
BTOC)
GROUNDWATER POTENTIOMETRIC
ELEVATION (FT AMSL)
BENZENE (UG/L)
1,4-DCB
(UG/L)
1,1-DCA (UG/L)
1,2-DCP
(UG/L)
1,2-DCA
(UG/L)
Figures
Figure 1
VOC 2L Exceedance Comparisons Histograms
Dec-16 Max Dec-16 Max Dec-16 Max Dec-16 Max Dec-16 Max Dec-16 Max Dec-16 Max Dec-16 Max Dec-16 Max Dec-16 Max Dec-16 Max
Benzene 1 1.1 7.1 5.3 13 1.3 5.6 2.5 6.1 1.1 1.1 3.2 6.7 2.8 7.8 2.6 5.3 2.3 4.9 2.1 3.2
Tetrachloroethylene 0.7 1.2 2.9
1,1-Dichloroethane 6 8 12.4
1,2-Dichloroethane 0.4 0.42 0.42
1,4-Dichlorobenzene 6 10.4 10.6 8.4 11.6 8.7 10.9 8.2 8.2
1,2-Dichloropropane 0.6 1.1
Max=Highest ever reported (1995 through Dec. 2016)
MW-11 MW-12 MW-15 MW-16 MW-26MW-7Parameter Name 2L Std. MW-1 MW-3 MW-4R MW-5 MW-6
0
2
4
6
8
10
12
14
0
2
4
6
8
10
12
14 MW-1 MW-3 MW-4R MW-5 MW-6 MW-7 MW-11 MW-12 MW-15 MW-16 MW-26 ug/L ug/L VOCs >2L Std (Dec 2016 & Max)
BENZENE Max PCE Max 1,1-DCA Max 1,2-DCA Max 1,4-DCB Max 1,2-DCP Max
BENZENE Dec-2016 PCE Dec-2016 1,1-DCA Dec-2016 1,2-DCA Dec-2016 1,4-DCB Dec-2016 1,2-DCP Dec-2016
Alexander County Active CDLF and Closed MSWLF Page 1 of 1
Figure 2
Phytoremediation Summary
8/27/2010
8/28/2010
8/29/2010
8/30/2010
8/31/2010
9/1/2010
9/2/2010
9/3/20109/4/20109/5/2010
9/6/2010
9/7/2010
9/8/2010
9/9/2010
9/10/2010
9/11/2010
9/12/2010
9/13/2010
9/14/2010
9/15/2010
9/16/2010
9/17/2010
9/18/2010
9/19/2010
9/20/2010
9/21/2010
9/22/2010
9/23/2010
9/24/20109/25/2010
9/26/2010
9/27/2010
Data Sources:
GW = Dedicated pressure transducers measurements recorded daily top graph. Manual measurements semi-annually bottom graph.
Precipitation = National Weather Services Cooperative Observer Program Station 318519. Measurements recorded daily.
Tree Size = Field measurements (Height + width + trunk circumference) of 10 designated sample trees. Measurements recorded quarterly.
945
950
955
960
965
970
975
0
5
10
15
20
25
30
35
8/12/2010 8/12/2011 8/12/2012 8/12/2013 8/12/2014 8/12/2015 8/12/2016 (ftamsl) (inches) Date
DAILY GROUNDWATER, PRECIPITATION & TREE GROWTH
Precipitation (Inches) Average Tree Size (in/10) MW-7 MW-12
940
945
950
955
960
965
970
975
980 Jan-95 Jan-96 Jan-97 Jan-98 Jan-99 Jan-00 Jan-01 Jan-02 Jan-03 Jan-04 Jan-05 Jan-06 Jan-07 Jan-08 Jan-09 Jan-10 Jan-11 Jan-12 Jan-13 Jan-14 Jan-15 Jan-16 Jan-17 (ftamsl) Date
SEMI-ANNUAL GROUNDWATER ELEVATIONS
MW-24 MW-25 MW-7 MW-12 MW-12D
Alexander County Active CDLF and Closed MSWLF Page 1 of 1
Alexander County Active CDLF and Closed MSWLF Page 1 of 1
Figure 3
June 30, 2009 – December 31, 2016
Well ID Benzene Benzene Benzene Benzene Benzene Benzene
Up MW-3 61.66 8.10 43.03 7.20 31.50 6.00 37.04 6.10 43.31 6.85 25.72 5.30 -17.59 -1.55 -41 -23
Up MW-11 53.28 5.00 46.25 4.50 40.81 5.90 43.20 4.20 45.89 4.90 43.11 2.80 -2.78 -2.10 -6 -43
Up MW-27 23.70 0.00 20.20 0.00 24.60 0.00 28.00 0.00 24.13 0.00 26.79 0.00 2.67 0.00 11 0
138.64 13.10 109.48 11.70 96.91 11.90 108.24 10.30 113.32 11.75 95.62 8.10 -17.70 -3.65 -16 -31
Down MW-26 39.40 1.40 20.00 1.40 39.50 3.20 29.00 1.60 31.98 1.90 34.18 2.10 2.21 0.20 7 11
Down MW-31 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0 0
39.40 1.40 20.00 1.40 39.50 3.20 29.00 1.60 31.98 1.90 34.18 2.10 2.21 0.20 7 11
Up&Down Gradient Total 178.04 14.50 129.48 13.10 136.41 15.10 137.24 11.90 145.29 13.65 129.80 10.20 -15.49 -3.45 -11 -25
Total VOCs and Benzene Concentrations Pre/Post Injection Comparison in AOC MW-26
Total VOCs & Benzene Concentrations Pre/Post Injection Comparison in AOC MW-26
Hydraulic
Gradient In
Relation to
Injection
Well (IW-1)
June 2009 (ug/L)Dec. 2009 (ug/L)July 2010 (ug/L)Dec. 2010 (ug/L)
Average of Four Events Preceding Injection (ug/L)Dec. 2016 (ug/L)
Difference Between Current and Baseline (ug/L)
Difference Between Current and Baseline (%)
All
VOCs
All
VOCs
All
VOCs
Benzen
e
All
VOCs
Benzen
e All VOCs
All
VOCs
All
VOCs
All
VOCs
Subtotal Upgradient
Subtotal Downgradient
2L
2/17/20112/17/2011Bac-9 InjectedBac-9 Injected
Alexander County Active CDLF and Closed MSWLF Page 1 of 1
Figure 4
Histograms of Dissolved Methane Concentrations
AOC ID WELL ID
DISSOLVED DISSOLVED DISSOLVED DISSOLVED DISSOLVED DISSOLVED DISSOLVED
METHANE METHANE METHANE METHANE METHANE METHANE METHANE REDUCTION
Post-Start Up Post-Start Up Post-Start Up Post-Start Up Post-Start Up Post-Start Up SINCE
06/15/12 06/27/13 06/26/14 06/16/15 01/06/16 07/05/16 12/29/16 START-UP
(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(mg/L)(%)
MW-1B
MW-1 6.78 0.08 0.00153 0.07580 0.0332 0.0903 0.1100 -98
MW-1A NS NS NS NS NS NS NS NA
MW-1B 1.90 0.69 ND<0.0004 0.099 0.0511 0.3430 0.3340 -82
MW-18 NS NS NS NS NS NS NS NA
MW-19 NS NS NS NS NS NS NS NA
AOC AVG 4.34 0.39 0.0009 0.0873 0.0422 0.2167 0.2220 -95
NS = Not sampled since not impacted
Pre-LFGCCS (June 15, 2012) Compared to Post-LFGGCCS (Dec 29, 2016)
Pre-Start Up
JUNE 2012 (Pre)JUNE 2013 (Post)JUNE 2014 (Post)DEC 2014 (Post)JUNE 2015 (Post)JAN 2016 (Post)JULY 2016 (Post)DEC 2016 (Post)
0
1
2
3
4
5
6
7
8
DISSOLVED METHANE IN GROUNDWATER
MW-1
MW-1Bmg/LExtraction Started NOV. 2012
Alexander County Active CDLF and Closed MSWLF Page 1 of 1
Figure 5
Total VOC Concentrations Histograms
Baseline (June 24, 2009-December 9, 2010) Compared to December 2016
AOC ID WELL ID
MW-1B
MW-1 27.86 6.49 -21.37 -77
MW-1A NS NS NA NA
MW-1B 17.31 7.02 -10.29 -59
MW-18 0.00 0.00 0.00 0
MW-19 3.48 0.00 -3.48 -100
AOC AVG 12.16 3.38 -8.79 -72
MW-16
MW-5 19.84 24.36 4.52 23
MW-10 3.24 0.23 -3.01 -93
MW-16 45.06 41.02 -4.04 -9
MW-32 0.00 0.00 0.00 0MW-33 4.40 7.09 2.69 61MW-34 0.30 0.00 -0.30 0
AOC AVG 12.14 12.12 -0.02 7
MW-24
MW-6 0.00 3.38 3.38 100
MW-7 15.27 17.23 1.96 13
MW-12 34.39 26.92 -7.47 -22
MW-12D 1.00 1.22 0.22 22
MW-13 1.59 0.17 -1.42 -89
MW-24 3.18 0.00 -3.18 -100
MW-25 0.00 4.86 4.86 100
AOC AVG 7.92 7.68 -0.24 -3
MW-26
MW-3 45.47 28.32 -17.15 -38
MW-11 47.84 30.91 -16.93 -35
MW-26 32.41 34.21 1.80 6
MW-27 24.32 12.60 -11.72 -48
MW-31 1.15 0.71 -0.44 -38
AOC AVG 30.24 21.35 -8.89 -29
30.99 3.06 0.00 -90
MW-4R 26.73 24.31 -2.42 -9
MW-9 19.55 10.30 -9.25 -47
MW-14 17.81 11.28 -6.53 -37
MW-15 13.38 13.42 0.04 0
MW-17 10.55 5.07 -5.48 -52
MW-20 0.69 0.81 0.12 17
MW-21 0.77 5.06 4.29 557
MW-22 2.70 0.00 -2.70 -100
MW-23 0.68 2.06 1.38 203AOC AVG 12.39 7.54 -4.85 -39ALL WELLS ALL WELLS AVG 14.58 10.28 -4.30 -29
NS = Not sampled since dry
TOTAL VOC(s) BASELINE
AVERAGE
(June 2009-
Dec. 2010)
(ug/l)
TOTAL VOC(s)
LATEST
Dec 2016
(ug/l)
DIFFERENCE BETWEEN
LATEST AND
BASELINE (ug/L)
DIFFERENCE BETWEEN
LATEST AND
BASELINE
(%)

STATISTICAL
TREND*
Between June
2009 – Dec
2016
DownwardNo TrendDownwardNo TrendNo TrendDownwardNo TrendNo TrendNo TrendNo TrendNo TrendNo Trend
No TrendNo Trend
No TrendDownwardNo TrendNo TrendNo TrendNo TrendNo TrendDownwardDownwardNo TrendDownwardNo TrendDownward
Undesignated
(No
Remediation)
MW-2 7/16 No TrendDownwardDownwardNo TrendNo TrendNo TrendNo TrendNo TrendNo TrendNo TrendDownwardDownward
* = Statistical trend analysis of all events between June 2009 and July 2016 via Sen's Slope Estimator at both a 90% or 95% Confidence Level
7/16 = MW-2 dry in December 2016 so July 2016 results shown
MW-1B MW-16 MW-26 MW-24 UNDESIGNATED SITEWIDE
0
5
10
15
20
25
30
35
TOTAL VOC(s) BASELINE AVERAGE COMPARED TO DECEMBER 2016
BASELINE AVERAGE
DEC 2016AREA OF CONCERNug/LNot updated for
dec 2017 event
Table
Table 1
Groundwater Monitoring Well Construction Table
December 29-31, 2016
Well
Diameter
Total
Well
Depth
Top of
Screen
Depth
Screen
Length
Top of
Casing
Elevation
Ground
Elevation
Groundwater
Elevation
Depth to
Water
(inches)(ft bgs)(ft bgs)(ft)(ft amsl)(ft amsl)(ft amsl)(ft btoc)
MW-1 9/14/90 2 40.00 25.00 15 Soil & Rock 1080.54 1077.98 1044.58 35.96 35.8389 -81.1478
MW-1A 9/30/94 2 47.50 32.50 15 Soil & Rock 1085.32 1083.28 <1035.78 Dry (>49.54)35.8389 -81.1478
MW-1B 5/21/03 2 61.00 46.00 15 Rock 1082.56 1079.56 1041.01 41.55 35.8391 -81.1478
MW-2 9/6/90 2 30.00 15.00 15 Soil 1004.48 1002.28 <974.03 30.45 35.8376 -81.1524
MW-3 9/19/90 2 33.00 13.00 20 Soil & Rock 1024.73 1024.23 999.01 25.72 35.8365 -81.1503
MW-4R 9/30/94 2 20.50 5.50 15 Soil & Rock 1012.64 1008.54 995.73 16.91 35.8366 -81.1479
MW-5 9/16/94 2 48.80 33.80 15 Soil & Rock 1051.26 1049.01 1008.23 43.03 35.8373 -81.1465
MW-6 9/29/94 2 41.00 26.00 15 Rock 1010.79 1008.29 975.44 35.35 35.8369 -81.1364
MW-7 9/29/94 2 53.00 38.00 15 Rock 1009.24 1005.84 968.64 40.60 35.8364 -81.1522
MW-9 10/24/00 2 31.50 16.50 15 Rock 996.27 993.76 984.05 12.22 35.8361 -81.1481
MW-10 10/25/00 2 91.00 76.00 15 Rock 1040.80 1037.83 1004.59 36.21 35.8366 -81.1469
MW-11 10/24/00 2 56.00 41.00 15 Rock 1011.96 1008.98 968.85 43.11 35.8359 -81.1505
MW-12 10/23/00 2 66.50 51.50 15 Soil 1007.35 1004.46 951.56 55.79 35.3577 -81.1525
MW-12D 6/9/00 2 100.00 90.00 10 Rock 1008.46 1006.03 944.46 64.00 35.3577 -81.1525
MW-13 10/25/00 2 60.50 45.50 15 Rock 1004.56 1001.63 957.29 47.27 35.8368 -81.1532
MW-14 10/26/00 2 40.50 25.50 15 Soil & Rock 997.44 994.06 955.63 41.81 35.8376 -81.1525
MW-15 10/25/00 2 35.00 20.00 15 Soil & Rock 1023.44 1020.81 997.74 25.70 35.8385 -81.1508
MW-16 12/20/07 2 40.25 25.25 15 Rock 1037.56 1034.94 1005.76 31.80 35.8371 -81.1465
MW-17 6/10/03 2 22.30 7.30 15 Rock 991.16 988.36 970.26 20.90 35.8386 -81.1511
MW-18 12/19/07 2 56.70 41.70 15 Rock 1084.33 1081.52 1031.48 52.85 35.8392 -81.1467
MW-19 12/20/07 2 63.92 48.92 15 Rock 1071.48 1068.67 1019.15 52.33 35.8391 -81.1487
MW-20 12/20/07 2 63.55 48.55 15 Rock 1046.92 1044.19 1006.00 40.92 35.8391 -81.1502
MW-21 12/19/07 2 41.05 26.05 15 Rock 990.00 987.08 953.75 36.25 35.8386 -81.1514
MW-22 12/19/07 2 18.12 8.12 10 Rock 958.97 956.21 942.62 16.35 35.8381 -81.1524
MW-23 12/19/07 2 21.54 6.54 15 Soil 950.48 947.83 930.87 19.61 35.8376 -81.1529
MW-24 12/20/07 2 35.35 20.35 15 Soil 974.04 971.29 940.42 33.62 35.8356 -81.1533
MW-25 12/19/07 2 44.48 29.48 15 Rock 981.93 979.93 947.78 34.15 35.8353 -81.1528
MW-26 12/20/07 2 49.80 34.80 15 Rock 990.69 988.08 956.51 34.18 35.8354 -81.1504
MW-27 12/20/07 2 49.82 34.82 15 Rock 992.19 989.19 965.40 26.79 35.8356 -81.1493
MW-31 8/16/10 2 32.56 17.56 15 Soil 985.42 982.42 955.21 30.21 35.8348 -81.1506
MW-32 8/16/10 2 42.70 27.7 15 Rock 1025.256 1022.26 992.71 32.55 35.8361 -81.1469
MW-33 4/27/13 2 21.38 6.38 15 PWR 1007.40 1004.40 993.15 14.25 35.8367 -81.1462
MW-34 4/27/13 2 21.19 6.19 15 PWR 1014.60 1011.60 1005.46 9.14 35.8373 -81.1459
IW-1 2/14/11 4 52.44 37.44 15 Rock 990.44 987.44 NR NR 35.8356 -81.1504
NOTE:
bgs = below ground surface
amsl= above mean sea level
btoc = below top of casing (PVC well casing)
PWR = partially weathered rock
Monitoring
Well
Date
Installed
Geology of
Screened
Interval Latitude Longitude
Alexander County Active CDLF and Closed MSWLF Page 1 of 1
Table 2
Field Observations of Monitoring Locations
December 29-31, 2016
Sample
Location
Viable
Monitoring
Location
Lack of Any
Evidence of
Tampering
Locked Hinge/Hasp
Operational
Tagged
or
Labeled
Concrete
Surface
Pad
Effective
Comments
MW-1 Yes Yes Yes Yes Yes ?Pad Slightly Cracked
MW-1A No Yes Yes Yes Yes Yes Dry which is typical
MW-1B Yes Yes Yes Yes Yes Yes
MW-2 No Dry Yes Yes Yes Yes ?Surface pad covered with soil
MW-3 Yes Yes Yes Yes Yes Yes Slow recharge
MW-4R Yes Yes Yes Yes Yes Yes Purge water has sulfur smell.
MW-5 Yes Yes Yes Yes Yes Yes Needs MNA tubing
MW-6 Yes Yes Yes Yes Yes Yes
MW-7 Yes Yes Yes Yes Yes ?Pad Cracked
MW-9 Yes Yes Yes Yes Yes Yes
MW-10 Yes Yes Yes Yes Yes Yes Purge water has sulfur smell. Very slow recharge
MW-11 Yes Yes Yes Yes Yes Yes
MW-12 Yes Yes Yes Yes Yes ?Pad Slightly Cracked
MW-12D Yes Yes Yes Yes Yes Yes
MW-13 Yes Yes Yes Yes Yes Yes
MW-14 Yes Yes Yes Yes Yes ?Surface pad cracked
MW-15 Yes Yes Yes Yes Yes Yes
MW-16 Yes Yes Yes Yes Yes ?Surface pad covered with soil
MW-17 Yes Yes Yes Yes Yes Yes
MW-18 Yes Yes Yes Yes Yes Yes
MW-19 Yes Yes Yes Yes Yes Yes
MW-20 Yes Yes Yes Yes Yes Yes
MW-21 Yes Yes Yes Yes Yes Yes
MW-22 Yes Yes Yes Yes Yes Yes
MW-23 Yes Yes Yes Yes Yes Yes
MW-24 Yes Yes Yes Yes Yes Yes
MW-25 Yes Yes Yes Yes Yes Yes
MW-26 Yes Yes Yes Yes Yes Yes
MW-27 Yes Yes Yes Yes Yes Yes
MW-31 Yes Yes Yes Yes Yes Yes
MW-32 Yes Yes Yes Yes Yes Yes
MW-33 Yes Yes Yes Yes Yes Yes
MW-34 Yes Yes Yes Yes Yes Yes Surface pad covered with soil
IW-1 Yes Yes Yes Yes Yes Yes Injection well. Not sampled this event.
SW-3 Yes -----Low gage height and flow rate
SW-4R Yes -----Low gage height and flow rate
SW-5 Yes -----Low gage height and flow rate
SW-6 Yes -----Low gage height and flow rate
Any unusual field conditions, observations, or events:
*MW-5 was damaged by MESCO but repaired by MESCO. Stickup elevation attempted to be maintained but should be re-surveyed for accuracy.
LFG extraction system operating in AOC MW-1B which is typical.
Alexander County Active CDLF and Closed MSWLF Page 1 of 1
Table 3
Field Parameter Data Summary
December 29-31, 2017
Parameter
Water
Depth
Water
Elevation
TOC
Elevation Temp.ORP DO pH
Specific
Conductance TDS
Methane Gas
in Headspace
Turbidity of
Metal Sample
Units ft (btoc)ft (amsl)ft (amsl) C mV mg/L SU umhos/cm mg/L % Vol.Visual or NTU
MW-1 35.62 1044.92 1080.54 16.4 NR NR 5.7 472 NR NR Clear
MW-1B 42.12 1040.44 1082.56 15.1 NR NR 4.6 76 NR NR Clear
MW-2 >30.45 <974.03 1004.48 NR NR NR NR NR NR NR NR
MW-3 25.72 999.01 1024.73 17.1 NR NR 5.7 438 NR NR Slight
MW-4R 16.91 995.73 1012.64 16.3 83 NR 5.9 446 NR NR Clear
MW-5 43.03 1008.23 1051.26 14.8 -1 0.3 5.9 379 NR NR Slight
MW-6 35.35 975.44 1010.79 14.5 -11 1.1 7.0 231 NR NR Clear
MW-7 40.60 968.64 1009.24 16.1 NR NR 6.0 740 NR NR Clear
MW-9 12.22 984.05 996.27 16.1 NR NR 5.9 581 NR NR NR
MW-10 36.21 1004.59 1040.80 14.7 NR NR 6.7 582 NR NR Clear
MW-11 43.11 968.85 1011.96 16.4 31 0.1 5.6 685 NR NR Clear
MW-12 55.79 951.56 1007.35 15.6 60 0.5 5.4 385 NR NR Clear
MW-12D 64.00 944.46 1008.46 14.2 62 0.7 7.3 884 NR NR Clear
MW-13 47.27 957.29 1004.56 14.0 NR NR 5.4 250 NR NR Clear
MW-14 41.81 955.63 997.44 13.6 NR NR 5.9 369 NR NR Slight
MW-15 25.70 997.74 1023.44 15.4 NR NR 5.3 385 NR NR Clear
MW-16 31.80 1005.76 1037.56 14.7 299 0.5 5.6 149 NR NR Clear
MW-17 20.90 970.26 991.16 14.9 NR NR 5.2 138 NR NR Slight
MW-18 52.85 1031.48 1084.33 14.6 313 2.1 5.0 27 NR NR Clear
MW-19 52.33 1019.15 1071.48 14.3 NR NR 6.2 464 NR NR Clear
MW-20 40.92 1006.00 1046.92 14.0 NR NR 5.4 69 NR NR Clear
MW-21 36.25 953.75 990.00 14.1 NR NR 4.7 92 NR NR Clear
MW-22 16.35 942.62 958.97 14.6 NR NR 6.6 46 NR NR Clear
MW-23 19.61 930.87 950.48 14.3 NR NR 5.1 103 NR NR Slight
MW-24 33.62 940.42 974.04 14.1 291 0.3 5.7 168 NR NR Clear
MW-25 34.15 947.78 981.93 13.8 NR NR 5.7 194 NR NR Clear
MW-26 34.18 956.51 990.69 16.1 65 1.1 5.8 762 NR NR Clear
MW-27 26.79 965.40 992.19 15.5 86 2.8 6.4 454 NR NR Clear
MW-31 30.21 955.21 985.42 15.3 NR NR 5.3 137 NR NR Slight
MW-32 32.55 992.71 1025.256 14.4 144 NR 6.0 156 NR NR Slight
MW-33 14.25 993.15 1007.40 15.4 310 NR 5.3 51 NR NR Slight
MW-34 9.14 1005.46 1014.60 13.9 77 NR 5.6 36 NR NR Slight
Minimum 9.14 930.87 950.48 13.6 -11 0.1 4.6 27 NR NR Clear
Average 33.91 981.07 1014.65 15.0 129 1.0 5.7 321 NR NR Slight
Maximum 64.00 1044.92 1084.33 17.1 313 2.8 7.3 884 NR NR Slight
SW-3 ---8.9 NR NR 6.6 142 NR NR Clear
SW-4R ---4.3 NR NR 6.4 50 NR NR Clear
SW-5 ---5.7 NR NR 6.5 81 NR NR Clear
SW-6 ---8.8 NR NR 6.1 38 NR NR Clear
Minimum ---4.3 NR NR 6.1 38 NR NR Clear
Average ---6.9 NR NR 6.4 78 NR NR Clear
Maximum ---8.9 NR NR 6.6 142 NR NR Clear
NR = No Reading Attempted
Alexander County Active CDLF and Closed MSWLF Page 1 of 1
Table 4
Sampling and Analysis Summary
December 29-31, 2016
App. II
ConstituentVOCsTotal MetalsMercury (Total)VFAHydrogenMethane, DissolvedEthene/EthaneCarbon DioxideAlkalinitySulfateSulfideChlorideTOCCODBODIron, DissolvedNitrateMW-1 x x x x
MW-1A
MW-1B x x x x
MW-2
MW-3 x x x x x x x
MW-4R x x
MW-5 x x x x
MW-6 x x x x x
MW-7 x x
MW-9 x x
MW-10 x x
MW-11 x x x x x x x x x x x x x
MW-12 x x x x x x x x x x x x x
MW-12D x x x x x x x x x x x x x
MW-13 x x
MW-14 x x
MW-15 x x x
MW-16 x x x x
MW-17 x x x
MW-18 x x x x x
MW-19 x x
MW-20 x x
MW-21 x x x
MW-22 x x
MW-23 x x
MW-24 x x x x x x x x x x x x
MW-25 x x x
MW-26 x x x x x x x x x x x
MW-27 x x x
MW-31 x x x x x x x x x x x
MW-32 x x
MW-33 x x
MW-34 x x
SW-3 x x
SW-4R x x
SW-5 x x
SW-6 x x
EB x x
TB x
App. I MNA
Dry so not sampled which is typical
App I & II = Appendix I Listed in current 40 CFR 258
Dry so not sampled which is atypical
Alexander County Active CDLF and Closed MSWLF Page 1 of 1
Table 5
Groundwater Detections
December 29-31, 2016
MW-1 MW-1B MW-3 MW-4R MW-5 MW-6 MW-7 MW-9 MW-11 MW-12 MW-12D MW-13 MW-14 MW-15 MW-16 MW-17 MW-18 MW-19 MW-20 MW-21 MW-22 MW-23 MW-24 MW-25 MW-26 MW-27 MW-31 MW-32 MW-33 MW-34 TB EBSSSSSSSSSSSSSSSSBGSSSSSSSSSSSSSQCQC
Antimony, total 3.8 6 1 6 ----
Arsenic, total 2.5 10 10 10 --5.3 J 4.8 J 3 J 5.5 J 4.2 J 2.6 J 4.8 J 3.4 J 7 J 3.3 J 4.1 J --
Barium, total 3.8 100 700 2000 38.9 J 67.8 J --124 55.2 J 88.6 J 4.9 J 170 163 120 13.8 J 15.9 J 12.7 J 54.7 J 58.7 J 75 J 16 J 8.8 J 54.6 J 52.5 J 68 J 52.2 J 49.9 J 15.3 J 51.3 J 63.4 J 121 11.3 J 32.4 J 21.1 J --
Beryllium, total 0.5 1 4 4 --1 --
Cadmium, total 0.5 1 2 5 1.3 --0.73 J 0.6 J --
Chromium, total 2.5 10 10 100 --3.5 J 3 J 8.1 J 2.8 J 3.6 J 3.5 J --
Cobalt, total 2.5 10 1 NE 7.3 J (N)89.5 (N)--93.7 (N)89.4 (N)197 (N)97.3 (N)88 (N)4.3 J (N)5.2 J (N)105 (N)57.5 (N)6 J (N)14.1 (N)64.7 (N)11.8 (N)--
Copper, total 2.5 10 1000 1300 --2.6 J 10.5 81 7.1 J 5.9 J --
Lead, total 2.5 10 15 15 --3.2 J 3.4 J --
Nickel, total 0.5 50 100 NE 4.3 J 7.1 J --5.2 J 18.8 J 69.1 14 J 7.6 J 10.3 J 3.4 J 7 J 7.6 J 2.5 J 4.4 J 2.8 J 3.1 J 3.4 J 18.8 J 22.4 J 4.2 J 2.7 J 9.7 J --
Thallium, total 5 5.5 0.28 2 5.7 (N)5.6 (N)----
Vanadium, total 2.5 25 0.3 NE --4.2 J (N)--
Zinc, total 5 10 1000 NE 31.3 14.3 --19.7 33.8 36 5.7 J 15.6 64.2 38.5 12.4 7.8 J 32 13 10.2 7.2 J 5.8 J 8.4 J 9 J 6.7 J 9.6 J 5 J 7 J 9.2 J --
1,1-Dichloroethane 0.32 5 6 NE 0.46 J 2.3 J 4.6 J 1.7 J 0.53 J 0.4 J 1.3 J 0.95 J 8 (L)0.81 J 0.4 J 0.81 J 0.61 J 0.35 J 1.7 J
1,2-Dichlorobenzene 0.3 5 20 NE 0.75 J 0.47 J 0.3 J
1,2-Dichloroethane 0.24 1 0.4 5 0.26 J 0.36 J 0.31 J 0.27 J 0.42 J (L)0.34 J 0.27 J 0.29 J 0.32 J
1,2-Dichloropropane 0.27 1 0.6 5 0.39 J 0.83 J (L)
1,4-Dichlorobenzene 0.33 1 6 75 3.5 3.1 10.4 (L)4.1 2.1 0.96 J 2 0.37 J 8.4 (L)8.7 (L)2.4 0.85 J 2.3 0.49 J 0.5 J 0.34 J 0.48 J 1.7 8.2 (L)0.75 J
Benzene 0.25 1 1 5 1.1 (L)0.43 J 5.3 (L)1.3 (L)2.5 (L)1.1 (L)3.2 (L)2.8 (L)0.73 J 0.43 J 0.26 J 2.6 (L)2.3 (L)0.96 J 0.74 J 0.59 J 2.1 (L)
Carbon disulfide 0.18 100 700 NE
Chlorobenzene 0.18 3 50 100 0.23 J 1.5 J 1.5 J 0.69 J 0.32 J 1.5 J 2 J 2.6 J 0.88 J 0.88 J 0.75 J 0.37 J 0.36 J 2 J 0.24 J
Chloroethane 0.21 10 3000 NE 1.3 J 1.2 J 0.84 J 0.84 J 0.62 J
Chloromethane 0.14 1 3 NE 0.13 J 0.14 J 0.15 J 0.2 J 0.17 J 0.14 J 0.12 J 0.12 J 0.14 J
cis-1,2-Dichloroethene 0.11 5 70 70 1.4 J 1.6 J 5.4 13.5 13.1 1 J 7.6 9.4 16.7 10.6 0.59 J 6.9 7.3 23.3 2.3 J 0.41 J 2.6 J 1.6 J 0.91 J 1.6 J 20.8 12.6 0.71 J 4.4 J
Ethylbenzene 0.97 1 600 70 0.33 J 1.1
Tetrachloroethene 0.97 1 0.7 5 1.2 (L)
Toluene 0.97 1 600 1000 0.35 J
Trichloroethene 0.97 1 3 5 0.56 J 0.71 J 0.68 J 1.3 1.5
Xylene (Total)0.2 5 500 10000 1.1 J 2.6 J
Mercury, total 0.1 0.2 1 2 0.73 ----------------------0.26 0.73 ----0.1 J ----------------------
Red Bold Above Established MCL/2L/GWP Std.
Above Established Federal MCL Drinking Water Std.
MDL = Method Detection Limit, SWSL = Solid Waste Section Limit, 2L/GWP Standard = NC 2L and IMAC Standards adopted by SWS, MCL = Maximum Contaminant Level for Drinking Water
J = "J-qualified". Concentration detected between MDL and SWSL. Considered estimated value
(N) Preliminary source is believed to be Natural originating from erosion of natural deposits. Source not anthropogenic.
(L) Leachate &/or Landfill Gas released from the landfill.
A definitive source of the detections was not determined as part of this report.
BG = Background Well Sample, QC = Quality Control Sample, S = Sentinal Well Sample
Parameter Name MDL SWSL 2L/GWP Std MCL
Metals (Appendix I)
VOCs (Appendix I)
Metals (Appendix II)
Units ug/L, Blank cells means Not Detected, -- means not tested
No regulatory compliance significance.
Alexander County Active CDLF and Closed MSWLF Page 1 of 1
Table 6
Surface Water Detections
December 30-31, 2016
Parameter Name MDL SWSL 2B MCL SW-3 SW-4R SW-5 SW-6
Arsenic, total 2.5 10 10 10 2.6 J 5.4 J
Barium, total 3.8 100 20000 2000 65.5 J 34.9 J 33.8
J
19.1
JCadmium, total 0.5 1 2 5 1.2 0.5 J 0.78
JChromium, total 2.5 10 50 100 4 J 2.9 J
Cobalt, total 2.5 10 270 NE 6.1 J 8 J
Nickel, total 0.5 50 88 NE 4.9 J
Thallium, total 5 5.5 0.47 2 5.6 (N)5.8 (N)
Vanadium, total 2.5 25 NE NE 3.5 J 2.6 J
Zinc, total 5 10 50 NE 7.2 J 6.4 J 7 J
cis-1,2-Dichloroethene 0.1 5 4900 70 0.53 J
Red Bold Above Established MCL/2L/GWP Std.
Above Established Federal MCL Drinking Water Std.
MDL = Method Detection Limit, SWSL = Solid Waste Section Limit, 2B Standard = NC 2B Surface Water Std,
MCL = Maximum Contaminant Level for Drinking Water
J = "J-qualified". Concentration detected between MDL and SWSL. Considered estimated value
(N) Preliminary source is believed to be Natural originating from erosion of natural deposits. Source not anthropogenic.
A definitive source of the detections was not determined as part of this report.
Metals (Appendix I)
VOCs (Appendix I)
Units ug/L, Blank cells means Not Detected, -- means not tested
No regulatory compliance significance.
Alexander County Active CDLF and Closed MSWLF Page 1 of 1
Table 7
Hydrologic Properties at Monitoring Well Locations
December 29-31, 2016
Monitoring
Well
Hydraulic
Conductivity
(cm/sec)
Effective
Porosity
(%)
Hydraulic
Gradient
(ft/ft)
Average Linear
Velocity Rate
(ft/yr)
Flow
Direction
Depth to
Groundwater
(ft btoc)
Groundwater
Potentiometric
Elevation (ft amsl)
Screened Interval
Lithology
MW-2 3.70E-06 28 --N60W >30.45 <974.03 UC
MW-12 n/a 28 0.026 n/a S62W 55.79 951.56 UC
MW-16 8.72E-04 17 0.027 143 S22E 31.80 1005.76 UC
MW-17 n/a 17 0.148 n/a N71W 20.90 970.26 UC
MW-21 3.77E-03 28 0.055 768 N64W 36.25 953.75 UC
MW-22 6.04E-04 28 0.075 167 N76W 16.35 942.62 UC
MW-23 9.83E-04 28 0.046 166 N45W 19.61 930.87 UC
MW-24 1.33E-02 28 0.022 1086 N89W 33.62 940.42 UC
MW-31 n/a 28 0.020 n/a S28W 30.21 955.21 UC
MW-33 n/a 28 0.233 n/a S41E 14.25 993.15 UC
MW-34 n/a 28 0.023 n/a S31E 9.14 1005.46 UC
Minimum 3.70E-006 17 0.020 143 -9.14 930.87 -
Average 3.26E-003 26 0.067 466 -26.79 964.91 -
Maximum 1.33E-002 28 0.233 1086 -55.79 1005.76 -
MW-1 5.60E-05 10 0.233 135 N57W 35.96 1044.58 UC/UBR
MW-3 3.90E-06 10 0.011 0.4 S31W 25.72 999.01 UC/UBR
MW-4R 4.90E-04 10 0.046 235 S05E 16.91 995.73 UC/UBR
MW-5 6.40E-05 28 0.026 6 S22E 43.03 1008.23 UC/UBR
MW-14 n/a 10 0.832 n/a N48W 41.81 955.63 UC/UBR
MW-15 n/a 10 0.029 n/a N56W 25.70 997.74 UC/UBR
Minimum 3.90E-06 10 0.011 0 -16.91 955.63 -
Average 1.53E-04 13 0.196 94 -31.52 1000.15 -
Maximum 4.90E-04 28 0.832 235 -43.03 1044.58 -
MW-1B n/a 10 0.085 n/a N15W 44.77 1037.79 UBR
MW-6 2.40E-05 10 0.436 108 S87W 26.27 975.44 UBR
MW-7 1.60E-06 10 0.067 1 S28W 40.60 968.64 UBR
MW-9 n/a 10 0.132 n/a S27E 12.22 984.05 UBR
MW-11 n/a 10 0.055 n/a S15W 43.11 968.85 UBR
MW-13 n/a 10 0.168 n/a S41W 47.27 957.29 UBR
MW-19 1.92E-06 10 0.019 0 N45W 52.33 1019.15 UBR
MW-20 5.49E-05 10 0.052 30 N70W 40.92 1006.00 UBR
MW-25 5.41E-05 10 0.020 11 S48W 34.15 947.78 UBR
MW-26 1.16E-04 10 0.106 127 S27W 34.18 956.51 UBR
MW-27 2.83E-05 10 0.077 22 S06W 26.79 965.40 UBR
MW-32 n/a 10 0.104 n/a S06E 32.55 992.71 UBR
Minimum 1.60E-06 10 0.019 0 -12.22 947.78 -
Average 4.01E-05 10 0.110 43 -36.26 981.63 -
Maximum 1.16E-04 10 0.436 127 -52.33 1037.79 -
MW-10 n/a 10 0.109 n/a S18W 36.21 1004.59 LBR
MW-12D n/a 10 0.082 n/a S57W 64.00 944.46 LBR
MW-18 1.19E-04 10 0.158 n/a N07W 52.85 1031.48 LBR
Minimum 1.19E-04 10 0.082 --36.21 944.46 -
Average 1.19E-04 10 0.116 --51.02 993.51 -
Maximum 1.19E-04 10 0.158 --64.00 1031.48 -
NOTE:Values for hydraulic conductivity obtained from GAI Consultants Sampling Report (April, 1995) & MESCO ACM Report (2008).
Average Linear Groundwater Velocities calculated only for UC & UBR wells with hydraulic conductivity values.K= hydraulic conductivity
UC = Unconfined/saprolite; UBR = Upper Bedrock fracture system; LBR = Lower Bedrock fracture system.ne = effective porosity
Wells screened in LBR not utilized for flow directions/gradients.dh= head difference
Hydrologic Gradient taken from water elevations recorded between December 29-31, 2016.dl= horizontal distance
Flow rate (Q) calculated via modified Darcy's equation:
dl
dh
n
KQ
e
×-=
Alexander County Active CDLF and Closed MSWLF Page 1 of 1
Table 8
MNA Parameter Data Summary
December 29, 2016
MW-18 MW-3 MW-5 MW-6 MW-7 MW-11 MW-12 MW-12D MW-16 MW-24 MW-25 MW-26 MW-27 MW-31 MW-33 MW-34
12/29/16 12/29/16 12/29/16 12/29/16 12/29/16 12/29/16 12/29/16 12/29/16 12/29/16 12/29/16 12/29/16 12/29/16 12/29/16 12/29/16 12/29/16 12/29/16
VFA – Acetic Acid AM23G NS ug/L NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
VFA – Butyric Acid AM23G NS ug/L NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
VFA – Lactic Acid AM23G NS ug/L NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
VFA – Propionic Acid AM23G NS ug/L NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
VFA – Pyruvic Acid AM23G NS ug/L NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
Hydrogen AM20GAX NS nM NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
Methane RSK175 10 ug/L NS NS NS NS NS NS 3060 3140 NS NS NS NS NS NS NS NS
Ethene AM20GAX NS ug/L NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
Ethane AM20GAX NS ug/L NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
CO2-Dissolved
Field HACH
Kit NS mg/L 20 NS >100 30 NS >100 >100 40 >100 >100 NS >100 >100 NS NS NS
Alkalinity SM 2320B 1000 ug/L NS 93600 NS NS NS 166000 141000 399000 NS NS NS 176000 NS 35300 NS NS
Sulfate EPA 300.0 1000 ug/L NS 1870 J NS NS NS 3230 J 4930 J <1000 U NS NS NS 3280 J NS 2150 J NS NS
Sulfide
SM 4500-
S2D 100 ug/L NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
Chloride
SM 4500-Cl-
E 500 ug/L NS 25300 NS NS NS 78400 13200 69300 NS NS NS 72000 NS 13500 NS NS
TOC SM 5310B 500 ug/L NS 4820 NS NS NS 6070 845 J 3790 NS NS NS 6260 NS 1310 NS NS
COD SM 5220D 12500 ug/L NS 28000 NS NS NS 45000 21000 J 16000 J NS NS NS 37000 NS <12500 U NS NS
BOD SM5210B NS ug/L NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
Iron (total-dissolved)EPA 6010 25 ug/L <25 U NS NS NS NS 39100 38400 498 NS NS NS 7370 NS 177 J NS NS
Nitrate EPA 353.2 10 ug/L NS NS NS NS NS <10 U <10 U <10 U NS NS NS <10 U NS 1480 J NS NS
Temperature
Field
Instrument 0 C 14.6 17.1 14.8 14.5 16.1 16.4 15.6 14.2 14.7 14.1 13.8 16.1 15.5 15.3 15.4 13.9
ORP
Field
Instrument 0 mV 313 NS -1 -11 NS 31 60 67 299 291 NS 65 86 NS 310 77
DO
Field
Instrument 0 mg/L 2.1 NS 0.3 1.1 NS 0.1 0.5 7.0 0.5 0.3 NS 2.6 2.8 NS NS NS
pH
Field
Instrument 0 SU 5 5.70 5.9 7.03 6 5.6 5.4 7.3 5.6 5.7 5.7 5.8 6.4 5.3 5.3 5.6
Sp. Conductance
Field
Instrument 0 us/cm 27 438 379 231 740 685 385 884 149 168 194 762 454 137 51 36
Turbidity
Field
Instrument 0 NTU 21 ST 163 C C 27 12 31 C 19 C 38 41 ST ST ST
Notes:
VFA = Volatile Fatty Acids
MDL* = Lab Method Detection Limit or lowest field measurement possible
< = Not Detected above MDL value
MNA monitoring not required for MW-31 by SWS but recorded per NC Underground Injection Control (UIC) Permit requirement
NS = Not Sampled since not required during this specific event
>100 = CO2 Concentration exceeds maximum capability of method used
j = “J-Qualified” by laboratory indicating value between MDL and Method Reporting Limit (MRL)
Parameters Method MDL*Units
Alexander County Active CDLF and Closed MSWLF Page 1 of 1
Appendix A
Laboratory Analysis Reports
Chains of Custody
#=CL#
January 20, 2017
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92325007
92325007
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
ALEXANDER LF-SWS
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory between December 30,
2016 and January 03, 2017. The results relate only to the samples included in this report. Results
reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's
Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 125
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 125
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Lab ID Sample ID Matrix Date Collected Date Received
92325007001 MW-1 Water 12/29/16 11:50 12/30/16 07:00
92325007002 MW-1B Water 12/29/16 11:48 12/30/16 07:00
92325007003 MW-12 Water 12/29/16 09:10 12/30/16 07:00
92325007004 MW-12D Water 12/29/16 16:30 12/30/16 07:00
92325007005 MW-13 Water 12/29/16 16:00 12/30/16 07:00
92325007006 MW-14 Water 12/29/16 15:00 12/30/16 07:00
92325007007 MW-15 Water 12/29/16 16:45 12/30/16 07:00
92325007008 MW-17 Water 12/29/16 16:50 12/30/16 07:00
92325007009 MW-19 Water 12/29/16 11:55 12/30/16 07:00
92325007010 MW-20 Water 12/29/16 16:30 12/30/16 07:00
92325007011 MW-21 Water 12/29/16 16:40 12/30/16 07:00
92325007012 MW-24 Water 12/29/16 15:20 12/30/16 07:00
92325007013 MW-25 Water 12/29/16 15:35 12/30/16 07:00
92325007014 MW-7 Water 12/29/16 17:10 12/30/16 07:00
92325007015 MW-6 Water 12/29/16 00:00 12/30/16 07:00
92325007016 MW-4R Water 12/30/16 10:50 01/03/17 11:45
92325007017 MW-5 Water 12/30/16 11:35 01/03/17 11:45
92325007018 MW-9 Water 12/30/16 12:05 01/03/17 11:45
92325007019 MW-10 Water 12/31/16 11:00 01/03/17 11:45
92325007020 MW-16 Water 12/31/16 11:45 01/03/17 11:45
92325007021 MW-22 Water 12/31/16 10:30 01/03/17 11:45
92325007022 MW-23 Water 12/31/16 11:20 01/03/17 11:45
92325007023 MW-32 Water 12/31/16 08:35 01/03/17 11:45
92325007024 MW-33 Water 12/30/16 08:30 01/03/17 11:45
92325007025 MW-34 Water 12/30/16 09:00 01/03/17 11:45
92325007026 SW-3 Water 12/30/16 10:00 01/03/17 11:45
92325007027 SW-4R Water 12/31/16 11:05 01/03/17 11:45
92325007028 SW-5 Water 12/30/16 09:25 01/03/17 11:45
92325007029 SW-6 Water 12/30/16 09:40 01/03/17 11:45
92325007030 EB Water 12/31/16 12:00 01/03/17 11:45
92325007031 TB Water 12/31/16 00:00 01/03/17 11:45
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 125
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92325007001 MW-1 RSK 175 Modified 1 PASI-CWDV
EPA 6010 15 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8260 50 PASI-CZDO
92325007002 MW-1B RSK 175 Modified 1 PASI-CWDV
EPA 6010 15 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8260 50 PASI-CZDO
92325007003 MW-12 RSK 175 Modified 1 PASI-CWDV
EPA 6010 15 PASI-ASH1
EPA 6010 1 PASI-ASH1
EPA 8260 50 PASI-CZDO
SM 2320B 1 PASI-AKDF
SM 4500-S2D 1 PASI-AEWS
EPA 300.0 1 PASI-AAES2
EPA 353.2 1 PASI-AWRC
SM 4500-Cl-E 1 PASI-AWRC
SM 5220D 1 PASI-AEWS
SM 5310B 1 PASI-AMDW
92325007004 MW-12D RSK 175 Modified 1 PASI-CWDV
EPA 6010 15 PASI-ASH1
EPA 6010 1 PASI-ASH1
EPA 8260 50 PASI-CZDO
SM 2320B 1 PASI-AKDF
SM 4500-S2D 1 PASI-AEWS
EPA 300.0 1 PASI-AAES2
EPA 353.2 1 PASI-AWRC
SM 4500-Cl-E 1 PASI-AWRC
SM 5220D 1 PASI-AEWS
SM 5310B 1 PASI-AMDW
92325007005 MW-13 EPA 6010 15 PASI-ASER
EPA 8260 50 PASI-CZDO
92325007006 MW-14 EPA 6010 15 PASI-ASER
EPA 8260 50 PASI-CZDO
92325007007 MW-15 EPA 6010 15 PASI-ASER
EPA 7470 1 PASI-AWAB
EPA 8260 50 PASI-CZDO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 125
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92325007008 MW-17 EPA 6010 15 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8260 50 PASI-CZDO
92325007009 MW-19 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CZDO
92325007010 MW-20 EPA 6010 15 PASI-ASER
EPA 8260 50 PASI-CZDO
92325007011 MW-21 EPA 6010 15 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8260 50 PASI-CZDO
92325007012 MW-24 RSK 175 Modified 1 PASI-CWDV
EPA 6010 15 PASI-ASER
EPA 6010 1 PASI-ASH1
EPA 8260 50 PASI-CZDO
SM 2320B 1 PASI-AKDF
SM 4500-S2D 1 PASI-AEWS
EPA 300.0 1 PASI-AAES2
EPA 353.2 1 PASI-AWRC
SM 4500-Cl-E 1 PASI-AWRC
SM 5220D 1 PASI-AEWS
SM 5310B 1 PASI-AMDW
92325007013 MW-25 RSK 175 Modified 1 PASI-CWDV
EPA 6010 15 PASI-ASER
EPA 8260 50 PASI-CZDO
92325007014 MW-7 EPA 6010 15 PASI-ASER
EPA 8260 50 PASI-CZDO
92325007015 MW-6 RSK 175 Modified 1 PASI-CWDV
EPA 6010 15 PASI-ASER
EPA 7470 1 PASI-AWAB
EPA 8260 50 PASI-CZDO
92325007016 MW-4R EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CZDO
92325007017 MW-5 RSK 175 Modified 1 PASI-CWDV
EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CZDO
92325007018 MW-9 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CZDO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 125
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92325007019 MW-10 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CZDO
92325007020 MW-16 RSK 175 Modified 1 PASI-CWDV
EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CZDO
92325007021 MW-22 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CZDO
92325007022 MW-23 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CZDO
92325007023 MW-32 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CZDO
92325007024 MW-33 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CZDO
92325007025 MW-34 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CZDO
92325007026 SW-3 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CZDO
92325007027 SW-4R EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CZDO
92325007028 SW-5 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CZDO
92325007029 SW-6 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CZDO
92325007030 EB EPA 6010 16 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8260 50 PASI-CZDO
92325007031 TB EPA 8260 50 PASI-CZDO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-1 Lab ID:92325007001 Collected:12/29/16 11:50 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: RSK 175 ModifiedRSK 175 Headspace
Methane 110 ug/L 01/06/17 13:01 74-82-8 N210.0 10.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/05/17 16:05 7440-36-001/04/17 20:006.0 3.8 1
Arsenic ND ug/L 01/05/17 16:05 7440-38-201/04/17 20:0010.0 2.5 1
Barium 38.9J ug/L 01/05/17 16:05 7440-39-301/04/17 20:001002.5 1
Beryllium ND ug/L 01/05/17 16:05 7440-41-701/04/17 20:001.0 0.50 1
Cadmium 1.3 ug/L 01/05/17 16:05 7440-43-901/04/17 20:001.0 0.50 1
Chromium ND ug/L 01/05/17 16:05 7440-47-301/04/17 20:0010.0 2.5 1
Cobalt 7.3J ug/L 01/05/17 16:05 7440-48-401/04/17 20:0010.0 2.5 1
Copper ND ug/L 01/05/17 16:05 7440-50-801/04/17 20:0010.0 2.5 1
Lead ND ug/L 01/05/17 16:05 7439-92-101/04/17 20:0010.0 2.5 1
Nickel 4.3J ug/L 01/05/17 16:05 7440-02-001/04/17 20:0050.0 2.5 1
Selenium ND ug/L 01/05/17 16:05 7782-49-201/04/17 20:0010.0 5.0 1
Silver ND ug/L 01/05/17 16:05 7440-22-401/04/17 20:0010.0 2.5 1
Thallium 5.7 ug/L 01/05/17 16:05 7440-28-001/04/17 20:005.5 5.0 1
Vanadium ND ug/L 01/05/17 16:05 7440-62-201/04/17 20:0025.0 2.5 1
Zinc 31.3 ug/L 01/05/17 16:05 7440-66-601/04/17 20:0010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 01/04/17 15:12 7439-97-6 M101/04/17 04:000.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/17 16:55 67-64-110010.0 1
Acrylonitrile ND ug/L 01/03/17 16:55 107-13-12001.9 1
Benzene 1.1 ug/L 01/03/17 16:55 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/03/17 16:55 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/03/17 16:55 75-27-41.0 0.18 1
Bromoform ND ug/L 01/03/17 16:55 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/03/17 16:55 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/03/17 16:55 78-93-31000.96 1
Carbon disulfide ND ug/L 01/03/17 16:55 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/03/17 16:55 56-23-51.0 0.25 1
Chlorobenzene 0.23J ug/L 01/03/17 16:55 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/03/17 16:55 75-00-310.0 0.54 1
Chloroform ND ug/L 01/03/17 16:55 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/03/17 16:55 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/17 16:55 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/03/17 16:55 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/17 16:55 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/03/17 16:55 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/03/17 16:55 95-50-15.0 0.30 1
1,4-Dichlorobenzene 3.5 ug/L 01/03/17 16:55 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/17 16:55 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/03/17 16:55 75-34-35.0 0.32 1
1,2-Dichloroethane 0.26J ug/L 01/03/17 16:55 107-06-21.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-1 Lab ID:92325007001 Collected:12/29/16 11:50 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1-Dichloroethene ND ug/L 01/03/17 16:55 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 1.4J ug/L 01/03/17 16:55 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/03/17 16:55 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/03/17 16:55 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/03/17 16:55 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/03/17 16:55 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/03/17 16:55 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/03/17 16:55 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/03/17 16:55 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/03/17 16:55 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/17 16:55 108-10-11000.33 1
Styrene ND ug/L 01/03/17 16:55 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/17 16:55 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/17 16:55 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/03/17 16:55 127-18-41.0 0.46 1
Toluene ND ug/L 01/03/17 16:55 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/03/17 16:55 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/03/17 16:55 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/03/17 16:55 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/03/17 16:55 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/03/17 16:55 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/03/17 16:55 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/03/17 16:55 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/03/17 16:55 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %01/03/17 16:55 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %01/03/17 16:55 17060-07-070-130 1
Toluene-d8 (S)107 %01/03/17 16:55 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-1B Lab ID:92325007002 Collected:12/29/16 11:48 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: RSK 175 ModifiedRSK 175 Headspace
Methane 33.4 ug/L 01/06/17 13:16 74-82-8 N210.0 10.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/05/17 16:14 7440-36-001/04/17 20:006.0 3.8 1
Arsenic ND ug/L 01/05/17 16:14 7440-38-201/04/17 20:0010.0 2.5 1
Barium 67.8J ug/L 01/05/17 16:14 7440-39-301/04/17 20:001002.5 1
Beryllium ND ug/L 01/05/17 16:14 7440-41-701/04/17 20:001.0 0.50 1
Cadmium ND ug/L 01/05/17 16:14 7440-43-901/04/17 20:001.0 0.50 1
Chromium ND ug/L 01/05/17 16:14 7440-47-301/04/17 20:0010.0 2.5 1
Cobalt 89.5 ug/L 01/05/17 16:14 7440-48-401/04/17 20:0010.0 2.5 1
Copper ND ug/L 01/05/17 16:14 7440-50-801/04/17 20:0010.0 2.5 1
Lead ND ug/L 01/05/17 16:14 7439-92-101/04/17 20:0010.0 2.5 1
Nickel 7.1J ug/L 01/05/17 16:14 7440-02-001/04/17 20:0050.0 2.5 1
Selenium ND ug/L 01/05/17 16:14 7782-49-201/04/17 20:0010.0 5.0 1
Silver ND ug/L 01/05/17 16:14 7440-22-401/04/17 20:0010.0 2.5 1
Thallium 5.6 ug/L 01/05/17 16:14 7440-28-001/04/17 20:005.5 5.0 1
Vanadium ND ug/L 01/05/17 16:14 7440-62-201/04/17 20:0025.0 2.5 1
Zinc 14.3 ug/L 01/05/17 16:14 7440-66-601/04/17 20:0010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 0.73 ug/L 01/04/17 15:19 7439-97-601/04/17 04:000.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/17 17:12 67-64-110010.0 1
Acrylonitrile ND ug/L 01/03/17 17:12 107-13-12001.9 1
Benzene 0.43J ug/L 01/03/17 17:12 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/03/17 17:12 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/03/17 17:12 75-27-41.0 0.18 1
Bromoform ND ug/L 01/03/17 17:12 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/03/17 17:12 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/03/17 17:12 78-93-31000.96 1
Carbon disulfide ND ug/L 01/03/17 17:12 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/03/17 17:12 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/03/17 17:12 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/03/17 17:12 75-00-310.0 0.54 1
Chloroform ND ug/L 01/03/17 17:12 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/03/17 17:12 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/17 17:12 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/03/17 17:12 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/17 17:12 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/03/17 17:12 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/03/17 17:12 95-50-15.0 0.30 1
1,4-Dichlorobenzene 3.1 ug/L 01/03/17 17:12 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/17 17:12 110-57-61001.0 1
1,1-Dichloroethane 0.46J ug/L 01/03/17 17:12 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/03/17 17:12 107-06-21.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-1B Lab ID:92325007002 Collected:12/29/16 11:48 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1-Dichloroethene ND ug/L 01/03/17 17:12 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 1.6J ug/L 01/03/17 17:12 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/03/17 17:12 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/03/17 17:12 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/03/17 17:12 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/03/17 17:12 10061-02-61.0 0.26 1
Ethylbenzene 0.33J ug/L 01/03/17 17:12 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/03/17 17:12 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/03/17 17:12 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/03/17 17:12 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/17 17:12 108-10-11000.33 1
Styrene ND ug/L 01/03/17 17:12 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/17 17:12 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/17 17:12 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/03/17 17:12 127-18-41.0 0.46 1
Toluene ND ug/L 01/03/17 17:12 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/03/17 17:12 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/03/17 17:12 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/03/17 17:12 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/03/17 17:12 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/03/17 17:12 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/03/17 17:12 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/03/17 17:12 75-01-41.0 0.62 1
Xylene (Total)1.1J ug/L 01/03/17 17:12 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)104 %01/03/17 17:12 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %01/03/17 17:12 17060-07-070-130 1
Toluene-d8 (S)105 %01/03/17 17:12 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-12 Lab ID:92325007003 Collected:12/29/16 09:10 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: RSK 175 ModifiedRSK 175 Headspace
Methane 3060 ug/L 01/06/17 13:32 74-82-8 N210.0 10.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/05/17 16:17 7440-36-001/04/17 20:006.0 3.8 1
Arsenic 4.2J ug/L 01/05/17 16:17 7440-38-201/04/17 20:0010.0 2.5 1
Barium 120 ug/L 01/05/17 16:17 7440-39-301/04/17 20:001002.5 1
Beryllium ND ug/L 01/05/17 16:17 7440-41-701/04/17 20:001.0 0.50 1
Cadmium ND ug/L 01/05/17 16:17 7440-43-901/04/17 20:001.0 0.50 1
Chromium ND ug/L 01/05/17 16:17 7440-47-301/04/17 20:0010.0 2.5 1
Cobalt 88.0 ug/L 01/05/17 16:17 7440-48-401/04/17 20:0010.0 2.5 1
Copper ND ug/L 01/05/17 16:17 7440-50-801/04/17 20:0010.0 2.5 1
Lead ND ug/L 01/05/17 16:17 7439-92-101/04/17 20:0010.0 2.5 1
Nickel 7.6J ug/L 01/05/17 16:17 7440-02-001/04/17 20:0050.0 2.5 1
Selenium ND ug/L 01/05/17 16:17 7782-49-201/04/17 20:0010.0 5.0 1
Silver ND ug/L 01/05/17 16:17 7440-22-401/04/17 20:0010.0 2.5 1
Thallium ND ug/L 01/05/17 16:17 7440-28-001/04/17 20:005.5 5.0 1
Vanadium ND ug/L 01/05/17 16:17 7440-62-201/04/17 20:0025.0 2.5 1
Zinc 38.5 ug/L 01/05/17 16:17 7440-66-601/04/17 20:0010.0 5.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP, Lab Filtered
Iron, Dissolved 38400 ug/L 01/05/17 15:19 7439-89-601/04/17 21:0050.0 25.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/17 17:30 67-64-110010.0 1
Acrylonitrile ND ug/L 01/03/17 17:30 107-13-12001.9 1
Benzene 0.73J ug/L 01/03/17 17:30 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/03/17 17:30 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/03/17 17:30 75-27-41.0 0.18 1
Bromoform ND ug/L 01/03/17 17:30 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/03/17 17:30 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/03/17 17:30 78-93-31000.96 1
Carbon disulfide ND ug/L 01/03/17 17:30 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/03/17 17:30 56-23-51.0 0.25 1
Chlorobenzene 2.6J ug/L 01/03/17 17:30 108-90-73.0 0.23 1
Chloroethane 1.2J ug/L 01/03/17 17:30 75-00-310.0 0.54 1
Chloroform ND ug/L 01/03/17 17:30 67-66-35.0 0.14 1
Chloromethane 0.15J ug/L 01/03/17 17:30 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/17 17:30 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/03/17 17:30 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/17 17:30 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/03/17 17:30 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/03/17 17:30 95-50-15.0 0.30 1
1,4-Dichlorobenzene 8.7 ug/L 01/03/17 17:30 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/17 17:30 110-57-61001.0 1
1,1-Dichloroethane 1.3J ug/L 01/03/17 17:30 75-34-35.0 0.32 1
1,2-Dichloroethane 0.34J ug/L 01/03/17 17:30 107-06-21.0 0.24 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
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Page 11 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-12 Lab ID:92325007003 Collected:12/29/16 09:10 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1-Dichloroethene ND ug/L 01/03/17 17:30 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 10.6 ug/L 01/03/17 17:30 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/03/17 17:30 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/03/17 17:30 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/03/17 17:30 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/03/17 17:30 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/03/17 17:30 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/03/17 17:30 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/03/17 17:30 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/03/17 17:30 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/17 17:30 108-10-11000.33 1
Styrene ND ug/L 01/03/17 17:30 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/17 17:30 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/17 17:30 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/03/17 17:30 127-18-41.0 0.46 1
Toluene ND ug/L 01/03/17 17:30 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/03/17 17:30 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/03/17 17:30 79-00-51.0 0.29 1
Trichloroethene 1.3 ug/L 01/03/17 17:30 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/03/17 17:30 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/03/17 17:30 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/03/17 17:30 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/03/17 17:30 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/03/17 17:30 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %01/03/17 17:30 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %01/03/17 17:30 17060-07-070-130 1
Toluene-d8 (S)105 %01/03/17 17:30 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 141000 ug/L 01/06/17 00:36 M1500010001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 01/03/17 11:00 18496-25-810001001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 4930J ug/L 01/04/17 19:09 14808-79-825000010001
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND ug/L 12/30/16 21:18 M11000010.0 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 13200 ug/L 01/03/17 17:54 16887-00-610005001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 12 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-12 Lab ID:92325007003 Collected:12/29/16 09:10 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 21000J ug/L 01/04/17 15:0025000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 845J ug/L 01/19/17 22:15 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 13 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-12D Lab ID:92325007004 Collected:12/29/16 16:30 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: RSK 175 ModifiedRSK 175 Headspace
Methane 3140 ug/L 01/06/17 13:47 74-82-8 N210.0 10.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/05/17 16:20 7440-36-001/04/17 20:006.0 3.8 1
Arsenic ND ug/L 01/05/17 16:20 7440-38-201/04/17 20:0010.0 2.5 1
Barium 13.8J ug/L 01/05/17 16:20 7440-39-301/04/17 20:001002.5 1
Beryllium ND ug/L 01/05/17 16:20 7440-41-701/04/17 20:001.0 0.50 1
Cadmium ND ug/L 01/05/17 16:20 7440-43-901/04/17 20:001.0 0.50 1
Chromium ND ug/L 01/05/17 16:20 7440-47-301/04/17 20:0010.0 2.5 1
Cobalt ND ug/L 01/05/17 16:20 7440-48-401/04/17 20:0010.0 2.5 1
Copper ND ug/L 01/05/17 16:20 7440-50-801/04/17 20:0010.0 2.5 1
Lead ND ug/L 01/05/17 16:20 7439-92-101/04/17 20:0010.0 2.5 1
Nickel ND ug/L 01/05/17 16:20 7440-02-001/04/17 20:0050.0 2.5 1
Selenium ND ug/L 01/05/17 16:20 7782-49-201/04/17 20:0010.0 5.0 1
Silver ND ug/L 01/05/17 16:20 7440-22-401/04/17 20:0010.0 2.5 1
Thallium ND ug/L 01/05/17 16:20 7440-28-001/04/17 20:005.5 5.0 1
Vanadium ND ug/L 01/05/17 16:20 7440-62-201/04/17 20:0025.0 2.5 1
Zinc 12.4 ug/L 01/05/17 16:20 7440-66-601/04/17 20:0010.0 5.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP, Lab Filtered
Iron, Dissolved 498 ug/L 01/05/17 15:28 7439-89-601/04/17 21:0050.0 25.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/17 17:47 67-64-110010.0 1
Acrylonitrile ND ug/L 01/03/17 17:47 107-13-12001.9 1
Benzene 0.43J ug/L 01/03/17 17:47 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/03/17 17:47 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/03/17 17:47 75-27-41.0 0.18 1
Bromoform ND ug/L 01/03/17 17:47 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/03/17 17:47 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/03/17 17:47 78-93-31000.96 1
Carbon disulfide ND ug/L 01/03/17 17:47 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/03/17 17:47 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/03/17 17:47 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/03/17 17:47 75-00-310.0 0.54 1
Chloroform ND ug/L 01/03/17 17:47 67-66-35.0 0.14 1
Chloromethane 0.20J ug/L 01/03/17 17:47 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/17 17:47 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/03/17 17:47 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/17 17:47 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/03/17 17:47 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/03/17 17:47 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/03/17 17:47 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/17 17:47 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/03/17 17:47 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/03/17 17:47 107-06-21.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 14 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-12D Lab ID:92325007004 Collected:12/29/16 16:30 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1-Dichloroethene ND ug/L 01/03/17 17:47 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.59J ug/L 01/03/17 17:47 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/03/17 17:47 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/03/17 17:47 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/03/17 17:47 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/03/17 17:47 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/03/17 17:47 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/03/17 17:47 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/03/17 17:47 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/03/17 17:47 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/17 17:47 108-10-11000.33 1
Styrene ND ug/L 01/03/17 17:47 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/17 17:47 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/17 17:47 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/03/17 17:47 127-18-41.0 0.46 1
Toluene ND ug/L 01/03/17 17:47 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/03/17 17:47 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/03/17 17:47 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/03/17 17:47 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/03/17 17:47 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/03/17 17:47 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/03/17 17:47 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/03/17 17:47 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/03/17 17:47 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %01/03/17 17:47 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %01/03/17 17:47 17060-07-070-130 1
Toluene-d8 (S)106 %01/03/17 17:47 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 399000 ug/L 01/06/17 01:16500010001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 01/05/17 10:50 18496-25-8 M110001001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate ND ug/L 01/04/17 19:18 14808-79-825000010001
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND ug/L 01/04/17 20:53 H11000010.0 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 69300 ug/L 01/03/17 17:55 16887-00-6200010002
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-12D Lab ID:92325007004 Collected:12/29/16 16:30 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 16000J ug/L 01/04/17 15:0025000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 3790 ug/L 01/19/17 22:50 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 16 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-13 Lab ID:92325007005 Collected:12/29/16 16:00 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/05/17 01:35 7440-36-001/03/17 17:006.0 3.8 1
Arsenic ND ug/L 01/05/17 01:35 7440-38-201/03/17 17:0010.0 2.5 1
Barium 15.9J ug/L 01/05/17 01:35 7440-39-301/03/17 17:001002.5 1
Beryllium ND ug/L 01/05/17 01:35 7440-41-701/03/17 17:001.0 0.50 1
Cadmium ND ug/L 01/05/17 01:35 7440-43-901/03/17 17:001.0 0.50 1
Chromium ND ug/L 01/05/17 01:35 7440-47-301/03/17 17:0010.0 2.5 1
Cobalt 4.3J ug/L 01/05/17 01:35 7440-48-401/03/17 17:0010.0 2.5 1
Copper ND ug/L 01/05/17 01:35 7440-50-801/03/17 17:0010.0 2.5 1
Lead ND ug/L 01/05/17 01:35 7439-92-101/03/17 17:0010.0 2.5 1
Nickel 10.3J ug/L 01/05/17 01:35 7440-02-001/03/17 17:0050.0 2.5 1
Selenium ND ug/L 01/05/17 01:35 7782-49-201/03/17 17:0010.0 5.0 1
Silver ND ug/L 01/05/17 01:35 7440-22-401/03/17 17:0010.0 2.5 1
Thallium ND ug/L 01/05/17 01:35 7440-28-001/03/17 17:005.5 5.0 1
Vanadium ND ug/L 01/05/17 01:35 7440-62-201/03/17 17:0025.0 2.5 1
Zinc 7.8J ug/L 01/05/17 01:35 7440-66-601/03/17 17:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/17 18:05 67-64-110010.0 1
Acrylonitrile ND ug/L 01/03/17 18:05 107-13-12001.9 1
Benzene ND ug/L 01/03/17 18:05 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/03/17 18:05 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/03/17 18:05 75-27-41.0 0.18 1
Bromoform ND ug/L 01/03/17 18:05 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/03/17 18:05 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/03/17 18:05 78-93-31000.96 1
Carbon disulfide ND ug/L 01/03/17 18:05 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/03/17 18:05 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/03/17 18:05 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/03/17 18:05 75-00-310.0 0.54 1
Chloroform ND ug/L 01/03/17 18:05 67-66-35.0 0.14 1
Chloromethane 0.17J ug/L 01/03/17 18:05 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/17 18:05 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/03/17 18:05 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/17 18:05 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/03/17 18:05 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/03/17 18:05 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/03/17 18:05 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/17 18:05 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/03/17 18:05 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/03/17 18:05 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/03/17 18:05 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/03/17 18:05 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/03/17 18:05 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/03/17 18:05 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/03/17 18:05 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/03/17 18:05 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
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Page 17 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-13 Lab ID:92325007005 Collected:12/29/16 16:00 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/03/17 18:05 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/03/17 18:05 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/03/17 18:05 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/03/17 18:05 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/17 18:05 108-10-11000.33 1
Styrene ND ug/L 01/03/17 18:05 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/17 18:05 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/17 18:05 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/03/17 18:05 127-18-41.0 0.46 1
Toluene ND ug/L 01/03/17 18:05 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/03/17 18:05 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/03/17 18:05 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/03/17 18:05 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/03/17 18:05 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/03/17 18:05 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/03/17 18:05 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/03/17 18:05 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/03/17 18:05 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %01/03/17 18:05 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %01/03/17 18:05 17060-07-070-130 1
Toluene-d8 (S)106 %01/03/17 18:05 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
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Page 18 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-14 Lab ID:92325007006 Collected:12/29/16 15:00 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/05/17 01:38 7440-36-001/03/17 17:006.0 3.8 1
Arsenic ND ug/L 01/05/17 01:38 7440-38-201/03/17 17:0010.0 2.5 1
Barium 12.7J ug/L 01/05/17 01:38 7440-39-301/03/17 17:001002.5 1
Beryllium ND ug/L 01/05/17 01:38 7440-41-701/03/17 17:001.0 0.50 1
Cadmium ND ug/L 01/05/17 01:38 7440-43-901/03/17 17:001.0 0.50 1
Chromium ND ug/L 01/05/17 01:38 7440-47-301/03/17 17:0010.0 2.5 1
Cobalt ND ug/L 01/05/17 01:38 7440-48-401/03/17 17:0010.0 2.5 1
Copper 81.0 ug/L 01/05/17 01:38 7440-50-801/03/17 17:0010.0 2.5 1
Lead ND ug/L 01/05/17 01:38 7439-92-101/03/17 17:0010.0 2.5 1
Nickel ND ug/L 01/05/17 01:38 7440-02-001/03/17 17:0050.0 2.5 1
Selenium ND ug/L 01/05/17 01:38 7782-49-201/03/17 17:0010.0 5.0 1
Silver ND ug/L 01/05/17 01:38 7440-22-401/03/17 17:0010.0 2.5 1
Thallium ND ug/L 01/05/17 01:38 7440-28-001/03/17 17:005.5 5.0 1
Vanadium ND ug/L 01/05/17 01:38 7440-62-201/03/17 17:0025.0 2.5 1
Zinc 32.0 ug/L 01/05/17 01:38 7440-66-601/03/17 17:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/17 18:22 67-64-110010.0 1
Acrylonitrile ND ug/L 01/03/17 18:22 107-13-12001.9 1
Benzene 0.26J ug/L 01/03/17 18:22 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/03/17 18:22 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/03/17 18:22 75-27-41.0 0.18 1
Bromoform ND ug/L 01/03/17 18:22 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/03/17 18:22 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/03/17 18:22 78-93-31000.96 1
Carbon disulfide ND ug/L 01/03/17 18:22 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/03/17 18:22 56-23-51.0 0.25 1
Chlorobenzene 0.88J ug/L 01/03/17 18:22 108-90-73.0 0.23 1
Chloroethane 0.84J ug/L 01/03/17 18:22 75-00-310.0 0.54 1
Chloroform ND ug/L 01/03/17 18:22 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/03/17 18:22 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/17 18:22 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/03/17 18:22 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/17 18:22 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/03/17 18:22 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/03/17 18:22 95-50-15.0 0.30 1
1,4-Dichlorobenzene 2.4 ug/L 01/03/17 18:22 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/17 18:22 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/03/17 18:22 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/03/17 18:22 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/03/17 18:22 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 6.9 ug/L 01/03/17 18:22 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/03/17 18:22 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/03/17 18:22 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/03/17 18:22 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/03/17 18:22 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 19 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-14 Lab ID:92325007006 Collected:12/29/16 15:00 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/03/17 18:22 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/03/17 18:22 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/03/17 18:22 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/03/17 18:22 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/17 18:22 108-10-11000.33 1
Styrene ND ug/L 01/03/17 18:22 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/17 18:22 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/17 18:22 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/03/17 18:22 127-18-41.0 0.46 1
Toluene ND ug/L 01/03/17 18:22 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/03/17 18:22 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/03/17 18:22 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/03/17 18:22 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/03/17 18:22 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/03/17 18:22 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/03/17 18:22 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/03/17 18:22 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/03/17 18:22 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %01/03/17 18:22 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %01/03/17 18:22 17060-07-070-130 1
Toluene-d8 (S)104 %01/03/17 18:22 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-15 Lab ID:92325007007 Collected:12/29/16 16:45 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/05/17 01:42 7440-36-001/03/17 17:006.0 3.8 1
Arsenic ND ug/L 01/05/17 01:42 7440-38-201/03/17 17:0010.0 2.5 1
Barium 54.7J ug/L 01/05/17 01:42 7440-39-301/03/17 17:001002.5 1
Beryllium 1.0 ug/L 01/05/17 01:42 7440-41-701/03/17 17:001.0 0.50 1
Cadmium ND ug/L 01/05/17 01:42 7440-43-901/03/17 17:001.0 0.50 1
Chromium ND ug/L 01/05/17 01:42 7440-47-301/03/17 17:0010.0 2.5 1
Cobalt 5.2J ug/L 01/05/17 01:42 7440-48-401/03/17 17:0010.0 2.5 1
Copper ND ug/L 01/05/17 01:42 7440-50-801/03/17 17:0010.0 2.5 1
Lead ND ug/L 01/05/17 01:42 7439-92-101/03/17 17:0010.0 2.5 1
Nickel 3.4J ug/L 01/05/17 01:42 7440-02-001/03/17 17:0050.0 2.5 1
Selenium ND ug/L 01/05/17 01:42 7782-49-201/03/17 17:0010.0 5.0 1
Silver ND ug/L 01/05/17 01:42 7440-22-401/03/17 17:0010.0 2.5 1
Thallium ND ug/L 01/05/17 01:42 7440-28-001/03/17 17:005.5 5.0 1
Vanadium ND ug/L 01/05/17 01:42 7440-62-201/03/17 17:0025.0 2.5 1
Zinc ND ug/L 01/05/17 01:42 7440-66-601/03/17 17:0010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 01/04/17 15:21 7439-97-601/04/17 04:000.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/17 18:40 67-64-110010.0 1
Acrylonitrile ND ug/L 01/03/17 18:40 107-13-12001.9 1
Benzene 2.6 ug/L 01/03/17 18:40 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/03/17 18:40 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/03/17 18:40 75-27-41.0 0.18 1
Bromoform ND ug/L 01/03/17 18:40 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/03/17 18:40 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/03/17 18:40 78-93-31000.96 1
Carbon disulfide ND ug/L 01/03/17 18:40 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/03/17 18:40 56-23-51.0 0.25 1
Chlorobenzene 0.88J ug/L 01/03/17 18:40 108-90-73.0 0.23 1
Chloroethane 0.84J ug/L 01/03/17 18:40 75-00-310.0 0.54 1
Chloroform ND ug/L 01/03/17 18:40 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/03/17 18:40 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/17 18:40 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/03/17 18:40 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/17 18:40 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/03/17 18:40 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/03/17 18:40 95-50-15.0 0.30 1
1,4-Dichlorobenzene 0.85J ug/L 01/03/17 18:40 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/17 18:40 110-57-61001.0 1
1,1-Dichloroethane 0.95J ug/L 01/03/17 18:40 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/03/17 18:40 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/03/17 18:40 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 7.3 ug/L 01/03/17 18:40 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/03/17 18:40 156-60-55.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-15 Lab ID:92325007007 Collected:12/29/16 16:45 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 01/03/17 18:40 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/03/17 18:40 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/03/17 18:40 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/03/17 18:40 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/03/17 18:40 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/03/17 18:40 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/03/17 18:40 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/17 18:40 108-10-11000.33 1
Styrene ND ug/L 01/03/17 18:40 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/17 18:40 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/17 18:40 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/03/17 18:40 127-18-41.0 0.46 1
Toluene ND ug/L 01/03/17 18:40 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/03/17 18:40 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/03/17 18:40 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/03/17 18:40 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/03/17 18:40 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/03/17 18:40 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/03/17 18:40 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/03/17 18:40 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/03/17 18:40 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %01/03/17 18:40 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %01/03/17 18:40 17060-07-070-130 1
Toluene-d8 (S)105 %01/03/17 18:40 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-17 Lab ID:92325007008 Collected:12/29/16 16:50 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/05/17 16:23 7440-36-001/04/17 20:006.0 3.8 1
Arsenic ND ug/L 01/05/17 16:23 7440-38-201/04/17 20:0010.0 2.5 1
Barium 75.0J ug/L 01/05/17 16:23 7440-39-301/04/17 20:001002.5 1
Beryllium ND ug/L 01/05/17 16:23 7440-41-701/04/17 20:001.0 0.50 1
Cadmium ND ug/L 01/05/17 16:23 7440-43-901/04/17 20:001.0 0.50 1
Chromium ND ug/L 01/05/17 16:23 7440-47-301/04/17 20:0010.0 2.5 1
Cobalt 57.5 ug/L 01/05/17 16:23 7440-48-401/04/17 20:0010.0 2.5 1
Copper ND ug/L 01/05/17 16:23 7440-50-801/04/17 20:0010.0 2.5 1
Lead ND ug/L 01/05/17 16:23 7439-92-101/04/17 20:0010.0 2.5 1
Nickel 7.6J ug/L 01/05/17 16:23 7440-02-001/04/17 20:0050.0 2.5 1
Selenium ND ug/L 01/05/17 16:23 7782-49-201/04/17 20:0010.0 5.0 1
Silver ND ug/L 01/05/17 16:23 7440-22-401/04/17 20:0010.0 2.5 1
Thallium ND ug/L 01/05/17 16:23 7440-28-001/04/17 20:005.5 5.0 1
Vanadium ND ug/L 01/05/17 16:23 7440-62-201/04/17 20:0025.0 2.5 1
Zinc 10.2 ug/L 01/05/17 16:23 7440-66-601/04/17 20:0010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 0.26 ug/L 01/04/17 15:23 7439-97-601/04/17 04:000.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/17 18:57 67-64-110010.0 1
Acrylonitrile ND ug/L 01/03/17 18:57 107-13-12001.9 1
Benzene 0.96J ug/L 01/03/17 18:57 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/03/17 18:57 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/03/17 18:57 75-27-41.0 0.18 1
Bromoform ND ug/L 01/03/17 18:57 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/03/17 18:57 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/03/17 18:57 78-93-31000.96 1
Carbon disulfide ND ug/L 01/03/17 18:57 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/03/17 18:57 56-23-51.0 0.25 1
Chlorobenzene 0.37J ug/L 01/03/17 18:57 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/03/17 18:57 75-00-310.0 0.54 1
Chloroform ND ug/L 01/03/17 18:57 67-66-35.0 0.14 1
Chloromethane 0.14J ug/L 01/03/17 18:57 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/17 18:57 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/03/17 18:57 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/17 18:57 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/03/17 18:57 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/03/17 18:57 95-50-15.0 0.30 1
1,4-Dichlorobenzene 0.49J ug/L 01/03/17 18:57 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/17 18:57 110-57-61001.0 1
1,1-Dichloroethane 0.81J ug/L 01/03/17 18:57 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/03/17 18:57 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/03/17 18:57 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 2.3J ug/L 01/03/17 18:57 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/03/17 18:57 156-60-55.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-17 Lab ID:92325007008 Collected:12/29/16 16:50 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 01/03/17 18:57 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/03/17 18:57 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/03/17 18:57 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/03/17 18:57 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/03/17 18:57 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/03/17 18:57 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/03/17 18:57 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/17 18:57 108-10-11000.33 1
Styrene ND ug/L 01/03/17 18:57 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/17 18:57 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/17 18:57 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/03/17 18:57 127-18-41.0 0.46 1
Toluene ND ug/L 01/03/17 18:57 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/03/17 18:57 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/03/17 18:57 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/03/17 18:57 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/03/17 18:57 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/03/17 18:57 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/03/17 18:57 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/03/17 18:57 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/03/17 18:57 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %01/03/17 18:57 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %01/03/17 18:57 17060-07-070-130 1
Toluene-d8 (S)103 %01/03/17 18:57 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-19 Lab ID:92325007009 Collected:12/29/16 11:55 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/05/17 16:27 7440-36-001/04/17 20:006.0 3.8 1
Arsenic ND ug/L 01/05/17 16:27 7440-38-201/04/17 20:0010.0 2.5 1
Barium 8.8J ug/L 01/05/17 16:27 7440-39-301/04/17 20:001002.5 1
Beryllium ND ug/L 01/05/17 16:27 7440-41-701/04/17 20:001.0 0.50 1
Cadmium ND ug/L 01/05/17 16:27 7440-43-901/04/17 20:001.0 0.50 1
Chromium ND ug/L 01/05/17 16:27 7440-47-301/04/17 20:0010.0 2.5 1
Cobalt ND ug/L 01/05/17 16:27 7440-48-401/04/17 20:0010.0 2.5 1
Copper ND ug/L 01/05/17 16:27 7440-50-801/04/17 20:0010.0 2.5 1
Lead ND ug/L 01/05/17 16:27 7439-92-101/04/17 20:0010.0 2.5 1
Nickel ND ug/L 01/05/17 16:27 7440-02-001/04/17 20:0050.0 2.5 1
Selenium ND ug/L 01/05/17 16:27 7782-49-201/04/17 20:0010.0 5.0 1
Silver ND ug/L 01/05/17 16:27 7440-22-401/04/17 20:0010.0 2.5 1
Thallium ND ug/L 01/05/17 16:27 7440-28-001/04/17 20:005.5 5.0 1
Vanadium ND ug/L 01/05/17 16:27 7440-62-201/04/17 20:0025.0 2.5 1
Zinc ND ug/L 01/05/17 16:27 7440-66-601/04/17 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/17 19:15 67-64-110010.0 1
Acrylonitrile ND ug/L 01/03/17 19:15 107-13-12001.9 1
Benzene ND ug/L 01/03/17 19:15 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/03/17 19:15 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/03/17 19:15 75-27-41.0 0.18 1
Bromoform ND ug/L 01/03/17 19:15 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/03/17 19:15 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/03/17 19:15 78-93-31000.96 1
Carbon disulfide ND ug/L 01/03/17 19:15 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/03/17 19:15 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/03/17 19:15 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/03/17 19:15 75-00-310.0 0.54 1
Chloroform ND ug/L 01/03/17 19:15 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/03/17 19:15 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/17 19:15 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/03/17 19:15 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/17 19:15 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/03/17 19:15 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/03/17 19:15 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/03/17 19:15 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/17 19:15 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/03/17 19:15 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/03/17 19:15 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/03/17 19:15 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/03/17 19:15 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/03/17 19:15 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/03/17 19:15 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/03/17 19:15 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/03/17 19:15 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 25 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-19 Lab ID:92325007009 Collected:12/29/16 11:55 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/03/17 19:15 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/03/17 19:15 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/03/17 19:15 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/03/17 19:15 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/17 19:15 108-10-11000.33 1
Styrene ND ug/L 01/03/17 19:15 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/17 19:15 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/17 19:15 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/03/17 19:15 127-18-41.0 0.46 1
Toluene ND ug/L 01/03/17 19:15 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/03/17 19:15 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/03/17 19:15 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/03/17 19:15 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/03/17 19:15 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/03/17 19:15 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/03/17 19:15 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/03/17 19:15 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/03/17 19:15 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)103 %01/03/17 19:15 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %01/03/17 19:15 17060-07-070-130 1
Toluene-d8 (S)108 %01/03/17 19:15 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 26 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-20 Lab ID:92325007010 Collected:12/29/16 16:30 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/05/17 01:45 7440-36-001/03/17 17:006.0 3.8 1
Arsenic ND ug/L 01/05/17 01:45 7440-38-201/03/17 17:0010.0 2.5 1
Barium 54.6J ug/L 01/05/17 01:45 7440-39-301/03/17 17:001002.5 1
Beryllium ND ug/L 01/05/17 01:45 7440-41-701/03/17 17:001.0 0.50 1
Cadmium ND ug/L 01/05/17 01:45 7440-43-901/03/17 17:001.0 0.50 1
Chromium ND ug/L 01/05/17 01:45 7440-47-301/03/17 17:0010.0 2.5 1
Cobalt ND ug/L 01/05/17 01:45 7440-48-401/03/17 17:0010.0 2.5 1
Copper ND ug/L 01/05/17 01:45 7440-50-801/03/17 17:0010.0 2.5 1
Lead ND ug/L 01/05/17 01:45 7439-92-101/03/17 17:0010.0 2.5 1
Nickel ND ug/L 01/05/17 01:45 7440-02-001/03/17 17:0050.0 2.5 1
Selenium ND ug/L 01/05/17 01:45 7782-49-201/03/17 17:0010.0 5.0 1
Silver ND ug/L 01/05/17 01:45 7440-22-401/03/17 17:0010.0 2.5 1
Thallium ND ug/L 01/05/17 01:45 7440-28-001/03/17 17:005.5 5.0 1
Vanadium ND ug/L 01/05/17 01:45 7440-62-201/03/17 17:0025.0 2.5 1
Zinc ND ug/L 01/05/17 01:45 7440-66-601/03/17 17:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/17 19:32 67-64-110010.0 1
Acrylonitrile ND ug/L 01/03/17 19:32 107-13-12001.9 1
Benzene ND ug/L 01/03/17 19:32 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/03/17 19:32 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/03/17 19:32 75-27-41.0 0.18 1
Bromoform ND ug/L 01/03/17 19:32 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/03/17 19:32 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/03/17 19:32 78-93-31000.96 1
Carbon disulfide ND ug/L 01/03/17 19:32 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/03/17 19:32 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/03/17 19:32 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/03/17 19:32 75-00-310.0 0.54 1
Chloroform ND ug/L 01/03/17 19:32 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/03/17 19:32 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/17 19:32 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/03/17 19:32 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/17 19:32 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/03/17 19:32 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/03/17 19:32 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/03/17 19:32 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/17 19:32 110-57-61001.0 1
1,1-Dichloroethane 0.40J ug/L 01/03/17 19:32 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/03/17 19:32 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/03/17 19:32 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.41J ug/L 01/03/17 19:32 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/03/17 19:32 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/03/17 19:32 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/03/17 19:32 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/03/17 19:32 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-20 Lab ID:92325007010 Collected:12/29/16 16:30 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/03/17 19:32 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/03/17 19:32 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/03/17 19:32 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/03/17 19:32 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/17 19:32 108-10-11000.33 1
Styrene ND ug/L 01/03/17 19:32 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/17 19:32 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/17 19:32 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/03/17 19:32 127-18-41.0 0.46 1
Toluene ND ug/L 01/03/17 19:32 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/03/17 19:32 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/03/17 19:32 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/03/17 19:32 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/03/17 19:32 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/03/17 19:32 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/03/17 19:32 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/03/17 19:32 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/03/17 19:32 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %01/03/17 19:32 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %01/03/17 19:32 17060-07-070-130 1
Toluene-d8 (S)102 %01/03/17 19:32 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-21 Lab ID:92325007011 Collected:12/29/16 16:40 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/06/17 16:23 7440-36-001/04/17 20:006.0 3.8 1
Arsenic 4.8J ug/L 01/06/17 16:23 7440-38-201/04/17 20:0010.0 2.5 1
Barium 52.5J ug/L 01/05/17 16:46 7440-39-301/04/17 20:001002.5 1
Beryllium ND ug/L 01/05/17 16:46 7440-41-701/04/17 20:001.0 0.50 1
Cadmium ND ug/L 01/05/17 16:46 7440-43-901/04/17 20:001.0 0.50 1
Chromium ND ug/L 01/05/17 16:46 7440-47-301/04/17 20:0010.0 2.5 1
Cobalt 6.0J ug/L 01/06/17 16:23 7440-48-401/04/17 20:0010.0 2.5 1
Copper ND ug/L 01/06/17 16:23 7440-50-801/04/17 20:0010.0 2.5 1
Lead ND ug/L 01/06/17 16:23 7439-92-101/04/17 20:0010.0 2.5 1
Nickel 4.4J ug/L 01/05/17 16:46 7440-02-001/04/17 20:0050.0 2.5 1
Selenium ND ug/L 01/06/17 16:23 7782-49-201/04/17 20:0010.0 5.0 1
Silver ND ug/L 01/05/17 16:46 7440-22-401/04/17 20:0010.0 2.5 1
Thallium ND ug/L 01/05/17 16:46 7440-28-001/04/17 20:005.5 5.0 1
Vanadium ND ug/L 01/05/17 16:46 7440-62-201/04/17 20:0025.0 2.5 1
Zinc ND ug/L 01/06/17 16:23 7440-66-601/04/17 20:0010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 0.10J ug/L 01/04/17 15:26 7439-97-601/04/17 04:000.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/17 20:07 67-64-110010.0 1
Acrylonitrile ND ug/L 01/03/17 20:07 107-13-12001.9 1
Benzene 0.74J ug/L 01/03/17 20:07 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/03/17 20:07 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/03/17 20:07 75-27-41.0 0.18 1
Bromoform ND ug/L 01/03/17 20:07 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/03/17 20:07 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/03/17 20:07 78-93-31000.96 1
Carbon disulfide ND ug/L 01/03/17 20:07 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/03/17 20:07 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/03/17 20:07 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/03/17 20:07 75-00-310.0 0.54 1
Chloroform ND ug/L 01/03/17 20:07 67-66-35.0 0.14 1
Chloromethane 0.12J ug/L 01/03/17 20:07 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/17 20:07 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/03/17 20:07 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/17 20:07 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/03/17 20:07 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/03/17 20:07 95-50-15.0 0.30 1
1,4-Dichlorobenzene 0.50J ug/L 01/03/17 20:07 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/17 20:07 110-57-61001.0 1
1,1-Dichloroethane 0.81J ug/L 01/03/17 20:07 75-34-35.0 0.32 1
1,2-Dichloroethane 0.29J ug/L 01/03/17 20:07 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/03/17 20:07 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 2.6J ug/L 01/03/17 20:07 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/03/17 20:07 156-60-55.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-21 Lab ID:92325007011 Collected:12/29/16 16:40 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 01/03/17 20:07 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/03/17 20:07 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/03/17 20:07 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/03/17 20:07 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/03/17 20:07 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/03/17 20:07 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/03/17 20:07 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/17 20:07 108-10-11000.33 1
Styrene ND ug/L 01/03/17 20:07 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/17 20:07 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/17 20:07 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/03/17 20:07 127-18-41.0 0.46 1
Toluene ND ug/L 01/03/17 20:07 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/03/17 20:07 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/03/17 20:07 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/03/17 20:07 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/03/17 20:07 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/03/17 20:07 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/03/17 20:07 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/03/17 20:07 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/03/17 20:07 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %01/03/17 20:07 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %01/03/17 20:07 17060-07-070-130 1
Toluene-d8 (S)104 %01/03/17 20:07 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-24 Lab ID:92325007012 Collected:12/29/16 15:20 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: RSK 175 ModifiedRSK 175 Headspace
Methane 12.7 ug/L 01/06/17 14:02 74-82-8 N210.0 10.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/05/17 01:48 7440-36-001/03/17 17:006.0 3.8 1
Arsenic ND ug/L 01/05/17 01:48 7440-38-201/03/17 17:0010.0 2.5 1
Barium 49.9J ug/L 01/05/17 01:48 7440-39-301/03/17 17:001002.5 1
Beryllium ND ug/L 01/05/17 01:48 7440-41-701/03/17 17:001.0 0.50 1
Cadmium ND ug/L 01/05/17 01:48 7440-43-901/03/17 17:001.0 0.50 1
Chromium ND ug/L 01/05/17 01:48 7440-47-301/03/17 17:0010.0 2.5 1
Cobalt 14.1 ug/L 01/05/17 01:48 7440-48-401/03/17 17:0010.0 2.5 1
Copper ND ug/L 01/05/17 01:48 7440-50-801/03/17 17:0010.0 2.5 1
Lead ND ug/L 01/05/17 01:48 7439-92-101/03/17 17:0010.0 2.5 1
Nickel 3.1J ug/L 01/05/17 01:48 7440-02-001/03/17 17:0050.0 2.5 1
Selenium ND ug/L 01/05/17 01:48 7782-49-201/03/17 17:0010.0 5.0 1
Silver ND ug/L 01/05/17 01:48 7440-22-401/03/17 17:0010.0 2.5 1
Thallium ND ug/L 01/05/17 01:48 7440-28-001/03/17 17:005.5 5.0 1
Vanadium ND ug/L 01/05/17 01:48 7440-62-201/03/17 17:0025.0 2.5 1
Zinc 8.4J ug/L 01/05/17 01:48 7440-66-601/03/17 17:0010.0 5.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP, Lab Filtered
Iron, Dissolved 194 ug/L 01/05/17 15:31 7439-89-601/04/17 21:0050.0 25.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/17 20:24 67-64-110010.0 1
Acrylonitrile ND ug/L 01/03/17 20:24 107-13-12001.9 1
Benzene ND ug/L 01/03/17 20:24 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/03/17 20:24 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/03/17 20:24 75-27-41.0 0.18 1
Bromoform ND ug/L 01/03/17 20:24 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/03/17 20:24 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/03/17 20:24 78-93-31000.96 1
Carbon disulfide ND ug/L 01/03/17 20:24 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/03/17 20:24 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/03/17 20:24 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/03/17 20:24 75-00-310.0 0.54 1
Chloroform ND ug/L 01/03/17 20:24 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/03/17 20:24 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/17 20:24 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/03/17 20:24 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/17 20:24 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/03/17 20:24 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/03/17 20:24 95-50-15.0 0.30 1
1,4-Dichlorobenzene 0.48J ug/L 01/03/17 20:24 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/17 20:24 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/03/17 20:24 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/03/17 20:24 107-06-21.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
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Page 31 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-24 Lab ID:92325007012 Collected:12/29/16 15:20 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1-Dichloroethene ND ug/L 01/03/17 20:24 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.91J ug/L 01/03/17 20:24 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/03/17 20:24 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/03/17 20:24 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/03/17 20:24 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/03/17 20:24 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/03/17 20:24 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/03/17 20:24 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/03/17 20:24 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/03/17 20:24 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/17 20:24 108-10-11000.33 1
Styrene ND ug/L 01/03/17 20:24 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/17 20:24 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/17 20:24 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/03/17 20:24 127-18-41.0 0.46 1
Toluene ND ug/L 01/03/17 20:24 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/03/17 20:24 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/03/17 20:24 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/03/17 20:24 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/03/17 20:24 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/03/17 20:24 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/03/17 20:24 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/03/17 20:24 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/03/17 20:24 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %01/03/17 20:24 460-00-470-130 1
1,2-Dichloroethane-d4 (S)111 %01/03/17 20:24 17060-07-070-130 1
Toluene-d8 (S)111 %01/03/17 20:24 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 36200 ug/L 01/06/17 01:42500010001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 01/05/17 10:50 18496-25-810001001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 5660J ug/L 01/04/17 19:27 14808-79-825000010001
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate 325J ug/L 12/30/16 21:291000010.0 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 18900 ug/L 01/03/17 17:58 16887-00-610005001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 32 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-24 Lab ID:92325007012 Collected:12/29/16 15:20 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand ND ug/L 01/04/17 15:0025000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 1660 ug/L 01/19/17 23:04 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 33 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-25 Lab ID:92325007013 Collected:12/29/16 15:35 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: RSK 175 ModifiedRSK 175 Headspace
Methane 903 ug/L 01/06/17 14:17 74-82-8 N210.0 10.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/05/17 02:00 7440-36-001/03/17 17:006.0 3.8 1
Arsenic ND ug/L 01/05/17 02:00 7440-38-201/03/17 17:0010.0 2.5 1
Barium 15.3J ug/L 01/05/17 02:00 7440-39-301/03/17 17:001002.5 1
Beryllium ND ug/L 01/05/17 02:00 7440-41-701/03/17 17:001.0 0.50 1
Cadmium ND ug/L 01/05/17 02:00 7440-43-901/03/17 17:001.0 0.50 1
Chromium ND ug/L 01/05/17 02:00 7440-47-301/03/17 17:0010.0 2.5 1
Cobalt ND ug/L 01/05/17 02:00 7440-48-401/03/17 17:0010.0 2.5 1
Copper ND ug/L 01/05/17 02:00 7440-50-801/03/17 17:0010.0 2.5 1
Lead ND ug/L 01/05/17 02:00 7439-92-101/03/17 17:0010.0 2.5 1
Nickel 3.4J ug/L 01/05/17 02:00 7440-02-001/03/17 17:0050.0 2.5 1
Selenium ND ug/L 01/05/17 02:00 7782-49-201/03/17 17:0010.0 5.0 1
Silver ND ug/L 01/05/17 02:00 7440-22-401/03/17 17:0010.0 2.5 1
Thallium ND ug/L 01/05/17 02:00 7440-28-001/03/17 17:005.5 5.0 1
Vanadium ND ug/L 01/05/17 02:00 7440-62-201/03/17 17:0025.0 2.5 1
Zinc ND ug/L 01/05/17 02:00 7440-66-601/03/17 17:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/17 20:42 67-64-110010.0 1
Acrylonitrile ND ug/L 01/03/17 20:42 107-13-12001.9 1
Benzene 0.59J ug/L 01/03/17 20:42 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/03/17 20:42 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/03/17 20:42 75-27-41.0 0.18 1
Bromoform ND ug/L 01/03/17 20:42 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/03/17 20:42 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/03/17 20:42 78-93-31000.96 1
Carbon disulfide ND ug/L 01/03/17 20:42 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/03/17 20:42 56-23-51.0 0.25 1
Chlorobenzene 0.36J ug/L 01/03/17 20:42 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/03/17 20:42 75-00-310.0 0.54 1
Chloroform ND ug/L 01/03/17 20:42 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/03/17 20:42 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/17 20:42 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/03/17 20:42 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/17 20:42 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/03/17 20:42 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/03/17 20:42 95-50-15.0 0.30 1
1,4-Dichlorobenzene 1.7 ug/L 01/03/17 20:42 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/17 20:42 110-57-61001.0 1
1,1-Dichloroethane 0.61J ug/L 01/03/17 20:42 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/03/17 20:42 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/03/17 20:42 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 1.6J ug/L 01/03/17 20:42 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/03/17 20:42 156-60-55.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-25 Lab ID:92325007013 Collected:12/29/16 15:35 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 01/03/17 20:42 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/03/17 20:42 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/03/17 20:42 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/03/17 20:42 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/03/17 20:42 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/03/17 20:42 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/03/17 20:42 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/17 20:42 108-10-11000.33 1
Styrene ND ug/L 01/03/17 20:42 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/17 20:42 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/17 20:42 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/03/17 20:42 127-18-41.0 0.46 1
Toluene ND ug/L 01/03/17 20:42 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/03/17 20:42 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/03/17 20:42 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/03/17 20:42 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/03/17 20:42 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/03/17 20:42 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/03/17 20:42 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/03/17 20:42 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/03/17 20:42 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %01/03/17 20:42 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %01/03/17 20:42 17060-07-070-130 1
Toluene-d8 (S)108 %01/03/17 20:42 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-7 Lab ID:92325007014 Collected:12/29/16 17:10 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/11/17 11:49 7440-36-001/09/17 17:006.0 3.8 1
Arsenic 3.0J ug/L 01/11/17 11:49 7440-38-201/09/17 17:0010.0 2.5 1
Barium 4.9J ug/L 01/11/17 11:49 7440-39-301/09/17 17:001002.5 1
Beryllium ND ug/L 01/11/17 11:49 7440-41-701/09/17 17:001.0 0.50 1
Cadmium ND ug/L 01/11/17 11:49 7440-43-901/09/17 17:001.0 0.50 1
Chromium ND ug/L 01/11/17 11:49 7440-47-301/09/17 17:0010.0 2.5 1
Cobalt ND ug/L 01/11/17 11:49 7440-48-401/09/17 17:0010.0 2.5 1
Copper ND ug/L 01/11/17 11:49 7440-50-801/09/17 17:0010.0 2.5 1
Lead 3.2J ug/L 01/11/17 11:49 7439-92-101/09/17 17:0010.0 2.5 1
Nickel ND ug/L 01/11/17 11:49 7440-02-001/09/17 17:0050.0 2.5 1
Selenium ND ug/L 01/11/17 11:49 7782-49-201/09/17 17:0010.0 5.0 1
Silver ND ug/L 01/11/17 11:49 7440-22-401/09/17 17:0010.0 2.5 1
Thallium ND ug/L 01/11/17 11:49 7440-28-001/09/17 17:005.5 5.0 1
Vanadium ND ug/L 01/11/17 11:49 7440-62-201/09/17 17:0025.0 2.5 1
Zinc 5.7J ug/L 01/11/17 11:49 7440-66-601/09/17 17:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/17 20:59 67-64-110010.0 1
Acrylonitrile ND ug/L 01/03/17 20:59 107-13-12001.9 1
Benzene 3.2 ug/L 01/03/17 20:59 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/03/17 20:59 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/03/17 20:59 75-27-41.0 0.18 1
Bromoform ND ug/L 01/03/17 20:59 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/03/17 20:59 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/03/17 20:59 78-93-31000.96 1
Carbon disulfide ND ug/L 01/03/17 20:59 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/03/17 20:59 56-23-51.0 0.25 1
Chlorobenzene 1.5J ug/L 01/03/17 20:59 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/03/17 20:59 75-00-310.0 0.54 1
Chloroform ND ug/L 01/03/17 20:59 67-66-35.0 0.14 1
Chloromethane 0.13J ug/L 01/03/17 20:59 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/17 20:59 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/03/17 20:59 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/17 20:59 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/03/17 20:59 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/03/17 20:59 95-50-15.0 0.30 1
1,4-Dichlorobenzene 2.0 ug/L 01/03/17 20:59 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/17 20:59 110-57-61001.0 1
1,1-Dichloroethane 1.7J ug/L 01/03/17 20:59 75-34-35.0 0.32 1
1,2-Dichloroethane 0.42J ug/L 01/03/17 20:59 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/03/17 20:59 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 7.6 ug/L 01/03/17 20:59 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/03/17 20:59 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/03/17 20:59 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/03/17 20:59 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/03/17 20:59 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-7 Lab ID:92325007014 Collected:12/29/16 17:10 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/03/17 20:59 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/03/17 20:59 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/03/17 20:59 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/03/17 20:59 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/17 20:59 108-10-11000.33 1
Styrene ND ug/L 01/03/17 20:59 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/17 20:59 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/17 20:59 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/03/17 20:59 127-18-41.0 0.46 1
Toluene ND ug/L 01/03/17 20:59 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/03/17 20:59 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/03/17 20:59 79-00-51.0 0.29 1
Trichloroethene 0.68J ug/L 01/03/17 20:59 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/03/17 20:59 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/03/17 20:59 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/03/17 20:59 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/03/17 20:59 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/03/17 20:59 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %01/03/17 20:59 460-00-470-130 1
1,2-Dichloroethane-d4 (S)112 %01/03/17 20:59 17060-07-070-130 1
Toluene-d8 (S)110 %01/03/17 20:59 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-6 Lab ID:92325007015 Collected:12/29/16 00:00 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: RSK 175 ModifiedRSK 175 Headspace
Methane 863 ug/L 01/06/17 14:33 74-82-8 N210.0 10.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/05/17 02:03 7440-36-001/03/17 17:006.0 3.8 1
Arsenic ND ug/L 01/05/17 02:03 7440-38-201/03/17 17:0010.0 2.5 1
Barium 88.6J ug/L 01/05/17 02:03 7440-39-301/03/17 17:001002.5 1
Beryllium ND ug/L 01/05/17 02:03 7440-41-701/03/17 17:001.0 0.50 1
Cadmium 0.73J ug/L 01/05/17 02:03 7440-43-901/03/17 17:001.0 0.50 1
Chromium 3.5J ug/L 01/05/17 02:03 7440-47-301/03/17 17:0010.0 2.5 1
Cobalt 89.4 ug/L 01/05/17 02:03 7440-48-401/03/17 17:0010.0 2.5 1
Copper 2.6J ug/L 01/05/17 02:03 7440-50-801/03/17 17:0010.0 2.5 1
Lead ND ug/L 01/05/17 02:03 7439-92-101/03/17 17:0010.0 2.5 1
Nickel 18.8J ug/L 01/05/17 02:03 7440-02-001/03/17 17:0050.0 2.5 1
Selenium ND ug/L 01/05/17 02:03 7782-49-201/03/17 17:0010.0 5.0 1
Silver ND ug/L 01/05/17 02:03 7440-22-401/03/17 17:0010.0 2.5 1
Thallium ND ug/L 01/05/17 02:03 7440-28-001/03/17 17:005.5 5.0 1
Vanadium ND ug/L 01/05/17 02:03 7440-62-201/03/17 17:0025.0 2.5 1
Zinc 36.0 ug/L 01/05/17 02:03 7440-66-601/03/17 17:0010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 01/04/17 15:33 7439-97-601/04/17 04:000.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/17 21:17 67-64-110010.0 1
Acrylonitrile ND ug/L 01/03/17 21:17 107-13-12001.9 1
Benzene 1.1 ug/L 01/03/17 21:17 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/03/17 21:17 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/03/17 21:17 75-27-41.0 0.18 1
Bromoform ND ug/L 01/03/17 21:17 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/03/17 21:17 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/03/17 21:17 78-93-31000.96 1
Carbon disulfide ND ug/L 01/03/17 21:17 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/03/17 21:17 56-23-51.0 0.25 1
Chlorobenzene 0.32J ug/L 01/03/17 21:17 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/03/17 21:17 75-00-310.0 0.54 1
Chloroform ND ug/L 01/03/17 21:17 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/03/17 21:17 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/17 21:17 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/03/17 21:17 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/17 21:17 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/03/17 21:17 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/03/17 21:17 95-50-15.0 0.30 1
1,4-Dichlorobenzene 0.96J ug/L 01/03/17 21:17 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/17 21:17 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/03/17 21:17 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/03/17 21:17 107-06-21.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-6 Lab ID:92325007015 Collected:12/29/16 00:00 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1-Dichloroethene ND ug/L 01/03/17 21:17 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 1.0J ug/L 01/03/17 21:17 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/03/17 21:17 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/03/17 21:17 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/03/17 21:17 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/03/17 21:17 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/03/17 21:17 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/03/17 21:17 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/03/17 21:17 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/03/17 21:17 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/17 21:17 108-10-11000.33 1
Styrene ND ug/L 01/03/17 21:17 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/17 21:17 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/17 21:17 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/03/17 21:17 127-18-41.0 0.46 1
Toluene ND ug/L 01/03/17 21:17 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/03/17 21:17 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/03/17 21:17 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/03/17 21:17 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/03/17 21:17 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/03/17 21:17 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/03/17 21:17 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/03/17 21:17 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/03/17 21:17 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %01/03/17 21:17 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %01/03/17 21:17 17060-07-070-130 1
Toluene-d8 (S)103 %01/03/17 21:17 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-4R Lab ID:92325007016 Collected:12/30/16 10:50 Received:01/03/17 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/06/17 16:41 7440-36-001/04/17 20:006.0 3.8 1
Arsenic 5.3J ug/L 01/06/17 16:41 7440-38-201/04/17 20:0010.0 2.5 1
Barium 124 ug/L 01/05/17 16:55 7440-39-301/04/17 20:001002.5 1
Beryllium ND ug/L 01/05/17 16:55 7440-41-701/04/17 20:001.0 0.50 1
Cadmium ND ug/L 01/05/17 16:55 7440-43-901/04/17 20:001.0 0.50 1
Chromium ND ug/L 01/05/17 16:55 7440-47-301/04/17 20:0010.0 2.5 1
Cobalt 93.7 ug/L 01/06/17 16:41 7440-48-401/04/17 20:0010.0 2.5 1
Copper ND ug/L 01/06/17 16:41 7440-50-801/04/17 20:0010.0 2.5 1
Lead ND ug/L 01/06/17 16:41 7439-92-101/04/17 20:0010.0 2.5 1
Nickel 5.2J ug/L 01/05/17 16:55 7440-02-001/04/17 20:0050.0 2.5 1
Selenium ND ug/L 01/06/17 16:41 7782-49-201/04/17 20:0010.0 5.0 1
Silver ND ug/L 01/05/17 16:55 7440-22-401/04/17 20:0010.0 2.5 1
Thallium ND ug/L 01/05/17 16:55 7440-28-001/04/17 20:005.5 5.0 1
Vanadium ND ug/L 01/05/17 16:55 7440-62-201/04/17 20:0025.0 2.5 1
Zinc 19.7 ug/L 01/06/17 16:41 7440-66-601/04/17 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/04/17 12:39 67-64-110010.0 1
Acrylonitrile ND ug/L 01/04/17 12:39 107-13-12001.9 1
Benzene 1.3 ug/L 01/04/17 12:39 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/04/17 12:39 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/04/17 12:39 75-27-41.0 0.18 1
Bromoform ND ug/L 01/04/17 12:39 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/04/17 12:39 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/04/17 12:39 78-93-31000.96 1
Carbon disulfide ND ug/L 01/04/17 12:39 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/04/17 12:39 56-23-51.0 0.25 1
Chlorobenzene 1.5J ug/L 01/04/17 12:39 108-90-73.0 0.23 1
Chloroethane 1.3J ug/L 01/04/17 12:39 75-00-310.0 0.54 1
Chloroform ND ug/L 01/04/17 12:39 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/04/17 12:39 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/04/17 12:39 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/04/17 12:39 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/04/17 12:39 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/04/17 12:39 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/04/17 12:39 95-50-15.0 0.30 1
1,4-Dichlorobenzene 4.1 ug/L 01/04/17 12:39 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/04/17 12:39 110-57-61001.0 1
1,1-Dichloroethane 2.3J ug/L 01/04/17 12:39 75-34-35.0 0.32 1
1,2-Dichloroethane 0.31J ug/L 01/04/17 12:39 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/04/17 12:39 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 13.5 ug/L 01/04/17 12:39 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/04/17 12:39 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/04/17 12:39 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/04/17 12:39 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/04/17 12:39 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-4R Lab ID:92325007016 Collected:12/30/16 10:50 Received:01/03/17 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/04/17 12:39 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/04/17 12:39 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/04/17 12:39 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/04/17 12:39 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/04/17 12:39 108-10-11000.33 1
Styrene ND ug/L 01/04/17 12:39 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/04/17 12:39 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/04/17 12:39 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/04/17 12:39 127-18-41.0 0.46 1
Toluene ND ug/L 01/04/17 12:39 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/04/17 12:39 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/04/17 12:39 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/04/17 12:39 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/04/17 12:39 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/04/17 12:39 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/04/17 12:39 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/04/17 12:39 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/04/17 12:39 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %01/04/17 12:39 460-00-470-130 1
1,2-Dichloroethane-d4 (S)113 %01/04/17 12:39 17060-07-070-130 1
Toluene-d8 (S)107 %01/04/17 12:39 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-5 Lab ID:92325007017 Collected:12/30/16 11:35 Received:01/03/17 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: RSK 175 ModifiedRSK 175 Headspace
Methane 5260 ug/L 01/06/17 14:48 74-82-8 N210.0 10.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/06/17 16:45 7440-36-001/04/17 20:006.0 3.8 1
Arsenic 4.8J ug/L 01/06/17 16:45 7440-38-201/04/17 20:0010.0 2.5 1
Barium 55.2J ug/L 01/05/17 16:59 7440-39-301/04/17 20:001002.5 1
Beryllium ND ug/L 01/05/17 16:59 7440-41-701/04/17 20:001.0 0.50 1
Cadmium ND ug/L 01/05/17 16:59 7440-43-901/04/17 20:001.0 0.50 1
Chromium ND ug/L 01/05/17 16:59 7440-47-301/04/17 20:0010.0 2.5 1
Cobalt ND ug/L 01/06/17 16:45 7440-48-401/04/17 20:0010.0 2.5 1
Copper ND ug/L 01/06/17 16:45 7440-50-801/04/17 20:0010.0 2.5 1
Lead ND ug/L 01/06/17 16:45 7439-92-101/04/17 20:0010.0 2.5 1
Nickel ND ug/L 01/05/17 16:59 7440-02-001/04/17 20:0050.0 2.5 1
Selenium ND ug/L 01/06/17 16:45 7782-49-201/04/17 20:0010.0 5.0 1
Silver ND ug/L 01/05/17 16:59 7440-22-401/04/17 20:0010.0 2.5 1
Thallium ND ug/L 01/05/17 16:59 7440-28-001/04/17 20:005.5 5.0 1
Vanadium ND ug/L 01/05/17 16:59 7440-62-201/04/17 20:0025.0 2.5 1
Zinc 33.8 ug/L 01/06/17 16:45 7440-66-601/04/17 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/04/17 12:56 67-64-110010.0 1
Acrylonitrile ND ug/L 01/04/17 12:56 107-13-12001.9 1
Benzene 2.5 ug/L 01/04/17 12:56 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/04/17 12:56 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/04/17 12:56 75-27-41.0 0.18 1
Bromoform ND ug/L 01/04/17 12:56 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/04/17 12:56 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/04/17 12:56 78-93-31000.96 1
Carbon disulfide ND ug/L 01/04/17 12:56 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/04/17 12:56 56-23-51.0 0.25 1
Chlorobenzene 0.69J ug/L 01/04/17 12:56 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/04/17 12:56 75-00-310.0 0.54 1
Chloroform ND ug/L 01/04/17 12:56 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/04/17 12:56 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/04/17 12:56 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/04/17 12:56 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/04/17 12:56 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/04/17 12:56 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/04/17 12:56 95-50-15.0 0.30 1
1,4-Dichlorobenzene 2.1 ug/L 01/04/17 12:56 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/04/17 12:56 110-57-61001.0 1
1,1-Dichloroethane 4.6J ug/L 01/04/17 12:56 75-34-35.0 0.32 1
1,2-Dichloroethane 0.27J ug/L 01/04/17 12:56 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/04/17 12:56 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 13.1 ug/L 01/04/17 12:56 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/04/17 12:56 156-60-55.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-5 Lab ID:92325007017 Collected:12/30/16 11:35 Received:01/03/17 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane 0.39J ug/L 01/04/17 12:56 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/04/17 12:56 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/04/17 12:56 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/04/17 12:56 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/04/17 12:56 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/04/17 12:56 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/04/17 12:56 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/04/17 12:56 108-10-11000.33 1
Styrene ND ug/L 01/04/17 12:56 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/04/17 12:56 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/04/17 12:56 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/04/17 12:56 127-18-41.0 0.46 1
Toluene ND ug/L 01/04/17 12:56 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/04/17 12:56 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/04/17 12:56 79-00-51.0 0.29 1
Trichloroethene 0.71J ug/L 01/04/17 12:56 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/04/17 12:56 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/04/17 12:56 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/04/17 12:56 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/04/17 12:56 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/04/17 12:56 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %01/04/17 12:56 460-00-470-130 1
1,2-Dichloroethane-d4 (S)111 %01/04/17 12:56 17060-07-070-130 1
Toluene-d8 (S)105 %01/04/17 12:56 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-9 Lab ID:92325007018 Collected:12/30/16 12:05 Received:01/03/17 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/06/17 16:48 7440-36-001/04/17 20:006.0 3.8 1
Arsenic ND ug/L 01/06/17 16:48 7440-38-201/04/17 20:0010.0 2.5 1
Barium 170 ug/L 01/05/17 17:02 7440-39-301/04/17 20:001002.5 1
Beryllium ND ug/L 01/05/17 17:02 7440-41-701/04/17 20:001.0 0.50 1
Cadmium ND ug/L 01/05/17 17:02 7440-43-901/04/17 20:001.0 0.50 1
Chromium 3.0J ug/L 01/05/17 17:02 7440-47-301/04/17 20:0010.0 2.5 1
Cobalt 197 ug/L 01/06/17 16:48 7440-48-401/04/17 20:0010.0 2.5 1
Copper ND ug/L 01/06/17 16:48 7440-50-801/04/17 20:0010.0 2.5 1
Lead ND ug/L 01/06/17 16:48 7439-92-101/04/17 20:0010.0 2.5 1
Nickel 69.1 ug/L 01/05/17 17:02 7440-02-001/04/17 20:0050.0 2.5 1
Selenium ND ug/L 01/06/17 16:48 7782-49-201/04/17 20:0010.0 5.0 1
Silver ND ug/L 01/05/17 17:02 7440-22-401/04/17 20:0010.0 2.5 1
Thallium ND ug/L 01/05/17 17:02 7440-28-001/04/17 20:005.5 5.0 1
Vanadium ND ug/L 01/05/17 17:02 7440-62-201/04/17 20:0025.0 2.5 1
Zinc 15.6 ug/L 01/06/17 16:48 7440-66-601/04/17 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/04/17 13:13 67-64-110010.0 1
Acrylonitrile ND ug/L 01/04/17 13:13 107-13-12001.9 1
Benzene ND ug/L 01/04/17 13:13 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/04/17 13:13 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/04/17 13:13 75-27-41.0 0.18 1
Bromoform ND ug/L 01/04/17 13:13 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/04/17 13:13 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/04/17 13:13 78-93-31000.96 1
Carbon disulfide ND ug/L 01/04/17 13:13 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/04/17 13:13 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/04/17 13:13 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/04/17 13:13 75-00-310.0 0.54 1
Chloroform ND ug/L 01/04/17 13:13 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/04/17 13:13 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/04/17 13:13 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/04/17 13:13 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/04/17 13:13 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/04/17 13:13 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/04/17 13:13 95-50-15.0 0.30 1
1,4-Dichlorobenzene 0.37J ug/L 01/04/17 13:13 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/04/17 13:13 110-57-61001.0 1
1,1-Dichloroethane 0.53J ug/L 01/04/17 13:13 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/04/17 13:13 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/04/17 13:13 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 9.4 ug/L 01/04/17 13:13 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/04/17 13:13 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/04/17 13:13 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/04/17 13:13 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/04/17 13:13 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 44 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-9 Lab ID:92325007018 Collected:12/30/16 12:05 Received:01/03/17 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/04/17 13:13 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/04/17 13:13 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/04/17 13:13 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/04/17 13:13 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/04/17 13:13 108-10-11000.33 1
Styrene ND ug/L 01/04/17 13:13 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/04/17 13:13 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/04/17 13:13 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/04/17 13:13 127-18-41.0 0.46 1
Toluene ND ug/L 01/04/17 13:13 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/04/17 13:13 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/04/17 13:13 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/04/17 13:13 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/04/17 13:13 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/04/17 13:13 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/04/17 13:13 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/04/17 13:13 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/04/17 13:13 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)96 %01/04/17 13:13 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %01/04/17 13:13 17060-07-070-130 1
Toluene-d8 (S)109 %01/04/17 13:13 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-10 Lab ID:92325007019 Collected:12/31/16 11:00 Received:01/03/17 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/06/17 16:51 7440-36-001/04/17 20:006.0 3.8 1
Arsenic ND ug/L 01/06/17 16:51 7440-38-201/04/17 20:0010.0 2.5 1
Barium 25.9J ug/L 01/05/17 17:05 7440-39-301/04/17 20:001002.5 1
Beryllium ND ug/L 01/05/17 17:05 7440-41-701/04/17 20:001.0 0.50 1
Cadmium ND ug/L 01/05/17 17:05 7440-43-901/04/17 20:001.0 0.50 1
Chromium ND ug/L 01/05/17 17:05 7440-47-301/04/17 20:0010.0 2.5 1
Cobalt ND ug/L 01/06/17 16:51 7440-48-401/04/17 20:0010.0 2.5 1
Copper ND ug/L 01/06/17 16:51 7440-50-801/04/17 20:0010.0 2.5 1
Lead ND ug/L 01/06/17 16:51 7439-92-101/04/17 20:0010.0 2.5 1
Nickel ND ug/L 01/05/17 17:05 7440-02-001/04/17 20:0050.0 2.5 1
Selenium ND ug/L 01/06/17 16:51 7782-49-201/04/17 20:0010.0 5.0 1
Silver ND ug/L 01/05/17 17:05 7440-22-401/04/17 20:0010.0 2.5 1
Thallium ND ug/L 01/05/17 17:05 7440-28-001/04/17 20:005.5 5.0 1
Vanadium ND ug/L 01/05/17 17:05 7440-62-201/04/17 20:0025.0 2.5 1
Zinc ND ug/L 01/06/17 16:51 7440-66-601/04/17 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/04/17 14:58 67-64-110010.0 1
Acrylonitrile ND ug/L 01/04/17 14:58 107-13-12001.9 1
Benzene ND ug/L 01/04/17 14:58 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/04/17 14:58 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/04/17 14:58 75-27-41.0 0.18 1
Bromoform ND ug/L 01/04/17 14:58 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/04/17 14:58 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/04/17 14:58 78-93-31000.96 1
Carbon disulfide ND ug/L 01/04/17 14:58 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/04/17 14:58 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/04/17 14:58 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/04/17 14:58 75-00-310.0 0.54 1
Chloroform ND ug/L 01/04/17 14:58 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/04/17 14:58 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/04/17 14:58 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/04/17 14:58 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/04/17 14:58 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/04/17 14:58 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/04/17 14:58 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/04/17 14:58 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/04/17 14:58 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/04/17 14:58 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/04/17 14:58 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/04/17 14:58 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.23J ug/L 01/04/17 14:58 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/04/17 14:58 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/04/17 14:58 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/04/17 14:58 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/04/17 14:58 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-10 Lab ID:92325007019 Collected:12/31/16 11:00 Received:01/03/17 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/04/17 14:58 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/04/17 14:58 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/04/17 14:58 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/04/17 14:58 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/04/17 14:58 108-10-11000.33 1
Styrene ND ug/L 01/04/17 14:58 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/04/17 14:58 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/04/17 14:58 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/04/17 14:58 127-18-41.0 0.46 1
Toluene ND ug/L 01/04/17 14:58 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/04/17 14:58 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/04/17 14:58 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/04/17 14:58 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/04/17 14:58 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/04/17 14:58 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/04/17 14:58 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/04/17 14:58 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/04/17 14:58 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %01/04/17 14:58 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %01/04/17 14:58 17060-07-070-130 1
Toluene-d8 (S)108 %01/04/17 14:58 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-16 Lab ID:92325007020 Collected:12/31/16 11:45 Received:01/03/17 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: RSK 175 ModifiedRSK 175 Headspace
Methane 3300 ug/L 01/06/17 15:03 74-82-8 N210.0 10.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/06/17 16:54 7440-36-001/04/17 20:006.0 3.8 1
Arsenic ND ug/L 01/06/17 16:54 7440-38-201/04/17 20:0010.0 2.5 1
Barium 58.7J ug/L 01/05/17 17:08 7440-39-301/04/17 20:001002.5 1
Beryllium ND ug/L 01/05/17 17:08 7440-41-701/04/17 20:001.0 0.50 1
Cadmium ND ug/L 01/05/17 17:08 7440-43-901/04/17 20:001.0 0.50 1
Chromium ND ug/L 01/05/17 17:08 7440-47-301/04/17 20:0010.0 2.5 1
Cobalt 105 ug/L 01/06/17 16:54 7440-48-401/04/17 20:0010.0 2.5 1
Copper 7.1J ug/L 01/06/17 16:54 7440-50-801/04/17 20:0010.0 2.5 1
Lead ND ug/L 01/06/17 16:54 7439-92-101/04/17 20:0010.0 2.5 1
Nickel 7.0J ug/L 01/05/17 17:08 7440-02-001/04/17 20:0050.0 2.5 1
Selenium ND ug/L 01/06/17 16:54 7782-49-201/04/17 20:0010.0 5.0 1
Silver ND ug/L 01/05/17 17:08 7440-22-401/04/17 20:0010.0 2.5 1
Thallium ND ug/L 01/05/17 17:08 7440-28-001/04/17 20:005.5 5.0 1
Vanadium ND ug/L 01/05/17 17:08 7440-62-201/04/17 20:0025.0 2.5 1
Zinc 13.0 ug/L 01/06/17 16:54 7440-66-601/04/17 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/04/17 15:16 67-64-110010.0 1
Acrylonitrile ND ug/L 01/04/17 15:16 107-13-12001.9 1
Benzene 2.3 ug/L 01/04/17 15:16 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/04/17 15:16 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/04/17 15:16 75-27-41.0 0.18 1
Bromoform ND ug/L 01/04/17 15:16 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/04/17 15:16 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/04/17 15:16 78-93-31000.96 1
Carbon disulfide ND ug/L 01/04/17 15:16 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/04/17 15:16 56-23-51.0 0.25 1
Chlorobenzene 0.75J ug/L 01/04/17 15:16 108-90-73.0 0.23 1
Chloroethane 0.62J ug/L 01/04/17 15:16 75-00-310.0 0.54 1
Chloroform ND ug/L 01/04/17 15:16 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/04/17 15:16 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/04/17 15:16 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/04/17 15:16 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/04/17 15:16 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/04/17 15:16 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/04/17 15:16 95-50-15.0 0.30 1
1,4-Dichlorobenzene 2.3 ug/L 01/04/17 15:16 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/04/17 15:16 110-57-61001.0 1
1,1-Dichloroethane 8.0 ug/L 01/04/17 15:16 75-34-35.0 0.32 1
1,2-Dichloroethane 0.27J ug/L 01/04/17 15:16 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/04/17 15:16 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 23.3 ug/L 01/04/17 15:16 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/04/17 15:16 156-60-55.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-16 Lab ID:92325007020 Collected:12/31/16 11:45 Received:01/03/17 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane 0.83J ug/L 01/04/17 15:16 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/04/17 15:16 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/04/17 15:16 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/04/17 15:16 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/04/17 15:16 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/04/17 15:16 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/04/17 15:16 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/04/17 15:16 108-10-11000.33 1
Styrene ND ug/L 01/04/17 15:16 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/04/17 15:16 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/04/17 15:16 79-34-53.0 0.40 1
Tetrachloroethene 1.2 ug/L 01/04/17 15:16 127-18-41.0 0.46 1
Toluene ND ug/L 01/04/17 15:16 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/04/17 15:16 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/04/17 15:16 79-00-51.0 0.29 1
Trichloroethene 1.5 ug/L 01/04/17 15:16 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/04/17 15:16 75-69-4 M11.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/04/17 15:16 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/04/17 15:16 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/04/17 15:16 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/04/17 15:16 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %01/04/17 15:16 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %01/04/17 15:16 17060-07-070-130 1
Toluene-d8 (S)105 %01/04/17 15:16 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-22 Lab ID:92325007021 Collected:12/31/16 10:30 Received:01/03/17 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/06/17 16:57 7440-36-001/04/17 20:006.0 3.8 1
Arsenic ND ug/L 01/06/17 16:57 7440-38-201/04/17 20:0010.0 2.5 1
Barium 68.0J ug/L 01/05/17 17:21 7440-39-301/04/17 20:001002.5 1
Beryllium ND ug/L 01/05/17 17:21 7440-41-701/04/17 20:001.0 0.50 1
Cadmium ND ug/L 01/05/17 17:21 7440-43-901/04/17 20:001.0 0.50 1
Chromium 2.8J ug/L 01/05/17 17:21 7440-47-301/04/17 20:0010.0 2.5 1
Cobalt ND ug/L 01/06/17 16:57 7440-48-401/04/17 20:0010.0 2.5 1
Copper ND ug/L 01/06/17 16:57 7440-50-801/04/17 20:0010.0 2.5 1
Lead ND ug/L 01/06/17 16:57 7439-92-101/04/17 20:0010.0 2.5 1
Nickel ND ug/L 01/05/17 17:21 7440-02-001/04/17 20:0050.0 2.5 1
Selenium ND ug/L 01/06/17 16:57 7782-49-201/04/17 20:0010.0 5.0 1
Silver ND ug/L 01/05/17 17:21 7440-22-401/04/17 20:0010.0 2.5 1
Thallium ND ug/L 01/05/17 17:21 7440-28-001/04/17 20:005.5 5.0 1
Vanadium ND ug/L 01/05/17 17:21 7440-62-201/04/17 20:0025.0 2.5 1
Zinc 7.2J ug/L 01/06/17 16:57 7440-66-601/04/17 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/04/17 15:33 67-64-110010.0 1
Acrylonitrile ND ug/L 01/04/17 15:33 107-13-12001.9 1
Benzene ND ug/L 01/04/17 15:33 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/04/17 15:33 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/04/17 15:33 75-27-41.0 0.18 1
Bromoform ND ug/L 01/04/17 15:33 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/04/17 15:33 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/04/17 15:33 78-93-31000.96 1
Carbon disulfide ND ug/L 01/04/17 15:33 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/04/17 15:33 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/04/17 15:33 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/04/17 15:33 75-00-310.0 0.54 1
Chloroform ND ug/L 01/04/17 15:33 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/04/17 15:33 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/04/17 15:33 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/04/17 15:33 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/04/17 15:33 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/04/17 15:33 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/04/17 15:33 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/04/17 15:33 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/04/17 15:33 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/04/17 15:33 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/04/17 15:33 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/04/17 15:33 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/04/17 15:33 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/04/17 15:33 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/04/17 15:33 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/04/17 15:33 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/04/17 15:33 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 50 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-22 Lab ID:92325007021 Collected:12/31/16 10:30 Received:01/03/17 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/04/17 15:33 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/04/17 15:33 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/04/17 15:33 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/04/17 15:33 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/04/17 15:33 108-10-11000.33 1
Styrene ND ug/L 01/04/17 15:33 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/04/17 15:33 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/04/17 15:33 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/04/17 15:33 127-18-41.0 0.46 1
Toluene ND ug/L 01/04/17 15:33 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/04/17 15:33 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/04/17 15:33 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/04/17 15:33 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/04/17 15:33 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/04/17 15:33 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/04/17 15:33 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/04/17 15:33 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/04/17 15:33 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)95 %01/04/17 15:33 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %01/04/17 15:33 17060-07-070-130 1
Toluene-d8 (S)107 %01/04/17 15:33 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 51 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-23 Lab ID:92325007022 Collected:12/31/16 11:20 Received:01/03/17 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/06/17 17:01 7440-36-001/04/17 20:006.0 3.8 1
Arsenic 3.4J ug/L 01/06/17 17:01 7440-38-201/04/17 20:0010.0 2.5 1
Barium 52.2J ug/L 01/05/17 17:24 7440-39-301/04/17 20:001002.5 1
Beryllium ND ug/L 01/05/17 17:24 7440-41-701/04/17 20:001.0 0.50 1
Cadmium ND ug/L 01/05/17 17:24 7440-43-901/04/17 20:001.0 0.50 1
Chromium ND ug/L 01/05/17 17:24 7440-47-301/04/17 20:0010.0 2.5 1
Cobalt ND ug/L 01/06/17 17:01 7440-48-401/04/17 20:0010.0 2.5 1
Copper ND ug/L 01/06/17 17:01 7440-50-801/04/17 20:0010.0 2.5 1
Lead ND ug/L 01/06/17 17:01 7439-92-101/04/17 20:0010.0 2.5 1
Nickel 2.8J ug/L 01/05/17 17:24 7440-02-001/04/17 20:0050.0 2.5 1
Selenium ND ug/L 01/06/17 17:01 7782-49-201/04/17 20:0010.0 5.0 1
Silver ND ug/L 01/05/17 17:24 7440-22-401/04/17 20:0010.0 2.5 1
Thallium ND ug/L 01/05/17 17:24 7440-28-001/04/17 20:005.5 5.0 1
Vanadium ND ug/L 01/05/17 17:24 7440-62-201/04/17 20:0025.0 2.5 1
Zinc 5.8J ug/L 01/06/17 17:01 7440-66-601/04/17 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/04/17 15:50 67-64-110010.0 1
Acrylonitrile ND ug/L 01/04/17 15:50 107-13-12001.9 1
Benzene ND ug/L 01/04/17 15:50 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/04/17 15:50 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/04/17 15:50 75-27-41.0 0.18 1
Bromoform ND ug/L 01/04/17 15:50 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/04/17 15:50 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/04/17 15:50 78-93-31000.96 1
Carbon disulfide ND ug/L 01/04/17 15:50 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/04/17 15:50 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/04/17 15:50 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/04/17 15:50 75-00-310.0 0.54 1
Chloroform ND ug/L 01/04/17 15:50 67-66-35.0 0.14 1
Chloromethane 0.12J ug/L 01/04/17 15:50 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/04/17 15:50 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/04/17 15:50 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/04/17 15:50 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/04/17 15:50 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/04/17 15:50 95-50-15.0 0.30 1
1,4-Dichlorobenzene 0.34J ug/L 01/04/17 15:50 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/04/17 15:50 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/04/17 15:50 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/04/17 15:50 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/04/17 15:50 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 1.6J ug/L 01/04/17 15:50 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/04/17 15:50 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/04/17 15:50 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/04/17 15:50 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/04/17 15:50 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-23 Lab ID:92325007022 Collected:12/31/16 11:20 Received:01/03/17 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/04/17 15:50 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/04/17 15:50 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/04/17 15:50 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/04/17 15:50 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/04/17 15:50 108-10-11000.33 1
Styrene ND ug/L 01/04/17 15:50 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/04/17 15:50 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/04/17 15:50 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/04/17 15:50 127-18-41.0 0.46 1
Toluene ND ug/L 01/04/17 15:50 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/04/17 15:50 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/04/17 15:50 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/04/17 15:50 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/04/17 15:50 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/04/17 15:50 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/04/17 15:50 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/04/17 15:50 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/04/17 15:50 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)95 %01/04/17 15:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)111 %01/04/17 15:50 17060-07-070-130 1
Toluene-d8 (S)114 %01/04/17 15:50 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-32 Lab ID:92325007023 Collected:12/31/16 08:35 Received:01/03/17 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/06/17 17:04 7440-36-001/04/17 20:006.0 3.8 1
Arsenic ND ug/L 01/06/17 17:04 7440-38-201/04/17 20:0010.0 2.5 1
Barium 11.3J ug/L 01/05/17 17:27 7440-39-301/04/17 20:001002.5 1
Beryllium ND ug/L 01/05/17 17:27 7440-41-701/04/17 20:001.0 0.50 1
Cadmium 0.60J ug/L 01/05/17 17:27 7440-43-901/04/17 20:001.0 0.50 1
Chromium ND ug/L 01/05/17 17:27 7440-47-301/04/17 20:0010.0 2.5 1
Cobalt ND ug/L 01/06/17 17:04 7440-48-401/04/17 20:0010.0 2.5 1
Copper ND ug/L 01/06/17 17:04 7440-50-801/04/17 20:0010.0 2.5 1
Lead ND ug/L 01/06/17 17:04 7439-92-101/04/17 20:0010.0 2.5 1
Nickel 2.7J ug/L 01/05/17 17:27 7440-02-001/04/17 20:0050.0 2.5 1
Selenium ND ug/L 01/06/17 17:04 7782-49-201/04/17 20:0010.0 5.0 1
Silver ND ug/L 01/05/17 17:27 7440-22-401/04/17 20:0010.0 2.5 1
Thallium ND ug/L 01/05/17 17:27 7440-28-001/04/17 20:005.5 5.0 1
Vanadium ND ug/L 01/05/17 17:27 7440-62-201/04/17 20:0025.0 2.5 1
Zinc 5.0J ug/L 01/06/17 17:04 7440-66-601/04/17 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/04/17 16:08 67-64-110010.0 1
Acrylonitrile ND ug/L 01/04/17 16:08 107-13-12001.9 1
Benzene ND ug/L 01/04/17 16:08 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/04/17 16:08 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/04/17 16:08 75-27-41.0 0.18 1
Bromoform ND ug/L 01/04/17 16:08 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/04/17 16:08 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/04/17 16:08 78-93-31000.96 1
Carbon disulfide ND ug/L 01/04/17 16:08 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/04/17 16:08 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/04/17 16:08 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/04/17 16:08 75-00-310.0 0.54 1
Chloroform ND ug/L 01/04/17 16:08 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/04/17 16:08 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/04/17 16:08 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/04/17 16:08 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/04/17 16:08 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/04/17 16:08 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/04/17 16:08 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/04/17 16:08 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/04/17 16:08 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/04/17 16:08 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/04/17 16:08 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/04/17 16:08 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/04/17 16:08 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/04/17 16:08 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/04/17 16:08 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/04/17 16:08 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/04/17 16:08 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-32 Lab ID:92325007023 Collected:12/31/16 08:35 Received:01/03/17 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/04/17 16:08 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/04/17 16:08 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/04/17 16:08 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/04/17 16:08 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/04/17 16:08 108-10-11000.33 1
Styrene ND ug/L 01/04/17 16:08 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/04/17 16:08 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/04/17 16:08 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/04/17 16:08 127-18-41.0 0.46 1
Toluene ND ug/L 01/04/17 16:08 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/04/17 16:08 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/04/17 16:08 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/04/17 16:08 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/04/17 16:08 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/04/17 16:08 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/04/17 16:08 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/04/17 16:08 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/04/17 16:08 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)96 %01/04/17 16:08 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %01/04/17 16:08 17060-07-070-130 1
Toluene-d8 (S)119 %01/04/17 16:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-33 Lab ID:92325007024 Collected:12/30/16 08:30 Received:01/03/17 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/06/17 17:16 7440-36-001/04/17 20:006.0 3.8 1
Arsenic ND ug/L 01/06/17 17:16 7440-38-201/04/17 20:0010.0 2.5 1
Barium 32.4J ug/L 01/05/17 17:30 7440-39-301/04/17 20:001002.5 1
Beryllium ND ug/L 01/05/17 17:30 7440-41-701/04/17 20:001.0 0.50 1
Cadmium ND ug/L 01/05/17 17:30 7440-43-901/04/17 20:001.0 0.50 1
Chromium ND ug/L 01/05/17 17:30 7440-47-301/04/17 20:0010.0 2.5 1
Cobalt 11.8 ug/L 01/06/17 17:16 7440-48-401/04/17 20:0010.0 2.5 1
Copper 5.9J ug/L 01/06/17 17:16 7440-50-801/04/17 20:0010.0 2.5 1
Lead ND ug/L 01/06/17 17:16 7439-92-101/04/17 20:0010.0 2.5 1
Nickel 9.7J ug/L 01/05/17 17:30 7440-02-001/04/17 20:0050.0 2.5 1
Selenium ND ug/L 01/06/17 17:16 7782-49-201/04/17 20:0010.0 5.0 1
Silver ND ug/L 01/05/17 17:30 7440-22-401/04/17 20:0010.0 2.5 1
Thallium ND ug/L 01/05/17 17:30 7440-28-001/04/17 20:005.5 5.0 1
Vanadium ND ug/L 01/05/17 17:30 7440-62-201/04/17 20:0025.0 2.5 1
Zinc 7.0J ug/L 01/06/17 17:16 7440-66-601/04/17 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/04/17 13:31 67-64-110010.0 1
Acrylonitrile ND ug/L 01/04/17 13:31 107-13-12001.9 1
Benzene ND ug/L 01/04/17 13:31 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/04/17 13:31 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/04/17 13:31 75-27-41.0 0.18 1
Bromoform ND ug/L 01/04/17 13:31 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/04/17 13:31 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/04/17 13:31 78-93-31000.96 1
Carbon disulfide ND ug/L 01/04/17 13:31 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/04/17 13:31 56-23-51.0 0.25 1
Chlorobenzene 0.24J ug/L 01/04/17 13:31 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/04/17 13:31 75-00-310.0 0.54 1
Chloroform ND ug/L 01/04/17 13:31 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/04/17 13:31 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/04/17 13:31 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/04/17 13:31 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/04/17 13:31 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/04/17 13:31 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/04/17 13:31 95-50-15.0 0.30 1
1,4-Dichlorobenzene 0.75J ug/L 01/04/17 13:31 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/04/17 13:31 110-57-61001.0 1
1,1-Dichloroethane 1.7J ug/L 01/04/17 13:31 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/04/17 13:31 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/04/17 13:31 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 4.4J ug/L 01/04/17 13:31 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/04/17 13:31 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/04/17 13:31 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/04/17 13:31 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/04/17 13:31 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 56 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-33 Lab ID:92325007024 Collected:12/30/16 08:30 Received:01/03/17 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/04/17 13:31 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/04/17 13:31 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/04/17 13:31 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/04/17 13:31 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/04/17 13:31 108-10-11000.33 1
Styrene ND ug/L 01/04/17 13:31 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/04/17 13:31 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/04/17 13:31 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/04/17 13:31 127-18-41.0 0.46 1
Toluene ND ug/L 01/04/17 13:31 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/04/17 13:31 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/04/17 13:31 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/04/17 13:31 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/04/17 13:31 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/04/17 13:31 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/04/17 13:31 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/04/17 13:31 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/04/17 13:31 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %01/04/17 13:31 460-00-470-130 1
1,2-Dichloroethane-d4 (S)113 %01/04/17 13:31 17060-07-070-130 1
Toluene-d8 (S)111 %01/04/17 13:31 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 57 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-34 Lab ID:92325007025 Collected:12/30/16 09:00 Received:01/03/17 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/06/17 17:19 7440-36-001/04/17 20:006.0 3.8 1
Arsenic 4.1J ug/L 01/06/17 17:19 7440-38-201/04/17 20:0010.0 2.5 1
Barium 21.1J ug/L 01/05/17 17:33 7440-39-301/04/17 20:001002.5 1
Beryllium ND ug/L 01/05/17 17:33 7440-41-701/04/17 20:001.0 0.50 1
Cadmium ND ug/L 01/05/17 17:33 7440-43-901/04/17 20:001.0 0.50 1
Chromium ND ug/L 01/05/17 17:33 7440-47-301/04/17 20:0010.0 2.5 1
Cobalt ND ug/L 01/06/17 17:19 7440-48-401/04/17 20:0010.0 2.5 1
Copper ND ug/L 01/06/17 17:19 7440-50-801/04/17 20:0010.0 2.5 1
Lead ND ug/L 01/06/17 17:19 7439-92-101/04/17 20:0010.0 2.5 1
Nickel ND ug/L 01/05/17 17:33 7440-02-001/04/17 20:0050.0 2.5 1
Selenium ND ug/L 01/06/17 17:19 7782-49-201/04/17 20:0010.0 5.0 1
Silver ND ug/L 01/05/17 17:33 7440-22-401/04/17 20:0010.0 2.5 1
Thallium ND ug/L 01/05/17 17:33 7440-28-001/04/17 20:005.5 5.0 1
Vanadium ND ug/L 01/05/17 17:33 7440-62-201/04/17 20:0025.0 2.5 1
Zinc 9.2J ug/L 01/06/17 17:19 7440-66-601/04/17 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/04/17 13:48 67-64-110010.0 1
Acrylonitrile ND ug/L 01/04/17 13:48 107-13-12001.9 1
Benzene ND ug/L 01/04/17 13:48 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/04/17 13:48 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/04/17 13:48 75-27-41.0 0.18 1
Bromoform ND ug/L 01/04/17 13:48 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/04/17 13:48 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/04/17 13:48 78-93-31000.96 1
Carbon disulfide ND ug/L 01/04/17 13:48 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/04/17 13:48 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/04/17 13:48 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/04/17 13:48 75-00-310.0 0.54 1
Chloroform ND ug/L 01/04/17 13:48 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/04/17 13:48 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/04/17 13:48 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/04/17 13:48 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/04/17 13:48 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/04/17 13:48 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/04/17 13:48 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/04/17 13:48 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/04/17 13:48 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/04/17 13:48 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/04/17 13:48 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/04/17 13:48 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/04/17 13:48 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/04/17 13:48 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/04/17 13:48 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/04/17 13:48 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/04/17 13:48 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:MW-34 Lab ID:92325007025 Collected:12/30/16 09:00 Received:01/03/17 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/04/17 13:48 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/04/17 13:48 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/04/17 13:48 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/04/17 13:48 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/04/17 13:48 108-10-11000.33 1
Styrene ND ug/L 01/04/17 13:48 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/04/17 13:48 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/04/17 13:48 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/04/17 13:48 127-18-41.0 0.46 1
Toluene ND ug/L 01/04/17 13:48 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/04/17 13:48 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/04/17 13:48 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/04/17 13:48 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/04/17 13:48 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/04/17 13:48 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/04/17 13:48 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/04/17 13:48 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/04/17 13:48 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %01/04/17 13:48 460-00-470-130 1
1,2-Dichloroethane-d4 (S)112 %01/04/17 13:48 17060-07-070-130 1
Toluene-d8 (S)109 %01/04/17 13:48 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:SW-3 Lab ID:92325007026 Collected:12/30/16 10:00 Received:01/03/17 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/06/17 17:29 7440-36-001/04/17 20:006.0 3.8 1
Arsenic 2.6J ug/L 01/06/17 17:29 7440-38-201/04/17 20:0010.0 2.5 1
Barium 65.5J ug/L 01/05/17 17:49 7440-39-301/04/17 20:001002.5 1
Beryllium ND ug/L 01/05/17 17:49 7440-41-701/04/17 20:001.0 0.50 1
Cadmium ND ug/L 01/05/17 17:49 7440-43-901/04/17 20:001.0 0.50 1
Chromium 4.0J ug/L 01/05/17 17:49 7440-47-301/04/17 20:0010.0 2.5 1
Cobalt 6.1J ug/L 01/06/17 17:29 7440-48-401/04/17 20:0010.0 2.5 1
Copper ND ug/L 01/06/17 17:29 7440-50-801/04/17 20:0010.0 2.5 1
Lead ND ug/L 01/06/17 17:29 7439-92-101/04/17 20:0010.0 2.5 1
Nickel 4.9J ug/L 01/05/17 17:49 7440-02-001/04/17 20:0050.0 2.5 1
Selenium ND ug/L 01/06/17 17:29 7782-49-201/04/17 20:0010.0 5.0 1
Silver ND ug/L 01/05/17 17:49 7440-22-401/04/17 20:0010.0 2.5 1
Thallium 5.6 ug/L 01/05/17 17:49 7440-28-001/04/17 20:005.5 5.0 1
Vanadium 3.5J ug/L 01/05/17 17:49 7440-62-201/04/17 20:0025.0 2.5 1
Zinc 7.2J ug/L 01/06/17 17:29 7440-66-601/04/17 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/04/17 14:06 67-64-110010.0 1
Acrylonitrile ND ug/L 01/04/17 14:06 107-13-12001.9 1
Benzene ND ug/L 01/04/17 14:06 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/04/17 14:06 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/04/17 14:06 75-27-41.0 0.18 1
Bromoform ND ug/L 01/04/17 14:06 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/04/17 14:06 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/04/17 14:06 78-93-31000.96 1
Carbon disulfide ND ug/L 01/04/17 14:06 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/04/17 14:06 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/04/17 14:06 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/04/17 14:06 75-00-310.0 0.54 1
Chloroform ND ug/L 01/04/17 14:06 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/04/17 14:06 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/04/17 14:06 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/04/17 14:06 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/04/17 14:06 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/04/17 14:06 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/04/17 14:06 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/04/17 14:06 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/04/17 14:06 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/04/17 14:06 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/04/17 14:06 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/04/17 14:06 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.53J ug/L 01/04/17 14:06 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/04/17 14:06 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/04/17 14:06 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/04/17 14:06 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/04/17 14:06 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:SW-3 Lab ID:92325007026 Collected:12/30/16 10:00 Received:01/03/17 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/04/17 14:06 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/04/17 14:06 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/04/17 14:06 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/04/17 14:06 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/04/17 14:06 108-10-11000.33 1
Styrene ND ug/L 01/04/17 14:06 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/04/17 14:06 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/04/17 14:06 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/04/17 14:06 127-18-41.0 0.46 1
Toluene ND ug/L 01/04/17 14:06 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/04/17 14:06 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/04/17 14:06 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/04/17 14:06 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/04/17 14:06 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/04/17 14:06 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/04/17 14:06 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/04/17 14:06 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/04/17 14:06 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %01/04/17 14:06 460-00-470-130 1
1,2-Dichloroethane-d4 (S)111 %01/04/17 14:06 17060-07-070-130 1
Toluene-d8 (S)108 %01/04/17 14:06 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:SW-4R Lab ID:92325007027 Collected:12/31/16 11:05 Received:01/03/17 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/05/17 18:07 7440-36-001/04/17 20:006.0 3.8 1
Arsenic 5.4J ug/L 01/06/17 17:38 7440-38-201/04/17 20:0010.0 2.5 1
Barium 34.9J ug/L 01/05/17 18:07 7440-39-301/04/17 20:001002.5 1
Beryllium ND ug/L 01/05/17 18:07 7440-41-701/04/17 20:001.0 0.50 1
Cadmium 1.2 ug/L 01/05/17 18:07 7440-43-901/04/17 20:001.0 0.50 1
Chromium 2.9J ug/L 01/05/17 18:07 7440-47-301/04/17 20:0010.0 2.5 1
Cobalt ND ug/L 01/05/17 18:07 7440-48-401/04/17 20:0010.0 2.5 1
Copper ND ug/L 01/05/17 18:07 7440-50-801/04/17 20:0010.0 2.5 1
Lead ND ug/L 01/05/17 18:07 7439-92-101/04/17 20:0010.0 2.5 1
Nickel ND ug/L 01/05/17 18:07 7440-02-001/04/17 20:0050.0 2.5 1
Selenium ND ug/L 01/05/17 18:07 7782-49-201/04/17 20:0010.0 5.0 1
Silver ND ug/L 01/05/17 18:07 7440-22-401/04/17 20:0010.0 2.5 1
Thallium 5.8 ug/L 01/05/17 18:07 7440-28-001/04/17 20:005.5 5.0 1
Vanadium 2.6J ug/L 01/05/17 18:07 7440-62-201/04/17 20:0025.0 2.5 1
Zinc 6.4J ug/L 01/05/17 18:07 7440-66-601/04/17 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/04/17 16:25 67-64-110010.0 1
Acrylonitrile ND ug/L 01/04/17 16:25 107-13-12001.9 1
Benzene ND ug/L 01/04/17 16:25 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/04/17 16:25 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/04/17 16:25 75-27-41.0 0.18 1
Bromoform ND ug/L 01/04/17 16:25 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/04/17 16:25 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/04/17 16:25 78-93-31000.96 1
Carbon disulfide ND ug/L 01/04/17 16:25 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/04/17 16:25 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/04/17 16:25 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/04/17 16:25 75-00-310.0 0.54 1
Chloroform ND ug/L 01/04/17 16:25 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/04/17 16:25 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/04/17 16:25 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/04/17 16:25 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/04/17 16:25 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/04/17 16:25 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/04/17 16:25 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/04/17 16:25 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/04/17 16:25 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/04/17 16:25 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/04/17 16:25 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/04/17 16:25 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/04/17 16:25 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/04/17 16:25 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/04/17 16:25 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/04/17 16:25 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/04/17 16:25 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
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Page 62 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:SW-4R Lab ID:92325007027 Collected:12/31/16 11:05 Received:01/03/17 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/04/17 16:25 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/04/17 16:25 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/04/17 16:25 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/04/17 16:25 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/04/17 16:25 108-10-11000.33 1
Styrene ND ug/L 01/04/17 16:25 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/04/17 16:25 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/04/17 16:25 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/04/17 16:25 127-18-41.0 0.46 1
Toluene ND ug/L 01/04/17 16:25 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/04/17 16:25 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/04/17 16:25 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/04/17 16:25 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/04/17 16:25 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/04/17 16:25 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/04/17 16:25 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/04/17 16:25 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/04/17 16:25 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %01/04/17 16:25 460-00-470-130 1
1,2-Dichloroethane-d4 (S)111 %01/04/17 16:25 17060-07-070-130 1
Toluene-d8 (S)106 %01/04/17 16:25 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 63 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:SW-5 Lab ID:92325007028 Collected:12/30/16 09:25 Received:01/03/17 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/05/17 18:10 7440-36-001/04/17 20:006.0 3.8 1
Arsenic ND ug/L 01/06/17 17:41 7440-38-201/04/17 20:0010.0 2.5 1
Barium 33.8J ug/L 01/05/17 18:10 7440-39-301/04/17 20:001002.5 1
Beryllium ND ug/L 01/05/17 18:10 7440-41-701/04/17 20:001.0 0.50 1
Cadmium 0.50J ug/L 01/05/17 18:10 7440-43-901/04/17 20:001.0 0.50 1
Chromium ND ug/L 01/05/17 18:10 7440-47-301/04/17 20:0010.0 2.5 1
Cobalt ND ug/L 01/05/17 18:10 7440-48-401/04/17 20:0010.0 2.5 1
Copper ND ug/L 01/05/17 18:10 7440-50-801/04/17 20:0010.0 2.5 1
Lead ND ug/L 01/05/17 18:10 7439-92-101/04/17 20:0010.0 2.5 1
Nickel ND ug/L 01/05/17 18:10 7440-02-001/04/17 20:0050.0 2.5 1
Selenium ND ug/L 01/05/17 18:10 7782-49-201/04/17 20:0010.0 5.0 1
Silver ND ug/L 01/05/17 18:10 7440-22-401/04/17 20:0010.0 2.5 1
Thallium ND ug/L 01/05/17 18:10 7440-28-001/04/17 20:005.5 5.0 1
Vanadium ND ug/L 01/05/17 18:10 7440-62-201/04/17 20:0025.0 2.5 1
Zinc ND ug/L 01/05/17 18:10 7440-66-601/04/17 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/04/17 14:23 67-64-110010.0 1
Acrylonitrile ND ug/L 01/04/17 14:23 107-13-12001.9 1
Benzene ND ug/L 01/04/17 14:23 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/04/17 14:23 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/04/17 14:23 75-27-41.0 0.18 1
Bromoform ND ug/L 01/04/17 14:23 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/04/17 14:23 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/04/17 14:23 78-93-31000.96 1
Carbon disulfide ND ug/L 01/04/17 14:23 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/04/17 14:23 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/04/17 14:23 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/04/17 14:23 75-00-310.0 0.54 1
Chloroform ND ug/L 01/04/17 14:23 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/04/17 14:23 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/04/17 14:23 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/04/17 14:23 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/04/17 14:23 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/04/17 14:23 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/04/17 14:23 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/04/17 14:23 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/04/17 14:23 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/04/17 14:23 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/04/17 14:23 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/04/17 14:23 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/04/17 14:23 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/04/17 14:23 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/04/17 14:23 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/04/17 14:23 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/04/17 14:23 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:SW-5 Lab ID:92325007028 Collected:12/30/16 09:25 Received:01/03/17 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/04/17 14:23 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/04/17 14:23 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/04/17 14:23 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/04/17 14:23 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/04/17 14:23 108-10-11000.33 1
Styrene ND ug/L 01/04/17 14:23 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/04/17 14:23 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/04/17 14:23 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/04/17 14:23 127-18-41.0 0.46 1
Toluene ND ug/L 01/04/17 14:23 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/04/17 14:23 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/04/17 14:23 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/04/17 14:23 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/04/17 14:23 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/04/17 14:23 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/04/17 14:23 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/04/17 14:23 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/04/17 14:23 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %01/04/17 14:23 460-00-470-130 1
1,2-Dichloroethane-d4 (S)114 %01/04/17 14:23 17060-07-070-130 1
Toluene-d8 (S)109 %01/04/17 14:23 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:SW-6 Lab ID:92325007029 Collected:12/30/16 09:40 Received:01/03/17 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/05/17 18:13 7440-36-001/04/17 20:006.0 3.8 1
Arsenic ND ug/L 01/06/17 17:44 7440-38-201/04/17 20:0010.0 2.5 1
Barium 19.1J ug/L 01/05/17 18:13 7440-39-301/04/17 20:001002.5 1
Beryllium ND ug/L 01/05/17 18:13 7440-41-701/04/17 20:001.0 0.50 1
Cadmium 0.78J ug/L 01/05/17 18:13 7440-43-901/04/17 20:001.0 0.50 1
Chromium ND ug/L 01/05/17 18:13 7440-47-301/04/17 20:0010.0 2.5 1
Cobalt 8.0J ug/L 01/05/17 18:13 7440-48-401/04/17 20:0010.0 2.5 1
Copper ND ug/L 01/05/17 18:13 7440-50-801/04/17 20:0010.0 2.5 1
Lead ND ug/L 01/05/17 18:13 7439-92-101/04/17 20:0010.0 2.5 1
Nickel ND ug/L 01/05/17 18:13 7440-02-001/04/17 20:0050.0 2.5 1
Selenium ND ug/L 01/05/17 18:13 7782-49-201/04/17 20:0010.0 5.0 1
Silver ND ug/L 01/05/17 18:13 7440-22-401/04/17 20:0010.0 2.5 1
Thallium ND ug/L 01/05/17 18:13 7440-28-001/04/17 20:005.5 5.0 1
Vanadium ND ug/L 01/05/17 18:13 7440-62-201/04/17 20:0025.0 2.5 1
Zinc 7.0J ug/L 01/05/17 18:13 7440-66-601/04/17 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/04/17 14:41 67-64-110010.0 1
Acrylonitrile ND ug/L 01/04/17 14:41 107-13-12001.9 1
Benzene ND ug/L 01/04/17 14:41 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/04/17 14:41 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/04/17 14:41 75-27-41.0 0.18 1
Bromoform ND ug/L 01/04/17 14:41 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/04/17 14:41 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/04/17 14:41 78-93-31000.96 1
Carbon disulfide ND ug/L 01/04/17 14:41 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/04/17 14:41 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/04/17 14:41 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/04/17 14:41 75-00-310.0 0.54 1
Chloroform ND ug/L 01/04/17 14:41 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/04/17 14:41 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/04/17 14:41 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/04/17 14:41 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/04/17 14:41 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/04/17 14:41 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/04/17 14:41 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/04/17 14:41 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/04/17 14:41 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/04/17 14:41 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/04/17 14:41 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/04/17 14:41 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/04/17 14:41 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/04/17 14:41 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/04/17 14:41 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/04/17 14:41 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/04/17 14:41 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:SW-6 Lab ID:92325007029 Collected:12/30/16 09:40 Received:01/03/17 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/04/17 14:41 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/04/17 14:41 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/04/17 14:41 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/04/17 14:41 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/04/17 14:41 108-10-11000.33 1
Styrene ND ug/L 01/04/17 14:41 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/04/17 14:41 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/04/17 14:41 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/04/17 14:41 127-18-41.0 0.46 1
Toluene ND ug/L 01/04/17 14:41 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/04/17 14:41 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/04/17 14:41 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/04/17 14:41 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/04/17 14:41 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/04/17 14:41 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/04/17 14:41 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/04/17 14:41 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/04/17 14:41 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %01/04/17 14:41 460-00-470-130 1
1,2-Dichloroethane-d4 (S)112 %01/04/17 14:41 17060-07-070-130 1
Toluene-d8 (S)105 %01/04/17 14:41 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:EB Lab ID:92325007030 Collected:12/31/16 12:00 Received:01/03/17 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/05/17 18:17 7440-36-001/04/17 20:006.0 3.8 1
Arsenic ND ug/L 01/10/17 15:41 7440-38-201/04/17 20:0010.0 2.5 1
Barium ND ug/L 01/05/17 18:17 7440-39-301/04/17 20:001002.5 1
Beryllium ND ug/L 01/05/17 18:17 7440-41-701/04/17 20:001.0 0.50 1
Cadmium ND ug/L 01/05/17 18:17 7440-43-901/04/17 20:001.0 0.50 1
Chromium ND ug/L 01/05/17 18:17 7440-47-301/04/17 20:0010.0 2.5 1
Cobalt ND ug/L 01/05/17 18:17 7440-48-401/04/17 20:0010.0 2.5 1
Copper ND ug/L 01/05/17 18:17 7440-50-801/04/17 20:0010.0 2.5 1
Lead ND ug/L 01/05/17 18:17 7439-92-101/04/17 20:0010.0 2.5 1
Nickel ND ug/L 01/05/17 18:17 7440-02-001/04/17 20:0050.0 2.5 1
Selenium ND ug/L 01/05/17 18:17 7782-49-201/04/17 20:0010.0 5.0 1
Silver ND ug/L 01/05/17 18:17 7440-22-401/04/17 20:0010.0 2.5 1
Thallium ND ug/L 01/05/17 18:17 7440-28-001/04/17 20:005.5 5.0 1
Tin ND ug/L 01/05/17 18:17 7440-31-501/04/17 20:001002.5 1
Vanadium ND ug/L 01/05/17 18:17 7440-62-201/04/17 20:0025.0 2.5 1
Zinc ND ug/L 01/05/17 18:17 7440-66-601/04/17 20:0010.0 5.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury ND ug/L 01/04/17 15:38 7439-97-601/04/17 04:000.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/04/17 16:43 67-64-110010.0 1
Acrylonitrile ND ug/L 01/04/17 16:43 107-13-12001.9 1
Benzene ND ug/L 01/04/17 16:43 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/04/17 16:43 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/04/17 16:43 75-27-41.0 0.18 1
Bromoform ND ug/L 01/04/17 16:43 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/04/17 16:43 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/04/17 16:43 78-93-31000.96 1
Carbon disulfide ND ug/L 01/04/17 16:43 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/04/17 16:43 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/04/17 16:43 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/04/17 16:43 75-00-310.0 0.54 1
Chloroform ND ug/L 01/04/17 16:43 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/04/17 16:43 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/04/17 16:43 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/04/17 16:43 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/04/17 16:43 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/04/17 16:43 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/04/17 16:43 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/04/17 16:43 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/04/17 16:43 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/04/17 16:43 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/04/17 16:43 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/04/17 16:43 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/04/17 16:43 156-59-25.0 0.19 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
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Huntersville, NC 28078
[phone]
Page 68 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:EB Lab ID:92325007030 Collected:12/31/16 12:00 Received:01/03/17 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,2-Dichloroethene ND ug/L 01/04/17 16:43 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/04/17 16:43 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/04/17 16:43 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/04/17 16:43 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/04/17 16:43 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/04/17 16:43 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/04/17 16:43 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/04/17 16:43 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/04/17 16:43 108-10-11000.33 1
Styrene ND ug/L 01/04/17 16:43 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/04/17 16:43 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/04/17 16:43 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/04/17 16:43 127-18-41.0 0.46 1
Toluene ND ug/L 01/04/17 16:43 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/04/17 16:43 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/04/17 16:43 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/04/17 16:43 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/04/17 16:43 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/04/17 16:43 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/04/17 16:43 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/04/17 16:43 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/04/17 16:43 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %01/04/17 16:43 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %01/04/17 16:43 17060-07-070-130 1
Toluene-d8 (S)111 %01/04/17 16:43 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:TB Lab ID:92325007031 Collected:12/31/16 00:00 Received:01/03/17 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/04/17 17:00 67-64-110010.0 1
Acrylonitrile ND ug/L 01/04/17 17:00 107-13-12001.9 1
Benzene ND ug/L 01/04/17 17:00 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/04/17 17:00 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/04/17 17:00 75-27-41.0 0.18 1
Bromoform ND ug/L 01/04/17 17:00 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/04/17 17:00 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/04/17 17:00 78-93-31000.96 1
Carbon disulfide ND ug/L 01/04/17 17:00 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/04/17 17:00 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/04/17 17:00 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/04/17 17:00 75-00-310.0 0.54 1
Chloroform ND ug/L 01/04/17 17:00 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/04/17 17:00 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/04/17 17:00 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/04/17 17:00 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/04/17 17:00 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/04/17 17:00 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/04/17 17:00 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/04/17 17:00 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/04/17 17:00 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/04/17 17:00 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/04/17 17:00 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/04/17 17:00 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/04/17 17:00 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/04/17 17:00 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/04/17 17:00 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/04/17 17:00 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/04/17 17:00 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/04/17 17:00 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/04/17 17:00 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/04/17 17:00 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/04/17 17:00 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/04/17 17:00 108-10-11000.33 1
Styrene ND ug/L 01/04/17 17:00 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/04/17 17:00 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/04/17 17:00 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/04/17 17:00 127-18-41.0 0.46 1
Toluene ND ug/L 01/04/17 17:00 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/04/17 17:00 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/04/17 17:00 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/04/17 17:00 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/04/17 17:00 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/04/17 17:00 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/04/17 17:00 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/04/17 17:00 75-01-41.0 0.62 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Sample:TB Lab ID:92325007031 Collected:12/31/16 00:00 Received:01/03/17 11:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Xylene (Total)ND ug/L 01/04/17 17:00 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %01/04/17 17:00 460-00-470-130 1
1,2-Dichloroethane-d4 (S)111 %01/04/17 17:00 17060-07-070-130 1
Toluene-d8 (S)107 %01/04/17 17:00 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343300
RSK 175 Modified
RSK 175 Modified
RSK 175 HEADSPACE
Associated Lab Samples:92325007001, 92325007002, 92325007003, 92325007004, 92325007012, 92325007013, 92325007015,
92325007017, 92325007020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1904059
Associated Lab Samples:92325007001, 92325007002, 92325007003, 92325007004, 92325007012, 92325007013, 92325007015,
92325007017, 92325007020
Matrix:Water
AnalyzedMDL
Methane ug/L ND 10.0 N201/06/17 10:5910.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1904060LABORATORY CONTROL SAMPLE:
LCSSpike
Methane ug/L 430 N239610970-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1906664MATRIX SPIKE SAMPLE:
MSSpike
Result
92324946022
Methane ug/L 458 N239611670-130ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92324946024
1906665SAMPLE DUPLICATE:
Methane ug/L 49.0 N222049.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343250
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92325007001, 92325007002, 92325007007, 92325007008, 92325007011, 92325007015, 92325007030
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1903882
Associated Lab Samples:92325007001, 92325007002, 92325007007, 92325007008, 92325007011, 92325007015, 92325007030
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 01/04/17 15:070.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1903883LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.52.5 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1903884MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92325007001
1903885
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L M12.5 40 75-12533 18 252.5ND 1.0 0.83
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 73 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343179
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92325007005, 92325007006, 92325007007, 92325007010, 92325007012, 92325007013, 92325007015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1903459
Associated Lab Samples:92325007005, 92325007006, 92325007007, 92325007010, 92325007012, 92325007013, 92325007015
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 01/05/17 00:403.8
Arsenic ug/L ND 10.0 01/05/17 00:402.5
Barium ug/L ND 100 01/05/17 00:402.5
Beryllium ug/L ND 1.0 01/05/17 00:400.50
Cadmium ug/L ND 1.0 01/05/17 00:400.50
Chromium ug/L ND 10.0 01/05/17 00:402.5
Cobalt ug/L ND 10.0 01/05/17 00:402.5
Copper ug/L ND 10.0 01/05/17 00:402.5
Lead ug/L ND 10.0 01/05/17 00:402.5
Nickel ug/L ND 50.0 01/05/17 00:402.5
Selenium ug/L ND 10.0 01/05/17 00:405.0
Silver ug/L ND 10.0 01/05/17 00:402.5
Thallium ug/L ND 5.5 01/05/17 00:405.0
Vanadium ug/L ND 25.0 01/05/17 00:402.5
Zinc ug/L ND 10.0 01/05/17 00:405.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1903460LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 468500 94 80-120
Arsenic ug/L 463500 93 80-120
Barium ug/L 504500 101 80-120
Beryllium ug/L 484500 97 80-120
Cadmium ug/L 472500 94 80-120
Chromium ug/L 494500 99 80-120
Cobalt ug/L 475500 95 80-120
Copper ug/L 488500 98 80-120
Lead ug/L 469500 94 80-120
Nickel ug/L 470500 94 80-120
Selenium ug/L 478500 96 80-120
Silver ug/L 242250 97 80-120
Thallium ug/L 497500 99 80-120
Vanadium ug/L 472500 94 80-120
Zinc ug/L 483500 97 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 74 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1903461MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92324987001
1903462
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 94 75-12593 1 25500ND473469
Arsenic ug/L 500 94 75-12593 1 25500ND470464
Barium ug/L 500 102 75-12596 4 25500172683654
Beryllium ug/L 500 99 75-12594 5 25500ND494471
Cadmium ug/L 500 95 75-12593 2 25500ND474463
Chromium ug/L 500 99 75-12595 4 25500ND494476
Cobalt ug/L 500 93 75-12591 2 25500ND463453
Copper ug/L 500 98 75-12595 3 25500ND490474
Lead ug/L 500 91 75-12590 2 25500ND456449
Nickel ug/L 500 91 75-12589 2 25500ND456446
Selenium ug/L 500 95 75-12594 1 25500ND477472
Silver ug/L 250 96 75-12593 3 25250ND242234
Thallium ug/L 500 95 75-12595 0 25500ND479477
Vanadium ug/L 500 96 75-12593 3 25500ND481466
Zinc ug/L 500 94 75-12592 2 25500ND471462
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 75 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343387
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92325007001, 92325007002, 92325007003, 92325007004, 92325007008, 92325007009, 92325007011,
92325007016, 92325007017, 92325007018, 92325007019, 92325007020, 92325007021, 92325007022,
92325007023, 92325007024, 92325007025
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1904720
Associated Lab Samples:92325007001, 92325007002, 92325007003, 92325007004, 92325007008, 92325007009, 92325007011,
92325007016, 92325007017, 92325007018, 92325007019, 92325007020, 92325007021, 92325007022,
92325007023, 92325007024, 92325007025
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 01/05/17 15:593.8
Arsenic ug/L ND 10.0 01/05/17 15:592.5
Barium ug/L ND 100 01/05/17 15:592.5
Beryllium ug/L ND 1.0 01/05/17 15:590.50
Cadmium ug/L ND 1.0 01/05/17 15:590.50
Chromium ug/L ND 10.0 01/05/17 15:592.5
Cobalt ug/L ND 10.0 01/05/17 15:592.5
Copper ug/L ND 10.0 01/05/17 15:592.5
Lead ug/L ND 10.0 01/05/17 15:592.5
Nickel ug/L ND 50.0 01/05/17 15:592.5
Selenium ug/L ND 10.0 01/05/17 15:595.0
Silver ug/L ND 10.0 01/05/17 15:592.5
Thallium ug/L ND 5.5 01/05/17 15:595.0
Vanadium ug/L ND 25.0 01/05/17 15:592.5
Zinc ug/L ND 10.0 01/05/17 15:595.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1904721LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 440500 88 80-120
Arsenic ug/L 422500 84 80-120
Barium ug/L 496500 99 80-120
Beryllium ug/L 495500 99 80-120
Cadmium ug/L 458500 92 80-120
Chromium ug/L 476500 95 80-120
Cobalt ug/L 449500 90 80-120
Copper ug/L 472500 94 80-120
Lead ug/L 445500 89 80-120
Nickel ug/L 450500 90 80-120
Selenium ug/L 446500 89 80-120
Silver ug/L 237250 95 80-120
Thallium ug/L 482500 96 80-120
Vanadium ug/L 456500 91 80-120
Zinc ug/L 445500 89 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 76 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1904722MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92325007001
1904723
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 90 75-12589 2 25500ND451444
Arsenic ug/L 500 85 75-12585 1 25500ND430426
Barium ug/L 500 100 75-12598 2 2550038.9J 539 528
Beryllium ug/L 500 102 75-12599 3 25500ND509496
Cadmium ug/L 500 93 75-12591 2 255001.3 466 458
Chromium ug/L 500 95 75-12594 0 25500ND474472
Cobalt ug/L 500 90 75-12588 2 255007.3J 456 449
Copper ug/L 500 96 75-12594 2 25500ND478470
Lead ug/L 500 88 75-12587 1 25500ND444438
Nickel ug/L 500 89 75-12588 1 255004.3J 451 444
Selenium ug/L 500 90 75-12588 2 25500ND450442
Silver ug/L 250 97 75-12595 2 25250ND241236
Thallium ug/L 500 95 75-12595 0 255005.7 479 479
Vanadium ug/L 500 94 75-12592 2 25500ND471462
Zinc ug/L 500 89 75-12588 1 2550031.3 477 470
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 77 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343388
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92325007026, 92325007027, 92325007028, 92325007029, 92325007030
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1904725
Associated Lab Samples:92325007026, 92325007027, 92325007028, 92325007029, 92325007030
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 01/06/17 17:233.8
Arsenic ug/L ND 10.0 01/10/17 15:382.5
Barium ug/L ND 100 01/05/17 17:402.5
Beryllium ug/L ND 1.0 01/05/17 17:400.50
Cadmium ug/L ND 1.0 01/05/17 17:400.50
Chromium ug/L ND 10.0 01/05/17 17:402.5
Cobalt ug/L ND 10.0 01/06/17 17:232.5
Copper ug/L ND 10.0 01/06/17 17:232.5
Lead ug/L ND 10.0 01/06/17 17:232.5
Nickel ug/L ND 50.0 01/05/17 17:402.5
Selenium ug/L ND 10.0 01/06/17 17:235.0
Silver ug/L ND 10.0 01/05/17 17:402.5
Thallium ug/L ND 5.5 01/05/17 17:405.0
Tin ug/L ND 100 01/05/17 17:402.5
Vanadium ug/L ND 25.0 01/05/17 17:402.5
Zinc ug/L ND 10.0 01/06/17 17:235.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1904726LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 485500 97 80-120
Arsenic ug/L 479500 96 80-120
Barium ug/L 495500 99 80-120
Beryllium ug/L 495500 99 80-120
Cadmium ug/L 457500 91 80-120
Chromium ug/L 474500 95 80-120
Cobalt ug/L 491500 98 80-120
Copper ug/L 496500 99 80-120
Lead ug/L 481500 96 80-120
Nickel ug/L 446500 89 80-120
Selenium ug/L 490500 98 80-120
Silver ug/L 236250 95 80-120
Thallium ug/L 463500 93 80-120
Tin ug/L 448500 90 80-120
Vanadium ug/L 456500 91 80-120
Zinc ug/L 493500 99 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
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Huntersville, NC 28078
[phone]
Page 78 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1904727MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92325007026
1904728
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 86 75-12586 1 25500ND430432
Arsenic ug/L 500 94 75-12597 3 255002.6J 472 486
Barium ug/L 500 95 75-12597 2 2550065.5J 541 553
Beryllium ug/L 500 96 75-12598 1 25500ND482489
Cadmium ug/L 500 89 75-12590 2 25500ND445452
Chromium ug/L 500 91 75-12594 4 255004.0J 457 475
Cobalt ug/L 500 87 75-12588 1 255006.1J 439 445
Copper ug/L 500 91 75-12594 3 25500ND456471
Lead ug/L 500 85 75-12587 2 25500ND427433
Nickel ug/L 500 86 75-12588 2 255004.9J 436 443
Selenium ug/L 500 86 75-12588 2 25500ND433441
Silver ug/L 250 92 75-12594 2 25250ND230235
Thallium ug/L 500 88 75-12590 2 255005.6 446 454
Tin ug/L 500 88 75-12589 1 25500ND440446
Vanadium ug/L 500 90 75-12591 2 255003.5J 452 460
Zinc ug/L 500 88 75-12589 1 255007.2J 447 450
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
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9800 Kincey Ave. Suite 100
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[phone]
Page 79 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343644
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92325007014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1906014
Associated Lab Samples:92325007014
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 01/11/17 11:433.8
Arsenic ug/L ND 10.0 01/11/17 11:432.5
Barium ug/L ND 100 01/11/17 11:432.5
Beryllium ug/L ND 1.0 01/11/17 11:430.50
Cadmium ug/L ND 1.0 01/11/17 11:430.50
Chromium ug/L ND 10.0 01/11/17 11:432.5
Cobalt ug/L ND 10.0 01/11/17 11:432.5
Copper ug/L ND 10.0 01/11/17 11:432.5
Lead ug/L ND 10.0 01/11/17 11:432.5
Nickel ug/L ND 50.0 01/11/17 11:432.5
Selenium ug/L ND 10.0 01/11/17 11:435.0
Silver ug/L ND 10.0 01/11/17 11:432.5
Thallium ug/L ND 5.5 01/11/17 11:435.0
Vanadium ug/L ND 25.0 01/11/17 11:432.5
Zinc ug/L ND 10.0 01/11/17 11:435.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1906015LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 475500 95 80-120
Arsenic ug/L 492500 98 80-120
Barium ug/L 501500 100 80-120
Beryllium ug/L 506500 101 80-120
Cadmium ug/L 515500 103 80-120
Chromium ug/L 500500 100 80-120
Cobalt ug/L 512500 102 80-120
Copper ug/L 520500 104 80-120
Lead ug/L 503500 101 80-120
Nickel ug/L 503500 101 80-120
Selenium ug/L 506500 101 80-120
Silver ug/L 239250 96 80-120
Thallium ug/L 540500 108 80-120
Vanadium ug/L 488500 98 80-120
Zinc ug/L 507500 101 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 80 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1906016MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92325007014
1906017
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 93 75-12593 0 25500ND466467
Arsenic ug/L 500 98 75-12598 0 255003.0J 493 491
Barium ug/L 500 99 75-12599 0 255004.9J 502 502
Beryllium ug/L 500 102 75-125102 0 25500ND510512
Cadmium ug/L 500 101 75-125101 0 25500ND505503
Chromium ug/L 500 98 75-12598 0 25500ND491491
Cobalt ug/L 500 97 75-12597 1 25500ND486484
Copper ug/L 500 104 75-125104 0 25500ND521522
Lead ug/L 500 95 75-12595 0 255003.2J 478 476
Nickel ug/L 500 96 75-12595 1 25500ND478476
Selenium ug/L 500 99 75-12599 0 25500ND495494
Silver ug/L 250 95 75-12595 0 25250ND237237
Thallium ug/L 500 97 75-12597 0 25500ND487487
Vanadium ug/L 500 98 75-12599 1 25500ND489493
Zinc ug/L 500 96 75-12595 0 255005.7J 485 483
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 81 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343403
EPA 3010
EPA 6010
6010 MET Filtered Diss.
Associated Lab Samples:92325007003, 92325007004, 92325007012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1904826
Associated Lab Samples:92325007003, 92325007004, 92325007012
Matrix:Water
AnalyzedMDL
Iron, Dissolved ug/L ND 50.0 01/05/17 15:0325.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1904827LABORATORY CONTROL SAMPLE:
LCSSpike
Iron, Dissolved ug/L 43405000 87 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1904828MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92325007003
1904829
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Iron, Dissolved ug/L 5000 75 75-12576 0 205000384004220042200
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 82 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343140
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92325007001, 92325007002, 92325007003, 92325007004, 92325007005, 92325007006, 92325007007,
92325007008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1903274
Associated Lab Samples:92325007001, 92325007002, 92325007003, 92325007004, 92325007005, 92325007006, 92325007007,
92325007008
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 01/03/17 12:330.33
1,1,1-Trichloroethane ug/L ND 1.0 01/03/17 12:330.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 01/03/17 12:330.40
1,1,2-Trichloroethane ug/L ND 1.0 01/03/17 12:330.29
1,1-Dichloroethane ug/L ND 5.0 01/03/17 12:330.32
1,1-Dichloroethene ug/L ND 5.0 01/03/17 12:330.56
1,2,3-Trichloropropane ug/L ND 1.0 01/03/17 12:330.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 01/03/17 12:332.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 01/03/17 12:330.27
1,2-Dichlorobenzene ug/L ND 5.0 01/03/17 12:330.30
1,2-Dichloroethane ug/L ND 1.0 01/03/17 12:330.24
1,2-Dichloropropane ug/L ND 1.0 01/03/17 12:330.27
1,4-Dichlorobenzene ug/L ND 1.0 01/03/17 12:330.33
2-Butanone (MEK)ug/L ND 100 01/03/17 12:330.96
2-Hexanone ug/L ND 50.0 01/03/17 12:330.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 01/03/17 12:330.33
Acetone ug/L ND 100 01/03/17 12:3310.0
Acrylonitrile ug/L ND 200 01/03/17 12:331.9
Benzene ug/L ND 1.0 01/03/17 12:330.25
Bromochloromethane ug/L ND 3.0 01/03/17 12:330.17
Bromodichloromethane ug/L ND 1.0 01/03/17 12:330.18
Bromoform ug/L ND 3.0 01/03/17 12:330.26
Bromomethane ug/L ND 10.0 01/03/17 12:330.29
Carbon disulfide ug/L ND 100 01/03/17 12:331.2
Carbon tetrachloride ug/L ND 1.0 01/03/17 12:330.25
Chlorobenzene ug/L ND 3.0 01/03/17 12:330.23
Chloroethane ug/L ND 10.0 01/03/17 12:330.54
Chloroform ug/L ND 5.0 01/03/17 12:330.14
Chloromethane ug/L ND 1.0 01/03/17 12:330.11
cis-1,2-Dichloroethene ug/L ND 5.0 01/03/17 12:330.19
cis-1,3-Dichloropropene ug/L ND 1.0 01/03/17 12:330.13
Dibromochloromethane ug/L ND 3.0 01/03/17 12:330.21
Dibromomethane ug/L ND 10.0 01/03/17 12:330.21
Ethylbenzene ug/L ND 1.0 01/03/17 12:330.30
Iodomethane ug/L ND 10.0 01/03/17 12:330.32
Methylene Chloride ug/L ND 1.0 01/03/17 12:330.97
Styrene ug/L ND 1.0 01/03/17 12:330.26
Tetrachloroethene ug/L ND 1.0 01/03/17 12:330.46
Toluene ug/L ND 1.0 01/03/17 12:330.26
trans-1,2-Dichloroethene ug/L ND 5.0 01/03/17 12:330.49
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 83 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1903274
Associated Lab Samples:92325007001, 92325007002, 92325007003, 92325007004, 92325007005, 92325007006, 92325007007,
92325007008
Matrix:Water
AnalyzedMDL
trans-1,3-Dichloropropene ug/L ND 1.0 01/03/17 12:330.26
trans-1,4-Dichloro-2-butene ug/L ND 100 01/03/17 12:331.0
Trichloroethene ug/L ND 1.0 01/03/17 12:330.47
Trichlorofluoromethane ug/L ND 1.0 01/03/17 12:330.20
Vinyl acetate ug/L ND 50.0 01/03/17 12:330.35
Vinyl chloride ug/L ND 1.0 01/03/17 12:330.62
Xylene (Total)ug/L ND 5.0 01/03/17 12:330.66
1,2-Dichloroethane-d4 (S)%102 70-130 01/03/17 12:33
4-Bromofluorobenzene (S)%102 70-130 01/03/17 12:33
Toluene-d8 (S)%108 70-130 01/03/17 12:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1903275LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 53.250 106 80-125
1,1,1-Trichloroethane ug/L 60.150 120 71-129
1,1,2,2-Tetrachloroethane ug/L 49.850 100 79-124
1,1,2-Trichloroethane ug/L 56.750 113 85-125
1,1-Dichloroethane ug/L 55.350 111 73-126
1,1-Dichloroethene ug/L 58.750 117 66-135
1,2,3-Trichloropropane ug/L 49.250 98 75-130
1,2-Dibromo-3-chloropropane ug/L 50.750 101 71-133
1,2-Dibromoethane (EDB)ug/L 51.750 103 83-124
1,2-Dichlorobenzene ug/L 46.850 94 80-133
1,2-Dichloroethane ug/L 55.850 112 67-128
1,2-Dichloropropane ug/L 54.750 109 75-132
1,4-Dichlorobenzene ug/L 46.050 92 78-130
2-Butanone (MEK)ug/L 121100 121 61-144
2-Hexanone ug/L 104100 104 68-143
4-Methyl-2-pentanone (MIBK)ug/L 111100 111 72-135
Acetone ug/L 122100 122 48-146
Acrylonitrile ug/L 292250 117 40-160
Benzene ug/L 56.350 113 80-125
Bromochloromethane ug/L 55.750 111 71-125
Bromodichloromethane ug/L 58.050 116 78-124
Bromoform ug/L 46.850 94 71-128
Bromomethane ug/L 51.150 102 40-160
Carbon disulfide ug/L 56.3J50 113 50-160
Carbon tetrachloride ug/L 56.950 114 69-131
Chlorobenzene ug/L 48.650 97 81-122
Chloroethane ug/L 57.650 115 39-148
Chloroform ug/L 56.750 113 73-127
Chloromethane ug/L 60.450 121 44-146
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 84 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1903275LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 55.350 111 74-124
cis-1,3-Dichloropropene ug/L 60.650 121 72-132
Dibromochloromethane ug/L 48.850 98 78-125
Dibromomethane ug/L 51.950 104 82-120
Ethylbenzene ug/L 48.750 97 79-121
Iodomethane ug/L 109100 109 39-154
Methylene Chloride ug/L 55.350 111 64-133
Styrene ug/L 48.750 97 84-126
Tetrachloroethene ug/L 46.450 93 78-122
Toluene ug/L 53.450 107 80-121
trans-1,2-Dichloroethene ug/L 58.650 117 71-127
trans-1,3-Dichloropropene ug/L 62.250 124 69-141
trans-1,4-Dichloro-2-butene ug/L 55.7J50 111 40-160
Trichloroethene ug/L 52.850 106 78-122
Trichlorofluoromethane ug/L 61.750 123 53-137
Vinyl acetate ug/L 114100 114 40-160
Vinyl chloride ug/L 47.250 94 58-137
Xylene (Total)ug/L 146150 97 81-126
1,2-Dichloroethane-d4 (S)%106 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1903276MATRIX SPIKE SAMPLE:
MSSpike
Result
92324987006
1,1,1,2-Tetrachloroethane ug/L 21.920 109 70-130ND
1,1,1-Trichloroethane ug/L 22.620 113 70-130ND
1,1,2,2-Tetrachloroethane ug/L 22.020 110 70-130ND
1,1,2-Trichloroethane ug/L 22.320 112 70-130ND
1,1-Dichloroethane ug/L 25.020 109 70-1303.1J
1,1-Dichloroethene ug/L 24.220 121 70-166ND
1,2,3-Trichloropropane ug/L 22.320 111 70-130ND
1,2-Dibromo-3-chloropropane ug/L 23.320 116 70-130ND
1,2-Dibromoethane (EDB)ug/L 22.820 114 70-130ND
1,2-Dichlorobenzene ug/L 22.320 111 70-130ND
1,2-Dichloroethane ug/L 22.020 108 70-1300.34J
1,2-Dichloropropane ug/L 24.120 112 70-1301.7
1,4-Dichlorobenzene ug/L 27.220 110 70-1305.3
2-Butanone (MEK)ug/L 46.2J40 116 70-130ND
2-Hexanone ug/L 46.7J40 117 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 43.0J40 108 70-130ND
Acetone ug/L 46.9J40 117 70-130ND
Acrylonitrile ug/L 113J100 113 70-130ND
Benzene ug/L 23.620 115 70-1480.68J
Bromochloromethane ug/L 21.120 106 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 85 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1903276MATRIX SPIKE SAMPLE:
MSSpike
Result
92324987006
Bromodichloromethane ug/L 23.220 116 70-130ND
Bromoform ug/L 19.720 98 70-130ND
Bromomethane ug/L 21.420 107 70-130ND
Carbon disulfide ug/L 22.1J20 110 70-130ND
Carbon tetrachloride ug/L 23.020 115 70-130ND
Chlorobenzene ug/L 28.020 117 70-1464.6
Chloroethane ug/L 23.820 117 70-130ND
Chloroform ug/L 22.120 110 70-130ND
Chloromethane ug/L 25.020 124 70-1300.17J
cis-1,2-Dichloroethene ug/L 50.920 103 70-13030.3
cis-1,3-Dichloropropene ug/L 22.220 111 70-130ND
Dibromochloromethane ug/L 20.220 101 70-130ND
Dibromomethane ug/L 19.720 99 70-130ND
Ethylbenzene ug/L 23.220 116 70-130ND
Iodomethane ug/L 40.840 102 70-130ND
Methylene Chloride ug/L 19.720 99 70-130ND
Styrene ug/L 22.820 114 70-130ND
Tetrachloroethene ug/L 21.020 105 70-130ND
Toluene ug/L 22.220 111 70-155ND
trans-1,2-Dichloroethene ug/L 23.420 115 70-130ND
trans-1,3-Dichloropropene ug/L 22.020 110 70-130ND
trans-1,4-Dichloro-2-butene ug/L 19.8J20 99 70-130ND
Trichloroethene ug/L 22.220 108 69-1510.66J
Trichlorofluoromethane ug/L 25.220 126 70-130ND
Vinyl acetate ug/L 33.9J40 85 70-130ND
Vinyl chloride ug/L 21.320 95 70-1302.2
1,2-Dichloroethane-d4 (S)%107 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92324987007
1903277SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 3.8J 4 304.0J
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L 0.32J 300.29J
1,2-Dichloropropane ug/L 1.0 300.99J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 86 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92324987007
1903277SAMPLE DUPLICATE:
1,4-Dichlorobenzene ug/L 5.4 2 305.3
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L 0.81J 300.84J
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L 3.6 0 303.6
Chloroethane ug/L 0.91J 301.1J
Chloroform ug/L ND 30ND
Chloromethane ug/L 0.30J 300.27J
cis-1,2-Dichloroethene ug/L 34.3 3 3035.3
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L 0.84J 300.87J
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L 2.0 2 301.9
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L 1.2 6 301.2
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%103 0103
4-Bromofluorobenzene (S)%100 1101
Toluene-d8 (S)%107 2104
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 87 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343141
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92325007009, 92325007010, 92325007011, 92325007012, 92325007013, 92325007014, 92325007015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1903278
Associated Lab Samples:92325007009, 92325007010, 92325007011, 92325007012, 92325007013, 92325007014, 92325007015
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 01/03/17 12:510.33
1,1,1-Trichloroethane ug/L ND 1.0 01/03/17 12:510.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 01/03/17 12:510.40
1,1,2-Trichloroethane ug/L ND 1.0 01/03/17 12:510.29
1,1-Dichloroethane ug/L ND 5.0 01/03/17 12:510.32
1,1-Dichloroethene ug/L ND 5.0 01/03/17 12:510.56
1,2,3-Trichloropropane ug/L ND 1.0 01/03/17 12:510.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 01/03/17 12:512.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 01/03/17 12:510.27
1,2-Dichlorobenzene ug/L ND 5.0 01/03/17 12:510.30
1,2-Dichloroethane ug/L ND 1.0 01/03/17 12:510.24
1,2-Dichloropropane ug/L ND 1.0 01/03/17 12:510.27
1,4-Dichlorobenzene ug/L ND 1.0 01/03/17 12:510.33
2-Butanone (MEK)ug/L ND 100 01/03/17 12:510.96
2-Hexanone ug/L ND 50.0 01/03/17 12:510.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 01/03/17 12:510.33
Acetone ug/L ND 100 01/03/17 12:5110.0
Acrylonitrile ug/L ND 200 01/03/17 12:511.9
Benzene ug/L ND 1.0 01/03/17 12:510.25
Bromochloromethane ug/L ND 3.0 01/03/17 12:510.17
Bromodichloromethane ug/L ND 1.0 01/03/17 12:510.18
Bromoform ug/L ND 3.0 01/03/17 12:510.26
Bromomethane ug/L ND 10.0 01/03/17 12:510.29
Carbon disulfide ug/L ND 100 01/03/17 12:511.2
Carbon tetrachloride ug/L ND 1.0 01/03/17 12:510.25
Chlorobenzene ug/L ND 3.0 01/03/17 12:510.23
Chloroethane ug/L ND 10.0 01/03/17 12:510.54
Chloroform ug/L ND 5.0 01/03/17 12:510.14
Chloromethane ug/L ND 1.0 01/03/17 12:510.11
cis-1,2-Dichloroethene ug/L ND 5.0 01/03/17 12:510.19
cis-1,3-Dichloropropene ug/L ND 1.0 01/03/17 12:510.13
Dibromochloromethane ug/L ND 3.0 01/03/17 12:510.21
Dibromomethane ug/L ND 10.0 01/03/17 12:510.21
Ethylbenzene ug/L ND 1.0 01/03/17 12:510.30
Iodomethane ug/L ND 10.0 01/03/17 12:510.32
Methylene Chloride ug/L ND 1.0 01/03/17 12:510.97
Styrene ug/L ND 1.0 01/03/17 12:510.26
Tetrachloroethene ug/L ND 1.0 01/03/17 12:510.46
Toluene ug/L ND 1.0 01/03/17 12:510.26
trans-1,2-Dichloroethene ug/L ND 5.0 01/03/17 12:510.49
trans-1,3-Dichloropropene ug/L ND 1.0 01/03/17 12:510.26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 88 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1903278
Associated Lab Samples:92325007009, 92325007010, 92325007011, 92325007012, 92325007013, 92325007014, 92325007015
Matrix:Water
AnalyzedMDL
trans-1,4-Dichloro-2-butene ug/L ND 100 01/03/17 12:511.0
Trichloroethene ug/L ND 1.0 01/03/17 12:510.47
Trichlorofluoromethane ug/L ND 1.0 01/03/17 12:510.20
Vinyl acetate ug/L ND 50.0 01/03/17 12:510.35
Vinyl chloride ug/L ND 1.0 01/03/17 12:510.62
Xylene (Total)ug/L ND 5.0 01/03/17 12:510.66
1,2-Dichloroethane-d4 (S)%104 70-130 01/03/17 12:51
4-Bromofluorobenzene (S)%104 70-130 01/03/17 12:51
Toluene-d8 (S)%106 70-130 01/03/17 12:51
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1903279LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 53.250 106 80-125
1,1,1-Trichloroethane ug/L 56.350 113 71-129
1,1,2,2-Tetrachloroethane ug/L 49.350 99 79-124
1,1,2-Trichloroethane ug/L 56.050 112 85-125
1,1-Dichloroethane ug/L 52.050 104 73-126
1,1-Dichloroethene ug/L 55.050 110 66-135
1,2,3-Trichloropropane ug/L 49.650 99 75-130
1,2-Dibromo-3-chloropropane ug/L 50.950 102 71-133
1,2-Dibromoethane (EDB)ug/L 50.550 101 83-124
1,2-Dichlorobenzene ug/L 46.750 93 80-133
1,2-Dichloroethane ug/L 53.050 106 67-128
1,2-Dichloropropane ug/L 53.950 108 75-132
1,4-Dichlorobenzene ug/L 45.650 91 78-130
2-Butanone (MEK)ug/L 113100 113 61-144
2-Hexanone ug/L 103100 103 68-143
4-Methyl-2-pentanone (MIBK)ug/L 108100 108 72-135
Acetone ug/L 109100 109 48-146
Acrylonitrile ug/L 268250 107 40-160
Benzene ug/L 55.850 112 80-125
Bromochloromethane ug/L 52.250 104 71-125
Bromodichloromethane ug/L 57.950 116 78-124
Bromoform ug/L 46.350 93 71-128
Bromomethane ug/L 49.050 98 40-160
Carbon disulfide ug/L 53.2J50 106 50-160
Carbon tetrachloride ug/L 56.450 113 69-131
Chlorobenzene ug/L 48.550 97 81-122
Chloroethane ug/L 54.350 109 39-148
Chloroform ug/L 52.150 104 73-127
Chloromethane ug/L 56.750 113 44-146
cis-1,2-Dichloroethene ug/L 51.350 103 74-124
cis-1,3-Dichloropropene ug/L 59.950 120 72-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 89 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1903279LABORATORY CONTROL SAMPLE:
LCSSpike
Dibromochloromethane ug/L 47.750 95 78-125
Dibromomethane ug/L 49.550 99 82-120
Ethylbenzene ug/L 48.550 97 79-121
Iodomethane ug/L 100100 100 39-154
Methylene Chloride ug/L 51.450 103 64-133
Styrene ug/L 48.650 97 84-126
Tetrachloroethene ug/L 46.350 93 78-122
Toluene ug/L 52.750 105 80-121
trans-1,2-Dichloroethene ug/L 54.850 110 71-127
trans-1,3-Dichloropropene ug/L 61.850 124 69-141
trans-1,4-Dichloro-2-butene ug/L 49.5J50 99 40-160
Trichloroethene ug/L 51.350 103 78-122
Trichlorofluoromethane ug/L 57.650 115 53-137
Vinyl acetate ug/L 107100 107 40-160
Vinyl chloride ug/L 45.050 90 58-137
Xylene (Total)ug/L 145150 97 81-126
1,2-Dichloroethane-d4 (S)%105 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1903280MATRIX SPIKE SAMPLE:
MSSpike
Result
92325007009
1,1,1,2-Tetrachloroethane ug/L 20.520 102 70-130ND
1,1,1-Trichloroethane ug/L 22.420 112 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.720 103 70-130ND
1,1,2-Trichloroethane ug/L 21.020 105 70-130ND
1,1-Dichloroethane ug/L 21.520 108 70-130ND
1,1-Dichloroethene ug/L 22.420 112 70-166ND
1,2,3-Trichloropropane ug/L 20.720 103 70-130ND
1,2-Dibromo-3-chloropropane ug/L 21.220 106 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.220 106 70-130ND
1,2-Dichlorobenzene ug/L 21.720 108 70-130ND
1,2-Dichloroethane ug/L 22.020 109 70-130ND
1,2-Dichloropropane ug/L 21.220 106 70-130ND
1,4-Dichlorobenzene ug/L 21.320 107 70-130ND
2-Butanone (MEK)ug/L 41.1J40 103 70-130ND
2-Hexanone ug/L 42.4J40 106 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 40.7J40 102 70-130ND
Acetone ug/L 46.2J40 111 70-130ND
Acrylonitrile ug/L 109J100 109 70-130ND
Benzene ug/L 22.320 112 70-148ND
Bromochloromethane ug/L 21.020 105 70-130ND
Bromodichloromethane ug/L 22.820 114 70-130ND
Bromoform ug/L 18.720 94 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 90 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1903280MATRIX SPIKE SAMPLE:
MSSpike
Result
92325007009
Bromomethane ug/L 19.720 98 70-130ND
Carbon disulfide ug/L 21.6J20 108 70-130ND
Carbon tetrachloride ug/L 22.020 110 70-130ND
Chlorobenzene ug/L 21.820 109 70-146ND
Chloroethane ug/L 23.620 118 70-130ND
Chloroform ug/L 21.320 107 70-130ND
Chloromethane ug/L 24.220 121 70-130ND
cis-1,2-Dichloroethene ug/L 21.520 107 70-130ND
cis-1,3-Dichloropropene ug/L 20.620 103 70-130ND
Dibromochloromethane ug/L 19.920 99 70-130ND
Dibromomethane ug/L 19.320 97 70-130ND
Ethylbenzene ug/L 22.420 112 70-130ND
Iodomethane ug/L 37.940 95 70-130ND
Methylene Chloride ug/L 19.220 96 70-130ND
Styrene ug/L 21.320 107 70-130ND
Tetrachloroethene ug/L 19.820 99 70-130ND
Toluene ug/L 21.720 109 70-155ND
trans-1,2-Dichloroethene ug/L 22.420 112 70-130ND
trans-1,3-Dichloropropene ug/L 21.020 105 70-130ND
trans-1,4-Dichloro-2-butene ug/L 18.5J20 92 70-130ND
Trichloroethene ug/L 20.320 102 69-151ND
Trichlorofluoromethane ug/L 25.720 128 70-130ND
Vinyl acetate ug/L 32.1J40 80 70-130ND
Vinyl chloride ug/L 19.220 96 70-130ND
1,2-Dichloroethane-d4 (S)%112 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92325007010
1903281SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 0.37J 300.40J
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 91 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92325007010
1903281SAMPLE DUPLICATE:
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 0.48J 300.41J
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%108 1108
4-Bromofluorobenzene (S)%100 3102
Toluene-d8 (S)%103 1102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 92 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343283
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92325007016, 92325007017, 92325007018, 92325007019, 92325007020, 92325007021, 92325007022,
92325007023, 92325007024, 92325007025, 92325007026, 92325007027, 92325007028, 92325007029,
92325007030, 92325007031
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1903982
Associated Lab Samples:92325007016, 92325007017, 92325007018, 92325007019, 92325007020, 92325007021, 92325007022,
92325007023, 92325007024, 92325007025, 92325007026, 92325007027, 92325007028, 92325007029,
92325007030, 92325007031
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 01/04/17 11:460.33
1,1,1-Trichloroethane ug/L ND 1.0 01/04/17 11:460.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 01/04/17 11:460.40
1,1,2-Trichloroethane ug/L ND 1.0 01/04/17 11:460.29
1,1-Dichloroethane ug/L ND 5.0 01/04/17 11:460.32
1,1-Dichloroethene ug/L ND 5.0 01/04/17 11:460.56
1,2,3-Trichloropropane ug/L ND 1.0 01/04/17 11:460.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 01/04/17 11:462.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 01/04/17 11:460.27
1,2-Dichlorobenzene ug/L ND 5.0 01/04/17 11:460.30
1,2-Dichloroethane ug/L ND 1.0 01/04/17 11:460.24
1,2-Dichloropropane ug/L ND 1.0 01/04/17 11:460.27
1,4-Dichlorobenzene ug/L ND 1.0 01/04/17 11:460.33
2-Butanone (MEK)ug/L ND 100 01/04/17 11:460.96
2-Hexanone ug/L ND 50.0 01/04/17 11:460.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 01/04/17 11:460.33
Acetone ug/L ND 100 01/04/17 11:4610.0
Acrylonitrile ug/L ND 200 01/04/17 11:461.9
Benzene ug/L ND 1.0 01/04/17 11:460.25
Bromochloromethane ug/L ND 3.0 01/04/17 11:460.17
Bromodichloromethane ug/L ND 1.0 01/04/17 11:460.18
Bromoform ug/L ND 3.0 01/04/17 11:460.26
Bromomethane ug/L ND 10.0 01/04/17 11:460.29
Carbon disulfide ug/L ND 100 01/04/17 11:461.2
Carbon tetrachloride ug/L ND 1.0 01/04/17 11:460.25
Chlorobenzene ug/L ND 3.0 01/04/17 11:460.23
Chloroethane ug/L ND 10.0 01/04/17 11:460.54
Chloroform ug/L ND 5.0 01/04/17 11:460.14
Chloromethane ug/L ND 1.0 01/04/17 11:460.11
cis-1,2-Dichloroethene ug/L ND 5.0 01/04/17 11:460.19
cis-1,3-Dichloropropene ug/L ND 1.0 01/04/17 11:460.13
Dibromochloromethane ug/L ND 3.0 01/04/17 11:460.21
Dibromomethane ug/L ND 10.0 01/04/17 11:460.21
Ethylbenzene ug/L ND 1.0 01/04/17 11:460.30
Iodomethane ug/L ND 10.0 01/04/17 11:460.32
Methylene Chloride ug/L ND 1.0 01/04/17 11:460.97
Styrene ug/L ND 1.0 01/04/17 11:460.26
Tetrachloroethene ug/L ND 1.0 01/04/17 11:460.46
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 93 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1903982
Associated Lab Samples:92325007016, 92325007017, 92325007018, 92325007019, 92325007020, 92325007021, 92325007022,
92325007023, 92325007024, 92325007025, 92325007026, 92325007027, 92325007028, 92325007029,
92325007030, 92325007031
Matrix:Water
AnalyzedMDL
Toluene ug/L ND 1.0 01/04/17 11:460.26
trans-1,2-Dichloroethene ug/L ND 5.0 01/04/17 11:460.49
trans-1,3-Dichloropropene ug/L ND 1.0 01/04/17 11:460.26
trans-1,4-Dichloro-2-butene ug/L ND 100 01/04/17 11:461.0
Trichloroethene ug/L ND 1.0 01/04/17 11:460.47
Trichlorofluoromethane ug/L ND 1.0 01/04/17 11:460.20
Vinyl acetate ug/L ND 50.0 01/04/17 11:460.35
Vinyl chloride ug/L ND 1.0 01/04/17 11:460.62
Xylene (Total)ug/L ND 5.0 01/04/17 11:460.66
1,2-Dichloroethane-d4 (S)%109 70-130 01/04/17 11:46
4-Bromofluorobenzene (S)%100 70-130 01/04/17 11:46
Toluene-d8 (S)%105 70-130 01/04/17 11:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1903983LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 55.550 111 80-125
1,1,1-Trichloroethane ug/L 50.050 100 71-129
1,1,2,2-Tetrachloroethane ug/L 51.750 103 79-124
1,1,2-Trichloroethane ug/L 52.250 104 85-125
1,1-Dichloroethane ug/L 47.550 95 73-126
1,1-Dichloroethene ug/L 50.950 102 66-135
1,2,3-Trichloropropane ug/L 51.950 104 75-130
1,2-Dibromo-3-chloropropane ug/L 55.450 111 71-133
1,2-Dibromoethane (EDB)ug/L 53.550 107 83-124
1,2-Dichlorobenzene ug/L 50.550 101 80-133
1,2-Dichloroethane ug/L 49.650 99 67-128
1,2-Dichloropropane ug/L 50.550 101 75-132
1,4-Dichlorobenzene ug/L 49.450 99 78-130
2-Butanone (MEK)ug/L 111100 111 61-144
2-Hexanone ug/L 114100 114 68-143
4-Methyl-2-pentanone (MIBK)ug/L 103100 103 72-135
Acetone ug/L 122100 122 48-146
Acrylonitrile ug/L 245250 98 40-160
Benzene ug/L 51.650 103 80-125
Bromochloromethane ug/L 46.550 93 71-125
Bromodichloromethane ug/L 53.850 108 78-124
Bromoform ug/L 47.750 95 71-128
Bromomethane ug/L 47.650 95 40-160
Carbon disulfide ug/L 47.3J50 95 50-160
Carbon tetrachloride ug/L 51.750 103 69-131
Chlorobenzene ug/L 50.850 102 81-122
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 94 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1903983LABORATORY CONTROL SAMPLE:
LCSSpike
Chloroethane ug/L 49.450 99 39-148
Chloroform ug/L 47.850 96 73-127
Chloromethane ug/L 49.550 99 44-146
cis-1,2-Dichloroethene ug/L 47.450 95 74-124
cis-1,3-Dichloropropene ug/L 54.950 110 72-132
Dibromochloromethane ug/L 51.050 102 78-125
Dibromomethane ug/L 45.750 91 82-120
Ethylbenzene ug/L 50.750 101 79-121
Iodomethane ug/L 92.3100 92 39-154
Methylene Chloride ug/L 47.150 94 64-133
Styrene ug/L 51.850 104 84-126
Tetrachloroethene ug/L 47.950 96 78-122
Toluene ug/L 48.950 98 80-121
trans-1,2-Dichloroethene ug/L 50.150 100 71-127
trans-1,3-Dichloropropene ug/L 56.950 114 69-141
trans-1,4-Dichloro-2-butene ug/L 67.0J50 134 40-160
Trichloroethene ug/L 47.750 95 78-122
Trichlorofluoromethane ug/L 53.050 106 53-137
Vinyl acetate ug/L 97.5100 98 40-160
Vinyl chloride ug/L 39.950 80 58-137
Xylene (Total)ug/L 155150 103 81-126
1,2-Dichloroethane-d4 (S)%104 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1903984MATRIX SPIKE SAMPLE:
MSSpike
Result
92325007020
1,1,1,2-Tetrachloroethane ug/L 21.920 110 70-130ND
1,1,1-Trichloroethane ug/L 23.820 119 70-130ND
1,1,2,2-Tetrachloroethane ug/L 22.420 112 70-130ND
1,1,2-Trichloroethane ug/L 22.620 113 70-130ND
1,1-Dichloroethane ug/L 31.720 118 70-1308.0
1,1-Dichloroethene ug/L 25.720 129 70-166ND
1,2,3-Trichloropropane ug/L 22.320 112 70-130ND
1,2-Dibromo-3-chloropropane ug/L 23.020 115 70-130ND
1,2-Dibromoethane (EDB)ug/L 22.520 113 70-130ND
1,2-Dichlorobenzene ug/L 23.020 115 70-130ND
1,2-Dichloroethane ug/L 23.120 114 70-1300.27J
1,2-Dichloropropane ug/L 24.120 116 70-1300.83J
1,4-Dichlorobenzene ug/L 24.620 111 70-1302.3
2-Butanone (MEK)ug/L 45.6J40 114 70-130ND
2-Hexanone ug/L 45.0J40 113 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 43.3J40 108 70-130ND
Acetone ug/L 46.3J40 116 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 95 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1903984MATRIX SPIKE SAMPLE:
MSSpike
Result
92325007020
Acrylonitrile ug/L 112J100 112 70-130ND
Benzene ug/L 26.120 119 70-1482.3
Bromochloromethane ug/L 21.620 108 70-130ND
Bromodichloromethane ug/L 23.920 120 70-130ND
Bromoform ug/L 19.820 99 70-130ND
Bromomethane ug/L 22.420 112 70-130ND
Carbon disulfide ug/L 22.8J20 114 70-130ND
Carbon tetrachloride ug/L 23.420 117 70-130ND
Chlorobenzene ug/L 23.420 113 70-1460.75J
Chloroethane ug/L 24.920 122 70-1300.62J
Chloroform ug/L 23.620 118 70-130ND
Chloromethane ug/L 26.020 130 70-130ND
cis-1,2-Dichloroethene ug/L 46.020 113 70-13023.3
cis-1,3-Dichloropropene ug/L 22.220 111 70-130ND
Dibromochloromethane ug/L 21.420 107 70-130ND
Dibromomethane ug/L 20.220 101 70-130ND
Ethylbenzene ug/L 23.220 116 70-130ND
Iodomethane ug/L 40.640 102 70-130ND
Methylene Chloride ug/L 21.220 106 70-130ND
Styrene ug/L 17.820 89 70-130ND
Tetrachloroethene ug/L 22.020 104 70-1301.2
Toluene ug/L 22.720 113 70-155ND
trans-1,2-Dichloroethene ug/L 23.620 117 70-130ND
trans-1,3-Dichloropropene ug/L 22.520 112 70-130ND
trans-1,4-Dichloro-2-butene ug/L 21.9J20 110 70-130ND
Trichloroethene ug/L 23.420 109 69-1511.5
Trichlorofluoromethane ug/L 27.7 M12013970-130ND
Vinyl acetate ug/L 32.9J40 82 70-130ND
Vinyl chloride ug/L 19.920 100 70-130ND
1,2-Dichloroethane-d4 (S)%115 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92325025006
1903985SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 96 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92325025006
1903985SAMPLE DUPLICATE:
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L 0.13J 30ND
cis-1,2-Dichloroethene ug/L 13.4 6 3012.6
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%108 4113
4-Bromofluorobenzene (S)%98 395
Toluene-d8 (S)%109 2107
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 97 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343493
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92325007003, 92325007004, 92325007012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1905258
Associated Lab Samples:92325007003, 92325007004, 92325007012
Matrix:Water
AnalyzedMDL
Alkalinity, Total as CaCO3 ug/L ND 5000 01/06/17 00:161000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1905259LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 ug/L 5130050000 103 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1905260MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92325007003
1905261
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L M1500002480-12031 2 2550000141000153000157000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 98 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343148
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92325007003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1903332
Associated Lab Samples:92325007003
Matrix:Water
AnalyzedMDL
Sulfide ug/L ND 1000 01/03/17 11:00100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1903333LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 506J500 101 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1903334MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92324946007
1903335
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L M1,R15004780-12069 38 10500ND233J344J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1903336MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92324946017
1903337
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L M1,R15008380-12067 22 10500ND415J333J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 99 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343373
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92325007004, 92325007012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1904652
Associated Lab Samples:92325007004, 92325007012
Matrix:Water
AnalyzedMDL
Sulfide ug/L ND 1000 01/05/17 10:50100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1904653LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 500J500 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1904654MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92325007004
1904655
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L M15006580-12066 3 10500ND323J332J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 100 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343338
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92325007003, 92325007004, 92325007012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1904351
Associated Lab Samples:92325007003, 92325007004, 92325007012
Matrix:Water
AnalyzedMDL
Sulfate ug/L ND 250000 01/04/17 17:201000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1904352LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 20500J20000 103 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1904353MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92324351001
1904354
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L 20000 92 90-11093 1 10200009.4 mg/L 27800J 28000J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1904355MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92325025002
1904356
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L 20000 92 90-11092 0 10200003230J21700J21700J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 101 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343084
EPA 353.2
EPA 353.2
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples:92325007003, 92325007012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1903107
Associated Lab Samples:92325007003, 92325007012
Matrix:Water
AnalyzedMDL
Nitrogen, Nitrate ug/L ND 20.0 12/30/16 21:1510.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1903108LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate ug/L 24802500 99 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1903109MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92325007003
1903110
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Nitrate ug/L M125006090-11060 1 102500ND15101500
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 102 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343398
EPA 353.2
EPA 353.2
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples:92325007004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1904781
Associated Lab Samples:92325007004
Matrix:Water
AnalyzedMDL
Nitrogen, Nitrate ug/L ND 20.0 01/04/17 20:4110.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1904782LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate ug/L 24402500 97 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1904783MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92325175002
1904784
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Nitrate ug/L 2500 99 90-11099 0 102500ND24702470
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 103 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343216
SM 4500-Cl-E
SM 4500-Cl-E
4500 Chloride
Associated Lab Samples:92325007003, 92325007004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1903778
Associated Lab Samples:92325007003, 92325007004
Matrix:Water
AnalyzedMDL
Chloride ug/L ND 1000 01/03/17 17:29500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1903779LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride ug/L 1930020000 96 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1903780MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92323984001
1903781
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L 10000 105 90-110104 0 101000038701430014300
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1903782MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92324286002
1903783
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L 10000 95 90-11092 1 1010000301003960039300
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 104 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343225
SM 4500-Cl-E
SM 4500-Cl-E
4500 Chloride
Associated Lab Samples:92325007012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1903834
Associated Lab Samples:92325007012
Matrix:Water
AnalyzedMDL
Chloride ug/L ND 1000 01/03/17 17:56500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1903835LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride ug/L 1930020000 96 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1903836MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92325007012
1903837
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L 10000 105 90-110101 1 1010000189002940029000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 105 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343325
SM 5220D
SM 5220D
5220D COD
Associated Lab Samples:92325007003, 92325007004, 92325007012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1904170
Associated Lab Samples:92325007003, 92325007004, 92325007012
Matrix:Water
AnalyzedMDL
Chemical Oxygen Demand ug/L ND 25000 01/04/17 15:0012500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1904171LABORATORY CONTROL SAMPLE:
LCSSpike
Chemical Oxygen Demand ug/L 796000750000 106 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1904172MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92324988001
1904173
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L M17500005990-11059 0 37500004270 mg/L 4720000 4720000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1904174MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92325150001
1904175
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L 750000 98 90-11099 1 3750000ND742000753000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 106 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
344965
SM 5310B
SM 5310B
5310B TOC
Associated Lab Samples:92325007003, 92325007004, 92325007012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1914017
Associated Lab Samples:92325007003, 92325007004, 92325007012
Matrix:Water
AnalyzedMDL
Total Organic Carbon ug/L ND 1000 01/19/17 21:26500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1914018LABORATORY CONTROL SAMPLE:
LCSSpike
Total Organic Carbon ug/L 2580025000 103 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1914019MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92325007003
1914020
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Total Organic Carbon ug/L 25000 105 90-110106 1 1025000845J2710027400
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
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9800 Kincey Ave. Suite 100
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[phone]
Page 107 of 125
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analysis conducted outside the EPA method holding time.H1
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter.N2
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
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9800 Kincey Ave. Suite 100
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Page 108 of 125
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92325007001 343300MW-1 RSK 175 Modified
92325007002 343300MW-1B RSK 175 Modified
92325007003 343300MW-12 RSK 175 Modified
92325007004 343300MW-12D RSK 175 Modified
92325007012 343300MW-24 RSK 175 Modified
92325007013 343300MW-25 RSK 175 Modified
92325007015 343300MW-6 RSK 175 Modified
92325007017 343300MW-5 RSK 175 Modified
92325007020 343300MW-16 RSK 175 Modified
92325007001 343387 343415MW-1 EPA 3010A EPA 6010
92325007002 343387 343415MW-1B EPA 3010A EPA 6010
92325007003 343387 343415MW-12 EPA 3010A EPA 6010
92325007004 343387 343415MW-12D EPA 3010A EPA 6010
92325007005 343179 343232MW-13 EPA 3010A EPA 6010
92325007006 343179 343232MW-14 EPA 3010A EPA 6010
92325007007 343179 343232MW-15 EPA 3010A EPA 6010
92325007008 343387 343415MW-17 EPA 3010A EPA 6010
92325007009 343387 343415MW-19 EPA 3010A EPA 6010
92325007010 343179 343232MW-20 EPA 3010A EPA 6010
92325007011 343387 343415MW-21 EPA 3010A EPA 6010
92325007012 343179 343232MW-24 EPA 3010A EPA 6010
92325007013 343179 343232MW-25 EPA 3010A EPA 6010
92325007014 343644 343787MW-7 EPA 3010A EPA 6010
92325007015 343179 343232MW-6 EPA 3010A EPA 6010
92325007016 343387 343415MW-4R EPA 3010A EPA 6010
92325007017 343387 343415MW-5 EPA 3010A EPA 6010
92325007018 343387 343415MW-9 EPA 3010A EPA 6010
92325007019 343387 343415MW-10 EPA 3010A EPA 6010
92325007020 343387 343415MW-16 EPA 3010A EPA 6010
92325007021 343387 343415MW-22 EPA 3010A EPA 6010
92325007022 343387 343415MW-23 EPA 3010A EPA 6010
92325007023 343387 343415MW-32 EPA 3010A EPA 6010
92325007024 343387 343415MW-33 EPA 3010A EPA 6010
92325007025 343387 343415MW-34 EPA 3010A EPA 6010
92325007026 343388 343416SW-3 EPA 3010A EPA 6010
92325007027 343388 343416SW-4R EPA 3010A EPA 6010
92325007028 343388 343416SW-5 EPA 3010A EPA 6010
92325007029 343388 343416SW-6 EPA 3010A EPA 6010
92325007030 343388 343416EBEPA 3010A EPA 6010
92325007003 343403 343417MW-12 EPA 3010 EPA 6010
92325007004 343403 343417MW-12D EPA 3010 EPA 6010
92325007012 343403 343417MW-24 EPA 3010 EPA 6010
92325007001 343250 343260MW-1 EPA 7470 EPA 7470
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
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Page 109 of 125
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92325007002 343250 343260MW-1B EPA 7470 EPA 7470
92325007007 343250 343260MW-15 EPA 7470 EPA 7470
92325007008 343250 343260MW-17 EPA 7470 EPA 7470
92325007011 343250 343260MW-21 EPA 7470 EPA 7470
92325007015 343250 343260MW-6 EPA 7470 EPA 7470
92325007030 343250 343260EBEPA 7470 EPA 7470
92325007001 343140MW-1 EPA 8260
92325007002 343140MW-1B EPA 8260
92325007003 343140MW-12 EPA 8260
92325007004 343140MW-12D EPA 8260
92325007005 343140MW-13 EPA 8260
92325007006 343140MW-14 EPA 8260
92325007007 343140MW-15 EPA 8260
92325007008 343140MW-17 EPA 8260
92325007009 343141MW-19 EPA 8260
92325007010 343141MW-20 EPA 8260
92325007011 343141MW-21 EPA 8260
92325007012 343141MW-24 EPA 8260
92325007013 343141MW-25 EPA 8260
92325007014 343141MW-7 EPA 8260
92325007015 343141MW-6 EPA 8260
92325007016 343283MW-4R EPA 8260
92325007017 343283MW-5 EPA 8260
92325007018 343283MW-9 EPA 8260
92325007019 343283MW-10 EPA 8260
92325007020 343283MW-16 EPA 8260
92325007021 343283MW-22 EPA 8260
92325007022 343283MW-23 EPA 8260
92325007023 343283MW-32 EPA 8260
92325007024 343283MW-33 EPA 8260
92325007025 343283MW-34 EPA 8260
92325007026 343283SW-3 EPA 8260
92325007027 343283SW-4R EPA 8260
92325007028 343283SW-5 EPA 8260
92325007029 343283SW-6 EPA 8260
92325007030 343283EBEPA 8260
92325007031 343283TBEPA 8260
92325007003 343493MW-12 SM 2320B
92325007004 343493MW-12D SM 2320B
92325007012 343493MW-24 SM 2320B
92325007003 343148MW-12 SM 4500-S2D
92325007004 343373MW-12D SM 4500-S2D
92325007012 343373MW-24 SM 4500-S2D
92325007003 343338MW-12 EPA 300.0
92325007004 343338MW-12D EPA 300.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
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Page 110 of 125
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92325007
ALEXANDER LF-SWS
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92325007012 343338MW-24 EPA 300.0
92325007003 343084MW-12 EPA 353.2
92325007004 343398MW-12D EPA 353.2
92325007012 343084MW-24 EPA 353.2
92325007003 343216MW-12 SM 4500-Cl-E
92325007004 343216MW-12D SM 4500-Cl-E
92325007012 343225MW-24 SM 4500-Cl-E
92325007003 343325MW-12 SM 5220D
92325007004 343325MW-12D SM 5220D
92325007012 343325MW-24 SM 5220D
92325007003 344965MW-12 SM 5310B
92325007004 344965MW-12D SM 5310B
92325007012 344965MW-24 SM 5310B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:20 AM
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Page 111 of 125
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#=CL#
January 20, 2017
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92325025
92325025
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
Alexander LF (SWS & UIC)
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory between December 30,
2016 and January 03, 2017. The results relate only to the samples included in this report. Results
reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's
Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 56
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
Page 2 of 56
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Lab ID Sample ID Matrix Date Collected Date Received
92325025001 MW-3 Water 12/29/16 15:10 12/30/16 07:00
92325025002 MW-11 Water 12/29/16 15:50 12/30/16 07:00
92325025003 MW-26 Water 12/29/16 13:35 12/30/16 07:00
92325025004 MW-31 Water 12/29/16 12:00 12/30/16 07:00
92325025005 MW-18 Water 12/29/16 11:52 12/30/16 07:00
92325025006 MW-27 Water 12/31/16 09:50 01/03/17 09:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 3 of 56
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92325025001 MW-3 EPA 8260 50 PASI-CZDO
SM 2320B 1 PASI-AKDF
EPA 300.0 1 PASI-AAES2
SM 4500-Cl-E 1 PASI-AWRC
SM 5220D 1 PASI-AEWS
SM 5310B 1 PASI-AMDW
92325025002 MW-11 EPA 6010 15 PASI-ASER
EPA 6010 1 PASI-ASH1
EPA 8260 50 PASI-CZDO
SM 2320B 1 PASI-AKDF
SM 4500-S2D 1 PASI-AEWS
EPA 300.0 1 PASI-AAES2
EPA 353.2 1 PASI-AWRC
SM 4500-Cl-E 1 PASI-AWRC
SM 5220D 1 PASI-AEWS
SM 5310B 1 PASI-AMDW
92325025003 MW-26 EPA 6010 15 PASI-ASER
EPA 6010 1 PASI-ASH1
EPA 8260 50 PASI-CZDO
SM 2320B 1 PASI-AKDF
SM 4500-S2D 1 PASI-AEWS
EPA 300.0 1 PASI-AAES2
EPA 353.2 1 PASI-AWRC
SM 4500-Cl-E 1 PASI-AWRC
SM 5220D 1 PASI-AEWS
SM 5310B 1 PASI-AMDW
92325025004 MW-31 EPA 6010 15 PASI-ASH1
EPA 6010 1 PASI-ASH1
EPA 8260 50 PASI-CZDO
SM 2320B 1 PASI-AKDF
SM 4500-S2D 1 PASI-AEWS
EPA 300.0 1 PASI-AAES2
EPA 353.2 1 PASI-AWRC
SM 4500-Cl-E 1 PASI-AWRC
SM 5220D 1 PASI-AEWS
SM 5310B 1 PASI-AMDW
92325025005 MW-18 EPA 6010 15 PASI-ASH1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 56
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 6010 1 PASI-ASH1
EPA 7470 1 PASI-AWAB
EPA 8260 50 PASI-CZDO
92325025006 MW-27 EPA 6010 15 PASI-ASH1
EPA 8260 50 PASI-CZDO
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Sample:MW-3 Lab ID:92325025001 Collected:12/29/16 15:10 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/17 21:34 67-64-110010.0 1
Acrylonitrile ND ug/L 01/03/17 21:34 107-13-12001.9 1
Benzene 5.3 ug/L 01/03/17 21:34 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/03/17 21:34 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/03/17 21:34 75-27-41.0 0.18 1
Bromoform ND ug/L 01/03/17 21:34 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/03/17 21:34 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/03/17 21:34 78-93-31000.96 1
Carbon disulfide ND ug/L 01/03/17 21:34 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/03/17 21:34 56-23-51.0 0.25 1
Chlorobenzene 1.5J ug/L 01/03/17 21:34 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/03/17 21:34 75-00-310.0 0.54 1
Chloroform ND ug/L 01/03/17 21:34 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/03/17 21:34 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/17 21:34 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/03/17 21:34 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/17 21:34 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/03/17 21:34 74-95-310.0 0.21 1
1,2-Dichlorobenzene 0.75J ug/L 01/03/17 21:34 95-50-15.0 0.30 1
1,4-Dichlorobenzene 10.4 ug/L 01/03/17 21:34 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/17 21:34 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/03/17 21:34 75-34-35.0 0.32 1
1,2-Dichloroethane 0.36J ug/L 01/03/17 21:34 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/03/17 21:34 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 5.4 ug/L 01/03/17 21:34 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/03/17 21:34 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/03/17 21:34 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/03/17 21:34 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/03/17 21:34 10061-02-61.0 0.26 1
Ethylbenzene 1.1 ug/L 01/03/17 21:34 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/03/17 21:34 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/03/17 21:34 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/03/17 21:34 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/17 21:34 108-10-11000.33 1
Styrene ND ug/L 01/03/17 21:34 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/17 21:34 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/17 21:34 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/03/17 21:34 127-18-41.0 0.46 1
Toluene 0.35J ug/L 01/03/17 21:34 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/03/17 21:34 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/03/17 21:34 79-00-51.0 0.29 1
Trichloroethene 0.56J ug/L 01/03/17 21:34 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/03/17 21:34 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/03/17 21:34 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/03/17 21:34 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/03/17 21:34 75-01-41.0 0.62 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
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Page 6 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Sample:MW-3 Lab ID:92325025001 Collected:12/29/16 15:10 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Xylene (Total)2.6J ug/L 01/03/17 21:34 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %01/03/17 21:34 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %01/03/17 21:34 17060-07-070-130 1
Toluene-d8 (S)103 %01/03/17 21:34 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 93600 ug/L 01/06/17 01:58500010001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 1870J ug/L 01/04/17 19:36 14808-79-825000010001
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 25300 ug/L 01/03/17 18:03 16887-00-610005001
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 28000 ug/L 01/06/17 15:0025000125001
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 4820 ug/L 01/20/17 00:25 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 7 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Sample:MW-11 Lab ID:92325025002 Collected:12/29/16 15:50 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/05/17 02:06 7440-36-001/03/17 17:006.0 3.8 1
Arsenic 5.5J ug/L 01/05/17 02:06 7440-38-201/03/17 17:0010.0 2.5 1
Barium 163 ug/L 01/05/17 02:06 7440-39-301/03/17 17:001002.5 1
Beryllium ND ug/L 01/05/17 02:06 7440-41-701/03/17 17:001.0 0.50 1
Cadmium ND ug/L 01/05/17 02:06 7440-43-901/03/17 17:001.0 0.50 1
Chromium 8.1J ug/L 01/05/17 02:06 7440-47-301/03/17 17:0010.0 2.5 1
Cobalt 97.3 ug/L 01/05/17 02:06 7440-48-401/03/17 17:0010.0 2.5 1
Copper 10.5 ug/L 01/05/17 02:06 7440-50-801/03/17 17:0010.0 2.5 1
Lead 3.4J ug/L 01/05/17 02:06 7439-92-101/03/17 17:0010.0 2.5 1
Nickel 14.0J ug/L 01/05/17 02:06 7440-02-001/03/17 17:0050.0 2.5 1
Selenium ND ug/L 01/05/17 02:06 7782-49-201/03/17 17:0010.0 5.0 1
Silver ND ug/L 01/05/17 02:06 7440-22-401/03/17 17:0010.0 2.5 1
Thallium ND ug/L 01/05/17 02:06 7440-28-001/03/17 17:005.5 5.0 1
Vanadium ND ug/L 01/05/17 02:06 7440-62-201/03/17 17:0025.0 2.5 1
Zinc 64.2 ug/L 01/05/17 02:06 7440-66-601/03/17 17:0010.0 5.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP, Lab Filtered
Iron, Dissolved 39100 ug/L 01/05/17 15:34 7439-89-601/04/17 21:0050.0 25.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/17 21:52 67-64-110010.0 1
Acrylonitrile ND ug/L 01/03/17 21:52 107-13-12001.9 1
Benzene 2.8 ug/L 01/03/17 21:52 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/03/17 21:52 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/03/17 21:52 75-27-41.0 0.18 1
Bromoform ND ug/L 01/03/17 21:52 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/03/17 21:52 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/03/17 21:52 78-93-31000.96 1
Carbon disulfide ND ug/L 01/03/17 21:52 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/03/17 21:52 56-23-51.0 0.25 1
Chlorobenzene 2.0J ug/L 01/03/17 21:52 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/03/17 21:52 75-00-310.0 0.54 1
Chloroform ND ug/L 01/03/17 21:52 67-66-35.0 0.14 1
Chloromethane 0.14J ug/L 01/03/17 21:52 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/17 21:52 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/03/17 21:52 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/17 21:52 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/03/17 21:52 74-95-310.0 0.21 1
1,2-Dichlorobenzene 0.47J ug/L 01/03/17 21:52 95-50-15.0 0.30 1
1,4-Dichlorobenzene 8.4 ug/L 01/03/17 21:52 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/17 21:52 110-57-61001.0 1
1,1-Dichloroethane 0.40J ug/L 01/03/17 21:52 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/03/17 21:52 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/03/17 21:52 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 16.7 ug/L 01/03/17 21:52 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/03/17 21:52 156-60-55.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
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Page 8 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Sample:MW-11 Lab ID:92325025002 Collected:12/29/16 15:50 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 01/03/17 21:52 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/03/17 21:52 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/03/17 21:52 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/03/17 21:52 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/03/17 21:52 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/03/17 21:52 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/03/17 21:52 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/17 21:52 108-10-11000.33 1
Styrene ND ug/L 01/03/17 21:52 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/17 21:52 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/17 21:52 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/03/17 21:52 127-18-41.0 0.46 1
Toluene ND ug/L 01/03/17 21:52 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/03/17 21:52 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/03/17 21:52 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/03/17 21:52 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/03/17 21:52 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/03/17 21:52 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/03/17 21:52 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/03/17 21:52 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/03/17 21:52 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %01/03/17 21:52 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %01/03/17 21:52 17060-07-070-130 1
Toluene-d8 (S)103 %01/03/17 21:52 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 166000 ug/L 01/06/17 02:12500010001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 01/05/17 10:50 18496-25-810001001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 3230J ug/L 01/04/17 19:45 14808-79-825000010001
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND ug/L 12/30/16 21:301000010.0 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 78400 ug/L 01/03/17 18:09 16887-00-6500025005
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 45000 ug/L 01/06/17 15:0025000125001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Sample:MW-11 Lab ID:92325025002 Collected:12/29/16 15:50 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 6070 ug/L 01/20/17 00:35 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Sample:MW-26 Lab ID:92325025003 Collected:12/29/16 13:35 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/05/17 02:10 7440-36-001/03/17 17:006.0 3.8 1
Arsenic 7.0J ug/L 01/05/17 02:10 7440-38-201/03/17 17:0010.0 2.5 1
Barium 51.3J ug/L 01/05/17 02:10 7440-39-301/03/17 17:001002.5 1
Beryllium ND ug/L 01/05/17 02:10 7440-41-701/03/17 17:001.0 0.50 1
Cadmium ND ug/L 01/05/17 02:10 7440-43-901/03/17 17:001.0 0.50 1
Chromium 3.6J ug/L 01/05/17 02:10 7440-47-301/03/17 17:0010.0 2.5 1
Cobalt 64.7 ug/L 01/05/17 02:10 7440-48-401/03/17 17:0010.0 2.5 1
Copper ND ug/L 01/05/17 02:10 7440-50-801/03/17 17:0010.0 2.5 1
Lead ND ug/L 01/05/17 02:10 7439-92-101/03/17 17:0010.0 2.5 1
Nickel 18.8J ug/L 01/05/17 02:10 7440-02-001/03/17 17:0050.0 2.5 1
Selenium ND ug/L 01/05/17 02:10 7782-49-201/03/17 17:0010.0 5.0 1
Silver ND ug/L 01/05/17 02:10 7440-22-401/03/17 17:0010.0 2.5 1
Thallium ND ug/L 01/05/17 02:10 7440-28-001/03/17 17:005.5 5.0 1
Vanadium ND ug/L 01/05/17 02:10 7440-62-201/03/17 17:0025.0 2.5 1
Zinc 9.0J ug/L 01/05/17 02:10 7440-66-601/03/17 17:0010.0 5.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP, Lab Filtered
Iron, Dissolved 7370 ug/L 01/05/17 15:37 7439-89-601/04/17 21:0050.0 25.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/03/17 22:09 67-64-110010.0 1
Acrylonitrile ND ug/L 01/03/17 22:09 107-13-12001.9 1
Benzene 2.1 ug/L 01/03/17 22:09 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/03/17 22:09 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/03/17 22:09 75-27-41.0 0.18 1
Bromoform ND ug/L 01/03/17 22:09 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/03/17 22:09 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/03/17 22:09 78-93-31000.96 1
Carbon disulfide ND ug/L 01/03/17 22:09 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/03/17 22:09 56-23-51.0 0.25 1
Chlorobenzene 2.0J ug/L 01/03/17 22:09 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/03/17 22:09 75-00-310.0 0.54 1
Chloroform ND ug/L 01/03/17 22:09 67-66-35.0 0.14 1
Chloromethane 0.14J ug/L 01/03/17 22:09 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/03/17 22:09 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/03/17 22:09 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/03/17 22:09 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/03/17 22:09 74-95-310.0 0.21 1
1,2-Dichlorobenzene 0.30J ug/L 01/03/17 22:09 95-50-15.0 0.30 1
1,4-Dichlorobenzene 8.2 ug/L 01/03/17 22:09 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/03/17 22:09 110-57-61001.0 1
1,1-Dichloroethane 0.35J ug/L 01/03/17 22:09 75-34-35.0 0.32 1
1,2-Dichloroethane 0.32J ug/L 01/03/17 22:09 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/03/17 22:09 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 20.8 ug/L 01/03/17 22:09 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/03/17 22:09 156-60-55.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Sample:MW-26 Lab ID:92325025003 Collected:12/29/16 13:35 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 01/03/17 22:09 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/03/17 22:09 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/03/17 22:09 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/03/17 22:09 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/03/17 22:09 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/03/17 22:09 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/03/17 22:09 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/03/17 22:09 108-10-11000.33 1
Styrene ND ug/L 01/03/17 22:09 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/03/17 22:09 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/03/17 22:09 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/03/17 22:09 127-18-41.0 0.46 1
Toluene ND ug/L 01/03/17 22:09 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/03/17 22:09 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/03/17 22:09 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/03/17 22:09 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/03/17 22:09 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/03/17 22:09 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/03/17 22:09 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/03/17 22:09 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/03/17 22:09 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %01/03/17 22:09 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %01/03/17 22:09 17060-07-070-130 1
Toluene-d8 (S)113 %01/03/17 22:09 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 176000 ug/L 01/06/17 02:31500010001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide ND ug/L 01/05/17 10:50 18496-25-810001001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 3280J ug/L 01/04/17 20:13 14808-79-825000010001
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND ug/L 12/30/16 21:241000010.0 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 72000 ug/L 01/03/17 18:10 16887-00-6500025005
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 37000 ug/L 01/06/17 15:0025000125001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Sample:MW-26 Lab ID:92325025003 Collected:12/29/16 13:35 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 6260 ug/L 01/20/17 00:50 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Sample:MW-31 Lab ID:92325025004 Collected:12/29/16 12:00 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/06/17 16:35 7440-36-001/04/17 20:006.0 3.8 1
Arsenic 3.3J ug/L 01/06/17 16:35 7440-38-201/04/17 20:0010.0 2.5 1
Barium 121 ug/L 01/05/17 16:49 7440-39-301/04/17 20:001002.5 1
Beryllium ND ug/L 01/05/17 16:49 7440-41-701/04/17 20:001.0 0.50 1
Cadmium ND ug/L 01/05/17 16:49 7440-43-901/04/17 20:001.0 0.50 1
Chromium 3.5J ug/L 01/05/17 16:49 7440-47-301/04/17 20:0010.0 2.5 1
Cobalt ND ug/L 01/06/17 16:35 7440-48-401/04/17 20:0010.0 2.5 1
Copper ND ug/L 01/06/17 16:35 7440-50-801/04/17 20:0010.0 2.5 1
Lead ND ug/L 01/06/17 16:35 7439-92-101/04/17 20:0010.0 2.5 1
Nickel 4.2J ug/L 01/05/17 16:49 7440-02-001/04/17 20:0050.0 2.5 1
Selenium ND ug/L 01/06/17 16:35 7782-49-201/04/17 20:0010.0 5.0 1
Silver ND ug/L 01/05/17 16:49 7440-22-401/04/17 20:0010.0 2.5 1
Thallium ND ug/L 01/05/17 16:49 7440-28-001/04/17 20:005.5 5.0 1
Vanadium 4.2J ug/L 01/05/17 16:49 7440-62-201/04/17 20:0025.0 2.5 1
Zinc 9.6J ug/L 01/06/17 16:35 7440-66-601/04/17 20:0010.0 5.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP, Lab Filtered
Iron, Dissolved 177 ug/L 01/05/17 15:40 7439-89-601/04/17 21:0050.0 25.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/04/17 01:21 67-64-110010.0 1
Acrylonitrile ND ug/L 01/04/17 01:21 107-13-12001.9 1
Benzene ND ug/L 01/04/17 01:21 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/04/17 01:21 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/04/17 01:21 75-27-41.0 0.18 1
Bromoform ND ug/L 01/04/17 01:21 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/04/17 01:21 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/04/17 01:21 78-93-31000.96 1
Carbon disulfide ND ug/L 01/04/17 01:21 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/04/17 01:21 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/04/17 01:21 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/04/17 01:21 75-00-310.0 0.54 1
Chloroform ND ug/L 01/04/17 01:21 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/04/17 01:21 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/04/17 01:21 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/04/17 01:21 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/04/17 01:21 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/04/17 01:21 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/04/17 01:21 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/04/17 01:21 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/04/17 01:21 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/04/17 01:21 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/04/17 01:21 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/04/17 01:21 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.71J ug/L 01/04/17 01:21 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/04/17 01:21 156-60-55.0 0.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Sample:MW-31 Lab ID:92325025004 Collected:12/29/16 12:00 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,2-Dichloropropane ND ug/L 01/04/17 01:21 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/04/17 01:21 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/04/17 01:21 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/04/17 01:21 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/04/17 01:21 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/04/17 01:21 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/04/17 01:21 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/04/17 01:21 108-10-11000.33 1
Styrene ND ug/L 01/04/17 01:21 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/04/17 01:21 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/04/17 01:21 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/04/17 01:21 127-18-41.0 0.46 1
Toluene ND ug/L 01/04/17 01:21 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/04/17 01:21 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/04/17 01:21 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/04/17 01:21 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/04/17 01:21 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/04/17 01:21 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/04/17 01:21 108-05-4 M150.0 0.35 1
Vinyl chloride ND ug/L 01/04/17 01:21 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/04/17 01:21 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %01/04/17 01:21 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %01/04/17 01:21 17060-07-070-130 1
Toluene-d8 (S)105 %01/04/17 01:21 2037-26-570-130 1
Analytical Method: SM 2320B2320B Alkalinity
Alkalinity, Total as CaCO3 35300 ug/L 01/06/17 03:31500010001
Analytical Method: SM 4500-S2D4500S2D Sulfide Water
Sulfide 525J ug/L 01/05/17 10:50 18496-25-810001001
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 2150J ug/L 01/04/17 20:22 14808-79-825000010001
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate 1480J ug/L 12/30/16 21:231000010.0 1
Analytical Method: SM 4500-Cl-E4500 Chloride
Chloride 13500 ug/L 01/03/17 18:05 16887-00-610005001
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand ND ug/L 01/06/17 15:0025000125001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 15 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Sample:MW-31 Lab ID:92325025004 Collected:12/29/16 12:00 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 5310B5310B TOC
Total Organic Carbon 1310 ug/L 01/20/17 01:04 7440-44-010005001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
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9800 Kincey Ave. Suite 100
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[phone]
Page 16 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Sample:MW-18 Lab ID:92325025005 Collected:12/29/16 11:52 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/06/17 16:38 7440-36-001/04/17 20:006.0 3.8 1
Arsenic 2.6J ug/L 01/06/17 16:38 7440-38-201/04/17 20:0010.0 2.5 1
Barium 16.0J ug/L 01/05/17 16:52 7440-39-301/04/17 20:001002.5 1
Beryllium ND ug/L 01/05/17 16:52 7440-41-701/04/17 20:001.0 0.50 1
Cadmium ND ug/L 01/05/17 16:52 7440-43-901/04/17 20:001.0 0.50 1
Chromium ND ug/L 01/05/17 16:52 7440-47-301/04/17 20:0010.0 2.5 1
Cobalt ND ug/L 01/06/17 16:38 7440-48-401/04/17 20:0010.0 2.5 1
Copper ND ug/L 01/06/17 16:38 7440-50-801/04/17 20:0010.0 2.5 1
Lead ND ug/L 01/06/17 16:38 7439-92-101/04/17 20:0010.0 2.5 1
Nickel 2.5J ug/L 01/05/17 16:52 7440-02-001/04/17 20:0050.0 2.5 1
Selenium ND ug/L 01/06/17 16:38 7782-49-201/04/17 20:0010.0 5.0 1
Silver ND ug/L 01/05/17 16:52 7440-22-401/04/17 20:0010.0 2.5 1
Thallium ND ug/L 01/05/17 16:52 7440-28-001/04/17 20:005.5 5.0 1
Vanadium ND ug/L 01/05/17 16:52 7440-62-201/04/17 20:0025.0 2.5 1
Zinc ND ug/L 01/06/17 16:38 7440-66-601/04/17 20:0010.0 5.0 1
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP, Lab Filtered
Iron, Dissolved ND ug/L 01/05/17 15:43 7439-89-601/04/17 21:0050.0 25.0 1
Analytical Method: EPA 7470 Preparation Method: EPA 74707470 Mercury
Mercury 0.73 ug/L 01/04/17 15:35 7439-97-601/04/17 04:000.20 0.10 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/04/17 01:39 67-64-110010.0 1
Acrylonitrile ND ug/L 01/04/17 01:39 107-13-12001.9 1
Benzene ND ug/L 01/04/17 01:39 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/04/17 01:39 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/04/17 01:39 75-27-41.0 0.18 1
Bromoform ND ug/L 01/04/17 01:39 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/04/17 01:39 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/04/17 01:39 78-93-31000.96 1
Carbon disulfide ND ug/L 01/04/17 01:39 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/04/17 01:39 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/04/17 01:39 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/04/17 01:39 75-00-310.0 0.54 1
Chloroform ND ug/L 01/04/17 01:39 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/04/17 01:39 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/04/17 01:39 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/04/17 01:39 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/04/17 01:39 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/04/17 01:39 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/04/17 01:39 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/04/17 01:39 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/04/17 01:39 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/04/17 01:39 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/04/17 01:39 107-06-21.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
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Page 17 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Sample:MW-18 Lab ID:92325025005 Collected:12/29/16 11:52 Received:12/30/16 07:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
1,1-Dichloroethene ND ug/L 01/04/17 01:39 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 01/04/17 01:39 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/04/17 01:39 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/04/17 01:39 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/04/17 01:39 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/04/17 01:39 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 01/04/17 01:39 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/04/17 01:39 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/04/17 01:39 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/04/17 01:39 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/04/17 01:39 108-10-11000.33 1
Styrene ND ug/L 01/04/17 01:39 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/04/17 01:39 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/04/17 01:39 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/04/17 01:39 127-18-41.0 0.46 1
Toluene ND ug/L 01/04/17 01:39 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/04/17 01:39 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/04/17 01:39 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/04/17 01:39 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/04/17 01:39 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/04/17 01:39 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/04/17 01:39 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/04/17 01:39 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/04/17 01:39 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %01/04/17 01:39 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %01/04/17 01:39 17060-07-070-130 1
Toluene-d8 (S)109 %01/04/17 01:39 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
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Page 18 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Sample:MW-27 Lab ID:92325025006 Collected:12/31/16 09:50 Received:01/03/17 09:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3010A6010 ICP Groundwater
Antimony ND ug/L 01/05/17 18:20 7440-36-001/04/17 20:006.0 3.8 1
Arsenic ND ug/L 01/10/17 15:45 7440-38-201/04/17 20:0010.0 2.5 1
Barium 63.4J ug/L 01/05/17 18:20 7440-39-301/04/17 20:001002.5 1
Beryllium ND ug/L 01/05/17 18:20 7440-41-701/04/17 20:001.0 0.50 1
Cadmium ND ug/L 01/05/17 18:20 7440-43-901/04/17 20:001.0 0.50 1
Chromium ND ug/L 01/05/17 18:20 7440-47-301/04/17 20:0010.0 2.5 1
Cobalt ND ug/L 01/05/17 18:20 7440-48-401/04/17 20:0010.0 2.5 1
Copper ND ug/L 01/05/17 18:20 7440-50-801/04/17 20:0010.0 2.5 1
Lead ND ug/L 01/05/17 18:20 7439-92-101/04/17 20:0010.0 2.5 1
Nickel 22.4J ug/L 01/05/17 18:20 7440-02-001/04/17 20:0050.0 2.5 1
Selenium ND ug/L 01/05/17 18:20 7782-49-201/04/17 20:0010.0 5.0 1
Silver ND ug/L 01/05/17 18:20 7440-22-401/04/17 20:0010.0 2.5 1
Thallium ND ug/L 01/05/17 18:20 7440-28-001/04/17 20:005.5 5.0 1
Vanadium ND ug/L 01/05/17 18:20 7440-62-201/04/17 20:0025.0 2.5 1
Zinc 6.7J ug/L 01/05/17 18:20 7440-66-601/04/17 20:0010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 01/04/17 17:17 67-64-110010.0 1
Acrylonitrile ND ug/L 01/04/17 17:17 107-13-12001.9 1
Benzene ND ug/L 01/04/17 17:17 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 01/04/17 17:17 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 01/04/17 17:17 75-27-41.0 0.18 1
Bromoform ND ug/L 01/04/17 17:17 75-25-23.0 0.26 1
Bromomethane ND ug/L 01/04/17 17:17 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 01/04/17 17:17 78-93-31000.96 1
Carbon disulfide ND ug/L 01/04/17 17:17 75-15-01001.2 1
Carbon tetrachloride ND ug/L 01/04/17 17:17 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 01/04/17 17:17 108-90-73.0 0.23 1
Chloroethane ND ug/L 01/04/17 17:17 75-00-310.0 0.54 1
Chloroform ND ug/L 01/04/17 17:17 67-66-35.0 0.14 1
Chloromethane ND ug/L 01/04/17 17:17 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 01/04/17 17:17 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 01/04/17 17:17 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 01/04/17 17:17 106-93-41.0 0.27 1
Dibromomethane ND ug/L 01/04/17 17:17 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 01/04/17 17:17 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 01/04/17 17:17 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 01/04/17 17:17 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 01/04/17 17:17 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 01/04/17 17:17 107-06-21.0 0.24 1
1,1-Dichloroethene ND ug/L 01/04/17 17:17 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 12.6 ug/L 01/04/17 17:17 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 01/04/17 17:17 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 01/04/17 17:17 78-87-51.0 0.27 1
cis-1,3-Dichloropropene ND ug/L 01/04/17 17:17 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 01/04/17 17:17 10061-02-61.0 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 56
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Sample:MW-27 Lab ID:92325025006 Collected:12/31/16 09:50 Received:01/03/17 09:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Ethylbenzene ND ug/L 01/04/17 17:17 100-41-41.0 0.30 1
2-Hexanone ND ug/L 01/04/17 17:17 591-78-650.0 0.46 1
Iodomethane ND ug/L 01/04/17 17:17 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 01/04/17 17:17 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 01/04/17 17:17 108-10-11000.33 1
Styrene ND ug/L 01/04/17 17:17 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 01/04/17 17:17 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 01/04/17 17:17 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 01/04/17 17:17 127-18-41.0 0.46 1
Toluene ND ug/L 01/04/17 17:17 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 01/04/17 17:17 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 01/04/17 17:17 79-00-51.0 0.29 1
Trichloroethene ND ug/L 01/04/17 17:17 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 01/04/17 17:17 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 01/04/17 17:17 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 01/04/17 17:17 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 01/04/17 17:17 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 01/04/17 17:17 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)95 %01/04/17 17:17 460-00-470-130 1
1,2-Dichloroethane-d4 (S)113 %01/04/17 17:17 17060-07-070-130 1
Toluene-d8 (S)107 %01/04/17 17:17 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343250
EPA 7470
EPA 7470
7470 Mercury
Associated Lab Samples:92325025005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1903882
Associated Lab Samples:92325025005
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 01/04/17 15:070.10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1903883LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.52.5 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1903884MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92325007001
1903885
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L M12.5 40 75-12533 18 252.5ND 1.0 0.83
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343179
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92325025002, 92325025003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1903459
Associated Lab Samples:92325025002, 92325025003
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 01/05/17 00:403.8
Arsenic ug/L ND 10.0 01/05/17 00:402.5
Barium ug/L ND 100 01/05/17 00:402.5
Beryllium ug/L ND 1.0 01/05/17 00:400.50
Cadmium ug/L ND 1.0 01/05/17 00:400.50
Chromium ug/L ND 10.0 01/05/17 00:402.5
Cobalt ug/L ND 10.0 01/05/17 00:402.5
Copper ug/L ND 10.0 01/05/17 00:402.5
Lead ug/L ND 10.0 01/05/17 00:402.5
Nickel ug/L ND 50.0 01/05/17 00:402.5
Selenium ug/L ND 10.0 01/05/17 00:405.0
Silver ug/L ND 10.0 01/05/17 00:402.5
Thallium ug/L ND 5.5 01/05/17 00:405.0
Vanadium ug/L ND 25.0 01/05/17 00:402.5
Zinc ug/L ND 10.0 01/05/17 00:405.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1903460LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 468500 94 80-120
Arsenic ug/L 463500 93 80-120
Barium ug/L 504500 101 80-120
Beryllium ug/L 484500 97 80-120
Cadmium ug/L 472500 94 80-120
Chromium ug/L 494500 99 80-120
Cobalt ug/L 475500 95 80-120
Copper ug/L 488500 98 80-120
Lead ug/L 469500 94 80-120
Nickel ug/L 470500 94 80-120
Selenium ug/L 478500 96 80-120
Silver ug/L 242250 97 80-120
Thallium ug/L 497500 99 80-120
Vanadium ug/L 472500 94 80-120
Zinc ug/L 483500 97 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1903461MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92324987001
1903462
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 94 75-12593 1 25500ND473469
Arsenic ug/L 500 94 75-12593 1 25500ND470464
Barium ug/L 500 102 75-12596 4 25500172683654
Beryllium ug/L 500 99 75-12594 5 25500ND494471
Cadmium ug/L 500 95 75-12593 2 25500ND474463
Chromium ug/L 500 99 75-12595 4 25500ND494476
Cobalt ug/L 500 93 75-12591 2 25500ND463453
Copper ug/L 500 98 75-12595 3 25500ND490474
Lead ug/L 500 91 75-12590 2 25500ND456449
Nickel ug/L 500 91 75-12589 2 25500ND456446
Selenium ug/L 500 95 75-12594 1 25500ND477472
Silver ug/L 250 96 75-12593 3 25250ND242234
Thallium ug/L 500 95 75-12595 0 25500ND479477
Vanadium ug/L 500 96 75-12593 3 25500ND481466
Zinc ug/L 500 94 75-12592 2 25500ND471462
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343387
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92325025004, 92325025005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1904720
Associated Lab Samples:92325025004, 92325025005
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 01/05/17 15:593.8
Arsenic ug/L ND 10.0 01/05/17 15:592.5
Barium ug/L ND 100 01/05/17 15:592.5
Beryllium ug/L ND 1.0 01/05/17 15:590.50
Cadmium ug/L ND 1.0 01/05/17 15:590.50
Chromium ug/L ND 10.0 01/05/17 15:592.5
Cobalt ug/L ND 10.0 01/05/17 15:592.5
Copper ug/L ND 10.0 01/05/17 15:592.5
Lead ug/L ND 10.0 01/05/17 15:592.5
Nickel ug/L ND 50.0 01/05/17 15:592.5
Selenium ug/L ND 10.0 01/05/17 15:595.0
Silver ug/L ND 10.0 01/05/17 15:592.5
Thallium ug/L ND 5.5 01/05/17 15:595.0
Vanadium ug/L ND 25.0 01/05/17 15:592.5
Zinc ug/L ND 10.0 01/05/17 15:595.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1904721LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 440500 88 80-120
Arsenic ug/L 422500 84 80-120
Barium ug/L 496500 99 80-120
Beryllium ug/L 495500 99 80-120
Cadmium ug/L 458500 92 80-120
Chromium ug/L 476500 95 80-120
Cobalt ug/L 449500 90 80-120
Copper ug/L 472500 94 80-120
Lead ug/L 445500 89 80-120
Nickel ug/L 450500 90 80-120
Selenium ug/L 446500 89 80-120
Silver ug/L 237250 95 80-120
Thallium ug/L 482500 96 80-120
Vanadium ug/L 456500 91 80-120
Zinc ug/L 445500 89 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1904722MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92325007001
1904723
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 90 75-12589 2 25500ND451444
Arsenic ug/L 500 85 75-12585 1 25500ND430426
Barium ug/L 500 100 75-12598 2 2550038.9J 539 528
Beryllium ug/L 500 102 75-12599 3 25500ND509496
Cadmium ug/L 500 93 75-12591 2 255001.3 466 458
Chromium ug/L 500 95 75-12594 0 25500ND474472
Cobalt ug/L 500 90 75-12588 2 255007.3J 456 449
Copper ug/L 500 96 75-12594 2 25500ND478470
Lead ug/L 500 88 75-12587 1 25500ND444438
Nickel ug/L 500 89 75-12588 1 255004.3J 451 444
Selenium ug/L 500 90 75-12588 2 25500ND450442
Silver ug/L 250 97 75-12595 2 25250ND241236
Thallium ug/L 500 95 75-12595 0 255005.7 479 479
Vanadium ug/L 500 94 75-12592 2 25500ND471462
Zinc ug/L 500 89 75-12588 1 2550031.3 477 470
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343388
EPA 3010A
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92325025006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1904725
Associated Lab Samples:92325025006
Matrix:Water
AnalyzedMDL
Antimony ug/L ND 6.0 01/06/17 17:233.8
Arsenic ug/L ND 10.0 01/10/17 15:382.5
Barium ug/L ND 100 01/05/17 17:402.5
Beryllium ug/L ND 1.0 01/05/17 17:400.50
Cadmium ug/L ND 1.0 01/05/17 17:400.50
Chromium ug/L ND 10.0 01/05/17 17:402.5
Cobalt ug/L ND 10.0 01/06/17 17:232.5
Copper ug/L ND 10.0 01/06/17 17:232.5
Lead ug/L ND 10.0 01/06/17 17:232.5
Nickel ug/L ND 50.0 01/05/17 17:402.5
Selenium ug/L ND 10.0 01/06/17 17:235.0
Silver ug/L ND 10.0 01/05/17 17:402.5
Thallium ug/L ND 5.5 01/05/17 17:405.0
Vanadium ug/L ND 25.0 01/05/17 17:402.5
Zinc ug/L ND 10.0 01/06/17 17:235.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1904726LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 485500 97 80-120
Arsenic ug/L 479500 96 80-120
Barium ug/L 495500 99 80-120
Beryllium ug/L 495500 99 80-120
Cadmium ug/L 457500 91 80-120
Chromium ug/L 474500 95 80-120
Cobalt ug/L 491500 98 80-120
Copper ug/L 496500 99 80-120
Lead ug/L 481500 96 80-120
Nickel ug/L 446500 89 80-120
Selenium ug/L 490500 98 80-120
Silver ug/L 236250 95 80-120
Thallium ug/L 463500 93 80-120
Vanadium ug/L 456500 91 80-120
Zinc ug/L 493500 99 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1904727MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92325007026
1904728
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 86 75-12586 1 25500ND430432
Arsenic ug/L 500 94 75-12597 3 255002.6J 472 486
Barium ug/L 500 95 75-12597 2 2550065.5J 541 553
Beryllium ug/L 500 96 75-12598 1 25500ND482489
Cadmium ug/L 500 89 75-12590 2 25500ND445452
Chromium ug/L 500 91 75-12594 4 255004.0J 457 475
Cobalt ug/L 500 87 75-12588 1 255006.1J 439 445
Copper ug/L 500 91 75-12594 3 25500ND456471
Lead ug/L 500 85 75-12587 2 25500ND427433
Nickel ug/L 500 86 75-12588 2 255004.9J 436 443
Selenium ug/L 500 86 75-12588 2 25500ND433441
Silver ug/L 250 92 75-12594 2 25250ND230235
Thallium ug/L 500 88 75-12590 2 255005.6 446 454
Vanadium ug/L 500 90 75-12591 2 255003.5J 452 460
Zinc ug/L 500 88 75-12589 1 255007.2J 447 450
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343403
EPA 3010
EPA 6010
6010 MET Filtered Diss.
Associated Lab Samples:92325025002, 92325025003, 92325025004, 92325025005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1904826
Associated Lab Samples:92325025002, 92325025003, 92325025004, 92325025005
Matrix:Water
AnalyzedMDL
Iron, Dissolved ug/L ND 50.0 01/05/17 15:0325.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1904827LABORATORY CONTROL SAMPLE:
LCSSpike
Iron, Dissolved ug/L 43405000 87 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1904828MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92325007003
1904829
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Iron, Dissolved ug/L 5000 75 75-12576 0 205000384004220042200
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343141
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92325025001, 92325025002, 92325025003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1903278
Associated Lab Samples:92325025001, 92325025002, 92325025003
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 01/03/17 12:510.33
1,1,1-Trichloroethane ug/L ND 1.0 01/03/17 12:510.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 01/03/17 12:510.40
1,1,2-Trichloroethane ug/L ND 1.0 01/03/17 12:510.29
1,1-Dichloroethane ug/L ND 5.0 01/03/17 12:510.32
1,1-Dichloroethene ug/L ND 5.0 01/03/17 12:510.56
1,2,3-Trichloropropane ug/L ND 1.0 01/03/17 12:510.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 01/03/17 12:512.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 01/03/17 12:510.27
1,2-Dichlorobenzene ug/L ND 5.0 01/03/17 12:510.30
1,2-Dichloroethane ug/L ND 1.0 01/03/17 12:510.24
1,2-Dichloropropane ug/L ND 1.0 01/03/17 12:510.27
1,4-Dichlorobenzene ug/L ND 1.0 01/03/17 12:510.33
2-Butanone (MEK)ug/L ND 100 01/03/17 12:510.96
2-Hexanone ug/L ND 50.0 01/03/17 12:510.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 01/03/17 12:510.33
Acetone ug/L ND 100 01/03/17 12:5110.0
Acrylonitrile ug/L ND 200 01/03/17 12:511.9
Benzene ug/L ND 1.0 01/03/17 12:510.25
Bromochloromethane ug/L ND 3.0 01/03/17 12:510.17
Bromodichloromethane ug/L ND 1.0 01/03/17 12:510.18
Bromoform ug/L ND 3.0 01/03/17 12:510.26
Bromomethane ug/L ND 10.0 01/03/17 12:510.29
Carbon disulfide ug/L ND 100 01/03/17 12:511.2
Carbon tetrachloride ug/L ND 1.0 01/03/17 12:510.25
Chlorobenzene ug/L ND 3.0 01/03/17 12:510.23
Chloroethane ug/L ND 10.0 01/03/17 12:510.54
Chloroform ug/L ND 5.0 01/03/17 12:510.14
Chloromethane ug/L ND 1.0 01/03/17 12:510.11
cis-1,2-Dichloroethene ug/L ND 5.0 01/03/17 12:510.19
cis-1,3-Dichloropropene ug/L ND 1.0 01/03/17 12:510.13
Dibromochloromethane ug/L ND 3.0 01/03/17 12:510.21
Dibromomethane ug/L ND 10.0 01/03/17 12:510.21
Ethylbenzene ug/L ND 1.0 01/03/17 12:510.30
Iodomethane ug/L ND 10.0 01/03/17 12:510.32
Methylene Chloride ug/L ND 1.0 01/03/17 12:510.97
Styrene ug/L ND 1.0 01/03/17 12:510.26
Tetrachloroethene ug/L ND 1.0 01/03/17 12:510.46
Toluene ug/L ND 1.0 01/03/17 12:510.26
trans-1,2-Dichloroethene ug/L ND 5.0 01/03/17 12:510.49
trans-1,3-Dichloropropene ug/L ND 1.0 01/03/17 12:510.26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1903278
Associated Lab Samples:92325025001, 92325025002, 92325025003
Matrix:Water
AnalyzedMDL
trans-1,4-Dichloro-2-butene ug/L ND 100 01/03/17 12:511.0
Trichloroethene ug/L ND 1.0 01/03/17 12:510.47
Trichlorofluoromethane ug/L ND 1.0 01/03/17 12:510.20
Vinyl acetate ug/L ND 50.0 01/03/17 12:510.35
Vinyl chloride ug/L ND 1.0 01/03/17 12:510.62
Xylene (Total)ug/L ND 5.0 01/03/17 12:510.66
1,2-Dichloroethane-d4 (S)%104 70-130 01/03/17 12:51
4-Bromofluorobenzene (S)%104 70-130 01/03/17 12:51
Toluene-d8 (S)%106 70-130 01/03/17 12:51
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1903279LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 53.250 106 80-125
1,1,1-Trichloroethane ug/L 56.350 113 71-129
1,1,2,2-Tetrachloroethane ug/L 49.350 99 79-124
1,1,2-Trichloroethane ug/L 56.050 112 85-125
1,1-Dichloroethane ug/L 52.050 104 73-126
1,1-Dichloroethene ug/L 55.050 110 66-135
1,2,3-Trichloropropane ug/L 49.650 99 75-130
1,2-Dibromo-3-chloropropane ug/L 50.950 102 71-133
1,2-Dibromoethane (EDB)ug/L 50.550 101 83-124
1,2-Dichlorobenzene ug/L 46.750 93 80-133
1,2-Dichloroethane ug/L 53.050 106 67-128
1,2-Dichloropropane ug/L 53.950 108 75-132
1,4-Dichlorobenzene ug/L 45.650 91 78-130
2-Butanone (MEK)ug/L 113100 113 61-144
2-Hexanone ug/L 103100 103 68-143
4-Methyl-2-pentanone (MIBK)ug/L 108100 108 72-135
Acetone ug/L 109100 109 48-146
Acrylonitrile ug/L 268250 107 40-160
Benzene ug/L 55.850 112 80-125
Bromochloromethane ug/L 52.250 104 71-125
Bromodichloromethane ug/L 57.950 116 78-124
Bromoform ug/L 46.350 93 71-128
Bromomethane ug/L 49.050 98 40-160
Carbon disulfide ug/L 53.2J50 106 50-160
Carbon tetrachloride ug/L 56.450 113 69-131
Chlorobenzene ug/L 48.550 97 81-122
Chloroethane ug/L 54.350 109 39-148
Chloroform ug/L 52.150 104 73-127
Chloromethane ug/L 56.750 113 44-146
cis-1,2-Dichloroethene ug/L 51.350 103 74-124
cis-1,3-Dichloropropene ug/L 59.950 120 72-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1903279LABORATORY CONTROL SAMPLE:
LCSSpike
Dibromochloromethane ug/L 47.750 95 78-125
Dibromomethane ug/L 49.550 99 82-120
Ethylbenzene ug/L 48.550 97 79-121
Iodomethane ug/L 100100 100 39-154
Methylene Chloride ug/L 51.450 103 64-133
Styrene ug/L 48.650 97 84-126
Tetrachloroethene ug/L 46.350 93 78-122
Toluene ug/L 52.750 105 80-121
trans-1,2-Dichloroethene ug/L 54.850 110 71-127
trans-1,3-Dichloropropene ug/L 61.850 124 69-141
trans-1,4-Dichloro-2-butene ug/L 49.5J50 99 40-160
Trichloroethene ug/L 51.350 103 78-122
Trichlorofluoromethane ug/L 57.650 115 53-137
Vinyl acetate ug/L 107100 107 40-160
Vinyl chloride ug/L 45.050 90 58-137
Xylene (Total)ug/L 145150 97 81-126
1,2-Dichloroethane-d4 (S)%105 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1903280MATRIX SPIKE SAMPLE:
MSSpike
Result
92325007009
1,1,1,2-Tetrachloroethane ug/L 20.520 102 70-130ND
1,1,1-Trichloroethane ug/L 22.420 112 70-130ND
1,1,2,2-Tetrachloroethane ug/L 20.720 103 70-130ND
1,1,2-Trichloroethane ug/L 21.020 105 70-130ND
1,1-Dichloroethane ug/L 21.520 108 70-130ND
1,1-Dichloroethene ug/L 22.420 112 70-166ND
1,2,3-Trichloropropane ug/L 20.720 103 70-130ND
1,2-Dibromo-3-chloropropane ug/L 21.220 106 70-130ND
1,2-Dibromoethane (EDB)ug/L 21.220 106 70-130ND
1,2-Dichlorobenzene ug/L 21.720 108 70-130ND
1,2-Dichloroethane ug/L 22.020 109 70-130ND
1,2-Dichloropropane ug/L 21.220 106 70-130ND
1,4-Dichlorobenzene ug/L 21.320 107 70-130ND
2-Butanone (MEK)ug/L 41.1J40 103 70-130ND
2-Hexanone ug/L 42.4J40 106 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 40.7J40 102 70-130ND
Acetone ug/L 46.2J40 111 70-130ND
Acrylonitrile ug/L 109J100 109 70-130ND
Benzene ug/L 22.320 112 70-148ND
Bromochloromethane ug/L 21.020 105 70-130ND
Bromodichloromethane ug/L 22.820 114 70-130ND
Bromoform ug/L 18.720 94 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1903280MATRIX SPIKE SAMPLE:
MSSpike
Result
92325007009
Bromomethane ug/L 19.720 98 70-130ND
Carbon disulfide ug/L 21.6J20 108 70-130ND
Carbon tetrachloride ug/L 22.020 110 70-130ND
Chlorobenzene ug/L 21.820 109 70-146ND
Chloroethane ug/L 23.620 118 70-130ND
Chloroform ug/L 21.320 107 70-130ND
Chloromethane ug/L 24.220 121 70-130ND
cis-1,2-Dichloroethene ug/L 21.520 107 70-130ND
cis-1,3-Dichloropropene ug/L 20.620 103 70-130ND
Dibromochloromethane ug/L 19.920 99 70-130ND
Dibromomethane ug/L 19.320 97 70-130ND
Ethylbenzene ug/L 22.420 112 70-130ND
Iodomethane ug/L 37.940 95 70-130ND
Methylene Chloride ug/L 19.220 96 70-130ND
Styrene ug/L 21.320 107 70-130ND
Tetrachloroethene ug/L 19.820 99 70-130ND
Toluene ug/L 21.720 109 70-155ND
trans-1,2-Dichloroethene ug/L 22.420 112 70-130ND
trans-1,3-Dichloropropene ug/L 21.020 105 70-130ND
trans-1,4-Dichloro-2-butene ug/L 18.5J20 92 70-130ND
Trichloroethene ug/L 20.320 102 69-151ND
Trichlorofluoromethane ug/L 25.720 128 70-130ND
Vinyl acetate ug/L 32.1J40 80 70-130ND
Vinyl chloride ug/L 19.220 96 70-130ND
1,2-Dichloroethane-d4 (S)%112 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92325007010
1903281SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 0.37J 300.40J
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92325007010
1903281SAMPLE DUPLICATE:
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 0.48J 300.41J
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%108 1108
4-Bromofluorobenzene (S)%100 3102
Toluene-d8 (S)%103 1102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343144
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92325025004, 92325025005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1903299
Associated Lab Samples:92325025004, 92325025005
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 01/04/17 00:460.33
1,1,1-Trichloroethane ug/L ND 1.0 01/04/17 00:460.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 01/04/17 00:460.40
1,1,2-Trichloroethane ug/L ND 1.0 01/04/17 00:460.29
1,1-Dichloroethane ug/L ND 5.0 01/04/17 00:460.32
1,1-Dichloroethene ug/L ND 5.0 01/04/17 00:460.56
1,2,3-Trichloropropane ug/L ND 1.0 01/04/17 00:460.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 01/04/17 00:462.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 01/04/17 00:460.27
1,2-Dichlorobenzene ug/L ND 5.0 01/04/17 00:460.30
1,2-Dichloroethane ug/L ND 1.0 01/04/17 00:460.24
1,2-Dichloropropane ug/L ND 1.0 01/04/17 00:460.27
1,4-Dichlorobenzene ug/L ND 1.0 01/04/17 00:460.33
2-Butanone (MEK)ug/L ND 100 01/04/17 00:460.96
2-Hexanone ug/L ND 50.0 01/04/17 00:460.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 01/04/17 00:460.33
Acetone ug/L ND 100 01/04/17 00:4610.0
Acrylonitrile ug/L ND 200 01/04/17 00:461.9
Benzene ug/L ND 1.0 01/04/17 00:460.25
Bromochloromethane ug/L ND 3.0 01/04/17 00:460.17
Bromodichloromethane ug/L ND 1.0 01/04/17 00:460.18
Bromoform ug/L ND 3.0 01/04/17 00:460.26
Bromomethane ug/L ND 10.0 01/04/17 00:460.29
Carbon disulfide ug/L ND 100 01/04/17 00:461.2
Carbon tetrachloride ug/L ND 1.0 01/04/17 00:460.25
Chlorobenzene ug/L ND 3.0 01/04/17 00:460.23
Chloroethane ug/L ND 10.0 01/04/17 00:460.54
Chloroform ug/L ND 5.0 01/04/17 00:460.14
Chloromethane ug/L ND 1.0 01/04/17 00:460.11
cis-1,2-Dichloroethene ug/L ND 5.0 01/04/17 00:460.19
cis-1,3-Dichloropropene ug/L ND 1.0 01/04/17 00:460.13
Dibromochloromethane ug/L ND 3.0 01/04/17 00:460.21
Dibromomethane ug/L ND 10.0 01/04/17 00:460.21
Ethylbenzene ug/L ND 1.0 01/04/17 00:460.30
Iodomethane ug/L ND 10.0 01/04/17 00:460.32
Methylene Chloride ug/L ND 1.0 01/04/17 00:460.97
Styrene ug/L ND 1.0 01/04/17 00:460.26
Tetrachloroethene ug/L ND 1.0 01/04/17 00:460.46
Toluene ug/L ND 1.0 01/04/17 00:460.26
trans-1,2-Dichloroethene ug/L ND 5.0 01/04/17 00:460.49
trans-1,3-Dichloropropene ug/L ND 1.0 01/04/17 00:460.26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1903299
Associated Lab Samples:92325025004, 92325025005
Matrix:Water
AnalyzedMDL
trans-1,4-Dichloro-2-butene ug/L ND 100 01/04/17 00:461.0
Trichloroethene ug/L ND 1.0 01/04/17 00:460.47
Trichlorofluoromethane ug/L ND 1.0 01/04/17 00:460.20
Vinyl acetate ug/L ND 50.0 01/04/17 00:460.35
Vinyl chloride ug/L ND 1.0 01/04/17 00:460.62
Xylene (Total)ug/L ND 5.0 01/04/17 00:460.66
1,2-Dichloroethane-d4 (S)%105 70-130 01/04/17 00:46
4-Bromofluorobenzene (S)%99 70-130 01/04/17 00:46
Toluene-d8 (S)%107 70-130 01/04/17 00:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1903300LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.750 105 80-125
1,1,1-Trichloroethane ug/L 50.950 102 71-129
1,1,2,2-Tetrachloroethane ug/L 49.150 98 79-124
1,1,2-Trichloroethane ug/L 51.650 103 85-125
1,1-Dichloroethane ug/L 47.950 96 73-126
1,1-Dichloroethene ug/L 50.950 102 66-135
1,2,3-Trichloropropane ug/L 48.650 97 75-130
1,2-Dibromo-3-chloropropane ug/L 51.850 104 71-133
1,2-Dibromoethane (EDB)ug/L 53.250 106 83-124
1,2-Dichlorobenzene ug/L 49.950 100 80-133
1,2-Dichloroethane ug/L 49.650 99 67-128
1,2-Dichloropropane ug/L 50.650 101 75-132
1,4-Dichlorobenzene ug/L 48.450 97 78-130
2-Butanone (MEK)ug/L 102100 102 61-144
2-Hexanone ug/L 108100 108 68-143
4-Methyl-2-pentanone (MIBK)ug/L 96.9J100 97 72-135
Acetone ug/L 105100 105 48-146
Acrylonitrile ug/L 248250 99 40-160
Benzene ug/L 51.850 104 80-125
Bromochloromethane ug/L 46.850 94 71-125
Bromodichloromethane ug/L 55.150 110 78-124
Bromoform ug/L 44.650 89 71-128
Bromomethane ug/L 46.350 93 40-160
Carbon disulfide ug/L 45.3J50 91 50-160
Carbon tetrachloride ug/L 51.550 103 69-131
Chlorobenzene ug/L 49.850 100 81-122
Chloroethane ug/L 50.050 100 39-148
Chloroform ug/L 48.250 96 73-127
Chloromethane ug/L 51.750 103 44-146
cis-1,2-Dichloroethene ug/L 47.550 95 74-124
cis-1,3-Dichloropropene ug/L 54.050 108 72-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1903300LABORATORY CONTROL SAMPLE:
LCSSpike
Dibromochloromethane ug/L 49.650 99 78-125
Dibromomethane ug/L 46.950 94 82-120
Ethylbenzene ug/L 51.250 102 79-121
Iodomethane ug/L 93.7100 94 39-154
Methylene Chloride ug/L 48.250 96 64-133
Styrene ug/L 53.450 107 84-126
Tetrachloroethene ug/L 45.150 90 78-122
Toluene ug/L 47.750 95 80-121
trans-1,2-Dichloroethene ug/L 50.050 100 71-127
trans-1,3-Dichloropropene ug/L 54.550 109 69-141
trans-1,4-Dichloro-2-butene ug/L 48.3J50 97 40-160
Trichloroethene ug/L 48.250 96 78-122
Trichlorofluoromethane ug/L 52.850 106 53-137
Vinyl acetate ug/L 90.1100 90 40-160
Vinyl chloride ug/L 40.050 80 58-137
Xylene (Total)ug/L 158150 106 81-126
1,2-Dichloroethane-d4 (S)%108 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1903301MATRIX SPIKE SAMPLE:
MSSpike
Result
92325025004
1,1,1,2-Tetrachloroethane ug/L 21.920 110 70-130ND
1,1,1-Trichloroethane ug/L 22.120 110 70-130ND
1,1,2,2-Tetrachloroethane ug/L 23.020 115 70-130ND
1,1,2-Trichloroethane ug/L 21.920 110 70-130ND
1,1-Dichloroethane ug/L 20.520 103 70-130ND
1,1-Dichloroethene ug/L 22.820 114 70-166ND
1,2,3-Trichloropropane ug/L 22.420 112 70-130ND
1,2-Dibromo-3-chloropropane ug/L 23.820 119 70-130ND
1,2-Dibromoethane (EDB)ug/L 23.020 115 70-130ND
1,2-Dichlorobenzene ug/L 21.720 109 70-130ND
1,2-Dichloroethane ug/L 21.520 107 70-130ND
1,2-Dichloropropane ug/L 22.220 111 70-130ND
1,4-Dichlorobenzene ug/L 21.620 107 70-130ND
2-Butanone (MEK)ug/L 48.1J40 120 70-130ND
2-Hexanone ug/L 49.9J40 125 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 45.1J40 113 70-130ND
Acetone ug/L 49.5J40 124 70-130ND
Acrylonitrile ug/L 112J100 112 70-130ND
Benzene ug/L 22.820 114 70-148ND
Bromochloromethane ug/L 20.420 102 70-130ND
Bromodichloromethane ug/L 23.220 116 70-130ND
Bromoform ug/L 19.720 99 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1903301MATRIX SPIKE SAMPLE:
MSSpike
Result
92325025004
Bromomethane ug/L 20.720 103 70-130ND
Carbon disulfide ug/L 20.7J20 104 70-130ND
Carbon tetrachloride ug/L 22.420 112 70-130ND
Chlorobenzene ug/L 22.620 113 70-146ND
Chloroethane ug/L 22.620 113 70-130ND
Chloroform ug/L 21.120 105 70-130ND
Chloromethane ug/L 24.120 121 70-130ND
cis-1,2-Dichloroethene ug/L 21.120 102 70-1300.71J
cis-1,3-Dichloropropene ug/L 21.020 105 70-130ND
Dibromochloromethane ug/L 20.820 104 70-130ND
Dibromomethane ug/L 19.720 98 70-130ND
Ethylbenzene ug/L 23.220 116 70-130ND
Iodomethane ug/L 38.640 97 70-130ND
Methylene Chloride ug/L 18.520 93 70-130ND
Styrene ug/L 18.320 91 70-130ND
Tetrachloroethene ug/L 21.120 105 70-130ND
Toluene ug/L 22.020 110 70-155ND
trans-1,2-Dichloroethene ug/L 21.620 108 70-130ND
trans-1,3-Dichloropropene ug/L 21.420 107 70-130ND
trans-1,4-Dichloro-2-butene ug/L 21.0J20 105 70-130ND
Trichloroethene ug/L 20.620 103 69-151ND
Trichlorofluoromethane ug/L 23.720 118 70-130ND
Vinyl acetate ug/L 25.2J M1406370-130ND
Vinyl chloride ug/L 18.120 91 70-130ND
1,2-Dichloroethane-d4 (S)%106 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92325025005
1903302SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92325025005
1903302SAMPLE DUPLICATE:
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%110 2108
4-Bromofluorobenzene (S)%100 299
Toluene-d8 (S)%105 5109
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343283
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92325025006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1903982
Associated Lab Samples:92325025006
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 01/04/17 11:460.33
1,1,1-Trichloroethane ug/L ND 1.0 01/04/17 11:460.48
1,1,2,2-Tetrachloroethane ug/L ND 3.0 01/04/17 11:460.40
1,1,2-Trichloroethane ug/L ND 1.0 01/04/17 11:460.29
1,1-Dichloroethane ug/L ND 5.0 01/04/17 11:460.32
1,1-Dichloroethene ug/L ND 5.0 01/04/17 11:460.56
1,2,3-Trichloropropane ug/L ND 1.0 01/04/17 11:460.41
1,2-Dibromo-3-chloropropane ug/L ND 13.0 01/04/17 11:462.0
1,2-Dibromoethane (EDB)ug/L ND 1.0 01/04/17 11:460.27
1,2-Dichlorobenzene ug/L ND 5.0 01/04/17 11:460.30
1,2-Dichloroethane ug/L ND 1.0 01/04/17 11:460.24
1,2-Dichloropropane ug/L ND 1.0 01/04/17 11:460.27
1,4-Dichlorobenzene ug/L ND 1.0 01/04/17 11:460.33
2-Butanone (MEK)ug/L ND 100 01/04/17 11:460.96
2-Hexanone ug/L ND 50.0 01/04/17 11:460.46
4-Methyl-2-pentanone (MIBK)ug/L ND 100 01/04/17 11:460.33
Acetone ug/L ND 100 01/04/17 11:4610.0
Acrylonitrile ug/L ND 200 01/04/17 11:461.9
Benzene ug/L ND 1.0 01/04/17 11:460.25
Bromochloromethane ug/L ND 3.0 01/04/17 11:460.17
Bromodichloromethane ug/L ND 1.0 01/04/17 11:460.18
Bromoform ug/L ND 3.0 01/04/17 11:460.26
Bromomethane ug/L ND 10.0 01/04/17 11:460.29
Carbon disulfide ug/L ND 100 01/04/17 11:461.2
Carbon tetrachloride ug/L ND 1.0 01/04/17 11:460.25
Chlorobenzene ug/L ND 3.0 01/04/17 11:460.23
Chloroethane ug/L ND 10.0 01/04/17 11:460.54
Chloroform ug/L ND 5.0 01/04/17 11:460.14
Chloromethane ug/L ND 1.0 01/04/17 11:460.11
cis-1,2-Dichloroethene ug/L ND 5.0 01/04/17 11:460.19
cis-1,3-Dichloropropene ug/L ND 1.0 01/04/17 11:460.13
Dibromochloromethane ug/L ND 3.0 01/04/17 11:460.21
Dibromomethane ug/L ND 10.0 01/04/17 11:460.21
Ethylbenzene ug/L ND 1.0 01/04/17 11:460.30
Iodomethane ug/L ND 10.0 01/04/17 11:460.32
Methylene Chloride ug/L ND 1.0 01/04/17 11:460.97
Styrene ug/L ND 1.0 01/04/17 11:460.26
Tetrachloroethene ug/L ND 1.0 01/04/17 11:460.46
Toluene ug/L ND 1.0 01/04/17 11:460.26
trans-1,2-Dichloroethene ug/L ND 5.0 01/04/17 11:460.49
trans-1,3-Dichloropropene ug/L ND 1.0 01/04/17 11:460.26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1903982
Associated Lab Samples:92325025006
Matrix:Water
AnalyzedMDL
trans-1,4-Dichloro-2-butene ug/L ND 100 01/04/17 11:461.0
Trichloroethene ug/L ND 1.0 01/04/17 11:460.47
Trichlorofluoromethane ug/L ND 1.0 01/04/17 11:460.20
Vinyl acetate ug/L ND 50.0 01/04/17 11:460.35
Vinyl chloride ug/L ND 1.0 01/04/17 11:460.62
Xylene (Total)ug/L ND 5.0 01/04/17 11:460.66
1,2-Dichloroethane-d4 (S)%109 70-130 01/04/17 11:46
4-Bromofluorobenzene (S)%100 70-130 01/04/17 11:46
Toluene-d8 (S)%105 70-130 01/04/17 11:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1903983LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 55.550 111 80-125
1,1,1-Trichloroethane ug/L 50.050 100 71-129
1,1,2,2-Tetrachloroethane ug/L 51.750 103 79-124
1,1,2-Trichloroethane ug/L 52.250 104 85-125
1,1-Dichloroethane ug/L 47.550 95 73-126
1,1-Dichloroethene ug/L 50.950 102 66-135
1,2,3-Trichloropropane ug/L 51.950 104 75-130
1,2-Dibromo-3-chloropropane ug/L 55.450 111 71-133
1,2-Dibromoethane (EDB)ug/L 53.550 107 83-124
1,2-Dichlorobenzene ug/L 50.550 101 80-133
1,2-Dichloroethane ug/L 49.650 99 67-128
1,2-Dichloropropane ug/L 50.550 101 75-132
1,4-Dichlorobenzene ug/L 49.450 99 78-130
2-Butanone (MEK)ug/L 111100 111 61-144
2-Hexanone ug/L 114100 114 68-143
4-Methyl-2-pentanone (MIBK)ug/L 103100 103 72-135
Acetone ug/L 122100 122 48-146
Acrylonitrile ug/L 245250 98 40-160
Benzene ug/L 51.650 103 80-125
Bromochloromethane ug/L 46.550 93 71-125
Bromodichloromethane ug/L 53.850 108 78-124
Bromoform ug/L 47.750 95 71-128
Bromomethane ug/L 47.650 95 40-160
Carbon disulfide ug/L 47.3J50 95 50-160
Carbon tetrachloride ug/L 51.750 103 69-131
Chlorobenzene ug/L 50.850 102 81-122
Chloroethane ug/L 49.450 99 39-148
Chloroform ug/L 47.850 96 73-127
Chloromethane ug/L 49.550 99 44-146
cis-1,2-Dichloroethene ug/L 47.450 95 74-124
cis-1,3-Dichloropropene ug/L 54.950 110 72-132
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
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Huntersville, NC 28078
[phone]
Page 40 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1903983LABORATORY CONTROL SAMPLE:
LCSSpike
Dibromochloromethane ug/L 51.050 102 78-125
Dibromomethane ug/L 45.750 91 82-120
Ethylbenzene ug/L 50.750 101 79-121
Iodomethane ug/L 92.3100 92 39-154
Methylene Chloride ug/L 47.150 94 64-133
Styrene ug/L 51.850 104 84-126
Tetrachloroethene ug/L 47.950 96 78-122
Toluene ug/L 48.950 98 80-121
trans-1,2-Dichloroethene ug/L 50.150 100 71-127
trans-1,3-Dichloropropene ug/L 56.950 114 69-141
trans-1,4-Dichloro-2-butene ug/L 67.0J50 134 40-160
Trichloroethene ug/L 47.750 95 78-122
Trichlorofluoromethane ug/L 53.050 106 53-137
Vinyl acetate ug/L 97.5100 98 40-160
Vinyl chloride ug/L 39.950 80 58-137
Xylene (Total)ug/L 155150 103 81-126
1,2-Dichloroethane-d4 (S)%104 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1903984MATRIX SPIKE SAMPLE:
MSSpike
Result
92325007020
1,1,1,2-Tetrachloroethane ug/L 21.920 110 70-130ND
1,1,1-Trichloroethane ug/L 23.820 119 70-130ND
1,1,2,2-Tetrachloroethane ug/L 22.420 112 70-130ND
1,1,2-Trichloroethane ug/L 22.620 113 70-130ND
1,1-Dichloroethane ug/L 31.720 118 70-1308.0
1,1-Dichloroethene ug/L 25.720 129 70-166ND
1,2,3-Trichloropropane ug/L 22.320 112 70-130ND
1,2-Dibromo-3-chloropropane ug/L 23.020 115 70-130ND
1,2-Dibromoethane (EDB)ug/L 22.520 113 70-130ND
1,2-Dichlorobenzene ug/L 23.020 115 70-130ND
1,2-Dichloroethane ug/L 23.120 114 70-1300.27J
1,2-Dichloropropane ug/L 24.120 116 70-1300.83J
1,4-Dichlorobenzene ug/L 24.620 111 70-1302.3
2-Butanone (MEK)ug/L 45.6J40 114 70-130ND
2-Hexanone ug/L 45.0J40 113 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 43.3J40 108 70-130ND
Acetone ug/L 46.3J40 116 70-130ND
Acrylonitrile ug/L 112J100 112 70-130ND
Benzene ug/L 26.120 119 70-1482.3
Bromochloromethane ug/L 21.620 108 70-130ND
Bromodichloromethane ug/L 23.920 120 70-130ND
Bromoform ug/L 19.820 99 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
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Huntersville, NC 28078
[phone]
Page 41 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1903984MATRIX SPIKE SAMPLE:
MSSpike
Result
92325007020
Bromomethane ug/L 22.420 112 70-130ND
Carbon disulfide ug/L 22.8J20 114 70-130ND
Carbon tetrachloride ug/L 23.420 117 70-130ND
Chlorobenzene ug/L 23.420 113 70-1460.75J
Chloroethane ug/L 24.920 122 70-1300.62J
Chloroform ug/L 23.620 118 70-130ND
Chloromethane ug/L 26.020 130 70-130ND
cis-1,2-Dichloroethene ug/L 46.020 113 70-13023.3
cis-1,3-Dichloropropene ug/L 22.220 111 70-130ND
Dibromochloromethane ug/L 21.420 107 70-130ND
Dibromomethane ug/L 20.220 101 70-130ND
Ethylbenzene ug/L 23.220 116 70-130ND
Iodomethane ug/L 40.640 102 70-130ND
Methylene Chloride ug/L 21.220 106 70-130ND
Styrene ug/L 17.820 89 70-130ND
Tetrachloroethene ug/L 22.020 104 70-1301.2
Toluene ug/L 22.720 113 70-155ND
trans-1,2-Dichloroethene ug/L 23.620 117 70-130ND
trans-1,3-Dichloropropene ug/L 22.520 112 70-130ND
trans-1,4-Dichloro-2-butene ug/L 21.9J20 110 70-130ND
Trichloroethene ug/L 23.420 109 69-1511.5
Trichlorofluoromethane ug/L 27.7 M12013970-130ND
Vinyl acetate ug/L 32.9J40 82 70-130ND
Vinyl chloride ug/L 19.920 100 70-130ND
1,2-Dichloroethane-d4 (S)%115 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92325025006
1903985SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92325025006
1903985SAMPLE DUPLICATE:
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L 0.13J 30ND
cis-1,2-Dichloroethene ug/L 13.4 6 3012.6
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%108 4113
4-Bromofluorobenzene (S)%98 395
Toluene-d8 (S)%109 2107
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343493
SM 2320B
SM 2320B
2320B Alkalinity
Associated Lab Samples:92325025001, 92325025002, 92325025003, 92325025004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1905258
Associated Lab Samples:92325025001, 92325025002, 92325025003, 92325025004
Matrix:Water
AnalyzedMDL
Alkalinity, Total as CaCO3 ug/L ND 5000 01/06/17 00:161000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1905259LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 ug/L 5130050000 103 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1905260MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92325007003
1905261
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 ug/L M1500002480-12031 2 2550000141000153000157000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343373
SM 4500-S2D
SM 4500-S2D
4500S2D Sulfide Water
Associated Lab Samples:92325025002, 92325025003, 92325025004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1904652
Associated Lab Samples:92325025002, 92325025003, 92325025004
Matrix:Water
AnalyzedMDL
Sulfide ug/L ND 1000 01/05/17 10:50100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1904653LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfide ug/L 500J500 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1904654MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92325007004
1904655
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfide ug/L M15006580-12066 3 10500ND323J332J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343338
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92325025001, 92325025002, 92325025003, 92325025004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1904351
Associated Lab Samples:92325025001, 92325025002, 92325025003, 92325025004
Matrix:Water
AnalyzedMDL
Sulfate ug/L ND 250000 01/04/17 17:201000
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1904352LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 20500J20000 103 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1904353MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92324351001
1904354
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L 20000 92 90-11093 1 10200009.4 mg/L 27800J 28000J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1904355MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92325025002
1904356
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L 20000 92 90-11092 0 10200003230J21700J21700J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343084
EPA 353.2
EPA 353.2
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples:92325025002, 92325025003, 92325025004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1903107
Associated Lab Samples:92325025002, 92325025003, 92325025004
Matrix:Water
AnalyzedMDL
Nitrogen, Nitrate ug/L ND 20.0 12/30/16 21:1510.0
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1903108LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate ug/L 24802500 99 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1903109MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92325007003
1903110
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Nitrate ug/L M125006090-11060 1 102500ND15101500
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343225
SM 4500-Cl-E
SM 4500-Cl-E
4500 Chloride
Associated Lab Samples:92325025001, 92325025002, 92325025003, 92325025004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1903834
Associated Lab Samples:92325025001, 92325025002, 92325025003, 92325025004
Matrix:Water
AnalyzedMDL
Chloride ug/L ND 1000 01/03/17 17:56500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1903835LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride ug/L 1930020000 96 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1903836MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92325007012
1903837
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride ug/L 10000 105 90-110101 1 1010000189002940029000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
343609
SM 5220D
SM 5220D
5220D COD
Associated Lab Samples:92325025001, 92325025002, 92325025003, 92325025004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1905852
Associated Lab Samples:92325025001, 92325025002, 92325025003, 92325025004
Matrix:Water
AnalyzedMDL
Chemical Oxygen Demand ug/L ND 25000 01/06/17 15:0012500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1905853LABORATORY CONTROL SAMPLE:
LCSSpike
Chemical Oxygen Demand ug/L 772000750000 103 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1905854MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92325163001
1905855
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L M675000099290-110960 2 37500002630 mg/L 1010000
0 9830000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1905856MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92325025001
1905857
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L 750000 98 90-11099 1 375000028000762000767000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 56
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
344965
SM 5310B
SM 5310B
5310B TOC
Associated Lab Samples:92325025001, 92325025002, 92325025003, 92325025004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1914017
Associated Lab Samples:92325025001, 92325025002, 92325025003, 92325025004
Matrix:Water
AnalyzedMDL
Total Organic Carbon ug/L ND 1000 01/19/17 21:26500
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1914018LABORATORY CONTROL SAMPLE:
LCSSpike
Total Organic Carbon ug/L 2580025000 103 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1914019MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92325007003
1914020
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Total Organic Carbon ug/L 25000 105 90-110106 1 1025000845J2710027400
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 56
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 56
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92325025002 343179 343232MW-11 EPA 3010A EPA 6010
92325025003 343179 343232MW-26 EPA 3010A EPA 6010
92325025004 343387 343415MW-31 EPA 3010A EPA 6010
92325025005 343387 343415MW-18 EPA 3010A EPA 6010
92325025006 343388 343416MW-27 EPA 3010A EPA 6010
92325025002 343403 343417MW-11 EPA 3010 EPA 6010
92325025003 343403 343417MW-26 EPA 3010 EPA 6010
92325025004 343403 343417MW-31 EPA 3010 EPA 6010
92325025005 343403 343417MW-18 EPA 3010 EPA 6010
92325025005 343250 343260MW-18 EPA 7470 EPA 7470
92325025001 343141MW-3 EPA 8260
92325025002 343141MW-11 EPA 8260
92325025003 343141MW-26 EPA 8260
92325025004 343144MW-31 EPA 8260
92325025005 343144MW-18 EPA 8260
92325025006 343283MW-27 EPA 8260
92325025001 343493MW-3 SM 2320B
92325025002 343493MW-11 SM 2320B
92325025003 343493MW-26 SM 2320B
92325025004 343493MW-31 SM 2320B
92325025002 343373MW-11 SM 4500-S2D
92325025003 343373MW-26 SM 4500-S2D
92325025004 343373MW-31 SM 4500-S2D
92325025001 343338MW-3 EPA 300.0
92325025002 343338MW-11 EPA 300.0
92325025003 343338MW-26 EPA 300.0
92325025004 343338MW-31 EPA 300.0
92325025002 343084MW-11 EPA 353.2
92325025003 343084MW-26 EPA 353.2
92325025004 343084MW-31 EPA 353.2
92325025001 343225MW-3 SM 4500-Cl-E
92325025002 343225MW-11 SM 4500-Cl-E
92325025003 343225MW-26 SM 4500-Cl-E
92325025004 343225MW-31 SM 4500-Cl-E
92325025001 343609MW-3 SM 5220D
92325025002 343609MW-11 SM 5220D
92325025003 343609MW-26 SM 5220D
92325025004 343609MW-31 SM 5220D
92325025001 344965MW-3 SM 5310B
92325025002 344965MW-11 SM 5310B
92325025003 344965MW-26 SM 5310B
92325025004 344965MW-31 SM 5310B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 56
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92325025
Alexander LF (SWS & UIC)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/20/2017 09:08 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 56
Page 54 of 56
Page 55 of 56
Page 56 of 56
Appendix B
Field Sampling Parameter Data Sheet(s)