WQ0003487_Renewal Application_1_20210401

Initial Review
Reviewer Thornburg, Nathaniel
Is this submittal an application? (Excluding additional information.)*
r Yes r No
Permit Number (IR)* WQ0003487
Applicant/Permittee Novozymes North America, Inc.
Applicant/Permittee Address 77 Perrys Chapel Church Rd., Franklinton, NC 27525
Is the owner in BIMS? r Yes r No Is the facility in BIMS? r Yes r No
Owner Type Organization
Facility Name Novozymes DCAR
County Franklin
Fee Category Major
Is this a complete
application?*
c Yes r No
Signature Authority
Signature Authority Title
Signature Authority Email
Document Type (if non -application)
Email Notifications
Does this need review bythe hydrogeologist?* r Yes r No
Regional Office
CO Reviewer
Admin Reviewer
Fee Amount $395
Complete App Date 04/01/2021
Below list any additional email address that need notification about a new project.
Email Address
Comments to be added to email notfication
Comments for Kendall
Comments for RO

Comments for Reviewer
Comments for Applicant

Submittal Form
Project Contact Information
Rease provide information on the person to be contacted by N B Staff
Name * Steve Stadelman
Email Address*
[e-mail]
electronic subnittal, confirmation of receipt, and other correspondence.
Phone Number*
919-495-0333
Project Information
...............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
6- Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
O Modification - Minor
C Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
r Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
r Wastewater Irrigation r High -Rate Infiltration
r Other Wastewater r Reclaimed Water
r Closed -Loop Recycle r Residuals
r Single -Family Residence Wastewater r Other
Irrigation
Permit Number:*
WO0003487
Fbs Current Existing perrrit number
Applicant/Permittee *
Novozymes North America, Inc.
Applicant/Permittee Address*
77 Perrys Chapel Church Rd., Franklinton, NC 27525
Facility Name *
Novozymes DCAR
Please provide comments/notes
on your current submittal below.
permit application is for modification
and renewal
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form Engineering Rans, Spec'rfications, Calculations, Rc.)
WQ0003487_Novozymes_permit _mod_renewal_applicati... 25.08MB
upload only 1 RCF docurrent (less than 250 vB). NL@iple documents nest be combined into one RDF file unless file is larger than
upload limit.
* W By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 3/24/2021

novozY mes.*
Novozymes North America Inc.
PO BOX 576
Franklinton
United States
Phone: [phone]
www.novozymes.com
North Carolina Department of Environmental Quality
Division of Water Resources - Water Quality Permit Section
Non -Discharge Permitting Unit
1636 Mail Service Center
Raleigh, NC 27699-1636
March 24, 2021
Subject: Class A Residuals Application for Permit Renewal with Major Modification,
Permit# WQ0003487
Dear Sir/Madam,
Novozymes is pleased to submit the permit application package for Permit # WQ0003487. The current permit
is scheduled to expire on November 30, 2021. As such, this renewal package is being submitted 180 days
prior to the expiration date as required for permit renewal.
Also, Novozymes is requesting a major permit modification to 1) add waste residuals from reverse osmosis
(RO) treatment of process wastewater and 2) to construct a new above -ground concrete residuals storage
tank.
As required by a Groundwater Corrective Action Plan dated July 16, 2015 and approved by NCDEQ in a letter
dated January 31, 2017, Novozymes has received a new NPDES permit for discharge of process wastewater
to meet the required reduction in wastewater irrigation. Novozymes will be installing a reverse osmosis sys-
tem to ensure compliance with effluent limits with construction expected to start in 1 H 2O22 and commission-
ing and start up in 2H 2O22. Waste from the reverse osmosis system is proposed for addition to the residuals
for land application in this permit. A new above ground concrete residuals storage tank is proposed to man-
age the additional volume and is planned to be constructed and and commissioned on the same timeline as
the reverse osmosis system.
Included in the permit application are:
1. Form DCAR 11-15
2. Form RSC 11-15
3. Site Vicinity Map
4. Process Narrative and Process Flow Diagram
5. Engineering plans (new residuals storage tank)
6. Additional information, Marketability Statement, and Product Information Sheet
7. Certified Lab Results for Residuals and Process Wastewater - TCLP and Metals Analysis
8. Certified Lab Results for RO waste analyses
9. Certified Lab Results for Residuals (SBM) waste analyses — 2020
10. Branch — Residuals —Report _3_22_2021
11.Operation and Maintenance Plan Documentation
Rethink Tomorrow

novozY mes.
The application fee for $395 will be sent to NCDEQ under separate cover.
Please contact me at your convenience if you have any questions or if additional information is required.
Best regards,
Steve Stadelman
Manager/Specialist, NZNA
[e-mail]
919-495-0333
Page 212

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS
INSTRUCTIONS FOR FORM: DCAR 06-16 & SUPPORTING DOCUMENTATION
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted the Applicant shall submit one original and two conies of the avylication and
supporting documentation
For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit websitt
General — This application is for treatment, storage, transport, distribution, land application, and/or marketing of Class A (or Equivalent)
residuals under 15A NCAC 02T ,1100.
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Distribution of Class A Residuals (FORM: DCAR 06-16):
® Submit the completed and appropriately executed Distribution of Class A Residuals (FORM: DCAR 06-16) form. Please do
not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to
the application may be made, as long as the attachments are numbered to correspond to the section and item to which they
refer.
® The project name should be consistent on the plans, specifications, etc.
® The Applicant's Certification on Page 3 of this form shall be signed in accordance with k NC k(' 07T .0106(b). An alternate
person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in 15A
NCAC 02T .0106(b).
® If this project is for a modification of an existing permit, submit one copy of the existing permit.
® Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to
operation of proposed facility(ics) for application packages involving new or changes to treatment and storage units.
B. Application Fee (New and Major Modification Application Packages)
® Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environmental
Quality (NCDEQ).
Facility Classification New Permit Major Modification t
Major (residuals permitted for distribution >_ 3,000 dry tons/year) $1,310 $395
Minor (residuals permitted for distribution < 3,000 dry tons/year) $810 $245
- A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage;
adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted.
There is no fee for minor permit modifications.
C. Cover Letter (All Application Packages)
® List all items included in the application package, as well as a brief description of the requested permitting action.
INSTRUCTIONS FOR FORM: DCAR 06-16 Pagel of 3

D. Program Information (All Application Packages)
® Provide a narrative explaining the following:
® How the materials will be handled and transported from where the residuals were produced to where it will be treated.
® How the residuals will be processed/treated (attach process flow diagram).
❑ How leachate collection will be handled.
® Where the residuals will be stored until processed.
® How the final product will be distributed (packaging, bulk, etc.)
® What nutrients or other constituents (i.e. nitrogen, phosphorous, aluminum, calcium, etc.) are used or recommended as the
limiting parameter for determination of residuals loading rate to ensure that it does not overload the soil and cause
contravention of surface water or groundwater standards, limit crop growth, or adversely impact soil quality.
® Attach a marketability statement detailing destinations and approximate amounts of the final product to be distributed.
® Provide either a label that shall be affixed to the bagged processed residual or an information sheet that shall be provided to the
person who receives the processed residual. The label or information sheet shall contain, at a minimum, the following
information:
❑ Name and address of the person who prepared the residual that is sold or given away.
❑ A statement that application of the residuals to the land shall be in accordance with the instructions on the label or
information sheet.
❑ A statement that the residuals shall not be applied to any site that is flooded, frozen or snow-covered.
❑ A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored
residuals into any surface waters.
❑ Information on all applicable setbacks in accordance with 15A NCAC 02T . l 10,�c h }.
❑ A statement that the residuals shall be applied at agronomic or recommended rates for intended uses.
E. Detailed Plans and Specifications (Application Involving New or Changes to Treatment or Storage Units)
® Submit detailed plans and specifications that have been signed, sealed, and dated by a NC Professional Engineer per 15 4
NCAC 02"1 .1104(a). Specifications for standard equipment may only be omitted for municipalities with approved standard
specifications, but use of the standard specifications must be noted on each sheet of the plans.
® Plans must include the following minimum items: a general location map, a topographic map, plan and profile view of the
residuals treatment and storage units as well as the proximity of the residuals treatment and storage units to other utilities and
natural features within 500 feet of all treatment and storage facilities, and detail drawings of all items pertinent to the residuals
treatment and storage units. Depict minimum separations required in 15A NCAC 02T .1 I081a) on the plans.
® Specifications must include, at a minimum, the following for all items pertinent to residuals treatment and storage units:
description of materials to be used, methods of construction, quality of construction testing procedures to ensure the integrity
of the final product in accordance with 15A NCAC 02T. I 104(a)(2)(B), including leakage and pressure testing as appropriate.
® Plans and specifications must not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR
CONSTRUCTION, etc.) that indicate that they are anything other than final plans and specifications. However, the plans and
specifications may be labeled with the phrase: FINAL DESIGN - NOT RELEASED FOR CONSTRUCTION.
F. Engineering Calculations (Application Involving New or Changes to Treatment or Storage Units)
❑ Submit all design calculations that have been signed, sealed, and dated by a NC Professional Engineer per 15A NCAC 02T
.1 104(a).
G. Environmental Assessments (May be Required — See 15A NCAC 1C .0300)
❑ Subunit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include
information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the residuals
treatment and storage facilities. An EA may also he required for private systems if any public funds and/or lands are used for
the construction of the subject facilities.
INSTRUCTIONS FOR FORM: DCAR 06-16 Page 2 of 3

H. Operation and Maintenance Plan (New and Renewal Application Packages)
® For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan.
® Submit the O&M Plan in accordance with 15A NCAC 021 .1110 and include at a minimum:
® Operational functions; describe the operation of the program to show what operations are necessary for the program to function
and by whom the functions are to be conducted.
® Maintenance schedules; may include equipments calibration, maintenance of signs, etc.
® Safety measures; may include safety training program, manuals, signs, etc.
® Spill response plan; including control, containment, remediation, emergency contact information, etc.
® Inspection plan including the following information;
® Names and titles of personnel responsible for conducting the inspections.
® Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected
location(s) and inspection frequency are representative of the residuals management program.
® Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event
that noncompliance is observed.
® Sampling and monitoring plan including the following information;
® Names and titles of personnel responsible for conducting the sampling and monitoring.
® Detailed description of monitoring procedures including parameters to be monitored.
® Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow,
and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling
plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet
pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual
sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected
by cold temperatures.
ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL
SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS:
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY
DIVISION OF WATER RESOURCES
WATER QUALITY PERMITTING SECTION
NON -DISCHARGE PERMITTING UNIT
By U.S. Postal Service:
1617 MAIL SERVICE CENTER
RALEIGH, NORTH CAROLINA 27699-1617
TELEPHONE NUMBER: [phone]
By Courier/Special Delivery:
512 N. SALISBURY STREET
RALEIGH, NORTH CAROLINA 27604
FAX NUMBER: [phone]
INSTRUCTIONS FOR FORM: DCAR 06-16 Page 3 of 3

DWR
State of North Carolina
Department of Environmental Quality
Division of Water Resources
Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS
FORM: DCAR 06-16
I. APPLICANT INFORMATION:
1. Applicant's name: Novozymes North America, Inc.
Applicant type: ❑ Individual ® Corporation ❑ General Partnership ❑ Privately -Owned Public Utility
❑ Federal ❑ State ❑ Municipal ❑ County
Signature authority's name per 15A NCAC 02T .0106: Charles Shapiro Title: Sr. Director, Deputy General Counsel,
Americas
Applicant's mailing address: 77 Perrys Chapel Ch. Rd.
City: Franklinton State: NC Zip: 27525-
Telephone number: 9{ 19) 494-3024 Email Address: chsh(cmovozymes.com
2. Consultant's name: Chris Stahl License Number (for P.E.): 023224
Affiliation: ❑ On Staff ® Retained (Firm: S&ME, Inc.)
Consultant's mailing address: 2016 Ayrsley Town Blvd., Suite 2-A
C'itv: Charlotte State: NC Zip: 28273-
Telephone number: [phone] Email Address: estahl(asmeinc.com
3. Fee submitted: $395.00 (See Instruction B)
II. PERMIT INFORMATION:
1. Application is for (check all that apply): ❑ new, ® modified, ® renewed permit
2. If this application is being submitted to renew or modify an existing permit, provide the following:
Permit number: W00003487
Date of most -recently issued permit: December L 2016
Date of most -recently certified Attachment A (if different than the permit): June 7, 2017
III. FACILITY INFORMATION:
1. Name of residuals processing facility: Novozymes North America, Inc.
City: Franklinton State: NC Zip: 27525-
Coordinates: Latitude: 35 05' 41" Longitude: 78` 24' 20"
Datum: Level of accuracy:
Method of measurement: Franklin County GIS Parcel Map
County where facility is located: Franklin
2. Facility contact (person familiar with residuals preparation):
Name: Chase McGee Title: Environmental Operation, Utilities, and Granulation Manager
Mailing address: 77 Perrys Chapel Ch. Rd.
City: Franklinton State: NC Zip: 27525-
Telephone number: [phone] E-mail address: evm(i_:noyozymes.com
FORM: DCAR 06-16 Pagel of 3

3. Is the residual process facility also the generator? ® Yes; ❑ No
If No, please specify delivery frequency and quantity of residual to be processed.
4. Length of residuals storage at facility: 22 days (Note: the Division requires minimum 30 days storage in units that are separate
from treatment system, i.e. not in clarifiers, aeration basins, etc.)
IV, RESIDUALS QUALITY INFORMATION;
1. Specify how these residuals will be distributed:
❑ sold or given away in bags or other containers; ❑ lawn (bulk); ❑ home garden (bulk);
® other (explain); residual is hauled and spread on farmland by Novozymes' contractor
Note: Bulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a
load capacity of one metric ton or less.
2. Complete the following if residuals are to be mixed with other materials:
Type of Materials
Amounts to be added
er 1.0 dry ton of residuals (dry ton
Hydrated Lime
0.1
3. Approximate amounts of the residuals received and processed at the facility: 19,200 dry tons per year.
4. Approximate amounts of the final product (processed residuals) to be distributed: 20,000 dry tons per year.
5. Provide a description of the onsite storage management plan for the treated residuals (including estimated average and
maximum storage times prior to distribution): Treated residuals are stored in 3 existing and 1 new above ground concrete
storage tanks for at least 24 hours and maximum of 22 days prior to land application
6. Does the facility have a stormwater management plan? ® Yes; ❑ No
Explain whether the treatment and storage areas are under roof or how stormwater runoff will be handled: Treatment and
storage areas are wades so that stormwater is collected in a common sump numg and then pumped into the residual storage
tanks
V. RESIDUALS SOURCE INFORMATION; (Required for all new, renewed, or modified residuals source)
Complete and submit the attached Residuals Source Certification and all associated documentation.
RSC 06-16.doc
FORM: DCAR 06-16 Page 2 of 3

Professional Engineer's Certification: (Application Involving New or Changes to Treatment or Storage Units)
I, Clz\MrTOQ IAZZL .J•l.., nx-c4k L , attest that this application for Wb"JO Z T-IMS
- ri btt~1C,%h !A-VAM%< A
has been reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of my knowledge
the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal package
may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have reviewed
this material and have judged it to be consistent with the proposed design.
North Carolina Professional Engineer's Seal, Signature, and Date: I
II A 4 pr
oQ 'FESS.0 '
S A
224
cz,
PH ER
f 1 r,�,[,�,}t�\
Applicant's Certification: Z 1
The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper
closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active
compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105.
❑ Yes ❑ No, Explain', 1 ,(
(Signature Authority's Name — PLEASE PRINT) (Title)
attest that this application for V o VOA ylYl if,s 4—/Of of r
(Facility Name)
has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources
may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically
granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action,
which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water
Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed
and that if all required supporting information and attachments are not included, this application package will be returned to me as
incomplete.
Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.613, any person who knowingly makes any false
statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to
exceed $10,000 as well as ' ' penal i p to $2i"Ir
olation. � A
Signature: Date: %
FORM: DCAR 06-16 Page 3 of 3

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
INSTRUCTIONS FOR FORM: RSC 06-16
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and
supporting documentation
For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit
General — This certification provides detailed information of residuals source generating facility and its residuals quality for land
application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without
a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15).
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Residuals Source Certification (FORM: RSC 11-15):
® Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not
make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the
application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer.
® For new or renewed permits, submit a separate certification for each source facility.
® For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification.
® Complete the residuals source facility summary page. List all new, renewed, or modified facilities.
B. Residuals Source -Generating Facility Information:
® For each source facility, attach the following:
® Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance for
Residuals Land Application Permits".
® Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals
are to be generated, treated, processed, and stored at the facility.
® Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8.
Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of
the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed,
and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during
processing.
® Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies
sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition,
ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and
vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as
they are to be land applied, distributed, and/or disposed.
C. Residuals Quality Information:
® For each source facility, attach the following:
® Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification.
® Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector
attraction reduction requirements.
❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please
attach analytical results of residuals generated from a similar facility along with the description of similarities of the two
facilities.
INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1

RESIDUALS SOURCE FACILITY SUMMARY
Applicant's name: Novoames North America, Inc.
Status
Code a
Facility Permit Holder
Facility Name
County
Permit Number
Maximum Dry Tons Per Year
Current n
Proposed
R,M
Novozymes North America,
Inc.
Novozymes North America,
Inc. — Franklin County
Facility
Franklin
WQ0003487,
WQ0002806, and
NCO089621
41,000
41,000
a Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted)
SUMMARY FOR FORM: RSC 06-16 Page 1

b The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility).
FORM: RSC 06-16 Page 2 of 5

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: tovozymes North America, Inc.
2. Facility permit holder is: ❑ Federal, ❑ State, 0 Local Government, or 0 Private.
Facility permit issued by: ® Div. of Water Resources, Div. of Environmental Health,
or ❑ Other (explain: M.
3. Facility contact person and title: Chase McGee, Enviro ntal Operations, Utilities, and Granulation Manager
Complete mailing address: �7 Perrys Chapel Ch. Rd.
City: Franklinton State: NC Zip: 27525-
Telephone number: [phone] E-mail address: evmna,novozymes.com
4. Facility physical address: 77 Perrys Chpel Ch. Rd.
City: Franklint State: NC Zip: 27525-
Coordinates: Latitude: 35' 05' 41" Longitude: 78' 24' 20"
Datum: I Level of accuracy:
Method of measurement: Franklin County GIS Parcel Search
5. Purpose of the facility:
treatment of municipal wastewater, treatment of 100% domestic wastewater,
treatment of potable water, treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: = % industrial and % domestic)
other (explain: s=t bioma�om ferm'ena-tion operations ).
6. Does the facility have an approved pretreatment program: 11 Yes No
7. Facility permitted/design flow: 0.70 MGD non -discharge + 0.525MGD discharge to POTW+2MGD NPDES flow
MGD and facility average daily flow: 0.700 MGD
8. Average amount of residuals being generated at this facility 18,200 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: 77o—ve ground tanks - 194,000 gallons
Type and volume of residuals storage (i.e., outside of residuals treatment units): Above ground tanks with total storage of
MG (3.35 MG existing plus 1.65 MG new)
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
40 CFR Part 503 or ® 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
Biological 0 Non -Biological
FORM: RSC 06-16 Page 1 of 5

Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no.
If yes, list the number(s): =
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: 0 yes 0 no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: Enco La and Date of analysis: _
Passed corrosivity test: yes no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: yes no. Flashpoint: _ °F (> 140°F)
Passed reactivity test: 0 yes Ono. HCN: _ mg/kg (<250) & HzS: _ mg/kg (<500)
TCLP Parameter
Limit
(Mg/1)
Result
(Mg/1)
TCLP Parameter
Limit
(Mg/1)
Result
(Mg/1)
Arsenic
5.0
No detection
Hexachlorobenzene
0.13
No detection
Barium
100.0
No detection
Hexachloro-1,3-Butadiene
0.5
No detection
Benzene
0.5
No detection
Hexachloroethane
3.0
No detection
Cadmium
1.0
0.0235
Lead
5.0
0.121
Carbon Tetrachloride
0.5
No detection
Lindane
0.4
No detection
Chlordane
0.03
No detection
Mercury
0.2
No detection
Chlorobenzene
100.0
No detection
Methoxychlor
10.0
No detection
Chloroform
6.0
No detection
Methyl Ethyl Ketone
200.0
No detection
Chromium
5.0
No detection
Nitrobenzene
2.0
No detection
m-Cresol
200.0
No detection
Pentachlorophenol
100.0
No detection
o-Cresol
200.0
No detection
Pyridine
5.0
No detection
p-Cresol
200.0
No detection
Selenium
1.0
No detection
Cresol
200.0
No detection
Silver
5.0
No detection
2,4-D
10.0
No detection
Tetrachloroethylene
0.7
No detection
1,4-Dichlorobenzene
7.5
No detection
Toxaphene
0.5
No detection
1,2-Dichloroethane
0.5
No detection
Trichloroethylene
0.5
No detection
1, 1 -Dichloroethylene
0.7
No detection
2,4,5-Trichlorophenol
400.0
No detection
2,4-Dinitrotoluene
0.13
No detection
2,4,6-Trichlorophenol
2.0
No detection
Endrin
0.02
No detection
2,4,5-TP (Silvex)
1.0
No detection
Heptachlor and its Hydroxide
0.008
No detection
Vinyl Chloride
0.2
No detection
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: ENCO LM and Date of analysis: 2020 residual testing data, RO trial data (see report from Branch Residuals)
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mg/kg)
Monthly Average
Concentration Limits
(Class A Only)
(mg/*g)
Result
(mg/W
Arsenic
75
41
1.475
Cadmium
85
39
0.070
Copper
4,300
1,500
4.623
Lead
840
300
0.612
Mercury
57
17
0.024
Molybdenum
75
n/a
0.733
Nickel
420
420
0.994
Selenium
100
100
1.204
Zinc
7,500
2,800
11.444
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: _ and Date of analysis: _
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
El > 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
❑ > 100 but < 125
53
360
390
❑ > 125
62
450
420
Result (mg/kg)
FORM: RSC 06-16 Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: E %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: ENCO Labs and Date of analysis: �020 residual testing data, RO trial data (see report from Branch Residuals)
Parameter
Result
(mg1kg)
Aluminum
2,478
Ammonia -Nitrogen
2,103
Calcium
70,963
Magnesium
891
Nitrate -Nitrite Nitrogen
2999
pH (Standard Unit)
12.17
Phosphorus
10,758
Potassium
24,503
Sodium
23,062
Total Kjeldahl Nitrogen
31,854
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR):
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: %. This
rate is a (check one): default value, or 09 actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals:
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (11) Year PAN
Five -Year
Maximum Adjusted PAN
(mg/kg)
(mg/kg)
Surface
15,951
21,897
Injection/Incorporation
17,002
22,948
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses: Increased sodium and salinity from RO waste have been evaluated. See attached narrative.
FORM: RSC 06-16 Page 4 of 5

7. Pathogen Reduction: Per 15A NCAC 02T.11061 specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent.
A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
® A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
❑ Alternative 1 [ 15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance.
Alternative 2 [15A NCAC 02T.I 106(b)(3)(B)] - Alkaline Treatment.
Alternative 3 [15A NCAC 02T. 1106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 5 [15A NCAC 02T.1106 (3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: ❑ composting, 4 heat drying, ❑ heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of Class B:
Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration.
Alternative 2 [15A NCAC 02T.I 106(c)(2)l - Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑ aerobic digestion, air drying, ❑ anaerobic digestion,
❑ composting, 4 1 lime stabilization.
c. For Surface Disposal:
Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
rl Alternative 1 [15A NCAC 02T. 1 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
❑ Alternative 3 [15A NCAC 02T. 1 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
❑ Alternative 5 [15A NCAC 02T. 1 107(a)(5)] - 14-Day Aerobic Processes.
Alternative 6 [15A NCAC 02T. 1 107(a)(6)] - Alkaline Stabilization.
Alternative 7 [15A NCAC 02T. 1 107(a)(7)] - Drying of Stabilized Residuals.
❑ Alternative 8 [15A NCAC 02T. 1 107(a)(8)] - Drying of Unstabilized Residuals.
❑ Alternative 9 [15A NCAC 02T. 1 107(a)(9)] - Injection.
❑ Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation.
❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [ 15A NCAC 02T.I 107(b)(2)].
E] Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5

Vicinity Map - Novozymes North America Inc.
June 6, 2016 1:4,514
0 290 580 1,160 ft
0 87.5 175 350 m
Source: Esri, DigitalG lobe, GeoEye, Earthstar Geographics,
CNES/Airbus DS, USDA, USGS, AEX, Getmapping, Aerogrid, IGN,
IGP, swisstopo, and the GIS User Community
Esri, HERE, DeLorme, Mapmylndia, © OpenStreetMap contributors,
and the GIS user community
2016

Permit WQ0003487
Production
Waste Solids
from WWTF
SBM from Fermentation SBM from Other
and Recovery Production (Source: Rejected WAS tank
Process prod ucts/d isp osa Is, WQ0002806
cleanin g o f tanks)
Treatment of
Solids from WWTF
SBM
primary clarifier
with lime at this
WQ0002806
point
(Land application)
RO waste collected Pumped to storage
under NPDES tanks for land Dewater
NCO089621 application — new Soli (By the
storage tank to be centrifuge)
added
Water
Green boxes reflect the 3rd party trucking
permit change — addition takes from tanks to field
of RO waste to the Goes back to
permit and addition of Wastewater
p Treatment
new storage tank
Actual land
application
(NZ tractors & wagons,
Contract Operator)
Residuals Process Flow Diagram
Novozymes North America, Inc.
June 2021

a
N()V(D2!YMES SBM TANK ADDITION
ISSUED FOR CONSTRUCTION
DISCIPLINES:
CIVIL, STRUCTURAL, MECHANICAL PROCESS,
ELECTRICAL, INSTRUMENTATION
HIPP ENGINEERING & CONSULTING, INC
PROJECT NO. R20162
04 MARCH 2O21
PREPARED FOR
novozvme
Rethink Tomo
Novozymes North America Inc.
rrow
77 Perrys Chapel Church Road
Franklinton, North Carolina 27525 USA
Tel [phone]
PREPARED BY
Hlf'f' ENGINEER-INC
& CONSULTING, INC.
2301 REXWOODS DRIVE, SUITE 200
RALEIGH, NC 27607
TEL:[phone] FAX:[phone]
NC FIRM LICENSE NUMBER: C-2146
STEWART
223 S. WEST STREET
SUITE 1100
RLEIGH, NC 27603
TEL: 1 } 0- 7 0
FIRM LICENSE N: -1 01
DRAWING NUMBER
DRAWING TITLE
ISSUED FOR
CONSTRUCTION
04MAR2021
CIVIL
FLF31001_U502986_NEW
EXISTING CONDITIONS PLAN
A
FLF31002_U502986_NEW
SITE PLAN
A
FLF31401
U502986
NEW
EROSION CONTROL PLAN (PHASE 1)
A
FLF31402
U502986
NEW
EROSION CONTROL PLAN (PHASE 11)
A
FLF31403
U502986
NEW
EROSION CONTROL PLAN (PHASE III)
A
FLF31301
U502986
NEW
GRADING AND DRAINAGE PLAN
A
FLF30801
U502986
NEW
CIVIL DETAILS
A
STRUCTURAL
FLF40001
U502986
REF
GENERAL NOTES AND DESIGN CRITERIA
A
FLF40002
U502986
REF
ABBREVIATIONS, LEGEND & SYMBOLS
A
FLF40101
U502986
NEW
PARTIAL FOUNDATION PLAN - SITE
A
FLF40301
U502986
NEW
FOUNDATION SECTIONS AND DETAILS
A
FLF40601
U502986
NEW
CATWALKS AND TANK ACCESS PLATFORM - FRAMING PLANS
A
FLF40701
U502986
NEW
TYPICAL FLOOR FRAMING SECTIONS AND DETAILS
A
FLF407O2
U502986
NEW
TANK D ACCESS TOWER & PLATFORM - SECTIONS AND DETAILS
A
FLF40703_U502986_NEW
NEW AND EXISTING CATWALKS - SECTIONS AND DETAILS
A
MECHANICAL PROCESS
FLF72001_U502986_REF
PI -DIAGRAM LEGEND
A
FLF72002_U502986_REF
PI -DIAGRAM EXAMPLE SHEET
A
FLF71001_U502986_REF
PROCESS PIPING SPECIFICATIONS & DETAILS
A
FAA72963 U502986
PI -DIAGRAM TREATED SBM STORAGE FACILITIES
8A
FLF75001
U502986
NEW
FLF96DT GENERAL ARRANGEMENT
A
FLF73002
U502986
NEW
PI PING ARRANGEMENT TO FLF96DT
A
FLF74003
U502986
NEW
SECTIONS AND ENLARGED VIEWS
A
ELECTRICAL
FLF60001
U502986
REF
POWER, LIGHTING & MISC. SYSTEMS LEGEND
A
FLF60002
U502986
REF
ELECTRICAL SPECIFICATIONS
A
FLF68001
U502986
NEW
480/277V ONE LI NE DIAGRAM AND MCC FRONT VI EW
A
FLF62001
U502986
NEW
POWER PLAN - SITE
A
FLF67001
U502986
NEW
PANELBOARD SCHEDULE & HEAT TRACE BOM
A
FLF60701
U502986
NEW
MOTOR ELEMENTARY DIAGRAM - STARTERS
A
FLF62101
U502986
NEW
ELECTRICAL DETAILS
A
INSTRUMENTATION
FLF84001_U502986_NEW
INSTRUMENTATION INSTALLATION DETAILS
A
SWIFT
PARTNERS
HIPP ENGINEERING
& CONSULTING, INC.
2301 REXWOODS DRIVE, SUITE 200
RALEIGH, NC 27607
TEL:[phone] FAX:[phone]
NC FIRM LICENSE NUMBER: C-2146
WWW.HIPP-USA.COM
THIS DRAWING IS THE PROPERTY OF HIPP, INC.,
AND IS NOT TO BE REPRODUCED, COPIED OR USED
FOR ANY PURPOSE OTHER THAN CONSTRUCTION
OF THIS PROJECT WITHOUT THE WRITTEN
CONSENT OF HE&C, INC.
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SURVEY LEGEND:
EXISTING CONDITION NOTES:
0
SURVEY CONTROL POINT
0 EIP
EXISTING IRON PIPE
1.
THIS SURVEY MAP IS INTENDED TO REPRESENT THE EXISTING CON DITIONS/TOPOGRAPHY ON A PORTION OF THE
PROPERTY AND ALL ENCUMBRANCES UPON THE PROPERTY MAY NOT BE SHOWN.
❑ ECM
EXISTING CONCRETE MONUMENT
2.
HORIZONTAL DATUM IS NAD 83-2011 AND VERTICAL DATUM IS NAVD88.
♦
COMPUTED POINT
@
STORM DRAIN MANHOLE
3.
THIS DRAWING DOES NOT CONFORM TO N.C. GS47-30 AND THEREFORE IS NOT FOR RECORDATION.
®
STORM DRAIN CURB INLET
4.
UTILITIES SHOWN HEREON ARE BASED ON ABOVE GROUND VISIBLE EVIDENCE AND UTILITY DESIGNATION /
MARKING SERVICES PERFORMED BY STEWART INC, AND THE AVAILABLE RECORD INFORMATION. CONTRACTOR
(5)
SANITARY SEWER MANHOLE
SHALL FIELD VERIFY LOCATION OF ALL UTILITIES PRIOR TO COMMENCING CONSTRUCTION.
0
SANITARY SEWER CLEANOUT
5.
SURVEY INFORMATION BASED ON FIELD SURVEY BY FEI COMPLETED ON DEC 9, 2020
®
SANITARY FORCEMAIN VALVE
6.
TREES SHOWN HEREON MAY NOT REPRESENT ALL VEGETATION ON THE SUBJECT PROPERTY.
(b
HYDRANT
WV
7.
NO WETLANDS HAVE BEEN IDENTIFIED WITHIN THE PROJECT OR PARCEL SHOWN.
>Q
WATER VALVE
WM
O
WATER METER
WATER MANHOLE
0
WATER VAULT
WELL
DEMOLITION NOTES:
D4
GAS VALVE
❑.GM
GAS METER
1.
THE CONTRACTOR SHALL REMOVE CONCRETE (WHERE REQUIRED) TO THE FIRST COLD JOINT OR SAW CUT TO
OO
TELEPHONE MANHOLE
OBTAIN A CLEAN EDGE.
TPED
O
TELEPHONE PEDESTAL
2.
THE CONTRACTOR SHALL SAWCUT EXISTING ASPHALT (WHERE REQUIRED) TO OBTAIN A CLEAN EDGE.
©
TV MANHOLE
CATV
3.
CLEANOUTS AND WATER VALVES LOCATED IN AREAS OF DEMOLITION OR SUBSEQUENT CONSTRUCTION SHALL BE
El
TV PEDESTAL
PROTECTED FROM DAMAGE AND RAISED TO BE FLUSH WITH NEW GRADE.
FOWP
O
FIBER OPTIC WITNESS POST
4.
ANY UTILITY SERVICES SHOWN TO BE REMOVED OR RELOCATED SHALL BE COORDINATED WITH THE APPROPRIATE
Fo
FIBER OPTIC BOX
UTILITY PROVIDER. CONTRACTOR IS RESPONSIBLE FOR APPROPRIATE SEQUENCING OF UTILITY DEMOLITION WITH
THE RESPECTIVE UTILITY AGENCIES.
EO
ELECTRIC MANHOLE
5.
CONTRACTOR IS RESPONSIBLE FOR VERIFYING ALL UTILITIES PRIOR TO BEGINNING DEMOLITION OPERATIONS.
EM
Ill
ELECTRIC METER
NOTIFY "NORTH CAROLINA ONE CALL" (TELEPHONE [phone]) AT LEAST 48 HOURS PRIOR TO START OF
EB
ELECTRIC BOX
DEMOLITION TO HAVE EXISTING UTILITIES LOCATED. CONTRACTOR SHALL CONTACT ANY LOCAL UTILITIES THAT
PROVIDE THEIR OWN LOCATOR SERVICES INDEPENDENT OF "NORTH CAROLINA ONE CALL."
UTILITY POLE
-0
GUY POLE
6.
CLEAN SOILS SHALL BE UTILIZED FOR BACKFILL. COMPACTION OF THESE SOILS SHALL BE PERFORMED IN
ACCORDANCE WITH THE CONSTRUCTION DOCUMENTS.
-
GUY WIRE
7.
ALL ITEMS DESIGNATED TO BE REMOVED SHALL BE REMOVED COMPLETELY, INCLUDING ALL SUBGRADE MATERIALS
LIGHT POLE
DIRECTLY ASSOCIATED WITH ITEMS TO BE REMOVED.
MANHOLE
TS
TRAFFIC SIGNAL BOX
8.
ALL ITEMS DESIGNATED TO BE REMOVED SHALL BE DISPOSED OF LEGALLY OFF -SITE UNLESS OTHERWISE NOTED
ON THIS PLAN.
�
TRAFFIC SIGNAL POST
MW
MONITORING WELL
9.
REFER TO LANDSCAPE AND EROSION CONTROL DRAWINGS FOR TREE PROTECTION PLAN AND REQUIREMENTS.
�BOR
BORING LOCATION
10.
ALL DEMOLITION SHALL BE IN ACCORDANCE WITH ALL APPLICABLE STATE AND LOCAL JURISDICTIONAL CODES OR
REQUIREMENTS.
•
BOLLARD
SIGN
11.
TREE PROTECTION FENCING SHALL BE IN PLACE PRIOR TO BEGINNING DEMOLITION
FF= '
limp,
FINISHED FLOOR ELEVATION
12.
EROSION CONTROL PERMIT SHALL BE OBTAINED AND ONSITE PRIOR TO BEGINNING DEMOLITION.
DECIDUOUS TREE
13.
ITEMS DESIGNATED TO BE SALVAGED AND/OR RE -USED SHALL BE REMOVED BY THE CONTRACTOR AND PROVIDED
EVERGREEN TREE
TO THE OWNER. COORDINATE STORAGE LOCATION WITH OWNER'S REPRESENTATIVE.
BUSH
14.
WHERE UTILITIES ("TO BE REMOVED") IMPACT THE FOOTPRINT OF THE NEW STRUCTURE, THE CONTRACTOR SHALL
X
WIRE FENCE
EXECUTE AND REMOVE AN ADDITIONAL 2 FEET OF SOILS TO EITHER SIDE OF THE PIPE, AND 1 FOOT BELOW. CLEAN
SUITABLE SOIL SHALL BE UTILIZED FOR BACKFILL AND COMPACTED IN ACCORDANCE WITH THE CONTRACT
O
CHAIN LINK FENCE
DOCUMENTS.
T
UNDERGROUND TELEPHONE LINE
15.
DEMOLITION AND SUBSEQUENT CONSTRUCTION OF STORM DRAINAGE PIPING SHALL BE PERFORMED IN SUCH A
F0
MANNER THAT THE OLD PIPE AND STRUCTURES REMOVED DO NOT IMPACT DRAINAGE UPSTREAM OF THE SYSTEM.
UNDERGROUND FIBER OPTIC LINE
PROVISIONS SHALL BE MADE TO MAINTAIN STORM WATER DRAINAGE PATTERNS DURING CONSTRUCTION.
G
UNDERGROUND GAS LINE
16.
DEMOLITION AND SUBSEQUENT CONSTRUCTION OF UTILITIES (WATER, SEWER, ETC) SHALL BE PERFORMED IN
—UGE—
UNDERGROUND ELECTRIC LINE
SUCH A MANNER THAT THE OLD PIPE AND STRUCTURES REMOVED DO NOT IMPACT OR MINIMIZE SERVICE
INTERRUPTION TO EXISTING FACILITIES TO REMAIN. PROVISIONS SHALL BE MADE TO MAINTAIN SERVICE DURING
W
UNDERGROUND WATER LINE
CONSTRUCTION.
SS
SANITARY SEWER LINE
17.
THE CONTRACTOR SHALL BE RESPONSIBLE FOR REPAIRING ALL DAMAGES TO THE EXISTING DRIVEWAY, PARKING
= =
STORM DRAIN LINE
LOT, SIDEWALK AND CURB AND GUTTER AS A RESULT OF CONSTRUCTION ACTIVITY AND TRAFFIC. CONTRACTOR
SHALL MAINTAIN A PRE -CONSTRUCTION VIDEO OR PHOTO DOCUMENTATION TO SHOW NO DAMAGES OCCURRED.
0HW
OVERHEAD WIRES
18.
ALL MATERIALS, FURNISHINGS, UTILITIES, AND PAVEMENT THAT ARE NOT SCHEDULED TO BE DEMOLISHED AND ARE
U
UNIDENTIFIED LINE
DAMAGED BY THE CONTRACTOR AS A RESULT OF THE DEMOLITION OR CONSTRUCTION OPERATIONS SHALL BE
UNKNOWN DESTINATION
REPAIRED BY THE CONTRACTOR AT NO ADDITIONAL COST TO THE OWNER.
CONCRETE SURFACE
19.
WHERE UTILITIES ARE SHOWN TO BE "REMOVED", CONTRACTOR SHALL INCLUDE NECESSARY PLUG OR VALVES TO
ENSURE UTILITY LINES TO REMAIN WILL CONTINUE TO BE IN SERVICE. COORDINATE NECESSARY SHUT DOWN AND
DIP
DUCTILE IRON PIPE
REMOVAL WITH THE LOCAL JURISDICTION OR UTILITY OWNER.
PVC
POLYVINYL CHLORIDE PIPE
20.
CONTRACTOR SHALL PROVIDE PEDESTRIAN INGRESS / EGRESS TO ALL EXISTING BUILDINGS, PARKING LOTS, AND
HDPE
HIGH -DENSITY POLYETHYLENE PIPE
PATHS OF PEDESTRIAN TRAVEL THROUGHOUT THE CONSTRUCTION PERIOD
RCP
REINFORCED CONCRETE PIPE
CMP
CORRUGATED METAL PIPE
--_
CB
CATCH BASIN
i
DEMOLITION
LEGEND:
SYMBOL
DESCRIPTION
-
REMOVE BUILDING
®
REMOVE ASPHALT
0000
°o°0°
REMOVE GRAVEL
0 0 0
REMOVE BRICK WALKWAY
REMOVE CONCRETE
REMOVE RIPRAP
REMOVE VEGETATION
� W �
REMOVE WATER LINE
� SS �
REMOVE SANITARY SEWER LINE
REMOVE STORM DRAINAGE
� X �
REMOVE FENCE
TP
TREE PROTECTION FENCE
JSWIFT
PARTNERS
LIMITS OF DISTURBANCE
COORDINATE LIGHT POLE REMOVAL
REMOVE TREE
REMOVE TREELINE
REMOVE WHEEL STOP
REMOVE CURB & GUTTER
REMOVE SIGN
L - 0 10 20 40
SCALE: 1" = 20' NORTH
04MAR2021
F
HIPP ENGINEERING
& CONSULTING, INC.
2301 REXWOODS DRIVE, SUITE 200
RALEIGH, NC 27607
TEL:[phone] FAX:[phone]
NC FIRM LICENSE NUMBER: C-2146
WWW.HIPP-USA.COM

GENERAL NOTES:
PROVIDE GRAVEL BENEATH PIPING BETWEEN
PUMPS AND TANK, COORDINATE WITH MEP
CHAIN LINK FENCE TO REPLACE PORTION OF
EXISTING FENCE REMOVED DURING GRADING
OPERATIONS
CONCRETE PAD & PUMP
SYSTEM
PROTECTIVE BOLLARD
29.00' RETAINING WALL (SEE STRUCTURAL SHEETS FOR DETAILS)
DESIGNED BY OTHERS
®® / SEE STRUCTURAL SHEETS
----- UE ----- UEUL
PROPOSED 100'0 SPENT BIOMASS PROCESSING FACILITY
OPEN TOP - 1,645,000 GAL
SEE VENDOR DRAWINGS FOR TANK CONSTRUCTION DETAILS
PAD MOUNTED UTILITY TRANSFORMER
---- UE ----- UE ---_-
UE - /�_
uc
vc �UF,
OF _
1. ALL MATERIALS AND METHODS OF CONSTRUCTION SHALL BE IN COMPLIANCE WITH THE OFFICE OF STATE
CONSTRUCTION, DEPARTMENT OF INSURANCE, NCDENR, AND ALL OTHER APPLICABLE LOCAL, STATE AND FEDERAL
GUIDELINES. ALL UTILITY CONSTRUCTION SHALL COMPLY WITH APPLICABLE LOCAL JURISDICTIONAL STANDARDS
AND SPECIFICATIONS.
2. EXISTING SURVEY INFORMATION INCLUDING TOPOGRAPHIC INFORMATION PROVIDED BY FEI, UNLESS OTHERWISE
NOTED. THE CONTRACTOR SHALL BE RESPONSIBLE FOR FIELD VERIFYING EXISTING CONDITIONS PRIOR TO
COMMENCEMENT OF ANY WORK. THE CONTRACTOR SHALL IMMEDIATELY NOTIFY THE OWNER'S REPRESENTATIVE
OF ANY DISCREPANCIES OR CONFLICTS.
3. THE CONTRACTOR SHALL BE RESPONSIBLE FOR CONTACTING, COORDINATING AND PAYMENT FOR ALL
NECESSARY LOCATING SERVICES INCLUDING INDEPENDENT LOCATING SERVICES. THE CONTRACTOR SHALL
PROVIDE NOTICE OF EXCAVATION TO NOTIFICATION CENTER AND FACILITY OWNERS (PER NC STATUTE) NO LESS
THAN 3 BUSINESS DAYS AND NO MORE THAN 12 WORKING DAYS PRIOR TO BEGINNING DEMOLITION, EXCAVATION
OR ANY OTHER FORM OF CONSTRUCTION. THE CONTRACTOR SHALL IMMEDIATELY NOTIFY THE OWNER'S
REPRESENTATIVE OF ANY DISCREPANCIES OR CONFLICTS. NO EXCAVATION OR DEMOLITION SHALL BE STARTED
WITHOUT ALL UTILITIES BEING LOCATED.
4. ALL SUB -SURFACE UTILITIES IDENTIFIED ON THE CONSTRUCTION DOCUMENTS ARE SHOWN IN THEIR APPROXIMATE
LOCATION BASED ON SURVEY INFORMATION GATHERED FROM FIELD INSPECTION AND/OR ANY OTHER APPLICABLE
RECORD DRAWINGS WHICH MAY BE AVAILABLE. THE CONTRACTOR SHALL IMMEDIATELY NOTIFY THE OWNER'S
REPRESENTATIVE OF ANY DISCREPANCIES OR CONFLICTS.
5. EXISTING IMPROVEMENTS DAMAGED OR DESTROYED BY THE CONTRACTOR DURING CONSTRUCTION SHALL BE
RESTORED OR REPLACED TO ORIGINAL CONDITION AND TO THE SATISFACTION OF THE OWNER'S REPRESENTATIVE
AT THE CONTRACTOR'S EXPENSE.
6. THE CONTRACTOR SHALL BE RESPONSIBLE FOR OBTAINING AND COORDINATING PERMITS, INSPECTIONS,
CERTIFICATIONS AND OTHER REQUIREMENTS WHICH MUST BE MET UNDER THIS CONTRACT.
7. THE CONTRACTOR SHALL MAINTAIN "AS -BUILT" DRAWINGS TO RECORD THE ACTUAL LOCATION OF ALL PIPING
PRIOR TO CONCEALMENT, VALVE AND MANHOLE CHANGES, AND HARDSCAPE OR LANDSCAPE CHANGES.
DRAWINGS SHALL BE PROVIDED TO THE OWNER'S REPRESENTATIVE AT REGULAR INTERVALS, OR AS REQUESTED
THROUGHOUT THE PROJECT FOR RECORD KEEPING.
8. IF DEPARTURES FROM THE PROJECT DRAWINGS OR SPECIFICATIONS ARE DEEMED NECESSARY BY THE
CONTRACTOR, DETAILS OF SUCH DEPARTURES AND REASONS THERE OF SHALL BE SUBMITTED TO THE OWNER'S
REPRESENTATIVE FOR REVIEW. NO DEPARTURES FROM THE CONTRACT DOCUMENTS SHALL BE MADE WITHOUT
THE EXPRESS WRITTEN PERMISSION OF THE OWNER'S REPRESENTATIVE.
9. THE CONTRACTOR SHALL BE RESPONSIBLE FOR THE RELOCATION OF ANY EXISTING UTILITY LINES REQUIRED TO
COMPLETE ANY PORTION OF CONSTRUCTION. THE CONTRACTOR SHALL ALSO BE RESPONSIBLE FOR THE
COORDINATION AND COSTS OF THE RELOCATION AND ASSOCIATED WORK.
10. THE CONTRACTOR SHALL BE RESPONSIBLE FOR KEEPING THE PREMISES FREE FROM ACCUMULATIONS OF WASTE
MATERIALS AND RUBBISH CAUSED BY THE CONTRACTOR. ALL DEBRIS SHALL BE REMOVED FROM THE PROJECT
SITE ON A DAILY BASIS.
11. THE ENGINEER AND/OR OWNER DISCLAIM ANY ROLE IN THE CONSTRUCTION MEANS AND/OR METHODS
ASSOCIATED WITH THE PROJECT AS SET FORTH IN THESE PLANS.
12. ROADWAYS (TEMPORARY OR PERMANENT) MUST BE CAPABLE OF SUPPORTING FIRE FIGHTING APPARATUS (85,000
LBS) DURING ALL PHASES OF CONSTRUCTION ONCE VERTICAL CONSTRUCTION HAS BEGUN.
SITE NOTES:
1. THE CONTRACTOR SHALL BE RESPONSIBLE FOR THE INSTALLATION AND MAINTENANCE OF THE
CONSTRUCTION LAYDOWN AREA, PERIMETER FENCE, AND ASSOCIATED GATES. THE CONTRACTOR SHALL
ALSO BE RESPONSIBLE FOR THE REMOVAL OF THE CONSTRUCTION LAYDOWN AREA PERIMETER FENCE AND
ASSOCIATED GATES AT THE COMPLETION OF THE PROJECT.
2. REFER TO VENDOR PLANS FOR TANK CONSTRUCTION DOCUMENTS
3. ALL DIMENSIONS ARE IN DECIMAL FEET TO OUTSIDE FACE OF BUILDINGS, TO CENTERLINES, AND/OR FACE OF
CURB UNLESS OTHERWISE NOTED.
4. THE CONTRACTOR SHALL VERIFY ALL DIMENSIONS AND COORDINATES AND REPORT ANY DISCREPANCIES TO
THE OWNER'S REPRESENTATIVE PRIOR TO ANY CONSTRUCTION.
5. ALL WRITTEN DIMENSIONS SHALL PREVAIL. DO NOT SCALE FROM DRAWINGS.
6. CONTRACTOR SHALL REFER TO AND COORDINATE WITH VENDOR, STRUCTURAL, AND MEP DRAWINGS AT ALL
TIMES PRIOR TO AND DURING CONSTRUCTION.
SWIFT
PARTNERS
oa�N CA ssfjo��E
= L
A PER
04MAR2021
■
HIPP ENGINEERING
& CONSULTING, INC.
2301 REXWOODS DRIVE, SUITE 200
RALEIGH, NC 27607
TEL:[phone] FAX:[phone]
NC FIRM LICENSE NUMBER: C-2146
WWW.HII'I'-USA.COM
SITE LEGEND:
SYMBOL DESCRIPTION
PROPOSED BUILDING
IFT*A... PROPOSED CONCRETE SIDEWALK
PROPOSED BRICK SIDEWALK
PROPOSED HEAVY DUTY PAVEMENT
PROPOSED CONCRETE PAVERS
PROPOSED GRAVEL
PROPOSED CURB & GUTTER
PROPOSED STOP BAR
PROPOSED CROSSWALK
PROPOSED 6' WIDE
STANDARD CROSSWALK
CROSOSSED WALKO' WIDE HIGH VISIBILITY
1111111
PROPOSED SIGN
H/C PROPOSED ADA PARKING SPACE
0 PROPOSED KEYSTONE WALL
PROPOSED CIP WALL
PROPOSED WHEEL STOP
PROPOSED GRAVEL TRAIL
- PROPOSED ASPHALT TRAIL
PROPOSED TREELINE
X PROPOSED FENCE
J_Yq PROPOSED VEHICLE GATE (X' WIDE)
❑--* PROPOSED LIGHT
PROPOSED BIKE RACK
0 PROPOSED BENCH
• PROPOSED BOLLARD
PROPOSED PEDESTRIAN STEEL PLATE
LIMITS OF DISTURBANCE
0 10 20 40
SCALE: 1" = 20'

EROSION CONTROL NOTES:
SEEDING PREPARATION:
1. CHISEL COMPACTED AREAS AND SPREAD TOPSOIL 3 INCHES DEEP OVER ADVERSE SOIL CONDITIONED, IF
AVAILABLE.
2. RIP THE ENTIRE AREA TO 6 INCHES DEPTH.
3. REMOVE ALL LOOSE ROCK, ROOTS, AND OTHER OBSTRUCTIONS LEAVING SURFACE REASONABLY SMOOTH
AND UNIFORM.
4. APPLY ALL AGRICULTURAL LIME, FERTILIZER, AND SUPERPHOSPHATE UNIFORMLY AND MIX WITH SOIL (SEE
BELOW).
5. CONTINUE TILLAGE UNTIL A WELL PULVERIZED, FIRM, REASONABLY UNIFORM 4 TO 6 INCHES DEEP SEEDBED IS
PREPARED.
6. SEED ON A FRESHLY PREPARED SEED BED AND COVER SEED LIGHTLY WITH SEEDING EQUIPMENT OR
CULTIPACK AFTER SEEDING.
7. MULCH IMMEDIATELY AFTER SEEDING AND ANCHOR MULCH.
8. INSPECT ALL SEEDED AREAS AND MAKE NECESSARY REPAIRS OR RESENDING WITHIN THE PLANTING SEASON,
IF POSSIBLE. IF STAND SHOULD BE OVER 60% DAMAGED, REESTABLISH FOLLOWING ORIGINAL LIME,
FERTILIZER AND SEEDING RATES.
TEMPORARY SEEDING PREPARATION:
1 CHISEL COMPACTED AREAS AND SPREAD TOPSOIL THREE INCHES DEEP OVER ADVERSE SOIL CONDITIONS, IF
AVAILABLE.
2. RIP THE ENTIRE AREA TO SIX INCHES DEEP.
3. REMOVE ALL LOOSE ROCK, ROOTS AND OTHER OBSTRUCTIONS, LEAVING SURFACE REASONABLY SMOOTH
AND UNIFORM.
4. APPLY AGRICULTURAL LIME, FERTILIZER AND SUPER PHOSPHATE UNIFORMLY AND MIX WITH SOIL (SEE
ADMIXTURE BELOW).
5. CONTINUE TILLAGE UNTIL A WELL -PULVERIZED, FIRM, REASONABLY UNIFORM SEEDBED IS PREPARED FOUR TO
SIX INCHES DEEP.
6. SEED ON A FRESHLY PREPARED SEEDBED AND COVER SEED LIGHTLY WITH SEEDING EQUIPMENT OR
CULTIPACK AFTER SEEDING.
7. MULCH IMMEDIATELY AFTER SEEDING AND ANCHOR MULCH.
SEQUENCE OF CONSTRUCTION ACTIVITIES:
1. DETERMINE AND MARK LIMITS OF DISTURBANCE.
2. HOLD A PRE -CONSTRUCTION CONFERENCE WITH SWIFT PARTNERS PLLC
ENGINEER 48 HOURS BEFORE GRADING ACTIVIES
3. INSTALL CONSTRUCTION ENTRANCE, SILT FENCE, PERIMETER EROSION
CONTROL DEVICES
4. REMOVE AND/OR STORE TOPSOIL.
5. BEGIN GRADING OPERATIONS. INSTALL TEMPORARY MEASURES TO SUPPORT
CONCRETE APRON AND GRAVEL DRIVE AT GRADE DISLOCATION
6. UNDERCUT AND REMOVE UNSUITABLE MATERIAL 18" BELOW BOTTOM OF
TANK SLAB ELEVATION. REPLACE WITH SELECT BACKFILL MATERIAL.
7. GRADE SITE TO EROSION CONTROL PHASE II ELEVATION. CREATE 15, CLEAR
PATH AROUND PROPOSED TANK LOCATION
8. CONSTRUCT TANK AND PIPE BRIDGE STRUCTURE PER PLANS (BY OTHERS)
9. BRING GRADE TO FINISHED ELEVATION
10. PLACE TEMPORARY SEEDING ON ALL DISTURBED AREAS THAT WILL BE IDLE
14 DAYS OR LONGER.
11. PERMANENT SURFACE STABILIZATION SHALL BE INSTALLED FOR ALL AREAS
WITHIN 14 DAYS AFTER FINAL GRADE HAS BEEN REACHED. AS NECESSARY,
FERTILIZE, WATER AND RESEED AS REQUIRED TO ESTABLISH AND MAINTAIN
A VIGOROUS STAND OF GRASS.
12. AFTER COMPLETION OF CONSTRUCTION AND THE SITE IS STABILIZED,
REMOVE TEMPORARY EROSION CONTROL MEASURES, SMOOTH AREA AND
APPLY APPROPRIATE STABILIZATION.
1. ALL EROSION CONTROL MEASURES SHALL BE INSTALLED IN BEST LOCATION BASED ON FIELD CONDITIONS.
2. THE CONTRACTOR SHALL BE RESPONSIBLE FOR THE INSTALLATION AND MAINTENANCE OF ALL EROSION CONTROL
MEASURES THROUGHOUT THE DURATION OF CONSTRUCTION.
3. THE CONTRACTOR SHALL BE RESPONSIBLE FOR THE INSTALLATION OF CONSTRUCTION ENTRANCES AS NECESSARY
TO PREVENT THE TRACKING OF SEDIMENT OFF -SITE. THE OWNER IS RESPONSIBLE FOR MAINTENANCE OF ALL
PERMANENT EROSION CONTROL METHODS AFTER CONSTRUCTION IS COMPLETE, IF ANY PERMANENT METHODS
ARE REQUIRED.
4. APPROVAL OF THIS EROSION AND SEDIMENTATION CONTROL (ESC) PLAN DOES NOT CONSTITUTE AN APPROVAL OF
DRAINAGE DESIGN (E.G., SIZE AND LOCATION OF ROADS, PIPES, RESTRICTORS, CHANNELS, RETENTION FACILITIES,
UTILITIES, ETC.).
5. THE IMPLEMENTATION OF THESE ESC PLANS AND THE CONSTRUCTION, MAINTENANCE, REPLACEMENT, AND
UPGRADING OF THESE ESC FACILITIES IS THE RESPONSIBILITY OF THE CONTRACTOR AND ESC SUPERVISOR UNTIL
ALL CONSTRUCTION IS APPROVED.
6. DURING THE CONSTRUCTION PERIOD, NO DISTURBANCE BEYOND THE LIMITS OF DISTURBANCE (L.O.D.) SHALL BE
PERMITTED. THE L.O.D. SHALL BE MAINTAINED BY THE ESC SUPERVISOR FOR THE DURATION OF CONSTRUCTION.
7. THE ESC FACILITIES SHOWN ON THIS PLAN MUST BE CONSTRUCTED PRIOR TO OR IN CONJUNCTION WITH ALL
CLEARING AND GRADING SO AS TO ENSURE THAT THE TRANSPORT OF SEDIMENT TO DRAINAGE SYSTEMS, AND
ADJACENT PROPERTIES IS MINIMIZED.
8. THE ESC FACILITIES SHOWN ON THIS PLAN ARE THE MINIMUM REQUIREMENTS FOR ANTICIPATED SITE CONDITIONS.
DURING THE CONSTRUCTION PERIOD, THESE ESC FACILITIES SHALL BE UPGRADED AS NEEDED FOR UNEXPECTED
STORM EVENTS AND MODIFIED TO ACCOUNT FOR CHANGING SITE CONDITIONS (E.G., ADDITIONAL SUMP PUMPS,
RELOCATION OF DITCHES AND SILT FENCES, ETC.).
9. THE ESC FACILITIES SHALL BE INSPECTED DAILY BY THE ESC SUPERVISOR AND MAINTAINED TO ENSURE CONTINUED
PROPER FUNCTIONING. WRITTEN RECORDS SHALL BE MAINTAINED BY THE CONTRACTOR THROUGHOUT THE
DURATION OF THE PROJECT. COPIES OF THE WRITTEN INSPECTION REPORTS SHALL BE PROVIDED TO THE OWNER'S
REPRESENTATIVE TWICE PER WEEK AND AFTER RAINS OF GREATER THAN 0.5". RAIN GAUGE REQUIRED ON SITE.
10. ANY AREAS OF EXPOSED SOILS THAT WILL NOT BE DISTURBED FOR FOURTEEN DAYS SHALL BE IMMEDIATELY
STABILIZED WITH THE APPROVED ESC METHODS (E.G., SEEDING, MULCHING, PLASTIC COVERING, ETC.).
11. THE ESC FACILITIES ON INACTIVE SITES SHALL BE INSPECTED AND MAINTAINED A MINIMUM OF ONCE A MONTH OR
WITHIN FORTY EIGHT (48) HOURS FOLLOWING A STORM EVENT.
12. AT NO TIME SHALL MORE THAN ONE (1) FOOT OF SEDIMENT BE ALLOWED TO ACCUMULATE WITHIN A CATCH BASIN.
ALL CATCH BASINS AND CONVEYANCE LINES SHALL BE CLEANED PRIOR TO PAVING. THE CLEANING OPERATION
SHALL NOT FLUSH SEDIMENT LADEN WATER INTO THE DOWNSTREAM SYSTEM.
13. STABILIZED CONSTRUCTION ENTRANCES AND ROADS SHALL BE INSTALLED AT THE BEGINNING OF CONSTRUCTION
AND MAINTAINED FOR THE DURATION OF THE PROJECT. ADDITIONAL MEASURES, SUCH AS WASH PADS, MAY BE
REQUIRED TO ENSURE THAT ALL PAVED AREAS ARE KEPT CLEAN FOR THE DURATION OF THE PROJECT.
14. WHERE STRAW MULCH FOR TEMPORARY EROSION CONTROL IS REQUIRED, IT SHALL BE A MINIMUM THICKNESS OF 2
TO 3 INCHES.
15. INTERIM SLOPES MAY BE GRADED TO A MAXIMUM SLOPE OF 2:1 (HORIZONTAL: VERTICAL); CUT SLOPES SHALL BE
LIMITED TO A MAXIMUM SLOPE OF 1.5:1.
16. THE SURFACE OF AREAS SLOPES STEEPER THAN 1 VERTICAL TO 4 HORIZONTAL THAT ARE TO RECEIVE INTERIM FILL
SHALL BE PLOWED, FURROWED, TILLED OR BROKEN UP PRIOR TO PLACING FILL SO THAT FILL MATERIAL WILL BOND
WITH EXISTING. " SURFACE. INTERIM FILL SHALL BE PLACED AS SPECIFIED FOR PERMANENT FILLS AND IN LIFTS NOT
GREATER THAN 6".
17. PROVIDE DUST CONTROL MEASURES INCLUDING, BUT NOT LIMITED TO, WETTING DOWN TO CONTROL DUST ON SITE,
IN ORDER TO PREVENT ANNOYANCE/AND OR DAMAGE TO ADJACENT SITES. CALCIUM CHLORIDE OR ANY OTHER
CHEMICAL MATERIAL MAY NOT BE USED ON SUBGRADES OF AREAS TO BE SEEDED OR PLANTED.
18. SEDIMENT LADEN RUNOFF FROM EXCAVATIONS SHALL NOT BE PUMPED DIRECTLY TO STORM DRAINAGE.
19. CONSTRUCTION AND MAINTENANCE OF ALL EROSION CONTROL DEVICES SHALL CONFORM TO THE STANDARDS SET
FORTH IN THE NORTH CAROLINA DEPARTMENT OF ENVIRONMENT, HEALTH AND NATURAL RESOURCES LAND
QUALITY SECTION EROSION AND SEDIMENT CONTROL PLANNING LAND DESIGN MANUAL.
EROSION CONTROL LEGEND:
SYMBOL DESCRIPTION
LIMITS OF DISTURBANCE
SF
SILT FENCE
TP
TREE PROTECTION
DD
DIVERSION DITCH
- - - -
100 YR FLOOD ELEV.
BLOCK & GRAVEL INLET PROTECTION
IP
QSILT
IP
FENCE AND WIRE INLET PROTECTION
HORSE SHOE INLET PROTECTION
SILT FENCE OUTLET
CHECK DAM
FLARED END SECTION (FES)
SEDIMENT TRAP
RIPRAP DISSIPATER
WID°DDp°D
TEMPORARY CONSTRUCTION ENTRANCE
U.DDD �°OD
v p�V p DD
ALL CONSTRUCTION SHALL BE IN ACCORDANCE WITH NORTH
CAROLINA EROSION CONTROL SPECIFICATIONS
STRUCTURAL BACKFILL MATERIAL REQUIREMENTS - SEE GEOTECH REPORT FOR FULL DETAILS
1. NO DELETERIOUS MATERIAL
2. NO ROCKS GREATER THAN 3 INCHES IN DIAMETER OR GREATER THAN 30%
RETAINED ON THE %-INCH SIEVE.
3. MAXIMUM DRY DENSITY (MDD) OF 95 POUNDS PER CUBIC FOOT (PCF) OR
GREATER, AS DETERMINED BY THE STANDARD PROCTOR COMPACTION TEST
(ASTM D698)
4. LIQUID LIMIT (LL) OF 50 OR LESS AND A PLASTICITY INDEX (PI) OF 25 OR LESS,
AS DETERMINED BY ATTERBERG LIMIT TESTING (ASTM D4318)
5. ORGANIC CONTENT NO GREATER THAN 3%
6. COMPACT STRUCTURAL FILL TO 98% OF THE SOILS MAXIMUM DRY DENSITY
6.1. 8-10" LIFTS USING LARGE RIDE -ON COMPACTORS
6.2. 4-6" LIFTS USING RAMMAX-TYPE COMPACTRS
6.3. NO MORE THAN 4" LIFT USING SLED OR JUMPING -JACK TAMPERS
JSWIFT
PARTNERS
1�A CA f30j(4
O0 10 20 40
_- -_ SCALE: 1" = 20' NORTH
04MAR2021
■A 03-04-21 LAP LAP ISSUED FOR CONSTRUCTION
F Rev.: IRev. date: I Dwg I I Revisions:
Novozymes North America, Inc.
- - - - -- - - 77 Perry Chapel Church Road
P.O. Box 576
HIPP ENGINEERING
& CONSULTING, INC.
2301 REXWOODS DRIVE, SUITE 200
RALEIGH, NC 27607
TEL:[phone] FAX:[phone]
NC FIRM LICENSE NUMBER: C-2146
WWW.HIPP-USA.COM

EROSION CONTROL NOTES:
SEEDING PREPARATION: TEMPORARY SEEDING PREPARATION:
1
1. CHISEL COMPACTED AREAS AND SPREAD TOPSOIL 3 INCHES DEEP OVER ADVERSE SOIL CONDITIONED, IF CHISEL COMPACTED AREAS AND SPREAD TOPSOIL THREE INCHES DEEP OVER ADVERSE SOIL CONDITIONS, IFAVAILABLE.
AVAILABLE.
2. RIP THE ENTIRE AREA TO SIX INCHES DEEP.
2. RIP THE ENTIRE AREA TO 6 INCHES DEPTH.
3. REMOVE ALL LOOSE ROCK, ROOTS, AND OTHER OBSTRUCTIONS LEAVING SURFACE REASONABLY SMOOTH 3. REMOVE ALL LOOSE ROCK, ROOTS AND OTHER OBSTRUCTIONS, LEAVING SURFACE REASONABLY SMOOTH
AND UNIFORM. AND UNIFORM.
4. APPLY ALL AGRICULTURAL LIME, FERTILIZER, AND SUPERPHOSPHATE UNIFORMLY AND MIX WITH SOIL (SEE 4. APPLY AGRICULTURAL LIME, FERTILIZER AND SUPER PHOSPHATE UNIFORMLY AND MIX WITH SOIL (SEE
BELOW). ADMIXTURE BELOW).
5. CONTINUE TILLAGE UNTIL A WELL PULVERIZED, FIRM, REASONABLY UNIFORM 4 TO 6 INCHES DEEP SEEDBED IS 5. CONTINUE TILLAGE UNTIL A WELL -PULVERIZED, FIRM, REASONABLY UNIFORM SEEDBED IS PREPARED FOUR TO
PREPARED. SIX INCHES DEEP.
6. SEED ON A FRESHLY PREPARED SEED BED AND COVER SEED LIGHTLY WITH SEEDING EQUIPMENT OR 6. SEED ON A FRESHLY PREPARED SEEDBED AND COVER SEED LIGHTLY WITH SEEDING EQUIPMENT OR
CULTIPACK AFTER SEEDING. CULTIPACK AFTER SEEDING.
7. MULCH IMMEDIATELY AFTER SEEDING AND ANCHOR MULCH.
8. INSPECT ALL SEEDED AREAS AND MAKE NECESSARY REPAIRS OR RESENDING WITHIN THE PLANTING SEASON,
IF POSSIBLE. IF STAND SHOULD BE OVER 60% DAMAGED, REESTABLISH FOLLOWING ORIGINAL LIME,
FERTILIZER AND SEEDING RATES.
9. INSPECT ALL SEEDED AREAS AND MAKE NECESSARY REPAIRS OR RESENDING WITHIN THE PLANTING SEASON,
IF POSSIBLE. IF STAND SHOULD BE OVER 50% DAMAGED, REESTABLISH FOLLOWING ORIGINAL LIME,
FERTILIZER AND SEEDING RATES AND LANDSCAPING PLANS.
10. SEE LANDSCAPING PLANS FOR PERMANENT SEEDING, MULCHING, AND FERTILIZING RATES. ALL AREAS NOT
DESIGNATED TO RECEIVE PLANTS SHALL BE SEEDED PER THE LANDSCAPING PLANS.
SEQUENCE OF CONSTRUCTION ACTIVITIES:
1. DETERMINE AND MARK LIMITS OF DISTURBANCE.
2. HOLD A PRE -CONSTRUCTION CONFERENCE WITH SWIFT PARTNERS PLLC
ENGINEER 48 HOURS BEFORE GRADING ACTIVIES
3. INSTALL CONSTRUCTION ENTRANCE, SILT FENCE, PERIMETER EROSION
CONTROL DEVICES
4. REMOVE AND/OR STORE TOPSOIL.
5. BEGIN GRADING OPERATIONS. INSTALL TEMPORARY MEASURES TO SUPPORT
CONCRETE APRON AND GRAVEL DRIVE AT GRADE DISLOCATION
6. UNDERCUT AND REMOVE UNSUITABLE MATERIAL 18" BELOW BOTTOM OF
TANK SLAB ELEVATION. REPLACE WITH SELECT BACKFILL MATERIAL.
7. GRADE SITE TO EROSION CONTROL PHASE II ELEVATION. CREATE 15, CLEAR
PATH AROUND PROPOSED TANK LOCATION
8. CONSTRUCT TANK AND PIPE BRIDGE STRUCTURE PER PLANS (BY OTHERS)
9. BRING GRADE TO FINISHED ELEVATION
10. PLACE TEMPORARY SEEDING ON ALL DISTURBED AREAS THAT WILL BE IDLE
14 DAYS OR LONGER.
11. PERMANENT SURFACE STABILIZATION SHALL BE INSTALLED FOR ALL AREAS
WITHIN 14 DAYS AFTER FINAL GRADE HAS BEEN REACHED. AS NECESSARY,
FERTILIZE, WATER AND RESEED AS REQUIRED TO ESTABLISH AND MAINTAIN
A VIGOROUS STAND OF GRASS.
12. AFTER COMPLETION OF CONSTRUCTION AND THE SITE IS STABILIZED,
REMOVE TEMPORARY EROSION CONTROL MEASURES, SMOOTH AREA AND
APPLY APPROPRIATE STABILIZATION.
EROSION CONTROL LEGEND:
SYMBOL
DESCRIPTION
1. ALL EROSION CONTROL MEASURES SHALL BE INSTALLED IN BEST LOCATION BASED ON FIELD CONDITIONS.
2. THE CONTRACTOR SHALL BE RESPONSIBLE FOR THE INSTALLATION AND MAINTENANCE OF ALL EROSION CONTROL
LIMITS OF DISTURBANCE
MEASURES THROUGHOUT THE DURATION OF CONSTRUCTION.
SF
SILT FENCE
3. THE CONTRACTOR SHALL BE RESPONSIBLE FOR THE INSTALLATION OF CONSTRUCTION ENTRANCES AS NECESSARY
TP
TREE PROTECTION
TO PREVENT THE TRACKING OF SEDIMENT OFF -SITE. THE OWNER IS RESPONSIBLE FOR MAINTENANCE OF ALL
DD
DIVERSION DITCH
PERMANENT EROSION CONTROL METHODS AFTER CONSTRUCTION IS COMPLETE, IF ANY PERMANENT METHODS
- - - -
100 YR FLOOD ELEV.
ARE REQUIRED.
�q
I I
BLOCK &GRAVEL INLET PROTECTION
4. APPROVAL OF THIS EROSION AND SEDIMENTATION CONTROL (ESC) PLAN DOES NOT CONSTITUTE AN APPROVAL OF
Fd /P
DRAINAGE DESIGN (E.G., SIZE AND LOCATION OF ROADS, PIPES, RESTRICTORS, CHANNELS, RETENTION FACILITIES,
UTILITIES, ETC.).
0
SILT FENCE AND WIRE INLET PROTECTION
5. THE IMPLEMENTATION OF THESE ESC PLANS AND THE CONSTRUCTION, MAINTENANCE, REPLACEMENT, AND
IP
UPGRADING OF THESE ESC FACILITIES IS THE RESPONSIBILITY OF THE CONTRACTOR AND ESC SUPERVISOR UNTIL
ALL CONSTRUCTION IS APPROVED.
HORSE SHOE INLET PROTECTION
6. DURING THE CONSTRUCTION PERIOD, NO DISTURBANCE BEYOND THE LIMITS OF DISTURBANCE (L.O.D.) SHALL BE
-_
SILT FENCE OUTLET
PERMITTED. THE L.O.D. SHALL BE MAINTAINED BY THE ESC SUPERVISOR FOR THE DURATION OF CONSTRUCTION.
CHECK DAM
7. THE ESC FACILITIES SHOWN ON THIS PLAN MUST BE CONSTRUCTED PRIOR TO OR IN CONJUNCTION WITH ALL
CLEARING AND GRADING SO AS TO ENSURE THAT THE TRANSPORT OF SEDIMENT TO DRAINAGE SYSTEMS, AND
ADJACENT PROPERTIES IS MINIMIZED.
FLARED END SECTION (FES)
8. THE ESC FACILITIES SHOWN ON THIS PLAN ARE THE MINIMUM REQUIREMENTS FOR ANTICIPATED SITE CONDITIONS.
DURING THE CONSTRUCTION PERIOD, THESE ESC FACILITIES SHALL BE UPGRADED AS NEEDED FOR UNEXPECTED
SEDIMENT TRAP
STORM EVENTS AND MODIFIED TO ACCOUNT FOR CHANGING SITE CONDITIONS (E.G., ADDITIONAL SUMP PUMPS,
RELOCATION OF DITCHES AND SILT FENCES, ETC.).
RIPRAP DISSIPATER
9. THE ESC FACILITIES SHALL BE INSPECTED DAILY BY THE ESC SUPERVISOR AND MAINTAINED TO ENSURE CONTINUED
PROPER FUNCTIONING. WRITTEN RECORDS SHALL BE MAINTAINED BY THE CONTRACTOR THROUGHOUT THE
W
DURATION OF THE PROJECT. COPIES OF THE WRITTEN INSPECTION REPORTS SHALL BE PROVIDED TO THE OWNER'S
1 ° o o p° o°
TEMPORARY CONSTRUCTION ENTRANCE
REPRESENTATIVE TWICE PER WEEK AND AFTER RAINS OF GREATER THAN 0.5". RAIN GAUGE REQUIRED ON SITE.
10. ANY AREAS OF EXPOSED SOILS THAT WILL NOT BE DISTURBED FOR FOURTEEN DAYS SHALL BE IMMEDIATELY
STABILIZED WITH THE APPROVED ESC METHODS (E.G., SEEDING, MULCHING, PLASTIC COVERING, ETC.).
11. THE ESC FACILITIES ON INACTIVE SITES SHALL BE INSPECTED AND MAINTAINED A MINIMUM OF ONCE A MONTH OR
WITHIN FORTY EIGHT (48) HOURS FOLLOWING A STORM EVENT.
12. AT NO TIME SHALL MORE THAN ONE (1) FOOT OF SEDIMENT BE ALLOWED TO ACCUMULATE WITHIN A CATCH BASIN.
ALL CATCH BASINS AND CONVEYANCE LINES SHALL BE CLEANED PRIOR TO PAVING. THE CLEANING OPERATION
SHALL NOT FLUSH SEDIMENT LADEN WATER INTO THE DOWNSTREAM SYSTEM.
13. STABILIZED CONSTRUCTION ENTRANCES AND ROADS SHALL BE INSTALLED AT THE BEGINNING OF CONSTRUCTION
AND MAINTAINED FOR THE DURATION OF THE PROJECT. ADDITIONAL MEASURES, SUCH AS WASH PADS, MAY BE
REQUIRED TO ENSURE THAT ALL PAVED AREAS ARE KEPT CLEAN FOR THE DURATION OF THE PROJECT.
14. WHERE STRAW MULCH FOR TEMPORARY EROSION CONTROL IS REQUIRED, IT SHALL BE A MINIMUM THICKNESS OF 2
TO 3 INCHES.
15. INTERIM SLOPES MAY BE GRADED TO A MAXIMUM SLOPE OF 2:1 (HORIZONTAL: VERTICAL); CUT SLOPES SHALL BE
LIMITED TO A MAXIMUM SLOPE OF 1.5:1.
16. THE SURFACE OF AREAS SLOPES STEEPER THAN 1 VERTICAL TO 4 HORIZONTAL THAT ARE TO RECEIVE INTERIM FILL
SHALL BE PLOWED, FURROWED, TILLED OR BROKEN UP PRIOR TO PLACING FILL SO THAT FILL MATERIAL WILL BOND
WITH EXISTING. " SURFACE. INTERIM FILL SHALL BE PLACED AS SPECIFIED FOR PERMANENT FILLS AND IN LIFTS NOT
GREATER THAN 6".
17. PROVIDE DUST CONTROL MEASURES INCLUDING, BUT NOT LIMITED TO, WETTING DOWN TO CONTROL DUST ON SITE,
IN ORDER TO PREVENT ANNOYANCE/AND OR DAMAGE TO ADJACENT SITES. CALCIUM CHLORIDE OR ANY OTHER
CHEMICAL MATERIAL MAY NOT BE USED ON SUBGRADES OF AREAS TO BE SEEDED OR PLANTED.
18. SEDIMENT LADEN RUNOFF FROM EXCAVATIONS SHALL NOT BE PUMPED DIRECTLY TO STORM DRAINAGE.
19. CONSTRUCTION AND MAINTENANCE OF ALL EROSION CONTROL DEVICES SHALL CONFORM TO THE STANDARDS SET
FORTH IN THE NORTH CAROLINA DEPARTMENT OF ENVIRONMENT, HEALTH AND NATURAL RESOURCES LAND
QUALITY SECTION EROSION AND SEDIMENT CONTROL PLANNING LAND DESIGN MANUAL.
ALL CONSTRUCTION SHALL BE IN ACCORDANCE WITH NORTH
CAROLINA EROSION CONTROL SPECIFICATIONS
STRUCTURAL BACKFILL MATERIAL REQUIREMENTS - SEE GEOTECH REPORT FOR FULL DETAILS
1. NO DELETERIOUS MATERIAL
2. NO ROCKS GREATER THAN 3 INCHES IN DIAMETER OR GREATER THAN 30%
RETAINED ON THE 3/4-INCH SIEVE.
3. MAXIMUM DRY DENSITY (MDD) OF 95 POUNDS PER CUBIC FOOT (PCF) OR
GREATER, AS DETERMINED BY THE STANDARD PROCTOR COMPACTION TEST
(ASTM D698)
4. LIQUID LIMIT (LL) OF 50 OR LESS AND A PLASTICITY INDEX (PI) OF 25 OR LESS,
AS DETERMINED BY ATTERBERG LIMIT TESTING (ASTM D4318)
5. ORGANIC CONTENT NO GREATER THAN 3%
6. COMPACT STRUCTURAL FILL TO 98% OF THE SOILS MAXIMUM DRY DENSITY
6.1. 8-10" LIFTS USING LARGE RIDE -ON COMPACTORS
6.2. 4-6" LIFTS USING RAMMAX-TYPE COMPACTRS
6.3. NO MORE THAN 4" LIFT USING SLED OR JUMPING -JACK TAMPERS
SWIFT
PARTNERS
10 . 9
L�
A PER
04MAR2021
■
HIPP ENGINEERING
& CONSULTING, INC.
2301 REXWOODS DRIVE, SUITE 200
RALEIGH, NC 27607
TEL:[phone] FAX:[phone]
NC FIRM LICENSE NUMBER: C-2146
WWW.HII'I'-USA.COM
7m�� 0 ("-r
0 10 20 40
SCALE: 1" = 20' NORTH

EROSION CONTROL NOTES:
SEEDING PREPARATION:
1. CHISEL COMPACTED AREAS AND SPREAD TOPSOIL 3 INCHES DEEP OVER ADVERSE SOIL CONDITIONED, IF
AVAILABLE.
2. RIP THE ENTIRE AREA TO 6 INCHES DEPTH.
3. REMOVE ALL LOOSE ROCK, ROOTS, AND OTHER OBSTRUCTIONS LEAVING SURFACE REASONABLY SMOOTH
AND UNIFORM.
4. APPLY ALL AGRICULTURAL LIME, FERTILIZER, AND SUPERPHOSPHATE UNIFORMLY AND MIX WITH SOIL (SEE
BELOW).
5. CONTINUE TILLAGE UNTIL A WELL PULVERIZED, FIRM, REASONABLY UNIFORM 4 TO 6 INCHES DEEP SEEDBED IS
PREPARED.
6. SEED ON A FRESHLY PREPARED SEED BED AND COVER SEED LIGHTLY WITH SEEDING EQUIPMENT OR
CULTIPACK AFTER SEEDING.
7. MULCH IMMEDIATELY AFTER SEEDING AND ANCHOR MULCH.
8. INSPECT ALL SEEDED AREAS AND MAKE NECESSARY REPAIRS OR RESENDING WITHIN THE PLANTING SEASON,
IF POSSIBLE. IF STAND SHOULD BE OVER 60% DAMAGED, REESTABLISH FOLLOWING ORIGINAL LIME,
FERTILIZER AND SEEDING RATES.
9. INSPECT ALL SEEDED AREAS AND MAKE NECESSARY REPAIRS OR RESENDING WITHIN THE PLANTING SEASON,
IF POSSIBLE. IF STAND SHOULD BE OVER 50% DAMAGED, REESTABLISH FOLLOWING ORIGINAL LIME,
FERTILIZER AND SEEDING RATES AND LANDSCAPING PLANS.
10. SEE LANDSCAPING PLANS FOR PERMANENT SEEDING, MULCHING, AND FERTILIZING RATES. ALL AREAS NOT
DESIGNATED TO RECEIVE PLANTS SHALL BE SEEDED PER THE LANDSCAPING PLANS.
TEMPORARY SEEDING PREPARATION:
1 CHISEL COMPACTED AREAS AND SPREAD TOPSOIL THREE INCHES DEEP OVER ADVERSE SOIL CONDITIONS, IF
AVAILABLE.
2. RIP THE ENTIRE AREA TO SIX INCHES DEEP.
3. REMOVE ALL LOOSE ROCK, ROOTS AND OTHER OBSTRUCTIONS, LEAVING SURFACE REASONABLY SMOOTH
AND UNIFORM.
4. APPLY AGRICULTURAL LIME, FERTILIZER AND SUPER PHOSPHATE UNIFORMLY AND MIX WITH SOIL (SEE
ADMIXTURE BELOW).
5. CONTINUE TILLAGE UNTIL A WELL -PULVERIZED, FIRM, REASONABLY UNIFORM SEEDBED IS PREPARED FOUR TO
SIX INCHES DEEP.
6. SEED ON A FRESHLY PREPARED SEEDBED AND COVER SEED LIGHTLY WITH SEEDING EQUIPMENT OR
CULTIPACK AFTER SEEDING.
SEQUENCE OF CONSTRUCTION ACTIVITIES:
1. DETERMINE AND MARK LIMITS OF DISTURBANCE.
2. HOLD A PRE -CONSTRUCTION CONFERENCE WITH SWIFT PARTNERS PLLC
ENGINEER 48 HOURS BEFORE GRADING ACTIVIES
3. INSTALL CONSTRUCTION ENTRANCE, SILT FENCE, PERIMETER EROSION
CONTROL DEVICES
4. REMOVE AND/OR STORE TOPSOIL.
5. BEGIN GRADING OPERATIONS. INSTALL TEMPORARY MEASURES TO SUPPORT
CONCRETE APRON AND GRAVEL DRIVE AT GRADE DISLOCATION
6. UNDERCUT AND REMOVE UNSUITABLE MATERIAL 18" BELOW BOTTOM OF
TANK SLAB ELEVATION. REPLACE WITH SELECT BACKFILL MATERIAL.
7. GRADE SITE TO EROSION CONTROL PHASE II ELEVATION. CREATE 15, CLEAR
PATH AROUND PROPOSED TANK LOCATION
8. CONSTRUCT TANK AND PIPE BRIDGE STRUCTURE PER PLANS (BY OTHERS)
9. BRING GRADE TO FINISHED ELEVATION
10. PLACE TEMPORARY SEEDING ON ALL DISTURBED AREAS THAT WILL BE IDLE
14 DAYS OR LONGER.
11. PERMANENT SURFACE STABILIZATION SHALL BE INSTALLED FOR ALL AREAS
WITHIN 14 DAYS AFTER FINAL GRADE HAS BEEN REACHED. AS NECESSARY,
FERTILIZE, WATER AND RESEED AS REQUIRED TO ESTABLISH AND MAINTAIN
A VIGOROUS STAND OF GRASS.
12. AFTER COMPLETION OF CONSTRUCTION AND THE SITE IS STABILIZED,
REMOVE TEMPORARY EROSION CONTROL MEASURES, SMOOTH AREA AND
APPLY APPROPRIATE STABILIZATION.
1. ALL EROSION CONTROL MEASURES SHALL BE INSTALLED IN BEST LOCATION BASED ON FIELD CONDITIONS.
2. THE CONTRACTOR SHALL BE RESPONSIBLE FOR THE INSTALLATION AND MAINTENANCE OF ALL EROSION CONTROL
MEASURES THROUGHOUT THE DURATION OF CONSTRUCTION.
3. THE CONTRACTOR SHALL BE RESPONSIBLE FOR THE INSTALLATION OF CONSTRUCTION ENTRANCES AS NECESSARY
TO PREVENT THE TRACKING OF SEDIMENT OFF -SITE. THE OWNER IS RESPONSIBLE FOR MAINTENANCE OF ALL
PERMANENT EROSION CONTROL METHODS AFTER CONSTRUCTION IS COMPLETE, IF ANY PERMANENT METHODS
ARE REQUIRED.
4. APPROVAL OF THIS EROSION AND SEDIMENTATION CONTROL (ESC) PLAN DOES NOT CONSTITUTE AN APPROVAL OF
DRAINAGE DESIGN (E.G., SIZE AND LOCATION OF ROADS, PIPES, RESTRICTORS, CHANNELS, RETENTION FACILITIES,
UTILITIES, ETC.).
5. THE IMPLEMENTATION OF THESE ESC PLANS AND THE CONSTRUCTION, MAINTENANCE, REPLACEMENT, AND
UPGRADING OF THESE ESC FACILITIES IS THE RESPONSIBILITY OF THE CONTRACTOR AND ESC SUPERVISOR UNTIL
ALL CONSTRUCTION IS APPROVED.
6. DURING THE CONSTRUCTION PERIOD, NO DISTURBANCE BEYOND THE LIMITS OF DISTURBANCE (L.O.D.) SHALL BE
PERMITTED. THE L.O.D. SHALL BE MAINTAINED BY THE ESC SUPERVISOR FOR THE DURATION OF CONSTRUCTION.
7. THE ESC FACILITIES SHOWN ON THIS PLAN MUST BE CONSTRUCTED PRIOR TO OR IN CONJUNCTION WITH ALL
CLEARING AND GRADING SO AS TO ENSURE THAT THE TRANSPORT OF SEDIMENT TO DRAINAGE SYSTEMS, AND
ADJACENT PROPERTIES IS MINIMIZED.
8. THE ESC FACILITIES SHOWN ON THIS PLAN ARE THE MINIMUM REQUIREMENTS FOR ANTICIPATED SITE CONDITIONS.
DURING THE CONSTRUCTION PERIOD, THESE ESC FACILITIES SHALL BE UPGRADED AS NEEDED FOR UNEXPECTED
STORM EVENTS AND MODIFIED TO ACCOUNT FOR CHANGING SITE CONDITIONS (E.G., ADDITIONAL SUMP PUMPS,
RELOCATION OF DITCHES AND SILT FENCES, ETC.).
9. THE ESC FACILITIES SHALL BE INSPECTED DAILY BY THE ESC SUPERVISOR AND MAINTAINED TO ENSURE CONTINUED
PROPER FUNCTIONING. WRITTEN RECORDS SHALL BE MAINTAINED BY THE CONTRACTOR THROUGHOUT THE
DURATION OF THE PROJECT. COPIES OF THE WRITTEN INSPECTION REPORTS SHALL BE PROVIDED TO THE OWNER'S
REPRESENTATIVE TWICE PER WEEK AND AFTER RAINS OF GREATER THAN 0.5". RAIN GAUGE REQUIRED ON SITE.
10. ANY AREAS OF EXPOSED SOILS THAT WILL NOT BE DISTURBED FOR FOURTEEN DAYS SHALL BE IMMEDIATELY
STABILIZED WITH THE APPROVED ESC METHODS (E.G., SEEDING, MULCHING, PLASTIC COVERING, ETC.).
11. THE ESC FACILITIES ON INACTIVE SITES SHALL BE INSPECTED AND MAINTAINED A MINIMUM OF ONCE A MONTH OR
WITHIN FORTY EIGHT (48) HOURS FOLLOWING A STORM EVENT.
12. AT NO TIME SHALL MORE THAN ONE (1) FOOT OF SEDIMENT BE ALLOWED TO ACCUMULATE WITHIN A CATCH BASIN.
ALL CATCH BASINS AND CONVEYANCE LINES SHALL BE CLEANED PRIOR TO PAVING. THE CLEANING OPERATION
SHALL NOT FLUSH SEDIMENT LADEN WATER INTO THE DOWNSTREAM SYSTEM.
13. STABILIZED CONSTRUCTION ENTRANCES AND ROADS SHALL BE INSTALLED AT THE BEGINNING OF CONSTRUCTION
AND MAINTAINED FOR THE DURATION OF THE PROJECT. ADDITIONAL MEASURES, SUCH AS WASH PADS, MAY BE
REQUIRED TO ENSURE THAT ALL PAVED AREAS ARE KEPT CLEAN FOR THE DURATION OF THE PROJECT.
14. WHERE STRAW MULCH FOR TEMPORARY EROSION CONTROL IS REQUIRED, IT SHALL BE A MINIMUM THICKNESS OF 2
TO 3 INCHES.
15. INTERIM SLOPES MAY BE GRADED TO A MAXIMUM SLOPE OF 2:1 (HORIZONTAL: VERTICAL); CUT SLOPES SHALL BE
LIMITED TO A MAXIMUM SLOPE OF 1.5:1.
16. THE SURFACE OF AREAS SLOPES STEEPER THAN 1 VERTICAL TO 4 HORIZONTAL THAT ARE TO RECEIVE INTERIM FILL
SHALL BE PLOWED, FURROWED, TILLED OR BROKEN UP PRIOR TO PLACING FILL SO THAT FILL MATERIAL WILL BOND
WITH EXISTING. " SURFACE. INTERIM FILL SHALL BE PLACED AS SPECIFIED FOR PERMANENT FILLS AND IN LIFTS NOT
GREATER THAN 6".
17. PROVIDE DUST CONTROL MEASURES INCLUDING, BUT NOT LIMITED TO, WETTING DOWN TO CONTROL DUST ON SITE,
IN ORDER TO PREVENT ANNOYANCE/AND OR DAMAGE TO ADJACENT SITES. CALCIUM CHLORIDE OR ANY OTHER
CHEMICAL MATERIAL MAY NOT BE USED ON SUBGRADES OF AREAS TO BE SEEDED OR PLANTED.
18. SEDIMENT LADEN RUNOFF FROM EXCAVATIONS SHALL NOT BE PUMPED DIRECTLY TO STORM DRAINAGE.
19. CONSTRUCTION AND MAINTENANCE OF ALL EROSION CONTROL DEVICES SHALL CONFORM TO THE STANDARDS SET
FORTH IN THE NORTH CAROLINA DEPARTMENT OF ENVIRONMENT, HEALTH AND NATURAL RESOURCES LAND
QUALITY SECTION EROSION AND SEDIMENT CONTROL PLANNING LAND DESIGN MANUAL.
EROSION CONTROL LEGEND:
SYMBOL DESCRIPTION
LIMITS OF DISTURBANCE
SF
SILT FENCE
TP
TREE PROTECTION
DD
DIVERSION DITCH
- - - -
100 YR FLOOD ELEV.
BLOCK & GRAVEL INLET PROTECTION
IP
0
IP
SILT FENCE AND WIRE INLET PROTECTION
HORSE SHOE INLET PROTECTION
SILT FENCE OUTLET
CHECK DAM
FLARED END SECTION (FES)
SEDIMENT TRAP
r"
RIPRAP DISSIPATER
W
TEMPORARY CONSTRUCTION ENTRANCE
ALL CONSTRUCTION SHALL BE IN ACCORDANCE WITH NORTH
CAROLINA EROSION CONTROL SPECIFICATIONS
STRUCTURAL BACKFILL MATERIAL REQUIREMENTS - SEE GEOTECH REPORT FOR FULL DETAILS
1. NO DELETERIOUS MATERIAL
2. NO ROCKS GREATER THAN 3 INCHES IN DIAMETER OR GREATER THAN 30%
RETAINED ON THE'/4-INCH SIEVE.
3. MAXIMUM DRY DENSITY (MDD) OF 95 POUNDS PER CUBIC FOOT (PCF) OR
GREATER, AS DETERMINED BY THE STANDARD PROCTOR COMPACTION TEST
(ASTM D698)
4. LIQUID LIMIT (LL) OF 50 OR LESS AND A PLASTICITY INDEX (PI) OF 25 OR LESS,
AS DETERMINED BY ATTERBERG LIMIT TESTING (ASTM D4318)
5. ORGANIC CONTENT NO GREATER THAN 3%
6. COMPACT STRUCTURAL FILL TO 98% OF THE SOILS MAXIMUM DRY DENSITY
6.1. 8-10" LIFTS USING LARGE RIDE -ON COMPACTORS
6.2. 4-6" LIFTS USING RAMMAX-TYPE COMPACTRS
6.3. NO MORE THAN 4" LIFT USING SLED OR JUMPING -JACK TAMPERS
JSWIFT
PARTNERS
10 . 9
L-�
A PER
04MAR2021
■
HIPP ENGINEERING
& CONSULTING, INC.
2301 REXWOODS DRIVE, SUITE 200
RALEIGH, NC 27607
TEL:[phone] FAX:[phone]
NC FIRM LICENSE NUMBER: C-2146
WWW.HII'I'-USA.COM
7m�� 0 ("-r
0 10 20 40
SCALE: 1" = 20' NORTH

15.00' WORK AREA
DURING
CONSTRUCTION
SEE EROSION CONTROL
PLANS
SEE CONSTRUCTION
SEQUENCE
EXTEND BACKFILL AND
STONE BASE
CONSTRUCTION GRADE
367.74
EL TANK TOP 396.24 (TO MATCH EXISTING TANKS)
-I111 111 111 111
SEE TANK
VENDOR FOR
TANK
CONSTRUCTION
DETAILS
TOP OF SLAB ELEVATION: 368.24
I I I I I I I I I I I I
0
0
00
N
u
AFTER TANK CONSTRUCTION, ADD 2ND
III I I I I I STAGE OF BACKFILL AROUND TANK TO
BRING TO FINISHED GRADE 1
18" STRUCTURAL BACKFILL PER GEOTECH REPORT
6" OF COMPACTED #57 STONE SEE BACKFILL NOTE THIS SHEET
SEE GEOTECH REPORT ADDENDUM SEE EROSION CONTROL PLANS
FOR CONSTRUCTION SEQUENCING
ILLUSTRATIVE TANK SECTION (NTS)
STRUCTURE FOUNDATIONS (DESIGNED BY
OTHERS) TO BE SUPPORTED WITH
STRUCTURAL BACKFILL. SEE STRUCTURAL
PLANS FOR DETAILS ON FOUNDATION
FINISHED GRADE EL
371.50
I E _110
—ICI ICI _,11
EXTEND STRUCTURAL BACKFILL UP TO
FINISHED GRADE AT NEW CATWALK
TOWER STRUCTURE
GRADING AND STORM DRAINAGE NOTES:
1. CONTRACTOR SHALL REPORT ANY GRADE DISCREPANCIES TO THE OWNER'S REPRESENTATIVE PRIOR TO
BEGINNING CONSTRUCTION OPERATIONS.
GRADING LEGEND:
SYMBOL DESCRIPTION
LIMITS OF DISTURBANCE
2. PRIOR TO ISSUANCE OF A BUILDING CERTIFICATE OF OCCUPANCY THE CONTRACTOR SHALL PROVIDE THE
200
PROPOSED MAJOR CONTOUR
OWNER WITH THE VIDEO INSPECTION OF THE STORM SEWER SYSTEM. (BOTH PUBLIC AND PRIVATE). THIS
PROPOSED MINOR CONTOUR
SUBMITTAL MAY NEED TO BE REVIEWED AND ACCEPTED BY THE LOCAL JURISDICTION PRIOR TO THE
EXISTING MAJOR CONTOUR
ISSUANCE OF THE BUILDING CO.
EXISTING MINOR CONTOUR
3. REFER TO THE EROSION CONTROL DETAILS SHEET FOR THE SEQUENCE OF CONSTRUCTION
PROPOSED STORM DRAINAGE
PROPOSED JUNCTION BOX
4. INTERIM GRADING SHALL BE PROVIDED THAT ENSURES THE PROTECTION OF STRUCTURES, UTILITIES,
SIDEWALKS, PAVEMENTS, AND OTHER FACILITIES FROM DAMAGE CAUSED BY SETTLEMENT, LATERAL
MOVEMENT, UNDERMINING, AND WASHOUT.
PROPOSED CATCH BASIN
5. INTERIM GRADING SHALL BE PROVIDED TO DIRECT WATER AWAY FROM STRUCTURES AND PREVENT
PROPOSED AREA DRAIN
PONDING.
'®-
RIPRAP DISSIPATOR
6. PROPOSED CONTOURS ARE APPROXIMATE. SPOT ELEVATIONS AND ROADWAY PROFILES SHALL BE USED IN
CASE OF DISCREPANCY.
FLOW DIRECTION
7. CONTRACTOR SHALL SLOPE GRADES TO ASSURE POSITIVE STORMWATER FLOW TO KEEP WATER FROM
44.50
PROPOSED ELEVATION
POOLING ALONG STRUCTURE WALLS
TC 44.50
BC 44.00
TOP/BOTTOM OF CURB
BACKFILL REQUIREMENTS - SEE GEOTECH REPORT FOR FULL DETAILS
TW46.00
BW 44.00
TOP/BOTTOM OF WALL
8. NO DELETERIOUS MATERIAL
9. NO ROCKS GREATER THAN 3 INCHES IN DIAMETER OR GREATER THAN 30% RETAINED ON THE 3/4-INCH SIEVE.
10. MAXIMUM DRY DENSITY (MDD) OF 95 POUNDS PER CUBIC FOOT (PCF) OR GREATER, AS DETERMINED BY
11. THE STANDARD PROCTOR COMPACTION TEST (ASTM D698)
12. LIQUID LIMIT (LL) OF 50 OR LESS AND A PLASTICITY INDEX (PI) OF 25 OR LESS, AS DETERMINED BY
13. ATTERBERG LIMIT TESTING (ASTM D4318)
14. ORGANIC CONTENT NO GREATER THAN 3%
15. COMPACT STRUCTURAL FILL TO 98% OF THE SOILS MAXIMUM DRY DENSITY
15.1. 8-10" LIFTS USING LARGE RIDE -ON COMPACTORS
15.2. 4-6" LIFTS USING RAMMAX-TYPE COMPACTRS
15.3. NO MORE THAN 4" LIFT USING SLED OR JUMPING -JACK TAMPERS
JSWIFT
PARTNERS
CA fjoZ
41
- L -
A
04MAR2021
■
HIPP ENGINEERING
& CONSULTING, INC.
2301 REXWOODS DRIVE, SUITE 200
RALEIGH, NC 27607
TEL:[phone] FAX:[phone]
NC FIRM LICENSE NUMBER: C-2146
WWW.HlPP-USA.COM
0 10 20 40
SCALE: 1" = 20' NORTH

MIN. 10 GA.
LINE WIRES
0
I
M N
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STEEL POST
- WOVEN WIRE FABRIC
SILT FENCE GEOTEXTILE FABRIC
FILL SLOPE
GRADE
6" COVER
OVER SKIRT*
N
EXTEND WIRE 6" MIN. INTO
TRENCH AND ANCHOR SKIRT
AS DIRECTED BY ENGINEER *
SIDE VIEW
MIN. 12-1/2 GA.
INTERMEDIATE
WIRES
-- GRADE
NOTES:
• USE SILT FENCE ONLY WHEN DRAINAGE AREA DOES NOT EXCEED 1/4 ACRE AND NEVER IN
AREAS OF CONCENTRATED FLOW
• END OF SILT FENCE NEEDS TO BE TURNED UPHILL.
• FOR REPAIR OF SILT FENCE FAILURES, USE No. 57 WASHED STONE.
• FOR ANCHOR WHEN SILT FENCE IS PROTECTING CATCH BASIN.
(:DS TEMPORARY SILT FENCE
NTS
5' METAL POSTS SUNK 2'
INTO GROUND (TYPICAL
EACH CORNER)
OWIRE POST INLET PROTECTION
NTS
JM 19—GAUGE
NARE CLOTH (1/4"
OPENINGS)
#57 WASHED STONE
(2:1 SLOPE w/
HEIGHT OF 16")
TnP \/I�\AI
SILT FENCE SILT FENCE
2' � senor rrnlr�r
C I I T rrnl/"r
�NTS
SILT FENCE STONE OUTLET
SWIFT
PARTNERS
04MAR2021
Farr
HIPP ENGINEERING
& CONSULTING, INC.
2301 REXWOODS DRIVE, SUITE 200
RALEIGH, NC 27607
TEL:[phone] FAX:[phone]
NC FIRM LICENSE NUMBER: C-2146
WWW.HIPP-USA.COM

r_GtiGoni
STRUCTURAL STAINLESS STEEL
STRUCTURAL MASONRY
1. THESE GENERAL NOTES ARE NOT INTENDED TO REPLACE SPECIFICATIONS. SEE SPECIFICATIONS FOR REQUIREMENTS IN ADDITION TO GENERAL NOTES.
2. THE STRUCTURAL DRAWINGS AND SPECIFICATIONS REPRESENT THE FINISHED STRUCTURE, AND, EXCEPT WHERE SPECIFICALLY SHOWN, DO NOT
INDICATE THE METHOD OR MEANS OF CONSTRUCTION. THE CONTRACTOR SHALL SUPERVISE AND DIRECT THE WORK AND SHALL BE SOLELY
RESPONSIBLE FOR ALL CONSTRUCTION MEANS, METHODS, PROCEDURES, TECHNIQUES, AND SEQUENCE. ALL APPLICABLE SAFETY REGULATIONS TO BE
FOLLOWED STRICTLY.
3. THE STRUCTURE HAS BEEN DESIGNED TO RESIST DESIGN LOADS ONLY AS A COMPLETED STRUCTURE. APPLICATIONS OF CONSTRUCTION LOADS TO THE
PARTIALLY COMPLETED STRUCTURE SHALL BE CONSIDERED BY THE CONTRACTOR AND SO INCLUDED IN THE DESIGN OF SHORING, BRACING,
FORMWORK, AND ANY OTHER SUPPORTING ELEMENTS PROVIDED FOR CONSTRUCTION OF THE STRUCTURE. DURING ERECTION AND UNTIL ALL
PERMANENT CONNECTIONS ARE MADE, THE CONTRACTOR MUST PROVIDE TEMPORARY BRACING FOR THE STRUCTURE IN ALL DIRECTIONS.
4. THE CONTRACTOR SHALL CHECK AND VERIFY ALL DIMENSIONS AND GRADE CONDITIONS (BOTH NEW AND EXISTING), REPORTING ANY DISCREPANCIES
TO THE ARCHITECT PRIOR TO ORDERING MATERIALS OR PROCEEDING WITH ANY PHASE OF THE WORK.
5. THE CONTRACTOR SHALL COMPARE STRUCTURAL SECTIONS WITH ARCHITECTURAL SECTIONS AND REPORT ANY DISCREPANCY TO THE ARCHITECT PRIOR
TO FABRICATION OR INSTALLATION OF STRUCTURAL MEMBERS.
6. DO NOT SCALE DIMENSIONS FROM DRAWINGS. THE CONTRACTOR SHALL REQUEST, FROM THE ARCHITECT, NECESSARY DIMENSIONS NOT SHOWN ON
THE DRAWINGS.
7. IF ANY BIDDER IS IN DOUBT AS TO THE INTENT OF THE PLANS OR SPECIFICATIONS, THEY SHALL REQUEST AN INTERPRETATION FROM THE ARCHITECT
IN WRITING AT LEAST TEN (10) DAYS PRIOR TO THE SCHEDULED BID DATE.
8. WHERE A CONFLICT BETWEEN DRAWINGS AND SPECIFICATIONS OCCURS THE MORE STRINGENT REQUIREMENT SHALL APPLY.
9. WHERE A DETAIL IS SHOWN FOR ONE CONDITION, IT SHALL APPLY FOR ALL LIKE OR SIMILAR CONDITIONS EVEN THOUGH NOT SPECIFICALLY
REFERENCED ON THE DRAWINGS.
10. SEVERAL ITEMS NOTED HEREIN AND IN THE SPECIFICATIONS REQUIRE THE CONTRACTOR TO ENGAGE A PROFESSIONAL ENGINEER LICENSED IN THE
STATE IN WHICH THE PROJECT IS LOCATED, TO PROVIDE DESIGN AND/OR DETAILING OF STRUCTURAL ELEMENTS. SEE INDIVIDUAL NOTES AND
SPECIFICATION SECTIONS FOR ADDITIONAL INFORMATION AND REQUIREMENTS. DELEGATED DESIGN ELEMENTS INCLUDE, BUT ARE NOT LIMITED TO:
A. PRE -MANUFACTURED / MODULAR PIPE SUPPORT SYSTEMS
DESIGN CRITERIA
1. APPLICABLE CODES:
A. 2018 NORTH CAROLINA STATE EXISTING BUILDING CODE (2015 INTERNATIONAL EXISTING BUILDING CODE WITH REVISIONS)
B. MINIMUM DESIGN LOADS FOR BUILDINGS AND OTHER STRUCTURES (ASCE/SEI 7-10)
C. BUILDING CODE REQUIREMENTS FOR STRUCTURAL CONCRETE (ACI 318-14)
D. BUILDING CODE REQUIRE MENTSISPECIFICATIONS FOR MASONRY STRUCTURES (ACI 5301530.1-13)
E. SPECIFICATION FOR STRUCTURAL STEEL BUILDINGS (AISC 360-10)
F. NATIONAL DESIGN SPECIFICATION FOR WOOD CONSTRUCTION (ANSI/AWC NDS-2015)
G. NORTH AMERICAN SPECIFICATION FOR THE DESIGN OF COLD -FORMED STEEL STRUCTURAL MEMBERS (AISI S100-12)
2. LIVE LOADS UNIFORM (PSF) CONCENTRATED (LB)
CATWALK 60 300
TANK ACCESS PLATFORM 60 1000
STAIRS 100 300
STORAGE 125 NA
3. RISK CATEGORY II
4. EXISTING BUILDING CODE APPROACH
A. COMPLIANCE METHOD - WORK AREA
B. NEW CONSTRUCTION - 2018 NORTH CAROLINA STATE BUILDING CODE (2015 INTERNATIONAL BUILDING CODE WITH REVISIONS)
5. SNOW LOAD:
GROUND SNOW LOAD Pg = 10 PSF
IMPORTANCE FACTOR Is = 1
SNOW EXPOSURE FACTOR Ce = 1.0
THERMAL FACTOR Ct = 1.0
FLAT SNOW ROOF LOAD Pf = 15 PSF
6. WIND LOAD:
BASIC DESIGN WIND VELOCITY V = 115 MPH
EXPOSURE CATEGORY C
INTERNAL PRESSURE COEFFICIENTS N/A (ALL WORK IS EXTERIOR)
BASE SHEAR Vx = Xk Vy = Xk
COMPONENTS AND CLADDING -
ALL BUILDING COMPONENTS AND CLADDING ENGINEERED BY THE COMPONENT MANUFACTURER ARE TO BE DESIGNED BY THE
MANUFACTURER'S ENGINEER FOR WIND LOADS DETERMINED PER THE GOVERNING BUILDING CODE FOR THE BASIC DESIGN WIND VELOCITY
AND EXPOSURE CATEGORY LISTED ABOVE.
7. SEISMIC LOAD (2008 USGS SEISMIC DESIGN MAPS):
DESIGN METHOD - EQUIVALENT LATERAL FORCE PROCEDURE
Ss 13.9 %g
S1 7.0 %g
Sds 14.8 %g
Sd1 11.3 %g
IMPORTANCE FACTOR Ie = 1.0
SITE CLASS D (ASSUMED)
SEISMIC DESIGN CATEGORY B
SEISMIC FORCE -RESISTING SYSTEM -
STEEL SYSTEMS NOT SPECIFICALLY DETAILED FOR SEISMIC RESISTANCE, EXCLUDING CANTILEVER COLUMN SYSTEMS
RESPONSE MODIFICATION COEFFICIENT Rx = 3 Ry = 3
DEFLECTION AMPLIFICATION FACTOR Cdx = 3 Cdy = 3
SEISMIC RESPONSE COEFFICIENT Csx = 0.049 Csy = 0.049
BASE SHEAR Vx = X Vy = X
NONSTRUCTURAL COMPONENT ANCHORAGE -
ALL ARCHITECTURAL, ELECTRICAL, MECHANICAL, AND PLUMBING COMPONENTS ARE TO BE ATTACHED AS REQUIRED BY ASCE/SEI 7 CHAPTER 13,
"SEISMIC DESIGN REQUIREMENTS FOR NONSTRUCTURAL COMPONENTS". EACH INDIVIDUAL CONTRACTOR RESPONSIBLE FOR THE COMPONENT
MUST PROVIDE PROJECT SPECIFIC DESIGN AND DOCUMENTATION PREPARED BY AN ENGINEER LICENSED IN THE STATE IN WHICH THE PROJECT
IS LOCATED. CHAPTER 13 DEFINES THE FORCE REQUIRED TO SUPPORT THE COMPONENT FOR THE ANCHORAGE AND BRACING. THE COST OF
PREPARING THIS INFORMATION AND DESIGN SHALL BE INCLUDED IN EACH CONTRACTOR'S BID THAT IS PROVIDING THE COMPONENT.
8. FUTURE LOADS:
UNLESS SPECIFICALLY NOTED, THERE ARE NO PROVISIONS MADE FOR FUTURE FLOORS, ROOFS, OR OTHER LOADS.
FOUNDATIONS
1. FOUNDATION DESIGN IS BASED ON THE GEOTECHNICAL INVESTIGATION REPORT BY:
STEWART INC., DATED DECEMBER 23, 2020, PROJECT #F20027.00
THE DESIGN ALLOWABLE SOIL BEARING PRESSURE IS 2,100 PSF, BASED ON THIS REPORT.
2. FOOTINGS SHALL BE CARRIED TO LOWER ELEVATIONS THAN THOSE SHOWN ON THE DRAWINGS IF REQUIRED BY THE GEOTECHNICAL ENGINEER OR
TESTING LAB TO REACH SOIL CAPABLE OF PROVIDING THE DESIGN ALLOWABLE SOIL BEARING PRESSURE.
3. REFER TO THE GEOTECHNICAL REPORT FOR SUBGRADE PREPARATION AND STRUCTURAL FILL REQUIREMENTS.
PREPARE SUBGRADE AND UNDERFLOOR FILL TO A POINT THAT EXTENDS T-0" (MINIMUM) BEYOND THE LIMITS OF THE FOUNDATIONS.
COMPACT ALL FILL UNDER BUILDING TO 98% MAXIMUM DENSITY AS DETERMINED BY ASTM D698.
PLACE IN LAYERS OF 8" (MAXIMUM) LOOSE THICKNESS.
FIELD COMPACTION SHALL BE VERIFIED WITH AT LEAST ONE TEST PER 2,000 SQUARE FEET PER LAYER, IN ACCORDANCE WITH ASTM D1556 (SAND -CONE
METHOD), ASTM D6938 (NUCLEAR METHODS, SHALLOW DEPTH), ASTM D2167 (RUBBER BALLOON METHOD), AND/OR ASTM D2937 (DRIVE -CYLINDER
METHOD).
SEE GEOTECHNICAL SPECIFICATIONS FOR OTHER TESTING REQUIREMENTS.
4. WALLS RETAINING SOIL SHALL BE TEMPORARILY BRACED DURING BACKFILLING AND UNTIL ALL SUPPORTING SOIL AND SLABS ARE IN PLACE AND ARE AT
DESIGN STRENGTH UNLESS NOTED OTHERWISE ON PLANS AND DETAILS.
5. UTILITY LINES SHALL NOT BE PLACED THROUGH OR BELOW FOUNDATIONS WITHOUT APPROVAL OF THE STRUCTURAL ENGINEER. CONTRACTOR SHALL
SUBMIT DETAILED DRAWINGS OF ALL SUCH CONDITIONS PRIOR TO CONSTRUCTION.
STRUCTURAL STEEL
1. DESIGN, FABRICATION, AND ERECTION SHALL BE PER THE SPECIFICATION FOR STRUCTURAL STEEL BUILDINGS (AISC 360).
2. STRUCTURAL STEEL:
WIDE FLANGE SHAPES (W SECTIONS) - ASTM A992, GRADE 50 (FY=50 KSI)
CHANNELS, ANGLES, RODS, AND BARS - A36 (FY=36 KSI)
PLATES - ASTM A36 (FY=36 KSI) OR ASTM A572, GRADE 50 (FY=50 KSI)
SQUARE AND RECTANGULAR TUBES - ASTM A500, GRADE B (FY=46 KSI)
PIPES OR ROUND TUBES - ASTM A53, GRADE B (FY=35 KSI) OR ASTM A500, GRADE B (FY=42 KSI)
3. ANCHOR BOLTS AND THREADED RODS SHALL CONFORM TO ASTM F1554, GRADE 36, UNO.
4. BEAM SIMPLE SHEAR AND BRACED FRAME CONNECTIONS NOT DETAILED ON STRUCTURAL DRAWINGS SHALL BE DESIGNED BY A PROFESSIONAL
ENGINEER RETAINED BY THE STEEL SUPPLIER AND REGISTERED IN THE STATE IN WHICH THE PROJECT IS LOCATED. CONNECTIONS SHALL BE MADE
WITH ASTM A325 3/4" 0 BOLTS (MINIMUM), TIGHTENED TO A SNUG -TIGHT CONDITION PER AISC REQUIREMENTS.
5. THE CONNECTIONS FOR NON -COMPOSITE BEAMS SHALL BE DESIGNED FOR REACTIONS SHOWN ON DRAWINGS OR FOR REACTIONS DETERMINED BY
USING THE MAXIMUM TOTAL UNIFORM LOAD TABULATED IN PART 3 OF THE AISC STEEL CONSTRUCTION MANUAL FOR THE SECTION, SPAN AND
STRENGTH OF STEEL SPECIFIED.
6. THE CONNECTION ENGINEER SHALL SUBMIT A SIGNED AND SEALED LETTER STATING THEY HAVE REVIEWED THE STEEL SHOP DRAWINGS AND THE
CONNECTIONS ARE CONSISTENT WITH THEIR CALCULATIONS AND INTENT.
7. WHERE STEEL MEMBERS ARE WELDED AND NO SIZE IS SPECIFIED, PROVIDE FULL LENGTH FILLET WELDS BOTH SIDES OF MEMBER. WELD SIZES SHALL
BE AS FOLLOWS UNLESS NOTED OTHERWISE:
MEMBER THICKNESS WELD SIZE
3/16" - 5/16" 3/16"
3/8" - 7/16" 1/4"
1/2" 5/16"
9/16" 3/8"
5/8" 7/16"
8. SPLICING OF STRUCTURAL STEEL MEMBERS IS PROHIBITED WITHOUT PRIOR APPROVAL OF THE ENGINEER AS TO LOCATION AND TYPE OF SPLICE TO BE
MADE. ANY MEMBER HAVING A SPLICE NOT SHOWN AND DETAILED ON SHOP DRAWINGS WILL BE REJECTED.
9. ALL WELDING SHALL CONFORM TO THE AMERICAN WELDING SOCIETY CODE. USE E70 SERIES ELECTRODES FOR ALL STRUCTURAL STEEL WELDS.
10. ALL STRUCTURAL STEEL AND CONNECTIONS TO BE HOT -DIP GALVANIZED AFTER FABRICATION.
11. ULTRASONIC INSPECTION BY THE TESTING LABORATORY SHALL BE PROVIDED FOR ALL WELDS CALLED FOR ON THE STRUCTURAL DRAWINGS OR SHOP
DRAWINGS AS FULL PENETRATION WELDS.
1. WHERE INDICATED ON PLAN, STRUCTURAL STAINLESS STEEL SHALL BE OF TYPE 304/304L (S30400/S30403) OR 316/316L (S31600/S31603) ANNEALED
STAINLESS STEEL (UNLESS OTHWERWISE NOTED ON THE ARCHITECTURAL DRAWINGS) WITH A MINIMUM SPECIFIED YIELD STRENGTH FY = 30 KSI AND
CONFORM TO THE FOLLOWING SPECIFICATIONS:
PLATES -ASTM A240
BARS AND HOT ROLLED SHAPES -ASTM A276
CHECKER PLATE -ASTM A793
2. STAINLESS STEEL THREADED RODS AND ANCHOR BOLTS SHALL CONFORM TO ASTM F593 (FY = 45 KSI)
3. DESIGN, FABRICATION AND ERECTION SHALL BE AS PER SPECIFICATION FOR STRUCTURAL STEEL BUILDINGS (AISC 360-10), AS AMENDED BY AISC
DESIGN GUIDE 27 FOR STRUCTURAL STAINLESS STEEL.
4. WHERE STEEL MEMBERS ARE WELDED AND NO SIZE IS SPECIFIED, PROVIDE FULL LENGTH FILLET WELDS BOTH SIDES OF MEMBER. WELD SIZES SHALL BE
AS FOLLOWS UNLESS NOTED OTHERWISE:
MEMBER THICKNESS WELD SIZE
3/16" 3/16"
1/4" 3/16"
5/16" 3/16"
3/8" 1/4"
7/16" 1/4"
1/2" 5/16"
9/16" 3/8"
5/8" 7/16"
5. WELDING OF STRUCTURAL STAINLESS STEEL (INCLUDING STAINLESS STEEL FLOOR PLATE) SHALL CONFORM TO AWS D1.6 (STRUCTURAL WELDING CODE -
STAINLESS STEEL) AND INDUSTRY STANDARDS. USE E308L SERIES ELECTRODES (MINIMUM TENSILE STRENGTH 75 KSI) FOR ALL STRUCTURAL STAINLESS
STEEL WELDS.
6. ULTRASONIC INSPECTION BY THE TESTING LABRATORY SHALL BE PROVIDED FOR ALL WELDS CALLED FOR ON THE STRUCTURAL DRAWINGS OR SHOP
DRAWINGS AS FULL PENETRATION WELDS.
CONCRETE I REINFORCING STEEL
1. ALL CONCRETE DESIGN AND CONSTRUCTION SHALL CONFORM TO THE REFERENCED EDITION OF THE BUILDING CODE REQUIREMENTS FOR STRUCTURAL
CONCRETE (ACI 318).
2. CONCRETE MIXTURES AS REQUIRED (BASED ON CLASS DESIGNATION):
CLASS A - FOOTINGS, GRADE/TIE BEAMS NWC 3,000 PSI
CLASS B - FOUNDATION WALLS NWC 4,500 PSI
CLASS F - EXTERIOR SLABS ON GRADE, PADS, TOPPINGS NWC 4,500 PSI
3. REINFORCING:
TYPICAL - ASTM A615, GRADE 60
REINFORCING TO BE WELDED - ASTM A706
DEFORMED BAR ANCHORS - ASTM A496
WELDED WIRE FABRIC - ASTM A1064 (FLAT SHEETS ONLY)
4. GROUT UNDER BASE PLATES TO BE HIGH STRENGTH (5,000 PSI), NON -SHRINK.
5. REFER TO THE DRAWINGS FOR REINFORCING LAP REQUIREMENTS. WHERE LAP SPLICES ARE NOT SHOWN, LAP PER ACI 318 OR CRSI STANDARDS.
6. LAP WELDED WIRE FABRIC SHEETS 8" MINIMUM.
7. CLEAR COVER FROM FACE OF CONCRETE:
CAST IN PLACE CONCRETE (MEASURE TO OUTERMOST REINFORCING) -
CONCRETE CAST AGAINST AND EXPOSED TO EARTH 3"
CONCRETE EXPOSED TO EARTH/WEATHER 2" FOR #6 BARS AND LARGER, 1 1/2" ELSE
CONCRETE NOT EXPOSED TO EARTH/WEATHER 3/4" FOR SLABS AND WALLS, 1 1/2" (TO TIES) FOR BEAMS AND COLUMNS
POST -TENSIONED CONCRETE (MEASURE TO OUTERMOST REINFORCING) -
CONCRETE CAST AGAINST AND EXPOSED TO EARTH 3"
CONCRETE EXPOSED TO EARTH/WEATHER 1" FOR SLABS AND WALLS, 1 1/2" ELSE
CONCRETE NOT EXPOSED TO EARTH/WEATHER 3/4" FOR SLABS AND WALLS
1" (TO TIES) AND 1 1/2" (TO MAIN BARS) FOR BEAMS AND COLUMNS
8. PROVIDE REINFORCING IN SLABS ON GRADE, 1-1/2" FROM TOP OF SLAB:
4" SLABS 6x6-W2.1xW2.1
5" SLABS 6x6-W2.9xW2.9
6" SLABS #3@12"OC EACH WAY
9. BAR SUPPORTS FOR CONCRETE EXPOSED TO VIEW SHALL HAVE PLASTIC COATED LEGS OR BE HOT -DIP GALVANIZED AFTER FABRICATION.
10. EMBED PLATES MUST BE SET IN THE FORM BEFORE POURING CONCRETE, NOT PLACED INTO TOP OF WET CONCRETE. THE CONTRACTOR SHALL CONTACT
THE ARCHITECT FOR CORRECTIVE DETAILS FOR ANY EMBED PLATES LEFT OUT OF CONCRETE POURS.
11. FOR SLABS ON GRADE, SLAB AND FOOTING REINFORCING SHALL BE HELD IN PLACE BY BAR SUPPORTS WITH SAND PLATES, OR PRECAST CONCRETE BAR
SUPPORTS AS DESCRIBED IN CHAPTER 3 OF THE CRSI MANUAL OF STANDARD PRACTICE. BAR SUPPORTS SHALL BE SPACED AT A MAXIMUM OF 4'-0110C
BOTH WAYS. ROCKS, CMU, OR CLAY BRICK WILL NOT BE USED AS SUPPORTS.
12. REBAR SHALL NOT BE HEATED WITH A TORCH IN THE FIELD.
13. THE CONTRACTOR SHALL NOTIFY THE ENGINEER FAR ENOUGH IN ADVANCE (48 HOURS) OF EACH CONCRETE POUR TO ALLOW AMPLE TIME TO CHECK THE
LAYOUT OF THE STEEL BEFORE THE BEGINNING OF THE ACTUAL POUR, BUT NOT PRIOR TO 90% OF THE STEEL HAVING BEEN PLACED.
EXISTING CONSTRUCTION
1. EXISTING FRAMING INFORMATION SHOWN ON THE STRUCTURAL DRAWINGS HAS BEEN PREPARED BASED ON EITHER SITE VISITS AND/OR EXISTING
DRAWINGS. IN LOCATIONS WHERE NEW FRAMING IS CONNECTING TO EXISTING FRAMING, THE CONTRACTOR SHALL VERIFY THE EXISTING CONDITION
PRIOR TO SHOP DRAWING CREATION, MATERIAL FABRICATION, OR WORK BEING PERFORMED. SELECTIVE DEMOLITION SHALL BE INCLUDED IF REQUIRED
TO VERIFY EXISTING CONDITIONS.
2. DETAILS NOTED ON THE STRUCTURAL DRAWINGS ARE BASED ON ASSUMED CONDITIONS. IT IS THE RESPONSIBILITY OF THE CONTRACTOR TO FIELD
MEASURE EXISTING MEMBERS AT POINT OF CONNECTION, ELEVATIONS, AND LOCATIONS TO ENSURE EXISTING CONSTRUCTION MATCHES DETAILS
PROVIDED IN THE STRUCTURAL DRAWINGS.
3. ANY DIMENSIONS SHOWN FROM NEW FRAMING TO EXISTING FRAMING ARE APPROXIMATED AND MUST BE FIELD VERIFIED. PRIOR TO ANY FABRICATION,
ALL DIMENSIONS THAT RELATE TO MEMBER DIMENSIONS SHALL BE FIELD VERIFIED.
4. STEEL CONNECTION DESIGN OF NEW FRAMING, UNLESS SPECIFICALLY SHOWN, IS ASSUMED TO BE SIMPLE SHEAR CONNECTIONS AND TO BE WELDED
TO THE EXISTING STEEL. DESIGN AND DETAILING OF THE STEEL CONNECTIONS ARE THE RESPONSIBILITY OF THE FABRICATOR, AND ARE COVERED
FURTHER IN THE STRUCTURAL STEEL SECTION OF THESE GENERAL NOTES. EXISTING MEMBERS HAVE BEEN REVIEWED BY THE ENGINEER OF RECORD
AND ARE CAPABLE (WITH ADDED REINFORCING WHERE DETAILED) OF SUPPORTING THE NEW FRAMING.
DEMOLITION
1. THE CONTRACTOR SHALL NOTIFY ALL LOCAL AGENCIES HAVING JURISDICTION, AND SHALL OBTAIN ALL NECESSARY PERMITS REQUIRED FOR THE
DEMOLITION AND REMOVAL OF THE DEBRIS RESULTING FROM THE DEMOLITION.
2. CONTRACTOR SHALL RETAIN, AT THEIR EXPENSE, A REGISTERED PROFESSIONAL ENGINEER LICENSED IN THE STATE IN WHICH THE PROJECT IS
LOCATED, TO DETERMINE ALL CONSTRUCTION PHASE SHORING REQUIREMENTS. CONTRACTOR SHALL SUBMIT TO THE OWNER AND THE ENGINEER OF
RECORD, SIGNED AND SEALED DRAWINGS, OUTLINING OPERATIONAL SEQUENCES, SHORING CONCEPTUAL PLANS, METHODS USED FOR THE
PROTECTION OF STRUCTURES TO REMAIN AND NEIGHBORING STRUCTURES.
3. CONTRACTOR SHALL BE SOLELY RESPONSIBLE FOR THE PROTECTION AND STABILITY OF EXISTING AND NEW STRUCTURES DURING CONSTRUCTION.
4. BEFORE UNDERTAKING ANY DEMOLITION WORK OR ORDERING MATERIAL, ASCERTAIN BY SURVEY THE EXISTING CONDITIONS OF THE PROPERTIES AND
BUILDINGS ADJOINING OR IN CLOSE PROXIMITY TO THE PREMISES. THE ENGINEER SHALL BE NOTIFIED OF ANY DISCREPANCY.
5. PROVIDE AND MAINTAIN BRACING AND SHORING AS NEEDED. KEEP SUPPORTING STRUCTURE IN PLACE DURING NEW CONSTRUCTION AND UNTIL NEW
STRUCTURE IS COMPLETED.
6. STORE AND PROTECT ALL MATERIAL TO BE REMOVED AND REUSED.
7. IF SAFETY OR INTEGRITY OF STRUCTURAL SYSTEM APPEARS TO BE COMPROMISED, CEASE OPERATIONS IMMEDIATELY AND NOTIFY THE OWNER AND THE
ENGINEER. PROPERLY BRACE AND SUPPORT STRUCTURE BEFORE RESUMING OPERATIONS.
8. ANY DAMAGE OCCURRING TO THE EXISTING STRUCTURE, ADJACENT STRUCTURES, STREETS, SIDEWALKS, UTILITY LINES OR ANY OTHER PUBLIC OR
PRIVATE PROPERTIES, SHALL BE REINSTALLED TO THE ORIGINAL CONDITION BY THE CONTRACTOR AT NO COST TO THE OWNER OR THE ENGINEER.
9. ALL OPENINGS IN EXISTING CONSTRUCTION SHALL BE SAW CUT OR DRILLED.
10. ALL EXISTING INFORMATION SHOWN IS REFERENCED FROM EXISTING DRAWINGS PROVIDED BY THE OWNER.
STEEL RAILINGS
1. REFER TO THE ARCHITECTURAL DRAWINGS IN ADDITION TO THESE STRUCTURAL DRAWINGS FOR ADDITIONAL REQUIREMENTS REGARDING GUARDRAIL
CONSTRUCTION, DETAILING, AND FINISHES. WHERE A CONFLICT BETWEEN HANDRAIL REQUIREMENTS OCCURS BETWEEN THE ARCHITECTURAL AND
STRUCTURAL DRAWINGS, THE REQUIREMENTS FROM THE ARCHITECTURAL DRAWINGS SHALL APPLY.
2. GUARDRAIL (ALSO SOMETIMES REFERRED TO AS "HANDRAIL") SHALL BE SOURCED FROM A COMPANY NORMALLY ENGAGED IN THE MANUFACTURE OF PIPE
RAILING. RAILING SHALL BE SHOP ASSEMBLED IN LENGTHS NOT TO EXCEED 24 FT FOR ERECTION AND SHALL CONFORM TO APPLICABLE OSHA GUIDELINES
AND THE 2018 NORTH CAROLINA BUILDING CODE.
3. UNLESS NOTED OTHERWISE ON THE ARCHITECTURAL DRAWINGS, THE GUARDRAIL SHALL BE MADE OF ATSM A53 GRADE B STRUCTURAL STEEL PIPE
SECTIONS WELDED OR FITTED TOGETHER WITH COMPONENT FITTINGS DESIGNED PER THE REQUIREMENTS OF THE ANSI/NAAMM STANDARD AMP 521-01
(R2012). SAMPLES OF ALL COMPONENTS, BASES, TOE PLATE AND PIPE SHALL BE SUBMITTED FOR APPROVAL AT THE REQUEST OF THE ENGINEER.
4. ALL RAILINGS (STEEL OR OTHERWISE) AND THEIR CONNECTIONS SHALL BE DESIGNED FOR A LATERAL LOAD OF 50 PLF APPLIED TO THE TOP OF THE RAIL
OR A 200 POUND LOAD AT ANY POINT IN ANY DIRECTION, WHICHEVER GOVERNS THE DESIGN. ALL RAILING SHOP DRAWINGS SHALL BEAR THE SEAL OF A
REGISTERED PROFESSIONAL ENGINEER LICENSED IN THE STATE IN WHICH THE PROJECT IS LOCATED. CALCULATIONS SHALL BE SUBMITTED FOR REVIEW
WITH THE RAILING SHOP DRAWINGS.
5. POSTS SHALL NOT INTERRUPT THE CONTINUATION OF THE TOP RAIL AT ANY POINT ALONG THE RAILING, INCLUDING CORNERS AND END TERMINATIONS
(OSHA 1910.23). THE TOP SURFACE OF THE TOP RAILING SHALL BE SMOOTH AND SHALL NOT BE INTERRUPTED BY PROJECTED FITTINGS.
6. THE MID -RAIL AT A CORNER RETURN SHALL BE ABLE TO WITHSTAND A 200 LB LOAD WITHOUT LOOSENING. THE VENDOR SHALL DETERMINE THE
APPROPRIATE FREE OVERHANG DISTANCE OF THE RAILING AT A CORNER BEYOND THE NEAREST POST FOR THE SYSTEM BEING INSTALLED.
7. HANDRAIL MAY BE TOP OR SIDE MOUNTED TO STRUCTURAL STEEL AND/OR CONCRETE STRUCTURE. UNLESS NOTED OTHERWISE, HANDRAIL SHALL NOT BE
ATTACHED TO GRATING, CHECKERED PLATE, FLOORING/ROOFING MATERIAL, CLADDING, VENEERS, OR OTHER NON-STRUCTURAL ELEMENTS. COORDINATE
ANY DEVIATIONS WITH THE ENGINEER OF RECORD AND/OR OWNER.
8. REFER TO THE ARCHITECTURAL DRAWINGS FOR COATING AND/OR GALVANIZING REQUIREMENTS, IF ANY.
STEEL STAIRS
1. STEEL STAIRS AND LANDINGS AND ALL CONNECTIONS SHALL BE DESIGNED BY THE SUPPLIER FOR A LIVE LOAD OF 100 PSF. TREADS SHALL BE DESIGNED
FOR A 300 POUND POINT LOAD DISTRIBUTED OVER 4 SQUARE INCHES. ALL STAIR SHOP DRAWINGS SHALL BEAR THE SEAL OF A REGISTERED
PROFESSIONAL ENGINEER LICENSED IN THE STATE IN WHICH THE PROJECT IS LOCATED. CALCULATIONS SHALL BE SUBMITTED FOR REVIEW WITH THE
STAIR SHOP DRAWINGS.
1. ALL MASONRY DESIGN AND CONSTRUCTION SHALL CONFORM TO THE REFERENCED EDITION OF THE BUILDING CODE REQUIREMENTS ISPECIFICATIONS
FOR MASONRY STRUCTURES (ACI 5301530.1).
2. LOAD BEARING MASONRY WALLS, PILASTERS, PIERS, RETAINING WALLS, FOUNDATION WALLS AND ANY OTHER MASONRY SO DESIGNATED ON
DRAWINGS IS CONSIDERED HERE TO BE STRUCTURAL MASONRY.
3. REQUIRED COMPRESSIVE STRENGTH OF MASONRY UNITS:
SOLID CLAY UNITS - 6,200 PSI
CONCRETE UNITS - 2,000 PSI ON NET AREA
4. CONCRETE MASONRY UNITS (CMU) SHALL BE LIGHT WEIGHT (105 PCF) CONFORMING TO ASTM C90. REFER TO ARCHITECTURAL DRAWINGS AND
SPECIFICATIONS FOR UNIT SIZE, FACE, COLOR, JOINTING, ETC.
5. MORTAR SHALL BE TYPE S, ASTM C270.
6. GROUT FOR REINFORCED MASONRY SHALL BE FINE GROUT, ASTM C476. MINIMUM 28-DAY COMPRESSIVE STRENGTH SHALL BE 2,000 PSI.
7. MINIMUM 28-DAY COMPRESSIVE STRENGTH (f',) OF THE MASONRY WALLS SHALL BE 2,000 PSI. MASONRY STRENGTH SHALL BE DETERMINED BY THE
UNIT STRENGTH METHOD OR THE PRISM TEST METHOD AS DESCRIBED BY ACI 530.
8. REINFORCING:
TYPICAL - ASTM A615, GRADE 60
ALL REINFORCING TO BE WELDED - ASTM A706
9. REFER TO THE DRAWINGS FOR REINFORCING LAP TYPICAL DETAIL AND SCHEDULE REQUIREMENTS. WHERE LAP SPLICES ARE NOT SHOWN, LAP 72 BAR
DIAMETERS.
10. MAXIMUM HEIGHT TO WHICH MASONRY SHALL BE LAID BEFORE GROUTING IS 5 FEET ABOVE CONSTRUCTION SURFACE OR PREVIOUSLY GROUTED
MASONRY. IF GROUT POUR HEIGHT EXCEEDS 5 FEET, THEN "HIGH LIFT" GROUTING PROCEDURE MUST BE FOLLOWED. PROVIDE CLEANOUT OPENINGS AT
THE BOTTOM OF EACH GROUT POUR HEIGHT. CLEANOUT OPENINGS SHALL BE PROVIDED AT EACH CELL TO BE FILLED WITH GROUT.
11. ALL GROUT PLACED OVER 12" IN HEIGHT SHALL BE MECHANICALLY CONSOLIDATED DURING GROUTING. GROUT SHALL BE RECONSOLIDATED BY
MECHANICAL VIBRATION AFTER INITIAL WATER LOSS AND SETTLEMENT HAS OCCURRED.
12. MAXIMUM GROUT LIFT (GROUT POURED IN ONE CONTINUOUS OPERATION) IS 5 FEET. THIS LIMIT ALSO APPLIES TO "HIGH LIFT" GROUTING.
13. REINFORCE MASONRY WHERE SHOWN ON STRUCTURAL DRAWINGS. TIE REINFORCING IN POSITION AND PLACE GROUT AROUND REINFORCING. DO NOT
PUSH REINFORCING DOWN INTO PREVIOUSLY PLACED GROUT FILL. SET BOLTS SIMILARLY.
14. TIE MASONRY WYTHES WITH HORIZONTAL REINFORCING AS SPECIFIED.
15. PROVIDE VERTICAL BARS, SIZE MATCHING WALL REINFORCING, AT ALL CORNERS, ENDS OF WALLS, EACH SIDE OF CONTROL JOINTS AND EACH SIDE OF
WALL OPENINGS. TIE EACH BAR TO THE FOUNDATION WITH A MATCHING DOWEL.
16. ALL CORNERS AND INTERSECTIONS OF STRUCTURAL MASONRY WALLS SHALL BE CONSTRUCTED BY INTERLOCKING COURSES.
17. ALL LINTELS TO BEAR 8" MINIMUM EACH SIDE OF OPENING, UNLESS NOTED OTHERWISE.
18. GROUT ALL MASONRY WALLS AND CAVITY BELOW GRADE SOLID. GROUT ALL WALLS ABOVE GRADE AT THE REINFORCED CELLS (MINIMUM) OR AS
INDICATED IN SPECIFIC SECTIONS.
19. ONE 3/4" 0 (MAXIMUM) VERTICAL CONDUIT ALLOWED IN ANY REINFORCED CELL PROVIDED 1" CLEAR IS MAINTAINED BETWEEN REINFORCING AND
CONDUIT. NO OTHER VERTICAL OR HORIZONTAL CONDUITS, PIPES, OR SLEEVES SHALL BE LOCATED IN REINFORCED CELLS UNLESS OTHERWISE
APPROVED BY THE STRUCTURAL ENGINEER. CONTRACTOR SHALL COORDINATE LAYOUT TO AVOID REINFORCED CELLS.
REPRODUCTION
1. THE USE OF REPRODUCTIONS OF THESE CONTRACT DRAWINGS BY ANY CONTRACTOR, SUBCONTRACTOR, ERECTOR, FABRICATOR, OR MATERIAL SUPPLIER
IN LIEU OF PREPARATION OF SHOP DRAWINGS SIGNIFIES HIS ACCEPTANCE OF ALL INFORMATION SHOWN HEREIN AS CORRECT, AND OBLIGATES
HIMSELF TO ANY JOB EXPENSE, REAL OR IMPLIED, ARISING DUE TO ANY ERRORS THAT MAY OCCUR HERE ON.
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SUITE 1100 FIRM LICENSE #C-1051
RALEIGH, NC 27603 PROJECT #S20231.00
HIPP ENGINEERING
& CONSULTING, INC.
2301 REXWOODS DRIVE, SUITE 200
RALEIGH, NC 27607
TEL:[phone] FAX:[phone]
NC FIRM LICENSE NUMBER: C-2146
WWW.Hll'l'-U SA.COM

STRUCTURAL
ABBREVIATIONS, LEGEND & SYMBOLS
SUBCONTRACTOR
GENERAL TERM
ABBREVIATIONS
GRAPHIC SYMBOLS
TRADE
ABBREVIATIONS
ACS
ACOUSTICAL CEILING
AB
ANCHOR BOLT
DBL
DOUBLE
I
MOMENT OF INERTIA
OC
ON CENTER
S
SECTION MODULUS
BL
BUILDER (AUSTIN)
ACI
AMERICAN CONCRETE
DEFL
DEFLECTION
ID
INSIDE DIAMETER
OD
OUTSIDE DIAMETER
SCH
SCHEDULE
DIRECTION OF VIEW
CONC
CONCRETE
INSTITUTE
DEG
DEGREE
IN
INCH
OPNG
OPENING
SDG
SIDING
2
SECTION NUMBER
CMT
CERAMIC TILE
ACU
AIR CONDITIONING UNIT
DEM
DEMOLISH
INCL
INCLUSIVE
OPP
OPPOSITE
SDL
SUPERIMPOSED DEAD LOAD
FEI
FEI
CPT
CARPETING
ACT
ACOUSTICAL TILE
DEPR
DEPRESSION
INFO
INFORMATION
OVHD
OVERHEAD
SECT
SECTION
41401
SHEET NUMBER WHERE SECTION CAN BE FOUND
41401
CSS
COLD STORAGE
ADDL
ADDITIONAL
DET
DETAIL
INT
INTERIOR
0 TO 0
OUT -TO -OUT
SEIS
SEISMIC
(OMITTED WHEN SHOWN ON SAME SHEET)
CWS
CASEWORK
ADJ
ADJUST
DIA
DIAMETER
INTER
INTERMEDIATE
SEW
SEWER
THRU SECTION
DES
DOCK EQUIPMENT
AFF
ABOVE FINISHED FLOOR
DIAG
DIAGONAL
INV
INVERT
SHT
SHEET
2
DPS
DAMPPROOFING
AGGR
AGGREGATE
DIM
DIMENSION
PART
PARTITION
SHTG
SHEATING OR SHEETING
DIRECTION OF VIEW
DWS
DRYWALL
AISC
AMERICAN INSTITUTE OF
DISC
DISCONTINUOUS
PC
PIECE
SIM
SIMILAR
SECTION NUMBER ELEVATION NUMBER
ELS
ELECTRICAL
STEEL CONSTRUCTION
DIST
DISTANCE
JT
JOINT
PCF
POUNDS PER CUBIC FOOT
SKL
SKYLIGHT
jel 3
ELV
ELEVATOR
AL
ALUMINUM
D JT
DUMMY JOINT
JST
JOIST
PED
PEDESTAL
SLV
SLEEVE
FEI
1
FEI 3
EWS
EARTHWORK
ALT
ALTERNATE
DK
DECK
PEN
PENETRATION
SO
SOUTH
41401
SHEET NUMBER WHERE SECTION / ELEVATION CAN BE
41201
FCS
FENCING
ARCH
ARCHITECTURAL
DL
DEAD LOAD
PERP
PERPENDICULAR
SPC
SPACES
FOUND (OMITTED WHEN SHOWN ON SAME SHEET)
K
KIP (EQUALS 1,000 LBS)
4
FCRP
FINISH CARPENTRY
ASPH
ASPHALT
DO
DOOR OPENING
PL
PROPERTY LINE
SPEC
SPECIFICATION
FOR MULTIPLE ELEVATIONS, SAME ROOM
FPS
FLAGPOLE
ASTM
AMERICAN SOCIETY OF
DWG
DRAWING
R
PLATE
SQ
SQUARE
SECTION
ELEVATION
GGS
GLASS AND GLAZING
TESTING MATERIALS
DWL
DOWEL
PLAS
PLASTER
SS
STAINLESS STEEL
DETAIL NUMBER FOR
HDS
HOLLOW METAL DOOR
AVG
AVERAGE
L
LENGTH
PLASTC
PLASTIC
ST
STREET
ENLARGED AREA
AREA SHOWN ON
IMS
INSULATED METAL SIDING
AWS
AMERICAN WELDING
E
EAST
LAM
LAMINATED
PLAT
PLATFORM
STG
STAGGER
SHEET WHERE
INST
INSTRUMENT
SOCIETY
EA
EACH
LAT
LATERAL
PNL
PANEL
STD
STANDARD
9 SHEET NUMBER WHERE SYMBOL APPEARS
KES
KITCHEN EQUIPMENT
EF
EACH FACE
LB
POUND
PRCST
PRECAST
STIFF
STIFFENER
41201 DETAIL CAN BE FOUND XXX-ZZ
(OMITTED WHEN SHOWN
D
LBS
LES
LOCKERS & BENCHES
LABORATORY EQUIPMENT
BET
BETWEEN
EXP BL
EXP JT
EXPANSION BOLT
EXPANSION JOINT
LDG
LANDING
PREFAB
PRESS
PREFABRICATED
PRESSURE
STIR
STL
STIRRUP
STEEL
DETAIL
ON SAME SHEET)
SHEET NUMBER FOR
LG
LONG
DETAIL NUMBER FOR
LNS
LANDSCAPING
BEV
BEVEL
EL
ELEVATION
LIN
LINEAL
PRMLD
PREMOLDED
STIR
STRUCTURAL
ENLARGED PLAN ADJACENT AREA
MAS
MASONRY
BLDG
BUILDING
ELECT
ELECTRICAL
LL
LIVE LOAD
PROJ
PROJECTION
STWY
STAIRWAY
LETTER OF ADJACENT AREA
MDS
METAL DECK
BLKG
BLOCKING
ELEV
ELEVATOR
LLBB
LONG LEG BACK-TO-BACK
PS
POINT OF SWITCH
SUPT
SUPERINTENDENT
12 SHEET NUMBER WHERE
PLAN CAN BE FOUND
MES
MECHANICAL
BM
BEAM OR BENCH MARK
ENGR
ENGINEER
LLH
LONG LEG HORIZONTAL
PSF
POUNDS PER SQUARE FOOT
SUR
SURFACE
41201
(OMITTED WHEN SHOWN
MIC
MISCELLANEOUS METAL
BOCA
BUILDING OFFICIALS &
EQ
EQUAL
LLV
LONG LEG VERTICAL
PSI
POUNDS PER SQUARE INCH
SUSP
SUSPENDED
ENLARGED PLAN
ON SAME SHEET) MATCH LINE
MIL
MILLWORK
CODE ADMINISTRATORS
EQUIP
EQUIPMENT
LP
LOW POINT
PT
POINT OR POINT OF
SYM
SYMETRICAL
ODS
ORN
OVERHEAD DOOR
ORNAMENTAL IRON
BOS OR B/S
BOT
BOTTOM OF STEEL
BOTTOM
EXC
EXIST
EXCAVATE
EXISTING
LS
LTL
LAG SCREW
LINTEL
PV
TANGENCY
PAVING
COLUMN MARK
q REVISION MARK
O
PBS
PLUMBING
B PL
BASE PLATE
EXP
EXPANSION OR EXPAND
LT WT
LIGHT WEIGHT
PVMT
PAVEMENT
T
TREAD
ELEVATION MARK
PCs
PRECAST CONCRETE
BRG
BEARING
EXPO
EXPOSE
LVR
LOUVER
TEMP
TEMPERATURE
PFB
PREFAB BUILDING
BRKT
BRACKET
EXT
EXTERIOR
LWC
LIGHT WEIGHT CONCRETE
TEN
TENSION
PGS
PIPING
BS
BOTH SIDES
EW
EACH WAY
LWIC
LIGHTWEIGHT INSULATING
QTY
QUANTITY
THK
THICKNESS
PIS
PIPING INSULATION
BT
BENT
CONCRETE
THIRD
THREADED
PLS
PLASTERING
BUR
BUILT-UP ROOFING
THRU
THROUGH
PTG
PAINTING
B TO B
BACK-TO-BACK
FD
FLOOR DRAIN
R
RADIUS
TOS OR T/S
TOP OF STEEL
PVS
PAVING
FDN
FOUNDATION
MACH
MACHINE
RD
ROAD
TYP
TYPICAL
RCRP
ROUGH CARPENTRY
FILL
FILLET
MAS
MASONRY
REBAR
REINFORCING BAR
T/
TOP OF
RFD
ROLLING FIRE DOOR
CALCS
CALCULATIONS
FIN
FINISH
MAT
MATERIAL
RECT
RECTANGULAR
RFL
RESILIENT FLOORING
CB
CATCH BASIN
FL
FLUSH
MAX
MAXIMUM
REF
REFERENCE
RTS
RAILROAD TRACK
CE
CIVIL ENGINEER
FLG
FLANGE
MECH
MECHANICAL
REINF
REINFORCE OR REINFORCING
UBC
UNIFORM BUILDING CODE
RSM
ROOFING & SHEET METAL
CEIL
CEILING
FL JT
FLUSH JOINT
MEMB
MEMBRANE OR MEMBER
REM
REMOVE
UL
UNDERWRITER'S LABORATORY
RSS
ROLLING STEEL SHUTTER
CEM
CEMENT
FLR
FLOOR
MEP
MECHANICAL / ELECTRICAL 1 PLUMBING
REQ
REQUIRED
ULT
ULTIMATE
SCS
SEALANTS & CAULKING
CHAM
CHAMBER
FOW
FACE OF WALL
MEZZ
MEZZANINE
REV
REVISION
UNO
UNLESS NOTED OTHERWISE
VICINITY MAP
SFS
SEAMLESS FLOORING
CHAN
CHANNEL
FRMG
FRAMING
MFR
MANUFACTURER
RE
ROOF
USD
ULTIMATE STRESS DESIGN
SGN
SIGNAGE
CI
CAST IRON
FS
FAR SIDE
MH
MANHOLE
RFG
ROOFING
UTIL
UTILITY
SKL
SKYLIGHT
CIP
CAST IRON PIPE
FT
FOOT
MIN
MINIMUM
RFTR
RAFTER
LOUISBURG
SPD
SPECIAL DOOR
CIR
CIRCLE
FTG
FOOTING
MISC
MISCELLANEOUS
RM
ROOM
VB
VAPOR BARRIER
STL
STRUCTURAL STEEL
CJ
CONTROL JOINT
FUT
FUTURE
MK
MARK
RND
ROUND
VIF
VERIFY IN FIELD
FRAN KLINTON
TAS
TOILET ROOM ACCESSORIES
CL OR
CENTER LINE
MO
MASONRY OPENING
RR
RAILROAD
VERT
VERTICAL
TPS
TOILET PARTITIONS
CLKG
CAULKING
MOM
MOMENT
RTU
ROOF TOP UNIT
TRZ
TERRAllO FLOORING
CLR
CLEAR OR CLEARANCE
GA
GAUGE
MTG
MOUNTING
RUB
RUBBER
VOL
VOLUME
1 /
WBS
WINDOW BLINDS
CMU
CONCRETE MASONRY UNIT
GAL
GALLON
MTL
METAL
WDS
WOOD DOOR
COL
COLUMN
GALV
GALVANIZE
WHSE
WAREHOUSE
i
WWS
WINDOW WALL
COMB
COMBINATION
GIRD
GIRDER
WP
WORK POINT
85 loos
COMP
COMPRESSION
GL LAM
GLUE LAMINATED
N
NORTH
WPT
WORKING POINT
56
CONC
CONCRETE
GR
GRADE OR GUARDRAIL
NBS
NATIONAL BUREAU OF
WSD
WORKING STRESS DESIGN
CONN
CONNECTION
GIRT
GROUT
STANDARDS
WT
WEIGHT OR WATERTIGHT
5s
JROJECT
CONST
CONSTRUCTION
GRTG
GRATING
NFPA
NATIONAL FIRE
WWF
WELDED WIRE FABRIC
CONT
CONTINUOUS
GYP
GYPSUM
PROTECTION ASSOCIATION
W/
WITH
SITE
CONTR
CONTRACTOR
NIC
NOT -IN -CONTRACT
WIO
WITHOUT
o
CR
CRANE
NO
NUMBER
1 401
HGT
HEIGHT
CS
CSK
CHANNELSTUD
COUNTERSUNK
HK
HOR
HOOK
HANGER
NOM
NS
NTS
NOMINAL
NEAR SIDE
NOT -TO -SCALE
70
40
SYMBOLS AND SHAPE
DESIGNATIONS
CST JT
CONSTRUCTION JOINT
HP
HORIZONTAL
CTR
CU
CENTER
CUBIC
H P
HR
HIGH POINT
HANDRAIL OR HOUR
64
\
W WIDE FLANGE SHAPE
S
AMERICAN STANDARD SHAPE
C/C
CENTER -TO -CENTER
HYD
HYDRANT
C
CHANNELSHAPE
MC
MISCELLANEOUS CHANNEL SHAPE
1
WT
STRUCTURAL TEE SHAPE
401 70
TS
STRUCTURAL TUBE SHAPE
L
ANGLE SHAPE
RALEIGH
L
ANGLES, BACK-TO-BACK
DIAMETER
D U R H A M
❑
SQUARE
CENTER LINE
R
PLATE
PIPE
PIPE
Q
BAR
FLAT, SQUARE OR
ROUND SOLID BAR
AA
SEA
045 6
Y
9•••••"�GIN EE •� �:
3/4/z1
STFWART
223 SOUTH WEST ST T 919.380.8750
SUITE 1100 FIRM LICENSE #C-1051
RALEIGH, NC 27603 PROJECT #S20231.00
HIPP ENGINEERING
& CONSULTING, INC.
2301 REXWOODS DRIVE, SUITE 200
RALEIGH, NC 27607
TEL:[phone] FAX:[phone]
NC FIRM LICENSE NUMBER: C-2146
WWW.Hll'l'-U SA.COM

8'-2"
COORD W/ MEP & DUKE ENERGY
PARTIAL FOUNDATION PLAN - SITE
1/4" = V-0"
1 H
NOTES: 0' 2' 4' 8' 16'
1. FOR GENERAL NOTES AND DESIGN CRITERIA, SEE DWG 40001.
2. FOR ABBREVIATIONS, LEGEND AND SYMBOLS, SEE DWG 40002.
3. (E) AND HALF -TONE LINEWORK INDICATE EXISTING COMPONENTS. INFORMATION REGARDING EXISTING STRUCTURES/COMPONENTS HAS BEEN TAKEN FROM FACILITY RECORD DRAWINGS PROVIDED BY OWNER. CONTRACTOR
SHALL VERIFY IN FIELD ALL EXISTING CONDITIONS AND REPORT ANY DISCREPANCIES TO THE OWNER AND ENGINEER OF RECORD.
4. SEE CIVIL DWGS FOR GRADING INFORMATION, INCLUDING FINISHED GRADE ELEVATIONS AT NEW AND EXISTING STRUCTURE(S).
5. SEE MEP DWGS FOR LOCATION OF NEW CONCRETE SPENT BIOMASS TANK "D". COORDINATE W/ CERTIFIED VENDOR DWGS FOR TANK FOR ALL INFORMATION REGARDING THE NEW TANK.
6. "P#" INDICATES NEW CONCRETE PEDESTAL, SEE X/40301.
7. CONTRACTOR SHALL COORDINATE W/ MEP ENGINEER, CIVIL DWGS AND TANK VENDOR TO LOCATE THE POSITIONS OF THE NEW TANK AND THE ACCESS TOWER COLUMN GRIDS PRIOR TO ORDERING MATERIAL. IF THE
DISTANCE OF THE COLUMN GRID NEAREST TO THE TANK EXCEEDS THE FACE OF WALL ("FOW") DIMENSION SHOWN, CONTACT THE OWNER AND ENGINEER OF RECORD FOR ADDITIONAL DIRECTION.
8. SEE MEP DRAWINGS, AND COORDINATE W/ OWNER & DUKE ENERGY FOR LOCATION & SIZE OF TRANSFORMER PAD. TRANSFORMER PAD SHALL BE OF 4,000 PSI NORMAL WEIGHT CONCRETE AND SHALL BE CONSTRUCTED ON A
PREPARED SUBGRADE OF 4"(MIN) #57 CRUSHED, COMPACTED STONE. CONTRACTOR SHALL DETAIL AND FURNISH THE PAD IN ACCORDANCE WITH THE DESIGN FOR A "LARGE PIT PAD FOR THREE-PHASE PAD -MOUNTED
TRANSFORMERS" SHOWN IN APPENDIX C, PAGE 2, OF THE DUKE ENERGY DOCUMENT "REQUIREMENTS FOR ELECTRIC SERVICE AND METER INSTALLATIONS - NORTH CAROLINA AND SOUTH CAROLINA" (PUBLISHED JUNE 2020
BY DUKE ENERGY).
EXIST CONC TANK "C",
VIF
CL EXIST &
NEW TANKS
NT BIOMASS
BY VENDOR;
)R LOCATION
WALL OF NEW TANK
COORD W/ MEP &
VENDOR DWGS
AA
SEA
045 6
Y
9•••••"�GINEER •� �:
yq � P•RAOV P
3/4/zs
STFWART
223 SOUTH WEST ST T 919.380.8750
SUITE 1100 FIRM LICENSE #C-1051
RALEIGH, NC 27603 PROJECT #S20231.00
HIPP ENGINEERING
& CONSULTING, INC.
2301 REXWOODS DRIVE, SUITE 200
RALEIGH, NC 27607
TEL:[phone] FAX:[phone]
NC FIRM LICENSE NUMBER: C-2146
WWW.Hll'l'-U SA.COM

CONCRETE RETAINING WALL SCHEDULE
8" DEEP BOND
BEAM W/(2)#5
CONT
8" CMU, GROUT SOLID
HORIZ JT REINF @
16"OC, TYP
FINISH GRADE,
SEE CIVIL
LM
° • d d,
a • e. d
d,°
B
A LAP BARS 72 BAR
DIAMETERS WITH
B WALL BARS
Lai
MAX
HEIGHT
H
DIMENSIONS
REINFORCEMENT
A
B
CIfl
4'-0"
1'-0"
4'-0"
V-0"
#5@16"OC
#5@16"OC
#5@16"OC
(5)#5
(2)#5
4'-0"
1'-0"
5'-0"
1'-0"
#6@16"OC
#6@16"OC
#6@16"OC
(5)#5
(2)#5
CMU RETAINING WALL SCHEDULE
CL
1'-0"
I
EQ EQ 1 1/2"
TYP
INS
BOLTS W/ 12" (MIN)
EMBEDMENT
TYPICAL BASE PLATE FOR NEW HSS COLUMN
3" = V-0"
HANGER ROD AND
ATTACHMENT HARDWARE
BY PIPING CONTRACTOR,
TYP
.. TOS ELEV
COORD W/ PIPING
X
a
O
2" HIGH STRENGTH,
NON -SHRINK GROUT
FINISH GRADE
SEE CIVIL
o z
CL
4'-0" MAX
W6x15
I
I
I
I I I
I
I
1
�x 1
I
I
XI
N I I
� I I
U I
2 I I
PIPING, SEE MEP
DWGS & NOTE 3,
TYP
1/4 NOTE 21 TYP
(4) 3/4"0 ANCHOR BOLTS
W/ 9 (MIN) EMBED
3/4"x11"x11"
III BASE PL
l l a•: a °-, •: II I
ad - 11/2
I_Cp
—I TYP I I I-1 11—I
I I=1 I I-1 I I1 I I -I I1 1 11 I I1 i I
-0" SQ " (4)#5 TOP & BOT
EA WAY
NOTES:
1. ALL STRUCTURAL STEEL AND CONNECTION TO BE GALVANIZED.
2. TOP CONNECTION MAY BE SHOP WELDED AS REQUIRED.
3. SUPPORT RATED FOR A MAXIMUM OF (2) 10"0 SCHD 80 PVC PIPES AND THEIR CONTENTS.
PS1 - PIPE SUPPORT DETAIL
HIGH STRENGTH, NON -
SHRINK GROUT
N
T PEDESTAL
SEE PLAN OR
SECTIONS
U
ANCHOR BOLTS, SEE
4/40301
TO
SEE PLAN
#3 TIES @12"OC
CC
(8) #6 VERT
CL
I
CONCRETE TO BE 4,500 PSI,
AIR -ENTRAINED
COL, SEE PLAN & 3/4" CHAMFER, TYP #6@12"OC EA WAY
I I SECTIONS
I I
FINISHED GRADE OR
I I
BASE PLATE, TOC PAVING, SEE CIVIL
CIIIIIIISEE 4/40301 SEE CIVIL
I I I z III np �_
I O ,;� III .d d - d 'A III —III —III
I z w a d a,
I w ~O M U
I„ `fl w = d - 2
FINISH GRADE, "' =• i 1 �•¢d,
SEE CIVIL
(2)#6 CONT, TYP
II 1-0
i III (3) ADDL TIES @2"OC OPTION 1
AROUND ANCHOR BOLTS TYP
d d
FOOTING, SEE
a d° •4 a°
2/40301 CONCRETE TO BE 4,500 PSI,
ELEVATION
CL
0"
0"
91, I 911
PLAN
PEDESTAL P1 - TYPICAL DETAILS
AIR -ENTRAINED
3/4" CHAMFER, TYP
#6@12"OC EA WAY, T&B
FINISHED GRADE OR
PAVING, SEE CIVIL
TOC
SEE CIVIL -
z
=
°
11 F7M_
` a
A
:� ; _a_4 - - .a
d4 a4" " , , d�a' ° `, 111TF
z
w
°b
O
4,
d,
. a°
am
_ ,
,--I
w
W
d
d
a 4-
OPTION 2
NOTES:
1. THE EXACT SIZE, SHAPE, AND LOCATION OF EQUIPMENT PADS SHALL BE DETERMINED BY THE
CONTRACTOR IN COORDINATION W/ THE MEP ENGINEER, AFTER APPROVAL OF EQUIPMENT
SHOP DRAWINGS. ANCHOR BOLTS WHERE REQUIRED SHALL BE SIZED AND LOCATED
ACCORDING TO MANUFACTURER'S REQUIREMENTS.
2. INCREASE DEPTH AS REQUIRED BY THE GEOTECHNICAL REPORT FOR AREA -SPECIFIC FREEZE -
THAW DEPTHS.
TYPICAL EXTERIOR EQUIPMENT PAD
NTS 40301 NTS 40301 NTS 40301 NTS
F
3/4" CHAMFER, TYP
FINISH GRADE,
SEE CIVIL
z=1IIIIrII '
I=111; •
TOW
X SEE CIVIL
A LU
FINISH GRADE, �v
SEE CIVIL > �o Cp
-D I
SEE TYPICAL RETAINING
WALL DRAINAGE
SYSTEM DETAIL _
CONT 2x4 KEYWAY
w
A
B
C
B
C
MAX
DIMENSIONS
REINFORCEMENT
HEIGHT
11H11
A
B
C
D
E
F
❑A
❑B
❑C
❑D
❑E
❑F
1'-0"
4'-0"
2'-4"
1'-8"
1'-0"
8"
#4@12"OC
#4@12"OC
#4@12"OC
#4@12"OC
(5)#4
(2)#4
1'-0"
T-0"
T-4"
2'-0"
V-0"
8"
#5@12"OC
#5@12"OC
#5@12"OC
#5@12"OC
(6)#4
(2)#4
TOS ELEV
COORD W/ PIPING
X
a
0
In
SEE CIVIL
PIPING, SEE MEP
DWGS & NOTE 1
(4) 3/4"0 HILTI KH-EZ
GALV CONC SCREW
ANCHORS W/ 3-1/2" (MIN)
NOMINAL EMBEDMENT
INTO CONC
3/4"x11"x11" BASE PL
EXIST OR NEW CONC
PAD, MIN 6" THICK; SEE
PLAN AND/OR VIF AS
NEEDED
NOTES:
1. SUPPORT RATED FOR A MAXIMUM OF (2) 10"0 SCHD 80 PVC PIPES AND THEIR CONTENTS.
2. FOR INFORMATION NOT SHOWN AND ADDITIONAL NOTES, SEE 5/40301.
PS1A - PIPE SUPPORT DETAIL
NTS
3/4" = V-0"
�01
TOW
PRECAST BOLLARD
SEE CIVIL
CAP, BY SUPPLIER
DRAINAGE COMPOSITE BOARD
= SHALL BE MEL-DRAIN 9055 (W.R.
ap
6"0 STD STEEL PIPE,
a '<' I- o MEADOWS) OR MIRAFI G100NC
FILL WITH CONCRETE,
I (TENCATE GEOSYNTHETICS),
PAINT OSHA YELLOW
INSTALL PER MANUFACTURER
°.-'" REQUIREMENTS
SLOPE TOP SURFACE AWAY FROM POST,
a
• ° ' ' �� APPROVED BACKFILL
FLUSH EDGE W/SURROUNDING GRADE
PROVIDE 1 1/2"0 WEEPS @
8'-0"OC IF FOUNDATION DRAIN IS FILTER FABRIC
NOT PROVIDED
18" OF FREE -DRAINING
GRANULAR BACKFILL;
EXTEND UP WALL IF
C14FINISH GRADE _ _ _
FINISH GRADE, SEE CIVIL DRAINAGE BOARD IS NOT
SEE CIVIL
PROVIDED
I —III —III— ", ° : d °; -III—III—I I
_ _
-IIIIIIIII—III d '° 6"0 PERFORATED FLEXIBLE
,
I —III —III —I . I —III —III —I
LIIII °a ' PVC PIPE, SLOPE TO NEAREST
III —III —III— -A, —III=1 I I=1 I
CONT KEYWAY IIIX STORM SEWER OR OUTLET AS
a
—X APPROVED BY CIVIL
FILL W/ 3,000 0
M
� 8
PSI CONCRETE Y a
a,, a,a . • : :. `° n' ." :. °� ° .-
40
a,
-
IIIIII-III-'
NOTES:
9
1. THIS DETAIL IS INTENDED TO SPECIFY ONLY THE REQUIRED DRAINAGE SYSTEM
NOTE:
FOR ALL SITE RETAINING WALLS. SEE OTHER SECTIONS AND DETAILS FOR WALL
1. SEE CIVIL DWGS FOR NUMBER AND 1'-6" 0
AND FOOTING SIZES, REINFORCING, ETC.
LOCATION OF BOLLARDS
io TYPICAL CONCRETE BOLLARD
TYP SITE RETAINING WALL DRAINAGE SYSTEM
40301 3/4" = V-0"
1/2" = V-0"
372'-6"
T/ FTG (NEW
369'-6"
SECTION
3/4" = V-0"
BASE PL, SEE
4/40301, TYP
o z 1I I
�I 1I—
N IIIII
O _
TANK BOT IFFE
368'-3"
SEE PLAN
I 1
FINISH GRADE,
SEE CIVIL STRUCTURAL FILL PER
GEOTECH, COORD W/ CIVIL
FOR EXTENTS I
IIIIIIIIIIIII I � IIIII I IIIIIIIII—III— I _
-II I I IIIII IIIIIIIIIIIII 111 I II 11_1 111 111 111 111 111 I 1 I 11 I-
111=IIIIIIIIIIIIIIIIII1I11I1I 1 II 1 I1 1 11 1 1I 1 II 1 I 1 1 11 �
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—I I I I III—III—III=III _(12)#7 TOP & I —III —III III —III —III III —III— I 11-1
-IIII I I —III —III —III II BOT, EA WAY—III—III—IIIIIIIII—III—III—III—I I—
—III III —III —III —III-I � 11 � 11II—III—IIIIII—III—IIIIII—III— III —I �
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1=1 11=1 11=1 11=1 11=1 11=1 11=1 11=1 11=1 11=1 11=1 I II I I— I I—IIII 11=1 11=1 11=1 11=1 11=1 11=1 11=1 11=1 11=1 11=1 I
PEDESTAL, SEE
PLAN AND 3/40301,
TYP
L
% -\N CARP �.
1�'�l'9
SEA
045pf600
=
Y
GIN EEFi
PRABNP �.
3141,21
■ A 03-04-21 JEW AP ISSUED FOR CONSTRUCTION
Rev.: Rev. date: Dwg Chk Revisions:
Novozymes North America Inc.
77 Perry Chapel Church Road
P.O. Box 576
novozymes® Franklinton, N.C. 27525-0576 USA
HIPP ENGINEERING Rethink Tomorrow Tel [phone]
& CONSULTING, INC. Est. date: 12-23-2020 NZNA - FLF
STEWART 2301 REXWOODS DRIVE, SUITE 200 Designer: AKSHAY P., PE STRUCTURAL
RALEKGH, NC 27607 Scale: AS NOTED FOUNDATION SECTIONS AND DETAILS
223 SOUTH WEST ST T 919.380.8750 TEL: [phone] FAX: [phone]
SUITE 1100 FIRM LICENSE #C-1051 NC FIRM LICENSE NUMBER: C-2146 group no.: FLF40301 _U502986_N EW
RALEIGH, NC 27603 PROJECT #S20231.00 WWW.HIPP-USA.COM Page no.:

1_443/8 (-10"),
TYP OF 3
VERTICAL PIPING,
SEE MEP DWGS
:LS TO BOT OF
AL SUPPORT TO
MAX OC, COORD
DWGS
)OR,
2 NEW TANK D ACCESS PLATFORM - FRAMING PLAN
40601 1/2" = V-0"
NOTES: 0' 1' 2' 4'
1. FOR GENERAL NOTES AND DESIGN CRITERIA, SEE DWG 40001.
2. FOR ABBREVIATIONS, LEGEND AND SYMBOLS, SEE DWG 40002.
3. SEE 40701 FOR TYPICAL FLOOR FRAMIN SECTIONS AND DETAILS.
4. (E) AND HALF -TONE LINEWORK INDICATE EXISTING COMPONENTS. INFORMATION REGARDING EXISTING STRUCTURES/COMPONENTS HAS BEEN TAKEN FROM FACILITY RECORD
DRAWINGS PROVIDED BY THE OWNER. CONTRACTOR SHALL VERIFY IN FIELD ALL EXISTING CONDITIONS AND REPORT ANY DISCREPANCIES TO THE OWNER AND ENGINEER OF RECORD.
5. FINISHED FLOOR ELEVATION OF PLATFORM IS 398'-8 1/4" ABOVE REFERENCE ELEVATION OF U-0". TOP OF STEEL ELEVATION IS 1-1/4" BELOW FINISHED FLOOR UNO. ALL REFERENCE
ELEVATIONS ARE TAKEN FROM EXISTING DRAWINGS, VERIFY IN FIELD. [No] INDICATES TOP OF STEEL ELEVATION RELATIVE TO PLATFORM FFE.
6. _G1 INDICATES SPAN DIRECTION OF NEW WELDED, GALVANIZED STEEL BAR GRATING, W/ 3/16"x1-1/4" BEARING BARS @ 1-3/16" OC OR BETTER.
7. SEE CIVIL DWGS FOR GRADING INFORMATION, INCLUDING FINISHED GRADE ELEVATIONS AT NEW AND EXISTING STRUCTURE(S).
8. LOCATE ALL PLATFORM COLUMNS PER SITE PLAN SHOWN IN 1/40101. COORDINATE W/ CIVI, MEP & TANK VENDOR DRAWINGS.
d
(2) EQ SPACES @ 4'-6" 1 KAINJl I WIN I U rUK INtuu r1r11NU, Ott TYP
VERTICAL, COORD 3/40703, TYP
W/ MEP DWGS
EXIST "BENT 2"
STRUCTURE, VIF
OVER ROAD, VIF
CL EXIST 6"0
PIPE COL
_ 1
AIR UP TO
ATFORM,
SUPPLIER
M
U_ o
i TANK D ACCESS CATWALK - FRAMING PLAN
40601 1/2" = V-0"
NOTES:
1. FOR GENERAL NOTES AND DESIGN CRITERIA, SEE DWG 40001.
2. FOR ABBREVIATIONS, LEGEND AND SYMBOLS, SEE DWG 40002.
3. SEE 40701 FOR TYPICAL FLOOR FRAMING SECTIONS AND DETAILS.
4. (E) AND HALF -TONE LINEWORK INDICATE EXISTING COMPONENTS. INFORMATION REGARDING EXISTING STRUCTURES/COMPONENTS HAS BEEN TAKEN FROM FACILITY RECORD DRAWINGS
PROVIDED BY THE OWNER. CONTRACTOR SHALL VERIFY IN FIELD ALL EXISTING CONDITIONS AND REPORT ANY DISCREPANCIES TO THE OWNER AND ENGINEER OF RECORD.
5. FINISHED FLOOR ELEVATION OF NEW CATWALK TO MATCH EXISTING AT 392'-2 1/4" ABOVE REFERENCE ELEVATION OF 0'-0" AS PER EXISTING DRAWINGS, VERIFY IN FIELD. (No) INDICATES
TOP OF STEEL ELEVATION RELATIVE TO 0'-0".
6. "HI" & "LO" INDICATE TOP OF STEEL ELEVATIONS AT THE UPPER & LOWER LEVELS OF FRAMING FOR THE CATWALK. SEE PLAN FOR ELEVATIONS.
7. G1 INDICATES SPAN DIRECTION OF NEW WELDED, GALVANIZED STEEL BAR GRATING, W/ 3/16"x1-1/4" BEARING BARS @ 1-3/16" OC OR BETTER.
8. SEEVIL DWGS FOR GRADING INFORMATION, INCLUDING FINISHED GRADE ELEVATIONS AT NEW AND EXISTING STRUCTURE(S).
9. LOCATE ALL PLATFORM COLUMNS PER SITE PLAN SHOWN IN 1/40101. COORDINATE W/ CIVI, MEP & TANK VENDOR DRAWINGS.
3 PLAN @ TOP OF EXIST CATWALK
40601 1/2" = V-0"
NOTES:
1. FOR GENERAL NOTES AND DESIGN CRITERIA, SEE DWG 40001.
2. FOR ABBREVIATIONS, LEGEND AND SYMBOLS, SEE DWG 40002.
3. FINISHED FLOOR IS EXISTING, WITH TOP ELEVATION AT 392'-2 1/4" ABOVE REFERENCE ELEVATION OF 0'-0" AS PER EXISTING DRAWINGS, VERIFY IN FIELD. (No) INDICATES TOP OF STEEL ELEVATION RELATIVE TO FFE.
4. (E) AND HALF -TONE LINEWORK INDICATE EXISTING COMPONENTS. INFORMATION REGARDING EXISTING STRUCTURES/COMPONENTS HAS BEEN TAKEN FROM FACILITY RECORD DRAWINGS PROVIDED BY THE OWNER.
CONTRACTOR SHALL VERIFY IN FIELD ALL EXISTING CONDITIONS AND REPORT ANY DISCREPANCIES TO THE OWNER AND ENGINEER OF RECORD.
5. G(E) INDICATES SPAN DIRECTION OF EXISTING STEEL BAR GRATING, VERIFY SIZE AND SPAN IN FIELD IF REQUIRED.
6. SEA IL DWGS FOR GRADING INFORMATION, INCLUDING FINISHED GRADE ELEVATIONS AT NEW AND EXISTING STRUCTURE(S).
0' 1' 2' 4'
Off'
�. A CARP
� e.
SEA
045 600
=
Y
G I N
�'iSygY PRAB�`P� �•
3/4/zs
0
IF I
HIPP ENGINEERING
& CONSULTING, INC.
0' 1' 2' 4' 8'
A 03-04-21 JEW AP ISSUED FOR CONSTRUCTION
Rev.: Rev. date: Dwg Chk Revisions:
novozymes®
Rethink Tomorrow
Novozymes North America Inc.
77 Perry Chapel Church Road
P.O. Box 576
Franklinton, N.C. 27525-0576 USA
Tel [phone]
STEWART
223 SOUTH WEST ST T 919.380.8750
SUITE 1100 FIRM LICENSE #C-1051
RALEIGH, NC 27603 PROJECT #S20231.00
2301 REXWOODS DRIVE, SUITE 200
RALEICH, NC 27607
TEL:[phone] FAX:[phone]
NC FIRM LICENSE NUMBER: C-2146
WWW.HIPP-USA.COM
Est. date:
12-23-2020
Designer:
AKSHAY P., PE
Scale:
AS NOTED
Group no.:
Page no.:
NZNA - FLF
STRUCTURAL
CATWALKS AND TANK ACCESS PLATFORM - FRAMING PLANS
F L F40601 _U 502986_N EW

CL
TYP
1/4" CAP SEE PLAN BEAM, SEE PLAN
PLATE
CL VERT BRACE, SEE PLAN
& SECTIONS FOR SIZE /
1/4" CONT TOE
PL, TYP
T1/8
1/4" TOE PL OR MITER TOE PL AT NEW PENETRATION THRU GRTG,
PIECE OF PIPE, CORNERS, TYP
C'L
AND ORIENTATION
SEE MEP DWGS, TYP
TOS
/
2" CONT @
2" CONT @
SEE NOTE 2
SEE PLAN
i ® a
/
/
ENDS
1-9 ENDS 1/8 1-9
GUARDRAIL WHERE REQD, BY
_ _ _ _
/'
_
SUPPLIER, SEE PLAN FOR
® �
3/8" GUSSET PL /' 4 3/4"0 A325
EXTENTS AND 2/40701 FOR TYP
/ BOLT, TYP
i i CONSTRUCTION
/
FE
FFE
1
��
'"-SEE PLAN
SEE PLAN
1/4"x4" CONT TOE PL BY
� � �
PROVIDE CONNECTION @
WP
z
GUARDRAIL SUPPLIER
i 12 OC OR BETTER
/
COLUMN,
SEE PLAN1y�'L
II 3/8" GUSSET PLATE,
1
"\
GRATING, BY
/ J TYP
\
i /
SUPPLIER, SEE PLAN
1
WP
FFE
1/4 3
r
SEE PLAN
i
1/4 3 TYP
/
FLOOR, SEE
BRACE MEMBER SEE
'
z z i
PLAN, TYP
GRATING ATTACHMENT,
PLANS &SECTIONS
a � i i
1/4
1/4" TOE PL,7 EXIT RT ,VIF, TYP
CONT 1/4" TOE PL MAY BE
,
BOLT &CLIP BY GRATING
WP i
�
w ,d i i
cwi� � i � 1/4
SEE NOTE 2
PROVIDED ALONG WITH
SUPPLIER
1/4 4" MIN
�
B/BASE PL l
GUARDRAIL (WHERE
COL SEE TYP
i 1/4 4" MIN
SEE PLAN
PRESENT) AT OWNER'S /
PLAN &
BEAM, SEE
CONTRACTOR'S OPTION
BEAM, SEE PLAN
SECTIONS
PLAN, TYP
NOTES:
1. OPENINGS UP TO 10"0 OR 10" SQ MAY BE CUT IN GRATING WITHOUT ADDITIONAL EDGE SUPPORT.
2. OPENINGS UP TO 10"0 OR 10" SQ MAY BE BANDED IN LIEU OF PROVIDING TOE PLATE.
iz
TYPICAL KNEE BRACE
s
VERTICAL BRACE TO HSS COLUMN TYPICAL CONNECTION
5
TYPICAL TOE PLATE ATTACHMENT TO STRUCTURAL STEEL
4 TYPICAL PENETRATION THROUGH GRATING
i
TYPICAL GRATING
ATTACHMENT TO STRUCTURAL STEEL
40701
3/4" = V-0"
40701
1 1/2" = V-0"
40701
NTS
40701 NTS
40701
1 1/2" = V-0"
3'-0" V-6"
BY SUPPLIER
LOCATE AS NEEDED MAX
5'-0" MAX
FOR ACCESS
TYP
1/4 7\
CL-
CL 5/8"OA325 BOLT,
- - - - - — HANDRAIL POST
GUARDRAIL POST
WP BEAM, SEE PLAN
TYP BRACE MEMBER (-3),
MOUNTING BRACKET,
BRACKET AND CONN
SEE PLAN, TYP
BY SUPPLIER
BY SUPPLIER
TOS
�i
SEE PLAN o
\
�\ iii L �t
CYdb
LU
;
will
?
BRACE MEMBER, SEE
1
1/4 4 \\�` - 1
_X
/ n x \ PLANS & SECTIONS,
TYP \ i Q �' / Jri�,
14 4
/
CONTINUOUS EDGE
PLATE OR TOE PLATE,
-
TYP
„
\ ��� ��, i „� , '�A
�`\titiQ
FINISHED FLOOR SEE OTHER SECTIONS
BEAM, SEE PLAN SIDE MOUNT
BEAM, SEE PLAN
/
i �, n ���
CONNECTION,
BY
\v�X
/� \\
SUPPLIER
L--------
i
\\\—
SIDE MOUNT CONNECTION
TOP MOUNT CONNECTION
z
TYP 1/4 3" MIN 3/8" GUSSET PL
TOP OF STRUCTURAL
STEEL
MEMBER, SEE PLAN
TYPICAL REMOVABLE GUARDRAIL CONNECTION DETAIL
BEAM, SEE PLAN, TYP WP 3/8" GUSSET PL,
CUT TO CLEAR BEAM CONN
SEE TYPICAL GUARDRAIL
(FOR ATTACHMENT
TO STRUCTURAL STEEL)
TYP
CONNECTION DETAIL NOTES:
1. PAINT ALL GUARDRAIL MEMBERS, COMPONENTS AND CONNECTIONS OSHA SAFETY YELLOW UNO.
NOTES:
2. SEE DWG S-001
FOR ADDITIONAL REQUIREMENTS FOR GUARDRAIL CONSTRUCTION.
1. A BOLTED CONNECTION W/ (2) 3/4"0 A325 BOLTS MAY BE PROVIDED IN LIEU OF WELDED
CONNECTION BETWEEN BRACE MEMBER AND GUSSET PL.
i3
TYPICAL CHEVRON BRACE
9
TYPICAL HORIZONTAL BRACE CONNECTION
z TYPICAL GUARDRAIL CONSTRUCTION
40701
3/4" = 1'-0"
40701
1 1/2" = 1'-0"
40701 3/4" = 1'-0"
t (2) 3/4"o BOLTS IN HOR
LONG SLOTTED HOLES
1/4" CAP PL CL 1/4 BY STEEL
1/4 SUPPLIER
CL A325 BOLTS IN HORIZ LONG
SLOTTED HOLES, SEE NOTE 2
(2) 1-500/8 CLIP ANGLES
FIELD DRILL HOLES IN
(1 NS/ 1 FS), SEE NOTE 1
TOS
WEB OF EXISTING BEAM (2) 1-500/8 CLIP ANGLES
511
SEE PLAN
TO MATCH (1 NS/ 1 FS), SEE NOTE 1
CL
E E
NEW BEAM,
i i Q
SEE NOTE 2
SEE PLAN
1/2"x6-1/2"x1'-0" PL
1 3/4"0 A325 BOLT, FIELD
HSS BEAM OR
DRILL HOLES IN WEB OF �
COL, SEE PLAN &
SECTIONS
TOS
EXIST BEAM TO MATCH CLIP
SEE PLAN
ANGLE -4—
BEAM, SEE PLAN
3/8" SHEAR TAB
1 1/2" �1 1/2"
CL 3/4"0 A325 BOLTS,
SEE NOTES
� �
(4)3/4"0 i
A325 BOLTS i BEAM, SEE PLAN
NEW L500/8" CLIP
ANGLE, TYP NS/FS
i i
i i
EXIST BEAM, PLAN TYP
SEE PLAN,VIF,
i i
i i i
TYP
1/4 i
EXIST BEAM OR
i COL, SEE PLAN
COLUMN, SEE COPE BOT FLANGE
i
AND SECTIONS
11i L11
PLAN, VIF IF REQD
OPTION A
OPTION B
NOTE:
1. EITHER OR BOTH CLIP ANGLES MAY BE REPLACED BY AN APPROPRIATELY SIZED
PLATE SHEAR TAB CONNECTION WELDED TO BEAM, DESIGNED BY STEEL SUPPLIER.
NOTES:
NOTE:
PROVIDE HORIZ SLOTTED HOLES IN ALL CONNECTIONS TO EXISTING BEAMS.
1. PROVIDE A 2 BOLT CONNECTION AT ALL W8X10 BEAM ENDS.
1. AT CONTRACTOR'S OPTION, SHEAR TABS MAY BE USED IN LIEU OF L50 CLIP ANGLES.
2. PROVIDE A 3 BOLT CONNECTION AT THE ENDS OF W8x15 AND LARGER BEAMS.
2. SHEAR CONNECTION DESIGN BY STEEL SUPPLIER, SEE NOTES ON S-001.
i4
TYPICAL BEAM CANTILEVERED OVER COLUMN
io
TYPICAL SHEAR CONNECTION - NEW BEAM TO EXISTING
6
TYPICAL WIDE FLANGE BEAM TO HSS SHEAR CONNECTION
3 TYPICAL SHEAR CONNECTION - NEW BEAM TO EXISTING
40701
3/4" = 1'-0"
40701
1 1/2" = 1'-0"
�111
1/2" = 1'-0"
1 1/2" = 1'-0"
�11
TJ/1/4
CL4 TYP
\ /
F
1/ 4
TYP
X / VERT BRACE, SEE PLAN &
40701 BEAM, SEE PLAN
/ SECTIONS FOR STEEL
ORIENTATION, TYP
/ WP, TYP
\ / `
3/8" FILLER PL W/
TOS
WP
3/4"0 A325 BOLT
I SEE PLAN
3/8" GUSSET PL, TYP
`�
T�A�
oFEssioti'-'�/ 11
5" MIN
--- --� -- ------------- — - — - —
9` .y
/ O 5" MIN
`
SEA
04
HSS COLUMN, SEE
Y :•
PLANGIN
'�, 9• F
/
\
/ \
\ VERT BRACE SEE PLAN &
1/11, ABNP`��``
3/4"0 A325 BOLT, TYP
\
/
\ SECTIONS FOR SIZE AND
3/4"0 A325
314
�z�
\
BOLT TYP \ ORIENTATION
■
A 03-04-21 JEW
AP ISSUED FOR CONSTRUCTION
Rev.: Rev. date: Dwg
Chk Revisions:
OPTION A
OPTION B
Novozymes North America Inc.
3/8" GUSSET
77 Perry Chapel Church Road
PL, TYP
P.O. Box 576
NOTES:
HIPP ENGINEERING
novozymes®
Franklinton, N.C. 27525-0576 USA
Tel [phone]
1. TURN BRACING ANGLES INSIDE OR OUTSIDE AS REQD TO AVOID INTERFERENCES WITH EQUIPMENT.
2. BOLTED BRACES MAY BE ATTACHED TO EITHER SIDE OF GUSSET PL AS REQD.
NOTES:
1. BEAM SHEAR CONNECTION BY STEEL SUPPLIER, SEE 6/40701.
& CONSULTING, INC.
STEWART
Rethink Tomorrow
Est. date: 12-23-2020
NZNA - FLF
TYPICAL X BRACE CONNECTION
�
DETAIL
2301 REXW000s DRIVE, SUITE 200
Designer: AKSHAY P., PE
STRUCTURAL
RALEKGH, NC 27607
223 SOUTH WEST ST T 919.380.8750 TEL: [phone] FAX: [phone]
Scale: AS NOTED
Group no.:
TYPICAL FLOOR FRAMING SECTIONS AND DETAILS
40701 1 1/2" = V-0"
40701 TYPICAL CONN OF VERT BRACE AT BEAM COLUMN INTERSECTIONS
= "
1 1/2 1-0
SUITE 1100 FIRM LICENSE #C-1051 NC FIRM LICENSE NUMBER: C-2146
FLF40701 EW
RALEIGH, NC 27603 PROJECT #S20231.00 WWW.HIPP-USA.COM
Page no.:
_U502986_N

1/8" f
COORD W/ MEP, EQUIP & TANK VENDOR
COORD
_V-6
W/ MEP &
EQUIP
CL CL
CL CL
WALL OF CONC TANK
CL (2) 3" 0 STD PIPE,
SEE PLAN SEE PLAN
BEAM SEE PLAN
STAINLESS STEEL
SEE PLAN
L2x2x1/4 x 0'-4",
I
STAINLESS STEEL,
TYP NS/FS
1/4" STAINLESS
ClIkFFE
STEEL CAP PL, TYP
GUARDRAIL, BY SUPPLIER, 3,_�„
GUARDRAIL BY SUPPLIER
3/8" STAINLESS
SEE PLAN
SEE PLAN & 2/40701
SEE PLAN &�2/40701
STAINLESS STEEL STEEL PL
EMBED PL, BY
TANK VENDOR STAINLESS STEEL PIPE,
SEE OTHER SECTIONS
I I I
I
I
I I
- -
I I
I I
I I
T/ TANK WALL
I I
COORD W/ VENDOR
°
BEAM,SEE SHEAR CONN W/
PLAN TYP UNO
BEAM, SEE PLAN,
(2) 3/4"0 A325
TYP UNO
BOLTS, TYP
°
WALL OF CONC TANK
PLATFORM FFE
398 -8 1/4
PLATFORM FFE
398 -8 1/4
• <� I I
BY VENOOR
®Illy
o
— —^
I41
` 13
40701
III ( \ III
III \ I TYP
TYP3/16
I I \ I I
I I � I I 40701
NOTES:
1. SEE NOTES FOR STRUCTURAL STAINLESS STEEL AND WELDING ON 40001.
x
¢
IIi \ iIi
iIi �\ iIi
4 DETAIL
TYP
I
i u1 / BEAM SHEAR CONN ` 1 1 8
I I \ I I
g
�121 1/2„ 1 = -0
4
I PER 6/40701,TYP I 40701
BEAM SHEAR CONN
I � I
40702ION
CATWALK FFE I I
PER 6/40701, TYP
CATWALK FFE40701
Irill,
�
392'-2 1/4" io a
392'-2 1/4" o `'
CL
'
- -
III �' W12x22
39WR D LEVEL 2 - TOS I ® ®I 1
° - - - - - - - + - o III 7 SIM, TYP
39WR D LEVEL 2 - TOS W8x10 I I
i I ® - - - - - - ®I i 7 SIM, TYP
- -
YI---- o 0
40701
d
I
I I I I 40701
ICI I III
i i\\\ l' i i
, I,
11
HSS BEAM, SEE
I I
II \\ II
\\ I
STAINLESS STEEL PIPE,
III \\ PLAN, TYP OF 2
III I I
SEE OTHER SECTIONS I I CL (4) 1/2"0 STAINLESS
I I
I I \ I
I I \ I I
STEEL THREADED RODS ON
I \ I
III \
I I ��
7 0 BOLT CIRCLE; DRILL &
INSTALL INTO CONC FLOOR IN
SS WELD ; ;
1/4 i I i HILTI HIT HY200 ADHESIVE
I (OR APPROVED ALTERNATE),
EMBED 4-1/2" MIN)
I
o
LEVELING NUT, TYP
>
III 00 00 i
1 1 1 00 ` 40701 00
1/2"x10"0
b
I I \ I 40701
171)
STAINLESS STEEL PL
M o
I x x l
LrI
I I x \ x I I
HIGH STRENGTH, NON- ; ; BOT OF SUMP, COORD
oIi``"„
SHRINK GROUT
W/ TANK VENDOR
<"
/
p
- �_ _ °-
d d - , , , — b °
01A:°, ;
m
m
I
_ I W8X10 \\ III I
TWR D LEVEL 1 TOS I
I I 7 TYP
381-6 I ° - - - - - - °
-
_ I I / W8X10 \\
TWR D LEVEL 1 TOS i l I i I 7 TYPOF2
381-6 I ® - - - - - - ° I
I
d.
®- o 40701
o 40701
i i
I
II'I \\ II'I1
I®
I I
III \` III 1
NOTES:
1. SEE NOTES FOR STRUCTURAL STAINLESS STEEL AND WELDING ON 40001.
III
�
5 DETAIL
I
III
1 1 \ 1 1
III III
1 1 \ 1 1
40702 3" = V-0"
I
I I
I I
Itp
I I I I
I I I I
��
iII \ III
I I
I I
III / \ III
a
I
\ I
TYP OF 2 \\ i
8 \\ III
I I \ I I
WP TYP
8 TYP OF 2 III \\ III '
PUMP, BY
40701
1 \ I
\\ I
40701 I I \\
VENDOR
PEDESTAL, \\ WP TYP
SEE PLAN, �\\ I II i
TYP \ i u 4 TYP OF 2
I I `\\ I I ; 4 TYP OF 2
40301
FIN GRADE, SEE ; 40301
I �1 FIN GRADE, SEE I
B/ TANK
o a I CIVIL DWGS
T, I I
o a I I CIVIL DWGS
}
T, I I �� I I 1 PEDESTAL, SEE
d � ° COOR 0
T PEDESTAL _ _ _ f
T PEDESTAL PLAN, TYP
a d
d VENDOR
372'-6" :�d' a"
�'•-
372'-6" 1
I
a
a. p ' `a IIIIIIIIIIIIIIIIIIIIIIIIIIII --
11 I 1 11 1= I I 1 1 1 1 11 1 11 11=1 I I°' "8 a 11 1
IIIIIIIIIIIIIIIIIIIIIIII—III
=1 1 1111 11 1 1 1 11 1 11 1 11 1 11 11=1 1 11 1 11 I 1
n 1111 11 11 111 1=1 11 111 111 I 1=1 111 a ; - , a1=
1=III
11 111 1 111 I 1=1 111 111 111 111 111 111 111 I I 11 11 11
III 1 I 1 1 I F
44
—III1 I =. � :a a- a: I I 1=1 1 11 1 11 11=1 I I-1 1 11 11=1 11=1 1 11 11=1 •_; �- I I 1=1 11=
1 11 I I 1=1 11=1 1 11 1 11 11=1 1 11 1 11 11=1 11=1 I I 11 11=1 11=1
�:' g:
1 d; a�q I I
11=1 I I ". a 1-1 11 1 I I 1 1— 11=1 1 1 I I21-:1EII
III 1 11 I I I I I I I I 111 III111—
_I=1
1 11 11 1 III III11 1 11 111T/
°. ;a °
FTG (NEW) 111 = 9-=1"1 111 1„�11=11 `d` �; 111�
T FTG NEW —III I =III 1° 1 11=1=1 1111=1=11
a ° �1=1111�
369 6 - ° a III 1-
•. d
e 1 I 1
,�`; a111=1 ,°
369 6 1 ` ° a a - . �a III-
1 ` a
B/ SUMP
°
` d' . ^. . • ' ; ° ' g
=1 _. -'- �. <=••4`< -
" a - 1=
..:: °`..• d : , " ° a g A
= '_ - - _ ` g�` -d- - a_ 111=
a °
COORD W/ VENDOR
°
/ e
e
° °
_� ,•-d- _ .-' _ _,-�-•;.8 ,-
-. .- "a°fd'-..'a.a
I
_ _ .< _• _�,_ .-' _ _°�d,-�-•-
m_a_ - - _.• .. .g a°?d•-
d °
° ° ° d°
4
e
° d 4°
d
_ 'e-,•
n
—I _. 'S] _ ° .° • a .P _ _ d ,° a d _ _ I-
_
n
d •y] _ ° .d- a p - d^ a° .a d 1 I 1-1 11
-
°
°
TYP
1 d vd 3 d•e _ % .da °
d: 1 1
=I—• — — e-—d --III=
-
-1 ° a 9 . d- ad 3 d•Q _ % .'d
1 I 1 11—
— -- -- —— e-—d— —III=
5
1-1111-1-1—I 11-1 1—I 1—I 1-1-1-111111-1111�
-1-1 —I I I 1-1-1 11-1 I I I I— 1 1— I— I-111-1 —1 11-
40702
FOOTING,
SEE 2/40301
SEED 2/40301
3 40702 - 03
2 SECTION
i SECTION
�O21/2" = 1'-0"
40702 1/2" = 1'-0"
4�O21/2" = 1'-0"
CARP e.
= SEA =
045 6 =
Y
N
3141,21
■ A 03-04-21 JEW AP ISSUED FOR CONSTRUCTION
Rev.: Rev. date: Dwg Chk Revisions:
Novozymes North America Inc.
77 Perry Chapel Church Road
P.O. Box 576
novozymes- Franklinton, N.C. 27525-0576 USA
HIPP ENGINEERING Tel [phone]
Rethink Tomorrow
& CONSULTING, INC. Est. date: 12-23-2020 NZNA - FLF
STEWART
2301 REXWOODS DRIVE, SUITE 200 Designer: AKSHAY P., PE STRUCTURAL
RALEIGH, NC 27607 Scale: AS NOTED TANK D ACCESS TOWER & PLATFORM - SECTIONS AND DETAILS
223 SOUTH WEST ST T 919.380.8750 TEL: [phone] FAX: [phone]
SUITE 1100 FIRM LICENSE #C-1051 NC FIRM LICENSE NUMBER: C-2146 Group no.: IFLF407 02 U502986 EW
RALEIGH, NC 27603 PROJECT #S20231.00 WWW.HIPP-USA.COM Page no.: _N

CL
CL
CL
CL
SEE PLAN
SEE PLAN
SEE PLAN
VIF i
VIF
i
i
i
GUARDRAIL, BY SUPPLIER,
SEE PLAN AND 2/40701 BY RAILING
SUPPLIER
I
i
I
I
i SEE PLAN I
GRATING, SEE PLAN
EXIST BEAM, SEE
EXIST CATWALK
i
PAN, VIF; TYP
OVER ROAD, VIF
NEW PIPING, SEE
NEW PIPING, SEE
� 3/16
GUARDRAIL 1/4" STIFFENER PL CTRD 3/16 3 SIDES,
CONNECTION, BY
MEP DWGS, TYP
i
MEP DWGS, TYP
ON BEAM ABOVE/BELOW,
SUPPLIER
TYP; SEE NOTE 2
(E) FFE
i
EXIST BEAM,
(E) FFE
I
I
4" MIN
(4) 3/4"0 A325
CATWALK FFE BOLTS ON GAGE,
SEE PLAN, VIF
TYP PLAN, VIF;
SEE PLAN, VIF
4" MIN TYP
I TYP
MATCHIEXIST, VIF
TOS ELEV BEAM SHEAR CONN
PER 6/40701, TYP
391'-3"
i
0
1'-9" I
14"
T T
BEAM,
BEAM, SEE PLAN
BEAM, SEE PLAN,
SEE PLAN
TYP
NOTES:
NOTES:
NOTES:
1. FOR TYPICAL CATWALK CONSTRUCTION, SEE 1/40701.
1. FOR INFORMATION NOT SHOWN & NOTES, SEE 3/40703.
1. ALL STRUCTURAL
STEEL AND CONNECTIONS TO BE GALVANIZED.
2. PROVIDE STIFFENER PLATES ON BOTH SIDES OF BEAM EXCEPT WHERE PREVENTED DUE TO INTERFERENCE
WITH ANOTHER COMPONENT OR CONNECTION.
4 PS3 - PIPE
SUPPORT
DETAIL
3 PS2 - PIPE
SUPPORT DETAIL
i
NEW CATWALK - TYPICAL CONSTRUCTION
40703 3/4" = 1'-0"
40703 3/4" = 1'-0"
40703
3/4" = 1'-0"
CL
CL
EXIST COL,
I
CL (4) 3/4"0 A325 BOLTS IN
SEE PLAN, VIF
HORIZ LONG SLOTTED HOLES
1 ADJUST THIS
i
DIMENSION TO LAND
i
2 BOTTOM OF STAIR ON
3/8" CAP PL
40702 CENTERLINE
FFE
1/4" SUPPORTING BEAM
—--------------------------
i
SEE PLAN
BEAM, SEE PLAN,
I
I
(C�D
i I
i
i
z
TYP
11 TREADS @ 11"
I
I
I
I
I
I
I
-�- -
I
i
i
i
i
- - - - - -
i
----------
-
iL
GUARDRAIL, BY
SUPPLIER, SEE
I
i
i
2/40701;TYP
I
I
I
i
i 1/4
i
1/4
EXIST COL,
SEE PLAN, TYP
3/8"x4"x10" PL
FFE
3/8"x4"x11" PL W/ 3/4" 0
SEE PLAN
STD HOLES (BEYOND)
ELEVATION
PLAN
-
5 DETAIL
I
�703NTS
z
a
a
0
w
w
U)
Off
®
I
NEW STEEL STAIR W/
GRATING TREADS, BY
®
SUPPLIER
n FFE
I
SEE PLAN
-------------
— o
0
0
—
BEAM, SEE PLAN, TYP
I
II
II
u
u
1'-0" , EDGE OF
I
GRATING
I
z SECTION
40703 3/4" = V-0"
CARP �.
ES
= SEA =
045 6 =
Y
N
3/4/,21
■
A 03-04-21 JEW AP ISSUED FOR CONSTRUCTION
Rev.: Rev. date: Dwg Chk Revisions:
Novozymes North America Inc.
77 Perry Chapel Church Road
P.O. Box 576
novozymes® Franklinton, N.C. 27525-0576 USA
HIPP ENGINEERING
Tel [phone]
STEWART
& CONSULTING, INC.
Rethink Tomorrow
Est. date: 12-23-2020 NZNA - FLF
2301 REXWOODS DRIVE, SUITE 200
Designer: AKSHAY P., PE STRUCTURAL
RALEIGH, NC 27607
Scale: AS NOTED NEW AND EXISTING CATWALKS - SECTIONS AND DETAILS
223 SOUTH WEST ST
T 919.380.8750 TEL: [phone] FAX: [phone]
SUITE 1100
FIRM LICENSE #C-1051 NC FIRM LICENSE NUMBER: C-2146
Group no.: FLF40703_U502986_N EW
RALEIGH, NC 27603
PROJECT #S20231.00 WWW.HIPP-USA.COM
Page no.:
'YP

VALVES IDENTIFICATIONS NOTES
USV2D UNSPECIFIED VALVE SV23P CHANGE —OVER VALVE INSULATION SPEC. 1— FOR INSTRUMENT IDENTIFICATION AND
CAI BAL2H BALL VALVE CYJ GAT2H GATE VALVE PLUG2H PLUG VALVE >< PISTON ACTUATOR (NORMALLY CLOSED) ��� VCON1 VALVE CONNECTION MATERIAL SPEC. SYMBOLOGY REFER FLF72002.
FLANGED ENDS SEQUENTIAL NO.
BAL2P BALL VALVE WITH EQUIPMENT NUMBER FOR 0GLOBE VALVE, STRAIGHT THROUGH SOURCE OR DESTINATION DRAWING N.
PISTON ACTUATOR C� SEA2H
PLUG3H PLUG VALVE, 3—WAY � USV3H UNSPECIFIED VALVE — 3 WAY SV43P CHANGE —OVER VALVE VCON2 VALVE CONNECTION OF THE PIPE SECTION NO) 2- FOR CAD GUIDELINES REFER TO DOCUMENT
Q BAL2D BALL VALVE WITH 4 SEA2P GLOBE VALVE WITH 1 (T—BORE) (NORMALLY OPEN) SCREWED ENDS SERVICE TYPE CAD FOR EXISTING FACILITY (NZNA) 9-14-15
C� DIAPHRAGM ACTUATOR PISTON ACTUATOR NDL2X NEEDLE VALVE ADJ2H ADJUSTING VALVE VCON3 VALVE CONNECTION MEDIA LINE SIZE
ON OFF VALVE SCREWED END AND NIPPLE
BAL3H BALL VALVE, 3—WAY SEA2D DIAPHRAGM GLOBE VACTIUATOR AIR ESCAPE VALVE USJ2D ADJUSTING VALVE TH SV33P N RMALLY CLOSEDsms
DIAPHRAGM ACTUATOR ( ) VCON4 VALVE CONNECTION 77 TO V694 1"—SMS-30101-400-10
BAL3P BALL VALVE, 3—WAY WITH WELDED ENDS 2ND FL i FFG72772
C PISTON ACTUATOR [)o�l SEA3H GLOBE VALVE, 3—WAY ES02X EMERGENCY SHUT—OFF USV2M UNSPECIFIED SOLENOID VALVE SV13P ON/OFF VALVES VCON5 VALVE CONNECTION
VALVE DIAPHRAGM ACTUATOR BAL3D BALL VALVE, 3—WAY WITH SEA3P GLOBE VALVE, 3—WAY WITH NORMALLY OPEN SCREWED AND WELDED ENDS
( )
DIAPHRAGM ACTUATOR C PISTON ACTUATOR D� EXCESS FLOW VALVE USV2UA SOLENOID VALVE —BALL TYPE ELECTRONIC TO PNEUMATIC LINO. OF ORIGINATING OR DESTINATION P&ID
DIAPHRAGM ACTUATOR VALVE OPERATOR
SEA3D GLOBE VALVE, 3—WAY WITH 1
�I Bi BUTTERFLY VALVE C DIAPHRAGM ACTUATOR SPRING & ACTUATED SAFETY TR LOCATION (PORT NUMBER, FLOOR, ECT)
RELIEF VALVE DUOS SAM01 SAMPLING VALVE � TRV THERMAL RELIEF VALVE
eFP REDUCED PRESSURE 3 DIGIT SECTION NUMBER (THIRD DIGIT OPTIONAL)
BUT2P BUTTERFLY VALVE WITH �^ � SAFE —FLOW VALVE � BACKFLOW PREVENTER
PISTON ACTUATOR �' SEA2A GLOBE VALVE, ANGLE �I SAF2A SAFETY OR RELIEF VALVE DOUBLE SEAT PROCESS OR UTILITY PIPE
BUT2D BUTTERFLY VALVE WITH
DIAPHRAGM ACTUATOR .4 CHK2X CHECK VALVE, n MIXVALVE
STRAIGHT THROUGH SAli PRD2X PRESSURE REDUCING VALVE PCVD SELF REGULATING VALVE
_ MIX PROOF VALVE INSULATED PIPE
r5�1 DIA2H DIAPHRAGM VALVE ► 1 CHK2L CHECK VALVE, PRD2L PRESSURE REDUCING VALVE
STRAIGHT THROUGH SAF2x
DIA2P DIAPHRAGM VALVE WITH � ROTOVLV ROTOVALVE TRACED PIPE
PISTON ACTUATOR r CHK2A CHECK VALVE, ANGLE >_1 USV2H UNSPECIFIED VALVE FILTER REG1 FILTER REGULATOR
DIA2D DIAPHRAGM VALVE WITH BAL3D UNSPECIFIED VALVE VENDOR SUPPLIED PACKAGE
DIAPHRAGM ACTUATOR XXXXX NON —RETURN VALVE DIAPHRAGM ACTUATOR
PPE CONNECTONS_PUMPS- MSC SYMBOLS-
LINE DESIGNATION
• CON00 CONNECTION
CON01
BLIND FLANGE OR
FLANGED CONNECTION
CONO2
SCREWED TYPE JOINT
II
CONO3
CONNECTION WITH
RESTRICTION ORIFICE
CON04
HIGH PRESSURE TRI CLAMP
Ll
Ll
CON05
BAYONET CONNECTION
CON06
FLANGED CONNECTION WITH
LINE —BLIND INDICATOR
CON07
UNION CONNECTION
CON08
NIPPLE
CON09
QUICK CONNECTION
CON10
REDUCER/TRANSITION
CON11
EXPANSION JOINT
&GHT GLASS
0 SIG01 SIGHT GLASS
O
SIG03 SIGHT
GLASS WITH LIGHT
SIG02 SIGHT
GLASS WITH
FLOW
INDICATOR
O
SIG04 SIGHT
GLASS WITH
HUMIDITY
INDICATOR
FLOW METERS
C
FL001
UNSPECIFIED FLOW METER
ll
FL004
ORIFICE FLOW METER
0
FL002
VENTURI FLOW METER
®
FL005
TURBINE FLOW METER
O
FL003
ROTAMETER
BL OCK
A T TRISU TES
�vm) (0
L BLOCK ATTRIBUTE
1. DO NOT EXPLODE BLOCKS
2. BLOCKS ARE CREATED ON
LAYER"O". INSERT BLOCK
ON CORRECT LAYERS (IE.
VALVE ON LAYER EQUIP).
3. ADD INSTRUMENT SYMBOL
TO DESIGNATE AUTOMATED
VALVES
4. MOST BLOCKS CONTAIN
ATTRIBUTES. USE THE
ATTRIBUTES. DO NOT
EXPLODE AND ADD TEXT.
PD
CON12PD
CONNECT TO PROCESS SEWER
C
PCENT
CENTRIFUGAL PUMP
SD
CON12SD
CONNECT TO STORM SEWER
O
PPIST
PISTON PUMP
SS
CONI2SS
CONNECT TO SANITARY SEWER
PDIAP
AIR DIAPHRAGM PUMP
SEE DRAIN DETAILS THIS PAGE
PPINI
VACUUM PUMP OR
SCREW COMPRESSOR
CON13
HOSE/FLEXIBLE CONNECTION
00
PMONO
HOSE PUMP
L
BAYONET HALF CONNECTION
PCPMP
PROGRESSIVE CAVITY
PUMP
HOSE CONNECTION (FEMALE)
O
PLOBE
LOBE PUMP
HOSE CONNECTION (MALE)
PGEAR
GEAR PUMP
UNION UNION CONNECTION (SCREWED)
S BREAKL PIPE BREAK
0 PEND PIPE BREAK
PCAP PIPE CAP
M�SC EQUPMENT_
® SCREW CONVEYOR
® STATIC MIXER
SHELL & TUBE
HEAT EXCHANGER
PFHX PLATE & FRAME
HEAT EXCHANGER
CIP NOZZLE
CIRCUIT SETTER
IDS DIAPHRAGM SEAL
DAMP1 DAMPER
�J TAN05 AGITATOR
04 EJECTOR/EDUCTOR
I D RDISK RUPTURE DISK
SEP01 STRAINER OR INLINE FILTER
0\% (W/VALVE) STRAINER BLOWDOWN
SEP02 LIQUID SEPARATOR
SEP03 STEAM TRAP
NOT
A CCEP T% BL E % CCEP Tel BL E
U001
Qv
Q001
•
oot
v
1. VALVE ACTUATORS POINT UP
OR TO THE LEFT AS SHOWN
ABOVE
TAN04 BLADES
CCEP Tel BL E
v
use pipe connection
do not break lines
IN
NO T
CCEP T% BL E
v
D
AV
102
1. USE CONNECTOR TO CONNECT
PIPE . DO NOT BREAK LINES.
0
MOTOR, VARIABLE SPEED
EXHAUST
UPECIALTY
SITEM
DETAIL
NUMBER
FAN1 FAN
ARROWI FLOW DIRECTION
': r 3 WAY VALVE
ARROW2 FLOW DIRECTION
`R r' 3 WAY VALVE
► ARROW4 FLOW DIRECTION
SLOPE
ID5 ID FLAG
ID6 ID FLAG
TRI REV TRIANGLE
TR11 REV TRIANGLE
FOR PROCESS
FLOW DIAGRAMS
TEMP
TEMPERATURE BOX
VI SC
VISCOSITY BOX
=P
DENS
DENSITY BOX
C__P
FLOW
FLOW BOX
QINSO4
PRESSURE BOX
V% L VE
CONNEC TIONS
V012
FLANGED
SCREWED
WELDED
SCREWED & WELDED
L V107 L
CLAMPED
1. LISTED BELOW ARE EXAMPLES OF
VALVE CONNECTION TYPES
WHEN CREA TING THE P&ID THIS
INFORMA TION WILL BE ADDED.
A AIR
AF FERMENTATION AIR
Al INSTRUMENT AIR
AE EXHAUST AIR
AP PLANT AIR
ATM ATMOSPHERIC AIR (ATMOSPHERE)
AZ VACUUM AIR
BD BLOWDOWN
BF BISULFATE
B/ BISULFITE — ADDED BY PPS
B BROTH
C CONDENSATE
CCW CHILLED COOLING WATER
CCWS CHILLED COOLING WATER SUPPLY
CIF CHEMICAL FEED
CGW CHILLED WATER
CGWR CHILLED WATER RETURN
CGWS CHILLED WATER SUPPLY
CI CAST IRON
CIP CLEAN IN PLACE
CIPR CLEAN IN PLACE RETURN
CIPS CLEAN IN PLACE SUPPLY
CONC CONCENTRATE
CSL CORN STEEP LIQUOR
CW COOLING WATER
CWR COOLING WATER RETURN
CWS COOLING WATER SUPPLY
D DRAIN
GLUC GLUCOSE
HHW HOT HEATING WATER
HHWR HOT HEATING WATER RETURN
HHWS HOT HEATING WATER SUPPLY
HPO PHOSPHORIC ACID
KOH POTASSIUM HYDROXIDE
NG NATURAL GAS
NH3 ) AMMONIA, GAS
NH3 II AMMONIA, LIQUID
OAF ANTI FOAM OIL
OF FUEL OIL
OIL LUBE OIL
03 OZONE
P PROPANE
PC PUMPED CONDENSATE
PHP PHOSPHATE
PRC PRECOAT
PROD PRODUCT
PS PROCESS SLUDGE
RDL ROOF DRAIN LEADER
RML RAW MATERIAL LIQUID
RMS RAW MATERIAL SOLID
R22 R22 REFRIGERANT
S STEAM
SBM SPENT BIOMASS
SD STORM DRAIN
SH STEAM HIGH PRESSURE (-8 BARG, 115 PSIG)
SL STEAM LOW PRESSURE (N1 BARG, 15 PSIG)
SM STEAM MEDIUM PRESSURE li BARG, 45 PSIG)
SMB STEAM MEDIUM PRESSURE, BOILING
SMS STEAM MEDIUM PRESSURE, STERILIZATION
SS SANITARY SEWER
SUNS SUBSTRATE, NON —STERILE
SUC SUCROSE
SUL SULFITE
SUS SUBSTRATE, STERILE
V VENT
WBF BOILER FEED WATER
WC CITY WATER (POTABLE DRINKING WATER)
WCH HOT CITY WATER
WD DEMINERALIZED WATER
WP PLANT WATER
WPH HOT PLANT WATER
WPP PRESSURIZED PLANT WATER
WS SOFTENED WATER
WWP PROCESS WASTE WATER
WWR RECYCLED WASTE WATER
DRAIN DIRECTLY TO FLOOR
(DO NOT SHOW OR,4/N
S YMBOL)
MD
If the discharge is non —routine (ie— drain
for Maintenance activities, do not show a
drain symbol. This non —routine discharge
would be discharged directly 4"AFF (above
finished floor.
DRAIN TO FLOOR DRAIN
LP
PS = PROCESS DRAIN
SD = STORM SEWER
SS = SANITARY SEWER
If there is a discharge to a
floor drain show a floor drain
symbol which would require
the discharge be piped to a
process floor drain or trench
drain with an air gap to
meet plumbing code.
PIPE SPECIFl CA TION BREAK
400 460
1 "—SMS-30101-400 1 "—SMS-30101-460
MINIMUM D/S T% NCE
MINIMUM
DISTANCE
V471
NOTE 1
MEANINGS Of VALVE POSITIONS
NO
NORMALLY OPEN
NC
NORMALLY CLOSED
ATO
AIR TO OPEN
ATC
AIR TO CLOSE
FO
FAIL OPEN
FC
FAIL CLOSE
MISCELLANOUS ABBREVIATIONS
LP LOW POINT DRAIN
MD MAINTENANCE DRAIN
HP HIGH POINT VENT
04 Mar 2021
1 91
Hlf'f' ENGINEERWG
& CONSULTING, INC.
2301 REXWOODS DRIVE, SUITE 200
RALEIGH, NC 27607
TEL:[phone] FAX:[phone]
NC FIRM LICENSE NUMBER: C-2146
W W W.H I PP-USA.COM
03-04-2021
1 SPS I
LAV
JISSUED FOR CONSTRUCTION
Rev.:
IRev. date:
I Dwg I
lRevisions:
Novozymes North America, Inc.
77 Perry Chapel Church Road
P.O. Box 576
novozymes® ` Franklinton, N.C. 27525 0576 USA
Rethink Tomorrow Tel [phone]
Est. date: 12-10-20
NZNA NLR
PI DIAGRAM
LEGEND
Designer: SPS
Scale: NONE
Group no.:
FLF72001
U502986
— —
REF
Page no.:

NSTRUMENTATION
MEANINGS OF INSTRUMENT IDENTIFICATION LETTER
NOTES
1- FOR P&ID IDENTIFICATION AND
SYMBOLOGY REFER FLF72001.
2- FOR CAD GUIDELINES REFER TO DOCUMENT
SYMBOLS
IDENTIFICATIONS
FIRST LETTER
SUCCEEDING LETTERS
CAD FOR EXISTING FACILITY (NZNA) 9-14-15
OINS13
LOCALLY MOUNTED INSTRUMENT
SERIAL LETTER
A
ANALYSIS, e.g. pH
A
ALARM
SECTION NO.
B
NOVO=FLAME, ISA=BURNER
B
USER'S CHOICE
INS12
PANEL MOUNTED INSTRUMENT
C
NOVO=CONDUCTIVITY, ISA=USER'S CHOICE
C
CONTROLLER
e
(CENTRAL PANEL)
MEASURED VARIABLE
D
NOVO=DENSITY, ISA=USER'S CHOICE
D
DIFFERENTIAL
E
VOLTAGE
E
PRIMARY MEASURING INSTRUMENT
INS10
PANEL MOUNTED INSTRUMENT
INSTRUMENT TYPE
F
FLOW
F
RATIO
®
(LOCAL PANEL)
SERIAL NUMBER
G
NOVO=GAS (ANALYSIS/DETECTION,DISSOLVED OR FREE)
G
NOVO=USER'S CHOICE
H
ISA=USER'S CHOICE
ISA=GLASS, VIEWING DEVICE
e
INS11
REAR PANEL MOUNTED INSTRUMENT
H
I
HAND OPERATED
CURRENT
H
I
HIGH LIMIT
INDICATOR
(CENTRAL PANEL)
FTD1
J
POWER
K
CONTROL STATION
®
INS09
REAR PANEL MOUNTED INSTRUMENT
COMPLETE NUMBER OBVIOUS
K
TIME
L
LIGHT OR LOW LIMIT
(LOCAL PANEL)
L
LEVEL
M
NOVO=USER'S CHOICE
COMPLETE NUMBER NOT OBVIOUS
M
NOVO=MOISTURE OR HUMIDITY, ISA=USER'S CHOICE
N
ISA=MIDDLE INTERMEDIATE
COMBINATION FIELD MOUNTED
N
NOVO=PHOTO SENSOR, ISA=USER'S CHOICE
USER'S CHOICE
INSTRUMENTS
3OMpT01 (COMPLETE INSTRUMENT NUMBER)
P
PRESSURE
0
ORIFICE, RESTRICTION
FK
OR 0
FURNISHED WITH EQUIPMENT
Q
R
NOVO=USER'S CHOICE, ISA=QUANTITY
RADIATION
P
Q
MEASUREMENT POINT
INTEGRATE OR TOTALIZE
PACKAGE
SERIAL NUMBER
S
REVOLUTIONS OR SPEED
R
RECORDER
T
TEMPERATURE
S
SWITCH
O
HARDWARE OR SOFTWARE
TYPE OF INSTRUMENT
U
NOVO=USER'S CHOICE, ISA=MULTIVARIABLE
T
TRANSMITTER
IMPLEMENTED FUNCTION
V
NOVO=VISCOSITY, ISA=VIBRATION, MECHANICAL ANALYSIS
U
MULTI...
®
INS06
INDEPENDENT PLC FUNCTION
SERIAL LETTER (MAIN COMPONENT)
W
X
WEIGHT
UNCLASSIFIED
V
W
VALVE, DAMPER
WELL
SECTION NO. (MAIN COMPONENT)
Y
NOVO=USER'S CHOICE, ISA=EVENT, STATE, OR PRESENCE
X
UNCLASSIFIED
EXAMPLE : FLOW TRANSMITTER
Z
POSITION
Y
SIGNAL CONVERTER
IO
INS05
HARDWIRED INTERLOCK
Z
NOVO=USER'S CHOICE
ISA=DRIVER, ACTUATOR
INPUT A RRO W
A CCEP TA BL E
LA YOU T
T---,>A
A
LT
03
A
02
UNSPECIFIED INSTRUMENT LINE
ELECTRIC INSTRUMENT LINE
-•--•--•- CAPILLARY INSTRUMENT LINE
PNEUMATIC INSTRUMENT LINE
INTERNAL SYSTEM OR DATA LINK
INSTRUMENT AIR SUPPLY
TRA NSMI T TERS
FT A
01 1
FE
0,
MASS
LT A
01
PT A
01
TT A
01
TE
01
Wr PB
01
WE
0,
r01 A
AE
01
PH s
A
D
A
D
c
ANALOG INPUT
DIGITAL INPUT
ANALOG OUTPUT
DIGITAL OUTPUT
COUNTER INPUT
BCD BCD INPUT
FL O W
s ADD TYPE OF METER
MASS
MAG
ORIFlCE
ANNUBAR
VORTEX
LEVEL AND
PRESSURE
TRA NSMI T TER
TEMPERA TURF
TRA NSMI T TER
WEIGH T
TRA NSMI T TER
VIA PROFIBUS
ANAL PSIS
TRA NSIVII T TER
s ADD TYPE OF ANALYSIS
pH — pH
DO — dESOLVED OXYGEN
OOND— CONDEC71MTY
OX — OXYGEN
FREON — FREON
S W/ TCHES
D
01
�
D
01
D
01
T_71>11)
PRESSURE
TEMPERA TURF
L E VEL
FL O W
INDI CA TORS
i
01
Til
01
PRESSURE AND
TEMPERA TORE
INDI CA TORS
LOCAL NO
SIGNAL
CON TROL
VA L VES
ON OFF
VA L VE
FL O W
L E VEL
PRESSURE
TEMPERA TORE
PUMPS
P01
DIA PHRA M
PUMP W/VFD
04 Mar 2021
H I PP ENGIN EER1 NG
& CONSULTING, INC.
2301 REXWOODS DRIVL, SUI FE 200
RALEIGH, NC 27607
TEL:[phone] FAX:[phone]
NC FIRM LICENSE NUMBER: C-2146
WWW.I III'f-USA.COM
03-04-21 1 SPS I LAV JISSUED FOR CONSTRUCTION
Rev.: IRev. date: I Dwg I lRevisions:
Novozymes North America, Inc.
77 Perry Chapel Church Road
P.O. Box 576
novozymes- Eranklinton, N.C. 27525 0576 USA
Rethink Tomorrow Tel [phone]
Est. date: 1 21020 NZNA FLF
Designer: SPS PI —DIAGRAM
Scale: NONE EXAMPL F SHEET
Group
no.: FLF72002 U502986 REF
Pa e no.: —

SBM & WATER PIPING
PART 1 - GENERAL
1.0 REFER TO NOVOZYMES SPECIFICATION 130805-31-001 PIPE SPEC NO'S 30, 36, AND 55 FOR
CONSTRUCTION SPECIFICATIONS FOR ABOVEGROUND WATER AND SBM PIPING INCLUDING VALVES
AND OTHER ACCESSORIES NOT COVERED IN THIS SPECIFICATION. CONTRACTOR TO MATCH PIPING
PIPING MATERIALS EXISTING IN FIELD.
1.1 SUBMITTALS
A. PRODUCT DATA: FOR EACH TYPE OF PRODUCT INDICATED.
B. COORDINATION DRAWINGS: SHOW PIPE SIZES, LOCATIONS, AND ELEVATIONS. SHOW OTHER
PIPING IN SAME TRENCH AND CLEARANCES FROM SEWERAGE SYSTEM PIPING. INDICATE
INTERFACE AND SPATIAL RELATIONSHIP BETWEEN PIPING AND PROXIMATE STRUCTURES.
C. FIELD QUALITY -CONTROL TEST REPORTS.
D. OPERATION AND MAINTENANCE DATA: TO INCLUDE IN EMERGENCY, OPERATION, AND
MAINTENANCE MANUALS.
1.2 QUALITY ASSURANCE
A. ELECTRICAL COMPONENTS, DEVICES, AND ACCESSORIES: LISTED AND LABELED AS DEFINED
IN NFPA 70, BY A QUALIFIED TESTING AGENCY, AND MARKED FOR INTENDED LOCATION AND
APPLICATION.
B. NFPA COMPLIANCE:
1. COMPLY WITH NFPA 70, "NATIONAL ELECTRICAL CODE."
2. COMPLY WITH NFPA 318, "STANDARD FOR THE PROTECTION OF SEMICONDUCTOR
FABRICATION FACILITIES"
3. COMPLY WITH NFPA 30, "FLAMMABLE AND COMBUSTIBLE LIQUIDS CODE."
C. VALVES: MANUFACTURER'S NAME AND PRESSURE RATING SHALL BE MARKED ON VALVE
BODY.
1.3 DELIVERY, STORAGE, AND HANDLING
A. DELIVER AND STORE PIPING AND SPECIALTIES WITH SEALING PLUGS IN ENDS OR WITH END
PROTECTION.
B. DO NOT STORE PLASTIC PIPE OR FITTINGS IN DIRECT SUNLIGHT.
C. PROTECT PIPE, FITTINGS, AND SEALS FROM DIRT AND DAMAGE.
PART 2 - PRODUCTS
2.0 ALL PIPING, MATERIALS, VALVES, AND ACCESSORIES SHALL BE CAPABLE OF WITHSTANDING THE
PRESSURES AND TEMPERATURES STATED IN PART 3 OF THIS SPECIFICATION.
2.1 APPROVED ALTERNATIVE WATER PIPING
A. ABOVE GROUND
1. PVC, SCHEDULE 80; SOCKET FITTINGS; AND SOLVENT -CEMENTED JOINTS IN
ACCORDANCE WITH NZNA PIPING SPEC. NO. 30.
B. UNDERGROUND
1. PVC, SCHEDULE 80; SOCKET FITTINGS; AND SOLVENT -CEMENTED JOINTS
2.2 INSULATION
A. FOR ABOVE GROUND POTABLE WATER PIPING:
1. MINERAL -FIBER, PREFORMED PIPE INSULATION, TYPE 1: 2" THICK.
2.3 TRANSITION FITTINGS
A. PLASTIC -TO -METAL TRANSITION FITTINGS:
1. ONE-PIECE FITTING WITH ONE THREADED METAL INSERT AND ONE FUSION -JOINT END
OF MATERIAL AND WALL THICKNESS TO MATCH PLASTIC PIPE MATERIAL.
2.4 CHECK VALVES
A. SBM PIPING
1. CHECK VALVES: ONE-PIECE HDPE BODY, PE100 CLASS, SPRING ACTION, HDPE
CLOSING DISC AND STAINLESS STEEL WORKING PARTS, WITH FLANGED ENDS.
0-RINGS SHALL BE EPDM RUBBER.
B. WATER PIPING
1. CHECK VALVES: BRONZE BODY WITH SPRING LOADED REINFORCED TFE BALL AND
SCREWED ENDS.
2.5 BALL VALVES
A. SBM PIPING
1. BALL VALVES: 1/2 TO 2 INCHES; 200 PSI AT 74 DEG F. HDPE BODY AND BALL,
EPDM SEAT AND SEAL, STAINLESS STEEL STEM, FULL BORE, BUTT FUSION END
CONNECTIONS. FLANGED END CONNECTIONS IF REQUIRED. NSF STANDARD 61
CERTIFIED.
2. BALL VALVES: 2 TO 12 INCHES; 200 PSI AT 74 DEG F. HDPE BODY AND BALL,
EPDM SEAT AND SEAL, STAINLESS STEEL STEM, FULL BORE, BUTT FUSION END
CONNECTIONS. FLANGED END CONNECTIONS IF REQUIRED. NSF STANDARD 61
CERTIFIED.
B. WATER PIPING
1. BALL VALVES: 1" AND LESS; ASTM B62 BRONZE BODY AND CHROMIUM PLATED BALL
WITH 1-1 /4" EXTENSION STEM AND SCREWED ENDS.
2.6 BUTTERFLY VALVES:
A. HDPE BUTTERFLY VALVES, 2-1/2" AND LARGER, PE100 CLASS, FUSIBLE WAFER STYLE,
HDPE BODY WITH 316 SS STEM AND DISC AND FLANGED END CONNECTIONS. OPERATING
LEVER FOR 2-6" SIZES AND GEARBOX FOR 8"-10" SIZES.
2.7 SLURRY FLEX HOSE:
A. 6" ID BLACK NATURAL RUBBER BLEND TUBE, 1 /4" THICK, WITH SMOOTH SBR 3/32" THICK
COVER AND HIGH TENSILE STRENGTH CORD REINFORCEMENT. PRESSURE/VACUUM RATED
FOR 150 PSI AND A SAFETY FACTOR OF 4:1.
PART - 3 EXECUTION
3.0 PERFORMANCE REQUIREMENTS
A. PIPING, COMPONENTS, AND INSTALLATION SHALL BE CAPABLE OF WITHSTANDING THE
FOLLOWING WORKING PRESSURES AND TEMPERATURES:
1. SBM PIPING: 80 PSIG AND 73 DEG F.
2. WATER PIPING: 125 PSIG, 200 DEG F.
3.1 PIPING INSTALLATION
A. DRAWING PLANS, SCHEMATICS, AND DIAGRAMS INDICATE GENERAL LOCATION AND
ARRANGEMENT OF PIPING SYSTEMS. INSTALL PIPING AS INDICATED UNLESS DEVIATIONS TO
LAYOUT ARE APPROVED ON COORDINATION DRAWINGS.
B. INSTALL PIPING TO PERMIT VALVE SERVICING.
C. INSTALL PIPING FREE OF SAGS AND BENDS.
D. INSTALL FITTINGS FOR CHANGES IN DIRECTION AND BRANCH CONNECTIONS.
E. INSTALL PIPING TO ALLOW APPLICATION OF INSULATION IF REQUIRED.
F. SELECT SYSTEM COMPONENTS WITH PRESSURE RATING EQUAL TO OR GREATER THAN
SYSTEM OPERATING PRESSURE.
G. REDUCE PIPE SIZES USING ECCENTRIC REDUCER FITTING INSTALLED WITH LEVEL SIDE UP.
H. INSTALL BRANCH CONNECTIONS TO MAINS USING MECHANICALLY FORMED TEE FITTINGS IN
MAIN PIPE, WITH THE BRANCH CONNECTED TO THE BOTTOM OF THE MAIN PIPE. FOR
UP -FEED RISERS, CONNECT THE BRANCH TO THE TOP OF THE MAIN PIPE.
3.2 VALVE INSTALLATION
A. VALVES SHALL BE THE FULL SIZE OF THE LINE IN WHICH THEY ARE INSTALLED.
B. INSTALL VALVES IN NEAT ARRANGEMENTS WITH ACCESSIBILITY FOR MAINTENANCE.
3.3 HANGER AND SUPPORT INSTALLATION
A. INSTALL THE FOLLOWING:
1. VERTICAL PIPING: MSS TYPE 8 OR MSS TYPE 42, RISER CLAMPS.
2. INDIVIDUAL, STRAIGHT, HORIZONTAL PIPING RUNS:
a. 100 FEET AND LESS: MSS TYPE 1, ADJUSTABLE, STEEL CLEVIS HANGERS.
b. LONGER THAN 100 FEET: MSS TYPE 43, ADJUSTABLE ROLLER HANGERS.
c. LONGER THAN 100 FEET, IF INDICATED: MSS TYPE 49, SPRING CUSHION ROLLS.
3. MULTIPLE, STRAIGHT, HORIZONTAL PIPING RUNS 100 FEET OR LONGER: MSS TYPE
44, PIPE ROLLS.
4. BASE OF VERTICAL PIPING: MSS TYPE 52, SPRING HANGERS.
B. SUPPORT HORIZONTAL PIPING AND TUBING WITHIN 12 INCHES OF EACH FITTING AND
COUPLING.
C. INSTALL PIPE SUPPORTS WITH THE MAXIMUM HORIZONTAL SPACING AND MINIMUM ROD
DIAMETERS AS INDICATED BY PIPING MANUFACTURER OR THE NORTH CAROLINA
MECHANICAL CODE, WHICHEVER IS MORE STRINGENT.
D. VERTICAL PVC PIPING SHOULD BE SUPPORTED PROPERLY AND HAVE A MID -STORY GUIDE
OR IN ACCORDANCE WITH PIPING MANUFACTURER'S GUIDELINES.
E. THE PIPE SHOULD NOT BE ANCHORED TIGHTLY BY THE SUPPORT, BUT SECURED IN A
MANNER TO ALLOW FOR MOVEMENT CAUSED BY THERMAL EXPANSION AND CONTRACTION.
F. PIPE HANGERS AND SUPPORTS MUST BE COMPATIBLE WITH HDPE. ANY METAL HANGERS
SHOULD HAVE A PLASTIC INSERT BETWEEN THE HDPE AND METAL SUPPORT.
3.4 CONNECTIONS
A. DRAWINGS INDICATE GENERAL ARRANGEMENT OF PIPING, FITTINGS, AND SPECIALTIES.
B. MAKE CONNECTIONS TO EXISTING PIPING SO FINISHED WORK COMPLIES AS NEARLY AS
PRACTICAL WITH REQUIREMENTS SPECIFIED FOR NEW WORK.
C. INSTALL PIPING ADJACENT TO EQUIPMENT TO ALLOW SERVICE AND MAINTENANCE.
3.5 LABELING AND IDENTIFICATION
A. PIPING SHALL BE LABELED IN ACCORDANCE WITH NOVOZYMES STANDARDS.
3.6 TESTING
A. BEFORE CONDUCTING TESTS, VALVE -OFF OR DISCONNECT ANY EQUIPMENT AND APPARATUS
WHICH MAY BE DAMAGED BY THE TEST PRESSURES HIGHER THAN NORMAL WORKING
PRESSURES. ALL TESTING SHALL BE WITNESSED AND APPROVED BY THE OWNER.
B. PRESSURE SYSTEMS:
1. THE SYSTEM SHALL BE TESTED IN ACCORDANCE WITH ALL LOCAL
PLUMBING/MECHANICAL CODES HAVING JURISDICTION IN THE TERRITORY WHERE THE
INSTALLATION IS TO TAKE PLACE. ALL SECTIONS SHALL BE HYDRAULICALLY TESTED
TO A MAXIMUM OF 150% OF THE DESIGNED WORKING PRESSURE.
C. REPLACE LEAKING PIPING USING NEW MATERIALS, AND REPEAT TESTING UNTIL LEAKAGE IS
WITHIN ALLOWANCES SPECIFIED.
D. PIPING WILL BE CONSIDERED DEFECTIVE IF IT DOES NOT PASS TESTS AND INSPECTIONS.
E. PREPARE TEST AND INSPECTION REPORTS.
3.7 CLEANING
A. USE PROCEDURES PRESCRIBED BY AUTHORITIES HAVING JURISDICTION OR, IF NOT
PRESCRIBED, USE PROCEDURES DESCRIBED BELOW:
1. PURGE NEW PIPING AND PARTS OF EXISTING PIPING THAT HAVE BEEN ALTERED,
EXTENDED, OR REPAIRED BEFORE USING.
2. CLEAN PIPING BY FLUSHING WITH POTABLE WATER.
3.8 PERFORM THE FOLLOWING BEFORE OPERATING THE SYSTEM:
A. OPEN MANUAL VALVES FULLY.
B. INSPECT PUMPS FOR PROPER ROTATION.
C. VERIFY LUBRICATION OF MOTORS AND BEARINGS.
10" DIA. PIPE
TYP.
BAR 1/2
11x1 "xWIDTF
STEEL SUF
6" DIA. PI
TYP
BAR 1/'e
"x1 "xWIDT
STEEL SU
3/8" STEEL PLATE
GALV. ROLLED TO I.D.
TO FIT O.D. OF PIPE
1/4" STEEL PLATE
3/8" THICK
PLATE 12"
LONG
PIPING SUPPO�TDETAIL
� NOT TO SCALE
FEEL PLATE
TOLLED TO I.D.
O.D. OF PIPING
EL PLATE
SICK
12"
PIPING SUPPORT DETAIL
NOT TO SCALE
1 /8" 1 /8" TH K SS
REINFORCING PAD USE
ONLY FOR SS PIPE
DO NOT CUT HOLE
IN HEADER OR PAD
1 /4"
1 /4" �
BASE PLATE ASTM A36
1/8"0 VENT HOLE
- PIPE "A" ASTM A53
1/4"0 VENT HOLE
1 1/2" GROUT
(4) EXPANSION ANCHORS
EDGE DIM. (TYP.)
(PIPE SIZE - 2" THRU 36")
3 BASE ELBOW- RIGID
NOT TO SCALE
B-LINE B2000
SERIES P.100
(STRUT CATALOG)
'2SH
1 .TV
SERIES P. 51 (STRUT
(STRUT CATALOG)
CATALOG)
NOTES:
1. SIZE STRUT AND CLAMP TO ADEQUATELY SUPPORT LOAD
(REFER TO B-LINE STRUT CATALOG).
2. B2000 AVAILABLE IN ZINC PLATED, HOT -DIP GALVANIZED,
PVC COATED, COPPER PAINTED, STAINLESS STEEL AND
ALUMINUM.
3. STRUT AVAILABLE IN DURAGREENT) EPDXY PAINTED,
GALVANIZED, HOT -DIP GALVANIZED, PVC COATED,
STAINLESS STEEL AND ALUMINUM.
HANGING MULTIPLE PIPE SUPPORT
NO SCALE
04 Mar 2021
HIPP ENGINEERING
& CONSULTING, INC.
2301 REXWOODS DRIVE, SUITE 200
RALEIGH, NC 27607
TEL:[phone] FAX:[phone]
NC FIRM LICENSE NUMBER: C-2146
WWW.HIPP-USA.COM

KEY NOTES
NOTE:
0
MINIMUM STRAIGHT LENGTH OF PIPE TO
BE 50"
CONTROL SIGNAL DESIGN NOT IN
UPSTREAM OF RECIRCULATION PUMP.
FLF96DP01
FLF96DP02
FLF96DT
FLF96ED01-10
H I PP SCOPE AND I S NOT
O
MINIMUM STRAIGHT LENGTH OF PIPE TO
BE 30"
SBM LOADING PUMP
RECIRCULATION PUMP
SBM STORAGE TANK
2" FNPT EDUCTOR
UPSTREAM OF FLOW METER.
DEPICTED ON THIS P&I D
VULCAN HDS 20OL-A
GOULDS MODEL JC
1.645M GAL
138 GPM MOTIVE,
3
0
MINIMUM STRAIGHT LENGTH OF PIPE TO
BE 12"
8A 925 GPM @ 25' TDH
1450 GPM @ 145' TDH
100' DIA X 28'H
689 GPM OUTLET,
DOWNSTREAM OF FLOW METER.
15HP, 460V/3P/60HZ
125HP, 460V/3P/60HZ
5l 65FT MAX PLUME
O
TRANSITION FROM HDPE TO CAST IRON
EDUCTOR RING
PROVIDED BY VENDOR.
O
REFERENCE DETAIL 1 pH PROBE ASSEMBLY ON
DRAWING FLF84001.
O
CONTROL SCOPE FOR VFD BY OWNER.
GJVI RGl1VVlJVLJ0 LJRIVL, JUIIL LUU
RALEIGH, NC 27607
TEL:[phone] FAX:[phone]
NC FIRM LICENSE NUMBER: C-2146
VAM.HIPP-USA.COM
ONOVOZYMES PIPE SPECIFICATION 30 TO BE USED AS
ALTERNATE TO MATCH EXISTING PIPING.
O HEAT TRACE 1 /2" WATER LINE; SEE ELECTRICAL
PLANS FOR HEAT TRACING INFORMATION.
0 1" TAP UPSTREAM OF CHECK VALVE; BALL VALVE TO
BE OPENED TO ALLOW FOR VENTING BACK TO TANK.
LEGEND
REDUCER
M
MOTOR OPERATED VALVE
0
SOLENOID OPERATED VALVE
'I
DIAPHRAGM OPERATED VALVE
PLUG VALVE
1�81-
BALL VALVE
1>4
CHECK VALVE
F7470-
BUTTERFLY VALVE
II
KNIFE GATE
T
C.
CONTROL VALVE
FLOW METER
WYE STRAINER
6Aq 03-04-21 1 SPS I LAV I ISSUED FOR CONSTRUCTION
924-98 RB SAST I REVISED PER FIELD COMMENTS
Rev.: Rev. date: Dwa Chk Revisions:
Novo
Nordisk
BioChem, North
Americo (NNBNA)
0
Novo Nordisk
BioChem North
America State Road 1003 P.O. Box 576 Franklinton, N.C. 27525 USA Tel [phone]
Z
a
Est. date:
01 /06/97
NNBNA FH G
Designer:
RB
PI —DIAGRAM
• z
TREATED SBM
STORAGE FACILITIES
Scale: NONE
Group na
FAA72963
U502986
Page no.:
—

3" 0 RECIRCULATION LINE
EXISTING 0.67mg SBM TANK
� EQUIP # FLF96AT
\ I �
I I
�I- - - - - - - - - - - - -
I I
I
N --
TRUCK
APRON
I&
MCC
FLF69MM
a_
VFD
D0
12'X14' PAD
0
c�CD
FOR NEW
v J
PUMP & MCC
w LL
ry
PAD
—7
MOUNTED
UTILITY
8'_2"
TRANSFORMER
O
EXISTING 1.645m.g. SBM TANK
EQUIP # FLF96CT
TOP EXISTING TANK
WALL = 396.24 /
i
i
\
1+
40.75'
2'0"
C
SBM LOADING PUMP
FLF96DPOl
\ 39`
\O , \
( EDUCTOR RING
0100'0" ID
20'0" CLEAR
NEW SP
6FLF D TANK
,227 m3 1,645,000 GAL
/N CARp�
040380
WN��
04Mar 2021
Fib?
HIPP ENGINEERING
& CONSULTING, INC.
2301 KEXWOODS DRIVE, SUITE 200
R-ALEIGH, NC 27607
TEL:[phone] FAX:[phone]
NC FIRM LICENSE NUMBER: C-2146
WWW.HIPP-USA.COM
KEY NOTES
O 72" DIA. X 48" DEEP SUMP BY TANK VENDOR. SEE
SECTION C ON DRAWING FLF74003.
O EDUCTOR RING PROVIDED BY VENDOR. CONTRACTOR
TO COORDINATE FINAL LOCATION.
O3 TRANSFORMER PAD TO BE LOCATED EAST OF THE
TANK, JUST NORTH OF THE SERVICE ROAD. BOLLARD
PROTECTION TO BE PROVIDED AROUND PAD.
COORDINATE EXACT LOCATION WITH OWNER AND DUKE
ENERGY.
M
122' B"
03-04-21 1 SPS I LAV JISSUED FOR CONSTRUCTION
Rev.: Rev. date: I Dwc I lRevisions:
novozymes�
Rethink Tomorrow
Est. date: 12-10-20
Desi ner. SPS
Scale: 1 8" V 0"
Group no.:
Page no.:
Novozymes North America, Inc.
77 Perry Chapel Church Road
P.O. Box 576
Franklinton, N.C. 275250576 USA
Tel [phone]
NZNA — FLF
MECHANICAL PROCESS
FLF96DT GENERAL ARRANGEMENT
FLF75001 U502986 NEW

3"0 RECIRCULATION LINE
EXISTING 0.67mg SBM TANK
� EQUIP # FLF96AT
\ I �
? 6 "B" TRUCK LOADING
? 6"0 TANK "C
? 2"0 DRAIN LINE
EXISTING 6"0 TRUCK LOADING
2"0 DRAIN LINE TO EXISTING SUMP PIT
CORE DRILL SUMP SOFFITT AND SEAL
WITH 6 LINKS OF LINK —SEAL LS-300—S
?= 392.06'
TOP EXISTING TANK
\ WALL = 396.24
v 41
4"0 RECIRC LINE
SWING JOINT (TYR)
0 TANK TRUCK LOADING LINE �?= 392.88'
6" TRANSFER LINE (TOP)
6110 TA "C" FILL LINE (BOTT)
7= 392.82'
REFIT XFR LINE
Ill IN-11 MvM
V---TT.
•s:1= =�I'- � �� — 11111 IIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIiYIIIIIIIII IIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIII� INNMM-IIIIIIIh1
---- � IIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIII
• .. IIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIII
© ,dl
. ,Ills^
qi�; • •
• � D • • III l=
RECIRV PUMP
ELF 6DP02
TRUCK
APRON
6"—SI
INL
?= 392.56'
T
39244
_mil mow♦
6" LOADOUT
\
1 /2 WC
8"—SBM
EL= 380.58' 8 S B M
2 AE \\
c 01 V
F 740 3 — — \ 0'
14,
10"-SBM \ \
EL= 373.50' \
EXISTING 1.645m.g. SBM TANK
EQUIP # FLF96CT
6" BYPASS
BACK TO TANK
DOWN TO
LOADOUT LINE
C,
SBM LOADING PUMP
O FLF96DPOl
1
8"-SBM
�O` EL=369.24'
1 \
\
\
�c
�o \
\
\
NEW SBM LLF D TANK
6,227 m3 1,645,000 GAL_
�N CARO�
�o oFEss/o/ w
� 040380 �
Q1V�NGINEFwNE v0���
04 Mar 2021
GENERAL NOTES
1. NUMBER AND LOCATION OF PIPE SUPPORTS IS
FOR REFERENCE ONLY. CONTRACTOR TO VERIFY
MAXIMUM SPACING DISTANCE WITH PIPE VENDOR.
2. REFERENCE STRUCTURAL DRAWINGS FOR PIPE
SUPPORT DETAILS.
3. SEE DRAWING FLF73001 FOR EXISTING TANKS
AND PIPING.
4. ELEVATIONS ARE SHOWN AT CENTERLINE OF
PIPING; TYPICAL FOR ALL UNLESS OTHERWISE
NOTED.
KEY NOTES
(D
MINIMUM PIPE PENETRATION IS BOP 3'-10" ABOVE TANK
BOTTOM. TANK VENDOR TO PROVIDE PIPE SUPPORTS
�\
WITHIN TANK.
0
pH PROBE LOCATED BELOW PIPE. SEE SECTION VIEW FOR
MORE DETAIL.
O
FOR CONTINUATION REFERENCE ENLARGED PIPING PLAN
VIEW 1 ON SHEET FL74003.
O
FLOW TRANSMITTER FIT-01 AND HAND SWITCH HS-03
TO BE LOCATED AT TRUCK LOADOUT 4'-0" ABOVE
FINISHED GRADE.
0
1" VENT TO BE FIELD ROUTED TO TANK. CONTRACTOR
TO COORDINATE PIPING PENETRATION WITH TANK
VENDOR. BALL VALVE IN VERTICAL TO BE OPENED TO
ALLOW FOR VENTING BACK TO TANK.
OWATER
PIPING TO BE ROUTED UNDERGROUND IN THIS
LOCATION.
HIPP ENGINEERING
& CONSULTING, INC.
2301 REXWOODS DRIVE, SUITE 200
RALEIGH, NC 27607
TEL:[phone] FAX:[phone]
NC FIRM LICENSE NUMBER: C-2146
WWW.HIP-USA.COM
,y 1 03-04—,)1 I S 'S I I AV I SSU-C ECR CONSTRUCTION
Rev.: lRev. date: I -)wg I jRevisions7
Novozymes North America, Inc.
77 Perry Chapel Church Road
P.O. Box 576
novozymes® FrankJnton, N.C. 27525 0576 USA
Rethink Tomorrow Tel [phone]
Est. date: 12-10-20 NZNA EL_E
Desi ner: SPS MECHANICAL PROCESS
Scale: PIPING ARRANGEMENT TO FL_F96DT
Group no.: FLF73002 U502986 NEW
Page no.: — —

6"_SBM
ENLARGED PIPING PLAN
SCALE: 1 /8"=1'-0"
6"—SBM
6"—SBM PUMP 6"—SBM TRUCK TANK
DISCH LOAD —OUT BYPASS
q»
6"—SBM BYPASS
I I I
I I I
I r--------- ------- ---------------
-
--- ------
I I I
I I I
I I I
I I I
I I I
I I I
L J L _
NOTE: STRUCTURE SHOWN
FOR REFERENCE ONLY.
SECTION rD
SCALE: 3/8"=1'-0" F 3 1
RECIRC PUMP
FLF96DP02
PAD
EL 371.
1
6"—SBM TANK FILL
77
10?
16
REFERENCE S
DRAWING
6"-SBM 6"-SBM
LOADOUT FILL
TANK 6"-SBM PUMP 6"-SBM
TANK
WALL DISCH. BYPASS
2'-52„ 3'-516» 2'-32»
6"-SBM
BYPASS
6" 1'-44„
II
II
II
II
II
III
II
II
II
II
II
SECTIONrA
SCALE: 3/8"=1'-0" F 3 1
- 1116"-SBM BYPASS
I I \\ I I
/ \\
,I TOC TANK
WALL=396.24
I• I I I / j \\ \ I I
�• � I I // \ I I I
I I
I I
I I
I. I
I — — — — I
I
I• I
I
J
I I
I
I I 6"—SBM
7D--
• I
I I
_FILL
I I EL. 389'-9"
I I
I• I
I' I
I I
L J
lel
I.I
I I
I. I
ICI
NOTE: STRUCTURE SHOWN
ICI
FOR REFERENCE ONLY.
I•q
I .I
I I
I I
I �I
I
SECTIONrE
p •I SCALE: 3/8"=1'-0" F 3 1
I I
I 'I
I. I
I J
I I
Iel
Iy
I. I
I �
I I
I I
I �
I I
I•el
I I
I I
I I
I I
J
Li
U
Q
a
d
I
6'—SBM BYPASS
EL. 389'-9"
I
I
I
I
I
I
I
6"—SBM PUMP
HDPE
FLEX
T
EL= 394.49'
6"SBM BYPASS
6"-SBM LOADOU
EL=39256'
SECTION B
SCALE: 3/8"=1'-0" F 3 1
" 6"-SBM
6-SBM
6"-SBM PUMP TANK
DISCH LOADOUT BYPASS
2, 52„ 3, 516„ 2,-92„
6"-SBM
BYPASS
1'-44„
I
is mI =
---------- ---
---------- i I i
I I I
I I
I I
I I
,I TOC TANK
WALL=396.24
L I I I/
I I I r
I• I I I
I I 6"—SBM
I• I I I LOADOU_
I I I I
I• I I I
I' I L J
�.I
I
I
I. I
I•I
I I
I I
I•I
I.q
I .I
I I
I I
I �I
I
I
I I
\
\
I
I
I
\ \
\ \
I
I I
\ \
\ \
I I
I I
\ \
I I
\
I
I I
I \
III
I I
I I
I
\I
v I
I I
I
I
I I
I I
i
I
I I
NOTE: STRUCTURE SHOWN
FOR REFERENCE ONLY.
I•• SECTIONrF
SCALE: 3/8"=1'-0" F730 1
I
I
I �
I I
lel
ly
I �
I I
I I
I �
I I
I
I I
I I
6"=SBM BYPASS
EL. 389'-9"
x
I
I
I
I
I
I
I
I
cn
w
�
J
Q
=
w
U
0
o
I
CD
w
w
J
w
w
6'
SECTION rc_"'�
SCALE: 3/8"=1'-0" F 3 1
RAIL GUIDES AND SUPPORTS
LOCATED EVERY FIVE FEET
MAXIMUM. SEE STRUCTURAL
DRAWINGS FOR MORE
INFORMATION.
CAR��i
Ess/o�� w
� 040380 �
FNGINV-
ti gNNE v
04 Mar 2021
I IF ?
HIPP ENGINEERING
& CONSULTING, INC.
2301 REXWOODS DRIVE, SUITE 200
RALEIGH, NC 27607
TEL:[phone] FAX:[phone]
NC FIRM LICENSE NUMBER: C-2146
W W W.HIPP-USA.COM

POWER, SIGHTING 8c MIS(. SYSTEM
ABBREVIATIONS,, LEGEND 8c SYMBOLS
GENERAL TERM
SINGLE
LINE DIAGRAM SYMBOLS
POWER
AND CONTROL PLAN SYMBOLS
POWER AND LIGHTING PLAN SYMBOLS
CONTROL
SCHEMATIC DIAGRAM SYMBOLS
GRAPHIC SYMBOLS
ABBREVIATI❑NS
A
AMPERES
BUS
SERVICE OR FEEDER CIRCUIT
FLUORESCENT FIXTURE - 2'X 4'
O
CIRCUIT CONNECTION
A/C
AIR CONDITIONING
RUN EXPOSED
THRU SECTION
AFF
AL
ABOVE FINISHED FLOOR
ALUMINUM
CABLE
BRANCH CIRCUIT RUN EXPOSED
®
FLUORESCENT FIXTURE - 2'X 4' - NIGHT LIGHT
FLUORESCENT FIXTURE - VX 4'
O
1
TERMINAL
PUSHBUTTON -SINGLE CIRCUIT
DIRECTION OF VIE
2 SECTION DESIGNATION 2
BOT
BOTTOM OF TRAY
NORMALLY OPEN -MOMENTARY
C
CONDUIT
O
TERMINAL
BRANCH CIRCUIT RUN CONCEALED IN
FLUORESCENT FIXTURE - 1'X 4' - NIGHT LIGHT
800-7 SHEET NUMBER WHERE SECTION CAN BE F❑UNB--
CAT.No.
CATALOGUE NUMBER
CEILING, WALL OR IN/UNDER FLOOR
PUSHBUTTON -SINGLE CIRCUIT
(❑MITTED WHEN SHOWN [IN SAME SHEET)
CB
CIRCUIT BREAKER
NORMALLY CLOSED -MOMENTARY
CLG
CEILING
O
CONNECTION
UNDERGROUND DIRECT BURIAL
®
FLUORESCENT FIXTURE - 1'X 4' - CONTINUOS ROW
CKT, CCT CIRCUIT
SELECTOR SWITCH -DOUBLE
ELEVATION
CL
CURRENT LIMITING}
Q
HID FIXTURE
CIRCUIT -ONE OPEN -ONE
SECTION
TRANSFORMER
UNDERGROUND DUCT LINE
CLOSED -MAINTAINED
DIRECTION OF VIEW 2
CONT
CONTINUED
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OVERLOAD ELEMENT
CP
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0
HID FIXTURE - NIGHT LIGHT
SECTI❑N DESIGNATI❑N ELEVATI❑N NUMBE
CPT
CONTROL POWER TRANSFORMER
0
DELTA WINDING
E:
CROSS SECTION IDENTIFICATION
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3 1 1 3
CT
CURRENT TRANSFORMER
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-
CU
COPPER
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DIA
DIAMETER
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BATTERY OPERATED EMERGENCY FIXTURE
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DN
DOWN
FOR MULTIPLE ELEVATI❑NS, SAME INTERI❑R
DT
DUST TIGHT
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GROUND
H❑
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DRAWING
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TRANSFORMER
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ELECTRICAL
INDICATES FACE OF FIXTURE
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ELEVATION
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THIN WALL CONDUIT
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O- -0
CIRCUIT BREAKER
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SERVICE WEATHERHEAD
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ono
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ELECTRIC WATER COOLER
THREE WAY SWITCH
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FIXTURE
FUSE
PULL BOX,DEVICE BOX,SOLENOID
VALVE, LIMIT SWITCH,ETC.
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SINGLE RECEPTACLE OUTLET
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OPERATING COIL OF MAGNETIC STARTER
AREA ENLARGED SHEET NUMBER FOR
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FLOOR
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DUPLEX RECEPTACLE OUTLET
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OPERATING COIL OF CONTROL RELAY
LETTER OF ADJACENT AREA
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FULL LOAD AMPERES
FUSE
DRAWOUT CONTACT
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JUNCTION BOX
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OPERATING COIL OF TIMING RELAY
COLUMN MARK A REVISION MARK
-0
QUADRUPLEX RECEPTACLE OUTLET
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FLTS
FLOW SWITCH
FLOAT SWITCH
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CONTACT
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WELDING RECEPTACLE
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SINGLE SPECIAL-PURPOSE RECEPTACLE OUTLET
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GROUND
OVERLOAD
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SPECIAL PURPOSE RECEPTACLE
O
PILOT LIGHT
ELEVATION MARK ROOM NUMBER 126
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CLOCK HANGER RECEPTACLE
HP
HORSEPOWER
- -
NORMALLY OPEN CONTACT
POTENTIAL TRANSFORMER
0
CONDUIT -TURNED UP
MULTIOUTLET ASSEMBLY
NORMALLY CLOSED CONTACT
AUXILIARY PLAN SYMBOLS
VICINITY M A P
INST
INSTRUMENT
IMC
INTERMEDIATE METAL CONDUIT
CURRENT TRANSFORMER
0
CONDUIT -TURNED DOWN
FLOOR DUPLEX RECEPTACLE OUTLET, WP
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NORMALLY OPEN LIMIT SWITCH
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INTERRUPTING SHORT CIRCUIT
FACP
FIRE ALARM CONTROL PANEL
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JUNCTION BOX
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CAPACITOR
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NORMALLY CLOSED LIMIT SWITCH
FAAP
FIRE ALARM ANNUNCIATOR PANEL
F R A N K L I N T❑ N
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WALL TELEPHONE OUTLET
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FLOW -ACTUATED SWITCH
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LIMIT SWITCH
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SURGE ARRESTOR
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CONDUIT SEAL FITTING
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FIRE ALARM HORN AND VISUAL
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LVLS
LIGHTING
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FLOOR TELEPHONE OUTLET, WP
FLOW -ACTUATED SWITCH
FIRE ALARM BELL
1
q0
AMMETER
FLEXIBLE CONDUIT
OPENS ON INCREASE IN FLOW
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FIRE ALARM PULL STATION
JUNCTION BOX AND UNDERFLOOR SINGLE DUCT
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LIQUID -LEVEL -ACTUATED SWITCH
MAX
MAXIMUM
GVOLTMETER
MOTOR, NO. INDICATES HORSEPOWER
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WATER FLOW SWITCH
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MCC
MECH
MOTOR CONTROL CENTER
MECHANICAL
JUNCTION BOX AND UNDERFLOOR DOUBLE DUCT
LIQUID-LEVEL-ACTUATEDSWITCH
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TAMPER SWITCH
56''
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WATTHOUR METER
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DISCONNECT SWITCH, NON -FUSED
ENS E
MIN
MTD
MINIMUM
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PHOTO CELL
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PRESSURE -OR VACUUM -ACTUATED SWITCH
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FIRE ALARM SMOKE DETECTOR
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POWER FACTOR METER
FUSED DISCONNECT SWITCH
CLOSES ON RISING PRESSURE
P R E J E C T
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FIRE ALARM HEAT DETECTOR
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NOT IN CONTRACT
PANELBOARD
PRESSURE -OR VACUUM -ACTUATED SWITCH
SITE
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NUMBER
AS
AMMETER SWITCHr7l
COMBINATION ER &FUSED
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END OF LINE RESISTOR
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DISCONNECT SWITCH
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POWER PANEL
o
TEMPERATURE -ACTUATED SWITCH
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TROUBLE BELL
VOLTMETER SWITCH
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CIRCUIT BREAKER
0
JUNCTION BOX
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HORN TYPE SPEAKER
70
P
POLE
TEMPERATURE -ACTUATED SWITCH
40
PB
PUSHBUTTON
MAGNETIC STARTER
PANELBOARD
C:=
CABINET
OPENS ON RISING TEMPERATURE
O
BAFFLE TYPE SPEAKER
64
PNLBD
PANELBOARD
PRI
PRIMARY
BRANCH CIRCUIT RUN EXPOSED
o
NORMALLY OPEN SWITCH
TTC
TELEPHONE TERMINAL CABINET
PS
PRESSURE SWITCH
O O
PUSHBUTTON CONTROL STATION
®
POWER PANEL
WITH TIME -DELAY CLOSING
PT
POTENTIAL TRANSFORMER
BRANCH CIRCUIT RUN CONCEALED IN CEILING,
DTC
DATA TERMINAL CABINET
WALL,IN/UNDER FLOOR
NORMALLY CLOSED SWITCH
1
SELECTOR SWITCH
p
PUSHBUTTON CONTROL STATION
WITH TIME -DELAY OPENING
AMP
PUBLIC ADDRESS AMPLIFIER
401 70
RGC
RIGID GALVANIZED CONDUIT
CONTROL STATION
0
BRANCH CIRCUIT HOME RUN TO PANELBOARD
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RT
RAINTIGHT
(NUMBER OF ARROWS INDICATES NUMBER OF CIRCUITS)
°�o
NORMALLY OPEN SWITCH
WITH DELAY OPENING
R A L E I G H
ENCLOSURE
SELECTOR SWITCH CONTROL STATION
SEC
SECONDARY
SLASHED LINES INDICATE NUMBER OF WIRES
SHLD
SHIELD
(LONG SLASH INDICATES NEUTRAL)
NORMALLY CLOSED SWITCH
D U R H A M
SPEAKER
O
PROTECTIVE RELAY
MANUAL MOTOR STARTER,
WITH TIME -DELAY CLOSING
SPKR
'T' INDICATES THERMAL OVERLOAD
_A_
FLEXIBLE CONDUIT
STRD
STRANDED
O
TERMINAL LOCATED IN CONTROL PANEL
SW
SWITCH
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STARTER OR CONTACTOR COIL
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THERMOSTAT
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SWBD
SWITCHBOARD
❑
TERMINAL LOCATED IN MOTOR CONTROL CENTER
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SWGR
SWITCHGEAR
❑
PANEL
3
CONDUIT -TURNED DOWN
H 0 A
❑
TERMINAL LOCATED IN CENTRAL PANEL
NORTH
INCOMING LINE CONNECTION
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HAND -OFF -AUTOMATIC
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TB
TERMINAL BOARD
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FRACTIONAL H.P. MOTOR
m
TERMINAL LOCATED IN LOCAL JUNCTION BOX
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TELEPHONE
TEMPERATURE SWITCH
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STRESS CONE CONNECTION
DEVICE LOCATED IN PANEL
GROUNDING PLAN SYMBOLS
TS
0-0
LIGHT STANDARD MOUNTED ON POLE
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PULL BOX,DEVICE BOX,SOLENOID
♦
DEVICE LOCATED IN FIELD
VALVE, LIMIT SWITCH, ETC.
O
POWER FEEDER (CONDUIT AND CABLE)
-- G -- UNDERGROUND GROUND CABLE
UNG
UNDERGROUND
UH
UNIT HEATER
❑
JUNCTION BOX
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DEVICE LOCATED IN MCC
G EXPOSED GROUND CABLE
V
VOLTS
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HORN
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HORSEPOWER
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WATTS
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WEATHER PROOF
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WELDING RECEPTACLE
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TRANSFORMER
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BUZZER
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2E1362
04 Mar 2021
I
HIPP ENGINEERING
& CONSULTING, INC.
2301 REXWOODS DRIVE, SUITE 200
RALEIGH, NC 27607
TEL:[phone] FAX:[phone]
NC FIRM LICENSE NUMBER: C-2146
WWW.HIPP-USA.COM

1.0 GENERAL:
1.1 REVIEW THE CONTRACT DOCUMENTS AND C❑❑RDINATE ALL WORK WITH ALL OTHER TRADES AS NECESSARY TO
PR❑VIDE EQUIPMENT MANUFACTURER'S RECOMMENDED CLEARANCES TO PR❑VIDE EQUIPMENT ❑PERATI❑N SUCH
THAT IT IS NOT DETRIMENTAL TO OTHER EQUIPMENT AND TO AVOID CONFLICTS AND INTERFERENCE.
1.2 C❑❑RDINATE ALL CONNECTION, PR❑TECTI❑N, AND BRANCH CIRCUITING WITH OTHER TRADES TO CORRESPOND
WITH REQUIREMENTS OF EQUIPMENT PROVIDED BY THE OWNER AS WELL AS OTHER TRADES.
1.3 L❑CATIONS INDICATED FOR ALL DEVICES AND EQUIPMENT ARE APPROXIMATE AND SHALL BE FIELD VERIFIED
AND COORDINATED WITH THE OWNER'S REPRESENTATIVE AND OTHER TRADES, THE DRAWINGS ARE DIAGRAMMATIC
AND ARE NOT INTENDED TO INCLUDE EVERY DETAIL OF C❑NSTRUCTI❑N, MATERIALS, CIRCUITRY, EQUIPMENT, OR
EXACT ROUTING ❑F CIRCUITRY, TAKE ACTUAL FIELD MEASUREMENTS AT THE JOB SITE IN LIEU OF SCALING
THE DRAWINGS.
1.4 MAINTAIN A CLEAN MARK-UP SET OF DRAWINGS, SHOWING AS -BUILT C❑NDITI❑NS, ALL CHANGES OR
CLARIFICATIONS TO THE INSTALLATION MADE IN THE FIELD SHALL BE REFLECTED ON A SINGLE MASTER SET
WITHIN 48 HOURS OF MAKING ANY CHANGES FROM THE C❑NSTRUCTI❑N DOCUMENTS. THIS MASTER SET WILL BE
PROFESSIONALLY MAINTAINED AND BE AVAILABLE FOR PERI❑DIC REVIEW, TURN IN THIS MASTER SET AT
THE END OF C❑NSTRUCTI❑N,
1.5 REPORT ALL CONFLICTS WITHIN THE CONTRACT DOCUMENTS OR WITH EXISTING C❑NDITI❑NS IN THE FIELD TO
THE ENGINEER AS SOON AS POSSIBLE TO DETERMINE THE BEST CORRECTIVE ACTION. SUBMIT PHOTOGRAPHS
AND/OR SKETCHES TO CLARIFY C❑NDITI❑NS UPON REQUEST,
1.6 INSTALLATION SHALL COMPLY WITH ALL LAWS APPLYING TO ELECTRICAL INSTALLATION. THE WORK SHALL BE
IN ACCORDANCE WITH THE LATEST EDITION OF THE F❑LL❑WING CODES AND ALL LOCAL GOVERNING CODES AND
ORDINANCES AND WITH THE REGULATIONS OF THE SERVING UTILITY COMPANY AS A MINIMUM:
A. NFPA 70 - NATI❑NAL ELECTRICAL CODE
B. NFPA 72 - NATIONAL FIRE ALARM CODE
C. NFPA 101 - LIFE SAFETY CODE
D. NORTH CAR❑LINA BUILDING AND FIRE CODES
1.7 WHERE REQUIREMENTS OF THE CONTRACT DOCUMENTS ARE IN EXCESS OF THE ABOVE CODE REQUIREMENTS,
THE CONTRACT DOCUMENTS SHALL GOVERN,
1.8 THE CONTRACTOR IS RESPONSIBLE FOR OBTAINING ALL PERMITS ASSOCIATED WITH THE WORK DEFINED IN
THE CONTRACT DOCUMENTS. PROVIDE ALL REQUIRED PERMITS IN A TIMELY FASHION TO ENSURE NO NEGATIVE
IMPACT ON THE C❑NSTRUCTI❑N SCHEDULE.
1.9 SHOP DRAWINGS: PR❑VIDE SPECIFIC INFORMATION RELATING TO PR❑VIDED MATERIALS FOR THIS PROJECT,
INCLUDE MANUFACTURER'S STANDARD CATALOG DATA, INSTALLATION INSTRUCTIONS AND RECOMMENDATIONS,
DRAWINGS, CERTIFICATIONS AND OTHER DETAILED INFORMATION DESCRIBING THE MATERIAL AND PRODUCT
SPECIFIED. ALL MATERIALS MUST MEET ENGINEER OR OWNER APPROVAL PRIOR TO PURCHASE.
1.10 WORKING CLEARANCES AROUND EQUIPMENT REQUIRING ELECTRICAL SERVICE SHALL COMPLY WITH NATI❑NAL
ELECTRICAL CODE REQUIREMENTS.
1.11 ALL MATERIALS AND EQUIPMENT SHALL BE NEW AND SHALL BE LISTED BY THE UNDERWRITER'S
LAB❑RAT❑RIES, INC., FOR THE USE INTENDED WHEN A STANDARD FOR SUCH MATERIAL AND USE EXISTS.
1.12 ALL PRODUCTS AND MATERIALS SHALL COMPLY WITH ALL APPLICABLE STANDARDS AND PUBLICATIONS OF
NEMA, ANSI, ASTM, IEEE, AEIC, ICEA OR OTHER PUBLICATIONS REFERENCED,
1.13 ALL EQUIPMENT OF A PARTICULAR KIND SUCH AS WIRING DEVICES AND PANELB❑ARDS, SHALL BE THE
PRODUCT OF THE SAME MANUFACTURER,
1.14 INSTALL MATERIALS AND EQUIPMENT IN ACCORDANCE WITH MANUFACTURER'S INSTRUCTIONS AND
RECOMMENDATIONS. CARE SHALL BE USED IN THE ERECTION OF EQUIPMENT AND MATERIAL TO AV❑ID CAUSING
DAMAGE. REPAIR OF DAMAGED EQUIPMENT INCLUDING MATERIALS INSTALLED BY OTHER TRADES SHALL BE
MADE AT NO ADDITI❑NAL EXPENSE TO THE OWNER,
1.15 IT SHALL BE THE RESP❑NSIBILITY OF THE ELECTRICAL CONTRACTOR TO NOTIFY THE CODE ENFORCING
AUTHORITIES AND TO SCHEDULE ALL REQUIRED INSPECTIONS WITH THE STATE, COUNTY & CITY OFFICIALS
(WHERE APPLICABLE), AND LOCAL AUTHORITY HAVING JURISDICTION,
1.16 PR❑VIDE ALL WORK, EQUIPMENT, SERVICES, LABOR, AND MATERIALS FOR THE INSTALLATION OF COMPLETE
AND FUNCTI❑NAL ELECTRICAL SYSTEMS AS DESCRIBED OR IMPLIED BY THE CONTRACT D❑CUMENTS,
1.17 WHERE SUBSTITUTION OF OTHER THAN SPECIFIED EQUIPMENT IS MADE AND SUCH CHANGE REQUIRES CHANGES
IN THE ELECTRICAL POWER SUPPLY (WIRE, C❑NDUIT, CIRCUIT BREAKERS, STARTERS, ETC.), THE CONTRACTOR
INSTALLING THE SUBSTITUTED EQUIPMENT SHALL INCLUDE IN HIS BID THE ADDED COST FOR THE ELECTRICAL
CHANGES REQUIRED.
1.18 PR❑VIDE ALL CUTTING AND PATCHING NECESSARY FOR THE PROPER INSTALLATION OF ALL WORK AND TO
REPAIR ANY DAMAGE D❑NE,
1.19 PR❑VIDE NEMA 1 ENCLOSURES FOR INTERIOR LOCATIONS AND NEMA 3R ENCLOSURES FOR EXTERIOR LOCATIONS
UNLESS NOTED OTHERWISE.
1.20 WARRANT ALL MATERIALS, EQUIPMENT, AND W❑RKMANSHIP SHOWN OR IMPLIED BY THESE DOCUMENTS To BE
FREE OF DEFECTS FOR A PERIOD OF ONE YEAR FROM THE TIME OF ACCEPTANCE BY THE OWNER. IF WITHIN
THE FIRST YEAR AFTER THE OWNER'S ACCEPTANCE DATE ANY WORK OR EQUIPMENT IS FOUND To BE
DEFECTIVE, CORRECT IT PROMPTLY AT NO COST TO THE OWNER,
1.21 AN ELECTRICAL INSPECTION CERTIFICATE SHALL BE ISSUED BY THE INSPECTION AUTHORITIES HAVING
JURISDICTION BEFORE WORK WILL BE APPROVED FOR FINAL PAYMENT.
1.22 ALL WORK AND MATERIALS IN ELECTRICALLY HAZARDOUS AREAS SHALL BE IN ACCORDANCE WITH NEC
ARTICLE 500.
2.0 DEM❑LITI❑N:
2.1 DISC❑NNECT ELECTRICAL SYSTEMS IN WALLS, FLOORS, AND CEILINGS TO BE REMOVED.
2.2 C❑❑RDINATE UTILITY SERVICE OUTAGES WITH UTILITY COMPANY.
2.3 PR❑VIDE TEMPORARY WIRING AND CONNECTIONS TO MAINTAIN EXISTING SYSTEMS IN SERVICE DURING
C❑NSTRUCTI❑N. WHEN WORK MUST BE PERFORMED ON ENERGIZED EQUIPMENT OR CIRCUITS, USE PERSONNEL
EXPERIENCED IN SUCH ❑PERATI❑NS,
2,4 EXISTING ELECTRICAL SERVICE: MAINTAIN EXISTING SYSTEM IN SERVICE UNTIL NEW SYSTEM IS COMPLETE
AND READY FOR SERVICE, DISABLE SYSTEM ONLY TO MAKE SWITCH❑VERS AND C❑NNECTI❑NS, COORDINATE
OUTAGES WITH THE OWNER TO MINIMIZE OUTAGE DURATION,
3.0 EXTENSION OF EXISTING ELECTRICAL WORK:
3.1 REMOVE, RELOCATE, AND EXTEND EXISTING INSTALLATIONS TO ACCOMMODATE NEW CONSTRUCTION.
3.2 REMOVE ABANDONED WIRING TO SOURCE OF SUPPLY.
3.3 REMOVE EXPOSED ABANDONED CONDUIT, INCLUDING ABANDONED C❑NDUIT ABOVE ACCESSIBLE CEILING
FINISHES. CUT CONDUIT FLUSH WITH WALLS AND FLOORS, AND PATCH SURFACES.
3.4 DISC❑NNECT ABANDONED OUTLETS AND REMOVE DEVICES, REMOVE ABANDONED OUTLETS IF C❑NDUIT
SERVICING THEM IS ABANDONED AND REMOVED. PR❑VIDE BLANK COVER FOR ABANDONED OUTLETS WHICH
ARE NOT REMOVED.
3.5 DISC❑NNECT AND REMOVE ABANDONED PANELB❑ARDS AND DISTRIBUTION EQUIPMENT.
3.6 DISC❑NNECT AND REMOVE ELECTRICAL DEVICES AND EQUIPMENT SERVING UTILIZATION EQUIPMENT THAT HAS
BEEN REMOVED,
3.7 DISC❑NNECT AND REMOVE ABANDONED LUMINAIRES. REMOVE BRACKETS, STEMS, HANGERS, AND OTHER
ACCESS❑RIES.
3.8 REPAIR ADJACENT CONSTRUCTION AND FINISHES DAMAGED DURING DEM❑LITI❑N AND EXTENSION WORK,
3.9 MAINTAIN ACCESS TO EXISTING ELECTRICAL INSTALLATION WHICH REMAIN ACTIVE, MODIFY INSTALLATION
OR PROVIDE ACCESS PANEL AS APPR❑PRIATE.
3.10 EXTEND EXISTING INSTALLATIONS USING MATERIALS AND METHODS COMPATIBLE WITH EXISTING ELECTRICAL
INSTALLATIONS, OR AS SPECIFIED.
3.11 RELAMP ALL EXISTING LIGHT FIXTURES IN THE AREAS BEING RENOVATED WITH LAMPS THAT MATCH THE
EXISTING TYPE,
4.0 WIRING:
4.1 CONDUCTORS, NOT INSTALLED IN CABLE TRAYS, SHALL BE COPPER, 600V, THHN/THWN, STRANDED. MINIMUM
POWER CONDUCTOR SIZE SHALL BE #12 AWG. MINIMUM CONTROL CIRCUIT CONDUCTOR SIZE SHALL BE #14
AWG, STRANDED, ALL 208/120 VAC CONDUCTORS SHALL BE COLOR -CODED BLACK, RED, BLUE, WHITE, AND
GREEN FOR PHASES A, B, C, NEUTRAL, AND GROUND RESPECTIVELY, ALL 480/277VAC CONDUCTORS SHALL
BE COLOR -CODED BROWN, ORANGE, YELLOW, GRAY, AND GREEN FOR PHASE A, B, C, NEUTRAL, AND GROUND,
RESPECTIVELY.
4.2 SPLICING SHALL BE ACCOMPLISHED WITH "APPROVED" WIRE NUTS ON S❑LID AND STRANDED CONDUCTORS,
4.3 VERIFY THAT THE ELECTRICAL CHARACTERISTICS, SUCH AS VOLTAGE, PHASE/WIRE AND OVERCURRENT
PR❑TECTI❑N, OF THE CIRCUITS ARE CORRECT PRIOR TO ENERGIZING ANY EQUIPMENT. PR❑VIDE CONDUCTORS
AND CIRCUIT BREAKER SIZES AS NECESSARY TO MEET THE NAMEPLATE AND MANUFACTURER LISTED
REQUIREMENTS OF THE ACTUAL EQUIPMENT SUPPLIED TO THE JOB.
4.4 FULLY C❑❑RDINATE WITH THE OTHER TRADES TO DETERMINE THE POWER REQUIREMENTS AND C❑NNECTI❑N
PINTS FOR EQUIPMENT FURNISHED BY OTHERS, PR❑VIDE ELECTRICAL POWER WIRING AND ❑VERCURRENT
PR❑TECTI❑N TO EACH PIECE OF EQUIPMENT BASED UPON THE MANUFACTURER'S WIRING DIAGRAMS AND UNIT
MOUNTED NAMEPLATES,
4.5 ALL FEEDERS AND CIRCUITRY SHALL BE TORQUED PER THE PANEL, BREAKER, TERMINAL C❑NNECTI❑N, AND/❑R
PARTICULAR EQUIPMENT MANUFACTURER'S PUBLISHED SPECIFICATIONS,
4.6 GROUND CONDUCTORS SHALL BE PR❑VIDED WITH ALL FEEDERS AND BRANCH CIRCUITS, USING ELECTRICAL
CONDUIT AS GROUND CONDUCTOR IS NOT ACCEPTABLE.
4.7 CABLE INSTALLED IN CABLE TRAYS SHALL BE UL LISTED NEC TYPE TC, RATED 600V, COMPOSED OF
STRANDED COPPER PHASE CONDUCTORS AND A STRANDED COPPER GROUND CONDUCTOR (FOR MULTI -CONDUCTOR
CABLES). CONDUCTOR INSULATION SHALL BE 90C XHHW WITH A SUNLIGHT RESISTANT PVC JACKET, CABLE
SHALL BE SUITABLE FOR DIRECT BURIAL AND WET LOCATIONS.
4.8 FOR GROUND CONDUCTORS, INSTALL S❑LID CONDUCTORS FOR NO. 8 AWG AND SMALLER, AND STRANDED FOR
NO. 6 AWG AND LARGER UNLESS ❑THERWISE INDICATED.
5.0 RACEWAY:
5.1 EXCEPT AS NOTED BELOW, ALL CONDUITS SHALL BE 3/4" MINIMUM SIZE, AC OR MC CABLE MAY BE USED IN
LIEU OF CONDUIT WHERE PERMITTED BY NEC,
5.2 TERMINATE ALL RGS OR IMC C❑NDUITS ENTERING ENCLOSURES WITH A FIBER BUSHING OR BOND BUSHING
(WHERE THE NEC REQUIRES IT), INSULATING THROATS SHALL BE MANUFACTURED WITH THE CONNECTORS; USE
OF INSULATING SLEEVES IS NOT ALLOWED,
5.3 FLEXIBLE CONDUIT CONNECTORS SHALL BE T & B NYLON INSULATED "TITE-BITE" OR APPROVED EQUAL.
5.4 LIQUID -TIGHT FLEXIBLE C❑NDUIT SHALL BE USED FOR FINAL EQUIPMENT CONNECTIONS, AND IN DAMP
L❑CATIONS.
5.5 SECURE C❑NDUITS USING MANUFACTURED, GALVANIZED STRAPS, TIE WIRE IS NOT ALL❑WED,
5.6 EXCEPT FOR MECHANICAL EQUIPMENT, INDUSTRIAL, AND OPEN CEILING AREAS, ROUTE ALL C❑NDUIT CONCEALED
ABOVE CEILING OR IN WALL. ROUTE ALL C❑NDUITS PARALLEL OR PERPENDICULAR TO STRUCTURAL ELEMENTS
AND IN GROUPS, WHEN INSTALLED AT THE ROOF OR CEILING, GROUPINGS SHALL BE SINGLE DEPTH AND TIGHT
AGAINST THE STRUCTURE, FOR MULTIPLE DEPTH GROUPINGS AND OTHER SITUATIONS, A TRAPEZE ARRANGEMENT
USING APPR❑PRIATE CHANNELS SUSPENDED FROM THE STRUCTURE USING THREADED RODS OF SUFFICIENT
SUPPORTING STRENGTH WILL BE PERMITTED. WHERE A TRAPEZE ARRANGEMENT IS INSTALLED FOR C❑NDUIT A
MINIMUM OF 25% SPACE SHALL BE PR❑VIDED FOR FUTURE C❑NDUIT INSTALLATION. KEEP A MINIMUM OF SIX
(6) INCHES AWAY FROM ANY PARALLEL RUNS OF STEAM OR HOT WATER PIPES AND FLUES, AND 18" FROM
NEAREST SPRINKLER HEAD,
5.7 PROVIDE 100-POUND TEST, NYLON PULL CORDS IN ALL EMPTY C❑NDUITS, CONDUITS STUBBED AND BUSHED
ABOVE FINISHED CEILINGS OR AT STRUCTURE FROM FLOOR BOXES , TELECOMMUNICATION PANELS, OR OTHER
EQUIPMENT SHALL BE LABELED. THE LABEL SHALL INDICATE THE BOX, PANEL, OR EQUIPMENT FROM WHICH
THE C❑NDUIT ORIGINATES, AND SHALL BE MARKED WITH INDELIBLE INK ON THE C❑NDUIT.
5.8 SEAL ALL C❑NDUIT PENETRATIONS THROUGH FIRE -RATED WALLS OR FLOORS WITH IMPERVI❑US,
NON-COMBUSTIBLE MATERIALS WITH UL LISTED SYSTEM AND IN SUCH MANNER THAT THE ORIGINAL FIRE
RATING IS RESTORED, CONDUITS PENETRATING BLOCK WALLS SHALL BE SLEEVED AND THEN SEALED, IT IS
THE CONTRACTOR'S RESP❑NSIBILITY TO CONFIRM WALL, FLOOR, CEILING AND ROOF RATINGS WITH THE OWNER.
ALSO SEAL ALL WALL AND FLOOR PENETRATIONS LEFT BEHIND ONCE THE C❑NDUIT TO BE DEMOLISHED HAS
BEEN REMOVED.
5.9 ALL OUTLET BOXES SHALL BE GALVANIZED STEEL EXCEPT THAT CAST BOXES WITH GASKETED COVERS SHALL
BE REQUIRED IN ALL INTERIOR WET AREAS AND ON THE EXTERIOR OF THE BUILDING. OUTLET BOXES SHALL
BE NO LESS THAN 4" SQUARE BY 1-1/2" DEEP UNLESS NOTED ❑THERWISE, MULTIGANG BOXES SHALL BE ❑F
SINGLE PIECE CONSTRUCTION.
5.10PULL BOXES SHALL BE CONSTRUCTED OF CODE GAUGE GALVANIZED SHEET METAL AND SHALL COMPLY WITH
NEC, MARK ALL JUNCTION AND PULL BOXES WITH PANEL AND CIRCUIT NUMBERS.
5.11 C❑NDUIT ROUTING SHOWN ON THE DRAWINGS IS SCHEMATIC, CONTRACTOR TO C❑❑RDINATE INSTALLATION WITH
OTHER TRADES.
5.12 CONCEALED C❑NDUIT ROUTED BEHIND FINISHED WALLS OR CEILINGS IN OFFICE AREAS MAY BE ZINC -COATED
EMT, 3/4" MINIMUM SIZE. EMT FITTINGS SHALL BE STEEL COMPRESSION TYPE, EMT CONNECTORS SHALL HAVE
INSULATED THROATS. ALL OTHER C❑NDUIT SHALL BE RGS.
6.0 DEVICES:
6.1 ALL WIRING DEVICES SHALL BE SPECIFICATION GRADE. THE COLOR SHALL BE WHITE,
6.2 SWITCHES FOR 120/277V LINE VOLTAGE LIGHT CONTROLS SHALL BE QUIET ❑PERATING TYPES RATED
20A-120/277 VAC.
6.3 RECEPTACLES SHALL BE NEMA 5-20R TYPES UNLESS OTHERWISE NOTED. SPECIAL PURPOSE RECEPTACLES
SHALL BE HEAVY DUTY, SPECIFICATION GRADE TYPES, C❑❑RDINATE EACH DEVICE FOR THE CIRCUIT AND
EQUIPMENT TO WHICH IT WILL BE CONNECTED, PROVIDE THE PROPER DEVICE BASED UPON THE ACTUAL
EQUIPMENT SUPPLIED TO THE PROJECT.
6.4 PR❑VIDE A SINGLE MULTI -GANG BOX AND DEVICE PLATE FOR ALL GROUP MOUNTED WIRING DEVICES.
PR❑VIDE FULL HEIGHT AND DEPTH BARRIERS IN OUTLET BOXES WHERE POWER AND COMMUNICATION
CONDUCTORS WOULD BE MIXED,
6.5 ALL COVER PLATES SHALL BE GRAY, OR "302" STAINLESS STEEL AS APPROVED BY OWNER REPRESENTATIVE.
7.0 POWER EQUIPMENT:
7.1 SAFETY SWITCHES SHALL BE HEAVY DUTY, QUICK -MAKE QUICK -BREAK TYPE OF THE SIZE AND FUSE
AMPACITY AS NOTED ON THE DRAWINGS. PR❑VIDE GROUND BUS, S❑LID NEUTRAL (WHEN REQUIRED), BUSSMAN
FRS-R CLASS RK-5 DUAL ELEMENT TIME DELAY FUSES, REJECTION TYPE FUSE HOLDERS, AND NEMA RATED
ENCLOSURE, PROVIDE ONE N.O. AND ONE N.C, AUXILIARY CONTACT PER SWITCH,
7.2 ALL LUGS AND TERMINALS FOR POWER CONDUCTORS, AND POWER EQUIPMENT (SUCH AS TRANSFORMERS,
PANELS, CIRCUIT BREAKERS, DISCONNECTS, SWITCHES, STARTERS, AND DEVICES) SHALL BE RATED FOR 75
DEGREES C CONDUCTORS.
7.3 ALL ELECTRICAL EQUIPMENT SHALL BE SQUARE D, OR AS APPROVED BY THE OWNER, UNLESS ❑THERWISE
NOTED.
8.0 OTHER REQUIREMENTS:
8.1 PR❑VIDE ENGRAVED, PHENOLIC NAMEPLATES, WHITE LETTERS ON BLACK BACKGROUND (208 VAC), (480 VAC),
AND (60OV) FOR EACH PANELB❑ARD, TRANSFORMER, STARTER, WIRING TROUGH, AND DISCONNECT SWITCH.
NAMEPLATES SHALL INDICATE NAME OF EQUIPMENT, VOLTAGE AND PHASE, AND SOURCE FROM WHICH
EQUIPMENT IS POWERED, NAMEPLATE SHALL BE PERMANENTLY ATTACHED TO THE EQUIPMENT,
8.2 ALL RECEPTACLES, LIGHT SWITCHES, JUNCTION BOXES, AND FIXED EQUIPMENT SHALL HAVE A PERMANENT
LABEL INDICATING PANEL AND CIRCUIT NUMBER, LABEL SHALL BE CLEAR WITH MINIMUM 1/8" HIGH BLACK
TEXT ON A LAMINATED ADHESIVE BACKED HEAT AND SCRATCH RESISTANT TAPE. PRINT METHOD SHALL BE
THERMAL TRANSFER TYPE.
8.3 FURNISH AND INSTALL GALVANIZED STEEL SUPPORTS, FASTENERS, MOUNTS, HANGERS, SIDE BRACES, ETC„
WHICH MAY BE REQUIRED TO SECURELY ANCHOR AND SUPPORT ELECTRICAL EQUIPMENT,
8.4 CONTRACTOR SHALL UPDATE EXISTING PANEL SCHEDULES IN A MANNER ACCEPTABLE TO THE OWNER.
9.0 CLEANING, REPAIR, AND TESTING:
9.1 CLEAN, REPAIR, AND TEST EXISTING MATERIALS AND EQUIPMENT WHICH REMAIN OR ARE To BE REUSED.
TESTING SHALL BE COMPLETED BY QUALIFIED PERSONS,
9.2 SWITCHB❑ARDS AND PANELB❑ARDS: CLEAN EXPOSED SURFACES AND CHECK TIGHTNESS OF ELECTRICAL
C❑NNECTI❑NS, REPLACE DAMAGED CIRCUIT BREAKERS AND PR❑VIDE CLOSURE PLATES FOR VACANT
POSITIONS. PR❑VIDE TYPED CIRCUIT DIRECTORY SH❑WING REVISED CIRCUITING ARRANGEMENTS.
9.3 MOTOR CONTROL CENTERS: CLEAN EXPOSED SURFACES AND CHECK TIGHTNESS OF ELECTRICAL CONNECTIONS.
CHECK AND REPLACE DAMAGED STARTER COMPONENTS. REPLACE DAMAGED OR NON-FUNCTI❑NING COMPONENTS,
CHECK AND REPLACE STARTER OVERLOAD HEATER ELEMENTS FOR THE MOTOR FULL LOAD CURRENT.
9.4 TEST ALL DE -ENERGIZED WIRING FOR CONTINUITY, TEST ALL 600V AND 240V POWER CIRCUITS
PHASE -TO -PHASE AND PHASE -TO -GROUND WITH A 1000V MEGGER TO VERIFY INSULATION INTEGRITY,
10.0 ELECTRICAL FREEZE PROTECTION:
PART 1 - GENERAL
10.11 SUMMARY
A. WORK INCLUDES: DESIGN, FURNISH AND INSTALL FREEZE PR❑TECTI❑N SYSTEMS FOR INSULATED PIPES AS SHOWN ON THE PROJECT
PIPING AND INSTRUMENTATION DIAGRAMS. THE WORK SHALL INCLUDE, BUT NOT BE LIMITED TO:
1. DESIGN OF THE FREEZE PR❑TECTI❑N SYSTEM,
2. FURNISHING ALL MATERIALS, EQUIPMENT, COMPONENTS AND ANCILLARY ITEMS NECESSARY FOR COMPLETE INSTALLATION OF THE
WORK, TO INCLUDE, BUT NOT LIMITED TO, ELECTRICAL HEAT TRACING SYSTEMS AND COMPONENTS, HEAT TRACE CABLES, AMBIENT
SENSING THERMOSTATS, CIRCUIT BREAKERS, ALARM AND INDICATION, AND ANY OTHER ASSOCIATED WIRING, COMPONENTS AND
ACCESS❑RIES,
3. SYSTEM START-UP/TESTING,
4. SYSTEM DOCUMENTATION, AND
5. TRAINING OF OWNER PERSONNEL,
B. WORK NOT INCLUDED: IMPEDANCE AND INDUCTANCE HEATING SYSTEMS.
10.12 DESIGN REQUIREMENTS
A. PR❑VIDE FREEZE PR❑TECTI❑N FOR LIQUID LINES, AND/OR TO PR❑VIDE SUFFICIENT HEAT TO MAINTAIN THE TEMPERATURE OF PROCESS
PIPES AND VESSELS WITHIN A SPECIFIED TEMPERATURE RANGE ABOVE THE NORMAL FREEZE TEMPERATURE (32°F), NO LINES IN THIS
CONTRACT REQUIRE PROCESS HEAT TRACING,
B. ELECTRIC HEAT TRACE SHALL NOT BE USED ON PIPING/EQUIPMENT REQUIRING MORE THAN 20 WATTS PER LINEAR FOOT, UNLESS
JUSTIFIED BY LIFE-CYCLE-C❑STS,
C. THE DESIGN AND CONTROL OF AN ELECTRICAL HEAT TRACE SYSTEM SHALL PROVIDE FOR MAXIMUM ENERGY CONSERVATION.
D. FREEZE PR❑TECTI❑N:
1. FREEZE PR❑TECTI❑N SYSTEMS TO BE TURNED ON AND OFF VIA AN(A) AMBIENT AIR SENSING THERM❑STAT(S). AMBIENT THERMOSTAT
SETTINGS SHALL BE 40°F. FREEZE PR❑TECTI❑N SYSTEM SHALL BE DESIGNED SUCH THAT THE AMBIENT SENSING THERMOSTAT
CONTACTS DIRECTLY ENERGIZE THE HEAT TRACE CABLE,
2, LOCAL INDICATION OF POWER FAILURE SHALL BE PROVIDED,
E. THERMAL DESIGN:
1. HEAT LOSS CALCULATIONS SHALL BE IN CONFORMANCE WITH IEEE 515,
2. A MINIMUM 10% DESIGN MARGIN SHALL BE APPLIED TO ALL FINAL HEAT LOSS CALCULATIONS.
3. THE CONDITIONS USED IN HEAT LOSS CALCULATIONS ARE AS FOLLOWS:
MINIMUM MAINTAIN TEMPERATURE: 40F
MINIMUM AMBIENT TEMPERATURE = 0°F
MAXIMUM WIND SPEED = 20 MPH
10.13 SUBMITTALS
A. CONTRACTOR SHALL SUBMIT THE F❑LL❑WING WITH THE BID PROPOSAL:
1. DETAILED MANUFACTURERS LITERATURE COVERING THE CONSTRUCTION DETAILS, ❑PERATING CHARACTERISTICS, AND PERTINENT
RATINGS OF ALL OF THE QUOTED PRODUCTS, COMPONENTS AND ACCESS❑RIES.
2, COMPLETE INSTALLATION DETAIL DRAWINGS AND WRITTEN INSTALLATION INSTRUCTIONS.
3. ANY EXCEPTIONS TO THE CONTRACT DOCUMENTS,
B. CONTRACTOR SHALL SUBMIT THE FOLLOWING AT LEAST TEN WORKING DAYS PRIOR TO START OF WORK:
HEAT TRACE IS❑METRICS AND HEAT TRACE ELECTRIC SCHEMATIC DRAWINGS. THESE DRAWINGS SHALL INCLUDE ELECTRICAL RATINGS FOR EACH
SPECIFIC HEAT TRACE RUN (WATTS/FOOT, VOLTAGE, CATALOG NUMBER, ETC,). THE LENGTH OF EACH HEAT TRACE CIRCUIT/RUN
SHALL BE INDICATED ON THE IS❑METRIC DRAWINGS.
10.14 QUALITY ASSURANCE
A. CODES AND STANDARDS
ALL MATERIALS, W❑RKMANSHIP, DESIGN AND INSTALLATION DESCRIBED HEREIN MUST COMPLY WITH THE LATEST EDITIONS AND
ADDENDA OF THE CODES AND STANDARDS LISTED BELOW, INCLUDING ALL APPLICABLE FEDERAL, STATE AND LOCAL CODES,
ANSI AMERICAN NATI❑NAL STANDARDS INSTITUTE
FM FACTORY MUTUAL
IEEE NASI/IEEE 515, INSTITUTE OF ELECTRICAL AND ELECTRONIC ENGINEERS
NEC NATIONAL ELECTRICAL CODE
NEMA NATI❑NAL ELECTRICAL MANUFACTURERS ASS❑CIATI❑N
NFPA NATI❑NAL FIRE PR❑TECTI❑N ASS❑CIATI❑N
UL UNDERWRITERS LABORATORIES
B. UL/FM LISTING: ALL HEATING CABLES, COMPONENTS AND ACCESS❑RIES SHALL BE UL/FM LISTED FOR THE ELECTRICAL CLASSIFICATION
FOR THE SPECIFIC INSTALLATION.
C. ALL HEAT TRACE MATERIALS, COMPONENTS, AND ACCESS❑RIES SHALL BE NEW, UNUSED, UNDAMAGED, CURRENT DESIGN AND OF A
GRADE AND QUALITY SPECIFIED IN THE MANUFACTURERS LITERATURE.
PART 2 - PRODUCTS
10.21 MANUFACTURERS AND MATERIALS
ALL PRODUCTS SHALL BE AS MANUFACTURED BY RAYCHEM. THE MATERIALS, EQUIPMENT, AND COMPONENTS
SUPPLIED SHALL BE IN STRICT CONFORMANCE TO THIS SPECIFICATION.
10.22 FREEZE PROTECTION
A. THE HEATING CABLE SHALL BE C❑NTINU❑US EXPOSURE WITH MAINTAIN CAPABILITY UP TO 150°F (65°C) AND MAXIMUM EXPOSURE
CAPABILITY UP TO 185°F (85°C).
B. THE HEATING CABLE SHALL BE A SELF-REGULATING AND CONSIST OF A SEMI -CONDUCTIVE CORE EXTRUDED OVER AND BETWEEN 2
PARALLEL COPPER 16 GAUGE (MINIMUM) NICKEL -PLATED BUS WIRES, THE HEATING CABLE WILL VARY ITS POWER OUTPUT (WATTS/FOOT)
INVERSELY WITH PIPE TEMPERATURE AT EVERY PINT ALONG ITS ENTIRE LENGTH SUCH THAT POWER (HEAT OUTPUT) IS REDUCED AS
PIPE TEMPERATURE INCREASES.
C. THE HEATING CABLE SHALL HAVE A MODIFIED P❑LYOLEFIN JACKET EXTRUDED OVER THE SEMI -CONDUCTIVE CORE TO EFFECTIVELY OVER
SEAL THE CORE MATERIAL. A C❑NTINU❑US TINNED-C❑PPER BRAID SHALL BE INSTALLED OVER THE JACKETS. THIS METAL JACKET SHALL
THEN BE COVERED WITH A FLU❑R❑P❑LYMER OVER JACKET,
D. THIS HEATING CABLE SHALL HAVE A MAXIMUM UNCONDITIONAL TEMPERATURE RATING ❑F 185°F OR LESS.
10.23 SYSTEM COMPONENTS
THERMOSTATS, FITTINGS, HEAT TRACE, COMPONENTS AND ACCESS❑RIES SHALL BE LISTED FOR NEMA 12, 4, 4X, 7 OR 9 AS REQUIRED.
PART 3 - EXECUTION
10.31 INSTALLATION
A. THE ELECTRIC HEATING CABLE SHALL BE DESIGNED TO BE CUT TO LENGTH IN THE FIELD WITHOUT EFFECTING POWER OUTPUT PER UNIT
LENGTH, AND TO SATISFY INSTALLATION CONDITIONS AND MAINTAIN A CONTINUOUS HEATING CIRCUIT,
B. THE HEATING CABLE SHALL OPERATE AT NOMINAL SUPPLY VOLTAGE AS INDICATED ON THE DRAWINGS.
C. HEAT TRACE SHALL BE INSTALLED LINEARLY ON THE BOTTOM HALF OF THE PIPE, SPIRAL WRAPPING IS NOT PERMITTED.
D. SELF REGULATING HEAT TRACE SHALL BE SECURED TO THE PIPE PER MANUFACTURER'S RECOMMENDATIONS.
E. GROUND FAULT PR❑TECTI❑N (30MA) IS REQUIRED FOR ALL HEAT TRACING CIRCUITS, REFER TO THE DRAWINGS FOR POWER SUPPLY
L❑CATION,
F. EACH HEAT TRACE CIRCUIT/RUN SHALL BE FITTED WITH THE SPECIFIC C❑NNECTI❑N/TERMINATION KIT AND ACCESS❑RIES SPECIFIED BY
THE MANUFACTURER, ALL COMPONENTS SHALL BE PART OF THE UL/FM SYSTEM APPROVAL FOR THE SPECIFICALLY DESIGNATED AREA
CLASSIFICATION.
G. ALL CONNECTIONS/TERMINATIONS SHALL BE EFFECTIVELY AND PERMANENTLY WATERPROOFED.
H. HEAT TRACE SHALL BE INSTALLED TO ALLOW EASY REMOVAL OF EQUIPMENT REQUIRING PERI❑DIC MAINTENANCE, SUCH AS VALVES,
PUMPS, STRAINERS, FILTERS, ETC,
I. ADHESIVE MYLAR SIGNS SHALL BE PLACED EVERY 10 FEET ON ALTERNATING SIDES AND APPLIED TO THE OUTSIDE SURFACE OF THE
INSULATED PIPE. THESE SIGNS SHALL STATE THAT THE LINE IS ELECTRICALLY TRACED.
J. AT NO TIME SHALL THE HEATING CABLE EXIT THE THERMAL INSULATION SYSTEM AND BE EXPOSED WITHOUT PR❑TECTI❑N FROM
MECHANICAL DAMAGE OR ABUSE,
10.32 THERMAL INSULATION
A. ALL HEAT TRACED PIPE LINES AND EQUIPMENT SHALL BE INSTALLED WITH A DRY THERMAL INSULATION WITH A WEATHER BARRIER.
B, INSULATION SHALL NOT BE INSTALLED UNTIL PIPE LINES HAVE BEEN PRESSURE TESTED, AND HEAT TRACE HAS BEEN INSTALLED AND
TESTED,
10.33 START UP/TESTING
A. UPON COMPLETION OF THE HEAT TRACE INSTALLATION, EACH HEAT TRACE RUN SHALL BE MEGGERED WITH A 2,500 VDC MEGGER.
ELECTRICAL INSULATION RESISTANCE SHALL NOT BE LESS THAN 20 MEGOHMS REGARDLESS OF LENGTH OF RUN, THIS TEST SHALL BE
PERFORMED BOTH BEFORE AND AFTER INSTALLATION OF THE THERMAL INSULATION. MEGGER TESTING FOR EACH HEATING CABLE SHALL
LAST AT LEAST ONE MINUTE.
B. EACH CIRCUIT SHALL BE ENERGIZED, AND VOLTAGE, PIPE TEMPERATURE AND CURRENT MEASURED AND DOCUMENTED, TO VERIFY
CORRECT OPERATION, TEMPERATURE M❑NIT❑RING AND CONTROLS SHALL ALSO BE OPERATED TO VERIFY PROPER OPERATION,
10.34 D❑CUMENTATI❑N
THE INSTALLED SYSTEM D❑CUMENTATI❑N SHALL INCLUDE ALL ITEMS LISTED IN THE SUBMITTAL SECTION OF THIS SPECIFICATION.
ADDITIONALLY, ALL TEST DATA GENERATED DURING START UP, INCLUDING ALL TEST VALUES, SHALL BE TURNED OVER TO PLANT
MAINTENANCE TO ASSIST IN FUTURE MAINTENANCE EFFORTS.
10.35 TRAINING
THE CONTRACTOR SHALL PROVIDE TRAINING, AT NO CHARGE TO OWNER, FOR PERSONS INVOLVED IN THE DESIGN, INSTALLATION,
C❑MMISSI❑NING, ❑PERATI❑N, AND MAINTENANCE FOR ANY SPECIFICALLY DESIGNED HEAT TRACE PROJECTS.
C.AaL
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8362
04 Mar 2021
HIPP ENGINEERING
& CONSULTING, INC.
2301 REXWOODS DRIVE, SUITE 200
RALEIGH, NC 27607
TEL:[phone] FAX:[phone]
NC FIRM LICENSE NUMBER: C-2146
WWW.HIPP-LISA.COM

GENERAL NOTES
A
B
C
D
E
F
G
H
J
K
L
M
27-5/8" 27
1
1A
2A
POWER
METER
25
S
1C
2E
SERVICE
CEI`
ENTR.
PI\
600A
2G
MAIN
FLF9E
BREAKER
RE(
SECTION
PL
(BOTTOM
2J
FEED)
FLF9F
LOA[
PU
2M
SP/
FLF69MMCCD ELEVATION
NO SCALE
TO UTILITY
UTILITY PROVIDED
XFMR.
500 KVA
FLF96DP02
RECIRC
PUMP
C A R��/
aL
Q28362
••• FVGINEF�
04 Mar 2021
HIPP ENGINEERING
& CONSULTING, INC.
2301 REXWOODS DRIVE, SUITE 200
RALEIGH, NC 27607
TEL: [phone] FAX- 919-755-9995
NC FIRM LICENSE NUMBER: C-2146
W W W.HIPP-USA.COM
1, FOR SYMBOLS AND ABBREVIATI❑NS SEE SHEET
FLF60001 FOR MORE DETAILS.
2, EXISTING CABLE TO CENTER PIV❑T TO BE
DISC❑NNECTED AND REROUTED FROM EXISTING MCC
FLFMCCA TO MCC FLF69MMCCD. THE EXISTING CABLE
TO BE ROUTED TO BE CLEAR OF THE L❑CATI❑N FOR
THE NEW TANK,
KEY NOTES
1, DRIVE SHALL BE YASKAWA NEMA 3R HD GA800
SERIES C❑NFIGURED DRIVE, MODEL NO. G8C7B156PC,

GENERAL NOTES
\ I �
O
UTILITY POLE TANK SELECTOR
SERVICE ENTRANCE PANEL
�� FLFLPAB 0
0- - - - -
MCC A L XFMR
EXISTING 0.67mg SBM TANK
EQUIP # FLF96BT
i
TOP EXISTING TANK
WALL = 396.24
TWR #1
I
I
LOADING
FLFLPAB
N
❑LOADING
STATION #2
FIT FIE
01 01
HS
03 /
TRUCK
APRON 10
LOADING
STATION #3
FLFLPAB - 18
- 22
VALVE
FLF96CV055
MCC
TOP EXISTING TANK
WALL = 396.24
LOADING PUMP`S
FLF96CP01 `
FLF96CV051 AGITATOR
' J7961BOI
FLF96CV050 \�...
PAD
MOUNTED
UTILITY
ANSFORMER
7
FLOW TRAN
FLF96CFT01
0
,
,
,
,
EXISTING 1.645m.g. SBM TANK
EQUIP # FLF96CT
I
LEVEL TRANSMITTER
FLF96CLT01
O 1 O
I
FLFLPAB - 16
7
/ FLFLPAB -18
0 I
SBM LOADING PUMP
FLF96DPOl
F�N'ePe
I
9
I
EDUCTOR RING--"4
I
I NEW SBM FLF D TANK
6,227 m3 — 1,645,000 GAL
ATOR
6CB03
1, SEE SHEET FLF60302 FOR PREVI❑US SET OF SHEET
NOTES.
2. SEE SHEET FLF67001 FOR PANEL AND FEEDER
SCHEDULE,
3, SEE SHEET FAA72963 FOR REFERENCED EQUIPMENT
TAG NUMBERS,
KEY NOTES
1, CONNECT NEW GR❑UNDING RING AROUND NEW TANK
TO EXISTING GR❑UNDING SYSTEM WITH COPPER
STRANDED CABLE SIZE #4/0, C❑NNECTI❑NS ARE TO
BE MADE USING AN EX❑THERMIC CADWELD PROCESS.
2, NEW RECIRCULATION PUMP TO BE POWERED FROM
FLF69MMCCD CUBICLE 2G, SEE SHEET FLF68001 FOR
FEEDER AND WIRE SIZE,
3, PR❑VIDE GR❑UNDING SYSTEM TO INCLUDE
GALVANIZED STEEL GR❑UNDING ELECTRODES WITH
COPPER —WELDED EXTERI❑R. 3/4' DIAMETER BY 10
FEET LONG, SPACE GROUNDING ELECTRODES EVENLY
AROUND THE CIRCUMFERENCE OF THE TANK
(TYPICAL),
4, COPPER STRANDED CABLE, SIZE #4/0 TO CONNECT
GR❑UNDING ELECTRODES AND TO CONNECT TO
STRUCTURAL STEEL OF TOWERS, CATWALK, AND MCC
ENCLOSURE TO GR❑UNDING GRID, CABLE TO BE
BURIED AT LEAST 18" BELOW FINISHED GRADE.
5, CONNECT COPPER STRANDED CABLE TO GR❑UNDING
ELECTRODES USING AN EX❑THERMIC CADWELD
PROCESS (TYPICAL),
6, MOUNT LIGHT UNDERNEATH CATWALK TO ILLUMINATE
WALKING PATH. PR❑VIDE 120VAC, HUBBELL LIGHT
FIXTURE (CAT.# VL15D-4G) RATED FOR OUTDOOR
USE.
7, MOUNT LIGHT ON POLE, PROVIDE 120VAC, HUBBELL
LIGHT FIXTURE (CAT,# VL15D-4G) RATED FOR
OUTDOOR USE,
8, NEW 3PHASE, 3 WIRE, 30A NEMA 4X FUSED AT 30A
DISC❑NNECT.
9, NEW L❑AD❑UT PUMP TO BE POWERED FROM
FLF69MMCCD CUBICLE 2J, SEE SHEET FLF68001 FOR
FEEDER AND WIRE SIZE,
10. HEAT TRACE CIRCUIT. SEE BILL OF MATERIAL ON
SHEET FLF607001.
11. EXISTING FEED TO CENTER PIVOT WILL BE
DISC❑NNECTED FROM EXISTING MCC "A' AND
REROUTED AND FED FROM NEW MCC,
12. CONTRACTOR RESP❑NSIBLE FOR R❑UTING CABLING
BELOW GRADE AND STUBBING UP PVC C❑NDUIT (4'
PER FEEDER FROM UTILITY PAD MOUNTED
TRANSFORMER TO INC❑MING LINE OF MCC
FLF69MMCCD),
13. C❑❑RDINATE FINAL L❑CATION OF CONDUIT STUB —UP
TO VFD WITH LAYOUT OF REBAR FOR CONCRETE PAD
BY STRUCTURAL,
A 03-04-21 1 JAB I PAS JISSUED FOR CONSTRUCTION
Rev.: IRev, date: I D wg I lRevisions:
Novozymes North America, Inc.
,AAA"CARA 77 Perry Chapel Church Road
Essio'� P.O. Box 576
novozymes® Franklinton, N.C. 275250576 USA
�- HIPP ENGINEERING Rethink Tomorrow Tel [phone]
28362 & CONSULTING INC. Est. date: 11-24-20
_�'•. FNc�NE��;� NZNA FLF
2301 REXWOODS DRIVE, SUITE 200 Design er: JAB
RALEIGI�,Nc 27607 ELECTRICAL LAYOUT
rEL: 919-755-1033 FAX: [phone] Scale: 1 8 " - 1 ' - 0 " POWER PLAN — SITE
04Mar 2021 NC FIRM LICENSE NUMBER:(-2146 Group no.: FLF62001 U502986 NEW
W W W.I IIPP-USA.COM Page no.: —

Catalog Number
Description
Qty
Units
3BTV1-CT
3 W/ft, 120V Raychem Self -Reg Heating Cable
127
ft
E-100-L-A
Above -Insulation Lighted End Seal Kit
1
each
JBS-SPA
Small Pipe Adapterfor E-100, JBS-100, and JS-100
1
bag
ETL-ENGLISH
Electric Traced Label fortraced pipes and tanks
10
each
GT-66
Glass Tape (66ft/roll) (not for stainless -steel pipes)
1
roll
PS-3
Pipe Strap 1to 3 in.
2
each
AMC- 1A
nVent Raychem Ambient Sensing Thermostat Adj. 15-14ODeg. F
leach
HEAT TRACE
B LL OF MATERIAL
SCOPE OF WORK
r-
SCOPEOF WORK
L_
NOTES:
PANEL NAME & NO. FLF LP AB LOCATION SBM TANK MAINS 100 CABINET MTG SURFACE
VOLTS: 208/120 PHASE: 3 0 , WIRE: 4 W. , 60 HZ., MIN. INTERRUPTING ,RATING : 10,000 AIC,
LOAD SERVED
BRANCH CIRCUIT
CONDUIT & WIRING
BREAKER
KVA
CKT
❑
CKT
KVA
BREAKER
BRANCH CIRCUIT
CONDUIT & WIRING
LOAD SERVED
POLE
AMP
I AMP
POLE
MAIN BREAKER
—
3
100
1
A
2
1.5
20
1
2—#10, 1—#12G, 3/4"
LIGHTING
3
100
3
B
4
1.0
20
1
2—#10, 1—#12G, 3/4"
LIGHTING
if
3
100
5
C
6
1.0
20
1
2—#10, 1—#12G, 3/4"
LIGHTING
LEVEL TRAN. FLF96CLT01
2—#12, 1—#12G, 3/4"
1
20
0.5
1 7
A
8
1.0
1 20
1
2—#10, 1—#12G, 3/4"
LIGHTING
FLOW TRAN. FLF96CFT01
2—#12, 1—#12G, 3/4"
1
20
0.5
9
B
10
1.0
20
1
2—#10, 1—#12G, 3/4"
RECEPTACLES
VALVE FLF96CV050
2—#10, 1—#12G, 3/4"
1
20
0.5
11
C
12
2.5
20
2
2—#10, 1—#12G, 3/4"
HEAT TRACE
VALVE FLF96CV051
2—#10, 1—#12G, 3/4"
1
20
0.5
13
A
14
1.0
3/4"
CIRCUIT 1
VALVE FLF96CV055
2—#10, 1—#12G, 3/4"
1
20
0.5
15
B
16
1.0
20
1
2—#10, 1—#12G, 3/4"
LIGHTING
TANK SELECTOR PANEL
2—#12, 1—#12G, 3/4"
1
20
1
17
C
18
0.5
20
1
2—#10, 1—#12G, 3/4"
RECEPTACLE
PH MONITOR AIT-01
2—#12, 1—#12G, 3/4"
1
20
0.5
19
A
20
0.5
20
1
2—#12, 1—#12G, 3/4"
FLOW MONITOR FIT-01
KNIFE VALVE V-01
2—#12, 1—#12G, 3/4"
1
20
0.5
21
B
1 22
1.0
30
1
2—#12, 1—#12G, 3/4"
HEAT TRACE*
23
C
24
25
1 A
26
27
B
28
29
C
30
REMARKS: * BREAKERS SHALL BE GROUND FAULT TYPE CONNECTED KVA: 16.50 TOTAL NO. POLES 30
1. EXISTING CABLE TO BE DISCONNECTED FROM EXISTING MCC AND ROUTED TO
NEW MCC. EXISTING CABLING TO CENTER PIVOT SHALL BE LOCATED AND
REROUTED CLEAR OF NEW TANK INSTALLATION. THE EXISTING CABLING IS
ASSUMED TO BE IN DIRECT BURIED CONDUIT FROM MCC AND TRANSITIONS
TO DIRECT BURIED CABLE. FIELD TO CONFIRM. REPLACE CABLE WITH NEW IF
REWORKED CABLE HAS INSUFFICIENT LENGTH. DO NOT SPLICE.
■
CAROC/,,
041
=8362 =
HIPP ENGINEERING
=- °y'•. FNciNE�� ;
& CONSULTING, INC.
ems,
/P .A .•
22301 EX SUITE 200
N60OODSDRIVE,
04 Mar 2021
TEL: [phone] FAX [phone]
NC FIRM LICENSE NUMBER: C-2146
W W W.HIPP-USA.COM

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04 Mar 2021
HIPP ENGINEERING
& CONSULTING, INC.
2301 REXWOODS DRIVE, SUITE 200
RALEIGH, NC 27607
TEL:[phone] FAX:[phone]
NC FIRM LICENSE NUMBER: C-2146
W W W.HIPP-USA.COM

G
IS WIDER THANu30', DOES yNOT NHAVE TO BE CENTERED
ON THE EQUIPMENT BUT AT LEAST EVEN WITH ONE
EDGE, EQUIPMENT DOOR SHALL BE ABLE TO OPEN AT
LEAST 90 DEG.
NOTEi
1. THIS FIGURE ILLUSTRATES THE
W❑RKING SPACE IN FRONT OF
ELECTRICAL EQUIPMENT REQUIRED
BY SECTI❑N 110.26 OF THE
NATI❑NAL ELECTRIC CODE.
LL ELECTRICAL EQUIPMENT
GENERAL NOTES-.
1. THIS EQUIPMENT INCLUDES BUT IS NOT LIMITED TO PANELBOARDS, SAFETY
SWITCHES, MOTOR STARTERS, JUNCTION BOXES AND OTHER ELECTRICAL
EQUIPMENT,
DEDICAT
THROUGH D SPACE
S�SPENPI ONTINUFc
NOTE:
STRUCTURAL CEILING
SUSPENDED CEILING
1. THIS FIGURE ILLUSTRATES THE
ADDITI❑NAL EXCLUSIVELY DEDICATED
SPACE REQUIRED OVER AND UNDER
PANELBOARDS FOR CABLES, RACEWAYS,
ETC, TO AND FROM PANELBOARDS
REQUIRED BY SECTI❑N 110.26 OF THE
NATI❑NAL ELECTRIC CODE.
PANELBOARDS
TABLE 'A' - WORKING CLEARANCES
VOLTAGE TO
GROUND,
N❑MINAL
MINIMUM CLEAR DISTANCE
CONDITION 1
CONDITION 2
CONDITION 3
0-150
3'-0'
3'-0'
3'-0'
151- 600
3'-0'
3'-6'
4'-0'
WHERE THE 'CONDITIONS' ARE AS FOLLOWS;
1. EXPOSED LIVE PARTS ON ONE SIDE AND NO LIVE OR GROUNDED PARTS ON THE OTHER
2. NO PIPING, DUCTS OR EQUIPMENT FOREIGN TO THE ELECTRICAL EQUIPMENT SIDE OF THE WORKING SPACE, OR EXPOSED LIVE PARTS ON BOTH SIDES EFFECTIVELY
OR ARCHITECTURAL APPURTENANCES SHALL BE PERMITTED TO BE INSTALLED GUARDED BY SUITABLE WOOD OR OTHER INSULATING MATERIALS. INSULATED WIRE OR
IN, ENTER OR PASS THROUGH THE DEDICATED SPACES SHOWN ABOVE, INSULATED BUSBARS OPERATING AT NOT OVER 300V SHALL NOT BE CONSIDERED LIVE
PARTS.
ODEDICATED
NOT TO SCALE
Il
2. EXPOSED LIVE PARTS ON ONE SIDE AND GROUNDED PARTS ON THE OTHER SIDE.
3. EXPOSED LIVE PARTS ON BOTH SIDES OF THE WORK SPACE (NOT GUARDED AS PROVIDED
IN CONDITION 1) WITH THE OPERATOR BETWEEN.
WORKING SPACE REQUIREMENTS FOR ELECTRICAL EQUIPMENT
44/n AWF. RARE STRAWFlI
112' LOCK WASHER
TYPICAL SKID
M.
EQUIPMENT SKID GROUNDING - COMPRESSION FITTING
NOT TO SCALE
VERTICAL
COLUMN
EXOTHERMAL WELD CAI
TYPE VBC-2Q WELD ME
OR ACCEPTABLE EQUAL
GROUND CONDUCTOR
COLUMN BASE
PLATE
COLUMN BASE
TYPICAL EXOTHERMAL WELD
NOT TO SCALE
POWER CABLE
RIGID CONDUIT
LOCKNUTS
GROUND BUS TO BE
BONDED TO ENCLOSURE
NEUTRAL BUS TO BE
INSULATED FROM
ENCLOSURE
CIRCUIT BREAKER OR
FUSES
PHASE WIRES
INSULATED GROUNDING
BUSHING
TYPICAL POWER CABLE TERMINATION AT ELECTRICAL ENCLOSURE
NOT TO SCALE
Essiol/
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z836z - & CONSULTING, INC.
/<< .A S�\° 22301 RFH N60OODSDRIVE, SUITE 200
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TEL:[phone] FAX:[phone]
04 Mar 2021 NC FIRM LICENSE NUMBER: C-2146
W W W.H I PP-USA.COM

pH PROBE ASSEMBLY
� NOT TO SCALE
NOTE
ADDITI❑NAL C❑NDUIT ENTRYWAY
SHALL BE PLUGGED WITH PTFE TAPE
AND STAINLESS STEEL PLUG,
30' MIN, STRAIGHT RUN
N❑TES=
1, SENSOR SHALL BE MOUNTED S❑
OF THE FLOW ARROW SHOWN ON
IN DIRECTI❑N OF FLOW,
THAT THE FORWARD END
THE SENSOR ID TAG P❑INTS
2, TOP OF SENSOR SHALL BE EITHER VERTICAL OR H❑RIZ❑NTAL,
3, SENSOR SHALL BE INSTALLED IN A P❑SITI❑N WHICH ENSURES
THE SENSOR REMAINS FULL DURING ❑PERATI❑N, VERTICAL WITH
UPWARD FLOW IS PREFERRED. H❑RIZ❑NTAL IS ACCEPTABLE PR❑VIDED
THE SENSOR REMAINS FULL.
10
2" NPT PIPE M❑UNTIN
FLOWMETER TRANSMITTER GROUNDING
NOT TO SCALE
FLOWMETER TRANSMITTER MOUNTING
NOT TO SCALE
c�nr-�vrT ri icy r nAi 1"1rT1 ire T Air rrr
GROUND STRAP
�)) CONDUIT FROM TRANSMITTER
12' MIN
ARROW INDICATING DIRECTI❑N OF FLOW,
GASKETS PR❑VIDED BY INSTALLER,
/2-14 NPT
LECTRICAL CONNECTION
POWER AND SIGNAL)
'T
4L C❑NNECTI❑N
ELEMENT)
.j W&@jjl
TRANSMITTER BODY
nrr I T AIC no nrr-L
TRANSMITTER
POWER CABLE
ANALOG SIGNAL
CABLE
FLOWMETER TRANSMITTER WIRING
NOT TO SCALE
ELEMENT JUNCTI❑N
BOX
ANALOG SIGNAL
CABLE
SENSOR WIRING
CABLE
�pH TRANSMITTER WIRING
� NOT TO SCALE
FLOWMETER ELEMENT WIRING
NOT TO SCALE
TRANSMITTER
JUNCTI❑N BOX
ELEMENT SIDE
'NATI❑N SIGNAL
CABLE PR❑VIDED
7, CONDUCTORS
:D TO EQUAL LENGTHS.
BILL OF MATERIALS/MAGNETIC FLOWMETER
ITEM
QTY,
DESCRIPTI❑N
MFR.
MODEL
1
6
1/2' LIQUID TIGHT FLEX CONNECTOR
APPLET❑N
4QSS50T
2
3
3/4' CONDUIT DRAIN VENT
APPLET❑N
CRN75
3
3
3/4' CONDUIT TEE
APPLET❑N
T200M
4
A/R
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S❑UTHWIRE
58046201
5
1 3
3/4' TO 1/2' REDUCING BUSHING
I APPLET❑N
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N❑TEI USE PARTS OR APPROVED EQUAL
TO ANALOG SIGNAL
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02 929 & CONSULTING, INC.
FNGINE��: c
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RLEIGH
TEL:[phone] FAX:[phone]
04 Mar 2021 NC FIRM LICENSE NUMBER: C-2146
W W W.HIPP-LISA.COM
NOTE
FROM 120 VAC
POWER SOURCE
NOTE
ADDITI❑NAL C❑NDUIT ENTRYWAY
SHALL BE PLUGGED WITH PTFE TAPE
AND STAINLESS STEEL PLUG.
FLOWMETER CONDUIT DETAILS
NOT TO SCALE
/A 1 03-04-21 1 GCL I JJW I ISSUED FOR CONSTRUCTION
Rev.: lRev. date: I Dwg I jRevisions:
Novozymes North America, Inc.
77 Perry Chapel Church Road
P.O. Box 576
novozymesx (-ranklinton, N.C. 27525-0576 USA
Rethink Tomorrow Tel [phone]
Est. date: 02-01-21 NZNA — SBM TANK ADDITION
Designer: R. EEONARD INSTRUMENTATION
Scale: AS NOTED INSTALLATION DETAILS
Group no,: Page no.: FLF84001 U502986 NEW
— —

novozymes
NOVOZYMES
FRANKLINTON, NORTH CAROLINA
SBM TANK ADDITION
SPECIFICATIONS
HIPP PROJECT #R20162
04MAR2021
Rev
Date
Purpose of Issuance
A
14JAN2021
Issued for Review
B
10FEB2021
Issued for Final Review
0
04MAR2021
Issued for Construction
Fi?;1
HIPP ENGINEEKING
& CONSULTING, INC.
2301 Rexwoods Drive Suite 200
Raleigh, NC 27607
Telephone [phone]
Fax [phone]

I??
HIPP ENGINEERING
& CONSULTING, INC.
Professional Seal
NOVOZYMES
HIPP Project No.: R20162
SBM TANK ADDITION
DATE: 04MAR2021
SPECIFICATIONS
ISSUED FOR CONSTRUCTION
MECHANICAL PROCESS
INSTRUMENTATION & CONTROLS
2301 Rexwoods Drive, Suite 200 • Raleigh, North Carolina • 27607 • Tel: [phone] • Fax: [phone]

1 P?
HIPP ENGINEERING
& CONSULTING, INC.
SPECIFICATION INDEX
NOVOZYMES
SBM TANK ADDITION
HIPP PROJECT NO.:R20162
04MAR2021
Section
Specification Title
Rev.
DIVISION 13
SPECIAL CONSTRUCTION
13200
PRESTRESSED CONCRETE STORAGE TANK
0
-
FLF96DP01 SBM LOADOUT PUMP DATA SHEET
0
-
FLF96DP02 SBM CIRCULATION PUMP DATA SHEET
0
-
FLF96ED01-10 SBM IN -TANK EDUCTORS DATA SHEET
0
130805-31-001
CONSTRUCTION SPECIFICATIONS FOR ABOVEGROUND
PIPING
For Reference
Only
DIVISION 23
HEATING, VENTILATION, AND AIR CONDITIONING (HVAC)
230902
SEQUENCE OF OPERATIONS
0
SPECIFICATION INDEX
Paae 1 of 1
HIPP •2301 REXWOODS DRIVE, SUITE 200 • RALEIGH, NORTH CAROLINA • 27607 • TEL: [phone] • FAX: [phone]

NOVOZYMES NORTH AMERICA INC.
FRANKLINTON, NC
SBM TANK ADDITION
SECTION 13200
PRESTRESSED CONCRETE STORAGE TANK
PART 1 - GENERAL
1.1 SCOPE OF WORK
H I P P PROJECT #R20162
SECTION 13200
REV. 0
A. This section specifies the design and construction of an ANSI/AWWA D110 wire -wound
prestressed concrete storage tank with a Type II core wall and galvanized steel
diaphragm including all reinforcing, concrete work, accessories, disinfection and testing
directly related to the tank.
B. The tank contractor is responsible for furnishing all labor, materials, tools and equipment
necessary to design and construct the prestressed concrete storage tank as indicated
on the drawings and as described in this specification.
1.2 REFERENCES
A. ACI 117 Specification for Tolerances for Concrete Construction and Materials
B. ACI 301/301 M — Specifications for Structural Concrete for Buildings.
C. ACI 305R — Guide to Hot Weather Concreting.
D. ACI 306R — Guide to Cold Weather Concreting.
E. ACI 347R — Guide to Formwork for Concrete.
F. ACI 350/35OR — Code Requirements for Environmental Engineering Concrete Structures
and Commentary.
G. ACI 350.3 — Seismic Design of Liquid -Containing Concrete Structures and Commentary.
H. ACI 372R — Design and Construction of Circular Wire- and Strand -Wrapped Prestressed
Concrete Structures.
ACI 506R — Guide to Shotcrete.
J. ACI 506.2 — Specification for Materials, Proportioning, and Application of Shotcrete.
K. ACI SP4: Formwork for Concrete.
L. ANSI/AWWA C652 — Disinfection of Water Storage Facilities.
HIPP ENGINEERING AND CONSULTING, INC. SECTION 230902
RALEIGH, NC SEQUENCE OF OPERATIONS
PAGE 1 OF 16

NOVOZYMES NORTH AMERICA INC. H I P P PROJECT #R20162
FRANKLINTON, NC SECTION 13200
SBM TANK ADDITION REV. 0
M. ANSI/AWWA D110 — Wire- and Strand -Wound, Circular, Prestressed Concrete Water
Tanks.
N. ASCE Standard 7 — Minimum Design Loads for Buildings and Other Structures.
O. ASTM A416/A416M — Standard Specification for Steel Strand, Uncoated Seven -Wire for
Prestressed Concrete.
P. ASTM A475/475M — Standard Specification for Zinc -Coated Steel Wire Strand.
Q. ASTM A603/603M — Standard Specification for Zinc -Coated Steel Structural Wire Rope.
R. ASTM A615/A615M — Standard Specification for Deformed and Plain Carbon -Steel Bars
for Concrete Reinforcement.
S. ASTM A653/653M — Standard Specification for Steel Sheet, Zinc Coated (Galvanized)
or Zinc Iron Alloy Coated (Galvannealed) by Hot Dip Process.
T. ASTM A821/A821M — Standard Specification for Steel Wire, Hard Drawn for
Prestressing Concrete Tanks.
U. ASTM A884/A884M — Standard Specification for Epoxy Coated Steel Wire and Welded
Wire Reinforcement.
V. ASTM Al064/A1064M — Standard Specification for Carbon Steel Wire and Welded Wire
Reinforcement, Plain and Deformed, for Concrete.
W. ASTM C31/C31 M — Standard Practice for Making and Curing Concrete Test Specimens
in the Field.
X. ASTM C33/C33M — Standard Specification for Concrete Aggregates.
Y. ASTM C39/C39M — Standard Test Method for Compressive Strength of Cylindrical
Concrete Specimens.
Z. ASTM C143/C143M — Standard Test Method for Slump of Hydraulic -Cement.
AA. ASTM C172/C172M — Standard Practice for Sampling Freshly Mixed Concrete.
BB. ASTM C231 /C231 M — Standard Test Method for Air Content of Freshly Mixed Concrete
by the Pressure Method.
CC. ASTM C881/C881M — Standard Specification for Epoxy -Resin -Base Bonding Systems
for Concrete.
DD. ASTM D1056 — Standard Specification for Flexible Cellular Materials -Sponge or
Expanded Rubber.
EE. ASTM D1557 — Standard Test Method for Laboratory Compaction Characteristics of Soil
Using Modified Effort.
HIPP ENGINEERING AND CONSULTING, INC. SECTION 230902
RALEIGH, NC SEQUENCE OF OPERATIONS
PAGE 2 OF 16

NOVOZYMES NORTH AMERICA INC. H I P P PROJECT #R20162
FRANKLINTON, NC SECTION 13200
SBM TANK ADDITION REV. 0
FF. ASTM D4397 — Standard Specification for Polyethylene Sheeting for Construction,
Industrial, and Agricultural Applications.
GG. ASTM F593 Standard Specification for Stainless Steel Bolts, Hex Cap Screws, and
Studs.
HH. AWS D1.2 — Structural Welding Code — Aluminum.
II. "Earthquake Induced Sloshing in Tanks with Insufficient Freeboard" by P.K. Malhotra,
Structural Engineering International, IASBSE, 3/2006 pp 222-225.
JJ. OSHA 29 CFR 1910 — OSHA General Industry Regulations.
KK. U.S. Army Corps of Engineers CRD-C-572-74 — Specification for Polyvinylchloride (PVC)
Waterstop
Note: Where reference is made to one of the above standards, the revision in effect at the time of
bid opening shall apply.
1.3 SUBMITTALS
A. Prequalification Data: Provide prequalification data prior to the bid in accordance with
Section 1.5 B. of this specification.
B. Shop Drawings: Provide shop drawings with a minimum size of 18" x 24" with a complete
plan, elevation, and sectional views showing critical dimensions as follows:
1. Size, location and number of all reinforcing bars.
2. Thickness of all parts of the tank structure including floor, core wall, dome, and
covercoat.
3. Prestressing schedule including number and placement of prestressing wires on
the tank wall and total applied force per foot of wall height.
4. Location and details of all accessories required.
C. Concrete Data: Submit concrete design mixes including ingredient proportions,
minimum cementitious content, and water/cementitious ratio in accordance with Section
2.2 and 2.3 of this specification.
D. Design Data: Submit structural calculations for the tank, signed and sealed by a
professional engineer in accordance with Section 1.5 A.3 of this specification.
E. Coating Data: Submit color charts for review by the engineer and owner. Once a color
is chosen, submit actual drawdown samples for final approval prior to application of
coating.
F. Test Reports: Submit concrete strength reports for 7-day and 28-day breaks taken in
accordance with the requirements of Section 3.3 A.1.
HIPP ENGINEERING AND CONSULTING, INC. SECTION 230902
RALEIGH, NC SEQUENCE OF OPERATIONS
PAGE 3 OF 16

NOVOZYMES NORTH AMERICA INC. H I P P PROJECT #R20162
FRANKLINTON, NC SECTION 13200
SBM TANK ADDITION REV. 0
G. Warranty Document: Submit warranty document in Owner's name in accordance with
Section 1.6. of this specification.
(:
1.4
L
0
Cleaning and Disinfection Plan: Submit a cleaning and disinfection plan which complies
with Section 3.4 of this specification.
Project Record Documents: Record actual location layout and final configuration of tank
and accessories on shop drawings and submit to engineer after construction of the tank
is complete.
QUALITY ASSURANCE
Qualifications and Experience:
1. Tank Construction Company: Shall be a firm with a minimum of three years of
experience in the design and construction of ANSI/AWWA D110 wire -wound,
circular prestressed concrete tanks with Type II core walls to ensure the owner that
it has the organization, technical skill, quality control, reliability, and financial
stability to build and guarantee the tank in accordance with the quality required by
these specifications. The tank construction company shall have built with its own
resources and have under warranty, a minimum of ten (10) prestressed concrete
tanks of equal or greater size than that required for this project which meet these
specifications and are now providing satisfactory service.
2. Construction: The entire tank, including all portions of the floor and wall shall be
built by the tank construction company, using its own trained personnel and
equipment.
3. Design: All design work for the tank shall be performed by a professional engineer
with no less than five years of experience in the design and construction of
ANSI/AWWA D110 wire -wound, circular prestressed concrete tanks with Type II
core walls. The professional engineer shall be a full-time staff member of the tank
construction company and shall be licensed to work in the state where the project
is located.
4. The diaphragm design and epoxy injection procedure shall have been used in the
ten tanks required in Section 1.5 A.1 of this specification.
Prequalification:
1. All tank construction companies must be prequalified and meet the criteria stated
in Section 1.5 A.1 of this specification to be considered an acceptable tank builder.
2. A complete prequalification package shall be submitted to the Engineer for
consideration by the date set for receipt of bids. The prequalification submittal
shall include the following items:
a. Complete construction drawings showing the principal sizes, thicknesses,
reinforcing size and spacing for all structural members including: floor, wall,
dome shell and dome edge.
b. Complete details of other structural appurtenances as required by the project
drawings showing principal sizes, thickness and reinforcing sizes and
spacing.
HIPP ENGINEERING AND CONSULTING, INC. SECTION 230902
RALEIGH, NC SEQUENCE OF OPERATIONS
PAGE 4 OF 16

NOVOZYMES NORTH AMERICA INC.
FRANKLINTON, NC
SBM TANK ADDITION
H I P P PROJECT #R20162
SECTION 13200
REV. 0
C. Complete design calculations which address applicable loads provided in
Section 1.7 B. of this specification.
d. Complete experience record for the tanks used to meet the experience
requirement of Section 1.5 A. of this specification that have been designed
and built in the tank construction company's own name and shall include
only those tanks that are under the company's warranty. The record shall
include the size of the tank, name, address and telephone number of the
Owner, the year of construction and the name and telephone number of the
Engineer for the project.
e. Experience in prestressed concrete tanks of the type specified herein for the
construction superintendent, foreman, and three most experienced
tankbuilders. Experience shall be with the bidder during the three previous
years.
f. Construction schedule which details the duration for tank construction.
3. The following are preapproved as acceptable tank construction companies:
a. The Crom Corporation, Gainesville, Florida.
b. Precon Corporation, Newberry, Florida
C. Approved alternate
1.5 WARRANTY
A. The tank construction company shall provide a warranty for workmanship and materials
on the complete structural portion of the tank for a five-year period from the date of
acceptance of the work. The warranty shall not apply to any accessory, equipment or
product that is not a structural part of the tank and is manufactured by a company other
than the tank construction company.
B. If any leakage or other defects appear within the five-year period, the tank construction
company shall promptly repair the tank at its own expense upon written notice by the
Owner that such defects have been found. Leakage is defined as a stream flow of liquid
appearing on the exterior of the tank, the source of which is from the inside of the tank.
1.6 DESIGN CRITERIA
A. The design shall be in conformance with applicable portions of American Concrete
Institute (ACI) 372R Design and Construction of Circular Wire- and Strand -Wrapped
Prestressed Concrete Structures, ANSI/AWWA D110 Wire- and Strand -Wound,
Circular, Prestressed Concrete Water Tanks with Type II core walls, and currently
accepted engineering principles and practices for the design of such structures.
B. Reference the following drawings:
1. FLF73002 Piping Arrangement to FLF96DT
2. FLF75001 FLF96DT General Arrangement
HIPP ENGINEERING AND CONSULTING, INC. SECTION 230902
RALEIGH, NC SEQUENCE OF OPERATIONS
PAGE 5 OF 16

NOVOZYMES NORTH AMERICA INC. H I P P PROJECT #R20162
FRANKLINTON, NC SECTION 13200
SBM TANK ADDITION REV. 0
C. The following loadings shall be utilized in the design:
1. Capacity: 1.645M Gallons
2. Dimensions: 100 ft Inside Diameter
3. 28 ft Total Height
4. Sump: provide a 72" diameter by 4 foot deep sump located as indicated on
drawings.
5. Fluid Loads: Shall be the weight of all liquid when the reservoir is filled to capacity.
The unit weight of the liquid material shall be 71.76 Ibs/ft3. Specific gravity = 1.15.
6. Dead Loads: Consideration shall be given to all permanent imposed loads
including concrete and steel.
7. Seismic Loads:
a. Seismic forces and moments resulting from water sloshing and seismic
accelerations of the tank dome, wall, and water loads shall be calculated in
accordance with ACI 350.3 or ANSI/AWWA D110.
b. If sufficient freeboard height is not provided to prevent uplift forces due to
sloshing, the impulsive participation shall be increased due to the
constrained motion of liquid, and the tank roof and its connection shall be
designed to resist the uplift forces in accordance with P.K. Malhotra's
"Earthquake Induced Sloshing in Tanks with Insufficient Freeboard".
8. Soil Pressure: Earth loads shall be determined by rational methods of soil
mechanics. Soil pressure shall not be used in the design of the core wall to
counteract hydraulic loads or provide residual compression in the wall.
9. Differential Backfill Loads: Forces from differential backfill loads shall be
considered in the design and shall be based on the at -rest coefficient. Passive
resistance shall not be used to resist differential backfill loads.
10. Wind Loads: Wind loads shall be considered in the design in accordance with
ASCE 7.
D. Subbase: A granular base material shall be used beneath the membrane slab when the
subgrade materials do not allow free drainage.
1. The base material should consist of a clean, well -compacted, angular or sub -
angular material with a minimum thickness of 6 in.
2. The gradation of the base material should be selected to permit free drainage
without the loss of fines or intermixing with the subgrade material.
3. The maximum particle size of the base material should be limited to provide a
relatively level working surface without potential intrusion of the base materials into
the membrane floor slab concrete.
4. Base material should be compacted to 95 percent of the maximum laboratory
density determined by ASTM D1557.
E. Floor: The design of the floor for the prestressed concrete tank shall conform to the
following:
Concrete membrane floors shall be a minimum of 6" thick and have a minimum
thickness of 8" of concrete over all pipe encasements and around sumps.
HIPP ENGINEERING AND CONSULTING, INC. SECTION 230902
RALEIGH, NC SEQUENCE OF OPERATIONS
PAGE 6 OF 16

NOVOZYMES NORTH AMERICA INC. H I P P PROJECT #R20162
FRANKLINTON, NC SECTION 13200
SBM TANK ADDITION REV. 0
2. A minimum percentage of 0.60% reinforcing steel shall be used in the membrane
floor. The minimum percentage shall apply to all thickened sections and shall
extend a minimum of 2 ft into the adjacent membrane floor.
F. Core wall:
1. The wire -wound, prestressed concrete tank core wall shall be designed as a thin
shell cylindrical element using shotcrete and an embedded, mechanically bonded,
galvanized steel shell diaphragm.
2. The design of the core wall shall take into account appropriate edge restraint. To
compensate for bending moments, shrinkage, differential drying, and temperature
stresses, the following minimum reinforcing steel shall be incorporated into the
design:
a. The top 2 ft of core wall shall have not less than 1 % circumferential
reinforcing.
b. The bottom 3 ft of core wall shall have not less than 1 % circumferential
reinforcing.
C. Inside Face:
1) The inside face of the core wall shall utilize the diaphragm as effective
reinforcing.
2) Additional vertical and horizontal reinforcing steel bars shall be used
as required by design computations.
d. Outside Face:
1) Vertical reinforcing steel in the outside face of the core wall shall be:
minimum of #4 bars at 12" center to center.
2) Additional vertical and horizontal reinforcing steel bars shall be used
as required by design computations.
3. The minimum core wall thickness shall be 3'/2".
4. Reinforcing steel used in the core wall shall be designed using a maximum
allowable design tensile stress, fs, of 18,000 psi.
5. Allowable compressive stress in the core wall due to initial prestressing force, fg;,
shall be:
a. 1250 psi + 75t psi/in. with 0.5 f'g; maximum or less (where f'g; is defined as
compressive strength at time initial prestressing force is applied and t is the
thickness of the core wall in inches).
b. Maximum of 2250 psi.
6. Allowable compressive stress in the core wall due to final prestressing force, fg,
shall be:
a. 1250 psi + 75t psi/in. with 0.45 f'g maximum (where f'g is defined as
compressive strength required for final prestressing force and t is the
thickness of the core wall in inches).
b. Maximum of 2025 psi.
HIPP ENGINEERING AND CONSULTING, INC. SECTION 230902
RALEIGH, NC SEQUENCE OF OPERATIONS
PAGE 7 OF 16

NOVOZYMES NORTH AMERICA INC.
FRANKLINTON, NC
SBM TANK ADDITION
H I P P PROJECT #R20162
SECTION 13200
REV. 0
G. Prestressing:
1. Circumferential prestressing of the tank shall be achieved by the application of
cold -drawn, high -carbon steel wire placed under high tension.
2. A substantial allowance shall be made for prestressing losses due to shrinkage
and plastic flow in the shotcrete and due to relaxation in the prestressing steel.
3. The prestressing design shall conform to the following minimum requirements:
a. Working stress for the tank wall, fs, shall be a maximum of 115,000 psi.
b. The allowable design tensile stress in the prestressing wire before losses,
fsi shall be 145,600 psi or no greater than 0.63 fu, where fu is defined as the
ultimate strength of the wire.
C. Areas to be prestressed will contain no fewer than 10 wires per foot of wall
for 8 gauge and 8 wires per foot of wall for 6 gauge.
d. A maximum of 24 wires per layer per foot for 8 gauge and 20 wires per layer
per foot for 6 gauge will be allowed.
H. Wall Openings:
1. When it is necessary for a pipe to pass through the tank wall, the invert of such
pipe or sleeve shall provide no less than 18" clear space at the bottom of the wall
to provide sufficient clear area for the prestressing wires. The prestressing wires
required at the pipe elevation shall be distributed into circumferential bands
immediately above and below the opening to maintain the required prestressing
force while leaving an unbanded strip around the entire tank.
2. Unbanded strips shall have a vertical dimension of no more than 36" unless an axi-
symmetric shell analysis is performed to account for compressive forces plus shear
and moments caused by displacement of the prestressing wires into adjacent
bands.
PART 2 - PRODUCTS
2.1 PERFORMANCE
A. Performance of the materials used in the tank construction shall conform to the minimum
requirements of this specification.
B. Substitutions to the materials in this specification may only be made if submitted in writing
and approved by the engineer.
C. Any material that can come into contact with tank liquid contents must be able to
withstand a chloride concentration of 1300 PPM. Vendor to supply suitable material or
provide coating as required.
HIPP ENGINEERING AND CONSULTING, INC. SECTION 230902
RALEIGH, NC SEQUENCE OF OPERATIONS
PAGE 8 OF 16

NOVOZYMES NORTH AMERICA INC.
FRANKLINTON, NC
SBM TANK ADDITION
2.2 CONCRETE
19
B.
C.
D.
E.
F.
H I P P PROJECT #R20162
SECTION 13200
REV. 0
Concrete shall conform to ACI 301/301 M as well as ACI 305R/306R IAW Section 1.2 of
this Specification.
All concrete shall utilize Type 1/11 Portland cement.
A maximum of 25% of cementitious material may be fly ash.
Admixtures other than air -entraining and water reducing admixtures will not be permitted
unless approved by the engineer.
Coarse and fine aggregate shall meet the requirements of ASTM C33/C33M.
Concrete mixes used in the construction of the tank shall conform to the following:
Compressive
Minimum
Maximum
Maximum
Air
Mix
Strength
Cement
Aggregate
W/C
Content
Slump
(psi)
Content
Size
Ratio
N
(in)
(Ibs)
(in)
Floor
4000
560
3/4
0.45
2.3 SHOTCRETE
ra
1.9
C.
Shotcrete shall conform to the requirements of ACI 506.2 except as modified herein.
All shotcrete mixes shall utilize Type 1/II cement.
A maximum of 25% of cementitious material may be fly ash.
D. All shotcrete in contact with diaphragm or prestressing wire shall be proportioned to
consist of not more than three parts sand to one part Portland cement by weight. All
other shotcrete shall be proportioned to consist of not more than four parts sand to one
part Portland cement by weight.
E
F
G
Admixtures will not contain more than trace amounts of chlorides, fluorides, sulfides or
nitrates.
Fine aggregate shall meet the requirements of ASTM C33/C33M.
Shotcrete mixes used in the tank construction shall conform to the following:
Compressive
Maximum
Air
Slump
Fiber
Mix
Strength
W/C
Content
(�n)
Reinforcement
(psi)
Ratio
M
(Ibs/cyd)
Core Wall
4000
0.42
5"+/-1"
-
Covercoat
4000
0.42
5"+/-1"
HIPP ENGINEERING AND CONSULTING, INC. SECTION 230902
RALEIGH, NC SEQUENCE OF OPERATIONS
PAGE 9 OF 16

NOVOZYMES NORTH AMERICA INC. H I P P PROJECT #R20162
FRANKLINTON, NC SECTION 13200
SBM TANK ADDITION REV. 0
2.4 MOISTURE BARRIER
A. The moisture barrier shall be polyethylene, Class A, conforming to ASTM D4397 with a
minimum thickness of 6-mils.
2.5 PRESTRESSED REINFORCEMENT
A. The prestressing wire shall conform to the requirements of ASTM A821 /A821 M, Type B.
B. The prestressing wire size shall be 0.162" (8 gauge), 0.192" (6 gauge) or larger, but no
larger than 0.250".
C. The ultimate tensile strength, fu shall be, 231,000 psi or greater for 8 gauge wire, 222,000
psi or greater for 6 gauge.
D. Splices for horizontal prestressed reinforcement shall be ferrous material compatible with
the prestressing reinforcement and shall develop the full strength of the wire.
2.6 NON -PRESTRESSED REINFORCEMENT
A. Non -prestressed mild reinforcing steel shall be new billet steel meeting the requirements
of ASTM A615/A615M with a minimum yield strength, fy, of 60,000 psi.
B. Welded wire reinforcing shall be plain wire conforming to the requirements of ASTM
A1064/A1064M with a minimum yield strength, fy, of 65,000 psi.
2.7 GALVANIZED STEEL DIAPHRAGM
A. The galvanized steel diaphragm used in the construction of the core wall shall be 26
gauge with a minimum thickness of 0.017 in. conforming to the requirements of ASTM
A653/A653M. Weight of zinc coating shall be not less than G90 of Table 1 of ASTM
A653/A653M.
B. The diaphragm shall be formed with re-entrant angles and erected so that a mechanical
key is created between the shotcrete and diaphragm.
C. The diaphragm shall be continuous to within 3 in. of the top and bottom of the wall.
Horizontal joints or splices will not be permitted.
D. All vertical joints in the diaphragm shall be rolled seamed, crimped and sealed watertight
using epoxy injection.
E. In all tanks designed to use a waterstop at the floor/wall joint, the steel shell diaphragm
shall be epoxy bonded to the waterstop.
HIPP ENGINEERING AND CONSULTING, INC. SECTION 230902
RALEIGH, NC SEQUENCE OF OPERATIONS
PAGE 10 OF 16

NOVOZYMES NORTH AMERICA INC. H I P P PROJECT #R20162
FRANKLINTON, NC SECTION 13200
SBM TANK ADDITION REV. 0
2.8 PVC WATERSTOPS, BEARING PADS AND SPONGE FILLER
A. Plastic waterstops shall be extruded from an elastomeric plastic material of which the
base resin is virgin polyvinylchloride (PVC). PVC waterstops shall conform to the
requirements of CRD-C-572-74.
B. The profile and size of the waterstop shall be suitable for the hydrostatic pressure and
movements to which it is exposed.
C. Bearing pads used in floor/wall joints shall consist of neoprene, natural rubber or
polyvinyl chloride.
D. Sponge filler at the floor/wall joint shall be closed -cell neoprene.
2.9 EPDXY
A. Epoxy Sealants:
1. Epoxy shall conform to the requirements of ASTM C881/C881 M.
2. Epoxy used for sealing the diaphragm shall be Type III, Grade 1, and shall be
100% solids, moisture insensitive, low modulus epoxy.
3. Epoxy used for placing the waterstop shall be Type II, Grade 2, and shall be 100%
solids, moisture insensitive, low exotherm epoxy.
4. When pumped, maximum viscosity of the epoxy shall be 10 poises at 77°F.
5. The epoxy sealants used in the tank construction shall be suitable for bonding to
concrete, shotcrete, PVC and steel.
B. Bonding Epoxy:
1. Epoxy resins used for enhancing the bond between fresh concrete and hardened
concrete shall conform to the requirements of ASTM C881/C881 M.
2. Epoxy resins shall be a two -component, 100% solids, moisture -insensitive epoxy
and shall be Type II, Grade 2.
2.10 SEISMIC RESTRAINT CABLES
A. When required by design, seismic restraint cables shall be'/2-inch diameter, seven -wire
strand conforming to ASTM A416/A416M, prior to galvanizing.
B. The strand shall be galvanized in accordance with ASTM A475, or ASTM A603, with a
minimum weight per unit of coated wire surface, Class A.
C. The minimum yield strength of the seven -wire strand shall be 270,000 psi.
HIPP ENGINEERING AND CONSULTING, INC. SECTION 230902
RALEIGH, NC SEQUENCE OF OPERATIONS
PAGE 11 OF 16

NOVOZYMES NORTH AMERICA INC.
FRANKLINTON, NC
SBM TANK ADDITION
2.11 TANK ACCESSORIES
H I P P PROJECT #R20162
SECTION 13200
REV. 0
A. Where any tank accessory can come into contact with tank liquid contents, vendor to
provide an alternate material able to withstand a chloride concentration of 1300 PPM or
provide coating as required.
B. Minimum of one, 1' 5" x 4' 4" rectangular Type 316 stainless steel wall manhole for
access to the interior of the tank. The cover shall also be of Type 316 stainless steel.
The wall manhole shall be designed to resist hydraulic loading without excessive
deflection.
C. Through -wall pipe sleeves shall be Type 316 stainless steel sleeves with neoprene
modular seal units. Waterstop rings on wall -pipes shall be Type 316 stainless steel.
D. Accessory hardware, unless otherwise noted, shall be Type 316 stainless steel
conforming to ASTM F593.
E. Provide pipe supports for horizontal and vertical pipe as well as the eductor manifold as
indicated on drawings.
PART 3 - EXECUTION
3.1 EXAMINATION
A. All subgrade elevations shall be verified prior to starting tank construction.
3.2 INSTALLATION
A. Floor:
1. The subgrade shall be prepared by fine grading to ensure proper placement of
reinforcing steel with proper bottom cover.
2. A 6-mil polyethylene vapor -barrier shall be placed after subgrade preparation has
been completed.
3. Form and screed boards shall be of proper thickness and sufficiently braced to
ensure that the floor is constructed within proper thickness tolerances.
4. Plate bolsters shall be used to support reinforcing steel supported directly on the
subgrade to ensure positive control of placement of reinforcing steel.
5. The floor shall be vibratory screeded to effect consolidation of concrete and proper
encasement of floor reinforcing steel.
6. The floor shall be water cured for a minimum of 7 days after casting.
7. The floor shall receive a light broom finish.
HIPP ENGINEERING AND CONSULTING, INC. SECTION 230902
RALEIGH, NC SEQUENCE OF OPERATIONS
PAGE 12 OF 16

NOVOZYMES NORTH AMERICA INC.
FRANKLINTON, NC
SBM TANK ADDITION
B. Core Wall:
H I P P PROJECT #R20162
SECTION 13200
REV. 0
1. The wall shall be constructed utilizing diaphragm and shotcrete with each
conforming to the following:
a. Diaphragm Erection:
1) The diaphragm shall be protected against damage before, during, and
after erection. Nail or other holes shall not be made in the diaphragm
for erection except in the top 3 inches. Holes shall not be made in the
diaphragm except for inserting wall pipes or sleeves, reinforcing steel,
bolts, or other special appurtenances. Such penetrations shall be
sealed with an epoxy sealant which complies with Section 2.8 Epoxy.
b. Shotcrete:
1) All shotcrete shall be applied by or under direct supervision of
experienced nozzlemen certified by the American Concrete Institute
(ACI) as outlined in ACI certification publication CP-60.
2) Each shotcrete layer shall be broomed prior to final set to effect
satisfactory bonding of the following layer.
3) No shotcrete shall be applied to reinforcing steel or diaphragm that is
encrusted with overspray.
4) No less than '/8" thick shotcrete shall separate reinforcing steel and
prestressing wire.
5) The diaphragm shall be encased and protected with no less than 1" of
shotcrete in all locations.
6) The interior shotcrete shall receive a light broom finish.
C. Curing:
1) Interior and exterior portions of the shotcrete wall shall be water cured
for a minimum of 7 days or until prestressing is completed.
C. Epoxy Injection:
1. Epoxy injection shall be carried out from bottom to top of wall using a pressure
pumping procedure.
2. Epoxy injection shall proceed only after the diaphragm has been fully encased,
inside and outside, with shotcrete.
D. Prestressing:
1. The initial tension in each wire shall be read and recorded to verify that the total
aggregate force is no less than that required by the design. Averaging or
estimating the force of the wire on the wall shall not be considered satisfactory
evidence of correct placement of prestressing wires.
HIPP ENGINEERING AND CONSULTING, INC. SECTION 230902
RALEIGH, NC SEQUENCE OF OPERATIONS
PAGE 13 OF 16

NOVOZYMES NORTH AMERICA INC.
FRANKLINTON, NC
SBM TANK ADDITION
H I P P PROJECT #R20162
SECTION 13200
REV. 0
2. Placement of the prestressing steel wire shall be in a continuous and uniform helix
of such pitch as to provide in each lineal foot of core wall height an initial force and
unit compressive force equal to that shown on the design drawings. Splicing of
the wire shall be permitted only when completing the application of a full coil of
wire or when removing a defective section of wire.
3. Shotcrete shall be used to completely encase each individual wire and to protect
it from corrosion. To facilitate this encasement, the clear space between adjacent
wires is to be no less than one wire diameter.
4. Prestressing shall be accomplished by a machine capable of continuously inducing
a uniform initial tension in the wire before it is positioned on the tank wall. Tension
in the wire shall be generated by methods not dependent on cold working or re-
drawing of the wire. In determining compliance with design requirements, the
aggregate force of all tensioned wires per foot of wall shall be considered rather
than the force per individual wire, and such aggregate force shall be no less than
that required by the design and as shown on approved drawings.
5. The tank construction company shall supply equipment at the construction site to
measure tension in the wire after it is positioned on the tank wall. The stress
measuring equipment shall include: electronic direct reading stressometer
accurate to within 2%, calibrated dynamometers and a test stand to verify the
accuracy of the equipment.
6. After circumferential prestressing wires have been placed, they shall be protected
by encasement in shotcrete. This encasement shall completely encapsulate each
wire and permanently bond the wire to the tank wall.
7. When multiple layers of wire are required, shotcrete cover between layers shall be
no less than '/8" thick.
E. Covercoat:
1. After all circumferential prestressing wires have been placed, a shotcrete cover
having a thickness of no less than 1" shall be placed over the prestressing wires.
2. Horizontal sections of the wall shall form true circles without flat areas, excessive
bumps or hollows.
3. The covercoat shall receive a sliced trowel finish.
F. Wall Openings:
All wall pipes, sleeves and manholes passing through the wall shall be sealed to
the diaphragm by epoxy injection.
G. Coatings:
No coatings required.
HIPP ENGINEERING AND CONSULTING, INC. SECTION 230902
RALEIGH, NC SEQUENCE OF OPERATIONS
PAGE 14 OF 16

NOVOZYMES NORTH AMERICA INC.
FRANKLINTON, NC
SBM TANK ADDITION
3.3 FIELD QUALITY CONTROL
A. Inspection and Testing:
Concrete and Shotcrete Testing:
a. Compression Tests:
H I P P PROJECT #R20162
SECTION 13200
REV. 0
1) Compression test specimens shall be taken during construction from
the first placement of each class of concrete specified herein and at
intervals thereafter as selected by the Engineer to insure continued
compliance with these Specifications. At least one set of test
specimens shall be made for each 50 yards of concrete/shotcrete
placed. Each set of test specimens shall be a minimum of 5 cylinders.
2) Compression test specimens for concrete/shotcrete shall conform to
ASTM C172/C172M for sampling and ASTM C31/C31 M for making
and curing test cylinders. Test specimens shall be 6-inch diameter by
12-inch high or 4-inch diameter by 8-inch high cylinders.
3) Compression test shall be performed in accordance with ASTM
C39/C39M. Two test cylinders will be tested at 7 days and two at 28
days. The remaining cylinder will be held to verify test results, if
needed.
b. Air Content Tests (concrete only):
1) Air content tests shall conform to ASTM C231 /C231 M (Pressure
Method for Air Content).
2) Tests for air content shall be made prior to concrete placement and
whenever compression test specimens are made.
C. Slump Tests (concrete only):
1) Slump tests shall be made in accordance with ASTM C143/C143M.
2) Slump tests shall be made whenever compression test specimens are
made.
2. Hydrostatic Testing:
a. The tank shall be tested for watertightness upon completion.
b. The testing for watertightness shall be completed as follows:
1) Fill the tank with water to the maximum water level and let it stand for
a minimum of 24 hours.
2) Inspect the exterior of the tank wall and footing for damp spots. Damp
spots shall be defined as spots where moisture can be picked up on a
dry hand, the source of which is from inside the tank.
3) Leakage through the wall or wall -base joint shall be repaired and the
tank shall be retested using the above procedure.
HIPP ENGINEERING AND CONSULTING, INC. SECTION 230902
RALEIGH, NC SEQUENCE OF OPERATIONS
PAGE 15 OF 16

NOVOZYMES NORTH AMERICA INC.
FRANKLINTON, NC
SBM TANK ADDITION
3.4 CLEANING
H I P P PROJECT #R20162
SECTION 13200
REV. 0
A. The interior of the tank shall be cleaned to remove debris, construction items, and
equipment prior to testing and disinfection.
END OF SECTION 13200
HIPP ENGINEERING AND CONSULTING, INC. SECTION 230902
RALEIGH, NC SEQUENCE OF OPERATIONS
PAGE 16 OF 16

Submersible Pump Data Sheet
pip?
HIPP EICC.IM EERINC,
& CONSII"IN� INS_
Equipment Names : SBM Loadout Pump
Quantity: 1
Equipment Numbers : FLF96DP0l
Issued for Construction, Rev. 0
Client: Novoz mes
04MAR2021
Project: SBM Tank Addition
Project #R20162
Design Criteria
Pumped Fluid
Sent Biomass Wastewater
Maximum Temperature de F
120
Minimum Temperature de F
20
Design Specific Gravity
1.15
Design Viscosity c
1.00
Design pH
11.5-12.5
Design Capacity GPM
925
Developed Head TDH feet of pumped liquid)
25
NPSHn feet of pumped liquid)
2
Casing Material
* See Note 4
Shaft Material
* See Note 4
Finish of Wetted Surfaces
* See note 4
Seal
Mechanical internal slurry seal
Unit Design
Manufacturer
Vulcan
Model Number
HDS 200L-A
Maximum Impeller Diameter
Selected Impeller Diameter
Motor
Submersible, 15HP
Electrical
460V / 3 / 60Hz
Service Factor
1.15
Motor Speed (rpm)
900
Suction Size / Type
Discharge Size / Type
6" / Flange
Frame
Seal Manufacture / Model No.
NPSHR feet of pumped liquid)
Operating Efficiency %
Notes and Other Design Requirements
1. (*) indicates data required from vendor.
2. Refer to P&ID FAA72963-U502986.
3. Installation type is semi -permanent, wet.
4. Vendor to ensure construction is able to withstand chloride concentration of 1300 PPM; provide coating
for pump, motor, and other wetted parts as required.
5. Vendor to provide long radius discharge elbow, rail guides, and mounts material or coating as required
to withstand high chloride concentration. Installation contractor to provide 3" rails at required length as
specified on structural drawings.

Centrifugal Pump Data Sheet
pip?
HIPP EKC.IM EERINC
S IJN,II"INU- INS_
Equipment Names : SBM Recirculation Pump
Quantity: 1
Equipment Numbers : FLF96DP02
Issued for Construction, Rev. 0
Client: Novoz mes
04MAR2021
Project: SBM Tank Addition
Project #R20162
Desian Criteria
Pumped Fluid
Sent Biomass Wastewater
Maximum Temperature de F
120
Minimum Temperature de F
20
Design Specific Gravity
1.15
Design Viscosity c
1.00
Design pH
11.5-12.5
Design Capacity GPM
1450
Developed Head TDH feet of pumped liquid)
145
NPSHn feet of pumped liquid)
16
Casing Material
* See Note 3
Shaft Material
* See Note 3
Finish of Wetted Surfaces
* See Note 3
Seal
Single Mechanical water purge)
Unit Desian
Manufacturer
Goulds
Model Number
JC 4J 6x6-14HS/5V
Maximum Impeller Diameter
Selected Impeller Diameter
Motor
Severe Duty, 125 HP
Electrical
460V / 3 / 60Hz
Service Factor
1.15
Motor Speed (rpm)
1800
Suction Size / Type
6" / Flange
Discharge Size / Type
6" / Flange
Frame
Seal Manufacture / Model No.
NPSHR feet of pumped liquid)
Operating Efficiency %
Notes and Other Design Requirements
1. (*) indicates data required from vendor.
2. Refer to P&ID FAA72963-U502986.
3. Vendor to ensure construction is able to withstand chloride concentration of 1300 PPM; provide coating
for wetted parts as required.

In -Tank Eductor Data Sheet
III PP FN(.IN IF ER I vr.
.v LJNIJLII,��. IM1L_
Equipment Names : SBM In -Tank Eductors
Quantity: 10
Equipment Numbers : FLF96ED01-10
Issued for Construction, Rev. 0
Client: Novoz mes
04MAR2021
Project: SBM Tank Addition
Project #R20162
Design Criteria
Pumped Fluid
Sent Biomass Wastewater
Maximum Temperature de F
120
Minimum Temperature de F
20
Design Specific Gravity
1.15
Design Viscosity c
1.00
Design pH
11.5-12.5
Particle Size
3-6% solids
Tank Height ft
28
Tank Diameter ft
100
Unit Design
Manufacturer
Jacoby -Tarbox
Model Number
TLA
Connection Size in / type)
2 / *
Material
* See note 4
Motive Flow pm
138 each
Differential Pressure (psig)
50
Discharge Flow pm
689 each
Flow Field ft
65 maximum
Turnover time
Less than 3 hours
Total Number eductors required
10
Notes and Other Design Requirements
1. (*) indicates data required from vendor.
2. Refer to P&ID FAA72963-U502986.
3. Vendor to provide 8" manifold ring design for eductors.
4. Vendor to provide material or coating for ring and eductors as necessary to ensure construction is able
to withstand a chloride concentration of 1300 PPM and an abrasive environment.
5. Vendor to provide support sizing requirements for manifold ring to tank vendor and installing contractor.

ENGINEERS
3100 SMOKETREE COURT, SUITE 800
RALEIGH, NC 27604
Tel:[phone] Fax:[phone]
novozymes.- J
*
Rethink Tomorrow
NOVOZYMES
FRANKLINTON, NC
MASTER SPECIFICATIONS
PPS Job No. 130805WT
CONSTRUCTION SPECIFICATIONS
FOR
ABOVEGROUND PIPING
SPECIFICATION NO.
130805-31-001
THIS TITLE SHEET IS THE FIRST PAGE OF THE SPECIFICATION AND IS A RECORD OF EACH ISSUE OR
REVISION.
REV
DATE
BY
CK
APPROVALS
PAGES
REMARKS
DEPT
PROJ.
CLIENT
DATE
A
12-16-03
JES
MAC
As Noted
® ENTIRE SPECIFICATION ISSUED
THIS REVISION
❑ REVISED PAGES ONLY ISSUED
THIS REVISION
SPECIFICATION ISSUED FOR
❑ IN HOUSE REVIEW ❑ PURCHASE
® CLIENT APPROVAL ❑ CONSTRUCTION
❑ INQUIRY/BID
1:1sk1/_\
FOR REFERENCE ONLY

Construction Specifications For
Aboveground Piping
Master Specification n y`
Novozymes, Franklinton, NC
Rethink Tomorrow
17000TC - TABLE OF CONTENTS
SECTION TITLE REV. DATE
17000 PIPING SPECIFICATIONS
17002 MEDIA SERVICE INDEX 12-13-13
17003.xxx PIPING SPECIFICATIONS SEE INDEX
17003.Bxxxx BRANCH CONNECTION TABLES 12-13-13
I:1Skv%\
FOR REFERENCE ONLY

MEDIA INDEX
n y 11 *
Rethink Tomorrow
PIPE
MEDIA DESCRIPTION
AREA
SPEC
SYMBOL
NOTES
AIR, COMPRESSED - 304L SS TUBING
Fermentation
400
A
AIR, EXHAUST - 304L SS TUBING
Fermentation
401
AE
Recovery
PIPE ' =
Granulation
AIR, FERMENTATION - CARBON STEEL
Fermentation
110
AF
AIR, INSTRUMENT (FILTERED) - CARBON STEEL
Utilities
55
Al
Fermentation
Recovery
-
Granulation
AIR, PLANT - CARBON STEEL
Utilities
55
AP
Fermentation
AIR, VACUUM -
Recovery
401
AZ
Granulation
Fermentation
380
NH3
AMMONIA - CARBON STEEL
PIPE LABEL=>"AMMONIA" - BLACK ON YE
BLOWDOWN - CARBON STEEL
Utilities
100
BD
BROTH - 316L SS - TUBING
Recovery
460
B
Fermentation
Granulation
PIPE •BROTH"
REV FOR REF- FENCE ONLY] Page 'ofe

MEDIA INDEX
- j
novozymes-
Rethink Tomorrow
PIPE
MEDIA DESCRIPTION
AREA
SPEC
SYMBOL
NOTES
CLEAN IN PLACE - 316L SS - TUBING
Sitewide
460
CIP
PIPE LABEL=>"CIP" - WHITE on PURPLE
CONCENTRATE - 316L SS - TUBING
Recovery
460
CONC
PIPE LABEL=>"CONC" - BLACK on WHITE
CONDENSATE - 150 PSIG - CARBON STEEL
Sitewide
100
C
PIPE • i
CORN STEEP LIQUOR - 316L SS
Fermentation
451
CSL
SEWER, SANITARY -
SS
PIPE LABEL=>"SANITARY SEWER" - BLACK on WHITE
DRAIN, STORM - CARBON STEEL
SD
GLUCOSE
Fermentation
GLUC
Recovery
CHILLED GLYCOL WATER - SUPPLY - CARBON STEEL
Utilities
110
CGWS
Fermentation
Recovery
_ • •, ,
CHILLED GLYCOL WATER - RETURN - CARBON STEEL
Utilities
110
CGWR
Fermentation
Recovery
PIPE As •
ON
REV A
FOR REFERENCE ONLY
Page 2 of 8

MEDIA INDEX
n y 11 *
Rothtnk Tomorrow
PIPE
MEDIA DESCRIPTION
AREA
SPEC
SYMBOL
NOTES
NITRIC ACID - 316L SS - TUBING
Recovery
460
HNO3
CLASS V
Granulation
PIPE LABEL=>"NITRIC ACID - BLACK on WHITE
GAS, NATURAL (FUEL) - CARBON STEEL
Utilities
320
NG
Fermentation
PIPE LABEL=>"NATURAL GAS" - BLACK ON YELLOW
OIL, ANTIFOAM - 304L SS
Fermentation
401
OAF
PIPE LABEL=>"ANTIFOAM OIL" - BLACK on YELLOW
OIL, FUEL - CARBON STEEL
Utilities
320
OF
PIPE LABEL=>"FUEL OIL -RETURN" - BLACK on
YELLOW
PHOSPHORIC ACID (FOOD GRADE) - 10% - 316L SS
Fermentation
451
HPO
Recovery
PIPE LABEL=>"PHOSPHORIC ACID - BLACK on
YELLOW
POTASSIUM HYDROXIDE (CAUSTIC) - CARBON STEEL
Fermentation
200
KOH
PIPE LABEL=>"POTASSIUM HYDROXIDE" - BLACK on
YELLOW
PERLITE -
Recovery
412
PRC
Granulation
PIPE LABEL=>"PERLITE" — WHITE on BLACK
PRECOAT - 316L SS - TUBING
f
Recovery
460
PRC
PIPE LABEL=>"PRECOAT" - WHITE on BLACK
PROCESS SLUDGE - 316L SS - TUBING
Recovery
460
PS
PIPE •_PROCESS SLUDGE"
- WHITE on BLACK
REV A
FOR REFERENCE ONLY
Page 3 of 8

MEDIA INDEX
n y 11 *
Rethink Tomorrow
MEDIA DESCRIPTION
AREA
PIPE
SPEC
SYMBOL
NOTES
PRODUCT - 316L SS - TUBING
Recovery
460
PROD
PIPE LABEL=>"PRODUCT" - WHITE on BLACK
SPENT BIOMASS - 304L SS - TUBING
Sitewide
412
SBM
SPENT BIOMASS - HDPE
Sitewide
36
SBM
BIOMASS"PIPE LABEL=>"SPENT
STEAM, HIGH PRESSURE (8 bar, 115 psig) - CARBON
STEEL
Utilities
Fermentation
Recovery
Granulation
100
SH
STEAM, MEDIUM PRESSURE (3 bar, 45 psig) - CARBON
STEEL
Fermentation
Recovery
Granulation
100
SM
LABEL=>"MP STEAM" - WHITE ON
STEAM, MEDIUM PRESSURE - BOILING - CARBON
STEEL
Fermentation
100
SMB
STEAM, MEDIUM PRESSURE - STERILIZATION -
CARBON STEEL
Fermentation
100
SMS
STERILIZATIONPIPE LABEL=>"MP ON
STEAM, MEDIUM PRESSURE - STERILIZATION - 316L SS
- TUBING
PIPE •c • ON
GREEN
Fermentation
402
SMS
RE A IFOR REFERENCE ONLY Page •ofe

MEDIA INDEX
n y 11 *
Rethink Tomorrow
MEDIA DESCRIPTION
AREA
PIPE
SPEC
SYMBOL
NOTES
STEAM, LOW PRESSURE (1 bar, 15 psig)- CARBON
STEEL
Fermentation
Recovery
Granulation
100
SL
PIPE • ON
GREEN
SUBSTRATE, NON -STERILE - 304L SS - TUBING
Fermentation
403
SUNS
PIPE A_NON-STERILE" - WHITE on
BLACK
SUBSTRATE, STERILE - CARBON STEEL
Fermentation
403
SUS
PIPE LABEL=>"SUBSTRATE STERILE" - WHITE on
BLACK
SUCROSE - 304L SS - TUBING
Fermentation
400
SUC
SUCROSE - 304L SS
Fermentation
401
SUC
SUCROSE - 316L SS
Fermentation
461
SUC
ROSE"
WATER, BOILER FEED - CARBON STEEL
102
WBF
PIPE Ac :• ON
GREEN
WATER, CHILLED (NON -PROCESS) - SUPPLY - CARBON
STEEL
Fermentation
Recovery
Granulation
110
CCWS
PIPE LABEL=>"CHILLED WATER -SUPPLY" - WHITE ON
GREEN
RE A IFOR REFERENCE ONLY' Page
SOfe

MEDIA INDEX
- j
novozymes-
Rethink Tomorrow
MEDIA DESCRIPTION
AREA
PIPE
SPEC
SYMBOL
NOTES
WATER, CHILLED (NON -PROCESS) - RETURN - CARBON
STEEL
Fermentation
Recovery
Granulation
110
CCWR
WATER, CITY (POTABLE DRINKING) - CARBON STEEL
Utilities
Fermentation
Recovery
Granulation
Waste Mgmt
Labs
55
WC
PIPE ' ON
WATER, COOLING (NON -PROCESS) - SUPPLY -
CARBON STEEL
Utilities
Fermentation
Recovery
Granulation
110
CWS
PIPE LABEL=>"CHILLED WATER -SUPPLY" - WHITE on
WATER, COOLING (NON -PROCESS) - RETURN -
CARBON STEEL
Utilities
Fermentation
Recovery
Granulation
110
CWR
PIPE ' =
WATER, DEMINERALIZED
WD
PIPE LABEL=>"DEMINERALIZED WATER" -WHITE ON
GREEN
WATER, FIRE - CARBON STEEL
FW
PIPE LABEL=>"FIRE WATER" — WHITE on RED
REV A
FOR REFERENCE ONLY
Page 6 of 8

MEDIA INDEX
n y 11 *
Rethink Tomorrow
MEDIA DESCRIPTION
AREA
PIPE
SPEC
SYMBOL
NOTES
WATER, HOT HEATING - SUPPLY - CARBON STEEL
Sitewide
100
HHWS
PIPE •
WHITE ON -
WATER, HOT HEATING - RETURN - CARBON STEEL
PIPE •
WHITE ON -
Sitewide
100
HHWR
WATER, PRESSURIZED PLANT -
Recovery
Granulation
102
WPP
•
WATER, PRESSURIZED PLANT -
Recovery
Granulation
412
WPP
PIPE LABEL=>"PRESSURIZED PLANT WATER" -WHITE
ON GREEN
WATER, PROCESS WASTE - CARBON STEEL
Aboveground
401
WWP
PIPE -• ON
GREEN
WATER, PROCESS WASTE - HDPE
-• ON -
GREEN
Belowground
Pressurized
36
WWP
WATER, PROCESS WASTE - PVC
Belowground
Gravity
30
WWP
PIPE -• ON
GREEN
WATER, SOFTENED - PVC
_►-» • •
Utilities
Fermentation
30
INS
WATER, PLANT (PROCESS)
Wp
PIPE • ON
REV A
Page 7of8
FOR REFERENCE ONLY

MEDIA INDEX
novozymes-
Rethink Tomorrow
PIPE
MEDIA DESCRIPTION
AREA
SPEC
SYMBOL
NOTES
WATER, HOT PLANT WATER (PROCESS)
WPH
PIPE A_ • ON
REV A
FOR REFERENCE ONLY
Page 8 of 8

PIPING SPEC NO: 30
- I i
novozymesm
Rethink Tomorrow
SERVICE: Refer to Piping Media Service Index
BASIC MATERIAL: Polyvinyl Chloride (PVC)
RATING CLASS: 0-100 PSIG, 30' F to 70' F, Max.
Temp. = 140° F, See Mfg's Rating for allowable pressure
in 73° F to 140° F Range
Corrosion Allowance: NA
Mechanical Strength: NA
Bending Allowance: NA
DESIGN BASIS - ASME B31.3
2" and smaller:
3" thru 16":
280 PSIG @ 70 DEGF
220 PSIG @ 70 DEGF
174 PSIG @ 100 DEGF
136 PSIG @ 100 DEGF
143 PSIG @ 110 DEGF
112 PSIG @ 110 DEGF
112 PSIG @ 120 DEGF
88 PSIG @ 120 DEGF
87 PSIG @ 130 DEGF
68 PSIG @ 130 DEGF
62 PSIG @ 140 DEGF
48 PSIG @ 140 DEGF
• Class 150 PVC flange rating is limiting design factor
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
PIPE
ASTM D 1785, PVC TYPE I,
1/2" thru 2"
SCH 80
Welded
Grade 1 (12454-B PER
ASTM D 1784
ASTM D 1785, PVC TYPE I,
3" thru 16"
SCH 40
Welded
Grade 1 (12454-B PER
ASTM D 1784
FLANGES
ASTM D 2467, PVC TYPE I,
1/2" thru 16"
CLASS 150
Socketweld
Grade 1 (12454-B PER
RF
ASTM D 1784), DRILLING
PER ASME B16.5
ASTM D 2467, PVC TYPE I,
1/2" thru 16"
CLASS 150
Blind
Grade 1 (12454-13 PER
FF
ASTM D 1784), DRILLING
PER ASME B16.5
FITTINGS
Cemented
ASTM D 2467, PVC TYPE I,
1/2" thru 2"
SCH 80
Socket Type
Grade 1 (12454-B PER
ASTM D 1784
Cemented
ASTM D 2467, PVC TYPE I,
3" thru 16"
SCH 40
Socket Type
Grade 1 (12454-B PER
ASTM D 1784
UNIONS
Cemented
ASTM D 2467, PVC TYPE I,
1/2" thru 2"
SCH 80
Socket Type
Grade 1 (12454-B PER
ASTM D 1784
BOLTING
ASTM A 307, Grade B
ALL
_
Hex Bolts &
Nuts
FOR REFERENCE ONLY
1 of 2

PIPING SPEC NO: 30
n * Lym4
Rethink Tomorrow
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
GASKETS
PTFE
1/8" thick, 60-70 Shore A
ALL
-
Bonded to
Durometer
EDPM
JOINT
Primer
MATERIALS
ALL
Cement
BALL
VALVES
1/2" thru 4"
-
Socketweld
PVC, EPT "O" Rings
CHECK
1/2" thru 3"
-
Socketweld
PVC, Ball Type
VALVES
4"thru 6"
CLASS 150
Flanged
PVC, FF, Swing Type
GLOBE
1/2" thru 2"
-
Socketweld
PVC, EDPM Seal
VALVES
NOTES
1) See Mfg's recommendation for assembly of flanged connections.
2) See Branch Table BTFIT.
FOR REFERENCE ONLY
2of2

PIPING SPEC NO: 31
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novozymesm
Rethink Tomorrow
SERVICE: Refer to Piping Media Service Index
BASIC MATERIAL: Fiberglass Reinforced Plastic (FRP) — Filament Wound, Resin is Aromatic Amine Epoxy
RATING CLASS: 0-55 PSIG, 195' F Max. & 150 PSIG, 120' F, Not for Air or Compressed Air
Corrosion Allowance: NA
Mechanical Strength: NA
Bending Allowance: NA
DESIGN BASIS - ASME B31.3
Maximum allowable working pressure
-temperature rating for pipe sizes 12" and smaller as follows:
NOTE: Pressure -temperature ratings for pipe and fittings are limited by the service.
Consult with the resin manufacturer for maximum temperature and vacuum rating
for the service being used.
150 psig at 180 degrees F.
150 psig at 200 degrees F.
<= High temperature resin is required
• Safety factor for pressure is 10:1
• Safety factor for vacuum is 5:1
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
PIPE
1" thru 12"
-
Socketweld
FRP, ASTM D 2996
FLANGES
FF
1" thru 1 1/2"
-
Compression
FRP
Molded
8" thru 12"
-
Spray -up
FRP
FITTINGS
1" thru 6"
-
Compression
FRP
Molded
BOLTING
ALL
-
Hex Bolts &
ASTM A 307, Grade B
Nuts
GASKETS
ALL
-
FF Buna-N
1/8" thick, 60-70 Shore A
Durometer
ADHESIVE
ALL
Epoxy
BUTTERFLY
VALVES
FRP Body with TFE Liner
2" thru 6"
_
_
and TFE Covered Disc, with
D.I. Notched, Throttling
Handle
FRP Body with TFE Liner
8" thru 12"
and TFE Covered Disc, with
—
Geared Handwheel Operator
BALL
VALVES
1" thru 4"
CLASS 150
FF
CPVC Body
FOR REFERENCE ONLY
1 of 2

PIPING SPEC NO: 31
novozymes-
Rethhk Tomorrow
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
CHECK
VALVES
1" thru 8"
CLASS 150
FF
PVDF with TFE Seat & Seal,
Swing Type
2
101,
CLASS 150
FF
All PVC
3
CPVC with PVDF Ball &
1" thru 3"
CLASS 150
FF
EDPM Seat & Seal, Ball
Type, Single Union
NOTES
1) See Mfg's recommendation for assembly of flanged
connections.
2) Rating varies according to size from 85 PSIG at 210°F Max. to 40 PSIG at 210' Max.
3) Maximum Rating is 50 PSIG at 70°F.
FOR REFERENCE ONLY
2of2

PIPING SPEC NO: 36
n * Lym4
Rethink Tomorrow
SERVICE: Refer to Piping Media Service Index
BASIC MATERIAL: High Density Polyethylene (HDPE)
RATING CLASS: 0-80 PSIG @ 73°F Max.
Corrosion Allowance: NA
Mechanical Strength: NA
Bending Allowance: NA
DESIGN BASIS - ASME B31.3
Maximum allowable working pressure -temperature rating for pipe sizes 36" and smaller as follows:
NOTE: Consult with the HDPE manufacturer.
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
PIPE
HDPE, IPS, Type III, PE
1/2" thru 6"
-
PE
3408, SDR 21, ASTM D-
3035
8" thru 36"
-
PE
HDPE, IPS, Type III, PE
3408, SDR 21, ASTM F-714
FLANGE
HDPE, Molded, IPS, PE
ADAPTERS
2" thru 36"
-
Butt Type
3408, SDR 21, ASTM D-
3261
LAP JOINT
2" thru 36"
CLASS 150
CS Lap Joint Flange, ANSI
FLANGES
B16.5
FITTINGS
1/2" thru 2"
-
Socket Type
HDPE, Molded, IPS, PE
3408, ASTM D-2683
HDPE, Molded, IPS, PE
3" thru 8"
Butt Type
3408, SDR 21, ASTM D-
3261
Fabricated from HDPE, IPS
Heavy Wall, Machined to
10" thru 36"
Butt Type
Match System Pipe, Full
Pressure Rated, PE 3408,
ASTM F-714
BOLTING
ALL
_
Hex Bolts &
ASTM A 307, Grade B
Nuts
NOTES
1) All pipe and fittings to be joined by heat fusion per manufacturer's specification.
FOR REFERENCE ONLY
1 of 1

PIPING SPEC NO: 55
n m -
Rethhk Tomorrow
SERVICE: Refer to Piping Media Service Index
BASIC MATERIAL: GALVANIZED CARBON STEEL
RATING CLASS: 0-125 PSIG, 200' F Max.
Corrosion Allowance:.025"
Mechanical Strength:.065"
Bending Allowance: 8% reduction for 5-diameter bends
DESIGN BASIS - ASME B31.1
285 PSIG @ 100 DEGF
260 PSIG @ 200 DEGF
230 PSIG @ 300 DEGF
200 PSIG @ 400 DEGF
170 PSIG @ 500 DEGF
140 PSIG @ 600 DEGF
125 PSIG @ 650 DEGF
110 PSIG @ 700 DEGF
95 PSIG @ 750 DEGF
• Class 150 flange rating is limiting design factor
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
PIPE
1/4" thru 6"
SCH 40
Welded
Galv., ASTM A 53, Gr B,
T&C, B16.10M
FLANGES
3" thru 6"
CLASS 125
FF, D.I.
Galv., ASTM A 105,
1,2
Threaded
B16.5
FITTINGS
1/4" thru 6"
CLASS 3000
Screwed
Galv., FS, ASTM A 105,
B16.11
UNIONS
1/4" thru 2"
CLASS 3000
Screwed
Galv., FS, ASTM A 105
PLUGS
Threaded,
Galv., ASTM A 105,
1/4" thru 3"
-
Solid Square
B16.11
Head
BOLTING
Bolts, Cap
ASTM A 307, Grade B
ALL
-
Screws,
Studs
GASKETS
ALL
CLASS 150
FF
1/16" Neoprene
BALL
Bronze Body and Chromium
VALVES
1/4" thru 3"
CLASS 150
Screwed
Plated Ball with 1 '/4" Ext.
Stem, ASTM B62
BUTTERFLY
Screwed,
Cl body, Aluminum -Bronze
VALVES
3" thru 6"
CLASS 125
Wafer
Disc, Buma-N Seat, 316SS
Stem with Lever Handle
CHECK
Bronze body and Spring
VALVES
1/4" thru 3"
CLASS 125
Screwed
Loaded Reinforced TFE Ball -
Cone
3" thru 6"
CLASS 125
Screwed,
Cl body, Buna-N Seal
Wafer
FOR REFERENCE ONLY
1 of 2

PIPING SPEC NO: 55
novozymes-
Rethink Tomorrow
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
GATE
Bronze body, Union Bonnet,
VALVES
1/2" thru 2"
CLASS 150
Threaded
Inside Screw, Traveling
Stem, Solid Wedge
Forged Cl body, Solid
2 1/2" thru 6"
CLASS 125
FF, Flanged
Wedge, Bronze Seat Rings,
OS&Y, Rising Stem
NOTES
1)
Schedule of fittings and the bore of weldneck or socketweld flanges shall be same as attached pipe.
2)
Use Teflon tape for threaded joints.
3)
See Branch Table BTSOL.
4)
Butterfly valves do not require gaskets
5)
Not for flammable service.
FOR REFERENCE ONLY
2of2

PIPING SPEC NO: 100
novozymesm
Rethink Tomorrow
SERVICE: Refer to Piping Media Service Index
BASIC MATERIAL: CARBON STEEL
RATING CLASS: 0-125 PSIG, 353' F Max.
Corrosion Allowance:.025"
Mechanical Strength:.065"
Bending Allowance: 8% reduction for 5-diameter bends
DESIGN BASIS - ASME B31.1
285 PSIG @ 100 DEGF
260 PSIG @ 200 DEGF
230 PSIG @ 300 DEGF
200 PSIG @ 400 DEGF
170 PSIG @ 500 DEGF
140 PSIG @ 600 DEGF
125 PSIG @ 650 DEGF
110 PSIG @ 700 DEGF
95 PSIG @ 750 DEGF
• Class 150 flange rating is limiting design factor
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
PIPE
1/2" thru 1 1/2"
XS
Welded
ASTM A 53, Gr B, T&C,
B16.10M
2"
XS
Seamless or
ASTM A 53, Gr B, PE,
Welded
B36.10M
2 1/2" thru 16"
STD
Seamless or
ASTM A 53, Gr B, PE,
Welded
B36.10M
FLANGES
1/2" thru 2"
CLASS 150
Threaded
ASTM A 105,
1,2,3
RF
B16.5
2 1/2" thru 16"
CLASS 150
Weldneck
ASTM A 105,
1,3
RF
B16.5
FITTINGS
1/2" thru 2"
CLASS 3000
Socketweld
ASTM A 105,
B16.11
2 1/2" thru 16"
STD
Buttweld
ASTM A 234 Grade WPB,
1
B16.9
UNIONS
With spiral wound Type 316
1/2" thru 2"
CLASS 3000
Socketweld
SS gasket and retainer ring,
"GRAPHITE" filler, ASTM A
105
PLUGS
Threaded,
ASTM A 105,
1/2" thru 2"
-
Solid Square
B16.11
Head
BOLTING
Bolts, Cap
ASTM A 307, Grade B,
ALL
-
Screws,
Studs
GASKETS
Spiral Wound with Graphite
1/2" thru 16"
CLASS 150
Ring Type
Filler
REV A
FOR REFERENCE ONLY
1 of 2

PIPING SPEC NO: 100
n m -
Rethink Tornorrow
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
STEAM
1/2" to 3/4"
250#
Cl Inverted
Integral Strainer, Internal
TRAPS
Bucket
Check Valve
1"to 1 1/4"
250#
Cl Inverted
Integral Strainer, Internal
Bucket
Check Valve
1/2" to 3/4"
-
Thermo-
For Driplegs & Outdoors
dynamic
Y-STRAINER
1/2" thru 3"
250#
Screwed
Cl w/.045" Perforated 304 SS
Screen
BALL
1/2" thru 2"
250#
Screwed
Bronze Body with 316 SS
VALVES
Ball & 2-1/4" Stem Ext.
CHECK
VALVES
1/2" thru 2"
150#
Screwed
Bronze Body, Swing Check
2" thru 12"
125#
FF, Flanged
g
IBBM Swing Check, Bronze
disk
GATE
1/2" thru 2"
150#
Screwed
Bronze Body, Union Bonnet
VALVES
Solid Wedge
2 1/2" thru 12"
125#
FF, Flanged
g
IBBM for Steam, OS&Y, (8"-
12 with By -Pass Attached
GLOBE
1/2" thru 2"
150#
Screwed
Bronze Body, SS Plug Disc &
VALVES
Seat Ring
1/2 thru 2"
800#
Socketweld
F.S., O.S. & Y. 13% Cr.
Trim, H.F. Seat
2 1/2" thru 10"
125#
FF, Flanged
IBBM, OS&Y, Renewable
Disc & Seat Ring
PLUG
Wrench Operated Plug,
VALVES
1/2" thru 2"
200#
Screwed
Screwed Gland Type,
Regular Pattern
Wrench Operated Plug,
2 1/2' thru 4"
200#
FF, Flanged
Screwed Gland Type,
Reg.Pattern,125# Flg.
Drilling.
Worm Gear Operated Plug,
6" thru 16"
200#
Flanged
Bolted Gland Type, Regular
Pattern,125# Fig. Drilling
NOTES
1) Schedule of fittings and the bore of weldneck or socketweld flanges shall be same as attached pipe.
2) Use Teflon tape for threaded joints.
3) Flange facing shall be "RAISED FACE" or as required to match the mating flange.
4) See Branch Table BTSOL.
5) Ball valves for on -off service only.
FOR REFERENCE ONLY
2of2

PIPING SPEC NO: 102
novozymesm
Rethink Tomorrow
SERVICE: Refer to Piping Media Service Index
BASIC MATERIAL: CARBON STEEL
RATING CLASS: 600 PSIG, 500' F
Corrosion Allowance:.025"
Mechanical Strength:.065"
Bending Allowance: 8% reduction for 5-diameter bends
DESIGN BASIS - ASME B31.1
740 PSIG @ 100 DEGF
675 PSIG @ 200 DEGF
655 PSIG @ 300 DEGF
635 PSIG @ 400 DEGF
600 PSIG @ 500 DEGF
550 PSIG @ 600 DEGF
535 PSIG @ 650 DEGF
535 PSIG @ 700 DEGF
505 PSIG @ 750 DEGF
• Class 300 flange rating is limiting design factor
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
PIPE
1/2" thru 2"
XS
Seamless
ASTM A 106 or A 53, Gr B,
T&C, B16.10M
2" thru 6"
XS
Seamless
ASTM A 106 or A 53, Gr B,
PE, B36.10M
FLANGES
Weldneck or
ASTM 6. 105,
1/2" thru 6"
CLASS 300
Slip -On
B16.5
1,2,3
RF
FITTINGS
1/2" thru 2"
3000#
Screwed
ASTM A 105,
B16.3
2 1/2" thru 6"
XS
Buttweld
ASTM A 234 Grade WPB,
1
B16.9
UNIONS
1/2" thru 2"
3000#
Screwed
Steel to Steel seats, ASTM A
197
PLUGS
Threaded,
ASTM A 105,
1/2" thru 2"
-
Solid Square
B16.11
Head
BOLTING
Bolts, Cap
ASTM A 193, Grade B7
ALL
-
Screws,
Studs with ASTM A 194,
Studs
Grade 2H Heavy Hex Nuts,
GASKETS
1/2" thru 16"
CLASS 300
Ring Type
Spiral -Wound Type 304 SS,
with Graphite Filler
Y-STRAINER
Threaded
Steel Body with 40Mesh
1/2" thru 2"
300#
Ends
Perforated 304 SS Screen
Provide NPT blowoff conn
Steel Body with 40Mesh
2 1/2" thru 6"
300#
Flanged
Perforated 304 SS Screen
Provide NPT blowoff conn
FOR REFERENCE ONLY
1 of 2

PIPING SPEC NO: 102
n m -
Rethink Tomorrow
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
BALL
3-Piece CS Body, SS Ball
VALVES
1/2" thru 2"
Class 300
Screwed
and Stem, Polyfill Seats, TFE
Ends
Coated SS Seal, Lever
Handle
CHECK
Horizontal Swing Check, Cast
VALVES
Screwed
Bronze Body and Cover,
1/2" thru 2"
Class 300
Ends
Bronze Disc, Integral Seat,
Not rated for less than 650
PSIG at 350°F, MSS-SP-80
Horizontal Swing Check, Disc
2 1/2" thru 6"
Class 300
Flanged
and Seat to be 13%
Chromium SS, ASME B16.5,
ASME B16.10, ASME B16.34
GATE
Bronze Body, Union Bonnet
VALVES
1/2" thru 2"
Class 300
Screwed
Solid Wedge, Not rated for
Ends
less than 650 PSIG at 350oF,
MSS-SP-80
Cast Steel, OS&Y, Rising
2 1/2" thru 6"
Class 300
FF, Flanged
Stem, for Steam Service,
ASME B16.5, ASME B16.10,
ASME B16.34
GLOBE
Bronze Body, Union Bonnet
VALVES
Plug Type Disc, Disc and
1/2" thru 2"
Class 300
Screwed
Seat to be 13% Chromium
Ends
SS, Not rated for less than
650 PSIG at 350°F, MSS-SP-
80
Cast Steel, OS&Y, Fanged
Bonnet, Renewable Disc &
2 1/2" thru 6"
Class 300
FF, Flanged
Seat Ring, Plug Type Disc,
Disc and Seat to be 13%
Chromium SS, ASME B16.5,
ASME B16.10, ASME B16.34
NOTES
1) Schedule of fittings and the bore of weldneck or socketweld flanges shall be same as attached pipe.
2) Use Teflon tape for threaded joints.
3) Flange facing shall be "RAISED FACE" or as required to match the mating flange.
4) See Branch Table BTSOL.
5) Ball valves for on -off service only.
FOR REFERENCE ONLY
2of2

PIPING SPEC NO: 110
novozymesm
Rethink Tomorrow
SERVICE: Refer to Piping Media Service Index
BASIC MATERIAL: CARBON STEEL
RATING CLASS: 0-125 PSIG, 288' F Max.
Corrosion Allowance:.025"
Mechanical Strength:.065"
Bending Allowance: 8% reduction for 5-diameter bends
DESIGN BASIS - ASME B31.1
285 PSIG @ 100 DEGF
260 PSIG @ 200 DEGF
230 PSIG @ 300 DEGF
200 PSIG @ 400 DEGF
170 PSIG @ 500 DEGF
140 PSIG @ 600 DEGF
125 PSIG @ 650 DEGF
110 PSIG @ 700 DEGF
95 PSIG @ 750 DEGF
• Class 150 flange rating is limiting design factor
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
PIPE
1/2" thru 2"
XS
Welded
ASTM A 53, Gr B, T&C,
B16.10M
2 1/2" thru 30"
STD
Seamless or
ASTM A 53, Gr B, PE,
Welded
B36.10M
FLANGES
1/2" thru 2"
CLASS 150
Threaded,
ASTM A 105,
1,2
FF, F.S.
B16.5
2 1/2" thru 10"
CLASS 150
Weldneck,
ASTM A 105,
1
FF
B16.5
3" thru 30"
CLASS 150
Weldneck
ASTM A 105,
1,3
RF
B16.5
FITTINGS
1/2" thru 2"
CLASS 3000
Threaded
ASTM A 105,
B16.11
2 1/2" thru 30"
STD
Buttweld
ASTM A 234 Grade WPB,
1
B16.9
UNIONS
With spiral wound Type 316
3/8" thru 2"
CLASS 3000
Threaded
SS gasket and retainer ring,
"GRAPHITE" filler, ASTM A
105
PLUGS
Threaded,
ASTM A 395,
3/8" thru 2"
-
Solid Square
B16.11
Head
BOLTING
Bolts, Cap
ASTM A 307, Grade B,
ALL
-
Screws,
Studs
GASKETS
3" thru 30"
CLASS 150
Ring Type
1/16" Thick, Neoprene
1/2" thru 10"
CLASS 150
FF
1/16" Thick, Neoprene
REV A
FOR REFERENCE ONLY
1 of 3

PIPING SPEC NO: 110
n m -
Rethink Tornorrow
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
Y-STRAINER
1/2" thru 2"
250#
Screwed
Cl w/.045" Perforated 304 SS
Screen,
2 1/2", 8"
125#
Flanged, FF
Cl w/.045" Perforated 304 SS
Screen
BUTTERFLY
2-Piece C.I. Body, one piece
VALVES
316 S.S. Stem & Disk, Buna-
1" thru 30"
150#
Wafer
N Resilient Seat, RTFE Lined
S.S. Stem Bearings, 2 1/2" -
4" Lever Operator, 6" - 30"
Gear Operated w/Handwheel
2-Piece C.I. Body, one piece
316 S.S. Stem & Disk, Buna-
N Resilient Seat, RTFE Lined
1" thru 30"
150#
Lug
S.S. Stem Bearings (For
dead end blinding only). 2
1/2" - 4" Lever Operator, 6" -
30" Gear Operated w/
Handwheel
BALL
3-Piece Body, Full Port,
VALVES
Regular Service, 316L Ball &
1/4" thru 2"
150#
Threaded
Stem, Reinforced PTFE
Seats and PTFE Seals,
Threaded ends, S.S. Handle.
CHECK
VALVES
1/2" thru 2"
CLASS 150
Screwed
Bronze Ball -Cone Check
C.I. Wafer Check, Swing
2 1/2" thru 30"
CLASS 125
Wafer
Type w/Return Spring, Buna-
N Seat
GATE
VALVES
1 1/2" thru 2"
CLASS 150
Screwed
Bronze
2'/2" thru 30"
CLASS 125
Flanged, FF
C.I. Body, Br. Trim, OS&Y
GLOBE
Stainless steel globe valve,
VALVES
type 316L stainless steel,
1/2" thru 2"
CLASS 150
Flanged, RF
plug disc, bolted bonnet,
OS&Y, Teflon packing and
gasket
2 1/2" thru 30"
CLASS 125
Flanged, FF
IBBM,C.I.oBody, Br. Trim,
OS&Y 13 /o Chromium SS
PLUG
Cast iron Body, regular
VALVES
pattern plug valve, integral
1/2' thru 2"
200#
Screwed
stop and locking device,
wrench operated, ASTM
A126B.
Cast iron Body, regular
pattern plug valve, integral
stop and locking device,
2 1/2" thru 4"
125#
Flanged, FF
wrench operated, ASTM
A126B.
FOR REFERENCE ONLY
2of3

PIPING SPEC NO: 110
NOTES
n * Lym4
Rethink Tomorrow
1) Schedule of fittings and the bore of weldneck or socketweld flanges shall be same as attached pipe.
2) Use Teflon tape for threaded joints.
3) Flange facing shall be "RAISED FACE" or as required to match the mating flange.
4) See Branch Table BTSOL.
5) Ball valves for on -off service only.
6) Not for flammable service.
FOR REFERENCE ONLY
3of3

PIPING SPEC NO: 200
novozymesm
Rethink Tomorrow
SERVICE: Refer to Piping Media Service Index
BASIC MATERIAL: CARBON STEEL
RATING CLASS: 0-125 PSIG, 200' F Max.
Corrosion Allowance:.025"
Mechanical Strength:.065"
Bending Allowance: 8% reduction for 5-diameter bends
DESIGN BASIS - ASME B31.1
285 PSIG @ 100 DEGF
260 PSIG @ 200 DEGF
230 PSIG @ 300 DEGF
200 PSIG @ 400 DEGF
170 PSIG @ 500 DEGF
140 PSIG @ 600 DEGF
125 PSIG @ 650 DEGF
110 PSIG @ 700 DEGF
95 PSIG @ 750 DEGF
• Class 150 flange rating is limiting design factor
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
PIPE
1/4" thru 2"
XS
Welded
ASTM A 53, Gr B, T&C,
B16.10M
2 1/2" thru 10"
STD
Seamless or
ASTM A 53, Gr B, PE,
Welded
B36.10M
FLANGES
3/4" thru 2"
CLASS 150
Threaded,
ASTM A 105,
1,2,3
RF
B16.5
1/2" thru 2"
CLASS 125
D.I.,
ASTM A 395,
1,2,3
Threaded, FF
B16.5
2 1/2" thru 10"
CLASS 150
Weldneck
ASTM A 105,
1,3
FF
B16.5
2 1/2" thru 10"
CLASS 150
Weldneck
ASTM A 105,
1,3
RF
B16.5
FITTINGS
1/2" thru 2"
CLASS 3000
Screwed
ASTM A 105,
2
B16.11
2 1/2" thru 10"
STD
Buttweld
ASTM A 234 Grade WPB,
1
B16.9
UNIONS
3/8" thru 2"
CLASS 150
Screwed
All iron integral seat
PLUGS
Threaded,
ASTM A 395,
1/4" thru 2"
-
Solid Square
B16.11
2
Head
BOLTING
Bolts, Cap
ASTM A 307, Grade B,
ALL
-
Screws,
Studs
GASKETS
All
CLASS 150
Ring Type,
1/16" Thick, Neoprene
and FF
FOR REFERENCE ONLY
1 of 2

PIPING SPEC NO: 200
n m -
Rethink Tomorrow
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
BUTTERFLY
C.I. Body 316 SS Disc. &
VALVES
2 1/2" thru 4"
150#
Wafer
Stem, Buna-N Seat, With
6
Lever Operator
C.I. Body 316 SS Disc. &
6" thru 10"
150#
Wafer
Stem, Buna-N Seat, With
6
Gear Operator
BALL
Carbon Steel Body, Stainless
VALVES
1/4" thru 2"
2000#/1500#
Screwed
Steel Ball with 1-1/4" SS, Ext.
Stem
CHECK
VALVES
1/2" thru 2"
300#
Screwed
Ductile Iron Body, Swing type
C.I. Wafer Check, Split Type
2 1/2" thru 10"
CLASS 125
Wafer
w/Return Spring, Buna-N
Seat
GATE
All Iron Body, Malleable Iron
VALVES
1 1/2" thru 2"
125#
Screwed
Disc, Non -Asbestos Packing
and Gaskets, ASME B1.20.1
ALL Iron Body, OS&Y, Rising
2'/2" thru 8"
125#
Flanged, FF
Stem, Integral Seats, Non -
Asbestos Packing and
Gaskets
GLOBE
Malleable Iron Body, Nickel
VALVES
1/2" thru 2"
300#
Screwed
Alloy Disc, Seat and Stem
13% Chromium SS, ASME
B1.20.1
All Iron, A126-B Body, Disc
2 1/2" thru 4"
125#
Flanged, FF
B62, Packing and Gasket
Non -Asbestos, Bronze Trim
DIAPHRAGM
Weir Type, Tefzel Lined
VALVES
Ductile Iron Body, With TFE
3/4" thru 3"
150#
Flanged, RF
Lined Ethylene Propylene
7
Diaphragm and Handwheel
Indicator
NOTES
1) Schedule of fittings and the bore of weldneck or socketweld flanges shall be same as attached pipe.
2) Use Teflon tape for threaded joints.
3) Flange facing shall be "RAISED FACE" or as required to match the mating flange.
4) See Branch Table BTSOL.
5) Ball valves for on -off service only.
6) Butterfly valves do not require gaskets.
7) Diaphragm valves installed in horizontal lines shall have valve stem 20' up from the horizontal for
optimum draining.
FOR REFERENCE ONLY
2of2

PIPING SPEC NO: 320
novozymesm
Rethink Tomorrow
SERVICE: Refer to Piping Media Service Index
BASIC MATERIAL: CARBON STEEL
RATING CLASS: 150 PSIG, 250'
F Max.
Corrosion Allowance:.025"
Mechanical Strength:.065"
Bending Allowance: 8% reduction for 5-diameter bends
DESIGN BASIS - ASME B31.1
285 PSIG @ 100 DEGF
260 PSIG @ 200 DEGF
230 PSIG @ 300 DEGF
200 PSIG @ 400 DEGF
170 PSIG @ 500 DEGF
140 PSIG @ 600 DEGF
125 PSIG @ 650 DEGF
110 PSIG @ 700 DEGF
95 PSIG @ 750 DEGF
• Class 150 flange rating is
limiting design factor
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
PIPE
1/4" thru 1 1/2"
XS
Welded
ASTM A 106, Gr B, T&C,
B16.10M
2" thru 6"
STD
Seamless
ASTM A 53, Gr B, PE,
B36.10M (2" T&C)
FLANGES
1/2" thru 2"
CLASS 150
Threaded,
ASTM A 181,
1,2
RF, FS
B16.5
2 1/2" thru 6"
CLASS 150
Weldneck,
ASTM A 181,
1,3
RF
B16.5
2 1/2" thru 6"
CLASS 150
Weldneck
ASTM A 105,
1,3
FF
B16.5
FITTINGS
1/4" thru 2"
150#
Screwed
ASTM A 105,
B16.11
2 1/2" thru 6"
STD
Buttweld
ASTM A 234 Grade WPB,
1
B16.9
UNIONS
1/4" thru 2"
150#
Screwed
Brass Ground Joint Seat,
ASTM A 105
PLUGS
Threaded,
ASTM A 395,
3/8" thru 2"
-
Solid Square
B16.11
Head
BOLTING
Bolts, Cap
ASTM A 307, Grade B, Wafer
ALL
-
Screws,
Valves: Carbon Steel Studs
Studs
with 2 Hex Nuts/Stud, A 108
GASKETS
1/2" thru 6"
CLASS 150
Ring Type
1/16" Thk, Neoprene
1/16" Thk, Neoprene
2 1/2" thru 6"
CLASS 150
FF
FOR REFERENCE ONLY
1 of 2

PIPING SPEC NO: 320
n m -
Rethink Tomorrow
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
Y-STRAINER
3/8" thru 2"
300#
Screwed
Bronze with w/.045"
Perforated Brass Screen
2 1/2" trhu 6"
150#
Flanged, FF
CS w/.045" Perforated 304
SS Screen
BALL
Bronze Body and Chrome
VALVES
1/4" thru 2"
250#
Screwed
Plated Ball, UL Listed, Seat
RPTFE, Seal PTFE
CHECK
1/2" thru 2"
CLASS 125
Screwed
Bronze with Bronze Tail
VALVES
Piece and Bronze Guide
3" thru 6"
CLASS 150
Wafer
C.S. Body and Buna-N Seat
GLOBE
1/4" thru 2"
CLASS 150
Screwed
Bronze Body, SS Plug Disk,
VALVES
Union Bonnet
PLUG
Cast iron Body, 3-Way, 3 Port
VALVES
1/2' thru 2"
200#
Screwed
Screwed Gland Type, ASTM
A 126-42B
Cast iron Body, Regular
1/2' thru 2"
200#
Screwed
Pattern Screwed Gland Type,
ASTM A 126-42B
Cast iron Body, Regular
2 1/2" thru 4"
125#
Flanged, FF
Pattern Screwed Gland Type,
ASTM A 126-42B
NOTES
1) Schedule of fittings and the bore of weldneck or socketweld flanges shall be same as attached pipe.
2) Use Teflon tape for threaded joints.
3) Flange facing shall be "RAISED FACE" or as required to match the mating flange.
4) See Branch Table BTSOL.
5) Ball valves for on -off service only.
6) Natural gas, propane, non -condensable gas and other flammable gases shall be electrically grounded in
accordance with the NFPA 54 - National Fuel Gas Code. All systems shall maintain a 15 PSIG
NITROGEN PURGE until systems is placed into service. Contact local gas authority concerning
requirements for safe discharge/venting of any flammable gas system.
7) This specification should follow NFPA 54.
8) Use plug valves for main header and branch isolation.
REV A
FOR REFERENCE ONLY
2of2

PIPING SPEC NO: 380
novozymesm
Rethink Tomorrow
SERVICE: Refer to Piping Media Service Index
BASIC MATERIAL: CARBON STEEL
RATING CLASS: 0-400 PSIG, 160' F Max.
Corrosion Allowance:.025"
Mechanical Strength:.065"
Bending Allowance: 8% reduction for 5-diameter bends
DESIGN BASIS - ASME B31.1
285 PSIG @ 100 DEGF
260 PSIG @ 200 DEGF
230 PSIG @ 300 DEGF
200 PSIG @ 400 DEGF
170 PSIG @ 500 DEGF
140 PSIG @ 600 DEGF
125 PSIG @ 650 DEGF
110 PSIG @ 700 DEGF
95 PSIG @ 750 DEGF
• Class 150 flange rating is limiting design factor
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
PIPE
1/4" thru 1 1/2"
XS
Welded
ASTM A 53, Gr B, PE,
B16.10M
2" thru 8"
XS
Seamless
ASTM A 53, Gr B, PE,
B36.10M
FLANGES
1/2" thru 2"
CLASS 150
Socketweld,
ASTM A 105,
1,2,3
RF
B16.5
2 1/2" thru 8"
CLASS 300
Weldneck,
SCH 80 Bore, ASTM A 181,
1,3
RF
B16.5
3" thru 6"
CLASS 150
Weldneck
ASTM A 105,
1
FF
B16.5
FITTINGS
1/4" thru 2"
3000#
Socketweld
ASTM A 105,
B16.11
2 1/2" thru 8"
SCH 80
Buttweld
ASTM A 234 Grade WPB,
1
B16.9
UNIONS
1/4" thru 2"
3000#
Socketweld
Forged Steel with Integral
Ground Seat, ASTM A 105
BOLTING
Alloy Steel, Each With Two
ALL
-
Stud Bolts
Carbon Steel Nuts, A 193,
Gr. B7 & A 194, Gr. 2H
GASKETS
ALL
-
Ring Type
1/16" Thk, TFE, Milled
Envelope
BALL
3-Piece, C.S. Body with 316
VALVES
1/4" thru 2"
-
Socketweld
Stainless Steel Ball and
4
Teflon Seats. Fire Safe
REV A
FOR REFERENCE ONLY
1 of 2

PIPING SPEC NO: 380
novozymes-
Rethink Tomorrow
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
CHECK
Piston Type With Carbon
VALVES
1/2" thru 2"
800#
Socketweld
Steel Body, !3% Chromium
Trim, Bolted Bonnet and
Integral Hardened Seat
Cast Steel Body with 13%
2 1/2" thru 8"
300#
Flanged, RF
Chromium Type 410 SS Trim
& Hard Faced Seat
GLOBE
Carbon Steel Body, Stainless
VALVES
Steel Stem, Threaded or
Flanged Bonnets and Non-
1/2" thru 2"
-
Socketweld
Rotating Self -Aligning Seat
Disc. Hand Wheel or Seal -
Cap (Refrigeration only)
Design
Cast Steel Body with 13%
2 1/2" thru 8"
300#
Flanged, RF
Chromium Type 410 SS Trim
& Hard Faced Seat
ANGLE SHUT
Cast Steel Body, TFE Seat
OFF VALVES
1' thru 4"
400#
Socketweld
Ring, Back Seating Design
NOTES
1) Schedule of fittings and the bore of weldneck or socketweld flanges shall be same as attached pipe.
2) Flange facing shall be "RAISED FACE" or as required to match the mating flange.
3) See Branch Table BTSOL.
4) Ball valves for on -off service only.
FOR REFERENCE ONLY
2of2

PIPING SPEC NO: 390
novozymesm
Rethink Tomorrow
SERVICE: Refer to Piping Media Service Index
BASIC MATERIAL: CARBON STEEL
RATING CLASS: 300 PSIG
Corrosion Allowance:.025"
Mechanical Strength:.065"
Bending Allowance: 8% reduction for 5-diameter bends
DESIGN BASIS - ASME B31.1
740 PSIG @ 100 DEGF
675 PSIG @ 200 DEGF
655 PSIG @ 300 DEGF
635 PSIG @ 400 DEGF
600 PSIG @ 500 DEGF
550 PSIG @ 600 DEGF
535 PSIG @ 650 DEGF
535 PSIG @ 700 DEGF
505 PSIG @ 750 DEGF
• Class 300 flange rating is imiting design factor
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
PIPE
1/4" thru 1 1/2"
XS
Welded
ASTM A 53, Gr B, PE,
B16.10M
2" thru 12"
STD
Seamless
ASTM A 53, Gr B, PE,
B36.10M
FLANGES
1/2" thru 1 1/2"
CLASS 300
Socketweld,
SCH 80 Bore, ASTM A 105,
1,2,3
RF
B16.5
Weldneck,
SCH STD Bore, ASTM A
2 1/2" thru 12"
CLASS 300
RF
181,
1,2,3
B16.5
FITTINGS
1/4" thru 1 1/2"
3000#
Socketweld
ASTM A 105,
B16.11
2" thru 12"
STD
Buttweld
ASTM A 105,
1
B16.9
UNIONS
Ammonia/Halocarbon
1/2" thru 1 1/2"
-
Socketweld
Tongue & Groove Flange Kit,
with Bolts, Nuts & Gaskets.
Ammonia/Halocarbon
2" thru 6"
-
Weldneck
Tongue & Groove Flange Kit,
with Bolts, Nuts & Gaskets.
BOLTING
Alloy Steel, Each With Two
ALL
-
Stud Bolts
Carbon Steel Nuts, A 193,
Gr. B7 & A 194, Gr. 2H
GASKETS
1/16" Thk, TFE, Milled
ALL
-
Ring Type
Envelope
FOR REFERENCE ONLY
1 of 2

PIPING SPEC NO: 390
novozymes-
Rethink Tornorrow
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
CHECK
1/2" thru 1 1/2"
-
Flanged
Ammonia / Halocarbon Disc
VALVES
Type, C.S. Body, F.S.
2" thru 12"
-
Weldneck
Ammonia / Halocarbon Disc
Type, C.S. Body, F.S.,
GLOBE
Ammonia / Halocarbon Globe
VALVES
1/2" thru 12"
-
Flanged
Valve, D.I. Body, Seal Cap
Type, Flanged Design with,
Bolts, Nuts & Gaskets.
ANGLE SHUT
Ammonia / Halocarbon Angle
OFF VALVES
1/2" thru 12"
-
Flanged
Valve, D.I. Body, Seal Cap
Type, Flanged with, Bolts,
Nuts & Gaskets.
EXPANSION
1/4" thru 1"
-
Screwed
Ammonia / Halocarbon Globe
VALVES
Type, D.I. Body.
Ammonia / Halocarbon Globe
1 1/4" thru
Flanged
Type, D.I. Body, Flanged
2"
Design with, Bolts, Nuts, &
Gaskets.
NOTES
1) Schedule of fittings and the bore of weldneck or socketweld flanges shall be same as attached pipe.
2) Flange facing shall be "RAISED FACE" or as required to match the mating flange.
3) See Branch Table BTSOL.
FOR REFERENCE ONLY
2of2

PIPING SPEC NO: 400
- I j
n m -
Rethink Tomorrow
SERVICE: Refer to Piping Media Service Index
BASIC MATERIAL: STAINLESS STEEL
RATING CLASS: 140 PSIG, 100' F Max.
Corrosion Allowance: NA
Mechanical Strength: NA
Bending Allowance: No bending allowance is included.
DESIGN BASIS - ASME B31.3
1/4" 5,100 PSIG @ 100 DEGF 2" 1,220 PSIG @ 100 DEGF
3/8" 3,300 PSIG @ 100 DEGF 2 1/2" 980 PSIG @ 100 DEGF
1/2" 4,880 PSIG @ 100 DEGF 3" 810 PSIG @ 100 DEGF
3/4" 3,250 PSIG @ 100 DEGF 4" 780 PSIG @ 100 DEGF
1 " 2,440 PSIG @ 100 DEGF 6" 680 PSIG @ 100 DEGF
1 1/2" 1,630 PSIG @ 100 DEGF 8" 510 PSIG @ 100 DEGF
10" 500 PSIG @ 100 DEGF
• Clamps are limiting design factor 12" 419 PSIG @ 100 DEGF
• Working Pressure is 1/4 of Burst Pressure
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
TUBING
1/2" thru 3"
.065" wall thk
Seamless
ASTM A 269, TP 304
4"
.083" wall thk
Seamless
ASTM A 269, TP 304
6" thru 8"
.109" wall thk
Seamless
ASTM A 269, TP 304
10" thru 12"
.134" wall thk
Seamless
ASTM A 269, TP 304
1
PIPE
1/4" thru 3/4"
SCH 40
Welded
(Steaming Out Branched)
ASTM A 269, TP 304
FITTINGS
SAME AS
1/4" thru 12"
TUBING OR
Buttweld
ASTM A 403-78CR
2
PIPE
FERRULES
SAME AS
Wall Thickness to Match
1" thru 4"
TUBING
Buttweld
Tube Male Bevel Seat Light,
2
ASTM A 269, TP 304
SAME AS
Wall Thickness to Match
1" thru 4"
TUBING
Buttweld
Tube Female Bevel Seat
2
Light, ASTM A 269, TP 304
FLANGES
1" thru 12"
CLASS 150
Lap Joint
Carbon Steel
Flange
STUB ENDS
1" thru 12"
SAME AS
Buttweld
ASTM A 269, TP 304
TUBING
UNIONS
SAME AS
Assemble from Male Ferrule,
1" thru 4"
TUBING
-
Female Ferrule & Hex Union
Nut ASTM A 269, TP 304
TUBING
304 SS, Polished, Acme
UNION HEX
1" thru 4"
-
Hex
Thread
NUTS
FOR REFERENCE ONLY
1 of 3

PIPING SPEC NO: 400
n m -
Rethink Tornorrow
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
GASKETS
Teflon with Non -Asbestos
ALL
-
Teflon
Filled Milled Envelope,
Gasket I.D. to be Compatible
with Tube I.D.
BOLTING
ALL
-
Hex Head
CS Machine Bolts & Hex
Nuts
BUTTERFLY
C.I. Body, with 316 SS Disc &
VALVES
1" thru 8"
Class 150
Wafer
TFE/EPDM Seat, Wrench
Operator
Sanitary, 304 SS Body and
1" thru 4"
-
Buttweld
Disc, EDPM Seals, 4 Position
Spring Loaded Handle
BALL
3 pc. Body, 316 SS Tube
VALVES
1/2" thru 1 1/2"
Class 150
Buttweld
O.D. Extended Butt Weld
Ends, 316 SS Body, Ball &
Stem TFE Seat & Seals
3 pc. Body, 316 SS B.W.
SCH 40 x
Sch. 40 End x Screwed end,
1/4" thru 3/4"
Screwed
Buttweld
316 SS Body, Ball & Stem
TFE Seat and Seals (For Use
in Steaming Out Branch
2-Way Ball Valve, 150# 316
1 1/2" thru 4"
Class 150
Buttweld
SS, TFE Seats and Seals,
Buttweld ends for O.D.
Tubing
3-Way Ball Valve, 150# 316
1 1/2" thru 4"
Class 150
Buttweld
SS, TFE Seats and Seals,
Buttweld ends for O.D.
Tubing
316 SS Body & Ball, Tube
3"
Class 300
Buttweld
O.D. Buttweld Ends, TFE
Seat & Seals
CHECK
1 1/2" thru 3"
Class 150
Clamp
Ball Check Type with Beveled
"Y"
VALVES
Seats, Body, 304 SS
KNIFE GATE
Cast Iron Body with 304 SS
VALVES
2" thru 6"
-
-
Wetted Parts, Viton Seat &
Teflon Packing
PLUG
2-Way Type with Beveled
VALVES
1" thru 4"
-
Flanged
Seats, 304 SS Plug & Body,
PTFE Sleeve
3-Way Type with Beveled
1" thru 4"
-
Flanged
Seats, 304 SS Plug & Body,
PTFE Sleeve
2-Way Type, 304 SS with
1" thru 4"
-
Buttweld
Buttweld ends for O.D.
Tubing
3-Way Type, 304 SS with
1" thru 4"
-
Buttweld
Buttweld ends for O.D.
Tubing
FOR REFERENCE ONLY
2 of 3

PIPING SPEC NO: 400
novozymes-
Rethink Tomorrow
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
DIAPHRAGM
316 SS, Forged Body,
VALVES
Handwheel Operated with
1/4" thru 3/4"
125#
Buttweld
Indicator & Travel Stop,
4
PTFE with 300 grade backing
diaphragm, Sch. 40S B.W.
B.W. x Screwed Ends.
125# B.W. 316 SS, Forged
Body, Handwheel Operated,
with Indicator & Travel Stop,
1/2" thru 4"
125#
Buttweld
PTFE with 300 grade backing
5
diaphragm, B.W. O.D. Tube
Ends. Ethylene Propylene
Diaphragm.
125# B.W. 316 SS Body with
Drain Bosses, Hand Wheel
Operated with Travel Stop &
1/2" thru 4"
125#
Buttweld
Indicating stem, PTFE with
5
300 grade backing
diaphragm, B.W. O.D. Tube
Ends, Ethylene Propylene
Diaphragm.
NOTES
1) All stainless steel tubing and fittings listed in this specification shall be furnished with standard interior
mechanically polished to 25RA (Microinch) finish, and the exterior unpolished bright -annealed finish
combination.
2) 304 stainless steel at valves, equipment and removable sections of tubing. All others to be designed for
orbital welding, wall thickness to be same as tubing
3) Bore to match tubing, ends suitable for orbital butt -welding.
4) Diaphragm Valves installed in horizontal lines shall have the stem positioned 20' up from the horizontal for
optimum draining.
5) Diaphragm Valves installed with vertical stem to be fitted with drain valves.
FOR REFERENCE ONLY
3of3

PIPING SPEC NO: 401
- I j
novozymesm
Rethink Tomorrow
SERVICE: Refer to Piping Media Service Index
BASIC MATERIAL: STAINLESS STEEL
RATING CLASS: 0-150 PSIG, 250' F Max.
Corrosion Allowance: NA
Mechanical Strength: NA
Bending Allowance: No bending allowance is included.
DESIGN BASIS - ASME B31.3
285 PSIG @ 100 DEGF 140 PSIG @ 600 DEGF
260 PSIG @ 200 DEGF 125 PSIG @ 650 DEGF
230 PSIG @ 300 DEGF 110 PSIG @ 700 DEGF
200 PSIG @ 400 DEGF 95 PSIG @ 750 DEGF
170 PSIG @ 500 DEGF 90 PSIG @ 800 DEGF
• Class 150 carbon steel flange rating is limiting design factor
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
PIPE
1/2" thru 1"
SCH 40S
Seamless or
ASTM A 312, TP 304E
Welded
1 1/2" thru 8"
SCH 10S
Seamless or
ASTM A 312, TP 304L
Welded
FITTINGS
1/2" thru 1"
SCH 40S
Buttweld
ASTM A 403
1 1/2" thru 8"
SCH 10S
Buttweld
ASTM A 403
STUB ENDS
1/2" thru 1"
SCH 40S
C
MSS Length, ASTM A 403,
TP 304L
1 1/2" thru 8"
SCH 10S
C
MSS Length, ASTM A 403,
TP 304L
FLANGES
1/2" thru 8"
CLASS 150
Lap Joint
Carbon Steel, Galvanized,
A 105
GASKETS
ALL
_
FF or Ring
1/16" Thick, TFE Milled
Style
Envelope
BOLTING
ALL
-
Hex
CS Hex head Machine Bolts
with Hex Nuts, A307 Gr. B
BUTTERFLY
316 SS Body, Disc & Stem,
VALVES
1" thru 8"
CLASS 150
Wafer or Lug
TFE Lined EPDM Seat, Satin
Finish Disc
BALL
3 Piece, 316 SS Body, Ball
VALVES
and Stem, TFE Seats and
1/2" thru 2"
600#
Buttweld
Seals Ball Valve, Schedule
40S buttweld & screwed ends
3 Piece, 316 SS Body, Ball
and Stem, TFE Seats and
1/2" thru 8"
CLASS 150
Flanged
Seals Full -port Ball Valve
FOR REFERENCE ONLY
1 of 2

PIPING SPEC NO: 401
novozymes-
Rethink Tomorrow
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
GATE
316L SS Body, Bonnet, Stem
VALVES
1/2" thru 8"
CLASS 150
Flanged, RF
& Solid Wedge Gate,150#
F.F. Flanged Ends, OS&Y
CHECK
1/2" thru 1 1/2"
CLASS 150
Flanged,
316 stainless steel, CF8M
VALVES
RF
2" thru 8"
CLASS 150
Wafer
316 stainless steel
DIAPHRAGM
Forged 316 SS body, ends to
VALVES
match adjoining pipe, 30
1/2" thru 8"
_
pinch Ra internal finish
1,2
TFE/EPDM backed
diaphragm, travel stop where
required.
GLOBE
Stainless steel globe valve,
VALVES
Flanged,
type 316L stainless steel,
1/2" thru 2"
CLASS 150
RF
plug disc, bolted bonnet,
OS&Y, teflon packing and
gasket
PLUG
1/2" thru 3"
CLASS 150
Flanged,
304 Stainless Steel Body
VALVES
RF
STEAM
TRAPS
1/2"
-
Buttweld
SS Thermodynamic Type
3
STEAM
1/2"
-
Threaded
SS Float & Thermostatic
4
TRAPS
Type
NOTES
1) Diaphragm Valves installed in horizontal lines shall be installed per manufactures instructions for optimum
draining.
2) Diaphragm Valves installed with vertical stem to be fitted with Drain Valves.
3) For use in distribution - Main drip service at Dosing Tanks.
4) For use at Antifoam Tanks.
FOR REFERENCE ONLY
2of2

PIPING SPEC NO: 402
n * Lym4
Rethin T rnorr,---v
SERVICE: Refer to Piping Media Service Index
BASIC MATERIAL: STAINLESS STEEL
RATING CLASS:
Corrosion Allowance: NA
Mechanical Strength: NA
Bending Allowance: No bending allowance is included.
DESIGN BASIS - ASME B31.3
1/8" 10,900 PSIG @ 100 DEGF
3/16" 7,000 PSIG @ 100 DEGF
1/4" 7,500 PSIG @ 100 DEGF
3/8" 4,800 PSIG @ 100 DEGF
• Working Pressure is 1/4" of Burst Pressure
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
TUBING
1/8" thru 3/16"
.035" wall thk
Seamless
ASTM A 269, TP 316
1/4" thru 3/8"
.049" wall thk
Seamless
ASTM A 269, TP 316
FITTINGS
1/8" thru 3/8"
SAME AS
Compression
Type 316 Stainless Steel
TUBING
ADAPTERS
1/8" thru 3/8"
SAME AS
Tubing x Pipe
Type 316 Stainless Steel
TUBING
Thread
UNIONS
1/8" thru 3/8"
SAME AS
Compression
Type 316 Stainless Steel
TUBING
BALL
1/8" thru 3/8"
_
_
Type 316 SS Body and Ball,
VALVES
TFE Seats, Viton "'O" Rings
CHECK
Type 316 SS Ball Check, 316
VALVES
1/4" thru 3/8"
-
-
SS Body, Ball, and Spring,
Viton "O" Ring
FOR REFERENCE ONLY
1 of 1

PIPING SPEC NO: 403
- I j
n m -
Rethink Tomorrow
SERVICE: Refer to Piping Media Service Index
BASIC MATERIAL: STAINLESS STEEL
RATING CLASS: 140 PSIG, 100' F Max.
Corrosion Allowance: NA
Mechanical Strength: NA
Bending Allowance: No bending allowance is included.
DESIGN BASIS - ASME B31.3
1/4" 5,100 PSIG @ 100 DEGF 2" 1,220 PSIG @ 100 DEGF
3/8" 3,300 PSIG @ 100 DEGF 2 1/2" 980 PSIG @ 100 DEGF
1/2" 4,880 PSIG @ 100 DEGF 3" 810 PSIG @ 100 DEGF
3/4" 3,250 PSIG @ 100 DEGF 4" 780 PSIG @ 100 DEGF
1 " 2,440 PSIG @ 100 DEGF 6" 680 PSIG @ 100 DEGF
1 1/2" 1,630 PSIG @ 100 DEGF 8" 510 PSIG @ 100 DEGF
10" 500 PSIG @ 100 DEGF
• Clamps are limiting design factor 12' 419 PSIG @ 100 DEGF
• Working Pressure is 1/4 of Burst Pressure
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
TUBING
1/2" thru 3"
.065" wall thk
Seamless
ASTM A 269, TP 304
4"
.083" wall thk
Seamless
ASTM A 269, TP 304
6" thru 8"
.109" wall thk
Seamless
ASTM A 269, TP 304
10" thru 12"
.134" wall thk
Seamless
ASTM A 269, TP 304
1
PIPE
1/4" thru 3/4"
SCH 40
Welded
(Steaming Out Branched)
ASTM A 269, TP 304
FITTINGS
SAME AS
1/4" thru 12"
TUBING OR
Buttweld
ASTM A 403-78CR
2
PIPE
FERRULES
SAME AS
Wall Thickness to Match
1" thru 4"
TUBING
Buttweld
Tube Male Bevel Seat, ASTM
2
A 269, TP 304
SAME AS
Wall Thickness to Match
1" thru 4"
TUBING
Buttweld
Tube Female Bevel Seat,
2
ASTM A 269, TP 304
FLANGES
1" thru 12"
CLASS 150
Lap Joint
Carbon Steel
Flange
STUB ENDS
1" thru 12"
SAME AS
Buttweld
ASTM A 269, TP 304
TUBING
UNIONS
SAME AS
Assemble from Male Ferrule,
1" thru 4"
TUBING
-
Female Ferrule & Hex Union
Nut ASTM A 269, TP 304
TUBING
304 SS, Polished, Acme
UNION HEX
1" thru 4"
-
Hex
Thread
NUTS
FOR REFERENCE ONLY
1 of 3

PIPING SPEC NO: 403
n m -
Rethink Tornorrow
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
GASKETS
Teflon with Non -Asbestos
ALL
-
Teflon
Filled Milled Envelope,
Gasket I.D. to be Compatible
with Tube I.D.
BOLTING
ALL
-
Hex Head
CS Machine Bolts & Hex
Nuts
BUTTERFLY
C.I. Body, with 316 SS Disc &
VALVES
1" thru 12"
Class 150
Wafer or Lug
TFE/EPDM Seat, Wrench
Operator
Sanitary, 304 SS Body and
1" thru 4"
-
Buttweld
Disc, EDPM Seals, 4 lockable
multi -positions handle
BALL
3 Piece, 316 SS body, ball
VALVES
and stem, TFE seats and
1/4" thru 3/4"
600#
-
seals full -port ball valve,
schedule 40 butt weld x
screwed ends.
2-Way Ball Valve, 150# 316
1/2" thru 4"
CLASS 150
Buttweld
SS, TFE seats and seals,
Buttweld ends for O.D.
Tubing
3-Way Ball Valve, 150# 316
1 1/2" thru 4"
CLASS 150
Buttweld
SS, TFE seats and seals,
Buttweld ends for O.D.
Tubing
CHECK
Hygienic tubing Y-type ball
VALVES
1" thru 3"
-
Clamped
check valve, 304 SS
construction, EPDM
elastomer
KNIFE GATE
Cast Iron Body with 304 SS
VALVES
2" thru 6"
-
-
Wetted Parts, Viton Seat &
Teflon Packing
PLUG
304 stainless steel body and
VALVES
1" thru 4"
CLASS 150
Flanged
plug, 2-way plug valve, TFE
seals, 150# flanged end
connections.
304 stainless steel body and
1" thru 4"
CLASS 150
Flanged
plug, 3-way plug valve, TFE
seals, flanged end
connections.
DIAPHRAGM
Forged 316 SS body, ends to
VALVES
match adjoining pipe or
tubing, 30 p-inch Ra internal
finish TFE/EPDM backed
1/4" thru 6"
_
_
diaphragm, travel stop where
4
required.
FOR REFERENCE ONLY
2 of 3

PIPING SPEC NO: 403
novozymesw
Rethink Tomorrow
NOTES
1) All stainless steel tubing and fittings listed in this specification shall be furnished with standard interior
mechanically polished to 25RA (Microinch) finish, and the exterior unpolished bright -annealed finish
combination.
2) 304 stainless steel at valves, equipment and removable sections of tubing. All others to be designed for
orbital welding, wall thickness to be same as tubing
3) Bore to match tubing, ends suitable for orbital butt -welding.
4) Diaphragm Valves installed in horizontal lines shall have the stem positioned 20' up from the horizontal for
optimum draining.
5) Diaphragm Valves installed with vertical stem to be fitted with drain valves.
REV A
FOR REFERENCE ONLY
3of3

PIPING SPEC NO: 410
- I j
novozymesm
Rethink Tomorrow
SERVICE: Refer to Piping Media Service Index
BASIC MATERIAL: STAINLESS STEEL
RATING CLASS: 0-150 PSIG, 250' F Max., Not for Flammable (See Note 1)
Corrosion Allowance: NA
Mechanical Strength: NA
Bending Allowance: No bending allowance is included.
DESIGN BASIS - ASME B31.3
1/4" 5,100 PSIG @ 100 DEGF 2" 1,140 PSIG @ 100 DEGF
3/8" 3,300 PSIG @ 100 DEGF 2 1/2" 910 PSIG @ 100 DEGF
1/2" 4,550 PSIG @ 100 DEGF 3" 760 PSIG @ 100 DEGF
3/4" 3,030 PSIG @ 100 DEGF 4" 730 PSIG @ 100 DEGF
1 " 2,280 PSIG @ 100 DEGF
1 1/2" 1,520 PSIG @ 100 DEGF
• Clamps are limiting design factor
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
TUBING
1/4" thru 3/8"
.035" wall thk
Seamless
ASTM A 269, TP 304L
1/2" thru 3"
.065" wall thk
Seamless
ASTM A 269, TP 304L
4"
.083" wall thk
Seamless
ASTM A 269, TP 304L
FITTINGS
1/2" thru 4"
SAME AS
Buttweld
ASTM A 269, TP 304L
2
TUBING
FERRULES
1" thru 4"
SAME AS
SAME AS
ASTM A 269, TP 304L
2
TUBING
TUBING
REDUCERS
1" thru 4"
SAME AS
Buttweld
ASTM A 269, TP 304L
2
TUBING
CLAMPS
1,200 PSIG @
Heavy
1/2" thru 3/4"
250 DEGF
Weight
ASTM A 269, TP 304L
2
Clam
250 PSIG @
Heavy
1" thru 2"
250 DEGF
Weight
ASTM A 269, TP 304L
2
Clamp
200 PSIG @
Heavy
2 1/2
250 DEGF
Weight
ASTM A 269, TP 304L
2
Clamp
150 PSIG @
Heavy
3
250 DEGF
Weight
ASTM A 269, TP 304L
2
Clamp
800 PSIG @
High
4
250 DEGF
Pressure
ASTM A 269, TP 304L
2
Clam
1" thru 4"
-
Hex
304 SS, Acme thread,
HEX NUTS
Polished
1" thru 6"
Same As
Lap Joint
304L SS
STUB ENDS
Tubing
FOR REFERENCE ONLY
1 of 2

PIPING SPEC NO: 410
n m -
Rethink Tomorrow
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
FLANGES
ALL
Class 150
Flat Faced
304 SS
FERRULE
ALL
-
EDPM
Type 1 — O-Ring
GASKETS
FLANGE
GASKETS
ALL
Class 150
EDPM
Ring Type - 1/8" Thk
SANITARY
UNIONS
1" thru 4"
Class 150
Short Pattern
304L SS, EDPM seat
3
BUTTERFLY
Sanitary, 316L stainless steel
VALVES
body, disc and stem EDPM
seats, Butt -welding end
1" thru 6"
Class 150
Buttweld
connections with two position
handle. Interior and exterior
smooth polished to a 32 Ra
Micro -inch finish.
BALL
316L stainless steel 3-piece,
VALVES
body, full port, RTFE seat
and TFE seal material, butt-
1" thru 4"
Class 150
Buttweld
welding O.D. tube ends to
match tubing thickness,
Standard SS handle.
CHECK
316L stainless steel, disc
VALVES
type, spring loaded, Interior
and exterior polished to RA
equivalent of 42-30 Micro -
inches. (Horizontal
Installation Only)
1" thru 6"
Class 150
Buttweld
316L stainless steel, Optional
Stabilizer Disc, Interior and
exterior polished to RA
equivalent of 42-50 Micro -
inches. (Vertical installation
only)
NOTES
1) All stainless steel tubing and fittings listed in this specification shall be furnished with standard interior
mechanically polished to 25RA (Microinch) finish, and the exterior unpolished bright -annealed finish
combination.
2) At valves, equipment and removable sections of tubing. All others to be designed for orbital welding, wall
thickness to be same as tubing
3) Bore to match tubing, ends suitable for orbital butt -welding.
FOR REFERENCE ONLY
2of2

PIPING SPEC NO: 412
- I J
novozymesm
Rethink Tomorrow
SERVICE: Refer to Piping Media Service Index
BASIC MATERIAL: STAINLESS STEEL
RATING CLASS: 600 PSIG, 100' F
Corrosion Allowance: NA
Mechanical Strength: NA
Bending Allowance: No bending allowance is included.
DESIGN BASIS - ASME B31.3
600 PSIG @ 100 DEGF
360 PSIG @ 600 DEGF
505 PSIG @ 200 DEGF
350 PSIG @ 650 DEGF
455 PSIG @ 300 DEGF
345 PSIG @ 700 DEGF
415 PSIG @ 400 DEGF
335 PSIG @ 750 DEGF
380 PSIG @ 500 DEGF
330 PSIG @ 800 DEGF
• Class 150 Type 304L stainless steel flange rating is limiting
design factor
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
PIPE
1/2" thru 6"
SCH 80S
Seamless or
ASTM A 312, TP 304L
Welded
FITTINGS
1/2" thru 6"
SCH 80S
Buttweld
ASTM A 182, F304L
1
FLANGES
1/2" thru 2"
CLASS 300
Weldneck or
ASTM A 182, F304L
1,2,3
Slip -On, RF
GASKETS
Spiral -Wound Type 304 SS,
ALL
CLASS 300
Ring Style
with Graphite Filler
BOLTING
ASTM A194 Grade 8 Hex
ALL
-
Hex
Head Machine Bolts with
ASTM A193 Grade B8 Hex
Nuts
UNIONS
1/2" thru 6"
CLASS 300
Screwed
304 or 304L SS, Ground Joint
Union
VALVES
1/2" thru 6"
CLASS 300
ALL
To be Furnished by Owner
NOTES
1) Schedule of fittings and the bore of weldneck or socketweld flanges
shall be same as attached pipe.
2) Use Teflon tape for threaded joints.
3) Flange facing shall be "RAISED FACE" or as required to match the mating flange.
4) See Branch Table BTSOL.
FOR REFERENCE ONLY
1 of 1

PIPING SPEC NO: 413
- I J
novozymesm
Rethink Tomorrow
SERVICE: Refer to Piping Media Service Index
BASIC MATERIAL: STAINLESS STEEL
RATING CLASS: 0-150 PSIG, 250' F Max.
Corrosion Allowance: NA
Mechanical Strength: NA
Bending Allowance: No bending allowance is included.
DESIGN BASIS - ASME B31.3
285 PSIG @ 100 DEGF 140 PSIG @ 600 DEGF
260 PSIG @ 200 DEGF 125 PSIG @ 650 DEGF
230 PSIG @ 300 DEGF 110 PSIG @ 700 DEGF
200 PSIG @ 400 DEGF 95 PSIG @ 750 DEGF
170 PSIG @ 500 DEGF 90 PSIG @ 800 DEGF
• Class 150 Type 304L stainless steel flange rating is limiting design factor
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
PIPE
1/2" thru 2"
SCH 40S
Seamless or
ASTM A 312, TP 304L
Welded
FITTINGS
1/2" thru 2"
SCH 40S
Socketweld
ASTM A 182, F304L
FLANGES
1/2" thru 2"
CLASS 150
Socketweld,
ASTM A 182, F304L
RF
GASKETS
ALL
-
Ring Style
1/16" Thick
BOLTING
ALL
-
Hex
304 Hex head Machine Bolts
with Hex Nuts, A 307 Gr. B
BALL
316 body, ball and stem, 3-
VALVES
piece. Reinforced TFE Seat
and stuffing ring, blow-out
1/2" thru 2"
-
Socketweld
proof stem design, adjustable
packing gland, all externals
stainless steel, Standard
Port, 2-1/4" Extended Stem,
Plastic coated lever handle
316 SS body, ball and stem,
3-piece. Reinforced TFE Seat
and Stuffing ring, blow-out
Socketweld x
proof stem design, adjustable
1/2" thru 1°
-
Threaded
Packing gland, all externals
stainless steel, Standard
Port, 2-1/2" Extended Stem,
Plastic coated lever handle
STEAM
Stainless steel
TRAPS
1/2" thru 2"
_
Thermo-
thermodynamic trap with
dynamic
integral Strainer
FOR REFERENCE ONLY
1 of 1

PIPING SPEC NO: 451
- I j
novozymesm
Rethink Tomorrow
SERVICE: Refer to Piping Media Service Index
BASIC MATERIAL: STAINLESS STEEL
RATING CLASS: 0-150 PSIG, 275° F Max.
Corrosion Allowance: NA
Mechanical Strength: NA
Bending Allowance: No bending allowance is included.
DESIGN BASIS - ASME B31.3
1/2" 135 PSIG @ 275 DEGF 3" 175 PSIG @ 275 DEGF
3/4" 110 PSIG @ 275 DEGF 4" 370 PSIG @ 275 DEGF
1" 365 PSIG @ 275 DEGF 6" 275 PSIG @ 275 DEGF
1 1/2" 250 PSIG @ 275 DEGF 8" 235 PSIG @ 275 DEGF
2" 195 PSIG @ 275 DEGF 10" 205 PSIG @ 275 DEGF
• 3/4" Pipe is limiting design factor
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
PIPE
1/2" thru 10"
SCH 10S
Seamless or
ASTM A 312, TP 316L
Welded
FITTINGS
1/2" thru 10"
SCH 10S
Buttweld
ASTM A 403
STUB ENDS
1/2" thru 10"
SCH 10S
Buttweld
MSS Length, ASTM A 403,
TP 316L
FLANGES
1/2" thru 10"
CLASS 150
Lap Joint
SS, ASTM A182, F304L
GASKETS
ALL
-
Ring Style
1/16" Thick, TFE Milled
Envelope
BOLTING
ALL
-
Hex
304 SS Hex Head Cap Screw
or Studs and Hex Nuts
BUTTERFLY
316 SS disc and stem, wafer
VALVES
type butterfly valve, valve
body, integrally cast top plate
for direct flush -mounting of
1" thru 10"
CLASS 150
Wafer
manual or power actuators
1
without use of brackets or
adaptors. Valves 8" and
larger to be provided with
manual gear operators.
BALL
3 Piece, 316 SS body, ball
VALVES
and stem, TFE seats and
seals full -port ball valve,
schedule 10S butt weld x
screwed ends.
1/2" thru 1 1/2"
600#
Buttweld x
Screwed
FOR REFERENCE ONLY
1 of 2

PIPING SPEC NO: 451
novozymes-
Rethink Tornorrow
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
BALL
316 SS Body and Ball. 3-
VALVES
Piece, Sch. 10S Buttweld
(CONT)
2" thru 4"
300#
Buttweld
Ends,316 SS Body and Ball,
TFE Seat and Seals, Plastic
Coated Steel Handle,
316 Stainless Steel Body &
6"
150#
Flanged, RF
Ball, Reinforced TFE Seats
and TFE Seals, Full Port
CHECK
316 SS, Ball -Cone Type,
VALVES
1/2" thru 1"
-
Screwed
CF8M
1 1/2"
CLASS 150
Flanged, RF
316 stainless steel, swing
type
Swing Type,316 SS Body
1" thru 1 1/2"
CLASS 150
Buttweld
with Schedule 10S Buttweld
Ends
316 SS Body, 316 SS split
2" thru 10"
CLASS 150
Wafer, RF
disk with Inconel Springs,
Viton seats
GLOBE
Flanged,
316 SS Body, OS&Y, with
VALVES
1/2" thru 4"
CLASS 150
RF
Rising Stem, Plug Disc and
Teflon Packing and Gaskets
PLUG
316 Stainless Steel Body and
VALVES
1/2" thru 4"
CLASS 150
Flanged,
Plug, PTFE Sleeve, Wrench
RF
operated except 4"-Gear
Operated
FOR REFERENCE ONLY
2of2

PIPING SPEC NO: 460
- I j
novozymesm
Rethink Tomorrow
SERVICE: Refer to Piping Media Service Index
BASIC MATERIAL: STAINLESS STEEL
RATING CLASS: 0-150 PSIG, 250' F Max., Not for Flammable (See Note 1)
Corrosion Allowance: NA
Mechanical Strength: NA
Bending Allowance: No bending allowance is included.
DESIGN BASIS - ASME B31.3
1/4" 5,100 PSIG @ 100 DEGF 2" 1,140 PSIG @ 100 DEGF
3/8" 3,300 PSIG @ 100 DEGF 2 1/2" 910 PSIG @ 100 DEGF
1/2" 4,550 PSIG @ 100 DEGF 3" 760 PSIG @ 100 DEGF
3/4" 3,030 PSIG @ 100 DEGF 4" 730 PSIG @ 100 DEGF
1 " 2,280 PSIG @ 100 DEGF 6" 640 PSIG @ 100 DEGF
1 1/2" 1,520 PSIG @ 100 DEGF
• Clamps are limiting design factor
• Working Pressure is 1/4" of Burst Pressure
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
TUBING
1/4" thru 3/8"
.035" wall thk
Seamless
ASTM A 269, TP 316L
1/2" thru 3"
.065" wall thk
Seamless
ASTM A 269, TP 316L
4"
.083" wall thk
Seamless
ASTM A 269, TP 316L
6"
.109" wall thk
Seamless
ASTM A 269, TP 316L
1
FITTINGS
1/2" thru 4"
SAME AS
HW Clamp
ASTM A 269, TP 316L
2
TUBING
6„
SAME AS
TUBING
Buttweld
ASTM A 269, TP 316L
2
FERRULES
1" thru 4"
SAME AS
SAME AS
ASTM A 269, TP 316L
2
TUBING
TUBING
REDUCERS
1" thru 4"
CLASS 3000
Buttweld
ASTM A 269, TP 316L
CLAMPS
1/2" thru 3/4"
1,200 PSIG @
HW Clamp
ASTM A 269, TP 316L
2
250 DEGF
1" thru 2"
250 PSIG @
250 DEGF
HW Clamp
ASTM A 269, TP 316L
2
2 1/2"
200 PSIG @
HW Clamp
ASTM A 269, TP 316L
2
250 DEGF
3„
150 PSIG @
250 DEGF
HW Clamp
ASTM A 269, TP 316L
2
4„
800 PSIG @
250 DEGF
HP Clamp
ASTM A 269, TP 316L
2
6„
SAME AS
SAME AS
ASTM A 269, TP 316L
2
TUBING
TUBING
FOR REFERENCE ONLY
1 of 2

PIPING SPEC NO: 460
nOar m -
Rethink Tomorrow
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
HEX NUTS
1" thru 4"
-
Hex
304 SS, Polished
STUB ENDS
1" thru 6"
Same As
Tubing
Lap Joint
316L SS
FLANGES
ALL
Class 150
Flat Faced
316 SS
FERRULE
GASKETS
ALL
-
EDPM
Type 1 — O-Ring
FLANGE
GASKETS
ALL
Class 150
EDPM
Ring Type - 1/8" Thk
SANITARY
UNIONS
1" thru 4"
Class 150
Short Pattern
316L SS, EDPM seat
3
BUTTERFLY
316L stainless steel body,
VALVES
disc and stem EDPM seats,
Butt -welding end connections
1" thru 6"
Class 150
Buttweld
with two position handle.
Interior and exterior smooth
polished to a 32 Ra Micro -
inch finish.
BALL
316L stainless steel body, full
VALVES
port, RTFE seat and TFE
seal material, butt -welding
1" thru 4"
Class 150
Buttweld
O.D. tube ends to match
tubing thickness, Standard
SS handle.
CHECK
316L stainless steel, disc
VALVES
type, spring loaded, Clamp
compatible ends, Interior and
exterior polished to RA
equivalent of 42-30 Micro -
inches. (Horizontal
Installation Only)
1" thru 6"
Class 150
Clamp
316L stainless steel, Optional
Stabilizer Disc, Clamp
compatible ends, Interior and
exterior polished to RA
equivalent of 42-50 Micro -
inches. (Vertical installation
only
NOTES
1) All stainless steel tubing and fittings listed in this specification shall be furnished with standard interior
mechanically polished to 25RA (Microinch) finish, and the exterior unpolished bright -annealed finish
combination.
2) 316L stainless steel at valves, equipment and removable sections of tubing. All others to be designed for
orbital welding, wall thickness to be same as tubing
3) Bore to match tubing, ends suitable for orbital butt -welding.
REV A
FOR REFERENCE ONLY
2of2

PIPING SPEC NO: 461
- I j
novozymesm
Rethink Tomorrow
SERVICE: Refer to Piping Media Service Index
BASIC MATERIAL: STAINLESS STEEL
RATING CLASS: 0-150 PSIG, 275' F Max.
Corrosion Allowance: NA
Mechanical Strength: NA
Bending Allowance: No bending allowance is included.
DESIGN BASIS - ASME B31.3
285 PSIG @ 100 DEGF 140 PSIG @ 600 DEGF
260 PSIG @ 200 DEGF 125 PSIG @ 650 DEGF
230 PSIG @ 300 DEGF 110 PSIG @ 700 DEGF
200 PSIG @ 400 DEGF 95 PSIG @ 750 DEGF
170 PSIG @ 500 DEGF
• Class 150 flange rating is limiting design factor
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
PIPE
1/2" thru 10"
SCH 10S
Seamless or
ASTM A 312, TP 316L
Welded
FITTINGS
1/2" thru 10"
SCH 10S
Buttweld
ASTM A 403
STUB ENDS
1/2" thru 10"
SCH 10S
Buttweld
MSS Length, ASTM A 403,
TP 316L
FLANGES
1/2" thru 10"
CLASS 150
Lap Joint
SS, ASTM 182 F304L
GASKETS
ALL
-
Ring Style
1/16" Thick, TFE Milled
Envelope
BOLTING
ALL
-
Hex
304 SS Hex Head Cap Screw
or Studs and Hex Nuts
BUTTERFLY
316 SS Body, TFE Lined,
VALVES
1" thru 10"
CLASS 150
Wafer
EPDM Seat,316 SS Disc and
1
Stem, Wafer Type
BALL
3 Piece, 316 SS body, ball
VALVES
Flanged, RF
and stem, TFE seats and
1/2" thru 1 1/2"
600#
or FNPT
seals full -port, schedule 10S
butt weld, FNPT or flanged
ends as needed.
CHECK
316 SS, Ball -Cone Type,
VALVES
1/2" thru 1"
-
Screwed
CF8M
1 1/2"
CLASS 150
Flanged, RF
316 stainless steel, Swing
Type
Swing Type,316 SS Body
with Schedule 10S Buttweld
Ends
1" thru 1 1/2"
CLASS 150
Buttweld
REV A
FOR REFERENCE ONLY
1 of 2

PIPING SPEC NO: 461
n * Lym4
Rethink Tomorrow
ITEM
SIZE
RATING/SCH
TYPE
SPECIFICATION
NOTES
CHECK
316 SS Body, 316 SS split
VALVES
2" thru 10"
CLASS 150
Wafer, RF
disk with Inconel Springs,
CONT
Viton seat
GLOBE
Flanged,
316 SS Body, OS&Y, with
VALVES
1/2" thru 4"
CLASS 150
RF
Rising Stem, Plug Disc and
Teflon Packing and Gaskets
PLUG
316 Stainless Steel Body and
VALVES
1/2" thru 4"
CLASS 150
Flanged,
Plug, PTFE Sleeve, Wrench
RF
operated except 4", Gear
Operated
FOR REFERENCE ONLY
2of2

BRANCH CONNECTION TABLE BTFIT
BTFIT-1
B
R
A
N
C
H
S
I
Z
E
S
nym*
Rethink Tomorrow
BRANCH CONNECTION TABLE - BTFIT
HEADER SIZES (INCHES) - DESIGN BASIS => ONLY TEES OR REDUCING TEES WHEN AVAILABLE
NPS
24
20
18
16
14
12
10
8
6
4
3
2
11/2
1
3/4
1/2
1/2
---
---
---
---
---
---
---
---
---
---
---
---
RTE
RTE
RTE
TEE
3/4
---
---
---
---
---
---
---
---
---
---
---
RTE
RTE
RTE
TEE
1
---
---
---
---
---
---
---
---
---
RTE
RTE
RTE
RTE
TEE
11/2
---
---
---
---
---
---
---
--
---
RTE
RTE
I RTE
TEE
2
---
---
---
---
---
---
RTE
RTE
RTE
RTE
RTE
TEE
---
--
--
RTE
RTE
RTE
RTE
TEE
---
---
RTE
RTE
RTE
RTE
TEE
---
---
RTEJ
RTE
RTE
TEE
--
RTE
RTEJ
I RTE
TEE
RTE
I RTE
RTE
TEE
RTE
RTE
TEE
RTE
TEE
TEE
TEE - FULL STRAIGHT TEE
RTE - REDUCING TEE
--- INDICATES NOT AVAILA
3
---
---
---
4
---
---
--
6
---
---
--
8
---
--
RTEJ
10
RTE
RTE
RTEJ
12
RTE
RTE
RTE
14
RTE
RTE
RTE
16
RTE
RTE
RTE
18
RTE
RTE
TEE
20
RTE
TEE
24
TEE
BLE
NOTES:
1) The actual design conditions shall be used to determine branch connection requirements as a minimum.
2) All branch connections shall be in accordance with ASME/ANSI 1331.1, Paragraph 104.3.1.
3) Design calculations for branch connections only consider design pressure and temperature. Thermal
forces/moments, hydraulic forces/moments and vibration may require additional reinforcement for the
branch connection.
END OF SECTION
REV A
FOR REFERENCE ONLY g(
1 of 1

novozymeso
BRANCH CONNECTION TABLE BTSOL Rethink Tomorrow
BTSOL-1
BRANCH CONNECTION TABLE - BTSOL
HEADER SIZES (INCHES) - DESIGN BASIS => 100% REINFORCEMENT REQUIRED
B
R
A
N
C
H
S
I
Z
E
S
NPS
48
42
36
30
24
20
18
16
14
12
10
8
6
4
3
2
11/2
1
3/4
1/2
1/2
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SWI SWI
SWI RTE
RTE
RTE
TEE
3/4
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
RTE
TEE
1
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
RTE
RTE
TEE
11/2
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
SOL
RTE
TEE
2
SOL
SOL
SOL
SOL
SOL
WOL
WOL
WOL
WOL
WOL
WOL
WOL
WOL
WOL
WOL
TEE
SOL
WOL
WOL
WOL
WOL
WOL
WOL
WOL
WOL
WOL
TEE
SOL
WOL
WOL
WOL
WOL
WOL
WOL
WOL
WOL
TEE
SOL
WOL
WOL
WOL
WOL
WOL
WOL
WOL
TEE
SOL
WOL
WOL
WOL
WOL
WOL
WOL
TEE
SOL
WOL
WOL
WOL
WOL
WOL
TEE
SOL
WOL
WOL
WOL
WOL
TEE
I SOL I SOL SOL SOL TEE
WOL WOL WOL TEE
WOL WOL TEE
WOL TEE
TEE
TEE - FULL STRAIGHT TEE
RTE - REDUCING TEE
RWD - REINFORCED NOZZLE WITH PAD
SOL - SOCKOLET or LIGHT -WEIGHT S/W PIPET
WOL - WELDOLET OR LIGHT -WEIGHT B/W PIPET
SWI - FULL TEE WITH S/W REDUCING INSERT
3
WOL
WOL
WOL
WOL
4
WOL
WOL
WOL
WOL
6
WOL
WOL
WOL
WOL
8
WOL
WOL
WOL
WOL
10
WOL
WOL
WOL
WOL
12
WOL
WOL
WOL
WOL
14
WOL
WOL
WOL
WOL
16
WOL
WOL
WOL
WOL
18
WOL
WOL
WOL
WOL
20
WOL
WOL
WOL
WOL
24
WOL
WOL
WOL
WOL
30
RWD
RWD
RWD
TEE
36
RWD
RWD
TEE
42
RWD
TEE
48
TEE
NOTES:
1) The actual design conditions shall be used to determine branch connection requirements as a minimum.
2) All branch connections shall be in accordance with ASME/ANSI B31.1, Paragraph 104.3.1.
3) Design calculations for branch connections only consider design pressure and temperature. Thermal
forces/moments, hydraulic forces/moments and vibration may require additional reinforcement for the
branch connection.
END OF SECTION
REV A
FOR REFERENCE ONLY g(
1 of 1

Construction Specifications For
Aboveground Piping
Master Specification
Novozymes, Franklinton, NC
- . j
novozymes-
Rethink Tomorrow
REVISION LOG
REVISION
DATE
DESCRIPTION
0
12/13/13
1 Initial Release
FOR REFERENCE ONLY
1 of 1

NOVOZYMES NORTH AMERICA INC.
FRANKLINTON, NC
SBM TANK ADDITION
SECTION 230902
SEQUENCE OF OPERATIONS
PART 1 - GENERAL
1.1 Summary
HIPP PROJECT #R20162
SECTION 230902
REV. 0
A. The following sequence of operations addresses the SBM Tank Addition for Novozymes.
This document should be reviewed with the P&ID FAA72963_U502986 and the instrument
index where applicable.
PART 2 - SEQUENCE OF OPERATIONS
2.1 SBM Storage Tank FLF96DT
A. The SBM Storage Tank is an eductor agitated tank driven by recirculation pump
FLF96DP02. The recirculation pump operates between 6'-8" and 27' level, as indicated
by level transmitter with appropriate indication feedback to the operator station as desired
by the client. At a minimum the recirculation pumps will not operate with less than 6'
indicated and valve FLF96DT-V-01 shall close at the 27' indication.
B. Recirculation pump FLF996DP02 is provided with a variable frequency drive, (specified
and integrated by others).
C. The tank pH level is monitored by FLF96DT-AIT-01 which should be configured for client
determined high or low alarms.
2.2 Transfer Valve FLF96DT-V-01 is a gate valve which isolates the SBM Storage Tank from
the facility unless a transfer is desired by the operator. The valve comes with limit switches
and appropriate valve malfunction alarming should be implemented. This valve shall be
software interlocked to a high high tank level of 27'.
2.3 Truck Loading and Flow Monitoring
A. Stored SBM is truck loaded for offsite disposal. Submerged pump FLF96DP01 pumps
SBM through magnetic flowmeter FLF96DT-FIT-01 into the truck. The flowmeter is used
for monitoring purposes as the truck is loaded. The transmitter and display is remotely
mounted at the truck loading station where a maintained hand switch HS-03 is provided.
This switch is a request to the DCS to run the pump, it does not control the pump directly.
Operator permissive and tank level approve or deny truck loading.
B. Pump FLF96DP01 has a HOA switch at the MCC for maintenance purposes. The switch
provides local indication and control.
END OF SECTION 230902
HIPP ENGINEERING AND CONSULTING, INC. SECTION 230902
RALEIGH, NC SEQUENCE OF OPERATIONS
PAGE 1 OF 1

Class A Residuals Application for Permit Modification and Renewal, Permit# WQ0003487
Novozymes North America, Inc.
Additional Information
The information provided below is presented for the Distribution of Class A Residual (DCAR) and the Residual
Source Classification (RSC) forms.
1. DCAR
2. RSC
1. DCAR Section D. Program Information
Residual Solids Generation
Novozymes currently has two main sources of residuals: 1) enzyme fermentation spent biomass and 2) the onsite
biological wastewater treatment facility. Both residuals sources produce a liquid slurry residual waste. In addition to
the cellular mass from fermentation, Novozymes spent biomass may include off -spec fermentation raw materials,
off -spec fermentation batches, or finished goods that do not meet customer quality standards.
Residuals generated from the onsite wastewater treatment facility include waste activated sludge from biological
treatment of process wastewater and solids from the primary clarifier. The onsite plant treats 100% industrial
wastewater; all sanitary waste is sent separately to the Franklin County Publicly Owned Treatment Works.
The requested modification is to add reverse osmosis (RO) waste to the residual waste stream. The RO
waste will be generated as a byproduct of RO operation, which will be implemented and operated as part of
the new wastewater treatment NPDES permit NC008962.
Residuals Treatment
All sources of solid residuals are treated in the same manner. The residuals are pumped from the production area
to one of two lime treatment systems, where either bulk lime or hydrated lime is added to achieve a pH set -point of
12 s.u. After the residuals have met the pH setpoint, they are pumped to three concrete storage tanks, equipped
with mixing.
The requested modification includes addition of a fourth concrete tank to offset increased volume from RO
waste.
To maximize storage capacity, a side -stream of waste activated sludge is processed via decanter centrifuge for
dewatering prior to alkaline stabilization. The centrate water from this activity is returned to the process wastewater
treatment plant. If needed, spent fermentation biomass can be dewatered in this system. In the event of an
emergency, dewatered residuals cake can also be sent to a roll -off dumpster for disposal through a third -party
contractor.
Residuals Storage
Novozymes has two 700,000-gallon concrete storage tanks, each with three 20-HP mixers and one 1.645-million-
gallon concrete storage with three 20-HP mixers for residuals storage. Additionally, Novozymes has one 292,300-
gallon glass -lined metal tank that is used as emergency residuals storage. The fourth proposed tank will also be a
1.645-million-gallon concrete storage tank with pumped agitation.
Residuals Disposal
From the three main concrete storage tanks and the future fourth concrete tank, liquid residuals slurry is pumped
into tanker trucks at a loading bay and hauled by a third -party contractor to the application fields. The residuals are
transferred from the tanker trucks to tractor -drawn slurry wagons and sprayed onto agricultural fields at a standard
rate of 6,000 gallons per acre. Prior to residuals application, a Novozymes employee flags the required setbacks
and any field hazards for the tractor operators. At the end of the application, the flags are removed, and the site is
inspected.
Nutrients
Novozymes residual is very low in heavy metals, contains no detectable pathogens, and is low in nutrients.
Novozymes residual is registered with the North Carolina Department of Agriculture as a fertilizer with low nitrogen

Class A Residuals Application for Permit Modification and Renewal, Permit# WQ0003487
Novozymes North America, Inc.
(N), phosphorus (P), and potassium (K) content. The standard application rate of 6,000 gallons per acre typically
provides only a small amount of N and K required by receiver crops and most of the P requirement.
The proposed modification to add RO waste to the residual will not significantly change the N or P content of the
residual. The K content of the residual will increase and provide more benefit for receiver crops.
Other constituents
Novozymes residual is very low in heavy metals and contains no detectable pathogens. Hydrated lime is added to
the residual to achieve vector attraction reduction. Lime is beneficial to crop receiver sites due to low soil pH
typical of the region.
The addition of RO waste to the residual will increase sodium and overall salinity. The sodium adsorption ratio
(SAR) is expected to increase to approximately 5 which is below the permit limit of 10. Novozymes conducted plot
studies in 2020 to assess potential crop effects from increased salinity, and no impacts to plant health were
observed. Novozymes will conduct additional soil and vegetation testing to monitor and prevent adverse effects
from increased salinity.
Marketability statement
Novozymes' residuals application program includes farms in Franklin, Vance, Warren, Granville, Wake, and Nash
Counties. Under normal operating conditions, application is limited to farms within a 40-mile radius of the
Novozymes Franklinton, NC facility.
Novozymes currently has approximately 200 landowners actively participating in the residual land application
program, with a total approximate area of 20,000 acres.
The typical residuals application rate is 6,000 gallons of liquid residuals per acre per year with a limited number of
sites receiving 12,000 gallons per acre per year.
All hauling and spreading of residuals is done by a third party contracted by Novozymes and operates under
Novozymes oversight.
Novozymes controls the application or residuals via a third party. Landowners are provided an information sheet
with relevant information on nutrients and lime provided. The information sheet is attached below.
Novozymes Spent Biomass Nutrient Value
Typical Nutrients from 6,000 gallacre application at Current Future
S% solids
Total nitrogen
Plant available nitrogen —grasses- 40% PAN
Plant available nitrogen - corn, wheat - 60% PAN
Phosphate
Potash
Lime
Capper
Zino
NutMentcorlant of SSM bawd on monthly cerlMaalab sampling
(Ibslacre) (Ibslacre)
100 80
45 35"
65 55
50 40
50 60
300 300
0.01 0.01
0.03 0_03
For more info or scheduling contact
Scott Creech cell (919} 496-0862
Email [e-mail] novoryme5'

Class A Residuals Application for Permit Modification and Renewal, Permit# WQ0003487
Novozymes North America, Inc.
2. RSC additional information
Data used to prepare sections 3, 4, 5, and 6 include:
Section 3. Hazardous Waste Determination — Novozymes residual (SBM) and process waste water
effluent (PWW) were tested. Reports from ENCO are attached. The results from the SBM sample were
used in Section 3.
Section 4. Metals Determination
Section 5. Nutrient/Micronutrient Determination
Section 6. Other Pollutants Determination
The results of 2020 monthly lab testing of Novozymes residual and five (5) analyses of reverse osmosis
waste solids generated during a pilot project in 2019-2020 were used to estimate the future residual
quality after addition of RO waste. The predicted quality from the addition of RO waste was estimated by
Novozymes and provided to Branch Residuals for analyses (see Attachment A in the report by Branch
Residuals).

Novozymes Residual
2020 testing results
A-k
Cadmium
Copper
Lead
Mercury
Molybedium
Nickel
Selenium
Zinc
Aluminium
Ammonia
Calcium
Magnesium
Md.
NRmte
NRrite♦Nit- phosphorous
potassium
Sodium
TKN
Total Nitrogen
SAR
%Solids
FIF16_ML_As F1196_MLCd
1IF96_MI Cu FLF96_MLpb
FLF96_MLHg
FLF96_ML_Mb
FLF96_MLNi
FLF96_ML_5e FLF96_ML_Zn
FLF96_ML_Al
FLF96_ML_NH3
FLF96_ML_Ca
FLF96_ML_Mg FLF96_MLN02
FLF96_MLN03
FLF96_ML_Tp
FLF96_ML_K
FLF96_ML_Na LF96_ML_TK
NitrlteaNitrate+TKN LF96_ML_SA
FLF96_ML_TS
■
grab
grab
9mb
grab
grab
grab
9mb
grab
grab
grab
grab
grab
grab
grab
grab
9mb
9mb
9mb
grab
grab
grab
grab
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
1/7/2020
0.076
0.0036
0.2030
0.033
0.00075
0.0527
0.0517
0.062
0.568
95.30
100
2540
48.00
0.240
6.5
6.74
560
452
267
1900
1906.74
1.43
4.5
2/4/2020
0.076
0.0036
0.5390
0.031
0.00075
0.0796
0.0717
0.062
1.860
615.00
62
2100
76.70
0.540
1000.0
1000.54
630
542
284
1700
2700.54
1.65
5.1
3/3/2020
0.076
0.0036
0.2590
0.031
0.00075
0.0396
0.0571
0.062
0.645
150.00
96
2020
27.90
0.042
13.0
13.04
650
510
301
1900
1913.04
1.82
11.0
4/7/2020
0.076
0.0036
0.1660
0.031
0.00150
0.0405
0.0594
0.062
0.258
5.39
210
2110
30.40
0.630
18.0
18.63
680
1000
509
2300
2318.63
3.01
5.2
5/31/2020
0.076
0.0036
0.0478
0.031
0.00075
0.0250
0.0239
0.062
0.095
19.70
150
1960
4.61
0.240
2.8
3.04
660
323
202
1800
1803.04
1.25
4.7
6/2/2020
0.076
0.0036
0.1200
0.031
0.00150
0.0360
0.0293
0.062
0.392
64.10
180
2970
14.20
0.430
7.5
7.93
640
398
237
2000
2007.93
1.19
4.6
7/7/2020
0.076
0.0036
0.6370
0.031
0.00015
0.0312
0.0680
0.062
1.300
456.00
170
5540
77.40
0.290
5.0
5.29
820
591
564
2500
2505.29
2.06
2.9
8/3/2020
0.076
0.0036
0.8510
0.031
0.00300
0.0549
0.1470
0.062
2.080
215.00
43
7560
111.00
0.460
1.8
2.26
1100
693
276
1400
1402.26
0.86
4.8
9/1/2020
0.076
0.0036
0.1990
0.031
0.00150
0.0274
0.0258
0.062
0.133
15.60
100
2800
15.40
0.190
2.9
3.09
790
339
278
2500
2503.09
1.44
5.9
10/6/2020
0.076
0.0036
0.0337
0.031
0.00075
0.0250
0.0377
0.062
0.278
49.40
130
3370
10.70
0.210
19.0
19.21
560
589
303
1900
1919.21
1.43
3.4
11/3/2020
0.076
0.0036
0.0782
0.031
0.00150
0.0250
0.0308
0.062
0.113
7.75
160
3340
51.00
0.240
15.0
15.24
170
660
364
1300
1315.24
1.71
3.8
12/3/2020
0.076
0.0036
0.0160
0.031
0.00150
0.0250
0.0220
0.062
0.079
34.80
50
2360
14.10
2.500
918.0
920.50
56
532
468
1000
1920.50
2.64
4.8
Average 0.076 0.0036 0.2625 0.031 0.0012 0.0385 0.0520 0.062 0.650 144 121 3223 40.12 0.501 167.5 167.96 610 552 338 1850 2017.96 1.71

SBM residual (average flow and average concentrations) RO waste (oroiected flow and average concentrations) Predicted future SBM residual with RO waste
Flow
673003 L
Percent Solids (%)
5.1
Arsenic
0.076 mg/L
1.502 mg/kg
Cadmium
0.0036 mg/L
0.071 mg/kg
Copper
0.262 mg/L
5.189 mg/kg
Lead
0.031 mg/L
0.616 mg/kg
Mercury
0.00120 mg/L
0.024 mg/kg
Molybdenum
0.0385 mg/L
0.761 mg/kg
Nickel
0.052 mg/L
1.029 mg/kg
Selenium
0.062 mg/L
1.226 mg/kg
Zinc
0.65 mg/L
12.852 mg/kg
Aluminium
144 mg/L
2847 mg/kg
Ammonia
121 mg/L
2390 mg/kg
Calcium
3223 mg/L
63707 mg/kg
Magnesium
40 mg/L
793 mg/kg
Nitrate -Nitrite
168 mg/L
3320 mg/kg
Phosphorus
609.7 mg/L
12053 mg/kg
Potassium
552 mg/L
10921 mg/kg
Sodium
338 mg/L
6677 mg/kg
TKN
1850 mg/L
36573 mg/kg
2018 mg/L
39894 mg/kg
ITN
Chloride
420 mg/L
8303 mg/kg
TDS
18000 mg/L
355848 mg/kg
Flow
189000 L
Percent Solids (%)
2.7
Arsenic
0.035 mg/L
1.295 mg/kg
Cadmium
0.0017 mg/L
0.061 mg/kg
Copper
0.023 mg/L
0.844 mg/kg
Lead
0.016 mg/L
0.588 mg/kg
Mercury
0.00063 mg/L
0.023 mg/kg
Molybdenum
0.0149 mg/L
0.550 mg/kg
Nickel
0.0207 mg/L
0.765 mg/kg
Selenium
0.029 mg/L
1.056 mg/kg
Zinc
0.055 mg/L
2.053 mg/kg
Aluminium
0.455 mg/L
17 mg/kg
Ammonia
5.00 mg/L
185 mg/kg
Calcium
3223.00 mg/L
119370 mg/kg
Magnesium
42 mg/L
1541 mg/kg
Nitrate -Nitrite
23.000 mg/L
852 mg/kg
Phosphorus
57.3 mg/L
2120 mg/kg
Potassium
3108 mg/L
115111 mg/kg
Sodium
3574 mg/L
132370 mg/kg
TKN
10 mg/L
370 mg/kg
33 mg/L
1222 mg/kg
ITN
Chloride
3020 mg/L
111852 mg/kg
TDS
19400 mg/L
718519 mg/kg
Flow
862003 L
Percent Solids (%)
4.54
Arsenic
0.07 mg/L
1.475 mg/kg
Cadmium
0.00 mg/L
0.070 mg/kg
Copper
0.21 mg/L
4.623 mg/kg
Lead
0.03 mg/L
0.612 mg/kg
Mercury
0.00 mg/L
0.024 mg/kg
Molybdenum
0.03 mg/L
0.733 mg/kg
Nickel
0.05 mg/L
0.994 mg/kg
Selenium
0.05 mg/L
1.204 mg/kg
Zinc
0.52 mg/L
11.444 mg/kg
Aluminium
112.53 mg/L
2478 mg/kg
Ammonia
95.50 mg/L
2103 mg/kg
Calcium
3222.61 mg/L
70963 mg/kg
Magnesium
40.45 mg/L
891 mg/kg
Nitrate -Nitrite
136.18 mg/L
2999 mg/kg
Phosphorus
488.55 mg/L
10758 mg/kg
Potassium
1112.75 mg/L
24503 mg/kg
Sodium
1047.32 mg/L
23062 mg/kg
TKN
1446.57 mg/L
31854 mg/kg
1582,74 mg/L
34853 mg/kg
�TN
Chloride
990 mg/L
i
21802 mg/kg
TDS
18307 mg/L
403126 mg/kg

2�SQ pCCgF ENCO Laboratories
9e0
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Thursday, March 4, 2021
Novozymes North America (N0008)
Attn: Joe Ladd
77 Perry Chapel Church Road
Franklinton, NC 27525
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: SBMPWW2021
ENCO Workorder(s): CE01993
Dear Joe Ladd,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, February 16, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
O"6LC'=-:;tA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 14

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: Clarifier 2
Lab ID: CE01993-01
Sampled: 02/16/21 07:30
Received: 02/16/21 08:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 1010A
NO PREP
03/02/21
02/25/21 08:00
02/25/21 10:17
EPA 6010D
EPA 3010A
08/15/21
08/23/21
02/24/21 16:17
02/25/21 13:03
EPA 7470A
EPA 7470A
03/16/21
03/24/21
02/24/21 12:34
02/25/21 09:51
EPA 8260D
EPA 503013_MS
03/02/21
03/11/21
02/25/21 00:00
02/25/21 13:36
EPA 8270E
EPA 3510C_MS
02/23/21
04/05/21
02/24/21 06:25
02/24/21 21:48
EPA 9040C
NO PREP
02/16/21 07:44
03/03/21 12:47
03/03/21 14:26
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 14

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SAMPLE DETECTION SUMMARY
Client ID: Clarifier 2 Lab ID: CE01993-03
Analvte Results Flag MDL Q Units Method Notes
pH
Temperature for pH (deg. Q
7.8 1.0 1.0 pH Units EPA 9040C Q-01
20 pH Units EPA 9040C Q-01
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 14

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ANALYTICAL RESULTS
Description: Clarifier 2 Lab Sample ID:CE01993-01 Received: 02/16/21 08:00
Matrix: Waste Water Sampled: 02/16/2107:30 Work Order: CE01993
Project: SBMPWW2021 Sampled By:Adam Fauccette
TCLP Volatile Organics by GCMS
^ - ENCO Orlando certified analyte [NC 424]
Analvte FCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,1-Dichloroethene [75-35-4]^
0.094
UD
mg/L
100
0.094
0.10
1B25018
EPA 8260D
02/25/21 13:36
kkw
1,2-Dichloroethane [107-06-2]^
0.063
UD
mg/L
100
0.063
0.10
1B25018
EPA 8260D
02/25/21 13:36
kkw
2-Butanone [78-93-3]^
0.45
UD
mg/L
100
0.45
0.50
1B25018
EPA 8260D
02/25/21 13:36
kkw
Benzene[71-43-2]^
0.071
UD
mg/L
100
0.071
0.10
1B25018
EPA 8260D
02/25/21 13:36
kkw
Carbon Tetrachloride [56-23-5]^
0.094
UD
mg/L
100
0.094
0.10
1B25018
EPA 8260D
02/25/21 13:36
kkw
Chlorobenzene [108-90-7]^
0.072
UD
mg/L
100
0.072
0.10
1B25018
EPA 8260D
02/25/21 13:36
kkw
Chloroform [67-66-3]^
0.080
UD
mg/L
100
0.080
0.10
1B25018
EPA 8260D
02/25/21 13:36
kkw
Tetrachloroethene [127-18-4]^
0.076
UD
mg/L
100
0.076
0.10
1B25018
EPA 8260D
02/25/21 13:36
kkw
Trichloroethene [79-01-6]^
0.089
UD
mg/L
100
0.089
0.10
1B25018
EPA 8260D
02/25/21 13:36
kkw
Vinyl chloride [75-01-4]^
0.071
UD
mg/L
100
0.071
0.10
1B25018
EPA 8260D
02/25/21 13:36
kkw
Surrogates
Results
DF
Spike L v/
% Rec
% Rec Limits
Batch
Method
Analvzed
"
Notes
4-8romofluorobenzene
0.047
1
0,0500
94 %
41-142
1825018
EPA 8260D
02125121 13:36
kkw
Dibromofluoromethane
0.057
1
0,0500
114 %
53-146
1825018
EPA 8260D
02125121 13:36
kkw
Toluene-&
0,049
1
amo
98 %
41-146
1825018
EPA 8260D
02125121 13:36
kkw
TCLP Semivolatile Organics by GCMS
^ - ENCO Orlando certified analyte [NC 424]
Analvte MAS Numberl
Results
Flaa
Units
DF
MDL I•Q
Batch
Method
Analyzed
gy
Notes
1,4-Dichlorobenzene [106-46-7]^
0.02
UD
mg/L
5
0.02 0.05
1B23004
EPA 8270E
02/24/21 21:48
jfi
2,4,5-Trichlorophenol [95-95-4]^
0.02
UD
mg/L
5
0.02 0.05
1B23004
EPA 8270E
02/24/21 21:48
jfi
2,4,6-Trichlorophenol [88-06-2]^
0.03
UD
mg/L
5
0.03 0.05
1B23004
EPA 8270E
02/24/21 21:48
jfi
2,4-Dinitrotoluene [121-14-2]^
0.02
UD
mg/L
5
0.02 0.05
1B23004
EPA 8270E
02/24/21 21:48
jfi
2-Methylphenol [95-48-7]^
0.02
UD
mg/L
5
0.02 0.05
1B23004
EPA 8270E
02/24/21 21:48
jfi
3 & 4-Methylphenol [108-39-4/106-44-5]^
0.04
UD
mg/L
5
0.04 0.05
1B23004
EPA 8270E
02/24/21 21:48
jfi
QV-01
Hexachlorobenzene [118-74-1]^
0.02
UD
mg/L
5
0.02 0.05
1B23004
EPA 8270E
02/24/21 21:48
jfi
Hexachlorobutadiene [87-68-3]^
0.02
UD
mg/L
5
0.02 0.05
1B23004
EPA 8270E
02/24/21 21:48
jfi
Hexachloroethane [67-72-1]^
0.02
UD
mg/L
5
0.02 0.05
1B23004
EPA 8270E
02/24/21 21:48
jfi
Nitrobenzene [98-95-3]^
0.02
UD
mg/L
5
0.02 0.05
1B23004
EPA 8270E
02/24/21 21:48
jfi
Pentachlorophenol [87-86-5]^
0.04
UD
mg/L
5
0.04 0.05
1B23004
EPA 8270E
02/24/21 21:48
jfi
QV-01
Pyridine [110-86-1]^
0.02
UD
mg/L
5
0.02 0.05
1B23004
EPA 8270E
02/24/21 21:48
jfi
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
2,4,6-Tribromophenol
0.30
5
0.250
120 %
33-145
1823004
EPA 8270E
0212412121:48
jfl
2-Fluorobiphenyl
0.18
5
0.250
72 %
32-116
1823004
EPA 8270E
0212412121:48
jfi
2-Fluorophenol
0.11
5
0.250
44 %
11-100
1823004
EPA 8270E
0212412121:48
jfi
Nitrobenzene-d5
0.17
5
0.250
68 %
24-107
1823004
EPA 8270E
0212412121:48
if/
Phenol-d5
0.077
5
0.250
31 %
10-100
1823004
EPA 8270E
0212412121:48
if/
Terphenyl-d14
0.30
5
0.250
118 %
52-150
1323004
EPA 8270E
0212412121:48
if/
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 14

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ANALYTICAL RESULTS
Description: Clarifier 2 Lab Sample ID:CE01993-01 Received: 02/16/21 08:00
Matrix: Waste Water Sampled: 02/16/2107:30 Work Order: CE01993
Project: SBMPWW2021 Sampled By:Adam Fauccette
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Orlando certified analyte [NC 424]
Analyte fCAS Numberl Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
Arsenic[7440-38-2]^ 0.110
U
mg/L
1
0.110
0.500
1B24006
EPA 6010D
02/25/21 13:03
JSS
Barium [7440-39-3]^ 0.140
U
mg/L
1
0.140
0.500
1B24006
EPA 6010D
02/25/21 13:03
JSS
Cadmium [7440-43-9]^ 0.0200
U
mg/L
1
0.0200
0.0500
1B24006
EPA 6010D
02/25/21 13:03
JSS
Chromium [7440-47-3]^ 0.110
U
mg/L
1
0.110
0.250
1B24006
EPA 6010D
02/25/21 13:03
JSS
Lead [7439-92-1]^ 0.110
U
mg/L
1
0.110
0.250
1B24006
EPA 6010D
02/25/21 13:03
JSS
Mercury [7439-97-6]^ 0.000230
U
mg/L
1
0.000230
0.00200
1B24003
EPA 7470A
02/25/21 09:51
SSE
Selenium [7782-49-2]^ 0.600
U
mg/L
1
0.600
1.00
1B24006
EPA 6010D
02/25/21 13:03
JSS
Silver[7440-22-4]^ 0.0800
U
mg/L
1
0.0800
0.250
1B24006
EPA 6010D
02/25/21 13:03
JSS
Classical Chemistry Parameters
^ - ENCO Orlando certified analyte [NC 424]
Analyte fCAS Numberl Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
pH^ 7.8
pH Units
1
1.0
1.0
1B27007
EPA 9040C
03/03/21 14:26
ASR
Q-01
Temperature for pH (deg. Q 20
pH Units
1
1B27007
EPA 9040C
03/03/21 14:26
ASR
Q-01
Classical Chemistry Parameters
^ - ENCO Jacksonville certified analyte [NC 442]
Analyte fCAS Numberl
ASTMD93 PMCC Flashpoint^
Results Flaa Units DF MDL P L Batch Method Analyzed AX Notes
> 200 of 1 1B23003 EPA 1010A 02/25/21 10:17 LTS
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 14

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QUALITY CONTROL DATA
TCLP Volatile Organics by GCMS - Quality Control
Batch 1825018 - EPA 5030E MS
Blank (1B25018-BLK3) Prepared: 02/25/2021 00:00 Analyzed: 02/25/2021 11:41
Analvte
Result
Flaq
POL
Units
1,1-Dichloroethene
0.00094
U
0.0010
mg/L
1,2-Dichloroethane
0.00063
U
0.0010
mg/L
2-Butanone
0.0045
U
0.0050
mg/L
Benzene
0.00071
U
0.0010
mg/L
Carbon Tetrachloride
0.00094
U
0.0010
mg/L
Chlorobenzene
0.00072
U
0.0010
mg/L
Chloroform
0.00080
U
0.0010
mg/L
Tetrachloroethene
0.00076
U
0.0010
mg/L
Trichloroethene
0.00089
U
0.0010
mg/L
Vinyl chloride
0.00071
U
0.0010
mg/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
4-Bromofluorobenzene 0.044 m91L 0.0500 68 41-142
Dibromofluoromethane 0.056 m91L 0.0500 111 53-146
Toluene-d8 0.047 m91L 0.0500 94 41-146
Blank (1B25018-BLK2) Prepared: 02/25/2021 00:00 Analyzed: 02/25/2021 11:13
Spike
Source
%REC RPD
Analvte
Result
Flaq
POL
Units
Level
Result %REC
Limits RPD Limit Notes
1,1-Dichloroethene
0.094
UD
0.10
mg/L
1,2-Dichloroethane
0.063
UD
0.10
mg/L
2-Butanone
0.45
UD
0.50
mg/L
Benzene
0.071
UD
0.10
mg/L
Carbon Tetrachloride
0.094
UD
0.10
mg/L
Chlorobenzene
0.072
UD
0.10
mg/L
Chloroform
0.080
UD
0.10
mg/L
Tetrachloroethene
0.076
UD
0.10
mg/L
Trichloroethene
0.089
UD
0.10
mg/L
Vinyl chloride
0.071
UD
0.10
mg/L
4-Bromofluorobenzene
0.047
m91L
0.0500
94
41-142
Dibromofluoromethane
0.057
m91L
0.0500
114
53-146
Toluene-d8
0.049
m91L
0.0500
97
41-146
LCS (1B25018-BS1)
Prepared: 02/25/2021 00:00 Analyzed: 02/25/2021 08:49
Spike
Source
%REC RPD
Analvte
Result
Flaq POL
Units
Level
Result %REC
Limits RPD Limit Notes
1,1-Dichloroethene
0.019
0.0010
mg/L
0.0200
94
47-139
Benzene
0.020
0.0010
mg/L
0.0200
100
56-136
Chlorobenzene
0.020
0.0010
mg/L
0.0200
100
51-139
Trichloroethene
0.020
0.0010
mg/L
0.0200
100
62-135
4-Bromofluorobenzene
0.051
m91L
0.0500
103
41-142
Dibromofluoromethane
0.051
m91L
0.0500
102
53-146
Toluene-d8
0.053
m91L
0.0500
107
41-146
Matrix Spike (1B25018-MS3)
Prepared: 02/25/2021 00:00 Analyzed: 02/25/2021 09:18
Source: AE01306-01
Spike
Source
%REC RPD
Analvte
Result Flaq POL
Units
Level
Result
%REC
Limits RPD Limit Notes
1,1-Dichloroethene
0.024 0.0010
mg/L
0.0200
0.00094 U
118
47-139
Benzene
0.022 0.0010
mg/L
0.0200
0.00071 U
110
56-136
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 14

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QUALITY CONTROL DATA
TCLP Volatile Organics by GCMS - Quality Control
Batch IB25018 - EPA 5030E MS - Continued
Matrix Spike (1B25018-MS3) Continued Prepared: 02/25/2021 00:00 Analyzed: 02/25/2021 09:18
Source: AE01306-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Chlorobenzene
0.021
0.0010
mg/L
0.0200
0.00072 U
105
51-139
Trichloroethene
0.022
0.0010
mg/L
0.0200
0.00089 U
111
62-135
4-Bromofluorobenzene
0.048
mg/L
0.0500
96
41-142
Dibromofluoromethane
0.055
m91L
0.0500
111
53-146
Toluene-d8
0.049
m91L
0.0500
98
41-146
Matrix Spike Dup (1B25018-MSD1)
Prepared: 02/25/2021 00:00 Analyzed: 02/25/2021 09:46
Source: AE01306-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
0.022
0.0010
mg/L
0.0200
0.00094 U
ill
47-139
16
Benzene
0.021
0.0010
mg/L
0.0200
0.00071 U
105
56-136
14
Chlorobenzene
0.021
0.0010
mg/L
0.0200
0.00072 U
103
51-139
13
Trichloroethene
0.021
0.0010
mg/L
0.0200
0.00089 U
106
62-135
20
4-Bromofluorobenzene
0.048
mg/L
0.0500
96
41-142
Dibromofluoromethane
0.055
mg/L
0.0500
110
53-146
Toluene-d8
0.049
m91L
0.0500
96
41-146
TCLP Semivolatile Organics by GCMS - Quality Control
Batch IB23004 - EPA 3510C MS
Blank (1B23004-BLK3)
Prepared: 02/23/2021 06:30 Analyzed: 02/24/2021 15:19
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,4-Dichlorobenzene
0.0006
U
0.002
mg/L
2,4,5-Trichlorophenol
0.0008
U
0.002
mg/L
2,4,6-Trichlorophenol
0.001
U
0.002
mg/L
2,4-Dinitrotoluene
0.0006
U
0.002
mg/L
2-Methylphenol
0.0007
U
0.002
mg/L
3 & 4-Methylphenol
0.002
U
0.002
mg/L
Hexachlorobenzene
0.0006
U
0.002
mg/L
Hexachlorobutadiene
0.0008
U
0.002
mg/L
Hexachloroethane
0.0006
U
0.002
mg/L
Nitrobenzene
0.0006
U
0.002
mg/L
Pentachlorophenol
0.002
U
0.002
mg/L
Pyridine
0.0007
U
0.002
mg/L
2,4,6-Tribromophenol
0.046
mg/L
0.0500
92
33-145
2-Fluorob/phenyl
0.041
m91L
0.0500
82
32-116
2-Fluorophenol
0.030
m91L
0.0500
59
11-100
Nitrobenzene-d5
0.042
m91L
0.0500
83
24-107
P17enol-d5
0.022
m91L
0.0500
44
10-100
Terphenyl-d14
0.052
m91L
0.0500
104
52-150
Blank (1B23004-BLK2)
Prepared: 02/24/2021 06:25 Analyzed: 02/24/2021 15:48
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
1,4-Dichlorobenzene 0.003 U 0.01 mg/L
2,4,5-Trichlorophenol 0.004 U 0.01 mg/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 14

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QUALITY CONTROL DATA
TCLP Semivolatile Organics by GCMS - Quality Control
Batch IB23004 - EPA 3510C MS - Continued
Blank (1B23004-BLK2) Continued Prepared: 02/24/2021 06:25 Analyzed: 02/24/2021 15:48
Analvte
Result
Flaq
POL
Units
2,4,6-Trichlorophenol
0.006
U
0.01
mg/L
2,4-Dinitrotoluene
0.003
U
0.01
mg/L
2-Methylphenol
0.004
U
0.01
mg/L
3 & 4-Methylphenol
0.008
U
0.01
mg/L
Hexachlorobenzene
0.003
U
0.01
mg/L
Hexachlorobutadiene
0.004
U
0.01
mg/L
Hexachloroethane
0.003
U
0.01
mg/L
Nitrobenzene
0.003
U
0.01
mg/L
Pentachlorophenol
0.008
U
0.01
mg/L
Pyridine
0.004
U
0.01
mg/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
2,4,6-Tribromophenol
0.23
m91L
0,250
92
33-145
2-Fluorobiphenyl
0.16
m91L
0.250
65
32-116
2-Fluo-phenol
0.12
m91L
a250
49
11-100
Nitrobenzene-d5
0.17
m91L
0,250
66
24-107
Phenol-d5
0,092
m91L
a250
37
10-100
Terphenyl-dM
0.26
m91L
0.250
103
52-150
Blank (1B23004-BLK3)
Prepared: 02/24/2021 06:25 Analyzed: 02/24/2021 16:18
Analvte
Result
Flaq
POL
Units
1,4-Dichlorobenzene
0.003
U
0.01
mg/L
2,4,5-Trichlorophenol
0.004
U
0.01
mg/L
2,4,6-Trichlorophenol
0.006
U
0.01
mg/L
2,4-Dinitrotoluene
0.003
U
0.01
mg/L
2-Methylphenol
0.004
U
0.01
mg/L
3 & 4-Methylphenol
0.008
U
0.01
mg/L
Hexachlorobenzene
0.003
U
0.01
mg/L
Hexachlorobutadiene
0.004
U
0.01
mg/L
Hexachloroethane
0.003
U
0.01
mg/L
Nitrobenzene
0.003
U
0.01
mg/L
Pentachlorophenol
0.008
U
0.01
mg/L
Pyridine
0.004
U
0.01
mg/L
Spike Source %REC RPD
Level Result %REC Limi RPD Mina Notes
2,4,6-Tribromophenol
0.19
m91L
0.250
77
33-145
2-Fluorobiphenyl
0.14
m91L
0,250
56
32-116
2-Fiuorophenol
0.099
m91L
0.250
40
11-100
Nitrobenzene-d5
0.14
m91L
0.250
56
24-107
Phenol-d5
0,071
m91L
0,250
29
10-100
Terphenyl-dM
0.23
m91L
0.250
93
52-150
LCS (1B23004-BS1)
Prepared: 02/23/202106:30 Analyzed: 02/24/2021 16:48
Spike
Source
%REC RPD
Analvte
Result Flaq POL
Units
Level
Result %REC
Limits RPD Limit Notes
1,4-Dichlorobenzene
0.05 0.002
mg/L
0.0500
95
10-101
Pentachlorophenol
0.06 0.002
mg/L
0.0500
112
5-139
2,4,6-Tribromophenol
0,053
m9/L
0.0500
105
33-145
2-Fluorobiphenyl
0.040
m91L
0.0500
79
32-116
2-Fluorophenol
0,031
m91L
0.0500
62
11-100
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 14

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QUALITY CONTROL DATA
TCLP Semivolatile Organics by GCMS - Quality Control
Batch 1 B23004 - EPA 3510C MS - Continued
LCS (1B23004-BSI) Continued Prepared: 02/23/2021 06:30 Analyzed: 02/24/2021 16:48
Spike Source %REC RPD
Analvte
Result Flaq POL
Units
Level Result %REC Limits RPD Limit Notes
Nitrobenzene-d5
0.046
m91L
0.0500 93 24-107
Phenol-d5
0.023
m91L
0.0500 47 10-100
Terphenyl-d14
0.051
m91L
0.0500 102 52-150
Matrix Spike (1B23004-MS1)
Prepared: 02/23/2021 06:30 Analyzed: 02/24/2021 17:18
Source: AE01385-01
Spike
Source
%REC RPD
Analvte
Result Flaq POL Units
Level
Result
%REC Limits RPD Limit Notes
1,4-Dichlorobenzene
0.04 0.002 mg/L
0.0500
0.0006 U
90 10-101
Pentachlorophenol
0.05 0.002 mg/L
0.0500
0.002 U
108 5-139
2,4,6-Tribromopheno/
0.051
m91L
0.0500
102
33-145
2-Fluorobiphenyl
0.039
m91L
0.0500
77
32-116
2-Fluorophenol
0.030
m91L
0.0500
60
11-100
Nitrobenzene-d5
0.044
m91L
0.0500
89
24-107
Phenol-d5
0.022
m91L
0.0500
45
10-100
Terphenyl-d14
0.050
m91L
0.0500
99
52-150
Matrix Spike (1B23004-MS2)
Prepared: 02/24/2021 06:25 Analyzed: 02/25/2021 13:50
Source: AE01370-01
Spike
Source
%REC RPD
Analvte
Result Flaq POL Units
Level
Result
%REC Limits RPD Limit Notes
1,4-Dichlorobenzene
0.13 D 0.05 mg/L
0.250
0.02 U
51 10-101
Pentachlorophenol
0.16 D 0.05 mg/L
0.250
0.04 U
64 5-139
2,4,6-Tribromopheno/
0.22
m91L
0.250
66
33-145
2-Fluorobiphenyl
0.16
m91L
0.250
65
32-116
2-Fluorop17enol
0.078
m91L
0.250
31
11-100
Nitrobenzene-d5
0.15
m91L
0.250
59
24-107
Phenol-d5
0.069
m91L
0.250
28
10-100
Terphenyl-d14
0.23
m91L
0.250
93
52-150
Matrix Spike Dup (1B23004-MSD1)
Prepared: 02/23/2021 06:30 Analyzed: 02/24/2021 17:47
Source: AE01385-01
Spike
Source
%REC
RPD
Analvte
Result Flaq POL Units
Level
Result
%REC Limits RPD
Limit Notes
1,4-Dichlorobenzene
0.04 0.002 mg/L
0.0500
0.0006 U
80 10-101 11
18
Pentachlorophenol
0.05 0.002 mg/L
0.0500
0.002 U
108 5-139 0.5
23
2,4,6-Tribromopheno/ 0.049
m91L
0.0500
99
33-145
2-Fluorobiphenyl 0.036
m91L
0.0500
72
32-116
2-Fluorophenol 0.026
m91L
0.0500
57
11-100
Nitrobenzene-d5 0.041
m91L
0.0500
83
24-107
Phenol-d5 0.022
m91L
0.0500
43
10-100
Terphenyl-d14 0.047
m91L
0.0500
94
52-150
TCLP Metals by 6000/7000 Series Methods - Quality Control
Batch IB24003 - EPA 7470A
Blank (1B24003-BLK1) Prepared: 02/24/2021 10:39 Analyzed: 02/25/2021 08:14
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 14

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QUALITY CONTROL DATA
TCLP Metals by 6000/7000 Series Methods - Quality Control
Batch 1B24003 - EPA 7470A - Continued
Blank (SB24003-BLK1) Continued Prepared: 02/24/2021 10:39 Analyzed: 02/25/2021 08:14
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Mercury 2.30E-5 U 0.000200 mg/L
Blank (1B24003-BLK2) Prepared: 02/24/2021 10:39 Analyzed: 02/25/2021 08:17
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Mercury 0.000230 U 0.00200 mg/L
Blank (1B24003-BLK3) Prepared: 02/24/2021 10:39 Analyzed: 02/25/2021 08:21
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Mercury 0.000230 U 0.00200 mg/L
Blank (1B24003-BLK4) Prepared: 02/24/2021 12:34 Analyzed: 02/25/2021 08:24
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Mercury 0.000230 U 0.00200 mg/L
LCS (1B24003-BS1) Prepared: 02/24/2021 10:39 Analyzed: 02/25/2021 08:27
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Mercury
0.00504
0.000200
mg/L
0.00500
101
80-120
Matrix Spike (1B24003-MS3)
Prepared: 02/24/2021 10:39 Analyzed: 02/25/2021 08:33
Source: AE01121-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Mercury
0.0503
0.00200
mg/L
0.0500
0.000230 U
101
75-125
Matrix Spike Dup (1B24003-MSDS)
Prepared: 02/24/2021 10:39 Analyzed: 02/25/2021 08:36
Source: AE01121-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Mercury
0.0511
0.00200
mg/L
0.0500
0.000230 U
102
75-125 2
20
Batch 1824006 - EPA 3010A
Blank (1B24006-BLK3) Prepared: 02/24/2021 16:17 Analyzed: 02/25/2021 10:53
Analvte
Result
Flaq
POL
Units
Arsenic
0.110
U
0.500
mg/L
Barium
0.140
U
0.500
mg/L
Cadmium
0.0200
U
0.0500
mg/L
Chromium
0.110
U
0.250
mg/L
Lead
0.110
U
0.250
mg/L
Selenium
0.600
U
1.00
mg/L
Silver
0.0800
U
0.250
mg/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit
Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 14

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QUALITY CONTROL DATA
TCLP Metals by 6000/7000 Series Methods - Quality Control
Batch IB24006 - EPA 3010A - Continued
Blank (1B24006-BLK2)
Prepared: 02/24/2021 16:17 Analyzed: 02/25/2021 10:57
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Arsenic
0.110
U
0.500
mg/L
Barium
0.140
U
0.500
mg/L
Cadmium
0.0200
U
0.0500
mg/L
Chromium
0.110
U
0.250
mg/L
Lead
0.110
U
0.250
mg/L
Selenium
0.600
U
1.00
mg/L
Silver
0.0800
U
0.250
mg/L
Blank (1B24006-BLK3)
Prepared: 02/24/2021 16:17 Analyzed: 02/25/2021 11:00
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Arsenic
0.110
U
0.500
mg/L
Barium
0.140
U
0.500
mg/L
Cadmium
0.0200
U
0.0500
mg/L
Chromium
0.110
U
0.250
mg/L
Lead
0.110
U
0.250
mg/L
Selenium
0.600
U
1.00
mg/L
Silver
0.0800
U
0.250
mg/L
Blank (1B24006-BLK4)
Prepared: 02/24/2021 16:17 Analyzed: 02/25/2021 11:04
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Arsenic
0.110
U
0.500
mg/L
Barium
0.140
U
0.500
mg/L
Cadmium
0.0200
U
0.0500
mg/L
Chromium
0.110
U
0.250
mg/L
Lead
0.110
U
0.250
mg/L
Selenium
0.600
U
1.00
mg/L
Silver
0.0800
U
0.250
mg/L
LCS (1B24006-BSI)
Prepared: 02/24/2021 16:17 Analyzed: 02/25/2021 11:08
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Arsenic
12.8
0.500
mg/L
12.5 102 80-120
Barium
12.6
0.500
mg/L
12.4 102 80-120
Cadmium
1.24
0.0500
mg/L
1.24 100 80-120
Chromium
12.4
0.250
mg/L
12.5 100 80-120
Lead
12.3
0.250
mg/L
12.6 98 80-120
Selenium
12.4
1.00
mg/L
12.5 99 80-120
Silver
2.16
0.250
mg/L
2.29 94 80-120
Matrix Spike (1B24006-MS1)
Prepared: 02/24/2021 16:17 Analyzed: 02/25/2021 11:15
Source: AE01121-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Arsenic
12.8
0.500
mg/L
12.5 0.110 U 103 75-125
Barium
12.5
0.500
mg/L
12.4 0.140 U 100 75-125
Cadmium
1.23
0.0500
mg/L
1.24 0.0216 97 75-125
Chromium
12.3
0.250
mg/L
12.5 0.110 U 98 75-125
FINAL
This report relates only to the sample as received by the
laboratory, and may only be reproduced in full.
Page 11 of 14

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QUALITY CONTROL DATA
TCLP Metals by 6000/7000 Series Methods - Quality Control
Batch IB24006 - EPA 3010A - Continued
Matrix Spike (11324006-14S3) Continued
Prepared: 02/24/2021 16:17 Analyzed: 02/25/2021 11:15
Source: AE01121-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Lead
12.1
0.250
mg/L
12.6
0.110 U
97
75-125
Selenium
12.4
1.00
mg/L
12.5
0.600 U
99
75-125
Silver
2.13
0.250
mg/L
2.29
0.0800 U
93
75-125
Matrix Spike Dup (11324006-MSDS)
Prepared: 02/24/2021 16:17 Analyzed: 02/25/2021 11:18
Source: AE01121-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Arsenic
12.8
0.500
mg/L
12.5
0.110 U
103
75-125
0.009
20
Barium
12.5
0.500
mg/L
12.4
0.140 U
100
75-125
0.06
20
Cadmium
1.23
0.0500
mg/L
1.24
0.0216
97
75-125
0.3
20
Chromium
12.3
0.250
mg/L
12.5
0.110 U
98
75-125
0.2
20
Lead
12.1
0.250
mg/L
12.6
0.110 U
96
75-125
0.3
20
Selenium
12.5
1.00
mg/L
12.5
0.600 U
100
75-125
0.5
20
Silver
2.15
0.250
mg/L
2.29
0.0800 U
94
75-125
1
20
Classical Chemistry Parameters - Quality Control
Batch IB27007 - NO PREP
LCS (1627007-113SI) Prepared: 03/03/2021 12:47 Analyzed: 03/03/2021 14:26
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits
RPD
Limit
Notes
pH
7.0
1.0
pH Units
7.00
100 99-102
Duplicate (111327007-DUP3)
Prepared: 03/03/2021 12:47 Analyzed: 03/03/2021 14:26
Source: CE01993-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits
RPD
Limit
Notes
pH
7.9
1.0
pH Units
7.8
0.1
10
Q-01
Temperature for pH (deg. C)
20
pH Units
20
0
200
Q-01
Classical Chemistry Parameters -
Quality Control
Batch IB23003 - NO PREP
LCS (111323003-13SI) Prepared: 02/25/2021 08:00 Analyzed: 02/25/2021 08:07
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
ASTMD93 PMCC Flashpoint 81.0 OF 81.0 100 98-102
Duplicate (11323003-DUPIL) Prepared: 02/25/2021 08:00 Analyzed: 02/25/2021 12:13
Source: BE00472-01
Analvte
ASTMD93 PMCC Flashpoint
Spike Source %REC
Result Flaq POL Units Level Result %REC Limits RPD
> 200 U OF 200 0.00
RPD
Limit Notes
5
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 14

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
Q-01 Analysis performed outside of method - specified holding time.
QV-01 The associated continuing calibration verification standard exhibited high bias; since the result is ND, there
is no impact.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 14

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ler #'s & Temps on Receipt
rL--, - �,� A 0 l
Condition upon Receipt
�-- Acceptable Unacceptab(e
Matrix 7 GW-Groundwater SOSoilDW-Drinking Water SE-Sadiment SW -Surface Water WW-Wastewater A -Air O-Other detail In comments) Preservation: I -Ice H-HCI N-H{403 S-H2SO4 NO-NaOH O.Other (detail in comments)
Note : All samples submitted to ENCO Labs are in accordance with the lemis and conditions listed on the reverse of this form, unless prior written agreements exist

2�SQ pCCgF ENCO Laboratories
9e0
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Thursday, March 4, 2021
Novozymes North America (N0008)
Attn: Joe Ladd
77 Perry Chapel Church Road
Franklinton, NC 27525
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: SBMPWW2021
ENCO Workorder(s): CE01842
Dear Joe Ladd,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, February 16, 2021.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
O"6LC'=-:;tA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 14

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: SBM C Side
Lab ID: CE01842-01
Sampled: 02/16/21 07:05
Received: 02/16/21 08:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 1010A
NO PREP
03/02/21
02/25/21 08:00
02/25/21 09:15
EPA 6010D
EPA 3010A
08/15/21
08/23/21
02/24/21 16:17
02/25/21 12:59
EPA 7470A
EPA 7470A
03/16/21
03/24/21
02/24/21 12:34
02/25/21 09:48
EPA 8260D
EPA 503013_MS
03/02/21
03/11/21
02/25/21 00:00
02/25/21 13:08
EPA 8270E
EPA 3510C_MS
02/23/21
04/05/21
02/24/21 06:25
02/24/21 19:50
EPA 9045D
NO PREP
03/03/21 13:01
03/03/21 12:47
03/03/21 14:48
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 14

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SAMPLE DETECTION SUMMARY
Client ID: SBM C Side
Lab ID:
CE01842-01
Analvte
Results
Flag MDL
Q
Units
Method
Notes
Cadmium - TCLP
0.0235
3 0.0200
0.0500
mg/L
EPA 6010D
Lead - TCLP
0.121
3 0.110
0.250
mg/L
EPA 6010D
pH
11
1.0
1.0
pH Units
EPA 9045D
Q-01
Temperature for pH (deg. C)
20
pH Units
EPA 9045D
Q-01
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 14

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ANALYTICAL RESULTS
Description: SBM C Side Lab Sample ID:CE01842-01 Received: 02/16/21 08:00
Matrix: Solid Sampled: 02/16/2107:05 Work Order: CE01842
Project: SBMPWW2021 Sampled By:Adam Fauccette % Solids:
TCLP Volatile Organics
by GCMS
A - ENCO Orlando certified analyte [NC 424]
Analyte KAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay Notes
1,1-Dichloroethene [75-35-4]^
0.094
UD
mg/L
100
0.094
0.10
1B25018
EPA 8260D
02/25/21
13:08
kkw
1,2-Dichloroethane [107-06-2]^
0.063
UD
mg/L
100
0.063
0.10
1B25018
EPA 8260D
02/25/21
13:08
kkw
2-Butanone [78-93-3]^
0.45
UD
mg/L
100
0.45
0.50
1B25018
EPA 8260D
02/25/21
13:08
kkw
Benzene [71-43-2]^
0.071
UD
mg/L
100
0.071
0.10
1B25018
EPA 8260D
02/25/21
13:08
kkw
Carbon Tetrachloride [56-23-5]^
0.094
UD
mg/L
100
0.094
0.10
1B25018
EPA 8260D
02/25/21
13:08
kkw
Chlorobenzene [108-90-7]^
0.072
UD
mg/L
100
0.072
0.10
1B25018
EPA 8260D
02/25/21
13:08
kkw
Chloroform [67-66-3]^
0.080
UD
mg/L
100
0.080
0.10
1B25018
EPA 8260D
02/25/21
13:08
kkw
Tetrachloroethene [127-18-4]^
0.076
UD
mg/L
100
0.076
0.10
1B25018
EPA 8260D
02/25/21
13:08
kkw
Trichloroethene [79-01-6]^
0.089
UD
mg/L
100
0.089
0.10
1B25018
EPA 8260D
02/25/21
13:08
kkw
Vinyl chloride [75-01-4]^
0.071
UD
mg/L
100
0.071
0.10
1B25018
EPA 8260D
02/25/21
13:08
kkw
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
0.047
1
0.0500
94 %
41-142
IB25016
EPA 6260D
02125121 13:08
kkw
Dibromofluoromethane
0.056
1
0.0500
115 %
53-146
IB25016
EPA 6260D
02125121 13:08
kkw
Toluene-&
0.049
1
0.0500
97 %
41-146
IB25016
EPA 6260D
02125121 13:08
kkw
TCLP Semivolatile Organics by GCMS
A - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dichlorobenzene [106-46-7]^
0.02
UD
mg/L
5
0.02 0.05
1B23004
EPA 8270E
02/24/21 19:50
jfi
2,4,5-Trichlorophenol [95-95-4]^
0.02
UD
mg/L
5
0.02 0.05
1B23004
EPA 8270E
02/24/21 19:50
jfi
2,4,6-Trichlorophenol [88-06-2]^
0.03
UD
mg/L
5
0.03 0.05
1B23004
EPA 8270E
02/24/21 19:50
jfi
2,4-Dinitrotoluene [121-14-2]^
0.02
UD
mg/L
5
0.02 0.05
1B23004
EPA 8270E
02/24/21 19:50
jfi
2-Methylphenol [95-48-7]^
0.02
UD
mg/L
5
0.02 0.05
1B23004
EPA 8270E
02/24/21 19:50
jfi
3 & 4-Methylphenol[108-39-4/106-44-5]^
0.04
UD
mg/L
5
0.04 0.05
1B23004
EPA 8270E
02/24/21 19:50
jfi
QV-01
Hexachlorobenzene [118-74-1]^
0.02
UD
mg/L
5
0.02 0.05
1B23004
EPA 8270E
02/24/21 19:50
jfi
Hexachlorobutadiene [87-68-3]^
0.02
UD
mg/L
5
0.02 0.05
1B23004
EPA 8270E
02/24/21 19:50
jfi
Hexachloroethane [67-72-1]^
0.02
UD
mg/L
5
0.02 0.05
1B23004
EPA 8270E
02/24/21 19:50
jfi
Nitrobenzene [98-95-3]^
0.02
UD
mg/L
5
0.02 0.05
1B23004
EPA 8270E
02/24/21 19:50
jfi
Pentachlorophenol [87-86-5]^
0.04
UD
mg/L
5
0.04 0.05
1B23004
EPA 8270E
02/24/21 19:50
jfi
QV-01
Pyridine [110-86-1]^
0.02
UD
mg/L
5
0.02 0.05
1B23004
EPA 8270E
02/24/21 19:50
jfi
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffly
Notes
2,4,6-Tribromophenol
0.22
5
0.250
90 %
33-145
1B23004
EPA 8270E
02124121 19:50
jfi
2-Fluorobiphenyl
0.19
5
0.250
75 %
32-116
1B23004
EPA 8270E
02124121 19:50
jfi
2-Fluorophenol
0.10
5
0.250
42 %
11-100
1 B23004
EPA 8270E
02124121 19:50
jfi
Nitrobenzene-d5
0.18
5
0.250
72 %
24-107
1B23004
EPA 8270E
02124121 19:50
jfi
Phenol-d5
0.074
5
0.250
30 %
10-100
IB23004
EPA 8270E
02124121 19:50
jfi
Terphenyl-d14
0.26
5
0.250
105 %
52-150
IS23004
EPA 8270E
02124121 19:50
jfi
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 14

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ANALYTICAL RESULTS
Description: SBM C Side Lab Sample ID:CE01842-01 Received: 02/16/21 08:00
Matrix: Solid Sampled: 02/16/2107:05 Work Order: CE01842
Project: SBMPWW2021 Sampled By:Adam Fauccette % Solids:
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Orlando certified analyte [NC 424]
Analyte fCAS Numberl Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
Arsenic[7440-38-2]^ 0.110
U
mg/L
1
0.110
0.500
1B24006
EPA 6010D
02/25/21 12:59
JSS
Barium [7440-39-3]^ 0.140
U
mg/L
1
0.140
0.500
1B24006
EPA 6010D
02/25/21 12:59
JSS
Cadmium [7440-43-9]^ 0.0235
J
mg/L
1
0.0200
0.0500
1B24006
EPA 6010D
02/25/21 12:59
JSS
Chromium [7440-47-3]^ 0.110
U
mg/L
1
0.110
0.250
1B24006
EPA 6010D
02/25/21 12:59
JSS
Lead [7439-92-1]^ 0.121
J
mg/L
1
0.110
0.250
1B24006
EPA 6010D
02/25/21 12:59
JSS
Mercury [7439-97-6]^ 0.000230
U
mg/L
1
0.000230
0.00200
1B24003
EPA 7470A
02/25/21 09:48
SSE
Selenium [7782-49-2]^ 0.600
U
mg/L
1
0.600
1.00
1B24006
EPA 6010D
02/25/21 12:59
JSS
Silver[7440-22-4]^ 0.0800
U
mg/L
1
0.0800
0.250
1B24006
EPA 6010D
02/25/21 12:59
JSS
Classical Chemistry Parameters
^ - ENCO Orlando certified analyte [NC 424]
Analyte fCAS Numberl Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
pH^ 11
pH Units
1
1.0
1.0
1B27008
EPA 9045D
03/03/21 14:48
ASR
Q-01
Temperature for pH (deg. C) 20
pH Units
1
1B27008
EPA 9045D
03/03/21 14:48
ASR
Q-01
Classical Chemistry Parameters
^ - ENCO Jacksonville certified analyte [NC 442]
Analyte fCAS Numberl
ASTMD93 PMCC Flashpoint^
Results Flaa Units DF MDL P L Batch Method Analyzed AX Notes
> 200 of 1 1B23003 EPA 1010A 02/25/21 09:15 LTS
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 14

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QUALITY CONTROL DATA
TCLP Volatile Organics by GCMS - Quality Control
Batch 1825018 - EPA 5030E MS
Blank (1B25018-BLK3) Prepared: 02/25/2021 00:00 Analyzed: 02/25/2021 11:41
Analvte
Result
Flaq
POL
Units
1,1-Dichloroethene
0.00094
U
0.0010
mg/L
1,2-Dichloroethane
0.00063
U
0.0010
mg/L
2-Butanone
0.0045
U
0.0050
mg/L
Benzene
0.00071
U
0.0010
mg/L
Carbon Tetrachloride
0.00094
U
0.0010
mg/L
Chlorobenzene
0.00072
U
0.0010
mg/L
Chloroform
0.00080
U
0.0010
mg/L
Tetrachloroethene
0.00076
U
0.0010
mg/L
Trichloroethene
0.00089
U
0.0010
mg/L
Vinyl chloride
0.00071
U
0.0010
mg/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
4-Bromofluorobenzene 0.044 m91L 0.0500 68 41-142
Dibromofluoromethane 0.056 m91L 0.0500 111 53-146
Toluene-d8 0.047 m91L 0.0500 94 41-146
Blank (1B25018-BLK2) Prepared: 02/25/2021 00:00 Analyzed: 02/25/2021 11:13
Spike
Source
%REC RPD
Analvte
Result
Flaq
POL
Units
Level
Result %REC
Limits RPD Limit Notes
1,1-Dichloroethene
0.094
UD
0.10
mg/L
1,2-Dichloroethane
0.063
UD
0.10
mg/L
2-Butanone
0.45
UD
0.50
mg/L
Benzene
0.071
UD
0.10
mg/L
Carbon Tetrachloride
0.094
UD
0.10
mg/L
Chlorobenzene
0.072
UD
0.10
mg/L
Chloroform
0.080
UD
0.10
mg/L
Tetrachloroethene
0.076
UD
0.10
mg/L
Trichloroethene
0.089
UD
0.10
mg/L
Vinyl chloride
0.071
UD
0.10
mg/L
4-Bromofluorobenzene
0.047
m91L
0.0500
94
41-142
Dibromofluoromethane
0.057
m91L
0.0500
114
53-146
Toluene-d8
0.049
m91L
0.0500
97
41-146
LCS (1B25018-BS1)
Prepared: 02/25/2021 00:00 Analyzed: 02/25/2021 08:49
Spike
Source
%REC RPD
Analvte
Result
Flaq POL
Units
Level
Result %REC
Limits RPD Limit Notes
1,1-Dichloroethene
0.019
0.0010
mg/L
0.0200
94
47-139
Benzene
0.020
0.0010
mg/L
0.0200
100
56-136
Chlorobenzene
0.020
0.0010
mg/L
0.0200
100
51-139
Trichloroethene
0.020
0.0010
mg/L
0.0200
100
62-135
4-Bromofluorobenzene
0.051
m91L
0.0500
103
41-142
Dibromofluoromethane
0.051
m91L
0.0500
102
53-146
Toluene-d8
0.053
m91L
0.0500
107
41-146
Matrix Spike (1B25018-MS3)
Prepared: 02/25/2021 00:00 Analyzed: 02/25/2021 09:18
Source: AE01306-01
Spike
Source
%REC RPD
Analvte
Result Flaq POL
Units
Level
Result
%REC
Limits RPD Limit Notes
1,1-Dichloroethene
0.024 0.0010
mg/L
0.0200
0.00094 U
118
47-139
Benzene
0.022 0.0010
mg/L
0.0200
0.00071 U
110
56-136
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 14

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QUALITY CONTROL DATA
TCLP Volatile Organics by GCMS - Quality Control
Batch IB25018 - EPA 5030E MS - Continued
Matrix Spike (1B25018-MS3) Continued Prepared: 02/25/2021 00:00 Analyzed: 02/25/2021 09:18
Source: AE01306-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Chlorobenzene
0.021
0.0010
mg/L
0.0200
0.00072 U
105
51-139
Trichloroethene
0.022
0.0010
mg/L
0.0200
0.00089 U
111
62-135
4-Bromofluorobenzene
0.048
mg/L
0.0500
96
41-142
Dibromofluoromethane
0.055
m91L
0.0500
111
53-146
Toluene-d8
0.049
m91L
0.0500
98
41-146
Matrix Spike Dup (1B25018-MSD1)
Prepared: 02/25/2021 00:00 Analyzed: 02/25/2021 09:46
Source: AE01306-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
0.022
0.0010
mg/L
0.0200
0.00094 U
ill
47-139
16
Benzene
0.021
0.0010
mg/L
0.0200
0.00071 U
105
56-136
14
Chlorobenzene
0.021
0.0010
mg/L
0.0200
0.00072 U
103
51-139
13
Trichloroethene
0.021
0.0010
mg/L
0.0200
0.00089 U
106
62-135
20
4-Bromofluorobenzene
0.048
mg/L
0.0500
96
41-142
Dibromofluoromethane
0.055
mg/L
0.0500
110
53-146
Toluene-d8
0.049
m91L
0.0500
96
41-146
TCLP Semivolatile Organics by GCMS - Quality Control
Batch IB23004 - EPA 3510C MS
Blank (1B23004-BLK3)
Prepared: 02/23/2021 06:30 Analyzed: 02/24/2021 15:19
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,4-Dichlorobenzene
0.0006
U
0.002
mg/L
2,4,5-Trichlorophenol
0.0008
U
0.002
mg/L
2,4,6-Trichlorophenol
0.001
U
0.002
mg/L
2,4-Dinitrotoluene
0.0006
U
0.002
mg/L
2-Methylphenol
0.0007
U
0.002
mg/L
3 & 4-Methylphenol
0.002
U
0.002
mg/L
Hexachlorobenzene
0.0006
U
0.002
mg/L
Hexachlorobutadiene
0.0008
U
0.002
mg/L
Hexachloroethane
0.0006
U
0.002
mg/L
Nitrobenzene
0.0006
U
0.002
mg/L
Pentachlorophenol
0.002
U
0.002
mg/L
Pyridine
0.0007
U
0.002
mg/L
2,4,6-Tribromophenol
0.046
mg/L
0.0500
92
33-145
2-Fluorob/phenyl
0.041
m91L
0.0500
82
32-116
2-Fluorophenol
0.030
m91L
0.0500
59
11-100
Nitrobenzene-d5
0.042
m91L
0.0500
83
24-107
P17enol-d5
0.022
m91L
0.0500
44
10-100
Terphenyl-d14
0.052
m91L
0.0500
104
52-150
Blank (1B23004-BLK2)
Prepared: 02/24/2021 06:25 Analyzed: 02/24/2021 15:48
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
1,4-Dichlorobenzene 0.003 U 0.01 mg/L
2,4,5-Trichlorophenol 0.004 U 0.01 mg/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 14

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QUALITY CONTROL DATA
TCLP Semivolatile Organics by GCMS - Quality Control
Batch IB23004 - EPA 3510C MS - Continued
Blank (1B23004-BLK2) Continued Prepared: 02/24/2021 06:25 Analyzed: 02/24/2021 15:48
Analvte
Result
Flaq
POL
Units
2,4,6-Trichlorophenol
0.006
U
0.01
mg/L
2,4-Dinitrotoluene
0.003
U
0.01
mg/L
2-Methylphenol
0.004
U
0.01
mg/L
3 & 4-Methylphenol
0.008
U
0.01
mg/L
Hexachlorobenzene
0.003
U
0.01
mg/L
Hexachlorobutadiene
0.004
U
0.01
mg/L
Hexachloroethane
0.003
U
0.01
mg/L
Nitrobenzene
0.003
U
0.01
mg/L
Pentachlorophenol
0.008
U
0.01
mg/L
Pyridine
0.004
U
0.01
mg/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
2,4,6-Tribromophenol
0.23
m91L
0,250
92
33-145
2-Fluorobiphenyl
0.16
m91L
0.250
65
32-116
2-Fluo-phenol
0.12
m91L
a250
49
11-100
Nitrobenzene-d5
0.17
m91L
0,250
66
24-107
Phenol-d5
0,092
m91L
a250
37
10-100
Terphenyl-dM
0.26
m91L
0.250
103
52-150
Blank (1B23004-BLK3)
Prepared: 02/24/2021 06:25 Analyzed: 02/24/2021 16:18
Analvte
Result
Flaq
POL
Units
1,4-Dichlorobenzene
0.003
U
0.01
mg/L
2,4,5-Trichlorophenol
0.004
U
0.01
mg/L
2,4,6-Trichlorophenol
0.006
U
0.01
mg/L
2,4-Dinitrotoluene
0.003
U
0.01
mg/L
2-Methylphenol
0.004
U
0.01
mg/L
3 & 4-Methylphenol
0.008
U
0.01
mg/L
Hexachlorobenzene
0.003
U
0.01
mg/L
Hexachlorobutadiene
0.004
U
0.01
mg/L
Hexachloroethane
0.003
U
0.01
mg/L
Nitrobenzene
0.003
U
0.01
mg/L
Pentachlorophenol
0.008
U
0.01
mg/L
Pyridine
0.004
U
0.01
mg/L
Spike Source %REC RPD
Level Result %REC Limi RPD Mina Notes
2,4,6-Tribromophenol
0.19
m91L
0.250
77
33-145
2-Fluorobiphenyl
0.14
m91L
0,250
56
32-116
2-Fiuorophenol
0.099
m91L
0.250
40
11-100
Nitrobenzene-d5
0.14
m91L
0.250
56
24-107
Phenol-d5
0,071
m91L
0,250
29
10-100
Terphenyl-dM
0.23
m91L
0.250
93
52-150
LCS (1B23004-BS1)
Prepared: 02/23/202106:30 Analyzed: 02/24/2021 16:48
Spike
Source
%REC RPD
Analvte
Result Flaq POL
Units
Level
Result %REC
Limits RPD Limit Notes
1,4-Dichlorobenzene
0.05 0.002
mg/L
0.0500
95
10-101
Pentachlorophenol
0.06 0.002
mg/L
0.0500
112
5-139
2,4,6-Tribromophenol
0,053
m9/L
0.0500
105
33-145
2-Fluorobiphenyl
0.040
m91L
0.0500
79
32-116
2-Fluorophenol
0,031
m91L
0.0500
62
11-100
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 14

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QUALITY CONTROL DATA
TCLP Semivolatile Organics by GCMS - Quality Control
Batch 1 B23004 - EPA 3510C MS - Continued
LCS (1B23004-BSI) Continued Prepared: 02/23/2021 06:30 Analyzed: 02/24/2021 16:48
Spike Source %REC RPD
Analvte
Result Flaq POL
Units
Level Result %REC Limits RPD Limit Notes
Nitrobenzene-d5
0.046
m91L
0.0500 93 24-107
Phenol-d5
0.023
m91L
0.0500 47 10-100
Terphenyl-d14
0.051
m91L
0.0500 102 52-150
Matrix Spike (1B23004-MS1)
Prepared: 02/23/2021 06:30 Analyzed: 02/24/2021 17:18
Source: AE01385-01
Spike
Source
%REC RPD
Analvte
Result Flaq POL Units
Level
Result
%REC Limits RPD Limit Notes
1,4-Dichlorobenzene
0.04 0.002 mg/L
0.0500
0.0006 U
90 10-101
Pentachlorophenol
0.05 0.002 mg/L
0.0500
0.002 U
108 5-139
2,4,6-Tribromopheno/
0.051
m91L
0.0500
102
33-145
2-Fluorobiphenyl
0.039
m91L
0.0500
77
32-116
2-Fluorophenol
0.030
m91L
0.0500
60
11-100
Nitrobenzene-d5
0.044
m91L
0.0500
89
24-107
Phenol-d5
0.022
m91L
0.0500
45
10-100
Terphenyl-d14
0.050
m91L
0.0500
99
52-150
Matrix Spike (1B23004-MS2)
Prepared: 02/24/2021 06:25 Analyzed: 02/25/2021 13:50
Source: CE01842-01
Spike
Source
%REC RPD
Analvte
Result Flaq POL Units
Level
Result
%REC Limits RPD Limit Notes
1,4-Dichlorobenzene
0.13 D 0.05 mg/L
0.250
0.02 U
51 10-101
Pentachlorophenol
0.16 D 0.05 mg/L
0.250
0.04 U
64 5-139
2,4,6-Tribromopheno/
0.22
m91L
0.250
66
33-145
2-Fluorobiphenyl
0.16
m91L
0.250
65
32-116
2-Fluorop17enol
0.078
m91L
0.250
31
11-100
Nitrobenzene-d5
0.15
m91L
0.250
59
24-107
Phenol-d5
0.069
m91L
0.250
28
10-100
Terphenyl-d14
0.23
m91L
0.250
93
52-150
Matrix Spike Dup (1B23004-MSD1)
Prepared: 02/23/2021 06:30 Analyzed: 02/24/2021 17:47
Source: AE01385-01
Spike
Source
%REC
RPD
Analvte
Result Flaq POL Units
Level
Result
%REC Limits RPD
Limit Notes
1,4-Dichlorobenzene
0.04 0.002 mg/L
0.0500
0.0006 U
80 10-101 11
18
Pentachlorophenol
0.05 0.002 mg/L
0.0500
0.002 U
108 5-139 0.5
23
2,4,6-Tribromopheno/ 0.049
m91L
0.0500
99
33-145
2-Fluorobiphenyl 0.036
m91L
0.0500
72
32-116
2-Fluorophenol 0.026
m91L
0.0500
57
11-100
Nitrobenzene-d5 0.041
m91L
0.0500
83
24-107
Phenol-d5 0.022
m91L
0.0500
43
10-100
Terphenyl-d14 0.047
m91L
0.0500
94
52-150
TCLP Metals by 6000/7000 Series Methods - Quality Control
Batch IB24003 - EPA 7470A
Blank (1B24003-BLK1) Prepared: 02/24/2021 10:39 Analyzed: 02/25/2021 08:14
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 14

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QUALITY CONTROL DATA
TCLP Metals by 6000/7000 Series Methods - Quality Control
Batch 1B24003 - EPA 7470A - Continued
Blank (SB24003-BLK1) Continued Prepared: 02/24/2021 10:39 Analyzed: 02/25/2021 08:14
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Mercury 2.30E-5 U 0.000200 mg/L
Blank (1B24003-BLK2) Prepared: 02/24/2021 10:39 Analyzed: 02/25/2021 08:17
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Mercury 0.000230 U 0.00200 mg/L
Blank (1B24003-BLK3) Prepared: 02/24/2021 10:39 Analyzed: 02/25/2021 08:21
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Mercury 0.000230 U 0.00200 mg/L
Blank (1B24003-BLK4) Prepared: 02/24/2021 12:34 Analyzed: 02/25/2021 08:24
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Mercury 0.000230 U 0.00200 mg/L
LCS (1B24003-BS1) Prepared: 02/24/2021 10:39 Analyzed: 02/25/2021 08:27
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Mercury
0.00504
0.000200
mg/L
0.00500
101
80-120
Matrix Spike (1B24003-MS3)
Prepared: 02/24/2021 10:39 Analyzed: 02/25/2021 08:33
Source: AE01121-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Mercury
0.0503
0.00200
mg/L
0.0500
0.000230 U
101
75-125
Matrix Spike Dup (1B24003-MSDS)
Prepared: 02/24/2021 10:39 Analyzed: 02/25/2021 08:36
Source: AE01121-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Mercury
0.0511
0.00200
mg/L
0.0500
0.000230 U
102
75-125 2
20
Batch 1824006 - EPA 3010A
Blank (1B24006-BLK3) Prepared: 02/24/2021 16:17 Analyzed: 02/25/2021 10:53
Analvte
Result
Flaq
POL
Units
Arsenic
0.110
U
0.500
mg/L
Barium
0.140
U
0.500
mg/L
Cadmium
0.0200
U
0.0500
mg/L
Chromium
0.110
U
0.250
mg/L
Lead
0.110
U
0.250
mg/L
Selenium
0.600
U
1.00
mg/L
Silver
0.0800
U
0.250
mg/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit
Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 14

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QUALITY CONTROL DATA
TCLP Metals by 6000/7000 Series Methods - Quality Control
Batch IB24006 - EPA 3010A - Continued
Blank (1B24006-BLK2)
Prepared: 02/24/2021 16:17 Analyzed: 02/25/2021 10:57
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Arsenic
0.110
U
0.500
mg/L
Barium
0.140
U
0.500
mg/L
Cadmium
0.0200
U
0.0500
mg/L
Chromium
0.110
U
0.250
mg/L
Lead
0.110
U
0.250
mg/L
Selenium
0.600
U
1.00
mg/L
Silver
0.0800
U
0.250
mg/L
Blank (1B24006-BLK3)
Prepared: 02/24/2021 16:17 Analyzed: 02/25/2021 11:00
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Arsenic
0.110
U
0.500
mg/L
Barium
0.140
U
0.500
mg/L
Cadmium
0.0200
U
0.0500
mg/L
Chromium
0.110
U
0.250
mg/L
Lead
0.110
U
0.250
mg/L
Selenium
0.600
U
1.00
mg/L
Silver
0.0800
U
0.250
mg/L
Blank (1B24006-BLK4)
Prepared: 02/24/2021 16:17 Analyzed: 02/25/2021 11:04
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Arsenic
0.110
U
0.500
mg/L
Barium
0.140
U
0.500
mg/L
Cadmium
0.0200
U
0.0500
mg/L
Chromium
0.110
U
0.250
mg/L
Lead
0.110
U
0.250
mg/L
Selenium
0.600
U
1.00
mg/L
Silver
0.0800
U
0.250
mg/L
LCS (1B24006-BSI)
Prepared: 02/24/2021 16:17 Analyzed: 02/25/2021 11:08
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Arsenic
12.8
0.500
mg/L
12.5 102 80-120
Barium
12.6
0.500
mg/L
12.4 102 80-120
Cadmium
1.24
0.0500
mg/L
1.24 100 80-120
Chromium
12.4
0.250
mg/L
12.5 100 80-120
Lead
12.3
0.250
mg/L
12.6 98 80-120
Selenium
12.4
1.00
mg/L
12.5 99 80-120
Silver
2.16
0.250
mg/L
2.29 94 80-120
Matrix Spike (1B24006-MS1)
Prepared: 02/24/2021 16:17 Analyzed: 02/25/2021 11:15
Source: AE01121-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Arsenic
12.8
0.500
mg/L
12.5 0.110 U 103 75-125
Barium
12.5
0.500
mg/L
12.4 0.140 U 100 75-125
Cadmium
1.23
0.0500
mg/L
1.24 0.0216 97 75-125
Chromium
12.3
0.250
mg/L
12.5 0.110 U 98 75-125
FINAL
This report relates only to the sample as received by the
laboratory, and may only be reproduced in full.
Page 11 of 14

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QUALITY CONTROL DATA
TCLP Metals by 6000/7000 Series Methods - Quality Control
Batch IB24006 - EPA 3010A - Continued
Matrix Spike (1824006-14S3) Continued
Prepared: 02/24/2021 16:17 Analyzed: 02/25/2021 11:15
Source: AE01121-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Lead
12.1
0.250
mg/L
12.6
0.110 U
97
75-125
Selenium
12.4
1.00
mg/L
12.5
0.600 U
99
75-125
Silver
2.13
0.250
mg/L
2.29
0.0800 U
93
75-125
Matrix Spike Dup (1824006-MSDS)
Prepared: 02/24/2021 16:17 Analyzed: 02/25/2021 11:18
Source: AE01121-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Arsenic
12.8
0.500
mg/L
12.5
0.110 U
103
75-125
0.009
20
Barium
12.5
0.500
mg/L
12.4
0.140 U
100
75-125
0.06
20
Cadmium
1.23
0.0500
mg/L
1.24
0.0216
97
75-125
0.3
20
Chromium
12.3
0.250
mg/L
12.5
0.110 U
98
75-125
0.2
20
Lead
12.1
0.250
mg/L
12.6
0.110 U
96
75-125
0.3
20
Selenium
12.5
1.00
mg/L
12.5
0.600 U
100
75-125
0.5
20
Silver
2.15
0.250
mg/L
2.29
0.0800 U
94
75-125
1
20
Classical Chemistry Parameters - Quality Control
Batch IB2700B - NO PREP
LCS (1827008-113SI) Prepared: 03/03/2021 12:47 Analyzed: 03/03/2021 14:48
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits
RPD
Limit
Notes
pH
7.0
1.0
pH Units
7.00
100 99-101
Duplicate (1827008-DUP3)
Prepared: 03/03/2021 12:47 Analyzed: 03/03/2021 14:48
Source: AE01644-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits
RPD
Limit
Notes
pH
5.1
1.0
pH Units
5.2
0.4
25
Q-01
Temperature for pH (deg. C)
21
pH Units
21
0.5
200
Q-01
Classical Chemistry Parameters -
Quality Control
Batch IB23003 - NO PREP
LCS (1823003-13SI) Prepared: 02/25/2021 08:00 Analyzed: 02/25/2021 08:07
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
ASTMD93 PMCC Flashpoint 81.0 OF 81.0 100 98-102
Duplicate (1823003-DUPIL) Prepared: 02/25/2021 08:00 Analyzed: 02/25/2021 12:13
Source: CE01842-01
Analvte
ASTMD93 PMCC Flashpoint
Spike Source %REC
Result Flaq POL Units Level Result %REC Limits RPD
> 200 U OF > 200 0.00
RPD
Limit Notes
5
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 14

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
Q-01 Analysis performed outside of method - specified holding time.
QV-01 The associated continuing calibration verification standard exhibited high bias; since the result is ND, there
is no impact.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 14

ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD
CO 1D775 Gentrai Port Dr. 4810 Executive Park Court, Suite 111 102-A Woodwinds Industrial Ct
Orlando, FL 32824 Jacksonville, FL 3221"%9 Cary, NC 27511
[phone] [phone] Fax [phone] (919) 467--NM Fax [phone]
Client Name Project Number Requested Analyses
Noyozymes North America 0008 none 5
Address Project! Name)Oesc
77 Perry Chwd ChurCh Road SBMPWVM21
City1STlZip i PO N I Billing info
Frar"nton, NO 27525
Tel Fax Reporting Contact
494-X370 Joe Ladd
Sampler(s) Name, Affiliation (Print) i- h ' f
Billing Contact
L' M W
► G "L Accounts Payable
Samnrarrcl Rianawm Site Location ITime Zone
By
n)
Correction Date
Collection
Time
Comp I Grab
M
(see
S
By
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Page of
Times
Note : Rush requests subject to
acceptance by the facility
�
9il
_j
U
F"
�
°
p
o
_Im
aD 2
a a
2 ~ ~
Preservation (See Codes) (Combine as necessary)
Standard
` Expedited
Due
Lab Workorder
CE01842
itr€x Total y of
odes) Containers
Sample Comments
ID 6
X
X
X
X
X_
<-- Tota) # of Containers
�—
Detefrime
�_
Received By
Date!llme
VQ44 Zi a
Date-Mme
Received By
Dataimme
DatelTme Received By I Datemme
Cooler ti's S Temps on Haceipt
Matrix: GW-Groundwaler SO -Soil DW-Drinking Water SE -Sediment SW-Surtace Water WW-Wastewater A -Air Other (detail in comments) Preservation: I -Ice H-HCI N-HNO3 SH2504 NO-NaOH O.Other (detail in comments)
Note: All samples submitted to ENCO labs are in accordance with the terms and conditions listed on the reverse of this form. unless prior written agreements exist

2�SENCO Laboratories
9g
Accurate. Timely. Respousive. luuavative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Tuesday, November 12, 2019
Novozymes North America (N0008)
Attn: Scott Creech
77 Perry Chapel Church Road
Franklinton, NC 27525
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: RO Pilot
ENCO Workorder(s): CC17860
Dear Scott Creech,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, October 22, 2019.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
0"CLC'L�CA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 23

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: MBBR Feed
Lab ID: CC17860-01
Sampled: 10/21/19 10:50
Received: 10/22/19
11:58
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 6010D
EPA 3005A
04/18/20
10/30/19
09:44
10/31/19
12:51
SM 5210 B-2011
NO PREP
10/23/19
10:50
10/23/19
09:43
10/23/19
09:43
Client ID: RO Feed
Lab ID: CC17860-02
Sampled: 10/21/19 10:50
Received: 10/22/19
11:58
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
CALC
[CALC]
11/18/19
10/30/19
20:51
10/31/19
19:33
EPA 300.0
NO PREP
11/18/19
10/22/19
12:48
10/23/19
00:50
EPA 310.2
NO PREP
11/04/19
10/28/19
15:13
10/28/19
17:30
EPA 335.4
Same
11/04/19
10/25/19
09:36
10/25/19
16:18
EPA 351.2
Same
11/18/19
10/29/19
10:54
10/31/19
19:33
EPA 353.2
NO PREP
11/18/19
10/30/19
20:51
10/30/19
20:51
EPA 365.1
NO PREP
10/23/19
10:50
10/23/19
10:26
10/23/19
10:26
EPA 6010D
EPA 3005A
04/18/20
10/30/19
09:44
10/31/19
12:17
EPA 7470A
EPA 7470A
11/18/19
10/30/19
13:45
10/31/19
14:48
SM 213OB-2011
NO PREP
10/23/19
10:50
10/22/19
15:28
10/22/19
15:28
SM 251OB-2011
NO PREP
11/18/19
10/31/19
11:00
10/31/19
11:00
SM 254OC-2011
NO PREP
10/28/19
10/24/19
14:15
10/24/19
14:15
SM 254OD-2011
NO PREP
10/28/19
10/24/19
09:57
10/24/19
09:57
SM 4500002 D-2011
NO PREP
07/16/22
10/31/19
10:14
10/31/19
10:14
SM 4500H+B-2011
NO PREP
10/21/19
11:04
10/25/19
10:38
10/25/19
10:38
SM 5220D-2011
Same
11/18/19
10/24/19
11:19
10/24/19
16:38
Client ID: RO Feed
Lab ID: CC17860-02RE1
Sampled: 10/21/19 10:50
Received: 10/22/19
11:58
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 300.0
NO PREP
11/18/19
10/22/19
12:48
10/23/19
01:08
EPA 365.4
Same
11/18/19
10/29/19
10:54
11/01/19
16:24
Client ID: RO Permeate
Lab ID: CC17860-03
Sampled: 10/21/19 10:50
Received: 10/22/19
11:58
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
CALC
[CALC]
11/18/19
10/30/19
20:52
10/31/19
19:35
EPA 300.0
NO PREP
11/18/19
10/22/19
12:48
10/23/19
01:25
EPA 310.2
NO PREP
11/04/19
10/28/19
15:13
10/28/19
17:30
EPA 335.4
Same
11/04/19
10/25/19
09:36
10/25/19
16:35
EPA 351.2
Same
11/18/19
10/29/19
10:54
10/31/19
19:35
EPA 353.2
NO PREP
11/18/19
10/30/19
20:52
10/30/19
20:52
EPA 365.1
NO PREP
10/23/19
10:50
10/23/19
10:29
10/23/19
10:29
EPA 365.4
Same
11/18/19
10/29/19
10:54
11/01/19
13:22
EPA 6010D
EPA 3005A
04/18/20
10/30/19
09:44
10/31/19
12:20
EPA 7470A
EPA 7470A
11/18/19
10/30/19
13:45
10/31/19
14:50
SM 213OB-2011
NO PREP
10/23/19
10:50
10/22/19
15:28
10/22/19
15:28
SM 251OB-2011
NO PREP
11/18/19
10/31/19
11:00
10/31/19
11:00
SM 2540C-2011
NO PREP
10/28/19
10/24/19
14:15
10/24/19
14:15
SM 254OD-2011
NO PREP
10/28/19
10/28/19
14:27
10/28/19
14:27
SM 4500002 D-2011
NO PREP
07/16/22
10/31/19
10:14
10/31/19
10:14
SM 4500H+B-2011
NO PREP
10/21/19
11:04
10/25/19
10:38
10/25/19
10:38
SM 5210 B-2011
NO PREP
10/23/19
10:50
10/23/19
09:43
10/23/19
09:43
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 23

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: RO Reject
Lab ID: CC17860-04
Sampled: 10/21/19 10:50
Received: 10/22/19 11:58
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
CALC
[CALC]
11/18/19
10/30/19 20:53
11/01/19 15:42
EPA 310.2
NO PREP
11/04/19
10/28/19 15:13
10/28/19 17:31
EPA 335.4
Same
11/04/19
10/25/19 09:36
10/25/19 16:36
EPA 353.2
NO PREP
11/18/19
10/30/19 20:53
10/30/19 20:53
EPA 365.1
NO PREP
10/23/19 10:50
10/23/19 10:48
10/23/19 10:48
EPA 6010D
EPA 3005A
04/18/20
10/30/19 09:44
10/31/19 12:23
EPA 7470A
EPA 7470A
11/18/19
10/30/19 13:45
10/31/19 14:57
SM 213OB-2011
NO PREP
10/23/19 10:50
10/22/19 15:28
10/22/19 15:28
SM 251OB-2011
NO PREP
11/18/19
10/31/19 11:00
10/31/19 11:00
SM 2540C-2011
NO PREP
10/28/19
10/24/19 14:15
10/24/19 14:15
SM 254OD-2011
NO PREP
10/28/19
10/24/19 09:57
10/24/19 09:57
SM 4500002 D-2011
NO PREP
07/16/22
10/31/19 10:14
10/31/19 10:14
SM 4500H+B-2011
NO PREP
10/21/19 11:04
10/25/19 10:38
10/25/19 10:38
SM 5220D-2011
Same
11/18/19
10/24/19 11:19
10/24/19 16:38
Client ID: RO Reject
Lab ID: CC17860-04RE1
Sampled: 10/21/19 10:50
Received: 10/22/19 11:58
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 300.0
NO PREP
11/18/19
10/22/19 12:48
10/23/19 11:59
EPA 351.2
Same
11/18/19
10/29/19 10:54
11/01/19 15:42
Client ID: RO Reject
Lab ID: CC17860-04RE2
Sampled: 10/21/19 10:50
Received: 10/22/19 11:58
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 365.4
Same
11/18/19
10/29/19 10:54
11/07/19 14:21
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 23

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SAMPLE DETECTION SUMMARY
Client ID: MBBR Feed
Lab ID:
CC17860-03
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Biochemical Oxygen Demand - Dissolved
26
2.0
2.0
mg/L
SM 5210 B-2011
Calcium - Dissolved
108
0.195
0.500
mg/L
EPA 6010D
Magnesium - Dissolved
7380
145
500
ug/L
EPA 6010D
Silica (Si02) - Dissolved
17.2
0.1
1.1
mg/L
EPA 6010D
Client ID: RO Feed
Lab ID:
CC17860-02
Anal a
Results
Flag
MDL
Q
Units
Method
Notes
Bicarbonate (as CaCO3)
740
14
15
mg/L
SM 4500002 D-2011
Boron - Total
0.0777
J
0.0570
0.500
mg/L
EPA 6010D
Calcium - Total
69.5
0.390
1.00
mg/L
EPA 6010D
Chemical Oxygen Demand
90
10
10
mg/L
SM 5220D-2011
Chloride
320
D
22
50
mg/L
EPA 300.0
Iron - Total
0.368
J
0.220
0.500
mg/L
EPA 6010D
Magnesium - Total
4.10
0.290
1.00
mg/L
EPA 6010D
Mercury - Total
0.000760
J
0.000750
0.00100
mg/L
EPA 7470A
Nitrate/Nitrite as N
1.5
D
0.41
1.0
mg/L
EPA 353.2
Orthophosphate as P
8.1
B
0.16
0.50
mg/L
EPA 365.1
QB-01
PH
8.2
1.0
1.0
pH
SM 4500H+B-2011
Q-01
Potassium - Total
261
1.50
5.00
mg/L
EPA 6010D
Silica (Si02) - Total
14.2
0.3
2.1
mg/L
EPA 6010D
Sodium - Total
269
4.00
5.00
mg/L
EPA 6010D
Specific Conductance (EC) at 25 Deg C
2900
1.0
1.0
umhos/cm
SM 251OB-2011
Temperature for pH (deg. C)
19
pH
SM 4500H+B-2011
Q-01
Total Alkalinity as CaCO3
750
D
140
150
mg/L
EPA 310.2
Total Dissolved Solids
1700
50
50
mg/L
SM 2540C-2011
Total Kjeldahl Nitrogen
24
0.26
0.48
mg/L
EPA 351.2
Total Nitrogen
25
D
0.41
1.0
mg/L
CALC
Zinc - Total
0.0508
J
0.0440
0.100
mg/L
EPA 6010D
Client ID: RO Feed
Lab ID:
CC17860-02RE1
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Phosphorus
8.1
D
0.12
0.50
mg/L
EPA 365.4
Sulfate as SO4
120
D
5.8
10
mg/L
EPA 300.0
Client ID: RO Permeate
Lab ID:
CC17860-03
Anal a
Results
Flag MDL
POL
Units
Method
Notes
Bicarbonate (as CaCO3)
24
14
15
mg/L
SM 4500002 D-2011
Boron - Total
0.0642
J 0.0570
0.500
mg/L
EPA 6010D
Chloride
6.9
2.2
5.0
mg/L
EPA 300.0
Nitrate/Nitrite as N
0.19
0.041
0.10
mg/L
EPA 353.2
Orthophosphate as P
0.34
JB 0.16
0.50
mg/L
EPA 365.1
J-01
PH
5.7
1.0
1.0
pH
SM 4500H+B-2011
Q-01
Phosphorus
0.33
0.025
0.10
mg/L
EPA 365.4
Potassium - Total
14.9
1.50
5.00
mg/L
EPA 6010D
Sodium - Total
9.54
4.00
5.00
mg/L
EPA 6010D
Specific Conductance (EC) at 25 Deg C
94
1.0
1.0
umhos/cm
SM 251OB-2011
Temperature for pH (deg. C)
20
pH
SM 4500H+B-2011
Q-01
Total Alkalinity as CaCO3
24
14
15
mg/L
EPA 310.2
Total Kjeldahl Nitrogen
3.3
0.26
0.48
mg/L
EPA 351.2
Total Nitrogen
3.5
0.26
0.48
mg/L
CALC
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 23

0Nk"q09
www.encolabs.com
SAMPLE DETECTION SUMMARY
Client ID: RO Reject
Lab ID:
CC17860-04
Analvte
Results
Flaa
MDL
Q
Units
Method
Notes
Bicarbonate (as CaCO3)
1900
14
15
mg/L
SM 4500002 D-2011
Boron - Total
0.234
J
0.0570
0.500
mg/L
EPA 6010D
Calcium - Total
737
0.390
1.00
mg/L
EPA 6010D
Chemical Oxygen Demand
1200
20
20
mg/L
SM 5220D-2011
Chromium - Total
0.0259
J
0.0140
0.100
mg/L
EPA 6010D
Copper - Total
0.0253
J
0.0160
0.100
mg/L
EPA 6010D
Iron - Total
3.63
0.220
0.500
mg/L
EPA 6010D
Magnesium - Total
42.5
0.290
1.00
mg/L
EPA 6010D
Molybdenum - Total
0.0294
J
0.0250
0.100
mg/L
EPA 6010D
Nickel - Total
0.0403
J
0.0220
0.100
mg/L
EPA 6010D
Nitrate/Nitrite as N
12
D
2.0
4.8
mg/L
EPA 353.2
Orthophosphate as P
55
BD
1.6
5.0
mg/L
EPA 365.1
QB-01
PH
7.3
1.0
1.0
pH
SM 4500H+B-2011
Q-01
Potassium - Total
2760
1.50
5.00
mg/L
EPA 6010D
Silica (Si02) - Total
166
0.3
2.1
mg/L
EPA 6010D
Sodium - Total
2840
4.00
5.00
mg/L
EPA 6010D
Specific Conductance (EC) at 25 Deg C
20000
1.0
1.0
umhos/cm
SM 251OB-2011
Temperature for pH (deg. C)
20
pH
SM 4500H+B-2011
Q-01
Total Alkalinity as CaCO3
1900
D
140
150
mg/L
EPA 310.2
Total Dissolved Solids
16000
50
50
mg/L
SM 2540C-2011
Total Nitrogen
190
D
2.6
4.8
mg/L
CALC
Total Suspended Solids
2.7
2.5
2.5
mg/L
SM 2540D-2011
Turbidity
3.9
0.50
1.0
NTU
SM 213OB-2011
Zinc - Total
0.146
0.0440
0.100
mg/L
EPA 6010D
Client ID: RO Reject
Lab ID:
CC17860-04RE1
Analvte
Results
Flaa
MDL
Q
Units
Method
Notes
Chloride
2700
D
220
500
mg/L
EPA 300.0
Sulfate as SO4
5400
D
290
500
mg/L
EPA 300.0
Total Kjeldahl Nitrogen
180
D
2.6
4.8
mg/L
EPA 351.2
Client ID: RO Reject
Lab ID:
CC17860-04RE2
Anal a
Results
Flaa
MDL
Q
Units
Method
Notes
Phosphorus
78
D
1.2
5.0
mg/L
EPA 365.4
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 23

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ANALYTICAL RESULTS
Description: MBBR Feed Lab Sample ID:CC17860-01 Received: 10/22/19 11:58
Matrix: Waste Water Sampled:10/21/19 10:50 Work Order: CC17860
Project: RO Pilot Sampled By:Jelena El Barigi
Metals (Dissolved) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flao
Units
DF
MOIL
P L
Batch
Method
Analyzed
By Notes
Calcium [7440-70-2]^ 108
mg/L
5
0.195
0.500
9330014
EPA 6010D
10/31/19 12:51
JDH
Magnesium [7439-95-4]^ 7380
ug/L
5
145
500
9330014
EPA 6010D
10/31/19 12:51
JDH
Silica (Si02) [763-18-69]^ 17.2
mg/L
5
0.1
1.1
9330014
EPA 6010D
10/31/19 12:51
JDH
Classical Chemistry Parameters (Dissolved)
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flao
Units
OF
MOIL
P L
Batch
Method
Analyzed
By Notes
Biochemical Oxygen Demand^ 26
mg/L
1
2.0
2.0
9323001
SM 5210 B-2011
10/23/19 09:43
JOC
Description: RO Feed Lab Sample ID:CC17860-02 Received: 10/22/19 11:58
Matrix: Waste Water Sampled:10/21/19 10:50 Work Order: CC17860
Project: RO Pilot Sampled By:Jelena El Barigi
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MOIL
P L
Batch
Method
Analyzed
By
Notes
Mercury [7439-97-6]^
0.000760
J
mg/L
5
0.000750
0.00100
9330032
EPA 7470A
10/31/19 14:48
KAH
Silica (Si02) [763-18-69]^
14.2
mg/L
10
0.3
2.1
9330014
EPA 6010D
10/31/19 12:17
JDH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MOIL
P L
Batch
Method
Analyzed
By
Notes
Aluminum [7429-90-5]^
0.420
U
mg/L
10
0.420
1.00
9330014
EPA 6010D
10/31/19 12:17
JDH
Arsenic[7440-38-2]^
0.0760
U
mg/L
10
0.0760
0.100
9330014
EPA 6010D
10/31/19 12:17
JDH
Boron [7440-42-8]^
0.0777
J
mg/L
10
0.0570
0.500
9330014
EPA 6010D
10/31/19 12:17
JDH
Cadmium [7440-43-9]^
0.00360
U
mg/L
10
0.00360
0.0100
9330014
EPA 6010D
10/31/19 12:17
JDH
Calcium [7440-70-2]^
69.5
mg/L
10
0.390
1.00
9330014
EPA 6010D
10/31/19 12:17
JDH
Chromium [7440-47-3]^
0.0140
U
mg/L
10
0.0140
0.100
9330014
EPA 6010D
10/31/19 12:17
JDH
Copper[7440-50-8]^
0.0160
U
mg/L
10
0.0160
0.100
9330014
EPA 6010D
10/31/19 12:17
JDH
Iron [7439-89-6]^
0.368
J
mg/L
10
0.220
0.500
9330014
EPA 6010D
10/31/19 12:17
JDH
Lead [7439-92-1]^
0.0310
U
mg/L
10
0.0310
0.100
9330014
EPA 6010D
10/31/19 12:17
JDH
Magnesium [7439-95-4]^
4.10
mg/L
10
0.290
1.00
9330014
EPA 6010D
10/31/19 12:17
JDH
Molybdenum [7439-98-7]^
0.0250
U
mg/L
10
0.0250
0.100
9330014
EPA 6010D
10/31/19 12:17
JDH
Nickel[7440-02-0]^
0.0220
U
mg/L
10
0.0220
0.100
9330014
EPA 6010D
10/31/19 12:17
JDH
Potassium [7440-09-7]^
261
mg/L
10
1.50
5.00
9330014
EPA 6010D
10/31/19 12:17
JDH
Selenium [7782-49-2]^
0.0620
U
mg/L
10
0.0620
0.100
9330014
EPA 6010D
10/31/19 12:17
JDH
Silver[7440-22-4]^
0.0190
U
mg/L
10
0.0190
0.100
9330014
EPA 6010D
10/31/19 12:17
JDH
Sodium [7440-23-5]^
269
mg/L
10
4.00
5.00
9330014
EPA 6010D
10/31/19 12:17
JDH
Zinc [7440-66-6]^
0.0508
J
mg/L
10
0.0440
0.100
9330014
EPA 6010D
10/31/19 12:17
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By
Notes
Bicarbonate (as CaCO3) [71-52-3]
740
mg/L
1
14
15
9331024
M 45000O2 D-201
10/31/19 10:14
PDK
Carbonate (as CaCO3)[3812-32-6]
14
U
mg/L
1
14
15
9331024
M 45000O2 D-201
10/31/19 10:14
PDK
Chemical Oxygen Demand^
90
mg/L
1
10
10
9324013
SM 5220D-2011
10/24/19 16:38
JOC
Chloride [16887-00-6]^
320
D
mg/L
10
22
50
9322024
EPA 300.0
10/23/19 00:50
PDK
Cyanide (total) [57-12-5]^
0.0049
U
mg/L
1
0.0049
0.0050
9325006
EPA 335.4
10/25/19 16:18
NMN
Nitrate/Nitrite as N^
1.5
D
mg/L
10
0.41
1.0
9329026
EPA 353.2
10/30/19 20:51
AKF
FINAL
This report relates only
to the sample as received by the laboratory,
and may only
be reproduced
in full.
Page 6 of 23

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www.encolabs.com
ANALYTICAL RESULTS
Description: RO Feed Lab Sample ID:CC17860-02 Received: 10/22/19 11:58
Matrix: Waste Water Sampled:10/21/19 10:50 Work Order: CC17860
Project: RO Pilot Sampled By:Jelena El Barigi
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results
Flao
Units
DF
MDL
P L
Batch
Method
Analyzed
By
Notes
Orthophosphate as P [1426-54-42]A
8.1
B
mg/L
1
0.16
0.50
9323009
EPA 365.1
10/23/19 10:26
NMN
QB-01
pH
8.2
pH
1
1.0
1.0
9325019
iM 4500H+B-2011
10/25/19 10:38
BDC
Q-01
Phosphorus[7723-14-O]A
8.1
D
mg/L
5
0.12
0.50
9329007
EPA 365.4
11/01/19 16:24
AKF
Specific Conductance (EC) at 25 Deg
2900
umhos/cm
1
1.0
1.0
9331027
SM 251OB-2011
10/31/19 11:00
JOC
CA
Sulfate as SO4 [14808-79-8]A
120
D
mg/L
2
5.8
10
9122024
EPA 300.0
10/23/19 01:08
PDK
Temperature for pH (deg. C)
19
pH
1
9125019
311 4500H+B-2011
10/25/19 10:38
BDC
Q-01
Total Alkalinity as CaCO3 [471-34-1]A
750
D
mg/L
10
140
150
9128025
EPA 310.2
10/28/19 17:30
AKF
Total Dissolved SolidsA
1700
mg/L
1
50
50
9124009
SM 2540C-2011
10/24/19 14:15
JOC
Total Kjeldahl Nitrogen
24
mg/L
1
0.26
0.48
9129006
EPA 351.2
10/31/19 19:33
AKF
Total Nitrogen [17778-88-0]
25
D
mg/L
10
0.41
1.0
[CALC]
CALC
10/31/19 19:33
AKF
Total Suspended Solids^
2.5
U
mg/L
1
2.5
2.5
9J24010
SM 2540D-2011
10/24/19 09:57
JAH
Turbidity^
0.50
U
NTU
1
0.50
1.0
9J22034
SM 213OB-2011
10/22/19 15:28
JOC
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 23

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ANALYTICAL RESULTS
Description: RO Permeate Lab Sample ID:CC17860-03 Received: 10/22/19 11:58
Matrix: Waste Water Sampled:10/21/19 10:50 Work Order: CC17860
Project: RO Pilot Sampled By:Jelena El Barigi
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flao
Units
DF
MDL
P L
Batch
Method
Analyzed
-By
Notes
Mercury[7439-97-6]^
0.000750
U
mg/L
5
0.000750
0.00100
9330032
EPA 7470A
10/31/19 14:50
KAH
Silica (Si02) [763-18-69]^
0.3
U
mg/L
10
0.3
2.1
9330014
EPA 6010D
10/31/19 12:20
JDH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flao
Units
DF
MDL
P L
Batch
Method
Analyzed
By
Notes
Aluminum [7429-90-5]^
0.420
U
mg/L
10
0.420
1.00
9330014
EPA 6010D
10/31/19 12:20
JDH
Arsenic[7440-38-2]^
0.0760
U
mg/L
10
0.0760
0.100
9330014
EPA 6010D
10/31/19 12:20
JDH
Boron [7440-42-8]^
0.0642
J
mg/L
10
0.0570
0.500
9330014
EPA 6010D
10/31/19 12:20
JDH
Cadmium [7440-43-9]^
0.00360
U
mg/L
10
0.00360
0.0100
9330014
EPA 6010D
10/31/19 12:20
JDH
Calcium [7440-70-2]^
0.390
U
mg/L
10
0.390
1.00
9330014
EPA 6010D
10/31/19 12:20
JDH
Chromium [7440-47-3]^
0.0140
U
mg/L
10
0.0140
0.100
9330014
EPA 6010D
10/31/19 12:20
JDH
Copper[7440-50-8]^
0.0160
U
mg/L
10
0.0160
0.100
9330014
EPA 6010D
10/31/19 12:20
JDH
Iron [7439-89-6]^
0.220
U
mg/L
10
0.220
0.500
9330014
EPA 6010D
10/31/19 12:20
JDH
Lead [7439-92-1]^
0.0310
U
mg/L
10
0.0310
0.100
9330014
EPA 6010D
10/31/19 12:20
JDH
Magnesium [7439-95-4]^
0.290
U
mg/L
10
0.290
1.00
9330014
EPA 6010D
10/31/19 12:20
JDH
Molybdenum [7439-98-7]^
0.0250
U
mg/L
10
0.0250
0.100
9330014
EPA 6010D
10/31/19 12:20
JDH
Nickel[7440-02-0]^
0.0220
U
mg/L
10
0.0220
0.100
9330014
EPA 6010D
10/31/19 12:20
JDH
Potassium [7440-09-7]^
14.9
mg/L
10
1.50
5.00
9330014
EPA 6010D
10/31/19 12:20
JDH
Selenium [7782-49-2]^
0.0620
U
mg/L
10
0.0620
0.100
9330014
EPA 6010D
10/31/19 12:20
JDH
Silver[7440-22-4]^
0.0190
U
mg/L
10
0.0190
0.100
9330014
EPA 6010D
10/31/19 12:20
JDH
Sodium [7440-23-5]^
9.54
mg/L
10
4.00
5.00
9330014
EPA 6010D
10/31/19 12:20
JDH
Zinc[7440-66-6]^
0.0440
U
mg/L
10
0.0440
0.100
9330014
EPA 6010D
10/31/19 12:20
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flao
Units
DF
MDL
P L
Batch
Method
Analyzed
By
Notes
Bicarbonate (as CaCO3) [71-52-3]
24
mg/L
1
14
15
9331024
M 4500002 D-201
10/31/19 10:14
PDK
Carbonate (as CaCO3)[3812-32-6]
14
U
mg/L
1
14
15
9331024
M 4500002 D-201
10/31/19 10:14
PDK
Chloride [16887-00-6]^
6.9
mg/L
1
2.2
5.0
9322024
EPA 300.0
10/23/19 01:25
PDK
Cyanide (total) [57-12-5]^
0.0049
U
mg/L
1
0.0049
0.0050
9325006
EPA 335.4
10/25/19 16:35
NMN
Nitrate/Nitrite as N^
0.19
mg/L
1
0.041
0.10
9329026
EPA 353.2
10/30/19 20:52
AKF
Orthophosphate as P [1426-54-42]^
0.34
JB
mg/L
1
0.16
0.50
9323009
EPA 365.1
10/23/19 10:29
NMN
3-01
pH ^
5.7
pH
1
1.0
1.0
9325019
iM 4500H+B-2011
10/25/19 10:38
BDC
Q-01
Phosphorus[7723-14-O]^
0.33
mg/L
1
0.025
0.10
9329007
EPA 365.4
11/01/19 13:22
AKF
Specific Conductance (EC) at 25 Deg
94
umhos/cm
1
1.0
1.0
9331027
SM 251OB-2011
10/31/19 11:00
JOC
C^
Sulfate as SO4 [14808-79-8]^
2.9
U
mg/L
1
2.9
5.0
9J22024
EPA 300.0
10/23/19 01:25
PDK
Temperature for pH (deg. C)
20
pH
1
9125019
3M 450011+13-2011
10/25/19 10:38
BDC
Q-01
Total Alkalinity as CaCO3 [471-34-1]^
24
mg/L
1
14
15
9128025
EPA 310.2
10/28/19 17:30
AKF
Total Dissolved Solids^
50
U
mg/L
1
50
50
9J24009
SM 2540C-2011
10/24/19 14:15
JOC
Total Kjeldahl Nitrogen^
3.3
mg/L
1
0.26
0.48
9129006
EPA 351.2
10/31/19 19:35
AKF
Total Nitrogen [17778-88-0]
3.5
mg/L
1
0.26
0.48
[CALC]
CALC
10/31/19 19:35
AKF
Total Suspended Solids^
6.8
U
mg/L
2.7
6.8
6.8
9J28023
SM 2540D-2011
10/28/19 14:27
BDC
1-06,
LP-03
Turbidity^
0.50
U
NTU
1
0.50
1.0
9J22034
SM 213OB-2011
10/22/19 15:28
JOC
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 23

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ANALYTICAL RESULTS
Description: RO Permeate Lab Sample ID:CC17860-03 Received: 10/22/19 11:58
Matrix: Waste Water Sampled:10/21/19 10:50 Work Order: CC17860
Project: RO Pilot Sampled By:Jelena El Barigi
Classical Chemistry Parameters (Dissolved)
^ - ENCO Cary certified analyte [NC 5911
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Biochemical Oxygen Demand^ 2.0 U mg/L 1 2.0 2.0 9323001 SM 5210 B-2011 10/23/19 09:43 JOC
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 23

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ANALYTICAL RESULTS
Description: RO Reject Lab Sample ID:CC17860-04 Received: 10/22/19 11:58
Matrix: Waste Water Sampled:10/21/19 10:50 Work Order: CC17860
Project: RO Pilot Sampled By:Jelena El Barigi
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flao Units DF MDL P L Batch Method
Analyzed -By Notes
Mercury[7439-97-6]^ 0.000750 U mg/L 5 0.000750 0.00100 9330032 EPA 7470A
10/31/19 14:57 KAH
Silica (Si02) [763-18-69]^ 166 mg/L 10 0.3 2.1 9330014 EPA 6010D
10/31/19 12:23 JDH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flao
Units
DF
MDL
P L
Batch
Method
Analyzed
By
Notes
Aluminum [7429-90-5]^
0.420
U
mg/L
10
0.420
1.00
9330014
EPA 6010D
10/31/19 12:23
JDH
Arsenic[7440-38-2]^
0.0760
U
mg/L
10
0.0760
0.100
9330014
EPA 6010D
10/31/19 12:23
JDH
Boron [7440-42-8]^
0.234
J
mg/L
10
0.0570
0.500
9330014
EPA 6010D
10/31/19 12:23
JDH
Cadmium [7440-43-9]^
0.00360
U
mg/L
10
0.00360
0.0100
9330014
EPA 6010D
10/31/19 12:23
JDH
Calcium [7440-70-2]^
737
mg/L
10
0.390
1.00
9330014
EPA 6010D
10/31/19 12:23
JDH
Chromium [7440-47-3]^
0.0259
J
mg/L
10
0.0140
0.100
9330014
EPA 6010D
10/31/19 12:23
JDH
Copper[7440-50-8]^
0.0253
J
mg/L
10
0.0160
0.100
9330014
EPA 6010D
10/31/19 12:23
JDH
Iron [7439-89-6]^
3.63
mg/L
10
0.220
0.500
9330014
EPA 6010D
10/31/19 12:23
JDH
Lead [7439-92-1]^
0.0310
U
mg/L
10
0.0310
0.100
9330014
EPA 6010D
10/31/19 12:23
JDH
Magnesium [7439-95-4]^
42.5
mg/L
10
0.290
1.00
9330014
EPA 6010D
10/31/19 12:23
JDH
Molybdenum [7439-98-7]^
0.0294
J
mg/L
10
0.0250
0.100
9330014
EPA 6010D
10/31/19 12:23
JDH
Nickel[7440-02-O]^
0.0403
J
mg/L
10
0.0220
0.100
9330014
EPA 6010D
10/31/19 12:23
JDH
Potassium [7440-09-7]^
2760
mg/L
10
1.50
5.00
9330014
EPA 6010D
10/31/19 12:23
JDH
Selenium [7782-49-2]^
0.0620
U
mg/L
10
0.0620
0.100
9330014
EPA 6010D
10/31/19 12:23
JDH
Silver[7440-22-4]^
0.0190
U
mg/L
10
0.0190
0.100
9330014
EPA 6010D
10/31/19 12:23
JDH
Sodium [7440-23-5]^
2840
mg/L
10
4.00
5.00
9330014
EPA 6010D
10/31/19 12:23
JDH
Zinc [7440-66-6]^
0.146
mg/L
10
0.0440
0.100
9330014
EPA 6010D
10/31/19 12:23
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flao
Units
DF
MDL
P L
Batch
Method
Analyzed
By
Notes
Bicarbonate (as CaCO3) [71-52-3]
1900
mg/L
1
14
15
9331024
M 4500002 D-201
10/31/19 10:14
PDK
Carbonate (as CaCO3)[3812-32-6]
14
U
mg/L
1
14
15
9331024
M 4500002 D-201
10/31/19 10:14
PDK
Chemical Oxygen Demand^
1200
mg/L
2
20
20
9324013
SM 5220D-2011
10/24/19 16:38
JOC
Chloride [16887-00-6]^
2700
D
mg/L
100
220
500
9322024
EPA 300.0
10/23/19 11:59
PDK
Cyanide (total) [57-12-5]^
0.0049
U
mg/L
1
0.0049
0.0050
9325006
EPA 335.4
10/25/19 16:36
NMN
Nitrate/Nitrite as N^
12
D
mg/L
48
2.0
4.8
9329026
EPA 353.2
10/30/19 20:53
AKF
Orthophosphate as P [1426-54-42]^
55
BD
mg/L
10
1.6
5.0
9323009
EPA 365.1
10/23/19 10:48
NMN
QB-01
pH ^
7.3
pH
1
1.0
1.0
9325019
iM 4500H+B-2011
10/25/19 10:38
BDC
Q-01
Phosphorus[7723-14-0]^
78
D
mg/L
50
1.2
5.0
9329007
EPA 365.4
11/07/19 14:21
AKF
Specific Conductance (EC) at 25 Deg
20000
umhos/cm
1
1.0
1.0
9331027
SM 251OB-2011
10/31/19 11:00
JOC
C^
Sulfate as SO4 [14808-79-8]^
5400
D
mg/L
100
290
500
9122024
EPA 300.0
10/23/19 11:59
PDK
Temperature for pH (deg. C)
20
pH
1
9125019
3M 4500H+B-2011
10/25/19 10:38
BDC
Q-01
Total Alkalinity as CaCO3 [471-34-1]^
1900
D
mg/L
10
140
150
9128025
EPA 310.2
10/28/19 17:31
AKF
Total Dissolved Solids^
16000
mg/L
1
50
50
9124009
SM 2540C-2011
10/24/19 14:15
JOC
Total Kjeldahl Nitrogen^
180
D
mg/L
10
2.6
4.8
9129006
EPA 351.2
11/01/19 15:42
AKF
Total Nitrogen [17778-88-0]
190
D
mg/L
48
2.6
4.8
[CALC]
CALC
11/01/19 15:42
AKF
Total Suspended Solids^
2.7
mg/L
1
2.5
2.5
9124010
SM 2540D-2011
10/24/19 09:57
JAH
Turbidity^
3.9
NTU
1
0.50
1.0
9122034
SM 213OB-2011
10/22/19 15:28
JOC
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 23

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 9.730014 - EPA 3005A
Blank (9330014-BLK3) Prepared: 10/30/2019 09:44 Analyzed: 10/31/2019 11:45
Spike Source %REC
RPD
Analvte
Result
Flaq
Q
Units
Level Result %REC Limits RPD
Limit Notes
Silica (Si02)
0.03
U
0.2
mg/L
Blank (9330014-BLK2)
Prepared: 10/30/2019 09:44 Analyzed: 10/31/2019 11:48
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Silica (Si02)
0.03
U
0.2
mg/L
Batch 9130032 - EPA 7470A
Blank (9330032-BLK1) Prepared: 10/30/2019 13:45 Analyzed: 10/31/2019 13:43
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Mercury 0.000150 U 0.000200 mg/L
LCS (9330032-BS3) Prepared: 10/30/2019 13:45 Analyzed: 10/31/2019 13:46
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00500
0.000200
mg/L
0.00500
100
80-120
Matrix Spike (9330032-MS3)
Prepared: 10/30/2019 13:45 Analyzed: 10/31/2019 13:52
Source: CC14867-04
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00488
0.000200
mg/L
0.00500
0.000150 U
98
75-125
Matrix Spike Dup (9330032-MSDI)
Prepared: 10/30/2019 13:45 Analyzed: 10/31/2019 13:54
Source: CC14867-04
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00490
0.000200
mg/L
0.00500
0.000150 U
98
75-125 0.4
25
Post Spike (9330032-PS3)
Prepared: 10/30/2019 13:45 Analyzed: 10/31/2019 14:01
Source: CC14867-04
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
5.61
0.200
ug/L
5.00
-0.0450
112
75-125
Metals (total recoverable) by EPA 6000/7000
Series Methods - Quality Control
Batch 9.730014 - EPA 3005A
Blank (9330014-BLK3) Prepared: 10/30/2019 09:44 Analyzed: 10/31/2019 11:45
Analvte
Result
Flaq
Q
Units
Aluminum
0.0420
U
0.100
mg/L
Arsenic
0.00760
U
0.0100
mg/L
Boron
0.00570
U
0.0500
mg/L
Cadmium
0.000360
U
0.00100
mg/L
Calcium
0.0390
U
0.100
mg/L
Chromium
0.00140
U
0.0100
mg/L
Copper
0.00160
U
0.0100
mg/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit
Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 23

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 9J30014 - EPA 3005A - Continued
Blank (9330014-BLK3) Continued Prepared: 10/30/2019 09:44 Analyzed: 10/31/2019 11:45
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Iron
0.0220
U
0.0500
mg/L
Lead
0.00310
U
0.0100
mg/L
Magnesium
0.0290
U
0.100
mg/L
Molybdenum
0.00250
U
0.0100
mg/L
Nickel
0.00220
U
0.0100
mg/L
Potassium
0.150
U
0.500
mg/L
Selenium
0.00620
U
0.0100
mg/L
Silver
0.00190
U
0.0100
mg/L
Sodium
0.400
U
0.500
mg/L
Zinc
0.00440
U
0.0100
mg/L
Blank (9330014-BLK2)
Prepared: 10/30/2019 09:44 Analyzed: 10/31/2019 11:48
Spike Source %REC RPD
Analvte
Result
Flaq
PQL
Units
Level Result %REC Limits RPD Limit Notes
Aluminum
0.0420
U
0.100
mg/L
Arsenic
0.00760
U
0.0100
mg/L
Boron
0.00570
U
0.0500
mg/L
Cadmium
0.000360
U
0.00100
mg/L
Calcium
0.0390
U
0.100
mg/L
Chromium
0.00140
U
0.0100
mg/L
Copper
0.00160
U
0.0100
mg/L
Iron
0.0220
U
0.0500
mg/L
Lead
0.00310
U
0.0100
mg/L
Magnesium
0.0290
U
0.100
mg/L
Molybdenum
0.00250
U
0.0100
mg/L
Nickel
0.00220
U
0.0100
mg/L
Potassium
0.150
U
0.500
mg/L
Selenium
0.00620
U
0.0100
mg/L
Silver
0.00190
U
0.0100
mg/L
Sodium
0.400
U
0.500
mg/L
Zinc
0.00440
U
0.0100
mg/L
LCS (9330014-BS1)
Prepared: 10/30/2019 09:44 Analyzed: 10/31/2019 11:54
Spike
Source
%REC RPD
Analvte
Result
Flaq POL
Units
Level
Result %REC
Limits RPD Limit Notes
Aluminum
1.90
0.100
mg/L
2.00
95
80-120
Arsenic
0.192
0.0100
mg/L
0.200
96
80-120
Boron
0.964
0.0500
mg/L
1.00
96
80-120
Cadmium
0.0195
0.00100
mg/L
0.0200
98
80-120
Calcium
2.01
0.100
mg/L
2.00
100
80-120
Chromium
0.189
0.0100
mg/L
0.200
94
80-120
Copper
0.183
0.0100
mg/L
0.200
92
80-120
Iron
0.949
0.0500
mg/L
1.00
95
80-120
Lead
0.190
0.0100
mg/L
0.200
95
80-120
Magnesium
1.92
0.100
mg/L
2.00
96
80-120
Molybdenum
0.185
0.0100
mg/L
0.200
92
80-120
Nickel
0.192
0.0100
mg/L
0.200
96
80-120
Potassium
9.90
0.500
mg/L
10.0
99
80-120
Selenium
0.189
0.0100
mg/L
0.200
95
80-120
FINAL
This report relates only to the sample as received by the
laboratory, and
may only be reproduced in
full. Page 12 of 23

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 9J30014 - EPA 3005A - Continued
LCS (9330014-BS3) Continued Prepared: 10/30/2019 09:44 Analyzed: 10/31/2019 11:54
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Silver
0.197
0.0100
mg/L
0.200
98
80-120
Sodium
9.85
0.500
mg/L
10.0
98
80-120
Zinc
0.207
0.0100
mg/L
0.200
103
80-120
Matrix Spike (9330014-MS1)
Prepared:
10/30/2019
09:44 Analyzed: 10/31/2019 11:57
Source: CC14867-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Aluminum
1.99
0.100
mg/L
2.00
0.0831
95
75-125
Arsenic
0.192
0.0100
mg/L
0.200
0.00760 U
96
75-125
Boron
1.00
0.0500
mg/L
1.00
0.00759
100
75-125
Cadmium
0.0197
0.00100
mg/L
0.0200
0.000360 U
98
75-125
Calcium
12.2
0.100
mg/L
2.00
10.9
70
75-125
QM-07
Chromium
0.194
0.0100
mg/L
0.200
0.00170
96
75-125
Copper
0.187
0.0100
mg/L
0.200
0.00160 U
93
75-125
Iron
1.83
0.0500
mg/L
1.00
0.907
92
75-125
Lead
0.194
0.0100
mg/L
0.200
0.00310 U
97
75-125
Magnesium
8.49
0.100
mg/L
2.00
6.73
88
75-125
Molybdenum
0.191
0.0100
mg/L
0.200
0.00250 U
95
75-125
Nickel
0.198
0.0100
mg/L
0.200
0.00399
97
75-125
Potassium
14.1
0.500
mg/L
10.0
4.21
99
75-125
Selenium
0.191
0.0100
mg/L
0.200
0.00620 U
95
75-125
Silver
0.196
0.0100
mg/L
0.200
0.00190 U
98
75-125
Sodium
17.9
0.500
mg/L
10.0
8.34
96
75-125
Zinc
0.214
0.0100
mg/L
0.200
0.00782
103
75-125
Matrix Spike Dup (9330014-MSD1)
Prepared:
10/30/2019
09:44 Analyzed: 10/31/2019 11:59
Source: CC14867-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Aluminum
2.10
0.100
mg/L
2.00
0.0831
101
75-125
6
20
Arsenic
0.193
0.0100
mg/L
0.200
0.00760 U
96
75-125
0.3
20
Boron
1.02
0.0500
mg/L
1.00
0.00759
101
75-125
1
20
Cadmium
0.0198
0.00100
mg/L
0.0200
0.000360 U
99
75-125
0.5
20
Calcium
12.7
0.100
mg/L
2.00
10.9
92
75-125
4
20
Chromium
0.196
0.0100
mg/L
0.200
0.00170
97
75-125
1
20
Copper
0.189
0.0100
mg/L
0.200
0.00160 U
94
75-125
1
20
Iron
1.93
0.0500
mg/L
1.00
0.907
103
75-125
5
20
Lead
0.195
0.0100
mg/L
0.200
0.00310 U
98
75-125
0.8
20
Magnesium
8.63
0.100
mg/L
2.00
6.73
95
75-125
2
20
Molybdenum
0.192
0.0100
mg/L
0.200
0.00250 U
96
75-125
0.5
20
Nickel
0.199
0.0100
mg/L
0.200
0.00399
98
75-125
0.7
20
Potassium
14.4
0.500
mg/L
10.0
4.21
102
75-125
2
20
Selenium
0.193
0.0100
mg/L
0.200
0.00620 U
97
75-125
1
20
Silver
0.199
0.0100
mg/L
0.200
0.00190 U
99
75-125
2
20
Sodium
18.4
0.500
mg/L
10.0
8.34
100
75-125
3
20
Zinc
0.217
0.0100
mg/L
0.200
0.00782
105
75-125
2
20
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 23

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 9J30014 - EPA 3005A - Continued
Post Spike (9]30014-PS1)
Prepared: 10/30/2019 09:44 Analyzed: 10/31/2019 12:02
Source: CC14867-01
Spike
Source
%REC RPD
Analvte
Result
Flaq Q
Units
Level
Result
%REC
Limits RPD Limit Notes
Aluminum
2.03
0.100
mg/L
2.00
0.0831
97
80-120
Arsenic
0.201
0.0100
mg/L
0.200
-0.00179
100
80-120
Boron
1.03
0.0500
mg/L
1.00
0.00759
103
80-120
Cadmium
0.0202
0.00100
mg/L
0.0200
0.000319
99
80-120
Calcium
12.1
0.100
mg/L
2.00
10.9
62
80-120 QM-08
Chromium
0.199
0.0100
mg/L
0.200
0.00170
99
80-120
Copper
0.191
0.0100
mg/L
0.200
4.26E-5
96
80-120
Iron
1.89
0.0500
mg/L
1.00
0.907
99
80-120
Lead
0.198
0.0100
mg/L
0.200
-0.00192
99
80-120
Magnesium
8.41
0.100
mg/L
2.00
6.73
84
80-120
Molybdenum
0.194
0.0100
mg/L
0.200
0.00104
96
80-120
Nickel
0.202
0.0100
mg/L
0.200
0.00399
99
80-120
Potassium
13.9
0.500
mg/L
10.0
4.21
97
80-120
Selenium
0.195
0.0100
mg/L
0.200
-0.00705
98
80-120
Silver
0.207
0.0100
mg/L
0.200
-0.000466
103
80-120
Sodium
17.7
0.500
mg/L
10.0
8.34
94
80-120
Zinc
0.218
0.0100
mg/L
0.200
0.00782
105
80-120
Metals (Dissolved) by EPA 6000/7000
Series
Methods - Quality
Control
Batch 9J30014 - EPA 3005A
Blank (9330014-BLK3)
Prepared: 10/30/2019 09:44 Analyzed: 10/31/2019 11:45
Spike Source %REC
RPD
Analvte
Result
Flaq
PQL
Units
Level Result %REC Limits RPD
Limit Notes
Calcium
0.0390
U
0.100
mg/L
Magnesium
29.0
U
100
ug/L
Silica (Si02)
0.03
U
0.2
mg/L
Blank (9330014-BLK2)
Prepared: 10/30/2019 09:44 Analyzed: 10/31/2019 11:48
Spike Source %REC
RPD
Analvte
Result
Flaq
PQL
Units
Level Result %REC Limits RPD
Limit Notes
Calcium
0.0390
U
0.100
mg/L
Magnesium
29.0
U
100
ug/L
Silica (Si02)
0.03
U
0.2
mg/L
LCS (9330014-BSI)
Prepared: 10/30/2019 09:44 Analyzed: 10/31/2019 11:54
Spike Source %REC
RPD
Analvte
Result
Flaq
PQL
Units
Level Result %REC Limits RPD
Limit Notes
Calcium
2.01
0.100
mg/L
2.00 100 80-120
Magnesium
1920
100
ug/L
2000 96 80-120
Matrix Spike (9330014-MS1)
Prepared: 10/30/2019 09:44 Analyzed: 10/31/2019 11:57
Source: CC14867-01
Spike Source %REC RPD
Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes
Calcium 12.2 0.100 mg/L 2.00 10.9 70 75-125 QM-07
Magnesium 8490 100 ug/L 2000 6730 88 75-125
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 14 of 23

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QUALITY CONTROL DATA
Metals (Dissolved) by EPA 6000/7000 Series Methods - Quality Control
Batch 9J30014 - EPA 3005A - Continued
Matrix Spike Dup (9130014-MSDI)
Prepared: 10/30/2019 09:44 Analyzed: 10/31/2019 11:59
Source: CC14867-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Calcium
12.7
0.100
mg/L
2.00
10.9
92
75-125 4
20
Magnesium
8630
100
ug/L
2000
6730
95
75-125 2
20
Post Spike (9330014-PS1)
Prepared: 10/30/2019 09:44 Analyzed: 10/31/2019 12:02
Source: CC14867-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Calcium
12.1
0.100
mg/L
2.00
10.9
62
80-120
QM-08
Magnesium
8.41
0.100
mg/L
2.00
6.73
84
80-120
Classical Chemistry Parameters - Quality Control
Batch 9J22024 - NO PREP
Blank (9122024-BLK3) Prepared: 10/22/2019 12:48 Analyzed: 10/22/2019 19:32
Spike Source %REC RPD
Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes
Chloride 2.2 U 5.0 mg/L
Sulfate as SO4 2.9 U 5.0 mg/L
LCS (9322024-BSI) Prepared: 10/22/2019 12:48 Analyzed: 10/22/2019 19:49
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chloride
51
5.0
mg/L
50.0 102 90-110
Sulfate as SO4
50
5.0
mg/L
50.0 99 90-110
Matrix Spike (9322024-MS3)
Prepared: 10/22/2019 12:48 Analyzed: 10/22/2019 20:25
Source: CC17199-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chloride
19
5.0
mg/L
20.0 2.2 U 96 90-110
Sulfate as SO4
20
5.0
mg/L
20.0 2.9 U 98 90-110
Matrix Spike (9722024-MS2)
Prepared: 10/22/2019 12:48 Analyzed: 10/22/2019 21:18
Source: CC14655-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chloride
24
5.0
mg/L
20.0 5.4 95 90-110
Sulfate as SO4
31
5.0
mg/L
20.0 12 94 90-110
Matrix Spike Dup (9322024-MSDI)
Prepared: 10/22/2019 12:48 Analyzed: 10/22/2019 20:42
Source: CC17199-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chloride
20
5.0
mg/L
20.0 2.2 U 98 90-110 2
10
Sulfate as SO4
20
5.0
mg/L
20.0 2.9 U 101 90-110 3
10
Batch 9J22034 - NO PREP
Blank (9322034-BLK3) Prepared & Analyzed: 10/22/2019 15:28
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 15 of 23

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9J22O34 - NO PREP - Continued
Blank (9322034-BLK3) Continued Prepared & Analyzed: 10/22/2019 15:28
Spike Source %REC RPD
Analvte Result Flag Q Units Level Result %REC Limits RPD Limit Notes
Turbidity 0.50 U 1.0 NTU
LCS (9322034-BSI) Prepared & Analyzed: 10/22/2019 15:28
Spike Source %REC
RPD
Analvte
Result Flag
POL
Units
Level Result %REC Limits RPD
Limit Notes
Turbidity
20
1.0
NTU
20.0 98 80-120
Duplicate (9322034-DUPl)
Prepared & Analyzed: 10/22/2019 15:28
Source: CC14655-01
Spike Source %REC
RPD
Analvte
Result Flag
POL
Units
Level Result %REC Limits RPD
Limit Notes
Turbidity
0.83 J
1.0
NTU
0.84 1
25
Batch 9J23OO9 - NO PREP
Blank (9323009-BLK3) Prepared: 10/23/2019 09:53 Analyzed: 10/23/2019 09:53
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Orthophosphate as P
0.30
3
0.50
mg/L
3-01, QB-0,
LCS (9323009-BSI)
Prepared & Analyzed: 10/23/2019 09:53
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Orthophosphate as P
5.5
B
0.50
mg/L
5.00 109 90-110
Matrix Spike (9323009-MS1)
Prepared: 10/23/2019 10:27 Analyzed: 10/23/2019 10:27
Source: CC17860-02
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Orthophosphate as P
11
BE
0.50
mg/L
2.00 8.1 127 90-110
QM-07
Matrix Spike Dup (9323009-MSDI)
Prepared: 10/23/2019 10:28 Analyzed: 10/23/2019 10:28
Source: CC17860-02
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Orthophosphate as P
11
BE
0.50
mg/L
2.00 8.1 137 90-110
2
10
QM-07
Batch 9J24OO9 - NO PREP
Blank (9324009-BLK3)
Prepared & Analyzed: 10/24/2019 14:15
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Total Dissolved Solids
50
U
50
mg/L
LCS (9324009-BSI)
Prepared & Analyzed: 10/24/2019 14:15
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Total Dissolved Solids
1000
50
mg/L
1000 101 80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 16 of 23

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9J24009 - NO PREP - Continued
Duplicate (9324009-DUPl)
Prepared & Analyzed: 10/24/2019 14:15
Source: CC14867-01
Spike Source %REC
RPD
Analvte
Result Flag
Q
Units
Level Result %REC Limits
RPD
Limit Notes
Total Dissolved Solids
100
50
mg/L
96
4
20
Duplicate (9324009-DUP2)
Prepared & Analyzed: 10/24/2019 14:15
Source: CC14867-02
Spike Source %REC
RPD
Analvte
Result Flag
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Total Dissolved Solids
220
50
mg/L
220
3
20
Batch 9J24010 - NO PREP
Blank (9324010-BLK1) Prepared & Analyzed: 10/24/2019 09:57
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Total Suspended Solids 2.5 U 2.5 mg/L
LCS (9324030-BS3) Prepared & Analyzed: 10/24/2019 09:57
Spike Source %REC
RPD
Analvte
Result Flag
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Total Suspended Solids
85
2.5
mg/L
100 85 80-120
Duplicate (9324030-DUP3)
Prepared & Analyzed: 10/24/2019 09:57
Source: CC14778-01
Spike Source %REC
RPD
Analvte
Result Flag
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Total Suspended Solids
45
25
mg/L
51
12
20
Duplicate (9324030-DUP2)
Prepared & Analyzed: 10/24/2019 09:57
Source: CC15631-01
Spike Source %REC
RPD
Analvte
Result Flag
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Total Suspended Solids
240
45
mg/L
230
1
20
Batch 9J24013 - Same
Blank (9324013-BLK3) Prepared: 10/24/2019 11:19 Analyzed: 10/24/2019 16:38
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Chemical Oxygen Demand 10 U 10 mg/L
LCS (9324013-BSI) Prepared: 10/24/2019 11:19 Analyzed: 10/24/2019 16:38
Spike
Source
%REC
RPD
Analvte
Result Flag
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Chemical Oxygen Demand
500
10
mg/L
500
101
90-110
Matrix Spike (9324013-MS1)
Prepared: 10/24/2019 11:19 Analyzed: 10/24/2019 16:38
Source: CC14778-01
Spike
Source
%REC
RPD
Analvte
Result Flag
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Chemical Oxygen Demand
820
10
mg/L
526
300
98
90-110
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 17 of 23

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9J24013 - Same - Continued
Matrix Spike Dup (9124013-MSDI) Prepared: 10/24/2019 11:19 Analyzed: 10/24/2019 16:38
Source: CC14778-01
Spike Source %REC RPD
Analvte Result Flag Q Units Level Result %REC Limits RPD Limit Notes
Chemical Oxygen Demand 790 10 mg/L 526 300 93 90-110 3 5
Batch 9J25006 - Same
Blank (9325006-BLK3) Prepared: 10/25/2019 09:36 Analyzed: 10/25/2019 15:45
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Cyanide (total) 0.0049 U 0.0050 mg/L
LCS (9325006-BSI) Prepared: 10/25/2019 09:36 Analyzed: 10/25/2019 16:16
Spike
Source
%REC
RPD
Analvte
Result
Flag POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Cyanide (total)
0.14
0.0050
mg/L
0.150
93
90-110
Matrix Spike (9325006-MS3)
Prepared: 10/25/2019 09:36 Analyzed: 10/25/2019 16:20
Source: CC17860-02
Spike
Source
%REC
RPD
Analvte
Result
Flag Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Cyanide (total)
0.11
0.0050
mg/L
0.150
0.0049 U
76
90-110
QM-07
Matrix Spike Dup (9325006-MSD3)
Prepared: 10/25/2019 09:36 Analyzed: 10/25/2019 16:22
Source: CC17860-02
Spike
Source
%REC
RPD
Analvte
Result
Flag POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Cyanide (total)
0.12
0.0050
mg/L
0.150
0.0049 U
82
90-110 7
10
QM-07
Batch 9J25019 - NO PREP
LCS (9325019-BSI) Prepared & Analyzed: 10/25/2019 10:38
Spike Source %REC
RPD
Analvte
Result Flag
POL
Units
Level Result %REC Limits RPD
Limit Notes
pH
7.0
1.0
pH
7.00 100 99-101
Duplicate (9725019-DUPl)
Prepared & Analyzed: 10/25/2019 10:38
Source: CCO1090-02
Spike Source %REC
RPD
Analvte
Result Flag
POL
Units
Level Result %REC Limits RPD
Limit Notes
pH
6.8
1.0
pH
6.9 2
25
Batch 9J28023 - NO PREP
Blank (9328023-BLK3) Prepared & Analyzed: 10/28/2019 14:27
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Total Suspended Solids 2.5 U 2.5 mg/L
LCS (9328023-BSI) Prepared & Analyzed: 10/28/2019 14:27
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Total Suspended Solids 70 2.5 mg/L 100 70 80-120 3-06
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 18 of 23

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9J28023 - NO PREP - Continued
Duplicate (9128023-DUPl)
Prepared & Analyzed: 10/28/2019 14:27
Source: CC17388-01
Spike Source %REC
RPD
Analvte
Result Flag
Q
Units
Level Result %REC Limits
RPD
Limit Notes
Total Suspended Solids
25
25
mg/L
26
4
20
Duplicate (9328023-DUP2)
Prepared & Analyzed: 10/28/2019 14:27
Source: CC15630-01
Spike Source %REC
RPD
Analvte
Result Flag
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Total Suspended Solids
220
49
mg/L
240
11
20
Batch 9J28015 - NO PREP
Blank (9328025-BLK1) Prepared: 10/28/2019 15:13 Analyzed: 10/28/2019 17:13
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Total Alkalinity as CaCO3 14 U 15 mg/L
LCS (9728025-BS3) Prepared: 10/28/2019 15:13 Analyzed: 10/28/2019 17:14
Spike
Source
%REC
RPD
Analvte
Result Flag
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Total Alkalinity as CaCO3
100
15
mg/L
100
103
80-120
Matrix Spike (9328025-MS3)
Prepared: 10/28/2019 15:13 Analyzed: 10/28/2019 17:15
Source: CC17199-01
Spike
Source
%REC
RPD
Analvte
Result Flag
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Total Alkalinity as CaCO3
37
15
mg/L
37.8
14 U
98
80-120
Matrix Spike Dup (9328025-MSDI)
Prepared: 10/28/2019 15:13 Analyzed: 10/28/2019 17:16
Source: CC17199-01
Spike
Source
%REC
RPD
Analvte
Result Flag
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Total Alkalinity as CaCO3
36
15
mg/L
37.8
14 U
95
80-120 4
25
Batch 9J29006 - Same
Blank (9329006-BLK3)
Prepared: 10/29/2019 10:54 Analyzed: 10/31/2019 18:43
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Kjeldahl Nitrogen
0.26
U
0.48
mg/L
Blank (9329006-BLK2)
Prepared: 10/29/2019 08:14 Analyzed: 11/01/2019 15:32
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Kjeldahl Nitrogen
0.26
U
0.48
mg/L
LCS (9329006-BSI)
Prepared: 10/29/2019 10:54 Analyzed: 10/31/2019 18:45
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Kjeldahl Nitrogen
12
0.48
mg/L
12.0 100 90-110
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 19 of 23

QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9J29006 - Same - Continued
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LCS (9129006-BS2) Prepared: 10/29/2019 08:14 Analyzed: 11/01/2019 15:33
Spike Source %REC
RPD
Analvte
Result
Flaq
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
13
0.48
mg/L
12.0 105 90-110
Matrix Spike (9329006-MS3)
Prepared: 10/29/2019 10:54 Analyzed: 10/31/2019 18:54
Source: CC14655-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
4.7
0.48
mg/L
4.80 0.26 U 98 90-110
Matrix Spike (9329006-MS2)
Prepared: 10/29/2019 10:54 Analyzed: 11/01/2019 15:39
Source: CC16320-02RE1
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
35
D
0.96
mg/L
4.80 30 109 90-110
Matrix Spike Dup (9729006-MSDI)
Prepared: 10/29/2019 10:54 Analyzed: 10/31/2019 18:55
Source: CC14655-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
4.8
0.48
mg/L
4.80 0.26 U 99 90-110 1
10
Batch 9J29007 - Same
Blank (9329007-BLK3) Prepared: 10/29/2019 10:54 Analyzed: 11/01/2019 12:45
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Phosphorus 0.025 U 0.10 mg/L
Blank (9329007-BLK2) Prepared: 10/29/2019 10:54 Analyzed: 11/07/2019 14:02
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Phosphorus 0.025 U 0.10 mg/L
LCS (9729007-BS1) Prepared: 10/29/2019 10:54 Analyzed: 11/01/2019 12:46
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Phosphorus 1.6 0.10 mg/L 1.60 98 80-120
LCS (9329007-BS2) Prepared: 10/29/2019 10:54 Analyzed: 11/07/2019 14:03
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Phosphorus
1.6
0.10
mg/L
1.60 98 80-120
Matrix Spike (9329007-MS1)
Prepared: 10/29/2019 10:54 Analyzed: 11/01/2019 12:53
Source: CC14655-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Phosphorus
0.60
0.10
mg/L
0.640 0.025 U 94 80-120
Matrix Spike Dup (9729007-MSD1)
Prepared: 10/29/2019 10:54 Analyzed: 11/01/2019 12:54
Source: CC14655-01
Spike Source %REC RPD
Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Notes
Page 20 of 23

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9J29007 - Same - Continued
Matrix Spike Dup (9129007-MSDI) Continued Prepared: 10/29/2019 10:54 Analyzed: 11/01/2019 12:54
Source: CC14655-01
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Phosphorus 0.60 0.10 mg/L 0.640 0.025 U 94 80-120 0.2 25
Batch 9J29026 - NO PREP
Blank (9329026-BLK3)
Prepared: 10/30/2019 20:12 Analyzed: 10/30/2019 20:12
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
0.041
Ll
0.10
mg/L
LCS (9329026-BSI)
Prepared & Analyzed: 10/30/2019 20:14
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
1.3
0.10
mg/L
1.25 104 90-110
Matrix Spike (9329026-MS3)
Prepared: 10/30/2019 20:17 Analyzed: 10/30/2019 20:17
Source: CC16854-07
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
0.68
0.10
mg/L
0.521 0.18 96 90-110
Matrix Spike (9329026-MS2)
Prepared: 10/30/2019 20:22 Analyzed: 10/30/2019 20:22
Source: CC14778-01
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
27
5.0
mg/L
25.0 2.4 100 90-110
Matrix Spike Dup (9329026-MSDI)
Prepared: 10/30/2019 20:19 Analyzed: 10/30/2019 20:19
Source: CC16854-07
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
0.69
0.10
mg/L
0.521 0.18 98 90-110 2
10
Batch 9.731027 - NO PREP
Blank (9331027-BLK3)
Prepared & Analyzed: 10/31/2019 11:00
Spike Source %REC
RPD
Analvte
Result
Flag
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Specific Conductance (EC) at 25 Deg C
1.0
Ll
1.0
umhos/cm
LCS (9333027-BSI)
Prepared & Analyzed: 10/31/2019 11:00
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Specific Conductance (EC) at 25 Deg C
720
1.0
umhos/cm
705 102 90-110
Duplicate (9333027-DUPl)
Prepared & Analyzed: 10/31/2019 11:00
Source: CC15630-03
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Specific Conductance (EC) at 25 Deg C
840
1.0
umhos/cm
840 0.1
25
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 21 of 23

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
3-01 Result may be biased high due to positive results in the associated method blank at a concentration above
the MDL and/or greater than one-half the MRL.
3-06 The associated laboratory control sample exhibited low bias; the reported result should be considered to
be a minimum estimate.
LP-03 Sample amount received by the laboratory did not meet minimum method requirements for analysis.
Q-01 Analysis performed outside of method - specified holding time.
QB-01 The method blank had a positive result for the analyte; however, the concentration in the method blank is
less than 10% of the sample result. There is minimal impact to the data.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 22 of 23

ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com
14
cei \S C� 10775 Central Port Dr. 4810 Executive Park Court, Suite 111 102-A Woodwinds Industrial Ct
Orlando. FL 32824 Jacksonville, FL 32216-6069 Cary, NC 27511
[phone] Fax [phone] (904) 296-3D07 Fax [phone] [phone] Fax [phone] Page of
Client Name
Novazyrnes North America (NO008)
Project Number
[none]
Requested
Analyses
Requested Turnaround
Times
Note: Rush requests subject to
acceptance by the facility
Standard
/� Expedited
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Address
77 Pernf Chapel Church Road1L0
Prro�,ectt NamelDesc
I�II()t
CitylSTOp
Frankllnton, NC 27525
PO # 1 Billin Info
380OW 507
Tel Fax
[phone]
Re orting Contact
S�C4tt Creech
Sampler(s) Name, Affiliation (Print)
Bit' 'ng Contact
Recounts Payable.
Sampleris) Signature
t��
Sde Location I Time Zone
lab Workprder
Preservation
(See
Codes)
(Combine
as necessary)
llem ii
Sample 0 (Field Identification)
Collection Date
Collection
Time
Comp I Grab
Matrix
(see codes)
Total # of
Containers
,S ple Comments
BBR Feed
11,0 j -L t
Ja" o
'�
WW
2
X
X
O Feed
O Permeate
�ZI ��
jC'121(19
`1
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WW
WW
5
5
X
X
X
X
X
X
X
X
X
x
X
X
X
X
X
X
O Reject
\c r Z l i l9
C' •'q�
1
WW
5
X
X
X
X
X
X
X
X
Total # of Containers
Sample Kit Prepared By Daterrime Relinquished By Date/Time Received By Data -me
` �j�•c �{o1ZI1zo1") r1D K,�`
CommenWSpacial Reporting Requirements
Relinquished By
Date/Time
eceived By
Date(Time I
Qr
Relinqulshed By
DatoMme
Aeceivhty,
OaWrimfT
Cooler it's & Temps on Receipt _
1' 3
Candilian lJ n Receipt
Acceptable Unacceptable
Matrix: GW-Groundwater SO -Soil DW-Drinking Water SE -Sediment SW -Surface Water WW-Wastewater A -Air O-Other (detail in comments) Preservation: blue H-HCl N-HNO3 S-H2504 NO-NaV11 O-Omer {aetaii En comments)
Note 7 All samples submitted to ENCO Labs are in accordance with the terms and conditions listed on the reverse of this form, unless prior written agreements exist

ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com
C� 10775 Central Port Dr. 4810 Executive Park Court, Suite 111 t02-A Woodwinds Industrial Ct.
Orlando. FL 32824 Jacksonville, FL 32216-6069 Cary, NC 27511
[phone] Fax [phone] [phone] Fax [phone] [phone] Fax [phone] Page Of
Client Name
Novazymes North America (N0008)
Pro'ecI Number
['none
Requested
Analyses
Requested Turnaround
Times
Note: Rush requests subject to
acceptance by the facility
Standard
Expedite�d
`
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d
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❑
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Addre
77'%rry Chapel Church Road
PrgigcZN�IfSG 0t
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I�rWklllnl NC 27525
PO # ill'n info
30905507
Tel JFa
[phone]
Re rung Contact
Scott Creech
Samplers) Name, Affiliation (Pant)
adX COAau'nts Payable
Sampler(s) Signature
_irC
Site Location /Time Zone
Lab WOrkOrdef
Preservation
(See
Codes)
(Combine
as necessary)
Item #
Sample ID (Field Identification)
Collection Date
Collection
Time
Comp I Grab
Matrix
(see codes)
Total # of
Containers
a ple Comments
MBBR Feed
tiC 201 ` j
td ,,6�
Ww
2
X
RO Feed
lO 2 1�
•75C,,
C'�
ww
5
X
X
RO Permeate
fi (2� 10
a "50.
C'\
Ww
5
X
X
RO Rill
101(21
lei ., 5o
C-;\
ww
5
X
X
Ll
<-- Total # of Containers
Sample Kit Prepared By
Datums
Relinquished By
11k
Daternme
10 1 z 1 zo19
Re
v %
T
Daty ' a r
Comments/Speciat Reporting Requirements
Relinquished By V
Datemme
Received By
to
Dalerfime
la
Relinquished By
Daterrime
Received By
Date/Time
Cooler #'a & Temps on Receipt
f' t
Condition Upon Receipt
__X_A5Ceptab1e Unacceptable
Matrix: GW-Groundwater SO -Soil Diff-Drinking Water SE -Sediment SW -Surface Water WW-Wastewater A -Air O-Other (detail in comments) Preservation: I -Ice Ill N-NNo3 5-HZS04 No-NeQH o-Other (derail in commentsl
Note : All samples submitted to FNCO Labs are in accordance with the terms and conditions listed on the reverse of this form, unless prior written agreements exist

Sample Preservation Verification 99CEOD
ENCO Cary
Work Order: CC17860 Project: RO Pilot
Client: Novozymes North America (N0008) Project #: [none]
Logged In: 22-Oct-19 12:18 Logged By: John C King -� 7
Preservation Check Performed By: � Date/Time: b .r-(q rp �S
CC17860-02
Cont
Type
Pres (pH)
pH Checked /
pH Adjusted DateMme
Reagent used/Comments
Requirement
In Control
Adjusted
B
250mLP+HNO3
<2
Y I N I NA
Y 'N / NA
C
250mLP+NaOH
>12
I N I NA
Y I / NA
E
500mLP+H2SO4
<2
CY)/ N I NA
rY I I NA
CC17860-03
Cant
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted Date/Time
Adjusted
Reagent tlsedlComments
B
250mLP+HNO3
<2
Y / N / NA
Y 1 / NA
C
250mLP+NaOH
>12
09 / N I NA
Y I 1 NA
E
500mLP+H2SO4
<2
10I N / NA
Y / / NA
CC17860-04
Cont
Type
Pres (pH)
pH Checked /:
pH Adjusted Datelrme
Reagent Used/Comments
Requirement
In Control
Adjusted
8
250mLP+HNO3
<2
Y /& NA
l:J N / NA
C
250mLP+NaOH
>12
0 / N / NA
Y /() / NA
E
500mLP+H2504
<2
by)/ N / NA
I Y / / NA
Rea ent Name M ID
1 `}�G U. t
2
pH Strip ID: q1M �-
Reactent Name ID
3
4
Reagent Name ID
5
6
C:IELMNTIPrintlwko_PreservationCheck. rpt Page 1 of 1

2�SENCO Laboratories
9g
Accurate. Timely. Respousive. luuavative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Friday, December 13, 2019
Novozymes North America (N0008)
Attn: Scott Creech
77 Perry Chapel Church Road
Franklinton, NC 27525
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: RO Pilot
ENCO Workorder(s): CC17678
Dear Scott Creech,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Wednesday, November 20, 2019.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
OUCLC'=-:�CA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 28

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: MBBR Feed
Lab ID: CC17678-01
Sampled: 11/19/19 10:00
Received: 11/20/19 09:45
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
05/17/20
11/22/19 10:47
12/04/19 11:32
SM 5210 B-2011
NO PREP
11/21/19 10:00
11/20/19 13:25
11/20/19 13:25
Client ID: MBBR Feed
Lab ID: CC17678-01RE3
Sampled: 11/19/19 10:00
Received: 11/20/19 09:45
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 310.2
NO PREP
12/03/19
12/02/19 14:08
12/02/19 14:08
Client ID: RO Feed
Lab ID: CC17678-02
Sampled: 11/19/19 10:00
Received: 11/20/19 09:45
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
CALC
[CALC]
12/17/19
12/05/19 09:20
12/10/19 18:12
EPA 300.0
NO PREP
12/17/19
11/27/19 15:34
11/28/19 05:11
EPA 310.2
NO PREP
12/03/19
11/22/19 13:48
11/22/19 17:12
EPA 335.4
Same
12/03/19
12/02/19 09:47
12/02/19 15:27
EPA 353.2
NO PREP
11/21/19 10:00
11/21/19 08:50
11/21/19 10:18
EPA 353.2
[CALC]
11/21/19 10:00
12/05/19 09:20
12/05/19 13:52
EPA 353.2
NO PREP
12/17/19
12/05/19 09:20
12/05/19 13:52
EPA 365.1
NO PREP
11/21/19 10:00
11/20/19 10:26
11/20/19 12:40
EPA 365.4
Same
12/17/19
11/25/19 10:48
12/10/19 15:55
EPA 6010D
EPA 3005A
05/17/20
11/22/19 10:47
12/04/19 11:35
EPA 7470A
EPA 7470A
12/17/19
11/21/19 10:04
11/25/19 15:10
SM 213OB-2011
NO PREP
11/21/19 10:00
11/21/19 08:32
11/21/19 08:32
SM 251OB-2011
NO PREP
12/17/19
11/25/19 11:30
11/25/19 11:30
SM 2540C-2011
NO PREP
11/26/19
11/23/19 16:21
11/23/19 16:21
SM 254OD-2011
NO PREP
11/26/19
11/25/19 13:08
11/25/19 13:08
SM 4500002 D-2011
NO PREP
08/14/22
12/04/19 15:28
12/04/19 15:28
SM 4500H+B-2011
NO PREP
11/19/19 10:14
11/26/19 14:47
11/26/19 14:47
SM 5220D-2011
Same
12/17/19
11/28/19 11:21
11/28/19 13:55
SM 531OB-2011
Same
12/17/19
11/22/19 09:00
11/22/19 10:37
Client ID: RO Feed
Lab ID: CC17678-02RE1
Sampled: 11/19/19 10:00
Received: 11/20/19 09:45
Parameter
Preparation
Hold Date/Time(sl
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 350.1
NO PREP
12/17/19
12/11/19 09:11
12/11/19 14:32
EPA 351.2
Same
12/17/19
11/25/19 10:48
12/10/19 18:12
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 28

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: RO Permeate
Lab ID: CC17678-03
Sampled: 11/19/19 10:00
Received: 11/20/19
09:45
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
CALC
[CALC]
12/17/19
12/05/19
09:20
12/06/19
18:48
EPA 300.0
NO PREP
12/17/19
12/02/19
19:08
12/02/19
19:08
EPA 310.2
NO PREP
12/03/19
11/22/19
13:48
11/22/19
17:13
EPA 335.4
Same
12/03/19
12/02/19
09:47
12/02/19
15:35
EPA 351.2
Same
12/17/19
11/25/19
10:48
12/06/19
18:48
EPA 353.2
NO PREP
11/21/19
10:00
11/21/19
08:50
11/21/19
09:54
EPA 353.2
[CALC]
11/21/19
10:00
12/05/19
09:20
12/05/19
16:30
EPA 365.1
NO PREP
11/21/19
10:00
11/20/19
10:26
11/20/19
12:21
EPA 365.4
Same
12/17/19
11/25/19
10:48
12/10/19
15:57
EPA 6010D
EPA 3005A
05/17/20
11/22/19
10:47
12/04/19
11:56
EPA 7470A
EPA 7470A
12/17/19
11/21/19
10:04
11/25/19
15:12
SM 213OB-2011
NO PREP
11/21/19
10:00
11/21/19
08:32
11/21/19
08:32
SM 251OB-2011
NO PREP
12/17/19
11/25/19
11:30
11/25/19
11:30
SM 254OC-2011
NO PREP
11/26/19
11/23/19
16:21
11/23/19
16:21
SM 2540D-2011
NO PREP
11/26/19
11/25/19
13:08
11/25/19
13:08
SM 4500002 D-2011
NO PREP
08/14/22
12/04/19
15:28
12/04/19
15:28
SM 4500H+B-2011
NO PREP
11/19/19
10:14
11/26/19
14:47
11/26/19
14:47
SM 5210 B-2011
NO PREP
11/21/19
10:00
11/20/19
13:25
11/20/19
13:25
SM 5220D-2011
Same
12/17/19
11/28/19
11:21
11/28/19
13:55
Client ID: RO Permeate
Lab ID: CC17678-03RE1
Sampled: 11/19/19 10:00
Received: 11/20/19
09:45
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 350.1
NO PREP
12/17/19
12/11/19
09:11
12/11/19
14:34
EPA 353.2
NO PREP
12/17/19
12/05/19
09:20
12/05/19
16:30
Client ID: RO Reject
Lab ID: CC17678-04
Sampled: 11/19/19 10:00
Received: 11/20/19
09:45
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
CALC
[CALC]
12/17/19
12/05/19
09:20
12/10/19
18:13
EPA 300.0
NO PREP
12/17/19
12/02/19
19:25
12/02/19
19:25
EPA 310.2
NO PREP
12/03/19
11/22/19
13:48
11/22/19
17:13
EPA 335.4
Same
12/03/19
12/02/19
09:47
12/02/19
15:41
EPA 353.2
NO PREP
11/21/19
10:00
11/21/19
08:50
11/21/19
10:36
EPA 353.2
[CALC]
11/21/19
10:00
12/05/19
09:20
12/05/19
16:32
EPA 365.1
NO PREP
11/21/19
10:00
11/20/19
10:26
11/20/19
12:43
EPA 365.4
Same
12/17/19
11/25/19
10:48
12/10/19
15:58
EPA 6010D
EPA 3005A
05/17/20
11/22/19
10:47
12/04/19
17:25
EPA 7470A
EPA 7470A
12/17/19
11/21/19
10:04
11/25/19
15:14
SM 213OB-2011
NO PREP
11/21/19
10:00
11/21/19
08:32
11/21/19
08:32
SM 251OB-2011
NO PREP
12/17/19
11/25/19
11:30
11/25/19
11:30
SM 2540C-2011
NO PREP
11/26/19
11/23/19
16:21
11/23/19
16:21
SM 254OD-2011
NO PREP
11/26/19
11/25/19
13:08
11/25/19
13:08
SM 4500002 D-2011
NO PREP
08/14/22
12/04/19
15:28
12/04/19
15:28
SM 4500H+B-2011
NO PREP
11/19/19
10:14
11/26/19
14:47
11/26/19
14:47
SM 5220D-2011
Same
12/17/19
11/28/19
11:21
11/28/19
13:55
Client ID: RO Reject
Lab ID: CC17678-04RE1
Sampled: 11/19/19 10:00
Received: 11/20/19
09:45
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 351.2
Same
12/17/19
11/25/19
10:48
12/10/19
18:13
EPA 353.2
NO PREP
12/17/19
12/05/19
09:20
12/05/19
16:32
EPA 6010D
EPA 3005A
05/17/20
11/22/19
10:47
12/04/19
11:58
Client ID: MBBR Feed
Lab ID: CC17678-05
Sampled: 11/19/19 10:00
Received: 11/20/19
09:45
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 6010D
EPA 3005A
05/17/20
11/22/19
10:47
12/04/19
12:01
FINAL
This report relates only to the sample
as received by the laboratory, and may only be reproduced in full.
Page 3 of 28

0Nk"q09
www.encolabs.com
SAMPLE DETECTION SUMMARY
Client ID: MBBR Feed
Lab ID:
CC17678-01
Analvte
Results
Flaa
MDL
POLL
Units
Method
Notes
Biochemical Oxygen Demand - Dissolved
80
2.0
2.0
mg/L
SM 5210 B-2011
Calcium - Dissolved
100
0.0390
0.100
mg/L
EPA 6010D
Magnesium - Dissolved
6320
29.0
100
ug/L
EPA 6010D
Silica (Si02) - Dissolved
17.5
0.03
0.2
mg/L
EPA 6010D
Client ID: MBBR Feed
Lab ID:
CC17678-01RE3
Anal a
Results
Flaa
MDL
Q
Units
Method
Notes
Total Alkalinity as CaCO3
1600
D
140
150
mg/L
EPA 310.2
Client ID: RO Feed
Lab ID:
CC17678-02
Anal a
Results
Flaa
MDL
Q
Units
Method
Notes
Bicarbonate (as CaCO3)
1300
14
15
mg/L
SM 45000O2 D-2011
Boron - Total
0.0423
J
0.00570
0.0500
mg/L
EPA 6010D
Calcium - Total
87.9
B
0.0390
0.100
mg/L
EPA 6010D
Carbonate (as CaCO3)
30
14
15
mg/L
SM 45000O2 D-2011
Chemical Oxygen Demand
120
10
10
mg/L
SM 5220D-2011
Chloride
360
D
22
50
mg/L
EPA 300.0
Copper - Total
0.00379
J
0.00160
0.0100
mg/L
EPA 6010D
Cyanide (total)
0.0051
0.0049
0.0050
mg/L
EPA 335.4
Iron - Total
0.0513
0.0220
0.0500
mg/L
EPA 6010D
Magnesium - Total
5.00
B
0.0290
0.100
mg/L
EPA 6010D
Nickel - Total
0.00220
J
0.00220
0.0100
mg/L
EPA 6010D
Nitrate as N
17
D
2.0
4.8
mg/L
EPA 353.2
Nitrate/Nitrite as N
21
D
2.0
4.8
mg/L
EPA 353.2
Nitrite as N
3.6
D
0.084
0.50
mg/L
EPA 353.2
Q-01
Orthophosphate as P
9.1
BD
0.80
2.5
mg/L
EPA 365.1
PH
8.4
1.0
1.0
pH
SM 4500H+B-2011
Q-01
Phosphorus
12
D
0.12
0.50
mg/L
EPA 365.4
Potassium - Total
505
0.150
0.500
mg/L
EPA 6010D
Silica (Si02) - Total
18.7
0.03
0.2
mg/L
EPA 6010D
Sodium - Total
485
0.400
0.500
mg/L
EPA 6010D
Specific Conductance (EC) at 25 Deg C
3800
1.0
1.0
umhos/cm
SM 251OB-2011
Sulfate as SO4
91
D
29
50
mg/L
EPA 300.0
Temperature for pH (deg. C)
15
pH
SM 4500H+B-2011
Q-01
Total Alkalinity as CaCO3
1300
D
140
150
mg/L
EPA 310.2
Total Dissolved Solids
2300
50
50
mg/L
SM 2540C-2011
Total Nitrogen
52
D
2.0
4.8
mg/L
CALC
Total Organic Carbon
33
0.34
1.0
mg/L
SM 531OB-2011
Total Suspended Solids
2.5
2.5
2.5
mg/L
SM 2540D-2011
Turbidity
4.0
0.50
1.0
NTU
SM 213OB-2011
Zinc - Total
0.00721
J
0.00440
0.0100
mg/L
EPA 6010D
Client ID: RO Feed
Lab ID:
CC17678-02RE1
Analvte
Results Flaa MDL
PQL
Units Method Notes
Ammonia as N
18 D 0.45
1.0
mg/L EPA 350.1
Total Kjeldahl Nitrogen
31 D 0.52
0.96
mg/L EPA 351.2
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 28

0Nk"q09
www.encolabs.com
SAMPLE DETECTION SUMMARY
Client ID: RO Permeate
Lab ID: CC17678-03
Analvte
Results
Flaa
MDL
Q
Units
Method
Notes
Bicarbonate (as CaCO3)
20
14
15
mg/L
SM 4500002 D-2011
Boron - Total
0.0182
J
0.00570
0.0500
mg/L
EPA 6010D
Cadmium - Total
0.000469
J
0.000360
0.00100
mg/L
EPA 6010D
Calcium - Total
0.168
B
0.0390
0.100
mg/L
EPA 6010D
Chloride
4.4
J
2.2
5.0
mg/L
EPA 300.0
Nitrate as N
0.086
J
0.041
0.10
mg/L
EPA 353.2
Nitrite as N
0.28
0.017
0.10
mg/L
EPA 353.2
Orthophosphate as P
0.23
JB
0.16
0.50
mg/L
EPA 365.1
PH
5.6
1.0
1.0
pH
SM 4500H+B-2011
Q-01
Phosphorus
0.11
0.025
0.10
mg/L
EPA 365.4
Potassium - Total
10.1
0.150
0.500
mg/L
EPA 6010D
Silica (Si02) - Total
0.09
J
0.03
0.2
mg/L
EPA 6010D
Sodium - Total
4.88
0.400
0.500
mg/L
EPA 6010D
Specific Conductance (EC) at 25 Deg C
72
1.0
1.0
umhos/cm
SM 251OB-2011
Temperature for pH (deg. C)
15
pH
SM 4500H+B-2011
Q-01
Total Alkalinity as CaCO3
20
14
15
mg/L
EPA 310.2
Total Kjeldahl Nitrogen
2.2
0.26
0.48
mg/L
EPA 351.2
Total Nitrogen
2.6
0.26
0.48
mg/L
CALC
Client ID: RO Permeate
Lab ID: CC17678-03RE3
Anal a
Results
Flaa
MDL
Q
Units
Method
Notes
Ammonia as N
2.2
D
0.090
0.20
mg/L
EPA 350.1
Nitrate/Nitrite as N
0.37
0.041
0.10
mg/L
EPA 353.2
I Client ID: RO Reject Lab ID: CC17678-04
Analvte
Results
Flaa
MDL
Q
Units
Method
Notes
Aluminum - Total
0.351
0.0420
0.100
mg/L
EPA 6010D
Bicarbonate (as CaCO3)
2100
14
15
mg/L
SM 4500002 D-2011
Boron - Total
0.164
0.00570
0.0500
mg/L
EPA 6010D
Chemical Oxygen Demand
800
20
20
mg/L
SM 5220D-2011
Chloride
1700
D
220
500
mg/L
EPA 300.0
Chromium - Total
0.00978
J
0.00140
0.0100
mg/L
EPA 6010D
Copper - Total
0.0165
0.00160
0.0100
mg/L
EPA 6010D
Cyanide (total)
0.021
0.0049
0.0050
mg/L
EPA 335.4
Iron - Total
0.447
0.0220
0.0500
mg/L
EPA 6010D
Magnesium - Total
30.1
B
0.0290
0.100
mg/L
EPA 6010D
Molybdenum - Total
0.00576
J
0.00250
0.0100
mg/L
EPA 6010D
Nickel - Total
0.0118
0.00220
0.0100
mg/L
EPA 6010D
Nitrate as N
12
D
0.82
2.7
mg/L
EPA 353.2
Nitrite as N
19
D
0.45
2.7
mg/L
EPA 353.2
Q-01
Orthophosphate as P
50
BD
0.80
2.5
mg/L
EPA 365.1
PH
7.1
1.0
1.0
pH
SM 4500H+B-2011
Q-01
Phosphorus
78
D
1.2
5.0
mg/L
EPA 365.4
Silica (Si02) - Total
118
0.03
0.2
mg/L
EPA 6010D
Specific Conductance (EC) at 25 Deg C
20000
1.0
1.0
umhos/cm
SM 251OB-2011
Sulfate as SO4
4900
D
290
500
mg/L
EPA 300.0
Temperature for pH (deg. C)
16
pH
SM 4500H+B-2011
Q-01
Total Alkalinity as CaCO3
2100
D
280
300
mg/L
EPA 310.2
Total Dissolved Solids
16000
500
500
mg/L
SM 2540C-2011
Total Nitrogen
170
D
5.2
9.6
mg/L
CALC
Turbidity
4.3
0.50
1.0
NTU
SM 213OB-2011
Zinc - Total
0.0238
0.00440
0.0100
mg/L
EPA 6010D
Client ID: RO Reject
Lab ID:
CC17678-04RE3
Analvte
Results
Flaa
MDL
Q
Units
Method
Notes
Calcium - Total
567
BD
0.390
1.00
mg/L
EPA 6010D
Nitrate/Nitrite as N
31
D
0.82
2.0
mg/L
EPA 353.2
Potassium - Total
3000
D
1.50
5.00
mg/L
EPA 6010D
Sodium - Total
2920
D
4.00
5.00
mg/L
EPA 6010D
Total Kjeldahl Nitrogen
140
D
5.2
9.6
mg/L
EPA 351.2
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 28

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SAMPLE DETECTION SUMMARY
Client ID: MBBR Feed Lab ID: CC17678-05
Anala Results Flaa MDL POLL Units Method Notes
Silica (Si02) - Total 26.7 0.03 0.2 mg/L EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 28

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: MBBR Feed Lab Sample ID:CC17678-01 Received: 11/20/19 09:45
Matrix: Waste Water Sampled:11/19/19 10:00 Work Order: CC17678
Project: RO Pilot Sampled By:Jelena El Barigi
Metals (Dissolved) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flao
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Calcium [7440-70-2]^ 100
mg/L
1
0.0390
0.100
91<22025
EPA 6010D
12/04/19 11:32
JDH
Magnesium [7439-95-4]^ 6320
ug/L
1
29.0
100
91<22025
EPA 6010D
12/04/19 11:32
JDH
Silica (Si02) [763-18-69]^ 17.5
mg/L
1
0.03
0.2
91<22025
EPA 6010D
12/04/19 11:32
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flao
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Total Alkalinity as CaCO3 [471-34-1]^ 1600 D
mg/L
10
140
150
9LO2010
EPA 310.2
12/02/19 14:08
AKF
Classical Chemistry Parameters (Dissolved)
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flao
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Biochemical Oxygen Demand^ 80
mg/L
1
2.0
2.0
91<20026
SM 5210 B-2011
11/20/19 13:25
JOC
Description: RO Feed Lab Sample ID:CC17678-02 Received: 11/20/19 09:45
Matrix: Waste Water Sampled:11/19/19 10:00 Work Order: CC17678
Project: RO Pilot Sampled By:Jelena El Barigi
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Mercury [7439-97-6]^
0.000150
U
mg/L
1
0.000150
0.000200
91<21014
EPA 7470A
11/25/19 15:10
KAH
Silica (Si02) [763-18-69]^
18.7
mg/L
1
0.03
0.2
91<22025
EPA 6010D
12/04/19 11:35
JDH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Aluminum [7429-90-5]^
0.0420
U
mg/L
1
0.0420
0.100
91<22025
EPA 6010D
12/04/19 11:35
JDH
Arsenic[7440-38-2]^
0.00760
U
mg/L
1
0.00760
0.0100
91<22025
EPA 6010D
12/04/19 11:35
JDH
Boron [7440-42-8]^
0.0423
J
mg/L
1
0.00570
0.0500
91<22025
EPA 6010D
12/04/19 11:35
JDH
Cadmium [7440-43-9]^
0.000360
U
mg/L
1
0.000360
0.00100
91<22025
EPA 6010D
12/04/19 11:35
JDH
Calcium [7440-70-2]^
87.9
B
mg/L
1
0.0390
0.100
91<22025
EPA 6010D
12/04/19 11:35
JDH
Chromium [7440-47-3]^
0.00140
U
mg/L
1
0.00140
0.0100
91<22025
EPA 6010D
12/04/19 11:35
JDH
Copper[7440-50-8]^
0.00379
J
mg/L
1
0.00160
0.0100
91<22025
EPA 6010D
12/04/19 11:35
JDH
Iron [7439-89-6]^
0.0513
mg/L
1
0.0220
0.0500
91<22025
EPA 6010D
12/04/19 11:35
JDH
Lead [7439-92-1]^
0.00310
U
mg/L
1
0.00310
0.0100
91<22025
EPA 6010D
12/04/19 11:35
JDH
Magnesium [7439-95-4]^
5.00
B
mg/L
1
0.0290
0.100
91<22025
EPA 6010D
12/04/19 11:35
JDH
Molybdenum [7439-98-7]^
0.00250
U
mg/L
1
0.00250
0.0100
91<22025
EPA 6010D
12/04/19 11:35
JDH
Nickel[7440-02-O]^
0.00220
J
mg/L
1
0.00220
0.0100
91<22025
EPA 6010D
12/04/19 11:35
JDH
Potassium [7440-09-7]^
505
mg/L
1
0.150
0.500
91<22025
EPA 6010D
12/04/19 11:35
JDH
Selenium [7782-49-2]^
0.00620
U
mg/L
1
0.00620
0.0100
91<22025
EPA 6010D
12/04/19 11:35
JDH
Silver[7440-22-4]^
0.00190
U
mg/L
1
0.00190
0.0100
91<22025
EPA 6010D
12/04/19 11:35
JDH
Sodium [7440-23-5]^
485
mg/L
1
0.400
0.500
91<22025
EPA 6010D
12/04/19 11:35
JDH
Zinc[7440-66-6]^
0.00721
J
mg/L
1
0.00440
0.0100
91<22025
EPA 6010D
12/04/19 11:35
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Ammonia as N [7664-41-7]^
18
D
mg/L
10
0.45
1.0
91-11013
EPA 350.1
12/11/19 14:32
AKF
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 28

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: RO Feed Lab Sample ID:CC17678-02 Received: 11/20/19 09:45
Matrix: Waste Water Sampled:11/19/19 10:00 Work Order: CC17678
Project: RO Pilot Sampled By:Jelena El Barigi
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results
Flao
Units
DF
MDL
P L
Batch
Method
Analyzed
By
Notes
Bicarbonate (as CaCO3)[71-52-3]
1300
mg/L
1
14
15
9LO4049
M 4500002 D-201
12/04/19 15:28
JAH
Carbonate (as CaCO3)[3812-32-6]
30
mg/L
1
14
15
9LO4049
M 4500002 D-201
12/04/19 15:28
JAH
Chemical Oxygen Demand^
120
mg/L
1
10
10
91<28001
SM 5220D-2011
11/28/19 13:55
JOC
Chloride [16887-00-6]^
360
D
mg/L
10
22
50
91<27025
EPA 300.0
11/28/19 05:11
PDK
Cyanide (total)[57-12-5]^
0.0051
mg/L
1
0.0049
0.0050
9LO2005
EPA 335.4
12/02/19 15:27
AKF
Nitrate as N [14797-55-8]
17
D
mg/L
48
2.0
4.8
[CALC]
EPA 353.2
12/05/19 13:52
AKF
Nitrate/Nitrite as IN
21
D
mg/L
48
2.0
4.8
9LO5016
EPA 353.2
12/05/19 13:52
AKF
Nitrite as N [14797-65-0]^
3.6
D
mg/L
5
0.084
0.50
91<21007
EPA 353.2
11/21/19 10:18
AKF
Q-01
Orthophosphate as P [1426-54-42]^
9.1
BD
mg/L
5
0.80
2.5
91<20024
EPA 365.1
11/20/19 12:40
AKF
pH
8.4
pH
1
1.0
1.0
91<26027
iM 4500H+B-2011
11/26/19 14:47
BDC
Q-01
Phosphorus[7723-14-O]^
12
D
mg/L
5
0.12
0.50
91<25013
EPA 365.4
12/10/19 15:55
AKF
Specific Conductance (EC) at 25 Deg
3800
umhos/cm
1
1.0
1.0
91<25014
SM 251OB-2011
11/25/19 11:30
JOC
C^
Sulfate as SO4 [14808-79-8]^
91
D
mg/L
10
29
50
91<27025
EPA 300.0
11/28/19 05:11
PDK
Temperature for pH (deg. C)
15
pH
1
91<26027
iM 4500H+B-2011
11/26/19 14:47
BDC
Q-01
Total Alkalinity as CaCO3 [471-34-1]^
1300
D
mg/L
10
140
150
91<22033
EPA 310.2
11/22/19 17:12
AKF
Total Dissolved Solids^
2300
mg/L
1
50
50
91<22007
SM 2540C-2011
11/23/19 16:21
JOC
Total Kjeldahl Nitrogen
31
D
mg/L
2
0.52
0.96
91<25012
EPA 351.2
12/10/19 18:12
AKF
Total Nitrogen [17778-88-0]
52
D
mg/L
48
2.0
4.8
[CALC]
CALC
12/10/19 18:12
AKF
Total Suspended Solids^
2.5
mg/L
1
2.5
2.5
91<25035
SM 2540D-2011
11/25/19 13:08
JAH
Turbidity^
4.0
NTU
1
0.50
1.0
91<21004
SM 213OB-2011
11/21/19 08:32
JOC
Classical Chemistry Parameters
^ - ENCO Orlando certified analyte [NC 424]
Analyte fCAS Numberl Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
Total Organic Carbon^
33
mg/L
1
0.34
1.0
91<22006
SM 531OB-2011
11/22/19 10:37
JSS
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 28

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ANALYTICAL RESULTS
Description: RO Permeate Lab Sample ID:CC17678-03 Received: 11/20/19 09:45
Matrix: Waste Water Sampled:11/19/19 10:00 Work Order: CC17678
Project: RO Pilot Sampled By:Jelena El Barigi
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flao
Units
DF
MDL
P L
Batch
Method
Analyzed
-By Notes
Mercury [7439-97-6]^
0.000150
U
mg/L
1
0.000150
0.000200
91<21014
EPA 7470A
11/25/19 15:12
KAH
Silica (Si02) [763-18-69]A
0.09
J
mg/L
1
0.03
0.2
91<22025
EPA 6010D
12/04/19 11:56
JDH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flao
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Aluminum [7429-90-5]^
0.0420
U
mg/L
1
0.0420
0.100
91<22025
EPA 6010D
12/04/19 11:56
JDH
Arsenic[7440-38-2]^
0.00760
U
mg/L
1
0.00760
0.0100
91<22025
EPA 6010D
12/04/19 11:56
JDH
Boron [7440-42-8]A
0.0182
J
mg/L
1
0.00570
0.0500
91<22025
EPA 6010D
12/04/19 11:56
JDH
Cadmium [7440-43-9]A
0.000469
J
mg/L
1
0.000360
0.00100
91<22025
EPA 6010D
12/04/19 11:56
JDH
Calcium [7440-70-2]A
0.168
B
mg/L
1
0.0390
0.100
91<22025
EPA 6010D
12/04/19 11:56
JDH
Chromium [7440-47-3]^
0.00140
U
mg/L
1
0.00140
0.0100
91<22025
EPA 6010D
12/04/19 11:56
JDH
Copper[7440-50-8]^
0.00160
U
mg/L
1
0.00160
0.0100
91<22025
EPA 6010D
12/04/19 11:56
JDH
Iron [7439-89-6]^
0.0220
U
mg/L
1
0.0220
0.0500
91<22025
EPA 6010D
12/04/19 11:56
JDH
Lead [7439-92-1]^
0.00310
U
mg/L
1
0.00310
0.0100
91<22025
EPA 6010D
12/04/19 11:56
JDH
Magnesium [7439-95-4]^
0.0290
U
mg/L
1
0.0290
0.100
91<22025
EPA 6010D
12/04/19 11:56
JDH
Molybdenum [7439-98-7]^
0.00250
U
mg/L
1
0.00250
0.0100
91<22025
EPA 6010D
12/04/19 11:56
JDH
Nickel[7440-02-0]^
0.00220
U
mg/L
1
0.00220
0.0100
91<22025
EPA 6010D
12/04/19 11:56
JDH
Potassium [7440-09-7]A
10.1
mg/L
1
0.150
0.500
91<22025
EPA 6010D
12/04/19 11:56
JDH
Selenium [7782-49-2]^
0.00620
U
mg/L
1
0.00620
0.0100
91<22025
EPA 6010D
12/04/19 11:56
JDH
Silver[7440-22-4]^
0.00190
U
mg/L
1
0.00190
0.0100
91<22025
EPA 6010D
12/04/19 11:56
JDH
Sodium [7440-23-5]A
4.88
mg/L
1
0.400
0.500
91<22025
EPA 6010D
12/04/19 11:56
JDH
Zinc[7440-66-6]^
0.00440
U
mg/L
1
0.00440
0.0100
91<22025
EPA 6010D
12/04/19 11:56
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flao
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Ammonia as N [7664-41-7]A
2.2
D
mg/L
2
0.090
0.20
91-11013
EPA 350.1
12/11/19 14:34
AKF
Bicarbonate (as CaCO3)[71-52-3]
20
mg/L
1
14
15
9LO4049
M 4500002 D-201
12/04/19 15:28
JAH
Carbonate (as CaCO3)[3812-32-6]
14
U
mg/L
1
14
15
9LO4049
M 4500002 D-201
12/04/19 15:28
JAH
Chemical Oxygen Demand^
10
U
mg/L
1
10
10
91<28001
SM 5220D-2011
11/28/19 13:55
JOC
Chloride [ 16887-00-6] A
4.4
J
mg/L
1
2.2
5.0
9LO2037
EPA 300.0
12/02/19 19:08
PDK
Cyanide (total) [57-12-5]^
0.0049
U
mg/L
1
0.0049
0.0050
9LO2005
EPA 335.4
12/02/19 15:35
AKF
Nitrate as N [14797-55-8]
0.086
J
mg/L
1
0.041
0.10
[CALC]
EPA 353.2
12/05/19 16:30
AKF
Nitrate/Nitrite as NA
0.37
mg/L
1
0.041
0.10
9LO5016
EPA 353.2
12/05/19 16:30
AKF
Nitrite as N [ 14797-65-0] A
0.28
mg/L
1
0.017
0.10
91<21007
EPA 353.2
11/21/19 09:54
AKF
Orthophosphate as P [1426-54-42]A
0.23
JB
mg/L
1
0.16
0.50
91<20024
EPA 365.1
11/20/19 12:21
AKF
pH
5.6
pH
1
1.0
1.0
91<26027
iM 4500H+B-2011
11/26/19 14:47
BDC Q-01
Phosphorus[7723-14-O]A
0.11
mg/L
1
0.025
0.10
91<25013
EPA 365.4
12/10/19 15:57
AKF
Specific Conductance (EC) at 25 Deg
72
umhos/cm
1
1.0
1.0
91<25014
SM 251OB-2011
11/25/19 11:30
JOC
CA
Sulfate as SO4 [14808-79-8]^
2.9
U
mg/L
1
2.9
5.0
9LO2037
EPA 300.0
12/02/19 19:08
PDK
Temperature for pH (deg. C)
15
pH
1
91K26027
iM 450011+13-2011
11/26/19 14:47
BDC Q-01
Total Alkalinity as CaCO3 [471-34-1]A
20
mg/L
1
14
15
91K22033
EPA 310.2
11/22/19 17:13
AKF
Total Dissolved Solids^
50
U
mg/L
1
50
50
91<22007
SM 2540C-2011
11/23/19 16:21
JOC
Total Kjeldahl Nitrogen
2.2
mg/L
1
0.26
0.48
9K25012
EPA 351.2
12/06/19 18:48
AKF
Total Nitrogen [17778-88-0]
2.6
mg/L
1
0.26
0.48
[CALC]
CALC
12/06/19 18:48
AKF
Total Suspended Solids^
2.5
U
mg/L
1
2.5
2.5
91<25035
SM 2540D-2011
11/25/19 13:08
JAH
FINAL
This report relates only
to the
sample as received by the laboratory,
and may only be reproduced
in full.
Page 9 of 28

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: RO Permeate Lab Sample ID:CC17678-03 Received: 11/20/19 09:45
Matrix: Waste Water Sampled:11/19/19 10:00 Work Order: CC17678
Project: RO Pilot Sampled By:Jelena El Barigi
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
TurbidityA 0.50 U
NTU
1
0.50
1.0
91<21004
SM 213OB-2011
11/21/19 08:32
JOC
Classical Chemistry Parameters (Dissolved)
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Biochemical Oxygen DemandA 2.0 U
mg/L
1
2.0
2.0
91<20026
SM 5210 B-2011
11/20/19 13:25
JOC
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 28

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ANALYTICAL RESULTS
Description: RO Reject Lab Sample ID:CC17678-04 Received: 11/20/19 09:45
Matrix: Waste Water Sampled:11/19/19 10:00 Work Order: CC17678
Project: RO Pilot Sampled By:Jelena El Barigi
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary cediFed analyte [NC 591]
Analyte rCAS Numberl Results Flao Units DF MDL P L Batch Method Analyzed -By Notes
Mercury [7439-97-6]^ 0.000150 U mg/L 1 0.000150 0.000200 91<21014 EPA 7470A 11/25/19 15:14 KAH
Silica (Si02) [763-18-69]^ 118 mg/L 1 0.03 0.2 91<22025 EPA 6010D 12/04/19 17:25 JDH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flao
Units
DF
MDL
P L
Batch
Method
Analyzed
By
Notes
Aluminum [7429-90-5]^
0.351
mg/L
1
0.0420
0.100
91<22025
EPA 6010D
12/04/19 17:25
JDH
Arsenic[7440-38-2]^
0.00760
U
mg/L
1
0.00760
0.0100
91<22025
EPA 6010D
12/04/19 17:25
JDH
Boron [7440-42-8]^
0.164
mg/L
1
0.00570
0.0500
91<22025
EPA 6010D
12/04/19 17:25
JDH
Cadmium [7440-43-9]^
0.000360
U
mg/L
1
0.000360
0.00100
91<22025
EPA 6010D
12/04/19 17:25
JDH
Calcium [7440-70-2]^
567
BD
mg/L
10
0.390
1.00
91<22025
EPA 6010D
12/04/19 11:58
JDH
Chromium [7440-47-3]^
0.00978
J
mg/L
1
0.00140
0.0100
91<22025
EPA 6010D
12/04/19 17:25
JDH
Copper[7440-50-8]^
0.0165
mg/L
1
0.00160
0.0100
91<22025
EPA 6010D
12/04/19 17:25
JDH
Iron [7439-89-6]^
0.447
mg/L
1
0.0220
0.0500
91<22025
EPA 6010D
12/04/19 17:25
JDH
Lead [7439-92-1]^
0.00310
U
mg/L
1
0.00310
0.0100
91<22025
EPA 6010D
12/04/19 17:25
JDH
Magnesium [7439-95-4]^
30.1
B
mg/L
1
0.0290
0.100
91<22025
EPA 6010D
12/04/19 17:25
JDH
Molybdenum [7439-98-7]^
0.00576
J
mg/L
1
0.00250
0.0100
91<22025
EPA 6010D
12/04/19 17:25
JDH
Nickel[7440-02-O]^
0.0118
mg/L
1
0.00220
0.0100
91<22025
EPA 6010D
12/04/19 17:25
JDH
Potassium [7440-09-7]^
3000
D
mg/L
10
1.50
5.00
91<22025
EPA 6010D
12/04/19 11:58
JDH
Selenium [7782-49-2]^
0.00620
U
mg/L
1
0.00620
0.0100
91<22025
EPA 6010D
12/04/19 17:25
JDH
Silver[7440-22-4]^
0.00190
U
mg/L
1
0.00190
0.0100
91<22025
EPA 6010D
12/04/19 17:25
JDH
Sodium [7440-23-5]^
2920
D
mg/L
10
4.00
5.00
91<22025
EPA 6010D
12/04/19 11:58
JDH
Zinc[7440-66-6]^
0.0238
mg/L
1
0.00440
0.0100
91<22025
EPA 6010D
12/04/19 17:25
JDH
Classical Chemistry Parameters
^ - ENCO Cary cediFed analyte [NC 591]
Analyte rCAS Numberl
Results
Flao
Units
DF
MDL
P L
Batch
Method
Analyzed
-By
Notes
Bicarbonate (as CaCO3)[71-52-3]
2100
mg/L
1
14
15
9LO4049
M 4500002 D-201
12/04/19 15:28
JAH
Carbonate (as CaCO3)[3812-32-6]
14
U
mg/L
1
14
15
9LO4049
M 4500002 D-201
12/04/19 15:28
JAH
Chemical Oxygen Demand
800
mg/L
2
20
20
91<28001
SM 5220D-2011
11/28/19 13:55
JOC
Chloride [16887-00-6]^
1700
D
mg/L
100
220
500
9LO2037
EPA 300.0
12/02/19 19:25
PDK
Cyanide (total)[57-12-5]^
0.021
mg/L
1
0.0049
0.0050
9LO2005
EPA 335.4
12/02/19 15:41
AKF
Nitrate as N [14797-55-8]
12
D
mg/L
27
0.82
2.7
[CALC]
EPA 353.2
12/05/19 16:32
AKF
Nitrate/Nitrite as N^
31
D
mg/L
20
0.82
2.0
9LO5016
EPA 353.2
12/05/19 16:32
AKF
Nitrite as N [14797-65-0]^
19
D
mg/L
26.67
0.45
2.7
91<21007
EPA 353.2
11/21/19 10:36
AKF
Q-01
Orthophosphate as P [1426-54-42]^
50
BD
mg/L
5
0.80
2.5
91<20024
EPA 365.1
11/20/19 12:43
AKF
pH
7.1
pH
1
1.0
1.0
91<26027
iM 4500H+B-2011
11/26/19 14:47
BDC
Q-01
Phosphorus[7723-14-0]^
78
D
mg/L
50
1.2
5.0
91<25013
EPA 365.4
12/10/19 15:58
AKF
Specific Conductance (EC) at 25 Deg
20000
umhos/cm
1
1.0
1.0
91<25014
SM 251OB-2011
11/25/19 11:30
JOC
C^
Sulfate as SO4 [14808-79-8]^
4900
D
mg/L
100
290
500
9LO2037
EPA 300.0
12/02/19 19:25
PDK
Temperature for pH (deg. C)
16
pH
1
9K26027
iM 450011+13-2011
11/26/19 14:47
BDC
Q-01
Total Alkalinity as CaCO3 [471-34-1]^
2100
D
mg/L
20
280
300
9K22033
EPA 310.2
11/22/19 17:13
AKF
Total Dissolved Solids^
16000
mg/L
10
500
500
9K22007
SM 2540C-2011
11/23/19 16:21
JOC
Total Kjeldahl Nitrogen
140
D
mg/L
20
5.2
9.6
9K25012
EPA 351.2
12/10/19 18:13
AKF
Total Nitrogen [17778-88-0]
170
D
mg/L
20
5.2
9.6
[CALC]
CALC
12/10/19 18:13
AKF
Total Suspended Solids^
2.5
U
mg/L
1
2.5
2.5
91<25035
SM 2540D-2011
11/25/19 13:08
JAH
Turbidity^
4.3
NTU
1
0.50
1.0
9K21004
SM 213OB-2011
11/21/19 08:32
JOC
FINAL
This report relates only
to the sample as received by the laboratory,
and may only
be reproduced
in full.
Page 11 of 28

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ANALYTICAL RESULTS
Description: MBBR Feed Lab Sample ID:CC17678-05 Received: 11/20/19 09:45
Matrix: Waste Water Sampled:11/19/19 10:00 Work Order: CC17678
Project: RO Pilot Sampled By:Jelena El Barigi
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed I;Y Notes
Silica (Si02) [763-18-69]A 26.7 mg/L 1 0.03 0.2 91<22025 EPA 6010D 12/04/19 12:01 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 28

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 9K21014 - EPA 7470A
Blank (9K23014-BLKI)
Prepared: 11/21/2019 10:04 Analyzed: 11/25/2019 14:44
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Mercury
0.000150
U
0.000200
mg/L
Blank (9K23014-BLK2)
Prepared: 11/21/2019 10:04 Analyzed: 11/25/2019 14:46
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Mercury
0.00300
U
0.00400
mg/L
LCS (9K21014-BS3)
Prepared: 11/21/2019 10:04 Analyzed: 11/25/2019 14:49
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Mercury
0.00479
0.000200
mg/L
0.00500 96 80-120
Matrix Spike (9K21014-MS3)
Prepared: 11/21/2019 10:04 Analyzed: 11/25/2019 14:54
Source: CC17854-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Mercury
0.00446
0.000200
mg/L
0.00500 0.000150 U 89 75-125
Matrix Spike Dup (9K23014-MSD3)
Prepared: 11/21/2019 10:04 Analyzed: 11/25/2019 14:56
Source: CC17854-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Mercury
0.00423
0.000200
mg/L
0.00500 0.000150 U 85 75-125 5
25
Post Spike (9K21014-PS1)
Prepared: 11/21/2019 10:04 Analyzed: 11/25/2019 14:59
Source: CC17854-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Mercury
4.67
0.200
ug/L
5.00 0.00700 93 75-125
Batch 9K22025 - EPA 3005A
Blank (9K22025-BLK1) Prepared: 11/22/2019 10:47 Analyzed: 12/04/2019 10:58
Spike Source %REC RPD
Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes
Silica (Si02) 0.03 U 0.2 mg/L
Blank (9K22025-BLK2) Prepared: 11/22/2019 10:47 Analyzed: 12/04/2019 11:11
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Silica (Si02) 0.03 U 0.2 mg/L
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 9K22025 - EPA 3005A
Blank (9K22025-BLKS) Prepared: 11/22/2019 10:47 Analyzed: 12/04/2019 10:58
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Aluminum 0.0425 3 0.100 mg/L
Arsenic 0.00760 U 0.0100 mg/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 28

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www.encolabs.com
QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 9K22025 - EPA 3005A - Continued
Blank (9K22025-BLKI) Continued Prepared: 11/22/2019 10:47 Analyzed: 12/04/2019 10:58
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Boron
0.00570
U
0.0500
mg/L
Cadmium
0.00044
3
0.00100
mg/L
7
Calcium
0.0449
1
0.100
mg/L
Chromium
0.00140
U
0.0100
mg/L
Copper
0.00160
U
0.0100
mg/L
Iron
0.0220
U
0.0500
mg/L
Lead
0.00310
U
0.0100
mg/L
Magnesium
0.0349
1
0.100
mg/L
Molybdenum
0.00250
U
0.0100
mg/L
Nickel
0.00220
U
0.0100
mg/L
Potassium
0.150
U
0.500
mg/L
Selenium
0.00620
U
0.0100
mg/L
Silver
0.00190
U
0.0100
mg/L
Sodium
0.400
U
0.500
mg/L
Zinc
0.00440
U
0.0100
mg/L
Blank (9K22025-BLK2)
Prepared: 11/22/2019 10:47 Analyzed: 12/04/2019 11:11
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Aluminum
0.0445
3
0.100
mg/L
Arsenic
0.00760
U
0.0100
mg/L
Boron
0.00570
U
0.0500
mg/L
Cadmium
0.000360
U
0.00100
mg/L
Calcium
0.0390
U
0.100
mg/L
Chromium
0.00140
U
0.0100
mg/L
Copper
0.00160
U
0.0100
mg/L
Iron
0.0220
U
0.0500
mg/L
Lead
0.00310
U
0.0100
mg/L
Magnesium
0.0326
3
0.100
mg/L
Molybdenum
0.00250
U
0.0100
mg/L
Nickel
0.00220
U
0.0100
mg/L
Potassium
0.150
U
0.500
mg/L
Selenium
0.00620
U
0.0100
mg/L
Silver
0.00190
U
0.0100
mg/L
Sodium
0.400
U
0.500
mg/L
Zinc
0.00440
U
0.0100
mg/L
LCS (9K22025-BS1)
Prepared: 11/22/2019 10:47 Analyzed: 12/04/2019 11:17
Spike
Source
%REC RPD
Analvte
Result
Flaq POL
Units
Level
Result %REC
Limits RPD Limit Notes
Aluminum
2.01
0.100
mg/L
2.00
101
80-120
Arsenic
0.189
0.0100
mg/L
0.200
94
80-120
Boron
0.957
0.0500
mg/L
1.00
96
80-120
Cadmium
0.0188
0.00100
mg/L
0.0200
94
80-120
Calcium
2.13
B 0.100
mg/L
2.00
106
80-120
Chromium
0.191
0.0100
mg/L
0.200
96
80-120
Copper
0.188
0.0100
mg/L
0.200
94
80-120
Iron
0.991
0.0500
mg/L
1.00
99
80-120
FINAL
This report relates only to the sample as received by the
laboratory, and
may only be reproduced in
full. Page 14 of 28

(� �Eo
www.encolabs.com
QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 9K22025 - EPA 3005A - Continued
LCS (9K22025-BS3) Continued Prepared: 11/22/2019 10:47 Analyzed: 12/04/2019 11:17
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Lead
0.187
0.0100
mg/L
0.200
94
80-120
Magnesium
1.98
B
0.100
mg/L
2.00
99
80-120
Molybdenum
0.184
0.0100
mg/L
0.200
92
80-120
Nickel
0.190
0.0100
mg/L
0.200
95
80-120
Potassium
9.92
0.500
mg/L
10.0
99
80-120
Selenium
0.193
0.0100
mg/L
0.200
96
80-120
Silver
0.196
0.0100
mg/L
0.200
98
80-120
Sodium
9.77
0.500
mg/L
10.0
98
80-120
Zinc
0.193
0.0100
mg/L
0.200
96
80-120
Matrix Spike (9K22025-MS1)
Prepared:
11/22/2019
10:47 Analyzed: 12/04/2019 11:22
Source: CC17854-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Aluminum
2.06
0.100
mg/L
2.00
0.118
97
75-125
Arsenic
0.174
0.0100
mg/L
0.200
0.00760 U
87
75-125
Boron
1.01
0.0500
mg/L
1.00
0.0255
98
75-125
Cadmium
0.0186
0.00100
mg/L
0.0200
0.000360 U
93
75-125
Calcium
74.4
B
0.100
mg/L
2.00
154
NR
75-125
QM-07
Chromium
0.189
0.0100
mg/L
0.200
0.00159
94
75-125
Copper
0.228
0.0100
mg/L
0.200
0.00160 U
114
75-125
Iron
1.59
0.0500
mg/L
1.00
1.16
43
75-125
QM-07
Lead
0.198
0.0100
mg/L
0.200
0.00310 U
99
75-125
Magnesium
37.3
B
0.100
mg/L
2.00
90.6
NR
75-125
QM-07
Molybdenum
0.190
0.0100
mg/L
0.200
0.00604
92
75-125
Nickel
0.197
0.0100
mg/L
0.200
0.00220 U
99
75-125
Potassium
11.9
0.500
mg/L
10.0
5.80
61
75-125
QM-07
Selenium
0.184
0.0100
mg/L
0.200
0.00620 U
92
75-125
Silver
0.192
0.0100
mg/L
0.200
0.00190 U
96
75-125
Sodium
11.3
0.500
mg/L
10.0
5.77
56
75-125
QM-07
Zinc
0.229
0.0100
mg/L
0.200
0.00440 U
114
75-125
Matrix Spike Dup (9K22025-MSD1)
Prepared:
11/22/2019
10:47 Analyzed: 12/04/2019 11:24
Source: CC17854-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits
RPD
Limit
Notes
Aluminum
2.05
0.100
mg/L
2.00
0.118
96
75-125
0.5
20
Arsenic
0.176
0.0100
mg/L
0.200
0.00760 U
88
75-125
1
20
Boron
0.990
0.0500
mg/L
1.00
0.0255
96
75-125
2
20
Cadmium
0.0184
0.00100
mg/L
0.0200
0.000360 U
92
75-125
1
20
Calcium
74.6
B 0.100
mg/L
2.00
154
NR
75-125
0.3
20
QM-07
Chromium
0.187
0.0100
mg/L
0.200
0.00159
92
75-125
1
20
Copper
0.271
0.0100
mg/L
0.200
0.00160 U
135
75-125
17
20
QM-07
Iron
1.58
0.0500
mg/L
1.00
1.16
42
75-125
0.9
20
QM-07
Lead
0.190
0.0100
mg/L
0.200
0.00310 U
95
75-125
4
20
Magnesium
37.2
B 0.100
mg/L
2.00
90.6
NR
75-125
0.1
20
QM-07
Molybdenum
0.186
0.0100
mg/L
0.200
0.00604
90
75-125
2
20
Nickel
0.193
0.0100
mg/L
0.200
0.00220 U
97
75-125
2
20
Potassium
11.9
0.500
mg/L
10.0
5.80
61
75-125
0.3
20
QM-07
Selenium
0.182
0.0100
mg/L
0.200
0.00620 U
91
75-125
1
20
Silver
0.189
0.0100
mg/L
0.200
0.00190 U
94
75-125
2
20
FINAL
This report relates only to the sample as received by the
laboratory, and may only be reproduced in
full.
Page 15 of 28

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www.encolabs.com
QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 9K22025 - EPA 3005A - Continued
Matrix Spike Dup (9K22025-MSD3) Continued
Prepared: 11/22/2019 10:47 Analyzed: 12/04/2019 11:24
Source: CC17854-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Sodium
11.3
0.500
mg/L
10.0
5.77
56
75-125 0.06
20
QM-07
Zinc
0.231
0.0100
mg/L
0.200
0.00440 U
116
75-125 0.9
20
Post Spike (9K22025-PS1)
Prepared: 11/22/2019 10:47 Analyzed: 12/04/2019 11:27
Source: CC17854-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Aluminum
2.07
0.100
mg/L
2.00
0.118
98
80-120
Arsenic
0.180
0.0100
mg/L
0.200
-0.0232
90
80-120
Boron
1.01
0.0500
mg/L
1.00
0.0255
99
80-120
Cadmium
0.0187
0.00100
mg/L
0.0200
-0.000985
93
80-120
Calcium
72.5
B
0.100
mg/L
2.00
154
NR
80-120
QM-08
Chromium
0.193
0.0100
mg/L
0.200
0.00159
95
80-120
Copper
0.210
0.0100
mg/L
0.200
-0.00231
105
80-120
Iron
1.58
0.0500
mg/L
1.00
1.16
41
80-120
QM-08
Lead
0.198
0.0100
mg/L
0.200
0.00200
98
80-120
Magnesium
36.1
B
0.100
mg/L
2.00
90.6
NR
80-120
QM-08
Molybdenum
0.190
0.0100
mg/L
0.200
0.00604
92
80-120
Nickel
0.198
0.0100
mg/L
0.200
0.00173
98
80-120
Potassium
12.0
0.500
mg/L
10.0
5.80
62
80-120
QM-08
Selenium
0.177
0.0100
mg/L
0.200
-0.0256
88
80-120
Silver
0.198
0.0100
mg/L
0.200
0.000318
99
80-120
Sodium
11.3
0.500
mg/L
10.0
5.77
55
80-120
QM-08
Zinc
0.231
0.0100
mg/L
0.200
0.00418
113
80-120
Metals (Dissolved) by EPA 6000/7000 Series Methods - Quality
Control
Batch 9K22025 - EPA 3005A
Blank (9K22025-BLK1) Prepared: 11/22/2019 10:47 Analyzed: 12/04/2019 10:58
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Calcium
0.0449
3
0.100
mg/L
Magnesium
34.9
3
100
ug/L
Silica (Si02)
0.03
U
0.2
mg/L
Blank (9K22025-BLK2)
Prepared: 11/22/2019 10:47 Analyzed: 12/04/2019 11:11
Spike Source %REC RPD
Analvte
Result
Flaq
Q
Units
Level Result %REC Limits RPD Limit Notes
Calcium
0.0390
U
0.100
mg/L
Magnesium
32.6
3
100
ug/L
Silica (Si02)
0.03
U
0.2
mg/L
LCS (9K22025-BS3)
Prepared: 11/22/2019 10:47 Analyzed: 12/04/2019 11:17
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Calcium 2.13 0.100 mg/L 2.00 106 80-120
Magnesium 1980 100 ug/L 2000 99 80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 16 of 28

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www.encolabs.com
QUALITY CONTROL DATA
Metals (Dissolved) by EPA 6000/7000 Series Methods - Quality Control
Batch 9K22025 - EPA 3005A - Continued
Matrix Spike (9K22025-MS3)
Prepared: 11/22/2019 10:47 Analyzed: 12/04/2019 11:22
Source: CC17854-01
Spike Source %REC
RPD
Analvte
Result Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Calcium
74.4
0.100
mg/L
2.00 154 NR 75-125
QM-07
Magnesium
37300
100
ug/L
2000 90600 NR 75-125
QM-07
Matrix Spike Dup (9K22025-MSD3)
Prepared: 11/22/2019 10:47 Analyzed: 12/04/2019 11:24
Source: CC17854-01
Spike Source %REC
RPD
Analvte
Result Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Calcium
74.6
0.100
mg/L
2.00 154 NR 75-125 0.3
20
QM-07
Magnesium
37200
100
ug/L
2000 90600 NR 75-125 0.1
20
QM-07
Post Spike (9K22025-PSI)
Prepared: 11/22/2019 10:47 Analyzed: 12/04/2019 11:27
Source: CC17854-01
Spike Source %REC
RPD
Analvte
Result Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Calcium
72.5
0.100
mg/L
2.00 154 NR 80-120
QM-08
Magnesium
36.1
0.100
mg/L
2.00 90.6 NR 80-120
QM-08
Classical Chemistry Parameters - Quality Control
Batch 9K20014 - NO PREP
Blank (9K20024-BLKI) Prepared: 11/20/2019 10:26 Analyzed: 11/20/2019 12:15
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Orthophosphate as P 0.20 1 0.50 mg/L
LCS (9K20024-BS3) Prepared: 11/20/2019 10:26 Analyzed: 11/20/2019 12:24
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit Notes
Orthophosphate as P
4.9
B
0.50
mg/L
5.00 98 90-110
Matrix Spike (9K20024-MSI)
Prepared: 11/20/2019 10:26 Analyzed: 11/20/2019 12:41
Source: CC17678-02
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit Notes
Orthophosphate as P
11
BD
2.5
mg/L
2.00 9.1 94 90-110
Matrix Spike Dup (9K20024-MSD3)
Prepared: 11/20/2019 10:26 Analyzed: 11/20/2019 12:42
11
Source: CC17678-02
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit Notes
Orthophosphate as P
11
BD
2.5
mg/L
2.00 9.1 97 90-110 0.5
10
Batch 9K21004 - NO PREP
Blank (9K23004-BLK1)
Prepared & Analyzed: 11/21/2019 08:32
Spike Source %REC
RPD
Analvte
Result
Flag
Q
Units
Level Result %REC Limits RPD
Limit Notes
Turbidity
0.50
U
1.0
NTU
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 17 of 28

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www.encolabs.com
QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9K21004 - NO PREP - Continued
LCS (9K21004-BS3) Prepared & Analyzed: 11/21/2019 08:32
Spike Source %REC
RPD
Analvte
Result Flaq
Q
Units
Level Result %REC Limits RPD
Limit Notes
Turbidity
20
1.0
NTU
20.0 100 80-120
Duplicate (9K23004-DUP3)
Prepared & Analyzed: 11/21/2019 08:32
Source: CC16679-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Turbidity
0.50 U
1.0
NTU
0.50 U
25
Batch 9K21007 - NO PREP
Blank (9K23007-BLKS)
Prepared: 11/21/2019 08:50 Analyzed: 11/21/2019 09:48
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
0.017
U
0.10
mg/L
LCS (9K21007-BS3)
Prepared: 11/21/2019 08:50 Analyzed: 11/21/2019 09:40
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
1.0
0.10
mg/L
1.00 101 90-110
Matrix Spike (9K21007-MSi)
Prepared: 11/21/2019 08:50 Analyzed: 11/21/2019 09:50
Source: CC18642-03
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
1.1
0.10
mg/L
1.00 0.017 U 112 90-110
QM-07
Matrix Spike Dup (9K21007-MSD3)
Prepared: 11/21/2019 08:50 Analyzed: 11/21/2019 09:51
Source: CC18642-03
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
1.1
0.10
mg/L
1.00 0.017 U 114 90-110 1
10
QM-07
Batch 9K22007 - NO PREP
Blank (9K22007-BLK1)
Prepared & Analyzed: 11/23/2019 16:21
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Dissolved Solids
50
U
50
mg/L
LCS (9K22007-BS1)
Prepared & Analyzed: 11/23/2019 16:21
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Dissolved Solids
990
50
mg/L
1000 99 80-120
Duplicate (9K22007-DUPI)
Prepared & Analyzed: 11/23/2019 16:21
Source: CC16868-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Dissolved Solids
2300
50
mg/L
2200 1
20
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 18 of 28

(� �Eo
www.encolabs.com
QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9K22007 - NO PREP - Continued
Duplicate (9K22007-DUP2) Prepared & Analyzed: 11/23/2019 16:21
Source: CC18500-01
Spike Source %REC RPD
Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes
Total Dissolved Solids 88 50 mg/L 94 7 20
Batch 9K22033 - NO PREP
Blank (9K22033-BLKl) Prepared: 11/22/2019 13:48 Analyzed: 11/22/2019 17:04
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Alkalinity as CaCO3 14 U 15 mg/L
LCS (9K22033-BS3) Prepared: 11/22/2019 13:48 Analyzed: 11/22/2019 17:06
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Alkalinity as CaCO3
99
15
mg/L
100 99 80-120
Matrix Spike (9K22033-MS3)
Prepared: 11/22/2019 13:48 Analyzed: 11/22/2019 17:07
Source: CC18499-01
Spike Source %REC
RPD
Analvte
Result
Flaq
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Total Alkalinity as CaCO3
72
15
mg/L
37.8 22 132 80-120
QM-07
Matrix Spike (9K22033-MS2)
Prepared: 11/22/2019 13:48 Analyzed: 11/22/2019 17:11
Source: CC18642-03
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Alkalinity as CaCO3
46
15
mg/L
37.8 14 U 121 80-120
QM-07
Matrix Spike Dup (9K22033-MSD3)
Prepared: 11/22/2019 13:48 Analyzed: 11/22/2019 17:08
Source: CC18499-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Alkalinity as CaCO3
71
15
mg/L
37.8 22 128 80-120 2
25
QM-07
Batch 9K25012 - Same
Blank (9K25012-BLK1)
Prepared: 11/25/2019 10:48 Analyzed: 12/06/2019 18:34
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Kjeldahl Nitrogen
0.26
U
0.48
mg/L
LCS (9K25012-BS1)
Prepared: 11/25/2019 10:48 Analyzed: 12/06/2019 18:36
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Kjeldahl Nitrogen
11
0.48
mg/L
12.0 93 90-110
LCS (9K25012-BS2)
Prepared: 11/25/2019 10:48 Analyzed: 12/12/2019 13:18
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Kjeldahl Nitrogen
12
0.48
mg/L
12.0 98 90-110
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 19 of 28

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9K25012 - Same - Continued
Matrix Spike (9K25012-MS3)
Prepared: 11/25/2019 10:48 Analyzed: 12/06/2019 18:39
Source: CC16868-02
Spike Source %REC
RPD
Analvte
Result Flag
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
3.0
0.48
mg/L
4.80 0.66 49 90-110
QM-07
Matrix Spike (9K25012-MS2)
Prepared: 11/25/2019 10:48 Analyzed: 12/06/2019 18:44
Source: CC16870-01
Spike Source %REC
RPD
Analvte
Result Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
2.1
0.48
mg/L
4.80 1.7 8 90-110
QM-07
Matrix Spike Dup (9K25012-MSD3)
Prepared: 11/25/2019 10:48 Analyzed: 12/06/2019 18:41
Source: CC16868-02
Spike Source %REC
RPD
Analvte
Result Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
3.7
0.48
mg/L
4.80 0.66 63 90-110 21
10
QM-07
Batch 9K25013 - Same
Blank (9K25013-BLK1) Prepared: 11/25/2019 10:48 Analyzed: 12/10/2019 15:47
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
0.025
U
0.10
mg/L
LCS (9K25013-BS1)
Prepared: 11/25/2019 10:48 Analyzed: 12/10/2019 15:49
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
1.4
0.10
mg/L
1.60 90 80-120
Matrix Spike (9K25013-MS1)
Prepared: 11/25/2019 10:48 Analyzed: 12/10/2019 15:51
Source: CC16868-02
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
2.1
0.10
mg/L
0.640 1.3 111 80-120
Matrix Spike Dup (9K25013-MSD1)
Prepared: 11/25/2019 10:48 Analyzed: 12/10/2019 15:53
Source: CC16868-02
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
2.0
0.10
mg/L
0.640 1.3 98 80-120 4
25
Batch 9K25014 - NO PREP
Blank (9K25014-BLK1)
Prepared & Analyzed: 11/25/2019 11:30
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Specific Conductance (EC) at 25 Deg C
1.0
U
1.0
umhos/cm
LCS (9K25014-BS3)
Prepared & Analyzed: 11/25/2019 11:30
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Specific Conductance (EC) at 25 Deg C
720
1.0
umhos/cm
705 102 90-110
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 20 of 28

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9K25014 - NO PREP - Continued
Duplicate (9K25014-DUPl)
Prepared & Analyzed: 11/25/2019 11:30
Source: CC16868-03
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Specific Conductance (EC) at 25 Deg C
3400
1.0
umhos/cm
3300
0.6
25
Duplicate (9K25014-DUP2)
Prepared & Analyzed: 11/25/2019 11:30
Source: CC17678-02
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Specific Conductance (EC) at 25 Deg C
3800
1.0
umhos/cm
3800
0
25
Batch 9K25035 - NO PREP
Blank (9K25035-BLKS) Prepared & Analyzed: 11/25/2019 13:08
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Suspended Solids 2.5 U 2.5 mg/L
LCS (9K25035-BS3) Prepared & Analyzed: 11/25/2019 13:08
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Total Suspended Solids
93
2.5
mg/L
100 93 80-120
Duplicate (9K25035-DUP3)
Prepared & Analyzed: 11/25/2019 13:08
Source: CC16656-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Total Suspended Solids
260
78
mg/L
280
8
20
Duplicate (9K25035-DUP2)
Prepared & Analyzed: 11/25/2019 13:08
Source: CC18645-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Total Suspended Solids
61
25
mg/L
50
20
20
Batch 9K26027 - NO PREP
LCS (9K26027-BS3) Prepared & Analyzed: 11/26/2019 14:47
Spike Source %REC
RPD
Analvte
Result Flag
Q
Units
Level Result %REC Limits RPD
Limit Notes
pH
7.0
1.0
pH
7.00 99 99-101
Duplicate (9K26027-DUPi)
Prepared & Analyzed: 11/26/2019 14:47
Source: CC14689-02
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
pH
7.5
1.0
pH
7.5 0.1
25
Batch 9K27015 - NO PREP
Blank (9K27025-BLKS) Prepared: 11/27/2019 15:34 Analyzed: 12/02/2019 11:13
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Chloride 2.2 U 5.0 mg/L
Sulfate as SO4 2.9 U 5.0 mg/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 21 of 28

QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9K27025 - NO PREP - Continued
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LCS (9K27025-BS3) Prepared: 11/27/2019 15:34 Analyzed: 11/28/2019 02:32
Spike Source %REC
RPD
Analvte
Result
Flaq
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Chloride
50
5.0
mg/L
50.0 101 90-110
Sulfate as SO4
52
5.0
mg/L
50.0 103 90-110
Matrix Spike (9K27025-MSI)
Prepared: 11/27/2019 15:34 Analyzed: 11/28/2019 03:43
Source: CC18820-03
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chloride
46
5.0
mg/L
20.0 25 106 90-110
Sulfate as SO4
53
5.0
mg/L
20.0 31 113 90-110
QM-07
Matrix Spike (9K27025-MS2)
Prepared: 11/27/2019 15:34 Analyzed: 11/28/2019 04:36
Source: CC18820-04
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chloride
21
5.0
mg/L
20.0 2.4 92 90-110
Sulfate as SO4
23
5.0
mg/L
20.0 3.9 97 90-110
Matrix Spike Dup (9K27025-MSD3)
Prepared: 11/27/2019 15:34 Analyzed: 11/28/2019 04:01
Source: CC18820-03
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chloride
47
5.0
mg/L
20.0 25 108 90-110 0.6
10
Sulfate as SO4
54
5.0
mg/L
20.0 31 115 90-110 0.8
10
QM-07
Batch 9K28001 - Same
Blank (9K28001-BLKS) Prepared: 11/28/2019 11:21 Analyzed: 11/28/2019 13:55
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Chemical Oxygen Demand 10 U 10 mg/L
LCS (9K28001-BS3) Prepared: 11/28/2019 11:21 Analyzed: 11/28/2019 13:55
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Chemical Oxygen Demand
480
10
mg/L
500 97 90-110
Matrix Spike (9K28001-MSi)
Prepared: 11/28/2019 11:21 Analyzed: 11/28/2019 13:55
Source: CC17678-02
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Chemical Oxygen Demand
630
10
mg/L
526 120 96 90-110
Matrix Spike Dup (9K28001-MSD3)
Prepared: 11/28/2019 11:21 Analyzed: 11/28/2019 13:55
111
Source: CC17678-02
Analvte
Chemical Oxygen Demand
Batch 9LO2005 - Same
Result Flaq POL
620
10
Spike Source %REC
Units Level Result %REC Limits RPD
mg/L 526 120 94 90-110 2
RPD
Limit Notes
5
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 22 of 28

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9LO2005 - Same - Continued
Blank (9L02005-BLK3) Prepared: 12/02/2019 09:47 Analyzed: 12/02/2019 15:23
Spike Source %REC RPD
Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes
Cyanide (total) 0.0049 U 0.0050 mg/L
LCS (9L02005-BSI) Prepared: 12/02/2019 09:47 Analyzed: 12/02/2019 15:25
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Cyanide (total)
0.16
0.0050
mg/L
0.150 109 90-110
Matrix Spike (9L02005-MS3)
Prepared: 12/02/2019 09:47 Analyzed: 12/02/2019 15:32
Source: CC17678-02
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Cyanide (total)
0.18
0.0050
mg/L
0.150 0.0051 114 90-110
QM-07
Matrix Spike (9L02005-MS2)
Prepared: 12/02/2019 09:47 Analyzed: 12/02/2019 15:37
Source: CC17678-03
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Cyanide (total)
0.17
0.0050
mg/L
0.150 0.0049 U 113 90-110
QM-07
Matrix Spike Dup (9L02005-MSD3)
Prepared: 12/02/2019 09:47 Analyzed: 12/02/2019 15:34
Source: CC17678-02
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Cyanide (total)
0.17
0.0050
mg/L
0.150 0.0051 109 90-110 4
10
Batch 9LO2010 - NO PREP
Blank (9L02010-BLK1) Prepared: 12/02/2019 09:25 Analyzed: 12/02/2019 13:25
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Alkalinity as CaCO3 14 U 15 mg/L
LCS (9L02010-BS3) Prepared: 12/02/2019 09:25 Analyzed: 12/02/2019 13:26
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Total Alkalinity as CaCO3
100
15
mg/L
100
104
80-120
Matrix Spike (9L02030-MS3)
Prepared: 12/02/2019 09:25 Analyzed: 12/02/2019 13:27
Source: CC18500-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Total Alkalinity as CaCO3
90
15
mg/L
37.8
37
141
80-120
QM-07
Matrix Spike Dup (9L02030-MSDI)
Prepared: 12/02/2019 09:25 Analyzed: 12/02/2019 13:28
Source: CC18500-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Total Alkalinity as CaCO3
87
15
mg/L
37.8
37
132
80-120 4
25
QM-07
Batch 9LO2037 - NO PREP
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 23 of 28

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9LO2037 - NO PREP - Continued
Blank (9L02037-BLK3) Prepared: 12/02/2019 14:00 Analyzed: 12/02/2019 17:04
Spike Source %REC RPD
Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes
Chloride 2.2 U 5.0 mg/L
Sulfate as SO4 2.9 U 5.0 mg/L
LCS (911-02037-BSI) Prepared: 12/02/2019 14:00 Analyzed: 12/02/2019 17:21
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chloride
48
5.0
mg/L
50.0 97 90-110
Sulfate as SO4
48
5.0
mg/L
50.0 95 90-110
Matrix Spike (911-02037-MS3)
Prepared: 12/02/2019 14:00 Analyzed: 12/02/2019 17:57
Source: CC18642-03
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chloride
24
5.0
mg/L
20.0 5.1 94 90-110
Sulfate as SO4
28
5.0
mg/L
20.0 9.2 96 90-110
Matrix Spike (911-02037-MS2)
Prepared: 12/02/2019 14:00 Analyzed: 12/02/2019 18:50
Source: CC18496-07
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chloride
88
5.0
mg/L
20.0 68 98 90-110
Sulfate as SO4
63
5.0
mg/L
20.0 43 101 90-110
Matrix Spike Dup (9L02037-MSDI)
Prepared: 12/02/2019 14:00 Analyzed: 12/02/2019 18:14
Source: CC18642-03
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chloride
24
5.0
mg/L
20.0 5.1 96 90-110 1
10
Sulfate as SO4
29
5.0
mg/L
20.0 9.2 97 90-110 1
10
Batch 9L05016 - NO PREP
Blank (9L05016-BLK3)
Prepared: 12/05/2019 09:20 Analyzed: 12/05/2019 13:02
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
0.041
U
0.10
mg/L
LCS (911-05016-BSI)
Prepared: 12/05/2019 09:20 Analyzed: 12/05/2019 13:04
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
1.3
0.10
mg/L
1.25 102 90-110
Matrix Spike (9L05016-MS3)
Prepared: 12/05/2019 09:20 Analyzed: 12/05/2019 13:08
Source: CC18642-03
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
0.51
0.10
mg/L
0.521 0.041 U 99 90-110
Matrix Spike (911-05016-MS2)
Prepared: 12/05/2019 09:20 Analyzed: 12/05/2019 13:13
Source: CC18642-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
FINAL
This report relates only to the sample as received by the
laboratory, and may only be reproduced in full.
Page 24 of 28

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9L05016 - NO PREP - Continued
Matrix Spike (911-05016-MS2) Continued
Prepared: 12/05/2019 09:20 Analyzed: 12/05/2019 13:13
Source: CC18642-01
Spike Source %REC
RPD
Analvte
Result Flaq
Q
Units
Level Result %REC Limits RPD
Limit Notes
Nitrate/Nitrite as N
1.1
0.10
mg/L
0.521 0.51 106 90-110
Matrix Spike Dup (911-05016-MSD3)
Prepared: 12/05/2019 09:20 Analyzed: 12/05/2019 13:09
Source: CC18642-03
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrate/Nitrite as N
0.53
0.10
mg/L
0.521 0.041 U 101 90-110 2
10
Batch 9L11013 - NO PREP
Blank (911-11013-BL11(l)
Prepared: 12/11/2019 09:11 Analyzed: 12/11/2019 13:01
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Ammonia as N 0.045 U 0.10 mg/L
LCS (9L11013-BS1) Prepared: 12/11/2019 09:11 Analyzed: 12/11/2019 13:03
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Ammonia as N
1.0
0.10
mg/L
1.01
99
90-110
Matrix Spike (9L33013-MS3)
Prepared: 12/11/2019 09:11 Analyzed: 12/11/2019 13:06
Source: CC12662-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Ammonia as N
0.40
0.10
mg/L
0.393
0.062
86
90-110
QM-07
Matrix Spike (9L11013-MS2)
Prepared: 12/11/2019 09:11 Analyzed: 12/11/2019 13:15
Source: CC17932-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Ammonia as N
0.97
0.10
mg/L
0.393
0.60
94
90-110
Matrix Spike Dup (911-11013-MSDl)
Prepared: 12/11/2019 09:11 Analyzed: 12/11/2019 13:08
Source: CC12662-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Ammonia as N
0.40
0.10
mg/L
0.393
0.062
85
90-110 1
10
QM-07
Classical Chemistry Parameters - Quality Control
Batch 9K22006 - NO PREP
Blank (9K22006-BLK1) Prepared: 11/22/2019 09:00 Analyzed: 11/22/2019 10:37
Spike Source %REC RPD
Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes
Total Organic Carbon 0.34 U 1.0 mg/L
LCS (9K22006-BS3) Prepared: 11/22/2019 09:00 Analyzed: 11/22/2019 10:37
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Organic Carbon 38 1.0 mg/L 40.0 95 85-115
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 25 of 28

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9K22006 - NO PREP - Continued
Matrix Spike (9K22006-MS3)
Prepared: 11/22/2019 09:00 Analyzed: 11/22/2019 10:37
Source: AC08219-03
Spike
Source
%REC
RPD
Analvte Result Flag
Q
Units
Level
Result
%REC Limits RPD
Limit Notes
Total Organic Carbon 41
1.0
mg/L
40.0
1.1
99 85-115
Matrix Spike Dup (9K22006-MSD3)
Prepared: 11/22/2019 09:00 Analyzed: 11/22/2019 10:37
Source: AC08219-03
Spike
Source
%REC
RPD
Analvte Result Flag
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Total Organic Carbon 39
1.0
mg/L
40.0
1.1
95 85-115 4
21
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 26 of 28

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
Q-01 Analysis performed outside of method - specified holding time.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 27 of 28

ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com
10775 Central Port C� Orlando, F 32824 Dr Jacksonville, FL10 Executivep32216-6069 ark Court, Suite 1 f 1 Cary, NC 22751 ids Industrial Ct.
[phone] Fax [phone] (9Q4) 296.3007 Fax [phone]
(919) 487-309Q Fax {9f9) 4&7.35f 5 Page of
Client Name Project Number Requested Analyses Requested Turnaround
Novozymes Nort h America (NO008) [none] Times
Address Project Name/Desc
J Note : Rush requests subject to
77 Perry Ghf apel Church Road RO Pilot Q � y�j acceptance by the facility
City/ST/2'ip PO # 1 Billing Info
Franldinw, NC :27525 4550996257Tel Fax Reporting Contact tr_ a Standard
(919),494-3000 r Scott Creech 6 N o J �,; v
v_ ,n I— v Expedited
Sam ler(s) Nome, Affiliation (Print) Billing Contact V t.:- �} (+7 IN
` Accounts nts Payable l2. �- - Due
�I_I
Sampler(s) Signature Site Location / Time Zone � � �6 � O � � w r Lab Workorder
L! p �R m U U I CL � !n � �G f77
Preservation (See Codes) (Combine as necessary)
Collection Matrix Total a of
Ilem f: Sample ID (Field Identification) Collection nate Time Camp / Grab {see codes) Containers Sample Comments
IE313R Feed 1V ( 0 ( [9 kC Wk Ca
Q Fe(Bd ll [ 1 �I tCj 1(,- Ck k WW
ci FP 4 rmfiFAe tl {() Ick
—LEE
-- Total # of Containers
Sample Kit Prepared By Datef ime Relinquished By DelarTtme Received Dalefrime
`__)CCsCt s.� 1 I r kl)AD
CommenwSpecial Reporting Requirements Relinquished By DateMmei By Date me
C&. T Olt,
UN C) �A Relinquished By Date/Time eceived By Dateim e
1 Y` r
ler #'s & Temps on Receipt Condifian pon Receipt
r ` L- Acceptable _ Unacceptable
Matrix: GW-Groundwater SO -Soil DW-Dnnktng Water SE-Sedimenl SW -Surface Water WW-Wastewater A -Air O.Olher (detail in comments) Preservation: l-Ice H-HCl N-HNO3 S-H2SO4 NO-NaOH O-Other (detail in comments)
Note: All samples submitted to ENCO Labs are in accordance with the terms and conditions listed on the reverse of this form, unless prior written agreements exjst

Sample Preservation Verification
ENCO Cary
@jhl: CEGD)
Work Order: CC17678 Project: RO Pilot
Client: Novozymes North America (NO008) Project #: [none]
Logged In: 20-Nov-19 09:46 Logged By: John C King Preservation Check Performed By: Date/Time: <I /% ene- z
CC17678-02
Cant
Type
y
Pres (pH)
Requirement
pH Checked/
In Control
Date/Time
pH Adjusted Adjusted
Reagent Used/Comments
B
250mLP+HNO3
<2
Y 1 N 1 NA
/ N / NA
C
250mLP+NaOH
>12
I N I NA
Y I N/ NA
E
500mLP+H2SO4
<2
Y / N I NA
Y /i / NA
CC17678-03
Cant
Type
yp
Pres (pH)
Requirement
pH Checked /
In Control
tDate�me
pH Adjusted Adjusted
Reagent Used/Comments
B
250mLP+HNO3
<2
/ N / NA
Y / R / NA
C
250mLP+NaOH
>12
/ N I NA
Y / Uf I / NA
E
500mLP+H2SO4 1
2
I N / NA
I Y / N` NA
CC 17678-04
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted Datemme
Adjusted
Reagent Used/Comments
B
250mLP+HNO3
<2
Y / NA
1f I N / NA
C
250mLP+NaOH
>12
/ N / NA
Y 2 / NA
E
500mLP+H2SO4
<2
I N/ NA
Y/ I NA
CC17678-05
Cont
yp
Type
Pres (pH)
Requirement
pH Checked i
In Control
Date/Time
pH Adjusted Adiusted
Reagent Used/Comments
A
25CmLP+HNO3
<2
Y 1 N / NA
Y )U4 / NA
Rea ent Name 1D
1
2 TEE
pH Strip ID: ;L
Reacent dame ID
3
4 :::-F I
Rea ent Name ID
5
6
C:IELMNT1Printlwko_PreservatjonCheck. rpt Page 1 of 1

2�SENCO Laboratories
9g
Accurate. Timely. Respousive. luuavative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Thursday, November 14, 2019
Novozymes North America (N0008)
Attn: Scott Creech
77 Perry Chapel Church Road
Franklinton, NC 27525
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: RO Pilot
ENCO Workorder(s): CC17581
Dear Scott Creech,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Wednesday, October 30, 2019.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
0"CLC'L�CA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 25

(� �Eo
www.encolabs.com
SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: MBBR Feed
Lab ID: CC17581-01
Sampled: 10/29/19 14:15
Received: 10/30/19
09:30
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 6010D
EPA 3005A
04/26/20
11/05/19
13:09
11/07/19
12:17
SM 5210 B-2011
NO PREP
10/31/19
14:15
10/31/19
12:36
10/31/19
12:36
Client ID: RO Feed
Lab ID: CC17581-02
Sampled: 10/29/19 14:15
Received: 10/30/19
09:30
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
CALC
[CALC]
11/26/19
11/08/19
13:26
11/08/19
18:03
EPA 300.0
NO PREP
11/26/19
11/05/19
13:35
11/05/19
21:32
EPA 310.2
NO PREP
11/12/19
11/05/19
11:35
11/05/19
16:22
EPA 335.4
Same
11/12/19
11/06/19
14:37
11/11/19
16:02
EPA 350.1
NO PREP
11/26/19
11/12/19
09:26
11/12/19
11:45
EPA 351.2
Same
11/26/19
10/31/19
10:45
11/07/19
13:13
EPA 353.2
NO PREP
10/31/19
14:15
10/31/19
09:36
10/31/19
11:28
EPA 353.2
[CALC]
10/31/19
14:15
11/08/19
13:26
11/08/19
18:03
EPA 353.2
NO PREP
11/26/19
11/08/19
13:26
11/08/19
18:03
EPA 365.1
NO PREP
10/31/19
14:15
10/31/19
09:40
10/31/19
11:54
EPA 365.4
Same
11/26/19
10/31/19
10:45
11/07/19
14:26
EPA 6010D
EPA 3005A
04/26/20
11/05/19
13:17
11/07/19
15:05
EPA 7470A
EPA 7470A
11/26/19
11/04/19
14:53
11/05/19
13:55
SM 213OB-2011
NO PREP
10/31/19
14:15
10/31/19
08:45
10/31/19
08:45
SM 251OB-2011
NO PREP
11/26/19
11/05/19
15:00
11/05/19
15:00
SM 2540C-2011
NO PREP
11/05/19
11/01/19
15:20
11/01/19
15:20
SM 254OD-2011
NO PREP
11/05/19
11/01/19
10:32
11/01/19
10:32
SM 4500002 D-2011
NO PREP
07/24/22
11/08/19
13:10
11/08/19
13:10
SM 4500H+B-2011
NO PREP
10/29/19
14:29
11/01/19
16:34
11/01/19
16:34
SM 5220D-2011
Same
11/26/19
11/05/19
10:29
11/05/19
14:05
Client ID: RO Feed
Lab ID: CC17581-02RE1
Sampled: 10/29/19 14:15
Received: 10/30/19
09:30
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 365.4
Same
11/26/19
10/31/19
10:45
11/07/19
19:01
Client ID: RO Permeate
Lab ID: CC17581-03
Sampled: 10/29/19 14:15
Received: 10/30/19
09:30
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
CALC
[CALC]
11/26/19
11/08/19
13:26
11/08/19
18:05
EPA 300.0
NO PREP
11/26/19
11/05/19
13:35
11/05/19
21:50
EPA 310.2
NO PREP
11/12/19
11/05/19
11:35
11/05/19
16:22
EPA 335.4
Same
11/12/19
11/06/19
14:37
11/11/19
16:04
EPA 350.1
NO PREP
11/26/19
11/12/19
09:26
11/12/19
11:47
EPA 351.2
Same
11/26/19
10/31/19
10:45
11/07/19
13:15
EPA 353.2
NO PREP
10/31/19
14:15
10/31/19
09:36
10/31/19
11:33
EPA 353.2
[CALC]
10/31/19
14:15
11/08/19
13:26
11/08/19
18:05
EPA 353.2
NO PREP
11/26/19
11/08/19
13:26
11/08/19
18:05
EPA 365.1
NO PREP
10/31/19
14:15
10/31/19
09:40
10/31/19
11:57
EPA 365.4
Same
11/26/19
10/31/19
10:45
11/07/19
14:28
EPA 6010D
EPA 3005A
04/26/20
11/05/19
13:17
11/07/19
10:53
EPA 7470A
EPA 7470A
11/26/19
11/04/19
14:53
11/05/19
13:58
SM 213OB-2011
NO PREP
10/31/19
14:15
10/31/19
08:45
10/31/19
08:45
SM 251OB-2011
NO PREP
11/26/19
11/05/19
15:00
11/05/19
15:00
SM 254OC-2011
NO PREP
11/05/19
11/01/19
15:20
11/01/19
15:20
SM 2540D-2011
NO PREP
11/05/19
11/01/19
10:32
11/01/19
10:32
SM 4500002 D-2011
NO PREP
07/24/22
11/08/19
13:10
11/08/19
13:10
SM 4500H+B-2011
NO PREP
10/29/19
14:29
11/01/19
16:34
11/01/19
16:34
SM 5210 B-2011
NO PREP
10/31/19
14:15
10/31/19
12:36
10/31/19
12:36
SM 5220D-2011
Same
11/26/19
11/05/19
10:29
11/05/19
14:05
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 25

(� �Eo
www.encolabs.com
SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: RO Reject
Lab ID: CC17581-04
Sampled: 10/29/19 14:15
Received: 10/30/19 09:30
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
CALC
[CALC]
11/26/19
11/13/19
14:37
11/13/19
19:41
EPA 335.4
Same
11/12/19
11/06/19
14:37
11/11/19
16:05
EPA 350.1
NO PREP
11/26/19
11/12/19
09:26
11/12/19
11:49
EPA 351.2
Same
11/26/19
10/31/19
10:45
11/07/19
13:17
EPA 353.2
NO PREP
10/31/19
14:15
10/31/19
09:36
10/31/19
11:34
EPA 353.2
[CALC]
10/31/19
14:15
11/13/19
14:37
11/13/19
19:41
EPA 365.1
NO PREP
10/31/19
14:15
10/31/19
09:40
10/31/19
12:22
EPA 365.4
Same
11/26/19
10/31/19
10:45
11/07/19
14:29
EPA 6010D
EPA 3005A
04/26/20
11/05/19
13:17
11/07/19
10:55
EPA 7470A
EPA 7470A
11/26/19
11/04/19
14:53
11/05/19
14:00
SM 213OB-2011
NO PREP
10/31/19
14:15
10/31/19
08:45
10/31/19
08:45
SM 251OB-2011
NO PREP
11/26/19
11/05/19
15:00
11/05/19
15:00
SM 254OC-2011
NO PREP
11/05/19
11/01/19
15:20
11/01/19
15:20
SM 254OD-2011
NO PREP
11/05/19
11/01/19
10:32
11/01/19
10:32
SM 4500002 D-2011
NO PREP
07/24/22
11/08/19
13:10
11/08/19
13:10
SM 4500H+B-2011
NO PREP
10/29/19
14:29
11/01/19
16:34
11/01/19
16:34
SM 5220D-2011
Same
11/26/19
11/05/19
10:29
11/05/19
14:05
Client ID: RO Reject
Lab ID: CC17581-04RE1
Sampled: 10/29/19 14:15
Received: 10/30/19 09:30
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 300.0
NO PREP
11/26/19
11/05/19
13:35
11/06/19
13:09
EPA 310.2
NO PREP
11/12/19
11/11/19
10:23
11/11/19
18:34
EPA 353.2
NO PREP
11/26/19
11/13/19
14:37
11/13/19
19:41
Client ID: MBBR Feed
Lab ID: CC17581-05
Sampled: 10/29/19 14:15
Received: 10/30/19 09:30
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 6010D
EPA 3005A
04/26/20
11/05/19
13:17
11/07/19
11:04
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 25

0Nk"q09
www.encolabs.com
SAMPLE DETECTION SUMMARY
Client ID: MBBR Feed
Lab ID:
CC17581-03
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Biochemical Oxygen Demand - Dissolved
10
2.0
2.0
mg/L
SM 5210 B-2011
Calcium - Dissolved
220
0.195
0.500
mg/L
EPA 6010D
Magnesium - Dissolved
7930
145
500
ug/L
EPA 6010D
Silica (Si02) - Dissolved
22.9
0.1
1.1
mg/L
EPA 6010D
Client ID: RO Feed
Lab ID:
CC17581-02
Anal a
Results
Flag
MDL
Q
Units
Method
Notes
Aluminum - Total
0.478
J
0.420
1.00
mg/L
EPA 6010D
Ammonia as N
0.55
0.045
0.10
mg/L
EPA 350.1
Bicarbonate (as CaCO3)
1200
14
15
mg/L
SM 45000O2 D-2011
Calcium - Total
192
0.390
1.00
mg/L
EPA 6010D
Carbonate (as CaCO3)
28
14
15
mg/L
SM 45000O2 D-2011
Chemical Oxygen Demand
79
10
10
mg/L
SM 5220D-2011
Chloride
580
D
22
50
mg/L
EPA 300.0
Iron - Total
0.239
J
0.220
0.500
mg/L
EPA 6010D
Magnesium - Total
6.57
0.290
1.00
mg/L
EPA 6010D
Nitrate as N
0.40
JD
0.20
0.50
mg/L
EPA 353.2
Nitrate/Nitrite as N
0.67
D
0.20
0.50
mg/L
EPA 353.2
Nitrite as N
0.27
0.017
0.10
mg/L
EPA 353.2
Orthophosphate as P
2.6
0.16
0.50
mg/L
EPA 365.1
PH
8.4
1.0
1.0
pH
SM 4500H+B-2011
Q-01
Phosphorus
2.6
D
0.12
0.50
mg/L
EPA 365.4
Potassium - Total
321
1.50
5.00
mg/L
EPA 6010D
Silica (Si02) - Total
22.7
0.3
2.1
mg/L
EPA 6010D
Sodium - Total
536
4.00
5.00
mg/L
EPA 6010D
Specific Conductance (EC) at 25 Deg C
3800
1.0
1.0
umhos/cm
SM 251OB-2011
Sulfate as SO4
110
D
29
50
mg/L
EPA 300.0
Temperature for pH (deg. C)
22
pH
SM 4500H+B-2011
Q-01
Total Alkalinity as CaCO3
1200
D
140
150
mg/L
EPA 310.2
Total Dissolved Solids
2500
50
50
mg/L
SM 2540C-2011
Total Kjeldahl Nitrogen
3.9
0.26
0.48
mg/L
EPA 351.2
Total Nitrogen
4.6
D
0.26
0.50
mg/L
CALC
Client ID: RO Feed
Lab ID:
CC17581-02RE1
Anal a
Results
Flag
MDL
4
Units
Method
Notes
Phosphorus
2.7
D
0.050
0.20
mg/L
EPA 365.4
Client ID: RO Permeate
Lab ID:
CC17581-03
Anal a
Results
Flag
MDL
POLL
Units
Method
Notes
Ammonia as N
0.19
0.045
0.10
mg/L
EPA 350.1
Bicarbonate (as CaCO3)
28
14
15
mg/L
SM 45000O2 D-2011
Calcium - Total
0.560
J
0.390
1.00
mg/L
EPA 6010D
Chloride
13
2.2
5.0
mg/L
EPA 300.0
Nitrate/Nitrite as N
0.079
J
0.041
0.10
mg/L
EPA 353.2
Nitrite as N
0.045
J
0.017
0.10
mg/L
EPA 353.2
PH
5.4
1.0
1.0
pH
SM 4500H+B-2011
Q-01
Potassium - Total
12.5
1.50
5.00
mg/L
EPA 6010D
Sodium - Total
10.8
4.00
5.00
mg/L
EPA 6010D
Specific Conductance (EC) at 25 Deg C
110
1.0
1.0
umhos/cm
SM 251OB-2011
Temperature for pH (deg. C)
22
pH
SM 4500H+B-2011
Q-01
Total Alkalinity as CaCO3
28
14
15
mg/L
EPA 310.2
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 25

0Nk"q09
www.encolabs.com
SAMPLE DETECTION SUMMARY
Client ID: RO Reject
Lab ID:
CC17581-04
Analvte
Results
Flaa
MDL
PQL
Units
Method
Notes
Aluminum - Total
0.617
J
0.420
1.00
mg/L
EPA 6010D
Ammonia as N
3.2
D
0.090
0.20
mg/L
EPA 350.1
Bicarbonate (as CaCO3)
2000
14
15
mg/L
SM 4500002 D-2011
Boron - Total
0.163
J
0.0570
0.500
mg/L
EPA 6010D
Calcium - Total
928
0.390
1.00
mg/L
EPA 6010D
Chemical Oxygen Demand
650
20
20
mg/L
SM 5220D-2011
Copper - Total
0.0360
J
0.0160
0.100
mg/L
EPA 6010D
Cyanide (total)
0.0085
0.0049
0.0050
mg/L
EPA 335.4
Iron - Total
1.41
0.220
0.500
mg/L
EPA 6010D
Magnesium - Total
50.9
0.290
1.00
mg/L
EPA 6010D
Nitrate as N
2.7
D
0.082
0.20
mg/L
EPA 353.2
Nitrite as N
1.9
0.017
0.10
mg/L
EPA 353.2
Orthophosphate as P
21
D
0.80
2.5
mg/L
EPA 365.1
PH
7.5
1.0
1.0
pH
SM 4500H+B-2011
Q-01
Phosphorus
31
D
0.25
1.0
mg/L
EPA 365.4
Potassium - Total
2420
1.50
5.00
mg/L
EPA 6010D
Silica (Si02) - Total
181
0.3
2.1
mg/L
EPA 6010D
Sodium - Total
4080
4.00
5.00
mg/L
EPA 6010D
Specific Conductance (EC) at 25 Deg C
24000
1.0
1.0
umhos/cm
SM 251OB-2011
Temperature for pH (deg. C)
22
pH
SM 4500H+B-2011
Q-01
Total Dissolved Solids
23000
50
50
mg/L
SM 2540C-2011
Total Kjeldahl Nitrogen
34
D
0.52
0.96
mg/L
EPA 351.2
Total Nitrogen
39
D
0.52
0.96
mg/L
CALC
Total Suspended Solids
14
3.4
3.4
mg/L
SM 2540D-2011
Turbidity
4.8
0.50
1.0
NTU
SM 213OB-2011
Zinc - Total
0.0693
J
0.0440
0.100
mg/L
EPA 6010D
Client ID: RO Reject
Lab ID:
CC17581-04REI
Anal a
Results
Flaa
MDL
PQL
Units
Method
Notes
Chloride
4200
D
220
500
mg/L
EPA 300.0
Nitrate/Nitrite as N
4.6
D
0.082
0.20
mg/L
EPA 353.2
Sulfate as SO4
6500
D
290
500
mg/L
EPA 300.0
Total Alkalinity as CaCO3
2000
D
280
300
mg/L
EPA 310.2
Client ID: MBBR Feed
Lab ID:
CC17581-05
Anal a
Results
Flaa
MDL
4
Units
Method
Notes
Silica (Si02) - Total
34.6
0.1
1.1
mg/L
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 25

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: MBBR Feed Lab Sample ID:CC17581-01 Received: 10/30/19 09:30
Matrix: Waste Water Sampled:10/29/19 14:15 Work Order: CC17581
Project: RO Pilot Sampled By:Jelena El Barigi
Metals (Dissolved) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flao
Units
DF
MOIL
P L
Batch
Method
Analyzed
By Notes
Calcium [7440-70-2]^ 220
mg/L
5
0.195
0.500
9KO5028
EPA 6010D
11/07/19 12:17
JDH
Magnesium [7439-95-4]^ 7930
ug/L
5
145
500
9KO5028
EPA 6010D
11/07/19 12:17
JDH
Silica (Si02) [763-18-69]^ 22.9
mg/L
5
0.1
1.1
9KO5028
EPA 6010D
11/07/19 12:17
JDH
Classical Chemistry Parameters (Dissolved)
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flao
Units
OF
MOIL
P L
Batch
Method
Analyzed
By Notes
Biochemical Oxygen Demand 10
mg/L
1
2.0
2.0
9331007
SM 5210 B-2011
10/31/19 12:36
JOC
Description: RO Feed Lab Sample ID:CC17581-02 Received: 10/30/19 09:30
Matrix: Waste Water Sampled:10/29/19 14:15 Work Order: CC17581
Project: RO Pilot Sampled By:Jelena El Barigi
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MOIL
P L
Batch
Method
Analyzed
By
Notes
Mercury[7439-97-6]^
0.000750
U
mg/L
5
0.000750
0.00100
9KO4029
EPA 7470A
11/05/19 13:55
KAH
Silica (Si02) [763-18-69]^
22.7
mg/L
10
0.3
2.1
9KO5031
EPA 6010D
11/07/19 15:05
JDH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MOIL
P L
Batch
Method
Analyzed
By
Notes
Aluminum [7429-90-5]^
0.478
J
mg/L
10
0.420
1.00
9KO5031
EPA 6010D
11/07/19 15:05
JDH
Arsenic [7440-38-2]^
0.0760
U
mg/L
10
0.0760
0.100
9KO5031
EPA 6010D
11/07/19 15:05
JDH
Boron [7440-42-8]^
0.0570
U
mg/L
10
0.0570
0.500
9KO5031
EPA 6010D
11/07/19 15:05
JDH
Cadmium [7440-43-9]^
0.00360
U
mg/L
10
0.00360
0.0100
9KO5031
EPA 6010D
11/07/19 15:05
JDH
Calcium [7440-70-2]^
192
mg/L
10
0.390
1.00
9KO5031
EPA 6010D
11/07/19 15:05
JDH
Chromium [7440-47-3]^
0.0140
U
mg/L
10
0.0140
0.100
9KO5031
EPA 6010D
11/07/19 15:05
JDH
Copper[7440-50-8]^
0.0160
U
mg/L
10
0.0160
0.100
9KO5031
EPA 6010D
11/07/19 15:05
JDH
Iron [7439-89-6]^
0.239
J
mg/L
10
0.220
0.500
9KO5031
EPA 6010D
11/07/19 15:05
JDH
Lead [7439-92-1]^
0.0310
U
mg/L
10
0.0310
0.100
9KO5031
EPA 6010D
11/07/19 15:05
JDH
Magnesium [7439-95-4]^
6.57
mg/L
10
0.290
1.00
9KO5031
EPA 6010D
11/07/19 15:05
JDH
Molybdenum [7439-98-7]^
0.0250
U
mg/L
10
0.0250
0.100
9KO5031
EPA 6010D
11/07/19 15:05
JDH
Nickel[7440-02-0]^
0.0220
U
mg/L
10
0.0220
0.100
9KO5031
EPA 6010D
11/07/19 15:05
JDH
Potassium [7440-09-7]^
321
mg/L
10
1.50
5.00
9KO5031
EPA 6010D
11/07/19 15:05
JDH
Selenium [7782-49-2]^
0.0620
U
mg/L
10
0.0620
0.100
9KO5031
EPA 6010D
11/07/19 15:05
JDH
Silver[7440-22-4]^
0.0190
U
mg/L
10
0.0190
0.100
9KO5031
EPA 6010D
11/07/19 15:05
JDH
Sodium [7440-23-5]^
536
mg/L
10
4.00
5.00
9KO5031
EPA 6010D
11/07/19 15:05
JDH
Zinc[7440-66-6]^
0.0440
U
mg/L
10
0.0440
0.100
9KO5031
EPA 6010D
11/07/19 15:05
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MOIL
P L
Batch
Method
Analyzed
By
Notes
Ammonia as N [7664-41-7]^
0.55
mg/L
1
0.045
0.10
9K12021
EPA 350.1
11/12/19 11:45
PDK
Bicarbonate (as CaCO3)[71-52-3]
1200
mg/L
1
14
15
9KO8017
M 4500002 D-201
11/08/19 13:10
JAH
Carbonate (as CaCO3)[3812-32-6]
28
mg/L
1
14
15
9KO8017
M 4500002 D-201
11/08/19 13:10
JAH
Chemical Oxygen Demand^
79
mg/L
1
10
10
9KO5009
SM 5220D-2011
11/05/19 14:05
JOC
Chloride [16887-00-6]^
580
D
mg/L
10
22
50
9KO5034
EPA 300.0
11/05/19 21:32
PDK
Cyanide (total) [57-12-5]^
0.0049
U
mg/L
1
0.0049
0.0050
9KO6033
EPA 335.4
11/11/19 16:02
AKF
FINAL
This report relates only
to the sample as received by the laboratory,
and may only
be reproduced
in full.
Page 6 of 25

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: RO Feed Lab Sample ID:CC17581-02 Received: 10/30/19 09:30
Matrix: Waste Water Sampled:10/29/19 14:15 Work Order: CC17581
Project: RO Pilot Sampled By:Jelena El Barigi
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results
Flao
Units
DF
MDL
P L
Batch
Method
Analyzed
By
Notes
Nitrate as N [14797-55-8]
0.40
JD
mg/L
5
0.20
0.50
[CALC]
EPA 353.2
11/08/19 18:03
AKF
Nitrate/Nitrite as IN
0.67
D
mg/L
5
0.20
0.50
9KO8019
EPA 353.2
11/08/19 18:03
AKF
Nitrite as N [14797-65-0]^
0.27
mg/L
1
0.017
0.10
9331018
EPA 353.2
10/31/19 11:28
AKF
Orthophosphate as P [1426-54-42]^
2.6
mg/L
1
0.16
0.50
9331019
EPA 365.1
10/31/19 11:54
AKF
pH
8.4
pH
1
1.0
1.0
9KO1038
iM 4500H+B-2011
11/01/19 16:34
JAH
Q-01
Phosphorus[7723-14-0]^
2.6
D
mg/L
5
0.12
0.50
9331010
EPA 365.4
11/07/19 14:26
AKF
Phosphorus[7723-14-O]^
2.7
D
mg/L
2
0.050
0.20
9331010
EPA 365.4
11/07/19 19:01
AKF
Specific Conductance (EC) at 25 Deg
3800
umhos/cm
1
1.0
1.0
9KO5036
SM 251OB-2011
11/05/19 15:00
JOC
C^
Sulfate as SO4 [14808-79-8]^
110
D
mg/L
10
29
50
9KO5034
EPA 300.0
11/05/19 21:32
PDK
Temperature for pH (deg. C)
22
pH
1
9KO1038
iM 4500H+B-2011
11/01/19 16:34
JAH
Q-01
Total Alkalinity as CaCO3 [471-34-1]^
1200
D
mg/L
10
140
150
9KO5022
EPA 310.2
11/05/19 16:22
AKF
Total Dissolved Solids^
2500
mg/L
1
50
50
9KO1006
SM 2540C-2011
11/01/19 15:20
JOC
Total Kjeldahl Nitrogen
3.9
mg/L
1
0.26
0.48
9131009
EPA 351.2
11/07/19 13:13
AKF
Total Nitrogen [17778-88-0]
4.6
D
mg/L
5
0.26
0.50
[CALC]
CALC
11/08/19 18:03
AKF
Total Suspended Solids^
2.5
U
mg/L
1
2.5
2.5
9KO1011
SM 2540D-2011
11/01/19 10:32
JAH
LP-03
Turbidity^
0.50
U
NTU
1
0.50
1.0
9J31006
SM 213OB-2011
10/31/19 08:45
JOC
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 25

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: RO Permeate Lab Sample ID:CC17581-03 Received: 10/30/19 09:30
Matrix: Waste Water Sampled:10/29/19 14:15 Work Order: CC17581
Project: RO Pilot Sampled By:Jelena El Barigi
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary cediFed analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
-By Notes
Mercury[7439-97-6]^
0.000750
U
mg/L
5
0.000750
0.00100
9KO4029
EPA 7470A
11/05/19 13:58
KAH
Silica (Si02) [763-18-69]^
0.3
U
mg/L
10
0.3
2.1
9KO5031
EPA 6010D
11/07/19 10:53
JDH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary cediFed analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Aluminum [7429-90-5]^
0.420
U
mg/L
10
0.420
1.00
9KO5031
EPA 6010D
11/07/19 10:53
JDH
Arsenic[7440-38-2]^
0.0760
U
mg/L
10
0.0760
0.100
9KO5031
EPA 6010D
11/07/19 10:53
JDH
Boron [7440-42-8]A
0.0570
U
mg/L
10
0.0570
0.500
9KO5031
EPA 6010D
11/07/19 10:53
JDH
Cadmium [7440-43-9]^
0.00360
U
mg/L
10
0.00360
0.0100
9KO5031
EPA 6010D
11/07/19 10:53
JDH
Calcium [7440-70-2]A
0.560
J
mg/L
10
0.390
1.00
9KO5031
EPA 6010D
11/07/19 10:53
JDH
Chromium [7440-47-3]^
0.0140
U
mg/L
10
0.0140
0.100
9KO5031
EPA 6010D
11/07/19 10:53
JDH
Copper[7440-50-8]^
0.0160
U
mg/L
10
0.0160
0.100
9KO5031
EPA 6010D
11/07/19 10:53
JDH
Iron [7439-89-6]^
0.220
U
mg/L
10
0.220
0.500
9KO5031
EPA 6010D
11/07/19 10:53
JDH
Lead [7439-92-1]^
0.0310
U
mg/L
10
0.0310
0.100
9KO5031
EPA 6010D
11/07/19 10:53
JDH
Magnesium [7439-95-4]^
0.290
U
mg/L
10
0.290
1.00
9KO5031
EPA 6010D
11/07/19 10:53
JDH
Molybdenum [7439-98-7]^
0.0250
U
mg/L
10
0.0250
0.100
9KO5031
EPA 6010D
11/07/19 10:53
JDH
Nickel[7440-02-0]^
0.0220
U
mg/L
10
0.0220
0.100
9KO5031
EPA 6010D
11/07/19 10:53
JDH
Potassium [7440-09-7]A
12.5
mg/L
10
1.50
5.00
9KO5031
EPA 6010D
11/07/19 10:53
JDH
Selenium [7782-49-2]^
0.0620
U
mg/L
10
0.0620
0.100
9KO5031
EPA 6010D
11/07/19 10:53
JDH
Silver[7440-22-4]^
0.0190
U
mg/L
10
0.0190
0.100
9KO5031
EPA 6010D
11/07/19 10:53
JDH
Sodium [7440-23-5]A
10.8
mg/L
10
4.00
5.00
9KO5031
EPA 6010D
11/07/19 10:53
JDH
Zinc[7440-66-6]^
0.0440
U
mg/L
10
0.0440
0.100
9KO5031
EPA 6010D
11/07/19 10:53
JDH
Classical Chemistry Parameters
^ - ENCO Cary cediFed analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Ammonia as N [7664-41-7]A
0.19
mg/L
1
0.045
0.10
9K12021
EPA 350.1
11/12/19 11:47
PDK
Bicarbonate (as CaCO3)[71-52-3]
28
mg/L
1
14
15
9KO8017
M 4500002 D-201
11/08/19 13:10
JAH
Carbonate (as CaCO3)[3812-32-6]
14
U
mg/L
1
14
15
9KO8017
M 4500002 D-201
11/08/19 13:10
JAH
Chemical Oxygen Demand^
10
U
mg/L
1
10
10
9KO5009
SM 5220D-2011
11/05/19 14:05
JOC
Chloride [16887-00-6]A
13
mg/L
1
2.2
5.0
9KO5034
EPA 300.0
11/05/19 21:50
PDK
Cyanide (total) [57-12-5]^
0.0049
U
mg/L
1
0.0049
0.0050
9KO6033
EPA 335.4
11/11/19 16:04
AKF
Nitrate as N [14797-55-8]
0.041
U
mg/L
1
0.041
0.10
[CALC]
EPA 353.2
11/08/19 18:05
AKF
Nitrate/Nitrite as NA
0.079
J
mg/L
1
0.041
0.10
9KO8019
EPA 353.2
11/08/19 18:05
AKF
Nitrite as N [14797-65-0]A
0.045
J
mg/L
1
0.017
0.10
9331018
EPA 353.2
10/31/19 11:33
AKF
Orthophosphate as P [1426-54-42]^
0.16
U
mg/L
1
0.16
0.50
9331019
EPA 365.1
10/31/19 11:57
AKF
pH
5.4
pH
1
1.0
1.0
9KO1038
iM 4500H+B-2011
11/01/19 16:34
JAH Q-01
Phosphorus[7723-14-0]^
0.025
U
mg/L
1
0.025
0.10
9331010
EPA 365.4
11/07/19 14:28
AKF
Specific Conductance (EC) at 25 Deg
110
umhos/cm
1
1.0
1.0
9KO5036
SM 251OB-2011
11/05/19 15:00
JOC
CA
Sulfate as SO4 [14808-79-8]^
2.9
U
mg/L
1
2.9
5.0
9KO5034
EPA 300.0
11/05/19 21:50
PDK
Temperature for pH (deg. C)
22
pH
1
9KO1038
3M 4500H+B-2011
11/01/19 16:34
JAH Q-01
Total Alkalinity as CaCO3 [471-34-1]A
28
mg/L
1
14
15
9KO5022
EPA 310.2
11/05/19 16:22
AKF
Total Dissolved Solids^
50
U
mg/L
1
50
50
9KO1006
SM 2540C-2011
11/01/19 15:20
JOC
Total Kjeldahl Nitrogen
0.26
U
mg/L
1
0.26
0.48
9J31009
EPA 351.2
11/07/19 13:15
AKF
Total Nitrogen [17778-88-0]
0.26
U
mg/L
1
0.26
0.48
[CALC]
CALC
11/08/19 18:05
AKF
Total Suspended Solids^
5.0
U
mg/L
2
5.0
5.0
9KO1011
SM 2540D-2011
11/01/19 10:32
JAH
FINAL
This report relates only
to the
sample as received by the laboratory,
and may only be reproduced
in full.
Page 8 of 25

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: RO Permeate Lab Sample ID:CC17581-03 Received: 10/30/19 09:30
Matrix: Waste Water Sampled:10/29/19 14:15 Work Order: CC17581
Project: RO Pilot Sampled By:Jelena El Barigi
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
TurbidityA 0.50 U
NTU
1
0.50
1.0
9331006
SM 213OB-2011
10/31/19 08:45
JOC
Classical Chemistry Parameters (Dissolved)
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Biochemical Oxygen DemandA 2.0 U
mg/L
1
2.0
2.0
9331007
SM 5210 B-2011
10/31/19 12:36
JOC
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 25

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: RO Reject Lab Sample ID:CC17581-04 Received: 10/30/19 09:30
Matrix: Waste Water Sampled:10/29/19 14:15 Work Order: CC17581
Project: RO Pilot Sampled By:Jelena El Barigi
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary ced1fied analyte [NC 591]
Analyte rCAS Numberl
Results
Flao
Units
DF
MOIL
P L
Batch
Method
Analyzed
-By Notes
Mercury[7439-97-6]^
0.000750
U
mg/L
5
0.000750
0.00100
9KO4029
EPA 7470A
11/05/19 14:00
KAH
Silica (Si02) [763-18-69]^
181
mg/L
10
0.3
2.1
9KO5031
EPA 6010D
11/07/19 10:55
JDH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flao
Units
DF
MOIL
P L
Batch
Method
Analyzed
By Notes
Aluminum [7429-90-5]^
0.617
J
mg/L
10
0.420
1.00
9KO5031
EPA 6010D
11/07/19 10:55
JDH
Arsenic[7440-38-2]^
0.0760
U
mg/L
10
0.0760
0.100
9KO5031
EPA 6010D
11/07/19 10:55
JDH
Boron [7440-42-8]^
0.163
J
mg/L
10
0.0570
0.500
9KO5031
EPA 6010D
11/07/19 10:55
JDH
Cadmium [7440-43-9]^
0.00360
U
mg/L
10
0.00360
0.0100
9KO5031
EPA 6010D
11/07/19 10:55
JDH
Calcium [7440-70-2]^
928
mg/L
10
0.390
1.00
9KO5031
EPA 6010D
11/07/19 10:55
JDH
Chromium [7440-47-3]^
0.0140
U
mg/L
10
0.0140
0.100
9KO5031
EPA 6010D
11/07/19 10:55
JDH
Copper[7440-50-8]^
0.0360
J
mg/L
10
0.0160
0.100
9KO5031
EPA 6010D
11/07/19 10:55
JDH
Iron [7439-89-6]^
1.41
mg/L
10
0.220
0.500
9KO5031
EPA 6010D
11/07/19 10:55
JDH
Lead [7439-92-1]^
0.0310
U
mg/L
10
0.0310
0.100
9KO5031
EPA 6010D
11/07/19 10:55
JDH
Magnesium [7439-95-4]^
50.9
mg/L
10
0.290
1.00
9KO5031
EPA 6010D
11/07/19 10:55
JDH
Molybdenum [7439-98-7]^
0.0250
U
mg/L
10
0.0250
0.100
9KO5031
EPA 6010D
11/07/19 10:55
JDH
Nickel[7440-02-0]^
0.0220
U
mg/L
10
0.0220
0.100
9KO5031
EPA 6010D
11/07/19 10:55
JDH
Potassium [7440-09-7]^
2420
mg/L
10
1.50
5.00
9KO5031
EPA 6010D
11/07/19 10:55
JDH
Selenium [7782-49-2]^
0.0620
U
mg/L
10
0.0620
0.100
9KO5031
EPA 6010D
11/07/19 10:55
JDH
Silver[7440-22-4]^
0.0190
U
mg/L
10
0.0190
0.100
9KO5031
EPA 6010D
11/07/19 10:55
JDH
Sodium [7440-23-5]^
4080
mg/L
10
4.00
5.00
9KO5031
EPA 6010D
11/07/19 10:55
JDH
Zinc[7440-66-6]^
0.0693
J
mg/L
10
0.0440
0.100
9KO5031
EPA 6010D
11/07/19 10:55
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flao
Units
DF
MOIL
P L
Batch
Method
Analyzed
By Notes
Ammonia as N [7664-41-7]^
3.2
D
mg/L
2
0.090
0.20
9K12021
EPA 350.1
11/12/19 11:49
PDK
Bicarbonate (as CaCO3)[71-52-3]
2000
mg/L
1
14
15
9KO8017
M 4500002 D-201
11/08/19 13:10
JAH
Carbonate (as CaCO3)[3812-32-6]
14
U
mg/L
1
14
15
9KO8017
M 4500002 D-201
11/08/19 13:10
JAH
Chemical Oxygen Demand
650
mg/L
2
20
20
9KO5009
SM 5220D-2011
11/05/19 14:05
JOC
Chloride [16887-00-6]^
4200
D
mg/L
100
220
500
9KO5034
EPA 300.0
11/06/19 13:09
PDK
Cyanide (total)[57-12-5]^
0.0085
mg/L
1
0.0049
0.0050
9KO6033
EPA 335.4
11/11/19 16:05
AKF
Nitrate as N [14797-55-8]
2.7
D
mg/L
2
0.082
0.20
[CALC]
EPA 353.2
11/13/19 19:41
AKF
Nitrate/Nitrite as N^
4.6
D
mg/L
2
0.082
0.20
9K13039
EPA 353.2
11/13/19 19:41
AKF
Nitrite as N [14797-65-0]^
Orthophosphate as P[1426-54-42]^
pH
Phosphorus[7723-14-O]^
Specific Conductance (EC) at 25 Deg
C^
Sulfate as SO4 [14808-79-8]^
Temperature for pH (deg. C)
Total Alkalinity as CaCO3 [471-34-1]^
Total Dissolved Solids^
Total Kjeldahl Nitrogen
Total Nitrogen [17778-88-0]
Total Suspended Solids^
1.9
mg/L
21
D
mg/L
7.5
pH
31
D
mg/L
24000
umhos/cm
6500
D
mg/L
22
pH
2000
D
mg/L
23000
mg/L
34
D
mg/L
39
D
mg/L
14
mg/L
1 0.017 0.10 9331018 EPA 353.2
5 0.80 2.5 9331019 EPA 365.1
1 1.0 1.0 9KO1038 iM 4500H+B-2011
10 0.25 1.0 9331010 EPA 365.4
1 1.0 1.0 9KO5036 SM 251OB-2011
100 290 500 9KO5034 EPA 300.0
1 9KO1038 iM 450011+13-2011
20 280 300 9K11019 EPA 310.2
1 50 50 9KO1006 SM 2540C-2011
2 0.52 0.96 9131009 EPA 351.2
2 0.52 0.96 [CALC] CALC
1.38 3.4 3.4 9KO1011 SM 2540D-2011
10/31/19 11:34 AKF
10/31/19 12:22 AKF
11/01/19 16:34 JAH Q-01
11/07/19 14:29 AKF
11/05/1915:00 JOC
11/06/19 13:09
11/01/19 16:34
11/11/19 18:34
11/01/19 15:20
11/07/19 13:17
11/13/19 19:41
11/01/19 10:32
PDK
JAH
AKF
JOC
AKF
AKF
JAH
Q-01
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 25

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ANALYTICAL RESULTS
Description: RO Reject Lab Sample ID:CC17581-04 Received: 10/30/19 09:30
Matrix: Waste Water Sampled:10/29/19 14:15 Work Order: CC17581
Project: RO Pilot Sampled By:Jelena El Barigi
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Turbidity^ 4.8 NTU 1 0.50 1.0 9331006 SM 213OB-2011 10/31/19 08:45 JOC
Description: MBBR Feed Lab Sample ID:CC17581-05 Received: 10/30/19 09:30
Matrix: Waste Water Sampled:10/29/19 14:15 Work Order: CC17581
Project: RO Pilot Sampled By:Jelena El Barigi
(Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Notes
Silica (Si02) [763-18-69]^ 34.6 mg/L 5 0.1 1.1 9KO5031 EPA 6010D 11/07/19 11:04 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 25

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 9K04029 - EPA 7470A
Blank (9K04029-BLK1) Prepared: 11/04/2019 14:53 Analyzed: 11/05/2019 12:59
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Mercury 0.000150 U 0.000200 mg/L
LCS (9K04029-BS3) Prepared: 11/04/2019 14:53 Analyzed: 11/05/2019 13:01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Mercury
0.00531
0.000200
mg/L
0.00500 106 80-120
Matrix Spike (9K04029-MSI)
Prepared: 11/04/2019 14:53 Analyzed: 11/05/2019 13:07
Source: CC14870-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Mercury
0.00510
0.000200
mg/L
0.00500 0.000150 U 102 75-125
Matrix Spike Dup (9K04029-MSD3)
Prepared: 11/04/2019 14:53 Analyzed: 11/05/2019 13:09
Source: CC14870-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Mercury
0.00502
0.000200
mg/L
0.00500 0.000150 U 100 75-125 2
25
Post Spike (9K04029-PSI)
Prepared: 11/04/2019 14:53 Analyzed: 11/05/2019 13:11
Source: CC14870-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Mercury
5.67
0.200
ug/L
5.00-0.0960 113 75-125
Batch 9K05031 - EPA 3005A
Blank (9K05031-BLKS)
Prepared: 11/05/2019 13:17 Analyzed: 11/07/2019 10:04
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Silica (Si02) 0.03 U 0.2 mg/L
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 9K05031 - EPA 3005A
Blank (9K05031-BLKS) Prepared: 11/05/2019 13:17 Analyzed: 11/07/2019 10:04
Analvte
Result
Flaq
POL
Units
Aluminum
0.0420
U
0.100
mg/L
Arsenic
0.00760
U
0.0100
mg/L
Boron
0.00570
U
0.0500
mg/L
Cadmium
0.000360
U
0.00100
mg/L
Calcium
0.0390
U
0.100
mg/L
Chromium
0.00140
U
0.0100
mg/L
Copper
0.00160
U
0.0100
mg/L
Iron
0.0220
U
0.0500
mg/L
Lead
0.00310
U
0.0100
mg/L
Magnesium
0.0290
U
0.100
mg/L
Molybdenum
0.00250
U
0.0100
mg/L
Nickel
0.00220
U
0.0100
mg/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit
Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 25

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 9KO5031 - EPA 3005A - Continued
Blank (9K05031-BLK1) Continued
Prepared: 11/05/2019 13:17 Analyzed: 11/07/2019 10:04
Spike Source %REC RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD Limit Notes
Potassium
0.150
U
0.500
mg/L
Selenium
0.00620
U
0.0100
mg/L
Silver
0.00190
U
0.0100
mg/L
Sodium
0.400
U
0.500
mg/L
Zinc
0.00440
U
0.0100
mg/L
LCS (9K05031-BS1)
Prepared: 11/05/2019 13:17 Analyzed: 11/07/2019 10:13
Spike Source
%REC RPD
Analvte
Result
Flaq POL
Units
Level Result
%REC
Limi RPD Limi Notes
Aluminum
2.07
0.100
mg/L
2.00
104
80-120
Arsenic
0.191
0.0100
mg/L
0.200
96
80-120
Boron
1.01
0.0500
mg/L
1.00
101
80-120
Cadmium
0.0200
0.00100
mg/L
0.0200
100
80-120
Calcium
1.95
0.100
mg/L
2.00
97
80-120
Chromium
0.199
0.0100
mg/L
0.200
100
80-120
Copper
0.197
0.0100
mg/L
0.200
98
80-120
Iron
0.998
0.0500
mg/L
1.00
100
80-120
Lead
0.201
0.0100
mg/L
0.200
101
80-120
Magnesium
2.10
0.100
mg/L
2.00
105
80-120
Molybdenum
0.192
0.0100
mg/L
0.200
96
80-120
Nickel
0.199
0.0100
mg/L
0.200
100
80-120
Potassium
10.3
0.500
mg/L
10.0
103
80-120
Selenium
0.199
0.0100
mg/L
0.200
100
80-120
Silver
0.204
0.0100
mg/L
0.200
102
80-120
Sodium
10.4
0.500
mg/L
10.0
104
80-120
Zinc
0.209
0.0100
mg/L
0.200
105
80-120
Matrix Spike (9K05031-MS3)
Prepared: 11/05/2019
13:17 Analyzed: 11/07/2019 10:16
Source: CC16437-08
Spike
Source
%REC RPD
An
Result
Flaa POL
Uni
Level
Result
%REC
Limits RPD Limit Notes
Aluminum
2.08
0.100
mg/L
2.00
0.0703
100
75-125
Arsenic
0.191
0.0100
mg/L
0.200
0.00760 U
95
75-125
Boron
1.01
0.0500
mg/L
1.00
0.0307
98
75-125
Cadmium
0.0188
0.00100
mg/L
0.0200
0.000360 U
94
75-125
Calcium
9.21
0.100
mg/L
2.00
7.04
109
75-125
Chromium
0.188
0.0100
mg/L
0.200
0.00327
92
75-125
Copper
0.185
0.0100
mg/L
0.200
0.00275
91
75-125
Iron
0.941
0.0500
mg/L
1.00
0.0220 U
94
75-125
Lead
0.194
0.0100
mg/L
0.200
0.00310 U
97
75-125
Magnesium
2.49
0.100
mg/L
2.00
0.487
100
75-125
Molybdenum
0.193
0.0100
mg/L
0.200
0.00695
93
75-125
Nickel
0.194
0.0100
mg/L
0.200
0.00220 U
97
75-125
Potassium
12.3
0.500
mg/L
10.0
2.40
99
75-125
Selenium
0.193
0.0100
mg/L
0.200
0.00620 U
97
75-125
Silver
0.186
0.0100
mg/L
0.200
0.00190 U
93
75-125
Sodium
55.1
0.500
mg/L
10.0
43.4
117
75-125
Zinc
0.203
0.0100
mg/L
0.200
0.00709
98
75-125
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 25

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 9K05031 - EPA 3005A - Continued
Matrix Spike Dup (9K05031-MSD3)
Prepared:
11/05/2019
13:17 Analyzed: 11/07/2019 10:19
Source: CC16437-08
Spike
Source
%REC
RPD
Analvte
Result Flaq
Q
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Aluminum
1.99
0.100
mg/L
2.00
0.0703
96
75-125
4
20
Arsenic
0.198
0.0100
mg/L
0.200
0.00760 U
99
75-125
4
20
Boron
1.01
0.0500
mg/L
1.00
0.0307
98
75-125
0.3
20
Cadmium
0.0189
0.00100
mg/L
0.0200
0.000360 U
95
75-125
0.7
20
Calcium
9.29
0.100
mg/L
2.00
7.04
113
75-125
0.9
20
Chromium
0.192
0.0100
mg/L
0.200
0.00327
94
75-125
2
20
Copper
0.190
0.0100
mg/L
0.200
0.00275
94
75-125
3
20
Iron
0.961
0.0500
mg/L
1.00
0.0220 U
96
75-125
2
20
Lead
0.192
0.0100
mg/L
0.200
0.00310 U
96
75-125
0.7
20
Magnesium
2.43
0.100
mg/L
2.00
0.487
97
75-125
3
20
Molybdenum
0.194
0.0100
mg/L
0.200
0.00695
93
75-125
0.6
20
Nickel
0.195
0.0100
mg/L
0.200
0.00220 U
97
75-125
0.3
20
Potassium
12.5
0.500
mg/L
10.0
2.40
101
75-125
1
20
Selenium
0.202
0.0100
mg/L
0.200
0.00620 U
101
75-125
4
20
Silver
0.193
0.0100
mg/L
0.200
0.00190 U
96
75-125
3
20
Sodium
55.5
0.500
mg/L
10.0
43.4
121
75-125
0.6
20
Zinc
0.216
0.0100
mg/L
0.200
0.00709
104
75-125
6
20
Post Spike (9K05031-PS1)
Prepared:
11/05/2019
13:17 Analyzed: 11/07/2019 10:21
Source: CC16437-08
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Aluminum
2.16
0.100
mg/L
2.00
0.0703
105
80-120
Arsenic
0.202
0.0100
mg/L
0.200
0.000463
101
80-120
Boron
1.06
0.0500
mg/L
1.00
0.0307
103
80-120
Cadmium
0.0200
0.00100
mg/L
0.0200
-0.000125
100
80-120
Calcium
9.04
0.100
mg/L
2.00
7.04
100
80-120
Chromium
0.197
0.0100
mg/L
0.200
0.00327
97
80-120
Copper
0.191
0.0100
mg/L
0.200
0.00275
94
80-120
Iron
0.986
0.0500
mg/L
1.00
0.00662
98
80-120
Lead
0.201
0.0100
mg/L
0.200
0.000190
100
80-120
Magnesium
2.54
0.100
mg/L
2.00
0.487
103
80-120
Molybdenum
0.202
0.0100
mg/L
0.200
0.00695
98
80-120
Nickel
0.205
0.0100
mg/L
0.200
0.000757
102
80-120
Potassium
12.8
0.500
mg/L
10.0
2.40
104
80-120
Selenium
0.208
0.0100
mg/L
0.200
0.00401
102
80-120
Silver
0.200
0.0100
mg/L
0.200
0.000202
100
80-120
Sodium
53.5
0.500
mg/L
10.0
43.4
101
80-120
Zinc
0.219
0.0100
mg/L
0.200
0.00709
106
80-120
Metals (Dissolved) by EPA 6000/7000 Series Methods
- Quality
Control
Batch 9K05028 - EPA 3005A
Blank (9K05028-BLK1) Prepared: 11/05/2019 13:09 Analyzed: 11/07/2019 11:24
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Calcium 0.0390 U 0.100 mg/L
Magnesium 29.0 U 100 ug/L
Silica (Si02) 0.03 U 0.2 mg/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 14 of 25

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QUALITY CONTROL DATA
Metals (Dissolved) by EPA 6000/7000 Series Methods - Quality Control
Batch 9K05028 - EPA 3005A - Continued
Blank (9K05028-BLK2)
Prepared: 11/05/2019 13:09 Analyzed: 11/07/2019 11:27
Spike Source %REC RPD
Analvte
Result
Flaq
Q
Units
Level Result %REC Limits RPD Limit Notes
Calcium
0.0390
U
0.100
mg/L
Magnesium
29.0
U
100
ug/L
Silica (Si02)
0.03
U
0.2
mg/L
LCS (9K05028-BS3)
Prepared: 11/05/2019 13:09 Analyzed: 11/07/2019 11:34
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Calcium
1.96
0.100
mg/L
2.00
98
80-120
Magnesium
2020
100
ug/L
2000
101
80-120
Matrix Spike (9K05028-MS1)
Prepared: 11/05/2019 13:09 Analyzed: 11/07/2019 11:36
Source: CC16437-07
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Calcium
22.5
0.100
mg/L
2.00
20.7
87
75-125
Magnesium
9620
100
ug/L
2000
7930
85
75-125
Matrix Spike Dup (9K05028-MSDI)
Prepared: 11/05/2019 13:09 Analyzed: 11/07/2019 11:39
Source: CC16437-07
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Calcium
21.9
0.100
mg/L
2.00
20.7
57
75-125 3
20
QM-07
Magnesium
9650
100
ug/L
2000
7930
86
75-125 0.4
20
Post Spike (9K05028-PSI)
Prepared: 11/05/2019 13:09 Analyzed: 11/07/2019 11:41
Source: CC16437-07
Spike
Source
%REC
RPD
Analvte
Result
Flaq
Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Calcium
22.3
0.100
mg/L
2.00
20.7
80
80-120
Magnesium
9.63
0.100
mg/L
2.00
7.93
85
80-120
Classical Chemistry Parameters - Quality Control
Batch 9131006 - NO PREP
Blank (9331006-BLKI) Prepared & Analyzed: 10/31/2019 08:45
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Turbidity 0.50 U 1.0 NTU
LCS (9331006-BSI) Prepared & Analyzed: 10/31/2019 08:45
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Turbidity 20 1.0 NTU 20.0 98 80-120
Duplicate (9333006-DUPl) Prepared & Analyzed: 10/31/2019 08:45
Source: CC17581-02
Analvte
Turbidity
Batch 031009 - Same
Result Flaq POL
0.50 U
1.0
Spike Source %REC
Units Level Result %REC Limits RPD
NTU 0.50 U
RPD
Limit Notes
25
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 15 of 25

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9J31009 - Same - Continued
Blank (9331009-BLK3) Prepared: 10/31/2019 10:45 Analyzed: 11/07/2019 12:42
Spike Source %REC RPD
Analvte Result Flag Q Units Level Result %REC Limits RPD Limit Notes
Total Kjeldahl Nitrogen 0.26 U 0.48 mg/L
LCS (9333009-BSI) Prepared: 10/31/2019 10:45 Analyzed: 11/07/2019 12:43
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
12
0.48
mg/L
12.0 103 90-110
Matrix Spike (9331009-MS1)
Prepared: 10/31/2019 10:45 Analyzed: 11/07/2019 12:49
Source: CC14900-02
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
9.1
0.48
mg/L
4.80 3.3 121 90-110
QM-07
Matrix Spike (9333009-MS2)
Prepared: 10/31/2019 10:45 Analyzed: 11/07/2019 12:54
Source: CC14780-01
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
49
D
2.4
mg/L
4.80 45 84 90-110
QM-07
Matrix Spike Dup (9333009-MSD3)
Prepared: 10/31/2019 10:45 Analyzed: 11/07/2019 12:50
Source: CC14900-02
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
8.7
0.48
mg/L
4.80 3.3 112 90-110 5
10
QM-07
Batch 9J31010 - Same
Blank (9331010-BLK1) Prepared: 10/31/2019 10:45 Analyzed: 11/07/2019 13:54
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Phosphorus 0.025 U 0.10 mg/L
Blank (9331010-BLK2) Prepared: 10/31/2019 10:45 Analyzed: 11/07/2019 18:59
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Phosphorus 0.025 U 0.10 mg/L
LCS (9333030-BSI) Prepared: 10/31/2019 10:45 Analyzed: 11/07/2019 13:55
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Phosphorus 1.6 0.10 mg/L 1.60 99 80-120
LCS (9331010-BS2) Prepared: 10/31/2019 10:45 Analyzed: 11/07/2019 19:00
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Phosphorus 1.6 0.10 mg/L 1.60 99 80-120
Matrix Spike (9333030-MS1) Prepared: 10/31/2019 10:45 Analyzed: 11/07/2019 13:59
Source: CC14900-02
Spike Source %REC RPD
Analvte Result Flag Q Units Level Result %REC Limits RPD Limit
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Notes
Page 16 of 25

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9J31010 - Same - Continued
Matrix Spike (9333030-MS3) Continued
Prepared: 10/31/2019 10:45 Analyzed: 11/07/2019 13:59
Source: CC14900-02
Spike Source %REC
RPD
Analvte
Result
Flag
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
1.8
0.10
mg/L
0.640 1.1 103 80-120
Matrix Spike Dup (9333030-MSD1)
Prepared: 10/31/2019 10:45 Analyzed: 11/07/2019 14:01
Source: CC14900-02
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
1.8
0.10
mg/L
0.640 1.1 104 80-120 0.2
25
Batch 9J31018 - NO PREP
Blank (9331018-BLK1)
Prepared: 10/31/2019 09:36 Analyzed: 10/31/2019 11:27
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
0.017
U
0.10
mg/L
LCS (9733018-BS1)
Prepared: 10/31/2019 09:36 Analyzed: 10/31/2019 11:20
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
1.0
0.10
mg/L
1.00 100 90-110
Matrix Spike (9333018-MSI)
Prepared: 10/31/2019 09:36 Analyzed: 10/31/2019 11:29
Source: CC17581-02
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
1.3
0.10
mg/L
1.00 0.27 99 90-110
Matrix Spike Dup (9333018-MSDI)
Prepared: 10/31/2019 09:36 Analyzed: 10/31/2019 11:30
Source: CC17581-02
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
1.3
0.10
mg/L
1.00 0.27 102 90-110 3
10
Batch 9.731019 - NO PREP
Blank (9331019-BLK3)
Prepared: 10/31/2019 09:40 Analyzed: 10/31/2019 11:53
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Orthophosphate as P
0.16
U
0.50
mg/L
LCS (9333019-BSI)
Prepared: 10/31/2019 09:40 Analyzed: 10/31/2019 11:52
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Orthophosphate as P
5.2
0.50
mg/L
5.00 103 90-110
Matrix Spike (9331019-MS1)
Prepared: 10/31/2019 09:40 Analyzed: 10/31/2019 11:55
Source: CC17581-02
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Orthophosphate as P
4.5
0.50
mg/L
2.00 2.6 97 90-110
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 17 of 25

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9J31019 - NO PREP - Continued
Matrix Spike Dup (9133019-MSDl) Prepared: 10/31/2019 09:40 Analyzed: 10/31/2019 11:56
Source: CC17581-02
Spike Source %REC RPD
Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes
Orthophosphate as P 4.6 0.50 mg/L 2.00 2.6 100 90-110 1 10
Batch 9K01006 - NO PREP
Blank (9K03006-BLK1) Prepared & Analyzed: 11/01/2019 15:20
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Dissolved Solids 50 U 50 mg/L
LCS (9K01006-BS3) Prepared & Analyzed: 11/01/2019 15:20
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Total Dissolved Solids
1000
50
mg/L
1000 103 80-120
Duplicate (9K03006-DUPl)
Prepared & Analyzed: 11/01/2019 15:20
Source: CC14900-01
Spike Source %REC
RPD
Analvte
Result Flaq
Q
Units
Level Result %REC Limits
RPD
Limit Notes
Total Dissolved Solids
2000
50
mg/L
2100
6
20
Duplicate (9K03006-DUP2)
Prepared & Analyzed: 11/01/2019 15:20
Source: CC14900-02
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Total Dissolved Solids
2100
50
mg/L
2200
4
20
Batch 9K01011 -NO PREP
Blank (9K03011-BLKS) Prepared & Analyzed: 11/01/2019 10:32
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Suspended Solids 2.5 U 2.5 mg/L
LCS (9K01011-BS3) Prepared & Analyzed: 11/01/2019 10:32
Spike Source %REC
RPD
Analvte
Result Flag
Q
Units
Level Result %REC Limits
RPD
Limit
Notes
Total Suspended Solids
98
2.5
mg/L
100 98 80-120
Duplicate (9K03011-DUPi)
Prepared & Analyzed: 11/01/2019 10:32
Source: CC14647-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Total Suspended Solids
360
100
mg/L
430
18
20
Duplicate (9K01011-DUP2)
Prepared & Analyzed: 11/01/2019 10:32
Source: CC14780-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Total Suspended Solids
35
25
mg/L
34
3
20
Batch 9K01038 - NO PREP
FINAL
This report relates only to the sample as received by the
laboratory, and may only be reproduced in full.
Page 18 of 25

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9K01038 - NO PREP - Continued
LCS (9K01038-BS3) Prepared & Analyzed: 11/01/2019 16:34
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
pH
7.1
1.0
pH
7.00 101 99-101
Duplicate (9K03038-DUPi)
Prepared & Analyzed: 11/01/2019 16:34
Source: CC17581-02
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
pH
8.3
1.0
pH
8.4 2
25
Batch 9K05009 - Same
Blank (9K05009-BLKS) Prepared: 11/05/2019 10:29 Analyzed: 11/05/2019 14:05
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Chemical Oxygen Demand 10 U 10 mg/L
LCS (9K05009-BS3) Prepared: 11/05/2019 10:29 Analyzed: 11/05/2019 14:05
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Chemical Oxygen Demand
510
10
mg/L
500
101
90-110
Matrix Spike (9K05009-MSi)
Prepared: 11/05/2019 10:29 Analyzed: 11/05/2019 14:05
Source: CC12553-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Chemical Oxygen Demand
530
10
mg/L
526
18
96
90-110
Matrix Spike Dup (9K05009-MSD3)
Prepared: 11/05/2019 10:29 Analyzed: 11/05/2019 14:05
Source: CC12553-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Chemical Oxygen Demand
540
10
mg/L
526
18
99
90-110 3
5
Batch 9K05022 - NO PREP
Blank (9K05022-BLK1) Prepared: 11/05/2019 11:35 Analyzed: 11/05/2019 16:10
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Alkalinity as CaCO3 14 U 15 mg/L
LCS (9K05022-BS3) Prepared: 11/05/2019 11:35 Analyzed: 11/05/2019 16:10
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Total Alkalinity as CaCO3
100
15
mg/L
100
100
80-120
Matrix Spike (9K05022-MSI)
Prepared: 11/05/2019 11:35 Analyzed: 11/05/2019 16:12
Source: CC16612-15
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Total Alkalinity as CaCO3
48
15
mg/L
37.8
14 U
128
80-120
QM-07
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 19 of 25

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9K05022 - NO PREP - Continued
Matrix Spike Dup (9K05022-MSD3) Prepared: 11/05/2019 11:35 Analyzed: 11/05/2019 16:12
Source: CC16612-15
Spike Source %REC RPD
Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes
Total Alkalinity as CaCO3 49 15 mg/L 37.8 14 U 130 80-120 2 25 QM-07
Batch 9K05034 - NO PREP
Blank (9K05034-BLK1) Prepared: 11/05/2019 13:35 Analyzed: 11/05/2019 15:57
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Chloride 2.2 U 5.0 mg/L
Sulfate as SO4 2.9 U 5.0 mg/L
LCS (9K05034-BS3) Prepared: 11/05/2019 13:35 Analyzed: 11/05/2019 16:14
Spike Source %REC
RPD
Analvte
Result
Flaq
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Chloride
50
5.0
mg/L
50.0 99 90-110
Sulfate as SO4
48
5.0
mg/L
50.0 96 90-110
Matrix Spike (9K05034-MSI)
Prepared: 11/05/2019 13:35 Analyzed: 11/05/2019 16:50
Source: CC16612-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chloride
410
E
5.0
mg/L
20.0 390 101 90-110
Sulfate as SO4
18
5.0
mg/L
20.0 2.9 U 91 90-110
Matrix Spike (9K05034-MS2)
Prepared: 11/05/2019 13:35 Analyzed: 11/05/2019 17:43
Source: CC16612-02
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chloride
180
50
mg/L
200 22 U 89 90-110
QM-07
Sulfate as SO4
170
50
mg/L
200 29 U 87 90-110
QM-07
Matrix Spike Dup (9K05034-MSD3)
Prepared: 11/05/2019 13:35 Analyzed: 11/05/2019 17:07
Source: CC16612-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chloride
410
E
5.0
mg/L
20.0 390 100 90-110 0.04
10
Sulfate as SO4
19
5.0
mg/L
20.0 2.9 U 93 90-110 1
10
Batch 9K05036 - NO PREP
Blank (9K05036-BLKS) Prepared & Analyzed: 11/05/2019 15:00
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Specific Conductance (EC) at 25 Deg C 1.0 U 1.0 umhos/cm
LCS (9K05036-BS3) Prepared & Analyzed: 11/05/2019 15:00
Spike Source %REC RPD
Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes
Specific Conductance (EC) at 25 Deg C 720 1.0 umhos/cm 705 102 90-110
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 20 of 25

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9K05036 - NO PREP - Continued
Duplicate (9K05036-DUPl)
Prepared & Analyzed: 11/05/2019 15:00
Source: CC14900-03
Spike Source %REC
RPD
Analvte
Result Flag
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Specific Conductance (EC) at 25 Deg C
3400
1.0
umhos/cm
3400
0.9
25
Duplicate (9K05036-DUP2)
Prepared & Analyzed: 11/05/2019 15:00
Source: CC14901-03
Spike Source %REC
RPD
Analvte
Result Flag
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Specific Conductance (EC) at 25 Deg C
3400
1.0
umhos/cm
3400
0.6
25
Batch 9K06033 - Same
Blank (9K06033-BLKS) Prepared: 11/06/2019 14:37 Analyzed: 11/11/2019 15:48
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Cyanide (total) 0.0049 U 0.0050 mg/L
LCS (9K06033-BS3) Prepared: 11/06/2019 14:37 Analyzed: 11/11/2019 15:50
Spike
Source
%REC
RPD
Analvte
Result
Flag Q
Units
Level
Result
%REC
Limits RPD
Limit Notes
Cyanide (total)
0.14
0.0050
mg/L
0.150
92
90-110
Matrix Spike (9K06033-MSi)
Prepared: 11/06/2019 14:37 Analyzed: 11/11/2019 15:53
Source: CC17525-01
Spike
Source
%REC
RPD
Analvte
Result
Flag POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Cyanide (total)
0.14
0.0050
mg/L
0.150
0.0049 U
94
90-110
Matrix Spike Dup (9K06033-MSD3)
Prepared: 11/06/2019 14:37 Analyzed: 11/11/2019 15:55
Source: CC17525-01
Spike
Source
%REC
RPD
Analvte
Result
Flag POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Cyanide (total)
0.14
0.0050
mg/L
0.150
0.0049 U
91
90-110 3
10
Batch 9K08019 - NO PREP
Blank (9K08019-BLK1) Prepared: 11/08/2019 13:26 Analyzed: 11/08/2019 17:31
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Nitrate/Nitrite as N 0.041 U 0.10 mg/L
LCS (9K08019-BS3) Prepared: 11/08/2019 13:26 Analyzed: 11/08/2019 17:33
Spike
Source
%REC
RPD
Analvte
Result Flag
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Nitrate/Nitrite as N
1.3
0.10
mg/L
1.25
102
90-110
Matrix Spike (9K08019-MSl)
Prepared: 11/08/2019 13:26 Analyzed: 11/08/2019 17:36
Source: CC16334-01
Spike
Source
%REC
RPD
Analvte
Result Flag
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Nitrate/Nitrite as N
0.71
0.10
mg/L
0.521
0.16
106
90-110
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 21 of 25

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9K08019 - NO PREP - Continued
Matrix Spike (9K08019-MS2)
Prepared: 11/08/2019 13:26 Analyzed: 11/08/2019 17:41
Source: CC16334-02
Spike Source %REC
RPD
Analvte
Result Flag
Q
Units
Level Result %REC Limits RPD
Limit Notes
Nitrate/Nitrite as N
0.76
0.10
mg/L
0.521 0.19 110 90-110
Matrix Spike Dup (9K08019-MSD3)
Prepared: 11/08/2019 13:26 Analyzed: 11/08/2019 17:38
Source: CC16334-01
Spike Source %REC
RPD
Analvte
Result Flag
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrate/Nitrite as N
0.70
0.10
mg/L
0.521 0.16 104 90-110 2
10
Batch 9K11019 - NO PREP
Blank (9K13019-BLKS)
Prepared: 11/11/2019 10:23 Analyzed: 11/11/2019 18:29
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Total Alkalinity as CaCO3 14 U 15 mg/L
LCS (9K31019-BS3) Prepared: 11/11/2019 10:23 Analyzed: 11/11/2019 18:30
Spike
Source
%REC
RPD
Analvte
Result Flag
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Total Alkalinity as CaCO3
98
15
mg/L
100
98
80-120
Matrix Spike (9K31019-MSi)
Prepared: 11/11/2019 10:23 Analyzed: 11/11/2019 18:31
Source: CC17679-03
Spike
Source
%REC
RPD
Analvte
Result Flag
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Total Alkalinity as CaCO3
67
15
mg/L
37.8
23
119
80-120
Matrix Spike Dup (9K11019-MSD3)
Prepared: 11/11/2019 10:23 Analyzed: 11/11/2019 18:32
Source: CC17679-03
Spike
Source
%REC
RPD
Analvte
Result Flag
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Total Alkalinity as CaCO3
69
15
mg/L
37.8
23
124
80-120 3
25
QM-07
Batch 9K12021 - NO PREP
Blank (9K12021-BLK1) Prepared: 11/12/2019 09:26 Analyzed: 11/12/2019 11:02
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Ammonia as N 0.045 U 0.10 mg/L
LCS (9K32021-BS3) Prepared: 11/12/2019 09:26 Analyzed: 11/12/2019 11:03
Spike
Source
%REC
RPD
Analvte
Result Flag
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Ammonia as N
0.98
0.10
mg/L
1.01
97
90-110
Matrix Spike (9K32021-MS1)
Prepared: 11/12/2019 09:26 Analyzed: 11/12/2019 11:12
Source: CC12661-01
Spike
Source
%REC
RPD
Analvte
Result Flag
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Ammonia as N
0.44
0.10
mg/L
0.393
0.059
98
90-110
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 22 of 25

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9K12021 - NO PREP - Continued
Matrix Spike (9K32021-MS2)
Prepared: 11/12/2019 09:26 Analyzed: 11/12/2019 11:17
Source: CC16334-01
Spike Source %REC
RPD
Analvte
Result Flag
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
0.63
0.10
mg/L
0.393 0.30 86 90-110
QM-07
Matrix Spike Dup (9K32021-MSD3)
Prepared: 11/12/2019 09:26 Analyzed: 11/12/2019 11:14
Source: CC12661-01
Spike Source %REC
RPD
Analvte
Result Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
0.39
0.10
mg/L
0.393 0.059 84 90-110 13
10
QM-07,
QM-11
Batch 9K13039 - NO PREP
Blank (9K13039-BLKS) Prepared: 11/13/2019 14:37 Analyzed: 11/13/2019 19:05
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Nitrate/Nitrite as N 0.041 U 0.10 mg/L
LCS (9K33039-BS3) Prepared: 11/13/2019 14:37 Analyzed: 11/13/2019 19:06
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
1.3
0.10
mg/L
1.25 101 90-110
Matrix Spike (9K13039-MS3)
Prepared: 11/13/2019 14:37 Analyzed: 11/13/2019 19:10
Source: CC14792-01
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
0.41
0.10
mg/L
0.521 0.10 59 90-110
QM-07
Matrix Spike (9K33039-MS2)
Prepared: 11/13/2019 14:37 Analyzed: 11/13/2019 19:15
Source: CC14791-01
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
0.57
0.10
mg/L
0.521 0.14 82 90-110
QM-07
Matrix Spike Dup (9K33039-MSD3)
Prepared: 11/13/2019 14:37 Analyzed: 11/13/2019 19:12
Source: CC14792-01
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
0.41
0.10
mg/L
0.521 0.10 60 90-110 0.7
10
QM-07
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 23 of 25

(� �Eo
www.encolabs.com
FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
LP-03 Sample amount received by the laboratory did not meet minimum method requirements for analysis.
Q-01 Analysis performed outside of method - specified holding time.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 24 of 25

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Sample Preservation Verification rig
ENCO Cary CSNI
Work Order: CC17581 Project: RO Pilot
Client: Novozymes North America (N0008) Project #: [none]
Logged ln: 30-Oct-19 10:14 Logged By: David E. Wilder
Preservation Check Performed By: Date/Time: l��� ��•
CC17581-01
Cant Type Pres (pH) pH Checked / DateMme
YP Requirement In Control PH Adjusted Adjusted Reagent UsedlComments
C 250mLP+HNO3 <2 Y I& NA N I NA 0 f 0, -4� �(
CC17581-02
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted DatelTme
Adjusted
Reagent Used/Comments
B
250mLP+HNO3
<2
'Y 1 N / NA
Y N / NA
C
250mLP+NaOH
?12
1 N! NA
Y/ I NA
E
500mLP+H2SO4
<2
/ N I NA
YIM / ! NA
CC17581-03
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted Date/Time
Adjusted
Reagent Used/Comments
B
250mLP+HNO3
2
61/ N / NA
Y 1 t� / NA
C
250mLP+NaOH
>12
60 / N / NA
Y l�t�l / NA
E
500mLP+H2SO4
<2
7 N / NA
Y / 0 / NA
C C 17581-04
Cont
Type
Pres (pH)
Requirement
pH Checked /
in Control
pH Adjusted ; DateMme
' Adjusted
Reagent used/comments
B
250mLP+HNO3
<2
Y )/ NA
W/ N ! NA 17-30 10=b
.-\ZM(_ NQL2
C-
250mLP+NaOH
>12
Y /CN)/ NA
/ N / NA to ( tgM
joh,_
E
500mLP+H2SO4
<2
/ N / NA
Y / / NA
Reagent Name ID
1
r'-1
J
pH Strip ID. Cq-�0:53__;L
C:IELMNT1Print%wko_PreservationCheck. rpt
Reaclent Name ID Reacient Name ID
31 1 5
41 6
Page 1 c

2�SENCO Laboratories
9g
Accurate. Timely. Respousive. luuavative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Tuesday, November 26, 2019
Novozymes North America (N0008)
Attn: Scott Creech
77 Perry Chapel Church Road
Franklinton, NC 27525
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: RO Pilot
ENCO Workorder(s): CC17679
Dear Scott Creech,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, November 5, 2019.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
O"6XLC'=-:�CA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 28

(� �Eo
www.encolabs.com
SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: MBBR Feed
Lab ID: CC17679-01
Sampled: 11/04/19 16:30
Received: 11/05/19 09:36
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(sl
EPA 6010D
EPA 3005A
05/02/20
11/08/19 15:01
11/13/19 13:16
SM 5210 B-2011
NO PREP
11/06/19 16:30
11/06/19 10:32
11/06/19 10:32
Client ID: RO Feed
Lab ID: CC17679-02
Sampled: 11/04/19 16:30
Received: 11/05/19 09:36
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
CALC
[CALC]
12/02/19
11/18/19 13:30
11/19/19 11:38
EPA 300.0
NO PREP
12/02/19
11/07/19 13:14
11/08/19 00:19
EPA 310.2
NO PREP
11/18/19
11/11/19 10:23
11/11/19 18:34
EPA 335.4
Same
11/18/19
11/08/19 09:27
11/11/19 17:23
EPA 350.1
NO PREP
12/02/19
11/15/19 15:02
11/15/19 15:02
EPA 351.2
Same
12/02/19
11/06/19 10:13
11/07/19 16:47
EPA 353.2
NO PREP
11/06/19 16:30
11/05/19 15:37
11/05/19 19:09
EPA 353.2
[CALC]
11/06/19 16:30
11/18/19 13:30
11/19/19 11:38
EPA 365.1
NO PREP
11/06/19 16:30
11/05/19 18:16
11/05/19 18:16
EPA 365.4
Same
12/02/19
11/06/19 10:13
11/07/19 18:16
EPA 6010D
EPA 3005A
05/02/20
11/08/19 15:01
11/13/19 13:19
EPA 7470A
EPA 7470A
12/02/19
11/06/19 16:23
11/08/19 13:23
SM 213OB-2011
NO PREP
11/06/19 16:30
11/05/19 15:49
11/05/19 15:49
SM 251OB-2011
NO PREP
12/02/19
11/05/19 15:00
11/05/19 15:00
SM 254OC-2011
NO PREP
11/11/19
11/08/19 10:14
11/08/19 10:14
SM 2540D-2011
NO PREP
11/11/19
11/07/19 14:02
11/07/19 14:02
SM 4500002 D-2011
NO PREP
07/30/22
11/13/19 14:31
11/13/19 14:31
SM 4500H+B-2011
NO PREP
11/04/19 16:44
11/11/19 12:05
11/11/19 12:05
SM 5220D-2011
Same
12/02/19
11/08/19 09:03
11/08/19 15:40
Client ID: RO Feed
Lab ID: CC17679-02RE1
Sampled: 11/04/19 16:30
Received: 11/05/19 09:36
Parameter
Preparation
Hold Date/Time(sl
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 300.0
NO PREP
12/02/19
11/07/19 13:14
11/08/19 00:37
Client ID: RO Feed
Lab ID: CC17679-02RE2
Sampled: 11/04/19 16:30
Received: 11/05/19 09:36
Parameter
Preparation
Hold Date/Time(sl
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 353.2
NO PREP
12/02/19
11/18/19 13:30
11/19/19 11:38
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 28

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www.encolabs.com
SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: RO Permeate
Lab ID: CC17679-03
Sampled: 11/04/19 16:30
Received: 11/05/19
09:36
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
CALC
[CALC]
12/02/19
11/18/19
13:30
11/19/19
10:46
EPA 300.0
NO PREP
12/02/19
11/07/19
13:14
11/08/19
00:54
EPA 310.2
NO PREP
11/18/19
11/11/19
10:23
11/11/19
18:30
EPA 335.4
Same
11/18/19
11/08/19
09:27
11/11/19
17:24
EPA 350.1
NO PREP
12/02/19
11/14/19
19:25
11/14/19
19:25
EPA 351.2
Same
12/02/19
11/06/19
10:13
11/07/19
16:49
EPA 353.2
NO PREP
11/06/19
16:30
11/05/19
15:37
11/05/19
18:40
EPA 353.2
[CALC]
11/06/19
16:30
11/18/19
13:30
11/19/19
10:46
EPA 365.1
NO PREP
11/06/19
16:30
11/05/19
18:18
11/05/19
18:18
EPA 365.4
Same
12/02/19
11/06/19
10:13
11/07/19
18:17
EPA 6010D
EPA 3005A
05/02/20
11/08/19
15:01
11/13/19
13:22
EPA 7470A
EPA 7470A
12/02/19
11/06/19
16:23
11/08/19
13:25
SM 213OB-2011
NO PREP
11/06/19
16:30
11/05/19
15:49
11/05/19
15:49
SM 251OB-2011
NO PREP
12/02/19
11/05/19
15:00
11/05/19
15:00
SM 2540C-2011
NO PREP
11/11/19
11/08/19
10:14
11/08/19
10:14
SM 254OD-2011
NO PREP
11/11/19
11/07/19
14:02
11/07/19
14:02
SM 4500002 D-2011
NO PREP
07/30/22
11/13/19
14:31
11/13/19
14:31
SM 4500H+B-2011
NO PREP
11/04/19
16:44
11/11/19
12:05
11/11/19
12:05
SM 5210 B-2011
NO PREP
11/06/19
16:30
11/06/19
10:32
11/06/19
10:32
SM 5220D-2011
Same
12/02/19
11/08/19
09:03
11/08/19
15:40
Client ID: RO Permeate
Lab ID: CC17679-03RE1
Sampled: 11/04/19 16:30
Received: 11/05/19
09:36
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 353.2
NO PREP
12/02/19
11/18/19
13:30
11/19/19
10:46
Client ID: RO Reject
Lab ID: CC17679-04
Sampled: 11/04/19 16:30
Received: 11/05/19
09:36
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
CALC
[CALC]
12/02/19
11/18/19
13:30
11/19/19
10:55
EPA 310.2
NO PREP
11/18/19
11/05/19
11:35
11/05/19
16:24
EPA 335.4
Same
11/18/19
11/08/19
09:27
11/11/19
17:26
EPA 351.2
Same
12/02/19
11/06/19
10:13
11/07/19
16:50
EPA 353.2
[CALC]
11/06/19
16:30
11/18/19
13:30
11/19/19
10:55
EPA 365.1
NO PREP
11/06/19
16:30
11/05/19
19:18
11/05/19
19:18
EPA 6010D
EPA 3005A
05/02/20
11/08/19
15:01
11/13/19
13:25
EPA 7470A
EPA 7470A
12/02/19
11/06/19
16:23
11/08/19
13:27
SM 213OB-2011
NO PREP
11/06/19
16:30
11/05/19
15:49
11/05/19
15:49
SM 251OB-2011
NO PREP
12/02/19
11/05/19
15:00
11/05/19
15:00
SM 254OC-2011
NO PREP
11/11/19
11/08/19
10:14
11/08/19
10:14
SM 254OD-2011
NO PREP
11/11/19
11/07/19
14:02
11/07/19
14:02
SM 4500002 D-2011
NO PREP
07/30/22
11/13/19
14:31
11/13/19
14:31
SM 4500H+B-2011
NO PREP
11/04/19
16:44
11/11/19
12:05
11/11/19
12:05
SM 5220D-2011
Same
12/02/19
11/08/19
09:03
11/08/19
15:40
Client ID: RO Reject
Lab ID: CC17679-04RE1
Sampled: 11/04/19 16:30
Received: 11/05/19
09:36
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 300.0
NO PREP
12/02/19
11/26/19
00:20
11/26/19
00:20
EPA 350.1
NO PREP
12/02/19
11/15/19
09:55
11/15/19
09:55
EPA 353.2
NO PREP
11/06/19
16:30
11/13/19
10:56
11/13/19
12:16
EPA 365.4
Same
12/02/19
11/06/19
10:13
11/08/19
14:41
EPA 6010D
EPA 3005A
05/02/20
11/08/19
15:01
11/13/19
16:05
Client ID: RO Reject
Lab ID: CC17679-04RE2
Sampled: 11/04/19 16:30
Received: 11/05/19
09:36
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 353.2
NO PREP
12/02/19
11/18/19
13:30
11/19/19
10:55
FINAL
This report relates only to the sample
as received by the laboratory, and may only be reproduced in full.
Page 3 of 28

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www.encolabs.com
SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: MBBR Feed Lab ID: CC17679-05 Sampled: 11/04/19 16:30 Received: 11/05/19 09:36
Parameter Preparation Hold Date/Time(s)
EPA 6010D EPA 3005A 05/02/20
Prep Date/Time(s) Analysis Date/Time(s)
11/08/19 15:01 11/13/19 13:28
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 28

0Nk"q09
www.encolabs.com
SAMPLE DETECTION SUMMARY
Client ID: MBBR Feed
Lab ID:
CC17679-01
Analvte
Results
Flag
MDL
POLL
Units
Method
Notes
Biochemical Oxygen Demand - Dissolved
6.4
2.0
2.0
mg/L
SM 5210 B-2011
Calcium - Dissolved
85.7
0.0390
0.100
mg/L
EPA 6010D
Magnesium - Dissolved
5740
29.0
100
ug/L
EPA 6010D
Silica (Si02) - Dissolved
19.6
0.03
0.2
mg/L
EPA 6010D
Client ID: RO Feed
Lab ID:
CC17679-02
Anal a
Results
Flag
MDL
Q
Units
Method
Notes
Ammonia as N
0.80
0.045
0.10
mg/L
EPA 350.1
Bicarbonate (as CaCO3)
1100
14
15
mg/L
SM 45000O2 D-2011
Boron- Total
0.0356
J
0.00570
0.0500
mg/L
EPA 6010D
Calcium - Total
85.4
0.0390
0.100
mg/L
EPA 6010D
Carbonate (as CaCO3)
20
14
15
mg/L
SM 45000O2 D-2011
Chemical Oxygen Demand
73
10
10
mg/L
SM 5220D-2011
Copper - Total
0.00290
J
0.00160
0.0100
mg/L
EPA 6010D
Iron - Total
0.0519
0.0220
0.0500
mg/L
EPA 6010D
Magnesium - Total
5.63
0.0290
0.100
mg/L
EPA 6010D
Nitrate as N
27
D
2.0
4.8
mg/L
EPA 353.2
Nitrite as N
25
D
0.45
2.7
mg/L
EPA 353.2
Orthophosphate as P
7.2
B
0.16
0.50
mg/L
EPA 365.1
QB-01
PH
8.3
1.0
1.0
pH
SM 4500H+B-2011
Q-01
Phosphorus
8.0
D
0.12
0.50
mg/L
EPA 365.4
Potassium - Total
443
0.150
0.500
mg/L
EPA 6010D
Silica (Si02) - Total
19.8
0.03
0.2
mg/L
EPA 6010D
Sodium - Total
516
0.400
0.500
mg/L
EPA 6010D
Specific Conductance (EC) at 25 Deg C
3800
1.0
1.0
umhos/cm
SM 251OB-2011
Sulfate as SO4
150
D
5.8
10
mg/L
EPA 300.0
Temperature for pH (deg. C)
14
pH
SM 4500H+B-2011
Q-01
Total Alkalinity as CaCO3
1100
D
140
150
mg/L
EPA 310.2
Total Dissolved Solids
2400
50
50
mg/L
SM 2540C-2011
Total Kjeldahl Nitrogen
3.7
0.26
0.48
mg/L
EPA 351.2
Total Nitrogen
55
D
2.0
4.8
mg/L
CALC
I Client ID: RO Feed Lab ID: CC17679-02RE1
Anal a
Results
Flag
MDL
4
Units
Method Notes
Chloride
420
D
22
50
mg/L
EPA 300.0
Client ID: RO Feed
Lab ID:
CC17679-02RE2
Anal a
Results
Flag
MDL
POLL
Units
Method Notes
Nitrate/Nitrite as N
52
D
2.0
4.8
mg/L
EPA 353.2
Client ID: RO Permeate
Lab ID:
CC17679-03
Anal a
Results
Flag
MDL
4
Units
Method
Notes
Ammonia as N
0.30
0.045
0.10
mg/L
EPA 350.1
Bicarbonate (as CaCO3)
23
14
15
mg/L
SM 45000O2 D-2011
Boron - Total
0.0202
J
0.00570
0.0500
mg/L
EPA 6010D
Calcium - Total
0.393
0.0390
0.100
mg/L
EPA 6010D
Chemical Oxygen Demand
15
10
10
mg/L
SM 5220D-2011
Chloride
9.4
2.2
5.0
mg/L
EPA 300.0
Nitrate as N
2.8
D
0.20
0.50
mg/L
EPA 353.2
Nitrite as N
2.9
D
0.084
0.50
mg/L
EPA 353.2
Orthophosphate as P
0.27
JB
0.16
0.50
mg/L
EPA 365.1
J-01
PH
7.8
1.0
1.0
pH
SM 4500H+B-2011
Q-01
Potassium - Total
23.5
0.150
0.500
mg/L
EPA 6010D
Silica (Si02) - Total
0.2
0.03
0.2
mg/L
EPA 6010D
Sodium - Total
14.1
0.400
0.500
mg/L
EPA 6010D
Specific Conductance (EC) at 25 Deg C
140
1.0
1.0
umhos/cm
SM 251OB-2011
Temperature for pH (deg. C)
14
pH
SM 4500H+B-2011
Q-01
Total Alkalinity as CaCO3
23
14
15
mg/L
EPA 310.2
Total Dissolved Solids
94
50
50
mg/L
SM 2540C-2011
Total Nitrogen
5.7
D
0.26
0.50
mg/L
CALC
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 28

(� �Eo
www.encolabs.com
SAMPLE DETECTION SUMMARY
Client ID: RO Permeate
Lab ID:
CC17679-03RE3
Anala
Results
Flaa
MDL
4
Units
Method
Notes
Nitrate/Nitrite as N
5.7
D
0.20
0.50
mg/L
EPA 353.2
Client ID: RO Reject
Lab ID:
CC17679-04
Anala
Results
Flaa
MDL
4
Units
Method
Notes
Aluminum - Total
0.267
0.0420
0.100
mg/L
EPA 6010D
Bicarbonate (as CaCO3)
2000
14
15
mg/L
SM 4500002 D-2011
Boron - Total
0.139
0.00570
0.0500
mg/L
EPA 6010D
Chemical Oxygen Demand
550
20
20
mg/L
SM 5220D-2011
Chromium - Total
0.00940
1
0.00140
0.0100
mg/L
EPA 6010D
Copper - Total
0.0140
0.00160
0.0100
mg/L
EPA 6010D
Cyanide (total)
0.041
0.0049
0.0050
mg/L
EPA 335.4
Iron - Total
0.398
0.0220
0.0500
mg/L
EPA 6010D
Magnesium - Total
44.1
0.0290
0.100
mg/L
EPA 6010D
Molybdenum - Total
0.00599
1
0.00250
0.0100
mg/L
EPA 6010D
Nickel - Total
0.0141
0.00220
0.0100
mg/L
EPA 6010D
Nitrate as N
270
D
8.2
20
mg/L
EPA 353.2
Orthophosphate as P
52
BD
4.0
12
mg/L
EPA 365.1
QB-01
pH
7.2
1.0
1.0
pH
SM 4500H+B-2011
Q-01
Silica (Si02) - Total
177
0.03
0.2
mg/L
EPA 6010D
Specific Conductance (EC) at 25 Deg C
25000
1.0
1.0
umhos/cm
SM 251OB-2011
Temperature for pH (deg. C)
15
pH
SM 4500H+B-2011
Q-01
Total Alkalinity as CaCO3
2000
D
140
150
mg/L
EPA 310.2
Total Dissolved Solids
20000
50
50
mg/L
SM 2540C-2011
Total Kjeldahl Nitrogen
19
D
2.6
4.8
mg/L
EPA 351.2
Total Nitrogen
440
D
8.2
20
mg/L
CALC
Total Suspended Solids
4.0
2.5
2.5
mg/L
SM 2540D-2011
Turbidity
7.5
0.50
1.0
NTU
SM 213OB-2011
Zinc - Total
0.0226
0.00440
0.0100
mg/L
EPA 6010D
Client ID: RO Reject
Lab ID:
CC17679-04RE3
Anala
Results
Flaa
MDL
4
Units
Method
Notes
Ammonia as N
5.3
D
0.22
0.50
mg/L
EPA 350.1
Calcium - Total
719
D
0.390
1.00
mg/L
EPA 6010D
Chloride
3200
D
220
500
mg/L
EPA 300.0
Nitrite as N
150
BD
1.3
8.0
mg/L
EPA 353.2
Q-01
Phosphorus
74
D
1.2
5.0
mg/L
EPA 365.4
Potassium - Total
3450
D
1.50
5.00
mg/L
EPA 6010D
Sodium - Total
4120
D
4.00
5.00
mg/L
EPA 6010D
Sulfate as SO4
6200
D
290
500
mg/L
EPA 300.0
Client ID: RO Reject
Lab ID:
CC17679-04RE2
Anala
Results
Flaa
MDL
4
Units
Method
Notes
Nitrate/Nitrite as N
420
D
8.2
20
mg/L
EPA 353.2
Client ID: MBBR Feed Lab ID: CC17679-05
Anala Results Flaa MDL 4 Units Method Notes
Silica (Si02) - Total 28.3 0.03 0.2 mg/L EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 28

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www.encolabs.com
ANALYTICAL RESULTS
Description: MBBR Feed Lab Sample ID:CC17679-01 Received: 11/05/19 09:36
Matrix: Waste Water Sampled:11/04/19 16:30 Work Order: CC17679
Project: RO Pilot Sampled By: Scott Creech
Metals (Dissolved) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flao
Units
DF
MOIL
P L
Batch
Method
Analyzed
By Notes
Calcium [7440-70-2]^ 85.7
mg/L
1
0.0390
0.100
9KO8026
EPA 6010D
11/13/19 13:16
JDH
Magnesium [7439-95-4]^ 5740
ug/L
1
29.0
100
9KO8026
EPA 6010D
11/13/19 13:16
JDH
Silica (Si02) [763-18-69]^ 19.6
mg/L
1
0.03
0.2
9KO8026
EPA 6010D
11/13/19 13:16
JDH
Classical Chemistry Parameters (Dissolved)
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flao
Units
OF
MOIL
P L
Batch
Method
Analyzed
By Notes
Biochemical Oxygen Demand 6.4
mg/L
1
2.0
2.0
9KO6007
SM 5210 B-2011
11/06/19 10:32
JOC
Description: RO Feed Lab Sample ID:CC17679-02 Received: 11/05/19 09:36
Matrix: Waste Water Sampled:11/04/19 16:30 Work Order: CC17679
Project: RO Pilot Sampled By: Scott Creech
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MOIL
P L
Batch
Method
Analyzed
By
Notes
Mercury[7439-97-6]^
0.000750
U
mg/L
5
0.000750
0.00100
9KO6050
EPA 7470A
11/08/19 13:23
KAH
Silica (Si02) [763-18-69]^
19.8
mg/L
1
0.03
0.2
9KO8026
EPA 6010D
11/13/19 13:19
JDH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MOIL
P L
Batch
Method
Analyzed
By
Notes
Aluminum [7429-90-5]^
0.0420
U
mg/L
1
0.0420
0.100
9KO8026
EPA 6010D
11/13/19 13:19
JDH
Arsenic[7440-38-2]^
0.00760
U
mg/L
1
0.00760
0.0100
9KO8026
EPA 6010D
11/13/19 13:19
JDH
Boron [7440-42-8]^
0.0356
J
mg/L
1
0.00570
0.0500
9KO8026
EPA 6010D
11/13/19 13:19
JDH
Cadmium [7440-43-9]^
0.000360
U
mg/L
1
0.000360
0.00100
9KO8026
EPA 6010D
11/13/19 13:19
JDH
Calcium [7440-70-2]^
85.4
mg/L
1
0.0390
0.100
9KO8026
EPA 6010D
11/13/19 13:19
JDH
Chromium [7440-47-3]^
0.00140
U
mg/L
1
0.00140
0.0100
9KO8026
EPA 6010D
11/13/19 13:19
JDH
Copper[7440-50-8]^
0.00290
J
mg/L
1
0.00160
0.0100
9KO8026
EPA 6010D
11/13/19 13:19
JDH
Iron [7439-89-6]^
0.0519
mg/L
1
0.0220
0.0500
9KO8026
EPA 6010D
11/13/19 13:19
JDH
Lead [7439-92-1]^
0.00310
U
mg/L
1
0.00310
0.0100
9KO8026
EPA 6010D
11/13/19 13:19
JDH
Magnesium [7439-95-4]^
5.63
mg/L
1
0.0290
0.100
9KO8026
EPA 6010D
11/13/19 13:19
JDH
Molybdenum [7439-98-7]^
0.00250
U
mg/L
1
0.00250
0.0100
9KO8026
EPA 6010D
11/13/19 13:19
JDH
Nickel[7440-02-0]^
0.00220
U
mg/L
1
0.00220
0.0100
9KO8026
EPA 6010D
11/13/19 13:19
JDH
Potassium [7440-09-7]^
443
mg/L
1
0.150
0.500
9KO8026
EPA 6010D
11/13/19 13:19
JDH
Selenium [7782-49-2]^
0.00620
U
mg/L
1
0.00620
0.0100
9KO8026
EPA 6010D
11/13/19 13:19
JDH
Silver[7440-22-4]^
0.00190
U
mg/L
1
0.00190
0.0100
9KO8026
EPA 6010D
11/13/19 13:19
JDH
Sodium [7440-23-5]^
516
mg/L
1
0.400
0.500
9KO8026
EPA 6010D
11/13/19 13:19
JDH
Zinc[7440-66-6]^
0.00440
U
mg/L
1
0.00440
0.0100
9KO8026
EPA 6010D
11/13/19 13:19
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MOIL
P L
Batch
Method
Analyzed
By
Notes
Ammonia as N [7664-41-7]^
0.80
mg/L
1
0.045
0.10
9K14035
EPA 350.1
11/15/19 15:02
AKF
Bicarbonate (as CaCO3)[71-52-3]
1100
mg/L
1
14
15
9K13038
M 45000O2 D-201
11/13/19 14:31
JAH
Carbonate (as CaCO3)[3812-32-6]
20
mg/L
1
14
15
9K13038
M 45000O2 D-201
11/13/19 14:31
JAH
Chemical Oxygen Demand^
73
mg/L
1
10
10
9KO8002
SM 5220D-2011
11/08/19 15:40
JOC
Chloride [16887-00-6]^
420
D
mg/L
10
22
50
9KO7029
EPA 300.0
11/08/19 00:37
PDK
Cyanide (total) [57-12-5]^
0.0049
U
mg/L
1
0.0049
0.0050
9KO8005
EPA 335.4
11/11/19 17:23
AKF
FINAL
This report relates only
to the sample as received by the laboratory,
and may only
be reproduced
in full.
Page 7 of 28

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: RO Feed Lab Sample ID:CC17679-02 Received: 11/05/19 09:36
Matrix: Waste Water Sampled:11/04/19 16:30 Work Order: CC17679
Project: RO Pilot Sampled By: Scott Creech
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results
Flao
Units
DF
MDL
P L
Batch
Method
Analyzed
By
Notes
Nitrate as N [14797-55-8]
27
D
mg/L
48
2.0
4.8
[CALC]
EPA 353.2
11/19/19 11:38
AKF
Nitrate/Nitrite as IN
52
D
mg/L
48
2.0
4.8
9K14026
EPA 353.2
11/19/19 11:38
AKF
Nitrite as N [14797-65-0]^
25
D
mg/L
26.67
0.45
2.7
9KO5041
EPA 353.2
11/05/19 19:09
AKF
Orthophosphate as P [1426-54-42]^
7.2
B
mg/L
1
0.16
0.50
9KO5045
EPA 365.1
11/05/19 18:16
AKF
QB-01
pH
8.3
pH
1
1.0
1.0
9K11023
iM 4500H+B-2011
11/11/19 12:05
BDC
Q-01
Phosphorus[7723-14-0]^
8.0
D
mg/L
5
0.12
0.50
9KO6016
EPA 365.4
11/07/19 18:16
AKF
Specific Conductance (EC) at 25 Deg
3800
umhos/cm
1
1.0
1.0
9KO5036
SM 251OB-2011
11/05/19 15:00
JOC
C^
Sulfate as SO4 [14808-79-8]^
150
D
mg/L
2
5.8
10
9KO7029
EPA 300.0
11/08/19 00:19
PDK
Temperature for pH (deg. C)
14
pH
1
9K11023
iM 4500H+B-2011
11/11/19 12:05
BDC
Q-01
Total Alkalinity as CaCO3 [471-34-1]^
1100
D
mg/L
10
140
150
9K11019
EPA 310.2
11/11/19 18:34
AKF
Total Dissolved Solids^
2400
mg/L
1
50
50
9KO7028
SM 2540C-2011
11/08/19 10:14
JOC
Total Kjeldahl Nitrogen^
3.7
mg/L
1
0.26
0.48
9KO6015
EPA 351.2
11/07/19 16:47
AKF
Total Nitrogen [17778-88-0]
55
D
mg/L
48
2.0
4.8
[CALC]
CALC
11/19/19 11:38
AKF
Total Suspended Solids^
2.5
U
mg/L
1
2.5
2.5
9KO7032
SM 2540D-2011
11/07/19 14:02
BDC
Turbidity^
0.50
U
NTU
1
0.50
1.0
9KO5044
SM 213OB-2011
11/05/19 15:49
JOC
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 28

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: RO Permeate Lab Sample ID:CC17679-03 Received: 11/05/19 09:36
Matrix: Waste Water Sampled:11/04/19 16:30 Work Order: CC17679
Project: RO Pilot Sampled By: Scott Creech
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flao
Units
DF
MDL
P L
Batch
Method
Analyzed
-By Notes
Mercury[7439-97-6]^
0.000750
U
mg/L
5
0.000750
0.00100
9KO6050
EPA 7470A
11/08/19 13:25
KAH
Silica (Si02) [763-18-69]A
0.2
mg/L
1
0.03
0.2
9KO8026
EPA 6010D
11/13/19 13:22
JDH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flao
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Aluminum [7429-90-5]^
0.0420
U
mg/L
1
0.0420
0.100
9KO8026
EPA 6010D
11/13/19 13:22
JDH
Arsenic[7440-38-2]^
0.00760
U
mg/L
1
0.00760
0.0100
9KO8026
EPA 6010D
11/13/19 13:22
JDH
Boron [7440-42-8]A
0.0202
J
mg/L
1
0.00570
0.0500
9KO8026
EPA 6010D
11/13/19 13:22
JDH
Cadmium [7440-43-9]^
0.000360
U
mg/L
1
0.000360
0.00100
9KO8026
EPA 6010D
11/13/19 13:22
JDH
Calcium [7440-70-2]A
0.393
mg/L
1
0.0390
0.100
9KO8026
EPA 6010D
11/13/19 13:22
JDH
Chromium [7440-47-3]^
0.00140
U
mg/L
1
0.00140
0.0100
9KO8026
EPA 6010D
11/13/19 13:22
JDH
Copper[7440-50-8]^
0.00160
U
mg/L
1
0.00160
0.0100
9KO8026
EPA 6010D
11/13/19 13:22
JDH
Iron [7439-89-6]^
0.0220
U
mg/L
1
0.0220
0.0500
9KO8026
EPA 6010D
11/13/19 13:22
JDH
Lead [7439-92-1]^
0.00310
U
mg/L
1
0.00310
0.0100
9KO8026
EPA 6010D
11/13/19 13:22
JDH
Magnesium [7439-95-4]^
0.0290
U
mg/L
1
0.0290
0.100
9KO8026
EPA 6010D
11/13/19 13:22
JDH
Molybdenum [7439-98-7]^
0.00250
U
mg/L
1
0.00250
0.0100
9KO8026
EPA 6010D
11/13/19 13:22
JDH
Nickel[7440-02-0]^
0.00220
U
mg/L
1
0.00220
0.0100
9KO8026
EPA 6010D
11/13/19 13:22
JDH
Potassium [7440-09-7]A
23.5
mg/L
1
0.150
0.500
9KO8026
EPA 6010D
11/13/19 13:22
JDH
Selenium [7782-49-2]^
0.00620
U
mg/L
1
0.00620
0.0100
9KO8026
EPA 6010D
11/13/19 13:22
JDH
Silver[7440-22-4]^
0.00190
U
mg/L
1
0.00190
0.0100
9KO8026
EPA 6010D
11/13/19 13:22
JDH
Sodium [7440-23-5]A
14.1
mg/L
1
0.400
0.500
9KO8026
EPA 6010D
11/13/19 13:22
JDH
Zinc[7440-66-6]^
0.00440
U
mg/L
1
0.00440
0.0100
9KO8026
EPA 6010D
11/13/19 13:22
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flao
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Ammonia as N [7664-41-7]A
0.30
mg/L
1
0.045
0.10
9K14035
EPA 350.1
11/14/19 19:25
AKF
Bicarbonate (as CaCO3)[71-52-3]
23
mg/L
1
14
15
9K13038
M 4500002 D-201
11/13/19 14:31
JAH
Carbonate (as CaCO3)[3812-32-6]
14
U
mg/L
1
14
15
9K13038
M 4500002 D-201
11/13/19 14:31
JAH
Chemical Oxygen DemandA
15
mg/L
1
10
10
9KO8002
SM 5220D-2011
11/08/19 15:40
JOC
Chloride [ 16887-00-6] A
9.4
mg/L
1
2.2
5.0
9KO7029
EPA 300.0
11/08/19 00:54
PDK
Cyanide (total) [57-12-5]^
0.0049
U
mg/L
1
0.0049
0.0050
9KO8005
EPA 335.4
11/11/19 17:24
AKF
Nitrate as N [14797-55-8]
2.8
D
mg/L
5
0.20
0.50
[CALC]
EPA 353.2
11/19/19 10:46
AKF
Nitrate/Nitrite as NA
5.7
D
mg/L
5
0.20
0.50
9K14026
EPA 353.2
11/19/19 10:46
AKF
Nitrite as N [ 14797-65-0] A
Orthophosphate as P [1426-54-42] A
pH
Phosphorus[7723-14-0]^
Specific Conductance (EC) at 25 Deg
CA
Sulfate as SO4 [14808-79-8]^
Temperature for pH (deg. C)
Total Alkalinity as CaCO3 [471-34-1]A
Total Dissolved Solids^
Total Kjeldahl Nitrogen^
Total Nitrogen [17778-88-0]
Total Suspended Solids^
2.9
D
mg/L
0.27
JB
mg/L
7.8
pH
0.025
U
mg/L
140
umhos/cm
2.9
U
mg/L
14
pH
23
mg/L
94
mg/L
0.26
U
mg/L
5.7
D
mg/L
3.3
U
mg/L
5 0.084 0.50 9KO5041 EPA 353.2
1 0.16 0.50 9KO5045 EPA 365.1
1 1.0 1.0 9K11023 iM 4500H+B-2011
1 0.025 0.10 9KO6016 EPA 365.4
1 1.0 1.0 9KO5036 SM 251OB-2011
1 2.9 5.0 9KO7029 EPA 300.0
1 9K11023 iM 450011+13-2011
1 14 15 9K11019 EPA 310.2
1 50 50 9KO7028 SM 2540C-2011
1 0.26 0.48 9KO6015 EPA 351.2
5 0.26 0.50 [CALC] CALC
1.33 3.3 3.3 9KO7032 SM 2540D-2011
11/05/19 18:40 AKF
11/05/19 18:18 AKF 3-01
11/11/19 12:05 BDC Q-01
11/07/19 18:17 AKF
11/05/1915:00 JOC
11/08/19
00:54
PDK
11/11/19
12:05
BDC Q-01
11/11/19
18:30
AKF
11/08/1910:14
JOC
11/07/19
16:49
AKF
11/19/19
10:46
AKF
11/07/19
14:02
BDC LP-03
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 28

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ANALYTICAL RESULTS
Description: RO Permeate Lab Sample ID:CC17679-03 Received: 11/05/19 09:36
Matrix: Waste Water Sampled:11/04/19 16:30 Work Order: CC17679
Project: RO Pilot Sampled By: Scott Creech
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
TurbidityA 0.50 U
NTU
1
0.50
1.0
9KO5044
SM 213OB-2011
11/05/19 15:49
JOC
Classical Chemistry Parameters (Dissolved)
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Biochemical Oxygen DemandA 2.0 U
mg/L
1
2.0
2.0
9KO6007
SM 5210 B-2011
11/06/19 10:32
JOC
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 28

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ANALYTICAL RESULTS
Description: RO Reject Lab Sample ID:CC17679-04 Received: 11/05/19 09:36
Matrix: Waste Water Sampled:11/04/19 16:30 Work Order: CC17679
Project: RO Pilot Sampled By: Scott Creech
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary ced1fied analyte [NC 591]
Analyte rCAS Numberl
Results
Flao
Units
DF
MDL
P L
Batch
Method
Analyzed
-By Notes
Mercury[7439-97-6]^
0.000750
U
mg/L
5
0.000750
0.00100
9KO6050
EPA 7470A
11/08/19 13:27
KAH
Silica (Si02) [763-18-69]^
177
mg/L
1
0.03
0.2
9KO8026
EPA 6010D
11/13/19 13:25
JDH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flao
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Aluminum [7429-90-5]^
0.267
mg/L
1
0.0420
0.100
9KO8026
EPA 6010D
11/13/19 13:25
JDH
Arsenic[7440-38-2]^
0.00760
U
mg/L
1
0.00760
0.0100
9KO8026
EPA 6010D
11/13/19 13:25
JDH
Boron [7440-42-8]^
0.139
mg/L
1
0.00570
0.0500
9KO8026
EPA 6010D
11/13/19 13:25
JDH
Cadmium [7440-43-9]^
0.000360
U
mg/L
1
0.000360
0.00100
9KO8026
EPA 6010D
11/13/19 13:25
JDH
Calcium [7440-70-2]^
719
D
mg/L
10
0.390
1.00
9KO8026
EPA 6010D
11/13/19 16:05
JDH
Chromium [7440-47-3]^
0.00940
J
mg/L
1
0.00140
0.0100
9KO8026
EPA 6010D
11/13/19 13:25
JDH
Copper[7440-50-8]^
0.0140
mg/L
1
0.00160
0.0100
9KO8026
EPA 6010D
11/13/19 13:25
JDH
Iron [7439-89-6]^
0.398
mg/L
1
0.0220
0.0500
9KO8026
EPA 6010D
11/13/19 13:25
JDH
Lead [7439-92-1]^
0.00310
U
mg/L
1
0.00310
0.0100
9KO8026
EPA 6010D
11/13/19 13:25
JDH
Magnesium [7439-95-4]^
44.1
mg/L
1
0.0290
0.100
9KO8026
EPA 6010D
11/13/19 13:25
JDH
Molybdenum [7439-98-7]^
0.00599
J
mg/L
1
0.00250
0.0100
9KO8026
EPA 6010D
11/13/19 13:25
JDH
Nickel[7440-02-O]^
0.0141
mg/L
1
0.00220
0.0100
9KO8026
EPA 6010D
11/13/19 13:25
JDH
Potassium [7440-09-7]^
3450
D
mg/L
10
1.50
5.00
9KO8026
EPA 6010D
11/13/19 16:05
JDH
Selenium [7782-49-2]^
0.00620
U
mg/L
1
0.00620
0.0100
9KO8026
EPA 6010D
11/13/19 13:25
JDH
Silver[7440-22-4]^
0.00190
U
mg/L
1
0.00190
0.0100
9KO8026
EPA 6010D
11/13/19 13:25
JDH
Sodium [7440-23-5]^
4120
D
mg/L
10
4.00
5.00
9KO8026
EPA 6010D
11/13/19 16:05
JDH
Zinc[7440-66-6]^
0.0226
mg/L
1
0.00440
0.0100
9KO8026
EPA 6010D
11/13/19 13:25
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flao
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Ammonia as N [7664-41-7]^
5.3
D
mg/L
5
0.22
0.50
9K14035
EPA 350.1
11/15/19 09:55
AKF
Bicarbonate (as CaCO3)[71-52-3]
2000
mg/L
1
14
15
9K13038
M 4500002 D-201
11/13/19 14:31
JAH
Carbonate (as CaCO3)[3812-32-6]
14
U
mg/L
1
14
15
9K13038
M 4500002 D-201
11/13/19 14:31
JAH
Chemical Oxygen Demand
550
mg/L
2
20
20
9KO8002
SM 5220D-2011
11/08/19 15:40
JOC
Chloride [16887-00-6]^
3200
D
mg/L
100
220
500
91<25025
EPA 300.0
11/26/19 00:20
PDK
Cyanide (total)[57-12-5]^
0.041
mg/L
1
0.0049
0.0050
9KO8005
EPA 335.4
11/11/19 17:26
AKF
Nitrate as N [14797-55-8]
270
D
mg/L
200
8.2
20
[CALC]
EPA 353.2
11/19/19 10:55
AKF
Nitrate/Nitrite as N^
420
D
mg/L
200
8.2
20
9K14026
EPA 353.2
11/19/19 10:55
AKF
Nitrite as N [14797-65-0]^
Orthophosphate as P[1426-54-42]^
pH
Phosphorus[7723-14-O]^
Specific Conductance (EC) at 25 Deg
C^
Sulfate as SO4 [14808-79-8]^
Temperature for pH (deg. C)
Total Alkalinity as CaCO3 [471-34-1]^
Total Dissolved Solids^
Total Kjeldahl Nitrogen
Total Nitrogen [17778-88-0]
Total Suspended Solids^
150
BD
mg/L
52
BD
mg/L
7.2
pH
74
D
mg/L
25000
umhos/cm
6200
D
mg/L
15
pH
2000
D
mg/L
20000
mg/L
19
D
mg/L
440
D
mg/L
4.0
mg/L
80
1.3
8.0
9K13023
EPA 353.2
25
4.0
12
9KO5045
EPA 365.1
1
1.0
1.0
9KII023
iM 4500H+B-2011
50
1.2
5.0
9KO6016
EPA 365.4
1
1.0
1.0
9KO5036
SM 251OB-2011
100
290
500
91<25025
EPA 300.0
1
91<11023
iM 4500H+B-2011
10
140
150
9KO5022
EPA 310.2
1
50
50
9KO7028
SM 2540C-2011
10
2.6
4.8
9KO6015
EPA 351.2
200
8.2
20
[CALC]
CALC
1
2.5
2.5
9KO7032
SM 2540D-2011
11/13/19 12:16 AKF Q-01
11/05/19 19:18 AKF QB-01
11/11/19 12:05 BDC Q-01
11/08/19 14:41 AKF
11/05/1915:00 JOC
11/26/19 00:20
11/11/19 12:05
11/05/19 16:24
11/08/19 10:14
11/07/19 16:50
11/19/19 10:55
11/07/19 14:02
PDK
BDC
AKF
JOC
AKF
AKF
BDC
Q-01
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 28

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ANALYTICAL RESULTS
Description: RO Reject Lab Sample ID:CC17679-04 Received: 11/05/19 09:36
Matrix: Waste Water Sampled:11/04/19 16:30 Work Order: CC17679
Project: RO Pilot Sampled By: Scott Creech
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Turbidity^ 7.5 NTU 1 0.50 1.0 9KO5044 SM 213OB-2011 11/05/19 15:49 30C
Description: MBBR Feed Lab Sample ID:CC17679-05 Received: 11/05/19 09:36
Matrix: Waste Water Sampled:11/04/19 16:30 Work Order: CC17679
Project: RO Pilot Sampled By: Scott Creech
(Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Notes
Silica (Si02) [763-18-69]^ 28.3 mg/L 1 0.03 0.2 9KO8026 EPA 6010D 11/13/19 13:28 ]DH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 28

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 9K06050 - EPA 7470A
Blank (9K06050-BLKI) Prepared: 11/06/2019 16:23 Analyzed: 11/08/2019 12:31
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Mercury 0.000150 U 0.000200 mg/L
LCS (9K06050-BSI) Prepared: 11/06/2019 16:23 Analyzed: 11/08/2019 14:17
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Mercury
0.00474
0.000200
mg/L
0.00500 95 80-120
Matrix Spike (9K06050-MS3)
Prepared: 11/06/2019 16:23 Analyzed: 11/08/2019 12:39
Source: CC18269-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Mercury
0.00507
0.000200
mg/L
0.00500 0.000150 U 101 75-125
Matrix Spike Dup (9K06050-MSD3)
Prepared: 11/06/2019 16:23 Analyzed: 11/08/2019 12:41
Source: CC18269-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Mercury
0.00489
0.000200
mg/L
0.00500 0.000150 U 98 75-125 4
25
Post Spike (9K06050-PSI)
Prepared: 11/06/2019 16:23 Analyzed: 11/08/2019 12:44
Source: CC18269-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Mercury
4.80
0.200
ug/L
4.76-0.0667 101 75-125
Batch 9K08026 - EPA 3005A
Blank (9K08026-BLKS)
Prepared: 11/08/2019 15:01 Analyzed: 11/13/2019 11:15
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Silica (Si02) 0.03 U 0.2 mg/L
Blank (9K08026-BLK2) Prepared: 11/08/2019 15:01 Analyzed: 11/13/2019 11:19
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Silica (Si02) 0.03 U 0.2 mg/L
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 9K08026 - EPA 3005A
Blank (9K08026-BLK1) Prepared: 11/08/2019 15:01 Analyzed: 11/13/2019 11:15
Analvte
Result
Flaq
Q
Units
Aluminum
0.0420
U
0.100
mg/L
Arsenic
0.00760
U
0.0100
mg/L
Boron
0.00570
U
0.0500
mg/L
Cadmium
0.000360
U
0.00100
mg/L
Calcium
0.0390
U
0.100
mg/L
Chromium
0.00140
U
0.0100
mg/L
Copper
0.00160
U
0.0100
mg/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit
Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 28

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 9KO8026 - EPA 3005A - Continued
Blank (9K08026-BLKI) Continued Prepared: 11/08/2019 15:01 Analyzed: 11/13/2019 11:15
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Iron
0.0220
U
0.0500
mg/L
Lead
0.00310
U
0.0100
mg/L
Magnesium
0.0290
U
0.100
mg/L
Molybdenum
0.00250
U
0.0100
mg/L
Nickel
0.00220
U
0.0100
mg/L
Potassium
0.150
U
0.500
mg/L
Selenium
0.00620
U
0.0100
mg/L
Silver
0.00190
U
0.0100
mg/L
Sodium
0.400
U
0.500
mg/L
Zinc
0.00440
U
0.0100
mg/L
Blank (9K08026-BLK2)
Prepared: 11/08/2019 15:01 Analyzed: 11/13/2019 11:19
Spike Source %REC RPD
Analvte
Result
Flaq
PQL
Units
Level Result %REC Limits RPD Limit Notes
Aluminum
0.0420
U
0.100
mg/L
Arsenic
0.00760
U
0.0100
mg/L
Boron
0.00570
U
0.0500
mg/L
Cadmium
0.000360
U
0.00100
mg/L
Calcium
0.0390
U
0.100
mg/L
Chromium
0.00140
U
0.0100
mg/L
Copper
0.00160
U
0.0100
mg/L
Iron
0.0220
U
0.0500
mg/L
Lead
0.00310
U
0.0100
mg/L
Magnesium
0.0290
U
0.100
mg/L
Molybdenum
0.00250
U
0.0100
mg/L
Nickel
0.00220
U
0.0100
mg/L
Potassium
0.150
U
0.500
mg/L
Selenium
0.00620
U
0.0100
mg/L
Silver
0.00190
U
0.0100
mg/L
Sodium
0.400
U
0.500
mg/L
Zinc
0.00440
U
0.0100
mg/L
LCS (9K08026-BS1)
Prepared: 11/08/2019 15:01 Analyzed: 11/13/2019 11:24
Spike
Source
%REC RPD
Analvte
Result
Flaq POL
Units
Level
Result %REC
Limits RPD Limit Notes
Aluminum
2.00
0.100
mg/L
2.00
100
80-120
Arsenic
0.194
0.0100
mg/L
0.200
97
80-120
Boron
1.03
0.0500
mg/L
1.00
103
80-120
Cadmium
0.0207
0.00100
mg/L
0.0200
104
80-120
Calcium
1.95
0.100
mg/L
2.00
97
80-120
Chromium
0.206
0.0100
mg/L
0.200
103
80-120
Copper
0.200
0.0100
mg/L
0.200
100
80-120
Iron
1.02
0.0500
mg/L
1.00
102
80-120
Lead
0.199
0.0100
mg/L
0.200
100
80-120
Magnesium
1.98
0.100
mg/L
2.00
99
80-120
Molybdenum
0.198
0.0100
mg/L
0.200
99
80-120
Nickel
0.204
0.0100
mg/L
0.200
102
80-120
Potassium
10.2
0.500
mg/L
10.0
102
80-120
Selenium
0.196
0.0100
mg/L
0.200
98
80-120
FINAL
This report relates only to the sample as received by the
laboratory, and
may only be reproduced in
full. Page 14 of 28

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 9K08026 - EPA 3005A - Continued
LCS (9K08026-BS3) Continued Prepared: 11/08/2019 15:01 Analyzed: 11/13/2019 11:24
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Silver
0.213
0.0100
mg/L
0.200
107
80-120
Sodium
10.3
0.500
mg/L
10.0
103
80-120
Zinc
0.208
0.0100
mg/L
0.200
104
80-120
Matrix Spike (9K08026-MS1)
Prepared:
11/08/2019
15:01 Analyzed: 11/13/2019 11:32
Source: CC15266-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Aluminum
2.05
0.100
mg/L
2.00
0.0509
100
75-125
Arsenic
0.185
0.0100
mg/L
0.200
0.00760 U
92
75-125
Boron
1.04
0.0500
mg/L
1.00
0.0194
102
75-125
Cadmium
0.0194
0.00100
mg/L
0.0200
0.000360 U
97
75-125
Calcium
68.1
0.100
mg/L
2.00
63.8
215
75-125
QM-07
Chromium
0.195
0.0100
mg/L
0.200
0.00140 U
97
75-125
Copper
0.193
0.0100
mg/L
0.200
0.00344
95
75-125
Iron
1.07
0.0500
mg/L
1.00
0.0511
102
75-125
Lead
0.191
0.0100
mg/L
0.200
0.00310 U
96
75-125
Magnesium
4.90
0.100
mg/L
2.00
2.84
103
75-125
Molybdenum
0.197
0.0100
mg/L
0.200
0.00369
97
75-125
Nickel
0.200
0.0100
mg/L
0.200
0.00220 U
100
75-125
Potassium
12.2
0.500
mg/L
10.0
1.70
105
75-125
Selenium
0.192
0.0100
mg/L
0.200
0.00620 U
96
75-125
Silver
0.198
0.0100
mg/L
0.200
0.00190 U
99
75-125
Sodium
24.3
0.500
mg/L
10.0
13.3
109
75-125
Zinc
0.209
0.0100
mg/L
0.200
0.00548
102
75-125
Matrix Spike Dup (9K08026-MSD1)
Prepared:
11/08/2019
15:01 Analyzed: 11/13/2019 11:35
Source: CC15266-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Aluminum
2.04
0.100
mg/L
2.00
0.0509
99
75-125
0.8
20
Arsenic
0.181
0.0100
mg/L
0.200
0.00760 U
90
75-125
2
20
Boron
1.05
0.0500
mg/L
1.00
0.0194
103
75-125
0.6
20
Cadmium
0.0197
0.00100
mg/L
0.0200
0.000360 U
98
75-125
1
20
Calcium
66.8
0.100
mg/L
2.00
63.8
149
75-125
2
20 QM-07
Chromium
0.195
0.0100
mg/L
0.200
0.00140 U
98
75-125
0.3
20
Copper
0.192
0.0100
mg/L
0.200
0.00344
94
75-125
0.7
20
Iron
1.08
0.0500
mg/L
1.00
0.0511
103
75-125
0.9
20
Lead
0.190
0.0100
mg/L
0.200
0.00310 U
95
75-125
0.5
20
Magnesium
4.92
0.100
mg/L
2.00
2.84
104
75-125
0.2
20
Molybdenum
0.197
0.0100
mg/L
0.200
0.00369
97
75-125
0.008
20
Nickel
0.202
0.0100
mg/L
0.200
0.00220 U
101
75-125
0.6
20
Potassium
12.0
0.500
mg/L
10.0
1.70
103
75-125
2
20
Selenium
0.190
0.0100
mg/L
0.200
0.00620 U
95
75-125
0.8
20
Silver
0.198
0.0100
mg/L
0.200
0.00190 U
99
75-125
0.2
20
Sodium
23.6
0.500
mg/L
10.0
13.3
103
75-125
3
20
Zinc
0.211
0.0100
mg/L
0.200
0.00548
103
75-125
1
20
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 15 of 28

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 9K08026 - EPA 3005A - Continued
Post Spike (9K08026-PS3)
Prepared: 11/08/2019 15:01 Analyzed: 11/13/2019 11:37
Source: CC15266-01
Spike
Source
%REC RPD
Analvte
Result
Flaq Q
Units
Level
Result
%REC
Limits RPD Limit Notes
Aluminum
2.04
0.100
mg/L
2.00
0.0509
100
80-120
Arsenic
0.185
0.0100
mg/L
0.200
-0.00700
92
80-120
Boron
1.04
0.0500
mg/L
1.00
0.0194
102
80-120
Cadmium
0.0197
0.00100
mg/L
0.0200
-0.000289
99
80-120
Calcium
66.7
0.100
mg/L
2.00
63.8
144
80-120 QM-08
Chromium
0.194
0.0100
mg/L
0.200
0.000205
97
80-120
Copper
0.194
0.0100
mg/L
0.200
0.00344
95
80-120
Iron
1.07
0.0500
mg/L
1.00
0.0511
102
80-120
Lead
0.195
0.0100
mg/L
0.200
-0.00132
98
80-120
Magnesium
4.91
0.100
mg/L
2.00
2.84
104
80-120
Molybdenum
0.196
0.0100
mg/L
0.200
0.00369
96
80-120
Nickel
0.201
0.0100
mg/L
0.200
0.000648
100
80-120
Potassium
12.3
0.500
mg/L
10.0
1.70
106
80-120
Selenium
0.191
0.0100
mg/L
0.200
-0.0163
96
80-120
Silver
0.199
0.0100
mg/L
0.200
8.15E-5
99
80-120
Sodium
23.5
0.500
mg/L
10.0
13.3
101
80-120
Zinc
0.212
0.0100
mg/L
0.200
0.00548
103
80-120
Metals (Dissolved) by EPA 6000/7000 Series
Methods - Quality
Control
Batch 9K08026 - EPA 3005A
Blank (9K08026-BLK1)
Prepared: 11/08/2019 15:01 Analyzed: 11/13/2019 11:15
Spike Source %REC
RPD
Analvte
Result
Flaq
PQL
Units
Level Result %REC Limits RPD
Limit Notes
Calcium
0.0390
U
0.100
mg/L
Magnesium
29.0
U
100
ug/L
Silica (Si02)
0.03
U
0.2
mg/L
Blank (9K08026-BLK2)
Prepared: 11/08/2019 15:01 Analyzed: 11/13/2019 11:19
Spike Source %REC
RPD
Analvte
Result
Flaq
PQL
Units
Level Result %REC Limits RPD
Limit Notes
Calcium
0.0390
U
0.100
mg/L
Magnesium
29.0
U
100
ug/L
Silica (Si02)
0.03
U
0.2
mg/L
LCS (9K08026-BSI)
Prepared: 11/08/2019 15:01 Analyzed: 11/13/2019 11:24
Spike Source %REC
RPD
Analvte
Result
Flaq
PQL
Units
Level Result %REC Limits RPD
Limit Notes
Calcium
1.95
0.100
mg/L
2.00 97 80-120
Magnesium
1980
100
ug/L
2000 99 80-120
Matrix Spike (9K08026-MS1)
Prepared: 11/08/2019 15:01 Analyzed: 11/13/2019 11:32
Source: CC15266-01
Spike Source %REC RPD
Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes
Calcium 68.1 0.100 mg/L 2.00 63.8 215 75-125 QM-07
Magnesium 4900 100 ug/L 2000 2840 103 75-125
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 16 of 28

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QUALITY CONTROL DATA
Metals (Dissolved) by EPA 6000/7000 Series Methods - Quality Control
Batch 9K08026 - EPA 3005A - Continued
Matrix Spike Dup (9K08026-MSD3)
Prepared: 11/08/2019 15:01 Analyzed: 11/13/2019 11:35
Source: CC15266-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Calcium
66.8
0.100
mg/L
2.00
63.8
149
75-125 2
20
QM-07
Magnesium
4920
100
ug/L
2000
2840
104
75-125 0.2
20
Post Spike (9K08026-PS1)
Prepared: 11/08/2019 15:01 Analyzed: 11/13/2019 11:37
Source: CC15266-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Calcium
66.7
0.100
mg/L
2.00
63.8
144
80-120
QM-08
Magnesium
4.91
0.100
mg/L
2.00
2.84
104
80-120
Classical Chemistry Parameters - Quality Control
Batch 9K05022 - NO PREP
Blank (9K05022-BLKI) Prepared: 11/05/2019 11:35 Analyzed: 11/05/2019 16:10
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Alkalinity as CaCO3 14 U 15 mg/L
LCS (9K05022-BSI) Prepared: 11/05/2019 11:35 Analyzed: 11/05/2019 16:10
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Alkalinity as CaCO3
100
15
mg/L
100 100 80-120
Matrix Spike (9K05022-MSI)
Prepared: 11/05/2019 11:35 Analyzed: 11/05/2019 16:12
Source: CC16612-15
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Alkalinity as CaCO3
48
15
mg/L
37.8 14 U 128 80-120
QM-07
Matrix Spike Dup (9K05022-MSD3)
Prepared: 11/05/2019 11:35 Analyzed: 11/05/2019 16:12
Source: CC16612-15
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Alkalinity as CaCO3
49
15
mg/L
37.8 14 U 130 80-120 2
25
QM-07
Batch 9K05036 - NO PREP
Blank (9K05036-BLKl) Prepared & Analyzed: 11/05/2019 15:00
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Specific Conductance (EC) at 25 Deg C 1.0 U 1.0 umhos/cm
LCS (9K05036-BS3) Prepared & Analyzed: 11/05/2019 15:00
Spike Source %REC
RPD
Analvte
Result Flaq POL Units Level Result %REC Limits RPD
Limit Notes
Specific Conductance (EC) at 25 Deg C
720 1.0 umhos/cm 705 102 90-110
Duplicate (9K05036-DUPl)
Prepared & Analyzed: 11/05/2019 15:00
Source: CC14900-03
Spike Source %REC
RPD
Analvte
Result Flaq Q Units Level Result %REC Limits RPD
Limit Notes
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 17 of 28

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9K05036 - NO PREP - Continued
Duplicate (9K05036-DUPl) Continued
Prepared & Analyzed: 11/05/2019 15:00
Source: CC14900-03
Spike Source %REC
RPD
Analvte Result Flag
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Specific Conductance (EC) at 25 Deg C 3400
1.0
umhos/cm
3400
0.9
25
Duplicate (9K05036-DUP2)
Prepared & Analyzed: 11/05/2019 15:00
Source: CC14901-03
Spike Source %REC
RPD
Analvte Result Flag
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Specific Conductance (EC) at 25 Deg C 3400
1.0
umhos/cm
3400
0.6
25
Batch 9K05041 - NO PREP
Blank (9K05041-BLKS)
Prepared: 11/05/2019 15:37 Analyzed: 11/05/2019 17:36
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
0.017
U
0.10
mg/L
LCS (9K05041-BS3)
Prepared: 11/05/2019 15:37 Analyzed: 11/05/2019 17:55
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
0.99
0.10
mg/L
1.00 99 90-110
Matrix Spike (9K05041-MSi)
Prepared: 11/05/2019 15:37 Analyzed: 11/05/2019 17:38
Source: CC16645-01
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
1.0
0.10
mg/L
1.00 0.067 95 90-110
Matrix Spike (9K05041-MS2)
Prepared: 11/05/2019 15:37 Analyzed: 11/05/2019 17:43
Source: CC16647-01
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
1.1
0.10
mg/L
1.00 0.20 87 90-110
QM-07
Matrix Spike Dup (9K05041-MSD3)
Prepared: 11/05/2019 15:37 Analyzed: 11/05/2019 17:39
Source: CC16645-01
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
1.0
0.10
mg/L
1.00 0.067 95 90-110 0.6
10
Batch 9K05044 - NO PREP
Blank (9K05044-BLK1)
Prepared & Analyzed: 11/05/2019 15:49
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Turbidity
0.50
U
1.0
NTU
LCS (9K05044-BS3)
Prepared & Analyzed: 11/05/2019 15:49
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Turbidity
20
1.0
NTU
20.0 98 80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 18 of 28

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9KO5044 - NO PREP - Continued
Duplicate (9K05044-DUPl) Prepared & Analyzed: 11/05/2019 15:49
Source: CC14901-03
Spike Source %REC RPD
Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes
Turbidity 1.3 1.0 NTU 1.3 5 25
Batch 9KO5045 - NO PREP
Blank (9K05045-BLK1)
Prepared: 11/05/2019 18:15 Analyzed: 11/05/2019 18:15
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Orthophosphate as P
0.24
3
0.50
mg/L
1-01, Q13-0.
LCS (9KO5045-BS3)
Prepared: 11/05/2019 18:14 Analyzed: 11/05/2019 18:14
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Orthophosphate as P
5.0
B
0.50
mg/L
5.00 100 90-110
LCS (91(05045-BS2)
Prepared & Analyzed: 11/05/2019 18:22
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Orthophosphate as P
5.0
B
0.50
mg/L
5.00 101 90-110
Matrix Spike (9KO5045-MSi)
Prepared: 11/05/2019 18:16 Analyzed: 11/05/2019 18:16
Source: CC17679-02
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Orthophosphate as P
10
B
0.50
mg/L
2.00 7.2 139 90-110
QM-07
Matrix Spike Dup (9K05045-MSD3)
Prepared: 11/05/2019 18:17 Analyzed: 11/05/2019 18:17
Source: CC17679-02
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Orthophosphate as P
9.4
B
0.50
mg/L
2.00 7.2 111 90-110 6
10
QM-07
Batch 9KO6015 - Same
Blank (9K06015-BLK1)
Prepared: 11/06/2019 10:13 Analyzed: 11/07/2019 16:15
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Kjeldahl Nitrogen
0.26
U
0.48
mg/L
Blank (9K06015-BLK2)
Prepared: 11/06/2019 10:13 Analyzed: 11/08/2019 13:48
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Kjeldahl Nitrogen
0.26
U
0.48
mg/L
LCS (9KO6015-BS3)
Prepared: 11/06/2019 10:13 Analyzed: 11/07/2019 16:17
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Kjeldahl Nitrogen
12
0.48
mg/L
12.0 101 90-110
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 19 of 28

QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9KO6015 - Same - Continued
0Nk"q09
www.encolabs.com
LCS (9K06015-BS2) Prepared: 11/06/2019 10:13 Analyzed: 11/08/2019 13:50
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
13
0.48
mg/L
12.0 110 90-110
Matrix Spike (9K06015-MS1)
Prepared: 11/06/2019 10:13 Analyzed: 11/07/2019 16:21
Source: CC17923-01
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
6.3
0.48
mg/L
4.80 0.93 113 90-110
QM-07
Matrix Spike (9K06015-MS2)
Prepared: 11/06/2019 10:13 Analyzed: 11/07/2019 16:26
Source: CC17929-01
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limi RPD
Limit
Notes
Total Kjeldahl Nitrogen
4.4
0.48
mg/L
4.80 0.86 74 90-110
QM-07
Matrix Spike Dup (9Ko6015-MSD1)
Prepared: 11/06/2019 10:13 Analyzed: 11/07/2019 16:22
Source: CC17923-01
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
5.8
0.48
mg/L
4.80 0.93 100 90-110 10
10
Batch 9KO6016 - Same
Blank (9K06016-BLK1)
Prepared: 11/06/2019 10:13 Analyzed: 11/07/2019 17:53
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
0.025
U
0.10
mg/L
Blank (9K06016-BLK2)
Prepared: 11/06/2019 10:13 Analyzed: 11/08/2019 14:36
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
0.025
U
0.10
mg/L
Blank (9K06016-BLK3)
Prepared: 11/06/2019 10:13 Analyzed: 11/19/2019 15:52
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
0.025
U
0.10
mg/L
LCS (9K06016-BSI)
Prepared: 11/06/2019 10:13 Analyzed: 11/07/2019 17:54
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
1.6
0.10
mg/L
1.60 103 80-120
LCS (9K06016-BS2)
Prepared: 11/06/2019 10:13 Analyzed: 11/08/2019 14:38
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limi RPD
Mma
Notes
Phosphorus
1.7
0.10
mg/L
1.60 104 80-120
LCS (9K06016-BS3)
Prepared: 11/06/2019 10:13 Analyzed: 11/19/2019 15:54
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 20 of 28

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9K06016 - Same - Continued
LCS (9K06016-BS3) Continued Prepared: 11/06/2019 10:13 Analyzed: 11/19/2019 15:54
Spike Source %REC
RPD
Analvte
Result
Flag
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
1.6
0.10
mg/L
1.60 100 80-120
Matrix Spike (9K06016-MS1)
Prepared: 11/06/2019 10:13 Analyzed: 11/07/2019 17:57
Source: CC17923-01
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
7.4
D
0.50
mg/L
0.640 6.7 109 80-120
Matrix Spike Dup (91(06016-MSD1)
Prepared: 11/06/2019 10:13 Analyzed: 11/07/2019 17:58
Source: CC17923-01
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
7.1
D
0.50
mg/L
0.640 6.7 68 80-120 4
25
QM-07
Batch 9K0702B - NO PREP
Blank (9K07028-BLK1)
Prepared & Analyzed: 11/08/2019 10:14
Spike Source %REC RPD
Analvte Result Flag Q Units Level Result %REC Limits RPD Limit Notes
Total Dissolved Solids 50 U 50 mg/L
LCS (9K07028-BS3) Prepared & Analyzed: 11/08/2019 10:14
Spike Source %REC
RPD
Analvte
Result Flag
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Total Dissolved Solids
1100
50
mg/L
1000 108 80-120
Duplicate (9K07028-DUPI)
Prepared & Analyzed: 11/08/2019 10:14
Source: CC14791-01
Spike Source %REC
RPD
Analvte
Result Flag
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Total Dissolved Solids
12000
50
mg/L
11000
10
20
Duplicate (9K07028-DUP2)
Prepared & Analyzed: 11/08/2019 10:14
Source: CC14792-01
Spike Source %REC
RPD
Analvte
Result Flag
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Total Dissolved Solids
18000
50
mg/L
20000
9
20
Batch 9K07029 - NO PREP
Blank (9K07029-BLK1) Prepared: 11/07/2019 13:14 Analyzed: 11/07/2019 20:29
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Chloride 2.2 U 5.0 mg/L
Sulfate as SO4 2.9 U 5.0 mg/L
LCS (9K07029-BS3) Prepared: 11/07/2019 13:14 Analyzed: 11/07/2019 20:47
Spike Source %REC RPD
Analvte Result Flag Q Units Level Result %REC Limits RPD Limit Notes
Chloride 51 5.0 mg/L 50.0 102 90-110
Sulfate as SO4 50 5.0 mg/L 50.0 99 90-110
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 21 of 28

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9K07029 - NO PREP - Continued
Matrix Spike (9K07029-MS3)
Prepared: 11/07/2019 13:14 Analyzed: 11/07/2019 21:22
Source: CC18269-01
Spike Source %REC
RPD
Analvte
Result Flaq
Q
Units
Level Result %REC Limits RPD
Limit Notes
Chloride
57
5.0
mg/L
20.0 36 110 90-110
Sulfate as SO4
20
5.0
mg/L
20.0 2.9 U 101 90-110
Matrix Spike (9K07029-MS2)
Prepared: 11/07/2019 13:14 Analyzed: 11/07/2019 22:15
Source: CC18270-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Chloride
49
5.0
mg/L
20.0 27 108 90-110
Sulfate as SO4
22
5.0
mg/L
20.0 3.1 92 90-110
Matrix Spike Dup (9K07029-MSD3)
Prepared: 11/07/2019 13:14 Analyzed: 11/07/2019 21:40
Source: CC18269-01
Spike Source %REC
RPD
Analvte
Result Flaq POL Units
Level Result %REC Limits RPD
Limit Notes
Chloride
58 5.0 mg/L
20.0 36 111 90-110 0.4
10 QM-07
Sulfate as SO4
20 5.0 mg/L
20.0 2.9 U 102 90-110 0.9
10
Batch 9K07032 - NO PREP
Blank (9K07032-BLK1)
Prepared & Analyzed: 11/07/2019 14:02
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Suspended Solids 2.5 U 2.5 mg/L
LCS (9K07032-BS3) Prepared & Analyzed: 11/07/2019 14:02
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Total Suspended Solids
95
2.5
mg/L
100 95 80-120
Duplicate (9K07032-DUPI)
Prepared & Analyzed: 11/07/2019 14:02
Source: CC16334-04
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Total Suspended Solids
29
25
mg/L
30
3
20
Duplicate (9K07032-DUP2)
Prepared & Analyzed: 11/07/2019 14:02
Source: CC17729-01
Spike Source %REC
RPD
Analvte
Result Flaq
Q
Units
Level Result %REC Limits
RPD
Limit Notes
Total Suspended Solids
690
210
mg/L
660
5
20
Batch 9K08002 - Same
Blank (9K08002-BLKI) Prepared: 11/08/2019 09:03 Analyzed: 11/08/2019 15:40
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Chemical Oxygen Demand 10 U 10 mg/L
LCS (9K08002-BS3) Prepared: 11/08/2019 09:03 Analyzed: 11/08/2019 15:40
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 22 of 28

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9K08002 - Same - Continued
LCS (9K08002-BS3) Continued Prepared: 11/08/2019 09:03 Analyzed: 11/08/2019 15:40
Spike
Source
%REC
RPD
Analvte
Result Flag
Q
Units
Level
Result
%REC
Limits RPD
Limit Notes
Chemical Oxygen Demand
490
10
mg/L
500
97
90-110
Matrix Spike (9K08002-MSi)
Prepared: 11/08/2019 09:03 Analyzed: 11/08/2019 15:40
Source: CC14781-01
Spike
Source
%REC
RPD
Analvte
Result Flag
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Chemical Oxygen Demand
830
10
mg/L
526
310
100
90-110
Matrix Spike Dup (9K08002-MSD3)
Prepared: 11/08/2019 09:03 Analyzed: 11/08/2019 15:40
Source: CC14781-01
Spike
Source
%REC
RPD
Analvte
Result Flag
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Chemical Oxygen Demand
820
10
mg/L
526
310
97
90-110 2
5
Batch 9K08005 - Same
Blank (9K08005-BLK1) Prepared: 11/08/2019 09:27 Analyzed: 11/11/2019 16:55
Spike Source %REC RPD
Analvte Result Flag Q Units Level Result %REC Limits RPD Limit Notes
Cyanide (total) 0.0049 U 0.0050 mg/L
LCS (9K08005-BS3) Prepared: 11/08/2019 09:27 Analyzed: 11/11/2019 16:57
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Cyanide (total)
0.15
0.0050
mg/L
0.150 103 90-110
Matrix Spike (9K08005-MS1)
Prepared: 11/08/2019 09:27 Analyzed: 11/11/2019 17:04
Source: CC18269-01
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Cyanide (total)
0.14
0.0050
mg/L
0.150 0.0049 U 92 90-110
Matrix Spike (9K08005-MS2)
Prepared: 11/08/2019 09:27 Analyzed: 11/11/2019 17:09
Source: CC17523-29
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Cyanide (total)
0.16
0.0050
mg/L
0.150 0.0049 U 106 90-110
Matrix Spike Dup (9K08005-MSD3)
Prepared: 11/08/2019 09:27 Analyzed: 11/11/2019 17:06
Source: CC18269-01
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Cyanide (total)
0.14
0.0050
mg/L
0.150 0.0049 U 93 90-110 0.6
10
Batch 9K11019 - NO PREP
Blank (9K13019-BLKS) Prepared: 11/11/2019 10:23 Analyzed: 11/11/2019 18:29
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Total Alkalinity as CaCO3 14 U 15 mg/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 23 of 28

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9KII019 - NO PREP - Continued
LCS (9K31019-BS3) Prepared: 11/11/2019 10:23 Analyzed: 11/11/2019 18:30
Spike
Source
%REC
RPD
Analvte
Result Flaq
Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Total Alkalinity as CaCO3
98
15
mg/L
100
98
80-120
Matrix Spike (9K31019-MSi)
Prepared: 11/11/2019 10:23 Analyzed: 11/11/2019 18:31
Source: CC17679-03
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Total Alkalinity as CaCO3
67
15
mg/L
37.8
23
119
80-120
Matrix Spike Dup (9K11019-MSD3)
Prepared: 11/11/2019 10:23 Analyzed: 11/11/2019 18:32
Source: CC17679-03
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Total Alkalinity as CaCO3
69
15
mg/L
37.8
23
124
80-120 3
25
QM-07
Batch 9KI1023 - NO PREP
LCS (9K31023-BS3) Prepared & Analyzed: 11/11/2019 12:05
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
pH
7.0
1.0
pH
7.00 100 99-101
Duplicate (9K13023-DUP3)
Prepared & Analyzed: 11/11/2019 12:05
Source: CC16895-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
pH
8.4
1.0
pH
8.3 0.5
25
Batch 9K13023 - NO PREP
Blank (9K13023-BLKS) Prepared: 11/13/2019 10:56 Analyzed: 11/13/2019 12:08
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Nitrite as N 0.035 7 0.10 mg/L
LCS (9K33023-BS3) Prepared: 11/13/2019 10:56 Analyzed: 11/13/2019 12:27
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrite as N
1.1
B
0.10
mg/L
1.00 107 90-110
Matrix Spike (9K33023-MSi)
Prepared: 11/13/2019 10:56 Analyzed: 11/13/2019 12:10
Source: CC18215-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrite as N
1.0
B
0.10
mg/L
1.00 0.044 99 90-110
Matrix Spike (9K33023-MS2)
Prepared: 11/13/2019 10:56 Analyzed: 11/13/2019 12:15
Source: CC18215-02
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrite as N
1.0
B
0.10
mg/L
1.00 0.038 98 90-110
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 24 of 28

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9K13023 - NO PREP - Continued
Matrix Spike Dup (9K13023-MSD3) Prepared: 11/13/2019 10:56 Analyzed: 11/13/2019 12:11
Source: CC18215-01
Spike Source %REC RPD
Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes
Nitrite as N 1.0 B 0.10 mg/L 1.00 0.044 96 90-110 3 10
Batch 9K14026 - NO PREP
Blank (9K14026-BLK1)
Prepared: 11/18/2019 13:30 Analyzed: 11/18/2019 18:50
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
0.041
U
0.10
mg/L
LCS (91(14026-BS3)
Prepared: 11/18/2019 13:30 Analyzed: 11/18/2019 18:52
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
1.3
0.10
mg/L
1.25 100 90-110
Matrix Spike (9K34026-MS3)
Prepared: 11/18/2019 13:30 Analyzed: 11/18/2019 18:56
Source: CC17679-03
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
6.0
E
0.10
mg/L
0.521 5.4 109 90-110
Matrix Spike (9K34026-MS2)
Prepared: 11/18/2019 13:30 Analyzed: 11/18/2019 19:01
Source: CC18272-09
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
0.50
0.10
mg/L
0.521 0.041 U 97 90-110
Matrix Spike Dup (9K14026-MSD3)
Prepared: 11/18/2019 13:30 Analyzed: 11/18/2019 18:57
Source: CC17679-03
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
6.1
E
0.10
mg/L
0.521 5.4 121 90-110 1
10
QM-02
Batch 9K14035 - NO PREP
Blank (9K14035-BLK1)
Prepared: 11/14/2019 19:02 Analyzed: 11/14/2019 19:02
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
0.045
U
0.10
mg/L
LCS (9K34035-BS3)
Prepared: 11/14/2019 19:04 Analyzed: 11/14/2019 19:04
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
0.98
0.10
mg/L
1.01 97 90-110
Matrix Spike (9K34035-MS1)
Prepared: 11/15/2019 14:58 Analyzed: 11/15/2019 14:58
Source: CC16542-02
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
0.34
0.10
mg/L
0.393 0.045 U 86 90-110
QM-07
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 25 of 28

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9K14035 - NO PREP - Continued
Matrix Spike (9K34035-MS2)
Prepared: 11/15/2019 15:03 Analyzed: 11/15/2019 15:03
Source: CC17679-02
Spike Source %REC
RPD
Analvte
Result Flaq
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
1.1
0.10
mg/L
0.393 0.80 73 90-110
QM-07
Matrix Spike Dup (9K34035-MSD3)
Prepared: 11/15/2019 15:00 Analyzed: 11/15/2019 15:00
Source: CC16542-02
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
0.33
0.10
mg/L
0.393 0.045 U 84 90-110 2
10
QM-07
Batch 9K25025 - NO PREP
Blank (9K25025-BLKS) Prepared: 11/25/2019 10:26 Analyzed: 11/25/2019 21:41
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Chloride 2.2 U 5.0 mg/L
Sulfate as SO4 2.9 U 5.0 mg/L
LCS (9K25025-BSI) Prepared: 11/25/2019 10:26 Analyzed: 11/25/2019 21:58
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Chloride
50
5.0
mg/L
50.0 100 90-110
Sulfate as SO4
50
5.0
mg/L
50.0 100 90-110
Matrix Spike (9K25025-MS3)
Prepared: 11/25/2019 10:26 Analyzed: 11/25/2019 23:09
Source: CC18022-01
Spike Source %REC
RPD
Analvte
Result Flaq
Q
Units
Level Result %REC Limits RPD
Limit Notes
Chloride
42
5.0
mg/L
20.0 21 103 90-110
Sulfate as SO4
42
5.0
mg/L
20.0 21 103 90-110
Matrix Spike (9K25025-MS2)
Prepared: 11/25/2019 10:26 Analyzed: 11/26/2019 00:02
Source: CC18022-02
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Chloride
52
5.0
mg/L
20.0 31 105 90-110
Sulfate as SO4
18
5.0
mg/L
20.0 2.9 U 91 90-110
Matrix Spike Dup (9K25025-MSD3)
Prepared: 11/25/2019 10:26 Analyzed: 11/25/2019 23:27
Source: CC18022-01
Spike
Source
%REC
RPD
Analvte Result Flaq POL Units
Level
Result
%REC Limits RPD
Limit Notes
Chloride 42 5.0 mg/L
20.0
21
105 90-110 1
10
Sulfate as SO4 42 5.0 mg/L
20.0
21
105 90-110 0.9
10
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 26 of 28

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
3-01 Result may be biased high due to positive results in the associated method blank at a concentration above
the MDL and/or greater than one-half the MRL.
LP-03 Sample amount received by the laboratory did not meet minimum method requirements for analysis.
Q-01 Analysis performed outside of method - specified holding time.
QB-01 The method blank had a positive result for the analyte; however, the concentration in the method blank is
less than 10% of the sample result. There is minimal impact to the data.
QM-02 The RPD and/or percent recovery for this QC spike sample cannot be accurately calculated due to the high
concentration of analyte present in the sample.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 27 of 28

w� 10775 Central Port Dr. 010 Fxecufive Park Court, Suite Ill 102-A Woodwinds Industrial Cl.
Orlando, FL 32824 Jacksonville, FL 32216-6069 Cary, NC 27511
[phone] Fax (407) 85"945 [phone] Fax [phone] [phone] Fax (919j 467-3515 Page Of
Client Name Project Number Requested Anslyses Requested Turnaround
Novozymes North America (N0008) [none] Times
Address Project Name/Desc > Note : Rush requests subject to
77 Perry Chapel Church Road RQ Pilot rtr O I acceptance by the facility
CitylSTfZlp PO # / Billing Into S r 9 L
Franklinton, NC 27525 4550996257 '� �
{ ❑ Standard
Tel Fax Reporting Contact n ,� Q
[phone] Scot Creech 8888' � � � _Expedited
Sampler(s) Name, Affiliation (Print) Billing Contact U N /� co
s Accounts Payable m va Due 1
Sampler(s) Signature Site LocatioA 1 Time Zone 3 ' Q = CO) tab Woricarder
.79 10. m U U 2 LL (1) V) (—
Preservation (See Codes) (Combine as necessary) CC 17679
Collection Matrix Total k of
Item kSample ID (Fold Idenfificalion) Collection Date Time Comp 1 Grab (see codes) Containers Sample Comments
MBBR Feed Ik" 1630
RO Feed 6 - -0 ( b7 D
�f-y-fit ��30
—Total # of Containers
Sample Kit Prepared By
DaieiTime
Relinquished By
DalelTme
Received By
DateMme . .
j
Commems/Special Reporting Requirements
Relinquished By
DalwTima
Rec ive By
DalwTima
1[ 5
Relinquished By
DatetTme
Rilceived By
DateTme
Co ler 4's & Temps on Receipt
Condition U n Receipt
Acceptable Unacceptable
Matrix - GW-Groundwater SO -Soil DW-Drinking Water SE -Sediment SW-Suriace Water WW-Wastewater A -Air O-Other (detail in comments) Preservation: I -Ice H-HCI N-HNO3 S-H2SO4 NO-NaOH O-Other (detait In comments)
Note: All samples submitted to FNCO Labs are in accordance with the terms and conditions listed on the reverse of this form, unless prior written agreements exist

Sample Preservation Verification.
ENCO Cary
Work Order: CC17679 Project: RO Pilot
Client: Novozymes North America (N0008) Project #r:: [none]
Logged in: 05-Nov-19 10:08 f Logged By: ,John C King
Preservation Check Performed By: t Date/Time:
CC17679-01
Cont
Type
Pres (pH)
pH Checked /
pH Adjusted DateMme
Reagent Used/Comments
Requirement
In Control
Adjusted
C
250mLP+HNO3
<2
_Y / N / NA
Y If 1 NA
CC17679-02
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted DatefFirne
Adjusted
Reagent Used/Comments
B
250mLP+HNO3
<2
/ N I NA
Y 1 NA
C
250mLP+NaOH
>12
/ N / NA
Y /($II 1 NA
E
500mLP+H2SO4
<2
Y 1 N/ NA
Y/ 0 1 NA
C C 17679-03
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted Date/Time
Adjusted
Reagent Used/Comments
B
250mLP+HNO3
<2
I N/ NA
Y N/ NA
C
250mLP+NaOH
>12Y
/ N I NA
Y I 1 NA
E
504mLP+H2SO4
<2
Y 1 N/ NA
Y NA
CC17679-04
Cant
Type.
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted Date/Time
Adjusted
Reagent Used/Comments
8
250mLP+HNO3
<2
Y / ;)/ NA
IJ / N / NA
C
250mLP+NaOH
>12
1 N/ NA
Y /C� 1 NA
E
500mLP+H2SO4
1 <2
Z�y N / NA
Y / / NA
Reagent Name ID
1 �-- N ) L)---Q) I�`� 5
2
pH Strip ID: L
Reagent Name ID
3
4
Rea ent Name ID
5
6
C:%ELMNT1Printlwko_PreservationCheck .rpt Page 1

2�SENCO Laboratories
9g
Accurate. Timely. Respousive. luuavative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Friday, December 13, 2019
Novozymes North America (N0008)
Attn: Scott Creech
77 Perry Chapel Church Road
Franklinton, NC 27525
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: RO Pilot
ENCO Workorder(s): CC19005
Dear Scott Creech,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, November 12, 2019.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
OUCLC'=-:�CA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 28

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: MBBR Feed
Lab ID: CC19005-01
Sampled: 11/11/19 13:30
Received: 11/12/19
11:46
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 6010D
EPA 3005A
05/09/20
11/12/19
16:24
11/15/19
13:18
SM 5210 B-2011
NO PREP
11/13/19
13:30
11/13/19
11:47
11/13/19
11:47
Client ID: RO Feed
Lab ID: CC19005-02
Sampled: 11/11/19 13:30
Received: 11/12/19
11:46
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
CALC
[CALC]
12/09/19
11/14/19
11:53
11/25/19
16:53
EPA 300.0
NO PREP
12/09/19
11/26/19
15:40
11/27/19
09:13
EPA 310.2
NO PREP
11/25/19
11/13/19
11:53
11/13/19
14:47
EPA 335.4
Same
11/25/19
11/19/19
09:47
11/20/19
11:13
EPA 350.1
NO PREP
12/09/19
12/02/19
17:59
12/02/19
17:59
EPA 351.2
Same
12/09/19
11/14/19
11:53
11/25/19
16:53
EPA 353.2
[CALC]
11/13/19
13:30
11/12/19
17:25
11/12/19
17:25
EPA 353.2
NO PREP
11/13/19
13:30
11/12/19
17:25
11/12/19
17:25
EPA 365.1
NO PREP
11/13/19
13:30
11/13/19
12:47
11/13/19
12:47
EPA 7470A
EPA 7470A
12/09/19
11/18/19
09:51
11/19/19
12:37
SM 213OB-2011
NO PREP
11/13/19
13:30
11/13/19
08:46
11/13/19
08:46
SM 251OB-2011
NO PREP
12/09/19
11/14/19
08:40
11/14/19
08:40
SM 254OC-2011
NO PREP
11/18/19
11/18/19
08:55
11/18/19
08:55
SM 2540D-2011
NO PREP
11/18/19
11/14/19
14:49
11/14/19
14:49
SM 4500002 D-2011
NO PREP
08/06/22
11/22/19
11:32
11/22/19
11:32
SM 4500H+B-2011
NO PREP
11/11/19
13:44
11/15/19
13:20
11/15/19
13:20
SM 5220D-2011
Same
12/09/19
11/14/19
11:35
11/14/19
16:40
Client ID: RO Feed
Lab ID: CC19005-02RE1
Sampled: 11/11/19 13:30
Received: 11/12/19
11:46
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 365.4
Same
12/09/19
11/14/19
11:53
11/26/19
14:12
EPA 6010D
EPA 3005A
05/09/20
12/09/19
12:29
12/10/19
11:50
Client ID: RO Permeate
Lab ID: CC19005-03
Sampled: 11/11/19 13:30
Received: 11/12/19
11:46
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
CALC
[CALC]
12/09/19
11/22/19
10:22
11/25/19
16:55
EPA 300.0
NO PREP
12/09/19
11/26/19
15:40
11/27/19
09:31
EPA 310.2
NO PREP
11/25/19
11/13/19
11:53
11/13/19
14:45
EPA 335.4
Same
11/25/19
11/19/19
09:47
11/20/19
11:14
EPA 350.1
NO PREP
12/09/19
12/02/19
18:01
12/02/19
18:01
EPA 351.2
Same
12/09/19
11/14/19
11:53
11/25/19
16:55
EPA 353.2
NO PREP
11/13/19
13:30
11/12/19
17:06
11/12/19
17:06
EPA 353.2
[CALC]
11/13/19
13:30
11/22/19
10:22
11/22/19
15:32
EPA 353.2
NO PREP
12/09/19
11/22/19
10:22
11/22/19
15:32
EPA 365.1
NO PREP
11/13/19
13:30
11/13/19
12:50
11/13/19
12:50
EPA 365.4
Same
12/09/19
11/14/19
11:53
11/25/19
18:26
EPA 7470A
EPA 7470A
12/09/19
11/18/19
09:51
11/19/19
12:45
SM 213OB-2011
NO PREP
11/13/19
13:30
11/13/19
08:46
11/13/19
08:46
SM 251OB-2011
NO PREP
12/09/19
11/14/19
08:40
11/14/19
08:40
SM 254OC-2011
NO PREP
11/18/19
11/18/19
08:55
11/18/19
08:55
SM 2540D-2011
NO PREP
11/18/19
11/14/19
14:49
11/14/19
14:49
SM 4500002 D-2011
NO PREP
08/06/22
11/22/19
11:32
11/22/19
11:32
SM 4500H+B-2011
NO PREP
11/11/19
13:44
11/15/19
13:20
11/15/19
13:20
SM 5210 B-2011
NO PREP
11/13/19
13:30
11/13/19
11:47
11/13/19
11:47
SM 5220D-2011
Same
12/09/19
11/14/19
11:35
11/14/19
16:40
Client ID: RO Permeate
Lab ID: CC19005-03RE1
Sampled: 11/11/19 13:30
Received: 11/12/19
11:46
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 6010D
EPA 3005A
05/09/20
12/10/19
10:04
12/11/19
12:24
FINAL
This report relates only to the sample
as received by the laboratory, and may only be reproduced in full.
Page 2 of 28

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: RO Reject
Lab ID: CC19005-04
Sampled: 11/11/19 13:30
Received: 11/12/19 11:46
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
CALC
[CALC]
12/09/19
11/14/19 11:53
11/26/19 12:31
EPA 310.2
NO PREP
11/25/19
11/13/19 11:53
11/13/19 14:48
EPA 335.4
Same
11/25/19
11/19/19 09:47
11/20/19 11:20
EPA 350.1
NO PREP
12/09/19
12/02/19 18:03
12/02/19 18:03
EPA 353.2
[CALC]
11/13/19 13:30
11/12/19 18:06
11/12/19 18:06
EPA 365.1
NO PREP
11/13/19 13:30
11/13/19 13:09
11/13/19 13:09
EPA 365.4
Same
12/09/19
11/14/19 11:53
11/25/19 18:27
EPA 7470A
EPA 7470A
12/09/19
11/18/19 09:51
11/19/19 12:47
SM 213OB-2011
NO PREP
11/13/19 13:30
11/13/19 08:46
11/13/19 08:46
SM 251OB-2011
NO PREP
12/09/19
11/14/19 08:40
11/14/19 08:40
SM 254OC-2011
NO PREP
11/18/19
11/18/19 08:55
11/18/19 08:55
SM 2540D-2011
NO PREP
11/18/19
11/14/19 14:49
11/14/19 14:49
SM 4500002 D-2011
NO PREP
08/06/22
11/22/19 11:32
11/22/19 11:32
SM 4500H+B-2011
NO PREP
11/11/19 13:44
11/15/19 13:20
11/15/19 13:20
SM 5220D-2011
Same
12/09/19
11/14/19 11:35
11/14/19 16:40
Client ID: RO Reject
Lab ID: CC19005-04RE1
Sampled: 11/11/19 13:30
Received: 11/12/19 11:46
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 300.0
NO PREP
12/09/19
11/27/19 15:32
11/28/19 01:57
EPA 351.2
Same
12/09/19
11/14/19 11:53
11/26/19 12:31
EPA 353.2
NO PREP
11/13/19 13:30
11/12/19 18:06
11/12/19 18:06
EPA 6010D
EPA 3005A
05/09/20
12/10/19 10:04
12/11/19 15:49
Client ID: RO Reject
Lab ID: CC19005-04RE2
Sampled: 11/11/19 13:30
Received: 11/12/19 11:46
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 300.0
NO PREP
12/09/19
11/27/19 15:32
11/28/19 02:14
EPA 6010D
EPA 3005A
05/09/20
12/10/19 10:04
12/11/19 12:28
Client ID: MBBR Feed
Lab ID: CC19005-05
Sampled: 11/11/19 13:30
Received: 11/12/19 11:46
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
05/09/20
11/14/19 10:04
11/18/19 13:38
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 28

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SAMPLE DETECTION SUMMARY
Client ID: MBBR Feed
Lab ID:
CC19005-01
Anala
Results
Flag
MDL
POLL
Units
Method
Notes
Calcium - Dissolved
78.1
0.0390
0.100
mg/L
EPA 6010D
Magnesium - Dissolved
5000
29.0
100
ug/L
EPA 6010D
Silica (Si02) - Dissolved
18.7
0.03
0.2
mg/L
EPA 6010D
Client ID: RO Feed
Lab ID:
CC19005-02
Anala
Results
Flag
MDL
POLL
Units
Method
Notes
Ammonia as N
1.1
0.045
0.10
mg/L
EPA 350.1
Bicarbonate (as CaCO3)
870
14
15
mg/L
SM 4500002 D-2011
Chemical Oxygen Demand
84
10
10
mg/L
SM 5220D-2011
Chloride
390
D
22
50
mg/L
EPA 300.0
Nitrite as N
23
D
0.45
2.7
mg/L
EPA 353.2
Orthophosphate as P
3.7
B
0.16
0.50
mg/L
EPA 365.1
QB-01
pH
8.2
1.0
1.0
pH
SM 4500H+B-2011
Q-01
Specific Conductance (EC) at 25 Deg C
3700
1.0
1.0
umhos/cm
SM 251OB-2011
Sulfate as SO4
87
D
29
50
mg/L
EPA 300.0
Temperature for pH (deg. C)
17
pH
SM 4500H+B-2011
Q-01
Total Alkalinity as CaCO3
880
D
140
150
mg/L
EPA 310.2
Total Dissolved Solids
2400
50
50
mg/L
SM 2540C-2011
Total Kjeldahl Nitrogen
5.4
0.26
0.48
mg/L
EPA 351.2
Total Nitrogen
5.4
0.26
0.48
mg/L
CALC
Client ID: RO Feed
Lab ID:
CC19005-02RE1
Anala
Results
Flag
MDL
POLL
Units
Method
Notes
Aluminum - Total
0.108
0.0420
0.100
mg/L
EPA 6010D
Boron - Total
0.0443
J
0.00570
0.0500
mg/L
EPA 6010D
Calcium - Total
82.5
0.0390
0.100
mg/L
EPA 6010D
Chromium - Total
0.00160
J
0.00140
0.0100
mg/L
EPA 6010D
Copper - Total
0.00518
J
0.00160
0.0100
mg/L
EPA 6010D
Iron - Total
0.0806
0.0220
0.0500
mg/L
EPA 6010D
Magnesium - Total
5.07
0.0290
0.100
mg/L
EPA 6010D
Nickel - Total
0.00266
J
0.00220
0.0100
mg/L
EPA 6010D
Phosphorus
3.8
D
0.050
0.20
mg/L
EPA 365.4
Potassium - Total
520
0.150
0.500
mg/L
EPA 6010D
Silica (Si02) - Total
20.1
0.03
0.2
mg/L
EPA 6010D
Sodium - Total
487
0.400
0.500
mg/L
EPA 6010D
Zinc - Total
0.00479
J
0.00440
0.0100
mg/L
EPA 6010D
Client ID: RO Permeate
Lab ID:
CC19005-03
Anala
Results
Flag
MDL
POLL
Units
Method
Notes
Ammonia as N
0.34
0.045
0.10
mg/L
EPA 350.1
Bicarbonate (as CaCO3)
19
14
15
mg/L
SM 4500002 D-2011
Chloride
6.6
2.2
5.0
mg/L
EPA 300.0
Nitrate as N
4.5
D
0.20
0.50
mg/L
EPA 353.2
Nitrate/Nitrite as N
6.4
D
0.20
0.50
mg/L
EPA 353.2
Nitrite as N
2.0
D
0.084
0.50
mg/L
EPA 353.2
Orthophosphate as P
0.27
JB
0.16
0.50
mg/L
EPA 365.1
J-01
pH
5.6
1.0
1.0
pH
SM 4500H+B-2011
Q-01
Specific Conductance (EC) at 25 Deg C
130
1.0
1.0
umhos/cm
SM 251OB-2011
Temperature for pH (deg. C)
17
pH
SM 4500H+B-2011
Q-01
Total Alkalinity as CaCO3
19
14
15
mg/L
EPA 310.2
Total Dissolved Solids
64
50
50
mg/L
SM 2540C-2011
Total Kjeldahl Nitrogen
0.30
J
0.26
0.48
mg/L
EPA 351.2
Total Nitrogen
6.7
D
0.26
0.50
mg/L
CALC
Client ID: RO Permeate
Lab ID:
CC19005-03RE1
Anala
Results
Flag
MDL
POLL
Units
Method
Notes
Boron - Total
0.0205
J
0.00570
0.0500
mg/L
EPA 6010D
Calcium - Total
0.300
0.0390
0.100
mg/L
EPA 6010D
Potassium - Total
21.5
0.150
0.500
mg/L
EPA 6010D
Silica (Si02) - Total
0.1
J
0.03
0.2
mg/L
EPA 6010D
Sodium - Total
10.8
0.400
0.500
mg/L
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 28

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SAMPLE DETECTION SUMMARY
Client ID: RO Reject
Lab ID:
CC19005-04
Anala
Results
Flag
MDL
4
Units
Method
Notes
Ammonia as N
8.3
D
0.22
0.50
mg/L
EPA 350.1
Bicarbonate (as CaCO3)
2100
14
15
mg/L
SM 4500002 D-2011
Chemical Oxygen Demand
690
20
20
mg/L
SM 5220D-2011
Cyanide (total)
0.095
0.0049
0.0050
mg/L
EPA 335.4
Orthophosphate as P
35
BD
0.80
2.5
mg/L
EPA 365.1
QB-01
pH
7.3
1.0
1.0
pH
SM 4500H+B-2011
Q-01
Phosphorus
46
D
1.2
5.0
mg/L
EPA 365.4
Specific Conductance (EC) at 25 Deg C
26000
1.0
1.0
umhos/cm
SM 251OB-2011
Temperature for pH (deg. C)
18
pH
SM 4500H+B-2011
Q-01
Total Alkalinity as CaCO3
2100
D
280
300
mg/L
EPA 310.2
Total Dissolved Solids
22000
50
50
mg/L
SM 2540C-2011
Total Nitrogen
34
D
0.52
0.96
mg/L
CALC
Turbidity
1.1
0.50
1.0
NTU
SM 213OB-2011
Client ID: RO Reject
Lab ID:
CC19005-04RE3
Anala
Results
Flag
MDL
4
Units
Method
Notes
Aluminum - Total
0.474
0.0420
0.100
mg/L
EPA 6010D
Boron - Total
0.191
0.00570
0.0500
mg/L
EPA 6010D
Chloride
3300
D
110
250
mg/L
EPA 300.0
Chromium - Total
0.00782
1
0.00140
0.0100
mg/L
EPA 6010D
Copper - Total
0.0221
0.00160
0.0100
mg/L
EPA 6010D
Iron - Total
0.638
0.0220
0.0500
mg/L
EPA 6010D
Lead - Total
0.0112
0.00310
0.0100
mg/L
EPA 6010D
Magnesium - Total
40.5
0.0290
0.100
mg/L
EPA 6010D
Molybdenum - Total
0.00811
1
0.00250
0.0100
mg/L
EPA 6010D
Nickel - Total
0.0151
0.00220
0.0100
mg/L
EPA 6010D
Nitrite as N
21
D
1.3
8.0
mg/L
EPA 353.2
Silica (Si02) - Total
190
0.03
0.2
mg/L
EPA 6010D
Total Kjeldahl Nitrogen
34
D
0.52
0.96
mg/L
EPA 351.2
Zinc - Total
0.0154
0.00440
0.0100
mg/L
EPA 6010D
Client ID: RO Reject
Lab ID:
CC19005-04RE2
Anala
Results
Flag
MDL
4
Units
Method
Notes
Calcium - Total
633
D
0.390
1.00
mg/L
EPA 6010D
Potassium - Total
3910
D
1.50
5.00
mg/L
EPA 6010D
Sodium - Total
3910
D
4.00
5.00
mg/L
EPA 6010D
Sulfate as SO4
6300
D
290
500
mg/L
EPA 300.0
Client ID: MBBR Feed
Lab ID:
CC19005-05
Anala
Results
Flag
MDL
4
Units
Method
Notes
Silica (Si02) - Total
32.3
0.1
1.1
mg/L
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 28

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ANALYTICAL RESULTS
Description: MBBR Feed Lab Sample ID:CC19005-01 Received: 11/12/19 11:46
Matrix: Waste Water Sampled:11/11/19 13:30 Work Order: CC19005
Project: RO Pilot Sampled By: Scott Creech
Metals (Dissolved) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flao
Units
DF
MOIL
P L
Batch
Method
Analyzed
By Notes
Calcium [7440-70-2]^ 78.1
mg/L
1
0.0390
0.100
9K12043
EPA 6010D
11/15/19 13:18
JDH
Magnesium [7439-95-4]^ 5000
ug/L
1
29.0
100
9K12043
EPA 6010D
11/15/19 13:18
JDH
Silica (Si02) [763-18-69]^ 18.7
mg/L
1
0.03
0.2
9K12043
EPA 6010D
11/15/19 13:18
JDH
Classical Chemistry Parameters (Dissolved)
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flao
Units
OF
MOIL
P L
Batch
Method
Analyzed
By Notes
Biochemical Oxygen Demand^ 2.0 U
mg/L
1
2.0
2.0
9K13008
SM 5210 B-2011
11/13/19 11:47
JOC
Description: RO Feed Lab Sample ID:CC19005-02 Received: 11/12/19 11:46
Matrix: Waste Water Sampled:11/11/19 13:30 Work Order: CC19005
Project: RO Pilot Sampled By: Scott Creech
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MOIL
P L
Batch
Method
Analyzed
By
Notes
Mercury[7439-97-6]^
0.000750
U
mg/L
5
0.000750
0.00100
9K18016
EPA 7470A
11/19/19 12:37
KAH
Silica (Si02) [763-18-69]^
20.1
mg/L
1
0.03
0.2
9LO9022
EPA 6010D
12/10/19 11:50
JDH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MOIL
P L
Batch
Method
Analyzed
By
Notes
Aluminum [7429-90-5]^
0.108
mg/L
1
0.0420
0.100
9LO9022
EPA 6010D
12/10/19 11:50
JDH
Arsenic[7440-38-2]^
0.00760
U
mg/L
1
0.00760
0.0100
9LO9022
EPA 6010D
12/10/19 11:50
JDH
Boron [7440-42-8]^
0.0443
J
mg/L
1
0.00570
0.0500
9LO9022
EPA 6010D
12/10/19 11:50
JDH
Cadmium [7440-43-9]^
0.000360
U
mg/L
1
0.000360
0.00100
9LO9022
EPA 6010D
12/10/19 11:50
JDH
Calcium [7440-70-2]^
82.5
mg/L
1
0.0390
0.100
9LO9022
EPA 6010D
12/10/19 11:50
JDH
Chromium [7440-47-3]^
0.00160
J
mg/L
1
0.00140
0.0100
9LO9022
EPA 6010D
12/10/19 11:50
JDH
Copper[7440-50-8]^
0.00518
J
mg/L
1
0.00160
0.0100
9LO9022
EPA 6010D
12/10/19 11:50
JDH
Iron [7439-89-6]^
0.0806
mg/L
1
0.0220
0.0500
9LO9022
EPA 6010D
12/10/19 11:50
JDH
Lead [7439-92-1]^
0.00310
U
mg/L
1
0.00310
0.0100
9LO9022
EPA 6010D
12/10/19 11:50
JDH
Magnesium [7439-95-4]^
5.07
mg/L
1
0.0290
0.100
9LO9022
EPA 6010D
12/10/19 11:50
JDH
Molybdenum [7439-98-7]^
0.00250
U
mg/L
1
0.00250
0.0100
9LO9022
EPA 6010D
12/10/19 11:50
JDH
Nickel[7440-02-O]^
0.00266
J
mg/L
1
0.00220
0.0100
9LO9022
EPA 6010D
12/10/19 11:50
JDH
Potassium [7440-09-7]^
520
mg/L
1
0.150
0.500
9LO9022
EPA 6010D
12/10/19 11:50
JDH
Selenium [7782-49-2]^
0.00620
U
mg/L
1
0.00620
0.0100
9LO9022
EPA 6010D
12/10/19 11:50
JDH
QB-02
Silver[7440-22-4]^
0.00190
U
mg/L
1
0.00190
0.0100
9LO9022
EPA 6010D
12/10/19 11:50
JDH
Sodium [7440-23-5]^
487
mg/L
1
0.400
0.500
9LO9022
EPA 6010D
12/10/19 11:50
JDH
Zinc[7440-66-6]^
0.00479
J
mg/L
1
0.00440
0.0100
9LO9022
EPA 6010D
12/10/19 11:50
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MOIL
P L
Batch
Method
Analyzed
By
Notes
Ammonia as N [7664-41-7]^
1.1
mg/L
1
0.045
0.10
9LO2040
EPA 350.1
12/02/19 17:59
AKF
Bicarbonate (as CaCO3)[71-52-3]
870
mg/L
1
14
15
91<22028
M 45000O2 D-201
11/22/19 11:32
JAH
Carbonate (as CaCO3)[3812-32-6]
14
U
mg/L
1
14
15
91<22028
M 45000O2 D-201
11/22/19 11:32
JAH
Chemical Oxygen Demand^
84
mg/L
1
10
10
9K14025
SM 5220D-2011
11/14/19 16:40
JOC
Chloride [16887-00-6]^
390
D
mg/L
10
22
50
91<26034
EPA 300.0
11/27/19 09:13
PDK
Cyanide (total) [57-12-5]^
0.0049
U
mg/L
1
0.0049
0.0050
9K15003
EPA 335.4
11/20/19 11:13
AKF
FINAL
This report relates only
to the sample as received by the laboratory,
and may only
be reproduced
in full.
Page 6 of 28

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www.encolabs.com
ANALYTICAL RESULTS
Description: RO Feed Lab Sample ID:CC19005-02 Received: 11/12/19 11:46
Matrix: Waste Water Sampled:11/11/19 13:30 Work Order: CC19005
Project: RO Pilot Sampled By: Scott Creech
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results
Flao
Units
DF
MDL
P L
Batch
Method
Analyzed
By
Notes
Nitrate as N [14797-55-8]
0.45
UD
mg/L
27
0.45
2.7
[CALC]
EPA 353.2
11/12/19 17:25
PDK
Nitrite as N [14797-65-0]^
23
D
mg/L
26.67
0.45
2.7
9K12037
EPA 353.2
11/12/19 17:25
PDK
Orthophosphate as P [1426-54-42]^
3.7
B
mg/L
1
0.16
0.50
9K13011
EPA 365.1
11/13/19 12:47
AKF
QB-01
pH^
8.2
pH
1
1.0
1.0
9K15023
iM 4500H+B-2011
11/15/19 13:20
BDC
Q-01
Phosphorus[7723-14-O]^
3.8
D
mg/L
2
0.050
0.20
9K14010
EPA 365.4
11/26/19 14:12
AKF
Specific Conductance (EC) at 25 Deg
3700
umhos/cm
1
1.0
1.0
9K14007
SM 251OB-2011
11/14/19 08:40
JOC
C^
Sulfate as SO4 [14808-79-8]^
87
D
mg/L
10
29
50
9K26034
EPA 300.0
11/27/19 09:13
PDK
Temperature for pH (deg. C)
17
pH
1
9K15023
iM 4500H+B-2011
11/15/19 13:20
BDC
Q-01
Total Alkalinity as CaCO3 [471-34-1]^
880
D
mg/L
10
140
150
9K13027
EPA 310.2
11/13/19 14:47
AKF
Total Dissolved Solids^
2400
mg/L
1
50
50
9K16001
SM 2540C-2011
11/18/19 08:55
JOC
Total Kjeldahl Nitrogen^
5.4
mg/L
1
0.26
0.48
9K14011
EPA 351.2
11/25/19 16:53
AKF
Total Nitrogen [17778-88-0]
5.4
mg/L
1
0.26
0.48
[CALC]
CALC
11/25/19 16:53
AKF
Total Suspended Solids^
2.5
U
mg/L
1
2.5
2.5
9K14040
SM 2540D-2011
11/14/19 14:49
BDC
Turbidity^
0.50
U
NTU
1
0.50
1.0
9K13009
SM 213OB-2011
11/13/19 08:46
JOC
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 28

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ANALYTICAL RESULTS
Description: RO Permeate Lab Sample ID:CC19005-03 Received: 11/12/19 11:46
Matrix: Waste Water Sampled:11/11/19 13:30 Work Order: CC19005
Project: RO Pilot Sampled By: Scott Creech
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary ced1fied analyte [NC 591]
Analyte rCAS Numberl
Results
Flao
Units
DF
MDL
P L
Batch
Method
Analyzed
-By Notes
Mercury[7439-97-6]^
0.000750
U
mg/L
5
0.000750
0.00100
9K18016
EPA 7470A
11/19/19 12:45
KAH
Silica (Si02) [763-18-69]A
0.1
J
mg/L
1
0.03
0.2
9LO9022
EPA 6010D
12/11/19 12:24
JDH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flao
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Aluminum [7429-90-5]^
0.0420
U
mg/L
1
0.0420
0.100
9LO9022
EPA 6010D
12/11/19 12:24
JDH
Arsenic[7440-38-2]^
0.00760
U
mg/L
1
0.00760
0.0100
9LO9022
EPA 6010D
12/11/19 12:24
JDH
Boron [7440-42-8]A
0.0205
J
mg/L
1
0.00570
0.0500
9LO9022
EPA 6010D
12/11/19 12:24
JDH
Cadmium [7440-43-9]^
0.000360
U
mg/L
1
0.000360
0.00100
9LO9022
EPA 6010D
12/11/19 12:24
JDH
Calcium [7440-70-2]A
0.300
mg/L
1
0.0390
0.100
9LO9022
EPA 6010D
12/11/19 12:24
JDH
Chromium [7440-47-3]^
0.00140
U
mg/L
1
0.00140
0.0100
9LO9022
EPA 6010D
12/11/19 12:24
JDH
Copper[7440-50-8]^
0.00160
U
mg/L
1
0.00160
0.0100
9LO9022
EPA 6010D
12/11/19 12:24
JDH
Iron [7439-89-6]^
0.0220
U
mg/L
1
0.0220
0.0500
9LO9022
EPA 6010D
12/11/19 12:24
JDH
Lead [7439-92-1]^
0.00310
U
mg/L
1
0.00310
0.0100
9LO9022
EPA 6010D
12/11/19 12:24
JDH
Magnesium [7439-95-4]^
0.0290
U
mg/L
1
0.0290
0.100
9LO9022
EPA 6010D
12/11/19 12:24
JDH
Molybdenum [7439-98-7]^
0.00250
U
mg/L
1
0.00250
0.0100
9LO9022
EPA 6010D
12/11/19 12:24
JDH
Nickel[7440-02-0]^
0.00220
U
mg/L
1
0.00220
0.0100
9LO9022
EPA 6010D
12/11/19 12:24
JDH
Potassium [7440-09-7]A
21.5
mg/L
1
0.150
0.500
9LO9022
EPA 6010D
12/11/19 12:24
JDH
Selenium [7782-49-2]^
0.00620
U
mg/L
1
0.00620
0.0100
9LO9022
EPA 6010D
12/11/19 12:24
JDH
Silver[7440-22-4]^
0.00190
U
mg/L
1
0.00190
0.0100
9LO9022
EPA 6010D
12/11/19 12:24
JDH
Sodium [7440-23-5]A
10.8
mg/L
1
0.400
0.500
9LO9022
EPA 6010D
12/11/19 12:24
JDH
Zinc[7440-66-6]^
0.00440
U
mg/L
1
0.00440
0.0100
9LO9022
EPA 6010D
12/11/19 12:24
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flao
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Ammonia as N [7664-41-7]A
0.34
mg/L
1
0.045
0.10
9LO2040
EPA 350.1
12/02/19 18:01
AKF
Bicarbonate (as CaCO3)[71-52-3]
19
mg/L
1
14
15
91<22028
M 4500002 D-201
11/22/19 11:32
JAH
Carbonate (as CaCO3)[3812-32-6]
14
U
mg/L
1
14
15
91<22028
M 4500002 D-201
11/22/19 11:32
JAH
Chemical Oxygen Demand^
10
U
mg/L
1
10
10
9K14025
SM 5220D-2011
11/14/19 16:40
JOC
Chloride [ 16887-00-6] A
6.6
mg/L
1
2.2
5.0
91<26034
EPA 300.0
11/27/19 09:31
PDK
Cyanide (total) [57-12-5]^
0.0049
U
mg/L
1
0.0049
0.0050
9K15003
EPA 335.4
11/20/19 11:14
AKF
Nitrate as N [14797-55-8]
4.5
D
mg/L
5
0.20
0.50
[CALC]
EPA 353.2
11/22/19 15:32
PDK
Nitrate/Nitrite as NA
6.4
D
mg/L
5
0.20
0.50
91<22022
EPA 353.2
11/22/19 15:32
AKF
Nitrite as N [ 14797-65-0] A
Orthophosphate as P [1426-54-42] A
pH
Phosphorus[7723-14-0]^
Specific Conductance (EC) at 25 Deg
CA
Sulfate as SO4 [14808-79-8]^
Temperature for pH (deg. C)
Total Alkalinity as CaCO3 [471-34-1]A
Total Dissolved Solids^
Total Kjeldahl Nitrogen
Total Nitrogen [17778-88-0]
Total Suspended Solids^
2.0
D
mg/L
0.27
JB
mg/L
5.6
pH
0.025
U
mg/L
130
umhos/cm
2.9
U
mg/L
17
pH
19
mg/L
64
mg/L
0.30
J
mg/L
6.7
D
mg/L
5.0
U
mg/L
5 0.084
0.50
9K12038
EPA 353.2
1 0.16
0.50
9K13011
EPA 365.1
1 1.0
1.0
9K15023
iM 4500H+B-2011
1 0.025
0.10
9K14010
EPA 365.4
1 1.0
1.0
9K14007
SM 251OB-2011
1 2.9
5.0
9K26034
EPA 300.0
1
9K15023
iM 450011+13-2011
1 14
15
9K13027
EPA 310.2
1 50
50
9K16001
SM 2540C-2011
1 0.26
0.48
9K14011
EPA 351.2
5 0.26
0.50
[CALC]
CALC
2 5.0
5.0
9K14040
SM 2540D-2011
11/12/19 17:06 PDK
11/13/19 12:50 AKF 3-01
11/15/19 13:20 BDC Q-01
11/25/19 18:26 AKF
11/14/19 08:40 JOC
11/27/19 09:31
PDK
11/15/19 13:20
BDC Q-01
11/13/19 14:45
AKF
11/18/19 08:55
JOC
11/25/19 16:55
AKF
11/25/19 16:55
AKF
11/14/19 14:49
BDC LP-03
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 28

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ANALYTICAL RESULTS
Description: RO Permeate Lab Sample ID:CC19005-03 Received: 11/12/19 11:46
Matrix: Waste Water Sampled:11/11/19 13:30 Work Order: CC19005
Project: RO Pilot Sampled By: Scott Creech
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
TurbidityA 0.50 U
NTU
1
0.50
1.0
9K13009
SM 213OB-2011
11/13/19 08:46
JOC
Classical Chemistry Parameters (Dissolved)
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Biochemical Oxygen DemandA 2.0 U
mg/L
1
2.0
2.0
9K13008
SM 5210 B-2011
11/13/19 11:47
JOC
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 28

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ANALYTICAL RESULTS
Description: RO Reject Lab Sample ID:CC19005-04 Received: 11/12/19 11:46
Matrix: Waste Water Sampled:11/11/19 13:30 Work Order: CC19005
Project: RO Pilot Sampled By: Scott Creech
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary cediFed analyte [NC 591]
Analyte rCAS Numberl Results Flao Units DF MDL P L Batch Method Analyzed -By Notes
Mercury[7439-97-6]^ 0.000750 U mg/L 5 0.000750 0.00100 9K18016 EPA 7470A 11/19/19 12:47 KAH
Silica (Si02) [763-18-69]^ 190 mg/L 1 0.03 0.2 9LO9022 EPA 6010D 12/11/19 15:49 JDH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flao
Units
DF
MDL
P L
Batch
Method
Analyzed
By
Notes
Aluminum [7429-90-5]^
0.474
mg/L
1
0.0420
0.100
9LO9022
EPA 6010D
12/11/19 15:49
JDH
Arsenic[7440-38-2]^
0.00760
U
mg/L
1
0.00760
0.0100
9LO9022
EPA 6010D
12/11/19 15:49
JDH
Boron [7440-42-8]^
0.191
mg/L
1
0.00570
0.0500
9LO9022
EPA 6010D
12/11/19 15:49
JDH
Cadmium [7440-43-9]^
0.000360
U
mg/L
1
0.000360
0.00100
9LO9022
EPA 6010D
12/11/19 15:49
JDH
Calcium [7440-70-2]^
633
D
mg/L
10
0.390
1.00
9LO9022
EPA 6010D
12/11/19 12:28
JDH
Chromium [7440-47-3]^
0.00782
J
mg/L
1
0.00140
0.0100
9LO9022
EPA 6010D
12/11/19 15:49
JDH
Copper[7440-50-8]^
0.0221
mg/L
1
0.00160
0.0100
9LO9022
EPA 6010D
12/11/19 15:49
JDH
Iron [7439-89-6]^
0.638
mg/L
1
0.0220
0.0500
9LO9022
EPA 6010D
12/11/19 15:49
JDH
Lead [7439-92-1]^
0.0112
mg/L
1
0.00310
0.0100
9LO9022
EPA 6010D
12/11/19 15:49
JDH
Magnesium [7439-95-4]^
40.5
mg/L
1
0.0290
0.100
9LO9022
EPA 6010D
12/11/19 15:49
JDH
Molybdenum [7439-98-7]^
0.00811
J
mg/L
1
0.00250
0.0100
9LO9022
EPA 6010D
12/11/19 15:49
JDH
Nickel[7440-02-O]^
0.0151
mg/L
1
0.00220
0.0100
9LO9022
EPA 6010D
12/11/19 15:49
JDH
Potassium [7440-09-7]1
3910
D
mg/L
10
1.50
5.00
9LO9022
EPA 6010D
12/11/19 12:28
JDH
Selenium [7782-49-2]^
0.00620
U
mg/L
1
0.00620
0.0100
9LO9022
EPA 6010D
12/11/19 15:49
JDH
Silver[7440-22-4]^
0.00190
U
mg/L
1
0.00190
0.0100
9LO9022
EPA 6010D
12/11/19 15:49
JDH
Sodium [7440-23-5]^
3910
D
mg/L
10
4.00
5.00
9LO9022
EPA 6010D
12/11/19 12:28
JDH
Zinc[7440-66-6]^
0.0154
mg/L
1
0.00440
0.0100
9LO9022
EPA 6010D
12/11/19 15:49
JDH
Classical Chemistry Parameters
^ - ENCO Cary cediFed analyte [NC 591]
Analyte rCAS Numberl
Results
Flao
Units
DF
MDL
P L
Batch
Method
Analyzed
-By
Notes
Ammonia as N [7664-41-7]^
8.3
D
mg/L
5
0.22
0.50
9LO2040
EPA 350.1
12/02/19 18:03
AKF
Bicarbonate (as CaCO3)[71-52-3]
2100
mg/L
1
14
15
91<22028
M 4500002 D-201
11/22/19 11:32
JAH
Carbonate (as CaCO3)[3812-32-6]
14
U
mg/L
1
14
15
91<22028
M 4500002 D-201
11/22/19 11:32
JAH
Chemical Oxygen Demand
690
mg/L
2
20
20
9K14025
SM 5220D-2011
11/14/19 16:40
JOC
Chloride [16887-00-6]^
3300
D
mg/L
50
110
250
91<27024
EPA 300.0
11/28/19 01:57
PDK
Cyanide (total)[57-12-5]^
0.095
mg/L
1
0.0049
0.0050
9K15003
EPA 335.4
11/20/19 11:20
AKF
Nitrate as N [14797-55-8]
1.3
UD
mg/L
80
1.3
8.0
[CALC]
EPA 353.2
11/12/19 18:06
PDK
Nitrite as N [14797-65-0]^
21
D
mg/L
80
1.3
8.0
9K12038
EPA 353.2
11/12/19 18:06
PDK
Orthophosphate as P [1426-54-42]^
35
BD
mg/L
5
0.80
2.5
9K13011
EPA 365.1
11/13/19 13:09
AKF
QB-01
pH
7.3
pH
1
1.0
1.0
9K15023
iM 4500H+B-2011
11/15/19 13:20
BDC
Q-01
Phosphorus[7723-14-0]^
46
D
mg/L
50
1.2
5.0
9K14010
EPA 365.4
11/25/19 18:27
AKF
Specific Conductance (EC) at 25 Deg
26000
umhos/cm
1
1.0
1.0
9K14007
SM 251OB-2011
11/14/19 08:40
JOC
C^
Sulfate as SO4 [14808-79-8]^
6300
D
mg/L
100
290
500
9K27024
EPA 300.0
11/28/19 02:14
PDK
Temperature for pH (deg. C)
18
pH
1
9K15023
iM 450011+13-2011
11/15/19 13:20
BDC
Q-01
Total Alkalinity as CaCO3 [471-34-1]^
2100
D
mg/L
20
280
300
9K13027
EPA 310.2
11/13/19 14:48
AKF
Total Dissolved Solids^
22000
mg/L
1
50
50
9K16001
SM 2540C-2011
11/18/19 08:55
JOC
Total Kjeldahl Nitrogen
34
D
mg/L
2
0.52
0.96
9K14011
EPA 351.2
11/26/19 12:31
AKF
Total Nitrogen [17778-88-0]
34
D
mg/L
2
0.52
0.96
[CALC]
CALC
11/26/19 12:31
AKF
Total Suspended Solids^
2.5
U
mg/L
1
2.5
2.5
9K14040
SM 2540D-2011
11/14/19 14:49
BDC
Turbidity^
1.1
NTU
1
0.50
1.0
9K13009
SM 213OB-2011
11/13/19 08:46
JOC
FINAL
This report relates only
to the sample as received by the laboratory,
and may only
be reproduced
in full.
Page 10 of 28

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ANALYTICAL RESULTS
Description: MBBR Feed Lab Sample ID:CC19005-05 Received: 11/12/19 11:46
Matrix: Waste Water Sampled:11/11/19 13:30 Work Order: CC19005
Project: RO Pilot Sampled By: Scott Creech
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed I;Y Notes
Silica (Si02) [763-18-69]A 32.3 mg/L 5 0.1 1.1 9K14018 EPA 6010D 11/18/19 13:38 ]DH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 28

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 9K14018 - EPA 3005A
Blank (9K14018-BLKI) Prepared: 11/14/2019 10:04 Analyzed: 11/18/2019 12:56
Spike Source %REC
RPD
Analvte
Result
Flag
Q
Units
Level Result %REC Limits RPD
Limit Notes
Silica (Si02)
0.03
U
0.2
mg/L
Blank (9K14018-BLK2)
Prepared: 11/14/2019 10:04 Analyzed: 11/18/2019 12:59
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit Notes
Silica (Si02)
0.03
U
0.2
mg/L
Batch 9K18016 - EPA 7470A
Blank (9K18016-BLKS)
Prepared: 11/18/2019 09:52 Analyzed: 11/19/2019 11:37
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Mercury
0.000150
U
0.000200
mg/L
LCS (9K38016-BS3)
Prepared: 11/18/2019 09:52 Analyzed: 11/19/2019 11:39
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Mercury
0.00495
0.000200
mg/L
0.00500 99 80-120
Matrix Spike (9K38016-MS3)
Prepared: 11/18/2019 09:52 Analyzed: 11/19/2019 11:50
Source: CC18168-02
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Mercury
0.00548
0.000200
mg/L
0.00500 0.000924 91 75-125
Matrix Spike Dup (9K18016-MSD3)
Prepared: 11/18/2019 09:52 Analyzed: 11/19/2019 11:52
Source: CC18168-02
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Mercury
0.00546
0.000200
mg/L
0.00500 0.000924 91 75-125 0.4
25
Post Spike (9K38016-PS3)
Prepared: 11/18/2019 09:52 Analyzed: 11/19/2019 11:54
Source: CC18168-02
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Mercury
5.60
0.200
ug/L
5.00 0.924 94 75-125
Batch 9L09022 - EPA 3005A
Blank (9L09022-BLK3)
Prepared: 12/09/2019 12:59 Analyzed: 12/10/2019 11:10
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Silica (Si02) 0.03 U 0.2 mg/L
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 9K14018 - EPA 3005A
Blank (9K14018-BLK1) Prepared: 11/14/2019 10:04 Analyzed: 11/18/2019 12:56
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 28

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 9K14018 - EPA 3005A - Continued
Blank (9K34018-BLK1) Continued Prepared: 11/14/2019 10:04 Analyzed: 11/18/2019 12:56
Spike Source %REC RPD
Analvte
Result
Flaq
Q
Units
Level Result %REC Limits RPD Limit Notes
Aluminum
0.0420
U
0.100
mg/L
Arsenic
0.00760
U
0.0100
mg/L
Boron
0.00570
U
0.0500
mg/L
Cadmium
0.000360
U
0.00100
mg/L
Calcium
0.0390
U
0.100
mg/L
Chromium
0.00140
U
0.0100
mg/L
Copper
0.00160
U
0.0100
mg/L
Iron
0.0220
U
0.0500
mg/L
Lead
0.00310
U
0.0100
mg/L
Magnesium
0.0290
U
0.100
mg/L
Molybdenum
0.00250
U
0.0100
mg/L
Nickel
0.00220
U
0.0100
mg/L
Potassium
0.150
U
0.500
mg/L
Selenium
0.00620
U
0.0100
mg/L
Silver
0.00190
U
0.0100
mg/L
Sodium
0.400
U
0.500
mg/L
Zinc
0.00440
U
0.0100
mg/L
Blank (9K14018-BLK2)
Prepared: 11/14/2019 10:04 Analyzed: 11/18/2019 12:59
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Aluminum
0.0420
U
0.100
mg/L
Arsenic
0.00760
U
0.0100
mg/L
Boron
0.00570
U
0.0500
mg/L
Cadmium
0.000360
U
0.00100
mg/L
Calcium
0.0390
U
0.100
mg/L
Chromium
0.00140
U
0.0100
mg/L
Copper
0.00160
U
0.0100
mg/L
Iron
0.0220
U
0.0500
mg/L
Lead
0.00310
U
0.0100
mg/L
Magnesium
0.0290
U
0.100
mg/L
Molybdenum
0.00250
U
0.0100
mg/L
Nickel
0.00220
U
0.0100
mg/L
Potassium
0.150
U
0.500
mg/L
Selenium
0.00620
U
0.0100
mg/L
Silver
0.00190
U
0.0100
mg/L
Sodium
0.400
U
0.500
mg/L
Zinc
0.00440
U
0.0100
mg/L
LCS (9K14018-BS1)
Prepared: 11/14/2019 10:04 Analyzed: 11/18/2019 13:06
Spike
Source
%REC RPD
Analvte
Result
Flaq POL
Units
Level
Result %REC
Limits RPD Limit Notes
Aluminum
2.06
0.100
mg/L
2.00
103
80-120
Arsenic
0.194
0.0100
mg/L
0.200
97
80-120
Boron
0.976
0.0500
mg/L
1.00
98
80-120
Cadmium
0.0189
0.00100
mg/L
0.0200
95
80-120
Calcium
2.02
0.100
mg/L
2.00
101
80-120
Chromium
0.192
0.0100
mg/L
0.200
96
80-120
Copper
0.190
0.0100
mg/L
0.200
95
80-120
FINAL
This report relates only to the sample as received by the
laboratory, and
may only be reproduced in
full. Page 13 of 28

0Nk"q09
www.encolabs.com
QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 9K1401B - EPA 3005A - Continued
LCS (9K34018-BS1) Continued Prepared: 11/14/2019 10:04 Analyzed: 11/18/2019 13:06
Spike
Source
%REC
RPD
Analvte
Result
Flaa POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Iron
0.956
0.0500
mg/L
1.00
96
80-120
Lead
0.189
0.0100
mg/L
0.200
95
80-120
Magnesium
2.03
0.100
mg/L
2.00
102
80-120
Molybdenum
0.188
0.0100
mg/L
0.200
94
80-120
Nickel
0.192
0.0100
mg/L
0.200
96
80-120
Potassium
10.5
0.500
mg/L
10.0
105
80-120
Selenium
0.188
0.0100
mg/L
0.200
94
80-120
Silver
0.198
0.0100
mg/L
0.200
99
80-120
Sodium
10.0
0.500
mg/L
10.0
100
80-120
Zinc
0.203
0.0100
mg/L
0.200
102
80-120
Matrix Spike (9K34018-MS3)
Prepared:
11/14/2019
10:04 Analyzed: 11/18/2019 13:17
Source: CC19076-01
Spike
Source
%REC
RPD
Analvte
Result
Flaa POL
Uni
Level
Result
%REC
Limits RPD
Limit Notes
Aluminum
3.08
0.100
mg/L
2.00
0.221
143
75-125
QM-07
Arsenic
0.186
0.0100
mg/L
0.200
0.00760 U
93
75-125
Boron
0.982
0.0500
mg/L
1.00
0.00570 U
98
75-125
Cadmium
0.0187
0.00100
mg/L
0.0200
0.000360 U
94
75-125
Calcium
4.94
0.100
mg/L
2.00
3.16
89
75-125
Chromium
0.193
0.0100
mg/L
0.200
0.00140 U
97
75-125
Copper
0.192
0.0100
mg/L
0.200
0.00160 U
96
75-125
Iron
1.26
0.0500
mg/L
1.00
0.143
112
75-125
Lead
0.187
0.0100
mg/L
0.200
0.00310 U
93
75-125
Magnesium
3.74
0.100
mg/L
2.00
1.73
101
75-125
Molybdenum
0.188
0.0100
mg/L
0.200
0.00250 U
94
75-125
Nickel
0.193
0.0100
mg/L
0.200
0.00220 U
97
75-125
Potassium
17.5
0.500
mg/L
10.0
6.93
106
75-125
Selenium
0.192
0.0100
mg/L
0.200
0.00620 U
96
75-125
Silver
0.199
0.0100
mg/L
0.200
0.00190 U
100
75-125
Sodium
21.6
0.500
mg/L
10.0
11.5
101
75-125
Zinc
0.223
0.0100
mg/L
0.200
0.0179
103
75-125
Matrix Spike Dup (9K14018-MSD1)
Prepared:
11/14/2019
10:04 Analyzed: 11/18/2019 13:19
Source: CC19076-01
Spike
Source
%REC
RPD
Analvte
Result
Flaa POL
Units
Level
Res l
%REC
Limits
RPD
Limit
Notes
Aluminum
5.53
0.100
mg/L
2.00
0.221
266
75-125
57
20
QM-07,
QM-11
Arsenic
0.186
0.0100
mg/L
0.200
0.00760 U
93
75-125
0.04
20
Boron
0.991
0.0500
mg/L
1.00
0.00570 U
99
75-125
0.9
20
Cadmium
0.0188
0.00100
mg/L
0.0200
0.000360 U
94
75-125
0.1
20
Calcium
4.72
0.100
mg/L
2.00
3.16
78
75-125
5
20
Chromium
0.198
0.0100
mg/L
0.200
0.00140 U
99
75-125
3
20
Copper
0.193
0.0100
mg/L
0.200
0.00160 U
97
75-125
0.6
20
Iron
2.17
0.0500
mg/L
1.00
0.143
203
75-125
53
20
QM-07,
QM-11
Lead
0.190
0.0100
mg/L
0.200
0.00310 U
95
75-125
2
20
Magnesium
3.61
0.100
mg/L
2.00
1.73
94
75-125
4
20
Molybdenum
0.190
0.0100
mg/L
0.200
0.00250 U
95
75-125
0.8
20
Nickel
0.195
0.0100
mg/L
0.200
0.00220 U
97
75-125
0.7
20
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in
full.
Page 14 of 28

(� �Eo
www.encolabs.com
QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 9K14018 - EPA 3005A - Continued
Matrix Spike Dup (9K14018-MSD3) Continued
Prepared: 11/14/2019 10:04 Analyzed: 11/18/2019 13:19
Source: CC19076-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Potassium
16.6
0.500
mg/L
10.0 6.93 96 75-125 5
20
Selenium
0.185
0.0100
mg/L
0.200 0.00620 U 93 75-125 3
20
Silver
0.198
0.0100
mg/L
0.200 0.00190 U 99 75-125 0.5
20
Sodium
20.2
0.500
mg/L
10.0 11.5 88 75-125 7
20
Zinc
0.217
0.0100
mg/L
0.200 0.0179 99 75-125 3
20
Post Spike (9K14018-PS1)
Prepared: 11/14/2019 10:04 Analyzed: 11/18/2019 13:22
Source: CC19076-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Aluminum
2.46
0.100
mg/L
2.00
0.221
112
80-120
Arsenic
0.191
0.0100
mg/L
0.200
-0.00167
95
80-120
Boron
1.04
0.0500
mg/L
1.00
0.000927
103
80-120
Cadmium
0.0197
0.00100
mg/L
0.0200
1.38E-5
99
80-120
Calcium
4.76
0.100
mg/L
2.00
3.16
80
80-120
Chromium
0.202
0.0100
mg/L
0.200
0.000833
101
80-120
Copper
0.201
0.0100
mg/L
0.200
0.000950
100
80-120
Iron
1.14
0.0500
mg/L
1.00
0.143
99
80-120
Lead
0.199
0.0100
mg/L
0.200
4.44E-5
100
80-120
Magnesium
3.75
0.100
mg/L
2.00
1.73
101
80-120
Molybdenum
0.198
0.0100
mg/L
0.200
0.000880
99
80-120
Nickel
0.201
0.0100
mg/L
0.200
0.00134
100
80-120
Potassium
17.1
0.500
mg/L
10.0
6.93
102
80-120
Selenium
0.201
0.0100
mg/L
0.200
0.000775
100
80-120
Silver
0.212
0.0100
mg/L
0.200
0.000419
106
80-120
Sodium
20.9
0.500
mg/L
10.0
11.5
94
80-120
Zinc
0.227
0.0100
mg/L
0.200
0.0179
105
80-120
Batch 9LO9022 - EPA 3005A
Blank (9L09022-BLK3)
Prepared:
12/09/2019
12:59 Analyzed: 12/10/2019 11:10
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Aluminum
0.0420
U
0.100
mg/L
Arsenic
0.00760
U
0.0100
mg/L
Boron
0.00570
U
0.0500
mg/L
Cadmium
0.000360
U
0.00100
mg/L
Calcium
0.0390
U
0.100
mg/L
Chromium
0.00140
U
0.0100
mg/L
Copper
0.00160
U
0.0100
mg/L
Iron
0.0220
U
0.0500
mg/L
Lead
0.00310
U
0.0100
mg/L
Magnesium
0.0290
U
0.100
mg/L
Molybdenum
0.00250
U
0.0100
mg/L
Nickel
0.00220
U
0.0100
mg/L
Potassium
0.150
U
0.500
mg/L
Selenium
0.00622
1
0.0100
mg/L
Silver
0.00190
U
0.0100
mg/L
Sodium
0.400
U
0.500
mg/L
Zinc
0.00440
U
0.0100
mg/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 15 of 28

0Nk"q09
www.encolabs.com
QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 9LO9022 - EPA 3005A - Continued
LCS (9L09022-BSI) Prepared: 12/09/2019 12:59 Analyzed: 12/10/2019 11:38
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Aluminum
2.18
0.100
mg/L
2.00
109
80-120
Arsenic
0.216
0.0100
mg/L
0.200
108
80-120
Boron
1.06
0.0500
mg/L
1.00
106
80-120
Cadmium
0.0214
0.00100
mg/L
0.0200
107
80-120
Calcium
2.22
0.100
mg/L
2.00
111
80-120
Chromium
0.212
0.0100
mg/L
0.200
106
80-120
Copper
0.208
0.0100
mg/L
0.200
104
80-120
Iron
1.12
0.0500
mg/L
1.00
112
80-120
Lead
0.208
0.0100
mg/L
0.200
104
80-120
Magnesium
2.16
0.100
mg/L
2.00
108
80-120
Molybdenum
0.210
0.0100
mg/L
0.200
105
80-120
Nickel
0.213
0.0100
mg/L
0.200
107
80-120
Potassium
10.7
0.500
mg/L
10.0
107
80-120
Selenium
0.210
B
0.0100
mg/L
0.200
105
80-120
Silver
0.214
0.0100
mg/L
0.200
107
80-120
Sodium
10.9
0.500
mg/L
10.0
109
80-120
Zinc
0.224
0.0100
mg/L
0.200
112
80-120
Matrix Spike (9L09022-MS3)
Prepared: 12/09/2019
12:59 Analyzed: 12/10/2019 11:41
Source: CC19670-02
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limi RPD
Limi Notes
Aluminum
2.10
0.100
mg/L
2.00
0.0420 U
105
75-125
Arsenic
0.188
0.0100
mg/L
0.200
0.00760 U
94
75-125
Boron
1.05
0.0500
mg/L
1.00
0.0132
104
75-125
Cadmium
0.0201
0.00100
mg/L
0.0200
0.000360 U
101
75-125
Calcium
27.8
0.100
mg/L
2.00
25.5
114
75-125
Chromium
0.204
0.0100
mg/L
0.200
0.00140 U
102
75-125
Copper
0.202
0.0100
mg/L
0.200
0.00160 U
101
75-125
Iron
1.10
0.0500
mg/L
1.00
0.0220 U
110
75-125
Lead
0.197
0.0100
mg/L
0.200
0.00310 U
98
75-125
Magnesium
13.0
0.100
mg/L
2.00
11.0
103
75-125
Molybdenum
0.205
0.0100
mg/L
0.200
0.00250 U
102
75-125
Nickel
0.204
0.0100
mg/L
0.200
0.00220 U
102
75-125
Potassium
12.7
0.500
mg/L
10.0
2.09
106
75-125
Selenium
0.200
B
0.0100
mg/L
0.200
0.00620 U
100
75-125
Silver
0.205
0.0100
mg/L
0.200
0.00234
101
75-125
Sodium
30.1
0.500
mg/L
10.0
19.3
108
75-125
Zinc
0.217
0.0100
mg/L
0.200
0.00639
105
75-125
Matrix Spike Dup (9L09022-MSD3)
Prepared: 12/09/2019
12:59 Analyzed: 12/10/2019 11:43
Source: CC19670-02
Spike
Source
%REC
RPD
An
Result
Flaa POL
Uni
Level
Result
%REC
Limits
RPD
Limit Notes
Aluminum
2.05
0.100
mg/L
2.00
0.0420 U
103
75-125
2
20
Arsenic
0.188
0.0100
mg/L
0.200
0.00760 U
94
75-125
0.1
20
Boron
1.03
0.0500
mg/L
1.00
0.0132
102
75-125
1
20
Cadmium
0.0200
0.00100
mg/L
0.0200
0.000360 U
100
75-125
0.8
20
Calcium
27.5
0.100
mg/L
2.00
25.5
97
75-125
1
20
Chromium
0.201
0.0100
mg/L
0.200
0.00140 U
101
75-125
1
20
Copper
0.199
0.0100
mg/L
0.200
0.00160 U
100
75-125
1
20
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in
full.
Page 16 of 28

(� �Eo
www.encolabs.com
QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 9L09022 - EPA 3005A - Continued
Matrix Spike Dup (9L09022-MSD3) Continued
Prepared: 12/09/2019 12:59 Analyzed: 12/10/2019 11:43
Source: CC19670-02
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Iron
1.07
0.0500
mg/L
1.00
0.0220 U
107
75-125
2
20
Lead
0.195
0.0100
mg/L
0.200
0.00310 U
98
75-125
0.7
20
Magnesium
12.9
0.100
mg/L
2.00
11.0
95
75-125
1
20
Molybdenum
0.202
0.0100
mg/L
0.200
0.00250 U
101
75-125
2
20
Nickel
0.203
0.0100
mg/L
0.200
0.00220 U
101
75-125
0.5
20
Potassium
12.7
0.500
mg/L
10.0
2.09
106
75-125
0.2
20
Selenium
0.210
B
0.0100
mg/L
0.200
0.00620 U
105
75-125
5
20
Silver
0.202
0.0100
mg/L
0.200
0.00234
100
75-125
1
20
Sodium
29.9
0.500
mg/L
10.0
19.3
105
75-125
0.8
20
Zinc
0.215
0.0100
mg/L
0.200
0.00639
104
75-125
1
20
Post Spike (911-09022-PS1)
Prepared: 12/09/2019 12:59 Analyzed: 12/10/2019 11:46
Source: CC19670-02
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Aluminum
2.19
0.100
mg/L
2.00
-0.0356
110
80-120
Arsenic
0.196
0.0100
mg/L
0.200
-0.0187
98
80-120
Boron
1.08
0.0500
mg/L
1.00
0.0132
107
80-120
Cadmium
0.0207
0.00100
mg/L
0.0200
-5.70E-5
104
80-120
Calcium
26.9
0.100
mg/L
2.00
25.5
67
80-120
QM-08
Chromium
0.210
0.0100
mg/L
0.200
0.00115
104
80-120
Copper
0.206
0.0100
mg/L
0.200
-4.97E-5
103
80-120
Iron
1.12
0.0500
mg/L
1.00
0.0189
110
80-120
Lead
0.205
0.0100
mg/L
0.200
-0.00391
103
80-120
Magnesium
12.9
0.100
mg/L
2.00
11.0
99
80-120
Molybdenum
0.210
0.0100
mg/L
0.200
-0.000102
105
80-120
Nickel
0.210
0.0100
mg/L
0.200
0.00149
104
80-120
Potassium
12.7
0.500
mg/L
10.0
2.09
106
80-120
Selenium
0.214
B
0.0100
mg/L
0.200
-0.00698
107
80-120
Silver
0.215
0.0100
mg/L
0.200
0.00234
106
80-120
Sodium
29.7
0.500
mg/L
10.0
19.3
103
80-120
Zinc
0.225
0.0100
mg/L
0.200
0.00639
109
80-120
Metals (Dissolved) by EPA 6000/7000 Series Methods - Quality Control
Batch 9K12043 - EPA 3005A
Blank (9K12043-BLKS) Prepared: 11/12/2019 16:24 Analyzed: 11/15/2019 11:50
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Calcium
0.0390
U
0.100
mg/L
Magnesium
29.0
U
100
ug/L
Silica (Si02)
0.03
U
0.2
mg/L
Blank (9K12043-BLK2)
Prepared: 11/12/2019 16:24 Analyzed: 11/15/2019 12:00
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units Level Result %REC Limits RPD Limit Notes
Calcium
0.0390
U
0.100
mg/L
Magnesium
29.0
U
100
ug/L
Silica (Si02)
0.03
U
0.2
mg/L
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 17 of 28

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QUALITY CONTROL DATA
Metals (Dissolved) by EPA 6000/7000 Series Methods - Quality Control
Batch 9K12043 - EPA 3005A - Continued
LCS (9K32043-BS3) Prepared: 11/12/2019 16:24 Analyzed: 11/15/2019 12:05
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Calcium
2.13
0.100
mg/L
2.00
106
80-120
Magnesium
2140
100
ug/L
2000
107
80-120
Matrix Spike (9K12043-MS1)
Prepared: 11/12/2019 16:24 Analyzed: 11/15/2019 12:08
Source: CC18177-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Calcium
2.77
0.100
mg/L
2.00
0.757
101
75-125
Magnesium
2500
100
ug/L
2000
280
111
75-125
Matrix Spike Dup (9K12043-MSD1)
Prepared: 11/12/2019 16:24 Analyzed: 11/15/2019 12:10
Source: CC18177-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Calcium
2.64
0.100
mg/L
2.00
0.757
94
75-125 5
20
Magnesium
2530
100
ug/L
2000
280
112
75-125 1
20
Post Spike (9K12043-PS1)
Prepared: 11/12/2019 16:24 Analyzed: 11/15/2019 12:13
Source: CC18177-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Calcium
2.68
0.100
mg/L
2.00
0.757
96
80-120
Magnesium
2.43
0.100
mg/L
2.00
0.280
107
80-120
Classical Chemistry Parameters - Quality Control
Batch 9KI2037 - NO PREP
Blank (9K12037-BLK1) Prepared: 11/12/2019 16:16 Analyzed: 11/12/2019 16:16
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Nitrite as N 0.017 Ll 0.10 mg/L
LCS (9K12037-BS3) Prepared: 11/12/2019 16:37 Analyzed: 11/12/2019 16:37
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrite as N
1.0
0.10
mg/L
1.00 103 90-110
Matrix Spike (9K32037-MS3)
Prepared: 11/12/2019 18:02 Analyzed: 11/12/2019 18:02
Source: CC18217-01
Spike Source %REC
RPD
Analvte
Result Flaq
Q
Units
Level Result %REC Limits RPD
Limit Notes
Nitrite as N
1.0
0.10
mg/L
1.00 0.039 99 90-110
Matrix Spike (9K32037-MS2)
Prepared: 11/12/2019 18:05 Analyzed: 11/12/2019 18:05
Source: CC18217-02
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrite as N
1.0
0.10
mg/L
1.00 0.037 99 90-110
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 18 of 28

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9K12O37 - NO PREP - Continued
Matrix Spike Dup (9K12037-MSD3) Prepared: 11/12/2019 18:03 Analyzed: 11/12/2019 18:03
Source: CC18217-01
Spike Source %REC RPD
Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes
Nitrite as N 1.0 0.10 mg/L 1.00 0.039 100 90-110 1 10
Batch 9K12O3B - NO PREP
Blank (9K12038-BLKl) Prepared: 11/12/2019 16:48 Analyzed: 11/12/2019 16:48
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Nitrite as N 0.017 U 0.10 mg/L
LCS (91(12038-BS3) Prepared: 11/12/2019 16:49 Analyzed: 11/12/2019 16:49
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Nitrite as N
1.0
0.10
mg/L
1.00 105 90-110
Matrix Spike (9K32038-MS3)
Prepared & Analyzed: 11/12/2019 17:07
Source: CC19005-03
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Nitrite as N
3.1
D
0.50
mg/L
1.00 2.0 109 90-110
Matrix Spike Dup (91(32038-MSD3)
Prepared: 11/12/2019 17:07 Analyzed: 11/12/2019 17:07
Source: CC19005-03
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Nitrite as N
3.1
D
0.50
mg/L
1.00 2.0 107 90-110
0.7
10
Batch 9K13OO9 - NO PREP
Blank (9K13009-BLKS) Prepared & Analyzed: 11/13/2019 08:46
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Turbidity 0.50 U 1.0 NTU
LCS (9K33009-BS3) Prepared & Analyzed: 11/13/2019 08:46
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Turbidity
20
1.0
NTU
20.0 98 80-120
Duplicate (9K13009-DUPi)
Prepared & Analyzed: 11/13/2019 08:46
Source: CC16867-03
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Turbidity
1.9
1.0
NTU
2.0 2
25
Batch 9K13O11 - NO PREP
Blank (9K13011-BLKS) Prepared: 11/13/2019 12:46 Analyzed: 11/13/2019 12:46
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Orthophosphate as P 0.23 J 0.50 mg/L 1-01, Q13-0.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 19 of 28

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9K13O11 - NO PREP - Continued
LCS (9K33011-BS3) Prepared: 11/13/2019 12:46 Analyzed: 11/13/2019 12:46
Spike Source %REC RPD
Analvte Result Flag Q Units Level Result %REC Limits RPD Limit Notes
Orthophosphate as P 4.5 B 0.50 mg/L 5.00 91 90-110
LCS (9K13011-BS2) Prepared: 11/13/2019 12:53 Analyzed: 11/13/2019 12:53
Spike
Source
%REC
RPD
Analvte
Result
Flag
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Orthophosphate as P
4.6
B
0.50
mg/L
5.00
92
90-110
Matrix Spike (9K13011-MS1)
Prepared: 11/13/2019 12:48 Analyzed: 11/13/2019 12:48
Source: CC19005-02
Spike
Source
%REC
RPD
Analvte
Result
Flag
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Orthophosphate as P
5.6
B
0.50
mg/L
2.00
3.7
99
90-110
Matrix Spike Dup (9K13031-MSD1)
Prepared: 11/13/2019 12:49 Analyzed: 11/13/2019 12:49
Source: CC19005-02
Spike
Source
%REC
RPD
Analvte
Result
Flag
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Orthophosphate as P
5.7
B
0.50
mg/L
2.00
3.7
101
90-110 0.8
10
Batch 9K13O27 - NO PREP
Blank (9K13027-BLK1) Prepared: 11/13/2019 11:53 Analyzed: 11/13/2019 14:43
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Total Alkalinity as CaCO3 14 U 15 mg/L
LCS (9K13027-BS3) Prepared: 11/13/2019 11:53 Analyzed: 11/13/2019 14:44
Spike
Source
%REC
RPD
Analvte
Result Flag
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Total Alkalinity as CaCO3
97
15
mg/L
100
97
80-120
Matrix Spike (9K33027-MS3)
Prepared: 11/13/2019 11:53 Analyzed: 11/13/2019 14:45
Source: CC19005-03
Spike
Source
%REC
RPD
Analvte
Result Flag
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Total Alkalinity as CaCO3
60
15
mg/L
37.8
19
109
80-120
Matrix Spike Dup (9K33027-MSD3)
Prepared: 11/13/2019 11:53 Analyzed: 11/13/2019 14:46
Source: CC19005-03
Spike
Source
%REC
RPD
Analvte
Result Flag
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Total Alkalinity as CaCO3
66
15
mg/L
37.8
19
124
80-120 9
25
QM-07
Batch 9K14OO7 - NO PREP
Blank (9K14007-BLKS) Prepared & Analyzed: 11/14/2019 08:40
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Specific Conductance (EC) at 25 Deg C 1.0 U 1.0 umhos/cm
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 20 of 28

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9K14007 - NO PREP - Continued
LCS (9K34007-BS3) Prepared & Analyzed: 11/14/2019 08:40
Spike
Source
%REC
RPD
Analvte
Result Flag
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Specific Conductance (EC) at 25 Deg C
730
1.0
umhos/cm
705
104 90-110
Duplicate (9K14007-DUPI)
Prepared & Analyzed: 11/14/2019 08:40
Source: CC16542-03
Spike
Source
%REC
RPD
Analvte
Result Flag
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Specific Conductance (EC) at 25 Deg C
770
1.0
umhos/cm
770
0.1
25
Batch 9K14010 - Same
Blank (9K14010-BLKS) Prepared: 11/14/2019 11:53 Analyzed: 11/25/2019 17:50
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Phosphorus 0.032 1 0.10 mg/L
Blank (9K14030-BLK2) Prepared: 11/14/2019 11:53 Analyzed: 11/26/2019 14:04
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Phosphorus 0.049 3 0.10 mg/L
LCS (9K14010-BS1) Prepared: 11/14/2019 11:53 Analyzed: 11/25/2019 17:52
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Phosphorus 1.6 0.10 mg/L 1.60 99 80-120
LCS (9K14010-BS2) Prepared: 11/14/2019 11:53 Analyzed: 11/26/2019 14:06
Spike Source %REC
RPD
Analvte
Result Flag
POL
Units
Level Result %REC Limits RPD
Limit Notes
Phosphorus
1.6
0.10
mg/L
1.60 103 80-120
Matrix Spike (9K14010-MS1)
Prepared: 11/14/2019 11:53 Analyzed: 11/25/2019 17:54
Source: CC12339-01
Spike Source %REC
RPD
Analvte
Result Flag
POL
Units
Level Result %REC Limits RPD
Limit Notes
Phosphorus
1.7
0.10
mg/L
0.640 0.99 108 80-120
Matrix Spike Dup (9K14030-MSD1)
Prepared: 11/14/2019 11:53 Analyzed: 11/25/2019 17:56
111
Source: CC12339-01
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Phosphorus 1.7 0.10 mg/L 0.640 0.99 111 80-120 1 25
Batch 9K14011 - Same
Blank (9K14011-BLKS) Prepared: 11/14/2019 11:53 Analyzed: 11/25/2019 16:08
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Total Kjeldahl Nitrogen 0.26 U 0.48 mg/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 21 of 28

QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9K14011 - Same - Continued
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Blank (9K14011-BLK2) Prepared: 11/14/2019 11:53 Analyzed: 11/26/2019 12:25
Spike Source %REC RPD
Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes
Total Kjeldahl Nitrogen 0.26 U 0.48 mg/L
LCS (9KI4011-BSI) Prepared: 11/14/2019 11:53 Analyzed: 11/25/2019 16:10
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Kjeldahl Nitrogen 12 0.48 mg/L 12.0 103 90-110
LCS (91(14011-BS2) Prepared: 11/14/2019 11:53 Analyzed: 11/26/2019 12:27
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
13
0.48
mg/L
12.0 108 90-110
Matrix Spike (9K34011-MS3)
Prepared: 11/14/2019 11:53 Analyzed: 11/25/2019 16:14
Source: CC12339-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
11
0.48
mg/L
4.80 5.7 107 90-110
Matrix Spike (9KI4011-MS2)
Prepared: 11/14/2019 11:53 Analyzed: 11/25/2019 16:19
Source: CC12555-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
5.5
0.48
mg/L
4.80 0.65 102 90-110
Matrix Spike Dup (9K14011-MSD3)
Prepared: 11/14/2019 11:53 Analyzed: 11/25/2019 16:15
Source: CC12339-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
11
0.48
mg/L
4.80 5.7 114 90-110 3
10
QM-07
Batch 9K14025 - Same
Blank (9K14025-BLK1) Prepared: 11/14/2019 11:35 Analyzed: 11/14/2019 16:40
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Chemical Oxygen Demand 10 U 10 mg/L
LCS (9KI4025-BS3) Prepared: 11/14/2019 11:35 Analyzed: 11/14/2019 16:40
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Chemical Oxygen Demand
510
10
mg/L
500 101 90-110
Matrix Spike (9K34025-MS1)
Prepared: 11/14/2019 11:35 Analyzed: 11/14/2019 16:40
Source: CC12339-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Chemical Oxygen Demand
690
10
mg/L
526 210 92 90-110
Matrix Spike Dup (9K14025-MSD3)
Prepared: 11/14/2019 11:35 Analyzed: 11/14/2019 16:40
Source: CC12339-01
Spike Source %REC RPD
Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Notes
Page 22 of 28

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9K14025 - Same - Continued
Matrix Spike Dup (9K14025-MSD3) Continued Prepared: 11/14/2019 11:35 Analyzed: 11/14/2019 16:40
Source: CC12339-01
Spike Source %REC RPD
Analvte Result Flag Q Units Level Result %REC Limits RPD Limit Notes
Chemical Oxygen Demand 690 10 mg/L 526 210 93 90-110 0.3 5
Batch 9K14040 - NO PREP
Blank (9K14040-BLK1) Prepared & Analyzed: 11/14/2019 14:49
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Total Suspended Solids 2.5 U 2.5 mg/L
LCS (9K14040-BS3) Prepared & Analyzed: 11/14/2019 14:49
Spike Source %REC
RPD
Analvte
Result Flag
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Total Suspended Solids
90
2.5
mg/L
100 90 80-120
Duplicate (911(14040-DUP3)
Prepared & Analyzed: 11/14/2019 14:49
Source: CC16542-01
Spike Source %REC
RPD
Analvte
Result Flag
Q
Units
Level Result %REC Limits
RPD
Limit Notes
Total Suspended Solids
270
62
mg/L
290
5
20
Duplicate (9K34040-DUP2)
Prepared & Analyzed: 11/14/2019 14:49
Source: CC17720-01
Spike Source %REC
RPD
Analvte
Result Flag
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Total Suspended Solids
68
45
mg/L
69
2
20
Batch 9K15003 - Same
Blank (9K15003-BLKS) Prepared: 11/19/2019 09:47 Analyzed: 11/20/2019 10:52
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Cyanide (total) 0.0049 U 0.0050 mg/L
LCS (9K35003-BS3) Prepared: 11/19/2019 09:47 Analyzed: 11/20/2019 10:54
Spike Source %REC
RPD
Analvte
Result
Flag POL
Units
Level Result %REC Limits RPD
Limit
Notes
Cyanide (total)
0.15
0.0050
mg/L
0.150 102 90-110
Matrix Spike (9K35003-MSi)
Prepared: 11/19/2019 09:47 Analyzed: 11/20/2019 11:01
Source: CC18406-01
Spike Source %REC
RPD
Analvte
Result
Flag POL
Units
Level Result %REC Limits RPD
Limit
Notes
Cyanide (total)
0.16
0.0050
mg/L
0.150 0.0049 U 104 90-110
Matrix Spike Dup (9K15003-MSD3)
Prepared: 11/19/2019 09:47 Analyzed: 11/20/2019 11:02
Source: CC18406-01
Spike Source %REC
RPD
Analvte
Result
Flag POL
Units
Level Result %REC Limits RPD
Limit
Notes
Cyanide (total)
0.15
0.0050
mg/L
0.150 0.0049 U 100 90-110 4
10
Batch 9K15023 - NO PREP
FINAL
This report relates only to the sample as received by the
laboratory, and may only be reproduced in full.
Page 23 of 28

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9K15023 - NO PREP - Continued
LCS (9K1S023-BS3) Prepared & Analyzed: 11/15/2019 13:20
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
pH
6.9
1.0
pH
7.00 99 99-101
Duplicate (9K15023-DUPi)
Prepared & Analyzed: 11/15/2019 13:20
Source: CC17274-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
pH
7.1
1.0
pH
7.2 1
25
Batch 9K16001 - NO PREP
Blank (9K16001-BLKS) Prepared & Analyzed: 11/18/2019 08:55
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Dissolved Solids 50 U 50 mg/L
LCS (9K36001-BS3) Prepared & Analyzed: 11/18/2019 08:55
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Total Dissolved Solids
990
50
mg/L
1000 99 80-120
Duplicate (9K16001-DUPi)
Prepared & Analyzed: 11/18/2019 08:55
Source: CC16867-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Total Dissolved Solids
2300
50
mg/L
2400
3
20
Duplicate (9K16001-DUP2)
Prepared & Analyzed: 11/18/2019 08:55
Source: CC18217-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Total Dissolved Solids
96
50
mg/L
80
18
20
Batch 9K22022 - NO PREP
Blank (9K22022-BLK1) Prepared: 11/22/2019 10:22 Analyzed: 11/22/2019 14:50
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Nitrate/Nitrite as N 0.041 U 0.10 mg/L
LCS (9K22022-BS3) Prepared: 11/22/2019 10:22 Analyzed: 11/22/2019 14:51
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Nitrate/Nitrite as N
1.2
0.10
mg/L
1.25
98
90-110
Matrix Spike (9K22022-MSI)
Prepared: 11/22/2019 10:22 Analyzed: 11/22/2019 14:55
Source: CC17274-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Nitrate/Nitrite as N
0.47
0.10
mg/L
0.521
0.13
64
90-110
QM-07
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 24 of 28

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9K22022 - NO PREP - Continued
Matrix Spike (9K22022-MS2)
Prepared: 11/22/2019 10:22 Analyzed: 11/22/2019 15:04
Source: CC17732-01
Spike Source %REC
RPD
Analvte
Result Flag
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
20 E
0.10
mg/L
0.521 20 69 90-110
QM-07
Matrix Spike Dup (9K22022-MSD3)
Prepared: 11/22/2019 10:22 Analyzed: 11/22/2019 14:57
Source: CC17274-01
Spike Source %REC
RPD
Analvte
Result Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
0.47
0.10
mg/L
0.521 0.13 65 90-110 0.7
10
QM-07
Batch 9K26034 - NO PREP
Blank (9K26034-BLKS)
Prepared: 11/26/2019 15:40 Analyzed: 11/27/2019 01:34
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Chloride 2.2 U 5.0 mg/L
Sulfate as SO4 2.9 U 5.0 mg/L
LCS (9K26034-BSI) Prepared: 11/26/2019 15:40 Analyzed: 11/27/2019 00:05
Spike Source %REC
RPD
Analvte
Result Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chloride
51
5.0
mg/L
50.0 102 90-110
Sulfate as SO4
52
5.0
mg/L
50.0 105 90-110
Matrix Spike (9K26034-MS3)
Prepared: 11/26/2019 15:40 Analyzed: 11/27/2019 00:41
Source: CC19076-01
Spike Source %REC
RPD
Analvte
Result Flag
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Chloride
28
5.0
mg/L
20.0 13 75 90-110
QM-07
Sulfate as SO4
13
5.0
mg/L
20.0 2.9 U 67 90-110
QM-07
Matrix Spike (9K26034-MS2)
Prepared: 11/26/2019 15:40 Analyzed: 11/27/2019 02:09
Source: CC19076-02
Spike Source %REC
RPD
Analvte
Result Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chloride
18
5.0
mg/L
20.0 3.7 71 90-110
QM-07
Sulfate as SO4
23
5.0
mg/L
20.0 7.7 75 90-110
QM-07
Matrix Spike Dup (9K26034-MSD3)
Prepared: 11/26/2019 15:40 Analyzed: 11/27/2019 00:58
Ill
Source: CC19076-01
Spike
Source
%REC
RPD
Analvte
Result
Flag
POL
Units
Level
Result
%REC
Limits
RPD
Limit
Notes
Chloride
32
5.0
mg/L
20.0
13
95
90-110
13
10
QM-11
Sulfate as SO4
17
5.0
mg/L
20.0
2.9 U
85
90-110
24
10
QM-07,
QM-11
Batch 9K27024 - NO PREP
Blank (9K27024-BLK1)
Prepared: 11/27/2019 15:32 Analyzed: 11/27/2019 17:07
Spike
Source
%REC
RPD
Analvte
Result
Flag
POL
Units
Level
Result
%REC
Limits
RPD
Limit
Notes
Chloride
2.2
U
5.0
mg/L
Sulfate as SO4
2.9
U
5.0
mg/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 25 of 28

QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9K27024 - NO PREP - Continued
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LCS (9K27024-BS3) Prepared: 11/27/2019 15:32 Analyzed: 11/27/2019 17:24
Spike Source %REC
RPD
Analvte
Result
Flag
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Chloride
49
5.0
mg/L
50.0 99 90-110
Sulfate as SO4
51
5.0
mg/L
50.0 102 90-110
Matrix Spike (9K27024-MSI)
Prepared: 11/27/2019 15:32 Analyzed: 11/27/2019 18:00
Source: CC18101-01
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chloride
39
5.0
mg/L
20.0 18 104 90-110
Sulfate as SO4
28
5.0
mg/L
20.0 7.7 101 90-110
Matrix Spike (9K27024-MS2)
Prepared: 11/27/2019 15:32 Analyzed: 11/27/2019 18:53
Source: CC18101-02
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chloride
33
5.0
mg/L
20.0 17 84 90-110
QM-07
Sulfate as SO4
34
5.0
mg/L
20.0 17 82 90-110
QM-07
Matrix Spike Dup (9K27024-MSD3)
Prepared: 11/27/2019 15:32 Analyzed: 11/27/2019 18:17
Source: CC18101-01
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chloride
39
5.0
mg/L
20.0 18 105 90-110 0.6
10
Sulfate as SO4
28
5.0
mg/L
20.0 7.7 102 90-110 0.9
10
Batch 9L02040 - NO PREP
Blank (9L02040-BLK1) Prepared: 12/02/2019 14:59 Analyzed: 12/02/2019 17:14
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Ammonia as N 0.045 U 0.10 mg/L
LCS (9L02040-BS3) Prepared: 12/02/2019 14:59 Analyzed: 12/02/2019 17:16
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
0.98
0.10
mg/L
1.01 97 90-110
Matrix Spike (9L02040-MS3)
Prepared: 12/02/2019 14:59 Analyzed: 12/02/2019 17:19
Source: CC12725-01
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
0.94
0.10
mg/L
0.393 0.60 88 90-110
QM-07
Matrix Spike (91-02040-MS2)
Prepared: 12/02/2019 14:59 Analyzed: 12/02/2019 17:25
Source: CC16715-01
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
5.3
E
0.10
mg/L
0.393 5.3 23 90-110
QM-07
Matrix Spike Dup (9L02040-MSDI)
Prepared: 12/02/2019 14:59 Analyzed: 12/02/2019 17:21
Source: CC12725-01
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
0.96
0.10
mg/L
0.393 0.60 91 90-110 1
10
FINAL
This report relates only to the sample as received by the
laboratory, and may only be reproduced in full.
Page 26 of 28

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
3-01 Result may be biased high due to positive results in the associated method blank at a concentration above
the MDL and/or greater than one-half the MRL.
LP-03 Sample amount received by the laboratory did not meet minimum method requirements for analysis.
Q-01 Analysis performed outside of method - specified holding time.
QB-01 The method blank had a positive result for the analyte; however, the concentration in the method blank is
less than 10% of the sample result. There is minimal impact to the data.
QB-02 The method blank contains analyte at a concentration above the MDL and/or greater than one-half the
MRL. The analyte was not detected in the sample.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 27 of 28

_ 10775 Central Port Dr. 4810 Executive Park Court, Suite 111 102•A Woodwinds Industrial Cl.
Orlando, FL 32824 Jacksonvl)te. FL 32216-6069 Cary, NC 27511
1407) 826-5314 Fax [phone] (904) 296-3Q07 Fax [phone]❑ [phone] Fax [phone] Page of
Client Name
Novozymes North America (NO008)
Project Number
[none]
Requested
Analyses
Requested Turnaround
Times
Note : Rush requests subject to
acceptance by the facility
_ Standard
_Expedited
Due _1 1
m
Z
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Address
77 Perry Chapel Church Road
Project Name/Desc
1
RO Pilot
CiIyJST/Zip
Franidinton, NC 27525
PO # 1 Billing Into
4550996257
Tel
[phone]
Ftor
Reporting Contact
Scott Creech
Sampler(s) Name, Atti(iation (Print)
"D .t.
Billing Contact
Ac counts Payable
Sampler(s) Signature
Site Location l Time Zone
L r o
4-7680
Preservation
(See
Codes)
(Combine
as necessary)
ttem a
Sample ID IFletd Identification)
Colleeban pate
Collection
Time
Cam Gra
Matrix
{see codes)
Total rr of
Containers
Sample Comments
MRRR Feed
4t-0-44
33b
tW(14.q
e
t/Jf—t(r[/w�f
b
X
11 r��� j
f
1
—Total # of Containers
Sample Kit Prepared By
Dateirime
Relin wished By
DateMme
i� i-t�i-t }3
Received By
---
Date�me
Co mentslSpecial Repoo m quirarnents
i
1 O .p J�l
Relinquished By
DateMme
Received By
Da efrrim
rq b
Relinquished By
DafefT-ime
Received By
ilatelTim
Cooler #'s &Temps on Receipt
r 1,
1
Condition Upon Receipt
I )(— Acceptable Unacceptable
Matrix: GW-Groundwater SO-Soif UW-Drinking Water SE -Sediment SW -Surface Water WW-Wastewater A -Air O-Other (detail in comments) Preservation: I -Ice R-IjCI N-HNO3 S-1-12SO4 NO-NoOH 0-01her (detail in comments)
Note: M samples submitted to FNCO Labs are in accordance with the terms and conditions listed on the reverse or this form, unless prior written agreements exist

Sample Preservation Verification
ENCO Cary
Work Order: CC19005
Client: Novozymes North America (NO008)
Logged In: 12-Nov-19 14:01 11
Preservation Check Performed By:
CC19005-02
Project: RO Pilot
Project #: [none]
Logged By: John C King
,1 C
DatelTime: I ]
Cont
Type
Pres (pH)
Requirement
pH Checked I
In Control
pH Adjusted Date/Time
Adjusted
Reagent Used/Comments
B
250mLP+HNO3
<2
Y 1 N / NA
Y ! N..I NA
C
250mLP+NaOH
>12
& I N I NA
Y It) / NA
E
500mLP+H2SO4
<2
I N/ NA
I Y I c�l)1 NA
CC 19005-03
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted DateMme
Adjusted
Reagent Used/Comments
B
250mLP+HNO3
<2
Yu' I N I NA
Y I 1 NA
C
250mLP+NaOH
>12
I N 1 NA
Y 10 / NA
E
500mLP+H2SO4
<2
GY / N I NA
Y I )/ NA
CC19005-04
Type
Pres (pH)
Requirement
pH Checked 1
In Control
Date/TimeGont
pH Adjusted Adjusted
Reagent UsedlComments
B
25OmLP+HNO3
<2
Y ILN) l NA
& 1 N / NA
C
250mLP+NaOH
>12
OY 1 N I NA
Y 1(1 / NA
E
500mLP+H2SO4
<2
6 1 N I NA
Y/ (9 1 NA
C C 19005-05
Cant
Type
Pres (pH)
Requirement
pH Checked !
In Control
pH Adjusted DateMme
Adjusted
Reagent used/Comments
A
250mLP+HNO3
<2
tY,-/ N 1 NA
Y '` N, / NA
Reacient Name ID
1 IL 6 C�1
A
2
pH Strip ID:�(�. 3
Rea ent Name ID
3
4
Reaclent Name ID
5
6
C:\ELMNTIPrintlwko_PreservationCheck.rpt Page 1

2�SENCO Laboratories
9g
Accurate. Timely. Respousive. luuavative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Thursday, January 16, 2020
Novozymes North America (NO008)
Attn: Scott Creech
77 Perry Chapel Church Road
Franklinton, NC 27525
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: Monthly - Week One - SBM
ENCO Workorder(s): CC21020
Dear Scott Creech,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, January 7, 2020.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
0"CLC'L�CA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 13

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: SBM
Lab ID: CC21020-01
Sampled: 01/07/20 03:45
Received: 01/07/20 09:54
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
CSU Method
NO PREP
10/02/22
01/07/20
12:52
01/09/20
15:10
EPA 350.1
NO PREP
02/04/20
01/07/20
13:41
01/07/20
16:04
EPA 351.2
Same
02/04/20
01/08/20
07:31
01/09/20
11:32
EPA 353.2
NO PREP
01/09/20
03:45
01/07/20
10:41
01/07/20
12:48
EPA 353.2
[CALC]
01/09/20
03:45
01/10/20
10:19
01/10/20
15:00
EPA 353.2
NO PREP
02/04/20
01/10/20
10:19
01/10/20
15:00
EPA 365.4
Same
02/04/20
01/08/20
07:31
01/09/20
14:55
EPA 6010D
EPA 3005A
07/05/20
01/07/20
12:52
01/09/20
11:16
EPA 7470A
EPA 7470A
02/04/20
01/08/20
11:32
01/11/20
18:03
SM 2540B-2011
NO PREP
01/14/20
01/10/20
15:49
01/10/20
15:49
SM 254OD-2011
NO PREP
01/14/20
01/08/20
12:08
01/09/20
14:33
SM 5210 B-2011
NO PREP
01/09/20
03:45
01/08/20
10:08
01/08/20
10:08
SM 5220D-2011
Same
02/04/20
01/07/20
14:20
01/07/20
16:40
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 13

0Nk"q09
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SAMPLE DETECTION SUMMARY
Client ID: SBM
Lab ID: CC21020-01
Analvte
Results
Flaa
MDL
PQL
Units
Method Notes
Aluminum - Total
95.3
0.420
1.00
mg/L
EPA 6010D
Ammonia as N
100
D
4.0
9.0
mg/L
EPA 350.1
Biochemical Oxygen Demand
9200
2.0
2.0
mg/L
SM 5210 B-2011
Calcium - Total
2540
0.390
1.00
mg/L
EPA 6010D
Chemical Oxygen Demand
28000
400
400
mg/L
SM 5220D-2011
Copper - Total
0.203
0.0160
0.100
mg/L
EPA 6010D
Lead - Total
0.0327
3
0.0310
0.100
mg/L
EPA 6010D
Magnesium - Total
48.0
0.290
1.00
mg/L
EPA 6010D
Molybdenum - Total
0.0527
3
0.0250
0.100
mg/L
EPA 6010D
Nickel - Total
0.0517
3
0.0220
0.100
mg/L
EPA 6010D
Nitrate as N
6.5
D
0.82
2.0
mg/L
EPA 353.2
Nitrate/Nitrite as N
6.8
D
0.82
2.0
mg/L
EPA 353.2
Nitrite as N
0.24
0.017
0.10
mg/L
EPA 353.2
Phosphorus
560
D
12
50
mg/L
EPA 365.4
Potassium - Total
452
1.50
5.00
mg/L
EPA 6010D
Sodium - Total
267
4.00
5.00
mg/L
EPA 6010D
Sodium Adsorption Ratio
1.43
[blank]
CSU Method
Total Kjeldahl Nitrogen
1900
D
26
48
mg/L
EPA 351.2
Total Solids
4.5
0.0050
0.0050
% by Volume
SM 2540B-2011
Total Suspended Solids
20000
5000
5000
mg/L
SM 2540D-2011
Zinc - Total
0.568
0.0440
0.100
mg/L
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 13

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ANALYTICAL RESULTS
Description: SBM Lab Sample ID:CC21020-01 Received: 01/07/20 09:54
Matrix: Sludge Sampled: 01/07/20 03:45 Work Order: CC21020
Project: Monthly - Week One - SBM Sampled By: Ray Dixon
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flao
Units
DF
MDL
P L
Batch
Method
Analyzed
-By Notes
Mercury[7439-97-6]^
0.000750
U
mg/L
5
0.000750
0.00100
OA08036
EPA 7470A
O1/11/20 18:03
KAH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flao
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Aluminum [7429-90-5]^
95.3
mg/L
10
0.420
1.00
OA07029
EPA 6010D
O1/09/20 11:16
3DH
Arsenic [7440-38-2]1
0.0760
U
mg/L
10
0.0760
0.100
OA07029
EPA 6010D
O1/09/20 11:16
3DH
Cadmium [7440-43-9]1
0.00360
U
mg/L
10
0.00360
0.0100
OA07029
EPA 6010D
O1/09/20 11:16
3DH
Calcium [7440-70-2]^
2540
mg/L
10
0.390
1.00
OA07029
EPA 6010D
O1/09/20 11:16
3DH
Copper[7440-50-8]^
0.203
mg/L
10
0.0160
0.100
OA07029
EPA 6010D
O1/09/20 11:16
3DH
Lead [7439-92-1]^
0.0327
3
mg/L
10
0.0310
0.100
OA07029
EPA 6010D
O1/09/20 11:16
3DH
Magnesium [7439-95-4]^
48.0
mg/L
10
0.290
1.00
OA07029
EPA 6010D
O1/09/20 11:16
3DH
Molybdenum [7439-98-7]^
0.0527
3
mg/L
10
0.0250
0.100
OA07029
EPA 6010D
O1/09/20 11:16
3DH
Nickel[7440-02-O]^
0.0517
3
mg/L
10
0.0220
0.100
OA07029
EPA 6010D
O1/09/20 11:16
3DH
Potassium [7440-09-7]^
452
mg/L
10
1.50
5.00
OA07029
EPA 6010D
O1/09/20 11:16
3DH
Selenium [7782-49-2]^
0.0620
U
mg/L
10
0.0620
0.100
OA07029
EPA 6010D
O1/09/20 11:16
3DH
Sodium [7440-23-5]^
267
mg/L
10
4.00
5.00
OA07029
EPA 6010D
O1/09/20 11:16
3DH
Zinc[7440-66-6]^
0.568
mg/L
10
0.0440
0.100
OA07029
EPA 6010D
O1/09/20 11:16
3DH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flao
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Ammonia as N [7664-41-7]^
100
D
mg/L
90
4.0
9.0
OA07031
EPA 350.1
01/07/20 16:04
AKF
Biochemical Oxygen Demand
9200
mg/L
1
2.0
2.0
OA08008
SM 5210 B-2011
01/08/20 10:08
JOC
Chemical Oxygen Demand^
28000
mg/L
40
400
400
OA07025
SM 5220D-2011
01/07/20 16:40
JOC
Nitrate as N [14797-55-8]
6.5
D
mg/L
20
0.82
2.0
[CALC]
EPA 353.2
01/10/20 15:00
AKF
Nitrate/Nitrite as IN
6.8
D
mg/L
20
0.82
2.0
OA10025
EPA 353.2
01/10/20 15:00
AKF
Nitrite as N [14797-65-0]^
0.24
mg/L
1
0.017
0.10
OA07018
EPA 353.2
01/07/20 12:48
AKF
Phosphorus[7723-14-O]^
560
D
mg/L
500
12
50
OA08001
EPA 365.4
01/09/20 14:55
AKF
Sodium Adsorption Ratio
1.43
[blank]
1
OA07029
CSU Method
01/09/20 15:10
3DH
Total Kjeldahl Nitrogen
1900
D
mg/L
100
26
48
OA08002
EPA 351.2
01/09/20 11:32
AKF
Total Solids^
4.5
% by Volume
1
0.0050
0.0050
OA10045
SM 2540B-2011
01/10/20 15:49
JOC
Total Suspended Solids^
20000
mg/L
2000
5000
5000
OA08038
SM 2540D-2011
01/09/20 14:33
ZGW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 13

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch OA08036 - EPA 7470A
Blank (OA08036-BLK3) Prepared: 01/08/2020 11:32 Analyzed: 01/11/2020 17:16
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Mercury 0.000150 U 0.000200 mg/L
LCS (OA08036-BSI) Prepared: 01/08/2020 11:32 Analyzed: 01/11/2020 17:23
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00516
0.000200
mg/L
0.00500
103
80-120
Matrix Spike (OA08036-MS1)
Prepared: 01/08/2020 11:32 Analyzed: 01/11/2020 17:28
Source: CC20892-05
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00540
0.000200
mg/L
0.00500
0.000150 U
108
75-125
Matrix Spike Dup (OA08036-MSD1)
Prepared: 01/08/2020 11:32 Analyzed: 01/11/2020 17:30
Source: CC20892-05
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00534
0.000200
mg/L
0.00500
0.000150 U
107
75-125 1
25
Post Spike (OA08036-PSI)
Prepared: 01/08/2020 11:32 Analyzed: 01/11/2020 17:33
Source: CC20892-05
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
5.85
0.200
ug/L
5.00
-0.0430
117
75-125
Metals (total recoverable) by EPA 6000/7000
Series Methods - Quality Control
Batch OA07029 - EPA 3005A
Blank (OA07029-BLKI) Prepared: 01/07/2020 12:52 Analyzed: 01/09/2020 10:19
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Aluminum
0.0420
U
0.100
mg/L
Arsenic
0.00760
U
0.0100
mg/L
Cadmium
0.000360
U
0.00100
mg/L
Calcium
0.0390
U
0.100
mg/L
Copper
0.00160
U
0.0100
mg/L
Lead
0.00310
U
0.0100
mg/L
Magnesium
0.0290
U
0.100
mg/L
Molybdenum
0.00250
U
0.0100
mg/L
Nickel
0.00220
U
0.0100
mg/L
Potassium
0.150
U
0.500
mg/L
Selenium
0.00620
U
0.0100
mg/L
Sodium
0.400
U
0.500
mg/L
Zinc
0.00440
U
0.0100
mg/L
LCS (OA07029-BSI)
Prepared: 01/07/2020 12:52 Analyzed: 01/09/2020 10:28
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Aluminum 1.99 0.100 mg/L 2.00 99 80-120
Arsenic 0.198 0.0100 mg/L 0.200 99 80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 13

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch OA07029 - EPA 3005A - Continued
LCS (OA07029-BSI) Continued Prepared: 01/07/2020 12:52 Analyzed: 01/09/2020 10:28
Spike
Source
%REC
RPD
Analvte
Result
Flaq Q
Units
Level
Result
%REC
Limits RPD
Limit Notes
Cadmium
0.0198
0.00100
mg/L
0.0200
99
80-120
Calcium
2.17
0.100
mg/L
2.00
109
80-120
Copper
0.201
0.0100
mg/L
0.200
100
80-120
Lead
0.199
0.0100
mg/L
0.200
100
80-120
Magnesium
2.05
0.100
mg/L
2.00
102
80-120
Molybdenum
0.207
0.0100
mg/L
0.200
103
80-120
Nickel
0.203
0.0100
mg/L
0.200
101
80-120
Potassium
10.2
0.500
mg/L
10.0
102
80-120
Selenium
0.212
0.0100
mg/L
0.200
106
80-120
Sodium
10.5
0.500
mg/L
10.0
105
80-120
Zinc
0.204
0.0100
mg/L
0.200
102
80-120
Matrix Spike (OA07029-MS1)
Prepared:
01/07/2020
12:52 Analyzed: 01/09/2020 10:32
Source: CDO0317-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Aluminum
2.07
0.100
mg/L
2.00
0.0711
100
75-125
Arsenic
0.207
0.0100
mg/L
0.200
0.00760 U
103
75-125
Cadmium
0.0211
0.00100
mg/L
0.0200
0.000360 U
106
75-125
Calcium
9.04
0.100
mg/L
2.00
7.11
97
75-125
Copper
0.204
0.0100
mg/L
0.200
0.00858
98
75-125
Lead
0.207
0.0100
mg/L
0.200
0.00310 U
103
75-125
Magnesium
9.64
0.100
mg/L
2.00
7.71
96
75-125
Molybdenum
0.207
0.0100
mg/L
0.200
0.00250 U
103
75-125
Nickel
0.217
0.0100
mg/L
0.200
0.00701
105
75-125
Potassium
12.9
0.500
mg/L
10.0
2.64
102
75-125
Selenium
0.203
0.0100
mg/L
0.200
0.00620 U
101
75-125
Sodium
25.5
0.500
mg/L
10.0
15.1
104
75-125
Zinc
0.249
0.0100
mg/L
0.200
0.0365
106
75-125
Matrix Spike Dup (OA07029-MSD1)
Prepared:
01/07/2020
12:52 Analyzed: 01/09/2020 10:35
Source: CDO0317-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Aluminum
2.07
0.100
mg/L
2.00
0.0711
100
75-125
0.4
20
Arsenic
0.195
0.0100
mg/L
0.200
0.00760 U
98
75-125
6
20
Cadmium
0.0198
0.00100
mg/L
0.0200
0.000360 U
99
75-125
6
20
Calcium
9.55
0.100
mg/L
2.00
7.11
122
75-125
5
20
Copper
0.202
0.0100
mg/L
0.200
0.00858
97
75-125
1
20
Lead
0.197
0.0100
mg/L
0.200
0.00310 U
99
75-125
5
20
Magnesium
9.73
0.100
mg/L
2.00
7.71
101
75-125
0.9
20
Molybdenum
0.199
0.0100
mg/L
0.200
0.00250 U
100
75-125
4
20
Nickel
0.208
0.0100
mg/L
0.200
0.00701
100
75-125
4
20
Potassium
12.9
0.500
mg/L
10.0
2.64
103
75-125
0.5
20
Selenium
0.208
0.0100
mg/L
0.200
0.00620 U
104
75-125
3
20
Sodium
25.4
0.500
mg/L
10.0
15.1
102
75-125
0.6
20
Zinc
0.236
0.0100
mg/L
0.200
0.0365
100
75-125
5
20
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 13

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch OA07029 - EPA 3005A - Continued
Post Spike (OA07029-PS3)
Prepared: 01/07/2020 12:52 Analyzed: 01/09/2020 10:37
Source: CDO0317-01
Spike
Source
%REC RPD
Analvte
Result Flag
Q
Units
Level
Result
%REC
Limits RPD Limit Notes
Aluminum
2.11
0.100
mg/L
2.00
0.0711
102
80-120
Arsenic
0.200
0.0100
mg/L
0.200
-0.00210
100
80-120
Cadmium
0.0208
0.00100
mg/L
0.0200
0.000115
104
80-120
Calcium
9.25
0.100
mg/L
2.00
7.11
107
80-120
Copper
0.208
0.0100
mg/L
0.200
0.00858
100
80-120
Lead
0.204
0.0100
mg/L
0.200
0.00129
102
80-120
Magnesium
9.58
0.100
mg/L
2.00
7.71
94
80-120
Molybdenum
0.207
0.0100
mg/L
0.200
-0.000664
104
80-120
Nickel
0.217
0.0100
mg/L
0.200
0.00701
105
80-120
Potassium
13.1
0.500
mg/L
10.0
2.64
105
80-120
Selenium
0.215
0.0100
mg/L
0.200
0.000968
107
80-120
Sodium
25.4
0.500
mg/L
10.0
15.1
102
80-120
Zinc
0.247
0.0100
mg/L
0.200
0.0365
105
80-120
Classical Chemistry Parameters - Quality Control
Batch OA07018 - NO PREP
Blank (OA07018-BLK3)
Prepared: 01/07/2020 10:41 Analyzed: 01/07/2020 12:24
Spike Source %REC
RPD
Analvte
Result
Flag
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
0.017
Ll
0.10
mg/L
LCS (OA07018-BSI)
Prepared: 01/07/2020 10:41 Analyzed: 01/07/2020 12:16
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
0.99
0.10
mg/L
1.00 99 90-110
LCS (OA07018-BS2)
Prepared: 01/07/2020 10:41 Analyzed: 01/07/2020 13:52
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
0.98
0.10
mg/L
1.00 98 90-110
Matrix Spike (OA07018-MS3)
Prepared: 01/07/2020 10:41 Analyzed: 01/07/2020 13:56
Source: CDO0194-01
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
5.6
1.0
mg/L
2.00 3.3 116 90-110
QM-07
Matrix Spike Dup (OA07018-MSDS)
Prepared: 01/07/2020 10:41 Analyzed: 01/07/2020 13:57
Source: CDO0194-01
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
5.5
1.0
mg/L
2.00 3.3 111 90-110 2
10
QM-07
Batch OA07025 - Same
Blank (OA07025-BLKI)
Prepared: 01/07/2020 14:20 Analyzed: 01/07/2020 16:40
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OA07025 - Same - Continued
Blank (OA07025-BLK3) Continued Prepared: 01/07/2020 14:20 Analyzed: 01/07/2020 16:40
Spike Source %REC RPD
Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes
Chemical Oxygen Demand 10 U 10 mg/L
LCS (OA07025-BSI) Prepared: 01/07/2020 14:20 Analyzed: 01/07/2020 16:40
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Chemical Oxygen Demand
500
10
mg/L
500
100
90-110
Matrix Spike (OA07025-MS1)
Prepared: 01/07/2020 14:20 Analyzed: 01/07/2020 16:40
Source: CC20969-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Chemical Oxygen Demand
20000
200
mg/L
10000
11000
93
90-110
Matrix Spike Dup (OA07025-MSD1)
Prepared: 01/07/2020 14:20 Analyzed: 01/07/2020 16:40
Source: CC20969-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Chemical Oxygen Demand
20000
200
mg/L
10000
11000
91
90-110 0.8
5
Batch OA07029 - EPA 3005A
Blank (OA07029-BLKi) Prepared: 01/07/2020 12:52 Analyzed: 01/09/2020 15:11
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Sodium Adsorption Ratio 0.00 U [blank]
Batch OA07031 - NO PREP
Blank (OA07031-BLKi) Prepared: 01/07/2020 13:41 Analyzed: 01/07/2020 15:50
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Ammonia as N 0.045 U 0.10 mg/L
LCS (OA07031-BSI) Prepared: 01/07/2020 13:41 Analyzed: 01/07/2020 15:52
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
0.96
0.10
mg/L
1.01 95 90-110
Matrix Spike (OA07031-MS3)
Prepared: 01/07/2020 13:41 Analyzed: 01/07/2020 15:55
Source: CC21019-02
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
0.51
0.10
mg/L
0.393 0.21 75 90-110
QM-07
Matrix Spike (OA07031-MS2)
Prepared: 01/07/2020 13:41 Analyzed: 01/07/2020 16:00
Source: CC21019-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
1.4
0.10
mg/L
0.393 1.2 56 90-110
QM-07
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OAO7O31 - NO PREP - Continued
Matrix Spike Dup (OA07031-MSD1) Prepared: O1/07/2020 13:41 Analyzed: 01/07/2020 15:57
Source: CC21019-02
Spike Source %REC RPD
Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes
Ammonia as N 0.52 0.10 mg/L 0.393 0.21 77 90-110 2 10 QM-07
Batch OAO8OO1 - Same
Blank (OA08001-BLKi) Prepared: O1/08/2020 07:31 Analyzed: 01/09/2020 14:43
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Phosphorus 0.025 U 0.10 mg/L
LCS (OA08001-BSI) Prepared: 01/O8/2020 07:31 Analyzed: 01/09/2020 14:44
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Phosphorus
1.5
0.10
mg/L
1.60 96 80-120
Matrix Spike (OA08001-MS1)
Prepared: 01/08/2020 07:31 Analyzed: 01/09/2020 14:47
Source: CC18367-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Phosphorus
5.3
D
0.50
mg/L
0.640 4.6 118 80-120
Matrix Spike Dup (OA08001-MSDI)
Prepared: 01/08/2020 07:31 Analyzed: 01/09/2020 14:48
Source: CC18367-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Phosphorus
5.3
D
0.50
mg/L
0.640 4.6 120 80-120 0.3
25
Batch OAO8OO2 - Same
Blank (OA08002-BLKi) Prepared: O1/08/2020 07:31 Analyzed: 01/09/2020 11:11
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Kjeldahl Nitrogen 0.26 U 0.48 mg/L
LCS (OA08002-BSI) Prepared: O1/08/2020 07:31 Analyzed: 01/09/2020 11:13
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
12
0.48
mg/L
12.0 100 90-110
Matrix Spike (OA08002-MS3)
Prepared: O1/08/2020 07:31 Analyzed: 01/09/2020 11:16
Source: CC18367-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
110
D
2.4
mg/L
4.80 110 127 90-110
QM-07
Matrix Spike (OA08002-MS2)
Prepared: O1/08/2020 07:31 Analyzed: 01/09/2020 11:21
Source: CC20344-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
49
D
4.8
mg/L
4.80 47 43 90-110
QM-07
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OAO8OO2 - Same - Continued
Matrix Spike Dup (OA08002-MSD1) Prepared: 01/08/2020 07:31 Analyzed: 01/09/2020 11:18
Source: CC18367-01
Spike Source %REC RPD
Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes
Total Kjeldahl Nitrogen 110 D 2.4 mg/L 4.80 110 75 90-110 2 10 QM-07
Batch 0AO8OO8 - NO PREP
Blank (OA08008-BLK3) Prepared & Analyzed: 01/08/2020 10:08
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Biochemical Oxygen Demand 2.0 U 2.0 mg/L
LCS (OA08008-BSI) Prepared & Analyzed: 01/08/2020 10:08
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Biochemical Oxygen Demand
190
2.0
mg/L
198
95 85-115
Duplicate (OA08008-DUPl)
Prepared & Analyzed: 01/08/2020 10:08
Source: CC18320-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
Q
Units
Level
Result
%REC Limits RPD
Limit Notes
Biochemical Oxygen Demand
2.5
2.0
mg/L
2.6
4
30
Batch OAOB038 - NO PREP
Blank (OA08038-BLKi) Prepared: 01/08/2020 12:08 Analyzed: 01/09/2020 14:33
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Suspended Solids 2.5 U 2.5 mg/L
LCS (OA08038-BSI) Prepared: 01/08/2020 12:08 Analyzed: 01/09/2020 14:33
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Suspended Solids
89
2.5
mg/L
100 89 80-120
Duplicate (OA08038-DUPl)
Prepared: 01/08/2020 12:08 Analyzed: 01/09/2020 14:33
Source: CC21020-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Suspended Solids
29000
5000
mg/L
20000 33
20
QM-12
Duplicate (OA08038-DUP2)
Prepared: 01/08/2020 12:08 Analyzed: 01/09/2020 14:33
Source: CC20344-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Suspended Solids
160
35
mg/L
160 0
20
Batch OA1OO25 - NO PREP
Blank (OA10025-BLKi) Prepared: 01/10/2020 10:19 Analyzed: 01/10/2020 14:17
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Nitrate/Nitrite as N 0.041 U 0.10 mg/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OA1OO25 - NO PREP - Continued
LCS (OA30025-BSI) Prepared: 01/10/2020 10:19 Analyzed: 01/10/2020 14:18
Spike Source %REC
RPD
Analvte
Result
Flag
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
1.3
0.10
mg/L
1.25 102 90-110
Matrix Spike (OA10025-MS3)
Prepared: 01/10/2020 10:19 Analyzed: 01/10/2020 14:22
Source: CC20344-01
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
1.3
0.10
mg/L
0.521 0.78 108 90-110
Matrix Spike (OA10025-MS2)
Prepared: 01/10/2020 10:19 Analyzed: 01/10/2020 14:27
Source: CC20969-01
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
0.77
0.10
mg/L
0.521 0.51 51 90-110
QM-07
Matrix Spike Dup (OA30025-MSD1)
Prepared: 01/10/2020 10:19 Analyzed: 01/10/2020 14:24
Source: CC20344-01
Spike Source %REC
RPD
Analvte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
1.3
0.10
mg/L
0.521 0.78 107 90-110 0.3
10
Batch OA1OO45 - NO PREP
Blank (OA30045-BLKi) Prepared & Analyzed: 01/10/2020 15:49
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Total Solids 0.0050 U 0.0050 % by Volume
LCS (OA30045-BSI) Prepared & Analyzed: 01/10/2020 15:49
Spike Source %REC
RPD
Analvte
Result
Flag POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Solids
1100
50
mg/L
1100 99 80-120
Duplicate (OA30045-DUPl)
Prepared & Analyzed: 01/10/2020 15:49
Source: CC20361-01
Spike Source %REC
RPD
Analvte
Result
Flag POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Solids
0.33
0.0050
% by Volume
0.33 0.006
20
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 13

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-12 Precision between duplicate samples was outside acceptance limits.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 13

ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD
www.encolabs.com
10775 Central Port Dr. 4810 Executive Park Court, Suite 111
1 D2-A Woodwinds Industrial Ct.
=SNOrlando.
CO
FL 32824 Jacksonville, FL 32216-6069
[phone] [phone] Fax [phone]
Cary, NC 27511
[phone] Fax [phone]
Page Of
Client Name Project Number
Novozyrnes North America (NCXM) [none]
Address Project NamelDesc
77 Perry Chao Church Road Monthly -Week One -SBM
a
Y
�
Requested Analyses
�
Requested Turnaround
Times
Note : Rush requests subject to
acceptance by the facility
CitylSTlZip
Frankiintlon, NC 27525
Tel Fax
(919) 494
Sam ] Name. (Print)
Sampl sign
Po # 1 Billing Into
3800414630
Reporting Contact-30DQ
Seoit Creech
BillinCc tact
nts Payable
Site Location 1 Time Zone
;
{
k
�p
mlo
O
cooV
to
p
2
= I-
_ Standard
_Expedited
due
Lab Workorder
CC21020
Preservation(See Codes) (Combine as necessary)
Collection Matrix Total it of
item # Sample ID (Field identification) Collection Bate Time Comp l Grab (see codes) Containers
Sample Comments
SBM
6?-
SL
B
X
X
X
X
X
X
X
<- Total # of Containers
Sample Kit Prepared'Ry Date!rime Reli hod 8
Datatet,Time/}h
Received B
DatwTime
'
CommenlslSpecial Reporting Requirements
elinqu By
Dale/Time
Race B
'
D/ate i e
(%1
t
511
Relinquished By
DateMme
Received By
batelflmN
Cooler #'s e. Temps on Receipt
- L
Condition Uppoo.� Receipt
YAcceptable , Unacceptable
Matrix : OW -Groundwater So -Soil DW-Drinking Water SE -Sediment SW-Suftce Water WIN -Wastewater A -Air O-Other (detail in comments) Preservation: I -Ice H-HCl N-HNO3 S-H2SO4 NO-N80H o-Other (detail in comments)
Note : All samples submitted to ENCO Labs are in accordance with the terms and conditions listed on the reverse of this form. unless prior written agreements exist

Sample Preservation Verification
ENCQ Cary
Work Order: CC21020 Project: Monthly - Week One - SBM
Client: Novozymes North America (N0008) Project #: [none]
Lagged In: 07-Jan-20 10:43 Logged By: John C King
Preservation Check Performed By: I(. DatelTime: f ZO /(Jgo
CC21020-01
Cunt
Type
Yp
Pres (pH)
Requirement
pH Checked 1
in Control
DatefTime
PH Adjusted Adjusted
Reagent Used/Comments
C
250mLP+H2SO4
<2
Y 1(5)1 NA
& 1 N / NA 1_ �? Zv ,
f zmG
D
250mLP+HNO3
<2
Y I N I NA
/ N / NA ,
2IN- r/
90
Rea ent Name ID
1
2
pH Strip ID: �� [
Rea ent Name ID
3
4
Rea ent Name ID
5
6
C �1ELMNT\Printlwko_PreservationCheck.rpt
Page 1 of 1

2�SQ pCCgF ENCO Laboratories
9e0
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Thursday, February 13, 2020
Novozymes North America (N0008)
Attn: Scott Creech
77 Perry Chapel Church Road
Franklinton, NC 27525
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: Monthly - Week One - SBM
ENCO Workorder(s): CDO0226
Dear Scott Creech,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, February 4, 2020.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
0"6LC'=-:;tA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 14

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: SBM
Lab ID: CD00226-01
Sampled: 02/04/20 08:00
Received: 02/04/20 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
CSU Method
NO PREP
10/30/22
02/04/20
10:25
02/07/20
15:57
EPA 350.1
NO PREP
03/03/20
02/10/20
14:49
02/10/20
18:50
EPA 351.2
Same
03/03/20
02/06/20
09:38
02/06/20
16:57
EPA 353.2
NO PREP
02/06/20
08:00
02/05/20
08:41
02/05/20
11:44
EPA 353.2
[CALC]
02/06/20
08:00
02/11/20
10:42
02/11/20
17:24
EPA 6010D
EPA 3005A
08/02/20
02/04/20
10:25
02/07/20
11:02
EPA 7470A
EPA 7470A
03/03/20
02/06/20
09:38
02/07/20
16:34
SM 254OB-2011
NO PREP
02/11/20
02/06/20
12:25
02/06/20
12:25
SM 2540D-2011
NO PREP
02/11/20
02/05/20
14:11
02/05/20
14:11
SM 4500CIE-2011
NO PREP
03/03/20
02/12/20
14:13
02/12/20
15:06
SM 5210 B-2011
NO PREP
02/06/20
08:00
02/05/20
13:33
02/05/20
13:33
SM 5220D-2011
Same
03/03/20
02/06/20
10:03
02/06/20
17:21
Client ID: SBM
Lab ID: CD00226-OIRE1
Sampled: 02/04/20 08:00
Received: 02/04/20 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 353.2
NO PREP
03/03/20
02/11/20
10:42
02/11/20
17:24
EPA 365.4
Same
03/03/20
02/06/20
09:38
02/07/20
09:52
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 14

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SAMPLE DETECTION SUMMARY :1
Client ID: SBM
Lab ID:
CDO0226-01
Analvte
Results
Flag
MDL
Q
Units
Method Notes
Aluminum - Total
615
0.420
1.00
mg/L
EPA 6010D
Ammonia as N
62
D
4.0
9.0
mg/L
EPA 350.1
Biochemical Oxygen Demand
8800
2.0
2.0
mg/L
SM 5210 B-2011 B-04
Calcium - Total
2100
0.390
1.00
mg/L
EPA 6010D
Chemical Oxygen Demand
32000
800
800
mg/L
SM 5220D-2011
Chloride
200
1.9
5.0
mg/L
SM 4500CI E-2011
Copper- Total
0.539
0.0160
0.100
mg/L
EPA 6010D
Magnesium - Total
76.7
0.290
1.00
mg/L
EPA 6010D
Molybdenum - Total
0.0796
3
0.0250
0.100
mg/L
EPA 6010D
Nickel - Total
0.0717
3
0.0220
0.100
mg/L
EPA 6010D
Nitrate as N
1000
D
20
50
mg/L
EPA 353.2
Nitrite as N
0.54
0.017
0.10
mg/L
EPA 353.2
Potassium - Total
542
1.50
5.00
mg/L
EPA 6010D
Sodium - Total
284
4.00
5.00
mg/L
EPA 6010D
Sodium Adsorption Ratio
1.65
[blank]
CSU Method
Total Kjeldahl Nitrogen
1700
D
26
48
mg/L
EPA 351.2
Total Solids
5.1
0.25
0.25
% by Volume
SM 254OB-2011
Total Suspended Solids
34000
2500
2500
mg/L
SM 2540D-2011
Zinc - Total
1.86
0.0440
0.100
mg/L
EPA 6010D
Client ID: SBM
Lab ID:
CD00226-01RE1
Anal a
Results
Flag
MDL
POLL
Units
Method Notes
Nitrate/Nitrite as N
1000
D
20
50
mg/L
EPA 353.2
Phosphorus
630
D
12
50
mg/L
EPA 365.4
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 14

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ANALYTICAL RESULTS
Description: SBM Lab Sample ID:CD00226-01 Received: 02/04/20 10:15
Matrix: Sludge Sampled:02/04/20 08:00 Work Order: CD00226
Project: Monthly - Week One - SBM Sampled By: Adam Fauccette
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
Mercury [7439-97-6]^
0.000750
U
mg/L
5
0.000750
0.00100
OB06016
EPA 7470A
02/07/20 16:34
KAH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Ay
Notes
Aluminum [7429-90-5]^
615
mg/L
10
0.420
1.00
OB04031
EPA 6010D
02/07/20 11:02
JDH
Arsenic [7440-38-2]^
0.0760
U
mg/L
10
0.0760
0.100
OB04031
EPA 6010D
02/07/20 11:02
JDH
Cadmium [7440-43-9]^
0.00360
U
mg/L
10
0.00360
0.0100
OB04031
EPA 6010D
02/07/20 11:02
JDH
Calcium [7440-70-2]^
2100
mg/L
10
0.390
1.00
OB04031
EPA 6010D
02/07/20 11:02
JDH
Copper[7440-50-8]^
0.539
mg/L
10
0.0160
0.100
OB04031
EPA 6010D
02/07/20 11:02
JDH
Lead [7439-92-1]^
0.0310
U
mg/L
10
0.0310
0.100
OB04031
EPA 6010D
02/07/20 11:02
JDH
Magnesium [7439-95-4]^
76.7
mg/L
10
0.290
1.00
OB04031
EPA 6010D
02/07/20 11:02
JDH
Molybdenum [7439-98-7]^
0.0796
J
mg/L
10
0.0250
0.100
OB04031
EPA 6010D
02/07/20 11:02
JDH
Nickel[7440-02-O]^
0.0717
J
mg/L
10
0.0220
0.100
OB04031
EPA 6010D
02/07/20 11:02
JDH
Potassium [7440-09-7]^
542
mg/L
10
1.50
5.00
OB04031
EPA 6010D
02/07/20 11:02
JDH
Selenium [7782-49-2]^
0.0620
U
mg/L
10
0.0620
0.100
OB04031
EPA 6010D
02/07/20 11:02
JDH
Sodium [7440-23-5]^
284
mg/L
10
4.00
5.00
OB04031
EPA 6010D
02/07/20 11:02
JDH
Zinc[7440-66-6]^
1.86
mg/L
10
0.0440
0.100
OB04031
EPA 6010D
02/07/20 11:02
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Ay
Notes
Ammonia as N [7664-41-7]^
62
D
mg/L
90
4.0
9.0
OB10034
EPA 350.1
02/10/20 18:50
AKF
Biochemical Oxygen Demand^
8800
mg/L
1
2.0
2.0
OB05002
SM 5210 B-2011
02/05/20 13:33
JOC
B-04
Chemical Oxygen Demand^
32000
mg/L
80
800
800
OB05059
SM 5220D-2011
02/06/20 17:21
JOC
Chloride [16887-00-6]^
200
mg/L
1
1.9
5.0
OB12050
SM 4500CIE-2011
02/12/20 15:06
AKF
Nitrate as N [14797-55-8]
1000
D
mg/L
500
20
50
[CALC]
EPA 353.2
02/11/20 17:24
AKF
Nitrate/Nitrite as N^
1000
D
mg/L
500
20
50
OB11020
EPA 353.2
02/11/20 17:24
AKF
Nitrite as N [14797-65-0]^
0.54
mg/L
1
0.017
0.10
OB05015
EPA 353.2
02/05/20 11:44
AKF
Phosphorus[7723-14-O]^
630
D
mg/L
500
12
50
OB06004
EPA 365.4
02/07/20 09:52
AKF
Sodium Adsorption Ratio
1.65
[blank]
1
OB04031
CSU Method
02/07/20 15:57
JDH
Total Kjeldahl Nitrogen^
1700
D
mg/L
100
26
48
OB06005
EPA 351.2
02/06/20 16:57
AKF
Total Solids^
5.1
% by Volume
50
0.25
0.25
OB06003
SM 2540B-2011
02/06/20 12:25
JOC
Total Suspended Solids^
34000
mg/L
1000
2500
2500
OB05045
SM 2540D-2011
02/05/20 14:11
BDC
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 14

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch OBO6O16 - EPA 747OA
Blank (OB06016-BLK3) Prepared: 02/06/2020 09:38 Analyzed: 02/07/2020 15:43
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Mercury 0.000150 U 0.000200 mg/L
Blank (OB06016-BLK2) Prepared: 02/06/2020 09:38 Analyzed: 02/07/2020 15:46
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Mercury 0.00300 U 0.00400 mg/L
LCS (OB06016-BSI) Prepared: 02/06/2020 09:38 Analyzed: 02/07/2020 15:48
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00513
0.000200
mg/L
0.00500
103
80-120
Matrix Spike (OB06016-MS3)
Prepared: 02/06/2020 09:38 Analyzed: 02/07/2020 15:54
Source: CD00845-02
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00512
0.000200
mg/L
0.00500
0.000195
99
75-125
Matrix Spike Dup (OB06016-MSD1)
Prepared: 02/06/2020 09:38 Analyzed: 02/07/2020 15:57
Source: CD00845-02
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00527
0.000200
mg/L
0.00500
0.000195
102
75-125 3
25
Post Spike (OB06016-PS1)
Prepared: 02/06/2020 09:38 Analyzed: 02/07/2020 16:04
Source: CD00845-02
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
5.76
0.200
ug/L
5.00
0.195
111
75-125
Metals (total recoverable) by EPA 6000/7000
Series Methods - Quality Control
Batch OBO4O31 - EPA 3OO5A
Blank (OB04031-BLK3) Prepared: 02/04/2020 10:25 Analyzed: 02/07/2020 09:56
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Aluminum
0.0420
U
0.100
mg/L
Arsenic
0.00760
U
0.0100
mg/L
Cadmium
0.000360
U
0.00100
mg/L
Calcium
0.0390
U
0.100
mg/L
Copper
0.00160
U
0.0100
mg/L
Lead
0.00310
U
0.0100
mg/L
Magnesium
0.0290
U
0.100
mg/L
Molybdenum
0.00250
U
0.0100
mg/L
Nickel
0.00220
U
0.0100
mg/L
Potassium
0.150
U
0.500
mg/L
Selenium
0.00620
U
0.0100
mg/L
Sodium
0.400
U
0.500
mg/L
Zinc
0.00440
U
0.0100
mg/L
FINAL
This report relates only
to the sample as received by the laboratory, and may only be reproduced in full.
Page 5 of 14

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch OBO4O31 - EPA 3OO5A - Continued
Blank (OB04031-BLK2) Prepared: 02/04/2020 10:25 Analyzed: 02/07/2020 09:59
Spike Source O/oREC RPD
Analvte
Result
Flaq
POL
Units Level Result O/oREC Limits RPD Limit Notes
Aluminum
0.0420
U
0.100
mg/L
Arsenic
0.00760
U
0.0100
mg/L
Cadmium
0.000360
U
0.00100
mg/L
Calcium
0.0390
U
0.100
mg/L
Copper
0.00160
U
0.0100
mg/L
Lead
0.00310
U
0.0100
mg/L
Magnesium
0.0290
U
0.100
mg/L
Molybdenum
0.00250
U
0.0100
mg/L
Nickel
0.00220
U
0.0100
mg/L
Potassium
0.150
U
0.500
mg/L
Selenium
0.00620
U
0.0100
mg/L
Sodium
0.400
U
0.500
mg/L
Zinc
0.00440
U
0.0100
mg/L
LCS (OB04031-BS1)
Prepared: 02/04/2020 10:25 Analyzed: 02/07/2020 10:06
Spike
Source
O/oREC RPD
Analvte
Result
Flaq POL
Units
Level
Result O/oREC
Limits RPD Limit Notes
Aluminum
2.01
0.100
mg/L
2.00
101
80-120
Arsenic
0.199
0.0100
mg/L
0.200
99
80-120
Cadmium
0.0201
0.00100
mg/L
0.0200
100
80-120
Calcium
1.90
0.100
mg/L
2.00
95
80-120
Copper
0.199
0.0100
mg/L
0.200
99
80-120
Lead
0.196
0.0100
mg/L
0.200
98
80-120
Magnesium
2.00
0.100
mg/L
2.00
100
80-120
Molybdenum
0.196
0.0100
mg/L
0.200
98
80-120
Nickel
0.199
0.0100
mg/L
0.200
100
80-120
Potassium
9.77
0.500
mg/L
10.0
98
80-120
Selenium
0.210
0.0100
mg/L
0.200
105
80-120
Sodium
10.1
0.500
mg/L
10.0
101
80-120
Zinc
0.201
0.0100
mg/L
0.200
100
80-120
Matrix Spike (OB04031-MS1)
Prepared:
02/04/2020 10:25 Analyzed: 02/07/2020 10:09
Source: CD01443-03
Spike
Source
O/oREC RPD
Analvte
Result
Flaq POL
Units
Level
Result
O/oREC
Limits RPD Limit Notes
Aluminum
2.06
0.100
mg/L
2.00
0.0469
101
75-125
Arsenic
0.202
0.0100
mg/L
0.200
0.00760 U
101
75-125
Cadmium
0.0198
0.00100
mg/L
0.0200
0.000360 U
99
75-125
Calcium
2.09
0.100
mg/L
2.00
0.187
95
75-125
Copper
0.199
0.0100
mg/L
0.200
0.00253
98
75-125
Lead
0.195
0.0100
mg/L
0.200
0.00310 U
97
75-125
Magnesium
2.23
0.100
mg/L
2.00
0.194
102
75-125
Molybdenum
0.195
0.0100
mg/L
0.200
0.00250 U
98
75-125
Nickel
0.197
0.0100
mg/L
0.200
0.00220 U
99
75-125
Potassium
20.6
0.500
mg/L
10.0
10.8
98
75-125
Selenium
0.190
0.0100
mg/L
0.200
0.00620 U
95
75-125
Sodium
31.6
0.500
mg/L
10.0
22.0
95
75-125
Zinc
0.268
0.0100
mg/L
0.200
0.0707
98
75-125
FINAL
This report relates only to the sample as received by the
laboratory, and may only be reproduced in
full. Page 6 of 14

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch OB04031 - EPA 3005A - Continued
Matrix Spike Dup (OB04031-MSDI)
Prepared:
02/04/2020
10:25 Analyzed: 02/07/2020 10:11
Source: CDO1443-03
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Aluminum
2.05
0.100
mg/L
2.00
0.0469
100
75-125
0.4
20
Arsenic
0.207
0.0100
mg/L
0.200
0.00760 U
103
75-125
2
20
Cadmium
0.0205
0.00100
mg/L
0.0200
0.000360 U
103
75-125
3
20
Calcium
2.12
0.100
mg/L
2.00
0.187
97
75-125
1
20
Copper
0.202
0.0100
mg/L
0.200
0.00253
100
75-125
2
20
Lead
0.201
0.0100
mg/L
0.200
0.00310 U
101
75-125
3
20
Magnesium
2.23
0.100
mg/L
2.00
0.194
102
75-125
0.2
20
Molybdenum
0.201
0.0100
mg/L
0.200
0.00250 U
100
75-125
3
20
Nickel
0.203
0.0100
mg/L
0.200
0.00220 U
101
75-125
3
20
Potassium
20.7
0.500
mg/L
10.0
10.8
99
75-125
0.5
20
Selenium
0.191
0.0100
mg/L
0.200
0.00620 U
96
75-125
0.5
20
Sodium
31.7
0.500
mg/L
10.0
22.0
97
75-125
0.4
20
Zinc
0.274
0.0100
mg/L
0.200
0.0707
101
75-125
2
20
Post Spike (OB04031-PS1)
Prepared:
02/04/2020
10:25 Analyzed: 02/07/2020 10:14
Source: CDO1443-03
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Aluminum
2.11
0.100
mg/L
2.00
0.0469
103
80-120
Arsenic
0.204
0.0100
mg/L
0.200
0.00269
101
80-120
Cadmium
0.0206
0.00100
mg/L
0.0200
-0.000246
103
80-120
Calcium
2.21
0.100
mg/L
2.00
0.187
101
80-120
Copper
0.207
0.0100
mg/L
0.200
0.00253
102
80-120
Lead
0.207
0.0100
mg/L
0.200
-0.00300
104
80-120
Magnesium
2.27
0.100
mg/L
2.00
0.194
104
80-120
Molybdenum
0.203
0.0100
mg/L
0.200
0.00126
101
80-120
Nickel
0.205
0.0100
mg/L
0.200
0.000913
102
80-120
Potassium
21.1
0.500
mg/L
10.0
10.8
102
80-120
Selenium
0.219
0.0100
mg/L
0.200
-0.00631
109
80-120
Sodium
31.9
0.500
mg/L
10.0
22.0
99
80-120
Zinc
0.276
0.0100
mg/L
0.200
0.0707
103
80-120
Classical Chemistry Parameters
- Quality Control
Batch 0804031 - EPA 3005A
Blank (OB04031-BLK3) Prepared: 02/04/2020 10:25 Analyzed: 02/07/2020 16:00
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Sodium Adsorption Ratio
0.00
U
[blank]
Blank (OB04031-BLK2)
Prepared: 02/04/2020 10:25 Analyzed: 02/07/2020 16:00
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Sodium Adsorption Ratio
0.00
U
[blank]
Batch OB05002 - NO PREP
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 14

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OBO5OO2 - NO PREP - Continued
Blank (OB05002-BLK1)
Prepared & Analyzed: 02/05/2020 13:33
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Biochemical Oxygen Demand
2.0
U
2.0
mg/L
LCS (OB05002-BS1)
Prepared & Analyzed: 02/05/2020 13:33
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Biochemical Oxygen Demand
170
2.0
mg/L
198 86 85-115
B-04
Duplicate (OB05002-DUPI)
Prepared & Analyzed: 02/05/2020 13:33
Source: CC20426-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Biochemical Oxygen Demand
1000
2.0
mg/L
980 6
30
B-04
Batch OBO5O15 - NO PREP
Blank (OB05015-BLK1)
Prepared: 02/05/2020 08:41 Analyzed: 02/05/2020 11:37
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
0.017
U
0.10
mg/L
LCS (OB05015-BS1)
Prepared: 02/05/2020 08:41 Analyzed: 02/05/2020 11:31
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
0.99
0.10
mg/L
1.00 99 90-110
Matrix Spike (0B05015-MS3)
Prepared: 02/05/2020 08:41 Analyzed: 02/05/2020 11:41
Source: CD00225-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
1.5
0.10
mg/L
1.00 0.44 105 90-110
Matrix Spike (OBO5015-MS2)
Prepared: 02/05/2020 08:41 Analyzed: 02/05/2020 11:49
Source: CD00842-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
1.1
0.10
mg/L
1.00 0.017 U 107 90-110
Matrix Spike Dup (OB05015-MSD1)
Prepared: 02/05/2020 08:41 Analyzed: 02/05/2020 11:42
Source: CD00225-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
1.6
0.10
mg/L
1.00 0.44 112 90-110 5
10
QM-07
Batch OBO5O45 - NO PREP
Blank (OB05045-BLK3) Prepared & Analyzed: 02/05/2020 14:11
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Suspended Solids 2.5 U 2.5 mg/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 14

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OB05045 - NO PREP - Continued
LCS (OB05045-BSI)
Prepared & Analyzed: 02/05/2020 14:11
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Suspended Solids
90
2.5
mg/L
100 90 80-120
Duplicate (OB05045-DUPl)
Prepared & Analyzed: 02/05/2020 14:11
Source: CC20551-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Suspended Solids
1100
160
mg/L
1200 4
20
Duplicate (OB05045-DUP2)
Prepared & Analyzed: 02/05/2020 14:11
Source: CDO1352-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Suspended Solids
200
42
mg/L
200 2
20
Batch OB05059 - Same
Blank (OB05059-BLK1)
Prepared: 02/06/2020 00:03 Analyzed: 02/06/2020 17:21
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chemical Oxygen Demand
10
U
10
mg/L
LCS (OB05059-BS1)
Prepared: 02/06/2020 00:03 Analyzed: 02/06/2020 17:21
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chemical Oxygen Demand
520
10
mg/L
500 103 90-110
Matrix Spike (OB05059-MS3)
Prepared: 02/06/2020 00:03 Analyzed: 02/06/2020 17:21
Source: CC20882-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chemical Oxygen Demand
67000
800
mg/L
40000 29000 96 90-110
Matrix Spike Dup (OB05059-MSDI)
Prepared: 02/06/2020 00:03 Analyzed: 02/06/2020 17:21
Source: CC20882-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chemical Oxygen Demand
67000
800
mg/L
40000 29000 97 90-110 0.5
5
Batch 0806003 - NO PREP
Blank (OB06003-BLK3) Prepared & Analyzed: 02/06/2020 12:25
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Solids
0.0050
U 0.0050
% by Volume
LCS (OB06003-BSI)
Prepared & Analyzed: 02/06/2020 12:25
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Solids
1100
50
mg/L
1100 99 80-120
FINAL
This report relates only to the sample
as received by the
laboratory, and may only be reproduced in full.
Page 9 of 14

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OBO6003 - NO PREP - Continued
Duplicate (OB06003-DUPl) Prepared & Analyzed: 02/06/2020 12:25
Source: CD00225-01
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Solids 0.23 0.0050 % by Volume 0.24 1 20
Batch OBO6OO4 - Same
Blank (OB06004-BLK3) Prepared: 02/06/2020 09:38 Analyzed: 02/06/2020 18:32
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
0.025
U
0.10
mg/L
LCS (OB06004-BSI)
Prepared: 02/06/2020 09:38 Analyzed: 02/06/2020 18:34
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
1.5
0.10
mg/L
1.60 96 80-120
Matrix Spike (OB06004-MS1)
Prepared: 02/06/2020 09:38 Analyzed: 02/07/2020 09:48
Source: CC12870-01RE1
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
8.8
D
1.0
mg/L
0.640 8.3 88 80-120
Matrix Spike Dup (OB06004-MSD1)
Prepared: 02/06/2020 09:38 Analyzed: 02/07/2020 09:49
Source: CC32870-01RE3
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
9.1
D
1.0
mg/L
0.640 8.3 123 80-120 2
25
QM-07
Batch OBO6OO5 - Same
Blank (OB06005-BLK3)
Prepared: 02/06/2020 09:38 Analyzed: 02/06/2020 16:36
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
0.26
U
0.48
mg/L
LCS (OB06005-BSI)
Prepared: 02/06/2020 09:38 Analyzed: 02/06/2020 16:38
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
12
0.48
mg/L
12.0 102 90-110
Matrix Spike (OB06005-MS3)
Prepared: 02/06/2020 09:38 Analyzed: 02/06/2020 16:41
Source: CC12870-01
Spike Source %REC
RPD
Analvte
Result
Flaa
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
11
0.48
mg/L
4.80 5.9 104 90-110
Matrix Spike (OB06005-MS2)
Prepared: 02/06/2020 09:38 Analyzed: 02/06/2020 16:47
Source: CC20426-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
84
D
2.4
mg/L
4.80 83 21 90-110
QM-07
FINAL
This report relates only to
the sample as received by the
laboratory, and may only be reproduced in full.
Page 10 of 14

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OB06005 - Same - Continued
Matrix Spike Dup (OB06005-MSDI) Prepared: 02/06/2020 09:38 Analyzed: 02/06/2020 16:43
Source: CC12870-01
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Kjeldahl Nitrogen 11 0.48 mg/L 4.80 5.9 111 90-110 3 10 QM-07
Batch OB10034 - NO PREP
Blank (OB10034-BLK3) Prepared: 02/10/2020 14:49 Analyzed: 02/10/2020 18:28
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Ammonia as N 0.045 U 0.10 mg/L
LCS (OB10034-BSI) Prepared: 02/10/2020 14:49 Analyzed: 02/10/2020 18:30
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
0.96
0.10
mg/L
1.01 95 90-110
Matrix Spike (OB10034-MS3)
Prepared: 02/10/2020 14:49 Analyzed: 02/10/2020 18:33
Source: CC12870-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
0.51
0.10
mg/L
0.393 0.19 81 90-110
QM-07
Matrix Spike (OB10034-MS2)
Prepared: 02/10/2020 14:49 Analyzed: 02/11/2020 10:20
Source: CC20551-02RE3
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
10
1.0
mg/L
4.04 6.0 102 90-110
Matrix Spike Dup (OB30034-MSDI)
Prepared: 02/10/2020 14:49 Analyzed: 02/10/2020 18:35
Source: CC12870-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
0.51
0.10
mg/L
0.393 0.19 82 90-110 0.9
10
QM-07
Batch OB11020 - NO PREP
Blank (OB31020-BLK1) Prepared: 02/11/2020 10:42 Analyzed: 02/11/2020 14:02
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Nitrate/Nitrite as N 0.041 U 0.10 mg/L
LCS (OB33020-BS3) Prepared: 02/11/2020 10:42 Analyzed: 02/11/2020 14:04
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrate/Nitrite as N
1.3
0.10
mg/L
1.25 103 90-110
Matrix Spike (OB13020-MS3)
Prepared: 02/11/2020 10:42 Analyzed: 02/11/2020 14:08
Source: CC12870-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrate/Nitrite as N
0.95
0.10
mg/L
0.521 0.43 100 90-110
FINAL
This report relates only to
the sample as received by the
laboratory, and may only be reproduced in full.
Page 11 of 14

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OB11O2O - NO PREP - Continued
Matrix Spike (OB11020-MS2)
Prepared: 02/11/2020 10:42 Analyzed: 02/11/2020 14:13
Source: CC20426-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrate/Nitrite as N
0.99
0.10
mg/L
0.521 0.40 113 90-110
QM-07
Matrix Spike Dup (OB33020-MSD1)
Prepared: 02/11/2020 10:42 Analyzed: 02/11/2020 14:10
Source: CC12870-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrate/Nitrite as N
0.97
0.10
mg/L
0.521 0.43 104 90-110 3
10
Batch OB12O5O - NO PREP
Blank (OB32050-BLK3) Prepared: 02/12/2020 14:13 Analyzed: 02/12/2020 15:03
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Chloride 1.9 U 5.0 mg/L
LCS (OB12050-BSI) Prepared: 02/12/2020 14:13 Analyzed: 02/12/2020 15:04
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chloride
98
5.0
mg/L
100 98 80-120
Duplicate (OB12050-DUPl)
Prepared: 02/12/2020 14:13 Analyzed: 02/12/2020 15:07
Source: CD00226-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chloride
200
5.0
mg/L
200 2
10
Matrix Spike (OB12050-MS3)
Prepared: 02/12/2020 14:13 Analyzed: 02/12/2020 15:05
Source: CD00047-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chloride
1100
50
mg/L
400 790 87 80-120
Matrix Spike Dup (OB12050-MSDI)
Prepared: 02/12/2020 14:13 Analyzed: 02/12/2020 15:05
Source: CD00047-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chloride
1100
50
mg/L
400 790 89 80-120 0.5
25
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 14

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
B-04 The average DO uptake of the seeded controls does not meet the method required 0.6 - 1.0 mg/L.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 14

10775 Centre! Pon Dr. 4810 Executive Park Cowl. Suite 111 102-A Woodwinds Industrial Ct.
Orlando, FL 32824 Jacksonville, FL 32216-60M Cary, NC 27511
(407) UM314 (9G4) 296-3007 Fax [phone]D (8191467-3090 Fax [phone] Page of
Client Name
Noviozyfflies North America (NOM)
Project Number
[clone]
Requested
Analyses
Requested Turnaround
Times
Nota :Rush requests subject to
acceptance by the facility
_ Standard
_ Expedited
Due
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Address
77 Ferry Chapel Church Road
Project NamefDesc
Monthly - Week One - SBM
ChyISTIDp
Fr&vMnton, NC 27525
PO # f Billing Info
3800414630
Tel
[phone]
Fax
Reporting Contact
Scot Creech
Sampler(s) Name, Affiliation !Print)
Billing Contact
Accounts Payable.
Samplers) Signature
Site Location I Time Zane
Lab 1Noricorder
% D V ! 226
Preservation
(See
Codes)
(Combine
as necessary)
ltem #
Sample ID (Field Idenlification)
Collection Dale
Collection
Time
Comp! Grab
Matrix
(see codes)
Total # Of
Containers
Sample Comments
SBM
SL
B
X
X
X
X
X
X
X
< Total # of Containers
Sample Kit Prepared By
DatelTime
Relinquished By
Dateffime
Received By
Dalemme
Comments/Special Reporting Requirements
Relinquished By
Daternme
Receiv y
Dateffime
t�rao
to: 6
Relinquished By
Date>tme
Received By
Dale/Time
Cooler it's & Temps On Receipt
Comditian Receipt
ay
Acceptable Unacceptable
Matrix: GW-Groundwater SO -Soil DW-Drinking Water SE-Secilment SW -Surface Water WW-Wastewater A -Air O-Other (detail in comments) Preservation. ]-Ice H-HCI N-HNO3 S-H2SO4 NO-NaOH O-Other (detail in comments)
Note: All samples submitted to ENCO Labs are in accordance with the terms and conditions listed on the reverse of this form, unless prior written agreements exist

Sample Preservation Verification
ENCO Cary
Work Order: CDO0226 Project: Monthly - Week One - SBM
Client: Novozymes North America (NO008) Project #: [none]
Logged In: 04-Feb-20 10:51 _ Logged By: John C King
1 Preservation Check Performed By: 1 Date[Time: /OS�� � i� i�
CDO0226-01
Corsi
Type
Pres (pH)
Requirement
pH Checked !
In Control
pH Adjusted DateMme
Adjusted
Reagent Used/Comments
C
250mLP+H2SO4
<2
Y LN)/ NA
1 N / NA r�'�LU A-10
+2mL jr�5(j
D
250mLP+HNO3
<2
Y 1 N / NA
/ N / NA
Al 41b
Rea ent Name ID
1 11-Au?lJ -?u S
2
pH Strip ID:�(��%�
Rea ent Name ID
3
4
Reagent Name ID
5
6
C:IELMNTIPrintlwko_PreservationCheck. rpt Page 1

2�SQ pCCgF ENCO Laboratories
9e0
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Wednesday, April 8, 2020
Novozymes North America (N0008)
Attn: Scott Creech
77 Perry Chapel Church Road
Franklinton, NC 27525
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: Monthly - Week One - SBM
ENCO Workorder(s): CD02113
Dear Scott Creech,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, March 3, 2020.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
0"6LC'=-:;tA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 13

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: SBM
Lab ID: CD02113-01
Sampled: 03/03/20 06:00
Received: 03/03/20 10:35
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
CSU Method
NO PREP
11/27/22
03/03/20 12:52
03/05/20 15:21
EPA 350.1
NO PREP
03/31/20
03/10/20 15:13
03/10/20 17:45
EPA 351.2
Same
03/31/20
03/04/20 10:41
03/12/20 11:48
EPA 353.2
NO PREP
03/05/20 06:00
03/03/20 14:30
03/03/20 16:38
EPA 353.2
[CALC]
03/05/20 06:00
03/11/20 09:24
03/11/20 13:42
EPA 353.2
NO PREP
03/31/20
03/11/20 09:24
03/11/20 13:42
EPA 6010D
EPA 3005A
08/30/20
03/03/20 12:52
03/05/20 10:58
EPA 7470A
EPA 7470A
03/31/20
03/04/20 09:56
03/04/20 16:07
SM 2540D-2011
NO PREP
03/10/20
03/05/20 12:01
03/05/20 13:13
SM 5210 B-2011
NO PREP
03/05/20 06:00
03/03/20 14:18
03/03/20 14:18
SM 5220D-2011
Same
03/31/20
03/06/20 09:48
03/06/20 15:56
Client ID: SBM
Lab ID: CD02113-01RE1
Sampled: 03/03/20 06:00
Received: 03/03/20 10:35
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 365.4
Same
03/31/20
03/04/20 10:41
03/12/20 17:07
SM 254OB-2011
NO PREP
03/10/20
04/06/20 17:40
03/09/20 16:43
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 13

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SAMPLE DETECTION SUMMARY
Client ID: SBM
Lab ID:
CD02113-01
Analvte
Results
Flag
MDL
Q
Units
Method Notes
Aluminum - Total
150
0.420
1.00
mg/L
EPA 6010D
Ammonia as N
96
D
4.0
9.0
mg/L
EPA 350.1
Biochemical Oxygen Demand
9300
2.0
2.0
mg/L
SM 5210 B-2011
Calcium - Total
2020
0.390
1.00
mg/L
EPA 6010D
Chemical Oxygen Demand
35000
800
800
mg/L
SM 5220D-2011
Copper - Total
0.259
0.0160
0.100
mg/L
EPA 6010D
Magnesium - Total
27.9
0.290
1.00
mg/L
EPA 6010D
Molybdenum - Total
0.0396
3
0.0250
0.100
mg/L
EPA 6010D
Nickel - Total
0.0571
3
0.0220
0.100
mg/L
EPA 6010D
Nitrate as N
13
D
0.82
2.0
mg/L
EPA 353.2
Nitrate/Nitrite as N
13
D
0.82
2.0
mg/L
EPA 353.2
Nitrite as N
0.042
3
0.017
0.10
mg/L
EPA 353.2
Potassium - Total
510
1.50
5.00
mg/L
EPA 6010D
Sodium - Total
301
4.00
5.00
mg/L
EPA 6010D
Sodium Adsorption Ratio
1.82
[blank]
CSU Method
Total Kjeldahl Nitrogen
1900
D
26
48
mg/L
EPA 351.2
Total Suspended Solids
25000
2500
2500
mg/L
SM 2540D-2011
Zinc - Total
0.645
0.0440
0.100
mg/L
EPA 6010D
Client ID: SBM
Lab ID:
CD02113-01RE1
Analvte
Results
Flag
MDL
Q
Units
Method Notes
Phosphorus
650
D
12
50
mg/L
EPA 365.4
Total Solids
4.0
0.0050
0.0050
% by Volume
SM 254OB-2011 Q-01
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 13

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ANALYTICAL RESULTS
Description: SBM Lab Sample ID:CD02113-01 Received: 03/03/20 10:35
Matrix: Sludge Sampled: 03/03/20 06:00 Work Order: CD02113
Project: Monthly - Week One - SBM Sampled By: Brooks Williams
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
Mercury [7439-97-6]^
0.000750
U
mg/L
5
0.000750
0.00100
0004034
EPA 7470A
03/04/20 16:07
KAH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Ay
Notes
Aluminum [7429-90-5]^
150
mg/L
10
0.420
1.00
0003027
EPA 6010D
03/05/20 10:58
JDH
Arsenic [7440-38-2]^
0.0760
U
mg/L
10
0.0760
0.100
0003027
EPA 6010D
03/05/20 10:58
JDH
Cadmium [7440-43-9]^
0.00360
U
mg/L
10
0.00360
0.0100
0003027
EPA 6010D
03/05/20 10:58
JDH
Calcium [7440-70-2]^
2020
mg/L
10
0.390
1.00
0003027
EPA 6010D
03/05/20 10:58
JDH
Copper[7440-50-8]^
0.259
mg/L
10
0.0160
0.100
0003027
EPA 6010D
03/05/20 10:58
JDH
Lead [7439-92-1]^
0.0310
U
mg/L
10
0.0310
0.100
0003027
EPA 6010D
03/05/20 10:58
JDH
Magnesium [7439-95-4]^
27.9
mg/L
10
0.290
1.00
0003027
EPA 6010D
03/05/20 10:58
JDH
Molybdenum [7439-98-7]^
0.0396
J
mg/L
10
0.0250
0.100
0003027
EPA 6010D
03/05/20 10:58
JDH
Nickel[7440-02-O]^
0.0571
J
mg/L
10
0.0220
0.100
0003027
EPA 6010D
03/05/20 10:58
JDH
Potassium [7440-09-7]^
530
mg/L
10
1.50
5.00
0003027
EPA 6010D
03/05/20 10:58
JDH
Selenium [7782-49-2]^
0.0620
U
mg/L
10
0.0620
0.100
0003027
EPA 6010D
03/05/20 10:58
JDH
Sodium [7440-23-5]^
301
mg/L
10
4.00
5.00
0003027
EPA 6010D
03/05/20 10:58
JDH
Zinc[7440-66-6]^
0.645
mg/L
10
0.0440
0.100
0003027
EPA 6010D
03/05/20 10:58
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Ay
Notes
Ammonia as N [7664-41-7]^
96
D
mg/L
90
4.0
9.0
OC10033
EPA 350.1
03/10/20 17:45
AKF
Biochemical Oxygen Demand^
9300
mg/L
1
2.0
2.0
0003028
SM 5210 B-2011
03/03/20 14:18
JOC
Chemical Oxygen Demand^
35000
mg/L
80
800
800
0006006
SM 5220D-2011
03/06/20 15:56
JOC
Nitrate as N [14797-55-8]
13
D
mg/L
20
0.82
2.0
[CALC]
EPA 353.2
03/11/20 13:42
AKF
Nitrate/Nitrite as N^
13
D
mg/L
20
0.82
2.0
OC11007
EPA 353.2
03/11/20 13:42
AKF
Nitrite as N [14797-65-0]^
0.042
J
mg/L
1
0.017
0.10
0003038
EPA 353.2
03/03/20 16:38
AKF
Phosphorus[7723-14-O]^
650
D
mg/L
500
12
50
0004018
EPA 365.4
03/12/20 17:07
AKF
Sodium Adsorption Ratio
1.82
[blank]
1
0003027
CSU Method
03/05/20 15:21
JDH
Total Kjeldahl Nitrogen^
1900
D
mg/L
100
26
48
0004017
EPA 351.2
03/12/20 11:48
AKF
Total Solids^
4.0
% by Volume
1
0.0050
0.0050
OD06021
SM 2540B-2011
03/09/20 16:43
JOC
Q-01
Total Suspended Solids^
25000
mg/L
1000
2500
2500
0005004
SM 2540D-2011
03/05/20 13:13
ZGW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 13

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch OCO4O34 - EPA 747OA
Blank (0004034-BLK3) Prepared: 03/04/2020 09:56 Analyzed: 03/04/2020 15:46
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Mercury 0.000150 U 0.000200 mg/L
LCS (0004034-BS3) Prepared: 03/04/2020 09:56 Analyzed: 03/04/2020 15:48
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00537
0.000200
mg/L
0.00500
107
80-120
Matrix Spike (0004034-MSI)
Prepared: 03/04/2020 09:56 Analyzed: 03/04/2020 15:52
Source: CD02790-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00546
0.000200
mg/L
0.00500
0.000150 U
109
75-125
Matrix Spike Dup (0004034-MSD3)
Prepared: 03/04/2020 09:56 Analyzed: 03/04/2020 15:55
Source: CD02790-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00544
0.000200
mg/L
0.00500
0.000150 U
109
75-125 0.4
25
Post Spike (0004034-PS3)
Prepared: 03/04/2020 09:56 Analyzed: 03/04/2020 16:02
Source: CD02790-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
6.21
0.200
ug/L
5.00
0.00600
124
75-125
Metals (total recoverable) by EPA 6000/7000
Series Methods - Quality Control
Batch OCO3O27 - EPA 3OO5A
Blank (0003027-BLK3)
Prepared: 03/03/2020 09:51 Analyzed: 03/05/2020 09:55
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Aluminum
0.0420
U
0.100
mg/L
Arsenic
0.00760
U
0.0100
mg/L
Cadmium
0.000360
U
0.00100
mg/L
Calcium
0.0390
U
0.100
mg/L
Copper
0.00160
U
0.0100
mg/L
Lead
0.00310
U
0.0100
mg/L
Magnesium
0.0290
U
0.100
mg/L
Molybdenum
0.00250
U
0.0100
mg/L
Nickel
0.00220
U
0.0100
mg/L
Potassium
0.150
U
0.500
mg/L
Selenium
0.00620
U
0.0100
mg/L
Sodium
0.400
U
0.500
mg/L
Zinc
0.00440
U
0.0100
mg/L
LCS (0003027-BSI)
Prepared: 03/03/2020 09:51 Analyzed: 03/05/2020 10:13
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Aluminum 1.94 0.100 mg/L 2.00 97 80-120
Arsenic 0.204 0.0100 mg/L 0.200 102 80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 13

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch OCO3O27 - EPA 3OO5A - Continued
LCS (0003027-BS1) Continued Prepared: 03/03/2020 09:51 Analyzed: 03/05/2020 10:13
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Cadmium
0.0190
0.00100
mg/L
0.0200
95
80-120
Calcium
1.97
0.100
mg/L
2.00
98
80-120
Copper
0.188
0.0100
mg/L
0.200
94
80-120
Lead
0.199
0.0100
mg/L
0.200
100
80-120
Magnesium
1.96
0.100
mg/L
2.00
98
80-120
Molybdenum
0.195
0.0100
mg/L
0.200
97
80-120
Nickel
0.194
0.0100
mg/L
0.200
97
80-120
Potassium
9.90
0.500
mg/L
10.0
99
80-120
Selenium
0.204
0.0100
mg/L
0.200
102
80-120
Sodium
10.0
0.500
mg/L
10.0
100
80-120
Zinc
0.193
0.0100
mg/L
0.200
97
80-120
Matrix Spike (0003027-MS1)
Prepared:
03/03/2020
09:51 Analyzed: 03/05/2020 10:16
Source: CD03782-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Aluminum
19.6
0.100
mg/L
2.00
17.2
121
75-125
Arsenic
0.181
0.0100
mg/L
0.200
0.00760 U
90
75-125
Cadmium
0.0178
0.00100
mg/L
0.0200
0.000360 U
89
75-125
Calcium
2.44
0.100
mg/L
2.00
0.569
94
75-125
Copper
0.207
0.0100
mg/L
0.200
0.0151
96
75-125
Lead
0.172
0.0100
mg/L
0.200
0.00310 U
86
75-125
Magnesium
2.11
0.100
mg/L
2.00
0.169
97
75-125
Molybdenum
0.203
0.0100
mg/L
0.200
0.0169
93
75-125
Nickel
0.183
0.0100
mg/L
0.200
0.00284
90
75-125
Potassium
33.6
0.500
mg/L
10.0
22.6
110
75-125
Selenium
0.204
0.0100
mg/L
0.200
0.00620 U
102
75-125
Sodium
423
0.500
mg/L
10.0
378
449
75-125
QM-07
Zinc
0.229
0.0100
mg/L
0.200
0.0223
103
75-125
Matrix Spike Dup (0003027-MSD1)
Prepared:
03/03/2020
09:51 Analyzed: 03/05/2020 10:19
Source: CD03782-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Aluminum
20.4
0.100
mg/L
2.00
17.2
161
75-125
4
20 QM-07
Arsenic
0.181
0.0100
mg/L
0.200
0.00760 U
90
75-125
0.04
20
Cadmium
0.0185
0.00100
mg/L
0.0200
0.000360 U
92
75-125
4
20
Calcium
2.47
0.100
mg/L
2.00
0.569
95
75-125
1
20
Copper
0.210
0.0100
mg/L
0.200
0.0151
97
75-125
1
20
Lead
0.174
0.0100
mg/L
0.200
0.00310 U
87
75-125
1
20
Magnesium
2.17
0.100
mg/L
2.00
0.169
100
75-125
3
20
Molybdenum
0.210
0.0100
mg/L
0.200
0.0169
96
75-125
3
20
Nickel
0.188
0.0100
mg/L
0.200
0.00284
93
75-125
3
20
Potassium
34.8
0.500
mg/L
10.0
22.6
122
75-125
3
20
Selenium
0.212
0.0100
mg/L
0.200
0.00620 U
106
75-125
4
20
Sodium
439
0.500
mg/L
10.0
378
609
75-125
4
20 QM-07
Zinc
0.236
0.0100
mg/L
0.200
0.0223
107
75-125
3
20
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 13

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch OCO3O27 - EPA 3OO5A - Continued
Post Spike (0003027-PS1)
Prepared: 03/03/2020 09:51 Analyzed: 03/05/2020 10:22
Source: CD03782-01
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD Limit
Notes
Aluminum
19.9
0.100
mg/L
2.00
17.2
139
80-120
QM-08
Arsenic
0.194
0.0100
mg/L
0.200
-0.00253
97
80-120
Cadmium
0.0186
0.00100
mg/L
0.0200
-0.000344
93
80-120
Calcium
2.55
0.100
mg/L
2.00
0.569
99
80-120
Copper
0.219
0.0100
mg/L
0.200
0.0151
102
80-120
Lead
0.186
0.0100
mg/L
0.200
-0.000306
93
80-120
Magnesium
2.27
0.100
mg/L
2.00
0.169
105
80-120
Molybdenum
0.219
0.0100
mg/L
0.200
0.0169
101
80-120
Nickel
0.192
0.0100
mg/L
0.200
0.00284
95
80-120
Potassium
34.7
0.500
mg/L
10.0
22.6
122
80-120
QM-08
Selenium
0.223
0.0100
mg/L
0.200
0.00530
109
80-120
Sodium
424
0.500
mg/L
10.0
378
459
80-120
QM-08
Zinc
0.239
0.0100
mg/L
0.200
0.0223
108
80-120
Classical Chemistry Parameters - Quality Control
Batch OCO3O27 - EPA 3OO5A
Blank (0003027-BLK3) Prepared: 03/03/2020 09:51 Analyzed: 03/05/2020 15:21
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Sodium Adsorption Ratio 0.00 U [blank]
Batch OCO3O28 - NO PREP
Blank (0003028-BLK3) Prepared & Analyzed: 03/03/2020 14:18
Spike Source %REC RPD
Analvte Result Flaa POL Units Level Result %REC Limits RPD Limit Notes
Biochemical Oxygen Demand 2.0 u 2.0 mg/L
LCS (0003028-BSI) Prepared & Analyzed: 03/03/2020 14:18
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Biochemical Oxygen Demand
180
2.0
mg/L
198
89 85-115
Duplicate (0003028-DUPI)
Prepared & Analyzed: 03/03/2020 14:18
Source: CC14637-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Biochemical Oxygen Demand
2.9
2.0
mg/L
3.5
19
30
Batch OCO3O38 - NO PREP
Blank (0003038-BLK3) Prepared: 03/03/2020 14:30 Analyzed: 03/03/2020 16:30
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Nitrite as N 0.017 u 0.10 mg/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OCO3O38 - NO PREP - Continued
LCS (0003038-BS1) Prepared: 03/03/2020 14:30 Analyzed: 03/03/2020 16:21
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
0.97
0.10
mg/L
1.00 97 90-110
Matrix Spike (0003038-MS1)
Prepared: 03/03/2020 14:30 Analyzed: 03/03/2020 16:32
Source: CD01610-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
1.8
0.10
mg/L
1.00 0.69 108 90-110
Matrix Spike (0003038-MS2)
Prepared: 03/03/2020 14:30 Analyzed: 03/03/2020 16:45
Source: CD03416-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
1.0
0.10
mg/L
1.00 0.017 U 105 90-110
Matrix Spike Dup (0003038-MSD3)
Prepared: 03/03/2020 14:30 Analyzed: 03/03/2020 16:33
Source: CD01610-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
1.8
0.10
mg/L
1.00 0.69 108 90-110 0.1
10
Batch OCO4O17 - Same
Blank (0004017-BLK3) Prepared: 03/04/2020 10:41 Analyzed: 03/12/2020 11:38
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Kjeldahl Nitrogen 0.26 U 0.48 mg/L
LCS (0004017-BSI) Prepared: 03/04/2020 10:41 Analyzed: 03/12/2020 11:40
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
13
0.48
mg/L
12.0
110
90-110
Matrix Spike (0004017-MSS)
Prepared: 03/04/2020 10:41 Analyzed: 03/12/2020 11:43
Source: CD00121-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
27
D
0.96
mg/L
4.80
22
108
90-110
Matrix Spike Dup (0004017-MSD3)
Prepared: 03/04/2020 10:41 Analyzed: 03/12/2020 11:45
Source: CD00121-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
28
D
0.96
mg/L
4.80
22
130
90-110 4
10
QM-07
Batch OCO4O18 - Same
Blank (0004018-BLK3) Prepared: 03/04/2020 10:41 Analyzed: 03/12/2020 16:31
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Phosphorus 0.036 3 0.10 mg/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 0004018 - Same - Continued
LCS (0004018-BS1) Prepared: 03/04/2020 10:41 Analyzed: 03/12/2020 13:54
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit
Notes
Phosphorus
1.5
0.10
mg/L
1.60 96 80-120
Matrix Spike (0004018-MS1)
Prepared: 03/04/2020 10:41 Analyzed: 03/12/2020 17:10
Source: CD02640-02RE1
Spike Source O/oREC
RPD
Analvte
Result
Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit
Notes
Phosphorus
4.3
D
0.50
mg/L
0.640 3.7 83 80-120
Matrix Spike Dup (0004018-MSD1)
Prepared: 03/04/2020 10:41 Analyzed: 03/12/2020 17:11
Source: CD02640-02RE1
Spike Source O/oREC
RPD
Analvte
Result
Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit
Notes
Phosphorus
16
DE
0.50
mg/L
0.640 3.7 NR 80-120 116
25
QM-07,
QM-11
Batch 0005004 - NO PREP
Blank (0005004-BLK3) Prepared: 03/05/2020 12:01 Analyzed: 03/05/2020 13:13
Spike Source O/oREC RPD
Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes
Total Suspended Solids 2.5 U 2.5 mg/L
LCS (0005004-BS3) Prepared: 03/05/2020 12:01 Analyzed: 03/05/2020 13:13
Spike Source O/oREC
RPD
Analvte
Result Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit Notes
Total Suspended Solids
100
2.5
mg/L
100 102 80-120
Duplicate (0005004-DUPi)
Prepared: 03/05/2020 12:01 Analyzed: 03/05/2020 13:13
Source: CC18108-01
Spike Source O/oREC
RPD
Analvte
Result Flaa
Q
Units
Level Result O/oREC Limits RPD
Limit Notes
Total Suspended Solids
200
50
mg/L
200 4
20
Duplicate (0005004-DUP2)
Prepared: 03/05/2020 12:01 Analyzed: 03/05/2020 13:13
Source: CD02113-01
Spike Source O/oREC
RPD
Analvte
Result Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit Notes
Total Suspended Solids
26000
2500
mg/L
25000 3
20
Batch 0006006 - Same
Blank (0006006-BLK3) Prepared: 03/06/2020 09:48 Analyzed: 03/06/2020 15:56
Spike Source O/oREC
RPD
Analvte
Result Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit Notes
Chemical Oxygen Demand
10 U
10
mg/L
LCS (0006006-BS3)
Prepared: 03/06/2020 09:48 Analyzed: 03/06/2020 15:56
Spike Source O/oREC
RPD
Analvte
Result Flaa
Q
Units
Level Result O/oREC Limits RPD
Limit Notes
Chemical Oxygen Demand
500
10
mg/L
500 100 90-110
FINAL
This report relates only to the sample as received by the
laboratory, and may only be reproduced in full.
Page 9 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 0006006 - Same - Continued
Matrix Spike (0006006-MSS)
Prepared: 03/06/2020 09:48 Analyzed: 03/06/2020 15:56
Source: CC11228-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Chemical Oxygen Demand
15000
200
mg/L
10000 4500 101 90-110
Matrix Spike Dup (0006006-MSD3)
Prepared: 03/06/2020 09:48 Analyzed: 03/06/2020 15:56
Source: CC11228-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Chemical Oxygen Demand
14000
200
mg/L
10000 4500 97 90-110 2
5
Batch OC10033 - NO PREP
Blank (OC10033-BLK3) Prepared: 03/10/2020 15:13 Analyzed: 03/10/2020 17:19
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Ammonia as N 0.045 U 0.10 mg/L
LCS (OC10033-BS1) Prepared: 03/10/2020 15:13 Analyzed: 03/10/2020 17:20
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
0.98
0.10
mg/L
1.01 97 90-110
Matrix Spike (OC30033-MS1)
Prepared: 03/10/2020 15:13 Analyzed: 03/10/2020 17:24
Source: CC18108-02
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
0.33
0.10
mg/L
0.393 0.045 U 84 90-110
QM-07
Matrix Spike (OC10033-MS2)
Prepared: 03/10/2020 15:13 Analyzed: 03/10/2020 17:29
Source: CDO1621-02
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
6.5
0.50
mg/L
2.02 4.7 89 90-110
QM-07
Matrix Spike Dup (OC10033-MSD3)
Prepared: 03/10/2020 15:13 Analyzed: 03/10/2020 17:26
Source: CC18108-02
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
0.34
0.10
mg/L
0.393 0.045 U 88 90-110 4
10
QM-07
Batch OC11007 - NO PREP
Blank (OC13007-BLK3) Prepared: 03/11/2020 09:24 Analyzed: 03/11/2020 13:20
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrate/Nitrite as N
0.041 U
0.10
mg/L
LCS (OC33007-BSI)
Prepared: 03/11/2020 09:24 Analyzed: 03/11/2020 13:22
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrate/Nitrite as N
1.3
0.10
mg/L
1.25 101 90-110
FINAL
This report relates only to
the sample as received by the
laboratory, and may only be reproduced in full.
Page 10 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OC11OO7 - NO PREP - Continued
Matrix Spike (OC31007-MSS)
Prepared: 03/11/2020 09:24 Analyzed: 03/11/2020 13:26
Source: CC18108-02
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrate/Nitrite as N
17
1.0
mg/L
5.00 12 99 90-110
Matrix Spike (OC11007-MS2)
Prepared: 03/11/2020 09:24 Analyzed: 03/11/2020 13:31
Source: CD01636-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrate/Nitrite as N
45
5.0
mg/L
25.0 18 108 90-110
Matrix Spike Dup (OC11007-MSD3)
Prepared: 03/11/2020 09:24 Analyzed: 03/11/2020 13:28
Source: CC18108-02
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrate/Nitrite as N
17
1.0
mg/L
5.00 12 102 90-110 0.7
10
Batch ODO6O21 - NO PREP
Blank (OD06021-BLK1) Prepared & Analyzed: 04/06/2020 17:40
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Solids 0.0050 U 0.0050 % by Volume
LCS (OD06021-BS1) Prepared & Analyzed: 04/06/2020 17:40
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Solids
1100
50
mg/L
1100 97 80-120
Duplicate (OD06021-DUP3)
Prepared & Analyzed: 04/06/2020 17:40
Source: C11302113-01RE1
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Solids
3.8
0.0050
% by Volume
4.0 5
20
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 13

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
Q-01 Analysis performed outside of method - specified holding time.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 13

10775 Central Port Dr. 4810 Executive Park Court, Suite 111 102-A Woodwinds Industrial Cl.
Orlando, FL 32824 Jacksonville, FL 32216-6069 Cary, NC 27511
[phone] [phone] Fax [phone] [phone] Fax [phone] Page of
Cheri Name
Navozymes North America N0008
Projecl Number
none
Requested
Analyses
Requested Turnaround
Times
Note :Rush requests subject to
acceplance by the tacility
� Standard
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Address
77 Perry Chapel Church Road
Project NamelDesc
Monthly - Week One - SBM
Ct1y1STf2ip
FrankOnton, NC 27525
PO # ! Billing Into
3800466333
Tel
(918) 4$4-300d
Fax
Reporting Contact
Scott Creech
Sampler(s) Na e, Affiliation (Prinl)
I
1 1/^S
Billing Contact
ACCDUntS Payable
Sign re
Site Location r Time zone
Lab WOrkOfder
Ca02113
Preservation
{See
Codes}
{Combino
as necessary)
Item k
Sample ID (Field ldantitication)
Collection Date
Collection
Time
Comp! Grab
Matrix
(see codes)
Total # of
Containers
Sample Comments
SSM
�3�av
0C; oo
G
SL
6
X
X
X
X
X
X
X
/j
—Total # of Containers
Sample Kit Prepared By
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Relir By ////j/
DateMme
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Received By
Dat�me
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Comments Special Reporting Requirements
e)inq hed Sy
DatelTme
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T,
Dalemme `
3) 3)Z �
Relinquished By
DateMme
Received By
DalerTime
Cooler #'sjj& Te Receipt r,
Condi ' n Upon Receipt
Imp's`�on
1
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Acceptable Unacceptable
Matrix: GW-Groundwater SO -Soil DW-Drinking Water SE -Sediment SW -Surface Water WW-Wastewater A -Air O.Other {detail in comments) Preservation: I -Ice H-HCI N-HNO3 S-H2$04 NO-NaOH O.Other (detaH in comments)
Note : All samples submltled to ENCO Labs are in accordance with the terms and conditions Tinted on the reverse of this form, unless prior written agreements exist

Sample Preservation Verification
ENCO Cary
Work Order; CD02113
Client: Novozymes North America (NO008)
Lagged In: 03-Mar-20 11:04
Preservation Check Performed By
CD02113-01
Project: Monthly - Week One - SBM
Project #; [none]
Logged By: John C King
Date/Time:
Cont
Yp
type
Pres (pH)
Requirement
pH Checked /
In Control
Date l ime
PH Adjusted Adjusted
Reagent Used/Comments
C
250mLP+H2SO4
<2
Y• /�q 1 NA
Y 16 I NA , c) }
z c- Z 4
D
250mLP+HNO3
<2
Y / NA
Y CN)/ NA
A- WAZ3
Rea ent Name ID
1
zsoq Ia.
pH Strip lD: OcAb-nga
Rea ent Name ID
3
4
Rea ent Name ID
5
6
CAELMNTIPrintlwko_PreservationCheck. rpt Page 1

2�SQ pCCgF ENCO Laboratories
9e0
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Tuesday, April 21, 2020
Novozymes North America (N0008)
Attn: Scott Creech
77 Perry Chapel Church Road
Franklinton, NC 27525
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: Monthly - Week One - SBM
ENCO Workorder(s): CD04433
Dear Scott Creech,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, April 7, 2020.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
0"CLC---�0
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 13

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: SBM
Lab ID: CD04433-01
Sampled: 04/07/20 01:20
Received: 04/07/20 11:47
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
CSU Method
NO PREP
01/01/23
04/08/20
10:01
04/09/20
14:40
EPA 350.1
NO PREP
05/05/20
04/13/20
14:54
04/14/20
09:15
EPA 351.2
Same
05/05/20
04/13/20
10:10
04/15/20
18:03
EPA 353.2
NO PREP
04/09/20
01:20
04/07/20
14:25
04/07/20
15:46
EPA 353.2
[CALC]
04/09/20
01:20
04/13/20
13:10
04/13/20
16:05
EPA 353.2
NO PREP
05/05/20
04/13/20
13:10
04/13/20
16:05
EPA 365.4
Same
05/05/20
04/13/20
10:10
04/17/20
14:03
EPA 6010D
EPA 3005A
10/04/20
04/08/20
10:01
04/09/20
13:13
EPA 7470A
EPA 7470A
05/05/20
04/09/20
11:18
04/10/20
16:42
SM 254OB-2011
NO PREP
04/14/20
04/13/20
09:07
04/13/20
09:07
SM 2540D-2011
NO PREP
04/14/20
04/13/20
11:17
04/13/20
11:17
SM 5210 B-2011
NO PREP
04/09/20
01:20
04/08/20
09:55
04/08/20
09:55
SM 5220D-2011
Same
05/05/20
04/10/20
11:11
04/10/20
16:35
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 13

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SAMPLE DETECTION SUMMARY
Client ID: SBM
Lab ID: CD04433-01
Analvte
Results
Flag
MDL
PQL
Units
Method Notes
Aluminum - Total
5.39
0.420
1.00
mg/L
EPA 6010D
Ammonia as N
210
D
9.0
20
mg/L
EPA 350.1
Biochemical Oxygen Demand
12000
2.0
2.0
mg/L
SM 5210 B-2011
Calcium - Total
2110
0.390
1.00
mg/L
EPA 6010D
Chemical Oxygen Demand
32000
800
800
mg/L
SM 5220D-2011
Copper - Total
0.166
0.0160
0.100
mg/L
EPA 6010D
Magnesium - Total
30.4
0.290
1.00
mg/L
EPA 6010D
Molybdenum - Total
0.0405
1
0.0250
0.100
mg/L
EPA 6010D
Nickel - Total
0.0594
3
0.0220
0.100
mg/L
EPA 6010D
Nitrate as N
18
D
2.0
4.8
mg/L
EPA 353.2
Nitrate/Nitrite as N
18
D
2.0
4.8
mg/L
EPA 353.2
Nitrite as N
0.63
0.017
0.10
mg/L
EPA 353.2
Phosphorus
680
D
25
100
mg/L
EPA 365.4
Potassium - Total
1000
1.50
5.00
mg/L
EPA 6010D
Sodium - Total
509
4.00
5.00
mg/L
EPA 6010D
Sodium Adsorption Ratio
3.01
[blank]
CSU Method
Total Kjeldahl Nitrogen
2300
D
26
48
mg/L
EPA 351.2
Total Solids
5.2
0.083
0.083
% by Volume
SM 254OB-2011
Total Suspended Solids
31000
2500
2500
mg/L
SM 2540D-2011
Zinc - Total
0.258
0.0440
0.100
mg/L
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 13

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ANALYTICAL RESULTS
Description: SBM Lab Sample ID:CD04433-01 Received: 04/07/20 11:47
Matrix: Sludge Sampled: 04/07/20 01:20 Work Order: CD04433
Project: Monthly - Week One - SBM Sampled By: ELbert Alston
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay Notes
Mercury [7439-97-6]^
0.00150
U
mg/L
10
0.00150
0.00200
OD09030
EPA 7470A
04/10/20 16:42
KAH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Ay Notes
Aluminum [7429-90-5]^
5.39
mg/L
10
0.420
1.00
OD08028
EPA 6010D
04/09/20 13:13
JDH
Arsenic [7440-38-2]^
0.0760
U
mg/L
10
0.0760
0.100
OD08028
EPA 6010D
04/09/20 13:13
JDH
Cadmium [7440-43-9]^
0.00360
U
mg/L
10
0.00360
0.0100
OD08028
EPA 6010D
04/09/20 13:13
JDH
Calcium [7440-70-2]^
2110
mg/L
10
0.390
1.00
OD08028
EPA 6010D
04/09/20 13:13
JDH
Copper[7440-50-8]^
0.166
mg/L
10
0.0160
0.100
OD08028
EPA 6010D
04/09/20 13:13
JDH
Lead [7439-92-1]^
0.0310
U
mg/L
10
0.0310
0.100
OD08028
EPA 6010D
04/09/20 13:13
JDH
Magnesium [7439-95-4]^
30.4
mg/L
10
0.290
1.00
OD08028
EPA 6010D
04/09/20 13:13
JDH
Molybdenum [7439-98-7]^
0.0405
J
mg/L
10
0.0250
0.100
OD08028
EPA 6010D
04/09/20 13:13
JDH
Nickel[7440-02-O]^
0.0594
J
mg/L
10
0.0220
0.100
OD08028
EPA 6010D
04/09/20 13:13
JDH
Potassium [7440-09-7]^
1000
mg/L
10
1.50
5.00
OD08028
EPA 6010D
04/09/20 13:13
JDH
Selenium [7782-49-2]^
0.0620
U
mg/L
10
0.0620
0.100
OD08028
EPA 6010D
04/09/20 13:13
JDH
Sodium [7440-23-5]^
509
mg/L
10
4.00
5.00
OD08028
EPA 6010D
04/09/20 13:13
JDH
Zinc[7440-66-6]^
0.258
mg/L
10
0.0440
0.100
OD08028
EPA 6010D
04/09/20 13:13
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Ay Notes
Ammonia as N [7664-41-7]^
210
D
mg/L
200
9.0
20
OD13041
EPA 350.1
04/14/20 09:15
JAH
Biochemical Oxygen Demand^
12000
mg/L
1
2.0
2.0
OD08007
SM 5210 B-2011
04/08/20 09:55
JOC
Chemical Oxygen Demand^
32000
mg/L
80
800
800
OD10008
SM 5220D-2011
04/10/20 16:35
JOC
Nitrate as N [14797-55-8]
18
D
mg/L
48
2.0
4.8
[CALC]
EPA 353.2
04/13/20 16:05
JAH
Nitrate/Nitrite as N^
18
D
mg/L
48
2.0
4.8
OD13039
EPA 353.2
04/13/20 16:05
JAH
Nitrite as N [14797-65-0]^
0.63
mg/L
1
0.017
0.10
OD07028
EPA 353.2
04/07/20 15:46
JAH
Phosphorus[7723-14-O]^
680
D
mg/L
1000
25
100
OD13004
EPA 365.4
04/17/20 14:03
JAH
Sodium Adsorption Ratio
3.01
[blank]
1
OD08028
CSU Method
04/09/20 14:40
JDH
Total Kjeldahl Nitrogen^
2300
D
mg/L
100
26
48
OD13005
EPA 351.2
04/15/20 18:03
JAH
Total Solids^
5.2
% by Volume
16.7
0.083
0.083
OD13014
SM 2540B-2011
04/13/20 09:07
JOC
Total Suspended Solids^
31000
mg/L
1000
2500
2500
OD13026
SM 2540D-2011
04/13/20 11:17
UI
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 13

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch ODO9O3O - EPA 747OA
Blank (OD09030-BLK1) Prepared: 04/09/2020 11:18 Analyzed: 04/10/2020 16:04
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Mercury 0.000150 U 0.000200 mg/L
LCS (OD09030-BS1) Prepared: 04/09/2020 11:18 Analyzed: 04/10/2020 16:07
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00506
0.000200
mg/L
0.00500
101
80-120
Matrix Spike (OD09030-MS3)
Prepared: 04/09/2020 11:18 Analyzed: 04/10/2020 16:11
Source: CD05167-02
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00507
0.000200
mg/L
0.00500
0.000150 U
101
75-125
Matrix Spike Dup (01309030-MS131)
Prepared: 04/09/2020 11:18 Analyzed: 04/10/2020 16:13
Source: CDO5167-02
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00480
0.000200
mg/L
0.00500
0.000150 U
96
75-125 6
25
Post Spike (OD09030-PS3)
Prepared: 04/09/2020 11:18 Analyzed: 04/10/2020 16:16
Source: CD05167-02
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
5.36
0.200
ug/L
5.00
-0.0330
107
75-125
Metals (total recoverable) by EPA 6000/7000
Series Methods - Quality Control
Batch ODO8O28 - EPA 3OO5A
Blank (OD08028-BLK3)
Prepared: 04/08/2020 10:01 Analyzed: 04/09/2020 11:17
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Aluminum
0.0420
U
0.100
mg/L
Arsenic
0.00760
U
0.0100
mg/L
Cadmium
0.000360
U
0.00100
mg/L
Calcium
0.0390
U
0.100
mg/L
Copper
0.00160
U
0.0100
mg/L
Lead
0.00310
U
0.0100
mg/L
Magnesium
0.0290
U
0.100
mg/L
Molybdenum
0.00250
U
0.0100
mg/L
Nickel
0.00220
U
0.0100
mg/L
Potassium
0.150
U
0.500
mg/L
Selenium
0.00620
U
0.0100
mg/L
Sodium
0.400
U
0.500
mg/L
Zinc
0.00440
U
0.0100
mg/L
LCS (OD08028-BSI)
Prepared: 04/08/2020 10:01 Analyzed: 04/09/2020 11:23
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Aluminum 1.99 0.100 mg/L 2.00 99 80-120
Arsenic 0.204 0.0100 mg/L 0.200 102 80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 13

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch ODO8O2B - EPA 3OO5A - Continued
LCS (OD08028-BSI) Continued Prepared: 04/08/2020 10:01 Analyzed: 04/09/2020 11:23
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Cadmium
0.0199
0.00100
mg/L
0.0200
100
80-120
Calcium
2.13
0.100
mg/L
2.00
107
80-120
Copper
0.188
0.0100
mg/L
0.200
94
80-120
Lead
0.201
0.0100
mg/L
0.200
101
80-120
Magnesium
1.99
0.100
mg/L
2.00
100
80-120
Molybdenum
0.194
0.0100
mg/L
0.200
97
80-120
Nickel
0.203
0.0100
mg/L
0.200
102
80-120
Potassium
9.71
0.500
mg/L
10.0
97
80-120
Selenium
0.212
0.0100
mg/L
0.200
106
80-120
Sodium
9.51
0.500
mg/L
10.0
95
80-120
Zinc
0.208
0.0100
mg/L
0.200
104
80-120
Matrix Spike (OD08028-MS1)
Prepared:
04/08/2020
10:01 Analyzed: 04/09/2020 11:26
Source: CD05436-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Aluminum
2.19
0.100
mg/L
2.00
0.196
99
75-125
Arsenic
0.200
0.0100
mg/L
0.200
0.00760 U
100
75-125
Cadmium
0.0200
0.00100
mg/L
0.0200
0.000360 U
100
75-125
Calcium
21.0
0.100
mg/L
2.00
19.3
85
75-125
Copper
0.192
0.0100
mg/L
0.200
0.00293
94
75-125
Lead
0.201
0.0100
mg/L
0.200
0.00310 U
100
75-125
Magnesium
7.39
0.100
mg/L
2.00
5.58
91
75-125
Molybdenum
0.195
0.0100
mg/L
0.200
0.00250 U
98
75-125
Nickel
0.201
0.0100
mg/L
0.200
0.00220 U
101
75-125
Potassium
10.5
0.500
mg/L
10.0
0.655
99
75-125
Selenium
0.204
0.0100
mg/L
0.200
0.00620 U
102
75-125
Sodium
16.1
0.500
mg/L
10.0
6.34
97
75-125
Zinc
0.211
0.0100
mg/L
0.200
0.00502
103
75-125
Matrix Spike Dup (OD08028-MSDS)
Prepared:
04/08/2020
10:01 Analyzed: 04/09/2020 11:28
Source: CD05436-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Aluminum
2.17
0.100
mg/L
2.00
0.196
99
75-125
0.8
20
Arsenic
0.195
0.0100
mg/L
0.200
0.00760 U
97
75-125
3
20
Cadmium
0.0203
0.00100
mg/L
0.0200
0.000360 U
102
75-125
2
20
Calcium
21.3
0.100
mg/L
2.00
19.3
102
75-125
2
20
Copper
0.193
0.0100
mg/L
0.200
0.00293
95
75-125
0.7
20
Lead
0.202
0.0100
mg/L
0.200
0.00310 U
101
75-125
0.9
20
Magnesium
7.43
0.100
mg/L
2.00
5.58
93
75-125
0.5
20
Molybdenum
0.198
0.0100
mg/L
0.200
0.00250 U
99
75-125
1
20
Nickel
0.204
0.0100
mg/L
0.200
0.00220 U
102
75-125
1
20
Potassium
10.5
0.500
mg/L
10.0
0.655
98
75-125
0.4
20
Selenium
0.211
0.0100
mg/L
0.200
0.00620 U
106
75-125
3
20
Sodium
16.4
0.500
mg/L
10.0
6.34
100
75-125
2
20
Zinc
0.214
0.0100
mg/L
0.200
0.00502
104
75-125
1
20
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 13

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch OD08028 - EPA 3005A - Continued
Post Spike (OD08028-PS3)
Prepared: 04/08/2020 10:01 Analyzed: 04/09/2020 11:30
Source: CDO5436-01
Spike
Source
O/oREC RPD
Analvte
Result Flaq
POL
Units
Level
Result
O/oREC
Limits RPD Limit Notes
Aluminum
2.17
0.100
mg/L
2.00
0.196
98
80-120
Arsenic
0.196
0.0100
mg/L
0.200
-0.000552
98
80-120
Cadmium
0.0201
0.00100
mg/L
0.0200
-0.000207
101
80-120
Calcium
21.1
0.100
mg/L
2.00
19.3
93
80-120
Copper
0.196
0.0100
mg/L
0.200
0.00293
97
80-120
Lead
0.204
0.0100
mg/L
0.200
0.000713
102
80-120
Magnesium
7.28
0.100
mg/L
2.00
5.58
85
80-120
Molybdenum
0.198
0.0100
mg/L
0.200
-0.000996
99
80-120
Nickel
0.204
0.0100
mg/L
0.200
0.000864
102
80-120
Potassium
10.6
0.500
mg/L
10.0
0.655
100
80-120
Selenium
0.208
0.0100
mg/L
0.200
-0.00124
104
80-120
Sodium
16.1
0.500
mg/L
10.0
6.34
98
80-120
Zinc
0.215
0.0100
mg/L
0.200
0.00502
105
80-120
Classical Chemistry Parameters - Quality Control
Batch OD07028 - NO PREP
Blank (OD07028-BLK1) Prepared: 04/07/2020 14:25 Analyzed: 04/07/2020 15:40
Spike Source O/oREC RPD
Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes
Nitrite as N 0.017 U 0.10 mg/L
LCS (OD07028-BS1) Prepared: 04/07/2020 14:25 Analyzed: 04/07/2020 15:14
Spike Source O/oREC
RPD
Analvte
Result Flaa
POL
Units
Level Result O/oREC Limits RPD
Limit Notes
Nitrite as N
1.0
0.10
mg/L
1.00 104 90-110
Matrix Spike (OD07028-MS3)
Prepared: 04/07/2020 14:25 Analyzed: 04/07/2020 15:42
Source: CD04432-01
Spike Source O/oREC
RPD
Analvte
Result Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit Notes
Nitrite as N
1.2
0.10
mg/L
1.00 0.18 103 90-110
Matrix Spike Dup (OD07028-MSD1)
Prepared: 04/07/2020 14:25 Analyzed: 04/07/2020 15:43
Source: CD04432-01
Spike Source O/oREC
RPD
Analvte
Result Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit Notes
Nitrite as N
1.3
0.10
mg/L
1.00 0.18 109 90-110 5
10
Batch OD08007 - NO PREP
Blank (OD08007-BLK3)
Prepared & Analyzed: 04/08/2020 09:55
Spike Source O/oREC
RPD
Analvte
Result Flaq POL Units Level Result O/oREC Limits RPD
Limit Notes
Biochemical Oxygen Demand
2.0 U 2.0 mg/L
LCS (OD08007-BSI)
Prepared & Analyzed: 04/08/2020 09:55
Spike Source O/oREC
RPD
Analvte
Result Flaq POL Units Level Result O/oREC Limits RPD
Limit Notes
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 7 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch ODOBOO7 - NO PREP - Continued
LCS (OD08007-BSI) Continued Prepared & Analyzed: 04/08/2020 09:55
Analvte
Biochemical Oxygen Demand
Result Flaq
210
POL
2.0
Units
mg/L
Spike
Level
198
Source
Result
%REC
%REC Limits RPD
104 85-115
RPD
Limit Notes
Duplicate (OD08007-DUPl)
Prepared & Analyzed: 04/08/2020 09:55
Source: CD00269-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Biochemical Oxygen Demand
2.0 U
2.0
mg/L
2.0 U
30
Batch ODO8O28 - EPA 3OO5A
Blank (OD08028-BLK3) Prepared: 04/08/2020 10:01 Analyzed: 04/09/2020 14:41
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Sodium Adsorption Ratio 0.00 U [blank]
Batch ODIOOOB - Same
Blank (OD30008-BLK1) Prepared: 04/10/2020 11:11 Analyzed: 04/10/2020 16:35
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Chemical Oxygen Demand 10 U 10 mg/L
LCS (OD10008-BS1) Prepared: 04/10/2020 11:11 Analyzed: 04/10/2020 16:35
Spike
Source
%REC
RPD
Analvte
Result Flaa
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Chemical Oxygen Demand
490
10
mg/L
500
99
90-110
Matrix Spike (0D10008-MS3)
Prepared: 04/10/2020 11:11 Analyzed: 04/10/2020 16:35
Source: CC19100-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Chemical Oxygen Demand
530
10
mg/L
526
10 U
101
90-110
Matrix Spike Dup (OD10008-MSDS)
Prepared: 04/10/2020 11:11 Analyzed: 04/10/2020 16:35
Source: CC19100-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Chemical Oxygen Demand
530
10
mg/L
526
10 U
100
90-110 1
5
Batch OD13OO4 - Same
Blank (OD33004-BLK3) Prepared: 04/13/2020 10:10 Analyzed: 04/17/2020 13:43
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Phosphorus
0.025 U
0.10
mg/L
LCS (OD13004-BSI)
Prepared: 04/13/2020 10:10 Analyzed: 04/17/2020 13:44
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Phosphorus
1.6
0.10
mg/L
1.60 100 80-120
FINAL
This report relates only to
the sample as received by the
laboratory, and may only be reproduced in full.
Page 8 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OD13OO4 - Same - Continued
Matrix Spike (OD13004-MS3)
Prepared: 04/13/2020 10:10 Analyzed: 04/17/2020 13:47
Source: CD03334-02
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Phosphorus
0.84
0.10
mg/L
0.640 0.19 102 80-120
Matrix Spike Dup (O1313004-MS131)
Prepared: 04/13/2020 10:10 Analyzed: 04/17/2020 13:48
Source: CD03334-02
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Phosphorus
0.80
0.10
mg/L
0.640 0.19 95 80-120 5
25
Batch OD13OO5 - Same
Blank (OD33005-BLK3) Prepared: 04/13/2020 10:10 Analyzed: 04/15/2020 17:51
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Kjeldahl Nitrogen 0.26 U 0.48 mg/L
LCS (OD13005-BSI) Prepared: 04/13/2020 10:10 Analyzed: 04/15/2020 17:53
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
13
0.48
mg/L
12.0 105 90-110
Matrix Spike (OD13005-MS3)
Prepared: 04/13/2020 10:10 Analyzed: 04/15/2020 17:56
Source: CD03334-02
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
6.0
0.48
mg/L
4.80 0.80 108 90-110
Matrix Spike (OD13005-MS2)
Prepared: 04/13/2020 10:10 Analyzed: 04/15/2020 18:26
Source: CD04764-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
31
E
0.48
mg/L
4.80 16 314 90-110
QM-02
Matrix Spike Dup (OD13005-MSDS)
Prepared: 04/13/2020 10:10 Analyzed: 04/15/2020 17:58
Source: CD03334-02
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
6.0
0.48
mg/L
4.80 0.80 109 90-110 0.9
10
Batch OD13O14 - NO PREP
Blank (OD33014-BLK3) Prepared & Analyzed: 04/13/2020 09:07
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Solids
0.0050
U 0.0050
% by Volume
LCS (OD13014-BSI)
Prepared & Analyzed: 04/13/2020 09:07
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Solids
1100
50
mg/L
1100 97 80-120
FINAL
This report relates only to the sample
as received by the
laboratory, and may only be reproduced in full.
Page 9 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OD13O14 - NO PREP - Continued
Duplicate (OD13014-DUPl) Prepared & Analyzed: 04/13/2020 09:07
Source: CD03768-01
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Solids 0.34 0.0050 % by Volume 0.34 2 20
Batch OD13O26 - NO PREP
Blank (OD33026-BLK3) Prepared & Analyzed: 04/13/2020 11:17
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Suspended Solids
2.5
U
2.5
mg/L
LCS (OD13026-BSI)
Prepared & Analyzed: 04/13/2020 11:17
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Suspended Solids
100
2.5
mg/L
100 101 80-120
Duplicate (OD13026-DUPl)
Prepared & Analyzed: 04/13/2020 11:17
Source: CD04474-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Suspended Solids
21
5.6
mg/L
44 73
20
QM-12
Duplicate (OD33026-DUP2)
Prepared & Analyzed: 04/13/2020 11:17
Source: CD03334-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Suspended Solids
150
28
mg/L
170 10
20
Batch OD13O39 - NO PREP
Blank (OD33039-BLK3)
Prepared: 04/13/2020 13:10 Analyzed: 04/13/2020 15:49
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
0.041
U
0.10
mg/L
LCS (OD13039-BSI)
Prepared: 04/13/2020 13:10 Analyzed: 04/13/2020 15:50
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
1.4
0.10
mg/L
1.25 109 90-110
Matrix Spike (OD13039-MS3)
Prepared: 04/13/2020 13:10 Analyzed: 04/13/2020 15:54
Source: CD04432-02
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
8.2
1.0
mg/L
5.00 2.7 110 90-110
Matrix Spike (OD13039-MS2)
Prepared: 04/13/2020 13:10 Analyzed: 04/13/2020 16:03
Source: CDOS001-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
7.3
0.50
mg/L
2.50 4.7 104 90-110
FINAL
This report relates only to
the sample as received by the
laboratory, and may only be reproduced in full.
Page 10 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OD13O39 - NO PREP - Continued
Matrix Spike Dup (OD13039-MSDI) Prepared: 04/13/2020 13:10 Analyzed: 04/13/2020 16:00
Source: CD04432-02
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Nitrate/Nitrite as N 7.9 1.0 mg/L 5.00 2.7 105 90-110 3 10
Batch OD13O41 - NO PREP
Blank (OD33041-BLK3) Prepared: 04/13/2020 14:54 Analyzed: 04/13/2020 18:13
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Ammonia as N 0.045 u 0.10 mg/L
LCS (OD13041-BSI) Prepared: 04/13/2020 14:54 Analyzed: 04/13/2020 18:15
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
1.0
0.10
mg/L
1.01 102 90-110
Matrix Spike (OD13041-MS3)
Prepared: 04/13/2020 14:54 Analyzed: 04/13/2020 18:18
Source: CD04297-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
1.4
0.10
mg/L
0.393 0.99 97 90-110
Matrix Spike (OD13041-MS2)
Prepared: 04/13/2020 14:54 Analyzed: 04/14/2020 09:02
Source: CD04297-02
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
0.46
0.10
mg/L
0.393 0.071 99 90-110
Matrix Spike Dup (OD13041-MSD1)
Prepared: 04/13/2020 14:54 Analyzed: 04/13/2020 18:20
Source: CD04297-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
1.4
0.10
mg/L
0.393 0.99 98 90-110 0.4
10
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 13

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QM-02 The RPD and/or percent recovery for this QC spike sample cannot be accurately calculated due to the high
concentration of analyte present in the sample.
QM-12 Precision between duplicate samples was outside acceptance limits.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 13

- 10775 Cenral Purr Dr. 4810 Executive Park Court, Suite li 1 102-A Woodwinds Industrial Ct.
LeEOrlando, FL 32824 Jacksonville, FL 32216.6069 Cary, NC 27519�1
[phone] [phone] Fax [phone] [phone] Fax [phone] Page of
Client Name
Nattrozyrnes North America (NO008)
Project Number
[none]
Requested
Analyses
Requested Turnaround
Times
Note : Rush requests subject to
acceptance by the facility
Standard
_Expedited
Due
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Address
77 Perry Chapel Church Road
Project NamefDesc
Monthly - Week One - SBM
C":ty/sTlrp
Franklinton, NC 27525
PO # 1 Billing Into
3800466333
Tel
[phone]
Fax
Reporting Contact
Scott Creech
Sampler(s) Name, Affiliation (Pri
�� L'�L}
{
lS
Bill! Contact
Accounts Payable
Samplers) Signa a
Site Location I - -rime Zone
Lab Workorder
CD04433
Preservation
(See
Codes)
(Combine
as necessary)
Item n
Sample ID (Field Identification)
Collection Date
Collection
Time
Complorah
Matrix
(sae codes)
Total # of
Containers
Sample Comments
SBM
'i-7-ZO
OUD
6PWb
SL
a
X
X
X
X
X
X
X
< Total # of Containers
Sample Kit Prepared By
Dalqfrime
�f Y -:111Ol�
R i hed y
T-
Datarnme
Cl
R i By
/
Datelfime
'
CammentslSpecial Reporting Requirements
Relinquished By
Datarnme
Rao d 8
Dat im �'
Relinquished By
Date/rime
Received By
Da lT e
Cooler p's & Temps on Receipt
Condition on Receipt
�� - i
Acceptable Unacceptable
Matrix GW-Groundwater SO -Soil DW-Drinking Water SE -Sediment SW -Surface Water WW-Wastewater A -Air O-Other (detail in comments) Preservation: I -Ica H-HCI N-HNO3 5-H2SO4 NO-NaOH O.Other (detail in comments)
Note: All samples submitted to ENCO Labs are in accordance with the terms and conditions listed on the reverse of this form, unless prior written agreements exist

Sample Preservation Verification
ENCD Cary
Work Order: CD04433 Project: Monthly - Week One - SBM
Client: Novozymes North America (N0008) Project #: [none]
Lagged In: 07-Apr-20 11:57 Logged By: John C King
Preservation Check Performed By: \7 DatelTime: `T " �� �2
CD04433-01
Cont:Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted DaterTime .
Adjusted
Reagent Used/Comments
C
250mLP+H2SO4
<2
Y 1 0 NA
Y./ N / NA C(.-79G I-ZCO
D
250mLP+HNO3
<2
Y / N NA
Y l ! NA
Rea ent Name ID
1 V ! ,
2 �7 �J
pH Strip ID:
1-
Rea ent Name ID
3
4
Reagent Name ID
5
6
C:\ELMNTIPrintlwko PreservationCheck.rpt Page 1

2�SQ pCCgF ENCO Laboratories
9e0
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Wednesday, June 10, 2020
Novozymes North America (N0008)
Attn: Scott Creech
77 Perry Chapel Church Road
Franklinton, NC 27525
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: Monthly - Week One - SBM
ENCO Workorder(s): CD08740
Dear Scott Creech,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Monday, June 1, 2020.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
0"6LC'=-:;tA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 13

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: SBM
Lab ID: CD08740-01
Sampled: 05/31/20 07:00
Received: 06/01/20 09:54
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
CSU Method
NO PREP
02/24/23
06/02/20 11:00
06/09/20 13:48
EPA 350.1
NO PREP
06/28/20
06/04/20 12:01
06/04/20 14:43
EPA 351.2
Same
06/28/20
06/02/20 08:00
06/04/20 11:03
EPA 353.2
NO PREP
06/02/20 07:00
06/01/20 15:44
06/01/20 17:25
EPA 353.2
[CALC]
06/02/20 07:00
06/03/20 09:28
06/03/20 15:11
EPA 365.4
Same
06/28/20
06/02/20 08:00
06/04/20 12:38
EPA 6010D
EPA 3005A
11/27/20
06/02/20 11:00
06/09/20 13:15
EPA 7470A
EPA 7470A
06/28/20
06/02/20 13:26
06/03/20 15:34
SM 2540B-2011
NO PREP
06/07/20
06/05/20 16:50
06/05/20 16:50
SM 254OD-2011
NO PREP
06/07/20
06/05/20 12:10
06/05/20 14:30
SM 5210 B-2011
NO PREP
06/02/20 07:00
06/01/20 15:54
06/01/20 15:54
SM 5220D-2011
Same
06/28/20
06/05/20 09:08
06/05/20 16:22
Client ID: SBM
Lab ID: CD08740-OIRE1
Sampled: 05/31/20 07:00
Received: 06/01/20 09:54
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 353.2
NO PREP
06/28/20
06/03/20 09:28
06/03/20 15:11
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 13

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SAMPLE DETECTION SUMMARY
Client ID: SBM
Lab ID:
CDO8740-01
Analvte
Results
Flag
MDL
Q
Units
Method Notes
Aluminum - Total
19.7
0.420
1.00
mg/L
EPA 6010D
Ammonia as N
150
D
4.0
9.0
mg/L
EPA 350.1
Biochemical Oxygen Demand
12000
2.0
2.0
mg/L
SM 5210 B-2011
Calcium - Total
1960
0.390
1.00
mg/L
EPA 6010D
Chemical Oxygen Demand
31000
800
800
mg/L
SM 5220D-2011
Copper - Total
0.0478
3
0.0160
0.100
mg/L
EPA 6010D
Magnesium - Total
4.61
0.290
1.00
mg/L
EPA 6010D
Nickel - Total
0.0239
3
0.0220
0.100
mg/L
EPA 6010D
Nitrate as N
2.8
D
0.20
0.50
mg/L
EPA 353.2
Nitrite as N
0.24
0.017
0.10
mg/L
EPA 353.2
Phosphorus
660
D
12
50
mg/L
EPA 365.4
Potassium - Total
323
1.50
5.00
mg/L
EPA 6010D
Sodium - Total
202
4.00
5.00
mg/L
EPA 6010D
Sodium Adsorption Ratio
1.25
[blank]
CSU Method
Total Kjeldahl Nitrogen
1800
D
26
48
mg/L
EPA 351.2
Total Solids
4.7
0.0050
0.0050
% by Volume
SM 254OB-2011
Total Suspended Solids
29000
250
250
mg/L
SM 2540D-2011
Zinc - Total
0.0953
3
0.0440
0.100
mg/L
EPA 6010D
Client ID: SBM
Lab ID:
CDO8740-01RE3
Analvte
Results
Flag
MDL
PQL
Units
Method Notes
Nitrate/Nitrite as N
3.1
D
0.20
0.50
mg/L
EPA 353.2
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 13

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ANALYTICAL RESULTS
Description: SBM Lab Sample ID:CD08740-01 Received: 06/01/20 09:54
Matrix: Sludge Sampled:05/31/20 07:00 Work Order: CD08740
Project: Monthly - Week One - SBM Sampled By: adam Fauccette
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay Notes
Mercury [7439-97-6]^
0.000750
U
mg/L
5
0.000750
0.00100
OF02019
EPA 7470A
06/03/20 15:34
KAH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Ay Notes
Aluminum [7429-90-5]^
19.7
mg/L
10
0.420
1.00
OF02013
EPA 6010D
06/09/20 13:15
JDH
Arsenic[7440-38-2]^
0.0760
U
mg/L
10
0.0760
0.100
OF02013
EPA 6010D
06/09/20 13:15
JDH
Cadmium [7440-43-9]^
0.00360
U
mg/L
10
0.00360
0.0100
OF02013
EPA 6010D
06/09/20 13:15
JDH
Calcium [7440-70-2]^
1960
mg/L
10
0.390
1.00
OF02013
EPA 6010D
06/09/20 13:15
JDH
Copper[7440-50-8]^
0.0478
J
mg/L
10
0.0160
0.100
OF02013
EPA 6010D
06/09/20 13:15
JDH
Lead [7439-92-1]^
0.0310
U
mg/L
10
0.0310
0.100
OF02013
EPA 6010D
06/09/20 13:15
JDH
Magnesium [7439-95-4]^
4.61
mg/L
10
0.290
1.00
OF02013
EPA 6010D
06/09/20 13:15
JDH
Molybdenum [7439-98-7]^
0.0250
U
mg/L
10
0.0250
0.100
OF02013
EPA 6010D
06/09/20 13:15
JDH
Nickel[7440-02-O]^
0.0239
J
mg/L
10
0.0220
0.100
OF02013
EPA 6010D
06/09/20 13:15
JDH
Potassium [7440-09-7]^
323
mg/L
10
1.50
5.00
OF02013
EPA 6010D
06/09/20 13:15
JDH
Selenium [7782-49-2]^
0.0620
U
mg/L
10
0.0620
0.100
OF02013
EPA 6010D
06/09/20 13:15
JDH
Sodium [7440-23-5]^
202
mg/L
10
4.00
5.00
OF02013
EPA 6010D
06/09/20 13:15
JDH
Zinc[7440-66-6]^
0.0953
J
mg/L
10
0.0440
0.100
OF02013
EPA 6010D
06/09/20 13:15
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Ay Notes
Ammonia as N [7664-41-7]^
150
D
mg/L
90
4.0
9.0
OF04028
EPA 350.1
06/04/20 14:43
JAH
Biochemical Oxygen Demand^
12000
mg/L
1
2.0
2.0
OF01047
SM 5210 B-2011
06/O1/20 15:54
JOC
Chemical Oxygen Demand^
31000
mg/L
80
800
800
OF05011
SM 5220D-2011
06/05/20 16:22
JOC
Nitrate as N [14797-55-8]
2.8
D
mg/L
5
0.20
0.50
[CALC]
EPA 353.2
06/03/20 15:11
JAH
Nitrate/Nitrite as N^
3.1
D
mg/L
5
0.20
0.50
OF03016
EPA 353.2
06/03/20 15:11
JAH
Nitrite as N [14797-65-0]^
0.24
mg/L
1
0.017
0.10
OF01050
EPA 353.2
06/O1/20 17:25
JAH
Phosphorus[7723-14-O]^
660
D
mg/L
500
12
50
OF02004
EPA 365.4
06/04/20 12:38
JAH
Sodium Adsorption Ratio
1.25
[blank]
1
OF02013
CSU Method
06/09/20 13:48
JDH
Total Kjeldahl Nitrogen^
1800
D
mg/L
100
26
48
OF02005
EPA 351.2
06/04/20 11:03
JAH
Total Solids^
4.7
% by Volume
1
0.0050
0.0050
OF05045
SM 2540B-2011
06/05/20 16:50
JOC
Total Suspended Solids^
29000
mg/L
100
250
250
OF05015
SM 2540D-2011
06/05/20 14:30
DMJ
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 13

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch OFO2O19 - EPA 747OA
Blank (OF02019-BLK3) Prepared: 06/02/2020 13:26 Analyzed: 06/03/2020 14:32
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Mercury 0.000150 U 0.000200 mg/L
LCS (OF02019-BS1) Prepared: 06/02/2020 13:26 Analyzed: 06/03/2020 14:35
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00518
0.000200
mg/L
0.00500
104
80-120
Matrix Spike (OF02019-MS3)
Prepared: 06/02/2020 13:26 Analyzed: 06/03/2020 14:39
Source: CD07826-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00549
0.000200
mg/L
0.00500
0.000150 U
110
75-125
Matrix Spike Dup (OF02019-MSD1)
Prepared: 06/02/2020 13:26 Analyzed: 06/03/2020 14:42
Source: CD07826-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00529
0.000200
mg/L
0.00500
0.000150 U
106
75-125 4
25
Post Spike (OF02019-PS3)
Prepared: 06/02/2020 13:26 Analyzed: 06/03/2020 14:44
Source: CD07826-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
5.47
0.200
ug/L
5.00
-0.00400
109
75-125
Metals (total recoverable) by EPA 6000/7000
Series Methods - Quality Control
Batch OFO2O13 - EPA 3OO5A
Blank (OF02013-BLK1)
Prepared: 06/02/2020 11:00 Analyzed: 06/09/2020 11:37
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Aluminum
0.0420
U
0.100
mg/L
Arsenic
0.00760
U
0.0100
mg/L
Cadmium
0.000360
U
0.00100
mg/L
Calcium
0.0390
U
0.100
mg/L
Copper
0.00160
U
0.0100
mg/L
Lead
0.00310
U
0.0100
mg/L
Magnesium
0.0290
U
0.100
mg/L
Molybdenum
0.00250
U
0.0100
mg/L
Nickel
0.00220
U
0.0100
mg/L
Potassium
0.150
U
0.500
mg/L
Selenium
0.00620
U
0.0100
mg/L
Sodium
0.400
U
0.500
mg/L
Zinc
0.00440
U
0.0100
mg/L
LCS (OF02013-BS1)
Prepared: 06/02/2020 11:00 Analyzed: 06/09/2020 11:43
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Aluminum 1.92 0.100 mg/L 2.00 96 80-120
Arsenic 0.200 0.0100 mg/L 0.200 100 80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 13

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch OFO2O13 - EPA 3OO5A - Continued
LCS (OF02013-BSI) Continued Prepared: 06/02/2020 11:00 Analyzed: 06/09/2020 11:43
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Cadmium
0.0199
0.00100
mg/L
0.0200
99
80-120
Calcium
2.05
0.100
mg/L
2.00
103
80-120
Copper
0.195
0.0100
mg/L
0.200
98
80-120
Lead
0.201
0.0100
mg/L
0.200
100
80-120
Magnesium
1.98
0.100
mg/L
2.00
99
80-120
Molybdenum
0.196
0.0100
mg/L
0.200
98
80-120
Nickel
0.206
0.0100
mg/L
0.200
103
80-120
Potassium
10.3
0.500
mg/L
10.0
103
80-120
Selenium
0.206
0.0100
mg/L
0.200
103
80-120
Sodium
10.4
0.500
mg/L
10.0
104
80-120
Zinc
0.206
0.0100
mg/L
0.200
103
80-120
Matrix Spike (OF02013-MS1)
Prepared:
06/02/2020
11:00 Analyzed: 06/09/2020 11:45
Source: CD07826-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Aluminum
1.97
0.100
mg/L
2.00
0.0420 U
98
75-125
Arsenic
0.206
0.0100
mg/L
0.200
0.00760 U
103
75-125
Cadmium
0.0199
0.00100
mg/L
0.0200
0.000360 U
100
75-125
Calcium
65.0
0.100
mg/L
2.00
63.3
82
75-125
Copper
0.202
0.0100
mg/L
0.200
0.00160 U
101
75-125
Lead
0.206
0.0100
mg/L
0.200
0.00310 U
103
75-125
Magnesium
24.1
0.100
mg/L
2.00
21.6
124
75-125
Molybdenum
0.202
0.0100
mg/L
0.200
0.00250 U
101
75-125
Nickel
0.211
0.0100
mg/L
0.200
0.00291
104
75-125
Potassium
17.1
0.500
mg/L
10.0
6.95
101
75-125
Selenium
0.211
0.0100
mg/L
0.200
0.00620 U
105
75-125
Sodium
61.0
0.500
mg/L
10.0
51.0
100
75-125
Zinc
0.217
0.0100
mg/L
0.200
0.00615
105
75-125
Matrix Spike Dup (OF02013-MSD1)
Prepared:
06/02/2020
11:00 Analyzed: 06/09/2020 11:52
Source: CD07826-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Aluminum
2.00
0.100
mg/L
2.00
0.0420 U
100
75-125
1
20
Arsenic
0.211
0.0100
mg/L
0.200
0.00760 U
106
75-125
2
20
Cadmium
0.0201
0.00100
mg/L
0.0200
0.000360 U
100
75-125
0.9
20
Calcium
65.7
0.100
mg/L
2.00
63.3
121
75-125
1
20
Copper
0.204
0.0100
mg/L
0.200
0.00160 U
102
75-125
1
20
Lead
0.207
0.0100
mg/L
0.200
0.00310 U
104
75-125
0.6
20
Magnesium
24.0
0.100
mg/L
2.00
21.6
121
75-125
0.2
20
Molybdenum
0.204
0.0100
mg/L
0.200
0.00250 U
102
75-125
1
20
Nickel
0.213
0.0100
mg/L
0.200
0.00291
105
75-125
1
20
Potassium
17.5
0.500
mg/L
10.0
6.95
105
75-125
2
20
Selenium
0.215
0.0100
mg/L
0.200
0.00620 U
108
75-125
2
20
Sodium
61.1
0.500
mg/L
10.0
51.0
101
75-125
0.2
20
Zinc
0.219
0.0100
mg/L
0.200
0.00615
107
75-125
1
20
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 13

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch OF02013 - EPA 3005A - Continued
Post Spike (OF02013-PS1)
Prepared: 06/02/2020 11:00 Analyzed: 06/09/2020 11:55
Source: CD07826-01
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD Limit Notes
Aluminum
1.99
0.100
mg/L
2.00
-0.00243
99
80-120
Arsenic
0.213
0.0100
mg/L
0.200
-0.00520
107
80-120
Cadmium
0.0203
0.00100
mg/L
0.0200
-0.000348
102
80-120
Calcium
64.2
0.100
mg/L
2.00
63.3
42
80-120 QM-08
Copper
0.207
0.0100
mg/L
0.200
0.000478
103
80-120
Lead
0.212
0.0100
mg/L
0.200
0.00106
105
80-120
Magnesium
23.2
0.100
mg/L
2.00
21.6
81
80-120
Molybdenum
0.207
0.0100
mg/L
0.200
0.00148
103
80-120
Nickel
0.217
0.0100
mg/L
0.200
0.00291
107
80-120
Potassium
17.3
0.500
mg/L
10.0
6.95
104
80-120
Selenium
0.222
0.0100
mg/L
0.200
0.000878
110
80-120
Sodium
60.3
0.500
mg/L
10.0
51.0
93
80-120
Zinc
0.235
0.0100
mg/L
0.200
0.00615
114
80-120
Classical Chemistry Parameters - Quality Control
Batch OF01047 - NO PREP
Blank (OF03047-BLKI) Prepared & Analyzed: 06/01/2020 15:54
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Biochemical Oxygen Demand 2.0 U 2.0 mg/L
LCS (OF03047-BS1) Prepared & Analyzed: 06/01/2020 15:54
Spike
Source
%REC
RPD
Analvte
Result Flaa
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Biochemical Oxygen Demand
200
2.0
mg/L
198
102 85-115
Duplicate (OF03047-DUP3)
Prepared & Analyzed: 06/01/2020 15:54
Source: CD06910-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Biochemical Oxygen Demand
2.0 U
2.0
mg/L
2.0 U
30
Batch OF01050 - NO PREP
Blank (OF01050-BLKI)
Prepared: 06/01/2020 15:44 Analyzed: 06/01/2020 17:21
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
0.017
U
0.10
mg/L
LCS (OF03050-BS1)
Prepared: 06/01/2020 15:44 Analyzed: 06/01/2020 17:28
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
1.0
0.10
mg/L
1.00 102 90-110
Matrix Spike (01`03050-MS3)
Prepared: 06/01/2020 15:44 Analyzed: 06/01/2020 17:23
Source: CD06910-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
FINAL
This report relates only to
the sample as received by the
laboratory, and may only be reproduced in full.
Page 7 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OFO1O5O - NO PREP - Continued
Matrix Spike (OFO1050-MS3) Continued
Prepared: 06/01/2020 15:44 Analyzed: 06/01/2020 17:23
Source: CD06910-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrite as N
1.1
0.10
mg/L
1.00 0.034 107 90-110
Matrix Spike Dup (OF03050-MSD3)
Prepared: 06/01/2020 15:44 Analyzed: 06/01/2020 17:24
Source: CD06910-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrite as N
1.1
0.10
mg/L
1.00 0.034 108 90-110 1
10
Batch OFO2OO4 - Same
Blank (OF02004-BLKi) Prepared: 06/02/2020 08:00 Analyzed: 06/04/2020 12:13
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Phosphorus 0.025 U 0.10 mg/L
LCS (OF02004-BS1) Prepared: 06/02/2020 08:00 Analyzed: 06/04/2020 12:14
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Phosphorus
1.6
0.10
mg/L
1.60 102 80-120
Matrix Spike (OF02004-MS1)
Prepared: 06/02/2020 08:00 Analyzed: 06/04/2020 12:17
Source: CD06910-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Phosphorus
1.8
D
0.50
mg/L
0.640 1.2 90 80-120
Matrix Spike Dup (OF02004-MSD1)
Prepared: 06/02/2020 08:00 Analyzed: 06/04/2020 12:18
Source: CD06910-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Phosphorus
1.9
D
0.50
mg/L
0.640 1.2 101 80-120 4
25
Batch OFO2OO5 - Same
Blank (OF02005-BLKi) Prepared: 06/02/2020 08:00 Analyzed: 06/04/2020 10:50
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Kjeldahl Nitrogen 0.26 U 0.48 mg/L
LCS (OF02005-BS1) Prepared: 06/02/2020 08:00 Analyzed: 06/04/2020 10:52
Spike Source %REC
RPD
Analvte
Result Flaa
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
13
0.48
mg/L
12.0 108 90-110
Matrix Spike (OF02005-MS3)
Prepared: 06/02/2020 08:00 Analyzed: 06/04/2020 10:55
Source: CD06910-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
4.7 D
0.96
mg/L
4.80 0.68 85 90-110
QM-07
FINAL
This report relates only to
the sample as received by the
laboratory, and may only be reproduced in full.
Page 8 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OF02005 - Same - Continued
Matrix Spike (OF02005-MS2)
Prepared: 06/02/2020 08:00 Analyzed: 06/04/2020 11:15
Source: CDO1630-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Kjeldahl Nitrogen
5.6
0.48
mg/L
4.80 0.87 99 90-110
Matrix Spike Dup (OF02005-MSD3)
Prepared: 06/02/2020 08:00 Analyzed: 06/04/2020 10:57
Source: CD06910-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Kjeldahl Nitrogen
5.2 D
0.96
mg/L
4.80 0.68 95 90-110 10
10
Batch OF02013 - EPA 3005A
Blank (OF02013-BLKi) Prepared: 06/02/2020 11:00 Analyzed: 06/09/2020 13:48
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Sodium Adsorption Ratio 0.00 U [blank]
Batch OF03016 - NO PREP
Blank (OF03016-BLKi) Prepared: 06/03/2020 09:28 Analyzed: 06/03/2020 14:00
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Nitrate/Nitrite as N 0.041 U 0.10 mg/L
LCS (OF03016-BS1) Prepared: 06/03/2020 09:28 Analyzed: 06/03/2020 14:01
Spike Source %REC
RPD
Analvte
Result
Flaa
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
1.3
0.10
mg/L
1.25 107 90-110
Matrix Spike (OF03016-MS3)
Prepared: 06/03/2020 09:28 Analyzed: 06/03/2020 14:05
Source: CD06827-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
0.74
0.10
mg/L
0.521 0.20 105 90-110
Matrix Spike (OF03016-MS2)
Prepared: 06/03/2020 09:28 Analyzed: 06/03/2020 14:10
Source: CD06827-02
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
1.8
0.10
mg/L
0.521 1.2 114 90-110
QM-07
Matrix Spike Dup (OF03016-MSD3)
Prepared: 06/03/2020 09:28 Analyzed: 06/03/2020 14:07
Source: CD06827-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
0.74
0.10
mg/L
0.521 0.20 104 90-110 0.4
10
Batch OF0402B - NO PREP
Blank (OF04028-BLKi) Prepared: 06/04/2020 12:01 Analyzed: 06/04/2020 14:07
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Ammonia as N 0.045 U 0.10 mg/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 0FO4O2B - NO PREP - Continued
LCS (OF04028-BSI) Prepared: 06/04/2020 12:01 Analyzed: 06/04/2020 14:09
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
1.0
0.10
mg/L
1.01 99 90-110
Matrix Spike (OF04028-MS3)
Prepared: 06/04/2020 12:01 Analyzed: 06/04/2020 14:12
Source: CD06897-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
4.3
1.0
mg/L
4.04 0.45 U 107 90-110
Matrix Spike (OF04028-MS2)
Prepared: 06/04/2020 12:01 Analyzed: 06/04/2020 14:17
Source: CD06900-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
0.74
0.10
mg/L
0.505 0.36 75 90-110
QM-07
Matrix Spike Dup (OF04028-MSD1)
Prepared: 06/04/2020 12:01 Analyzed: 06/04/2020 14:14
Source: CD06897-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
3.6
1.0
mg/L
4.04 0.45 U 89 90-110 18
10
QM-07,
QM-11
Batch 0FO5O11 - Same
Blank (OF05011-BLK1) Prepared: 06/05/2020 09:08 Analyzed: 06/05/2020 16:22
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Chemical Oxygen Demand 10 U 10 mg/L
LCS (OF05011-BS1) Prepared: 06/05/2020 09:08 Analyzed: 06/05/2020 16:22
Spike
Source
%REC
RPD
Analvte
Result Flaa
Q
Units
Level
Result
%REC
Limits RPD
Limit Notes
Chemical Oxygen Demand
500
10
mg/L
500
101
90-110
Matrix Spike (01`05011-MS3)
Prepared: 06/05/2020 09:08 Analyzed: 06/05/2020 16:22
Source: CD06201-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Chemical Oxygen Demand
610
10
mg/L
526
73
102
90-110
Matrix Spike Dup (OF05011-MSD3)
Prepared: 06/05/2020 09:08 Analyzed: 06/05/2020 16:22
Source: CD06201-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Chemical Oxygen Demand
610
10
mg/L
526
73
103
90-110 0.4
5
Batch 0FO5O15 - NO PREP
Blank (OF05015-BLK3) Prepared: 06/05/2020 12:10 Analyzed: 06/05/2020 14:30
Spike Source %REC RPD
Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes
Total Suspended Solids 2.5 U 2.5 mg/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OFO5O15 - NO PREP - Continued
LCS (OFO5O15-BSI)
Prepared: 06/05/2020 12:10 Analyzed: 06/05/2020 14:30
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Total Suspended Solids
92
2.5
mg/L
100 92 80-120
Duplicate (OF05015-DUPl)
Prepared: 06/05/2020 12:10 Analyzed: 06/05/2020 14:30
Source: CD08629-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Total Suspended Solids
17
17
mg/L
18
4
20
Duplicate (01`05015-DUP2)
Prepared: 06/05/2020 12:10 Analyzed: 06/05/2020 14:30
Source: CD08760-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Total Suspended Solids
26
8.3
mg/L
19
29
20
QM-12
Batch OFO5O45 - NO PREP
Blank (OF05045-BLKI)
Prepared & Analyzed: 06/05/2020 16:50
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Total Solids
0.0050
U
0.0050
% by Volume
LCS (OF05045-BS1)
Prepared & Analyzed: 06/05/2020 16:50
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Total Solids
1100
50
mg/L
1100 99 80-120
Duplicate (OF05045-DUP3)
Prepared & Analyzed: 06/05/2020 16:50
Source: CD07431-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Total Solids
0.23
0.0050
% by Volume
0.23
0.2
20
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 13

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits.
QM-12 Precision between duplicate samples was outside acceptance limits.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 13

10775 Central Port Dr. 4810 Executive Park Court, Suite 111
102-A Woodwinds Industsial Ct.
Lf��M­ MINIS
Orlando, FL 32824 Jacksonville, FL 32216-6M9
Cary, NC 27511
[phone] Fax (407) B50-6945 (904) 2963007 Fax [phone]
[phone] Fax [phone]
Page of
Client Name
Project Number
Requested Analyses
Requested Turnaround
Times
NoypgM I
Vorth America NO008) [nonel
OQ
Address
Project Natne/Desc
Note : Rush requests subject to
77 Perps
ipel Church Road
Monthly - Week One - SBM
acceptance by the facility
CitylsT/Zip
PON/Billing Info
H
0
Fraokh&, f
4C 27525
3800466333
0
8
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2
— Standard
tq
Q
Tel
Fax
Reporting Contact
X{912)
30
00
Scott Creech
Z.
LO to
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N
— Expedited
Samplers Name, Affillation
(Print)
Billing Contact
Accounts Payable
,$
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y
Due —f I
ljGt t.l {
Samplers) Signature
Ti
site Location 1 me Zone
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Lab WOrkOrder
c3v n rVNA-
a t
inU=
z
l+-
CD08740
f nmervatlon (See Codes) {Combine as necessary)
Collection Matrix Total # of
Sample Comments
Item H Sample ID
(Field Identification) Collection
Date Time Comp / Grab (see cedes) Containers
C) SL 7
X
X
X X
�/
X X
X
Total # of Containers
Sample Kit Prepared By
Dat (rime Relinquished By�
Date✓rme
Receive y
DatelTme
r r)
C/)Py
CommentsrSpecial Re
g Requirements
l
Relinquished By
Daterlime
Recei B
Dafr me
QJrr
'
Relinquished By
Dale>Tme
Received By
DaterTme
Cooler u's & Temps on Receipt
—
1- i—
Condition
pon Receipt
AcceptaWe Unacceptable
matrix: GW-Graundvraler SO -Sail DW-Drinking Water SE -Sediment SW -Surface Water W W-Wastewater A -Air O-Other (detail in comments)
Preservation: Flea H-HCI N-HNO3 5-H2SO4 NO-NaOH O-Other {detait in comments)
Note : All samples submitted to ENCO tabs are in accordance with the terms and
conditions
listed an the
reverse of this
Corm. unless prior written agreement& exist
I

Sample Preservation Verification
ENCO Cary
Q
Work Order: CDO8740 Project: Monthly - Week One - SBM
Client: Novozymes North America (N0008) Project #: [none]
Logged In: 01-Jun-20 10 10 Logged By: John C King
Preservation Check Performed By: DatelTime:
CDO8740-01
Cont
Type
Pres (pH)
Requirement
pH Checked I
In Control
pH Adjusted DatefTime
Adjusted
Reagent Used/Comments
D
250mLP+H2SO4
<2
Y I NA
N I NA �.I,ZD
L aq
E
250mLP+HNO3
<2
Y 1 N/ NA
Y 1 (' NA
mL f+W3
Rea ent Name ID
1f4 KV3
2 2Sioq
pH Strip ID: CQC%
Reagent Name ID
3
4
Rea ent Name ID
5
6
C:1ELMNTIPrintlwko_PreservationCheck.rpt Page 1

2�SQ pCCgF ENCO Laboratories
9e0
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Monday, June 15, 2020
Novozymes North America (N0008)
Attn: Scott Creech
77 Perry Chapel Church Road
Franklinton, NC 27525
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: Monthly - Week One - SBM
ENCO Workorder(s): CD08741
Dear Scott Creech,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, June 2, 2020.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
0"6LC'=-:;tA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 13

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: SBM
Lab ID: CD08741-01
Sampled: 06/02/20 01:30
Received: 06/02/20 11:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
CSU Method
NO PREP
02/26/23
06/04/20
11:37
06/10/20
16:27
EPA 350.1
NO PREP
06/30/20
06/04/20
12:01
06/04/20
14:49
EPA 351.2
Same
06/30/20
06/05/20
10:47
06/08/20
11:28
EPA 353.2
NO PREP
06/04/20
01:30
06/02/20
15:50
06/02/20
17:16
EPA 353.2
[CALC]
06/04/20
01:30
06/12/20
09:20
06/12/20
13:02
EPA 353.2
NO PREP
06/30/20
06/12/20
09:20
06/12/20
13:02
EPA 365.4
Same
06/30/20
06/05/20
10:47
06/08/20
13:22
EPA 6010D
EPA 3005A
11/29/20
06/04/20
11:37
06/10/20
15:07
EPA 7470A
EPA 7470A
06/30/20
06/02/20
13:26
06/03/20
15:36
SM 254OB-2011
NO PREP
06/09/20
06/05/20
16:50
06/05/20
16:50
SM 2540D-2011
NO PREP
06/09/20
06/08/20
12:45
06/08/20
12:45
SM 5210 B-2011
NO PREP
06/04/20
01:30
06/03/20
10:55
06/03/20
10:55
SM 5220D-2011
Same
06/30/20
06/05/20
09:08
06/05/20
16:22
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 13

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SAMPLE DETECTION SUMMARY
Client ID: SBM
Lab ID: CDO8741-01
Analvte
Results
Flag
MDL
PQL
Units
Method Notes
Aluminum - Total
64.1
D
0.420
1.00
mg/L
EPA 6010D
Ammonia as N
180
DE
4.0
9.0
mg/L
EPA 350.1
Biochemical Oxygen Demand
10000
2.0
2.0
mg/L
SM 5210 B-2011
Calcium - Total
2970
D
0.390
1.00
mg/L
EPA 6010D
Chemical Oxygen Demand
31000
800
800
mg/L
SM 5220D-2011
Copper - Total
0.120
D
0.0160
0.100
mg/L
EPA 6010D
Magnesium - Total
14.2
D
0.290
1.00
mg/L
EPA 6010D
Molybdenum - Total
0.0360
3D
0.0250
0.100
mg/L
EPA 6010D
Nickel - Total
0.0293
3D
0.0220
0.100
mg/L
EPA 6010D
Nitrate as N
7.5
D
0.82
2.0
mg/L
EPA 353.2
Nitrate/Nitrite as N
7.9
D
0.82
2.0
mg/L
EPA 353.2
Nitrite as N
0.43
0.017
0.10
mg/L
EPA 353.2
Phosphorus
640
D
12
50
mg/L
EPA 365.4
Potassium - Total
398
D
1.50
5.00
mg/L
EPA 6010D
Sodium - Total
237
D
4.00
5.00
mg/L
EPA 6010D
Sodium Adsorption Ratio
1.19
[blank]
CSU Method
Total Kjeldahl Nitrogen
2000
D
52
96
mg/L
EPA 351.2
Total Solids
4.6
0.0050
0.0050
% by Volume
SM 254OB-2011
Total Suspended Solids
13000
2500
2500
mg/L
SM 2540D-2011
Zinc - Total
0.392
D
0.0440
0.100
mg/L
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 13

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ANALYTICAL RESULTS
Description: SBM Lab Sample ID:CD08741-01 Received: 06/02/20 11:00
Matrix: Sludge Sampled: 06/02/20 01:30 Work Order: CD08741
Project: Monthly - Week One - SBM Sampled By: Elvin C Williamson
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay Notes
Mercury [7439-97-6]^
0.00150
U
mg/L
10
0.00150
0.00200
OF02019
EPA 7470A
06/03/20 15:36
KAH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Ay Notes
Aluminum [7429-90-5]^
64.1
D
mg/L
10
0.420
1.00
OF04027
EPA 6010D
06/10/20 15:07
JDH
Arsenic [7440-38-2]^
0.0760
UD
mg/L
10
0.0760
0.100
OF04027
EPA 6010D
06/10/20 15:07
JDH
Cadmium [7440-43-9]^
0.00360
UD
mg/L
10
0.00360
0.0100
OF04027
EPA 6010D
06/10/20 15:07
JDH
Calcium [7440-70-2]^
2970
D
mg/L
10
0.390
1.00
OF04027
EPA 6010D
06/10/20 15:07
JDH
Copper[7440-50-8]^
0.120
D
mg/L
10
0.0160
0.100
OF04027
EPA 6010D
06/10/20 15:07
JDH
Lead [7439-92-1]^
0.0310
UD
mg/L
10
0.0310
0.100
OF04027
EPA 6010D
06/10/20 15:07
JDH
Magnesium [7439-95-4]^
14.2
D
mg/L
10
0.290
1.00
OF04027
EPA 6010D
06/10/20 15:07
JDH
Molybdenum [7439-98-7]^
0.0360
JD
mg/L
10
0.0250
0.100
OF04027
EPA 6010D
06/10/20 15:07
JDH
Nickel[7440-02-O]^
0.0293
JD
mg/L
10
0.0220
0.100
OF04027
EPA 6010D
06/10/20 15:07
JDH
Potassium [7440-09-7]^
398
D
mg/L
10
1.50
5.00
OF04027
EPA 6010D
06/10/20 15:07
JDH
Selenium [7782-49-2]^
0.0620
UD
mg/L
10
0.0620
0.100
OF04027
EPA 6010D
06/10/20 15:07
JDH
Sodium [7440-23-5]^
237
D
mg/L
10
4.00
5.00
OF04027
EPA 6010D
06/10/20 15:07
JDH
Zinc[7440-66-6]^
0.392
D
mg/L
10
0.0440
0.100
OF04027
EPA 6010D
06/10/20 15:07
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Ay Notes
Ammonia as N [7664-41-7]^
180
DE
mg/L
90
4.0
9.0
OF04028
EPA 350.1
06/04/20 14:49
JAH
Biochemical Oxygen Demand^
10000
mg/L
1
2.0
2.0
OF03011
SM 5210 B-2011
06/03/20 10:55
JOC
Chemical Oxygen Demand^
31000
mg/L
80
800
800
OF05011
SM 5220D-2011
06/05/20 16:22
JOC
Nitrate as N [14797-55-8]
7.5
D
mg/L
20
0.82
2.0
[CALC]
EPA 353.2
06/12/20 13:02
JAH
Nitrate/Nitrite as N^
7.9
D
mg/L
20
0.82
2.0
OF12008
EPA 353.2
06/12/20 13:02
JAH
Nitrite as N [14797-65-0]^
0.43
mg/L
1
0.017
0.10
OF02025
EPA 353.2
06/02/20 17:16
JAH
Phosphorus[7723-14-O]^
640
D
mg/L
500
12
50
OF05017
EPA 365.4
06/08/20 13:22
JAH
Sodium Adsorption Ratio
1.19
[blank]
1
OF04027
CSU Method
06/10/20 16:27
JDH
Total Kjeldahl Nitrogen^
2000
D
mg/L
200
52
96
OF05018
EPA 351.2
06/08/20 11:28
JAH
Total Solids^
4.6
% by Volume
1
0.0050
0.0050
OF05045
SM 2540B-2011
06/05/20 16:50
JOC
Total Suspended Solids^
13000
mg/L
1000
2500
2500
OF05049
SM 2540D-2011
06/08/20 12:45
DMJ
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 13

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch OFO2O19 - EPA 747OA
Blank (OF02019-BLK3) Prepared: 06/02/2020 13:26 Analyzed: 06/03/2020 14:32
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Mercury 0.000150 U 0.000200 mg/L
LCS (OF02019-BS1) Prepared: 06/02/2020 13:26 Analyzed: 06/03/2020 14:35
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00518
0.000200
mg/L
0.00500
104
80-120
Matrix Spike (OF02019-MS3)
Prepared: 06/02/2020 13:26 Analyzed: 06/03/2020 14:39
Source: CD07826-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00549
0.000200
mg/L
0.00500
0.000150 U
110
75-125
Matrix Spike Dup (OF02019-MSD1)
Prepared: 06/02/2020 13:26 Analyzed: 06/03/2020 14:42
Source: CD07826-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00529
0.000200
mg/L
0.00500
0.000150 U
106
75-125 4
25
Post Spike (OF02019-PS3)
Prepared: 06/02/2020 13:26 Analyzed: 06/03/2020 14:44
Source: CD07826-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
5.47
0.200
ug/L
5.00
-0.00400
109
75-125
Metals (total recoverable) by EPA 6000/7000
Series Methods - Quality Control
Batch OFO4O27 - EPA 3OO5A
Blank (OF04027-BLK1)
Prepared: 06/04/2020 11:37 Analyzed: 06/10/2020 13:57
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Aluminum
0.0420
U
0.100
mg/L
Arsenic
0.00760
U
0.0100
mg/L
Cadmium
0.000360
U
0.00100
mg/L
Calcium
0.0390
U
0.100
mg/L
Copper
0.00160
U
0.0100
mg/L
Lead
0.00310
U
0.0100
mg/L
Magnesium
0.0290
U
0.100
mg/L
Molybdenum
0.00250
U
0.0100
mg/L
Nickel
0.00220
U
0.0100
mg/L
Potassium
0.150
U
0.500
mg/L
Selenium
0.00620
U
0.0100
mg/L
Sodium
0.400
U
0.500
mg/L
Zinc
0.00440
U
0.0100
mg/L
LCS (OF04027-BS1)
Prepared: 06/04/2020 11:37 Analyzed: 06/10/2020 14:02
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Aluminum 1.87 0.100 mg/L 2.00 93 80-120
Arsenic 0.188 0.0100 mg/L 0.200 94 80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 13

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch OFO4O27 - EPA 3OO5A - Continued
LCS (OF04027-BSI) Continued Prepared: 06/04/2020 11:37 Analyzed: 06/10/2020 14:02
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Cadmium
0.0188
0.00100
mg/L
0.0200
94
80-120
Calcium
1.99
0.100
mg/L
2.00
99
80-120
Copper
0.184
0.0100
mg/L
0.200
92
80-120
Lead
0.188
0.0100
mg/L
0.200
94
80-120
Magnesium
1.99
0.100
mg/L
2.00
99
80-120
Molybdenum
0.186
0.0100
mg/L
0.200
93
80-120
Nickel
0.193
0.0100
mg/L
0.200
97
80-120
Potassium
9.84
0.500
mg/L
10.0
98
80-120
Selenium
0.192
0.0100
mg/L
0.200
96
80-120
Sodium
9.97
0.500
mg/L
10.0
100
80-120
Zinc
0.192
0.0100
mg/L
0.200
96
80-120
Matrix Spike (OF04027-MS1)
Prepared:
06/04/2020
11:37 Analyzed: 06/10/2020 14:05
Source: CD07828-02
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Aluminum
2.01
0.100
mg/L
2.00
0.115
95
75-125
Arsenic
0.185
0.0100
mg/L
0.200
0.00760 U
92
75-125
Cadmium
0.0185
0.00100
mg/L
0.0200
0.000360 U
93
75-125
Calcium
28.8
0.100
mg/L
2.00
26.4
120
75-125
Copper
0.182
0.0100
mg/L
0.200
0.00160 U
91
75-125
Lead
0.189
0.0100
mg/L
0.200
0.00310 U
95
75-125
Magnesium
14.1
0.100
mg/L
2.00
12.1
101
75-125
Molybdenum
0.185
0.0100
mg/L
0.200
0.00250 U
92
75-125
Nickel
0.195
0.0100
mg/L
0.200
0.00459
95
75-125
Potassium
12.2
0.500
mg/L
10.0
2.41
98
75-125
Selenium
0.190
0.0100
mg/L
0.200
0.00620 U
95
75-125
Sodium
18.6
0.500
mg/L
10.0
8.65
100
75-125
Zinc
0.197
0.0100
mg/L
0.200
0.00654
95
75-125
Matrix Spike Dup (OF04027-MSD1)
Prepared:
06/04/2020
11:37 Analyzed: 06/10/2020 14:07
Source: CD07828-02
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Aluminum
1.97
0.100
mg/L
2.00
0.115
93
75-125
2
20
Arsenic
0.181
0.0100
mg/L
0.200
0.00760 U
90
75-125
2
20
Cadmium
0.0182
0.00100
mg/L
0.0200
0.000360 U
91
75-125
2
20
Calcium
28.0
0.100
mg/L
2.00
26.4
81
75-125
3
20
Copper
0.180
0.0100
mg/L
0.200
0.00160 U
90
75-125
1
20
Lead
0.184
0.0100
mg/L
0.200
0.00310 U
92
75-125
3
20
Magnesium
13.8
0.100
mg/L
2.00
12.1
86
75-125
2
20
Molybdenum
0.182
0.0100
mg/L
0.200
0.00250 U
91
75-125
1
20
Nickel
0.193
0.0100
mg/L
0.200
0.00459
94
75-125
2
20
Potassium
12.0
0.500
mg/L
10.0
2.41
96
75-125
1
20
Selenium
0.187
0.0100
mg/L
0.200
0.00620 U
93
75-125
2
20
Sodium
18.3
0.500
mg/L
10.0
8.65
96
75-125
2
20
Zinc
0.192
0.0100
mg/L
0.200
0.00654
93
75-125
2
20
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 13

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch OF04027 - EPA 3005A - Continued
Post Spike (OF04027-PS1)
Prepared: 06/04/2020 11:37 Analyzed: 06/10/2020 14:09
Source: CD07828-02
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD Limit Notes
Aluminum
1.98
0.100
mg/L
2.00
0.115
93
80-120
Arsenic
0.192
0.0100
mg/L
0.200
-0.00101
96
80-120
Cadmium
0.0190
0.00100
mg/L
0.0200
0.000221
94
80-120
Calcium
27.9
0.100
mg/L
2.00
26.4
75
80-120 QM-08
Copper
0.188
0.0100
mg/L
0.200
-0.00123
94
80-120
Lead
0.195
0.0100
mg/L
0.200
-0.000642
97
80-120
Magnesium
13.7
0.100
mg/L
2.00
12.1
82
80-120
Molybdenum
0.190
0.0100
mg/L
0.200
-0.000348
95
80-120
Nickel
0.201
0.0100
mg/L
0.200
0.00459
98
80-120
Potassium
12.4
0.500
mg/L
10.0
2.41
99
80-120
Selenium
0.195
0.0100
mg/L
0.200
0.00127
97
80-120
Sodium
18.6
0.500
mg/L
10.0
8.65
100
80-120
Zinc
0.211
0.0100
mg/L
0.200
0.00654
102
80-120
Classical Chemistry Parameters - Quality Control
Batch OF02025 - NO PREP
Blank (OF02025-BLKI) Prepared: 06/02/2020 15:50 Analyzed: 06/02/2020 17:02
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Nitrite as N 0.017 U 0.10 mg/L
LCS (OF02025-BS1) Prepared: 06/02/2020 15:50 Analyzed: 06/02/2020 17:20
Spike Source %REC
RPD
Analvte
Result Flaa
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrite as N
1.0
0.10
mg/L
1.00 104 90-110
Matrix Spike (OF02025-MS3)
Prepared: 06/02/2020 15:50 Analyzed: 06/02/2020 17:06
Source: CD07431-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrite as N
1.1
0.10
mg/L
1.00 0.089 100 90-110
Matrix Spike Dup (OF02025-MSD3)
Prepared: 06/02/2020 15:50 Analyzed: 06/02/2020 17:07
Source: CD07431-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrite as N
1.1
0.10
mg/L
1.00 0.089 100 90-110 0.3
10
Batch OF03011 - NO PREP
Blank (OF03011-BLK1)
Prepared & Analyzed: 06/03/2020 10:55
Spike Source %REC
RPD
Analvte
Result Flaq POL Units Level Result %REC Limits RPD
Limit Notes
Biochemical Oxygen Demand
2.0 U 2.0 mg/L
LCS (OF03011-BSI)
Prepared & Analyzed: 06/03/2020 10:55
Spike Source %REC
RPD
Analvte
Result Flaq POL Units Level Result %REC Limits RPD
Limit Notes
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 7 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OFO3O11 - NO PREP - Continued
LCS (OF03011-BSI) Continued Prepared & Analyzed: 06/03/2020 10:55
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Biochemical Oxygen Demand
180
2.0
mg/L
198
92 85-115
Duplicate (OF03011-DUPl)
Prepared & Analyzed: 06/03/2020 10:55
Source: CD07186-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Biochemical Oxygen Demand
870
2.0
mg/L
880
1
30
Batch OFO4O27 - EPA 3OO5A
Blank (OF04027-BLKi) Prepared: 06/04/2020 11:37 Analyzed: 06/10/2020 16:28
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Sodium Adsorption Ratio 0.00 U [blank]
Batch OFO4O2B - NO PREP
Blank (OF04028-BLKi) Prepared: 06/04/2020 12:01 Analyzed: 06/04/2020 14:07
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Ammonia as N 0.045 U 0.10 mg/L
LCS (OF04028-BS1) Prepared: 06/04/2020 12:01 Analyzed: 06/04/2020 14:09
Spike Source %REC
RPD
Analvte
Result
Flaa
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
1.0
0.10
mg/L
1.01 99 90-110
Matrix Spike (OF04028-MS3)
Prepared: 06/04/2020 12:01 Analyzed: 06/04/2020 14:12
Source: CD06897-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
4.3
1.0
mg/L
4.04 0.45 U 107 90-110
Matrix Spike (OF04028-MS2)
Prepared: 06/04/2020 12:01 Analyzed: 06/04/2020 14:17
Source: CD06900-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
0.74
0.10
mg/L
0.505 0.36 75 90-110
QM-07
Matrix Spike Dup (OF04028-MSD3)
Prepared: 06/04/2020 12:01 Analyzed: 06/04/2020 14:14
Source: CD06897-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
3.6
1.0
mg/L
4.04 0.45 U 89 90-110 18
10
QM-07,
QM-11
Batch OFO5O11 - Same
Blank (OF05011-BLK1) Prepared: 06/05/2020 09:08 Analyzed: 06/05/2020 16:22
Spike Source %REC RPD
Analvte Result Flaci Q Units Level Result %REC Limits RPD Limit Notes
Chemical Oxygen Demand 10 U 10 mg/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OFO5O11 - Same - Continued
LCS (OFO5011-BSI)
Prepared: 06/05/2020 09:08 Analyzed: 06/05/2020 16:22
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chemical Oxygen Demand
500
10
mg/L
500 101 90-110
Matrix Spike (OF05011-MS3)
Prepared: 06/05/2020 09:08 Analyzed: 06/05/2020 16:22
Source: CD06201-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chemical Oxygen Demand
610
10
mg/L
526 73 102 90-110
Matrix Spike Dup (OF05031-MSD3)
Prepared: 06/05/2020 09:08 Analyzed: 06/05/2020 16:22
Source: CD06201-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chemical Oxygen Demand
610
10
mg/L
526 73 103 90-110 0.4
5
Batch OFO5O17 - Same
Blank (OF05017-BLKI)
Prepared: 06/05/2020 10:47 Analyzed: 06/08/2020 12:48
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
0.025
U
0.10
mg/L
LCS (OF05017-BS1)
Prepared: 06/05/2020 10:47 Analyzed: 06/08/2020 12:49
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
1.5
0.10
mg/L
1.60 95 80-120
Matrix Spike (OF05017-MS1)
Prepared: 06/05/2020 10:47 Analyzed: 06/08/2020 12:52
Source: CD07438-02
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
1.5
0.10
mg/L
0.640 0.90 89 80-120
Matrix Spike Dup (OF05017-MSD1)
Prepared: 06/05/2020 10:47 Analyzed: 06/08/2020 12:54
Source: CD07438-02
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
1.5
0.10
mg/L
0.640 0.90 85 80-120 2
25
Batch OFO5O18 - Same
Blank (OF05018-BLK1) Prepared: 06/05/2020 10:47 Analyzed: 06/08/2020 10:42
Spike Source %REC
RPD
Analvte
Result Flaa
POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Kjeldahl Nitrogen
0.26 U
0.48
mg/L
LCS (OF05018-BSI)
Prepared: 06/05/2020 10:47 Analyzed: 06/08/2020 10:44
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Kjeldahl Nitrogen
13
0.48
mg/L
12.0 109 90-110
FINAL
This report relates only to
the sample as received by the
laboratory, and may only be reproduced in full.
Page 9 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OF05018 - Same - Continued
Matrix Spike (OF05018-MS3)
Prepared: 06/05/2020 10:47 Analyzed: 06/08/2020 10:48
Source: CD07438-02
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
8.7
0.48
mg/L
4.80 2.9 122 90-110
QM-07
Matrix Spike (OF05018-MS2)
Prepared: 06/05/2020 10:47 Analyzed: 06/08/2020 10:53
Source: CD07893-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
5.4
0.48
mg/L
4.80 0.75 98 90-110
Matrix Spike Dup (01`05018-MS133)
Prepared: 06/05/2020 10:47 Analyzed: 06/08/2020 10:49
Source: CD07438-02
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
8.5
0.48
mg/L
4.80 2.9 117 90-110 3
10
QM-07
Batch OF05045 - NO PREP
Blank (OF05045-BLKI) Prepared & Analyzed: 06/05/2020 16:50
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Solids 0.0050 U 0.0050 % by Volume
LCS (OF05045-BS1) Prepared & Analyzed: 06/05/2020 16:50
Analvte
Total Solids
Result
1100
Flaq POL
50
Units
mg/L
Spike Source %REC
Level Result %REC Limits RPD
1100 99 80-120
RPD
Limit Notes
Duplicate (OF05045-DUP3)
Prepared & Analyzed: 06/05/2020 16:50
Source: CD07431-01
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Solids
0.23
0.0050
% by Volume
0.23 0.2
20
Batch OF05049 - NO PREP
Blank (OF05049-BLKI) Prepared & Analyzed: 06/08/2020 12:45
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Suspended Solids 2.5 U 2.5 mg/L
LCS (OF05049-BS1) Prepared & Analyzed: 06/08/2020 12:45
Spike Source %REC
RPD
Analvte
Result Flaa
POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Suspended Solids
100
2.5
mg/L
100 101 80-120
Duplicate (OF05049-DUP3)
Prepared & Analyzed: 06/08/2020 12:45
Source: CD08452-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Suspended Solids
220
50
mg/L
210 3
20
FINAL
This report relates only to
the sample as received by the
laboratory, and may only be reproduced in full.
Page 10 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OFO5O49 - NO PREP - Continued
Duplicate (OF05049-DUP2) Prepared & Analyzed: 06/08/2020 12:45
Source: CD07930-01
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes
Total Suspended Solids 82 50 mg/L 94 14 20
Batch OF12OO8 - NO PREP
Blank (OF32008-BLK1) Prepared: 06/12/2020 09:20 Analyzed: 06/12/2020 12:29
Spike Source O/oREC RPD
Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes
Nitrate/Nitrite as N 0.041 U 0.10 mg/L
LCS (OF12008-BS1) Prepared: 06/12/2020 09:20 Analyzed: 06/12/2020 12:31
Spike Source O/oREC
RPD
Analvte
Result
Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
1.2
0.10
mg/L
1.25 97 90-110
Matrix Spike (OF32008-MS3)
Prepared: 06/12/2020 09:20 Analyzed: 06/12/2020 12:35
Source: CD07902-01
Spike Source O/oREC
RPD
Analvte
Result
Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
55
5.0
mg/L
25.0 32 90 90-110
Matrix Spike (OF32008-MS2)
Prepared: 06/12/2020 09:20 Analyzed: 06/12/2020 12:40
Source: CD07905-01
Spike Source O/oREC
RPD
Analvte
Result
Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
15
1.0
mg/L
5.00 9.5 105 90-110
Matrix Spike Dup (OF12008-MSD3)
Prepared: 06/12/2020 09:20 Analyzed: 06/12/2020 12:36
Source: CD07902-01
Spike Source O/oREC
RPD
Analvte
Result
Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
55
5.0
mg/L
25.0 32 90 90-110 0.2
10
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 13

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
QM-ii Precision between duplicate matrix spikes of the same sample was outside acceptance limits.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 13

10775 Central Port Dr- 4810Executive Paris Court, Suite 111 Cary, t_ Woodwinds Industrial G
Orlando, FL 32624 Jacksonville, FL 32218-6069 Cary, NC 27511
LeEnmk' [phone] Fax (407185"945 (904) 29a-3007 Fax [phone] [phone] Fax [phone] Page Of
Client Name
Nava es North America 1400€ 8)
Project Number
[nonel
Requested
Analyses
Requested Turnaround
Times
Note: Rush requests subject to
acceptance by the facility
_ Standard
_ Expedited
Due
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Project NamelDesc
Monthly - Week One - SBM
City'ST/Zip
Frankliftn, NC 27625
PO 9 / Billing Into
3800466333
Tel
[phone]
Fax
I
Reporting Contact
Scott Creech
Samplar(s) Name, Affiliation (Print)
B'slling Contact
Accounts Payable
Sampler(s) Signature ,
Site Location ! Time Zone
Lab Worlforder
CLD0 V 74 1
Preservatlon
(See
Codes)
(Combine
as necessary)
l lem x
Sample ID (Field Identification)
Collecion Date
Collection
Time
Comp 1 Grab
Matrix
(see codes)
Total tf of
Containers
Sample Comments
SBM
`_ C
011,30
G-'
S!_
7
x
x
x
X
X
X
x
—Total # of Containers
Sample Kit Prepared By
Dal
me
Relinquished By +
Dale/Time r
Rec '
Date ime ;
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Comments/Special Repo g Requiremants
Relinquished By
Datettime
Received By
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Relinquished By
Dalerllme
Received Ely
Datefrime
Copier tl's & Temps on Receipt
Condttlan pon Receipt
Acceptable _ Unacceptable
Matrix: GW-Groundwater SO -Soil DW-Drinking Water SE -Sediment SW -Surface Water WW-Waslewater A -Air O-Other (detail in comments) Preservation: I -Ice FFHCi N-HN63 S-H2SO4 NO-NaOH O.Other (detall €n comments)
Note - All samples submitted to ENCO Labs are in accordance with the terms and conditions listed on the reverse of this form, unless prior written agreements exist

Sample Preservation Verification
ENCO Cary
Work Order: CD08741
Client:-Novozymes North America (NO008)
Logged in: 02-Jun-20 12:22
Project: Monthly - Week One - SBM
Project #: [none]
Logged By: John C King
Preservation Check Performed By, _ � Date/Time: 6'�'Z o 12.6
CDO8741-01
Cont
Type
Pres (pH)
Requirement
pH Checked /
in Control
pH Adjusted Date/Time
Adjusted
Reagent Used/Comments
D
250mLP+H2SO4
Q
/ N ! NA
Y ' 5/NA
E
25DmLP+HNO3
<2
1 N / NA
Y ! Q�1 NA
Rea ent Name ID
1
2
pH Strip ID: 2ycase _^
Rea ent Name ID
3
4
Rea ent Name ID
5
6
CaELMNTIPrintlwko_PreservationCheck.rpt Page 1

2�SQ pCCgF ENCO Laboratories
9e0
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102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Friday, July 17, 2020
Novozymes North America (N0008)
Attn: Scott Creech
77 Perry Chapel Church Road
Franklinton, NC 27525
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: Monthly - Week One - SBM
ENCO Workorder(s): CD09845
Dear Scott Creech,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, July 7, 2020.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
0"6LC'=-:;tA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 13

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: SBM
Lab ID: CD09845-01
Sampled: 07/07/20 07:30
Received: 07/07/20 10:02
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
CSU Method
NO PREP
04/02/23
07/07/20
14:45
07/09/20
16:01
EPA 351.2
Same
08/04/20
07/09/20
10:10
07/15/20
10:05
EPA 353.2
NO PREP
07/09/20
07:30
07/07/20
15:15
07/08/20
09:58
EPA 353.2
[CALC]
07/09/20
07:30
07/13/20
09:58
07/13/20
13:55
EPA 353.2
NO PREP
08/04/20
07/13/20
09:58
07/13/20
13:55
EPA 365.4
Same
08/04/20
07/09/20
10:10
07/10/20
12:43
EPA 6010D
EPA 3005A
01/03/21
07/07/20
14:45
07/09/20
10:48
EPA 7470A
EPA 7470A
08/04/20
07/14/20
11:57
07/16/20
17:58
SM 2540B-2011
NO PREP
07/14/20
07/14/20
17:29
07/14/20
17:29
SM 254OD-2011
NO PREP
07/14/20
07/14/20
12:57
07/14/20
12:57
SM 5210 B-2011
NO PREP
07/09/20
07:30
07/08/20
09:55
07/08/20
09:55
SM 5220D-2011
Same
08/04/20
07/10/20
09:10
07/10/20
14:44
Client ID: SBM
Lab ID: CD09845-OIRE1
Sampled: 07/07/20 07:30
Received: 07/07/20 10:02
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 350.1
NO PREP
08/04/20
07/13/20
14:56
07/14/20
11:12
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 13

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SAMPLE DETECTION SUMMARY :1
Client ID: SBM
Lab ID:
CD09845-01
Analvte
Results
Flag
MDL
Q
Units
Method Notes
Aluminum - Total
456
D
0.420
1.00
mg/L
EPA 6010D
Biochemical Oxygen Demand
18000
2.0
2.0
mg/L
SM 5210 B-2011
Calcium - Total
5540
D
0.390
1.00
mg/L
EPA 6010D
Chemical Oxygen Demand
44000
800
800
mg/L
SM 5220D-2011
Copper - Total
0.637
D
0.0160
0.100
mg/L
EPA 6010D
Magnesium - Total
77.4
D
0.290
1.00
mg/L
EPA 6010D
Molybdenum - Total
0.0312
ID
0.0250
0.100
mg/L
EPA 6010D
Nickel - Total
0.0680
ID
0.0220
0.100
mg/L
EPA 6010D
Nitrate as N
5.0
D
0.82
2.0
mg/L
EPA 353.2
Nitrate/Nitrite as N
5.3
D
0.82
2.0
mg/L
EPA 353.2
Nitrite as N
0.29
0.017
0.10
mg/L
EPA 353.2
Phosphorus
820
D
12
50
mg/L
EPA 365.4
Potassium - Total
591
D
1.50
5.00
mg/L
EPA 6010D
Sodium - Total
564
D
4.00
5.00
mg/L
EPA 6010D
Sodium Adsorption Ratio
2.06
[blank]
CSU Method
Total Kjeldahl Nitrogen
2500
D
52
96
mg/L
EPA 351.2
Total Solids
2.9
0.12
0.12
% by Volume
SM 254OB-2011
Total Suspended Solids
8400
500
500
mg/L
SM 254OD-2011
Zinc - Total
1.30
D
0.0440
0.100
mg/L
EPA 6010D
Client ID: SBM
Lab ID:
CD09845-01RE1
Anal a
Results
Flag
MDL
POLL
Units
Method Notes
Ammonia as N
170
D
22
50
mg/L
EPA 350.1
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 13

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ANALYTICAL RESULTS
Description: SBM Lab Sample ID:CD09845-01 Received: 07/07/20 10:02
Matrix: Sludge Sampled:07/07/20 07:30 Work Order: CD09845
Project: Monthly - Week One - SBM Sampled By: Adam Fauccette
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Ay Notes
Mercury [7439-97-6]^
0.000150
U
mg/L
1
0.000150
0.000200
OG14036
EPA 7470A
07/16/20 17:58
KAH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Ay Notes
Aluminum [7429-90-5]^
456
D
mg/L
10
0.420
1.00
OG07035
EPA 6010D
07/09/20 10:48
JDH
Arsenic [7440-38-2]^
0.0760
UD
mg/L
10
0.0760
0.100
OG07035
EPA 6010D
07/09/20 10:48
JDH
Cadmium [7440-43-9]^
0.00360
UD
mg/L
10
0.00360
0.0100
OG07035
EPA 6010D
07/09/20 10:48
JDH
Calcium [7440-70-2]^
5540
D
mg/L
10
0.390
1.00
OG07035
EPA 6010D
07/09/20 10:48
JDH
Copper[7440-50-8]^
0.637
D
mg/L
10
0.0160
0.100
OG07035
EPA 6010D
07/09/20 10:48
JDH
Lead [7439-92-1]^
0.0310
UD
mg/L
10
0.0310
0.100
OG07035
EPA 6010D
07/09/20 10:48
JDH
Magnesium [7439-95-4]^
77.4
D
mg/L
10
0.290
1.00
OG07035
EPA 6010D
07/09/20 10:48
JDH
Molybdenum [7439-98-7]^
0.0312
JD
mg/L
10
0.0250
0.100
OG07035
EPA 6010D
07/09/20 10:48
JDH
Nickel[7440-02-O]^
0.0680
JD
mg/L
10
0.0220
0.100
OG07035
EPA 6010D
07/09/20 10:48
JDH
Potassium [7440-09-7]^
591
D
mg/L
10
1.50
5.00
OG07035
EPA 6010D
07/09/20 10:48
JDH
Selenium [7782-49-2]^
0.0620
UD
mg/L
10
0.0620
0.100
OG07035
EPA 6010D
07/09/20 10:48
JDH
Sodium [7440-23-5]^
564
D
mg/L
10
4.00
5.00
OG07035
EPA 6010D
07/09/20 10:48
JDH
Zinc[7440-66-6]^
1.30
D
mg/L
10
0.0440
0.100
OG07035
EPA 6010D
07/09/20 10:48
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Ay Notes
Ammonia as N [7664-41-7]^
170
D
mg/L
500
22
50
OG13031
EPA 350.1
07/14/20 11:12
JAH
Biochemical Oxygen Demand^
18000
mg/L
1
2.0
2.0
OG08006
SM 5210 B-2011
07/08/20 09:55
JOC
Chemical Oxygen Demand^
44000
mg/L
80
800
800
OG10008
SM 5220D-2011
07/10/20 14:44
JOC
Nitrate as N [14797-55-8]
5.0
D
mg/L
20
0.82
2.0
[CALC]
EPA 353.2
07/13/20 13:55
JAH
Nitrate/Nitrite as N^
5.3
D
mg/L
20
0.82
2.0
OG13012
EPA 353.2
07/13/20 13:55
JAH
Nitrite as N [14797-65-0]^
0.29
mg/L
1
0.017
0.10
OG07037
EPA 353.2
07/08/20 09:58
JAH
Phosphorus[7723-14-O]^
820
D
mg/L
500
12
50
OG09005
EPA 365.4
07/10/20 12:43
JAH
Sodium Adsorption Ratio
2.06
[blank]
1
OG07035
CSU Method
07/09/20 16:01
JDH
Total Kjeldahl Nitrogen^
2500
D
mg/L
200
52
96
OG09006
EPA 351.2
07/15/20 10:05
JAH
Total Solids^
2.9
% by Volume
25
0.12
0.12
OG14046
SM 2540B-2011
07/14/20 17:29
DMJ
Total Suspended Solids^
8400
mg/L
200
500
500
OG14020
SM 2540D-2011
07/14/20 12:57
DMJ
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 13

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 0614O36 - EPA 747OA
Blank (OG14036-BLK3) Prepared: 07/14/2020 11:57 Analyzed: 07/16/2020 17:36
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Mercury 0.000150 U 0.000200 mg/L
LCS (OG14036-BS3) Prepared: 07/14/2020 11:57 Analyzed: 07/16/2020 17:38
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00487
0.000200
mg/L
0.00500
97
80-120
Matrix Spike (OG14036-MS3)
Prepared: 07/14/2020 11:57 Analyzed: 07/16/2020 17:44
Source: CDIOOIO-02
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00488
0.000200
mg/L
0.00500
0.000150 U
98
75-125
Matrix Spike Dup (OG34036-MSD1)
Prepared: 07/14/2020 11:57 Analyzed: 07/16/2020 17:46
Source: CD10010-02
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00477
0.000200
mg/L
0.00500
0.000150 U
95
75-125 2
25
Post Spike (OG14036-PS1)
Prepared: 07/14/2020 11:57 Analyzed: 07/16/2020 17:48
Source: CD10010-02
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
5.18
0.200
ug/L
5.00
0.0160
103
75-125
Metals (total recoverable) by EPA 6000/7000
Series Methods - Quality Control
Batch 0GO7O35 - EPA 3OO5A
Blank (OG07035-BLK3)
Prepared: 07/07/2020 14:45 Analyzed: 07/09/2020 10:03
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Aluminum
0.0420
U
0.100
mg/L
Arsenic
0.00760
U
0.0100
mg/L
Cadmium
0.000360
U
0.00100
mg/L
Calcium
0.0390
U
0.100
mg/L
Copper
0.00160
U
0.0100
mg/L
Lead
0.00310
U
0.0100
mg/L
Magnesium
0.0290
U
0.100
mg/L
Molybdenum
0.00250
U
0.0100
mg/L
Nickel
0.00220
U
0.0100
mg/L
Potassium
0.150
U
0.500
mg/L
Selenium
0.00620
U
0.0100
mg/L
Sodium
0.400
U
0.500
mg/L
Zinc
0.00440
U
0.0100
mg/L
LCS (OG07035-BSI)
Prepared: 07/07/2020 14:45 Analyzed: 07/09/2020 10:09
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Aluminum 2.01 0.100 mg/L 2.00 101 80-120
Arsenic 0.188 0.0100 mg/L 0.200 94 80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 13

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 0607O35 - EPA 3OO5A - Continued
LCS (OG07035-BS3) Continued Prepared: 07/07/2020 14:45 Analyzed: 07/09/2020 10:09
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Cadmium
0.0192
0.00100
mg/L
0.0200
96
80-120
Calcium
2.12
0.100
mg/L
2.00
106
80-120
Copper
0.191
0.0100
mg/L
0.200
96
80-120
Lead
0.193
0.0100
mg/L
0.200
97
80-120
Magnesium
2.08
0.100
mg/L
2.00
104
80-120
Molybdenum
0.189
0.0100
mg/L
0.200
95
80-120
Nickel
0.201
0.0100
mg/L
0.200
101
80-120
Potassium
10.3
0.500
mg/L
10.0
103
80-120
Selenium
0.195
0.0100
mg/L
0.200
97
80-120
Sodium
10.3
0.500
mg/L
10.0
103
80-120
Zinc
0.202
0.0100
mg/L
0.200
101
80-120
Matrix Spike (OG07035-MS1)
Prepared:
07/07/2020
14:45 Analyzed: 07/09/2020 10:11
Source: CD08647-02
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Aluminum
2.29
0.100
mg/L
2.00
0.123
108
75-125
Arsenic
0.190
0.0100
mg/L
0.200
0.00760 U
95
75-125
Cadmium
0.0188
0.00100
mg/L
0.0200
0.000360 U
94
75-125
Calcium
9.65
0.100
mg/L
2.00
7.54
106
75-125
Copper
0.188
0.0100
mg/L
0.200
0.00160 U
94
75-125
Lead
0.190
0.0100
mg/L
0.200
0.00310 U
95
75-125
Magnesium
4.84
0.100
mg/L
2.00
2.70
107
75-125
Molybdenum
0.188
0.0100
mg/L
0.200
0.00250 U
94
75-125
Nickel
0.197
0.0100
mg/L
0.200
0.00220 U
98
75-125
Potassium
12.9
0.500
mg/L
10.0
2.86
101
75-125
Selenium
0.189
0.0100
mg/L
0.200
0.00620 U
94
75-125
Sodium
21.1
0.500
mg/L
10.0
11.1
100
75-125
Zinc
0.199
0.0100
mg/L
0.200
0.00440 U
100
75-125
Matrix Spike Dup (OG07035-MSD1)
Prepared:
07/07/2020
14:45 Analyzed: 07/09/2020 10:14
Source: CD08647-02
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Aluminum
2.24
0.100
mg/L
2.00
0.123
106
75-125
2
20
Arsenic
0.186
0.0100
mg/L
0.200
0.00760 U
93
75-125
2
20
Cadmium
0.0187
0.00100
mg/L
0.0200
0.000360 U
93
75-125
0.9
20
Calcium
9.51
0.100
mg/L
2.00
7.54
98
75-125
1
20
Copper
0.186
0.0100
mg/L
0.200
0.00160 U
93
75-125
1
20
Lead
0.189
0.0100
mg/L
0.200
0.00310 U
94
75-125
0.7
20
Magnesium
4.71
0.100
mg/L
2.00
2.70
101
75-125
3
20
Molybdenum
0.187
0.0100
mg/L
0.200
0.00250 U
93
75-125
0.7
20
Nickel
0.196
0.0100
mg/L
0.200
0.00220 U
98
75-125
0.07
20
Potassium
12.8
0.500
mg/L
10.0
2.86
99
75-125
1
20
Selenium
0.191
0.0100
mg/L
0.200
0.00620 U
96
75-125
1
20
Sodium
20.7
0.500
mg/L
10.0
11.1
97
75-125
2
20
Zinc
0.200
0.0100
mg/L
0.200
0.00440 U
100
75-125
0.1
20
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 13

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 0607035 - EPA 3005A - Continued
Post Spike (OG07035-PSI)
Prepared: 07/07/2020 14:45 Analyzed: 07/09/2020 10:16
Source: CDO8647-02
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD Limit Notes
Aluminum
2.13
0.100
mg/L
2.00
0.123
101
80-120
Arsenic
0.192
0.0100
mg/L
0.200
0.00335
94
80-120
Cadmium
0.0190
0.00100
mg/L
0.0200
2.00E-5
95
80-120
Calcium
9.41
0.100
mg/L
2.00
7.54
93
80-120
Copper
0.192
0.0100
mg/L
0.200
0.000843
96
80-120
Lead
0.194
0.0100
mg/L
0.200
-0.00103
97
80-120
Magnesium
4.64
0.100
mg/L
2.00
2.70
97
80-120
Molybdenum
0.191
0.0100
mg/L
0.200
0.00158
95
80-120
Nickel
0.200
0.0100
mg/L
0.200
0.000859
100
80-120
Potassium
13.0
0.500
mg/L
10.0
2.86
101
80-120
Selenium
0.202
0.0100
mg/L
0.200
0.00575
98
80-120
Sodium
20.9
0.500
mg/L
10.0
11.1
98
80-120
Zinc
0.205
0.0100
mg/L
0.200
0.00163
102
80-120
Classical Chemistry Parameters - Quality Control
Batch 0GO7035 - EPA 3005A
Blank (OG07035-BLK3) Prepared: 07/07/2020 14:45 Analyzed: 07/09/2020 16:02
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Sodium Adsorption Ratio 0.00 U [blank]
Batch 0GO7037 - NO PREP
Blank (OG07037-BLK3) Prepared: 07/07/2020 15:15 Analyzed: 07/08/2020 09:51
Spike Source %REC RPD
Analvte Result Flaa POL Units Level Result %REC Limits RPD Limit Notes
Nitrite as N 0.017 U 0.10 mg/L
LCS (OG07037-BSI) Prepared: 07/07/2020 15:15 Analyzed: 07/08/2020 10:07
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrite as N
1.0
0.10
mg/L
1.00 104 90-110
Matrix Spike (OG07037-MSS)
Prepared: 07/07/2020 15:15 Analyzed: 07/08/2020 10:23
Source: CD09844-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrite as N
2.2
D
0.50
mg/L
1.00 1.1 108 90-110
Matrix Spike Dup (OG07037-MSD3)
Prepared: 07/07/2020 15:15 Analyzed: 07/08/2020 10:24
Source: CD09844-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrite as N
2.2
D
0.50
mg/L
1.00 1.1 109 90-110 0.5
10
Batch 0GO8006 - NO PREP
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OGOBOO6 - NO PREP - Continued
Blank (OG08006-BLK3)
Prepared & Analyzed: 07/08/2020 09:55
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Biochemical Oxygen Demand
2.0
U
2.0
mg/L
LCS (OG08006-BS3)
Prepared & Analyzed: 07/08/2020 09:55
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Biochemical Oxygen Demand
190
2.0
mg/L
198 97 85-115
Duplicate (0008006-DUPl)
Prepared & Analyzed: 07/08/2020 09:55
Source: CD05597-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Biochemical Oxygen Demand
4900
2.0
mg/L
5000 2
30
Batch 0GO9OO5 - Same
Blank (OG09005-BLK3)
Prepared: 07/09/2020 10:10 Analyzed: 07/10/2020 12:25
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
0.025
U
0.10
mg/L
LCS (OG09005-BS1)
Prepared: 07/09/2020 10:10 Analyzed: 07/10/2020 12:26
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
1.7
0.10
mg/L
1.60 104 80-120
Matrix Spike (OG09005-MS1)
Prepared: 07/09/2020 10:10 Analyzed: 07/10/2020 12:29
Source: CD06449-02
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
1.0
0.10
mg/L
0.640 0.028 154 80-120
QM-07
Matrix Spike Dup (OG09005-MSD1)
Prepared: 07/09/2020 10:10 Analyzed: 07/10/2020 12:30
Source: CD06449-02
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
0.66
0.10
mg/L
0.640 0.028 99 80-120 43
25
QM-11
Batch 0GO9OO6 - Same
Blank (OG09006-BLK3) Prepared: 07/09/2020 10:10 Analyzed: 07/15/2020 09:43
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Kjeldahl Nitrogen
0.26 U
0.48
mg/L
LCS (OG09006-BSI)
Prepared: 07/09/2020 10:10 Analyzed: 07/15/2020 09:45
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Kjeldahl Nitrogen
13
0.48
mg/L
12.0 106 90-110
FINAL
This report relates only to
the sample as received by the
laboratory, and may only be reproduced in full.
Page 8 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 0609006 - Same - Continued
Matrix Spike (OG09006-MSS)
Prepared: 07/09/2020 10:10 Analyzed: 07/15/2020 09:48
Source: CD06449-02
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Kjeldahl Nitrogen
5.5
0.48
mg/L
4.80 0.72 100 90-110
Matrix Spike (OG09006-MS2)
Prepared: 07/09/2020 10:10 Analyzed: 07/15/2020 10:31
Source: CD08659-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Kjeldahl Nitrogen
6.7
0.48
mg/L
4.80 2.3 92 90-110
Matrix Spike Dup (OG09006-MSD3)
Prepared: 07/09/2020 10:10 Analyzed: 07/15/2020 09:50
Source: CD06449-02
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Kjeldahl Nitrogen
5.9
0.48
mg/L
4.80 0.72 108 90-110 7
10
Batch OG10008 - Same
Blank (OG10008-BLK3) Prepared: 07/10/2020 09:10 Analyzed: 07/10/2020 14:44
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Chemical Oxygen Demand 10 U 10 mg/L
LCS (OG30008-BS3) Prepared: 07/10/2020 09:10 Analyzed: 07/10/2020 14:44
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Chemical Oxygen Demand
520
10
mg/L
500
105
90-110
Matrix Spike (0G30008-MS3)
Prepared: 07/10/2020 09:10 Analyzed: 07/10/2020 14:44
Source: CDO8765-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Chemical Oxygen Demand
860
10
mg/L
526
310
104
90-110
Matrix Spike Dup (OG10008-MSD1)
Prepared: 07/10/2020 09:10 Analyzed: 07/10/2020 14:44
Source: CDO8765-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Chemical Oxygen Demand
840
10
mg/L
526
310
101
90-110 2
5
Batch OG13012 - NO PREP
Blank (OG13012-BLK3) Prepared: 07/13/2020 09:58 Analyzed: 07/13/2020 13:23
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrate/Nitrite as N
0.041 U
0.10
mg/L
LCS (OG13012-BSI)
Prepared: 07/13/2020 09:58 Analyzed: 07/13/2020 13:24
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrate/Nitrite as N
1.3
0.10
mg/L
1.25 102 90-110
FINAL
This report relates only to
the sample as received by the
laboratory, and may only be reproduced in full.
Page 9 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 0613012 - NO PREP - Continued
Matrix Spike (OG33012-MSS)
Prepared: 07/13/2020 09:58 Analyzed: 07/13/2020 13:32
Source: CDO8647-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrate/Nitrite as N
0.57
0.10
mg/L
0.521 0.043 101 90-110
Matrix Spike (OG13012-MS2)
Prepared: 07/13/2020 09:58 Analyzed: 07/13/2020 13:37
Source: CD08711-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrate/Nitrite as N
0.62
0.10
mg/L
0.521 0.048 109 90-110
Matrix Spike Dup (OG13012-MSDI)
Prepared: 07/13/2020 09:58 Analyzed: 07/13/2020 13:34
Source: CDO8647-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrate/Nitrite as N
0.57
0.10
mg/L
0.521 0.043 100 90-110 1
10
Batch OG13031 - NO PREP
Blank (OG13031-BLK3)
Prepared: 07/13/2020 14:56 Analyzed: 07/13/2020 17:30
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
0.045
U
0.10
mg/L
Blank (OG13031-BLK2)
Prepared: 07/13/2020 14:56 Analyzed: 07/14/2020 10:41
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
0.045
U
0.10
mg/L
LCS (OG13031-BSI)
Prepared: 07/13/2020 14:56 Analyzed: 07/13/2020 17:32
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
1.1
0.10
mg/L
1.01 105 90-110
LCS (OG13031-BS2)
Prepared: 07/13/2020 14:56 Analyzed: 07/14/2020 10:43
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
1.1
0.10
mg/L
1.01 104 90-110
Matrix Spike (OG33031-MS1)
Prepared: 07/13/2020 14:56 Analyzed: 07/13/2020 17:35
Source: CD06449-02
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
0.37
0.10
mg/L
0.393 0.045 U 94 90-110
Matrix Spike (OG13031-MS2)
Prepared: 07/13/2020 14:56 Analyzed: 07/13/2020 17:44
Source: CDOSS90-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
5.3
E
0.10
mg/L
0.393 4.9 97 90-110
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 0613031 - NO PREP - Continued
Matrix Spike Dup (OG33031-MSD1) Prepared: 07/13/2020 14:56 Analyzed: 07/13/2020 17:37
Source: CD06449-02
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Ammonia as N 0.37 0.10 mg/L 0.393 0.045 U 95 90-110 0.9 10
Batch OG14020 - NO PREP
Blank (OG14020-BLK3) Prepared & Analyzed: 07/14/2020 12:57
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Total Suspended Solids
2.5
U
2.5
mg/L
LCS (OG34020-BSI)
Prepared & Analyzed: 07/14/2020 12:57
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Total Suspended Solids
91
2.5
mg/L
100 91 80-120
Duplicate (OG34020-DUPl)
Prepared & Analyzed: 07/14/2020 12:57
Source: CD06449-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Total Suspended Solids
210
50
mg/L
210
0
20
Duplicate (OG34020-DUP2)
Prepared & Analyzed: 07/14/2020 12:57
Source: CD08641-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Total Suspended Solids
640
120
mg/L
760
17
20
Batch 04G14046 - NO PREP
Blank (OG14046-BLK3)
Prepared & Analyzed: 07/14/2020 17:29
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Total Solids
0.0050
U
0.0050
% by Volume
LCS (OG14046-BS3)
Prepared & Analyzed: 07/14/2020 17:29
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Total Solids
1100
50
mg/L
1100 99 80-120
Duplicate (OG34046-DUPl)
Prepared & Analyzed: 07/14/2020 17:29
Source: CD09844-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Total Solids
0.22
0.0050
% by Volume
0.22
0.09
20
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 13

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 13

ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD
www.encolabs.com
CQ
10775 Central Porl Dr. 41310 Executive Park Court, Suite 111
102-A Woodwinds Industrial CL
Orlando, FL 32824 .Jacksonville, FL 32216-6069
Cary, NC
27511
[phone] Fax [phone] [phone] Fax [phone]
[phone] Fax [phone]
Prig of
Client Name
Project Number
Requested Analyses
Requested Turnaround
Times
N
0Address
Project Name/ esc
L%
Note :Rush requests subject to
? P ha el h Road
Monthly- Week One - SBM
is
acceptance by the facility
CitylsTfLp
PO N I Billing into
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Franklinton NC 27525
38O 466333
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Reporting Contact
w
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N
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91 g 494_30Q0
Scott Creech
LO
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Expedited
Sampler(s) Name, Affiliation (Print)
Billing Contact
2
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Due
Accounts Payable
q
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Site Location ITime Tone
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Preservation (See Codes) (Combine as necessary)
Collection Matrix Total N or
Ilem N Sample ID (Feld identification) Collection Date Time Commpg! Grab (see codes) Containers
Sample Comments
o
'SD
—Total # of Containers
Sampie Kit Prepared By Dal&7ime Relinquished By
Datefrime
Recei d By
Dalefrime
@
—7y2v
x7
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CommentelSpecial Reporting Requirements
Relinquished By
DaIWTime
Rec ' d By
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Da ime
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Relinquished By
Datefrme
Received By
Dat ITtme
Cooler P's & Temps on Receipt
Cond:dKUReceipl
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Matrix: GW-Groundwater SO -Soil DW-Drinking Water SE -Sediment SW -Surface Water WW-Wastewater A -Air O-Other (detail in comments) Preservation: I -Ice H-HCl N-HNO3 S-H2SO4 NO-NaOH O Olher (detail In comments)
Note: All samples submitted to ENCO Lags are in accordance with the terms and conditions listed on the reverse of this form, unless prior written agreements exist

Sample Preservation Verification
ENCO Cary
Work Order: CD09845 Project:
Client: Novozymes North America (N0008) Project #:
Logged in: 07-Jul-20 10:19 _ Logged By:
Preservation Check Performed By: ' ip
CDO9845-01
Monthly - Week One - SBM
[none]
John C King
Date/Time:
Cant
Type
Pres (pH)
pH Checked 1
pH Adjusted Date/Time
Reagent Used/Comments
Requirement
In Control
Adjusted
D
25OmLP+H2SO4
<2
Y /LN� / NA
'Y t N / NA
i-y7 L
E
250mLP+HNO3
t2
Y I / NA
Y 1 / NA
�1L /yi7ic
1
2
Regnant Name in
V
L-J Z S-bj
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pH Strip ID: N" -13sS
Reagent Name ID
3
4
Reacient Name ID
5
6
C:IELMNTIPrintlwko_PreservationCheck. rpt Page 1 of

2�SQ pCCgF ENCO Laboratories
9e0
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Thursday, September 3, 2020
Novozymes North America (N0008)
Attn: Scott Creech
77 Perry Chapel Church Road
Franklinton, NC 27525
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: Monthly - Week One - SBM
ENCO Workorder(s): CD12061
Dear Scott Creech,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, August 4, 2020.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
0"CLC---�0
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 14

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: SBM
Lab ID: CD12061-01
Sampled: 08/03/20 22:50
Received: 08/04/20 09:45
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
CSU Method
NO PREP
04/29/23
08/05/20
10:30
08/10/20
14:04
EPA 350.1
NO PREP
08/31/20
08/13/20
08:43
08/13/20
11:25
EPA 351.2
Same
08/31/20
08/07/20
09:03
08/11/20
13:49
EPA 353.2
NO PREP
08/05/20
22:50
08/04/20
13:42
08/04/20
14:47
EPA 353.2
[CALC]
08/05/20
22:50
08/10/20
08:37
08/10/20
11:57
EPA 353.2
NO PREP
08/31/20
08/10/20
08:37
08/10/20
11:57
EPA 6010D
EPA 3005A
01/30/21
08/05/20
10:30
08/10/20
10:14
EPA 7470A
EPA 7470A
08/31/20
08/06/20
13:23
08/07/20
12:51
SM 2540B-2011
NO PREP
08/10/20
08/06/20
15:42
08/06/20
15:42
SM 254OD-2011
NO PREP
08/10/20
08/06/20
15:07
08/06/20
15:07
SM 5210 B-2011
NO PREP
08/05/20
22:50
08/05/20
10:11
08/05/20
10:11
SM 5220D-2011
Same
08/31/20
08/07/20
09:05
08/07/20
11:45
Client ID: SBM
Lab ID: CD12061-01RE1
Sampled: 08/03/20 22:50
Received: 08/04/20 09:45
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
EPA 365.4
Same
08/31/20
08/07/20
09:03
08/14/20
13:43
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 14

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SAMPLE DETECTION SUMMARY
Client ID: SBM
Lab ID:
CD12061-01
Analvte
Results
Flag
MDL
PQL
Units
Method Notes
Aluminum - Total
215
0.420
1.00
mg/L
EPA 6010D
Ammonia as N
43
D
4.0
9.0
mg/L
EPA 350.1
Biochemical Oxygen Demand
5000
2.0
2.0
mg/L
SM 5210 B-2011
Calcium - Total
7560
0.390
1.00
mg/L
EPA 6010D
Chemical Oxygen Demand
21000
400
400
mg/L
SM 5220D-2011
Copper - Total
0.851
0.0160
0.100
mg/L
EPA 6010D
Magnesium - Total
111
B
0.290
1.00
mg/L
EPA 6010D QB-01
Molybdenum - Total
0.0549
3
0.0250
0.100
mg/L
EPA 6010D
Nickel - Total
0.147
0.0220
0.100
mg/L
EPA 6010D
Nitrate as N
1.8
D
0.41
1.0
mg/L
EPA 353.2
Nitrate/Nitrite as N
2.3
D
0.41
1.0
mg/L
EPA 353.2
Nitrite as N
0.46
0.017
0.10
mg/L
EPA 353.2
Potassium - Total
693
1.50
5.00
mg/L
EPA 6010D
Sodium - Total
276
4.00
5.00
mg/L
EPA 6010D
Sodium Adsorption Ratio
0.862
[blank]
CSU Method
Total Kjeldahl Nitrogen
1400
D 52
96
mg/L
EPA 351.2
Total Solids
4.8
0.12
0.12
% by Volume
SM 254OB-2011
Total Suspended Solids
39000
500
500
mg/L
SM 2540D-2011
Zinc - Total
2.08
0.0440
0.100
mg/L
EPA 6010D
Client ID: SBM
Lab ID:
CD32061-01RE3
Analvte
Results
Flag MDL
PQL
Units
Method Notes
Phosphorus
1100
D 25
100
mg/L
EPA 365.4
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 14

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ANALYTICAL RESULTS
Description: SBM Lab Sample ID:CD12061-01 Received: 08/04/20 09:45
Matrix: Sludge Sampled:08/03/20 22:50 Work Order: CD12061
Project: Monthly - Week One - SBM Sampled By: John Caleb Hilliard Jr.
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
Mercury [7439-97-6]^
0.00300
U
mg/L
20
0.00300
0.00400
OH06035
EPA 7470A
08/07/20 12:51
KAH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Ay
Notes
Aluminum [7429-90-5]^
215
mg/L
10
0.420
1.00
OH05023
EPA 6010D
08/10/20 10:14
JDH
Arsenic[7440-38-2]^
0.0760
U
mg/L
10
0.0760
0.100
OH05023
EPA 6010D
08/10/20 10:14
JDH
Cadmium [7440-43-9]^
0.00360
U
mg/L
10
0.00360
0.0100
OH05023
EPA 6010D
08/10/20 10:14
JDH
Calcium [7440-70-2]^
7560
mg/L
10
0.390
1.00
OH05023
EPA 6010D
08/10/20 10:14
JDH
Copper[7440-50-8]^
0.851
mg/L
10
0.0160
0.100
OH05023
EPA 6010D
08/10/20 10:14
JDH
Lead [7439-92-1]^
0.0310
U
mg/L
10
0.0310
0.100
OH05023
EPA 6010D
08/10/20 10:14
JDH
Magnesium [7439-95-4]^
111
B
mg/L
10
0.290
1.00
OH05023
EPA 6010D
08/10/20 10:14
JDH
QB-01
Molybdenum [7439-98-7]^
0.0549
J
mg/L
10
0.0250
0.100
OH05023
EPA 6010D
08/10/20 10:14
JDH
Nickel[7440-02-O]^
0.147
mg/L
10
0.0220
0.100
OH05023
EPA 6010D
08/10/20 10:14
JDH
Potassium [7440-09-7]^
693
mg/L
10
1.50
5.00
OH05023
EPA 6010D
08/10/20 10:14
JDH
Selenium [7782-49-2]^
0.0620
U
mg/L
10
0.0620
0.100
OH05023
EPA 6010D
08/10/20 10:14
JDH
Sodium [7440-23-5]^
276
mg/L
10
4.00
5.00
OH05023
EPA 6010D
08/10/20 10:14
JDH
Zinc[7440-66-6]^
2.08
mg/L
10
0.0440
0.100
OH05023
EPA 6010D
08/10/20 10:14
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Ay
Notes
Ammonia as N [7664-41-7]^
43
D
mg/L
90
4.0
9.0
OH13007
EPA 350.1
08/13/20 11:25
JAH
Biochemical Oxygen Demand^
5000
mg/L
1
2.0
2.0
OH05010
SM 5210 B-2011
08/05/20 10:11
JOC
Chemical Oxygen Demand^
21000
mg/L
40
400
400
OH07004
SM 5220D-2011
08/07/20 11:45
JOC
Nitrate as N [14797-55-8]
1.8
D
mg/L
10
0.41
1.0
[CALC]
EPA 353.2
08/10/20 11:57
JAH
Nitrate/Nitrite as N^
2.3
D
mg/L
10
0.41
1.0
OH10006
EPA 353.2
08/10/20 11:57
JAH
Nitrite as N [14797-65-0]^
0.46
mg/L
1
0.017
0.10
OH04031
EPA 353.2
08/04/20 14:47
JAH
Phosphorus[7723-14-O]^
1100
D
mg/L
1000
25
100
OH06032
EPA 365.4
08/14/20 13:43
JAH
Sodium Adsorption Ratio
0.862
[blank]
1
OH05023
CSU Method
08/10/20 14:04
JDH
Total Kjeldahl Nitrogen^
1400
D
mg/L
200
52
96
OH06031
EPA 351.2
08/11/20 13:49
JAH
Total Solids^
4.8
% by Volume
25
0.12
0.12
OH06024
SM 2540B-2011
08/06/20 15:42
DMJ
Total Suspended Solids^
39000
mg/L
200
500
500
OH06022
SM 2540D-2011
08/06/20 15:07
DMJ
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 14

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch OHO6O35 - EPA 747OA
Blank (OH06035-BLKI) Prepared: 08/06/2020 13:23 Analyzed: 08/07/2020 12:23
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Mercury 0.000150 U 0.000200 mg/L
LCS (OH06035-BS1) Prepared: 08/06/2020 13:23 Analyzed: 08/07/2020 12:30
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result %REC
Limits RPD
Limit
Notes
Mercury
0.00536
0.000200
mg/L
0.00500
107
80-120
Matrix Spike (OH06035-MS3)
Prepared: 08/06/2020 13:23 Analyzed: 08/07/2020 12:35
Source: CD12477-09
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result %REC
Limits RPD
Limit
Notes
Mercury
0.00512
0.000200
mg/L
0.00500
0.000150 U 102
75-125
Matrix Spike Dup (OH06035-MSD1)
Prepared: 08/06/2020 13:23 Analyzed: 08/07/2020 12:37
Source: CD12477-09
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result %REC
Limits RPD
Limit
Notes
Mercury
0.00479
0.000200
mg/L
0.00500
0.000150 U 96
75-125 7
25
Post Spike (OH06035-PS3)
Prepared: 08/06/2020 13:23 Analyzed: 08/07/2020 12:39
Source: CD12477-09
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result %REC
Limits RPD
Limit
Notes
Mercury
5.54
0.200
ug/L
5.00
-0.0730 111
75-125
Metals (total recoverable) by EPA 6000/7000
Series Methods - Quality Control
Batch OHO5O23 - EPA 3OO5A
Blank (OH05023-BLK1)
Prepared: 08/05/2020 10:30 Analyzed: 08/10/2020 09:30
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Aluminum
0.0420
U
0.100
mg/L
Arsenic
0.00760
U
0.0100
mg/L
Cadmium
0.000360
U
0.00100
mg/L
Calcium
0.0390
U
0.100
mg/L
Copper
0.00160
U
0.0100
mg/L
Lead
0.00310
U
0.0100
mg/L
Magnesium
0.0500
3
0.100
mg/L
Molybdenum
0.00250
U
0.0100
mg/L
Nickel
0.00220
U
0.0100
mg/L
Potassium
0.150
U
0.500
mg/L
Selenium
0.00620
U
0.0100
mg/L
Sodium
0.400
U
0.500
mg/L
Zinc
0.00440
U
0.0100
mg/L
Blank (OH05023-BLK2)
Prepared: 08/05/2020 10:30 Analyzed: 08/10/2020 09:33
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Aluminum 0.0420 U 0.100 mg/L
Arsenic 0.00760 U 0.0100 mg/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 14

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch OHO5O23 - EPA 3OO5A - Continued
Blank (OH05023-BLK2) Continued Prepared: 08/05/2020 10:30 Analyzed: 08/10/2020 09:33
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units Level Result %REC Limits RPD Limit Notes
Cadmium
0.000360
U
0.00100
mg/L
Calcium
0.0390
U
0.100
mg/L
Copper
0.00160
U
0.0100
mg/L
Lead
0.00310
U
0.0100
mg/L
Magnesium
0.0495
3
0.100
mg/L
Molybdenum
0.00250
U
0.0100
mg/L
Nickel
0.00220
U
0.0100
mg/L
Potassium
0.150
U
0.500
mg/L
Selenium
0.00620
U
0.0100
mg/L
Sodium
0.400
U
0.500
mg/L
Zinc
0.00440
U
0.0100
mg/L
LCS (OH05023-BSI)
Prepared: 08/05/2020 10:30 Analyzed: 08/10/2020 09:42
Spike
Source
%REC RPD
Analvte
Result
Flaq POL
Units
Level
Result %REC
Limits RPD Limit Notes
Aluminum
2.01
0.100
mg/L
2.00
100
80-120
Arsenic
0.187
0.0100
mg/L
0.200
93
80-120
Cadmium
0.0187
0.00100
mg/L
0.0200
94
80-120
Calcium
2.00
0.100
mg/L
2.00
100
80-120
Copper
0.182
0.0100
mg/L
0.200
91
80-120
Lead
0.184
0.0100
mg/L
0.200
92
80-120
Magnesium
2.02
B 0.100
mg/L
2.00
101
80-120
Molybdenum
0.186
0.0100
mg/L
0.200
93
80-120
Nickel
0.193
0.0100
mg/L
0.200
97
80-120
Potassium
10.4
0.500
mg/L
10.0
104
80-120
Selenium
0.187
0.0100
mg/L
0.200
94
80-120
Sodium
10.4
0.500
mg/L
10.0
104
80-120
Zinc
0.195
0.0100
mg/L
0.200
97
80-120
Matrix Spike (OH05023-MS1)
Prepared:
08/05/2020 10:30 Analyzed: 08/10/2020 09:45
Source: CD12456-01
Spike
Source
%REC RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD Limit Notes
Aluminum
1.99
0.100
mg/L
2.00
0.0955
95
75-125
Arsenic
0.189
0.0100
mg/L
0.200
0.00760 U
94
75-125
Cadmium
0.0183
0.00100
mg/L
0.0200
0.000360 U
91
75-125
Calcium
28.5
0.100
mg/L
2.00
26.1
121
75-125
Copper
0.182
0.0100
mg/L
0.200
0.00160 U
91
75-125
Lead
0.182
0.0100
mg/L
0.200
0.00310 U
91
75-125
Magnesium
13.7
B 0.100
mg/L
2.00
11.6
109
75-125
Molybdenum
0.191
0.0100
mg/L
0.200
0.00445
93
75-125
Nickel
0.192
0.0100
mg/L
0.200
0.00220 U
96
75-125
Potassium
50.5
0.500
mg/L
10.0
39.9
106
75-125
Selenium
0.184
0.0100
mg/L
0.200
0.00620 U
92
75-125
Sodium
87.6
0.500
mg/L
10.0
75.4
123
75-125
Zinc
0.200
0.0100
mg/L
0.200
0.00452
98
75-125
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 14

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch OHO5O23 - EPA 3OO5A - Continued
Matrix Spike Dup (OH05023-MSD3)
Prepared: 08/05/2020 10:30 Analyzed: 08/10/2020 09:47
Source: CD12456-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit
Notes
Aluminum
1.99
0.100
mg/L
2.00
0.0955
95
75-125
0.5
20
Arsenic
0.187
0.0100
mg/L
0.200
0.00760 U
93
75-125
1
20
Cadmium
0.0182
0.00100
mg/L
0.0200
0.000360 U
91
75-125
0.2
20
Calcium
28.7
0.100
mg/L
2.00
26.1
130
75-125
0.7
20
QM-07
Copper
0.182
0.0100
mg/L
0.200
0.00160 U
91
75-125
0.2
20
Lead
0.182
0.0100
mg/L
0.200
0.00310 U
91
75-125
0.05
20
Magnesium
13.7 B
0.100
mg/L
2.00
11.6
106
75-125
0.4
20
Molybdenum
0.189
0.0100
mg/L
0.200
0.00445
92
75-125
1
20
Nickel
0.190
0.0100
mg/L
0.200
0.00220 U
95
75-125
0.8
20
Potassium
50.8
0.500
mg/L
10.0
39.9
109
75-125
0.7
20
Selenium
0.179
0.0100
mg/L
0.200
0.00620 U
89
75-125
3
20
Sodium
87.8
0.500
mg/L
10.0
75.4
124
75-125
0.1
20
Zinc
0.199
0.0100
mg/L
0.200
0.00452
97
75-125
0.9
20
Post Spike (OH05023-PS1)
Prepared: 08/05/2020 10:30 Analyzed: 08/10/2020 09:49
Source: CD12456-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit
Notes
Aluminum
2.12
0.100
mg/L
2.00
0.0955
101
80-120
Arsenic
0.206
0.0100
mg/L
0.200
0.00163
102
80-120
Cadmium
0.0198
0.00100
mg/L
0.0200
1.62E-6
99
80-120
Calcium
27.6
0.100
mg/L
2.00
26.1
76
80-120
QM-08
Copper
0.194
0.0100
mg/L
0.200
-0.000110
97
80-120
Lead
0.197
0.0100
mg/L
0.200
0.000631
98
80-120
Magnesium
13.3 B
0.100
mg/L
2.00
11.6
88
80-120
Molybdenum
0.205
0.0100
mg/L
0.200
0.00445
100
80-120
Nickel
0.208
0.0100
mg/L
0.200
0.000310
104
80-120
Potassium
49.4
0.500
mg/L
10.0
39.9
94
80-120
Selenium
0.205
0.0100
mg/L
0.200
-0.00230
102
80-120
Sodium
85.0
0.500
mg/L
10.0
75.4
96
80-120
Zinc
0.217
0.0100
mg/L
0.200
0.00452
106
80-120
Classical Chemistry Parameters - Quality Control
Batch OHO4O31 - NO PREP
Blank (OH04031-BLK1) Prepared: 08/04/2020 13:42 Analyzed: 08/04/2020 14:41
Spike Source %REC RPD
Analvte Result Flaa POL Units Level Result %REC Limits RPD Limit Notes
Nitrite as N 0.017 U 0.10 mg/L
LCS (OH04031-BSI) Prepared: 08/04/2020 13:42 Analyzed: 08/04/2020 15:21
Spike Source %REC
RPD
Analvte
Result Flaq POL Units Level Result %REC Limits RPD
Limit Notes
Nitrite as N
1.0 0.10 mg/L 1.00 104 90-110
Matrix Spike (OH04031-MS1)
Prepared: 08/04/2020 13:42 Analyzed: 08/04/2020 14:42
Source: CD12060-01
Spike Source %REC
RPD
Analvte
Result Flaq POL Units Level Result %REC Limits RPD
Limit Notes
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 7 of 14

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OH04031 - NO PREP - Continued
Matrix Spike (OH04031-MS3) Continued
Prepared: 08/04/2020 13:42 Analyzed: 08/04/2020 14:42
Source: CD12060-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrite as N
1.2
0.10
mg/L
1.00 0.25 97 90-110
Matrix Spike Dup (OH04031-MSD3)
Prepared: 08/04/2020 13:42 Analyzed: 08/04/2020 14:43
Source: CD12060-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrite as N
1.2
0.10
mg/L
1.00 0.25 98 90-110 1
10
Batch OH05010 - NO PREP
Blank (OH05010-BLKi)
Prepared & Analyzed: 08/05/2020 10:11
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Biochemical Oxygen Demand
2.0
U
2.0
mg/L
LCS (011-1105010-BSI)
Prepared & Analyzed: 08/05/2020 10:11
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Biochemical Oxygen Demand
170
2.0
mg/L
198 86 85-115
Duplicate (OH05030-DUPl)
Prepared & Analyzed: 08/05/2020 10:11
Source: CD06898-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Biochemical Oxygen Demand
2.0
U
2.0
mg/L
2.0 U
30
Batch OH05023 - EPA 3005A
Blank (OH05023-BLKi)
Prepared: 08/05/2020 10:30 Analyzed: 08/10/2020 14:05
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Sodium Adsorption Ratio
0.00
U
[blank]
Blank (OH05023-BLK2)
Prepared: 08/05/2020 10:30 Analyzed: 08/10/2020 14:05
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Sodium Adsorption Ratio
0.00
U
[blank]
Batch OH06022 - NO PREP
Blank (OH06022-BLK1)
Prepared & Analyzed: 08/06/2020 15:07
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Total Suspended Solids
2.5
U
2.5
mg/L
LCS (OH06022-BS1)
Prepared & Analyzed: 08/06/2020 15:07
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Total Suspended Solids
97
2.5
mg/L
100 97 80-120
FINAL
This report relates only to
the sample as received by the
laboratory, and may only be reproduced in full.
Page 8 of 14

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OHO6O22 - NO PREP - Continued
Duplicate (OH06022-DUPl)
Prepared & Analyzed: 08/06/2020 15:07
Source: CD06451-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Total Suspended Solids
240
50
mg/L
220
5
20
Duplicate (OH06022-DUP2)
Prepared & Analyzed: 08/06/2020 15:07
Source: CD12060-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Total Suspended Solids
770
50
mg/L
730
5
20
Batch OHO6O24 - NO PREP
Blank (OH06024-BLKi)
Prepared & Analyzed: 08/06/2020 15:42
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Solids
0.0050
U
0.0050
% by Volume
LCS (OH06024-BSI)
Prepared & Analyzed: 08/06/2020 15:42
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Solids
1100
50
mg/L
1100 100 80-120
Duplicate (OH06024-DUPl)
Prepared & Analyzed: 08/06/2020 15:42
Source: CD12060-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Solids
0.33
0.010
% by Volume
0.34 3
20
Batch OHO6O31 - Same
Blank (OH06031-BLKi)
Prepared: 08/07/2020 09:03 Analyzed: 08/11/2020 12:14
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
0.26
U
0.48
mg/L
LCS (OH06031-BSI)
Prepared: 08/07/2020 09:03 Analyzed: 08/11/2020 12:38
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
12
0.48
mg/L
12.0 103 90-110
Matrix Spike (OH06031-MS3)
Prepared: 08/07/2020 09:03 Analyzed: 08/11/2020 12:41
Source: CD08661-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
49
D
4.8
mg/L
4.80 41 164 90-110
QM-07
Matrix Spike (OH06031-MS2)
Prepared: 08/07/2020 09:03 Analyzed: 08/11/2020 12:46
Source: CD10644-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
53
D
2.4
mg/L
4.80 50 56 90-110
QM-07
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 14

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OH06031 - Same - Continued
Matrix Spike Dup (OH06031-MSD3) Prepared: 08/07/2020 09:03 Analyzed: 08/11/2020 12:43
Source: CDO8661-01
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Kjeldahl Nitrogen 44 D 4.8 mg/L 4.80 41 59 90-110 11 10 QM-07,
QM-11
Batch OH06032 - Same
Blank (OH06032-BLK1)
Prepared: 08/07/2020 09:03 Analyzed: 08/12/2020 13:30
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
0.025
U
0.10
mg/L
LCS (OH06032-BSI)
Prepared: 08/07/2020 09:03 Analyzed: 08/12/2020 13:48
Spike Source %REC
RPD
Analvte
Result
Flaa
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
1.6
0.10
mg/L
1.60 103 80-120
Matrix Spike (OH06032-MS1)
Prepared: 08/07/2020 09:03 Analyzed: 08/12/2020 13:51
Source: CDO8661-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
9.7
D
1.0
mg/L
0.640 9.1 90 80-120
Matrix Spike Dup (OH06032-MSD1)
Prepared: 08/07/2020 09:03 Analyzed: 08/12/2020 13:52
Source: CD08661-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
9.7
D
1.0
mg/L
0.640 9.1 94 80-120 0.2
25
Batch OH07004 - Same
Blank (OH07004-BLK1)
Prepared: 08/07/2020 09:05 Analyzed: 08/07/2020 11:45
Spike Source %REC
RPD
Analvte
Result
Flaa
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Chemical Oxygen Demand
10
U
10
mg/L
LCS (OH07004-BSI)
Prepared: 08/07/2020 09:05 Analyzed: 08/07/2020 11:45
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chemical Oxygen Demand
520
10
mg/L
500 104 90-110
Matrix Spike (OH07004-MS3)
Prepared: 08/07/2020 09:05 Analyzed: 08/07/2020 11:45
Source: CD10607-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chemical Oxygen Demand
640
10
mg/L
500 130 101 90-110
Matrix Spike Dup (OH07004-MSD3)
Prepared: 08/07/2020 09:05 Analyzed: 08/07/2020 11:45
Source: CD10607-01
Spike Source %REC
RPD
Analvte
Result
Flaa
Q
Units
Level Result %REC Limits RPD
Limit
Notes
Chemical Oxygen Demand
600
10
mg/L
500 130 95 90-110 5
5
Batch OH10006 - NO PREP
FINAL This
report relates only to the sample as received by the
laboratory, and may only be reproduced in full.
Page 10 of 14

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OH1OOO6 - NO PREP - Continued
Blank (OH10006-BLKI) Prepared: 08/10/2020 08:37 Analyzed: 08/10/2020 11:25
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes
Nitrate/Nitrite as N 0.041 U 0.10 mg/L
LCS (OH10006-BS1) Prepared: 08/10/2020 08:37 Analyzed: 08/10/2020 11:27
Spike Source O/oREC
RPD
Analvte
Result
Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
1.2
0.10
mg/L
1.25 98 90-110
Matrix Spike (OH10006-MS3)
Prepared: 08/10/2020 08:37 Analyzed: 08/10/2020 11:30
Source: CD12060-01
Spike Source O/oREC
RPD
Analvte
Result
Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
1.1
0.10
mg/L
0.521 0.53 103 90-110
Matrix Spike (OH10006-MS2)
Prepared: 08/10/2020 08:37 Analyzed: 08/10/2020 11:36
Source: CD12060-02
Spike Source O/oREC
RPD
Analvte
Result
Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
0.56
0.10
mg/L
0.521 0.091 90 90-110
Matrix Spike Dup (OH10006-MSD3)
Prepared: 08/10/2020 08:37 Analyzed: 08/10/2020 11:32
Source: CD12060-01
Spike Source O/oREC
RPD
Analvte
Result
Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
1.0
0.10
mg/L
0.521 0.53 101 90-110 0.9
10
Batch OH13OO7 - NO PREP
Blank (OH13007-BLKI) Prepared: 08/13/2020 08:43 Analyzed: 08/13/2020 10:50
Spike Source O/oREC RPD
Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes
Ammonia as N 0.045 U 0.10 mg/L
LCS (OH13007-BSI) Prepared: 08/13/2020 08:43 Analyzed: 08/13/2020 10:52
Spike Source O/oREC
RPD
Analvte
Result Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit Notes
Ammonia as N
1.0
0.10
mg/L
1.01 102 90-110
Matrix Spike (OH13007-MS3)
Prepared: 08/13/2020 08:43 Analyzed: 08/13/2020 10:56
Source: CD12032-01
Spike Source O/oREC
RPD
Analvte
Result Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit Notes
Ammonia as N
0.39
0.10
mg/L
0.393 0.045 U 98 90-110
Matrix Spike (OH13007-MS2)
Prepared: 08/13/2020 08:43 Analyzed: 08/13/2020 11:01
Source: CD12035-01
Spike Source O/oREC
RPD
Analvte
Result Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit Notes
Ammonia as N
0.36
0.10
mg/L
0.393 0.045 U 90 90-110
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 14

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OH13OO7 - NO PREP - Continued
Matrix Spike Dup (OH13007-MSD3) Prepared: 08/13/2020 08:43 Analyzed: 08/13/2020 10:57
Source: CD12032-01
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Ammonia as N 0.38 0.10 mg/L 0.393 0.045 U 96 90-110 2 10
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 14

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QB-01 The method blank had a positive result for the analyte; however, the concentration in the method blank is
less than 10% of the sample result. There is minimal impact to the data.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 14

ENVIRONMENTAL. CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com
C 10775 Central Port Dr. 4810 Executive Park Court, Suite 111 102-A Woodwinds Indusinal CL
Orlando, FL 32824 Jacksonville, FL 32216-BOW Cary, NC 27511
(407) B26-5314 Fax [phone] [phone] Fax [phone] [phone] Fax [phone] Page of
Client Name Project Number Requested Analyses Requested Turnaround
Nova es North America N 0008 none Q Times
Address Project Name/Desc c Note: Rush requests subject to
(�
77 Pe Chapel Church Road Monthlyc acceptance by the facility - Week One -SBM C
City/sTmp PO # / Billing Info O (/}
Frankiinton, NC 27525 3800466333 ¢ $ o _Standard
to 0 Tel Fax Reporting Contact ao
[phone] Scott Creech � k LO Ilin Cq Expedited
Sampler(s) Name, Aftiitation (Print) Billing Contact $ E +C
T Accounts Payable Due
c�tb (� Q
Sam ) Si Site Location !Tim one v Q 4l�lorkorder
Preservation (See Codes) (Combine as necessary)
Collection Matrix Total s of
Item S Sample ID (Feld ldemificalion) Collection Date Time Comp r Grab (see codes) Containers Sample Comments
SBM 0SL 7 X X X X X X X
<-- Total # of Containers
Sample Kit Prepa By
7Y
Date/Time
Relinquished By
�a 04(4=1 t,t� 4-
Date+Time
-4 6000
Recely
t
URkc
Commentsl5pecial Reporting Requirements
Relinquished By
DaterTime
Received By
D lerTime i
© i/
Relinquished By
Date/lime
Received By
DateTme
Cooler #'a R Temps on Receipt
e;7 • `
Conolion� Receipt
Acceptable Unacceptable
Matrix: GW-Groundwaler SO -Soil OW -Drinking Water SE-Sedlmenl SW -Surface Water WW-Wastewater A -Air O-Other (detail in comments) Preservation: Vice H-HCI N-HNO3 S-H2SO4 NO-NaOH O-Other (decal in (omments)
Note : All samples submitted to FNCO Labs are in accordance with the terms and conditions listed on the reverse of this form, unless prior written agreements exist

Sample Preservation Verification
ENCO Cary
Work Order: CD12061
Client: Novozymes North America (N0008)
Logged In: 04-Aug-20 10:00 _
Preservation Check Performed By: I ��
CD12061-01
Project:
Project #:
Logged By
Monthly - Week One - SBM
[none]
John C King
Daterrime: g' 4 26 /1,GtJ
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted Date/Time
Adjusted
Reagent Used/Comments
D
250mLP+H25O4
<2
Y 1 ' 1 NA
Y 1 L I NA
E
250mLP+HNO3
<2
Y / N / NA
Y / ` 1 NA
rh L
Rea ent Name ID
1 K,)U [b:,�V(1
2 t= o
pH Strip ID: ro pos<'S
Rea ent Name ID
3
4
Rea ent Name ID
5
6
C:IELMNTkPrintlwko_PreservationCheck. rpt Page I of 1

2�SQ pCCgF ENCO Laboratories
9e0
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Thursday, September 10, 2020
Novozymes North America (N0008)
Attn: Scott Creech
77 Perry Chapel Church Road
Franklinton, NC 27525
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: Monthly - Week One - SBM
ENCO Workorder(s): CD13978
Dear Scott Creech,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, September 1, 2020.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
0"6LC'=-:;tA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 13

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: SBM
Lab ID: CD13978-01
Sampled: 09/01/20 07:00
Received: 09/01/20 09:50
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
CSU Method
NO PREP
05/28/23
09/02/20
10:18
09/03/20
14:36
EPA 350.1
NO PREP
09/29/20
09/02/20
08:15
09/02/20
13:53
EPA 351.2
Same
09/29/20
09/02/20
12:59
09/08/20
13:35
EPA 353.2
[CALC]
09/03/20
07:00
09/01/20
15:36
09/01/20
17:22
EPA 353.2
NO PREP
09/03/20
07:00
09/01/20
15:36
09/01/20
17:22
EPA 353.2
NO PREP
09/29/20
09/01/20
12:25
09/01/20
15:09
EPA 365.4
Same
09/29/20
09/02/20
12:47
09/08/20
15:40
EPA 6010D
EPA 3005A
02/28/21
09/02/20
10:18
09/03/20
11:42
EPA 7470A
EPA 7470A
09/29/20
09/03/20
10:37
09/04/20
12:38
SM 254OB-2011
NO PREP
09/08/20
09/08/20
14:26
09/08/20
18:26
SM 2540D-2011
NO PREP
09/08/20
09/04/20
15:21
09/04/20
15:21
SM 5210 B-2011
NO PREP
09/03/20
07:00
09/02/20
08:28
09/02/20
08:28
SM 5220D-2011
Same
09/29/20
09/08/20
10:18
09/08/20
13:55
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 13

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SAMPLE DETECTION SUMMARY
Client ID: SBM
Lab ID: CD13978-01
Analvte
Results
Flag
MDL
Q
Units
Method Notes
Aluminum - Total
15.6
0.420
1.00
mg/L
EPA 6010D
Ammonia as N
100
D
9.0
20
mg/L
EPA 350.1
Biochemical Oxygen Demand
11000
2.0
2.0
mg/L
SM 5210 B-2011 B-07
Calcium - Total
2800
0.390
1.00
mg/L
EPA 6010D
Chemical Oxygen Demand
34000
800
800
mg/L
SM 5220D-2011
Copper - Total
0.199
0.0160
0.100
mg/L
EPA 6010D
Magnesium - Total
15.4
0.290
1.00
mg/L
EPA 6010D
Molybdenum - Total
0.0274
3
0.0250
0.100
mg/L
EPA 6010D
Nickel - Total
0.0258
3
0.0220
0.100
mg/L
EPA 6010D
Nitrate as N
2.9
D
0.41
1.0
mg/L
EPA 353.2
Nitrate/Nitrite as N
3.1
D
0.41
1.0
mg/L
EPA 353.2
Nitrite as N
0.19
0.017
0.10
mg/L
EPA 353.2
Phosphorus
790
D
25
100
mg/L
EPA 365.4
Potassium - Total
339
1.50
5.00
mg/L
EPA 6010D
Sodium - Total
278
4.00
5.00
mg/L
EPA 6010D
Sodium Adsorption Ratio
1.44
[blank]
CSU Method
Total Kjeldahl Nitrogen
2500
D
52
96
mg/L
EPA 351.2
Total Solids
5.9
0.12
0.12
% by Volume
SM 254OB-2011
Total Suspended Solids
38000
250
250
mg/L
SM 2540D-2011
Zinc - Total
0.133
0.0440
0.100
mg/L
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 13

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ANALYTICAL RESULTS
Description: SBM Lab Sample ID:CD13978-01 Received: 09/01/20 09:50
Matrix: Sludge Sampled: 09/01/20 07:00 Work Order: CD13978
Project: Monthly - Week One - SBM Sampled By: Adam Fauccette
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
Mercury [7439-97-6]^
0.00150
U
mg/L
10
0.00150
0.00200
0103011
EPA 7470A
09/04/20 12:38
KAH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Ay
Notes
Aluminum [7429-90-5]^
15.6
mg/L
10
0.420
1.00
0102014
EPA 6010D
09/03/20 11:42
JDH
Arsenic[7440-38-2]^
0.0760
U
mg/L
10
0.0760
0.100
0102014
EPA 6010D
09/03/20 11:42
JDH
Cadmium [7440-43-9]^
0.00360
U
mg/L
10
0.00360
0.0100
0102014
EPA 6010D
09/03/20 11:42
JDH
Calcium [7440-70-2]^
2800
mg/L
10
0.390
1.00
0102014
EPA 6010D
09/03/20 11:42
JDH
Copper[7440-50-8]^
0.199
mg/L
10
0.0160
0.100
0102014
EPA 6010D
09/03/20 11:42
JDH
Lead [7439-92-1]^
0.0310
U
mg/L
10
0.0310
0.100
0102014
EPA 6010D
09/03/20 11:42
JDH
Magnesium [7439-95-4]^
15.4
mg/L
10
0.290
1.00
0102014
EPA 6010D
09/03/20 11:42
JDH
Molybdenum [7439-98-7]^
0.0274
J
mg/L
10
0.0250
0.100
0102014
EPA 6010D
09/03/20 11:42
JDH
Nickel[7440-02-O]^
0.0258
J
mg/L
10
0.0220
0.100
0102014
EPA 6010D
09/03/20 11:42
JDH
Potassium [7440-09-7]^
339
mg/L
10
1.50
5.00
0102014
EPA 6010D
09/03/20 11:42
JDH
Selenium [7782-49-2]^
0.0620
U
mg/L
10
0.0620
0.100
0102014
EPA 6010D
09/03/20 11:42
JDH
Sodium [7440-23-5]^
278
mg/L
10
4.00
5.00
0102014
EPA 6010D
09/03/20 11:42
JDH
Zinc[7440-66-6]^
0.133
mg/L
10
0.0440
0.100
0102014
EPA 6010D
09/03/20 11:42
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Ay
Notes
Ammonia as N [7664-41-7]^
100
D
mg/L
200
9.0
20
0102007
EPA 350.1
09/02/20 13:53
JAH
Biochemical Oxygen Demand^
11000
mg/L
1
2.0
2.0
0102003
SM 5210 B-2011
09/02/20 08:28
JOC
B-07
Chemical Oxygen Demand^
34000
mg/L
80
800
800
0108018
SM 5220D-2011
09/08/20 13:55
JOC
Nitrate as N [14797-55-8]
2.9
D
mg/L
10
0.41
1.0
[CALC]
EPA 353.2
09/01/20 17:22
JAH
Nitrate/Nitrite as N^
3.1
D
mg/L
10
0.41
1.0
0101040
EPA 353.2
09/01/20 15:09
JAH
Nitrite as N [14797-65-0]^
0.19
mg/L
1
0.017
0.10
0101050
EPA 353.2
09/01/20 17:22
JAH
Phosphorus[7723-14-O]^
790
D
mg/L
1000
25
100
0102029
EPA 365.4
09/08/20 15:40
JAH
Sodium Adsorption Ratio
1.44
[blank]
1
0102014
CSU Method
09/03/20 14:36
JDH
Total Kjeldahl Nitrogen^
2500
D
mg/L
200
52
96
0102032
EPA 351.2
09/08/20 13:35
JAH
Total Solids^
5.9
% by Volume
25
0.12
0.12
0108040
SM 2540B-2011
09/08/20 18:26
DMJ
Total Suspended Solids^
38000
mg/L
100
250
250
0104011
SM 2540D-2011
09/04/20 15:21
DMJ
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 13

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 0103O11 - EPA 747OA
Blank (OI03011-BLK3) Prepared: 09/03/2020 10:37 Analyzed: 09/04/2020 12:10
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Mercury 0.000150 U 0.000200 mg/L
Blank (OI03011-BLK2) Prepared: 09/03/2020 10:37 Analyzed: 09/04/2020 12:12
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Mercury 0.00300 U 0.00400 mg/L
LCS (0I03011-BSI) Prepared: 09/03/2020 10:37 Analyzed: 09/04/2020 12:14
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00526
0.000200
mg/L
0.00500
105
80-120
Matrix Spike (OI03011-MSI)
Prepared: 09/03/2020 10:37 Analyzed: 09/04/2020 12:19
Source: CD14023-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00492
0.000200
mg/L
0.00500
0.000150 U
98
75-125
Matrix Spike Dup (OI03011-MSD3)
Prepared: 09/03/2020 10:37 Analyzed: 09/04/2020 12:22
Source: CD14023-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00485
0.000200
mg/L
0.00500
0.000150 U
97
75-125 2
25
Post Spike (0I03011-PSI)
Prepared: 09/03/2020 10:37 Analyzed: 09/04/2020 12:24
Source: CD14023-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
5.52
0.200
ug/L
5.00
-0.0260
110
75-125
Metals (total recoverable) by EPA 6000/7000
Series Methods - Quality Control
Batch OIO2O14 - EPA 3OO5A
Blank (0I02014-BLK3) Prepared: 09/02/2020 10:18 Analyzed: 09/03/2020 10:39
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Aluminum
0.0420
U
0.100
mg/L
Arsenic
0.00760
U
0.0100
mg/L
Cadmium
0.000360
U
0.00100
mg/L
Calcium
0.0390
U
0.100
mg/L
Copper
0.00160
U
0.0100
mg/L
Lead
0.00310
U
0.0100
mg/L
Magnesium
0.0290
U
0.100
mg/L
Molybdenum
0.00250
U
0.0100
mg/L
Nickel
0.00220
U
0.0100
mg/L
Potassium
0.150
U
0.500
mg/L
Selenium
0.00620
U
0.0100
mg/L
Sodium
0.400
U
0.500
mg/L
Zinc
0.00440
U
0.0100
mg/L
FINAL
This report relates only
to the sample as received by the laboratory, and may only be reproduced in full.
Page 5 of 13

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 0102O14 - EPA 3OO5A - Continued
LCS (0I02014-BS1) Prepared: 09/02/2020 10:18 Analyzed: 09/03/2020 11:05
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limi RPD
Limit Notes
Aluminum
2.08
0.100
mg/L
2.00
104
80-120
Arsenic
0.205
0.0100
mg/L
0.200
103
80-120
Cadmium
0.0209
0.00100
mg/L
0.0200
104
80-120
Calcium
2.15
0.100
mg/L
2.00
107
80-120
Copper
0.204
0.0100
mg/L
0.200
102
80-120
Lead
0.206
0.0100
mg/L
0.200
103
80-120
Magnesium
2.08
0.100
mg/L
2.00
104
80-120
Molybdenum
0.203
0.0100
mg/L
0.200
102
80-120
Nickel
0.212
0.0100
mg/L
0.200
106
80-120
Potassium
10.4
0.500
mg/L
10.0
104
80-120
Selenium
0.201
0.0100
mg/L
0.200
101
80-120
Sodium
11.0
0.500
mg/L
10.0
110
80-120
Zinc
0.216
0.0100
mg/L
0.200
108
80-120
Matrix Spike (OI02014-MS1)
Prepared: 09/02/2020
10:18 Analyzed: 09/03/2020 11:08
Source: CD09103-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Aluminum
3.60
0.100
mg/L
2.00
0.912
134
75-125
QM-07
Arsenic
0.200
0.0100
mg/L
0.200
0.00760 U
100
75-125
Cadmium
0.0204
0.00100
mg/L
0.0200
0.000360 U
102
75-125
Calcium
3.09
0.100
mg/L
2.00
1.06
101
75-125
Copper
0.200
0.0100
mg/L
0.200
0.00272
99
75-125
Lead
0.205
0.0100
mg/L
0.200
0.00310 U
102
75-125
Magnesium
2.38
0.100
mg/L
2.00
0.339
102
75-125
Molybdenum
0.198
0.0100
mg/L
0.200
0.00250 U
99
75-125
Nickel
0.209
0.0100
mg/L
0.200
0.00220 U
105
75-125
Potassium
12.2
0.500
mg/L
10.0
1.99
102
75-125
Selenium
0.203
0.0100
mg/L
0.200
0.00620 U
101
75-125
Sodium
11.0
0.500
mg/L
10.0
0.400 U
110
75-125
Zinc
0.217
0.0100
mg/L
0.200
0.00565
106
75-125
Matrix Spike Dup (0I02014-MSD3)
Prepared: 09/02/2020
10:18 Analyzed: 09/03/2020 11:10
Source: CD09103-01
Spike
Source
%REC
RPD
Analvte
Result
FFFlaa POL
Uni
Level
Result
%REC
Limits
RPD
Limit Notes
Aluminum
3.68
0.100
mg/L
2.00
0.912
138
75-125
2
20 QM-07
Arsenic
0.201
0.0100
mg/L
0.200
0.00760 U
101
75-125
0.7
20
Cadmium
0.0206
0.00100
mg/L
0.0200
0.000360 U
103
75-125
1
20
Calcium
3.20
0.100
mg/L
2.00
1.06
107
75-125
4
20
Copper
0.204
0.0100
mg/L
0.200
0.00272
101
75-125
2
20
Lead
0.206
0.0100
mg/L
0.200
0.00310 U
103
75-125
0.5
20
Magnesium
2.46
0.100
mg/L
2.00
0.339
106
75-125
3
20
Molybdenum
0.201
0.0100
mg/L
0.200
0.00250 U
101
75-125
1
20
Nickel
0.212
0.0100
mg/L
0.200
0.00220 U
106
75-125
1
20
Potassium
12.6
0.500
mg/L
10.0
1.99
106
75-125
3
20
Selenium
0.204
0.0100
mg/L
0.200
0.00620 U
102
75-125
0.8
20
Sodium
11.4
0.500
mg/L
10.0
0.400 U
114
75-125
3
20
Zinc
0.219
0.0100
mg/L
0.200
0.00565
107
75-125
1
20
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 13

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 0102014 - EPA 3OO5A - Continued
Post Spike (0I02014-PS1)
Prepared: 09/02/2020 10:18 Analyzed: 09/03/2020 11:12
Source: CD09103-01
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD Limit Notes
Aluminum
4.21
0.100
mg/L
2.00
0.912
165
80-120 QM-08
Arsenic
0.213
0.0100
mg/L
0.200
0.00158
106
80-120
Cadmium
0.0211
0.00100
mg/L
0.0200
-5.60E-5
106
80-120
Calcium
3.22
0.100
mg/L
2.00
1.06
108
80-120
Copper
0.210
0.0100
mg/L
0.200
0.00272
103
80-120
Lead
0.209
0.0100
mg/L
0.200
0.000857
104
80-120
Magnesium
2.50
0.100
mg/L
2.00
0.339
108
80-120
Molybdenum
0.206
0.0100
mg/L
0.200
-0.000500
103
80-120
Nickel
0.217
0.0100
mg/L
0.200
0.000265
108
80-120
Potassium
12.6
0.500
mg/L
10.0
1.99
106
80-120
Selenium
0.205
0.0100
mg/L
0.200
-0.00195
103
80-120
Sodium
11.4
0.500
mg/L
10.0
0.323
111
80-120
Zinc
0.224
0.0100
mg/L
0.200
0.00565
109
80-120
Classical Chemistry Parameters - Quality Control
Batch 0101040 - NO PREP
Blank (0I03040-BLK3) Prepared: 09/O1/2020 12:25 Analyzed: 09/O1/2020 1,134
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Nitrate/Nitrite as N 0.041 U 0.10 mg/L
LCS (OI01040-BS3) Prepared: 09/O1/2020 12:25 Analyzed: 09/O1/2020 14:58
Spike Source %REC
RPD
Analvte
Result
Flaa
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
1.1
0.10
mg/L
1.25 90 90-110
Matrix Spike (0I01040-MSi)
Prepared: 09/O1/2020 12:25 Analyzed: 09/O1/2020 15:02
Source: CD13977-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
5.4
E
0.10
mg/L
0.521 4.6 140 90-110
QM-07
Matrix Spike (OI01040-MS2)
Prepared: 09/O1/2020 12:25 Analyzed: 09/O1/2020 15:07
Source: CD13977-02
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
5.7
E
0.10
mg/L
0.521 5.1 113 90-110
QM-07
Matrix Spike Dup (OI03040-MSD3)
Prepared: 09/O1/2020 12:25 Analyzed: 09/O1/2020 15:04
Source: CD13977-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
5.2
E
0.10
mg/L
0.521 4.6 103 90-110 4
10
Batch 0101050 - NO PREP
Blank (0I03050-BLK3) Prepared: 09/O1/2020 15:36 Analyzed: 09/O1/2020 17:12
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 0101O5O - NO PREP - Continued
Blank (OI01050-BLK1) Continued Prepared: 09/01/2020 15:36 Analyzed: 09/01/2020 17:12
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Nitrite as N 0.017 U 0.10 mg/L
LCS (OI01050-BS3) Prepared: 09/01/2020 15:36 Analyzed: 09/01/2020 17:36
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
1.1
0.10
mg/L
1.00 106 90-110
Matrix Spike (0I01050-MSi)
Prepared: 09/01/2020 15:36 Analyzed: 09/01/2020 17:14
Source: CD13894-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
1.0
0.10
mg/L
1.00 0.017 U 100 90-110
Matrix Spike (OI01050-MS2)
Prepared: 09/01/2020 15:36 Analyzed: 09/01/2020 17:19
Source: CD13896-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
0.96
0.10
mg/L
1.00 0.017 U 96 90-110
Matrix Spike Dup (OI03050-MSD3)
Prepared: 09/01/2020 15:36 Analyzed: 09/01/2020 17:15
Source: CD13894-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
1.0
0.10
mg/L
1.00 0.017 U 101 90-110 1
10
Batch 0102003 - NO PREP
Blank (0I02003-BLK3) Prepared & Analyzed: 09/02/2020 08:28
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Biochemical Oxygen Demand 2.0 U 2.0 mg/L
LCS (OI02003-BS3) Prepared & Analyzed: 09/02/2020 08:28
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit
Notes
Biochemical Oxygen Demand
140
2.0
mg/L
198
69 85-115
B-07
Duplicate (OI02003-DUPl)
Prepared & Analyzed: 09/02/2020 08:28
Source: CD11460-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit
Notes
Biochemical Oxygen Demand
2.0 U
2.0
mg/L
2.0 U
30
B-07
Batch 0IO2OO7 - NO PREP
Blank (0I02007-BLK3) Prepared: 09/02/2020 08:15 Analyzed: 09/02/2020 12:56
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Ammonia as N 0.045 U 0.10 mg/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 0102OO7 - NO PREP - Continued
LCS (OI02007-BS3) Prepared: 09/02/2020 08:15 Analyzed: 09/02/2020 13:16
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
1.0
0.10
mg/L
1.01 101 90-110
Matrix Spike (OI02007-MS1)
Prepared: 09/02/2020 08:15 Analyzed: 09/02/2020 13:20
Source: CD13896-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
0.045
U
0.10
mg/L
0.393 0.045 U 90-110
QM-07
Matrix Spike (0I02007-MS2)
Prepared: 09/02/2020 08:15 Analyzed: 09/02/2020 13:28
Source: CD13897-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
0.045
U
0.10
mg/L
0.393 0.047 NR 90-110
QM-07
Matrix Spike Dup (OI02007-MSD1)
Prepared: 09/02/2020 08:15 Analyzed: 09/02/2020 13:21
Source: CD13896-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
0.045
U
0.10
mg/L
0.393 0.045 U 90-110
10
QM-07
Batch 0102O14 - EPA 3OO5A
Blank (OI02014-BLK3) Prepared: 09/02/2020 10:18 Analyzed: 09/03/2020 14:36
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Sodium Adsorption Ratio 0.00 U [blank]
Batch 0102O29 - Same
Blank (0I02029-BLK3) Prepared: 09/02/2020 12:47 Analyzed: 09/08/2020 15:02
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Phosphorus 0.025 U 0.10 mg/L
LCS (OI02029-BS1) Prepared: 09/02/2020 12:47 Analyzed: 09/08/2020 15:21
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
1.7
0.10
mg/L
1.60 106 80-120
Matrix Spike (OI02029-MS1)
Prepared: 09/02/2020 12:47 Analyzed: 09/08/2020 15:23
Source: CD10598-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
24
D
1.0
mg/L
0.640 22 269 80-120
QM-07
Matrix Spike Dup (0I02029-MSD1)
Prepared: 09/02/2020 12:47 Analyzed: 09/08/2020 15:25
Source: CD10598-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
23
D
1.0
mg/L
0.640 22 219 80-120 1
25
QM-07
Batch 0102O32 - Same
FINAL
This report relates only to
the sample as received by the
laboratory, and may only be reproduced in full.
Page 9 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 0102032 - Same - Continued
Blank (OI02032-BLK3) Prepared: 09/02/2020 12:59 Analyzed: 09/08/2020 10:15
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Kjeldahl Nitrogen 0.26 U 0.48 mg/L
LCS (OI02032-BS3) Prepared: 09/02/2020 12:59 Analyzed: 09/08/2020 11:33
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
13
0.48
mg/L
12.0 107 90-110
Matrix Spike (0I02032-MSi)
Prepared: 09/02/2020 12:59 Analyzed: 09/08/2020 11:36
Source: CD10598-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
75
E
0.48
mg/L
4.80 65 191 90-110
QM-07
Matrix Spike (OI02032-MS2)
Prepared: 09/02/2020 12:59 Analyzed: 09/08/2020 11:42
Source: CD11341-02
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
5.4
0.48
mg/L
4.80 0.96 92 90-110
Matrix Spike Dup (OI02032-MSD3)
Prepared: 09/02/2020 12:59 Analyzed: 09/08/2020 11:38
Source: CD10598-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
72
E
0.48
mg/L
4.80 65 146 90-110 3
10
QM-07
Batch 0104011 - NO PREP
Blank (0I04011-BLK3) Prepared & Analyzed: 09/04/2020 15:21
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Suspended Solids 2.5 U 2.5 mg/L
LCS (OI04011-BS3) Prepared & Analyzed: 09/04/2020 15:21
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Total Suspended Solids
98
2.5
mg/L
100 98 80-120
Duplicate (OI04011-DUPl)
Prepared & Analyzed: 09/04/2020 15:21
Source: CD12349-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Total Suspended Solids
64
25
mg/L
58
10
20
Duplicate (OI04011-DUP2)
Prepared & Analyzed: 09/04/2020 15:21
Source: CD13977-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Total Suspended Solids
41
25
mg/L
39
5
20
Batch 0108018 - Same
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 0108018 - Same - Continued
Blank (OI08018-BLK3) Prepared: 09/08/2020 10:18 Analyzed: 09/08/2020 13:55
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Chemical Oxygen Demand 10 U 10 mg/L
LCS (OI08018-BS3) Prepared: 09/08/2020 10:18 Analyzed: 09/08/2020 13:55
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Chemical Oxygen Demand
500
10
mg/L
500
101
90-110
Matrix Spike (0I08018-MSI)
Prepared: 09/08/2020 10:18 Analyzed: 09/08/2020 13:55
Source: CD12344-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Chemical Oxygen Demand
710
10
mg/L
526
180
101
90-110
Matrix Spike Dup (OI08018-MSD1)
Prepared: 09/08/2020 10:18 Analyzed: 09/08/2020 13:55
Source: CD12344-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Chemical Oxygen Demand
710
10
mg/L
526
180
100
90-110 0.6
5
Batch 0108040 - NO PREP
Blank (OI08040-BLK3) Prepared & Analyzed: 09/08/2020 18:26
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Solids 0.0050 U 0.0050 % by Volume
LCS (0I08040-BSI) Prepared & Analyzed: 09/08/2020 18:26
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Solids
1100
50
mg/L
1100 97 80-120
Duplicate (OI08040-DUPI)
Prepared & Analyzed: 09/08/2020 18:26
Source: CD13977-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Solids
0.20
0.010
% by Volume
0.19 0.2
20
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 13

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
B-07 LCS exceeded control limits for this test. The test can not be repeated due to method constraints. The
result should be considered an estimated value.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 13

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C� 10775 LPart er Executive4810 Suite 111 Woodwinds Industrial Ct-
Orlando, F32824 Jacksonfe, FL 3221fi069 Cary,
(407) R26-5314 Fax (407) M-6945 [phone] Fax (9(M) 296.6216 [phone] Fax [phone] Page of
Client Name Project Number Requested Analyses Requested Turnaround
Times
f1 N b p
Address Project Name/Desc y/j Note : Rush requests subject to
acceptance by the lacllity
rr church Road Month - Week One - SiiM � � C
City1STOP PO q / Billing Info w Qi, w
Franldintm, NC 27525 380046OW3 E � Q Standard
Tel Fax Reporting Contact a K P 19 N
[phone] Scott Creech Z. C*4 Expedited
Sampler(s) Name, AMiation ) Billing Contact C3 E Z
r,-u.� .P AmuMs Payable A s Gl1 N Due 1 1
Sampier(c) Signature Site Location! Time Zone U CEEq �D Lab Workorder
Its �
o ✓d—% i c (a4 L) _ I^
tj Preservation (See Codes) (Combine as necessary) C D 13978
Collection Matrix Total p of
item 4 Sample I (Field identification) Coilection Dale Time Comp %Grab (see codes) Containers Sample Comments
SBM - - -to Iyloo
<-- Total # of Containers
Sam
Dame
Relinquished By
Date/Time
—7-6 bl
Recev
batelme y� * �
i OR
CommentslSpecial Reporting Requirements
Relinquished By
6aterrime
Received By
D )me
q:50
Relinquished By
DateMrne
Received By
Dale me
Cooler #'s S Temps on Receipt
Condition Upon Receipt
Acceptable Unacceptable
Matrix: GW-Groundwater SO -Soil DW-Drinking Water SE -Sediment SW -Surface Water WW-Wastewater A -Air O-Other (detail in comments) Preservation: I -Ice H-NCI N-HNO3 S-H2SO4 NO-NaOH O-Other {derail in comments)
Note : Ali samples submitted to ENCO Labs are in accordance with the temrs and conditions listed on the reverse of this form, unless prior written agreements exist

Sample Preservation Verification
ENCO Cary
ENCO
Work Order: CD13978 Project: Monthly - Week One - SBM
Client: Novozymes North America (NO008) Project #: [none]
Lagged In: 01-Sep-20 10:00 Logged By: Rachel Ann Yoois
Preservation Check Performed By: -T� Date/Time: P
CD13978-01
Cont
Type
Pres (pH)
Requirement
pH Checked /
4n Control
pH Adjusted Date(Time
Adjusted
Reagent Used/Comments
D
250mLP+H2SO4
<2
I N/ NA
Y I N/ NA 1: ��
5
E
250mLP+HNO3
<2
Y N l NA
Y N I NA
B
t
,� •_ice►
Rea ent Name ID
3
4
Reagent Name ID
5
6
pH Strip ID:
PH Strips COF0555
C:lelmntlPrin,%vvKu_rieservationCheck. rpt Page 1 of 1

2�SQ pCCgF ENCO Laboratories
9e0
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Monday, October 19, 2020
Novozymes North America (N0008)
Attn: Scott Creech
77 Perry Chapel Church Road
Franklinton, NC 27525
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: Monthly - Week One - SBM
ENCO Workorder(s): CD15652
Dear Scott Creech,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, October 6, 2020.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
0"6LC'=-:;tA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 13

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: SBM
Lab ID: CD15652-01
Sampled: 10/06/20 00:50
Received: 10/06/20 09:00
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
CSU Method
NO PREP
07/02/23
10/06/20
13:21
10/07/20
15:21
EPA 350.1
NO PREP
11/03/20
10/14/20
08:26
10/14/20
11:58
EPA 351.2
Same
11/03/20
10/07/20
09:10
10/13/20
10:30
EPA 353.2
NO PREP
10/08/20
00:50
10/07/20
15:02
10/07/20
16:56
EPA 353.2
[CALC]
10/08/20
00:50
10/12/20
15:07
10/12/20
18:19
EPA 353.2
NO PREP
11/03/20
10/12/20
15:07
10/12/20
18:19
EPA 365.4
Same
11/03/20
10/07/20
09:09
10/13/20
12:14
EPA 6010D
EPA 3005A
04/04/21
10/06/20
13:21
10/07/20
10:25
EPA 7470A
EPA 7470A
11/03/20
10/11/20
18:13
10/13/20
14:05
SM 254OB-2011
NO PREP
10/13/20
10/08/20
18:02
10/08/20
18:02
SM 2540D-2011
NO PREP
10/13/20
10/12/20
14:37
10/12/20
14:37
SM 5210 B-2011
NO PREP
10/08/20
00:50
10/07/20
10:51
10/07/20
10:51
SM 5220D-2011
Same
11/03/20
10/09/20
08:25
10/09/20
11:25
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 13

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SAMPLE DETECTION SUMMARY
Client ID: SBM
Lab ID: CD15652-01
Analvte
Results
Flag
MDL
Q
Units
Method Notes
Aluminum - Total
49.4
0.420
1.00
mg/L
EPA 6010D
Ammonia as N
130
D
4.0
9.0
mg/L
EPA 350.1
Biochemical Oxygen Demand
12000
2.0
2.0
mg/L
SM 5210 B-2011
Calcium - Total
3370
0.390
1.00
mg/L
EPA 6010D
Chemical Oxygen Demand
34000
800
800
mg/L
SM 5220D-2011
Copper - Total
0.0337
3
0.0160
0.100
mg/L
EPA 6010D
Magnesium - Total
10.7
0.290
1.00
mg/L
EPA 6010D
Nickel - Total
0.0377
1
0.0220
0.100
mg/L
EPA 6010D
Nitrate as N
19
D
0.41
1.0
mg/L
EPA 353.2
Nitrate/Nitrite as N
19
D
0.41
1.0
mg/L
EPA 353.2
Nitrite as N
0.21
0.017
0.10
mg/L
EPA 353.2
Phosphorus
560
D
12
50
mg/L
EPA 365.4
Potassium - Total
589
1.50
5.00
mg/L
EPA 6010D
Sodium - Total
303
4.00
5.00
mg/L
EPA 6010D
Sodium Adsorption Ratio
1.43
[blank]
CSU Method
Total Kjeldahl Nitrogen
1900
D
52
96
mg/L
EPA 351.2
Total Solids
3.4
0.12
0.12
% by Volume
SM 254OB-2011
Total Suspended Solids
9300
500
500
mg/L
SM 254OD-2011
Zinc - Total
0.278
0.0440
0.100
mg/L
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 13

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ANALYTICAL RESULTS
Description: SBM Lab Sample ID:CD15652-01 Received: 10/06/20 09:00
Matrix: Sludge Sampled:10/06/20 00:50 Work Order: CD15652
Project: Monthly - Week One - SBM Sampled By: Elvin C Williamson
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay Notes
Mercury [7439-97-6]^
0.000750
U
mg/L
5
0.000750
0.00100
0J11003
EPA 7470A
10/13/20 14:05
KAH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Ay Notes
Aluminum [7429-90-5]^
49.4
mg/L
10
0.420
1.00
0306036
EPA 6010D
10/07/20 10:25
JDH
Arsenic[7440-38-2]^
0.0760
U
mg/L
10
0.0760
0.100
0J06036
EPA 6010D
10/07/20 10:25
JDH
Cadmium [7440-43-9]^
0.00360
U
mg/L
10
0.00360
0.0100
0J06036
EPA 6010D
10/07/20 10:25
JDH
Calcium [7440-70-2]^
3370
mg/L
10
0.390
1.00
0306036
EPA 6010D
10/07/20 10:25
JDH
Copper[7440-50-8]^
0.0337
J
mg/L
10
0.0160
0.100
0306036
EPA 6010D
10/07/20 10:25
JDH
Lead [7439-92-1]^
0.0310
U
mg/L
10
0.0310
0.100
0J06036
EPA 6010D
10/07/20 10:25
JDH
Magnesium [7439-95-4]^
10.7
mg/L
10
0.290
1.00
0306036
EPA 6010D
10/07/20 10:25
JDH
Molybdenum [7439-98-7]^
0.0250
U
mg/L
10
0.0250
0.100
0J06036
EPA 6010D
10/07/20 10:25
JDH
Nickel[7440-02-O]^
0.0377
J
mg/L
10
0.0220
0.100
0306036
EPA 6010D
10/07/20 10:25
JDH
Potassium [7440-09-7]^
589
mg/L
10
1.50
5.00
0306036
EPA 6010D
10/07/20 10:25
JDH
Selenium [7782-49-2]^
0.0620
U
mg/L
10
0.0620
0.100
0J06036
EPA 6010D
10/07/20 10:25
JDH
Sodium [7440-23-5]^
303
mg/L
10
4.00
5.00
0306036
EPA 6010D
10/07/20 10:25
JDH
Zinc[7440-66-6]^
0.278
mg/L
10
0.0440
0.100
0306036
EPA 6010D
10/07/20 10:25
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Ay Notes
Ammonia as N [7664-41-7]^
130
D
mg/L
90
4.0
9.0
0314008
EPA 350.1
10/14/20 11:58
JAH
Biochemical Oxygen Demand^
12000
mg/L
1
2.0
2.0
0307008
SM 5210 B-2011
10/07/20 10:51
JOC
Chemical Oxygen Demand^
34000
mg/L
80
800
800
0308042
SM 5220D-2011
10/09/20 11:25
JOC
Nitrate as N [14797-55-8]
19
D
mg/L
10
0.41
1.0
[CALC]
EPA 353.2
10/12/20 18:19
JAH
Nitrate/Nitrite as N^
19
D
mg/L
10
0.41
1.0
0312030
EPA 353.2
10/12/20 18:19
JAH
Nitrite as N [14797-65-0]^
0.21
mg/L
1
0.017
0.10
0307035
EPA 353.2
10/07/20 16:56
JAH
Phosphorus[7723-14-O]^
560
D
mg/L
500
12
50
0307010
EPA 365.4
10/13/20 12:14
JAH
Sodium Adsorption Ratio
1.43
[blank]
1
0306036
CSU Method
10/07/20 15:21
JDH
Total Kjeldahl Nitrogen^
1900
D
mg/L
200
52
96
0307011
EPA 351.2
10/13/20 10:30
JAH
Total Solids^
3.4
% by Volume
25
0.12
0.12
0308040
SM 2540B-2011
10/08/20 18:02
DMJ
Total Suspended Solids^
9300
mg/L
200
500
500
0309029
SM 2540D-2011
10/12/20 14:37
DMJ
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 13

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 0111003 - EPA 7470A
Blank (0311003-BLK1) Prepared: 10/11/2020 18:13 Analyzed: 10/13/2020 13:14
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Mercury 0.000150 U 0.000200 mg/L
Blank (0311003-BLK2) Prepared: 10/11/2020 18:13 Analyzed: 10/13/2020 13:16
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Mercury 0.00300 U 0.00400 mg/L
LCS (0311003-BSI) Prepared: 10/11/2020 18:13 Analyzed: 10/13/2020 13:19
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00528
0.000200
mg/L
0.00500
106
80-120
Matrix Spike (0311003-MS1)
Prepared: 10/11/2020 18:13 Analyzed: 10/13/2020 13:29
Source: CD15347-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00518
0.000200
mg/L
0.00500
0.000150 U
104
75-125
Matrix Spike Dup (0313003-MSD1)
Prepared: 10/11/2020 18:13 Analyzed: 10/13/2020 13:31
Source: C1335347-03
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00518
0.000200
mg/L
0.00500
0.000150 U
104
75-125 0
25
Post Spike (0313003-P51)
Prepared: 10/11/2020 18:13 Analyzed: 10/13/2020 13:33
Source: CD15347-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
5.62
0.200
ug/L
5.00
-0.0340
112
75-125
Metals (total recoverable) by EPA 6000/7000
Series Methods - Quality Control
Batch 0.706036 - EPA 3005A
Blank (0306036-BLK3) Prepared: 10/06/2020 13:21 Analyzed: 10/07/2020 09:50
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Aluminum
0.0420
U
0.100
mg/L
Arsenic
0.00760
U
0.0100
mg/L
Cadmium
0.000360
U
0.00100
mg/L
Calcium
0.0390
U
0.100
mg/L
Copper
0.00160
U
0.0100
mg/L
Lead
0.00310
U
0.0100
mg/L
Magnesium
0.0290
U
0.100
mg/L
Molybdenum
0.00250
U
0.0100
mg/L
Nickel
0.00220
U
0.0100
mg/L
Potassium
0.150
U
0.500
mg/L
Selenium
0.00620
U
0.0100
mg/L
Sodium
0.400
U
0.500
mg/L
Zinc
0.00440
U
0.0100
mg/L
FINAL
This report relates only
to the sample as received by the laboratory, and may only be reproduced in full.
Page 5 of 13

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 0JO6036 - EPA 3OO5A - Continued
LCS (OJ06036-BSI) Prepared: 10/06/2020 13:21 Analyzed: 10/07/2020 09:58
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limi RPD
Limit
Notes
Aluminum
2.20
0.100
mg/L
2.00
110
80-120
Arsenic
0.218
0.0100
mg/L
0.200
109
80-120
Cadmium
0.0218
0.00100
mg/L
0.0200
109
80-120
Calcium
2.24
0.100
mg/L
2.00
112
80-120
Copper
0.213
0.0100
mg/L
0.200
106
80-120
Lead
0.215
0.0100
mg/L
0.200
108
80-120
Magnesium
2.24
0.100
mg/L
2.00
112
80-120
Molybdenum
0.213
0.0100
mg/L
0.200
107
80-120
Nickel
0.225
0.0100
mg/L
0.200
113
80-120
Potassium
10.9
0.500
mg/L
10.0
109
80-120
Selenium
0.210
0.0100
mg/L
0.200
105
80-120
Sodium
11.0
0.500
mg/L
10.0
110
80-120
Zinc
0.228
0.0100
mg/L
0.200
114
80-120
Matrix Spike (0306036-MS3)
Prepared: 10/06/2020
13:21 Analyzed: 10/07/2020 10:01
Source: CD14322-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Aluminum
2.09
0.100
mg/L
2.00
0.0478
102
75-125
Arsenic
0.212
0.0100
mg/L
0.200
0.00760 U
106
75-125
Cadmium
0.0206
0.00100
mg/L
0.0200
0.000360 U
103
75-125
Calcium
35.8
0.100
mg/L
2.00
36.8
NR
75-125
QM-07
Copper
0.206
0.0100
mg/L
0.200
0.00160 U
103
75-125
Lead
0.203
0.0100
mg/L
0.200
0.00310 U
101
75-125
Magnesium
4.98
0.100
mg/L
2.00
3.18
90
75-125
Molybdenum
0.211
0.0100
mg/L
0.200
0.00250 U
106
75-125
Nickel
0.212
0.0100
mg/L
0.200
0.00220 U
106
75-125
Potassium
11.9
0.500
mg/L
10.0
1.68
102
75-125
Selenium
0.201
0.0100
mg/L
0.200
0.00620 U
101
75-125
Sodium
46.8
0.500
mg/L
10.0
39.8
70
75-125
QM-07
Zinc
0.245
0.0100
mg/L
0.200
0.0275
109
75-125
Matrix Spike Dup (0306036-MSD1)
Prepared: 10/06/2020
13:21 Analyzed: 10/07/2020 10:03
Source: CD14322-01
Spike
Source
%REC
RPD
Analvte
Result
FFFlaa POL
Uni
Level
Result
%REC
Limits
RPD
Limit Notes
Aluminum
2.17
0.100
mg/L
2.00
0.0478
106
75-125
4
20
Arsenic
0.216
0.0100
mg/L
0.200
0.00760 U
108
75-125
2
20
Cadmium
0.0209
0.00100
mg/L
0.0200
0.000360 U
104
75-125
1
20
Calcium
36.3
0.100
mg/L
2.00
36.8
NR
75-125
2
20 QM-07
Copper
0.208
0.0100
mg/L
0.200
0.00160 U
104
75-125
1
20
Lead
0.210
0.0100
mg/L
0.200
0.00310 U
105
75-125
3
20
Magnesium
5.11
0.100
mg/L
2.00
3.18
97
75-125
2
20
Molybdenum
0.214
0.0100
mg/L
0.200
0.00250 U
107
75-125
2
20
Nickel
0.217
0.0100
mg/L
0.200
0.00220 U
108
75-125
2
20
Potassium
12.3
0.500
mg/L
10.0
1.68
106
75-125
3
20
Selenium
0.203
0.0100
mg/L
0.200
0.00620 U
101
75-125
0.7
20
Sodium
47.6
0.500
mg/L
10.0
39.8
78
75-125
2
20
Zinc
0.254
0.0100
mg/L
0.200
0.0275
113
75-125
3
20
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 13

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 0JO6036 - EPA 3005A - Continued
Post Spike (O]06036-PS1)
Prepared: 10/06/2020 13:21 Analyzed: 10/07/2020 10:05
Source: CD14322-01
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD Limit Notes
Aluminum
4.22
0.100
mg/L
4.00
0.0478
104
80-120
Arsenic
0.427
0.0100
mg/L
0.400
7.91E-5
107
80-120
Cadmium
0.0427
0.00100
mg/L
0.0400
-0.000536
107
80-120
Calcium
37.4
0.100
mg/L
4.00
36.8
15
80-120 QM-07
Copper
0.419
0.0100
mg/L
0.400
0.00139
104
80-120
Lead
0.423
0.0100
mg/L
0.400
-0.000839
106
80-120
Magnesium
7.13
0.100
mg/L
4.00
3.18
99
80-120
Molybdenum
0.434
0.0100
mg/L
0.400
0.00195
108
80-120
Nickel
0.423
0.0100
mg/L
0.400
-0.000420
106
80-120
Potassium
22.3
0.500
mg/L
20.0
1.68
103
80-120
Selenium
0.430
0.0100
mg/L
0.400
-0.00217
107
80-120
Sodium
56.7
0.500
mg/L
20.0
39.8
85
80-120
Zinc
0.462
0.0100
mg/L
0.400
0.0275
109
80-120
Classical Chemistry Parameters - Quality Control
Batch 0JO6036 - EPA 3005A
Blank (0306036-BLK1) Prepared: 10/06/2020 13:21 Analyzed: 10/07/2020 15:22
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Sodium Adsorption Ratio
0.00
U
[blank]
Blank (0306036-BLK2)
Prepared: 10/06/2020 13:21 Analyzed: 10/07/2020 15:22
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Sodium Adsorption Ratio
0.00
U
[blank]
Batch 0.707008 - NO PREP
Blank (0107008-BLK3) Prepared & Analyzed: 10/07/2020 10:51
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Biochemical Oxygen Demand 2.0 U 2.0 mg/L
LCS (0307008-BS1) Prepared & Analyzed: 10/07/2020 10:51
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Biochemical Oxygen Demand
190
2.0
mg/L
198
95 85-115
Duplicate (0107008-DUPl)
Prepared & Analyzed: 10/07/2020 10:51
Source: CDO5573-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Biochemical Oxygen Demand
17000
2.0
mg/L
17000
0.7
30
Batch 0JO7010 - Same
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 0JO7010 - Same - Continued
Blank (0307010-BLK1) Prepared: 10/07/2020 09:09 Analyzed: 10/13/2020 11:48
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Phosphorus 0.025 U 0.10 mg/L
LCS (0707030-BS1) Prepared: 10/07/2020 09:09 Analyzed: 10/13/2020 11:49
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
1.6
0.10
mg/L
1.60 98 80-120
Matrix Spike (OJ07030-MS1)
Prepared: 10/07/2020 09:09 Analyzed: 10/13/2020 11:52
Source: CD12416-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
8.8
D
1.0
mg/L
0.640 8.4 72 80-120
QM-07
Matrix Spike Dup (0307010-MSD1)
Prepared: 10/07/2020 09:09 Analyzed: 10/13/2020 11:53
Source: CD12416-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
8.5
D
1.0
mg/L
0.640 8.4 21 80-120 4
25
QM-07
Batch 0JO7011 - Same
Blank (0307011-BLK3) Prepared: 10/07/2020 09:10 Analyzed: 10/13/2020 10:02
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Kjeldahl Nitrogen 0.26 U 0.48 mg/L
LCS (0307031-BSI) Prepared: 10/07/2020 09:10 Analyzed: 10/13/2020 10:04
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
12
0.48
mg/L
12.0 104 90-110
Matrix Spike (0307011-MS3)
Prepared: 10/07/2020 09:10 Analyzed: 10/13/2020 10:08
Source: CD12416-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
100
D
2.4
mg/L
4.80 94 138 90-110
QM-07
Matrix Spike (0307011-MS2)
Prepared: 10/07/2020 09:10 Analyzed: 10/13/2020 10:39
Source: CD14395-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
17
D
0.96
mg/L
4.80 43 NR 90-110
QM-07
Matrix Spike Dup (O307011-MSDI)
Prepared: 10/07/2020 09:10 Analyzed: 10/13/2020 10:09
Source: CD12416-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
97
D
2.4
mg/L
4.80 94 52 90-110 4
10
QM-07
Batch 0JO7035 - NO PREP
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 0JO7035 - NO PREP - Continued
Blank (0307035-BLK1) Prepared: 10/07/2020 15:02 Analyzed: 10/07/2020 16:45
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Nitrite as N 0.017 U 0.10 mg/L
LCS (0307035-BS3) Prepared: 10/07/2020 15:02 Analyzed: 10/07/2020 17:00
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrite as N
0.92
0.10
mg/L
1.00 92 90-110
Matrix Spike (0307035-MS3)
Prepared: 10/07/2020 15:02 Analyzed: 10/07/2020 16:48
Source: CD15625-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrite as N
0.98
0.10
mg/L
1.00 0.017 U 98 90-110
Matrix Spike Dup (0307035-MSDI)
Prepared: 10/07/2020 15:02 Analyzed: 10/07/2020 16:49
Source: CD15625-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrite as N
0.97
0.10
mg/L
1.00 0.017 U 97 90-110 1
10
Batch OJ08040 - NO PREP
Blank (0308040-BLK3) Prepared & Analyzed: 10/08/2020 18:02
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Solids 0.0050 U 0.0050 % by Volume
LCS (0308040-BSI) Prepared & Analyzed: 10/08/2020 18:02
Analvte
Total Solids
Result Flaq
1100
POL
50
Units
mg/L
Spike Source %REC
Level Result %REC Limits RPD
1100 98 80-120
RPD
Limit Notes
Duplicate (0308040-DUPl)
Prepared & Analyzed: 10/08/2020 18:02
Source: CD144O7-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Solids
0.41
0.010
% by Volume
0.41 2
20
Batch OJ08042 - Same
Blank (0308042-BLK3) Prepared: 10/09/2020 08:25 Analyzed: 10/09/2020 11:25
Spike Source %REC
RPD
Analvte
Result Flaa
POL
Units
Level Result %REC Limits RPD
Limit Notes
Chemical Oxygen Demand
10 U
10
mg/L
LCS (0308042-BSI)
Prepared: 10/09/2020 08:25 Analyzed: 10/09/2020 11:25
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Chemical Oxygen Demand
510
10
mg/L
500 102 90-110
FINAL
This report relates only to
the sample as received by the
laboratory, and may only be reproduced in full.
Page 9 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 0JOS042 - Same - Continued
Matrix Spike (0308042-MS3)
Prepared: 10/09/2020 08:25 Analyzed: 10/09/2020 11:25
Source: CD14395-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Chemical Oxygen Demand
720
10
mg/L
526 160 105 90-110
Matrix Spike Dup (0308042-MSD1)
Prepared: 10/09/2020 08:25 Analyzed: 10/09/2020 11:25
Source: CD14395-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Chemical Oxygen Demand
700
10
mg/L
526 160 102 90-110 2
5
Batch 0JO9029 - NO PREP
Blank (0309029-BLK3) Prepared & Analyzed: 10/12/2020 14:37
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Suspended Solids 2.5 U 2.5 mg/L
LCS (0309029-BS1) Prepared & Analyzed: 10/12/2020 14:37
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Total Suspended Solids
120
2.5
mg/L
100 118 80-120
Duplicate (0309029-DUPl)
Prepared & Analyzed: 10/12/2020 14:37
Source: CD15937-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Total Suspended Solids
180
50
mg/L
180
1
20
Duplicate (0309029-DUP2)
Prepared & Analyzed: 10/12/2020 14:37
Source: CD16331-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Total Suspended Solids
230
50
mg/L
270
14
20
Batch 0111030 - NO PREP
Blank (0312030-BLK1) Prepared: 10/12/2020 15:07 Analyzed: 10/12/2020 17:39
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Nitrate/Nitrite as N 0.041 U 0.10 mg/L
LCS (0312030-BS1) Prepared: 10/12/2020 15:07 Analyzed: 10/12/2020 17:40
Spike Source %REC
RPD
Analvte
Result Flaa
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrate/Nitrite as N
1.3
0.10
mg/L
1.25 103 90-110
Matrix Spike (0312030-MS3)
Prepared: 10/12/2020 15:07 Analyzed: 10/12/2020 17:44
Source: CD15261-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Nitrate/Nitrite as N
0.52
0.10
mg/L
0.521 0.041 U 100 90-110
FINAL
This report relates only to
the sample as received by the
laboratory, and may only be reproduced in full.
Page 10 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 0112030 - NO PREP - Continued
Matrix Spike (0312030-MS2)
Prepared: 10/12/2020 15:07 Analyzed: 10/12/2020 17:53
Source: CD15261-02
Spike Source O/oREC
RPD
Analvte
Result Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit Notes
Nitrate/Nitrite as N
0.55
0.10
mg/L
0.521 0.057 95 90-110
Matrix Spike Dup (0712030-MSD1)
Prepared: 10/12/2020 15:07 Analyzed: 10/12/2020 17:46
Source: CD15261-01
Spike Source O/oREC
RPD
Analvte
Result Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit Notes
Nitrate/Nitrite as N
0.51
0.10
mg/L
0.521 0.041 U 99 90-110 1
10
Batch 011400E - NO PREP
Blank (0114008-BLK3) Prepared: 10/14/2020 08:26 Analyzed: 10/14/2020 10:30
Spike Source O/oREC RPD
Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes
Ammonia as N 0.045 U 0.10 mg/L
LCS (OJ14008-BS1) Prepared: 10/14/2020 08:26 Analyzed: 10/14/2020 11:32
Spike Source O/oREC
RPD
Analvte
Result
Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit
Notes
Ammonia as N
1.1
0.10
mg/L
1.01 104 90-110
Matrix Spike (0314008-MS1)
Prepared: 10/14/2020 08:26 Analyzed: 10/14/2020 11:35
Source: CD15627-01
Spike Source O/oREC
RPD
Analvte
Result
Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit
Notes
Ammonia as N
0.37
0.10
mg/L
0.393 0.045 U 94 90-110
Matrix Spike (OJ14008-MS2)
Prepared: 10/14/2020 08:26 Analyzed: 10/14/2020 11:40
Source: CD15632-01
Spike Source O/oREC
RPD
Analvte
Result
Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit
Notes
Ammonia as N
0.37
0.10
mg/L
0.393 0.045 U 93 90-110
Matrix Spike Dup (0314008-MSD1)
Prepared: 10/14/2020 08:26 Analyzed: 10/14/2020 11:37
Source: CD15627-01
Spike Source O/oREC
RPD
Analvte
Result
Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit
Notes
Ammonia as N
0.38
0.10
mg/L
0.393 0.045 U 96 90-110 2
10
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 13

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 13

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C� 113775 Central Port Dr. 4610 Executive Park Court, Suite i 11 102-A Woodwinds Industrial U.
Orlando, FL 32824 Jacksonville, FL 32216-6069 Cary, NC 27611
[phone] Fax [phone]g45 [phone] Fax [phone] (919) 467-090 Fax [phone] Page of
Client Name Project Number Requested Analyses Requested Turnaround
Noyoz s NOFII7 America(NOON)__nom � Times
Address Project Name/Desc
77 Chi Church Road Monthly- Week One - SBM � � � Note :Rush requests subject to
acceptance by the facility
City/sTop PO # I Billing Info a $ p
Frank inton, NC 27525 3800466333 K N Standard
Tel Fax Reporting Contact N ry
[phone] Scott Creech:it 2L
7 � Expedited
Sampter(sl Name. Affiliation (POnt)Billing Contact [7 r
Acmunfs Payable to !n Us Due I,l_
Sampl s Signature Site Location 1 Time Zone a N U = (� tab WOrkorder
CS
Preservation (See Codes) (Combine as necessary) C D 1 5 ` 52
Collection Matrix Total # o1
Item n Sample ID (Raid identification) CoRectian Dale Time Comp f Grab (see codes} Containers Sample Comments
SBM SL 7 X X X X X
< Total # of Containers
Sample Kit Prepared By
DatelTime
Relinquished By
Dale/Time
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Received By
3'�"J�
Date/nme ; vo
10_4�'24z'v
Comments/Special Reporting Requirements
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Date/Time
Relinquished By
Datefllme
Received By
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Confer a's & Temps on Receipt
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rx : aw-Groundwarer SO -Soil DW-Drinking Water SE -Sediment SW-Surtace Water WW-Wastewater A -Air 0-Other Ideiail in comments) Preservation: 1-Ice H-HGI R-HNO3 S-H2SO4 NO-NaOH O-Outer (detaiiin comments)
Note: All samples submitted to ENCO Labs are in accordance with the terms and conditions listed on the reverse of this form, unless prior written agreements exist

Sample Preservation Verification
ENCO Cary
Work Order: CD15652 Project: Monthly - Week One - SBM
Client: Novozymes North America (NO008) Project #: [none]
Lagged In: 06-Oct-20 11:49 Logged By: John C King
Preservation Check Performed By: VAt Date/Time:
CD15652-01
Coat.
Type,
Pres ,(p)
Requirement ,
pH Checked 1
., In Control
Date/Time Adiusted :. .
pH.AdjrJsted ...iea.c3ent
,. USedlComments
D
250mLP+H2SO4
<2
Y / NA
Y O / NA 00 4)
+Zv-nL
E
250mLP+HNO3
<2
Y V / NA
Y / NA
-2
Reagent Name ID
1 �'44VUO 5C'aNlo�o
2 }� Ii 5 q
pH Strip ID: n�CjSv j
Rea ent Name ID
3
4
Rea ent Name ID
5
6
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Phone: [phone] FAX: [phone]
Thursday, November 12, 2020
Novozymes North America (N0008)
Attn: Scott Creech
77 Perry Chapel Church Road
Franklinton, NC 27525
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: Monthly - Week One - SBM
ENCO Workorder(s): CD16333
Dear Scott Creech,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, November 3, 2020.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
0"6LC'=-:;tA
Chuck Smith
Project Manager
Enclosure(s)
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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: SBM
Lab ID: CD16333-01
Sampled: 11/03/20 03:30
Received: 11/03/20 10:40
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis
Date/Time(s)
CSU Method
NO PREP
07/30/23
11/10/20
09:54
11/11/20
14:53
EPA 350.1
NO PREP
12/01/20
11/09/20
08:39
11/09/20
12:08
EPA 351.2
Same
12/01/20
11/05/20
08:52
11/10/20
10:40
EPA 353.2
NO PREP
11/05/20
03:30
11/03/20
15:51
11/03/20
17:08
EPA 353.2
[CALC]
11/05/20
03:30
11/06/20
11:12
11/06/20
14:24
EPA 353.2
NO PREP
12/01/20
11/06/20
11:12
11/06/20
14:24
EPA 365.4
Same
12/01/20
11/05/20
08:52
11/10/20
12:53
EPA 6010D
EPA 3005A
05/02/21
11/10/20
09:54
11/11/20
13:54
EPA 7470A
EPA 7470A
12/01/20
11/09/20
09:47
11/09/20
16:22
SM 254OB-2011
NO PREP
11/10/20
11/06/20
17:12
11/06/20
17:12
SM 2540D-2011
NO PREP
11/10/20
11/04/20
12:37
11/06/20
11:07
SM 5210 B-2011
NO PREP
11/05/20
03:30
11/04/20
10:10
11/04/20
10:10
SM 5220D-2011
Same
12/01/20
11/06/20
09:30
11/06/20
16:16
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 13

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SAMPLE DETECTION SUMMARY
Client ID: SBM
Lab ID: CD16333-01
Analvte
Results
Flag
MDL
PQL
Units
Method Notes
Aluminum - Total
7.75
0.420
1.00
mg/L
EPA 6010D
Ammonia as N
160
D
4.0
9.0
mg/L
EPA 350.1
Biochemical Oxygen Demand
11000
2.0
2.0
mg/L
SM 5210 B-2011
Calcium - Total
3340
0.390
1.00
mg/L
EPA 6010D
Chemical Oxygen Demand
34000
400
400
mg/L
SM 5220D-2011
Copper - Total
0.0782
3
0.0160
0.100
mg/L
EPA 6010D
Magnesium - Total
51.0
0.290
1.00
mg/L
EPA 6010D
Nickel - Total
0.0308
3
0.0220
0.100
mg/L
EPA 6010D
Nitrate as N
15
D
0.41
1.0
mg/L
EPA 353.2
Nitrate/Nitrite as N
15
D
0.41
1.0
mg/L
EPA 353.2
Nitrite as N
0.24
0.017
0.10
mg/L
EPA 353.2
Phosphorus
170
D
12
50
mg/L
EPA 365.4
Potassium - Total
660
1.50
5.00
mg/L
EPA 6010D
Sodium - Total
364
4.00
5.00
mg/L
EPA 6010D
Sodium Adsorption Ratio
1.71
[blank]
CSU Method
Total Kjeldahl Nitrogen
1300
D
52
96
mg/L
EPA 351.2
Total Solids
3.8
0.12
0.12
% by Volume
SM 254OB-2011
Total Suspended Solids
35000
5000
5000
mg/L
SM 2540D-2011
Zinc - Total
0.113
0.0440
0.100
mg/L
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 13

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ANALYTICAL RESULTS
Description: SBM Lab Sample ID:CD16333-01 Received: 11/03/20 10:40
Matrix: Sludge Sampled: 11/03/20 03:30 Work Order: CD16333
Project: Monthly - Week One - SBM Sampled By: HUNTER WILSON
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay Notes
Mercury [7439-97-6]^
0.00150
U
mg/L
10
0.00150
0.00200
OK09011
EPA 7470A
11/09/20 16:22
KAH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Ay Notes
Aluminum [7429-90-5]^
7.75
mg/L
10
0.420
1.00
OK10015
EPA 6010D
11/11/20 13:54
JDH
Arsenic[7440-38-2]^
0.0760
U
mg/L
10
0.0760
0.100
OK10015
EPA 6010D
11/11/20 13:54
JDH
Cadmium [7440-43-9]^
0.00360
U
mg/L
10
0.00360
0.0100
OK10015
EPA 6010D
11/11/20 13:54
JDH
Calcium [7440-70-2]^
3340
mg/L
10
0.390
1.00
OK10015
EPA 6010D
11/11/20 13:54
JDH
Copper[7440-50-8]^
0.0782
J
mg/L
10
0.0160
0.100
OK10015
EPA 6010D
11/11/20 13:54
JDH
Lead [7439-92-1]^
0.0310
U
mg/L
10
0.0310
0.100
OK10015
EPA 6010D
11/11/20 13:54
JDH
Magnesium [7439-95-4]^
51.0
mg/L
10
0.290
1.00
OK10015
EPA 6010D
11/11/20 13:54
JDH
Molybdenum [7439-98-7]^
0.0250
U
mg/L
10
0.0250
0.100
OK10015
EPA 6010D
11/11/20 13:54
JDH
Nickel[7440-02-O]^
0.0308
J
mg/L
10
0.0220
0.100
OK10015
EPA 6010D
11/11/20 13:54
JDH
Potassium [7440-09-7]^
660
mg/L
10
1.50
5.00
OK10015
EPA 6010D
11/11/20 13:54
JDH
Selenium [7782-49-2]^
0.0620
U
mg/L
10
0.0620
0.100
OK10015
EPA 6010D
11/11/20 13:54
JDH
Sodium [7440-23-5]^
364
mg/L
10
4.00
5.00
OK10015
EPA 6010D
11/11/20 13:54
JDH
Zinc[7440-66-6]^
0.113
mg/L
10
0.0440
0.100
OK10015
EPA 6010D
11/11/20 13:54
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Ay Notes
Ammonia as N [7664-41-7]^
160
D
mg/L
90
4.0
9.0
OK09006
EPA 350.1
11/09/20 12:08
JAH
Biochemical Oxygen Demand^
11000
mg/L
1
2.0
2.0
OK04011
SM 5210 B-2011
11/04/20 10:10
JOC
Chemical Oxygen Demand^
34000
mg/L
40
400
400
OK06006
SM 5220D-2011
11/06/20 16:16
JOC
Nitrate as N [14797-55-8]
15
D
mg/L
10
0.41
1.0
[CALC]
EPA 353.2
11/06/20 14:24
JAH
Nitrate/Nitrite as N^
15
D
mg/L
10
0.41
1.0
OK06023
EPA 353.2
11/06/20 14:24
JAH
Nitrite as N [14797-65-0]^
0.24
mg/L
1
0.017
0.10
OK03038
EPA 353.2
11/03/20 17:08
JAH
Phosphorus[7723-14-O]^
170
D
mg/L
500
12
50
OK04034
EPA 365.4
11/10/20 12:53
JAH
Sodium Adsorption Ratio
1.71
[blank]
1
OK10015
CSU Method
11/11/20 14:53
JDH
Total Kjeldahl Nitrogen^
1300
D
mg/L
200
52
96
OK04035
EPA 351.2
11/10/20 10:40
JAH
Total Solids^
3.8
% by Volume
25
0.12
0.12
OK06015
SM 2540B-2011
11/06/20 17:12
DMJ
Total Suspended Solids^
35000
mg/L
2000
5000
5000
OK04022
SM 2540D-2011
11/06/20 11:07
ZGW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 13

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch OKO9O11 - EPA 747OA
Blank (OK09011-BLKS) Prepared: 11/09/2020 09:47 Analyzed: 11/09/2020 15:41
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Mercury 0.000150 U 0.000200 mg/L
LCS (OK09011-BS3) Prepared: 11/09/2020 09:47 Analyzed: 11/09/2020 15:43
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result %REC
Limits RPD
Limit
Notes
Mercury
0.00503
0.000200
mg/L
0.00500
101
80-120
Matrix Spike (OK09011-MS3)
Prepared: 11/09/2020 09:47 Analyzed: 11/09/2020 15:49
Source: CD14128-07
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result %REC
Limits RPD
Limit
Notes
Mercury
0.00499
0.000200
mg/L
0.00500
0.000150 U 100
75-125
Matrix Spike Dup (OK09011-MSD1)
Prepared: 11/09/2020 09:47 Analyzed: 11/09/2020 15:51
Source: CD14128-07
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result %REC
Limits RPD
Limit
Notes
Mercury
0.00525
0.000200
mg/L
0.00500
0.000150 U 105
75-125 5
25
Post Spike (OK09011-PS3)
Prepared: 11/09/2020 09:47 Analyzed: 11/09/2020 15:53
Source: CD14128-07
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result %REC
Limits RPD
Limit
Notes
Mercury
5.55
0.200
ug/L
5.00
-0.0170 111
75-125
Metals (total recoverable) by EPA 6000/7000
Series Methods - Quality Control
Batch OK1OO15 - EPA 3OO5A
Blank (OK10015-BLK1)
Prepared: 11/10/2020 09:54 Analyzed: 11/11/2020 10:15
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Aluminum
0.0420
U
0.100
mg/L
Arsenic
0.00760
U
0.0100
mg/L
Cadmium
0.000360
U
0.00100
mg/L
Calcium
0.0390
U
0.100
mg/L
Copper
0.00160
U
0.0100
mg/L
Lead
0.00310
U
0.0100
mg/L
Magnesium
0.0290
U
0.100
mg/L
Molybdenum
0.00250
U
0.0100
mg/L
Nickel
0.00220
U
0.0100
mg/L
Potassium
0.150
U
0.500
mg/L
Selenium
0.00620
U
0.0100
mg/L
Sodium
0.400
U
0.500
mg/L
Zinc
0.00440
U
0.0100
mg/L
LCS (OK10015-BS1)
Prepared: 11/10/2020 09:54 Analyzed: 11/11/2020 11:37
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Aluminum 2.14 0.100 mg/L 2.00 107 80-120
Arsenic 0.209 0.0100 mg/L 0.200 104 80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 13

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch OK10015 - EPA 3OO5A - Continued
LCS (OK30015-BS3) Continued Prepared: 11/10/2020 09:54 Analyzed: 11/11/2020 11:37
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Cadmium
0.0213
0.00100
mg/L
0.0200
107
80-120
Calcium
2.20
0.100
mg/L
2.00
110
80-120
Copper
0.211
0.0100
mg/L
0.200
105
80-120
Lead
0.215
0.0100
mg/L
0.200
108
80-120
Magnesium
2.15
0.100
mg/L
2.00
108
80-120
Molybdenum
0.206
0.0100
mg/L
0.200
103
80-120
Nickel
0.219
0.0100
mg/L
0.200
110
80-120
Potassium
10.8
0.500
mg/L
10.0
108
80-120
Selenium
0.206
0.0100
mg/L
0.200
103
80-120
Sodium
10.9
0.500
mg/L
10.0
109
80-120
Zinc
0.220
0.0100
mg/L
0.200
110
80-120
Matrix Spike (OK10015-MS1)
Prepared:
11/10/2020
09:54 Analyzed: 11/11/2020 11:40
Source: CD16580-20
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Aluminum
2.11
0.100
mg/L
2.00
0.0420 U
106
75-125
Arsenic
0.206
0.0100
mg/L
0.200
0.00760 U
103
75-125
Cadmium
0.0206
0.00100
mg/L
0.0200
0.000360 U
103
75-125
Calcium
16.3
0.100
mg/L
2.00
14.8
75
75-125
Copper
0.200
0.0100
mg/L
0.200
0.00160 U
100
75-125
Lead
0.207
0.0100
mg/L
0.200
0.00310 U
103
75-125
Magnesium
12.5
0.100
mg/L
2.00
11.0
72
75-125
QM-07
Molybdenum
0.205
0.0100
mg/L
0.200
0.00250 U
103
75-125
Nickel
0.212
0.0100
mg/L
0.200
0.00220 U
106
75-125
Potassium
12.6
0.500
mg/L
10.0
2.18
104
75-125
Selenium
0.211
0.0100
mg/L
0.200
0.00620 U
105
75-125
Sodium
12.0
0.500
mg/L
10.0
1.64
104
75-125
Zinc
0.215
0.0100
mg/L
0.200
0.00440 U
107
75-125
Matrix Spike Dup (OK10015-MSD1)
Prepared:
11/10/2020
09:54 Analyzed: 11/11/2020 11:47
Source: CD16580-20
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Aluminum
2.21
0.100
mg/L
2.00
0.0420 U
110
75-125
5
20
Arsenic
0.212
0.0100
mg/L
0.200
0.00760 U
106
75-125
3
20
Cadmium
0.0211
0.00100
mg/L
0.0200
0.000360 U
106
75-125
3
20
Calcium
16.9
0.100
mg/L
2.00
14.8
105
75-125
4
20
Copper
0.208
0.0100
mg/L
0.200
0.00160 U
104
75-125
4
20
Lead
0.215
0.0100
mg/L
0.200
0.00310 U
108
75-125
4
20
Magnesium
12.9
0.100
mg/L
2.00
11.0
96
75-125
4
20
Molybdenum
0.213
0.0100
mg/L
0.200
0.00250 U
107
75-125
4
20
Nickel
0.219
0.0100
mg/L
0.200
0.00220 U
109
75-125
3
20
Potassium
13.2
0.500
mg/L
10.0
2.18
110
75-125
4
20
Selenium
0.211
0.0100
mg/L
0.200
0.00620 U
105
75-125
0.05
20
Sodium
12.5
0.500
mg/L
10.0
1.64
109
75-125
4
20
Zinc
0.221
0.0100
mg/L
0.200
0.00440 U
110
75-125
3
20
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 13

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch OK10015 - EPA 3005A - Continued
Post Spike (OK10015-PS1)
Prepared: 11/10/2020 09:54 Analyzed: 11/11/2020 11:49
Source: CD16580-20
Spike
Source
O/oREC RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD Limit Notes
Aluminum
4.30
0.100
mg/L
4.00
0.0419
107
80-120
Arsenic
0.417
0.0100
mg/L
0.400
-0.00159
104
80-120
Cadmium
0.0422
0.00100
mg/L
0.0400
-3.41E-5
106
80-120
Calcium
18.4
0.100
mg/L
4.00
14.8
91
80-120
Copper
0.412
0.0100
mg/L
0.400
0.00109
103
80-120
Lead
0.426
0.0100
mg/L
0.400
-0.000863
106
80-120
Magnesium
14.6
0.100
mg/L
4.00
11.0
88
80-120
Molybdenum
0.421
0.0100
mg/L
0.400
0.00167
105
80-120
Nickel
0.421
0.0100
mg/L
0.400
0.000142
105
80-120
Potassium
23.5
0.500
mg/L
20.0
2.18
107
80-120
Selenium
0.429
0.0100
mg/L
0.400
-0.00383
107
80-120
Sodium
22.9
0.500
mg/L
20.0
1.64
106
80-120
Zinc
0.440
0.0100
mg/L
0.400
0.00145
110
80-120
Classical Chemistry Parameters - Quality Control
Batch OK03038 - NO PREP
Blank (OK03038-BLKS) Prepared: 11/03/2020 15:51 Analyzed: 11/03/2020 17:03
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes
Nitrite as N 0.017 U 0.10 mg/L
LCS (OK03038-BS3) Prepared: 11/03/2020 15:51 Analyzed: 11/03/2020 17:16
Spike Source O/oREC
RPD
Analvte
Result Flaa
POL
Units
Level Result O/oREC Limits RPD
Limit Notes
Nitrite as N
1.0
0.10
mg/L
1.00 104 90-110
Matrix Spike (OK03038-MS3)
Prepared: 11/03/2020 15:51 Analyzed: 11/03/2020 17:05
Source: CD16116-01
Spike Source O/oREC
RPD
Analvte
Result Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit Notes
Nitrite as N
1.3
0.10
mg/L
1.00 0.19 109 90-110
Matrix Spike Dup (OK03038-MSD1)
Prepared: 11/03/2020 15:51 Analyzed: 11/03/2020 17:06
Source: CD16116-01
Spike Source O/oREC
RPD
Analvte
Result Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit Notes
Nitrite as N
1.3
0.10
mg/L
1.00 0.19 108 90-110 0.8
10
Batch OK04011 - NO PREP
Blank (OK04011-BLK1)
Prepared & Analyzed: 11/04/2020 10:10
Spike Source O/oREC
RPD
Analvte
Result Flaq POL Units Level Result O/oREC Limits RPD
Limit Notes
Biochemical Oxygen Demand
2.0 U 2.0 mg/L
LCS (OK04011-BS3)
Prepared & Analyzed: 11/04/2020 10:10
Spike Source O/oREC
RPD
Analvte
Result Flaq POL Units Level Result O/oREC Limits RPD
Limit Notes
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 7 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OKO4O11 - NO PREP - Continued
LCS (OK04011-BS3) Continued Prepared & Analyzed: 11/04/2020 10:10
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Biochemical Oxygen Demand
200
2.0
mg/L
198
102 85-115
Duplicate (OK04011-DUPl)
Prepared & Analyzed: 11/04/2020 10:10
Source: CD12550-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Biochemical Oxygen Demand
2.4
2.0
mg/L
2.4
1
30
Batch OKO4O22 - NO PREP
Blank (OK04022-BLK1)
Prepared: 11/04/2020 12:37 Analyzed: 11/06/2020 11:07
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Suspended Solids
2.5
U
2.5
mg/L
LCS (OK04022-BS3)
Prepared: 11/04/2020 12:37 Analyzed: 11/06/2020 11:07
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Suspended Solids
99
2.5
mg/L
100 99 80-120
Duplicate (OK04022-DUPl)
Prepared: 11/04/2020 12:37 Analyzed: 11/06/2020 11:07
Source: CD16333-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Suspended Solids
35000
5000
mg/L
35000 1
20
Batch OKO4O34 - Same
Blank (OK04034-BLK1)
Prepared: 11/05/2020 08:52 Analyzed: 11/10/2020 11:51
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
0.025
U
0.10
mg/L
LCS (OK04034-BS1)
Prepared: 11/05/2020 08:52 Analyzed: 11/10/2020 12:43
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
1.6
0.10
mg/L
1.60 103 80-120
Matrix Spike (OK04034-MS1)
Prepared: 11/05/2020 08:52 Analyzed: 11/10/2020 12:45
Source: CD11731-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
1.0
0.10
mg/L
0.640 0.48 81 80-120
Matrix Spike Dup (OK04034-MSD1)
Prepared: 11/05/2020 08:52 Analyzed: 11/10/2020 12:47
Source: CD11731-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
1.3
0.10
mg/L
0.640 0.48 123 80-120 23
25
QM-07
Batch OKO4O35 - Same
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OK04035 - Same - Continued
Blank (OK04035-BLKS) Prepared: 11/05/2020 08:52 Analyzed: 11/10/2020 10:00
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Kjeldahl Nitrogen 0.26 U 0.48 mg/L
LCS (OK04035-BS3) Prepared: 11/05/2020 08:52 Analyzed: 11/10/2020 10:02
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
12
0.48
mg/L
12.0 102 90-110
Matrix Spike (OK04035-MS3)
Prepared: 11/05/2020 08:52 Analyzed: 11/10/2020 10:05
Source: CD11731-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
7.1
0.48
mg/L
4.80 2.3 100 90-110
Matrix Spike (OK04035-MS2)
Prepared: 11/05/2020 08:52 Analyzed: 11/10/2020 10:11
Source: CD11732-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
13
0.48
mg/L
4.80 8.5 94 90-110
Matrix Spike Dup (OK04035-MSD3)
Prepared: 11/05/2020 08:52 Analyzed: 11/10/2020 10:07
Source: CD11731-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
7.0
0.48
mg/L
4.80 2.3 98 90-110 1
10
Batch OK06006 - Same
Blank (OK06006-BLKi) Prepared: 11/06/2020 09:30 Analyzed: 11/06/2020 16:16
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Chemical Oxygen Demand 10 U 10 mg/L
LCS (OK06006-BS3) Prepared: 11/06/2020 09:30 Analyzed: 11/06/2020 16:16
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Chemical Oxygen Demand
520
10
mg/L
500
103
90-110
Matrix Spike (OK06006-MS3)
Prepared: 11/06/2020 09:30 Analyzed: 11/06/2020 16:16
Source: CD15950-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Chemical Oxygen Demand
750
10
mg/L
526
200
105
90-110
Matrix Spike Dup (OK06006-MSD3)
Prepared: 11/06/2020 09:30 Analyzed: 11/06/2020 16:16
Source: CD15950-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Chemical Oxygen Demand
730
10
mg/L
526
200
101
90-110 3
5
Batch OK06015 - NO PREP
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OKO6O15 - NO PREP - Continued
Blank (OK06015-BLKS)
Prepared & Analyzed: 11/06/2020 17:12
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Solids
0.0050
U
0.0050
% by Volume
LCS (OK06015-BS3)
Prepared & Analyzed: 11/06/2020 17:12
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Solids
1100
50
mg/L
1100 102 80-120
Duplicate (OK06015-DUP3)
Prepared & Analyzed: 11/06/2020 17:12
Source: CD16332-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Solids
0.22
0.010
% by Volume
0.23 4
20
Batch OKO6O23 - NO PREP
Blank (OK06023-BLKS)
Prepared: 11/06/2020 11:12 Analyzed: 11/06/2020 14:02
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
0.041
U
0.10
mg/L
LCS (OK06023-BS3)
Prepared: 11/06/2020 11:12 Analyzed: 11/06/2020 14:03
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
1.3
0.10
mg/L
1.25 105 90-110
Matrix Spike (OK06023-MS3)
Prepared: 11/06/2020 11:12 Analyzed: 11/06/2020 14:07
Source: CD11731-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
0.85
0.10
mg/L
0.521 0.29 107 90-110
Matrix Spike (OK06023-MS2)
Prepared: 11/06/2020 11:12 Analyzed: 11/06/2020 14:16
Source: CD14369-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
1.3
0.10
mg/L
0.521 0.71 116 90-110
QM-07
Matrix Spike Dup (OK06023-MSD3)
Prepared: 11/06/2020 11:12 Analyzed: 11/06/2020 14:09
Source: CD11731-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrate/Nitrite as N
0.87
0.10
mg/L
0.521 0.29 111 90-110 2
10
QM-07
Batch OKO9OO6 - NO PREP
Blank (OK09006-BLKi) Prepared: 11/09/2020 08:39 Analyzed: 11/09/2020 11:47
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Ammonia as N 0.045 U 0.10 mg/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OKO9OO6 - NO PREP - Continued
LCS (OK09006-BS1) Prepared: 11/09/2020 08:39 Analyzed: 11/09/2020 11:48
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
1.0
0.10
mg/L
1.01 104 90-110
Matrix Spike (OK09006-MS1)
Prepared: 11/09/2020 08:39 Analyzed: 11/09/2020 11:52
Source: CD12550-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
0.92
0.10
mg/L
0.393 0.54 97 90-110
Matrix Spike (OK09006-MS2)
Prepared: 11/09/2020 08:39 Analyzed: 11/09/2020 12:01
Source: CD14369-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
14
2.0
mg/L
8.08 7.2 83 90-110
QM-07
Matrix Spike Dup (OK09006-MSD1)
Prepared: 11/09/2020 08:39 Analyzed: 11/09/2020 11:54
Source: CD12550-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
0.91
0.10
mg/L
0.393 0.54 96 90-110 0.2
10
Batch OK1OO15 - EPA 3OO5A
Blank (OK10015-BLK1) Prepared: 11/10/2020 09:54 Analyzed: 11/11/2020 14:54
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Sodium Adsorption Ratio 0.00 U [blank]
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 13

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 13

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Analyses
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Times
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Due - -.
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Address
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Pro
Monthly -Week One -SBM
City/STltp
Frwftntm, NC 27525
PO 4 1 Billing Into
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Tel
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Fax
Reporting Contact
Scott Leech
Samplers) Name, Affiliation (Pint)
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as necessary)
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Time
Comp! Grab
Matrix
(see codes)
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Containers
Sample Comments
SBM
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7
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Date,Tme
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Note: All samples submitted to ENCO Labs are in accordance with the terms and conditions listed on the reverse of this form, unless prior written agreements exist

Sample Preservation Verification
ENCo Cary
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Work Order: CD16333 Project: Monthly - Week One - SBM
Client: Novozymes North America (NO008) Project #: [none]
Logged In: 03-Nov-20 11:13 n, Logged By: Rachel Ann Y nis } hh
Preservation Check Performed By: Date/Time:�� ! i�
CD16333-01
Con.
Type
Tres (pH).
Requirement
pH Checked /
I.n Control
pH Adjusted Date/Time
Adiested
Reagent Used/Comments
D
25pmLP+H2SO4
<2
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Y N I NA] 7] [ l
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250mLP+HNO3
<2
Y� N 1 NA
Y 1 N/ NA
i 4
Rea ent Name ID
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2 t`7?_?
pH Strip ID: PH Strips COF0555
Rea ent Name ID
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Reagent Name ID
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A
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2�SQ pCCgF ENCO Laboratories
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102-A Woodwinds Industrial Court
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Phone: [phone] FAX: [phone]
Wednesday, December 23, 2020
Novozymes North America (N0008)
Attn: Scott Creech
77 Perry Chapel Church Road
Franklinton, NC 27525
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: Monthly - Week One - SBM
ENCO Workorder(s): CD19099
Dear Scott Creech,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Thursday, December 3, 2020.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
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If you have any questions or require further information, please do not hesitate to contact me.
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Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 13

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: SBM
Lab ID: CD19099-01
Sampled: 12/03/20 00:15
Received: 12/03/20 10:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
CALC
NO PREP
08/29/23
12/23/20 09:06
12/23/20 09:06
CSU Method
NO PREP
08/29/23
12/07/20 09:32
12/08/20 13:38
EPA 350.1
Same
12/31/20
12/11/20 14:24
12/14/20 09:49
EPA 353.2
NO PREP
12/05/20 00:15
12/04/20 15:56
12/04/20 16:53
EPA 365.4
Same
12/31/20
12/10/20 10:43
12/15/20 13:24
EPA 6010D
EPA 3005A
06/01/21
12/07/20 09:32
12/08/20 10:43
EPA 7470A
EPA 7470A
12/31/20
12/07/20 10:43
12/08/20 15:55
SM 254OB-2011
NO PREP
12/10/20
12/04/20 18:32
12/04/20 18:32
SM 2540D-2011
NO PREP
12/10/20
12/07/20 16:50
12/07/20 16:50
SM 5210 B-2011
NO PREP
12/05/20 00:15
12/03/20 11:21
12/03/20 11:21
SM 5220D-2011
Same
12/31/20
12/04/20 09:30
12/04/20 12:42
Client ID: SBM
Lab ID: CD19099-01RE1
Sampled: 12/03/20 00:15
Received: 12/03/20 10:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 351.2
Same
12/31/20
12/10/20 10:38
12/15/20 08:08
Client ID: SBM
Lab ID: CD19099-01RE2
Sampled: 12/03/20 00:15
Received: 12/03/20 10:55
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
SM 450ONO3 H-2011
Same
12/31/20
12/09/20 15:45
12/10/20 12:24
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 13

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SAMPLE DETECTION SUMMARY
Client ID: SBM
Lab ID:
CD19099-01
Analvte
Results
Flag
MDL
Q
Units
Method Notes
Aluminum - Total
34.8
0.420
1.00
mg/L
EPA 6010D
Ammonia as N
50
D
0.98
2.0
mg/L
EPA 350.1
Biochemical Oxygen Demand
8600
2.0
2.0
mg/L
SM 5210 B-2011
Calcium - Total
2360
0.390
1.00
mg/L
EPA 6010D
Chemical Oxygen Demand
31000
800
800
mg/L
SM 5220D-2011
Magnesium - Total
14.1
0.290
1.00
mg/L
EPA 6010D
Nitrate as N
918
0.02
0.10
mg/L
CALC
Nitrite as N
2.5
D
0.084
0.50
mg/L
EPA 353.2
Phosphorus
56
D
0.40
0.60
mg/L
EPA 365.4
Potassium - Total
532
1.50
5.00
mg/L
EPA 6010D
Sodium - Total
468
4.00
5.00
mg/L
EPA 6010D
Sodium Adsorption Ratio 2.64 [blank] CSU Method
Total Solids 4.8 0.12 0.12 % by Volume SM 254OB-2011
Total Suspended Solids
2900
500
500
mg/L
SM 2540D-2011
Zinc - Total
0.0790
3 0.0440
0.100
mg/L
EPA 6010D
Client ID: SBM
Lab ID:
CD39099-01RE3
Analvte
Results
Flag MDL
POLL
Units
Method Notes
Total Kieldahl Nitrogen
1000
D 15
20
mq/L
EPA 351.2
Client ID: SBM Lab ID: CD39099-01RE2
Analvte Results Flag MDL POLL Units Method Notes
Nitrate/Nitrite as N 920 D 32 100 mg/L SM 450ONO3 H-2011
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 13

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ANALYTICAL RESULTS
Description: SBM Lab Sample ID:CD19099-01 Received: 12/03/20 10:55
Matrix: Sludge Sampled: 12/03/20 00:15 Work Order: CD19099
Project: Monthly - Week One - SBM Sampled By:John C Hilliard Jr
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
Mercury [7439-97-6]^
0.00150
u
mg/L
10
0.00150
0.00200
0L07031
EPA 7470A
12/08/20 15:55
KAH
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Ay
Notes
Aluminum [7429-90-5]^
34.8
mg/L
10
0.420
1.00
0L07014
EPA 6010D
12/08/20 10:43
JDH
Arsenic [7440-38-2]^
0.0760
u
mg/L
10
0.0760
0.100
0L07014
EPA 6010D
12/08/20 10:43
JDH
Cadmium [7440-43-9]^
0.00360
u
mg/L
10
0.00360
0.0100
0L07014
EPA 6010D
12/08/20 10:43
JDH
Calcium [7440-70-2]^
2360
mg/L
10
0.390
1.00
0L07014
EPA 6010D
12/08/20 10:43
JDH
Copper[7440-50-8]^
0.0160
u
mg/L
10
0.0160
0.100
0L07014
EPA 6010D
12/08/20 10:43
JDH
Lead [7439-92-1]^
0.0310
u
mg/L
10
0.0310
0.100
0L07014
EPA 6010D
12/08/20 10:43
JDH
Magnesium [7439-95-4]^
14.1
mg/L
10
0.290
1.00
0L07014
EPA 6010D
12/08/20 10:43
JDH
Molybdenum [7439-98-7]^
0.0250
u
mg/L
10
0.0250
0.100
0L07014
EPA 6010D
12/08/20 10:43
JDH
Nickel[7440-02-O]^
0.0220
u
mg/L
10
0.0220
0.100
0L07014
EPA 6010D
12/08/20 10:43
JDH
Potassium [7440-09-7]^
532
mg/L
10
1.50
5.00
0L07014
EPA 6010D
12/08/20 10:43
JDH
Selenium [7782-49-2]^
0.0620
u
mg/L
10
0.0620
0.100
0L07014
EPA 6010D
12/08/20 10:43
JDH
Sodium [7440-23-5]^
468
mg/L
10
4.00
5.00
0L07014
EPA 6010D
12/08/20 10:43
JDH
Zinc[7440-66-6]^
0.0790
J
mg/L
10
0.0440
0.100
0L07014
EPA 6010D
12/08/20 10:43
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Ay
Notes
Biochemical Oxygen Demand^
8600
mg/L
1
2.0
2.0
0L03006
SM 5210 B-2011
12/03/20 11:21
JOC
Chemical Oxygen Demand^
31000
mg/L
80
800
800
0L03031
SM 5220D-2011
12/04/20 12:42
JOC
Nitrate as N [14797-55-8]
918
mg/L
1
0.02
0.10
0L23008
CALC
12/23/20 09:06
UI
Nitrite as N [14797-65-0]^
2.5
D
mg/L
5
0.084
0.50
0L04027
EPA 353.2
12/04/20 16:53
JAH
Sodium Adsorption Ratio
2.64
[blank]
1
0L07014
CSU Method
12/08/20 13:38
JDH
Total Solids^
4.8
% by Volume
25
0.12
0.12
0L04030
SM 2540B-2011
12/04/20 18:32
DMJ
Total Suspended Solids^
2900
mg/L
200
500
500
0L07021
SM 2540D-2011
12/07/20 16:50
DMJ
Classical Chemistry Parameters
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
Ammonia as N [7664-41-7]
50
D
mg/L
100
0.98
2.0
0L11034
EPA 350.1
12/14/20 09:49
cbarr
Nitrate/Nitrite as N
920
D
mg/L
2000
32
100
0L09048
M 450ONO3 H-201
12/10/20 12:24
cbarr
Phosphorus[7723-14-O]^
56
D
mg/L
20
0.40
0.60
0L10030
EPA 365.4
12/15/20 13:24
cbarr
Total Kjeldahl Nitrogen
1000
D
mg/L
400
15
20
0L10026
EPA 351.2
12/15/20 08:08
cbarr
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 13

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch OLO7O31 - EPA 747OA
Blank (OL07031-BLK1) Prepared: 12/07/2020 10:43 Analyzed: 12/08/2020 14:51
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Mercury 0.000150 U 0.000200 mg/L
LCS (OL07031-BS3) Prepared: 12/07/2020 10:43 Analyzed: 12/08/2020 14:53
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00490
0.000200
mg/L
0.00500
98
80-120
Matrix Spike (OL07031-MS3)
Prepared: 12/07/2020 10:43 Analyzed: 12/08/2020 15:39
Source: CD19358-02
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00423
0.000200
mg/L
0.00500
0.000185
81
75-125
Matrix Spike Dup (OL07031-MSD1)
Prepared: 12/07/2020 10:43 Analyzed: 12/08/2020 15:46
Source: CD19358-02
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
0.00423
0.000200
mg/L
0.00500
0.000185
81
75-125 0
25
Post Spike (OL07031-PS1)
Prepared: 12/07/2020 10:43 Analyzed: 12/08/2020 15:11
Source: CD19358-02
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
4.17
0.200
ug/L
5.00
0.185
80
75-125
Metals (total recoverable) by EPA 6000/7000
Series Methods - Quality Control
Batch OLO7O14 - EPA 3OO5A
Blank (OL07014-BLK3)
Prepared: 12/07/2020 09:32 Analyzed: 12/08/2020 10:03
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Aluminum
0.0420
U
0.100
mg/L
Arsenic
0.00760
U
0.0100
mg/L
Cadmium
0.000360
U
0.00100
mg/L
Calcium
0.0390
U
0.100
mg/L
Copper
0.00160
U
0.0100
mg/L
Lead
0.00310
U
0.0100
mg/L
Magnesium
0.0290
U
0.100
mg/L
Molybdenum
0.00250
U
0.0100
mg/L
Nickel
0.00220
U
0.0100
mg/L
Potassium
0.150
U
0.500
mg/L
Selenium
0.00620
U
0.0100
mg/L
Sodium
0.400
U
0.500
mg/L
Zinc
0.00440
U
0.0100
mg/L
Blank (OL07014-BLK2)
Prepared: 12/07/2020 09:32 Analyzed: 12/08/2020 10:06
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Aluminum 0.0420 U 0.100 mg/L
Arsenic 0.00760 U 0.0100 mg/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 13

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch OLO7O14 - EPA 3OO5A - Continued
Blank (OL07014-BLK2) Continued Prepared: 12/07/2020 09:32 Analyzed: 12/08/2020 10:06
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units Level Result %REC Limits RPD Limit Notes
Cadmium
0.000360
U
0.00100
mg/L
Calcium
0.0390
U
0.100
mg/L
Copper
0.00160
U
0.0100
mg/L
Lead
0.00310
U
0.0100
mg/L
Magnesium
0.0290
U
0.100
mg/L
Molybdenum
0.00250
U
0.0100
mg/L
Nickel
0.00220
U
0.0100
mg/L
Potassium
0.150
U
0.500
mg/L
Selenium
0.00620
U
0.0100
mg/L
Sodium
0.400
U
0.500
mg/L
Zinc
0.00440
U
0.0100
mg/L
LCS (OL07014-BSI)
Prepared: 12/07/2020 09:32 Analyzed: 12/08/2020 10:11
Spike
Source
%REC RPD
Analvte
Result
Flaq POL
Units
Level
Result %REC
Limits RPD Limit Notes
Aluminum
2.16
0.100
mg/L
2.00
108
80-120
Arsenic
0.215
0.0100
mg/L
0.200
107
80-120
Cadmium
0.0210
0.00100
mg/L
0.0200
105
80-120
Calcium
2.20
0.100
mg/L
2.00
110
80-120
Copper
0.207
0.0100
mg/L
0.200
103
80-120
Lead
0.210
0.0100
mg/L
0.200
105
80-120
Magnesium
2.20
0.100
mg/L
2.00
110
80-120
Molybdenum
0.203
0.0100
mg/L
0.200
101
80-120
Nickel
0.216
0.0100
mg/L
0.200
108
80-120
Potassium
10.7
0.500
mg/L
10.0
107
80-120
Selenium
0.204
0.0100
mg/L
0.200
102
80-120
Sodium
10.9
0.500
mg/L
10.0
109
80-120
Zinc
0.215
0.0100
mg/L
0.200
108
80-120
Matrix Spike (OL07014-MS1)
Prepared:
12/07/2020 09:32 Analyzed: 12/08/2020 10:14
Source: CD19092-10
Spike
Source
%REC RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD Limit Notes
Aluminum
2.17
0.100
mg/L
2.00
0.258
96
75-125
Arsenic
0.202
0.0100
mg/L
0.200
0.00760 U
101
75-125
Cadmium
0.0193
0.00100
mg/L
0.0200
0.000360 U
96
75-125
Calcium
98.9
0.100
mg/L
2.00
96.6
113
75-125
Copper
0.192
0.0100
mg/L
0.200
0.00160 U
96
75-125
Lead
0.195
0.0100
mg/L
0.200
0.00310 U
97
75-125
Magnesium
40.2
0.100
mg/L
2.00
38.2
100
75-125
Molybdenum
0.200
0.0100
mg/L
0.200
0.00250 U
100
75-125
Nickel
0.201
0.0100
mg/L
0.200
0.00220 U
101
75-125
Potassium
13.3
0.500
mg/L
10.0
3.04
103
75-125
Selenium
0.194
0.0100
mg/L
0.200
0.00620 U
97
75-125
Sodium
38.8
0.500
mg/L
10.0
28.8
100
75-125
Zinc
0.204
0.0100
mg/L
0.200
0.00570
99
75-125
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 13

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch OL07014 - EPA 3005A - Continued
Matrix Spike Dup (OL07014-MSDI)
Prepared: 12/07/2020 09:32 Analyzed: 12/08/2020 10:17
Source: CD19092-10
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit
Notes
Aluminum
2.35
0.100
mg/L
2.00
0.258
105
75-125
8
20
Arsenic
0.194
0.0100
mg/L
0.200
0.00760 U
97
75-125
4
20
Cadmium
0.0191
0.00100
mg/L
0.0200
0.000360 U
95
75-125
1
20
Calcium
98.3
0.100
mg/L
2.00
96.6
83
75-125
0.6
20
Copper
0.190
0.0100
mg/L
0.200
0.00160 U
95
75-125
0.8
20
Lead
0.191
0.0100
mg/L
0.200
0.00310 U
96
75-125
2
20
Magnesium
40.4
0.100
mg/L
2.00
38.2
107
75-125
0.4
20
Molybdenum
0.197
0.0100
mg/L
0.200
0.00250 U
99
75-125
2
20
Nickel
0.199
0.0100
mg/L
0.200
0.00220 U
99
75-125
1
20
Potassium
13.3
0.500
mg/L
10.0
3.04
103
75-125
0.2
20
Selenium
0.195
0.0100
mg/L
0.200
0.00620 U
97
75-125
0.5
20
Sodium
38.6
0.500
mg/L
10.0
28.8
99
75-125
0.3
20
Zinc
0.202
0.0100
mg/L
0.200
0.00570
98
75-125
1
20
Post Spike (OL07014-PS1)
Prepared: 12/07/2020 09:32 Analyzed: 12/08/2020 10:19
Source: CD19092-10
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit
Notes
Aluminum
2.43
0.100
mg/L
2.00
0.258
109
80-120
Arsenic
0.201
0.0100
mg/L
0.200
-0.00938
100
80-120
Cadmium
0.0203
0.00100
mg/L
0.0200
-0.000464
102
80-120
Calcium
96.9
0.100
mg/L
2.00
96.6
12
80-120
QM-08
Copper
0.203
0.0100
mg/L
0.200
-0.00757
101
80-120
Lead
0.206
0.0100
mg/L
0.200
-0.000223
103
80-120
Magnesium
39.7
0.100
mg/L
2.00
38.2
73
80-120
QM-08
Molybdenum
0.212
0.0100
mg/L
0.200
9.51E-5
106
80-120
Nickel
0.213
0.0100
mg/L
0.200
0.00161
105
80-120
Potassium
14.0
0.500
mg/L
10.0
3.04
109
80-120
Selenium
0.208
0.0100
mg/L
0.200
-0.0128
104
80-120
Sodium
39.0
0.500
mg/L
10.0
28.8
103
80-120
Zinc
0.216
0.0100
mg/L
0.200
0.00570
105
80-120
Classical Chemistry Parameters - Quality Control
Batch OL03006 - NO PREP
Blank (OL03006-BLK3) Prepared & Analyzed: 12/03/2020 11:21
Spike Source %REC RPD
Analvte Result Flaa POL Units Level Result %REC Limits RPD Limit Notes
Biochemical Oxygen Demand 2.0 U 2.0 mg/L
LCS (OL03006-BSI) Prepared & Analyzed: 12/03/2020 11:21
Spike Source %REC
RPD
Analvte
Result Flaq POL Units Level Result %REC Limits RPD
Limit Notes
Biochemical Oxygen Demand
180 2.0 mg/L 198 90 85-115
Duplicate (011-03006-DU131)
Prepared & Analyzed: 12/03/2020 11:21
Source: CD17759-01
Spike Source %REC
RPD
Analvte
Result Flaq POL Units Level Result %REC Limits RPD
Limit Notes
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 7 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OL03006 - NO PREP - Continued
Duplicate (01-03006-DU131) Continued Prepared & Analyzed: 12/03/2020 11:21
Source: CD17759-01
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Biochemical Oxygen Demand 1500 2.0 mg/L 1400 5 30
Batch OL03031 - Same
Blank (OL03031-BLK3) Prepared: 12/04/2020 09:30 Analyzed: 12/04/2020 12:42
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chemical Oxygen Demand
10
U
10
mg/L
LCS (OL03031-BSI)
Prepared: 12/04/2020 09:30 Analyzed: 12/04/2020 12:42
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chemical Oxygen Demand
530
10
mg/L
500 105 90-110
Matrix Spike (OL03031-MS3)
Prepared: 12/04/2020 09:30 Analyzed: 12/04/2020 12:42
Source: CD16327-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chemical Oxygen Demand
3400
40
mg/L
2000 1500 95 90-110
Matrix Spike Dup (OL03031-MSD1)
Prepared: 12/04/2020 09:30 Analyzed: 12/04/2020 12:42
Source: CD16327-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Chemical Oxygen Demand
3500
40
mg/L
2000 1500 100 90-110 3
5
Batch OL04027 - NO PREP
Blank (OL04027-BLK3)
Prepared: 12/04/2020 15:56 Analyzed: 12/04/2020 16:13
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
0.017
U
0.10
mg/L
LCS (OL04027-BS1)
Prepared: 12/04/2020 15:56 Analyzed: 12/04/2020 16:32
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
1.0
0.10
mg/L
1.00 103 90-110
Matrix Spike (OL04027-MS3)
Prepared: 12/04/2020 15:56 Analyzed: 12/04/2020 16:15
Source: CD19503-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
1.0
0.10
mg/L
1.00 0.021 101 90-110
Matrix Spike Dup (OL04027-MSDI)
Prepared: 12/04/2020 15:56 Analyzed: 12/04/2020 16:16
Source: CD19503-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Nitrite as N
1.0
0.10
mg/L
1.00 0.021 98 90-110 2
10
Batch OL04030 - NO PREP
FINAL This
report relates only to
the sample as received by the
laboratory, and may only be reproduced in full.
Page 8 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OL04030 - NO PREP - Continued
Blank (OL04030-BLK1)
Prepared & Analyzed: 12/04/2020 18:32
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Total Solids
0.0050
U
0.0050
% by Volume
LCS (OL04030-BS1)
Prepared & Analyzed: 12/04/2020 18:32
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Total Solids
1100
50
mg/L
1100 101 90-110
Duplicate (OL04030-DUPl)
Prepared & Analyzed: 12/04/2020 18:32
Source: CD17846-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Total Solids
0.31
0.010
% by Volume
0.31
0.1
5
Batch OL07014 -EPA 3005A
Blank (OL07014-BLK1)
Prepared: 12/07/2020 09:32 Analyzed: 12/08/2020 13:39
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Sodium Adsorption Ratio
0.00
U
[blank]
Blank (OL07014-BLK2)
Prepared: 12/07/2020 09:32 Analyzed: 12/08/2020 13:39
Spike Source %REC
RPD
Analvte
Result
Flaa
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Sodium Adsorption Ratio
0.00
U
[blank]
Batch OL07021 - NO PREP
Blank (OL07021-BLK3)
Prepared & Analyzed: 12/07/2020 16:50
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Total Suspended Solids
2.5
U
2.5
mg/L
LCS (OL07021-BS1)
Prepared & Analyzed: 12/07/2020 16:50
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Total Suspended Solids
96
2.5
mg/L
100 96 80-120
Duplicate (OL07021-DUPl)
Prepared & Analyzed: 12/07/2020 16:50
Source: CD17844-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Total Suspended Solids
160
50
mg/L
160
3
20
Duplicate (OL07021-DUP2)
Prepared & Analyzed: 12/07/2020 16:50
Source: CD17845-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits
RPD
Limit
Notes
Total Suspended Solids
170
50
mg/L
190
10
20
Classical Chemistry Parameters - Quality Control
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 9 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OL09048 - NO PREP
Blank (OL09048-BLK3) Prepared: 12/09/2020 15:45 Analyzed: 12/10/2020 11:06
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Nitrate/Nitrite as N 0.016 U 0.050 mg/L
LCS (OL09048-BSI) Prepared: 12/09/2020 15:45 Analyzed: 12/10/2020 11:07
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Nitrate/Nitrite as N
0.54
0.050
mg/L
0.500
108
84-116
Matrix Spike (OL09048-MS1)
Prepared: 12/09/2020 15:45 Analyzed: 12/10/2020 11:43
Source: AD08323-02
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Nitrate/Nitrite as N
0.55
0.050
mg/L
0.500
0.021
105
84-116
Matrix Spike Dup (OL09048-MSD1)
Prepared: 12/09/2020 15:45 Analyzed: 12/10/2020 11:44
Source: AD08323-02
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Nitrate/Nitrite as N
0.56
0.050
mg/L
0.500
0.021
108
84-116 3
10
Batch OL10026 - NO PREP
Blank (OL30026-BLK3) Prepared: 12/1O/2020 10:38 Analyzed: 12/15/2020 07:47
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Total Kjeldahl Nitrogen 0.037 U 0.050 mg/L
LCS (OL10026-BS1) Prepared: 12/10/2020 10:38 Analyzed: 12/15/2020 07:48
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
2.7
0.050
mg/L
2.50 108 90-110
Matrix Spike (OL10026-MS2)
Prepared: 12/10/2020 10:38 Analyzed: 12/15/2020 07:51
Source: AD08257-02
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
4.8
0.050
mg/L
2.50 2.2 104 90-110
Matrix Spike (OL10026-MS3)
Prepared: 12/10/2020 10:38 Analyzed: 12/15/2020 08:17
Source: AD08357-OIREI
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
370
D
5.0
mg/L
2.50 380 NR 90-110
QM-07
Matrix Spike Dup (OL10026-MSD3)
Prepared: 12/10/2020 10:38 Analyzed: 12/15/2020 08:19
Source: AD08357-01RE1
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Total Kjeldahl Nitrogen
370
D
5.0
mg/L
2.50 380 NR 90-110 0.3
10
QM-07
Batch OL10030 - NO PREP
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 13

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OL1003O - NO PREP - Continued
Blank (OL30030-BLK1) Prepared: 12/10/2020 10:43 Analyzed: 12/15/2020 12:28
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Phosphorus 0.020 U 0.030 mg/L
LCS (OL10030-BS1) Prepared: 12/10/2020 10:43 Analyzed: 12/15/2020 12:30
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
2.5
0.030
mg/L
2.50 99 90-110
Matrix Spike (OL10030-MSI)
Prepared: 12/10/2020 10:43 Analyzed: 12/15/2020 13:12
Source: AD08357-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
53
D
0.60
mg/L
2.50 53 NR 90-110
QM-07
Matrix Spike Dup (OL10030-MSD1)
Prepared: 12/10/2020 10:43 Analyzed: 12/15/2020 13:13
Source: AD08357-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Phosphorus
52
D
0.60
mg/L
2.50 53 NR 90-110 2
10
QM-07
Batch OL11O34 - NO PREP
Blank (OL31034-BLK3) Prepared: 12/11/2020 14:24 Analyzed: 12/14/2020 09:28
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Ammonia as N 0.0098 U 0.020 mg/L
LCS (OL11034-BSI) Prepared: 12/11/2020 14:24 Analyzed: 12/14/2020 09:29
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
0.98
0.020
mg/L
1.00 98 90-110
Matrix Spike (OL13034-MS1)
Prepared: 12/11/2020 14:24 Analyzed: 12/14/2020 09:34
Source: AD08306-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
1.9
0.020
mg/L
1.00 0.97 94 90-110
Matrix Spike (OL13034-MS3)
Prepared: 12/11/2020 14:24 Analyzed: 12/14/2020 09:53
Source: AD08309-01RE3
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
6.3
D
0.10
mg/L
1.00 5.4 95 90-110
Matrix Spike Dup (OL33034-MSDI)
Prepared: 12/11/2020 14:24 Analyzed: 12/14/2020 09:35
Source: AD08306-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Ammonia as N
1.9
0.020
mg/L
1.00 0.97 94 90-110 0
10
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 13

(� �Eo
www.encolabs.com
FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 13

ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com
CO 10775 Central Port Dr 4810 Executive Park Court, Suite 111 102-A Woodwinds industrial Ct.
Orlando, FL 32824 Jacksonville, FL 32216-6069 Cary, NC 27511
CS [phone] [phone] Fax [phone] {919) 467-3090 Fax [phone] Page of
Client Name Project Number Requested Analyses Requested Turnaround
Nava es North America N0008 none Times
Address Project NameiDesc st C1
I w! ?a Note : fiUSh regUeS[5 SUbjBL[ tP
77 Perry Chapel Church Road Monthly - Week One - SBM g acceptance by the facility
City15T21p Po # / Billing Info yZQ' cl. O
FrankGnton, NC 27525 3800466333 ap ❑ pO F ❑ ` Standard
Te} Fax Reporting Contact c
[phone] Scott Creech 7, LO to _Expedited
Sampier(s) Name, Miialio (Print)) Billing Contact E
Z
o r':ids Accounts Payable inU) �yh Due I�I
Sample ) Sig ure Site Location ! Time Zone j ru O 0 xT Lab Workorder
ll� ems' ` /� Q cM m i Z �rQ gQ99
Preservation {See Codes) (Combine as necessary)
Collection Matrix Total of
Item # Sample ID (Feld Identification) Collection Dale Time Camp: Grab (see codes) Containers Sampie Comments
SaM ,' '�1"v �,:� ?+� SL 7 X X X X X X
t
Total # of Containers
Sample Kit Prepared By
Date -Time
Relinquished By A
Datol ime
l9-1- 06,
Rec ved By
Datefrime
20 �D 3
CommentsiSpecial Reporting Requirements
Rel nquished By
DatelTime
Received By
Datefl-Ime
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Relinquished By
DaterTme
eceived By
DaterFlme
ler #'s & Temps on Receipt `
Condition Upon Receipt
r
Acceptable Unacceptabte
Matrix : GW-Groundwaler SO -Soil DW-Drinking Water SE -Sediment SW -Surface Water WW-Wastewater A -Air O-Other (detail in comments) Preservation: trice H.HCI N-HNO3 S-H2SO4 NO-NaOH O-Other (detail in comments)
Note : All samples submitted to ENCD Labs are in accordance with the terms and conditions listed on the reverse of INs form, unless prior written agreements exist

Sample Preservation Verification
ENCO Cary C
Da�
99Work Order: CD19099 Project: Monthly - Week One - SBM
Client: Novozymes North America (NO008) Project #: [none]
Logged In: 03-Dec-20 12:04 Logged By: Rachel Ann Yo ish t
Preservation Check Performed By: 7� Date/Time: V 7Z'� } l 1
CD19099-01
Cont
Type
Pres (pH)
Requirement
pH Checked 1
In Control
pH Adjusted Daterrime
Adjusted
Reagent Used/Comments
D
250mLP+H2SO4
<2
Y`/ N / NA
/ N / NA4Lm
L�-
E
250mLP+HNO3
<2
Y N / NA I
Y 1/ N / NA'
R a ent Name ID
1 _a 11 lq c)
2 F�JD Z.t1
pH Strip ID:
PH Strips COF0555
C:\elmnt\Prir,.,..,kj_11 Gaci vauvnt-.neGK, rpt
Reacient Name ID
3
4
Rea ent Name ID
5
6
Page 1 of 1

BRANCH RESIDUALS & SOILS, LLC
1735 Heckle Blvd. Suite 103-291, Rock Hill SC, 29732
PHONE [phone] • Cell [phone]
March 22, 2021
Novozymes North America, Inc.
77 Perry Chapel Road
Franklinton, NC 27525
Attention: Mr. Steve Stadelman
Manager/Specialist
Reference: REVISED TECHNICAL ASSISTANCE DISTRIBUTION PERMIT
Novozymes Franklinton, NC Facility
Branch Residuals & Soils, LLC Project No 2019-129
Dear Mr. Stadelman:
In fulfillment of Branch Residuals & Soils BRS Proposal 2020-6 dated October 28, 2020 Letter of
Authorization 2020-1 and Novozymes North America Purchase Order 4551062089, the following
report was prepared. Several tasks have been performed in support of a permit modification of
North Carolina Department of Environmental Quality (NCDEQ) permit WQ0003487, a Class A
residuals distribution permit. Novozymes provided the analytical data for Branch Residuals &
Soils to complete Items 5c, 5d, 5e, and 6 of the Residual Source Certification Attachment (RSCA).
Novozymes will be implementing a reverse osmosis unit (RO) in support of their pursuit of a North
Carolina discharge permit of ongoing operations in Franklinton, NC. The non -captured fraction
will be discharged and the captured fraction or RO rejects will be mixed with the spent biomass
(SBM) that is currently regulated under WQ0003487. Novozymes performed a pilot study in 2020
and provided an updated table on March 18. 2021 with production adjusted average SBM and
average concentrations of RO rejects (Attachment A). This analytical table is used to calculate the
inputs needed for items 5c — 6 in the RSCA. A copy of the RSCA has been included as Attachment
B.

Revised Technical Assistance — Distribution Permit
Novozymes Franklinton, NC
BR&S Project No. 2019-129
March 22, 2021
Item 5c Calculation of Sodium Adsorption Ratio (SAR). The SAR based on the information
provided is 5.02.
Item 5d. Mineralization rate. The mineralization rate for the average SBM plus RO rejects
should be 40%. This is different than listed in the permit which is 30% and assumes aerobic
treatment. Based on discussions with Novozymes, Novozymes commissioned a North Carolina
State University mineralization study on the SBM. The results of this study yielded a first -year
mineralization of 40%. This value should be listed as actually established based on the NC state
study.
Item 5e. Calculation of first year and five-year Plant Available Nitrogen (PAN).
Application Method
First (V) Year PAN
Five -Year
Maximum Adjusted PAN
(mg1k_9)
(mg1k_9)
Surface
15,951
21,897
Injection/Incorporation
17,002
22,948
The first -year and five-year PAN are calculated as seen in Attachment C. The formulas for PAN
surface and PAN injected or incorporated are as follows:
WZ
PANs„,= [(MR) x (TKN-NH3)] + [0.5 x (NH3)] + (NO3-NO2-N)
PANi„j= [(MR) x (TKN-NH3)] + (NH3) + (NO3-NO2-N)
Where:
TKN = Total Kjeldahl Nitrogen
NH3 = Ammonia Nitrogen
NO3-NO2 = Nitrate — Nitrite Nitrogen
MR = Mineralization Rate
Five -Year PAN surface was calculated using mineralization rates at 'h from the previous year
using EPA Guidance (i.e. 2"d year was 20% of the remaining organic nitrogen, Yd year was 10%
of the remaining organic nitrogen, 41h year was 5% of the remaining organic nitrogen and 51h year
2

Revised Technical Assistance — Distribution Permit BR&S Project No. 2019-129
Novozymes Franklinton, NC March 22, 2021
was 2.5% of the remaining organic nitrogen. The totaled PAN amounts contributed from years 2-
5 was 5,946 mg/Kg. The 1st year PAN (15,951 mg/Kg) plus 6,526.03 yields the five-year PANsur
of 21,897 mg/Kg.
Item 6.Other Pollutants Determination
Based on the data provided by Novozymes, concern was express for the increased salt load to the
land application and distribution of these residuals. During 2020, a plot study was performed to
determine if there were any impacts that were noted by adding the RO reject to the SBM. The
initial data indicated no statistical differences in soil and crop uptake between the SBM and the
SBM plus RO rejects. This study was a first step. Applications going forward will follow the
protocol identified in the Novozymes Crop Management Plan that will include additional soil and
plant testing in an effort to prevent any adverse effects to the crop or soil.
Site Life Calculations
Attached are site life calculations based on 40 CFR Part 503 metal limits and 40 CFR Part 257
Cation Exchange Capacity (CEC). The 257 regulations promulgated total metal ceiling levels of
five metals which were dependent on the soil's CEC. These regulations had three levels
corresponding to the soil's CEC; 0-5 milliequivalents/100grams (meq/100g), 5-15 meq/100g, and
15+ meq/100g. The 257 regulations were precursors to the Part 503 and only included levels for
cadmium, copper, lead, nickel, and zinc.
The following three rates were used:
• 24,836 gallons per acre (worst case scenario) would provide 150 pounds PAN/Acre/year,
• 6,000 gallons per acre (normal Novozymes application rate — single application) would
provide 36.24 pounds PAN/Acre/year, and
• 12,000 gallons per acre (occasional Novozymes application rate — application occurring
twice in a year) that would provide 72.48 pounds PAN/Acre/year.
The site life determinations are found in Attachment D.
3

Revised Technical Assistance — Distribution Permit BR&S Project No. 2019-129
Novozymes Franklinton, NC March 22, 2021
CLOSING REMARKS
Thank you for allowing BR&S the opportunity to perform this work as defined from your accepted
proposal. Please give me a call if you have any questions or comments about the issues raised in
this report.
Sincerely,
Robert T. Branch, L.S.S.
Soil Scientist/Owner
Attachments:
Attachment A: Novozymes Average SBM and Average RO Reject Data
Attachment B: Residuals Source Certification Attachment
Attachment C: PAN Calculations
Attachment D: Site life Calcualtions for Three Application Rates
4

Attachment A
Novozymes Average SBM and Average RO Reject Data

Novozymes Adjusted Average SBM and Average RO Reject 3/18/21
Flow
862003 L
Percent Solids (%)
4.54
Arsenic
0.07 mg/L
1.475 mg/kg
Cadmium
0.00 mg/L
0.070 mg/kg
Copper
0.21 mg/L
4.623 mg/kg
Lead
0.03 mg/L
0.612 mg/kg
Mercury
0.00 mg/L
0.024 mg/kg
Molybdenum
0.03 mg/L
0.733 mg/kg
Nickel
0.05 mg/L
0.994 mg/kg
Selenium
0.05 mg/L
1.204 mg/kg
Zinc
0.52 mg/L
11.444 mg/kg
Aluminium
112.53 mg/L
2478 mg/kg
Ammonia
95.50 mg/L
2103 mg/kg
Calcium
3222.61 mg/L
70963 mg/kg
Magnesium
40.45 mg/L
891 mg/kg
Nitrate -Nitrite
136.18 mg/L
2999 mg/kg
Phosphorus
488.55 mg/L
10758 mg/kg
Potassium
1112.75 mg/L
24503 mg/kg
Sodium
1047.32 mg/L
23062 mg/kg
TKN
1446.57 mg/L
31854 mg/kg
TN
1582.74 mg/L
34853 mg/kg
Chloride
990 mg/L
21802 mg/kg
TDS
18307 mg/L
403126 mg/kg

Attachment B
Residuals Source Certification Attachment

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
INSTRUCTIONS FOR FORM: RSC 06-16
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and
supporting documentation
For more information, visit the TVater Quality Permitting Section's Non -Discharge Permitting Unit
General — This certification provides detailed information of residuals source generating facility and its residuals quality for land
application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without
a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15).
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Residuals Source Certification (FORM: RSC 11-15):
❑ Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not
make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the
application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer.
❑ For new or renewed permits, submit a separate certification for each source facility.
❑ For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification.
❑ Complete the residuals source facility summary page. List all new, renewed, or modified facilities.
B. Residuals Source -Generating Facility Information:
❑ For each source facility, attach the following:
❑ Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance for
Residuals Land Application Permits".
❑ Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals
are to be generated, treated, processed, and stored at the facility.
❑ Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8.
Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of
the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed,
and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during
processing.
❑ Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies
sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition,
ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and
vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as
they are to be land applied, distributed, and/or disposed.
C. Residuals Quality Information:
❑ For each source facility, attach the following:
❑ Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification.
❑ Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector
attraction reduction requirements.
❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please
attach analytical results of residuals generated from a similar facility along with the description of similarities of the two
facilities.
INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1

RESIDUALS SOURCE FACILITY SUMMARY
Applicant's name:
Status Maximum Dry Tons Per Year
Facility Permit Holder Facility Name County Permit Number
Code a Current Proposed
a Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted)
b The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility).
SUMMARY FOR FORM: RSC 06-16 Page 1

I.
State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: L 2 . _i
2. Facility permit holder is: ❑ Federal, 0 State, ❑ Local Government, or ❑ Private.
Facility permit issued by: ❑ Div. of Water Resources, ❑ Div. of Environmental Health,
or ❑ Other (explain: K F 7 J).
3. Facility contact person and title:
Complete mailing address: .-
City: State: i Zip: F
Telephone number: (_) _ E-mail address:^ �J
4. Facility physical address:
City: State: Zip: f r-' 1
Coordinates: Latitude: _ _' _" Longitude:_' {_1"
Datum: Level of accuracy: '
Method of measurement:
5. Purpose of the facility:
❑ treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater,
❑ treatment of potable water, ❑ treatment of 100% industrial wastewater,
❑ treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: ' % industrial and % domestic)
❑ other (explain: ).
6. Does the facility have an approved pretreatment program: ❑ Yes ❑ No
7. Facility permitted/design flow: - MGD and facility average daily flow: . MGD
8. Average amount of residuals being generated at this facility I , dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment:
Type and volume of residuals storage (i.e., outside of residuals treatment units):
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
❑ 40 CFR Part 503 or ❑ 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
❑ Biological ❑ Non -Biological
Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
FORM: RSC 06-16 Page 1 of 5

3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes ❑ no.
If yes, list the number(s):
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: ❑ yes 0 no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: i and Date of analysis:
Passed corrosivity test: ❑ yes ❑ no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: ❑ yes ❑ no. Flashpoint: OF (> 140°F)
Passed reactivity test: ❑ yes ❑no. HCN: mg/kg (<250) & H2S: mg/kg (<500)
TCLP Parameter
Limit
(mg/1)
Result
(mg/1)
TCLP Parameter
Limit
(mg/1)
Result
(mg/1)
Arsenic
5.0
Hexachlorobenzene
0.13
Barium
100.0
Hexachloro-1,3-Butadiene
0.5
Benzene
0.5
Hexachloroethane
3.0
Cadmium
1.0
Lead
5.0
Carbon Tetrachloride
0.5
Lindane
0.4
Chlordane
0.03
Mercury
0.2
Chlorobenzene
100.0
Methoxychlor
10.0
Chloroform
6.0
Methyl Ethyl Ketone
200.0
Chromium
5.0
Nitrobenzene
2.0
m-Cresol
200.0
Pentachlorophenol
100.0
o-Cresol
200.0
Pyridine
5.0
p-Cresol
200.0
Selenium
1.0
Cresol
200.0
Silver
5.0
2,4-D
10.0
Tetrachloroethylene
0.7
1,4-Dichlorobenzene
7.5
Toxaphene
0.5
1,2-Dichloroethane
0.5
Trichloroethylene
0.5
1, 1 -Dichloroethylene
0.7
2,4,5-Trichlorophenol
400.0
2,4-Dinitrotoluene
0.13
2,4,6-Trichlorophenol
2.0
Endrin
0.02
2,4,5-TP (Silvex)
1.0
Heptachlor and its Hydroxide
0.008
Vinyl Chloride
0.2
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: and Date of analysis: F"-"
Parameter
Ceiling
Concentration Limits
(C1assA & ClassB)
(mg/k-g)
Monthly Average
Concentration Limits
(Class A Only)
(mglk-g)
Result
(mglk-g)
Arsenic
75
41
Cadmium
85
39
Copper
4,300
1,500
Lead
840
300
Mercury
57
17
Molybdenum
75
n/a
Nickel
420
420
Selenium
100
100
Zinc
7,500
2,800
b. For Surface Disposal Unit Rand ill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: and Date of analysis:
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mglk-g)
Chromium
(mg/kg)
Nickel
(mg/kg)
❑ > 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
❑ > 100 but < 125
53
360
390
❑ > 125
62
450
420
Result (nig/kg)
FORM: RSC 06-16 Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: !"_l %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: and Date of analysis:
Parameter
Result
(mg/kg)
Aluminum
Ammonia -Nitrogen
Calcium
Magnesium
Nitrate -Nitrite Nitrogen
pH (Standard Unit)
Phosphorus
Potassium
Sodium
Total Kjeldahl Nitrogen
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR):
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: L
This rate is a (check one): 0 default value, or EJ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals: r
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (15t) Year PAN
Five -Year
Maximum Adjusted PAN
(mg1kg)
(mg/kg)
Surface
Injection/Incorporation
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses:
FORM: RSC 06-16 Page 4 of 5

7. Pathoeen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
❑ Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance.
❑ Alternative 2 [15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment.
❑ Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
0 Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of Class B:
❑ Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration.
❑ Alternative 2 [15A NCAC 02T.I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑ aerobic digestion, ❑ air drying, ❑ anaerobic digestion,
❑ composting, or ❑ lime stabilization.
c. For Surface Disposal:
❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)].
❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
❑ Alternative 1 [15A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
❑ Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
❑ Alternative 4 [15A NCAC 02T.1107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
❑ Alternative 5 [15A NCAC 02T.1107(a)(5)] - 14-Day Aerobic Processes.
❑ Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization.
❑ Alternative 7 [15A NCAC 02T.1107(a)(7)] - Drying of Stabilized Residuals.
❑ Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals.
❑ Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection.
❑ Alternative 10 [15A NCAC 02T.I107(a)(10)] - Incorporation.
❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [ 15A NCAC 02T.I 107(b)(2)].
❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5

Attachment C
PAN Calculations

31,854.00
2,103.00
2,999.00
0.40
Application and PAN
PAN= [min.rate (TKN - NH3) + 0.5
First Year 1 0.40 1 29,751
rganic N Mineralized 1st Year
Residual PAN Calculation
Novozymes North America
01 LUZU +A
+ NO3-NO21 * 0.002
1,052
11,900.40 mg/Kg
PAN released from initial
....
.......
2
0.20
29,751
11,900
0
3
0.10
29,751
11,900
3,570
4
0.05
29,751
11,900
3,570
5
0.03
29,751
11,900
3,570
Cumulative
PAN Released Years 2 5
Tt J115/21
9,751.00
1,051.50
1,000.001
00
plication above
15,951 31.90
her In.`&
ora g0i
r ....
.......
...........
.. ........
0
0
31570
7.14
0
0
1,428
2.86
1,428
0
643
1.29
1,428
643
305
0.61
rig initial application
5,946.03
43.79

Attachment D
Site life Calcualtions for Three Application Rates

Adjusted Average SBM and Average RO Reject Scenario 3118/21
Site Life 40 CFR Part 503
Maximum Loading Rate 24,936 gallons at 150 # PAN/Ac 4.70 DT/Ac
.... . ..
.......... .
... ..... ..
poilatant
...............
Max
Application
Rate
... .... ... .....
lbs/DT.Ofe h P INt t.
as taken from attached
00*45
lbs.
POWWOW.
OPPIled:Ptr
Year
.. . .. ...... .
.
maximem AIJOWOW.�
Coweentra tJOn&Bg$Od--"�
..On 40:CFKPArt:503:;:
......... --------- -
- ------ --- --------
- ---------------
-------
-- -- --------------
-----------
--------------
. .... ..... ..
SiteUfeYtam - ---------
Arsenic
4.70
0.00295
0.01387
36.00
2,595
Cadmium
4.70
0.00014
0.00066
34.00
51,651
Copper
4.70
0.00925
0.04347
1,388.00
31,927
Lead
4.70
0.00122
0.00576
267.00
46,393
Mercury
4.70
0.00005
0.00023
15.00
66,462
Molybdenum
4.70
0.00147
0.00689
89.00
12,912
Nickel
4.70
0.00199
0.00935
374.00
40,011
Selenium
4.70
0.00241
0.01132
89-00
7,861
Zinc
4.70
0.02289
0.10762
2,498.00
23,212
The limiting site life is 2,595 years.
The limiting pollutant is Arsenic
Site Life 40 CFR Part 257 CEC 0 - 5 meq/100g
IMaximum Loading Rate 24,836 gallons at 150 # PAN/Ac 4.70 DT/Ac
Max
Application:
lbslo.Tofewchtollutantf
as taken ftom attached
Analysis
P.0flontant
OPPUCIVer:
you
Concentrations Based.
00 40 C FR Part 2$7
CEC 10 - 5
Arsenic
4.70
0.00295
0.01387
NA
NA
Cadmium
4.70
0.00014
0.00066
5.00
7,596
Copper
4.70
0.00925
0.04347
125.00
2,875
Lead
4.70
0.00122
0.00576
500,00
86,879
Mercury
4.70
0.00005
0.00023
NA
NA
Molybdenum
4.70
0,00147
0.00689
NA
NA
Nickel
4.70
0.00199
0.00935
125.00
13,373
Selenium
4.70
0.00241
0.01132
NA
NA
Zinc
4.70
0.02289
0,10762
250.00
2,323
limiting site life is 2,323 years.
limiting pollutant is Zinc
Site Life 40 CFR Part 257 CEC 5 - 15 meq/100g
Maximum Loading Rate 24,836 gallons at 150 # PAN/Ae 4.70 DT/Ac
Pollutant
Max
AppReAtIOnA
Rate
INIOT of each Poflutaat
as takerk flroM�Ottached
Analysis
lbs
Poliontant
applied per
year
Maximum Allowable:
Concentratiom Oased
on 4Q:CFR Part 257
CEC: 5 -15
------ ------
- --------------- ------- - ------------ ----------
----- --- - --
----------- --
.......... ........ ..
Sit LW ars
-W
Arsenic
4.70
0.00295
0.01387
NA
NA
Cadmium
4.70
0.00014
0.00066
10.00
15,191
Copper
4.70
0.00925
0.04347
250.00
5,751
Lead
4.70
0.00122
0.00576
1,000.00
173,757
Mercury
4.70
0.00005
0.00023
NA
NA
Molybdenum
4.70
0.00147
0.00689
NA
NA
Nickel
4.70
0.00199
0.00935
250.00
26,745
Selenium
4.70
0.00241
0.01132
NA
NA
Zinc
4.70
0.02289
0.10762
500.00
4,646
IThe limiting site life is 4,646 years.
The limiting pollutant is Zinc.
Site Life 40 CFR Part 257 CEC 15+ meq/100g
Maximum Loading Rate
24,836 gallons at 150 # PAN/Ac
4.70 DT/Ac
Max
A T:0040,X-011utafivl.
We to
..... . . . . I WII,;::.::::,;
V
k "eik ......
�ij�pp .
0 4 Or 2 .7
............
TEC ISO
S ...Life Years
Arsenic
4.70
0.00295
0.01387
NA
NA
Cadmium
4.70
0.00014
0.00066
20.00
30,383
Copper
4.70
0.00925
0.04347
500.00
11,501
Lead
4.70
0.00122
0.00576
2,000.00
347,514
Mercury
4.70
0.00005
0.00023
NA
NA
Molybdenum
4.70
0.00147
0.00689
NA
NA
Nickel
4.70
0.00199
0.00935
500.00
53,491
Selenium
4.70
0.00241
0.01132
NA
NA
Zinc
4.70
0.02289
1 0.10762
1,000.00
9,292
The limiting site life is
9,292 years.
The limiting
pollutant is
Zinc -
NA - Not Applicable for 257 comparisons

Adjusted Average SBM and Average RO Reject Scenario 3/18/21
Site Life 40 CFR Part 503
Loading rate at
6,000 gallons at 36.24# PAN/Ac
1.14 DT/Ac
.............
.....
.. ......
lb ......
......
...
........
.........
......... ...
.......
... ..............
..............
...
. a... ........ A.
:JW/D.T.:
:0 :0
...............
................
............... ............
i� !�TWWI Wt.-
.......
...........
................
. . . . . . . . . ..... ........
............. !III!
. : .............
............................................
............... ..................
...............................
... ........
....... ....
. ............
..............
ft-tIOW: ".d:
................ ....
::P.O.0 tan
4 M
ai
Arsenic
1.14
0.00295
0.00335
36.00
10,743
Cadmium
1.14
0.00014
0.00016
34.00
213,800
Copper
1.14
0.00925
0.01050
1,388.00
132,158
Lead
1.14
0.00122
0.00139
267.00
192,038
Mercury
1.14
0.00005
0.00005
15.00
275,110
Molybdenum
1.14
0.00147
0.00167
89.00
53,446
Nickel
1.14
0.00199
0.00226
374.00
165,620
Selenium
1.14
0.00241
0.00274
89.00
32,538
Zinc
1 1.14
1 0.02289
1 0.02600
2,498.00
96,082
limiting site life is
10,743 years.
IThe
The limiting pollutant
is
Arsenic
Site Life 40 CFR Part 257 CEC 0 - 5 meq/100g
Loading rate at
6,000 gallons at 36.24# PAN/Ac
1.14 DT/Ac
................ ...............
...
...
................
Mii ft: ...
...............................................
........
........
M.T:bf: -�i
iilv
................ ..........................
.......
...........
0.0lial"O.
10"k j f*
.7
........ ...... ............
'MV;1i
iiiiiiii R*
..
ar
.................... .............
C.
............
................
. . ....
Arsenic
1.14
0.00295
0.00335
NA
NA
Cadmium
1.14
0.00014
0.00016
5.00
31,441
Copper
1.14
0.00925
0.01050
125.00
11,902
Lead
1.14
0.00122
0.00139
500.00
359,621
Mercury
1.14
0.00005
0.00005
NA
NA
Molybdenum
1.14
0.00147
0.00167
NA
NA
Nickel
1.14
0.00199
0.00226
125.00
55,354
Selenium
1.14
0.00241
0.00274
NA
NA
Zinc
1.14
0.02289
0.02600 1
250.00
9,616
The limiting site life is
9,616 years.
The limiting pollutant
is
Zinc
Site Life 40 CFR Part 257 CEC 5 - 15 meq/100g
Loading rate at
6,000 gallons at 36.24# PAN/Ac
1.14 DT/Ac
MMAllowable I
...A" ..... -Aw,
.......... .. ...
..........
...............
..........
....... M., .........
ga
......
i�wpii ut-.�Ont�
::yow.
ow Bit $0
.....
on:::
...
WOhIYiO,IU,,4'ft "Aw,
::4010 .0:0 ....
..............
.....
..
Arsenic
1.14
0.00295
0.00335
NA
NA
Cadmium
1.14
0.00014
0.00016
10.00
62,882
Copper
1.14
0.00925
0.01050
250.00
23,804
Lead
1.14
0.00122
0.00139
1,000.00
719,243
Mercury
1.14
0.00005
0.00005
NA
NA
Molybdenum
1.14
0.00147
0.00167
NA
NA
Nickel
1.14
0.00199
0.00226
250.00
110,708
Selenium
1.14
0.00241
0.00274
NA
NA
Zinc
1.14
0.02289
1 0.02600
500.00
19,232
The limiting site life is
19,232 years.
The limiting_pollutant
is
Zinc
Site Life 40 CFR Part 257 CEC 15+ meq/100g
Loading rate at
6,000 gallons
at 36.24# PAN/Ac
1.14 DT/Ac
OV M.8
ro VON b. T. f
Pli
Vouutao
Arsenic
1.14
0.00295
0.00335
NA
NA
Cadmium
1.14
0.00014
0.00016
20.00
125,765
Copper
1.14
0.00925
0.01050
500.00
47,607
Lead
1.14
0.00122
0.00139
2,000.00
1,438,485
Mercury
1.14
0.00005
0.00005
NA
NA
Molybdenum
1.14
0.00147
0.00167
NA
NA
Nickel
1.14
0.00199
0.00226
500.00
221,417
Selenium
1.14
0.00241
0.00274
NA
NA
Zinc
1.14
0.02289
0.02600
1,000.00
38,464
The limiting site life is
38,464 years.
The limiting
pollutant is
Zinc
NA - Not Applicable for 257 comparisons

Adjusted Average SBM and Average Rd Reject Scenario 3/18/21
Site Life 40 CFR Part 503
Loading rate at
12,000 gallons at 72.48 # PAN/Ac
2.27 DT/Ac
............
...........
..........................................
.....................
...........
.... . .
.....
.......
......
...........
.........
1VkaatWD.T.
lo.:each Palku awiv:
....
OWIft 't,
......... 4.
........ ....
................ ...
:: ....... 0,10'a .ttri ...........
:
..............
.............
............
...........
a
................
...............
ten I OM .
......
.....................
.......
.........................
j:j:j:i:j
P
rs
.............................
Arsenic
2.27
0.00295
0.00670
36.00
5,372
Cadmium
2.27
0.00014
0.00032
34.00
106,900
Copper
2.27
0.00925
0.02101
1,388.00
66,079
Lead
2.27
0.00122
0.00278
267.00
96,019
Mercury
2.27
0.00005
0.00011
15.00
137,555
Molybdenum
2.27
0.00147
0.00333
89.00
26,723
Nickel
2.27
0.00199
0.00452
374.00
82,810
Selenium
2.27
0.00241
0.00547
89.00
16,269
Zinc
1 2.27
1 0.02289
1 0.05200
1 2,498.00
1
48,041
The limiting site life Is
5,372 years.
The limiting
pollutant is
Arsenic
Site Life 40 CFR Part 257 CEC 0 - 5 meq/100g
Loading rate at
12,000 gallons at 72.48 # PAN/Ac
2.27 DT/Ac
....
.......
........
............. .
.......
****'*'*'
.
................................
*- Abl"', XMIUM: O.W.-
------
.............
- ...... ..............
.
..........
........
bf--:66 l P�
..
40
.......
......................
ll ..
p!pr l l
........
lilllio"A
0114
.
..............
YO
C.0
...............
...
$1 w . ...........
Arsenic
2.27
0.00295
0.00670
NA
NA
Cadmium
2.27
0.00014
0.00032
5.00
15,721
Copper
2.27
0.00925
0.02101
125.00
5,951
Lead
2.27
0.00122
0.00278
500.00
179,811
Mercury
2.27
0.00005
0.00011
NA
NA
Molybdenum
2.27
0.00147
0.00333
NA
NA
Nickel
2.27
0.00199
0.00452
125.00
27,677
Selenium
2.27
0.00241
0.00547
NA
NA
Zinc
2.27
0.02289
0.05200
250.00
4,808
limiting site life is 4,808 years.
limiting pollutant Is Zinc
Site Life 40 CFR Part 257 CEC 5 - 15 meq/100g
Loading rate at
12,000 gallons at 72.48 # PAN/Ac
2.27 DT/Ac
. ...........
...
...............
..... . ....
...... .
..... .
r 0 i0i
::Mol Win .4
..........
1k.0blif. imt kWiii!
ii:a
::OW
:J
Arsenic
2.27
0.00295
0.00670
NA
NA
Cadmium
2.27
0.00014
0.00032
10.00
31,441
Copper
2.27
0.00925
0.02101
250.00
11,902
Lead
2.27
0.00122
0.00278
1,000.00
359,621
Mercury
2.27
0.00005
0.00011
NA
NA
Molybdenum
2.27
0.00147
0.00333
NA
NA
Nickel
2.27
0.00199
0.00452
250.00
NA
Selenium
2.27
0.00241
0.00547
NA
NA
Zinc
2.27
0.02289
0.05200
500.00
9,616
The limiting site life is
9,616 years.
The limiting pollutant
is
Zinc
Site Life 40 CFR Part 257 CEC 15+ meq/100g
Loading rate at
12,000 gallons
at 72.48 # PAN/Ac
2.27 DT/Ac
.....
Y-T
iir.�666t iw Ion . 4
00t 0OW
.......
..""
s og--1
it
Arsenic
2.27
0.00295
0.00670
NA
NA
Cadmium
2.27
0.00014
0.00032
20.00
62,882
Copper
2.27
0.00925
0.02101
500.00
23,804
Lead
2.27
0.00122
0.00278
2,000.00
719,243
Mercury
2.27
0.00005
0.00011
NA
NA
Molybdenum
2.27
0.00147
0.00333
NA
NA
Nickel
2.27
0.00199
0.00452
500.00
110,708
Selenium
2.27
0.00241
0.00547
NA
NA
Zinc
2.27
0.02289
0.05200
1,000.00
19,232
limiting site life is 19,232 years.
Is Zinc
NA - Not Applicable for 257 comparisons

Novozymes No. Version Page
My MS Document NZNAEO-42 10.0 1 of 2
Spent BioMass Operations & Maintenance Plan
Permit No. WQ0003487
Purpose This document provides information on operation and maintenance of
processes and equipment pursuant to and required by the regulatory
permit governing treatment and distribution of spent production bio-
mass.
Operations The following procedures cover operation of equipment and activities for
spent biomass:
Spills
Spent biomass treatment systems:
NZNAEO-48
FHG Line Treatment System
NZNAEO-47
FHG 407A & B Storage/Transfer Tanks
NZNAEO-46
FFI Lime Treatment System
NZNAEO-14
FHG 406AT Emergency Storage Tank
Spent biomass land application:
NZNAEO-12
SMB Transport
NZNAEO-13
Land Application of SBM
NZNAEO-13a
SBM Daily Application Sheet
NZNAEO-15
SBM FLF 96A, B, C Tanks
NZNAEO-21
SBM Applied Database
NZNAEO-27
SBM LANDOWNERS AGREEMENT
NZNAEO-50
Compliance Inspection
NZNAEO-50a
Site Inspections for SBM Land Application
NZNAEO-78
Daily SBM Sampling FLF96 Tanks
NZNAEO-37
Sent Biomass Spill Prevention and Control Plan
NZNASafe-2.01a
Emergency Action Plan
NZNASafe-2.32
Off -site Spent Biomass Spill or Release
Prepared by
SOCR (Scott Creech)
Valid from
16-03-2021
Continued on next page

Novozymes No. Version Page
My MS Document NZNAEO-42 10.0 2 of 2
Spent BioMass Operations & Maintenance Plan
Permit No. WQ0003487, Continued
Operational
Control NOAA Forecast and Accuweather Mobile Apps are the Data
Limits source for making the determination.
Winter Operation (November-
Summer Operation (April -October)
March)
If >50% chance of precipitation
If >60% chance of precipitation 0.5in+
0.5in.+ over the next 24 hours,
over the next 24 hours, increase buff -
residuals application will not
ers around surface waters, ditches,
proceed.
and meadow strips by 100%.
If >75% chance of precipitation 0.5in+
outside of hours of operation, operate
half -day schedule.
If >75% chance of precipitation 0.5in+
within hours of operation, residuals
application will not proceed.
Maintenance Equipment maintenance is planned and conducted:
a. in the site -wide SAP system for work orders, and
b. with local vendors for SBM tractor and wagon repairs
Safety Operations are conducted per:
a. site -wide safety training, and
b. safe equipment operating practices as provided by vendors and
equipment operating manuals
Revisions 3/16/21 - ]BUR - Adjusted format
9/3/2019 - removed NZNAEO-17 Contract SBM hauling database
Prepared by Valid from
SOCR (Scott Creech) 16-03-2021