9606_WayneCounty_MSWLF_February_GWM.pdf

Wayne County Subtitle D Lined MSWLF
Dudley, North Carolina
February, 2015
MESCO Project Number: G15016.0
Semi-Annual Water Quality Monitoring Report
Prepared for
Submittal Date: January 4, 2015
Municipal Engineering Services Company, P.A.
Garner and Boone, North Carolina
P.O. Box 97
Garner, NC 27529
License No. C-0281

Permit Number: 96-06
TABLE OF CONTENTS
SECTION
Introduction Page 1
Background Page 1
Sampling Procedures Page 2
Field Parameter Data Page 2
Laboratory Results Page 2
Quality Control Samples Page 2
Groundwater Samples Page 2
Surface Water Samples Page 2
Leachate Samples Page 3
Groundwater and Surface Water Characterization Page 3
Findings Page 3
Closing Page 3
FIGURES
Topographic Map with Site Location Figure 1
Potentiometric Map of Uppermost Aquifer Figure 2
TABLES
Groundwater Monitoring Well Construction Table Table 1
Field Observations of Monitoring Locations Table 2
Field Parameter Data Summary Table 3
Sampling and Analysis Summary Table 4
Detections Above SWSL, GWP, 2L, or 2B (Appendix 1) Table 5
Detections in Leachate Samples above SWSL, GWP or 2L Table 6
Hydrologic Properties at Monitoring Well Locations Table 7
APPENDICIES
Laboratory Analysis Report and Chains of Custody Appendix A
Field Sampling Parameter Data Sheet(s) Appendix B
January 4, 2016
Ms. Jaclynne Drummond
Solid Waste Section
Division of Waste Management
North Carolina Department of Environment and Natural Resources
217 West Jones Street
Raleigh, NC 27603
Re: Semi-Annual Water Quality Monitoring Report
Wayne County Subtitle D Lined MSWLF
Permit No. 96-06
MESCO Project No. G15016.0
Event Date(s): February 11-12, 2015
Introduction
On behalf of Wayne County, Municipal Engineering Services Company, P.A. (MESCO) is pleased to present this
Semi-Annual Water Quality Report for the winter 2015 event performed at the Wayne County Subtitle D Lined
Municipal Solid Waste Landfill (MSWLF). NCDENR Solid Waste Rules 15A NCAC 13B.1632 require that Wayne
County provide this report to the NC SWS on a semi-annual basis. This report documents the quality of the ground,
surface waters and leachate during this monitoring event performed on February 11-12, 2015.
During this event only a few metals were detected in groundwater samples collected both upgradient and
downgradient of the landfill. The preliminary source of the detected metals is not believed to be anthropogenic but
rather a product of erosion of natural deposits. Surface water samples lacked targeted constituents in levels
exceeding (2B) Standards.
Background
The Wayne County Subtitle D lined MSWLF, permit #96-06 (Phases 1-3), is located at 460-B South Landfill Road,
Dudley, Wayne County, North Carolina. The lined MSWLF is comprised of contiguous Phases 1, 2 & 3 which
are treated as a single unit in this report. Phase 3 was granted a Permit to Operate (PTO) on June 11, 2013 and at the
time of this event waste had been placed within the east sump drainage area which is hydraulically divided from the
west sump. Waste is planned to be placed on the west side of the divide prior to the next semiannual event.
Therefore, until waste is placed west side of the divide any detections in wells that monitor the west sump (MW-14
and MW-15) should not be attributed to leachate.
The lined landfill is located west and beyond a perennial local discharge feature from a C&D landfill operating upon
an unlined landfill which is monitored s
As specified within 15A NCAC 13B.1632(j), the SWS Environmental Monitoring Report Form and a recent SWS
memorandum this report contains sampling procedures, field and laboratory results, groundwater and surface water
characterization. Well construction summary table, field observations table, field parameter data table, sampling
and analysis summary table, detections compared to Standards tables, a groundwater flow directions/rates table,
potentiometric map, quality assurance/quality control data, and laboratory analytical data results are enclosed herein.

Sampling Procedure
Samples were collected in accordance with the Ground and Surface Water Sampling & Analysis Plan (SAP) [DIN
13717] dated April 25, 2011 and approved by the SWS on May 19, 2011 [DIN 13957]. The site specific SAP
includes water sample collection and analysis from twelve downgradient monitoring wells (MW-2 through MW-
16R), one background well (MW-1), four surface water locations (SW-2, SW-3, SW-4 and SW-5) and a leachate
sample (LE-1). Surface water point SW-1, located downstream of SW-3, monitors the unnamed tributary of
Edward's Branch as part of the Active C&D and Closed MSWLF SAP. Sampling results are presented as
supplementary data due to the shared discharge features. Quality control measures, which included analysis of
equipment blank samples (EB), field blank samples (FB), and trip blank samples (TB) were also reported.
Monitoring locations are depicted on the potentiometric map of the uppermost aquifer, Figure 2.
A summary detailing the construction of the water monitoring wells is presented on Table 1. The function and
integrity of all monitoring locations were visually evaluated and no deficiencies identified as documented on Table
2. The depth to water in each well was electronically gaged prior to purging to quantify the static water level
elevation. Low-flow pumping methodology or bailing was used to adequately purge the wells to a minimum of
three times the volume of standing water in the well or until dry. Surface water samples were dipped from the
surface at previously designated locations. During well purging and surface water sample collection the required
field parameters were recorded. The samples were then placed into laboratory-prepared, pre-preserved containers
via a new disposable polyethylene bailer. Samples were collected, kept on ice, and transported to a NC-certified
laboratory under proper chain of custody (C-O-C) protocols and analyzed within the proper hold-times.
Field Parameter Data
Stabilized field parameters were recorded during purging which included pH, specific conductance, temperature,
total dissolved solids (TDS) and visual turbidity. A summary of the field parameter data is presented in Table 3 and
the field sampling data sheet is enclosed in Appendix B.
Laboratory Results
Pace Analytical Laboratories (PACE) of Huntersville and Asheville, NC performed the laboratory analysis.
Groundwater, surface water and quality control blank samples were analyzed for the constituents listed in 40 CFR
258 Appendix I including volatile organic compounds (VOCs) by EPA Test Method 8260 and total unfiltered metals
by EPA Test Method series 6000/7000. Leachate samples (LE-1) were analyzed for a leachate specific list that
includes Appendix I parameters, nitrate, phosphorus, chemical oxygen demand (COD), biological oxygen demand
(BOD), sulfate, and pH. A sampling and analysis table summarizing the locations, constituents, and methods is
presented on Table 4.
Water samples were analyzed to the laboratory-established Method Detection Limits (MDL), which are at or below
the current Solid Waste Section Limit (SWSL). Table 5 summarizes constituents detected in groundwater and
surface water samples that attain or were above the current SWSL, Groundwater Protection Standards (GWP), North
Carolina Groundwater Standards (2L), the applicable North Carolina Surface Water Standards (2B) for a class C
waterbody, and Maximum Contaminant Levels (MCL) also known as “Federal Primary Drinking Water Standards”.
Laboratory results and C-O-Cs are presented in Appendix A.
Quality Control Samples
Cis-1,2-dichlroethene was detected in non-quantifiable (“j-qualified”) levels in all blanks (EB, FB, TB). Since cis-
1,2-dichroloethene was not detected in any ground or surface water samples above regulatory Standards, any
potential field/lab induced artifact contamination is non-consequential.
Groundwater Samples
The only constituent detected in a groundwater sample above the 2L Standard (10 ug/L) was total chromium (17.3
ug/L) in upgradient background well MW-1.
Surface Water Samples
None of the surface water samples contained detections at levels in exceedance of an established 2B Standard.
2
Figures
Topographic Map with Site Location
01 1 MILE
FIGURE 1
Wayne County Landfill North Carolina (Dudley)
CLOSED MSW FACILITY
SUBTITLE D MSW
LANDFILL FACILITY
460 B South Landfill Rd
Dudley, NC 28333
Lat:35-17-19.1338
Long:-78-04-17.2971
Northing:561283.19
Easting:2277068.62
N
Tables
Wayne County Subtitle D Lined MSWLF Page 1 of 1
Table 1
Groundwater Monitoring Well Construction Table
February 11-12, 2015
Latitude Longitude
(inches)(ft)
MW-1 12/5/97 2 22.50 7.50 15 soil 164.51 161.95 151.08 13.43 35.2980417 78.0666750
MW-2 12/5/97 2 20.00 5.00 15 soil 147.27 144.63 138.02 9.25 35.2946417 78.0699806
MW-3 12/4/97 2 20.00 5.00 15 soil 141.13 136.40 133.82 7.31 35.2940694 78.0725889
MW-4 12/3/97 2 25.00 10.00 15 soil 139.80 137.80 124.61 15.19 35.2934694 78.0756444
MW-5 12/3/97 2 23.00 8.00 15 soil 140.15 137.35 124.66 15.49 35.2941972 78.0757333
MW-6 12/3/97 2 25.00 10.00 15 soil 146.58 144.42 130.75 15.83 35.2946000 78.0741306
MW-7 12/4/97 2 20.00 5.00 15 soil 135.89 133.57 130.04 5.85 35.2878278 78.0740694
MW-8 12/18/97 2 20.00 5.00 15 soil 135.25 132.79 128.05 7.2 35.2973056 78.0733889
MW-9 12/4/97 2 23.00 8.00 15 soil 141.31 139.13 130.47 10.84 35.2939444 78.0739453
MW-10 12/4/97 2 23.00 8.00 15 soil 141.43 139.19 129.20 12.23 35.2937472 78.0747222
MW-11 4/15/04 2 15.49 5.49 10 soil 134.76 131.76 130.89 3.87 35.2980861 78.0729639
MW-12 4/15/04 2 16.45 6.45 10 soil 135.19 132.19 131.69 3.5 35.2991889 78.0727111
MW-13 4/15/04 2 15.85 5.85 10 soil 149.89 146.89 142.15 7.74 35.2952722 78.0687417
MW-14 9/21/06 2 21.24 6.24 15 soil 137.51 134.68 131.24 6.27 35.2998500 78.0728806
MW-15 9/26/06 2 16.17 6.17 10 soil 131.74 129.01 129.44 2.3 35.3006028 78.0727778
MW-16R 6/4/13 2 22.00 7.00 15 Soil sand 160.39 157.39 146.38 14.01 35.2962278 78.0673861
P-5 1/11/96 2 19.00 11.00 8 soil 159.42 156.25 145.76 13.66 35.3002167 78.0688833
P3-15S 9/21/06 2 16.53 6.53 10 soil 152.23 149.14 143.16 9.07 35.3005639 78.0700639
Na = not available
Monitoring
Well
Date
Installed
Well Diameter
Total
Well
Depth
Top of Screen Depth Screen Length Geology of
Screened
Interval
Top of
Casing
Elevation
Ground Elevation Groundwater Elevation Depth to Water
(ft bgs)(ft bgs)(ft amsl)(ft amsl)(ft amsl)(ft btoc)
bgs = below ground surface
amsl= above mean sea level
btoc = below top of PVC well casing
Wayne County Subtitle D Lined MSWLF Page 1 of 1
Table 2
Field Observations of Monitoring Locations
February 11-12, 2015
Locked Comments
MW-1 Yes Yes Yes Yes Yes Yes
MW-2 Yes Yes Yes Yes Yes Yes
MW-3 Yes Yes Yes Yes Yes Yes See comments below
MW-4 Yes Yes Yes Yes Yes Yes
MW-5 Yes Yes Yes Yes Yes Yes
MW-6 Yes Yes Yes Yes Yes Yes
MW-7 Yes Yes Yes Yes Yes Yes Not re-painted yet
MW-8 Yes Yes Yes Yes Yes Yes
MW-9 Yes Yes Yes Yes Yes Yes
MW-10 Yes Yes Yes Yes Yes Yes
MW-11 Yes Yes Yes Yes Yes Yes
MW-12 Yes Yes Yes Yes Yes Yes
MW-13 Yes Yes Yes Yes Yes Yes
MW-14 Yes Yes Yes Yes Yes Yes Ph 3 well
MW-15 Yes Yes Yes Yes Yes Yes Ph 3 well
MW-16R Yes Yes Yes Yes Yes Yes Ph 3 well. Methane gas venting from PVC
LE-1 Yes -----Leachate lagoon sample
SW-1 Yes -----Shared Downstream of SW-3
SW-2 Yes -----Shared nearest lined MW-2
SW-3 Yes -----Shared downstream of SW-2
SW-3 No -----Shared Upstream furthest east Dry
SW-4 Yes -----Downstream of Ph 1 on Edward's Branch
SW-5 Yes -----More defined channel than events prior to August 2013.
Any unusual field conditions, observations, or events:
Phase 3 now in operation. Waste placed only on the east side of divide. Potential for leachate to migrate towards the west is unlikely.
Sample
Location
Viable
Monitoring
Location
Lack of Any
Evidence of
Tampering
Hinge/Hasp
Operational
Tagged
or
Labeled
Concrete
Surface Pad
Assumed
Effective
Purge water has sulphur “reducing odor”
Adjoiner west of Edwards Branch across from Ph 2 & 3 has cleared forest since 9/12. Adjoiner may potentially impact wetlands.
County replaced pad and case around MW-3 in August 2013. Riser extended 2.63' so top of casing now 141.13 ft amsl.
Wayne County Subtitle D Lined MSWLF Page 1 of 1
Table 3
Field Parameter Data Summary
February 11-12, 2015
Parameter Temp.ORP DO pH TDS Turbidity
Units C mg/L SU visual %/vol
MW-1 13.43 151.08 164.51 16.5 NR NR 5.01 20 10 Slight NR
MW-2 9.25 138.02 147.27 15.1 NR NR 5.79 420 200 Slight NR
MW-3 7.31 133.82 141.13 14.9 NR NR 5.38 20 10 Slight NR
MW-4 15.19 124.61 139.80 16.1 NR NR 4.86 10 0 Slight NR
MW-5 15.49 124.66 140.15 15.8 NR NR 5.03 0 0 Clear NR
MW-6 15.83 130.75 146.58 16.1 NR NR 4.93 0 0 Clear NR
MW-7 5.85 130.04 135.89 15.9 NR NR 6.02 190 80 Very NR
MW-8 7.20 128.05 135.25 15.7 NR NR 4.83 10 0 Clear NR
MW-9 10.84 130.47 141.31 15.4 NR NR 4.62 0 0 Slight NR
MW-10 12.23 129.20 141.43 16.1 NR NR 5.33 0 0 Slight NR
MW-11 3.87 130.89 134.76 15.2 NR NR 5.11 0 0 Clear NR
MW-12 3.50 131.69 135.19 14.7 NR NR 4.73 10 0 Clear NR
MW-13 7.74 142.15 149.89 14.9 NR NR 4.93 40 20 Clear NR
MW-14 6.27 131.24 137.51 15.8 NR NR 5.62 80 30 Clear NR
MW-15 2.30 129.44 131.74 15.9 NR NR 5.47 70 30 Clear NR
MW-16R 14.01 146.38 160.39 16.3 NR NR 5.31 0 0 Clear 48
Minimum 2.30 124.61 131.74 14.7 NR NR 4.62 0 0 Clear NR
Average 9.39 133.28 142.68 15.7 NR NR 5.19 54 24 Slight NR
Maximum 15.83 151.08 164.51 16.5 NR NR 6.02 420 200 Very 48
SW-1 ---8.1 NR NR 6.97 60 20 Clear NR
SW-2 ---7.7 NR NR 6.93 60 20 Clear NR
SW-3 ---7.9 NR NR 6.98 60 20 Clear NR
SW-4 ---8.7 NR NR 6.83 60 20 Clear NR
SW-5 ---9.1 NR NR 6.77 60 20 Clear NR
Minimum ---7.7 NR NR 6.77 60 20 Clear NR
Average ---8.3 NR NR 6.90 60 20 Clear NR
Maximum ---9.1 NR NR 6.98 60 20 Clear NR
NR = No Reading Attempted and not required
Depth to
Water
Water
Elevation
TOC
Elevation
Specific
Conductance
Methane Gas
in Well
Headspace
ft (btoc)ft (amsl)ft (amsl)mV цs/cm Ppb
Wayne County Subtitle D Lined MSWLF Page 1 of 1
Table 4
Sampling and Analysis Summary
February 11-12, 2015
Field Parameter Leachate
Re
a
s
o
n

N
o
t

S
a
m
p
l
e
d
VO
C
s

To
t
a
l

M
e
t
a
l
s

Te
m
p
e
r
a
t
u
r
e
Co
n
d
u
c
t
i
v
i
t
y
To
t
a
l

D
i
s
s
o
l
v
e
d

S
o
l
i
d
s

(
T
D
S
)
pH Tu
r
b
i
d
i
t
y
Su
l
f
a
t
e
pH Ph
o
s
p
h
o
r
u
s
BO
D
,

5

d
a
y
CO
D
Ni
t
r
a
t
e
La
b

E
P
A

8
2
6
0
B
L
a
b

E
P
A

6
0
0
0
/
7
0
0
0
Fi
e
l
d

M
e
t
e
r
Fi
e
l
d

M
e
t
e
r
Fi
e
l
d

M
e
t
e
r
Fi
e
l
d

M
e
t
e
r
Fi
e
l
d

V
i
s
u
a
l
La
b

E
P
A

3
0
0
.
0
La
b

E
P
A
9
0
4
0
La
b

E
P
A
3
6
5
.
1
La
b

S
M

5
2
1
0
B
La
b

S
M

5
2
2
0
D
La
b

E
P
A

3
5
3
.
2
MW-1 x x x x x x x
MW-2 x x x x x x x
MW-3 x x x x x x x
MW-4 x x x x x x x
MW-5 x x x x x x x
MW-6 x x x x x x x
MW-7 x x x x x x x
MW-8 x x x x x x x
MW-9 x x x x x x x
MW-10 x x x x x x x
MW-11 x x x x x x x
MW-12 x x x x x x x
MW-13 x x x x x x x
MW-14 x x x x x x x
MW-15 x x x x x x x
MW-16R x x x x x x x
SW-1 x x x x x x x
SW-2 x x x x x x x
SW-3 Dry
SW-3 x x x x x x x
SW-4 x x x x x x x
SW-5 x x x x x x x
LE-1 x x x x x x x x
EB x x
FB x x
TB x
Appendix I = List from current 40 CFR 258
App. I
Wayne County Subtitle D MSWLF, Phases 1-3 Page 1 of 1
Table 5
Detections in Water Samples above SWSL, GWP, 2L or 2B (Appendix I)
February 11-12, 2015
Sample ID Result Unit
MW-1 Chromium, total 2/12/15 17.3 2.5 10 10 100 N & B
MW-1 Cadmium, total 2/12/15 1.3 0.5 1 2 5
MW-1 Vanadium, total 2/12/15 34.2 2.5 25 NE 3.5 NE
MW-1 Zinc, total 2/12/15 13.1 5 10 1000 5000
MW-2 Vanadium, total 2/12/15 4.3,j 2.5 25 NE 3.5 NE
MW-2 Thallium, total 2/12/15 7.2 5 5.5 NE 0.28 2
MW-2 Selenium, total 2/12/15 5.9,j 5 10 20 50
MW-3 Thallium, total 2/11/15 5.3,j 5 5.5 NE 0.28 2
MW-3 Cadmium, total 2/11/15 1.1 0.5 1 2 5
MW-5 Cadmium, total 2/12/15 1.2 0.5 1 2 5
MW-8 Vanadium, total 2/11/15 7.5,j 2.5 25 NE 3.5 NE
MW-8 Zinc, total 2/11/15 16.9 5 10 1000 5000
MW-9 Vanadium, total 2/11/15 3.8,j 2.5 25 NE 3.5 NE
MW-10 Cadmium, total 2/11/15 1.5 0.5 1 2 5
MW-12 Barium, total 2/11/15 144 2.5 100 700 2000
MW-12 Zinc, total 2/11/15 14.7 5 10 1000 5000
MW-12 Cobalt, total 2/11/15 61.6 2.5 10 NE 70 NE
MW-13 Zinc, total 2/11/15 41.2 5 10 1000 5000
MW-15 Zinc, total 2/11/15 10.2 5 10 1000 5000
SW-4 Zinc, total 2/11/15 15 5 10 50 5000
SW-5 Barium, total 2/11/15 320 2.5 100 200000 2000
SW-5 Zinc, total 2/11/15 18 5 10 50 5000
A definitive source of the detection was not determined as part of this report. Preliminary cause only listed pursuant to instructions
j =The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL),
adjusted for actual sample preparation data and moisture content, where applicable
B = Background as detected upgradient/upstream of facility
N = Natural originating from erosion of natural deposits. Source not anthropogenic.
BOLD = Concentration > 2L, 2B or MCL Standard
Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 Preliminary
Cause 8
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1 Table contains constituents detected at or above SWSL, GWP, 2L, or 2B
5 2B = North Carolina 15 NCAC 2B Surface Water Quality Standard for this Specific Stream Classification
6 GWP = Groundwater Protection Standard
7 MCL = Primary Drinking Water Standard (not currently applicable for regulatory comparisons)
8 Preliminary Cause = Refers to a preliminary analysis of the cause and/or source of a detection over the respective 2L/2B Standard.
Wayne County Subtitle D MSWLF Page 1 of 1
Table 6
Detections in Leachate Sample Above SWSL, GWP, 2L, 2B or MCL
February 12, 2015
Sample ID Result Unit
LE-1 2/12/15 0.41, j 0.12 1 0.4 37 5 1841
LE-1 2/12/15 1.4 0.3 1 550 NE 700 274
LE-1 Benzene 2/12/15 9.8 0.25 1 1 51 5 221
LE-1 Xylene (Total)2/12/15 18.2 0.66 5 530 670 10000 141
LE-1 Vanadium, total 2/12/15 4.2, j 2.5 25 NE NE 3.5 NE 17.9
LE-1 Antimony, total 2/12/15 7.5 3.8 6 NE 1.4 6 4520
LE-1 Barium, total 2/12/15 195 2.5 100 700 2000 2000 850
LE-1 BOD, 5 day 2/12/15 148000 2000 NE 3837000
LE-1 COD 2/12/15 1070000 12500 NE NE 4773000
adjusted for actual sample preparation data and moisture content, where applicable.
NE = Not Established
BOLD = Concentration > “Average Leachate”, 2L, 2B or MCL Standard
Parameter Name 1 Sample
Date MDL 2 SWSL 3 2L 4 2B 5 GWP 6 MCL 7 “Average
Leachate” 8
1,2-Dichloroethane ug/L
Ethylbenzene ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1 Table contains only constituents detected at or above SWSL, GWP, 2L, or 2B
2 MDL = Method Detection Limit
3 SWSL = Solid Waste Section Reporting Limit (Current as of Sampling Event)
4 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard (Current as of Sampling Event)
5 2B = North Carolina 15 NCAC 2B Surface Water Quality Standard for this Specific Stream Classification (Current as of Sampling Event)
6 GWP = Groundwater Protection Standard (Current as of Sampling Event)
7 MCL = Primary Drinking Water Standard (not currently applicable for regulatory comparisons)
8 Average concentration of leachate from a comparable “Dry Tomb” Landfill published in 1988 by EPA document Summary of Data on MSWLF Leachate Characteristics
J =The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL),
Wayne County Subtitle D Lined MSWLF Page 1 of 1
Table 7
February 11-12, 2015
Flow Rate
(cm/sec)(%)(ft/ft)(ft/yr)
MW-1 3.21E-04 31 0.0086 9 S80W 13.43 151.08
MW-2 1.37E-03 31 0.0100 46 S56W 9.25 138.02
MW-3 9.72E-04 31 0.0385 125 S89W 7.31 131.19
MW-4 2.33E-04 9 0.0128 34 S62W 15.19 124.61
MW-5 1.45E-04 9 0.0120 20 N81W 15.49 124.66
MW-6 8.38E-05 31 0.0147 4 N82W 15.83 130.75
MW-7 6.84E-05 9 0.0100 8 N83W 5.85 130.04
MW-8 1.68E-04 9 0.0214 41 S80W 7.20 128.05
MW-9 6.37E-04 31 0.0064 14 S43W 10.84 130.47
MW-10 4.74E-04 31 0.0308 49 S43W 12.23 129.2
MW-11 1.46E-04 22 0.0156 11 N89W 3.87 130.89
MW-12 1.63E-04 22 0.0115 9 N90W 3.50 131.69
MW-13 2.14E-03 22 0.0075 75 S32W 7.74 142.15
MW-14 2.63E-04 22 0.0088 11 N81W 6.27 131.24
MW-15 1.82E-05 22 0.0183 2 N65W 2.30 129.44
MW-16R 22 0.0386 S52W 14.01 146.38
Minimum 1.82E-05 9 0.0064 2 -2.30 124.61
Average 4.80E-04 22 0.0166 30 -9.39 133.12
Maximum 2.14E-03 31 0.0386 125 -15.83 151.08
NOTE:
Hydraulic Conductivity values from slug tests performed on each monitoring well.
where
Hydrologic Properties at Monitoring Well Locations
Monitoring
Well
Hydraulic
Conductivity
Effective
Porosity
Hydraulic
Gradient
Flow
Direction
Depth to
Groundwater
Groundwater
Potentiometric
Elevation
(ft btoc)(ft amsl)
na na
Effective porosity values from Design Hydrogeologic Studies for Wayne County.
Hydrologic gradient calculated from groundwater elevations recorded on February 11-12, 2015.
Average Linear Velocity rate (Q) is defined by modified Darcy's equation:
K= hydraulic conductivity
ne= effective porosity
dh= head difference
dl= horizontal distance
Q=−K
ne
⋅dh
dl
Appendix A
Laboratory Analysis Reports
Chains of Custody
#=CL#
February 27, 2015
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92237757
92237757
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
Wayne Lined MSWLF
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on February 13, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 68
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 68
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Lab ID Sample ID Matrix Date Collected Date Received
92237757001 MW-1 Water 02/12/15 09:25 02/13/15 15:45
92237757002 MW-2 Water 02/12/15 09:00 02/13/15 15:45
92237757003 MW-3 Water 02/11/15 10:35 02/13/15 15:45
92237757004 MW-4 Water 02/11/15 11:00 02/13/15 15:45
92237757005 MW-5 Water 02/11/15 13:55 02/13/15 15:45
92237757006 MW-6 Water 02/11/15 14:30 02/13/15 15:45
92237757007 MW-7 Water 02/11/15 15:40 02/13/15 15:45
92237757008 MW-8 Water 02/11/15 11:30 02/13/15 15:45
92237757009 MW-9 Water 02/11/15 13:30 02/13/15 15:45
92237757010 MW-10 Water 02/11/15 13:15 02/13/15 15:45
92237757011 MW-11 Water 02/11/15 12:05 02/13/15 15:45
92237757012 MW-12 Water 02/11/15 11:50 02/13/15 15:45
92237757013 MW-13 Water 02/11/15 08:35 02/13/15 15:45
92237757014 MW-14 Water 02/11/15 09:20 02/13/15 15:45
92237757015 MW-15 Water 02/11/15 09:05 02/13/15 15:45
92237757016 MW-16R Water 02/12/15 09:50 02/13/15 15:45
92237757017 SW-4 Water 02/11/15 08:30 02/13/15 15:45
92237757018 SW-5 Water 02/11/15 08:50 02/13/15 15:45
92237757019 LE-1 Water 02/12/15 17:00 02/13/15 15:45
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 68
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92237757001 MW-1 EPA 6010 15 PASI-ASH1
EPA 8260 51 PASI-CGAW
92237757002 MW-2 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 51 PASI-CGAW
92237757003 MW-3 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 51 PASI-CGAW
92237757004 MW-4 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 51 PASI-CGAW
92237757005 MW-5 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 51 PASI-CGAW
92237757006 MW-6 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 51 PASI-CGAW
92237757007 MW-7 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 51 PASI-CGAW
92237757008 MW-8 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 51 PASI-CGAW
92237757009 MW-9 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 51 PASI-CSNP
92237757010 MW-10 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 51 PASI-CSNP
92237757011 MW-11 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 51 PASI-CSNP
92237757012 MW-12 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 51 PASI-CSNP
92237757013 MW-13 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 51 PASI-CSNP
92237757014 MW-14 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 51 PASI-CSNP
92237757015 MW-15 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 51 PASI-CSNP
92237757016 MW-16R EPA 6010 15 PASI-AJMW, SH1
EPA 8260 51 PASI-CSNP
92237757017 SW-4 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 51 PASI-CSNP
92237757018 SW-5 EPA 6010 15 PASI-AJMW, SH1
EPA 8260 51 PASI-CSNP
92237757019 LE-1 EPA 6010 15 PASI-AJMW, SH1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 68
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8260 51 PASI-CSNP
SM 5210B 1 PASI-ASER
EPA 9040 1 PASI-AMLS
EPA 300.0 1 PASI-AAES2
EPA 353.2 1 PASI-ADMN
EPA 365.1 1 PASI-AJDA
SM 5220D 1 PASI-AMAB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:MW-1 Lab ID:92237757001 Collected:02/12/15 09:25 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 00:55 7440-36-002/16/15 16:106.0 3.8 1
Arsenic 6.6J ug/L 02/19/15 00:55 7440-38-202/16/15 16:1010.0 2.5 1
Barium 36.3J ug/L 02/19/15 00:55 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 00:55 7440-41-702/16/15 16:101.0 0.50 1
Cadmium 1.3 ug/L 02/19/15 00:55 7440-43-902/16/15 16:101.0 0.50 1
Chromium 17.3 ug/L 02/19/15 00:55 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/19/15 00:55 7440-48-402/16/15 16:1010.0 2.5 1
Copper 4.6J ug/L 02/19/15 00:55 7440-50-802/16/15 16:1010.0 2.5 1
Lead 5.3J ug/L 02/19/15 00:55 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/19/15 00:55 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 00:55 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 00:55 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/19/15 00:55 7440-28-002/16/15 16:105.5 5.0 1
Vanadium 34.2 ug/L 02/19/15 00:55 7440-62-202/16/15 16:1025.0 2.5 1
Zinc 13.1 ug/L 02/19/15 00:55 7440-66-602/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/25/15 18:59 67-64-110010.0 1
Acrylonitrile ND ug/L 02/25/15 18:59 107-13-12001.9 1
Benzene ND ug/L 02/25/15 18:59 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/25/15 18:59 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/25/15 18:59 75-27-41.0 0.18 1
Bromoform ND ug/L 02/25/15 18:59 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/25/15 18:59 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/25/15 18:59 78-93-31000.96 1
Carbon disulfide ND ug/L 02/25/15 18:59 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/25/15 18:59 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/25/15 18:59 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/25/15 18:59 75-00-310.0 0.54 1
Chloroform ND ug/L 02/25/15 18:59 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/25/15 18:59 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/25/15 18:59 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/25/15 18:59 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/25/15 18:59 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/25/15 18:59 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/25/15 18:59 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/25/15 18:59 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/25/15 18:59 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/25/15 18:59 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/25/15 18:59 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/25/15 18:59 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/25/15 18:59 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/25/15 18:59 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/25/15 18:59 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/25/15 18:59 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/25/15 18:59 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:MW-1 Lab ID:92237757001 Collected:02/12/15 09:25 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/25/15 18:59 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/25/15 18:59 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/25/15 18:59 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/25/15 18:59 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/25/15 18:59 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/25/15 18:59 108-10-11000.33 1
Styrene ND ug/L 02/25/15 18:59 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/25/15 18:59 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/25/15 18:59 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/25/15 18:59 127-18-41.0 0.46 1
Toluene ND ug/L 02/25/15 18:59 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/25/15 18:59 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/25/15 18:59 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/25/15 18:59 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/25/15 18:59 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/25/15 18:59 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/25/15 18:59 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/25/15 18:59 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/25/15 18:59 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %02/25/15 18:59 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %02/25/15 18:59 17060-07-070-130 1
Toluene-d8 (S)94 %02/25/15 18:59 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:MW-2 Lab ID:92237757002 Collected:02/12/15 09:00 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 01:17 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/19/15 01:17 7440-38-202/16/15 16:1010.0 2.5 1
Barium 14.0J ug/L 02/19/15 01:17 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 01:17 7440-41-702/16/15 16:101.0 0.50 1
Cadmium 0.63J ug/L 02/19/15 01:17 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/19/15 01:17 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/19/15 01:17 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/19/15 01:17 7440-50-802/16/15 16:1010.0 2.5 1
Lead 6.6J ug/L 02/19/15 01:17 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/19/15 01:17 7440-02-002/16/15 16:1050.0 2.5 1
Selenium 5.9J ug/L 02/19/15 01:17 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 01:17 7440-22-402/16/15 16:1010.0 2.5 1
Thallium 7.2 ug/L 02/19/15 01:17 7440-28-002/16/15 16:105.5 5.0 1
Vanadium 4.3J ug/L 02/19/15 01:17 7440-62-202/16/15 16:1025.0 2.5 1
Zinc ND ug/L 02/25/15 13:48 7440-66-602/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/25/15 19:16 67-64-110010.0 1
Acrylonitrile ND ug/L 02/25/15 19:16 107-13-12001.9 1
Benzene ND ug/L 02/25/15 19:16 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/25/15 19:16 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/25/15 19:16 75-27-41.0 0.18 1
Bromoform ND ug/L 02/25/15 19:16 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/25/15 19:16 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/25/15 19:16 78-93-31000.96 1
Carbon disulfide ND ug/L 02/25/15 19:16 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/25/15 19:16 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/25/15 19:16 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/25/15 19:16 75-00-310.0 0.54 1
Chloroform ND ug/L 02/25/15 19:16 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/25/15 19:16 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/25/15 19:16 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/25/15 19:16 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/25/15 19:16 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/25/15 19:16 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/25/15 19:16 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/25/15 19:16 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/25/15 19:16 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/25/15 19:16 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/25/15 19:16 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/25/15 19:16 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/25/15 19:16 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/25/15 19:16 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/25/15 19:16 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/25/15 19:16 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/25/15 19:16 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:MW-2 Lab ID:92237757002 Collected:02/12/15 09:00 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/25/15 19:16 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/25/15 19:16 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/25/15 19:16 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/25/15 19:16 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/25/15 19:16 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/25/15 19:16 108-10-11000.33 1
Styrene ND ug/L 02/25/15 19:16 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/25/15 19:16 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/25/15 19:16 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/25/15 19:16 127-18-41.0 0.46 1
Toluene ND ug/L 02/25/15 19:16 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/25/15 19:16 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/25/15 19:16 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/25/15 19:16 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/25/15 19:16 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/25/15 19:16 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/25/15 19:16 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/25/15 19:16 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/25/15 19:16 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)101 %02/25/15 19:16 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %02/25/15 19:16 17060-07-070-130 1
Toluene-d8 (S)95 %02/25/15 19:16 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:MW-3 Lab ID:92237757003 Collected:02/11/15 10:35 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 01:26 7440-36-002/16/15 16:106.0 3.8 1
Arsenic 6.9J ug/L 02/19/15 01:26 7440-38-202/16/15 16:1010.0 2.5 1
Barium 23.4J ug/L 02/19/15 01:26 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 01:26 7440-41-702/16/15 16:101.0 0.50 1
Cadmium 1.1 ug/L 02/19/15 01:26 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/19/15 01:26 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/19/15 01:26 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/19/15 01:26 7440-50-802/16/15 16:1010.0 2.5 1
Lead 3.0J ug/L 02/19/15 01:26 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/19/15 01:26 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 01:26 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 01:26 7440-22-402/16/15 16:1010.0 2.5 1
Thallium 5.3J ug/L 02/19/15 01:26 7440-28-002/16/15 16:105.5 5.0 1
Vanadium ND ug/L 02/19/15 01:26 7440-62-202/16/15 16:1025.0 2.5 1
Zinc 5.7J ug/L 02/25/15 13:56 7440-66-6 B02/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/25/15 19:33 67-64-110010.0 1
Acrylonitrile ND ug/L 02/25/15 19:33 107-13-12001.9 1
Benzene ND ug/L 02/25/15 19:33 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/25/15 19:33 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/25/15 19:33 75-27-41.0 0.18 1
Bromoform ND ug/L 02/25/15 19:33 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/25/15 19:33 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/25/15 19:33 78-93-31000.96 1
Carbon disulfide ND ug/L 02/25/15 19:33 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/25/15 19:33 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/25/15 19:33 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/25/15 19:33 75-00-310.0 0.54 1
Chloroform ND ug/L 02/25/15 19:33 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/25/15 19:33 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/25/15 19:33 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/25/15 19:33 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/25/15 19:33 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/25/15 19:33 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/25/15 19:33 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/25/15 19:33 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/25/15 19:33 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/25/15 19:33 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/25/15 19:33 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/25/15 19:33 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/25/15 19:33 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/25/15 19:33 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/25/15 19:33 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/25/15 19:33 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/25/15 19:33 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:MW-3 Lab ID:92237757003 Collected:02/11/15 10:35 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/25/15 19:33 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/25/15 19:33 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/25/15 19:33 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/25/15 19:33 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/25/15 19:33 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/25/15 19:33 108-10-11000.33 1
Styrene ND ug/L 02/25/15 19:33 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/25/15 19:33 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/25/15 19:33 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/25/15 19:33 127-18-41.0 0.46 1
Toluene ND ug/L 02/25/15 19:33 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/25/15 19:33 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/25/15 19:33 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/25/15 19:33 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/25/15 19:33 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/25/15 19:33 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/25/15 19:33 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/25/15 19:33 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/25/15 19:33 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %02/25/15 19:33 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %02/25/15 19:33 17060-07-070-130 1
Toluene-d8 (S)95 %02/25/15 19:33 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:MW-4 Lab ID:92237757004 Collected:02/11/15 11:00 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 01:29 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/19/15 01:29 7440-38-202/16/15 16:1010.0 2.5 1
Barium 32.3J ug/L 02/19/15 01:29 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 01:29 7440-41-702/16/15 16:101.0 0.50 1
Cadmium ND ug/L 02/19/15 01:29 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/19/15 01:29 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/19/15 01:29 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/19/15 01:29 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/19/15 01:29 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/19/15 01:29 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 01:29 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 01:29 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/19/15 01:29 7440-28-002/16/15 16:105.5 5.0 1
Vanadium ND ug/L 02/19/15 01:29 7440-62-202/16/15 16:1025.0 2.5 1
Zinc ND ug/L 02/25/15 13:59 7440-66-602/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/25/15 19:50 67-64-110010.0 1
Acrylonitrile ND ug/L 02/25/15 19:50 107-13-12001.9 1
Benzene ND ug/L 02/25/15 19:50 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/25/15 19:50 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/25/15 19:50 75-27-41.0 0.18 1
Bromoform ND ug/L 02/25/15 19:50 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/25/15 19:50 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/25/15 19:50 78-93-31000.96 1
Carbon disulfide ND ug/L 02/25/15 19:50 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/25/15 19:50 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/25/15 19:50 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/25/15 19:50 75-00-310.0 0.54 1
Chloroform ND ug/L 02/25/15 19:50 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/25/15 19:50 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/25/15 19:50 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/25/15 19:50 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/25/15 19:50 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/25/15 19:50 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/25/15 19:50 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/25/15 19:50 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/25/15 19:50 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/25/15 19:50 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/25/15 19:50 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/25/15 19:50 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/25/15 19:50 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/25/15 19:50 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/25/15 19:50 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/25/15 19:50 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/25/15 19:50 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:MW-4 Lab ID:92237757004 Collected:02/11/15 11:00 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/25/15 19:50 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/25/15 19:50 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/25/15 19:50 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/25/15 19:50 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/25/15 19:50 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/25/15 19:50 108-10-11000.33 1
Styrene ND ug/L 02/25/15 19:50 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/25/15 19:50 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/25/15 19:50 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/25/15 19:50 127-18-41.0 0.46 1
Toluene ND ug/L 02/25/15 19:50 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/25/15 19:50 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/25/15 19:50 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/25/15 19:50 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/25/15 19:50 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/25/15 19:50 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/25/15 19:50 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/25/15 19:50 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/25/15 19:50 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %02/25/15 19:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %02/25/15 19:50 17060-07-070-130 1
Toluene-d8 (S)93 %02/25/15 19:50 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:MW-5 Lab ID:92237757005 Collected:02/11/15 13:55 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 01:32 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/19/15 01:32 7440-38-202/16/15 16:1010.0 2.5 1
Barium 39.7J ug/L 02/19/15 01:32 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 01:32 7440-41-702/16/15 16:101.0 0.50 1
Cadmium 0.95J ug/L 02/19/15 01:32 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/19/15 01:32 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/19/15 01:32 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/19/15 01:32 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/19/15 01:32 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/19/15 01:32 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 01:32 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 01:32 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/19/15 01:32 7440-28-002/16/15 16:105.5 5.0 1
Vanadium ND ug/L 02/19/15 01:32 7440-62-202/16/15 16:1025.0 2.5 1
Zinc 5.5J ug/L 02/25/15 14:03 7440-66-6 B02/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/25/15 20:07 67-64-110010.0 1
Acrylonitrile ND ug/L 02/25/15 20:07 107-13-12001.9 1
Benzene ND ug/L 02/25/15 20:07 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/25/15 20:07 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/25/15 20:07 75-27-41.0 0.18 1
Bromoform ND ug/L 02/25/15 20:07 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/25/15 20:07 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/25/15 20:07 78-93-31000.96 1
Carbon disulfide ND ug/L 02/25/15 20:07 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/25/15 20:07 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/25/15 20:07 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/25/15 20:07 75-00-310.0 0.54 1
Chloroform ND ug/L 02/25/15 20:07 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/25/15 20:07 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/25/15 20:07 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/25/15 20:07 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/25/15 20:07 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/25/15 20:07 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/25/15 20:07 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/25/15 20:07 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/25/15 20:07 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/25/15 20:07 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/25/15 20:07 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/25/15 20:07 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/25/15 20:07 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/25/15 20:07 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/25/15 20:07 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/25/15 20:07 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/25/15 20:07 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:MW-5 Lab ID:92237757005 Collected:02/11/15 13:55 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/25/15 20:07 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/25/15 20:07 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/25/15 20:07 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/25/15 20:07 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/25/15 20:07 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/25/15 20:07 108-10-11000.33 1
Styrene ND ug/L 02/25/15 20:07 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/25/15 20:07 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/25/15 20:07 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/25/15 20:07 127-18-41.0 0.46 1
Toluene ND ug/L 02/25/15 20:07 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/25/15 20:07 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/25/15 20:07 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/25/15 20:07 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/25/15 20:07 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/25/15 20:07 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/25/15 20:07 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/25/15 20:07 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/25/15 20:07 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)102 %02/25/15 20:07 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %02/25/15 20:07 17060-07-070-130 1
Toluene-d8 (S)94 %02/25/15 20:07 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:MW-6 Lab ID:92237757006 Collected:02/11/15 14:30 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 01:35 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/19/15 01:35 7440-38-202/16/15 16:1010.0 2.5 1
Barium 48.2J ug/L 02/19/15 01:35 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 01:35 7440-41-702/16/15 16:101.0 0.50 1
Cadmium 0.51J ug/L 02/19/15 01:35 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/19/15 01:35 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/19/15 01:35 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/19/15 01:35 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/19/15 01:35 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/19/15 01:35 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 01:35 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 01:35 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/19/15 01:35 7440-28-002/16/15 16:105.5 5.0 1
Vanadium ND ug/L 02/19/15 01:35 7440-62-202/16/15 16:1025.0 2.5 1
Zinc ND ug/L 02/25/15 14:06 7440-66-602/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/25/15 20:24 67-64-110010.0 1
Acrylonitrile ND ug/L 02/25/15 20:24 107-13-12001.9 1
Benzene ND ug/L 02/25/15 20:24 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/25/15 20:24 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/25/15 20:24 75-27-41.0 0.18 1
Bromoform ND ug/L 02/25/15 20:24 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/25/15 20:24 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/25/15 20:24 78-93-31000.96 1
Carbon disulfide ND ug/L 02/25/15 20:24 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/25/15 20:24 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/25/15 20:24 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/25/15 20:24 75-00-310.0 0.54 1
Chloroform ND ug/L 02/25/15 20:24 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/25/15 20:24 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/25/15 20:24 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/25/15 20:24 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/25/15 20:24 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/25/15 20:24 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/25/15 20:24 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/25/15 20:24 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/25/15 20:24 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/25/15 20:24 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/25/15 20:24 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/25/15 20:24 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/25/15 20:24 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/25/15 20:24 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/25/15 20:24 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/25/15 20:24 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/25/15 20:24 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:MW-6 Lab ID:92237757006 Collected:02/11/15 14:30 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/25/15 20:24 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/25/15 20:24 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/25/15 20:24 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/25/15 20:24 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/25/15 20:24 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/25/15 20:24 108-10-11000.33 1
Styrene ND ug/L 02/25/15 20:24 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/25/15 20:24 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/25/15 20:24 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/25/15 20:24 127-18-41.0 0.46 1
Toluene ND ug/L 02/25/15 20:24 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/25/15 20:24 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/25/15 20:24 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/25/15 20:24 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/25/15 20:24 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/25/15 20:24 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/25/15 20:24 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/25/15 20:24 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/25/15 20:24 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %02/25/15 20:24 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %02/25/15 20:24 17060-07-070-130 1
Toluene-d8 (S)95 %02/25/15 20:24 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:MW-7 Lab ID:92237757007 Collected:02/11/15 15:40 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 01:47 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/19/15 01:47 7440-38-202/16/15 16:1010.0 2.5 1
Barium 23.9J ug/L 02/19/15 01:47 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 01:47 7440-41-702/16/15 16:101.0 0.50 1
Cadmium ND ug/L 02/19/15 01:47 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/19/15 01:47 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/19/15 01:47 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/19/15 01:47 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/19/15 01:47 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/19/15 01:47 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 01:47 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 01:47 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/19/15 01:47 7440-28-002/16/15 16:105.5 5.0 1
Vanadium ND ug/L 02/19/15 01:47 7440-62-202/16/15 16:1025.0 2.5 1
Zinc 5.2J ug/L 02/25/15 14:09 7440-66-6 B02/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/25/15 20:40 67-64-110010.0 1
Acrylonitrile ND ug/L 02/25/15 20:40 107-13-12001.9 1
Benzene ND ug/L 02/25/15 20:40 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/25/15 20:40 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/25/15 20:40 75-27-41.0 0.18 1
Bromoform ND ug/L 02/25/15 20:40 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/25/15 20:40 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/25/15 20:40 78-93-31000.96 1
Carbon disulfide ND ug/L 02/25/15 20:40 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/25/15 20:40 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/25/15 20:40 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/25/15 20:40 75-00-310.0 0.54 1
Chloroform ND ug/L 02/25/15 20:40 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/25/15 20:40 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/25/15 20:40 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/25/15 20:40 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/25/15 20:40 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/25/15 20:40 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/25/15 20:40 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/25/15 20:40 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/25/15 20:40 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/25/15 20:40 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/25/15 20:40 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/25/15 20:40 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/25/15 20:40 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/25/15 20:40 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/25/15 20:40 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/25/15 20:40 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/25/15 20:40 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:MW-7 Lab ID:92237757007 Collected:02/11/15 15:40 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/25/15 20:40 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/25/15 20:40 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/25/15 20:40 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/25/15 20:40 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/25/15 20:40 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/25/15 20:40 108-10-11000.33 1
Styrene ND ug/L 02/25/15 20:40 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/25/15 20:40 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/25/15 20:40 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/25/15 20:40 127-18-41.0 0.46 1
Toluene ND ug/L 02/25/15 20:40 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/25/15 20:40 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/25/15 20:40 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/25/15 20:40 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/25/15 20:40 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/25/15 20:40 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/25/15 20:40 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/25/15 20:40 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/25/15 20:40 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %02/25/15 20:40 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %02/25/15 20:40 17060-07-070-130 1
Toluene-d8 (S)96 %02/25/15 20:40 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:MW-8 Lab ID:92237757008 Collected:02/11/15 11:30 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 01:50 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/19/15 01:50 7440-38-202/16/15 16:1010.0 2.5 1
Barium 21.5J ug/L 02/19/15 01:50 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 01:50 7440-41-702/16/15 16:101.0 0.50 1
Cadmium ND ug/L 02/19/15 01:50 7440-43-902/16/15 16:101.0 0.50 1
Chromium 3.8J ug/L 02/19/15 01:50 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/19/15 01:50 7440-48-402/16/15 16:1010.0 2.5 1
Copper 2.7J ug/L 02/19/15 01:50 7440-50-802/16/15 16:1010.0 2.5 1
Lead 4.0J ug/L 02/19/15 01:50 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/19/15 01:50 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 01:50 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 01:50 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/19/15 01:50 7440-28-002/16/15 16:105.5 5.0 1
Vanadium 7.5J ug/L 02/19/15 01:50 7440-62-202/16/15 16:1025.0 2.5 1
Zinc 16.9 ug/L 02/25/15 14:12 7440-66-6 B02/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/25/15 20:57 67-64-110010.0 1
Acrylonitrile ND ug/L 02/25/15 20:57 107-13-12001.9 1
Benzene ND ug/L 02/25/15 20:57 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/25/15 20:57 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/25/15 20:57 75-27-41.0 0.18 1
Bromoform ND ug/L 02/25/15 20:57 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/25/15 20:57 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/25/15 20:57 78-93-31000.96 1
Carbon disulfide ND ug/L 02/25/15 20:57 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/25/15 20:57 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/25/15 20:57 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/25/15 20:57 75-00-310.0 0.54 1
Chloroform ND ug/L 02/25/15 20:57 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/25/15 20:57 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/25/15 20:57 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/25/15 20:57 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/25/15 20:57 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/25/15 20:57 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/25/15 20:57 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/25/15 20:57 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/25/15 20:57 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/25/15 20:57 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/25/15 20:57 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/25/15 20:57 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/25/15 20:57 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/25/15 20:57 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/25/15 20:57 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/25/15 20:57 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/25/15 20:57 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:MW-8 Lab ID:92237757008 Collected:02/11/15 11:30 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/25/15 20:57 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/25/15 20:57 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/25/15 20:57 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/25/15 20:57 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/25/15 20:57 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/25/15 20:57 108-10-11000.33 1
Styrene ND ug/L 02/25/15 20:57 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/25/15 20:57 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/25/15 20:57 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/25/15 20:57 127-18-41.0 0.46 1
Toluene ND ug/L 02/25/15 20:57 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/25/15 20:57 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/25/15 20:57 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/25/15 20:57 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/25/15 20:57 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/25/15 20:57 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/25/15 20:57 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/25/15 20:57 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/25/15 20:57 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)100 %02/25/15 20:57 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %02/25/15 20:57 17060-07-070-130 1
Toluene-d8 (S)94 %02/25/15 20:57 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:MW-9 Lab ID:92237757009 Collected:02/11/15 13:30 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 01:54 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/19/15 01:54 7440-38-202/16/15 16:1010.0 2.5 1
Barium 65.6J ug/L 02/19/15 01:54 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 01:54 7440-41-702/16/15 16:101.0 0.50 1
Cadmium ND ug/L 02/19/15 01:54 7440-43-902/16/15 16:101.0 0.50 1
Chromium 3.8J ug/L 02/19/15 01:54 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/19/15 01:54 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/19/15 01:54 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/19/15 01:54 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/19/15 01:54 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 01:54 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 01:54 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/19/15 01:54 7440-28-002/16/15 16:105.5 5.0 1
Vanadium 3.8J ug/L 02/19/15 01:54 7440-62-202/16/15 16:1025.0 2.5 1
Zinc ND ug/L 02/25/15 14:24 7440-66-602/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/25/15 19:07 67-64-110010.0 1
Acrylonitrile ND ug/L 02/25/15 19:07 107-13-12001.9 1
Benzene ND ug/L 02/25/15 19:07 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/25/15 19:07 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/25/15 19:07 75-27-41.0 0.18 1
Bromoform ND ug/L 02/25/15 19:07 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/25/15 19:07 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/25/15 19:07 78-93-31000.96 1
Carbon disulfide ND ug/L 02/25/15 19:07 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/25/15 19:07 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/25/15 19:07 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/25/15 19:07 75-00-310.0 0.54 1
Chloroform ND ug/L 02/25/15 19:07 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/25/15 19:07 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/25/15 19:07 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/25/15 19:07 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/25/15 19:07 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/25/15 19:07 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/25/15 19:07 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/25/15 19:07 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/25/15 19:07 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/25/15 19:07 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/25/15 19:07 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/25/15 19:07 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/25/15 19:07 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/25/15 19:07 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/25/15 19:07 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/25/15 19:07 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/25/15 19:07 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:MW-9 Lab ID:92237757009 Collected:02/11/15 13:30 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/25/15 19:07 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/25/15 19:07 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/25/15 19:07 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/25/15 19:07 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/25/15 19:07 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/25/15 19:07 108-10-11000.33 1
Styrene ND ug/L 02/25/15 19:07 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/25/15 19:07 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/25/15 19:07 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/25/15 19:07 127-18-41.0 0.46 1
Toluene ND ug/L 02/25/15 19:07 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/25/15 19:07 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/25/15 19:07 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/25/15 19:07 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/25/15 19:07 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/25/15 19:07 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/25/15 19:07 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/25/15 19:07 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/25/15 19:07 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)106 %02/25/15 19:07 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %02/25/15 19:07 17060-07-070-130 1
Toluene-d8 (S)98 %02/25/15 19:07 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:MW-10 Lab ID:92237757010 Collected:02/11/15 13:15 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 01:57 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/19/15 01:57 7440-38-202/16/15 16:1010.0 2.5 1
Barium 40.5J ug/L 02/19/15 01:57 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 01:57 7440-41-702/16/15 16:101.0 0.50 1
Cadmium 1.5 ug/L 02/19/15 01:57 7440-43-902/16/15 16:101.0 0.50 1
Chromium 2.5J ug/L 02/19/15 01:57 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/19/15 01:57 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/19/15 01:57 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/19/15 01:57 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/19/15 01:57 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 01:57 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 01:57 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/19/15 01:57 7440-28-002/16/15 16:105.5 5.0 1
Vanadium 2.8J ug/L 02/19/15 01:57 7440-62-202/16/15 16:1025.0 2.5 1
Zinc 5.9J ug/L 02/25/15 14:28 7440-66-6 B02/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/25/15 19:24 67-64-110010.0 1
Acrylonitrile ND ug/L 02/25/15 19:24 107-13-12001.9 1
Benzene ND ug/L 02/25/15 19:24 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/25/15 19:24 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/25/15 19:24 75-27-41.0 0.18 1
Bromoform ND ug/L 02/25/15 19:24 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/25/15 19:24 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/25/15 19:24 78-93-31000.96 1
Carbon disulfide ND ug/L 02/25/15 19:24 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/25/15 19:24 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/25/15 19:24 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/25/15 19:24 75-00-310.0 0.54 1
Chloroform ND ug/L 02/25/15 19:24 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/25/15 19:24 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/25/15 19:24 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/25/15 19:24 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/25/15 19:24 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/25/15 19:24 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/25/15 19:24 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/25/15 19:24 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/25/15 19:24 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/25/15 19:24 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/25/15 19:24 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/25/15 19:24 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/25/15 19:24 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/25/15 19:24 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/25/15 19:24 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/25/15 19:24 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/25/15 19:24 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:MW-10 Lab ID:92237757010 Collected:02/11/15 13:15 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/25/15 19:24 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/25/15 19:24 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/25/15 19:24 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/25/15 19:24 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/25/15 19:24 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/25/15 19:24 108-10-11000.33 1
Styrene ND ug/L 02/25/15 19:24 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/25/15 19:24 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/25/15 19:24 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/25/15 19:24 127-18-41.0 0.46 1
Toluene ND ug/L 02/25/15 19:24 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/25/15 19:24 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/25/15 19:24 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/25/15 19:24 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/25/15 19:24 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/25/15 19:24 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/25/15 19:24 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/25/15 19:24 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/25/15 19:24 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)108 %02/25/15 19:24 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %02/25/15 19:24 17060-07-070-130 1
Toluene-d8 (S)99 %02/25/15 19:24 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:MW-11 Lab ID:92237757011 Collected:02/11/15 12:05 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 02:00 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/19/15 02:00 7440-38-202/16/15 16:1010.0 2.5 1
Barium 26.0J ug/L 02/19/15 02:00 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 02:00 7440-41-702/16/15 16:101.0 0.50 1
Cadmium 1.2 ug/L 02/19/15 02:00 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/19/15 02:00 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/19/15 02:00 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/19/15 02:00 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/19/15 02:00 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/19/15 02:00 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 02:00 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 02:00 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/19/15 02:00 7440-28-002/16/15 16:105.5 5.0 1
Vanadium ND ug/L 02/19/15 02:00 7440-62-202/16/15 16:1025.0 2.5 1
Zinc 6.7J ug/L 02/25/15 14:31 7440-66-6 B02/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/25/15 19:41 67-64-110010.0 1
Acrylonitrile ND ug/L 02/25/15 19:41 107-13-12001.9 1
Benzene ND ug/L 02/25/15 19:41 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/25/15 19:41 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/25/15 19:41 75-27-41.0 0.18 1
Bromoform ND ug/L 02/25/15 19:41 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/25/15 19:41 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/25/15 19:41 78-93-31000.96 1
Carbon disulfide ND ug/L 02/25/15 19:41 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/25/15 19:41 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/25/15 19:41 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/25/15 19:41 75-00-310.0 0.54 1
Chloroform ND ug/L 02/25/15 19:41 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/25/15 19:41 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/25/15 19:41 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/25/15 19:41 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/25/15 19:41 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/25/15 19:41 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/25/15 19:41 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/25/15 19:41 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/25/15 19:41 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/25/15 19:41 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/25/15 19:41 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/25/15 19:41 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/25/15 19:41 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/25/15 19:41 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/25/15 19:41 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/25/15 19:41 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/25/15 19:41 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:MW-11 Lab ID:92237757011 Collected:02/11/15 12:05 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/25/15 19:41 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/25/15 19:41 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/25/15 19:41 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/25/15 19:41 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/25/15 19:41 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/25/15 19:41 108-10-11000.33 1
Styrene ND ug/L 02/25/15 19:41 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/25/15 19:41 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/25/15 19:41 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/25/15 19:41 127-18-41.0 0.46 1
Toluene ND ug/L 02/25/15 19:41 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/25/15 19:41 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/25/15 19:41 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/25/15 19:41 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/25/15 19:41 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/25/15 19:41 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/25/15 19:41 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/25/15 19:41 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/25/15 19:41 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)107 %02/25/15 19:41 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %02/25/15 19:41 17060-07-070-130 1
Toluene-d8 (S)99 %02/25/15 19:41 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:MW-12 Lab ID:92237757012 Collected:02/11/15 11:50 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 02:03 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/19/15 02:03 7440-38-202/16/15 16:1010.0 2.5 1
Barium 144 ug/L 02/19/15 02:03 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 02:03 7440-41-702/16/15 16:101.0 0.50 1
Cadmium ND ug/L 02/19/15 02:03 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/19/15 02:03 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt 61.6 ug/L 02/19/15 02:03 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/19/15 02:03 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/19/15 02:03 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/19/15 02:03 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 02:03 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 02:03 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/19/15 02:03 7440-28-002/16/15 16:105.5 5.0 1
Vanadium 2.8J ug/L 02/19/15 02:03 7440-62-202/16/15 16:1025.0 2.5 1
Zinc 14.7 ug/L 02/25/15 14:34 7440-66-6 B02/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/25/15 19:58 67-64-110010.0 1
Acrylonitrile ND ug/L 02/25/15 19:58 107-13-12001.9 1
Benzene 0.80J ug/L 02/25/15 19:58 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/25/15 19:58 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/25/15 19:58 75-27-41.0 0.18 1
Bromoform ND ug/L 02/25/15 19:58 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/25/15 19:58 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/25/15 19:58 78-93-31000.96 1
Carbon disulfide ND ug/L 02/25/15 19:58 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/25/15 19:58 56-23-51.0 0.25 1
Chlorobenzene 0.27J ug/L 02/25/15 19:58 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/25/15 19:58 75-00-310.0 0.54 1
Chloroform ND ug/L 02/25/15 19:58 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/25/15 19:58 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/25/15 19:58 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/25/15 19:58 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/25/15 19:58 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/25/15 19:58 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/25/15 19:58 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/25/15 19:58 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/25/15 19:58 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/25/15 19:58 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/25/15 19:58 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/25/15 19:58 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/25/15 19:58 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/25/15 19:58 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/25/15 19:58 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/25/15 19:58 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/25/15 19:58 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:MW-12 Lab ID:92237757012 Collected:02/11/15 11:50 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/25/15 19:58 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/25/15 19:58 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/25/15 19:58 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/25/15 19:58 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/25/15 19:58 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/25/15 19:58 108-10-11000.33 1
Styrene ND ug/L 02/25/15 19:58 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/25/15 19:58 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/25/15 19:58 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/25/15 19:58 127-18-41.0 0.46 1
Toluene ND ug/L 02/25/15 19:58 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/25/15 19:58 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/25/15 19:58 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/25/15 19:58 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/25/15 19:58 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/25/15 19:58 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/25/15 19:58 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/25/15 19:58 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/25/15 19:58 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)105 %02/25/15 19:58 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %02/25/15 19:58 17060-07-070-130 1
Toluene-d8 (S)98 %02/25/15 19:58 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:MW-13 Lab ID:92237757013 Collected:02/11/15 08:35 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 02:06 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/19/15 02:06 7440-38-202/16/15 16:1010.0 2.5 1
Barium 33.2J ug/L 02/19/15 02:06 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 02:06 7440-41-702/16/15 16:101.0 0.50 1
Cadmium 0.58J ug/L 02/19/15 02:06 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/19/15 02:06 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/19/15 02:06 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/19/15 02:06 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/19/15 02:06 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/19/15 02:06 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 02:06 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 02:06 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/19/15 02:06 7440-28-002/16/15 16:105.5 5.0 1
Vanadium ND ug/L 02/19/15 02:06 7440-62-202/16/15 16:1025.0 2.5 1
Zinc 41.2 ug/L 02/24/15 19:58 7440-66-6 B02/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/25/15 20:15 67-64-110010.0 1
Acrylonitrile ND ug/L 02/25/15 20:15 107-13-12001.9 1
Benzene 0.67J ug/L 02/25/15 20:15 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/25/15 20:15 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/25/15 20:15 75-27-41.0 0.18 1
Bromoform ND ug/L 02/25/15 20:15 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/25/15 20:15 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/25/15 20:15 78-93-31000.96 1
Carbon disulfide ND ug/L 02/25/15 20:15 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/25/15 20:15 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/25/15 20:15 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/25/15 20:15 75-00-310.0 0.54 1
Chloroform ND ug/L 02/25/15 20:15 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/25/15 20:15 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/25/15 20:15 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/25/15 20:15 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/25/15 20:15 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/25/15 20:15 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/25/15 20:15 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/25/15 20:15 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/25/15 20:15 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/25/15 20:15 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/25/15 20:15 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/25/15 20:15 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/25/15 20:15 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/25/15 20:15 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/25/15 20:15 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/25/15 20:15 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/25/15 20:15 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:MW-13 Lab ID:92237757013 Collected:02/11/15 08:35 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/25/15 20:15 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/25/15 20:15 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/25/15 20:15 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/25/15 20:15 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/25/15 20:15 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/25/15 20:15 108-10-11000.33 1
Styrene ND ug/L 02/25/15 20:15 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/25/15 20:15 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/25/15 20:15 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/25/15 20:15 127-18-41.0 0.46 1
Toluene ND ug/L 02/25/15 20:15 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/25/15 20:15 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/25/15 20:15 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/25/15 20:15 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/25/15 20:15 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/25/15 20:15 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/25/15 20:15 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/25/15 20:15 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/25/15 20:15 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)106 %02/25/15 20:15 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %02/25/15 20:15 17060-07-070-130 1
Toluene-d8 (S)97 %02/25/15 20:15 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:MW-14 Lab ID:92237757014 Collected:02/11/15 09:20 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 02:09 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/19/15 02:09 7440-38-202/16/15 16:1010.0 2.5 1
Barium 36.8J ug/L 02/19/15 02:09 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 02:09 7440-41-702/16/15 16:101.0 0.50 1
Cadmium ND ug/L 02/19/15 02:09 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/19/15 02:09 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/19/15 02:09 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/19/15 02:09 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/19/15 02:09 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/19/15 02:09 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 02:09 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 02:09 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/19/15 02:09 7440-28-002/16/15 16:105.5 5.0 1
Vanadium ND ug/L 02/19/15 02:09 7440-62-202/16/15 16:1025.0 2.5 1
Zinc 6.0J ug/L 02/24/15 20:01 7440-66-6 B02/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/25/15 20:32 67-64-110010.0 1
Acrylonitrile ND ug/L 02/25/15 20:32 107-13-12001.9 1
Benzene ND ug/L 02/25/15 20:32 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/25/15 20:32 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/25/15 20:32 75-27-41.0 0.18 1
Bromoform ND ug/L 02/25/15 20:32 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/25/15 20:32 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/25/15 20:32 78-93-31000.96 1
Carbon disulfide ND ug/L 02/25/15 20:32 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/25/15 20:32 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/25/15 20:32 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/25/15 20:32 75-00-310.0 0.54 1
Chloroform ND ug/L 02/25/15 20:32 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/25/15 20:32 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/25/15 20:32 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/25/15 20:32 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/25/15 20:32 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/25/15 20:32 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/25/15 20:32 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/25/15 20:32 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/25/15 20:32 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/25/15 20:32 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/25/15 20:32 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/25/15 20:32 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/25/15 20:32 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/25/15 20:32 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/25/15 20:32 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/25/15 20:32 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/25/15 20:32 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:MW-14 Lab ID:92237757014 Collected:02/11/15 09:20 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/25/15 20:32 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/25/15 20:32 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/25/15 20:32 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/25/15 20:32 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/25/15 20:32 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/25/15 20:32 108-10-11000.33 1
Styrene ND ug/L 02/25/15 20:32 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/25/15 20:32 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/25/15 20:32 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/25/15 20:32 127-18-41.0 0.46 1
Toluene ND ug/L 02/25/15 20:32 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/25/15 20:32 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/25/15 20:32 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/25/15 20:32 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/25/15 20:32 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/25/15 20:32 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/25/15 20:32 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/25/15 20:32 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/25/15 20:32 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)106 %02/25/15 20:32 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %02/25/15 20:32 17060-07-070-130 1
Toluene-d8 (S)99 %02/25/15 20:32 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:MW-15 Lab ID:92237757015 Collected:02/11/15 09:05 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 02:12 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/19/15 02:12 7440-38-202/16/15 16:1010.0 2.5 1
Barium ND ug/L 02/19/15 02:12 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 02:12 7440-41-702/16/15 16:101.0 0.50 1
Cadmium 0.85J ug/L 02/19/15 02:12 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/19/15 02:12 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/19/15 02:12 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/19/15 02:12 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/19/15 02:12 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/19/15 02:12 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 02:12 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 02:12 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/19/15 02:12 7440-28-002/16/15 16:105.5 5.0 1
Vanadium ND ug/L 02/19/15 02:12 7440-62-202/16/15 16:1025.0 2.5 1
Zinc 10.2 ug/L 02/24/15 20:04 7440-66-6 B02/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/25/15 20:48 67-64-110010.0 1
Acrylonitrile ND ug/L 02/25/15 20:48 107-13-12001.9 1
Benzene ND ug/L 02/25/15 20:48 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/25/15 20:48 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/25/15 20:48 75-27-41.0 0.18 1
Bromoform ND ug/L 02/25/15 20:48 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/25/15 20:48 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/25/15 20:48 78-93-31000.96 1
Carbon disulfide ND ug/L 02/25/15 20:48 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/25/15 20:48 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/25/15 20:48 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/25/15 20:48 75-00-310.0 0.54 1
Chloroform ND ug/L 02/25/15 20:48 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/25/15 20:48 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/25/15 20:48 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/25/15 20:48 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/25/15 20:48 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/25/15 20:48 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/25/15 20:48 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/25/15 20:48 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/25/15 20:48 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/25/15 20:48 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/25/15 20:48 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/25/15 20:48 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/25/15 20:48 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/25/15 20:48 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/25/15 20:48 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/25/15 20:48 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/25/15 20:48 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:MW-15 Lab ID:92237757015 Collected:02/11/15 09:05 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/25/15 20:48 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/25/15 20:48 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/25/15 20:48 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/25/15 20:48 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/25/15 20:48 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/25/15 20:48 108-10-11000.33 1
Styrene ND ug/L 02/25/15 20:48 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/25/15 20:48 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/25/15 20:48 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/25/15 20:48 127-18-41.0 0.46 1
Toluene ND ug/L 02/25/15 20:48 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/25/15 20:48 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/25/15 20:48 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/25/15 20:48 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/25/15 20:48 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/25/15 20:48 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/25/15 20:48 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/25/15 20:48 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/25/15 20:48 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)106 %02/25/15 20:48 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %02/25/15 20:48 17060-07-070-130 1
Toluene-d8 (S)99 %02/25/15 20:48 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:MW-16R Lab ID:92237757016 Collected:02/12/15 09:50 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 02:15 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/19/15 02:15 7440-38-202/16/15 16:1010.0 2.5 1
Barium 29.9J ug/L 02/19/15 02:15 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 02:15 7440-41-702/16/15 16:101.0 0.50 1
Cadmium ND ug/L 02/19/15 02:15 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/19/15 02:15 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/19/15 02:15 7440-48-402/16/15 16:1010.0 2.5 1
Copper 2.7J ug/L 02/19/15 02:15 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/19/15 02:15 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/19/15 02:15 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 02:15 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 02:15 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/19/15 02:15 7440-28-002/16/15 16:105.5 5.0 1
Vanadium 3.2J ug/L 02/19/15 02:15 7440-62-202/16/15 16:1025.0 2.5 1
Zinc ND ug/L 02/24/15 20:07 7440-66-602/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone 10.5J ug/L 02/25/15 21:05 67-64-110010.0 1
Acrylonitrile ND ug/L 02/25/15 21:05 107-13-12001.9 1
Benzene ND ug/L 02/25/15 21:05 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/25/15 21:05 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/25/15 21:05 75-27-41.0 0.18 1
Bromoform ND ug/L 02/25/15 21:05 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/25/15 21:05 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/25/15 21:05 78-93-31000.96 1
Carbon disulfide ND ug/L 02/25/15 21:05 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/25/15 21:05 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/25/15 21:05 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/25/15 21:05 75-00-310.0 0.54 1
Chloroform ND ug/L 02/25/15 21:05 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/25/15 21:05 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/25/15 21:05 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/25/15 21:05 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/25/15 21:05 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/25/15 21:05 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/25/15 21:05 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/25/15 21:05 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/25/15 21:05 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/25/15 21:05 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/25/15 21:05 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/25/15 21:05 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/25/15 21:05 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/25/15 21:05 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/25/15 21:05 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/25/15 21:05 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/25/15 21:05 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:MW-16R Lab ID:92237757016 Collected:02/12/15 09:50 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/25/15 21:05 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/25/15 21:05 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/25/15 21:05 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/25/15 21:05 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/25/15 21:05 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/25/15 21:05 108-10-11000.33 1
Styrene ND ug/L 02/25/15 21:05 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/25/15 21:05 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/25/15 21:05 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/25/15 21:05 127-18-41.0 0.46 1
Toluene ND ug/L 02/25/15 21:05 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/25/15 21:05 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/25/15 21:05 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/25/15 21:05 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/25/15 21:05 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/25/15 21:05 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/25/15 21:05 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/25/15 21:05 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/25/15 21:05 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)106 %02/25/15 21:05 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %02/25/15 21:05 17060-07-070-130 1
Toluene-d8 (S)99 %02/25/15 21:05 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:SW-4 Lab ID:92237757017 Collected:02/11/15 08:30 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 02:28 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/19/15 02:28 7440-38-202/16/15 16:1010.0 2.5 1
Barium 86.4J ug/L 02/19/15 02:28 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 02:28 7440-41-702/16/15 16:101.0 0.50 1
Cadmium 0.62J ug/L 02/19/15 02:28 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/19/15 02:28 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/19/15 02:28 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/19/15 02:28 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/19/15 02:28 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/19/15 02:28 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 02:28 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 02:28 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/19/15 02:28 7440-28-002/16/15 16:105.5 5.0 1
Vanadium ND ug/L 02/19/15 02:28 7440-62-202/16/15 16:1025.0 2.5 1
Zinc 15.0 ug/L 02/24/15 20:10 7440-66-6 B02/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/25/15 21:22 67-64-110010.0 1
Acrylonitrile ND ug/L 02/25/15 21:22 107-13-12001.9 1
Benzene ND ug/L 02/25/15 21:22 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/25/15 21:22 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/25/15 21:22 75-27-41.0 0.18 1
Bromoform ND ug/L 02/25/15 21:22 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/25/15 21:22 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/25/15 21:22 78-93-31000.96 1
Carbon disulfide ND ug/L 02/25/15 21:22 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/25/15 21:22 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/25/15 21:22 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/25/15 21:22 75-00-310.0 0.54 1
Chloroform ND ug/L 02/25/15 21:22 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/25/15 21:22 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/25/15 21:22 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/25/15 21:22 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/25/15 21:22 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/25/15 21:22 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/25/15 21:22 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/25/15 21:22 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/25/15 21:22 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/25/15 21:22 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/25/15 21:22 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/25/15 21:22 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/25/15 21:22 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/25/15 21:22 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/25/15 21:22 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/25/15 21:22 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/25/15 21:22 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:SW-4 Lab ID:92237757017 Collected:02/11/15 08:30 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/25/15 21:22 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/25/15 21:22 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/25/15 21:22 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/25/15 21:22 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/25/15 21:22 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/25/15 21:22 108-10-11000.33 1
Styrene ND ug/L 02/25/15 21:22 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/25/15 21:22 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/25/15 21:22 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/25/15 21:22 127-18-41.0 0.46 1
Toluene ND ug/L 02/25/15 21:22 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/25/15 21:22 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/25/15 21:22 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/25/15 21:22 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/25/15 21:22 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/25/15 21:22 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/25/15 21:22 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/25/15 21:22 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/25/15 21:22 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)104 %02/25/15 21:22 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %02/25/15 21:22 17060-07-070-130 1
Toluene-d8 (S)98 %02/25/15 21:22 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:SW-5 Lab ID:92237757018 Collected:02/11/15 08:50 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 02:31 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/19/15 02:31 7440-38-202/16/15 16:1010.0 2.5 1
Barium 320 ug/L 02/19/15 02:31 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 02:31 7440-41-702/16/15 16:101.0 0.50 1
Cadmium 0.60J ug/L 02/19/15 02:31 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/19/15 02:31 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/19/15 02:31 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/19/15 02:31 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/19/15 02:31 7439-92-102/16/15 16:1010.0 2.5 1
Nickel 3.3J ug/L 02/19/15 02:31 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 02:31 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 02:31 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/19/15 02:31 7440-28-002/16/15 16:105.5 5.0 1
Vanadium ND ug/L 02/19/15 02:31 7440-62-202/16/15 16:1025.0 2.5 1
Zinc 18.0 ug/L 02/24/15 20:13 7440-66-6 B02/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/25/15 21:39 67-64-110010.0 1
Acrylonitrile ND ug/L 02/25/15 21:39 107-13-12001.9 1
Benzene ND ug/L 02/25/15 21:39 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/25/15 21:39 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/25/15 21:39 75-27-41.0 0.18 1
Bromoform ND ug/L 02/25/15 21:39 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/25/15 21:39 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/25/15 21:39 78-93-31000.96 1
Carbon disulfide ND ug/L 02/25/15 21:39 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/25/15 21:39 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/25/15 21:39 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/25/15 21:39 75-00-310.0 0.54 1
Chloroform ND ug/L 02/25/15 21:39 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/25/15 21:39 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/25/15 21:39 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/25/15 21:39 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/25/15 21:39 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/25/15 21:39 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/25/15 21:39 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/25/15 21:39 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/25/15 21:39 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/25/15 21:39 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/25/15 21:39 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/25/15 21:39 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/25/15 21:39 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/25/15 21:39 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/25/15 21:39 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/25/15 21:39 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/25/15 21:39 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:SW-5 Lab ID:92237757018 Collected:02/11/15 08:50 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/25/15 21:39 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/25/15 21:39 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/25/15 21:39 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/25/15 21:39 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/25/15 21:39 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/25/15 21:39 108-10-11000.33 1
Styrene ND ug/L 02/25/15 21:39 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/25/15 21:39 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/25/15 21:39 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/25/15 21:39 127-18-41.0 0.46 1
Toluene ND ug/L 02/25/15 21:39 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/25/15 21:39 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/25/15 21:39 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/25/15 21:39 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/25/15 21:39 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/25/15 21:39 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/25/15 21:39 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/25/15 21:39 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/25/15 21:39 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)107 %02/25/15 21:39 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %02/25/15 21:39 17060-07-070-130 1
Toluene-d8 (S)99 %02/25/15 21:39 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:LE-1 Lab ID:92237757019 Collected:02/12/15 17:00 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony 7.5 ug/L 02/19/15 02:34 7440-36-002/16/15 16:106.0 3.8 1
Arsenic 8.2J ug/L 02/19/15 02:34 7440-38-202/16/15 16:1010.0 2.5 1
Barium 195 ug/L 02/19/15 02:34 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 02:34 7440-41-702/16/15 16:101.0 0.50 1
Cadmium ND ug/L 02/19/15 02:34 7440-43-902/16/15 16:101.0 0.50 1
Chromium 5.9J ug/L 02/19/15 02:34 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt 2.6J ug/L 02/19/15 02:34 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/19/15 02:34 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/19/15 02:34 7439-92-102/16/15 16:1010.0 2.5 1
Nickel 28.7J ug/L 02/19/15 02:34 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 02:34 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 02:34 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/19/15 02:34 7440-28-002/16/15 16:105.5 5.0 1
Vanadium 4.2J ug/L 02/19/15 02:34 7440-62-202/16/15 16:1025.0 2.5 1
Zinc 6.6J ug/L 02/24/15 20:17 7440-66-6 B02/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/25/15 21:56 67-64-110010.0 1
Acrylonitrile ND ug/L 02/25/15 21:56 107-13-12001.9 1
Benzene 9.8 ug/L 02/25/15 21:56 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/25/15 21:56 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/25/15 21:56 75-27-41.0 0.18 1
Bromoform ND ug/L 02/25/15 21:56 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/25/15 21:56 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/25/15 21:56 78-93-31000.96 1
Carbon disulfide ND ug/L 02/25/15 21:56 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/25/15 21:56 56-23-51.0 0.25 1
Chlorobenzene 1.4J ug/L 02/25/15 21:56 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/25/15 21:56 75-00-310.0 0.54 1
Chloroform ND ug/L 02/25/15 21:56 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/25/15 21:56 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/25/15 21:56 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/25/15 21:56 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/25/15 21:56 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/25/15 21:56 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/25/15 21:56 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/25/15 21:56 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/25/15 21:56 110-57-61001.0 1
1,1-Dichloroethane 0.57J ug/L 02/25/15 21:56 75-34-35.0 0.32 1
1,2-Dichloroethane 0.41J ug/L 02/25/15 21:56 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/25/15 21:56 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/25/15 21:56 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/25/15 21:56 156-60-55.0 0.49 1
1,2-Dichloropropane 0.53J ug/L 02/25/15 21:56 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/25/15 21:56 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/25/15 21:56 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
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[phone]
Page 42 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Sample:LE-1 Lab ID:92237757019 Collected:02/12/15 17:00 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/25/15 21:56 10061-02-61.0 0.26 1
Ethylbenzene 1.4 ug/L 02/25/15 21:56 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/25/15 21:56 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/25/15 21:56 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/25/15 21:56 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/25/15 21:56 108-10-11000.33 1
Styrene ND ug/L 02/25/15 21:56 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/25/15 21:56 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/25/15 21:56 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/25/15 21:56 127-18-41.0 0.46 1
Toluene 0.81J ug/L 02/25/15 21:56 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/25/15 21:56 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/25/15 21:56 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/25/15 21:56 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/25/15 21:56 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/25/15 21:56 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/25/15 21:56 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/25/15 21:56 75-01-41.0 0.62 1
Xylene (Total)18.2 ug/L 02/25/15 21:56 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)106 %02/25/15 21:56 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %02/25/15 21:56 17060-07-070-130 1
Toluene-d8 (S)98 %02/25/15 21:56 2037-26-570-130 1
Analytical Method: SM 5210B5210B BOD, 5 day
BOD, 5 day 148000 ug/L 02/19/15 05:40 L202/14/15 06:00200020001
Analytical Method: EPA 90409040 pH
pH 6.9 Std. Units 02/18/15 10:45 H60.10 0.10 1
Analytical Method: EPA 300.0300.0 IC Anions 28 Days
Sulfate 27800J ug/L 02/20/15 12:55 14808-79-850000020002
Analytical Method: EPA 353.2353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate ND ug/L 02/13/15 23:121000010.0 1
Analytical Method: EPA 365.1365.1 Phosphorus, Total
Phosphorus 1670 ug/L 02/23/15 14:50 7723-14-050.0 25.0 1
Analytical Method: SM 5220D5220D COD
Chemical Oxygen Demand 1070000 ug/L 02/19/15 10:2525000125001
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 68
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/17907
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92237757001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1392765
Associated Lab Samples:92237757001
Matrix:Water
Analyzed
Antimony ug/L ND 6.0 02/18/15 23:26
Arsenic ug/L ND 10.0 02/18/15 23:26
Barium ug/L ND 100 02/18/15 23:26
Beryllium ug/L ND 1.0 02/18/15 23:26
Cadmium ug/L ND 1.0 02/18/15 23:26
Chromium ug/L ND 10.0 02/18/15 23:26
Cobalt ug/L ND 10.0 02/18/15 23:26
Copper ug/L ND 10.0 02/18/15 23:26
Lead ug/L ND 10.0 02/18/15 23:26
Nickel ug/L ND 50.0 02/18/15 23:26
Selenium ug/L ND 10.0 02/18/15 23:26
Silver ug/L ND 10.0 02/18/15 23:26
Thallium ug/L ND 5.5 02/18/15 23:26
Vanadium ug/L ND 25.0 02/18/15 23:26
Zinc ug/L ND 10.0 02/18/15 23:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1392766LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 477500 95 80-120
Arsenic ug/L 464500 93 80-120
Barium ug/L 484500 97 80-120
Beryllium ug/L 480500 96 80-120
Cadmium ug/L 486500 97 80-120
Chromium ug/L 500500 100 80-120
Cobalt ug/L 490500 98 80-120
Copper ug/L 483500 97 80-120
Lead ug/L 490500 98 80-120
Nickel ug/L 480500 96 80-120
Selenium ug/L 465500 93 80-120
Silver ug/L 246250 98 80-120
Thallium ug/L 440500 88 80-120
Vanadium ug/L 471500 94 80-120
Zinc ug/L 466500 93 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 68
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1392767MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237748001
1392768
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 96 75-12598 2 25500ND479490
Arsenic ug/L 500 92 75-12595 3 25500ND462474
Barium ug/L 500 99 75-125101 3 25500ND493507
Beryllium ug/L 500 98 75-125101 3 25500ND490505
Cadmium ug/L 500 98 75-125100 3 25500ND488501
Chromium ug/L 500 102 75-125105 3 25500ND510525
Cobalt ug/L 500 99 75-125102 3 25500ND497511
Copper ug/L 500 98 75-125101 3 25500ND493507
Lead ug/L 500 99 75-125102 2 25500ND496509
Nickel ug/L 500 97 75-125100 3 25500ND486499
Selenium ug/L 500 92 75-12594 2 25500ND462470
Silver ug/L 250 99 75-125101 2 25250ND248254
Thallium ug/L 500 89 75-12592 4 25500ND448465
Vanadium ug/L 500 97 75-125100 3 25500ND486500
Zinc ug/L 500 93 75-12595 2 25500ND469479
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 68
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/17908
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92237757002, 92237757003, 92237757004, 92237757005, 92237757006, 92237757007, 92237757008,
92237757009, 92237757010, 92237757011, 92237757012, 92237757013, 92237757014, 92237757015,
92237757016, 92237757017, 92237757018, 92237757019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1392769
Associated Lab Samples:92237757002, 92237757003, 92237757004, 92237757005, 92237757006, 92237757007, 92237757008,
92237757009, 92237757010, 92237757011, 92237757012, 92237757013, 92237757014, 92237757015,
92237757016, 92237757017, 92237757018, 92237757019
Matrix:Water
Analyzed
Antimony ug/L ND 6.0 02/19/15 01:11
Arsenic ug/L ND 10.0 02/19/15 01:11
Barium ug/L ND 100 02/19/15 01:11
Beryllium ug/L ND 1.0 02/19/15 01:11
Cadmium ug/L ND 1.0 02/19/15 01:11
Chromium ug/L ND 10.0 02/19/15 01:11
Cobalt ug/L ND 10.0 02/19/15 01:11
Copper ug/L ND 10.0 02/19/15 01:11
Lead ug/L ND 10.0 02/19/15 01:11
Nickel ug/L ND 50.0 02/19/15 01:11
Selenium ug/L ND 10.0 02/19/15 01:11
Silver ug/L ND 10.0 02/19/15 01:11
Thallium ug/L ND 5.5 02/19/15 01:11
Vanadium ug/L ND 25.0 02/19/15 01:11
Zinc ug/L 5.6J 10.0 02/25/15 13:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1392770LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 491500 98 80-120
Arsenic ug/L 477500 95 80-120
Barium ug/L 508500 102 80-120
Beryllium ug/L 507500 101 80-120
Cadmium ug/L 503500 101 80-120
Chromium ug/L 528500 106 80-120
Cobalt ug/L 512500 102 80-120
Copper ug/L 508500 102 80-120
Lead ug/L 512500 102 80-120
Nickel ug/L 500500 100 80-120
Selenium ug/L 474500 95 80-120
Silver ug/L 255250 102 80-120
Thallium ug/L 474500 95 80-120
Vanadium ug/L 501500 100 80-120
Zinc ug/L 490500 98 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 68
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1392771MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237757002
1392772
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 96 75-12596 1 25500ND478481
Arsenic ug/L 500 94 75-12595 1 25500ND470473
Barium ug/L 500 100 75-125100 0 2550014.0J 515 516
Beryllium ug/L 500 99 75-12599 0 25500ND496496
Cadmium ug/L 500 100 75-125101 1 255000.63J 502 504
Chromium ug/L 500 105 75-125104 0 25500ND523521
Cobalt ug/L 500 101 75-125102 1 25500ND508510
Copper ug/L 500 101 75-125101 0 25500ND506506
Lead ug/L 500 101 75-125102 1 255006.6J 512 517
Nickel ug/L 500 98 75-12599 1 25500ND490494
Selenium ug/L 500 93 75-12593 0 255005.9J 473 473
Silver ug/L 250 100 75-125100 0 25250ND252252
Thallium ug/L 500 94 75-12596 2 255007.2 477 486
Vanadium ug/L 500 98 75-12598 0 255004.3J 496 496
Zinc ug/L 500 96 75-12596 0 25500ND482480
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 68
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/30489
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92237757001, 92237757002, 92237757003, 92237757004, 92237757005, 92237757006, 92237757007,
92237757008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1397928
Associated Lab Samples:92237757001, 92237757002, 92237757003, 92237757004, 92237757005, 92237757006, 92237757007,
92237757008
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 5.0 02/25/15 17:18
1,1,1-Trichloroethane ug/L ND 1.0 02/25/15 17:18
1,1,2,2-Tetrachloroethane ug/L ND 3.0 02/25/15 17:18
1,1,2-Trichloroethane ug/L ND 1.0 02/25/15 17:18
1,1-Dichloroethane ug/L ND 5.0 02/25/15 17:18
1,1-Dichloroethene ug/L ND 5.0 02/25/15 17:18
1,2,3-Trichloropropane ug/L ND 1.0 02/25/15 17:18
1,2-Dibromo-3-chloropropane ug/L ND 13.0 02/25/15 17:18
1,2-Dibromoethane (EDB)ug/L ND 1.0 02/25/15 17:18
1,2-Dichlorobenzene ug/L ND 5.0 02/25/15 17:18
1,2-Dichloroethane ug/L ND 1.0 02/25/15 17:18
1,2-Dichloropropane ug/L ND 1.0 02/25/15 17:18
1,3-Dichloropropane ug/L ND 1.0 02/25/15 17:18
1,4-Dichlorobenzene ug/L ND 1.0 02/25/15 17:18
2-Butanone (MEK)ug/L ND 100 02/25/15 17:18
2-Hexanone ug/L ND 50.0 02/25/15 17:18
4-Methyl-2-pentanone (MIBK)ug/L ND 100 02/25/15 17:18
Acetone ug/L ND 100 02/25/15 17:18
Acrylonitrile ug/L ND 200 02/25/15 17:18
Benzene ug/L ND 1.0 02/25/15 17:18
Bromochloromethane ug/L ND 3.0 02/25/15 17:18
Bromodichloromethane ug/L ND 1.0 02/25/15 17:18
Bromoform ug/L ND 3.0 02/25/15 17:18
Bromomethane ug/L ND 10.0 02/25/15 17:18
Carbon disulfide ug/L ND 100 02/25/15 17:18
Carbon tetrachloride ug/L ND 1.0 02/25/15 17:18
Chlorobenzene ug/L ND 3.0 02/25/15 17:18
Chloroethane ug/L ND 10.0 02/25/15 17:18
Chloroform ug/L ND 5.0 02/25/15 17:18
Chloromethane ug/L ND 1.0 02/25/15 17:18
cis-1,2-Dichloroethene ug/L ND 5.0 02/25/15 17:18
cis-1,3-Dichloropropene ug/L ND 1.0 02/25/15 17:18
Dibromochloromethane ug/L ND 3.0 02/25/15 17:18
Dibromomethane ug/L ND 10.0 02/25/15 17:18
Ethylbenzene ug/L ND 1.0 02/25/15 17:18
Iodomethane ug/L ND 10.0 02/25/15 17:18
Methylene Chloride ug/L ND 1.0 02/25/15 17:18
Styrene ug/L ND 1.0 02/25/15 17:18
Tetrachloroethene ug/L ND 1.0 02/25/15 17:18
Toluene ug/L ND 1.0 02/25/15 17:18
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 68
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1397928
Associated Lab Samples:92237757001, 92237757002, 92237757003, 92237757004, 92237757005, 92237757006, 92237757007,
92237757008
Matrix:Water
Analyzed
trans-1,2-Dichloroethene ug/L ND 5.0 02/25/15 17:18
trans-1,3-Dichloropropene ug/L ND 1.0 02/25/15 17:18
trans-1,4-Dichloro-2-butene ug/L ND 100 02/25/15 17:18
Trichloroethene ug/L ND 1.0 02/25/15 17:18
Trichlorofluoromethane ug/L ND 1.0 02/25/15 17:18
Vinyl acetate ug/L ND 50.0 02/25/15 17:18
Vinyl chloride ug/L ND 1.0 02/25/15 17:18
Xylene (Total)ug/L ND 5.0 02/25/15 17:18
1,2-Dichloroethane-d4 (S)%99 70-130 02/25/15 17:18
4-Bromofluorobenzene (S)%99 70-130 02/25/15 17:18
Toluene-d8 (S)%95 70-130 02/25/15 17:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1397929LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 47.050 94 80-125
1,1,1-Trichloroethane ug/L 48.350 97 71-129
1,1,2,2-Tetrachloroethane ug/L 46.450 93 79-124
1,1,2-Trichloroethane ug/L 48.350 97 85-125
1,1-Dichloroethane ug/L 48.250 96 73-126
1,1-Dichloroethene ug/L 46.450 93 66-135
1,2,3-Trichloropropane ug/L 48.150 96 75-130
1,2-Dibromo-3-chloropropane ug/L 46.550 93 71-133
1,2-Dibromoethane (EDB)ug/L 50.150 100 83-124
1,2-Dichlorobenzene ug/L 49.150 98 80-133
1,2-Dichloroethane ug/L 49.250 98 67-128
1,2-Dichloropropane ug/L 48.750 97 75-132
1,3-Dichloropropane ug/L 47.850 96 76-131
1,4-Dichlorobenzene ug/L 48.650 97 78-130
2-Butanone (MEK)ug/L 104100 104 61-144
2-Hexanone ug/L 93.8100 94 68-143
4-Methyl-2-pentanone (MIBK)ug/L 98.0J100 98 72-135
Acetone ug/L 105100 105 48-146
Acrylonitrile ug/L 258250 103 40-160
Benzene ug/L 49.850 100 80-125
Bromochloromethane ug/L 46.650 93 71-125
Bromodichloromethane ug/L 44.650 89 78-124
Bromoform ug/L 42.750 85 71-128
Bromomethane ug/L 44.450 89 40-160
Carbon disulfide ug/L 40.4J50 81 50-160
Carbon tetrachloride ug/L 48.450 97 69-131
Chlorobenzene ug/L 47.250 94 81-122
Chloroethane ug/L 36.850 74 39-148
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 68
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1397929LABORATORY CONTROL SAMPLE:
LCSSpike
Chloroform ug/L 44.250 88 73-127
Chloromethane ug/L 48.150 96 44-146
cis-1,2-Dichloroethene ug/L 49.350 99 74-124
cis-1,3-Dichloropropene ug/L 47.450 95 72-132
Dibromochloromethane ug/L 43.850 88 78-125
Dibromomethane ug/L 48.450 97 82-120
Ethylbenzene ug/L 47.650 95 79-121
Iodomethane ug/L 100100 100 39-154
Methylene Chloride ug/L 53.050 106 64-133
Styrene ug/L 48.550 97 84-126
Tetrachloroethene ug/L 47.550 95 78-122
Toluene ug/L 48.550 97 80-121
trans-1,2-Dichloroethene ug/L 48.650 97 71-127
trans-1,3-Dichloropropene ug/L 47.350 95 69-141
trans-1,4-Dichloro-2-butene ug/L 49.5J50 99 40-160
Trichloroethene ug/L 48.850 98 78-122
Trichlorofluoromethane ug/L 54.850 110 53-137
Vinyl acetate ug/L 108100 108 40-160
Vinyl chloride ug/L 42.650 85 58-137
Xylene (Total)ug/L 143150 95 81-126
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1398024MATRIX SPIKE SAMPLE:
MSSpike
Result
92238381004
1,1,1,2-Tetrachloroethane ug/L 42.640 107 70-130ND
1,1,1-Trichloroethane ug/L 45.740 114 70-130ND
1,1,2,2-Tetrachloroethane ug/L 39.940 100 70-130ND
1,1,2-Trichloroethane ug/L 42.540 106 70-130ND
1,1-Dichloroethane ug/L 43.140 108 70-130ND
1,1-Dichloroethene ug/L 45.140 113 70-166ND
1,2,3-Trichloropropane ug/L 41.440 103 70-130ND
1,2-Dibromo-3-chloropropane ug/L 38.440 96 70-130ND
1,2-Dibromoethane (EDB)ug/L 43.640 109 70-130ND
1,2-Dichlorobenzene ug/L 43.040 107 70-130ND
1,2-Dichloroethane ug/L 44.340 111 70-130ND
1,2-Dichloropropane ug/L 41.740 104 70-130ND
1,3-Dichloropropane ug/L 42.140 105 70-130ND
1,4-Dichlorobenzene ug/L 43.140 108 70-130ND
2-Butanone (MEK)ug/L 86.6J80 108 70-130ND
2-Hexanone ug/L 79.980 100 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 82.5J80 103 70-130ND
Acetone ug/L 86.6J80 104 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 68
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1398024MATRIX SPIKE SAMPLE:
MSSpike
Result
92238381004
Acrylonitrile ug/L 227200 113 70-130ND
Benzene ug/L 44.840 112 70-148ND
Bromochloromethane ug/L 43.240 108 70-130ND
Bromodichloromethane ug/L 39.340 98 70-130ND
Bromoform ug/L 36.240 90 70-130ND
Bromomethane ug/L 36.440 91 70-130ND
Carbon disulfide ug/L 36.6J40 92 70-130ND
Carbon tetrachloride ug/L 45.740 114 70-130ND
Chlorobenzene ug/L 42.140 105 70-146ND
Chloroethane ug/L 35.140 88 70-130ND
Chloroform ug/L 40.140 100 70-130ND
Chloromethane ug/L 41.740 104 70-130ND
cis-1,2-Dichloroethene ug/L 44.240 111 70-130ND
cis-1,3-Dichloropropene ug/L 38.840 97 70-130ND
Dibromochloromethane ug/L 38.440 96 70-130ND
Dibromomethane ug/L 41.840 104 70-130ND
Ethylbenzene ug/L 42.840 107 70-130ND
Iodomethane ug/L 85.080 106 70-130ND
Methylene Chloride ug/L 47.840 120 70-130ND
Styrene ug/L 42.740 107 70-130ND
Tetrachloroethene ug/L 42.040 105 70-130ND
Toluene ug/L 42.940 107 70-155ND
trans-1,2-Dichloroethene ug/L 44.840 112 70-130ND
trans-1,3-Dichloropropene ug/L 40.040 100 70-130ND
trans-1,4-Dichloro-2-butene ug/L 39.4J40 99 70-130ND
Trichloroethene ug/L 43.740 109 69-151ND
Trichlorofluoromethane ug/L 52.040 130 70-130ND
Vinyl acetate ug/L 70.680 88 70-130ND
Vinyl chloride ug/L 37.940 95 70-130ND
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1398900MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237647005
1398901
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 103 70-130103 0 3020ND20.6 20.5
1,1,1-Trichloroethane ug/L 20 109 70-130111 1 3020ND21.9 22.1
1,1,2,2-Tetrachloroethane ug/L 20 98 70-13098 1 3020ND19.6 19.5
1,1,2-Trichloroethane ug/L 20 103 70-130103 0 3020ND20.5 20.6
1,1-Dichloroethane ug/L 20 104 70-130106 2 3020ND20.8 21.2
1,1-Dichloroethene ug/L 20 105 70-166111 6 3020ND20.9 22.1
1,2,3-Trichloropropane ug/L 20 106 70-130107 0 3020ND21.2 21.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 68
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1398900MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237647005
1398901
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2-Dibromo-3-
chloropropane ug/L 20 95 70-13093 2 3020ND18.9 18.6
1,2-Dibromoethane (EDB)ug/L 20 102 70-130104 2 3020ND20.4 20.8
1,2-Dichlorobenzene ug/L 20 106 70-130105 1 3020ND21.2 21.0
1,2-Dichloroethane ug/L 20 105 70-130105 0 3020ND20.9 20.9
1,2-Dichloropropane ug/L 20 100 70-130101 1 3020ND19.9 20.1
1,3-Dichloropropane ug/L 20 100 70-130101 0 3020ND20.1 20.1
1,4-Dichlorobenzene ug/L 20 106 70-130107 1 3020ND21.2 21.4
2-Butanone (MEK)ug/L 40 104 70-130100 4 3040ND41.4J 40.0J
2-Hexanone ug/L 40 103 70-130101 2 3040ND41.3J 40.5J
4-Methyl-2-pentanone
(MIBK)ug/L 40 103 70-130103 0 3040ND41.1J 41.1J
Acetone ug/L 40 115 70-130109 5 3040ND45.9J 43.5J
Acrylonitrile ug/L 100 114 70-130113 1 30100ND114J113J
Benzene ug/L 20 110 70-148112 2 3020ND22.0 22.4
Bromochloromethane ug/L 20 100 70-130106 6 3020ND20.1 21.3
Bromodichloromethane ug/L 20 93 70-13094 0 3020ND18.6 18.7
Bromoform ug/L 20 88 70-13087 1 3020ND17.6 17.4
Bromomethane ug/L 20 75 70-13087 15 3020ND15.0 17.4
Carbon disulfide ug/L 20 88 70-13089 1 3020ND17.6J 17.9J
Carbon tetrachloride ug/L 20 115 70-130114 1 3020ND23.1 22.8
Chlorobenzene ug/L 20 104 70-146103 1 3020ND20.8 20.6
Chloroethane ug/L 20 89 70-13094 5 3020ND17.9 18.7
Chloroform ug/L 20 93 70-13097 4 3020ND18.7 19.4
Chloromethane ug/L 20 105 70-130104 1 3020ND21.1 20.8
cis-1,2-Dichloroethene ug/L 20 105 70-130106 1 3020ND21.0 21.2
cis-1,3-Dichloropropene ug/L 20 88 70-13089 1 3020ND17.6 17.8
Dibromochloromethane ug/L 20 90 70-13090 0 3020ND17.9 18.0
Dibromomethane ug/L 20 99 70-13099 1 3020ND19.7 19.9
Ethylbenzene ug/L 20 105 70-130107 1 3020ND21.1 21.4
Iodomethane ug/L 40 90 70-13098 8 3040ND35.9 39.1
Methylene Chloride ug/L 20 115 70-130115 0 3020ND22.9 23.0
Styrene ug/L 20 99 70-13099 0 3020ND19.8 19.8
Tetrachloroethene ug/L 20 101 70-130101 0 3020ND20.2 20.2
Toluene ug/L 20 105 70-155106 1 3020ND21.0 21.2
trans-1,2-Dichloroethene ug/L 20 106 70-130104 1 3020ND21.1 20.9
trans-1,3-Dichloropropene ug/L 20 92 70-13091 1 3020ND18.4 18.3
trans-1,4-Dichloro-2-butene ug/L 20 104 70-13099 5 3020ND20.9J 19.8J
Trichloroethene ug/L 20 109 69-151109 1 3020ND21.9 21.7
Trichlorofluoromethane ug/L M02013570-130130 4 3020ND27.1 25.9
Vinyl acetate ug/L 40 80 70-13082 3 3040ND31.9J 32.8J
Vinyl chloride ug/L 20 91 70-13093 2 3020ND18.2 18.5
1,2-Dichloroethane-d4 (S)%97 70-13099
4-Bromofluorobenzene (S)%H59370-13092
Toluene-d8 (S)%98 70-13097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 68
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92238381003
1398023SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 68
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92238381003
1398023SAMPLE DUPLICATE:
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%101 3104
4-Bromofluorobenzene (S)%100 298
Toluene-d8 (S)%94 194
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 68
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/30492
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92237757009, 92237757010, 92237757011, 92237757012, 92237757013, 92237757014, 92237757015,
92237757016, 92237757017, 92237757018, 92237757019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1397974
Associated Lab Samples:92237757009, 92237757010, 92237757011, 92237757012, 92237757013, 92237757014, 92237757015,
92237757016, 92237757017, 92237757018, 92237757019
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 5.0 02/25/15 16:01
1,1,1-Trichloroethane ug/L ND 1.0 02/25/15 16:01
1,1,2,2-Tetrachloroethane ug/L ND 3.0 02/25/15 16:01
1,1,2-Trichloroethane ug/L ND 1.0 02/25/15 16:01
1,1-Dichloroethane ug/L ND 5.0 02/25/15 16:01
1,1-Dichloroethene ug/L ND 5.0 02/25/15 16:01
1,2,3-Trichloropropane ug/L ND 1.0 02/25/15 16:01
1,2-Dibromo-3-chloropropane ug/L ND 13.0 02/25/15 16:01
1,2-Dibromoethane (EDB)ug/L ND 1.0 02/25/15 16:01
1,2-Dichlorobenzene ug/L ND 5.0 02/25/15 16:01
1,2-Dichloroethane ug/L ND 1.0 02/25/15 16:01
1,2-Dichloropropane ug/L ND 1.0 02/25/15 16:01
1,3-Dichloropropane ug/L ND 1.0 02/25/15 16:01
1,4-Dichlorobenzene ug/L ND 1.0 02/25/15 16:01
2-Butanone (MEK)ug/L ND 100 02/25/15 16:01
2-Hexanone ug/L ND 50.0 02/25/15 16:01
4-Methyl-2-pentanone (MIBK)ug/L ND 100 02/25/15 16:01
Acetone ug/L ND 100 02/25/15 16:01
Acrylonitrile ug/L ND 200 02/25/15 16:01
Benzene ug/L ND 1.0 02/25/15 16:01
Bromochloromethane ug/L ND 3.0 02/25/15 16:01
Bromodichloromethane ug/L ND 1.0 02/25/15 16:01
Bromoform ug/L ND 3.0 02/25/15 16:01
Bromomethane ug/L ND 10.0 02/25/15 16:01
Carbon disulfide ug/L ND 100 02/25/15 16:01
Carbon tetrachloride ug/L ND 1.0 02/25/15 16:01
Chlorobenzene ug/L ND 3.0 02/25/15 16:01
Chloroethane ug/L ND 10.0 02/25/15 16:01
Chloroform ug/L ND 5.0 02/25/15 16:01
Chloromethane ug/L ND 1.0 02/25/15 16:01
cis-1,2-Dichloroethene ug/L ND 5.0 02/25/15 16:01
cis-1,3-Dichloropropene ug/L ND 1.0 02/25/15 16:01
Dibromochloromethane ug/L ND 3.0 02/25/15 16:01
Dibromomethane ug/L ND 10.0 02/25/15 16:01
Ethylbenzene ug/L ND 1.0 02/25/15 16:01
Iodomethane ug/L ND 10.0 02/25/15 16:01
Methylene Chloride ug/L ND 1.0 02/25/15 16:01
Styrene ug/L ND 1.0 02/25/15 16:01
Tetrachloroethene ug/L ND 1.0 02/25/15 16:01
Toluene ug/L ND 1.0 02/25/15 16:01
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 68
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1397974
Associated Lab Samples:92237757009, 92237757010, 92237757011, 92237757012, 92237757013, 92237757014, 92237757015,
92237757016, 92237757017, 92237757018, 92237757019
Matrix:Water
Analyzed
trans-1,2-Dichloroethene ug/L ND 5.0 02/25/15 16:01
trans-1,3-Dichloropropene ug/L ND 1.0 02/25/15 16:01
trans-1,4-Dichloro-2-butene ug/L ND 100 02/25/15 16:01
Trichloroethene ug/L ND 1.0 02/25/15 16:01
Trichlorofluoromethane ug/L ND 1.0 02/25/15 16:01
Vinyl acetate ug/L ND 50.0 02/25/15 16:01
Vinyl chloride ug/L ND 1.0 02/25/15 16:01
Xylene (Total)ug/L ND 5.0 02/25/15 16:01
1,2-Dichloroethane-d4 (S)%98 70-130 02/25/15 16:01
4-Bromofluorobenzene (S)%108 70-130 02/25/15 16:01
Toluene-d8 (S)%99 70-130 02/25/15 16:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1397975LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.450 99 80-125
1,1,1-Trichloroethane ug/L 47.550 95 71-129
1,1,2,2-Tetrachloroethane ug/L 46.450 93 79-124
1,1,2-Trichloroethane ug/L 47.950 96 85-125
1,1-Dichloroethane ug/L 44.350 89 73-126
1,1-Dichloroethene ug/L 43.150 86 66-135
1,2,3-Trichloropropane ug/L 46.950 94 75-130
1,2-Dibromo-3-chloropropane ug/L 44.450 89 71-133
1,2-Dibromoethane (EDB)ug/L 47.350 95 83-124
1,2-Dichlorobenzene ug/L 45.350 91 80-133
1,2-Dichloroethane ug/L 44.350 89 67-128
1,2-Dichloropropane ug/L 46.750 93 75-132
1,3-Dichloropropane ug/L 45.350 91 76-131
1,4-Dichlorobenzene ug/L 45.950 92 78-130
2-Butanone (MEK)ug/L 89.2J100 89 61-144
2-Hexanone ug/L 97.6100 98 68-143
4-Methyl-2-pentanone (MIBK)ug/L 99.6J100 100 72-135
Acetone ug/L 95.6J100 96 48-146
Acrylonitrile ug/L 238250 95 40-160
Benzene ug/L 48.950 98 80-125
Bromochloromethane ug/L 47.250 94 71-125
Bromodichloromethane ug/L 44.850 90 78-124
Bromoform ug/L 40.950 82 71-128
Bromomethane ug/L 30.750 61 40-160
Carbon disulfide ug/L 39.0J50 78 50-160
Carbon tetrachloride ug/L 51.050 102 69-131
Chlorobenzene ug/L 46.750 93 81-122
Chloroethane ug/L 47.250 94 39-148
REPORT OF LABORATORY ANALYSIS
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Page 56 of 68
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1397975LABORATORY CONTROL SAMPLE:
LCSSpike
Chloroform ug/L 42.150 84 73-127
Chloromethane ug/L 40.850 82 44-146
cis-1,2-Dichloroethene ug/L 45.150 90 74-124
cis-1,3-Dichloropropene ug/L 50.850 102 72-132
Dibromochloromethane ug/L 40.150 80 78-125
Dibromomethane ug/L 52.750 105 82-120
Ethylbenzene ug/L 47.950 96 79-121
Iodomethane ug/L 80.6100 81 39-154
Methylene Chloride ug/L 46.050 92 64-133
Styrene ug/L 50.050 100 84-126
Tetrachloroethene ug/L 48.250 96 78-122
Toluene ug/L 49.250 98 80-121
trans-1,2-Dichloroethene ug/L 44.750 89 71-127
trans-1,3-Dichloropropene ug/L 47.150 94 69-141
trans-1,4-Dichloro-2-butene ug/L 50.0J50 100 40-160
Trichloroethene ug/L 48.050 96 78-122
Trichlorofluoromethane ug/L 49.550 99 53-137
Vinyl acetate ug/L 97.0100 97 40-160
Vinyl chloride ug/L 41.850 84 58-137
Xylene (Total)ug/L 143150 95 81-126
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%110 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/35720
SM 5210B
SM 5210B
5210B BOD, 5 day
Associated Lab Samples:92237757019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1392148
Associated Lab Samples:92237757019
Matrix:Water
Analyzed
BOD, 5 day ug/L ND 2000 02/19/15 05:40
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1392149LABORATORY CONTROL SAMPLE:
LCSSpike
BOD, 5 day ug/L 136000 L01980006984.5-115.4
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92237707001
1392150SAMPLE DUPLICATE:
BOD, 5 day ug/L ND 10<2.0 mg/L
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WET/35765
EPA 9040
EPA 9040
9040 pH
Associated Lab Samples:92237757019
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92237714001
1393390SAMPLE DUPLICATE:
pH Std. Units 8.0 H6098.0
REPORT OF LABORATORY ANALYSIS
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Page 59 of 68
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/21952
EPA 300.0
EPA 300.0
300.0 IC Anions
Associated Lab Samples:92237757019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1393460
Associated Lab Samples:92237757019
Matrix:Water
Analyzed
Sulfate ug/L ND 250000 02/19/15 12:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1393461LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate ug/L 18900J20000 95 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1393462MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237633002
1393463
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L M1200008990-11089 0 1020000ND19300J19400J
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1393464MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237208015
1393465
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Sulfate ug/L 20000 104 90-110101 1 102000015.6 mg/L 36400J 35900J
REPORT OF LABORATORY ANALYSIS
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Page 60 of 68
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/21921
EPA 353.2
EPA 353.2
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples:92237757019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1392134
Associated Lab Samples:92237757019
Matrix:Water
Analyzed
Nitrogen, Nitrate ug/L ND 20.0 02/13/15 22:57
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1392135LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate ug/L 24802500 99 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1392136MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237756001
1392137
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Nitrogen, Nitrate ug/L 2500 93 90-11093 0 102500880J32203200
REPORT OF LABORATORY ANALYSIS
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Page 61 of 68
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/22000
EPA 365.1
EPA 365.1
365.1 Phosphorus, Total
Associated Lab Samples:92237757019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1396034
Associated Lab Samples:92237757019
Matrix:Water
Analyzed
Phosphorus ug/L ND 50.0 02/23/15 14:45
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1396035LABORATORY CONTROL SAMPLE:
LCSSpike
Phosphorus ug/L 26302500 105 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1396036MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237098007
1396037
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phosphorus ug/L M1250012790-110114 2 10250015.0 mg/L 18200 17800
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1396038MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237892002
1396039
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phosphorus ug/L 2500 99 90-11097 2 102500ND24702420
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 62 of 68
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
WETA/21950
SM 5220D
SM 5220D
5220D COD
Associated Lab Samples:92237757019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1393350
Associated Lab Samples:92237757019
Matrix:Water
Analyzed
Chemical Oxygen Demand ug/L ND 25000 02/19/15 10:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1393351LABORATORY CONTROL SAMPLE:
LCSSpike
Chemical Oxygen Demand ug/L 770000750000 103 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1393352MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237491001
1393353
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L M17500007990-11077 1 3750000974 mg/L 1560000 1550000
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1393354MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237535006
1393355
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chemical Oxygen Demand ug/L 750000 108 90-110107 1 3750000ND809000804000
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 63 of 68
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
Reanalysis conducted in excess of EPA method holding time. Results confirm original analysis performed in hold time.H5
Analysis initiated outside of the 15 minute EPA recommended holding time.H6
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
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Page 64 of 68
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92237757
Wayne Lined MSWLF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92237757001 MPRP/17907 ICP/16106MW-1 EPA 3010 EPA 6010
92237757002 MPRP/17908 ICP/16105MW-2 EPA 3010 EPA 6010
92237757003 MPRP/17908 ICP/16105MW-3 EPA 3010 EPA 6010
92237757004 MPRP/17908 ICP/16105MW-4 EPA 3010 EPA 6010
92237757005 MPRP/17908 ICP/16105MW-5 EPA 3010 EPA 6010
92237757006 MPRP/17908 ICP/16105MW-6 EPA 3010 EPA 6010
92237757007 MPRP/17908 ICP/16105MW-7 EPA 3010 EPA 6010
92237757008 MPRP/17908 ICP/16105MW-8 EPA 3010 EPA 6010
92237757009 MPRP/17908 ICP/16105MW-9 EPA 3010 EPA 6010
92237757010 MPRP/17908 ICP/16105MW-10 EPA 3010 EPA 6010
92237757011 MPRP/17908 ICP/16105MW-11 EPA 3010 EPA 6010
92237757012 MPRP/17908 ICP/16105MW-12 EPA 3010 EPA 6010
92237757013 MPRP/17908 ICP/16105MW-13 EPA 3010 EPA 6010
92237757014 MPRP/17908 ICP/16105MW-14 EPA 3010 EPA 6010
92237757015 MPRP/17908 ICP/16105MW-15 EPA 3010 EPA 6010
92237757016 MPRP/17908 ICP/16105MW-16R EPA 3010 EPA 6010
92237757017 MPRP/17908 ICP/16105SW-4 EPA 3010 EPA 6010
92237757018 MPRP/17908 ICP/16105SW-5 EPA 3010 EPA 6010
92237757019 MPRP/17908 ICP/16105LE-1 EPA 3010 EPA 6010
92237757001 MSV/30489MW-1 EPA 8260
92237757002 MSV/30489MW-2 EPA 8260
92237757003 MSV/30489MW-3 EPA 8260
92237757004 MSV/30489MW-4 EPA 8260
92237757005 MSV/30489MW-5 EPA 8260
92237757006 MSV/30489MW-6 EPA 8260
92237757007 MSV/30489MW-7 EPA 8260
92237757008 MSV/30489MW-8 EPA 8260
92237757009 MSV/30492MW-9 EPA 8260
92237757010 MSV/30492MW-10 EPA 8260
92237757011 MSV/30492MW-11 EPA 8260
92237757012 MSV/30492MW-12 EPA 8260
92237757013 MSV/30492MW-13 EPA 8260
92237757014 MSV/30492MW-14 EPA 8260
92237757015 MSV/30492MW-15 EPA 8260
92237757016 MSV/30492MW-16R EPA 8260
92237757017 MSV/30492SW-4 EPA 8260
92237757018 MSV/30492SW-5 EPA 8260
92237757019 MSV/30492LE-1 EPA 8260
92237757019 WET/35720 WET/35722LE-1 SM 5210B SM 5210B
92237757019 WET/35765LE-1 EPA 9040
92237757019 WETA/21952LE-1 EPA 300.0
92237757019 WETA/21921LE-1 EPA 353.2
92237757019 WETA/22000LE-1 EPA 365.1
92237757019 WETA/21950LE-1 SM 5220D
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:06 PM
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Page 65 of 68
Page 66 of 68
Page 67 of 68
Page 68 of 68
#=CL#
February 27, 2015
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92237753
92237753
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
Wayne MSWLF-SWs
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on February 13, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
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Page 1 of 23
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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Page 2 of 23
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Lab ID Sample ID Matrix Date Collected Date Received
92237753001 SW-2 Water 02/11/15 17:15 02/13/15 15:45
92237753002 SW-3 Water 02/11/15 17:25 02/13/15 15:45
92237753003 SW-1 Water 02/11/15 17:35 02/13/15 15:45
REPORT OF LABORATORY ANALYSIS
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#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92237753001 SW-2 EPA 6010 15 PASI-ASH1
EPA 8260 51 PASI-CGAW
92237753002 SW-3 EPA 6010 15 PASI-ASH1
EPA 8260 51 PASI-CGAW
92237753003 SW-1 EPA 6010 15 PASI-ASH1
EPA 8260 51 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Sample:SW-2 Lab ID:92237753001 Collected:02/11/15 17:15 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 00:37 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/19/15 00:37 7440-38-202/16/15 16:1010.0 2.5 1
Barium 27.1J ug/L 02/19/15 00:37 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 00:37 7440-41-702/16/15 16:101.0 0.50 1
Cadmium ND ug/L 02/19/15 00:37 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/19/15 00:37 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/19/15 00:37 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/19/15 00:37 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/19/15 00:37 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/19/15 00:37 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 00:37 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 00:37 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/19/15 00:37 7440-28-002/16/15 16:105.5 5.0 1
Vanadium ND ug/L 02/19/15 00:37 7440-62-202/16/15 16:1025.0 2.5 1
Zinc 7.6J ug/L 02/19/15 00:37 7440-66-602/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/25/15 18:08 67-64-110010.0 1
Acrylonitrile ND ug/L 02/25/15 18:08 107-13-12001.9 1
Benzene ND ug/L 02/25/15 18:08 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/25/15 18:08 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/25/15 18:08 75-27-41.0 0.18 1
Bromoform ND ug/L 02/25/15 18:08 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/25/15 18:08 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/25/15 18:08 78-93-31000.96 1
Carbon disulfide ND ug/L 02/25/15 18:08 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/25/15 18:08 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/25/15 18:08 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/25/15 18:08 75-00-310.0 0.54 1
Chloroform ND ug/L 02/25/15 18:08 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/25/15 18:08 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/25/15 18:08 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/25/15 18:08 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/25/15 18:08 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/25/15 18:08 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/25/15 18:08 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/25/15 18:08 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/25/15 18:08 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/25/15 18:08 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/25/15 18:08 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/25/15 18:08 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/25/15 18:08 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/25/15 18:08 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/25/15 18:08 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/25/15 18:08 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/25/15 18:08 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Sample:SW-2 Lab ID:92237753001 Collected:02/11/15 17:15 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/25/15 18:08 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/25/15 18:08 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/25/15 18:08 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/25/15 18:08 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/25/15 18:08 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/25/15 18:08 108-10-11000.33 1
Styrene ND ug/L 02/25/15 18:08 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/25/15 18:08 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/25/15 18:08 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/25/15 18:08 127-18-41.0 0.46 1
Toluene ND ug/L 02/25/15 18:08 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/25/15 18:08 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/25/15 18:08 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/25/15 18:08 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/25/15 18:08 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/25/15 18:08 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/25/15 18:08 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/25/15 18:08 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/25/15 18:08 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %02/25/15 18:08 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %02/25/15 18:08 17060-07-070-130 1
Toluene-d8 (S)95 %02/25/15 18:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
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Huntersville, NC 28078
[phone]
Page 6 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Sample:SW-3 Lab ID:92237753002 Collected:02/11/15 17:25 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 00:40 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/19/15 00:40 7440-38-202/16/15 16:1010.0 2.5 1
Barium 60.1J ug/L 02/19/15 00:40 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 00:40 7440-41-702/16/15 16:101.0 0.50 1
Cadmium ND ug/L 02/19/15 00:40 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/19/15 00:40 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/19/15 00:40 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/19/15 00:40 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/19/15 00:40 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/19/15 00:40 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 00:40 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 00:40 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/19/15 00:40 7440-28-002/16/15 16:105.5 5.0 1
Vanadium ND ug/L 02/19/15 00:40 7440-62-202/16/15 16:1025.0 2.5 1
Zinc 7.1J ug/L 02/19/15 00:40 7440-66-602/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/25/15 18:25 67-64-110010.0 1
Acrylonitrile ND ug/L 02/25/15 18:25 107-13-12001.9 1
Benzene ND ug/L 02/25/15 18:25 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/25/15 18:25 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/25/15 18:25 75-27-41.0 0.18 1
Bromoform ND ug/L 02/25/15 18:25 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/25/15 18:25 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/25/15 18:25 78-93-31000.96 1
Carbon disulfide ND ug/L 02/25/15 18:25 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/25/15 18:25 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/25/15 18:25 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/25/15 18:25 75-00-310.0 0.54 1
Chloroform ND ug/L 02/25/15 18:25 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/25/15 18:25 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/25/15 18:25 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/25/15 18:25 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/25/15 18:25 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/25/15 18:25 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/25/15 18:25 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/25/15 18:25 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/25/15 18:25 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/25/15 18:25 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/25/15 18:25 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/25/15 18:25 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/25/15 18:25 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/25/15 18:25 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/25/15 18:25 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/25/15 18:25 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/25/15 18:25 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Sample:SW-3 Lab ID:92237753002 Collected:02/11/15 17:25 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/25/15 18:25 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/25/15 18:25 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/25/15 18:25 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/25/15 18:25 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/25/15 18:25 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/25/15 18:25 108-10-11000.33 1
Styrene ND ug/L 02/25/15 18:25 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/25/15 18:25 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/25/15 18:25 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/25/15 18:25 127-18-41.0 0.46 1
Toluene ND ug/L 02/25/15 18:25 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/25/15 18:25 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/25/15 18:25 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/25/15 18:25 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/25/15 18:25 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/25/15 18:25 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/25/15 18:25 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/25/15 18:25 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/25/15 18:25 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %02/25/15 18:25 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %02/25/15 18:25 17060-07-070-130 1
Toluene-d8 (S)94 %02/25/15 18:25 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Sample:SW-1 Lab ID:92237753003 Collected:02/11/15 17:35 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/19/15 00:43 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/19/15 00:43 7440-38-202/16/15 16:1010.0 2.5 1
Barium 63.3J ug/L 02/19/15 00:43 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/19/15 00:43 7440-41-702/16/15 16:101.0 0.50 1
Cadmium ND ug/L 02/19/15 00:43 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/19/15 00:43 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/19/15 00:43 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/19/15 00:43 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/19/15 00:43 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/19/15 00:43 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/19/15 00:43 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/19/15 00:43 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/19/15 00:43 7440-28-002/16/15 16:105.5 5.0 1
Vanadium ND ug/L 02/19/15 00:43 7440-62-202/16/15 16:1025.0 2.5 1
Zinc 5.8J ug/L 02/19/15 00:43 7440-66-602/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/25/15 18:42 67-64-110010.0 1
Acrylonitrile ND ug/L 02/25/15 18:42 107-13-12001.9 1
Benzene ND ug/L 02/25/15 18:42 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/25/15 18:42 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/25/15 18:42 75-27-41.0 0.18 1
Bromoform ND ug/L 02/25/15 18:42 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/25/15 18:42 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/25/15 18:42 78-93-31000.96 1
Carbon disulfide ND ug/L 02/25/15 18:42 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/25/15 18:42 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/25/15 18:42 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/25/15 18:42 75-00-310.0 0.54 1
Chloroform ND ug/L 02/25/15 18:42 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/25/15 18:42 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/25/15 18:42 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/25/15 18:42 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/25/15 18:42 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/25/15 18:42 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/25/15 18:42 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/25/15 18:42 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/25/15 18:42 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/25/15 18:42 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/25/15 18:42 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/25/15 18:42 75-35-45.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 02/25/15 18:42 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/25/15 18:42 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/25/15 18:42 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/25/15 18:42 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/25/15 18:42 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Sample:SW-1 Lab ID:92237753003 Collected:02/11/15 17:35 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/25/15 18:42 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/25/15 18:42 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/25/15 18:42 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/25/15 18:42 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/25/15 18:42 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/25/15 18:42 108-10-11000.33 1
Styrene ND ug/L 02/25/15 18:42 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/25/15 18:42 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/25/15 18:42 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/25/15 18:42 127-18-41.0 0.46 1
Toluene ND ug/L 02/25/15 18:42 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/25/15 18:42 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/25/15 18:42 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/25/15 18:42 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/25/15 18:42 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/25/15 18:42 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/25/15 18:42 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/25/15 18:42 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/25/15 18:42 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)99 %02/25/15 18:42 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %02/25/15 18:42 17060-07-070-130 1
Toluene-d8 (S)94 %02/25/15 18:42 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/17907
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92237753001, 92237753002, 92237753003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1392765
Associated Lab Samples:92237753001, 92237753002, 92237753003
Matrix:Water
Analyzed
Antimony ug/L ND 6.0 02/18/15 23:26
Arsenic ug/L ND 10.0 02/18/15 23:26
Barium ug/L ND 100 02/18/15 23:26
Beryllium ug/L ND 1.0 02/18/15 23:26
Cadmium ug/L ND 1.0 02/18/15 23:26
Chromium ug/L ND 10.0 02/18/15 23:26
Cobalt ug/L ND 10.0 02/18/15 23:26
Copper ug/L ND 10.0 02/18/15 23:26
Lead ug/L ND 10.0 02/18/15 23:26
Nickel ug/L ND 50.0 02/18/15 23:26
Selenium ug/L ND 10.0 02/18/15 23:26
Silver ug/L ND 10.0 02/18/15 23:26
Thallium ug/L ND 5.5 02/18/15 23:26
Vanadium ug/L ND 25.0 02/18/15 23:26
Zinc ug/L ND 10.0 02/18/15 23:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1392766LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 477500 95 80-120
Arsenic ug/L 464500 93 80-120
Barium ug/L 484500 97 80-120
Beryllium ug/L 480500 96 80-120
Cadmium ug/L 486500 97 80-120
Chromium ug/L 500500 100 80-120
Cobalt ug/L 490500 98 80-120
Copper ug/L 483500 97 80-120
Lead ug/L 490500 98 80-120
Nickel ug/L 480500 96 80-120
Selenium ug/L 465500 93 80-120
Silver ug/L 246250 98 80-120
Thallium ug/L 440500 88 80-120
Vanadium ug/L 471500 94 80-120
Zinc ug/L 466500 93 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1392767MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237748001
1392768
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 96 75-12598 2 25500ND479490
Arsenic ug/L 500 92 75-12595 3 25500ND462474
Barium ug/L 500 99 75-125101 3 25500ND493507
Beryllium ug/L 500 98 75-125101 3 25500ND490505
Cadmium ug/L 500 98 75-125100 3 25500ND488501
Chromium ug/L 500 102 75-125105 3 25500ND510525
Cobalt ug/L 500 99 75-125102 3 25500ND497511
Copper ug/L 500 98 75-125101 3 25500ND493507
Lead ug/L 500 99 75-125102 2 25500ND496509
Nickel ug/L 500 97 75-125100 3 25500ND486499
Selenium ug/L 500 92 75-12594 2 25500ND462470
Silver ug/L 250 99 75-125101 2 25250ND248254
Thallium ug/L 500 89 75-12592 4 25500ND448465
Vanadium ug/L 500 97 75-125100 3 25500ND486500
Zinc ug/L 500 93 75-12595 2 25500ND469479
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/30489
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92237753001, 92237753002, 92237753003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1397928
Associated Lab Samples:92237753001, 92237753002, 92237753003
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 5.0 02/25/15 17:18
1,1,1-Trichloroethane ug/L ND 1.0 02/25/15 17:18
1,1,2,2-Tetrachloroethane ug/L ND 3.0 02/25/15 17:18
1,1,2-Trichloroethane ug/L ND 1.0 02/25/15 17:18
1,1-Dichloroethane ug/L ND 5.0 02/25/15 17:18
1,1-Dichloroethene ug/L ND 5.0 02/25/15 17:18
1,2,3-Trichloropropane ug/L ND 1.0 02/25/15 17:18
1,2-Dibromo-3-chloropropane ug/L ND 13.0 02/25/15 17:18
1,2-Dibromoethane (EDB)ug/L ND 1.0 02/25/15 17:18
1,2-Dichlorobenzene ug/L ND 5.0 02/25/15 17:18
1,2-Dichloroethane ug/L ND 1.0 02/25/15 17:18
1,2-Dichloropropane ug/L ND 1.0 02/25/15 17:18
1,3-Dichloropropane ug/L ND 1.0 02/25/15 17:18
1,4-Dichlorobenzene ug/L ND 1.0 02/25/15 17:18
2-Butanone (MEK)ug/L ND 100 02/25/15 17:18
2-Hexanone ug/L ND 50.0 02/25/15 17:18
4-Methyl-2-pentanone (MIBK)ug/L ND 100 02/25/15 17:18
Acetone ug/L ND 100 02/25/15 17:18
Acrylonitrile ug/L ND 200 02/25/15 17:18
Benzene ug/L ND 1.0 02/25/15 17:18
Bromochloromethane ug/L ND 3.0 02/25/15 17:18
Bromodichloromethane ug/L ND 1.0 02/25/15 17:18
Bromoform ug/L ND 3.0 02/25/15 17:18
Bromomethane ug/L ND 10.0 02/25/15 17:18
Carbon disulfide ug/L ND 100 02/25/15 17:18
Carbon tetrachloride ug/L ND 1.0 02/25/15 17:18
Chlorobenzene ug/L ND 3.0 02/25/15 17:18
Chloroethane ug/L ND 10.0 02/25/15 17:18
Chloroform ug/L ND 5.0 02/25/15 17:18
Chloromethane ug/L ND 1.0 02/25/15 17:18
cis-1,2-Dichloroethene ug/L ND 5.0 02/25/15 17:18
cis-1,3-Dichloropropene ug/L ND 1.0 02/25/15 17:18
Dibromochloromethane ug/L ND 3.0 02/25/15 17:18
Dibromomethane ug/L ND 10.0 02/25/15 17:18
Ethylbenzene ug/L ND 1.0 02/25/15 17:18
Iodomethane ug/L ND 10.0 02/25/15 17:18
Methylene Chloride ug/L ND 1.0 02/25/15 17:18
Styrene ug/L ND 1.0 02/25/15 17:18
Tetrachloroethene ug/L ND 1.0 02/25/15 17:18
Toluene ug/L ND 1.0 02/25/15 17:18
trans-1,2-Dichloroethene ug/L ND 5.0 02/25/15 17:18
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1397928
Associated Lab Samples:92237753001, 92237753002, 92237753003
Matrix:Water
Analyzed
trans-1,3-Dichloropropene ug/L ND 1.0 02/25/15 17:18
trans-1,4-Dichloro-2-butene ug/L ND 100 02/25/15 17:18
Trichloroethene ug/L ND 1.0 02/25/15 17:18
Trichlorofluoromethane ug/L ND 1.0 02/25/15 17:18
Vinyl acetate ug/L ND 50.0 02/25/15 17:18
Vinyl chloride ug/L ND 1.0 02/25/15 17:18
Xylene (Total)ug/L ND 5.0 02/25/15 17:18
1,2-Dichloroethane-d4 (S)%99 70-130 02/25/15 17:18
4-Bromofluorobenzene (S)%99 70-130 02/25/15 17:18
Toluene-d8 (S)%95 70-130 02/25/15 17:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1397929LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 47.050 94 80-125
1,1,1-Trichloroethane ug/L 48.350 97 71-129
1,1,2,2-Tetrachloroethane ug/L 46.450 93 79-124
1,1,2-Trichloroethane ug/L 48.350 97 85-125
1,1-Dichloroethane ug/L 48.250 96 73-126
1,1-Dichloroethene ug/L 46.450 93 66-135
1,2,3-Trichloropropane ug/L 48.150 96 75-130
1,2-Dibromo-3-chloropropane ug/L 46.550 93 71-133
1,2-Dibromoethane (EDB)ug/L 50.150 100 83-124
1,2-Dichlorobenzene ug/L 49.150 98 80-133
1,2-Dichloroethane ug/L 49.250 98 67-128
1,2-Dichloropropane ug/L 48.750 97 75-132
1,3-Dichloropropane ug/L 47.850 96 76-131
1,4-Dichlorobenzene ug/L 48.650 97 78-130
2-Butanone (MEK)ug/L 104100 104 61-144
2-Hexanone ug/L 93.8100 94 68-143
4-Methyl-2-pentanone (MIBK)ug/L 98.0J100 98 72-135
Acetone ug/L 105100 105 48-146
Acrylonitrile ug/L 258250 103 40-160
Benzene ug/L 49.850 100 80-125
Bromochloromethane ug/L 46.650 93 71-125
Bromodichloromethane ug/L 44.650 89 78-124
Bromoform ug/L 42.750 85 71-128
Bromomethane ug/L 44.450 89 40-160
Carbon disulfide ug/L 40.4J50 81 50-160
Carbon tetrachloride ug/L 48.450 97 69-131
Chlorobenzene ug/L 47.250 94 81-122
Chloroethane ug/L 36.850 74 39-148
Chloroform ug/L 44.250 88 73-127
Chloromethane ug/L 48.150 96 44-146
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
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Huntersville, NC 28078
[phone]
Page 14 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1397929LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 49.350 99 74-124
cis-1,3-Dichloropropene ug/L 47.450 95 72-132
Dibromochloromethane ug/L 43.850 88 78-125
Dibromomethane ug/L 48.450 97 82-120
Ethylbenzene ug/L 47.650 95 79-121
Iodomethane ug/L 100100 100 39-154
Methylene Chloride ug/L 53.050 106 64-133
Styrene ug/L 48.550 97 84-126
Tetrachloroethene ug/L 47.550 95 78-122
Toluene ug/L 48.550 97 80-121
trans-1,2-Dichloroethene ug/L 48.650 97 71-127
trans-1,3-Dichloropropene ug/L 47.350 95 69-141
trans-1,4-Dichloro-2-butene ug/L 49.5J50 99 40-160
Trichloroethene ug/L 48.850 98 78-122
Trichlorofluoromethane ug/L 54.850 110 53-137
Vinyl acetate ug/L 108100 108 40-160
Vinyl chloride ug/L 42.650 85 58-137
Xylene (Total)ug/L 143150 95 81-126
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1398024MATRIX SPIKE SAMPLE:
MSSpike
Result
92238381004
1,1,1,2-Tetrachloroethane ug/L 42.640 107 70-130ND
1,1,1-Trichloroethane ug/L 45.740 114 70-130ND
1,1,2,2-Tetrachloroethane ug/L 39.940 100 70-130ND
1,1,2-Trichloroethane ug/L 42.540 106 70-130ND
1,1-Dichloroethane ug/L 43.140 108 70-130ND
1,1-Dichloroethene ug/L 45.140 113 70-166ND
1,2,3-Trichloropropane ug/L 41.440 103 70-130ND
1,2-Dibromo-3-chloropropane ug/L 38.440 96 70-130ND
1,2-Dibromoethane (EDB)ug/L 43.640 109 70-130ND
1,2-Dichlorobenzene ug/L 43.040 107 70-130ND
1,2-Dichloroethane ug/L 44.340 111 70-130ND
1,2-Dichloropropane ug/L 41.740 104 70-130ND
1,3-Dichloropropane ug/L 42.140 105 70-130ND
1,4-Dichlorobenzene ug/L 43.140 108 70-130ND
2-Butanone (MEK)ug/L 86.6J80 108 70-130ND
2-Hexanone ug/L 79.980 100 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 82.5J80 103 70-130ND
Acetone ug/L 86.6J80 104 70-130ND
Acrylonitrile ug/L 227200 113 70-130ND
Benzene ug/L 44.840 112 70-148ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
[phone]
Page 15 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1398024MATRIX SPIKE SAMPLE:
MSSpike
Result
92238381004
Bromochloromethane ug/L 43.240 108 70-130ND
Bromodichloromethane ug/L 39.340 98 70-130ND
Bromoform ug/L 36.240 90 70-130ND
Bromomethane ug/L 36.440 91 70-130ND
Carbon disulfide ug/L 36.6J40 92 70-130ND
Carbon tetrachloride ug/L 45.740 114 70-130ND
Chlorobenzene ug/L 42.140 105 70-146ND
Chloroethane ug/L 35.140 88 70-130ND
Chloroform ug/L 40.140 100 70-130ND
Chloromethane ug/L 41.740 104 70-130ND
cis-1,2-Dichloroethene ug/L 44.240 111 70-130ND
cis-1,3-Dichloropropene ug/L 38.840 97 70-130ND
Dibromochloromethane ug/L 38.440 96 70-130ND
Dibromomethane ug/L 41.840 104 70-130ND
Ethylbenzene ug/L 42.840 107 70-130ND
Iodomethane ug/L 85.080 106 70-130ND
Methylene Chloride ug/L 47.840 120 70-130ND
Styrene ug/L 42.740 107 70-130ND
Tetrachloroethene ug/L 42.040 105 70-130ND
Toluene ug/L 42.940 107 70-155ND
trans-1,2-Dichloroethene ug/L 44.840 112 70-130ND
trans-1,3-Dichloropropene ug/L 40.040 100 70-130ND
trans-1,4-Dichloro-2-butene ug/L 39.4J40 99 70-130ND
Trichloroethene ug/L 43.740 109 69-151ND
Trichlorofluoromethane ug/L 52.040 130 70-130ND
Vinyl acetate ug/L 70.680 88 70-130ND
Vinyl chloride ug/L 37.940 95 70-130ND
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1398900MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237647005
1398901
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 103 70-130103 0 3020ND20.6 20.5
1,1,1-Trichloroethane ug/L 20 109 70-130111 1 3020ND21.9 22.1
1,1,2,2-Tetrachloroethane ug/L 20 98 70-13098 1 3020ND19.6 19.5
1,1,2-Trichloroethane ug/L 20 103 70-130103 0 3020ND20.5 20.6
1,1-Dichloroethane ug/L 20 104 70-130106 2 3020ND20.8 21.2
1,1-Dichloroethene ug/L 20 105 70-166111 6 3020ND20.9 22.1
1,2,3-Trichloropropane ug/L 20 106 70-130107 0 3020ND21.2 21.3
1,2-Dibromo-3-
chloropropane ug/L 20 95 70-13093 2 3020ND18.9 18.6
1,2-Dibromoethane (EDB)ug/L 20 102 70-130104 2 3020ND20.4 20.8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1398900MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237647005
1398901
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2-Dichlorobenzene ug/L 20 106 70-130105 1 3020ND21.2 21.0
1,2-Dichloroethane ug/L 20 105 70-130105 0 3020ND20.9 20.9
1,2-Dichloropropane ug/L 20 100 70-130101 1 3020ND19.9 20.1
1,3-Dichloropropane ug/L 20 100 70-130101 0 3020ND20.1 20.1
1,4-Dichlorobenzene ug/L 20 106 70-130107 1 3020ND21.2 21.4
2-Butanone (MEK)ug/L 40 104 70-130100 4 3040ND41.4J 40.0J
2-Hexanone ug/L 40 103 70-130101 2 3040ND41.3J 40.5J
4-Methyl-2-pentanone
(MIBK)ug/L 40 103 70-130103 0 3040ND41.1J 41.1J
Acetone ug/L 40 115 70-130109 5 3040ND45.9J 43.5J
Acrylonitrile ug/L 100 114 70-130113 1 30100ND114J113J
Benzene ug/L 20 110 70-148112 2 3020ND22.0 22.4
Bromochloromethane ug/L 20 100 70-130106 6 3020ND20.1 21.3
Bromodichloromethane ug/L 20 93 70-13094 0 3020ND18.6 18.7
Bromoform ug/L 20 88 70-13087 1 3020ND17.6 17.4
Bromomethane ug/L 20 75 70-13087 15 3020ND15.0 17.4
Carbon disulfide ug/L 20 88 70-13089 1 3020ND17.6J 17.9J
Carbon tetrachloride ug/L 20 115 70-130114 1 3020ND23.1 22.8
Chlorobenzene ug/L 20 104 70-146103 1 3020ND20.8 20.6
Chloroethane ug/L 20 89 70-13094 5 3020ND17.9 18.7
Chloroform ug/L 20 93 70-13097 4 3020ND18.7 19.4
Chloromethane ug/L 20 105 70-130104 1 3020ND21.1 20.8
cis-1,2-Dichloroethene ug/L 20 105 70-130106 1 3020ND21.0 21.2
cis-1,3-Dichloropropene ug/L 20 88 70-13089 1 3020ND17.6 17.8
Dibromochloromethane ug/L 20 90 70-13090 0 3020ND17.9 18.0
Dibromomethane ug/L 20 99 70-13099 1 3020ND19.7 19.9
Ethylbenzene ug/L 20 105 70-130107 1 3020ND21.1 21.4
Iodomethane ug/L 40 90 70-13098 8 3040ND35.9 39.1
Methylene Chloride ug/L 20 115 70-130115 0 3020ND22.9 23.0
Styrene ug/L 20 99 70-13099 0 3020ND19.8 19.8
Tetrachloroethene ug/L 20 101 70-130101 0 3020ND20.2 20.2
Toluene ug/L 20 105 70-155106 1 3020ND21.0 21.2
trans-1,2-Dichloroethene ug/L 20 106 70-130104 1 3020ND21.1 20.9
trans-1,3-Dichloropropene ug/L 20 92 70-13091 1 3020ND18.4 18.3
trans-1,4-Dichloro-2-butene ug/L 20 104 70-13099 5 3020ND20.9J 19.8J
Trichloroethene ug/L 20 109 69-151109 1 3020ND21.9 21.7
Trichlorofluoromethane ug/L M02013570-130130 4 3020ND27.1 25.9
Vinyl acetate ug/L 40 80 70-13082 3 3040ND31.9J 32.8J
Vinyl chloride ug/L 20 91 70-13093 2 3020ND18.2 18.5
1,2-Dichloroethane-d4 (S)%97 70-13099
4-Bromofluorobenzene (S)%H59370-13092
Toluene-d8 (S)%98 70-13097
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92238381003
1398023SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Acrylonitrile ug/L ND 30ND
Benzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon disulfide ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Iodomethane ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
trans-1,4-Dichloro-2-butene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
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Huntersville, NC 28078
[phone]
Page 18 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92238381003
1398023SAMPLE DUPLICATE:
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%101 3104
4-Bromofluorobenzene (S)%100 298
Toluene-d8 (S)%94 194
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 23
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Reanalysis conducted in excess of EPA method holding time. Results confirm original analysis performed in hold time.H5
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
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Huntersville, NC 28078
[phone]
Page 20 of 23
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92237753
Wayne MSWLF-SWs
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92237753001 MPRP/17907 ICP/16106SW-2 EPA 3010 EPA 6010
92237753002 MPRP/17907 ICP/16106SW-3 EPA 3010 EPA 6010
92237753003 MPRP/17907 ICP/16106SW-1 EPA 3010 EPA 6010
92237753001 MSV/30489SW-2 EPA 8260
92237753002 MSV/30489SW-3 EPA 8260
92237753003 MSV/30489SW-1 EPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/27/2015 04:05 PM
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Huntersville, NC 28078
[phone]
Page 21 of 23
Page 22 of 23
Page 23 of 23
#=CL#
March 04, 2015
LIMS USE: FR - JONATHAN PFOHL
LIMS OBJECT ID: 92237748
92237748
Project:
Pace Project No.:
RE:
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
Wayne MSWLF Blanks
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on February 13, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Report revised 3/4/15 to remove false positive 1,2-Dichloroethane detection from Method Blank
#30436.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 20
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 20
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
Lab ID Sample ID Matrix Date Collected Date Received
92237748001 EB Water 02/12/15 17:15 02/13/15 15:45
92237748002 FB Water 02/12/15 17:30 02/13/15 15:45
92237748003 TB Water 02/12/15 00:00 02/13/15 15:45
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 20
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92237748001 EB EPA 6010 15 PASI-ASH1
EPA 8260 51 PASI-CGAW
92237748002 FB EPA 6010 15 PASI-ASH1
EPA 8260 51 PASI-CGAW
92237748003 TB EPA 8260 51 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
Sample:EB Lab ID:92237748001 Collected:02/12/15 17:15 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/18/15 23:32 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/18/15 23:32 7440-38-202/16/15 16:1010.0 2.5 1
Barium ND ug/L 02/18/15 23:32 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/18/15 23:32 7440-41-702/16/15 16:101.0 0.50 1
Cadmium ND ug/L 02/18/15 23:32 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/18/15 23:32 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/18/15 23:32 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/18/15 23:32 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/18/15 23:32 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/18/15 23:32 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/18/15 23:32 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/18/15 23:32 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/18/15 23:32 7440-28-002/16/15 16:105.5 5.0 1
Vanadium ND ug/L 02/18/15 23:32 7440-62-202/16/15 16:1025.0 2.5 1
Zinc ND ug/L 02/18/15 23:32 7440-66-602/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/22/15 14:23 67-64-110010.0 1
Acrylonitrile ND ug/L 02/22/15 14:23 107-13-12001.9 1
Benzene ND ug/L 02/22/15 14:23 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/22/15 14:23 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/22/15 14:23 75-27-41.0 0.18 1
Bromoform ND ug/L 02/22/15 14:23 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/22/15 14:23 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/22/15 14:23 78-93-31000.96 1
Carbon disulfide ND ug/L 02/22/15 14:23 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/22/15 14:23 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/22/15 14:23 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/22/15 14:23 75-00-310.0 0.54 1
Chloroform ND ug/L 02/22/15 14:23 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/22/15 14:23 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/22/15 14:23 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/22/15 14:23 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/22/15 14:23 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/22/15 14:23 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/22/15 14:23 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/22/15 14:23 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/22/15 14:23 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/22/15 14:23 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/22/15 14:23 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/22/15 14:23 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.47J ug/L 02/22/15 14:23 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/22/15 14:23 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/22/15 14:23 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/22/15 14:23 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/22/15 14:23 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 04:53 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
Sample:EB Lab ID:92237748001 Collected:02/12/15 17:15 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/22/15 14:23 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/22/15 14:23 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/22/15 14:23 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/22/15 14:23 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/22/15 14:23 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/22/15 14:23 108-10-11000.33 1
Styrene ND ug/L 02/22/15 14:23 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/22/15 14:23 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/22/15 14:23 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/22/15 14:23 127-18-41.0 0.46 1
Toluene ND ug/L 02/22/15 14:23 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/22/15 14:23 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/22/15 14:23 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/22/15 14:23 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/22/15 14:23 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/22/15 14:23 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/22/15 14:23 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/22/15 14:23 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/22/15 14:23 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %02/22/15 14:23 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %02/22/15 14:23 17060-07-070-130 1
Toluene-d8 (S)99 %02/22/15 14:23 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 04:53 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
Sample:FB Lab ID:92237748002 Collected:02/12/15 17:30 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 30106010 ICP Groundwater
Antimony ND ug/L 02/18/15 23:51 7440-36-002/16/15 16:106.0 3.8 1
Arsenic ND ug/L 02/18/15 23:51 7440-38-202/16/15 16:1010.0 2.5 1
Barium ND ug/L 02/18/15 23:51 7440-39-302/16/15 16:101002.5 1
Beryllium ND ug/L 02/18/15 23:51 7440-41-702/16/15 16:101.0 0.50 1
Cadmium ND ug/L 02/18/15 23:51 7440-43-902/16/15 16:101.0 0.50 1
Chromium ND ug/L 02/18/15 23:51 7440-47-302/16/15 16:1010.0 2.5 1
Cobalt ND ug/L 02/18/15 23:51 7440-48-402/16/15 16:1010.0 2.5 1
Copper ND ug/L 02/18/15 23:51 7440-50-802/16/15 16:1010.0 2.5 1
Lead ND ug/L 02/18/15 23:51 7439-92-102/16/15 16:1010.0 2.5 1
Nickel ND ug/L 02/18/15 23:51 7440-02-002/16/15 16:1050.0 2.5 1
Selenium ND ug/L 02/18/15 23:51 7782-49-202/16/15 16:1010.0 5.0 1
Silver ND ug/L 02/18/15 23:51 7440-22-402/16/15 16:1010.0 2.5 1
Thallium ND ug/L 02/18/15 23:51 7440-28-002/16/15 16:105.5 5.0 1
Vanadium ND ug/L 02/18/15 23:51 7440-62-202/16/15 16:1025.0 2.5 1
Zinc ND ug/L 02/18/15 23:51 7440-66-602/16/15 16:1010.0 5.0 1
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/22/15 14:40 67-64-110010.0 1
Acrylonitrile ND ug/L 02/22/15 14:40 107-13-12001.9 1
Benzene ND ug/L 02/22/15 14:40 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/22/15 14:40 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/22/15 14:40 75-27-41.0 0.18 1
Bromoform ND ug/L 02/22/15 14:40 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/22/15 14:40 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/22/15 14:40 78-93-31000.96 1
Carbon disulfide ND ug/L 02/22/15 14:40 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/22/15 14:40 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/22/15 14:40 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/22/15 14:40 75-00-310.0 0.54 1
Chloroform ND ug/L 02/22/15 14:40 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/22/15 14:40 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/22/15 14:40 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/22/15 14:40 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/22/15 14:40 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/22/15 14:40 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/22/15 14:40 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/22/15 14:40 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/22/15 14:40 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/22/15 14:40 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/22/15 14:40 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/22/15 14:40 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.37J ug/L 02/22/15 14:40 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/22/15 14:40 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/22/15 14:40 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/22/15 14:40 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/22/15 14:40 10061-01-51.0 0.13 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 04:53 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
Sample:FB Lab ID:92237748002 Collected:02/12/15 17:30 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
trans-1,3-Dichloropropene ND ug/L 02/22/15 14:40 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/22/15 14:40 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/22/15 14:40 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/22/15 14:40 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/22/15 14:40 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/22/15 14:40 108-10-11000.33 1
Styrene ND ug/L 02/22/15 14:40 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/22/15 14:40 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/22/15 14:40 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/22/15 14:40 127-18-41.0 0.46 1
Toluene ND ug/L 02/22/15 14:40 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/22/15 14:40 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/22/15 14:40 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/22/15 14:40 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/22/15 14:40 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/22/15 14:40 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/22/15 14:40 108-05-450.0 0.35 1
Vinyl chloride ND ug/L 02/22/15 14:40 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/22/15 14:40 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)98 %02/22/15 14:40 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %02/22/15 14:40 17060-07-070-130 1
Toluene-d8 (S)99 %02/22/15 14:40 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 04:53 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
Sample:TB Lab ID:92237748003 Collected:02/12/15 00:00 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Acetone ND ug/L 02/22/15 14:57 67-64-110010.0 1
Acrylonitrile ND ug/L 02/22/15 14:57 107-13-12001.9 1
Benzene ND ug/L 02/22/15 14:57 71-43-21.0 0.25 1
Bromochloromethane ND ug/L 02/22/15 14:57 74-97-53.0 0.17 1
Bromodichloromethane ND ug/L 02/22/15 14:57 75-27-41.0 0.18 1
Bromoform ND ug/L 02/22/15 14:57 75-25-23.0 0.26 1
Bromomethane ND ug/L 02/22/15 14:57 74-83-910.0 0.29 1
2-Butanone (MEK)ND ug/L 02/22/15 14:57 78-93-31000.96 1
Carbon disulfide ND ug/L 02/22/15 14:57 75-15-01001.2 1
Carbon tetrachloride ND ug/L 02/22/15 14:57 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 02/22/15 14:57 108-90-73.0 0.23 1
Chloroethane ND ug/L 02/22/15 14:57 75-00-310.0 0.54 1
Chloroform ND ug/L 02/22/15 14:57 67-66-35.0 0.14 1
Chloromethane ND ug/L 02/22/15 14:57 74-87-31.0 0.11 1
1,2-Dibromo-3-chloropropane ND ug/L 02/22/15 14:57 96-12-813.0 2.0 1
Dibromochloromethane ND ug/L 02/22/15 14:57 124-48-13.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 02/22/15 14:57 106-93-41.0 0.27 1
Dibromomethane ND ug/L 02/22/15 14:57 74-95-310.0 0.21 1
1,2-Dichlorobenzene ND ug/L 02/22/15 14:57 95-50-15.0 0.30 1
1,4-Dichlorobenzene ND ug/L 02/22/15 14:57 106-46-71.0 0.33 1
trans-1,4-Dichloro-2-butene ND ug/L 02/22/15 14:57 110-57-61001.0 1
1,1-Dichloroethane ND ug/L 02/22/15 14:57 75-34-35.0 0.32 1
1,2-Dichloroethane ND ug/L 02/22/15 14:57 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 02/22/15 14:57 75-35-45.0 0.56 1
cis-1,2-Dichloroethene 0.31J ug/L 02/22/15 14:57 156-59-25.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 02/22/15 14:57 156-60-55.0 0.49 1
1,2-Dichloropropane ND ug/L 02/22/15 14:57 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 02/22/15 14:57 142-28-91.0 0.28 1
cis-1,3-Dichloropropene ND ug/L 02/22/15 14:57 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 02/22/15 14:57 10061-02-61.0 0.26 1
Ethylbenzene ND ug/L 02/22/15 14:57 100-41-41.0 0.30 1
2-Hexanone ND ug/L 02/22/15 14:57 591-78-650.0 0.46 1
Iodomethane ND ug/L 02/22/15 14:57 74-88-410.0 0.32 1
Methylene Chloride ND ug/L 02/22/15 14:57 75-09-21.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/22/15 14:57 108-10-11000.33 1
Styrene ND ug/L 02/22/15 14:57 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 02/22/15 14:57 630-20-65.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 02/22/15 14:57 79-34-53.0 0.40 1
Tetrachloroethene ND ug/L 02/22/15 14:57 127-18-41.0 0.46 1
Toluene ND ug/L 02/22/15 14:57 108-88-31.0 0.26 1
1,1,1-Trichloroethane ND ug/L 02/22/15 14:57 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 02/22/15 14:57 79-00-51.0 0.29 1
Trichloroethene ND ug/L 02/22/15 14:57 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 02/22/15 14:57 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 02/22/15 14:57 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 02/22/15 14:57 108-05-450.0 0.35 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 04:53 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
Sample:TB Lab ID:92237748003 Collected:02/12/15 00:00 Received:02/13/15 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level Landfill
Vinyl chloride ND ug/L 02/22/15 14:57 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 02/22/15 14:57 1330-20-75.0 0.66 1
Surrogates
4-Bromofluorobenzene (S)97 %02/22/15 14:57 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %02/22/15 14:57 17060-07-070-130 1
Toluene-d8 (S)99 %02/22/15 14:57 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 04:53 PM
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Page 10 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/17907
EPA 3010
EPA 6010
6010 MET NC Groundwater
Associated Lab Samples:92237748001, 92237748002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1392765
Associated Lab Samples:92237748001, 92237748002
Matrix:Water
Analyzed
Antimony ug/L ND 6.0 02/18/15 23:26
Arsenic ug/L ND 10.0 02/18/15 23:26
Barium ug/L ND 100 02/18/15 23:26
Beryllium ug/L ND 1.0 02/18/15 23:26
Cadmium ug/L ND 1.0 02/18/15 23:26
Chromium ug/L ND 10.0 02/18/15 23:26
Cobalt ug/L ND 10.0 02/18/15 23:26
Copper ug/L ND 10.0 02/18/15 23:26
Lead ug/L ND 10.0 02/18/15 23:26
Nickel ug/L ND 50.0 02/18/15 23:26
Selenium ug/L ND 10.0 02/18/15 23:26
Silver ug/L ND 10.0 02/18/15 23:26
Thallium ug/L ND 5.5 02/18/15 23:26
Vanadium ug/L ND 25.0 02/18/15 23:26
Zinc ug/L ND 10.0 02/18/15 23:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1392766LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 477500 95 80-120
Arsenic ug/L 464500 93 80-120
Barium ug/L 484500 97 80-120
Beryllium ug/L 480500 96 80-120
Cadmium ug/L 486500 97 80-120
Chromium ug/L 500500 100 80-120
Cobalt ug/L 490500 98 80-120
Copper ug/L 483500 97 80-120
Lead ug/L 490500 98 80-120
Nickel ug/L 480500 96 80-120
Selenium ug/L 465500 93 80-120
Silver ug/L 246250 98 80-120
Thallium ug/L 440500 88 80-120
Vanadium ug/L 471500 94 80-120
Zinc ug/L 466500 93 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 04:53 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1392767MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237748001
1392768
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 500 96 75-12598 2 25500ND479490
Arsenic ug/L 500 92 75-12595 3 25500ND462474
Barium ug/L 500 99 75-125101 3 25500ND493507
Beryllium ug/L 500 98 75-125101 3 25500ND490505
Cadmium ug/L 500 98 75-125100 3 25500ND488501
Chromium ug/L 500 102 75-125105 3 25500ND510525
Cobalt ug/L 500 99 75-125102 3 25500ND497511
Copper ug/L 500 98 75-125101 3 25500ND493507
Lead ug/L 500 99 75-125102 2 25500ND496509
Nickel ug/L 500 97 75-125100 3 25500ND486499
Selenium ug/L 500 92 75-12594 2 25500ND462470
Silver ug/L 250 99 75-125101 2 25250ND248254
Thallium ug/L 500 89 75-12592 4 25500ND448465
Vanadium ug/L 500 97 75-125100 3 25500ND486500
Zinc ug/L 500 93 75-12595 2 25500ND469479
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 04:53 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 12 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/30436
EPA 8260
EPA 8260
8260 MSV Low Level Landfill
Associated Lab Samples:92237748001, 92237748002, 92237748003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1395932
Associated Lab Samples:92237748001, 92237748002, 92237748003
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 5.0 02/22/15 12:24
1,1,1-Trichloroethane ug/L ND 1.0 02/22/15 12:24
1,1,2,2-Tetrachloroethane ug/L ND 3.0 02/22/15 12:24
1,1,2-Trichloroethane ug/L ND 1.0 02/22/15 12:24
1,1-Dichloroethane ug/L ND 5.0 02/22/15 12:24
1,1-Dichloroethene ug/L ND 5.0 02/22/15 12:24
1,2,3-Trichloropropane ug/L ND 1.0 02/22/15 12:24
1,2-Dibromo-3-chloropropane ug/L ND 13.0 02/22/15 12:24
1,2-Dibromoethane (EDB)ug/L ND 1.0 02/22/15 12:24
1,2-Dichlorobenzene ug/L ND 5.0 02/22/15 12:24
1,2-Dichloroethane ug/L ND 1.0 02/22/15 12:24
1,2-Dichloropropane ug/L ND 1.0 02/22/15 12:24
1,3-Dichloropropane ug/L ND 1.0 02/22/15 12:24
1,4-Dichlorobenzene ug/L ND 1.0 02/22/15 12:24
2-Butanone (MEK)ug/L ND 100 02/22/15 12:24
2-Hexanone ug/L ND 50.0 02/22/15 12:24
4-Methyl-2-pentanone (MIBK)ug/L ND 100 02/22/15 12:24
Acetone ug/L ND 100 02/22/15 12:24
Acrylonitrile ug/L ND 200 02/22/15 12:24
Benzene ug/L ND 1.0 02/22/15 12:24
Bromochloromethane ug/L ND 3.0 02/22/15 12:24
Bromodichloromethane ug/L ND 1.0 02/22/15 12:24
Bromoform ug/L ND 3.0 02/22/15 12:24
Bromomethane ug/L ND 10.0 02/22/15 12:24
Carbon disulfide ug/L ND 100 02/22/15 12:24
Carbon tetrachloride ug/L ND 1.0 02/22/15 12:24
Chlorobenzene ug/L ND 3.0 02/22/15 12:24
Chloroethane ug/L ND 10.0 02/22/15 12:24
Chloroform ug/L ND 5.0 02/22/15 12:24
Chloromethane ug/L ND 1.0 02/22/15 12:24
cis-1,2-Dichloroethene ug/L ND 5.0 02/22/15 12:24
cis-1,3-Dichloropropene ug/L ND 1.0 02/22/15 12:24
Dibromochloromethane ug/L ND 3.0 02/22/15 12:24
Dibromomethane ug/L ND 10.0 02/22/15 12:24
Ethylbenzene ug/L ND 1.0 02/22/15 12:24
Iodomethane ug/L ND 10.0 02/22/15 12:24
Methylene Chloride ug/L ND 1.0 02/22/15 12:24
Styrene ug/L ND 1.0 02/22/15 12:24
Tetrachloroethene ug/L ND 1.0 02/22/15 12:24
Toluene ug/L ND 1.0 02/22/15 12:24
trans-1,2-Dichloroethene ug/L ND 5.0 02/22/15 12:24
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 04:53 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1395932
Associated Lab Samples:92237748001, 92237748002, 92237748003
Matrix:Water
Analyzed
trans-1,3-Dichloropropene ug/L ND 1.0 02/22/15 12:24
trans-1,4-Dichloro-2-butene ug/L ND 100 02/22/15 12:24
Trichloroethene ug/L ND 1.0 02/22/15 12:24
Trichlorofluoromethane ug/L ND 1.0 02/22/15 12:24
Vinyl acetate ug/L ND 50.0 02/22/15 12:24
Vinyl chloride ug/L ND 1.0 02/22/15 12:24
Xylene (Total)ug/L ND 5.0 02/22/15 12:24
1,2-Dichloroethane-d4 (S)%103 70-130 02/22/15 12:24
4-Bromofluorobenzene (S)%98 70-130 02/22/15 12:24
Toluene-d8 (S)%99 70-130 02/22/15 12:24
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1395933LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.250 104 80-125
1,1,1-Trichloroethane ug/L 50.750 101 71-129
1,1,2,2-Tetrachloroethane ug/L 49.850 100 79-124
1,1,2-Trichloroethane ug/L 51.150 102 85-125
1,1-Dichloroethane ug/L 49.650 99 73-126
1,1-Dichloroethene ug/L 48.050 96 66-135
1,2,3-Trichloropropane ug/L 49.450 99 75-130
1,2-Dibromo-3-chloropropane ug/L 49.350 99 71-133
1,2-Dibromoethane (EDB)ug/L 51.550 103 83-124
1,2-Dichlorobenzene ug/L 49.750 99 80-133
1,2-Dichloroethane ug/L 48.250 96 67-128
1,2-Dichloropropane ug/L 51.450 103 75-132
1,3-Dichloropropane ug/L 50.750 101 76-131
1,4-Dichlorobenzene ug/L 49.850 100 78-130
2-Butanone (MEK)ug/L 94.8J100 95 61-144
2-Hexanone ug/L 103100 103 68-143
4-Methyl-2-pentanone (MIBK)ug/L 102100 102 72-135
Acetone ug/L 102100 102 48-146
Acrylonitrile ug/L 263250 105 40-160
Benzene ug/L 53.050 106 80-125
Bromochloromethane ug/L 52.350 105 71-125
Bromodichloromethane ug/L 47.950 96 78-124
Bromoform ug/L 42.650 85 71-128
Bromomethane ug/L 44.250 88 40-160
Carbon disulfide ug/L 44.2J50 88 50-160
Carbon tetrachloride ug/L 52.850 106 69-131
Chlorobenzene ug/L 50.150 100 81-122
Chloroethane ug/L 52.950 106 39-148
Chloroform ug/L 45.950 92 73-127
Chloromethane ug/L 51.650 103 44-146
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 04:53 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 14 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1395933LABORATORY CONTROL SAMPLE:
LCSSpike
cis-1,2-Dichloroethene ug/L 50.450 101 74-124
cis-1,3-Dichloropropene ug/L 52.650 105 72-132
Dibromochloromethane ug/L 43.050 86 78-125
Dibromomethane ug/L 52.450 105 82-120
Ethylbenzene ug/L 50.650 101 79-121
Iodomethane ug/L 95.6100 96 39-154
Methylene Chloride ug/L 53.350 107 64-133
Styrene ug/L 53.750 107 84-126
Tetrachloroethene ug/L 48.650 97 78-122
Toluene ug/L 51.450 103 80-121
trans-1,2-Dichloroethene ug/L 50.050 100 71-127
trans-1,3-Dichloropropene ug/L 47.850 96 69-141
trans-1,4-Dichloro-2-butene ug/L 50.7J50 101 40-160
Trichloroethene ug/L 50.350 101 78-122
Trichlorofluoromethane ug/L 52.950 106 53-137
Vinyl acetate ug/L 98.3100 98 40-160
Vinyl chloride ug/L 50.050 100 58-137
Xylene (Total)ug/L 151150 101 81-126
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1400344MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237208015
1400345
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 3 3021.4 20.9
1,1,1-Trichloroethane ug/L 2 3024.1 23.7
1,1,2,2-Tetrachloroethane ug/L 2 3021.0 20.6
1,1,2-Trichloroethane ug/L 6 3021.9 20.7
1,1-Dichloroethane ug/L 20 114 70-130110 3 30201.3 24.1 23.4
1,1-Dichloroethene ug/L 20 112 70-166107 5 30200.84J 23.3 22.2
1,2,3-Trichloropropane ug/L 2 3021.3 20.9
1,2-Dibromo-3-
chloropropane ug/L 1 3019.5 19.7
1,2-Dibromoethane (EDB)ug/L 1 3021.4 21.2
1,2-Dichlorobenzene ug/L 3 3021.1 20.4
1,2-Dichloroethane ug/L 20 113 70-130108 4 3020ND22.6 21.7
1,2-Dichloropropane ug/L 4 3021.9 21.0
1,3-Dichloropropane ug/L 2 3021.5 21.0
1,4-Dichlorobenzene ug/L 4 3021.5 20.6
2-Butanone (MEK)ug/L 1 3040.8J 41.4J
2-Hexanone ug/L 1 3041.1J 41.6J
4-Methyl-2-pentanone
(MIBK)ug/L 3 3043.6J 42.3J
Acetone ug/L 1 3045.6J 45.8J
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 04:53 PM
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[phone]
Page 15 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1400344MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92237208015
1400345
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Acrylonitrile ug/L 0 30113J113J
Benzene ug/L 3 3023.2 22.4
Bromochloromethane ug/L 2 3022.7 22.2
Bromodichloromethane ug/L 4 3019.9 19.2
Bromoform ug/L 1 3017.8 17.7
Bromomethane ug/L 13 3020.7 18.2
Carbon disulfide ug/L 4 3019.1J 18.3J
Carbon tetrachloride ug/L 2 3022.6 22.1
Chlorobenzene ug/L 3 3021.6 21.0
Chloroethane ug/L 6 3026.3 24.7
Chloroform ug/L 1 3020.3 20.6
Chloromethane ug/L 4 3023.2 22.4
cis-1,2-Dichloroethene ug/L 20 106 70-13097 2 302084.1 105 104
cis-1,3-Dichloropropene ug/L 3 3020.2 19.6
Dibromochloromethane ug/L 1 3018.1 17.9
Dibromomethane ug/L 2 3021.5 21.0
Ethylbenzene ug/L 3 3022.4 21.8
Iodomethane ug/L 20 3034.7 42.6
Methylene Chloride ug/L 2 3022.5 22.1
Styrene ug/L 4 3022.2 21.2
Tetrachloroethene ug/L 4 3021.7 20.8
Toluene ug/L 3 3022.4 21.7
trans-1,2-Dichloroethene ug/L 20 113 70-130110 3 30201.3 24.0 23.3
trans-1,3-Dichloropropene ug/L 2 3019.3 18.9
trans-1,4-Dichloro-2-butene ug/L 2 3019.1J 19.5J
Trichloroethene ug/L 20 105 69-15191 3 302077.6 98.6 95.8
Trichlorofluoromethane ug/L 4 3026.6 25.4
Vinyl acetate ug/L 2 3030.6J 30.0J
Vinyl chloride ug/L 20 113 70-130109 4 3020ND22.7 21.7
1,2-Dichloroethane-d4 (S)%104 70-130102
4-Bromofluorobenzene (S)%100 70-130100
Toluene-d8 (S)%100 70-13098
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 04:53 PM
Pace Analytical Services, Inc.
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[phone]
Page 16 of 20
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 04:53 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 20
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92237748
Wayne MSWLF Blanks
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92237748001 MPRP/17907 ICP/16106EBEPA 3010 EPA 6010
92237748002 MPRP/17907 ICP/16106FBEPA 3010 EPA 6010
92237748001 MSV/30436EBEPA 8260
92237748002 MSV/30436FBEPA 8260
92237748003 MSV/30436TBEPA 8260
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/04/2015 04:53 PM
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[phone]
Page 18 of 20
Page 19 of 20
Page 20 of 20
Appendix B
Field Sampling Parameter Data Sheet(s)